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HomeMy WebLinkAbout25046_Harrelson Ford Supplemental Soil Excavation Completion Report_20240301Hanley Environmental, PLLC 323 Manning Drive Charlotte, North Carolina 28209 NC Engineering License P-2407 T: (704) 317-6970 www.hanleyenvironmental.com March 1, 2024 Bill Schmithorst, PG North Carolina Department of Environmental Quality Division of Waste Management – Brownfields Redevelopment Section 1646 Mail Service Center Raleigh, North Carolina 27699 Subject: Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 6500 South Boulevard Charlotte, North Carolina Brownfields Project Number: 25046-21-060 Hanley Environmental Project Number: PJ23030 Dear Bill Schmithorst: Hanley Environmental, PLLC is pleased to provide the enclosed Supplemental Soil Excavation Completion Report for the Harrelson Ford Brownfields Property located at 6500 South Boulevard in Charlotte, Mecklenburg County, North Carolina on behalf of Tri Pointe Homes Holdings, LLC. This Report has been prepared pursuant to the Soil Excavation and Post- Excavation Sampling Work Plan dated August 23, 2023. Please do not hesitate to contact the undersigned with any questions regarding this submittal. Sincerely, Joe Gentilcore David Hanley, PE Environmental Scientist Principal Engineer Cc: Sean Schuttler, Tri Pointe Homes Holdings, LLC Mary Katherine H. Stukes, Moore & Van Allen, PLLC Hanley Environmental, PLLC 323 Manning Drive Charlotte, North Carolina 28209 NC Engineering License P-2407 T: (704) 317-6970 www.hanleyenvironmental.com SUPPLEMENTAL SOIL EXCAVATION COMPLETION REPORT Harrelson Ford Brownfields Property 6500 South Boulevard Charlotte, North Carolina Brownfields Project Number: 25046-21-060 Hanley Environmental Project Number: PJ23030 March 1, 2024 Prepared for: Tri Pointe Homes Holdings, Inc. Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property i TABLE OF CONTENTS TABLE OF CONTENTS i 1.0 INTRODUCTION 1 1.1 Site Description and Redevelopment Activities 2 1.2 Previous Soil Excavation Activities 2 2.0 SOIL EXCAVATION ACTIVITIES 3 2.1 Excavation Procedures 3 2.2 Confirmation Soil Sampling Procedures 4 2.3 Confirmation Soil Sampling Results 5 3.0 SOIL GAS SAMPLING ACTIVITIES 5 3.1 Soil Gas Sampling Procedures 6 3.2 Soil Gas Sampling Results 7 3.3 Risk Calculations 8 4.0 QUALITY ASSURANCE/QUALITY CONTROL 9 5.0 CONCLUSIONS AND RECOMMENDATIONS 9 6.0 REFERENCES 12 List of Tables Table 1 Soil PID Response Summary Table 2 Confirmation Soil Analytical Results Summary Table 3 Post-Excavation Soil Gas Analytical Results Summary List of Figures Figure 1 Site Vicinity Map Figure 2 Site Map Figure 3 Excavation Area and Confirmation Soil Sample Location Map Figure 4 Post-Excavation Soil Gas Sample Locations Overlaying Redevelopment Plans Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property ii List of Appendices Appendix A Historical Data Summary Excerpts Appendix B Disposal Documentation Appendix C Laboratory Analytical Reports Appendix D Soil Boring Logs Appendix E Field Sampling Forms Appendix F Risk Calculator Outputs Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 1 1.0 INTRODUCTION This Supplemental Soil Excavation Completion Report presents methods and results of the supplemental soil over excavation and post-excavation soil gas sampling activities completed in December 2023 and January 2024 at the Harrelson Ford Brownfields Property located at 6500 South Boulevard in Charlotte, Mecklenburg County, North Carolina (the site). The site is undergoing redevelopment under the North Carolina Department of Environmental Quality (NCDEQ) Brownfields Redevelopment Section (BRS) (Brownfields Project No. 25046- 21-060). Current redevelopment plans for the site include construction of 165 residential townhomes and associated amenities. A Notice of Brownfields Property was filed on October 13, 2023, that included a Brownfields Agreement for the site. Land Use Restriction 12.b.(i) generally indicates that soil impacted with chlorinated solvent compounds at concentrations above NCDEQ Protection of Groundwater Preliminary Soil Remediation Goals (PSRGs) as identified in the Soil Excavation Completion Report prepared by Hart & Hickman, P.C., dated March 30, 2023, must be excavated prior to construction of townhomes at the site. Land Use Restriction 12.b.(ii) requires confirmation soil gas sampling at the areas of excavation with analytical results meeting residential risk criteria and with no trichloroethylene (TCE) detected above the Residential NCDEQ Vapor Intrusion Screening Level or other suitable level approved in advance of construction by NCDEQ. In a letter from the NCDEQ BRS dated August 25, 2023, (Re: Redevelopment Status) approval was given to proceed with townhome redevelopment in portions of the site not located within the areas of excavation. Previous soil excavation activities performed at the site were summarized in the Soil Excavation Completion Report (Completion Report) prepared by Hart & Hickman, P.C., dated March 30, 2023, and included removal of impacted soil from accessible areas of concern beneath two site buildings. Additional details of the previous excavation activities are discussed further in Section 1.2. A Soil Excavation and Post-Excavation Sampling Work Plan (Work Plan) was prepared by Hart & Hickman, P.C., dated October 6, 2023, presenting Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 2 procedures to remove limited volumes of soil that could not be removed below structural components within buildings during previous excavation activities, and to collect post- excavation soil gas samples to meet the requirements of Land Use Restrictions 12.b.(i) and 12.b.(ii). The Work Plan was approved by NCDEQ on October 9, 2023. Soil over excavation and post-excavation sampling activities were completed by Hanley Environmental, or under their supervision, on behalf of the current property owner, Tri Pointe Homes Holdings, Inc., and this report presents documentation of site activities, results, conclusions, and recommendations. 1.1 Site Description and Redevelopment Activities The site consists of one parcel (Parcel ID 17304204) with a total area of approximately 10.58 acres. A map depicting the site vicinity is included as Figure 1, and a site map is provided as Figure 2. Tri Pointe Homes Holdings, Inc. acquired the property on October 16, 2023. Demolition of site buildings was completed in October and November 2023, and site work/mass grading associated with the planned townhome redevelopment is ongoing pursuant to the Environmental Management Plan (EMP) dated October 20, 2023. 1.2 Previous Soil Excavation Activities Previous soil excavation activities at the site, which were performed on behalf of a prior owner, are summarized in the Soil Excavation Completion Report (Completion Report) dated March 30, 2023. Data summary excerpts from the Completion Report are included in Appendix A. Previous excavation activities were performed in accordance with the Soil Excavation Work Plan prepared by Hart & Hickman, P.C., dated November 22, 2022, and an EMP dated November 4, 2022. Previous soil excavation activities were conducted from January 2023 through March 2023 as a strategy to remove soil impacted with chlorinated solvents beneath two former building slabs. Soil excavation was performed in five areas of concern and resulted in approximately 1,736 tons of impacted soil removed and disposed of at the Republic Services Municipal Solid Waste landfill in Concord, North Carolina. The results of post-excavation confirmation soil Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 3 sample analyses indicated that chlorinated solvent-impacted soil beneath former auto service areas within the former Building 3 and Building 4 had been removed to unrestricted use levels for protection of human health. Trace levels of PCE and TCE were present in several discrete areas near load-bearing walls of Building 3 and Building 4 in soil that could not be easily excavated while maintaining structural integrity of the buildings. 2.0 SOIL EXCAVATION ACTIVITIES Pursuant to the Work Plan, residual contaminated soil beneath Building 3 and Building 4 was excavated following demolition of the buildings. The following sections provide information on excavation procedures, confirmation soil sampling procedures, sampling locations, and results. A map depicting excavation areas and soil sample locations is included as Figure 3. Procedures for excavation and sample collection generally followed the procedures described in the Work Plan. 2.1 Excavation Procedures On December 13, 2023, Hanley Environmental provided oversight of soil excavation activities completed by Paragon Site Solutions, LLC of Charlotte, North Carolina (Paragon). Over excavation areas were surveyed and staked in advance by Paragon using coordinates obtained from CAD files of the excavation areas provided by Hart & Hickman, PC. Over excavation was completed at the five over excavation areas depicted on Figure 3. Excavated soil was field screened using a calibrated photoionization detector (PID). The excavation areas initially extended horizontally to the surveyed boundaries, and were expanded further if necessary until field screening results indicated a low likelihood of impacts. Excavation depths ranged from approximately 9.0 feet below ground surface (ft bgs) to 10.6 ft bgs. The approximate depth to the groundwater capillary fringe in this portion of the site was reported in the Work Plan to be 9 ft bgs. The over excavation areas extended to the approximate depth of the water table capillary fringe, but did not extend into the water table, and groundwater was not encountered in excavations. Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 4 The final extents of over excavation areas are shown on Figure 3 and final excavation dimensions are summarized in the table below. Over Excavation Area Length (ft) Width (ft) Depth (ft) B 12.3 11.2 10.6 D 7.5 13.2 9.7 E1 7.3 10.2 9.5 E2 10.7 6.7 9.0 E3 13 8.2 9.0 Approximately 192 cubic yards (CY) of soil was direct-loaded into trucks and transported to the Republic Services Municipal Solid Waste Landfill located in Concord, North Carolina for disposal. Soil disposal documentation provided by Paragon is included in Appendix B. 2.2 Confirmation Soil Sampling Procedures Following soil excavation, soil sample aliquots from each excavation sidewall were collected directly from the excavator bucket, taking care not to sample soil in contact with the bucket. In accordance with the Work Plan, samples were not collected from the excavation bases because excavation depths were not shallower than 9 ft. One soil sample aliquot was collected at a frequency of every 10 linear feet from each excavation sidewall from the 0-3 ft bgs, 3-6 ft bgs, and 6-9 ft bgs depth intervals and field screened using a calibrated PID. The aliquot with the highest potential for impact based on field screening from each sidewall was selected for laboratory analysis. If soil sample aliquot PID responses did not indicate likely impacts, the 3-6 ft bgs depth interval was selected for laboratory analysis. A summary of confirmation PID response measurements is included in Table 1. The final excavation extents resulted in a total of 21 confirmation soil samples collected for laboratory analysis. The locations of the confirmation soil samples are shown in Figure 3. For quality assurance/quality control (QA/QC) purposes, one duplicate soil sample was Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 5 collected from the OEX-E3(C)-2 confirmation soil sample location. Soil samples were labeled with sample identification, date, and requested analysis, and placed in a cooler with ice. The samples were delivered to Waypoint Analytical, Inc. (Waypoint) of Charlotte, North Carolina, a North Carolina certified laboratory, under standard chain of custody protocol for analysis of PCE and TCE by EPA Method 8260. Confirmation soil sample locations were recorded using a hand-held global positioning system (GPS) unit. Following sample collection, the excavation basins were backfilled with compacted clean fill material imported from Vulcan Materials Company located at 10526 Old Nations Ford Road in Charlotte, North Carolina and/or cut soil from other parts of the site. 2.3 Confirmation Soil Sampling Results Confirmation soil sample analytical results were compared to the NCDEQ Protection of Groundwater PSRGs dated February 2024 and are summarized in Table 2. The laboratory analytical report and chain-of-custody record is included in Appendix C. Laboratory results indicate the presence of PCE in confirmation soil sample OEX-E2(C) (3-6 ft bgs) at an estimated “J-flag” value of 0.003 J milligrams per kilogram (mg/kg), which is below the Protection of Groundwater PSRG for PCE of 0.0063 mg/kg. Neither PCE nor TCE were detected in the other confirmation soil samples at a concentration above the laboratory method detection limits. The results of confirmation soil sampling demonstrated that PCE and TCE were not present at concentrations above the Protection of Groundwater PSRG and the requirements of Land Use Restriction 12.b.(i) related to townhome redevelopment have been satisfied. 3.0 SOIL GAS SAMPLING ACTIVITIES The following sections provide information on post-excavation soil gas sampling procedures and results. A map depicting the soil gas sample locations is included as Figure 4. These activities generally followed the procedures described in the Work Plan. Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 6 3.1 Soil Gas Sampling Procedures On January 10, 2023, approximately one month following the over excavation activities, eleven temporary soil gas probes were installed and subsequently sampled (BF-SG-1 through BF-SG-11) by Hanley Environmental. Five soil gas probes (BF-SG-1 through BF-SG-5) were installed within the footprints of Excavation A through Excavation D (beneath former Building 3), four soil gas probes were installed in the footprint of Excavation E (beneath former Building 4), one soil gas probe (BF-SG-10) was installed south of Excavation D, and one soil gas probe was installed east of Excavation E (BF-SG-11). Pursuant to the Work Plan, the soil gas samples were collected from approximately five ft bgs. The temporary soil gas sampling probes were installed using a decontaminated stainless-steel hand auger. Soil gas probes consisted of a 6-inch length screened soil gas sampling implant connected to ¼-inch diameter Teflon® tubing which extended to the ground surface for sample collection. A sand filter-pack was placed around the sampling implants to a height of approximately six inches above the screen (top of sand filter-pack was at four ft bgs). Hydrated granular bentonite was placed above the screen to the ground surface. The soil gas probes were allowed an equilibration period of 24 hours prior to sample collection. Boring logs and soil gas probe construction diagrams are included as Appendix D. Summa® canisters with 1.4-liter volume individually certified by the laboratory were used to collect the soil gas samples. Canisters were inspected prior to sampling to verify that vacuum levels were within 10% of the level recorded by the laboratory prior to shipment. Vacuum shut-in testing was performed at each sample location by closing a valve on the sample train to prevent airflow from the probe tubing to the sample train. The valve on the Summa® canister was then opened to confirm no vacuum losses occurred in the sample train. At least three sample train volumes of air were purged from each sample point prior to sampling. During purging, the sample canister, tubing, and sample point were surrounded with a shroud consisting of a plastic container. The container was filled with helium to Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 7 concentrations ranging from 9.1% to 12.2% as measured using a Dielectric MGD 2002 helium detector. Purged vapors were collected in Tedlar® bags using a GilAir5 air sampling pump. The helium concentration of the vapor in the Tedlar® bags was measured. If the concentration of helium in extracted vapors was greater than 10% of the helium concentration in the shroud, the sample train connections and sampling point seal were reevaluated and improved, and additional helium testing was performed until an acceptable result of less than 10% of the shroud helium concentration was measured. Following successful purging and leak testing, a soil gas sample was collected into the sample canister at a flow rate of approximately 140 milliliters per minute (mL/min). For QA/QC purposes, one duplicate sample (BF-SG-DUP) was collected from the BF-SG-1 location using a laboratory-supplied “T” fitting which allows for simultaneous collection of two samples from a single sample location. Final vacuum levels ranged from 4 to 5 inches of mercury (in Hg) vacuum in the canisters. Field sampling forms are included as Appendix E. After sampling, the canisters were transported under chain-of-custody protocols to Waypoint for analysis of volatile organic compounds (VOCs) by EPA Method TO-15 using the laboratory’s standard analyte list. Soil gas sample locations were recorded using a handheld GPS. After sample collection, the soil gas sampling probes were abandoned by Hanley Environmental. Soil cuttings generated during boring advancement were thin-spread on site. 3.2 Soil Gas Sampling Results Soil gas analytical results were compared to the NCDEQ Residential Sub-Slab and Exterior Soil Gas Screening Levels (SGSLs), based on the target cancer risk (TCR) of 1x10-6 and target hazard quotient (THQ) of 0.2, dated February 2024, and are summarized in Table 3. The laboratory analytical report and chain-of-custody record are included in Appendix C. Soil gas results indicate the presence of several VOCs at concentrations above laboratory reporting limits in each of the soil gas samples collected. TCE was detected at concentrations Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 8 exceeding the Residential SGSL of 14 micrograms per cubic meter (µg/m3) in two soil gas sample locations; BF-SG-1/BF-SG-DUP at concentrations up to 117 µg/m3, and BF-SG-9 at a concentration of 44.4 µg/m3. Several other compounds were detected at concentrations exceeding the Residential SGSLs including benzene (BF-SG-1/BF-SG-DUP through BF-SG-6, BF-SG-8, BF-SG-10, and BF-SG-11), bromodichloromethane (BF-SG-2), chloroform (BF-SG-2, BF-SG-4, and BF-SG-5), ethylbenzene (BF-SG-1 through BF-SG-6, BF-SG-8, BF-SG-10, and BF- SG-11), and naphthalene (BF-SG-1/BF-SG-DUP). No compounds were detected at concentrations above Non-Residential SGSLs. Figure 4 displays the locations of excavation areas and soil gas samples on a site plan with proposed building locations. The two locations with TCE concentrations exceeding the Residential SGSL (BF-SG-1 and BF-SG-9) are outside of proposed building footprints. Several sample locations are beneath proposed buildings (BF-SG-2 and BF-SG-5 beneath proposed Building 13 and BF-SG-8 beneath proposed Building 17), where TCE was not present in soil gas at concentrations above the Residential SGSL. Considering the density of soil gas samples collected and the isolated occurrence of TCE at concentrations exceeding its Residential SGSL at two of the eleven sample locations, the results of soil gas sampling are not indicative of a significant remaining source of chlorinated solvents in soil. The soil gas to indoor air pathway for the constituent concentrations detected can be reliably mitigated by installing and maintaining vapor intrusion mitigation systems on planned site buildings. 3.3 Risk Calculations To further evaluate the post-excavation soil gas data, Hanley Environmental utilized the NCDEQ Risk Calculator (February 2024 version) to calculate potential cumulative risks using concentrations of VOCs detected in the soil gas samples. The results of risk calculations are summarized in Table 3 and risk calculator outputs are provided in Appendix F. Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 9 Risk calculations were completed for each sample individually, and also using the highest detected concentration of each compound across all samples to represent a conservative, “worst case” risk for the post-excavation areas. As shown in Table 3, the calculated lifetime incremental cancer risk (LICR) did not exceed 10-4 in post-excavation soil gas samples, and the hazard index (HI) exceeded 1 in one sample (BF-SG-1/SG-DUP). The conservative, “worst- case” risk calculator results indicated a LICR of 3.2 x 10-5 and a HI of 2.2, however, a comparison of SG-1 risk calculator results indicates “worst-case” risk calculator results were predominantly influenced by soil gas sample BF-SG-1. The sample location with a hazard index exceeding 1 (BF-SG-1) was outside of proposed building footprints (see Figure 4). Sample locations beneath proposed buildings (BF-SG-2 and BF-SG-5 beneath proposed Building 13 and BF-SG-8 beneath proposed Building 17), had a LICR and HI below target values. 4.0 QUALITY ASSURANCE/QUALITY CONTROL For QA/QC purposes, one duplicate soil sample was collected from the OEX-E3(C)-2 confirmation soil sample location and one duplicate soil gas sample was collected from the BF-SG-1 location. A Level II QA/QC data package was included in the laboratory analytical reports. After a review of the QA/QC data in each laboratory report, the qualifiers listed in the laboratory reports are not considered to raise data quality concerns about the usability of data. Furthermore, comparison of the duplicate sample results to the parent samples indicated similar results. 5.0 CONCLUSIONS AND RECOMMENDATIONS Soil over excavation and post-excavation soil gas sampling activities were performed at the Harrelson Ford Brownfields Property in December 2023 and January 2024. Field activities were conducted pursuant to the Work Plan dated October 6, 2023. A summary of results and discussion of findings related to soil gas assessment results, risk to future occupants, and Land Use Restriction 12.b is presented below. Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 10 Soil  Approximately 192 CY of soil was excavated and disposed at a Subtitle D landfill. Excavations extended to the approximate depth of the water table capillary fringe.  The results of confirmation soil sampling demonstrated that PCE and TCE were not present at concentrations above the Protection of Groundwater PSRG.  The results of confirmation soil sampling demonstrate that the requirements of Land Use Restriction 12.b.(i) related to townhome redevelopment have been satisfied, and that no significant soil source of chlorinated solvents remains at the site following the remedial soil excavations. Soil Gas/Vapor Intrusion Potential  TCE was detected at concentrations above the Residential SGSL at two soil gas sample locations, BF-SG-1 and BF-SG-9. Benzene, bromodichloromethane, chloroform, ethylbenzene, and naphthalene were also detected at concentrations exceeding Residential SGSLs in one or more samples.  The two soil gas sample locations with TCE concentrations exceeding the Residential SGSL (BF-SG-1 and BF-SG-9) are outside of proposed building footprints. Several sample locations are beneath proposed buildings (BF-SG-2 and BF-SG-5 beneath proposed Building 13 and BF-SG-8 beneath proposed Building 17), where TCE was not present in soil gas at concentrations above the Residential SGSL.  The calculated LICR did not exceed 10-4 in post-excavation soil gas samples, and the HI exceeded 1 in one sample (BF-SG-1/SG-DUP).  As a conservative measure, the worst-case vapor intrusion risk was calculated using the maximum concentrations detected across all post-excavation soil gas samples. The risk calculator results indicated a LICR of 3.2 x 10-5 and a HI of 2.2, however, a comparison of SG-1 risk calculator results indicates “worst-case” risk calculator results were predominantly influenced by soil gas sample BF-SG-1. Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 11  The sample location with a hazard index exceeding 1 (BF-SG-1) was outside of proposed building footprints. Sample locations beneath proposed buildings (BF-SG-2 and BF-SG-5 beneath proposed Building 13 and BF-SG-8 beneath proposed Building 17), had a LICR and HI at levels meeting the standard set forth in LUR 12b.(ii). Vapor intrusion mitigation systems, which will be installed on all townhomes at the site, can reliably mitigate the soil gas to indoor air pathway for the constituent concentrations detected. In recognition of the isolated detections near Building 13 and Building 17 exceeding the thresholds set forth in LUR 12.b.(ii), active mitigation systems will be installed on those buildings as an additional measure to mitigate risk to occupants. Furthermore, trench dams will be installed at all site buildings along buried utilities at the locations where the utilities pass beneath site buildings to prevent soil gas transport underneath the buildings. Land Use Restriction 12.b.(ii) allows for approval of alternative suitable levels of confirmation soil gas results by NCDEQ in advance of townhome construction. Considering the extent and completeness of soil remediation conducted, the isolated occurrence of TCE detections exceeding the thresholds set forth in LUR 12.b.(ii), the locations of those TCE detections (outside of proposed building footprints), and the conservative mitigation measures that are proposed to be used in nearby buildings, the risk of vapor intrusion to proposed townhomes in the vicinity of the excavations is low. NCDEQ’s approval of townhome construction in areas of soil excavation is requested in accordance with LUR 12.b.(ii). Supplemental Soil Excavation Completion Report Harrelson Ford Brownfields Property 12 6.0 REFERENCES Hart & Hickman, P.C., Environmental Management Plan, dated November 4, 2022. Hart & Hickman, P.C., Soil Excavation Work Plan, dated November 22, 2022. Hart & Hickman, P.C., Soil Excavation Completion Report, dated March 20, 2023. Hart & Hickman, P.C., Soil Excavation and Post-Excavation Sampling Work Plan, dated October 6, 2023. Schmithorst, William, NCDEQ, Letter “Re: Redevelopment Status”, August 25, 2023. TABLES Table 1 Soil PID Response Summary Harrelson Ford Brownfields Property Brownfields Project Number 25046-21-060 Sample ID Depth Interval (ft bgs) PID Response (ppm) 0-3 0.2 3-6 0.2 6-9 0.3 0-3 0.2 3-6 0.3 6-9 0.3 0-3 0.2 3-6 0.3 6-9 0.3 0-3 0.1 3-6 0.1 6-9 0.1 0-3 0.3 3-6 0.3 6-9 0.2 0-3 0.2 3-6 0.2 6-9 0.3 0-3 6.8 3-6 7 6-9 5.9 0-3 10.7 3-6 14.1 6-9 33.4 0-3 4.7 3-6 3.6 6-9 6.7 0-3 8.7 3-6 10.8 6-9 52.4 0-3 0.3 3-6 0.6 6-9 8.1 0-3 0.3 3-6 0.3 6-9 0.2 0-3 0.2 3-6 0.2 6-9 0.2 0-3 0.3 3-6 0.2 6-9 0.2 0-3 0.2 3-6 0.7 6-9 0.4 0-3 0.4 3-6 0.3 6-9 0.2 0-3 0.3 3-6 0.1 6-9 0.2 0-3 0.1 3-6 0.1 6-9 0.3 0-3 0.3 3-6 0.3 6-9 0.2 0-3 0.3 3-6 0.3 6-9 0.1 0-3 0.3 3-6 0.3 6-9 0.2 0-3 0.2 3-6 0.2 6-9 0.2 Notes 1. Soil screened by Hanley Environmental during soil excavation activities conducted December 13, 2023. 2. PID = photoionization detector 3. ft bgs = feet below ground surface; ppm = parts per million 4. Soil at OEX-D1(C)* was overexcavated for off-site disposal. OEX-E3(A)-2 OEX-E3(B) OEX-E3(C)-1 OEX-E3(C)-2 OEX-E1(B) OEX-E1(C) OEX-E2(A) OEX-E2(B) OEX-E2(C) OEX-E3(A)-1 OEX-E1(A) OEX-B1(A)-1 OEX-B1(A)-2 OEX-B1(B)-1 OEX-B1(B)-2 OEX-B1(C)-1 OEX-B1(C)-2 OEX-D1(A) OEX-D1(B)-1 OEX-D1(B)-2 OEX-D1(C)* OEX-D1(C) Page 1 of 1 Table 2 Confirmation Soil Analytical Results Summary Harrelson Ford Brownfields Property Brownfields Project Number 25046-21-060 Sample ID OEX-B1(A)-1 OEX-B1(A)-2 OEX-B1(B)-1 OEX-B1(B)-2 OEX-B1(C)-1 OEX-B1(C)-2 OEX-D1(A)OEX-D1(B)-1 OEX-D1(B)-2 OEX-D1(C) Location Sample Date 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 Depth Interval (ft bgs)3-6 3-6 3-6 3-6 3-6 3-6 3-6 6-9 6-9 6-9 Tetrachloroethylene (PCE)<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0063 17 Trichloroethylene (TCE)<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.021 0.87 1. North Carolina Department of Environmental Quality (NCDEQ) Preliminary Soil Remediation Goals (PSRGs) dated February 2024. PSRGs based on target cancer risk of 1x10-6 and target hazard quotient of 0.1. 2. Detected concentrations are shown in bold 3. Values reported to the laboratory method detection limit. 4. Concentrations shown in milligrams per kilogram (mg/kg) 5. Only PCE and TCE reported for soil samples. 