24007_Wrights Executive Sales II_5th Water Sampling Event Letter Report_20230103

ECS SOUTHEAST, LLP "Setting the Standard for Service"
Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F NC Registered Geologists Firm C-553-553
SC Registered Engineering Firm 3239
January 3, 2023
Ms. Holly Samaha-Smith
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Reference: Water Sampling Letter Report — 5th Sampling Event
Wright's Executive Sales II
721 and 723 Rigsbee Avenue; 620 and 616 Foster Street
Durham, Durham County, North Carolina
Brownfields Project No. 24007-20-032
ECS Project No. 49-10039-B
Dear Ms. Samaha-Smith:
ECS Southeast, LLP (ECS) is pleased to present the results of water sampling conducted in support of
ongoing Brownfield redevelopment activity at the above -referenced site (Figures 1 and 2). ECS's water
sampling services were provided in accordance with the North Carolina Department of Environmental
Quality (NCDEQ) Division of Waste Management (DWM) Brownfields Program (the Program) June 7,
2022 approved Environmental Management Plan (EMP). Included in this report is a description of the field
activities, and the results obtained.
On December 16, 2022, ECS mobilized to the subject site to collect one (1) water sample, identified as
WS-5. The water sample was collected from an onsite 8,400-gallon FRAC tank utilizing new powder free
nitrile gloves and a new dedicated disposable polyethylene bailer. The location of the FRAC tank is
illustrated on Figure 3. Water in the FRAC tank was circulated with pumps and hosing just prior to the
sampling event in order to provide for a representative water quality sample from the FRAC tank. The
FRAC tank, was observed to be near 100% capacity at the time of sampling on December 16, 2022. The
water contained in the FRAC tank was generated from precipitation which had accumulated in various
open excavations on the Brownfields site and was not reinfiltrating at a rate which supported ongoing
redevelopment activities in those areas.
Following collection, the water sample, identified as WS-5, was submitted to Pace Analytical Services,
Inc., a North Carolina certified laboratory located in Huntersville, NC (NC Certification No. 12) for
analysis of volatile organic compounds (VOCs) using EPA Method 8260 and semi -volatile organic
compounds (SVOCs) using EPA Method 8270. ECS maintained chain of custody (COC) procedures
throughout the sample collection and transportation process.
Laboratory analysis of WS-5 did not report targeted VOCs or SVOCs at concentrations above their
respective laboratory method detection limits (MDLs). The laboratory analytical reports and a copy of
the COC documentation are included as attachments.
ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Southwest, LLP
www.ecslimited.com

Water Sampling Letter Report
Wrights Executive Sales 11
Brownfield Project No. 24007-20-032
ECS Project No. 49-10039-B
Based on this summary report's findings, ECS concluded that the laboratory analytical results of the
water sample collected on December 16, 2022, and identified as WS-5, did not report targeted
compounds above their respective North Carolina Administrative Code (NCAC) 213 Surface Water
Standards. Therefore, based upon these results and in accordance with the Brownfields approved EMP,
ECS recommended this water be managed on the site or discharged to the storm sewer in accordance
with municipal, state, and federal requirements.
ECS appreciates the opportunity to work with the Brownfields Program. If you have any questions
concerning this report or this project, please contact us.
Sincerely,
ECS SOUTHEAST,
ftoin- Nil. N rro, P.G.
Staff Project Manager
NC License No. 2832
[e-mail]
[phone]
Scott M. Werley, W.G.
Principal Geologist
NC License No. 2354
[e-mail]
[phone]
Attachments — Figures 1-3
Photo Documentation
Laboratory Analytical Reports and Chain of Custody
Cc: Mr. John Sunter, GeerHouse Owner, LLC, c/o [e-mail]
2

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SOURCE: N FIGURE 1
USGS TOPOGRAPHIC MAP wF SITE TOPOGRAPHIC LOCATION MAP
7.5 — MINUTE SERIES s
NORTHWEST DURHAM, NC (TOP) + Wright's Executive Sales
SOUTHWEST DURHAM, NC (BOTTOM) Brownfields Project Number 24007-20-032
DATED: 2019 721 & 723 Rigsbee Ave; 620 & 616 Foster St.
SCALE: 1 : 24,000 Durham, Durham County, North Carolina
CONTOUR INVERVAL = 10' TM ECS Project Number: 49-10039-B

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N FIGURE 2
SOURCE: F SITE FEATURES MAP
ECS Southeast, LLP s
Phase I ESA, December 6, 2019 Wright's Executive Sales
Brownfields Project Number 24007-20-032
APPROXIMATE SCALE: JEE 721 & 723 Rigsbee Ave; 620 & 616 Foster St.
100 FT. Durham, Durham County, North Carolina
TM ECS Project Number: 49-10039-B

P14
4
h
4
` FRAC Tank
[" f
SOURCE: FIGURE 3
ECS Southeast, LLP W�E FRAC TANK LOCATION MAP
Phase I ESA, December 6, 2019 S
Report of Environmental Assessment Rev.0.0, Wright's Executive Sales
December 18, 2020 Brownfields Project Number 24007-20-032
721 & 723 Rigsbee Ave; 620 & 616 Foster St.
APPROXIMATE SCALE: Durham, Durham County, North Carolina
50 FT. TM ECS Project Number: 49-10039-B

Photo 1— View of the FRAC tank used to pump precipitation accumulated in open excavations/trenches across
the subject property.
Photo 2 — View of the interior of the FRAC tank at the time of the second sampling event on December 16,
2022.
Wright's Executive Sales
Photo Documentation Brownfields Project Number 24007-20-032
9i 721 & 723 Rigsbee Ave; 620 & 616 Foster St.
Durham, Durham County, North Carolina
ECS Project Number: 49-10039-B

yv9
ff �; y
�
�
f
Photo 3 - Additional
view of the FRAC tank used to pump precipitation accumulated in open
excavations/trenches
across the subject property.
SABRE MFG., LLC
--,rements taken from the top mapwsw
5420 phoneE a 888 7r1 5580 46534 "
InrPtIon @ Center Une of Tank
t 98.8 3.q
2 197.6 4.7
3 2%.4 7.1
9 396.2 9.4
5 g94.0 11.8
6 592.8 14.1
) 691.7 l6.5
8 T90.5 18.8
9 889.3 31.2
t0 988.1 23.E
tt 1086.9 III25.9
12 1185.] 38.3
13 1284.5 30.E
IIIIIIIIIEMM1111IM11J6
15Orr"11111IM111
t6 1580.9 31.E
t) I6)9.] Q0.0
t8 1]78.6 42.3
19 IB]7.3 44.]
30 19)6.1 4).1
31 2075.0 49.4
22 3l)3.8 .51.8
33 32T2.6
24 2371A
25 24]0.2 56.6
26 I569.0 61.3
3) 366].8 63.5
38 2766.E 65.9
29 2865.4 68.3
JO 2964.I T1.6
31 3%3.0 72.9
32 3161.8 75.3
3J 3260.E 7].6
34 3369.5 80.0
JS 3458.3 82.3
356].1 eb.7
J) 3655.9 8/.0
38 3)Sq.) 69A
39 3853.E 91.)
40 3952.3 94.1
41 g06L1 %.5
43 d149.9 98.8
43 0248.] 101.3
44 434].:. ' 103,5
.3 IS).6
.9 1600
4) 4 69 6811.] � 362.3
48 4742.8 112.9 ]0 6916.5 164.]
49 484L6 119.3 ]t ]OI83 161.0
50 0940.0 117.E )2 ]114.1 169A
51 60392 1I0.0 )] 731i.9 1]i.]
52 5138.0 122.3 ]4 I311] I]4.1
53 5236.8 124.] ]5 ]430.6 1)6A
Sd 6335.E 12'7.0 )6 )509.4 1)H.8
55 5434.4 129.4 ]) ]608.2 1BL1
56 6533.2 131.] ]8 TS07.0 183.5
5) %3I.0 134.1 ]9 )806.8 186.9
68 5]30.8 136.0 80 ]904.6 188.2
59 5829.E 138.8 81 800
60 5938.4 141.2 62 8l
61 603).2 343.5 MEW
Mlllrmww145.9 Bd 839 .
6J 6224.9 L18,2 85 398.E
6q 6323.) 150.E 9 .q
66 6423.E 153.9
66 6621.3 155.3
Photo 4 - View of the FRAC tank measurement chart located on the side of the FRAC tank.
Wright's Executive Sales
Photo Documentation
Brownfields Project Number 24007-20-032
9S
721 & 723 Rigsbee Ave; 620 & 616 Foster St.
Durham, Durham County, North Carolina
ECS Project Number: 49-10039-B

