27003_Winston Container_Brownfields Assessment Report_20240226

February 26, 2024

Mr. Seth Titley, Brownfields Project Manager
North Carolina Department of Environmental Quality
Division of Waste Management, Brownfield Redevelopment Section
Mail Service Center 1646
Raleigh, North Carolina 27699-1646

Subject: Brownfields Assessment Report
Former Winston Container
4901 Winston Container Road, Charlotte, North Carolina
Mid-Atlantic Project #H1712.00
Brownfields Project #27003-23-060

Dear Mr. Titley:

On behalf of Industrial Development Partners, LLC (the Prospective Developer or PD)
Mid-Atlantic Associates, Inc. (Mid-Atlantic) has prepared this Brownfields Assessment
Report for the Former Winston Container Brownfields property (Brownfields Project
#27003-23-060) to document recent assessment activities conducted in November 2023.
The Brownfields property is located at 4901 Winston Container Road, Mecklenburg
County, North Carolina (subject site). The subject site consists of two (2) contiguous
parcels of land (Parcel ID #11510201 and 11510203) totaling approximately 15.5 acres
in a predominantly industrial area east of the Charlotte Douglas International Airport. A
topographic site map is included as Drawing 1.

The assessment activities were conducted in accordance with the North Carolina
Department of Environmental Quality (NCDEQ) approved Brownfields Assessment Work
Plan – Revision 1 (Work Plan) dated November 10, 2023. The Work Plan was prepared
and submitted to satisfy the requirements identified during recent data gap discussions
prior to the preparation of an Environmental Management Plan (EMP) for the proposed
redevelopment and the PD’s pursuit of a Brownfields Agreement (BFA).

Brownfields Assessment Report February 26, 2024 Former Winston Container – Charlotte, NC Page 2
NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

1.0 INTRODUCTION

The subject site is comprised of two (2) contiguous parcels of land that are zoned for
industrial use and is located less than a half-mile east of the Charlotte Douglas
International Airport. The subject site is developed with two (2) approximate 5,800 square
foot single-story warehouse structures that were constructed in 1946. The remaining
portions of the subject site consist of overgrown vegetative areas, portions of former
building slabs, and minor debris piles. A portion of Taggart Creek cuts through the
northern portion of the subject site and also borders the western and southern property
boundaries. A detailed site layout map is provided in Drawing 2.

The PD plans to redevelop the Brownfields property as primarily a surface storage and
lay-down yard (equipment, vehicles, containers, etc.). No new structures are currently
planned, and the existing warehouse structures will likely be re-purposed. The PD also
intends to connect the subject site to municipal water, which will involve extending an
existing water line through the southern portion of the Brownfields property. The location
of the proposed water line is depicted in Drawing 3. Prior to the submittal of an EMP for
the planned redevelopment, NCDEQ requested that assessment activities be conducted
on the Brownfields property to address certain gaps for redevelopment activities.

Based on discussions with Ms. Carolyn Minnich of the Brownfields Redevelopment
Section (BRS), Mid-Atlantic proposed to 1) collect surface water and sediment samples
within the on-site sections of Taggart Creek, 2) collect soil samples in the vicinity of areas
of concern from historical site operations, 3) collect composite soil samples along a
proposed water line extension connecting the site to municipal water, 4) collect
groundwater samples from the existing permanent monitoring wells to determine the
current groundwater conditions, and 5) collect interior soil vapor samples to determine
potential vapor intrusion risks for future development. Mid-Atlantic also proposed to
conduct a receptor survey for the site and surrounding area. The subject site background
and a summary of assessment activities conducted scope is provided below.

2.0 BACKGROUND

The Winston Container Company (WCC) site was originally developed in the late 1950’s
as a drum reconditioning facility. Operations continued until approximately 2006 when
operations ceased and the site was vacated. Drum reconditioning activities included the
use of several underground storage tanks (USTs) during the operational timeline at the
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NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

facility: one 10,000-gallon diesel tank (Tank #1), one 4,000-gallon methyl-ethyl ketone
(MEK) tank (Tank #2), and one 6,000-gallon #2 fuel oil tank (Tank #3). Additionally,
several wastewater aboveground storage tanks (ASTs) were utilized in central portions
of the subject site. Former on-site structures that were previously demolished included a
garage, drum conditioning plant, wastewater treatment station, and a drum cutting and
incineration area. Debris piles consisting of concrete, tires, and plastic drums have been
observed along the northernmost portions of Taggart Creek. Drum debris and other
historical facility waste have also been identified along the southernmost portions of
Taggart Creek, which borders the subject site to the west and south and flows through
the northcentral portion of the subject site. Historical site features are depicted on
Drawing 2.

In November 1992, Tank #1 and Tank #2 were reportedly emptied and closed in place
via inert concrete slurry. Assessment activities were conducted between November 1992
and February 1993 in relation to the UST closure activities. Results of the assessment
were documented in a UST Closure Report dated July 7, 1993 and described below:

• Four (4) soil samples (WC-6 through WC-9) were collected at the base of the
4,000-gallon MEK tank (Tank #2). Laboratory results indicated that concentrations
were below method detection limits for MEK.
• Four (4) soil samples (WC-1, WC-2, WC-4, and WC-5) were collected at the base
of the 10,000-gallon diesel tank (Tank #1). A fifth soil sample (WC-3) was collected
from beneath the product piping. Laboratory results indicated that concentrations
were below method detection limits for total petroleum hydrocarbons (TPH) diesel
range organics (DRO) in the samples collected from the base of Tank #1.
However, TPH DRO was detected at 486 milligrams per kilogram (mg/kg) in
product piping sample WC-3.
• Between December 1992 and February 1993, additional samples were collected
from underneath the product pump (UP), product line (UL), and end of tank (ET)
to delineate the vertical extent of soil impacts from Tank #1. Laboratory results
from initial samples collected from beneath the pump (UP-5’) and line (UL-5’)
indicated that TPH DRO was detected at concentrations of 17,154 mg/kg and
13,214 mg/kg, respectively.
• Impacted soils were excavated and subsequent sampling was conducted at the
base of the excavation of soils beneath the product pump and lines. Confirmation
sampling of the product line (UL2) indicated that TPH DRO was not detected above
method detection limits. However, samples collected beneath the product pump
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NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

(UP2 through UP4) indicated that TPH DRO was detected between 34 mg/kg and
657 mg/kg.
• Based on the analytical results, it was concluded that the likely source of soil
impacts around Tank #1 were the result of a leak from the pump. In total,
approximately 30 cubic yards of impacted soils were removed from the vicinity of
Tank #1 and place in the central portion of the subject site for future on-site
treatment via minimum rate landfarming.

An Initial Site Assessment was reportedly conducted in 2006 for the North Carolina
Department of Environment and Natural Resources (NCDENR, currently NCDEQ)
Aquifer Protection Section (APS). Assessment activities included the installation of four
(4) groundwater monitoring wells (MW-1 through MW-4). Additionally, Initial Abatement
Action activities were conducted in 2008 in relation to the 6,000-gallon #2 fuel oil tank
(Tank #3) which included the installation of two (2) monitoring wells (MW-5 and MW-6).

In February 2009, assessment and closure activities were conducted in relation to Tank
#3. Tank #3 was historically utilized for heating purposes and was installed in the 1970’s.
WCC stopped using Tank #3 sometime in the 1980’s due to the availability of natural gas;
however, the tank remained in place due to its location beneath the plant building, which
was constructed as an addition after the tank was installed. Following the cessation of
site activities in 2006, WCC opted to remove Tank #3 ahead of potential redevelopment
of the property. Results of the assessment and UST closure activities were documented
in a Limited Site Assessment Report for T03 – UST Closure dated June 29, 2009 and
described below:

• On January 25, 2008, Hill Enterprises emptied Tank #3 which consisted of remnant
a mixture of fuel oil and water. The basin around Tank #3 was subsequently
excavated and the tank was removed.
• Two (2) soil samples (W1 and W2) were collected at the base of Tank #3.
Laboratory results indicated that concentrations of TPH DRO and TPH gasoline
range organics (GRO) exceeded NCDENR UST Action Levels.
• Four (4) additional confirmation soil samples (E, N, W, and S) were collected
around the extent of the excavation to determine the horizontal extend of soil
impacts. Laboratory results indicated that concentrations of TPH DRO exceeded
UST Action Levels. Additional sample volume was included for risk-based
analyses including volatile organic compounds (VOCs), volatile petroleum
hydrocarbons (VPH), and extractable petroleum and hydrocarbons (EPH).
Laboratory results of the risk-based analyses did not indicate that concentrations
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NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

were present above UST Action Levels and Soil-to-Water Maximum Soil
Contaminant Concentrations (MSCCs).
• Monitoring wells installed during Initial Abatement Action activities (MW-5 and MW-
6) were sampled to determine if groundwater impacts from the apparent UST
release were present. MW-5 was installed upgradient of the former Tank #3
location and MW-6 was installed in the backfilled basin of Tank #3.
• Laboratory results indicated that concentrations were below method detection
limits for VOCs and VPH in the groundwater samples for MW-5 and MW-6.

On January 14, 2010, Shield Engineering, Inc. (Shield) was notified by the Mecklenburg
County Land Use and Environmental Services (LUESA) of potential drum remnants being
present on the subject site. Subsequent site reconnaissance was conducted along
Taggart Creek in the southwestern portion of the WWC property by Shield, LUESA, the
Environmental Protection Agency (EPA) Emergency Response personnel, and the US
EPA’s response contractor, Tetra Tech. Drum remnants, construction debris, plastics,
and other household debris were observed to be present from the surface to depths of
approximately 6 feet below ground surface (ft bgs). Tetra Tech collected four (4) soil
samples for lead (ICD-SS-1 through ICD-SS-4) and three (3) samples for paint waste
(ICD-WS-1 through ICD-WS-3). Lead results indicated concentrations ranged from 52
parts per million (ppm) to 55,400 ppm. Following initial soil assessment activities,
remedial actions were conducted by Shield and the findings are documented in an
Assessment and Remedial Activities Report dated May 12, 2010. A summary of the
results is below:

• Shield oversaw the excavation of two (2) test pits identified as Excavation 1 and
Excavation 2. The excavations were in the vicinity of the buried waste identified
along Taggart Creek and previous soil samples collected by Tetra Tech.
Excavation 1 extended to 10 ft bgs and included drum debris, tires, concrete, and
other debris. Excavation 2 extended to approximately 8 ft bgs and was observed
to primarily contain household debris and automotive parts. No remnant drums
were observed in Excavation 2.
• During the excavation activities, a silver/gray paint substance was observed in
Excavation 1 at a depth of approximately 6 ft bgs. Shield submitted a sample (WC-
1) of the material for laboratory analysis . Analytical results indicated the presence
of several VOCs, SVOCs and toxicity characteristic and leaching procedure
(TCLP) concentrations metals concentrations exceeding regulatory screening
levels.
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NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

• Shield collected two (2) soil samples from the base of the excavations (EX-1 Bot
and EX-2 Bot) for laboratory analysis of lead. Analytical results indicated that lead
was detected in EX-1 (219 mg/kg) and EX-2 (6.7 mg/kg) at concentrations below
the Soil-to-Water MSCC of 270 mg/kg.
• Between January 20 and 28, 2010, Shamrock Environmental Corporation
(Shamrock) conducted additional excavation, bank stabilization, and stream
protection activities along Taggart Creek. A total of approximately 1,227 tons of
contaminated soil and debris were disposed off-site to a Subtitle D landfill.
• Resampling of soil after the over-excavation activities indicated lead
concentrations in residual soils ranging from 4.4 ppm to 8.4 ppm which were below
the Soil-to-Water MSCC. Low-level detections of the VOCs acetone,
chlorobenzene, 1,3,-dichlorobenzene, 1,4-dichlorobenzene, isopropyltoluene,
naphthalene, 1,2,4-trimethylbenzene, and xylenes were also present in residual
soil but below their respective MSCCs.

As part of environmental due diligence activities for the Charlotte Douglas International
Airport, Amec Foster Wheeler (Amec) conducted a Phase I Environmental Site
Assessment (ESA) at the WCC property in December 2015 and identified the following
recognized environmental conditions (RECs) in connection with the subject site:

• The soil and groundwater contamination documented on the subject site and the
facility status in the Inactive Hazardous Sites Branch (IHSB) established by the
NCDEQ was considered to be a REC.
• The previous uses of the subject site as a drum reconditioning facility over an
approximate 50-year period and the former storage of hazardous materials was
considered a REC.
• Previous reports indicated the presence of a potable water supply well on the
subject site. The property owner informed Amec that two (2) water supply wells
were abandoned on May 12, 2007. As such, Amec did not consider the water
supply wells to constitute a REC.

Following Phase I ESA activities, Amec conducted groundwater assessment activities at
the subject site to determine the location of the potentially impacted groundwater relative
to Taggart Creek. Results of the assessment were submitted to the Charlotte Douglas
International Airport in a Report of Phase II ESA dated May 26, 2016. A summary of the
environmental findings is summarized below:

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NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

• On April 4, 2016, Amec oversaw the installation of five (5) temporary monitoring
wells (TW-1 through TW-5). Temporary monitoring wells TW-1 and TW-2 were
installed in the vicinity of the observed drum debris area from 2010, TW-3 and TW-
4 were installed between outfall pipes to Taggart Creek in the southwestern portion
of the subject site, and TW-5 was installed near the eastern property boundary and
permanent monitoring well MW-2.
• Groundwater was calculated to flow from the eastern portion of the property near
the former Winston Container building to the west and south toward Taggart Creek.
• Between April 13 and 14, 2016, Amec collected groundwater samples from four
(4) existing permanent monitoring wells (MW-1 through MW-4) and the five (5)
newly installed temporary monitoring wells.
• Laboratory analytical results of the groundwater samples collected indicated the
presence of several VOCs above method detection limits. Concentrations of
benzene, 1,1-dichloroethane, 1,2-dichloropropane, 1,2-dichlorobenzene, 1,4-
dichlorobenzene, naphthalene, tetrachloroethylene (PCE), toluene, xylenes, and
vinyl chloride were detected above North Carolina 15A NCAC 02L .0202
Groundwater Quality Standards (2L Standards).
• With the exception of PCE (MW-2 and MW-4), benzene (TW-3), and 1,4-
dichlorobenzene (TW-3), 2L Standard exceedances were mostly observed in
temporary wells installed in the vicinity of the drum debris area (TW-1 and TW-2).

The Prospective Developer (PD) petitioned the property into the BRS (Brownfields Project
#27003-23-060) and received a Letter of Eligibility (LOE) on July 14, 2023. Ms. Carolyn
Minnich, the PD, and Mid-Atlantic personnel participated in a data gap meeting on August
30, 2023 that outlined specific data gaps for the Brownfields property. Data gaps included
assessment activities to evaluate site soil, surface water, sediment, groundwater, and soil
vapor in order to evaluate the risk for future mixed-use development. Also included in the
assessment request was the completion of a receptor survey for the site and surrounding
area. The following Work Plan documents proposed assessment activities to satisfy the
data gap requirements ahead of planned redevelopment of the Brownfields property.

3.0 SCOPE OF WORK

The assessment activities were conducted in general accordance with the NCDEQ
Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup dated
July 2021, NCDEQ Division of Waste Management (DWM) Vapor Intrusion Guidance
dated March 2018, and most recent versions of the USEPA Region IV Science and
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NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

Ecosystem Support Division (SESD) Field Branches Quality System and Technical
Procedures guidelines.

A previous Subsurface Investigation Permit (SIP) through the Mecklenburg County
Environmental Health Department (SIP # 70002331) was issued on March 30, 2016. Mid-
Atlantic contacted the North Carolina public utility locating company (North Carolina 811)
to mark utilities at the proposed sample locations. Mid-Atlantic also subcontracted with a
private utility locator, Probe Utility Locating (PUL), to screen proposed sample locations
for subgrade utilities and conduct a ground penetrating radar (GPR) survey to determine
the location of potential orphan UST basins and/or other potential subgrade features.

Mid-Atlantic instructed the drilling subcontractor to be hand cleared utilizing a hand auger
each boring location to a depth of 5 ft bgs to further screen the boring locations for the
presence of subsurface utilities. All sampling locations were documented in the field using
a hand-held global position system (GPS) unit. The sampling locations are depicted on
Drawing 2 and Drawing 3, and described below:

• Three (3) co-located surface water and sediment samples were collected within
the on-site portions of Taggart Creek to determine if historical site operations have
impacted the creek and/or potential contaminants coming from upgradient
sources.
• Eleven (11) soil samples (SB-1 through SB-11) were collected in potential areas
of concern.
• Two (2) composite soil samples (WL-1 and WL-2) were collected along the
transect of the proposed water line extension.
• Four (4) interior sub-slab soil vapor samples (SSV-1 through SSV-4) were
collected beneath the existing structures to determine potential vapor intrusion
risks for future redevelopment.

Work Plan Deviations

Mid-Atlantic proposed to locate four (4) existing permanent monitoring wells (MW-1
through MW-4) and, if determined to be accessible, would collect samples to characterize
the current groundwater conditions. During initial field activities in November 2023, Mid-
Atlantic was only able to locate monitoring well MW-3. Mid-Atlantic re-mobilized to the
subject site in February 2024 to locate the additional wells and attempt to collect
groundwater samples. During re-mobilization activities, Mid-Atlantic personnel were able
to locate monitoring wells MW-1, MW-2, and MW-3. However, the well vault for MW-3 did
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NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

not allow for access without destroying the integrity of the casing. As such, groundwater
samples were not collected from MW-3 and MW-4. Monitoring wells MW-1 and MW-2
were able to be sampled and the methodology and results of the groundwater
assessment are provided in the sections below. The on-line SIP portal does not identify
any wells existing and/or being abandoned on the subject site. Based on the condition of
monitoring wells MW-1, MW-2, and MW-3, it is likely that MW-4 is still on-site and will
need to be addressed during redevelopment activities. All site monitoring wells will be
properly abandoned during subsequent redevelopment of the site.

4.0 RECEPTOR SURVEY

On November 17, 2023, Mid-Atlantic conducted receptor survey activities at the subject
site and nearby area. Receptor survey activities included an intensive pedestrian and
vehicular survey for subsurface structures such as basements, and possible water supply
wells, springs, and surface water intakes used as a source of water within a 1,500-foot
radius of the subject site. Mid-Atlantic utilized the online Mecklenburg County Well
Information System and NCDEQ Source Water Assessment Program (SWAP) to identify
potential potable water sources for properties located within a 1,500-foot radius of the
subject site. In addition, Mid-Atlantic identified the locations of main underground and
aboveground utilities, and land use and zoning in the vicinity of the subject site using
available Mecklenburg County online resources. Receptor survey maps are included as
Drawings 4 and 5, and a copy of the completed NCDEQ Brownfields Property Receptor
Survey form is provided as Appendix A. The results of the receptor survey are
summarized below.

4.1 Zoning

The subject site is currently zoned as a Manufacturing and Logistics (ML-2) district.
Adjacent and surrounding properties are currently a mix of Manufacturing and Logistics
(ML-1 and ML-2), Office Flex Campus (OFC), Institutional (INST), and General Business
(B-1). Zoning in the vicinity of the subject site is depicted in Drawings 4 and 5.

4.2 Municipal Water

Municipal water supplied by the City of Charlotte is available to the surrounding area. The
PD has proposed to extend existing City water lines along Morris Field Drive to the south
to the subject site for on-site use. Water sources for the City of Charlotte are Lake Norman
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NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

and Mountain Island Lake, which are located approximately 18 miles northwest of the
subject site. Based on review of information available via the Mecklenburg County Well
Information System, NCDEQ SWAP, and the Annual Water Quality Report published by
the City of Charlotte, Mid-Atlantic did not identify sources of public drinking water within
1,500 feet of the subject site.
4.3 Water Supply Wells

Mid-Atlantic conducted a pedestrian and vehicular survey of properties within a 1,500-
foot radius of the subject site to identify potential water supply wells. Mid-Atlantic also
utilized the Mecklenburg County Well Information System and NCDEQ SWAP geographic
information system maps to identify potential potable water supply wells located within a
one-mile radius of the subject site. As shown on Drawing 4, Mid-Atlantic did not identify
potable water supply wells within a 1,500-foot radius of the subject site. There is one (1)
active irrigation well located approximately 1,350 feet northeast of the subject site.
According to the Mecklenburg County Well Information System, fifteen (15) private water
supply wells are located within one mile of the subject site which are shown on Drawing
5. Of the private water supply wells, 12 are utilized for irrigation purposes and 3 have an
unknown use. Seven of the water supply wells are listed as either inactive or abandoned.
The nearest active potable private water supply well was identified outside of the 1-mile
radius. Based on the status and distances to surrounding private water supply wells and
availability of municipal water to the surrounding area, Mid-Atlantic does not consider the
presence of the private water supply wells to be impacted by the Brownfields property.

4.4 Surface Water

Taggart Creek borders the subject site to the south and west and runs through the central
portion of the subject site. Taggart Creek flows generally to the south towards Sugar
Creek where they intersect approximately 2 miles southeast of the subject site. Based on
the NCDEQ classification system, Sugar Creek is a Class C surface water body. A Class
C surface water body is defined as “waters protected for uses such as secondary
recreation, fishing, wildlife, fish consumption, aquatic life including propagation, survival
and maintenance of biological integrity, and agriculture. Secondary recreation includes
wading, boating, and other uses involving human body contact with water where such
activities take place in an infrequent, unorganized, or incidental manner.”

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NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

4.5 Subsurface Features

Mid-Atlantic contacted North Carolina 811, the public utility locator, to mark subsurface
utilities at the subject site. Mid-Atlantic also contracted a private utility locator, PUL, to
identify underground utilities and potential buried debris/orphan USTs using GPR
technology. PUL assisted in attempting to locate the existing monitoring wells during initial
field activities in November 2023. However, PUL was not able to locate the wells using
GPR methodology. The GPR survey did identify several subsurface features that required
alternative boring locations for the assessment: the 10,000-gallon diesel tank (Tank #1),
the 4,000-gallon MEK tank (Tank #2), and an apparent oil-water-separator near a former
AST near Tank #1.

Following utility location activities with PUL, Mid-Atlantic conducted a visual
reconnaissance in the area to identify potential subsurface structures within 1,000 feet of
the subject site. Mid-Atlantic observed evidence of subsurface utilities including sanitary
sewer, storm sewer, electrical, municipal water, and natural gas adjacent to the subject
site and nearby adjacent properties. Mid-Atlantic did not observe the presence of nearby
residential structures with basements within a 1,000-foot radius of the subject site.

5.0 BROWNFIELDS ASSESSMENT ACTIVITIES

Between November 17 and 21, 2023, Mid-Atlantic conducted field activities for the
Brownfields assessment described below. Mid-South Environmental (Mid-South) was
contracted with to advance the soil borings during assessment activities.

5.1 Soil Sampling Methodology

Grab Sampling
Mid-South advanced eleven (11) soil samples (SB-1 through SB-11) in potential areas of
concern from historical operations. The soil borings were advanced using a track-
mounted Geoprobe® drill rig to depths up to approximately 10 ft bgs via direct-push
technology (DPT) drilling methods. Continuous soil samples were collected from each
boring in acetate lined macrocore sleeves. Soil samples from soil boring advancement
were logged for lithological description and field screened for indication of potential
impacts by observation for staining, unusual odors, and the presence of organic vapors
using a calibrated photoionization detector (PID). Based on future redevelopment plans
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NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

including surficial grading, Mid-Atlantic collected one (1) soil sample from each boring
from a shallow depth interval (0 to 2 ft bgs).

Composite Sampling
Mid-South advanced ten (10) aliquot soil borings along the proposed water line extension
transect for the collection of composite samples. Based on the proposed depth of the
water line extension, Mid-Atlantic instructed Mid-South to advance the aliquot soil
samples to depths of approximately 2 ft bgs. Mid-Atlantic collected two (2) soil samples
per aliquot sampling location: one (1) was logged for lithological description and field
screened for indication of potential impacts by observation for staining, unusual odors,
and the presence of organic vapors using a calibrated photoionization detector (PID) and
one (1) was placed on ice. The additional aliquot soil samples placed on ice for each
screening interval were collected in this manner to prevent volatilization (i.e., not
homogenized and not screened by the PID). Following field screening results, the
additional aliquot soil samples were collected as discrete grab samples for laboratory
analysis of volatile organic compounds (VOCs) from the aliquot soil sample intervals
exhibiting the highest likelihood for impact (i.e., not be collected from the bag/container
used to screen for PID readings). Aliquot soil borings selected for VOC analysis are
depicted on Drawing 3 and PID screening results are provided on Table 1. Following
VOC sample collection, the remaining soil volume from the non-volatilized bag was
combined and homogenized in a decontaminated stainless-steel bowl to form one
composite soil sample for analysis of semi-volatile organic compounds (SVOCs),
Resource Conservation and Recovery Act (RCRA) metals plus hexavalent chromium,
and pesticides/insecticides.

Soil boring logs are provided in Appendix B. The soil samples were collected into
laboratory-supplied glassware and placed on ice for delivery under chain-of-custody
protocol within 24 hours of collection to Waypoint Analytical (Waypoint), a North Carolina
accredited laboratory. Soil samples collected were analyzed for VOCs by EPA Method
8260, SVOCs by EPA Method 8270, RCRA metals plus hexavalent chromium by EPA
Methods 6020/7471/7199 and pesticides/insecticides by EPA Method 8081.

5.2 Surface Water and Sediment Sampling Methodology

The co-located surface water and sediment samples were collected from the approximate
mid-point of the creek using a decontaminated swing sampler and a disposable
polyethylene container. Mid-Atlantic collected the samples from downstream to upstream
locations in order to minimize the disturbance of sediment and cross-contamination by
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NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

sampling personnel. Following sample collection in the swing sampler, samples were
transferred into laboratory-supplied glassware and placed on ice for delivery under chain-
of-custody protocol within 24 hours of collection to Waypoint. Surface water and soil
samples collected were analyzed for VOCs by EPA Method 8260, SVOCs by EPA
Method 8270, and RCRA metals by EPA Methods 6020/7471. The sediment samples
were also analyzed for hexavalent chromium by EPA Method 7199.

5.3 Sub-slab Vapor Implant Installation

Mid-Atlantic re-mobilized to the subject site on February 7, 2024 to collect groundwater
samples from the two located permanent monitoring wells (MW-1 and MW-2). The
monitoring wells were purged via disposable polyethylene bailers. Approximately three
(3) well volumes were removed from the monitoring wells prior to sample collection.
Groundwater samples were collected directly into laboratory supplied sample containers
from the polyethylene bailers. The sample containers were labeled with a unique sample
identification, date, time, and requested analysis, and placed in a laboratory supplied
cooler with ice. The samples were delivered to Waypoint in Charlotte, North Carolina
under standard chain-of-custody protocol for analysis of VOCs by EPA Method 8260,
SVOCs by EPA Method 8270, and RCRA metals by EPA Methods 6020/7471.

5.4 Sub-slab Vapor Implant Installation

Mid-Atlantic installed four (4) sub-slab vapor pins beneath footprint of the two existing
structures. The sub-slab vapor implants were installed using Cox Colvin Vapor Pins™
that were advanced with a hammer drill equipped with a 5/8-inch diameter drill bit. The
hammer drill was advanced though the concrete slab to approximately 6-inches into the
underlying soil. Following borehole advancement, loose cuttings were removed with a
shop-vac prior to installation of the Vapor Pins™. The Vapor Pin™ assembly, which is
comprised of a brass sampling point and silicone sleeve, was then placed into the drilled
hole by tapping the assembly using an installation/extraction tool and a dead blow
hammer to form an airtight seal. Following installation of the Vapor Pin™ assembly,
dedicated 1/4-inch Teflon sample tubing was connected to the barbed end of the vapor
implant.

5.5 Sub-slab Vapor Sampling Methodology

Following implant installation, Mid-Atlantic conducted a leak check at each sub-slab vapor
sampling location by utilizing helium as the tracer compound. The helium was introduced
Brownfields Assessment Report February 26, 2024 Former Winston Container – Charlotte, NC Page 14
NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

through a shroud over the probe and entire sampling train to a minimum concentration of
50% as measured using a LandTech Gem™ 5000 helium detector. With the canister
valve closed, Mid-Atlantic checked for the presence of helium from air collected into a
Tedlar® bag using a 60-milliliter syringe connected to the tubing. During the leak check,
Mid-Atlantic collected approximately three purge volumes from each sampling implant
into the Tedlar® bag and field screened each for the absence of Helium prior to opening
the sampling train between the Tedlar® bag and the Summa canister.

During leak check confirmation, helium was not detected in the sub-slab vapor implants
installed at the subject site. Thus, Mid-Atlantic considered the integrity of the soil vapor
implants to be adequate for sampling. Helium concentrations in the shroud, along with
concentrations from each purge volume, were recorded in the field data sheets. Mid-
Atlantic also conducted a shut-in test on the sampling process lines to ensure an air-tight
connection. The shut-in tests were conducted by applying vacuum pressure to the lines
and observing for vacuum pressure loss. Soil vapor sampling forms are included in
Appendix C.

Following successful shut-in tests and leak check to verify sample integrity, the sub-slab
vapor samples were collected using laboratory-supplied 1-Liter Summa canisters with
calibrated flow regulators set to 100 milliliters per minute (mL/min) to avoid sample short
circuiting and to further ensure sample integrity. Prior to sampling, vacuum readings,
Summa identification and flow controller identification for each sample were recorded on
the field data sheets. Following field documentation, the sample train was opened to the
Summa flow controller and the Summa canister was opened to allow collection of sub-
slab vapor volume. Sampling was deemed complete when the flow controller exhibited
no greater than -5 inches of mercury (approximately 10 minutes). Following sample
collection, the Summa canisters were closed, the final vacuum reading and sampling time
intervals were recorded on the canister tag, field data sheets, and laboratory chain-of-
custody form. Samples were delivered under proper chain-of-custody protocol to
Waypoint for analysis of VOCs by EPA Method TO-15, plus naphthalene.

5.6 Quality Assurance and Quality Control

For quality assurance/quality control (QA/QC) purposes, Mid-Atlantic collected one (1)
duplicate surface water sample (DUP-1), one (1) duplicate sediment sample (DUP-2),
one (1) duplicate soil sample (DUP-3), and one (1) duplicate soil vapor sample (DUP-4)
which were submitted for the same laboratory analysis as the parent sample. The
duplicate soil vapor sample was collected simultaneously as the parent sample (SSV-2)
Brownfields Assessment Report February 26, 2024 Former Winston Container – Charlotte, NC Page 15
NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

via a laboratory-supplied “T-connector.” Samples submitted for laboratory analysis
included an adequate sample volume for laboratory matrix spike (MS) and matrix spike
duplicate (MSD) analysis.

Nondedicated sampling equipment used for collecting the samples was decontaminated
prior to use at each sampling location. Laboratory QA/QC procedures were employed to
ensure appropriate sample handling and analysis and to aid in the review and validation
of the analytical data. Mid-Atlantic requested that the laboratory include estimated
concentrations for compounds that were detected at levels above the laboratory method
detection limit, but below the laboratory reporting limit (J flags). The laboratory analytical
data report and QA package for each group of samples submitted to and analyzed by the
subcontracted laboratory were provided in an appendix to the final report and included as
Appendix D. Laboratory QA data consistent with Level II documentation was provided
for this project.

5.7 Investigative Derived Waste

Investigative derived waste (IDW) generated during the assessment activities were
managed in general accordance with NCDEQ IHSB Guidelines for Assessment and
Cleanup. The soil generated was thin-spread on-site following sample collection.

6.0 BROWNFIELDS ASSESSMENT RESULTS

6.1 Soil Analytical Results

A tabular summary of the soil analytical results is provided in Table 1. The analytical
results were compared to the NCDEQ Industrial/Commercial Preliminary Soil
Remediation Goals (PSRGs) dated February 2024 and Maximum Soil Contaminant
Concentrations (MSCCs) dated September 2022. Additionally, metals results were also
compared to mean values of background concentrations for North Carolina soils taken
from Elements in North American Soils (Dragun and Chekri, 2005). Soil laboratory results
indicated the following:

• Several VOCs and SVOCs were detected above laboratory method detection limits
in soil samples collected. Concentrations of VOCs and SVOCs across the subject
site were below Industrial/Commercial PSRGs.
Brownfields Assessment Report February 26, 2024 Former Winston Container – Charlotte, NC Page 16
NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

• Concentrations of metals in sediment samples were below Industrial/Commercial
PSRGs, Non-Residential MSCCs, and/or within the range of background
concentrations for North Carolina soils.
• No pesticides/insecticides were detected above their respective
Industrial/Commercial PSRGs.

6.2 Surface Water and Sediment Analytical Results

A tabular summary of the surface water and sediment analytical results are provided in
Table 2 and Table 3, respectively. Surface water results were compared to North
Carolina 2B Surface Water Standards (2B Standards), EPA National Recommended
Water Quality Criteria for Aquatic Life and Human Health (NRWQC), and Division of
Water Resources (DWR) In-Stream Target Values for Surface Waters. Sediment results
were compared to the NCDEQ Industrial/Commercial PSRGs dated February 2024 and
MSCCs dated September 2022. Sediment results for metals were also compared to the
Elements in North American Soils (Dragun and Chekri, 2005) that were used for the soil
results. A summary of the surface water and sediment results is described below:

Surface Water
• The VOCs trichloroethylene (TCE), cis-1,2-dichloroethylene (DCE), and xylenes
were detected in surface water samples collected within Taggart Creek but were
below their respective surface water (2B) standards.
• The SVOC di-n—butyl phthalate was detected in SW-2 but at a concentration
below its applicable surface water standard.
• Barium and chromium were the only metals detected above laboratory detection
limits. Concentrations of barium ranged from 42.1 µg/L to 46.7 µg/L which are
below the 2B Standard of 1,000 µg/L. Concentrations of chromium ranged from
0.387 µg/L to 0.506 µg/L which are below the 2B Standard of 10 µg/L.

Sediment
• Several VOCs and SVOCs were detected above laboratory method detection limits
in sediment samples collected within Taggart Creek; however, concentrations
were below Industrial/Commercial PSRGs.
• Concentrations of metals in sediment samples were below Industrial/Commercial
PSRGs, Non-Residential MSCCs, and/or within the range of background
concentrations for North Carolina soils.
• No pesticides/insecticides were detected above Industrial/Commercial PSRGs in
sediment samples collected.
Brownfields Assessment Report February 26, 2024 Former Winston Container – Charlotte, NC Page 17
NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

6.3 Groundwater Analytical Results

A tabular summary of the groundwater analytical results is provided in Table 4.
Groundwater analytical results above applicable screening levels are depicted on
Drawing 6. The analytical results were compared to the 2L Standards dated April 2022,
Gross Contamination Levels (GCLs) dated October 2020, and DWM Groundwater
Screening Levels (GWSLs) for vapor intrusion dated February 2024. Groundwater
laboratory results indicated the following:

• Several VOCs and SVOCs were detected above laboratory method detection limits
in the groundwater samples collected from MW-1 and MW-2.
• The VOCs PCE (24.3 µg/L) and TCE (3.1 µg/L) were detected above 2L Standards
in monitoring well MW-2.
• The SVOCs dibenz(a,h)anthracene (6.82 µg/L) and indeno(1,2,3-cd)pyrene (6.70
µg/L) were detected above 2L Standards in monitoring well MW-1. The
concentration of dibenz(a,h)anthracene also exceeds the GCL of 1.2 µg/L.
• The metals barium, chromium, and lead were detected in groundwater samples
collected. However, the concentrations were below their respective 2L Standards.
• No concentrations exceeded Non-Residential GWSLs.

6.4 Soil Vapor Analytical Results

A tabular summary of the soil vapor analytical results is provided in Table 5. The analytical
results were compared to the NCDEQ DWM Residential Sub-slab and Exterior Soil Gas
Screening Levels (SGSLs) dated February 2024. Soil vapor sample laboratory results
indicated the following:

• Several VOCs were detected above laboratory method detection limits in soil vapor
samples within the two existing site structures.
• Of the detected VOCs, only benzene and ethylbenzene were detected at
concentrations exceeding Residential SGSLs.
• No soil gas concentrations exceeded their respective Non-Residential SGSLs.

6.5 Vapor Intrusion Risk Evaluation

The cumulative risk is calculated by entering the maximum concentrations of all
contaminants detected at each established exposure unit (EU) into the NCDEQ Risk
Brownfields Assessment Report February 26, 2024 Former Winston Container – Charlotte, NC Page 18
NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

Calculator. An EU is a defined area of a site represented by a specific set of land use(s),
receptors, contaminant concentrations, and exposure pathways. For this assessment, a
“worst case” EU was calculated using the highest concentrations in each sub-slab vapor
sample collected. The NCDEQ Risk Calculator determines the cancer risk sum for all
carcinogens and the cumulative hazard index for all non-carcinogens. The NCDEQ DWM
allows a maximum cancer risk sum for all carcinogens of 1.0 x 10-4 and a maximum non-
carcinogenic hazard index of 1.0. The hazard index is the sum of the hazard quotient
(HQs) calculated for each compound detected. Using the highest concentrations detected
in the “worst case” scenario, Mid-Atlantic utilized the NCDEQ Risk Calculator dated
February 2024 to evaluate the potential cumulative risk for the soil vapor to indoor air
vapor intrusion pathway. Risk calculator results are provided in Appendix E and
summarized in the table below:

Risk Input LICR HI Risk Exceedance?
Worst Case 2.7 x 10-7 0.0076 No

As shown in the table above, cumulative risk exceedances were not calculated under
both a residential and non-residential use from the sub-slab vapor concentrations
detected in the “worst case” scenario. Risk calculator results indicate that there is not
likely the potential for carcinogenic and/or non-carcinogenic vapor intrusion risks to be
present within the ground floor of the existing structures.

7.0 SUMMARY AND CONCLUSIONS

Mid-Atlantic has completed Brownfields assessment activities at the former Winston
Container Brownfields property located at 4901 Winston Container Road in Charlotte,
Mecklenburg County, North Carolina. The assessment activities were conducted in
accordance with the NCDEQ approved Work Plan dated November 10, 2023. The Work
Plan was prepared and submitted to satisfy the requirements identified during recent data
gap discussions prior to the preparation of an EMP for the proposed redevelopment and
the PD’s pursuit of a BFA. A brief summary of the Brownfields assessment activity results
are provided below:

• No VOCs, SVOCs, metals, pesticides, or insecticides were detected in subject site
soils at concentrations exceeding Industrial/Commercial PSRGs.

Brownfields Assessment Report February 26, 2024 Former Winston Container – Charlotte, NC Page 19
NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

• Surface water and sediment results did not indicate the presence of contaminants
above applicable regulatory standards.

• Due to the inability to locate existing site monitoring well MW-4 and inaccessibility
of located well MW-3, Mid-Atlantic was unable to collect groundwater samples from
these locations. Based on the condition of monitoring wells MW-1, MW-2, and MW-
3, it is likely that MW-4 is still on-site and will need to be addressed during
redevelopment activities. All site monitoring wells will be properly abandoned
during subsequent redevelopment of the site.

• The VOCs PCE and TCE were detected above 2L Standards in monitoring well
MW-2. The SVOCs dibenz(a,h)anthracene and indeno(1,2,3-cd)pyrene were
detected above 2L Standards in monitoring well MW-1. The concentration of
dibenz(a,h)anthracene also exceeded the GCL. Remaining groundwater
detections were below 2L Standards, GCLs, and Non-Residential GWSLs.

• Several VOCs were detected above laboratory method detection limits in soil vapor
samples across the subject site. However, concentrations were below their
respective Non-Residential SGSLs.

• Risk calculator results indicated that unacceptable risk exceedances were not
calculated under non-residential use scenarios from the highest soil vapor
concentrations detected.

Results of Brownfields assessment activities completed at the subject site indicate that
soil, groundwater, sediment, and surface water can be managed in accordance with a
NCDEQ approved EMP that will be submitted under a separate cover. Furthermore,
results of previous assessment activities also indicate that groundwater can be managed
in accordance with an EMP. The “worst-case” soil vapor results indicate that
unacceptable risk levels were not calculated under non-residential use scenarios for the
existing site structures. Risk calculator results indicate that vapor intrusion risks are likely
not present, and an active vapor intrusion mitigation system (VIMS) would not be required
for proposed future uses of the existing structure(s). Please contact the undersigned if
there are questions concerning the results and/or conclusions reached for this
Brownfields Assessment Report.

Brownfields Assessment Report February 26, 2024 Former Winston Container – Charlotte, NC Page 20
NCDEQ Brownfield Project #27003-23-060
Mid-Atlantic Project #H1712.00

With best regards,

MID-ATLANTIC ASSOCIATES, INC.

Shane Sisco, P.G. Greg D. Icenhour, P.G., MBA
Project Hydrogeologist Principal Geologist

Attachments: Tables
Table 1 – Soil Analytical Summary
Table 2 – Surface Water Analytical Summary
Table 3 – Sediment Analytical Summary
Table 4 – Groundwater Analytical Summary
Table 5 – Sub-slab Vapor Analytical Summary

Drawings
Drawing 1 – Topographic Site Map
Drawing 2 – Site and Sample Location Map
Drawing 3 – Proposed Water Line Extension Map
Drawing 4 – Receptor Survey Map (1,500 feet)
Drawing 5 – Receptor Survey Map (1-mile)
Drawing 6 – Groundwater Analytical Results Map

Appendices
Appendix A – Receptor Survey Form
Appendix B – Boring Logs
Appendix C – Brownfields Sampling Forms
Appendix D – Laboratory Analytical Reports
Appendix E – NCDEQ Risk Calculator (February 2024)

Mid-Atlantic is authorized to practice engineering by the North Carolina Board of Examiners for Engineers
and Surveyors, License F-0967 and Geology under the North Carolina Board for Licensing of Geologists,
License C-186.

TABLES

TABLE 1Soil Analytical SummaryFormer Winston Container4901 Winston Container Road, Charlotte, North Carolina NCDEQ Brownfields Project #27003-23-060Mid-Atlantic Project #H1712.00
Sample ID SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-8 SB-9 SB-10 SB-11 WL-1 WL-2
Sample Depth (ft bgs)0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2
Sample Date 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023
PID Results (ppm)0.2 0.2 0.4 4.8 0.6 0.5 52.5 27.9 0.0 0.0 6.0 8.0
Sample Location Contaminated Soil Application
VOCs (EPA Method 8260)
Acetone 14,000 210,000 ----0.066 0.048 0.056 0.07 0.101 0.179 0.069 0.113 0.109 0.062 0.019 J 0.022 0.177 1.10
Benzene 1.2 5.4 ----<0.0007 <0.0007 <0.0007 <0.0007 <0.0006 <0.0006 0.003 J 0.004 J 0.008 <0.0007 <0.0006 <0.0006 <0.0006 <0.0006
n-Butylbenzene 780 12,000 ----<0.0006 <0.0006 <0.0006 <0.0006 <0.0005 <0.0005 <0.0006 <0.0005 0.0006 J <0.0006 <0.0005 <0.0005 <0.0005 <0.0005
sec-Butylbenzene 1600 23000 ----<0.0007 <0.0007 <0.0007 <0.0007 <0.0006 <0.0006 <0.0007 0.0008 J 0.0007 J <0.0007 <0.0006 <0.0006 <0.0006 <0.0006
Carbon Disulfide 160 740 ----<0.0008 <0.0008 <0.0007 <0.0007 <0.0007 <0.0007 <0.0008 0.005 0.003 J <0.0008 <0.0007 <0.0007 <0.0007 <0.0007
1,2-Dichlorobenzene 380 2000 ----<0.0004 <0.0004 <0.0004 <0.0004 <0.0003 <0.0003 0.015 0.009 0.011 <0.0004 <0.0003 <0.0003 <0.0003 <0.0003
1,3-Dichlorobenzene NE NE ----<0.0005 <0.0005 <0.0004 <0.0004 <0.0004 <0.0004 0.001 J 0.001 J 0.003 J <0.0005 <0.0004 <0.0004 <0.0004 <0.0004
1,4-Dichlorobenzene 2.8 12 ----<0.0007 <0.0008 <0.0007 <0.0007 <0.0007 <0.0007 0.01 0.004 J 0.004 J <0.0008 <0.0006 <0.0006 <0.0007 <0.0006
1,1-Dichloroethane 3.8 17 ----<0.001 <0.001 <0.001 <0.001 <0.0009 <0.0009 0.034 0.025 0.001 J <0.001 <0.0009 <0.0008 <0.0009 <0.0009
1,1-Dichloroethene 48 210 ----<0.0009 <0.0009 <0.0009 <0.0008 <0.0008 <0.0008 0.002 J 0.002 J <0.0008 <0.0009 <0.0008 <0.0008 <0.0008 <0.0008
cis-1,2-Dichloroethene 31 470 ----<0.0009 <0.0010 <0.0009 <0.0009 <0.0009 <0.0009 0.008 0.017 0.009 <0.001 <0.0008 <0.0008 <0.0009 <0.0008
Ethylbenzene 6.1 27 ----<0.0007 <0.0007 <0.0007 <0.0007 <0.0006 0.0007 J 0.011 0.021 0.012 <0.0007 <0.0006 <0.0006 0.001 J 0.001 J
n-Hexane 130 540 ----<0.0008 <0.0008 <0.0008 <0.0008 <0.0007 <0.0007 0.005 J 0.018 0.07 <0.0008 <0.0007 <0.0007 <0.0007 <0.0007
Isopropylbenzene (Cumene)410 2,100 ----<0.0006 <0.0006 <0.0005 <0.0005 <0.0005 <0.0005 0.018 0.012 0.001 J <0.0006 <0.0005 <0.0005 <0.0005 <0.0005
4-Isopropyl toluene NE NE ----<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.005 J 0.004 J 0.006 <0.001 <0.001 <0.001 <0.001 <0.001
Methyl Ethyl Ketone (MEK)5,500 40,000 ----<0.0008 <0.0008 <0.0008 <0.0007 <0.0007 0.004 J <0.0008 <0.0007 <0.0007 <0.0008 <0.0007 <0.0007 <0.0007 <0.0007
Methylene Chloride 58 650 ----<0.001 0.002 J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.0001 <0.001 <0.001 <0.001 <0.001
Naphthalene 2.1 8.8 ----<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.018 0.012 0.003 J <0.001 <0.001 <0.001 <0.001 <0.001
n-Propylbenzene 780 5,100 ----<0.0006 <0.0007 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 0.001 J 0.001 J <0.0007 <0.0006 <0.0006 <0.0006 <0.0006
Toluene 990 9,700 ----<0.0008 <0.0008 <0.0008 0.001 J 0.001 J 0.003 J 0.022 0.015 0.021 <0.0008 <0.0007 <0.0007 <0.0007 0.001 J
1,2,3-Trichlorobenzene 13 190 ----<0.0006 <0.0007 <0.0006 <0.0006 <0.0006 <0.0006 0.003 J 0.002 J 0.001 J <0.0007 <0.0006 <0.0006 <0.0006 <0.0006
1,2,4,-Trichlorobenzene 12 55 ----<0.0008 <0.0008 <0.0007 <0.0007 <0.0007 <0.0007 0.0029 0.020 0.025 <0.0008 <0.0007 <0.0007 <0.0007 <0.0007
Trichlorethene 0.87 4 ----<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.001 J <0.001 <0.001 <0.0009 <0.0010 <0.0010
1,2,4-Trimethylbenzene NE NE ----<0.0006 <0.0006 <0.0006 <0.0006 <0.0005 0.002 J 0.004 J 0.01 0.008 <0.0006 <0.0005 <0.0005 <0.0005 <0.0006
1,3,5-Trimethylbenzene 56 320 ----<0.0006 <0.0007 <0.0006 <0.0006 <0.0006 0.0009 J 0.002 J 0.007 0.003 J <0.0007 <0.0006 <0.0006 <0.0006 <0.0006
Vinyl Chloride 0.06 2 ----<0.0006 <0.0006 <0.0006 <0.0006 <0.0005 <0.0005 0.001 J 0.003 J <0.0005 <0.0006 <0.0005 <0.0005 <0.0005 <0.0005
Xylene (Total)120 530 ----<0.0006 <0.0006 <0.0006 <0.0006 <0.0005 0.004 J 0.039 0.159 0.036 <0.0006 <0.0005 <0.0005 0.011 J 0.010 J
m&p-Xylene NE NE ----<0.001 <0.001 <0.001 <0.001 <0.001 0.002 J 0.026 0.129 0.020 <0.001 <0.001 <0.001 0.008 J 0.007 J
o-Xylene 140 590 ----<0.0006 <0.0006 <0.0006 <0.0006 <0.0005 0.001 J 0.013 0.030 0.015 <0.0006 <0.0005 <0.0005 0.003 J 0.003 J
SVOCs (EPA Method 8270)
Acenaphthylene NE NE ----<0.126 <0.132 <0.122 <0.120 <0.114 <0.116 <0.124 <0.462 <0.932 <0.134 <0.109 <0.108 0.671 J <0.129
Benzo(a)anthracene 1.1 21 ----<0.167 <0.175 <0.161 <0.159 <0.151 <0.154 <0.164 0.707 J <1.23 <0.178 <0.145 <0.143 1.89 J <0.154
Benzo(a)pyrene 0.11 2.1 ----<0.176 <0.185 <0.170 <0.168 <0.160 <0.163 <0.174 0.717 J <1.31 <1.88 <0.153 <0.151 1.99 J <0.163
Benzo(b)fluoranthene 1.1 21 ----<0.175 <0.183 <0.169 <0.167 <0.159 <0.162 <0.172 0.905 J <1.30 <1.87 <0.152 <0.150 2.55 J <0.162
Benzo(g,h,i)perylene NE NE ----<0.163 <0.171 <0.158 <0.156 <0.148 <0.150 <0.161 <0.598 <1.21 <1.74 <0.142 <0.140 1.48 J <0.151
Benzo(k)fluoranthene 11 210 ----<0.164 <0.172 <0.159 <0.157 <0.149 <0.152 <0.162 <0.602 <1.22 <1.75 <0.143 <0.141 0.890 J <0.152
Benzoic Acid 51,000 660,000 ----<0.697 M <0.730 M <0.674 M 0.955 JM <0.631 M <0.643 M <0.687 M <2.55 M <5.15 M <0.743 M <0.605 M <0.598 M <2.89 M <0.646 M
bis(2-Ethylhexyl)phthalate 39 160 ----<0.144 <0.151 <0.139 <0.137 <0.130 1.14 <0.142 2.88 J 103 <0.153 <0.125 <0.123 0.997 J 0.795
Butyl benzyl phthalate 290 1,200 ----<0.135 <0.142 <0.131 <0.129 <0.123 <0.125 <0.133 <0.497 2.00 J <0.144 <0.118 <0.116 <0.562 <0.125
Chrysene 110 2,100 ----<0.170 <0.178 <0.165 <0.163 <0.154 <0.157 <0.168 0.695 J <1.27 <0.182 <0.148 <0.146 1.73 J <0.158
Din-n-butyl phthalate 1,300 16,000 ----<0.128 <0.134 <0.124 <0.122 <0.116 <0.118 <0.126 1.85 J <0.950 <0.137 <0.111 <0.110 <0.532 0.136 J
Fluoranthene 480 6,000 ----<0.147 <0.154 <0.143 <0.141 <0.133 <0.136 <0.145 1.46 J <1.09 <0.157 <0.128 <0.126 4.08 <0.137
Indeno(1,2,3-cd)pyrene 1.1 21 ----<0.215 <0.225 <0.208 <0.205 <0.194 <0.198 <0.212 <0.787 <1.59 <0.229 <0.186 <0.184 1.41 J <0.199
1-Methylnaphthalene 18 73 ----<0.127 <0.133 <0.123 <0.121 <0.115 <0.117 <0.125 0.474 J <0.941 <0.135 <0.110 <0.109 <0.527 <0.118
2-Methylnaphthalene 48 600 ----<0.120 <0.125 <0.116 <0.114 <0.108 <0.110 <0.118 1.08 J <0.888 <0.128 <0.104 <0.103 <0.497 <0.111
Phenanthrene NE NE ----<0.250 <0.261 <0.241 <0.238 <0.226 <0.230 <0.246 1.11 J <1.84 <0.266 <0.217 <0.214 1.27 J <0.231
Pyrene 360 4,500 ----<0.161 <0.168 <0.155 <0.153 <0.145 <0.148 <0.158 1.33 J <1.19 <0.171 <0.139 <0.138 3.46 <0.149
Former Excavation Pit Former Debris Piles Proposed Water Line Extension
11/20/2023
10.7
Former Wastewater Treatment
StationFormer UST and AST Locations
PSRGs (1)Regional Background Metals in Soil (2)
Residential Industrial/Commercial Range Mean
TABLE 1Soil Analytical SummaryFormer Winston Container4901 Winston Container Road, Charlotte, North Carolina NCDEQ Brownfields Project #27003-23-060Mid-Atlantic Project #H1712.00
Sample ID SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-8 SB-9 SB-10 SB-11 WL-1 WL-2
Sample Depth (ft bgs)0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2
Sample Date 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023 11/20/2023
PID Results (ppm)0.2 0.2 0.4 4.8 0.6 0.5 52.5 27.9 0.0 0.0 6.0 8.0
Sample Location Contaminated Soil Application Former Excavation Pit Former Debris Piles Proposed Water Line Extension
11/20/2023
10.7
Former Wastewater Treatment
StationFormer UST and AST Locations
PSRGs (1)Regional Background Metals in Soil (2)
Residential Industrial/Commercial Range Mean
RCRA Metals (EPA Methods 6020/7471/7199)
Arsenic 0.68 3.0 1.0 - 18 4.8 0.458 0.877 1.16 1.63 0.662 2.20 1.24 1.30 2.11 0.867 0.424 0.327 1.00 0.895
Barium 3,100 47,000 50 - 1,000 356 82.7 97.4 57.7 49.8 78.3 336 84.5 190 254 129 188 238 44.3 128
Cadmium 1.4 20 1.0 - 10 4.3 <0.0312 <0.0327 <0.302 <0.0298 <0.0283 1.55 0.128 J 2.94 2.86 <0.0333 0.116 J 0.0368 J 0.0585 0.0923 J
Chromium (total)NE NE 7.0 - 300 65 48 132 22.7 97.4 60 99.1 48 44.2 83 78.5 27.8 22.4 31.2 28.5
Hexavalent Chromium 0.31 6.5 NE NE 0.311 0.428 <0.163 0.344 0.417 1.51 1.13 <0.155 <0.156 0.428 0.203 J <0.145 1.16 0.685
Lead 400*800*<0.1 - 50 16 4.21 4.01 7.83 7.53 4.67 184 21.2 51.5 252 4.69 3.27 3.62 8.92 12.5
Mercury 4.7 70 0.03 - 0.52 0.121 0.0179 J 0.0181 J <0.0140 0.055 0.0230 J 0.055 <0.0142 0.367 0.194 0.0574 0.0134 J <0.0124 0.131 0.215
Selenium 78 1,200 <0.1 - 0.8 0.42 0.305 0.318 0.269 J 0.402 0.261 J 0.662 0.436 0.842 0.516 0.608 0.244 J 0.271 0.453 0.338
Silver 78 1,200 <0.1 - 5.0 NE 0.0097 J 0.0128 J 0.0130 J 0.0177 J 0.0112 J 0.613 0.0581 J 0.0829 J 0.0844 J <0.0086 0.0234 J 0.0215 J 0.014 0.0789 J
Insecticides/Pesticides (EPA Method 8081)
alpha-BHC NE NE ----<0.0014 <0.0014 <0.0013 <0.0013 <0.0012 <0.0012 <0.0013 <0.0012 0.0099 <0.0015 <0.0012 <0.0012 <0.0014 <0.0013
alpha-Chlordane 7.1 100 ----<0.0022 <0.0023 <0.0021 <0.0021 <0.0020 <0.0020 <0.0022 0.0660 <0.0020 <0.0024 <0.0019 <0.0019 <0.0023 <0.0021
gamma-Chlordane 7.1 100 ----<0.0020 <0.0021 <0.0019 <0.0019 <0.0018 <0.0018 <0.0020 0.0388 Q <0.0018 <0.0021 <0.0017 <0.0017 <0.0021 <0.0018
4,4'-DDD 2.3 9.6 ----<0.0022 <0.0023 <0.0021 <0.0021 <0.0020 <0.0020 <0.0022 <0.0020 <0.0020 <0.0023 <0.0019 <0.0019 <0.0023 0.048
4,4'-DDE 2.0 9.3 ----<0.0024 <0.0025 <0.0023 <0.0023 <0.0022 <0.0022 <0.0024 0.039 <0.0022 <0.0026 <0.0021 <0.0021 0.0125 0.021
4,4'-DDT 1.9 8.5 ----<0.0018 <0.0019 <0.0017 <0.0017 <0.0016 <0.0016 <0.0018 0.0518 0.0663 0.0061 J <0.0015 <0.0015 0.0314 0.0418
Dieldrin 0.034 0.14 ----<0.0025 <0.0026 <0.0024 <0.0023 <0.0022 <0.0023 <0.0024 0.0586 <0.0023 0.0266 <0.0021 <0.0021 0.0553 0.0498
Endrin 3.8 49 ----<0.0023 <0.0024 <0.0022 <0.0022 <0.0020 <0.0021 <0.0022 <0.0021 <0.0021 <0.0024 <0.0020 <0.0019 0.0166 <0.0021
Endrin Aldehyde NE NE ----<0.0025 <0.0026 <0.0024 <0.0024 <0.0022 <0.0023 <0.0025 <0.0023 <0.0023 <0.0027 <0.0022 <0.0021 0.0075 0.016
Heptachlor 0.14 0.63 ----<0.0016 <0.0017 <0.0015 <0.0015 <0.0014 <0.0015 <0.0016 <0.0014 0.0722 <0.0017 <0.0014 <0.0014 0.0017 <0.0015
Heptachlor Epoxide 0.071 0.33 ----<0.0021 <0.0022 <0.0020 <0.0020 <0.0019 <0.0019 <0.0021 <0.00119 <0.0019 <0.0022 <0.0018 <0.0018 0.0303 <0.0019
Toxaphene 0.49 2.1 ----<0.0122 <0.0128 <0.0118 <0.0117 <0.0111 <0.0113 <0.0120 <0.0112 <0.0113 <0.0130 <0.0106 <0.0105 0.647 0.728
Notes:
1) North Carolina Department of Environmental Quality (NCDEQ) Preliminary Soil Remediation Goals (PSRGs) (February 2024).
Elements in North American Soils by Dragun and Chekiri, 2005.
values indicate the concentration was below the laboratory method detection limit
TABLE 2
Surface Water Analytical Summary
Former Winston Container
4901 Winston Container Road, Charlotte, North Carolina
NCDEQ Brownfields Project #27003-23-060
Mid-Atlantic Project #H1712.00
Sample ID SW-1 SW-3
Sample Date 11/17/2023 11/17/2023
Sample Location
VOCs (EPA Method 8260)
cis-1,2-Dichloroethene NE NE 720 <0.200 <0.200 <0.200 0.246 J
Trichloroethene 30 NE NE <0.220 0.408 J 0.287 J 0.265 J
m&p-Xylene NE NE 57,000 0.457 J <0.420 <0.420 <0.420
Xylene (Total)3.3 NE 120 0.457 J <0.21 <0.21 <0.21
SVOCs (EPA Method 8270)
Di-n-butyl phthalate 6,000 NE NE <2.06 2.54 J <2.06 <2.06
RCRA Metals (EPA Methods 6020/7471/7196
Barium 1,000 NE 21,000 42.1 44.8 46.7 46.4
Chromium 10 NE NE 0.387 J 0.506 J <0.346 0.445 J
Notes:
1) North Carolina Department of Environmental Quality (NCDEQ) 15A NCAC 02B Water Quality Standards (2B Standards) (November 2023).
2) EPA National Recommended Water Quality Criteria for Aquatic Life & Human Health (NRWQC) (July 2016).
3) North Carolina Division of Water Resources (DWR) In-Stream Target Values for Surface Waters (November 2023).
* = standards used were for Class C freshwater streams - Aquatic Life & Secondary Recreation
Only compounds detected in at least one sample are shown
Compound concentrations are reported in micrograms per liter (µg/L)
Compound concentrations are reported to the laboratory method detection limits
Laboratory analytical methods are shown in parantheses
values indicate the concentration was below the laboratory method detection limit
VOCs = volatile organic compounds
SVOCs = semi-volatile organic compounds
RCRA = Resource Conservation and Recovery Act
NE = Not Established
NS = Not Sampled
J = estimated concentration between the laboratory method detection limit and the laboratory reporting limit
11/17/2023
SW-2 / DUP-3Surface Water Standards*
2B
Standards (1)NRWQC (2)Values (3)Taggart Creek
TABLE 3Sediment Analytical Summary
Former Winston Container
4901 Winston Container Road, Charlotte, North Carolina
NCDEQ Brownfields Project #27003-23-060
Mid-Atlantic Project #H1712.00
Sample ID SED-1 SED-3
Sample Date 11/17/2023 11/17/2023
Sample Location Residential Industrial/Commercial Range Mean
VOCs (EPA Method 8260)
Acetone 14,000 210,000 ----0.350 0.211 0.203 0.048
4-Isopropyl toluene NE NE ----<0.001 0.001 J <0.001 <0.001
Methyl Ethyl Ketone (MEK)5,500 40,000 ----0.011 J 0.005 J <0.0007 <0.0007
Methylene Chloride 58 650 ----<0.001 0.002 J <0.001 0.004 J
Toluene 990 9,700 ----<0.0008 0.0008 J 0.0007 J <0.0007
SVOCs (EPA Method 8270E)
Benzo(a)anthracene 1.1 21 ----<0.663 <0.605 0.718 J <0.622
Benzo(a)pyrene 0.11 2.1 ----<0.701 <0.639 0.735 J <0.658
Benzo(b)fluoranthene 1.1 21 ----1.00 J 0.739 J 1.08 J <0.653
Benzo(g,h,i)perylene NE NE ----<0.649 <0.592 0.625 J <0.609
Chrysene 110 2,100 ----0.854 J 0.663 J 1.02 J <0.636
Fluoranthene 480 6,000 ----1.73 J 1.40 J 2.18 J 1.16 J
Pyrene 360 4,500 ----1.29 J 1.07 J 1.70 J 0.885
bis(2-Ethylhexyl)phthalate 39 160 ----<0.572 <0.522 0.583 J <0.537
RCRA Metals (EPA Methods 6020D/7471B/7199)
Arsenic 0.68 3.0 1.0 - 18 4.8 1.13 0.885 0.555 0.691
Barium 3,100 47,000 50 - 1,000 356 55.8 45.1 43.7 36.1
Cadmium 1.4 20 1.0 - 10 4.3 0.0891 J 0.0643 J 0.0776 J 0.0657 J
Chromium (total)NE NE 7.0 - 300 65 26.5 22.5 12.8 18.3
Hexavalent Chromium 0.31 6.5 NE NE 0.406 0.239 <0.156 0.244
Lead 400*800*<0.1 - 50 16 14.9 9.09 5.08 6.39
Mercury 4.7 70 0.03 - 0.52 0.121 0.0226 J 0.0162 J <0.0133 0.0134 J
Selenium 78 1,200 <0.1 - 0.8 0.42 0.704 1.05 0.51 0.547
Silver 78 1,200 <0.1 - 5.0 NE 0.0156 J 0.0150 J 0.0140 J 0.0320 J
Insecticides/Pesticides (EPA Method 8081)
Dieldrin 0.034 0.14 ----<0.0024 <0.0022 <0.0023 0.0031 J
Toxaphene 0.49 2.1 ----<0.0121 <0.0111 <0.0112 0.134
Notes:
1) North Carolina Department of Environmental Quality (NCDEQ) Preliminary Soil Remediation Goals (PSRGs) (February 2024).
Elements in North American Soils by Dragun and Chekiri, 2005.
* = No PSRGs established for this compound. NCDEQ Maximum Soil Contaminant Concentrations (MSCCs) dated September 2022 used instead.
Only compounds detected in at least one sample are shown
Compound concentrations are reported in milligrams per kilogram (mg/kg)
Compound concentrations are reported to the laboratory method detection limits
Laboratory analytical methods are shown in parantheses
VOCs = volatile organic compounds
SVOCs = semi-volatile organic compounds
RCRA = Resource Conservation and Recovery Act
ft bgs = feet below ground surface
NE = Not Established; -- = Not Applicable
J = estimated concentration between the laboratory method detection limit and the laboratory reporting limit
values indicate the concentration was below the laboratory method detection limit
PSRGs (1)Regional Background Metals in Soil (2)
Taggart Creek
11/17/2023
TABLE 4
Groundwater Analytical Summary
Former Winston Container
4901 Winston Container Road, Charlotte, North Carolina
NCDEQ Brownfields Project #27003-23-060
Mid-Atlantic Project #H1712.00
Sample ID MW-1 MW-2 MW-3 MW-4
Sample Date 2/7/2024 2/7/2024 ----
Sample Location Western Portion
of Site
Eastern Portion
of Site of Site
Former Drum
Cutting /
Incineration Area
VOCs (EPA Method 8260)
Chloroform 70 70,000 3.6 <0.220 1.19 NS NS
cis-1,2-Dichloroethene 70 NE NE <0.200 6.64 NS NS
Methyl Ethyl Ketone (MEK)4,000 4,000,000 1,900,000 0.855 J 0.835 J NS NS
Tetrachloroethene 0.7 700 48 <0.220 24.3 NS NS
Trichloroethene 3.0 3,000 4.4 <0.180 3.10 NS NS
SVOCs (EPA Method 8270)
Benzoic Acid 30,000 1,700,000 NE 6.56 J <1.10 NS NS
Dibenz(a,h)anthracene 0.005 1.2 NE 6.82 <0.434 NS NS
Di-n-Octyl Phthalate 100 NE NE 4.70 J <1.65 NS NS
Indeno(1,2,3-cd)pyrene 0.05 NE NE 6.70 <0.477 NS NS
Pentachlorophenol NE 300 NE 5.07 <1.43 NS NS
RCRA Metals (EPA Methods 6010D/7470A)
Barium 700 700,000 NE 129 145 NS NS
Chromium 10 10,000 NE 3.0 J 4.0 J NS NS
Lead 15 15,000 NE 3.0 J <3.0 NS NS
Notes:
1) North Carolina Department of Environmental Quality (NCDEQ) 15A NCAC 02L .0202 Groundwater Quality Standards (2L Standards) (April 2022).
2) NCDEQ Gross Contamination Levels (GCLs) for Groundwater (October 2020).
3) NCDEQ Division of Waste Management (DWM) Ground Water Screening Levels (GWSLs) (February 2024).
Only compounds detected in at least one sample are shown
Compound concentrations are reported in micrograms per liter (µg/L)
Compound concentrations are reported to the laboratory method detection limits
Laboratory analytical methods are shown in parantheses
Bold values indicates the an exceedance of the 2L Standard
values indicates the an exceedance of the GCL and/or Non-Residential GWSL
values indicate the concentration was below the laboratory method detection limit
VOCs = volatile organic compounds
SVOCs = semi-volatile organic compounds
RCRA = Resource Conservation and Recovery Act
NE = Not Established
NS = Not Sampled
J = estimated concentration between the laboratory method detection limit and the laboratory reporting limit
Groundwater Standards
2L
Standards (1)GCLs (2)Non-Residential
GWSLs (3)
TABLE 5Sub-slab Vapor Analytical Summary
Former Winston Container
4901 Winston Container Road, Charlotte, North Carolina
NCDEQ Brownfields Project #27003-23-060
Mid-Atlantic Project #H1712.00
Sample ID SSV-1 SSV-3 SSV-4
Sample Date 11/21/2023 11/21/2023 11/21/2023
Sample Location
VOCs (EPA Method TO-15)
Acetone NE NE --17.4 14 11.9 16.7 30.6
Benzene 12 160 --10.4 8.38 17.5 13.4 10.8
1,3-Butadiene 3.1 41 --2.34 1.63 <0.328 0.92 1.09 J
Carbon Disulfide 4,900 61,000 --0.442 J 0.784 J 0.868 J 0.423 0.582 J
Cyclohexane 42,000 530,000 --7.64 16.6 16.1 5.76 6.37
Dichlorodifluoromethane (Freon 12)700 8,800 --2.77 2.74 2.48 2.3 2.86
Ethyl Acetate 490 6,100 --7.41 24 23.9 4.37 5.73
Ethylbenzene 3.7 490 --11.1 5.15 18.7 10.3 7.4
4-Ethyltoluene NE NE --2.85 1.00 J 3.95 2.08 1.44 J
Heptane 2,800 35,000 --9.79 8.38 19.4 11.3 9.97
Hexane 4,900 61,000 --15.9 56.2 55.7 8.24 11.5
Isopropyl Alcohol 1,400 18,000 --8.86 6.36 4.51 6.47 9.43
Methyl Ethyl Ketone (MEK)35,000 440,000 --3.41 7.11 2.11 2.79 3.81
Methylene chloride 3,400 53,000 --1.40 J 1.89 2.55 2.5 2.64
4-Methyl-2-pentanone (MIBK)21,000 260,000 --0.651 J 0.880 J 0.892 J 1.2 1.35 J
Propene 21,000 260,000 --13.9 12.3 10.5 2.73 4.47
Styrene 7,000 88,000 --0.787 J 0.477 J 1.51 J 0.937 0.672 J
Tetrachloroethene 280 3,500 --1.06 J 0.603 J 0.807 J 3.32 2.22 J
Tetrahydrofuran 14,000 180,000 --1.38 J 0.775 J <0.107 0.406 0.787 J
Toluene 35,000 440,000 --53.4 37.4 99.3 77.6 54.2
1,1,1-Trichloroethane 35,000 440,000 --0.758 J <0.144 <0.144 0.927 1.31 J
Trichlorofluoromethane (Freon 11)NE NE --415 309 311 166 308
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)35,000 440,000 --<0.561 0.666 0.666 J 0.636 0.766 J
1,2,4-Trimethylbenzene 420 5,300 --8.9 3.87 8.67 6.72 4.83
1,3,5-Trimethylbenzene 420 5,300 --2.64 1.09 J 2.92 2.3 1.59 J
m&p-Xylene 700 8,800 --30.6 14.8 55.7 29.9 20.2
o-Xylene 700 8,800 --11.6 5.05 15.1 9.48 7.16
Xylene (Total)700 8,800 --42.2 19.9 70.8 39.4 27.4
Non-Residential Risk Calculator
LICR ----< 1.00E-04
Non-Carcinogenic HI ----< 1
Notes:
1) North Carolina Department of Environmental Quality (NCDEQ) Division of Waste Management (DWM) Sub-slab and Exterior Soil Gas Screening Levels (SGSLs) (February 2024).
2) NCDEQ DWM Risk Calculator (February 2024).
3) Risk Calculator results were calculated using the highest concentrations of each constituent detected in soil vapor samples collected.
Only compounds detected in at least one sample are shown
Compound concentrations are reported to the laboratory method detection limits
Laboratory analytical methods are shown in parantheses
values indicate the VOC was below the laboratory method reporting limit
VOCs = volatile organic compounds
LICR = Lifetime Incremental Carcinogenic Risk; HI = Hazard Index
NE = Not Established; -- = Not Applicable
ft bgs = feet below ground surface
J = estimated concentration between laboratory method detection limit and reporting limit
values indicate the concentration was below the laboratory method detection limit
Existing StructuresResidential
SGSLs (1)
DEQ Acceptable
Cumulative Risk
Levels (3)Non-Residential
SSV-2 / DUP-4
11/21/2023

DRAWINGS

DRAWN BY: DATE:
ENG. CHECK:
JOB NO:DRAFTCHECK: GIS NO:
SITE
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REFERENCES:
1. CHARLOTTE WEST, NC DIGITAL RASTER GRAPHICS, USGS, SCANNED FROM 1:24,000-SCALE MECKLENBURG COUNTY, NC TOPOGRAPHIC MAPS, PUBLISHED 2022, USGS.2. PROPERTY BOUNDARY FROM MECKLENBURG COUNTY GIS.3. INSET MAP DATA DOWNLOADED FROM ARCGIS ONLINE.
AREA SHOWN WITHINMECKLENBURG COUNTY, N.C.
TOPOGRAPHIC SITE MAPFORMER WINSTON CONTAINER4901 WINSTON CONTAINER ROADCHARLOTTE, NORTH CAROLINA
APPROVAL:
OCTOBER 2023
DWG NO: 1
CONTOUR INTERVAL = 10 FEET
GDI 07G-H1712.00-01
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´
RECEPTOR SURVEY MAP(1-MILE)FORMER WINSTON CONTAINER4901 WINSTON CONTAINER ROAD
CHARLOTTE, NORTH CAROLINA
LEGEND
@?PRIVATE WATER SUPPLY WELL -IRRIGATION (ACTIVE)
@?PRIVATE WATER SUPPLY WELL -IRRIGATION (INACTIVE)
@?PRIVATE WATER SUPPLY WELL -OTHER (UNKNOWN)
@?AMBIENT WELL - MONITORING(ACTIVE)
MSS
GDI
0 2,400 4,8001,200 Feet
SCALE =
1,500FT
1MILE
@A
@A
@A
@A
Winston Container Rd
Minuteman Wy
GROUNDWATER ANALYTICAL RESULTS MAPFORMER WINSTON CONTAINER4901 WINSTON CONTAINER ROADCHARLOTTE, NORTH CAROLINA
DRAWN BY:DATE:
ENG. CHECK:
JOB NO:
APPROVAL:
DRAFTCHECK:GIS NO:
DWG NO: 6
FEBRUARY 2024
H1712.00
REFERENCES: 1. 2023 AERIAL IMAGERY FROM NC ONEMAP. 2. PROPERTY BOUNDARIES FROM MECKLENBURG COUNTY GIS.
´
LEGEND
Subject Property
Parcel Boundaries
Creeks/Streams
Streets
@A Existing Monitoring Well
0 120 24060Feet
1:900SCALE =
MSS
GDI
07G-H1712.00-06
NOTES: 1. ONLY COMPOUNDS EXCEEDING APPLICABLE REGULATORY STANDARDS ARE SHOWN. 2. GROUNDWATER RESULTS COMPARED TO NCDEQ 2L STANDARDS DATED APRIL 2023. 3. µg/L = MICROGRAMS PER LITER 4. J = ESTIMATED CONCENTRATION 5. NS = NOT SAMPLED
MW-1
MW-2
MW-3
MW-4
(NS)
(NS)
Dibenz(a,h)anthracene 6.82Indeno(1,2,3-cd)pyrene 6.70
MW-1 (µg/L)2/7/24
PCE 24.3TCE3.10
MW-2 (µg/L)2/7/24
Taggart Creek