6. ft bgs = feet below ground surface 7. J indicates compound was detected at a concentration below the Reporting Limit (lowest calibration standard), detection is considered an estimate Notes: Overexcavation Area B Overexcavation Area D Volatile Organic Compounds (VOCs) - EPA Method 8260 (mg/kg) NCDEQ IHSB PSRGs1 Protection of Groundwater Residential Page 1 of 2 Table 2 Confirmation Soil Analytical Results Summary Harrelson Ford Brownfields Property Brownfields Project Number 25046-21-060 Sample ID OEX-E1(A)OEX-E1(B)OEX-E1(C)OEX-E2(A)OEX-E2(B)OEX-E2(C)OEX-E3(A)-1 OEX-E3(A)-2 OEX-E3(B)OEX-E3(C)-1 Location Sample Date 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 12/13/2023 Depth Interval (ft bgs)3-6 3-6 3-6 3-6 3-6 3-6 3-6 3-6 3-6 3-6 Tetrachloroethylene (PCE)<0.001 <0.001 <0.001 <0.001 <0.001 0.003 J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0063 17 Trichloroethylene (TCE)<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.021 0.87 1. North Carolina Department of Environmental Quality (NCDEQ) Preliminary Soil Remediation Goals (PSRGs) dated February 2024. PSRGs based on target cancer risk of 1x10-6 and target hazard quotient of 0.1. 2. Detected concentrations are shown in bold 3. Values reported to the laboratory method detection limit. 4. Concentrations shown in milligrams per kilogram (mg/kg) 5. Only PCE and TCE reported for soil samples. 6. ft bgs = feet below ground surface 7. J indicates compound was detected at a concentration below the Reporting Limit (lowest calibration standard), detection is considered an estimate 3-6 12/13/2023 Notes: Residential NCDEQ IHSB PSRGs1 Overexcavation Area E2Overexcavation Area E1 Protection of Groundwater Volatile Organic Compounds (VOCs) - EPA Method 8260 (mg/kg) OEX-E3(C)-2 / OEX-DUP Overexcavation Area E3 Page 2 of 2 Table 3 Post-Excavation Soil Gas Analytical Results Summary Harrelson Ford Brownfields Property Brownfields Project Number 25046-21-060 Sample ID BF-SG-2 BF-SG-3 BF-SG-4 BF-SG-5 BF-SG-6 BF-SG-7 BF-SG-8 BF-SG-9 BF-SG-10 BF-SG-11 Sample Type Soil Gas Soil Gas Soil Gas Soil Gas Soil Gas Soil Gas Soil Gas Soil Gas Soil Gas Soil Gas Sample Location Excavation B Excavation C South of Excavation D East of Excavation E Sample Duration Sample Collection Date Shroud Helium Concentration (%)9.4%11.0%9.6%9.1%10.0%10.8%9.7%9.1%10.4%10.0% Leak Check Helium Concentration (ppm)0 0 0 0 0 0 0 0 0 0 0 0 Acetone 18.0 21.7 24.6 29.8 76.2 103 31.7 11.5 44.2 9.78 64.5 38.0 Not Listed Not ListedBenzene75.8 74.8 41.1 23.4 16.4 32.8 22.2 5.05 28.7 1.24 J 27.7 32.4 12 160Bromodichloromethane<0.150 <0.150 5.08 <0.150 <0.150 <0.150 <0.150 <0.150 <0.150 <0.150 <0.150 <0.150 2.5 33Carbon Disulfide 20.6 18.1 7.19 10.9 2.49 J 8.38 4.65 J 3.97 J 12.4 0.504 J 37.3 17.9 4,900 61,000Carbon Tetrachloride 0.893 J 0.905 J <0.155 <0.155 <0.155 <0.155 <0.155 <0.155 <0.155 <0.155 <0.155 <0.155 16 200Chloroform1.65 J 1.70 J 45.2 1.04 J 4.21 10.6 0.912 J <0.086 1.74 J 1.07 J 1.15 J 1.79 J 4.1 53Cyclohexane<0.161 <0.161 <0.161 <0.161 <0.161 <0.161 <0.161 <0.161 <0.161 <0.161 7.34 2.36 J 42,000 530,0001,4-Dichlorobenzene <0.186 <0.186 0.625 J <0.186 <0.186 <0.186 <0.186 <0.186 <0.186 <0.186 <0.186 <0.186 8.5 110Dichlorodifluoromethane2.49 2.45 J 2.49 2.52 2.56 2.46 J 2.50 2.77 2.50 2.60 2.47 2.58 700 8,8001,1-Dichloroethane 1.79 J 1.80 J <0.101 <0.101 <0.101 <0.101 <0.101 <0.101 <0.101 <0.101 <0.101 <0.101 58 7701,1-Dichloroethene 2.61 2.66 <0.107 <0.107 <0.107 <0.107 <0.107 <0.107 <0.107 0.729 J 1.32 J <0.107 1,400 18,000cis-1,2-Dichloroethene 71.9 70.8 0.376 J <0.095 <0.095 <0.095 0.781 J <0.095 9.42 13.1 15.8 <0.095 280 3,500trans-1,2-Dichloroethene 2.34 2.36 <0.108 <0.108 <0.108 <0.108 <0.108 <0.108 <0.108 <0.108 0.693 J <0.108 280 3,500Ethyl Acetate 26.4 25.5 14.3 J 3.52 4.30 5.52 2.06 5.87 <0.136 <0.136 12.3 8.49 490 6,100Ethylbenzene58.2 57.9 74.4 44.9 49.4 60.2 38.9 7.12 52.6 0.620 J 47.9 64.6 37 4904-Ethyltoluene 7.23 7.31 13.1 6.33 5.08 7.80 5.67 0.806 J 5.68 <0.128 5.21 7.03 Not Listed Not ListedHeptane31.7 31.7 15.3 15.4 2.36 17.9 14.6 3.13 8.68 0.385 J 19.2 12.6 2,800 35,000n-Hexane 17.0 16.9 3.71 8.21 1.02 J 5.86 9.45 5.78 7.50 0.782 J 12.1 8.25 4,900 61,0002-Hexanone <0.285 <0.285 <0.285 <0.285 2.42 <0.285 <0.285 3.88 5.64 <0.285 <0.285 <0.285 210 2,600Isopropyl Alcohol 2.10 BJ 2.26 BJ 2.11 BJ 1.91 BJ 9.89 14.1 39.0 19.7 18.8 15.9 13.4 13.4 1,400 18,000Methyl Ethyl Ketone (MEK)4.96 5.62 4.66 5.00 13.3 16.7 5.03 3.50 12.2 1.58 16.3 6.21 35,000 440,000Methyl Tert-Butyl Ether (MTBE)26.2 26.2 1.71 J <0.033 4.04 3.45 <0.033 <0.033 1.15 J <0.033 0.767 J <0.033 360 4,7004-Methyl-2-Pentanone 3.11 3.15 1.54 J 0.991 J 0.901 J 2.30 1.61 J 1.58 J 2.15 0.634 J 1.67 J 1.15 J 21,000 260,000Methylene Chloride 3.75 3.62 2.90 3.22 2.83 2.57 2.06 1.16 J 2.80 1.26 J 2.35 1.62 J 3,400 53,000Naphthalene4.57 4.32 1.45 J 0.739 J <0.183 0.995 J 0.571 J 0.560 J <0.183 <0.183 0.566 J 0.571 J 2.8 36Propene3.62 3.67 1.94 5.81 3.17 5.22 2.74 4.63 30.5 77.1 23.0 12.1 21,000 260,000Styrene0.647 J 0.685 J 1.00 J 0.621 J 0.460 J 0.655 J 0.587 J <0.124 0.600 J <0.124 0.540 J 0.583 J 7,000 88,000Tetrachloroethene10610424.0 12.4 3.82 0.773 J 5.94 8.47 17.5 266 17.1 0.813 J 280 3,500Tetrahydrofuran17.0 23.5 1.89 2.48 2.46 1.03 J 6.68 8.45 51.5 0.333 J 4.73 2.00 14,000 180,000Toluene33834535623225033319449.0 288 4.47 244 323 35,000 440,000Trichloroethene1171155.64 <0.199 <0.199 <0.199 <0.199 0.607 J 2.55 44.4 8.19 <0.199 14 180Trichlorofluoromethane1.52 J 1.57 J 1.53 J 1.51 J 1.59 J 1.43 J 1.48 J 2.07 J 1.57 J 1.64 J 1.46 J 1.59 J Not Listed Not Listed1,1,2-Trichloro-1,2,2-trifluoroethane <0.561 <0.561 <0.561 <0.561 <0.561 <0.561 <0.561 0.567 J <0.561 <0.561 <0.561 <0.561 35,000 440,0001,2,4-Trimethylbenzene 24.8 24.6 41.0 19.7 15.0 23.7 16.8 2.51 15.5 <0.110 15.2 19.4 420 5,3001,3,5-Trimethylbenzene 6.81 6.78 10.4 5.12 4.32 6.41 4.39 0.688 J 4.97 <0.236 4.51 5.90 420 5,300Vinyl Chloride <0.127 1.90 <0.127 <0.127 <0.127 <0.127 <0.127 <0.127 <0.127 <0.127 <0.127 <0.127 5.6 280o-Xylene 42.2 41.9 51.6 31.4 33.9 41.3 26.1 4.34 34.1 0.603 J 32.2 42.1 700 8,800m,p-Xylene 134 135 174 104 113 139 89.5 14.7 115 1.44 J 108 145 700 8,800Xylene (Total)176 177 226 135 147 180 116 19.0 149 2.04 J 140 187 700 8,800 Residential Risk Calculator Output Calculated CR 2 x 10-5 3.7 x 10-6 3.7 x 10-6 7.3 x 10-6 3.3 X 10-6 8.8 x 10-7 4.4 x 10-6 3.9 X 10-6 4.6 X 10-6 5.4 X 10-6 Calculated HI 0.27 0.097 0.081 0.12 0.087 0.043 0.15 0.85 0.24 0.12 Rick Calculator Output Calculated CR Calculated HI 3. Only compounds detected in at least one sample shown in the table. Refer to laboratory analytical report for the full list of compounds.4. Detected concentrations are shown in bold Acceptable Risk Level Worst-Case Risk Calculations Acceptable Risk Level ≤1.0 ≤1 x 10-4 ≤1.0 ≤1 x 10-4 3.2 X 10-5 2.0 1.8 x 10-5 2.2 1/11/2024 10-minute NCDEQ Non- Residential SGSL (TCR = 1.0E-06; THQ=0.2) NCDEQ Residential SGSL (TCR = 1.0E-06; THQ=0.2) Volatile Organic Compounds (VOCs) - EPA Method TO-15 (μg/m3) 9. CR = cancer risk; TCR = target cancer risk; HI = hazard index; THQ = target hazard quotient; ppm = parts per million BF-SG-1 / SG-DUP Soil Gas Excavation A Excavation D Excavation E Notes:1. Concentrations shown in micrograms per cubic meter (µg/m3)2. NCDEQ SGSLs = North Carolina Department of Environmental Quality Vapor Intrusion Screening Level for Sub-Slab and Exterior Soil Gas (February 2024) Individual Sample Risk Calculations 5. Detected concentrations exceeding Residential SGSLs or acceptable risk levels are shaded in yellow6. Values shown with "<MDL" were not detected above the referenced method detection limit7. J indicates compound was detected at a concentration below the Reporting Limit (lowest calibration standard), detection is considered an estimate8. B indicates compound was detected in laboratory blank 12.2% Page 1 of 1 FIGURES 1 01/25/2024 PJ23030 NAH 0 Figure No.Date Project No. Drawn By Revision No. Title and Project Notes: 1. Topographic image obtained from United States Geological Services i(USGS) online interface managed by the USGS National Geospatial Program (NGP) on August 22, 2023. HANLEY ENVIRONMENTAL, PLLC323 MANNING DRIVECHARLOTTE, NORTH CAROLINANC LICENSE P-2407 Site Location Map Harrelson Ford Brownfields Property Brownfields Project Number 25046-21-060 6500 South Boulevard Charlotte, North Carolina Legend W E S N 1,000 2,000 FTSubject Property Boundary © 2024 Microsoft Corporation © 2023 Maxar ©CNES (2023) Distribution Airbus DS Former Building 1 Former Building 2 Former Building 3 Former Building 4 So u t h B l v d No r f o l k - S o u t h e r n R a i l w a y Cit y o f C h a r l o t t e B l u e l i n e ( L i g h t R a i l ) Old P i n e v i l l e R o a d 2 01/25/2024 PJ23030 NAH 0 Site Map Harrelson Ford Brownfields Property Brownfields Project Number 25046-21-060 6500 South Boulevard Charlotte, North Carolina Figure No.Date Project No. Drawn By Revision No. Title and Project Legend Notes: 1.Aerial image obtained from AutoCAD Geolocation feature © 2024 Microsoft Corporation © 2023 Maxar © CNES (2023) Distribution Airbus DS. 2.Subject property boundary provided in ALTA/NSPS Land Title Survey prepared by A.G. Zoutewelle Surveyors dated August 31, 2021. HANLEY ENVIRONMENTAL, PLLC 323 MANNING DRIVE CHARLOTTE, NORTH CAROLINA NC LICENSE P-2407 W E S N 30 ft 60 ft Subject Property Boundary OEX-E3(A)-2 OEX-E3(B) OEX-E3(C)-2 OEX-E3(C)-1 OEX-E2(B) OEX-E2(C) OEX-E1(B) OEX-E1(A) OEX-E1(C) OEX-D1(A)OEX-D1(C) OEX-D2(B)-2OEX-D1(B)-1 OEX-B1(C)-2 OEX-B1(C)-1 OEX-B1(B)-2 OEX-B1(A)-1 OEX-B1(A)-2 OEX-B1(B)-1 OEX-E3(A)-1 OEX-E2(A) 30 ft 60 ft 3 01/15/24 PJ23030 NAH 0 Excavation Area and Confirmation Soil Sample Location Map Harrelson Ford Brownfields Property Brownfields Project Number 25046-21-060 6500 South Boulevard Charlotte, North Carolina Figure No.Date Project No. Drawn By Revision No. Title and Project Legend Notes: 1.Aerial image obtained from Mecklenburg County Birdseye View dated January 2, 2024. 2.Subject property boundary provided in ALTA/NSPS Land Title Survey prepared by A.G. Zoutewelle Surveyors dated August 31, 2021. 3.Previous excavation extents provided in Soil Excavation Completed Report dated March 30, 2023 prepared by Hart & Hickman, PC. HANLEY ENVIRONMENTAL, PLLC 323 MANNING DRIVE CHARLOTTE, NORTH CAROLINA NC LICENSE P-2407 W E S N Subject Property Boundary Approximate Excavation Extent Previously Completed Overexcavation Extent Confirmation Soil Sample Excavation A Excavation D Excavation B Excavation C Excavation E BLDG #21 BLDG #20 BLDG #19 BLDG #18 BLDG #17 BLDG #15 BLDG #14 BLDG #11 BLDG #10 BLDG #7 BLDG #12 BLDG #9 BLDG #8 BLDG #25 BLDG #26 BLDG #6 BLDG #5 BLDG #4 BLDG #3 BLDG #2 BLDG #1 BLDG #22 BLDG #23 BLDG #24 BLDG #16 BLDG #13 BF-SG-11 BF-SG-1 BF-SG-3 BF-SG-5 BF-SG-10 BF-SG-8 BF-SG-7 BF-SG-6 BF-SG-2 BF-SG-9 BF-SG-4 BL D G # 2 5 BL D G # 2 5 BL D G # 2 5 BL D G # 2 5 BLDG #17 BLDG #15 BLDG #14 BLDG #11BLDG #12 BLDG #25 BLDG #24 BLDG #16 BLDG #13 BF-SG-11 BF-SG-1 BF-SG-3 BF-SG-5 BF-SG-10 BF-SG-8 BF-SG-7 BF-SG-6 BF-SG-2 BF-SG-9 BF-SG-4 4 01/26/2024 PJ23030 NAH 0 Post-Excavation Soil Gas Sample Locations Overlaying Redevelopment Plans Harrelson Ford Brownfields Property Brownfields Project Number 25046-21-060 6500 South Boulevard Charlotte, North Carolina Figure No.Date Project No. Drawn By Revision No. Title and Project Legend Notes: 1.Site redevelopment plan provided by LandDesign, Inc. dated May 17, 2023. 2.Subject property boundary provided in ALTA/NSPS Land Title Survey prepared by A.G. Zoutewelle Surveyors dated August 31, 2021. 3.Previous excavation extents provided in Soil Excavation Completed Report dated March 30, 2023 prepared by Hart & Hickman, PC. HANLEY ENVIRONMENTAL, PLLC 323 MANNING DRIVE CHARLOTTE, NORTH CAROLINA NC LICENSE P-2407 W E S N 15 ft 30 ft Subject Property Boundary Exterior Soil Gas Sample Location Approximate Excavation Extent Previously Completed Scale 50 100 ft Scale APPENDIX A Historical Data Summary Excerpts Table 1 Summary of Post-Excavation Confirmation Soil Samples for Excavation A Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXA-SW-N EXA-SW-S EXA-SW-W Depth (ft bgs)3-6 0-3 3-6 3-6 3-6 Sample Date 2/6/2023 2/6/2023 2/6/2023 2/6/2023 2/6/2023 Units VOCs (8260D) Chloromethane 0.0118 J 0.0119 J <0.0055 0.0217 <0.0051 0.015 23 99 cis-1,2-Dichloroethene <0.0024 0.012 0.0094 <0.0024 <0.0021 0.41 13 78 Methylene Chloride <0.0191 0.0216 J,C9 0.0868 C9 0.159 C9 <0.0168 0.025 58 650 Methyl tert-butyl ether <0.0026 0.0030 J <0.0024 <0.0026 <0.0023 0.09 49 220 Tetrachloroethene <0.0022 <0.0020 <0.0021 <0.0022 <0.0019 0.0063 17 82 Trichloroethene <0.0056 <0.0052 <0.0053 <0.0056 <0.0049 0.021 0.87 4.0 Notes: 1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laboratory analytical method shown in parentheses. Concentrations are reported in milligrams per kilogram (mg/kg). Concentrations are reported to the laboratory method detection limits. Only those compounds detected in at least one sample are shown in the table above. Bold values indicate compound concentration exceeds the Protection of Groundwater PSRG. VOCs = volatile organic compounds; ft bgs = feet below ground surfaceJ = Compound was detected at a concentration above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. C9 = Common laboratory contaminant. Screening Criteria Building 3 - Excavation A Protection of Groundwater PSRGs (1) mg/kg Residential PSRGs (1) Industrial/ Commercial PSRGs (1) EXA-SW-E https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/27/2023 Table 1 (Page 1 of 1) Hart & Hickman, PC Table 2 Summary of Post-Excavation Confirmation Soil Samples for Excavation B Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXB-SW-N1-2 EXB-SW-N2-2 EXB-TN-N2 EXB-SW-E1-2 EXB-SW-E2-2 EXB-SW-S2-2 EXB-SW-W1-A EXB-SW-W1-B EXB-SW-W2 Depth (ft bgs)3-6 3-6 5-7 3-6 3-6 3-6 3-6 3-6 3-6 Sample Date 2/14/2023 2/17/2023 2/23/2023 2/14/2023 2//14/2023 2/10/2023 2/16/2023 2/16/2023 2/6/2023 Units VOCs (8260D) Chloromethane 0.0060 J <0.0060 <0.0045 <0.0050 <0.0051 <0.0063 <0.0061 <0.0050 <0.0063 <0.0060 <0.0068 0.015 23 99 Methylene Chloride <0.0179 <0.0197 <0.0148 <0.0162 <0.0166 0.0314 C9 0.0818 C9 <0.0164 <0.0205 <0.0196 <0.0221 0.025 58 650 Tetrachloroethene <0.0021 0.0133 0.0037 J <0.0019 <0.0019 <0.0024 <0.0023 <0.0019 <0.0024 <0.0023 <0.0025 0.0063 17 82 Trichloroethene <0.0053 <0.0058 <0.0043 <0.0048 <0.0049 <0.0060 <0.0059 <0.0048 <0.0060 <0.0058 <0.0065 0.021 0.87 4.0 Xylene (Total)<0.0037 <0.0041 <0.0031 <0.0034 <0.0035 <0.0042 <0.0042 <0.0034 <0.0043 0.0143 <0.0046 9.9 120 530 m&p-Xylene <0.0045 <0.0049 <0.0037 <0.0040 <0.0042 <0.0051 <0.0050 <0.0041 <0.0051 0.0070 J <0.0055 9.8 120 500 o-Xylene <0.0029 <0.0032 <0.0024 <0.0026 <0.0027 <0.0033 <0.0032 <0.0026 <0.0033 0.0073 <0.0036 9.8 140 590 Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laborator anal tical method shown in parentheses. Concentrations are reported in milli rams per kilo ram m /k . Concentrations are reported to the laborator method detection limits. Only those compounds detected in at least one sample are shown in the table above. Bold values indicate compound concentration exceeds the Protection of Groundwater PSRG.VOCs = volatile organic compounds; ft bgs = feet below ground surface J = Compound was detected at a concentration above the laborator method detection limit, but below the laborator reportin limit resultin in a laborator estimated concentration. C9 = Common laborator contaminant. Building 3 - Excavation B mg/kg Protection of Groundwater PSRGs (1) Residential PSRGs (1) Industrial/ Commercial PSRGs (1) Screening Criteria 3-6 EXB-SW-S1-2/DUP-02 2/10/2023 https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/27/2023 Table 2 (Page 1 of 1) Hart & Hickman, PC Table 3 Summary of Post-Excavation Confirmation Soil Samples for Excavation C Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXC-SW-N EXC-SW-E EXC-SW-S EXC-SW-W EXC-B Depth (ft bgs)3-6 3-6 3-6 3-6 7 Sample Date 2/6/2023 2/6/2023 2/6/2023 2/6/2023 2/6/2023 Units VOCs (8260D) Methyl tert-butyl ether 0.0071 <0.0025 <0.0023 <0.0024 <0.0023 0.09 49 220 Methylene Chloride <0.0178 <0.0186 0.0532 C9 <0.0175 <0.0167 0.025 58 650 Tetrachloroethene <0.0021 <0.0021 <0.0019 <0.0020 <0.0019 0.0063 17 82 Trichloroethene <0.0052 <0.0055 <0.0050 <0.0052 <0.0049 0.021 0.87 4.0 Notes: 1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laboratory analytical method shown in parentheses. Concentrations are reported in milligrams per kilogram (mg/kg). Concentrations are reported to the laboratory method detection limits. Only those compounds detected in at least one sample are shown in the table above.Bold values indicate compound concentration exceeds the Protection of Groundwater PSRG. VOCs = volatile organic compounds; ft bgs = feet below ground surface C9 = Common laboratory contaminant. mg/kg Protection of Groundwater PSRGs (1) Screening Criteria Residential PSRGs (1) Industrial/ Commercial PSRGs (1) Building 3 - Excavation C https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/27/2023 Table 3 (Page 1 of 1) Hart & Hickman, PC Table 4 Summary of Post-Excavation Confirmation Soil Samples for Excavation D Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXD-SW-N-B EXD-SW-N2 EXD-SW-N3 EXD-SW-N4 Depth (ft bgs)3-6 6-9 3-6 3-6 Sample Date 3/1/2023 2/14/2023 2/8/2023 2/8/2023 Units VOCs (8260D) 2-Butanone (MEK)<0.0293 <0.0295 <0.0269 <0.0255 <0.0268 <0.0361 <0.0298 <0.0314 17 5,500 40,000 cis-1,2-Dichloroethene <0.0021 <0.0021 <0.0019 <0.0018 <0.0019 <0.0026 <0.0021 <0.0022 0.41 13 78 n-Butylbenzene <0.0038 <0.0039 <0.0035 <0.0033 <0.0035 <0.0047 0.0050 J <0.0041 4.5 780 12,000 sec-Butylbenzene <0.0027 <0.0027 <0.0025 <0.0023 <0.0025 <0.0033 <0.0027 <0.0029 4.1 1,600 23,000 Ethylbenzene 0.0059 J <0.0029 <0.0026 <0.0025 <0.0026 <0.0035 <0.0029 <0.0030 13 6.1 27 Methylene Chloride <0.0167 <0.0168 <0.0153 0.0450 C9 <0.0153 0.0498 C9,B <0.017 0.0398 C9 0.025 58 650 p-Isopropyltoluene <0.0030 <0.0030 <0.0028 <0.0026 <0.0027 <0.0037 <0.0031 <0.0032 NE NE NE Tetrachloroethene <0.0019 <0.0019 <0.0018 <0.0017 <0.0018 <0.0024 <0.0020 <0.0021 0.0063 17 82 Toluene 0.0089 0.0080 0.0049 J <0.0037 <0.0039 <0.0052 <0.0043 <0.0045 8.3 990 9,700 Trichloroethene <0.0049 <0.0049 <0.0045 <0.0043 <0.0045 <0.0061 <50.0050 <0.0053 0.021 0.87 4.0 1,2,4-Trimethylbenzene 0.0060 J <0.0036 <0.0033 <0.0032 <0.0033 <0.0045 <0.0037 <0.0039 12 63 370 Xylene (Total)0.0109 J <0.0035 <0.0032 <0.0030 <0.0032 <0.0043 <0.0035 <0.0037 9.9 120 530 m&p-Xylene 0.0109 J <0.0042 <0.0038 <0.0036 <0.0038 <0.0051 <0.0043 <0.0045 9.8 120 500 o-Xylene <0.0027 <0.0027 <0.0025 <0.0023 <0.0025 <0.0033 <0.0027 <0.0029 9.8 120 590 Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laboratory analytical method shown in parentheses. Concentrations are reported in milligrams per kilogram (mg/kg). Concentrations are reported to the laboratory method detection limits. Only those compounds detected in at least one sample are shown in the table aboveBold values indicate compound concentration exceeds the Protection of Groundwater PSRG VOCs = volatile organic compounds; ft bgs = feet below ground surface; NE = not established J = Compound was detected at a concentration above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. C9 = Common laboratory contaminant. B = Compound was detected in the laboratory method blank. mg/kg EXD-SW-N-C/DUP-08 3-6 3/1/2023 EXD-SW-N2/DUP-03 3-6 2/10/2023 Building 3 - Excavation D Screening Criteria Protection of Groundwater PSRGs (1) Residential PSRGs (1) Industrial/ Commercial PSRGs (1) https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/28/2023 Table 4 (Page 1 of 4) Hart & Hickman, PC Table 4 Summary of Post-Excavation Confirmation Soil Samples for Excavation D Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXD-SW-N5 EXD-SW-N6-A EXD-SW-N6-B-2 EXD-SW-E1 EXD-SW-E2 Depth (ft bgs)3-6 3-6 3-6 3-6 3-6 Sample Date 2/8/2023 2/16/2023 2/23/2023 2/16/2023 2/16/2023 Units VOCs (8260D) 2-Butanone (MEK)<0.0327 <0.0292 <0.0294 <0.0297 <0.0301 <0.0317 <0.0296 17 5,500 40,000 cis-1,2-Dichloroethene <0.0023 <0.0021 0.0365 <0.0021 <0.0021 <0.0023 <0.0021 0.41 13 78 n-Butylbenzene <0.0043 <0.0038 <0.0039 <0.0039 <0.0039 <0.0042 <0.0039 4.5 780 12,000 sec-Butylbenzene <0.0030 <0.0027 <0.0027 <0.0027 <0.0028 <0.0029 <0.0027 4.1 1,600 23,000 Ethylbenzene <0.0032 <0.0028 <0.0029 0.0036 J <0.0029 <0.0031 <0.0029 13 6.1 27 Methylene Chloride 0.0659 C9 <0.0167 <0.0168 <0.0170 <0.0172 <0.0181 <0.0169 0.025 58 650 p-Isopropyltoluene <0.0033 <0.0030 <0.0030 <0.0030 <0.0031 <0.0032 <0.0030 NE NE NE Tetrachloroethene <0.0022 <0.0019 0.0042 J <0.0020 <0.0020 <0.0021 <0.0020 0.0063 17 82 Toluene <0.0047 <0.0042 <0.0042 <0.0043 <0.0043 <0.0046 <0.0043 8.3 990 9,700 Trichloroethene <0.0055 <0.0049 <0.0049 <0.0050 <0.0050 <0.0053 <0.0050 0.021 0.87 4.0 1,2,4-Trimethylbenzene <0.0040 <0.0036 <0.0036 <0.0037 <0.0037 <0.0039 <0.0037 12 63 370 Xylene (Total)<0.0039 <0.0035 <0.0035 0.0153 <0.0036 <0.0038 <0.0035 9.9 120 530 m&p-Xylene <0.0047 <0.0042 <0.0042 0.0064 J <0.0043 <0.0045 <0.0042 9.8 120 500 o-Xylene <0.0030 <0.0027 <0.0027 0.0089 <0.0028 <0.0029 <0.0027 9.8 120 590 Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laboratory analytical method shown in parentheses. Concentrations are reported in milligrams per kilogram (mg/kg). Concentrations are reported to the laboratory method detection limits. Only those compounds detected in at least one sample are shown in the table aboveBold values indicate compound concentration exceeds the Protection of Groundwater PSRG VOCs = volatile organic compounds; ft bgs = feet below ground surface; NE = not established J = Compound was detected at a concentration above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. C9 = Common laboratory contaminant. B = Compound was detected in the laboratory method blank. mg/kg Building 3 - Excavation D Screening Criteria EXD-SW-N7/DUP-05 3-6 2/16/2023 Residential PSRGs (1) Industrial/ Commercial PSRGs (1) Protection of Groundwater PSRGs (1) https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/28/2023 Table 4 (Page 2 of 4) Hart & Hickman, PC Table 4 Summary of Post-Excavation Confirmation Soil Samples for Excavation D Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXD-TS-1 EXD-SW-S2-B EXD-SW-S3 EXD-SW-S4 EXD-SW-S4-2 Depth (ft bgs)3-6 6-9 5-7 6-9 3-6 3-6 0-3 Sample Date 2/14/2023 2/14/2023 2/21/2023 2/14/2023 2/8/2023 2/8/2023 2/9/2023 Units VOCs (8260D) 2-Butanone (MEK)<0.0262 0.0350 J <0.0259 <0.0254 <0.0269 <0.0270 <0.0273 <0.0281 <0.0271 17 5,500 40,000 cis-1,2-Dichloroethene <0.0019 <0.0025 <0.0018 <0.0018 <0.0019 <0.0019 <0.0019 <0.0020 <0.0019 0.41 13 78 n-Butylbenzene <0.0034 <0.0046 <0.0034 <0.0033 <0.0035 <0.0035 <0.0036 <0.0037 <0.0036 4.5 780 12,000 sec-Butylbenzene <0.0024 0.0305 <0.0024 <0.0023 <0.0025 <0.0025 <0.0025 <0.0026 <0.0025 4.1 1,600 23,000 Ethylbenzene <0.0025 <0.0034 <0.0025 <0.0025 <0.0026 <0.0026 <0.0026 <0.0027 <0.0026 13 6.1 27 Methylene Chloride 0.258 C9,B 0.327 C9 <0.0148 0.222 C9,B 0.0783 C9,B 0.241 C9,B 0.0519 C9 0.0876 C9 <0.0155 0.025 58 650 p-Isopropyltoluene <0.0027 <0.0036 <0.0027 <0.0026 <0.0028 <0.0028 <0.0028 <0.0029 <0.0028 NE NE NE Tetrachloroethene 0.564 3.81 <0.0017 <0.0017 <0.0018 <0.0018 <0.0018 <0.0018 <0.0018 0.0063 17 82 Toluene <0.0038 0.0226 <0.0037 <0.0036 <0.0039 <0.0039 <0.0039 <0.0040 <0.0039 8.3 990 9,700 Trichloroethene <0.0044 0.0270 <0.0044 <0.0043 <0.0045 <0.0045 <0.0046 <0.0047 <0.0046 0.021 0.87 4.0 1,2,4-Trimethylbenzene <0.0032 <0.0043 <0.0032 <0.0031 <0.0033 <0.0033 <0.0034 <0.0035 <0.0034 12 63 370 Xylene (Total)<0.0031 0.0356 <0.0031 <0.0030 <0.0032 <0.0032 <0.0032 <0.0033 <0.0032 9.9 120 530 m&p-Xylene <0.0037 0.0254 <0.0037 <0.0036 <0.0038 <0.0038 <0.0039 <0.0040 <0.0039 9.8 120 500 o-Xylene <0.0024 0.0102 <0.0024 <0.0023 <0.0025 <0.0025 <0.0025 <0.0026 <0.0025 9.8 120 590 Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laboratory analytical method shown in parentheses. Concentrations are reported in milligrams per kilogram (mg/kg). Concentrations are reported to the laboratory method detection limits. Only those compounds detected in at least one sample are shown in the table aboveBold values indicate compound concentration exceeds the Protection of Groundwater PSRG VOCs = volatile organic compounds; ft bgs = feet below ground surface; NE = not established J = Compound was detected at a concentration above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. C9 = Common laboratory contaminant. B = Compound was detected in the laboratory method blank. Residential PSRGs (1) Industrial/ Commercial PSRGs (1) Building 3 - Excavation D Protection of Groundwater PSRGs (1) Screening Criteria mg/kg 2/14/2023 EXD-SW-S1 EXD-SW-S2-B/DUP-04 3-6 https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/28/2023 Table 4 (Page 3 of 4) Hart & Hickman, PC Table 4 Summary of Post-Excavation Confirmation Soil Samples for Excavation D Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXD-SW-S5 EXD-SW-S6 EXD-SW-S7 EXD-SW-W2-2 EXD-SW-W3 Depth (ft bgs)3-6 3-6 3-6 3-6 6-9 5-7 3-6 Sample Date 2/8/2023 2/7/2023 2/16/2023 2/14/2023 2/14/2023 2/21/2023 3/1/2023 Units VOCs (8260D) 2-Butanone (MEK)<0.0451 <0.0296 <0.0301 <0.0285 <0.0496 <0.0383 <0.0288 17 5,500 40,000 cis-1,2-Dichloroethene <0.0032 0.0034 J <0.0021 <0.0020 <0.0035 <0.0027 <0.0020 0.41 13 78 n-Butylbenzene <0.0059 <0.0039 <0.0039 <0.0037 <0.0065 <0.0050 <0.0038 4.5 780 12,000 sec-Butylbenzene <0.0041 <0.0027 <0.0028 <0.0026 <0.0045 <0.0035 <0.0026 4.1 1,600 23,000 Ethylbenzene <0.0044 <0.0029 0.0041 J <0.0028 <0.0048 <0.0037 <0.0028 13 6.1 27 Methylene Chloride <0.0258 0.106 C9 <0.0172 0.239 C9,B 0.336 C9 <0.0219 <0.0164 0.025 58 650 p-Isopropyltoluene <0.0046 <0.0030 <0.0031 <0.0029 <0.0051 <0.0039 <0.0029 NE NE NE Tetrachloroethene <0.0030 <0.0019 <0.0020 <0.0019 <0.0033 <0.0025 <0.0019 0.0063 17 82 Toluene <0.0065 <0.0042 <0.0043 <0.0041 <0.0071 <0.0055 0.0050 J 8.3 990 9,700 Trichloroethene <0.0076 <0.0050 <0.0051 <0.0048 <0.0083 <0.0064 <0.0048 0.021 0.87 4.0 1,2,4-Trimethylbenzene <0.0056 <0.0037 <0.0037 <0.0035 <0.0061 <0.0047 <0.0036 12 63 370 Xylene (Total)<0.0054 <0.0035 0.0162 <0.0034 <0.0059 <0.0046 <0.0034 9.9 120 530 m&p-Xylene <0.0064 <0.0042 0.0072 J <0.0041 <0.0071 <0.0055 <0.0041 9.8 120 500 o-Xylene <0.0042 <0.0027 0.0090 <0.0026 <0.0046 <0.0035 <0.0026 9.8 120 590 Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laboratory analytical method shown in parentheses. Concentrations are reported in milligrams per kilogram (mg/kg). Concentrations are reported to the laboratory method detection limits. Only those compounds detected in at least one sample are shown in the table aboveBold values indicate compound concentration exceeds the Protection of Groundwater PSRG VOCs = volatile organic compounds; ft bgs = feet below ground surface; NE = not established J = Compound was detected at a concentration above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. C9 = Common laboratory contaminant. B = Compound was detected in the laboratory method blank. Screening Criteria Building 3 - Excavation D mg/kg EXD-SW-W1 Protection of Groundwater PSRGs (1) Residential PSRGs (1) Industrial/ Commercial PSRGs (1) https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/28/2023 Table 4 (Page 4 of 4) Hart & Hickman, PC Table 5 Summary of Post-Excavation Confirmation Soil Samples for Excavation E Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXE-SW-1N-A EXE-SW-1N-B EXE-SW-1N-C EXE-SW-2N EXE-SW-3N-A EXE-SW-3N-B EXE-SW-3N-C EXE-SW-4N EXE-SW-5N-A EXE-SW-5N-B EXE-SW-6N-3 EXE-TN-6 EXE-SW-7N-3 Depth (ft bgs)2-5 2-5 2-5 2-5 2-5 2-5 2-5 2-5 3-6 3-6 3-6 5-7 3-6 Sample Date 2/17/2023 2/17/2023 2/17/2023 2/8/2023 2/10/2023 2/10/2023 2/10/2023 2/8/2023 2/20/2023 2/20/2023 2/20/2023 2/22/2023 2/20/2023 Units VOCs (8260D) Acetone <0.0412 <0.0358 <0.0365 <0.0440 <0.0412 <0.0474 <0.0439 <0.0444 <0.0416 <0.0466 <0.0410 <0.0421 <0.0381 25 14,000 210,000 Bromomethane <0.0199 <0.0173 <0.0176 <0.0212 <0.0199 <0.0229 <0.0212 <0.0214 <0.0201 <0.0225 <0.0198 <0.0203 <0.0184 0.05 1.4 6.4 tert-Butylbenzene <0.0023 <0.0020 <0.0020 <0.0024 <0.0023 <0.0026 <0.0024 <0.0025 <0.0023 <0.0026 <0.0023 <0.0023 <0.0021 3.1 1,600 23,000 Chloromethane <0.0054 <0.0047 <0.0048 <0.0058 <0.0054 <0.0062 <0.0057 <0.0058 <0.0054 <0.0061 <0.0054 <0.0055 <0.0050 0.015 23 99 2-Chlorotoluene <0.023 <0.0020 <0.0020 <0.0024 <0.0023 <0.0026 <0.0024 <0.0024 <0.0023 <0.0026 <0.0023 <0.0023 <0.0021 2.0 310 4,700 cis-1,2-Dichloroethene 0.0436 <0.0019 0.0701 0.211 0.0942 0.0073 J 0.0203 0.0653 <0.0022 <0.0025 0.0056 J <0.0022 <0.0020 0.41 13 78 Diisopropyl ether <0.0017 <0.0015 <0.0015 <0.0018 <0.0017 <0.0020 <0.0018 <0.0019 <0.0018 <0.0020 <0.0017 <0.0018 <0.0016 0.36 480 2,000 Ethylbenzene <0.0030 <0.0026 <0.0026 <0.0032 <0.0030 <0.0034 <0.0032 <0.0032 <0.0030 <0.0034 0.0036 J <0.0031 <0.0028 13 6.1 27 p-Isopropyltoluene <0.0032 <0.0027 <0.0028 <0.0034 <0.0032 <0.0036 <0.0034 <0.0034 <0.0032 <0.0036 <0.0031 <0.0032 <0.0029 NE NE NE Methyl-tert-butyl ether 0.0049 J <0.0021 <0.0021 <0.0026 <0.0024 <0.0028 <0.0026 <0.0026 <0.0024 <0.0027 <0.0024 <0.0025 <0.0022 0.09 49 220 Methylene Chloride <0.0176 <0.0153 <0.0156 <0.0188 0.0532 C9 <0.0202 0.0702 C9 0.0300 C9 <0.0178 <0.0199 <0.0175 <0.0180 <0.0163 0.025 58 650 n-Propylbenzene <0.0023 <0.0020 <0.0020 <0.0024 <0.0023 <0.0026 <0.0024 <0.0025 <0.0023 <0.0026 <0.0023 <0.0023 <0.0021 2.6 780 5,100 Tetrachloroethene <0.0020 <0.0018 <0.0018 <0.0022 <0.0020 <0.0023 <0.0022 <0.0022 <0.0020 <0.0023 <0.0020 <0.0021 <0.0019 0.0063 17 82 Toluene <0.0044 <0.0038 <0.0039 <0.0047 <0.0044 <0.0051 <0.0047 <0.0048 <0.0045 <0.0050 <0.0044 <0.0045 <0.0041 8.3 990 9,700 Trichloroethene <0.0052 <0.0045 <0.0046 <0.0055 <0.0052 <0.0060 <0.0055 <0.0056 <0.0052 <0.0059 0.0057 J <0.0053 <0.0048 0.021 0.87 4.0 1,2,4-Trimethylbenzene <0.0038 <0.0033 <0.0034 <0.0041 <0.0038 <0.0044 <0.0041 <0.0041 <0.0039 0.0047 J 0.0079 <0.0039 0.0054 J 12 63 370 1,3,5-Trimethylbenzene <0.0022 <0.0019 <0.0019 <0.0023 <0.0022 <0.0025 <0.0023 <0.0023 <0.0022 <0.0024 0.0033 J <0.0022 0.0035 J 11 56 320 Xylene (Total)<0.0037 <0.0032 <0.0032 <0.0039 <0.0037 <0.0042 <0.0039 <0.0039 <0.0037 0.0088 J 0.0082 J <0.0037 0.0055 J 9.9 120 530 m&p-Xylene <0.0044 <0.0038 <0.0039 <0.0047 <0.0044 <0.0051 <0.0047 <0.0047 <0.0044 0.0088 J 0.0082 J <0.0045 0.0055 J 9.8 120 500 o-Xylene <0.0028 <0.0025 <0.0025 <0.0030 <0.0028 <0.0033 <0.0030 <0.0031 <0.0029 <0.0032 <0.0028 <0.0029 <0.0026 9.8 140 590 Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laborator anal tical method shown in parentheses. Concentrations are reported in milli rams per kilo ram m /k . Concentrations are reported to the laborator method detection limits.Only those compounds detected in at least one sample are shown in the table above. Bold values indicate compound concentration exceeds the Protection of Groundwater PSRG.VOCs = volatile organic compounds; ft bgs = feet below ground surface; NE = not establishedJ = Compound was detected at a concentration above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. C9 = Common laborator contaminant. B = Compound was detected in the laborator method blank. Building 4 - Excavation E - Northern Sidewall mg/kg Screening Criteria Protection of Groundwater PSRGs (1) Residential PSRGs (1) Industrial/ Commercial PSRGs (1) https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/28/2023 Table 5 (Page 1 of 5) Hart & Hickman, PC Table 5 Summary of Post-Excavation Confirmation Soil Samples for Excavation E Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXE-SW-8N-B EXE-SW-1S-B EXE-SW-2S-B EXE-SW-3S-A EXE-SW-4S-A EXE-SW-5S-B EXE-SW-6S-2 EXE-SW-7S-2 EXE-SW-8S EXE-TS-8 Depth (ft bgs)2-5 2-5 2-5 2-5 3-6 2-5 2-5 2-5 2-5 2-5 Sample Date 2/14/2023 2/17/2023 2/17/2023 2/17/2023 2/17/2023 2/8/2023 2/10/2023 2/10/2023 2/10/2023 2/22/2023 Units VOCs (8260D) Acetone <0.0481 0.0621 J <0.0381 <0.0384 <0.0396 <0.0380 <0.0383 <0.0414 <0.387 <0.0461 <0.0424 <0.0402 25 14,000 210,000 Bromomethane <0.0232 <0.0187 <0.0184 <0.0185 <0.0191 <0.0184 <0.0185 <0.0019 <0.187 <0.0223 <0.0205 <0.0194 0.05 1.4 6.4 tert-Butylbenzene <0.0027 <0.0022 <0.0021 <0.0021 <0.0022 <0.0021 0.0032 J <0.0023 <0.0215 <0.0026 <0.0024 <0.0022 3.1 1,600 23,000 Chloromethane <0.0063 <0.0051 <0.0050 <0.0050 <0.0052 <0.0050 0.0072 J <0.0054 39.6 <0.0060 0.0067 J <0.0053 0.015 23 99 2-Chlorotoluene <0.0027 <0.0021 <0.0021 <0.0021 <0.0022 <0.0021 0.0033 J <0.0023 <0.0214 <0.0025 <0.0023 <0.0022 2.0 310 4,700 cis-1,2-Dichloroethene <0.0026 <0.0021 <0.0020 <0.0020 <0.0021 <0.0020 <0.0020 <0.0022 <0.0206 0.0363 0.0188 <0.0021 0.41 13 78 Diisopropyl ether <0.0020 <0.0016 <0.0016 <0.0016 <0.0017 <0.0016 0.0080 0.0055 J <0.0163 <0.0019 <0.0018 0.0049 J 0.36 480 2,000 Ethylbenzene <0.0035 0.0046 J <0.0028 <0.0028 <0.0029 <0.0028 0.0060 0.0034 J <0.0281 <0.0033 <0.0031 <0.0029 13 6.1 27 p-Isopropyltoluene <0.0037 <0.0030 <0.0029 <0.0029 <0.0030 <0.0029 0.0040 J <0.0032 <0.0297 <0.0035 <0.0032 <0.0031 NE NE NE Methyl-tert-butyl ether <0.0028 <0.0023 <0.0022 <0.0022 <0.0023 <0.0022 <0.0022 <0.0024 <0.0226 <0.0027 <0.0025 <0.0023 0.09 49 220 Methylene Chloride 0.0576 C9,B <0.0166 <0.0163 <0.0164 <0.0169 0.0924 C9 <0.0163 <0.0177 1.26 C9 0.0375 C9 0.0882 C9 <0.0172 0.025 58 650 n-Propylbenzene <0.0027 <0.0022 <0.0021 <0.0021 <0.0022 <0.0021 0.0039 J <0.0023 <0.0215 <0.0026 <0.0024 <0.0022 2.6 780 5,100 Tetrachloroethene <0.0024 <0.0019 <0.0019 <0.0019 <0.0019 0.0217 <0.0019 <0.0020 <0.0191 <0.0023 <0.0021 <0.0020 0.0063 17 82 Toluene <0.0052 0.0069 0.0060 <0.0041 <0.0043 <0.0041 0.0060 0.0046 J <0.0416 <0.0050 <0.0046 <0.0043 8.3 990 9,700 Trichloroethene <0.0060 <0.0049 <0.0048 <0.0048 <0.0050 <0.0048 <0.0048 <0.0052 <0.0486 <0.0058 0.0058 J <0.0050 0.021 0.87 4.0 1,2,4-Trimethylbenzene <0.0045 <0.0036 <0.0035 <0.0036 <0.0037 <0.0035 0.0039 J <0.0038 <0.0358 <0.0043 <0.0039 <0.0037 12 63 370 1,3,5-Trimethylbenzene <0.0025 <0.0020 <0.0020 <0.0020 <0.0021 <0.0020 0.0045 J <0.0022 <0.0203 <0.0024 <0.0022 <0.0021 11 56 320 Xylene (Total)<0.0043 0.0152 <0.0034 <0.0034 <0.0035 <0.0034 0.0159 0.0058 J <0.0344 <0.0041 <0.0038 <0.0036 9.9 120 530 m&p-Xylene <0.0051 0.0087 J <0.0041 <0.0041 <0.0042 <0.0041 0.0092 J 0.0058 J <0.0413 <0.0049 <0.0045 <0.0043 9.8 120 500 o-Xylene <0.0033 0.0065 <0.0026 <0.0026 <0.0027 <0.0026 0.0067 <0.0029 <0.0267 <0.0032 <0.0029 <0.0028 9.8 140 590 Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laborator anal tical method shown in parentheses. Concentrations are reported in milli rams per kilo ram m /k . Concentrations are reported to the laborator method detection limits.Only those compounds detected in at least one sample are shown in the table above. Bold values indicate compound exceed the Protection of Groundwater PSRG, but were below the Residential PSRG.VOCs = volatile organic compounds; ft bgs = feet below ground surface; NE = not establishedJ = Compound was detected at a concentration above the laboratory method detection limits, but below the laboratory reporting limits resulting in a laboratory estimated concentration. C9 = Common laborator contaminant. B = Compound was detected in the laborator method blank. EXE-TS-5/DUP-07 25 2/22/2023 mg/kg Building 4 - Excavation E - Southern Sidewall Screening Criteria Protection of Groundwater PSRGs (1) Residential PSRGs (1) Industrial/ Commercial PSRGs (1) https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/28/2023 Table 5 (Page 2 of 5) Hart & Hickman, PC Table 5 Summary of Post-Excavation Confirmation Soil Samples for Excavation E Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXE-SW-1E-2-A EXE-SW-2E-2 EXE-SW-3E-2 EXE-SW-4E EXE-SW-5E EXE-SW-1W EXE-SW-2W EXE-SW-3W EXE-SW-4W Depth (ft bgs)2-5 2-5 2-5 2-5 2-5 2-5 2-5 2-5 2-5 Sample Date 2/14/2023 2/14/2023 2/14/2023 2/10/2023 2/10/2023 2/7/2023 2/7/2023 2/9/2023 2/17/2023 Units VOCs (8260D) Acetone <0.0466 <0.0482 <0.0427 <0.0435 <0.408 <0.0470 <0.0409 <0.0729 0.0510 J 25 14,000 210,000 Bromomethane <0.0225 <0.0233 <0.0206 <0.0210 <0.197 <0.0227 <0.0197 0.0355 J <0.0174 0.05 1.4 6.4 tert-Butylbenzene <0.0026 <0.0027 <0.0024 <0.0024 <0.0226 <0.0026 <0.0023 <0.0040 <0.0020 3.1 1,600 23,000 Chloromethane <0.0061 <0.0063 <0.0056 <0.0057 36.9 <0.0061 <0.0053 8.02 <0.0047 0.015 23 99 2-Chlorotoluene <0.0026 <0.0027 <0.0024 <0.0024 <0.0225 <0.0026 <0.0023 <0.0040 <0.0020 2.0 310 4,700 cis-1,2-Dichloroethene 0.0438 0.0294 0.0176 0.0102 <0.0217 0.114 0.138 0.0761 0.0168 0.41 13 78 Diisopropyl ether <0.0020 <0.0020 <0.0018 <0.0018 <0.0172 <0.0020 <0.0017 <0.0031 <0.0015 0.36 480 2,000 Ethylbenzene <0.0034 <0.0035 <0.0031 <0.0032 <0.0296 0.0049 J 0.0035 J <0.0053 <0.0026 13 6.1 27 p-Isopropyltoluene <0.0036 <0.0037 <0.0033 <0.0033 <0.0313 <0.0036 <0.0031 <0.0056 <0.0028 NE NE NE Methyl-tert-butyl ether <0.0027 <0.0028 <0.0025 <0.0025 <0.0238 <0.0027 0.0193 0.0117 <0.0021 0.09 49 220 Methylene Chloride 0.0624 C9,B 0.0555 C9,B 0.0991 C9,B 0.0502 C9 1.50 C9 <0.0201 <0.0174 <0.0311 <0.0154 0.025 58 650 n-Propylbenzene <0.0026 <0.0027 <0.0024 <0.0024 <0.0226 <0.0026 <0.0023 <0.0040 <0.0020 2.6 780 5,100 Tetrachloroethene 0.0173 <0.0024 0.0548 0.0054 J <0.0201 <0.0023 <0.0020 <0.0036 <0.0018 0.0063 17 82 Toluene <0.0050 <0.0052 <0.0046 <0.0047 <0.0439 <0.0050 <0.0044 <0.0078 <0.0039 8.3 990 9,700 Trichloroethene 0.0397 <0.0061 0.0307 <0.0055 <0.0513 <0.0059 <0.0051 <0.0092 <0.0045 0.021 0.87 4.0 1,2,4-Trimethylbenzene <0.0043 <0.0045 <0.0039 <0.0040 <0.0378 <0.0043 <0.0038 <0.0067 <0.0033 12 63 370 1,3,5-Trimethylbenzene <0.0024 <0.0025 <0.0022 <0.0023 <0.0214 <0.0025 <0.0021 <0.0038 <0.0019 11 56 320 Xylene (Total)<0.0041 <0.0043 <0.0038 <0.0039 <0.0362 0.0058 J <0.0036 <0.0065 <0.0032 9.9 120 530 m&p-Xylene <0.0050 <0.0051 <0.0045 <0.0046 <0.0435 0.0058 J <0.0044 <0.0078 <0.0038 9.8 120 500 o-Xylene <0.0032 <0.0033 <0.0029 <0.0030 <0.0281 <0.0032 <0.0028 <0.0050 <0.0025 9.8 140 590 Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laborator anal tical method shown in parentheses. Concentrations are reported in milli rams per kilo ram m /k . Concentrations are reported to the laborator method detection limits.Only those compounds detected in at least one sample are shown in the table above. Bold values indicate compound exceed the Protection of Groundwater PSRG, but were below the Residential PSRG.VOCs = volatile organic compounds; ft bgs = feet below ground surface; NE = not establishedJ = Compound was detected at a concentration above the laboratory method detection limits, but below the laboratory reporting limits resulting in a laboratory estimated concentration. C9 = Common laborator contaminant. B = Compound was detected in the laborator method blank. Building 4 - Excavation E - Eastern and Western Sidewalls mg/kg Screening Criteria Protection of Groundwater PSRGs (1) Residential PSRGs (1) Industrial/ Commercial PSRGs (1) https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/28/2023 Table 5 (Page 3 of 5) Hart & Hickman, PC Table 5 Summary of Post-Excavation Confirmation Soil Samples for Excavation E Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXE-B-1N EXE-B-2N EXE-B-3N EXE-B-4N EXE-B-5N EXE-B-6N-2 EXE-B-7N-2 EXE-B-8N EXE-B-2S EXE-B-2S-2 EXE-B-3S EXE-B-3S-2 Depth (ft bgs)5 5 5 5 5 7 7 7 5 5 5 5 Sample Date 2/17/2023 2/8/2023 2/8/2023 2/8/2023 2/8/2023 2/10/2023 2/14/2023 2/14/2023 2/8/2023 2/17/2023 2/9/2023 2/17/2023 Units VOCs (8260D) Acetone <0.0384 <0.0385 <0.0381 0.107 J <0.0356 <0.0539 <0.0408 <0.0424 0.0434 J <0.0360 <0.0447 <0.0398 25 14,000 210,000 Bromomethane <0.0185 <0.0186 <0.0184 <0.0241 <0.0172 <0.0260 <0.0197 <0.0205 <0.0183 <0.0174 <0.0216 <0.0192 0.05 1.4 6.4 tert-Butylbenzene <0.0021 <0.0021 <0.0021 <0.0028 <0.0020 <0.0030 <0.0023 <0.0023 <0.0021 <0.0020 <0.0025 <0.0022 3.1 1,600 23,000 Chloromethane <0.0050 <0.0050 <0.0050 <0.0065 <0.0047 0.0154 J <0.0053 <0.0055 <0.0050 <0.0047 0.0130 J <0.0052 0.015 23 99 2-Chlorotoluene <0.0021 <0.0021 <0.0021 <0.0028 <0.0020 <0.0030 <0.0023 <0.0023 <0.0021 <0.0020 <0.0025 <0.0022 2.0 310 4,700 cis-1,2-Dichloroethene <0.0020 0.531 0.0859 0.0392 0.0331 <0.0029 <0.0022 <0.0023 0.273 <0.0019 0.0902 <0.0021 0.41 13 78 Diisopropyl ether <0.0016 <0.0016 <0.0016 <0.0021 <0.0015 <0.0023 <0.0017 <0.0018 <0.0016 <0.0015 <0.0019 <0.0017 0.36 480 2,000 Ethylbenzene <0.0028 <0.0028 <0.0028 <0.0036 <0.0026 <0.0039 <0.0030 <0.0031 <0.0028 <0.0026 <0.0032 <0.0029 13 6.1 27 p-Isopropyltoluene <0.0029 <0.0030 <0.0029 <0.0038 <0.0027 <0.0041 <0.0031 <0.0032 <0.0029 <0.0028 <0.0034 <0.0030 NE NE NE Methyl-tert-butyl ether <0.0022 <0.0022 <0.0022 <0.0029 <0.0021 0.0135 <0.0024 <0.0025 0.0083 <0.0021 <0.0026 <0.0023 0.09 49 220 Methylene Chloride <0.0164 <0.0164 <0.0163 <0.0213 <0.0152 0.0659 C9 0.0306 C9,B 0.0456 C9,B 0.0688 C9 <0.0154 0.303 C9 <0.0170 0.025 58 650 n-Propylbenzene <0.0021 <0.0021 <0.0021 <0.0028 <0.0020 <0.0030 <0.0023 <0.0023 <0.0021 <0.0020 <0.0025 <0.0022 2.6 780 5,100 Tetrachloroethene <0.0019 <0.0019 <0.0019 <0.0025 <0.0018 <0.0027 <0.0020 <0.0021 <0.0019 <0.0018 <0.0022 <0.0020 0.0063 17 82 Toluene 0.0043 J <0.0041 <0.0041 <0.0054 <0.0038 <0.0058 <0.0044 <0.0046 <0.0041 <0.0039 <0.0048 <0.0043 8.3 990 9,700 Trichloroethene <0.0048 <0.0048 <0.0048 <0.0063 <0.0045 <0.0068 <0.0051 <0.0053 <0.0048 <0.0045 <0.0056 <0.0050 0.021 0.87 4.0 1,2,4-Trimethylbenzene <0.0036 <0.0036 <0.0035 <0.0046 <0.0033 <0.0050 <0.0038 <0.0039 <0.0035 0.0038 J <0.0041 <0.0037 12 63 370 1,3,5-Trimethylbenzene <0.0020 <0.0020 <0.0020 <0.0026 <0.0019 <0.0028 <0.0021 <0.0022 <0.0020 <0.0019 <0.0023 <0.0021 11 56 320 Xylene (Total)<0.0034 <0.0034 <0.0034 <0.0044 <0.0032 <0.0048 <0.0036 <0.0038 <0.0034 0.0048 J <0.0040 <0.0035 9.9 120 530 m&p-Xylene <0.0041 <0.0041 <0.0041 <0.0053 <0.0038 <0.0057 <0.0044 <0.0045 <0.0040 0.0048 J <0.0048 <0.0042 9.8 120 500 o-Xylene <0.0026 <0.0027 <0.0026 <0.0034 <0.0024 <0.0037 <0.0028 <0.0029 <0.0026 <0.0025 <0.0031 <0.0027 9.8 140 590 Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laborator anal tical method shown in parentheses. Concentrations are reported in milli rams per kilo ram m /k . Concentrations are reported to the laborator method detection limits.Only those compounds detected in at least one sample are shown in the table above. Bold values indicate compound exceed the Protection of Groundwater PSRG, but were below the Residential PSRG.VOCs = volatile organic compounds; ft bgs = feet below ground surface; NE = not establishedJ = Compound was detected at a concentration above the laboratory method detection limits, but below the laboratory reporting limits resulting in a laboratory estimated concentration. C9 = Common laborator contaminant. B = Compound was detected in the laborator method blank. mg/kg Building 4 - Excavation E - Base Screening Criteria Protection of Groundwater PSRGs (1) Residential PSRGs (1) Industrial/ Commercial PSRGs (1) https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/28/2023 Table 5 (Page 4 of 5) Hart & Hickman, PC Table 5 Summary of Post-Excavation Confirmation Soil Samples for Excavation E Harrelson Ford Charlotte, North Carolina H&H Job No. ACO-002 Location Sample ID EXE-B-4S EXE-B-4S-2 EXE-B-5S EXE-B-5S-2 EXE-B-6S EXE-B-7S EXE-B-7S-2 EXE-B-8S EXE-B-8S-3 EXE-B-1W EXE-B-2W EXE-B-3W Depth (ft bgs)5 5 5 5 5 5 5 5 7 5 5 5 Sample Date 2/9/2023 2/17/2023 2/6/2023 2/8/2023 2/6/2023 2/6/2023 2/13/2023 2/13/2023 2/14/2023 2/7/2023 2/7/2023 2/17/2023 Units VOCs (8260D) Acetone <0.0447 <0.0408 <0.0363 <0.0358 <0.137 <0.0471 <0.0403 <0.0400 <0.0348 <0.0423 0.0745 J <0.0375 25 14,000 210,000 Bromomethane <0.0216 <0.0197 <0.0175 <0.0173 <0.0663 <0.0227 <0.0195 <0.0193 <0.0168 <0.0204 <0.0192 <0.0181 0.05 1.4 6.4 tert-Butylbenzene <0.0025 <0.0023 <0.0020 <0.0020 <0.0076 <0.0026 <0.0022 <0.0022 <0.0019 <0.0023 <0.0022 <0.0021 3.1 1,600 23,000 Chloromethane <0.0058 <0.0053 <0.0048 <0.0047 10.9 <0.0062 0.0068 J <0.0052 <0.0046 <0.0055 <0.0052 <0.0049 0.015 23 99 2-Chlorotoluene <0.0025 <0.0022 <0.0020 <0.0020 <0.0076 <0.0026 <0.0022 <0.0022 <0.0019 <0.0023 <0.0022 <0.0021 2.0 310 4,700 cis-1,2-Dichloroethene 0.0227 <0.0022 <0.0019 0.0058 <0.0073 0.0134 0.201 <0.0021 <0.0019 0.647 0.0789 <0.0020 0.41 13 78 Diisopropyl ether <0.0019 <0.0017 <0.0015 <0.0015 <0.0058 <0.0020 <0.0017 <0.0017 <0.0015 <0.0018 <0.0017 <0.0016 0.36 480 2,000 Ethylbenzene <0.0032 <0.0030 <0.0026 <0.0026 <0.010 <0.0034 <0.0029 <0.0029 <0.0025 <0.0031 <0.0029 <0.0027 13 6.1 27 p-Isopropyltoluene <0.0034 <0.0031 <0.0028 <0.0027 <0.0105 <0.0036 <0.0031 <0.0031 <0.0027 <0.0032 <0.0030 <0.0029 NE NE NE Methyl-tert-butyl ether <0.0026 <0.0024 <0.0021 <0.0021 <0.0080 <0.0027 <0.0023 <0.0023 <0.0020 <0.0025 0.0125 <0.0022 0.09 49 220 Methylene Chloride <0.0191 <0.0174 0.183 C9,B 0.092 C9 0.121 C9 0.108 C9,B 0.0273 C9 <0.0171 <0.0148 <0.0181 0.0563 C9 <0.0160 0.025 58 650 n-Propylbenzene <0.0025 <0.0023 <0.0020 <0.0020 <0.0076 <0.0026 <0.0022 <0.0022 <0.0019 <0.0023 <0.0022 <0.0021 2.6 780 5,100 Tetrachloroethene <0.0022 <0.0020 <0.0018 <0.0018 <0.0068 <0.0023 <0.0020 <0.0020 <0.0017 <0.0021 <0.0020 <0.0018 0.0063 17 82 Toluene <0.0048 <0.0044 <0.0039 <0.0038 <0.0148 <0.0051 <0.0043 <0.0043 <0.0037 <0.0045 <0.0043 0.0041 J 8.3 990 9,700 Trichloroethene <0.0056 <0.0051 <0.0046 <0.0045 <0.0172 <0.0059 <0.0051 <0.0050 <0.0044 <0.0053 <0.0050 <0.0047 0.021 0.87 4.0 1,2,4-Trimethylbenzene <0.0041 0.0038 J <0.0034 <0.0033 <0.0127 <0.0044 <0.0037 <0.0037 <0.0032 <0.0039 <0.0037 0.0042 J 12 63 370 1,3,5-Trimethylbenzene <0.0023 <0.0021 <0.0019 <0.0019 <0.0072 <0.0025 <0.0021 <0.0021 <0.0018 <0.0022 <0.0021 <0.0020 11 56 320 Xylene (Total)<0.0040 0.0127 J <0.0032 0.0041 J <0.0122 <0.0042 <0.0036 <0.0036 <0.0031 <0.0038 <0.0035 0.0079 J 9.9 120 530 m&p-Xylene <0.0048 0.0074 J <0.0039 0.0041 J <0.0146 <0.0050 <0.0043 <0.0043 <0.0037 <0.0045 <0.0042 0.0079 J 9.8 120 500 o-Xylene <0.0031 0.0052 J <0.0025 <0.0025 <0.0095 <0.0032 <0.0028 <0.0028 <0.0024 <0.0029 <0.0027 <0.0026 9.8 140 590 Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023. Laborator anal tical method shown in parentheses. Concentrations are reported in milli rams per kilo ram m /k . Concentrations are reported to the laborator method detection limits.Only those compounds detected in at least one sample are shown in the table above. Bold values indicate compound exceed the Protection of Groundwater PSRG, but were below the Residential PSRG.VOCs = volatile organic compounds; ft bgs = feet below ground surface; NE = not establishedJ = Compound was detected at a concentration above the laboratory method detection limits, but below the laboratory reporting limits resulting in a laboratory estimated concentration. C9 = Common laborator contaminant. B = Compound was detected in the laborator method blank. mg/kg Screening Criteria Protection of Groundwater PSRGs (1) Residential PSRGs (1) Industrial/ Commercial PSRGs (1) Building 4 - Excavation E - Base https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Ardent ‐ ACO/ACO.002 ‐ 6500 South Boulevard/Brownfields/Soil Removal/Tables/Harrelson Ford ‐ Soil Removal Data Tables 3/28/2023 Table 5 (Page 5 of 5) Hart & Hickman, PC APPENDIX B Disposal Documentation 333630- Centurion Development Group Ticket # Contract Truck # MaterialRate Tons Total 12/13/2023 2014797 5010230210-1 KD9 SW-CONT SOIL-ALT DAILY COVER 20.50 TN 12/13/2023 2014802 5010230210-1 QB-5 SW-CONT SOIL-ALT DAILY COVER 19.51 TN 12/13/2023 2014809 5010230210-1 M011 SW-CONT SOIL-ALT DAILY COVER 20.34 TN 12/13/2023 2014818 5010230210-1 QB-3 SW-CONT SOIL-ALT DAILY COVER 24.33 TN 12/13/2023 2014837 5010230210-1 m006 SW-CONT SOIL-ALT DAILY COVER 22.93 TN 12/13/2023 2014858 5010230210-1 m009 SW-CONT SOIL-ALT DAILY COVER 20.29 TN 12/13/2023 2014870 5010230210-1 KD9 SW-CONT SOIL-ALT DAILY COVER 17.80 TN 12/13/2023 2014873 5010230210-1 QB-5 SW-CONT SOIL-ALT DAILY COVER 18.42 TN 12/13/2023 2014891 5010230210-1 M011 SW-CONT SOIL-ALT DAILY COVER 22.03 TN 12/13/2023 2014893 5010230210-1 QB-3 SW-CONT SOIL-ALT DAILY COVER 23.68 TN 12/13/2023 2014906 5010230210-1 m006 SW-CONT SOIL-ALT DAILY COVER 23.49 TN 12/13/2023 2014933 5010230210-1 m009 SW-CONT SOIL-ALT DAILY COVER 19.15 TN Tickets Reported: 12 Customer Totals: Material Summary Count BillingQuantity MaterialTotal Total Inbound Outbound VI - SW-CONT SOIL- ALT DAILY COVER TN 0.00 0.00 0.00 252.47 TN Cash Totals: Invoice Totals: Items Reported: 12 astonke 12/14/2023 8:19 AM APPENDIX C Laboratory Analytical Reports   Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.   12/18/2023 Hanley Environmental, PLLC Nick Hotzelt 323 Manning Drive Charlotte, NC, 28209 Ref: Analytical Testing Lab Report Number: 23-347-0033 Client Project Description: Harrelson Ford Dear Nick Hotzelt: Waypoint Analytical, LLC (Charlotte) received sample(s) on 12/13/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Page 1 of 58 Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date 07/31/202437735State ProgramNorth Carolina 12/31/2023402State ProgramNorth Carolina 07/31/202499012State ProgramSouth Carolina 12/31/202399012State ProgramSouth Carolina Page 1 of 1 00016/23-347-0033 Page 2 of 58 Report Number: Sample Summary Table Client Project Description: 23-347-0033 Harrelson Ford Lab No Client Sample ID Matrix Date Collected Date Received 12/13/2023 09:30Solids 91845 OEX-E3(A)-1 12/13/2023 15:30 12/13/2023 09:35Solids 91846 OEX-E3(A)-2 12/13/2023 15:30 12/13/2023 09:40Solids 91847 OEX-E3(B)12/13/2023 15:30 12/13/2023 09:45Solids 91848 OEX-E3(C)-1 12/13/2023 15:30 12/13/2023 09:50Solids 91849 OEX-E3(C)-2 12/13/2023 15:30 12/13/2023 10:20Solids 91850 OEX-E2(A)12/13/2023 15:30 12/13/2023 10:25Solids 91851 OEX-E2(B)12/13/2023 15:30 12/13/2023 10:30Solids 91852 OEX-E2(C)12/13/2023 15:30 12/13/2023 10:45Solids 91853 OEX-E1(A)12/13/2023 15:30 12/13/2023 10:50Solids 91854 OEX-E1(B)12/13/2023 15:30 12/13/2023 10:55Solids 91855 OEX-E1(C)12/13/2023 15:30 12/13/2023 11:45Solids 91856 OEX-D1(A)12/13/2023 15:30 12/13/2023 11:50Solids 91857 OEX-D1(B)-1 12/13/2023 15:30 12/13/2023 12:00Solids 91858 OEX-D1(B)-2 12/13/2023 15:30 12/13/2023 11:55Solids 91859 OEX-D1(C)12/13/2023 15:30 12/13/2023 13:30Solids 91860 OEX-B1(A)-1 12/13/2023 15:30 12/13/2023 13:35Solids 91861 OEX-B1(A)-2 12/13/2023 15:30 12/13/2023 13:40Solids 91862 OEX-B1(B)-1 12/13/2023 15:30 12/13/2023 13:45Solids 91863 OEX-B1(B)-2 12/13/2023 15:30 12/13/2023 13:50Solids 91864 OEX-B1(C)-1 12/13/2023 15:30 12/13/2023 13:55Solids 91865 OEX-B1(C)-2 12/13/2023 15:30 12/13/2023Solids 91866 OEX-DUP 12/13/2023 15:30 Page 3 of 58 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-347-0033 Report Limit Project:Harrelson Ford V 91845OEX-E3(A)-1 19.3 12/14/2023 16:00SW-DRYWT Moisture % V 91846OEX-E3(A)-2 11.9 12/14/2023 16:00SW-DRYWT Moisture % V 91847OEX-E3(B) 16.8 12/14/2023 16:00SW-DRYWT Moisture % V 91848OEX-E3(C)-1 19.8 12/14/2023 16:00SW-DRYWT Moisture % V 91849OEX-E3(C)-2 25.7 12/14/2023 16:00SW-DRYWT Moisture % V 91850OEX-E2(A) 24.4 12/14/2023 16:00SW-DRYWT Moisture % V 91851OEX-E2(B) 13.6 12/14/2023 16:00SW-DRYWT Moisture % V 91852OEX-E2(C) J0.003 12/14/2023 14:188260DTetrachloroethenemg/Kg - dry 0.001 27.8 12/14/2023 16:00SW-DRYWT Moisture % V 91853OEX-E1(A) 18.7 12/14/2023 16:00SW-DRYWT Moisture % V 91854OEX-E1(B) 16.0 12/14/2023 16:00SW-DRYWT Moisture % V 91855OEX-E1(C) 20.1 12/14/2023 16:00SW-DRYWT Moisture % V 91856OEX-D1(A) 23.6 12/14/2023 16:00SW-DRYWT Moisture % V 91857OEX-D1(B)-1 13.5 12/14/2023 16:00SW-DRYWT Moisture % V 91858OEX-D1(B)-2 15.3 12/14/2023 16:00SW-DRYWT Moisture % Page 4 of 58 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-347-0033 Report Limit Project:Harrelson Ford V 91859OEX-D1(C) 12.0 12/14/2023 16:44SW-DRYWT Moisture % V 91860OEX-B1(A)-1 14.3 12/14/2023 16:44SW-DRYWT Moisture % V 91861OEX-B1(A)-2 17.1 12/14/2023 16:44SW-DRYWT Moisture % V 91862OEX-B1(B)-1 12.5 12/14/2023 16:44SW-DRYWT Moisture % V 91863OEX-B1(B)-2 12.8 12/14/2023 16:44SW-DRYWT Moisture % V 91864OEX-B1(C)-1 15.9 12/14/2023 16:44SW-DRYWT Moisture % V 91865OEX-B1(C)-2 16.9 12/14/2023 16:44SW-DRYWT Moisture % V 91866OEX-DUP 14.4 12/14/2023 16:44SW-DRYWT Moisture % Page 5 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E3(A)-1 91845 Matrix: 12/13/2023 9:30 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 19.3 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 6 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E3(A)-1 91845 Matrix: 12/13/2023 9:30 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/14/23 11:09 V41397TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/14/23 11:09 V41397TBL Surrogate: 4-Bromofluorobenzene 96.4 Limits: 70-130%12/14/23 11:091 TBL V41397 Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/14/23 11:091 TBL V41397 Surrogate: Toluene-d8 97.2 Limits: 76-129%12/14/23 11:091 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 7 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E3(A)-2 91846 Matrix: 12/13/2023 9:35 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 11.9 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 8 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E3(A)-2 91846 Matrix: 12/13/2023 9:35 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/14/23 11:36 V41397TBL <0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/14/23 11:36 V41397TBL Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%12/14/23 11:361 TBL V41397 Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/14/23 11:361 TBL V41397 Surrogate: Toluene-d8 97.8 Limits: 76-129%12/14/23 11:361 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 9 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E3(B) 91847 Matrix: 12/13/2023 9:40 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 16.8 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 10 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E3(B) 91847 Matrix: 12/13/2023 9:40 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/14/23 12:03 V41397TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/14/23 12:03 V41397TBL Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%12/14/23 12:031 TBL V41397 Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/14/23 12:031 TBL V41397 Surrogate: Toluene-d8 98.0 Limits: 76-129%12/14/23 12:031 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 11 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E3(C)-1 91848 Matrix: 12/13/2023 9:45 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 19.8 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 12 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E3(C)-1 91848 Matrix: 12/13/2023 9:45 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/14/23 12:30 V41397TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/14/23 12:30 V41397TBL Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%12/14/23 12:301 TBL V41397 Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/14/23 12:301 TBL V41397 Surrogate: Toluene-d8 97.0 Limits: 76-129%12/14/23 12:301 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 13 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E3(C)-2 91849 Matrix: 12/13/2023 9:50 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 25.7 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 14 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E3(C)-2 91849 Matrix: 12/13/2023 9:50 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/14/23 12:57 V41397TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/14/23 12:57 V41397TBL Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%12/14/23 12:571 TBL V41397 Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/14/23 12:571 TBL V41397 Surrogate: Toluene-d8 97.6 Limits: 76-129%12/14/23 12:571 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 15 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E2(A) 91850 Matrix: 12/13/2023 10:20 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 24.4 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 16 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E2(A) 91850 Matrix: 12/13/2023 10:20 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/14/23 13:25 V41397TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/14/23 13:25 V41397TBL Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%12/14/23 13:251 TBL V41397 Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/14/23 13:251 TBL V41397 Surrogate: Toluene-d8 98.2 Limits: 76-129%12/14/23 13:251 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 17 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E2(B) 91851 Matrix: 12/13/2023 10:25 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 13.6 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 18 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E2(B) 91851 Matrix: 12/13/2023 10:25 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/14/23 13:52 V41397TBL <0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/14/23 13:52 V41397TBL Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%12/14/23 13:521 TBL V41397 Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/14/23 13:521 TBL V41397 Surrogate: Toluene-d8 98.4 Limits: 76-129%12/14/23 13:521 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 19 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E2(C) 91852 Matrix: 12/13/2023 10:30 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 27.8 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 20 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E2(C) 91852 Matrix: 12/13/2023 10:30 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 0.003 J mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/14/23 14:18 V41397TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/14/23 14:18 V41397TBL Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%12/14/23 