09003_Florence Mill_Forest City Monitoring Rpt_20230515

Memorandum

AECOM Technical Services of North Carolina, Inc. is pleased to provide the attached Semi-Annual Soil
Gas Sampling and Annual Groundwater Monitoring Report for the Florence Mill Brownfield Project
Site (the Site) located at 186 Mill Street, Forest City, North Carolina. In 2019, construction was completed
at the Site which was turned into a public outdoor space known as the Forest City Pavilion on Park
Square (POPS).
The results herein include data from the semi-annual soil vapor monitoring, and annual groundwater
monitoring events in accordance with the objectives defined in the approved scope of work originally
proposed in the environmental Management Plan (EMP) by Irminger Consulting Inc (IC), dated
December 2, 2013 and further established in the Brownfield Agreement (BA) for the project.
As documented in the Construction Completion and Monitoring Point Installation Memorandum, dated
May 24, 2019, ten soil gas vapor points (VP-1 to VP-10) were installed around the Site for monitoring of
soil gas at depths 5.5 ft below ground surface (bgs), and 20 ft bgs, respectively. Initial sampling of these
vapor points was completed in February 2019 along with sampling of monitoring wells MW-1R and MW-
17. Consistent with the BA, the soil vapor points were sampled in February 2023.
Report Objectives:
 Summarize the groundwater and soil vapor monitoring completed in February 2023.
 Present analytical results for groundwater and soil vapor samples.

Monitoring Well Sampling Methods

Monitoring wells MW-1R and MW-17 were sampled with pre-deployed HydraSleeve sampling bags on
February 21, 2023. Water quality parameters of temperature, pH, specific conductance, dissolved
oxygen, and oxygen reduction potential (ORP) were measured and recorded using a YSI Pro Plus
portable field instrument. Groundwater samples were collected in pre-preserved, laboratory provided
containers and were immediately placed on ice. The groundwater field-measured water quality data are
included in the field notes in Attachment A. The laboratory analytical reports for the groundwater
samples are presented in Attachment B and a Photo Log from the sampling event is included as
Attachment C.

Groundwater samples were transported to Pace Analytical Services – Charlotte in North Carolina under
chain of custody for analysis of VOCs by USEPA Method 8260D. Results for the February groundwater
Date: Monday, May 15, 2023
To: Sarah Hardison (NCDEQ Brownfields)
CC: Janet Mason and Amy Bridgers (Town of Forest City)
From: Cristin Dolan and Conan Fitzgerald (AECOM)
Subject: Florence Mill Brownfield Project Semi-Annual Soil Gas Sampling and Annual Groundwater Monitoring – February 2023

sampling data are presented in Table 1 and historic results are presented on Table 2. The only
exceedance of the North Carolina 15A NCAC 02L (2L) groundwater standards was for perchloroethylene
(PCE). Results were consistent with historical ranges.

Soil Vapor Sampling Methods
On February 21, 2023, soil gas samples were collected from nine of the ten site soil vapor monitoring
points. During the site activities, VP-5 was noted to contain water which prevented sample collection.
Vapor Points VP-1 to VP-4, and VP-6 to VP-10 were sampled using 6-liter Summa canisters fitted with
0.5-hour flow controllers.
Prior to sampling, helium leak tests were performed at each soil vapor location to verify a proper seal
between the permanently installed stainless steel vapor implants and the ground surface. Reference
Attachment A for field notes and parameters recorded during vapor sampling and leak testing.
Samples were submitted to a certified laboratory for analysis of volatile organic compounds (VOCs) by
United States Environmental Protection Agency (EPA) Method TO-15-full analyte list. The laboratory
analytical reports for the soil vapor monitoring points are presented in Attachment B. A Photo Log from
the sampling event is included as Attachment C. Samples were collected in accordance with the
AECOM sampling protocols (Attachment D).
Soil Gas Analytical Results
Results for February soil vapor sampling data are presented in Table 3. Results for tetrachloroethene
(PCE) and trichloroethylene (TCE) are summarized on Figure 1 for 2021 through 2023. For data
completeness, a summary of all historical soil gas analytical results for the since February 2019 can be
found in Table 4. The following VOCs were detected above their corresponding NC DEQ Non-
Residential Vapor Intrusion Screening levels for the February 2023 monitoring event.
 PCE and TCE were the only analytes detected above NC DEQ Non-Residential Vapor
Intrusion Screen Levels of 3,500, and 180 µg/m³, respectively.
 PCE was detected above its respected NC DEQ Non-Residential Vapor Intrusion Screening
Levels in four vapor monitoring points (VP-1 to VP-4) during the February 2023 sampling.
Highest PCE values were detected in VP-4 at 6,710,000 µg/m³ during the February 2023
sampling. TCE was detected above its Residential Screening criteria in VP-3 and VP-4, with
the greatest detection in VP-4 of 6860 µg/m³.
 Vapor points VP-1 through VP-4 were installed in the vicinity of the former drycleaner, so the
presence of elevated PCE concentrations in this location are not unexpected. The structure in
this area currently houses a concession stand and bathrooms, and thus is used very
intermittently. Indoor air sampling conducted in March 2021 confirmed that passive vapor
mitigation features installed within the structure is mitigating exposure for those using the
facility.
 Generally, the deeper screened nested monitoring points (19-20 ft bgs) exhibited significantly
higher PCE concentrations than the adjacent shallow screened (4.5-5.5 ft bgs) monitoring

points in this area. This continues to suggest that groundwater is the source of chlorinated
vapors in this area.

Next Monitoring Event
Per the BA, the next monitoring event is scheduled to occur in August of 2023 and will include soil vapor
data collection only.

Tables
Table 1. Summary of Detected Groundwater Sampling Results (February 2023)
Table 2. Groundwater Historical Summary
Table 3. Summary of Detected Soil Gas Sampling Results (February 2023)
Table 4. Soil Gas Historical Summary

Figures
Figure 1. Site Location Map with Soil Gas Results

Attachments
Attachment A. Field Notes
Attachment B. Laboratory Analytical Reports
Attachment C. Photo Log
Attachment D. AECOM Soil Gas Sampling Protocol