APPENDIX A
Receptor Survey Form

North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site:Former Winston Container
Address:4901 Winston Container Road
City:Charlotte
County:Mecklenburg
27003-23-060
Date 11/17/2023
Property and Building Characteristics
a. Provide occupancy and use information.
Vacant; former drum reconditioning facility
Brick single-story, 3-doors, windows (all boarded up)
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
Concrete slab/flooring
n/a
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
n/a
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information
requested below. Distances are measured from the site property boundary unless otherwise indicated by the DEQ Brownfield’s Project
Current Usage Proposed UsageSurface Conditions
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved
5.00%
30.00%
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and design
considerations (e.g. positive pressure?).
0.00%
15.00%
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as needed. If
numerous buildings are on-site, consult with your PM as only information on specific buildings may be needed.
b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings (e.g. windows, bay
doors), and height (number of stories).
% of property that is covered by buildings
Rev. 09/2015 Page 1 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
South
East
West
Y 870 SE
Y ~1,000 SW
N n/a n/a
Utilities
Please provide the utility providers for the subject property
For surrounding properties, please complete the following table with available information.
N
N
N
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject property.
Utility/Potential Receptor
For the subject property, please provide a map of known buried utilites. If available, include depth to top, construction material, and
diameter of the utilities. In addition, please provide the following information on utilty providers. If additional assessment is required,
the public utility locators should be contacted. This information can then be added to a site map.
Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses.
Distance
(ft)
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
DirectionDistance
(ft)Address
Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding areas. If
specific receptors are present, please provide addresses of the facilities.
Zoning/Land Use Proposed Usage Current Use/Occupant
See map
3210 Cpcc Harris Campus Dr
Specific Land Uses of Interest Y/N *
Rev. 09/2015 Page 2 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public ______ Private ______
Public water is not currently available to the site. The PD plans to connect the site to the municipal water via an extension
to the south along Morris Field Drive.
Surface Water & Wetlands
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity of the
Property.
Mixed rock and sediment
No
(e.g., rocky or concrete bottom, drainage ways or
impoundments)
surface water body?
wetlands on-site, are wetlands suspected on adjoining
properties?
Perennial stream
Runoff / groundwater
Natural
please complete a. to d.)
Provide Information regarding Surface Water and
Wetlands
Yes; Taggart Creek (Class C)
Direction Address
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property boundary?
Is an irrigation well within 1,500 ft of the Property boundary?
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include the water
Y/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a windshield
survey within 1,500 ft of the property boundaries should be completed to determine if water supply or irrigation wells may be present.
Information from applicable databases can and should be utilized; however, should not be utilized in lieu of the windshield survey. If
multiple wells are present within the requested radius, please provide a map of the well locations. If needed, please attach a separate
Distance
(ft)
Rev. 09/2015 Page 3 of 3

APPENDIX B
Boring Logs

APPENDIX C
Brownfields Sampling Forms

Job Name:Former Winston Container Sample ID:SSV-1
Job Number H1721.00 Summa Canister ID:11361
Task Number:30000 Flow Choke ID:14312
Location:Charlotte, NC Analysis Requested:VOCs via TO-15
Date:11/21/2023 Canister Size/Flow Rate:1 Liter (15 min)
"Shut-in" test:
Length of Sample Train:Ft.
Volume to Purge*:mL
Initial He Concentration:%
Purge Start Time:End Time:
Purge Volume:mL
He Concentration:% / ppm
Sample Start Time:12:05 End Time:12:18
Start Pressure ("Hg):-30.0 End Pressure ("Hg):-3.0
Sampled by:Troy Holzshuh
Comments:
1/8" tubing = 4mL/ft 1/4" tubing = 20mL/ft
(Length of tubing x conversion factor) x 4 = Volume to Purge*
200.0
2.0
SAMPLE COLLECTION
0.0
600.0
0.0
Soil Vapor Sampling - Field Data Sheet
SITE INFORMATION SAMPLE INFORMATION
PASS / FAIL
LEAK CHECK
Job Name:Former Winston Container Sample ID:SSV-2
Job Number H1721.00 Summa Canister ID:11376
Task Number:30000 Flow Choke ID:13119
Location:Charlotte, NC Analysis Requested:VOCs via TO-15
Date:11/21/2023 Canister Size/Flow Rate:1 Liter (15 min)
"Shut-in" test:
Length of Sample Train:Ft.
Volume to Purge*:mL
Initial He Concentration:%
Purge Start Time:End Time:
Purge Volume:mL
He Concentration:% / ppm
Sample Start Time:12:51 End Time:13:09
Start Pressure ("Hg):-29.0 End Pressure ("Hg):-3.0
Sampled by:Troy Holzshuh
Comments:DUP-4 (Summa #13706 / Choke #16205)
1/8" tubing = 4mL/ft 1/4" tubing = 20mL/ft
(Length of tubing x conversion factor) x 4 = Volume to Purge*
600.0
0.0
SAMPLE COLLECTION
LEAK CHECK
PASS / FAIL
2.0
200.0
0.0
Soil Vapor Sampling - Field Data Sheet
SITE INFORMATION SAMPLE INFORMATION
Job Name:Former Winston Container Sample ID:SSV-3
Job Number H1721.00 Summa Canister ID:15800
Task Number:30000 Flow Choke ID:6556
Location:Charlotte, NC Analysis Requested:VOCs via TO-15
Date:11/21/2023 Canister Size/Flow Rate:1 Liter (15 min)
"Shut-in" test:
Length of Sample Train:Ft.
Volume to Purge*:mL
Initial He Concentration:%
Purge Start Time:End Time:
Purge Volume:mL
He Concentration:% / ppm
Sample Start Time:12:39 End Time:12:52
Start Pressure ("Hg):-30.0 End Pressure ("Hg):-5.0
Sampled by:Troy Holzshuh
Comments:
1/8" tubing = 4mL/ft 1/4" tubing = 20mL/ft
(Length of tubing x conversion factor) x 4 = Volume to Purge*
600.0
0.0
SAMPLE COLLECTION
LEAK CHECK
PASS / FAIL
2.0
200.0
0.0
Soil Vapor Sampling - Field Data Sheet
SITE INFORMATION SAMPLE INFORMATION
Job Name:Former Winston Container Sample ID:SSV-4
Job Number H1721.00 Summa Canister ID:11363
Task Number:30000 Flow Choke ID:16226
Location:Charlotte, NC Analysis Requested:VOCs via TO-15
Date:11/21/2023 Canister Size/Flow Rate:1 Liter (15 min)
"Shut-in" test:
Length of Sample Train:Ft.
Volume to Purge*:mL
Initial He Concentration:%
Purge Start Time:End Time:
Purge Volume:mL
He Concentration:% / ppm
Sample Start Time:12:24 End Time:12:36
Start Pressure ("Hg):-28.0 End Pressure ("Hg):-5.0
Sampled by:Troy Holzshuh
Comments:
1/8" tubing = 4mL/ft 1/4" tubing = 20mL/ft
(Length of tubing x conversion factor) x 4 = Volume to Purge*
600.0
0.0
SAMPLE COLLECTION
LEAK CHECK
PASS / FAIL
2.0
200.0
0.0
Soil Vapor Sampling - Field Data Sheet
SITE INFORMATION SAMPLE INFORMATION

APPENDIX D
Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/12/2023
Mid-Atlantic Associates, Inc. - Raleigh Troy Holzschuh
409 Rogers View Court Raleigh, NC, 27610
Ref: Analytical Testing
Lab Report Number: 23-325-0008 Client Project Description: Former Winston Container
Dear Troy Holzschuh:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/21/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 208
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/29/202440750State ProgramAlabama
02/07/202488-0650State ProgramArkansas
06/30/20242904State ProgramCalifornia
06/30/2024E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202404015State ProgramGeorgia
10/31/2024200078State Program - NELAPIllinois
06/30/202480215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202404015State Program - NELAPLouisiana
11/14/2025MSState ProgramMississippi
07/31/202447701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202468-03195State Program - NELAPPennsylvania
06/30/202484002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2024T104704180State Program - NELAPTexas
06/30/202400106State ProgramVirginia
09/14/2024460181State Program - NELAPVirginia
Page 1 of 1 00016/23-325-0008
Page 2 of 208
Report Number:
Sample Summary Table
Client Project Description:
23-325-0008
Former Winston Container
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
11/20/2023 12:00Solids 89888 WL-1b 11/21/2023 09:01
11/20/2023 12:05Solids 89889 WL-1 11/21/2023 09:01
11/20/2023 12:05Solids 89889 WL-1 11/21/2023 09:01 6020B
11/20/2023 12:05Solids 89889 WL-1 11/21/2023 09:01 SW-7199
11/20/2023 12:10Solids 89890 WL-2c 11/21/2023 09:01
11/20/2023 12:15Solids 89891 WL-2 11/21/2023 09:01
11/20/2023 12:15Solids 89891 WL-2 11/21/2023 09:01 6020B
11/20/2023 12:15Solids 89891 WL-2 11/21/2023 09:01 SW-7199
11/20/2023 12:30Solids 89892 SB-1 (0-2)11/21/2023 09:01
11/20/2023 12:30Solids 89892 SB-1 (0-2)11/21/2023 09:01 SW-7199
11/20/2023 12:30Solids 89892 SB-1 (0-2)11/21/2023 09:01 6020B
11/20/2023 12:40Solids 89893 SB-2 (0-2)11/21/2023 09:01
11/20/2023 12:40Solids 89893 SB-2 (0-2)11/21/2023 09:01 SW-7199
11/20/2023 12:40Solids 89893 SB-2 (0-2)11/21/2023 09:01 6020B
11/20/2023 13:00Solids 89894 SB-3 (0-2)11/21/2023 09:01
11/20/2023 13:00Solids 89894 SB-3 (0-2)11/21/2023 09:01 SW-7199
11/20/2023 13:00Solids 89894 SB-3 (0-2)11/21/2023 09:01 6020B
11/20/2023 13:10Solids 89895 SB-4 (0-2)11/21/2023 09:01
11/20/2023 13:10Solids 89895 SB-4 (0-2)11/21/2023 09:01 SW-7199
11/20/2023 13:10Solids 89895 SB-4 (0-2)11/21/2023 09:01 6020B
11/20/2023 13:20Solids 89896 SB-5 (0-2)11/21/2023 09:01
11/20/2023 13:20Solids 89896 SB-5 (0-2)11/21/2023 09:01 SW-7199
11/20/2023 13:20Solids 89896 SB-5 (0-2)11/21/2023 09:01 6020B
11/20/2023Solids 89897 SB-6 (0-2)11/21/2023 09:01
11/20/2023Solids 89897 SB-6 (0-2)11/21/2023 09:01 SW-7199
11/20/2023Solids 89897 SB-6 (0-2)11/21/2023 09:01 6020B
11/20/2023Solids 89898 SB-7 (0-2)11/21/2023 09:01
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 208
Report Number:
Sample Summary Table
Client Project Description:
23-325-0008
Former Winston Container
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
11/20/2023Solids 89898 SB-7 (0-2)11/21/2023 09:01 SW-7199
11/20/2023Solids 89898 SB-7 (0-2)11/21/2023 09:01 6020B
11/20/2023Solids 89899 SB-8 (0-2)11/21/2023 09:01
11/20/2023Solids 89899 SB-8 (0-2)11/21/2023 09:01 6020B
11/20/2023Solids 89899 SB-8 (0-2)11/21/2023 09:01 SW-7199
11/20/2023Solids 89900 SB-9 (0-2)11/21/2023 09:01
11/20/2023Solids 89900 SB-9 (0-2)11/21/2023 09:01 SW-7199
11/20/2023Solids 89900 SB-9 (0-2)11/21/2023 09:01 6020B
11/20/2023Solids 89901 SB-10 (0-2)11/21/2023 09:01
11/20/2023Solids 89901 SB-10 (0-2)11/21/2023 09:01 SW-7199
11/20/2023Solids 89901 SB-10 (0-2)11/21/2023 09:01 6020B
11/20/2023Solids 89902 SB-11 (0-2)11/21/2023 09:01
11/20/2023Solids 89902 SB-11 (0-2)11/21/2023 09:01 SW-7199
11/20/2023Solids 89902 SB-11 (0-2)11/21/2023 09:01 6020B
11/20/2023Solids 89903 DUP-3 11/21/2023 09:01
11/20/2023Solids 89903 DUP-3 11/21/2023 09:01 SW-7199
11/20/2023Solids 89903 DUP-3 11/21/2023 09:01 6020B
11/20/2023 08:00Aqueous 89904 11/21/2023 09:01
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 4 of 208
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-325-0008
Report Limit
Project:Former Winston Container
V 89888WL-1b
0.177 11/22/2023 14:498260DAcetonemg/Kg - dry 0.002
J0.001 11/22/2023 14:498260DEthylbenzenemg/Kg - dry 0.0006
J0.003 11/22/2023 14:498260Do-Xylene mg/Kg - dry 0.0005
J0.008 11/22/2023 14:498260Dm,p-Xylene mg/Kg - dry 0.001
J0.011 11/22/2023 14:498260DXylene (Total)mg/Kg - dry 0.0005
7.98 11/22/2023 10:22SW-DRYWT Moisture %
V 89889WL-1
1.00 12/09/2023 15:216020BArsenicmg/Kg - dry 0.106
44.3 12/09/2023 15:216020BBariummg/Kg - dry 0.053
J0.0585 12/09/2023 15:216020BCadmiummg/Kg - dry 0.0323
31.2 12/12/2023 00:076020BChromiummg/Kg - dry 0.144
8.92 12/09/2023 15:216020BLeadmg/Kg - dry 0.0385
0.453 12/09/2023 15:216020BSeleniummg/Kg - dry 0.128
J0.0140 12/09/2023 15:216020BSilvermg/Kg - dry 0.0083
0.131 11/30/2023 16:387471BMercury (Total)mg/Kg - dry 0.0149
0.0125 11/30/2023 17:448081B4,4'-DDE mg/Kg - dry 0.0025
0.0314 11/30/2023 17:448081B4,4'-DDT mg/Kg - dry 0.0018
0.0553 11/30/2023 17:448081BDieldrinmg/Kg - dry 0.0025
Q0.0166 11/30/2023 17:448081BEndrinmg/Kg - dry 0.0023
0.0075 11/30/2023 17:448081BEndrin Aldehyde mg/Kg - dry 0.0026
J0.0017 11/30/2023 17:448081BHeptachlormg/Kg - dry 0.0016
0.0303 11/30/2023 17:448081BHeptachlor Epoxide mg/Kg - dry 0.0022
0.647 11/30/2023 17:448081BToxaphenemg/Kg - dry 0.0126
J0.671 11/27/2023 14:428270EAcenaphthylenemg/Kg - dry 0.522
J1.89 11/27/2023 14:428270EBenzo(a)anthracene mg/Kg - dry 0.691
J1.99 11/27/2023 14:428270EBenzo(a)pyrene mg/Kg - dry 0.731
J2.55 11/27/2023 14:428270EBenzo(b)fluoranthene mg/Kg - dry 0.726
J1.48 11/27/2023 14:428270EBenzo(g,h,i)perylene mg/Kg - dry 0.676
J0.890 11/27/2023 14:428270EBenzo(k)fluoranthene mg/Kg - dry 0.681
J0.997 11/27/2023 14:428270EBis(2-ethylhexyl)phthalate mg/Kg - dry 0.597
J1.73 11/27/2023 14:428270EChrysenemg/Kg - dry 0.706
4.08 11/27/2023 14:428270EFluoranthenemg/Kg - dry 0.611
J1.41 11/27/2023 14:428270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.890
J1.27 11/27/2023 14:428270EPhenanthrenemg/Kg - dry 1.03
3.46 11/27/2023 14:428270EPyrenemg/Kg - dry 0.666
1.16 12/06/2023 13:06SW-7199 Chromium, Hexavalent mg/Kg - dry 0.175
Page 5 of 208
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-325-0008
Report Limit
Project:Former Winston Container
V 89889WL-1
19.6 11/22/2023 10:22SW-DRYWT Moisture %
V 89890WL-2c
1.10 11/28/2023 13:298260DAcetonemg/Kg - dry 0.063
J0.001 11/22/2023 15:168260DEthylbenzenemg/Kg - dry 0.0006
J0.001 11/22/2023 15:168260DToluenemg/Kg - dry 0.0007
J0.003 11/22/2023 15:168260Do-Xylene mg/Kg - dry 0.0005
J0.007 11/22/2023 15:168260Dm,p-Xylene mg/Kg - dry 0.001
J0.010 11/22/2023 15:168260DXylene (Total)mg/Kg - dry 0.0005
5.60 11/22/2023 10:22SW-DRYWT Moisture %
V 89891WL-2
0.895 12/09/2023 15:256020BArsenicmg/Kg - dry 0.0953
128 12/09/2023 15:256020BBariummg/Kg - dry 0.047
J0.0923 12/09/2023 15:256020BCadmiummg/Kg - dry 0.0289
28.5 12/12/2023 00:206020BChromiummg/Kg - dry 0.129
12.5 12/09/2023 15:256020BLeadmg/Kg - dry 0.0345
0.338 12/09/2023 15:256020BSeleniummg/Kg - dry 0.114
J0.0789 12/09/2023 15:256020BSilvermg/Kg - dry 0.0075
0.215 11/30/2023 16:407471BMercury (Total)mg/Kg - dry 0.0134
0.0480 11/30/2023 17:588081B4,4'-DDD mg/Kg - dry 0.0020
0.0210 11/30/2023 17:588081B4,4'-DDE mg/Kg - dry 0.0022
0.0418 11/30/2023 17:588081B4,4'-DDT mg/Kg - dry 0.0016
0.0498 11/30/2023 17:588081BDieldrinmg/Kg - dry 0.0023
0.0160 11/30/2023 17:588081BEndrin Aldehyde mg/Kg - dry 0.0023
0.728 11/30/2023 17:588081BToxaphenemg/Kg - dry 0.0113
0.795 11/27/2023 18:058270EBis(2-ethylhexyl)phthalate mg/Kg - dry 0.133
J0.136 11/27/2023 18:058270EDi-n-butyl phthalate mg/Kg - dry 0.119
0.685 12/06/2023 13:16SW-7199 Chromium, Hexavalent mg/Kg - dry 0.157
10.3 11/22/2023 10:22SW-DRYWT Moisture %
V 89892SB-1 (0-2)
0.458 12/09/2023 15:296020BArsenicmg/Kg - dry 0.103
82.7 12/09/2023 15:296020BBariummg/Kg - dry 0.051
48.0 12/12/2023 00:246020BChromiummg/Kg - dry 0.139
4.21 12/09/2023 15:296020BLeadmg/Kg - dry 0.0372
0.305 12/09/2023 15:296020BSeleniummg/Kg - dry 0.123
J0.0097 12/09/2023 15:296020BSilvermg/Kg - dry 0.0081
Page 6 of 208
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-325-0008
Report Limit
Project:Former Winston Container
V 89892SB-1 (0-2)
J0.0179 11/30/2023 16:437471BMercury (Total)mg/Kg - dry 0.0144
0.066 11/22/2023 15:438260DAcetonemg/Kg - dry 0.002
0.311 12/06/2023 13:27SW-7199 Chromium, Hexavalent mg/Kg - dry 0.169
16.8 11/22/2023 10:22SW-DRYWT Moisture %
V 89893SB-2 (0-2)
0.877 12/09/2023 15:336020BArsenicmg/Kg - dry 0.108
97.4 12/09/2023 15:336020BBariummg/Kg - dry 0.053
132 12/12/2023 00:286020BChromiummg/Kg - dry 0.146
4.01 12/09/2023 15:336020BLeadmg/Kg - dry 0.0390
0.318 12/09/2023 15:336020BSeleniummg/Kg - dry 0.129
J0.0128 12/09/2023 15:336020BSilvermg/Kg - dry 0.0084
J0.0181 11/30/2023 16:457471BMercury (Total)mg/Kg - dry 0.0151
0.048 11/22/2023 16:108260DAcetonemg/Kg - dry 0.003
J0.002 11/22/2023 16:108260DMethylene Chloride mg/Kg - dry 0.001
0.428 12/06/2023 13:38SW-7199 Chromium, Hexavalent mg/Kg - dry 0.211
20.6 11/22/2023 10:22SW-DRYWT Moisture %
V 89894SB-3 (0-2)
1.16 12/09/2023 15:376020BArsenicmg/Kg - dry 0.0994
57.7 12/09/2023 15:376020BBariummg/Kg - dry 0.049
22.7 12/12/2023 00:326020BChromiummg/Kg - dry 0.134
7.83 12/09/2023 15:376020BLeadmg/Kg - dry 0.0360
J0.269 12/09/2023 15:376020BSeleniummg/Kg - dry 0.119
J0.0130 12/09/2023 15:376020BSilvermg/Kg - dry 0.0078
0.056 11/22/2023 16:378260DAcetonemg/Kg - dry 0.002
14.0 11/22/2023 10:22SW-DRYWT Moisture %
V 89895SB-4 (0-2)
1.63 12/09/2023 15:416020BArsenicmg/Kg - dry 0.0981
49.8 12/09/2023 15:416020BBariummg/Kg - dry 0.049
97.4 12/12/2023 00:366020BChromiummg/Kg - dry 0.133
7.53 12/09/2023 15:416020BLeadmg/Kg - dry 0.0355
0.402 12/09/2023 15:416020BSeleniummg/Kg - dry 0.118
J0.0177 12/09/2023 15:416020BSilvermg/Kg - dry 0.0077
0.0550 11/30/2023 16:507471BMercury (Total)mg/Kg - dry 0.0138
0.070 11/22/2023 17:048260DAcetonemg/Kg - dry 0.002
J0.001 11/22/2023 17:048260DToluenemg/Kg - dry 0.0008
Page 7 of 208
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-325-0008
Report Limit
Project:Former Winston Container
V 89895SB-4 (0-2)
JM0.955 11/27/2023 15:278270EBenzoic Acid mg/Kg - dry 0.665
0.344 12/06/2023 14:22SW-7199 Chromium, Hexavalent mg/Kg - dry 0.174
12.9 11/22/2023 10:22SW-DRYWT Moisture %
V 89896SB-5 (0-2)
0.662 12/09/2023 15:456020BArsenicmg/Kg - dry 0.0931
78.3 12/09/2023 15:456020BBariummg/Kg - dry 0.046
60.0 12/12/2023 00:406020BChromiummg/Kg - dry 0.126
4.67 12/09/2023 15:456020BLeadmg/Kg - dry 0.0337
J0.261 12/09/2023 15:456020BSeleniummg/Kg - dry 0.112
J0.0112 12/09/2023 15:456020BSilvermg/Kg - dry 0.0073
J0.0230 11/30/2023 16:537471BMercury (Total)mg/Kg - dry 0.0131
0.101 11/22/2023 17:318260DAcetonemg/Kg - dry 0.002
J0.001 11/22/2023 17:318260DToluenemg/Kg - dry 0.0007
0.417 12/06/2023 12:22SW-7199 Chromium, Hexavalent mg/Kg - dry 0.153
8.18 11/22/2023 10:22SW-DRYWT Moisture %
V 89897SB-6 (0-2)
2.20 12/09/2023 15:586020BArsenicmg/Kg - dry 0.0948
336 12/09/2023 15:586020BBariummg/Kg - dry 0.047
1.55 12/09/2023 15:586020BCadmiummg/Kg - dry 0.0288
99.1 12/09/2023 15:586020BChromiummg/Kg - dry 0.128
184 12/09/2023 15:586020BLeadmg/Kg - dry 0.0344
0.662 12/09/2023 15:586020BSeleniummg/Kg - dry 0.114
0.613 12/09/2023 15:586020BSilvermg/Kg - dry 0.0074
0.0550 11/30/2023 16:557471BMercury (Total)mg/Kg - dry 0.0133
0.179 11/22/2023 17:598260DAcetonemg/Kg - dry 0.002
J0.0007 11/22/2023 17:598260DEthylbenzenemg/Kg - dry 0.0006
J0.004 11/22/2023 17:598260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.003 11/22/2023 17:598260DToluenemg/Kg - dry 0.0007
J0.002 11/22/2023 17:598260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0005
J0.0009 11/22/2023 17:598260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
J0.001 11/22/2023 17:598260Do-Xylene mg/Kg - dry 0.0006
J0.002 11/22/2023 17:598260Dm,p-Xylene mg/Kg - dry 0.001
J0.004 11/22/2023 17:598260DXylene (Total)mg/Kg - dry 0.0006
1.14 11/27/2023 18:508270EBis(2-ethylhexyl)phthalate mg/Kg - dry 0.133
1.51 12/06/2023 14:33SW-7199 Chromium, Hexavalent mg/Kg - dry 0.156
Page 8 of 208
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-325-0008
Report Limit
Project:Former Winston Container
V 89897SB-6 (0-2)
9.89 11/22/2023 10:22SW-DRYWT Moisture %
V 89898SB-7 (0-2)
1.24 12/09/2023 16:026020BArsenicmg/Kg - dry 0.101
84.5 12/09/2023 16:026020BBariummg/Kg - dry 0.050
J0.128 12/09/2023 16:026020BCadmiummg/Kg - dry 0.0308
48.0 12/09/2023 16:026020BChromiummg/Kg - dry 0.137
21.2 12/09/2023 16:026020BLeadmg/Kg - dry 0.0367
0.436 12/09/2023 16:026020BSeleniummg/Kg - dry 0.122
J0.0581 12/09/2023 16:026020BSilvermg/Kg - dry 0.0079
0.069 11/27/2023 21:008260DAcetonemg/Kg - dry 0.002
J0.003 11/27/2023 21:008260DBenzenemg/Kg - dry 0.0007
0.015 11/27/2023 21:008260D1,2-Dichlorobenzene mg/Kg - dry 0.0004
J0.001 11/27/2023 21:008260D1,3-Dichlorobenzene mg/Kg - dry 0.0005
0.010 11/27/2023 21:008260D1,4-Dichlorobenzene mg/Kg - dry 0.0007
0.034 11/27/2023 21:008260D1,1-Dichloroethane mg/Kg - dry 0.001
J0.002 11/27/2023 21:008260D1,1-Dichloroethene mg/Kg - dry 0.0009
0.008 11/27/2023 21:008260Dcis-1,2-Dichloroethene mg/Kg - dry 0.0009
0.011 11/27/2023 21:008260DEthylbenzenemg/Kg - dry 0.0007
J0.005 11/27/2023 21:008260Dn-Hexane mg/Kg - dry 0.0008
0.018 11/27/2023 21:008260DIsopropylbenzenemg/Kg - dry 0.0005
J0.005 11/27/2023 21:008260D4-Isopropyl toluene mg/Kg - dry 0.001
0.018 11/27/2023 21:008260DNaphthalenemg/Kg - dry 0.001
0.022 11/27/2023 21:008260DToluenemg/Kg - dry 0.0008
J0.003 11/27/2023 21:008260D1,2,3-Trichlorobenzene mg/Kg - dry 0.0006
0.029 11/27/2023 21:008260D1,2,4-Trichlorobenzene mg/Kg - dry 0.0008
J0.004 11/27/2023 21:008260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.002 11/27/2023 21:008260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
J0.001 11/27/2023 21:008260DVinyl Chloride mg/Kg - dry 0.0006
0.013 11/27/2023 21:008260Do-Xylene mg/Kg - dry 0.0006
0.026 11/27/2023 21:008260Dm,p-Xylene mg/Kg - dry 0.001
0.039 11/27/2023 21:008260DXylene (Total)mg/Kg - dry 0.0006
1.13 12/06/2023 14:44SW-7199 Chromium, Hexavalent mg/Kg - dry 0.167
15.6 11/22/2023 10:22SW-DRYWT Moisture %
V 89899SB-8 (0-2)
2.11 12/09/2023 16:306020BArsenicmg/Kg - dry 0.0949
254 12/09/2023 16:306020BBariummg/Kg - dry 0.047
Page 9 of 208
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-325-0008
Report Limit
Project:Former Winston Container
V 89899SB-8 (0-2)
2.86 12/09/2023 16:306020BCadmiummg/Kg - dry 0.0288
83.0 12/09/2023 16:306020BChromiummg/Kg - dry 0.128
252 12/09/2023 16:306020BLeadmg/Kg - dry 0.0344
0.516 12/09/2023 16:306020BSeleniummg/Kg - dry 0.114
J0.0844 12/09/2023 16:306020BSilvermg/Kg - dry 0.0074
0.194 11/30/2023 17:007471BMercury (Total)mg/Kg - dry 0.0133
0.0099 11/30/2023 19:458081Balpha-BHC mg/Kg - dry 0.0012
0.0663 11/30/2023 19:458081B4,4'-DDT mg/Kg - dry 0.0016
0.0722 11/30/2023 19:458081BHeptachlormg/Kg - dry 0.0015
0.109 11/27/2023 21:278260DAcetonemg/Kg - dry 0.002
0.008 11/27/2023 21:278260DBenzenemg/Kg - dry 0.0006
J0.0006 11/27/2023 21:278260Dn-Butylbenzene mg/Kg - dry 0.0005
J0.0007 11/27/2023 21:278260Dsec-Butyl benzene mg/Kg - dry 0.0006
J0.003 11/27/2023 21:278260DCarbon Disulfide mg/Kg - dry 0.0007
0.011 11/27/2023 21:278260D1,2-Dichlorobenzene mg/Kg - dry 0.0003
J0.003 11/27/2023 21:278260D1,3-Dichlorobenzene mg/Kg - dry 0.0004
J0.004 11/27/2023 21:278260D1,4-Dichlorobenzene mg/Kg - dry 0.0007
J0.001 11/27/2023 21:278260D1,1-Dichloroethane mg/Kg - dry 0.0009
0.009 11/27/2023 21:278260Dcis-1,2-Dichloroethene mg/Kg - dry 0.0009
0.012 11/27/2023 21:278260DEthylbenzenemg/Kg - dry 0.0006
0.070 11/27/2023 21:278260Dn-Hexane mg/Kg - dry 0.0007
J0.001 11/27/2023 21:278260DIsopropylbenzenemg/Kg - dry 0.0005
0.006 11/27/2023 21:278260D4-Isopropyl toluene mg/Kg - dry 0.001
J0.003 11/27/2023 21:278260DNaphthalenemg/Kg - dry 0.001
J0.001 11/27/2023 21:278260Dn-Propylbenzene mg/Kg - dry 0.0006
0.021 11/27/2023 21:278260DToluenemg/Kg - dry 0.0007
J0.001 11/27/2023 21:278260D1,2,3-Trichlorobenzene mg/Kg - dry 0.0006
0.025 11/27/2023 21:278260D1,2,4-Trichlorobenzene mg/Kg - dry 0.0007
J0.001 11/27/2023 21:278260DTrichloroethenemg/Kg - dry 0.001
0.008 11/27/2023 21:278260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0005
J0.003 11/27/2023 21:278260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
0.015 11/27/2023 21:278260Do-Xylene mg/Kg - dry 0.0006
0.020 11/27/2023 21:278260Dm,p-Xylene mg/Kg - dry 0.001
0.036 11/27/2023 21:278260DXylene (Total)mg/Kg - dry 0.0006
103 11/27/2023 18:278270EBis(2-ethylhexyl)phthalate mg/Kg - dry 2.66
J2.00 11/27/2023 16:128270EButyl benzyl phthalate mg/Kg - dry 1.00
J1.22 11/27/2023 16:128270E1,2,4-Trichlorobenzene mg/Kg - dry 0.950
Page 10 of 208
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-325-0008
Report Limit
Project:Former Winston Container
V 89899SB-8 (0-2)
9.91 11/22/2023 10:22SW-DRYWT Moisture %
V 89900SB-9 (0-2)
0.867 12/09/2023 16:346020BArsenicmg/Kg - dry 0.110
129 12/09/2023 16:346020BBariummg/Kg - dry 0.054
78.5 12/09/2023 16:346020BChromiummg/Kg - dry 0.148
4.69 12/09/2023 16:346020BLeadmg/Kg - dry 0.0397
0.608 12/09/2023 16:346020BSeleniummg/Kg - dry 0.132
0.0574 12/01/2023 16:247471BMercury (Total)mg/Kg - dry 0.0154
J0.0061 11/30/2023 19:588081B4,4'-DDT mg/Kg - dry 0.0019
0.0266 11/30/2023 19:588081BDieldrinmg/Kg - dry 0.0026
0.062 11/22/2023 18:268260DAcetonemg/Kg - dry 0.003
0.428 12/06/2023 17:47SW-7199 Chromium, Hexavalent mg/Kg - dry 0.180
22.0 11/22/2023 10:22SW-DRYWT Moisture %
V 89901SB-10 (0-2)
0.424 12/09/2023 16:476020BArsenicmg/Kg - dry 0.0892
188 12/09/2023 16:476020BBariummg/Kg - dry 0.044
J0.116 12/09/2023 16:476020BCadmiummg/Kg - dry 0.0271
27.8 12/09/2023 16:476020BChromiummg/Kg - dry 0.121
3.27 12/09/2023 16:476020BLeadmg/Kg - dry 0.0323
J0.244 12/09/2023 16:476020BSeleniummg/Kg - dry 0.107
J0.0234 12/09/2023 16:476020BSilvermg/Kg - dry 0.0070
J0.0134 12/01/2023 16:267471BMercury (Total)mg/Kg - dry 0.0125
J0.019 11/22/2023 18:538260DAcetonemg/Kg - dry 0.002
J0.203 12/06/2023 17:58SW-7199 Chromium, Hexavalent mg/Kg - dry 0.147
4.24 11/22/2023 10:22SW-DRYWT Moisture %
V 89902SB-11 (0-2)
0.327 12/09/2023 16:516020BArsenicmg/Kg - dry 0.0881
238 12/09/2023 16:516020BBariummg/Kg - dry 0.044
J0.0698 12/09/2023 16:516020BCadmiummg/Kg - dry 0.0268
22.4 12/09/2023 16:516020BChromiummg/Kg - dry 0.119
3.62 12/09/2023 16:516020BLeadmg/Kg - dry 0.0319
0.271 12/09/2023 16:516020BSeleniummg/Kg - dry 0.106
J0.0215 12/09/2023 16:516020BSilvermg/Kg - dry 0.0069
0.022 11/22/2023 19:208260DAcetonemg/Kg - dry 0.002
3.04 11/22/2023 10:22SW-DRYWT Moisture %
Page 11 of 208
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-325-0008
Report Limit
Project:Former Winston Container
V 89903DUP-3
1.30 12/09/2023 16:556020BArsenicmg/Kg - dry 0.0940
190 12/09/2023 16:556020BBariummg/Kg - dry 0.047
2.94 12/09/2023 16:556020BCadmiummg/Kg - dry 0.0286
44.2 12/09/2023 16:556020BChromiummg/Kg - dry 0.127
51.5 12/09/2023 16:556020BLeadmg/Kg - dry 0.0341
0.842 12/09/2023 16:556020BSeleniummg/Kg - dry 0.113
J0.0829 12/09/2023 16:556020BSilvermg/Kg - dry 0.0074
0.367 12/01/2023 16:507471BMercury (Total)mg/Kg - dry 0.0132
0.0660 11/30/2023 20:398081Balpha-Chlordane mg/Kg - dry 0.0020
Q0.0388 11/30/2023 20:398081Bgamma-Chlordane mg/Kg - dry 0.0018
0.0390 11/30/2023 20:398081B4,4'-DDE mg/Kg - dry 0.0022
0.0518 11/30/2023 20:398081B4,4'-DDT mg/Kg - dry 0.0016
0.0586 11/30/2023 20:398081BDieldrinmg/Kg - dry 0.0022
0.113 11/22/2023 19:488260DAcetonemg/Kg - dry 0.002
J0.004 11/22/2023 19:488260DBenzenemg/Kg - dry 0.0006
J0.0008 11/22/2023 19:488260Dsec-Butyl benzene mg/Kg - dry 0.0006
0.005 11/22/2023 19:488260DCarbon Disulfide mg/Kg - dry 0.0007
0.009 11/22/2023 19:488260D1,2-Dichlorobenzene mg/Kg - dry 0.0003
J0.001 11/22/2023 19:488260D1,3-Dichlorobenzene mg/Kg - dry 0.0004
J0.004 11/22/2023 19:488260D1,4-Dichlorobenzene mg/Kg - dry 0.0007
0.025 11/22/2023 19:488260D1,1-Dichloroethane mg/Kg - dry 0.0009
J0.002 11/22/2023 19:488260D1,1-Dichloroethene mg/Kg - dry 0.0008
0.017 11/22/2023 19:488260Dcis-1,2-Dichloroethene mg/Kg - dry 0.0009
0.021 11/22/2023 19:488260DEthylbenzenemg/Kg - dry 0.0006
0.018 11/22/2023 19:488260Dn-Hexane mg/Kg - dry 0.0007
0.012 11/22/2023 19:488260DIsopropylbenzenemg/Kg - dry 0.0005
J0.004 11/22/2023 19:488260D4-Isopropyl toluene mg/Kg - dry 0.001
0.012 11/22/2023 19:488260DNaphthalenemg/Kg - dry 0.001
J0.001 11/22/2023 19:488260Dn-Propylbenzene mg/Kg - dry 0.0006
0.015 11/22/2023 19:488260DToluenemg/Kg - dry 0.0007
J0.002 11/22/2023 19:488260D1,2,3-Trichlorobenzene mg/Kg - dry 0.0006
0.020 11/22/2023 19:488260D1,2,4-Trichlorobenzene mg/Kg - dry 0.0007
0.010 11/22/2023 19:488260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0005
0.007 11/22/2023 19:488260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
J0.003 11/22/2023 19:488260DVinyl Chloride mg/Kg - dry 0.0005
0.030 11/22/2023 19:488260Do-Xylene mg/Kg - dry 0.0006
0.129 11/22/2023 19:488260Dm,p-Xylene mg/Kg - dry 0.001
Page 12 of 208
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-325-0008
Report Limit
Project:Former Winston Container
V 89903DUP-3
0.159 11/22/2023 19:488260DXylene (Total)mg/Kg - dry 0.0006
J0.707 11/27/2023 16:348270EBenzo(a)anthracene mg/Kg - dry 0.611
J0.717 11/27/2023 16:348270EBenzo(a)pyrene mg/Kg - dry 0.646
J0.905 11/27/2023 16:348270EBenzo(b)fluoranthene mg/Kg - dry 0.642
J2.88 11/27/2023 16:348270EBis(2-ethylhexyl)phthalate mg/Kg - dry 0.528
J0.695 11/27/2023 16:348270EChrysenemg/Kg - dry 0.624
J1.85 11/27/2023 16:348270EDi-n-butyl phthalate mg/Kg - dry 0.470
J1.46 11/27/2023 16:348270EFluoranthenemg/Kg - dry 0.541
J0.474 11/27/2023 16:348270E1-Methylnaphthalene mg/Kg - dry 0.466
J1.08 11/27/2023 16:348270E2-Methylnaphthalene mg/Kg - dry 0.440
J1.11 11/27/2023 16:348270EPhenanthrenemg/Kg - dry 0.915
J1.33 11/27/2023 16:348270EPyrenemg/Kg - dry 0.589
J1.17 11/27/2023 16:348270E1,2,4-Trichlorobenzene mg/Kg - dry 0.470
9.11 11/27/2023 12:18SW-DRYWT Moisture %
Page 13 of 208

Client: Mid-Atlantic Associates, Inc. - Raleigh CASE NARRATIVE
Project: Former Winston Container Lab Report Number: 23-325-0008
Date: 12/12/2023
Metals Analyses Method 6020B Sample 89898 (SB-7 (0-2)) Analyte: Arsenic
QC Batch No: L721715/L719373 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 89898 (SB-7 (0-2))
Analyte: Barium QC Batch No: L721715/L719373
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 89898 (SB-7 (0-2))
Analyte: Chromium QC Batch No: L721715/L719373
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 89898 (SB-7 (0-2)) Analyte: Lead QC Batch No: L721715/L719373
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 89898 (SB-7 (0-2))
Analyte: Selenium QC Batch No: L721715/L719373 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 89898 (SB-7 (0-2)) Analyte: Selenium QC Batch No: L722026/L719373 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94846 (Y311535-08) Analyte: Arsenic QC Batch No: L721715/L719374 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 14 of 208

Sample 94846 (Y311535-08) Analyte: Barium
QC Batch No: L721715/L719374 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94846 (Y311535-08) Analyte: Lead
QC Batch No: L721715/L719374 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Hexavalent Chromium by Ion Chromatography Method SW-7199 Sample 89896 (SB-5 (0-2)) Analyte: Hexavalent Chromium
QC Batch No: L720894/L720353 Matrix Spike Recovery Low: A measure of the sample pH and its oxidation reduction potential (ORP) indicate that
the sample has reducing qualities which may not allow for the presence of Hexavalent Chromium.
Sample 89902 (SB-11 (0-2)) Analyte: Hexavalent Chromium QC Batch No: L720941/L720354 Matrix Spike Recovery Low: A measure of the sample pH and its oxidation reduction potential (ORP) indicate that
the sample has reducing qualities which may not allow for the presence of Hexavalent Chromium. Organochlorine Pesticides by GC Method 8081B Sample 89889 (WL-1) Analyte: 4,4`-DDE QC Batch No: V40768/V40673 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 89889 (WL-1)
Analyte: 4,4`-DDT QC Batch No: V40768/V40673 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 89889 (WL-1) Analyte: alpha-Chlordane QC Batch No: V40768/V40673 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 89889 (WL-1) Analyte: beta-BHC QC Batch No: V40768/V40673 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 89889 (WL-1) Analyte: delta-BHC QC Batch No: V40768/V40673
Page 15 of 208

Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 89889 (WL-1)
Analyte: Dieldrin QC Batch No: V40768/V40673
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 89889 (WL-1)
Analyte: Dieldrin QC Batch No: V40768/V40673
The MS/MSD recoveries are outside QC limits due to the level of analyte present in the parent sample relative to the spike level. RPD is based on the MS/MSD results and should be evaluated as laboratory duplicates.
Sample 89889 (WL-1)
Analyte: Endosulfan I QC Batch No: V40768/V40673
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 89889 (WL-1) Analyte: Endrin aldehyde
QC Batch No: V40768/V40673 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 89889 (WL-1) Analyte: gamma-BHC
QC Batch No: V40768/V40673 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 89889 (WL-1) Analyte: gamma-Chlordane QC Batch No: V40768/V40673
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 89889 (WL-1) Analyte: Heptachlor QC Batch No: V40768/V40673 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 89889 (WL-1) Analyte: Heptachlor epoxide QC Batch No: V40768/V40673 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 89889 (WL-1) Analyte: Methoxychlor QC Batch No: V40768/V40673 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 89903 (DUP-3)
Page 16 of 208

Analyte: Tetrachloro-m-xylene
QC Batch No: V40768/V40673 Surrogate peak co-elude with non target analyte due to sample matrix. Dilutions confirm similar results. No effect
to other target analytes. Volatile Organic Compounds - GC/MS Method 8260D Analyte: 2-Butanone
QC Batch No: V40819/V40553 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Acetone
QC Batch No: V40819/V40553 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Acrolein
QC Batch No: V40819/V40553 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Acrylonitrile
QC Batch No: V40819/V40553 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Semivolatile Organic Compounds - GC/MS Method 8270E Sample 89889 (WL-1) QC Batch No: V40513/V40498
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 89899 (SB-8 (0-2)) QC Batch No: V40513/V40498 This sample extract was unable to be concentrated to the default method final volume. The final volume adjustment due to viscous extracts may result in surrogate recoveries below the minimum detectable concentration. Final volume of 2mL Sample 89899 (SB-8 (0-2)) QC Batch No: V40513/V40498 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample 89903 (DUP-3) QC Batch No: V40513/V40498 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Analyte: Benzoic Acid QC Batch No: V40513/V40498
Page 17 of 208

This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
The result for Benzoic acid was 4.444 which calculates to a recovery of 8.888%. This is below the acceptable recovery range.