14:181 TBL V41397 Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/14/23 14:181 TBL V41397 Surrogate: Toluene-d8 98.2 Limits: 76-129%12/14/23 14:181 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 21 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E1(A) 91853 Matrix: 12/13/2023 10:45 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 18.7 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 22 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E1(A) 91853 Matrix: 12/13/2023 10:45 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/14/23 14:46 V41397TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/14/23 14:46 V41397TBL Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%12/14/23 14:461 TBL V41397 Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/14/23 14:461 TBL V41397 Surrogate: Toluene-d8 97.0 Limits: 76-129%12/14/23 14:461 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 23 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E1(B) 91854 Matrix: 12/13/2023 10:50 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 16.0 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 24 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E1(B) 91854 Matrix: 12/13/2023 10:50 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/14/23 15:12 V41397TBL <0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/14/23 15:12 V41397TBL Surrogate: 4-Bromofluorobenzene 98.2 Limits: 70-130%12/14/23 15:121 TBL V41397 Surrogate: Dibromofluoromethane 105 Limits: 84-123%12/14/23 15:121 TBL V41397 Surrogate: Toluene-d8 97.6 Limits: 76-129%12/14/23 15:121 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 25 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E1(C) 91855 Matrix: 12/13/2023 10:55 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 20.1 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 26 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-E1(C) 91855 Matrix: 12/13/2023 10:55 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/14/23 15:39 V41397TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/14/23 15:39 V41397TBL Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%12/14/23 15:391 TBL V41397 Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/14/23 15:391 TBL V41397 Surrogate: Toluene-d8 98.2 Limits: 76-129%12/14/23 15:391 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 27 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-D1(A) 91856 Matrix: 12/13/2023 11:45 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 23.6 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 28 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-D1(A) 91856 Matrix: 12/13/2023 11:45 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/14/23 16:07 V41397TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/14/23 16:07 V41397TBL Surrogate: 4-Bromofluorobenzene 98.2 Limits: 70-130%12/14/23 16:071 TBL V41397 Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/14/23 16:071 TBL V41397 Surrogate: Toluene-d8 99.0 Limits: 76-129%12/14/23 16:071 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 29 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-D1(B)-1 91857 Matrix: 12/13/2023 11:50 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 13.5 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 30 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-D1(B)-1 91857 Matrix: 12/13/2023 11:50 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/14/23 16:34 V41397TBL <0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/14/23 16:34 V41397TBL Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%12/14/23 16:341 TBL V41397 Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/14/23 16:341 TBL V41397 Surrogate: Toluene-d8 97.4 Limits: 76-129%12/14/23 16:341 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 31 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-D1(B)-2 91858 Matrix: 12/13/2023 12:00 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 15.3 %Moisture 1 12/14/23 16:00 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 32 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-D1(B)-2 91858 Matrix: 12/13/2023 12:00 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/14/23 17:01 V41397TBL <0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/14/23 17:01 V41397TBL Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%12/14/23 17:011 TBL V41397 Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/14/23 17:011 TBL V41397 Surrogate: Toluene-d8 97.4 Limits: 76-129%12/14/23 17:011 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 33 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-D1(C) 91859 Matrix: 12/13/2023 11:55 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 12.0 %Moisture 1 12/14/23 16:44 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 34 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-D1(C) 91859 Matrix: 12/13/2023 11:55 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/14/23 17:29 V41397TBL <0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/14/23 17:29 V41397TBL Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%12/14/23 17:291 TBL V41397 Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/14/23 17:291 TBL V41397 Surrogate: Toluene-d8 98.8 Limits: 76-129%12/14/23 17:291 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 35 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(A)-1 91860 Matrix: 12/13/2023 13:30 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 14.3 %Moisture 1 12/14/23 16:44 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 36 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(A)-1 91860 Matrix: 12/13/2023 13:30 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/14/23 17:57 V41397TBL <0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/14/23 17:57 V41397TBL Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%12/14/23 17:571 TBL V41397 Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/14/23 17:571 TBL V41397 Surrogate: Toluene-d8 98.2 Limits: 76-129%12/14/23 17:571 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 37 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(A)-2 91861 Matrix: 12/13/2023 13:35 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 17.1 %Moisture 1 12/14/23 16:44 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 38 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(A)-2 91861 Matrix: 12/13/2023 13:35 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41406 12/16/23 08:00 <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/15/23 10:42 V41407TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/15/23 10:42 V41407TBL Surrogate: 4-Bromofluorobenzene 97.6 Limits: 70-130%12/15/23 10:421 TBL V41407 Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/15/23 10:421 TBL V41407 Surrogate: Toluene-d8 97.4 Limits: 76-129%12/15/23 10:421 TBL V41407 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 39 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(B)-1 91862 Matrix: 12/13/2023 13:40 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 12.5 %Moisture 1 12/14/23 16:44 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 40 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(B)-1 91862 Matrix: 12/13/2023 13:40 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/14/23 18:51 V41397TBL <0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/14/23 18:51 V41397TBL Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%12/14/23 18:511 TBL V41397 Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/14/23 18:511 TBL V41397 Surrogate: Toluene-d8 97.0 Limits: 76-129%12/14/23 18:511 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 41 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(B)-2 91863 Matrix: 12/13/2023 13:45 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 12.8 %Moisture 1 12/14/23 16:44 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 42 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(B)-2 91863 Matrix: 12/13/2023 13:45 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/14/23 19:18 V41397TBL <0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/14/23 19:18 V41397TBL Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%12/14/23 19:181 TBL V41397 Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/14/23 19:181 TBL V41397 Surrogate: Toluene-d8 96.6 Limits: 76-129%12/14/23 19:181 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 43 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(C)-1 91864 Matrix: 12/13/2023 13:50 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 15.9 %Moisture 1 12/14/23 16:44 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 44 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(C)-1 91864 Matrix: 12/13/2023 13:50 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41396 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/14/23 19:44 V41397TBL <0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/14/23 19:44 V41397TBL Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/14/23 19:441 TBL V41397 Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/14/23 19:441 TBL V41397 Surrogate: Toluene-d8 97.4 Limits: 76-129%12/14/23 19:441 TBL V41397 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 45 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(C)-2 91865 Matrix: 12/13/2023 13:55 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 16.9 %Moisture 1 12/14/23 16:44 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 46 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-B1(C)-2 91865 Matrix: 12/13/2023 13:55 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41398 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/14/23 20:10 V41399TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/14/23 20:10 V41399TBL Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%12/14/23 20:101 TBL V41399 Surrogate: Dibromofluoromethane 105 Limits: 84-123%12/14/23 20:101 TBL V41399 Surrogate: Toluene-d8 98.8 Limits: 76-129%12/14/23 20:101 TBL V41399 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 47 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-DUP 91866 Matrix: 12/13/2023 0:00 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 14.4 %Moisture 1 12/14/23 16:44 SW-DRYWTPEB Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 48 of 58 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 23-347-0033 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Received : 12/13/2023 Harrelson Ford Report Date : 12/18/2023 Sample ID : Lab No : Sampled:OEX-DUP 91866 Matrix: 12/13/2023 0:00 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V41398 12/14/23 08:00 <0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/14/23 20:37 V41399TBL <0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/14/23 20:37 V41399TBL Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%12/14/23 20:371 TBL V41399 Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/14/23 20:371 TBL V41399 Surrogate: Toluene-d8 97.6 Limits: 76-129%12/14/23 20:371 TBL V41399 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 49 of 58 Quality Control Data 23-347-0033Report No: Project Description: Client ID:Hanley Environmental, PLLC Harrelson Ford QC Prep Batch Method: Volatile Organic Compounds - GC/MS 8260D V41397QC Analytical Batch(es): Analysis Method: Analysis Description: 5035 QC Prep:V41396 Associated Lab Samples: 91845, 91846, 91847, 91848, 91849, 91850, 91851, 91852, 91853, 91854, 91855, 91856, 91857, 91858, 91859, 91860, 91862, 91863, 91864 LRB-V41396 Matrix: SOLLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 12/14/23 10:150.0050.0009<0.0009mg/KgTetrachloroethene 12/14/23 10:150.0050.0009<0.0009mg/KgTrichloroethene 12/14/23 10:154-Bromofluorobenzene (S)99.0 70-130 12/14/23 10:15Dibromofluoromethane (S)100 84-123 12/14/23 10:15Toluene-d8 (S)99.4 76-129 LCS-V41396 LCSD-V41396Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 0.044 89.892.00.0460.050mg/KgTetrachloroethene 68-130 2.4 20 0.045 91.093.20.0460.050mg/KgTrichloroethene 75-133 2.3 20 98.298.24-Bromofluorobenzene (S)70-130 101100Dibromofluoromethane (S)84-123 101100Toluene-d8 (S)76-129 Page 1 of 5Date:12/18/2023 04:38 PM Page 50 of 58 Quality Control Data 23-347-0033Report No: Project Description: Client ID:Hanley Environmental, PLLC Harrelson Ford QC Prep Batch Method: Volatile Organic Compounds - GC/MS 8260D V41399QC Analytical Batch(es): Analysis Method: Analysis Description: 5035 QC Prep:V41398 Associated Lab Samples: 91865, 91866 LRB-V41398 Matrix: SOLLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 12/14/23 10:150.0050.0009<0.0009mg/KgTetrachloroethene 12/14/23 10:150.0050.0009<0.0009mg/KgTrichloroethene 12/14/23 10:154-Bromofluorobenzene (S)99.0 70-130 12/14/23 10:15Dibromofluoromethane (S)100 84-123 12/14/23 10:15Toluene-d8 (S)99.4 76-129 LCS-V41398 LCSD-V41398Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 0.044 89.892.00.0460.050mg/KgTetrachloroethene 68-130 2.4 20 0.045 91.093.20.0460.050mg/KgTrichloroethene 75-133 2.3 20 98.298.24-Bromofluorobenzene (S)70-130 101100Dibromofluoromethane (S)84-123 101100Toluene-d8 (S)76-129 Page 2 of 5Date:12/18/2023 04:38 PM Page 51 of 58 Quality Control Data 23-347-0033Report No: Project Description: Client ID:Hanley Environmental, PLLC Harrelson Ford QC Prep Batch Method: Volatile Organic Compounds - GC/MS 8260D V41407QC Analytical Batch(es): Analysis Method: Analysis Description: 5035 QC Prep:V41406 Associated Lab Samples: 91861 LRB-V41406 Matrix: SOLLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 12/15/23 10:150.0050.0009<0.0009mg/KgTetrachloroethene 12/15/23 10:150.0050.0009<0.0009mg/KgTrichloroethene 12/15/23 10:154-Bromofluorobenzene (S)101 70-130 12/15/23 10:15Dibromofluoromethane (S)99.6 84-123 12/15/23 10:15Toluene-d8 (S)97.6 76-129 LCS-V41406 LCSD-V41406Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 0.041 82.890.00.0450.050mg/KgTetrachloroethene 68-130 8.3 20 0.043 87.688.80.0440.050mg/KgTrichloroethene 75-133 1.3 20 97.698.24-Bromofluorobenzene (S)70-130 100100Dibromofluoromethane (S)84-123 101100Toluene-d8 (S)76-129 Page 3 of 5Date:12/18/2023 04:38 PM Page 52 of 58 Quality Control Data 23-347-0033Report No: Project Description: Client ID:Hanley Environmental, PLLC Harrelson Ford Dry Weight Determination SW-DRYWT V41316QC Analytical Batch: Analysis Method: Analysis Description: V 91854-DUPDuplicate Max RPD Parameter AnalyzedRPDDUP Result Result Units 20.0 12/14/23 16:009.517.616.0%Moisture V 91872-DUPDuplicate Max RPD Parameter AnalyzedRPDDUP Result Result Units 20.0 12/14/23 16:001.920.420.8%Moisture Page 4 of 5Date:12/18/2023 04:38 PM Page 53 of 58 Quality Control Data 23-347-0033Report No: Project Description: Client ID:Hanley Environmental, PLLC Harrelson Ford Dry Weight Determination SW-DRYWT V41318QC Analytical Batch: Analysis Method: Analysis Description: V 91925-DUPDuplicate Max RPD Parameter AnalyzedRPDDUP Result Result Units 20.0 12/14/23 16:441.232.833.2%Moisture V 91926-DUPDuplicate Max RPD Parameter AnalyzedRPDDUP Result Result Units 20.0 12/14/23 16:440.632.332.5%Moisture Page 5 of 5Date:12/18/2023 04:38 PM Page 54 of 58 Fed Ex UPS US Postal Client Lab Courier Other : Shipment Receipt Form Customer Number: Customer Name: Report Number:23-347-0033 Hanley Environmental, PLLC 00293 Shipping Method Shipping container/cooler uncompromised? Thermometer ID:IRT15 1.4C Chain of Custody (COC) present?Yes No Yes No Not Present Yes No Not Present Yes No COC agrees with sample label(s)? Yes No COC properly completed Samples in proper containers? Sample containers intact? Sufficient sample volume for indicated test(s)? All samples received within holding time? Cooler temperature in compliance? Yes No Yes No Yes No Yes No Yes No Yes NoCooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Yes No N/A Yes No N/A Yes No N/ASoil VOA method 5035 – compliance criteria met Water - Sample containers properly preserved Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs ü Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü High concentration container (48 hr) Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Number of coolers/boxes received Yes No 1 Signature:Angelo Norvell Date & Time:12/13/2023 18:48:29 Special precautions or instructions included? Comments: Page 55 of 58 Pa g e 5 6 o f 5 8 Pa g e 5 7 o f 5 8 Pa g e 5 8 o f 5 8 DIVIDER PAGE INTENTIONALLY LEFT BLANK   Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.   1/24/2024 Hanley Environmental, PLLC Nick Hotzelt 323 Manning Drive Charlotte, NC, 28209 Ref: Analytical Testing Lab Report Number: 24-011-0012 Client Project Description: Harrelson Ford Project #PJ23030 Dear Nick Hotzelt: Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/11/2024 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Page 1 of 59 Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date 07/31/202437735State ProgramNorth Carolina 12/31/2024402State ProgramNorth Carolina 07/31/202499012State ProgramSouth Carolina 12/31/202399012State ProgramSouth Carolina Page 1 of 1 00016/24-011-0012 Page 2 of 59 Report Number: Sample Summary Table Client Project Description: 24-011-0012 Harrelson Ford Project #PJ23030 Lab No Client Sample ID Matrix Date Collected Date Received 01/11/2024 10:26Air 93794 BF-SG-1 01/11/2024 13:54 01/11/2024Air 93795 BF-SG-DUP 01/11/2024 13:54 01/11/2024 10:42Air 93796 BF-SG-2 01/11/2024 13:54 01/11/2024 10:58Air 93797 BF-SG-3 01/11/2024 13:54 01/11/2024 11:14Air 93798 BF-SG-4 01/11/2024 13:54 01/11/2024 11:30Air 93799 BF-SG-5 01/11/2024 13:54 01/11/2024 12:30Air 93800 BF-SG-6 01/11/2024 13:54 01/11/2024 12:50Air 93801 BF-SG-7 01/11/2024 13:54 01/11/2024 13:06Air 93802 BF-SG-8 01/11/2024 13:54 01/11/2024 13:30Air 93803 BF-SG-9 01/11/2024 13:54 01/11/2024 12:00Air 93804 BF-SG-10 01/11/2024 13:54 01/11/2024 13:50Air 93805 BF-SG-11 01/11/2024 13:54 Page 3 of 59 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 24-011-0012 Report Limit Project:Harrelson Ford V 93794BF-SG-1 18.0 01/12/2024 13:09TO-15 Acetone µg/m3 0.202 75.8 01/12/2024 13:09TO-15 Benzene µg/m3 0.073 20.6 01/12/2024 13:09TO-15 Carbon Disulfide µg/m3 0.060 J0.893 01/12/2024 13:09TO-15 Carbon Tetrachloride µg/m3 0.155 J1.65 01/12/2024 13:09TO-15 Chloroform µg/m3 0.086 2.49 01/12/2024 13:09TO-15 Dichlorodifluoromethane µg/m3 0.134 J1.79 01/12/2024 13:09TO-15 1,1-Dichloroethane µg/m3 0.101 2.61 01/12/2024 13:09TO-15 1,1-Dichloroethene µg/m3 0.107 71.9 01/12/2024 13:09TO-15 cis-1,2-Dichloroethene µg/m3 0.095 2.34 01/12/2024 13:09TO-15 trans-1,2-Dichloroethene µg/m3 0.108 26.4 01/12/2024 13:09TO-15 Ethyl Acetate µg/m3 0.136 58.2 01/12/2024 13:09TO-15 Ethylbenzene µg/m3 0.106 7.23 01/12/2024 13:09TO-15 4-Ethyltoluene µg/m3 0.128 31.7 01/12/2024 13:09TO-15 Heptane µg/m3 0.143 17.0 01/12/2024 13:09TO-15 n-Hexane µg/m3 0.047 JB2.10 01/12/2024 13:09TO-15 Isopropyl Alcohol µg/m3 0.139 4.96 01/12/2024 13:09TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 26.2 01/12/2024 13:09TO-15 Methyl tert-butyl ether (MTBE)µg/m3 0.033 3.11 01/12/2024 13:09TO-15 4-Methyl-2-Pentanone µg/m3 0.121 3.75 01/12/2024 13:09TO-15 Methylene Chloride µg/m3 0.488 4.57 01/12/2024 13:09TO-15 Naphthalene µg/m3 0.183 3.62 01/12/2024 13:09TO-15 Propene µg/m3 0.242 J0.647 01/12/2024 13:09TO-15 Styrene µg/m3 0.124 106 01/12/2024 13:09TO-15 Tetrachloroethene µg/m3 0.181 17.0 01/12/2024 13:09TO-15 Tetrahydrofuran µg/m3 0.107 338 01/11/2024 22:11TO-15 Toluene µg/m3 1.80 117 01/12/2024 13:09TO-15 Trichloroethene µg/m3 0.199 J1.52 01/12/2024 13:09TO-15 Trichlorofluoromethane µg/m3 0.130 24.8 01/12/2024 13:09TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 6.81 01/12/2024 13:09TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 42.2 01/12/2024 13:09TO-15 o-Xylene µg/m3 0.157 134 01/12/2024 13:09TO-15 m,p-Xylene µg/m3 0.217 176 01/12/2024 13:09TO-15 Xylene (Total)µg/m3 0.157 V 93795BF-SG-DUP 21.7 01/12/2024 14:00TO-15 Acetone µg/m3 0.202 74.8 01/12/2024 14:00TO-15 Benzene µg/m3 0.073 Page 4 of 59 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 24-011-0012 Report Limit Project:Harrelson Ford V 93795BF-SG-DUP 18.1 01/12/2024 14:00TO-15 Carbon Disulfide µg/m3 0.060 J0.905 01/12/2024 14:00TO-15 Carbon Tetrachloride µg/m3 0.155 J1.70 01/12/2024 14:00TO-15 Chloroform µg/m3 0.086 J2.45 01/12/2024 14:00TO-15 Dichlorodifluoromethane µg/m3 0.134 J1.80 01/12/2024 14:00TO-15 1,1-Dichloroethane µg/m3 0.101 2.66 01/12/2024 14:00TO-15 1,1-Dichloroethene µg/m3 0.107 70.8 01/12/2024 14:00TO-15 cis-1,2-Dichloroethene µg/m3 0.095 2.36 01/12/2024 14:00TO-15 trans-1,2-Dichloroethene µg/m3 0.108 25.5 01/12/2024 14:00TO-15 Ethyl Acetate µg/m3 0.136 57.9 01/12/2024 14:00TO-15 Ethylbenzene µg/m3 0.106 7.31 01/12/2024 14:00TO-15 4-Ethyltoluene µg/m3 0.128 31.7 01/12/2024 14:00TO-15 Heptane µg/m3 0.143 16.9 01/12/2024 14:00TO-15 n-Hexane µg/m3 0.047 JB2.26 01/12/2024 14:00TO-15 Isopropyl Alcohol µg/m3 0.139 5.62 01/12/2024 14:00TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 26.2 01/12/2024 14:00TO-15 Methyl tert-butyl ether (MTBE)µg/m3 0.033 3.15 01/12/2024 14:00TO-15 4-Methyl-2-Pentanone µg/m3 0.121 3.62 01/12/2024 14:00TO-15 Methylene Chloride µg/m3 0.488 4.32 01/12/2024 14:00TO-15 Naphthalene µg/m3 0.183 3.67 01/12/2024 14:00TO-15 Propene µg/m3 0.242 J0.685 01/12/2024 14:00TO-15 Styrene µg/m3 0.124 104 01/12/2024 14:00TO-15 Tetrachloroethene µg/m3 0.181 23.5 01/12/2024 14:00TO-15 Tetrahydrofuran µg/m3 0.107 345 01/11/2024 22:47TO-15 Toluene µg/m3 1.80 115 01/12/2024 14:00TO-15 Trichloroethene µg/m3 0.199 J1.57 01/12/2024 14:00TO-15 Trichlorofluoromethane µg/m3 0.130 24.6 01/12/2024 14:00TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 6.78 01/12/2024 14:00TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 1.90 01/12/2024 14:00TO-15 Vinyl Chloride µg/m3 0.127 41.9 01/12/2024 14:00TO-15 o-Xylene µg/m3 0.157 135 01/12/2024 14:00TO-15 m,p-Xylene µg/m3 0.217 177 01/12/2024 14:00TO-15 Xylene (Total)µg/m3 0.157 V 93796BF-SG-2 24.6 01/12/2024 14:52TO-15 Acetone µg/m3 0.202 41.1 01/12/2024 14:52TO-15 Benzene µg/m3 0.073 5.08 01/12/2024 14:52TO-15 Bromodichloromethane µg/m3 0.150 Page 5 of 59 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 24-011-0012 Report Limit Project:Harrelson Ford V 93796BF-SG-2 7.19 01/12/2024 14:52TO-15 Carbon Disulfide µg/m3 0.060 45.2 01/12/2024 14:52TO-15 Chloroform µg/m3 0.086 J0.625 01/12/2024 14:52TO-15 1,4-Dichlorobenzene µg/m3 0.186 2.49 01/12/2024 14:52TO-15 Dichlorodifluoromethane µg/m3 0.134 J0.376 01/12/2024 14:52TO-15 cis-1,2-Dichloroethene µg/m3 0.095 14.3 01/12/2024 14:52TO-15 Ethyl Acetate µg/m3 0.136 74.4 01/12/2024 14:52TO-15 Ethylbenzene µg/m3 0.106 13.1 01/12/2024 14:52TO-15 4-Ethyltoluene µg/m3 0.128 15.3 01/12/2024 14:52TO-15 Heptane µg/m3 0.143 3.71 01/12/2024 14:52TO-15 n-Hexane µg/m3 0.047 JB2.11 01/12/2024 14:52TO-15 Isopropyl Alcohol µg/m3 0.139 4.66 01/12/2024 14:52TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 J1.71 01/12/2024 14:52TO-15 Methyl tert-butyl ether (MTBE)µg/m3 0.033 J1.54 01/12/2024 14:52TO-15 4-Methyl-2-Pentanone µg/m3 0.121 2.90 01/12/2024 14:52TO-15 Methylene Chloride µg/m3 0.488 J1.45 01/12/2024 14:52TO-15 Naphthalene µg/m3 0.183 1.94 01/12/2024 14:52TO-15 Propene µg/m3 0.242 J1.00 01/12/2024 14:52TO-15 Styrene µg/m3 0.124 24.0 01/12/2024 14:52TO-15 Tetrachloroethene µg/m3 0.181 1.89 01/12/2024 14:52TO-15 Tetrahydrofuran µg/m3 0.107 356 01/11/2024 23:24TO-15 Toluene µg/m3 1.80 5.64 01/12/2024 14:52TO-15 Trichloroethene µg/m3 0.199 J1.53 01/12/2024 14:52TO-15 Trichlorofluoromethane µg/m3 0.130 41.0 01/12/2024 14:52TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 10.4 01/12/2024 14:52TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 51.6 01/12/2024 14:52TO-15 o-Xylene µg/m3 0.157 174 01/12/2024 14:52TO-15 m,p-Xylene µg/m3 0.217 226 01/12/2024 14:52TO-15 Xylene (Total)µg/m3 0.157 V 93797BF-SG-3 29.8 01/12/2024 15:45TO-15 Acetone µg/m3 0.202 23.4 01/12/2024 15:45TO-15 Benzene µg/m3 0.073 10.9 01/12/2024 15:45TO-15 Carbon Disulfide µg/m3 0.060 J1.04 01/12/2024 15:45TO-15 Chloroform µg/m3 0.086 2.52 01/12/2024 15:45TO-15 Dichlorodifluoromethane µg/m3 0.134 3.52 01/12/2024 15:45TO-15 Ethyl Acetate µg/m3 0.136 44.9 01/12/2024 15:45TO-15 Ethylbenzene µg/m3 0.106 Page 6 of 59 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 24-011-0012 Report Limit Project:Harrelson Ford V 93797BF-SG-3 6.33 01/12/2024 15:45TO-15 4-Ethyltoluene µg/m3 0.128 15.4 01/12/2024 15:45TO-15 Heptane µg/m3 0.143 8.21 01/12/2024 15:45TO-15 n-Hexane µg/m3 0.047 JB1.91 01/12/2024 15:45TO-15 Isopropyl Alcohol µg/m3 0.139 5.00 01/12/2024 15:45TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 J0.991 01/12/2024 15:45TO-15 4-Methyl-2-Pentanone µg/m3 0.121 3.22 01/12/2024 15:45TO-15 Methylene Chloride µg/m3 0.488 J0.739 01/12/2024 15:45TO-15 Naphthalene µg/m3 0.183 5.81 01/12/2024 15:45TO-15 Propene µg/m3 0.242 J0.621 01/12/2024 15:45TO-15 Styrene µg/m3 0.124 12.4 01/12/2024 15:45TO-15 Tetrachloroethene µg/m3 0.181 2.48 01/12/2024 15:45TO-15 Tetrahydrofuran µg/m3 0.107 232 01/12/2024 00:00TO-15 Toluene µg/m3 1.80 J1.51 01/12/2024 15:45TO-15 Trichlorofluoromethane µg/m3 0.130 19.7 01/12/2024 15:45TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 5.12 01/12/2024 15:45TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 31.4 01/12/2024 15:45TO-15 o-Xylene µg/m3 0.157 104 01/12/2024 15:45TO-15 m,p-Xylene µg/m3 0.217 135 01/12/2024 15:45TO-15 Xylene (Total)µg/m3 0.157 V 93798BF-SG-4 76.2 01/12/2024 16:39TO-15 Acetone µg/m3 0.202 16.4 01/12/2024 16:39TO-15 Benzene µg/m3 0.073 J2.49 01/12/2024 16:39TO-15 Carbon Disulfide µg/m3 0.060 4.21 01/12/2024 16:39TO-15 Chloroform µg/m3 0.086 2.56 01/12/2024 16:39TO-15 Dichlorodifluoromethane µg/m3 0.134 4.30 01/12/2024 16:39TO-15 Ethyl Acetate µg/m3 0.136 49.4 01/12/2024 16:39TO-15 Ethylbenzene µg/m3 0.106 5.08 01/12/2024 16:39TO-15 4-Ethyltoluene µg/m3 0.128 2.36 01/12/2024 16:39TO-15 Heptane µg/m3 0.143 J1.02 01/12/2024 16:39TO-15 n-Hexane µg/m3 0.047 2.42 01/12/2024 16:39TO-15 2-Hexanone µg/m3 0.285 9.89 01/12/2024 16:39TO-15 Isopropyl Alcohol µg/m3 0.139 13.3 01/12/2024 16:39TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 4.04 01/12/2024 16:39TO-15 Methyl tert-butyl ether (MTBE)µg/m3 0.033 J0.901 01/12/2024 16:39TO-15 4-Methyl-2-Pentanone µg/m3 0.121 2.83 01/12/2024 16:39TO-15 Methylene Chloride µg/m3 0.488 Page 7 of 59 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 24-011-0012 Report Limit Project:Harrelson Ford V 93798BF-SG-4 3.17 01/12/2024 16:39TO-15 Propene µg/m3 0.242 J0.460 01/12/2024 16:39TO-15 Styrene µg/m3 0.124 3.82 01/12/2024 16:39TO-15 Tetrachloroethene µg/m3 0.181 2.46 01/12/2024 16:39TO-15 Tetrahydrofuran µg/m3 0.107 250 01/12/2024 00:37TO-15 Toluene µg/m3 1.80 J1.59 01/12/2024 16:39TO-15 Trichlorofluoromethane µg/m3 0.130 15.0 01/12/2024 16:39TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 4.32 01/12/2024 16:39TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 33.9 01/12/2024 16:39TO-15 o-Xylene µg/m3 0.157 113 01/12/2024 16:39TO-15 m,p-Xylene µg/m3 0.217 147 01/12/2024 16:39TO-15 Xylene (Total)µg/m3 0.157 V 93799BF-SG-5 103 01/12/2024 17:28TO-15 Acetone µg/m3 0.202 32.8 01/12/2024 17:28TO-15 Benzene µg/m3 0.073 8.38 01/12/2024 17:28TO-15 Carbon Disulfide µg/m3 0.060 10.6 01/12/2024 17:28TO-15 Chloroform µg/m3 0.086 J2.46 01/12/2024 17:28TO-15 Dichlorodifluoromethane µg/m3 0.134 5.52 01/12/2024 17:28TO-15 Ethyl Acetate µg/m3 0.136 60.2 01/12/2024 17:28TO-15 Ethylbenzene µg/m3 0.106 7.80 01/12/2024 17:28TO-15 4-Ethyltoluene µg/m3 0.128 17.9 01/12/2024 17:28TO-15 Heptane µg/m3 0.143 5.86 01/12/2024 17:28TO-15 n-Hexane µg/m3 0.047 14.1 01/12/2024 17:28TO-15 Isopropyl Alcohol µg/m3 0.139 16.7 01/12/2024 17:28TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 3.45 01/12/2024 17:28TO-15 Methyl tert-butyl ether (MTBE)µg/m3 0.033 2.30 01/12/2024 17:28TO-15 4-Methyl-2-Pentanone µg/m3 0.121 2.57 01/12/2024 17:28TO-15 Methylene Chloride µg/m3 0.488 J0.995 01/12/2024 17:28TO-15 Naphthalene µg/m3 0.183 5.22 01/12/2024 17:28TO-15 Propene µg/m3 0.242 J0.655 01/12/2024 17:28TO-15 Styrene µg/m3 0.124 J0.773 01/12/2024 17:28TO-15 Tetrachloroethene µg/m3 0.181 J1.03 01/12/2024 17:28TO-15 Tetrahydrofuran µg/m3 0.107 333 01/12/2024 01:14TO-15 Toluene µg/m3 1.80 J1.43 01/12/2024 17:28TO-15 Trichlorofluoromethane µg/m3 0.130 23.7 01/12/2024 17:28TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 6.41 01/12/2024 17:28TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 Page 8 of 59 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 24-011-0012 Report Limit Project:Harrelson Ford V 93799BF-SG-5 41.3 01/12/2024 17:28TO-15 o-Xylene µg/m3 0.157 139 01/12/2024 17:28TO-15 m,p-Xylene µg/m3 0.217 180 01/12/2024 17:28TO-15 Xylene (Total)µg/m3 0.157 V 93800BF-SG-6 31.7 01/12/2024 18:21TO-15 Acetone