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 23, 2022
Ron Navarro
ECS Raleigh
5260 Greens Dairy Road
Raleigh, NC 27616
RE: Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
Dear Ron Navarro:
Enclosed are the analytical results for sample(s) received by the laboratory on December 17, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
This revision was issued on 12/23/22 to turn on J-Flags and report results to the MDL per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard for
Sara Poulson
[e-mail]
[phone]
Project Manager
Enclosures
cc: ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 24

lacmnalyfica('
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 24

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
Lab ID Sample ID Matrix Date Collected Date Received
92642813001 WS-5 Water 12/16/22 09:30 12/17/22 10:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 24

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92642813001 WS-5 EPA 8270E PKS 74 PASI-C
EPA 8260D SAS 63 PASI-C
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 24

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
Sample: WS-5
Lab ID:
92642813001
Collected:
12/16/22
09:30
Received: 12/17/22 10:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8270E RVE
Analytical
Method: EPA 8270E
Preparation Method: EPA 3510C
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/L
8.3
1.7
1
12/21/22 15:10
12/22/22 10:35
83-32-9
Acenaphthylene
ND
ug/L
8.3
1.6
1
12/21/22 15:10
12/22/22 10:35
208-96-8
Aniline
ND
ug/L
8.3
1.4
1
12/21/22 15:10
12/22/22 10:35
62-53-3
Anthracene
ND
ug/L
8.3
1.9
1
12/21/22 15:10
12/22/22 10:35
120-12-7
Benzo(a)anthracene
ND
ug/L
8.3
2.2
1
12/21/22 15:10
12/22/22 10:35
56-55-3
Benzo(a)pyrene
ND
ug/L
8.3
2.3
1
12/21/22 15:10
12/22/22 10:35
50-32-8
Benzo(b)fluoranthene
ND
ug/L
8.3
2.2
1
12/21/22 15:10
12/22/22 10:35
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
8.3
2.4
1
12/21/22 15:10
12/22/22 10:35
191-24-2
Benzo(k)fluoranthene
ND
ug/L
8.3
2.3
1
12/21/22 15:10
12/22/22 10:35
207-08-9
Benzoic Acid
ND
ug/L
41.7
18.3
1
12/21/22 15:10
12/22/22 10:35
65-85-0
Benzyl alcohol
ND
ug/L
16.7
2.4
1
12/21/22 15:10
12/22/22 10:35
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
8.3
1.5
1
12/21/22 15:10
12/22/22 10:35
101-55-3
Butylbenzylphthalate
ND
ug/L
8.3
2.6
1
12/21/22 15:10
12/22/22 10:35
85-68-7
v1
4-Chloro-3-methyl phenol
ND
ug/L
8.3
2.8
1
12/21/22 15:10
12/22/22 10:35
59-50-7
4-Chloroaniline
ND
ug/L
16.7
3.0
1
12/21/22 15:10
12/22/22 10:35
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
8.3
1.5
1
12/21/22 15:10
12/22/22 10:35
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
8.3
1.6
1
12/21/22 15:10
12/22/22 10:35
111-44-4
2-Chloronaphthalene
ND
ug/L
8.3
1.4
1
12/21/22 15:10
12/22/22 10:35
91-58-7
2-Chlorophenol
ND
ug/L
8.3
1.0
1
12/21/22 15:10
12/22/22 10:35
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
8.3
1.7
1
12/21/22 15:10
12/22/22 10:35
7005-72-3
Chrysene
ND
ug/L
8.3
2.3
1
12/21/22 15:10
12/22/22 10:35
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
8.3
2.5
1
12/21/22 15:10
12/22/22 10:35
53-70-3
Dibenzofuran
ND
ug/L
8.3
1.8
1
12/21/22 15:10
12/22/22 10:35
132-64-9
1,2-Dichlorobenzene
ND
ug/L
8.3
1.5
1
12/21/22 15:10
12/22/22 10:35
95-50-1
1,3-Dichlorobenzene
ND
ug/L
8.3
1.3
1
12/21/22 15:10
12/22/22 10:35
541-73-1
M1
1,4-Dichlorobenzene
ND
ug/L
8.3
1.4
1
12/21/22 15:10
12/22/22 10:35
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
16.7
6.8
1
12/21/22 15:10
12/22/22 10:35
91-94-1
2,4-Dichlorophenol
ND
ug/L
8.3
1.2
1
12/21/22 15:10
12/22/22 10:35
120-83-2
Diethylphthalate
ND
ug/L
8.3
1.7
1
12/21/22 15:10
12/22/22 10:35
84-66-2
2,4-Dimethylphenol
ND
ug/L
8.3
1.4
1
12/21/22 15:10
12/22/22 10:35
105-67-9
Dimethylphthalate
ND
ug/L
8.3
1.8
1
12/21/22 15:10
12/22/22 10:35
131-11-3
Di-n-butylphthalate
ND
ug/L
8.3
1.8
1
12/21/22 15:10
12/22/22 10:35
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
16.7
6.5
1
12/21/22 15:10
12/22/22 10:35
534-52-1
2,4-Dinitrophenol
ND
ug/L
41.7
21.7
1
12/21/22 15:10
12/22/22 10:35
51-28-5
2,4-Dinitrotoluene
ND
ug/L
8.3
1.4
1
12/21/22 15:10
12/22/22 10:35
121-14-2
2,6-Dinitrotoluene
ND
ug/L
8.3
1.4
1
12/21/22 15:10
12/22/22 10:35
606-20-2
Di-n-octylphthalate
ND
ug/L
8.3
3.3
1
12/21/22 15:10
12/22/22 10:35
117-84-0
v1
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
3.1
1
12/21/22 15:10
12/22/22 10:35
117-81-7
Fluoranthene
ND
ug/L
8.3
1.8
1
12/21/22 15:10
12/22/22 10:35
206-44-0
Fluorene
ND
ug/L
8.3
1.7
1
12/21/22 15:10
12/22/22 10:35
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
8.3
1.5
1
12/21/22 15:10
12/22/22 10:35
87-68-3
Hexachlorobenzene
ND
ug/L
8.3
1.8
1
12/21/22 15:10
12/22/22 10:35
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.3
1.3
1
12/21/22 15:10
12/22/22 10:35
77-47-4
Hexachloroethane
ND
ug/L
8.3
1.2
1
12/21/22 15:10
12/22/22 10:35
67-72-1
M1
Indeno(1,2,3-cd)pyrene
ND
ug/L
8.3
2.4
1
12/21/22 15:10
12/22/22 10:35
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 24