Page 18 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-1b
89888 Matrix:
11/20/2023 12:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
7.98 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 19 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-1b
89888 Matrix:
11/20/2023 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.177 mg/Kg - dry 0.002 0.021Acetone 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.021Acrolein 1 11/22/23 14:49 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 11/22/23 14:49 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 11/22/23 14:49 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 11/22/23 14:49 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Bromomethane 1 11/22/23 14:49 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 11/22/23 14:49 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/22/23 14:49 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 11/22/23 14:49 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/22/23 14:49 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 11/22/23 14:49 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 11/22/23 14:49 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/22/23 14:49 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 11/22/23 14:49 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/22/23 14:49 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/22/23 14:49 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/22/23 14:49 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 20 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-1b
89888 Matrix:
11/20/2023 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 11/22/23 14:49 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 11/22/23 14:49 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/22/23 14:49 V40555TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 11/22/23 14:49 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/22/23 14:49 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 11/22/23 14:49 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/22/23 14:49 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/22/23 14:49 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/22/23 14:49 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/22/23 14:49 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/22/23 14:49 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 11/22/23 14:49 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/22/23 14:49 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/22/23 14:49 V40555TBL
0.001 J mg/Kg - dry 0.0006 0.005Ethylbenzene 1 11/22/23 14:49 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.054Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 14:49 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.010Hexachlorobutadiene 1 11/22/23 14:49 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 11/22/23 14:49 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 21 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-1b
89888 Matrix:
11/20/2023 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0212-Hexanone 1 11/22/23 14:49 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/22/23 14:49 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 11/22/23 14:49 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/22/23 14:49 V40555TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Naphthalene 1 11/22/23 14:49 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/22/23 14:49 V40555TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 11/22/23 14:49 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.005 1 11/22/23 14:49 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005 1 11/22/23 14:49 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 11/22/23 14:49 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 11/22/23 14:49 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/22/23 14:49 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/22/23 14:49 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.005 1 11/22/23 14:49 V40555TBL
<0.002 mg/Kg - dry 0.002 0.010 1 11/22/23 14:49 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/22/23 14:49 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 11/22/23 14:49 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 22 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-1b
89888 Matrix:
11/20/2023 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/22/23 14:49 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 11/22/23 14:49 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 11/22/23 14:49 V40555TBL
0.003 J mg/Kg - dry 0.0005 0.005o-Xylene 1 11/22/23 14:49 V40555TBL
0.008 J mg/Kg - dry 0.001 0.010m,p-Xylene 1 11/22/23 14:49 V40555TBL
0.011 J mg/Kg - dry 0.0005 0.005Xylene (Total)1 11/22/23 14:49 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 23 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-1
89889 Matrix:
11/20/2023 12:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.6 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
1.16 mg/Kg - dry 0.175 0.248Chromium, Hexavalent 1 12/06/23 13:06 SW-7199SWB
1.00 mg/Kg - dry 0.106 0.311Arsenic 5 12/09/23 15:21 6020BBKN
44.3 mg/Kg - dry 0.053 0.310Barium 5 12/09/23 15:21 6020BBKN
0.0585 J mg/Kg - dry 0.0323 0.311Cadmium 5 12/09/23 15:21 6020BBKN
31.2 mg/Kg - dry 0.144 0.310Chromium 5 12/12/23 00:07 6020BJTR
8.92 mg/Kg - dry 0.0385 0.311Lead 5 12/09/23 15:21 6020BBKN
0.131 mg/Kg - dry 0.0149 0.0373Mercury (Total)1 11/30/23 16:38 7471BJKC
0.453 mg/Kg - dry 0.128 0.310Selenium 5 12/09/23 15:21 6020BJTR
0.0140 J mg/Kg - dry 0.0083 0.311Silver 5 12/09/23 15:21 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 24 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-1
89889 Matrix:
11/20/2023 12:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0022 mg/Kg - dry 0.0022 0.0062Aldrin 1 11/30/23 17:44 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0062alpha-BHC 1 11/30/23 17:44 V40768TJW
<0.0024 mg/Kg - dry 0.0024 0.0062beta-BHC 1 11/30/23 17:44 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.0062delta-BHC 1 11/30/23 17:44 V40768TJW
<0.0218 mg/Kg - dry 0.0218 0.0621Chlordane 1 11/30/23 17:44 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0062alpha-Chlordane 1 11/30/23 17:44 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0062gamma-Chlordane 1 11/30/23 17:44 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.00624,4'-DDD 1 11/30/23 17:44 V40768TJW
0.0125 mg/Kg - dry 0.0025 0.00624,4'-DDE 1 11/30/23 17:44 V40768TJW
0.0314 mg/Kg - dry 0.0018 0.00624,4'-DDT 1 11/30/23 17:44 V40768TJW
0.0553 mg/Kg - dry 0.0025 0.0062Dieldrin 1 11/30/23 17:44 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0062Endosulfan I 1 11/30/23 17:44 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0062Endosulfan II 1 11/30/23 17:44 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0062Endosulfan Sulfate 1 11/30/23 17:44 V40768TJW
0.0166 Q mg/Kg - dry 0.0023 0.0062Endrin 1 11/30/23 17:44 V40768TJW
0.0075 mg/Kg - dry 0.0026 0.0062Endrin Aldehyde 1 11/30/23 17:44 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0062Endrin Ketone 1 11/30/23 17:44 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.0062gamma-BHC 1 11/30/23 17:44 V40768TJW
0.0017 J mg/Kg - dry 0.0016 0.0062Heptachlor 1 11/30/23 17:44 V40768TJW
0.0303 mg/Kg - dry 0.0022 0.0062Heptachlor Epoxide 1 11/30/23 17:44 V40768TJW
<0.0032 mg/Kg - dry 0.0032 0.0062Methoxychlor 1 11/30/23 17:44 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 25 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-1
89889 Matrix:
11/20/2023 12:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
0.647 mg/Kg - dry 0.0126 0.0621 1 11/30/23 17:44 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.577 mg/Kg - dry 0.577 3.28Acenaphthene 4 11/27/23 14:42 V40513AMP
0.671 J mg/Kg - dry 0.522 3.28Acenaphthylene 4 11/27/23 14:42 V40513AMP
<0.756 mg/Kg - dry 0.756 3.28Aniline 4 11/27/23 14:42 V40513AMP
<0.711 mg/Kg - dry 0.711 3.28Anthracene 4 11/27/23 14:42 V40513AMP
1.89 J mg/Kg - dry 0.691 3.28Benzo(a)anthracene 4 11/27/23 14:42 V40513AMP
1.99 J mg/Kg - dry 0.731 3.28Benzo(a)pyrene 4 11/27/23 14:42 V40513AMP
2.55 J mg/Kg - dry 0.726 3.28Benzo(b)fluoranthene 4 11/27/23 14:42 V40513AMP
1.48 J mg/Kg - dry 0.676 3.28Benzo(g,h,i)perylene 4 11/27/23 14:42 V40513AMP
0.890 J mg/Kg - dry 0.681 3.28Benzo(k)fluoranthene 4 11/27/23 14:42 V40513AMP
<2.89 M mg/Kg - dry 2.89 9.95Benzoic Acid 4 11/27/23 14:42 V40513AMP
<0.522 mg/Kg - dry 0.522 3.28Benzyl alcohol 4 11/27/23 14:42 V40513AMP
<0.587 mg/Kg - dry 0.587 3.28Bis(2-Chloroethoxy)methane 4 11/27/23 14:42 V40513AMP
<0.532 mg/Kg - dry 0.532 3.28Bis(2-Chloroethyl)ether 4 11/27/23 14:42 V40513AMP
<0.676 mg/Kg - dry 0.676 1.64Bis(2-Chloroisopropyl)ether 4 11/27/23 14:42 V40513AMP
0.997 J mg/Kg - dry 0.597 3.28Bis(2-ethylhexyl)phthalate 4 11/27/23 14:42 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 26 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-1
89889 Matrix:
11/20/2023 12:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.542 mg/Kg - dry 0.542 3.284-Bromophenyl phenyl ether 4 11/27/23 14:42 V40513AMP
<0.562 mg/Kg - dry 0.562 1.64Butyl benzyl phthalate 4 11/27/23 14:42 V40513AMP
<0.460 mg/Kg - dry 0.460 3.284-Chloro-3-methylphenol 4 11/27/23 14:42 V40513AMP
<0.557 mg/Kg - dry 0.557 1.644-Chloroaniline 4 11/27/23 14:42 V40513AMP
<0.577 mg/Kg - dry 0.577 3.282-Chloronaphthalene 4 11/27/23 14:42 V40513AMP
<0.488 mg/Kg - dry 0.488 3.282-Chlorophenol 4 11/27/23 14:42 V40513AMP
<0.626 mg/Kg - dry 0.626 4.984-Chlorophenyl phenyl ether 4 11/27/23 14:42 V40513AMP
1.73 J mg/Kg - dry 0.706 3.28Chrysene 4 11/27/23 14:42 V40513AMP
<1.14 mg/Kg - dry 1.14 3.28Dibenz(a,h)anthracene 4 11/27/23 14:42 V40513AMP
<0.592 mg/Kg - dry 0.592 3.28Dibenzofuran 4 11/27/23 14:42 V40513AMP
<0.470 mg/Kg - dry 0.470 3.281,2-Dichlorobenzene 4 11/27/23 14:42 V40513AMP
<0.483 mg/Kg - dry 0.483 3.281,3-Dichlorobenzene 4 11/27/23 14:42 V40513AMP
<0.485 mg/Kg - dry 0.485 1.641,4-Dichlorobenzene 4 11/27/23 14:42 V40513AMP
<0.731 mg/Kg - dry 0.731 3.283,3'-Dichlorobenzidine 4 11/27/23 14:42 V40513AMP
<0.476 mg/Kg - dry 0.476 3.282,4-Dichlorophenol 4 11/27/23 14:42 V40513AMP
<0.895 mg/Kg - dry 0.895 3.28Diethyl phthalate 4 11/27/23 14:42 V40513AMP
<0.865 mg/Kg - dry 0.865 3.28Dimethyl phthalate 4 11/27/23 14:42 V40513AMP
<0.537 mg/Kg - dry 0.537 1.642,4-Dimethylphenol 4 11/27/23 14:42 V40513AMP
<0.532 mg/Kg - dry 0.532 3.28Di-n-butyl phthalate 4 11/27/23 14:42 V40513AMP
<1.19 mg/Kg - dry 1.19 7.464,6-Dinitro-2-methylphenol 4 11/27/23 14:42 V40513AMP
<2.59 mg/Kg - dry 2.59 7.462,4-Dinitrophenol 4 11/27/23 14:42 V40513AMP
<0.480 mg/Kg - dry 0.480 3.282,4-Dinitrotoluene 4 11/27/23 14:42 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 27 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-1
89889 Matrix:
11/20/2023 12:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.537 mg/Kg - dry 0.537 3.282,6-Dinitrotoluene 4 11/27/23 14:42 V40513AMP
<0.711 mg/Kg - dry 0.711 1.64Di-n-Octyl Phthalate 4 11/27/23 14:42 V40513AMP
4.08 mg/Kg - dry 0.611 3.28Fluoranthene 4 11/27/23 14:42 V40513AMP
<0.636 mg/Kg - dry 0.636 3.28Fluorene 4 11/27/23 14:42 V40513AMP
<0.527 mg/Kg - dry 0.527 3.28Hexachlorobenzene 4 11/27/23 14:42 V40513AMP
<0.485 mg/Kg - dry 0.485 3.28Hexachlorobutadiene 4 11/27/23 14:42 V40513AMP
<0.781 mg/Kg - dry 0.781 3.28Hexachlorocyclopentadiene 4 11/27/23 14:42 V40513AMP
<0.394 mg/Kg - dry 0.394 3.28Hexachloroethane 4 11/27/23 14:42 V40513AMP
1.41 J mg/Kg - dry 0.890 3.28Indeno(1,2,3-cd)pyrene 4 11/27/23 14:42 V40513AMP
<0.950 mg/Kg - dry 0.950 3.28Isophorone 4 11/27/23 14:42 V40513AMP
<0.527 mg/Kg - dry 0.527 3.281-Methylnaphthalene 4 11/27/23 14:42 V40513AMP
<0.497 mg/Kg - dry 0.497 3.282-Methylnaphthalene 4 11/27/23 14:42 V40513AMP
<0.482 mg/Kg - dry 0.482 3.282-Methylphenol 4 11/27/23 14:42 V40513AMP
<0.422 mg/Kg - dry 0.422 3.283&4 Methylphenol 4 11/27/23 14:42 V40513AMP
<0.716 mg/Kg - dry 0.716 3.28Naphthalene 4 11/27/23 14:42 V40513AMP
<0.481 mg/Kg - dry 0.481 3.282-Nitroaniline 4 11/27/23 14:42 V40513AMP
<0.597 mg/Kg - dry 0.597 3.283-Nitroaniline 4 11/27/23 14:42 V40513AMP
<0.463 mg/Kg - dry 0.463 1.644-Nitroaniline 4 11/27/23 14:42 V40513AMP
<0.577 mg/Kg - dry 0.577 1.64Nitrobenzene 4 11/27/23 14:42 V40513AMP
<0.441 mg/Kg - dry 0.441 3.282-Nitrophenol 4 11/27/23 14:42 V40513AMP
<0.582 mg/Kg - dry 0.582 3.284-Nitrophenol 4 11/27/23 14:42 V40513AMP
<1.31 mg/Kg - dry 1.31 3.28N-Nitrosodimethylamine 4 11/27/23 14:42 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 28 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-1
89889 Matrix:
11/20/2023 12:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.900 mg/Kg - dry 0.900 3.28N-Nitrosodiphenylamine 4 11/27/23 14:42 V40513AMP
<0.587 mg/Kg - dry 0.587 3.28N-Nitroso-di-n-propylamine 4 11/27/23 14:42 V40513AMP
<1.73 mg/Kg - dry 1.73 4.98Pentachlorophenol 4 11/27/23 14:42 V40513AMP
1.27 J mg/Kg - dry 1.03 3.28Phenanthrene 4 11/27/23 14:42 V40513AMP
<0.557 mg/Kg - dry 0.557 3.28Phenol 4 11/27/23 14:42 V40513AMP
3.46 mg/Kg - dry 0.666 3.28Pyrene 4 11/27/23 14:42 V40513AMP
<0.394 mg/Kg - dry 0.394 1.64Pyridine 4 11/27/23 14:42 V40513AMP
<0.532 mg/Kg - dry 0.532 3.281,2,4-Trichlorobenzene 4 11/27/23 14:42 V40513AMP
<0.478 mg/Kg - dry 0.478 3.282,4,5-Trichlorophenol 4 11/27/23 14:42 V40513AMP
<0.480 mg/Kg - dry 0.480 3.282,4,6-Trichlorophenol 4 11/27/23 14:42 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 29 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-2c
89890 Matrix:
11/20/2023 12:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
5.60 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 30 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-2c
89890 Matrix:
11/20/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00 V40670 11/28/23 08:00
1.10 mg/Kg - dry 0.063 0.529Acetone 50 11/28/23 13:29 V40671TBL
<0.001 mg/Kg - dry 0.001 0.021Acrolein 1 11/22/23 15:16 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 11/22/23 15:16 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 11/22/23 15:16 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 11/22/23 15:16 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Bromochloromethane 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Bromomethane 1 11/22/23 15:16 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 11/22/23 15:16 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/22/23 15:16 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 11/22/23 15:16 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/22/23 15:16 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 11/22/23 15:16 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005Chlorodibromomethane 1 11/22/23 15:16 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.010Chloroethane 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/22/23 15:16 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 11/22/23 15:16 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0052-Chlorotoluene 1 11/22/23 15:16 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/22/23 15:16 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/22/23 15:16 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 31 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-2c
89890 Matrix:
11/20/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00 V40670 11/28/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 11/22/23 15:16 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 11/22/23 15:16 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/22/23 15:16 V40555TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 11/22/23 15:16 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/22/23 15:16 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,4-Dichlorobenzene 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 11/22/23 15:16 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/22/23 15:16 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/22/23 15:16 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005cis-1,2-Dichloroethene 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/22/23 15:16 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/22/23 15:16 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/22/23 15:16 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 11/22/23 15:16 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/22/23 15:16 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005trans-1,3-Dichloropropene 1 11/22/23 15:16 V40555TBL
0.001 J mg/Kg - dry 0.0006 0.005Ethylbenzene 1 11/22/23 15:16 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.052Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 15:16 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.010Hexachlorobutadiene 1 11/22/23 15:16 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 11/22/23 15:16 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 32 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-2c
89890 Matrix:
11/20/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00 V40670 11/28/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0212-Hexanone 1 11/22/23 15:16 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/22/23 15:16 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 11/22/23 15:16 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/22/23 15:16 V40555TBL
<0.015 mg/Kg - dry 0.015 0.0214-Methyl-2-Pentanone 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Naphthalene 1 11/22/23 15:16 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/22/23 15:16 V40555TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 11/22/23 15:16 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.005 1 11/22/23 15:16 V40555TBL
0.001 J mg/Kg - dry 0.0007 0.005 1 11/22/23 15:16 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 11/22/23 15:16 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 11/22/23 15:16 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/22/23 15:16 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/22/23 15:16 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.005 1 11/22/23 15:16 V40555TBL
<0.002 mg/Kg - dry 0.002 0.010 1 11/22/23 15:16 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/22/23 15:16 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 11/22/23 15:16 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 33 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-2c
89890 Matrix:
11/20/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00 V40670 11/28/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/22/23 15:16 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 11/22/23 15:16 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 11/22/23 15:16 V40555TBL
0.003 J mg/Kg - dry 0.0005 0.005o-Xylene 1 11/22/23 15:16 V40555TBL
0.007 J mg/Kg - dry 0.001 0.010m,p-Xylene 1 11/22/23 15:16 V40555TBL
0.010 J mg/Kg - dry 0.0005 0.005Xylene (Total)1 11/22/23 15:16 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 34 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-2
89891 Matrix:
11/20/2023 12:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
10.3 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
0.685 mg/Kg - dry 0.157 0.222Chromium, Hexavalent 1 12/06/23 13:16 SW-7199SWB
0.895 mg/Kg - dry 0.0953 0.279Arsenic 5 12/09/23 15:25 6020BBKN
128 mg/Kg - dry 0.047 0.278Barium 5 12/09/23 15:25 6020BBKN
0.0923 J mg/Kg - dry 0.0289 0.279Cadmium 5 12/09/23 15:25 6020BBKN
28.5 mg/Kg - dry 0.129 0.278Chromium 5 12/12/23 00:20 6020BJTR
12.5 mg/Kg - dry 0.0345 0.279Lead 5 12/09/23 15:25 6020BBKN
0.215 mg/Kg - dry 0.0134 0.0334Mercury (Total)1 11/30/23 16:40 7471BJKC
0.338 mg/Kg - dry 0.114 0.278Selenium 5 12/09/23 15:25 6020BJTR
0.0789 J mg/Kg - dry 0.0075 0.279Silver 5 12/09/23 15:25 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 35 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-2
89891 Matrix:
11/20/2023 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0020 mg/Kg - dry 0.0020 0.0055Aldrin 1 11/30/23 17:58 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0055alpha-BHC 1 11/30/23 17:58 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0055beta-BHC 1 11/30/23 17:58 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0055delta-BHC 1 11/30/23 17:58 V40768TJW
<0.0196 mg/Kg - dry 0.0196 0.0557Chlordane 1 11/30/23 17:58 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0055alpha-Chlordane 1 11/30/23 17:58 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0055gamma-Chlordane 1 11/30/23 17:58 V40768TJW
0.0480 mg/Kg - dry 0.0020 0.00554,4'-DDD 1 11/30/23 17:58 V40768TJW
0.0210 mg/Kg - dry 0.0022 0.00554,4'-DDE 1 11/30/23 17:58 V40768TJW
0.0418 mg/Kg - dry 0.0016 0.00554,4'-DDT 1 11/30/23 17:58 V40768TJW
0.0498 mg/Kg - dry 0.0023 0.0055Dieldrin 1 11/30/23 17:58 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Endosulfan I 1 11/30/23 17:58 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Endosulfan II 1 11/30/23 17:58 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endosulfan Sulfate 1 11/30/23 17:58 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0055Endrin 1 11/30/23 17:58 V40768TJW
0.0160 mg/Kg - dry 0.0023 0.0055Endrin Aldehyde 1 11/30/23 17:58 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endrin Ketone 1 11/30/23 17:58 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0055gamma-BHC 1 11/30/23 17:58 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.0055Heptachlor 1 11/30/23 17:58 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Heptachlor Epoxide 1 11/30/23 17:58 V40768TJW
<0.0029 mg/Kg - dry 0.0029 0.0055Methoxychlor 1 11/30/23 17:58 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 36 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-2
89891 Matrix:
11/20/2023 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
0.728 mg/Kg - dry 0.0113 0.0557 1 11/30/23 17:58 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.129 mg/Kg - dry 0.129 0.735Acenaphthene 1 11/27/23 18:05 V40513AMP
<0.117 mg/Kg - dry 0.117 0.735Acenaphthylene 1 11/27/23 18:05 V40513AMP
<0.169 mg/Kg - dry 0.169 0.735Aniline 1 11/27/23 18:05 V40513AMP
<0.159 mg/Kg - dry 0.159 0.735Anthracene 1 11/27/23 18:05 V40513AMP
<0.154 mg/Kg - dry 0.154 0.735Benzo(a)anthracene 1 11/27/23 18:05 V40513AMP
<0.163 mg/Kg - dry 0.163 0.735Benzo(a)pyrene 1 11/27/23 18:05 V40513AMP
<0.162 mg/Kg - dry 0.162 0.735Benzo(b)fluoranthene 1 11/27/23 18:05 V40513AMP
<0.151 mg/Kg - dry 0.151 0.735Benzo(g,h,i)perylene 1 11/27/23 18:05 V40513AMP
<0.152 mg/Kg - dry 0.152 0.735Benzo(k)fluoranthene 1 11/27/23 18:05 V40513AMP
<0.646 M mg/Kg - dry 0.646 2.23Benzoic Acid 1 11/27/23 18:05 V40513AMP
<0.117 mg/Kg - dry 0.117 0.735Benzyl alcohol 1 11/27/23 18:05 V40513AMP
<0.131 mg/Kg - dry 0.131 0.735Bis(2-Chloroethoxy)methane 1 11/27/23 18:05 V40513AMP
<0.119 mg/Kg - dry 0.119 0.735Bis(2-Chloroethyl)ether 1 11/27/23 18:05 V40513AMP
<0.151 mg/Kg - dry 0.151 0.367Bis(2-Chloroisopropyl)ether 1 11/27/23 18:05 V40513AMP
0.795 mg/Kg - dry 0.133 0.735Bis(2-ethylhexyl)phthalate 1 11/27/23 18:05 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 37 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-2
89891 Matrix:
11/20/2023 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.121 mg/Kg - dry 0.121 0.7354-Bromophenyl phenyl ether 1 11/27/23 18:05 V40513AMP
<0.125 mg/Kg - dry 0.125 0.367Butyl benzyl phthalate 1 11/27/23 18:05 V40513AMP
<0.103 mg/Kg - dry 0.103 0.7354-Chloro-3-methylphenol 1 11/27/23 18:05 V40513AMP
<0.124 mg/Kg - dry 0.124 0.3674-Chloroaniline 1 11/27/23 18:05 V40513AMP
<0.129 mg/Kg - dry 0.129 0.7352-Chloronaphthalene 1 11/27/23 18:05 V40513AMP
<0.109 mg/Kg - dry 0.109 0.7352-Chlorophenol 1 11/27/23 18:05 V40513AMP
<0.140 mg/Kg - dry 0.140 1.114-Chlorophenyl phenyl ether 1 11/27/23 18:05 V40513AMP
<0.158 mg/Kg - dry 0.158 0.735Chrysene 1 11/27/23 18:05 V40513AMP
<0.256 mg/Kg - dry 0.256 0.735Dibenz(a,h)anthracene 1 11/27/23 18:05 V40513AMP
<0.132 mg/Kg - dry 0.132 0.735Dibenzofuran 1 11/27/23 18:05 V40513AMP
<0.105 mg/Kg - dry 0.105 0.7351,2-Dichlorobenzene 1 11/27/23 18:05 V40513AMP
<0.108 mg/Kg - dry 0.108 0.7351,3-Dichlorobenzene 1 11/27/23 18:05 V40513AMP
<0.108 mg/Kg - dry 0.108 0.3671,4-Dichlorobenzene 1 11/27/23 18:05 V40513AMP
<0.163 mg/Kg - dry 0.163 0.7353,3'-Dichlorobenzidine 1 11/27/23 18:05 V40513AMP
<0.106 mg/Kg - dry 0.106 0.7352,4-Dichlorophenol 1 11/27/23 18:05 V40513AMP
<0.200 mg/Kg - dry 0.200 0.735Diethyl phthalate 1 11/27/23 18:05 V40513AMP
<0.193 mg/Kg - dry 0.193 0.735Dimethyl phthalate 1 11/27/23 18:05 V40513AMP
<0.120 mg/Kg - dry 0.120 0.3672,4-Dimethylphenol 1 11/27/23 18:05 V40513AMP
0.136 J mg/Kg - dry 0.119 0.735Di-n-butyl phthalate 1 11/27/23 18:05 V40513AMP
<0.267 mg/Kg - dry 0.267 1.674,6-Dinitro-2-methylphenol 1 11/27/23 18:05 V40513AMP
<0.579 mg/Kg - dry 0.579 1.672,4-Dinitrophenol 1 11/27/23 18:05 V40513AMP
<0.107 mg/Kg - dry 0.107 0.7352,4-Dinitrotoluene 1 11/27/23 18:05 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 38 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-2
89891 Matrix:
11/20/2023 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.120 mg/Kg - dry 0.120 0.7352,6-Dinitrotoluene 1 11/27/23 18:05 V40513AMP
<0.159 mg/Kg - dry 0.159 0.367Di-n-Octyl Phthalate 1 11/27/23 18:05 V40513AMP
<0.137 mg/Kg - dry 0.137 0.735Fluoranthene 1 11/27/23 18:05 V40513AMP
<0.142 mg/Kg - dry 0.142 0.735Fluorene 1 11/27/23 18:05 V40513AMP
<0.118 mg/Kg - dry 0.118 0.735Hexachlorobenzene 1 11/27/23 18:05 V40513AMP
<0.108 mg/Kg - dry 0.108 0.735Hexachlorobutadiene 1 11/27/23 18:05 V40513AMP
<0.175 mg/Kg - dry 0.175 0.735Hexachlorocyclopentadiene 1 11/27/23 18:05 V40513AMP
<0.088 mg/Kg - dry 0.088 0.735Hexachloroethane 1 11/27/23 18:05 V40513AMP
<0.199 mg/Kg - dry 0.199 0.735Indeno(1,2,3-cd)pyrene 1 11/27/23 18:05 V40513AMP
<0.212 mg/Kg - dry 0.212 0.735Isophorone 1 11/27/23 18:05 V40513AMP
<0.118 mg/Kg - dry 0.118 0.7351-Methylnaphthalene 1 11/27/23 18:05 V40513AMP
<0.111 mg/Kg - dry 0.111 0.7352-Methylnaphthalene 1 11/27/23 18:05 V40513AMP
<0.108 mg/Kg - dry 0.108 0.7352-Methylphenol 1 11/27/23 18:05 V40513AMP
<0.094 mg/Kg - dry 0.094 0.7353&4 Methylphenol 1 11/27/23 18:05 V40513AMP
<0.160 mg/Kg - dry 0.160 0.735Naphthalene 1 11/27/23 18:05 V40513AMP
<0.107 mg/Kg - dry 0.107 0.7352-Nitroaniline 1 11/27/23 18:05 V40513AMP
<0.133 mg/Kg - dry 0.133 0.7353-Nitroaniline 1 11/27/23 18:05 V40513AMP
<0.104 mg/Kg - dry 0.104 0.3674-Nitroaniline 1 11/27/23 18:05 V40513AMP
<0.129 mg/Kg - dry 0.129 0.367Nitrobenzene 1 11/27/23 18:05 V40513AMP
<0.098 mg/Kg - dry 0.098 0.7352-Nitrophenol 1 11/27/23 18:05 V40513AMP
<0.130 mg/Kg - dry 0.130 0.7354-Nitrophenol 1 11/27/23 18:05 V40513AMP
<0.293 mg/Kg - dry 0.293 0.735N-Nitrosodimethylamine 1 11/27/23 18:05 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 39 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:WL-2
89891 Matrix:
11/20/2023 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.201 mg/Kg - dry 0.201 0.735N-Nitrosodiphenylamine 1 11/27/23 18:05 V40513AMP
<0.131 mg/Kg - dry 0.131 0.735N-Nitroso-di-n-propylamine 1 11/27/23 18:05 V40513AMP
<0.386 mg/Kg - dry 0.386 1.11Pentachlorophenol 1 11/27/23 18:05 V40513AMP
<0.231 mg/Kg - dry 0.231 0.735Phenanthrene 1 11/27/23 18:05 V40513AMP
<0.124 mg/Kg - dry 0.124 0.735Phenol 1 11/27/23 18:05 V40513AMP
<0.149 mg/Kg - dry 0.149 0.735Pyrene 1 11/27/23 18:05 V40513AMP
<0.088 mg/Kg - dry 0.088 0.367Pyridine 1 11/27/23 18:05 V40513AMP
<0.119 mg/Kg - dry 0.119 0.7351,2,4-Trichlorobenzene 1 11/27/23 18:05 V40513AMP
<0.107 mg/Kg - dry 0.107 0.7352,4,5-Trichlorophenol 1 11/27/23 18:05 V40513AMP
<0.107 mg/Kg - dry 0.107 0.7352,4,6-Trichlorophenol 1 11/27/23 18:05 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 40 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-1 (0-2)
89892 Matrix:
11/20/2023 12:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.8 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
0.311 mg/Kg - dry 0.169 0.240Chromium, Hexavalent 1 12/06/23 13:27 SW-7199SWB
0.458 mg/Kg - dry 0.103 0.300Arsenic 5 12/09/23 15:29 6020BBKN
82.7 mg/Kg - dry 0.051 0.300Barium 5 12/09/23 15:29 6020BBKN
<0.0312 mg/Kg - dry 0.0312 0.300Cadmium 5 12/09/23 15:29 6020BBKN
48.0 mg/Kg - dry 0.139 0.300Chromium 5 12/12/23 00:24 6020BJTR
4.21 mg/Kg - dry 0.0372 0.300Lead 5 12/09/23 15:29 6020BBKN
0.0179 J mg/Kg - dry 0.0144 0.0361Mercury (Total)1 11/30/23 16:43 7471BJKC
0.305 mg/Kg - dry 0.123 0.300Selenium 5 12/09/23 15:29 6020BJTR
0.0097 J mg/Kg - dry 0.0081 0.300Silver 5 12/09/23 15:29 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 41 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-1 (0-2)
89892 Matrix:
11/20/2023 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0022 mg/Kg - dry 0.0022 0.0060Aldrin 1 11/30/23 18:11 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0060alpha-BHC 1 11/30/23 18:11 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0060beta-BHC 1 11/30/23 18:11 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.0060delta-BHC 1 11/30/23 18:11 V40768TJW
<0.0211 mg/Kg - dry 0.0211 0.0600Chlordane 1 11/30/23 18:11 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0060alpha-Chlordane 1 11/30/23 18:11 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0060gamma-Chlordane 1 11/30/23 18:11 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.00604,4'-DDD 1 11/30/23 18:11 V40768TJW
<0.0024 mg/Kg - dry 0.0024 0.00604,4'-DDE 1 11/30/23 18:11 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.00604,4'-DDT 1 11/30/23 18:11 V40768TJW
<0.0025 mg/Kg - dry 0.0025 0.0060Dieldrin 1 11/30/23 18:11 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0060Endosulfan I 1 11/30/23 18:11 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0060Endosulfan II 1 11/30/23 18:11 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0060Endosulfan Sulfate 1 11/30/23 18:11 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0060Endrin 1 11/30/23 18:11 V40768TJW
<0.0025 mg/Kg - dry 0.0025 0.0060Endrin Aldehyde 1 11/30/23 18:11 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0060Endrin Ketone 1 11/30/23 18:11 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.0060gamma-BHC 1 11/30/23 18:11 V40768TJW
<0.0016 mg/Kg - dry 0.0016 0.0060Heptachlor 1 11/30/23 18:11 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0060Heptachlor Epoxide 1 11/30/23 18:11 V40768TJW
<0.0031 mg/Kg - dry 0.0031 0.0060Methoxychlor 1 11/30/23 18:11 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 42 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-1 (0-2)
89892 Matrix:
11/20/2023 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0122 mg/Kg - dry 0.0122 0.0600 1 11/30/23 18:11 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.066 mg/Kg - dry 0.002 0.024Acetone 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 11/22/23 15:43 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 11/22/23 15:43 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/22/23 15:43 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/22/23 15:43 V40555TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/22/23 15:43 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/22/23 15:43 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/22/23 15:43 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/22/23 15:43 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 43 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-1 (0-2)
89892 Matrix:
11/20/2023 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/22/23 15:43 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/22/23 15:43 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/22/23 15:43 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/22/23 15:43 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 11/22/23 15:43 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 11/22/23 15:43 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/22/23 15:43 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/22/23 15:43 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/22/23 15:43 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/22/23 15:43 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 11/22/23 15:43 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/22/23 15:43 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.006cis-1,2-Dichloroethene 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/22/23 15:43 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 11/22/23 15:43 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/22/23 15:43 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 44 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-1 (0-2)
89892 Matrix:
11/20/2023 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 11/22/23 15:43 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 11/22/23 15:43 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/22/23 15:43 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.060Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 15:43 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.012Hexachlorobutadiene 1 11/22/23 15:43 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/22/23 15:43 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0242-Hexanone 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/22/23 15:43 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 11/22/23 15:43 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 11/22/23 15:43 V40555TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Propylbenzene 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/22/23 15:43 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006 1 11/22/23 15:43 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.006 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,3-Trichlorobenzene 1 11/22/23 15:43 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 45 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-1 (0-2)
89892 Matrix:
11/20/2023 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006 1 11/22/23 15:43 V40555TBL
<0.002 mg/Kg - dry 0.002 0.012 1 11/22/23 15:43 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3,5-Trimethylbenzene 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/22/23 15:43 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/22/23 15:43 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/22/23 15:43 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.139 mg/Kg - dry 0.139 0.793Acenaphthene 1 11/22/23 23:20 V40513AMP
<0.126 mg/Kg - dry 0.126 0.793Acenaphthylene 1 11/22/23 23:20 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 46 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-1 (0-2)
89892 Matrix:
11/20/2023 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.182 mg/Kg - dry 0.182 0.793Aniline 1 11/22/23 23:20 V40513AMP
<0.171 mg/Kg - dry 0.171 0.793Anthracene 1 11/22/23 23:20 V40513AMP
<0.167 mg/Kg - dry 0.167 0.793Benzo(a)anthracene 1 11/22/23 23:20 V40513AMP
<0.176 mg/Kg - dry 0.176 0.793Benzo(a)pyrene 1 11/22/23 23:20 V40513AMP
<0.175 mg/Kg - dry 0.175 0.793Benzo(b)fluoranthene 1 11/22/23 23:20 V40513AMP
<0.163 mg/Kg - dry 0.163 0.793Benzo(g,h,i)perylene 1 11/22/23 23:20 V40513AMP
<0.164 mg/Kg - dry 0.164 0.793Benzo(k)fluoranthene 1 11/22/23 23:20 V40513AMP
<0.697 M mg/Kg - dry 0.697 2.40Benzoic Acid 1 11/22/23 23:20 V40513AMP
<0.126 mg/Kg - dry 0.126 0.793Benzyl alcohol 1 11/22/23 23:20 V40513AMP
<0.141 mg/Kg - dry 0.141 0.793Bis(2-Chloroethoxy)methane 1 11/22/23 23:20 V40513AMP
<0.128 mg/Kg - dry 0.128 0.793Bis(2-Chloroethyl)ether 1 11/22/23 23:20 V40513AMP
<0.163 mg/Kg - dry 0.163 0.396Bis(2-Chloroisopropyl)ether 1 11/22/23 23:20 V40513AMP
<0.144 mg/Kg - dry 0.144 0.793Bis(2-ethylhexyl)phthalate 1 11/22/23 23:20 V40513AMP
<0.131 mg/Kg - dry 0.131 0.7934-Bromophenyl phenyl ether 1 11/22/23 23:20 V40513AMP
<0.135 mg/Kg - dry 0.135 0.396Butyl benzyl phthalate 1 11/22/23 23:20 V40513AMP
<0.111 mg/Kg - dry 0.111 0.7934-Chloro-3-methylphenol 1 11/22/23 23:20 V40513AMP
<0.134 mg/Kg - dry 0.134 0.3964-Chloroaniline 1 11/22/23 23:20 V40513AMP
<0.139 mg/Kg - dry 0.139 0.7932-Chloronaphthalene 1 11/22/23 23:20 V40513AMP
<0.118 mg/Kg - dry 0.118 0.7932-Chlorophenol 1 11/22/23 23:20 V40513AMP
<0.151 mg/Kg - dry 0.151 1.204-Chlorophenyl phenyl ether 1 11/22/23 23:20 V40513AMP
<0.170 mg/Kg - dry 0.170 0.793Chrysene 1 11/22/23 23:20 V40513AMP
<0.276 mg/Kg - dry 0.276 0.793Dibenz(a,h)anthracene 1 11/22/23 23:20 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 47 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-1 (0-2)
89892 Matrix:
11/20/2023 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.143 mg/Kg - dry 0.143 0.793Dibenzofuran 1 11/22/23 23:20 V40513AMP
<0.113 mg/Kg - dry 0.113 0.7931,2-Dichlorobenzene 1 11/22/23 23:20 V40513AMP
<0.116 mg/Kg - dry 0.116 0.7931,3-Dichlorobenzene 1 11/22/23 23:20 V40513AMP
<0.117 mg/Kg - dry 0.117 0.3961,4-Dichlorobenzene 1 11/22/23 23:20 V40513AMP
<0.176 mg/Kg - dry 0.176 0.7933,3'-Dichlorobenzidine 1 11/22/23 23:20 V40513AMP
<0.115 mg/Kg - dry 0.115 0.7932,4-Dichlorophenol 1 11/22/23 23:20 V40513AMP
<0.216 mg/Kg - dry 0.216 0.793Diethyl phthalate 1 11/22/23 23:20 V40513AMP
<0.209 mg/Kg - dry 0.209 0.793Dimethyl phthalate 1 11/22/23 23:20 V40513AMP
<0.129 mg/Kg - dry 0.129 0.3962,4-Dimethylphenol 1 11/22/23 23:20 V40513AMP
<0.128 mg/Kg - dry 0.128 0.793Di-n-butyl phthalate 1 11/22/23 23:20 V40513AMP
<0.288 mg/Kg - dry 0.288 1.804,6-Dinitro-2-methylphenol 1 11/22/23 23:20 V40513AMP
<0.625 mg/Kg - dry 0.625 1.802,4-Dinitrophenol 1 11/22/23 23:20 V40513AMP
<0.116 mg/Kg - dry 0.116 0.7932,4-Dinitrotoluene 1 11/22/23 23:20 V40513AMP
<0.129 mg/Kg - dry 0.129 0.7932,6-Dinitrotoluene 1 11/22/23 23:20 V40513AMP
<0.171 mg/Kg - dry 0.171 0.396Di-n-Octyl Phthalate 1 11/22/23 23:20 V40513AMP
<0.147 mg/Kg - dry 0.147 0.793Fluoranthene 1 11/22/23 23:20 V40513AMP
<0.153 mg/Kg - dry 0.153 0.793Fluorene 1 11/22/23 23:20 V40513AMP
<0.127 mg/Kg - dry 0.127 0.793Hexachlorobenzene 1 11/22/23 23:20 V40513AMP
<0.117 mg/Kg - dry 0.117 0.793Hexachlorobutadiene 1 11/22/23 23:20 V40513AMP
<0.188 mg/Kg - dry 0.188 0.793Hexachlorocyclopentadiene 1 11/22/23 23:20 V40513AMP
<0.095 mg/Kg - dry 0.095 0.793Hexachloroethane 1 11/22/23 23:20 V40513AMP
<0.215 mg/Kg - dry 0.215 0.793Indeno(1,2,3-cd)pyrene 1 11/22/23 23:20 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 48 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-1 (0-2)
89892 Matrix:
11/20/2023 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.229 mg/Kg - dry 0.229 0.793Isophorone 1 11/22/23 23:20 V40513AMP
<0.127 mg/Kg - dry 0.127 0.7931-Methylnaphthalene 1 11/22/23 23:20 V40513AMP
<0.120 mg/Kg - dry 0.120 0.7932-Methylnaphthalene 1 11/22/23 23:20 V40513AMP
<0.116 mg/Kg - dry 0.116 0.7932-Methylphenol 1 11/22/23 23:20 V40513AMP
<0.102 mg/Kg - dry 0.102 0.7933&4 Methylphenol 1 11/22/23 23:20 V40513AMP
<0.173 mg/Kg - dry 0.173 0.793Naphthalene 1 11/22/23 23:20 V40513AMP
<0.116 mg/Kg - dry 0.116 0.7932-Nitroaniline 1 11/22/23 23:20 V40513AMP
<0.144 mg/Kg - dry 0.144 0.7933-Nitroaniline 1 11/22/23 23:20 V40513AMP
<0.112 mg/Kg - dry 0.112 0.3964-Nitroaniline 1 11/22/23 23:20 V40513AMP
<0.139 mg/Kg - dry 0.139 0.396Nitrobenzene 1 11/22/23 23:20 V40513AMP
<0.106 mg/Kg - dry 0.106 0.7932-Nitrophenol 1 11/22/23 23:20 V40513AMP
<0.140 mg/Kg - dry 0.140 0.7934-Nitrophenol 1 11/22/23 23:20 V40513AMP
<0.316 mg/Kg - dry 0.316 0.793N-Nitrosodimethylamine 1 11/22/23 23:20 V40513AMP
<0.217 mg/Kg - dry 0.217 0.793N-Nitrosodiphenylamine 1 11/22/23 23:20 V40513AMP
<0.141 mg/Kg - dry 0.141 0.793N-Nitroso-di-n-propylamine 1 11/22/23 23:20 V40513AMP
<0.417 mg/Kg - dry 0.417 1.20Pentachlorophenol 1 11/22/23 23:20 V40513AMP
<0.250 mg/Kg - dry 0.250 0.793Phenanthrene 1 11/22/23 23:20 V40513AMP
<0.134 mg/Kg - dry 0.134 0.793Phenol 1 11/22/23 23:20 V40513AMP
<0.161 mg/Kg - dry 0.161 0.793Pyrene 1 11/22/23 23:20 V40513AMP
<0.095 mg/Kg - dry 0.095 0.396Pyridine 1 11/22/23 23:20 V40513AMP
<0.128 mg/Kg - dry 0.128 0.7931,2,4-Trichlorobenzene 1 11/22/23 23:20 V40513AMP
<0.115 mg/Kg - dry 0.115 0.7932,4,5-Trichlorophenol 1 11/22/23 23:20 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 49 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-1 (0-2)
89892 Matrix:
11/20/2023 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.116 mg/Kg - dry 0.116 0.7932,4,6-Trichlorophenol 1 11/22/23 23:20 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 50 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-2 (0-2)
89893 Matrix:
11/20/2023 12:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.6 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
0.428 mg/Kg - dry 0.211 0.301Chromium, Hexavalent 1 12/06/23 13:38 SW-7199SWB
0.877 mg/Kg - dry 0.108 0.315Arsenic 5 12/09/23 15:33 6020BBKN
97.4 mg/Kg - dry 0.053 0.314Barium 5 12/09/23 15:33 6020BBKN
<0.0327 mg/Kg - dry 0.0327 0.315Cadmium 5 12/09/23 15:33 6020BBKN
132 mg/Kg - dry 0.146 0.314Chromium 5 12/12/23 00:28 6020BJTR
4.01 mg/Kg - dry 0.0390 0.315Lead 5 12/09/23 15:33 6020BBKN
0.0181 J mg/Kg - dry 0.0151 0.0378Mercury (Total)1 11/30/23 16:45 7471BJKC
0.318 mg/Kg - dry 0.129 0.314Selenium 5 12/09/23 15:33 6020BJTR
0.0128 J mg/Kg - dry 0.0084 0.315Silver 5 12/09/23 15:33 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 51 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-2 (0-2)
89893 Matrix:
11/20/2023 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0023 mg/Kg - dry 0.0023 0.0062Aldrin 1 11/30/23 18:25 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0062alpha-BHC 1 11/30/23 18:25 V40768TJW
<0.0025 mg/Kg - dry 0.0025 0.0062beta-BHC 1 11/30/23 18:25 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.0062delta-BHC 1 11/30/23 18:25 V40768TJW
<0.0221 mg/Kg - dry 0.0221 0.0629Chlordane 1 11/30/23 18:25 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0062alpha-Chlordane 1 11/30/23 18:25 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0062gamma-Chlordane 1 11/30/23 18:25 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.00624,4'-DDD 1 11/30/23 18:25 V40768TJW
<0.0025 mg/Kg - dry 0.0025 0.00624,4'-DDE 1 11/30/23 18:25 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.00624,4'-DDT 1 11/30/23 18:25 V40768TJW
<0.0026 mg/Kg - dry 0.0026 0.0062Dieldrin 1 11/30/23 18:25 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0062Endosulfan I 1 11/30/23 18:25 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0062Endosulfan II 1 11/30/23 18:25 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0062Endosulfan Sulfate 1 11/30/23 18:25 V40768TJW
<0.0024 mg/Kg - dry 0.0024 0.0062Endrin 1 11/30/23 18:25 V40768TJW
<0.0026 mg/Kg - dry 0.0026 0.0062Endrin Aldehyde 1 11/30/23 18:25 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0062Endrin Ketone 1 11/30/23 18:25 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.0062gamma-BHC 1 11/30/23 18:25 V40768TJW
<0.0017 mg/Kg - dry 0.0017 0.0062Heptachlor 1 11/30/23 18:25 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0062Heptachlor Epoxide 1 11/30/23 18:25 V40768TJW
<0.0033 mg/Kg - dry 0.0033 0.0062Methoxychlor 1 11/30/23 18:25 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 52 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-2 (0-2)
89893 Matrix:
11/20/2023 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0128 mg/Kg - dry 0.0128 0.0629 1 11/30/23 18:25 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.048 mg/Kg - dry 0.003 0.025Acetone 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 11/22/23 16:10 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 11/22/23 16:10 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/22/23 16:10 V40555TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/22/23 16:10 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/22/23 16:10 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/22/23 16:10 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/22/23 16:10 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 53 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-2 (0-2)
89893 Matrix:
11/20/2023 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/22/23 16:10 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/22/23 16:10 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/22/23 16:10 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 11/22/23 16:10 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 11/22/23 16:10 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/22/23 16:10 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/22/23 16:10 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/22/23 16:10 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 11/22/23 16:10 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/22/23 16:10 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/22/23 16:10 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/22/23 16:10 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 54 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-2 (0-2)
89893 Matrix:
11/20/2023 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 11/22/23 16:10 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/22/23 16:10 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 16:10 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 11/22/23 16:10 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/22/23 16:10 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/22/23 16:10 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 11/22/23 16:10 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/22/23 16:10 V40555TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 11/22/23 16:10 V40555TBL
0.002 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 11/22/23 16:10 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/22/23 16:10 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006 1 11/22/23 16:10 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.006 1 11/22/23 16:10 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 11/22/23 16:10 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 55 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-2 (0-2)
89893 Matrix:
11/20/2023 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006 1 11/22/23 16:10 V40555TBL
<0.002 mg/Kg - dry 0.002 0.012 1 11/22/23 16:10 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/22/23 16:10 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/22/23 16:10 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/22/23 16:10 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/22/23 16:10 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.146 mg/Kg - dry 0.146 0.831Acenaphthene 1 11/23/23 00:28 V40513AMP
<0.132 mg/Kg - dry 0.132 0.831Acenaphthylene 1 11/23/23 00:28 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 56 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-2 (0-2)
89893 Matrix:
11/20/2023 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.191 mg/Kg - dry 0.191 0.831Aniline 1 11/23/23 00:28 V40513AMP
<0.180 mg/Kg - dry 0.180 0.831Anthracene 1 11/23/23 00:28 V40513AMP
<0.175 mg/Kg - dry 0.175 0.831Benzo(a)anthracene 1 11/23/23 00:28 V40513AMP
<0.185 mg/Kg - dry 0.185 0.831Benzo(a)pyrene 1 11/23/23 00:28 V40513AMP
<0.183 mg/Kg - dry 0.183 0.831Benzo(b)fluoranthene 1 11/23/23 00:28 V40513AMP
<0.171 mg/Kg - dry 0.171 0.831Benzo(g,h,i)perylene 1 11/23/23 00:28 V40513AMP
<0.172 mg/Kg - dry 0.172 0.831Benzo(k)fluoranthene 1 11/23/23 00:28 V40513AMP
<0.730 M mg/Kg - dry 0.730 2.52Benzoic Acid 1 11/23/23 00:28 V40513AMP
<0.132 mg/Kg - dry 0.132 0.831Benzyl alcohol 1 11/23/23 00:28 V40513AMP
<0.148 mg/Kg - dry 0.148 0.831Bis(2-Chloroethoxy)methane 1 11/23/23 00:28 V40513AMP
<0.134 mg/Kg - dry 0.134 0.831Bis(2-Chloroethyl)ether 1 11/23/23 00:28 V40513AMP
<0.171 mg/Kg - dry 0.171 0.415Bis(2-Chloroisopropyl)ether 1 11/23/23 00:28 V40513AMP
<0.151 mg/Kg - dry 0.151 0.831Bis(2-ethylhexyl)phthalate 1 11/23/23 00:28 V40513AMP
<0.137 mg/Kg - dry 0.137 0.8314-Bromophenyl phenyl ether 1 11/23/23 00:28 V40513AMP
<0.142 mg/Kg - dry 0.142 0.415Butyl benzyl phthalate 1 11/23/23 00:28 V40513AMP
<0.116 mg/Kg - dry 0.116 0.8314-Chloro-3-methylphenol 1 11/23/23 00:28 V40513AMP
<0.141 mg/Kg - dry 0.141 0.4154-Chloroaniline 1 11/23/23 00:28 V40513AMP
<0.146 mg/Kg - dry 0.146 0.8312-Chloronaphthalene 1 11/23/23 00:28 V40513AMP
<0.123 mg/Kg - dry 0.123 0.8312-Chlorophenol 1 11/23/23 00:28 V40513AMP
<0.158 mg/Kg - dry 0.158 1.264-Chlorophenyl phenyl ether 1 11/23/23 00:28 V40513AMP
<0.178 mg/Kg - dry 0.178 0.831Chrysene 1 11/23/23 00:28 V40513AMP
<0.289 mg/Kg - dry 0.289 0.831Dibenz(a,h)anthracene 1 11/23/23 00:28 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 57 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-2 (0-2)
89893 Matrix:
11/20/2023 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.149 mg/Kg - dry 0.149 0.831Dibenzofuran 1 11/23/23 00:28 V40513AMP
<0.118 mg/Kg - dry 0.118 0.8311,2-Dichlorobenzene 1 11/23/23 00:28 V40513AMP
<0.122 mg/Kg - dry 0.122 0.8311,3-Dichlorobenzene 1 11/23/23 00:28 V40513AMP
<0.122 mg/Kg - dry 0.122 0.4151,4-Dichlorobenzene 1 11/23/23 00:28 V40513AMP
<0.185 mg/Kg - dry 0.185 0.8313,3'-Dichlorobenzidine 1 11/23/23 00:28 V40513AMP
<0.120 mg/Kg - dry 0.120 0.8312,4-Dichlorophenol 1 11/23/23 00:28 V40513AMP
<0.226 mg/Kg - dry 0.226 0.831Diethyl phthalate 1 11/23/23 00:28 V40513AMP
<0.219 mg/Kg - dry 0.219 0.831Dimethyl phthalate 1 11/23/23 00:28 V40513AMP
<0.136 mg/Kg - dry 0.136 0.4152,4-Dimethylphenol 1 11/23/23 00:28 V40513AMP
<0.134 mg/Kg - dry 0.134 0.831Di-n-butyl phthalate 1 11/23/23 00:28 V40513AMP
<0.302 mg/Kg - dry 0.302 1.894,6-Dinitro-2-methylphenol 1 11/23/23 00:28 V40513AMP
<0.654 mg/Kg - dry 0.654 1.892,4-Dinitrophenol 1 11/23/23 00:28 V40513AMP
<0.121 mg/Kg - dry 0.121 0.8312,4-Dinitrotoluene 1 11/23/23 00:28 V40513AMP
<0.136 mg/Kg - dry 0.136 0.8312,6-Dinitrotoluene 1 11/23/23 00:28 V40513AMP
<0.180 mg/Kg - dry 0.180 0.415Di-n-Octyl Phthalate 1 11/23/23 00:28 V40513AMP
<0.154 mg/Kg - dry 0.154 0.831Fluoranthene 1 11/23/23 00:28 V40513AMP
<0.161 mg/Kg - dry 0.161 0.831Fluorene 1 11/23/23 00:28 V40513AMP
<0.133 mg/Kg - dry 0.133 0.831Hexachlorobenzene 1 11/23/23 00:28 V40513AMP
<0.122 mg/Kg - dry 0.122 0.831Hexachlorobutadiene 1 11/23/23 00:28 V40513AMP
<0.197 mg/Kg - dry 0.197 0.831Hexachlorocyclopentadiene 1 11/23/23 00:28 V40513AMP
<0.099 mg/Kg - dry 0.099 0.831Hexachloroethane 1 11/23/23 00:28 V40513AMP
<0.225 mg/Kg - dry 0.225 0.831Indeno(1,2,3-cd)pyrene 1 11/23/23 00:28 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 58 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-2 (0-2)
89893 Matrix:
11/20/2023 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.240 mg/Kg - dry 0.240 0.831Isophorone 1 11/23/23 00:28 V40513AMP
<0.133 mg/Kg - dry 0.133 0.8311-Methylnaphthalene 1 11/23/23 00:28 V40513AMP
<0.125 mg/Kg - dry 0.125 0.8312-Methylnaphthalene 1 11/23/23 00:28 V40513AMP
<0.122 mg/Kg - dry 0.122 0.8312-Methylphenol 1 11/23/23 00:28 V40513AMP
<0.106 mg/Kg - dry 0.106 0.8313&4 Methylphenol 1 11/23/23 00:28 V40513AMP
<0.181 mg/Kg - dry 0.181 0.831Naphthalene 1 11/23/23 00:28 V40513AMP
<0.121 mg/Kg - dry 0.121 0.8312-Nitroaniline 1 11/23/23 00:28 V40513AMP
<0.151 mg/Kg - dry 0.151 0.8313-Nitroaniline 1 11/23/23 00:28 V40513AMP
<0.117 mg/Kg - dry 0.117 0.4154-Nitroaniline 1 11/23/23 00:28 V40513AMP
<0.146 mg/Kg - dry 0.146 0.415Nitrobenzene 1 11/23/23 00:28 V40513AMP
<0.111 mg/Kg - dry 0.111 0.8312-Nitrophenol 1 11/23/23 00:28 V40513AMP
<0.147 mg/Kg - dry 0.147 0.8314-Nitrophenol 1 11/23/23 00:28 V40513AMP
<0.331 mg/Kg - dry 0.331 0.831N-Nitrosodimethylamine 1 11/23/23 00:28 V40513AMP
<0.227 mg/Kg - dry 0.227 0.831N-Nitrosodiphenylamine 1 11/23/23 00:28 V40513AMP
<0.148 mg/Kg - dry 0.148 0.831N-Nitroso-di-n-propylamine 1 11/23/23 00:28 V40513AMP
<0.437 mg/Kg - dry 0.437 1.26Pentachlorophenol 1 11/23/23 00:28 V40513AMP
<0.261 mg/Kg - dry 0.261 0.831Phenanthrene 1 11/23/23 00:28 V40513AMP
<0.141 mg/Kg - dry 0.141 0.831Phenol 1 11/23/23 00:28 V40513AMP
<0.168 mg/Kg - dry 0.168 0.831Pyrene 1 11/23/23 00:28 V40513AMP
<0.099 mg/Kg - dry 0.099 0.415Pyridine 1 11/23/23 00:28 V40513AMP
<0.134 mg/Kg - dry 0.134 0.8311,2,4-Trichlorobenzene 1 11/23/23 00:28 V40513AMP
<0.121 mg/Kg - dry 0.121 0.8312,4,5-Trichlorophenol 1 11/23/23 00:28 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 59 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-2 (0-2)
89893 Matrix:
11/20/2023 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.121 mg/Kg - dry 0.121 0.8312,4,6-Trichlorophenol 1 11/23/23 00:28 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 60 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-3 (0-2)
89894 Matrix:
11/20/2023 13:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.0 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
<0.163 mg/Kg - dry 0.163 0.232Chromium, Hexavalent 1 12/06/23 14:11 SW-7199SWB
1.16 mg/Kg - dry 0.0994 0.291Arsenic 5 12/09/23 15:37 6020BBKN
57.7 mg/Kg - dry 0.049 0.290Barium 5 12/09/23 15:37 6020BBKN
<0.0302 mg/Kg - dry 0.0302 0.291Cadmium 5 12/09/23 15:37 6020BBKN
22.7 mg/Kg - dry 0.134 0.290Chromium 5 12/12/23 00:32 6020BJTR
7.83 mg/Kg - dry 0.0360 0.291Lead 5 12/09/23 15:37 6020BBKN
<0.0140 mg/Kg - dry 0.0140 0.0349Mercury (Total)1 11/30/23 16:48 7471BJKC
0.269 J mg/Kg - dry 0.119 0.290Selenium 5 12/09/23 15:37 6020BJTR
0.0130 J mg/Kg - dry 0.0078 0.291Silver 5 12/09/23 15:37 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 61 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-3 (0-2)
89894 Matrix:
11/20/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0021 mg/Kg - dry 0.0021 0.0058Aldrin 1 11/30/23 18:38 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0058alpha-BHC 1 11/30/23 18:38 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0058beta-BHC 1 11/30/23 18:38 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0058delta-BHC 1 11/30/23 18:38 V40768TJW
<0.0204 mg/Kg - dry 0.0204 0.0581Chlordane 1 11/30/23 18:38 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0058alpha-Chlordane 1 11/30/23 18:38 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0058gamma-Chlordane 1 11/30/23 18:38 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.00584,4'-DDD 1 11/30/23 18:38 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.00584,4'-DDE 1 11/30/23 18:38 V40768TJW
<0.0017 mg/Kg - dry 0.0017 0.00584,4'-DDT 1 11/30/23 18:38 V40768TJW
<0.0024 mg/Kg - dry 0.0024 0.0058Dieldrin 1 11/30/23 18:38 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0058Endosulfan I 1 11/30/23 18:38 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0058Endosulfan II 1 11/30/23 18:38 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0058Endosulfan Sulfate 1 11/30/23 18:38 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0058Endrin 1 11/30/23 18:38 V40768TJW
<0.0024 mg/Kg - dry 0.0024 0.0058Endrin Aldehyde 1 11/30/23 18:38 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0058Endrin Ketone 1 11/30/23 18:38 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0058gamma-BHC 1 11/30/23 18:38 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.0058Heptachlor 1 11/30/23 18:38 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0058Heptachlor Epoxide 1 11/30/23 18:38 V40768TJW
<0.0030 mg/Kg - dry 0.0030 0.0058Methoxychlor 1 11/30/23 18:38 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 62 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-3 (0-2)
89894 Matrix:
11/20/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0118 mg/Kg - dry 0.0118 0.0581 1 11/30/23 18:38 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.056 mg/Kg - dry 0.002 0.023Acetone 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 11/22/23 16:37 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 11/22/23 16:37 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/22/23 16:37 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/22/23 16:37 V40555TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/22/23 16:37 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/22/23 16:37 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/22/23 16:37 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/22/23 16:37 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 63 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-3 (0-2)
89894 Matrix:
11/20/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/22/23 16:37 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/22/23 16:37 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 11/22/23 16:37 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/22/23 16:37 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/22/23 16:37 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 11/22/23 16:37 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 11/22/23 16:37 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/22/23 16:37 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/22/23 16:37 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/22/23 16:37 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/22/23 16:37 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/22/23 16:37 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/22/23 16:37 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/22/23 16:37 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 64 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-3 (0-2)
89894 Matrix:
11/20/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/22/23 16:37 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/22/23 16:37 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/22/23 16:37 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 16:37 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/22/23 16:37 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/22/23 16:37 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 11/22/23 16:37 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/22/23 16:37 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 11/22/23 16:37 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/22/23 16:37 V40555TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/22/23 16:37 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/22/23 16:37 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/22/23 16:37 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 65 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-3 (0-2)
89894 Matrix:
11/20/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/22/23 16:37 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/22/23 16:37 V40555TBL
<0.002 mg/Kg - dry 0.002 0.011 1 11/22/23 16:37 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/22/23 16:37 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/22/23 16:37 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/22/23 16:37 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/22/23 16:37 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.134 mg/Kg - dry 0.134 0.767Acenaphthene 1 11/23/23 02:43 V40513AMP
<0.122 mg/Kg - dry 0.122 0.767Acenaphthylene 1 11/23/23 02:43 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 66 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-3 (0-2)
89894 Matrix:
11/20/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.176 mg/Kg - dry 0.176 0.767Aniline 1 11/23/23 02:43 V40513AMP
<0.166 mg/Kg - dry 0.166 0.767Anthracene 1 11/23/23 02:43 V40513AMP
<0.161 mg/Kg - dry 0.161 0.767Benzo(a)anthracene 1 11/23/23 02:43 V40513AMP
<0.170 mg/Kg - dry 0.170 0.767Benzo(a)pyrene 1 11/23/23 02:43 V40513AMP
<0.169 mg/Kg - dry 0.169 0.767Benzo(b)fluoranthene 1 11/23/23 02:43 V40513AMP
<0.158 mg/Kg - dry 0.158 0.767Benzo(g,h,i)perylene 1 11/23/23 02:43 V40513AMP
<0.159 mg/Kg - dry 0.159 0.767Benzo(k)fluoranthene 1 11/23/23 02:43 V40513AMP
<0.674 M mg/Kg - dry 0.674 2.33Benzoic Acid 1 11/23/23 02:43 V40513AMP
<0.122 mg/Kg - dry 0.122 0.767Benzyl alcohol 1 11/23/23 02:43 V40513AMP
<0.137 mg/Kg - dry 0.137 0.767Bis(2-Chloroethoxy)methane 1 11/23/23 02:43 V40513AMP
<0.124 mg/Kg - dry 0.124 0.767Bis(2-Chloroethyl)ether 1 11/23/23 02:43 V40513AMP
<0.158 mg/Kg - dry 0.158 0.383Bis(2-Chloroisopropyl)ether 1 11/23/23 02:43 V40513AMP
<0.139 mg/Kg - dry 0.139 0.767Bis(2-ethylhexyl)phthalate 1 11/23/23 02:43 V40513AMP
<0.126 mg/Kg - dry 0.126 0.7674-Bromophenyl phenyl ether 1 11/23/23 02:43 V40513AMP
<0.131 mg/Kg - dry 0.131 0.383Butyl benzyl phthalate 1 11/23/23 02:43 V40513AMP
<0.107 mg/Kg - dry 0.107 0.7674-Chloro-3-methylphenol 1 11/23/23 02:43 V40513AMP
<0.130 mg/Kg - dry 0.130 0.3834-Chloroaniline 1 11/23/23 02:43 V40513AMP
<0.134 mg/Kg - dry 0.134 0.7672-Chloronaphthalene 1 11/23/23 02:43 V40513AMP
<0.114 mg/Kg - dry 0.114 0.7672-Chlorophenol 1 11/23/23 02:43 V40513AMP
<0.146 mg/Kg - dry 0.146 1.164-Chlorophenyl phenyl ether 1 11/23/23 02:43 V40513AMP
<0.165 mg/Kg - dry 0.165 0.767Chrysene 1 11/23/23 02:43 V40513AMP
<0.267 mg/Kg - dry 0.267 0.767Dibenz(a,h)anthracene 1 11/23/23 02:43 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 67 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-3 (0-2)
89894 Matrix:
11/20/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.138 mg/Kg - dry 0.138 0.767Dibenzofuran 1 11/23/23 02:43 V40513AMP
<0.109 mg/Kg - dry 0.109 0.7671,2-Dichlorobenzene 1 11/23/23 02:43 V40513AMP
<0.113 mg/Kg - dry 0.113 0.7671,3-Dichlorobenzene 1 11/23/23 02:43 V40513AMP
<0.113 mg/Kg - dry 0.113 0.3831,4-Dichlorobenzene 1 11/23/23 02:43 V40513AMP
<0.170 mg/Kg - dry 0.170 0.7673,3'-Dichlorobenzidine 1 11/23/23 02:43 V40513AMP
<0.111 mg/Kg - dry 0.111 0.7672,4-Dichlorophenol 1 11/23/23 02:43 V40513AMP
<0.209 mg/Kg - dry 0.209 0.767Diethyl phthalate 1 11/23/23 02:43 V40513AMP
<0.202 mg/Kg - dry 0.202 0.767Dimethyl phthalate 1 11/23/23 02:43 V40513AMP
<0.125 mg/Kg - dry 0.125 0.3832,4-Dimethylphenol 1 11/23/23 02:43 V40513AMP
<0.124 mg/Kg - dry 0.124 0.767Di-n-butyl phthalate 1 11/23/23 02:43 V40513AMP
<0.279 mg/Kg - dry 0.279 1.744,6-Dinitro-2-methylphenol 1 11/23/23 02:43 V40513AMP
<0.604 mg/Kg - dry 0.604 1.742,4-Dinitrophenol 1 11/23/23 02:43 V40513AMP
<0.112 mg/Kg - dry 0.112 0.7672,4-Dinitrotoluene 1 11/23/23 02:43 V40513AMP
<0.125 mg/Kg - dry 0.125 0.7672,6-Dinitrotoluene 1 11/23/23 02:43 V40513AMP
<0.166 mg/Kg - dry 0.166 0.383Di-n-Octyl Phthalate 1 11/23/23 02:43 V40513AMP
<0.143 mg/Kg - dry 0.143 0.767Fluoranthene 1 11/23/23 02:43 V40513AMP
<0.148 mg/Kg - dry 0.148 0.767Fluorene 1 11/23/23 02:43 V40513AMP
<0.123 mg/Kg - dry 0.123 0.767Hexachlorobenzene 1 11/23/23 02:43 V40513AMP
<0.113 mg/Kg - dry 0.113 0.767Hexachlorobutadiene 1 11/23/23 02:43 V40513AMP
<0.182 mg/Kg - dry 0.182 0.767Hexachlorocyclopentadiene 1 11/23/23 02:43 V40513AMP
<0.092 mg/Kg - dry 0.092 0.767Hexachloroethane 1 11/23/23 02:43 V40513AMP
<0.208 mg/Kg - dry 0.208 0.767Indeno(1,2,3-cd)pyrene 1 11/23/23 02:43 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 68 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-3 (0-2)
89894 Matrix:
11/20/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.222 mg/Kg - dry 0.222 0.767Isophorone 1 11/23/23 02:43 V40513AMP
<0.123 mg/Kg - dry 0.123 0.7671-Methylnaphthalene 1 11/23/23 02:43 V40513AMP
<0.116 mg/Kg - dry 0.116 0.7672-Methylnaphthalene 1 11/23/23 02:43 V40513AMP
<0.112 mg/Kg - dry 0.112 0.7672-Methylphenol 1 11/23/23 02:43 V40513AMP
<0.098 mg/Kg - dry 0.098 0.7673&4 Methylphenol 1 11/23/23 02:43 V40513AMP
<0.167 mg/Kg - dry 0.167 0.767Naphthalene 1 11/23/23 02:43 V40513AMP
<0.112 mg/Kg - dry 0.112 0.7672-Nitroaniline 1 11/23/23 02:43 V40513AMP
<0.139 mg/Kg - dry 0.139 0.7673-Nitroaniline 1 11/23/23 02:43 V40513AMP
<0.108 mg/Kg - dry 0.108 0.3834-Nitroaniline 1 11/23/23 02:43 V40513AMP
<0.134 mg/Kg - dry 0.134 0.383Nitrobenzene 1 11/23/23 02:43 V40513AMP
<0.103 mg/Kg - dry 0.103 0.7672-Nitrophenol 1 11/23/23 02:43 V40513AMP
<0.136 mg/Kg - dry 0.136 0.7674-Nitrophenol 1 11/23/23 02:43 V40513AMP
<0.305 mg/Kg - dry 0.305 0.767N-Nitrosodimethylamine 1 11/23/23 02:43 V40513AMP
<0.210 mg/Kg - dry 0.210 0.767N-Nitrosodiphenylamine 1 11/23/23 02:43 V40513AMP
<0.137 mg/Kg - dry 0.137 0.767N-Nitroso-di-n-propylamine 1 11/23/23 02:43 V40513AMP
<0.403 mg/Kg - dry 0.403 1.16Pentachlorophenol 1 11/23/23 02:43 V40513AMP
<0.241 mg/Kg - dry 0.241 0.767Phenanthrene 1 11/23/23 02:43 V40513AMP
<0.130 mg/Kg - dry 0.130 0.767Phenol 1 11/23/23 02:43 V40513AMP
<0.155 mg/Kg - dry 0.155 0.767Pyrene 1 11/23/23 02:43 V40513AMP
<0.092 mg/Kg - dry 0.092 0.383Pyridine 1 11/23/23 02:43 V40513AMP
<0.124 mg/Kg - dry 0.124 0.7671,2,4-Trichlorobenzene 1 11/23/23 02:43 V40513AMP
<0.111 mg/Kg - dry 0.111 0.7672,4,5-Trichlorophenol 1 11/23/23 02:43 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 69 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-3 (0-2)
89894 Matrix:
11/20/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.112 mg/Kg - dry 0.112 0.7672,4,6-Trichlorophenol 1 11/23/23 02:43 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 70 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-4 (0-2)
89895 Matrix:
11/20/2023 13:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.9 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
0.344 mg/Kg - dry 0.174 0.247Chromium, Hexavalent 1 12/06/23 14:22 SW-7199SWB
1.63 mg/Kg - dry 0.0981 0.287Arsenic 5 12/09/23 15:41 6020BBKN
49.8 mg/Kg - dry 0.049 0.287Barium 5 12/09/23 15:41 6020BBKN
<0.0298 mg/Kg - dry 0.0298 0.287Cadmium 5 12/09/23 15:41 6020BBKN
97.4 mg/Kg - dry 0.133 0.287Chromium 5 12/12/23 00:36 6020BJTR
7.53 mg/Kg - dry 0.0355 0.287Lead 5 12/09/23 15:41 6020BBKN
0.0550 mg/Kg - dry 0.0138 0.0344Mercury (Total)1 11/30/23 16:50 7471BJKC
0.402 mg/Kg - dry 0.118 0.287Selenium 5 12/09/23 15:41 6020BJTR
0.0177 J mg/Kg - dry 0.0077 0.287Silver 5 12/09/23 15:41 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 71 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-4 (0-2)
89895 Matrix:
11/20/2023 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0021 mg/Kg - dry 0.0021 0.0057Aldrin 1 11/30/23 18:51 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0057alpha-BHC 1 11/30/23 18:51 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0057beta-BHC 1 11/30/23 18:51 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0057delta-BHC 1 11/30/23 18:51 V40768TJW
<0.0202 mg/Kg - dry 0.0202 0.0574Chlordane 1 11/30/23 18:51 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0057alpha-Chlordane 1 11/30/23 18:51 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0057gamma-Chlordane 1 11/30/23 18:51 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.00574,4'-DDD 1 11/30/23 18:51 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.00574,4'-DDE 1 11/30/23 18:51 V40768TJW
<0.0017 mg/Kg - dry 0.0017 0.00574,4'-DDT 1 11/30/23 18:51 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0057Dieldrin 1 11/30/23 18:51 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0057Endosulfan I 1 11/30/23 18:51 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0057Endosulfan II 1 11/30/23 18:51 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0057Endosulfan Sulfate 1 11/30/23 18:51 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0057Endrin 1 11/30/23 18:51 V40768TJW
<0.0024 mg/Kg - dry 0.0024 0.0057Endrin Aldehyde 1 11/30/23 18:51 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0057Endrin Ketone 1 11/30/23 18:51 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0057gamma-BHC 1 11/30/23 18:51 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.0057Heptachlor 1 11/30/23 18:51 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0057Heptachlor Epoxide 1 11/30/23 18:51 V40768TJW
<0.0030 mg/Kg - dry 0.0030 0.0057Methoxychlor 1 11/30/23 18:51 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 72 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-4 (0-2)
89895 Matrix:
11/20/2023 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0117 mg/Kg - dry 0.0117 0.0574 1 11/30/23 18:51 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.070 mg/Kg - dry 0.002 0.022Acetone 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 11/22/23 17:04 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 11/22/23 17:04 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/22/23 17:04 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/22/23 17:04 V40555TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/22/23 17:04 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/22/23 17:04 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/22/23 17:04 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 73 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-4 (0-2)
89895 Matrix:
11/20/2023 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/22/23 17:04 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/22/23 17:04 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/22/23 17:04 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/22/23 17:04 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/22/23 17:04 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/22/23 17:04 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/22/23 17:04 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/22/23 17:04 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/22/23 17:04 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/22/23 17:04 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/22/23 17:04 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/22/23 17:04 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/22/23 17:04 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 74 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-4 (0-2)
89895 Matrix:
11/20/2023 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/22/23 17:04 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/22/23 17:04 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/22/23 17:04 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 17:04 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/22/23 17:04 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/22/23 17:04 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 11/22/23 17:04 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/22/23 17:04 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 11/22/23 17:04 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/22/23 17:04 V40555TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/22/23 17:04 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/22/23 17:04 V40555TBL
0.001 J mg/Kg - dry 0.0008 0.005 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/22/23 17:04 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 75 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-4 (0-2)
89895 Matrix:
11/20/2023 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/22/23 17:04 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/22/23 17:04 V40555TBL
<0.002 mg/Kg - dry 0.002 0.011 1 11/22/23 17:04 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/22/23 17:04 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/22/23 17:04 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/22/23 17:04 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/22/23 17:04 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.133 mg/Kg - dry 0.133 0.758Acenaphthene 1 11/27/23 15:27 V40513AMP
<0.120 mg/Kg - dry 0.120 0.758Acenaphthylene 1 11/27/23 15:27 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 76 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-4 (0-2)
89895 Matrix:
11/20/2023 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.174 mg/Kg - dry 0.174 0.758Aniline 1 11/27/23 15:27 V40513AMP
<0.164 mg/Kg - dry 0.164 0.758Anthracene 1 11/27/23 15:27 V40513AMP
<0.159 mg/Kg - dry 0.159 0.758Benzo(a)anthracene 1 11/27/23 15:27 V40513AMP
<0.168 mg/Kg - dry 0.168 0.758Benzo(a)pyrene 1 11/27/23 15:27 V40513AMP
<0.167 mg/Kg - dry 0.167 0.758Benzo(b)fluoranthene 1 11/27/23 15:27 V40513AMP
<0.156 mg/Kg - dry 0.156 0.758Benzo(g,h,i)perylene 1 11/27/23 15:27 V40513AMP
<0.157 mg/Kg - dry 0.157 0.758Benzo(k)fluoranthene 1 11/27/23 15:27 V40513AMP
0.955 JM mg/Kg - dry 0.665 2.30Benzoic Acid 1 11/27/23 15:27 V40513AMP
<0.120 mg/Kg - dry 0.120 0.758Benzyl alcohol 1 11/27/23 15:27 V40513AMP
<0.135 mg/Kg - dry 0.135 0.758Bis(2-Chloroethoxy)methane 1 11/27/23 15:27 V40513AMP
<0.122 mg/Kg - dry 0.122 0.758Bis(2-Chloroethyl)ether 1 11/27/23 15:27 V40513AMP
<0.156 mg/Kg - dry 0.156 0.380Bis(2-Chloroisopropyl)ether 1 11/27/23 15:27 V40513AMP
<0.137 mg/Kg - dry 0.137 0.758Bis(2-ethylhexyl)phthalate 1 11/27/23 15:27 V40513AMP
<0.125 mg/Kg - dry 0.125 0.7584-Bromophenyl phenyl ether 1 11/27/23 15:27 V40513AMP
<0.129 mg/Kg - dry 0.129 0.380Butyl benzyl phthalate 1 11/27/23 15:27 V40513AMP
<0.106 mg/Kg - dry 0.106 0.7584-Chloro-3-methylphenol 1 11/27/23 15:27 V40513AMP
<0.128 mg/Kg - dry 0.128 0.3804-Chloroaniline 1 11/27/23 15:27 V40513AMP
<0.133 mg/Kg - dry 0.133 0.7582-Chloronaphthalene 1 11/27/23 15:27 V40513AMP
<0.112 mg/Kg - dry 0.112 0.7582-Chlorophenol 1 11/27/23 15:27 V40513AMP
<0.144 mg/Kg - dry 0.144 1.154-Chlorophenyl phenyl ether 1 11/27/23 15:27 V40513AMP
<0.163 mg/Kg - dry 0.163 0.758Chrysene 1 11/27/23 15:27 V40513AMP
<0.264 mg/Kg - dry 0.264 0.758Dibenz(a,h)anthracene 1 11/27/23 15:27 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 77 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-4 (0-2)
89895 Matrix:
11/20/2023 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.136 mg/Kg - dry 0.136 0.758Dibenzofuran 1 11/27/23 15:27 V40513AMP
<0.108 mg/Kg - dry 0.108 0.7581,2-Dichlorobenzene 1 11/27/23 15:27 V40513AMP
<0.111 mg/Kg - dry 0.111 0.7581,3-Dichlorobenzene 1 11/27/23 15:27 V40513AMP
<0.112 mg/Kg - dry 0.112 0.3801,4-Dichlorobenzene 1 11/27/23 15:27 V40513AMP
<0.168 mg/Kg - dry 0.168 0.7583,3'-Dichlorobenzidine 1 11/27/23 15:27 V40513AMP
<0.110 mg/Kg - dry 0.110 0.7582,4-Dichlorophenol 1 11/27/23 15:27 V40513AMP
<0.206 mg/Kg - dry 0.206 0.758Diethyl phthalate 1 11/27/23 15:27 V40513AMP
<0.199 mg/Kg - dry 0.199 0.758Dimethyl phthalate 1 11/27/23 15:27 V40513AMP
<0.123 mg/Kg - dry 0.123 0.3802,4-Dimethylphenol 1 11/27/23 15:27 V40513AMP
<0.122 mg/Kg - dry 0.122 0.758Di-n-butyl phthalate 1 11/27/23 15:27 V40513AMP
<0.275 mg/Kg - dry 0.275 1.724,6-Dinitro-2-methylphenol 1 11/27/23 15:27 V40513AMP
<0.597 mg/Kg - dry 0.597 1.722,4-Dinitrophenol 1 11/27/23 15:27 V40513AMP
<0.111 mg/Kg - dry 0.111 0.7582,4-Dinitrotoluene 1 11/27/23 15:27 V40513AMP
<0.123 mg/Kg - dry 0.123 0.7582,6-Dinitrotoluene 1 11/27/23 15:27 V40513AMP
<0.164 mg/Kg - dry 0.164 0.380Di-n-Octyl Phthalate 1 11/27/23 15:27 V40513AMP
<0.141 mg/Kg - dry 0.141 0.758Fluoranthene 1 11/27/23 15:27 V40513AMP
<0.146 mg/Kg - dry 0.146 0.758Fluorene 1 11/27/23 15:27 V40513AMP
<0.121 mg/Kg - dry 0.121 0.758Hexachlorobenzene 1 11/27/23 15:27 V40513AMP
<0.112 mg/Kg - dry 0.112 0.758Hexachlorobutadiene 1 11/27/23 15:27 V40513AMP
<0.180 mg/Kg - dry 0.180 0.758Hexachlorocyclopentadiene 1 11/27/23 15:27 V40513AMP
<0.091 mg/Kg - dry 0.091 0.758Hexachloroethane 1 11/27/23 15:27 V40513AMP
<0.205 mg/Kg - dry 0.205 0.758Indeno(1,2,3-cd)pyrene 1 11/27/23 15:27 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 78 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-4 (0-2)
89895 Matrix:
11/20/2023 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.219 mg/Kg - dry 0.219 0.758Isophorone 1 11/27/23 15:27 V40513AMP
<0.121 mg/Kg - dry 0.121 0.7581-Methylnaphthalene 1 11/27/23 15:27 V40513AMP
<0.114 mg/Kg - dry 0.114 0.7582-Methylnaphthalene 1 11/27/23 15:27 V40513AMP
<0.111 mg/Kg - dry 0.111 0.7582-Methylphenol 1 11/27/23 15:27 V40513AMP
<0.097 mg/Kg - dry 0.097 0.7583&4 Methylphenol 1 11/27/23 15:27 V40513AMP
<0.165 mg/Kg - dry 0.165 0.758Naphthalene 1 11/27/23 15:27 V40513AMP
<0.111 mg/Kg - dry 0.111 0.7582-Nitroaniline 1 11/27/23 15:27 V40513AMP
<0.137 mg/Kg - dry 0.137 0.7583-Nitroaniline 1 11/27/23 15:27 V40513AMP
<0.107 mg/Kg - dry 0.107 0.3804-Nitroaniline 1 11/27/23 15:27 V40513AMP
<0.133 mg/Kg - dry 0.133 0.380Nitrobenzene 1 11/27/23 15:27 V40513AMP
<0.102 mg/Kg - dry 0.102 0.7582-Nitrophenol 1 11/27/23 15:27 V40513AMP
<0.134 mg/Kg - dry 0.134 0.7584-Nitrophenol 1 11/27/23 15:27 V40513AMP
<0.301 mg/Kg - dry 0.301 0.758N-Nitrosodimethylamine 1 11/27/23 15:27 V40513AMP
<0.207 mg/Kg - dry 0.207 0.758N-Nitrosodiphenylamine 1 11/27/23 15:27 V40513AMP
<0.135 mg/Kg - dry 0.135 0.758N-Nitroso-di-n-propylamine 1 11/27/23 15:27 V40513AMP
<0.398 mg/Kg - dry 0.398 1.15Pentachlorophenol 1 11/27/23 15:27 V40513AMP
<0.238 mg/Kg - dry 0.238 0.758Phenanthrene 1 11/27/23 15:27 V40513AMP
<0.128 mg/Kg - dry 0.128 0.758Phenol 1 11/27/23 15:27 V40513AMP
<0.153 mg/Kg - dry 0.153 0.758Pyrene 1 11/27/23 15:27 V40513AMP
<0.091 mg/Kg - dry 0.091 0.380Pyridine 1 11/27/23 15:27 V40513AMP
<0.122 mg/Kg - dry 0.122 0.7581,2,4-Trichlorobenzene 1 11/27/23 15:27 V40513AMP
<0.110 mg/Kg - dry 0.110 0.7582,4,5-Trichlorophenol 1 11/27/23 15:27 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 79 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-4 (0-2)
89895 Matrix:
11/20/2023 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.111 mg/Kg - dry 0.111 0.7582,4,6-Trichlorophenol 1 11/27/23 15:27 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 80 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-5 (0-2)
89896 Matrix:
11/20/2023 13:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
8.18 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
0.417 mg/Kg - dry 0.153 0.217Chromium, Hexavalent 1 12/06/23 12:22 SW-7199SWB
0.662 mg/Kg - dry 0.0931 0.272Arsenic 5 12/09/23 15:45 6020BBKN
78.3 mg/Kg - dry 0.046 0.272Barium 5 12/09/23 15:45 6020BBKN
<0.0283 mg/Kg - dry 0.0283 0.272Cadmium 5 12/09/23 15:45 6020BBKN
60.0 mg/Kg - dry 0.126 0.272Chromium 5 12/12/23 00:40 6020BJTR
4.67 mg/Kg - dry 0.0337 0.272Lead 5 12/09/23 15:45 6020BBKN
0.0230 J mg/Kg - dry 0.0131 0.0327Mercury (Total)1 11/30/23 16:53 7471BJKC
0.261 J mg/Kg - dry 0.112 0.272Selenium 5 12/09/23 15:45 6020BJTR
0.0112 J mg/Kg - dry 0.0073 0.272Silver 5 12/09/23 15:45 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 81 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-5 (0-2)
89896 Matrix:
11/20/2023 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0020 mg/Kg - dry 0.0020 0.0054Aldrin 1 11/30/23 19:05 V40768TJW
<0.0012 mg/Kg - dry 0.0012 0.0054alpha-BHC 1 11/30/23 19:05 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0054beta-BHC 1 11/30/23 19:05 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0054delta-BHC 1 11/30/23 19:05 V40768TJW
<0.0191 mg/Kg - dry 0.0191 0.0544Chlordane 1 11/30/23 19:05 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0054alpha-Chlordane 1 11/30/23 19:05 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0054gamma-Chlordane 1 11/30/23 19:05 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.00544,4'-DDD 1 11/30/23 19:05 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.00544,4'-DDE 1 11/30/23 19:05 V40768TJW
<0.0016 mg/Kg - dry 0.0016 0.00544,4'-DDT 1 11/30/23 19:05 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0054Dieldrin 1 11/30/23 19:05 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0054Endosulfan I 1 11/30/23 19:05 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0054Endosulfan II 1 11/30/23 19:05 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0054Endosulfan Sulfate 1 11/30/23 19:05 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0054Endrin 1 11/30/23 19:05 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0054Endrin Aldehyde 1 11/30/23 19:05 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0054Endrin Ketone 1 11/30/23 19:05 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0054gamma-BHC 1 11/30/23 19:05 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0054Heptachlor 1 11/30/23 19:05 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0054Heptachlor Epoxide 1 11/30/23 19:05 V40768TJW
<0.0028 mg/Kg - dry 0.0028 0.0054Methoxychlor 1 11/30/23 19:05 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 82 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-5 (0-2)
89896 Matrix:
11/20/2023 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0111 mg/Kg - dry 0.0111 0.0544 1 11/30/23 19:05 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.101 mg/Kg - dry 0.002 0.021Acetone 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.021Acrolein 1 11/22/23 17:31 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 11/22/23 17:31 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 11/22/23 17:31 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Bromomethane 1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 11/22/23 17:31 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 11/22/23 17:31 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/22/23 17:31 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 11/22/23 17:31 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 83 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-5 (0-2)
89896 Matrix:
11/20/2023 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 11/22/23 17:31 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/22/23 17:31 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 11/22/23 17:31 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/22/23 17:31 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/22/23 17:31 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 11/22/23 17:31 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 11/22/23 17:31 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/22/23 17:31 V40555TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 11/22/23 17:31 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/22/23 17:31 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 11/22/23 17:31 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/22/23 17:31 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/22/23 17:31 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/22/23 17:31 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/22/23 17:31 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 84 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-5 (0-2)
89896 Matrix:
11/20/2023 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 11/22/23 17:31 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/22/23 17:31 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/22/23 17:31 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 11/22/23 17:31 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.054Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 17:31 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.010Hexachlorobutadiene 1 11/22/23 17:31 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 11/22/23 17:31 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0212-Hexanone 1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/22/23 17:31 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 11/22/23 17:31 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/22/23 17:31 V40555TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Naphthalene 1 11/22/23 17:31 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/22/23 17:31 V40555TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 11/22/23 17:31 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.005 1 11/22/23 17:31 V40555TBL
0.001 J mg/Kg - dry 0.0007 0.005 1 11/22/23 17:31 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 11/22/23 17:31 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 85 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-5 (0-2)
89896 Matrix:
11/20/2023 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/22/23 17:31 V40555TBL
<0.002 mg/Kg - dry 0.002 0.010 1 11/22/23 17:31 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 11/22/23 17:31 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 11/22/23 17:31 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 11/22/23 17:31 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 11/22/23 17:31 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.126 mg/Kg - dry 0.126 0.718Acenaphthene 1 11/23/23 03:51 V40513AMP
<0.114 mg/Kg - dry 0.114 0.718Acenaphthylene 1 11/23/23 03:51 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 86 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-5 (0-2)
89896 Matrix:
11/20/2023 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.165 mg/Kg - dry 0.165 0.718Aniline 1 11/23/23 03:51 V40513AMP
<0.155 mg/Kg - dry 0.155 0.718Anthracene 1 11/23/23 03:51 V40513AMP
<0.151 mg/Kg - dry 0.151 0.718Benzo(a)anthracene 1 11/23/23 03:51 V40513AMP
<0.160 mg/Kg - dry 0.160 0.718Benzo(a)pyrene 1 11/23/23 03:51 V40513AMP
<0.159 mg/Kg - dry 0.159 0.718Benzo(b)fluoranthene 1 11/23/23 03:51 V40513AMP
<0.148 mg/Kg - dry 0.148 0.718Benzo(g,h,i)perylene 1 11/23/23 03:51 V40513AMP
<0.149 mg/Kg - dry 0.149 0.718Benzo(k)fluoranthene 1 11/23/23 03:51 V40513AMP
<0.631 M mg/Kg - dry 0.631 2.18Benzoic Acid 1 11/23/23 03:51 V40513AMP
<0.114 mg/Kg - dry 0.114 0.718Benzyl alcohol 1 11/23/23 03:51 V40513AMP
<0.128 mg/Kg - dry 0.128 0.718Bis(2-Chloroethoxy)methane 1 11/23/23 03:51 V40513AMP
<0.116 mg/Kg - dry 0.116 0.718Bis(2-Chloroethyl)ether 1 11/23/23 03:51 V40513AMP
<0.148 mg/Kg - dry 0.148 0.359Bis(2-Chloroisopropyl)ether 1 11/23/23 03:51 V40513AMP
<0.130 mg/Kg - dry 0.130 0.718Bis(2-ethylhexyl)phthalate 1 11/23/23 03:51 V40513AMP
<0.118 mg/Kg - dry 0.118 0.7184-Bromophenyl phenyl ether 1 11/23/23 03:51 V40513AMP
<0.123 mg/Kg - dry 0.123 0.359Butyl benzyl phthalate 1 11/23/23 03:51 V40513AMP
<0.100 mg/Kg - dry 0.100 0.7184-Chloro-3-methylphenol 1 11/23/23 03:51 V40513AMP
<0.121 mg/Kg - dry 0.121 0.3594-Chloroaniline 1 11/23/23 03:51 V40513AMP
<0.126 mg/Kg - dry 0.126 0.7182-Chloronaphthalene 1 11/23/23 03:51 V40513AMP
<0.106 mg/Kg - dry 0.106 0.7182-Chlorophenol 1 11/23/23 03:51 V40513AMP
<0.137 mg/Kg - dry 0.137 1.094-Chlorophenyl phenyl ether 1 11/23/23 03:51 V40513AMP
<0.154 mg/Kg - dry 0.154 0.718Chrysene 1 11/23/23 03:51 V40513AMP
<0.250 mg/Kg - dry 0.250 0.718Dibenz(a,h)anthracene 1 11/23/23 03:51 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 87 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-5 (0-2)
89896 Matrix:
11/20/2023 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.129 mg/Kg - dry 0.129 0.718Dibenzofuran 1 11/23/23 03:51 V40513AMP
<0.102 mg/Kg - dry 0.102 0.7181,2-Dichlorobenzene 1 11/23/23 03:51 V40513AMP
<0.105 mg/Kg - dry 0.105 0.7181,3-Dichlorobenzene 1 11/23/23 03:51 V40513AMP
<0.106 mg/Kg - dry 0.106 0.3591,4-Dichlorobenzene 1 11/23/23 03:51 V40513AMP
<0.160 mg/Kg - dry 0.160 0.7183,3'-Dichlorobenzidine 1 11/23/23 03:51 V40513AMP
<0.104 mg/Kg - dry 0.104 0.7182,4-Dichlorophenol 1 11/23/23 03:51 V40513AMP
<0.196 mg/Kg - dry 0.196 0.718Diethyl phthalate 1 11/23/23 03:51 V40513AMP
<0.189 mg/Kg - dry 0.189 0.718Dimethyl phthalate 1 11/23/23 03:51 V40513AMP
<0.117 mg/Kg - dry 0.117 0.3592,4-Dimethylphenol 1 11/23/23 03:51 V40513AMP
<0.116 mg/Kg - dry 0.116 0.718Di-n-butyl phthalate 1 11/23/23 03:51 V40513AMP
<0.261 mg/Kg - dry 0.261 1.634,6-Dinitro-2-methylphenol 1 11/23/23 03:51 V40513AMP
<0.566 mg/Kg - dry 0.566 1.632,4-Dinitrophenol 1 11/23/23 03:51 V40513AMP
<0.105 mg/Kg - dry 0.105 0.7182,4-Dinitrotoluene 1 11/23/23 03:51 V40513AMP
<0.117 mg/Kg - dry 0.117 0.7182,6-Dinitrotoluene 1 11/23/23 03:51 V40513AMP
<0.155 mg/Kg - dry 0.155 0.359Di-n-Octyl Phthalate 1 11/23/23 03:51 V40513AMP
<0.133 mg/Kg - dry 0.133 0.718Fluoranthene 1 11/23/23 03:51 V40513AMP
<0.139 mg/Kg - dry 0.139 0.718Fluorene 1 11/23/23 03:51 V40513AMP
<0.115 mg/Kg - dry 0.115 0.718Hexachlorobenzene 1 11/23/23 03:51 V40513AMP
<0.106 mg/Kg - dry 0.106 0.718Hexachlorobutadiene 1 11/23/23 03:51 V40513AMP
<0.170 mg/Kg - dry 0.170 0.718Hexachlorocyclopentadiene 1 11/23/23 03:51 V40513AMP
<0.086 mg/Kg - dry 0.086 0.718Hexachloroethane 1 11/23/23 03:51 V40513AMP
<0.194 mg/Kg - dry 0.194 0.718Indeno(1,2,3-cd)pyrene 1 11/23/23 03:51 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 88 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-5 (0-2)
89896 Matrix:
11/20/2023 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.208 mg/Kg - dry 0.208 0.718Isophorone 1 11/23/23 03:51 V40513AMP
<0.115 mg/Kg - dry 0.115 0.7181-Methylnaphthalene 1 11/23/23 03:51 V40513AMP
<0.108 mg/Kg - dry 0.108 0.7182-Methylnaphthalene 1 11/23/23 03:51 V40513AMP
<0.105 mg/Kg - dry 0.105 0.7182-Methylphenol 1 11/23/23 03:51 V40513AMP
<0.092 mg/Kg - dry 0.092 0.7183&4 Methylphenol 1 11/23/23 03:51 V40513AMP
<0.156 mg/Kg - dry 0.156 0.718Naphthalene 1 11/23/23 03:51 V40513AMP
<0.105 mg/Kg - dry 0.105 0.7182-Nitroaniline 1 11/23/23 03:51 V40513AMP
<0.130 mg/Kg - dry 0.130 0.7183-Nitroaniline 1 11/23/23 03:51 V40513AMP
<0.101 mg/Kg - dry 0.101 0.3594-Nitroaniline 1 11/23/23 03:51 V40513AMP
<0.126 mg/Kg - dry 0.126 0.359Nitrobenzene 1 11/23/23 03:51 V40513AMP
<0.096 mg/Kg - dry 0.096 0.7182-Nitrophenol 1 11/23/23 03:51 V40513AMP
<0.127 mg/Kg - dry 0.127 0.7184-Nitrophenol 1 11/23/23 03:51 V40513AMP
<0.286 mg/Kg - dry 0.286 0.718N-Nitrosodimethylamine 1 11/23/23 03:51 V40513AMP
<0.197 mg/Kg - dry 0.197 0.718N-Nitrosodiphenylamine 1 11/23/23 03:51 V40513AMP
<0.128 mg/Kg - dry 0.128 0.718N-Nitroso-di-n-propylamine 1 11/23/23 03:51 V40513AMP
<0.377 mg/Kg - dry 0.377 1.09Pentachlorophenol 1 11/23/23 03:51 V40513AMP
<0.226 mg/Kg - dry 0.226 0.718Phenanthrene 1 11/23/23 03:51 V40513AMP
<0.121 mg/Kg - dry 0.121 0.718Phenol 1 11/23/23 03:51 V40513AMP
<0.145 mg/Kg - dry 0.145 0.718Pyrene 1 11/23/23 03:51 V40513AMP
<0.086 mg/Kg - dry 0.086 0.359Pyridine 1 11/23/23 03:51 V40513AMP
<0.116 mg/Kg - dry 0.116 0.7181,2,4-Trichlorobenzene 1 11/23/23 03:51 V40513AMP
<0.104 mg/Kg - dry 0.104 0.7182,4,5-Trichlorophenol 1 11/23/23 03:51 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 89 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-5 (0-2)
89896 Matrix:
11/20/2023 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.105 mg/Kg - dry 0.105 0.7182,4,6-Trichlorophenol 1 11/23/23 03:51 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 90 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-6 (0-2)
89897 Matrix:
11/20/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.89 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
1.51 mg/Kg - dry 0.156 0.221Chromium, Hexavalent 1 12/06/23 14:33 SW-7199SWB
2.20 mg/Kg - dry 0.0948 0.277Arsenic 5 12/09/23 15:58 6020BBKN
336 mg/Kg - dry 0.047 0.277Barium 5 12/09/23 15:58 6020BBKN
1.55 mg/Kg - dry 0.0288 0.277Cadmium 5 12/09/23 15:58 6020BBKN
99.1 mg/Kg - dry 0.128 0.277Chromium 5 12/09/23 15:58 6020BJTR
184 mg/Kg - dry 0.0344 0.277Lead 5 12/09/23 15:58 6020BBKN
0.0550 mg/Kg - dry 0.0133 0.0333Mercury (Total)1 11/30/23 16:55 7471BJKC
0.662 mg/Kg - dry 0.114 0.277Selenium 5 12/09/23 15:58 6020BJTR
0.613 mg/Kg - dry 0.0074 0.277Silver 5 12/09/23 15:58 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 91 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-6 (0-2)
89897 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0020 mg/Kg - dry 0.0020 0.0055Aldrin 1 11/30/23 19:18 V40768TJW
<0.0012 mg/Kg - dry 0.0012 0.0055alpha-BHC 1 11/30/23 19:18 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0055beta-BHC 1 11/30/23 19:18 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0055delta-BHC 1 11/30/23 19:18 V40768TJW
<0.0195 mg/Kg - dry 0.0195 0.0554Chlordane 1 11/30/23 19:18 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0055alpha-Chlordane 1 11/30/23 19:18 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0055gamma-Chlordane 1 11/30/23 19:18 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.00554,4'-DDD 1 11/30/23 19:18 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.00554,4'-DDE 1 11/30/23 19:18 V40768TJW
<0.0016 mg/Kg - dry 0.0016 0.00554,4'-DDT 1 11/30/23 19:18 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0055Dieldrin 1 11/30/23 19:18 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Endosulfan I 1 11/30/23 19:18 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Endosulfan II 1 11/30/23 19:18 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endosulfan Sulfate 1 11/30/23 19:18 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0055Endrin 1 11/30/23 19:18 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0055Endrin Aldehyde 1 11/30/23 19:18 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endrin Ketone 1 11/30/23 19:18 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0055gamma-BHC 1 11/30/23 19:18 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.0055Heptachlor 1 11/30/23 19:18 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Heptachlor Epoxide 1 11/30/23 19:18 V40768TJW
<0.0029 mg/Kg - dry 0.0029 0.0055Methoxychlor 1 11/30/23 19:18 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 92 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-6 (0-2)
89897 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0113 mg/Kg - dry 0.0113 0.0554 1 11/30/23 19:18 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.179 mg/Kg - dry 0.002 0.022Acetone 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 11/22/23 17:59 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 11/22/23 17:59 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 11/22/23 17:59 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/22/23 17:59 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/22/23 17:59 V40555TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 11/22/23 17:59 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 11/22/23 17:59 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/22/23 17:59 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/22/23 17:59 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/22/23 17:59 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 11/22/23 17:59 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 93 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-6 (0-2)
89897 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 11/22/23 17:59 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/22/23 17:59 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/22/23 17:59 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/22/23 17:59 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/22/23 17:59 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/22/23 17:59 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/22/23 17:59 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 11/22/23 17:59 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/22/23 17:59 V40555TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 11/22/23 17:59 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/22/23 17:59 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/22/23 17:59 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/22/23 17:59 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/22/23 17:59 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/22/23 17:59 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/22/23 17:59 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/22/23 17:59 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 94 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-6 (0-2)
89897 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 11/22/23 17:59 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/22/23 17:59 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/22/23 17:59 V40555TBL
0.0007 J mg/Kg - dry 0.0006 0.005Ethylbenzene 1 11/22/23 17:59 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 17:59 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/22/23 17:59 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 11/22/23 17:59 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 11/22/23 17:59 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/22/23 17:59 V40555TBL
0.004 J mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 11/22/23 17:59 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/22/23 17:59 V40555TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 11/22/23 17:59 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/22/23 17:59 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/22/23 17:59 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.005 1 11/22/23 17:59 V40555TBL
0.003 J mg/Kg - dry 0.0007 0.005 1 11/22/23 17:59 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/22/23 17:59 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 95 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-6 (0-2)
89897 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/22/23 17:59 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/22/23 17:59 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/22/23 17:59 V40555TBL
<0.002 mg/Kg - dry 0.002 0.011 1 11/22/23 17:59 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/22/23 17:59 V40555TBL
0.002 J mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 11/22/23 17:59 V40555TBL
0.0009 J mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/22/23 17:59 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/22/23 17:59 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 11/22/23 17:59 V40555TBL
0.001 J mg/Kg - dry 0.0006 0.005o-Xylene 1 11/22/23 17:59 V40555TBL
0.002 J mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/22/23 17:59 V40555TBL
0.004 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/22/23 17:59 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.128 mg/Kg - dry 0.128 0.732Acenaphthene 1 11/27/23 18:50 V40513AMP
<0.116 mg/Kg - dry 0.116 0.732Acenaphthylene 1 11/27/23 18:50 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 96 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-6 (0-2)
89897 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.168 mg/Kg - dry 0.168 0.732Aniline 1 11/27/23 18:50 V40513AMP
<0.158 mg/Kg - dry 0.158 0.732Anthracene 1 11/27/23 18:50 V40513AMP
<0.154 mg/Kg - dry 0.154 0.732Benzo(a)anthracene 1 11/27/23 18:50 V40513AMP
<0.163 mg/Kg - dry 0.163 0.732Benzo(a)pyrene 1 11/27/23 18:50 V40513AMP
<0.162 mg/Kg - dry 0.162 0.732Benzo(b)fluoranthene 1 11/27/23 18:50 V40513AMP
<0.150 mg/Kg - dry 0.150 0.732Benzo(g,h,i)perylene 1 11/27/23 18:50 V40513AMP
<0.152 mg/Kg - dry 0.152 0.732Benzo(k)fluoranthene 1 11/27/23 18:50 V40513AMP
<0.643 M mg/Kg - dry 0.643 2.22Benzoic Acid 1 11/27/23 18:50 V40513AMP
<0.116 mg/Kg - dry 0.116 0.732Benzyl alcohol 1 11/27/23 18:50 V40513AMP
<0.130 mg/Kg - dry 0.130 0.732Bis(2-Chloroethoxy)methane 1 11/27/23 18:50 V40513AMP
<0.118 mg/Kg - dry 0.118 0.732Bis(2-Chloroethyl)ether 1 11/27/23 18:50 V40513AMP
<0.150 mg/Kg - dry 0.150 0.366Bis(2-Chloroisopropyl)ether 1 11/27/23 18:50 V40513AMP
1.14 mg/Kg - dry 0.133 0.732Bis(2-ethylhexyl)phthalate 1 11/27/23 18:50 V40513AMP
<0.120 mg/Kg - dry 0.120 0.7324-Bromophenyl phenyl ether 1 11/27/23 18:50 V40513AMP
<0.125 mg/Kg - dry 0.125 0.366Butyl benzyl phthalate 1 11/27/23 18:50 V40513AMP
<0.102 mg/Kg - dry 0.102 0.7324-Chloro-3-methylphenol 1 11/27/23 18:50 V40513AMP
<0.124 mg/Kg - dry 0.124 0.3664-Chloroaniline 1 11/27/23 18:50 V40513AMP
<0.128 mg/Kg - dry 0.128 0.7322-Chloronaphthalene 1 11/27/23 18:50 V40513AMP
<0.108 mg/Kg - dry 0.108 0.7322-Chlorophenol 1 11/27/23 18:50 V40513AMP
<0.139 mg/Kg - dry 0.139 1.114-Chlorophenyl phenyl ether 1 11/27/23 18:50 V40513AMP
<0.157 mg/Kg - dry 0.157 0.732Chrysene 1 11/27/23 18:50 V40513AMP
<0.255 mg/Kg - dry 0.255 0.732Dibenz(a,h)anthracene 1 11/27/23 18:50 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 97 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-6 (0-2)
89897 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.132 mg/Kg - dry 0.132 0.732Dibenzofuran 1 11/27/23 18:50 V40513AMP
<0.104 mg/Kg - dry 0.104 0.7321,2-Dichlorobenzene 1 11/27/23 18:50 V40513AMP
<0.107 mg/Kg - dry 0.107 0.7321,3-Dichlorobenzene 1 11/27/23 18:50 V40513AMP
<0.108 mg/Kg - dry 0.108 0.3661,4-Dichlorobenzene 1 11/27/23 18:50 V40513AMP
<0.163 mg/Kg - dry 0.163 0.7323,3'-Dichlorobenzidine 1 11/27/23 18:50 V40513AMP
<0.106 mg/Kg - dry 0.106 0.7322,4-Dichlorophenol 1 11/27/23 18:50 V40513AMP
<0.199 mg/Kg - dry 0.199 0.732Diethyl phthalate 1 11/27/23 18:50 V40513AMP
<0.193 mg/Kg - dry 0.193 0.732Dimethyl phthalate 1 11/27/23 18:50 V40513AMP
<0.119 mg/Kg - dry 0.119 0.3662,4-Dimethylphenol 1 11/27/23 18:50 V40513AMP
<0.118 mg/Kg - dry 0.118 0.732Di-n-butyl phthalate 1 11/27/23 18:50 V40513AMP
<0.266 mg/Kg - dry 0.266 1.664,6-Dinitro-2-methylphenol 1 11/27/23 18:50 V40513AMP
<0.577 mg/Kg - dry 0.577 1.662,4-Dinitrophenol 1 11/27/23 18:50 V40513AMP
<0.107 mg/Kg - dry 0.107 0.7322,4-Dinitrotoluene 1 11/27/23 18:50 V40513AMP
<0.119 mg/Kg - dry 0.119 0.7322,6-Dinitrotoluene 1 11/27/23 18:50 V40513AMP
<0.158 mg/Kg - dry 0.158 0.366Di-n-Octyl Phthalate 1 11/27/23 18:50 V40513AMP
<0.136 mg/Kg - dry 0.136 0.732Fluoranthene 1 11/27/23 18:50 V40513AMP
<0.142 mg/Kg - dry 0.142 0.732Fluorene 1 11/27/23 18:50 V40513AMP
<0.117 mg/Kg - dry 0.117 0.732Hexachlorobenzene 1 11/27/23 18:50 V40513AMP
<0.108 mg/Kg - dry 0.108 0.732Hexachlorobutadiene 1 11/27/23 18:50 V40513AMP
<0.174 mg/Kg - dry 0.174 0.732Hexachlorocyclopentadiene 1 11/27/23 18:50 V40513AMP
<0.087 mg/Kg - dry 0.087 0.732Hexachloroethane 1 11/27/23 18:50 V40513AMP
<0.198 mg/Kg - dry 0.198 0.732Indeno(1,2,3-cd)pyrene 1 11/27/23 18:50 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 98 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-6 (0-2)
89897 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.211 mg/Kg - dry 0.211 0.732Isophorone 1 11/27/23 18:50 V40513AMP
<0.117 mg/Kg - dry 0.117 0.7321-Methylnaphthalene 1 11/27/23 18:50 V40513AMP
<0.110 mg/Kg - dry 0.110 0.7322-Methylnaphthalene 1 11/27/23 18:50 V40513AMP
<0.107 mg/Kg - dry 0.107 0.7322-Methylphenol 1 11/27/23 18:50 V40513AMP
<0.094 mg/Kg - dry 0.094 0.7323&4 Methylphenol 1 11/27/23 18:50 V40513AMP
<0.159 mg/Kg - dry 0.159 0.732Naphthalene 1 11/27/23 18:50 V40513AMP
<0.107 mg/Kg - dry 0.107 0.7322-Nitroaniline 1 11/27/23 18:50 V40513AMP
<0.133 mg/Kg - dry 0.133 0.7323-Nitroaniline 1 11/27/23 18:50 V40513AMP
<0.103 mg/Kg - dry 0.103 0.3664-Nitroaniline 1 11/27/23 18:50 V40513AMP
<0.128 mg/Kg - dry 0.128 0.366Nitrobenzene 1 11/27/23 18:50 V40513AMP
<0.098 mg/Kg - dry 0.098 0.7322-Nitrophenol 1 11/27/23 18:50 V40513AMP
<0.129 mg/Kg - dry 0.129 0.7324-Nitrophenol 1 11/27/23 18:50 V40513AMP
<0.291 mg/Kg - dry 0.291 0.732N-Nitrosodimethylamine 1 11/27/23 18:50 V40513AMP
<0.200 mg/Kg - dry 0.200 0.732N-Nitrosodiphenylamine 1 11/27/23 18:50 V40513AMP
<0.130 mg/Kg - dry 0.130 0.732N-Nitroso-di-n-propylamine 1 11/27/23 18:50 V40513AMP
<0.385 mg/Kg - dry 0.385 1.11Pentachlorophenol 1 11/27/23 18:50 V40513AMP
<0.230 mg/Kg - dry 0.230 0.732Phenanthrene 1 11/27/23 18:50 V40513AMP
<0.124 mg/Kg - dry 0.124 0.732Phenol 1 11/27/23 18:50 V40513AMP
<0.148 mg/Kg - dry 0.148 0.732Pyrene 1 11/27/23 18:50 V40513AMP
<0.087 mg/Kg - dry 0.087 0.366Pyridine 1 11/27/23 18:50 V40513AMP
<0.118 mg/Kg - dry 0.118 0.7321,2,4-Trichlorobenzene 1 11/27/23 18:50 V40513AMP
<0.106 mg/Kg - dry 0.106 0.7322,4,5-Trichlorophenol 1 11/27/23 18:50 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 99 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-6 (0-2)
89897 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.107 mg/Kg - dry 0.107 0.7322,4,6-Trichlorophenol 1 11/27/23 18:50 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 100 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-7 (0-2)
89898 Matrix:
11/20/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.6 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
1.13 mg/Kg - dry 0.167 0.236Chromium, Hexavalent 1 12/06/23 14:44 SW-7199SWB
1.24 mg/Kg - dry 0.101 0.296Arsenic 5 12/09/23 16:02 6020BBKN
84.5 mg/Kg - dry 0.050 0.296Barium 5 12/09/23 16:02 6020BBKN
0.128 J mg/Kg - dry 0.0308 0.296Cadmium 5 12/09/23 16:02 6020BBKN
48.0 mg/Kg - dry 0.137 0.296Chromium 5 12/09/23 16:02 6020BBKN
21.2 mg/Kg - dry 0.0367 0.296Lead 5 12/09/23 16:02 6020BBKN
<0.0142 mg/Kg - dry 0.0142 0.0355Mercury (Total)1 11/30/23 16:58 7471BJKC
0.436 mg/Kg - dry 0.122 0.296Selenium 5 12/09/23 16:02 6020BBKN
0.0581 J mg/Kg - dry 0.0079 0.296Silver 5 12/09/23 16:02 6020B
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 101 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-7 (0-2)
89898 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0021 mg/Kg - dry 0.0021 0.0059Aldrin 1 11/30/23 19:31 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0059alpha-BHC 1 11/30/23 19:31 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0059beta-BHC 1 11/30/23 19:31 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0059delta-BHC 1 11/30/23 19:31 V40768TJW
<0.0208 mg/Kg - dry 0.0208 0.0592Chlordane 1 11/30/23 19:31 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0059alpha-Chlordane 1 11/30/23 19:31 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0059gamma-Chlordane 1 11/30/23 19:31 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.00594,4'-DDD 1 11/30/23 19:31 V40768TJW
<0.0024 mg/Kg - dry 0.0024 0.00594,4'-DDE 1 11/30/23 19:31 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.00594,4'-DDT 1 11/30/23 19:31 V40768TJW
<0.0024 mg/Kg - dry 0.0024 0.0059Dieldrin 1 11/30/23 19:31 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0059Endosulfan I 1 11/30/23 19:31 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0059Endosulfan II 1 11/30/23 19:31 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0059Endosulfan Sulfate 1 11/30/23 19:31 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0059Endrin 1 11/30/23 19:31 V40768TJW
<0.0025 mg/Kg - dry 0.0025 0.0059Endrin Aldehyde 1 11/30/23 19:31 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0059Endrin Ketone 1 11/30/23 19:31 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0059gamma-BHC 1 11/30/23 19:31 V40768TJW
<0.0016 mg/Kg - dry 0.0016 0.0059Heptachlor 1 11/30/23 19:31 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0059Heptachlor Epoxide 1 11/30/23 19:31 V40768TJW
<0.0031 mg/Kg - dry 0.0031 0.0059Methoxychlor 1 11/30/23 19:31 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 102 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-7 (0-2)
89898 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0120 mg/Kg - dry 0.0120 0.0592 1 11/30/23 19:31 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/27/23 08:00
0.069 mg/Kg - dry 0.002 0.023Acetone 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 11/27/23 21:00 V40615TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 11/27/23 21:00 V40615TBL
0.003 J mg/Kg - dry 0.0007 0.005Benzene 1 11/27/23 21:00 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/27/23 21:00 V40615TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/27/23 21:00 V40615TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 11/27/23 21:00 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/27/23 21:00 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 11/27/23 21:00 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/27/23 21:00 V40615TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/27/23 21:00 V40615TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/27/23 21:00 V40615TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 103 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-7 (0-2)
89898 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/27/23 08:00
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/27/23 21:00 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/27/23 21:00 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/27/23 21:00 V40615TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 11/27/23 21:00 V40615TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 11/27/23 21:00 V40615TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/27/23 21:00 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 11/27/23 21:00 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 11/27/23 21:00 V40615TBL
0.015 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/27/23 21:00 V40615TBL
0.001 J mg/Kg - dry 0.0005 0.0051,3-Dichlorobenzene 1 11/27/23 21:00 V40615TBL
0.010 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/27/23 21:00 V40615TBL
0.034 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/27/23 21:00 V40615TBL
0.002 J mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 11/27/23 21:00 V40615TBL
0.008 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/27/23 21:00 V40615TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/27/23 21:00 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/27/23 21:00 V40615TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 104 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-7 (0-2)
89898 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/27/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/27/23 21:00 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/27/23 21:00 V40615TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/27/23 21:00 V40615TBL
0.011 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/27/23 21:00 V40615TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 11/27/23 21:00 V40615TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/27/23 21:00 V40615TBL
0.005 J mg/Kg - dry 0.0008 0.011n-Hexane 1 11/27/23 21:00 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 11/27/23 21:00 V40615TBL
0.018 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/27/23 21:00 V40615TBL
0.005 J mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/27/23 21:00 V40615TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 11/27/23 21:00 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/27/23 21:00 V40615TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/27/23 21:00 V40615TBL
0.018 mg/Kg - dry 0.001 0.011Naphthalene 1 11/27/23 21:00 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/27/23 21:00 V40615TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/27/23 21:00 V40615TBL
0.022 mg/Kg - dry 0.0008 0.005 1 11/27/23 21:00 V40615TBL
0.003 J mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/27/23 21:00 V40615TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 105 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-7 (0-2)
89898 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/27/23 08:00
0.029 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/27/23 21:00 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 11/27/23 21:00 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/27/23 21:00 V40615TBL
<0.002 mg/Kg - dry 0.002 0.011 1 11/27/23 21:00 V40615TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 11/27/23 21:00 V40615TBL
0.004 J mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/27/23 21:00 V40615TBL
0.002 J mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/27/23 21:00 V40615TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/27/23 21:00 V40615TBL
0.001 J mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/27/23 21:00 V40615TBL
0.013 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/27/23 21:00 V40615TBL
0.026 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/27/23 21:00 V40615TBL
0.039 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/27/23 21:00 V40615KCC
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.137 mg/Kg - dry 0.137 0.781Acenaphthene 1 11/27/23 15:49 V40513AMP
<0.124 mg/Kg - dry 0.124 0.781Acenaphthylene 1 11/27/23 15:49 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 106 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-7 (0-2)
89898 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.180 mg/Kg - dry 0.180 0.781Aniline 1 11/27/23 15:49 V40513AMP
<0.169 mg/Kg - dry 0.169 0.781Anthracene 1 11/27/23 15:49 V40513AMP
<0.164 mg/Kg - dry 0.164 0.781Benzo(a)anthracene 1 11/27/23 15:49 V40513AMP
<0.174 mg/Kg - dry 0.174 0.781Benzo(a)pyrene 1 11/27/23 15:49 V40513AMP
<0.172 mg/Kg - dry 0.172 0.781Benzo(b)fluoranthene 1 11/27/23 15:49 V40513AMP
<0.161 mg/Kg - dry 0.161 0.781Benzo(g,h,i)perylene 1 11/27/23 15:49 V40513AMP
<0.162 mg/Kg - dry 0.162 0.781Benzo(k)fluoranthene 1 11/27/23 15:49 V40513AMP
<0.687 M mg/Kg - dry 0.687 2.37Benzoic Acid 1 11/27/23 15:49 V40513AMP
<0.124 mg/Kg - dry 0.124 0.781Benzyl alcohol 1 11/27/23 15:49 V40513AMP
<0.139 mg/Kg - dry 0.139 0.781Bis(2-Chloroethoxy)methane 1 11/27/23 15:49 V40513AMP
<0.126 mg/Kg - dry 0.126 0.781Bis(2-Chloroethyl)ether 1 11/27/23 15:49 V40513AMP
<0.161 mg/Kg - dry 0.161 0.390Bis(2-Chloroisopropyl)ether 1 11/27/23 15:49 V40513AMP
<0.142 mg/Kg - dry 0.142 0.781Bis(2-ethylhexyl)phthalate 1 11/27/23 15:49 V40513AMP
<0.129 mg/Kg - dry 0.129 0.7814-Bromophenyl phenyl ether 1 11/27/23 15:49 V40513AMP
<0.133 mg/Kg - dry 0.133 0.390Butyl benzyl phthalate 1 11/27/23 15:49 V40513AMP
<0.109 mg/Kg - dry 0.109 0.7814-Chloro-3-methylphenol 1 11/27/23 15:49 V40513AMP
<0.132 mg/Kg - dry 0.132 0.3904-Chloroaniline 1 11/27/23 15:49 V40513AMP
<0.137 mg/Kg - dry 0.137 0.7812-Chloronaphthalene 1 11/27/23 15:49 V40513AMP
<0.116 mg/Kg - dry 0.116 0.7812-Chlorophenol 1 11/27/23 15:49 V40513AMP
<0.149 mg/Kg - dry 0.149 1.184-Chlorophenyl phenyl ether 1 11/27/23 15:49 V40513AMP
<0.168 mg/Kg - dry 0.168 0.781Chrysene 1 11/27/23 15:49 V40513AMP
<0.272 mg/Kg - dry 0.272 0.781Dibenz(a,h)anthracene 1 11/27/23 15:49 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 107 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-7 (0-2)
89898 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.140 mg/Kg - dry 0.140 0.781Dibenzofuran 1 11/27/23 15:49 V40513AMP
<0.111 mg/Kg - dry 0.111 0.7811,2-Dichlorobenzene 1 11/27/23 15:49 V40513AMP
<0.115 mg/Kg - dry 0.115 0.7811,3-Dichlorobenzene 1 11/27/23 15:49 V40513AMP
<0.115 mg/Kg - dry 0.115 0.3901,4-Dichlorobenzene 1 11/27/23 15:49 V40513AMP
<0.174 mg/Kg - dry 0.174 0.7813,3'-Dichlorobenzidine 1 11/27/23 15:49 V40513AMP
<0.113 mg/Kg - dry 0.113 0.7812,4-Dichlorophenol 1 11/27/23 15:49 V40513AMP
<0.213 mg/Kg - dry 0.213 0.781Diethyl phthalate 1 11/27/23 15:49 V40513AMP
<0.206 mg/Kg - dry 0.206 0.781Dimethyl phthalate 1 11/27/23 15:49 V40513AMP
<0.127 mg/Kg - dry 0.127 0.3902,4-Dimethylphenol 1 11/27/23 15:49 V40513AMP
<0.126 mg/Kg - dry 0.126 0.781Di-n-butyl phthalate 1 11/27/23 15:49 V40513AMP
<0.284 mg/Kg - dry 0.284 1.784,6-Dinitro-2-methylphenol 1 11/27/23 15:49 V40513AMP
<0.616 mg/Kg - dry 0.616 1.782,4-Dinitrophenol 1 11/27/23 15:49 V40513AMP
<0.114 mg/Kg - dry 0.114 0.7812,4-Dinitrotoluene 1 11/27/23 15:49 V40513AMP
<0.127 mg/Kg - dry 0.127 0.7812,6-Dinitrotoluene 1 11/27/23 15:49 V40513AMP
<0.169 mg/Kg - dry 0.169 0.390Di-n-Octyl Phthalate 1 11/27/23 15:49 V40513AMP
<0.145 mg/Kg - dry 0.145 0.781Fluoranthene 1 11/27/23 15:49 V40513AMP
<0.151 mg/Kg - dry 0.151 0.781Fluorene 1 11/27/23 15:49 V40513AMP
<0.125 mg/Kg - dry 0.125 0.781Hexachlorobenzene 1 11/27/23 15:49 V40513AMP
<0.115 mg/Kg - dry 0.115 0.781Hexachlorobutadiene 1 11/27/23 15:49 V40513AMP
<0.186 mg/Kg - dry 0.186 0.781Hexachlorocyclopentadiene 1 11/27/23 15:49 V40513AMP
<0.093 mg/Kg - dry 0.093 0.781Hexachloroethane 1 11/27/23 15:49 V40513AMP
<0.212 mg/Kg - dry 0.212 0.781Indeno(1,2,3-cd)pyrene 1 11/27/23 15:49 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 108 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-7 (0-2)
89898 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.226 mg/Kg - dry 0.226 0.781Isophorone 1 11/27/23 15:49 V40513AMP
<0.125 mg/Kg - dry 0.125 0.7811-Methylnaphthalene 1 11/27/23 15:49 V40513AMP
<0.118 mg/Kg - dry 0.118 0.7812-Methylnaphthalene 1 11/27/23 15:49 V40513AMP
<0.114 mg/Kg - dry 0.114 0.7812-Methylphenol 1 11/27/23 15:49 V40513AMP
<0.100 mg/Kg - dry 0.100 0.7813&4 Methylphenol 1 11/27/23 15:49 V40513AMP
<0.170 mg/Kg - dry 0.170 0.781Naphthalene 1 11/27/23 15:49 V40513AMP
<0.114 mg/Kg - dry 0.114 0.7812-Nitroaniline 1 11/27/23 15:49 V40513AMP
<0.142 mg/Kg - dry 0.142 0.7813-Nitroaniline 1 11/27/23 15:49 V40513AMP
<0.110 mg/Kg - dry 0.110 0.3904-Nitroaniline 1 11/27/23 15:49 V40513AMP
<0.137 mg/Kg - dry 0.137 0.390Nitrobenzene 1 11/27/23 15:49 V40513AMP
<0.105 mg/Kg - dry 0.105 0.7812-Nitrophenol 1 11/27/23 15:49 V40513AMP
<0.138 mg/Kg - dry 0.138 0.7814-Nitrophenol 1 11/27/23 15:49 V40513AMP
<0.311 mg/Kg - dry 0.311 0.781N-Nitrosodimethylamine 1 11/27/23 15:49 V40513AMP
<0.214 mg/Kg - dry 0.214 0.781N-Nitrosodiphenylamine 1 11/27/23 15:49 V40513AMP
<0.139 mg/Kg - dry 0.139 0.781N-Nitroso-di-n-propylamine 1 11/27/23 15:49 V40513AMP
<0.411 mg/Kg - dry 0.411 1.18Pentachlorophenol 1 11/27/23 15:49 V40513AMP
<0.246 mg/Kg - dry 0.246 0.781Phenanthrene 1 11/27/23 15:49 V40513AMP
<0.132 mg/Kg - dry 0.132 0.781Phenol 1 11/27/23 15:49 V40513AMP
<0.158 mg/Kg - dry 0.158 0.781Pyrene 1 11/27/23 15:49 V40513AMP
<0.093 mg/Kg - dry 0.093 0.390Pyridine 1 11/27/23 15:49 V40513AMP
<0.126 mg/Kg - dry 0.126 0.7811,2,4-Trichlorobenzene 1 11/27/23 15:49 V40513AMP
<0.113 mg/Kg - dry 0.113 0.7812,4,5-Trichlorophenol 1 11/27/23 15:49 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 109 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-7 (0-2)
89898 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.114 mg/Kg - dry 0.114 0.7812,4,6-Trichlorophenol 1 11/27/23 15:49 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 110 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-8 (0-2)
89899 Matrix:
11/20/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.91 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
<0.156 mg/Kg - dry 0.156 0.222Chromium, Hexavalent 1 12/06/23 14:55 SW-7199SWB
2.11 mg/Kg - dry 0.0949 0.278Arsenic 5 12/09/23 16:30 6020BBKN
254 mg/Kg - dry 0.047 0.277Barium 5 12/09/23 16:30 6020BBKN
2.86 mg/Kg - dry 0.0288 0.278Cadmium 5 12/09/23 16:30 6020BBKN
83.0 mg/Kg - dry 0.128 0.277Chromium 5 12/09/23 16:30 6020BBKN
252 mg/Kg - dry 0.0344 0.278Lead 5 12/09/23 16:30 6020BBKN
0.194 mg/Kg - dry 0.0133 0.0333Mercury (Total)1 11/30/23 17:00 7471BJKC
0.516 mg/Kg - dry 0.114 0.277Selenium 5 12/09/23 16:30 6020BJTR
0.0844 J mg/Kg - dry 0.0074 0.278Silver 5 12/09/23 16:30 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 111 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-8 (0-2)
89899 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0020 mg/Kg - dry 0.0020 0.0055Aldrin 1 11/30/23 19:45 V40768TJW
0.0099 mg/Kg - dry 0.0012 0.0055alpha-BHC 1 11/30/23 19:45 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0055beta-BHC 1 11/30/23 19:45 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0055delta-BHC 1 11/30/23 19:45 V40768TJW
<0.0195 mg/Kg - dry 0.0195 0.0555Chlordane 1 11/30/23 19:45 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0055alpha-Chlordane 1 11/30/23 19:45 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0055gamma-Chlordane 1 11/30/23 19:45 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.00554,4'-DDD 1 11/30/23 19:45 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.00554,4'-DDE 1 11/30/23 19:45 V40768TJW
0.0663 mg/Kg - dry 0.0016 0.00554,4'-DDT 1 11/30/23 19:45 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0055Dieldrin 1 11/30/23 19:45 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Endosulfan I 1 11/30/23 19:45 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Endosulfan II 1 11/30/23 19:45 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endosulfan Sulfate 1 11/30/23 19:45 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0055Endrin 1 11/30/23 19:45 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0055Endrin Aldehyde 1 11/30/23 19:45 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endrin Ketone 1 11/30/23 19:45 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0055gamma-BHC 1 11/30/23 19:45 V40768TJW
0.0722 mg/Kg - dry 0.0015 0.0055Heptachlor 1 11/30/23 19:45 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Heptachlor Epoxide 1 11/30/23 19:45 V40768TJW
<0.0029 mg/Kg - dry 0.0029 0.0055Methoxychlor 1 11/30/23 19:45 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 112 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-8 (0-2)
89899 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0113 mg/Kg - dry 0.0113 0.0555 1 11/30/23 19:45 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/27/23 08:00
0.109 mg/Kg - dry 0.002 0.022Acetone 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 11/27/23 21:27 V40615TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 11/27/23 21:27 V40615TBL
0.008 mg/Kg - dry 0.0006 0.005Benzene 1 11/27/23 21:27 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/27/23 21:27 V40615TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/27/23 21:27 V40615TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 11/27/23 21:27 V40615TBL
0.0006 J mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 11/27/23 21:27 V40615TBL
0.0007 J mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/27/23 21:27 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/27/23 21:27 V40615TBL
0.003 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/27/23 21:27 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 11/27/23 21:27 V40615TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 113 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-8 (0-2)
89899 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/27/23 08:00
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 11/27/23 21:27 V40615TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/27/23 21:27 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/27/23 21:27 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/27/23 21:27 V40615TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/27/23 21:27 V40615TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/27/23 21:27 V40615TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/27/23 21:27 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 11/27/23 21:27 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/27/23 21:27 V40615TBL
0.011 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 11/27/23 21:27 V40615TBL
0.003 J mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/27/23 21:27 V40615TBL
0.004 J mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/27/23 21:27 V40615TBL
0.001 J mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/27/23 21:27 V40615TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/27/23 21:27 V40615TBL
0.009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/27/23 21:27 V40615TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/27/23 21:27 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/27/23 21:27 V40615TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 114 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-8 (0-2)
89899 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/27/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 11/27/23 21:27 V40615TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/27/23 21:27 V40615TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/27/23 21:27 V40615TBL
0.012 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 11/27/23 21:27 V40615TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 11/27/23 21:27 V40615TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/27/23 21:27 V40615TBL
0.070 mg/Kg - dry 0.0007 0.011n-Hexane 1 11/27/23 21:27 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 11/27/23 21:27 V40615TBL
0.001 J mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/27/23 21:27 V40615TBL