µg/m3 0.202 22.2 01/12/2024 18:21TO-15 Benzene µg/m3 0.073 J4.65 01/12/2024 18:21TO-15 Carbon Disulfide µg/m3 0.060 J0.912 01/12/2024 18:21TO-15 Chloroform µg/m3 0.086 2.50 01/12/2024 18:21TO-15 Dichlorodifluoromethane µg/m3 0.134 J0.781 01/12/2024 18:21TO-15 cis-1,2-Dichloroethene µg/m3 0.095 2.06 01/12/2024 18:21TO-15 Ethyl Acetate µg/m3 0.136 38.9 01/12/2024 18:21TO-15 Ethylbenzene µg/m3 0.106 5.67 01/12/2024 18:21TO-15 4-Ethyltoluene µg/m3 0.128 14.6 01/12/2024 18:21TO-15 Heptane µg/m3 0.143 9.45 01/12/2024 18:21TO-15 n-Hexane µg/m3 0.047 39.0 01/12/2024 18:21TO-15 Isopropyl Alcohol µg/m3 0.139 5.03 01/12/2024 18:21TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 J1.61 01/12/2024 18:21TO-15 4-Methyl-2-Pentanone µg/m3 0.121 2.06 01/12/2024 18:21TO-15 Methylene Chloride µg/m3 0.488 J0.571 01/12/2024 18:21TO-15 Naphthalene µg/m3 0.183 2.74 01/12/2024 18:21TO-15 Propene µg/m3 0.242 J0.587 01/12/2024 18:21TO-15 Styrene µg/m3 0.124 5.94 01/12/2024 18:21TO-15 Tetrachloroethene µg/m3 0.181 6.68 01/12/2024 18:21TO-15 Tetrahydrofuran µg/m3 0.107 194 01/12/2024 01:50TO-15 Toluene µg/m3 1.80 J1.48 01/12/2024 18:21TO-15 Trichlorofluoromethane µg/m3 0.130 16.8 01/12/2024 18:21TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 4.39 01/12/2024 18:21TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 26.1 01/12/2024 18:21TO-15 o-Xylene µg/m3 0.157 89.5 01/12/2024 18:21TO-15 m,p-Xylene µg/m3 0.217 116 01/12/2024 18:21TO-15 Xylene (Total)µg/m3 0.157 V 93801BF-SG-7 11.5 01/12/2024 19:12TO-15 Acetone µg/m3 0.202 5.05 01/12/2024 19:12TO-15 Benzene µg/m3 0.073 J3.97 01/12/2024 19:12TO-15 Carbon Disulfide µg/m3 0.060 2.77 01/12/2024 19:12TO-15 Dichlorodifluoromethane µg/m3 0.134 Page 9 of 59 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 24-011-0012 Report Limit Project:Harrelson Ford V 93801BF-SG-7 5.87 01/12/2024 19:12TO-15 Ethyl Acetate µg/m3 0.136 7.12 01/12/2024 19:12TO-15 Ethylbenzene µg/m3 0.106 J0.806 01/12/2024 19:12TO-15 4-Ethyltoluene µg/m3 0.128 J0.567 01/12/2024 19:12TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561 3.13 01/12/2024 19:12TO-15 Heptane µg/m3 0.143 5.78 01/12/2024 19:12TO-15 n-Hexane µg/m3 0.047 3.88 01/12/2024 19:12TO-15 2-Hexanone µg/m3 0.285 19.7 01/12/2024 19:12TO-15 Isopropyl Alcohol µg/m3 0.139 3.50 01/12/2024 19:12TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 J1.58 01/12/2024 19:12TO-15 4-Methyl-2-Pentanone µg/m3 0.121 J1.16 01/12/2024 19:12TO-15 Methylene Chloride µg/m3 0.488 J0.560 01/12/2024 19:12TO-15 Naphthalene µg/m3 0.183 4.63 01/12/2024 19:12TO-15 Propene µg/m3 0.242 8.47 01/12/2024 19:12TO-15 Tetrachloroethene µg/m3 0.181 8.45 01/12/2024 19:12TO-15 Tetrahydrofuran µg/m3 0.107 49.0 01/12/2024 19:12TO-15 Toluene µg/m3 0.090 J0.607 01/12/2024 19:12TO-15 Trichloroethene µg/m3 0.199 J2.07 01/12/2024 19:12TO-15 Trichlorofluoromethane µg/m3 0.130 2.51 01/12/2024 19:12TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 J0.688 01/12/2024 19:12TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 4.34 01/12/2024 19:12TO-15 o-Xylene µg/m3 0.157 14.7 01/12/2024 19:12TO-15 m,p-Xylene µg/m3 0.217 19.0 01/12/2024 19:12TO-15 Xylene (Total)µg/m3 0.157 V 93802BF-SG-8 44.2 01/12/2024 20:04TO-15 Acetone µg/m3 0.202 28.7 01/12/2024 20:04TO-15 Benzene µg/m3 0.073 12.4 01/12/2024 20:04TO-15 Carbon Disulfide µg/m3 0.060 J1.74 01/12/2024 20:04TO-15 Chloroform µg/m3 0.086 2.50 01/12/2024 20:04TO-15 Dichlorodifluoromethane µg/m3 0.134 9.42 01/12/2024 20:04TO-15 cis-1,2-Dichloroethene µg/m3 0.095 52.6 01/12/2024 20:04TO-15 Ethylbenzene µg/m3 0.106 5.68 01/12/2024 20:04TO-15 4-Ethyltoluene µg/m3 0.128 8.68 01/12/2024 20:04TO-15 Heptane µg/m3 0.143 7.50 01/12/2024 20:04TO-15 n-Hexane µg/m3 0.047 5.64 01/12/2024 20:04TO-15 2-Hexanone µg/m3 0.285 18.8 01/12/2024 20:04TO-15 Isopropyl Alcohol µg/m3 0.139 Page 10 of 59 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 24-011-0012 Report Limit Project:Harrelson Ford V 93802BF-SG-8 12.2 01/12/2024 20:04TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 J1.15 01/12/2024 20:04TO-15 Methyl tert-butyl ether (MTBE)µg/m3 0.033 2.15 01/12/2024 20:04TO-15 4-Methyl-2-Pentanone µg/m3 0.121 2.80 01/12/2024 20:04TO-15 Methylene Chloride µg/m3 0.488 30.5 01/12/2024 20:04TO-15 Propene µg/m3 0.242 J0.600 01/12/2024 20:04TO-15 Styrene µg/m3 0.124 17.5 01/12/2024 20:04TO-15 Tetrachloroethene µg/m3 0.181 51.5 01/12/2024 20:04TO-15 Tetrahydrofuran µg/m3 0.107 288 01/12/2024 03:04TO-15 Toluene µg/m3 1.80 2.55 01/12/2024 20:04TO-15 Trichloroethene µg/m3 0.199 J1.57 01/12/2024 20:04TO-15 Trichlorofluoromethane µg/m3 0.130 15.5 01/12/2024 20:04TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 4.97 01/12/2024 20:04TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 34.1 01/12/2024 20:04TO-15 o-Xylene µg/m3 0.157 115 01/12/2024 20:04TO-15 m,p-Xylene µg/m3 0.217 149 01/12/2024 20:04TO-15 Xylene (Total)µg/m3 0.157 V 93803BF-SG-9 9.78 01/12/2024 20:56TO-15 Acetone µg/m3 0.202 J1.24 01/12/2024 20:56TO-15 Benzene µg/m3 0.073 J0.504 01/12/2024 20:56TO-15 Carbon Disulfide µg/m3 0.060 J1.07 01/12/2024 20:56TO-15 Chloroform µg/m3 0.086 2.60 01/12/2024 20:56TO-15 Dichlorodifluoromethane µg/m3 0.134 J0.729 01/12/2024 20:56TO-15 1,1-Dichloroethene µg/m3 0.107 13.1 01/12/2024 20:56TO-15 cis-1,2-Dichloroethene µg/m3 0.095 J0.620 01/12/2024 20:56TO-15 Ethylbenzene µg/m3 0.106 J0.385 01/12/2024 20:56TO-15 Heptane µg/m3 0.143 J0.782 01/12/2024 20:56TO-15 n-Hexane µg/m3 0.047 15.9 01/12/2024 20:56TO-15 Isopropyl Alcohol µg/m3 0.139 1.58 01/12/2024 20:56TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 J0.634 01/12/2024 20:56TO-15 4-Methyl-2-Pentanone µg/m3 0.121 J1.26 01/12/2024 20:56TO-15 Methylene Chloride µg/m3 0.488 77.1 01/12/2024 20:56TO-15 Propene µg/m3 0.242 266 01/12/2024 20:56TO-15 Tetrachloroethene µg/m3 0.181 J0.333 01/12/2024 20:56TO-15 Tetrahydrofuran µg/m3 0.107 4.47 01/12/2024 20:56TO-15 Toluene µg/m3 0.090 44.4 01/12/2024 20:56TO-15 Trichloroethene µg/m3 0.199 Page 11 of 59 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 24-011-0012 Report Limit Project:Harrelson Ford V 93803BF-SG-9 J1.64 01/12/2024 20:56TO-15 Trichlorofluoromethane µg/m3 0.130 J0.603 01/12/2024 20:56TO-15 o-Xylene µg/m3 0.157 J1.44 01/12/2024 20:56TO-15 m,p-Xylene µg/m3 0.217 J2.04 01/12/2024 20:56TO-15 Xylene (Total)µg/m3 0.157 V 93804BF-SG-10 64.5 01/12/2024 21:48TO-15 Acetone µg/m3 0.202 27.7 01/12/2024 21:48TO-15 Benzene µg/m3 0.073 37.3 01/12/2024 21:48TO-15 Carbon Disulfide µg/m3 0.060 J1.15 01/12/2024 21:48TO-15 Chloroform µg/m3 0.086 7.34 01/12/2024 21:48TO-15 Cyclohexane µg/m3 0.161 2.47 01/12/2024 21:48TO-15 Dichlorodifluoromethane µg/m3 0.134 J1.32 01/12/2024 21:48TO-15 1,1-Dichloroethene µg/m3 0.107 15.8 01/12/2024 21:48TO-15 cis-1,2-Dichloroethene µg/m3 0.095 J0.693 01/12/2024 21:48TO-15 trans-1,2-Dichloroethene µg/m3 0.108 12.3 01/12/2024 21:48TO-15 Ethyl Acetate µg/m3 0.136 47.9 01/12/2024 21:48TO-15 Ethylbenzene µg/m3 0.106 5.21 01/12/2024 21:48TO-15 4-Ethyltoluene µg/m3 0.128 19.2 01/12/2024 21:48TO-15 Heptane µg/m3 0.143 12.1 01/12/2024 21:48TO-15 n-Hexane µg/m3 0.047 13.4 01/12/2024 21:48TO-15 Isopropyl Alcohol µg/m3 0.139 16.3 01/12/2024 21:48TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 J0.767 01/12/2024 21:48TO-15 Methyl tert-butyl ether (MTBE)µg/m3 0.033 J1.67 01/12/2024 21:48TO-15 4-Methyl-2-Pentanone µg/m3 0.121 2.35 01/12/2024 21:48TO-15 Methylene Chloride µg/m3 0.488 J0.566 01/12/2024 21:48TO-15 Naphthalene µg/m3 0.183 23.0 01/12/2024 21:48TO-15 Propene µg/m3 0.242 J0.540 01/12/2024 21:48TO-15 Styrene µg/m3 0.124 17.1 01/12/2024 21:48TO-15 Tetrachloroethene µg/m3 0.181 4.73 01/12/2024 21:48TO-15 Tetrahydrofuran µg/m3 0.107 244 01/12/2024 04:17TO-15 Toluene µg/m3 1.80 8.19 01/12/2024 21:48TO-15 Trichloroethene µg/m3 0.199 J1.46 01/12/2024 21:48TO-15 Trichlorofluoromethane µg/m3 0.130 15.2 01/12/2024 21:48TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 4.51 01/12/2024 21:48TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 32.2 01/12/2024 21:48TO-15 o-Xylene µg/m3 0.157 108 01/12/2024 21:48TO-15 m,p-Xylene µg/m3 0.217 Page 12 of 59 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 24-011-0012 Report Limit Project:Harrelson Ford V 93804BF-SG-10 140 01/12/2024 21:48TO-15 Xylene (Total)µg/m3 0.157 V 93805BF-SG-11 38.0 01/12/2024 22:40TO-15 Acetone µg/m3 0.202 32.4 01/12/2024 22:40TO-15 Benzene µg/m3 0.073 17.9 01/12/2024 22:40TO-15 Carbon Disulfide µg/m3 0.060 J1.79 01/12/2024 22:40TO-15 Chloroform µg/m3 0.086 J2.36 01/12/2024 22:40TO-15 Cyclohexane µg/m3 0.161 2.58 01/12/2024 22:40TO-15 Dichlorodifluoromethane µg/m3 0.134 8.49 01/12/2024 22:40TO-15 Ethyl Acetate µg/m3 0.136 64.6 01/12/2024 22:40TO-15 Ethylbenzene µg/m3 0.106 7.03 01/12/2024 22:40TO-15 4-Ethyltoluene µg/m3 0.128 12.6 01/12/2024 22:40TO-15 Heptane µg/m3 0.143 8.25 01/12/2024 22:40TO-15 n-Hexane µg/m3 0.047 13.4 01/12/2024 22:40TO-15 Isopropyl Alcohol µg/m3 0.139 6.21 01/12/2024 22:40TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 J1.15 01/12/2024 22:40TO-15 4-Methyl-2-Pentanone µg/m3 0.121 J1.62 01/12/2024 22:40TO-15 Methylene Chloride µg/m3 0.488 J0.571 01/12/2024 22:40TO-15 Naphthalene µg/m3 0.183 12.1 01/12/2024 22:40TO-15 Propene µg/m3 0.242 J0.583 01/12/2024 22:40TO-15 Styrene µg/m3 0.124 J0.813 01/12/2024 22:40TO-15 Tetrachloroethene µg/m3 0.181 2.00 01/12/2024 22:40TO-15 Tetrahydrofuran µg/m3 0.107 323 01/12/2024 04:53TO-15 Toluene µg/m3 1.80 J1.59 01/12/2024 22:40TO-15 Trichlorofluoromethane µg/m3 0.130 19.4 01/12/2024 22:40TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 5.90 01/12/2024 22:40TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 42.1 01/12/2024 22:40TO-15 o-Xylene µg/m3 0.157 145 01/12/2024 22:40TO-15 m,p-Xylene µg/m3 0.217 187 01/12/2024 22:40TO-15 Xylene (Total)µg/m3 0.157 Page 13 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-1 93794 Matrix: 1/11/2024 10:26 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 18.0 µg/m3 0.202 4.75Acetone 1 01/12/24 13:09 V42301ENM 75.8 µg/m3 0.073 1.60Benzene 1 01/12/24 13:09 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 13:09 V42301ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 13:09 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 13:09 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 13:09 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 13:09 V42301ENM 20.6 µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 13:09 V42301ENM 0.893 J µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 13:09 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 13:09 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 13:09 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 13:09 V42301ENM 1.65 J µg/m3 0.086 2.44Chloroform 1 01/12/24 13:09 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 13:09 V42301ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 01/12/24 13:09 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 13:09 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 13:09 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 13:09 V42301ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 13:09 V42301ENM 2.49 µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 13:09 V42301ENM 1.79 J µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 13:09 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 13:09 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 14 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-1 93794 Matrix: 1/11/2024 10:26 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 2.61 µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 13:09 V42301ENM 71.9 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 13:09 V42301ENM 2.34 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 13:09 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 13:09 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 13:09 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 13:09 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 13:09 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 13:09 V42301ENM 26.4 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 13:09 V42301ENM 58.2 µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 13:09 V42301ENM 7.23 µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 13:09 V42301ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 13:09 V42301ENM 31.7 µg/m3 0.143 2.05Heptane 1 01/12/24 13:09 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 13:09 V42301ENM 17.0 µg/m3 0.047 1.76n-Hexane 1 01/12/24 13:09 V42301ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 01/12/24 13:09 V42301ENM 2.10 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 13:09 V42301ENM 4.96 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 13:09 V42301ENM 26.2 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 13:09 V42301ENM 3.11 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 13:09 V42301ENM 3.75 µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 13:09 V42301ENM 4.57 µg/m3 0.183 2.62Naphthalene 1 01/12/24 13:09 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 15 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-1 93794 Matrix: 1/11/2024 10:26 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 3.62 µg/m3 0.242 0.860Propene 1 01/12/24 13:09 V42301ENM 0.647 J µg/m3 0.124 2.13Styrene 1 01/12/24 13:09 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 13:09 V42301ENM 106 µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 13:09 V42301ENM 17.0 µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 13:09 V42301ENM 338 µg/m3 1.80 37.7Toluene 20 01/11/24 22:11 V42369ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 13:09 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 13:09 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 13:09 V42301ENM 117 µg/m3 0.199 2.15Trichloroethene 1 01/12/24 13:09 V42301ENM 1.52 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 13:09 V42301ENM 24.8 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 13:09 V42301ENM 6.81 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 13:09 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 13:09 V42301ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 13:09 V42301ENM 42.2 µg/m3 0.157 2.17o-Xylene 1 01/12/24 13:09 V42301ENM 134 µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 13:09 V42301ENM 176 µg/m3 0.157 2.17Xylene (Total)1 01/12/24 13:09 V42301 Surrogate: 4-Bromofluorobenzene 96.6 Limits: 70-130%01/12/24 13:091 ENM V42301 Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%01/11/24 22:1120 ENM V42369 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 16 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-DUP 93795 Matrix: 1/11/2024 0:00 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 21.7 µg/m3 0.202 4.75Acetone 1 01/12/24 14:00 V42301ENM 74.8 µg/m3 0.073 1.60Benzene 1 01/12/24 14:00 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 14:00 V42301ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 14:00 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 14:00 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 14:00 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 14:00 V42301ENM 18.1 µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 14:00 V42301ENM 0.905 J µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 14:00 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 14:00 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 14:00 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 14:00 V42301ENM 1.70 J µg/m3 0.086 2.44Chloroform 1 01/12/24 14:00 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 14:00 V42301ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 01/12/24 14:00 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 14:00 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 14:00 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 14:00 V42301ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 14:00 V42301ENM 2.45 J µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 14:00 V42301ENM 1.80 J µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 14:00 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 14:00 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 17 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-DUP 93795 Matrix: 1/11/2024 0:00 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 2.66 µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 14:00 V42301ENM 70.8 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 14:00 V42301ENM 2.36 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 14:00 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 14:00 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 14:00 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 14:00 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 14:00 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 14:00 V42301ENM 25.5 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 14:00 V42301ENM 57.9 µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 14:00 V42301ENM 7.31 µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 14:00 V42301ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 14:00 V42301ENM 31.7 µg/m3 0.143 2.05Heptane 1 01/12/24 14:00 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 14:00 V42301ENM 16.9 µg/m3 0.047 1.76n-Hexane 1 01/12/24 14:00 V42301ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 01/12/24 14:00 V42301ENM 2.26 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 14:00 V42301ENM 5.62 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 14:00 V42301ENM 26.2 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 14:00 V42301ENM 3.15 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 14:00 V42301ENM 3.62 µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 14:00 V42301ENM 4.32 µg/m3 0.183 2.62Naphthalene 1 01/12/24 14:00 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 18 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-DUP 93795 Matrix: 1/11/2024 0:00 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 3.67 µg/m3 0.242 0.860Propene 1 01/12/24 14:00 V42301ENM 0.685 J µg/m3 0.124 2.13Styrene 1 01/12/24 14:00 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 14:00 V42301ENM 104 µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 14:00 V42301ENM 23.5 µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 14:00 V42301ENM 345 µg/m3 1.80 37.7Toluene 20 01/11/24 22:47 V42369ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 14:00 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 14:00 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 14:00 V42301ENM 115 µg/m3 0.199 2.15Trichloroethene 1 01/12/24 14:00 V42301ENM 1.57 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 14:00 V42301ENM 24.6 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 14:00 V42301ENM 6.78 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 14:00 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 14:00 V42301ENM 1.90 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 14:00 V42301ENM 41.9 µg/m3 0.157 2.17o-Xylene 1 01/12/24 14:00 V42301ENM 135 µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 14:00 V42301ENM 177 µg/m3 0.157 2.17Xylene (Total)1 01/12/24 14:00 V42301 Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%01/12/24 14:001 ENM V42301 Surrogate: 4-Bromofluorobenzene 96.4 Limits: 70-130%01/11/24 22:4720 ENM V42369 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 19 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-2 93796 Matrix: 1/11/2024 10:42 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 24.6 µg/m3 0.202 4.75Acetone 1 01/12/24 14:52 V42301ENM 41.1 µg/m3 0.073 1.60Benzene 1 01/12/24 14:52 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 14:52 V42301ENM 5.08 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 14:52 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 14:52 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 14:52 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 14:52 V42301ENM 7.19 µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 14:52 V42301ENM <0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 14:52 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 14:52 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 14:52 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 14:52 V42301ENM 45.2 µg/m3 0.086 2.44Chloroform 1 01/12/24 14:52 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 14:52 V42301ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 01/12/24 14:52 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 14:52 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 14:52 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 14:52 V42301ENM 0.625 J µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 14:52 V42301ENM 2.49 µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 14:52 V42301ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 14:52 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 14:52 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 20 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-2 93796 Matrix: 1/11/2024 10:42 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 14:52 V42301ENM 0.376 J µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 14:52 V42301ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 14:52 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 14:52 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 14:52 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 14:52 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 14:52 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 14:52 V42301ENM 14.3 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 14:52 V42301ENM 74.4 µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 14:52 V42301ENM 13.1 µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 14:52 V42301ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 14:52 V42301ENM 15.3 µg/m3 0.143 2.05Heptane 1 01/12/24 14:52 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 14:52 V42301ENM 3.71 µg/m3 0.047 1.76n-Hexane 1 01/12/24 14:52 V42301ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 01/12/24 14:52 V42301ENM 2.11 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 14:52 V42301ENM 4.66 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 14:52 V42301ENM 1.71 J µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 14:52 V42301ENM 1.54 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 14:52 V42301ENM 2.90 µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 14:52 V42301ENM 1.45 J µg/m3 0.183 2.62Naphthalene 1 01/12/24 14:52 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 21 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-2 93796 Matrix: 1/11/2024 10:42 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 1.94 µg/m3 0.242 0.860Propene 1 01/12/24 14:52 V42301ENM 1.00 J µg/m3 0.124 2.13Styrene 1 01/12/24 14:52 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 14:52 V42301ENM 24.0 µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 14:52 V42301ENM 1.89 µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 14:52 V42301ENM 356 µg/m3 1.80 37.7Toluene 20 01/11/24 23:24 V42369ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 14:52 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 14:52 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 14:52 V42301ENM 5.64 µg/m3 0.199 2.15Trichloroethene 1 01/12/24 14:52 V42301ENM 1.53 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 14:52 V42301ENM 41.0 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 14:52 V42301ENM 10.4 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 14:52 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 14:52 V42301ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 14:52 V42301ENM 51.6 µg/m3 0.157 2.17o-Xylene 1 01/12/24 14:52 V42301ENM 174 µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 14:52 V42301ENM 226 µg/m3 0.157 2.17Xylene (Total)1 01/12/24 14:52 V42301 Surrogate: 4-Bromofluorobenzene 94.1 Limits: 70-130%01/12/24 14:521 ENM V42301 Surrogate: 4-Bromofluorobenzene 96.1 Limits: 70-130%01/11/24 23:2420 ENM V42369 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 22 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-3 93797 Matrix: 1/11/2024 10:58 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 29.8 µg/m3 0.202 4.75Acetone 1 01/12/24 15:45 V42301ENM 23.4 µg/m3 0.073 1.60Benzene 1 01/12/24 15:45 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 15:45 V42301ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 15:45 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 15:45 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 15:45 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 15:45 V42301ENM 10.9 µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 15:45 V42301ENM <0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 15:45 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 15:45 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 15:45 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 15:45 V42301ENM 1.04 J µg/m3 0.086 2.44Chloroform 1 01/12/24 15:45 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 15:45 V42301ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 01/12/24 15:45 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 15:45 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 15:45 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 15:45 V42301ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 15:45 V42301ENM 2.52 µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 15:45 V42301ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 15:45 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 15:45 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 23 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-3 93797 Matrix: 1/11/2024 10:58 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 15:45 V42301ENM <0.095 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 15:45 V42301ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 15:45 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 15:45 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 15:45 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 15:45 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 15:45 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 15:45 V42301ENM 3.52 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 15:45 V42301ENM 44.9 µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 15:45 V42301ENM 6.33 µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 15:45 V42301ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 15:45 V42301ENM 15.4 µg/m3 0.143 2.05Heptane 1 01/12/24 15:45 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 15:45 V42301ENM 8.21 µg/m3 0.047 1.76n-Hexane 1 01/12/24 15:45 V42301ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 01/12/24 15:45 V42301ENM 1.91 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 15:45 V42301ENM 5.00 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 15:45 V42301ENM <0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 15:45 V42301ENM 0.991 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 15:45 V42301ENM 3.22 µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 15:45 V42301ENM 0.739 J µg/m3 0.183 2.62Naphthalene 1 01/12/24 15:45 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 24 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-3 93797 Matrix: 1/11/2024 10:58 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 5.81 µg/m3 0.242 0.860Propene 1 01/12/24 15:45 V42301ENM 0.621 J µg/m3 0.124 2.13Styrene 1 01/12/24 15:45 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 15:45 V42301ENM 12.4 µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 15:45 V42301ENM 2.48 µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 15:45 V42301ENM 232 µg/m3 1.80 37.7Toluene 20 01/12/24 00:00 V42369ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 15:45 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 15:45 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 15:45 V42301ENM <0.199 µg/m3 0.199 2.15Trichloroethene 1 01/12/24 15:45 V42301ENM 1.51 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 15:45 V42301ENM 19.7 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 15:45 V42301ENM 5.12 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 15:45 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 15:45 V42301ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 15:45 V42301ENM 31.4 µg/m3 0.157 2.17o-Xylene 1 01/12/24 15:45 V42301ENM 104 µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 15:45 V42301ENM 135 µg/m3 0.157 2.17Xylene (Total)1 01/12/24 15:45 V42301 Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%01/12/24 