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[phone]
ANALYTICAL RESULTS
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
Sample: WS-5 Lab ID: 92642813001 Collected: 12/16/22 09:30 Received: 12/17/22 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Date: 12/23/2022 11:04 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services
- Charlotte
ND
ug/L
8.3
1.4
1
12/21/2215:10
12/22/22 10:35
78-59-1
ND
ug/L
8.3
1.7
1
12/21/2215:10
12/22/22 10:35
90-12-0
ND
ug/L
8.3
1.6
1
12/21 /22 15:10
12/22/22 10:35
91-57-6
ND
ug/L
8.3
1.6
1
12/21/2215:10
12/22/22 10:35
95-48-7
ND
ug/L
8.3
1.0
1
12/21/2215:10
12/22/22 10:35
15831-10-4
ND
ug/L
8.3
1.7
1
12/21 /22 15:10
12/22/22 10:35
91-20-3
ND
ug/L
16.7
2.5
1
12/21/2215:10
12/22/22 10:35
88-74-4
ND
ug/L
16.7
3.1
1
12/21/2215:10
12/22/22 10:35
99-09-2
ND
ug/L
16.7
4.2
1
12/21 /22 15:10
12/22/22 10:35
100-01-6
ND
ug/L
8.3
1.6
1
12/21/2215:10
12/22/22 10:35
98-95-3
ND
ug/L
8.3
1.2
1
12/21/2215:10
12/22/22 10:35
88-75-5
ND
ug/L
41.7
5.5
1
12/21/2215:10
12/22/22 10:35
100-02-7
ND
ug/L
8.3
1.6
1
12/21/2215:10
12/22/22 10:35
62-75-9
ND
ug/L
8.3
1.1
1
12/21 /22 15:10
12/22/22 10:35
621-64-7
ND
ug/L
8.3
2.5
1
12/21/2215:10
12/22/22 10:35
86-30-6
ND
ug/L
8.3
0.96
1
12/21/2215:10
12/22/22 10:35
108-60-1
ND
ug/L
16.7
3.1
1
12/21/2215:10
12/22/22 10:35
87-86-5
ND
ug/L
8.3
1.7
1
12/21 /22 15:10
12/22/22 10:35
85-01-8
ND
ug/L
8.3
1.1
1
12/21/2215:10
12/22/22 10:35
108-95-2
ND
ug/L
8.3
1.8
1
12/21/2215:10
12/22/22 10:35
129-00-0
ND
ug/L
8.3
1.4
1
12/21/2215:10
12/22/22 10:35
120-82-1
ND
ug/L
8.3
1.2
1
12/21/2215:10
12/22/22 10:35
95-95-4
ND
ug/L
8.3
1.3
1
12/21/2215:10
12/22/22 10:35
88-06-2
84
%
10-138
1
12/21 /22 15:10
12/22/22 10:35
4165-60-0
70
%
10-130
1
12/21/2215:10
12/22/22 10:35
321-60-8
118
%
19-191
1
12/21/2215:10
12/22/22 10:35
1718-51-0
52
%
10-130
1
12/21 /22 15:10
12/22/22 10:35
13127-88-3
63
%
10-130
1
12/21/2215:10
12/22/22 10:35
367-12-4
109
%
10-164
1
12/21 /22 15:10
12/22/22 10:35
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
5.1
1
12/20/2216:59
67-64-1
ND
ug/L
1.0
0.34
1
12/20/2216:59
71-43-2
ND
ug/L
1.0
0.29
1
12/20/2216:59
108-86-1
ND
ug/L
1.0
0.47
1
12/20/2216:59
74-97-5
ND
ug/L
1.0
0.31
1
12/20/2216:59
75-27-4
ND
ug/L
1.0
0.34
1
12/20/2216:59
75-25-2
ND
ug/L
2.0
1.7
1
12/20/2216:59
74-83-9
ND
ug/L
5.0
4.0
1
12/20/2216:59
78-93-3
ND
ug/L
1.0
0.33
1
12/20/2216:59
56-23-5
ND
ug/L
1.0
0.28
1
12/20/2216:59
108-90-7
ND
ug/L
1.0
0.65
1
12/20/2216:59
75-00-3
ND
ug/L
1.0
0.43
1
12/20/2216:59
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
R1
Page 6 of 24

leAnalyiical
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
Sample: WS-5 Lab ID: 92642813001 Collected: 12/16/22 09:30 Received: 12/17/22 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Chloromethane
ND
ug/L
1.0
0.54
1
12/20/22 16:59
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
0.32
1
12/20/22 16:59
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
0.32
1
12/20/22 16:59
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
12/20/22 16:59
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
12/20/22 16:59
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
12/20/22 16:59
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
12/20/22 16:59
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
12/20/22 16:59
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
0.34
1
12/20/22 16:59
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
12/20/22 16:59
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
0.35
1
12/20/22 16:59
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
12/20/22 16:59
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
12/20/22 16:59
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
12/20/22 16:59
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.38
1
12/20/22 16:59
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
12/20/22 16:59
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.36
1
12/20/22 16:59
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
0.28
1
12/20/22 16:59
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
0.39
1
12/20/22 16:59
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
0.43
1
12/20/22 16:59
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
12/20/22 16:59
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
12/20/22 16:59
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
0.31
1
12/20/22 16:59
108-20-3
Ethylbenzene
ND
ug/L
1.0
0.30
1
12/20/22 16:59
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1.5
1
12/20/22 16:59
87-68-3
2-Hexanone
ND
ug/L
5.0
0.48
1
12/20/22 16:59
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
0.41
1
12/20/22 16:59
99-87-6
Methylene Chloride
ND
ug/L
5.0
2.0
1
12/20/22 16:59
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
12/20/22 16:59
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
0.42
1
12/20/22 16:59
1634-04-4
Naphthalene
ND
ug/L
1.0
0.64
1
12/20/22 16:59
91-20-3
Styrene
ND
ug/L
1.0
0.29
1
12/20/22 16:59
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
12/20/22 16:59
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/20/22 16:59
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
12/20/22 16:59
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/20/22 16:59
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
0.81
1
12/20/22 16:59
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
0.64
1
12/20/22 16:59
120-82-1
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
12/20/22 16:59
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
12/20/22 16:59
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
12/20/22 16:59
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
12/20/22 16:59
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
12/20/22 16:59
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.3
1
12/20/22 16:59
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
12/20/22 16:59
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC.
Page 7 of 24

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
Sample: WS-5
Lab ID:
92642813001
Collected:
12/16/22 09:30
Received: 12/17/22 10:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Xylene (Total)
ND
ug/L
1.0
0.34
1
12/20/22 16:59
1330-20-7
m&p-Xylene
ND
ug/L
2.0
0.71
1
12/20/22 16:59
179601-23-1
o-Xylene
ND
ug/L
1.0
0.34
1
12/20/22 16:59
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
12/20/22 16:59
460-00-4
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
12/20/22 16:59
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
12/20/22 16:59
2037-26-5
Date: 12/23/2022 11:04 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 24

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
QC Batch: 744460 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92642813001
METHOD BLANK: 3873100
Associated Lab Samples: 92642813001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
12/20/22 13:27
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
12/20/22 13:27
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
12/20/22 13:27
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
12/20/22 13:27
1,1-Dichloroethane
ug/L
ND
1.0
0.37
12/20/22 13:27
1,1-Dichloroethene
ug/L
ND
1.0
0.35
12/20/22 13:27
1,1-Dichloropropene
ug/L
ND
1.0
0.43
12/20/22 13:27
1,2,3-Trichlorobenzene
ug/L
ND
1.0
0.81
12/20/22 13:27
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
12/20/22 13:27
1,2,4-Trichlorobenzene
ug/L
ND
1.0
0.64
12/20/22 13:27
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
12/20/22 13:27
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
12/20/22 13:27
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
12/20/22 13:27
1,2-Dichloroethane
ug/L
ND
1.0
0.32
12/20/22 13:27
1,2-Dichloropropane
ug/L
ND
1.0
0.36
12/20/22 13:27
1,3-Dichlorobenzene
ug/L
ND
1.0
0.34
12/20/22 13:27
1,3-Dichloropropane
ug/L
ND
1.0
0.28
12/20/22 13:27
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
12/20/22 13:27
2,2-Dichloropropane
ug/L
ND
1.0
0.39
12/20/22 13:27
2-Butanone (MEK)
ug/L
ND
5.0
4.0
12/20/22 13:27
2-Chlorotoluene
ug/L
ND
1.0
0.32
12/20/22 13:27
2-Hexanone
ug/L
ND
5.0
0.48
12/20/22 13:27
4-Chlorotoluene
ug/L
ND
1.0
0.32
12/20/22 13:27
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
12/20/22 13:27
Acetone
ug/L
ND
25.0
5.1
12/20/22 13:27
Benzene
ug/L
ND
1.0
0.34
12/20/22 13:27
Bromobenzene
ug/L
ND
1.0
0.29
12/20/22 13:27
Bromochloromethane
ug/L
ND
1.0
0.47
12/20/22 13:27
Bromodichloromethane
ug/L
ND
1.0
0.31
12/20/22 13:27
Bromoform
ug/L
ND
1.0
0.34
12/20/22 13:27
Bromomethane
ug/L
ND
2.0
1.7
12/20/22 13:27
Carbon tetrachloride
ug/L
ND
1.0
0.33
12/20/22 13:27
Chlorobenzene
ug/L
ND
1.0
0.28
12/20/22 13:27
Chloroethane
ug/L
ND
1.0
0.65
12/20/22 13:27
Chloroform
ug/L
ND
1.0
0.43
12/20/22 13:27
Chloromethane
ug/L
ND
1.0
0.54
12/20/22 13:27
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
12/20/22 13:27
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
12/20/22 13:27
Dibromochloromethane
ug/L
ND
1.0
0.36
12/20/22 13:27
Dibromomethane
ug/L
ND
1.0
0.39
12/20/22 13:27
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC.
Page 9 of 24

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
METHOD BLANK: 3873100
Associated Lab Samples: 92642813001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
Dichlorodifluoromethane
ug/L
ND
1.0
0.35
12/20/22 13:27
Diisopropyl ether
ug/L
ND
1.0
0.31
12/20/22 13:27
Ethylbenzene
ug/L
ND
1.0
0.30
12/20/22 13:27
Hexachloro-1,3-butadiene
ug/L
ND
2.0
1.5
12/20/22 13:27
m&p-Xylene
ug/L
ND
2.0
0.71
12/20/22 13:27
Methyl-tert-butyl ether
ug/L
ND
1.0
0.42
12/20/22 13:27
Methylene Chloride
ug/L
ND
5.0
2.0
12/20/22 13:27
Naphthalene
ug/L
ND
1.0
0.64
12/20/22 13:27
o-Xylene
ug/L
ND
1.0
0.34
12/20/22 13:27
p-Isopropyltoluene
ug/L
ND
1.0
0.41
12/20/22 13:27
Styrene
ug/L
ND
1.0
0.29
12/20/22 13:27
Tetrachloroethene
ug/L
ND
1.0
0.29
12/20/22 13:27
Toluene
ug/L
ND
1.0
0.24
12/20/22 13:27
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
12/20/22 13:27
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
12/20/22 13:27
Trichloroethene
ug/L
ND
1.0
0.38
12/20/22 13:27
Trichlorofluoromethane
ug/L
ND
1.0
0.30
12/20/22 13:27
Vinyl acetate
ug/L
ND
2.0
1.3
12/20/22 13:27
Vinyl chloride
ug/L
ND
1.0
0.39
12/20/22 13:27
Xylene (Total)
ug/L
ND
1.0
0.34
12/20/22 13:27
1,2-Dichloroethane-d4 (S)
%
101
70-130
12/20/22 13:27
4-Bromofluorobenzene (S)
%
103
70-130
12/20/22 13:27
Toluene-d8 (S)
%
103
70-130
12/20/22 13:27
LABORATORY CONTROL SAMPLE:
3873101
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
46.8
94
70-130
1,1,1-Trichloroethane
ug/L
50
46.9
94
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
46.1
92
70-130
1,1,2-Trichloroethane
ug/L
50
48.0
96
70-130
1,1-Dichloroethane
ug/L
50
46.1
92
70-130
1,1-Dichloroethene
ug/L
50
46.3
93
70-130
1,1-Dichloropropene
ug/L
50
50.0
100
70-130
1,2,3-Trichlorobenzene
ug/L
50
46.7
93
70-130
1,2,3-Trichloropropane
ug/L
50
44.6
89
70-130
1,2,4-Trichlorobenzene
ug/L
50
45.8
92
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
45.4
91
70-131
1,2-Dibromoethane (EDB)
ug/L
50
46.3
93
70-130
1,2-Dichlorobenzene
ug/L
50
45.1
90
70-130
1,2-Dichloroethane
ug/L
50
48.3
97
70-130
1,2-Dichloropropane
ug/L
50
47.9
96
70-130
1,3-Dichlorobenzene
ug/L
50
45.5
91
70-130
1,3-Dichloropropane
ug/L
50
45.8
92
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 24

leAnalyiical
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
LABORATORY CONTROL SAMPLE:
Parameter
3873101
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,4-Dichlorobenzene
ug/L
50
44.7
89
70-130
2,2-Dichloropropane
ug/L
50
46.0
92
68-135
2-Butanone (MEK)
ug/L
100
102
102
70-134
2-Chlorotoluene
ug/L
50
44.5
89
70-130
2-Hexanone
ug/L
100
92.3
92
70-131
4-Chlorotoluene
ug/L
50
44.9
90
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
97.1
97
70-130
Acetone
ug/L
100
97.5
98
70-133
Benzene
ug/L
50
44.5
89
70-130
Bromobenzene
ug/L
50
45.0
90
70-130
Bromochloromethane
ug/L
50
49.4
99
70-130
Bromodichloromethane
ug/L
50
46.9
94
70-130
Bromoform
ug/L
50
44.4
89
70-130
Bromomethane
ug/L
50
38.9
78
45-151
Carbon tetrachloride
ug/L
50
45.0
90
70-130
Chlorobenzene
ug/L
50
45.3
91
70-130
Chloroethane
ug/L
50
46.7
93
39-152
Chloroform
ug/L
50
47.3
95
70-130
Chloromethane
ug/L
50
41.1
82
58-130
cis-1,2-Dichloroethene
ug/L
50
47.4
95
70-130
cis-1,3-Dichloropropene
ug/L
50
48.3
97
70-130
Dibromochloromethane
ug/L
50
45.1
90
70-130
Dibromomethane
ug/L
50
46.8
94
70-130
Dichlorodifluoromethane
ug/L
50
35.1
70
54-133
Diisopropyl ether
ug/L
50
47.3
95
70-130
Ethylbenzene
ug/L
50
44.5
89
70-130
Hexachloro-1,3-butadiene
ug/L
50
40.8
82
70-135
m&p-Xylene
ug/L
100
89.1
89
70-130
Methyl-tert-butyl ether
ug/L
50
48.5
97
70-130
Methylene Chloride
ug/L
50
43.7
87
66-130
Naphthalene
ug/L
50
48.8
98
70-130
o-Xylene
ug/L
50
44.9
90
70-130
p-Isopropyltoluene
ug/L
50
46.0
92
70-130
Styrene
ug/L
50
45.2
90
70-130
Tetrachloroethene
ug/L
50
42.8
86
70-130
Toluene
ug/L
50
45.1
90
70-130
trans-1,2-Dichloroethene
ug/L
50
47.5
95
70-130
trans- 1,3-Dichloropropene
ug/L
50
47.9
96
70-130
Trichloroethene
ug/L
50
47.9
96
70-130
Trichlorofluoromethane
ug/L
50
40.9
82
62-130
Vinyl acetate
ug/L
100
94.7
95
70-144
Vinyl chloride
ug/L
50
40.9
82
62-130
Xylene (Total)
ug/L
150
134
89
70-130
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8(S)
%
101
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 24

leAnalyiical
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Pace Analytical Services, LLC
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QUALITY CONTROL DATA
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3873102
MS
92642740002 Spike
Parameter Units Result Conc.
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1, 2,2-Tetrachloroethane
1,1, 2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2-Dibromo-3-
chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone
(MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
3873103
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits
ug/L
ND
500
500
572
570
114
114
70-141
ug/L
ND
500
500
653
637
131
127
70-150
ug/L
ND
500
500
582
571
116
114
69-142
ug/L
ND
500
500
632
608
126
122
70-138
ug/L
ND
500
500
634
600
127
120
70-150
ug/L
ND
500
500
641
601
128
120
70-156
ug/L
ND
500
500
693
670
139
134
70-150
ug/L
ND
500
500
540
563
108
113
70-148
ug/L
ND
500
500
586
541
117
108
70-140
ug/L
ND
500
500
530
553
106
111
70-146
ug/L
ND
500
500
537
548
107
110
68-146
Max
RPD RPD Qual
1 30
2 30
2 30
4 30
5 30
6 30
3 30
4 30
8 30
4 30
2 30
ug/L
ND
500
500
581
568
116
114
70-138
2
30
ug/L
ND
500
500
556
565
111
113
70-141
1
30
ug/L
ND
500
500
639
627
128
125
69-143
2
30
ug/L
ND
500
500
640
620
128
124
68-156
3
30
ug/L
ND
500
500
560
561
112
112
70-143
0
30
ug/L
ND
500
500
574
570
115
114
70-138
1
30
ug/L
ND
500
500
545
555
109
111
70-142
2
30
ug/L
ND
500
500
591
567
118
113
52-170
4
30
ug/L
ND
1000
1000
1220
1160
122
116
60-157
5
30
ug/L
ND
500
500
565
587
113
117
70-147
4
30
ug/L
ND
1000
1000
1120
1110
112
111
68-146
1
30
ug/L
ND
500
500
555
561
111
112
70-142
1
30
ug/L
ND
1000
1000
1230
1200
123
120
70-141
2
30
ug/L
ND
1000
1000
1200
1120
120
112
58-157
6
30
ug/L
4210
500
500
4720
5470
102
252
70-142
15
30 E,M1
ug/L
ND
500
500
556
565
111
113
70-143
2
30
ug/L
ND
500
500
666
642
133
128
70-146
4
30
ug/L
ND
500
500
618
599
124
120
70-139
3
30
ug/L
ND
500
500
538
527
108
105
64-140
2
30
ug/L
ND
500
500
429
448
86
90
28-192
4
30
ug/L
ND
500
500
628
620
126
124
70-148
1
30
ug/L
ND
500
500
585
585
117
117
70-141
0
30
ug/L
ND
500
500
658
611
132
122
58-191
7
30
ug/L
ND
500
500
640
620
128
124
70-148
3
30
ug/L
ND
500
500
500
474
100
95
43-162
5
30
ug/L
ND
500
500
636
617
127
123
68-151
3
30
ug/L
ND
500
500
620
604
124
121
70-139
3
30
ug/L
ND
500
500
555
556
111
111
70-144
0
30
ug/L
ND
500
500
619
595
124
119
70-139
4
30
ug/L
ND
500
500
348
327
70
65
39-171
6
30
ug/L
27.4
500
500
624
620
119
118
67-142
1
30
ug/L
2060
500
500
2550
2980
98
183
70-143
15
30 M1
ug/L
ND
500
500
494
512
99
102
64-163
4
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 24

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3873102
3873103
MS
MSD
92642740002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
m&p-Xylene
ug/L
3970
1000
1000
4950
5760
98
179
70-144
15
30 M1
Methyl-tert-butyl ether
ug/L
ND
500
500
625
617
122
120
65-143
1
30
Methylene Chloride
ug/L
ND
500
500
611
578
122
116
62-149
6
30
Naphthalene
ug/L
656
500
500
1130
1320
95
132
67-147
15
30
o-Xylene
ug/L
94.3
500
500
657
684
113
118
70-145
4
30
p-Isopropyltoluene
ug/L
ND
500
500
606
623
121
125
70-147
3
30
Styrene
ug/L
ND
500
500
565
569
113
114
70-143
1
30
Tetrachloroethene
ug/L
ND
500
500
554
566
111
113
70-145
2
30
Toluene
ug/L
131
500
500
739
754
122
125
70-142
2
30
trans-1,2-Dichloroethene
ug/L
ND
500
500
627
607
125
121
70-151
3
30
trans-1,3-Dichloropropene
ug/L
ND
500
500
603
586
121
117
70-139
3
30
Trichloroethene
ug/L
ND
500
500
656
644
131
129
62-146
2
30
Trichlorofluoromethane
ug/L
ND
500
500
544
522
109
104
63-153
4
30
Vinyl acetate
ug/L
ND
1000
1000
1210
1180
121
118
61-162
2
30
Vinyl chloride
ug/L
ND
500
500
514
485
103
97
61-163
6
30
Xylene (Total)
ug/L
4060
1500
1500
5610
6440
103
158
70-143
14
30 MS
1,2-Dichloroethane-d4 (S)
%
101
100
70-130
4-Bromofluorobenzene (S)
%
101
100
70-130
Toluene-d8 (S)
%
102
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC.
Page 13 of 24

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
QC Batch: 744923 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92642813001
METHOD BLANK: 3875317
Associated Lab Samples: 92642813001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
10.0
1.7
12/22/22 09:44
1,2-Dichlorobenzene
ug/L
ND
10.0
1.8
12/22/22 09:44
1,3-Dichlorobenzene
ug/L
ND
10.0
1.6
12/22/22 09:44
1,4-Dichlorobenzene
ug/L
ND
10.0
1.7
12/22/22 09:44
1-Methylnaphthalene
ug/L
ND
10.0
2.0
12/22/22 09:44
2,2'-Oxybis(1-chloropropane)
ug/L
ND
10.0
1.2
12/22/22 09:44
2,4,5-Trichlorophenol
ug/L
ND
10.0
1.4
12/22/22 09:44
2,4,6-Trichlorophenol
ug/L
ND
10.0
1.6
12/22/22 09:44
2,4-Dichlorophenol
ug/L
ND
10.0
1.4
12/22/22 09:44
2,4-Dimethylphenol
ug/L
ND
10.0
1.7
12/22/22 09:44
2,4-Dinitrophenol
ug/L
ND
50.0
26.0
12/22/22 09:44
2,4-Dinitrotoluene
ug/L
ND
10.0
1.6
12/22/22 09:44
2,6-Dinitrotoluene
ug/L
ND
10.0
1.7
12/22/22 09:44
2-Chloronaphthalene
ug/L
ND
10.0
1.7
12/22/22 09:44
2-Chlorophenol
ug/L
ND
10.0
1.2
12/22/22 09:44
2-Methylnaphthalene
ug/L
ND
10.0
1.9
12/22/22 09:44
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
1.9
12/22/22 09:44
2-Nitroaniline
ug/L
ND
20.0
3.0
12/22/22 09:44
2-Nitrophenol
ug/L
ND
10.0
1.4
12/22/22 09:44
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
10.0
1.2
12/22/22 09:44
3,3'-Dichlorobenzidine
ug/L
ND
20.0
8.1
12/22/22 09:44
3-Nitroaniline
ug/L
ND
20.0
3.8
12/22/22 09:44
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
7.8
12/22/22 09:44
4-Bromophenylphenyl ether
ug/L
ND
10.0
1.8
12/22/22 09:44
4-ChIoro-3-methyl phenol
ug/L
ND
10.0
3.3
12/22/22 09:44
4-Chloroaniline
ug/L
ND
20.0
3.6
12/22/22 09:44
4-Chlorophenylphenyl ether
ug/L
ND
10.0
2.0
12/22/22 09:44
4-Nitroaniline
ug/L
ND
20.0
5.1
12/22/22 09:44
4-Nitrophenol
ug/L
ND
50.0
6.6
12/22/22 09:44
Acenaphthene
ug/L
ND
10.0
2.0
12/22/22 09:44
Acenaphthylene
ug/L
ND
10.0
2.0
12/22/22 09:44
Aniline
ug/L
ND
10.0
1.6
12/22/22 09:44
Anthracene
ug/L
ND
10.0
2.3
12/22/22 09:44
Benzo(a)anthracene
ug/L
ND
10.0
2.7
12/22/22 09:44
Benzo(a)pyrene
ug/L
ND
10.0
2.8
12/22/22 09:44
Benzo(b)fluoranthene
ug/L
ND
10.0
2.6
12/22/22 09:44
Benzo(g,h,i)perylene
ug/L
ND
10.0
2.8
12/22/22 09:44
Benzo(k)fluoranthene
ug/L
ND
10.0
2.7
12/22/22 09:44
Benzoic Acid
ug/L
ND
50.0
22.0
12/22/22 09:44
Benzyl alcohol
ug/L
ND
20.0
2.9
12/22/22 09:44
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 24

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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QUALITY CONTROL DATA
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
METHOD BLANK: 3875317
Associated Lab Samples: 92642813001
Parameter
Units
bis(2-Chloroethoxy)methane
ug/L
bis(2-Chloroethyl) ether
ug/L
bis(2-Ethylhexyl)phthalate
ug/L
Butylbenzylphthalate
ug/L
Chrysene
ug/L
Di-n-butylphthalate
ug/L
Di-n-octylphthalate
ug/L
Dibenz(a,h)anthracene
ug/L
Dibenzofuran
ug/L
Diethylphthalate
ug/L
Dimethylphthalate
ug/L
Fluoranthene
ug/L
Fluorene
ug/L
Hexachloro-1,3-butadiene
ug/L
Hexachlorobenzene
ug/L
Hexachlorocyclopentadiene
ug/L
Hexachloroethane
ug/L
Indeno(1,2,3-cd)pyrene
ug/L
Isophorone
ug/L
N-Nitroso-di-n-propylamine
ug/L
N-Nitrosodimethylamine
ug/L
N-Nitrosodiphenylamine
ug/L
Naphthalene
ug/L
Nitrobenzene
ug/L
Pentachlorophenol
ug/L
Phenanthrene
ug/L
Phenol
ug/L
Pyrene
ug/L
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol(S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Matrix: Water
Blank
Result
Reporting
Limit
MDL
Analyzed
ND
10.0
1.8
12/22/22 09:44
ND
10.0
1.9
12/22/22 09:44
ND
6.0
3.7
12/22/22 09:44
ND
10.0
3.1
12/22/22 09:44
ND
10.0
2.8
12/22/22 09:44
ND
10.0
2.2
12/22/22 09:44
ND
10.0
3.9
12/22/22 09:44
ND
10.0
3.0
12/22/22 09:44
ND
10.0
2.1
12/22/22 09:44
ND
10.0
2.0
12/22/22 09:44
ND
10.0
2.1
12/22/22 09:44
ND
10.0
2.2
12/22/22 09:44
ND
10.0
2.1
12/22/22 09:44
ND
10.0
1.8
12/22/22 09:44
ND
10.0
2.2
12/22/22 09:44
ND
10.0
1.6
12/22/22 09:44
ND
10.0
1.4
12/22/22 09:44
ND
10.0
2.9
12/22/22 09:44
ND
10.0
1.7
12/22/22 09:44
ND
10.0
1.3
12/22/22 09:44
ND
10.0
1.9
12/22/22 09:44
ND
10.0
3.0
12/22/22 09:44
ND
10.0
2.1
12/22/22 09:44
ND
10.0
1.9
12/22/22 09:44
ND
20.0
3.8
12/22/22 09:44
ND
10.0
2.0
12/22/22 09:44
ND
10.0
1.4
12/22/22 09:44
ND
10.0
2.2
12/22/22 09:44
105
10-164
12/22/22 09:44
64
10-130
12/22/22 09:44
66
10-130
12/22/22 09:44
88
10-138
12/22/22 09:44
59
10-130
12/22/22 09:44
115
19-191
12/22/22 09:44
v1
v1
Qualifiers
LABORATORY CONTROL SAMPLE:
3875318
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
33.3
67
11-130
1,2-Dichlorobenzene
ug/L
50
17.9
36
10-130
1,3-Dichlorobenzene
ug/L
50
15.7
31
10-130
1,4-Dichlorobenzene
ug/L
50
16.6
33
10-130
1-Methylnaphthalene
ug/L
50
47.2
94
23-130
2,2'-Oxybis(1-chloropropane)
ug/L
50
33.4
67
21-135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 24

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
LABORATORY CONTROL SAMPLE:
Parameter
3875318
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4,5-Trichlorophenol
ug/L
50
54.8
110
38-147
2,4,6-Trichlorophenol
ug/L
50
57.1
114
34-142
2,4-Dichlorophenol
ug/L
50
49.6
99
36-136
2,4-Dimethylphenol
ug/L
50
62.3
125
38-134
2,4-Dinitrophenol
ug/L
250
276
110
10-169
2,4-Dinitrotoluene
ug/L
50
61.3
123
44-154
2,6-Dinitrotoluene
ug/L
50
63.9
128
44-156
2-Chloronaphthalene
ug/L
50
52.1
104
25-130
2-Chlorophenol
ug/L
50
37.0
74
29-130
2-Methylnaphthalene
ug/L
50
44.8
90
23-130
2-Methylphenol(o-Cresol)
ug/L
50
41.8
84
31-130
2-Nitroaniline
ug/L
100
120
120
39-145
2-Nitrophenol
ug/L
50
50.9
102
29-142
3&4-Methyl phenol (m&p Cresol)
ug/L
50
42.6
85
30-130
3,3'-Dichlorobenzidine
ug/L
100
110
110
44-158
3-Nitroaniline
ug/L
100
127
127
45-152
4,6-Dinitro-2-methyl phenol
ug/L
100
122
122
39-158
4-Bromophenylphenyl ether
ug/L
50
54.9
110
47-147
4-ChIoro-3-methyl phenol
ug/L
100
110
110
40-138
4-Chloroaniline
ug/L
100
85.6
86
35-130
4-Chlorophenylphenyl ether
ug/L
50
52.0
104
36-139
4-Nitroaniline
ug/L
100
114
114
46-157
4-Nitrophenol
ug/L
250
187
75
17-130
Acenaphthene
ug/L
50
51.8
104
34-135
Acenaphthylene
ug/L
50
53.3
107
35-137
Aniline
ug/L
50
28.8
58
25-130
Anthracene
ug/L
50
54.1
108
47-146
Benzo(a)anthracene
ug/L
50
57.8
116
48-160
Benzo(a)pyrene
ug/L
50
59.1
118
47-165
Benzo(b)fluoranthene
ug/L
50
58.7
117
49-171
Benzo(g,h,i)perylene
ug/L
50
56.4
113
46-166
Benzo(k)fluoranthene
ug/L
50
57.8
116
55-162
Benzoic Acid
ug/L
250
150
60
10-130
Benzyl alcohol
ug/L
100
96.5
97
29-132
bis(2-Chloroethoxy)methane
ug/L
50
51.0
102
33-136
bis(2-Chloroethyl) ether
ug/L
50
38.4
77
30-142
bis(2-Ethylhexyl)phthalate
ug/L
50
67.0
134
46-173
Butylbenzylphthalate
ug/L
50
68.6
137
53-169 v1
Chrysene
ug/L
50
56.3
113
54-152
Di-n-butylphthalate
ug/L
50
63.9
128
49-161
Di-n-octylphthalate
ug/L
50
71.8
144
50-166 v1
Dibenz(a,h)anthracene
ug/L
50
57.5
115
46-166
Dibenzofuran
ug/L
50
53.0
106
37-136
Diethylphthalate
ug/L
50
57.8
116
45-149
Dimethylphthalate
ug/L
50
55.0
110
43-145
Fluoranthene
ug/L
50
59.5
119
50-153
Fluorene
ug/L
50
54.0
108
42-142
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
LABORATORY CONTROL SAMPLE:
Parameter
3875318
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Hexachloro-1,3-butadiene
ug/L
50
25.8
52
10-130
Hexachlorobenzene
ug/L
50
52.9
106
44-138
Hexachlorocyclopentadiene
ug/L
50
37.1
74
10-130
Hexachloroethane
ug/L
50
15.6
31
10-130
Indeno(1,2,3-cd)pyrene
ug/L
50
60.7
121
46-166
Isophorone
ug/L
50
54.9
110
36-135
N-Nitroso-di-n-propylamine
ug/L
50
51.4
103
33-140
N-Nitrosodimethylamine
ug/L
50
38.9
78
24-130
N-Nitrosodiphenylamine
ug/L
50
59.1
118
46-144
Naphthalene
ug/L
50
36.9
74
20-130
Nitrobenzene
ug/L
50
46.5
93
33-133
Pentachlorophenol
ug/L
100
120
120
21-163
Phenanthrene
ug/L
50
58.8
118
47-146
Phenol
ug/L
50
31.2
62
19-130
Pyrene
ug/L
50
59.4
119
53-155
2,4,6-Tribromophenol (S)
%
124
10-164
2-Fluorobiphenyl (S)
%
89
10-130
2-Fluorophenol(S)
%
74
10-130
Nitrobenzene-d5 (S)
%
107
10-138
Phenol-d6 (S)
%
66
10-130
Terphenyl-d14 (S)
%
120
19-191
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3875319
MS
92642813001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3875320
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,2,4-Trichoorobenzene
ug/L
ND
83.3
83.3
26.2
39.9
31
48
10-130
42
30 R1
1,2-Dichlorobenzene
ug/L
ND
83.3
83.3
10.11
21.2
12
25
10-130
30
1,3-Dichlorobenzene
ug/L
ND
83.3
83.3
7.2J
17.8
9
21
10-130
30 M1
1,4-Dichlorobenzene
ug/L
ND
83.3
83.3
8.1J
19.4
10
23
10-130
30
1-Methyl naphthalene
ug/L
ND
83.3
83.3
55.9
61.0
67
73
10-131
9
30
2,2'-Oxybis(1-
ug/L
ND
83.3
83.3
38.8
46.8
47
56
11-143
18
30
chloropropane)
2,4,5-Trichlorophenol
ug/L
ND
83.3
83.3
81.5
79.7
98
96
10-170
2
30
2,4,6-Trichlorophenol
ug/L
ND
83.3
83.3
79.6
78.6
96
94
10-166
1
30
2,4-Dichlorophenol
ug/L
ND
83.3
83.3
67.1
66.9
81
80
10-153
0
30
2,4-Dimethylphenol
ug/L
ND
83.3
83.3
83.5
80.9
100
97
20-147
3
30
2,4-Dinitrophenol
ug/L
ND
417
417
419
413
101
99
10-172
1
30
2,4-Dinitrotoluene
ug/L
ND
83.3
83.3
90.0
87.3
108
105
30-164
3
30
2,6-Dinitrotoluene
ug/L
ND
83.3
83.3
90.8
90.9
109
109
31-163
0
30
2-Chloronaphthalene
ug/L
ND
83.3
83.3
67.0
67.2
80
81
15-134
0
30
2-Chlorophenol
ug/L
ND
83.3
83.3
48.9
52.3
59
63
10-139
7
30
2-Methyl naphthalene
ug/L
ND
83.3
83.3
51.3
55.8
62
67
12-130
8
30
2-Methyl phenol(o-Cresol)
ug/L
ND
83.3
83.3
55.3
57.5
66
69
19-132
4
30
2-Nitroaniline
ug/L
ND
167
167
172
165
103
99
23-154
4
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC.
Page 17 of 24

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QUALITY CONTROL DATA
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3875319
MS
92642813001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3875320
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
2-Nitrophenol
ug/L
ND
83.3
83.3
63.8
68.7
77
82
10-159
7
30
3&4-Methylphenol(m&p
ug/L
ND
83.3
83.3
56.4
58.1
68
70
13-136
3
30
Cresol)
3,3'-Dichlorobenzidine
ug/L
ND
167
167
138
139
83
84
10-178
1
30
3-Nitroaniline
ug/L
ND
167
167
185
176
111
105
20-166
5
30
4,6-Dinitro-2-methylphenol
ug/L
ND
167
167
171
170
103
102
10-187
1
30
4-Bromophenylphenyl ether
ug/L
ND
83.3
83.3
77.0
77.7
92
93
31-157
1
30
4-Chloro-3-methylphenol
ug/L
ND
167
167
153
154
92
92
27-146
1
30
4-Chloroaniline
ug/L
ND
167
167
115
113
69
68
13-143
2
30
4-Chlorophenylphenyl ether
ug/L
ND
83.3
83.3
74.1
71.1
89
85
23-149
4
30
4-Nitroaniline
ug/L
ND
167
167
152
153
91
92
24-171
0
30
4-Nitrophenol
ug/L
ND
417
417
272
287
65
69
10-130
5
30
Acenaphthene
ug/L
ND
83.3
83.3
72.4
72.4
87
87
21-147
0
30
Acenaphthylene
ug/L
ND
83.3
83.3
74.4
72.5
89
87
19-150
3
30
Aniline
ug/L
ND
83.3
83.3
33.5
37.0
40
44
10-130
10
30
Anthracene
ug/L
ND
83.3
83.3
74.8
75.3
90
90
36-152
1
30
Benzo(a)anth race ne
ug/L
ND
83.3
83.3
82.9
82.6
99
99
42-163
0
30
Benzo(a)pyrene
ug/L
ND
83.3
83.3
81.4
85.7
98
103
40-169
5
30
Benzo(b)fluoranthene
ug/L
ND
83.3
83.3
87.6
84.6
105
102
40-177
4
30
Benzo(g,h,i)perylene
ug/L
ND
83.3
83.3
76.7
81.7
92
98
38-174
6
30
Benzo(k)fluoranthene
ug/L
ND
83.3
83.3
85.4
86.7
102
104
41-171
1
30
Benzoic Acid
ug/L
ND
417
417
265
280
64
67
10-130
6
30
Benzyl alcohol
ug/L
ND
167
167
123
132
74
79
18-141
7
30
bis(2-
ug/L
ND
83.3
83.3
63.8
65.7
77
79
19-146
3
30
Chloroethoxy)methane
bis(2-Chloroethyl) ether
ug/L
ND
83.3
83.3
49.1
56.0
59
67
19-151
13
30
bis(2- Ethyl hexyl)phthalate
ug/L
ND
83.3
83.3
101
101
122
121
42-168
1
30
Butylbenzylphthalate
ug/L
ND
83.3
83.3
104
106
125
127
42-177
2
30 v1
Chrysene
ug/L
ND
83.3
83.3
82.0
81.7
98
98
43-159
0
30
Di-n-butylphthalate
ug/L
ND
83.3
83.3
89.9
88.2
108
106
42-160
2
30
Di-n-octylphthalate
ug/L
ND
83.3
83.3
104
106
124
128
42-171
3
30 v1
Dibenz(a,h)anthracene
ug/L
ND
83.3
83.3
77.9
82.4
93
99
40-171
6
30
Dibenzofuran
ug/L
ND
83.3
83.3
73.9
73.0
89
88
23-147
1
30
Diethylphthalate
ug/L
ND
83.3
83.3
82.7
94.3
99
113
33-157
13
30
Dimethylphthalate
ug/L
ND
83.3
83.3
79.8
77.5
96
93
27-154
3
30
Fluoranthene
ug/L
ND
83.3
83.3
83.4
80.8
100
97
42-157
3
30
Fluorene
ug/L
ND
83.3
83.3
76.4
74.9
92
90
25-155
2
30
Hexachloro-1,3-butadiene
ug/L
ND
83.3
83.3
15.0J
28.1
18
34
10-130
30
Hexachlorobenzene
ug/L
ND
83.3
83.3
75.0
76.9
90
92
32-145
3
30
Hexachlorocyclopentadiene
ug/L
ND
83.3
83.3
36.9
46.4
44
56
10-130
23
30
Hexachloroethane
ug/L
ND
83.3
83.3
5.6J
16.3J
7
20
10-130
30 M1
Indeno(1,2,3-cd)pyrene
ug/L
ND
83.3
83.3
80.0
86.4
96
104
39-174
8
30
Isophorone
ug/L
ND
83.3
83.3
74.2
72.4
89
87
19-146
2
30
N-Nitroso-di-n-propylamine
ug/L
ND
83.3
83.3
65.0
68.0
78
82
20-150
4
30
N-Nitrosodimethylamine
ug/L
ND
83.3
83.3
55.2
59.5
66
71
13-130
7
30
N-Nitrosodiphenylamine
ug/L
ND
83.3
83.3
80.3
81.1
96
97
33-149
1
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 24

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QUALITY CONTROL DATA
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3875319
3875320
MS
MSD
92642813001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Naphthalene
ug/L
ND
83.3
83.3
34.5
44.7
41
54
10-128
26
30
Nitrobenzene
ug/L
ND
83.3
83.3
55.4
60.7
66
73
19-145
9
30
Pentachlorophenol
ug/L
ND
167
167
171
170
103
102
10-188
1
30
Phenanthrene
ug/L
ND
83.3
83.3
79.8
79.3
96
95
38-150
1
30
Phenol
ug/L
ND
83.3
83.3
42.2
45.6
51
55
10-130
8
30
Pyrene
ug/L
ND
83.3
83.3
89.2
87.1
107
104
42-163
2
30
2,4,6-Tribromophenol (S)
%
115
98
10-164
2-Fluorobiphenyl (S)
%
71
60
10-130
2-Fluorophenol(S)
%
62
55
10-130
Nitrobenzene-d5(S)
%
79
71
10-138
Phenol-d6 (S)
%
55
50
10-130
Terphenyl-d14 (S)
%
117
106
19-191
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2022 11:04 AM without the written consent of Pace Analytical Services, LLC.
Page 19 of 24

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QUALIFIERS
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
MS Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.
R1 RPD value was outside control limits.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: WRIGHT'S EXECUTIVE 10039-8-Revised Report
Pace Project No.: 92642813
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92642813001 WS-5 EPA 3510C 744923 EPA 8270E 745233
92642813001 WS-5 EPA 8260D 744460
Date: 12/23/2022 11:04 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 21 of 24

ace Lj%rff_ t irte: CNv t-ttiVl-P1UN1-l1Ul 3 v[]7 Sample Condition Upon Receipt
■`���a.0 rc vOLIM. VJr ILfaVL1U3J IL/CULL
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Fluntersville ❑ Raleigh❑ Mechanicsvillen AtiantaF Kernersvillen
Sample � � Client Name: - I
■G j�;t Project #: WQ1t : 92■6428,13
Courier: : ❑Fed Ex ❑UPS ❑LISPS []client II III II I II I Ili II �+ III
❑ Commercial []Pace ❑Other: III i I !I I 1 1
926421313
Custody Seal Present? ❑Yes ❑No Seals Intact? ❑Yes nNo
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other
Thermometer:
❑'IR Gun ID: � •>, <<� 7G�
Type of Ice: ❑Wet ❑Blue
Correction Factor:
Cooler Temp: �� Add/Subtract (°C)
Cooler Temp Corrected (■C): '
USDA Regulated Soil ( Q N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC
(check maps)? [-]Yes nNo
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (02 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match CDC?
-Includes Date/Time/ID/Analysis M
Headspace in VOA Vials (>S-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Project Manager SCURF Review:
.Project hlanager.SRF Review. __ ._-. -_. _. -
No
Yes
❑Yes ❑No ❑N/A
UYes (JNo L rv/A- 7.
❑Ye;�"QNo ❑N/A S,
Yes ❑No ❑N/A 9.
LJYes EjNo _ El N/A 1 10.
❑Yes PNri ❑N/A 11.M.-I"
(late/Initials Person Examining ContentI�?
Biological Tissue Frozen?
❑Yes QNo ❑N/A
[]None
Temp should be above freezing to 6■C
05amples out of temp criteria. Samples on ice, cooling process
hasbegun
Did samples originate from a foreign source (internationally,
including Hawaii and Puerto Rico)? ❑Yes ❑No
Comments/Discreoanev:
Field Data Required? Elyes ❑No
Lot ID of split containers:
Date/Time:
Date:
Date: --
Qualtrax ID: 69614 Page 1 of 2 Page 22 of 24

uuff t Itle: ervv-r-KIVI-Muhl-UUbS vU1_sample Condition Upon Receipt
Effective Date: 051121202205/12/2022
*Check mark top half of box if pH and/or dechlorination is verified and
within the acceptance range for preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/80I5 (water) DOC, Mig
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Project # WO# : 926428 13
PM: $I: Due Oate: 12/22/22
CLIENT: 92-ECS RPL
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pH Adjustment frog for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot 4
adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax 0: 69614 Page 2 of 2 Page 23 of 24

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VOCS 82W
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Page 24 of 24