0.006 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/27/23 21:27 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 11/27/23 21:27 V40615TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/27/23 21:27 V40615TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/27/23 21:27 V40615TBL
0.003 J mg/Kg - dry 0.001 0.011Naphthalene 1 11/27/23 21:27 V40615TBL
0.001 J mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/27/23 21:27 V40615TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/27/23 21:27 V40615TBL
<0.0010 mg/Kg - dry 0.0010 0.005 1 11/27/23 21:27 V40615TBL
0.021 mg/Kg - dry 0.0007 0.005 1 11/27/23 21:27 V40615TBL
0.001 J mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/27/23 21:27 V40615TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 115 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-8 (0-2)
89899 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/27/23 08:00
0.025 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/27/23 21:27 V40615TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/27/23 21:27 V40615TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/27/23 21:27 V40615TBL
0.001 J mg/Kg - dry 0.001 0.005 1 11/27/23 21:27 V40615TBL
<0.002 mg/Kg - dry 0.002 0.011 1 11/27/23 21:27 V40615TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/27/23 21:27 V40615TBL
0.008 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 11/27/23 21:27 V40615TBL
0.003 J mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/27/23 21:27 V40615TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/27/23 21:27 V40615TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 11/27/23 21:27 V40615TBL
0.015 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/27/23 21:27 V40615TBL
0.020 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/27/23 21:27 V40615TBL
0.036 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/27/23 21:27 V40615
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<1.03 mg/Kg - dry 1.03 5.86Acenaphthene 4 11/27/23 16:12 V40513AMP
<0.932 mg/Kg - dry 0.932 5.86Acenaphthylene 4 11/27/23 16:12 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 116 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-8 (0-2)
89899 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<1.35 mg/Kg - dry 1.35 5.86Aniline 4 11/27/23 16:12 V40513AMP
<1.27 mg/Kg - dry 1.27 5.86Anthracene 4 11/27/23 16:12 V40513AMP
<1.23 mg/Kg - dry 1.23 5.86Benzo(a)anthracene 4 11/27/23 16:12 V40513AMP
<1.31 mg/Kg - dry 1.31 5.86Benzo(a)pyrene 4 11/27/23 16:12 V40513AMP
<1.30 mg/Kg - dry 1.30 5.86Benzo(b)fluoranthene 4 11/27/23 16:12 V40513AMP
<1.21 mg/Kg - dry 1.21 5.86Benzo(g,h,i)perylene 4 11/27/23 16:12 V40513AMP
<1.22 mg/Kg - dry 1.22 5.86Benzo(k)fluoranthene 4 11/27/23 16:12 V40513AMP
<5.15 M mg/Kg - dry 5.15 17.8Benzoic Acid 4 11/27/23 16:12 V40513AMP
<0.932 mg/Kg - dry 0.932 5.86Benzyl alcohol 4 11/27/23 16:12 V40513AMP
<1.05 mg/Kg - dry 1.05 5.86Bis(2-Chloroethoxy)methane 4 11/27/23 16:12 V40513AMP
<0.950 mg/Kg - dry 0.950 5.86Bis(2-Chloroethyl)ether 4 11/27/23 16:12 V40513AMP
<1.21 mg/Kg - dry 1.21 2.93Bis(2-Chloroisopropyl)ether 4 11/27/23 16:12 V40513AMP
103 mg/Kg - dry 2.66 14.7Bis(2-ethylhexyl)phthalate 10 11/27/23 18:27 V40513AMP
<0.967 mg/Kg - dry 0.967 5.864-Bromophenyl phenyl ether 4 11/27/23 16:12 V40513AMP
2.00 J mg/Kg - dry 1.00 2.93Butyl benzyl phthalate 4 11/27/23 16:12 V40513AMP
<0.820 mg/Kg - dry 0.820 5.864-Chloro-3-methylphenol 4 11/27/23 16:12 V40513AMP
<0.994 mg/Kg - dry 0.994 2.934-Chloroaniline 4 11/27/23 16:12 V40513AMP
<1.03 mg/Kg - dry 1.03 5.862-Chloronaphthalene 4 11/27/23 16:12 V40513AMP
<0.872 mg/Kg - dry 0.872 5.862-Chlorophenol 4 11/27/23 16:12 V40513AMP
<1.12 mg/Kg - dry 1.12 8.884-Chlorophenyl phenyl ether 4 11/27/23 16:12 V40513AMP
<1.27 mg/Kg - dry 1.27 5.86Chrysene 4 11/27/23 16:12 V40513AMP
<2.04 mg/Kg - dry 2.04 5.86Dibenz(a,h)anthracene 4 11/27/23 16:12 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 117 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-8 (0-2)
89899 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<1.06 mg/Kg - dry 1.06 5.86Dibenzofuran 4 11/27/23 16:12 V40513AMP
<0.838 mg/Kg - dry 0.838 5.861,2-Dichlorobenzene 4 11/27/23 16:12 V40513AMP
<0.863 mg/Kg - dry 0.863 5.861,3-Dichlorobenzene 4 11/27/23 16:12 V40513AMP
<0.865 mg/Kg - dry 0.865 2.931,4-Dichlorobenzene 4 11/27/23 16:12 V40513AMP
<1.31 mg/Kg - dry 1.31 5.863,3'-Dichlorobenzidine 4 11/27/23 16:12 V40513AMP
<0.850 mg/Kg - dry 0.850 5.862,4-Dichlorophenol 4 11/27/23 16:12 V40513AMP
<1.60 mg/Kg - dry 1.60 5.86Diethyl phthalate 4 11/27/23 16:12 V40513AMP
<1.54 mg/Kg - dry 1.54 5.86Dimethyl phthalate 4 11/27/23 16:12 V40513AMP
<0.959 mg/Kg - dry 0.959 2.932,4-Dimethylphenol 4 11/27/23 16:12 V40513AMP
<0.950 mg/Kg - dry 0.950 5.86Di-n-butyl phthalate 4 11/27/23 16:12 V40513AMP
<2.13 mg/Kg - dry 2.13 13.34,6-Dinitro-2-methylphenol 4 11/27/23 16:12 V40513AMP
<4.62 mg/Kg - dry 4.62 13.32,4-Dinitrophenol 4 11/27/23 16:12 V40513AMP
<0.858 mg/Kg - dry 0.858 5.862,4-Dinitrotoluene 4 11/27/23 16:12 V40513AMP
<0.959 mg/Kg - dry 0.959 5.862,6-Dinitrotoluene 4 11/27/23 16:12 V40513AMP
<1.27 mg/Kg - dry 1.27 2.93Di-n-Octyl Phthalate 4 11/27/23 16:12 V40513AMP
<1.09 mg/Kg - dry 1.09 5.86Fluoranthene 4 11/27/23 16:12 V40513AMP
<1.13 mg/Kg - dry 1.13 5.86Fluorene 4 11/27/23 16:12 V40513AMP
<0.941 mg/Kg - dry 0.941 5.86Hexachlorobenzene 4 11/27/23 16:12 V40513AMP
<0.866 mg/Kg - dry 0.866 5.86Hexachlorobutadiene 4 11/27/23 16:12 V40513AMP
<1.40 mg/Kg - dry 1.40 5.86Hexachlorocyclopentadiene 4 11/27/23 16:12 V40513AMP
<0.703 mg/Kg - dry 0.703 5.86Hexachloroethane 4 11/27/23 16:12 V40513AMP
<1.59 mg/Kg - dry 1.59 5.86Indeno(1,2,3-cd)pyrene 4 11/27/23 16:12 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 118 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-8 (0-2)
89899 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<1.70 mg/Kg - dry 1.70 5.86Isophorone 4 11/27/23 16:12 V40513AMP
<0.941 mg/Kg - dry 0.941 5.861-Methylnaphthalene 4 11/27/23 16:12 V40513AMP
<0.888 mg/Kg - dry 0.888 5.862-Methylnaphthalene 4 11/27/23 16:12 V40513AMP
<0.861 mg/Kg - dry 0.861 5.862-Methylphenol 4 11/27/23 16:12 V40513AMP
<0.753 mg/Kg - dry 0.753 5.863&4 Methylphenol 4 11/27/23 16:12 V40513AMP
<1.28 mg/Kg - dry 1.28 5.86Naphthalene 4 11/27/23 16:12 V40513AMP
<0.859 mg/Kg - dry 0.859 5.862-Nitroaniline 4 11/27/23 16:12 V40513AMP
<1.07 mg/Kg - dry 1.07 5.863-Nitroaniline 4 11/27/23 16:12 V40513AMP
<0.828 mg/Kg - dry 0.828 2.934-Nitroaniline 4 11/27/23 16:12 V40513AMP
<1.03 mg/Kg - dry 1.03 2.93Nitrobenzene 4 11/27/23 16:12 V40513AMP
<0.788 mg/Kg - dry 0.788 5.862-Nitrophenol 4 11/27/23 16:12 V40513AMP
<1.04 mg/Kg - dry 1.04 5.864-Nitrophenol 4 11/27/23 16:12 V40513AMP
<2.33 mg/Kg - dry 2.33 5.86N-Nitrosodimethylamine 4 11/27/23 16:12 V40513AMP
<1.61 mg/Kg - dry 1.61 5.86N-Nitrosodiphenylamine 4 11/27/23 16:12 V40513AMP
<1.05 mg/Kg - dry 1.05 5.86N-Nitroso-di-n-propylamine 4 11/27/23 16:12 V40513AMP
<3.09 mg/Kg - dry 3.09 8.88Pentachlorophenol 4 11/27/23 16:12 V40513AMP
<1.84 mg/Kg - dry 1.84 5.86Phenanthrene 4 11/27/23 16:12 V40513AMP
<0.994 mg/Kg - dry 0.994 5.86Phenol 4 11/27/23 16:12 V40513AMP
<1.19 mg/Kg - dry 1.19 5.86Pyrene 4 11/27/23 16:12 V40513AMP
<0.703 mg/Kg - dry 0.703 2.93Pyridine 4 11/27/23 16:12 V40513AMP
1.22 J mg/Kg - dry 0.950 5.861,2,4-Trichlorobenzene 4 11/27/23 16:12 V40513AMP
<0.854 mg/Kg - dry 0.854 5.862,4,5-Trichlorophenol 4 11/27/23 16:12 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 119 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-8 (0-2)
89899 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.858 mg/Kg - dry 0.858 5.862,4,6-Trichlorophenol 4 11/27/23 16:12 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 120 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-9 (0-2)
89900 Matrix:
11/20/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.0 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
0.428 mg/Kg - dry 0.180 0.256Chromium, Hexavalent 1 12/06/23 17:47 SW-7199SWB
0.867 mg/Kg - dry 0.110 0.321Arsenic 5 12/09/23 16:34 6020BBKN
129 mg/Kg - dry 0.054 0.320Barium 5 12/09/23 16:34 6020BBKN
<0.0333 mg/Kg - dry 0.0333 0.321Cadmium 5 12/09/23 16:34 6020BBKN
78.5 mg/Kg - dry 0.148 0.320Chromium 5 12/09/23 16:34 6020BBKN
4.69 mg/Kg - dry 0.0397 0.321Lead 5 12/09/23 16:34 6020BBKN
0.0574 mg/Kg - dry 0.0154 0.0385Mercury (Total)1 12/01/23 16:24 7471BJKC
0.608 mg/Kg - dry 0.132 0.320Selenium 5 12/09/23 16:34 6020BJTR
<0.0086 mg/Kg - dry 0.0086 0.321Silver 5 12/09/23 16:34 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 121 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-9 (0-2)
89900 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0023 mg/Kg - dry 0.0023 0.0064Aldrin 1 11/30/23 19:58 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.0064alpha-BHC 1 11/30/23 19:58 V40768TJW
<0.0025 mg/Kg - dry 0.0025 0.0064beta-BHC 1 11/30/23 19:58 V40768TJW
<0.0016 mg/Kg - dry 0.0016 0.0064delta-BHC 1 11/30/23 19:58 V40768TJW
<0.0225 mg/Kg - dry 0.0225 0.0641Chlordane 1 11/30/23 19:58 V40768TJW
<0.0024 mg/Kg - dry 0.0024 0.0064alpha-Chlordane 1 11/30/23 19:58 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0064gamma-Chlordane 1 11/30/23 19:58 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.00644,4'-DDD 1 11/30/23 19:58 V40768TJW
<0.0026 mg/Kg - dry 0.0026 0.00644,4'-DDE 1 11/30/23 19:58 V40768TJW
0.0061 J mg/Kg - dry 0.0019 0.00644,4'-DDT 1 11/30/23 19:58 V40768TJW
0.0266 mg/Kg - dry 0.0026 0.0064Dieldrin 1 11/30/23 19:58 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0064Endosulfan I 1 11/30/23 19:58 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0064Endosulfan II 1 11/30/23 19:58 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0064Endosulfan Sulfate 1 11/30/23 19:58 V40768TJW
<0.0024 mg/Kg - dry 0.0024 0.0064Endrin 1 11/30/23 19:58 V40768TJW
<0.0027 mg/Kg - dry 0.0027 0.0064Endrin Aldehyde 1 11/30/23 19:58 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0064Endrin Ketone 1 11/30/23 19:58 V40768TJW
<0.0016 mg/Kg - dry 0.0016 0.0064gamma-BHC 1 11/30/23 19:58 V40768TJW
<0.0017 mg/Kg - dry 0.0017 0.0064Heptachlor 1 11/30/23 19:58 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0064Heptachlor Epoxide 1 11/30/23 19:58 V40768TJW
<0.0033 mg/Kg - dry 0.0033 0.0064Methoxychlor 1 11/30/23 19:58 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 122 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-9 (0-2)
89900 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0130 mg/Kg - dry 0.0130 0.0641 1 11/30/23 19:58 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.062 mg/Kg - dry 0.003 0.025Acetone 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 11/22/23 18:26 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 11/22/23 18:26 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/22/23 18:26 V40555TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/22/23 18:26 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/22/23 18:26 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/22/23 18:26 V40555TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/22/23 18:26 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/22/23 18:26 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 123 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-9 (0-2)
89900 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/22/23 18:26 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/22/23 18:26 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/22/23 18:26 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/22/23 18:26 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 11/22/23 18:26 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/22/23 18:26 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/22/23 18:26 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/22/23 18:26 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/22/23 18:26 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 11/22/23 18:26 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/22/23 18:26 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/22/23 18:26 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 124 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-9 (0-2)
89900 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 11/22/23 18:26 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/22/23 18:26 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 11/22/23 18:26 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/22/23 18:26 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/22/23 18:26 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 11/22/23 18:26 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/22/23 18:26 V40555TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 11/22/23 18:26 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/22/23 18:26 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006 1 11/22/23 18:26 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.006 1 11/22/23 18:26 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 11/22/23 18:26 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 125 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-9 (0-2)
89900 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.006 1 11/22/23 18:26 V40555TBL
<0.002 mg/Kg - dry 0.002 0.012 1 11/22/23 18:26 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/22/23 18:26 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/22/23 18:26 V40555TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/22/23 18:26 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/22/23 18:26 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.148 mg/Kg - dry 0.148 0.846Acenaphthene 1 11/23/23 03:05 V40513AMP
<0.134 mg/Kg - dry 0.134 0.846Acenaphthylene 1 11/23/23 03:05 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 126 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-9 (0-2)
89900 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.194 mg/Kg - dry 0.194 0.846Aniline 1 11/23/23 03:05 V40513AMP
<0.183 mg/Kg - dry 0.183 0.846Anthracene 1 11/23/23 03:05 V40513AMP
<0.178 mg/Kg - dry 0.178 0.846Benzo(a)anthracene 1 11/23/23 03:05 V40513AMP
<0.188 mg/Kg - dry 0.188 0.846Benzo(a)pyrene 1 11/23/23 03:05 V40513AMP
<0.187 mg/Kg - dry 0.187 0.846Benzo(b)fluoranthene 1 11/23/23 03:05 V40513AMP
<0.174 mg/Kg - dry 0.174 0.846Benzo(g,h,i)perylene 1 11/23/23 03:05 V40513AMP
<0.175 mg/Kg - dry 0.175 0.846Benzo(k)fluoranthene 1 11/23/23 03:05 V40513AMP
<0.743 M mg/Kg - dry 0.743 2.56Benzoic Acid 1 11/23/23 03:05 V40513AMP
<0.134 mg/Kg - dry 0.134 0.846Benzyl alcohol 1 11/23/23 03:05 V40513AMP
<0.151 mg/Kg - dry 0.151 0.846Bis(2-Chloroethoxy)methane 1 11/23/23 03:05 V40513AMP
<0.137 mg/Kg - dry 0.137 0.846Bis(2-Chloroethyl)ether 1 11/23/23 03:05 V40513AMP
<0.174 mg/Kg - dry 0.174 0.423Bis(2-Chloroisopropyl)ether 1 11/23/23 03:05 V40513AMP
<0.153 mg/Kg - dry 0.153 0.846Bis(2-ethylhexyl)phthalate 1 11/23/23 03:05 V40513AMP
<0.139 mg/Kg - dry 0.139 0.8464-Bromophenyl phenyl ether 1 11/23/23 03:05 V40513AMP
<0.144 mg/Kg - dry 0.144 0.423Butyl benzyl phthalate 1 11/23/23 03:05 V40513AMP
<0.118 mg/Kg - dry 0.118 0.8464-Chloro-3-methylphenol 1 11/23/23 03:05 V40513AMP
<0.143 mg/Kg - dry 0.143 0.4234-Chloroaniline 1 11/23/23 03:05 V40513AMP
<0.148 mg/Kg - dry 0.148 0.8462-Chloronaphthalene 1 11/23/23 03:05 V40513AMP
<0.125 mg/Kg - dry 0.125 0.8462-Chlorophenol 1 11/23/23 03:05 V40513AMP
<0.161 mg/Kg - dry 0.161 1.284-Chlorophenyl phenyl ether 1 11/23/23 03:05 V40513AMP
<0.182 mg/Kg - dry 0.182 0.846Chrysene 1 11/23/23 03:05 V40513AMP
<0.294 mg/Kg - dry 0.294 0.846Dibenz(a,h)anthracene 1 11/23/23 03:05 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 127 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-9 (0-2)
89900 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.152 mg/Kg - dry 0.152 0.846Dibenzofuran 1 11/23/23 03:05 V40513AMP
<0.121 mg/Kg - dry 0.121 0.8461,2-Dichlorobenzene 1 11/23/23 03:05 V40513AMP
<0.124 mg/Kg - dry 0.124 0.8461,3-Dichlorobenzene 1 11/23/23 03:05 V40513AMP
<0.125 mg/Kg - dry 0.125 0.4231,4-Dichlorobenzene 1 11/23/23 03:05 V40513AMP
<0.188 mg/Kg - dry 0.188 0.8463,3'-Dichlorobenzidine 1 11/23/23 03:05 V40513AMP
<0.122 mg/Kg - dry 0.122 0.8462,4-Dichlorophenol 1 11/23/23 03:05 V40513AMP
<0.230 mg/Kg - dry 0.230 0.846Diethyl phthalate 1 11/23/23 03:05 V40513AMP
<0.223 mg/Kg - dry 0.223 0.846Dimethyl phthalate 1 11/23/23 03:05 V40513AMP
<0.138 mg/Kg - dry 0.138 0.4232,4-Dimethylphenol 1 11/23/23 03:05 V40513AMP
<0.137 mg/Kg - dry 0.137 0.846Di-n-butyl phthalate 1 11/23/23 03:05 V40513AMP
<0.307 mg/Kg - dry 0.307 1.924,6-Dinitro-2-methylphenol 1 11/23/23 03:05 V40513AMP
<0.666 mg/Kg - dry 0.666 1.922,4-Dinitrophenol 1 11/23/23 03:05 V40513AMP
<0.123 mg/Kg - dry 0.123 0.8462,4-Dinitrotoluene 1 11/23/23 03:05 V40513AMP
<0.138 mg/Kg - dry 0.138 0.8462,6-Dinitrotoluene 1 11/23/23 03:05 V40513AMP
<0.183 mg/Kg - dry 0.183 0.423Di-n-Octyl Phthalate 1 11/23/23 03:05 V40513AMP
<0.157 mg/Kg - dry 0.157 0.846Fluoranthene 1 11/23/23 03:05 V40513AMP
<0.164 mg/Kg - dry 0.164 0.846Fluorene 1 11/23/23 03:05 V40513AMP
<0.135 mg/Kg - dry 0.135 0.846Hexachlorobenzene 1 11/23/23 03:05 V40513AMP
<0.125 mg/Kg - dry 0.125 0.846Hexachlorobutadiene 1 11/23/23 03:05 V40513AMP
<0.201 mg/Kg - dry 0.201 0.846Hexachlorocyclopentadiene 1 11/23/23 03:05 V40513AMP
<0.101 mg/Kg - dry 0.101 0.846Hexachloroethane 1 11/23/23 03:05 V40513AMP
<0.229 mg/Kg - dry 0.229 0.846Indeno(1,2,3-cd)pyrene 1 11/23/23 03:05 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 128 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-9 (0-2)
89900 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.244 mg/Kg - dry 0.244 0.846Isophorone 1 11/23/23 03:05 V40513AMP
<0.135 mg/Kg - dry 0.135 0.8461-Methylnaphthalene 1 11/23/23 03:05 V40513AMP
<0.128 mg/Kg - dry 0.128 0.8462-Methylnaphthalene 1 11/23/23 03:05 V40513AMP
<0.124 mg/Kg - dry 0.124 0.8462-Methylphenol 1 11/23/23 03:05 V40513AMP
<0.108 mg/Kg - dry 0.108 0.8463&4 Methylphenol 1 11/23/23 03:05 V40513AMP
<0.184 mg/Kg - dry 0.184 0.846Naphthalene 1 11/23/23 03:05 V40513AMP
<0.123 mg/Kg - dry 0.123 0.8462-Nitroaniline 1 11/23/23 03:05 V40513AMP
<0.153 mg/Kg - dry 0.153 0.8463-Nitroaniline 1 11/23/23 03:05 V40513AMP
<0.119 mg/Kg - dry 0.119 0.4234-Nitroaniline 1 11/23/23 03:05 V40513AMP
<0.148 mg/Kg - dry 0.148 0.423Nitrobenzene 1 11/23/23 03:05 V40513AMP
<0.113 mg/Kg - dry 0.113 0.8462-Nitrophenol 1 11/23/23 03:05 V40513AMP
<0.150 mg/Kg - dry 0.150 0.8464-Nitrophenol 1 11/23/23 03:05 V40513AMP
<0.337 mg/Kg - dry 0.337 0.846N-Nitrosodimethylamine 1 11/23/23 03:05 V40513AMP
<0.232 mg/Kg - dry 0.232 0.846N-Nitrosodiphenylamine 1 11/23/23 03:05 V40513AMP
<0.151 mg/Kg - dry 0.151 0.846N-Nitroso-di-n-propylamine 1 11/23/23 03:05 V40513AMP
<0.444 mg/Kg - dry 0.444 1.28Pentachlorophenol 1 11/23/23 03:05 V40513AMP
<0.266 mg/Kg - dry 0.266 0.846Phenanthrene 1 11/23/23 03:05 V40513AMP
<0.143 mg/Kg - dry 0.143 0.846Phenol 1 11/23/23 03:05 V40513AMP
<0.171 mg/Kg - dry 0.171 0.846Pyrene 1 11/23/23 03:05 V40513AMP
<0.101 mg/Kg - dry 0.101 0.423Pyridine 1 11/23/23 03:05 V40513AMP
<0.137 mg/Kg - dry 0.137 0.8461,2,4-Trichlorobenzene 1 11/23/23 03:05 V40513AMP
<0.123 mg/Kg - dry 0.123 0.8462,4,5-Trichlorophenol 1 11/23/23 03:05 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 129 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-9 (0-2)
89900 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.123 mg/Kg - dry 0.123 0.8462,4,6-Trichlorophenol 1 11/23/23 03:05 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 130 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-10 (0-2)
89901 Matrix:
11/20/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
4.24 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
0.203 J mg/Kg - dry 0.147 0.208Chromium, Hexavalent 1 12/06/23 17:58 SW-7199SWB
0.424 mg/Kg - dry 0.0892 0.261Arsenic 5 12/09/23 16:47 6020BBKN
188 mg/Kg - dry 0.044 0.261Barium 5 12/09/23 16:47 6020BBKN
0.116 J mg/Kg - dry 0.0271 0.261Cadmium 5 12/09/23 16:47 6020BBKN
27.8 mg/Kg - dry 0.121 0.261Chromium 5 12/09/23 16:47 6020BBKN
3.27 mg/Kg - dry 0.0323 0.261Lead 5 12/09/23 16:47 6020BBKN
0.0134 J mg/Kg - dry 0.0125 0.0313Mercury (Total)1 12/01/23 16:26 7471BJKC
0.244 J mg/Kg - dry 0.107 0.261Selenium 5 12/09/23 16:47 6020BJTR
0.0234 J mg/Kg - dry 0.0070 0.261Silver 5 12/09/23 16:47 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 131 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-10 (0-2)
89901 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0019 mg/Kg - dry 0.0019 0.0052Aldrin 1 11/30/23 20:12 V40768TJW
<0.0012 mg/Kg - dry 0.0012 0.0052alpha-BHC 1 11/30/23 20:12 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0052beta-BHC 1 11/30/23 20:12 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0052delta-BHC 1 11/30/23 20:12 V40768TJW
<0.0183 mg/Kg - dry 0.0183 0.0522Chlordane 1 11/30/23 20:12 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0052alpha-Chlordane 1 11/30/23 20:12 V40768TJW
<0.0017 mg/Kg - dry 0.0017 0.0052gamma-Chlordane 1 11/30/23 20:12 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.00524,4'-DDD 1 11/30/23 20:12 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.00524,4'-DDE 1 11/30/23 20:12 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.00524,4'-DDT 1 11/30/23 20:12 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0052Dieldrin 1 11/30/23 20:12 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0052Endosulfan I 1 11/30/23 20:12 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0052Endosulfan II 1 11/30/23 20:12 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0052Endosulfan Sulfate 1 11/30/23 20:12 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0052Endrin 1 11/30/23 20:12 V40768TJW
<0.0022 mg/Kg - dry 0.0022 0.0052Endrin Aldehyde 1 11/30/23 20:12 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0052Endrin Ketone 1 11/30/23 20:12 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0052gamma-BHC 1 11/30/23 20:12 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0052Heptachlor 1 11/30/23 20:12 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0052Heptachlor Epoxide 1 11/30/23 20:12 V40768TJW
<0.0027 mg/Kg - dry 0.0027 0.0052Methoxychlor 1 11/30/23 20:12 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 132 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-10 (0-2)
89901 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0106 mg/Kg - dry 0.0106 0.0522 1 11/30/23 20:12 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.019 J mg/Kg - dry 0.002 0.020Acetone 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.020Acrolein 1 11/22/23 18:53 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.020Acrylonitrile 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 11/22/23 18:53 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Bromochloromethane 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Bromomethane 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 11/22/23 18:53 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/22/23 18:53 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 11/22/23 18:53 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 133 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-10 (0-2)
89901 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.005Chlorodibromomethane 1 11/22/23 18:53 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.010Chloroethane 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/22/23 18:53 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0052-Chlorotoluene 1 11/22/23 18:53 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/22/23 18:53 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/22/23 18:53 V40555TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 11/22/23 18:53 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,4-Dichlorobenzene 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 11/22/23 18:53 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/22/23 18:53 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/22/23 18:53 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005cis-1,2-Dichloroethene 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/22/23 18:53 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 134 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-10 (0-2)
89901 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/22/23 18:53 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005trans-1,3-Dichloropropene 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 11/22/23 18:53 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.052Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 18:53 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.010Hexachlorobutadiene 1 11/22/23 18:53 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0202-Hexanone 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/22/23 18:53 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.020Methyl Ethyl Ketone (MEK)1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Methyl tert-butyl ether (MTBE)1 11/22/23 18:53 V40555TBL
<0.015 mg/Kg - dry 0.015 0.0204-Methyl-2-Pentanone 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Naphthalene 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/22/23 18:53 V40555TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 11/22/23 18:53 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005 1 11/22/23 18:53 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 11/22/23 18:53 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 135 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-10 (0-2)
89901 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/22/23 18:53 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.005 1 11/22/23 18:53 V40555TBL
<0.002 mg/Kg - dry 0.002 0.010 1 11/22/23 18:53 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 11/22/23 18:53 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 11/22/23 18:53 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 11/22/23 18:53 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 11/22/23 18:53 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.121 mg/Kg - dry 0.121 0.690Acenaphthene 1 11/23/23 00:50 V40513AMP
<0.109 mg/Kg - dry 0.109 0.690Acenaphthylene 1 11/23/23 00:50 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 136 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-10 (0-2)
89901 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.158 mg/Kg - dry 0.158 0.690Aniline 1 11/23/23 00:50 V40513AMP
<0.149 mg/Kg - dry 0.149 0.690Anthracene 1 11/23/23 00:50 V40513AMP
<0.145 mg/Kg - dry 0.145 0.690Benzo(a)anthracene 1 11/23/23 00:50 V40513AMP
<0.153 mg/Kg - dry 0.153 0.690Benzo(a)pyrene 1 11/23/23 00:50 V40513AMP
<0.152 mg/Kg - dry 0.152 0.690Benzo(b)fluoranthene 1 11/23/23 00:50 V40513AMP
<0.142 mg/Kg - dry 0.142 0.690Benzo(g,h,i)perylene 1 11/23/23 00:50 V40513AMP
<0.143 mg/Kg - dry 0.143 0.690Benzo(k)fluoranthene 1 11/23/23 00:50 V40513AMP
<0.605 M mg/Kg - dry 0.605 2.09Benzoic Acid 1 11/23/23 00:50 V40513AMP
<0.109 mg/Kg - dry 0.109 0.690Benzyl alcohol 1 11/23/23 00:50 V40513AMP
<0.123 mg/Kg - dry 0.123 0.690Bis(2-Chloroethoxy)methane 1 11/23/23 00:50 V40513AMP
<0.111 mg/Kg - dry 0.111 0.690Bis(2-Chloroethyl)ether 1 11/23/23 00:50 V40513AMP
<0.142 mg/Kg - dry 0.142 0.344Bis(2-Chloroisopropyl)ether 1 11/23/23 00:50 V40513AMP
<0.125 mg/Kg - dry 0.125 0.690Bis(2-ethylhexyl)phthalate 1 11/23/23 00:50 V40513AMP
<0.113 mg/Kg - dry 0.113 0.6904-Bromophenyl phenyl ether 1 11/23/23 00:50 V40513AMP
<0.118 mg/Kg - dry 0.118 0.344Butyl benzyl phthalate 1 11/23/23 00:50 V40513AMP
<0.096 mg/Kg - dry 0.096 0.6904-Chloro-3-methylphenol 1 11/23/23 00:50 V40513AMP
<0.116 mg/Kg - dry 0.116 0.3444-Chloroaniline 1 11/23/23 00:50 V40513AMP
<0.121 mg/Kg - dry 0.121 0.6902-Chloronaphthalene 1 11/23/23 00:50 V40513AMP
<0.102 mg/Kg - dry 0.102 0.6902-Chlorophenol 1 11/23/23 00:50 V40513AMP
<0.131 mg/Kg - dry 0.131 1.044-Chlorophenyl phenyl ether 1 11/23/23 00:50 V40513AMP
<0.148 mg/Kg - dry 0.148 0.690Chrysene 1 11/23/23 00:50 V40513AMP
<0.240 mg/Kg - dry 0.240 0.690Dibenz(a,h)anthracene 1 11/23/23 00:50 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 137 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-10 (0-2)
89901 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.124 mg/Kg - dry 0.124 0.690Dibenzofuran 1 11/23/23 00:50 V40513AMP
<0.098 mg/Kg - dry 0.098 0.6901,2-Dichlorobenzene 1 11/23/23 00:50 V40513AMP
<0.101 mg/Kg - dry 0.101 0.6901,3-Dichlorobenzene 1 11/23/23 00:50 V40513AMP
<0.101 mg/Kg - dry 0.101 0.3441,4-Dichlorobenzene 1 11/23/23 00:50 V40513AMP
<0.153 mg/Kg - dry 0.153 0.6903,3'-Dichlorobenzidine 1 11/23/23 00:50 V40513AMP
<0.100 mg/Kg - dry 0.100 0.6902,4-Dichlorophenol 1 11/23/23 00:50 V40513AMP
<0.187 mg/Kg - dry 0.187 0.690Diethyl phthalate 1 11/23/23 00:50 V40513AMP
<0.181 mg/Kg - dry 0.181 0.690Dimethyl phthalate 1 11/23/23 00:50 V40513AMP
<0.112 mg/Kg - dry 0.112 0.3442,4-Dimethylphenol 1 11/23/23 00:50 V40513AMP
<0.111 mg/Kg - dry 0.111 0.690Di-n-butyl phthalate 1 11/23/23 00:50 V40513AMP
<0.250 mg/Kg - dry 0.250 1.574,6-Dinitro-2-methylphenol 1 11/23/23 00:50 V40513AMP
<0.543 mg/Kg - dry 0.543 1.572,4-Dinitrophenol 1 11/23/23 00:50 V40513AMP
<0.100 mg/Kg - dry 0.100 0.6902,4-Dinitrotoluene 1 11/23/23 00:50 V40513AMP
<0.112 mg/Kg - dry 0.112 0.6902,6-Dinitrotoluene 1 11/23/23 00:50 V40513AMP
<0.149 mg/Kg - dry 0.149 0.344Di-n-Octyl Phthalate 1 11/23/23 00:50 V40513AMP
<0.128 mg/Kg - dry 0.128 0.690Fluoranthene 1 11/23/23 00:50 V40513AMP
<0.133 mg/Kg - dry 0.133 0.690Fluorene 1 11/23/23 00:50 V40513AMP
<0.110 mg/Kg - dry 0.110 0.690Hexachlorobenzene 1 11/23/23 00:50 V40513AMP
<0.102 mg/Kg - dry 0.102 0.690Hexachlorobutadiene 1 11/23/23 00:50 V40513AMP
<0.163 mg/Kg - dry 0.163 0.690Hexachlorocyclopentadiene 1 11/23/23 00:50 V40513AMP
<0.082 mg/Kg - dry 0.082 0.690Hexachloroethane 1 11/23/23 00:50 V40513AMP
<0.186 mg/Kg - dry 0.186 0.690Indeno(1,2,3-cd)pyrene 1 11/23/23 00:50 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 138 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-10 (0-2)
89901 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.199 mg/Kg - dry 0.199 0.690Isophorone 1 11/23/23 00:50 V40513AMP
<0.110 mg/Kg - dry 0.110 0.6901-Methylnaphthalene 1 11/23/23 00:50 V40513AMP
<0.104 mg/Kg - dry 0.104 0.6902-Methylnaphthalene 1 11/23/23 00:50 V40513AMP
<0.101 mg/Kg - dry 0.101 0.6902-Methylphenol 1 11/23/23 00:50 V40513AMP
<0.088 mg/Kg - dry 0.088 0.6903&4 Methylphenol 1 11/23/23 00:50 V40513AMP
<0.150 mg/Kg - dry 0.150 0.690Naphthalene 1 11/23/23 00:50 V40513AMP
<0.101 mg/Kg - dry 0.101 0.6902-Nitroaniline 1 11/23/23 00:50 V40513AMP
<0.125 mg/Kg - dry 0.125 0.6903-Nitroaniline 1 11/23/23 00:50 V40513AMP
<0.097 mg/Kg - dry 0.097 0.3444-Nitroaniline 1 11/23/23 00:50 V40513AMP
<0.121 mg/Kg - dry 0.121 0.344Nitrobenzene 1 11/23/23 00:50 V40513AMP
<0.092 mg/Kg - dry 0.092 0.6902-Nitrophenol 1 11/23/23 00:50 V40513AMP
<0.122 mg/Kg - dry 0.122 0.6904-Nitrophenol 1 11/23/23 00:50 V40513AMP
<0.274 mg/Kg - dry 0.274 0.690N-Nitrosodimethylamine 1 11/23/23 00:50 V40513AMP
<0.189 mg/Kg - dry 0.189 0.690N-Nitrosodiphenylamine 1 11/23/23 00:50 V40513AMP
<0.123 mg/Kg - dry 0.123 0.690N-Nitroso-di-n-propylamine 1 11/23/23 00:50 V40513AMP
<0.362 mg/Kg - dry 0.362 1.04Pentachlorophenol 1 11/23/23 00:50 V40513AMP
<0.217 mg/Kg - dry 0.217 0.690Phenanthrene 1 11/23/23 00:50 V40513AMP
<0.116 mg/Kg - dry 0.116 0.690Phenol 1 11/23/23 00:50 V40513AMP
<0.139 mg/Kg - dry 0.139 0.690Pyrene 1 11/23/23 00:50 V40513AMP
<0.082 mg/Kg - dry 0.082 0.344Pyridine 1 11/23/23 00:50 V40513AMP
<0.111 mg/Kg - dry 0.111 0.6901,2,4-Trichlorobenzene 1 11/23/23 00:50 V40513AMP
<0.100 mg/Kg - dry 0.100 0.6902,4,5-Trichlorophenol 1 11/23/23 00:50 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 139 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-10 (0-2)
89901 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.100 mg/Kg - dry 0.100 0.6902,4,6-Trichlorophenol 1 11/23/23 00:50 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 140 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-11 (0-2)
89902 Matrix:
11/20/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
3.04 %Moisture 1 11/22/23 10:22 SW-DRYWTCNC
<0.145 mg/Kg - dry 0.145 0.206Chromium, Hexavalent 1 12/06/23 16:41 SW-7199SWB
0.327 mg/Kg - dry 0.0881 0.258Arsenic 5 12/09/23 16:51 6020BBKN
238 mg/Kg - dry 0.044 0.257Barium 5 12/09/23 16:51 6020BBKN
0.0698 J mg/Kg - dry 0.0268 0.258Cadmium 5 12/09/23 16:51 6020BBKN
22.4 mg/Kg - dry 0.119 0.257Chromium 5 12/09/23 16:51 6020BBKN
3.62 mg/Kg - dry 0.0319 0.258Lead 5 12/09/23 16:51 6020BBKN
<0.0124 mg/Kg - dry 0.0124 0.0309Mercury (Total)1 12/01/23 16:47 7471BJKC
0.271 mg/Kg - dry 0.106 0.257Selenium 5 12/09/23 16:51 6020BJTR
0.0215 J mg/Kg - dry 0.0069 0.258Silver 5 12/09/23 16:51 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 141 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-11 (0-2)
89902 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0018 mg/Kg - dry 0.0018 0.0051Aldrin 1 11/30/23 20:25 V40768TJW
<0.0012 mg/Kg - dry 0.0012 0.0051alpha-BHC 1 11/30/23 20:25 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0051beta-BHC 1 11/30/23 20:25 V40768TJW
<0.0012 mg/Kg - dry 0.0012 0.0051delta-BHC 1 11/30/23 20:25 V40768TJW
<0.0181 mg/Kg - dry 0.0181 0.0515Chlordane 1 11/30/23 20:25 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0051alpha-Chlordane 1 11/30/23 20:25 V40768TJW
<0.0017 mg/Kg - dry 0.0017 0.0051gamma-Chlordane 1 11/30/23 20:25 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.00514,4'-DDD 1 11/30/23 20:25 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.00514,4'-DDE 1 11/30/23 20:25 V40768TJW
<0.0015 mg/Kg - dry 0.0015 0.00514,4'-DDT 1 11/30/23 20:25 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0051Dieldrin 1 11/30/23 20:25 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0051Endosulfan I 1 11/30/23 20:25 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0051Endosulfan II 1 11/30/23 20:25 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0051Endosulfan Sulfate 1 11/30/23 20:25 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0051Endrin 1 11/30/23 20:25 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0051Endrin Aldehyde 1 11/30/23 20:25 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0051Endrin Ketone 1 11/30/23 20:25 V40768TJW
<0.0012 mg/Kg - dry 0.0012 0.0051gamma-BHC 1 11/30/23 20:25 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0051Heptachlor 1 11/30/23 20:25 V40768TJW
<0.0018 mg/Kg - dry 0.0018 0.0051Heptachlor Epoxide 1 11/30/23 20:25 V40768TJW
<0.0027 mg/Kg - dry 0.0027 0.0051Methoxychlor 1 11/30/23 20:25 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 142 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-11 (0-2)
89902 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0105 mg/Kg - dry 0.0105 0.0515 1 11/30/23 20:25 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.022 mg/Kg - dry 0.002 0.020Acetone 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.020Acrolein 1 11/22/23 19:20 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.020Acrylonitrile 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 11/22/23 19:20 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Bromochloromethane 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Bromomethane 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 11/22/23 19:20 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/22/23 19:20 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 11/22/23 19:20 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 143 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-11 (0-2)
89902 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.005Chlorodibromomethane 1 11/22/23 19:20 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.010Chloroethane 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.010Chloromethane 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0052-Chlorotoluene 1 11/22/23 19:20 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/22/23 19:20 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/22/23 19:20 V40555TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 11/22/23 19:20 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,4-Dichlorobenzene 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 11/22/23 19:20 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethane 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/22/23 19:20 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/22/23 19:20 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005cis-1,2-Dichloroethene 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/22/23 19:20 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 144 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-11 (0-2)
89902 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/22/23 19:20 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005trans-1,3-Dichloropropene 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 11/22/23 19:20 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.051Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 19:20 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.010Hexachlorobutadiene 1 11/22/23 19:20 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0202-Hexanone 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/22/23 19:20 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.020Methyl Ethyl Ketone (MEK)1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Methyl tert-butyl ether (MTBE)1 11/22/23 19:20 V40555TBL
<0.015 mg/Kg - dry 0.015 0.0204-Methyl-2-Pentanone 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010Naphthalene 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/22/23 19:20 V40555TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 11/22/23 19:20 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005 1 11/22/23 19:20 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 11/22/23 19:20 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 145 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-11 (0-2)
89902 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/22/23 19:20 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005 1 11/22/23 19:20 V40555TBL
<0.002 mg/Kg - dry 0.002 0.010 1 11/22/23 19:20 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2,3-Trichloropropane 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 11/22/23 19:20 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 11/22/23 19:20 V40555TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 11/22/23 19:20 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 11/22/23 19:20 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.119 mg/Kg - dry 0.119 0.680Acenaphthene 1 11/23/23 01:13 V40513AMP
<0.108 mg/Kg - dry 0.108 0.680Acenaphthylene 1 11/23/23 01:13 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 146 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-11 (0-2)
89902 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.156 mg/Kg - dry 0.156 0.680Aniline 1 11/23/23 01:13 V40513AMP
<0.147 mg/Kg - dry 0.147 0.680Anthracene 1 11/23/23 01:13 V40513AMP
<0.143 mg/Kg - dry 0.143 0.680Benzo(a)anthracene 1 11/23/23 01:13 V40513AMP
<0.151 mg/Kg - dry 0.151 0.680Benzo(a)pyrene 1 11/23/23 01:13 V40513AMP
<0.150 mg/Kg - dry 0.150 0.680Benzo(b)fluoranthene 1 11/23/23 01:13 V40513AMP
<0.140 mg/Kg - dry 0.140 0.680Benzo(g,h,i)perylene 1 11/23/23 01:13 V40513AMP
<0.141 mg/Kg - dry 0.141 0.680Benzo(k)fluoranthene 1 11/23/23 01:13 V40513AMP
<0.598 M mg/Kg - dry 0.598 2.06Benzoic Acid 1 11/23/23 01:13 V40513AMP
<0.108 mg/Kg - dry 0.108 0.680Benzyl alcohol 1 11/23/23 01:13 V40513AMP
<0.121 mg/Kg - dry 0.121 0.680Bis(2-Chloroethoxy)methane 1 11/23/23 01:13 V40513AMP
<0.110 mg/Kg - dry 0.110 0.680Bis(2-Chloroethyl)ether 1 11/23/23 01:13 V40513AMP
<0.140 mg/Kg - dry 0.140 0.340Bis(2-Chloroisopropyl)ether 1 11/23/23 01:13 V40513AMP
<0.123 mg/Kg - dry 0.123 0.680Bis(2-ethylhexyl)phthalate 1 11/23/23 01:13 V40513AMP
<0.112 mg/Kg - dry 0.112 0.6804-Bromophenyl phenyl ether 1 11/23/23 01:13 V40513AMP
<0.116 mg/Kg - dry 0.116 0.340Butyl benzyl phthalate 1 11/23/23 01:13 V40513AMP
<0.095 mg/Kg - dry 0.095 0.6804-Chloro-3-methylphenol 1 11/23/23 01:13 V40513AMP
<0.115 mg/Kg - dry 0.115 0.3404-Chloroaniline 1 11/23/23 01:13 V40513AMP
<0.119 mg/Kg - dry 0.119 0.6802-Chloronaphthalene 1 11/23/23 01:13 V40513AMP
<0.101 mg/Kg - dry 0.101 0.6802-Chlorophenol 1 11/23/23 01:13 V40513AMP
<0.129 mg/Kg - dry 0.129 1.034-Chlorophenyl phenyl ether 1 11/23/23 01:13 V40513AMP
<0.146 mg/Kg - dry 0.146 0.680Chrysene 1 11/23/23 01:13 V40513AMP
<0.237 mg/Kg - dry 0.237 0.680Dibenz(a,h)anthracene 1 11/23/23 01:13 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 147 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-11 (0-2)
89902 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.122 mg/Kg - dry 0.122 0.680Dibenzofuran 1 11/23/23 01:13 V40513AMP
<0.097 mg/Kg - dry 0.097 0.6801,2-Dichlorobenzene 1 11/23/23 01:13 V40513AMP
<0.100 mg/Kg - dry 0.100 0.6801,3-Dichlorobenzene 1 11/23/23 01:13 V40513AMP
<0.100 mg/Kg - dry 0.100 0.3401,4-Dichlorobenzene 1 11/23/23 01:13 V40513AMP
<0.151 mg/Kg - dry 0.151 0.6803,3'-Dichlorobenzidine 1 11/23/23 01:13 V40513AMP
<0.098 mg/Kg - dry 0.098 0.6802,4-Dichlorophenol 1 11/23/23 01:13 V40513AMP
<0.185 mg/Kg - dry 0.185 0.680Diethyl phthalate 1 11/23/23 01:13 V40513AMP
<0.179 mg/Kg - dry 0.179 0.680Dimethyl phthalate 1 11/23/23 01:13 V40513AMP
<0.111 mg/Kg - dry 0.111 0.3402,4-Dimethylphenol 1 11/23/23 01:13 V40513AMP
<0.110 mg/Kg - dry 0.110 0.680Di-n-butyl phthalate 1 11/23/23 01:13 V40513AMP
<0.247 mg/Kg - dry 0.247 1.554,6-Dinitro-2-methylphenol 1 11/23/23 01:13 V40513AMP
<0.536 mg/Kg - dry 0.536 1.552,4-Dinitrophenol 1 11/23/23 01:13 V40513AMP
<0.099 mg/Kg - dry 0.099 0.6802,4-Dinitrotoluene 1 11/23/23 01:13 V40513AMP
<0.111 mg/Kg - dry 0.111 0.6802,6-Dinitrotoluene 1 11/23/23 01:13 V40513AMP
<0.147 mg/Kg - dry 0.147 0.340Di-n-Octyl Phthalate 1 11/23/23 01:13 V40513AMP
<0.126 mg/Kg - dry 0.126 0.680Fluoranthene 1 11/23/23 01:13 V40513AMP
<0.132 mg/Kg - dry 0.132 0.680Fluorene 1 11/23/23 01:13 V40513AMP
<0.109 mg/Kg - dry 0.109 0.680Hexachlorobenzene 1 11/23/23 01:13 V40513AMP
<0.100 mg/Kg - dry 0.100 0.680Hexachlorobutadiene 1 11/23/23 01:13 V40513AMP
<0.161 mg/Kg - dry 0.161 0.680Hexachlorocyclopentadiene 1 11/23/23 01:13 V40513AMP
<0.081 mg/Kg - dry 0.081 0.680Hexachloroethane 1 11/23/23 01:13 V40513AMP
<0.184 mg/Kg - dry 0.184 0.680Indeno(1,2,3-cd)pyrene 1 11/23/23 01:13 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 148 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-11 (0-2)
89902 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.196 mg/Kg - dry 0.196 0.680Isophorone 1 11/23/23 01:13 V40513AMP
<0.109 mg/Kg - dry 0.109 0.6801-Methylnaphthalene 1 11/23/23 01:13 V40513AMP
<0.103 mg/Kg - dry 0.103 0.6802-Methylnaphthalene 1 11/23/23 01:13 V40513AMP
<0.100 mg/Kg - dry 0.100 0.6802-Methylphenol 1 11/23/23 01:13 V40513AMP
<0.087 mg/Kg - dry 0.087 0.6803&4 Methylphenol 1 11/23/23 01:13 V40513AMP
<0.148 mg/Kg - dry 0.148 0.680Naphthalene 1 11/23/23 01:13 V40513AMP
<0.099 mg/Kg - dry 0.099 0.6802-Nitroaniline 1 11/23/23 01:13 V40513AMP
<0.123 mg/Kg - dry 0.123 0.6803-Nitroaniline 1 11/23/23 01:13 V40513AMP
<0.096 mg/Kg - dry 0.096 0.3404-Nitroaniline 1 11/23/23 01:13 V40513AMP
<0.119 mg/Kg - dry 0.119 0.340Nitrobenzene 1 11/23/23 01:13 V40513AMP
<0.091 mg/Kg - dry 0.091 0.6802-Nitrophenol 1 11/23/23 01:13 V40513AMP
<0.120 mg/Kg - dry 0.120 0.6804-Nitrophenol 1 11/23/23 01:13 V40513AMP
<0.271 mg/Kg - dry 0.271 0.680N-Nitrosodimethylamine 1 11/23/23 01:13 V40513AMP
<0.186 mg/Kg - dry 0.186 0.680N-Nitrosodiphenylamine 1 11/23/23 01:13 V40513AMP
<0.121 mg/Kg - dry 0.121 0.680N-Nitroso-di-n-propylamine 1 11/23/23 01:13 V40513AMP
<0.357 mg/Kg - dry 0.357 1.03Pentachlorophenol 1 11/23/23 01:13 V40513AMP
<0.214 mg/Kg - dry 0.214 0.680Phenanthrene 1 11/23/23 01:13 V40513AMP
<0.115 mg/Kg - dry 0.115 0.680Phenol 1 11/23/23 01:13 V40513AMP
<0.138 mg/Kg - dry 0.138 0.680Pyrene 1 11/23/23 01:13 V40513AMP
<0.081 mg/Kg - dry 0.081 0.340Pyridine 1 11/23/23 01:13 V40513AMP
<0.110 mg/Kg - dry 0.110 0.6801,2,4-Trichlorobenzene 1 11/23/23 01:13 V40513AMP
<0.099 mg/Kg - dry 0.099 0.6802,4,5-Trichlorophenol 1 11/23/23 01:13 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 149 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:SB-11 (0-2)
89902 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.099 mg/Kg - dry 0.099 0.6802,4,6-Trichlorophenol 1 11/23/23 01:13 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 150 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:DUP-3
89903 Matrix:
11/20/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.11 %Moisture 1 11/27/23 12:18 SW-DRYWTCNC
<0.155 mg/Kg - dry 0.155 0.220Chromium, Hexavalent 1 12/06/23 18:08 SW-7199SWB
1.30 mg/Kg - dry 0.0940 0.275Arsenic 5 12/09/23 16:55 6020BBKN
190 mg/Kg - dry 0.047 0.275Barium 5 12/09/23 16:55 6020BBKN
2.94 mg/Kg - dry 0.0286 0.275Cadmium 5 12/09/23 16:55 6020BBKN
44.2 mg/Kg - dry 0.127 0.275Chromium 5 12/09/23 16:55 6020BBKN
51.5 mg/Kg - dry 0.0341 0.275Lead 5 12/09/23 16:55 6020BBKN
0.367 mg/Kg - dry 0.0132 0.0330Mercury (Total)1 12/01/23 16:50 7471BJKC
0.842 mg/Kg - dry 0.113 0.275Selenium 5 12/09/23 16:55 6020BJTR
0.0829 J mg/Kg - dry 0.0074 0.275Silver 5 12/09/23 16:55 6020BBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 151 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:DUP-3
89903 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0020 mg/Kg - dry 0.0020 0.0055Aldrin 1 11/30/23 20:39 V40768TJW
<0.0012 mg/Kg - dry 0.0012 0.0055alpha-BHC 1 11/30/23 20:39 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0055beta-BHC 1 11/30/23 20:39 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0055delta-BHC 1 11/30/23 20:39 V40768TJW
<0.0193 mg/Kg - dry 0.0193 0.0550Chlordane 1 11/30/23 20:39 V40768TJW
0.0660 mg/Kg - dry 0.0020 0.0055alpha-Chlordane 1 11/30/23 20:39 V40768TJW
0.0388 Q mg/Kg - dry 0.0018 0.0055gamma-Chlordane 1 11/30/23 20:39 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.00554,4'-DDD 1 11/30/23 20:39 V40768TJW
0.0390 mg/Kg - dry 0.0022 0.00554,4'-DDE 1 11/30/23 20:39 V40768TJW
0.0518 mg/Kg - dry 0.0016 0.00554,4'-DDT 1 11/30/23 20:39 V40768TJW
0.0586 mg/Kg - dry 0.0022 0.0055Dieldrin 1 11/30/23 20:39 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Endosulfan I 1 11/30/23 20:39 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Endosulfan II 1 11/30/23 20:39 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endosulfan Sulfate 1 11/30/23 20:39 V40768TJW
<0.0021 mg/Kg - dry 0.0021 0.0055Endrin 1 11/30/23 20:39 V40768TJW
<0.0023 mg/Kg - dry 0.0023 0.0055Endrin Aldehyde 1 11/30/23 20:39 V40768TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endrin Ketone 1 11/30/23 20:39 V40768TJW
<0.0013 mg/Kg - dry 0.0013 0.0055gamma-BHC 1 11/30/23 20:39 V40768TJW
<0.0014 mg/Kg - dry 0.0014 0.0055Heptachlor 1 11/30/23 20:39 V40768TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Heptachlor Epoxide 1 11/30/23 20:39 V40768TJW
<0.0029 mg/Kg - dry 0.0029 0.0055Methoxychlor 1 11/30/23 20:39 V40768TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 152 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:DUP-3
89903 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/29/23 10:10
<0.0112 mg/Kg - dry 0.0112 0.0550 1 11/30/23 20:39 V40768TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.113 mg/Kg - dry 0.002 0.022Acetone 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 11/22/23 19:48 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 11/22/23 19:48 V40555TBL
0.004 J mg/Kg - dry 0.0006 0.005Benzene 1 11/22/23 19:48 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/22/23 19:48 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/22/23 19:48 V40555TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 11/22/23 19:48 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 11/22/23 19:48 V40555TBL
0.0008 J mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/22/23 19:48 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/22/23 19:48 V40555TBL
0.005 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/22/23 19:48 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 11/22/23 19:48 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 153 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:DUP-3
89903 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 11/22/23 19:48 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/22/23 19:48 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/22/23 19:48 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/22/23 19:48 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/22/23 19:48 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/22/23 19:48 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/22/23 19:48 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 11/22/23 19:48 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/22/23 19:48 V40555TBL
0.009 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 11/22/23 19:48 V40555TBL
0.001 J mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/22/23 19:48 V40555TBL
0.004 J mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/22/23 19:48 V40555TBL
0.025 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/22/23 19:48 V40555TBL
0.002 J mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/22/23 19:48 V40555TBL
0.017 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/22/23 19:48 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/22/23 19:48 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/22/23 19:48 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 154 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:DUP-3
89903 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 11/22/23 19:48 V40555TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/22/23 19:48 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/22/23 19:48 V40555TBL
0.021 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 11/22/23 19:48 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 11/22/23 19:48 V40555TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/22/23 19:48 V40555TBL
0.018 mg/Kg - dry 0.0007 0.011n-Hexane 1 11/22/23 19:48 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 11/22/23 19:48 V40555TBL
0.012 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/22/23 19:48 V40555TBL
0.004 J mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/22/23 19:48 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 11/22/23 19:48 V40555TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/22/23 19:48 V40555TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/22/23 19:48 V40555TBL
0.012 mg/Kg - dry 0.001 0.011Naphthalene 1 11/22/23 19:48 V40555TBL
0.001 J mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/22/23 19:48 V40555TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/22/23 19:48 V40555TBL
<0.0010 mg/Kg - dry 0.0010 0.005 1 11/22/23 19:48 V40555TBL
0.015 mg/Kg - dry 0.0007 0.005 1 11/22/23 19:48 V40555TBL
0.002 J mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/22/23 19:48 V40555TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 155 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:DUP-3
89903 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/22/23 08:00
0.020 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/22/23 19:48 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/22/23 19:48 V40555TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/22/23 19:48 V40555TBL
<0.002 mg/Kg - dry 0.002 0.011 1 11/22/23 19:48 V40555TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/22/23 19:48 V40555TBL
0.010 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 11/22/23 19:48 V40555TBL
0.007 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/22/23 19:48 V40555TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/22/23 19:48 V40555TBL
0.003 J mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 11/22/23 19:48 V40555TBL
0.030 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/22/23 19:48 V40555TBL
0.129 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/22/23 19:48 V40555TBL
0.159 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/22/23 19:48 V40555
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.510 mg/Kg - dry 0.510 2.90Acenaphthene 4 11/27/23 16:34 V40513AMP
<0.462 mg/Kg - dry 0.462 2.90Acenaphthylene 4 11/27/23 16:34 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 156 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:DUP-3
89903 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.668 mg/Kg - dry 0.668 2.90Aniline 4 11/27/23 16:34 V40513AMP
<0.629 mg/Kg - dry 0.629 2.90Anthracene 4 11/27/23 16:34 V40513AMP
0.707 J mg/Kg - dry 0.611 2.90Benzo(a)anthracene 4 11/27/23 16:34 V40513AMP
0.717 J mg/Kg - dry 0.646 2.90Benzo(a)pyrene 4 11/27/23 16:34 V40513AMP
0.905 J mg/Kg - dry 0.642 2.90Benzo(b)fluoranthene 4 11/27/23 16:34 V40513AMP
<0.598 mg/Kg - dry 0.598 2.90Benzo(g,h,i)perylene 4 11/27/23 16:34 V40513AMP
<0.602 mg/Kg - dry 0.602 2.90Benzo(k)fluoranthene 4 11/27/23 16:34 V40513AMP
<2.55 M mg/Kg - dry 2.55 8.81Benzoic Acid 4 11/27/23 16:34 V40513AMP
<0.462 mg/Kg - dry 0.462 2.90Benzyl alcohol 4 11/27/23 16:34 V40513AMP
<0.519 mg/Kg - dry 0.519 2.90Bis(2-Chloroethoxy)methane 4 11/27/23 16:34 V40513AMP
<0.470 mg/Kg - dry 0.470 2.90Bis(2-Chloroethyl)ether 4 11/27/23 16:34 V40513AMP
<0.598 mg/Kg - dry 0.598 1.45Bis(2-Chloroisopropyl)ether 4 11/27/23 16:34 V40513AMP
2.88 J mg/Kg - dry 0.528 2.90Bis(2-ethylhexyl)phthalate 4 11/27/23 16:34 V40513AMP
<0.479 mg/Kg - dry 0.479 2.904-Bromophenyl phenyl ether 4 11/27/23 16:34 V40513AMP
<0.497 mg/Kg - dry 0.497 1.45Butyl benzyl phthalate 4 11/27/23 16:34 V40513AMP
<0.407 mg/Kg - dry 0.407 2.904-Chloro-3-methylphenol 4 11/27/23 16:34 V40513AMP
<0.492 mg/Kg - dry 0.492 1.454-Chloroaniline 4 11/27/23 16:34 V40513AMP
<0.510 mg/Kg - dry 0.510 2.902-Chloronaphthalene 4 11/27/23 16:34 V40513AMP
<0.432 mg/Kg - dry 0.432 2.902-Chlorophenol 4 11/27/23 16:34 V40513AMP
<0.555 mg/Kg - dry 0.555 4.414-Chlorophenyl phenyl ether 4 11/27/23 16:34 V40513AMP
0.695 J mg/Kg - dry 0.624 2.90Chrysene 4 11/27/23 16:34 V40513AMP
<1.01 mg/Kg - dry 1.01 2.90Dibenz(a,h)anthracene 4 11/27/23 16:34 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 157 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:DUP-3
89903 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.523 mg/Kg - dry 0.523 2.90Dibenzofuran 4 11/27/23 16:34 V40513AMP
<0.415 mg/Kg - dry 0.415 2.901,2-Dichlorobenzene 4 11/27/23 16:34 V40513AMP
<0.427 mg/Kg - dry 0.427 2.901,3-Dichlorobenzene 4 11/27/23 16:34 V40513AMP
<0.429 mg/Kg - dry 0.429 1.451,4-Dichlorobenzene 4 11/27/23 16:34 V40513AMP
<0.646 mg/Kg - dry 0.646 2.903,3'-Dichlorobenzidine 4 11/27/23 16:34 V40513AMP
<0.421 mg/Kg - dry 0.421 2.902,4-Dichlorophenol 4 11/27/23 16:34 V40513AMP
<0.792 mg/Kg - dry 0.792 2.90Diethyl phthalate 4 11/27/23 16:34 V40513AMP
<0.765 mg/Kg - dry 0.765 2.90Dimethyl phthalate 4 11/27/23 16:34 V40513AMP
<0.475 mg/Kg - dry 0.475 1.452,4-Dimethylphenol 4 11/27/23 16:34 V40513AMP
1.85 J mg/Kg - dry 0.470 2.90Di-n-butyl phthalate 4 11/27/23 16:34 V40513AMP
<1.06 mg/Kg - dry 1.06 6.614,6-Dinitro-2-methylphenol 4 11/27/23 16:34 V40513AMP
<2.29 mg/Kg - dry 2.29 6.612,4-Dinitrophenol 4 11/27/23 16:34 V40513AMP
<0.424 mg/Kg - dry 0.424 2.902,4-Dinitrotoluene 4 11/27/23 16:34 V40513AMP
<0.475 mg/Kg - dry 0.475 2.902,6-Dinitrotoluene 4 11/27/23 16:34 V40513AMP
<0.629 mg/Kg - dry 0.629 1.45Di-n-Octyl Phthalate 4 11/27/23 16:34 V40513AMP
1.46 J mg/Kg - dry 0.541 2.90Fluoranthene 4 11/27/23 16:34 V40513AMP
<0.563 mg/Kg - dry 0.563 2.90Fluorene 4 11/27/23 16:34 V40513AMP
<0.466 mg/Kg - dry 0.466 2.90Hexachlorobenzene 4 11/27/23 16:34 V40513AMP
<0.429 mg/Kg - dry 0.429 2.90Hexachlorobutadiene 4 11/27/23 16:34 V40513AMP
<0.690 mg/Kg - dry 0.690 2.90Hexachlorocyclopentadiene 4 11/27/23 16:34 V40513AMP
<0.348 mg/Kg - dry 0.348 2.90Hexachloroethane 4 11/27/23 16:34 V40513AMP
<0.787 mg/Kg - dry 0.787 2.90Indeno(1,2,3-cd)pyrene 4 11/27/23 16:34 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 158 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:DUP-3
89903 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.840 mg/Kg - dry 0.840 2.90Isophorone 4 11/27/23 16:34 V40513AMP
0.474 J mg/Kg - dry 0.466 2.901-Methylnaphthalene 4 11/27/23 16:34 V40513AMP
1.08 J mg/Kg - dry 0.440 2.902-Methylnaphthalene 4 11/27/23 16:34 V40513AMP
<0.426 mg/Kg - dry 0.426 2.902-Methylphenol 4 11/27/23 16:34 V40513AMP
<0.374 mg/Kg - dry 0.374 2.903&4 Methylphenol 4 11/27/23 16:34 V40513AMP
<0.633 mg/Kg - dry 0.633 2.90Naphthalene 4 11/27/23 16:34 V40513AMP
<0.425 mg/Kg - dry 0.425 2.902-Nitroaniline 4 11/27/23 16:34 V40513AMP
<0.528 mg/Kg - dry 0.528 2.903-Nitroaniline 4 11/27/23 16:34 V40513AMP
<0.410 mg/Kg - dry 0.410 1.454-Nitroaniline 4 11/27/23 16:34 V40513AMP
<0.510 mg/Kg - dry 0.510 1.45Nitrobenzene 4 11/27/23 16:34 V40513AMP
<0.390 mg/Kg - dry 0.390 2.902-Nitrophenol 4 11/27/23 16:34 V40513AMP
<0.514 mg/Kg - dry 0.514 2.904-Nitrophenol 4 11/27/23 16:34 V40513AMP
<1.16 mg/Kg - dry 1.16 2.90N-Nitrosodimethylamine 4 11/27/23 16:34 V40513AMP
<0.796 mg/Kg - dry 0.796 2.90N-Nitrosodiphenylamine 4 11/27/23 16:34 V40513AMP
<0.519 mg/Kg - dry 0.519 2.90N-Nitroso-di-n-propylamine 4 11/27/23 16:34 V40513AMP
<1.53 mg/Kg - dry 1.53 4.41Pentachlorophenol 4 11/27/23 16:34 V40513AMP
1.11 J mg/Kg - dry 0.915 2.90Phenanthrene 4 11/27/23 16:34 V40513AMP
<0.492 mg/Kg - dry 0.492 2.90Phenol 4 11/27/23 16:34 V40513AMP
1.33 J mg/Kg - dry 0.589 2.90Pyrene 4 11/27/23 16:34 V40513AMP
<0.348 mg/Kg - dry 0.348 1.45Pyridine 4 11/27/23 16:34 V40513AMP
1.17 J mg/Kg - dry 0.470 2.901,2,4-Trichlorobenzene 4 11/27/23 16:34 V40513AMP
<0.423 mg/Kg - dry 0.423 2.902,4,5-Trichlorophenol 4 11/27/23 16:34 V40513AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 159 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:DUP-3
89903 Matrix:
11/20/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/22/23 09:40
<0.424 mg/Kg - dry 0.424 2.902,4,6-Trichlorophenol 4 11/27/23 16:34 V40513AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 160 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89904 Matrix:
11/20/2023 8:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/30/23 09:00
<1.80 µg/L 1.80 5.00Acetone 1 11/30/23 16:27 V40819MSA
<2.00 M µg/L 2.00 5.00Acrolein 1 11/30/23 16:27 V40819MSA
<0.230 M µg/L 0.230 5.00Acrylonitrile 1 11/30/23 16:27 V40819MSA
<0.180 µg/L 0.180 0.500Benzene 1 11/30/23 16:27 V40819MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/30/23 16:27 V40819MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/30/23 16:27 V40819MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/30/23 16:27 V40819MSA
<1.50 µg/L 1.50 5.00Bromoform 1 11/30/23 16:27 V40819MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 11/30/23 16:27 V40819MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 11/30/23 16:27 V40819MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 11/30/23 16:27 V40819MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/30/23 16:27 V40819MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 11/30/23 16:27 V40819MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/30/23 16:27 V40819MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/30/23 16:27 V40819MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/30/23 16:27 V40819MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 11/30/23 16:27 V40819MSA
<0.220 µg/L 0.220 0.500Chloroform 1 11/30/23 16:27 V40819MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 11/30/23 16:27 V40819MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/30/23 16:27 V40819MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/30/23 16:27 V40819MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 11/30/23 16:27 V40819MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 161 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89904 Matrix:
11/20/2023 8:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/30/23 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/30/23 16:27 V40819MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/30/23 16:27 V40819MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/30/23 16:27 V40819MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/30/23 16:27 V40819MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/30/23 16:27 V40819MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/30/23 16:27 V40819MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/30/23 16:27 V40819MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/30/23 16:27 V40819MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/30/23 16:27 V40819MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/30/23 16:27 V40819MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/30/23 16:27 V40819MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 11/30/23 16:27 V40819MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/30/23 16:27 V40819MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/30/23 16:27 V40819MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/30/23 16:27 V40819MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/30/23 16:27 V40819MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/30/23 16:27 V40819MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/30/23 16:27 V40819MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/30/23 16:27 V40819MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 11/30/23 16:27 V40819MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 11/30/23 16:27 V40819MSA
<1.30 µg/L 1.30 10.0n-Hexane 1 11/30/23 16:27 V40819MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 162 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89904 Matrix:
11/20/2023 8:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/30/23 09:00
<0.380 µg/L 0.380 5.002-Hexanone 1 11/30/23 16:27 V40819MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 11/30/23 16:27 V40819MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/30/23 16:27 V40819MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/30/23 16:27 V40819MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 11/30/23 16:27 V40819MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 11/30/23 16:27 V40819MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 11/30/23 16:27 V40819MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 11/30/23 16:27 V40819MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/30/23 16:27 V40819MSA
<0.220 µg/L 0.220 0.500Styrene 1 11/30/23 16:27 V40819MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/30/23 16:27 V40819MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/30/23 16:27 V40819MSA
<0.220 µg/L 0.220 0.500 1 11/30/23 16:27 V40819MSA
<0.220 µg/L 0.220 0.500 1 11/30/23 16:27 V40819MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 11/30/23 16:27 V40819MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 11/30/23 16:27 V40819MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/30/23 16:27 V40819MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/30/23 16:27 V40819MSA
<0.180 µg/L 0.180 0.500 1 11/30/23 16:27 V40819MSA
<0.180 µg/L 0.180 0.500 1 11/30/23 16:27 V40819MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 11/30/23 16:27 V40819MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/30/23 16:27 V40819MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 163 of 208
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-325-0008
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Raleigh
Received : 11/21/2023
Former Winston Container
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89904 Matrix:
11/20/2023 8:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/30/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/30/23 16:27 V40819MSA
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 11/30/23 16:27 V40819MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/30/23 16:27 V40819MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 11/30/23 16:27 V40819MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/30/23 16:27 V40819MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/30/23 16:27 V40819
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: 1,2-Dichloroethane - d4
Surrogate: Toluene-d8
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
RPD >40% dual column resultsQ
Page 164 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Metals Analyses
6020B
L721715,L721903,L722026QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L719373
Associated Lab Samples: 89889, 89891, 89892, 89893, 89894, 89895, 89896, 89897, 89898
LRB-L719373 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/09/23 14:200.2500.0855<0.0855mg/KgArsenic
12/09/23 14:200.2500.042<0.042mg/KgBarium
12/09/23 14:200.2500.0260<0.0260mg/KgCadmium
12/11/23 23:060.2500.116<0.116mg/KgChromium
12/09/23 14:200.2500.0310<0.0310mg/KgLead
12/09/23 14:200.2500.103<0.103mg/KgSelenium
12/09/23 14:200.2500.0067<0.0067mg/KgSilver
LCS-L719373Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
91.02.272.50mg/KgArsenic 80-120
83.04.165.00mg/KgBarium 80-120
86.00.4300.500mg/KgCadmium 80-120
91.04.575.00mg/KgChromium 80-120
92.02.312.50mg/KgLead 80-120
92.04.595.00mg/KgSelenium 80-120
87.00.4330.500mg/KgSilver 80-120
V 89898-MS-L719373 V 89898-MSD-L719373Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2.52 61.0*2.392.492.391.05mg/KgArsenic 54.0*75-125 5.2 80
93.2 458*78.44.974.7871.3mg/KgBarium 143*75-125 17.2 80
0.604 1040.5560.4970.4780.108mg/KgCadmium 90.0 75-125 8.2 80
58.2 370*51.74.974.7840.5mg/KgChromium 225*75-125 11.8 80
Page 1 of 41* QC Fail Date:12/12/2023 02:36 PM
Page 165 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Metals Analyses
6020B
L721715,L721903,L722026QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L719373
V 89898-MS-L719373 V 89898-MSD-L719373Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
21.8 163*19.32.492.3917.9mg/KgLead 56.0*75-125 12.1 80
3.36 63.0*3.344.974.780.368mg/KgSelenium 60.0*75-125 0.5 80
0.495 93.00.4990.4970.4780.0491mg/KgSilver 91.0 75-125 0.8 80
V 89898-PDS-L719373Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/09/23 16:1499.01.33mg/KgArsenic
12/09/23 16:1497.09.31mg/KgBarium
12/09/23 16:141020.265mg/KgCadmium
12/09/23 16:141006.52mg/KgChromium
12/09/23 16:141003.04mg/KgLead
12/09/23 16:141002.53mg/KgSelenium
12/09/23 16:141020.257mg/KgSilver
Page 2 of 41* QC Fail Date:12/12/2023 02:36 PM
Page 166 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Metals Analyses
6020B
L721715,L722026QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L719374
Associated Lab Samples: 89899, 89900, 89901, 89902, 89903
LRB-L719374 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/09/23 16:220.2500.0855<0.0855mg/KgArsenic
12/09/23 16:220.2500.042<0.042mg/KgBarium
12/09/23 16:220.2500.0260<0.0260mg/KgCadmium
12/09/23 16:220.2500.116<0.116mg/KgChromium
12/09/23 16:220.2500.0310<0.0310mg/KgLead
12/09/23 16:220.2500.103<0.103mg/KgSelenium
12/09/23 16:220.2500.0067<0.0067mg/KgSilver
LCS-L719374Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
90.02.252.50mg/KgArsenic 80-120
91.04.575.00mg/KgBarium 80-120
91.00.4570.500mg/KgCadmium 80-120
88.04.405.00mg/KgChromium 80-120
92.02.292.50mg/KgLead 80-120
90.04.525.00mg/KgSelenium 80-120
96.00.4790.500mg/KgSilver 80-120
L 94846-MS-L719374 L 94846-MSD-L719374Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
11.8 233*7.392.432.446.12mg/KgArsenic 52.0*75-125 45.9 80
79.2 334*66.34.854.8762.9mg/KgBarium 70.0*75-125 17.7 80
0.525 95.00.5040.4850.4870.0630mg/KgCadmium 91.0 75-125 4.0 80
12.3 91.012.64.854.877.87mg/KgChromium 97.0 75-125 2.4 80
Page 3 of 41* QC Fail Date:12/12/2023 02:36 PM
Page 167 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Metals Analyses
6020B
L721715,L722026QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L719374
L 94846-MS-L719374 L 94846-MSD-L719374Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
5.82 85.05.492.432.443.74mg/KgLead 72.0*75-125 5.8 80
4.43 85.04.144.854.870.273mg/KgSelenium 80.0 75-125 6.7 80
0.458 88.00.4650.4850.4870.0273mg/KgSilver 90.0 75-125 1.5 80
L 94846-PDS-L719374Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/09/23 18:2599.01.76mg/KgArsenic
12/09/23 18:251018.69mg/KgBarium
12/09/23 18:251010.243mg/KgCadmium
12/09/23 18:2597.03.03mg/KgChromium
12/09/23 18:2595.01.47mg/KgLead
12/09/23 18:2599.02.35mg/KgSelenium
12/09/23 18:251010.240mg/KgSilver
Page 4 of 41* QC Fail Date:12/12/2023 02:36 PM
Page 168 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V40759QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V40714
Associated Lab Samples: 89889, 89891, 89892, 89893, 89894, 89895, 89896, 89897, 89898, 89899
LRB-V40714 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/30/23 16:030.03000.0120<0.0120mg/KgMercury (Total)
LCS-V40714Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
99.00.4110.417mg/KgMercury (Total)80-120
V 89999-MS-V40714 V 89999-MSD-V40714Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.532 1190.4470.4100.4030.0504mg/KgMercury (Total)97.0 80-120 17.3 20
V 89999-PDS-V40714Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
11/30/23 16:1198.00.229mg/KgMercury (Total)
Page 5 of 41Date:12/12/2023 02:36 PM
Page 169 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V40797QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V40757
Associated Lab Samples: 89900, 89901, 89902, 89903
LRB-V40757 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/01/23 16:130.03000.0120<0.0120mg/KgMercury (Total)
LCS-V40757Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1040.4340.417mg/KgMercury (Total)80-120
V 89901-MS-V40757 V 89901-MSD-V40757Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.476 1140.4260.4170.4170.0128mg/KgMercury (Total)102 80-120 11.0 20
V 89901-PDS-V40757Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/01/23 16:291010.210mg/KgMercury (Total)
Page 6 of 41Date:12/12/2023 02:36 PM
Page 170 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Organochlorine Pesticides by GC
8081B
V40768QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40673
Associated Lab Samples: 89889, 89891, 89892, 89893, 89894, 89895, 89896, 89897, 89898, 89899, 89900, 89901, 89902, 89903
LRB-V40673 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/30/23 16:240.00500.0018<0.0018mg/KgAldrin
11/30/23 16:240.00500.0011<0.0011mg/Kgalpha-BHC
11/30/23 16:240.00500.0019<0.0019mg/Kgbeta-BHC
11/30/23 16:240.00500.0012<0.0012mg/Kgdelta-BHC
11/30/23 16:240.05000.0176<0.0176mg/KgChlordane
11/30/23 16:240.00500.0018<0.0018mg/Kgalpha-Chlordane
11/30/23 16:240.00500.0016<0.0016mg/Kggamma-Chlordane
11/30/23 16:240.00500.0018<0.0018mg/Kg4,4'-DDD
11/30/23 16:240.00500.0020<0.0020mg/Kg4,4'-DDE
11/30/23 16:240.00500.0015<0.0015mg/Kg4,4'-DDT
11/30/23 16:240.00500.0020<0.0020mg/KgDieldrin
11/30/23 16:240.00500.0017<0.0017mg/KgEndosulfan I
11/30/23 16:240.00500.0017<0.0017mg/KgEndosulfan II
11/30/23 16:240.00500.0018<0.0018mg/KgEndosulfan Sulfate
11/30/23 16:240.00500.0019<0.0019mg/KgEndrin
11/30/23 16:240.00500.0021<0.0021mg/KgEndrin Aldehyde
11/30/23 16:240.00500.0018<0.0018mg/KgEndrin Ketone
11/30/23 16:240.00500.0012<0.0012mg/Kggamma-BHC
11/30/23 16:240.00500.0013<0.0013mg/KgHeptachlor
11/30/23 16:240.00500.0017<0.0017mg/KgHeptachlor Epoxide
11/30/23 16:240.00500.0026<0.0026mg/KgMethoxychlor
11/30/23 16:240.05000.0102<0.0102mg/Kg
11/30/23 16:24Decachlorobiphenyl (S)126 26-204
11/30/23 16:24 96.0 40-162
Page 7 of 41Date:12/12/2023 02:36 PM
Page 171 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Organochlorine Pesticides by GC
8081B
V40768QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40673
LCS-V40673Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1090.03620.0333mg/KgAldrin 45-136
1250.04160.0333mg/Kgalpha-BHC 45-137
1070.03560.0333mg/Kgbeta-BHC 50-136
94.80.03160.0333mg/Kgdelta-BHC 47-139
1030.3440.333mg/KgChlordane 43-149
1180.03920.0333mg/Kgalpha-Chlordane 54-133
1130.03770.0333mg/Kggamma-Chlordane 53-135
1200.03980.0333mg/Kg4,4'-DDD 56-139
1260.04200.0333mg/Kg4,4'-DDE 56-134
1250.04170.0333mg/Kg4,4'-DDT 50-145
1180.03940.0333mg/KgDieldrin 56-136
1200.04000.0333mg/KgEndosulfan I 53-132
1170.03910.0333mg/KgEndosulfan II 53-134
1110.03690.0333mg/KgEndosulfan Sulfate 55-136
1170.03910.0333mg/KgEndrin 57-140
1040.03460.0333mg/KgEndrin Aldehyde 35-137
1200.04000.0333mg/KgEndrin Ketone 55-136
1190.03960.0333mg/Kggamma-BHC 49-135
1150.03820.0333mg/KgHeptachlor 47-136
1170.03890.0333mg/KgHeptachlor Epoxide 52-136
1180.03930.0333mg/KgMethoxychlor 52-143
1090.3640.333mg/Kg 33-141
123Decachlorobiphenyl (S)26-204
97.5 40-162
Page 8 of 41Date:12/12/2023 02:36 PM
Page 172 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Organochlorine Pesticides by GC
8081B
V40768QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40673
V 89889-MS-V40673 V 89889-MSD-V40673Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.0296 88.80.02230.03330.0333<0.0018mg/KgAldrin 66.9 45-136 28.1 29
0.0318 95.40.02560.03330.0333<0.0011mg/Kgalpha-BHC 76.8 45-137 21.6 24
0.0239 71.70.02000.03330.0333<0.0019mg/Kgbeta-BHC 60.0 50-136 17.7*17
0.0211 63.30.01670.03330.0333<0.0012mg/Kgdelta-BHC 50.1 47-139 23.2*18
0.0319 95.70.02270.03330.0333<0.0018mg/Kgalpha-Chlordane 68.1 54-133 33.6*25
0.0349 1050.02570.03330.0333<0.0016mg/Kggamma-Chlordane 77.1 53-135 30.3*27
0.0248 74.40.01980.03330.0333<0.0018mg/Kg4,4'-DDD 59.4 56-139 22.4 29
0.0381 84.00.02760.03330.03330.0101mg/Kg4,4'-DDE 52.5*56-134 31.9 36
0.0451 59.40.03660.03330.03330.0253mg/Kg4,4'-DDT 33.9*50-145 20.8 38
0.0509 19.2*0.03840.03330.03330.0445mg/KgDieldrin 0.0*56-136 27.9 30
0.0286 85.80.02010.03330.0333<0.0017mg/KgEndosulfan I 60.3 53-132 34.9*32
0.0350 1050.03080.03330.0333<0.0017mg/KgEndosulfan II 92.4 53-134 12.7 20
0.0263 78.90.02690.03330.0333<0.0018mg/KgEndosulfan Sulfate 80.7 55-136 2.2 24
0.0394 78.00.03410.03330.03330.0134mg/KgEndrin 62.1 57-140 14.4 21
0.0205 43.40.01590.03330.03330.0060mg/KgEndrin Aldehyde 29.6*35-137 25.2 35
0.0268 80.40.02320.03330.0333<0.0018mg/KgEndrin Ketone 69.6 55-136 14.4 18
0.0323 96.90.02580.03330.0333<0.0012mg/Kggamma-BHC 77.4 49-135 22.3*22
0.0288 86.40.01990.03330.03330.0014mg/KgHeptachlor 59.7 47-136 36.5*27
0.0488 73.20.03880.03330.03330.0244mg/KgHeptachlor Epoxide 43.2*52-136 22.8*18
0.0235 70.50.01510.03330.0333<0.0026mg/KgMethoxychlor 45.3*52-143 43.5*30
45.6Decachlorobiphenyl (S)35.1 26-204
79.2 68.4 40-162
Page 9 of 41* QC Fail Date:12/12/2023 02:36 PM
Page 173 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40555QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40553
Associated Lab Samples: 89888, 89890, 89892, 89893, 89894, 89895, 89896, 89897, 89900, 89901, 89902, 89903
LRB-V40553 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/22/23 14:210.0200.002<0.002mg/KgAcetone
11/22/23 14:210.0200.001<0.001mg/KgAcrolein
11/22/23 14:210.0200.0008<0.0008mg/KgAcrylonitrile
11/22/23 14:210.0050.0006<0.0006mg/KgBenzene
11/22/23 14:210.0050.0005<0.0005mg/KgBromobenzene
11/22/23 14:210.0050.0008<0.0008mg/KgBromochloromethane
11/22/23 14:210.0050.001<0.001mg/KgBromodichloromethane
11/22/23 14:210.0050.001<0.001mg/KgBromoform
11/22/23 14:210.0100.001<0.001mg/KgBromomethane
11/22/23 14:210.0050.0005<0.0005mg/Kgn-Butylbenzene
11/22/23 14:210.0050.0006<0.0006mg/Kgsec-Butyl benzene
11/22/23 14:210.0050.0005<0.0005mg/Kgtert-Butyl benzene
11/22/23 14:210.0050.0006<0.0006mg/KgCarbon Disulfide
11/22/23 14:210.0050.001<0.001mg/KgCarbon Tetrachloride
11/22/23 14:210.0050.0007<0.0007mg/KgChlorobenzene
11/22/23 14:210.0050.0009<0.0009mg/KgChlorodibromomethane
11/22/23 14:210.0100.0009<0.0009mg/KgChloroethane
11/22/23 14:210.0050.001<0.001mg/KgChloroform
11/22/23 14:210.0100.0006<0.0006mg/KgChloromethane
11/22/23 14:210.0050.0005<0.0005mg/Kg2-Chlorotoluene
11/22/23 14:210.0050.0004<0.0004mg/Kg4-Chlorotoluene
11/22/23 14:210.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
11/22/23 14:210.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
11/22/23 14:210.0050.0006<0.0006mg/Kg1,2-Dibromoethane
11/22/23 14:210.0050.0006<0.0006mg/KgDibromomethane
11/22/23 14:210.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
11/22/23 14:210.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 10 of 41Date:12/12/2023 02:36 PM
Page 174 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40555QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40553
Associated Lab Samples: 89888, 89890, 89892, 89893, 89894, 89895, 89896, 89897, 89900, 89901, 89902, 89903
LRB-V40553 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/22/23 14:210.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
11/22/23 14:210.0100.001<0.001mg/KgDichlorodifluoromethane
11/22/23 14:210.0050.0008<0.0008mg/Kg1,1-Dichloroethane
11/22/23 14:210.0050.001<0.001mg/Kg1,2-Dichloroethane
11/22/23 14:210.0050.0007<0.0007mg/Kg1,1-Dichloroethene
11/22/23 14:210.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
11/22/23 14:210.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
11/22/23 14:210.0050.0004<0.0004mg/Kg1,2-Dichloropropane
11/22/23 14:210.0050.0006<0.0006mg/Kg1,3-Dichloropropane
11/22/23 14:210.0050.001<0.001mg/Kg2,2-Dichloropropane
11/22/23 14:210.0050.0008<0.0008mg/Kg1,1-Dichloropropene
11/22/23 14:210.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
11/22/23 14:210.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
11/22/23 14:210.0050.0006<0.0006mg/KgEthylbenzene
11/22/23 14:210.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
11/22/23 14:210.0100.0008<0.0008mg/KgHexachlorobutadiene
11/22/23 14:210.0100.0007<0.0007mg/Kgn-Hexane
11/22/23 14:210.0200.0006<0.0006mg/Kg2-Hexanone
11/22/23 14:210.0050.0005<0.0005mg/KgIsopropylbenzene
11/22/23 14:210.0050.001<0.001mg/Kg4-Isopropyl toluene
11/22/23 14:210.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
11/22/23 14:210.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
11/22/23 14:210.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
11/22/23 14:210.0100.001<0.001mg/KgMethylene Chloride
11/22/23 14:210.0100.0010<0.0010mg/KgNaphthalene
11/22/23 14:210.0050.0005<0.0005mg/Kgn-Propylbenzene
11/22/23 14:210.0050.001<0.001mg/KgStyrene
Page 11 of 41Date:12/12/2023 02:36 PM
Page 175 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40555QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40553
Associated Lab Samples: 89888, 89890, 89892, 89893, 89894, 89895, 89896, 89897, 89900, 89901, 89902, 89903
LRB-V40553 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/22/23 14:210.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
11/22/23 14:210.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
11/22/23 14:210.0050.0009<0.0009mg/Kg
11/22/23 14:210.0050.0007<0.0007mg/Kg
11/22/23 14:210.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
11/22/23 14:210.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
11/22/23 14:210.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/22/23 14:210.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
11/22/23 14:210.0050.0009<0.0009mg/Kg
11/22/23 14:210.0100.002<0.002mg/Kg
11/22/23 14:210.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
11/22/23 14:210.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
11/22/23 14:210.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
11/22/23 14:210.0100.0005<0.0005mg/KgVinyl Acetate
11/22/23 14:210.0100.0005<0.0005mg/KgVinyl Chloride
11/22/23 14:210.0050.0005<0.0005mg/Kgo-Xylene
11/22/23 14:210.0100.001<0.001mg/Kgm,p-Xylene
11/22/23 14:214-Bromofluorobenzene (S)99.4 70-130
11/22/23 14:21Dibromofluoromethane (S)108 84-123
11/22/23 14:21 98.8 76-129
LCS-V40553 LCSD-V40553Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.088 88.591.60.0910.100mg/KgAcetone 29-198 3.4 20
0.103 1031080.1080.100mg/KgAcrolein 70-130 4.7 20
Page 12 of 41Date:12/12/2023 02:36 PM
Page 176 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40555QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40553
LCS-V40553 LCSD-V40553Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.097 97.81020.1020.100mg/KgAcrylonitrile 65-134 4.2 20
0.045 91.895.00.0470.050mg/KgBenzene 74-127 3.4 20
0.046 92.092.60.0460.050mg/KgBromobenzene 73-125 0.6 20
0.050 1011030.0510.050mg/KgBromochloromethane 72-134 1.7 20
0.051 1031050.0520.050mg/KgBromodichloromethane 75-122 1.9 20
0.049 98.498.40.0490.050mg/KgBromoform 66-135 0.0 20
0.043 86.086.00.0430.050mg/KgBromomethane 20-180 0.0 20
0.046 93.298.40.0490.050mg/Kgn-Butylbenzene 65-135 5.4 20
0.044 88.892.60.0460.050mg/Kgsec-Butyl benzene 66-131 4.1 20
0.045 91.493.80.0460.050mg/Kgtert-Butyl benzene 67-132 2.5 20
0.042 84.291.60.0450.050mg/KgCarbon Disulfide 61-129 8.4 20
0.051 1031100.0550.050mg/KgCarbon Tetrachloride 64-143 7.1 20
0.047 95.294.20.0470.050mg/KgChlorobenzene 74-118 1.0 20
0.049 99.298.60.0490.050mg/KgChlorodibromomethane 73-122 0.6 20
0.042 84.086.80.0430.050mg/KgChloroethane 33-149 3.2 20
0.049 98.81030.0510.050mg/KgChloroform 73-127 4.1 20
0.041 82.287.80.0430.050mg/KgChloromethane 45-143 6.5 20
0.045 91.093.60.0460.050mg/Kg2-Chlorotoluene 67-124 2.8 20
0.045 91.093.60.0460.050mg/Kg4-Chlorotoluene 71-126 2.8 20
0.043 87.091.80.0450.050mg/KgDi-Isopropyl Ether (DIPE)59-159 5.3 20
0.047 94.21010.0500.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 7.1 20
0.047 95.694.40.0470.050mg/Kg1,2-Dibromoethane 70-132 1.2 20
0.050 1021000.0500.050mg/KgDibromomethane 74-133 1.1 20
0.046 93.495.00.0470.050mg/Kg1,2-Dichlorobenzene 72-123 1.6 20
0.046 93.093.60.0460.050mg/Kg1,3-Dichlorobenzene 71-120 0.6 20
0.044 89.289.60.0440.050mg/Kg1,4-Dichlorobenzene 71-123 0.4 20
Page 13 of 41Date:12/12/2023 02:36 PM
Page 177 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40555QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40553
LCS-V40553 LCSD-V40553Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.043 87.895.80.0470.050mg/KgDichlorodifluoromethane 26-146 8.7 20
0.046 93.297.40.0480.050mg/Kg1,1-Dichloroethane 74-127 4.4 20
0.053 1061080.0530.050mg/Kg1,2-Dichloroethane 68-128 1.3 20
0.047 94.21010.0500.050mg/Kg1,1-Dichloroethene 67-149 7.1 20
0.048 96.21020.0500.050mg/Kgcis-1,2-Dichloroethene 76-134 5.4 20
0.047 94.41020.0510.050mg/Kgtrans-1,2-Dichloroethene 73-132 7.7 20
0.045 90.093.80.0460.050mg/Kg1,2-Dichloropropane 73-130 4.1 20
0.047 95.091.60.0450.050mg/Kg1,3-Dichloropropane 75-124 3.6 20
0.051 1021080.0530.050mg/Kg2,2-Dichloropropane 50-142 5.5 20
0.047 94.499.40.0490.050mg/Kg1,1-Dichloropropene 71-130 5.1 20
0.050 1011040.0510.050mg/Kgcis-1,3-Dichloropropene 71-125 2.3 20
0.053 1061100.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 3.7 20
0.046 92.492.80.0460.050mg/KgEthylbenzene 74-128 0.4 20
0.093 93.596.40.0960.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 3.0 20
0.050 1011030.0510.050mg/KgHexachlorobutadiene 64-125 1.5 20
0.044 89.41000.0500.050mg/Kgn-Hexane 70-130 11.3 20
0.043 87.890.20.0450.050mg/Kg2-Hexanone 61-157 2.6 20
0.044 88.892.20.0460.050mg/KgIsopropylbenzene 68-126 3.7 20
0.046 93.896.80.0480.050mg/Kg4-Isopropyl toluene 68-129 3.1 20
0.050 1001070.0530.050mg/KgMethyl Ethyl Ketone (MEK)63-149 5.9 20
0.047 95.896.40.0480.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.6 20
0.044 89.696.80.0480.050mg/Kg4-Methyl-2-Pentanone 57-162 7.7 20
0.044 88.891.20.0450.050mg/KgMethylene Chloride 74-129 2.6 20
0.047 94.897.80.0480.050mg/KgNaphthalene 57-157 3.1 20
0.044 89.891.60.0450.050mg/Kgn-Propylbenzene 67-130 1.9 20
0.050 1011000.0500.050mg/KgStyrene 77-121 0.9 20
Page 14 of 41Date:12/12/2023 02:36 PM
Page 178 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40555QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40553
LCS-V40553 LCSD-V40553Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 99.21010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.4 20
0.041 83.085.40.0420.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.8 20
0.047 95.21040.0510.050mg/Kg 68-130 8.4 20
0.046 93.096.60.0480.050mg/Kg 71-129 3.7 20
0.051 1031030.0510.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.0 20
0.052 1041050.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.1 20
0.051 1031100.0550.050mg/Kg1,1,1-Trichloroethane 67-131 6.7 20
0.046 92.293.20.0460.050mg/Kg1,1,2-Trichloroethane 70-133 1.0 20
0.046 93.21010.0500.050mg/Kg 75-133 7.6 20
0.047 94.01040.0510.050mg/Kg 44-146 9.7 20
0.042 85.088.20.0440.050mg/Kg1,2,3-Trichloropropane 60-137 3.6 20
0.046 93.697.00.0480.050mg/Kg1,2,4-Trimethylbenzene 69-129 3.5 20
0.046 93.895.00.0470.050mg/Kg1,3,5-Trimethylbenzene 69-128 1.2 20
0.056 1141200.0600.050mg/KgVinyl Acetate 60-140 5.6 20
0.041 82.085.60.0420.050mg/KgVinyl Chloride 48-147 4.2 20
0.047 95.497.80.0480.050mg/Kgo-Xylene 74-126 2.4 20
0.095 95.995.30.0950.100mg/Kgm,p-Xylene 75-124 0.6 20
1011004-Bromofluorobenzene (S)70-130
109108Dibromofluoromethane (S)84-123
10399.8 76-129
Page 15 of 41Date:12/12/2023 02:36 PM
Page 179 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40615QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40613
Associated Lab Samples: 89898, 89899
LRB-V40613 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/27/23 18:170.0200.002<0.002mg/KgAcetone
11/27/23 18:170.0200.001<0.001mg/KgAcrolein
11/27/23 18:170.0200.0008<0.0008mg/KgAcrylonitrile
11/27/23 18:170.0050.0006<0.0006mg/KgBenzene
11/27/23 18:170.0050.0005<0.0005mg/KgBromobenzene
11/27/23 18:170.0050.0008<0.0008mg/KgBromochloromethane
11/27/23 18:170.0050.001<0.001mg/KgBromodichloromethane
11/27/23 18:170.0050.001<0.001mg/KgBromoform
11/27/23 18:170.0100.001<0.001mg/KgBromomethane
11/27/23 18:170.0050.0005<0.0005mg/Kgn-Butylbenzene
11/27/23 18:170.0050.0006<0.0006mg/Kgsec-Butyl benzene
11/27/23 18:170.0050.0005<0.0005mg/Kgtert-Butyl benzene
11/27/23 18:170.0050.0006<0.0006mg/KgCarbon Disulfide
11/27/23 18:170.0050.001<0.001mg/KgCarbon Tetrachloride
11/27/23 18:170.0050.0007<0.0007mg/KgChlorobenzene
11/27/23 18:170.0050.0009<0.0009mg/KgChlorodibromomethane
11/27/23 18:170.0100.0009<0.0009mg/KgChloroethane
11/27/23 18:170.0050.001<0.001mg/KgChloroform
11/27/23 18:170.0100.0006<0.0006mg/KgChloromethane
11/27/23 18:170.0050.0005<0.0005mg/Kg2-Chlorotoluene
11/27/23 18:170.0050.0004<0.0004mg/Kg4-Chlorotoluene
11/27/23 18:170.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
11/27/23 18:170.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
11/27/23 18:170.0050.0006<0.0006mg/Kg1,2-Dibromoethane
11/27/23 18:170.0050.0006<0.0006mg/KgDibromomethane
11/27/23 18:170.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
11/27/23 18:170.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 16 of 41Date:12/12/2023 02:36 PM
Page 180 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40615QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40613
Associated Lab Samples: 89898, 89899
LRB-V40613 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/27/23 18:170.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
11/27/23 18:170.0100.001<0.001mg/KgDichlorodifluoromethane
11/27/23 18:170.0050.0008<0.0008mg/Kg1,1-Dichloroethane
11/27/23 18:170.0050.001<0.001mg/Kg1,2-Dichloroethane
11/27/23 18:170.0050.0007<0.0007mg/Kg1,1-Dichloroethene
11/27/23 18:170.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
11/27/23 18:170.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
11/27/23 18:170.0050.0004<0.0004mg/Kg1,2-Dichloropropane
11/27/23 18:170.0050.0006<0.0006mg/Kg1,3-Dichloropropane
11/27/23 18:170.0050.001<0.001mg/Kg2,2-Dichloropropane
11/27/23 18:170.0050.0008<0.0008mg/Kg1,1-Dichloropropene
11/27/23 18:170.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
11/27/23 18:170.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
11/27/23 18:170.0050.0006<0.0006mg/KgEthylbenzene
11/27/23 18:170.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
11/27/23 18:170.0100.0008<0.0008mg/KgHexachlorobutadiene
11/27/23 18:170.0100.0007<0.0007mg/Kgn-Hexane
11/27/23 18:170.0200.0006<0.0006mg/Kg2-Hexanone
11/27/23 18:170.0050.0005<0.0005mg/KgIsopropylbenzene
11/27/23 18:170.0050.001<0.001mg/Kg4-Isopropyl toluene
11/27/23 18:170.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
11/27/23 18:170.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
11/27/23 18:170.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
11/27/23 18:170.0100.001<0.001mg/KgMethylene Chloride
11/27/23 18:170.0100.0010<0.0010mg/KgNaphthalene
11/27/23 18:170.0050.0005<0.0005mg/Kgn-Propylbenzene
11/27/23 18:170.0050.001<0.001mg/KgStyrene
Page 17 of 41Date:12/12/2023 02:36 PM
Page 181 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40615QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40613
Associated Lab Samples: 89898, 89899
LRB-V40613 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/27/23 18:170.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
11/27/23 18:170.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
11/27/23 18:170.0050.0009<0.0009mg/Kg
11/27/23 18:170.0050.0007<0.0007mg/Kg
11/27/23 18:170.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
11/27/23 18:170.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
11/27/23 18:170.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/27/23 18:170.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
11/27/23 18:170.0050.0009<0.0009mg/Kg
11/27/23 18:170.0100.002<0.002mg/Kg
11/27/23 18:170.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
11/27/23 18:170.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
11/27/23 18:170.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
11/27/23 18:170.0100.0005<0.0005mg/KgVinyl Acetate
11/27/23 18:170.0100.0005<0.0005mg/KgVinyl Chloride
11/27/23 18:170.0050.0005<0.0005mg/Kgo-Xylene
11/27/23 18:170.0100.001<0.001mg/Kgm,p-Xylene
11/27/23 18:174-Bromofluorobenzene (S)102 70-130
11/27/23 18:17Dibromofluoromethane (S)108 84-123
11/27/23 18:17 99.8 76-129
LCS-V40613 LCSD-V40613Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.093 93.091.00.0910.100mg/KgAcetone 29-198 2.1 20
0.090 90.385.30.0850.100mg/KgAcrolein 70-130 5.6 20
Page 18 of 41Date:12/12/2023 02:36 PM
Page 182 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40615QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40613
LCS-V40613 LCSD-V40613Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.088 88.186.80.0860.100mg/KgAcrylonitrile 65-134 1.4 20
0.042 85.488.60.0440.050mg/KgBenzene 74-127 3.6 20
0.042 84.886.40.0430.050mg/KgBromobenzene 73-125 1.8 20
0.045 91.291.00.0450.050mg/KgBromochloromethane 72-134 0.2 20
0.048 97.097.00.0480.050mg/KgBromodichloromethane 75-122 0.0 20
0.044 89.290.20.0450.050mg/KgBromoform 66-135 1.1 20
0.043 87.486.80.0430.050mg/KgBromomethane 20-180 0.6 20
0.044 89.492.80.0460.050mg/Kgn-Butylbenzene 65-135 3.7 20
0.042 85.688.20.0440.050mg/Kgsec-Butyl benzene 66-131 2.9 20
0.043 87.090.00.0450.050mg/Kgtert-Butyl benzene 67-132 3.3 20
0.040 80.885.40.0420.050mg/KgCarbon Disulfide 61-129 5.5 20
0.051 1041090.0540.050mg/KgCarbon Tetrachloride 64-143 4.7 20
0.043 87.889.80.0440.050mg/KgChlorobenzene 74-118 2.2 20
0.045 90.292.20.0460.050mg/KgChlorodibromomethane 73-122 2.1 20
0.045 91.493.60.0460.050mg/KgChloroethane 33-149 2.3 20
0.046 93.097.00.0480.050mg/KgChloroform 73-127 4.2 20
0.037 75.690.60.0450.050mg/KgChloromethane 45-143 18.0 20
0.043 86.088.40.0440.050mg/Kg2-Chlorotoluene 67-124 2.7 20
0.043 86.288.40.0440.050mg/Kg4-Chlorotoluene 71-126 2.5 20
0.038 77.278.80.0390.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.0 20
0.044 88.484.80.0420.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 4.1 20
0.043 86.687.00.0430.050mg/Kg1,2-Dibromoethane 70-132 0.4 20
0.045 90.292.00.0460.050mg/KgDibromomethane 74-133 1.9 20
0.044 89.089.60.0440.050mg/Kg1,2-Dichlorobenzene 72-123 0.6 20
0.043 87.489.00.0440.050mg/Kg1,3-Dichlorobenzene 71-120 1.8 20
0.040 81.084.20.0420.050mg/Kg1,4-Dichlorobenzene 71-123 3.8 20
Page 19 of 41Date:12/12/2023 02:36 PM
Page 183 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40615QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40613
LCS-V40613 LCSD-V40613Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.040 80.685.40.0420.050mg/KgDichlorodifluoromethane 26-146 5.7 20
0.042 85.889.60.0440.050mg/Kg1,1-Dichloroethane 74-127 4.3 20
0.048 97.098.80.0490.050mg/Kg1,2-Dichloroethane 68-128 1.8 20
0.046 92.896.20.0480.050mg/Kg1,1-Dichloroethene 67-149 3.5 20
0.044 89.693.00.0460.050mg/Kgcis-1,2-Dichloroethene 76-134 3.7 20
0.045 90.495.80.0470.050mg/Kgtrans-1,2-Dichloroethene 73-132 5.8 20
0.041 83.085.20.0420.050mg/Kg1,2-Dichloropropane 73-130 2.6 20
0.042 85.284.80.0420.050mg/Kg1,3-Dichloropropane 75-124 0.4 20
0.049 99.81040.0520.050mg/Kg2,2-Dichloropropane 50-142 4.3 20
0.045 90.095.60.0470.050mg/Kg1,1-Dichloropropene 71-130 6.0 20
0.046 92.694.20.0470.050mg/Kgcis-1,3-Dichloropropene 71-125 1.7 20
0.049 98.41000.0500.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.6 20
0.042 85.290.40.0450.050mg/KgEthylbenzene 74-128 5.9 20
0.083 83.985.80.0850.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 2.2 20
0.048 97.698.20.0490.050mg/KgHexachlorobutadiene 64-125 0.6 20
0.044 88.896.60.0480.050mg/Kgn-Hexane 70-130 8.4 20
0.040 80.675.40.0370.050mg/Kg2-Hexanone 61-157 6.6 20
0.042 84.488.40.0440.050mg/KgIsopropylbenzene 68-126 4.6 20
0.044 89.892.20.0460.050mg/Kg4-Isopropyl toluene 68-129 2.6 20
0.043 86.291.00.0450.050mg/KgMethyl Ethyl Ketone (MEK)63-149 5.4 20
0.042 85.688.00.0440.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.7 20
0.040 80.883.00.0410.050mg/Kg4-Methyl-2-Pentanone 57-162 2.6 20
0.040 80.482.80.0410.050mg/KgMethylene Chloride 74-129 2.9 20
0.043 87.686.60.0430.050mg/KgNaphthalene 57-157 1.1 20
0.042 84.887.80.0430.050mg/Kgn-Propylbenzene 67-130 3.4 20
0.046 92.094.40.0470.050mg/KgStyrene 77-121 2.5 20
Page 20 of 41Date:12/12/2023 02:36 PM
Page 184 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40615QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40613
LCS-V40613 LCSD-V40613Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.047 94.495.20.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.8 20
0.036 73.274.60.0370.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.8 20
0.046 92.097.80.0480.050mg/Kg 68-130 6.1 20
0.043 87.490.00.0450.050mg/Kg 71-129 2.9 20
0.047 95.093.20.0460.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.9 20
0.047 95.498.00.0490.050mg/Kg1,2,4-Trichlorobenzene 66-125 2.6 20
0.050 1011040.0520.050mg/Kg1,1,1-Trichloroethane 67-131 2.9 20
0.041 83.485.00.0420.050mg/Kg1,1,2-Trichloroethane 70-133 1.9 20
0.045 91.095.80.0470.050mg/Kg 75-133 5.1 20
0.046 92.681.80.0400.050mg/Kg 44-146 12.3 20
0.039 79.083.60.0410.050mg/Kg1,2,3-Trichloropropane 60-137 5.6 20
0.044 89.690.60.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.1 20
0.044 88.891.60.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.1 20
0.046 93.81030.0510.050mg/KgVinyl Acetate 60-140 9.3 20
0.038 77.081.40.0400.050mg/KgVinyl Chloride 48-147 5.5 20
0.045 90.092.00.0460.050mg/Kgo-Xylene 74-126 2.1 20
0.089 89.292.10.0920.100mg/Kgm,p-Xylene 75-124 3.1 20
97.498.84-Bromofluorobenzene (S)70-130
106105Dibromofluoromethane (S)84-123
100100 76-129
Page 21 of 41Date:12/12/2023 02:36 PM
Page 185 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40671QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40670
Associated Lab Samples: 89890
LRB-V40670 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/28/23 09:240.0200.002<0.002mg/KgAcetone
11/28/23 09:244-Bromofluorobenzene (S)100 70-130
11/28/23 09:24Dibromofluoromethane (S)106 70-130
11/28/23 09:24 98.6 76-129
LCS-V40670 LCSD-V40670Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.098 98.599.90.0990.100mg/KgAcetone 29-198 1.4 20
99.299.84-Bromofluorobenzene (S)70-130
106104Dibromofluoromethane (S)70-130
102101 76-129
Page 22 of 41Date:12/12/2023 02:36 PM
Page 186 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40819QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40818
Associated Lab Samples: 89904
LRB-V40818 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/30/23 13:285.001.80<1.80µg/LAcetone
11/30/23 13:285.002.00<2.00µg/LAcrolein
11/30/23 13:285.000.230<0.230µg/LAcrylonitrile
11/30/23 13:280.5000.180<0.180µg/LBenzene
11/30/23 13:280.5000.210<0.210µg/LBromobenzene
11/30/23 13:281.000.420<0.420µg/LBromochloromethane
11/30/23 13:280.5000.160<0.160µg/LBromodichloromethane
11/30/23 13:285.001.50<1.50µg/LBromoform
11/30/23 13:281.000.280<0.280µg/LBromomethane
11/30/23 13:281.000.185<0.185µg/Ln-Butylbenzene
11/30/23 13:280.5000.200<0.200µg/Lsec-Butyl benzene
11/30/23 13:282.000.920<0.920µg/Ltert-Butyl benzene
11/30/23 13:285.000.150<0.150µg/LCarbon Disulfide
11/30/23 13:280.5000.180<0.180µg/LCarbon Tetrachloride
11/30/23 13:280.5000.190<0.190µg/LChlorobenzene
11/30/23 13:280.5000.190<0.190µg/LChlorodibromomethane
11/30/23 13:281.000.430<0.430µg/LChloroethane
11/30/23 13:280.5000.220<0.220µg/LChloroform
11/30/23 13:280.5000.220<0.220µg/LChloromethane
11/30/23 13:280.5000.200<0.200µg/L2-Chlorotoluene
11/30/23 13:280.5000.200<0.200µg/L4-Chlorotoluene
11/30/23 13:285.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
11/30/23 13:282.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
11/30/23 13:280.5000.200<0.200µg/L1,2-Dibromoethane
11/30/23 13:280.5000.230<0.230µg/LDibromomethane
11/30/23 13:280.5000.220<0.220µg/L1,2-Dichlorobenzene
11/30/23 13:280.5000.190<0.190µg/L1,3-Dichlorobenzene
Page 23 of 41Date:12/12/2023 02:36 PM
Page 187 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40819QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40818
Associated Lab Samples: 89904
LRB-V40818 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/30/23 13:280.5000.210<0.210µg/L1,4-Dichlorobenzene
11/30/23 13:285.001.20<1.20µg/LDichlorodifluoromethane
11/30/23 13:280.5000.240<0.240µg/L1,1-Dichloroethane
11/30/23 13:280.5000.150<0.150µg/L1,2-Dichloroethane
11/30/23 13:280.5000.150<0.150µg/L1,1-Dichloroethene
11/30/23 13:280.5000.200<0.200µg/Lcis-1,2-Dichloroethene
11/30/23 13:280.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
11/30/23 13:280.5000.190<0.190µg/L1,2-Dichloropropane
11/30/23 13:280.5000.130<0.130µg/L1,3-Dichloropropane
11/30/23 13:282.000.210<0.210µg/L2,2-Dichloropropane
11/30/23 13:280.5000.200<0.200µg/L1,1-Dichloropropene
11/30/23 13:280.5000.210<0.210µg/Lcis-1,3-Dichloropropene
11/30/23 13:280.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
11/30/23 13:280.5000.170<0.170µg/LEthylbenzene
11/30/23 13:2810.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
11/30/23 13:282.000.350<0.350µg/LHexachlorobutadiene
11/30/23 13:2810.01.30<1.30µg/Ln-Hexane
11/30/23 13:285.000.380<0.380µg/L2-Hexanone
11/30/23 13:285.000.180<0.180µg/LIsopropylbenzene
11/30/23 13:280.5000.089<0.089µg/L4-Isopropyl toluene
11/30/23 13:285.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
11/30/23 13:280.5000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
11/30/23 13:285.001.00<1.00µg/L4-Methyl-2-Pentanone
11/30/23 13:281.000.330<0.330µg/LMethylene Chloride
11/30/23 13:281.000.470<0.470µg/LNaphthalene
11/30/23 13:280.5000.190<0.190µg/Ln-Propylbenzene
11/30/23 13:280.5000.220<0.220µg/LStyrene
Page 24 of 41Date:12/12/2023 02:36 PM
Page 188 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40819QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40818
Associated Lab Samples: 89904
LRB-V40818 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/30/23 13:280.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
11/30/23 13:280.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
11/30/23 13:280.5000.220<0.220µg/L
11/30/23 13:280.5000.220<0.220µg/L
11/30/23 13:282.000.380<0.380µg/L1,2,3-Trichlorobenzene
11/30/23 13:281.000.310<0.310µg/L1,2,4-Trichlorobenzene
11/30/23 13:280.5000.160<0.160µg/L1,1,1-Trichloroethane
11/30/23 13:280.5000.096<0.096µg/L1,1,2-Trichloroethane
11/30/23 13:280.5000.180<0.180µg/L
11/30/23 13:280.5000.180<0.180µg/L
11/30/23 13:281.000.270<0.270µg/L1,2,3-Trichloropropane
11/30/23 13:280.5000.190<0.190µg/L1,2,4-Trimethylbenzene
11/30/23 13:280.5000.180<0.180µg/L1,3,5-Trimethylbenzene
11/30/23 13:282.001.00<1.00µg/LVinyl Acetate
11/30/23 13:280.5000.170<0.170µg/LVinyl Chloride
11/30/23 13:280.5000.210<0.210µg/Lo-Xylene
11/30/23 13:281.000.420<0.420µg/Lm,p-Xylene
11/30/23 13:284-Bromofluorobenzene (S)101 80-124
11/30/23 13:28Dibromofluoromethane (S)98.4 75-129
11/30/23 13:281,2-Dichloroethane - d4 (S)92.2 63-136
11/30/23 13:28 99.4 77-123
LCS-V40818 LCSD-V40818Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
63.4 159170*67.840.0µg/LAcetone 40-166 6.7 20.0
Page 25 of 41* QC Fail Date:12/12/2023 02:36 PM
Page 189 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40819QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40818
LCS-V40818 LCSD-V40818Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.0 45.0*47.2*18.940.0µg/LAcrolein 70-130 4.8 20.0
27.4 68.5*73.7*29.540.0µg/LAcrylonitrile 81-127 7.3 20.0
21.0 10511021.920.0µg/LBenzene 77-128 4.1 20.0
21.1 10610220.320.0µg/LBromobenzene 78-129 3.8 20.0
20.7 10410921.820.0µg/LBromochloromethane 78-135 5.1 20.0
20.7 10410721.320.0µg/LBromodichloromethane 76-138 2.8 20.0
17.7 88.595.519.120.0µg/LBromoform 71-135 7.6 20.0
24.1 12112424.820.0µg/LBromomethane 41-168 2.8 20.0
20.9 10510220.420.0µg/Ln-Butylbenzene 68-134 2.4 20.0
21.6 10810621.120.0µg/Lsec-Butyl benzene 71-131 2.3 20.0
21.0 10510521.020.0µg/Ltert-Butyl benzene 70-132 0.0 20.0
23.4 11711322.520.0µg/LCarbon Disulfide 59-135 3.9 20.0
23.6 11811422.720.0µg/LCarbon Tetrachloride 72-142 3.8 20.0
21.7 10910921.820.0µg/LChlorobenzene 78-119 0.4 20.0
21.3 10710721.420.0µg/LChlorodibromomethane 75-134 0.4 20.0
25.5 12812925.820.0µg/LChloroethane 57-142 1.1 20.0
21.7 10911122.120.0µg/LChloroform 77-130 1.8 20.0
24.5 12312725.420.0µg/LChloromethane 47-145 3.6 20.0
20.8 10410420.720.0µg/L2-Chlorotoluene 74-126 0.4 20.0
20.6 10310320.520.0µg/L4-Chlorotoluene 78-129 0.4 20.0
21.6 10811222.420.0µg/LDi-Isopropyl Ether (DIPE)60-154 3.6 20.0
16.1 80.583.016.620.0µg/L1,2-Dibromo-3-Chloropropane 63-134 3.0 20.0
20.2 10110320.620.0µg/L1,2-Dibromoethane 77-135 1.9 20.0
20.7 10410921.820.0µg/LDibromomethane 76-138 5.1 20.0
20.1 10110220.320.0µg/L1,2-Dichlorobenzene 78-128 0.9 20.0
20.7 10410621.120.0µg/L1,3-Dichlorobenzene 77-125 1.9 20.0
Page 26 of 41* QC Fail Date:12/12/2023 02:36 PM
Page 190 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40819QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40818
LCS-V40818 LCSD-V40818Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.4 10210320.620.0µg/L1,4-Dichlorobenzene 75-126 0.9 20.0
25.6 12813226.320.0µg/LDichlorodifluoromethane 28-163 2.6 20.0
23.3 11711923.820.0µg/L1,1-Dichloroethane 70-130 2.1 20.0
21.0 10510721.420.0µg/L1,2-Dichloroethane 68-131 1.8 20.0
23.6 11812124.220.0µg/L1,1-Dichloroethene 70-154 2.5 20.0
21.8 10911422.820.0µg/Lcis-1,2-Dichloroethene 76-141 4.4 20.0
21.9 11011823.620.0µg/Ltrans-1,2-Dichloroethene 76-135 7.4 20.0
22.4 11211723.320.0µg/L1,2-Dichloropropane 77-130 3.9 20.0
20.5 10310220.320.0µg/L1,3-Dichloropropane 76-132 0.9 20.0
22.8 11411723.420.0µg/L2,2-Dichloropropane 29-149 2.5 20.0
23.8 11911823.620.0µg/L1,1-Dichloropropene 71-136 0.8 20.0
19.8 99.010220.320.0µg/Lcis-1,3-Dichloropropene 65-140 2.4 20.0
19.5 97.510120.220.0µg/Ltrans-1,3-Dichloropropene 67-140 3.5 20.0
20.2 10110120.220.0µg/LEthylbenzene 80-127 0.0 20.0
43.5 10911244.940.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 3.1 20.0
21.6 10810921.720.0µg/LHexachlorobutadiene 61-134 0.4 20.0
22.6 11311823.520.0µg/Ln-Hexane 70-130 3.9 20.0
22.9 11511923.820.0µg/L2-Hexanone 64-137 3.8 20.0
21.8 10910721.420.0µg/LIsopropylbenzene 70-130 1.8 20.0
20.8 10410420.820.0µg/L4-Isopropyl toluene 69-132 0.0 20.0
24.5 123142*28.320.0µg/LMethyl Ethyl Ketone (MEK)71-134 14.3 20.0
19.9 99.510521.020.0µg/LMethyl tert-butyl ether (MTBE)68-135 5.3 20.0
17.9 89.599.519.920.0µg/L4-Methyl-2-Pentanone 69-134 10.5 20.0
21.9 11011122.120.0µg/LMethylene Chloride 73-131 0.9 20.0
15.1 75.576.515.320.0µg/LNaphthalene 64-136 1.3 20.0
21.4 10710520.920.0µg/Ln-Propylbenzene 72-132 2.3 20.0
Page 27 of 41* QC Fail Date:12/12/2023 02:36 PM
Page 191 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40819QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40818
LCS-V40818 LCSD-V40818Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.1 10110220.320.0µg/LStyrene 78-129 0.9 20.0
20.7 10410721.420.0µg/L1,1,1,2-Tetrachloroethane 79-134 3.3 20.0
19.4 97.010120.220.0µg/L1,1,2,2-Tetrachloroethane 62-127 4.0 20.0
22.3 11211422.720.0µg/L 80-129 1.7 20.0
20.9 10510621.220.0µg/L 76-131 1.4 20.0
16.1 80.575.015.020.0µg/L1,2,3-Trichlorobenzene 58-144 7.0 20.0
17.4 87.084.516.920.0µg/L1,2,4-Trichlorobenzene 66-139 2.9 20.0
22.1 11111623.120.0µg/L1,1,1-Trichloroethane 75-135 4.4 20.0
19.1 95.510621.120.0µg/L1,1,2-Trichloroethane 70-140 9.9 20.0
22.5 11311422.720.0µg/L 77-133 0.8 20.0
26.5 13313326.520.0µg/L 62-148 0.0 20.0
21.1 10610120.120.0µg/L1,2,3-Trichloropropane 71-127 4.8 20.0
20.5 10310520.920.0µg/L1,2,4-Trimethylbenzene 75-133 1.9 20.0
21.0 10510320.620.0µg/L1,3,5-Trimethylbenzene 75-131 1.9 20.0
15.1 75.584.016.820.0µg/LVinyl Acetate 34-167 10.6 20.0
27.4 13713426.820.0µg/LVinyl Chloride 57-141 2.2 20.0
20.7 10410320.520.0µg/Lo-Xylene 78-128 0.9 20.0
43.5 10910943.740.0µg/Lm,p-Xylene 77-133 0.4 20.0
98.698.84-Bromofluorobenzene (S)80-124
99.8101Dibromofluoromethane (S)75-129
97.41011,2-Dichloroethane - d4 (S)63-136
99.698.4 77-123
Page 28 of 41Date:12/12/2023 02:36 PM
Page 192 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40513QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40498
Associated Lab Samples: 89889, 89891, 89892, 89893, 89894, 89895, 89896, 89897, 89898, 89899, 89900, 89901, 89902, 89903
LRB-V40498 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/22/23 18:490.6600.116<0.116mg/KgAcenaphthene
11/22/23 18:490.6600.105<0.105mg/KgAcenaphthylene
11/22/23 18:490.6600.152<0.152mg/KgAniline
11/22/23 18:490.6600.143<0.143mg/KgAnthracene
11/22/23 18:490.6600.139<0.139mg/KgBenzo(a)anthracene
11/22/23 18:490.6600.147<0.147mg/KgBenzo(a)pyrene
11/22/23 18:490.6600.146<0.146mg/KgBenzo(b)fluoranthene
11/22/23 18:490.6600.136<0.136mg/KgBenzo(g,h,i)perylene
11/22/23 18:490.6600.137<0.137mg/KgBenzo(k)fluoranthene
11/22/23 18:492.000.580<0.580mg/KgBenzoic Acid
11/22/23 18:490.6600.105<0.105mg/KgBenzyl alcohol
11/22/23 18:490.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
11/22/23 18:490.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
11/22/23 18:490.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
11/22/23 18:490.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
11/22/23 18:490.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
11/22/23 18:490.3300.113<0.113mg/KgButyl benzyl phthalate
11/22/23 18:490.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
11/22/23 18:490.3300.112<0.112mg/Kg4-Chloroaniline
11/22/23 18:490.6600.116<0.116mg/Kg2-Chloronaphthalene
11/22/23 18:490.6600.098<0.098mg/Kg2-Chlorophenol
11/22/23 18:491.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
11/22/23 18:490.6600.142<0.142mg/KgChrysene
11/22/23 18:490.6600.230<0.230mg/KgDibenz(a,h)anthracene
11/22/23 18:490.6600.119<0.119mg/KgDibenzofuran
11/22/23 18:490.6600.094<0.094mg/Kg1,2-Dichlorobenzene
11/22/23 18:490.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 29 of 41Date:12/12/2023 02:36 PM
Page 193 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40513QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40498
Associated Lab Samples: 89889, 89891, 89892, 89893, 89894, 89895, 89896, 89897, 89898, 89899, 89900, 89901, 89902, 89903
LRB-V40498 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/22/23 18:490.3300.097<0.097mg/Kg1,4-Dichlorobenzene
11/22/23 18:490.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
11/22/23 18:490.6600.095<0.095mg/Kg2,4-Dichlorophenol
11/22/23 18:490.6600.180<0.180mg/KgDiethyl phthalate
11/22/23 18:490.6600.174<0.174mg/KgDimethyl phthalate
11/22/23 18:490.3300.108<0.108mg/Kg2,4-Dimethylphenol
11/22/23 18:490.6600.107<0.107mg/KgDi-n-butyl phthalate
11/22/23 18:491.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
11/22/23 18:491.500.520<0.520mg/Kg2,4-Dinitrophenol
11/22/23 18:490.6600.096<0.096mg/Kg2,4-Dinitrotoluene
11/22/23 18:490.6600.108<0.108mg/Kg2,6-Dinitrotoluene
11/22/23 18:490.3300.143<0.143mg/KgDi-n-Octyl Phthalate
11/22/23 18:490.6600.123<0.123mg/KgFluoranthene
11/22/23 18:490.6600.128<0.128mg/KgFluorene
11/22/23 18:490.6600.106<0.106mg/KgHexachlorobenzene
11/22/23 18:490.6600.097<0.097mg/KgHexachlorobutadiene
11/22/23 18:490.6600.157<0.157mg/KgHexachlorocyclopentadiene
11/22/23 18:490.6600.079<0.079mg/KgHexachloroethane
11/22/23 18:490.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
11/22/23 18:490.6600.191<0.191mg/KgIsophorone
11/22/23 18:490.6600.106<0.106mg/Kg1-Methylnaphthalene
11/22/23 18:490.6600.100<0.100mg/Kg2-Methylnaphthalene
11/22/23 18:490.6600.097<0.097mg/Kg2-Methylphenol
11/22/23 18:490.6600.084<0.084mg/Kg3&4 Methylphenol
11/22/23 18:490.6600.144<0.144mg/KgNaphthalene
11/22/23 18:490.6600.096<0.096mg/Kg2-Nitroaniline
11/22/23 18:490.6600.120<0.120mg/Kg3-Nitroaniline
Page 30 of 41Date:12/12/2023 02:36 PM
Page 194 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40513QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40498
Associated Lab Samples: 89889, 89891, 89892, 89893, 89894, 89895, 89896, 89897, 89898, 89899, 89900, 89901, 89902, 89903
LRB-V40498 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/22/23 18:490.3300.093<0.093mg/Kg4-Nitroaniline
11/22/23 18:490.3300.116<0.116mg/KgNitrobenzene
11/22/23 18:490.6600.088<0.088mg/Kg2-Nitrophenol
11/22/23 18:490.6600.117<0.117mg/Kg4-Nitrophenol
11/22/23 18:490.6600.263<0.263mg/KgN-Nitrosodimethylamine
11/22/23 18:490.6600.181<0.181mg/KgN-Nitrosodiphenylamine
11/22/23 18:490.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
11/22/23 18:491.000.347<0.347mg/KgPentachlorophenol
11/22/23 18:490.6600.208<0.208mg/KgPhenanthrene
11/22/23 18:490.6600.112<0.112mg/KgPhenol
11/22/23 18:490.6600.134<0.134mg/KgPyrene
11/22/23 18:490.3300.079<0.079mg/KgPyridine
11/22/23 18:490.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
11/22/23 18:490.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
11/22/23 18:490.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
11/22/23 18:492-Fluorobiphenyl (S)88.6 44-115
11/22/23 18:492-Fluorophenol (S)81.9 35-115
11/22/23 18:49Nitrobenzene-d5 (S)84.4 37-122
11/22/23 18:494-Terphenyl-d14 (S)82.0 54-127
11/22/23 18:492,4,6-Tribromophenol (S)83.1 39-132
11/22/23 18:49Phenol-d5 (S)81.6 34-121
LCS-V40498Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
87.41.461.67mg/KgAcenaphthene 40-123
86.81.451.67mg/KgAcenaphthylene 32-132
Page 31 of 41Date:12/12/2023 02:36 PM
Page 195 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40513QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40498
LCS-V40498Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1342.241.67mg/KgAniline 12-197
91.01.521.67mg/KgAnthracene 47-123
81.41.361.67mg/KgBenzo(a)anthracene 49-126
79.61.331.67mg/KgBenzo(a)pyrene 45-129
73.61.231.67mg/KgBenzo(b)fluoranthene 45-132
74.21.241.67mg/KgBenzo(g,h,i)perylene 43-134
70.01.171.67mg/KgBenzo(k)fluoranthene 47-132
0.0*<0.5801.67mg/KgBenzoic Acid 10-83
85.01.421.67mg/KgBenzyl alcohol 29-122
73.61.231.67mg/KgBis(2-Chloroethoxy)methane 36-121
73.01.221.67mg/KgBis(2-Chloroethyl)ether 31-120
78.41.311.67mg/KgBis(2-Chloroisopropyl)ether 33-131
90.41.511.67mg/KgBis(2-ethylhexyl)phthalate 51-133
86.21.441.67mg/Kg4-Bromophenyl phenyl ether 46-124
88.01.471.67mg/KgButyl benzyl phthalate 48-132
77.21.291.67mg/Kg4-Chloro-3-methylphenol 45-122
73.61.231.67mg/Kg4-Chloroaniline 17-106
88.01.471.67mg/Kg2-Chloronaphthalene 41-114
83.21.391.67mg/Kg2-Chlorophenol 34-121
85.01.421.67mg/Kg4-Chlorophenyl phenyl ether 45-121
83.21.391.67mg/KgChrysene 50-124
67.61.131.67mg/KgDibenz(a,h)anthracene 45-134
89.21.491.67mg/KgDibenzofuran 44-120
76.01.271.67mg/Kg1,2-Dichlorobenzene 33-117
75.41.261.67mg/Kg1,3-Dichlorobenzene 30-115
70.61.181.67mg/Kg1,4-Dichlorobenzene 31-115
64.01.071.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 32 of 41* QC Fail Date:12/12/2023 02:36 PM
Page 196 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40513QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40498
LCS-V40498Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
79.01.321.67mg/Kg2,4-Dichlorophenol 40-122
93.41.561.67mg/KgDiethyl phthalate 50-124
94.01.571.67mg/KgDimethyl phthalate 48-124
1021.711.67mg/Kg2,4-Dimethylphenol 30-127
98.21.641.67mg/KgDi-n-butyl phthalate 51-128
77.21.291.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
43.60.7291.67mg/Kg2,4-Dinitrophenol 27-129
99.41.661.67mg/Kg2,4-Dinitrotoluene 48-126
95.81.601.67mg/Kg2,6-Dinitrotoluene 46-124
76.01.271.67mg/KgDi-n-Octyl Phthalate 45-140
92.21.541.67mg/KgFluoranthene 50-127
91.61.531.67mg/KgFluorene 43-125
93.41.561.67mg/KgHexachlorobenzene 45-122
80.21.341.67mg/KgHexachlorobutadiene 32-123
75.41.261.67mg/KgHexachlorocyclopentadiene 32-117
74.21.241.67mg/KgHexachloroethane 28-117
74.81.251.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
70.61.181.67mg/KgIsophorone 30-122
72.41.211.67mg/Kg1-Methylnaphthalene 40-119
74.21.241.67mg/Kg2-Methylnaphthalene 38-122
80.81.351.67mg/Kg2-Methylphenol 32-122
74.21.241.67mg/Kg3&4 Methylphenol 34-119
71.21.191.67mg/KgNaphthalene 35-123
89.81.501.67mg/Kg2-Nitroaniline 44-127
82.61.381.67mg/Kg3-Nitroaniline 33-119
97.01.621.67mg/Kg4-Nitroaniline 63-147
75.41.261.67mg/KgNitrobenzene 34-122
Page 33 of 41Date:12/12/2023 02:36 PM
Page 197 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40513QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40498
LCS-V40498Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
74.21.241.67mg/Kg2-Nitrophenol 36-123
97.61.631.67mg/Kg4-Nitrophenol 30-132
67.61.131.67mg/KgN-Nitrosodimethylamine 10-146
1071.781.67mg/KgN-Nitrosodiphenylamine 38-127
82.61.381.67mg/KgN-Nitroso-di-n-propylamine 36-120
89.21.491.67mg/KgPentachlorophenol 25-133
92.21.541.67mg/KgPhenanthrene 50-121
79.01.321.67mg/KgPhenol 34-121
82.61.381.67mg/KgPyrene 47-127
50.70.8481.67mg/KgPyridine 10-80
71.81.201.67mg/Kg1,2,4-Trichlorobenzene 34-118
86.21.441.67mg/Kg2,4,5-Trichlorophenol 41-124
88.01.471.67mg/Kg2,4,6-Trichlorophenol 39-126
88.02-Fluorobiphenyl (S)44-115
85.22-Fluorophenol (S)35-115
74.2Nitrobenzene-d5 (S)37-122
80.24-Terphenyl-d14 (S)54-127
96.92,4,6-Tribromophenol (S)39-132
81.3Phenol-d5 (S)34-121
V 89892-MS-V40498 V 89892-MSD-V40498Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.36 81.41.331.661.67<0.116mg/KgAcenaphthene 80.1 40-123 2.2 20
1.33 79.61.341.661.67<0.105mg/KgAcenaphthylene 80.7 32-132 0.7 20
1.78 1071.811.661.67<0.152mg/KgAniline 109 12-197 1.6 20
Page 34 of 41Date:12/12/2023 02:36 PM
Page 198 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40513QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40498
V 89892-MS-V40498 V 89892-MSD-V40498Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.45 86.81.461.661.67<0.143mg/KgAnthracene 87.9 47-123 0.6 20
1.26 75.41.331.661.67<0.139mg/KgBenzo(a)anthracene 80.1 49-126 5.4 20
1.23 73.61.291.661.67<0.147mg/KgBenzo(a)pyrene 77.7 45-129 4.7 20
1.15 68.81.151.661.67<0.146mg/KgBenzo(b)fluoranthene 69.2 45-132 0.0 20
1.13 67.61.161.661.67<0.136mg/KgBenzo(g,h,i)perylene 69.8 43-134 2.6 20
1.09 65.21.181.661.67<0.137mg/KgBenzo(k)fluoranthene 71.0 47-132 7.9 20
1.14 68.21.131.661.67<0.580mg/KgBenzoic Acid 68.0 10-83 0.8 20
1.32 79.01.351.661.67<0.105mg/KgBenzyl alcohol 81.3 29-122 2.2 20
1.13 67.61.121.661.67<0.118mg/KgBis(2-Chloroethoxy)methane 67.4 36-121 0.8 20
1.10 65.81.121.661.67<0.107mg/KgBis(2-Chloroethyl)ether 67.4 31-120 1.8 20
1.18 70.61.161.661.67<0.136mg/KgBis(2-Chloroisopropyl)ether 69.8 33-131 1.7 20
1.41 84.41.481.661.67<0.120mg/KgBis(2-ethylhexyl)phthalate 89.1 51-133 4.8 20
1.34 80.21.341.661.67<0.109mg/Kg4-Bromophenyl phenyl ether 80.7 46-124 0.0 20
1.43 85.61.481.661.67<0.113mg/KgButyl benzyl phthalate 89.1 48-132 3.4 20
1.20 71.81.201.661.67<0.092mg/Kg4-Chloro-3-methylphenol 72.2 45-122 0.0 20
1.11 66.41.101.661.67<0.112mg/Kg4-Chloroaniline 66.2 17-106 0.9 20
1.37 82.01.361.661.67<0.116mg/Kg2-Chloronaphthalene 81.9 41-114 0.7 20
1.25 74.81.251.661.67<0.098mg/Kg2-Chlorophenol 75.3 34-121 0.0 20
1.30 77.81.311.661.67<0.126mg/Kg4-Chlorophenyl phenyl ether 78.9 45-121 0.7 20
1.33 79.61.381.661.67<0.142mg/KgChrysene 83.1 50-124 3.6 20
1.18 70.61.221.661.67<0.230mg/KgDibenz(a,h)anthracene 73.4 45-134 3.3 20
1.37 82.01.371.661.67<0.119mg/KgDibenzofuran 82.5 44-120 0.0 20
1.17 70.01.171.661.67<0.094mg/Kg1,2-Dichlorobenzene 70.4 33-117 0.0 20
1.13 67.61.121.661.67<0.097mg/Kg1,3-Dichlorobenzene 67.4 30-115 0.8 20
1.10 65.81.111.661.67<0.097mg/Kg1,4-Dichlorobenzene 66.8 31-115 0.9 20
0.847 50.70.9521.661.67<0.147mg/Kg3,3'-Dichlorobenzidine 57.3 22-121 11.6 20
Page 35 of 41Date:12/12/2023 02:36 PM
Page 199 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40513QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40498
V 89892-MS-V40498 V 89892-MSD-V40498Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.22 73.01.191.661.67<0.095mg/Kg2,4-Dichlorophenol 71.6 40-122 2.4 20
1.43 85.61.451.661.67<0.180mg/KgDiethyl phthalate 87.3 50-124 1.3 20
1.42 85.01.421.661.67<0.174mg/KgDimethyl phthalate 85.5 48-124 0.0 30
1.56 93.41.561.661.67<0.108mg/Kg2,4-Dimethylphenol 93.9 30-127 0.0 20
1.56 93.41.571.661.67<0.107mg/KgDi-n-butyl phthalate 94.5 51-128 0.6 20
1.30 77.81.321.661.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 79.5 29-132 1.5 20
1.20 71.81.241.661.67<0.520mg/Kg2,4-Dinitrophenol 74.6 27-129 3.2 20
1.52 91.01.541.661.67<0.096mg/Kg2,4-Dinitrotoluene 92.7 48-126 1.3 20
1.44 86.21.471.661.67<0.108mg/Kg2,6-Dinitrotoluene 88.5 46-124 2.0 20
1.19 71.21.241.661.67<0.143mg/KgDi-n-Octyl Phthalate 74.6 45-140 4.1 20
1.40 83.81.441.661.67<0.123mg/KgFluoranthene 86.7 50-127 2.8 20
1.41 84.41.431.661.67<0.128mg/KgFluorene 86.1 43-125 1.4 20
1.43 85.61.451.661.67<0.106mg/KgHexachlorobenzene 87.3 45-122 1.3 20
1.21 72.41.211.661.67<0.097mg/KgHexachlorobutadiene 72.8 32-123 0.0 20
0.986 59.00.9971.661.67<0.157mg/KgHexachlorocyclopentadiene 60.0 32-117 1.1 20
1.11 66.41.131.661.67<0.079mg/KgHexachloroethane 68.0 28-117 1.7 20
1.15 68.81.181.661.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 71.0 45-133 2.5 20
1.09 65.21.061.661.67<0.191mg/KgIsophorone 63.8 30-122 2.7 20
1.14 68.21.131.661.67<0.106mg/Kg1-Methylnaphthalene 68.0 40-119 0.8 20
1.15 68.81.151.661.67<0.100mg/Kg2-Methylnaphthalene 69.2 38-122 0.0 20
1.21 72.41.231.661.67<0.097mg/Kg2-Methylphenol 74.0 32-122 1.6 20
1.11 66.41.101.661.67<0.084mg/Kg3&4 Methylphenol 66.2 34-119 0.9 20
1.11 66.41.091.661.67<0.144mg/KgNaphthalene 65.6 35-123 1.8 20
1.39 83.21.391.661.67<0.096mg/Kg2-Nitroaniline 83.7 44-127 0.0 20
1.33 79.61.331.661.67<0.120mg/Kg3-Nitroaniline 80.1 33-119 0.0 20
1.40 83.81.481.661.67<0.093mg/Kg4-Nitroaniline 89.1 63-147 5.5 20
Page 36 of 41Date:12/12/2023 02:36 PM
Page 200 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40513QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40498
V 89892-MS-V40498 V 89892-MSD-V40498Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.15 68.81.151.661.67<0.116mg/KgNitrobenzene 69.2 34-122 0.0 20
1.11 66.41.111.661.67<0.088mg/Kg2-Nitrophenol 66.8 32-123 0.0 20
1.41 84.41.491.661.67<0.117mg/Kg4-Nitrophenol 89.7 30-132 5.5 20
1.01 60.41.031.661.67<0.263mg/KgN-Nitrosodimethylamine 62.0 10-146 1.9 30
1.64 98.21.671.661.67<0.181mg/KgN-Nitrosodiphenylamine 101 38-127 1.8 20
1.23 73.61.261.661.67<0.118mg/KgN-Nitroso-di-n-propylamine 75.9 36-120 2.4 20
1.50 89.81.501.661.67<0.347mg/KgPentachlorophenol 90.3 25-133 0.0 20
1.45 86.81.471.661.67<0.208mg/KgPhenanthrene 88.5 50-121 1.3 20
1.18 70.61.171.661.67<0.112mg/KgPhenol 70.4 34-121 0.8 20
1.33 79.61.371.661.67<0.134mg/KgPyrene 82.5 47-127 2.9 20
0.782 46.80.7421.661.67<0.079mg/KgPyridine 44.6 10-80 5.2 20
1.12 67.01.111.661.67<0.107mg/Kg1,2,4-Trichlorobenzene 66.8 34-118 0.8 20
1.35 80.81.351.661.67<0.096mg/Kg2,4,5-Trichlorophenol 81.3 41-124 0.0 20
1.32 79.01.331.661.67<0.096mg/Kg2,4,6-Trichlorophenol 80.1 39-126 0.7 20
82.02-Fluorobiphenyl (S)81.3 44-115
78.62-Fluorophenol (S)77.7 35-115
70.6Nitrobenzene-d5 (S)68.0 37-122
77.84-Terphenyl-d14 (S)80.7 54-127
89.72,4,6-Tribromophenol (S)91.2 39-132
75.6Phenol-d5 (S)73.8 34-121
Page 37 of 41Date:12/12/2023 02:36 PM
Page 201 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L720894QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L720353
Associated Lab Samples: 89889, 89891, 89892, 89893, 89894, 89895, 89896, 89897, 89898, 89899
LRB-L720353 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/06/23 12:000.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L720353Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
85.03.394.00mg/KgChromium, Hexavalent 80-120
V 89896-DUP-L720353Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20 12/06/23 12:3314.20.3320.383mg/KgChromium, Hexavalent
V 89896-MS-L720353Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
20.3 52.0*38.6<1.36mg/KgChromium, Hexavalent 75-125
Page 38 of 41Date:12/12/2023 02:36 PM
Page 202 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L720941QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L720354
Associated Lab Samples: 89900, 89901, 89902, 89903
LRB-L720354 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/06/23 16:190.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L720354Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
83.03.314.00mg/KgChromium, Hexavalent 80-120
V 89902-DUP-L720354Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20 12/06/23 16:520.0<0.200<0.200mg/KgChromium, Hexavalent
V 89902-MS-L720354Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
19.0 48.0*39.8<0.141mg/KgChromium, Hexavalent 75-125
Page 39 of 41Date:12/12/2023 02:36 PM
Page 203 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
Dry Weight Determination
SW-DRYWT
V40480QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89889-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/22/23 10:221.519.919.6%Moisture
V 90123-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/22/23 10:220.713.613.5%Moisture
Page 40 of 41Date:12/12/2023 02:36 PM
Page 204 of 208
Quality Control Data
23-325-0008Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
Former Winston Container
Dry Weight Determination
SW-DRYWT
V40537QC Analytical Batch:
Analysis Method:
Analysis Description:
V 90226-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/27/23 12:180.00.3250.325%Moisture
V 90323-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/27/23 12:180.84.514.55%Moisture
Page 41 of 41Date:12/12/2023 02:36 PM
Page 205 of 208
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-325-0008
Mid-Atlantic Associates, Inc. - Raleigh
01139
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 3.8C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:11/21/2023 11:09:18
Special precautions or instructions included?
Comments:
Page 206 of 208
Page 207 of 208
Page 208 of 208