15:451 ENM V42301 Surrogate: 4-Bromofluorobenzene 94.7 Limits: 70-130%01/12/24 00:0020 ENM V42369 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 25 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-4 93798 Matrix: 1/11/2024 11:14 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 76.2 µg/m3 0.202 4.75Acetone 1 01/12/24 16:39 V42301ENM 16.4 µg/m3 0.073 1.60Benzene 1 01/12/24 16:39 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 16:39 V42301ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 16:39 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 16:39 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 16:39 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 16:39 V42301ENM 2.49 J µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 16:39 V42301ENM <0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 16:39 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 16:39 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 16:39 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 16:39 V42301ENM 4.21 µg/m3 0.086 2.44Chloroform 1 01/12/24 16:39 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 16:39 V42301ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 01/12/24 16:39 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 16:39 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 16:39 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 16:39 V42301ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 16:39 V42301ENM 2.56 µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 16:39 V42301ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 16:39 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 16:39 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 26 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-4 93798 Matrix: 1/11/2024 11:14 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 16:39 V42301ENM <0.095 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 16:39 V42301ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 16:39 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 16:39 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 16:39 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 16:39 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 16:39 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 16:39 V42301ENM 4.30 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 16:39 V42301ENM 49.4 µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 16:39 V42301ENM 5.08 µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 16:39 V42301ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 16:39 V42301ENM 2.36 µg/m3 0.143 2.05Heptane 1 01/12/24 16:39 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 16:39 V42301ENM 1.02 J µg/m3 0.047 1.76n-Hexane 1 01/12/24 16:39 V42301ENM 2.42 µg/m3 0.285 2.052-Hexanone 1 01/12/24 16:39 V42301ENM 9.89 µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 16:39 V42301ENM 13.3 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 16:39 V42301ENM 4.04 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 16:39 V42301ENM 0.901 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 16:39 V42301ENM 2.83 µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 16:39 V42301ENM <0.183 µg/m3 0.183 2.62Naphthalene 1 01/12/24 16:39 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 27 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-4 93798 Matrix: 1/11/2024 11:14 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 3.17 µg/m3 0.242 0.860Propene 1 01/12/24 16:39 V42301ENM 0.460 J µg/m3 0.124 2.13Styrene 1 01/12/24 16:39 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 16:39 V42301ENM 3.82 µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 16:39 V42301ENM 2.46 µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 16:39 V42301ENM 250 µg/m3 1.80 37.7Toluene 20 01/12/24 00:37 V42369ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 16:39 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 16:39 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 16:39 V42301ENM <0.199 µg/m3 0.199 2.15Trichloroethene 1 01/12/24 16:39 V42301ENM 1.59 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 16:39 V42301ENM 15.0 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 16:39 V42301ENM 4.32 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 16:39 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 16:39 V42301ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 16:39 V42301ENM 33.9 µg/m3 0.157 2.17o-Xylene 1 01/12/24 16:39 V42301ENM 113 µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 16:39 V42301ENM 147 µg/m3 0.157 2.17Xylene (Total)1 01/12/24 16:39 V42301 Surrogate: 4-Bromofluorobenzene 96.9 Limits: 70-130%01/12/24 16:391 ENM V42301 Surrogate: 4-Bromofluorobenzene 95.3 Limits: 70-130%01/12/24 00:3720 ENM V42369 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 28 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-5 93799 Matrix: 1/11/2024 11:30 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 103 µg/m3 0.202 4.75Acetone 1 01/12/24 17:28 V42301ENM 32.8 µg/m3 0.073 1.60Benzene 1 01/12/24 17:28 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 17:28 V42301ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 17:28 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 17:28 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 17:28 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 17:28 V42301ENM 8.38 µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 17:28 V42301ENM <0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 17:28 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 17:28 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 17:28 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 17:28 V42301ENM 10.6 µg/m3 0.086 2.44Chloroform 1 01/12/24 17:28 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 17:28 V42301ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 01/12/24 17:28 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 17:28 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 17:28 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 17:28 V42301ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 17:28 V42301ENM 2.46 J µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 17:28 V42301ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 17:28 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 17:28 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 29 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-5 93799 Matrix: 1/11/2024 11:30 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 17:28 V42301ENM <0.095 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 17:28 V42301ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 17:28 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 17:28 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 17:28 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 17:28 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 17:28 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 17:28 V42301ENM 5.52 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 17:28 V42301ENM 60.2 µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 17:28 V42301ENM 7.80 µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 17:28 V42301ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 17:28 V42301ENM 17.9 µg/m3 0.143 2.05Heptane 1 01/12/24 17:28 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 17:28 V42301ENM 5.86 µg/m3 0.047 1.76n-Hexane 1 01/12/24 17:28 V42301ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 01/12/24 17:28 V42301ENM 14.1 µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 17:28 V42301ENM 16.7 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 17:28 V42301ENM 3.45 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 17:28 V42301ENM 2.30 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 17:28 V42301ENM 2.57 µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 17:28 V42301ENM 0.995 J µg/m3 0.183 2.62Naphthalene 1 01/12/24 17:28 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 30 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-5 93799 Matrix: 1/11/2024 11:30 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 5.22 µg/m3 0.242 0.860Propene 1 01/12/24 17:28 V42301ENM 0.655 J µg/m3 0.124 2.13Styrene 1 01/12/24 17:28 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 17:28 V42301ENM 0.773 J µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 17:28 V42301ENM 1.03 J µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 17:28 V42301ENM 333 µg/m3 1.80 37.7Toluene 20 01/12/24 01:14 V42369ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 17:28 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 17:28 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 17:28 V42301ENM <0.199 µg/m3 0.199 2.15Trichloroethene 1 01/12/24 17:28 V42301ENM 1.43 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 17:28 V42301ENM 23.7 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 17:28 V42301ENM 6.41 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 17:28 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 17:28 V42301ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 17:28 V42301ENM 41.3 µg/m3 0.157 2.17o-Xylene 1 01/12/24 17:28 V42301ENM 139 µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 17:28 V42301ENM 180 µg/m3 0.157 2.17Xylene (Total)1 01/12/24 17:28 V42301 Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%01/12/24 17:281 ENM V42301 Surrogate: 4-Bromofluorobenzene 95.3 Limits: 70-130%01/12/24 01:1420 ENM V42369 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 31 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-6 93800 Matrix: 1/11/2024 12:30 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 31.7 µg/m3 0.202 4.75Acetone 1 01/12/24 18:21 V42301ENM 22.2 µg/m3 0.073 1.60Benzene 1 01/12/24 18:21 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 18:21 V42301ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 18:21 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 18:21 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 18:21 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 18:21 V42301ENM 4.65 J µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 18:21 V42301ENM <0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 18:21 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 18:21 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 18:21 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 18:21 V42301ENM 0.912 J µg/m3 0.086 2.44Chloroform 1 01/12/24 18:21 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 18:21 V42301ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 01/12/24 18:21 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 18:21 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 18:21 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 18:21 V42301ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 18:21 V42301ENM 2.50 µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 18:21 V42301ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 18:21 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 18:21 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 32 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-6 93800 Matrix: 1/11/2024 12:30 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 18:21 V42301ENM 0.781 J µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 18:21 V42301ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 18:21 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 18:21 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 18:21 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 18:21 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 18:21 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 18:21 V42301ENM 2.06 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 18:21 V42301ENM 38.9 µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 18:21 V42301ENM 5.67 µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 18:21 V42301ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 18:21 V42301ENM 14.6 µg/m3 0.143 2.05Heptane 1 01/12/24 18:21 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 18:21 V42301ENM 9.45 µg/m3 0.047 1.76n-Hexane 1 01/12/24 18:21 V42301ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 01/12/24 18:21 V42301ENM 39.0 µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 18:21 V42301ENM 5.03 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 18:21 V42301ENM <0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 18:21 V42301ENM 1.61 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 18:21 V42301ENM 2.06 µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 18:21 V42301ENM 0.571 J µg/m3 0.183 2.62Naphthalene 1 01/12/24 18:21 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 33 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-6 93800 Matrix: 1/11/2024 12:30 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 2.74 µg/m3 0.242 0.860Propene 1 01/12/24 18:21 V42301ENM 0.587 J µg/m3 0.124 2.13Styrene 1 01/12/24 18:21 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 18:21 V42301ENM 5.94 µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 18:21 V42301ENM 6.68 µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 18:21 V42301ENM 194 µg/m3 1.80 37.7Toluene 20 01/12/24 01:50 V42369ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 18:21 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 18:21 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 18:21 V42301ENM <0.199 µg/m3 0.199 2.15Trichloroethene 1 01/12/24 18:21 V42301ENM 1.48 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 18:21 V42301ENM 16.8 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 18:21 V42301ENM 4.39 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 18:21 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 18:21 V42301ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 18:21 V42301ENM 26.1 µg/m3 0.157 2.17o-Xylene 1 01/12/24 18:21 V42301ENM 89.5 µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 18:21 V42301ENM 116 µg/m3 0.157 2.17Xylene (Total)1 01/12/24 18:21 V42301 Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%01/12/24 18:211 ENM V42301 Surrogate: 4-Bromofluorobenzene 94.7 Limits: 70-130%01/12/24 01:5020 ENM V42369 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 34 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-7 93801 Matrix: 1/11/2024 12:50 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 11.5 µg/m3 0.202 4.75Acetone 1 01/12/24 19:12 V42301ENM 5.05 µg/m3 0.073 1.60Benzene 1 01/12/24 19:12 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 19:12 V42301ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 19:12 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 19:12 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 19:12 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 19:12 V42301ENM 3.97 J µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 19:12 V42301ENM <0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 19:12 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 19:12 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 19:12 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 19:12 V42301ENM <0.086 µg/m3 0.086 2.44Chloroform 1 01/12/24 19:12 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 19:12 V42301ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 01/12/24 19:12 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 19:12 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 19:12 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 19:12 V42301ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 19:12 V42301ENM 2.77 µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 19:12 V42301ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 19:12 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 19:12 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 35 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-7 93801 Matrix: 1/11/2024 12:50 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 19:12 V42301ENM <0.095 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 19:12 V42301ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 19:12 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 19:12 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 19:12 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 19:12 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 19:12 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 19:12 V42301ENM 5.87 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 19:12 V42301ENM 7.12 µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 19:12 V42301ENM 0.806 J µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 19:12 V42301ENM 0.567 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 19:12 V42301ENM 3.13 µg/m3 0.143 2.05Heptane 1 01/12/24 19:12 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 19:12 V42301ENM 5.78 µg/m3 0.047 1.76n-Hexane 1 01/12/24 19:12 V42301ENM 3.88 µg/m3 0.285 2.052-Hexanone 1 01/12/24 19:12 V42301ENM 19.7 µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 19:12 V42301ENM 3.50 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 19:12 V42301ENM <0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 19:12 V42301ENM 1.58 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 19:12 V42301ENM 1.16 J µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 19:12 V42301ENM 0.560 J µg/m3 0.183 2.62Naphthalene 1 01/12/24 19:12 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 36 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-7 93801 Matrix: 1/11/2024 12:50 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 4.63 µg/m3 0.242 0.860Propene 1 01/12/24 19:12 V42301ENM <0.124 µg/m3 0.124 2.13Styrene 1 01/12/24 19:12 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 19:12 V42301ENM 8.47 µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 19:12 V42301ENM 8.45 µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 19:12 V42301ENM 49.0 µg/m3 0.090 1.88Toluene 1 01/12/24 19:12 V42301ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 19:12 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 19:12 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 19:12 V42301ENM 0.607 J µg/m3 0.199 2.15Trichloroethene 1 01/12/24 19:12 V42301ENM 2.07 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 19:12 V42301ENM 2.51 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 19:12 V42301ENM 0.688 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 19:12 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 19:12 V42301ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 19:12 V42301ENM 4.34 µg/m3 0.157 2.17o-Xylene 1 01/12/24 19:12 V42301ENM 14.7 µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 19:12 V42301ENM 19.0 µg/m3 0.157 2.17Xylene (Total)1 01/12/24 19:12 V42301 Surrogate: 4-Bromofluorobenzene 98.9 Limits: 70-130%01/12/24 19:121 ENM V42301 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 37 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-8 93802 Matrix: 1/11/2024 13:06 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 44.2 µg/m3 0.202 4.75Acetone 1 01/12/24 20:04 V42301ENM 28.7 µg/m3 0.073 1.60Benzene 1 01/12/24 20:04 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 20:04 V42301ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 20:04 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 20:04 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 20:04 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 20:04 V42301ENM 12.4 µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 20:04 V42301ENM <0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 20:04 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 20:04 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 20:04 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 20:04 V42301ENM 1.74 J µg/m3 0.086 2.44Chloroform 1 01/12/24 20:04 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 20:04 V42301ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 01/12/24 20:04 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 20:04 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 20:04 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 20:04 V42301ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 20:04 V42301ENM 2.50 µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 20:04 V42301ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 20:04 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 20:04 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 38 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-8 93802 Matrix: 1/11/2024 13:06 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 20:04 V42301ENM 9.42 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 20:04 V42301ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 20:04 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 20:04 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 20:04 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 20:04 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 20:04 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 20:04 V42301ENM <0.136 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 20:04 V42301ENM 52.6 µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 20:04 V42301ENM 5.68 µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 20:04 V42301ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 20:04 V42301ENM 8.68 µg/m3 0.143 2.05Heptane 1 01/12/24 20:04 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 20:04 V42301ENM 7.50 µg/m3 0.047 1.76n-Hexane 1 01/12/24 20:04 V42301ENM 5.64 µg/m3 0.285 2.052-Hexanone 1 01/12/24 20:04 V42301ENM 18.8 µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 20:04 V42301ENM 12.2 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 20:04 V42301ENM 1.15 J µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 20:04 V42301ENM 2.15 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 20:04 V42301ENM 2.80 µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 20:04 V42301ENM <0.183 µg/m3 0.183 2.62Naphthalene 1 01/12/24 20:04 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 39 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-8 93802 Matrix: 1/11/2024 13:06 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 30.5 µg/m3 0.242 0.860Propene 1 01/12/24 20:04 V42301ENM 0.600 J µg/m3 0.124 2.13Styrene 1 01/12/24 20:04 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 20:04 V42301ENM 17.5 µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 20:04 V42301ENM 51.5 µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 20:04 V42301ENM 288 µg/m3 1.80 37.7Toluene 20 01/12/24 03:04 V42369ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 20:04 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 20:04 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 20:04 V42301ENM 2.55 µg/m3 0.199 2.15Trichloroethene 1 01/12/24 20:04 V42301ENM 1.57 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 20:04 V42301ENM 15.5 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 20:04 V42301ENM 4.97 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 20:04 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 20:04 V42301ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 20:04 V42301ENM 34.1 µg/m3 0.157 2.17o-Xylene 1 01/12/24 20:04 V42301ENM 115 µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 20:04 V42301ENM 149 µg/m3 0.157 2.17Xylene (Total)1 01/12/24 20:04 V42301 Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%01/12/24 20:041 ENM V42301 Surrogate: 4-Bromofluorobenzene 94.7 Limits: 70-130%01/12/24 03:0420 ENM V42369 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 40 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-9 93803 Matrix: 1/11/2024 13:30 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 9.78 µg/m3 0.202 4.75Acetone 1 01/12/24 20:56 V42301ENM 1.24 J µg/m3 0.073 1.60Benzene 1 01/12/24 20:56 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 20:56 V42301ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 20:56 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 20:56 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 20:56 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 20:56 V42301ENM 0.504 J µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 20:56 V42301ENM <0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 20:56 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 20:56 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 20:56 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 20:56 V42301ENM 1.07 J µg/m3 0.086 2.44Chloroform 1 01/12/24 20:56 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 20:56 V42301ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 01/12/24 20:56 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 20:56 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 20:56 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 20:56 V42301ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 20:56 V42301ENM 2.60 µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 20:56 V42301ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 20:56 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 20:56 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 41 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-9 93803 Matrix: 1/11/2024 13:30 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 0.729 J µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 20:56 V42301ENM 13.1 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 20:56 V42301ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 20:56 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 20:56 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 20:56 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 20:56 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 20:56 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 20:56 V42301ENM <0.136 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 20:56 V42301ENM 0.620 J µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 20:56 V42301ENM <0.128 µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 20:56 V42301ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 20:56 V42301ENM 0.385 J µg/m3 0.143 2.05Heptane 1 01/12/24 20:56 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 20:56 V42301ENM 0.782 J µg/m3 0.047 1.76n-Hexane 1 01/12/24 20:56 V42301ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 01/12/24 20:56 V42301ENM 15.9 µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 20:56 V42301ENM 1.58 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 20:56 V42301ENM <0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 20:56 V42301ENM 0.634 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 20:56 V42301ENM 1.26 J µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 20:56 V42301ENM <0.183 µg/m3 0.183 2.62Naphthalene 1 01/12/24 20:56 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 42 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-9 93803 Matrix: 1/11/2024 13:30 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 77.1 µg/m3 0.242 0.860Propene 1 01/12/24 20:56 V42301ENM <0.124 µg/m3 0.124 2.13Styrene 1 01/12/24 20:56 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 20:56 V42301ENM 266 µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 20:56 V42301ENM 0.333 J µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 20:56 V42301ENM 4.47 µg/m3 0.090 1.88Toluene 1 01/12/24 20:56 V42301ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 20:56 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 20:56 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 20:56 V42301ENM 44.4 µg/m3 0.199 2.15Trichloroethene 1 01/12/24 20:56 V42301ENM 1.64 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 20:56 V42301ENM <0.110 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 20:56 V42301ENM <0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 20:56 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 20:56 V42301ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 20:56 V42301ENM 0.603 J µg/m3 0.157 2.17o-Xylene 1 01/12/24 20:56 V42301ENM 1.44 J µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 20:56 V42301ENM 2.04 J µg/m3 0.157 2.17Xylene (Total)1 01/12/24 20:56 V42301 Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%01/12/24 20:561 ENM V42301 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 43 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-10 93804 Matrix: 1/11/2024 12:00 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 64.5 µg/m3 0.202 4.75Acetone 1 01/12/24 21:48 V42301ENM 27.7 µg/m3 0.073 1.60Benzene 1 01/12/24 21:48 