Tables
Table 1
Summary of Detected Groundwater Sample Results
Florence Mill Brownfield Project
Forest City, NC
Location:MW-1R MW-17
Sample Date:2/21/2023 2/21/2023
Sample Type:Normal Normal
VOCs (SW-846 8260D)
Tetrachloroethene 0.7 1,600 166
1,2,4-Trichlorobenzene 70 <10 1.6
Notes:
< # - Not detected at the specified reporting limit
EPA - Environmental Protection Agency
NC 2L - NC Groundwater quality standard
SW-846 -Test Methods for Evaluating Solid Waste, Physical/Chemical Methods , EPA
VOC - Volatile organic compound
NC Groundwater quality standards for the protection of the groundwater are specified in 15A NCAC 2L .0202,
effective April 1, 2022. Sample concentrations that are greater than the standard are highlighted and bold.
NC 2L
This table presents a summary of results for analytes detected in groundwater samples collected in February
2023. Sample results have been qualified by AECOM based on the results of the data review process, which
is modeled after the USEPA Contract Laboratory Program National Functional Guidelines for Superfund
Organic Methods Data Review (EPA, November 2020). All sample results are reported in micrograms per liter
(µg/L).
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Table 2
Groundwater Historical Summary
Flemington Mills Brownfield Project
Forest City, North Carolina
Location:MW-1R MW-1R MW-1R MW-1R MW-1R MW-17 MW-17 MW-17 MW-17 MW-17
Sample Date:2/14/2019 2/13/2020 2/12/2021 2/24/2022 2/21/2023 2/14/2019 2/13/2020 2/12/2021 2/24/2022 2/21/2023
Sample Type:Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal
VOCs (SW-846 8260D)
Benzene 1 2.27 <4.5 <2.6 <10.0 <10.0 <0.331 <0.36 <0.13 <1.0 <1.0
n-Butylbenzene 70 0.902 J <5.2 <2.8 NA NA <0.361 UJ <0.42 <0.14 NA NA
Chloroform 70 1.66 J <4.2 <3.8 <10.0 <10.0 <0.324 <0.34 <0.19 <1.0 <1.0
1,2-Dichlorobenzene 20 <1.0 <4.0 <2.0 12.0 <10.0 <1.0 <0.32 <0.10 <1.0 <1.0
cis-1,2-Dichloroethene 70 <1.0 <3.2 <3.0 17.2 <10.0 <1.0 <0.26 <0.15 <1.0 <1.0
Isopropyl benzene 70 3.2 <4.2 <2.0 NA NA <0.326 <0.34 <0.10 NA NA
Naphthalene 6 48.8 J <7.8 UJ <3.0 <10.0 <10.0 6.47 J <0.62 UJ <0.15 <1.0 <1.0
n-Propylbenzene 70 0.694 J <3.2 <1.6 NA NA <0.349 UJ <0.26 <0.080 NA NA
Tetrachloroethene 0.7 2,830 2,300 2,100 1,370 1,600 200 120 64 82.4 166.0
Trichloroethene 3 5.14 <6.0 3.6 J <10.0 <10.0 <0.398 <0.48 <0.18 <1.0 <1.0
1,2,4-Trichlorobenzene 70 <1.0 <10.0 <3.2 <10.0 <10.0 <1.0 <0.080 <0.16 <1.0 1.6
1,2,3-Trimethylbenzene NS 43.8 J ND UJ1 <9.8 NA NA 0.786 J ND UJ1 <0.49 NA NA
1,2,4-Trimethylbenzene 400 54.2 J <4.5 <2.0 NA NA 0.635 J <0.36 <0.10 NA NA
1,3,5-Trimethylbenzene 400 16.3 J <3.5 <2.0 NA NA <0.387 UJ <0.28 <0.10 NA NA
Xylenes (Total)500 40.6 <4.2 <1.8 <10.0 <10.0 <1.06 <0.34 <0.090 <1.0 <1.0
Notes:
1 Analyte determined through a tentatively identified compound (TIC) search
< - Not detected at the specified detection limit
EPA - Environmental Protection Agency
J - Estimated value
NA - Not analyzed
NC 2L - NC Groundwater quality standard
ND - Not detected
SW-846 -Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, EPA
UJ - Not detected and the associated detection limit is estimated
VOC - Volatile organic compound
NC 2L
NS - Narrative standard per 15A NCAC 02L .0202(c), substances which are not naturally occurring and for which a standard has not been
specified shall not be permitted in concentrations at or above the practical quantitation limit in Class GA or Class GSA groundwaters.
This table presents a summary of results for analytes detected in groundwater samples collected in February 2019, 2020, 2021, 2022, and 2023.
Sample results have been qualified by AECOM based on the results of the data review process, which is modeled after the USEPA Contract
Laboratory Program National Functional Guidelines for Superfund Organic Methods Data Review (EPA, November 2020). All results are
reported in micrograms per liter (µg/L).
NC Groundwater quality standards for the protection of the groundwater are specified in 15A NCAC 2L .0202, effective April 1, 2022. Sample
concentrations that are greater than the standard are highlighted and bold. Sample detections are bold.
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Table 3
Summary of Detected Soil Gas Sample Results
Florence Mill Brownfield Project
Forest City, North Carolina
Location:VP-01 VP-02 VP-03 VP-04 VP-06 VP-07 VP-08 VP-09 VP-10
Sampling Date:02/21/2023 02/21/2023 02/21/2023 02/21/2023 02/21/2023 02/21/2023 02/21/2023 02/21/2023 02/21/2023
VOCs (EPA TO-15)
Acetone NE <2.97 <2,380 <1,190 <2,380 4.30 5.23 <2.97 6.34 <2.97
2-Butanone 440000 <3.69 <2,950 <1,470 <2,950 4.04 <3.69 <3.69 <3.69 <3.69
Carbon tetrachloride 200 2.95 <1,010 <504 <1,010 <1.26 <1.26 <1.26 <1.26 <1.26
Cyclohexane 530000 <0.689 <551 <276 <551 <0.689 1.28 6.44 <0.689 <0.689
1,3-Dichlorobenzene NE <1.20 <962 <481 <962 <1.20 <1.20 <1.20 <1.20 1.82
Dichlorodifluoromethane 8800 1.43 <791 <396 <791 1.81 1.85 1.78 1.64 1.63
1,1-Dichloroethane 770 <0.802 <641 <321 <641 <0.802 <0.802 2.71 <0.802 <0.802
1,1-Dichloroethylene NE <0.793 <634 <317 <634 <0.793 <0.793 2.92 <0.793 <0.793
1,2-cis-Dichloroethylene NE <0.793 <634 <317 3,640 <0.793 <0.793 <0.793 <0.793 <0.793
Ethanol (ethyl alcohol)NE <2.36 <1,890 1,490 <1,890 7.99 17.9 <2.36 27.3 <2.36
Ethyl Acetate 6100 <0.720 <576 <288 <576 <0.720 <0.720 <0.720 0.831 <0.720
Isopropanol 18000 <3.07 6,860 6,710 7,770 <3.07 <3.07 <3.07 3.88 <3.07
Methyl methacrylate 61320 <0.819 <655 553 <655 <0.819 <0.819 <0.819 <0.819 <0.819
Methylene chloride 53000 <0.694 <556 <278 <556 <0.694 0.844 <0.694 <0.694 <0.694
n-Hexane 61000 <2.22 2,190 2,560 3,320 <2.22 <2.22 <2.22 <2.22 <2.22
Tetrachloroethylene 3500 24,000 1,190,000 629,000 6,710,000 6.14 33.2 251 282 1,190
1,1,1-Trichloroethane 440000 <1.09 <870 <435 <870 <1.09 63.6 228 1.37 3.20
Trichloroethylene 180 3.16 <857 1,900 6,860 <1.07 <1.07 <1.07 <1.07 <1.07
Trichlorofluoromethane NE 5.96 <899 <450 <899 1.80 4.19 13.7 2.32 5.68
Notes:
(1) NC DEQ Non-Residential Vapor Intrusion Screening Levels, effective January 2022
< # - Not detected at the specified reporting limit
µg/m³ - Micrograms per cubic meter
EPA - Enviromental Protection Agency
NE - Not established
VOC - Volatile organic compound
Sample concentrations greater than NC DEQ Non-residential vapor intrusion soil gas screening levels are highlighted. Sample detections are shown in a bold font.
This table presents a summary of results for analytes detected in soil gas samples that were collected at the site in February 2023. All sample results are reported in micrograms per cubic
meter (µg/m³).
Exterior Soil Gas
Screening Level (1)
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Table 4
Soil Gas Historical Summary
Flemington Mills Brownfield Project
Forest City, North Carolina
Location:VP-1 VP-1 VP-1 VP-1 VP-1 VP-1 VP-2 VP-2 VP-2 VP-2 VP-2 VP-2 VP-2 VP-3 VP-3 VP-3 VP-3 VP-3 VP-3 VP-3 VP-3
Non-Residential (1)02/13/19 02/12/21 08/18/21 02/24/22 08/19/22 02/21/23 02/13/19 08/17/20 02/12/21 08/18/21 02/24/22 08/19/22 02/24/23 02/14/19 02/13/20 08/17/20 02/12/21 08/18/21 02/24/22 08/19/22 02/21/23
VOCs (EPA TO-15)
Acetone NE <190 <190 <140 <67 6.01 <2.97 <190 <7,100 <190 <140 <4,200 <238 <2,380 <190 <1,400 <7,100 <5,700 <190 <2,900 <1190 <1,190
Benzene 160 <6.4 <6.4 <4.8 <45 <1.28 <0.639 18 <240 <6.4 <4.8 <2,800 <51.1 <511 <6.4 <48 <240 <190 6.8 <1,900 <256 <256
Bromodichloromethane 33 <13 <13 <10 <95 <2.68 <1.70 <13 <500 <13 <10 <5,900 <107 <1,360 <13 <100 <500 <400 <13 <4,100 <537 <681
2-Butanone (MEK)440,000 <240 <240 <180 <42 <7.37 <3.69 9.2 J <8,800 <240 <180 <2,600 <295 <2,950 <240 <1,800 <8,800 <7,100 26 <1,800 <1470 <1,470
Carbon Disulfide 61,000 <62 <62 <47 110 <1.24 <0.622 190 J <2,300 <62 <47 <5,500 <49.8 <498 <62 <470 <2,300 <1,900 <62 <3,800 <249 <249
Carbon Tetrachloride 200 <13 <13 4.9 <89 8.06 2.95 38 <470 160 120 <5,500 <101 <1,010 <13 <94 <470 <380 <13 <3,800 <504 <504
Chloroform 53 <9.8 <9.8 <7.3 <69 <1.95 <0.973 17 <370 37 32 <4,300 <77.9 <779 <9.8 <73 <370 <290 <9.8 <3,000 <389 <389
Chloromethane 625 NA NA NA <58 0.985 <0.413 NA NA NA NA <3,600 <33.0 <330 NA NA NA NA NA <2,500 <165 <165
Cyclohexane 530,000 <14 <6.9 <5.2 NA NA <0.689 <14 <260 <6.9 <5.2 NA NA <551 <14 <52 <260 <210 <6.9 NA NA <276
Dibromochloromethane NE <17 <17 <13 <120 <3.40 <1.34 <17 <640 <17 <13 <7,500 <136 <1,070 <17 <130 <640 <510 <17 <5,200 <681 <537
1,3-Dichlorobenzene NE <12 <12 <9.0 <85 <2.40 <1.20 <12 <450 <12 <9.0 <5,300 <96.2 <962 <12 <90 <450 <360 <12 <3,600 <481 <481
Dichlorodifluoromethane (Freon 12)8,800 <9.9 <9.9 <7.4 <70 2.18 1.43 <9.9 <370 <9.9 <7.4 <4,300 <79.1 <791 <9.9 <74 <370 <300 <9.9 <4,300 <396 <396
1,1-Dichloroethane 770 <8.1 <8.1 <6.1 <57 <1.60 <0.802 <8.1 <300 <8.1 <6.1 <3,600 <64.1 <641 <8.1 <61 <300 <240 <8.1 <2,500 <321 <321
1,1-Dichloroethylene 18,000 <7.9 <7.9 <6.1 <56 <1.59 <0.793 <7.9 <300 <7.9 <5.9 <3,500 <63.4 <634 <7.9 <59 <300 <240 <7.9 <2,400 <317 <317
cis-1,2-Dichloroethylene NE <7.9 <7.9 <5.9 <56 <1.59 <0.793 <7.9 <300 13 14 <3,500 <63.4 <634 <7.9 <59 <300 <240 14 <2,400 <317 <317
trans-1,2-Dichloroethylene 3,500 <7.9 <7.9 <5.9 <56 <1.59 <0.793 <7.9 <300 <7.9 <5.9 <3,500 <63.4 <634 <7.9 <59 <300 <240 <7.9 <2,400 <317 <317
Ethanol NE <150 <150 <110 NA NA <2.36 <150 <5,700 <150 <110 NA NA <1,890 <150 <1,100 <5,700 <4,500 <150 NA NA 1,490
Ethyl Acetate 6,100 <7.2 <72 <54 NA NA <0.720 <7.2 <2,700 <72 <54 NA NA <576 <7.2 <54 <2,700 <2,200 <72 NA NA <288
Ethylbenzene 490 <8.7 <8.7 <6.5 <61 <1.73 <0.867 <8.7 <330 <8.7 <6.5 <3,800 <69.4 <694 <8.7 <65 <330 <260 <8.7 <2,600 <347 <347
Heptane 35,000 <8.2 <8.2 <6.1 NA NA <0.818 14 <310 <8.2 <6.1 NA NA <654 <8.2 <61 <310 <250 <8.2 NA NA <327
Hexane 61,000 <280 <280 <210 NA NA <2.22 23 J <11,000 <280 <210 NA NA 2,190 <280 <2,100 <11,000 <8,500 <280 NA NA 2,560
4-Methyl-2-pentanone (MIBK)260,000 <8.2 <8.2 <6.1 <58 <10.2 <5.12 <8.2 <310 <8.2 <6.1 <3,600 <409 <4,090 <8.2 <61 <310 <250 <8.2 <2,500 <2,050 <2,050
Methylene Chloride 53,000 <69 <69 <52 <49 <1.39 <0.694 <69 <2,600 <69 <52 <3,100 156 <556 <69 <520 <2,600 <2,100 <69 <2,100 521 <278
Naphthalene 36 <10 <10 <7.9 NA NA <3.30 <10 <390 <10 <7.9 NA NA <2,640 <10 <79 <390 <310 <10 NA NA <1,320
Propene 260,000 <140 <140 <100 NA NA <2.15 120 J <5,200 <140 <100 NA NA <1,720 <140 <1,000 <5,200 <4,100 <140 NA NA <861
Tetrachloroethylene 3,500 7,000 11,000 38,000 18,000 9,570 24,000 120,000 1,200,000 1,300,000 1,200,000 890,000 443,000 1,190,000 160,000 900,000 4,000,000 1,000,000 3,300,000 610,000 2,230,000 629,000
Tetrahydrofuran 180,000 <5.9 <59 <44 NA NA <0.590 <5.9 <2,200 <59 <44 NA NA <472 <5.9 <44 <2,200 <1,800 <59 NA NA <236
Toluene 440,000 <7.5 <7.5 <5.7 <53 <3.77 <1.88 59 <280 <7.5 <5.7 <3,300 <151 <1,510 <7.5 <57 <280 <230 <7.5 <2,300 <753 <753
1,1,1-Trichloroethane 440,000 <11 <11 <8.2 <77 <2.18 <1.09 <11 <410 <11 <8.2 <4,800 <87.0 <870 <11 <82 <410 340 <11 <3,300 <435 <435
Trichloroethylene 180 <11 <11 7.1 <76 8.30 3.16 140 890 1,500 1,400 <4,700 1,020 <857 140 240 580 <320 760 <3,300 648 <857
Trichlorofluoromethane (Freon 11)NE <45 <45 <34 <80 13.2 5.96 13 J <1,700 <45 29 <4,900 <89.9 <899 <45 <340 <1,700 <1,300 <45 <3,400 <450 <450
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)440,000 <61 <61 <46 <110 <3.07 <1.53 <61 <2,300 <61 <46 <6,700 <123 <1,230 <61 <460 <2,300 <1,800 <61 <4 600 <613 <613
1,2,4-Trimethylbenzene 5,300 <9.8 <9.8 <7.4 <70 <1.96 <0.982 <9.8 <370 <9.8 <7.4 <4,300 <78.5 <785 <9.8 <74 <370 <290 <9.8 <3,000 <393 <393
1,3,5-Trimethylbenzene 5,300 <9.8 <9.8 <7.4 <70 <1.96 <0.982 <9.8 <370 <9.8 <7.4 <4,300 <78.5 <785 <9.8 <74 <370 <290 <9.8 <3,000 <393 <393
Xylenes (total)8,800 <8.7 < 8.7 <20 NA <1.73 <0.867 <8.7 <330 < 8.7 <20 NA <69.4 <694 <8.7 <65 <330 <260 <26 NA <347 <347
Sub-slab and
Exterior Soil Gas
Screening Level
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Table 4
Soil Gas Historical Summary
Flemington Mills Brownfield Project
Forest City, North Carolina
Location:
Non-Residential (1)
VOCs (EPA TO-15)
Acetone NE
Benzene 160
Bromodichloromethane 33
2-Butanone (MEK)440,000
Carbon Disulfide 61,000
Carbon Tetrachloride 200
Chloroform 53
Chloromethane 625
Cyclohexane 530,000
Dibromochloromethane NE
1,3-Dichlorobenzene NE
Dichlorodifluoromethane (Freon 12)8,800
1,1-Dichloroethane 770
1,1-Dichloroethylene 18,000
cis-1,2-Dichloroethylene NE
trans-1,2-Dichloroethylene 3,500
Ethanol NE
Ethyl Acetate 6,100
Ethylbenzene 490
Heptane 35,000
Hexane 61,000
4-Methyl-2-pentanone (MIBK)260,000
Methylene Chloride 53,000
Naphthalene 36
Propene 260,000
Tetrachloroethylene 3,500
Tetrahydrofuran 180,000
Toluene 440,000
1,1,1-Trichloroethane 440,000
Trichloroethylene 180
Trichlorofluoromethane (Freon 11)NE
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)440,000
1,2,4-Trimethylbenzene 5,300
1,3,5-Trimethylbenzene 5,300
Xylenes (total)8,800
Sub-slab and
Exterior Soil Gas
Screening Level VP-4 VP-4 VP-4 VP-4 VP-4 VP-4 VP-4 VP-4 VP-5 VP-5 VP-5 VP-5 VP-5 VP-5 VP-5 VP-6 VP-6 VP-6 VP-6 VP-6 VP-6 VP-6
<57,000 <1,400 <7,100 <5,700 <140 <25,000 <5,940 <2,380 87 11 J 15 J <19 16 <9.6 <2.97 15 J <19 <19 18 <10 <2.97 4.30
<1,900 <48 <240 <190 7.0 <17,000 <1,280 <511 1.4 <0.64 0.22 J <0.64 <0.64 <6.5 <0.639 2.5 <0.64 <0.64 <0.64 <6.7 <0.639 <0.639
<4,000 <100 <500 <400 <10 <35,000 <2,680 <1,360 <1.3 <1.3 <1.3 <1.3 <1.3 <14 <1.34 <1.3 <1.3 <1.3 <1.3 <14 <1.34 <1.70
<71,000 <1,800 <8,800 <7,100 <180 <16,000 <7,370 <2,950 25 1.7 J 2.3 J <24 <24 19 <3.69 3.4 J <24 <24 <24 11 <3.69 4.04
<19,000 <470 <2,300 <1,900 <47 <33,000 <1,240 <498 18 J <6.2 <6.2 <6.2 <6.2 98 <0.622 14 J <6.2 <6.2 <6.2 <13 <0.622 <0.622
<3,800 <94 <470 <380 <9.4 <33,000 <2,520 <1,010 <1.3 <1.3 0.35 J <1.3 <1.3 <13 <1.26 <1.3 <1.3 <1.3 <1.3 <13 <1.26 <1.26
<2,900 220 <370 <290 230 <26,000 <1,950 <779 0.53 J <0.98 <0.98 <0.98 <0.98 <9.9 <0.973 0.53 J <0.98 <0.98 <0.98 <10 <0.973 <0.973
NA NA NA NA NA <22,000 <826 <330 NA NA NA NA NA <8.4 <0.413 NA NA NA NA <8.7 <0.413 <0.413
<4,100 <52 <260 <210 <5.2 NA NA <551 <1.4 <0.69 <0.69 <0.69 <0.69 NA NA <1.4 <0.69 <0.69 <0.69 NA NA <0.689
<5,100 <130 <640 <510 <13 <45,000 <3,400 <1,070 <1.7 <1.7 <1.7 <1.7 <1.7 <17 <1.70 <1.7 <1.7 <1.7 <1.7 <18 <1.70 <1.34
<3,600 <90 <450 <360 <9.0 <32,000 <2,400 <962 <1.2 <1.2 <1.2 <1.2 <1.2 <12 <1.20 <1.2 <1.2 <1.2 <1.2 <13 <1.20 <1.20
<3,000 <74 <370 <300 <6.1 <26,000 <1,980 <791 2.7 2.4 <0.99 <0.99 <0.99 <10 1.89 3.0 2.7 <0.99 <0.99 <10 2.14 1.81
<2,400 <61 <300 <240 <6.1 <21,000 <1,600 <641 <0.81 <0.81 <0.81 <0.81 <0.81 <8.2 <0.802 <0.81 <0.81 <0.81 <0.81 <8.5 <0.802 <0.802
<2,400 <59 <300 <240 <5.9 <21,000 <1,590 <634 <0.79 <0.79 <0.79 <0.79 <0.79 <8.0 <0.793 <0.79 <0.79 <0.79 <0.79 <8.4 <0.793 <0.793
<2,400 3,200 2,500 3,300 3,500 <21,000 3,840 3,640 <0.79 <0.79 0.36 J <0.79 <0.79 <8.0 <0.793 <0.79 <0.79 <0.79 <0.79 <8.4 <0.793 <0.793
<2,400 76 <300 <240 100 <21,000 <1,590 <634 <0.79 <0.79 <0.79 <0.79 <0.79 <8.0 <0.793 <0.79 <0.79 <0.79 <0.79 <8.4 <0.793 <0.793
<45,000 <1,100 <5,700 <4,500 <110 NA NA <1,890 10 J <15 5.8 J <15 78 NA NA <15 <15 <15 35 NA NA 7.99
<2,200 <54 <2,700 <2,200 <54 NA NA <576 9.7 <0.72 <7.2 <7.2 <7.2 NA NA <0.72 <0.72 <7.2 13 NA NA <0.720
<2,600 <65 <330 <260 <6.5 <23,000 <1,730 <694 0.68 J <0.87 <0.87 <0.87 <0.87 <8.8 <0.867 0.99 <0.87 <0.87 0.33 <9.1 <0.867 <0.867
<2,500 <61 <310 <250 <6.1 NA NA <654 0.95 <0.82 <0.82 <0.82 <0.82 NA NA 1.9 <0.82 <0.82 <0.82 NA NA <0.818
<85,000 <2,100 <11,000 <8,500 <210 NA NA 3,320 2.3 J <28 <28 <28 <28 NA NA 5.3 J <28 <28 <28 NA NA <2.22
<2,500 <61 <310 <250 <6.1 <22,000 <10,200 <4,090 1.5 <0.82 <0.82 <0.82 <0.82 <8.3 <5.12 3.1 <0.82 <0.82 <0.82 <8.6 <5.12 <5.12
<21,000 <520 <2,600 <2,100 <52 <18,000 <1,390 <556 1.5 J <6.9 <6.9 <6.9 <6.9 <7.0 <0.694 0.86 J <6.9 <6.9 <6.9 <7.3 <0.694 <0.694
<3,100 <79 <390 <310 <7.9 NA NA <2,640 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA 0.82 J <1.0 <1.0 <1.0 NA NA <3.30
<41,000 <1,000 <5,200 <4,100 <100 NA NA <1,720 44 <14 <14 <14 <14 NA NA 71 <14 <14 <14 NA NA <2.15
12,000,000 9,000,000 5,700,000 4,900,000 7,000,000 4,800,000 5,310,000 6,710,000 29 890 1300 19 <14 9.44 9.3 23 2.8 <14 5.61 6.14
<1,800 <44 <2,200 <1,800 <44 NA NA <472 2.5 <0.59 <5.9 <5.9 <5.9 NA NA <0.59 <0.59 <5.9 <5.9 NA NA <0.590
<2,300 <57 <280 <230 <5.7 <20,000 <3,770 <1,510 10 <0.75 0.44 J <0.75 7.9 <7.6 <1.88 18 <0.75 <0.75 5.4 <7.9 <1.88 <1.88
<3,300 <82 <410 <330 <8.2 <29,000 <2,180 <870 <1.1 <1.1 <1.1 <1.1 <1.1 <11 <1.09 0.94 J 0.74 J 0.57 J <11 <1.09 <1.09
4,100 5,800 4,600 5,400 6,300 <28,000 6,700 1,900 <1.1 <1.1 0.62 J <1.1 0.67 <11 <1.07 <1.1 <1.1 <1.1 <1.1 <11 <1.07 6,860
<13,000 <340 <1,700 <1,300 <34 <30,000 <2,250 <899 1.7 J 1.5 J 1.3 J <4.5 1.1 <11 1.74 2.7 J 2.2 J <4.5 <4.5 <12 1.91 1.80
<18,000 <460 <2,300 <1,800 <46 <40,000 <3,070 <1,230 <6.1 <6.1 <6.1 <6.1 <6.1 <15 <1.53 <6.1 <6.1 <6.1 <6.1 <16 <1.53 <1.53
<2,900 <74 <370 <290 <7.4 <26,000 <1,960 <785 <0.98 <0.98 <0.98 <0.98 <0.98 <9.9 <0.982 2.9 <0.98 <0.98 <0.98 <10 <0.982 <0.982
<2,900 <74 <370 <290 <7.4 <26,000 <1,960 <785 <0.98 <0.98 <0.98 <0.98 <0.98 <9.9 <0.982 <0.98 <0.98 <0.98 <0.98 <10 <0.982 <0.982
<2,600 <65 <330 <260 <20 NA <1,730 <694 2.5 J <0.87 <0.87 <0.87 <2.6 NA <0.867 3.8 <0.87 <0.87 0.89 NA <0.867 <0.867
\\na.aecomnet.com\LFS\AMER\Raleigh-USRAL3\DCS\Projects\ENV\60613889_FCBRWNFLDX\500_Deliverables\502_Monitoring rpts\2023\23_ 02 rpt\Tables\Table 4 2019-2023 Forest City Soil Gas_HL_NL.xlsx Page 2 of 4
Table 4
Soil Gas Historical Summary
Flemington Mills Brownfield Project
Forest City, North Carolina
Location:
Non-Residential (1)
VOCs (EPA TO-15)
Acetone NE
Benzene 160
Bromodichloromethane 33
2-Butanone (MEK)440,000
Carbon Disulfide 61,000
Carbon Tetrachloride 200
Chloroform 53
Chloromethane 625
Cyclohexane 530,000
Dibromochloromethane NE
1,3-Dichlorobenzene NE
Dichlorodifluoromethane (Freon 12)8,800
1,1-Dichloroethane 770
1,1-Dichloroethylene 18,000
cis-1,2-Dichloroethylene NE
trans-1,2-Dichloroethylene 3,500
Ethanol NE
Ethyl Acetate 6,100
Ethylbenzene 490
Heptane 35,000
Hexane 61,000
4-Methyl-2-pentanone (MIBK)260,000
Methylene Chloride 53,000
Naphthalene 36
Propene 260,000
Tetrachloroethylene 3,500
Tetrahydrofuran 180,000
Toluene 440,000
1,1,1-Trichloroethane 440,000
Trichloroethylene 180
Trichlorofluoromethane (Freon 11)NE
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)440,000
1,2,4-Trimethylbenzene 5,300
1,3,5-Trimethylbenzene 5,300
Xylenes (total)8,800
Sub-slab and
Exterior Soil Gas
Screening Level VP-7 VP-7 VP-7 VP-7 VP-7 VP-7 VP-7 VP-7 VP-8 VP-8 VP-8 VP-8 VP-8 VP-8 VP-8 VP-8
<19 10 J <19 <19 14 27 6.37 5.23 26 <19 17 J <19 37 <9.6 <2.97 <2.97
6.4 <0.64 <0.64 <0.64 <0.64 <6.7 <0.639 <0.639 1.1 <0.64 <0.64 <0.64 <0.64 <6.5 <0.639 <0.639
<1.3 <1.3 <1.3 <1.3 <1.3 <14 <1.34 <1.70 <1.3 <1.3 <1.3 <1.3 <1.3 <14 <1.34 <1.70
4.6 J 2.1 J <24 <24 <24 21 <3.69 <3.69 3.2 J <24 <24 <24 <24 <6.0 <3.69 <3.69
54 J 1.7 J 4.4 J <6.2 <6.2 45 <0.622 <0.622 12 J <6.2 <6.2 <6.2 <6.2 15 <0.622 <0.622
0.73 J <1.3 <1.3 <1.3 <1.3 <13 14.5 <1.26 <1.3 <1.3 <1.3 <1.3 <1.3 <13 <1.26 <1.26
<0.98 <0.98 <0.98 <0.98 0.55 <10 <0.973 <0.973 0.57 J 0.61 J 1.7 2.8 3.8 <9.9 5.60 <0.973
NA NA NA NA NA <8.7 0.568 <0.413 NA NA NA NA NA <8.4 <0.413 <0.413
49 <0.69 <0.69 <0.69 <0.69 NA NA 1.28 <1.4 <0.69 <0.69 <0.69 <0.69 NA NA 6.44
<1.7 <1.7 <1.7 <1.7 <1.7 <18 <1.70 <1.34 <1.7 <1.7 <1.7 <1.7 <1.7 <17 <1.70 <1.34
<1.2 <1.2 <1.2 <1.2 <1.2 <13 <1.20 <1.20 <1.2 <1.2 <1.2 <1.2 <1.2 <12 <1.20 <1.20
3.1 2.4 <0.99 <0.99 <0.99 <10 1.91 1.85 3.4 2.5 <0.99 <0.99 <0.99 <10 2.22 1.78
<0.81 <0.81 <0.81 <0.81 <0.81 <8.5 <0.802 <0.802 3.9 3.0 3.3 3.1 3.7 <8.2 3.70 2.71
<0.79 <0.79 <0.79 <0.79 <0.79 <8.4 <0.793 <0.793 5.6 3.2 <0.79 3.0 <0.79 <8.0 3.69 2.92
<0.79 <0.79 <0.79 <0.79 <0.79 <8.4 <0.793 <0.793 <0.79 <0.79 <0.79 <0.79 <0.79 <8.0 <0.793 <0.793
<0.79 <0.79 <0.79 <0.79 <0.79 <8.4 <0.793 <0.793 2.3 J <0.79 <0.79 <0.79 <0.79 <8.0 <0.793 <0.793
<15 <15 14 J <15 9.4 NA NA 17.9 9.4 J <15 10 J <15 12 NA NA <2.36
<0.72 <0.72 <7.2 <7.2 <7.2 NA NA <0.720 4.1 <0.72 <0.72 <7.2 <7.2 NA NA <0.720
0.76 J <0.87 <0.87 <0.87 <0.87 <9.1 <0.867 <0.867 0.69 J <0.87 <0.87 <0.87 <0.87 <8.8 <0.867 <0.867
8.9 <0.82 <0.82 <0.82 <0.82 NA NA <0.818 1.8 <0.82 <0.82 <0.82 <0.82 NA NA <0.818
23 J <28 <28 <28 <28 NA NA <2.22 3.4 J <28 <28 <28 <28 NA NA <2.22
<0.82 <0.82 <0.82 <0.82 <0.82 <8.6 <5.12 <5.12 <0.82 <0.82 <0.82 <0.82 <0.82 <8.3 <5.12 <5.12
1.4 J <6.9 <6.9 <6.9 <6.9 <7.3 <0.694 0.844 2.3 J <6.9 <6.9 <6.9 <6.9 <7.0 0.847 <0.694
<1.0 <1.0 <1.0 <1.0 <1.0 NA NA <3.30 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA <3.30
63 <14 <14 <14 <14 NA NA <2.15 <14 <14 <14 <14 <14 NA NA <2.15
12 460 88 34 22.5 33.2 210 210 250 240 266 251
<0.59 <0.59 <5.9 <5.9 <5.9 NA NA <0.590 <0.59 <0.59 <5.9 <5.9 <5.9 NA NA <0.590
29 <0.75 <0.75 <0.75 <0.75 <7.9 <1.88 <1.88 11 <0.75 <0.75 <0.75 <0.75 <7.6 <1.88 <1.88
20 130 230 110 90.8 63.6 230 240 230 260 247 228
<1.1 <1.1 <1.1 <1.1 <1.1 <11 <1.07 <1.07 1.0 J 0.58 J 0.60 J <1.1 <1.1 <11 1.54 <1.07
3.9 J 7.2 9.5 5.7 <4.5 <12 1.99 4.19 14 16 17 14 15 14 13.0 13.7
1.1 J <6.1 <6.1 <6.1 <6.1 <16 <1.53 <1.53 <6.1 <6.1 <6.1 <6.1 <6.1 <15 <1.53 <1.53
<0.98 <0.98 <0.98 <0.98 <0.98 <10 <0.982 <0.982 <0.98 <0.98 <0.98 <0.98 <0.98 <9.9 <0.982 <0.982
<0.98 <0.98 <0.98 <0.98 <0.98 <10 <0.982 <0.982 <0.98 <0.98 <0.98 <0.98 <0.98 <9.9 <0.982 <0.982
8.4 <0.87 <0.87 <0.87 <2.6 NA <0.867 <0.867 2.5 J <0.87 <0.87 <0.87 <2.6 NA <0.867 <0.867
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Table 4
Soil Gas Historical Summary
Flemington Mills Brownfield Project
Forest City, North Carolina
Location:
Non-Residential (1)
VOCs (EPA TO-15)
Acetone NE
Benzene 160
Bromodichloromethane 33
2-Butanone (MEK)440,000
Carbon Disulfide 61,000
Carbon Tetrachloride 200
Chloroform 53
Chloromethane 625
Cyclohexane 530,000
Dibromochloromethane NE
1,3-Dichlorobenzene NE
Dichlorodifluoromethane (Freon 12)8,800
1,1-Dichloroethane 770
1,1-Dichloroethylene 18,000
cis-1,2-Dichloroethylene NE
trans-1,2-Dichloroethylene 3,500
Ethanol NE
Ethyl Acetate 6,100
Ethylbenzene 490
Heptane 35,000
Hexane 61,000
4-Methyl-2-pentanone (MIBK)260,000
Methylene Chloride 53,000
Naphthalene 36
Propene 260,000
Tetrachloroethylene 3,500
Tetrahydrofuran 180,000
Toluene 440,000
1,1,1-Trichloroethane 440,000
Trichloroethylene 180
Trichlorofluoromethane (Freon 11)NE
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)440,000
1,2,4-Trimethylbenzene 5,300
1,3,5-Trimethylbenzene 5,300
Xylenes (total)8,800
Sub-slab and
Exterior Soil Gas
Screening Level VP-9 VP-9 VP-9 VP-9 VP-9 VP-9 VP-9 VP-9 VP-10 VP-10 VP-10 VP-10 VP-10 VP-10 VP-10
19 <19 <19 <19 12 <9.2 6.32 6.34 <19 40 <19 14 22 <2.97 <2.97
0.74 <0.64 <0.64 <0.64 <0.64 <6.2 <0.639 <0.639 9.9 3.5 <0.64 <0.64 <6.5 <0.639 <0.639
20 <1.3 <1.3 <1.3 <1.3 <13 <1.34 <1.70 <1.3 <1.3 <1.3 <1.3 <14 <1.34 <1.70
20 J <24 <24 <24 <24 <5.7 <3.69 <3.69 6.3 J 3.6 J <24 <24 <6.0 <3.69 <3.69
6.9 J <6.2 <6.2 <6.2 <6.2 37 <0.622 <0.622 60 J <6.2 <6.2 <6.2 120 <0.622 <0.622
<1.3 <1.3 <1.3 <1.3 <1.3 <12 <1.26 <1.26 0.75 J <1.3 <1.3 <1.3 <13 <1.26 <1.26
120 0.57 J 13 <0.98 15 <9.5 13.1 <0.973 <0.98 1.2 <0.98 1.5 <9.9 <0.973 <0.973
NA NA NA NA NA <8.0 <0.413 <0.413 NA NA NA NA <8.4 <0.413 <0.413
<1.4 <0.69 <0.69 <0.69 <0.69 NA NA <0.689 <1.4 <0.69 <0.69 <0.69 NA NA <0.689
4.2 <1.7 <1.7 <1.7 <1.7 <17 <1.70 <1.34 <1.7 <1.7 <1.7 <1.7 <17 <1.70 <1.34
<1.2 <1.2 <1.2 <1.2 <1.2 <12 <1.20 <1.20 25 5.4 7.1 15 <12 4.89 1.82
2.8 <0.99 <0.99 <0.99 <0.99 <9.6 1.97 1.64 <0.99 <0.99 <0.99 <0.99 <10 2.07 1.63
<0.81 <0.81 <0.81 <0.81 <0.81 <7.9 <0.802 <0.802 <0.81 <0.81 <0.81 <0.81 <8.2 <0.802 <0.802
<0.79 <0.79 <0.79 <0.79 <0.79 <7.7 <0.793 <0.793 <0.79 <0.79 <0.79 <0.79 <8.0 <0.793 <0.793
<0.79 <0.79 <0.79 <0.79 <0.79 <7.7 <0.793 <0.793 <0.79 <0.79 <0.79 <0.79 <8.0 10.1 <0.793
<0.79 <0.79 <0.79 <0.79 <0.79 <7.7 <0.793 <0.793 <0.79 <0.79 <0.79 <0.79 <8.0 <0.793 <0.793
<15 <15 6.4 J <15 26 NA NA 27.3 <15 6.2 J <15 11 NA NA <2.36
<0.72 <0.72 <7.2 <7.2 <7.2 NA NA 0.831 <0.72 <7.2 <7.2 <7.2 NA NA <0.720
<0.87 <0.87 <0.87 <0.87 <0.87 <8.4 <0.867 <0.867 5.0 0.92 <0.87 <0.87 <8.8 <0.867 <0.867
2.0 <0.82 <0.82 <0.82 <0.82 NA NA <0.818 51 <0.82 <0.82 <0.82 NA NA <0.818
4.5 J <28 <28 <28 <28 NA NA <2.22 83 <28 <28 <28 NA NA <2.22
<0.82 <0.82 <0.82 <0.82 <0.82 <8.0 <5.12 <5.12 <0.82 <0.82 <0.82 <0.82 <8.3 <5.12 <5.12
1.1 J <6.9 <6.9 <6.9 <6.9 <6.8 1.61 <0.694 <6.9 <6.9 <6.9 <6.9 <7.0 <0.694 <0.694
<1.0 <1.0 <1.0 <1.0 <1.0 NA NA <3.30 <1.0 <1.0 <1.0 <1.0 NA NA <3.30
<14 <14 <14 <14 <14 NA NA <2.15 740 J 5.2 J <14 <14 NA NA <2.15
300 270 1300 260 1,350 282 820 6.7 950 1,690 1,190
120 <0.59 <5.9 <5.9 <5.9 NA NA <0.590 <0.59 <5.9 <5.9 <5.9 NA NA <0.590
5.8 <0.75 <0.75 <0.75 2.2 <7.3 <1.88 <1.88 130 4.5 <0.75 <0.75 <7.6 <1.88 <1.88
1.3 1.6 4.4 2.1 <11 5.33 1.37 1.9 <1.1 3.7 <11 5.44 3.20
<1.1 <1.1 <1.1 <1.1 <1.1 <10 <1.07 <1.07 <1.1 <1.1 <1.1 <1.1 <11 64.3 <1.07
3.7 J 5.0 8.4 <4.5 6.1 <11 4.90 2.32 2.5 J 1.3 J 7.5 8.6 <11 7.42 5.68
<6.1 <6.1 <6.1 <6.1 <6.1 <15 <1.53 <1.53 <6.1 <6.1 <6.1 <6.1 <15 <1.53 <1.53
<0.98 <0.98 <0.98 <0.98 <0.98 <9.6 <0.982 <0.982 6.4 <0.98 <0.98 <0.98 <9.9 <0.982 <0.982
0.63 J <0.98 <0.98 <0.98 <0.98 <9.6 <0.982 <0.982 1.8 <0.98 <0.98 <0.98 <9.9 <0.982 <0.982
1.6 J <0.87 <0.87 <0.87 <2.6 NA <0.867 <0.867 15 3.2 <0.87 <2.6 NA <0.867 <0.867
\\na.aecomnet.com\LFS\AMER\Raleigh-USRAL3\DCS\Projects\ENV\60613889_FCBRWNFLDX\500_Deliverables\502_Monitoring rpts\2023\23_ 02 rpt\Tables\Table 4 2019-2023 Forest City Soil Gas_HL_NL.xlsx Page 4 of 4
Table 4
Soil Gas Historical Summary
Flemington Mills Brownfield Project
Forest City, North Carolina
Notes:
(1) NC DEQ Non-Residential Vapor Intrusion Screening Levels, effective February 2018
< # - Not detected at the specified reporting limit
EPA - Enviromental Protection Agency
J - Estimated value
MIBK - Methyl isobutyl ketone
NC DEQ - North Carolina Department of Environmental Quality
NE - Not established
VOC - Volatile organic compound
This table presents a summary of results for analytes detected in soil gas samples that were collected at the site since February 2019. All sample results are reported in
micrograms per cubic meter (µg/m³).
Sample concentrations greater than the NC DEQ Non-residential vapor intrusion soil gas screening levels are highlighted. Sample detections are bold.
\\na.aecomnet.com\LFS\AMER\Raleigh-USRAL3\DCS\Projects\ENV\60613889_FCBRWNFLDX\500_Deliverables\502_Monitoring rpts\2023\23_ 02 rpt\Tables\Table 4 2019-2023 Forest City Soil Gas_HL_NL.xlsx
Figures
VP-1VP-2
VP-3VP-4
VP-9VP-10
VP-7VP-8 VP-5VP-6
Project Management Initials: Designer: TSH Checked: SDB Approved: CDFFilename: C:\USERS\BIVOLARUL\AECOM\GDS GIS SERVICES - GIS CAD PROJECTS\DCS AMERICAS\SHELL\NORTH CAROLINA\20230511\_EDITS20230512\02. WORKSPACE\FOREST CITY.DWG
SOIL GAS RESULTS
2021-2023
Figure: 1
FLORENCE MILL BROWNFIELDBROWNFIELD PROJECT NO. 29003-05-81
FOREST CITY, NORTH CAROLINA
Project No.: 60686695 Date: 2023-05-12
Reference: ODEM ENGINEERING, PLLC, FINAL AS-BUILT, 2019Aerial: NC ONE MAPS GEOSPATIAL DATABASE, (3-7-2015)
NOT SAMPLED DUE TO WATER
PRESENT IN MONITORING POINTNS
TETRACHLOROETHENE
TRICHLOROETHENE
PCE
TCE
LEGEND
BELOW DETECTION LIMIT
MICROGRAMS PER CUBIC METER
BDL
µg/m³
SOIL VAPOR POINT PAIR (Feb. 2019)
PRE-EXISTING MONITORING WELL
BROWNFIELDS PERIMETER
MONITORING WELL (Feb. 2019)
SOIL GAS RESULTS (µg/m³)266
BELOW GROUND SURFACEbgs
Attachment A
Field Notes
Page____ of ____
Field Personnel:
Date:Project Number:
Daily Objective:
Daily Activity Log
Project Manager:
Client: Project Name:

Site:
Samplers:
Date:
Sample#
Location
Summa Canister ID
Flow Controller ID
NO/NO/NO/NO/NO/
Purge Time (Start)
Purge Time (Stop)
Total Purge Time (min)
Purge Volume
PID Test of Purge Air
Initial Tracer Gas Results
Sample Time (Start)
Sample Time (Stop)
Total Sample Time (min)
Sample Volume
YES / NO YES / NO YES / NO YES / NO YES / NO
Final Tracer Gas Results
Summa Canister Sampling Field Data Sheet

Site:
Samplers:
Date:
Sample#
Location
Summa Canister ID
Flow Controller ID
NO/NO/NO/NO/NO/
Purge Time (Start)
Purge Time (Stop)
Total Purge Time (min)
Purge Volume
PID Test of Purge Air
Initial Tracer Gas Results
Sample Time (Start)
Sample Time (Stop)
Total Sample Time (min)
Sample Volume
YES / NO YES / NO YES / NO YES / NO YES / NO
Final Tracer Gas Results
Summa Canister Sampling Field Data Sheet
CamScanner
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Daily Tailgate Meeting (S3AM-209-FM5) Revision 10 June 1. 2021PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET. 1 of 2
Americas
Daily Tailgate Meeting S3AM-209-FM5
Instructions: Conduct meeting prior to sending crews to individual tasks. Require attendance of all AECOM employees and subcontractors. Invite personnel from simultaneous operations for coordination purposes. Review scope of work and briefly discuss required and applicable topics. This meeting is a daily refresher, not a full orientation. Task-specific discussions associated with Task Hazard Assessment (THA) follow this meeting e n immediately beforeindividual task is started.
Date: Project Name/Location: Project Number:
Today’s Scope of Work:
Muster Point Location: First Aid Kit Location: Fire Extinguisher Location: Spill Kit Location:
1.Required Topics 2.Discuss if Applicable to Today’s Work
Check as reviewed or mark as not applicable
Biological/ Chemical / Electrical Hazards
Ergonomics - Lifting, Body Position
Lock Out/ Tag Out
Short Service Employees - visual identifier and mentor/
oversight assignment
Simultaneous/ Neighbouring Operations
Slip/ Trip/ Fall Hazards
Specialized PPE Needs
Traffic Control
Waste Management/ Decontamination
Weather Hazards / Heat Stress / Cold Stress
Subcontractor Requirements (e.g., JHAs, THAs,
procedures, reporting, etc.)
Work Permits / Plans required (e.g., Fall Protection,
Confined Space, Hot Work, etc.); in place,
understood (identify/attac ):
Other Topics (describe/attach):
Client specific requirements (describe):
3.Daily Check Out by Site Supervisor
The site is being left in a safe condition and work crew checked out as fit unless otherwise specified as above.
Site Supervisor Name Signature Date
Time (at end of day / shift)
Worker Acknowledgement / Sign In Sign Out sheets applicable to this meeting are on reverse and, if applicable, attached.
rir
h r

h r
tig r
Fitness for Duty requirements, all sign in / sign out
Required training (incl. task specific) completed and current
SH&E Plan onsite nderstood, reieed, signed all
(incl. scope, preplanning aard assessents / risk
registers, controls, procedres, reireents, etc.)
Task Hazard Assessments (THAs) are to be reieed and completed for each task immediately prior to conducting
STOP WORK Right & Responsibility- all task changes/changed conditions re-assess with THA
Requirement to report to supervisor any injury, illness, damage, near iss, nsafe act / condition
Emergency Response Plan – including muster point, first aid kit, fire extinguisher, clinic/hospital location
Personal Protective Equipment (PPE) - Required items per hazard assessments in good condition / in use by all
Equipment/machinery inspected (documented as required) and in good condition - operators properly trained/certified
Work area set up and demarcation/ barricades in place to protect workers, site staff, and the public
eired cecklists/records aailale, nderstood (describe):
essons earned / SH iproeents (descrie)
DCS Americas - This form may be replaced by the electronic Daily Tailgate Meeting Tool. Link - Ecosystem Daily Tailgate Meeting App Site
✔■

Daily Tailgate Meeting (S3AM-209-FM5) Revision 10 June 1, 2021PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET. 2 of 2
(Attach additional Site Worker sign-in/out sheets if needed) Identify number of attached sheets:
SITE VISITOR / SITE REPRESENTATIVE
Name Company Name Arrival Time Departure Time Signature
All employees:
STOP WORK if concerned / uncertain about safety / hazard or additional precaution is not recorded on the THA.
Be alert and communicate any changes in personnel or conditions at the worksite to the supervisor.
Reassess task, hazards, & mitigations on an ongoing basis; amend the THA if needed.
*The requirement to participate in creating, reviewing, updating hazard assessments (THA) applicable to your task(s).
The hazards control measures associated with each task you are about to perform.
Your authority obligation to “Stop Work” intervene, speak up/ listen up.
Your initials (right columns) certify that you arrived & departed fit for duty, & have reported all incidents/near misses; meaning:
*You are physically and mentally fit for duty n e nee u eue enue nn
* You are not under the influence of any type of medication, drugs, or alcohol that could affect your ability to work safely.*You are aware of your responsibility to immediately report any illness, injury (regardless of where or when it occurred), or
enue issue to the AECOM Supervisor.
* You signed out as fit / uninjured unless you have otherwise informed the AECOM Supervisor.
Print Name & Company Signature Initials & Sign In Time Initials & Sign Out Time
_________
Task Hazard Assessment

DCSA Task Hazard Assessment Form
Version 1 – October 22, 2018 1 of 4
Task Name: Summa Canister Sampling Control #: 01-01-22-04

Project Name: Client: Date:
Permits Required? (list): Work Location:
This THA must be fully reviewed with all staff members. All job steps, hazards, work practices, and PPE are clearly understood and have been implemented. All necessary revisions have been written on the THA.
Required PPE: Hard Hat Safety Glasses HiVis Vest Safety Toe Boots Gloves: Leather Hearing Protection Other:

Tools & Equipment: Summa canister Wrenches Tubing

REMINDER: Use 4-Sight at the start of, and continuously throughout the job/task to identify additional and/or hazards to act on!
Job Steps
List all steps required to perform
a task in the sequence they
are performed
Potential Hazards
How could you be hurt?
What would the injury be?
Risk
(initial)
Critical Actions To Mitigate Hazards
List control measures required to eliminate, control or protect against the
potential hazards associated with each job step to minimize the risk of
injury or environmental impact. Identify any ‘Stop Work’ triggers.
Risk
(final)
1. Set up equipment 1a. Muscle strain

1b. Equipment damage

1c. Pinch points, lacerations

1d. Tool/equipment failure caused by use
6

3

6

3
1a. Use proper precautions (lift with legs, not back) when lifting equipment into/out of vehicle. If lifting >50 lbs, use the buddy system. Avoid twisting, stooping, and/or extended reaching positions when handling or moving equipment.

1b. Use a solid work surface when assembling summa canisters to avoid dropping or damaging equipment. Work from the ground surface, floor, or the tailgate of the truck when applicable. Adhere to laboratory assembly instructions. Use correct size
wrenches to connect fittings. Ensure wrenches are properly seated on fittings prior to loosening or tightening fittings.

1c. Wear leather gloves to prevent hand injury in case the wrench slips off a fitting or while cutting tubing.

1d. Conduct physical inspection of all equipment. Worn or broken tools should be repaired or replaced.
4

2

1

1
On-
Site
Edits:

2. Collect Sample 2a. Slips, trips, falls

6

2a. Maintain clean and organized work area; keep walking paths clear of equipment and debris.

3

Task Hazard Analysis

Task Name: Error! Reference source not found. Control #: Error! Reference source not found.

DCSA Task Hazard Assessment Form
Version 1 – October 22, 2018 2 of 4
REMINDER: Use 4-Sight at the start of, and continuously throughout the job/task to identify additional and/or hazards to act on!
Job Steps
List all steps required to perform
a task in the sequence they
are performed
Potential Hazards
How could you be hurt?
What would the injury be?
Risk
(initial)
Critical Actions To Mitigate Hazards
List control measures required to eliminate, control or protect against the
potential hazards associated with each job step to minimize the risk of
injury or environmental impact. Identify any ‘Stop Work’ triggers.
Risk
(final)
2b. Injury from poor ergonomics 6 2b. Maintain proper body positioning/good ergonomic form. Avoid stooping and twisting. 2
On-
Site
Edits:

3. Pack Sample Cooler 3a. Muscle strain 6 3a. Use proper lifting techniques (lift with legs, not back) and use buddy system if lifting items >50 pounds. Avoid twisting, stooping, and/or extended reaching body positions when moving full coolers.
2
On-
Site
Edits:

Additional Notes:

Task Hazard Analysis

Task Name: Error! Reference source not found. Control #: Error! Reference source not found.

DCSA Task Hazard Assessment Form
Version 1 – October 22, 2018 3 of 4
All Employees:
STOP WORK if uncertain about safety or if a hazard or additional precaution is not recorded on the THA.
Be alert, recognize and communicate any changes in scope, personnel or conditions at the worksite to the supervisor.
Use 4-Sight, AECOM’s last minute risk assessment process continuously throughout the day by asking yourself and your co-workers to assess your task, hazards, and mitigations. Amend the THA when needed.
 What am I about to do?
 What can go wrong?
 What can be done to make it safer?
 What have I done to communicate the hazards?
For a more thorough identification of hazards, ask “What else could go wrong?” using the Hazard Categories

 Most hazards need more than one control
 What should you do? Stack your controls
 PPE can NEVER be your only means of protection

Worker Sign On Visitor Acknowledgement
I participated in the on-site review and fully understand the content of this Task Hazard Assessment. Visitors review task hazards and acknowledge understanding Printed Name Signature
1. Supervisor: 1.
2. 2.
3. 3.
4. 4.
5. 5.
6. 6.
7. 7.
8. 8.
9. 9.
10. 10.
Submit a new THA for addition to the DCSA THA Library or send THA improvement suggestions to [e-mail]
Vehicle Inspection Checklist (S3AM-005-FM2)
Revision 9 January 15, 2019
PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET.1 of 2
Americas
Vehicle Inspection Checklist S3AM-005-FM2
Vehicle Tag No: Mileage:Date:Time:Driver Name:Location:
Inspection Checklist:This Pre-Trip Vehicle Inspection Checklist is intended to be completed by the vehicle driver prior
to departing on a trip. Checking boxes means that item is present and functioning. Deficiencies that affect or could
potentially affect the safe operation of the vehicle shall be repaired or corrected prior to departure. This checklist should
only be used in addition to an on-going vehicle maintenance program.
Item Yes No N/A
1. General
1-1 Proof of insurance and registration available and current?
1-2 Is the date of the last regular maintenance known, or is the mileage/date of next scheduledmaintenance known?
1-3 Is the overall condition of the vehicle good (no body damage, unusual sounds, leaks, odors, etc.)?
2. Tires
2-1 Do all tires have sufficient tread for driving conditions? Legal limit: 2/32” (for rain/snow: > 4/32”)
2-2 Are tires sufficiently inflated for driving conditions?
2-3 Are the lug nuts and stem caps present and tight for each tire?
2-4 Is the spare tire and jack present and in good condition?
3. Vehicle Interior
3-1 Are the brake and accelerator pedal pads in good condition?
3-2 Are the floor mats in good condition and not interfering with the brake or accelerator pedals?
3-3 Is the seat properly adjusted (including the headrest)?
3-4 Is the seatbelt in good condition?
3-5 Are the mirrors in good condition (not broken, dirty)?
3-6 Are the dashboard/instrument lights working?
3-7 Is the dashboard free of warning lights and do the gauges appear to work when the car is started?
3-8 Does the horn work?
3-9 Are distractions such as cell phones and GPS units secured so they do not encourage use?
4. Lights and Signals
4-1 Do the headlights and high beams work?
4-2 Do the tail lights function properly?
4-3 Do the turn signals work (front and rear)?
4-4 Do the brake lights work (including high light in the rear window if applicable)?
4-5 Do the hazard lights (emergency flashers) work?
4-6 Do back up / reverse lights work?
4-7 If equipped with a back-up alarm can it be heard clearly?
5. Mechanical
5-1 Do the brakes work and feel solid (not soft)?
5-2 Does the parking/emergency brake work?
5-3 Is the steering in good working condition (not loose)?
5-4 Is the engine oil level full or in the operating zone?
5-5 Excessive vehicle bounce going over bumps reported (possible sign of worn shock absorbers)?
5-4 Is the fuel level full or at an adequate level for the proposed usage?

Vehicle Inspection Checklist (S3AM-005-FM2)
Revision 9 January 15, 2019
PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET.2 of 2
Item Yes No N/A
6. Windows and Windshield
6-1 Is the windshield clean and unbroken?
6-2 Are the wiper blades in good condition (front and rear)?
6-3 Are all the windows clean and unbroken and windshield fluid available and operational?
7. Emergency Equipment (as needed per conditions/project requirements)
7-1 Is there a “Safety Kit” (fire extinguisher, first aid, safety triangle and 2 reflective vests)?
7-2 Is there a first aid kit, has it been inspected recently?
7-3 Is survival gear and equipment available (blanket, water, heat source, flashlight, etc.)?
7-4 Is a means for emergency communication available?
8. Other Equipment (as needed per conditions/project requirements)
8-1 Is there a means to secured loads (cargo next, container)?
8-2 Are cones or other warning devices available?
8-3 Is weather specific equipment (snow chains, tires etc.)?
8-4 Does the vehicle have a snow brush/ice scraper?
8-5 Does the vehicle have a fire extinguisher?
9. Comments
Inspector Name:Signature:Date:
Attachment B
Laboratory Analytical Reports
Project Name: Florence Mill
Date: March 2023
Page No.: 1
1
Re: Florence Mill Brownfield DATA VALIDATION CERTIFICATION
SDG: 92653572

To Whom It May Concern:
I, Hannah Lucas, as a chemist of the data validation staff of AECOM in Raleigh, North Carolina,
certify that to the best of my knowledge and belief, the data validation for the field samples
collected from the Florence Brownfield site during February of 2023 was performed in
accordance with Method 8260D.
The laboratory analyzed these samples within the recommended analytical holding time and
performed dilutions appropriately and correctly. For all results, the data of interest appear to be
generally acceptable.
Sincerely,

Hannah Lucas
Project Name: Florence Mill
Date: March 2023
Page No.: 2
2
DATA VALIDATION REPORT
INTRODUCTION
During February of 2023, groundwater samples from two locations were collected from the
Florence Brownfield site. The samples were forwarded under chain of custody to Pace Analytical
Services in Huntsville, NC for analysis of a site-specific set of volatile organic compounds
(VOC). The samples were received under chain of custody, intact, and in good condition. In
accordance with the provisions of the approved work plan, one hundred percent of the data were
validated to a Stage 2A level. This report is applicable to the field sample data from the
following locations:
Pace SDG Sample ID Pace Lab Sample ID 8260D
9265372 MW-1R 92653572001 X
MW-17 92653572002 X
The analytical procedures employed in the course of the analyses are taken from United States
Environmental Protection Agency (USEPA)
(USEPA) SW-846, Test Methods for Evaluating Solid Wastes. The correct and current methods
as specified in the work plan were used by the laboratory.
.
The data were validated using USEPA National Functional Guidelines for Organic Superfund Data Review (November 2020, EPA 540-R-20-005). These were applied to the methods of
analysis such that the specifications of the methods take precedence over the specifications of the
validation protocol in those instances where the specifications differ.
The analytical data packages and the data validation notes are on file at AECOM’s Raleigh,
North Carolina office and are available for review upon request. In the sections that follow, the
findings of the validation effort are presented. Each review begins with a listing of the validation
parameters assessed. An asterisk before any individual item indicates that the data were
determined to be acceptable in that area of review or that element was not discussed further in
the report. Specifically, the data are deemed to be acceptable if (1) all technical criteria were met,
or (2) any observed failures have no impact on data quality and no data qualification is indicated.
Data qualifiers would be applied to the data to indicate that some of the data may be considered
estimated values, the result of background contamination, or unusable. The flags used in the
report are defined at the end of the report.

Project Name: Florence Mill
Date: March 2023
Page No.: 3
3
Volatile 8260D Organic Compounds
* • Holding Times
* • Method Blanks
* • Laboratory Control Spike/Laboratory Control Spike Duplicate (LCS/LCSD)
• Matrix Spike/Matrix Spike Duplicate (MS/MSD)
* • Surrogate Recovery
* • Sample Dilutions

1. Holding Times
The method holding time for 8260D is 14 days from sample collection, samples were analyzed
within analytical holding time:
Sample Date Collected Date Analyzed Days
MW-1R 02/21/2023 12:15 02/23/2023 14:21 2
MW-17 02/21/2023 11:12 02/23/2023 23:38 2

2. Method Blanks
The method blanks associated with samples were below reporting limit.

3. Laboratory Control Spike/Laboratory Control Spike Duplicate (LCS/LCSD)
The LCS/LCSD recoveries for all samples were within the laboratory control limits.

4. Matrix Spike/Matrix Spike Duplicate (MS/MSD)
The MS and MSD performed on field sample MW-1R displayed percent recoveries less than the
lower quality control limit for all analytes due to sample dilution. Therefore, qualification of data
is unwarranted.