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/5/2023
Mid-Atlantic Associates, Inc. - Charlotte Troy Holzschuh
1125 E. Morehead Street, Suite 104 Charlotte, NC, 28204
Ref: Analytical Testing
Lab Report Number: 23-321-0112 Client Project Description: Former Winston Container
Dear Troy Holzschuh:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/17/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 117
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/29/202440750State ProgramAlabama
02/07/202488-0650State ProgramArkansas
06/30/20242904State ProgramCalifornia
06/30/2024E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202404015State ProgramGeorgia
10/31/2024200078State Program - NELAPIllinois
06/30/202480215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202404015State Program - NELAPLouisiana
11/14/2025MSState ProgramMississippi
07/31/202447701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202468-03195State Program - NELAPPennsylvania
06/30/202484002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2024T104704180State Program - NELAPTexas
06/30/202400106State ProgramVirginia
09/14/2024460181State Program - NELAPVirginia
Page 1 of 1 00016/23-321-0112
Page 2 of 117
Report Number:
Sample Summary Table
Client Project Description:
23-321-0112
Former Winston Container
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
11/17/2023 12:00Aqueous 89739 SW-1 11/17/2023 13:54
11/17/2023 12:00Aqueous 89739 SW-1 11/17/2023 13:54 6020B
11/17/2023 12:00Aqueous 89739 SW-1 11/17/2023 13:54 7470A
11/17/2023 11:20Aqueous 89740 SW-2 11/17/2023 13:54
11/17/2023 11:20Aqueous 89740 SW-2 11/17/2023 13:54 7470A
11/17/2023 11:20Aqueous 89740 SW-2 11/17/2023 13:54 6020B
11/17/2023Aqueous 89741 Dup-1 11/17/2023 13:54
11/17/2023Aqueous 89741 Dup-1 11/17/2023 13:54 7470A
11/17/2023Aqueous 89741 Dup-1 11/17/2023 13:54 6020B
11/17/2023 10:40Aqueous 89742 SW-3 11/17/2023 13:54
11/17/2023 10:40Aqueous 89742 SW-3 11/17/2023 13:54 7470A
11/17/2023 10:40Aqueous 89742 SW-3 11/17/2023 13:54 6020B
11/17/2023 12:10Solids 89743 SED-1 11/17/2023 13:54
11/17/2023 12:10Solids 89743 SED-1 11/17/2023 13:54 SW-7199
11/17/2023 12:10Solids 89743 SED-1 11/17/2023 13:54 6020B
11/17/2023 11:25Solids 89744 SED-2 11/17/2023 13:54
11/17/2023 11:25Solids 89744 SED-2 11/17/2023 13:54 SW-7199
11/17/2023 11:25Solids 89744 SED-2 11/17/2023 13:54 6020B
11/17/2023Solids 89745 DUP-2 11/17/2023 13:54
11/17/2023Solids 89745 DUP-2 11/17/2023 13:54 SW-7199
11/17/2023Solids 89745 DUP-2 11/17/2023 13:54 6020B
11/17/2023 10:45Solids 89746 SED-3 11/17/2023 13:54
11/17/2023 10:45Solids 89746 SED-3 11/17/2023 13:54 SW-7199
11/17/2023 10:45Solids 89746 SED-3 11/17/2023 13:54 6020B
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 117
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-321-0112
Report Limit
Project:Former Winston Container
V 89739SW-1
42.1 11/29/2023 05:216020BBariumµg/L 0.453
J0.387 11/29/2023 05:216020BChromiumµg/L 0.346
J0.457 11/28/2023 22:538260Dm,p-Xylene µg/L 0.420
J0.457 11/28/2023 22:538260DXylene (Total)µg/L 0.210
V 89740SW-2
44.8 11/29/2023 05:266020BBariumµg/L 0.453
J0.506 11/29/2023 05:266020BChromiumµg/L 0.346
J0.408 11/28/2023 23:188260DTrichloroetheneµg/L 0.180
J2.54 11/20/2023 19:558270EDi-n-butyl phthalate µg/L 2.06
V 89741Dup-1
46.7 11/29/2023 05:306020BBariumµg/L 0.453
J0.287 11/28/2023 23:448260DTrichloroetheneµg/L 0.180
V 89742SW-3
46.4 11/29/2023 05:356020BBariumµg/L 0.453
J0.445 11/29/2023 05:356020BChromiumµg/L 0.346
J0.246 11/29/2023 00:098260Dcis-1,2-Dichloroethene µg/L 0.200
J0.265 11/29/2023 00:098260DTrichloroetheneµg/L 0.180
V 89743SED-1
1.13 11/28/2023 21:006020BArsenicmg/Kg - dry 0.102
55.8 11/28/2023 21:006020BBariummg/Kg - dry 0.051
J0.0891 11/28/2023 21:006020BCadmiummg/Kg - dry 0.0310
26.5 11/28/2023 21:006020BChromiummg/Kg - dry 0.138
14.9 11/28/2023 21:006020BLeadmg/Kg - dry 0.0369
0.704 11/28/2023 21:006020BSeleniummg/Kg - dry 0.122
J0.0156 11/28/2023 21:006020BSilvermg/Kg - dry 0.0080
J0.0226 11/29/2023 14:487471BMercury (Total)mg/Kg - dry 0.0143
0.350 11/21/2023 11:118260DAcetonemg/Kg - dry 0.002
J0.011 11/21/2023 11:118260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J1.00 11/21/2023 17:558270EBenzo(b)fluoranthene mg/Kg - dry 0.696
J0.854 11/21/2023 17:558270EChrysenemg/Kg - dry 0.677
J1.73 11/21/2023 17:558270EFluoranthenemg/Kg - dry 0.587
J1.29 11/21/2023 17:558270EPyrenemg/Kg - dry 0.639
B0.406 12/05/2023 10:38SW-7199 Chromium, Hexavalent mg/Kg - dry 0.168
16.2 11/21/2023 12:30SW-DRYWT Moisture %
Page 4 of 117
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-321-0112
Report Limit
Project:Former Winston Container
V 89744SED-2
0.885 11/28/2023 21:046020BArsenicmg/Kg - dry 0.0930
45.1 11/28/2023 21:046020BBariummg/Kg - dry 0.046
J0.0643 11/28/2023 21:046020BCadmiummg/Kg - dry 0.0282
22.5 11/28/2023 21:046020BChromiummg/Kg - dry 0.126
9.09 11/28/2023 21:046020BLeadmg/Kg - dry 0.0337
1.05 11/28/2023 21:046020BSeleniummg/Kg - dry 0.112
J0.0150 11/28/2023 21:046020BSilvermg/Kg - dry 0.0073
J0.0162 11/29/2023 14:517471BMercury (Total)mg/Kg - dry 0.0131
0.211 11/21/2023 11:398260DAcetonemg/Kg - dry 0.002
J0.001 11/21/2023 11:398260D4-Isopropyl toluene mg/Kg - dry 0.001
J0.005 11/21/2023 11:398260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.002 11/21/2023 11:398260DMethylene Chloride mg/Kg - dry 0.001
J0.0008 11/21/2023 11:398260DToluenemg/Kg - dry 0.0007
J0.739 11/21/2023 18:188270EBenzo(b)fluoranthene mg/Kg - dry 0.635
J0.663 11/21/2023 18:188270EChrysenemg/Kg - dry 0.618
J1.40 11/21/2023 18:188270EFluoranthenemg/Kg - dry 0.535
J1.07 11/21/2023 18:188270EPyrenemg/Kg - dry 0.583
B0.239 12/05/2023 10:49SW-7199 Chromium, Hexavalent mg/Kg - dry 0.153
8.12 11/21/2023 12:30SW-DRYWT Moisture %
V 89745DUP-2
0.555 11/28/2023 21:176020BArsenicmg/Kg - dry 0.0946
43.7 11/28/2023 21:176020BBariummg/Kg - dry 0.047
J0.0776 11/28/2023 21:176020BCadmiummg/Kg - dry 0.0287
12.8 11/28/2023 21:176020BChromiummg/Kg - dry 0.128
5.08 11/28/2023 21:176020BLeadmg/Kg - dry 0.0342
0.508 11/28/2023 21:176020BSeleniummg/Kg - dry 0.113
J0.0140 11/28/2023 21:176020BSilvermg/Kg - dry 0.0074
0.203 11/21/2023 12:068260DAcetonemg/Kg - dry 0.002
J0.0007 11/21/2023 12:068260DToluenemg/Kg - dry 0.0007
J0.718 11/21/2023 18:408270EBenzo(a)anthracene mg/Kg - dry 0.615
J0.735 11/21/2023 18:408270EBenzo(a)pyrene mg/Kg - dry 0.650
J1.08 11/21/2023 18:408270EBenzo(b)fluoranthene mg/Kg - dry 0.646
J0.625 11/21/2023 18:408270EBenzo(g,h,i)perylene mg/Kg - dry 0.601
J0.583 11/21/2023 18:408270EBis(2-ethylhexyl)phthalate mg/Kg - dry 0.531
J1.02 11/21/2023 18:408270EChrysenemg/Kg - dry 0.628
J2.18 11/21/2023 18:408270EFluoranthenemg/Kg - dry 0.544
Page 5 of 117
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-321-0112
Report Limit
Project:Former Winston Container
V 89745DUP-2
J1.70 11/21/2023 18:408270EPyrenemg/Kg - dry 0.593
9.62 11/21/2023 12:30SW-DRYWT Moisture %
V 89746SED-3
0.691 11/28/2023 21:216020BArsenicmg/Kg - dry 0.0957
36.1 11/28/2023 21:216020BBariummg/Kg - dry 0.047
J0.0657 11/28/2023 21:216020BCadmiummg/Kg - dry 0.0291
18.3 11/28/2023 21:216020BChromiummg/Kg - dry 0.129
6.39 11/28/2023 21:216020BLeadmg/Kg - dry 0.0347
0.547 11/28/2023 21:216020BSeleniummg/Kg - dry 0.115
J0.0320 11/28/2023 21:216020BSilvermg/Kg - dry 0.0075
J0.0134 11/29/2023 15:027471BMercury (Total)mg/Kg - dry 0.0134
J0.0031 11/27/2023 23:278081BDieldrinmg/Kg - dry 0.0023
0.134 11/27/2023 23:278081BToxaphenemg/Kg - dry 0.0114
0.048 11/21/2023 12:338260DAcetonemg/Kg - dry 0.002
J0.004 11/21/2023 12:338260DMethylene Chloride mg/Kg - dry 0.001
J1.16 11/21/2023 19:038270EFluoranthenemg/Kg - dry 0.550
J0.885 11/21/2023 19:038270EPyrenemg/Kg - dry 0.600
B0.244 12/05/2023 09:54SW-7199 Chromium, Hexavalent mg/Kg - dry 0.157
10.7 11/21/2023 12:30SW-DRYWT Moisture %
Page 6 of 117

Client: Mid-Atlantic Associates, Inc. - Charlotte CASE NARRATIVE
Project: Former Winston Container Lab Report Number: 23-321-0112
Date: 12/5/2023
Metals Analyses Method 6020B Sample 89998 (FG-1) Analyte: Arsenic
QC Batch No: L719430/L718975 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 89998 (FG-1)
Analyte: Barium QC Batch No: L719430/L718975
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 89998 (FG-1)
Analyte: Chromium QC Batch No: L719430/L718975
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 89998 (FG-1) Analyte: Lead QC Batch No: L719430/L718975
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Hexavalent Chromium by Ion Chromatography Method SW-7199 Analyte: Hexavalent Chromium QC Batch No: L720352 Target analyte(s) was identified in the method blank associated with this project, below the Method Quantitation Limit. Per laboratory protocol any associated affected sample result is flagged "B" to indicate that it was detected
in the method blank.
Sample 89746 (SED-3) Analyte: Hexavalent Chromium QC Batch No: L720352/L720005 Matrix Spike Recovery Low: A measure of the sample pH and its oxidation reduction potential (ORP) indicate that the sample has reducing qualities which may not allow for the presence of Hexavalent Chromium.
Total Aqueous Mercury Analysis - CVAA Method 7470A Sample 94942 (PL-3) Analyte: Mercury QC Batch No: L719601/L719407
Page 7 of 117