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 21:48 V42301ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 21:48 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 21:48 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 21:48 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 21:48 V42301ENM 37.3 µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 21:48 V42301ENM <0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 21:48 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 21:48 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 21:48 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 21:48 V42301ENM 1.15 J µg/m3 0.086 2.44Chloroform 1 01/12/24 21:48 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 21:48 V42301ENM 7.34 µg/m3 0.161 3.44Cyclohexane 1 01/12/24 21:48 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 21:48 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 21:48 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 21:48 V42301ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 21:48 V42301ENM 2.47 µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 21:48 V42301ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 21:48 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 21:48 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 44 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-10 93804 Matrix: 1/11/2024 12:00 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 1.32 J µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 21:48 V42301ENM 15.8 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 21:48 V42301ENM 0.693 J µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 21:48 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 21:48 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 21:48 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 21:48 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 21:48 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 21:48 V42301ENM 12.3 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 21:48 V42301ENM 47.9 µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 21:48 V42301ENM 5.21 µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 21:48 V42301ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 21:48 V42301ENM 19.2 µg/m3 0.143 2.05Heptane 1 01/12/24 21:48 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 21:48 V42301ENM 12.1 µg/m3 0.047 1.76n-Hexane 1 01/12/24 21:48 V42301ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 01/12/24 21:48 V42301ENM 13.4 µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 21:48 V42301ENM 16.3 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 21:48 V42301ENM 0.767 J µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 21:48 V42301ENM 1.67 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 21:48 V42301ENM 2.35 µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 21:48 V42301ENM 0.566 J µg/m3 0.183 2.62Naphthalene 1 01/12/24 21:48 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 45 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-10 93804 Matrix: 1/11/2024 12:00 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 23.0 µg/m3 0.242 0.860Propene 1 01/12/24 21:48 V42301ENM 0.540 J µg/m3 0.124 2.13Styrene 1 01/12/24 21:48 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 21:48 V42301ENM 17.1 µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 21:48 V42301ENM 4.73 µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 21:48 V42301ENM 244 µg/m3 1.80 37.7Toluene 20 01/12/24 04:17 V42369ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 21:48 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 21:48 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 21:48 V42301ENM 8.19 µg/m3 0.199 2.15Trichloroethene 1 01/12/24 21:48 V42301ENM 1.46 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 21:48 V42301ENM 15.2 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 21:48 V42301ENM 4.51 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 21:48 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 21:48 V42301ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 21:48 V42301ENM 32.2 µg/m3 0.157 2.17o-Xylene 1 01/12/24 21:48 V42301ENM 108 µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 21:48 V42301ENM 140 µg/m3 0.157 2.17Xylene (Total)1 01/12/24 21:48 V42301 Surrogate: 4-Bromofluorobenzene 95.0 Limits: 70-130%01/12/24 21:481 ENM V42301 Surrogate: 4-Bromofluorobenzene 93.9 Limits: 70-130%01/12/24 04:1720 ENM V42369 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 46 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-11 93805 Matrix: 1/11/2024 13:50 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 38.0 µg/m3 0.202 4.75Acetone 1 01/12/24 22:40 V42301ENM 32.4 µg/m3 0.073 1.60Benzene 1 01/12/24 22:40 V42301ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 01/12/24 22:40 V42301ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 01/12/24 22:40 V42301ENM <0.153 µg/m3 0.153 5.17Bromoform 1 01/12/24 22:40 V42301ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 01/12/24 22:40 V42301ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 01/12/24 22:40 V42301ENM 17.9 µg/m3 0.060 6.23Carbon Disulfide 1 01/12/24 22:40 V42301ENM <0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 01/12/24 22:40 V42301ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 01/12/24 22:40 V42301ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 01/12/24 22:40 V42301ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 01/12/24 22:40 V42301ENM 1.79 J µg/m3 0.086 2.44Chloroform 1 01/12/24 22:40 V42301ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 01/12/24 22:40 V42301ENM 2.36 J µg/m3 0.161 3.44Cyclohexane 1 01/12/24 22:40 V42301ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 01/12/24 22:40 V42301ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 01/12/24 22:40 V42301ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 01/12/24 22:40 V42301ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 01/12/24 22:40 V42301ENM 2.58 µg/m3 0.134 2.47Dichlorodifluoromethane 1 01/12/24 22:40 V42301ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 01/12/24 22:40 V42301ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 01/12/24 22:40 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 47 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-11 93805 Matrix: 1/11/2024 13:50 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 01/12/24 22:40 V42301ENM <0.095 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 01/12/24 22:40 V42301ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 01/12/24 22:40 V42301ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 01/12/24 22:40 V42301ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 01/12/24 22:40 V42301ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 01/12/24 22:40 V42301ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 01/12/24 22:40 V42301ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 01/12/24 22:40 V42301ENM 8.49 µg/m3 0.136 1.80Ethyl Acetate 1 01/12/24 22:40 V42301ENM 64.6 µg/m3 0.106 2.17Ethylbenzene 1 01/12/24 22:40 V42301ENM 7.03 µg/m3 0.128 2.464-Ethyltoluene 1 01/12/24 22:40 V42301ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 01/12/24 22:40 V42301ENM 12.6 µg/m3 0.143 2.05Heptane 1 01/12/24 22:40 V42301ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 01/12/24 22:40 V42301ENM 8.25 µg/m3 0.047 1.76n-Hexane 1 01/12/24 22:40 V42301ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 01/12/24 22:40 V42301ENM 13.4 µg/m3 0.139 4.92Isopropyl Alcohol 1 01/12/24 22:40 V42301ENM 6.21 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 01/12/24 22:40 V42301ENM <0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 01/12/24 22:40 V42301ENM 1.15 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 01/12/24 22:40 V42301ENM 1.62 J µg/m3 0.488 1.74Methylene Chloride 1 01/12/24 22:40 V42301ENM 0.571 J µg/m3 0.183 2.62Naphthalene 1 01/12/24 22:40 V42301ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 48 of 59 , REPORT OF ANALYSISReport Number : Project Information : NC 28209 24-011-0012 00293 Hanley Environmental, PLLC 323 Manning Drive Nick Hotzelt Charlotte Danyale Love Project Manager Project #PJ23030 Received : 01/11/2024 Harrelson Ford Report Date : 01/24/2024 Sample ID : Lab No : Sampled:BF-SG-11 93805 Matrix: 1/11/2024 13:50 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V42291 01/12/24 09:00 V42362 01/11/24 09:00 12.1 µg/m3 0.242 0.860Propene 1 01/12/24 22:40 V42301ENM 0.583 J µg/m3 0.124 2.13Styrene 1 01/12/24 22:40 V42301ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 01/12/24 22:40 V42301ENM 0.813 J µg/m3 0.181 3.39Tetrachloroethene 1 01/12/24 22:40 V42301ENM 2.00 µg/m3 0.107 1.47Tetrahydrofuran 1 01/12/24 22:40 V42301ENM 323 µg/m3 1.80 37.7Toluene 20 01/12/24 04:53 V42369ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 01/12/24 22:40 V42301ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 01/12/24 22:40 V42301ENM <0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 01/12/24 22:40 V42301ENM <0.199 µg/m3 0.199 2.15Trichloroethene 1 01/12/24 22:40 V42301ENM 1.59 J µg/m3 0.130 2.81Trichlorofluoromethane 1 01/12/24 22:40 V42301ENM 19.4 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 01/12/24 22:40 V42301ENM 5.90 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 01/12/24 22:40 V42301ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 01/12/24 22:40 V42301ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 01/12/24 22:40 V42301ENM 42.1 µg/m3 0.157 2.17o-Xylene 1 01/12/24 22:40 V42301ENM 145 µg/m3 0.217 5.65m,p-Xylene 1 01/12/24 22:40 V42301ENM 187 µg/m3 0.157 2.17Xylene (Total)1 01/12/24 22:40 V42301 Surrogate: 4-Bromofluorobenzene 94.7 Limits: 70-130%01/12/24 22:401 ENM V42301 Surrogate: 4-Bromofluorobenzene 93.6 Limits: 70-130%01/12/24 04:5320 ENM V42369 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 49 of 59 Quality Control Data 24-011-0012Report No: Project Description: Client ID:Hanley Environmental, PLLC Harrelson Ford QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V42301QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V42291 Associated Lab Samples: 93794, 93795, 93796, 93797, 93798, 93799, 93800, 93801, 93802, 93803, 93804, 93805 LRB-V42291 Matrix: AIRLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 01/12/24 11:344.750.2020.382µg/m3Acetone 01/12/24 11:341.600.073<0.073µg/m3Benzene 01/12/24 11:3410.40.147<0.147µg/m3Benzyl Chloride 01/12/24 11:343.350.150<0.150µg/m3Bromodichloromethane 01/12/24 11:345.170.153<0.153µg/m3Bromoform 01/12/24 11:341.940.115<0.115µg/m3Bromomethane 01/12/24 11:341.110.328<0.328µg/m31,3-Butadiene 01/12/24 11:346.230.060<0.060µg/m3Carbon Disulfide 01/12/24 11:343.150.155<0.155µg/m3Carbon Tetrachloride 01/12/24 11:342.300.107<0.107µg/m3Chlorobenzene 01/12/24 11:344.260.208<0.208µg/m3Chlorodibromomethane 01/12/24 11:341.320.164<0.164µg/m3Chloroethane 01/12/24 11:342.440.086<0.086µg/m3Chloroform 01/12/24 11:341.030.067<0.067µg/m3Chloromethane 01/12/24 11:343.440.161<0.161µg/m3Cyclohexane 01/12/24 11:343.840.151<0.151µg/m31,2-Dibromoethane 01/12/24 11:343.010.096<0.096µg/m31,2-Dichlorobenzene 01/12/24 11:3412.00.174<0.174µg/m31,3-Dichlorobenzene 01/12/24 11:343.010.186<0.186µg/m31,4-Dichlorobenzene 01/12/24 11:342.470.134<0.134µg/m3Dichlorodifluoromethane 01/12/24 11:342.020.101<0.101µg/m31,1-Dichloroethane 01/12/24 11:342.020.129<0.129µg/m31,2-Dichloroethane 01/12/24 11:341.980.107<0.107µg/m31,1-Dichloroethene 01/12/24 11:341.980.095<0.095µg/m3cis-1,2-Dichloroethene 01/12/24 11:341.980.108<0.108µg/m3trans-1,2-Dichloroethene 01/12/24 11:342.310.205<0.205µg/m31,2-Dichloropropane 01/12/24 11:343.500.622<0.622µg/m31,2-Dichlorotetrafluoroethane Page 1 of 6Date:01/18/2024 04:27 PM Page 50 of 59 Quality Control Data 24-011-0012Report No: Project Description: Client ID:Hanley Environmental, PLLC Harrelson Ford QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V42301QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V42291 Associated Lab Samples: 93794, 93795, 93796, 93797, 93798, 93799, 93800, 93801, 93802, 93803, 93804, 93805 LRB-V42291 Matrix: AIRLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 01/12/24 11:342.270.178<0.178µg/m3cis-1,3-Dichloropropene 01/12/24 11:342.270.178<0.178µg/m3trans-1,3-Dichloropropene 01/12/24 11:341.800.435<0.435µg/m31,4-Dioxane 01/12/24 11:341.800.136<0.136µg/m3Ethyl Acetate 01/12/24 11:342.170.106<0.106µg/m3Ethylbenzene 01/12/24 11:342.460.128<0.128µg/m34-Ethyltoluene 01/12/24 11:343.830.561<0.561µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 01/12/24 11:342.050.143<0.143µg/m3Heptane 01/12/24 11:345.330.330<0.330µg/m3Hexachlorobutadiene 01/12/24 11:341.760.047<0.047µg/m3n-Hexane 01/12/24 11:342.050.285<0.285µg/m32-Hexanone 01/12/24 11:344.920.1390.612µg/m3Isopropyl Alcohol 01/12/24 11:341.470.224<0.224µg/m3Methyl Ethyl Ketone (MEK) 01/12/24 11:341.800.033<0.033µg/m3Methyl tert-butyl ether (MTBE) 01/12/24 11:342.050.121<0.121µg/m34-Methyl-2-Pentanone 01/12/24 11:341.740.488<0.488µg/m3Methylene Chloride 01/12/24 11:342.620.183<0.183µg/m3Naphthalene 01/12/24 11:340.8600.242<0.242µg/m3Propene 01/12/24 11:342.130.124<0.124µg/m3Styrene 01/12/24 11:343.430.104<0.104µg/m31,1,2,2-Tetrachloroethane 01/12/24 11:343.390.181<0.181µg/m3Tetrachloroethene 01/12/24 11:341.470.107<0.107µg/m3Tetrahydrofuran 01/12/24 11:341.880.090<0.090µg/m3Toluene 01/12/24 11:343.710.209<0.209µg/m31,2,4-Trichlorobenzene 01/12/24 11:342.730.144<0.144µg/m31,1,1-Trichloroethane 01/12/24 11:342.730.087<0.087µg/m31,1,2-Trichloroethane 01/12/24 11:342.150.199<0.199µg/m3Trichloroethene Page 2 of 6Date:01/18/2024 04:27 PM Page 51 of 59 Quality Control Data 24-011-0012Report No: Project Description: Client ID:Hanley Environmental, PLLC Harrelson Ford QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V42301QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V42291 Associated Lab Samples: 93794, 93795, 93796, 93797, 93798, 93799, 93800, 93801, 93802, 93803, 93804, 93805 LRB-V42291 Matrix: AIRLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 01/12/24 11:342.810.130<0.130µg/m3Trichlorofluoromethane 01/12/24 11:342.460.110<0.110µg/m31,2,4-Trimethylbenzene 01/12/24 11:342.460.236<0.236µg/m31,3,5-Trimethylbenzene 01/12/24 11:341.760.224<0.224µg/m3Vinyl Acetate 01/12/24 11:341.280.127<0.127µg/m3Vinyl Chloride 01/12/24 11:342.170.157<0.157µg/m3o-Xylene 01/12/24 11:345.650.217<0.217µg/m3m,p-Xylene 01/12/24 11:344-Bromofluorobenzene (S)89.9 70-130 LCS-V42291Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 10412.411.9µg/m3Acetone 70-130 99.315.916.0µg/m3Benzene 70-130 11028.525.9µg/m3Benzyl Chloride 70-130 99.733.433.5µg/m3Bromodichloromethane 70-130 10353.251.7µg/m3Bromoform 70-130 11021.419.4µg/m3Bromomethane 70-130 11312.511.1µg/m31,3-Butadiene 70-130 11217.515.6µg/m3Carbon Disulfide 70-130 97.130.631.5µg/m3Carbon Tetrachloride 70-130 10423.923.0µg/m3Chlorobenzene 70-130 10243.642.6µg/m3Chlorodibromomethane 70-130 11114.713.2µg/m3Chloroethane 70-130 10124.724.4µg/m3Chloroform 70-130 11712.010.3µg/m3Chloromethane 70-130 10417.917.2µg/m3Cyclohexane 70-130 Page 3 of 6Date:01/18/2024 04:27 PM Page 52 of 59 Quality Control Data 24-011-0012Report No: Project Description: Client ID:Hanley Environmental, PLLC Harrelson Ford QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V42301QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V42291 LCS-V42291Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 10540.338.4µg/m31,2-Dibromoethane 70-130 11033.230.1µg/m31,2-Dichlorobenzene 70-130 11233.630.1µg/m31,3-Dichlorobenzene 70-130 11133.530.1µg/m31,4-Dichlorobenzene 70-130 11027.224.7µg/m3Dichlorodifluoromethane 70-130 11322.920.2µg/m31,1-Dichloroethane 70-130 10220.720.2µg/m31,2-Dichloroethane 70-130 11322.319.8µg/m31,1-Dichloroethene 70-130 11422.519.8µg/m3cis-1,2-Dichloroethene 70-130 11522.719.8µg/m3trans-1,2-Dichloroethene 70-130 10123.423.1µg/m31,2-Dichloropropane 70-130 11138.735.0µg/m31,2-Dichlorotetrafluoroethane 70-130 10022.822.7µg/m3cis-1,3-Dichloropropene 70-130 97.722.222.7µg/m3trans-1,3-Dichloropropene 70-130 94.417.018.0µg/m31,4-Dioxane 70-130 10919.718.0µg/m3Ethyl Acetate 70-130 10522.821.7µg/m3Ethylbenzene 70-130 10926.724.6µg/m34-Ethyltoluene 70-130 11042.138.3µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 70-130 10521.520.5µg/m3Heptane 70-130 10555.853.3µg/m3Hexachlorobutadiene 70-130 11219.717.6µg/m3n-Hexane 70-130 10822.220.5µg/m32-Hexanone 70-130 10913.412.3µg/m3Isopropyl Alcohol 70-130 11116.514.8µg/m3Methyl Ethyl Ketone (MEK)70-130 10819.418.0µg/m3Methyl tert-butyl ether (MTBE)70-130 10321.220.5µg/m34-Methyl-2-Pentanone 70-130 Page 4 of 6Date:01/18/2024 04:27 PM Page 53 of 59 Quality Control Data 24-011-0012Report No: Project Description: Client ID:Hanley Environmental, PLLC Harrelson Ford QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V42301QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V42291 LCS-V42291Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 11019.117.4µg/m3Methylene Chloride 70-130 12031.426.2µg/m3Naphthalene 70-130 1129.638.61µg/m3Propene 70-130 10622.621.3µg/m3Styrene 70-130 10636.234.3µg/m31,1,2,2-Tetrachloroethane 70-130 97.933.233.9µg/m3Tetrachloroethene 70-130 10415.314.7µg/m3Tetrahydrofuran 70-130 99.418.718.8µg/m3Toluene 70-130 11643.037.1µg/m31,2,4-Trichlorobenzene 70-130 98.126.827.3µg/m31,1,1-Trichloroethane 70-130 10428.427.3µg/m31,1,2-Trichloroethane 70-130 98.526.526.9µg/m3Trichloroethene 70-130 11131.128.1µg/m3Trichlorofluoromethane 70-130 11327.824.6µg/m31,2,4-Trimethylbenzene 70-130 11127.224.6µg/m31,3,5-Trimethylbenzene 70-130 10117.717.6µg/m3Vinyl Acetate 70-130 11214.312.8µg/m3Vinyl Chloride 70-130 10723.221.7µg/m3o-Xylene 70-130 10646.243.4µg/m3m,p-Xylene 70-130 97.74-Bromofluorobenzene (S)70-130 Page 5 of 6Date:01/18/2024 04:27 PM Page 54 of 59 Quality Control Data 24-011-0012Report No: Project Description: Client ID:Hanley Environmental, PLLC Harrelson Ford QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V42369QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V42362 Associated Lab Samples: 93794, 93795, 93796, 93797, 93798, 93799, 93800, 93802, 93804, 93805 LRB-V42362 Matrix: AIRLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 01/11/24 17:421.880.090<0.090µg/m3Toluene 01/11/24 17:424-Bromofluorobenzene (S)93.0 70-130 LCS-V42362Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 96.218.118.8µg/m3Toluene 70-130 99.74-Bromofluorobenzene (S)70-130 Page 6 of 6Date:01/18/2024 04:27 PM Page 55 of 59 Fed Ex UPS US Postal Client Lab Courier Other : Shipment Receipt Form Customer Number: Customer Name: Report Number:24-011-0012 Hanley Environmental, PLLC 00293 Shipping Method Shipping container/cooler uncompromised? Thermometer ID:N/A Chain of Custody (COC) present?Yes No Yes No Not Present Yes No Not Present Yes No COC agrees with sample label(s)? Yes No COC properly completed Samples in proper containers? Sample containers intact? Sufficient sample volume for indicated test(s)? All samples received within holding time? Cooler temperature in compliance? Yes No Yes No Yes No Yes No Yes No Yes NoCooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Yes No N/A Yes No N/A Yes No N/ASoil VOA method 5035 – compliance criteria met Water - Sample containers properly preserved Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) High concentration container (48 hr) Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Number of coolers/boxes received Yes No 1 Signature:Angelo Norvell Date & Time:01/11/2024 14:14:59 Special precautions or instructions included? Comments: Page 56 of 59 Pa g e 5 7 o f 5 9 Pa g e 5 8 o f 5 9 Pa g e 5 9 o f 5 9 APPENDIX D Soil Boring Logs NOTES: generated using LOGitEASY.com Client: Project: Address: Tri Pointe Homes Harrelson Ford, PJ23030 6500 South Boulevard, Charlotte,NC WELL LOG Well No. Page: BF-SG-1 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 1/10/24 1/10/24 Hanley Environmental Hand Auger Rig JG JG Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (Lat, Long): 5 2.25 Grab N/A N/A N/A N/A Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: Hydrated Bent. Sand Pack DE P T H ( f t ) LI T H O L O G Y WA T E R L E V E L WE L L CO M P L E T I O N COLLECT Sa m p l e T y p e Ti m e Bl o w C o u n t s Re c o v e r y ( f t ) SOIL/ROCK VISUAL DESCRIPTION MEASURE PI D ( p p m ) La b S a m p l e DE P T H ( f t ) 0 5 10 GR 5.00 (0.00') Sandy SILT (ML); medium stiff, wet, light brown (1') As Above: moist (5.00') Boring terminated 0.7 0.5 0.6 0 5 10 Checked by: NH 5 0.1 1/4" Teflon Tubing 6" SS Screened Implant 35.1453086°, -080.8776233° NOTES: generated using LOGitEASY.com Client: Project: Address: Tri Pointe Homes Harrelson Ford, PJ23030 6500 South Boulevard, Charlotte,NC WELL LOG Well No. Page: BF-SG-2 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: JG JG Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (Lat, Long): 5 2.25 Grab N/A N/A N/A N/A Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5 0.1 DE P T H ( f t ) LI T H O L O G Y WA T E R L E V E L WE L L CO M P L E T I O N COLLECT Sa m p l e T y p e Ti m e Bl o w C o u n t s Re c o v e r y ( f t ) SOIL/ROCK VISUAL DESCRIPTION MEASURE PI D ( p p m ) La b S a m p l e DE P T H ( f t ) 0 5 10 GR 5.00 (0.00') Sandy SILT (ML); medium stiff, wet, light brown (1') As Above: moist (5.00') Boring terminated 1.1 1.4 0.9 0 5 10 Checked by: NH 1/4" Teflon Tubing 6" SS Screened Implant Hydrated Bent. Sand Pack 1/10/24 1/10/24 Hanley Environmental Hand Auger 35.1452888°, -080.8774353° NOTES: generated using LOGitEASY.com Client: Project: Address: Tri Pointe Homes Harrelson Ford, PJ23030 6500 South Boulevard, Charlotte,NC WELL LOG Well No. Page: BF-SG-3 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: JG JG Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (Lat, Long): 5 2.25 Grab N/A N/A N/A N/A Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5 0.1 DE P T H ( f t ) LI T H O L O G Y WA T E R L E V E L WE L L CO M P L E T I O N COLLECT Sa m p l e T y p e Ti m e Bl o w C o u n t s Re c o v e r y ( f t ) SOIL/ROCK VISUAL DESCRIPTION MEASURE PI D ( p p m ) La b S a m p l e DE P T H ( f t ) 0 5 10 GR 5.00 (0.00') Sandy SILT (ML); medium stiff, wet, light brown (1') As Above: moist (3.50') Silty CLAY (CL-ML); trace fine-medium sand, stiff, moist, reddish-brown (5.00') Boring terminated 0.5 1.1 0.8 0 5 10 Checked by: NH 1/4" Teflon Tubing 6" SS Screened Implant Hydrated Bent. Sand Pack 1/10/24 1/10/24 Hanley Environmental Hand Auger 35.1453157°, -080.8772969° NOTES: generated using LOGitEASY.com Client: Project: Address: Tri Pointe Homes Harrelson Ford, PJ23030 6500 South Boulevard, Charlotte,NC WELL LOG Well No. Page: BF-SG-4 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: JG JG Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (Lat, Long): 5 2.25 Grab N/A N/A N/A N/A Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5 0.1 DE P T H ( f t ) LI T H O L O G Y WA T E R L E V E L WE L L CO M P L E T I O N COLLECT Sa m p l e T y p e Ti m e Bl o w C o u n t s Re c o v e r y ( f t ) SOIL/ROCK VISUAL DESCRIPTION MEASURE PI D ( p p m ) La b S a m p l e DE P T H ( f t ) 0 5 10 GR 5.00 (0.00') Sandy SILT (ML); medium stiff, wet, light brown (1') As Above: moist, brown (3') natural organic matter (5.00') Boring terminated 1.2 0.9 1.2 0 5 10 Checked by: NH 1/4" Teflon Tubing 6" SS Screened Implant Hydrated Bent. Sand Pack 1/10/24 1/10/24 Hanley Environmental Hand Auger 35.1452144°, -080.8776696° NOTES: generated using LOGitEASY.com Client: Project: Address: Tri Pointe Homes Harrelson Ford, PJ23030 6500 South Boulevard, Charlotte,NC WELL LOG Well No. Page: BF-SG-5 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: JG JG Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (Lat, Long): 5 2.25 Grab N/A N/A N/A N/A Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5 0.1 DE P T H ( f t ) LI T H O L O G Y WA T E R L E V E L WE L L CO M P L E T I O N COLLECT Sa m p l e T y p e Ti m e Bl o w C o u n t s Re c o v e r y ( f t ) SOIL/ROCK VISUAL DESCRIPTION MEASURE PI D ( p p m ) La b S a m p l e DE P T H ( f t ) 0 5 10 GR 5.00 (0.00') Sandy SILT (ML); medium stiff, wet, light brown, trace gravel (1') As Above: moist (5.00') Boring terminated 2 1.6 1.4 0 5 10 Checked by: NH 1/4" Teflon Tubing 6" SS Screened Implant Hydrated Bent. Sand Pack 1/10/24 1/10/24 Hanley Environmental Hand Auger 35.1452157°, -080.8775242° NOTES: generated using LOGitEASY.com Client: Project: Address: Tri Pointe Homes Harrelson Ford, PJ23030 6500 South Boulevard, Charlotte,NC WELL LOG Well No. Page: BF-SG-6 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: JG JG Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (Lat, Long): 5 2.25 Grab N/A N/A N/A N/A Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5 0.1 DE P T H ( f t ) LI T H O L O G Y WA T E R L E V E L WE L L CO M P L E T I O N COLLECT Sa m p l e T y p e Ti m e Bl o w C o u n t s Re c o v e r y ( f t ) SOIL/ROCK VISUAL DESCRIPTION MEASURE PI D ( p p m ) La b S a m p l e DE P T H ( f t ) 0 5 10 GR 5.00 (0.00') Sandy SILT (ML); medium stiff, wet, light brown and brown (1') As Above: moist (5.00') Boring terminated 0.5 0.3 1 0 5 10 Checked by: NH 1/4" Teflon Tubing 6" SS Screened Implant HydratedBent. SandPack 1/10/24 1/10/24 Hanley Environmental Hand Auger 35.1448030°, -080.8774680° NOTES: generated using LOGitEASY.com Client: Project: Address: Tri Pointe Homes Harrelson Ford, PJ23030 6500 South Boulevard, Charlotte,NC WELL LOG Well No. Page: BF-SG-7 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: JG JG Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (Lat, Long): 5 2.25 Grab N/A N/A N/A N/A Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5 0.1 DE P T H ( f t ) LI T H O L O G Y WA T E R L E V E L WE L L CO M P L E T I O N COLLECT Sa m p l e T y p e Ti m e Bl o w C o u n t s Re c o v e r y ( f t ) SOIL/ROCK VISUAL DESCRIPTION MEASURE PI D ( p p m ) La b S a m p l e DE P T H ( f t ) 0 5 10 GR 5.00 (0.00') Sandy SILT (ML); medium stiff, wet, light brown (1') As Above: moist (5.00') Boring terminated 0.9 0.9 1.1 0 5 10 Checked by: NH 1/4" Teflon Tubing 6" SS Screened Implant Hydrated Bent. Sand Pack 1/10/24 1/10/24 Hanley Environmental Hand Auger 35.1448583°, -080.8774211° NOTES: generated using LOGitEASY.com Client: Project: Address: Tri Pointe Homes Harrelson Ford, PJ23030 6500 South Boulevard, Charlotte,NC WELL LOG Well No. Page: BF-SG-8 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: JG JG Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (Lat, Long): 5 2.25 Grab N/A N/A N/A N/A Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5 0.1 DE P T H ( f t ) LI T H O L O G Y WA T E R L E V E L WE L L CO M P L E T I O N COLLECT Sa m p l e T y p e Ti m e Bl o w C o u n t s Re c o v e r y ( f t ) SOIL/ROCK VISUAL DESCRIPTION MEASURE PI D ( p p m ) La b S a m p l e DE P T H ( f t ) 0 5 10 GR 5.00 (0.00') Sandy SILT (ML); medium stiff, wet, light brown (1') As Above: moist (5.00') Boring terminated 1.7 1.9 0.8 0 5 10 Checked by: NH 1/4" Teflon Tubing 6" SS Screened Implant Hydrated Bent. Sand Pack 1/10/24 1/10/24 Hanley Environmental Hand Auger 35.1448034°, -080.8773378° NOTES: generated using LOGitEASY.com Client: Project: Address: Tri Pointe Homes Harrelson Ford, PJ23030 6500 South Boulevard, Charlotte,NC WELL LOG Well No. Page: BF-SG-9 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: JG JG Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (Lat, Long): 5 2.25 Grab N/A N/A N/A N/A Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5 0.1 DE P T H ( f t ) LI T H O L O G Y WA T E R L E V E L WE L L CO M P L E T I O N COLLECT Sa m p l e T y p e Ti m e Bl o w C o u n t s Re c o v e r y ( f t ) SOIL/ROCK VISUAL DESCRIPTION MEASURE PI D ( p p m ) La b S a m p l e DE P T H ( f t ) 0 5 10 GR 5.00 (0.00') Sandy SILT (ML); medium stiff, wet, light brown, few coarse gravel (1') As Above: moist, no gravel (4.5') As Above: few clay (5.00') Boring terminated 0.4 0.6 1 0 5 10 Checked by: NH 1/4" Teflon Tubing 6" SS Screened Implant Hydrated Bent. Sand Pack 1/10/24 1/10/24 Hanley Environmental Hand Auger 35.1448501°, -080.8772972° NOTES: generated using LOGitEASY.com Client: Project: Address: Tri Pointe Homes Harrelson Ford, PJ23030 6500 South Boulevard, Charlotte,NC WELL LOG Well No. Page: BF-SG-10 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: JG JG Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (Lat, Long): 5 2.25 Grab N/A N/A N/A N/A Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5 0.1 DE P T H ( f t ) LI T H O L O G Y WA T E R L E V E L WE L L CO M P L E T I O N COLLECT Sa m p l e T y p e Ti m e Bl o w C o u n t s Re c o v e r y ( f t ) SOIL/ROCK VISUAL DESCRIPTION MEASURE PI D ( p