5. Surrogate Recovery
Surrogate recovery for all samples was within the method requirement of 70-130% recovery.

6. Sample Dilutions
Samples were analyzed at a standard dilution of approximately 1x and were analyzed at higher
dilutions due to high concentrations:
Sample Dilution concentration (µg/L)
MW-1R 10 Tetrachloroethene (1,600)
These dilutions were performed appropriately and correctly.
#=CL#
February 27, 2023
LIMS USE: FR - CONAN FITZGERALD
LIMS OBJECT ID: 92653572
92653572
Project:
Pace Project No.:
RE:
Conan Fitzgerald
AECOM
5438 Wade Park Blvd
Suite 200
Raleigh, NC 27607
FLORENCE MILL BROWNFIELD-FORES
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s) received by the laboratory on February 22, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 17
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 17
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92653572001 MW-1R EPA 8260D 63 PASI-CSAS
92653572002 MW-17 EPA 8260D 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Sample: MW-1R Lab ID: 92653572001 Collected: 02/21/23 12:15 Received: 02/22/23 11:12 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/23/23 14:21 67-64-1 M1250 10
Benzene ND ug/L 02/23/23 14:21 71-43-2 M110.0 10
Bromobenzene ND ug/L 02/23/23 14:21 108-86-1 M110.0 10
Bromochloromethane ND ug/L 02/23/23 14:21 74-97-5 M110.0 10
Bromodichloromethane ND ug/L 02/23/23 14:21 75-27-4 M110.0 10
Bromoform ND ug/L 02/23/23 14:21 75-25-2 M110.0 10
Bromomethane ND ug/L 02/23/23 14:21 74-83-9 M1,v220.0 10
2-Butanone (MEK)ND ug/L 02/23/23 14:21 78-93-3 M150.0 10
Carbon tetrachloride ND ug/L 02/23/23 14:21 56-23-5 M1,v110.0 10
Chlorobenzene ND ug/L 02/23/23 14:21 108-90-7 M110.0 10
Chloroethane ND ug/L 02/23/23 14:21 75-00-3 M110.0 10
Chloroform ND ug/L 02/23/23 14:21 67-66-3 M110.0 10
Chloromethane ND ug/L 02/23/23 14:21 74-87-3 M110.0 10
2-Chlorotoluene ND ug/L 02/23/23 14:21 95-49-8 M110.0 10
4-Chlorotoluene ND ug/L 02/23/23 14:21 106-43-4 M110.0 10
1,2-Dibromo-3-chloropropane ND ug/L 02/23/23 14:21 96-12-8 M120.0 10
Dibromochloromethane ND ug/L 02/23/23 14:21 124-48-1 M110.0 10
1,2-Dibromoethane (EDB)ND ug/L 02/23/23 14:21 106-93-4 M110.0 10
Dibromomethane ND ug/L 02/23/23 14:21 74-95-3 M110.0 10
1,2-Dichlorobenzene ND ug/L 02/23/23 14:21 95-50-1 M110.0 10
1,3-Dichlorobenzene ND ug/L 02/23/23 14:21 541-73-1 M110.0 10
1,4-Dichlorobenzene ND ug/L 02/23/23 14:21 106-46-7 M110.0 10
Dichlorodifluoromethane ND ug/L 02/23/23 14:21 75-71-8 M110.0 10
1,1-Dichloroethane ND ug/L 02/23/23 14:21 75-34-3 M110.0 10
1,2-Dichloroethane ND ug/L 02/23/23 14:21 107-06-2 M110.0 10
1,1-Dichloroethene ND ug/L 02/23/23 14:21 75-35-4 M1,v110.0 10
cis-1,2-Dichloroethene ND ug/L 02/23/23 14:21 156-59-2 M110.0 10
trans-1,2-Dichloroethene ND ug/L 02/23/23 14:21 156-60-5 M110.0 10
1,2-Dichloropropane ND ug/L 02/23/23 14:21 78-87-5 M110.0 10
1,3-Dichloropropane ND ug/L 02/23/23 14:21 142-28-9 M110.0 10
2,2-Dichloropropane ND ug/L 02/23/23 14:21 594-20-7 M110.0 10
1,1-Dichloropropene ND ug/L 02/23/23 14:21 563-58-6 M110.0 10
cis-1,3-Dichloropropene ND ug/L 02/23/23 14:21 10061-01-5 M110.0 10
trans-1,3-Dichloropropene ND ug/L 02/23/23 14:21 10061-02-6 M110.0 10
Diisopropyl ether ND ug/L 02/23/23 14:21 108-20-3 M110.0 10
Ethylbenzene ND ug/L 02/23/23 14:21 100-41-4 M110.0 10
Hexachloro-1,3-butadiene ND ug/L 02/23/23 14:21 87-68-3 M120.0 10
2-Hexanone ND ug/L 02/23/23 14:21 591-78-6 M150.0 10
p-Isopropyltoluene ND ug/L 02/23/23 14:21 99-87-6 M110.0 10
Methylene Chloride ND ug/L 02/23/23 14:21 75-09-2 M150.0 10
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/23 14:21 108-10-1 M150.0 10
Methyl-tert-butyl ether ND ug/L 02/23/23 14:21 1634-04-4 M110.0 10
Naphthalene ND ug/L 02/23/23 14:21 91-20-3 M110.0 10
Styrene ND ug/L 02/23/23 14:21 100-42-5 M110.0 10
1,1,1,2-Tetrachloroethane ND ug/L 02/23/23 14:21 630-20-6 M110.0 10
1,1,2,2-Tetrachloroethane ND ug/L 02/23/23 14:21 79-34-5 M110.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2023 08:55 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Sample: MW-1R Lab ID: 92653572001 Collected: 02/21/23 12:15 Received: 02/22/23 11:12 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Tetrachloroethene 1600 ug/L 02/23/23 14:21 127-18-4 M110.0 10
Toluene ND ug/L 02/23/23 14:21 108-88-3 M110.0 10
1,2,3-Trichlorobenzene ND ug/L 02/23/23 14:21 87-61-6 M110.0 10
1,2,4-Trichlorobenzene ND ug/L 02/23/23 14:21 120-82-1 M110.0 10
1,1,1-Trichloroethane ND ug/L 02/23/23 14:21 71-55-6 M110.0 10
1,1,2-Trichloroethane ND ug/L 02/23/23 14:21 79-00-5 M110.0 10
Trichloroethene ND ug/L 02/23/23 14:21 79-01-6 M110.0 10
Trichlorofluoromethane ND ug/L 02/23/23 14:21 75-69-4 M110.0 10
1,2,3-Trichloropropane ND ug/L 02/23/23 14:21 96-18-4 M110.0 10
Vinyl acetate ND ug/L 02/23/23 14:21 108-05-4 IK,M120.0 10
Vinyl chloride ND ug/L 02/23/23 14:21 75-01-4 M110.0 10
Xylene (Total)ND ug/L 02/23/23 14:21 1330-20-7 MS10.0 10
m&p-Xylene ND ug/L 02/23/23 14:21 179601-23-1 M120.0 10
o-Xylene ND ug/L 02/23/23 14:21 95-47-6 M110.0 10
Surrogates
4-Bromofluorobenzene (S)100 %02/23/23 14:21 460-00-470-130 10
1,2-Dichloroethane-d4 (S)104 %02/23/23 14:21 17060-07-070-130 10
Toluene-d8 (S)104 %02/23/23 14:21 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2023 08:55 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Sample: MW-17 Lab ID: 92653572002 Collected: 02/21/23 12:50 Received: 02/22/23 11:12 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/23/23 17:03 67-64-125.0 1
Benzene ND ug/L 02/23/23 17:03 71-43-21.0 1
Bromobenzene ND ug/L 02/23/23 17:03 108-86-11.0 1
Bromochloromethane ND ug/L 02/23/23 17:03 74-97-51.0 1
Bromodichloromethane ND ug/L 02/23/23 17:03 75-27-41.0 1
Bromoform ND ug/L 02/23/23 17:03 75-25-21.0 1
Bromomethane ND ug/L 02/23/23 17:03 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 02/23/23 17:03 78-93-35.0 1
Carbon tetrachloride ND ug/L 02/23/23 17:03 56-23-5 v11.0 1
Chlorobenzene ND ug/L 02/23/23 17:03 108-90-71.0 1
Chloroethane ND ug/L 02/23/23 17:03 75-00-31.0 1
Chloroform ND ug/L 02/23/23 17:03 67-66-31.0 1
Chloromethane ND ug/L 02/23/23 17:03 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/23/23 17:03 95-49-81.0 1
4-Chlorotoluene ND ug/L 02/23/23 17:03 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 02/23/23 17:03 96-12-82.0 1
Dibromochloromethane ND ug/L 02/23/23 17:03 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 02/23/23 17:03 106-93-41.0 1
Dibromomethane ND ug/L 02/23/23 17:03 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 02/23/23 17:03 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 02/23/23 17:03 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 02/23/23 17:03 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 02/23/23 17:03 75-71-81.0 1
1,1-Dichloroethane ND ug/L 02/23/23 17:03 75-34-31.0 1
1,2-Dichloroethane ND ug/L 02/23/23 17:03 107-06-21.0 1
1,1-Dichloroethene ND ug/L 02/23/23 17:03 75-35-4 v11.0 1
cis-1,2-Dichloroethene ND ug/L 02/23/23 17:03 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 02/23/23 17:03 156-60-51.0 1
1,2-Dichloropropane ND ug/L 02/23/23 17:03 78-87-51.0 1
1,3-Dichloropropane ND ug/L 02/23/23 17:03 142-28-91.0 1
2,2-Dichloropropane ND ug/L 02/23/23 17:03 594-20-71.0 1
1,1-Dichloropropene ND ug/L 02/23/23 17:03 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 02/23/23 17:03 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 02/23/23 17:03 10061-02-61.0 1
Diisopropyl ether ND ug/L 02/23/23 17:03 108-20-31.0 1
Ethylbenzene ND ug/L 02/23/23 17:03 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 02/23/23 17:03 87-68-32.0 1
2-Hexanone ND ug/L 02/23/23 17:03 591-78-65.0 1
p-Isopropyltoluene ND ug/L 02/23/23 17:03 99-87-61.0 1
Methylene Chloride ND ug/L 02/23/23 17:03 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/23 17:03 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 02/23/23 17:03 1634-04-41.0 1
Naphthalene ND ug/L 02/23/23 17:03 91-20-31.0 1
Styrene ND ug/L 02/23/23 17:03 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 02/23/23 17:03 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 02/23/23 17:03 79-34-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2023 08:55 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Sample: MW-17 Lab ID: 92653572002 Collected: 02/21/23 12:50 Received: 02/22/23 11:12 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Tetrachloroethene 166 ug/L 02/23/23 17:03 127-18-41.0 1
Toluene ND ug/L 02/23/23 17:03 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 02/23/23 17:03 87-61-61.0 1
1,2,4-Trichlorobenzene 1.6 ug/L 02/23/23 17:03 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 02/23/23 17:03 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 02/23/23 17:03 79-00-51.0 1
Trichloroethene ND ug/L 02/23/23 17:03 79-01-61.0 1
Trichlorofluoromethane ND ug/L 02/23/23 17:03 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/23/23 17:03 96-18-41.0 1
Vinyl acetate ND ug/L 02/23/23 17:03 108-05-4 IK2.0 1
Vinyl chloride ND ug/L 02/23/23 17:03 75-01-41.0 1
Xylene (Total)ND ug/L 02/23/23 17:03 1330-20-71.0 1
m&p-Xylene ND ug/L 02/23/23 17:03 179601-23-12.0 1
o-Xylene ND ug/L 02/23/23 17:03 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %02/23/23 17:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %02/23/23 17:03 17060-07-070-130 1
Toluene-d8 (S)104 %02/23/23 17:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2023 08:55 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
757725
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92653572001, 92653572002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3936180
Associated Lab Samples:92653572001, 92653572002
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/23/23 13:26
1,1,1-Trichloroethane ug/L ND 1.0 02/23/23 13:26
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/23/23 13:26
1,1,2-Trichloroethane ug/L ND 1.0 02/23/23 13:26
1,1-Dichloroethane ug/L ND 1.0 02/23/23 13:26
1,1-Dichloroethene ug/L ND 1.0 v102/23/23 13:26
1,1-Dichloropropene ug/L ND 1.0 02/23/23 13:26
1,2,3-Trichlorobenzene ug/L ND 1.0 02/23/23 13:26
1,2,3-Trichloropropane ug/L ND 1.0 02/23/23 13:26
1,2,4-Trichlorobenzene ug/L ND 1.0 02/23/23 13:26
1,2-Dibromo-3-chloropropane ug/L ND 2.0 02/23/23 13:26
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/23/23 13:26
1,2-Dichlorobenzene ug/L ND 1.0 02/23/23 13:26
1,2-Dichloroethane ug/L ND 1.0 02/23/23 13:26
1,2-Dichloropropane ug/L ND 1.0 02/23/23 13:26
1,3-Dichlorobenzene ug/L ND 1.0 02/23/23 13:26
1,3-Dichloropropane ug/L ND 1.0 02/23/23 13:26
1,4-Dichlorobenzene ug/L ND 1.0 02/23/23 13:26
2,2-Dichloropropane ug/L ND 1.0 02/23/23 13:26
2-Butanone (MEK)ug/L ND 5.0 02/23/23 13:26
2-Chlorotoluene ug/L ND 1.0 02/23/23 13:26
2-Hexanone ug/L ND 5.0 02/23/23 13:26
4-Chlorotoluene ug/L ND 1.0 02/23/23 13:26
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/23/23 13:26
Acetone ug/L ND 25.0 02/23/23 13:26
Benzene ug/L ND 1.0 02/23/23 13:26
Bromobenzene ug/L ND 1.0 02/23/23 13:26
Bromochloromethane ug/L ND 1.0 02/23/23 13:26
Bromodichloromethane ug/L ND 1.0 02/23/23 13:26
Bromoform ug/L ND 1.0 02/23/23 13:26
Bromomethane ug/L ND 2.0 v202/23/23 13:26
Carbon tetrachloride ug/L ND 1.0 v102/23/23 13:26
Chlorobenzene ug/L ND 1.0 02/23/23 13:26
Chloroethane ug/L ND 1.0 02/23/23 13:26
Chloroform ug/L ND 1.0 02/23/23 13:26
Chloromethane ug/L ND 1.0 02/23/23 13:26
cis-1,2-Dichloroethene ug/L ND 1.0 02/23/23 13:26
cis-1,3-Dichloropropene ug/L ND 1.0 02/23/23 13:26
Dibromochloromethane ug/L ND 1.0 02/23/23 13:26
Dibromomethane ug/L ND 1.0 02/23/23 13:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2023 08:55 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3936180
Associated Lab Samples:92653572001, 92653572002
Matrix: Water
Analyzed
Dichlorodifluoromethane ug/L ND 1.0 02/23/23 13:26
Diisopropyl ether ug/L ND 1.0 02/23/23 13:26
Ethylbenzene ug/L ND 1.0 02/23/23 13:26
Hexachloro-1,3-butadiene ug/L ND 2.0 02/23/23 13:26
m&p-Xylene ug/L ND 2.0 02/23/23 13:26
Methyl-tert-butyl ether ug/L ND 1.0 02/23/23 13:26
Methylene Chloride ug/L ND 5.0 02/23/23 13:26
Naphthalene ug/L ND 1.0 02/23/23 13:26
o-Xylene ug/L ND 1.0 02/23/23 13:26
p-Isopropyltoluene ug/L ND 1.0 02/23/23 13:26
Styrene ug/L ND 1.0 02/23/23 13:26
Tetrachloroethene ug/L ND 1.0 02/23/23 13:26
Toluene ug/L ND 1.0 02/23/23 13:26
trans-1,2-Dichloroethene ug/L ND 1.0 02/23/23 13:26
trans-1,3-Dichloropropene ug/L ND 1.0 02/23/23 13:26
Trichloroethene ug/L ND 1.0 02/23/23 13:26
Trichlorofluoromethane ug/L ND 1.0 02/23/23 13:26
Vinyl acetate ug/L ND 2.0 IK02/23/23 13:26
Vinyl chloride ug/L ND 1.0 02/23/23 13:26
Xylene (Total)ug/L ND 1.0 02/23/23 13:26
1,2-Dichloroethane-d4 (S)%105 70-130 02/23/23 13:26
4-Bromofluorobenzene (S)%98 70-130 02/23/23 13:26
Toluene-d8 (S)%109 70-130 02/23/23 13:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3936181LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.820 109 70-130
1,1,1-Trichloroethane ug/L 23.020 115 70-130
1,1,2,2-Tetrachloroethane ug/L 21.520 108 70-130
1,1,2-Trichloroethane ug/L 21.320 106 70-130
1,1-Dichloroethane ug/L 22.020 110 70-130
1,1-Dichloroethene ug/L 24.0 v120120 70-130
1,1-Dichloropropene ug/L 25.320 127 70-130
1,2,3-Trichlorobenzene ug/L 18.620 93 70-130
1,2,3-Trichloropropane ug/L 19.020 95 70-130
1,2,4-Trichlorobenzene ug/L 19.520 98 70-130
1,2-Dibromo-3-chloropropane ug/L 20.220 101 70-131
1,2-Dibromoethane (EDB)ug/L 21.120 105 70-130
1,2-Dichlorobenzene ug/L 20.320 102 70-130
1,2-Dichloroethane ug/L 22.620 113 70-130
1,2-Dichloropropane ug/L 22.020 110 70-130
1,3-Dichlorobenzene ug/L 21.220 106 70-130
1,3-Dichloropropane ug/L 22.120 110 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2023 08:55 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3936181LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 20.120 101 70-130
2,2-Dichloropropane ug/L 23.120 115 68-135
2-Butanone (MEK)ug/L 43.640 109 70-134
2-Chlorotoluene ug/L 20.320 102 70-130
2-Hexanone ug/L 40.040 100 70-131
4-Chlorotoluene ug/L 21.020 105 70-130
4-Methyl-2-pentanone (MIBK)ug/L 41.240 103 70-130
Acetone ug/L 42.940 107 70-133
Benzene ug/L 21.120 105 70-130
Bromobenzene ug/L 20.220 101 70-130
Bromochloromethane ug/L 22.120 110 70-130
Bromodichloromethane ug/L 21.020 105 70-130
Bromoform ug/L 20.820 104 70-130
Bromomethane ug/L 11.3 v32057 45-151
Carbon tetrachloride ug/L 21.4 v120107 70-130
Chlorobenzene ug/L 21.320 107 70-130
Chloroethane ug/L 24.020 120 39-152
Chloroform ug/L 23.120 115 70-130
Chloromethane ug/L 19.120 96 58-130
cis-1,2-Dichloroethene ug/L 22.720 114 70-130
cis-1,3-Dichloropropene ug/L 21.720 109 70-130
Dibromochloromethane ug/L 21.220 106 70-130
Dibromomethane ug/L 20.720 104 70-130
Dichlorodifluoromethane ug/L 14.320 71 54-133
Diisopropyl ether ug/L 20.420 102 70-130
Ethylbenzene ug/L 21.120 106 70-130
Hexachloro-1,3-butadiene ug/L 20.320 102 70-135
m&p-Xylene ug/L 42.440 106 70-130
Methyl-tert-butyl ether ug/L 22.420 112 70-130
Methylene Chloride ug/L 21.020 105 66-130
Naphthalene ug/L 18.920 95 70-130
o-Xylene ug/L 20.920 105 70-130
p-Isopropyltoluene ug/L 20.620 103 70-130
Styrene ug/L 22.020 110 70-130
Tetrachloroethene ug/L 21.020 105 70-130
Toluene ug/L 20.520 103 70-130
trans-1,2-Dichloroethene ug/L 22.220 111 70-130
trans-1,3-Dichloropropene ug/L 20.320 102 70-130
Trichloroethene ug/L 22.120 110 70-130
Trichlorofluoromethane ug/L 20.820 104 62-130
Vinyl acetate ug/L 36.3 IK4091 70-144
Vinyl chloride ug/L 19.620 98 62-130
Xylene (Total)ug/L 63.360 106 70-130
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2023 08:55 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3936182MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653572001
3936183
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L M12001170-14111 6200ND22.5 21.1
1,1,1-Trichloroethane ug/L M12001170-15012 7200ND22.0 23.6
1,1,2,2-Tetrachloroethane ug/L M12001269-14213 8200ND23.6 25.5
1,1,2-Trichloroethane ug/L M12001270-13813 9200ND24.1 26.3
1,1-Dichloroethane ug/L M12001270-15013 8200ND23.5 25.6
1,1-Dichloroethene ug/L M1,v12001170-15612 8200ND22.4 24.2
1,1-Dichloropropene ug/L M1200970-15010 11200ND18.1 20.2
1,2,3-Trichlorobenzene ug/L M1200970-14810 9200ND17.6 19.4
1,2,3-Trichloropropane ug/L M12001270-14012 1200ND24.0 24.2
1,2,4-Trichlorobenzene ug/L M12001070-14611 12200ND19.6 22.1
1,2-Dibromo-3-chloropropane ug/L M1200968-14613200ND17.9J 26.8
1,2-Dibromoethane (EDB)ug/L M12001170-1389 17200ND22.2 18.8
1,2-Dichlorobenzene ug/L M12001170-14111 3200ND22.9 22.1
1,2-Dichloroethane ug/L M12001269-14313 1200ND25.0 25.1
1,2-Dichloropropane ug/L M12001268-15612 2200ND23.4 23.8
1,3-Dichlorobenzene ug/L M12001170-14311 6200ND21.4 22.6
1,3-Dichloropropane ug/L M12001170-13811 2200ND21.6 21.9
1,4-Dichlorobenzene ug/L M12001070-14210 3200ND20.3 19.8
2,2-Dichloropropane ug/L M12001052-17010 0200ND20.9 20.9
2-Butanone (MEK)ug/L M14001260-15712400ND46.7J 46.1J
2-Chlorotoluene ug/L M12001170-14712 2200ND22.6 23.1
2-Hexanone ug/L M14001168-14611400ND42.6J 45.6J
4-Chlorotoluene ug/L M12001170-14211 1200ND22.3 22.4
4-Methyl-2-pentanone (MIBK) ug/L M14001270-14112400ND48.3J ND
Acetone ug/L M14001358-15715400ND52.8J 59.6J
Benzene ug/L M1200870-1429 10200ND21.0 23.1
Bromobenzene ug/L M12001270-14312 0200ND23.7 23.7
Bromochloromethane ug/L M12001270-14612 4200ND24.7 23.7
Bromodichloromethane ug/L M12001170-13912 14200ND21.5 24.6
Bromoform ug/L M12001064-14011 5200ND21.0 22.1
Bromomethane ug/L M1,v32001128-19211 2200ND22.7 22.1
Carbon tetrachloride ug/L M1,v12001170-14812 1200ND22.8 23.0
Chlorobenzene ug/L M12001170-14111 1200ND22.6 22.5
Chloroethane ug/L M12001258-19112 0200ND23.4 23.3
Chloroform ug/L M12001370-14814 6200ND26.3 27.9
Chloromethane ug/L M12001343-16210 24200ND25.2 19.8
cis-1,2-Dichloroethene ug/L M12001268-15113 4200ND24.5 25.4
cis-1,3-Dichloropropene ug/L M12001070-13911 8200ND19.7 21.4
Dibromochloromethane ug/L M12001070-14412 17200ND20.7 24.5
Dibromomethane ug/L M12001170-13911 1200ND22.1 22.3
Dichlorodifluoromethane ug/L M1200739-1718 14200ND13.1 15.0
Diisopropyl ether ug/L M12001067-14210 1200ND21.3 21.5
Ethylbenzene ug/L M12001070-14311 7200ND20.0 21.5
Hexachloro-1,3-butadiene ug/L M12001064-16310200ND19.6J 19.8J
m&p-Xylene ug/L M14001070-14411 4400ND41.8 43.7
Methyl-tert-butyl ether ug/L M12001065-14310 4200ND19.5 20.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2023 08:55 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3936182MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653572001
3936183
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L M12001062-14910200ND40.8J 41.8J
Naphthalene ug/L M1200967-1479 7200ND17.4 18.6
o-Xylene ug/L M12001170-14510 4200ND21.7 20.9
p-Isopropyltoluene ug/L M12001070-14711 7200ND19.7 21.1
Styrene ug/L M12001070-14311 15200ND19.1 22.1
Tetrachloroethene ug/L M1200-84 70-145-59 320016001440 1490
Toluene ug/L M12001270-14212 0200ND23.7 23.8
trans-1,2-Dichloroethene ug/L M12001370-15113 3200ND25.3 26.0
trans-1,3-Dichloropropene ug/L M12001270-13911 6200ND23.6 22.1
Trichloroethene ug/L M12001162-14612 2200ND22.7 23.1
Trichlorofluoromethane ug/L M12001063-15310 8200ND19.2 20.8
Vinyl acetate ug/L IK,M14001161-16212 2400ND45.4 46.4
Vinyl chloride ug/L M1200961-16310 11200ND17.6 19.7
Xylene (Total)ug/L MS6001170-14311 2600ND63.6 64.6
1,2-Dichloroethane-d4 (S)%102 70-130103
4-Bromofluorobenzene (S)%98 70-130101
Toluene-d8 (S)%103 70-130105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2023 08:55 AM
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2023 08:55 AM
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9800 Kincey Ave. Suite 100
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Page 13 of 17
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92653572
FLORENCE MILL BROWNFIELD-FORES
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92653572001 757725MW-1R EPA 8260D
92653572002 757725MW-17 EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2023 08:55 AM
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Page 14 of 17
Page 15 of 17
Page 16 of 17
Page 17 of 17
Project Name: Florence Mill
Date: March 2023
Page No.: 1
1
Re: Florence Mill Brownfield DATA VALIDATION CERTIFICATION
SDG: 92653832

To Whom It May Concern:
I, Hannah Lucas, as a chemist of the data validation staff of AECOM in Raleigh, North Carolina,
certify that to the best of my knowledge and belief, the data validation for the field samples
collected from the Florence Brownfield site during February of 2023 was performed in
accordance with Method TO-15.
The laboratory analyzed these samples within the recommended analytical holding time and
performed dilutions appropriately and correctly. For all results, the data of interest appear to be
generally acceptable.
Sincerely,

Hannah Lucas

Project Name: Florence Mill
Date: March 2023
Page No.: 2
2
DATA VALIDATION REPORT
INTRODUCTION
During February of 2023, air samples from nine locations were collected from the Florence
Brownfield site. The samples were forwarded under chain of custody to Pace Analytical Services
in Huntsville, NC for analysis of a site-specific set of volatile organic compounds under
Compendium Method TO-15. The samples were received under chain of custody, intact, and in
good condition. In accordance with the provisions of the approved work plan, one hundred
percent of the data were validated to a Stage 2A level. This report is applicable to the field
sample data from the following locations:
Pace SDG Sample ID Pace Lab Sample ID TO-15
92653832
VP-1 9265383201 X
VP-2 9265383202 X VP-3 9265383203 X VP-4 9265383204 X
VP-6 9265383205 X VP-7 9265383206 X VP-8 9265383207 X VP-9 9265383208 X
VP-10 9265383209 X
The analytical procedures employed in the course of the analyses are taken from United States
Environmental Protection Agency (USEPA) Ambient Monitoring Technology Information
Center (AMTIC) Compendium of Methods for the Determination of Toxic Organic Compounds
in Ambient Air.
The data were validated using USEPA National Functional Guidelines for Organic Superfund
Data Review (November 2020, EPA 540-R-20-005). These were applied to the methods of
analysis such that the specifications of the methods take precedence over the specifications of the
validation protocol in those instances where the specifications differ.
The analytical data packages and the data validation notes are on file at AECOM’s Raleigh,
North Carolina office and are available for review upon request. In the sections that follow, the
findings of the validation effort are presented. Each review begins with a listing of the validation
parameters assessed. An asterisk before any individual item indicates that the data were
determined to be acceptable in that area of review or that element was not discussed further in
the report. Specifically, the data are deemed to be acceptable if (1) all technical criteria were met,
or (2) any observed failures have no impact on data quality and no data qualification is indicated.
Data qualifiers would be applied to the data to indicate that some of the data may be considered
estimated values, the result of background contamination, or unusable. The flags used in the
report are defined at the end of the report.

Project Name: Florence Mill
Date: March 2023
Page No.: 3
3
TO-15 Volatile Organic Compounds
* • Holding Times
* • Method Blanks
* • Laboratory Control Spike/Laboratory Control Spike Duplicate (LCS/LCSD)
* • Surrogate Recovery
* • Sample Dilutions
1. Holding Times
The method holding time for TO-15 is 30 days from sample collection, samples were analyzed
within analytical holding time:
Sample Date Collected Date Analyzed Days
VP-1 2/21/2023 10:40 2/24/2023 13:41 3
VP-2 2/21/2023 10:40 2/25/2023 00:57 3
VP-3 2/21/2023 10:58 2/25/2023 00:18 3
VP-4 2/21/2023 10:58 2/25/2023 01:36 3
VP-6 2/21/2023 14:36 2/24/2023 14:21 3
VP-7 2/21/2023 15:44 2/24/2023 15:00 3
VP-8 2/21/2023 15:44 2/24/2023 15:41 3
VP-9 2/21/2023 12:05 2/24/2023 16:21 3
VP-10 2/21/2023 12:05 2/24/2023 17:01 3
2. Method Blanks
The method blanks associated with samples were below reporting limit.
3. Laboratory Control Spike/Laboratory Control Spike Duplicate (LCS/LCSD)
Laboratory Control Spike/Laboratory Control Spike Duplicate recovery for all samples was
within the method requirement of 70-130% recovery.
4. Surrogate Recovery
Surrogate recovery for all samples was within the method requirement of 70-130% recovery.
5. Sample Dilutions
Samples were analyzed at a standard pressure dilution of approximately 1x and were analyzed at
higher dilutions due to high concentrations:
Sample Dilution (µg/m3)
VP-1 400 Tetrachloroethene (24,000)
VP-2 2000 Tetrachloroethene (1,190,000)
VP-3 5000 Tetrachloroethene (629,000)
VP-4 10000 Tetrachloroethene (6,710,000)
VP-10 10 Tetrachloroethene (1,190)
These dilutions were performed appropriately and correctly.
#=CL#
February 28, 2023
LIMS USE: FR - CONAN FITZGERALD
LIMS OBJECT ID: 92653832
92653832
Project:
Pace Project No.:
RE:
Conan Fitzgerald
AECOM
5438 Wade Park Blvd
Suite 200
Raleigh, NC 27607
Forest City Brownfield
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s) received by the laboratory on February 21, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 32
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 32
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92653832
Forest City Brownfield
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92653832001 VP-1 TO-15 69 PANDAH
92653832002 VP-2 TO-15 69 PANDAH, DBB
92653832003 VP-3 TO-15 69 PANDAH, DBB
92653832004 VP-4 TO-15 69 PANDAH, DBB
92653832005 VP-6 TO-15 69 PANDAH, DBB
92653832006 VP-7 TO-15 69 PANDAH
92653832007 VP-8 TO-15 69 PANDAH
92653832008 VP-9 TO-15 69 PANDAH
92653832009 VP-10 TO-15 69 PANDAH, DBB
PAN = Pace National - Mt. Juliet
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Page 3 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-1 Lab ID: 92653832001 Collected: 02/21/23 10:40 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Acetone ND ug/m3 02/24/23 13:41 67-64-102/24/23 13:412.97 1
Allyl chloride ND ug/m3 02/24/23 13:41 107-05-102/24/23 13:410.626 1
Benzene ND ug/m3 02/24/23 13:41 71-43-202/24/23 13:410.639 1
Benzyl chloride ND ug/m3 02/24/23 13:41 100-44-702/24/23 13:411.04 1
Bromodichloromethane ND ug/m3 02/24/23 13:41 75-27-402/24/23 13:411.34 1
Bromoform ND ug/m3 02/24/23 13:41 75-25-202/24/23 13:416.21 1
Bromomethane ND ug/m3 02/24/23 13:41 74-83-902/24/23 13:410.776 1
1,3-Butadiene ND ug/m3 02/24/23 13:41 106-99-002/24/23 13:414.43 1
Carbon disulfide ND ug/m3 02/24/23 13:41 75-15-002/24/23 13:410.622 1
Carbon tetrachloride 2.95 ug/m3 02/24/23 13:41 56-23-502/24/23 13:411.26 1
Chlorobenzene ND ug/m3 02/24/23 13:41 108-90-702/24/23 13:410.924 1
Chloroethane ND ug/m3 02/24/23 13:41 75-00-302/24/23 13:410.528 1
Chloroform ND ug/m3 02/24/23 13:41 67-66-302/24/23 13:410.973 1
Chloromethane ND ug/m3 02/24/23 13:41 74-87-302/24/23 13:410.413 1
2-Chlorotoluene ND ug/m3 02/24/23 13:41 95-49-802/24/23 13:411.03 1
Cyclohexane ND ug/m3 02/24/23 13:41 110-82-702/24/23 13:410.689 1
Dibromochloromethane ND ug/m3 02/24/23 13:41 124-48-102/24/23 13:411.70 1
1,2-Dibromoethane (EDB)ND ug/m3 02/24/23 13:41 106-93-402/24/23 13:411.54 1
1,2-Dichlorobenzene ND ug/m3 02/24/23 13:41 95-50-102/24/23 13:411.20 1
1,3-Dichlorobenzene ND ug/m3 02/24/23 13:41 541-73-102/24/23 13:411.20 1
1,4-Dichlorobenzene ND ug/m3 02/24/23 13:41 106-46-702/24/23 13:411.20 1
1,2-Dichloroethane ND ug/m3 02/24/23 13:41 107-06-202/24/23 13:410.810 1
1,1-Dichloroethane ND ug/m3 02/24/23 13:41 75-34-302/24/23 13:410.802 1
1,1-Dichloroethene ND ug/m3 02/24/23 13:41 75-35-402/24/23 13:410.793 1
cis-1,2-Dichloroethene ND ug/m3 02/24/23 13:41 156-59-202/24/23 13:410.793 1
trans-1,2-Dichloroethene ND ug/m3 02/24/23 13:41 156-60-502/24/23 13:410.793 1
1,2-Dichloropropane ND ug/m3 02/24/23 13:41 78-87-502/24/23 13:410.924 1
cis-1,3-Dichloropropene ND ug/m3 02/24/23 13:41 10061-01-502/24/23 13:410.908 1
trans-1,3-Dichloropropene ND ug/m3 02/24/23 13:41 10061-02-602/24/23 13:410.908 1
1,4-Dioxane (p-Dioxane)ND ug/m3 02/24/23 13:41 123-91-102/24/23 13:410.721 1
Ethanol ND ug/m3 02/24/23 13:41 64-17-502/24/23 13:412.36 1
Ethylbenzene ND ug/m3 02/24/23 13:41 100-41-402/24/23 13:410.867 1
Ethyl acetate ND ug/m3 02/24/23 13:41 141-78-602/24/23 13:410.720 1
4-Ethyltoluene ND ug/m3 02/24/23 13:41 622-96-802/24/23 13:410.982 1
Trichlorofluoromethane 5.96 ug/m3 02/24/23 13:41 75-69-402/24/23 13:411.12 1
Dichlorodifluoromethane 1.43 ug/m3 02/24/23 13:41 75-71-802/24/23 13:410.989 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 02/24/23 13:41 76-13-102/24/23 13:411.53 1
Dichlorotetrafluoroethane ND ug/m3 02/24/23 13:41 76-14-202/24/23 13:411.40 1
n-Heptane ND ug/m3 02/24/23 13:41 142-82-502/24/23 13:410.818 1
Hexachloro-1,3-butadiene ND ug/m3 02/24/23 13:41 87-68-302/24/23 13:416.73 1
n-Hexane ND ug/m3 02/24/23 13:41 110-54-302/24/23 13:412.22 1
Isopropylbenzene (Cumene)ND ug/m3 02/24/23 13:41 98-82-802/24/23 13:410.983 1
Methylene Chloride ND ug/m3 02/24/23 13:41 75-09-202/24/23 13:410.694 1
2-Hexanone ND ug/m3 02/24/23 13:41 591-78-602/24/23 13:415.11 1
2-Butanone (MEK)ND ug/m3 02/24/23 13:41 78-93-302/24/23 13:413.69 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 02/24/23 13:41 108-10-102/24/23 13:415.12 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
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Page 4 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-1 Lab ID: 92653832001 Collected: 02/21/23 10:40 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Methyl methacrylate ND ug/m3 02/24/23 13:41 80-62-602/24/23 13:410.819 1
Methyl-tert-butyl ether ND ug/m3 02/24/23 13:41 1634-04-402/24/23 13:410.721 1
Naphthalene ND ug/m3 02/24/23 13:41 91-20-302/24/23 13:413.30 1
2-Propanol ND ug/m3 02/24/23 13:41 67-63-002/24/23 13:413.07 1
Propylene ND ug/m3 02/24/23 13:41 115-07-102/24/23 13:412.15 1
Styrene ND ug/m3 02/24/23 13:41 100-42-502/24/23 13:410.851 1
1,1,2,2-Tetrachloroethane ND ug/m3 02/24/23 13:41 79-34-502/24/23 13:411.37 1
Tetrachloroethene 24000 ug/m3 02/27/23 18:13 127-18-402/27/23 18:13543 400
Tetrahydrofuran ND ug/m3 02/24/23 13:41 109-99-902/24/23 13:410.590 1
Toluene ND ug/m3 02/24/23 13:41 108-88-302/24/23 13:411.88 1
1,2,4-Trichlorobenzene ND ug/m3 02/24/23 13:41 120-82-102/24/23 13:414.66 1
1,1,1-Trichloroethane ND ug/m3 02/24/23 13:41 71-55-602/24/23 13:411.09 1
1,1,2-Trichloroethane ND ug/m3 02/24/23 13:41 79-00-502/24/23 13:411.09 1
Trichloroethene 3.16 ug/m3 02/24/23 13:41 79-01-602/24/23 13:411.07 1
1,2,4-Trimethylbenzene ND ug/m3 02/24/23 13:41 95-63-602/24/23 13:410.982 1
1,3,5-Trimethylbenzene ND ug/m3 02/24/23 13:41 108-67-802/24/23 13:410.982 1
2,2,4-Trimethylpentane ND ug/m3 02/24/23 13:41 540-84-102/24/23 13:410.934 1
Vinyl chloride ND ug/m3 02/24/23 13:41 75-01-402/24/23 13:410.511 1
Vinyl bromide ND ug/m3 02/24/23 13:41 593-60-202/24/23 13:410.875 1
Vinyl acetate ND ug/m3 02/24/23 13:41 108-05-402/24/23 13:410.704 1
m&p-Xylene ND ug/m3 02/24/23 13:41 179601-23-102/24/23 13:411.73 1
o-Xylene ND ug/m3 02/24/23 13:41 95-47-602/24/23 13:410.867 1
Surrogates
1,4-Dichlorobenzene-d4 (IS)96.0 %02/24/23 13:41 3855-82-102/24/23 13:4160.0-140 1
1,4-Dichlorobenzene-d4 (IS)95.0 %02/27/23 18:13 3855-82-102/27/23 18:1360.0-140 400
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
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Page 5 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-2 Lab ID: 92653832002 Collected: 02/21/23 10:40 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Acetone ND ug/m3 02/25/23 00:57 67-64-102/25/23 00:572380 800
Allyl chloride ND ug/m3 02/25/23 00:57 107-05-102/25/23 00:57501 800
Benzene ND ug/m3 02/25/23 00:57 71-43-202/25/23 00:57511 800
Benzyl chloride ND ug/m3 02/25/23 00:57 100-44-702/25/23 00:57831 800
Bromodichloromethane ND ug/m3 02/25/23 00:57 75-27-402/25/23 00:571070 800
Bromoform ND ug/m3 02/25/23 00:57 75-25-202/25/23 00:574970 800
Bromomethane ND ug/m3 02/25/23 00:57 74-83-902/25/23 00:57621 800
1,3-Butadiene ND ug/m3 02/25/23 00:57 106-99-002/25/23 00:573540 800
Carbon disulfide ND ug/m3 02/25/23 00:57 75-15-002/25/23 00:57498 800
Carbon tetrachloride ND ug/m3 02/25/23 00:57 56-23-502/25/23 00:571010 800
Chlorobenzene ND ug/m3 02/25/23 00:57 108-90-702/25/23 00:57739 800
Chloroethane ND ug/m3 02/25/23 00:57 75-00-302/25/23 00:57422 800
Chloroform ND ug/m3 02/25/23 00:57 67-66-302/25/23 00:57779 800
Chloromethane ND ug/m3 02/25/23 00:57 74-87-302/25/23 00:57330 800
2-Chlorotoluene ND ug/m3 02/25/23 00:57 95-49-802/25/23 00:57825 800
Cyclohexane ND ug/m3 02/25/23 00:57 110-82-702/25/23 00:57551 800
Dibromochloromethane ND ug/m3 02/25/23 00:57 124-48-102/25/23 00:571360 800
1,2-Dibromoethane (EDB)ND ug/m3 02/25/23 00:57 106-93-402/25/23 00:571230 800
1,2-Dichlorobenzene ND ug/m3 02/25/23 00:57 95-50-102/25/23 00:57962 800
1,3-Dichlorobenzene ND ug/m3 02/25/23 00:57 541-73-102/25/23 00:57962 800
1,4-Dichlorobenzene ND ug/m3 02/25/23 00:57 106-46-702/25/23 00:57962 800
1,2-Dichloroethane ND ug/m3 02/25/23 00:57 107-06-202/25/23 00:57648 800
1,1-Dichloroethane ND ug/m3 02/25/23 00:57 75-34-302/25/23 00:57641 800
1,1-Dichloroethene ND ug/m3 02/25/23 00:57 75-35-402/25/23 00:57634 800
cis-1,2-Dichloroethene ND ug/m3 02/25/23 00:57 156-59-202/25/23 00:57634 800
trans-1,2-Dichloroethene ND ug/m3 02/25/23 00:57 156-60-502/25/23 00:57634 800
1,2-Dichloropropane ND ug/m3 02/25/23 00:57 78-87-502/25/23 00:57739 800
cis-1,3-Dichloropropene ND ug/m3 02/25/23 00:57 10061-01-502/25/23 00:57726 800
trans-1,3-Dichloropropene ND ug/m3 02/25/23 00:57 10061-02-602/25/23 00:57726 800
1,4-Dioxane (p-Dioxane)ND ug/m3 02/25/23 00:57 123-91-102/25/23 00:57577 800
Ethanol ND ug/m3 02/25/23 00:57 64-17-502/25/23 00:571890 800
Ethylbenzene ND ug/m3 02/25/23 00:57 100-41-402/25/23 00:57694 800
Ethyl acetate ND ug/m3 02/25/23 00:57 141-78-602/25/23 00:57576 800
4-Ethyltoluene ND ug/m3 02/25/23 00:57 622-96-802/25/23 00:57785 800
Trichlorofluoromethane ND ug/m3 02/25/23 00:57 75-69-402/25/23 00:57899 800
Dichlorodifluoromethane ND ug/m3 02/25/23 00:57 75-71-802/25/23 00:57791 800
1,1,2-Trichlorotrifluoroethane ND ug/m3 02/25/23 00:57 76-13-102/25/23 00:571230 800
Dichlorotetrafluoroethane ND ug/m3 02/25/23 00:57 76-14-202/25/23 00:571120 800
n-Heptane ND ug/m3 02/25/23 00:57 142-82-502/25/23 00:57654 800
Hexachloro-1,3-butadiene ND ug/m3 02/25/23 00:57 87-68-302/25/23 00:575380 800
n-Hexane 2190 ug/m3 02/25/23 00:57 110-54-302/25/23 00:571780 800
Isopropylbenzene (Cumene)ND ug/m3 02/25/23 00:57 98-82-802/25/23 00:57787 800
Methylene Chloride ND ug/m3 02/25/23 00:57 75-09-202/25/23 00:57556 800
2-Hexanone ND ug/m3 02/25/23 00:57 591-78-602/25/23 00:574090 800
2-Butanone (MEK)ND ug/m3 02/25/23 00:57 78-93-302/25/23 00:572950 800
4-Methyl-2-pentanone (MIBK)ND ug/m3 02/25/23 00:57 108-10-102/25/23 00:574090 800
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-2 Lab ID: 92653832002 Collected: 02/21/23 10:40 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Methyl methacrylate ND ug/m3 02/25/23 00:57 80-62-602/25/23 00:57655 800
Methyl-tert-butyl ether ND ug/m3 02/25/23 00:57 1634-04-402/25/23 00:57577 800
Naphthalene ND ug/m3 02/25/23 00:57 91-20-302/25/23 00:572640 800
2-Propanol 6860 ug/m3 02/25/23 00:57 67-63-002/25/23 00:572460 800
Propylene ND ug/m3 02/25/23 00:57 115-07-102/25/23 00:571720 800
Styrene ND ug/m3 02/25/23 00:57 100-42-502/25/23 00:57681 800
1,1,2,2-Tetrachloroethane ND ug/m3 02/25/23 00:57 79-34-502/25/23 00:571100 800
Tetrachloroethene 1190000 ug/m3 02/25/23 20:57 127-18-402/25/23 20:572720 2000
Tetrahydrofuran ND ug/m3 02/25/23 00:57 109-99-902/25/23 00:57472 800
Toluene ND ug/m3 02/25/23 00:57 108-88-302/25/23 00:571510 800
1,2,4-Trichlorobenzene ND ug/m3 02/25/23 00:57 120-82-102/25/23 00:573730 800
1,1,1-Trichloroethane ND ug/m3 02/25/23 00:57 71-55-602/25/23 00:57870 800
1,1,2-Trichloroethane ND ug/m3 02/25/23 00:57 79-00-502/25/23 00:57870 800
Trichloroethene ND ug/m3 02/25/23 00:57 79-01-602/25/23 00:57857 800
1,2,4-Trimethylbenzene ND ug/m3 02/25/23 00:57 95-63-602/25/23 00:57785 800
1,3,5-Trimethylbenzene ND ug/m3 02/25/23 00:57 108-67-802/25/23 00:57785 800
2,2,4-Trimethylpentane ND ug/m3 02/25/23 00:57 540-84-102/25/23 00:57747 800
Vinyl chloride ND ug/m3 02/25/23 00:57 75-01-402/25/23 00:57409 800
Vinyl bromide ND ug/m3 02/25/23 00:57 593-60-202/25/23 00:57700 800
Vinyl acetate ND ug/m3 02/25/23 00:57 108-05-402/25/23 00:57563 800
m&p-Xylene ND ug/m3 02/25/23 00:57 179601-23-102/25/23 00:571390 800
o-Xylene ND ug/m3 02/25/23 00:57 95-47-602/25/23 00:57694 800
Surrogates
1,4-Dichlorobenzene-d4 (IS)92.4 %02/25/23 00:57 3855-82-102/25/23 00:5760.0-140 800
1,4-Dichlorobenzene-d4 (IS)93.4 %02/25/23 20:57 3855-82-102/25/23 20:5760.0-140 2000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-3 Lab ID: 92653832003 Collected: 02/21/23 10:58 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Acetone ND ug/m3 02/25/23 00:18 67-64-102/25/23 00:181190 400
Allyl chloride ND ug/m3 02/25/23 00:18 107-05-102/25/23 00:18250 400
Benzene ND ug/m3 02/25/23 00:18 71-43-202/25/23 00:18256 400
Benzyl chloride ND ug/m3 02/25/23 00:18 100-44-702/25/23 00:18416 400
Bromodichloromethane ND ug/m3 02/25/23 00:18 75-27-402/25/23 00:18537 400
Bromoform ND ug/m3 02/25/23 00:18 75-25-202/25/23 00:182480 400
Bromomethane ND ug/m3 02/25/23 00:18 74-83-902/25/23 00:18311 400
1,3-Butadiene ND ug/m3 02/25/23 00:18 106-99-002/25/23 00:181770 400
Carbon disulfide ND ug/m3 02/25/23 00:18 75-15-002/25/23 00:18249 400
Carbon tetrachloride ND ug/m3 02/25/23 00:18 56-23-502/25/23 00:18504 400
Chlorobenzene ND ug/m3 02/25/23 00:18 108-90-702/25/23 00:18370 400
Chloroethane ND ug/m3 02/25/23 00:18 75-00-302/25/23 00:18211 400
Chloroform ND ug/m3 02/25/23 00:18 67-66-302/25/23 00:18389 400
Chloromethane ND ug/m3 02/25/23 00:18 74-87-302/25/23 00:18165 400
2-Chlorotoluene ND ug/m3 02/25/23 00:18 95-49-802/25/23 00:18412 400
Cyclohexane ND ug/m3 02/25/23 00:18 110-82-702/25/23 00:18276 400
Dibromochloromethane ND ug/m3 02/25/23 00:18 124-48-102/25/23 00:18681 400
1,2-Dibromoethane (EDB)ND ug/m3 02/25/23 00:18 106-93-402/25/23 00:18615 400
1,2-Dichlorobenzene ND ug/m3 02/25/23 00:18 95-50-102/25/23 00:18481 400
1,3-Dichlorobenzene ND ug/m3 02/25/23 00:18 541-73-102/25/23 00:18481 400
1,4-Dichlorobenzene ND ug/m3 02/25/23 00:18 106-46-702/25/23 00:18481 400
1,2-Dichloroethane ND ug/m3 02/25/23 00:18 107-06-202/25/23 00:18324 400
1,1-Dichloroethane ND ug/m3 02/25/23 00:18 75-34-302/25/23 00:18321 400
1,1-Dichloroethene ND ug/m3 02/25/23 00:18 75-35-402/25/23 00:18317 400
cis-1,2-Dichloroethene ND ug/m3 02/25/23 00:18 156-59-202/25/23 00:18317 400
trans-1,2-Dichloroethene ND ug/m3 02/25/23 00:18 156-60-502/25/23 00:18317 400
1,2-Dichloropropane ND ug/m3 02/25/23 00:18 78-87-502/25/23 00:18370 400
cis-1,3-Dichloropropene ND ug/m3 02/25/23 00:18 10061-01-502/25/23 00:18363 400
trans-1,3-Dichloropropene ND ug/m3 02/25/23 00:18 10061-02-602/25/23 00:18363 400
1,4-Dioxane (p-Dioxane)ND ug/m3 02/25/23 00:18 123-91-102/25/23 00:18288 400
Ethanol 1490 ug/m3 02/25/23 00:18 64-17-502/25/23 00:18943 400
Ethylbenzene ND ug/m3 02/25/23 00:18 100-41-402/25/23 00:18347 400
Ethyl acetate ND ug/m3 02/25/23 00:18 141-78-602/25/23 00:18288 400
4-Ethyltoluene ND ug/m3 02/25/23 00:18 622-96-802/25/23 00:18393 400
Trichlorofluoromethane ND ug/m3 02/25/23 00:18 75-69-402/25/23 00:18450 400
Dichlorodifluoromethane ND ug/m3 02/25/23 00:18 75-71-802/25/23 00:18396 400
1,1,2-Trichlorotrifluoroethane ND ug/m3 02/25/23 00:18 76-13-102/25/23 00:18613 400
Dichlorotetrafluoroethane ND ug/m3 02/25/23 00:18 76-14-202/25/23 00:18560 400
n-Heptane ND ug/m3 02/25/23 00:18 142-82-502/25/23 00:18327 400
Hexachloro-1,3-butadiene ND ug/m3 02/25/23 00:18 87-68-302/25/23 00:182690 400
n-Hexane 2560 ug/m3 02/25/23 00:18 110-54-302/25/23 00:18888 400
Isopropylbenzene (Cumene)ND ug/m3 02/25/23 00:18 98-82-802/25/23 00:18393 400
Methylene Chloride ND ug/m3 02/25/23 00:18 75-09-202/25/23 00:18278 400
2-Hexanone ND ug/m3 02/25/23 00:18 591-78-602/25/23 00:182040 400
2-Butanone (MEK)ND ug/m3 02/25/23 00:18 78-93-302/25/23 00:181470 400
4-Methyl-2-pentanone (MIBK)ND ug/m3 02/25/23 00:18 108-10-102/25/23 00:182050 400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-3 Lab ID: 92653832003 Collected: 02/21/23 10:58 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Methyl methacrylate 553 ug/m3 02/25/23 00:18 80-62-602/25/23 00:18328 400
Methyl-tert-butyl ether ND ug/m3 02/25/23 00:18 1634-04-402/25/23 00:18288 400
Naphthalene ND ug/m3 02/25/23 00:18 91-20-302/25/23 00:181320 400
2-Propanol 6710 ug/m3 02/25/23 00:18 67-63-002/25/23 00:181230 400
Propylene ND ug/m3 02/25/23 00:18 115-07-102/25/23 00:18861 400
Styrene ND ug/m3 02/25/23 00:18 100-42-502/25/23 00:18340 400
1,1,2,2-Tetrachloroethane ND ug/m3 02/25/23 00:18 79-34-502/25/23 00:18550 400
Tetrachloroethene 629000 ug/m3 02/25/23 21:32 127-18-402/25/23 21:326790 5000
Tetrahydrofuran ND ug/m3 02/25/23 00:18 109-99-902/25/23 00:18236 400
Toluene ND ug/m3 02/25/23 00:18 108-88-302/25/23 00:18753 400
1,2,4-Trichlorobenzene ND ug/m3 02/25/23 00:18 120-82-102/25/23 00:181870 400
1,1,1-Trichloroethane ND ug/m3 02/25/23 00:18 71-55-602/25/23 00:18435 400
1,1,2-Trichloroethane ND ug/m3 02/25/23 00:18 79-00-502/25/23 00:18435 400
Trichloroethene 1900 ug/m3 02/25/23 00:18 79-01-602/25/23 00:18429 400
1,2,4-Trimethylbenzene ND ug/m3 02/25/23 00:18 95-63-602/25/23 00:18393 400
1,3,5-Trimethylbenzene ND ug/m3 02/25/23 00:18 108-67-802/25/23 00:18393 400
2,2,4-Trimethylpentane ND ug/m3 02/25/23 00:18 540-84-102/25/23 00:18374 400
Vinyl chloride ND ug/m3 02/25/23 00:18 75-01-402/25/23 00:18204 400
Vinyl bromide ND ug/m3 02/25/23 00:18 593-60-202/25/23 00:18350 400
Vinyl acetate ND ug/m3 02/25/23 00:18 108-05-402/25/23 00:18282 400
m&p-Xylene ND ug/m3 02/25/23 00:18 179601-23-102/25/23 00:18694 400
o-Xylene ND ug/m3 02/25/23 00:18 95-47-602/25/23 00:18347 400
Surrogates
1,4-Dichlorobenzene-d4 (IS)94.1 %02/25/23 00:18 3855-82-102/25/23 00:1860.0-140 400
1,4-Dichlorobenzene-d4 (IS)90.0 %02/25/23 21:32 3855-82-102/25/23 21:3260.0-140 5000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-4 Lab ID: 92653832004 Collected: 02/21/23 10:58 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Acetone ND ug/m3 02/25/23 01:36 67-64-102/25/23 01:362380 800
Allyl chloride ND ug/m3 02/25/23 01:36 107-05-102/25/23 01:36501 800
Benzene ND ug/m3 02/25/23 01:36 71-43-202/25/23 01:36511 800
Benzyl chloride ND ug/m3 02/25/23 01:36 100-44-702/25/23 01:36831 800
Bromodichloromethane ND ug/m3 02/25/23 01:36 75-27-402/25/23 01:361070 800
Bromoform ND ug/m3 02/25/23 01:36 75-25-202/25/23 01:364970 800
Bromomethane ND ug/m3 02/25/23 01:36 74-83-902/25/23 01:36621 800
1,3-Butadiene ND ug/m3 02/25/23 01:36 106-99-002/25/23 01:363540 800
Carbon disulfide ND ug/m3 02/25/23 01:36 75-15-002/25/23 01:36498 800
Carbon tetrachloride ND ug/m3 02/25/23 01:36 56-23-502/25/23 01:361010 800
Chlorobenzene ND ug/m3 02/25/23 01:36 108-90-702/25/23 01:36739 800
Chloroethane ND ug/m3 02/25/23 01:36 75-00-302/25/23 01:36422 800
Chloroform ND ug/m3 02/25/23 01:36 67-66-302/25/23 01:36779 800
Chloromethane ND ug/m3 02/25/23 01:36 74-87-302/25/23 01:36330 800
2-Chlorotoluene ND ug/m3 02/25/23 01:36 95-49-802/25/23 01:36825 800
Cyclohexane ND ug/m3 02/25/23 01:36 110-82-702/25/23 01:36551 800
Dibromochloromethane ND ug/m3 02/25/23 01:36 124-48-102/25/23 01:361360 800
1,2-Dibromoethane (EDB)ND ug/m3 02/25/23 01:36 106-93-402/25/23 01:361230 800
1,2-Dichlorobenzene ND ug/m3 02/25/23 01:36 95-50-102/25/23 01:36962 800
1,3-Dichlorobenzene ND ug/m3 02/25/23 01:36 541-73-102/25/23 01:36962 800
1,4-Dichlorobenzene ND ug/m3 02/25/23 01:36 106-46-702/25/23 01:36962 800
1,2-Dichloroethane ND ug/m3 02/25/23 01:36 107-06-202/25/23 01:36648 800
1,1-Dichloroethane ND ug/m3 02/25/23 01:36 75-34-302/25/23 01:36641 800
1,1-Dichloroethene ND ug/m3 02/25/23 01:36 75-35-402/25/23 01:36634 800
cis-1,2-Dichloroethene 3640 ug/m3 02/25/23 01:36 156-59-202/25/23 01:36634 800
trans-1,2-Dichloroethene ND ug/m3 02/25/23 01:36 156-60-502/25/23 01:36634 800
1,2-Dichloropropane ND ug/m3 02/25/23 01:36 78-87-502/25/23 01:36739 800
cis-1,3-Dichloropropene ND ug/m3 02/25/23 01:36 10061-01-502/25/23 01:36726 800
trans-1,3-Dichloropropene ND ug/m3 02/25/23 01:36 10061-02-602/25/23 01:36726 800
1,4-Dioxane (p-Dioxane)ND ug/m3 02/25/23 01:36 123-91-102/25/23 01:36577 800
Ethanol ND ug/m3 02/25/23 01:36 64-17-502/25/23 01:361890 800
Ethylbenzene ND ug/m3 02/25/23 01:36 100-41-402/25/23 01:36694 800
Ethyl acetate ND ug/m3 02/25/23 01:36 141-78-602/25/23 01:36576 800
4-Ethyltoluene ND ug/m3 02/25/23 01:36 622-96-802/25/23 01:36785 800
Trichlorofluoromethane ND ug/m3 02/25/23 01:36 75-69-402/25/23 01:36899 800
Dichlorodifluoromethane ND ug/m3 02/25/23 01:36 75-71-802/25/23 01:36791 800
1,1,2-Trichlorotrifluoroethane ND ug/m3 02/25/23 01:36 76-13-102/25/23 01:361230 800
Dichlorotetrafluoroethane ND ug/m3 02/25/23 01:36 76-14-202/25/23 01:361120 800
n-Heptane ND ug/m3 02/25/23 01:36 142-82-502/25/23 01:36654 800
Hexachloro-1,3-butadiene ND ug/m3 02/25/23 01:36 87-68-302/25/23 01:365380 800
n-Hexane 3320 ug/m3 02/25/23 01:36 110-54-302/25/23 01:361780 800
Isopropylbenzene (Cumene)ND ug/m3 02/25/23 01:36 98-82-802/25/23 01:36787 800
Methylene Chloride ND ug/m3 02/25/23 01:36 75-09-202/25/23 01:36556 800
2-Hexanone ND ug/m3 02/25/23 01:36 591-78-602/25/23 01:364090 800
2-Butanone (MEK)ND ug/m3 02/25/23 01:36 78-93-302/25/23 01:362950 800
4-Methyl-2-pentanone (MIBK)ND ug/m3 02/25/23 01:36 108-10-102/25/23 01:364090 800
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-4 Lab ID: 92653832004 Collected: 02/21/23 10:58 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Methyl methacrylate ND ug/m3 02/25/23 01:36 80-62-602/25/23 01:36655 800
Methyl-tert-butyl ether ND ug/m3 02/25/23 01:36 1634-04-402/25/23 01:36577 800
Naphthalene ND ug/m3 02/25/23 01:36 91-20-302/25/23 01:362640 800
2-Propanol 7770 ug/m3 02/25/23 01:36 67-63-002/25/23 01:362460 800
Propylene ND ug/m3 02/25/23 01:36 115-07-102/25/23 01:361720 800
Styrene ND ug/m3 02/25/23 01:36 100-42-502/25/23 01:36681 800
1,1,2,2-Tetrachloroethane ND ug/m3 02/25/23 01:36 79-34-502/25/23 01:361100 800
Tetrachloroethene 6710000 ug/m3 02/25/23 22:09 127-18-402/25/23 22:0913600 10000
Tetrahydrofuran ND ug/m3 02/25/23 01:36 109-99-902/25/23 01:36472 800
Toluene ND ug/m3 02/25/23 01:36 108-88-302/25/23 01:361510 800
1,2,4-Trichlorobenzene ND ug/m3 02/25/23 01:36 120-82-102/25/23 01:363730 800
1,1,1-Trichloroethane ND ug/m3 02/25/23 01:36 71-55-602/25/23 01:36870 800
1,1,2-Trichloroethane ND ug/m3 02/25/23 01:36 79-00-502/25/23 01:36870 800
Trichloroethene 6860 ug/m3 02/25/23 01:36 79-01-602/25/23 01:36857 800
1,2,4-Trimethylbenzene ND ug/m3 02/25/23 01:36 95-63-602/25/23 01:36785 800
1,3,5-Trimethylbenzene ND ug/m3 02/25/23 01:36 108-67-802/25/23 01:36785 800
2,2,4-Trimethylpentane ND ug/m3 02/25/23 01:36 540-84-102/25/23 01:36747 800
Vinyl chloride ND ug/m3 02/25/23 01:36 75-01-402/25/23 01:36409 800
Vinyl bromide ND ug/m3 02/25/23 01:36 593-60-202/25/23 01:36700 800
Vinyl acetate ND ug/m3 02/25/23 01:36 108-05-402/25/23 01:36563 800
m&p-Xylene ND ug/m3 02/25/23 01:36 179601-23-102/25/23 01:361390 800
o-Xylene ND ug/m3 02/25/23 01:36 95-47-602/25/23 01:36694 800
Surrogates
1,4-Dichlorobenzene-d4 (IS)93.5 %02/25/23 01:36 3855-82-102/25/23 01:3660.0-140 800
1,4-Dichlorobenzene-d4 (IS)101 %02/25/23 22:09 3855-82-102/25/23 22:0960.0-140 10000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-6 Lab ID: 92653832005 Collected: 02/21/23 14:36 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Acetone 4.30 ug/m3 02/24/23 14:21 67-64-102/24/23 14:212.97 1
Allyl chloride ND ug/m3 02/24/23 14:21 107-05-102/24/23 14:210.626 1
Benzene ND ug/m3 02/24/23 14:21 71-43-202/24/23 14:210.639 1
Benzyl chloride ND ug/m3 02/24/23 14:21 100-44-702/24/23 14:211.04 1
Bromodichloromethane ND ug/m3 02/24/23 14:21 75-27-402/24/23 14:211.34 1
Bromoform ND ug/m3 02/24/23 14:21 75-25-202/24/23 14:216.21 1
Bromomethane ND ug/m3 02/24/23 14:21 74-83-902/24/23 14:210.776 1
1,3-Butadiene ND ug/m3 02/24/23 14:21 106-99-002/24/23 14:214.43 1
Carbon disulfide ND ug/m3 02/24/23 14:21 75-15-002/24/23 14:210.622 1
Carbon tetrachloride ND ug/m3 02/24/23 14:21 56-23-502/24/23 14:211.26 1
Chlorobenzene ND ug/m3 02/24/23 14:21 108-90-702/24/23 14:210.924 1
Chloroethane ND ug/m3 02/24/23 14:21 75-00-302/24/23 14:210.528 1
Chloroform ND ug/m3 02/24/23 14:21 67-66-302/24/23 14:210.973 1
Chloromethane ND ug/m3 02/24/23 14:21 74-87-302/24/23 14:210.413 1
2-Chlorotoluene ND ug/m3 02/24/23 14:21 95-49-802/24/23 14:211.03 1
Cyclohexane ND ug/m3 02/24/23 14:21 110-82-702/24/23 14:210.689 1
Dibromochloromethane ND ug/m3 02/24/23 14:21 124-48-102/24/23 14:211.70 1
1,2-Dibromoethane (EDB)ND ug/m3 02/24/23 14:21 106-93-402/24/23 14:211.54 1
1,2-Dichlorobenzene ND ug/m3 02/24/23 14:21 95-50-102/24/23 14:211.20 1
1,3-Dichlorobenzene ND ug/m3 02/24/23 14:21 541-73-102/24/23 14:211.20 1
1,4-Dichlorobenzene ND ug/m3 02/24/23 14:21 106-46-702/24/23 14:211.20 1
1,2-Dichloroethane ND ug/m3 02/24/23 14:21 107-06-202/24/23 14:210.810 1
1,1-Dichloroethane ND ug/m3 02/24/23 14:21 75-34-302/24/23 14:210.802 1
1,1-Dichloroethene ND ug/m3 02/24/23 14:21 75-35-402/24/23 14:210.793 1
cis-1,2-Dichloroethene ND ug/m3 02/24/23 14:21 156-59-202/24/23 14:210.793 1
trans-1,2-Dichloroethene ND ug/m3 02/24/23 14:21 156-60-502/24/23 14:210.793 1
1,2-Dichloropropane ND ug/m3 02/24/23 14:21 78-87-502/24/23 14:210.924 1
cis-1,3-Dichloropropene ND ug/m3 02/24/23 14:21 10061-01-502/24/23 14:210.908 1
trans-1,3-Dichloropropene ND ug/m3 02/24/23 14:21 10061-02-602/24/23 14:210.908 1
1,4-Dioxane (p-Dioxane)ND ug/m3 02/24/23 14:21 123-91-102/24/23 14:210.721 1
Ethanol 7.99 ug/m3 02/24/23 14:21 64-17-502/24/23 14:212.36 1
Ethylbenzene ND ug/m3 02/24/23 14:21 100-41-402/24/23 14:210.867 1
Ethyl acetate ND ug/m3 02/24/23 14:21 141-78-602/24/23 14:210.720 1
4-Ethyltoluene ND ug/m3 02/24/23 14:21 622-96-802/24/23 14:210.982 1
Trichlorofluoromethane 1.80 ug/m3 02/24/23 14:21 75-69-402/24/23 14:211.12 1
Dichlorodifluoromethane 1.81 ug/m3 02/24/23 14:21 75-71-802/24/23 14:210.989 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 02/24/23 14:21 76-13-102/24/23 14:211.53 1
Dichlorotetrafluoroethane ND ug/m3 02/24/23 14:21 76-14-202/24/23 14:211.40 1
n-Heptane ND ug/m3 02/24/23 14:21 142-82-502/24/23 14:210.818 1
Hexachloro-1,3-butadiene ND ug/m3 02/24/23 14:21 87-68-302/24/23 14:216.73 1
n-Hexane ND ug/m3 02/24/23 14:21 110-54-302/24/23 14:212.22 1
Isopropylbenzene (Cumene)ND ug/m3 02/24/23 14:21 98-82-802/24/23 14:210.983 1
Methylene Chloride ND ug/m3 02/24/23 14:21 75-09-202/24/23 14:210.694 1
2-Hexanone ND ug/m3 02/24/23 14:21 591-78-602/24/23 14:215.11 1
2-Butanone (MEK)4.04 ug/m3 02/24/23 14:21 78-93-302/24/23 14:213.69 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 02/24/23 14:21 108-10-102/24/23 14:215.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-6 Lab ID: 92653832005 Collected: 02/21/23 14:36 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Methyl methacrylate ND ug/m3 02/24/23 14:21 80-62-602/24/23 14:210.819 1
Methyl-tert-butyl ether ND ug/m3 02/24/23 14:21 1634-04-402/24/23 14:210.721 1
Naphthalene ND ug/m3 02/24/23 14:21 91-20-302/24/23 14:213.30 1
2-Propanol ND ug/m3 02/24/23 14:21 67-63-002/24/23 14:213.07 1
Propylene ND ug/m3 02/24/23 14:21 115-07-102/24/23 14:212.15 1
Styrene ND ug/m3 02/24/23 14:21 100-42-502/24/23 14:210.851 1
1,1,2,2-Tetrachloroethane ND ug/m3 02/24/23 14:21 79-34-502/24/23 14:211.37 1
Tetrachloroethene 6.14 ug/m3 02/25/23 11:44 127-18-402/25/23 11:441.36 1
Tetrahydrofuran ND ug/m3 02/24/23 14:21 109-99-902/24/23 14:210.590 1
Toluene ND ug/m3 02/24/23 14:21 108-88-302/24/23 14:211.88 1
1,2,4-Trichlorobenzene ND ug/m3 02/24/23 14:21 120-82-102/24/23 14:214.66 1
1,1,1-Trichloroethane ND ug/m3 02/24/23 14:21 71-55-602/24/23 14:211.09 1
1,1,2-Trichloroethane ND ug/m3 02/24/23 14:21 79-00-502/24/23 14:211.09 1
Trichloroethene ND ug/m3 02/24/23 14:21 79-01-602/24/23 14:211.07 1
1,2,4-Trimethylbenzene ND ug/m3 02/24/23 14:21 95-63-602/24/23 14:210.982 1
1,3,5-Trimethylbenzene ND ug/m3 02/24/23 14:21 108-67-802/24/23 14:210.982 1
2,2,4-Trimethylpentane ND ug/m3 02/24/23 14:21 540-84-102/24/23 14:210.934 1
Vinyl chloride ND ug/m3 02/24/23 14:21 75-01-402/24/23 14:210.511 1
Vinyl bromide ND ug/m3 02/24/23 14:21 593-60-202/24/23 14:210.875 1
Vinyl acetate ND ug/m3 02/24/23 14:21 108-05-402/24/23 14:210.704 1
m&p-Xylene ND ug/m3 02/24/23 14:21 179601-23-102/24/23 14:211.73 1
o-Xylene ND ug/m3 02/24/23 14:21 95-47-602/24/23 14:210.867 1
Surrogates
1,4-Dichlorobenzene-d4 (IS)94.8 %02/24/23 14:21 3855-82-102/24/23 14:2160.0-140 1
1,4-Dichlorobenzene-d4 (IS)93.6 %02/25/23 11:44 3855-82-102/25/23 11:4460.0-140 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-7 Lab ID: 92653832006 Collected: 02/21/23 15:44 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Acetone 5.23 ug/m3 02/24/23 15:00 67-64-102/24/23 15:002.97 1
Allyl chloride ND ug/m3 02/24/23 15:00 107-05-102/24/23 15:000.626 1
Benzene ND ug/m3 02/24/23 15:00 71-43-202/24/23 15:000.639 1
Benzyl chloride ND ug/m3 02/24/23 15:00 100-44-702/24/23 15:001.04 1
Bromodichloromethane ND ug/m3 02/24/23 15:00 75-27-402/24/23 15:001.34 1
Bromoform ND ug/m3 02/24/23 15:00 75-25-202/24/23 15:006.21 1
Bromomethane ND ug/m3 02/24/23 15:00 74-83-902/24/23 15:000.776 1
1,3-Butadiene ND ug/m3 02/24/23 15:00 106-99-002/24/23 15:004.43 1
Carbon disulfide ND ug/m3 02/24/23 15:00 75-15-002/24/23 15:000.622 1
Carbon tetrachloride ND ug/m3 02/24/23 15:00 56-23-502/24/23 15:001.26 1
Chlorobenzene ND ug/m3 02/24/23 15:00 108-90-702/24/23 15:000.924 1
Chloroethane ND ug/m3 02/24/23 15:00 75-00-302/24/23 15:000.528 1
Chloroform ND ug/m3 02/24/23 15:00 67-66-302/24/23 15:000.973 1
Chloromethane ND ug/m3 02/24/23 15:00 74-87-302/24/23 15:000.413 1
2-Chlorotoluene ND ug/m3 02/24/23 15:00 95-49-802/24/23 15:001.03 1
Cyclohexane 1.28 ug/m3 02/24/23 15:00 110-82-702/24/23 15:000.689 1
Dibromochloromethane ND ug/m3 02/24/23 15:00 124-48-102/24/23 15:001.70 1
1,2-Dibromoethane (EDB)ND ug/m3 02/24/23 15:00 106-93-402/24/23 15:001.54 1
1,2-Dichlorobenzene ND ug/m3 02/24/23 15:00 95-50-102/24/23 15:001.20 1
1,3-Dichlorobenzene ND ug/m3 02/24/23 15:00 541-73-102/24/23 15:001.20 1
1,4-Dichlorobenzene ND ug/m3 02/24/23 15:00 106-46-702/24/23 15:001.20 1
1,2-Dichloroethane ND ug/m3 02/24/23 15:00 107-06-202/24/23 15:000.810 1
1,1-Dichloroethane ND ug/m3 02/24/23 15:00 75-34-302/24/23 15:000.802 1
1,1-Dichloroethene ND ug/m3 02/24/23 15:00 75-35-402/24/23 15:000.793 1
cis-1,2-Dichloroethene ND ug/m3 02/24/23 15:00 156-59-202/24/23 15:000.793 1
trans-1,2-Dichloroethene ND ug/m3 02/24/23 15:00 156-60-502/24/23 15:000.793 1
1,2-Dichloropropane ND ug/m3 02/24/23 15:00 78-87-502/24/23 15:000.924 1
cis-1,3-Dichloropropene ND ug/m3 02/24/23 15:00 10061-01-502/24/23 15:000.908 1
trans-1,3-Dichloropropene ND ug/m3 02/24/23 15:00 10061-02-602/24/23 15:000.908 1
1,4-Dioxane (p-Dioxane)ND ug/m3 02/24/23 15:00 123-91-102/24/23 15:000.721 1
Ethanol 17.9 ug/m3 02/24/23 15:00 64-17-502/24/23 15:002.36 1
Ethylbenzene ND ug/m3 02/24/23 15:00 100-41-402/24/23 15:000.867 1
Ethyl acetate ND ug/m3 02/24/23 15:00 141-78-602/24/23 15:000.720 1
4-Ethyltoluene ND ug/m3 02/24/23 15:00 622-96-802/24/23 15:000.982 1
Trichlorofluoromethane 4.19 ug/m3 02/24/23 15:00 75-69-402/24/23 15:001.12 1
Dichlorodifluoromethane 1.85 ug/m3 02/24/23 15:00 75-71-802/24/23 15:000.989 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 02/24/23 15:00 76-13-102/24/23 15:001.53 1
Dichlorotetrafluoroethane ND ug/m3 02/24/23 15:00 76-14-202/24/23 15:001.40 1
n-Heptane ND ug/m3 02/24/23 15:00 142-82-502/24/23 15:000.818 1
Hexachloro-1,3-butadiene ND ug/m3 02/24/23 15:00 87-68-302/24/23 15:006.73 1
n-Hexane ND ug/m3 02/24/23 15:00 110-54-302/24/23 15:002.22 1
Isopropylbenzene (Cumene)ND ug/m3 02/24/23 15:00 98-82-802/24/23 15:000.983 1
Methylene Chloride 0.844 ug/m3 02/24/23 15:00 75-09-202/24/23 15:000.694 1
2-Hexanone ND ug/m3 02/24/23 15:00 591-78-602/24/23 15:005.11 1
2-Butanone (MEK)ND ug/m3 02/24/23 15:00 78-93-302/24/23 15:003.69 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 02/24/23 15:00 108-10-102/24/23 15:005.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-7 Lab ID: 92653832006 Collected: 02/21/23 15:44 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Methyl methacrylate ND ug/m3 02/24/23 15:00 80-62-602/24/23 15:000.819 1
Methyl-tert-butyl ether ND ug/m3 02/24/23 15:00 1634-04-402/24/23 15:000.721 1
Naphthalene ND ug/m3 02/24/23 15:00 91-20-302/24/23 15:003.30 1
2-Propanol ND ug/m3 02/24/23 15:00 67-63-002/24/23 15:003.07 1
Propylene ND ug/m3 02/24/23 15:00 115-07-102/24/23 15:002.15 1
Styrene ND ug/m3 02/24/23 15:00 100-42-502/24/23 15:000.851 1
1,1,2,2-Tetrachloroethane ND ug/m3 02/24/23 15:00 79-34-502/24/23 15:001.37 1
Tetrachloroethene 33.2 ug/m3 02/24/23 15:00 127-18-402/24/23 15:001.36 1
Tetrahydrofuran ND ug/m3 02/24/23 15:00 109-99-902/24/23 15:000.590 1
Toluene ND ug/m3 02/24/23 15:00 108-88-302/24/23 15:001.88 1
1,2,4-Trichlorobenzene ND ug/m3 02/24/23 15:00 120-82-102/24/23 15:004.66 1
1,1,1-Trichloroethane 63.6 ug/m3 02/24/23 15:00 71-55-602/24/23 15:001.09 1
1,1,2-Trichloroethane ND ug/m3 02/24/23 15:00 79-00-502/24/23 15:001.09 1
Trichloroethene ND ug/m3 02/24/23 15:00 79-01-602/24/23 15:001.07 1
1,2,4-Trimethylbenzene ND ug/m3 02/24/23 15:00 95-63-602/24/23 15:000.982 1
1,3,5-Trimethylbenzene ND ug/m3 02/24/23 15:00 108-67-802/24/23 15:000.982 1
2,2,4-Trimethylpentane ND ug/m3 02/24/23 15:00 540-84-102/24/23 15:000.934 1
Vinyl chloride ND ug/m3 02/24/23 15:00 75-01-402/24/23 15:000.511 1
Vinyl bromide ND ug/m3 02/24/23 15:00 593-60-202/24/23 15:000.875 1
Vinyl acetate ND ug/m3 02/24/23 15:00 108-05-402/24/23 15:000.704 1
m&p-Xylene ND ug/m3 02/24/23 15:00 179601-23-102/24/23 15:001.73 1
o-Xylene ND ug/m3 02/24/23 15:00 95-47-602/24/23 15:000.867 1
Surrogates
1,4-Dichlorobenzene-d4 (IS)94.7 %02/24/23 15:00 3855-82-102/24/23 15:0060.0-140 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-8 Lab ID: 92653832007 Collected: 02/21/23 15:44 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Acetone ND ug/m3 02/24/23 15:41 67-64-102/24/23 15:412.97 1
Allyl chloride ND ug/m3 02/24/23 15:41 107-05-102/24/23 15:410.626 1
Benzene ND ug/m3 02/24/23 15:41 71-43-202/24/23 15:410.639 1
Benzyl chloride ND ug/m3 02/24/23 15:41 100-44-702/24/23 15:411.04 1
Bromodichloromethane ND ug/m3 02/24/23 15:41 75-27-402/24/23 15:411.34 1
Bromoform ND ug/m3 02/24/23 15:41 75-25-202/24/23 15:416.21 1
Bromomethane ND ug/m3 02/24/23 15:41 74-83-902/24/23 15:410.776 1
1,3-Butadiene ND ug/m3 02/24/23 15:41 106-99-002/24/23 15:414.43 1
Carbon disulfide ND ug/m3 02/24/23 15:41 75-15-002/24/23 15:410.622 1
Carbon tetrachloride ND ug/m3 02/24/23 15:41 56-23-502/24/23 15:411.26 1
Chlorobenzene ND ug/m3 02/24/23 15:41 108-90-702/24/23 15:410.924 1
Chloroethane ND ug/m3 02/24/23 15:41 75-00-302/24/23 15:410.528 1
Chloroform ND ug/m3 02/24/23 15:41 67-66-302/24/23 15:410.973 1
Chloromethane ND ug/m3 02/24/23 15:41 74-87-302/24/23 15:410.413 1
2-Chlorotoluene ND ug/m3 02/24/23 15:41 95-49-802/24/23 15:411.03 1
Cyclohexane 6.44 ug/m3 02/24/23 15:41 110-82-702/24/23 15:410.689 1
Dibromochloromethane ND ug/m3 02/24/23 15:41 124-48-102/24/23 15:411.70 1
1,2-Dibromoethane (EDB)ND ug/m3 02/24/23 15:41 106-93-402/24/23 15:411.54 1
1,2-Dichlorobenzene ND ug/m3 02/24/23 15:41 95-50-102/24/23 15:411.20 1
1,3-Dichlorobenzene ND ug/m3 02/24/23 15:41 541-73-102/24/23 15:411.20 1
1,4-Dichlorobenzene ND ug/m3 02/24/23 15:41 106-46-702/24/23 15:411.20 1
1,2-Dichloroethane ND ug/m3 02/24/23 15:41 107-06-202/24/23 15:410.810 1
1,1-Dichloroethane 2.71 ug/m3 02/24/23 15:41 75-34-302/24/23 15:410.802 1
1,1-Dichloroethene 2.92 ug/m3 02/24/23 15:41 75-35-402/24/23 15:410.793 1
cis-1,2-Dichloroethene ND ug/m3 02/24/23 15:41 156-59-202/24/23 15:410.793 1
trans-1,2-Dichloroethene ND ug/m3 02/24/23 15:41 156-60-502/24/23 15:410.793 1
1,2-Dichloropropane ND ug/m3 02/24/23 15:41 78-87-502/24/23 15:410.924 1
cis-1,3-Dichloropropene ND ug/m3 02/24/23 15:41 10061-01-502/24/23 15:410.908 1
trans-1,3-Dichloropropene ND ug/m3 02/24/23 15:41 10061-02-602/24/23 15:410.908 1
1,4-Dioxane (p-Dioxane)ND ug/m3 02/24/23 15:41 123-91-102/24/23 15:410.721 1
Ethanol ND ug/m3 02/24/23 15:41 64-17-502/24/23 15:412.36 1
Ethylbenzene ND ug/m3 02/24/23 15:41 100-41-402/24/23 15:410.867 1
Ethyl acetate ND ug/m3 02/24/23 15:41 141-78-602/24/23 15:410.720 1
4-Ethyltoluene ND ug/m3 02/24/23 15:41 622-96-802/24/23 15:410.982 1
Trichlorofluoromethane 13.7 ug/m3 02/24/23 15:41 75-69-402/24/23 15:411.12 1
Dichlorodifluoromethane 1.78 ug/m3 02/24/23 15:41 75-71-802/24/23 15:410.989 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 02/24/23 15:41 76-13-102/24/23 15:411.53 1
Dichlorotetrafluoroethane ND ug/m3 02/24/23 15:41 76-14-202/24/23 15:411.40 1
n-Heptane ND ug/m3 02/24/23 15:41 142-82-502/24/23 15:410.818 1
Hexachloro-1,3-butadiene ND ug/m3 02/24/23 15:41 87-68-302/24/23 15:416.73 1
n-Hexane ND ug/m3 02/24/23 15:41 110-54-302/24/23 15:412.22 1
Isopropylbenzene (Cumene)ND ug/m3 02/24/23 15:41 98-82-802/24/23 15:410.983 1
Methylene Chloride ND ug/m3 02/24/23 15:41 75-09-202/24/23 15:410.694 1
2-Hexanone ND ug/m3 02/24/23 15:41 591-78-602/24/23 15:415.11 1
2-Butanone (MEK)ND ug/m3 02/24/23 15:41 78-93-302/24/23 15:413.69 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 02/24/23 15:41 108-10-102/24/23 15:415.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-8 Lab ID: 92653832007 Collected: 02/21/23 15:44 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Methyl methacrylate ND ug/m3 02/24/23 15:41 80-62-602/24/23 15:410.819 1
Methyl-tert-butyl ether ND ug/m3 02/24/23 15:41 1634-04-402/24/23 15:410.721 1
Naphthalene ND ug/m3 02/24/23 15:41 91-20-302/24/23 15:413.30 1
2-Propanol ND ug/m3 02/24/23 15:41 67-63-002/24/23 15:413.07 1
Propylene ND ug/m3 02/24/23 15:41 115-07-102/24/23 15:412.15 1
Styrene ND ug/m3 02/24/23 15:41 100-42-502/24/23 15:410.851 1
1,1,2,2-Tetrachloroethane ND ug/m3 02/24/23 15:41 79-34-502/24/23 15:411.37 1
Tetrachloroethene 251 ug/m3 02/24/23 15:41 127-18-402/24/23 15:411.36 1
Tetrahydrofuran ND ug/m3 02/24/23 15:41 109-99-902/24/23 15:410.590 1
Toluene ND ug/m3 02/24/23 15:41 108-88-302/24/23 15:411.88 1
1,2,4-Trichlorobenzene ND ug/m3 02/24/23 15:41 120-82-102/24/23 15:414.66 1
1,1,1-Trichloroethane 228 ug/m3 02/24/23 15:41 71-55-602/24/23 15:411.09 1
1,1,2-Trichloroethane ND ug/m3 02/24/23 15:41 79-00-502/24/23 15:411.09 1
Trichloroethene ND ug/m3 02/24/23 15:41 79-01-602/24/23 15:411.07 1
1,2,4-Trimethylbenzene ND ug/m3 02/24/23 15:41 95-63-602/24/23 15:410.982 1
1,3,5-Trimethylbenzene ND ug/m3 02/24/23 15:41 108-67-802/24/23 15:410.982 1
2,2,4-Trimethylpentane ND ug/m3 02/24/23 15:41 540-84-102/24/23 15:410.934 1
Vinyl chloride ND ug/m3 02/24/23 15:41 75-01-402/24/23 15:410.511 1
Vinyl bromide ND ug/m3 02/24/23 15:41 593-60-202/24/23 15:410.875 1
Vinyl acetate ND ug/m3 02/24/23 15:41 108-05-402/24/23 15:410.704 1
m&p-Xylene ND ug/m3 02/24/23 15:41 179601-23-102/24/23 15:411.73 1
o-Xylene ND ug/m3 02/24/23 15:41 95-47-602/24/23 15:410.867 1
Surrogates
1,4-Dichlorobenzene-d4 (IS)92.5 %02/24/23 15:41 3855-82-102/24/23 15:4160.0-140 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-9 Lab ID: 92653832008 Collected: 02/21/23 12:05 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Acetone 6.34 ug/m3 02/24/23 16:21 67-64-102/24/23 16:212.97 1
Allyl chloride ND ug/m3 02/24/23 16:21 107-05-102/24/23 16:210.626 1
Benzene ND ug/m3 02/24/23 16:21 71-43-202/24/23 16:210.639 1
Benzyl chloride ND ug/m3 02/24/23 16:21 100-44-702/24/23 16:211.04 1
Bromodichloromethane ND ug/m3 02/24/23 16:21 75-27-402/24/23 16:211.34 1
Bromoform ND ug/m3 02/24/23 16:21 75-25-202/24/23 16:216.21 1
Bromomethane ND ug/m3 02/24/23 16:21 74-83-902/24/23 16:210.776 1
1,3-Butadiene ND ug/m3 02/24/23 16:21 106-99-002/24/23 16:214.43 1
Carbon disulfide ND ug/m3 02/24/23 16:21 75-15-002/24/23 16:210.622 1
Carbon tetrachloride ND ug/m3 02/24/23 16:21 56-23-502/24/23 16:211.26 1
Chlorobenzene ND ug/m3 02/24/23 16:21 108-90-702/24/23 16:210.924 1
Chloroethane ND ug/m3 02/24/23 16:21 75-00-302/24/23 16:210.528 1
Chloroform ND ug/m3 02/24/23 16:21 67-66-302/24/23 16:210.973 1
Chloromethane ND ug/m3 02/24/23 16:21 74-87-302/24/23 16:210.413 1
2-Chlorotoluene ND ug/m3 02/24/23 16:21 95-49-802/24/23 16:211.03 1
Cyclohexane ND ug/m3 02/24/23 16:21 110-82-702/24/23 16:210.689 1
Dibromochloromethane ND ug/m3 02/24/23 16:21 124-48-102/24/23 16:211.70 1
1,2-Dibromoethane (EDB)ND ug/m3 02/24/23 16:21 106-93-402/24/23 16:211.54 1
1,2-Dichlorobenzene ND ug/m3 02/24/23 16:21 95-50-102/24/23 16:211.20 1
1,3-Dichlorobenzene ND ug/m3 02/24/23 16:21 541-73-102/24/23 16:211.20 1
1,4-Dichlorobenzene ND ug/m3 02/24/23 16:21 106-46-702/24/23 16:211.20 1
1,2-Dichloroethane ND ug/m3 02/24/23 16:21 107-06-202/24/23 16:210.810 1
1,1-Dichloroethane ND ug/m3 02/24/23 16:21 75-34-302/24/23 16:210.802 1
1,1-Dichloroethene ND ug/m3 02/24/23 16:21 75-35-402/24/23 16:210.793 1
cis-1,2-Dichloroethene ND ug/m3 02/24/23 16:21 156-59-202/24/23 16:210.793 1
trans-1,2-Dichloroethene ND ug/m3 02/24/23 16:21 156-60-502/24/23 16:210.793 1
1,2-Dichloropropane ND ug/m3 02/24/23 16:21 78-87-502/24/23 16:210.924 1
cis-1,3-Dichloropropene ND ug/m3 02/24/23 16:21 10061-01-502/24/23 16:210.908 1
trans-1,3-Dichloropropene ND ug/m3 02/24/23 16:21 10061-02-602/24/23 16:210.908 1
1,4-Dioxane (p-Dioxane)ND ug/m3 02/24/23 16:21 123-91-102/24/23 16:210.721 1
Ethanol 27.3 ug/m3 02/24/23 16:21 64-17-502/24/23 16:212.36 1
Ethylbenzene ND ug/m3 02/24/23 16:21 100-41-402/24/23 16:210.867 1
Ethyl acetate 0.831 ug/m3 02/24/23 16:21 141-78-602/24/23 16:210.720 1
4-Ethyltoluene ND ug/m3 02/24/23 16:21 622-96-802/24/23 16:210.982 1
Trichlorofluoromethane 2.32 ug/m3 02/24/23 16:21 75-69-402/24/23 16:211.12 1
Dichlorodifluoromethane 1.64 ug/m3 02/24/23 16:21 75-71-802/24/23 16:210.989 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 02/24/23 16:21 76-13-102/24/23 16:211.53 1
Dichlorotetrafluoroethane ND ug/m3 02/24/23 16:21 76-14-202/24/23 16:211.40 1
n-Heptane ND ug/m3 02/24/23 16:21 142-82-502/24/23 16:210.818 1
Hexachloro-1,3-butadiene ND ug/m3 02/24/23 16:21 87-68-302/24/23 16:216.73 1
n-Hexane ND ug/m3 02/24/23 16:21 110-54-302/24/23 16:212.22 1
Isopropylbenzene (Cumene)ND ug/m3 02/24/23 16:21 98-82-802/24/23 16:210.983 1
Methylene Chloride ND ug/m3 02/24/23 16:21 75-09-202/24/23 16:210.694 1
2-Hexanone ND ug/m3 02/24/23 16:21 591-78-602/24/23 16:215.11 1
2-Butanone (MEK)ND ug/m3 02/24/23 16:21 78-93-302/24/23 16:213.69 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 02/24/23 16:21 108-10-102/24/23 16:215.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-9 Lab ID: 92653832008 Collected: 02/21/23 12:05 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Methyl methacrylate ND ug/m3 02/24/23 16:21 80-62-602/24/23 16:210.819 1
Methyl-tert-butyl ether ND ug/m3 02/24/23 16:21 1634-04-402/24/23 16:210.721 1
Naphthalene ND ug/m3 02/24/23 16:21 91-20-302/24/23 16:213.30 1
2-Propanol 3.88 ug/m3 02/24/23 16:21 67-63-002/24/23 16:213.07 1
Propylene ND ug/m3 02/24/23 16:21 115-07-102/24/23 16:212.15 1
Styrene ND ug/m3 02/24/23 16:21 100-42-502/24/23 16:210.851 1
1,1,2,2-Tetrachloroethane ND ug/m3 02/24/23 16:21 79-34-502/24/23 16:211.37 1
Tetrachloroethene 282 ug/m3 02/24/23 16:21 127-18-402/24/23 16:211.36 1
Tetrahydrofuran ND ug/m3 02/24/23 16:21 109-99-902/24/23 16:210.590 1
Toluene ND ug/m3 02/24/23 16:21 108-88-302/24/23 16:211.88 1
1,2,4-Trichlorobenzene ND ug/m3 02/24/23 16:21 120-82-102/24/23 16:214.66 1
1,1,1-Trichloroethane 1.37 ug/m3 02/24/23 16:21 71-55-602/24/23 16:211.09 1
1,1,2-Trichloroethane ND ug/m3 02/24/23 16:21 79-00-502/24/23 16:211.09 1
Trichloroethene ND ug/m3 02/24/23 16:21 79-01-602/24/23 16:211.07 1
1,2,4-Trimethylbenzene ND ug/m3 02/24/23 16:21 95-63-602/24/23 16:210.982 1
1,3,5-Trimethylbenzene ND ug/m3 02/24/23 16:21 108-67-802/24/23 16:210.982 1
2,2,4-Trimethylpentane ND ug/m3 02/24/23 16:21 540-84-102/24/23 16:210.934 1
Vinyl chloride ND ug/m3 02/24/23 16:21 75-01-402/24/23 16:210.511 1
Vinyl bromide ND ug/m3 02/24/23 16:21 593-60-202/24/23 16:210.875 1
Vinyl acetate ND ug/m3 02/24/23 16:21 108-05-402/24/23 16:210.704 1
m&p-Xylene ND ug/m3 02/24/23 16:21 179601-23-102/24/23 16:211.73 1
o-Xylene ND ug/m3 02/24/23 16:21 95-47-602/24/23 16:210.867 1
Surrogates
1,4-Dichlorobenzene-d4 (IS)93.3 %02/24/23 16:21 3855-82-102/24/23 16:2160.0-140 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-10 Lab ID: 92653832009 Collected: 02/21/23 12:05 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Acetone ND ug/m3 02/24/23 17:01 67-64-102/24/23 17:012.97 1
Allyl chloride ND ug/m3 02/24/23 17:01 107-05-102/24/23 17:010.626 1
Benzene ND ug/m3 02/24/23 17:01 71-43-202/24/23 17:010.639 1
Benzyl chloride ND ug/m3 02/24/23 17:01 100-44-702/24/23 17:011.04 1
Bromodichloromethane ND ug/m3 02/24/23 17:01 75-27-402/24/23 17:011.34 1
Bromoform ND ug/m3 02/24/23 17:01 75-25-202/24/23 17:016.21 1
Bromomethane ND ug/m3 02/24/23 17:01 74-83-902/24/23 17:010.776 1
1,3-Butadiene ND ug/m3 02/24/23 17:01 106-99-002/24/23 17:014.43 1
Carbon disulfide ND ug/m3 02/24/23 17:01 75-15-002/24/23 17:010.622 1
Carbon tetrachloride ND ug/m3 02/24/23 17:01 56-23-502/24/23 17:011.26 1
Chlorobenzene ND ug/m3 02/24/23 17:01 108-90-702/24/23 17:010.924 1
Chloroethane ND ug/m3 02/24/23 17:01 75-00-302/24/23 17:010.528 1
Chloroform ND ug/m3 02/24/23 17:01 67-66-302/24/23 17:010.973 1
Chloromethane ND ug/m3 02/24/23 17:01 74-87-302/24/23 17:010.413 1
2-Chlorotoluene ND ug/m3 02/24/23 17:01 95-49-802/24/23 17:011.03 1
Cyclohexane ND ug/m3 02/24/23 17:01 110-82-702/24/23 17:010.689 1
Dibromochloromethane ND ug/m3 02/24/23 17:01 124-48-102/24/23 17:011.70 1
1,2-Dibromoethane (EDB)ND ug/m3 02/24/23 17:01 106-93-402/24/23 17:011.54 1
1,2-Dichlorobenzene ND ug/m3 02/24/23 17:01 95-50-102/24/23 17:011.20 1
1,3-Dichlorobenzene 1.82 ug/m3 02/24/23 17:01 541-73-102/24/23 17:011.20 1
1,4-Dichlorobenzene ND ug/m3 02/24/23 17:01 106-46-702/24/23 17:011.20 1
1,2-Dichloroethane ND ug/m3 02/24/23 17:01 107-06-202/24/23 17:010.810 1
1,1-Dichloroethane ND ug/m3 02/24/23 17:01 75-34-302/24/23 17:010.802 1
1,1-Dichloroethene ND ug/m3 02/24/23 17:01 75-35-402/24/23 17:010.793 1
cis-1,2-Dichloroethene ND ug/m3 02/24/23 17:01 156-59-202/24/23 17:010.793 1
trans-1,2-Dichloroethene ND ug/m3 02/24/23 17:01 156-60-502/24/23 17:010.793 1
1,2-Dichloropropane ND ug/m3 02/24/23 17:01 78-87-502/24/23 17:010.924 1
cis-1,3-Dichloropropene ND ug/m3 02/24/23 17:01 10061-01-502/24/23 17:010.908 1
trans-1,3-Dichloropropene ND ug/m3 02/24/23 17:01 10061-02-602/24/23 17:010.908 1
1,4-Dioxane (p-Dioxane)ND ug/m3 02/24/23 17:01 123-91-102/24/23 17:010.721 1
Ethanol ND ug/m3 02/24/23 17:01 64-17-502/24/23 17:012.36 1
Ethylbenzene ND ug/m3 02/24/23 17:01 100-41-402/24/23 17:010.867 1
Ethyl acetate ND ug/m3 02/24/23 17:01 141-78-602/24/23 17:010.720 1
4-Ethyltoluene ND ug/m3 02/24/23 17:01 622-96-802/24/23 17:010.982 1
Trichlorofluoromethane 5.68 ug/m3 02/24/23 17:01 75-69-402/24/23 17:011.12 1
Dichlorodifluoromethane 1.63 ug/m3 02/24/23 17:01 75-71-802/24/23 17:010.989 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 02/24/23 17:01 76-13-102/24/23 17:011.53 1
Dichlorotetrafluoroethane ND ug/m3 02/24/23 17:01 76-14-202/24/23 17:011.40 1
n-Heptane ND ug/m3 02/24/23 17:01 142-82-502/24/23 17:010.818 1
Hexachloro-1,3-butadiene ND ug/m3 02/24/23 17:01 87-68-302/24/23 17:016.73 1
n-Hexane ND ug/m3 02/24/23 17:01 110-54-302/24/23 17:012.22 1
Isopropylbenzene (Cumene)ND ug/m3 02/24/23 17:01 98-82-802/24/23 17:010.983 1
Methylene Chloride ND ug/m3 02/24/23 17:01 75-09-202/24/23 17:010.694 1
2-Hexanone ND ug/m3 02/24/23 17:01 591-78-602/24/23 17:015.11 1
2-Butanone (MEK)ND ug/m3 02/24/23 17:01 78-93-302/24/23 17:013.69 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 02/24/23 17:01 108-10-102/24/23 17:015.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653832
Forest City Brownfield
Sample: VP-10 Lab ID: 92653832009 Collected: 02/21/23 12:05 Received: 02/21/23 17:00 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: TO-15 Preparation Method: TO-15
Pace National - Mt. Juliet
VOA (MS) TO-15
Methyl methacrylate ND ug/m3 02/24/23 17:01 80-62-602/24/23 17:010.819 1
Methyl-tert-butyl ether ND ug/m3 02/24/23 17:01 1634-04-402/24/23 17:010.721 1
Naphthalene ND ug/m3 02/24/23 17:01 91-20-302/24/23 17:013.30 1
2-Propanol ND ug/m3 02/24/23 17:01 67-63-002/24/23 17:013.07 1
Propylene ND ug/m3 02/24/23 17:01 115-07-102/24/23 17:012.15 1
Styrene ND ug/m3 02/24/23 17:01 100-42-502/24/23 17:010.851 1
1,1,2,2-Tetrachloroethane ND ug/m3 02/24/23 17:01 79-34-502/24/23 17:011.37 1
Tetrachloroethene 1190 ug/m3 02/25/23 14:59 127-18-402/25/23 14:5913.6 10
Tetrahydrofuran ND ug/m3 02/24/23 17:01 109-99-902/24/23 17:010.590 1
Toluene ND ug/m3 02/24/23 17:01 108-88-302/24/23 17:011.88 1
1,2,4-Trichlorobenzene ND ug/m3 02/24/23 17:01 120-82-102/24/23 17:014.66 1
1,1,1-Trichloroethane 3.20 ug/m3 02/24/23 17:01 71-55-602/24/23 17:011.09 1
1,1,2-Trichloroethane ND ug/m3 02/24/23 17:01 79-00-502/24/23 17:011.09 1
Trichloroethene ND ug/m3 02/24/23 17:01 79-01-602/24/23 17:011.07 1
1,2,4-Trimethylbenzene ND ug/m3 02/24/23 17:01 95-63-602/24/23 17:010.982 1
1,3,5-Trimethylbenzene ND ug/m3 02/24/23 17:01 108-67-802/24/23 17:010.982 1
2,2,4-Trimethylpentane ND ug/m3 02/24/23 17:01 540-84-102/24/23 17:010.934 1
Vinyl chloride ND ug/m3 02/24/23 17:01 75-01-402/24/23 17:010.511 1
Vinyl bromide ND ug/m3 02/24/23 17:01 593-60-202/24/23 17:010.875 1
Vinyl acetate ND ug/m3 02/24/23 17:01 108-05-402/24/23 17:010.704 1
m&p-Xylene ND ug/m3 02/24/23 17:01 179601-23-102/24/23 17:011.73 1
o-Xylene ND ug/m3 02/24/23 17:01 95-47-602/24/23 17:010.867 1
Surrogates
1,4-Dichlorobenzene-d4 (IS)93.7 %02/24/23 17:01 3855-82-102/24/23 17:0160.0-140 1
1,4-Dichlorobenzene-d4 (IS)90.4 %02/25/23 14:59 3855-82-102/25/23 14:5960.0-140 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653832
Forest City Brownfield
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2012373
TO-15
TO-15
VOA (MS) TO-15
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92653832001, 92653832002, 92653832003, 92653832004, 92653832005, 92653832006, 92653832007,
92653832008, 92653832009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3894801-3
Associated Lab Samples: 92653832001, 92653832002, 92653832003, 92653832004, 92653832005, 92653832006, 92653832007,
92653832008, 92653832009
Matrix: Air
Analyzed
Acetone ppbv ND 1.25 02/24/23 10:10
Allyl chloride ppbv ND 0.200 02/24/23 10:10
Benzene ppbv ND 0.200 02/24/23 10:10
Benzyl chloride ppbv ND 0.200 02/24/23 10:10
Bromodichloromethane ppbv ND 0.200 02/24/23 10:10
Bromoform ppbv ND 0.600 02/24/23 10:10
Bromomethane ppbv ND 0.200 02/24/23 10:10
1,3-Butadiene ppbv ND 2.00 02/24/23 10:10
Carbon disulfide ppbv ND 0.200 02/24/23 10:10
Carbon tetrachloride ppbv ND 0.200 02/24/23 10:10
Chlorobenzene ppbv ND 0.200 02/24/23 10:10
Chloroethane ppbv ND 0.200 02/24/23 10:10
Chloroform ppbv ND 0.200 02/24/23 10:10
Chloromethane ppbv ND 0.200 02/24/23 10:10
2-Chlorotoluene ppbv ND 0.200 02/24/23 10:10
Cyclohexane ppbv ND 0.200 02/24/23 10:10
Dibromochloromethane ppbv ND 0.200 02/24/23 10:10
1,2-Dibromoethane (EDB)ppbv ND 0.200 02/24/23 10:10
1,2-Dichlorobenzene ppbv ND 0.200 02/24/23 10:10
1,3-Dichlorobenzene ppbv ND 0.200 02/24/23 10:10
1,4-Dichlorobenzene ppbv ND 0.200 02/24/23 10:10
1,2-Dichloroethane ppbv ND 0.200 02/24/23 10:10
1,1-Dichloroethane ppbv ND 0.200 02/24/23 10:10
1,1-Dichloroethene ppbv ND 0.200 02/24/23 10:10
cis-1,2-Dichloroethene ppbv ND 0.200 02/24/23 10:10
trans-1,2-Dichloroethene ppbv ND 0.200 02/24/23 10:10
1,2-Dichloropropane ppbv ND 0.200 02/24/23 10:10
cis-1,3-Dichloropropene ppbv ND 0.200 02/24/23 10:10
trans-1,3-Dichloropropene ppbv ND 0.200 02/24/23 10:10
1,4-Dioxane (p-Dioxane)ppbv ND 0.200 02/24/23 10:10
Ethanol ppbv ND 1.25 02/24/23 10:10
Ethylbenzene ppbv ND 0.200 02/24/23 10:10
Ethyl acetate ppbv ND 0.200 02/24/23 10:10
4-Ethyltoluene ppbv ND 0.200 02/24/23 10:10
Trichlorofluoromethane ppbv ND 0.200 02/24/23 10:10
Dichlorodifluoromethane ppbv ND 0.200 02/24/23 10:10
1,1,2-Trichlorotrifluoroethane ppbv ND 0.200 02/24/23 10:10
Dichlorotetrafluoroethane ppbv ND 0.200 02/24/23 10:10
n-Heptane ppbv ND 0.200 02/24/23 10:10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
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[phone]
Page 22 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653832
Forest City Brownfield
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3894801-3
Associated Lab Samples: 92653832001, 92653832002, 92653832003, 92653832004, 92653832005, 92653832006, 92653832007,
92653832008, 92653832009
Matrix: Air
Analyzed
Hexachloro-1,3-butadiene ppbv ND 0.630 02/24/23 10:10
n-Hexane ppbv ND 0.630 02/24/23 10:10
Isopropylbenzene (Cumene)ppbv ND 0.200 02/24/23 10:10
Methylene Chloride ppbv ND 0.200 02/24/23 10:10
2-Hexanone ppbv ND 1.25 02/24/23 10:10
2-Butanone (MEK)ppbv ND 1.25 02/24/23 10:10
4-Methyl-2-pentanone (MIBK)ppbv ND 1.25 02/24/23 10:10
Methyl methacrylate ppbv ND 0.200 02/24/23 10:10
Methyl-tert-butyl ether ppbv ND 0.200 02/24/23 10:10
Naphthalene ppbv ND 0.630 02/24/23 10:10
2-Propanol ppbv ND 1.25 02/24/23 10:10
Propylene ppbv ND 1.25 02/24/23 10:10
Styrene ppbv ND 0.200 02/24/23 10:10
1,1,2,2-Tetrachloroethane ppbv ND 0.200 02/24/23 10:10
Tetrachloroethene ppbv ND 0.200 02/24/23 10:10
Tetrahydrofuran ppbv ND 0.200 02/24/23 10:10
Toluene ppbv ND 0.500 02/24/23 10:10
1,2,4-Trichlorobenzene ppbv ND 0.630 02/24/23 10:10
1,1,1-Trichloroethane ppbv ND 0.200 02/24/23 10:10
1,1,2-Trichloroethane ppbv ND 0.200 02/24/23 10:10
Trichloroethene ppbv ND 0.200 02/24/23 10:10
1,2,4-Trimethylbenzene ppbv ND 0.200 02/24/23 10:10
1,3,5-Trimethylbenzene ppbv ND 0.200 02/24/23 10:10
2,2,4-Trimethylpentane ppbv ND 0.200 02/24/23 10:10
Vinyl chloride ppbv ND 0.200 02/24/23 10:10
Vinyl bromide ppbv ND 0.200 02/24/23 10:10
Vinyl acetate ppbv ND 0.200 02/24/23 10:10
m&p-Xylene ppbv ND 0.400 02/24/23 10:10
o-Xylene ppbv ND 0.200 02/24/23 10:10
1,4-Dichlorobenzene-d4 (IS)%94.3 60.0-140 02/24/23 10:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3894801-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3894801-2
Acetone ppbv 3.283.75 87.5 70.0-13088.03.30 0.608 25
Allyl chloride ppbv 3.253.75 86.7 70.0-13088.83.33 2.43 25
Benzene ppbv 3.493.75 93.1 70.0-13093.93.52 0.856 25
Benzyl chloride ppbv 3.803.75 101 70.0-1521033.86 1.57 25
Bromodichloromethane ppbv 3.643.75 97.1 70.0-13097.63.66 0.548 25
Bromoform ppbv 3.803.75 101 70.0-1301023.81 0.263 25
Bromomethane ppbv 3.733.75 99.5 70.0-1301013.80 1.86 25
1,3-Butadiene ppbv 3.343.75 89.1 70.0-13089.33.35 0.299 25
Carbon disulfide ppbv 3.373.75 89.9 70.0-13090.93.41 1.18 25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
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[phone]
Page 23 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653832
Forest City Brownfield
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3894801-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3894801-2
Carbon tetrachloride ppbv 3.823.75 102 70.0-1301033.86 1.04 25
Chlorobenzene ppbv 3.913.75 104 70.0-1301053.93 0.510 25
Chloroethane ppbv 3.343.75 89.1 70.0-13091.53.43 2.66 25
Chloroform ppbv 3.543.75 94.4 70.0-13095.23.57 0.844 25
Chloromethane ppbv 3.413.75 90.9 70.0-13091.73.44 0.876 25
2-Chlorotoluene ppbv 4.013.75 107 70.0-1301063.98 0.751 25
Cyclohexane ppbv 3.403.75 90.7 70.0-13092.83.48 2.33 25
Dibromochloromethane ppbv 3.813.75 102 70.0-1301043.89 2.08 25
1,2-Dibromoethane (EDB)ppbv 3.803.75 101 70.0-1301023.83 0.786 25
1,2-Dichlorobenzene ppbv 4.023.75 107 70.0-1301074.03 0.248 25
1,3-Dichlorobenzene ppbv 4.023.75 107 70.0-1301074.02 0.00 25
1,4-Dichlorobenzene ppbv 4.003.75 107 70.0-1301074.02 0.499 25
1,2-Dichloroethane ppbv 3.713.75 98.9 70.0-1301023.82 2.92 25
1,1-Dichloroethane ppbv 3.393.75 90.4 70.0-13092.03.45 1.75 25
1,1-Dichloroethene ppbv 3.383.75 90.1 70.0-13092.33.46 2.34 25
cis-1,2-Dichloroethene ppbv 3.423.75 91.2 70.0-13091.23.42 0.00 25
trans-1,2-Dichloroethene ppbv 3.433.75 91.5 70.0-13092.33.46 0.871 25
1,2-Dichloropropane ppbv 3.413.75 90.9 70.0-13089.93.37 1.18 25
cis-1,3-Dichloropropene ppbv 3.513.75 93.6 70.0-13093.63.51 0.00 25
trans-1,3-Dichloropropene ppbv 3.603.75 96.0 70.0-13097.33.65 1.38 25
1,4-Dioxane (p-Dioxane)ppbv 3.573.75 95.2 70.0-14092.83.48 2.55 25
Ethanol ppbv 3.333.75 88.8 55.0-14889.93.37 1.19 25
Ethylbenzene ppbv 3.663.75 97.6 70.0-13096.83.63 0.823 25
Ethyl acetate ppbv 3.103.75 82.7 70.0-13082.43.09 0.323 25
4-Ethyltoluene ppbv 3.743.75 99.7 70.0-1301023.83 2.38 25
Trichlorofluoromethane ppbv 4.103.75 109 70.0-1301094.10 0.00 25
Dichlorodifluoromethane ppbv 3.433.75 91.5 64.0-1391033.87 12.1 25
1,1,2-Trichlorotrifluoroethane ppbv 3.623.75 96.5 70.0-13096.83.63 0.276 25
Dichlorotetrafluoroethane ppbv 3.513.75 93.6 70.0-1301094.08 15.0 25
n-Heptane ppbv 3.433.75 91.5 70.0-13092.53.47 1.16 25
Hexachloro-1,3-butadiene ppbv 4.003.75 107 70.0-1511053.95 1.26 25
n-Hexane ppbv 3.183.75 84.8 70.0-13085.63.21 0.939 25
Isopropylbenzene (Cumene)ppbv 3.773.75 101 70.0-1301013.77 0.00 25
Methylene Chloride ppbv 3.243.75 86.4 70.0-13085.63.21 0.930 25
2-Hexanone ppbv 3.433.75 91.5 70.0-14990.73.40 0.878 25
2-Butanone (MEK)ppbv 3.383.75 90.1 70.0-13091.73.44 1.76 25
4-Methyl-2-pentanone (MIBK)ppbv 4.063.75 108 70.0-13991.53.43 16.8 25
Methyl methacrylate ppbv 3.443.75 91.7 70.0-13091.73.44 0.00 25
Methyl-tert-butyl ether ppbv 3.463.75 92.3 70.0-13094.73.55 2.57 25
Naphthalene ppbv 4.093.75 109 70.0-1591104.11 0.488 25
2-Propanol ppbv 3.383.75 90.1 70.0-13990.43.39 0.295 25
Propylene ppbv 3.553.75 94.7 64.0-14497.63.66 3.05 25
Styrene ppbv 3.773.75 101 70.0-1301013.79 0.529 25
1,1,2,2-Tetrachloroethane ppbv 3.613.75 96.3 70.0-13096.33.61 0.00 25
Tetrachloroethene ppbv 3.953.75 105 70.0-1301084.05 2.50 25
Tetrahydrofuran ppbv 3.173.75 84.5 70.0-13785.13.19 0.629 25
Toluene ppbv 3.643.75 97.1 70.0-13098.93.71 1.90 25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653832
Forest City Brownfield
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3894801-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3894801-2
1,2,4-Trichlorobenzene ppbv 4.173.75 111 70.0-1601084.05 2.92 25
1,1,1-Trichloroethane ppbv 3.753.75 100 70.0-1301003.75 0.00 25
1,1,2-Trichloroethane ppbv 3.653.75 97.3 70.0-13097.93.67 0.546 25
Trichloroethene ppbv 3.703.75 98.7 70.0-13099.73.74 1.08 25
1,2,4-Trimethylbenzene ppbv 3.873.75 103 70.0-1301033.85 0.518 25
1,3,5-Trimethylbenzene ppbv 3.853.75 103 70.0-1301003.76 2.37 25
2,2,4-Trimethylpentane ppbv 3.223.75 85.9 70.0-13086.73.25 0.927 25
Vinyl chloride ppbv 3.563.75 94.9 70.0-13094.93.56 0.00 25
Vinyl bromide ppbv 3.823.75 102 70.0-1301043.89 1.82 25
Vinyl acetate ppbv 3.303.75 88.0 70.0-13089.63.36 1.80 25
m&p-Xylene ppbv 7.327.50 97.6 70.0-13097.97.34 0.273 25
o-Xylene ppbv 3.633.75 96.8 70.0-13097.33.65 0.549 25
1,4-Dichlorobenzene-d4 (IS)%97.1 60.0-14096.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
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Page 25 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653832
Forest City Brownfield
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2012881
TO-15
TO-15
VOA (MS) TO-15
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92653832002, 92653832003, 92653832004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3894919-3
Associated Lab Samples:92653832002, 92653832003, 92653832004
Matrix: Air
Analyzed
Tetrachloroethene ppbv ND 0.200 02/25/23 08:35
1,4-Dichlorobenzene-d4 (IS)%95.1 60.0-140 02/25/23 08:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3894919-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3894919-2
Tetrachloroethene ppbv 4.213.75 112 70.0-1301134.24 0.710 25
1,4-Dichlorobenzene-d4 (IS)%95.4 60.0-14095.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653832
Forest City Brownfield
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2012899
TO-15
TO-15
VOA (MS) TO-15
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92653832005, 92653832009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3895069-3
Associated Lab Samples:92653832005, 92653832009
Matrix: Air
Analyzed
Tetrachloroethene ppbv ND 0.200 02/25/23 08:23
1,4-Dichlorobenzene-d4 (IS)%92.3 60.0-140 02/25/23 08:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3895069-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3895069-2
Tetrachloroethene ppbv 4.263.75 114 70.0-1301124.20 1.42 25
1,4-Dichlorobenzene-d4 (IS)%95.4 60.0-14095.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653832
Forest City Brownfield
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2013530
TO-15
TO-15
VOA (MS) TO-15
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92653832001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3895446-3
Associated Lab Samples:92653832001
Matrix: Air
Analyzed
Tetrachloroethene ppbv ND 0.200 02/27/23 10:57
1,4-Dichlorobenzene-d4 (IS)%90.4 60.0-140 02/27/23 10:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3895446-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3895446-2
Tetrachloroethene ppbv 4.253.75 113 70.0-1301144.27 0.469 25
1,4-Dichlorobenzene-d4 (IS)%96.0 60.0-14096.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 32
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92653832
Forest City Brownfield
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 32
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92653832
Forest City Brownfield
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92653832001 2012373 2012373VP-1 TO-15 TO-15
92653832001 2013530 2013530VP-1 TO-15 TO-15
92653832002 2012373 2012373VP-2 TO-15 TO-15
92653832002 2012881 2012881VP-2 TO-15 TO-15
92653832003 2012373 2012373VP-3 TO-15 TO-15
92653832003 2012881 2012881VP-3 TO-15 TO-15
92653832004 2012373 2012373VP-4 TO-15 TO-15
92653832004 2012881 2012881VP-4 TO-15 TO-15
92653832005 2012373 2012373VP-6 TO-15 TO-15
92653832005 2012899 2012899VP-6 TO-15 TO-15
92653832006 2012373 2012373VP-7 TO-15 TO-15
92653832007 2012373 2012373VP-8 TO-15 TO-15
92653832008 2012373 2012373VP-9 TO-15 TO-15
92653832009 2012373 2012373VP-10 TO-15 TO-15
92653832009 2012899 2012899VP-10 TO-15 TO-15
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2023 11:00 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 32
Page 31 of 32
Page 32 of 32
Attachment C
Photo Log

PHOTOGRAPHIC LOG
Site Name:
Florence Mill Brownfield Project
Site Location:
186 Mill Street, Forest City, Rutherford County, NC
Brownfield Project#
09003-05-081
Photo No. 1 Date: 2/21/23

Direction Photo Taken: Southeast
Description: Helium Leak Test performed at permanent soil vapor monitoring points VP-1/VP-2.
Photo No. 2
Date: 2/21/23

Direction Photo Taken: South
Description: Helium Leak Test performed at permanent soil vapor monitoring points VP-3/VP-4.

PHOTOGRAPHIC LOG
Site Name:
Florence Mill Brownfield Project
Site Location:
186 Mill Street, Forest City, Rutherford County, NC
Brownfield Project#
09003-05-081
Photo No. 3 Date: 2/21/23

Direction Photo Taken: East
Description: Helium Leak Test performed at permanent soil vapor monitoring points VP-5/VP-6.
Photo No. 4
Date: 2/21/23

Direction Photo Taken: Northeast
Description: Helium Leak Test performed at permanent soil vapor monitoring points VP-7/VP-8.

PHOTOGRAPHIC LOG
Site Name:
Florence Mill Brownfield Project
Site Location:
186 Mill Street, Forest City, Rutherford County, NC
Brownfield Project#
09003-05-081
Photo No. 5 Date: 2/21/23

Direction Photo Taken: East
Description: Helium Leak Test performed at permanent soil vapor monitoring points VP-9/VP-10.

Attachment D
AECOM Soil Gas and Air Sampling Procedures

(Rev1) March 13, 2018

AECOM – North Carolina Standard Operating Procedures

1. Purpose and Scope
Standard operating procedure for the collection of soil gas samples using laboratory provided Summa canisters.
2. Procedure
2.1 Required Equipment:

• Project Health and Safety Plan (HASP)
• Work Plan
• Summa Canister with a Flow Regulator from a certified laboratory (precalibrated for an 0.5 hour interval)
• Field forms – Summa Canister Field Sampling Data Sheet
• ¼” Stainless steel nuts and ferrules
• AMS Probe Kit or Hand Auger
• 1/4" OD x 1/8" ID Teflon tubing
• #2 driller sand
• Hydraulic cement or bentonite
• Water • Ziplock bags • Helium detector • Helium
• Hand Vacuum Pump or Gilian GilAir Pump
• Tedlar bags
• Safety Cones
• Laminated Sign to notify Air Sampling in progress
• Chain of Custody (COC)
• FedEx forms
• Standard wrench set
• Digital camera

2.2 AMS Soil Gas Sampling Method

1. Prior to sampling, locate any underground utilities to insure the safety of subsurface work conditions.
2. Use a 1½ inch stainless steel concrete bit and rotary hammer drill to core an entrance into the concrete or
asphalt slab if needed.
3. Attach Teflon tubing to the barb tang of the retractable stainless steel screened soil gas vapor sampling tip.
4. Cut the tubing to the desired length so you can feed it through extra extension rods.

5. Attach the Retractable stainless steel screened soil gas vapor sampling tip to the extension rod. Place the
extension drive adaptor to the opposite end of extension rod to protect threads when using the rotary hammer
drill.

(Rev1) March 13, 2018

6. Place the tip and the extension rod into the cored out hole and place the hammer drill in line with the extension
drive adaptor.
7. Using the hammer drill, drive the tip and extension rod into the ground and add extension rods as needed to the
desired depth beneath the ground surface. Fully tighten rods together to protect threads.
8. Using the jack supplied in the kit, jack out the extension rod a couple of inches to release the screen.
9. With the screen released, use a hand held vacuum pump to purge the subsurface air through the Teflon tubing.
10. After the soil gas vapor sampler is purged, connect the stainless steel summa canister to the Teflon tubing using
air tight stainless steel fittings. Utilize the laboratory supplied flow controller to pull the sample over the desired
time interval.

11. To remove the retractable stainless steel vapor sampling tip, use the jack supplied in the kit. Connect it under
the extension drive adaptor and continue to jack the tip out of the ground fully.
12. Dissassemble the stainless steel vapor sampling tip.
13. Remove the Teflon tubing from the barb tang at the top of tip and dispose of the tubing.
14. Decontaminate the tip with soap that does not affect environmental parameters (Liquinox) and use a soft-bristle
brush to wash away all dirt from the extensions and tip parts. Rinse with clean fresh water and let air dry.
2.3 Permanent Soil Gas Vapor Sampler:
1. Permanent sampling tips can also be installed using the same method as described above. However, a different
sampling tip is installed.

2. The tip shown above is a permanent tip that can be used for multiple vapor monitoring events. The design is the
same but uses a Teflon umbrella to seal the screen into place. (Bentonite can also be placed in the hole above
the screen to provide a tighter seal for a longer period of time).
3. Sampling from the permanent tips can be performed using the method described above.

(Rev1) March 13, 2018

2.4 AMS Vapor Implants Sampling Method
1. Prior to sampling, locate any underground utilities to insure the safety of subsurface work conditions.
2. Use a clean, stainless steel hand auger to auger down to the desired depth of soil gas vapor sampling beneath
the ground surface. Note: Vapor implant should not be placed in saturated soils.
3. Attach Teflon tubing to the barbed tang of a 6” AMS Vapor Implant (AMS Item #21010). Make sure that the
connection between the barbed end of the implant and the Teflon tubing is secure.

4. Lower the AMS Vapor Implant and attached tubing into the borehole until the Implant reaches the desired depth.
The top of the vapor implant should be a minimum of five feet below ground surface.
5. Cut the tubing to the desired length so that you have approximately 2’ of extra tubing to attach to the summa
canister.
6. Using #2A filter sand, add enough sand to cover the 6” Implant and 2-3” above the Implant. Check the depth of
sand using a measuring tape.
7. Add 10-12” of hydraulic cement or bentonite to the top of the sand to create a seal. Check the depth of sand
using a measuring tape. If using bentonite, hydrate the bentonite to ensure a proper seal. Wait 2 hours or until
the hydraulic cement has fully hardened, whichever is longer.
8. Use a hand held vacuum pump to purge the subsurface air through the Teflon tubing. Purge a minimum of one
pore volume of the borehole. The pore volume should be a minimum of the volume of the tubing and sand filter pack.
Calculate pore volume using formula: v = π ra2La + π rt2Lt where:
v = Volume
La = Length of sand-filled annular space, and
ra = Radius of annular space
Lt = Length of tubing, and
rt = Radius of tubing

9. Thread the tubing through the helium leak test device (helium chamber).
10. Attach the helium detector to the helium leak test device. Attach the helium container to the leak test device
using teflon tubing and fill the leak test device with helium until the helium detector reads >50%.
11. Use the hand pump to fill a 1 Liter tedlar bag with air from the sample port.
12. Close the tedlar bag and detach it from the pump.
13. Turn off the flow of helium into the helium leak test device.
14. Remove the helium detector from the leak test device and allow the helium detector reading to reach 0 ppm.
15. Insert the helium detector into the silicon tubing attached to the tedlar bag and open valve on the bag.
16. Record the reading. If the reading is below 10% of the value measured within the test device, proceed to the
next step. If the reading is above 10%, repeat the leak test and reconstruct the sample point as necessary.

(Rev1) March 13, 2018

17. Be sure that the valve to the tedlar bag is open and that nothing is blocking the flow to the helium detector. The
detector may produce false readings if the detector pump is strained or if methane is present in the soil gas.
18. After the helium test has been satisfactorily completed and soil gas vapor sampler is purged, connect the
stainless steel summa canister to the Teflon tubing using air tight stainless steel fittings. Utilize the laboratory
supplied flow controller to pull the sample over the desired time interval.
19. To remove the stainless steel Implant, break up the hydraulic seal. Tug gently on the Teflon tubing until the
Implant is freed.
20. Remove the Teflon tubing from the barb and dispose of the tubing and the disposable stainless steel Implant.
21. Backfill borehole.
3. Records
a. Summa Canister Field Data Sheet
b. Equipment Calibration Sheets
4. Attachments
a. Summa Canister Field Data Sheet
Site:
Samplers:
Date:
Sample#
Location
Summa Canister ID
Flow Controller ID
NO/NO/NO/NO/NO/
Purge Time (Start)
Purge Time (Stop)
Total Purge Time (min)
Purge Volume
PID Test of Purge Air
Initial Tracer Gas Results
Sample Time (Start)
Sample Time (Stop)
Total Sample Time (min)
Sample Volume
YES / NO YES / NO YES / NO YES / NO YES / NO
Final Tracer Gas Results
Summa Canister Sampling Field Data Sheet