The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Organochlorine Pesticides by GC Method 8081B QC Batch No: V40591/V40383 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
QC Batch No: V40591/V40383
Prep standard used in LCS/LCSD became concentrated due to the age of the standard. CCV and all surrogates associated with this batch pass indicating instrumentation running properly and no affect on the data.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Acrylonitrile QC Batch No: V40674/V40672
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: Vinyl chloride QC Batch No: V40674/V40672
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: 1-Methylnaphthalene
QC Batch No: V40413/V40378 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: 2,4-Dinitrophenol
QC Batch No: V40463/V40378 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Benzoic Acid QC Batch No: V40463/V40378 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Benzoic Acid QC Batch No: V40463/V40378 Analyte was flagged for 0% recovery in the LCS and LCSD due to the result being below the MQL. The actual result was 4.899 and 9.014 respectively, which calculates to a recovery of 9.798% and 18.028%. The LCS is failing low while the LCSD is within the acceptable recovery range. Analyte: Hexachlorocyclopentadiene QC Batch No: V40413/V40378 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Page 8 of 117

Analyte: Naphthalene QC Batch No: V40413/V40378
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Sample 89743 (SED-1) QC Batch No: V40463/V40450
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 89744 (SED-2) QC Batch No: V40463/V40450
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 89745 (DUP-2) QC Batch No: V40463/V40450
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 89746 (SED-3) QC Batch No: V40463/V40450
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Page 9 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-1
89739 Matrix:
11/17/2023 12:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.297 µg/L 0.297 1.00Arsenic 1 11/29/23 05:21 6020BCPW
42.1 µg/L 0.453 1.00Barium 1 11/29/23 05:21 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 11/29/23 05:21 6020BCPW
0.387 J µg/L 0.346 1.00Chromium 1 11/29/23 05:21 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 11/29/23 05:21 6020BCPW
<0.00010 mg/L 0.00010 0.00020Mercury (Total)1 11/29/23 14:10 7470AFDS
<0.703 µg/L 0.703 1.00Selenium 1 11/29/23 05:21 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 11/29/23 05:21 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 10 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-1
89739 Matrix:
11/17/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.80 µg/L 1.80 5.00Acetone 1 11/28/23 22:53 V40674MSA
<2.00 M µg/L 2.00 5.00Acrolein 1 11/28/23 22:53 V40674MSA
<0.230 M µg/L 0.230 5.00Acrylonitrile 1 11/28/23 22:53 V40674MSA
<0.180 µg/L 0.180 0.500Benzene 1 11/28/23 22:53 V40674MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/28/23 22:53 V40674MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/28/23 22:53 V40674MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/28/23 22:53 V40674MSA
<1.50 µg/L 1.50 5.00Bromoform 1 11/28/23 22:53 V40674MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 11/28/23 22:53 V40674MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 11/28/23 22:53 V40674MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 11/28/23 22:53 V40674MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/28/23 22:53 V40674MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 11/28/23 22:53 V40674MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/28/23 22:53 V40674MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/28/23 22:53 V40674MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/28/23 22:53 V40674MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 11/28/23 22:53 V40674MSA
<0.220 µg/L 0.220 0.500Chloroform 1 11/28/23 22:53 V40674MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 11/28/23 22:53 V40674MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/28/23 22:53 V40674MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/28/23 22:53 V40674MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 11/28/23 22:53 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 11 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-1
89739 Matrix:
11/17/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/28/23 22:53 V40674MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/28/23 22:53 V40674MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/28/23 22:53 V40674MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/28/23 22:53 V40674MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/28/23 22:53 V40674MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/28/23 22:53 V40674MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/28/23 22:53 V40674MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/28/23 22:53 V40674MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/28/23 22:53 V40674MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/28/23 22:53 V40674MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/28/23 22:53 V40674MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 11/28/23 22:53 V40674MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/28/23 22:53 V40674MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/28/23 22:53 V40674MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/28/23 22:53 V40674MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/28/23 22:53 V40674MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/28/23 22:53 V40674MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/28/23 22:53 V40674MSA
<42.0 µg/L 42.0 200Ethanol 1 11/28/23 22:53 V40674MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/28/23 22:53 V40674MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 11/28/23 22:53 V40674MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 11/28/23 22:53 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 12 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-1
89739 Matrix:
11/17/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 11/28/23 22:53 V40674MSA
<0.380 µg/L 0.380 5.002-Hexanone 1 11/28/23 22:53 V40674MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 11/28/23 22:53 V40674MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/28/23 22:53 V40674MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/28/23 22:53 V40674MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 11/28/23 22:53 V40674MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 11/28/23 22:53 V40674MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 11/28/23 22:53 V40674MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 11/28/23 22:53 V40674MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/28/23 22:53 V40674MSA
<0.220 µg/L 0.220 0.500Styrene 1 11/28/23 22:53 V40674MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/28/23 22:53 V40674MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/28/23 22:53 V40674MSA
<0.220 µg/L 0.220 0.500 1 11/28/23 22:53 V40674MSA
<0.220 µg/L 0.220 0.500 1 11/28/23 22:53 V40674MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 11/28/23 22:53 V40674MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 11/28/23 22:53 V40674MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/28/23 22:53 V40674MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/28/23 22:53 V40674MSA
<0.180 µg/L 0.180 0.500 1 11/28/23 22:53 V40674MSA
<0.180 µg/L 0.180 0.500 1 11/28/23 22:53 V40674MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 11/28/23 22:53 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 13 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-1
89739 Matrix:
11/17/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/28/23 22:53 V40674MSA
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 11/28/23 22:53 V40674MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/28/23 22:53 V40674MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 11/28/23 22:53 V40674MSA
0.457 J µg/L 0.420 1.00m,p-Xylene 1 11/28/23 22:53 V40674MSA
0.457 J µg/L 0.210 0.500Xylene (Total)1 11/28/23 22:53 V40674
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: 1,2-Dichloroethane - d4
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<0.302 µg/L 0.302 2.00Acenaphthene 1 11/20/23 19:32 V40413AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 11/20/23 19:32 V40413AMP
<2.05 µg/L 2.05 5.00Aniline 1 11/20/23 19:32 V40413AMP
<0.836 µg/L 0.836 2.00Anthracene 1 11/20/23 19:32 V40413AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 11/20/23 19:32 V40413AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 11/20/23 19:32 V40413AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 11/20/23 19:32 V40413AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 11/20/23 19:32 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 14 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-1
89739 Matrix:
11/17/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 11/20/23 19:32 V40413AMP
<1.10 µg/L 1.10 10.0Benzoic Acid 1 11/20/23 19:32 V40413AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 11/20/23 19:32 V40413AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 11/20/23 19:32 V40413AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 11/20/23 19:32 V40413AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 11/20/23 19:32 V40413AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 11/20/23 19:32 V40413AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 11/20/23 19:32 V40413AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 11/20/23 19:32 V40413AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 11/20/23 19:32 V40413AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 11/20/23 19:32 V40413AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 11/20/23 19:32 V40413AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 11/20/23 19:32 V40413AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 11/20/23 19:32 V40413AMP
<0.405 µg/L 0.405 2.00Chrysene 1 11/20/23 19:32 V40413AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 11/20/23 19:32 V40413AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 11/20/23 19:32 V40413AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 11/20/23 19:32 V40413AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 11/20/23 19:32 V40413AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 11/20/23 19:32 V40413AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 11/20/23 19:32 V40413AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 11/20/23 19:32 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 15 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-1
89739 Matrix:
11/17/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 11/20/23 19:32 V40413AMP
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 11/20/23 19:32 V40413AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 11/20/23 19:32 V40413AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 11/20/23 19:32 V40413AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 11/20/23 19:32 V40413AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 11/20/23 19:32 V40413AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 11/20/23 19:32 V40413AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 11/20/23 19:32 V40413AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 11/20/23 19:32 V40413AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 11/20/23 19:32 V40413AMP
<0.807 µg/L 0.807 2.00Fluorene 1 11/20/23 19:32 V40413AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 11/20/23 19:32 V40413AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 11/20/23 19:32 V40413AMP
<2.05 M µg/L 2.05 5.00Hexachlorocyclopentadiene 1 11/20/23 19:32 V40413AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 11/20/23 19:32 V40413AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 11/20/23 19:32 V40413AMP
<0.444 µg/L 0.444 5.00Isophorone 1 11/20/23 19:32 V40413AMP
<1.14 M µg/L 1.14 2.001-Methylnaphthalene 1 11/20/23 19:32 V40413AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 11/20/23 19:32 V40413AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 11/20/23 19:32 V40413AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 11/20/23 19:32 V40413AMP
<0.728 M µg/L 0.728 2.00Naphthalene 1 11/20/23 19:32 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 16 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-1
89739 Matrix:
11/17/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<1.39 µg/L 1.39 5.002-Nitroaniline 1 11/20/23 19:32 V40413AMP
<1.39 µg/L 1.39 5.003-Nitroaniline 1 11/20/23 19:32 V40413AMP
<1.53 µg/L 1.53 5.004-Nitroaniline 1 11/20/23 19:32 V40413AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 11/20/23 19:32 V40413AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 11/20/23 19:32 V40413AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 11/20/23 19:32 V40413AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 11/20/23 19:32 V40413AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 11/20/23 19:32 V40413AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 11/20/23 19:32 V40413AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 11/20/23 19:32 V40413AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 11/20/23 19:32 V40413AMP
<0.651 µg/L 0.651 5.00Phenol 1 11/20/23 19:32 V40413AMP
<0.434 µg/L 0.434 2.00Pyrene 1 11/20/23 19:32 V40413AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 11/20/23 19:32 V40413AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 11/20/23 19:32 V40413AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 11/20/23 19:32 V40413AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 17 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-2
89740 Matrix:
11/17/2023 11:20
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.297 µg/L 0.297 1.00Arsenic 1 11/29/23 05:26 6020BCPW
44.8 µg/L 0.453 1.00Barium 1 11/29/23 05:26 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 11/29/23 05:26 6020BCPW
0.506 J µg/L 0.346 1.00Chromium 1 11/29/23 05:26 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 11/29/23 05:26 6020BCPW
<0.00010 mg/L 0.00010 0.00020Mercury (Total)1 11/29/23 14:11 7470AFDS
<0.703 µg/L 0.703 1.00Selenium 1 11/29/23 05:26 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 11/29/23 05:26 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 18 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-2
89740 Matrix:
11/17/2023 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.80 µg/L 1.80 5.00Acetone 1 11/28/23 23:18 V40674MSA
<2.00 M µg/L 2.00 5.00Acrolein 1 11/28/23 23:18 V40674MSA
<0.230 M µg/L 0.230 5.00Acrylonitrile 1 11/28/23 23:18 V40674MSA
<0.180 µg/L 0.180 0.500Benzene 1 11/28/23 23:18 V40674MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/28/23 23:18 V40674MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/28/23 23:18 V40674MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/28/23 23:18 V40674MSA
<1.50 µg/L 1.50 5.00Bromoform 1 11/28/23 23:18 V40674MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 11/28/23 23:18 V40674MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 11/28/23 23:18 V40674MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 11/28/23 23:18 V40674MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/28/23 23:18 V40674MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 11/28/23 23:18 V40674MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/28/23 23:18 V40674MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/28/23 23:18 V40674MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/28/23 23:18 V40674MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 11/28/23 23:18 V40674MSA
<0.220 µg/L 0.220 0.500Chloroform 1 11/28/23 23:18 V40674MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 11/28/23 23:18 V40674MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/28/23 23:18 V40674MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/28/23 23:18 V40674MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 11/28/23 23:18 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 19 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-2
89740 Matrix:
11/17/2023 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/28/23 23:18 V40674MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/28/23 23:18 V40674MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/28/23 23:18 V40674MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/28/23 23:18 V40674MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/28/23 23:18 V40674MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/28/23 23:18 V40674MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/28/23 23:18 V40674MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/28/23 23:18 V40674MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/28/23 23:18 V40674MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/28/23 23:18 V40674MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/28/23 23:18 V40674MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 11/28/23 23:18 V40674MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/28/23 23:18 V40674MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/28/23 23:18 V40674MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/28/23 23:18 V40674MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/28/23 23:18 V40674MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/28/23 23:18 V40674MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/28/23 23:18 V40674MSA
<42.0 µg/L 42.0 200Ethanol 1 11/28/23 23:18 V40674MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/28/23 23:18 V40674MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 11/28/23 23:18 V40674MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 11/28/23 23:18 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 20 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-2
89740 Matrix:
11/17/2023 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 11/28/23 23:18 V40674MSA
<0.380 µg/L 0.380 5.002-Hexanone 1 11/28/23 23:18 V40674MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 11/28/23 23:18 V40674MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/28/23 23:18 V40674MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/28/23 23:18 V40674MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 11/28/23 23:18 V40674MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 11/28/23 23:18 V40674MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 11/28/23 23:18 V40674MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 11/28/23 23:18 V40674MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/28/23 23:18 V40674MSA
<0.220 µg/L 0.220 0.500Styrene 1 11/28/23 23:18 V40674MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/28/23 23:18 V40674MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/28/23 23:18 V40674MSA
<0.220 µg/L 0.220 0.500 1 11/28/23 23:18 V40674MSA
<0.220 µg/L 0.220 0.500 1 11/28/23 23:18 V40674MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 11/28/23 23:18 V40674MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 11/28/23 23:18 V40674MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/28/23 23:18 V40674MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/28/23 23:18 V40674MSA
0.408 J µg/L 0.180 0.500 1 11/28/23 23:18 V40674MSA
<0.180 µg/L 0.180 0.500 1 11/28/23 23:18 V40674MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 11/28/23 23:18 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 21 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-2
89740 Matrix:
11/17/2023 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/28/23 23:18 V40674MSA
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 11/28/23 23:18 V40674MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/28/23 23:18 V40674MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 11/28/23 23:18 V40674MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/28/23 23:18 V40674MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/28/23 23:18 V40674
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: 1,2-Dichloroethane - d4
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<0.302 µg/L 0.302 2.00Acenaphthene 1 11/20/23 19:55 V40413AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 11/20/23 19:55 V40413AMP
<2.05 µg/L 2.05 5.00Aniline 1 11/20/23 19:55 V40413AMP
<0.836 µg/L 0.836 2.00Anthracene 1 11/20/23 19:55 V40413AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 11/20/23 19:55 V40413AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 11/20/23 19:55 V40413AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 11/20/23 19:55 V40413AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 11/20/23 19:55 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 22 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-2
89740 Matrix:
11/17/2023 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 11/20/23 19:55 V40413AMP
<1.10 µg/L 1.10 10.0Benzoic Acid 1 11/20/23 19:55 V40413AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 11/20/23 19:55 V40413AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 11/20/23 19:55 V40413AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 11/20/23 19:55 V40413AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 11/20/23 19:55 V40413AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 11/20/23 19:55 V40413AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 11/20/23 19:55 V40413AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 11/20/23 19:55 V40413AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 11/20/23 19:55 V40413AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 11/20/23 19:55 V40413AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 11/20/23 19:55 V40413AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 11/20/23 19:55 V40413AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 11/20/23 19:55 V40413AMP
<0.405 µg/L 0.405 2.00Chrysene 1 11/20/23 19:55 V40413AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 11/20/23 19:55 V40413AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 11/20/23 19:55 V40413AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 11/20/23 19:55 V40413AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 11/20/23 19:55 V40413AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 11/20/23 19:55 V40413AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 11/20/23 19:55 V40413AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 11/20/23 19:55 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 23 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-2
89740 Matrix:
11/17/2023 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 11/20/23 19:55 V40413AMP
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 11/20/23 19:55 V40413AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 11/20/23 19:55 V40413AMP
2.54 J µg/L 2.06 5.00Di-n-butyl phthalate 1 11/20/23 19:55 V40413AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 11/20/23 19:55 V40413AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 11/20/23 19:55 V40413AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 11/20/23 19:55 V40413AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 11/20/23 19:55 V40413AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 11/20/23 19:55 V40413AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 11/20/23 19:55 V40413AMP
<0.807 µg/L 0.807 2.00Fluorene 1 11/20/23 19:55 V40413AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 11/20/23 19:55 V40413AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 11/20/23 19:55 V40413AMP
<2.05 M µg/L 2.05 5.00Hexachlorocyclopentadiene 1 11/20/23 19:55 V40413AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 11/20/23 19:55 V40413AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 11/20/23 19:55 V40413AMP
<0.444 µg/L 0.444 5.00Isophorone 1 11/20/23 19:55 V40413AMP
<1.14 M µg/L 1.14 2.001-Methylnaphthalene 1 11/20/23 19:55 V40413AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 11/20/23 19:55 V40413AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 11/20/23 19:55 V40413AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 11/20/23 19:55 V40413AMP
<0.728 M µg/L 0.728 2.00Naphthalene 1 11/20/23 19:55 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 24 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-2
89740 Matrix:
11/17/2023 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<1.39 µg/L 1.39 5.002-Nitroaniline 1 11/20/23 19:55 V40413AMP
<1.39 µg/L 1.39 5.003-Nitroaniline 1 11/20/23 19:55 V40413AMP
<1.53 µg/L 1.53 5.004-Nitroaniline 1 11/20/23 19:55 V40413AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 11/20/23 19:55 V40413AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 11/20/23 19:55 V40413AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 11/20/23 19:55 V40413AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 11/20/23 19:55 V40413AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 11/20/23 19:55 V40413AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 11/20/23 19:55 V40413AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 11/20/23 19:55 V40413AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 11/20/23 19:55 V40413AMP
<0.651 µg/L 0.651 5.00Phenol 1 11/20/23 19:55 V40413AMP
<0.434 µg/L 0.434 2.00Pyrene 1 11/20/23 19:55 V40413AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 11/20/23 19:55 V40413AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 11/20/23 19:55 V40413AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 11/20/23 19:55 V40413AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 25 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:Dup-1
89741 Matrix:
11/17/2023 0:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.297 µg/L 0.297 1.00Arsenic 1 11/29/23 05:30 6020BCPW
46.7 µg/L 0.453 1.00Barium 1 11/29/23 05:30 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 11/29/23 05:30 6020BCPW
<0.346 µg/L 0.346 1.00Chromium 1 11/29/23 05:30 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 11/29/23 05:30 6020BCPW
<0.00010 mg/L 0.00010 0.00020Mercury (Total)1 11/29/23 14:13 7470AFDS
<0.703 µg/L 0.703 1.00Selenium 1 11/29/23 05:30 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 11/29/23 05:30 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 26 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:Dup-1
89741 Matrix:
11/17/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.80 µg/L 1.80 5.00Acetone 1 11/28/23 23:44 V40674MSA
<2.00 M µg/L 2.00 5.00Acrolein 1 11/28/23 23:44 V40674MSA
<0.230 M µg/L 0.230 5.00Acrylonitrile 1 11/28/23 23:44 V40674MSA
<0.180 µg/L 0.180 0.500Benzene 1 11/28/23 23:44 V40674MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/28/23 23:44 V40674MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/28/23 23:44 V40674MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/28/23 23:44 V40674MSA
<1.50 µg/L 1.50 5.00Bromoform 1 11/28/23 23:44 V40674MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 11/28/23 23:44 V40674MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 11/28/23 23:44 V40674MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 11/28/23 23:44 V40674MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/28/23 23:44 V40674MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 11/28/23 23:44 V40674MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/28/23 23:44 V40674MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/28/23 23:44 V40674MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/28/23 23:44 V40674MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 11/28/23 23:44 V40674MSA
<0.220 µg/L 0.220 0.500Chloroform 1 11/28/23 23:44 V40674MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 11/28/23 23:44 V40674MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/28/23 23:44 V40674MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/28/23 23:44 V40674MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 11/28/23 23:44 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 27 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:Dup-1
89741 Matrix:
11/17/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/28/23 23:44 V40674MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/28/23 23:44 V40674MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/28/23 23:44 V40674MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/28/23 23:44 V40674MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/28/23 23:44 V40674MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/28/23 23:44 V40674MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/28/23 23:44 V40674MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/28/23 23:44 V40674MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/28/23 23:44 V40674MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/28/23 23:44 V40674MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/28/23 23:44 V40674MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 11/28/23 23:44 V40674MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/28/23 23:44 V40674MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/28/23 23:44 V40674MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/28/23 23:44 V40674MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/28/23 23:44 V40674MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/28/23 23:44 V40674MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/28/23 23:44 V40674MSA
<42.0 µg/L 42.0 200Ethanol 1 11/28/23 23:44 V40674MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/28/23 23:44 V40674MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 11/28/23 23:44 V40674MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 11/28/23 23:44 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 28 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:Dup-1
89741 Matrix:
11/17/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 11/28/23 23:44 V40674MSA
<0.380 µg/L 0.380 5.002-Hexanone 1 11/28/23 23:44 V40674MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 11/28/23 23:44 V40674MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/28/23 23:44 V40674MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/28/23 23:44 V40674MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 11/28/23 23:44 V40674MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 11/28/23 23:44 V40674MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 11/28/23 23:44 V40674MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 11/28/23 23:44 V40674MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/28/23 23:44 V40674MSA
<0.220 µg/L 0.220 0.500Styrene 1 11/28/23 23:44 V40674MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/28/23 23:44 V40674MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/28/23 23:44 V40674MSA
<0.220 µg/L 0.220 0.500 1 11/28/23 23:44 V40674MSA
<0.220 µg/L 0.220 0.500 1 11/28/23 23:44 V40674MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 11/28/23 23:44 V40674MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 11/28/23 23:44 V40674MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/28/23 23:44 V40674MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/28/23 23:44 V40674MSA
0.287 J µg/L 0.180 0.500 1 11/28/23 23:44 V40674MSA
<0.180 µg/L 0.180 0.500 1 11/28/23 23:44 V40674MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 11/28/23 23:44 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 29 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:Dup-1
89741 Matrix:
11/17/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/28/23 23:44 V40674MSA
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 11/28/23 23:44 V40674MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/28/23 23:44 V40674MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 11/28/23 23:44 V40674MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/28/23 23:44 V40674MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/28/23 23:44 V40674
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: 1,2-Dichloroethane - d4
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<0.302 µg/L 0.302 2.00Acenaphthene 1 11/20/23 20:17 V40413AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 11/20/23 20:17 V40413AMP
<2.05 µg/L 2.05 5.00Aniline 1 11/20/23 20:17 V40413AMP
<0.836 µg/L 0.836 2.00Anthracene 1 11/20/23 20:17 V40413AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 11/20/23 20:17 V40413AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 11/20/23 20:17 V40413AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 11/20/23 20:17 V40413AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 11/20/23 20:17 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 30 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:Dup-1
89741 Matrix:
11/17/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 11/20/23 20:17 V40413AMP
<1.10 µg/L 1.10 10.0Benzoic Acid 1 11/20/23 20:17 V40413AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 11/20/23 20:17 V40413AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 11/20/23 20:17 V40413AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 11/20/23 20:17 V40413AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 11/20/23 20:17 V40413AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 11/20/23 20:17 V40413AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 11/20/23 20:17 V40413AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 11/20/23 20:17 V40413AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 11/20/23 20:17 V40413AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 11/20/23 20:17 V40413AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 11/20/23 20:17 V40413AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 11/20/23 20:17 V40413AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 11/20/23 20:17 V40413AMP
<0.405 µg/L 0.405 2.00Chrysene 1 11/20/23 20:17 V40413AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 11/20/23 20:17 V40413AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 11/20/23 20:17 V40413AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 11/20/23 20:17 V40413AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 11/20/23 20:17 V40413AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 11/20/23 20:17 V40413AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 11/20/23 20:17 V40413AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 11/20/23 20:17 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 31 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:Dup-1
89741 Matrix:
11/17/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 11/20/23 20:17 V40413AMP
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 11/20/23 20:17 V40413AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 11/20/23 20:17 V40413AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 11/20/23 20:17 V40413AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 11/20/23 20:17 V40413AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 11/20/23 20:17 V40413AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 11/20/23 20:17 V40413AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 11/20/23 20:17 V40413AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 11/20/23 20:17 V40413AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 11/20/23 20:17 V40413AMP
<0.807 µg/L 0.807 2.00Fluorene 1 11/20/23 20:17 V40413AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 11/20/23 20:17 V40413AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 11/20/23 20:17 V40413AMP
<2.05 M µg/L 2.05 5.00Hexachlorocyclopentadiene 1 11/20/23 20:17 V40413AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 11/20/23 20:17 V40413AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 11/20/23 20:17 V40413AMP
<0.444 µg/L 0.444 5.00Isophorone 1 11/20/23 20:17 V40413AMP
<1.14 M µg/L 1.14 2.001-Methylnaphthalene 1 11/20/23 20:17 V40413AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 11/20/23 20:17 V40413AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 11/20/23 20:17 V40413AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 11/20/23 20:17 V40413AMP
<0.728 M µg/L 0.728 2.00Naphthalene 1 11/20/23 20:17 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 32 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:Dup-1
89741 Matrix:
11/17/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<1.39 µg/L 1.39 5.002-Nitroaniline 1 11/20/23 20:17 V40413AMP
<1.39 µg/L 1.39 5.003-Nitroaniline 1 11/20/23 20:17 V40413AMP
<1.53 µg/L 1.53 5.004-Nitroaniline 1 11/20/23 20:17 V40413AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 11/20/23 20:17 V40413AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 11/20/23 20:17 V40413AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 11/20/23 20:17 V40413AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 11/20/23 20:17 V40413AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 11/20/23 20:17 V40413AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 11/20/23 20:17 V40413AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 11/20/23 20:17 V40413AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 11/20/23 20:17 V40413AMP
<0.651 µg/L 0.651 5.00Phenol 1 11/20/23 20:17 V40413AMP
<0.434 µg/L 0.434 2.00Pyrene 1 11/20/23 20:17 V40413AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 11/20/23 20:17 V40413AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 11/20/23 20:17 V40413AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 11/20/23 20:17 V40413AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 33 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-3
89742 Matrix:
11/17/2023 10:40
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.297 µg/L 0.297 1.00Arsenic 1 11/29/23 05:35 6020BCPW
46.4 µg/L 0.453 1.00Barium 1 11/29/23 05:35 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 11/29/23 05:35 6020BCPW
0.445 J µg/L 0.346 1.00Chromium 1 11/29/23 05:35 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 11/29/23 05:35 6020BCPW
<0.00010 mg/L 0.00010 0.00020Mercury (Total)1 11/29/23 14:14 7470AFDS
<0.703 µg/L 0.703 1.00Selenium 1 11/29/23 05:35 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 11/29/23 05:35 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 34 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-3
89742 Matrix:
11/17/2023 10:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.80 µg/L 1.80 5.00Acetone 1 11/29/23 00:09 V40674MSA
<2.00 M µg/L 2.00 5.00Acrolein 1 11/29/23 00:09 V40674MSA
<0.230 M µg/L 0.230 5.00Acrylonitrile 1 11/29/23 00:09 V40674MSA
<0.180 µg/L 0.180 0.500Benzene 1 11/29/23 00:09 V40674MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/29/23 00:09 V40674MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/29/23 00:09 V40674MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/29/23 00:09 V40674MSA
<1.50 µg/L 1.50 5.00Bromoform 1 11/29/23 00:09 V40674MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 11/29/23 00:09 V40674MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 11/29/23 00:09 V40674MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 11/29/23 00:09 V40674MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/29/23 00:09 V40674MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 11/29/23 00:09 V40674MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/29/23 00:09 V40674MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/29/23 00:09 V40674MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/29/23 00:09 V40674MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 11/29/23 00:09 V40674MSA
<0.220 µg/L 0.220 0.500Chloroform 1 11/29/23 00:09 V40674MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 11/29/23 00:09 V40674MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/29/23 00:09 V40674MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/29/23 00:09 V40674MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 11/29/23 00:09 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 35 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-3
89742 Matrix:
11/17/2023 10:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/29/23 00:09 V40674MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/29/23 00:09 V40674MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/29/23 00:09 V40674MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/29/23 00:09 V40674MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/29/23 00:09 V40674MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/29/23 00:09 V40674MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/29/23 00:09 V40674MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/29/23 00:09 V40674MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/29/23 00:09 V40674MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/29/23 00:09 V40674MSA
0.246 J µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/29/23 00:09 V40674MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 11/29/23 00:09 V40674MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/29/23 00:09 V40674MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/29/23 00:09 V40674MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/29/23 00:09 V40674MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/29/23 00:09 V40674MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/29/23 00:09 V40674MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/29/23 00:09 V40674MSA
<42.0 µg/L 42.0 200Ethanol 1 11/29/23 00:09 V40674MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/29/23 00:09 V40674MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 11/29/23 00:09 V40674MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 11/29/23 00:09 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 36 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-3
89742 Matrix:
11/17/2023 10:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 11/29/23 00:09 V40674MSA
<0.380 µg/L 0.380 5.002-Hexanone 1 11/29/23 00:09 V40674MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 11/29/23 00:09 V40674MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/29/23 00:09 V40674MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/29/23 00:09 V40674MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 11/29/23 00:09 V40674MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 11/29/23 00:09 V40674MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 11/29/23 00:09 V40674MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 11/29/23 00:09 V40674MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/29/23 00:09 V40674MSA
<0.220 µg/L 0.220 0.500Styrene 1 11/29/23 00:09 V40674MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/29/23 00:09 V40674MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/29/23 00:09 V40674MSA
<0.220 µg/L 0.220 0.500 1 11/29/23 00:09 V40674MSA
<0.220 µg/L 0.220 0.500 1 11/29/23 00:09 V40674MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 11/29/23 00:09 V40674MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 11/29/23 00:09 V40674MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/29/23 00:09 V40674MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/29/23 00:09 V40674MSA
0.265 J µg/L 0.180 0.500 1 11/29/23 00:09 V40674MSA
<0.180 µg/L 0.180 0.500 1 11/29/23 00:09 V40674MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 11/29/23 00:09 V40674MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 37 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-3
89742 Matrix:
11/17/2023 10:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):11/28/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/29/23 00:09 V40674MSA
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 11/29/23 00:09 V40674MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/29/23 00:09 V40674MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 11/29/23 00:09 V40674MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/29/23 00:09 V40674MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/29/23 00:09 V40674
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: 1,2-Dichloroethane - d4
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<0.302 µg/L 0.302 2.00Acenaphthene 1 11/20/23 20:39 V40413AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 11/20/23 20:39 V40413AMP
<2.05 µg/L 2.05 5.00Aniline 1 11/20/23 20:39 V40413AMP
<0.836 µg/L 0.836 2.00Anthracene 1 11/20/23 20:39 V40413AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 11/20/23 20:39 V40413AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 11/20/23 20:39 V40413AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 11/20/23 20:39 V40413AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 11/20/23 20:39 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 38 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-3
89742 Matrix:
11/17/2023 10:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 11/20/23 20:39 V40413AMP
<1.10 µg/L 1.10 10.0Benzoic Acid 1 11/20/23 20:39 V40413AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 11/20/23 20:39 V40413AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 11/20/23 20:39 V40413AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 11/20/23 20:39 V40413AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 11/20/23 20:39 V40413AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 11/20/23 20:39 V40413AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 11/20/23 20:39 V40413AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 11/20/23 20:39 V40413AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 11/20/23 20:39 V40413AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 11/20/23 20:39 V40413AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 11/20/23 20:39 V40413AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 11/20/23 20:39 V40413AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 11/20/23 20:39 V40413AMP
<0.405 µg/L 0.405 2.00Chrysene 1 11/20/23 20:39 V40413AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 11/20/23 20:39 V40413AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 11/20/23 20:39 V40413AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 11/20/23 20:39 V40413AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 11/20/23 20:39 V40413AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 11/20/23 20:39 V40413AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 11/20/23 20:39 V40413AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 11/20/23 20:39 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 39 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-3
89742 Matrix:
11/17/2023 10:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 11/20/23 20:39 V40413AMP
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 11/20/23 20:39 V40413AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 11/20/23 20:39 V40413AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 11/20/23 20:39 V40413AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 11/20/23 20:39 V40413AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 11/20/23 20:39 V40413AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 11/20/23 20:39 V40413AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 11/20/23 20:39 V40413AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 11/20/23 20:39 V40413AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 11/20/23 20:39 V40413AMP
<0.807 µg/L 0.807 2.00Fluorene 1 11/20/23 20:39 V40413AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 11/20/23 20:39 V40413AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 11/20/23 20:39 V40413AMP
<2.05 M µg/L 2.05 5.00Hexachlorocyclopentadiene 1 11/20/23 20:39 V40413AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 11/20/23 20:39 V40413AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 11/20/23 20:39 V40413AMP
<0.444 µg/L 0.444 5.00Isophorone 1 11/20/23 20:39 V40413AMP
<1.14 M µg/L 1.14 2.001-Methylnaphthalene 1 11/20/23 20:39 V40413AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 11/20/23 20:39 V40413AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 11/20/23 20:39 V40413AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 11/20/23 20:39 V40413AMP
<0.728 M µg/L 0.728 2.00Naphthalene 1 11/20/23 20:39 V40413AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 40 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SW-3
89742 Matrix:
11/17/2023 10:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):11/20/23 11:07
<1.39 µg/L 1.39 5.002-Nitroaniline 1 11/20/23 20:39 V40413AMP
<1.39 µg/L 1.39 5.003-Nitroaniline 1 11/20/23 20:39 V40413AMP
<1.53 µg/L 1.53 5.004-Nitroaniline 1 11/20/23 20:39 V40413AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 11/20/23 20:39 V40413AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 11/20/23 20:39 V40413AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 11/20/23 20:39 V40413AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 11/20/23 20:39 V40413AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 11/20/23 20:39 V40413AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 11/20/23 20:39 V40413AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 11/20/23 20:39 V40413AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 11/20/23 20:39 V40413AMP
<0.651 µg/L 0.651 5.00Phenol 1 11/20/23 20:39 V40413AMP
<0.434 µg/L 0.434 2.00Pyrene 1 11/20/23 20:39 V40413AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 11/20/23 20:39 V40413AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 11/20/23 20:39 V40413AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 11/20/23 20:39 V40413AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 41 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-1
89743 Matrix:
11/17/2023 12:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.2 %Moisture 1 11/21/23 12:30 SW-DRYWTCNC
0.406 B mg/Kg - dry 0.168 0.238Chromium, Hexavalent 1 12/05/23 10:38 SW-7199SWB
1.13 mg/Kg - dry 0.102 0.298Arsenic 5 11/28/23 21:00 6020BCPW
55.8 mg/Kg - dry 0.051 0.298Barium 5 11/28/23 21:00 6020BCPW
0.0891 J mg/Kg - dry 0.0310 0.298Cadmium 5 11/28/23 21:00 6020BCPW
26.5 mg/Kg - dry 0.138 0.298Chromium 5 11/28/23 21:00 6020BCPW
14.9 mg/Kg - dry 0.0369 0.298Lead 5 11/28/23 21:00 6020BCPW
0.0226 J mg/Kg - dry 0.0143 0.0358Mercury (Total)1 11/29/23 14:48 7471BJKC
0.704 mg/Kg - dry 0.122 0.298Selenium 5 11/28/23 21:00 6020BCPW
0.0156 J mg/Kg - dry 0.0080 0.298Silver 5 11/28/23 21:00 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 42 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-1
89743 Matrix:
11/17/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/20/23 11:50
<0.0021 mg/Kg - dry 0.0021 0.0059Aldrin 1 11/27/23 22:46 V40591TJW
<0.0013 mg/Kg - dry 0.0013 0.0059alpha-BHC 1 11/27/23 22:46 V40591TJW
<0.0023 mg/Kg - dry 0.0023 0.0059beta-BHC 1 11/27/23 22:46 V40591TJW
<0.0014 mg/Kg - dry 0.0014 0.0059delta-BHC 1 11/27/23 22:46 V40591TJW
<0.0210 mg/Kg - dry 0.0210 0.0596Chlordane 1 11/27/23 22:46 V40591TJW
<0.0022 mg/Kg - dry 0.0022 0.0059alpha-Chlordane 1 11/27/23 22:46 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0059gamma-Chlordane 1 11/27/23 22:46 V40591TJW
<0.0022 mg/Kg - dry 0.0022 0.00594,4'-DDD 1 11/27/23 22:46 V40591TJW
<0.0024 mg/Kg - dry 0.0024 0.00594,4'-DDE 1 11/27/23 22:46 V40591TJW
<0.0018 mg/Kg - dry 0.0018 0.00594,4'-DDT 1 11/27/23 22:46 V40591TJW
<0.0024 mg/Kg - dry 0.0024 0.0059Dieldrin 1 11/27/23 22:46 V40591TJW
<0.0021 mg/Kg - dry 0.0021 0.0059Endosulfan I 1 11/27/23 22:46 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0059Endosulfan II 1 11/27/23 22:46 V40591TJW
<0.0021 mg/Kg - dry 0.0021 0.0059Endosulfan Sulfate 1 11/27/23 22:46 V40591TJW
<0.0022 mg/Kg - dry 0.0022 0.0059Endrin 1 11/27/23 22:46 V40591TJW
<0.0025 mg/Kg - dry 0.0025 0.0059Endrin Aldehyde 1 11/27/23 22:46 V40591TJW
<0.0021 mg/Kg - dry 0.0021 0.0059Endrin Ketone 1 11/27/23 22:46 V40591TJW
<0.0015 mg/Kg - dry 0.0015 0.0059gamma-BHC 1 11/27/23 22:46 V40591TJW
<0.0016 mg/Kg - dry 0.0016 0.0059Heptachlor 1 11/27/23 22:46 V40591TJW
<0.0021 mg/Kg - dry 0.0021 0.0059Heptachlor Epoxide 1 11/27/23 22:46 V40591TJW
<0.0031 mg/Kg - dry 0.0031 0.0059Methoxychlor 1 11/27/23 22:46 V40591TJW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 43 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-1
89743 Matrix:
11/17/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/20/23 11:50
<0.0121 mg/Kg - dry 0.0121 0.0596 1 11/27/23 22:46 V40591TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
0.350 mg/Kg - dry 0.002 0.023Acetone 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 11/21/23 11:11 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 11/21/23 11:11 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/21/23 11:11 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/21/23 11:11 V40484TBL
<0.0010 mg/Kg - dry 0.0010 0.005Bromochloromethane 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/21/23 11:11 V40484TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 11/21/23 11:11 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/21/23 11:11 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 11/21/23 11:11 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/21/23 11:11 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/21/23 11:11 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/21/23 11:11 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 44 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-1
89743 Matrix:
11/17/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/21/23 11:11 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.011Chloromethane 1 11/21/23 11:11 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/21/23 11:11 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 11/21/23 11:11 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 11/21/23 11:11 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/21/23 11:11 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 11/21/23 11:11 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 11/21/23 11:11 V40484TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/21/23 11:11 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,3-Dichlorobenzene 1 11/21/23 11:11 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/21/23 11:11 V40484TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/21/23 11:11 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 11/21/23 11:11 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/21/23 11:11 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/21/23 11:11 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/21/23 11:11 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 45 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-1
89743 Matrix:
11/17/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/21/23 11:11 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/21/23 11:11 V40484TBL
<0.0010 mg/Kg - dry 0.0010 0.005trans-1,3-Dichloropropene 1 11/21/23 11:11 V40484TBL
<0.016 mg/Kg - dry 0.016 0.298Ethanol 1 11/21/23 11:11 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/21/23 11:11 V40484TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 11/21/23 11:11 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/21/23 11:11 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/21/23 11:11 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 11/21/23 11:11 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/21/23 11:11 V40484TBL
0.011 J mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 11/21/23 11:11 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/21/23 11:11 V40484TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 11/21/23 11:11 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/21/23 11:11 V40484TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/21/23 11:11 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.005 1 11/21/23 11:11 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 46 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-1
89743 Matrix:
11/17/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/21/23 11:11 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/21/23 11:11 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/21/23 11:11 V40484TBL
<0.002 mg/Kg - dry 0.002 0.011 1 11/21/23 11:11 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 11/21/23 11:11 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/21/23 11:11 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/21/23 11:11 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/21/23 11:11 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/21/23 11:11 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/21/23 11:11 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/21/23 11:11 V40484
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.553 mg/Kg - dry 0.553 3.15Acenaphthene 4 11/21/23 17:55 V40463AMP
<0.501 mg/Kg - dry 0.501 3.15Acenaphthylene 4 11/21/23 17:55 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 47 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-1
89743 Matrix:
11/17/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.725 mg/Kg - dry 0.725 3.15Aniline 4 11/21/23 17:55 V40463AMP
<0.682 mg/Kg - dry 0.682 3.15Anthracene 4 11/21/23 17:55 V40463AMP
<0.663 mg/Kg - dry 0.663 3.15Benzo(a)anthracene 4 11/21/23 17:55 V40463AMP
<0.701 mg/Kg - dry 0.701 3.15Benzo(a)pyrene 4 11/21/23 17:55 V40463AMP
1.00 J mg/Kg - dry 0.696 3.15Benzo(b)fluoranthene 4 11/21/23 17:55 V40463AMP
<0.649 mg/Kg - dry 0.649 3.15Benzo(g,h,i)perylene 4 11/21/23 17:55 V40463AMP
<0.653 mg/Kg - dry 0.653 3.15Benzo(k)fluoranthene 4 11/21/23 17:55 V40463AMP
<2.77 M mg/Kg - dry 2.77 9.56Benzoic Acid 4 11/21/23 17:55 V40463AMP
<0.501 mg/Kg - dry 0.501 3.15Benzyl alcohol 4 11/21/23 17:55 V40463AMP
<0.563 mg/Kg - dry 0.563 3.15Bis(2-Chloroethoxy)methane 4 11/21/23 17:55 V40463AMP
<0.510 mg/Kg - dry 0.510 3.15Bis(2-Chloroethyl)ether 4 11/21/23 17:55 V40463AMP
<0.649 mg/Kg - dry 0.649 1.58Bis(2-Chloroisopropyl)ether 4 11/21/23 17:55 V40463AMP
<0.572 mg/Kg - dry 0.572 3.15Bis(2-ethylhexyl)phthalate 4 11/21/23 17:55 V40463AMP
<0.520 mg/Kg - dry 0.520 3.154-Bromophenyl phenyl ether 4 11/21/23 17:55 V40463AMP
<0.539 mg/Kg - dry 0.539 1.58Butyl benzyl phthalate 4 11/21/23 17:55 V40463AMP
<0.441 mg/Kg - dry 0.441 3.154-Chloro-3-methylphenol 4 11/21/23 17:55 V40463AMP
<0.534 mg/Kg - dry 0.534 1.584-Chloroaniline 4 11/21/23 17:55 V40463AMP
<0.553 mg/Kg - dry 0.553 3.152-Chloronaphthalene 4 11/21/23 17:55 V40463AMP
<0.468 mg/Kg - dry 0.468 3.152-Chlorophenol 4 11/21/23 17:55 V40463AMP
<0.601 mg/Kg - dry 0.601 4.774-Chlorophenyl phenyl ether 4 11/21/23 17:55 V40463AMP
0.854 J mg/Kg - dry 0.677 3.15Chrysene 4 11/21/23 17:55 V40463AMP
<1.10 mg/Kg - dry 1.10 3.15Dibenz(a,h)anthracene 4 11/21/23 17:55 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 48 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-1
89743 Matrix:
11/17/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.568 mg/Kg - dry 0.568 3.15Dibenzofuran 4 11/21/23 17:55 V40463AMP
<0.451 mg/Kg - dry 0.451 3.151,2-Dichlorobenzene 4 11/21/23 17:55 V40463AMP
<0.464 mg/Kg - dry 0.464 3.151,3-Dichlorobenzene 4 11/21/23 17:55 V40463AMP
<0.465 mg/Kg - dry 0.465 1.581,4-Dichlorobenzene 4 11/21/23 17:55 V40463AMP
<0.701 mg/Kg - dry 0.701 3.153,3'-Dichlorobenzidine 4 11/21/23 17:55 V40463AMP
<0.457 mg/Kg - dry 0.457 3.152,4-Dichlorophenol 4 11/21/23 17:55 V40463AMP
<0.859 mg/Kg - dry 0.859 3.15Diethyl phthalate 4 11/21/23 17:55 V40463AMP
<0.830 mg/Kg - dry 0.830 3.15Dimethyl phthalate 4 11/21/23 17:55 V40463AMP
<0.515 mg/Kg - dry 0.515 1.582,4-Dimethylphenol 4 11/21/23 17:55 V40463AMP
<0.510 mg/Kg - dry 0.510 3.15Di-n-butyl phthalate 4 11/21/23 17:55 V40463AMP
<1.15 mg/Kg - dry 1.15 7.174,6-Dinitro-2-methylphenol 4 11/21/23 17:55 V40463AMP
<2.48 mg/Kg - dry 2.48 7.172,4-Dinitrophenol 4 11/21/23 17:55 V40463AMP
<0.460 mg/Kg - dry 0.460 3.152,4-Dinitrotoluene 4 11/21/23 17:55 V40463AMP
<0.515 mg/Kg - dry 0.515 3.152,6-Dinitrotoluene 4 11/21/23 17:55 V40463AMP
<0.682 mg/Kg - dry 0.682 1.58Di-n-Octyl Phthalate 4 11/21/23 17:55 V40463AMP
1.73 J mg/Kg - dry 0.587 3.15Fluoranthene 4 11/21/23 17:55 V40463AMP
<0.610 mg/Kg - dry 0.610 3.15Fluorene 4 11/21/23 17:55 V40463AMP
<0.505 mg/Kg - dry 0.505 3.15Hexachlorobenzene 4 11/21/23 17:55 V40463AMP
<0.465 mg/Kg - dry 0.465 3.15Hexachlorobutadiene 4 11/21/23 17:55 V40463AMP
<0.749 mg/Kg - dry 0.749 3.15Hexachlorocyclopentadiene 4 11/21/23 17:55 V40463AMP
<0.378 mg/Kg - dry 0.378 3.15Hexachloroethane 4 11/21/23 17:55 V40463AMP
<0.854 mg/Kg - dry 0.854 3.15Indeno(1,2,3-cd)pyrene 4 11/21/23 17:55 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 49 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-1
89743 Matrix:
11/17/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.911 mg/Kg - dry 0.911 3.15Isophorone 4 11/21/23 17:55 V40463AMP
<0.505 mg/Kg - dry 0.505 3.151-Methylnaphthalene 4 11/21/23 17:55 V40463AMP
<0.477 mg/Kg - dry 0.477 3.152-Methylnaphthalene 4 11/21/23 17:55 V40463AMP
<0.463 mg/Kg - dry 0.463 3.152-Methylphenol 4 11/21/23 17:55 V40463AMP
<0.405 mg/Kg - dry 0.405 3.153&4 Methylphenol 4 11/21/23 17:55 V40463AMP
<0.687 mg/Kg - dry 0.687 3.15Naphthalene 4 11/21/23 17:55 V40463AMP
<0.461 mg/Kg - dry 0.461 3.152-Nitroaniline 4 11/21/23 17:55 V40463AMP
<0.572 mg/Kg - dry 0.572 3.153-Nitroaniline 4 11/21/23 17:55 V40463AMP
<0.445 mg/Kg - dry 0.445 1.584-Nitroaniline 4 11/21/23 17:55 V40463AMP
<0.553 mg/Kg - dry 0.553 1.58Nitrobenzene 4 11/21/23 17:55 V40463AMP
<0.423 mg/Kg - dry 0.423 3.152-Nitrophenol 4 11/21/23 17:55 V40463AMP
<0.558 mg/Kg - dry 0.558 3.154-Nitrophenol 4 11/21/23 17:55 V40463AMP
<1.25 mg/Kg - dry 1.25 3.15N-Nitrosodimethylamine 4 11/21/23 17:55 V40463AMP
<0.863 mg/Kg - dry 0.863 3.15N-Nitrosodiphenylamine 4 11/21/23 17:55 V40463AMP
<0.563 mg/Kg - dry 0.563 3.15N-Nitroso-di-n-propylamine 4 11/21/23 17:55 V40463AMP
<1.66 mg/Kg - dry 1.66 4.77Pentachlorophenol 4 11/21/23 17:55 V40463AMP
<0.992 mg/Kg - dry 0.992 3.15Phenanthrene 4 11/21/23 17:55 V40463AMP
<0.534 mg/Kg - dry 0.534 3.15Phenol 4 11/21/23 17:55 V40463AMP
1.29 J mg/Kg - dry 0.639 3.15Pyrene 4 11/21/23 17:55 V40463AMP
<0.510 mg/Kg - dry 0.510 3.151,2,4-Trichlorobenzene 4 11/21/23 17:55 V40463AMP
<0.459 mg/Kg - dry 0.459 3.152,4,5-Trichlorophenol 4 11/21/23 17:55 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 50 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-1
89743 Matrix:
11/17/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.460 mg/Kg - dry 0.460 3.152,4,6-Trichlorophenol 4 11/21/23 17:55 V40463AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 51 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-2
89744 Matrix:
11/17/2023 11:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
8.12 %Moisture 1 11/21/23 12:30 SW-DRYWTCNC
0.239 B mg/Kg - dry 0.153 0.217Chromium, Hexavalent 1 12/05/23 10:49 SW-7199SWB
0.885 mg/Kg - dry 0.0930 0.272Arsenic 5 11/28/23 21:04 6020BCPW
45.1 mg/Kg - dry 0.046 0.272Barium 5 11/28/23 21:04 6020BCPW
0.0643 J mg/Kg - dry 0.0282 0.272Cadmium 5 11/28/23 21:04 6020BCPW
22.5 mg/Kg - dry 0.126 0.272Chromium 5 11/28/23 21:04 6020BCPW
9.09 mg/Kg - dry 0.0337 0.272Lead 5 11/28/23 21:04 6020BCPW
0.0162 J mg/Kg - dry 0.0131 0.0327Mercury (Total)1 11/29/23 14:51 7471BJKC
1.05 mg/Kg - dry 0.112 0.272Selenium 5 11/28/23 21:04 6020BCPW
0.0150 J mg/Kg - dry 0.0073 0.272Silver 5 11/28/23 21:04 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 52 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-2
89744 Matrix:
11/17/2023 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/20/23 11:50
<0.0020 mg/Kg - dry 0.0020 0.0054Aldrin 1 11/27/23 23:00 V40591TJW
<0.0012 mg/Kg - dry 0.0012 0.0054alpha-BHC 1 11/27/23 23:00 V40591TJW
<0.0021 mg/Kg - dry 0.0021 0.0054beta-BHC 1 11/27/23 23:00 V40591TJW
<0.0013 mg/Kg - dry 0.0013 0.0054delta-BHC 1 11/27/23 23:00 V40591TJW
<0.0191 mg/Kg - dry 0.0191 0.0544Chlordane 1 11/27/23 23:00 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0054alpha-Chlordane 1 11/27/23 23:00 V40591TJW
<0.0018 mg/Kg - dry 0.0018 0.0054gamma-Chlordane 1 11/27/23 23:00 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.00544,4'-DDD 1 11/27/23 23:00 V40591TJW
<0.0022 mg/Kg - dry 0.0022 0.00544,4'-DDE 1 11/27/23 23:00 V40591TJW
<0.0016 mg/Kg - dry 0.0016 0.00544,4'-DDT 1 11/27/23 23:00 V40591TJW
<0.0022 mg/Kg - dry 0.0022 0.0054Dieldrin 1 11/27/23 23:00 V40591TJW
<0.0019 mg/Kg - dry 0.0019 0.0054Endosulfan I 1 11/27/23 23:00 V40591TJW
<0.0019 mg/Kg - dry 0.0019 0.0054Endosulfan II 1 11/27/23 23:00 V40591TJW
<0.0019 mg/Kg - dry 0.0019 0.0054Endosulfan Sulfate 1 11/27/23 23:00 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0054Endrin 1 11/27/23 23:00 V40591TJW
<0.0022 mg/Kg - dry 0.0022 0.0054Endrin Aldehyde 1 11/27/23 23:00 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0054Endrin Ketone 1 11/27/23 23:00 V40591TJW
<0.0013 mg/Kg - dry 0.0013 0.0054gamma-BHC 1 11/27/23 23:00 V40591TJW
<0.0014 mg/Kg - dry 0.0014 0.0054Heptachlor 1 11/27/23 23:00 V40591TJW
<0.0019 mg/Kg - dry 0.0019 0.0054Heptachlor Epoxide 1 11/27/23 23:00 V40591TJW
<0.0028 mg/Kg - dry 0.0028 0.0054Methoxychlor 1 11/27/23 23:00 V40591TJW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 53 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-2
89744 Matrix:
11/17/2023 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/20/23 11:50
<0.0111 mg/Kg - dry 0.0111 0.0544 1 11/27/23 23:00 V40591TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
0.211 mg/Kg - dry 0.002 0.021Acetone 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.021Acrolein 1 11/21/23 11:39 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 11/21/23 11:39 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 11/21/23 11:39 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 11/21/23 11:39 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.010Bromomethane 1 11/21/23 11:39 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 11/21/23 11:39 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/21/23 11:39 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 11/21/23 11:39 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/21/23 11:39 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 11/21/23 11:39 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 54 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-2
89744 Matrix:
11/17/2023 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 11/21/23 11:39 V40484TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/21/23 11:39 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 11/21/23 11:39 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/21/23 11:39 V40484TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/21/23 11:39 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/21/23 11:39 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 11/21/23 11:39 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 11/21/23 11:39 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/21/23 11:39 V40484TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 11/21/23 11:39 V40484TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/21/23 11:39 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 11/21/23 11:39 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/21/23 11:39 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/21/23 11:39 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/21/23 11:39 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/21/23 11:39 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/21/23 11:39 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 55 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-2
89744 Matrix:
11/17/2023 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 11/21/23 11:39 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/21/23 11:39 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/21/23 11:39 V40484TBL
<0.015 mg/Kg - dry 0.015 0.272Ethanol 1 11/21/23 11:39 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 11/21/23 11:39 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.054Ethyl Tertiary Butyl Ether (ETBE)1 11/21/23 11:39 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.010Hexachlorobutadiene 1 11/21/23 11:39 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 11/21/23 11:39 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0212-Hexanone 1 11/21/23 11:39 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/21/23 11:39 V40484TBL
0.001 J mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/21/23 11:39 V40484TBL
0.005 J mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 11/21/23 11:39 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/21/23 11:39 V40484TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 11/21/23 11:39 V40484TBL
0.002 J mg/Kg - dry 0.001 0.010Methylene Chloride 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.010Naphthalene 1 11/21/23 11:39 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/21/23 11:39 V40484TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 11/21/23 11:39 V40484TBL
<0.0010 mg/Kg - dry 0.0010 0.005 1 11/21/23 11:39 V40484TBL
0.0008 J mg/Kg - dry 0.0007 0.005 1 11/21/23 11:39 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 56 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-2
89744 Matrix:
11/17/2023 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 11/21/23 11:39 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/21/23 11:39 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/21/23 11:39 V40484TBL
<0.002 mg/Kg - dry 0.002 0.010 1 11/21/23 11:39 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/21/23 11:39 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/21/23 11:39 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 11/21/23 11:39 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 11/21/23 11:39 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 11/21/23 11:39 V40484TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 11/21/23 11:39 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 11/21/23 11:39 V40484
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.505 mg/Kg - dry 0.505 2.87Acenaphthene 4 11/21/23 18:18 V40463AMP
<0.457 mg/Kg - dry 0.457 2.87Acenaphthylene 4 11/21/23 18:18 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 57 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-2
89744 Matrix:
11/17/2023 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.661 mg/Kg - dry 0.661 2.87Aniline 4 11/21/23 18:18 V40463AMP
<0.622 mg/Kg - dry 0.622 2.87Anthracene 4 11/21/23 18:18 V40463AMP
<0.605 mg/Kg - dry 0.605 2.87Benzo(a)anthracene 4 11/21/23 18:18 V40463AMP
<0.639 mg/Kg - dry 0.639 2.87Benzo(a)pyrene 4 11/21/23 18:18 V40463AMP
0.739 J mg/Kg - dry 0.635 2.87Benzo(b)fluoranthene 4 11/21/23 18:18 V40463AMP
<0.592 mg/Kg - dry 0.592 2.87Benzo(g,h,i)perylene 4 11/21/23 18:18 V40463AMP
<0.596 mg/Kg - dry 0.596 2.87Benzo(k)fluoranthene 4 11/21/23 18:18 V40463AMP
<2.53 M mg/Kg - dry 2.53 8.71Benzoic Acid 4 11/21/23 18:18 V40463AMP
<0.457 mg/Kg - dry 0.457 2.87Benzyl alcohol 4 11/21/23 18:18 V40463AMP
<0.513 mg/Kg - dry 0.513 2.87Bis(2-Chloroethoxy)methane 4 11/21/23 18:18 V40463AMP
<0.465 mg/Kg - dry 0.465 2.87Bis(2-Chloroethyl)ether 4 11/21/23 18:18 V40463AMP
<0.592 mg/Kg - dry 0.592 1.44Bis(2-Chloroisopropyl)ether 4 11/21/23 18:18 V40463AMP
<0.522 mg/Kg - dry 0.522 2.87Bis(2-ethylhexyl)phthalate 4 11/21/23 18:18 V40463AMP
<0.474 mg/Kg - dry 0.474 2.874-Bromophenyl phenyl ether 4 11/21/23 18:18 V40463AMP
<0.491 mg/Kg - dry 0.491 1.44Butyl benzyl phthalate 4 11/21/23 18:18 V40463AMP
<0.402 mg/Kg - dry 0.402 2.874-Chloro-3-methylphenol 4 11/21/23 18:18 V40463AMP
<0.487 mg/Kg - dry 0.487 1.444-Chloroaniline 4 11/21/23 18:18 V40463AMP
<0.505 mg/Kg - dry 0.505 2.872-Chloronaphthalene 4 11/21/23 18:18 V40463AMP
<0.427 mg/Kg - dry 0.427 2.872-Chlorophenol 4 11/21/23 18:18 V40463AMP
<0.548 mg/Kg - dry 0.548 4.354-Chlorophenyl phenyl ether 4 11/21/23 18:18 V40463AMP
0.663 J mg/Kg - dry 0.618 2.87Chrysene 4 11/21/23 18:18 V40463AMP
<1.00 mg/Kg - dry 1.00 2.87Dibenz(a,h)anthracene 4 11/21/23 18:18 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 58 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-2
89744 Matrix:
11/17/2023 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.518 mg/Kg - dry 0.518 2.87Dibenzofuran 4 11/21/23 18:18 V40463AMP
<0.411 mg/Kg - dry 0.411 2.871,2-Dichlorobenzene 4 11/21/23 18:18 V40463AMP
<0.423 mg/Kg - dry 0.423 2.871,3-Dichlorobenzene 4 11/21/23 18:18 V40463AMP
<0.424 mg/Kg - dry 0.424 1.441,4-Dichlorobenzene 4 11/21/23 18:18 V40463AMP
<0.639 mg/Kg - dry 0.639 2.873,3'-Dichlorobenzidine 4 11/21/23 18:18 V40463AMP
<0.416 mg/Kg - dry 0.416 2.872,4-Dichlorophenol 4 11/21/23 18:18 V40463AMP
<0.783 mg/Kg - dry 0.783 2.87Diethyl phthalate 4 11/21/23 18:18 V40463AMP
<0.757 mg/Kg - dry 0.757 2.87Dimethyl phthalate 4 11/21/23 18:18 V40463AMP
<0.470 mg/Kg - dry 0.470 1.442,4-Dimethylphenol 4 11/21/23 18:18 V40463AMP
<0.465 mg/Kg - dry 0.465 2.87Di-n-butyl phthalate 4 11/21/23 18:18 V40463AMP
<1.04 mg/Kg - dry 1.04 6.534,6-Dinitro-2-methylphenol 4 11/21/23 18:18 V40463AMP
<2.26 mg/Kg - dry 2.26 6.532,4-Dinitrophenol 4 11/21/23 18:18 V40463AMP
<0.420 mg/Kg - dry 0.420 2.872,4-Dinitrotoluene 4 11/21/23 18:18 V40463AMP
<0.470 mg/Kg - dry 0.470 2.872,6-Dinitrotoluene 4 11/21/23 18:18 V40463AMP
<0.622 mg/Kg - dry 0.622 1.44Di-n-Octyl Phthalate 4 11/21/23 18:18 V40463AMP
1.40 J mg/Kg - dry 0.535 2.87Fluoranthene 4 11/21/23 18:18 V40463AMP
<0.557 mg/Kg - dry 0.557 2.87Fluorene 4 11/21/23 18:18 V40463AMP
<0.461 mg/Kg - dry 0.461 2.87Hexachlorobenzene 4 11/21/23 18:18 V40463AMP
<0.424 mg/Kg - dry 0.424 2.87Hexachlorobutadiene 4 11/21/23 18:18 V40463AMP
<0.683 mg/Kg - dry 0.683 2.87Hexachlorocyclopentadiene 4 11/21/23 18:18 V40463AMP
<0.345 mg/Kg - dry 0.345 2.87Hexachloroethane 4 11/21/23 18:18 V40463AMP
<0.779 mg/Kg - dry 0.779 2.87Indeno(1,2,3-cd)pyrene 4 11/21/23 18:18 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 59 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-2
89744 Matrix:
11/17/2023 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.831 mg/Kg - dry 0.831 2.87Isophorone 4 11/21/23 18:18 V40463AMP
<0.461 mg/Kg - dry 0.461 2.871-Methylnaphthalene 4 11/21/23 18:18 V40463AMP
<0.435 mg/Kg - dry 0.435 2.872-Methylnaphthalene 4 11/21/23 18:18 V40463AMP
<0.422 mg/Kg - dry 0.422 2.872-Methylphenol 4 11/21/23 18:18 V40463AMP
<0.370 mg/Kg - dry 0.370 2.873&4 Methylphenol 4 11/21/23 18:18 V40463AMP
<0.626 mg/Kg - dry 0.626 2.87Naphthalene 4 11/21/23 18:18 V40463AMP
<0.421 mg/Kg - dry 0.421 2.872-Nitroaniline 4 11/21/23 18:18 V40463AMP
<0.522 mg/Kg - dry 0.522 2.873-Nitroaniline 4 11/21/23 18:18 V40463AMP
<0.405 mg/Kg - dry 0.405 1.444-Nitroaniline 4 11/21/23 18:18 V40463AMP
<0.505 mg/Kg - dry 0.505 1.44Nitrobenzene 4 11/21/23 18:18 V40463AMP
<0.386 mg/Kg - dry 0.386 2.872-Nitrophenol 4 11/21/23 18:18 V40463AMP
<0.509 mg/Kg - dry 0.509 2.874-Nitrophenol 4 11/21/23 18:18 V40463AMP
<1.14 mg/Kg - dry 1.14 2.87N-Nitrosodimethylamine 4 11/21/23 18:18 V40463AMP
<0.787 mg/Kg - dry 0.787 2.87N-Nitrosodiphenylamine 4 11/21/23 18:18 V40463AMP
<0.513 mg/Kg - dry 0.513 2.87N-Nitroso-di-n-propylamine 4 11/21/23 18:18 V40463AMP
<1.51 mg/Kg - dry 1.51 4.35Pentachlorophenol 4 11/21/23 18:18 V40463AMP
<0.905 mg/Kg - dry 0.905 2.87Phenanthrene 4 11/21/23 18:18 V40463AMP
<0.487 mg/Kg - dry 0.487 2.87Phenol 4 11/21/23 18:18 V40463AMP
1.07 J mg/Kg - dry 0.583 2.87Pyrene 4 11/21/23 18:18 V40463AMP
<0.465 mg/Kg - dry 0.465 2.871,2,4-Trichlorobenzene 4 11/21/23 18:18 V40463AMP
<0.419 mg/Kg - dry 0.419 2.872,4,5-Trichlorophenol 4 11/21/23 18:18 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 60 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-2
89744 Matrix:
11/17/2023 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.420 mg/Kg - dry 0.420 2.872,4,6-Trichlorophenol 4 11/21/23 18:18 V40463AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 61 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:DUP-2
89745 Matrix:
11/17/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.62 %Moisture 1 11/21/23 12:30 SW-DRYWTCNC
<0.156 mg/Kg - dry 0.156 0.221Chromium, Hexavalent 1 12/05/23 11:00 SW-7199SWB
0.555 mg/Kg - dry 0.0946 0.277Arsenic 5 11/28/23 21:17 6020BCPW
43.7 mg/Kg - dry 0.047 0.276Barium 5 11/28/23 21:17 6020BCPW
0.0776 J mg/Kg - dry 0.0287 0.277Cadmium 5 11/28/23 21:17 6020BCPW
12.8 mg/Kg - dry 0.128 0.276Chromium 5 11/28/23 21:17 6020BCPW
5.08 mg/Kg - dry 0.0342 0.277Lead 5 11/28/23 21:17 6020BCPW
<0.0133 mg/Kg - dry 0.0133 0.0332Mercury (Total)1 11/29/23 14:53 7471BJKC
0.508 mg/Kg - dry 0.113 0.276Selenium 5 11/28/23 21:17 6020BCPW
0.0140 J mg/Kg - dry 0.0074 0.277Silver 5 11/28/23 21:17 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 62 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:DUP-2
89745 Matrix:
11/17/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/20/23 11:50
<0.0020 mg/Kg - dry 0.0020 0.0055Aldrin 1 11/27/23 23:13 V40591TJW
<0.0012 mg/Kg - dry 0.0012 0.0055alpha-BHC 1 11/27/23 23:13 V40591TJW
<0.0022 mg/Kg - dry 0.0022 0.0055beta-BHC 1 11/27/23 23:13 V40591TJW
<0.0013 mg/Kg - dry 0.0013 0.0055delta-BHC 1 11/27/23 23:13 V40591TJW
<0.0194 mg/Kg - dry 0.0194 0.0553Chlordane 1 11/27/23 23:13 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0055alpha-Chlordane 1 11/27/23 23:13 V40591TJW
<0.0018 mg/Kg - dry 0.0018 0.0055gamma-Chlordane 1 11/27/23 23:13 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.00554,4'-DDD 1 11/27/23 23:13 V40591TJW
<0.0022 mg/Kg - dry 0.0022 0.00554,4'-DDE 1 11/27/23 23:13 V40591TJW
<0.0016 mg/Kg - dry 0.0016 0.00554,4'-DDT 1 11/27/23 23:13 V40591TJW
<0.0023 mg/Kg - dry 0.0023 0.0055Dieldrin 1 11/27/23 23:13 V40591TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Endosulfan I 1 11/27/23 23:13 V40591TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Endosulfan II 1 11/27/23 23:13 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endosulfan Sulfate 1 11/27/23 23:13 V40591TJW
<0.0021 mg/Kg - dry 0.0021 0.0055Endrin 1 11/27/23 23:13 V40591TJW
<0.0023 mg/Kg - dry 0.0023 0.0055Endrin Aldehyde 1 11/27/23 23:13 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endrin Ketone 1 11/27/23 23:13 V40591TJW
<0.0013 mg/Kg - dry 0.0013 0.0055gamma-BHC 1 11/27/23 23:13 V40591TJW
<0.0015 mg/Kg - dry 0.0015 0.0055Heptachlor 1 11/27/23 23:13 V40591TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Heptachlor Epoxide 1 11/27/23 23:13 V40591TJW
<0.0029 mg/Kg - dry 0.0029 0.0055Methoxychlor 1 11/27/23 23:13 V40591TJW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 63 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:DUP-2
89745 Matrix:
11/17/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/20/23 11:50
<0.0112 mg/Kg - dry 0.0112 0.0553 1 11/27/23 23:13 V40591TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
0.203 mg/Kg - dry 0.002 0.022Acetone 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 11/21/23 12:06 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/21/23 12:06 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/21/23 12:06 V40484TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 11/21/23 12:06 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/21/23 12:06 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/21/23 12:06 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 11/21/23 12:06 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 64 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:DUP-2
89745 Matrix:
11/17/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 11/21/23 12:06 V40484TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/21/23 12:06 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/21/23 12:06 V40484TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/21/23 12:06 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/21/23 12:06 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/21/23 12:06 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/21/23 12:06 V40484TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 11/21/23 12:06 V40484TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/21/23 12:06 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/21/23 12:06 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/21/23 12:06 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/21/23 12:06 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/21/23 12:06 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/21/23 12:06 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 65 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:DUP-2
89745 Matrix:
11/17/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/21/23 12:06 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/21/23 12:06 V40484TBL
<0.015 mg/Kg - dry 0.015 0.276Ethanol 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 11/21/23 12:06 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 11/21/23 12:06 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/21/23 12:06 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 11/21/23 12:06 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 11/21/23 12:06 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/21/23 12:06 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 11/21/23 12:06 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/21/23 12:06 V40484TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/21/23 12:06 V40484TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/21/23 12:06 V40484TBL
<0.0010 mg/Kg - dry 0.0010 0.005 1 11/21/23 12:06 V40484TBL
0.0007 J mg/Kg - dry 0.0007 0.005 1 11/21/23 12:06 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 66 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:DUP-2
89745 Matrix:
11/17/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/21/23 12:06 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/21/23 12:06 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/21/23 12:06 V40484TBL
<0.002 mg/Kg - dry 0.002 0.011 1 11/21/23 12:06 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/21/23 12:06 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/21/23 12:06 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/21/23 12:06 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/21/23 12:06 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/21/23 12:06 V40484
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.513 mg/Kg - dry 0.513 2.92Acenaphthene 4 11/21/23 18:40 V40463AMP
<0.464 mg/Kg - dry 0.464 2.92Acenaphthylene 4 11/21/23 18:40 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 67 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:DUP-2
89745 Matrix:
11/17/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.672 mg/Kg - dry 0.672 2.92Aniline 4 11/21/23 18:40 V40463AMP
<0.632 mg/Kg - dry 0.632 2.92Anthracene 4 11/21/23 18:40 V40463AMP
0.718 J mg/Kg - dry 0.615 2.92Benzo(a)anthracene 4 11/21/23 18:40 V40463AMP
0.735 J mg/Kg - dry 0.650 2.92Benzo(a)pyrene 4 11/21/23 18:40 V40463AMP
1.08 J mg/Kg - dry 0.646 2.92Benzo(b)fluoranthene 4 11/21/23 18:40 V40463AMP
0.625 J mg/Kg - dry 0.601 2.92Benzo(g,h,i)perylene 4 11/21/23 18:40 V40463AMP
<0.606 mg/Kg - dry 0.606 2.92Benzo(k)fluoranthene 4 11/21/23 18:40 V40463AMP
<2.57 M mg/Kg - dry 2.57 8.86Benzoic Acid 4 11/21/23 18:40 V40463AMP
<0.464 mg/Kg - dry 0.464 2.92Benzyl alcohol 4 11/21/23 18:40 V40463AMP
<0.522 mg/Kg - dry 0.522 2.92Bis(2-Chloroethoxy)methane 4 11/21/23 18:40 V40463AMP
<0.473 mg/Kg - dry 0.473 2.92Bis(2-Chloroethyl)ether 4 11/21/23 18:40 V40463AMP
<0.601 mg/Kg - dry 0.601 1.46Bis(2-Chloroisopropyl)ether 4 11/21/23 18:40 V40463AMP
0.583 J mg/Kg - dry 0.531 2.92Bis(2-ethylhexyl)phthalate 4 11/21/23 18:40 V40463AMP
<0.482 mg/Kg - dry 0.482 2.924-Bromophenyl phenyl ether 4 11/21/23 18:40 V40463AMP
<0.500 mg/Kg - dry 0.500 1.46Butyl benzyl phthalate 4 11/21/23 18:40 V40463AMP
<0.409 mg/Kg - dry 0.409 2.924-Chloro-3-methylphenol 4 11/21/23 18:40 V40463AMP
<0.495 mg/Kg - dry 0.495 1.464-Chloroaniline 4 11/21/23 18:40 V40463AMP
<0.513 mg/Kg - dry 0.513 2.922-Chloronaphthalene 4 11/21/23 18:40 V40463AMP
<0.434 mg/Kg - dry 0.434 2.922-Chlorophenol 4 11/21/23 18:40 V40463AMP
<0.558 mg/Kg - dry 0.558 4.444-Chlorophenyl phenyl ether 4 11/21/23 18:40 V40463AMP
1.02 J mg/Kg - dry 0.628 2.92Chrysene 4 11/21/23 18:40 V40463AMP
<1.02 mg/Kg - dry 1.02 2.92Dibenz(a,h)anthracene 4 11/21/23 18:40 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 68 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:DUP-2
89745 Matrix:
11/17/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.526 mg/Kg - dry 0.526 2.92Dibenzofuran 4 11/21/23 18:40 V40463AMP
<0.418 mg/Kg - dry 0.418 2.921,2-Dichlorobenzene 4 11/21/23 18:40 V40463AMP
<0.430 mg/Kg - dry 0.430 2.921,3-Dichlorobenzene 4 11/21/23 18:40 V40463AMP
<0.431 mg/Kg - dry 0.431 1.461,4-Dichlorobenzene 4 11/21/23 18:40 V40463AMP
<0.650 mg/Kg - dry 0.650 2.923,3'-Dichlorobenzidine 4 11/21/23 18:40 V40463AMP
<0.423 mg/Kg - dry 0.423 2.922,4-Dichlorophenol 4 11/21/23 18:40 V40463AMP
<0.796 mg/Kg - dry 0.796 2.92Diethyl phthalate 4 11/21/23 18:40 V40463AMP
<0.770 mg/Kg - dry 0.770 2.92Dimethyl phthalate 4 11/21/23 18:40 V40463AMP
<0.477 mg/Kg - dry 0.477 1.462,4-Dimethylphenol 4 11/21/23 18:40 V40463AMP
<0.473 mg/Kg - dry 0.473 2.92Di-n-butyl phthalate 4 11/21/23 18:40 V40463AMP
<1.06 mg/Kg - dry 1.06 6.654,6-Dinitro-2-methylphenol 4 11/21/23 18:40 V40463AMP
<2.30 mg/Kg - dry 2.30 6.652,4-Dinitrophenol 4 11/21/23 18:40 V40463AMP
<0.427 mg/Kg - dry 0.427 2.922,4-Dinitrotoluene 4 11/21/23 18:40 V40463AMP
<0.477 mg/Kg - dry 0.477 2.922,6-Dinitrotoluene 4 11/21/23 18:40 V40463AMP
<0.632 mg/Kg - dry 0.632 1.46Di-n-Octyl Phthalate 4 11/21/23 18:40 V40463AMP
2.18 J mg/Kg - dry 0.544 2.92Fluoranthene 4 11/21/23 18:40 V40463AMP
<0.566 mg/Kg - dry 0.566 2.92Fluorene 4 11/21/23 18:40 V40463AMP
<0.469 mg/Kg - dry 0.469 2.92Hexachlorobenzene 4 11/21/23 18:40 V40463AMP
<0.431 mg/Kg - dry 0.431 2.92Hexachlorobutadiene 4 11/21/23 18:40 V40463AMP
<0.694 mg/Kg - dry 0.694 2.92Hexachlorocyclopentadiene 4 11/21/23 18:40 V40463AMP
<0.350 mg/Kg - dry 0.350 2.92Hexachloroethane 4 11/21/23 18:40 V40463AMP
<0.792 mg/Kg - dry 0.792 2.92Indeno(1,2,3-cd)pyrene 4 11/21/23 18:40 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 69 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:DUP-2
89745 Matrix:
11/17/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.845 mg/Kg - dry 0.845 2.92Isophorone 4 11/21/23 18:40 V40463AMP
<0.469 mg/Kg - dry 0.469 2.921-Methylnaphthalene 4 11/21/23 18:40 V40463AMP
<0.442 mg/Kg - dry 0.442 2.922-Methylnaphthalene 4 11/21/23 18:40 V40463AMP
<0.429 mg/Kg - dry 0.429 2.922-Methylphenol 4 11/21/23 18:40 V40463AMP
<0.376 mg/Kg - dry 0.376 2.923&4 Methylphenol 4 11/21/23 18:40 V40463AMP
<0.637 mg/Kg - dry 0.637 2.92Naphthalene 4 11/21/23 18:40 V40463AMP
<0.428 mg/Kg - dry 0.428 2.922-Nitroaniline 4 11/21/23 18:40 V40463AMP
<0.531 mg/Kg - dry 0.531 2.923-Nitroaniline 4 11/21/23 18:40 V40463AMP
<0.412 mg/Kg - dry 0.412 1.464-Nitroaniline 4 11/21/23 18:40 V40463AMP
<0.513 mg/Kg - dry 0.513 1.46Nitrobenzene 4 11/21/23 18:40 V40463AMP
<0.392 mg/Kg - dry 0.392 2.922-Nitrophenol 4 11/21/23 18:40 V40463AMP
<0.517 mg/Kg - dry 0.517 2.924-Nitrophenol 4 11/21/23 18:40 V40463AMP
<1.16 mg/Kg - dry 1.16 2.92N-Nitrosodimethylamine 4 11/21/23 18:40 V40463AMP
<0.801 mg/Kg - dry 0.801 2.92N-Nitrosodiphenylamine 4 11/21/23 18:40 V40463AMP
<0.522 mg/Kg - dry 0.522 2.92N-Nitroso-di-n-propylamine 4 11/21/23 18:40 V40463AMP
<1.54 mg/Kg - dry 1.54 4.44Pentachlorophenol 4 11/21/23 18:40 V40463AMP
<0.920 mg/Kg - dry 0.920 2.92Phenanthrene 4 11/21/23 18:40 V40463AMP
<0.495 mg/Kg - dry 0.495 2.92Phenol 4 11/21/23 18:40 V40463AMP
1.70 J mg/Kg - dry 0.593 2.92Pyrene 4 11/21/23 18:40 V40463AMP
<0.473 mg/Kg - dry 0.473 2.921,2,4-Trichlorobenzene 4 11/21/23 18:40 V40463AMP
<0.425 mg/Kg - dry 0.425 2.922,4,5-Trichlorophenol 4 11/21/23 18:40 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 70 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:DUP-2
89745 Matrix:
11/17/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.427 mg/Kg - dry 0.427 2.922,4,6-Trichlorophenol 4 11/21/23 18:40 V40463AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 71 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-3
89746 Matrix:
11/17/2023 10:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
10.7 %Moisture 1 11/21/23 12:30 SW-DRYWTCNC
0.244 B mg/Kg - dry 0.157 0.223Chromium, Hexavalent 1 12/05/23 09:54 SW-7199SWB
0.691 mg/Kg - dry 0.0957 0.280Arsenic 5 11/28/23 21:21 6020BCPW
36.1 mg/Kg - dry 0.047 0.279Barium 5 11/28/23 21:21 6020BCPW
0.0657 J mg/Kg - dry 0.0291 0.280Cadmium 5 11/28/23 21:21 6020BCPW
18.3 mg/Kg - dry 0.129 0.279Chromium 5 11/28/23 21:21 6020BCPW
6.39 mg/Kg - dry 0.0347 0.280Lead 5 11/28/23 21:21 6020BCPW
0.0134 J mg/Kg - dry 0.0134 0.0336Mercury (Total)1 11/29/23 15:02 7471BJKC
0.547 mg/Kg - dry 0.115 0.279Selenium 5 11/28/23 21:21 6020BCPW
0.0320 J mg/Kg - dry 0.0075 0.280Silver 5 11/28/23 21:21 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 72 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-3
89746 Matrix:
11/17/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/20/23 11:50
<0.0020 mg/Kg - dry 0.0020 0.0055Aldrin 1 11/27/23 23:27 V40591TJW
<0.0013 mg/Kg - dry 0.0013 0.0055alpha-BHC 1 11/27/23 23:27 V40591TJW
<0.0022 mg/Kg - dry 0.0022 0.0055beta-BHC 1 11/27/23 23:27 V40591TJW
<0.0013 mg/Kg - dry 0.0013 0.0055delta-BHC 1 11/27/23 23:27 V40591TJW
<0.0197 mg/Kg - dry 0.0197 0.0559Chlordane 1 11/27/23 23:27 V40591TJW
<0.0021 mg/Kg - dry 0.0021 0.0055alpha-Chlordane 1 11/27/23 23:27 V40591TJW
<0.0018 mg/Kg - dry 0.0018 0.0055gamma-Chlordane 1 11/27/23 23:27 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.00554,4'-DDD 1 11/27/23 23:27 V40591TJW
<0.0022 mg/Kg - dry 0.0022 0.00554,4'-DDE 1 11/27/23 23:27 V40591TJW
<0.0017 mg/Kg - dry 0.0017 0.00554,4'-DDT 1 11/27/23 23:27 V40591TJW
0.0031 J mg/Kg - dry 0.0023 0.0055Dieldrin 1 11/27/23 23:27 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endosulfan I 1 11/27/23 23:27 V40591TJW
<0.0019 mg/Kg - dry 0.0019 0.0055Endosulfan II 1 11/27/23 23:27 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endosulfan Sulfate 1 11/27/23 23:27 V40591TJW
<0.0021 mg/Kg - dry 0.0021 0.0055Endrin 1 11/27/23 23:27 V40591TJW
<0.0023 mg/Kg - dry 0.0023 0.0055Endrin Aldehyde 1 11/27/23 23:27 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Endrin Ketone 1 11/27/23 23:27 V40591TJW
<0.0014 mg/Kg - dry 0.0014 0.0055gamma-BHC 1 11/27/23 23:27 V40591TJW
<0.0015 mg/Kg - dry 0.0015 0.0055Heptachlor 1 11/27/23 23:27 V40591TJW
<0.0020 mg/Kg - dry 0.0020 0.0055Heptachlor Epoxide 1 11/27/23 23:27 V40591TJW
<0.0029 mg/Kg - dry 0.0029 0.0055Methoxychlor 1 11/27/23 23:27 V40591TJW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 73 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-3
89746 Matrix:
11/17/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):11/20/23 11:50
0.134 mg/Kg - dry 0.0114 0.0559 1 11/27/23 23:27 V40591TJW
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
0.048 mg/Kg - dry 0.002 0.022Acetone 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 11/21/23 12:33 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/21/23 12:33 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/21/23 12:33 V40484TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 11/21/23 12:33 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/21/23 12:33 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/21/23 12:33 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/21/23 12:33 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 74 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-3
89746 Matrix:
11/17/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 11/21/23 12:33 V40484TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/21/23 12:33 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/21/23 12:33 V40484TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/21/23 12:33 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/21/23 12:33 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/21/23 12:33 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/21/23 12:33 V40484TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 11/21/23 12:33 V40484TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/21/23 12:33 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/21/23 12:33 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 11/21/23 12:33 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/21/23 12:33 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/21/23 12:33 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/21/23 12:33 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 75 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-3
89746 Matrix:
11/17/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/21/23 12:33 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/21/23 12:33 V40484TBL
<0.015 mg/Kg - dry 0.015 0.279Ethanol 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 11/21/23 12:33 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 11/21/23 12:33 V40484TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/21/23 12:33 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 11/21/23 12:33 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 11/21/23 12:33 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/21/23 12:33 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 11/21/23 12:33 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/21/23 12:33 V40484TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 11/21/23 12:33 V40484TBL
0.004 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/21/23 12:33 V40484TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/21/23 12:33 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.005 1 11/21/23 12:33 V40484TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 76 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-3
89746 Matrix:
11/17/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):11/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/21/23 12:33 V40484TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/21/23 12:33 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.005 1 11/21/23 12:33 V40484TBL
<0.002 mg/Kg - dry 0.002 0.011 1 11/21/23 12:33 V40484TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/21/23 12:33 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/21/23 12:33 V40484TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/21/23 12:33 V40484TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/21/23 12:33 V40484TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/21/23 12:33 V40484
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluoromethane
Surrogate: Toluene-d8
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.519 mg/Kg - dry 0.519 2.96Acenaphthene 4 11/21/23 19:03 V40463AMP
<0.470 mg/Kg - dry 0.470 2.96Acenaphthylene 4 11/21/23 19:03 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 77 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-3
89746 Matrix:
11/17/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.680 mg/Kg - dry 0.680 2.96Aniline 4 11/21/23 19:03 V40463AMP
<0.640 mg/Kg - dry 0.640 2.96Anthracene 4 11/21/23 19:03 V40463AMP
<0.622 mg/Kg - dry 0.622 2.96Benzo(a)anthracene 4 11/21/23 19:03 V40463AMP
<0.658 mg/Kg - dry 0.658 2.96Benzo(a)pyrene 4 11/21/23 19:03 V40463AMP
<0.653 mg/Kg - dry 0.653 2.96Benzo(b)fluoranthene 4 11/21/23 19:03 V40463AMP
<0.609 mg/Kg - dry 0.609 2.96Benzo(g,h,i)perylene 4 11/21/23 19:03 V40463AMP
<0.613 mg/Kg - dry 0.613 2.96Benzo(k)fluoranthene 4 11/21/23 19:03 V40463AMP
<2.60 M mg/Kg - dry 2.60 8.96Benzoic Acid 4 11/21/23 19:03 V40463AMP
<0.470 mg/Kg - dry 0.470 2.96Benzyl alcohol 4 11/21/23 19:03 V40463AMP
<0.528 mg/Kg - dry 0.528 2.96Bis(2-Chloroethoxy)methane 4 11/21/23 19:03 V40463AMP
<0.479 mg/Kg - dry 0.479 2.96Bis(2-Chloroethyl)ether 4 11/21/23 19:03 V40463AMP
<0.609 mg/Kg - dry 0.609 1.48Bis(2-Chloroisopropyl)ether 4 11/21/23 19:03 V40463AMP
<0.537 mg/Kg - dry 0.537 2.96Bis(2-ethylhexyl)phthalate 4 11/21/23 19:03 V40463AMP
<0.488 mg/Kg - dry 0.488 2.964-Bromophenyl phenyl ether 4 11/21/23 19:03 V40463AMP
<0.506 mg/Kg - dry 0.506 1.48Butyl benzyl phthalate 4 11/21/23 19:03 V40463AMP
<0.414 mg/Kg - dry 0.414 2.964-Chloro-3-methylphenol 4 11/21/23 19:03 V40463AMP
<0.501 mg/Kg - dry 0.501 1.484-Chloroaniline 4 11/21/23 19:03 V40463AMP
<0.519 mg/Kg - dry 0.519 2.962-Chloronaphthalene 4 11/21/23 19:03 V40463AMP
<0.440 mg/Kg - dry 0.440 2.962-Chlorophenol 4 11/21/23 19:03 V40463AMP
<0.564 mg/Kg - dry 0.564 4.484-Chlorophenyl phenyl ether 4 11/21/23 19:03 V40463AMP
<0.636 mg/Kg - dry 0.636 2.96Chrysene 4 11/21/23 19:03 V40463AMP
<1.03 mg/Kg - dry 1.03 2.96Dibenz(a,h)anthracene 4 11/21/23 19:03 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 78 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-3
89746 Matrix:
11/17/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.533 mg/Kg - dry 0.533 2.96Dibenzofuran 4 11/21/23 19:03 V40463AMP
<0.423 mg/Kg - dry 0.423 2.961,2-Dichlorobenzene 4 11/21/23 19:03 V40463AMP
<0.435 mg/Kg - dry 0.435 2.961,3-Dichlorobenzene 4 11/21/23 19:03 V40463AMP
<0.436 mg/Kg - dry 0.436 1.481,4-Dichlorobenzene 4 11/21/23 19:03 V40463AMP
<0.658 mg/Kg - dry 0.658 2.963,3'-Dichlorobenzidine 4 11/21/23 19:03 V40463AMP
<0.428 mg/Kg - dry 0.428 2.962,4-Dichlorophenol 4 11/21/23 19:03 V40463AMP
<0.806 mg/Kg - dry 0.806 2.96Diethyl phthalate 4 11/21/23 19:03 V40463AMP
<0.779 mg/Kg - dry 0.779 2.96Dimethyl phthalate 4 11/21/23 19:03 V40463AMP
<0.483 mg/Kg - dry 0.483 1.482,4-Dimethylphenol 4 11/21/23 19:03 V40463AMP
<0.479 mg/Kg - dry 0.479 2.96Di-n-butyl phthalate 4 11/21/23 19:03 V40463AMP
<1.08 mg/Kg - dry 1.08 6.724,6-Dinitro-2-methylphenol 4 11/21/23 19:03 V40463AMP
<2.33 mg/Kg - dry 2.33 6.722,4-Dinitrophenol 4 11/21/23 19:03 V40463AMP
<0.432 mg/Kg - dry 0.432 2.962,4-Dinitrotoluene 4 11/21/23 19:03 V40463AMP
<0.483 mg/Kg - dry 0.483 2.962,6-Dinitrotoluene 4 11/21/23 19:03 V40463AMP
<0.640 mg/Kg - dry 0.640 1.48Di-n-Octyl Phthalate 4 11/21/23 19:03 V40463AMP
1.16 J mg/Kg - dry 0.550 2.96Fluoranthene 4 11/21/23 19:03 V40463AMP
<0.573 mg/Kg - dry 0.573 2.96Fluorene 4 11/21/23 19:03 V40463AMP
<0.474 mg/Kg - dry 0.474 2.96Hexachlorobenzene 4 11/21/23 19:03 V40463AMP
<0.436 mg/Kg - dry 0.436 2.96Hexachlorobutadiene 4 11/21/23 19:03 V40463AMP
<0.703 mg/Kg - dry 0.703 2.96Hexachlorocyclopentadiene 4 11/21/23 19:03 V40463AMP
<0.354 mg/Kg - dry 0.354 2.96Hexachloroethane 4 11/21/23 19:03 V40463AMP
<0.801 mg/Kg - dry 0.801 2.96Indeno(1,2,3-cd)pyrene 4 11/21/23 19:03 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 79 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-3
89746 Matrix:
11/17/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.855 mg/Kg - dry 0.855 2.96Isophorone 4 11/21/23 19:03 V40463AMP
<0.474 mg/Kg - dry 0.474 2.961-Methylnaphthalene 4 11/21/23 19:03 V40463AMP
<0.447 mg/Kg - dry 0.447 2.962-Methylnaphthalene 4 11/21/23 19:03 V40463AMP
<0.434 mg/Kg - dry 0.434 2.962-Methylphenol 4 11/21/23 19:03 V40463AMP
<0.380 mg/Kg - dry 0.380 2.963&4 Methylphenol 4 11/21/23 19:03 V40463AMP
<0.645 mg/Kg - dry 0.645 2.96Naphthalene 4 11/21/23 19:03 V40463AMP
<0.433 mg/Kg - dry 0.433 2.962-Nitroaniline 4 11/21/23 19:03 V40463AMP
<0.537 mg/Kg - dry 0.537 2.963-Nitroaniline 4 11/21/23 19:03 V40463AMP
<0.417 mg/Kg - dry 0.417 1.484-Nitroaniline 4 11/21/23 19:03 V40463AMP
<0.519 mg/Kg - dry 0.519 1.48Nitrobenzene 4 11/21/23 19:03 V40463AMP
<0.397 mg/Kg - dry 0.397 2.962-Nitrophenol 4 11/21/23 19:03 V40463AMP
<0.524 mg/Kg - dry 0.524 2.964-Nitrophenol 4 11/21/23 19:03 V40463AMP
<1.18 mg/Kg - dry 1.18 2.96N-Nitrosodimethylamine 4 11/21/23 19:03 V40463AMP
<0.810 mg/Kg - dry 0.810 2.96N-Nitrosodiphenylamine 4 11/21/23 19:03 V40463AMP
<0.528 mg/Kg - dry 0.528 2.96N-Nitroso-di-n-propylamine 4 11/21/23 19:03 V40463AMP
<1.56 mg/Kg - dry 1.56 4.48Pentachlorophenol 4 11/21/23 19:03 V40463AMP
<0.931 mg/Kg - dry 0.931 2.96Phenanthrene 4 11/21/23 19:03 V40463AMP
<0.501 mg/Kg - dry 0.501 2.96Phenol 4 11/21/23 19:03 V40463AMP
0.885 J mg/Kg - dry 0.600 2.96Pyrene 4 11/21/23 19:03 V40463AMP
<0.479 mg/Kg - dry 0.479 2.961,2,4-Trichlorobenzene 4 11/21/23 19:03 V40463AMP
<0.431 mg/Kg - dry 0.431 2.962,4,5-Trichlorophenol 4 11/21/23 19:03 V40463AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 80 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-321-0112
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/17/2023
Former Winston Container
Report Date : 12/05/2023
Sample ID :
Lab No :
Sampled:SED-3
89746 Matrix:
11/17/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):11/21/23 10:10
<0.432 mg/Kg - dry 0.432 2.962,4,6-Trichlorophenol 4 11/21/23 19:03 V40463AMP
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 81 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Metals Analyses
6020B
L719432QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:L718903
Associated Lab Samples: 89739, 89740, 89741, 89742
LRB-L718903 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/29/23 03:591.000.297<0.297µg/LArsenic
11/29/23 03:591.000.453<0.453µg/LBarium
11/29/23 03:591.000.350<0.350µg/LCadmium
11/29/23 03:591.000.346<0.346µg/LChromium
11/29/23 03:591.000.264<0.264µg/LLead
11/29/23 03:591.000.703<0.703µg/LSelenium
11/29/23 03:591.000.0570<0.0570µg/LSilver
LCS-L718903Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
93.046.450.0µg/LArsenic 80-120
89.089.4100µg/LBarium 80-120
93.09.3410.0µg/LCadmium 80-120
91.090.5100µg/LChromium 80-120
95.047.450.0µg/LLead 80-120
94.094.4100µg/LSelenium 80-120
92.09.1710.0µg/LSilver 80-120
V 89928-MS-L718903 V 89928-MSD-L718903Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
49.4 95.047.450.050.01.85µg/LArsenic 91.0 75-125 4.1 20.0
154 91.015510010063.2µg/LBarium 92.0 75-125 0.6 20.0
8.74 87.09.0710.010.0< 0.350µg/LCadmium 91.0 75-125 3.7 20.0
90.0 90.088.01001000.419µg/LChromium 88.0 75-125 2.2 20.0
Page 1 of 34Date:12/05/2023 04:12 PM
Page 82 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Metals Analyses
6020B
L719432QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:L718903
V 89928-MS-L718903 V 89928-MSD-L718903Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
47.0 94.046.750.050.0< 0.264µg/LLead 93.0 75-125 0.6 20.0
102 10296.4100100< 0.703µg/LSelenium 96.0 75-125 5.6 20.0
8.58 86.08.5310.010.0< 0.0570µg/LSilver 85.0 75-125 0.5 20.0
V 89928-PDS-L718903Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
11/29/23 06:2095.024.7µg/LArsenic
11/29/23 06:2094.077.1µg/LBarium
11/29/23 06:2087.04.35µg/LCadmium
11/29/23 06:2087.043.9µg/LChromium
11/29/23 06:2092.022.9µg/LLead
11/29/23 06:2010050.2µg/LSelenium
11/29/23 06:2087.04.37µg/LSilver
Page 2 of 34Date:12/05/2023 04:12 PM
Page 83 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Metals Analyses
6020B
L719430,L719663QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L718975
Associated Lab Samples: 89743, 89744, 89745, 89746
LRB-L718975 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/28/23 20:260.2500.0855<0.0855mg/KgArsenic
11/28/23 20:260.2500.042<0.042mg/KgBarium
11/28/23 20:260.2500.0260<0.0260mg/KgCadmium
11/28/23 20:260.2500.116<0.116mg/KgChromium
11/28/23 20:260.2500.0310<0.0310mg/KgLead
11/28/23 20:260.2500.103<0.103mg/KgSelenium
11/28/23 20:260.2500.0067<0.0067mg/KgSilver
LCS-L718975Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
89.02.222.50mg/KgArsenic 80-120
92.04.585.00mg/KgBarium 80-120
90.00.4510.500mg/KgCadmium 80-120
91.04.545.00mg/KgChromium 80-120
89.02.222.50mg/KgLead 80-120
95.04.765.00mg/KgSelenium 80-120
88.00.4410.500mg/KgSilver 80-120
V 89998-MS-L718975 V 89998-MSD-L718975Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
3.35 57.0*3.352.432.461.95mg/KgArsenic 58.0*75-125 0.0 80
38.0 0.0*44.34.854.9241.3mg/KgBarium 62.0*75-125 15.3 80
0.544 92.00.4740.4850.4920.0890mg/KgCadmium 79.0 75-125 13.7 80
20.6 0.0*22.74.854.9222.2mg/KgChromium 10.0*75-125 9.6 80
Page 3 of 34* QC Fail Date:12/05/2023 04:12 PM
Page 84 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Metals Analyses
6020B
L719430,L719663QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L718975
V 89998-MS-L718975 V 89998-MSD-L718975Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
16.8 0.0*19.32.432.4621.3mg/KgLead 0.0*75-125 13.8 80
4.64 75.04.774.854.920.927mg/KgSelenium 79.0 75-125 2.7 80
0.471 92.00.4670.4850.4920.0200mg/KgSilver 92.0 75-125 0.8 80
V 89998-PDS-L718975Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
11/28/23 22:2688.01.26mg/KgArsenic
11/28/23 22:2678.05.16mg/KgBarium
11/28/23 22:2690.00.229mg/KgCadmium
11/28/23 22:2682.03.82mg/KgChromium
11/28/23 22:2679.02.66mg/KgLead
11/28/23 22:2693.02.37mg/KgSelenium
11/28/23 22:2695.00.235mg/KgSilver
Page 4 of 34* QC Fail Date:12/05/2023 04:12 PM
Page 85 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Total Aqueous Mercury Analysis - CVAA
7470A
L719601QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7470A
QC Prep:L719407
Associated Lab Samples: 89739, 89740, 89741, 89742
LRB-L719407 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/29/23 14:070.000200.00010<0.00010mg/LMercury (Total)
LCS-L719407Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
91.00.003650.00400mg/LMercury (Total)80-120
L 94942-MS-L719407 L 94942-MSD-L719407Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.00275 69.0*0.002690.004000.00400< 0.00010mg/LMercury (Total)67.0*80-120 2.2 20.0
L 94942-PDS-L719407Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
11/29/23 14:3194.00.00468mg/LMercury (Total)
Page 5 of 34* QC Fail Date:12/05/2023 04:12 PM
Page 86 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V40695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V40652
Associated Lab Samples: 89743, 89744, 89745, 89746
LRB-V40652 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/29/23 14:300.03000.0120<0.0120mg/KgMercury (Total)
LCS-V40652Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1020.4240.417mg/KgMercury (Total)80-120
V 89998-MS-V40652 V 89998-MSD-V40652Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.432 81.00.4560.4170.4170.0944mg/KgMercury (Total)87.0 80-120 5.4 20
V 89998-PDS-V40652Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
11/29/23 15:3898.00.249mg/KgMercury (Total)
Page 6 of 34Date:12/05/2023 04:12 PM
Page 87 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Organochlorine Pesticides by GC
8081B
V40591QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40383
Associated Lab Samples: 89743, 89744, 89745, 89746
LRB-V40383 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/27/23 20:450.00500.0018<0.0018mg/KgAldrin
11/27/23 20:450.00500.0011<0.0011mg/Kgalpha-BHC
11/27/23 20:450.00500.0019<0.0019mg/Kgbeta-BHC
11/27/23 20:450.00500.0012<0.0012mg/Kgdelta-BHC
11/27/23 20:450.05000.0176<0.0176mg/KgChlordane
11/27/23 20:450.00500.0018<0.0018mg/Kgalpha-Chlordane
11/27/23 20:450.00500.0016<0.0016mg/Kggamma-Chlordane
11/27/23 20:450.00500.0018<0.0018mg/Kg4,4'-DDD
11/27/23 20:450.00500.0020<0.0020mg/Kg4,4'-DDE
11/27/23 20:450.00500.0015<0.0015mg/Kg4,4'-DDT
11/27/23 20:450.00500.0020<0.0020mg/KgDieldrin
11/27/23 20:450.00500.0017<0.0017mg/KgEndosulfan I
11/27/23 20:450.00500.0017<0.0017mg/KgEndosulfan II
11/27/23 20:450.00500.0018<0.0018mg/KgEndosulfan Sulfate
11/27/23 20:450.00500.0019<0.0019mg/KgEndrin
11/27/23 20:450.00500.0021<0.0021mg/KgEndrin Aldehyde
11/27/23 20:450.00500.0018<0.0018mg/KgEndrin Ketone
11/27/23 20:450.00500.0012<0.0012mg/Kggamma-BHC
11/27/23 20:450.00500.0013<0.0013mg/KgHeptachlor
11/27/23 20:450.00500.0017<0.0017mg/KgHeptachlor Epoxide
11/27/23 20:450.00500.0026<0.0026mg/KgMethoxychlor
11/27/23 20:450.05000.0102<0.0102mg/Kg
11/27/23 20:45Decachlorobiphenyl (S)119 26-204
11/27/23 20:45 105 40-162
Page 7 of 34Date:12/05/2023 04:12 PM
Page 88 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Organochlorine Pesticides by GC
8081B
V40591QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40383
LCS-V40383Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1000.3340.333mg/KgChlordane 43-149
1020.3400.333mg/Kg 33-141
LCS-V40383 LCSD-V40383Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits
106123Decachlorobiphenyl (S)26-204
99.3109 40-162
Page 8 of 34Date:12/05/2023 04:12 PM
Page 89 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40484QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40483
Associated Lab Samples: 89743, 89744, 89745, 89746
LRB-V40483 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/21/23 10:440.0200.002<0.002mg/KgAcetone
11/21/23 10:440.0200.001<0.001mg/KgAcrolein
11/21/23 10:440.0200.0008<0.0008mg/KgAcrylonitrile
11/21/23 10:440.0050.0006<0.0006mg/KgBenzene
11/21/23 10:440.0050.0005<0.0005mg/KgBromobenzene
11/21/23 10:440.0050.0008<0.0008mg/KgBromochloromethane
11/21/23 10:440.0050.001<0.001mg/KgBromodichloromethane
11/21/23 10:440.0050.001<0.001mg/KgBromoform
11/21/23 10:440.0100.001<0.001mg/KgBromomethane
11/21/23 10:440.0050.0005<0.0005mg/Kgn-Butylbenzene
11/21/23 10:440.0050.0006<0.0006mg/Kgsec-Butyl benzene
11/21/23 10:440.0050.0005<0.0005mg/Kgtert-Butyl benzene
11/21/23 10:440.0050.0006<0.0006mg/KgCarbon Disulfide
11/21/23 10:440.0050.001<0.001mg/KgCarbon Tetrachloride
11/21/23 10:440.0050.0007<0.0007mg/KgChlorobenzene
11/21/23 10:440.0050.0009<0.0009mg/KgChlorodibromomethane
11/21/23 10:440.0100.0009<0.0009mg/KgChloroethane
11/21/23 10:440.0050.001<0.001mg/KgChloroform
11/21/23 10:440.0100.0006<0.0006mg/KgChloromethane
11/21/23 10:440.0050.0005<0.0005mg/Kg2-Chlorotoluene
11/21/23 10:440.0050.0004<0.0004mg/Kg4-Chlorotoluene
11/21/23 10:440.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
11/21/23 10:440.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
11/21/23 10:440.0050.0006<0.0006mg/Kg1,2-Dibromoethane
11/21/23 10:440.0050.0006<0.0006mg/KgDibromomethane
11/21/23 10:440.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
11/21/23 10:440.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 9 of 34Date:12/05/2023 04:12 PM
Page 90 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40484QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40483
Associated Lab Samples: 89743, 89744, 89745, 89746
LRB-V40483 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/21/23 10:440.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
11/21/23 10:440.0100.001<0.001mg/KgDichlorodifluoromethane
11/21/23 10:440.0050.0008<0.0008mg/Kg1,1-Dichloroethane
11/21/23 10:440.0050.001<0.001mg/Kg1,2-Dichloroethane
11/21/23 10:440.0050.0007<0.0007mg/Kg1,1-Dichloroethene
11/21/23 10:440.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
11/21/23 10:440.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
11/21/23 10:440.0050.0004<0.0004mg/Kg1,2-Dichloropropane
11/21/23 10:440.0050.0006<0.0006mg/Kg1,3-Dichloropropane
11/21/23 10:440.0050.001<0.001mg/Kg2,2-Dichloropropane
11/21/23 10:440.0050.0008<0.0008mg/Kg1,1-Dichloropropene
11/21/23 10:440.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
11/21/23 10:440.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
11/21/23 10:440.2500.014<0.014mg/KgEthanol
11/21/23 10:440.0050.0006<0.0006mg/KgEthylbenzene
11/21/23 10:440.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
11/21/23 10:440.0100.0008<0.0008mg/KgHexachlorobutadiene
11/21/23 10:440.0100.0007<0.0007mg/Kgn-Hexane
11/21/23 10:440.0200.0006<0.0006mg/Kg2-Hexanone
11/21/23 10:440.0050.0005<0.0005mg/KgIsopropylbenzene
11/21/23 10:440.0050.001<0.001mg/Kg4-Isopropyl toluene
11/21/23 10:440.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
11/21/23 10:440.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
11/21/23 10:440.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
11/21/23 10:440.0100.001<0.001mg/KgMethylene Chloride
11/21/23 10:440.0100.0010<0.0010mg/KgNaphthalene
11/21/23 10:440.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 10 of 34Date:12/05/2023 04:12 PM
Page 91 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40484QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40483
Associated Lab Samples: 89743, 89744, 89745, 89746
LRB-V40483 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/21/23 10:440.0050.001<0.001mg/KgStyrene
11/21/23 10:440.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
11/21/23 10:440.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
11/21/23 10:440.0050.0009<0.0009mg/Kg
11/21/23 10:440.0050.0007<0.0007mg/Kg
11/21/23 10:440.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
11/21/23 10:440.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
11/21/23 10:440.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/21/23 10:440.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
11/21/23 10:440.0050.0009<0.0009mg/Kg
11/21/23 10:440.0100.002<0.002mg/Kg
11/21/23 10:440.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
11/21/23 10:440.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
11/21/23 10:440.0100.0005<0.0005mg/KgVinyl Acetate
11/21/23 10:440.0100.0005<0.0005mg/KgVinyl Chloride
11/21/23 10:440.0050.0005<0.0005mg/Kgo-Xylene
11/21/23 10:440.0100.001<0.001mg/Kgm,p-Xylene
11/21/23 10:444-Bromofluorobenzene (S)101 70-130
11/21/23 10:44Dibromofluoromethane (S)110 84-123
11/21/23 10:44 101 76-129
LCS-V40483 LCSD-V40483Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.093 93.381.00.0810.100mg/KgAcetone 29-198 14.1 20
0.087 87.593.00.0930.100mg/KgAcrolein 70-130 6.0 20
Page 11 of 34Date:12/05/2023 04:12 PM
Page 92 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40484QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40483
LCS-V40483 LCSD-V40483Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.087 87.088.30.0880.100mg/KgAcrylonitrile 65-134 1.4 20
0.045 91.095.20.0470.050mg/KgBenzene 74-127 4.5 20
0.045 91.893.60.0460.050mg/KgBromobenzene 73-125 1.9 20
0.049 98.81010.0500.050mg/KgBromochloromethane 72-134 1.8 20
0.052 1051080.0530.050mg/KgBromodichloromethane 75-122 2.6 20
0.048 96.697.20.0480.050mg/KgBromoform 66-135 0.6 20
0.042 84.21010.0500.050mg/KgBromomethane 20-180 17.9 20
0.045 91.699.60.0490.050mg/Kgn-Butylbenzene 65-135 8.3 20
0.044 88.093.20.0460.050mg/Kgsec-Butyl benzene 66-131 5.7 20
0.045 91.094.80.0470.050mg/Kgtert-Butyl benzene 67-132 4.0 20
0.041 82.689.60.0440.050mg/KgCarbon Disulfide 61-129 8.1 20
0.050 1011110.0550.050mg/KgCarbon Tetrachloride 64-143 9.2 20
0.046 93.695.00.0470.050mg/KgChlorobenzene 74-118 1.4 20
0.050 1001010.0500.050mg/KgChlorodibromomethane 73-122 0.5 20
0.042 85.092.00.0460.050mg/KgChloroethane 33-149 7.9 20
0.049 99.01040.0510.050mg/KgChloroform 73-127 4.7 20
0.042 84.695.80.0470.050mg/KgChloromethane 45-143 12.4 20
0.045 91.494.60.0470.050mg/Kg2-Chlorotoluene 67-124 3.4 20
0.045 91.494.60.0470.050mg/Kg4-Chlorotoluene 71-126 3.4 20
0.043 86.888.80.0440.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.2 20
0.046 93.090.20.0450.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.0 20
0.046 93.897.00.0480.050mg/Kg1,2-Dibromoethane 70-132 3.3 20
0.050 1001000.0500.050mg/KgDibromomethane 74-133 0.3 20
0.046 93.897.00.0480.050mg/Kg1,2-Dichlorobenzene 72-123 3.3 20
0.046 93.095.40.0470.050mg/Kg1,3-Dichlorobenzene 71-120 2.5 20
0.043 87.891.00.0450.050mg/Kg1,4-Dichlorobenzene 71-123 3.5 20
Page 12 of 34Date:12/05/2023 04:12 PM
Page 93 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40484QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40483
LCS-V40483 LCSD-V40483Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 90.81030.0510.050mg/KgDichlorodifluoromethane 26-146 12.3 20
0.045 91.697.00.0480.050mg/Kg1,1-Dichloroethane 74-127 5.7 20
0.052 1041080.0530.050mg/Kg1,2-Dichloroethane 68-128 3.5 20
0.046 92.899.40.0490.050mg/Kg1,1-Dichloroethene 67-149 6.8 20
0.047 95.21000.0500.050mg/Kgcis-1,2-Dichloroethene 76-134 5.3 20
0.046 92.21020.0510.050mg/Kgtrans-1,2-Dichloroethene 73-132 10.4 20
0.043 87.292.60.0460.050mg/Kg1,2-Dichloropropane 73-130 6.0 20
0.046 93.695.00.0470.050mg/Kg1,3-Dichloropropane 75-124 1.4 20
0.050 1001090.0540.050mg/Kg2,2-Dichloropropane 50-142 8.6 20
0.046 92.098.80.0490.050mg/Kg1,1-Dichloropropene 71-130 7.1 20
0.050 1011020.0500.050mg/Kgcis-1,3-Dichloropropene 71-125 0.1 20
0.052 1051070.0530.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.0 20
1.08 86.483.21.041.25mg/KgEthanol 70-130 3.7 20
0.045 90.095.40.0470.050mg/KgEthylbenzene 74-128 5.8 20
0.093 93.395.10.0950.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.9 20
0.048 96.81050.0520.050mg/KgHexachlorobutadiene 64-125 7.9 20
0.044 88.494.40.0470.050mg/Kgn-Hexane 70-130 6.5 20
0.043 87.084.80.0420.050mg/Kg2-Hexanone 61-157 2.5 20
0.044 88.693.60.0460.050mg/KgIsopropylbenzene 68-126 5.4 20
0.046 93.297.00.0480.050mg/Kg4-Isopropyl toluene 68-129 3.9 20
0.047 94.292.60.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.7 20
0.046 92.496.40.0480.050mg/KgMethyl tert-butyl ether (MTBE)70-130 4.2 20
0.044 89.289.00.0440.050mg/Kg4-Methyl-2-Pentanone 57-162 0.2 20
0.044 88.492.80.0460.050mg/KgMethylene Chloride 74-129 4.8 20
0.045 91.290.60.0450.050mg/KgNaphthalene 57-157 0.6 20
0.044 88.893.60.0460.050mg/Kgn-Propylbenzene 67-130 5.2 20
Page 13 of 34Date:12/05/2023 04:12 PM
Page 94 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40484QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V40483
LCS-V40483 LCSD-V40483Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 98.61030.0510.050mg/KgStyrene 77-121 3.9 20
0.049 98.61030.0510.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.3 20
0.040 81.079.60.0390.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.7 20
0.047 94.61030.0510.050mg/Kg 68-130 8.3 20
0.045 91.496.00.0480.050mg/Kg 71-129 4.9 20
0.050 10099.00.0490.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.0 20
0.051 1031040.0510.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.9 20
0.050 1001090.0540.050mg/Kg1,1,1-Trichloroethane 67-131 8.0 20
0.046 93.294.40.0470.050mg/Kg1,1,2-Trichloroethane 70-133 1.2 20
0.046 92.21010.0500.050mg/Kg 75-133 8.9 20
0.046 93.81040.0520.050mg/Kg 44-146 10.6 20
0.043 86.087.40.0430.050mg/Kg1,2,3-Trichloropropane 60-137 1.6 20
0.046 93.497.60.0480.050mg/Kg1,3,5-Trimethylbenzene 69-128 4.3 20
0.053 10795.80.0470.050mg/KgVinyl Acetate 60-140 10.8 20
0.040 80.486.80.0430.050mg/KgVinyl Chloride 48-147 7.6 20
0.047 94.499.60.0490.050mg/Kgo-Xylene 74-126 5.3 20
0.093 93.398.90.0980.100mg/Kgm,p-Xylene 75-124 5.8 20
1001004-Bromofluorobenzene (S)70-130
107109Dibromofluoromethane (S)84-123
100101 76-129
Page 14 of 34Date:12/05/2023 04:12 PM
Page 95 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40672
Associated Lab Samples: 89739, 89740, 89741, 89742
LRB-V40672 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/28/23 21:115.001.80<1.80µg/LAcetone
11/28/23 21:115.002.00<2.00µg/LAcrolein
11/28/23 21:115.000.230<0.230µg/LAcrylonitrile
11/28/23 21:110.5000.180<0.180µg/LBenzene
11/28/23 21:110.5000.210<0.210µg/LBromobenzene
11/28/23 21:111.000.420<0.420µg/LBromochloromethane
11/28/23 21:110.5000.160<0.160µg/LBromodichloromethane
11/28/23 21:115.001.50<1.50µg/LBromoform
11/28/23 21:111.000.280<0.280µg/LBromomethane
11/28/23 21:111.000.185<0.185µg/Ln-Butylbenzene
11/28/23 21:110.5000.200<0.200µg/Lsec-Butyl benzene
11/28/23 21:112.000.920<0.920µg/Ltert-Butyl benzene
11/28/23 21:115.000.150<0.150µg/LCarbon Disulfide
11/28/23 21:110.5000.180<0.180µg/LCarbon Tetrachloride
11/28/23 21:110.5000.190<0.190µg/LChlorobenzene
11/28/23 21:110.5000.190<0.190µg/LChlorodibromomethane
11/28/23 21:111.000.430<0.430µg/LChloroethane
11/28/23 21:110.5000.220<0.220µg/LChloroform
11/28/23 21:110.5000.220<0.220µg/LChloromethane
11/28/23 21:110.5000.200<0.200µg/L2-Chlorotoluene
11/28/23 21:110.5000.200<0.200µg/L4-Chlorotoluene
11/28/23 21:115.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
11/28/23 21:112.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
11/28/23 21:110.5000.200<0.200µg/L1,2-Dibromoethane
11/28/23 21:110.5000.230<0.230µg/LDibromomethane
11/28/23 21:110.5000.220<0.220µg/L1,2-Dichlorobenzene
11/28/23 21:110.5000.190<0.190µg/L1,3-Dichlorobenzene
Page 15 of 34Date:12/05/2023 04:12 PM
Page 96 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40672
Associated Lab Samples: 89739, 89740, 89741, 89742
LRB-V40672 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/28/23 21:110.5000.210<0.210µg/L1,4-Dichlorobenzene
11/28/23 21:115.001.20<1.20µg/LDichlorodifluoromethane
11/28/23 21:110.5000.240<0.240µg/L1,1-Dichloroethane
11/28/23 21:110.5000.150<0.150µg/L1,2-Dichloroethane
11/28/23 21:110.5000.150<0.150µg/L1,1-Dichloroethene
11/28/23 21:110.5000.200<0.200µg/Lcis-1,2-Dichloroethene
11/28/23 21:110.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
11/28/23 21:110.5000.190<0.190µg/L1,2-Dichloropropane
11/28/23 21:110.5000.130<0.130µg/L1,3-Dichloropropane
11/28/23 21:112.000.210<0.210µg/L2,2-Dichloropropane
11/28/23 21:110.5000.200<0.200µg/L1,1-Dichloropropene
11/28/23 21:110.5000.210<0.210µg/Lcis-1,3-Dichloropropene
11/28/23 21:110.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
11/28/23 21:1120042.0<42.0µg/LEthanol
11/28/23 21:110.5000.170<0.170µg/LEthylbenzene
11/28/23 21:1110.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
11/28/23 21:112.000.350<0.350µg/LHexachlorobutadiene
11/28/23 21:1110.01.30<1.30µg/Ln-Hexane
11/28/23 21:115.000.380<0.380µg/L2-Hexanone
11/28/23 21:115.000.180<0.180µg/LIsopropylbenzene
11/28/23 21:110.5000.089<0.089µg/L4-Isopropyl toluene
11/28/23 21:115.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
11/28/23 21:110.5000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
11/28/23 21:115.001.00<1.00µg/L4-Methyl-2-Pentanone
11/28/23 21:111.000.330<0.330µg/LMethylene Chloride
11/28/23 21:111.000.470<0.470µg/LNaphthalene
11/28/23 21:110.5000.190<0.190µg/Ln-Propylbenzene
Page 16 of 34Date:12/05/2023 04:12 PM
Page 97 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40672
Associated Lab Samples: 89739, 89740, 89741, 89742
LRB-V40672 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/28/23 21:110.5000.220<0.220µg/LStyrene
11/28/23 21:110.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
11/28/23 21:110.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
11/28/23 21:110.5000.220<0.220µg/L
11/28/23 21:110.5000.220<0.220µg/L
11/28/23 21:112.000.380<0.380µg/L1,2,3-Trichlorobenzene
11/28/23 21:111.000.310<0.310µg/L1,2,4-Trichlorobenzene
11/28/23 21:110.5000.160<0.160µg/L1,1,1-Trichloroethane
11/28/23 21:110.5000.096<0.096µg/L1,1,2-Trichloroethane
11/28/23 21:110.5000.180<0.180µg/L
11/28/23 21:110.5000.180<0.180µg/L
11/28/23 21:111.000.270<0.270µg/L1,2,3-Trichloropropane
11/28/23 21:110.5000.180<0.180µg/L1,3,5-Trimethylbenzene
11/28/23 21:112.001.00<1.00µg/LVinyl Acetate
11/28/23 21:110.5000.170<0.170µg/LVinyl Chloride
11/28/23 21:110.5000.210<0.210µg/Lo-Xylene
11/28/23 21:111.000.420<0.420µg/Lm,p-Xylene
11/28/23 21:114-Bromofluorobenzene (S)99.2 80-124
11/28/23 21:11Dibromofluoromethane (S)100 75-129
11/28/23 21:111,2-Dichloroethane - d4 (S)93.0 63-136
11/28/23 21:11 99.0 77-123
LCS-V40672 LCSD-V40672Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
53.9 13514658.440.0µg/LAcetone 40-166 8.0 20.0
Page 17 of 34Date:12/05/2023 04:12 PM
Page 98 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40672
LCS-V40672 LCSD-V40672Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.0 50.0*57.7*23.140.0µg/LAcrolein 70-130 14.3 20.0
30.7 76.7*85.034.040.0µg/LAcrylonitrile 81-127 10.2 20.0
21.8 10910721.420.0µg/LBenzene 77-128 1.8 20.0
21.1 10610220.420.0µg/LBromobenzene 78-129 3.3 20.0
21.4 10710520.920.0µg/LBromochloromethane 78-135 2.3 20.0
20.8 10410420.820.0µg/LBromodichloromethane 76-138 0.0 20.0
18.9 94.589.017.820.0µg/LBromoform 71-135 5.9 20.0
25.8 12912725.420.0µg/LBromomethane 41-168 1.5 20.0
20.8 10410220.320.0µg/Ln-Butylbenzene 68-134 2.4 20.0
21.6 10810520.920.0µg/Lsec-Butyl benzene 71-131 3.2 20.0
21.4 10710621.120.0µg/Ltert-Butyl benzene 70-132 1.4 20.0
22.1 11111122.120.0µg/LCarbon Disulfide 59-135 0.0 20.0
23.1 11611422.720.0µg/LCarbon Tetrachloride 72-142 1.7 20.0
21.8 10910821.520.0µg/LChlorobenzene 78-119 1.3 20.0
21.5 10810721.320.0µg/LChlorodibromomethane 75-134 0.9 20.0
26.1 13113226.320.0µg/LChloroethane 57-142 0.7 20.0
21.7 10910921.720.0µg/LChloroform 77-130 0.0 20.0
25.5 12813026.020.0µg/LChloromethane 47-145 1.9 20.0
21.1 10610420.820.0µg/L2-Chlorotoluene 74-126 1.4 20.0
20.8 10410120.220.0µg/L4-Chlorotoluene 78-129 2.9 20.0
21.7 10910721.320.0µg/LDi-Isopropyl Ether (DIPE)60-154 1.8 20.0
18.4 92.080.516.120.0µg/L1,2-Dibromo-3-Chloropropane 63-134 13.3 20.0
20.4 10210721.320.0µg/L1,2-Dibromoethane 77-135 4.3 20.0
21.3 10710220.320.0µg/LDibromomethane 76-138 4.8 20.0
21.3 10710220.420.0µg/L1,2-Dichlorobenzene 78-128 4.3 20.0
21.0 10510420.820.0µg/L1,3-Dichlorobenzene 77-125 0.9 20.0
Page 18 of 34* QC Fail Date:12/05/2023 04:12 PM
Page 99 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40672
LCS-V40672 LCSD-V40672Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.2 10610220.420.0µg/L1,4-Dichlorobenzene 75-126 3.8 20.0
27.2 13613627.120.0µg/LDichlorodifluoromethane 28-163 0.3 20.0
22.8 11411222.420.0µg/L1,1-Dichloroethane 70-130 1.7 20.0
20.5 10310120.120.0µg/L1,2-Dichloroethane 68-131 1.9 20.0
23.2 11611523.020.0µg/L1,1-Dichloroethene 70-154 0.8 20.0
21.7 10910821.620.0µg/Lcis-1,2-Dichloroethene 76-141 0.4 20.0
21.6 10811222.420.0µg/Ltrans-1,2-Dichloroethene 76-135 3.6 20.0
22.6 11310821.620.0µg/L1,2-Dichloropropane 77-130 4.5 20.0
20.6 10310420.820.0µg/L1,3-Dichloropropane 76-132 0.9 20.0
22.7 11411122.120.0µg/L2,2-Dichloropropane 29-149 2.6 20.0
22.9 11511122.220.0µg/L1,1-Dichloropropene 71-136 3.1 20.0
20.5 10310120.220.0µg/Lcis-1,3-Dichloropropene 65-140 1.4 20.0
20.3 10299.519.920.0µg/Ltrans-1,3-Dichloropropene 67-140 1.9 20.0
433 86.690.8454500µg/LEthanol 70-130 4.7 20.0
20.3 10298.519.720.0µg/LEthylbenzene 80-127 3.0 20.0
43.6 10910843.240.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20.0
21.4 10710621.220.0µg/LHexachlorobutadiene 61-134 0.9 20.0
22.8 11410020.020.0µg/Ln-Hexane 70-130 13.0 20.0
19.4 97.010621.120.0µg/L2-Hexanone 64-137 8.3 20.0
21.5 10810621.220.0µg/LIsopropylbenzene 70-130 1.4 20.0
21.3 10710521.020.0µg/L4-Isopropyl toluene 69-132 1.4 20.0
22.7 11412424.720.0µg/LMethyl Ethyl Ketone (MEK)71-134 8.4 20.0
20.0 10010320.520.0µg/LMethyl tert-butyl ether (MTBE)68-135 2.4 20.0
17.3 86.594.018.820.0µg/L4-Methyl-2-Pentanone 69-134 8.3 20.0
21.5 10811021.920.0µg/LMethylene Chloride 73-131 1.8 20.0
15.9 79.574.514.920.0µg/LNaphthalene 64-136 6.4 20.0
Page 19 of 34Date:12/05/2023 04:12 PM
Page 100 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V40674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V40672
LCS-V40672 LCSD-V40672Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.1 10610320.520.0µg/Ln-Propylbenzene 72-132 2.8 20.0
20.7 10410320.520.0µg/LStyrene 78-129 0.9 20.0
21.4 10710520.920.0µg/L1,1,1,2-Tetrachloroethane 79-134 2.3 20.0
20.8 10492.518.520.0µg/L1,1,2,2-Tetrachloroethane 62-127 11.7 20.0
22.3 11210921.820.0µg/L 80-129 2.2 20.0
21.0 10510320.620.0µg/L 76-131 1.9 20.0
16.7 83.578.015.620.0µg/L1,2,3-Trichlorobenzene 58-144 6.8 20.0
16.4 82.080.016.020.0µg/L1,2,4-Trichlorobenzene 66-139 2.4 20.0
22.5 11310921.720.0µg/L1,1,1-Trichloroethane 75-135 3.6 20.0
19.6 98.010120.120.0µg/L1,1,2-Trichloroethane 70-140 2.5 20.0
22.5 11311021.920.0µg/L 77-133 2.7 20.0
26.5 13313326.520.0µg/L 62-148 0.0 20.0
21.7 10910621.220.0µg/L1,2,3-Trichloropropane 71-127 2.3 20.0
21.1 10610420.820.0µg/L1,3,5-Trimethylbenzene 75-131 1.4 20.0
18.4 92.085.017.020.0µg/LVinyl Acetate 34-167 7.9 20.0
27.6 138142*28.420.0µg/LVinyl Chloride 57-141 2.8 20.0
20.6 10310320.620.0µg/Lo-Xylene 78-128 0.0 20.0
43.3 10810843.240.0µg/Lm,p-Xylene 77-133 0.2 20.0
98.898.44-Bromofluorobenzene (S)80-124
101102Dibromofluoromethane (S)75-129
97.698.61,2-Dichloroethane - d4 (S)63-136
99.699.4 77-123
Page 20 of 34* QC Fail Date:12/05/2023 04:12 PM
Page 101 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40413QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V40378
Associated Lab Samples: 89739, 89740, 89741, 89742
LRB-V40378 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/20/23 17:392.000.302<0.302µg/LAcenaphthene
11/20/23 17:392.000.297<0.297µg/LAcenaphthylene
11/20/23 17:395.002.05<2.05µg/LAniline
11/20/23 17:392.000.836<0.836µg/LAnthracene
11/20/23 17:392.000.637<0.637µg/LBenzo(a)anthracene
11/20/23 17:392.001.02<1.02µg/LBenzo(a)pyrene
11/20/23 17:395.002.49<2.49µg/LBenzo(b)fluoranthene
11/20/23 17:395.001.01<1.01µg/LBenzo(g,h,i)perylene
11/20/23 17:395.001.99<1.99µg/LBenzo(k)fluoranthene
11/20/23 17:3910.01.10<1.10µg/LBenzoic Acid
11/20/23 17:395.000.684<0.684µg/LBenzyl alcohol
11/20/23 17:395.000.468<0.468µg/LBis(2-Chloroethoxy)methane
11/20/23 17:395.001.04<1.04µg/LBis(2-Chloroethyl)ether
11/20/23 17:395.001.08<1.08µg/LBis(2-Chloroisopropyl)ether
11/20/23 17:3910.03.46<3.46µg/LBis(2-ethylhexyl)phthalate
11/20/23 17:395.001.11<1.11µg/L4-Bromophenyl phenyl ether
11/20/23 17:395.001.83<1.83µg/LButyl benzyl phthalate
11/20/23 17:395.001.18<1.18µg/L4-Chloro-3-methylphenol
11/20/23 17:395.001.33<1.33µg/L4-Chloroaniline
11/20/23 17:3920.01.83<1.83µg/L2-Chloronaphthalene
11/20/23 17:3910.00.938<0.938µg/L2-Chlorophenol
11/20/23 17:395.001.71<1.71µg/L4-Chlorophenyl phenyl ether
11/20/23 17:392.000.405<0.405µg/LChrysene
11/20/23 17:392.000.434<0.434µg/LDibenz(a,h)anthracene
11/20/23 17:395.000.856<0.856µg/LDibenzofuran
11/20/23 17:395.002.00<2.00µg/L1,2-Dichlorobenzene
11/20/23 17:395.002.00<2.00µg/L1,3-Dichlorobenzene
Page 21 of 34Date:12/05/2023 04:12 PM
Page 102 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40413QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V40378
Associated Lab Samples: 89739, 89740, 89741, 89742
LRB-V40378 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/20/23 17:395.002.05<2.05µg/L1,4-Dichlorobenzene
11/20/23 17:395.001.89<1.89µg/L3,3'-Dichlorobenzidine
11/20/23 17:3910.01.46<1.46µg/L2,4-Dichlorophenol
11/20/23 17:395.000.745<0.745µg/LDiethyl phthalate
11/20/23 17:395.000.939<0.939µg/LDimethyl phthalate
11/20/23 17:3920.01.57<1.57µg/L2,4-Dimethylphenol
11/20/23 17:395.002.06<2.06µg/LDi-n-butyl phthalate
11/20/23 17:3910.02.07<2.07µg/L4,6-Dinitro-2-methylphenol
11/20/23 17:3910.01.92<1.92µg/L2,4-Dinitrophenol
11/20/23 17:395.001.11<1.11µg/L2,4-Dinitrotoluene
11/20/23 17:395.000.809<0.809µg/L2,6-Dinitrotoluene
11/20/23 17:395.001.65<1.65µg/LDi-n-Octyl Phthalate
11/20/23 17:392.000.250<0.250µg/LFluoranthene
11/20/23 17:392.000.807<0.807µg/LFluorene
11/20/23 17:395.000.979<0.979µg/LHexachlorobenzene
11/20/23 17:395.002.73<2.73µg/LHexachlorobutadiene
11/20/23 17:395.002.05<2.05µg/LHexachlorocyclopentadiene
11/20/23 17:395.001.76<1.76µg/LHexachloroethane
11/20/23 17:392.000.477<0.477µg/LIndeno(1,2,3-cd)pyrene
11/20/23 17:395.000.444<0.444µg/LIsophorone
11/20/23 17:392.001.14<1.14µg/L1-Methylnaphthalene
11/20/23 17:392.000.666<0.666µg/L2-Methylnaphthalene
11/20/23 17:395.001.15<1.15µg/L2-Methylphenol
11/20/23 17:3910.00.880<0.880µg/L3&4 Methylphenol
11/20/23 17:392.000.728<0.728µg/LNaphthalene
11/20/23 17:395.001.39<1.39µg/L2-Nitroaniline
11/20/23 17:395.001.39<1.39µg/L3-Nitroaniline
Page 22 of 34Date:12/05/2023 04:12 PM
Page 103 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40413QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V40378
Associated Lab Samples: 89739, 89740, 89741, 89742
LRB-V40378 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/20/23 17:395.001.53<1.53µg/L4-Nitroaniline
11/20/23 17:395.000.905<0.905µg/LNitrobenzene
11/20/23 17:395.000.493<0.493µg/L2-Nitrophenol
11/20/23 17:3910.01.23<1.23µg/L4-Nitrophenol
11/20/23 17:395.000.450<0.450µg/LN-Nitrosodimethylamine
11/20/23 17:395.001.10<1.10µg/LN-Nitrosodiphenylamine
11/20/23 17:395.000.641<0.641µg/LN-Nitroso-di-n-propylamine
11/20/23 17:395.001.43<1.43µg/LPentachlorophenol
11/20/23 17:392.000.428<0.428µg/LPhenanthrene
11/20/23 17:395.000.651<0.651µg/LPhenol
11/20/23 17:392.000.434<0.434µg/LPyrene
11/20/23 17:395.002.21<2.21µg/L1,2,4-Trichlorobenzene
11/20/23 17:395.001.31<1.31µg/L2,4,5-Trichlorophenol
11/20/23 17:395.001.32<1.32µg/L2,4,6-Trichlorophenol
11/20/23 17:392-Fluorobiphenyl (S)61.2 44-119
11/20/23 17:392-Fluorophenol (S)35.4 19-119
11/20/23 17:39Nitrobenzene-d5 (S)57.6 44-120
11/20/23 17:394-Terphenyl-d14 (S)74.2 50-134
11/20/23 17:392,4,6-Tribromophenol (S)76.8 43-140
11/20/23 17:39Phenol-d5 (S)23.0 11-100
LCS-V40378 LCSD-V40378Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
26.8 53.653.226.650.0µg/LAcenaphthene 38-117 0.7 20.0
27.3 54.653.426.750.0µg/LAcenaphthylene 41-130 2.2 20.0
Page 23 of 34Date:12/05/2023 04:12 PM
Page 104 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40413QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V40378
LCS-V40378 LCSD-V40378Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
38.7 77.479.239.650.0µg/LAniline 12-197 2.2 20.0
37.7 75.475.437.750.0µg/LAnthracene 57-123 0.0 20.0
34.3 68.666.433.250.0µg/LBenzo(a)anthracene 58-125 3.2 20.0
33.2 66.464.032.050.0µg/LBenzo(a)pyrene 54-128 3.6 20.0
30.8 61.659.429.750.0µg/LBenzo(b)fluoranthene 53-131 3.6 20.0
30.7 61.459.629.850.0µg/LBenzo(g,h,i)perylene 50-134 2.9 20.0
29.6 59.256.228.150.0µg/LBenzo(k)fluoranthene 53-131 5.1 20.0
10.2 20.423.011.550.0µg/LBenzoic Acid 10-125 11.9 20.0
26.0 52.051.625.850.0µg/LBenzyl alcohol 31-112 0.7 20.0
25.5 51.050.025.050.0µg/LBis(2-Chloroethoxy)methane 48-120 1.9 20.0
23.7 47.445.222.650.0µg/LBis(2-Chloroethyl)ether 43-118 4.7 20.0
21.8 43.641.620.850.0µg/LBis(2-Chloroisopropyl)ether 37-130 4.6 20.0
38.7 77.475.037.550.0µg/LBis(2-ethylhexyl)phthalate 55-135 3.1 20.0
32.0 64.062.631.350.0µg/L4-Bromophenyl phenyl ether 55-124 2.2 20.0
36.4 72.872.036.050.0µg/LButyl benzyl phthalate 53-134 1.1 20.0
30.0 60.058.029.050.0µg/L4-Chloro-3-methylphenol 52-119 3.3 20.0
27.5 55.055.627.850.0µg/L4-Chloroaniline 33-117 1.0 20.0
25.0 50.049.224.650.0µg/L2-Chloronaphthalene 40-116 1.6 20.0
25.4 50.849.024.550.0µg/L2-Chlorophenol 38-117 3.6 20.0
28.4 56.855.827.950.0µg/L4-Chlorophenyl phenyl ether 53-121 1.7 20.0
35.3 70.668.234.150.0µg/LChrysene 59-123 3.4 20.0
28.2 56.452.026.050.0µg/LDibenz(a,h)anthracene 51-134 8.1 20.0
29.4 58.857.828.950.0µg/LDibenzofuran 53-118 1.7 20.0
19.4 38.837.218.650.0µg/L1,2-Dichlorobenzene 32-111 4.2 20.0
18.9 37.835.617.850.0µg/L1,3-Dichlorobenzene 28-110 5.9 20.0
18.4 36.834.017.050.0µg/L1,4-Dichlorobenzene 29-112 7.9 20.0
Page 24 of 34Date:12/05/2023 04:12 PM
Page 105 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40413QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V40378
LCS-V40378 LCSD-V40378Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
29.4 58.854.227.150.0µg/L3,3'-Dichlorobenzidine 27-129 8.1 20.0
27.1 54.253.626.850.0µg/L2,4-Dichlorophenol 47-121 1.1 20.0
37.7 75.473.236.650.0µg/LDiethyl phthalate 56-125 2.9 20.0
36.9 73.871.635.850.0µg/LDimethyl phthalate 45-127 3.0 20.0
37.9 75.876.638.350.0µg/L2,4-Dimethylphenol 31-124 1.0 20.0
42.4 84.881.640.850.0µg/LDi-n-butyl phthalate 59-127 3.8 20.0
32.2 64.463.631.850.0µg/L4,6-Dinitro-2-methylphenol 44-137 1.2 20.0
31.2 62.456.428.250.0µg/L2,4-Dinitrophenol 23-143 10.1 20.0
40.4 80.877.238.650.0µg/L2,4-Dinitrotoluene 57-128 4.5 20.0
37.6 75.271.835.950.0µg/L2,6-Dinitrotoluene 57-124 4.6 20.0
32.3 64.662.831.450.0µg/LDi-n-Octyl Phthalate 51-140 2.8 20.0
38.7 77.474.837.450.0µg/LFluoranthene 57-128 3.4 20.0
32.1 64.262.831.450.0µg/LFluorene 52-124 2.2 20.0
38.0 76.073.036.550.0µg/LHexachlorobenzene 53-125 4.0 20.0
20.5 41.039.819.950.0µg/LHexachlorobutadiene 22-124 2.9 20.0
15.8 31.6*31.0*15.550.0µg/LHexachlorocyclopentadiene 32-117 1.9 20.0
17.3 34.633.616.850.0µg/LHexachloroethane 21-115 2.9 20.0
31.6 63.260.630.350.0µg/LIndeno(1,2,3-cd)pyrene 52-134 4.2 20.0
25.4 50.851.025.550.0µg/LIsophorone 42-124 0.3 20.0
20.5 41.040.8*20.450.0µg/L1-Methylnaphthalene 41-119 0.4 20.0
20.7 41.441.020.550.0µg/L2-Methylnaphthalene 40-121 0.9 20.0
24.0 48.047.823.950.0µg/L2-Methylphenol 30-117 0.4 20.0
20.2 40.440.420.250.0µg/L3&4 Methylphenol 29-110 0.0 20.0
20.0 40.038.8*19.450.0µg/LNaphthalene 40-121 3.0 20.0
33.8 67.664.432.250.0µg/L2-Nitroaniline 55-127 4.8 20.0
34.9 69.867.433.750.0µg/L3-Nitroaniline 41-128 3.4 20.0
Page 25 of 34* QC Fail Date:12/05/2023 04:12 PM
Page 106 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40413QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V40378
LCS-V40378 LCSD-V40378Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
38.0 76.074.037.050.0µg/L4-Nitroaniline 45-135 2.6 20.0
24.7 49.448.224.150.0µg/LNitrobenzene 45-121 2.4 20.0
24.4 48.848.424.250.0µg/L2-Nitrophenol 47-123 0.8 20.0
13.4 26.828.214.150.0µg/L4-Nitrophenol 10-105 5.0 20.0
15.9 31.832.416.250.0µg/LN-Nitrosodimethylamine 10-119 1.8 20.0
43.5 87.083.841.950.0µg/LN-Nitrosodiphenylamine 51-123 3.7 20.0
27.8 55.652.826.450.0µg/LN-Nitroso-di-n-propylamine 49-119 5.1 20.0
39.7 79.477.638.850.0µg/LPentachlorophenol 35-138 2.2 20.0
37.1 74.273.036.550.0µg/LPhenanthrene 59-120 1.6 20.0
11.9 23.825.212.650.0µg/LPhenol 12-58 5.7 20.0
36.8 73.671.235.650.0µg/LPyrene 57-126 3.3 20.0
19.3 38.637.018.550.0µg/L1,2,4-Trichlorobenzene 29-126 4.2 20.0
31.4 62.862.231.150.0µg/L2,4,5-Trichlorophenol 53-123 0.9 20.0
32.0 64.062.431.250.0µg/L2,4,6-Trichlorophenol 50-125 2.5 20.0
57.456.82-Fluorobiphenyl (S)44-119
32.634.02-Fluorophenol (S)19-119
50.449.6Nitrobenzene-d5 (S)44-120
71.270.64-Terphenyl-d14 (S)50-134
77.878.42,4,6-Tribromophenol (S)43-140
21.923.2Phenol-d5 (S)11-100
Page 26 of 34Date:12/05/2023 04:12 PM
Page 107 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40463QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40450
Associated Lab Samples: 89743, 89744, 89745, 89746
LRB-V40450 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/21/23 16:020.6600.116<0.116mg/KgAcenaphthene
11/21/23 16:020.6600.105<0.105mg/KgAcenaphthylene
11/21/23 16:020.6600.152<0.152mg/KgAniline
11/21/23 16:020.6600.143<0.143mg/KgAnthracene
11/21/23 16:020.6600.139<0.139mg/KgBenzo(a)anthracene
11/21/23 16:020.6600.147<0.147mg/KgBenzo(a)pyrene
11/21/23 16:020.6600.146<0.146mg/KgBenzo(b)fluoranthene
11/21/23 16:020.6600.136<0.136mg/KgBenzo(g,h,i)perylene
11/21/23 16:020.6600.137<0.137mg/KgBenzo(k)fluoranthene
11/21/23 16:022.000.580<0.580mg/KgBenzoic Acid
11/21/23 16:020.6600.105<0.105mg/KgBenzyl alcohol
11/21/23 16:020.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
11/21/23 16:020.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
11/21/23 16:020.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
11/21/23 16:020.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
11/21/23 16:020.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
11/21/23 16:020.3300.113<0.113mg/KgButyl benzyl phthalate
11/21/23 16:020.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
11/21/23 16:020.3300.112<0.112mg/Kg4-Chloroaniline
11/21/23 16:020.6600.116<0.116mg/Kg2-Chloronaphthalene
11/21/23 16:020.6600.098<0.098mg/Kg2-Chlorophenol
11/21/23 16:021.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
11/21/23 16:020.6600.142<0.142mg/KgChrysene
11/21/23 16:020.6600.230<0.230mg/KgDibenz(a,h)anthracene
11/21/23 16:020.6600.119<0.119mg/KgDibenzofuran
11/21/23 16:020.6600.094<0.094mg/Kg1,2-Dichlorobenzene
11/21/23 16:020.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 27 of 34Date:12/05/2023 04:12 PM
Page 108 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40463QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40450
Associated Lab Samples: 89743, 89744, 89745, 89746
LRB-V40450 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/21/23 16:020.3300.097<0.097mg/Kg1,4-Dichlorobenzene
11/21/23 16:020.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
11/21/23 16:020.6600.095<0.095mg/Kg2,4-Dichlorophenol
11/21/23 16:020.6600.180<0.180mg/KgDiethyl phthalate
11/21/23 16:020.6600.174<0.174mg/KgDimethyl phthalate
11/21/23 16:020.3300.108<0.108mg/Kg2,4-Dimethylphenol
11/21/23 16:020.6600.107<0.107mg/KgDi-n-butyl phthalate
11/21/23 16:021.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
11/21/23 16:021.500.520<0.520mg/Kg2,4-Dinitrophenol
11/21/23 16:020.6600.096<0.096mg/Kg2,4-Dinitrotoluene
11/21/23 16:020.6600.108<0.108mg/Kg2,6-Dinitrotoluene
11/21/23 16:020.3300.143<0.143mg/KgDi-n-Octyl Phthalate
11/21/23 16:020.6600.123<0.123mg/KgFluoranthene
11/21/23 16:020.6600.128<0.128mg/KgFluorene
11/21/23 16:020.6600.106<0.106mg/KgHexachlorobenzene
11/21/23 16:020.6600.097<0.097mg/KgHexachlorobutadiene
11/21/23 16:020.6600.157<0.157mg/KgHexachlorocyclopentadiene
11/21/23 16:020.6600.079<0.079mg/KgHexachloroethane
11/21/23 16:020.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
11/21/23 16:020.6600.191<0.191mg/KgIsophorone
11/21/23 16:020.6600.106<0.106mg/Kg1-Methylnaphthalene
11/21/23 16:020.6600.100<0.100mg/Kg2-Methylnaphthalene
11/21/23 16:020.6600.097<0.097mg/Kg2-Methylphenol
11/21/23 16:020.6600.084<0.084mg/Kg3&4 Methylphenol
11/21/23 16:020.6600.144<0.144mg/KgNaphthalene
11/21/23 16:020.6600.096<0.096mg/Kg2-Nitroaniline
11/21/23 16:020.6600.120<0.120mg/Kg3-Nitroaniline
Page 28 of 34Date:12/05/2023 04:12 PM
Page 109 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40463QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40450
Associated Lab Samples: 89743, 89744, 89745, 89746
LRB-V40450 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/21/23 16:020.3300.093<0.093mg/Kg4-Nitroaniline
11/21/23 16:020.3300.116<0.116mg/KgNitrobenzene
11/21/23 16:020.6600.088<0.088mg/Kg2-Nitrophenol
11/21/23 16:020.6600.117<0.117mg/Kg4-Nitrophenol
11/21/23 16:020.6600.263<0.263mg/KgN-Nitrosodimethylamine
11/21/23 16:020.6600.181<0.181mg/KgN-Nitrosodiphenylamine
11/21/23 16:020.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
11/21/23 16:021.000.347<0.347mg/KgPentachlorophenol
11/21/23 16:020.6600.208<0.208mg/KgPhenanthrene
11/21/23 16:020.6600.112<0.112mg/KgPhenol
11/21/23 16:020.6600.134<0.134mg/KgPyrene
11/21/23 16:020.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
11/21/23 16:020.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
11/21/23 16:020.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
11/21/23 16:022-Fluorobiphenyl (S)84.4 44-115
11/21/23 16:022-Fluorophenol (S)78.6 35-115
11/21/23 16:02Nitrobenzene-d5 (S)78.4 37-122
11/21/23 16:024-Terphenyl-d14 (S)79.6 54-127
11/21/23 16:022,4,6-Tribromophenol (S)86.1 39-132
11/21/23 16:02Phenol-d5 (S)78.0 34-121
LCS-V40450 LCSD-V40450Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.45 86.884.41.411.67mg/KgAcenaphthene 40-123 2.7 20
1.42 85.083.81.401.67mg/KgAcenaphthylene 32-132 1.4 20
Page 29 of 34Date:12/05/2023 04:12 PM
Page 110 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40463QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40450
LCS-V40450 LCSD-V40450Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
2.23 1341252.081.67mg/KgAniline 12-197 6.9 20
1.61 96.492.81.551.67mg/KgAnthracene 47-123 3.7 20
1.38 82.679.61.331.67mg/KgBenzo(a)anthracene 49-126 3.6 20
1.35 80.877.81.301.67mg/KgBenzo(a)pyrene 45-129 3.7 20
1.20 71.869.41.161.67mg/KgBenzo(b)fluoranthene 45-132 3.3 20
1.23 73.671.21.191.67mg/KgBenzo(g,h,i)perylene 43-134 3.3 20
1.21 72.469.41.161.67mg/KgBenzo(k)fluoranthene 47-132 4.2 20
<0.580 0.0*0.0*<0.5801.67mg/KgBenzoic Acid 10-83 0.0 20
1.44 86.281.41.361.67mg/KgBenzyl alcohol 29-122 5.7 20
1.21 72.469.41.161.67mg/KgBis(2-Chloroethoxy)methane 36-121 4.2 20
1.14 68.264.01.071.67mg/KgBis(2-Chloroethyl)ether 31-120 6.3 20
1.24 74.271.21.191.67mg/KgBis(2-Chloroisopropyl)ether 33-131 4.1 20
1.51 90.487.41.461.67mg/KgBis(2-ethylhexyl)phthalate 51-133 3.3 20
1.46 87.484.41.411.67mg/Kg4-Bromophenyl phenyl ether 46-124 3.4 20
1.46 87.485.61.431.67mg/KgButyl benzyl phthalate 48-132 2.0 20
1.31 78.476.61.281.67mg/Kg4-Chloro-3-methylphenol 45-122 2.3 20
1.22 73.070.01.171.67mg/Kg4-Chloroaniline 17-106 4.1 20
1.47 88.085.61.431.67mg/Kg2-Chloronaphthalene 41-114 2.7 20
1.38 82.678.41.311.67mg/Kg2-Chlorophenol 34-121 5.2 20
1.43 85.683.21.391.67mg/Kg4-Chlorophenyl phenyl ether 45-121 2.8 20
1.43 85.683.21.391.67mg/KgChrysene 50-124 2.8 20
1.13 67.665.81.101.67mg/KgDibenz(a,h)anthracene 45-134 2.6 20
1.49 89.287.41.461.67mg/KgDibenzofuran 44-120 2.0 20
1.29 77.274.81.251.67mg/Kg1,2-Dichlorobenzene 33-117 3.1 20
1.26 75.471.21.191.67mg/Kg1,3-Dichlorobenzene 30-115 5.7 20
1.19 71.269.41.161.67mg/Kg1,4-Dichlorobenzene 31-115 2.5 20
Page 30 of 34* QC Fail Date:12/05/2023 04:12 PM
Page 111 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40463QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40450
LCS-V40450 LCSD-V40450Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.16 69.461.61.031.67mg/Kg3,3'-Dichlorobenzidine 22-121 11.8 20
1.31 78.476.61.281.67mg/Kg2,4-Dichlorophenol 40-122 2.3 20
1.55 92.891.01.521.67mg/KgDiethyl phthalate 50-124 1.9 20
1.56 93.492.21.541.67mg/KgDimethyl phthalate 48-124 1.2 20
1.64 98.296.41.611.67mg/Kg2,4-Dimethylphenol 30-127 1.8 20
1.70 10297.01.621.67mg/KgDi-n-butyl phthalate 51-128 4.8 20
1.42 85.077.81.301.67mg/Kg4,6-Dinitro-2-methylphenol 29-132 8.8 20
1.16 69.454.40.9091.67mg/Kg2,4-Dinitrophenol 27-129 24.2*20
1.67 10096.41.611.67mg/Kg2,4-Dinitrotoluene 48-126 3.6 20
1.57 94.092.21.541.67mg/Kg2,6-Dinitrotoluene 46-124 1.9 20
1.25 74.871.81.201.67mg/KgDi-n-Octyl Phthalate 45-140 4.0 20
1.57 94.091.61.531.67mg/KgFluoranthene 50-127 2.5 20
1.52 91.089.81.501.67mg/KgFluorene 43-125 1.3 20
1.63 97.692.81.551.67mg/KgHexachlorobenzene 45-122 5.0 20
1.37 82.079.01.321.67mg/KgHexachlorobutadiene 32-123 3.7 20
1.12 67.062.21.041.67mg/KgHexachlorocyclopentadiene 32-117 7.4 20
1.24 74.271.81.201.67mg/KgHexachloroethane 28-117 3.2 20
1.28 76.672.41.211.67mg/KgIndeno(1,2,3-cd)pyrene 45-133 5.6 20
1.16 69.468.21.141.67mg/KgIsophorone 30-122 1.7 20
1.24 74.272.41.211.67mg/Kg1-Methylnaphthalene 40-119 2.4 20
1.27 76.073.61.231.67mg/Kg2-Methylnaphthalene 38-122 3.2 20
1.39 83.278.41.311.67mg/Kg2-Methylphenol 32-122 5.9 20
1.23 73.670.61.181.67mg/Kg3&4 Methylphenol 34-119 4.1 20
1.21 72.469.41.161.67mg/KgNaphthalene 35-123 4.2 20
1.44 86.285.61.431.67mg/Kg2-Nitroaniline 44-127 0.6 20
1.37 82.075.41.261.67mg/Kg3-Nitroaniline 33-119 8.3 20
Page 31 of 34* QC Fail Date:12/05/2023 04:12 PM
Page 112 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V40463QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V40450
LCS-V40450 LCSD-V40450Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.60 95.894.01.571.67mg/Kg4-Nitroaniline 63-147 1.8 20
1.23 73.672.41.211.67mg/KgNitrobenzene 34-122 1.6 20
1.23 73.670.61.181.67mg/Kg2-Nitrophenol 36-123 4.1 20
1.29 77.275.41.261.67mg/Kg4-Nitrophenol 30-132 2.3 20
1.09 65.264.01.071.67mg/KgN-Nitrosodimethylamine 10-146 1.8 20
1.79 1071041.731.67mg/KgN-Nitrosodiphenylamine 38-127 3.4 20
1.37 82.077.81.301.67mg/KgN-Nitroso-di-n-propylamine 36-120 5.2 20
1.50 89.880.21.341.67mg/KgPentachlorophenol 25-133 11.2 20
1.57 94.090.41.511.67mg/KgPhenanthrene 50-121 3.8 20
1.31 78.474.81.251.67mg/KgPhenol 34-121 4.6 20
1.41 84.483.21.391.67mg/KgPyrene 47-127 1.4 20
1.23 73.671.21.191.67mg/Kg1,2,4-Trichlorobenzene 34-118 3.3 20
1.41 84.482.61.381.67mg/Kg2,4,5-Trichlorophenol 41-124 2.1 20
1.43 85.685.01.421.67mg/Kg2,4,6-Trichlorophenol 39-126 0.7 20
86.286.82-Fluorobiphenyl (S)44-115
82.882.22-Fluorophenol (S)35-115
72.472.4Nitrobenzene-d5 (S)37-122
82.081.44-Terphenyl-d14 (S)54-127
98.198.12,4,6-Tribromophenol (S)39-132
81.078.3Phenol-d5 (S)34-121
Page 32 of 34Date:12/05/2023 04:12 PM
Page 113 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L720352QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L720005
Associated Lab Samples: 89743, 89744, 89745, 89746
LRB-L720005 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/05/23 09:320.2000.1410.165mg/KgChromium, Hexavalent
LCS-L720005Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1084.314.00mg/KgChromium, Hexavalent 80-120
V 89746-DUP-L720005Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20 12/05/23 10:058.6<0.2000.218mg/KgChromium, Hexavalent
V 89746-MS-L720005Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
5.51 13.0*39.9<1.41mg/KgChromium, Hexavalent 75-125
Page 33 of 34Date:12/05/2023 04:12 PM
Page 114 of 117
Quality Control Data
23-321-0112Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
Dry Weight Determination
SW-DRYWT
V40437QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89523-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/21/23 12:307.71.731.87%Moisture
V 89746-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/21/23 12:300.910.810.7%Moisture
Page 34 of 34Date:12/05/2023 04:12 PM
Page 115 of 117
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-321-0112
Mid-Atlantic Associates, Inc. - Charlotte
01138
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 3.4C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:11/17/2023 17:00:47
Special precautions or instructions included?
Comments:
Page 116 of 117
Page 117 of 117

