09003_Florence Mill_Final Grade Sample Rpt_2018.08.11

AECOM
1600 Perimeter Park Drive, Suite 400
Morrisville, NC 27560
Phone: [phone]
Fax: [phone]
Memorandum
This memorandum summarizes the results of final grade sampling of exposed soil at the Forest City
Brownfield Project Site (the Site).
Objectives:
After final grading of the Site, collect samples of exposed soil at four locations.
Analyze soils samples for the following: volatile organic compounds (VOCs), semi-volatile
organic compounds (SVOCs), and RCRA metals, including arsenic, barium, cadmium,
chromium (speciated), mercury, lead, selenium, and silver.
Summary:
On July 17, 2018, after final grading of the Site was completed, AECOM collected samples of exposed
soil from four locations (SB-1, SB-2, SB-3, and SB-4). These locations are shown on the attached Soil
Sampling Locations Map. Sample locations were selected in the vicinity of former dry-cleaning
operations and remediation to represent the maximum risk. Soil samples were collected from the
surface (0” to 6”) using a stainless-steel hand auger and were submitted to SGS Accutest of Orlando,
FL for analysis of VOCs, SVOCs, and eight RCRA metals, consistent with the Environmental
Management Plan (EMP) for the site.
Soil sampling results are present in the attached Soil Analytical Results Table. Arsenic exceeded the
NC Residential Health-Based Preliminary Soil Remediation Goal (Soil PSRG) at all four sampling
locations. Chromium was detected in all four samples as well, but the speciated analyses indicated
that hexavalent chromium was present at less than 1 mg/kg in each sample. VOCs detected included
tetrachloroethylene (PCE) and cis-1,2-dichloroethylene (cDCE), which relate to historic dry-cleaning
activity at the site.
Discussion:
The North Carolina Department of Environmental Quality (NCDEQ), has calculated a site specific
protection of groundwater value of 138 µg/kg for PCE under the Dry-Cleaning Solvent Clean-up Act
[URS Corporation, February 2017]. All detections were below this result.
Date: Monday, July 30, 2018
To: Tracy Wahl (NC Brownfields – Asheville Regional Office)
CC: John Condray and Jimmy Clay (Town of Forest City)
From: Conan Fitzgerald (AECOM)
Subject: Results of Final Grade Sampling – Forest City Brownfields Project Site
Page 2 of 5

The metals analysis results are similar to the borrow material analyses results submitted to the
NCDEQ Brownfields department by email on August 8, 2017. The average arsenic result for the final
grade samples is slightly less than the average result for the borrow material, while all of the final
grade hexavalent chromium results are less than their corresponding analyses in the borrow material.
Conclusions:
Final Grade sampling indicates that the exposed soil is safe for unrestricted use at the site. The
metals detected are consistent with the background concentrations detected in the borrow soil
approved for use at the site. VOCs detected are below residential health based criteria, as well as the
site specific protection of groundwater value for PCE.
Attachments
Figure Soil Sampling Locations
Table Soil Analytical Results

References
Fitzgerald, Conan (AECOM), email correspondence to Tracy Wahl (NCDEQ-Brownfields), August 8,
2017 regarding “Forest City Borrow Soil Samples”..
URS Corporation, “Risk-Based Corrective Action Report Forms for North Carolina Dry-Cleaning
Solvent Cleanup Act Program”, February 2, 2017.

Table and Figure
Table 1
Post Grading Soil Analyses
Flemington Mills Brownfield Project
Forest City, North Carlina
Job Number:
Account:Pro ect:
Pro ect Number:Legend:Hit Exceed
Client Sam le ID:NC Soil PSRG - NC Soil PSRG - NC Soil PSRG - SB-1 SB-2 SB-3 SB-4
Lab Sam le ID:Residential Industrial Protection o FA55659-1 FA55659-FA55659-FA55659-
Date Sam led:Health-Based Health-Based Groundwate 7/9/2018 7/9/2018 7/9/2018 7/9/2018Matrix:NCDENR 2/18 NCDENR 2/18 NCDENR 2/18 Soil Soil Soil Soil
Acetone ug/kg 12000000 100000000 25000 ND (10) ND (11) 11.3 JB a 18.9 JB a
cis-1,2-Dichloroethylen ug/kg 31000 470000 410 ND (1.4) 2.2 J ND (1.5)ND (1.7)
Tetrachloroethylen ug/kg 17000 82000 138 ND (1.3) 6.8 73.8 6.7
Arsenic mg/kg 0.68 3 5.8 6.5 c 7.4 c 12.0 c 6.0 c
Barium mg/kg 3100 47000 580 161 c 110 c 113 c 147 c
Chromium mg/kg 23000 350000 360000 58.1 c 84.6 c 40.3 c 98.9 c
Lead mg/kg NE NE 270 25.6 c 28.3 c 19.7 c 25.7 c
Mercur mg/kg 2.3 9.7 1 0.020 J 0.05 0.026 J 0.028 J
Chromium, Hexavalen mg/kg 0.31 6.5 3.8 0.84 0.46 U 0.55 0.67
Solids, Percen %---83.9 82.8 87.1 83.7
60547658.1
NE - Criteria not established
PoG - Protection of Groundwater criteria for Soil under NC Preliminary Soil Remediation Goals
NC DSCA - North Carolina Dry-Cleaning Solvent Cleanup Program
SGS Orlando, FL Jul 17, 2018 16:38 pm
FA55659
AECOM, INC.
Forest City, N
Results flagged as "Exceed" if any of the selected criteria exceeded (most stringent
MS Volatiles (SW846 8260B)
Metals Analysi
General Chemistr
purposes only. SGS assumes no responsibility for errors in regulatory documents or changes to criteria detailed in later versions of th
referenced regulation. It is the responsibility of the user to verify these limits before using or reporting any dat
7 results exceeded regulatory criteriaHITS ONLY. Only parameters detected in at least one sample are shown
Footnotes:
a Suspected laboratory contaminant.
Site specific PoG for PCE is 138 ug/kg, as calculated by the NC DSCA program 2/3/2017.c Sample dilution required due to difficult matrix.
Analysis performed at SGS Dayton, NJ.
Regulatory limits listed in this document have been obtained from the latest version of the regulations cited and are used for adviso
Q:\DCS\Projects\L‐URS\Jobs4\_Projects\Forest City\5 Deliverables\5.1 Working Documents\5.1.5 Rpt\fa55659_table_hits edited.xlsx
APPROX. SCALE, ft.
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LEGEND
FINAL GRADE SOIL SAMPLE
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07/17/18
Technical Report for
AECOM, INC.
Forest City, NC
60547658.1
SGS Job Number: FA55659
Sampling Date: 07/09/18
Report to:
AECOM, INC.
[e-mail]
ATTN: Martha Meyers
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc.  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone]  fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Heather Wandrey 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 07/17/18
e-Hardcopy 2.0
Automated Report
80
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
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Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Case Narrative/Conformance Summary ..............................................................4
Section 3: Summary of Hits ....................................................................................................10
Section 4: Sample Results ........................................................................................................11
4.1: FA55659-1: SB-1 ..........................................................................................................12
4.2: FA55659-2: SB-2 ..........................................................................................................19
4.3: FA55659-3: SB-3 ..........................................................................................................26
4.4: FA55659-4: SB-4 ..........................................................................................................33
Section 5: Misc. Forms ............................................................................................................40
5.1: Chain of Custody ...........................................................................................................41
5.2: Analyst Legend ..............................................................................................................44
Section 6: MS Volatiles - QC Data Summaries .....................................................................45
6.1: Method Blank Summary ................................................................................................46
6.2: Blank Spike Summary ...................................................................................................48
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................50
Section 7: MS Semi-volatiles - QC Data Summaries ............................................................52
7.1: Method Blank Summary ................................................................................................53
7.2: Blank Spike Summary ...................................................................................................56
7.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................59
Section 8: Metals Analysis - QC Data Summaries ................................................................62
8.1: Prep QC MP34003: As,Ba,Cd,Cr,Pb,Se,Ag ..................................................................63
8.2: Prep QC MP34022: Hg ..................................................................................................68
Section 9: Misc. Forms (SGS Dayton, NJ) .............................................................................73
9.1: Chain of Custody ...........................................................................................................74
9.2: Analyst Legend ..............................................................................................................76
Section 10: General Chemistry - QC Data (SGS Dayton, NJ) .............................................77
10.1: Method Blank and Spike Results Summary ................................................................78
10.2: Duplicate Results Summary ........................................................................................79
10.3: Matrix Spike Results Summary ...................................................................................80
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Sample Summary
AECOM, INC.
Job No:FA55659
Forest City, NC
Project No: 60547658.1
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA55659-1 07/09/18 14:40 EL 07/10/18 SO Soil SB-1
FA55659-2 07/09/18 15:00 EL 07/10/18 SO Soil SB-2
FA55659-3 07/09/18 15:15 EL 07/10/18 SO Soil SB-3
FA55659-4 07/09/18 15:30 EL 07/10/18 SO Soil SB-4
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: AECOM, INC. Job FA55659
Site: Forest City, NC Report 7/17/2018 2:55:34
4 Sample(s), 0 Trip Blank(s) and 0 Field Blank(s) were collected on 07/09/2018 and were received at SGS North America Inc -
Orlando on 07/10/2018 properly preserved, at 3.9 Deg. C and intact. These Samples received an SGS Orlando job number of
FA55659. A listing of the Laboratory Sample ID, Client Sample ID and dates of collection are presented in the Results
Summary Section.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For
more information, please refer to QC summary pages.
MS Volatiles By Method SW846 8260B
Matrix: SO Batch ID: V2B351
All samples were analyzed within the recommended method holding time.
Sample(s) FA55659-2MS, FA55659-2MSD were used as the QC samples indicated.
Sample(s) FA55659-3, FA55659-4 have compound(s) reported with a “B” qualifier, indicating analyte is found in the associated method blank.
Matrix Spike Recovery(s) for 1,1-Dichloroethylene, Acetone, Carbon Tetrachloride, Cyclohexane, Dichlorodifluoromethane, Freon 113, Methyl Acetate, Methylcyclohexane, Tetrachloroethylene, Trichlorofluoromethane, Vinyl Chloride are outside control limits. Probable cause is due to matrix interference.
Matrix Spike Duplicate Recovery(s) for 1,2,3-Trichlorobenzene, 1,2,4-Trichlorobenzene, Cyclohexane, Dichlorodifluoromethane, Freon 113, Methyl Acetate, Methylcyclohexane, Trichlorofluoromethane, Vinyl Chloride are outside control limits. Probable cause is due to matrix interference.
FA55659-3 for Acetone: Suspected laboratory contaminant.
FA55659-4 for Acetone: Suspected laboratory contaminant.
MS Semi-volatiles By Method SW846 8270D
Matrix: SO Batch ID: OP70835
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) FA55659-1MS, FA55659-1MSD were used as the QC samples indicated.
FA55659-1 for 3,3'-Dichlorobenzidine: Associated CCV outside of control limits high, sample was ND.
FA55659-2 for 3,3'-Dichlorobenzidine: Associated CCV outside of control limits high, sample was ND.
FA55659-3 for 3,3'-Dichlorobenzidine: Associated CCV outside of control limits high, sample was ND.
FA55659-4 for 3,3'-Dichlorobenzidine: Associated CCV outside of control limits high, sample was ND.
Metals Analysis By Method SW846 6010D Matrix: SO Batch ID: MP34003
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) FA55659-1DUP, FA55659-1MS, FA55659-1MSD, FA55659-1SDL were used as the QC samples for metals.
Matrix Spike Recovery(s) for Chromium, Arsenic, Cadmium, Selenium, Silver are outside control limits. Spike amount low relative to the sample amount. Refer to lab control or spike blank for recovery information. Matrix Spike Duplicate Recovery(s) for Arsenic, Cadmium, Chromium, Selenium, Silver are outside control limits. Probable cause is due to matrix interference.
Matrix Spike Recovery(s) for Chromium are outside control limits. Spike amount low relative to the sample amount. Refer to lab control or spike blank for recovery information.
RPD(s) for Duplicate for Chromium are outside control limits for sample MP34003-D1. High RPD due to possible sample non-homogeneity.
RPD(s) for Serial Dilution for Arsenic, Barium, Chromium, Lead are outside control limits for sample MP34003-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).

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Metals Analysis By Method SW846 6010D Matrix: SO Batch ID: MP34003
FA55659-1 for Arsenic: Sample dilution required due to difficult matrix.
FA55659-1 for Barium: Sample dilution required due to difficult matrix.
FA55659-1 for Cadmium: Sample dilution required due to difficult matrix.
FA55659-1 for Chromium: Sample dilution required due to difficult matrix.
FA55659-1 for Lead: Sample dilution required due to difficult matrix. FA55659-1 for Selenium: Sample dilution required due to difficult matrix.
FA55659-1 for Silver: Sample dilution required due to difficult matrix. FA55659-2 for Arsenic: Sample dilution required due to difficult matrix.
FA55659-2 for Barium: Sample dilution required due to difficult matrix. FA55659-2 for Cadmium: Sample dilution required due to difficult matrix.
FA55659-2 for Chromium: Sample dilution required due to difficult matrix.
FA55659-2 for Lead: Sample dilution required due to difficult matrix.
FA55659-2 for Selenium: Sample dilution required due to difficult matrix.
FA55659-2 for Silver: Sample dilution required due to difficult matrix.
FA55659-3 for Arsenic: Sample dilution required due to difficult matrix.
FA55659-3 for Barium: Sample dilution required due to difficult matrix.
FA55659-3 for Cadmium: Sample dilution required due to difficult matrix.
FA55659-3 for Chromium: Sample dilution required due to difficult matrix. FA55659-3 for Lead: Sample dilution required due to difficult matrix.
FA55659-3 for Selenium: Sample dilution required due to difficult matrix. FA55659-3 for Silver: Sample dilution required due to difficult matrix.
FA55659-4 for Arsenic: Sample dilution required due to difficult matrix.
FA55659-4 for Barium: Sample dilution required due to difficult matrix.
FA55659-4 for Cadmium: Sample dilution required due to difficult matrix.
FA55659-4 for Chromium: Sample dilution required due to difficult matrix.
FA55659-4 for Lead: Sample dilution required due to difficult matrix.
FA55659-4 for Selenium: Sample dilution required due to difficult matrix.
FA55659-4 for Silver: Sample dilution required due to difficult matrix.
MP34003-SD1 for Chromium: Serial dilution indicates possible matrix interference.
MP34003-SD1 for Barium: Serial dilution indicates possible matrix interference.
MP34003-SD1 for Lead: Serial dilution indicates possible matrix interference. MP34003-S1 for Arsenic: Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
MP34003-S1 for Cadmium: Spike recovery indicates possible matrix interference and/or sample non-homogeneity. MP34003-S1 for Selenium: Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
MP34003-S1 for Silver: Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
Metals Analysis By Method SW846 7471B Matrix: SO Batch ID: MP34022
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) FA55684-1MS, FA55684-1MSD, FA55684-1SDL, FA55684-1DUP were used as the QC samples for metals. RPD(s) for Duplicate for Mercury are outside control limits for sample MP34022-D1. RPD acceptable due to low duplicate and sample concentrations.
RPD(s) for Serial Dilution for Mercury are outside control limits for sample MP34022-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
General Chemistry By Method SM19 2540G Matrix: SO Batch ID: GN79174
Sample(s) FA55659-3DUP were used as the QC samples for Solids, Percent.

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General Chemistry By Method SW846 3060A/7196A Matrix: SO Batch ID: N:GP14493
FA55659-1 for Chromium, Hexavalent: Analysis performed at SGS Dayton, NJ.
FA55659-2 for Chromium, Hexavalent: Analysis performed at SGS Dayton, NJ.
FA55659-3 for Chromium, Hexavalent: Analysis performed at SGS Dayton, NJ.
FA55659-4 for Chromium, Hexavalent: Analysis performed at SGS Dayton, NJ.

SGS Orlando certifies that this report meets the project requirements for analytical data produced for the samples as received at
SGS Orlando and as stated on the COC. SGS Orlando certifies that the data meets the Data Quality Objectives for
precision, accuracy and completeness as specified in the SGS Orlando Quality Manual except as noted above. This report is to
be used in its entirety. SGS Orlando is not responsible for any assumptions of data quality if partial data packages are used.

Narrative prepared by:

_______________________________________
Ellen Pampel, LogIn Supervisor (signature on file)

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Laboratory Report Glossary 

Client Sample ID:   Normally refers to a point of collection – a monitoring well, discharge outfall, treatment facility 
intake, soil core grid location and depth, or any other identification client assigns to a sample. 
Lab Sample ID:   Letter prefix identifies one of SGS Accutest laboratories and the rest is a consecutive number of 
the job (or SDG) received. Number after dash is a sample number and it is unequivocally linked in the LIMS to the 
Client Sample ID (see above). 
Matrix (Matrix Code): 
 AQ‐ Water Samples 
 SO‐ Soil/Solid Samples 
 LIQ‐ Non‐Water Liquid Samples 
 OIL‐ Oil Samples 
Matrix Type: 
 SW for Surface Water 
 SO for Soil/Sediment 
 GW   for Ground Water 
 DW for Drinking Water 
All available definitions are found on Chain of Custody form.   

Deg. C:   Degrees Celsius, measurement of temperature. 
Method:   Analytical and preparation methods used for the analysis, with the version or revision identified.   
Date Sampled:  This information is entered from Chain of Custody at the time of login for every sample.   
Date Received:    When the job was received by SGS Accutest Laboratories. 
Percent Solids:    Applicable only to SO matrix. For other matrices this field defaults to “n/a”. 
Run #:  Provides information how many attempts were made in the analysis of the sample. LIMS can merge 
information from several attempts and lists all of them, including dilution, confirmation, etc. #1 designation is 
assigned to the analytical run with majority of analytes reported from it, not necessarily in chronological order. 
File ID:  Actual instrument data acquisition file that produced the final result. Letter prefix identifies the 
instrument; the rest is a consecutive injection number for that instrument. 
DF (Dilution Factor):  Most common reasons are either to fit into the range of the calibration, or alleviate matrix 
interference.   DF other than 1 are accompanied with a comment at the end of the sample report.   
Analyzed:  Date of analysis. 
By:  Field Technician or Analyst uniquely identified by initials.   
Prep Date:  Date of sample preparation.   If hold time is 72 hours or less, time of preparation is also indicated. 
Prep Batch:  Letter prefix OP followed by a consecutive number. For VOC analysis preparation happens at the time 
of analysis, therefore analytical batch and preparation batch are the same. Size of prep batch is limited to 20 field 
samples of similar matrix and the entire batch should be completed within 12 hour time. 
Analytical Batch:   Letter prefix identifies the instrument and is followed by a consecutive number. Not limited by a 
number of samples.   
Initial Weight or Initial Volume:   Raw sample size used for preparation.   
Final Volume:  Final volume of extract. If different from method‐prescribed volume, reasons are reflected in the 
comments at the end of the report form. 
CAS Number:   Chemical Abstracts Service (CAS), a division of the American Chemical Society. 
Compound:   Most commonly used names of chemical compounds.   
Result:  Depending on project requirements, this field could be set up as text, such as ND (for Non Detected) or a 
number. The number may be reported with a qualifier. 
MDL (Method Detection Limit): This value is defined as 99% probability that analyte above this concentration is 
positively (qualitatively) identified. 
RL (Reporting Limit): This value is supported by the low calibration standard and defines lowest point of 
quantitative identification of analyte. 
DL (Detection Limit):   The smallest analyte concentration that can be demonstrated to be different from zero or a 
blank concentration with 99% confidence.   At the DL, the false positive rate (Type I error) is 1%. 
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LOD (Limit of Detection):     The smallest concentration of a substance that must be present in a sample in order to 
be detected at the DL with 99% confidence. At the LOD, the false negative rate (Type II error) is 1%. 
LOQ (Limit of Quantitation):   The smallest concentration that produces a quantitative result with known and 
recorded precision and bias. 
Units:   ug/l (micrograms per liter) for aqueous samples and ug/kg (micrograms per kilogram) for solids (or ppb – 
parts per billion). The units could be set according to project or state‐specific requirements, such as mg/l 
(milligrams per liter), or mg/kg (milligrams per kilogram).   
Qualifiers (Q):  Definitions of most often used qualifiers are found at the bottom of each result page. Applied 
depending on the program – state‐specific (Florida A.C. 62‐160), CLP‐like, AFCEE, DOD QSM, etc. 
Tentatively Identified Compound (TIC):  Used when client requests a search for analytes that are not part of 
instrument calibration. Unknown peaks are compared with published spectral libraries and best match is reported 
as TIC.   
Surrogate (S1, S2, S3 etc.): are positive controls that are used in most organics methods to ascertain preparation 
efficiency and matrix effect in individual samples. These chemicals mimic common method constituents but are 
unlikely to be found in real samples. Recoveries can be reported for every analytical run used in the analysis. 
IS (Internal Standard IS1, IS2, IS3, etc):   quantitative reference used to adjust for instrument performance 
fluctuations.   
Area (of chromatographic peak):   signal intensity directly related to compound concentration. 
RT (Retention Time):   time required for analyte to traverse the length of analytical column. Used for compound 
identification. 
ICAL (Initial Calibration):   Must pass calibration criteria established by method. 
ICV (Independent Calibration Verification): Used to verify ICAL preparation and concentration of calibration points. 
CCV (Continuing Calibration Verification): Used to assess calibration status of the instrument and must recover 
within established acceptance criteria. 
MB (Method Blank):   is a negative batch control. MB is an aliquot of matrix free of analyte of interest (either 
ASTM Type II water or appropriate solid substance) that is put through all the preparation and possible clean‐up 
steps alongside investigative (field) samples. MB should be free of interferences above a set level.   
BS (Blank Spike, Laboratory Fortified Blank ‐ LFB, Laboratory Control Sample ‐ LCS):   is a positive control used to 
determine method accuracy ‐ in clean matrix, i.e. matrix free of analytes of interest. 
BSD (Blank Spike Duplicate):   Used to assess recovery reproducibility ‐ method precision – per analytical method 
requirement. %Recovery and Relative Percent Difference (%RPD) are compared with the established acceptance 
criteria. 
MS and/or MSD (Matrix Spike and Matrix Spike Duplicate):   positive batch controls which indicate matrix effect 
on the precision and accuracy of the method in given sample matrix. Results are expressed in %Recovery and 
Relative Percent Difference (%RPD), and compared with the established acceptance criteria. 
DUP (Matrix Duplicate):   Positive batch control, a way of assessing laboratory’s precision; however, the 
composition of the samples is unknown and may not yield meaningful results. 
REC (Recovery in Percent):   expresses method accuracy.   
RPD (Relative Percent Difference):  expresses method precision. 
Limits:   Recovery limits for surrogates and spikes. 
SDG: Sample delivery group. 

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On 07/12/2018, 4 Sample(s), 0 Trip Blank(s) and 0 Field Blank(s) were received at SGS North America Inc. at a maximum
corrected temperature of 2.9 C. Samples were intact and chemically preserved, unless noted below. A SGS North America Inc. Job
Number of FA55659 was assigned to the project. Laboratory sample ID, client sample ID and dates of sample collection are
detailed in the report’s Results Summary Section.
Specified quality control criteria were achieved for this job except as noted below. For more information, please refer to the
analytical results and QC summary pages.
Client:SGS Orlando, FL
Site:URSNCM: Forest City, NC
Job No FA55659
Report Date 7/16/2018 5:56:30 PM
CASE NARRATIVE / CONFORMANCE SUMMARY
Compounds qualified as out of range in the continuing calibration summary report are acceptable as per method requirements when
there is a high bias but the sample result is non-detect.
General Chemistry By Method SW846 3060A/7196A
Matrix:SO Batch ID:GP14493
All samples were prepared within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) FA55659-1DUP, FA55659-1MS were used as the QC samples for Chromium, Hexavalent.
Matrix Spike Recovery(s) for Chromium, Hexavalent are outside control limits. Soluble XCR matrix spike recovery indicates
possible matrix interference. Good post spike recovery (105%) on this sample.
SGS North America Inc. certifies that data reported for samples received, listed on the associated custody chain or analytical task
order, were produced to specifications meeting the Quality System precision, accuracy and completeness objectives except as noted.
Estimated non-standard method measurement uncertainty data is available on request, based on quality control bias and implicit for
standard methods. Acceptable uncertainty requires tested parameter quality control data to meet method criteria.
SGS North America Inc. is not responsible for data quality assumptions if partial reports are used and recommends that this report
be used in its entirety. Data release is authorized by SGS North America Inc indicated via signature on the report cover
Monday, July 16, 2018 Page 1 of 1
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Summary of Hits Page 1 of 1
Job Number:FA55659
Account:AECOM, INC.
Project:Forest City, NC
Collected:07/09/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA55659-1 SB-1
Arsenic a 6.5 4.1 0.83 mg/kg SW846 6010D
Barium a 161 83 0.41 mg/kg SW846 6010D
Chromium a 58.1 4.1 0.41 mg/kg SW846 6010D
Lead a 25.6 8.3 0.41 mg/kg SW846 6010D
Mercury 0.020 J 0.047 0.0047 mg/kg SW846 7471B
Chromium, Hexavalent b 0.84 0.48 0.45 mg/kg SW846 3060A/7196A
FA55659-2 SB-2
cis-1,2-Dichloroethylene 2.2 J 5.5 1.5 ug/kg SW846 8260B
Tetrachloroethylene 6.8 5.5 1.4 ug/kg SW846 8260B
Arsenic a 7.4 2.3 0.47 mg/kg SW846 6010D
Barium a 110 47 0.23 mg/kg SW846 6010D
Chromium a 84.6 2.3 0.23 mg/kg SW846 6010D
Lead a 28.3 4.7 0.23 mg/kg SW846 6010D
Mercury 0.050 0.045 0.0045 mg/kg SW846 7471B
FA55659-3 SB-3
Acetone c 11.3 JB 54 11 ug/kg SW846 8260B
Tetrachloroethylene 73.8 5.4 1.4 ug/kg SW846 8260B
Arsenic a 12.0 2.6 0.52 mg/kg SW846 6010D
Barium a 113 52 0.26 mg/kg SW846 6010D
Chromium a 40.3 2.6 0.26 mg/kg SW846 6010D
Lead a 19.7 5.2 0.26 mg/kg SW846 6010D
Mercury 0.026 J 0.045 0.0045 mg/kg SW846 7471B
Chromium, Hexavalent b 0.55 0.46 0.44 mg/kg SW846 3060A/7196A
FA55659-4 SB-4
Acetone c 18.9 JB 61 12 ug/kg SW846 8260B
Tetrachloroethylene 6.7 6.1 1.6 ug/kg SW846 8260B
Arsenic a 6.0 2.8 0.57 mg/kg SW846 6010D
Barium a 147 57 0.28 mg/kg SW846 6010D
Chromium a 98.9 2.8 0.28 mg/kg SW846 6010D
Lead a 25.7 5.7 0.28 mg/kg SW846 6010D
Mercury 0.028 J 0.043 0.0043 mg/kg SW846 7471B
Chromium, Hexavalent b 0.67 0.48 0.45 mg/kg SW846 3060A/7196A
(a) Sample dilution required due to difficult matrix.
(b) Analysis performed at SGS Dayton, NJ.
(c) Suspected laboratory contaminant.
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SGS LabLink@15:37 17-Jul-2018
Sample Results
Report of Analysis
Orlando, FL
Section 4
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SGS LabLink@15:37 17-Jul-2018
Report of Analysis Page 1 of 2
Client Sample ID:SB-1
Lab Sample ID:FA55659-1 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8260B Percent Solids:83.9
Project:Forest City, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2B9358.D 1 07/12/18 18:44 SP n/a n/a V2B351
Run #2
Initial Weight Final Volume
Run #1 5.72 g 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 52 10 ug/kg
71-43-2 Benzene ND 5.2 1.3 ug/kg
74-97-5 Bromochloromethane ND 5.2 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.2 1.0 ug/kg
75-25-2 Bromoform ND 5.2 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 26 7.6 ug/kg
75-15-0 Carbon Disulfide ND 5.2 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.2 1.1 ug/kg
108-90-7 Chlorobenzene ND 5.2 1.0 ug/kg
75-00-3 Chloroethane ND 5.2 2.1 ug/kg
67-66-3 Chloroform ND 5.2 1.4 ug/kg
110-82-7 Cyclohexane ND 5.2 1.3 ug/kg
124-48-1 Dibromochloromethane ND 5.2 1.0 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.2 2.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.2 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.2 2.1 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.2 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.2 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.2 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.2 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.2 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.2 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.2 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.2 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.2 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.2 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.2 1.0 ug/kg
123-91-1 1,4-Dioxane ND 210 42 ug/kg
100-41-4 Ethylbenzene ND 5.2 1.0 ug/kg
76-13-1 Freon 113 ND 5.2 1.4 ug/kg
591-78-6 2-Hexanone ND 26 7.8 ug/kg
98-82-8 Isopropylbenzene ND 5.2 1.0 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS LabLink@15:37 17-Jul-2018
Report of Analysis Page 2 of 2
Client Sample ID:SB-1
Lab Sample ID:FA55659-1 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8260B Percent Solids:83.9
Project:Forest City, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate ND 26 9.3 ug/kg
74-83-9 Methyl Bromide ND 5.2 2.1 ug/kg
74-87-3 Methyl Chloride ND 5.2 2.1 ug/kg
108-87-2 Methylcyclohexane ND 5.2 1.8 ug/kg
75-09-2 Methylene Chloride ND 10 4.2 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 26 7.8 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.2 1.0 ug/kg
100-42-5 Styrene ND 5.2 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.2 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.2 1.3 ug/kg
108-88-3 Toluene ND 5.2 1.0 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.2 1.5 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.2 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.2 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.2 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.2 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.2 2.1 ug/kg
75-01-4 Vinyl Chloride ND 5.2 1.0 ug/kg
m,p-Xylene ND 10 1.1 ug/kg
95-47-6 o-Xylene ND 5.2 1.0 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%75-124%
17060-07-0 1,2-Dichloroethane-D4 107%72-135%
2037-26-5 Toluene-D8 104%75-126%
460-00-4 4-Bromofluorobenzene 103%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS LabLink@15:37 17-Jul-2018
Report of Analysis Page 1 of 3
Client Sample ID:SB-1
Lab Sample ID:FA55659-1 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:83.9
Project:Forest City, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X061247.D 1 07/12/18 12:27 MV 07/11/18 10:15 OP70835 SX2551
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
105-60-2 Caprolactam ND 200 32 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 200 22 ug/kg
95-57-8 2-Chlorophenol ND 200 24 ug/kg
120-83-2 2,4-Dichlorophenol ND 200 23 ug/kg
105-67-9 2,4-Dimethylphenol ND 200 53 ug/kg
51-28-5 2,4-Dinitrophenol ND 990 200 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 400 79 ug/kg
95-48-7 2-Methylphenol ND 200 24 ug/kg
3&4-Methylphenol ND 200 33 ug/kg
88-75-5 2-Nitrophenol ND 200 22 ug/kg
100-02-7 4-Nitrophenol ND 990 200 ug/kg
87-86-5 Pentachlorophenol ND 990 200 ug/kg
108-95-2 Phenol ND 200 20 ug/kg
58-90-2 2,3,4,6-Tetrachlorophenol ND 200 24 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 200 32 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 200 23 ug/kg
83-32-9 Acenaphthene ND 200 21 ug/kg
208-96-8 Acenaphthylene ND 200 20 ug/kg
98-86-2 Acetophenone ND 200 20 ug/kg
120-12-7 Anthracene ND 200 22 ug/kg
1912-24-9 Atrazine ND 200 24 ug/kg
100-52-7 Benzaldehyde ND 990 200 ug/kg
56-55-3 Benzo(a)anthracene ND 200 20 ug/kg
50-32-8 Benzo(a)pyrene ND 200 23 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 22 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 21 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 26 ug/kg
92-52-4 1,1'-Biphenyl ND 200 20 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 200 21 ug/kg
85-68-7 Butyl benzyl phthalate ND 200 40 ug/kg
86-74-8 Carbazole ND 200 28 ug/kg
106-47-8 4-Chloroaniline ND 200 50 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS LabLink@15:37 17-Jul-2018
Report of Analysis Page 2 of 3
Client Sample ID:SB-1
Lab Sample ID:FA55659-1 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:83.9
Project:Forest City, NC
ABN TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
111-91-1 bis(2-Chloroethoxy)methane ND 200 20 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 200 23 ug/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 200 25 ug/kg
91-58-7 2-Chloronaphthalene ND 200 20 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 200 20 ug/kg
218-01-9 Chrysene ND 200 20 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 25 ug/kg
132-64-9 Dibenzofuran ND 200 20 ug/kg
91-94-1 3,3'-Dichlorobenzidine a ND 200 47 ug/kg
84-66-2 Diethyl Phthalate ND 400 40 ug/kg
131-11-3 Dimethyl Phthalate ND 200 40 ug/kg
117-84-0 Di-n-octyl Phthalate ND 200 40 ug/kg
84-74-2 Di-n-butyl Phthalate ND 400 79 ug/kg
121-14-2 2,4-Dinitrotoluene ND 200 20 ug/kg
606-20-2 2,6-Dinitrotoluene ND 200 26 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 400 40 ug/kg
206-44-0 Fluoranthene ND 200 20 ug/kg
86-73-7 Fluorene ND 200 21 ug/kg
118-74-1 Hexachlorobenzene ND 200 20 ug/kg
87-68-3 Hexachlorobutadiene ND 200 20 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 200 40 ug/kg
67-72-1 Hexachloroethane ND 200 23 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 24 ug/kg
78-59-1 Isophorone ND 200 20 ug/kg
91-57-6 2-Methylnaphthalene ND 200 20 ug/kg
91-20-3 Naphthalene ND 200 20 ug/kg
88-74-4 2-Nitroaniline ND 200 46 ug/kg
99-09-2 3-Nitroaniline ND 200 23 ug/kg
100-01-6 4-Nitroaniline ND 200 57 ug/kg
98-95-3 Nitrobenzene ND 200 20 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 200 20 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 200 21 ug/kg
85-01-8 Phenanthrene ND 200 20 ug/kg
129-00-0 Pyrene ND 200 23 ug/kg
95-94-3 1,2,4,5-Tetrachlorobenzene ND 200 20 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 69%40-102%
4165-62-2 Phenol-d5 69%41-100%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS LabLink@15:37 17-Jul-2018
Report of Analysis Page 3 of 3
Client Sample ID:SB-1
Lab Sample ID:FA55659-1 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:83.9
Project:Forest City, NC
ABN TCL (SOM01.1) List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
118-79-6 2,4,6-Tribromophenol 86%42-108%
4165-60-0 Nitrobenzene-d5 66%40-105%
321-60-8 2-Fluorobiphenyl 73%43-107%
1718-51-0 Terphenyl-d14 87%45-119%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS LabLink@15:37 17-Jul-2018
Report of Analysis Page 1 of 1
Client Sample ID:SB-1
Lab Sample ID:FA55659-1 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Percent Solids:83.9
Project:Forest City, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic a 6.5 4.1 0.83 mg/kg 10 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Barium a 161 83 0.41 mg/kg 10 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Cadmium a 0.21 U 1.7 0.21 mg/kg 10 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Chromium a 58.1 4.1 0.41 mg/kg 10 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Lead a 25.6 8.3 0.41 mg/kg 10 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Mercury 0.020 J 0.047 0.0047 mg/kg 1 07/16/18 07/16/18 JC SW846 7471B 2 SW846 7471B 4
Selenium a 0.99 U 8.3 0.99 mg/kg 10 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Silver a 0.34 U 4.1 0.34 mg/kg 10 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
(1) Instrument QC Batch: MA15039
(2) Instrument QC Batch: MA15045
(3) Prep QC Batch: MP34003
(4) Prep QC Batch: MP34022
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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SGS LabLink@15:37 17-Jul-2018
Report of Analysis Page 1 of 1
Client Sample ID:SB-1
Lab Sample ID:FA55659-1 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Percent Solids:83.9
Project:Forest City, NC
General Chemistry
Analyte Result RL MDL Units DF Analyzed By Method
Chromium, Hexavalent a 0.84 0.48 0.45 mg/kg 1 07/16/18 17:10 ANJ SW846 3060A/7196A
Solids, Percent 83.9 %1 07/12/18 10:39 JC SM19 2540G
(a) Analysis performed at SGS Dayton, NJ.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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SGS LabLink@15:37 17-Jul-2018
Report of Analysis Page 1 of 2
Client Sample ID:SB-2
Lab Sample ID:FA55659-2 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8260B Percent Solids:82.8
Project:Forest City, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2B9359.D 1 07/12/18 19:08 SP n/a n/a V2B351
Run #2
Initial Weight Final Volume
Run #1 5.52 g 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 55 11 ug/kg
71-43-2 Benzene ND 5.5 1.3 ug/kg
74-97-5 Bromochloromethane ND 5.5 1.6 ug/kg
75-27-4 Bromodichloromethane ND 5.5 1.1 ug/kg
75-25-2 Bromoform ND 5.5 1.1 ug/kg
78-93-3 2-Butanone (MEK)ND 27 8.0 ug/kg
75-15-0 Carbon Disulfide ND 5.5 1.1 ug/kg
56-23-5 Carbon Tetrachloride ND 5.5 1.1 ug/kg
108-90-7 Chlorobenzene ND 5.5 1.1 ug/kg
75-00-3 Chloroethane ND 5.5 2.2 ug/kg
67-66-3 Chloroform ND 5.5 1.5 ug/kg
110-82-7 Cyclohexane ND 5.5 1.4 ug/kg
124-48-1 Dibromochloromethane ND 5.5 1.1 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.5 2.1 ug/kg
106-93-4 1,2-Dibromoethane ND 5.5 1.1 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.5 2.2 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.5 1.1 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.5 1.1 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.5 1.3 ug/kg
75-34-3 1,1-Dichloroethane ND 5.5 1.9 ug/kg
107-06-2 1,2-Dichloroethane ND 5.5 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.5 1.1 ug/kg
156-59-2 cis-1,2-Dichloroethylene 2.2 5.5 1.5 ug/kg J
156-60-5 trans-1,2-Dichloroethylene ND 5.5 1.1 ug/kg
78-87-5 1,2-Dichloropropane ND 5.5 1.1 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.5 1.1 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.5 1.1 ug/kg
123-91-1 1,4-Dioxane ND 220 44 ug/kg
100-41-4 Ethylbenzene ND 5.5 1.1 ug/kg
76-13-1 Freon 113 ND 5.5 1.4 ug/kg
591-78-6 2-Hexanone ND 27 8.2 ug/kg
98-82-8 Isopropylbenzene ND 5.5 1.1 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-2
Lab Sample ID:FA55659-2 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8260B Percent Solids:82.8
Project:Forest City, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate ND 27 9.7 ug/kg
74-83-9 Methyl Bromide ND 5.5 2.2 ug/kg
74-87-3 Methyl Chloride ND 5.5 2.2 ug/kg
108-87-2 Methylcyclohexane ND 5.5 1.9 ug/kg
75-09-2 Methylene Chloride ND 11 4.4 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 27 8.2 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.5 1.1 ug/kg
100-42-5 Styrene ND 5.5 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.5 1.1 ug/kg
127-18-4 Tetrachloroethylene 6.8 5.5 1.4 ug/kg
108-88-3 Toluene ND 5.5 1.1 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.5 1.5 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.5 1.1 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.5 1.1 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.5 1.1 ug/kg
79-01-6 Trichloroethylene ND 5.5 1.1 ug/kg
75-69-4 Trichlorofluoromethane ND 5.5 2.2 ug/kg
75-01-4 Vinyl Chloride ND 5.5 1.1 ug/kg
m,p-Xylene ND 11 1.2 ug/kg
95-47-6 o-Xylene ND 5.5 1.1 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%75-124%
17060-07-0 1,2-Dichloroethane-D4 109%72-135%
2037-26-5 Toluene-D8 105%75-126%
460-00-4 4-Bromofluorobenzene 108%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Lab Sample ID:FA55659-2 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:82.8
Project:Forest City, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X061231.D 1 07/11/18 17:34 MV 07/11/18 10:15 OP70835 SX2550
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
105-60-2 Caprolactam ND 200 32 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 200 23 ug/kg
95-57-8 2-Chlorophenol ND 200 25 ug/kg
120-83-2 2,4-Dichlorophenol ND 200 23 ug/kg
105-67-9 2,4-Dimethylphenol ND 200 54 ug/kg
51-28-5 2,4-Dinitrophenol ND 1000 200 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 400 81 ug/kg
95-48-7 2-Methylphenol ND 200 24 ug/kg
3&4-Methylphenol ND 200 33 ug/kg
88-75-5 2-Nitrophenol ND 200 22 ug/kg
100-02-7 4-Nitrophenol ND 1000 200 ug/kg
87-86-5 Pentachlorophenol ND 1000 200 ug/kg
108-95-2 Phenol ND 200 20 ug/kg
58-90-2 2,3,4,6-Tetrachlorophenol ND 200 24 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 200 32 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 200 23 ug/kg
83-32-9 Acenaphthene ND 200 21 ug/kg
208-96-8 Acenaphthylene ND 200 20 ug/kg
98-86-2 Acetophenone ND 200 20 ug/kg
120-12-7 Anthracene ND 200 23 ug/kg
1912-24-9 Atrazine ND 200 24 ug/kg
100-52-7 Benzaldehyde ND 1000 200 ug/kg
56-55-3 Benzo(a)anthracene ND 200 20 ug/kg
50-32-8 Benzo(a)pyrene ND 200 24 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 22 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 21 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 26 ug/kg
92-52-4 1,1'-Biphenyl ND 200 20 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 200 21 ug/kg
85-68-7 Butyl benzyl phthalate ND 200 40 ug/kg
86-74-8 Carbazole ND 200 28 ug/kg
106-47-8 4-Chloroaniline ND 200 51 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-2
Lab Sample ID:FA55659-2 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:82.8
Project:Forest City, NC
ABN TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
111-91-1 bis(2-Chloroethoxy)methane ND 200 20 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 200 23 ug/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 200 25 ug/kg
91-58-7 2-Chloronaphthalene ND 200 20 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 200 20 ug/kg
218-01-9 Chrysene ND 200 21 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 25 ug/kg
132-64-9 Dibenzofuran ND 200 20 ug/kg
91-94-1 3,3'-Dichlorobenzidine a ND 200 48 ug/kg
84-66-2 Diethyl Phthalate ND 400 40 ug/kg
131-11-3 Dimethyl Phthalate ND 200 40 ug/kg
117-84-0 Di-n-octyl Phthalate ND 200 40 ug/kg
84-74-2 Di-n-butyl Phthalate ND 400 81 ug/kg
121-14-2 2,4-Dinitrotoluene ND 200 20 ug/kg
606-20-2 2,6-Dinitrotoluene ND 200 26 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 400 40 ug/kg
206-44-0 Fluoranthene ND 200 20 ug/kg
86-73-7 Fluorene ND 200 22 ug/kg
118-74-1 Hexachlorobenzene ND 200 20 ug/kg
87-68-3 Hexachlorobutadiene ND 200 20 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 200 40 ug/kg
67-72-1 Hexachloroethane ND 200 24 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 25 ug/kg
78-59-1 Isophorone ND 200 20 ug/kg
91-57-6 2-Methylnaphthalene ND 200 20 ug/kg
91-20-3 Naphthalene ND 200 20 ug/kg
88-74-4 2-Nitroaniline ND 200 47 ug/kg
99-09-2 3-Nitroaniline ND 200 23 ug/kg
100-01-6 4-Nitroaniline ND 200 58 ug/kg
98-95-3 Nitrobenzene ND 200 20 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 200 20 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 200 22 ug/kg
85-01-8 Phenanthrene ND 200 20 ug/kg
129-00-0 Pyrene ND 200 23 ug/kg
95-94-3 1,2,4,5-Tetrachlorobenzene ND 200 20 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 73%40-102%
4165-62-2 Phenol-d5 73%41-100%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-2
Lab Sample ID:FA55659-2 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:82.8
Project:Forest City, NC
ABN TCL (SOM01.1) List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
118-79-6 2,4,6-Tribromophenol 90%42-108%
4165-60-0 Nitrobenzene-d5 71%40-105%
321-60-8 2-Fluorobiphenyl 81%43-107%
1718-51-0 Terphenyl-d14 93%45-119%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:SB-2
Lab Sample ID:FA55659-2 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Percent Solids:82.8
Project:Forest City, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic a 7.4 2.3 0.47 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Barium a 110 47 0.23 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Cadmium a 0.12 U 0.94 0.12 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Chromium a 84.6 2.3 0.23 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Lead a 28.3 4.7 0.23 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Mercury 0.050 0.045 0.0045 mg/kg 1 07/16/18 07/16/18 JC SW846 7471B 2 SW846 7471B 4
Selenium a 0.56 U 4.7 0.56 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Silver a 0.19 U 2.3 0.19 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
(1) Instrument QC Batch: MA15039
(2) Instrument QC Batch: MA15045
(3) Prep QC Batch: MP34003
(4) Prep QC Batch: MP34022
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Lab Sample ID:FA55659-2 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Percent Solids:82.8
Project:Forest City, NC
General Chemistry
Analyte Result RL MDL Units DF Analyzed By Method
Chromium, Hexavalent a 0.46 U 0.48 0.46 mg/kg 1 07/16/18 17:15 ANJ SW846 3060A/7196A
Solids, Percent 82.8 %1 07/12/18 10:39 JC SM19 2540G
(a) Analysis performed at SGS Dayton, NJ.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 2
Client Sample ID:SB-3
Lab Sample ID:FA55659-3 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8260B Percent Solids:87.1
Project:Forest City, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2B9360.D 1 07/12/18 19:32 SP n/a n/a V2B351
Run #2
Initial Weight Final Volume
Run #1 5.28 g 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone a 11.3 54 11 ug/kg JB
71-43-2 Benzene ND 5.4 1.3 ug/kg
74-97-5 Bromochloromethane ND 5.4 1.6 ug/kg
75-27-4 Bromodichloromethane ND 5.4 1.1 ug/kg
75-25-2 Bromoform ND 5.4 1.1 ug/kg
78-93-3 2-Butanone (MEK)ND 27 7.9 ug/kg
75-15-0 Carbon Disulfide ND 5.4 1.1 ug/kg
56-23-5 Carbon Tetrachloride ND 5.4 1.1 ug/kg
108-90-7 Chlorobenzene ND 5.4 1.1 ug/kg
75-00-3 Chloroethane ND 5.4 2.2 ug/kg
67-66-3 Chloroform ND 5.4 1.4 ug/kg
110-82-7 Cyclohexane ND 5.4 1.4 ug/kg
124-48-1 Dibromochloromethane ND 5.4 1.1 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.4 2.1 ug/kg
106-93-4 1,2-Dibromoethane ND 5.4 1.1 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.4 2.2 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.4 1.1 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.4 1.1 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.4 1.3 ug/kg
75-34-3 1,1-Dichloroethane ND 5.4 1.9 ug/kg
107-06-2 1,2-Dichloroethane ND 5.4 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.4 1.1 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.4 1.5 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.4 1.1 ug/kg
78-87-5 1,2-Dichloropropane ND 5.4 1.1 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.4 1.1 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.4 1.1 ug/kg
123-91-1 1,4-Dioxane ND 220 44 ug/kg
100-41-4 Ethylbenzene ND 5.4 1.1 ug/kg
76-13-1 Freon 113 ND 5.4 1.4 ug/kg
591-78-6 2-Hexanone ND 27 8.2 ug/kg
98-82-8 Isopropylbenzene ND 5.4 1.1 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:SB-3
Lab Sample ID:FA55659-3 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8260B Percent Solids:87.1
Project:Forest City, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate ND 27 9.7 ug/kg
74-83-9 Methyl Bromide ND 5.4 2.2 ug/kg
74-87-3 Methyl Chloride ND 5.4 2.2 ug/kg
108-87-2 Methylcyclohexane ND 5.4 1.8 ug/kg
75-09-2 Methylene Chloride ND 11 4.3 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 27 8.2 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.4 1.1 ug/kg
100-42-5 Styrene ND 5.4 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.4 1.1 ug/kg
127-18-4 Tetrachloroethylene 73.8 5.4 1.4 ug/kg
108-88-3 Toluene ND 5.4 1.1 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.4 1.5 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.4 1.1 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.4 1.1 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.4 1.1 ug/kg
79-01-6 Trichloroethylene ND 5.4 1.1 ug/kg
75-69-4 Trichlorofluoromethane ND 5.4 2.2 ug/kg
75-01-4 Vinyl Chloride ND 5.4 1.1 ug/kg
m,p-Xylene ND 11 1.2 ug/kg
95-47-6 o-Xylene ND 5.4 1.1 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 109%75-124%
17060-07-0 1,2-Dichloroethane-D4 112%72-135%
2037-26-5 Toluene-D8 105%75-126%
460-00-4 4-Bromofluorobenzene 111%71-133%
(a) Suspected laboratory contaminant.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-3
Lab Sample ID:FA55659-3 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:87.1
Project:Forest City, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X061232.D 1 07/11/18 18:00 MV 07/11/18 10:15 OP70835 SX2550
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
105-60-2 Caprolactam ND 190 31 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 190 22 ug/kg
95-57-8 2-Chlorophenol ND 190 23 ug/kg
120-83-2 2,4-Dichlorophenol ND 190 22 ug/kg
105-67-9 2,4-Dimethylphenol ND 190 51 ug/kg
51-28-5 2,4-Dinitrophenol ND 960 190 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 380 77 ug/kg
95-48-7 2-Methylphenol ND 190 23 ug/kg
3&4-Methylphenol ND 190 31 ug/kg
88-75-5 2-Nitrophenol ND 190 21 ug/kg
100-02-7 4-Nitrophenol ND 960 190 ug/kg
87-86-5 Pentachlorophenol ND 960 190 ug/kg
108-95-2 Phenol ND 190 19 ug/kg
58-90-2 2,3,4,6-Tetrachlorophenol ND 190 23 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 190 31 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 190 22 ug/kg
83-32-9 Acenaphthene ND 190 20 ug/kg
208-96-8 Acenaphthylene ND 190 19 ug/kg
98-86-2 Acetophenone ND 190 19 ug/kg
120-12-7 Anthracene ND 190 21 ug/kg
1912-24-9 Atrazine ND 190 23 ug/kg
100-52-7 Benzaldehyde ND 960 190 ug/kg
56-55-3 Benzo(a)anthracene ND 190 19 ug/kg
50-32-8 Benzo(a)pyrene ND 190 23 ug/kg
205-99-2 Benzo(b)fluoranthene ND 190 21 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 190 20 ug/kg
207-08-9 Benzo(k)fluoranthene ND 190 25 ug/kg
92-52-4 1,1'-Biphenyl ND 190 19 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 190 20 ug/kg
85-68-7 Butyl benzyl phthalate ND 190 38 ug/kg
86-74-8 Carbazole ND 190 27 ug/kg
106-47-8 4-Chloroaniline ND 190 48 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:SB-3
Lab Sample ID:FA55659-3 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:87.1
Project:Forest City, NC
ABN TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
111-91-1 bis(2-Chloroethoxy)methane ND 190 19 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 190 22 ug/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 190 24 ug/kg
91-58-7 2-Chloronaphthalene ND 190 19 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 190 19 ug/kg
218-01-9 Chrysene ND 190 20 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 190 24 ug/kg
132-64-9 Dibenzofuran ND 190 19 ug/kg
91-94-1 3,3'-Dichlorobenzidine a ND 190 46 ug/kg
84-66-2 Diethyl Phthalate ND 380 38 ug/kg
131-11-3 Dimethyl Phthalate ND 190 38 ug/kg
117-84-0 Di-n-octyl Phthalate ND 190 38 ug/kg
84-74-2 Di-n-butyl Phthalate ND 380 77 ug/kg
121-14-2 2,4-Dinitrotoluene ND 190 19 ug/kg
606-20-2 2,6-Dinitrotoluene ND 190 25 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 380 38 ug/kg
206-44-0 Fluoranthene ND 190 19 ug/kg
86-73-7 Fluorene ND 190 21 ug/kg
118-74-1 Hexachlorobenzene ND 190 19 ug/kg
87-68-3 Hexachlorobutadiene ND 190 19 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 190 38 ug/kg
67-72-1 Hexachloroethane ND 190 23 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 190 23 ug/kg
78-59-1 Isophorone ND 190 19 ug/kg
91-57-6 2-Methylnaphthalene ND 190 19 ug/kg
91-20-3 Naphthalene ND 190 19 ug/kg
88-74-4 2-Nitroaniline ND 190 44 ug/kg
99-09-2 3-Nitroaniline ND 190 22 ug/kg
100-01-6 4-Nitroaniline ND 190 55 ug/kg
98-95-3 Nitrobenzene ND 190 19 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 190 19 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 190 21 ug/kg
85-01-8 Phenanthrene ND 190 19 ug/kg
129-00-0 Pyrene ND 190 22 ug/kg
95-94-3 1,2,4,5-Tetrachlorobenzene ND 190 19 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 68%40-102%
4165-62-2 Phenol-d5 68%41-100%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:SB-3
Lab Sample ID:FA55659-3 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:87.1
Project:Forest City, NC
ABN TCL (SOM01.1) List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
118-79-6 2,4,6-Tribromophenol 89%42-108%
4165-60-0 Nitrobenzene-d5 67%40-105%
321-60-8 2-Fluorobiphenyl 77%43-107%
1718-51-0 Terphenyl-d14 91%45-119%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS LabLink@15:37 17-Jul-2018
Report of Analysis Page 1 of 1
Client Sample ID:SB-3
Lab Sample ID:FA55659-3 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Percent Solids:87.1
Project:Forest City, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic a 12.0 2.6 0.52 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Barium a 113 52 0.26 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Cadmium a 0.13 U 1.0 0.13 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Chromium a 40.3 2.6 0.26 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Lead a 19.7 5.2 0.26 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Mercury 0.026 J 0.045 0.0045 mg/kg 1 07/16/18 07/16/18 JC SW846 7471B 2 SW846 7471B 4
Selenium a 0.63 U 5.2 0.63 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Silver a 0.21 U 2.6 0.21 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
(1) Instrument QC Batch: MA15039
(2) Instrument QC Batch: MA15045
(3) Prep QC Batch: MP34003
(4) Prep QC Batch: MP34022
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 1
Client Sample ID:SB-3
Lab Sample ID:FA55659-3 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Percent Solids:87.1
Project:Forest City, NC
General Chemistry
Analyte Result RL MDL Units DF Analyzed By Method
Chromium, Hexavalent a 0.55 0.46 0.44 mg/kg 1 07/16/18 17:15 ANJ SW846 3060A/7196A
Solids, Percent 87.1 %1 07/12/18 10:39 JC SM19 2540G
(a) Analysis performed at SGS Dayton, NJ.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 2
Client Sample ID:SB-4
Lab Sample ID:FA55659-4 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8260B Percent Solids:83.7
Project:Forest City, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2B9361.D 1 07/12/18 19:56 SP n/a n/a V2B351
Run #2
Initial Weight Final Volume
Run #1 4.93 g 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone a 18.9 61 12 ug/kg JB
71-43-2 Benzene ND 6.1 1.5 ug/kg
74-97-5 Bromochloromethane ND 6.1 1.8 ug/kg
75-27-4 Bromodichloromethane ND 6.1 1.2 ug/kg
75-25-2 Bromoform ND 6.1 1.2 ug/kg
78-93-3 2-Butanone (MEK)ND 30 8.8 ug/kg
75-15-0 Carbon Disulfide ND 6.1 1.2 ug/kg
56-23-5 Carbon Tetrachloride ND 6.1 1.2 ug/kg
108-90-7 Chlorobenzene ND 6.1 1.2 ug/kg
75-00-3 Chloroethane ND 6.1 2.4 ug/kg
67-66-3 Chloroform ND 6.1 1.6 ug/kg
110-82-7 Cyclohexane ND 6.1 1.5 ug/kg
124-48-1 Dibromochloromethane ND 6.1 1.2 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 6.1 2.3 ug/kg
106-93-4 1,2-Dibromoethane ND 6.1 1.2 ug/kg
75-71-8 Dichlorodifluoromethane ND 6.1 2.4 ug/kg
95-50-1 1,2-Dichlorobenzene ND 6.1 1.2 ug/kg
541-73-1 1,3-Dichlorobenzene ND 6.1 1.2 ug/kg
106-46-7 1,4-Dichlorobenzene ND 6.1 1.4 ug/kg
75-34-3 1,1-Dichloroethane ND 6.1 2.1 ug/kg
107-06-2 1,2-Dichloroethane ND 6.1 1.2 ug/kg
75-35-4 1,1-Dichloroethylene ND 6.1 1.2 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 6.1 1.7 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 6.1 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 6.1 1.2 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 6.1 1.2 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 6.1 1.2 ug/kg
123-91-1 1,4-Dioxane ND 240 49 ug/kg
100-41-4 Ethylbenzene ND 6.1 1.2 ug/kg
76-13-1 Freon 113 ND 6.1 1.6 ug/kg
591-78-6 2-Hexanone ND 30 9.1 ug/kg
98-82-8 Isopropylbenzene ND 6.1 1.2 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:SB-4
Lab Sample ID:FA55659-4 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8260B Percent Solids:83.7
Project:Forest City, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate ND 30 11 ug/kg
74-83-9 Methyl Bromide ND 6.1 2.4 ug/kg
74-87-3 Methyl Chloride ND 6.1 2.4 ug/kg
108-87-2 Methylcyclohexane ND 6.1 2.1 ug/kg
75-09-2 Methylene Chloride ND 12 4.8 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 30 9.1 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 6.1 1.2 ug/kg
100-42-5 Styrene ND 6.1 1.2 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 6.1 1.2 ug/kg
127-18-4 Tetrachloroethylene 6.7 6.1 1.6 ug/kg
108-88-3 Toluene ND 6.1 1.2 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 6.1 1.7 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 6.1 1.2 ug/kg
71-55-6 1,1,1-Trichloroethane ND 6.1 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane ND 6.1 1.2 ug/kg
79-01-6 Trichloroethylene ND 6.1 1.2 ug/kg
75-69-4 Trichlorofluoromethane ND 6.1 2.4 ug/kg
75-01-4 Vinyl Chloride ND 6.1 1.2 ug/kg
m,p-Xylene ND 12 1.3 ug/kg
95-47-6 o-Xylene ND 6.1 1.2 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%75-124%
17060-07-0 1,2-Dichloroethane-D4 112%72-135%
2037-26-5 Toluene-D8 104%75-126%
460-00-4 4-Bromofluorobenzene 104%71-133%
(a) Suspected laboratory contaminant.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:SB-4
Lab Sample ID:FA55659-4 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:83.7
Project:Forest City, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X061233.D 1 07/11/18 18:27 MV 07/11/18 10:15 OP70835 SX2550
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
ABN TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
105-60-2 Caprolactam ND 200 32 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 200 22 ug/kg
95-57-8 2-Chlorophenol ND 200 24 ug/kg
120-83-2 2,4-Dichlorophenol ND 200 23 ug/kg
105-67-9 2,4-Dimethylphenol ND 200 52 ug/kg
51-28-5 2,4-Dinitrophenol ND 990 200 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 390 79 ug/kg
95-48-7 2-Methylphenol ND 200 24 ug/kg
3&4-Methylphenol ND 200 32 ug/kg
88-75-5 2-Nitrophenol ND 200 21 ug/kg
100-02-7 4-Nitrophenol ND 990 200 ug/kg
87-86-5 Pentachlorophenol ND 990 200 ug/kg
108-95-2 Phenol ND 200 20 ug/kg
58-90-2 2,3,4,6-Tetrachlorophenol ND 200 24 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 200 32 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 200 23 ug/kg
83-32-9 Acenaphthene ND 200 21 ug/kg
208-96-8 Acenaphthylene ND 200 20 ug/kg
98-86-2 Acetophenone ND 200 20 ug/kg
120-12-7 Anthracene ND 200 22 ug/kg
1912-24-9 Atrazine ND 200 24 ug/kg
100-52-7 Benzaldehyde ND 990 200 ug/kg
56-55-3 Benzo(a)anthracene ND 200 20 ug/kg
50-32-8 Benzo(a)pyrene ND 200 23 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 22 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 20 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 26 ug/kg
92-52-4 1,1'-Biphenyl ND 200 20 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 200 20 ug/kg
85-68-7 Butyl benzyl phthalate ND 200 39 ug/kg
86-74-8 Carbazole ND 200 27 ug/kg
106-47-8 4-Chloroaniline ND 200 50 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:SB-4
Lab Sample ID:FA55659-4 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:83.7
Project:Forest City, NC
ABN TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
111-91-1 bis(2-Chloroethoxy)methane ND 200 20 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 200 23 ug/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 200 25 ug/kg
91-58-7 2-Chloronaphthalene ND 200 20 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 200 20 ug/kg
218-01-9 Chrysene ND 200 20 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 25 ug/kg
132-64-9 Dibenzofuran ND 200 20 ug/kg
91-94-1 3,3'-Dichlorobenzidine a ND 200 47 ug/kg
84-66-2 Diethyl Phthalate ND 390 39 ug/kg
131-11-3 Dimethyl Phthalate ND 200 39 ug/kg
117-84-0 Di-n-octyl Phthalate ND 200 39 ug/kg
84-74-2 Di-n-butyl Phthalate ND 390 79 ug/kg
121-14-2 2,4-Dinitrotoluene ND 200 20 ug/kg
606-20-2 2,6-Dinitrotoluene ND 200 25 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 390 39 ug/kg
206-44-0 Fluoranthene ND 200 20 ug/kg
86-73-7 Fluorene ND 200 21 ug/kg
118-74-1 Hexachlorobenzene ND 200 20 ug/kg
87-68-3 Hexachlorobutadiene ND 200 20 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 200 39 ug/kg
67-72-1 Hexachloroethane ND 200 23 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 24 ug/kg
78-59-1 Isophorone ND 200 20 ug/kg
91-57-6 2-Methylnaphthalene ND 200 20 ug/kg
91-20-3 Naphthalene ND 200 20 ug/kg
88-74-4 2-Nitroaniline ND 200 46 ug/kg
99-09-2 3-Nitroaniline ND 200 23 ug/kg
100-01-6 4-Nitroaniline ND 200 57 ug/kg
98-95-3 Nitrobenzene ND 200 20 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 200 20 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 200 21 ug/kg
85-01-8 Phenanthrene ND 200 20 ug/kg
129-00-0 Pyrene ND 200 23 ug/kg
95-94-3 1,2,4,5-Tetrachlorobenzene ND 200 20 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 71%40-102%
4165-62-2 Phenol-d5 71%41-100%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:SB-4
Lab Sample ID:FA55659-4 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Method:SW846 8270D SW846 3550C Percent Solids:83.7
Project:Forest City, NC
ABN TCL (SOM01.1) List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
118-79-6 2,4,6-Tribromophenol 90%42-108%
4165-60-0 Nitrobenzene-d5 69%40-105%
321-60-8 2-Fluorobiphenyl 78%43-107%
1718-51-0 Terphenyl-d14 91%45-119%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:SB-4
Lab Sample ID:FA55659-4 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Percent Solids:83.7
Project:Forest City, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic a 6.0 2.8 0.57 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Barium a 147 57 0.28 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Cadmium a 0.14 U 1.1 0.14 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Chromium a 98.9 2.8 0.28 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Lead a 25.7 5.7 0.28 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Mercury 0.028 J 0.043 0.0043 mg/kg 1 07/16/18 07/16/18 JC SW846 7471B 2 SW846 7471B 4
Selenium a 0.68 U 5.7 0.68 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
Silver a 0.23 U 2.8 0.23 mg/kg 5 07/11/18 07/12/18 DM SW846 6010D 1 SW846 3050B 3
(1) Instrument QC Batch: MA15039
(2) Instrument QC Batch: MA15045
(3) Prep QC Batch: MP34003
(4) Prep QC Batch: MP34022
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 1
Client Sample ID:SB-4
Lab Sample ID:FA55659-4 Date Sampled:07/09/18
Matrix:SO - Soil Date Received:07/10/18
Percent Solids:83.7
Project:Forest City, NC
General Chemistry
Analyte Result RL MDL Units DF Analyzed By Method
Chromium, Hexavalent a 0.67 0.48 0.45 mg/kg 1 07/16/18 17:15 ANJ SW846 3060A/7196A
Solids, Percent 83.7 %1 07/12/18 10:39 JC SM19 2540G
(a) Analysis performed at SGS Dayton, NJ.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
 Chain of Custody
 Analyst Legend
Orlando, FL
Section 5
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FA55659: Chain of Custody
Page 1 of 3
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5
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Job Number:FA55659 Client:AECOM
Date / Time Received:7/10/2018 9:15:00 AM Delivery Method:FED EX
Project:FOREST CITY, NC
Airbill #'s:1015899921360003281100812565568154
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.8);
Cooler 1: (3.9);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:4Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.1; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP Date:Date:7/10/2018 9:15:00 AM
FA55659: Chain of Custody
Page 2 of 3
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Accutest Laboratories Southeast •• ■ACCUTEST@ 4405 ��n�!�d, ?u! £��rt?ct�l,2s11 fASSt.S, PAGE. _ _.,__OF_1_ Accutest JOB #
LABORATORIES TEL. [phone] • FAX: [phone]
www .accutest.com Accutest uuote IF '"
':J<:::::, <:,· Client/ ReportinA Information
Company Name A.EC.n (IA
Accutest Samr,le #
2 3 t../
Field ID I Point of Collection
S�-4-
·:\l'll,i . ''
:: TURNAROUND TIME (Business Davs1
D 1 O Days Standard 0 7 Day RUSH □5 Day RUSH 0 3 Day EMERGENCY 0 2 Day EMERGENGY 0 1 Day EMERGENCY 0 OTHER
Approved By: I Rush Code
Emergency or Rush T/A Data Available VIA Email or Lablink
Proiect Information
Project Name:
Street
TOTAL# SAMPLED OF ov. MATRIX --2
"' Data I eliverable Information □ COMMERCIAL "A" (RESULTS ONLY) □ COMMERCIAL "B" (RESULA c:('.;d�:: .._ r
2 \
□ REDT1 �A LEVEL 3) . " ) □FULT1 i�li..11= OU=EN c i r i□EDD'S CLl NC 2a2aa
...... -
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•". -'•, ·· ··<:, .. < ::,-�amr ,.,, r.ustodll must be dn,-ument belnw e h time c:�mn!,:,c: channe nnssessinn inclurlinn coUriAr deliverv
Relinquished
5
Date Time: Received By:
6
Lab Use Onlv: Cuslody Seal in Place: Y N Temo Blank Provided: Y N
Relinquished by:
7
Preserved where Applicable: Y N Total# of Coolers:
Analvtica! Information
Comments / Remarks
I
Matrix Codes
DW -Drinking Water GW -Ground Waler WW-Water SW -Surface Water SO-Soll SL-Sludge 01-0ll LIO· Other liquid AIR-Air .SOL· Other Solid WP-Wipe
"" .... "'""
I._ Date lime: Re ued o/: ' · �,,-,i/1n/i�
Cooler Temperature (s) Celsius: 6 , '1
' '
Hexa
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a
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ent
c
hr
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um
*KT 07/11/2018
 
FA55659: Chain of Custody
Page 3 of 3
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Analyst Legend Page 1 of 1
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Initials Full Name Analysis Type
SP Sean Pioro MS Volatiles
MV Martha Valls MS Semi-volatiles
DM Dave Metzgar Metals Analysis
JC Jordan Cuoco Metals Analysis
JC Jordan Cuoco General Chemistry
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MS Volatiles
QC Data Summaries
Includes the following where applicable:
 Method Blank Summaries
 Blank Spike Summaries
 Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
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Method Blank Summary Page 1 of 2
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B351-MB 2B9353.D 1 07/12/18 SP n/a n/a V2B351
The QC reported here applies to the following samples:Method: SW846 8260B
FA55659-1, FA55659-2, FA55659-3, FA55659-4
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 21.0 50 10 ug/kg J
71-43-2 Benzene ND 5.0 1.2 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
75-15-0 Carbon Disulfide ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
110-82-7 Cyclohexane ND 5.0 1.3 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 1.9 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
123-91-1 1,4-Dioxane ND 200 40 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
76-13-1 Freon 113 ND 5.0 1.3 ug/kg
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
79-20-9 Methyl Acetate ND 25 8.9 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
108-87-2 Methylcyclohexane ND 5.0 1.7 ug/kg
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Method Blank Summary Page 2 of 2
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B351-MB 2B9353.D 1 07/12/18 SP n/a n/a V2B351
The QC reported here applies to the following samples:Method: SW846 8260B
FA55659-1, FA55659-2, FA55659-3, FA55659-4
CAS No.Compound Result RL MDL Units Q
75-09-2 Methylene Chloride ND 10 4.0 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 5.0 1.0 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
m,p-Xylene ND 10 1.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 105%72-135%
2037-26-5 Toluene-D8 105%75-126%
460-00-4 4-Bromofluorobenzene 103%71-133%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
75-37-6 Ethane, 1,1-difluoro-2.63 88 ug/kg JN
3680-02-2 Ethene, (methylsulfonyl)-3.74 120 ug/kg JN
Total TIC, Volatile 208 ug/kg J
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Blank Spike Summary Page 1 of 2
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B351-BS 2B9352.D 1 07/12/18 SP n/a n/a V2B351
The QC reported here applies to the following samples:Method: SW846 8260B
FA55659-1, FA55659-2, FA55659-3, FA55659-4
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 305 122 61-152
71-43-2 Benzene 50 54.9 110 76-126
74-97-5 Bromochloromethane 50 53.9 108 77-120
75-27-4 Bromodichloromethane 50 55.7 111 74-130
75-25-2 Bromoform 50 57.0 114 76-127
78-93-3 2-Butanone (MEK)250 282 113 75-137
75-15-0 Carbon Disulfide 50 53.5 107 72-122
56-23-5 Carbon Tetrachloride 50 55.3 111 78-133
108-90-7 Chlorobenzene 50 55.7 111 81-129
75-00-3 Chloroethane 50 55.0 110 68-133
67-66-3 Chloroform 50 52.7 105 72-123
110-82-7 Cyclohexane 50 56.6 113 73-126
124-48-1 Dibromochloromethane 50 56.0 112 76-127
96-12-8 1,2-Dibromo-3-chloropropane 50 56.2 112 70-137
106-93-4 1,2-Dibromoethane 50 57.9 116 77-126
75-71-8 Dichlorodifluoromethane 50 51.3 103 68-168
95-50-1 1,2-Dichlorobenzene 50 56.3 113 80-129
541-73-1 1,3-Dichlorobenzene 50 57.8 116 81-129
106-46-7 1,4-Dichlorobenzene 50 56.5 113 76-130
75-34-3 1,1-Dichloroethane 50 56.2 112 73-125
107-06-2 1,2-Dichloroethane 50 53.1 106 74-128
75-35-4 1,1-Dichloroethylene 50 56.2 112 81-136
156-59-2 cis-1,2-Dichloroethylene 50 56.1 112 74-126
156-60-5 trans-1,2-Dichloroethylene 50 57.6 115 70-127
78-87-5 1,2-Dichloropropane 50 55.0 110 74-125
10061-01-5 cis-1,3-Dichloropropene 50 53.5 107 80-123
10061-02-6 trans-1,3-Dichloropropene 50 56.2 112 75-131
123-91-1 1,4-Dioxane 1000 843 84 56-152
100-41-4 Ethylbenzene 50 54.2 108 77-123
76-13-1 Freon 113 50 50.6 101 71-129
591-78-6 2-Hexanone 250 293 117 72-133
98-82-8 Isopropylbenzene 50 57.3 115 80-136
79-20-9 Methyl Acetate 250 261 104 67-137
74-83-9 Methyl Bromide 50 54.5 109 65-139
74-87-3 Methyl Chloride 50 52.2 104 71-144
108-87-2 Methylcyclohexane 50 56.7 113 75-128
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 2
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B351-BS 2B9352.D 1 07/12/18 SP n/a n/a V2B351
The QC reported here applies to the following samples:Method: SW846 8260B
FA55659-1, FA55659-2, FA55659-3, FA55659-4
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
75-09-2 Methylene Chloride 50 54.3 109 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 288 115 76-132
1634-04-4 Methyl Tert Butyl Ether 50 55.3 111 77-120
100-42-5 Styrene 50 55.0 110 78-125
79-34-5 1,1,2,2-Tetrachloroethane 50 58.5 117 71-126
127-18-4 Tetrachloroethylene 50 58.9 118 79-130
108-88-3 Toluene 50 56.3 113 76-124
87-61-6 1,2,3-Trichlorobenzene 50 61.3 123 77-128
120-82-1 1,2,4-Trichlorobenzene 50 61.2 122 78-130
71-55-6 1,1,1-Trichloroethane 50 51.6 103 70-129
79-00-5 1,1,2-Trichloroethane 50 56.3 113 74-124
79-01-6 Trichloroethylene 50 55.3 111 75-128
75-69-4 Trichlorofluoromethane 50 54.1 108 73-145
75-01-4 Vinyl Chloride 50 54.7 109 76-141
m,p-Xylene 100 113 113 80-128
95-47-6 o-Xylene 50 53.4 107 80-132
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 98%75-124%
17060-07-0 1,2-Dichloroethane-D4 95%72-135%
2037-26-5 Toluene-D8 101%75-126%
460-00-4 4-Bromofluorobenzene 102%71-133%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA55659-2MS 2B9367.D 1 07/12/18 SP n/a n/a V2B351
FA55659-2MSD 2B9368.D 1 07/12/18 SP n/a n/a V2B351
FA55659-2 2B9359.D 1 07/12/18 SP n/a n/a V2B351
The QC reported here applies to the following samples:Method: SW846 8260B
FA55659-1, FA55659-2, FA55659-3, FA55659-4
FA55659-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone ND 341 524 154*343 517 151 1 61-152/27
71-43-2 Benzene ND 68.2 60.7 89 68.6 61.5 90 1 76-126/26
74-97-5 Bromochloromethane ND 68.2 62.6 92 68.6 63.5 93 1 77-120/24
75-27-4 Bromodichloromethane ND 68.2 68.3 100 68.6 69.8 102 2 74-130/25
75-25-2 Bromoform ND 68.2 64.3 94 68.6 66.2 96 3 76-127/26
78-93-3 2-Butanone (MEK)ND 341 314 92 343 314 92 0 75-137/25
75-15-0 Carbon Disulfide ND 68.2 50.5 74 68.6 53.0 77 5 72-122/29
56-23-5 Carbon Tetrachloride ND 68.2 52.2 77*68.6 53.3 78 2 78-133/29
108-90-7 Chlorobenzene ND 68.2 63.4 93 68.6 63.9 93 1 81-129/29
75-00-3 Chloroethane ND 68.2 60.8 89 68.6 64.5 94 6 68-133/29
67-66-3 Chloroform ND 68.2 63.6 93 68.6 64.2 94 1 72-123/26
110-82-7 Cyclohexane ND 68.2 37.0 54*68.6 36.5 53*1 73-126/32
124-48-1 Dibromochloromethane ND 68.2 64.4 94 68.6 65.8 96 2 76-127/27
96-12-8 1,2-Dibromo-3-chloropropane ND 68.2 63.4 93 68.6 65.0 95 2 70-137/29
106-93-4 1,2-Dibromoethane ND 68.2 66.1 97 68.6 67.0 98 1 77-126/26
75-71-8 Dichlorodifluoromethane ND 68.2 31.0 45*68.6 32.3 47*4 68-168/29
95-50-1 1,2-Dichlorobenzene ND 68.2 60.9 89 68.6 59.1 86 3 80-129/32
541-73-1 1,3-Dichlorobenzene ND 68.2 62.3 91 68.6 61.5 90 1 81-129/33
106-46-7 1,4-Dichlorobenzene ND 68.2 61.6 90 68.6 61.2 89 1 76-130/32
75-34-3 1,1-Dichloroethane ND 68.2 66.0 97 68.6 67.2 98 2 73-125/27
107-06-2 1,2-Dichloroethane ND 68.2 69.4 102 68.6 70.1 102 1 74-128/23
75-35-4 1,1-Dichloroethylene ND 68.2 53.3 78*68.6 55.6 81 4 81-136/28
156-59-2 cis-1,2-Dichloroethylene 2.2 J 68.2 61.4 87 68.6 63.0 89 3 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 68.2 61.3 90 68.6 62.9 92 3 70-127/27
78-87-5 1,2-Dichloropropane ND 68.2 65.0 95 68.6 66.2 96 2 74-125/25
10061-01-5 cis-1,3-Dichloropropene ND 68.2 62.2 91 68.6 62.2 91 0 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 68.2 65.9 97 68.6 66.0 96 0 75-131/28
123-91-1 1,4-Dioxane ND 1360 1520 112 1370 1660 121 9 56-152/37
100-41-4 Ethylbenzene ND 68.2 60.1 88 68.6 60.9 89 1 77-123/31
76-13-1 Freon 113 ND 68.2 34.0 50*68.6 33.6 49*1 71-129/30
591-78-6 2-Hexanone ND 341 338 99 343 337 98 0 72-133/26
98-82-8 Isopropylbenzene ND 68.2 60.5 89 68.6 60.5 88 0 80-136/32
79-20-9 Methyl Acetate ND 341 526 154*343 522 152*1 67-137/30
74-83-9 Methyl Bromide ND 68.2 56.9 83 68.6 62.8 92 10 65-139/31
74-87-3 Methyl Chloride ND 68.2 55.7 82 68.6 59.4 87 6 71-144/27
108-87-2 Methylcyclohexane ND 68.2 34.7 51*68.6 33.2 48*4 75-128/31
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA55659-2MS 2B9367.D 1 07/12/18 SP n/a n/a V2B351
FA55659-2MSD 2B9368.D 1 07/12/18 SP n/a n/a V2B351
FA55659-2 2B9359.D 1 07/12/18 SP n/a n/a V2B351
The QC reported here applies to the following samples:Method: SW846 8260B
FA55659-1, FA55659-2, FA55659-3, FA55659-4
FA55659-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
75-09-2 Methylene Chloride ND 68.2 75.1 110 68.6 76.0 111 1 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 341 354 104 343 353 103 0 76-132/26
1634-04-4 Methyl Tert Butyl Ether ND 68.2 65.3 96 68.6 66.9 97 2 77-120/24
100-42-5 Styrene ND 68.2 60.2 88 68.6 60.3 88 0 78-125/30
79-34-5 1,1,2,2-Tetrachloroethane ND 68.2 70.0 103 68.6 69.3 101 1 71-126/30
127-18-4 Tetrachloroethylene 6.8 68.2 60.1 78*68.6 62.7 81 4 79-130/31
108-88-3 Toluene ND 68.2 62.5 92 68.6 64.0 93 2 76-124/30
87-61-6 1,2,3-Trichlorobenzene ND 68.2 52.2 77 68.6 49.7 72*5 77-128/35
120-82-1 1,2,4-Trichlorobenzene ND 68.2 55.1 81 68.6 51.8 75*6 78-130/34
71-55-6 1,1,1-Trichloroethane ND 68.2 54.7 80 68.6 54.5 79 0 70-129/27
79-00-5 1,1,2-Trichloroethane ND 68.2 68.3 100 68.6 68.8 100 1 74-124/28
79-01-6 Trichloroethylene ND 68.2 62.2 91 68.6 62.3 91 0 75-128/27
75-69-4 Trichlorofluoromethane ND 68.2 41.7 61*68.6 42.0 61*1 73-145/31
75-01-4 Vinyl Chloride ND 68.2 46.5 68*68.6 51.7 75*11 76-141/27
m,p-Xylene ND 136 127 93 137 129 94 2 80-128/30
95-47-6 o-Xylene ND 68.2 60.5 89 68.6 61.1 89 1 80-132/30
CAS No.Surrogate Recoveries MS MSD FA55659-2 Limits
1868-53-7 Dibromofluoromethane 99%99%105%75-124%
17060-07-0 1,2-Dichloroethane-D4 104%102%109%72-135%
2037-26-5 Toluene-D8 99%102%105%75-126%
460-00-4 4-Bromofluorobenzene 98%98%108%71-133%
* = Outside of Control Limits.
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SGS LabLink@15:38 17-Jul-2018
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
 Method Blank Summaries
 Blank Spike Summaries
 Matrix Spike and Duplicate Summaries
Orlando, FL
Section 7
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Method Blank Summary Page 1 of 3
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP70835-MB X061226.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
The QC reported here applies to the following samples:Method: SW846 8270D
FA55659-1, FA55659-2, FA55659-3, FA55659-4
CAS No.Compound Result RL MDL Units Q
105-60-2 Caprolactam ND 170 27 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 170 19 ug/kg
95-57-8 2-Chlorophenol ND 170 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 170 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 170 44 ug/kg
51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg
95-48-7 2-Methylphenol ND 170 20 ug/kg
3&4-Methylphenol ND 170 27 ug/kg
88-75-5 2-Nitrophenol ND 170 18 ug/kg
100-02-7 4-Nitrophenol ND 830 170 ug/kg
87-86-5 Pentachlorophenol ND 830 170 ug/kg
108-95-2 Phenol ND 170 17 ug/kg
58-90-2 2,3,4,6-Tetrachlorophenol ND 170 20 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 170 27 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 170 19 ug/kg
83-32-9 Acenaphthene ND 170 18 ug/kg
208-96-8 Acenaphthylene ND 170 17 ug/kg
98-86-2 Acetophenone ND 170 17 ug/kg
120-12-7 Anthracene ND 170 19 ug/kg
1912-24-9 Atrazine ND 170 20 ug/kg
100-52-7 Benzaldehyde ND 830 170 ug/kg
56-55-3 Benzo(a)anthracene ND 170 17 ug/kg
50-32-8 Benzo(a)pyrene ND 170 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 170 18 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg
207-08-9 Benzo(k)fluoranthene ND 170 22 ug/kg
92-52-4 1,1'-Biphenyl ND 170 17 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg
85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg
86-74-8 Carbazole ND 170 23 ug/kg
106-47-8 4-Chloroaniline ND 170 42 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 170 19 ug/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 170 21 ug/kg
91-58-7 2-Chloronaphthalene ND 170 17 ug/kg
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Method Blank Summary Page 2 of 3
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP70835-MB X061226.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
The QC reported here applies to the following samples:Method: SW846 8270D
FA55659-1, FA55659-2, FA55659-3, FA55659-4
CAS No.Compound Result RL MDL Units Q
7005-72-3 4-Chlorophenyl phenyl ether ND 170 17 ug/kg
218-01-9 Chrysene ND 170 17 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 170 21 ug/kg
132-64-9 Dibenzofuran ND 170 17 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 170 40 ug/kg
84-66-2 Diethyl Phthalate ND 330 33 ug/kg
131-11-3 Dimethyl Phthalate ND 170 33 ug/kg
117-84-0 Di-n-octyl Phthalate ND 170 33 ug/kg
84-74-2 Di-n-butyl Phthalate ND 330 67 ug/kg
121-14-2 2,4-Dinitrotoluene ND 170 17 ug/kg
606-20-2 2,6-Dinitrotoluene ND 170 21 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg
206-44-0 Fluoranthene ND 170 17 ug/kg
86-73-7 Fluorene ND 170 18 ug/kg
118-74-1 Hexachlorobenzene ND 170 17 ug/kg
87-68-3 Hexachlorobutadiene ND 170 17 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 170 33 ug/kg
67-72-1 Hexachloroethane ND 170 20 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 170 20 ug/kg
78-59-1 Isophorone ND 170 17 ug/kg
91-57-6 2-Methylnaphthalene ND 170 17 ug/kg
91-20-3 Naphthalene ND 170 17 ug/kg
88-74-4 2-Nitroaniline ND 170 39 ug/kg
99-09-2 3-Nitroaniline ND 170 19 ug/kg
100-01-6 4-Nitroaniline ND 170 48 ug/kg
98-95-3 Nitrobenzene ND 170 17 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 170 17 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 170 18 ug/kg
85-01-8 Phenanthrene ND 170 17 ug/kg
129-00-0 Pyrene ND 170 19 ug/kg
95-94-3 1,2,4,5-Tetrachlorobenzene ND 170 17 ug/kg
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 72%40-102%
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Method Blank Summary Page 3 of 3
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP70835-MB X061226.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
The QC reported here applies to the following samples:Method: SW846 8270D
FA55659-1, FA55659-2, FA55659-3, FA55659-4
CAS No.Surrogate Recoveries Limits
4165-62-2 Phenol-d5 72%41-100%
118-79-6 2,4,6-Tribromophenol 86%42-108%
4165-60-0 Nitrobenzene-d5 70%40-105%
321-60-8 2-Fluorobiphenyl 77%43-107%
1718-51-0 Terphenyl-d14 88%45-119%
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Blank Spike Summary Page 1 of 3
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP70835-BS X061225.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
The QC reported here applies to the following samples:Method: SW846 8270D
FA55659-1, FA55659-2, FA55659-3, FA55659-4
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
105-60-2 Caprolactam 1670 1240 74 40-110
59-50-7 4-Chloro-3-methyl Phenol 1670 1230 74 52-108
95-57-8 2-Chlorophenol 1670 1130 68 48-104
120-83-2 2,4-Dichlorophenol 1670 1320 79 51-105
105-67-9 2,4-Dimethylphenol 1670 879 53 43-96
51-28-5 2,4-Dinitrophenol 3330 2340 70 40-119
534-52-1 4,6-Dinitro-o-cresol 3330 2830 85 64-121
95-48-7 2-Methylphenol 1670 1030 62 46-107
3&4-Methylphenol 3330 2110 63 44-111
88-75-5 2-Nitrophenol 1670 1250 75 49-104
100-02-7 4-Nitrophenol 3330 2460 74 56-116
87-86-5 Pentachlorophenol 3330 2860 86 61-114
108-95-2 Phenol 1670 977 59 45-110
58-90-2 2,3,4,6-Tetrachlorophenol 1670 1360 82 61-108
95-95-4 2,4,5-Trichlorophenol 1670 1420 85 58-112
88-06-2 2,4,6-Trichlorophenol 1670 1410 85 56-109
83-32-9 Acenaphthene 1670 1220 73 56-109
208-96-8 Acenaphthylene 1670 1260 76 56-106
98-86-2 Acetophenone 1670 1050 63 48-107
120-12-7 Anthracene 1670 1140 68 61-110
1912-24-9 Atrazine 1670 1280 77 60-112
100-52-7 Benzaldehyde 1670 1210 73 27-123
56-55-3 Benzo(a)anthracene 1670 1280 77 66-111
50-32-8 Benzo(a)pyrene 1670 1300 78 59-104
205-99-2 Benzo(b)fluoranthene 1670 1390 83 67-113
191-24-2 Benzo(g,h,i)perylene 1670 1340 80 67-113
207-08-9 Benzo(k)fluoranthene 1670 1320 79 67-114
92-52-4 1,1'-Biphenyl 1670 1240 74 53-106
101-55-3 4-Bromophenyl phenyl ether 1670 1380 83 62-110
85-68-7 Butyl benzyl phthalate 1670 1300 78 65-113
86-74-8 Carbazole 1670 1380 83 60-111
106-47-8 4-Chloroaniline 1670 1200 72 30-115
111-91-1 bis(2-Chloroethoxy)methane 1670 1060 64 48-105
111-44-4 bis(2-Chloroethyl)ether 1670 996 60 46-103
108-60-1 2,2'-Oxybis(1-chloropropane)1670 934 56 40-110
91-58-7 2-Chloronaphthalene 1670 1210 73 53-106
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 3
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP70835-BS X061225.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
The QC reported here applies to the following samples:Method: SW846 8270D
FA55659-1, FA55659-2, FA55659-3, FA55659-4
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
7005-72-3 4-Chlorophenyl phenyl ether 1670 1300 78 58-106
218-01-9 Chrysene 1670 1300 78 65-112
53-70-3 Dibenzo(a,h)anthracene 1670 1390 83 68-115
132-64-9 Dibenzofuran 1670 1330 80 57-108
84-66-2 Diethyl Phthalate 1670 1280 77 61-109
131-11-3 Dimethyl Phthalate 1670 1270 76 59-108
117-84-0 Di-n-octyl Phthalate 1670 1430 86 64-119
84-74-2 Di-n-butyl Phthalate 1670 1300 78 63-108
121-14-2 2,4-Dinitrotoluene 1670 1280 77 59-109
606-20-2 2,6-Dinitrotoluene 1670 1240 74 61-107
117-81-7 bis(2-Ethylhexyl)phthalate 1670 1340 80 64-115
206-44-0 Fluoranthene 1670 1330 80 60-108
86-73-7 Fluorene 1670 1290 77 58-109
118-74-1 Hexachlorobenzene 1670 1360 82 59-111
87-68-3 Hexachlorobutadiene 1670 1270 76 41-108
77-47-4 Hexachlorocyclopentadiene 1670 1260 76 49-110
67-72-1 Hexachloroethane 1670 1010 61 40-105
193-39-5 Indeno(1,2,3-cd)pyrene 1670 1430 86 66-116
78-59-1 Isophorone 1670 1040 62 42-89
91-57-6 2-Methylnaphthalene 1670 1280 77 47-106
91-20-3 Naphthalene 1670 1130 68 44-104
88-74-4 2-Nitroaniline 1670 1250 75 56-123
99-09-2 3-Nitroaniline 1670 1260 76 41-111
100-01-6 4-Nitroaniline 1670 1250 75 54-113
98-95-3 Nitrobenzene 1670 1050 63 43-108
621-64-7 N-Nitrosodi-n-propylamine 1670 979 59 48-108
86-30-6 N-Nitrosodiphenylamine 1670 1230 74 62-110
85-01-8 Phenanthrene 1670 1280 77 63-111
129-00-0 Pyrene 1670 1340 80 65-115
95-94-3 1,2,4,5-Tetrachlorobenzene 1670 1220 73 46-101
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 65%40-102%
4165-62-2 Phenol-d5 64%41-100%
* = Outside of Control Limits.
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Blank Spike Summary Page 3 of 3
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP70835-BS X061225.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
The QC reported here applies to the following samples:Method: SW846 8270D
FA55659-1, FA55659-2, FA55659-3, FA55659-4
CAS No.Surrogate Recoveries BSP Limits
118-79-6 2,4,6-Tribromophenol 80%42-108%
4165-60-0 Nitrobenzene-d5 64%40-105%
321-60-8 2-Fluorobiphenyl 69%43-107%
1718-51-0 Terphenyl-d14 79%45-119%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP70835-MS X061229.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
OP70835-MSD X061230.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
FA55659-1 X061247.D 1 07/12/18 MV 07/11/18 OP70835 SX2551
The QC reported here applies to the following samples:Method: SW846 8270D
FA55659-1, FA55659-2, FA55659-3, FA55659-4
FA55659-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
105-60-2 Caprolactam ND 1990 1540 78 1990 1570 79 2 40-110/22
59-50-7 4-Chloro-3-methyl Phenol ND 1990 1520 77 1990 1610 81 6 52-108/21
95-57-8 2-Chlorophenol ND 1990 1380 69 1990 1470 74 6 48-104/26
120-83-2 2,4-Dichlorophenol ND 1990 1630 82 1990 1730 87 6 51-105/27
105-67-9 2,4-Dimethylphenol ND 1990 1120 56 1990 1180 59 5 43-96/23
51-28-5 2,4-Dinitrophenol ND 3970 2520 63 3970 2790 70 10 40-119/32
534-52-1 4,6-Dinitro-o-cresol ND 3970 3290 83 3970 3460 87 5 64-121/29
95-48-7 2-Methylphenol ND 1990 1280 64 1990 1350 68 5 46-107/24
3&4-Methylphenol ND 3970 2640 66 3970 2770 70 5 44-111/24
88-75-5 2-Nitrophenol ND 1990 1560 79 1990 1630 82 4 49-104/27
100-02-7 4-Nitrophenol ND 3970 3140 79 3970 3280 83 4 56-116/23
87-86-5 Pentachlorophenol ND 3970 3680 93 3970 3790 95 3 61-114/23
108-95-2 Phenol ND 1990 1190 60 1990 1260 63 6 45-110/24
58-90-2 2,3,4,6-Tetrachlorophenol ND 1990 1730 87 1990 1820 92 5 61-108/21
95-95-4 2,4,5-Trichlorophenol ND 1990 1770 89 1990 1840 93 4 58-112/22
88-06-2 2,4,6-Trichlorophenol ND 1990 1790 90 1990 1890 95 5 56-109/25
83-32-9 Acenaphthene ND 1990 1530 77 1990 1620 82 6 56-109/23
208-96-8 Acenaphthylene ND 1990 1600 81 1990 1660 84 4 56-106/23
98-86-2 Acetophenone ND 1990 1290 65 1990 1370 69 6 48-107/27
120-12-7 Anthracene ND 1990 1470 74 1990 1520 77 3 61-110/21
1912-24-9 Atrazine ND 1990 1650 83 1990 1730 87 5 60-112/21
100-52-7 Benzaldehyde ND 1990 1460 73 1990 1520 77 4 27-123/30
56-55-3 Benzo(a)anthracene ND 1990 1660 84 1990 1720 87 4 66-111/23
50-32-8 Benzo(a)pyrene ND 1990 1670 84 1990 1740 88 4 59-104/23
205-99-2 Benzo(b)fluoranthene ND 1990 1820 92 1990 1880 95 3 67-113/24
191-24-2 Benzo(g,h,i)perylene ND 1990 1810 91 1990 1850 93 2 67-113/21
207-08-9 Benzo(k)fluoranthene ND 1990 1650 83 1990 1760 89 6 67-114/22
92-52-4 1,1'-Biphenyl ND 1990 1530 77 1990 1620 82 6 53-106/24
101-55-3 4-Bromophenyl phenyl ether ND 1990 1780 90 1990 1860 94 4 62-110/21
85-68-7 Butyl benzyl phthalate ND 1990 1720 87 1990 1810 91 5 65-113/20
86-74-8 Carbazole ND 1990 1760 89 1990 1860 94 6 60-111/19
106-47-8 4-Chloroaniline ND 1990 1480 75 1990 1580 80 7 30-115/30
111-91-1 bis(2-Chloroethoxy)methane ND 1990 1310 66 1990 1380 69 5 48-105/24
111-44-4 bis(2-Chloroethyl)ether ND 1990 1250 63 1990 1300 65 4 46-103/27
108-60-1 2,2'-Oxybis(1-chloropropane)ND 1990 1180 59 1990 1230 62 4 40-110/25
91-58-7 2-Chloronaphthalene ND 1990 1510 76 1990 1610 81 6 53-106/23
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP70835-MS X061229.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
OP70835-MSD X061230.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
FA55659-1 X061247.D 1 07/12/18 MV 07/11/18 OP70835 SX2551
The QC reported here applies to the following samples:Method: SW846 8270D
FA55659-1, FA55659-2, FA55659-3, FA55659-4
FA55659-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
7005-72-3 4-Chlorophenyl phenyl ether ND 1990 1620 82 1990 1700 86 5 58-106/21
218-01-9 Chrysene ND 1990 1670 84 1990 1730 87 4 65-112/25
53-70-3 Dibenzo(a,h)anthracene ND 1990 1850 93 1990 1910 96 3 68-115/23
132-64-9 Dibenzofuran ND 1990 1650 83 1990 1750 88 6 57-108/22
84-66-2 Diethyl Phthalate ND 1990 1610 81 1990 1700 86 5 61-109/20
131-11-3 Dimethyl Phthalate ND 1990 1620 82 1990 1680 85 4 59-108/20
117-84-0 Di-n-octyl Phthalate ND 1990 1890 95 1990 2020 102 7 64-119/21
84-74-2 Di-n-butyl Phthalate ND 1990 1660 84 1990 1730 87 4 63-108/19
121-14-2 2,4-Dinitrotoluene ND 1990 1600 81 1990 1660 84 4 59-109/20
606-20-2 2,6-Dinitrotoluene ND 1990 1560 79 1990 1650 83 6 61-107/22
117-81-7 bis(2-Ethylhexyl)phthalate ND 1990 1750 88 1990 1850 93 6 64-115/23
206-44-0 Fluoranthene ND 1990 1670 84 1990 1730 87 4 60-108/25
86-73-7 Fluorene ND 1990 1610 81 1990 1690 85 5 58-109/21
118-74-1 Hexachlorobenzene ND 1990 1740 88 1990 1780 90 2 59-111/21
87-68-3 Hexachlorobutadiene ND 1990 1570 79 1990 1650 83 5 41-108/27
77-47-4 Hexachlorocyclopentadiene ND 1990 1430 72 1990 1560 79 9 49-110/31
67-72-1 Hexachloroethane ND 1990 1230 62 1990 1280 64 4 40-105/32
193-39-5 Indeno(1,2,3-cd)pyrene ND 1990 1880 95 1990 2000 101 6 66-116/22
78-59-1 Isophorone ND 1990 1310 66 1990 1390 70 6 42-89/22
91-57-6 2-Methylnaphthalene ND 1990 1570 79 1990 1660 84 6 47-106/27
91-20-3 Naphthalene ND 1990 1370 69 1990 1450 73 6 44-104/27
88-74-4 2-Nitroaniline ND 1990 1560 79 1990 1680 85 7 56-123/24
99-09-2 3-Nitroaniline ND 1990 1630 82 1990 1700 86 4 41-111/25
100-01-6 4-Nitroaniline ND 1990 1620 82 1990 1720 87 6 54-113/22
98-95-3 Nitrobenzene ND 1990 1300 65 1990 1370 69 5 43-108/25
621-64-7 N-Nitrosodi-n-propylamine ND 1990 1240 62 1990 1290 65 4 48-108/27
86-30-6 N-Nitrosodiphenylamine ND 1990 1630 82 1990 1690 85 4 62-110/21
85-01-8 Phenanthrene ND 1990 1650 83 1990 1700 86 3 63-111/22
129-00-0 Pyrene ND 1990 1810 91 1990 1890 95 4 65-115/25
95-94-3 1,2,4,5-Tetrachlorobenzene ND 1990 1490 75 1990 1590 80 6 46-101/24
CAS No.Surrogate Recoveries MS MSD FA55659-1 Limits
367-12-4 2-Fluorophenol 67%71%69%40-102%
4165-62-2 Phenol-d5 67%71%69%41-100%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA55659
Account:URSNCM AECOM, INC.
Project:Forest City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP70835-MS X061229.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
OP70835-MSD X061230.D 1 07/11/18 MV 07/11/18 OP70835 SX2550
FA55659-1 X061247.D 1 07/12/18 MV 07/11/18 OP70835 SX2551
The QC reported here applies to the following samples:Method: SW846 8270D
FA55659-1, FA55659-2, FA55659-3, FA55659-4
CAS No.Surrogate Recoveries MS MSD FA55659-1 Limits
118-79-6 2,4,6-Tribromophenol 88%92%86%42-108%
4165-60-0 Nitrobenzene-d5 65%70%66%40-105%
321-60-8 2-Fluorobiphenyl 73%79%73%43-107%
1718-51-0 Terphenyl-d14 88%93%87%45-119%
* = Outside of Control Limits.
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SGS LabLink@15:38 17-Jul-2018
Metals Analysis
QC Data Summaries
Includes the following where applicable:
 Method Blank Summaries
 Matrix Spike and Duplicate Summaries
 Blank Spike and Lab Control Sample Summaries
 Serial Dilution Summaries
Orlando, FL
Section 8
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BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA55659
Account: URSNCM - AECOM, INC.
Project: Forest City, NC
QC Batch ID: MP34003 Methods: SW846 6010D
Matrix Type: SOLID Units: mg/kg
Prep Date: 07/11/18
MB
Metal RL IDL MDL raw final
Aluminum 10 .7 1.8
Antimony 1.0 .05 .065
Arsenic 0.50 .065 .1 -0.040 <0.50
Barium 10 .05 .05 0.15 <10
Beryllium 0.25 .01 .025
Cadmium 0.20 .01 .025 -0.0030 <0.20
Calcium 250 2.5 2.5
Chromium 0.50 .05 .05 0.035 <0.50
Cobalt 2.5 .01 .025
Copper 1.3 .05 .05
Iron 15 .85 .85
Lead 1.0 .05 .05 -0.030 <1.0
Magnesium 250 1.8 1.8
Manganese 0.75 .025 .025
Molybdenum 2.5 .015 .025
Nickel 2.0 .02 .025
Potassium 500 10 10
Selenium 1.0 .12 .12 -0.0050 <1.0
Silver 0.50 .035 .041 -0.015 <0.50
Sodium 500 25 25
Strontium 0.50 .025 .025
Thallium 0.50 .055 .055
Tin 2.5 .045 .045
Titanium 0.50 .025 .025
Vanadium 2.5 .025 .025
Zinc 1.0 .15 .15
Associated samples MP34003: FA55659-1, FA55659-2, FA55659-3, FA55659-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55659
Account: URSNCM - AECOM, INC.
Project: Forest City, NC
QC Batch ID: MP34003 Methods: SW846 6010D
Matrix Type: SOLID Units: mg/kg
Prep Date: 07/11/18 07/11/18
FA55659-1 QC FA55659-1 Spikelot QC
Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 6.5 7.6 (a) 15.6 0-20 6.5 91.2 (a) 115 73.9N(c) 80-120
Barium 161 173 (a) 7.2 0-20 161 277 (a) 115 101.2 80-120
Beryllium
Cadmium 0.0 0.0 (a) NC 0-20 0.0 1.8 (a) 2.87 62.8N(c) 80-120
Calcium
Chromium 58.1 93.6 (a) 46.8*(b) 0-20 58.1 72.3 (a) 11.5 123.9(d) 80-120
Cobalt
Copper
Iron
Lead 25.6 23.2 (a) 9.8 0-20 25.6 50.1 (a) 28.7 85.5 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 0.0 0.0 (a) NC 0-20 0.0 85.3 (a) 115 74.4N(c) 80-120
Silver 0.0 0.0 (a) NC 0-20 0.0 2.0 (a) 2.87 69.8N(c) 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP34003: FA55659-1, FA55659-2, FA55659-3, FA55659-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) Sample dilution required due to difficult matrix.
(b) High RPD due to possible sample non-homogeneity.
(c) Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
(d) Spike amount low relative to the sample amount. Refer to lab control or spike blank for recovery
information.
_________________________________________________________________________________________________________
Page 1
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55659
Account: URSNCM - AECOM, INC.
Project: Forest City, NC
QC Batch ID: MP34003 Methods: SW846 6010D
Matrix Type: SOLID Units: mg/kg
Prep Date: 07/11/18
FA55659-1 Spikelot MSD QC
Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum
Antimony
Arsenic 6.5 90.5 (a) 114 74.0N(b) 0.8 20
Barium 161 288 (a) 114 111.9 3.9 20
Beryllium
Cadmium 0.0 1.7 (a) 2.84 59.9N(b) 5.7 20
Calcium
Chromium 58.1 73.7 (a) 11.4 137.4(c) 1.9 20
Cobalt
Copper
Iron
Lead 25.6 51.6 (a) 28.4 91.6 2.9 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 0.0 85.2 (a) 114 75.1N(b) 0.1 20
Silver 0.0 2.2 (a) 2.84 77.5N(b) 9.5 20
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP34003: FA55659-1, FA55659-2, FA55659-3, FA55659-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) Sample dilution required due to difficult matrix.
(b) Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
(c) Spike amount low relative to the sample amount. Refer to lab control or spike blank for recovery
information.
_________________________________________________________________________________________________________
Page 2
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SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA55659
Account: URSNCM - AECOM, INC.
Project: Forest City, NC
QC Batch ID: MP34003 Methods: SW846 6010D
Matrix Type: SOLID Units: mg/kg
Prep Date: 07/11/18
BSP Spikelot QC
Metal Result MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 98.2 100 98.2 80-120
Barium 104 100 104.0 80-120
Beryllium
Cadmium 2.6 2.5 104.0 80-120
Calcium
Chromium 10.4 10 104.0 80-120
Cobalt
Copper
Iron
Lead 23.6 25 94.4 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 97.5 100 97.5 80-120
Silver 2.5 2.5 100.0 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP34003: FA55659-1, FA55659-2, FA55659-3, FA55659-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
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SERIAL DILUTION RESULTS SUMMARY
Login Number: FA55659
Account: URSNCM - AECOM, INC.
Project: Forest City, NC
QC Batch ID: MP34003 Methods: SW846 6010D
Matrix Type: SOLID Units: ug/l
Prep Date: 07/11/18
FA55659-1 QC
Metal Original SDL 10:50%DIF Limits
Aluminum
Antimony
Arsenic 156 214 37.5 (a) 0-10
Barium 3900 4600 18.1*(b) 0-10
Beryllium
Cadmium 0.00 0.00 NC 0-10
Calcium
Chromium 1410 1670 19.0*(b) 0-10
Cobalt
Copper
Iron
Lead 618 528 14.7*(b) 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 0.00 0.00 NC 0-10
Silver 0.00 0.00 NC 0-10
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP34003: FA55659-1, FA55659-2, FA55659-3, FA55659-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
(b) Serial dilution indicates possible matrix interference.
_________________________________________________________________________________________________________
Page 1
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BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA55659
Account: URSNCM - AECOM, INC.
Project: Forest City, NC
QC Batch ID: MP34022 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 07/16/18
MB
Metal RL IDL MDL raw final
Mercury 0.042 .0025 .0042 -0.0015 <0.042
Associated samples MP34022: FA55659-1, FA55659-2, FA55659-3, FA55659-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55659
Account: URSNCM - AECOM, INC.
Project: Forest City, NC
QC Batch ID: MP34022 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 07/16/18 07/16/18
FA55684-1 QC FA55684-1 Spikelot QC
Metal Original DUP RPD Limits Original MS HGFLWS1 % Rec Limits
Mercury 0.0038 0.0077 67.8 (a) 0-20 0.0038 0.28 0.259 106.5 80-120
Associated samples MP34022: FA55659-1, FA55659-2, FA55659-3, FA55659-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) RPD acceptable due to low duplicate and sample concentrations.
_________________________________________________________________________________________________________
Page 1
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55659
Account: URSNCM - AECOM, INC.
Project: Forest City, NC
QC Batch ID: MP34022 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 07/16/18
FA55684-1 Spikelot MSD QC
Metal Original MSD HGFLWS1 % Rec RPD Limit
Mercury 0.0038 0.29 0.264 108.6 3.5 20
Associated samples MP34022: FA55659-1, FA55659-2, FA55659-3, FA55659-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
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SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA55659
Account: URSNCM - AECOM, INC.
Project: Forest City, NC
QC Batch ID: MP34022 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 07/16/18
BSP Spikelot QC
Metal Result HGFLWS1 % Rec Limits
Mercury 0.27 0.25 108.0 80-120
Associated samples MP34022: FA55659-1, FA55659-2, FA55659-3, FA55659-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
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SERIAL DILUTION RESULTS SUMMARY
Login Number: FA55659
Account: URSNCM - AECOM, INC.
Project: Forest City, NC
QC Batch ID: MP34022 Methods: SW846 7471B
Matrix Type: SOLID Units: ug/l
Prep Date: 07/16/18
FA55684-1 QC
Metal Original SDL 1:5 %DIF Limits
Mercury 0.0448 0.00 100.0(a) 0-10
Associated samples MP34022: FA55659-1, FA55659-2, FA55659-3, FA55659-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
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SGS LabLink@15:38 17-Jul-2018
Misc. Forms
Custody Documents and Other Forms
(SGS Dayton, NJ)
Includes the following where applicable:
 Chain of Custody
 Analyst Legend
Orlando, FL
Section 9
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9 CHAIN OF CUSTODY Page 1 of 1
SGS FED-EX Tracking # Bottle Order Control #
! 4405 Vineland Rd, Suite C-IS, Orlando, FL 3281 I SGS Quote # SGS Job# FA55659TEL. [phone] FAX [phone]
Client I Reporting Information Project Information Requested !\nalysisj see~T,CODE sheet) Matrix Codes
Comp.a.ny~ rr·::.]e-:.t Na((~e. -
8G8 North America Inc. Forest City, NC DW -Drinking Water
GW -Ground Water Street Address Street WW-Water
4405 Vineland Rd, 8uite C-15 &IV -Surface Water
Billing Information ( if different from Report to) SO Soil City State Zip City State Company Name SL-Sludge
Orlando FL 32811 SED-Sediment
ai-Oil Project Contact E-mail Project # Street Address UQ -Other Liquid
[e-mail] AIR-Air
Phone # Fax # Client Purohase Order # City SOL -Other Solid State Zip WP-Wipe
407 -425-6700 FB-Field Blank
Sampler!s) Name!s) Phone Project Manager Attention' EB-Equipment Blank
RB-Rinse Blank EL TB-Trip Blank
Collection Number of preserved Bottles
OJ <i(5 OJ J: 0::
5GS Sampled J: 8 0 0::.
#ofbottles ~ 0 C/) z 0 u U Sample' Field ID 1Point of Collection MEOHIDI Vial # Date TIme by Matrix ., z ~ 0 w z X LAB USE ONLY z J: Z ::; OJ
1 88-1 7/9/18 2:40:00 PM EL SO X
2 88-2 7/9/18 3:00:00 PM EL SO X
3 88-3 7/9/18 3:15:00 PM EL SO X ~.
4 88-4 7/9/18 3:30:00 PM EL SO X
--­
~
/01
f -.,,'"-...,......­
Turnaround Time ( Business days) Data Deliverable Information Comments f Special Instructions
Approved By (SOS PM): I Date: D Commercial "A" (Level 1, Results Only) SGS-Dayton o 10 Day (business) o Commercial "B" ( Level 2, Results + QC summary) Please portion out a 20z jar to sub to NJ o 5-7Day D REDT1 (Level 3) o 3 Day RUSH D FULT1 (Level 4) o 2DayRUsH II DOD FULT1 (Level 4) X (';l iNITIAL ASESSMENT_~1)&/11o 1 Day RUSH rn Other COMMBN
I]J other Due 7116/2018 D EDD Format ERPIMs LABEL VE::tlFJCATION -
Rush T/A data available VIA Lablink
A Sample Custody must be documented below each time samples change possession, including courier delivery. -,./
1[j{AA1~/ D~:T~I¥ \lt~c£ Received By: <hr'. Relinquished By: ~ ~j~)ji 1;"0 Receive~~
1 2 2 ~
~u;;edby Sampler: D Date Time: Relinquished By: ... Date Time: .:!"'" -Received By: Received By:
3 3 4 4 ) Relinquished by: Date Time: Received By: Custody Seal # o Intact Preserved where applicable ~ Cooler Temp. d-7j~5 5 0 Not intact 0 ~

FA55659: Chain of Custody
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SGS Dayton, NJ
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Job Number:FA55659 Client:
Date / Time Received:7/12/2018 9:30:00 AM Delivery Method:
Project:
4. No. Coolers:1
Airbill #'s:
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Cooler temp verification:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
IR Gun
Ice (Bag)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (2.9);
Cooler 1: (2.9);
SM089-03Rev. Date 12/7/17
SGS Sample Receipt Summary
Test Strip Lot #s:pH 1-12:216017 pH 12+:208717 Other: (Specify)
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Analyst Legend Page 1 of 1
Job Number:FA55659
Account:ALSE SGS Orlando, FL
Project:URSNCM: Forest City, NC
Initials Full Name Analysis Type
DC Deepthi Chappidi General Chemistry
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SGS LabLink@15:38 17-Jul-2018
General Chemistry
QC Data Summaries
(SGS Dayton, NJ)
Includes the following where applicable:
 Method Blank and Blank Spike Summaries
 Duplicate Summaries
 Matrix Spike Summaries
Orlando, FL
Section 10
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METHOD BLANK AND SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA55659
Account: ALSE - SGS Orlando, FL
Project: URSNCM: Forest City, NC
MB Spike BSP BSP QC
Analyte Batch ID RL Result Units Amount Result %Recov Limits
Chromium, Hexavalent GP14493/GN82858 0.40 0.0 mg/kg 1106.931 1030 93.1 80-120%
Chromium, Hexavalent GP14493/GN82858 mg/kg 40 39.7 99.3 80-120%
Associated Samples:
Batch GP14493: FA55659-1, FA55659-2, FA55659-3, FA55659-4
(*) Outside of QC limits
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DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA55659
Account: ALSE - SGS Orlando, FL
Project: URSNCM: Forest City, NC
QC Original DUP QC
Analyte Batch ID Sample Units Result Result RPD Limits
Chromium, Hexavalent GP14493/GN82858 FA55659-1 mg/kg 0.84 0.81 3.6 0-20%
Associated Samples:
Batch GP14493: FA55659-1, FA55659-2, FA55659-3, FA55659-4
(*) Outside of QC limits
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MATRIX SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA55659
Account: ALSE - SGS Orlando, FL
Project: URSNCM: Forest City, NC
QC Original Spike MS QC
Analyte Batch ID Sample Units Result Amount Result %Rec Limits
Chromium, Hexavalent GP14493/GN82858 FA55659-1 mg/kg 0.84 1490 1540 103.0(a) 75-125%
Chromium, Hexavalent GP14493/GN82858 FA55659-1 mg/kg 0.84 47.5 34.2 70.3N(b) 75-125%
Associated Samples:
Batch GP14493: FA55659-1, FA55659-2, FA55659-3, FA55659-4
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(a) Good recovery on insoluble XCR matrix spike. See additional comments on soluble matrix spike recovery.
(b) Soluble XCR matrix spike recovery indicates possible matrix interference. Good post spike recovery (105%) on this
sample.
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