p m ) La b S a m p l e DE P T H ( f t ) 0 5 10 GR 5.00 (0.00') Sandy SILT (ML); medium stiff, wet, light brown (1') As Above: moist (2.50') Sandy SILT (ML); trace coarse gravel, few clay, stiff, moist, brown (5.00') Boring terminated 1.4 0.9 0.9 0 5 10 Checked by: NH 1/4" Teflon Tubing 6" SS Screened Implant Hydrated Bent. Sand Pack 1/10/24 1/10/24 Hanley Environmental Hand Auger 35.1451309°, -080.8776216° NOTES: generated using LOGitEASY.com Client: Project: Address: Tri Pointe Homes Harrelson Ford, PJ23030 6500 South Boulevard, Charlotte,NC WELL LOG Well No. Page: BF-SG-11 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: JG JG Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (Lat, Long): 5 2.25 Grab N/A N/A N/A N/A Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5 0.1 DE P T H ( f t ) LI T H O L O G Y WA T E R L E V E L WE L L CO M P L E T I O N COLLECT Sa m p l e T y p e Ti m e Bl o w C o u n t s Re c o v e r y ( f t ) SOIL/ROCK VISUAL DESCRIPTION MEASURE PI D ( p p m ) La b S a m p l e DE P T H ( f t ) 0 5 10 GR 5.00 (0.00') Sandy SILT (ML); medium stiff, wet, light brown and brown (1') As Above: moist (2.5') trace gravel (5.00') Boring terminated 1.7 0.5 0.9 0 5 10 Checked by: NH 1/4" Teflon Tubing 6" SS Screened Implant Hydrated Bent. Sand Pack 1/10/24 1/10/24 Hanley Environmental Hand Auger 35.1448580°, -080.8771626° APPENDIX E Field Sampling Forms Sample Location ID:Date: Project Number:Field Personnel: Project Name:Weather: Sample Point Construction: Summa Canister ID:Flow Controller ID: Shut-In Test Duration:Shut-In Test Result: Shroud Helium Concentration:Volume Purged: Sample Helium Concentration: Sample Start Time:Sample End Time: Sample Start Vacuum:Sample End Vacuum: Comments: Soil Gas Sampling Record 16211 Pass 10:3610:26 12.1% 10 minutes 5552 1/11/2024BF-SG-1 6-inch stainless steel vapor monitoring implant with Teflon tubing installed PJ23030 Harrelson Ford to 5 feet below ground surface. One ft of sand and bentonite seal to surface. sunny 40s-50s F JG 1.1 liters 0.0 ppm Individually certified canister. Duplicate sample (BF-SG-DUP) collected concurrently using laboratory supplied "T" bar. -28" -5" Sample Location ID:Date: Project Number:Field Personnel: Project Name:Weather: Sample Point Construction: Summa Canister ID:Flow Controller ID: Shut-In Test Duration:Shut-In Test Result: Shroud Helium Concentration:Volume Purged: Sample Helium Concentration: Sample Start Time:Sample End Time: Sample Start Vacuum:Sample End Vacuum: Comments: Soil Gas Sampling Record 13135 Pass 10:5210:42 9.4% 10 minutes 5547 1/11/2024BF-SG-2 6-inch stainless steel vapor monitoring implant with Teflon tubing installed PJ23030 Harrelson Ford to 5 feet below ground surface. One ft of sand and bentonite seal to surface. sunny 40s-50s F JG 1.1 liters 0.0 ppm Individually certified canister. -28" -4" Sample Location ID:Date: Project Number:Field Personnel: Project Name:Weather: Sample Point Construction: Summa Canister ID:Flow Controller ID: Shut-In Test Duration:Shut-In Test Result: Shroud Helium Concentration:Volume Purged: Sample Helium Concentration: Sample Start Time:Sample End Time: Sample Start Vacuum:Sample End Vacuum: Comments: Soil Gas Sampling Record 6562 Pass 11:0810:58 11.0% 10 minutes 5901 1/11/2024BF-SG-3 6-inch stainless steel vapor monitoring implant with Teflon tubing installed PJ23030 Harrelson Ford to 5 feet below ground surface. One ft of sand and bentonite seal to surface. sunny 40s-50s F JG 1.1 liters 0.0 ppm Individually certified canister. -28" -5" Sample Location ID:Date: Project Number:Field Personnel: Project Name:Weather: Sample Point Construction: Summa Canister ID:Flow Controller ID: Shut-In Test Duration:Shut-In Test Result: Shroud Helium Concentration:Volume Purged: Sample Helium Concentration: Sample Start Time:Sample End Time: Sample Start Vacuum:Sample End Vacuum: Comments: Soil Gas Sampling Record 6561 Pass 11:2411:14 9.6% 10 minutes 6007 1/11/2024BF-SG-4 6-inch stainless steel vapor monitoring implant with Teflon tubing installed PJ23030 Harrelson Ford to 5 feet below ground surface. One ft of sand and bentonite seal to surface. sunny 40s-50s F JG 1.1 liters 0.0 ppm Individually certified canister. -27" -5" Sample Location ID:Date: Project Number:Field Personnel: Project Name:Weather: Sample Point Construction: Summa Canister ID:Flow Controller ID: Shut-In Test Duration:Shut-In Test Result: Shroud Helium Concentration:Volume Purged: Sample Helium Concentration: Sample Start Time:Sample End Time: Sample Start Vacuum:Sample End Vacuum: Comments: Soil Gas Sampling Record 5962 Pass 11:4011:30 9.1% 10 minutes 6569 1/11/2024BF-SG-5 6-inch stainless steel vapor monitoring implant with Teflon tubing installed PJ23030 Harrelson Ford to 5 feet below ground surface. One ft of sand and bentonite seal to surface. sunny 40s-50s F JG 1.1 liters 0.0 ppm Individually certified canister. -28" -4" Sample Location ID:Date: Project Number:Field Personnel: Project Name:Weather: Sample Point Construction: Summa Canister ID:Flow Controller ID: Shut-In Test Duration:Shut-In Test Result: Shroud Helium Concentration:Volume Purged: Sample Helium Concentration: Sample Start Time:Sample End Time: Sample Start Vacuum:Sample End Vacuum: Comments: Soil Gas Sampling Record 14301 Pass 12:4012:30 10.0% 10 minutes 11362 1/11/2024BF-SG-6 6-inch stainless steel vapor monitoring implant with Teflon tubing installed PJ23030 Harrelson Ford to 5 feet below ground surface. One ft of sand and bentonite seal to surface. sunny 40s-50s F JG 1.1 liters 0.0 ppm Individually certified canister. -28" -5" Sample Location ID:Date: Project Number:Field Personnel: Project Name:Weather: Sample Point Construction: Summa Canister ID:Flow Controller ID: Shut-In Test Duration:Shut-In Test Result: Shroud Helium Concentration:Volume Purged: Sample Helium Concentration: Sample Start Time:Sample End Time: Sample Start Vacuum:Sample End Vacuum: Comments: sunny 40s-50s F JG 1.1 liters 0.0 ppm Individually certified canister. -28" -5" Soil Gas Sampling Record 13109 Pass 13:0012:50 10.8% 10 minutes 13702 1/11/2024BF-SG-7 6-inch stainless steel vapor monitoring implant with Teflon tubing installed PJ23030 Harrelson Ford to 5 feet below ground surface. One ft of sand and bentonite seal to surface. Sample Location ID:Date: Project Number:Field Personnel: Project Name:Weather: Sample Point Construction: Summa Canister ID:Flow Controller ID: Shut-In Test Duration:Shut-In Test Result: Shroud Helium Concentration:Volume Purged: Sample Helium Concentration: Sample Start Time:Sample End Time: Sample Start Vacuum:Sample End Vacuum: Comments: sunny 40s-50s F JG 1.1 liters 0.0 ppm Individually certified canister. -28" -5" Soil Gas Sampling Record 14302 Pass 13:1613:06 9.7% 10 minutes 11359 1/11/2024BF-SG-8 6-inch stainless steel vapor monitoring implant with Teflon tubing installed PJ23030 Harrelson Ford to 5 feet below ground surface. One ft of sand and bentonite seal to surface. Sample Location ID:Date: Project Number:Field Personnel: Project Name:Weather: Sample Point Construction: Summa Canister ID:Flow Controller ID: Shut-In Test Duration:Shut-In Test Result: Shroud Helium Concentration:Volume Purged: Sample Helium Concentration: Sample Start Time:Sample End Time: Sample Start Vacuum:Sample End Vacuum: Comments: sunny 40s-50s F JG 1.1 liters 0.0 ppm Individually certified canister. -28" -5" Soil Gas Sampling Record 13128 Pass 13:4013:30 9.1% 10 minutes 15647 1/11/2024BF-SG-9 6-inch stainless steel vapor monitoring implant with Teflon tubing installed PJ23030 Harrelson Ford to 5 feet below ground surface. One ft of sand and bentonite seal to surface. Sample Location ID:Date: Project Number:Field Personnel: Project Name:Weather: Sample Point Construction: Summa Canister ID:Flow Controller ID: Shut-In Test Duration:Shut-In Test Result: Shroud Helium Concentration:Volume Purged: Sample Helium Concentration: Sample Start Time:Sample End Time: Sample Start Vacuum:Sample End Vacuum: Comments: sunny 40s-50s F JG 1.1 liters 0.0 ppm Individually certified canister. -28" -5" Soil Gas Sampling Record 13137 Pass 12:1012:00 10.4% 10 minutes 13690 1/11/2024BF-SG-10 6-inch stainless steel vapor monitoring implant with Teflon tubing installed PJ23030 Harrelson Ford to 5 feet below ground surface. One ft of sand and bentonite seal to surface. Sample Location ID:Date: Project Number:Field Personnel: Project Name:Weather: Sample Point Construction: Summa Canister ID:Flow Controller ID: Shut-In Test Duration:Shut-In Test Result: Shroud Helium Concentration:Volume Purged: Sample Helium Concentration: Sample Start Time:Sample End Time: Sample Start Vacuum:Sample End Vacuum: Comments: sunny 40s-50s F JG 1.1 liters 0.0 ppm Individually certified canister. -28" -5" Soil Gas Sampling Record 16229 Pass 14:0013:50 10.0% 10 minutes 6010 1/11/2024BF-SG-11 6-inch stainless steel vapor monitoring implant with Teflon tubing installed PJ23030 Harrelson Ford to 5 feet below ground surface. One ft of sand and bentonite seal to surface. APPENDIX F Risk Calculator Outputs DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: BF-SG-1 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 21.7 0.651 -- 71-43-2 Benzene 75.8 2.274 3.6E-01 6.3E+00 6.3E-06 7.3E-02 75-15-0 Carbon Disulfide 20.6 0.618 -1.5E+02 8.5E-04 56-23-5 Carbon Tetrachloride 0.905 0.02715 4.7E-01 2.1E+01 5.8E-08 2.6E-04 67-66-3 Chloroform 1.7 0.051 1.2E-01 2.0E+01 4.2E-07 5.0E-04 75-71-8 Dichlorodifluoromethane 2.49 0.0747 -2.1E+01 7.2E-04 75-34-3 Dichloroethane, 1,1-1.8 0.054 1.8E+00 -3.1E-08 75-35-4 Dichloroethylene, 1,1-2.66 0.0798 -4.2E+01 3.8E-04 156-59-2 Dichloroethylene, cis-1,2-71.9 2.157 -8.3E+00 5.2E-02 156-60-5 Dichloroethylene, trans-1,2-2.36 0.0708 -8.3E+00 1.7E-03 141-78-6 Ethyl Acetate 26.4 0.792 -1.5E+01 1.1E-02 100-41-4 Ethylbenzene 58.2 1.746 1.1E+00 2.1E+02 1.6E-06 1.7E-03 109-99-9 ~Tetrahydrofuran 23.5 0.705 -4.2E+02 3.4E-04 142-82-5 Heptane, N-31.7 0.951 -8.3E+01 2.3E-03 110-54-3 Hexane, N-17 0.51 -1.5E+02 7.0E-04 67-63-0 Isopropanol 2.26 0.0678 -4.2E+01 3.3E-04 78-93-3 Methyl Ethyl Ketone (2-Butanone)5.62 0.1686 -1.0E+03 3.2E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)3.15 0.0945 -6.3E+02 3.0E-05 1634-04-4 Methyl tert-Butyl Ether (MTBE)26.2 0.786 1.1E+01 6.3E+02 7.3E-08 2.5E-04 75-09-2 Methylene Chloride 3.75 0.1125 1.0E+02 1.3E+02 1.1E-09 1.8E-04 91-20-3 ~Naphthalene 4.57 0.1371 8.3E-02 6.3E-01 1.7E-06 4.4E-02 115-07-1 Propylene 3.67 0.1101 - 6.3E+02 3.5E-05 100-42-5 Styrene 0.685 0.02055 -2.1E+02 2.0E-05 127-18-4 Tetrachloroethylene 106 3.18 1.1E+01 8.3E+00 2.9E-07 7.6E-02 108-88-3 Toluene 345 10.35 -1.0E+03 2.0E-03 79-01-6 Trichloroethylene 117 3.51 4.8E-01 4.2E-01 7.3E-06 1.7E+00 75-69-4 Trichlorofluoromethane 1.57 0.0471 -- 95-63-6 Trimethylbenzene, 1,2,4-24.8 0.744 -1.3E+01 1.2E-02 108-67-8 Trimethylbenzene, 1,3,5-6.81 0.2043 -1.3E+01 3.3E-03 75-01-4 Vinyl Chloride 1.9 0.057 1.7E-01 2.1E+01 3.4E-07 5.5E-04 1330-20-7 Xylenes 177 5.31 -2.1E+01 5.1E-02 Cumulative: 1.8E-05 2.0E+00 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: BF-SG-2 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 24.6 0.738 -- 71-43-2 Benzene 41.1 1.233 3.6E-01 6.3E+00 3.4E-06 3.9E-02 75-27-4 Bromodichloromethane 5.08 0.1524 7.6E-02 -2.0E-06 75-15-0 Carbon Disulfide 7.19 0.2157 -1.5E+02 3.0E-04 67-66-3 Chloroform 45.2 1.356 1.2E-01 2.0E+01 1.1E-05 1.3E-02 106-46-7 Dichlorobenzene, 1,4-0.625 0.01875 2.6E-01 1.7E+02 7.3E-08 2.2E-05 75-71-8 Dichlorodifluoromethane 2.49 0.0747 -2.1E+01 7.2E-04 156-59-2 Dichloroethylene, cis-1,2-0.376 0.01128 -8.3E+00 2.7E-04 141-78-6 Ethyl Acetate 14.3 0.429 -1.5E+01 5.9E-03 100-41-4 Ethylbenzene 74.4 2.232 1.1E+00 2.1E+02 2.0E-06 2.1E-03 109-99-9 ~Tetrahydrofuran 1.89 0.0567 -4.2E+02 2.7E-05 142-82-5 Heptane, N-15.3 0.459 -8.3E+01 1.1E-03 110-54-3 Hexane, N-3.71 0.1113 -1.5E+02 1.5E-04 67-63-0 Isopropanol 2.11 0.0633 -4.2E+01 3.0E-04 78-93-3 Methyl Ethyl Ketone (2-Butanone)4.66 0.1398 -1.0E+03 2.7E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)1.54 0.0462 -6.3E+02 1.5E-05 1634-04-4 Methyl tert-Butyl Ether (MTBE)1.71 0.0513 1.1E+01 6.3E+02 4.8E-09 1.6E-05 75-09-2 Methylene Chloride 2.9 0.087 1.0E+02 1.3E+02 8.6E-10 1.4E-04 91-20-3 ~Naphthalene 1.45 0.0435 8.3E-02 6.3E-01 5.3E-07 1.4E-02 115-07-1 Propylene 1.94 0.0582 - 6.3E+02 1.9E-05 100-42-5 Styrene 1 0.03 -2.1E+02 2.9E-05 127-18-4 Tetrachloroethylene 24 0.72 1.1E+01 8.3E+00 6.7E-08 1.7E-02 108-88-3 Toluene 356 10.68 -1.0E+03 2.0E-03 79-01-6 Trichloroethylene 5.64 0.1692 4.8E-01 4.2E-01 3.5E-07 8.1E-02 75-69-4 Trichlorofluoromethane 1.53 0.0459 -- 95-63-6 Trimethylbenzene, 1,2,4-41 1.23 -1.3E+01 2.0E-02 108-67-8 Trimethylbenzene, 1,3,5-10.4 0.312 -1.3E+01 5.0E-03 1330-20-7 Xylenes 226 6.78 -2.1E+01 6.5E-02 Cumulative: 2.0E-05 2.7E-01 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: BF-SG-3 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 29.8 0.894 -- 71-43-2 Benzene 23.4 0.702 3.6E-01 6.3E+00 2.0E-06 2.2E-02 75-15-0 Carbon Disulfide 10.9 0.327 -1.5E+02 4.5E-04 67-66-3 Chloroform 1.04 0.0312 1.2E-01 2.0E+01 2.6E-07 3.1E-04 75-71-8 Dichlorodifluoromethane 2.52 0.0756 -2.1E+01 7.2E-04 141-78-6 Ethyl Acetate 3.52 0.1056 -1.5E+01 1.4E-03 100-41-4 Ethylbenzene 44.9 1.347 1.1E+00 2.1E+02 1.2E-06 1.3E-03 109-99-9 ~Tetrahydrofuran 2.48 0.0744 -4.2E+02 3.6E-05 142-82-5 Heptane, N-15.4 0.462 -8.3E+01 1.1E-03 110-54-3 Hexane, N-8.21 0.2463 -1.5E+02 3.4E-04 67-63-0 Isopropanol 1.91 0.0573 -4.2E+01 2.7E-04 78-93-3 Methyl Ethyl Ketone (2-Butanone)5 0.15 -1.0E+03 2.9E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)0.991 0.02973 -6.3E+02 9.5E-06 75-09-2 Methylene Chloride 3.22 0.0966 1.0E+02 1.3E+02 9.5E-10 1.5E-04 91-20-3 ~Naphthalene 0.739 0.02217 8.3E-02 6.3E-01 2.7E-07 7.1E-03 115-07-1 Propylene 5.81 0.1743 - 6.3E+02 5.6E-05 100-42-5 Styrene 0.621 0.01863 -2.1E+02 1.8E-05 127-18-4 Tetrachloroethylene 12.4 0.372 1.1E+01 8.3E+00 3.4E-08 8.9E-03 108-88-3 Toluene 232 6.96 -1.0E+03 1.3E-03 75-69-4 Trichlorofluoromethane 1.51 0.0453 -- 95-63-6 Trimethylbenzene, 1,2,4-19.7 0.591 -1.3E+01 9.4E-03 108-67-8 Trimethylbenzene, 1,3,5-5.12 0.1536 -1.3E+01 2.5E-03 1330-20-7 Xylenes 135 4.05 -2.1E+01 3.9E-02 Cumulative: 3.7E-06 9.7E-02 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: BF-SG-4 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 76.2 2.286 -- 71-43-2 Benzene 16.4 0.492 3.6E-01 6.3E+00 1.4E-06 1.6E-02 75-15-0 Carbon Disulfide 2.49 0.0747 -1.5E+02 1.0E-04 67-66-3 Chloroform 4.21 0.1263 1.2E-01 2.0E+01 1.0E-06 1.2E-03 75-71-8 Dichlorodifluoromethane 2.56 0.0768 -2.1E+01 7.4E-04 141-78-6 Ethyl Acetate 4.3 0.129 -1.5E+01 1.8E-03 100-41-4 Ethylbenzene 49.4 1.482 1.1E+00 2.1E+02 1.3E-06 1.4E-03 109-99-9 ~Tetrahydrofuran 2.46 0.0738 -4.2E+02 3.5E-05 142-82-5 Heptane, N-2.36 0.0708 -8.3E+01 1.7E-04 110-54-3 Hexane, N-1.02 0.0306 -1.5E+02 4.2E-05 591-78-6 Hexanone, 2-2.42 0.0726 -6.3E+00 2.3E-03 67-63-0 Isopropanol 9.89 0.2967 -4.2E+01 1.4E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)13.3 0.399 -1.0E+03 7.7E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)9.89 0.2967 -6.3E+02 9.5E-05 1634-04-4 Methyl tert-Butyl Ether (MTBE)4.04 0.1212 1.1E+01 6.3E+02 1.1E-08 3.9E-05 75-09-2 Methylene Chloride 2.83 0.0849 1.0E+02 1.3E+02 8.4E-10 1.4E-04 115-07-1 Propylene 3.17 0.0951 - 6.3E+02 3.0E-05 100-42-5 Styrene 0.46 0.0138 -2.1E+02 1.3E-05 127-18-4 Tetrachloroethylene 3.82 0.1146 1.1E+01 8.3E+00 1.1E-08 2.7E-03 108-88-3 Toluene 250 7.5 -1.0E+03 1.4E-03 75-69-4 Trichlorofluoromethane 1.59 0.0477 -- 95-63-6 Trimethylbenzene, 1,2,4-15 0.45 -1.3E+01 7.2E-03 108-67-8 Trimethylbenzene, 1,3,5-4.32 0.1296 -1.3E+01 2.1E-03 1330-20-7 Xylenes 147 4.41 -2.1E+01 4.2E-02 Cumulative: 3.7E-06 8.1E-02 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: BF-SG-5 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 103 3.09 -- 71-43-2 Benzene 32.8 0.984 3.6E-01 6.3E+00 2.7E-06 3.1E-02 75-15-0 Carbon Disulfide 8.38 0.2514 -1.5E+02 3.4E-04 67-66-3 Chloroform 10.6 0.318 1.2E-01 2.0E+01 2.6E-06 3.1E-03 75-71-8 Dichlorodifluoromethane 2.46 0.0738 -2.1E+01 7.1E-04 141-78-6 Ethyl Acetate 5.52 0.1656 -1.5E+01 2.3E-03 100-41-4 Ethylbenzene 60.2 1.806 1.1E+00 2.1E+02 1.6E-06 1.7E-03 109-99-9 ~Tetrahydrofuran 1.03 0.0309 -4.2E+02 1.5E-05 142-82-5 Heptane, N-17.9 0.537 -8.3E+01 1.3E-03 110-54-3 Hexane, N-5.86 0.1758 -1.5E+02 2.4E-04 67-63-0 Isopropanol 14.1 0.423 -4.2E+01 2.0E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)16.7 0.501 -1.0E+03 9.6E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)2.3 0.069 -6.3E+02 2.2E-05 1634-04-4 Methyl tert-Butyl Ether (MTBE)3.45 0.1035 1.1E+01 6.3E+02 9.6E-09 3.3E-05 75-09-2 Methylene Chloride 2.57 0.0771 1.0E+02 1.3E+02 7.6E-10 1.2E-04 91-20-3 ~Naphthalene 0.995 0.02985 8.3E-02 6.3E-01 3.6E-07 9.5E-03 115-07-1 Propylene 5.22 0.1566 - 6.3E+02 5.0E-05 100-42-5 Styrene 0.655 0.01965 -2.1E+02 1.9E-05 127-18-4 Tetrachloroethylene 0.773 0.02319 1.1E+01 8.3E+00 2.1E-09 5.6E-04 108-88-3 Toluene 333 9.99 -1.0E+03 1.9E-03 75-69-4 Trichlorofluoromethane 1.43 0.0429 -- 95-63-6 Trimethylbenzene, 1,2,4-23.7 0.711 -1.3E+01 1.1E-02 108-67-8 Trimethylbenzene, 1,3,5-6.41 0.1923 -1.3E+01 3.1E-03 1330-20-7 Xylenes 180 5.4 -2.1E+01 5.2E-02 Cumulative: 7.3E-06 1.2E-01 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: BF-SG-6 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 31.7 0.951 -- 71-43-2 Benzene 22.2 0.666 3.6E-01 6.3E+00 1.9E-06 2.1E-02 75-15-0 Carbon Disulfide 4.65 0.1395 -1.5E+02 1.9E-04 67-66-3 Chloroform 0.912 0.02736 1.2E-01 2.0E+01 2.2E-07 2.7E-04 75-71-8 Dichlorodifluoromethane 2.5 0.075 -2.1E+01 7.2E-04 156-59-2 Dichloroethylene, cis-1,2-0.781 0.02343 -8.3E+00 5.6E-04 141-78-6 Ethyl Acetate 2.06 0.0618 -1.5E+01 8.5E-04 100-41-4 Ethylbenzene 38.9 1.167 1.1E+00 2.1E+02 1.0E-06 1.1E-03 109-99-9 ~Tetrahydrofuran 6.68 0.2004 -4.2E+02 9.6E-05 142-82-5 Heptane, N-14.6 0.438 -8.3E+01 1.1E-03 110-54-3 Hexane, N-9.45 0.2835 -1.5E+02 3.9E-04 67-63-0 Isopropanol 39 1.17 -4.2E+01 5.6E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)5.03 0.1509 -1.0E+03 2.9E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)1.61 0.0483 -6.3E+02 1.5E-05 75-09-2 Methylene Chloride 2.06 0.0618 1.0E+02 1.3E+02 6.1E-10 9.9E-05 91-20-3 ~Naphthalene 0.571 0.01713 8.3E-02 6.3E-01 2.1E-07 5.5E-03 115-07-1 Propylene 2.74 0.0822 - 6.3E+02 2.6E-05 100-42-5 Styrene 0.587 0.01761 -2.1E+02 1.7E-05 127-18-4 Tetrachloroethylene 5.94 0.1782 1.1E+01 8.3E+00 1.7E-08 4.3E-03 108-88-3 Toluene 194 5.82 -1.0E+03 1.1E-03 75-69-4 Trichlorofluoromethane 1.48 0.0444 -- 95-63-6 Trimethylbenzene, 1,2,4-16.8 0.504 -1.3E+01 8.1E-03 108-67-8 Trimethylbenzene, 1,3,5-4.39 0.1317 -1.3E+01 2.1E-03 1330-20-7 Xylenes 116 3.48 -2.1E+01 3.3E-02 Cumulative: 3.3E-06 8.7E-02 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: BF-SG-7 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 11.5 0.345 -- 71-43-2 Benzene 5.05 0.1515 3.6E-01 6.3E+00 4.2E-07 4.8E-03 75-15-0 Carbon Disulfide 3.97 0.1191 -1.5E+02 1.6E-04 75-71-8 Dichlorodifluoromethane 2.77 0.0831 -2.1E+01 8.0E-04 141-78-6 Ethyl Acetate 5.87 0.1761 -1.5E+01 2.4E-03 100-41-4 Ethylbenzene 7.12 0.2136 1.1E+00 2.1E+02 1.9E-07 2.0E-04 109-99-9 ~Tetrahydrofuran 8.45 0.2535 -4.2E+02 1.2E-04 142-82-5 Heptane, N-3.13 0.0939 -8.3E+01 2.3E-04 110-54-3 Hexane, N-5.78 0.1734 -1.5E+02 2.4E-04 591-78-6 Hexanone, 2-3.88 0.1164 -6.3E+00 3.7E-03 67-63-0 Isopropanol 19.7 0.591 -4.2E+01 2.8E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)3.5 0.105 -1.0E+03 2.0E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)1.58 0.0474 -6.3E+02 1.5E-05 75-09-2 Methylene Chloride 1.16 0.0348 1.0E+02 1.3E+02 3.4E-10 5.6E-05 91-20-3 ~Naphthalene 0.56 0.0168 8.3E-02 6.3E-01 2.0E-07 5.4E-03 115-07-1 Propylene 4.63 0.1389 - 6.3E+02 4.4E-05 127-18-4 Tetrachloroethylene 8.47 0.2541 1.1E+01 8.3E+00 2.4E-08 6.1E-03 108-88-3 Toluene 49 1.47 -1.0E+03 2.8E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-0.567 0.01701 -1.0E+03 3.3E-06 79-01-6 Trichloroethylene 0.607 0.01821 4.8E-01 4.2E-01 3.8E-08 8.7E-03 75-69-4 Trichlorofluoromethane 2.07 0.0621 -- 95-63-6 Trimethylbenzene, 1,2,4-2.51 0.0753 -1.3E+01 1.2E-03 108-67-8 Trimethylbenzene, 1,3,5-0.688 0.02064 -1.3E+01 3.3E-04 1330-20-7 Xylenes 19 0.57 -2.1E+01 5.5E-03 Cumulative: 8.8E-07 4.3E-02 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: BF-SG-8 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 44.2 1.326 -- 71-43-2 Benzene 28.7 0.861 3.6E-01 6.3E+00 2.4E-06 2.8E-02 75-15-0 Carbon Disulfide 12.4 0.372 -1.5E+02 5.1E-04 67-66-3 Chloroform 1.74 0.0522 1.2E-01 2.0E+01 4.3E-07 5.1E-04 75-71-8 Dichlorodifluoromethane 2.5 0.075 -2.1E+01 7.2E-04 156-59-2 Dichloroethylene, cis-1,2-9.42 0.2826 -8.3E+00 6.8E-03 100-41-4 Ethylbenzene 52.6 1.578 1.1E+00 2.1E+02 1.4E-06 1.5E-03 109-99-9 ~Tetrahydrofuran 51.5 1.545 -4.2E+02 7.4E-04 142-82-5 Heptane, N-8.68 0.2604 -8.3E+01 6.2E-04 110-54-3 Hexane, N-7.5 0.225 -1.5E+02 3.1E-04 67-63-0 Isopropanol 18.8 0.564 -4.2E+01 2.7E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)12.2 0.366 -1.0E+03 7.0E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)2.15 0.0645 -6.3E+02 2.1E-05 1634-04-4 Methyl tert-Butyl Ether (MTBE)1.15 0.0345 1.1E+01 6.3E+02 3.2E-09 1.1E-05 75-09-2 Methylene Chloride 2.8 0.084 1.0E+02 1.3E+02 8.3E-10 1.3E-04 115-07-1 Propylene 60.5 1.815 - 6.3E+02 5.8E-04 100-42-5 Styrene 0.6 0.018 -2.1E+02 1.7E-05 127-18-4 Tetrachloroethylene 17.5 0.525 1.1E+01 8.3E+00 4.9E-08 1.3E-02 108-88-3 Toluene 288 8.64 -1.0E+03 1.7E-03 79-01-6 Trichloroethylene 2.55 0.0765 4.8E-01 4.2E-01 1.6E-07 3.7E-02 75-69-4 Trichlorofluoromethane 1.57 0.0471 -- 95-63-6 Trimethylbenzene, 1,2,4-15.5 0.465 -1.3E+01 7.4E-03 108-67-8 Trimethylbenzene, 1,3,5-4.97 0.1491 -1.3E+01 2.4E-03 1330-20-7 Xylenes 149 4.47 -2.1E+01 4.3E-02 Cumulative: 4.4E-06 1.5E-01 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: BF-SG-9 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 9.78 0.2934 -- 71-43-2 Benzene 1.24 0.0372 3.6E-01 6.3E+00 1.0E-07 1.2E-03 75-15-0 Carbon Disulfide 0.504 0.01512 -1.5E+02 2.1E-05 67-66-3 Chloroform 1.07 0.0321 1.2E-01 2.0E+01 2.6E-07 3.1E-04 75-71-8 Dichlorodifluoromethane 2.6 0.078 -2.1E+01 7.5E-04 75-35-4 Dichloroethylene, 1,1-0.729 0.02187 -4.2E+01 1.0E-04 156-59-2 Dichloroethylene, cis-1,2-13.1 0.393 -8.3E+00 9.4E-03 100-41-4 Ethylbenzene 0.62 0.0186 1.1E+00 2.1E+02 1.7E-08 1.8E-05 109-99-9 ~Tetrahydrofuran 0.333 0.00999 -4.2E+02 4.8E-06 142-82-5 Heptane, N-0.385 0.01155 -8.3E+01 2.8E-05 110-54-3 Hexane, N-0.782 0.02346 -1.5E+02 3.2E-05 67-63-0 Isopropanol 15.9 0.477 -4.2E+01 2.3E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)1.58 0.0474 -1.0E+03 9.1E-06 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)0.634 0.01902 -6.3E+02 6.1E-06 75-09-2 Methylene Chloride 1.26 0.0378 1.0E+02 1.3E+02 3.7E-10 6.0E-05 115-07-1 Propylene 77.1 2.313 - 6.3E+02 7.4E-04 127-18-4 Tetrachloroethylene 266 7.98 1.1E+01 8.3E+00 7.4E-07 1.9E-01 108-88-3 Toluene 4.47 0.1341 -1.0E+03 2.6E-05 79-01-6 Trichloroethylene 44.4 1.332 4.8E-01 4.2E-01 2.8E-06 6.4E-01 75-69-4 Trichlorofluoromethane 1.64 0.0492 -- 1330-20-7 Xylenes 2.04 0.0612 -2.1E+01 5.9E-04 Cumulative: 3.9E-06 8.5E-01 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: BF-SG-10 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 64.5 1.935 -- 71-43-2 Benzene 27.7 0.831 3.6E-01 6.3E+00 2.3E-06 2.7E-02 75-15-0 Carbon Disulfide 37.3 1.119 -1.5E+02 1.5E-03 67-66-3 Chloroform 1.15 0.0345 1.2E-01 2.0E+01 2.8E-07 3.4E-04 110-82-7 Cyclohexane 7.34 0.2202 -1.3E+03 3.5E-05 75-71-8 Dichlorodifluoromethane 2.47 0.0741 -2.1E+01 7.1E-04 75-35-4 Dichloroethylene, 1,1-1.32 0.0396 -4.2E+01 1.9E-04 156-59-2 Dichloroethylene, cis-1,2-15.8 0.474 -8.3E+00 1.1E-02 156-60-5 Dichloroethylene, trans-1,2-0.693 0.02079 -8.3E+00 5.0E-04 141-78-6 Ethyl Acetate 12.3 0.369 -1.5E+01 5.1E-03 100-41-4 Ethylbenzene 47.9 1.437 1.1E+00 2.1E+02 1.3E-06 1.4E-03 109-99-9 ~Tetrahydrofuran 4.73 0.1419 -4.2E+02 6.8E-05 142-82-5 Heptane, N-19.2 0.576 -8.3E+01 1.4E-03 110-54-3 Hexane, N-12.1 0.363 -1.5E+02 5.0E-04 67-63-0 Isopropanol 13.4 0.402 -4.2E+01 1.9E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)16.3 0.489 -1.0E+03 9.4E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)1.67 0.0501 -6.3E+02 1.6E-05 1634-04-4 Methyl tert-Butyl Ether (MTBE)0.767 0.02301 1.1E+01 6.3E+02 2.1E-09 7.4E-06 75-09-2 Methylene Chloride 2.35 0.0705 1.0E+02 1.3E+02 7.0E-10 1.1E-04 91-20-3 ~Naphthalene 0.566 0.01698 8.3E-02 6.3E-01 2.1E-07 5.4E-03 115-07-1 Propylene 23 0.69 - 6.3E+02 2.2E-04 100-42-5 Styrene 0.54 0.0162 -2.1E+02 1.6E-05 127-18-4 Tetrachloroethylene 17.1 0.513 1.1E+01 8.3E+00 4.8E-08 1.2E-02 108-88-3 Toluene 244 7.32 -1.0E+03 1.4E-03 79-01-6 Trichloroethylene 8.19 0.2457 4.8E-01 4.2E-01 5.1E-07 1.2E-01 75-69-4 Trichlorofluoromethane 1.46 0.0438 -- 95-63-6 Trimethylbenzene, 1,2,4-15.2 0.456 -1.3E+01 7.3E-03 108-67-8 Trimethylbenzene, 1,3,5-4.51 0.1353 -1.3E+01 2.2E-03 1330-20-7 Xylenes 140 4.2 -2.1E+01 4.0E-02 Cumulative: 4.6E-06 2.4E-01 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: BF-SG-11 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 38 1.14 -- 71-43-2 Benzene 32.4 0.972 3.6E-01 6.3E+00 2.7E-06 3.1E-02 75-15-0 Carbon Disulfide 17.9 0.537 -1.5E+02 7.4E-04 67-66-3 Chloroform 1.79 0.0537 1.2E-01 2.0E+01 4.4E-07 5.3E-04 75-71-8 Dichlorodifluoromethane 2.58 0.0774 -2.1E+01 7.4E-04 141-78-6 Ethyl Acetate 8.49 0.2547 -1.5E+01 3.5E-03 100-41-4 Ethylbenzene 64.6 1.938 1.1E+00 2.1E+02 1.7E-06 1.9E-03 109-99-9 ~Tetrahydrofuran 2 0.06 -4.2E+02 2.9E-05 142-82-5 Heptane, N-12.6 0.378 -8.3E+01 9.1E-04 110-54-3 Hexane, N-8.25 0.2475 -1.5E+02 3.4E-04 67-63-0 Isopropanol 13.4 0.402 -4.2E+01 1.9E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)6.21 0.1863 -1.0E+03 3.6E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)1.15 0.0345 -6.3E+02 1.1E-05 75-09-2 Methylene Chloride 1.62 0.0486 1.0E+02 1.3E+02 4.8E-10 7.8E-05 91-20-3 ~Naphthalene 0.571 0.01713 8.3E-02 6.3E-01 2.1E-07 5.5E-03 115-07-1 Propylene 12.1 0.363 - 6.3E+02 1.2E-04 100-42-5 Styrene 0.583 0.01749 -2.1E+02 1.7E-05 127-18-4 Tetrachloroethylene 0.813 0.02439 1.1E+01 8.3E+00 2.3E-09 5.8E-04 108-88-3 Toluene 323 9.69 -1.0E+03 1.9E-03 75-69-4 Trichlorofluoromethane 1.59 0.0477 -- 95-63-6 Trimethylbenzene, 1,2,4-19.4 0.582 -1.3E+01 9.3E-03 108-67-8 Trimethylbenzene, 1,3,5-5.9 0.177 -1.3E+01 2.8E-03 1330-20-7 Xylenes 187 5.61 -2.1E+01 5.4E-02 Cumulative: 5.1E-06 1.2E-01 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: February 2024 Basis: November 2023 EPA RSL Table Site ID: 25046-21-060 Exposure Unit ID: Worst-Case CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 103 3.09 -- 71-43-2 Benzene 75.8 2.274 3.6E-01 6.3E+00 6.3E-06 7.3E-02 75-27-4 Bromodichloromethane 5.08 0.1524 7.6E-02 -2.0E-06 75-15-0 Carbon Disulfide 37.3 1.119 -1.5E+02 1.5E-03 56-23-5 Carbon Tetrachloride 0.905 0.02715 4.7E-01 2.1E+01 5.8E-08 2.6E-04 67-66-3 Chloroform 45.2 1.356 1.2E-01 2.0E+01 1.1E-05 1.3E-02 110-82-7 Cyclohexane 7.34 0.2202 -1.3E+03 3.5E-05 106-46-7 Dichlorobenzene, 1,4-0.625 0.01875 2.6E-01 1.7E+02 7.3E-08 2.2E-05 75-71-8 Dichlorodifluoromethane 2.77 0.0831 -2.1E+01 8.0E-04 75-34-3 Dichloroethane, 1,1-1.8 0.054 1.8E+00 -3.1E-08 75-35-4 Dichloroethylene, 1,1-2.66 0.0798 -4.2E+01 3.8E-04 156-59-2 Dichloroethylene, cis-1,2-71.9 2.157 -8.3E+00 5.2E-02 156-60-5 Dichloroethylene, trans-1,2-2.36 0.0708 -8.3E+00 1.7E-03 141-78-6 Ethyl Acetate 26.4 0.792 -1.5E+01 1.1E-02 100-41-4 Ethylbenzene 74.4 2.232 1.1E+00 2.1E+02 2.0E-06 2.1E-03 109-99-9 ~Tetrahydrofuran 51.5 1.545 -4.2E+02 7.4E-04 142-82-5 Heptane, N-31.7 0.951 -8.3E+01 2.3E-03 110-54-3 Hexane, N-17 0.51 -1.5E+02 7.0E-04 591-78-6 Hexanone, 2-5.64 0.1692 -6.3E+00 5.4E-03 67-63-0 Isopropanol 39 1.17 -4.2E+01 5.6E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)16.7 0.501 -1.0E+03 9.6E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)3.15 0.0945 -6.3E+02 3.0E-05 1634-04-4 Methyl tert-Butyl Ether (MTBE)26.2 0.786 1.1E+01 6.3E+02 7.3E-08 2.5E-04 75-09-2 Methylene Chloride 3.75 0.1125 1.0E+02 1.3E+02 1.1E-09 1.8E-04 91-20-3 ~Naphthalene 4.57 0.1371 8.3E-02 6.3E-01 1.7E-06 4.4E-02 115-07-1 Propylene 77.1 2.313 - 6.3E+02 7.4E-04 100-42-5 Styrene 1 0.03 -2.1E+02 2.9E-05 127-18-4 Tetrachloroethylene 266 7.98 1.1E+01 8.3E+00 7.4E-07 1.9E-01 108-88-3 Toluene 356 10.68 -1.0E+03 2.0E-03 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-0.567 0.01701 -1.0E+03 3.3E-06 79-01-6 Trichloroethylene 117 3.51 4.8E-01 4.2E-01 7.3E-06 1.7E+00 75-69-4 Trichlorofluoromethane 2.07 0.0621 -- 95-63-6 Trimethylbenzene, 1,2,4-41 1.23 -1.3E+01 2.0E-02 108-67-8 Trimethylbenzene, 1,3,5-10.4 0.312 -1.3E+01 5.0E-03 75-01-4 Vinyl Chloride 1.9 0.057 1.7E-01 2.1E+01 3.4E-07 5.5E-04 1330-20-7 Xylenes 226 6.78 -2.1E+01 6.5E-02 Cumulative: 3.2E-05 2.2E+00 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator