III.F. Environmental Reports - 2015-03-11 Terracon LSI-OCR

Limited Site Investigation
Proposed City of Durham Police Headquarters
113 S. Elizabeth Street, 601 E. Ramseur Street, 605 E. Ramseur Street,
101 S. Elizabeth Street, 616 E. Main Street, and 102 Hood Street
Durham, Durham County, North Carolina
March 11, 2015
Terracon Project No. 70157304
Prepared for:
City of Durham
Durham, North Carolina
Prepared by:
Terracon Consultants, Inc.
Raleigh, North Carolina
TABLE OF CONTENTS
ii
1.0 SITE DESCRIPTION ....................................................................................................... 1
1.1 113 S. Elizabeth Street ........................................................................................ 1
1.2 601 E. Ramseur Street......................................................................................... 3
1.3 101 S. Elizabeth Street ........................................................................................ 3
1.4 616 E. Main Street ............................................................................................... 4
2.0 SCOPE OF SERVICES ................................................................................................... 4
2.1 Standard of Care.................................................................................................. 4
2.2 Additional Scope Limitations ................................................................................ 4
2.3 Reliance ............................................................................................................... 5
3.0 FIELD INVESTIGATION ................................................................................................. 5
3.1 Soil Borings.......................................................................................................... 5
4.0 RESULTS OF THE FIELD INVESTIGATION .................................................................. 9
4.1 Geology ............................................................................................................... 9
4.2 Field Screening .................................................................................................... 9
5.0 ANALYTICAL RESULTS ................................................................................................ 9
5.1 Soil Sample Results ............................................................................................. 9
5.1.1 113 S. Elizabeth Street Parcel .................................................................. 9
5.1.2 101 S. Elizabeth Street Parcel ................................................................ 10
5.1.3 601 E. Ramseur Street Parcel ................................................................ 11
5.1.4 616 E. Main Street Parcel ....................................................................... 11
5.2 Potential for Vapor Intrusion ............................................................................... 11
6.0 CONCLUSIONS ............................................................................................................ 12
7.0 RECOMMENDATIONS ................................................................................................. 12
APPENDICES
APPENDIX A:Exhibit No. 1 – Topographic Vicinity Map
Exhibit No. 2 – Site Layout and Current Occupants
Exhibit No. 3 – Boring Locations
Exhibit No. 4 – TPH-DRO Results (SB-1 to SB-14)
Exhibit No. 5 – TPH-DRO Results (SB-15 to SB-39)
Exhibit No. 6 – TPH-DRO Results (SB-40 to SB-54)
APPENDIX B:Table 1 – Summary of Soil Analytical Data for TPH Analysis
Table 2 – Summary of Soil Analytical Data for VOC Analysis
APPENDIX C:Soil Boring Logs
APPENDIX D:Laboratory Analytical Reports and Chain of Custody Records
Responsive ■Resourceful ■Reliable 1
LIMITED SITE INVESTIGATION
PROPOSED CITY OF DURHAM POLICE HEADQUARTERS
113 S. ELIZABETH STREET, 601 E. RAMSEUR STREET, 605 E. RAMSEUR STREET,
101 S. ELIZABETH STREET, 616 E. MAIN STREET, AND 102 HOOD STREET
DURHAM, DURHAM COUNTY, NORTH CAROLINA
Terracon Project No. 70157304
March 11, 2015
1.0 SITE DESCRIPTION
The site consists of six parcels totaling 4.5 acres located in downtown Durham, Durham County,
North Carolina, within the city block formed by S. Elizabeth Street to the north, E. Main Street to
the east, Hood Street to the south, and E. Ramseur Street to the west (Exhibit No. 1). Walker
Street bisects the east end of the site in a north-south orientation. Walker Street is included in
the site as it is owned by the current site owner and not a public street. The site encompasses
the following addresses: 113 S. Elizabeth Street, 601 E. Ramseur Street, 605 E. Ramseur
Street, 101 S. Elizabeth Street, 616 E. Main Street, and 102 Hood Street.
The following site features and/or historical uses were identified during completion of a
Phase I Environmental Site Assessment (ESA) (Terracon Project No. 70147828 dated
December 19, 2014), during conversations with Mr. Mark Carpenter (current property owner),
and subsequent site visits. Site features are shown Exhibits No. 2 and 3.
1.1 113 S. Elizabeth Street
Terracon observed and/or understands the following areas of concern (AOCs), which are
depicted on Exhibits No. 4 and 5, on the 113 S. Elizabeth Street parcel:
n Two 6,000-gallon gasoline underground storage tanks (USTs) were formerly located
near the northeast corner of the existing Carolina Auto Masters building. The original
6,000-gallon gasoline UST (Tank 1) was removed in 1988 and an unreported quantity of
soil was excavated. The second 6,000-gallon gasoline UST (Tank 1A) was installed in
its place and removed in 1997.
n A 1,000-gallon diesel UST (Tank 3) and a 2,000-gallon waste oil UST (Tank 2) were
formerly located in the center of the parking lot to the north of the Cider Works facility.
n A 2,000-gallon waste oil UST (Tank 2A) was formerly located on the east end of the auto
service garage/warehouse building located at 113 S. Elizabeth Street and removed in
1997.
n One former below-ground truck repair pit within the Cider Works facility. The pit is
currently covered by a refrigeration unit. According to Mr. Carpenter, the pit had a
ladder or stairs to access the pit and allowed for large trucks to be parked over the pit
Limited Site Investigation
Proposed City of Durham Police Headquarters ■ Durham, North Carolina
March 11, 2015 ■ Terracon Project No. 70157304
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while employees worked on trucks from within the pit. He was unaware of any drains
within the pit and indicated the pit was mostly filled with concrete years ago.
n One sump pit (or possible oil/water separator) located along the southern wall within the
former auto repair area. According to Mr. Carpenter, the trench drains that are oriented
west-east in the still active auto repair area gravity drain to the sump pit. The sump pit
reportedly formerly drained to the city sewer system extending along Hood Street.
n One oil/water separator was observed within the Cider Works facility. According to
Mr. Carpenter, the oil/water separator was formerly associated with the truck repair
operations and had not been utilized for many years. He indicated the unit drained to a
storm water drain north of the building.
n Evidence of numerous former in-ground hydraulic lifts was observed within the former
auto service area. Terracon estimates approximately 15 former lifts; however, an exact
number could not be determined due to the presence of objects stored within the
building at the time of the site reconnaissance. Each lift contained a small hydraulic oil
tank contained in sub-grade concrete vaults. According to Mr. Mark Carpenter, the lifts
have been abandoned by filling the vaults with sand and covering the vaults with
concrete.
n Three unidentified in-ground ports and associated underground piping, which appeared
to be interconnected, were observed in an east-west orientation, within the center of the
Durham Collision facility. When opened, the ports exhibited an obvious petroleum odor.
n An interior floor drain was observed within the service bay area associated with the
Carolina Auto Masters facility. The floor drain reportedly discharges to the municipal
sewer or storm water system
n Within the Carolina Auto Masters tenant space and the Durham Auto Center, Terracon
observed numerous containers including five 55-gallon plastic drums of used oil, one
55-gallon plastic drum of antifreeze, five 19-gallon drums of racing fuel, a parts washer
with petroleum solvent, and several smaller containers of petroleum products including
hydraulic fluid, transmission fluid, new and used oil, fuel additives, etc. The containers
were observed to be stored on the concrete floor of the buildings. Surficial staining was
observed on the concrete floor beneath the containers.
n Numerous areas of stained concrete were observed within the current and former
service bay areas associated with auto repair operations. The staining appeared to be
contained on the concrete floor within the building.
Limited Site Investigation
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March 11, 2015 ■ Terracon Project No. 70157304
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1.2 601 E. Ramseur Street
Terracon observed and/or understands the following AOCs, which are depicted on
Exhibit No. 3, on the 601 E. Ramseur Street parcel:
n This property was formerly occupied by P&H Engineering & Mfg. Co., which
manufactured and assembled airplane and electronic components during the 1980s.
Additionally, operations of a former tenant during the 2000s included auto detailing and
collision repair.
n A suspect UST was identified via ground penetrating radar (GPR) near the southwestern
property boundary during utility location activities conducted prior to drilling. The
suspect UST measured approximately 7 feet long by 3 feet wide.
1.3 101 S. Elizabeth Street
Terracon observed and/or understands the following AOCs, which are depicted on
Exhibit No. 6, on the 101 S. Elizabeth Street parcel:
n An on-site filling station, formerly located at the corner of S. Elizabeth Street & Walker
Street, operated during the 1930s until at least the 1950s. Two former USTs are
depicted on historical Sanborn fire insurance maps along S. Elizabeth Street and one
UST is depicted along Walker Street. Terracon did not observe evidence of current
USTs and the status of the three USTs is unknown.
n Auto service/repair operations occurred on this parcel since the late 1920s, which
included the operation of a paint booth with an apparently associated floor drain, within
the building since at least the 1930s.
n An interior floor drain was observed within the former service bay area in the current
vocational training center. The floor drain reportedly discharges to the municipal sewer
or storm water system.
n Numerous areas of stained concrete were observed within the current and former
service bay areas associated with auto repair operations. The staining appeared to be
contained on the concrete floor within the building.
Limited Site Investigation
Proposed City of Durham Police Headquarters ■ Durham, North Carolina
March 11, 2015 ■ Terracon Project No. 70157304
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1.4 616 E. Main Street
Terracon observed and/or understands the following AOCs, which are depicted on
Exhibit No. 6, on the 616 E. Main Street parcel:
n A former filling station with the undocumented removal of up to three 250-gallon USTs in
1988, operated on the northwestern portion of this parcel during the 1930s. A Sanborn
fire insurance map identified at least two USTs in this area.
n An auto sales and service building is depicted on the southeastern portion of this parcel
in the historical Sanborn fire insurance maps during the 1930s and 1950s.
n Prior reports depict two 1,000-gallon fuel oil USTs on this parcel. The reported UST use
was associated with fueling building furnaces. The tanks were reportedly removed in
1988 and closure reports are not available as this pre-dates UST closure reporting
requirements.
2.0 SCOPE OF SERVICES
At the request of the client, Terracon’s LSI was conducted to investigate the presence or
absence of indicator contaminants associated with the identified AOCs mentioned above. The
scope work is not intended to provide complete delineation, but will provide sufficient data to
evaluate the AOCs and better define potential costs and environmental liabilities associated with
potential purchase or lease of the site.
2.1 Standard of Care
Terracon’s services were performed in a manner consistent with generally accepted practices of
the profession undertaken in similar studies in the same geographical area during the same
time. Terracon makes no warranties, either express or implied, regarding the findings,
conclusions, or recommendations. Please note that Terracon does not warrant the work of
laboratories, regulatory agencies, or other third parties supplying information used in the
preparation of the report. These LSI services were performed in accordance with the scope of
work agreed with you, our client, as reflected in Terracon’s Proposal No. P70150027, dated
January 13, 2015 and were not restricted by ASTM E1903-11.
2.2 Additional Scope Limitations
Findings, conclusions, and recommendations resulting from these services are based upon
information derived from the on-site activities and other services performed under this scope of
work; such information is subject to change over time. Certain indicators of the presence of
hazardous substances, petroleum products, or other constituents may have been latent,
Limited Site Investigation
Proposed City of Durham Police Headquarters ■ Durham, North Carolina
March 11, 2015 ■ Terracon Project No. 70157304
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inaccessible, unobservable, non-detectable, or not present during these services. We cannot
represent that the site contains no hazardous substances, toxic materials, petroleum products,
or other latent conditions beyond those identified during this LSI. Subsurface conditions may
vary from those encountered at specific borings or wells or during other surveys, tests,
assessments, investigations, or exploratory services. The data, interpretations, findings, and our
recommendations are based solely upon data obtained at the time and within the scope of these
services.
2.3 Reliance
This report has been prepared for the exclusive use of the City of Durham, and any
authorization for use or reliance by any other party (except a governmental entity having
jurisdiction over the site) is prohibited without the express written authorization of the City of
Durham and Terracon. Any unauthorized distribution or reuse is at the City of Durham’s sole
risk. Reliance by authorized parties will be subject to the terms, conditions, and limitations
stated in Terracon’s Proposal No. P70150027 dated January 13, 2015, and the Agreement for
Services between the City of Durham and Terracon. The limitation of liability defined in the
terms and conditions is the aggregate limit of Terracon’s liability to the City of Durham and all
relying parties unless otherwise agreed in writing.
3.0 FIELD INVESTIGATION
Field activities were conducted from February 10 through February 12, 2015. Terracon
conducted the fieldwork under a health and safety plan developed for this project. Work was
performed using United States Environmental Protection Agency (USEPA) Level D work attire
consisting of hard hats, safety glasses, protective gloves, and protective boots. Additionally,
Terracon contacted the North Carolina 811 and requested location and markings for utilities that
the service was responsible for before commencing intrusive activities at the site. In an attempt
to identify sub-grade utility lines at the site and evaluate for potential USTs, Terracon also
supervised GPR and electromagnetic (EM) surveys of the AOCs. The GPR and EM surveys
along with boring layout were conducted on February 4, 2015.
3.1 Soil Borings
Investigation activities were focused on twenty-five targeted AOCs on four of the six site parcels
as identified during the completion of the Phase I ESA. A total of 54 soil borings were
conducted in these areas. The completed soil borings were advanced by a North
Carolina-licensed well driller utilizing a track-mounted direct-push technology (DPT) Geoprobe
6712DT drill rig. The approximate locations of the 54 soil borings are shown on Exhibit No. 3.
Limited Site Investigation
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March 11, 2015 ■ Terracon Project No. 70157304
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Thirty-nine borings (SB-1 through SB-39) were conducted on the 113 S. Elizabeth Street parcel.
The borings were placed in the following locations:
n Boring SB-1 was located within the western third of the Cider Works facility, adjacently
west of a suspected oil/water separator UST, and advanced to approximately 10 feet
below land surface (bls);
n Boring SB-2 was located within the central third of the Cider Works facility, adjacently
north of the former truck pit, and advanced to approximately 8 feet bls;
n Boring SB-3 was located within the eastern third of the Cider Works facility, adjacently
east of an apparent drain sump, and advanced to approximately 8 feet bls;
n Boring SB-4 was located within the central portion of the Carolina Auto Masters facility,
adjacent to a floor drain, and advanced to approximately 8 feet bls;
n Borings SB-5 through SB-8 were located adjacent to the northeast corner of the Carolina
Auto Masters facility, adjacent to an area that formerly contained two 6,000-gallon
gasoline USTs, and advanced to approximately 15 to 17.5 feet bls;
n Borings SB-9 through SB-12 were located in the center of the parking lot to the north of
the Cider Works facility, adjacent to an area that formerly contained one 2,000-gallon
waste oil UST and/or one 1,000-gallon diesel UST, and advanced to approximately 12 to
14.5 feet bls;
n Borings SB-13 and SB-14 were located adjacent to a storm drain located in the center of
the parking lot to the north of the Cider Works facility and advanced to approximately
8 feet bls.
n Borings SB-15 through SB-18 were located, adjacently east of the Durham Collision
facility around an area that formerly contained one 2,000-gallon waste oil UST, and
advanced to approximately 12 to 14 feet bls;
n Borings SB-19, SB-21, SB-22, and SB-24 were located within the Durham Collision
facility, adjacent to former in-ground hydraulic lifts, and advanced to approximately
10 feet bls;
n Borings SB-20, SB-23, and SB-25 were conducted within the Durham Collision facility,
adjacent to unidentified, apparently interconnected ports, emitting petroleum odors, and
advanced to approximately 10 to 14 feet bls;
n Borings SB-26, SB-28, SB-29, SB-30, and SB-31 were located within the Lo Mo Market
Food Truck facility, adjacent to in-ground hydraulic lifts, and advanced to approximately
10 feet bls;
n Borings SB-27, SB-32, and SB-33 were located with the Lo Mo Market Food Truck
facility, adjacent to the trench drains and associated drainage sump, and advanced to
approximately 10 to 13 feet bls;
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n Borings SB-34 through SB-35 were located within the southern portion (wash bay) of the
Custom Stone facility along the trench drain and advanced to approximately 9.5 to
10 feet bls;
n Borings SB-36 and SB-37 were located within the northern portion of the Custom Stone
facility along the trench drain and advanced to approximately 4 to 6 feet bls;
n Boring SB-38 was located within the northern portion of the Custom Stone facility and
was advanced to approximately 9 feet bls; and
n Boring SB-39 was located within the central portion of the Custom Stone facility,
adjacent to an in-ground hydraulic lift, and advanced to approximately 9 beet bls.
Two borings (SB-40 and SB-41) were conducted on the 601 E. Ramseur Street parcel. The
borings were placed in the following locations:
n Boring SB-40 was located adjacently north of the Super Graphics facility and advanced
to approximately 10 feet bls; and
n Boring SB-41 was located adjacently west of the Super Graphics facility, adjacent to a
large bay door and a suspected UST identified by GPR implemented as part of the utility
location process completed prior to commencing drilling activities, and advanced to
approximately 10 feet bls.
Five borings (SB-42 and SB-46) were conducted on the 101 S. Elizabeth Street parcel. The
borings were placed in the following locations:
n Borings SB-42 and SB-43 were completed adjacently east of the northeast corner of
Carpenter building and advanced to approximately 12 feet bls;
n Boring SB-44 was located within the central portion of the vocational training facility,
adjacent to a floor drain, and advanced to approximately 10 feet bls; and
n Borings SB-45 and SB-46 were located within the storage warehouse, adjacently
southwest and northeast, respectively, of a floor drain near a former paint booth, and
were advanced to approximately 10 feet bls.
Eight borings (SB-47 and SB-54) were conducted on the 616 E. Main Street parcel. The
borings were placed in the following locations:
n Borings SB-47 through SB-49 were located on the northwest corner of this parcel in the
area of a former filling station with two to three former gasoline USTs and advanced to
approximately 12 feet bls; and
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n Borings SB-50 through SB-54 were located on the central portion of this parcel in the
area of two former 1,000-gallon fuel oil USTs and former automotive repair operations
and advanced to approximately 12 feet bls.
Soil samples were collected continuously from the borings via Macro-Core® samplers to
document soil type, relative moisture content, and other lithological characteristics. Each soil
sample was placed into a dedicated, re-sealable plastic bag and screened for organic vapors
using a 10.6 eV photoionization detector (PID). A summary of PID readings is included on the
soil boring logs in Appendix C.
Soils were generally characterized as brown, orange, gray, and tan sandy clays and clays from
the ground surface to approximately 5 to 10 feet bls before transitioning to a reddish brown silt.
DPT refusal was encountered in the reddish brown silt from approximately 13 to 17.5 feet bls.
On the southwestern portion of the building within the Custom Stone facility, DPT refusal was
met between 5 and 10 feet in partially weathered sandstone.
Based on the field screening results and to evaluate on-site AOCs, soil samples were collected
from 40 of the 54 completed borings for laboratory analysis. Refer to Tables 1 and 2 for a list of
collected samples and sample depths. The soil samples were collected and packed in sample
containers provided by Shealy Environmental Services, Inc. (Shealy). The sample containers
were packed in ice and shipped via FedEx along with chain of custody documentation to Shealy
in West Columbia, South Carolina (NCDENR Certification #329). Soil samples were collected
for select laboratory analysis, which may have included the following, depending on the targeted
contaminants of concern in a given AOC:
n Total petroleum hydrocarbons (TPH) – diesel range organics (DRO) via EPA Method
8015/3550;
n TPH – gasoline range organics (GRO) via EPA Method 8015/5030;
n TPH – oil and grease via EPA Method 8015/9071; and
n Volatile organic compounds (VOCs) via EPA Method 8260B.
The drilling equipment used in the field was thoroughly decontaminated prior to use and
between each sample collection point. All non-dedicated sampling equipment was
decontaminated using a Liquinox®/water wash followed by a distilled water rinse.
Investigative-derived wastes (i.e. wash/rinse water, soil cuttings, etc.) were containerized in one
55-gallon drum and staged on-site.
Limited Site Investigation
Proposed City of Durham Police Headquarters ■ Durham, North Carolina
March 11, 2015 ■ Terracon Project No. 70157304
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4.0 RESULTS OF THE FIELD INVESTIGATION
4.1 Geology
The boring logs detail the observed soil lithology and are located in Appendix C. In general,
Terracon encountered brown, orange, gray, and tan sandy clays and clays (CL and CH) to
approximately 5 to 10 feet bls before transitioning to a reddish brown silt (ML). DPT refusal was
encountered in reddish brown silt from approximately 13 to 17.5 feet bls. On the southwestern
portion of the building within the Custom Stone facility, DPT refusal was met between 5 and
10 feet in partially weathered sandstone. Groundwater was not encountered in the completed
borings.
4.2 Field Screening
The field screening results are summarized on the boring logs in Appendix C. PID readings
were detected in soil collected from the borings ranging from below one parts per million (ppm)
to approximately 958.9 ppm. Petroleum odors were observed in several of the completed
borings. Refer to the attached soil boring logs provided in Appendix C for depths and location of
observed petroleum odors.
5.0 ANALYTICAL RESULTS
Analytical data is summarized in Appendix B. The laboratory analytical reports and
chain-of-custody records are attached in Appendix D. The following sections describe the
results of the sampling. Reported concentrations from soil samples were compared to the
NCDENR Action Levels, Soil-to-Groundwater Maximum Soil Contaminant Concentrations
(MSCCs) and Industrial/Commercial Soil Cleanup Levels.
5.1 Soil Sample Results
5.1.1 113 S. Elizabeth Street Parcel
TPH Analysis
TPH-DRO concentrations exceeded NCDENR’s Action Level of 10 milligrams per kilogram
(mg/kg) in 25 of 29 samples with concentrations up to 50,000 mg/kg. The highest observed
concentrations were in the vicinity of former hydraulic lifts, former USTs, and the unidentified
ports.
TPH-Oil & Grease concentrations exceeded NCDENR’s Action Level of 10 mg/kg in 4 of 16
samples with concentrations up to 510 mg/kg. The highest observed concentrations were in the
vicinity of former USTs.
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A review of sample chromatograms by the laboratory confirmed the peaks identified in the
method blank did not correspond with peaks observed in the DRO analysis of samples from the
113 S. Elizabeth Street parcel with the exception of samples SB-13 (2’-4’) and SB-14 (6’-8’),
which may be a result of laboratory contamination. Thus, DRO detections and concentrations in
site samples are considered valid with the exception of samples SB-13 (2’-4’) and SB-14 (6’-8’).
Chromatograph patterns from the 113 S. Elizabeth Street parcel are consistent with patterns for
motor oil, fuel oil, and gasoline. Refer to Table 1 for sample specific pattern matches.
Volatile Organic Compounds
The following soil samples had concentrations of VOCs above their NCDENR
Soil-to-Groundwater MSCCs:
n Boring SB-7 had concentrations of ethylbenzene (26 mg/kg), isopropylbenzene
(5.8 mg/kg), toluene (50 mg/kg), and total xylenes (140 mg/kg) above their respective
NCDENR Soil-to-Groundwater MSCCs; and
n Boring SB-16 had a concentration of tetrachloroethene (0.0091 mg/kg) above its
NCDENR Soil-to-Groundwater MSCC.
VOC concentrations were not detected above NCDENR’s Industrial/Commercial Soil Cleanup
Levels.
5.1.2 101 S. Elizabeth Street Parcel
TPH Analysis
TPH-DRO concentrations exceeded NCDENR’s Action Level of 10 mg/kg in 3 of 4 samples with
concentrations up to 150 mg/kg. The highest observed concentrations were in the vicinity of
former USTs.
TPH-GRO concentrations exceeded NCDENR’s Action Level of 10 mg/kg in one sample in the
vicinity of former USTs.
A review of sample chromatograms by the laboratory confirmed the peaks identified in the
method blank did not correspond with peaks observed in the DRO analysis of samples from the
101 S. Elizabeth Street parcel. Thus, DRO detections and concentrations in site samples are
considered valid. Chromatograph patterns from the 101 S. Elizabeth Street parcel are
consistent with patterns for motor oil.
Volatile Organic Compounds
Soil samples did not contain concentrations of VOCs above the laboratory’s reporting limit.
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5.1.3 601 E. Ramseur Street Parcel
Volatile Organic Compounds
Soil samples did not contain concentrations of VOCs above the laboratory’s reporting limit.
5.1.4 616 E. Main Street Parcel
TPH Analysis
TPH-DRO concentrations exceeded NCDENR’s Action Level of 10 mg/kg in 4 of 5 samples with
concentrations up to 59,000 mg/kg. The highest observed concentrations were in the vicinity of
former USTs.
TPH-GRO concentrations exceeded NCDENR’s Action Level of 10 mg/kg in 1 of 2 samples with
concentrations up to 21 mg/kg. The highest observed concentrations were in the vicinity of
former USTs.
TPH-Oil & Grease concentrations exceeded NCDENR’s Action Level of 10 mg/kg in 1 of 3
samples in the vicinity of former USTs.
A review of sample chromatograms by the laboratory confirmed the peaks identified in the
method blank did not correspond with peaks observed in the DRO analysis of samples from the
site. Thus, DRO detections and concentrations in site samples are considered valid.
Chromatograph patterns from the 113 S. Elizabeth Street parcel are consistent with patterns for
motor oil.
5.2 Potential for Vapor Intrusion
The potential for vapor intrusion was evaluated based on the ITRC Petroleum Vapor Intrusion:
Fundamentals of Screening, Investigation, and Management (PVI-1), the NCDENR Non-
Residential Vapor Intrusion Screening Levels (VISLs), and analytical data from the soil samples
collected at the site.
Site data indicates that VOC concentrations are not anticipated to pose a vapor intrusion
concern.
Limited Site Investigation
Proposed City of Durham Police Headquarters ■ Durham, North Carolina
March 11, 2015 ■ Terracon Project No. 70157304
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6.0 CONCLUSIONS
Based on the scope of services described in this report and subject to the limitations described
herein, Terracon concludes the following:
n A suspect UST was identified adjacent to the western exterior of the building located on
the 601 E. Ramseur Street parcel.
n Based on DRO detections consistent with fuel oil, there is a potential that additional
unidentified USTs may exist at the site.
n TPH was reported above NCDENR Action Levels in 32 of 38 soil samples collected at
the site.
n VOC concentrations were detected in two samples, SB-7 (ethylbenzene,
isopropylbenzene, toluene, and total xylenes) and SB-16 (tetrachloroethene), above
their respective soil-to-groundwater MSCCs.
n Based on existing data, soil impacts are not anticipated to pose a vapor intrusion
concern for existing buildings and further vapor intrusion evaluation is not warranted at
this time.
n Soil data indicates low level residual impacts of petroleum and possible solvents across
the site.
7.0 RECOMMENDATIONS
Terracon recommends the results from this Limited Site Investigation be reported to NCDENR
by the current property owner prior to purchase of the site by the City of Durham. At the
discretion of NCDENR, further investigation may be warranted to determine the extent of
impacts at the site.
APPENDIX A
Exhibit No. 1 – Topographic Vicinity Map
Exhibit No. 2 – Site Layout and Current Operations
Exhibit No. 3 – Boring Locations
Exhibit No. 4 – TPH-DRO Results (SB-1 to SB-14)
Exhibit No. 5 – TPH-DRO Results (SB-15 to SB-39)
Exhibit No. 6 – TPH-DRO Results (SB-40 to SB-54)
Copyright:© 2013 National Geographic Society, i-cubed
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70157304MTJ
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MTJ 2/24/15 2401 Brentwood Drive, Suite 107 Raleigh, NC 27612
Phone: [phone] Fax: [phone]
Topographic Vicinity Map
Proposed Durham Police HeadquartersDurham, Durham County, North Carolina
USGS TOPOGRAPHIC MAP
SOUTHWEST DURHAM, NC QUADRANGLE
2002
500 0 500 1,000 1,500 2,000 2,500 3,000 3,500 4,000 4,500 5,000250Feet
CONTOUR INTERVAL 10 FEET
A
B
C
D
E
F
G
H
I
Gravel Lot
(storage
o
f

s
t
o
n
e
and tile)
Canopy
J
K
Vacant
Vacant
grass cov
e
r
e
d
N
Parking fo
r

D
u
r
h
a
m

C
o
u
n
t
y

D
e
p
a
r
t
m
e
n
t
of Public
H
e
a
l
t
h
601 E. Ramseu
r

S
t
113 S. Elizabe
t
h

S
t
101 S. Elizabe
t
h

S
t
605 E. Ramse
u
r

S
t
616 E. Main S
t
102 Hood St
Hood St
W
a
l
k
e
r

S
t
R
a
m
s
e
u
r

S
t
S Elizabe
t
h

S
t
E
M
a
i
n

S
t
Newman

S
t
E
P
e
a
b
o
d
y

S
t
N Eliza
b
e
t
h

S
t
Com
m
e
r
c
e

S
t
E
M
a
i
n

S
t
Newma
n

S
t
NC OneMap, NC Center for Geographic Information and Analysis, NC 911 Board
Date:
Project No.
CMP
LCD
2
Drawn By:
Checked By:
12/17/14
1 inch = 80 feet
70157304
EXHIBITNO.Site Layout and Current Occupants
Phase I Environmental Site AssessmentProposed Durham Police HeadquartersDurham, Durham County, North Carolina0408020Feet
2401 Brentwood Drive, Suite 107 Raleigh, NC 27612
Phone: [phone] Fax: [phone]
A Super Graphic - 601 E. Ramseur St.B Auto Storage - 605 E. Ramseur St.C Carolina Auto Masters -
113 S. Elizabeth St.D
E Bull City Cider Works -
113 S. Elizabeth St.F Durham Collision Center Auto Repair
218 Hood St. G Benjamin Motors Sales Office -
206 Hood St. H CET Vocational Training -
101 S. Elizabeth St./600 E. Main St.I Office Building, multiple office tenants
101 S. Elizabeth St./600 E. Main St. J Vacant - 616 E. Main St.K Not Just Wings Snack Bar -
102 Hood St.
Current Occupant - Address
Site Boundary
Parcel Boundaries
Road
Structures
Legend
Lo Mo Market Food Truck Operation
113 S. Elizabeth St.
Auto Stora
g
e
Former Aut
o

R
e
p
a
i
r
Canopy
Vacant
N
N
R
S
T Former Air
p
l
a
n
e

&

E
l
e
c
t
r
o
n
i
c
Componen
t

M
a
n
u
f
a
c
t
u
r
i
n
g
&
Former Au
t
o

B
o
d
y

S
h
o
p
Current Au
t
o
Repair
&
Former Tru
c
k
and Auto
Service
Current
&
Former
Auto
Repair
Former A
u
t
o

R
e
p
a
i
r
and Serv
i
c
e
trench dra
i
n
trench dra
i
n
Former fuel oil USTs
(location unknown)
Former
Filling
Station
601 E. Ramse
u
r

S
t
113 S. Elizabe
t
h

S
t
101 S. Elizabe
t
h

S
t
605 E. Ramse
u
r

S
t
616 E. Main S
t
102 Hood St
For
m
e
r

F
i
l
l
i
n
g

S
t
a
t
i
o
n
MW-2
MW-1 MW-5D
MW-3
MW-4
Numerous

F
o
r
m
e
r

In-Groun
d
Hydraulic
L
i
f
t
s S
SB-1
SB-2
SB-3SB-4
SB-9
SB-5 SB-6
SB-7
SB-8
SB-40
SB-41
SB-43
SB-42
SB-15
SB-16SB-17
SB-21
SB-25
SB-23
SB-22
SB-19
SB-20
SB-33
SB-32
SB-30
SB-27
SB-29
SB-36
SB-34SB-35
SB-39
SB-38
SB-37
SB-52
SB-53
SB-54
SB-50
SB-51
SB-48SB-47
SB-49
SB-45
SB-46
SB-44
SB-12
SB-10
SB-11
SB-13
SB-18
SB-24
SB-31
SB-26
SB-28
SB-14
Hood St
W
a
l
k
e
r

S
t
S Elizabet
h

S
t
E
M
a
i
n

S
t
R
a
m
s
e
u
r

S
t
E P
e
a
b
o
d
y

S
t
Newman

S
t
N Eliza
b
e
t
h

S
t
Date:
Project No.
CMP
MTJ
3
Drawn By:
Checked By:
2/19/15
1 inch = 60 feet
70157304
EXHIBITNO.Boring Locations
Proposed Durham Police HeadquartersDurham, Durham County, North Carolina0306015Feet
2401 Brentwood Drive, Suite 107 Raleigh, NC 27612
Phone: [phone] Fax: [phone]
Legend
Boring (sampled for VOCs & TPH)
Boring (sampled for TPH)
Boring (sampled for VOCs)
Borings (screened only)
Abandoned Monitoring Wells
Suspect UST
Former Paint Booth
Former Truck Pit
Oil Water Separator
Sump
Former Underground Storage Tank Pit
Former USTs as shown on Sanborn Maps
Site Boundary
Parcel Boundaries
Road
Structures
Canopy
FormerFilling Station
113 S. Elizabe
t
h

S
t
PB
73 B OilSB-15 (10'-12')
300 B OilSB-16 (8'-10')
9,500 B OilSB-19 (4'-6')
22 B OilSB-20 (2'-4')
1,000 B OilSB-21 (6'-8')50,000 B OilSB-22 (2'-4')
5,700 B Fuel OilSB-23 (2'-4')
2,700 B 2,700 BSB-24 (6'-8')
34 B OilSB-25 (0-2')
31 B OilSB-27 (8'-10')
420 B OilSB-28 (6'-8')
220 B OilSB-29 (6'-8')
24 B Fuel OilSB-4 (2'-4')
290 B GasolineSB-7 (10'-12')
24 B Motor OilSB-1 (4'-6')
39 BJ Motor OilSB-13 (2'-4')
24 B Motor OilSB-2 (6'-8')
24 B Motor OilSB-3 (6'-8')
5,300 B Motor OilSB-9 (10'-12')
3.3 BJ Motor Oil
SB-14 (6'-8')
SB-5
SB-6
SB-8
SB-12
SB-10
SB-11
S Elizabeth St
Date:
Project No.
CMP
MTJ
4
Drawn By:
Checked By:
3/9/15
1 inch = 20 feet
70157304
EXHIBITNO.Soil TPH-DRO Results (SB-1 to SB-14)
0 10 205Feet
2401 Brentwood Drive, Suite 107 Raleigh, NC 27612
Phone: [phone] Fax: [phone]
Proposed Durham Police HeadquartersDurham, Durham County, North Carolina
3.3 BJ Oil
SB-14 (6'-8')
Sample ID Sample Depth
TPH-DRO
Result
DRO Pattern
Match
Notes:
1) Results in milligrams per kilograms
2) Sample depth in feet below land surface
4) TPH-DRO: Total Petroleum Hydrocarbons
Diesel Range Organics
3) B: consituent was detected in laboratory
method blank
4) J: constituent detected at estimated
concentration between method detection
limit and practical quantitation limit
5) Concentrations in bold exceed NCDENR
Action Level
Legend
Boring (sampled for VOCs &
TPH)
Boring (sampled for TPH)
Boring (sampled for VOCs)
Boring (field screened only)
Former Truck Pit
Oil Water Separator
Sump
Former Underground Storage
Tank Pit
Site Boundary
Parcel Boundaries
Structures
StormDrain
FloorDrain
1
2
UST Pit Former Tank Volume (gallons)Content
1 6,000 Gasoline
1A 6,000 Gasoline
2 2,000 Waste Oil
3 1,000 Diesel
2
1
trench dra
i
n
PB
TP
trench dra
i
n
730 B Gasoline & Oil
SB-34 (0-2')
73 B Motor OilSB-15 (10'-12')
300 B Motor OilSB-16 (8'-10')
9,500 B Motor OilSB-19 (4'-6')
22 B Motor OilSB-20 (2'-4')
1,000 B Motor OilSB-21 (6'-8')50,000 B Motor OilSB-22 (2'-4')
5,700 B Fuel OilSB-23 (2'-4')
2,700 B Motor OilSB-24 (6'-8')
34 B Motor OilSB-25 (0-2')
360 B Motor OilSB-26 (6'-8')
31 B Motor OilSB-27 (8'-10')
420 B Motor OilSB-28 (6'-8')
220 B Motor OilSB-29 (6'-8')
1,200 B Motor OilSB-30 (5'-10')1,700 B Motor OilSB-31 (0-5')
70 B Motor OilSB-33 (8'-10')
730 B Gasoline &
Motor Oil
SB-34 (0-2')
4.7 BJ Unknown
SB-35 (2'-4')
6.1 BJ Unknown
SB-36 (2'-4')
2.7 BJ Unknown
SB-39 (4'-6')
110 B Motor OilSB-32 (8'-10')
3
Wash
Bay
SB-18
SB-17
SB-38
SB-37
Hood St
Date:
Project No.
CMP
MTJ
5
Drawn By:
Checked By:
3/9/15
1 inch = 20 feet
70157304 Soil TPH-DRO Results (SB-15 to SB-39)
0 10 205Feet
2401 Brentwood Drive, Suite 107 Raleigh, NC 27612
Phone: [phone] Fax: [phone]
Proposed Durham Police HeadquartersDurham, Durham County, North Carolina
3.3 BJ Oil
SB-14 (6'-8')
Sample ID Sample Depth
TPH-DRO
Result
DRO Pattern
Match
Notes:
1) Results in milligrams per kilograms
2) Sample depth in feet below land surface
4) TPH DRO: Total Petroleum Hydrocarbons
Diesel Range Organics
3) B: consituent was detected in laboratory
method blank
4) J: constituent detected at estimated
concentration between method detection
limit and practical quantitation limit
5) Concentrations in bold exceed NCDENR
Action Level
Legend
Boring (sampled for VOCs &
TPH)
Boring (sampled for TPH)
Boring (sampled for VOCs)
Boring (field screened only)
Unidentified Ports
Oil Water Separator
Sump
Former Underground Storage
Tank Pit
Site Boundary
Parcel Boundaries
Structures
EXHIBITNO.
UST Pit Tank
Volume (gallons)Content
3 2A 2,000 Waste Oil
Vacant
N
N
113 S. Elizabe
t
h

S
t
101 S. Elizab
e
t
h

S
t
616 E. Main S
t
102 Hood St
TP
OWS
73 B OilSB-15 (10'-12')
300 B OilSB-16 (8'-10')
9,500 BOilSB-19 (4'-6')
22 BOilSB-20 (2'-4')
1,000 B OilSB-21 (6'-8')50,000 BOilSB-22 (2'-4')
5,700 BFuel OilSB-23 (2'-4')
2,700 B2,700 BSB-24 (6'-8')
34 BOilSB-25 (0-2')
420 BOilSB-28 (6'-8')
1,700 BOilSB-31 (0-5')
730 B Gasoline & Oil
SB-34 (0-2')
24 BOilSB-1 (4'-6')
24 BOilSB-2 (6'-8')
24 BOilSB-3 (6'-8')
24 BFuel OilSB-4 (2'-4')
290 BGasolineSB-7 (10'-12')
5,300 BOilSB-9 (10'-12')
39 BJOilSB-13 (2'-4')
3.3 BJ Oil
SB-14 (6'-8')Canopy
150 B Motor OilSB-43 (4'-6')
2.3 BJ Unknown
SB-44 (2'-4')
12 B Motor OilSB-45 (4'-6')
12 B Motor OilSB-46 (2'-4')
87 BJ UnknownSB-49 (2'-4')
59,000 B Motor OilSB-52 (8'-10')
390 B Motor OilSB-53 (10'-12')
6.5 BJ Unknown
SB-54 (10'-12')
FloorDrain
FloorDrain
95 B Motor OilSB-47 (8'-10')
E M
a
i
n

S
t
W
a
l
k
e
r

S
t
Hood St
S Elizabeth S
t
SB-42
SB-50
SB-51
SB-48
Date:
Project No.
CMP
MTJ
6
Drawn By:
Checked By:
3/9/15
1 inch = 30 feet
70157304
EXHIBITNO.Soil TPH-DRO Results (SB-43 to SB-54)
0 10 20 305Feet
2401 Brentwood Drive, Suite 107 Raleigh, NC 27612
Phone: [phone] Fax: [phone]
Proposed Durham Police HeadquartersDurham, Durham County, North Carolina
3.3 BJ Oil
SB-14 (6'-8')
Sample ID Sample Depth
TPH-DRO
Result
DRO Pattern
MatchNotes:
1) Results in milligrams per kilograms
2) Sample depth in feet below land surface
4) TPH DRO: Total Petroleum Hydrocarbons
Diesel Range Organics
3) B: consituent was detected in laboratory
method blank
4) J: constituent detected at estimated
concentration between method detection
limit and practical quantitation limit
5) Concentrations in bold exceed NCDENR
Action Level
Legend
Boring (sampled for VOCs &
TPH)
Boring (sampled for TPH)
Boring (sampled for VOCs)
Boring (screened only)
Former Paint Booth
Former USTs as shown on
Sanborn Maps
Site Boundary
Parcel Boundaries
Structures
APPENDIX B
Table 1 – Summary of Soil Analytical Data for TPH Analysis
Table 2 – Summary of Soil Analytical Data for VOC Analysis
TPH GRO
(mg/kg)
TPH DRO
(mg/kg)
TPH Oil & Grease
(mg/kg)
SB-1 (4'-6')02/10/15 Cider Works OWS NA 24 B <240 Motor Oil
SB-2 (6'-8')02/10/15 Cider Works OWS NA 24 B <240 Motor Oil
SB-3 (6'-8')02/10/15 Cider Works sump NA 24 B <240 Motor Oil
SB-4 (2'-4')02/10/15 Carolina Auto Masters floor drain NA 24 B <250 Fuel Oil
SB-7 (12'-15')02/10/15 NE building corner near
Carolina Auto Masters two 6,000-gallon gasoline USTs NA 290 B <250 Gasoline
SB-9 (10'-12')02/10/15 center of parking lot north
of Cider Works
one 2,000-gallon waste oil UST and/or
one 1,000-gallon diesel UST NA 5,300 B 380 Motor Oil
SB-13 (2'-4')02/10/15 NA 39 BJ <300 Motor Oil
SB-14 (6'-8')02/10/15 NA 3.3 BJ <290 Motor Oil
SB-15 (10'-12')02/11/15 NA 73 B 510 Motor Oil
SB-16 (8'-10')02/11/15 NA 300 B 470 Motor Oil
SB-19 (4'-6')02/11/15 NA 9,500 B NA Motor Oil
SB-20 (2'-4')02/11/15 NA 22 B NA Motor Oil
SB-21 (6'-8')02/11/15 NA 1,000 B NA Motor Oil
SB-22 (2'-4')02/11/15 NA 50,000 B NA Motor Oil
SB-23 (2'-4')02/11/15 NA 5,700 B NA Fuel Oil
SB-24 (6'-8')02/11/15 NA 2,700 B NA Motor Oil
SB-25 (0-2')02/11/15 NA 34 B NA Motor Oil
SB-26 (6'-8')02/11/15 NA 360 B <230 Motor Oil
SB-27 (8'-10')02/11/15 NA 31 B <220 Motor Oil
SB-28 (6'-8')02/11/15 NA 420 B NA Motor Oil
SB-29 (6'-8')02/11/15 NA 220 B NA Motor Oil
SB-30 (5'-10')02/11/15 NA 1,200 B NA Motor Oil
SB-31 (0-5')02/11/15 NA 1,700 B NA Motor Oil
SB-32 (8'-10')02/11/15 NA 110 B <240 Motor Oil
SB-33 (8'-10')02/11/15 NA 70 B <260 Motor Oil
SB-34 (0-2')02/12/15 NA 730 B 430 Gasoline &
Motor Oil
SB-35 (2'-4')02/12/15 NA 4.7 BJ <240 Unknown
SB-36 (2'-4')02/12/15 NA 6.1 BJ NA Unknown
SB-39 (4'-6')02/12/15 NA 2.7 BJ NA Unknown
SB-43 (4'-6')02/12/15 NE building corner
Walker Street former UST 150 150 B NA Motor Oil
SB-44 (2'-4')02/12/15 Vocational Training floor drain NA 2.3 BJ NA Unknown
SB-45 (4'-6')02/11/15 NA 12 B NA Motor Oil
SB-46 (2'-4')02/11/15 NA 12 B NA Motor Oil
SB-47 (8'-10')02/12/15 <5.4 95 B NA Motor Oil
SB-49 (2'-4')02/12/15 21 87 BJ NA Unknown
SB-52 (8'-10')02/12/15 NA 59,000 B <260 Motor Oil
SB-53 (10'-12')02/12/15 NA 390 B 500 Motor Oil
SB-54 (10'-12')02/12/15 NA 6.5 BJ <220 Unknown
10 10 10
3) B = Analyte detected in method blank
4) J = Analyte detected at a concentration above the method detection limit, but below the laboratory's practical quantitation limit
6) Bolded concentrations were detected above the method detection limit
7) Concentrations highlighted in gray exceed NCDENR's Action Level
Date
Collected
(mm/dd/yy)
ID # (Depth)AOC
5) NA = Not Analyzed
Location
east of Durham Collision one 2,000-gallon waste oil UST
Durham Collision/
Lo Mo/Custom Stone
trench drains (junctions with discharge
pipe)
four northern small hydraulic lifts
six bays with hydraulic lift
two central large hydraulic lifts
two central hydraulic lifts
three double piston lifts
two southern hydraulic lifts
Analysis
central portion of parcel
(former auto repair)two 1,000-gallon fuel oil USTs
NW corner of parcel
(former gas station)two to three gasoline USTs
center of parking lot north
of Cider Works storm drain
wash pit (southern bay)
collection sump
Storage floor drain in paint booth area
Table 1
Summary of Soil Analytical Data for TPH Analysis
Proposed City of Durham Police Headquarters
Durham, Durham County, North Carolina
Terracon Project No. 70157304
DRO
Pattern
Match
113 S. Elizabeth Street
101 S. Elizabeth Street
616 E. Main Street
Notes: 1) mg/kg = milligrams per kilogram
2) AOC = Area of Concern
NCDENR Action Level
Durham Collision
Lo Mo
Custom Stone
Sample I.D. (Depth)Location AOC
Date Collected
(mm/dd/yy)
SB-1 (4'-6')Cider Works OWS 02/10/15 0.060 <0.0050 <0.0058 J <0.0050 <0.0050 <0.0050 <0.0050 <0.0050 <0.0050 <0.0050 <0.0050 <0.0050 <0.0050 <0.0050 <0.0050 <0.0050
SB-2 (6'-8')Cider Works OWS 02/10/15 <0.017 <0.0043 <0.0043 <0.0043 <0.0043 <0.0043 <0.0043 <0.0043 <0.0043 <0.0043 <0.0043 <0.0043 <0.0043 <0.0043 <0.0043 <0.0043
SB-3 (6'-8')Cider Works Sump 02/10/15 0.024 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046
SB-4 (2'-4')Carolina Auto Masters floor drain 02/10/15 0.120 <0.0059 0.014 <0.0059 <0.0059 <0.0059 <0.0059 <0.0059 <0.0059 <0.0059 0.0018 J <0.0059 <0.0059 <0.0059 <0.0059 <0.0059
SB-7 (12'-15')NE building corner near
Carolina Auto Masters
two 6,000-gallon
gasoline USTs 02/10/15 <2.3 <0.570 <0.570 <0.570 <0.570 <0.570 26 5.8 <0.570 <0.570 <0.570 5.0 <0.570 <0.570 50 140
SB-9 (10'-12')center of parking lot north
of Cider Works
one 2,000-gallon waste oil
UST and/or one 1,000-gallon diesel UST 02/10/15 0.038 B <0.0048 <0.570 <0.570 0.0083 <0.570 0.032 0.0054 <0.570 0.0067 <0.570 0.011 <0.570 0.00083 J <0.570 0.190
SB-13 (2'-4')02/10/15 0.014 J <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068
SB-14 (6'-8')02/10/15 <0.052 <0.0054 0.0085 J <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054
SB-15 (10'-12')02/11/15 <0.024 <0.0059 <0.0059 <0.0059 <0.0059 <0.0059 <0.0059 <0.0059 <0.0059 0.0055 J <0.0059 <0.0059 <0.0059 <0.0059 <0.0059 <0.0059
SB-16 (8'-10')02/11/15 0.025 B <0.0056 <0.0056 <0.0056 0.0032 J 0.0023 J <0.0056 0.0029 J <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 0.0091 <0.0056 <0.0056
SB-20 (2'-4')02/11/15 0.051 <0.0054 0.0095 J 0.0028 J <0.0054 <0.0054 <0.0054 <0.0054 0.0042 J 0.0014 J <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054
SB-23 (2'-4')02/11/15 0.120 B 0.0032 J <0.0053 <0.0053 0.011 0.0031 J <0.0053 0.011 <0.0053 0.00085 J <0.0053 0.110 <0.0053 <0.0053 <0.0053 0.0036 J
SB-25 (0-2')02/11/15 0.0083 J <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055
SB-26 (6'-8')02/11/15 0.0075 J <0.0052 <0.0052 <0.0052 <0.0052 <0.0052 <0.0052 0.0052 <0.0052 <0.0052 <0.0052 0.023 <0.0052 <0.0052 <0.0052 <0.0052
SB-27 (8'-10')02/11/15 <0.019 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047
SB-32 (8'-10')02/11/15 <0.018 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 <0.0046 0.0010 J <0.0046 <0.0046
SB-33 (8'-10')02/11/15 0.013 BJ <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 0.0028 J <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049
SB-34 (0-2')02/12/15 0.042 BJ <0.0048 <0.0048 <0.0048 <0.0048 <0.0048 0.0027 J 0.021 <0.0048 <0.0048 <0.0048 0.0015 J <0.0048 <0.0048 <0.0048 0.0081
SB-35 (2'-4')02/12/15 <0.020 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049 <0.0049
SB-40 (4'-6')north bay door 02/12/15 0.0058 BJ <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054 <0.0054
SB-41 (6'-8')west bay door 02/12/15 0.078 BJ <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056
SB-44 (2'-4') Vocational Training floor drain 02/12/15 <0.022 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055
SB-45 (4'-6')02/11/15 0.010 J <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 0.0042 J <0.0056
SB-46 (2'-4')02/11/15 0.011 J <0.0056 <0.0056 <0.0056 0.0033 J <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 <0.0056 0.00067 J <0.0056 <0.0056 <0.0056 0.0072
8.2 0.0056 16 0.44 0.23 0.10 4.9 1.7 NS 0.091 0.4 NS 0.16 0.0074 4.3 4.6
940 18 9,385 312 1,400 110 1,560 1,564 NS 350 1,200 NS 313 1 1,200 3,129
24,000 164 245,280 8,176 36,000 1,000 40,000 40,880 NS 3,100 32,000 NS 8,176 10 3,200 81,760
Notes: 1) mg/kg = milligrams per kilogram .
2) AOC = Area of Concern
3) B = Analyte detected in method blank
4) J = Analyte detected at a concentration above the method detection limit, but below the laboratory's practical quantitation limit
6) Bolded concentrations were detected above the method detection limit
7) MSCC = Maximum Soil Contaminant Concentration
7) Concentrations highlighted in gray exceed NCDENR's soil-to-groundwater MSCC
Is
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p
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o
p
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e
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Me
t
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y
l

t
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-
B
u
t
y
l

E
t
h
y
l

(
M
T
B
E
)
Na
p
h
t
h
a
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e
Be
n
z
e
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e
2-
B
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a
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e

(
M
E
K
)
1,
2
-
D
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a
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t
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1,
4
-
D
i
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l
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o
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Ac
e
t
o
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4-
M
e
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-
2
-
p
e
n
t
a
n
o
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(
M
I
B
K
)
113 S. Elizabeth Street
Soil-to-Groundwater MSCC
Residential MSCC
Industrical/Commercial MSCC
Xy
l
e
n
e
s

(
T
o
t
a
l
)
Te
t
r
a
c
h
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o
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n
e
To
l
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Eth
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Table 2
Summary of Soil Analytical Data VOC Analysis
Proposed City of Durham Police Headquarters
Durham, Durham County, North Carolina
Terracon Project No.: 70157304
center of parking lot northof Cider Works storm drain
Analytical Method →VOCs by EPA Method 8260B
Contaminant of Concern (mg/kg)→
one 2,000-gallon
waste oil UST
Durham Collision possible fill ports in floor
trench drains (juctions with
discharge pipe)
Durham Collision/
Lo Mo/Custom Stone
Lo Mo
east of Durham Collision
Custom Stone
collection sump
wash pit (southern bay)
Super Graphics
Storage floor drain in paint
booth area
601 E. Ramseur Street
101 S. Elizabeth Street
APPENDIX C
Soil Boring Logs
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1020Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11 - Boring terminated at ~10.0 bls
12 - Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
ML
CL/CH
Grab VOCs DRO Oil and Grease
De
p
t
h

(
f
t
)
4-6
Soil Boring Log
Boring ID: SB-1
City of Durham
Depth (ft)Grab/Composite Analysis
Project Number: 70157304
Start Date/Time: 2/10/15 - 0955
Finish Date/Time: 2/10/15 -1020
Depth of Boring: 10 feet bls
Water Level: -
Well Installed: No
Site Location: Durham, NC
Weather: rainy; 30s
Driller: Regional Probing
493
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o
v
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r
y

(
i
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s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
923
1132
504
0'-2': Mix of concrete and brown clay; moist
2-'-6': Brown clay; moist
6'-8': Reddish brown Triassic silt; moist
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1100Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9 - Boring terminated at ~8.0 bls
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Groundwater not encountered in the boring
1355
4801
ML
ML
CH/CL
1484
48.72
ppm 6'-8': Reddish brown triassic silt; dry
4'-6': Dark brown and orange clay mottled with gray clay; moist
0'-4': Reddish brown Triassic silt; moist
De
p
t
h

(
f
t
)
Re
c
o
v
e
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y

(
i
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c
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e
s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis6-8 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 8 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-2
City of Durham Start Date/Time: 2/10/15 - 1025
Project Number: 70157304 Finish Date/Time: 2/10/15 -1055
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1142Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9 - Boring terminated at ~8.0 bls
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Groundwater not encountered in the boring
1840.0
2202
CL/CH
SC
1800 0'-2': Compressed core with concrete, brown clay and some sand
84.07
ppm 6'-8': Lighter in color, tan loamy, mix of clay and sand
2'-6': Brown clay with some sand
De
p
t
h

(
f
t
)
Re
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o
v
e
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y

(
i
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c
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s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis6-8 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 8 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-3
City of Durham Start Date/Time: 2/10/15 - 1135
Project Number: 70157304 Finish Date/Time: 2/10/15 -1155
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1110Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicable
bls = below land surface
0'-2': Brown clay with some sand; fine to medium-grained; moist
2'-6': Reddish brown Triassic silt; moist
6'-8': Reddish brown Triassic silt mottled with tan clay and sand; fine to medium-
grained; moist
CH/CL
- Boring terminated at ~8.0 bls
- Groundwater not encountered in the boring
ML
2673
2160
1604
2502
De
p
t
h

(
f
t
)
Re
c
o
v
e
r
y

(
i
n
c
h
e
s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Sc
r
e
e
n
i
n
g
:
Depth (ft)Grab/Composite Analysis2-4 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 8 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-4
City of Durham Start Date/Time: 2/10/15 - 1100
Project Number: 70157304 Finish Date/Time: 2/10/15 -1125
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample MethodHand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicable
bls = below land surface
ML
507
734
SC
CH/CL
- Boring met refusal at ~17.5 bls
- Groundwater not encountered in the boring
15'-17.5': Reddish brown Triassic silt; moist
1071
1157
1124
363.9
ppm
2568
0'-10': Clayey sand; red, brown, orange (fill); moist
10'-15': Sandy clay; reddish brown, moist; stong petroleum odor
2211
De
p
t
h

(
f
t
)
Re
c
o
v
e
r
y

(
i
n
c
h
e
s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Sc
r
e
e
n
i
n
g
:
Depth (ft)Grab/Composite Analysis
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 17.5 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-5
City of Durham Start Date/Time: 2/10/15 - 1450
Project Number: 70157304 Finish Date/Time: 2/10/15 -1515
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample MethodHand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18 - Boring met refusal at ~17.0 bls
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Groundwater not encountered in the boring
228.5
ppm
1305
2178
GM
CH/CL
0'-12': Gravel backfill
12'-15': Sandy clay; reddish brown; fine to medium-grained; moist; strong petroleum
odor
15'-17': Reddish brown Triassic silt; moistML
De
p
t
h

(
f
t
)
Re
c
o
v
e
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y

(
i
n
c
h
e
s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 17 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-6
City of Durham Start Date/Time: 2/10/15 - 1515
Project Number: 70157304 Finish Date/Time: 2/10/15 -1535
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1555Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
- Boring met refusal at ~17.25 bls
19
- Groundwater not encountered in the boring
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
0'-8': Orange and brown to moist gray clay; moist
15'-17.25': Reddish brown Triassic silt; dry
8'-12': Orangish tan sandy clay;fine to medium-grained; moist (fill); very strong
petroleum odor at 12 to 15 ft bls
ML
CL/CH
1641
1818
1568
1130
958.9
ppm
3121
2364
1891
De
p
t
h

(
f
t
)
Re
c
o
v
e
r
y

(
i
n
c
h
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s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis12-15 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 17.25 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-7
City of Durham Start Date/Time: 2/10/15 - 1540
Project Number: 70157304 Finish Date/Time: 2/10/15 -1555
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample MethodHand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~15.0 bls per scope
- Groundwater not encountered in the boring
1211 GM
CH/CL
0'-8': Gravel backfill
8'-15': Reddish brown sandy clay; fine to medium-grained; moist; slight petroleum
odor
4196
3117
2101
De
p
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h

(
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)
Re
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o
v
e
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y

(
i
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c
h
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s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 15 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-8
City of Durham Start Date/Time: 2/10/15 - 1600
Project Number: 70157304 Finish Date/Time: 2/10/15 -1620
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1205Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~12.0 bls per scope
- Groundwater not encountered in the boring
2425.0
36.24
ppm
2'-4': Gray and black clay with sand; fine to medium-grained; moist
ML
149.1
ppm
4'-12': Reddish brown Triassic silt; moist; petroleum odor at 6 to 8 ft bls
43.6
ppm
20.01
ppm
2112
CH/CL
0'-2': Orange and brown clay with sand; fine to medium-grained; moist
De
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h

(
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)
Re
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o
v
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(
i
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis10-12 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-9
City of Durham Start Date/Time: 2/10/15 - 1200
Project Number: 70157304 Finish Date/Time: 2/10/15 -1210
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample MethodHand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13 - Boring terminated at ~12.0 bls
14 - Groundwater not encountered in the boring
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
501
631
ML
311
906
0'-12': Reddish brown Triassic silt; moist
De
p
t
h

(
f
t
)
Re
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o
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y

(
i
n
c
h
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s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
1162
1652
Depth (ft)Grab/Composite Analysis
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-10
City of Durham Start Date/Time: 2/10/15 - 1215
Project Number: 70157304 Finish Date/Time: 2/10/15 -1235
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample MethodHand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~12.0 bls
- Groundwater not encountered in the boring
ML
7351
4'-12': Reddish brown Triassic silt; moist
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
2019
0'-4': Orange and gray clay; moist
1440
CH/CL
3419
4603
De
p
t
h

(
f
t
)
Re
c
o
v
e
r
y

(
i
n
c
h
e
s
)
1450
Depth (ft)Grab/Composite Analysis
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-11
City of Durham Start Date/Time: 2/10/15 - 1240
Project Number: 70157304 Finish Date/Time: 2/10/15 -1300
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample MethodHand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
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g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~14.5 ft bls
- Groundwater not encountered in the boring
17.43
ppm
12.12
ppm
ML
CH/CL
55.25
ppm
6111
2415 0'-3': Orange and brown clay to gray clay; moist
3'-14.5': Reddish brown Triassic silt, moist; petroleum odor at 5 to 12 ft bls
13.45
ppm
24.39
ppm
De
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis
Site Location: Durham, NC
Weather: Cloudy / 40's Depth of Boring: 14.5 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-12
City of Durham Start Date/Time: 2/10/15 - 1315
Project Number: 70157304 Finish Date/Time: 2/10/15 -1337
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1412Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9 - Boring terminated at ~8.0 bls
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Groundwater not encountered in the boring
2003
1340 ML
0'-5': Orange and brown clay; moist
5'-8': Reddish brown Triassic silt; moist
1895 CH/CL
1399
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis2-4 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 8 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-13
City of Durham Start Date/Time: 2/10/15 - 1345
Project Number: 70157304 Finish Date/Time: 2/10/15 -1405
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 67125DT Rock Core
Time Sample Method1430Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
CH/CL
ML
1121
2180
- Boring terminated at ~8.0 bls
- Groundwater not encountered in the boring
De
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
3268
0'-5': Orange and brown to gray clay
5'-8': Reddish brown Triassic silt; moist
2745
Depth (ft)Grab/Composite Analysis6-8 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: Cloudy, 40's Depth of Boring: 8 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-14
City of Durham Start Date/Time: 2/10/15 - 1410
Project Number: 70157304 Finish Date/Time: 2/10/15 -1430
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1330Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Groundwater not encountered in the boring
1307
1831
871
2'-9': Gray clay with some sand; fine to medium-grained; moist
9'-14': Reddish brown Triassic silt; moist
7440
- Boring met refusal at ~14.0 bls
909 0'-2': Brown and yellow sandy clay; fine to meidum-grained; moist
ML
CH/CL
1875
6070
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis10-12 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun & clouds /Depth of Boring: 14 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-15
City of Durham Start Date/Time: 2/11/15 - 1320
Project Number: 70157304 Finish Date/Time: 2/11/15 -1325
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1345Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
1083
2465
0'-6': Orange and gray clay with some sand; fine to medium-grained; moist
1147
8'-10': Red brown triassic
3829
- Boring terminated at ~12.0 bls
- Groundwater not encountered in the boring
ML
CH/CL
7878 6'-8': Gray clay; mosit
11.75
ppm
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(
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis8-10 VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun & clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-16
City of Durham Start Date/Time: 2/11/15 - 1330
Project Number: 70157304 Finish Date/Time: 2/11/15 -1345
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample MethodHand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13 - Boring terminated at ~12.0 bls
14 - Groundwater not encountered in the boring
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
1507
1328
1294
1230
0'-7': Orange and gray clay with sand, moist
7'-12': Red brown triassic
1372
1062
ML
CH/CL
De
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(
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-17
City of Durham Start Date/Time: 2/11/15 - 1345
Project Number: 70157304 Finish Date/Time: 2/11/15 -1400
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample MethodHand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~14.0 bls
- Groundwater not encountered in the boring
0'-12': Gravel backfill
3153
GM
ML 12'-14': Reddish brown Triassic silt; dry
De
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 14 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-18
City of Durham Start Date/Time: 2/11/15 - 1400
Project Number: 70157304 Finish Date/Time: 2/11/15 -1415
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method950Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~10.0 bls
655
2158
ML
728
SC 0'-6': Orangish brown sand with clay; (possible fill); wet; strong petroluem odor,
possible product at 4 to 6 feet bls
CH/CL10286'-8': Orange gray clay with sand; fine to medium-grained; moist
841 8'-10': Reddish brown Triassic silt; moist
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis4-6 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-19
City of Durham Start Date/Time: 2/11/15 - 0940
Project Number: 70157304 Finish Date/Time: 2/11/15 -0950
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1011Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~10.0 bls
14.02
ppm
6564
0'-4': Red and gray clay with sand, fine to medium-grained; moist
4'-8': Gray clay; moist to wet by 6 feet bls
CH/CL
ML
1452
2309
1350 8'-10': Reddish brown Triassic silt; moist
De
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(
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis2-4 VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-20
City of Durham Start Date/Time: 2/11/15 - 1000
Project Number: 70157304 Finish Date/Time: 2/11/15 -1015
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1049Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11 - Boring terminated at ~10.0 bls
12 - Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
989
1677
0-7': Orange and gray clay, moist
7'-10': Reddish brown Trassic silt; moist
2026
776
1915
ML
CH/CL
De
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(
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis6-8 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-21
City of Durham Start Date/Time: 2/11/15 - 1030
Project Number: 70157304 Finish Date/Time: 2/11/15 -1050
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1055Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11 - Boring terminated at ~10.0 bls
12 - Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
3639
2012
SM
SC
0'-6': Red brown sand; moist
6'-10': Gray sand with clay; wet
2553
1336
1804
De
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(
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis2-4 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-22
City of Durham Start Date/Time: 2/11/15 - 1050
Project Number: 70157304 Finish Date/Time: 2/11/15 -1100
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1124Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12 - Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring met refusal at ~14.0 bls
405.8
ppm
84.34
ppm SC
0'-4': Red brown clay, moist
4'-6': Gray clay, moist
6'-14': Red brown clay with sand
2855
10.05
ppm
2854
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(
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis2-4 Grab VOCs DRO
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 14 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-23
City of Durham Start Date/Time: 2/11/15 - 1100
Project Number: 70157304 Finish Date/Time: 2/11/15 -1125
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1145Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11 - Boring terminated at ~10.0 bls
12 - Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
1480
1448
2606 6'-8': Gray and red clay; moist
1820 8'-10': Red brown Triassic silt; moist
0'-5': Red clay; moist
2235
5'-6': Gray clay with sand; fine to medium-grained; moist
CH/CL
ML
De
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(
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis6-8 DRO
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-24
City of Durham Start Date/Time: 2/11/15 - 1130
Project Number: 70157304 Finish Date/Time: 2/11/15 -1145
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1200Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14 - Groundwater not encountered in the boring
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~12.0 bls
CH/CL
ML
0'-7': Red clay; moist
7'-8': Gray clay; moist
8'-12': Reddish brown Triassic silt; moist
1372
1063
1124
1113
824
50%
De
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(
i
n
c
h
e
s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis0-2 Grab VOCs DRO
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-25
City of Durham Start Date/Time: 2/11/15 - 1145
Project Number: 70157304 Finish Date/Time: 2/11/15 -1200
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1611Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11 - Boring terminated at ~10.0 bls per scope
12 - Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
7'-10': Reddish brown Triassic silt; moist
1427
4018
ML
1588 0'-2': Orange clay; moist
2'-7': Tan clay; moist
CH/CL
77.42
ppm
15.78
ppm
De
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(
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis6-8 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-26
City of Durham Start Date/Time: 2/11/15 - 1600
Project Number: 70157304 Finish Date/Time: 2/11/15 -1615
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1637Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~10.0 bls
966
709
0'-7': Tan clay with sand; fine to mediium-grained; moist
7'-10': Reddish brown Triassic silt; moist
1247
ML
CH/CL
986
1951
De
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(
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis8-10 VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-27
City of Durham Start Date/Time: 2/11/15 - 1625
Project Number: 70157304 Finish Date/Time: 2/11/15 -1635
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1615Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
0'-2': Tan clay with sand; fine to medium-grianed; moist
CH/CL
ML
2'-7': Tan clay with less sand; fine to medium-grained; moist
7'-10': Reddish brown Triassic silt; moist
- Boring terminated at ~10.0 bls per scope
3721
3032
2223
1903
1603
De
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(
i
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h
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis6-8 Grab DRO
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-28
City of Durham Start Date/Time: 2/11/15 - 1600
Project Number: 70157304 Finish Date/Time: 2/11/15 -1625
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1652Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~10.0 bls
1819
1839
0'-3': Tan clay with some sand; fine to medium-grained; moist
3'-10': Reddish brown Triassic silt; moist
111 CL/CH
ML
2338
1911
De
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(
i
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h
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis6-8 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-29
City of Durham Start Date/Time: 2/11/15 - 1645
Project Number: 70157304 Finish Date/Time: 2/11/15 -1655
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1600Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
- Groundwater not encountered in the boring
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring met refusal at ~14.0 bls
137
951
2781
ML 0'-14':Red sandy silt; fine to medium-grained; moist
50%
50%
5-10 Grab DRO
De
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(
i
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
50%
Soil Boring Log
Boring ID: SB-30
City of Durham Start Date/Time: 2/11/15 - 1545
Project Number: 70157304 Finish Date/Time: 2/11/15 -1600
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 14 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Depth (ft)Grab/Composite Analysis
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1629Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~10.0 bls per scope
0'-5' - Red orange clay; moist
2144
2220
CL/CH
ML
5'-9' -: Brown clay; moist
9'-10' - Reddish brown Triassic silt; moist
70%
70%
De
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(
i
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis0-5 VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouids / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-31
City of Durham Start Date/Time: 2/11/15 - 1615
Project Number: 70157304 Finish Date/Time: 2/11/15 -1625
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1515Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15 - Groundwater not encountered in the boring
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
8'-13': Reddish brown Triassic silt; moist
- Boring met refusal at ~13.0 bls
1323
2277
1164
CL/CH
ML
4'-8': Gray and tan clay; moist
1842
0'-4': Tan clay; moist
1102
5813
De
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f
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(
i
n
c
h
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis8-10 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 13 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-32
City of Durham Start Date/Time: 2/11/15 - 1500
Project Number: 70157304 Finish Date/Time: 2/11/15 -1515
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1538Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15 - Groundwater not encountered in the boring
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
6'-13': Gray and tan clay, saturated
- Boring met refusal at ~13.0 bls
1690
1764
1941
CL/CH
0'-5': Gray clay with some gravel backfill; wet
5'-6': Tan clay; moist
1747
2314
2805
De
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(
i
n
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h
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis8-10 VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 13 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-33
City of Durham Start Date/Time: 2/11/15 - 1525
Project Number: 70157304 Finish Date/Time: 2/11/15 -1540
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1118Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~10.0 bls
451
10.01
ppm ML 0'-10': Reddish brown Triassic silt; moist
452.7
ppm
2030
2944
De
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(
i
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c
h
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis0-2 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-34
City of Durham Start Date/Time: 2/12/15 - 1055
Project Number: 70157304 Finish Date/Time: 2/12/15 -1101
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1135Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring met refusal at ~9.5 bls
SM
0'-5': Reddish brown Triassic silt; moist
6'-9.5': Tan sand, fine to medium-grianed; dry
958
1036
ML
1106
1062
De
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(
i
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis2-4 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 9.5 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-35
City of Durham Start Date/Time: 2/12/15 - 1115
Project Number: 70157304 Finish Date/Time: 2/12/15 -1124
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1018Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
- Groundwater not encountered in the boring
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring met refusal at ~4.0 bls in partially weathered sandstone
1818
0'-4': Red brown Triassic sitl; dry
1720
ML
De
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(
i
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis2-4 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 4 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-36
City of Durham Start Date/Time: 2/12/15 - 0952
Project Number: 70157304 Finish Date/Time: 2/12/15 -0957
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1022Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
- Groundwater not encountered in the boring
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~6.0 bls in partially weathered sandstone
660
787
0'-4': Reddish brown Triassic silt; dry
4'-6': Tan sand; fine to medium-grained; dry
1110
ML
SM
De
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(
i
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis0-2 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 6 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-37
City of Durham Start Date/Time: 2/12/15 - 1005
Project Number: 70157304 Finish Date/Time: 2/12/15 -1015
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1046Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11 - Groundwater not encountered in the boring
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
0'-7': Reddish brown Triassic silt; dry
7'-9': Tan sand; fine to medium-grained; dry
- Boring met refusal at ~9.0 bls
896
963
978
ML
SM
814
De
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(
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(
i
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis6-8 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 9 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-38
City of Durham Start Date/Time: 2/12/15 - 1023
Project Number: 70157304 Finish Date/Time: 2/12/15 -1040
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1057Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11 - Groundwater not encountered in the boring
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
1124
1437
- Boring terminated at ~9.0 bls
7'-9': Dark gray sand with some gravel; fine to medium-grained; wet
0'-7': Reddish brown Triassic silt; dry
770
ML
SM1443
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(
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis4-6 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 9 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-39
City of Durham Start Date/Time: 2/12/15 - 1038
Project Number: 70157304 Finish Date/Time: 2/12/15 -1049
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Georpobe 6712DT Rock Core
Time Sample Method932Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~10.0 bls
1015
1199 CL/CH
0'-3': Tan and brown sandy clay; fine to medium-grained; moist
3'-10': Tan clay with sand; fine to medium-grained; moist
652
1002
905
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(
i
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis4-6 Grab VOCs
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-40
City of Durham Start Date/Time: 2/12/15 - 0855
Project Number: 70157304 Finish Date/Time: 2/12/15 -0910
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method941Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
1710
5'-10': Reddish brown Triassic silt; moistML
- Boring terminated at ~10.0 bls
CL/CH
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
1940
0'-5': Tan clay with some sand; fine to medium-grained; moist
1722
1780
1744
Depth (ft)Grab/Composite Analysis6-8 Grab VOCs
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-41
City of Durham Start Date/Time: 2/12/15 - 0915
Project Number: 70157304 Finish Date/Time: 2/12/15 -0926
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample MethodHand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
- Groundwater not encountered in the boring
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
6095
- Boring terminated at ~12.0 bls
16.23
ppm
15.60
ppm
CL/CH0'-12': Orange gray clay with sand; fine to medium-grained; moist
16.41
ppm
6749
5083
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(
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-42
City of Durham Start Date/Time: 2/12/15 - 1534
Project Number: 70157304 Finish Date/Time: 2/12/15 -1543
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1606Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
- Groundwater not encountered in the boring
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
19.40
ppm
- Boring terminated at ~12.0 bls
17.41
ppm
72.99
ppm
0'-12': Gray clay; wetCL/CH
8116
16.85
ppm
21.74
ppm
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(
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis4-6 Grab GRO DRO
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-43
City of Durham Start Date/Time: 2/12/15 - 1547
Project Number: 70157304 Finish Date/Time: 2/12/15 -1605
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Rock Core
Time Sample Method1310Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~10.0 bls
3431
1507 CL/CH
0'-8': Tan clay with sand; fine to medium-grained; moist
2151
2646
3179 8'-10': Tan clay; moist
De
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h

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(
i
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Drill Rig: 6712DT
Depth (ft)Grab/Composite Analysis2-4 Grab VOCs DRO
Site Location: Durham, NC
Weather: rainy; 30s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-44
City of Durham Start Date/Time: 2/12/15 - 1250
Project Number: 70157304 Finish Date/Time: 2/12/15 -1303
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method902Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~10.0 bls
694
1061 CL/CH
566
0'-10': Reddish brown clay with sand, fine to medium-grained; moist
269
1053
De
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f
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(
i
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h
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis4-6 Grab VOCs DRO
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-45
City of Durham Start Date/Time: 2/11/15 - 0840
Project Number: 70157304 Finish Date/Time: 2/11/15 -0850
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method905Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
- Groundwater not encountered in the boring
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~10.0 bls
1797
1476 CL/CH
0'-5': Gray clay with sand; fine to medium-grianed; moist
5'-10': Reddish brown clay with sand; fine to medium-grained; moist
623
1394
1708
De
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f
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(
i
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c
h
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis2-4 Grab VOCs DRO
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 10 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-46
City of Durham Start Date/Time: 2/11/15 - 0855
Project Number: 70157304 Finish Date/Time: 2/11/15 -0905
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1508Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14 - Groundwater not encountered in the boring
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
2812
- Boring terminated at ~12.0 bls
2524
2776
CL/CH
0'-5': Tan and orange clay with some sand; fine to medium-grained; moist
5'-9': Red clay; moist
9'-12': Tan sandy ; fine to medium-grained; moist
2771
2026
2711
De
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f
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(
i
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h
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis8-10 Grab GRO DRO
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-47
City of Durham Start Date/Time: 2/12/15 - 1434
Project Number: 70157304 Finish Date/Time: 2/12/15 -1445
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample MethodHand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
- Groundwater not encountered in the boring
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
2122
- Boring terminated at ~12.0
2011
2096
0'-5': Gray clay, moist; petroleum odor at 5'
2356
CL/CH
ML 7'-12': Reddish brown Triassic silt; moist
5'-7': Gray sandy clay; fine to medium-grained; moist
2734
2138
De
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(
i
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h
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Grab/Composite AnalysisDepth (ft)
Soil Boring Log
Boring ID: SB-48
City of Durham Start Date/Time: 2/12/15 - 1451
Project Number: 70157304 Finish Date/Time: 2/12/15 -1502
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Georprobe 6712DT Rock Core
Time Sample Method1543Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
- Groundwater not encountered in the boring
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
2094
- Boring terminated at ~12.0 bls
11.12
pmm
7423 CL/CH
ML
2'-4': Red clay with sand; fine to medium-grained; moist
2142 0'-2': Tan clay; moist
4'-10': Gray clay; wet
10'-12': Reddish brown Triassic silt; moist
2320
1967
De
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(
i
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SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis2-4 Grab GRO DRO
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-49
City of Durham Start Date/Time: 2/12/15 - 1510
Project Number: 70157304 Finish Date/Time: 2/12/15 -1527
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1336Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
- Groundwater not encountered in the boring
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
- Boring terminated at ~12.0 bls
0'-2': Orange tan clay with sand, fine to medium-grained; dry
2'-6': tan sandy clay; fine to medium-grained; dry
ML
CL/CH
1361
6'-12': Reddish brown Triassic silt' dry
2322
2494
3185
2304
2811
De
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(
i
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c
h
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis10-12 Grab VOCs DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: --
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-50
City of Durham Start Date/Time: 2/12/15 - 1316
Project Number: 70157304 Finish Date/Time: 2/12/15 -1325
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample MethodHand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
- Groundwater not encountered in the boring
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
1991
2423
2098
CL/CH
6'-12': tan sandy clay; fine to medium-grained; dry
- Boring terminated at ~12.0 bls
1723
1515
0'-4': Orange tan clay with sand; fine to medium-grained; dry
4'-6' - tan sandy clay; fine to medium-grained; dry
1572
De
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f
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(
i
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h
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-51
City of Durham Start Date/Time: 2/12/15 - 1330
Project Number: 70157304 Finish Date/Time: 2/12/15 -1341
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1404Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14 - Groundwater not encountered in the boring15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
0-2' - tan clay; moist
1439
CL/CH
ML
- Boring terminated at ~12.0 bls
6'-12' - reddish brown Triassic silt; moist
3160
2076
3853
1796
1911
De
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h

(
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(
i
n
c
h
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)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis8-10 Grab DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-52
City of Durham Start Date/Time: 2/12/15 - 1347
Project Number: 70157304 Finish Date/Time: 2/12/15 -1359
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Rock Core
Time Sample Method1419Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14 - Groundwater not encountered in the boring15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
3307
2951
- Boring terminated at ~12.0 bls
4'-12' - reddish brown Triassic silt; moist
2136
CL/CH0-4' - tan clay; moist
ML
1678
2800
3591
De
p
t
h

(
f
t
)
Re
c
o
v
e
r
y

(
i
n
c
h
e
s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis10-12 Grab DRO Oil and Grease
Drill Rig: Geoprobe 6712DT
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-53
City of Durham Start Date/Time: 2/12/15 - 1402
Project Number: 70157304 Finish Date/Time: 2/12/15 -1413
Client:Drilling Method
Hand Auger
Boring Diameter: 3 inch X DPT
HSA
Logged By: JLF Mud Rotary
Air Rotary
Drill Rig: Geoprobe 6712DT Rock Core
Time Sample Method1447Hand Auger
X Macro-Core
Split SpoonShelby Tube
Blo
w
s

p
e
r

6
"
PID

(
p
p
b
)
Sc
r
e
e
n
i
n
g
:
U.S
.
C
.
S
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15 - Groundwater not encountered in the boring
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Notes:NA= Not applicablebls = below land surface
2949
2769
- Boring terminated at ~12.0 bls
3288
ML 4'-12' - reddish brown Triassic silt; dry
2403
CL/CH
3357
2711
0-4' - tan clay; moist
De
p
t
h

(
f
t
)
Re
c
o
v
e
r
y

(
i
n
c
h
e
s
)
SOIL DESCRIPTION: Color, moisture, grain size/range, MAIN COMPONENT, minor
component(s), structure, angularity, odor, and Geologic Unit
Depth (ft)Grab/Composite Analysis10-12 Grab DRO Oil and Grease
Site Location: Durham, NC
Weather: sun and clouds / 40s Depth of Boring: 12 feet bls
Water Level: -
Driller: Regional Probing Well Installed: No
Soil Boring Log
Boring ID: SB-54
City of Durham Start Date/Time: 2/12/15 - 1420
Project Number: 70157304 Finish Date/Time: 2/12/15 -1430
APPENDIX D
Laboratory Analytical Reports and Chain of Custody Records
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Terracon Consultants, Inc.
2401 Brentwood Road
Suite 107 I
Raleigh, NC 27604
Attention: Justin.Fabriziani
QB12017Lot Number:
70157304Project Number:
Proposed Durham PDHQProject Name:
02/19/2015Date Completed:
Nisreen Saikaly
Project Manager
*QB12017*

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Terracon Consultants, Inc.
Lot Number: QB12017
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
DRO
All DRO sample patterns resemble an oil pattern except samples -004 (SB-4 (2'-4')) and -008 (SB-7 (12'-15')). Sample -004 resembles fuel oil
pattern. Sample -008 resembles gasoline pattern.
The DRO pattern in the MB does not resemble the pattern in any of the sample samples except for samples -006 (SB-13 (2'-4')) and -007 SB-14 (6'-
8').
Page: 2 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terracon Consultants, Inc.
Lot Number: QB12017

Sample Number Sample ID Matrix Date Sampled Date Received
001 02/10/2015 1020SB-1 (4'-6')Solid 02/12/2015
002 02/10/2015 1100SB-2 (6'-8')Solid 02/12/2015
003 02/10/2015 1142SB-3 (6'-8')Solid 02/12/2015
004 02/10/2015 1110SB-4 (2'-4')Solid 02/12/2015
005 02/10/2015 1205SB-9 (10'-12')Solid 02/12/2015
006 02/10/2015 1412SB-13 (2'-4')Solid 02/12/2015
007 02/10/2015 1430SB-14 (6'-8')Solid 02/12/2015
008 02/10/2015 1555SB-7 (12'-15')Solid 02/12/2015
009 02/10/2015Trip Blank Aqueous 02/12/2015
(9 samples)
Page: 3 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Terracon Consultants, Inc.
Lot Number: QB12017

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SB-1 (4'-6')Solid Acetone 8260B 60 ug/kg 6
001 SB-1 (4'-6')Solid 2-Butanone (MEK)8260B 5.8 J ug/kg 6
001 SB-1 (4'-6')Solid TPH-DRO 8015C 24000 B ug/kg 8
002 SB-2 (6'-8')Solid TPH-DRO 8015C 24000 B ug/kg 12
003 SB-3 (6'-8')Solid Acetone 8260B 24 ug/kg 14
003 SB-3 (6'-8')Solid TPH-DRO 8015C 24000 B ug/kg 16
004 SB-4 (2'-4')Solid Acetone 8260B 120 ug/kg 18
004 SB-4 (2'-4')Solid 2-Butanone (MEK)8260B 14 ug/kg 18
004 SB-4 (2'-4')Solid 4-Methyl-2-pentanone 8260B 1.8 J ug/kg 18
004 SB-4 (2'-4')Solid TPH-DRO 8015C 24000 B ug/kg 20
005 SB-9 (10'-12')Solid HEM (oil and grease)9071B 380 mg/kg 21
005 SB-9 (10'-12')Solid Acetone 8260B 38 B ug/kg 22
005 SB-9 (10'-12')Solid 1,2-Dichlorobenzene 8260B 8.3 ug/kg 22
005 SB-9 (10'-12')Solid Ethylbenzene 8260B 32 ug/kg 22
005 SB-9 (10'-12')Solid Isopropylbenzene 8260B 5.4 ug/kg 22
005 SB-9 (10'-12')Solid Methyl tertiary butyl ether (MTBE)8260B 6.7 ug/kg 22
005 SB-9 (10'-12')Solid Methylcyclohexane 8260B 11 ug/kg 22
005 SB-9 (10'-12')Solid Tetrachloroethene 8260B 0.83 J ug/kg 22
005 SB-9 (10'-12')Solid Xylenes (total)8260B 190 ug/kg 23
005 SB-9 (10'-12')Solid TPH-DRO 8015C 5300000 B ug/kg 24
006 SB-13 (2'-4')Solid Acetone 8260B 14 J ug/kg 26
006 SB-13 (2'-4')Solid TPH-DRO 8015C 39000 BJ ug/kg 28
007 SB-14 (6'-8')Solid Acetone 8260B 52 ug/kg 30
007 SB-14 (6'-8')Solid 2-Butanone (MEK)8260B 8.5 J ug/kg 30
007 SB-14 (6'-8')Solid TPH-DRO 8015C 3300 BJ ug/kg 32
008 SB-7 (12'-15')Solid Ethylbenzene 8260B 26000 ug/kg 34
008 SB-7 (12'-15')Solid Isopropylbenzene 8260B 5800 ug/kg 34
008 SB-7 (12'-15')Solid Methylcyclohexane 8260B 5000 ug/kg 34
008 SB-7 (12'-15')Solid Toluene 8260B 50000 ug/kg 34
008 SB-7 (12'-15')Solid Xylenes (total)8260B 140000 ug/kg 35
008 SB-7 (12'-15')Solid TPH-DRO 8015C 290000 B ug/kg 36
(31 detections)
Page: 4 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-1 (4'-6')
QB12017-001
02/10/2015 1020
02/12/2015
Solid
% Solids:83.5 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg200240
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-1 (4'-6')
QB12017-001
02/10/2015 1020
02/12/2015
Solid
% Solids:83.5 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1341 DCS 67778 6.04
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 60 1ug/kg6.620
Benzene 71-43-2 8260B ND 1ug/kg1.15.0
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.75.0
Bromoform 75-25-2 8260B ND 1ug/kg0.695.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg1.85.0
2-Butanone (MEK)78-93-3 8260B 5.8 J 1ug/kg2.49.9
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.35.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.85.0
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.75.0
Chloroethane 75-00-3 8260B ND 1ug/kg1.35.0
Chloroform 67-66-3 8260B ND 1ug/kg0.825.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg0.995.0
Cyclohexane 110-82-7 8260B ND 1ug/kg0.675.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.55.0
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.75.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.845.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.75.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.75.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.75.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.65.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.725.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg0.995.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.75.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.755.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.55.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg0.905.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.675.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.815.0
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.75.0
2-Hexanone 591-78-6 8260B ND 1ug/kg1.39.9
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.235.0
Methyl acetate 79-20-9 8260B ND 1ug/kg0.975.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.405.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.59.9
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.415.0
Methylene chloride 75-09-2 8260B ND 1ug/kg2.65.0
Styrene 100-42-5 8260B ND 1ug/kg1.15.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.475.0
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.505.0
Toluene 108-88-3 8260B ND 1ug/kg1.75.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.625.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.75.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.845.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.785.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-1 (4'-6')
QB12017-001
02/10/2015 1020
02/12/2015
Solid
% Solids:83.5 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1341 DCS 67778 6.04
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg1.95.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.55.0
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.855.0
Xylenes (total)1330-20-7 8260B ND 1ug/kg2.95.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 104 53-142
Bromofluorobenzene 103 47-138
Toluene-d8 105 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-1 (4'-6')
QB12017-001
02/10/2015 1020
02/12/2015
Solid
% Solids:83.5 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 2255 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 24000 B 1ug/kg15008000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 85 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-2 (6'-8')
QB12017-002
02/10/2015 1100
02/12/2015
Solid
% Solids:82.6 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg200240
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-2 (6'-8')
QB12017-002
02/10/2015 1100
02/12/2015
Solid
% Solids:82.6 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1402 DCS 67778 7.01
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg5.817
Benzene 71-43-2 8260B ND 1ug/kg0.954.3
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.54.3
Bromoform 75-25-2 8260B ND 1ug/kg0.604.3
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg1.64.3
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg2.18.6
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.14.3
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.64.3
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.54.3
Chloroethane 75-00-3 8260B ND 1ug/kg1.14.3
Chloroform 67-66-3 8260B ND 1ug/kg0.724.3
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg0.864.3
Cyclohexane 110-82-7 8260B ND 1ug/kg0.584.3
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.34.3
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.54.3
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.734.3
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.54.3
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.54.3
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.54.3
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.44.3
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.634.3
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg0.864.3
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.54.3
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.664.3
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.34.3
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg0.794.3
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.594.3
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.714.3
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.54.3
2-Hexanone 591-78-6 8260B ND 1ug/kg1.18.6
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.204.3
Methyl acetate 79-20-9 8260B ND 1ug/kg0.854.3
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.354.3
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.38.6
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.354.3
Methylene chloride 75-09-2 8260B ND 1ug/kg2.24.3
Styrene 100-42-5 8260B ND 1ug/kg0.954.3
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.414.3
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.434.3
Toluene 108-88-3 8260B ND 1ug/kg1.54.3
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.544.3
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.54.3
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.734.3
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.684.3
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-2 (6'-8')
QB12017-002
02/10/2015 1100
02/12/2015
Solid
% Solids:82.6 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1402 DCS 67778 7.01
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg1.64.3
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.34.3
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.744.3
Xylenes (total)1330-20-7 8260B ND 1ug/kg2.54.3
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 104 53-142
Bromofluorobenzene 103 47-138
Toluene-d8 104 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-2 (6'-8')
QB12017-002
02/10/2015 1100
02/12/2015
Solid
% Solids:82.6 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 2316 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 24000 B 1ug/kg15008100
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 83 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-3 (6'-8')
QB12017-003
02/10/2015 1142
02/12/2015
Solid
% Solids:81.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg200240
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-3 (6'-8')
QB12017-003
02/10/2015 1142
02/12/2015
Solid
% Solids:81.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1423 DCS 67778 6.60
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 24 1ug/kg6.219
Benzene 71-43-2 8260B ND 1ug/kg1.04.6
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.64.6
Bromoform 75-25-2 8260B ND 1ug/kg0.654.6
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg1.74.6
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg2.29.3
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.24.6
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.74.6
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.64.6
Chloroethane 75-00-3 8260B ND 1ug/kg1.24.6
Chloroform 67-66-3 8260B ND 1ug/kg0.774.6
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg0.934.6
Cyclohexane 110-82-7 8260B ND 1ug/kg0.624.6
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.44.6
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.64.6
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.794.6
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.64.6
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.64.6
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.64.6
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.54.6
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.684.6
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg0.934.6
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.64.6
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.704.6
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.44.6
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg0.844.6
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.634.6
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.764.6
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.64.6
2-Hexanone 591-78-6 8260B ND 1ug/kg1.29.3
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.214.6
Methyl acetate 79-20-9 8260B ND 1ug/kg0.914.6
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.374.6
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.49.3
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.384.6
Methylene chloride 75-09-2 8260B ND 1ug/kg2.44.6
Styrene 100-42-5 8260B ND 1ug/kg1.04.6
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.444.6
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.464.6
Toluene 108-88-3 8260B ND 1ug/kg1.64.6
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.584.6
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.64.6
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.794.6
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.734.6
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-3 (6'-8')
QB12017-003
02/10/2015 1142
02/12/2015
Solid
% Solids:81.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1423 DCS 67778 6.60
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg1.84.6
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.44.6
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.804.6
Xylenes (total)1330-20-7 8260B ND 1ug/kg2.74.6
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 53-142
Bromofluorobenzene 102 47-138
Toluene-d8 105 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-3 (6'-8')
QB12017-003
02/10/2015 1142
02/12/2015
Solid
% Solids:81.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 2337 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 24000 B 1ug/kg15008100
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 84 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-4 (2'-4')
QB12017-004
02/10/2015 1110
02/12/2015
Solid
% Solids:80.7 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg210250
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 17 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-4 (2'-4')
QB12017-004
02/10/2015 1110
02/12/2015
Solid
% Solids:80.7 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1444 DCS 67778 5.27
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 120 1ug/kg7.924
Benzene 71-43-2 8260B ND 1ug/kg1.35.9
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.05.9
Bromoform 75-25-2 8260B ND 1ug/kg0.825.9
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.15.9
2-Butanone (MEK)78-93-3 8260B 14 1ug/kg2.812
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.55.9
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.15.9
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.05.9
Chloroethane 75-00-3 8260B ND 1ug/kg1.55.9
Chloroform 67-66-3 8260B ND 1ug/kg0.985.9
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.25.9
Cyclohexane 110-82-7 8260B ND 1ug/kg0.795.9
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.85.9
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.05.9
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg1.05.9
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.05.9
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.05.9
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.05.9
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.95.9
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.865.9
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.25.9
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.05.9
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.895.9
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.85.9
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.15.9
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.805.9
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.965.9
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.05.9
2-Hexanone 591-78-6 8260B ND 1ug/kg1.512
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.275.9
Methyl acetate 79-20-9 8260B ND 1ug/kg1.25.9
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.475.9
4-Methyl-2-pentanone 108-10-1 8260B 1.8 J 1ug/kg1.812
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.485.9
Methylene chloride 75-09-2 8260B ND 1ug/kg3.15.9
Styrene 100-42-5 8260B ND 1ug/kg1.35.9
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.555.9
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.595.9
Toluene 108-88-3 8260B ND 1ug/kg2.05.9
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.745.9
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.05.9
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg1.05.9
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.935.9
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 18 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-4 (2'-4')
QB12017-004
02/10/2015 1110
02/12/2015
Solid
% Solids:80.7 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1444 DCS 67778 5.27
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.25.9
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.85.9
Vinyl chloride 75-01-4 8260B ND 1ug/kg1.05.9
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.45.9
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 115 53-142
Bromofluorobenzene 110 47-138
Toluene-d8 111 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 19 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-4 (2'-4')
QB12017-004
02/10/2015 1110
02/12/2015
Solid
% Solids:80.7 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 2358 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 24000 B 1ug/kg15008300
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 81 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 20 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-9 (10'-12')
QB12017-005
02/10/2015 1205
02/12/2015
Solid
% Solids:79.9 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B 380 1mg/kg210250
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 21 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-9 (10'-12')
QB12017-005
02/10/2015 1205
02/12/2015
Solid
% Solids:79.9 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 1 02/16/2015 1406 DCS 67933 6.48
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 38 B 2ug/kg4.919
Benzene 71-43-2 8260B ND 2ug/kg1.54.8
Bromodichloromethane 75-27-4 8260B ND 2ug/kg1.64.8
Bromoform 75-25-2 8260B ND 2ug/kg1.94.8
Bromomethane (Methyl bromide)74-83-9 8260B ND 2ug/kg2.14.8
2-Butanone (MEK)78-93-3 8260B ND 2ug/kg4.19.7
Carbon disulfide 75-15-0 8260B ND 2ug/kg1.34.8
Carbon tetrachloride 56-23-5 8260B ND 2ug/kg1.44.8
Chlorobenzene 108-90-7 8260B ND 2ug/kg1.64.8
Chloroethane 75-00-3 8260B ND 2ug/kg2.34.8
Chloroform 67-66-3 8260B ND 2ug/kg1.44.8
Chloromethane (Methyl chloride)74-87-3 8260B ND 2ug/kg1.94.8
Cyclohexane 110-82-7 8260B ND 2ug/kg1.74.8
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 2ug/kg2.04.8
Dibromochloromethane 124-48-1 8260B ND 2ug/kg1.74.8
1,2-Dibromoethane (EDB)106-93-4 8260B ND 2ug/kg1.74.8
1,2-Dichlorobenzene 95-50-1 8260B 8.3 2ug/kg1.64.8
1,3-Dichlorobenzene 541-73-1 8260B ND 2ug/kg1.64.8
1,4-Dichlorobenzene 106-46-7 8260B ND 2ug/kg1.44.8
Dichlorodifluoromethane 75-71-8 8260B ND 2ug/kg3.64.8
1,1-Dichloroethane 75-34-3 8260B ND 2ug/kg1.44.8
1,2-Dichloroethane 107-06-2 8260B ND 2ug/kg1.54.8
1,1-Dichloroethene 75-35-4 8260B ND 2ug/kg1.74.8
cis-1,2-Dichloroethene 156-59-2 8260B ND 2ug/kg1.54.8
trans-1,2-Dichloroethene 156-60-5 8260B ND 2ug/kg1.54.8
1,2-Dichloropropane 78-87-5 8260B ND 2ug/kg1.44.8
cis-1,3-Dichloropropene 10061-01-5 8260B ND 2ug/kg1.44.8
trans-1,3-Dichloropropene 10061-02-6 8260B ND 2ug/kg1.54.8
Ethylbenzene 100-41-4 8260B 32 2ug/kg1.64.8
2-Hexanone 591-78-6 8260B ND 2ug/kg3.69.7
Isopropylbenzene 98-82-8 8260B 5.4 2ug/kg1.54.8
Methyl acetate 79-20-9 8260B ND 2ug/kg0.954.8
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 6.7 2ug/kg0.394.8
4-Methyl-2-pentanone 108-10-1 8260B ND 2ug/kg1.49.7
Methylcyclohexane 108-87-2 8260B 11 2ug/kg0.404.8
Methylene chloride 75-09-2 8260B ND 2ug/kg2.54.8
Styrene 100-42-5 8260B ND 2ug/kg1.14.8
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 2ug/kg0.454.8
Tetrachloroethene 127-18-4 8260B 0.83 J 2ug/kg0.484.8
Toluene 108-88-3 8260B ND 2ug/kg1.64.8
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 2ug/kg0.614.8
1,2,4-Trichlorobenzene 120-82-1 8260B ND 2ug/kg1.64.8
1,1,1-Trichloroethane 71-55-6 8260B ND 2ug/kg0.824.8
1,1,2-Trichloroethane 79-00-5 8260B ND 2ug/kg0.764.8
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 22 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-9 (10'-12')
QB12017-005
02/10/2015 1205
02/12/2015
Solid
% Solids:79.9 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 1 02/16/2015 1406 DCS 67933 6.48
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 2ug/kg1.84.8
Trichlorofluoromethane 75-69-4 8260B ND 2ug/kg1.44.8
Vinyl chloride 75-01-4 8260B ND 2ug/kg0.834.8
Xylenes (total)1330-20-7 8260B 190 2ug/kg2.84.8
AcceptanceRun 2
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 95 53-142
Bromofluorobenzene 93 47-138
Toluene-d8 96 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 23 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-9 (10'-12')
QB12017-005
02/10/2015 1205
02/12/2015
Solid
% Solids:79.9 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0100 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 5300000 B 1ug/kg1500081000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 84 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 24 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-13 (2'-4')
QB12017-006
02/10/2015 1412
02/12/2015
Solid
% Solids:67.7 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg250300
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 25 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-13 (2'-4')
QB12017-006
02/10/2015 1412
02/12/2015
Solid
% Solids:67.7 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1526 DCS 67778 5.43
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 14 J 1ug/kg9.127
Benzene 71-43-2 8260B ND 1ug/kg1.56.8
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.36.8
Bromoform 75-25-2 8260B ND 1ug/kg0.956.8
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.46.8
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg3.314
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.86.8
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.46.8
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.36.8
Chloroethane 75-00-3 8260B ND 1ug/kg1.86.8
Chloroform 67-66-3 8260B ND 1ug/kg1.16.8
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.46.8
Cyclohexane 110-82-7 8260B ND 1ug/kg0.926.8
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.06.8
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.36.8
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg1.26.8
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.36.8
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.36.8
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.36.8
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.26.8
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.996.8
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.46.8
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.36.8
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg1.06.8
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.06.8
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.26.8
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.936.8
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg1.16.8
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.36.8
2-Hexanone 591-78-6 8260B ND 1ug/kg1.814
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.316.8
Methyl acetate 79-20-9 8260B ND 1ug/kg1.36.8
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.546.8
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg2.014
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.566.8
Methylene chloride 75-09-2 8260B ND 1ug/kg3.56.8
Styrene 100-42-5 8260B ND 1ug/kg1.56.8
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.646.8
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.686.8
Toluene 108-88-3 8260B ND 1ug/kg2.36.8
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.866.8
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.36.8
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg1.26.8
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg1.16.8
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 26 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-13 (2'-4')
QB12017-006
02/10/2015 1412
02/12/2015
Solid
% Solids:67.7 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1526 DCS 67778 5.43
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.66.8
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.06.8
Vinyl chloride 75-01-4 8260B ND 1ug/kg1.26.8
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.96.8
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 100 53-142
Bromofluorobenzene 102 47-138
Toluene-d8 105 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 27 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-13 (2'-4')
QB12017-006
02/10/2015 1412
02/12/2015
Solid
% Solids:67.7 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0121 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 39000 BJ 1ug/kg1800096000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 83 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 28 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-14 (6'-8')
QB12017-007
02/10/2015 1430
02/12/2015
Solid
% Solids:68.3 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg240290
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 29 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-14 (6'-8')
QB12017-007
02/10/2015 1430
02/12/2015
Solid
% Solids:68.3 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1547 DCS 67778 6.74
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 52 1ug/kg7.322
Benzene 71-43-2 8260B ND 1ug/kg1.25.4
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.85.4
Bromoform 75-25-2 8260B ND 1ug/kg0.765.4
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.05.4
2-Butanone (MEK)78-93-3 8260B 8.5 J 1ug/kg2.611
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.45.4
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.05.4
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.85.4
Chloroethane 75-00-3 8260B ND 1ug/kg1.45.4
Chloroform 67-66-3 8260B ND 1ug/kg0.905.4
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.15.4
Cyclohexane 110-82-7 8260B ND 1ug/kg0.735.4
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.65.4
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.85.4
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.925.4
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.85.4
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.85.4
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.85.4
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.75.4
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.795.4
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.15.4
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.85.4
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.835.4
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.65.4
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg0.995.4
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.745.4
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.895.4
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.85.4
2-Hexanone 591-78-6 8260B ND 1ug/kg1.411
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.255.4
Methyl acetate 79-20-9 8260B ND 1ug/kg1.15.4
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.435.4
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.611
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.455.4
Methylene chloride 75-09-2 8260B ND 1ug/kg2.85.4
Styrene 100-42-5 8260B ND 1ug/kg1.25.4
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.515.4
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.545.4
Toluene 108-88-3 8260B ND 1ug/kg1.85.4
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.685.4
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.85.4
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.925.4
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.865.4
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 30 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-14 (6'-8')
QB12017-007
02/10/2015 1430
02/12/2015
Solid
% Solids:68.3 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1547 DCS 67778 6.74
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.4
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.65.4
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.935.4
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.15.4
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 53-142
Bromofluorobenzene 102 47-138
Toluene-d8 105 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 31 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-14 (6'-8')
QB12017-007
02/10/2015 1430
02/12/2015
Solid
% Solids:68.3 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0142 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 3300 BJ 1ug/kg18009700
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 81 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 32 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-7 (12'-15')
QB12017-008
02/10/2015 1555
02/12/2015
Solid
% Solids:81.2 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg210250
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 33 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-7 (12'-15')
QB12017-008
02/10/2015 1555
02/12/2015
Solid
% Solids:81.2 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 100 02/18/2015 1324 DCS 68101 5.38
3 5035 8260B 1000 02/18/2015 1449 DCS 68116 5.38
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 2ug/kg5802300
Benzene 71-43-2 8260B ND 2ug/kg180570
Bromodichloromethane 75-27-4 8260B ND 2ug/kg190570
Bromoform 75-25-2 8260B ND 2ug/kg230570
Bromomethane (Methyl bromide)74-83-9 8260B ND 2ug/kg250570
2-Butanone (MEK)78-93-3 8260B ND 2ug/kg4801100
Carbon disulfide 75-15-0 8260B ND 2ug/kg150570
Carbon tetrachloride 56-23-5 8260B ND 2ug/kg160570
Chlorobenzene 108-90-7 8260B ND 2ug/kg180570
Chloroethane 75-00-3 8260B ND 2ug/kg270570
Chloroform 67-66-3 8260B ND 2ug/kg170570
Chloromethane (Methyl chloride)74-87-3 8260B ND 2ug/kg230570
Cyclohexane 110-82-7 8260B ND 2ug/kg200570
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 2ug/kg240570
Dibromochloromethane 124-48-1 8260B ND 2ug/kg200570
1,2-Dibromoethane (EDB)106-93-4 8260B ND 2ug/kg200570
1,2-Dichlorobenzene 95-50-1 8260B ND 2ug/kg190570
1,3-Dichlorobenzene 541-73-1 8260B ND 2ug/kg190570
1,4-Dichlorobenzene 106-46-7 8260B ND 2ug/kg170570
Dichlorodifluoromethane 75-71-8 8260B ND 2ug/kg430570
1,1-Dichloroethane 75-34-3 8260B ND 2ug/kg170570
1,2-Dichloroethane 107-06-2 8260B ND 2ug/kg180570
1,1-Dichloroethene 75-35-4 8260B ND 2ug/kg210570
cis-1,2-Dichloroethene 156-59-2 8260B ND 2ug/kg180570
trans-1,2-Dichloroethene 156-60-5 8260B ND 2ug/kg170570
1,2-Dichloropropane 78-87-5 8260B ND 2ug/kg170570
cis-1,3-Dichloropropene 10061-01-5 8260B ND 2ug/kg170570
trans-1,3-Dichloropropene 10061-02-6 8260B ND 2ug/kg170570
Ethylbenzene 100-41-4 8260B 26000 3ug/kg19005700
2-Hexanone 591-78-6 8260B ND 2ug/kg4301100
Isopropylbenzene 98-82-8 8260B 5800 2ug/kg180570
Methyl acetate 79-20-9 8260B ND 2ug/kg200570
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 2ug/kg180570
4-Methyl-2-pentanone 108-10-1 8260B ND 2ug/kg4201100
Methylcyclohexane 108-87-2 8260B 5000 2ug/kg190570
Methylene chloride 75-09-2 8260B ND 2ug/kg140570
Styrene 100-42-5 8260B ND 2ug/kg200570
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 2ug/kg54570
Tetrachloroethene 127-18-4 8260B ND 2ug/kg57570
Toluene 108-88-3 8260B 50000 3ug/kg19005700
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 2ug/kg72570
1,2,4-Trichlorobenzene 120-82-1 8260B ND 2ug/kg190570
1,1,1-Trichloroethane 71-55-6 8260B ND 2ug/kg97570
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 34 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-7 (12'-15')
QB12017-008
02/10/2015 1555
02/12/2015
Solid
% Solids:81.2 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 100 02/18/2015 1324 DCS 68101 5.38
3 5035 8260B 1000 02/18/2015 1449 DCS 68116 5.38
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,1,2-Trichloroethane 79-00-5 8260B ND 2ug/kg210570
Trichloroethene 79-01-6 8260B ND 2ug/kg220570
Trichlorofluoromethane 75-69-4 8260B ND 2ug/kg170570
Vinyl chloride 75-01-4 8260B ND 2ug/kg98570
Xylenes (total)1330-20-7 8260B 140000 3ug/kg33005700
AcceptanceAcceptanceRun 3Run 2
Surrogate Q % Recovery Limits % Recovery LimitsQ
1,2-Dichloroethane-d4 85 53-142 92 53-142
Bromofluorobenzene 98 47-138 117 47-138
Toluene-d8 95 68-124 97 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 35 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-7 (12'-15')
QB12017-008
02/10/2015 1555
02/12/2015
Solid
% Solids:81.2 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0203 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 290000 B 1ug/kg15008200
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 81 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 36 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
Page: 37 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - MB
Batch:
Sample ID:QQ67843-001
67843
Analytical Method:9071B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
HEM (oil and grease)ND 02/14/2015 1120200170mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 38 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - LCS
Batch:
Sample ID:QQ67843-002
67843
Analytical Method:9071B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
HEM (oil and grease)2200 02/14/2015 1120110200070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 39 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ67778-001
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 02/13/2015 1102206.7 ug/kg1
Benzene ND 02/13/2015 11025.0 1.1 ug/kg1
Bromodichloromethane ND 02/13/2015 11025.0 1.7 ug/kg1
Bromoform ND 02/13/2015 11025.0 0.70 ug/kg1
Bromomethane (Methyl bromide)ND 02/13/2015 11025.0 1.8 ug/kg1
2-Butanone (MEK)ND 02/13/2015 1102102.4 ug/kg1
Carbon disulfide ND 02/13/2015 11025.0 1.3 ug/kg1
Carbon tetrachloride ND 02/13/2015 11025.0 1.8 ug/kg1
Chlorobenzene ND 02/13/2015 11025.0 1.7 ug/kg1
Chloroethane ND 02/13/2015 11025.0 1.3 ug/kg1
Chloroform ND 02/13/2015 11025.0 0.83 ug/kg1
Chloromethane (Methyl chloride)ND 02/13/2015 11025.0 1.0 ug/kg1
Cyclohexane ND 02/13/2015 11025.0 0.67 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 02/13/2015 11025.0 1.5 ug/kg1
Dibromochloromethane ND 02/13/2015 11025.0 1.7 ug/kg1
1,2-Dibromoethane (EDB)ND 02/13/2015 11025.0 0.85 ug/kg1
1,3-Dichlorobenzene ND 02/13/2015 11025.0 1.7 ug/kg1
1,2-Dichlorobenzene ND 02/13/2015 11025.0 1.7 ug/kg1
1,4-Dichlorobenzene ND 02/13/2015 11025.0 1.7 ug/kg1
Dichlorodifluoromethane ND 02/13/2015 11025.0 1.6 ug/kg1
1,1-Dichloroethane ND 02/13/2015 11025.0 0.73 ug/kg1
1,2-Dichloroethane ND 02/13/2015 11025.0 1.0 ug/kg1
1,1-Dichloroethene ND 02/13/2015 11025.0 1.7 ug/kg1
cis-1,2-Dichloroethene ND 02/13/2015 11025.0 0.76 ug/kg1
trans-1,2-Dichloroethene ND 02/13/2015 11025.0 1.5 ug/kg1
1,2-Dichloropropane ND 02/13/2015 11025.0 0.91 ug/kg1
cis-1,3-Dichloropropene ND 02/13/2015 11025.0 0.68 ug/kg1
trans-1,3-Dichloropropene ND 02/13/2015 11025.0 0.82 ug/kg1
Ethylbenzene ND 02/13/2015 11025.0 1.7 ug/kg1
2-Hexanone ND 02/13/2015 1102101.3 ug/kg1
Isopropylbenzene ND 02/13/2015 11025.0 0.23 ug/kg1
Methyl acetate ND 02/13/2015 11025.0 0.98 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 02/13/2015 11025.0 0.40 ug/kg1
4-Methyl-2-pentanone ND 02/13/2015 1102101.5 ug/kg1
Methylcyclohexane ND 02/13/2015 11025.0 0.41 ug/kg1
Methylene chloride ND 02/13/2015 11025.0 2.6 ug/kg1
Styrene ND 02/13/2015 11025.0 1.1 ug/kg1
1,1,2,2-Tetrachloroethane ND 02/13/2015 11025.0 0.47 ug/kg1
Tetrachloroethene ND 02/13/2015 11025.0 0.50 ug/kg1
Toluene ND 02/13/2015 11025.0 1.7 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 02/13/2015 11025.0 0.63 ug/kg1
1,2,4-Trichlorobenzene ND 02/13/2015 11025.0 1.7 ug/kg1
1,1,2-Trichloroethane ND 02/13/2015 11025.0 0.79 ug/kg1
1,1,1-Trichloroethane ND 02/13/2015 11025.0 0.85 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 40 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ67778-001
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Trichloroethene ND 02/13/2015 11025.0 1.9 ug/kg1
Trichlorofluoromethane ND 02/13/2015 11025.0 1.5 ug/kg1
Vinyl chloride ND 02/13/2015 11025.0 0.86 ug/kg1
Xylenes (total)ND 02/13/2015 11025.0 2.9 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 47-138
1,2-Dichloroethane-d4 99 53-142
Toluene-d8 106 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 41 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ67778-002
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 130 02/13/2015 102013010060-1401
Benzene 56 02/13/2015 10201125069-1231
Bromodichloromethane 55 02/13/2015 10201115069-1211
Bromoform 53 02/13/2015 10201055061-1191
Bromomethane (Methyl bromide)59 02/13/2015 10201175010-1681
2-Butanone (MEK)110 02/13/2015 102011210057-1481
Carbon disulfide 58 02/13/2015 10201175058-1221
Carbon tetrachloride 59 02/13/2015 10201185058-1361
Chlorobenzene 54 02/13/2015 10201085059-1291
Chloroethane 59 02/13/2015 10201195042-1631
Chloroform 57 02/13/2015 10201145071-1251
Chloromethane (Methyl chloride)59 02/13/2015 10201185034-1341
Cyclohexane 57 02/13/2015 10201145053-1391
1,2-Dibromo-3-chloropropane (DBCP)49 02/13/2015 1020995055-1251
Dibromochloromethane 53 02/13/2015 10201065066-1191
1,2-Dibromoethane (EDB)53 02/13/2015 10201065074-1241
1,3-Dichlorobenzene 54 02/13/2015 10201085051-1341
1,2-Dichlorobenzene 54 02/13/2015 10201075057-1311
1,4-Dichlorobenzene 53 02/13/2015 10201055052-1331
Dichlorodifluoromethane 66 02/13/2015 10201325010-1571
1,1-Dichloroethane 57 02/13/2015 10201145071-1271
1,2-Dichloroethane 55 02/13/2015 10201105067-1291
1,1-Dichloroethene 61 02/13/2015 10201225069-1381
cis-1,2-Dichloroethene 57 02/13/2015 10201145070-1221
trans-1,2-Dichloroethene 59 02/13/2015 10201185068-1311
1,2-Dichloropropane 55 02/13/2015 10201105072-1241
cis-1,3-Dichloropropene 56 02/13/2015 10201125070-1261
trans-1,3-Dichloropropene 55 02/13/2015 10201095070-1241
Ethylbenzene 56 02/13/2015 10201125059-1281
2-Hexanone 94 02/13/2015 10209410054-1371
Isopropylbenzene 57 02/13/2015 10201135050-1361
Methyl acetate 54 02/13/2015 10201085059-1371
Methyl tertiary butyl ether (MTBE)55 02/13/2015 10201095070-1301
4-Methyl-2-pentanone 97 02/13/2015 10209710060-1341
Methylcyclohexane 58 02/13/2015 10201165041-1441
Methylene chloride 56 02/13/2015 10201135070-1301
Styrene 54 02/13/2015 10201095054-1361
1,1,2,2-Tetrachloroethane 52 02/13/2015 10201045069-1321
Tetrachloroethene 57 02/13/2015 10201145045-1501
Toluene 56 02/13/2015 10201125061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 68 02/13/2015 1020N1375049-1361
1,2,4-Trichlorobenzene 55 02/13/2015 10201115034-1451
1,1,2-Trichloroethane 50 02/13/2015 10201005055-1281
1,1,1-Trichloroethane 58 02/13/2015 10201175063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 42 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ67778-002
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 56 02/13/2015 10201125062-1261
Trichlorofluoromethane 60 02/13/2015 10201195045-1381
Vinyl chloride 61 02/13/2015 10201215042-1321
Xylenes (total)110 02/13/2015 102011010058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 98 47-138
1,2-Dichloroethane-d4 94 53-142
Toluene-d8 106 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 43 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:QB12017-001MS
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acetone 140 02/13/2015 19177511060-140601
Benzene 33 02/13/2015 1917N615469-123ND1
Bromodichloromethane 30 02/13/2015 1917N565469-121ND1
Bromoform 25 02/13/2015 1917N475461-119ND1
Bromomethane (Methyl bromide)40 02/13/2015 1917755435-144ND1
2-Butanone (MEK)66 02/13/2015 1917N5611057-1485.8 1
Carbon disulfide 35 02/13/2015 1917665458-122ND1
Carbon tetrachloride 37 02/13/2015 1917685458-136ND1
Chlorobenzene 28 02/13/2015 1917N535459-129ND1
Chloroethane 42 02/13/2015 1917775450-132ND1
Chloroform 33 02/13/2015 1917N615471-125ND1
Chloromethane (Methyl chloride)40 02/13/2015 1917755434-134ND1
Cyclohexane 38 02/13/2015 1917705453-139ND1
1,2-Dibromo-3-chloropropane (DBCP)26 02/13/2015 1917N485455-125ND1
Dibromochloromethane 26 02/13/2015 1917N495466-119ND1
1,2-Dibromoethane (EDB)28 02/13/2015 1917N525474-124ND1
1,2-Dichlorobenzene 24 02/13/2015 1917N455457-131ND1
1,3-Dichlorobenzene 25 02/13/2015 1917N465451-134ND1
1,4-Dichlorobenzene 23 02/13/2015 1917N435452-133ND1
Dichlorodifluoromethane 46 02/13/2015 1917875410-157ND1
1,1-Dichloroethane 34 02/13/2015 1917N645471-127ND1
1,2-Dichloroethane 30 02/13/2015 1917N565467-129ND1
1,1-Dichloroethene 38 02/13/2015 1917715469-138ND1
cis-1,2-Dichloroethene 33 02/13/2015 1917N625470-122ND1
trans-1,2-Dichloroethene 35 02/13/2015 1917N655468-131ND1
1,2-Dichloropropane 31 02/13/2015 1917N585472-124ND1
cis-1,3-Dichloropropene 29 02/13/2015 1917N535470-126ND1
trans-1,3-Dichloropropene 27 02/13/2015 1917N505470-124ND1
Ethylbenzene 31 02/13/2015 1917N585459-128ND1
2-Hexanone 50 02/13/2015 1917N4611054-137ND1
Isopropylbenzene 32 02/13/2015 1917595450-136ND1
Methyl acetate 32 02/13/2015 1917605459-137ND1
Methyl tertiary butyl ether (MTBE)31 02/13/2015 1917N575470-130ND1
4-Methyl-2-pentanone 56 02/13/2015 1917N5211060-134ND1
Methylcyclohexane 38 02/13/2015 1917705441-144ND1
Methylene chloride 31 02/13/2015 1917N585477-129ND1
Styrene 27 02/13/2015 1917N495454-136ND1
1,1,2,2-Tetrachloroethane 28 02/13/2015 1917N525469-132ND1
Tetrachloroethene 33 02/13/2015 1917N625470-130ND1
Toluene 33 02/13/2015 1917615461-129ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane 45 02/13/2015 1917835449-136ND1
1,2,4-Trichlorobenzene 18 02/13/2015 1917345434-145ND1
1,1,1-Trichloroethane 37 02/13/2015 1917695463-128ND1
1,1,2-Trichloroethane 27 02/13/2015 1917N505455-128ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 44 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:QB12017-001MS
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Trichloroethene 33 02/13/2015 1917N615462-126ND1
Trichlorofluoromethane 43 02/13/2015 1917805445-138ND1
Vinyl chloride 44 02/13/2015 1917825442-132ND1
Xylenes (total)62 02/13/2015 1917N5711058-128ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 97 53-142
Bromofluorobenzene 102 47-138
Toluene-d8 104 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 45 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ67933-001
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone 5.8 02/16/2015 1241J205.1 ug/kg1
Benzene ND 02/16/2015 12415.0 1.6 ug/kg1
Bromodichloromethane ND 02/16/2015 12415.0 1.7 ug/kg1
Bromoform ND 02/16/2015 12415.0 2.0 ug/kg1
Bromomethane (Methyl bromide)ND 02/16/2015 12415.0 2.2 ug/kg1
2-Butanone (MEK)ND 02/16/2015 1241104.2 ug/kg1
Carbon disulfide ND 02/16/2015 12415.0 1.3 ug/kg1
Carbon tetrachloride ND 02/16/2015 12415.0 1.4 ug/kg1
Chlorobenzene ND 02/16/2015 12415.0 1.6 ug/kg1
Chloroethane ND 02/16/2015 12415.0 2.4 ug/kg1
Chloroform ND 02/16/2015 12415.0 1.5 ug/kg1
Chloromethane (Methyl chloride)ND 02/16/2015 12415.0 2.0 ug/kg1
Cyclohexane ND 02/16/2015 12415.0 1.7 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 02/16/2015 12415.0 2.1 ug/kg1
Dibromochloromethane ND 02/16/2015 12415.0 1.7 ug/kg1
1,2-Dibromoethane (EDB)ND 02/16/2015 12415.0 1.7 ug/kg1
1,4-Dichlorobenzene ND 02/16/2015 12415.0 1.5 ug/kg1
1,2-Dichlorobenzene ND 02/16/2015 12415.0 1.7 ug/kg1
1,3-Dichlorobenzene ND 02/16/2015 12415.0 1.7 ug/kg1
Dichlorodifluoromethane ND 02/16/2015 12415.0 3.7 ug/kg1
1,2-Dichloroethane ND 02/16/2015 12415.0 1.6 ug/kg1
1,1-Dichloroethane ND 02/16/2015 12415.0 1.5 ug/kg1
trans-1,2-Dichloroethene ND 02/16/2015 12415.0 1.5 ug/kg1
cis-1,2-Dichloroethene ND 02/16/2015 12415.0 1.6 ug/kg1
1,1-Dichloroethene ND 02/16/2015 12415.0 1.8 ug/kg1
1,2-Dichloropropane ND 02/16/2015 12415.0 1.5 ug/kg1
trans-1,3-Dichloropropene ND 02/16/2015 12415.0 1.5 ug/kg1
cis-1,3-Dichloropropene ND 02/16/2015 12415.0 1.5 ug/kg1
Ethylbenzene ND 02/16/2015 12415.0 1.6 ug/kg1
2-Hexanone ND 02/16/2015 1241103.8 ug/kg1
Isopropylbenzene ND 02/16/2015 12415.0 1.5 ug/kg1
Methyl acetate ND 02/16/2015 12415.0 0.98 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 02/16/2015 12415.0 0.40 ug/kg1
4-Methyl-2-pentanone ND 02/16/2015 1241101.5 ug/kg1
Methylcyclohexane ND 02/16/2015 12415.0 0.41 ug/kg1
Methylene chloride ND 02/16/2015 12415.0 2.6 ug/kg1
Styrene ND 02/16/2015 12415.0 1.1 ug/kg1
1,1,2,2-Tetrachloroethane ND 02/16/2015 12415.0 0.47 ug/kg1
Tetrachloroethene ND 02/16/2015 12415.0 0.50 ug/kg1
Toluene ND 02/16/2015 12415.0 1.7 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 02/16/2015 12415.0 0.63 ug/kg1
1,2,4-Trichlorobenzene ND 02/16/2015 12415.0 1.7 ug/kg1
1,1,2-Trichloroethane ND 02/16/2015 12415.0 0.79 ug/kg1
1,1,1-Trichloroethane ND 02/16/2015 12415.0 0.85 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 46 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ67933-001
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Trichloroethene ND 02/16/2015 12415.0 1.9 ug/kg1
Trichlorofluoromethane ND 02/16/2015 12415.0 1.5 ug/kg1
Vinyl chloride ND 02/16/2015 12415.0 0.86 ug/kg1
Xylenes (total)ND 02/16/2015 12415.0 2.9 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 93 47-138
1,2-Dichloroethane-d4 94 53-142
Toluene-d8 94 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 47 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ67933-002
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 100 02/16/2015 114410010060-1401
Benzene 46 02/16/2015 1144935069-1231
Bromodichloromethane 48 02/16/2015 1144965069-1211
Bromoform 48 02/16/2015 1144965061-1191
Bromomethane (Methyl bromide)56 02/16/2015 11441115010-1681
2-Butanone (MEK)94 02/16/2015 11449410057-1481
Carbon disulfide 45 02/16/2015 1144905058-1221
Carbon tetrachloride 48 02/16/2015 1144975058-1361
Chlorobenzene 47 02/16/2015 1144955059-1291
Chloroethane 55 02/16/2015 11441105042-1631
Chloroform 48 02/16/2015 1144955071-1251
Chloromethane (Methyl chloride)56 02/16/2015 11441115034-1341
Cyclohexane 46 02/16/2015 1144925053-1391
1,2-Dibromo-3-chloropropane (DBCP)47 02/16/2015 1144945055-1251
Dibromochloromethane 49 02/16/2015 1144975066-1191
1,2-Dibromoethane (EDB)47 02/16/2015 1144945074-1241
1,4-Dichlorobenzene 48 02/16/2015 1144965052-1331
1,2-Dichlorobenzene 48 02/16/2015 1144965057-1311
1,3-Dichlorobenzene 49 02/16/2015 1144975051-1341
Dichlorodifluoromethane 60 02/16/2015 11441195010-1571
1,2-Dichloroethane 46 02/16/2015 1144925067-1291
1,1-Dichloroethane 47 02/16/2015 1144945071-1271
trans-1,2-Dichloroethene 47 02/16/2015 1144945068-1311
cis-1,2-Dichloroethene 48 02/16/2015 1144965070-1221
1,1-Dichloroethene 46 02/16/2015 1144925069-1381
1,2-Dichloropropane 46 02/16/2015 1144935072-1241
trans-1,3-Dichloropropene 48 02/16/2015 1144955070-1241
cis-1,3-Dichloropropene 47 02/16/2015 1144955070-1261
Ethylbenzene 48 02/16/2015 1144965059-1281
2-Hexanone 91 02/16/2015 11449110054-1371
Isopropylbenzene 49 02/16/2015 1144985050-1361
Methyl acetate 49 02/16/2015 1144975059-1371
Methyl tertiary butyl ether (MTBE)46 02/16/2015 1144925070-1301
4-Methyl-2-pentanone 90 02/16/2015 11449010060-1341
Methylcyclohexane 47 02/16/2015 1144935041-1441
Methylene chloride 43 02/16/2015 1144865070-1301
Styrene 49 02/16/2015 1144975054-1361
1,1,2,2-Tetrachloroethane 47 02/16/2015 1144945069-1321
Tetrachloroethene 48 02/16/2015 1144965045-1501
Toluene 44 02/16/2015 1144885061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 46 02/16/2015 1144935049-1361
1,2,4-Trichlorobenzene 47 02/16/2015 1144955034-1451
1,1,2-Trichloroethane 46 02/16/2015 1144925055-1281
1,1,1-Trichloroethane 48 02/16/2015 1144975063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 48 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ67933-002
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 47 02/16/2015 1144945062-1261
Trichlorofluoromethane 56 02/16/2015 11441125045-1381
Vinyl chloride 57 02/16/2015 11441145042-1321
Xylenes (total)95 02/16/2015 11449510058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 92 47-138
1,2-Dichloroethane-d4 85 53-142
Toluene-d8 94 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 49 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ68101-001
68101 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 02/18/2015 11541000250ug/kg50
Benzene ND 02/18/2015 115425078ug/kg50
Bromodichloromethane ND 02/18/2015 115425084ug/kg50
Bromoform ND 02/18/2015 115425099ug/kg50
Bromomethane (Methyl bromide)ND 02/18/2015 1154250110ug/kg50
2-Butanone (MEK)ND 02/18/2015 1154500210ug/kg50
Carbon disulfide ND 02/18/2015 115425067ug/kg50
Carbon tetrachloride ND 02/18/2015 115425072ug/kg50
Chlorobenzene ND 02/18/2015 115425081ug/kg50
Chloroethane ND 02/18/2015 1154250120ug/kg50
Chloroform ND 02/18/2015 115425075ug/kg50
Chloromethane (Methyl chloride)ND 02/18/2015 1154250100ug/kg50
Cyclohexane ND 02/18/2015 115425087ug/kg50
1,2-Dibromo-3-chloropropane (DBCP)ND 02/18/2015 1154250100ug/kg50
Dibromochloromethane ND 02/18/2015 115425086ug/kg50
1,2-Dibromoethane (EDB)ND 02/18/2015 115425086ug/kg50
1,4-Dichlorobenzene ND 02/18/2015 115425075ug/kg50
1,3-Dichlorobenzene ND 02/18/2015 115425084ug/kg50
1,2-Dichlorobenzene ND 02/18/2015 115425085ug/kg50
Dichlorodifluoromethane ND 02/18/2015 1154250190ug/kg50
1,2-Dichloroethane ND 02/18/2015 115425080ug/kg50
1,1-Dichloroethane ND 02/18/2015 115425074ug/kg50
trans-1,2-Dichloroethene ND 02/18/2015 115425076ug/kg50
cis-1,2-Dichloroethene ND 02/18/2015 115425079ug/kg50
1,1-Dichloroethene ND 02/18/2015 115425091ug/kg50
1,2-Dichloropropane ND 02/18/2015 115425075ug/kg50
trans-1,3-Dichloropropene ND 02/18/2015 115425076ug/kg50
cis-1,3-Dichloropropene ND 02/18/2015 115425075ug/kg50
2-Hexanone ND 02/18/2015 1154500190ug/kg50
Isopropylbenzene ND 02/18/2015 115425077ug/kg50
Methyl acetate ND 02/18/2015 115425090ug/kg50
Methyl tertiary butyl ether (MTBE)ND 02/18/2015 115425079ug/kg50
4-Methyl-2-pentanone ND 02/18/2015 1154500180ug/kg50
Methylcyclohexane ND 02/18/2015 115425084ug/kg50
Methylene chloride ND 02/18/2015 115425062ug/kg50
Styrene ND 02/18/2015 115425086ug/kg50
1,1,2,2-Tetrachloroethane ND 02/18/2015 115425024ug/kg50
Tetrachloroethene ND 02/18/2015 115425025ug/kg50
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 02/18/2015 115425032ug/kg50
1,2,4-Trichlorobenzene ND 02/18/2015 115425085ug/kg50
1,1,2-Trichloroethane ND 02/18/2015 115425092ug/kg50
1,1,1-Trichloroethane ND 02/18/2015 115425043ug/kg50
Trichloroethene ND 02/18/2015 115425095ug/kg50
Trichlorofluoromethane ND 02/18/2015 115425075ug/kg50
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 50 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ68101-001
68101 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Vinyl chloride ND 02/18/2015 115425043ug/kg50
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 114 47-138
1,2-Dichloroethane-d4 102 53-142
Toluene-d8 104 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 51 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ68101-002
68101 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 5400 02/18/2015 1031109500060-14050
Benzene 2600 02/18/2015 1031105250069-12350
Bromodichloromethane 2600 02/18/2015 1031105250069-12150
Bromoform 2500 02/18/2015 1031101250061-11950
Bromomethane (Methyl bromide)1900 02/18/2015 103178250010-16850
2-Butanone (MEK)5400 02/18/2015 1031107500057-14850
Carbon disulfide 2600 02/18/2015 1031103250058-12250
Carbon tetrachloride 2800 02/18/2015 1031113250058-13650
Chlorobenzene 2600 02/18/2015 1031104250059-12950
Chloroethane 2100 02/18/2015 103184250042-16350
Chloroform 2700 02/18/2015 1031107250071-12550
Chloromethane (Methyl chloride)2300 02/18/2015 103192250034-13450
Cyclohexane 2500 02/18/2015 1031102250053-13950
1,2-Dibromo-3-chloropropane (DBCP)2600 02/18/2015 1031104250055-12550
Dibromochloromethane 2600 02/18/2015 1031102250066-11950
1,2-Dibromoethane (EDB)2600 02/18/2015 1031102250074-12450
1,4-Dichlorobenzene 2500 02/18/2015 103199250052-13350
1,3-Dichlorobenzene 2500 02/18/2015 1031102250051-13450
1,2-Dichlorobenzene 2600 02/18/2015 1031103250057-13150
Dichlorodifluoromethane 1700 02/18/2015 103168250010-15750
1,2-Dichloroethane 2700 02/18/2015 1031107250067-12950
1,1-Dichloroethane 2700 02/18/2015 1031109250071-12750
trans-1,2-Dichloroethene 2700 02/18/2015 1031108250068-13150
cis-1,2-Dichloroethene 2700 02/18/2015 1031110250070-12250
1,1-Dichloroethene 2700 02/18/2015 1031108250069-13850
1,2-Dichloropropane 2700 02/18/2015 1031107250072-12450
trans-1,3-Dichloropropene 2600 02/18/2015 1031105250070-12450
cis-1,3-Dichloropropene 2700 02/18/2015 1031106250070-12650
2-Hexanone 5100 02/18/2015 1031101500054-13750
Isopropylbenzene 2700 02/18/2015 1031108250050-13650
Methyl acetate 2800 02/18/2015 1031112250059-13750
Methyl tertiary butyl ether (MTBE)2600 02/18/2015 1031106250070-13050
4-Methyl-2-pentanone 5100 02/18/2015 1031102500060-13450
Methylcyclohexane 2700 02/18/2015 1031109250041-14450
Methylene chloride 2400 02/18/2015 103197250070-13050
Styrene 2600 02/18/2015 1031104250054-13650
1,1,2,2-Tetrachloroethane 2600 02/18/2015 1031105250069-13250
Tetrachloroethene 2700 02/18/2015 1031108250045-15050
1,1,2-Trichloro-1,2,2-Trifluoroethane 2700 02/18/2015 1031107250049-13650
1,2,4-Trichlorobenzene 2400 02/18/2015 103196250034-14550
1,1,2-Trichloroethane 2500 02/18/2015 1031100250055-12850
1,1,1-Trichloroethane 2700 02/18/2015 1031109250063-12850
Trichloroethene 2700 02/18/2015 1031107250062-12650
Trichlorofluoromethane 2700 02/18/2015 1031107250045-13850
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 52 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ68101-002
68101 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Vinyl chloride 2500 02/18/2015 103199250042-13250
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 96 47-138
1,2-Dichloroethane-d4 82 53-142
Toluene-d8 88 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 53 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:QQ68101-003
68101 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 5300 02/18/2015 1051106500060-1402.3 2050
Benzene 2500 02/18/2015 1051102250069-1232.7 2050
Bromodichloromethane 2600 02/18/2015 1051104250069-1211.4 2050
Bromoform 2500 02/18/2015 1051100250061-1191.0 2050
Bromomethane (Methyl bromide)1700 02/18/2015 105170250010-16811 2050
2-Butanone (MEK)5000 02/18/2015 1051100500057-1486.9 2050
Carbon disulfide 2400 02/18/2015 105197250058-1226.1 2050
Carbon tetrachloride 2600 02/18/2015 1051105250058-1366.8 2050
Chlorobenzene 2500 02/18/2015 1051101250059-1292.6 2050
Chloroethane 2000 02/18/2015 105181250042-1634.3 2050
Chloroform 2600 02/18/2015 1051104250071-1253.0 2050
Chloromethane (Methyl chloride)2100 02/18/2015 105183250034-13411 2050
Cyclohexane 2400 02/18/2015 105196250053-1395.9 2050
1,2-Dibromo-3-chloropropane (DBCP)2500 02/18/2015 105199250055-1255.0 2050
Dibromochloromethane 2600 02/18/2015 1051102250066-1190.31 2050
1,2-Dibromoethane (EDB)2500 02/18/2015 1051102250074-1240.27 2050
1,4-Dichlorobenzene 2400 02/18/2015 105197250052-1332.1 2050
1,3-Dichlorobenzene 2500 02/18/2015 1051100250051-1342.0 2050
1,2-Dichlorobenzene 2500 02/18/2015 1051101250057-1311.7 2050
Dichlorodifluoromethane 1500 02/18/2015 105159250010-15713 2050
1,2-Dichloroethane 2600 02/18/2015 1051105250067-1291.8 2050
1,1-Dichloroethane 2600 02/18/2015 1051104250071-1274.9 2050
trans-1,2-Dichloroethene 2500 02/18/2015 1051102250068-1316.2 2050
cis-1,2-Dichloroethene 2600 02/18/2015 1051105250070-1223.7 2050
1,1-Dichloroethene 2500 02/18/2015 105199250069-1389.1 2050
1,2-Dichloropropane 2600 02/18/2015 1051105250072-1242.5 2050
trans-1,3-Dichloropropene 2600 02/18/2015 1051106250070-1240.46 2050
cis-1,3-Dichloropropene 2700 02/18/2015 1051107250070-1261.3 2050
2-Hexanone 5000 02/18/2015 1051100500054-1371.6 2050
Isopropylbenzene 2600 02/18/2015 1051106250050-1362.6 2050
Methyl acetate 2700 02/18/2015 1051107250059-1374.1 2050
Methyl tertiary butyl ether (MTBE)2600 02/18/2015 1051104250070-1301.6 2050
4-Methyl-2-pentanone 5000 02/18/2015 105199500060-1342.8 2050
Methylcyclohexane 2500 02/18/2015 1051100250041-1448.5 2050
Methylene chloride 2400 02/18/2015 105195250070-1302.1 2050
Styrene 2600 02/18/2015 1051103250054-1361.1 2050
1,1,2,2-Tetrachloroethane 2600 02/18/2015 1051104250069-1321.1 2050
Tetrachloroethene 2500 02/18/2015 1051101250045-1506.5 2050
1,1,2-Trichloro-1,2,2-Trifluoroethane 2500 02/18/2015 1051100250049-1366.8 2050
1,2,4-Trichlorobenzene 2400 02/18/2015 105197250034-1451.3 2050
1,1,2-Trichloroethane 2500 02/18/2015 1051100250055-1280.053 2050
1,1,1-Trichloroethane 2600 02/18/2015 1051105250063-1283.6 2050
Trichloroethene 2600 02/18/2015 1051104250062-1263.5 2050
Trichlorofluoromethane 2500 02/18/2015 105198250045-1388.6 2050
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 54 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:QQ68101-003
68101 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Vinyl chloride 2200 02/18/2015 105189250042-13211 2050
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 105 47-138
1,2-Dichloroethane-d4 90 53-142
Toluene-d8 96 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 55 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:QB12017-008MS
68101 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acetone 11000 02/18/2015 1345931100060-140ND100
Benzene 5000 02/18/2015 134587570069-123ND100
Bromodichloromethane 5500 02/18/2015 134596570069-121ND100
Bromoform 4800 02/18/2015 134584570061-119ND100
Bromomethane (Methyl bromide)4400 02/18/2015 134577570035-144ND100
2-Butanone (MEK)9300 02/18/2015 1345811100057-148ND100
Carbon disulfide 4900 02/18/2015 134586570058-122ND100
Carbon tetrachloride 5200 02/18/2015 134591570058-136ND100
Chlorobenzene 4800 02/18/2015 134584570059-129ND100
Chloroethane 4800 02/18/2015 134583570050-132ND100
Chloroform 5200 02/18/2015 134590570071-125ND100
Chloromethane (Methyl chloride)4700 02/18/2015 134581570034-134ND100
Cyclohexane 14000 02/18/2015 1345N247570053-139ND100
1,2-Dibromo-3-chloropropane (DBCP)9400 02/18/2015 1345N163570055-125ND100
Dibromochloromethane 4900 02/18/2015 134585570066-119ND100
1,2-Dibromoethane (EDB)5000 02/18/2015 134587570074-124ND100
1,2-Dichlorobenzene 4800 02/18/2015 134583570057-131ND100
1,3-Dichlorobenzene 4600 02/18/2015 134580570051-134ND100
1,4-Dichlorobenzene 4400 02/18/2015 134578570052-133ND100
Dichlorodifluoromethane 4300 02/18/2015 134575570010-157ND100
1,1-Dichloroethane 5100 02/18/2015 134589570071-127ND100
1,2-Dichloroethane 5000 02/18/2015 134587570067-129ND100
1,1-Dichloroethene 5200 02/18/2015 134590570069-138ND100
cis-1,2-Dichloroethene 5100 02/18/2015 134589570070-122ND100
trans-1,2-Dichloroethene 5000 02/18/2015 134588570068-131ND100
1,2-Dichloropropane 5300 02/18/2015 134592570072-124ND100
cis-1,3-Dichloropropene 5100 02/18/2015 134589570070-126ND100
trans-1,3-Dichloropropene 5000 02/18/2015 134587570070-124ND100
2-Hexanone 10000 02/18/2015 1345881100054-137ND100
Isopropylbenzene 11000 02/18/2015 134585570050-1365800100
Methyl acetate 5900 02/18/2015 1345103570059-137ND100
Methyl tertiary butyl ether (MTBE)5100 02/18/2015 134589570070-130ND100
4-Methyl-2-pentanone 9900 02/18/2015 1345871100060-134ND100
Methylcyclohexane 9500 02/18/2015 134578570041-1445000100
Methylene chloride 4700 02/18/2015 134582570077-129ND100
Styrene 6300 02/18/2015 1345109570054-136ND100
1,1,2,2-Tetrachloroethane 5400 02/18/2015 134595570069-132ND100
Tetrachloroethene 4800 02/18/2015 134584570070-130ND100
1,1,2-Trichloro-1,2,2-Trifluoroethane 5000 02/18/2015 134586570049-136ND100
1,2,4-Trichlorobenzene 4800 02/18/2015 134583570034-145ND100
1,1,1-Trichloroethane 5100 02/18/2015 134589570063-128ND100
1,1,2-Trichloroethane 5400 02/18/2015 134595570055-128ND100
Trichloroethene 5000 02/18/2015 134587570062-126ND100
Trichlorofluoromethane 4800 02/18/2015 134584570045-138ND100
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 56 of 66
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:QB12017-008MS
68101 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Vinyl chloride 5000 02/18/2015 134587570042-132ND100
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 82 53-142
Bromofluorobenzene 92 47-138
Toluene-d8 92 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 57 of 66
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Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Sample ID:QB12017-008MD
68101 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acetone 11000 02/18/2015 1406991100060-1406.1 20ND100
Benzene 5000 02/18/2015 140688570069-1230.41 20ND100
Bromodichloromethane 5500 02/18/2015 140696570069-1210.56 20ND100
Bromoform 5000 02/18/2015 140687570061-1194.0 20ND100
Bromomethane (Methyl bromide)4500 02/18/2015 140679570035-1442.7 20ND100
2-Butanone (MEK)11000 02/18/2015 1406+10011000 57-14821 20ND100
Carbon disulfide 4900 02/18/2015 140686570058-1220.40 20ND100
Carbon tetrachloride 5200 02/18/2015 140691570058-1360.14 20ND100
Chlorobenzene 4800 02/18/2015 140685570059-1291.0 20ND100
Chloroethane 4800 02/18/2015 140684570050-1320.96 20ND100
Chloroform 5300 02/18/2015 140693570071-1252.6 20ND100
Chloromethane (Methyl chloride)4700 02/18/2015 140682570034-1340.66 20ND100
Cyclohexane 4600 02/18/2015 1406+805700 53-139100 20ND100
1,2-Dibromo-3-chloropropane (DBCP)9200 02/18/2015 1406N161570055-1251.5 20ND100
Dibromochloromethane 5000 02/18/2015 140688570066-1192.7 20ND100
1,2-Dibromoethane (EDB)5200 02/18/2015 140690570074-1243.7 20ND100
1,2-Dichlorobenzene 4800 02/18/2015 140683570057-1310.065 20ND100
1,3-Dichlorobenzene 4400 02/18/2015 140678570051-1342.8 20ND100
1,4-Dichlorobenzene 4300 02/18/2015 140675570052-1333.4 20ND100
Dichlorodifluoromethane 4300 02/18/2015 140676570010-1570.34 20ND100
1,1-Dichloroethane 5200 02/18/2015 140691570071-1272.9 20ND100
1,2-Dichloroethane 5200 02/18/2015 140691570067-1294.9 20ND100
1,1-Dichloroethene 5200 02/18/2015 140691570069-1380.74 20ND100
cis-1,2-Dichloroethene 5200 02/18/2015 140691570070-1222.0 20ND100
trans-1,2-Dichloroethene 5100 02/18/2015 140690570068-1311.8 20ND100
1,2-Dichloropropane 5400 02/18/2015 140694570072-1242.7 20ND100
cis-1,3-Dichloropropene 5200 02/18/2015 140690570070-1261.2 20ND100
trans-1,3-Dichloropropene 5200 02/18/2015 140690570070-1243.3 20ND100
2-Hexanone 11000 02/18/2015 1406931100054-1375.2 20ND100
Isopropylbenzene 9800 02/18/2015 140671570050-1367.9 205800100
Methyl acetate 5900 02/18/2015 1406104570059-1370.76 20ND100
Methyl tertiary butyl ether (MTBE)5300 02/18/2015 140693570070-1304.5 20ND100
4-Methyl-2-pentanone 11000 02/18/2015 1406981100060-13412 20ND100
Methylcyclohexane 8900 02/18/2015 140667570041-1447.3 205000100
Methylene chloride 4900 02/18/2015 140685570077-1294.3 20ND100
Styrene 6100 02/18/2015 1406106570054-1362.9 20ND100
1,1,2,2-Tetrachloroethane 5500 02/18/2015 140697570069-1322.1 20ND100
Tetrachloroethene 4600 02/18/2015 140680570070-1305.0 20ND100
1,1,2-Trichloro-1,2,2-Trifluoroethane 5000 02/18/2015 140688570049-1361.3 20ND100
1,2,4-Trichlorobenzene 4700 02/18/2015 140681570034-1451.8 20ND100
1,1,1-Trichloroethane 5200 02/18/2015 140691570063-1282.2 20ND100
1,1,2-Trichloroethane 5600 02/18/2015 140697570055-1282.1 20ND100
Trichloroethene 4900 02/18/2015 140686570062-1260.56 20ND100
Trichlorofluoromethane 5000 02/18/2015 140687570045-1383.2 20ND100
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 58 of 66
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Sample ID:QB12017-008MD
68101 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Vinyl chloride 5000 02/18/2015 140687570042-1320.40 20ND100
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 78 53-142
Bromofluorobenzene 84 47-138
Toluene-d8 85 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 59 of 66
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Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ68116-001
68116 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Ethylbenzene ND 02/18/2015 115425081ug/kg50
Toluene ND 02/18/2015 115425085ug/kg50
Xylenes (total)ND 02/18/2015 1154250150ug/kg50
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 114 47-138
1,2-Dichloroethane-d4 102 53-142
Toluene-d8 104 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 60 of 66
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Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ68116-002
68116 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Ethylbenzene 2700 02/18/2015 1031106250059-12850
Toluene 2600 02/18/2015 1031105250061-12950
Xylenes (total)5200 02/18/2015 1031105500058-12850
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 96 47-138
1,2-Dichloroethane-d4 82 53-142
Toluene-d8 88 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 61 of 66
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Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:QQ68116-003
68116 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Ethylbenzene 2600 02/18/2015 1051103250059-1283.5 2050
Toluene 2600 02/18/2015 1051104250061-1290.65 2050
Xylenes (total)5000 02/18/2015 1051101500058-1283.5 2050
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 105 47-138
1,2-Dichloroethane-d4 90 53-142
Toluene-d8 96 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 62 of 66
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Level 1 Report v2.1
TPH - DRO - MB
Batch:Prep Method:
Prep Date:
Sample ID:QQ67845-001
67845 3550C
02/14/2015 1210Analytical Method:8015C
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
TPH-DRO 2700 02/16/2015 2214J67001200ug/kg1
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 85 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 63 of 66
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Level 1 Report v2.1
TPH - DRO - LCS
Batch:Prep Method:
Prep Date:
Sample ID:QQ67845-002
67845 3550C
02/14/2015 1210Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
TPH-DRO 71000 02/16/2015 2234858300070-1301
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 82 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 64 of 66
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Level 1 Report v2.1
TPH - DRO - MS
Batch:Prep Method:
Prep Date:
Sample ID:QB12017-004MS
67845 3550C
02/14/2015 1210Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
TPH-DRO 96000 02/17/2015 00197010000070-130240001
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 80 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 65 of 66
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Level 1 Report v2.1
TPH - DRO - MSD
Batch:Prep Method:
Prep Date:
Sample ID:QB12017-004MD
67845 3550C
02/14/2015 1210Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
TPH-DRO 950000 02/17/2015 0039+921000000 70-130160 20240001
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 79 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 66 of 66
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Terracon Consultants, Inc.
2401 Brentwood Road
Suite 107 I
Raleigh, NC 27604
Attention: Justin.Fabriziani
QB12016Lot Number:
70152304Project Number:
Proposed Durham PDHQProject Name:
02/19/2015Date Completed:
Nisreen Saikaly
Project Manager
*QB12016*

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 79
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Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Terracon Consultants, Inc.
Lot Number: QB12016
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
DRO
All DRO sample patterns resemble an oil pattern except sample -007 (SB-23(2'-4')). Sample -007 resembles fuel oil pattern.
The DRO pattern in the MB does not resemble the pattern in any of the sample samples.
Page: 2 of 79
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Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terracon Consultants, Inc.
Lot Number: QB12016

Sample Number Sample ID Matrix Date Sampled Date Received
001 02/11/2015 0902SB-45(4'-6')Solid 02/12/2015
002 02/11/2015 0905SB-46(2'-4')Solid 02/12/2015
003 02/11/2015 0950SB-19(4'-6')Solid 02/12/2015
004 02/11/2015 1011SB-20(2'-4')Solid 02/12/2015
005 02/11/2015 1049SB-21(6'-8')Solid 02/12/2015
006 02/11/2015 1055SB-22(2'-4')Solid 02/12/2015
007 02/11/2015 1124SB-23(2'-4')Solid 02/12/2015
008 02/11/2015 1145SB-24(6'-8')Solid 02/12/2015
009 02/11/2015 1200SB-25(0'-2')Solid 02/12/2015
010 02/11/2015 1330SB-15(10'-12')Solid 02/12/2015
011 02/11/2015 1345SB-16(8'-10')Solid 02/12/2015
012 02/11/2015 1515SB-32(8'-10')Solid 02/12/2015
013 02/11/2015 1538SB-33(8'-10')Solid 02/12/2015
014 02/11/2015 1600SB-30(5'-10')Solid 02/12/2015
015 02/11/2015 1611SB-26(6'-8')Solid 02/12/2015
016 02/11/2015 1615SB-28(6'-8')Solid 02/12/2015
017 02/11/2015 1629SB-31(0'-5')Solid 02/12/2015
018 02/11/2015 1637SB-27(8'-10')Solid 02/12/2015
019 02/11/2015 1652SB-29(6'-8')Solid 02/12/2015
020 02/11/2015TRIP BLANK Aqueous 02/12/2015
021 02/11/2015TRIP BLANK(SH3001)Aqueous 02/12/2015
(21 samples)
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Terracon Consultants, Inc.
Lot Number: QB12016

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SB-45(4'-6')Solid Acetone 8260B 10 J ug/kg 6
001 SB-45(4'-6')Solid Toluene 8260B 2.1 J ug/kg 6
001 SB-45(4'-6')Solid Xylenes (total)8260B 4.2 J ug/kg 7
001 SB-45(4'-6')Solid TPH-DRO 8015C 12000 B ug/kg 8
002 SB-46(2'-4')Solid Acetone 8260B 11 J ug/kg 9
002 SB-46(2'-4')Solid 1,2-Dichlorobenzene 8260B 3.3 J ug/kg 9
002 SB-46(2'-4')Solid Methylcyclohexane 8260B 0.67 J ug/kg 9
002 SB-46(2'-4')Solid Xylenes (total)8260B 7.2 ug/kg 10
002 SB-46(2'-4')Solid TPH-DRO 8015C 12000 B ug/kg 11
003 SB-19(4'-6')Solid TPH-DRO 8015C 9500000 B ug/kg 12
004 SB-20(2'-4')Solid Acetone 8260B 51 ug/kg 13
004 SB-20(2'-4')Solid 2-Butanone (MEK)8260B 9.5 J ug/kg 13
004 SB-20(2'-4')Solid Chlorobenzene 8260B 2.8 J ug/kg 13
004 SB-20(2'-4')Solid Methyl acetate 8260B 4.2 J ug/kg 13
004 SB-20(2'-4')Solid Methyl tertiary butyl ether (MTBE)8260B 1.4 J ug/kg 13
004 SB-20(2'-4')Solid TPH-DRO 8015C 22000 B ug/kg 15
005 SB-21(6'-8')Solid TPH-DRO 8015C 1000000 B ug/kg 16
006 SB-22(2'-4')Solid TPH-DRO 8015C 50000000 B ug/kg 17
007 SB-23(2'-4')Solid Acetone 8260B 120 B ug/kg 18
007 SB-23(2'-4')Solid Benzene 8260B 3.2 J ug/kg 18
007 SB-23(2'-4')Solid Chlorobenzene 8260B 9.0 ug/kg 18
007 SB-23(2'-4')Solid Chloroform 8260B 9.8 ug/kg 18
007 SB-23(2'-4')Solid 1,2-Dichlorobenzene 8260B 11 ug/kg 18
007 SB-23(2'-4')Solid 1,4-Dichlorobenzene 8260B 3.1 J ug/kg 18
007 SB-23(2'-4')Solid Isopropylbenzene 8260B 11 ug/kg 18
007 SB-23(2'-4')Solid Methyl tertiary butyl ether (MTBE)8260B 0.85 J ug/kg 18
007 SB-23(2'-4')Solid Methylcyclohexane 8260B 110 ug/kg 18
007 SB-23(2'-4')Solid Xylenes (total)8260B 3.6 J ug/kg 19
007 SB-23(2'-4')Solid TPH-DRO 8015C 5700000 B ug/kg 20
008 SB-24(6'-8')Solid TPH-DRO 8015C 2700000 B ug/kg 21
009 SB-25(0'-2')Solid Acetone 8260B 8.3 J ug/kg 22
009 SB-25(0'-2')Solid TPH-DRO 8015C 34000 B ug/kg 24
010 SB-15(10'-12')Solid HEM (oil and grease)9071B 510 mg/kg 25
010 SB-15(10'-12')Solid Methyl tertiary butyl ether (MTBE)8260B 0.55 J ug/kg 26
010 SB-15(10'-12')Solid TPH-DRO 8015C 73000 B ug/kg 28
011 SB-16(8'-10')Solid HEM (oil and grease)9071B 470 mg/kg 29
011 SB-16(8'-10')Solid Acetone 8260B 25 B ug/kg 30
011 SB-16(8'-10')Solid 1,2-Dichlorobenzene 8260B 3.2 J ug/kg 30
011 SB-16(8'-10')Solid 1,4-Dichlorobenzene 8260B 2.3 J ug/kg 30
011 SB-16(8'-10')Solid Ethylbenzene 8260B 6.5 ug/kg 30
011 SB-16(8'-10')Solid Isopropylbenzene 8260B 2.9 J ug/kg 30
011 SB-16(8'-10')Solid Methylcyclohexane 8260B 10 ug/kg 30
011 SB-16(8'-10')Solid Tetrachloroethene 8260B 9.1 ug/kg 30
011 SB-16(8'-10')Solid TPH-DRO 8015C 300000 B ug/kg 32
012 SB-32(8'-10')Solid Tetrachloroethene 8260B 1.0 J ug/kg 34
Page: 4 of 79
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Executive Summary (Continued)
Lot Number: QB12016
Sample Sample ID Matrix Parameter Method Result Q Units Page
012 SB-32(8'-10')Solid TPH-DRO 8015C 110000 B ug/kg 36
013 SB-33(8'-10')Solid Acetone 8260B 13 BJ ug/kg 38
013 SB-33(8'-10')Solid Methyl tertiary butyl ether (MTBE)8260B 2.8 J ug/kg 38
013 SB-33(8'-10')Solid TPH-DRO 8015C 70000 B ug/kg 40
014 SB-30(5'-10')Solid TPH-DRO 8015C 1200000 B ug/kg 41
015 SB-26(6'-8')Solid Acetone 8260B 7.5 J ug/kg 43
015 SB-26(6'-8')Solid Isopropylbenzene 8260B 5.2 ug/kg 43
015 SB-26(6'-8')Solid Methylcyclohexane 8260B 23 ug/kg 43
015 SB-26(6'-8')Solid TPH-DRO 8015C 360000 B ug/kg 45
016 SB-28(6'-8')Solid TPH-DRO 8015C 420000 B ug/kg 46
017 SB-31(0'-5')Solid TPH-DRO 8015C 1700000 B ug/kg 47
018 SB-27(8'-10')Solid TPH-DRO 8015C 31000 B ug/kg 51
019 SB-29(6'-8')Solid TPH-DRO 8015C 220000 B ug/kg 52
(58 detections)
Page: 5 of 79
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-45(4'-6')
QB12016-001
02/11/2015 0902
02/12/2015
Solid
% Solids:73.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1732 DCS 67778 6.06
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 J 1ug/kg7.623
Benzene 71-43-2 8260B ND 1ug/kg1.25.6
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.95.6
Bromoform 75-25-2 8260B ND 1ug/kg0.795.6
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.05.6
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg2.711
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.55.6
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.05.6
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.95.6
Chloroethane 75-00-3 8260B ND 1ug/kg1.55.6
Chloroform 67-66-3 8260B ND 1ug/kg0.945.6
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.15.6
Cyclohexane 110-82-7 8260B ND 1ug/kg0.765.6
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.75.6
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.95.6
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.965.6
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.95.6
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.95.6
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.95.6
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.85.6
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.825.6
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.15.6
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.95.6
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.865.6
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.75.6
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.05.6
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.775.6
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.935.6
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.95.6
2-Hexanone 591-78-6 8260B ND 1ug/kg1.511
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.265.6
Methyl acetate 79-20-9 8260B ND 1ug/kg1.15.6
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.455.6
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.711
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.465.6
Methylene chloride 75-09-2 8260B ND 1ug/kg2.95.6
Styrene 100-42-5 8260B ND 1ug/kg1.25.6
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.535.6
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.565.6
Toluene 108-88-3 8260B 2.1 J 1ug/kg1.95.6
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.715.6
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.95.6
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.965.6
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.895.6
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-45(4'-6')
QB12016-001
02/11/2015 0902
02/12/2015
Solid
% Solids:73.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1732 DCS 67778 6.06
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.6
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.75.6
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.975.6
Xylenes (total)1330-20-7 8260B 4.2 J 1ug/kg3.35.6
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 53-142
Bromofluorobenzene 103 47-138
Toluene-d8 105 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-45(4'-6')
QB12016-001
02/11/2015 0902
02/12/2015
Solid
% Solids:73.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 1351 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 12000 B 1ug/kg17009200
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 63 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-46(2'-4')
QB12016-002
02/11/2015 0905
02/12/2015
Solid
% Solids:73.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1753 DCS 67778 6.00
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 11 J 1ug/kg7.623
Benzene 71-43-2 8260B ND 1ug/kg1.25.6
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.95.6
Bromoform 75-25-2 8260B ND 1ug/kg0.795.6
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.05.6
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg2.711
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.55.6
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.05.6
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.95.6
Chloroethane 75-00-3 8260B ND 1ug/kg1.55.6
Chloroform 67-66-3 8260B ND 1ug/kg0.945.6
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.15.6
Cyclohexane 110-82-7 8260B ND 1ug/kg0.765.6
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.75.6
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.95.6
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.965.6
1,2-Dichlorobenzene 95-50-1 8260B 3.3 J 1ug/kg1.95.6
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.95.6
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.95.6
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.85.6
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.825.6
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.15.6
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.95.6
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.865.6
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.75.6
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.05.6
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.775.6
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.935.6
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.95.6
2-Hexanone 591-78-6 8260B ND 1ug/kg1.511
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.265.6
Methyl acetate 79-20-9 8260B ND 1ug/kg1.15.6
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.455.6
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.711
Methylcyclohexane 108-87-2 8260B 0.67 J 1ug/kg0.465.6
Methylene chloride 75-09-2 8260B ND 1ug/kg2.95.6
Styrene 100-42-5 8260B ND 1ug/kg1.25.6
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.535.6
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.565.6
Toluene 108-88-3 8260B ND 1ug/kg1.95.6
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.715.6
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.95.6
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.965.6
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.895.6
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-46(2'-4')
QB12016-002
02/11/2015 0905
02/12/2015
Solid
% Solids:73.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1753 DCS 67778 6.00
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.6
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.75.6
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.975.6
Xylenes (total)1330-20-7 8260B 7.2 1ug/kg3.35.6
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 53-142
Bromofluorobenzene 104 47-138
Toluene-d8 103 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-46(2'-4')
QB12016-002
02/11/2015 0905
02/12/2015
Solid
% Solids:73.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 1433 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 12000 B 1ug/kg17009100
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 65 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-19(4'-6')
QB12016-003
02/11/2015 0950
02/12/2015
Solid
% Solids:84.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 10 02/17/2015 0551 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 9500000 B 1ug/kg1400078000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 110 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-20(2'-4')
QB12016-004
02/11/2015 1011
02/12/2015
Solid
% Solids:74.4 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1814 DCS 67778 6.21
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 51 1ug/kg7.222
Benzene 71-43-2 8260B ND 1ug/kg1.25.4
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.85.4
Bromoform 75-25-2 8260B ND 1ug/kg0.765.4
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg1.95.4
2-Butanone (MEK)78-93-3 8260B 9.5 J 1ug/kg2.611
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.45.4
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.95.4
Chlorobenzene 108-90-7 8260B 2.8 J 1ug/kg1.85.4
Chloroethane 75-00-3 8260B ND 1ug/kg1.45.4
Chloroform 67-66-3 8260B ND 1ug/kg0.905.4
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.15.4
Cyclohexane 110-82-7 8260B ND 1ug/kg0.735.4
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.65.4
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.85.4
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.925.4
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.85.4
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.85.4
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.85.4
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.75.4
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.795.4
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.15.4
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.85.4
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.825.4
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.65.4
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg0.985.4
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.745.4
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.895.4
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.85.4
2-Hexanone 591-78-6 8260B ND 1ug/kg1.411
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.255.4
Methyl acetate 79-20-9 8260B 4.2 J 1ug/kg1.15.4
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 1.4 J 1ug/kg0.435.4
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.611
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.445.4
Methylene chloride 75-09-2 8260B ND 1ug/kg2.85.4
Styrene 100-42-5 8260B ND 1ug/kg1.25.4
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.515.4
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.545.4
Toluene 108-88-3 8260B ND 1ug/kg1.85.4
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.685.4
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.85.4
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.925.4
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.855.4
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-20(2'-4')
QB12016-004
02/11/2015 1011
02/12/2015
Solid
% Solids:74.4 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1814 DCS 67778 6.21
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.4
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.65.4
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.935.4
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.15.4
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 97 53-142
Bromofluorobenzene 101 47-138
Toluene-d8 106 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-20(2'-4')
QB12016-004
02/11/2015 1011
02/12/2015
Solid
% Solids:74.4 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 1557 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 22000 B 1ug/kg16008900
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 75 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-21(6'-8')
QB12016-005
02/11/2015 1049
02/12/2015
Solid
% Solids:77.5 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 1618 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 1000000 B 1ug/kg16008600
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 82 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-22(2'-4')
QB12016-006
02/11/2015 1055
02/12/2015
Solid
% Solids:94.3 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 50 02/17/2015 0953 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 50000000 B 1ug/kg65000360000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl N 37 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 17 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-23(2'-4')
QB12016-007
02/11/2015 1124
02/12/2015
Solid
% Solids:75.7 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 1 02/16/2015 1907 DCS 67933 6.23
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 120 B 2ug/kg5.421
Benzene 71-43-2 8260B 3.2 J 2ug/kg1.65.3
Bromodichloromethane 75-27-4 8260B ND 2ug/kg1.85.3
Bromoform 75-25-2 8260B ND 2ug/kg2.15.3
Bromomethane (Methyl bromide)74-83-9 8260B ND 2ug/kg2.35.3
2-Butanone (MEK)78-93-3 8260B ND 2ug/kg4.511
Carbon disulfide 75-15-0 8260B ND 2ug/kg1.45.3
Carbon tetrachloride 56-23-5 8260B ND 2ug/kg1.55.3
Chlorobenzene 108-90-7 8260B 9.0 2ug/kg1.75.3
Chloroethane 75-00-3 8260B ND 2ug/kg2.55.3
Chloroform 67-66-3 8260B 9.8 2ug/kg1.65.3
Chloromethane (Methyl chloride)74-87-3 8260B ND 2ug/kg2.15.3
Cyclohexane 110-82-7 8260B ND 2ug/kg1.85.3
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 2ug/kg2.25.3
Dibromochloromethane 124-48-1 8260B ND 2ug/kg1.85.3
1,2-Dibromoethane (EDB)106-93-4 8260B ND 2ug/kg1.85.3
1,2-Dichlorobenzene 95-50-1 8260B 11 2ug/kg1.85.3
1,3-Dichlorobenzene 541-73-1 8260B ND 2ug/kg1.85.3
1,4-Dichlorobenzene 106-46-7 8260B 3.1 J 2ug/kg1.65.3
Dichlorodifluoromethane 75-71-8 8260B ND 2ug/kg4.05.3
1,1-Dichloroethane 75-34-3 8260B ND 2ug/kg1.65.3
1,2-Dichloroethane 107-06-2 8260B ND 2ug/kg1.75.3
1,1-Dichloroethene 75-35-4 8260B ND 2ug/kg1.95.3
cis-1,2-Dichloroethene 156-59-2 8260B ND 2ug/kg1.75.3
trans-1,2-Dichloroethene 156-60-5 8260B ND 2ug/kg1.65.3
1,2-Dichloropropane 78-87-5 8260B ND 2ug/kg1.65.3
cis-1,3-Dichloropropene 10061-01-5 8260B ND 2ug/kg1.65.3
trans-1,3-Dichloropropene 10061-02-6 8260B ND 2ug/kg1.65.3
Ethylbenzene 100-41-4 8260B ND 2ug/kg1.75.3
2-Hexanone 591-78-6 8260B ND 2ug/kg4.011
Isopropylbenzene 98-82-8 8260B 11 2ug/kg1.65.3
Methyl acetate 79-20-9 8260B ND 2ug/kg1.05.3
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 0.85 J 2ug/kg0.425.3
4-Methyl-2-pentanone 108-10-1 8260B ND 2ug/kg1.611
Methylcyclohexane 108-87-2 8260B 110 2ug/kg0.435.3
Methylene chloride 75-09-2 8260B ND 2ug/kg2.85.3
Styrene 100-42-5 8260B ND 2ug/kg1.25.3
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 2ug/kg0.505.3
Tetrachloroethene 127-18-4 8260B ND 2ug/kg0.535.3
Toluene 108-88-3 8260B ND 2ug/kg1.85.3
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 2ug/kg0.675.3
1,2,4-Trichlorobenzene 120-82-1 8260B ND 2ug/kg1.85.3
1,1,1-Trichloroethane 71-55-6 8260B ND 2ug/kg0.905.3
1,1,2-Trichloroethane 79-00-5 8260B ND 2ug/kg0.845.3
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 18 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-23(2'-4')
QB12016-007
02/11/2015 1124
02/12/2015
Solid
% Solids:75.7 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 1 02/16/2015 1907 DCS 67933 6.23
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 2ug/kg2.05.3
Trichlorofluoromethane 75-69-4 8260B ND 2ug/kg1.65.3
Vinyl chloride 75-01-4 8260B ND 2ug/kg0.915.3
Xylenes (total)1330-20-7 8260B 3.6 J 2ug/kg3.15.3
AcceptanceRun 2
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 96 53-142
Bromofluorobenzene 95 47-138
Toluene-d8 103 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 19 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-23(2'-4')
QB12016-007
02/11/2015 1124
02/12/2015
Solid
% Solids:75.7 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 5 02/17/2015 1014 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 5700000 B 1ug/kg810044000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 74 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 20 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-24(6'-8')
QB12016-008
02/11/2015 1145
02/12/2015
Solid
% Solids:80.5 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 5 02/17/2015 1035 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 2700000 B 1ug/kg740040000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 84 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 21 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-25(0'-2')
QB12016-009
02/11/2015 1200
02/12/2015
Solid
% Solids:75.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/17/2015 1717 DCS 68027 6.05
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 8.3 J 1ug/kg5.622
Benzene 71-43-2 8260B ND 1ug/kg1.75.5
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.85.5
Bromoform 75-25-2 8260B ND 1ug/kg2.25.5
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.45.5
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.711
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.55.5
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.65.5
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.85.5
Chloroethane 75-00-3 8260B ND 1ug/kg2.65.5
Chloroform 67-66-3 8260B ND 1ug/kg1.75.5
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.25.5
Cyclohexane 110-82-7 8260B ND 1ug/kg1.95.5
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.35.5
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.95.5
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg1.95.5
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.95.5
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.85.5
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.75.5
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.15.5
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg1.65.5
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.85.5
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.05.5
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg1.75.5
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.75.5
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.65.5
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg1.65.5
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg1.75.5
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.85.5
2-Hexanone 591-78-6 8260B ND 1ug/kg4.111
Isopropylbenzene 98-82-8 8260B ND 1ug/kg1.75.5
Methyl acetate 79-20-9 8260B ND 1ug/kg2.05.5
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg1.75.5
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.011
Methylcyclohexane 108-87-2 8260B ND 1ug/kg1.85.5
Methylene chloride 75-09-2 8260B ND 1ug/kg1.45.5
Styrene 100-42-5 8260B ND 1ug/kg1.95.5
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.525.5
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.555.5
Toluene 108-88-3 8260B ND 1ug/kg1.95.5
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.695.5
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.95.5
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.945.5
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.05.5
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 22 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-25(0'-2')
QB12016-009
02/11/2015 1200
02/12/2015
Solid
% Solids:75.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/17/2015 1717 DCS 68027 6.05
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.5
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.75.5
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.955.5
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.25.5
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 89 53-142
Bromofluorobenzene 93 47-138
Toluene-d8 93 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 23 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-25(0'-2')
QB12016-009
02/11/2015 1200
02/12/2015
Solid
% Solids:75.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 1742 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 34000 B 1ug/kg16008900
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 79 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 24 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-15(10'-12')
QB12016-010
02/11/2015 1330
02/12/2015
Solid
% Solids:78.0 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B 510 1mg/kg210260
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 25 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-15(10'-12')
QB12016-010
02/11/2015 1330
02/12/2015
Solid
% Solids:78.0 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1558 DCS 67933 5.42
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg6.024
Benzene 71-43-2 8260B ND 1ug/kg1.85.9
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.05.9
Bromoform 75-25-2 8260B ND 1ug/kg2.35.9
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.65.9
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg5.012
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.65.9
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.75.9
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.95.9
Chloroethane 75-00-3 8260B ND 1ug/kg2.85.9
Chloroform 67-66-3 8260B ND 1ug/kg1.85.9
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.45.9
Cyclohexane 110-82-7 8260B ND 1ug/kg2.05.9
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.55.9
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.05.9
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.05.9
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.05.9
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.05.9
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.85.9
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.45.9
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg1.75.9
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.95.9
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.15.9
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg1.95.9
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.85.9
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.85.9
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg1.85.9
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg1.85.9
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.95.9
2-Hexanone 591-78-6 8260B ND 1ug/kg4.412
Isopropylbenzene 98-82-8 8260B ND 1ug/kg1.85.9
Methyl acetate 79-20-9 8260B ND 1ug/kg1.25.9
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 0.55 J 1ug/kg0.475.9
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.812
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.495.9
Methylene chloride 75-09-2 8260B ND 1ug/kg3.15.9
Styrene 100-42-5 8260B ND 1ug/kg1.35.9
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.565.9
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.595.9
Toluene 108-88-3 8260B ND 1ug/kg2.05.9
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.755.9
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.05.9
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg1.05.9
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.935.9
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 26 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-15(10'-12')
QB12016-010
02/11/2015 1330
02/12/2015
Solid
% Solids:78.0 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1558 DCS 67933 5.42
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.25.9
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.85.9
Vinyl chloride 75-01-4 8260B ND 1ug/kg1.05.9
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.45.9
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 94 53-142
Bromofluorobenzene 92 47-138
Toluene-d8 95 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 27 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-15(10'-12')
QB12016-010
02/11/2015 1330
02/12/2015
Solid
% Solids:78.0 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 1803 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 73000 B 1ug/kg16008600
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 80 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 28 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-16(8'-10')
QB12016-011
02/11/2015 1345
02/12/2015
Solid
% Solids:74.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B 470 1mg/kg230270
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 29 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-16(8'-10')
QB12016-011
02/11/2015 1345
02/12/2015
Solid
% Solids:74.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1619 DCS 67933 5.99
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 25 B 1ug/kg5.723
Benzene 71-43-2 8260B ND 1ug/kg1.75.6
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.95.6
Bromoform 75-25-2 8260B ND 1ug/kg2.25.6
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.45.6
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.811
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.55.6
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.65.6
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.85.6
Chloroethane 75-00-3 8260B ND 1ug/kg2.75.6
Chloroform 67-66-3 8260B ND 1ug/kg1.75.6
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.35.6
Cyclohexane 110-82-7 8260B ND 1ug/kg1.95.6
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.35.6
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.95.6
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg1.95.6
1,2-Dichlorobenzene 95-50-1 8260B 3.2 J 1ug/kg1.95.6
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.95.6
1,4-Dichlorobenzene 106-46-7 8260B 2.3 J 1ug/kg1.75.6
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.25.6
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg1.75.6
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.85.6
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.05.6
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg1.85.6
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.75.6
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.75.6
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg1.75.6
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg1.75.6
Ethylbenzene 100-41-4 8260B 6.5 1ug/kg1.85.6
2-Hexanone 591-78-6 8260B ND 1ug/kg4.211
Isopropylbenzene 98-82-8 8260B 2.9 J 1ug/kg1.75.6
Methyl acetate 79-20-9 8260B ND 1ug/kg1.15.6
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.455.6
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.711
Methylcyclohexane 108-87-2 8260B 10 1ug/kg0.465.6
Methylene chloride 75-09-2 8260B ND 1ug/kg2.95.6
Styrene 100-42-5 8260B ND 1ug/kg1.25.6
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.535.6
Tetrachloroethene 127-18-4 8260B 9.1 1ug/kg0.565.6
Toluene 108-88-3 8260B ND 1ug/kg1.95.6
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.715.6
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.95.6
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.965.6
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.895.6
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 30 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-16(8'-10')
QB12016-011
02/11/2015 1345
02/12/2015
Solid
% Solids:74.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1619 DCS 67933 5.99
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.6
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.75.6
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.975.6
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.35.6
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 95 53-142
Bromofluorobenzene 93 47-138
Toluene-d8 97 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 31 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-16(8'-10')
QB12016-011
02/11/2015 1345
02/12/2015
Solid
% Solids:74.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 1824 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 300000 B 1ug/kg16009000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 80 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 32 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-32(8'-10')
QB12016-012
02/11/2015 1515
02/12/2015
Solid
% Solids:84.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg200240
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 33 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-32(8'-10')
QB12016-012
02/11/2015 1515
02/12/2015
Solid
% Solids:84.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1640 DCS 67933 6.46
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg4.718
Benzene 71-43-2 8260B ND 1ug/kg1.44.6
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.54.6
Bromoform 75-25-2 8260B ND 1ug/kg1.84.6
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.04.6
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg3.99.2
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.24.6
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.34.6
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.54.6
Chloroethane 75-00-3 8260B ND 1ug/kg2.24.6
Chloroform 67-66-3 8260B ND 1ug/kg1.44.6
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.84.6
Cyclohexane 110-82-7 8260B ND 1ug/kg1.64.6
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.94.6
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.64.6
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg1.64.6
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.64.6
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.54.6
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.44.6
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg3.44.6
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg1.44.6
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.54.6
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.74.6
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg1.54.6
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.44.6
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.44.6
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg1.44.6
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg1.44.6
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.54.6
2-Hexanone 591-78-6 8260B ND 1ug/kg3.59.2
Isopropylbenzene 98-82-8 8260B ND 1ug/kg1.44.6
Methyl acetate 79-20-9 8260B ND 1ug/kg0.904.6
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.374.6
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.49.2
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.384.6
Methylene chloride 75-09-2 8260B ND 1ug/kg2.44.6
Styrene 100-42-5 8260B ND 1ug/kg1.04.6
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.434.6
Tetrachloroethene 127-18-4 8260B 1.0 J 1ug/kg0.464.6
Toluene 108-88-3 8260B ND 1ug/kg1.64.6
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.584.6
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.64.6
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.784.6
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.734.6
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 34 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-32(8'-10')
QB12016-012
02/11/2015 1515
02/12/2015
Solid
% Solids:84.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1640 DCS 67933 6.46
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg1.74.6
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.44.6
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.794.6
Xylenes (total)1330-20-7 8260B ND 1ug/kg2.74.6
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 53-142
Bromofluorobenzene 94 47-138
Toluene-d8 96 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 35 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-32(8'-10')
QB12016-012
02/11/2015 1515
02/12/2015
Solid
% Solids:84.1 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 1845 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 110000 B 1ug/kg14007900
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 79 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 36 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-33(8'-10')
QB12016-013
02/11/2015 1538
02/12/2015
Solid
% Solids:77.2 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg220260
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 37 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-33(8'-10')
QB12016-013
02/11/2015 1538
02/12/2015
Solid
% Solids:77.2 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1701 DCS 67933 6.66
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 13 BJ 1ug/kg4.919
Benzene 71-43-2 8260B ND 1ug/kg1.54.9
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.64.9
Bromoform 75-25-2 8260B ND 1ug/kg1.94.9
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.14.9
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.19.7
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.34.9
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.44.9
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.64.9
Chloroethane 75-00-3 8260B ND 1ug/kg2.34.9
Chloroform 67-66-3 8260B ND 1ug/kg1.54.9
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.94.9
Cyclohexane 110-82-7 8260B ND 1ug/kg1.74.9
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.04.9
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.74.9
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg1.74.9
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.74.9
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.64.9
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.54.9
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg3.64.9
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg1.44.9
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.64.9
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.84.9
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg1.54.9
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.54.9
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.44.9
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg1.44.9
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg1.54.9
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.64.9
2-Hexanone 591-78-6 8260B ND 1ug/kg3.79.7
Isopropylbenzene 98-82-8 8260B ND 1ug/kg1.54.9
Methyl acetate 79-20-9 8260B ND 1ug/kg0.954.9
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 2.8 J 1ug/kg0.394.9
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.59.7
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.404.9
Methylene chloride 75-09-2 8260B ND 1ug/kg2.54.9
Styrene 100-42-5 8260B ND 1ug/kg1.14.9
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.464.9
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.494.9
Toluene 108-88-3 8260B ND 1ug/kg1.74.9
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.614.9
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.74.9
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.834.9
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.774.9
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 38 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-33(8'-10')
QB12016-013
02/11/2015 1538
02/12/2015
Solid
% Solids:77.2 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1701 DCS 67933 6.66
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg1.84.9
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.54.9
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.844.9
Xylenes (total)1330-20-7 8260B ND 1ug/kg2.84.9
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 97 53-142
Bromofluorobenzene 92 47-138
Toluene-d8 95 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 39 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-33(8'-10')
QB12016-013
02/11/2015 1538
02/12/2015
Solid
% Solids:77.2 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 1906 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 70000 B 1ug/kg16008500
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 80 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 40 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-30(5'-10')
QB12016-014
02/11/2015 1600
02/12/2015
Solid
% Solids:84.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 1926 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 1200000 B 1ug/kg14007700
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 82 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 41 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-26(6'-8')
QB12016-015
02/11/2015 1611
02/12/2015
Solid
% Solids:85.9 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg190230
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 42 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-26(6'-8')
QB12016-015
02/11/2015 1611
02/12/2015
Solid
% Solids:85.9 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1259 DCS 67778 5.63
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 7.5 J 1ug/kg6.921
Benzene 71-43-2 8260B ND 1ug/kg1.15.2
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.85.2
Bromoform 75-25-2 8260B ND 1ug/kg0.725.2
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg1.95.2
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg2.510
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.35.2
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.95.2
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.85.2
Chloroethane 75-00-3 8260B ND 1ug/kg1.35.2
Chloroform 67-66-3 8260B ND 1ug/kg0.865.2
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.05.2
Cyclohexane 110-82-7 8260B ND 1ug/kg0.705.2
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.65.2
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.85.2
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.885.2
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.85.2
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.85.2
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.85.2
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.75.2
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.765.2
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.05.2
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.85.2
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.795.2
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.65.2
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg0.945.2
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.705.2
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.855.2
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.85.2
2-Hexanone 591-78-6 8260B ND 1ug/kg1.310
Isopropylbenzene 98-82-8 8260B 5.2 1ug/kg0.245.2
Methyl acetate 79-20-9 8260B ND 1ug/kg1.05.2
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.415.2
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.610
Methylcyclohexane 108-87-2 8260B 23 1ug/kg0.425.2
Methylene chloride 75-09-2 8260B ND 1ug/kg2.75.2
Styrene 100-42-5 8260B ND 1ug/kg1.15.2
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.495.2
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.525.2
Toluene 108-88-3 8260B ND 1ug/kg1.85.2
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.655.2
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.85.2
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.885.2
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.825.2
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 43 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-26(6'-8')
QB12016-015
02/11/2015 1611
02/12/2015
Solid
% Solids:85.9 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1259 DCS 67778 5.63
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.05.2
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.65.2
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.895.2
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.05.2
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 53-142
Bromofluorobenzene 100 47-138
Toluene-d8 106 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 44 of 79
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-26(6'-8')
QB12016-015
02/11/2015 1611
02/12/2015
Solid
% Solids:85.9 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 1947 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 360000 B 1ug/kg14007800
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 85 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 45 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-28(6'-8')
QB12016-016
02/11/2015 1615
02/12/2015
Solid
% Solids:77.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 2008 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 420000 B 1ug/kg16008600
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 79 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 46 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-31(0'-5')
QB12016-017
02/11/2015 1629
02/12/2015
Solid
% Solids:84.9 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 2029 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 1700000 B 1ug/kg14007900
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 95 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 47 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-27(8'-10')
QB12016-018
02/11/2015 1637
02/12/2015
Solid
% Solids:89.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg190220
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 48 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-27(8'-10')
QB12016-018
02/11/2015 1637
02/12/2015
Solid
% Solids:89.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1320 DCS 67778 5.96
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg6.319
Benzene 71-43-2 8260B ND 1ug/kg1.04.7
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.64.7
Bromoform 75-25-2 8260B ND 1ug/kg0.654.7
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg1.74.7
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg2.29.3
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.24.7
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.74.7
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.64.7
Chloroethane 75-00-3 8260B ND 1ug/kg1.24.7
Chloroform 67-66-3 8260B ND 1ug/kg0.784.7
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg0.934.7
Cyclohexane 110-82-7 8260B ND 1ug/kg0.634.7
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.44.7
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.64.7
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.794.7
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.64.7
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.64.7
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.64.7
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.54.7
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.684.7
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg0.934.7
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.64.7
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.714.7
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.44.7
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg0.854.7
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.644.7
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.774.7
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.64.7
2-Hexanone 591-78-6 8260B ND 1ug/kg1.29.3
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.214.7
Methyl acetate 79-20-9 8260B ND 1ug/kg0.924.7
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.374.7
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.49.3
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.384.7
Methylene chloride 75-09-2 8260B ND 1ug/kg2.44.7
Styrene 100-42-5 8260B ND 1ug/kg1.04.7
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.444.7
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.474.7
Toluene 108-88-3 8260B ND 1ug/kg1.64.7
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.594.7
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.64.7
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.794.7
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.744.7
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 49 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-27(8'-10')
QB12016-018
02/11/2015 1637
02/12/2015
Solid
% Solids:89.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/13/2015 1320 DCS 67778 5.96
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg1.84.7
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.44.7
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.804.7
Xylenes (total)1330-20-7 8260B ND 1ug/kg2.74.7
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 53-142
Bromofluorobenzene 103 47-138
Toluene-d8 105 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 50 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-27(8'-10')
QB12016-018
02/11/2015 1637
02/12/2015
Solid
% Solids:89.8 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 2050 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 31000 B 1ug/kg14007400
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 81 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 51 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-29(6'-8')
QB12016-019
02/11/2015 1652
02/12/2015
Solid
% Solids:87.2 02/12/2015 1957
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/16/2015 2111 MEM 02/13/2015 1636 67792
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 220000 B 1ug/kg14007600
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 77 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 52 of 79
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
Page: 53 of 79
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - MB
Batch:
Sample ID:QQ67843-001
67843
Analytical Method:9071B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
HEM (oil and grease)ND 02/14/2015 1120200170mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 54 of 79
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - LCS
Batch:
Sample ID:QQ67843-002
67843
Analytical Method:9071B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
HEM (oil and grease)2200 02/14/2015 1120110200070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 55 of 79
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - Duplicate
Batch:
Sample ID:QB12016-010DU
67843
Analytical Method:9071B
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)
HEM (oil and grease)510 02/14/2015 112013205101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 56 of 79
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - MS
Batch:
Sample ID:QB12016-010MS
67843
Analytical Method:9071B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
HEM (oil and grease)2800 02/14/2015 112090260070-1305101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 57 of 79
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ67778-001
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 02/13/2015 1102206.7 ug/kg1
Benzene ND 02/13/2015 11025.0 1.1 ug/kg1
Bromodichloromethane ND 02/13/2015 11025.0 1.7 ug/kg1
Bromoform ND 02/13/2015 11025.0 0.70 ug/kg1
Bromomethane (Methyl bromide)ND 02/13/2015 11025.0 1.8 ug/kg1
2-Butanone (MEK)ND 02/13/2015 1102102.4 ug/kg1
Carbon disulfide ND 02/13/2015 11025.0 1.3 ug/kg1
Carbon tetrachloride ND 02/13/2015 11025.0 1.8 ug/kg1
Chlorobenzene ND 02/13/2015 11025.0 1.7 ug/kg1
Chloroethane ND 02/13/2015 11025.0 1.3 ug/kg1
Chloroform ND 02/13/2015 11025.0 0.83 ug/kg1
Chloromethane (Methyl chloride)ND 02/13/2015 11025.0 1.0 ug/kg1
Cyclohexane ND 02/13/2015 11025.0 0.67 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 02/13/2015 11025.0 1.5 ug/kg1
Dibromochloromethane ND 02/13/2015 11025.0 1.7 ug/kg1
1,2-Dibromoethane (EDB)ND 02/13/2015 11025.0 0.85 ug/kg1
1,3-Dichlorobenzene ND 02/13/2015 11025.0 1.7 ug/kg1
1,2-Dichlorobenzene ND 02/13/2015 11025.0 1.7 ug/kg1
1,4-Dichlorobenzene ND 02/13/2015 11025.0 1.7 ug/kg1
Dichlorodifluoromethane ND 02/13/2015 11025.0 1.6 ug/kg1
1,1-Dichloroethane ND 02/13/2015 11025.0 0.73 ug/kg1
1,2-Dichloroethane ND 02/13/2015 11025.0 1.0 ug/kg1
1,1-Dichloroethene ND 02/13/2015 11025.0 1.7 ug/kg1
cis-1,2-Dichloroethene ND 02/13/2015 11025.0 0.76 ug/kg1
trans-1,2-Dichloroethene ND 02/13/2015 11025.0 1.5 ug/kg1
1,2-Dichloropropane ND 02/13/2015 11025.0 0.91 ug/kg1
cis-1,3-Dichloropropene ND 02/13/2015 11025.0 0.68 ug/kg1
trans-1,3-Dichloropropene ND 02/13/2015 11025.0 0.82 ug/kg1
Ethylbenzene ND 02/13/2015 11025.0 1.7 ug/kg1
2-Hexanone ND 02/13/2015 1102101.3 ug/kg1
Isopropylbenzene ND 02/13/2015 11025.0 0.23 ug/kg1
Methyl acetate ND 02/13/2015 11025.0 0.98 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 02/13/2015 11025.0 0.40 ug/kg1
4-Methyl-2-pentanone ND 02/13/2015 1102101.5 ug/kg1
Methylcyclohexane ND 02/13/2015 11025.0 0.41 ug/kg1
Methylene chloride ND 02/13/2015 11025.0 2.6 ug/kg1
Styrene ND 02/13/2015 11025.0 1.1 ug/kg1
1,1,2,2-Tetrachloroethane ND 02/13/2015 11025.0 0.47 ug/kg1
Tetrachloroethene ND 02/13/2015 11025.0 0.50 ug/kg1
Toluene ND 02/13/2015 11025.0 1.7 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 02/13/2015 11025.0 0.63 ug/kg1
1,2,4-Trichlorobenzene ND 02/13/2015 11025.0 1.7 ug/kg1
1,1,2-Trichloroethane ND 02/13/2015 11025.0 0.79 ug/kg1
1,1,1-Trichloroethane ND 02/13/2015 11025.0 0.85 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 58 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ67778-001
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Trichloroethene ND 02/13/2015 11025.0 1.9 ug/kg1
Trichlorofluoromethane ND 02/13/2015 11025.0 1.5 ug/kg1
Vinyl chloride ND 02/13/2015 11025.0 0.86 ug/kg1
Xylenes (total)ND 02/13/2015 11025.0 2.9 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 47-138
1,2-Dichloroethane-d4 99 53-142
Toluene-d8 106 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 59 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ67778-002
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 130 02/13/2015 102013010060-1401
Benzene 56 02/13/2015 10201125069-1231
Bromodichloromethane 55 02/13/2015 10201115069-1211
Bromoform 53 02/13/2015 10201055061-1191
Bromomethane (Methyl bromide)59 02/13/2015 10201175010-1681
2-Butanone (MEK)110 02/13/2015 102011210057-1481
Carbon disulfide 58 02/13/2015 10201175058-1221
Carbon tetrachloride 59 02/13/2015 10201185058-1361
Chlorobenzene 54 02/13/2015 10201085059-1291
Chloroethane 59 02/13/2015 10201195042-1631
Chloroform 57 02/13/2015 10201145071-1251
Chloromethane (Methyl chloride)59 02/13/2015 10201185034-1341
Cyclohexane 57 02/13/2015 10201145053-1391
1,2-Dibromo-3-chloropropane (DBCP)49 02/13/2015 1020995055-1251
Dibromochloromethane 53 02/13/2015 10201065066-1191
1,2-Dibromoethane (EDB)53 02/13/2015 10201065074-1241
1,3-Dichlorobenzene 54 02/13/2015 10201085051-1341
1,2-Dichlorobenzene 54 02/13/2015 10201075057-1311
1,4-Dichlorobenzene 53 02/13/2015 10201055052-1331
Dichlorodifluoromethane 66 02/13/2015 10201325010-1571
1,1-Dichloroethane 57 02/13/2015 10201145071-1271
1,2-Dichloroethane 55 02/13/2015 10201105067-1291
1,1-Dichloroethene 61 02/13/2015 10201225069-1381
cis-1,2-Dichloroethene 57 02/13/2015 10201145070-1221
trans-1,2-Dichloroethene 59 02/13/2015 10201185068-1311
1,2-Dichloropropane 55 02/13/2015 10201105072-1241
cis-1,3-Dichloropropene 56 02/13/2015 10201125070-1261
trans-1,3-Dichloropropene 55 02/13/2015 10201095070-1241
Ethylbenzene 56 02/13/2015 10201125059-1281
2-Hexanone 94 02/13/2015 10209410054-1371
Isopropylbenzene 57 02/13/2015 10201135050-1361
Methyl acetate 54 02/13/2015 10201085059-1371
Methyl tertiary butyl ether (MTBE)55 02/13/2015 10201095070-1301
4-Methyl-2-pentanone 97 02/13/2015 10209710060-1341
Methylcyclohexane 58 02/13/2015 10201165041-1441
Methylene chloride 56 02/13/2015 10201135070-1301
Styrene 54 02/13/2015 10201095054-1361
1,1,2,2-Tetrachloroethane 52 02/13/2015 10201045069-1321
Tetrachloroethene 57 02/13/2015 10201145045-1501
Toluene 56 02/13/2015 10201125061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 68 02/13/2015 1020N1375049-1361
1,2,4-Trichlorobenzene 55 02/13/2015 10201115034-1451
1,1,2-Trichloroethane 50 02/13/2015 10201005055-1281
1,1,1-Trichloroethane 58 02/13/2015 10201175063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 60 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ67778-002
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 56 02/13/2015 10201125062-1261
Trichlorofluoromethane 60 02/13/2015 10201195045-1381
Vinyl chloride 61 02/13/2015 10201215042-1321
Xylenes (total)110 02/13/2015 102011010058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 98 47-138
1,2-Dichloroethane-d4 94 53-142
Toluene-d8 106 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 61 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:QB12016-018DU
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Acetone 11 02/13/2015 1856+75 20ND1
Benzene ND 02/13/2015 18560.00 20ND1
Bromodichloromethane ND 02/13/2015 18560.00 20ND1
Bromoform ND 02/13/2015 18560.00 20ND1
Bromomethane (Methyl bromide)ND 02/13/2015 18560.00 20ND1
2-Butanone (MEK)ND 02/13/2015 18560.00 20ND1
Carbon disulfide ND 02/13/2015 18560.00 20ND1
Carbon tetrachloride ND 02/13/2015 18560.00 20ND1
Chlorobenzene ND 02/13/2015 18560.00 20ND1
Chloroethane ND 02/13/2015 18560.00 20ND1
Chloroform ND 02/13/2015 18560.00 20ND1
Chloromethane (Methyl chloride)ND 02/13/2015 18560.00 20ND1
Cyclohexane ND 02/13/2015 18560.00 20ND1
1,2-Dibromo-3-chloropropane (DBCP)ND 02/13/2015 18560.00 20ND1
Dibromochloromethane ND 02/13/2015 18560.00 20ND1
1,2-Dibromoethane (EDB)ND 02/13/2015 18560.00 20ND1
1,2-Dichlorobenzene ND 02/13/2015 18560.00 20ND1
1,3-Dichlorobenzene ND 02/13/2015 18560.00 20ND1
1,4-Dichlorobenzene ND 02/13/2015 18560.00 20ND1
Dichlorodifluoromethane ND 02/13/2015 18560.00 20ND1
1,1-Dichloroethane ND 02/13/2015 18560.00 20ND1
1,2-Dichloroethane ND 02/13/2015 18560.00 20ND1
1,1-Dichloroethene ND 02/13/2015 18560.00 20ND1
cis-1,2-Dichloroethene ND 02/13/2015 18560.00 20ND1
trans-1,2-Dichloroethene ND 02/13/2015 18560.00 20ND1
1,2-Dichloropropane ND 02/13/2015 18560.00 20ND1
cis-1,3-Dichloropropene ND 02/13/2015 18560.00 20ND1
trans-1,3-Dichloropropene ND 02/13/2015 18560.00 20ND1
Ethylbenzene ND 02/13/2015 18560.00 20ND1
2-Hexanone ND 02/13/2015 18560.00 20ND1
Isopropylbenzene ND 02/13/2015 18560.00 20ND1
Methyl acetate ND 02/13/2015 18560.00 20ND1
Methyl tertiary butyl ether (MTBE)ND 02/13/2015 18560.00 20ND1
4-Methyl-2-pentanone ND 02/13/2015 18560.00 20ND1
Methylcyclohexane ND 02/13/2015 18560.00 20ND1
Methylene chloride ND 02/13/2015 18560.00 20ND1
Styrene ND 02/13/2015 18560.00 20ND1
1,1,2,2-Tetrachloroethane ND 02/13/2015 18560.00 20ND1
Tetrachloroethene ND 02/13/2015 18560.00 20ND1
Toluene ND 02/13/2015 18560.00 20ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 02/13/2015 18560.00 20ND1
1,2,4-Trichlorobenzene ND 02/13/2015 18560.00 20ND1
1,1,1-Trichloroethane ND 02/13/2015 18560.00 20ND1
1,1,2-Trichloroethane ND 02/13/2015 18560.00 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 62 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:QB12016-018DU
67778 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Trichloroethene ND 02/13/2015 18560.00 20ND1
Trichlorofluoromethane ND 02/13/2015 18560.00 20ND1
Vinyl chloride ND 02/13/2015 18560.00 20ND1
Xylenes (total)ND 02/13/2015 18560.00 20ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 100 53-142
Bromofluorobenzene 105 47-138
Toluene-d8 103 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 63 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ67933-001
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone 5.8 02/16/2015 1241J205.1 ug/kg1
Benzene ND 02/16/2015 12415.0 1.6 ug/kg1
Bromodichloromethane ND 02/16/2015 12415.0 1.7 ug/kg1
Bromoform ND 02/16/2015 12415.0 2.0 ug/kg1
Bromomethane (Methyl bromide)ND 02/16/2015 12415.0 2.2 ug/kg1
2-Butanone (MEK)ND 02/16/2015 1241104.2 ug/kg1
Carbon disulfide ND 02/16/2015 12415.0 1.3 ug/kg1
Carbon tetrachloride ND 02/16/2015 12415.0 1.4 ug/kg1
Chlorobenzene ND 02/16/2015 12415.0 1.6 ug/kg1
Chloroethane ND 02/16/2015 12415.0 2.4 ug/kg1
Chloroform ND 02/16/2015 12415.0 1.5 ug/kg1
Chloromethane (Methyl chloride)ND 02/16/2015 12415.0 2.0 ug/kg1
Cyclohexane ND 02/16/2015 12415.0 1.7 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 02/16/2015 12415.0 2.1 ug/kg1
Dibromochloromethane ND 02/16/2015 12415.0 1.7 ug/kg1
1,2-Dibromoethane (EDB)ND 02/16/2015 12415.0 1.7 ug/kg1
1,4-Dichlorobenzene ND 02/16/2015 12415.0 1.5 ug/kg1
1,2-Dichlorobenzene ND 02/16/2015 12415.0 1.7 ug/kg1
1,3-Dichlorobenzene ND 02/16/2015 12415.0 1.7 ug/kg1
Dichlorodifluoromethane ND 02/16/2015 12415.0 3.7 ug/kg1
1,2-Dichloroethane ND 02/16/2015 12415.0 1.6 ug/kg1
1,1-Dichloroethane ND 02/16/2015 12415.0 1.5 ug/kg1
trans-1,2-Dichloroethene ND 02/16/2015 12415.0 1.5 ug/kg1
cis-1,2-Dichloroethene ND 02/16/2015 12415.0 1.6 ug/kg1
1,1-Dichloroethene ND 02/16/2015 12415.0 1.8 ug/kg1
1,2-Dichloropropane ND 02/16/2015 12415.0 1.5 ug/kg1
trans-1,3-Dichloropropene ND 02/16/2015 12415.0 1.5 ug/kg1
cis-1,3-Dichloropropene ND 02/16/2015 12415.0 1.5 ug/kg1
Ethylbenzene ND 02/16/2015 12415.0 1.6 ug/kg1
2-Hexanone ND 02/16/2015 1241103.8 ug/kg1
Isopropylbenzene ND 02/16/2015 12415.0 1.5 ug/kg1
Methyl acetate ND 02/16/2015 12415.0 0.98 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 02/16/2015 12415.0 0.40 ug/kg1
4-Methyl-2-pentanone ND 02/16/2015 1241101.5 ug/kg1
Methylcyclohexane ND 02/16/2015 12415.0 0.41 ug/kg1
Methylene chloride ND 02/16/2015 12415.0 2.6 ug/kg1
Styrene ND 02/16/2015 12415.0 1.1 ug/kg1
1,1,2,2-Tetrachloroethane ND 02/16/2015 12415.0 0.47 ug/kg1
Tetrachloroethene ND 02/16/2015 12415.0 0.50 ug/kg1
Toluene ND 02/16/2015 12415.0 1.7 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 02/16/2015 12415.0 0.63 ug/kg1
1,2,4-Trichlorobenzene ND 02/16/2015 12415.0 1.7 ug/kg1
1,1,2-Trichloroethane ND 02/16/2015 12415.0 0.79 ug/kg1
1,1,1-Trichloroethane ND 02/16/2015 12415.0 0.85 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 64 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ67933-001
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Trichloroethene ND 02/16/2015 12415.0 1.9 ug/kg1
Trichlorofluoromethane ND 02/16/2015 12415.0 1.5 ug/kg1
Vinyl chloride ND 02/16/2015 12415.0 0.86 ug/kg1
Xylenes (total)ND 02/16/2015 12415.0 2.9 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 93 47-138
1,2-Dichloroethane-d4 94 53-142
Toluene-d8 94 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 65 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ67933-002
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 100 02/16/2015 114410010060-1401
Benzene 46 02/16/2015 1144935069-1231
Bromodichloromethane 48 02/16/2015 1144965069-1211
Bromoform 48 02/16/2015 1144965061-1191
Bromomethane (Methyl bromide)56 02/16/2015 11441115010-1681
2-Butanone (MEK)94 02/16/2015 11449410057-1481
Carbon disulfide 45 02/16/2015 1144905058-1221
Carbon tetrachloride 48 02/16/2015 1144975058-1361
Chlorobenzene 47 02/16/2015 1144955059-1291
Chloroethane 55 02/16/2015 11441105042-1631
Chloroform 48 02/16/2015 1144955071-1251
Chloromethane (Methyl chloride)56 02/16/2015 11441115034-1341
Cyclohexane 46 02/16/2015 1144925053-1391
1,2-Dibromo-3-chloropropane (DBCP)47 02/16/2015 1144945055-1251
Dibromochloromethane 49 02/16/2015 1144975066-1191
1,2-Dibromoethane (EDB)47 02/16/2015 1144945074-1241
1,4-Dichlorobenzene 48 02/16/2015 1144965052-1331
1,2-Dichlorobenzene 48 02/16/2015 1144965057-1311
1,3-Dichlorobenzene 49 02/16/2015 1144975051-1341
Dichlorodifluoromethane 60 02/16/2015 11441195010-1571
1,2-Dichloroethane 46 02/16/2015 1144925067-1291
1,1-Dichloroethane 47 02/16/2015 1144945071-1271
trans-1,2-Dichloroethene 47 02/16/2015 1144945068-1311
cis-1,2-Dichloroethene 48 02/16/2015 1144965070-1221
1,1-Dichloroethene 46 02/16/2015 1144925069-1381
1,2-Dichloropropane 46 02/16/2015 1144935072-1241
trans-1,3-Dichloropropene 48 02/16/2015 1144955070-1241
cis-1,3-Dichloropropene 47 02/16/2015 1144955070-1261
Ethylbenzene 48 02/16/2015 1144965059-1281
2-Hexanone 91 02/16/2015 11449110054-1371
Isopropylbenzene 49 02/16/2015 1144985050-1361
Methyl acetate 49 02/16/2015 1144975059-1371
Methyl tertiary butyl ether (MTBE)46 02/16/2015 1144925070-1301
4-Methyl-2-pentanone 90 02/16/2015 11449010060-1341
Methylcyclohexane 47 02/16/2015 1144935041-1441
Methylene chloride 43 02/16/2015 1144865070-1301
Styrene 49 02/16/2015 1144975054-1361
1,1,2,2-Tetrachloroethane 47 02/16/2015 1144945069-1321
Tetrachloroethene 48 02/16/2015 1144965045-1501
Toluene 44 02/16/2015 1144885061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 46 02/16/2015 1144935049-1361
1,2,4-Trichlorobenzene 47 02/16/2015 1144955034-1451
1,1,2-Trichloroethane 46 02/16/2015 1144925055-1281
1,1,1-Trichloroethane 48 02/16/2015 1144975063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 66 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ67933-002
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 47 02/16/2015 1144945062-1261
Trichlorofluoromethane 56 02/16/2015 11441125045-1381
Vinyl chloride 57 02/16/2015 11441145042-1321
Xylenes (total)95 02/16/2015 11449510058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 92 47-138
1,2-Dichloroethane-d4 85 53-142
Toluene-d8 94 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 67 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:QB12016-010DU
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Acetone ND 02/16/2015 19510.00 20ND1
Benzene ND 02/16/2015 19510.00 20ND1
Bromodichloromethane ND 02/16/2015 19510.00 20ND1
Bromoform ND 02/16/2015 19510.00 20ND1
Bromomethane (Methyl bromide)ND 02/16/2015 19510.00 20ND1
2-Butanone (MEK)ND 02/16/2015 19510.00 20ND1
Carbon disulfide ND 02/16/2015 19510.00 20ND1
Carbon tetrachloride ND 02/16/2015 19510.00 20ND1
Chlorobenzene ND 02/16/2015 19510.00 20ND1
Chloroethane ND 02/16/2015 19510.00 20ND1
Chloroform ND 02/16/2015 19510.00 20ND1
Chloromethane (Methyl chloride)ND 02/16/2015 19510.00 20ND1
Cyclohexane ND 02/16/2015 19510.00 20ND1
1,2-Dibromo-3-chloropropane (DBCP)ND 02/16/2015 19510.00 20ND1
Dibromochloromethane ND 02/16/2015 19510.00 20ND1
1,2-Dibromoethane (EDB)ND 02/16/2015 19510.00 20ND1
1,2-Dichlorobenzene ND 02/16/2015 19510.00 20ND1
1,3-Dichlorobenzene ND 02/16/2015 19510.00 20ND1
1,4-Dichlorobenzene ND 02/16/2015 19510.00 20ND1
Dichlorodifluoromethane ND 02/16/2015 19510.00 20ND1
1,1-Dichloroethane 1.8 02/16/2015 1951+80 20ND1
1,2-Dichloroethane ND 02/16/2015 19510.00 20ND1
1,1-Dichloroethene ND 02/16/2015 19510.00 20ND1
cis-1,2-Dichloroethene ND 02/16/2015 19510.00 20ND1
trans-1,2-Dichloroethene ND 02/16/2015 19510.00 20ND1
1,2-Dichloropropane ND 02/16/2015 19510.00 20ND1
cis-1,3-Dichloropropene ND 02/16/2015 19510.00 20ND1
trans-1,3-Dichloropropene ND 02/16/2015 19510.00 20ND1
Ethylbenzene ND 02/16/2015 19510.00 20ND1
2-Hexanone ND 02/16/2015 19510.00 20ND1
Isopropylbenzene ND 02/16/2015 19510.00 20ND1
Methyl acetate ND 02/16/2015 19510.00 20ND1
Methyl tertiary butyl ether (MTBE)0.76 02/16/2015 1951+33 200.55 1
4-Methyl-2-pentanone ND 02/16/2015 19510.00 20ND1
Methylcyclohexane ND 02/16/2015 19510.00 20ND1
Methylene chloride ND 02/16/2015 19510.00 20ND1
Styrene ND 02/16/2015 19510.00 20ND1
1,1,2,2-Tetrachloroethane ND 02/16/2015 19510.00 20ND1
Tetrachloroethene 0.55 02/16/2015 1951+24 20ND1
Toluene ND 02/16/2015 19510.00 20ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 02/16/2015 19510.00 20ND1
1,2,4-Trichlorobenzene ND 02/16/2015 19510.00 20ND1
1,1,1-Trichloroethane ND 02/16/2015 19510.00 20ND1
1,1,2-Trichloroethane ND 02/16/2015 19510.00 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 68 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:QB12016-010DU
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Trichloroethene ND 02/16/2015 19510.00 20ND1
Trichlorofluoromethane ND 02/16/2015 19510.00 20ND1
Vinyl chloride ND 02/16/2015 19510.00 20ND1
Xylenes (total)ND 02/16/2015 19510.00 20ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 100 53-142
Bromofluorobenzene 95 47-138
Toluene-d8 92 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 69 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:QB12016-013MS
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acetone 100 02/16/2015 20138011060-140131
Benzene 47 02/16/2015 2013835669-123ND1
Bromodichloromethane 49 02/16/2015 2013875669-121ND1
Bromoform 48 02/16/2015 2013855661-119ND1
Bromomethane (Methyl bromide)48 02/16/2015 2013865635-144ND1
2-Butanone (MEK)100 02/16/2015 20138911057-148ND1
Carbon disulfide 44 02/16/2015 2013775658-122ND1
Carbon tetrachloride 44 02/16/2015 2013775658-136ND1
Chlorobenzene 41 02/16/2015 2013735659-129ND1
Chloroethane 48 02/16/2015 2013845650-132ND1
Chloroform 49 02/16/2015 2013875671-125ND1
Chloromethane (Methyl chloride)48 02/16/2015 2013845634-134ND1
Cyclohexane 31 02/16/2015 2013565653-139ND1
1,2-Dibromo-3-chloropropane (DBCP)45 02/16/2015 2013795655-125ND1
Dibromochloromethane 49 02/16/2015 2013865666-119ND1
1,2-Dibromoethane (EDB)49 02/16/2015 2013875674-124ND1
1,2-Dichlorobenzene 35 02/16/2015 2013615657-131ND1
1,3-Dichlorobenzene 33 02/16/2015 2013585651-134ND1
1,4-Dichlorobenzene 33 02/16/2015 2013595652-133ND1
Dichlorodifluoromethane 49 02/16/2015 2013865610-157ND1
1,1-Dichloroethane 49 02/16/2015 2013865671-127ND1
1,2-Dichloroethane 50 02/16/2015 2013895667-129ND1
1,1-Dichloroethene 45 02/16/2015 2013805669-138ND1
cis-1,2-Dichloroethene 49 02/16/2015 2013875670-122ND1
trans-1,2-Dichloroethene 48 02/16/2015 2013845668-131ND1
1,2-Dichloropropane 48 02/16/2015 2013845672-124ND1
cis-1,3-Dichloropropene 50 02/16/2015 2013885670-126ND1
trans-1,3-Dichloropropene 48 02/16/2015 2013855670-124ND1
Ethylbenzene 37 02/16/2015 2013665659-128ND1
2-Hexanone 93 02/16/2015 20138211054-137ND1
Isopropylbenzene 33 02/16/2015 2013595650-136ND1
Methyl acetate 55 02/16/2015 2013975659-137ND1
Methyl tertiary butyl ether (MTBE)55 02/16/2015 2013935670-1302.8 1
4-Methyl-2-pentanone 100 02/16/2015 20139011060-134ND1
Methylcyclohexane 26 02/16/2015 2013465641-144ND1
Methylene chloride 46 02/16/2015 2013815677-129ND1
Styrene 41 02/16/2015 2013725654-136ND1
1,1,2,2-Tetrachloroethane 49 02/16/2015 2013875669-132ND1
Tetrachloroethene 35 02/16/2015 2013N625670-130ND1
Toluene 41 02/16/2015 2013735661-129ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane 39 02/16/2015 2013695649-136ND1
1,2,4-Trichlorobenzene 23 02/16/2015 2013405634-145ND1
1,1,1-Trichloroethane 47 02/16/2015 2013835663-128ND1
1,1,2-Trichloroethane 48 02/16/2015 2013855655-128ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 70 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:QB12016-013MS
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Trichloroethene 45 02/16/2015 2013795662-126ND1
Trichlorofluoromethane 45 02/16/2015 2013795645-138ND1
Vinyl chloride 49 02/16/2015 2013885642-132ND1
Xylenes (total)74 02/16/2015 20136511058-128ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 93 53-142
Bromofluorobenzene 90 47-138
Toluene-d8 96 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 71 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ68027-001
68027 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 02/17/2015 1615205.1 ug/kg1
Benzene ND 02/17/2015 16155.0 1.6 ug/kg1
Bromodichloromethane ND 02/17/2015 16155.0 1.7 ug/kg1
Bromoform ND 02/17/2015 16155.0 2.0 ug/kg1
Bromomethane (Methyl bromide)ND 02/17/2015 16155.0 2.2 ug/kg1
2-Butanone (MEK)ND 02/17/2015 1615104.2 ug/kg1
Carbon disulfide ND 02/17/2015 16155.0 1.3 ug/kg1
Carbon tetrachloride ND 02/17/2015 16155.0 1.4 ug/kg1
Chlorobenzene ND 02/17/2015 16155.0 1.6 ug/kg1
Chloroethane ND 02/17/2015 16155.0 2.4 ug/kg1
Chloroform ND 02/17/2015 16155.0 1.5 ug/kg1
Chloromethane (Methyl chloride)ND 02/17/2015 16155.0 2.0 ug/kg1
Cyclohexane ND 02/17/2015 16155.0 1.7 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 02/17/2015 16155.0 2.1 ug/kg1
Dibromochloromethane ND 02/17/2015 16155.0 1.7 ug/kg1
1,2-Dibromoethane (EDB)ND 02/17/2015 16155.0 1.7 ug/kg1
1,3-Dichlorobenzene ND 02/17/2015 16155.0 1.7 ug/kg1
1,2-Dichlorobenzene ND 02/17/2015 16155.0 1.7 ug/kg1
1,4-Dichlorobenzene ND 02/17/2015 16155.0 1.5 ug/kg1
Dichlorodifluoromethane ND 02/17/2015 16155.0 3.7 ug/kg1
1,2-Dichloroethane ND 02/17/2015 16155.0 1.6 ug/kg1
1,1-Dichloroethane ND 02/17/2015 16155.0 1.5 ug/kg1
trans-1,2-Dichloroethene ND 02/17/2015 16155.0 1.5 ug/kg1
cis-1,2-Dichloroethene ND 02/17/2015 16155.0 1.6 ug/kg1
1,1-Dichloroethene ND 02/17/2015 16155.0 1.8 ug/kg1
1,2-Dichloropropane ND 02/17/2015 16155.0 1.5 ug/kg1
trans-1,3-Dichloropropene ND 02/17/2015 16155.0 1.5 ug/kg1
cis-1,3-Dichloropropene ND 02/17/2015 16155.0 1.5 ug/kg1
Ethylbenzene ND 02/17/2015 16155.0 1.6 ug/kg1
2-Hexanone ND 02/17/2015 1615103.8 ug/kg1
Isopropylbenzene ND 02/17/2015 16155.0 1.5 ug/kg1
Methyl acetate ND 02/17/2015 16155.0 1.8 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 02/17/2015 16155.0 1.6 ug/kg1
4-Methyl-2-pentanone ND 02/17/2015 1615103.6 ug/kg1
Methylcyclohexane ND 02/17/2015 16155.0 1.7 ug/kg1
Methylene chloride ND 02/17/2015 16155.0 1.2 ug/kg1
Styrene ND 02/17/2015 16155.0 1.7 ug/kg1
1,1,2,2-Tetrachloroethane ND 02/17/2015 16155.0 0.47 ug/kg1
Tetrachloroethene ND 02/17/2015 16155.0 0.50 ug/kg1
Toluene ND 02/17/2015 16155.0 1.7 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 02/17/2015 16155.0 0.63 ug/kg1
1,2,4-Trichlorobenzene ND 02/17/2015 16155.0 1.7 ug/kg1
1,1,1-Trichloroethane ND 02/17/2015 16155.0 0.85 ug/kg1
1,1,2-Trichloroethane ND 02/17/2015 16155.0 1.8 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 72 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ68027-001
68027 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Trichloroethene ND 02/17/2015 16155.0 1.9 ug/kg1
Trichlorofluoromethane ND 02/17/2015 16155.0 1.5 ug/kg1
Vinyl chloride ND 02/17/2015 16155.0 0.86 ug/kg1
Xylenes (total)ND 02/17/2015 16155.0 2.9 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 94 47-138
1,2-Dichloroethane-d4 89 53-142
Toluene-d8 95 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 73 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ68027-002
68027 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 120 02/17/2015 151611910060-1401
Benzene 45 02/17/2015 1516915069-1231
Bromodichloromethane 47 02/17/2015 1516955069-1211
Bromoform 47 02/17/2015 1516935061-1191
Bromomethane (Methyl bromide)45 02/17/2015 1516915010-1681
2-Butanone (MEK)100 02/17/2015 151610310057-1481
Carbon disulfide 43 02/17/2015 1516875058-1221
Carbon tetrachloride 46 02/17/2015 1516925058-1361
Chlorobenzene 45 02/17/2015 1516905059-1291
Chloroethane 47 02/17/2015 1516955042-1631
Chloroform 46 02/17/2015 1516925071-1251
Chloromethane (Methyl chloride)43 02/17/2015 1516875034-1341
Cyclohexane 42 02/17/2015 1516835053-1391
1,2-Dibromo-3-chloropropane (DBCP)47 02/17/2015 1516955055-1251
Dibromochloromethane 46 02/17/2015 1516935066-1191
1,2-Dibromoethane (EDB)47 02/17/2015 1516935074-1241
1,3-Dichlorobenzene 45 02/17/2015 1516905051-1341
1,2-Dichlorobenzene 46 02/17/2015 1516925057-1311
1,4-Dichlorobenzene 45 02/17/2015 1516895052-1331
Dichlorodifluoromethane 48 02/17/2015 1516965010-1571
1,2-Dichloroethane 47 02/17/2015 1516955067-1291
1,1-Dichloroethane 45 02/17/2015 1516905071-1271
trans-1,2-Dichloroethene 45 02/17/2015 1516905068-1311
cis-1,2-Dichloroethene 47 02/17/2015 1516945070-1221
1,1-Dichloroethene 44 02/17/2015 1516895069-1381
1,2-Dichloropropane 46 02/17/2015 1516935072-1241
trans-1,3-Dichloropropene 48 02/17/2015 1516975070-1241
cis-1,3-Dichloropropene 48 02/17/2015 1516975070-1261
Ethylbenzene 45 02/17/2015 1516905059-1281
2-Hexanone 91 02/17/2015 15169110054-1371
Isopropylbenzene 46 02/17/2015 1516925050-1361
Methyl acetate 50 02/17/2015 1516995059-1371
Methyl tertiary butyl ether (MTBE)46 02/17/2015 1516935070-1301
4-Methyl-2-pentanone 94 02/17/2015 15169410060-1341
Methylcyclohexane 44 02/17/2015 1516885041-1441
Methylene chloride 43 02/17/2015 1516855070-1301
Styrene 46 02/17/2015 1516915054-1361
1,1,2,2-Tetrachloroethane 48 02/17/2015 1516965069-1321
Tetrachloroethene 45 02/17/2015 1516915045-1501
Toluene 46 02/17/2015 1516925061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 45 02/17/2015 1516895049-1361
1,2,4-Trichlorobenzene 46 02/17/2015 1516935034-1451
1,1,1-Trichloroethane 45 02/17/2015 1516915063-1281
1,1,2-Trichloroethane 45 02/17/2015 1516905055-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 74 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ68027-002
68027 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 46 02/17/2015 1516925062-1261
Trichlorofluoromethane 48 02/17/2015 1516965045-1381
Vinyl chloride 46 02/17/2015 1516925042-1321
Xylenes (total)89 02/17/2015 15168910058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 92 47-138
1,2-Dichloroethane-d4 89 53-142
Toluene-d8 96 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 75 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO - MB
Batch:Prep Method:
Prep Date:
Sample ID:QQ67792-001
67792 3550C
02/13/2015 1636Analytical Method:8015C
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
TPH-DRO 3000 02/16/2015 1412J67001200ug/kg1
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 76 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 76 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO - LCS
Batch:Prep Method:
Prep Date:
Sample ID:QQ67792-002
67792 3550C
02/13/2015 1636Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
TPH-DRO 63000 02/16/2015 1330768300070-1301
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 79 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 77 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO - MS
Batch:Prep Method:
Prep Date:
Sample ID:QB12016-003MS
67792 3550C
02/13/2015 1636Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
TPH-DRO 7500000 02/17/2015 0612N-205098000 70-130950000010
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 102 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 78 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO - MSD
Batch:Prep Method:
Prep Date:
Sample ID:QB12016-003MD
67792 3550C
02/13/2015 1636Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
TPH-DRO 7100000 02/17/2015 0632N-236099000 70-1304.5 20950000010
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 106 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 79 of 79
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Terracon Consultants, Inc.
2401 Brentwood Road
Suite 107 I
Raleigh, NC 27604
Attention: Justin Fabriziani
QB13011Lot Number:
70157304Project Number:
Proposed Durham PDHQProject Name:
02/19/2015Date Completed:
Nisreen Saikaly
Project Manager
*QB13011*

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Terracon Consultants, Inc.
Lot Number: QB13011
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
DRO Pattern Identification
QB13011-003 SB-36 (2'-4') DRO pattern unknown.
QB13011-004 SB-39 (4'-6') DRO pattern unknown.
QB13011-005 SB-34 (0'-2') Pattern resembles a mixture of gasoline and oil
QB13011-006 SB-35 (2'-4') DRO pattern unknown.
QB13011-007 SB-44 (2'-4') DRO pattern unknown.
QB13011-009 SB-52 (8'-10') DRO resemble an oil pattern.
QB13011-010 SB-53 (10'-12') DRO resemble an oil pattern.
QB13011-011 SB-47 (8'-10') DRO resemble an oil pattern.
QB13011-012 SB-49 (2'-4') DRO pattern unknown.
QB13011-013 SB-43 (4'-6') DRO resemble an oil pattern.
QB13011-014 SB-54 DRO pattern unknown.
The DRO pattern in the MB does not resemble the pattern in any of the sample samples.
Page: 2 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terracon Consultants, Inc.
Lot Number: QB13011

Sample Number Sample ID Matrix Date Sampled Date Received
001 02/12/2015 0932SB-40 (4'-6')Solid 02/13/2015
002 02/12/2015 0941SB-41 (6'-8')Solid 02/13/2015
003 02/12/2015 1018SB-36 (2'-4')Solid 02/13/2015
004 02/12/2015 1057SB-39 (4'-6')Solid 02/13/2015
005 02/12/2015 1118SB-34 (0'-2')Solid 02/13/2015
006 02/12/2015 1135SB-35 (2'-4')Solid 02/13/2015
007 02/12/2015 1310SB-44 (2'-4')Solid 02/13/2015
008 02/12/2015 1336SB-50 (10'-12')Solid
009 02/12/2015 1404SB-52 (8'-10')Solid 02/13/2015
010 02/12/2015 1419SB-53 (10'-12')Solid 02/13/2015
011 02/12/2015 1508SB-47 (8'-10')Solid 02/13/2015
012 02/12/2015 1543SB-49 (2'-4')Solid 02/13/2015
013 02/12/2015 1606SB-43 (4'-6')Solid 02/13/2015
014 02/12/2015Trip Blank (1 per cooler)Aqueous 02/13/2015
015 02/12/2015 1447SB-54 Solid 02/13/2015
(15 samples)
Page: 3 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Terracon Consultants, Inc.
Lot Number: QB13011

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SB-40 (4'-6')Solid Acetone 8260B 5.8 BJ ug/kg 5
002 SB-41 (6'-8')Solid Acetone 8260B 78 B ug/kg 7
003 SB-36 (2'-4')Solid TPH-DRO 8015C 6100 BJ ug/kg 9
004 SB-39 (4'-6')Solid TPH-DRO 8015C 2700 BJ ug/kg 10
005 SB-34 (0'-2')Solid HEM (oil and grease)9071B 430 mg/kg 11
005 SB-34 (0'-2')Solid Acetone 8260B 42 B ug/kg 12
005 SB-34 (0'-2')Solid Ethylbenzene 8260B 2.7 J ug/kg 12
005 SB-34 (0'-2')Solid Isopropylbenzene 8260B 21 ug/kg 12
005 SB-34 (0'-2')Solid Methylcyclohexane 8260B 1.5 J ug/kg 12
005 SB-34 (0'-2')Solid Xylenes (total)8260B 8.1 ug/kg 13
005 SB-34 (0'-2')Solid TPH-DRO 8015C 730000 B ug/kg 14
006 SB-35 (2'-4')Solid TPH-DRO 8015C 4700 BJ ug/kg 18
007 SB-44 (2'-4')Solid TPH-DRO 8015C 2300 BJ ug/kg 21
009 SB-52 (8'-10')Solid TPH-DRO 8015C 59000000 B ug/kg 23
010 SB-53 (10'-12')Solid HEM (oil and grease)9071B 500 mg/kg 24
010 SB-53 (10'-12')Solid TPH-DRO 8015C 390000 B ug/kg 25
011 SB-47 (8'-10')Solid TPH-DRO 8015C 95000 B ug/kg 26
012 SB-49 (2'-4')Solid TPH-DRO 8015C 87000 BJ ug/kg 28
012 SB-49 (2'-4')Solid TPH-GRO 8015C 21000 ug/kg 29
013 SB-43 (4'-6')Solid TPH-DRO 8015C 150000 B ug/kg 30
013 SB-43 (4'-6')Solid TPH-GRO 8015C 150000 ug/kg 31
015 SB-54 Solid TPH-DRO 8015C 6500 BJ ug/kg 33
(22 detections)
Page: 4 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-40 (4'-6')
QB13011-001
02/12/2015 0932
02/13/2015
Solid
% Solids:79.2 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1722 DCS 67933 5.82
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 5.8 BJ 1ug/kg5.522
Benzene 71-43-2 8260B ND 1ug/kg1.75.4
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.85.4
Bromoform 75-25-2 8260B ND 1ug/kg2.15.4
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.35.4
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.611
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.45.4
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.65.4
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.75.4
Chloroethane 75-00-3 8260B ND 1ug/kg2.65.4
Chloroform 67-66-3 8260B ND 1ug/kg1.65.4
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.25.4
Cyclohexane 110-82-7 8260B ND 1ug/kg1.95.4
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.35.4
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.95.4
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg1.95.4
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.85.4
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.85.4
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.65.4
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.05.4
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg1.65.4
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.75.4
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.05.4
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg1.75.4
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.65.4
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.65.4
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg1.65.4
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg1.65.4
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.85.4
2-Hexanone 591-78-6 8260B ND 1ug/kg4.111
Isopropylbenzene 98-82-8 8260B ND 1ug/kg1.75.4
Methyl acetate 79-20-9 8260B ND 1ug/kg1.15.4
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.435.4
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.611
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.445.4
Methylene chloride 75-09-2 8260B ND 1ug/kg2.85.4
Styrene 100-42-5 8260B ND 1ug/kg1.25.4
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.515.4
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.545.4
Toluene 108-88-3 8260B ND 1ug/kg1.85.4
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.685.4
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.85.4
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.925.4
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.865.4
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-40 (4'-6')
QB13011-001
02/12/2015 0932
02/13/2015
Solid
% Solids:79.2 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1722 DCS 67933 5.82
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.4
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.65.4
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.935.4
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.15.4
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 95 53-142
Bromofluorobenzene 93 47-138
Toluene-d8 96 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-41 (6'-8')
QB13011-002
02/12/2015 0941
02/13/2015
Solid
% Solids:77.5 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1743 DCS 67933 5.80
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 78 B 1ug/kg5.622
Benzene 71-43-2 8260B ND 1ug/kg1.75.6
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.95.6
Bromoform 75-25-2 8260B ND 1ug/kg2.25.6
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.45.6
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.711
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.55.6
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.65.6
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.85.6
Chloroethane 75-00-3 8260B ND 1ug/kg2.65.6
Chloroform 67-66-3 8260B ND 1ug/kg1.75.6
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.25.6
Cyclohexane 110-82-7 8260B ND 1ug/kg1.95.6
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.35.6
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.95.6
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg1.95.6
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.95.6
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.95.6
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.75.6
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.15.6
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg1.65.6
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.85.6
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.05.6
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg1.85.6
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.75.6
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.75.6
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg1.75.6
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg1.75.6
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.85.6
2-Hexanone 591-78-6 8260B ND 1ug/kg4.211
Isopropylbenzene 98-82-8 8260B ND 1ug/kg1.75.6
Methyl acetate 79-20-9 8260B ND 1ug/kg1.15.6
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.445.6
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.711
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.465.6
Methylene chloride 75-09-2 8260B ND 1ug/kg2.95.6
Styrene 100-42-5 8260B ND 1ug/kg1.25.6
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.525.6
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.565.6
Toluene 108-88-3 8260B ND 1ug/kg1.95.6
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.705.6
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.95.6
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.955.6
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.885.6
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-41 (6'-8')
QB13011-002
02/12/2015 0941
02/13/2015
Solid
% Solids:77.5 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1743 DCS 67933 5.80
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.6
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.75.6
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.965.6
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.25.6
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 53-142
Bromofluorobenzene 94 47-138
Toluene-d8 96 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 53
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-36 (2'-4')
QB13011-003
02/12/2015 1018
02/13/2015
Solid
% Solids:91.6 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0223 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 6100 BJ 1ug/kg13007300
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 81 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-39 (4'-6')
QB13011-004
02/12/2015 1057
02/13/2015
Solid
% Solids:87.2 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0244 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 2700 BJ 1ug/kg14007700
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 83 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 53
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-34 (0'-2')
QB13011-005
02/12/2015 1118
02/13/2015
Solid
% Solids:81.3 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B 430 1mg/kg210250
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-34 (0'-2')
QB13011-005
02/12/2015 1118
02/13/2015
Solid
% Solids:81.3 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1805 DCS 67933 6.40
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 42 B 1ug/kg4.919
Benzene 71-43-2 8260B ND 1ug/kg1.54.8
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.64.8
Bromoform 75-25-2 8260B ND 1ug/kg1.94.8
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.14.8
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.19.6
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.34.8
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.44.8
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.54.8
Chloroethane 75-00-3 8260B ND 1ug/kg2.34.8
Chloroform 67-66-3 8260B ND 1ug/kg1.44.8
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.94.8
Cyclohexane 110-82-7 8260B ND 1ug/kg1.74.8
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.04.8
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.64.8
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg1.64.8
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.64.8
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.64.8
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.44.8
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg3.64.8
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg1.44.8
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.54.8
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.74.8
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg1.54.8
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.54.8
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.44.8
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg1.44.8
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg1.54.8
Ethylbenzene 100-41-4 8260B 2.7 J 1ug/kg1.64.8
2-Hexanone 591-78-6 8260B ND 1ug/kg3.69.6
Isopropylbenzene 98-82-8 8260B 21 1ug/kg1.54.8
Methyl acetate 79-20-9 8260B ND 1ug/kg0.944.8
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.384.8
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.49.6
Methylcyclohexane 108-87-2 8260B 1.5 J 1ug/kg0.394.8
Methylene chloride 75-09-2 8260B ND 1ug/kg2.54.8
Styrene 100-42-5 8260B ND 1ug/kg1.14.8
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.454.8
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.484.8
Toluene 108-88-3 8260B ND 1ug/kg1.64.8
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.614.8
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.64.8
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.824.8
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.764.8
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-34 (0'-2')
QB13011-005
02/12/2015 1118
02/13/2015
Solid
% Solids:81.3 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1805 DCS 67933 6.40
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg1.84.8
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.44.8
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.834.8
Xylenes (total)1330-20-7 8260B 8.1 1ug/kg2.84.8
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 53-142
Bromofluorobenzene 94 47-138
Toluene-d8 98 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-34 (0'-2')
QB13011-005
02/12/2015 1118
02/13/2015
Solid
% Solids:81.3 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0305 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 730000 B 1ug/kg15008200
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 84 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-35 (2'-4')
QB13011-006
02/12/2015 1135
02/13/2015
Solid
% Solids:83.2 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg200240
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-35 (2'-4')
QB13011-006
02/12/2015 1135
02/13/2015
Solid
% Solids:83.2 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1826 DCS 67933 6.07
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg5.020
Benzene 71-43-2 8260B ND 1ug/kg1.54.9
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.74.9
Bromoform 75-25-2 8260B ND 1ug/kg1.94.9
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.14.9
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.29.9
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.34.9
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.44.9
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.64.9
Chloroethane 75-00-3 8260B ND 1ug/kg2.34.9
Chloroform 67-66-3 8260B ND 1ug/kg1.54.9
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.04.9
Cyclohexane 110-82-7 8260B ND 1ug/kg1.74.9
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.14.9
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.74.9
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg1.74.9
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.74.9
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.74.9
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.54.9
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg3.74.9
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg1.54.9
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.64.9
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.84.9
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg1.64.9
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.54.9
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.54.9
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg1.54.9
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg1.54.9
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.64.9
2-Hexanone 591-78-6 8260B ND 1ug/kg3.79.9
Isopropylbenzene 98-82-8 8260B ND 1ug/kg1.54.9
Methyl acetate 79-20-9 8260B ND 1ug/kg0.974.9
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.404.9
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.59.9
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.414.9
Methylene chloride 75-09-2 8260B ND 1ug/kg2.64.9
Styrene 100-42-5 8260B ND 1ug/kg1.14.9
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.474.9
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.494.9
Toluene 108-88-3 8260B ND 1ug/kg1.74.9
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.624.9
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.74.9
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.844.9
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.784.9
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-35 (2'-4')
QB13011-006
02/12/2015 1135
02/13/2015
Solid
% Solids:83.2 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1826 DCS 67933 6.07
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg1.94.9
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.54.9
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.854.9
Xylenes (total)1330-20-7 8260B ND 1ug/kg2.94.9
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 95 53-142
Bromofluorobenzene 94 47-138
Toluene-d8 94 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 17 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-35 (2'-4')
QB13011-006
02/12/2015 1135
02/13/2015
Solid
% Solids:83.2 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0326 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 4700 BJ 1ug/kg15008000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 84 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 18 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-44 (2'-4')
QB13011-007
02/12/2015 1310
02/13/2015
Solid
% Solids:74.1 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1847 DCS 67933 6.18
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg5.522
Benzene 71-43-2 8260B ND 1ug/kg1.75.5
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.85.5
Bromoform 75-25-2 8260B ND 1ug/kg2.25.5
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.45.5
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.611
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.55.5
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.65.5
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.85.5
Chloroethane 75-00-3 8260B ND 1ug/kg2.65.5
Chloroform 67-66-3 8260B ND 1ug/kg1.65.5
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.25.5
Cyclohexane 110-82-7 8260B ND 1ug/kg1.95.5
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.35.5
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.95.5
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg1.95.5
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.95.5
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.85.5
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.65.5
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.15.5
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg1.65.5
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.75.5
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.05.5
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg1.75.5
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.65.5
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.65.5
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg1.65.5
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg1.65.5
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.85.5
2-Hexanone 591-78-6 8260B ND 1ug/kg4.111
Isopropylbenzene 98-82-8 8260B ND 1ug/kg1.75.5
Methyl acetate 79-20-9 8260B ND 1ug/kg1.15.5
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.445.5
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.611
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.455.5
Methylene chloride 75-09-2 8260B ND 1ug/kg2.85.5
Styrene 100-42-5 8260B ND 1ug/kg1.25.5
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.515.5
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.555.5
Toluene 108-88-3 8260B ND 1ug/kg1.95.5
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.695.5
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.95.5
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.935.5
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.865.5
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 19 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-44 (2'-4')
QB13011-007
02/12/2015 1310
02/13/2015
Solid
% Solids:74.1 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/16/2015 1847 DCS 67933 6.18
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.5
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.65.5
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.945.5
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.25.5
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 53-142
Bromofluorobenzene 94 47-138
Toluene-d8 96 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 20 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-44 (2'-4')
QB13011-007
02/12/2015 1310
02/13/2015
Solid
% Solids:74.1 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0346 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 2300 BJ 1ug/kg16009000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 85 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 21 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-52 (8'-10')
QB13011-009
02/12/2015 1404
02/13/2015
Solid
% Solids:76.7 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg220260
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 22 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-52 (8'-10')
QB13011-009
02/12/2015 1404
02/13/2015
Solid
% Solids:76.7 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 5 02/17/2015 1056 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 59000000 B 1ug/kg77000420000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 89 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 23 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-53 (10'-12')
QB13011-010
02/12/2015 1419
02/13/2015
Solid
% Solids:89.5 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/14/2015 1120 JDW 67843
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B 500 1mg/kg190220
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 24 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-53 (10'-12')
QB13011-010
02/12/2015 1419
02/13/2015
Solid
% Solids:89.5 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0428 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 390000 B 1ug/kg1300072000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 82 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 25 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-47 (8'-10')
QB13011-011
02/12/2015 1508
02/13/2015
Solid
% Solids:75.9 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0449 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 95000 B 1ug/kg1600085000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 81 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 26 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - GRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-47 (8'-10')
QB13011-011
02/12/2015 1508
02/13/2015
Solid
% Solids:75.9 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8015C 1 02/16/2015 1652 DCS 67943
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-GRO 8015C ND 1ug/kg6805400
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 100 23-179
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 27 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-49 (2'-4')
QB13011-012
02/12/2015 1543
02/13/2015
Solid
% Solids:69.9 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0509 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 87000 BJ 1ug/kg1700093000
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 82 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 28 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - GRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-49 (2'-4')
QB13011-012
02/12/2015 1543
02/13/2015
Solid
% Solids:69.9 02/13/2015 1924
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8015C 1 02/16/2015 1716 DCS 67943
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-GRO 8015C 21000 1ug/kg6905500
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 153 23-179
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 29 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-43 (4'-6')
QB13011-013
02/12/2015 1606
02/13/2015
Solid
% Solids:80.0 02/14/2015 1140
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/17/2015 0530 MEM 02/14/2015 1210 67845
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 150000 B 1ug/kg15008300
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 82 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 30 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - GRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-43 (4'-6')
QB13011-013
02/12/2015 1606
02/13/2015
Solid
% Solids:80.0 02/14/2015 1140
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8015C 1 02/16/2015 1739 DCS 67943
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-GRO 8015C 150000 1ug/kg6505200
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 111 23-179
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 31 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-54
QB13011-015
02/12/2015 1447
02/13/2015
Solid
% Solids:89.1 02/17/2015 1730
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (HEM (oil and) 9071B 1 02/18/2015 1418 RPB 68112
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
HEM (oil and grease)9071B ND 1mg/kg190220
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 32 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
SB-54
QB13011-015
02/12/2015 1447
02/13/2015
Solid
% Solids:89.1 02/17/2015 1730
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 02/19/2015 0954 MEM 02/18/2015 1057 68083
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
TPH-DRO 8015C 6500 BJ 1ug/kg14007500
AcceptanceRun 1
Surrogate Q % Recovery Limits
o - Terphenyl 83 55-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 33 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
Page: 34 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - MB
Batch:
Sample ID:QQ67843-001
67843
Analytical Method:9071B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
HEM (oil and grease)ND 02/14/2015 1120200170mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 35 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - LCS
Batch:
Sample ID:QQ67843-002
67843
Analytical Method:9071B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
HEM (oil and grease)2200 02/14/2015 1120110200070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 36 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - MB
Batch:
Sample ID:QQ68112-001
68112
Analytical Method:9071B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
HEM (oil and grease)ND 02/18/2015 1418200170mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 37 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - LCS
Batch:
Sample ID:QQ68112-002
68112
Analytical Method:9071B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
HEM (oil and grease)2200 02/18/2015 1418110200070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 38 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - Duplicate
Batch:
Sample ID:QB13011-015DU
68112
Analytical Method:9071B
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)
HEM (oil and grease)ND 02/18/2015 14180.00 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 39 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - MS
Batch:
Sample ID:QB13011-015MS
68112
Analytical Method:9071B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
HEM (oil and grease)2200 02/18/2015 1418109200070-130ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 40 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ67933-001
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone 5.8 02/16/2015 1241J205.1 ug/kg1
Benzene ND 02/16/2015 12415.0 1.6 ug/kg1
Bromodichloromethane ND 02/16/2015 12415.0 1.7 ug/kg1
Bromoform ND 02/16/2015 12415.0 2.0 ug/kg1
Bromomethane (Methyl bromide)ND 02/16/2015 12415.0 2.2 ug/kg1
2-Butanone (MEK)ND 02/16/2015 1241104.2 ug/kg1
Carbon disulfide ND 02/16/2015 12415.0 1.3 ug/kg1
Carbon tetrachloride ND 02/16/2015 12415.0 1.4 ug/kg1
Chlorobenzene ND 02/16/2015 12415.0 1.6 ug/kg1
Chloroethane ND 02/16/2015 12415.0 2.4 ug/kg1
Chloroform ND 02/16/2015 12415.0 1.5 ug/kg1
Chloromethane (Methyl chloride)ND 02/16/2015 12415.0 2.0 ug/kg1
Cyclohexane ND 02/16/2015 12415.0 1.7 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 02/16/2015 12415.0 2.1 ug/kg1
Dibromochloromethane ND 02/16/2015 12415.0 1.7 ug/kg1
1,2-Dibromoethane (EDB)ND 02/16/2015 12415.0 1.7 ug/kg1
1,4-Dichlorobenzene ND 02/16/2015 12415.0 1.5 ug/kg1
1,2-Dichlorobenzene ND 02/16/2015 12415.0 1.7 ug/kg1
1,3-Dichlorobenzene ND 02/16/2015 12415.0 1.7 ug/kg1
Dichlorodifluoromethane ND 02/16/2015 12415.0 3.7 ug/kg1
1,2-Dichloroethane ND 02/16/2015 12415.0 1.6 ug/kg1
1,1-Dichloroethane ND 02/16/2015 12415.0 1.5 ug/kg1
trans-1,2-Dichloroethene ND 02/16/2015 12415.0 1.5 ug/kg1
cis-1,2-Dichloroethene ND 02/16/2015 12415.0 1.6 ug/kg1
1,1-Dichloroethene ND 02/16/2015 12415.0 1.8 ug/kg1
1,2-Dichloropropane ND 02/16/2015 12415.0 1.5 ug/kg1
trans-1,3-Dichloropropene ND 02/16/2015 12415.0 1.5 ug/kg1
cis-1,3-Dichloropropene ND 02/16/2015 12415.0 1.5 ug/kg1
Ethylbenzene ND 02/16/2015 12415.0 1.6 ug/kg1
2-Hexanone ND 02/16/2015 1241103.8 ug/kg1
Isopropylbenzene ND 02/16/2015 12415.0 1.5 ug/kg1
Methyl acetate ND 02/16/2015 12415.0 0.98 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 02/16/2015 12415.0 0.40 ug/kg1
4-Methyl-2-pentanone ND 02/16/2015 1241101.5 ug/kg1
Methylcyclohexane ND 02/16/2015 12415.0 0.41 ug/kg1
Methylene chloride ND 02/16/2015 12415.0 2.6 ug/kg1
Styrene ND 02/16/2015 12415.0 1.1 ug/kg1
1,1,2,2-Tetrachloroethane ND 02/16/2015 12415.0 0.47 ug/kg1
Tetrachloroethene ND 02/16/2015 12415.0 0.50 ug/kg1
Toluene ND 02/16/2015 12415.0 1.7 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 02/16/2015 12415.0 0.63 ug/kg1
1,2,4-Trichlorobenzene ND 02/16/2015 12415.0 1.7 ug/kg1
1,1,2-Trichloroethane ND 02/16/2015 12415.0 0.79 ug/kg1
1,1,1-Trichloroethane ND 02/16/2015 12415.0 0.85 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 41 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ67933-001
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Trichloroethene ND 02/16/2015 12415.0 1.9 ug/kg1
Trichlorofluoromethane ND 02/16/2015 12415.0 1.5 ug/kg1
Vinyl chloride ND 02/16/2015 12415.0 0.86 ug/kg1
Xylenes (total)ND 02/16/2015 12415.0 2.9 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 93 47-138
1,2-Dichloroethane-d4 94 53-142
Toluene-d8 94 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 42 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ67933-002
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 100 02/16/2015 114410010060-1401
Benzene 46 02/16/2015 1144935069-1231
Bromodichloromethane 48 02/16/2015 1144965069-1211
Bromoform 48 02/16/2015 1144965061-1191
Bromomethane (Methyl bromide)56 02/16/2015 11441115010-1681
2-Butanone (MEK)94 02/16/2015 11449410057-1481
Carbon disulfide 45 02/16/2015 1144905058-1221
Carbon tetrachloride 48 02/16/2015 1144975058-1361
Chlorobenzene 47 02/16/2015 1144955059-1291
Chloroethane 55 02/16/2015 11441105042-1631
Chloroform 48 02/16/2015 1144955071-1251
Chloromethane (Methyl chloride)56 02/16/2015 11441115034-1341
Cyclohexane 46 02/16/2015 1144925053-1391
1,2-Dibromo-3-chloropropane (DBCP)47 02/16/2015 1144945055-1251
Dibromochloromethane 49 02/16/2015 1144975066-1191
1,2-Dibromoethane (EDB)47 02/16/2015 1144945074-1241
1,4-Dichlorobenzene 48 02/16/2015 1144965052-1331
1,2-Dichlorobenzene 48 02/16/2015 1144965057-1311
1,3-Dichlorobenzene 49 02/16/2015 1144975051-1341
Dichlorodifluoromethane 60 02/16/2015 11441195010-1571
1,2-Dichloroethane 46 02/16/2015 1144925067-1291
1,1-Dichloroethane 47 02/16/2015 1144945071-1271
trans-1,2-Dichloroethene 47 02/16/2015 1144945068-1311
cis-1,2-Dichloroethene 48 02/16/2015 1144965070-1221
1,1-Dichloroethene 46 02/16/2015 1144925069-1381
1,2-Dichloropropane 46 02/16/2015 1144935072-1241
trans-1,3-Dichloropropene 48 02/16/2015 1144955070-1241
cis-1,3-Dichloropropene 47 02/16/2015 1144955070-1261
Ethylbenzene 48 02/16/2015 1144965059-1281
2-Hexanone 91 02/16/2015 11449110054-1371
Isopropylbenzene 49 02/16/2015 1144985050-1361
Methyl acetate 49 02/16/2015 1144975059-1371
Methyl tertiary butyl ether (MTBE)46 02/16/2015 1144925070-1301
4-Methyl-2-pentanone 90 02/16/2015 11449010060-1341
Methylcyclohexane 47 02/16/2015 1144935041-1441
Methylene chloride 43 02/16/2015 1144865070-1301
Styrene 49 02/16/2015 1144975054-1361
1,1,2,2-Tetrachloroethane 47 02/16/2015 1144945069-1321
Tetrachloroethene 48 02/16/2015 1144965045-1501
Toluene 44 02/16/2015 1144885061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 46 02/16/2015 1144935049-1361
1,2,4-Trichlorobenzene 47 02/16/2015 1144955034-1451
1,1,2-Trichloroethane 46 02/16/2015 1144925055-1281
1,1,1-Trichloroethane 48 02/16/2015 1144975063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 43 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ67933-002
67933 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 47 02/16/2015 1144945062-1261
Trichlorofluoromethane 56 02/16/2015 11441125045-1381
Vinyl chloride 57 02/16/2015 11441145042-1321
Xylenes (total)95 02/16/2015 11449510058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 92 47-138
1,2-Dichloroethane-d4 85 53-142
Toluene-d8 94 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 44 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO - MB
Batch:Prep Method:
Prep Date:
Sample ID:QQ67845-001
67845 3550C
02/14/2015 1210Analytical Method:8015C
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
TPH-DRO 2700 02/16/2015 2214J67001200ug/kg1
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 85 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 45 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO - LCS
Batch:Prep Method:
Prep Date:
Sample ID:QQ67845-002
67845 3550C
02/14/2015 1210Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
TPH-DRO 71000 02/16/2015 2234858300070-1301
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 82 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 46 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO - MB
Batch:Prep Method:
Prep Date:
Sample ID:QQ68083-001
68083 3550C
02/18/2015 1057Analytical Method:8015C
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
TPH-DRO 1400 02/19/2015 0912J67001200ug/kg1
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 83 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 47 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO - LCS
Batch:Prep Method:
Prep Date:
Sample ID:QQ68083-002
68083 3550C
02/18/2015 1057Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
TPH-DRO 74000 02/19/2015 0933888300070-1301
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 85 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 48 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO - MS
Batch:Prep Method:
Prep Date:
Sample ID:QB13011-015MS
68083 3550C
02/18/2015 1057Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
TPH-DRO 77000 02/19/2015 1014769400070-13065001
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 83 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 49 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - DRO - MSD
Batch:Prep Method:
Prep Date:
Sample ID:QB13011-015MD
68083 3550C
02/18/2015 1057Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
TPH-DRO 80000 02/19/2015 1035799400070-1303.7 2065001
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl 84 55-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 50 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - GRO - MB
Batch:Prep Method:
Sample ID:QQ67943-001
67943 5030B
Analytical Method:8015C
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
TPH-GRO ND 02/16/2015 16045000630ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 118 23-179
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 51 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - GRO - LCS
Batch:Prep Method:
Sample ID:QQ67943-002
67943 5030B
Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
TPH-GRO 64000 02/16/2015 15161275000070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 111 23-179
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 52 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
TPH - GRO - LCSD
Batch:Prep Method:
Sample ID:QQ67943-003
67943 5030B
Analytical Method:8015C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
TPH-GRO 59000 02/16/2015 15391185000070-1307.2 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 109 23-179
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 53 of 53
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1