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/1/2023
Mid-Atlantic Associates, Inc. - Charlotte Troy Holzschuh
1125 E. Morehead Street, Suite 104 Charlotte, NC, 28204
Ref: Analytical Testing
Lab Report Number: 23-326-0001 Client Project Description: Former Winston Container
Dear Troy Holzschuh:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/21/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 30
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-326-0001
Page 2 of 30
Report Number:
Sample Summary Table
Client Project Description:
23-326-0001
Former Winston Container
Lab No Client Sample ID Matrix Date Collected Date Received
11/21/2023 12:05Air 90164 SSV-1 11/21/2023 13:55
11/21/2023 12:51Air 90165 SSV-2 11/21/2023 13:55
11/21/2023 12:51Air 90166 DUP-4 11/21/2023 13:55
11/21/2023 12:24Air 90167 SSV-4 11/21/2023 13:55
11/21/2023 12:34Air 90168 SSV-3 11/21/2023 13:55
Page 3 of 30
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-326-0001
Report Limit
Project:Former Winston Container
V 90164SSV-1
17.4 11/30/2023 21:25TO-15 Acetone µg/m3 0.202
10.4 11/30/2023 21:25TO-15 Benzene µg/m3 0.073
2.34 11/30/2023 21:25TO-15 1,3-Butadiene µg/m3 0.328
JB0.442 11/30/2023 21:25TO-15 Carbon Disulfide µg/m3 0.060
7.64 11/30/2023 21:25TO-15 Cyclohexane µg/m3 0.161
2.77 11/30/2023 21:25TO-15 Dichlorodifluoromethane µg/m3 0.134
7.41 11/30/2023 21:25TO-15 Ethyl Acetate µg/m3 0.136
11.1 11/30/2023 21:25TO-15 Ethylbenzene µg/m3 0.106
2.85 11/30/2023 21:25TO-15 4-Ethyltoluene µg/m3 0.128
9.79 11/30/2023 21:25TO-15 Heptane µg/m3 0.143
15.9 11/30/2023 21:25TO-15 n-Hexane µg/m3 0.047
8.86 11/30/2023 21:25TO-15 Isopropyl Alcohol µg/m3 0.139
3.41 11/30/2023 21:25TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J0.651 11/30/2023 21:25TO-15 4-Methyl-2-Pentanone µg/m3 0.121
JB1.40 11/30/2023 21:25TO-15 Methylene Chloride µg/m3 0.488
13.9 11/30/2023 21:25TO-15 Propene µg/m3 0.242
J0.787 11/30/2023 21:25TO-15 Styrene µg/m3 0.124
J1.06 11/30/2023 21:25TO-15 Tetrachloroethene µg/m3 0.181
J1.38 11/30/2023 21:25TO-15 Tetrahydrofuran µg/m3 0.107
53.4 11/30/2023 21:25TO-15 Toluene µg/m3 0.090
J0.758 11/30/2023 21:25TO-15 1,1,1-Trichloroethane µg/m3 0.144
415 11/30/2023 13:39TO-15 Trichlorofluoromethane µg/m3 2.60
8.90 11/30/2023 21:25TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
2.64 11/30/2023 21:25TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
11.6 11/30/2023 21:25TO-15 o-Xylene µg/m3 0.157
30.6 11/30/2023 21:25TO-15 m,p-Xylene µg/m3 0.217
42.2 11/30/2023 21:25TO-15 Xylene (Total)µg/m3 0.157
V 90165SSV-2
14.0 11/30/2023 22:14TO-15 Acetone µg/m3 0.202
8.38 11/30/2023 22:14TO-15 Benzene µg/m3 0.073
1.63 11/30/2023 22:14TO-15 1,3-Butadiene µg/m3 0.328
JB0.784 11/30/2023 22:14TO-15 Carbon Disulfide µg/m3 0.060
16.6 11/30/2023 22:14TO-15 Cyclohexane µg/m3 0.161
2.74 11/30/2023 22:14TO-15 Dichlorodifluoromethane µg/m3 0.134
24.0 11/30/2023 22:14TO-15 Ethyl Acetate µg/m3 0.136
5.15 11/30/2023 22:14TO-15 Ethylbenzene µg/m3 0.106
Page 4 of 30
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-326-0001
Report Limit
Project:Former Winston Container
V 90165SSV-2
J1.00 11/30/2023 22:14TO-15 4-Ethyltoluene µg/m3 0.128
J0.666 11/30/2023 22:14TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
8.38 11/30/2023 22:14TO-15 Heptane µg/m3 0.143
56.2 11/30/2023 22:14TO-15 n-Hexane µg/m3 0.047
B6.36 11/30/2023 22:14TO-15 Isopropyl Alcohol µg/m3 0.139
7.11 11/30/2023 22:14TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J0.880 11/30/2023 22:14TO-15 4-Methyl-2-Pentanone µg/m3 0.121
B1.89 11/30/2023 22:14TO-15 Methylene Chloride µg/m3 0.488
12.3 11/30/2023 22:14TO-15 Propene µg/m3 0.242
J0.477 11/30/2023 22:14TO-15 Styrene µg/m3 0.124
J0.603 11/30/2023 22:14TO-15 Tetrachloroethene µg/m3 0.181
J0.775 11/30/2023 22:14TO-15 Tetrahydrofuran µg/m3 0.107
37.4 11/30/2023 22:14TO-15 Toluene µg/m3 0.090
309 11/30/2023 14:16TO-15 Trichlorofluoromethane µg/m3 2.60
3.87 11/30/2023 22:14TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J1.09 11/30/2023 22:14TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
5.05 11/30/2023 22:14TO-15 o-Xylene µg/m3 0.157
14.8 11/30/2023 22:14TO-15 m,p-Xylene µg/m3 0.217
19.9 11/30/2023 22:14TO-15 Xylene (Total)µg/m3 0.157
V 90166DUP-4
11.9 11/30/2023 23:03TO-15 Acetone µg/m3 0.202
17.5 11/30/2023 23:03TO-15 Benzene µg/m3 0.073
JB0.868 11/30/2023 23:03TO-15 Carbon Disulfide µg/m3 0.060
16.1 11/30/2023 23:03TO-15 Cyclohexane µg/m3 0.161
2.48 11/30/2023 23:03TO-15 Dichlorodifluoromethane µg/m3 0.134
23.9 11/30/2023 23:03TO-15 Ethyl Acetate µg/m3 0.136
18.7 11/30/2023 23:03TO-15 Ethylbenzene µg/m3 0.106
3.95 11/30/2023 23:03TO-15 4-Ethyltoluene µg/m3 0.128
J0.666 11/30/2023 23:03TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
19.4 11/30/2023 23:03TO-15 Heptane µg/m3 0.143
55.7 11/30/2023 23:03TO-15 n-Hexane µg/m3 0.047
JB4.51 11/30/2023 23:03TO-15 Isopropyl Alcohol µg/m3 0.139
2.11 11/30/2023 23:03TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J0.892 11/30/2023 23:03TO-15 4-Methyl-2-Pentanone µg/m3 0.121
B2.55 11/30/2023 23:03TO-15 Methylene Chloride µg/m3 0.488
10.5 11/30/2023 23:03TO-15 Propene µg/m3 0.242
Page 5 of 30
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-326-0001
Report Limit
Project:Former Winston Container
V 90166DUP-4
J1.51 11/30/2023 23:03TO-15 Styrene µg/m3 0.124
J0.807 11/30/2023 23:03TO-15 Tetrachloroethene µg/m3 0.181
99.3 11/30/2023 23:03TO-15 Toluene µg/m3 0.090
311 11/30/2023 14:52TO-15 Trichlorofluoromethane µg/m3 2.60
8.67 11/30/2023 23:03TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
2.92 11/30/2023 23:03TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
15.1 11/30/2023 23:03TO-15 o-Xylene µg/m3 0.157
55.7 11/30/2023 23:03TO-15 m,p-Xylene µg/m3 0.217
70.8 11/30/2023 23:03TO-15 Xylene (Total)µg/m3 0.157
V 90167SSV-4
30.6 11/30/2023 23:55TO-15 Acetone µg/m3 0.202
10.8 11/30/2023 23:55TO-15 Benzene µg/m3 0.073
J1.09 11/30/2023 23:55TO-15 1,3-Butadiene µg/m3 0.328
JB0.582 11/30/2023 23:55TO-15 Carbon Disulfide µg/m3 0.060
6.37 11/30/2023 23:55TO-15 Cyclohexane µg/m3 0.161
2.86 11/30/2023 23:55TO-15 Dichlorodifluoromethane µg/m3 0.134
5.73 11/30/2023 23:55TO-15 Ethyl Acetate µg/m3 0.136
7.40 11/30/2023 23:55TO-15 Ethylbenzene µg/m3 0.106
J1.44 11/30/2023 23:55TO-15 4-Ethyltoluene µg/m3 0.128
J0.766 11/30/2023 23:55TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
9.97 11/30/2023 23:55TO-15 Heptane µg/m3 0.143
11.5 11/30/2023 23:55TO-15 n-Hexane µg/m3 0.047
9.43 11/30/2023 23:55TO-15 Isopropyl Alcohol µg/m3 0.139
3.81 11/30/2023 23:55TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J1.35 11/30/2023 23:55TO-15 4-Methyl-2-Pentanone µg/m3 0.121
B2.64 11/30/2023 23:55TO-15 Methylene Chloride µg/m3 0.488
4.47 11/30/2023 23:55TO-15 Propene µg/m3 0.242
J0.672 11/30/2023 23:55TO-15 Styrene µg/m3 0.124
J2.22 11/30/2023 23:55TO-15 Tetrachloroethene µg/m3 0.181
J0.787 11/30/2023 23:55TO-15 Tetrahydrofuran µg/m3 0.107
54.2 11/30/2023 23:55TO-15 Toluene µg/m3 0.090
J1.31 11/30/2023 23:55TO-15 1,1,1-Trichloroethane µg/m3 0.144
308 11/30/2023 15:29TO-15 Trichlorofluoromethane µg/m3 2.60
4.83 11/30/2023 23:55TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J1.59 11/30/2023 23:55TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
7.16 11/30/2023 23:55TO-15 o-Xylene µg/m3 0.157
Page 6 of 30
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-326-0001
Report Limit
Project:Former Winston Container
V 90167SSV-4
20.2 11/30/2023 23:55TO-15 m,p-Xylene µg/m3 0.217
27.4 11/30/2023 23:55TO-15 Xylene (Total)µg/m3 0.157
V 90168SSV-3
16.7 12/01/2023 00:45TO-15 Acetone µg/m3 0.202
13.4 12/01/2023 00:45TO-15 Benzene µg/m3 0.073
J0.920 12/01/2023 00:45TO-15 1,3-Butadiene µg/m3 0.328
JB0.423 12/01/2023 00:45TO-15 Carbon Disulfide µg/m3 0.060
5.76 12/01/2023 00:45TO-15 Cyclohexane µg/m3 0.161
J2.30 12/01/2023 00:45TO-15 Dichlorodifluoromethane µg/m3 0.134
4.37 12/01/2023 00:45TO-15 Ethyl Acetate µg/m3 0.136
10.3 12/01/2023 00:45TO-15 Ethylbenzene µg/m3 0.106
J2.08 12/01/2023 00:45TO-15 4-Ethyltoluene µg/m3 0.128
J0.636 12/01/2023 00:45TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
11.3 12/01/2023 00:45TO-15 Heptane µg/m3 0.143
8.24 12/01/2023 00:45TO-15 n-Hexane µg/m3 0.047
B6.47 12/01/2023 00:45TO-15 Isopropyl Alcohol µg/m3 0.139
2.79 12/01/2023 00:45TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J1.20 12/01/2023 00:45TO-15 4-Methyl-2-Pentanone µg/m3 0.121
B2.50 12/01/2023 00:45TO-15 Methylene Chloride µg/m3 0.488
2.73 12/01/2023 00:45TO-15 Propene µg/m3 0.242
J0.937 12/01/2023 00:45TO-15 Styrene µg/m3 0.124
J3.32 12/01/2023 00:45TO-15 Tetrachloroethene µg/m3 0.181
J0.406 12/01/2023 00:45TO-15 Tetrahydrofuran µg/m3 0.107
77.6 12/01/2023 00:45TO-15 Toluene µg/m3 0.090
J0.927 12/01/2023 00:45TO-15 1,1,1-Trichloroethane µg/m3 0.144
166 12/01/2023 00:45TO-15 Trichlorofluoromethane µg/m3 0.130
6.72 12/01/2023 00:45TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J2.30 12/01/2023 00:45TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
9.48 12/01/2023 00:45TO-15 o-Xylene µg/m3 0.157
29.9 12/01/2023 00:45TO-15 m,p-Xylene µg/m3 0.217
39.4 12/01/2023 00:45TO-15 Xylene (Total)µg/m3 0.157
Page 7 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-1
90164 Matrix:
11/21/2023 12:05
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
17.4 µg/m3 0.202 4.75Acetone 1 11/30/23 21:25 V40771ENM
10.4 µg/m3 0.073 1.60Benzene 1 11/30/23 21:25 V40771ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 11/30/23 21:25 V40771ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 11/30/23 21:25 V40771ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 11/30/23 21:25 V40771ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 11/30/23 21:25 V40771ENM
2.34 µg/m3 0.328 1.111,3-Butadiene 1 11/30/23 21:25 V40771ENM
0.442 JB µg/m3 0.060 6.23Carbon Disulfide 1 11/30/23 21:25 V40771ENM
<0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 11/30/23 21:25 V40771ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 11/30/23 21:25 V40771ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 11/30/23 21:25 V40771ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 11/30/23 21:25 V40771ENM
<0.086 µg/m3 0.086 2.44Chloroform 1 11/30/23 21:25 V40771ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 11/30/23 21:25 V40771ENM
7.64 µg/m3 0.161 3.44Cyclohexane 1 11/30/23 21:25 V40771ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 11/30/23 21:25 V40771ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 11/30/23 21:25 V40771ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 11/30/23 21:25 V40771ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 11/30/23 21:25 V40771ENM
2.77 µg/m3 0.134 2.47Dichlorodifluoromethane 1 11/30/23 21:25 V40771ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 11/30/23 21:25 V40771ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 11/30/23 21:25 V40771ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-1
90164 Matrix:
11/21/2023 12:05
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 11/30/23 21:25 V40771ENM
<0.095 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 11/30/23 21:25 V40771ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 11/30/23 21:25 V40771ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 11/30/23 21:25 V40771ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 11/30/23 21:25 V40771ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 11/30/23 21:25 V40771ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 11/30/23 21:25 V40771ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 11/30/23 21:25 V40771ENM
7.41 µg/m3 0.136 1.80Ethyl Acetate 1 11/30/23 21:25 V40771ENM
11.1 µg/m3 0.106 2.17Ethylbenzene 1 11/30/23 21:25 V40771ENM
2.85 µg/m3 0.128 2.464-Ethyltoluene 1 11/30/23 21:25 V40771ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 11/30/23 21:25 V40771ENM
9.79 µg/m3 0.143 2.05Heptane 1 11/30/23 21:25 V40771ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 11/30/23 21:25 V40771ENM
15.9 µg/m3 0.047 1.76n-Hexane 1 11/30/23 21:25 V40771ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 11/30/23 21:25 V40771ENM
8.86 µg/m3 0.139 4.92Isopropyl Alcohol 1 11/30/23 21:25 V40771ENM
3.41 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 11/30/23 21:25 V40771ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 11/30/23 21:25 V40771ENM
0.651 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 11/30/23 21:25 V40771ENM
1.40 JB µg/m3 0.488 1.74Methylene Chloride 1 11/30/23 21:25 V40771ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 11/30/23 21:25 V40771ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-1
90164 Matrix:
11/21/2023 12:05
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
13.9 µg/m3 0.242 0.860Propene 1 11/30/23 21:25 V40771ENM
0.787 J µg/m3 0.124 2.13Styrene 1 11/30/23 21:25 V40771ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 11/30/23 21:25 V40771ENM
1.06 J µg/m3 0.181 3.39 1 11/30/23 21:25 V40771ENM
1.38 J µg/m3 0.107 1.47 1 11/30/23 21:25 V40771ENM
53.4 µg/m3 0.090 1.88 1 11/30/23 21:25 V40771ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 11/30/23 21:25 V40771ENM
0.758 J µg/m3 0.144 2.731,1,1-Trichloroethane 1 11/30/23 21:25 V40771ENM
<0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 11/30/23 21:25 V40771ENM
<0.199 µg/m3 0.199 2.15 1 11/30/23 21:25 V40771ENM
415 µg/m3 2.60 56.2 20 11/30/23 13:39 V40771ENM
8.90 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 11/30/23 21:25 V40771ENM
2.64 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 11/30/23 21:25 V40771ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 11/30/23 21:25 V40771ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 11/30/23 21:25 V40771ENM
11.6 µg/m3 0.157 2.17o-Xylene 1 11/30/23 21:25 V40771ENM
30.6 µg/m3 0.217 5.65m,p-Xylene 1 11/30/23 21:25 V40771ENM
42.2 µg/m3 0.157 2.17Xylene (Total)1 11/30/23 21:25 V40771
Surrogate: 4-Bromofluorobenzene
Surrogate: 4-Bromofluorobenzene
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-2
90165 Matrix:
11/21/2023 12:51
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
14.0 µg/m3 0.202 4.75Acetone 1 11/30/23 22:14 V40771ENM
8.38 µg/m3 0.073 1.60Benzene 1 11/30/23 22:14 V40771ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 11/30/23 22:14 V40771ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 11/30/23 22:14 V40771ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 11/30/23 22:14 V40771ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 11/30/23 22:14 V40771ENM
1.63 µg/m3 0.328 1.111,3-Butadiene 1 11/30/23 22:14 V40771ENM
0.784 JB µg/m3 0.060 6.23Carbon Disulfide 1 11/30/23 22:14 V40771ENM
<0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 11/30/23 22:14 V40771ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 11/30/23 22:14 V40771ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 11/30/23 22:14 V40771ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 11/30/23 22:14 V40771ENM
<0.086 µg/m3 0.086 2.44Chloroform 1 11/30/23 22:14 V40771ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 11/30/23 22:14 V40771ENM
16.6 µg/m3 0.161 3.44Cyclohexane 1 11/30/23 22:14 V40771ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 11/30/23 22:14 V40771ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 11/30/23 22:14 V40771ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 11/30/23 22:14 V40771ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 11/30/23 22:14 V40771ENM
2.74 µg/m3 0.134 2.47Dichlorodifluoromethane 1 11/30/23 22:14 V40771ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 11/30/23 22:14 V40771ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 11/30/23 22:14 V40771ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-2
90165 Matrix:
11/21/2023 12:51
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 11/30/23 22:14 V40771ENM
<0.095 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 11/30/23 22:14 V40771ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 11/30/23 22:14 V40771ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 11/30/23 22:14 V40771ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 11/30/23 22:14 V40771ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 11/30/23 22:14 V40771ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 11/30/23 22:14 V40771ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 11/30/23 22:14 V40771ENM
24.0 µg/m3 0.136 1.80Ethyl Acetate 1 11/30/23 22:14 V40771ENM
5.15 µg/m3 0.106 2.17Ethylbenzene 1 11/30/23 22:14 V40771ENM
1.00 J µg/m3 0.128 2.464-Ethyltoluene 1 11/30/23 22:14 V40771ENM
0.666 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 11/30/23 22:14 V40771ENM
8.38 µg/m3 0.143 2.05Heptane 1 11/30/23 22:14 V40771ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 11/30/23 22:14 V40771ENM
56.2 µg/m3 0.047 1.76n-Hexane 1 11/30/23 22:14 V40771ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 11/30/23 22:14 V40771ENM
6.36 B µg/m3 0.139 4.92Isopropyl Alcohol 1 11/30/23 22:14 V40771ENM
7.11 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 11/30/23 22:14 V40771ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 11/30/23 22:14 V40771ENM
0.880 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 11/30/23 22:14 V40771ENM
1.89 B µg/m3 0.488 1.74Methylene Chloride 1 11/30/23 22:14 V40771ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 11/30/23 22:14 V40771ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-2
90165 Matrix:
11/21/2023 12:51
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
12.3 µg/m3 0.242 0.860Propene 1 11/30/23 22:14 V40771ENM
0.477 J µg/m3 0.124 2.13Styrene 1 11/30/23 22:14 V40771ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 11/30/23 22:14 V40771ENM
0.603 J µg/m3 0.181 3.39 1 11/30/23 22:14 V40771ENM
0.775 J µg/m3 0.107 1.47 1 11/30/23 22:14 V40771ENM
37.4 µg/m3 0.090 1.88 1 11/30/23 22:14 V40771ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 11/30/23 22:14 V40771ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 11/30/23 22:14 V40771ENM
<0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 11/30/23 22:14 V40771ENM
<0.199 µg/m3 0.199 2.15 1 11/30/23 22:14 V40771ENM
309 µg/m3 2.60 56.2 20 11/30/23 14:16 V40771ENM
3.87 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 11/30/23 22:14 V40771ENM
1.09 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 11/30/23 22:14 V40771ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 11/30/23 22:14 V40771ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 11/30/23 22:14 V40771ENM
5.05 µg/m3 0.157 2.17o-Xylene 1 11/30/23 22:14 V40771ENM
14.8 µg/m3 0.217 5.65m,p-Xylene 1 11/30/23 22:14 V40771ENM
19.9 µg/m3 0.157 2.17Xylene (Total)1 11/30/23 22:14 V40771
Surrogate: 4-Bromofluorobenzene
Surrogate: 4-Bromofluorobenzene
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:DUP-4
90166 Matrix:
11/21/2023 12:51
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
11.9 µg/m3 0.202 4.75Acetone 1 11/30/23 23:03 V40771ENM
17.5 µg/m3 0.073 1.60Benzene 1 11/30/23 23:03 V40771ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 11/30/23 23:03 V40771ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 11/30/23 23:03 V40771ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 11/30/23 23:03 V40771ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 11/30/23 23:03 V40771ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 11/30/23 23:03 V40771ENM
0.868 JB µg/m3 0.060 6.23Carbon Disulfide 1 11/30/23 23:03 V40771ENM
<0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 11/30/23 23:03 V40771ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 11/30/23 23:03 V40771ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 11/30/23 23:03 V40771ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 11/30/23 23:03 V40771ENM
<0.086 µg/m3 0.086 2.44Chloroform 1 11/30/23 23:03 V40771ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 11/30/23 23:03 V40771ENM
16.1 µg/m3 0.161 3.44Cyclohexane 1 11/30/23 23:03 V40771ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 11/30/23 23:03 V40771ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 11/30/23 23:03 V40771ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 11/30/23 23:03 V40771ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 11/30/23 23:03 V40771ENM
2.48 µg/m3 0.134 2.47Dichlorodifluoromethane 1 11/30/23 23:03 V40771ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 11/30/23 23:03 V40771ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 11/30/23 23:03 V40771ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:DUP-4
90166 Matrix:
11/21/2023 12:51
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 11/30/23 23:03 V40771ENM
<0.095 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 11/30/23 23:03 V40771ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 11/30/23 23:03 V40771ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 11/30/23 23:03 V40771ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 11/30/23 23:03 V40771ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 11/30/23 23:03 V40771ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 11/30/23 23:03 V40771ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 11/30/23 23:03 V40771ENM
23.9 µg/m3 0.136 1.80Ethyl Acetate 1 11/30/23 23:03 V40771ENM
18.7 µg/m3 0.106 2.17Ethylbenzene 1 11/30/23 23:03 V40771ENM
3.95 µg/m3 0.128 2.464-Ethyltoluene 1 11/30/23 23:03 V40771ENM
0.666 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 11/30/23 23:03 V40771ENM
19.4 µg/m3 0.143 2.05Heptane 1 11/30/23 23:03 V40771ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 11/30/23 23:03 V40771ENM
55.7 µg/m3 0.047 1.76n-Hexane 1 11/30/23 23:03 V40771ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 11/30/23 23:03 V40771ENM
4.51 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 11/30/23 23:03 V40771ENM
2.11 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 11/30/23 23:03 V40771ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 11/30/23 23:03 V40771ENM
0.892 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 11/30/23 23:03 V40771ENM
2.55 B µg/m3 0.488 1.74Methylene Chloride 1 11/30/23 23:03 V40771ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 11/30/23 23:03 V40771ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:DUP-4
90166 Matrix:
11/21/2023 12:51
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
10.5 µg/m3 0.242 0.860Propene 1 11/30/23 23:03 V40771ENM
1.51 J µg/m3 0.124 2.13Styrene 1 11/30/23 23:03 V40771ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 11/30/23 23:03 V40771ENM
0.807 J µg/m3 0.181 3.39 1 11/30/23 23:03 V40771ENM
<0.107 µg/m3 0.107 1.47 1 11/30/23 23:03 V40771ENM
99.3 µg/m3 0.090 1.88 1 11/30/23 23:03 V40771ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 11/30/23 23:03 V40771ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 11/30/23 23:03 V40771ENM
<0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 11/30/23 23:03 V40771ENM
<0.199 µg/m3 0.199 2.15 1 11/30/23 23:03 V40771ENM
311 µg/m3 2.60 56.2 20 11/30/23 14:52 V40771ENM
8.67 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 11/30/23 23:03 V40771ENM
2.92 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 11/30/23 23:03 V40771ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 11/30/23 23:03 V40771ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 11/30/23 23:03 V40771ENM
15.1 µg/m3 0.157 2.17o-Xylene 1 11/30/23 23:03 V40771ENM
55.7 µg/m3 0.217 5.65m,p-Xylene 1 11/30/23 23:03 V40771ENM
70.8 µg/m3 0.157 2.17Xylene (Total)1 11/30/23 23:03 V40771
Surrogate: 4-Bromofluorobenzene
Surrogate: 4-Bromofluorobenzene
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-4
90167 Matrix:
11/21/2023 12:24
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
30.6 µg/m3 0.202 4.75Acetone 1 11/30/23 23:55 V40771ENM
10.8 µg/m3 0.073 1.60Benzene 1 11/30/23 23:55 V40771ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 11/30/23 23:55 V40771ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 11/30/23 23:55 V40771ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 11/30/23 23:55 V40771ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 11/30/23 23:55 V40771ENM
1.09 J µg/m3 0.328 1.111,3-Butadiene 1 11/30/23 23:55 V40771ENM
0.582 JB µg/m3 0.060 6.23Carbon Disulfide 1 11/30/23 23:55 V40771ENM
<0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 11/30/23 23:55 V40771ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 11/30/23 23:55 V40771ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 11/30/23 23:55 V40771ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 11/30/23 23:55 V40771ENM
<0.086 µg/m3 0.086 2.44Chloroform 1 11/30/23 23:55 V40771ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 11/30/23 23:55 V40771ENM
6.37 µg/m3 0.161 3.44Cyclohexane 1 11/30/23 23:55 V40771ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 11/30/23 23:55 V40771ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 11/30/23 23:55 V40771ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 11/30/23 23:55 V40771ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 11/30/23 23:55 V40771ENM
2.86 µg/m3 0.134 2.47Dichlorodifluoromethane 1 11/30/23 23:55 V40771ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 11/30/23 23:55 V40771ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 11/30/23 23:55 V40771ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-4
90167 Matrix:
11/21/2023 12:24
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 11/30/23 23:55 V40771ENM
<0.095 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 11/30/23 23:55 V40771ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 11/30/23 23:55 V40771ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 11/30/23 23:55 V40771ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 11/30/23 23:55 V40771ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 11/30/23 23:55 V40771ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 11/30/23 23:55 V40771ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 11/30/23 23:55 V40771ENM
5.73 µg/m3 0.136 1.80Ethyl Acetate 1 11/30/23 23:55 V40771ENM
7.40 µg/m3 0.106 2.17Ethylbenzene 1 11/30/23 23:55 V40771ENM
1.44 J µg/m3 0.128 2.464-Ethyltoluene 1 11/30/23 23:55 V40771ENM
0.766 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 11/30/23 23:55 V40771ENM
9.97 µg/m3 0.143 2.05Heptane 1 11/30/23 23:55 V40771ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 11/30/23 23:55 V40771ENM
11.5 µg/m3 0.047 1.76n-Hexane 1 11/30/23 23:55 V40771ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 11/30/23 23:55 V40771ENM
9.43 µg/m3 0.139 4.92Isopropyl Alcohol 1 11/30/23 23:55 V40771ENM
3.81 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 11/30/23 23:55 V40771ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 11/30/23 23:55 V40771ENM
1.35 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 11/30/23 23:55 V40771ENM
2.64 B µg/m3 0.488 1.74Methylene Chloride 1 11/30/23 23:55 V40771ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 11/30/23 23:55 V40771ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-4
90167 Matrix:
11/21/2023 12:24
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
4.47 µg/m3 0.242 0.860Propene 1 11/30/23 23:55 V40771ENM
0.672 J µg/m3 0.124 2.13Styrene 1 11/30/23 23:55 V40771ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 11/30/23 23:55 V40771ENM
2.22 J µg/m3 0.181 3.39 1 11/30/23 23:55 V40771ENM
0.787 J µg/m3 0.107 1.47 1 11/30/23 23:55 V40771ENM
54.2 µg/m3 0.090 1.88 1 11/30/23 23:55 V40771ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 11/30/23 23:55 V40771ENM
1.31 J µg/m3 0.144 2.731,1,1-Trichloroethane 1 11/30/23 23:55 V40771ENM
<0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 11/30/23 23:55 V40771ENM
<0.199 µg/m3 0.199 2.15 1 11/30/23 23:55 V40771ENM
308 µg/m3 2.60 56.2 20 11/30/23 15:29 V40771ENM
4.83 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 11/30/23 23:55 V40771ENM
1.59 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 11/30/23 23:55 V40771ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 11/30/23 23:55 V40771ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 11/30/23 23:55 V40771ENM
7.16 µg/m3 0.157 2.17o-Xylene 1 11/30/23 23:55 V40771ENM
20.2 µg/m3 0.217 5.65m,p-Xylene 1 11/30/23 23:55 V40771ENM
27.4 µg/m3 0.157 2.17Xylene (Total)1 11/30/23 23:55 V40771
Surrogate: 4-Bromofluorobenzene
Surrogate: 4-Bromofluorobenzene
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-3
90168 Matrix:
11/21/2023 12:34
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
16.7 µg/m3 0.202 4.75Acetone 1 12/01/23 00:45 V40771ENM
13.4 µg/m3 0.073 1.60Benzene 1 12/01/23 00:45 V40771ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 12/01/23 00:45 V40771ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 12/01/23 00:45 V40771ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 12/01/23 00:45 V40771ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 12/01/23 00:45 V40771ENM
0.920 J µg/m3 0.328 1.111,3-Butadiene 1 12/01/23 00:45 V40771ENM
0.423 JB µg/m3 0.060 6.23Carbon Disulfide 1 12/01/23 00:45 V40771ENM
<0.155 µg/m3 0.155 3.15Carbon Tetrachloride 1 12/01/23 00:45 V40771ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 12/01/23 00:45 V40771ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 12/01/23 00:45 V40771ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 12/01/23 00:45 V40771ENM
<0.086 µg/m3 0.086 2.44Chloroform 1 12/01/23 00:45 V40771ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 12/01/23 00:45 V40771ENM
5.76 µg/m3 0.161 3.44Cyclohexane 1 12/01/23 00:45 V40771ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 12/01/23 00:45 V40771ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 12/01/23 00:45 V40771ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 12/01/23 00:45 V40771ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 12/01/23 00:45 V40771ENM
2.30 J µg/m3 0.134 2.47Dichlorodifluoromethane 1 12/01/23 00:45 V40771ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 12/01/23 00:45 V40771ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 12/01/23 00:45 V40771ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-3
90168 Matrix:
11/21/2023 12:34
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 12/01/23 00:45 V40771ENM
<0.095 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 12/01/23 00:45 V40771ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 12/01/23 00:45 V40771ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 12/01/23 00:45 V40771ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 12/01/23 00:45 V40771ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 12/01/23 00:45 V40771ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 12/01/23 00:45 V40771ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 12/01/23 00:45 V40771ENM
4.37 µg/m3 0.136 1.80Ethyl Acetate 1 12/01/23 00:45 V40771ENM
10.3 µg/m3 0.106 2.17Ethylbenzene 1 12/01/23 00:45 V40771ENM
2.08 J µg/m3 0.128 2.464-Ethyltoluene 1 12/01/23 00:45 V40771ENM
0.636 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 12/01/23 00:45 V40771ENM
11.3 µg/m3 0.143 2.05Heptane 1 12/01/23 00:45 V40771ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 12/01/23 00:45 V40771ENM
8.24 µg/m3 0.047 1.76n-Hexane 1 12/01/23 00:45 V40771ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 12/01/23 00:45 V40771ENM
6.47 B µg/m3 0.139 4.92Isopropyl Alcohol 1 12/01/23 00:45 V40771ENM
2.79 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 12/01/23 00:45 V40771ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 12/01/23 00:45 V40771ENM
1.20 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 12/01/23 00:45 V40771ENM
2.50 B µg/m3 0.488 1.74Methylene Chloride 1 12/01/23 00:45 V40771ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 12/01/23 00:45 V40771ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 30
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
23-326-0001
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Charlotte
Received : 11/21/2023
Former Winston Container
Report Date : 12/01/2023
Sample ID :
Lab No :
Sampled:SSV-3
90168 Matrix:
11/21/2023 12:34
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):11/30/23 09:00
2.73 µg/m3 0.242 0.860Propene 1 12/01/23 00:45 V40771ENM
0.937 J µg/m3 0.124 2.13Styrene 1 12/01/23 00:45 V40771ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 12/01/23 00:45 V40771ENM
3.32 J µg/m3 0.181 3.39 1 12/01/23 00:45 V40771ENM
0.406 J µg/m3 0.107 1.47 1 12/01/23 00:45 V40771ENM
77.6 µg/m3 0.090 1.88 1 12/01/23 00:45 V40771ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 12/01/23 00:45 V40771ENM
0.927 J µg/m3 0.144 2.731,1,1-Trichloroethane 1 12/01/23 00:45 V40771ENM
<0.087 µg/m3 0.087 2.731,1,2-Trichloroethane 1 12/01/23 00:45 V40771ENM
<0.199 µg/m3 0.199 2.15 1 12/01/23 00:45 V40771ENM
166 µg/m3 0.130 2.81 1 12/01/23 00:45 V40771ENM
6.72 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 12/01/23 00:45 V40771ENM
2.30 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 12/01/23 00:45 V40771ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 12/01/23 00:45 V40771ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 12/01/23 00:45 V40771ENM
9.48 µg/m3 0.157 2.17o-Xylene 1 12/01/23 00:45 V40771ENM
29.9 µg/m3 0.217 5.65m,p-Xylene 1 12/01/23 00:45 V40771ENM
39.4 µg/m3 0.157 2.17Xylene (Total)1 12/01/23 00:45 V40771
Surrogate: 4-Bromofluorobenzene
Surrogate: 4-Bromofluorobenzene
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 30
Quality Control Data
23-326-0001Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
V40771QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V40763
Associated Lab Samples: 90164, 90165, 90166, 90167, 90168
LRB-V40763 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/30/23 10:514.750.2020.429µg/m3Acetone
11/30/23 10:511.600.0730.533µg/m3Benzene
11/30/23 10:5110.40.147<0.147µg/m3Benzyl Chloride
11/30/23 10:513.350.150<0.150µg/m3Bromodichloromethane
11/30/23 10:515.170.153<0.153µg/m3Bromoform
11/30/23 10:511.940.115<0.115µg/m3Bromomethane
11/30/23 10:511.110.328<0.328µg/m31,3-Butadiene
11/30/23 10:516.230.0600.706µg/m3Carbon Disulfide
11/30/23 10:513.150.155<0.155µg/m3Carbon Tetrachloride
11/30/23 10:512.300.107<0.107µg/m3Chlorobenzene
11/30/23 10:514.260.208<0.208µg/m3Chlorodibromomethane
11/30/23 10:511.320.164<0.164µg/m3Chloroethane
11/30/23 10:512.440.086<0.086µg/m3Chloroform
11/30/23 10:511.030.067<0.067µg/m3Chloromethane
11/30/23 10:513.440.161<0.161µg/m3Cyclohexane
11/30/23 10:513.840.151<0.151µg/m31,2-Dibromoethane
11/30/23 10:513.010.096<0.096µg/m31,2-Dichlorobenzene
11/30/23 10:5112.00.174<0.174µg/m31,3-Dichlorobenzene
11/30/23 10:513.010.186<0.186µg/m31,4-Dichlorobenzene
11/30/23 10:512.470.134<0.134µg/m3Dichlorodifluoromethane
11/30/23 10:512.020.101<0.101µg/m31,1-Dichloroethane
11/30/23 10:512.020.129<0.129µg/m31,2-Dichloroethane
11/30/23 10:511.980.107<0.107µg/m31,1-Dichloroethene
11/30/23 10:511.980.095<0.095µg/m3cis-1,2-Dichloroethene
11/30/23 10:511.980.108<0.108µg/m3trans-1,2-Dichloroethene
11/30/23 10:512.310.205<0.205µg/m31,2-Dichloropropane
11/30/23 10:513.500.622<0.622µg/m31,2-Dichlorotetrafluoroethane
Page 1 of 5Date:12/01/2023 03:30 PM
Page 23 of 30
Quality Control Data
23-326-0001Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
V40771QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V40763
Associated Lab Samples: 90164, 90165, 90166, 90167, 90168
LRB-V40763 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/30/23 10:512.270.178<0.178µg/m3cis-1,3-Dichloropropene
11/30/23 10:512.270.178<0.178µg/m3trans-1,3-Dichloropropene
11/30/23 10:511.800.435<0.435µg/m31,4-Dioxane
11/30/23 10:511.800.136<0.136µg/m3Ethyl Acetate
11/30/23 10:512.170.106<0.106µg/m3Ethylbenzene
11/30/23 10:512.460.128<0.128µg/m34-Ethyltoluene
11/30/23 10:513.830.561<0.561µg/m31,1,2-Trichloro-1,2,2-trifluoroethane
11/30/23 10:512.050.143<0.143µg/m3Heptane
11/30/23 10:515.330.330<0.330µg/m3Hexachlorobutadiene
11/30/23 10:511.760.047<0.047µg/m3n-Hexane
11/30/23 10:512.050.285<0.285µg/m32-Hexanone
11/30/23 10:514.920.1390.690µg/m3Isopropyl Alcohol
11/30/23 10:511.470.224<0.224µg/m3Methyl Ethyl Ketone (MEK)
11/30/23 10:511.800.033<0.033µg/m3Methyl tert-butyl ether (MTBE)
11/30/23 10:512.050.121<0.121µg/m34-Methyl-2-Pentanone
11/30/23 10:511.740.4880.819µg/m3Methylene Chloride
11/30/23 10:512.620.183<0.183µg/m3Naphthalene
11/30/23 10:510.8600.242<0.242µg/m3Propene
11/30/23 10:512.130.124<0.124µg/m3Styrene
11/30/23 10:513.430.104<0.104µg/m31,1,2,2-Tetrachloroethane
11/30/23 10:513.390.181<0.181µg/m3
11/30/23 10:511.470.107<0.107µg/m3
11/30/23 10:511.880.0900.896µg/m3
11/30/23 10:513.710.209<0.209µg/m31,2,4-Trichlorobenzene
11/30/23 10:512.730.144<0.144µg/m31,1,1-Trichloroethane
11/30/23 10:512.730.087<0.087µg/m31,1,2-Trichloroethane
11/30/23 10:512.150.199<0.199µg/m3
Page 2 of 5Date:12/01/2023 03:30 PM
Page 24 of 30
Quality Control Data
23-326-0001Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
V40771QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V40763
Associated Lab Samples: 90164, 90165, 90166, 90167, 90168
LRB-V40763 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/30/23 10:512.810.130<0.130µg/m3
11/30/23 10:512.460.110<0.110µg/m31,2,4-Trimethylbenzene
11/30/23 10:512.460.236<0.236µg/m31,3,5-Trimethylbenzene
11/30/23 10:511.760.224<0.224µg/m3Vinyl Acetate
11/30/23 10:511.280.127<0.127µg/m3Vinyl Chloride
11/30/23 10:512.170.157<0.157µg/m3o-Xylene
11/30/23 10:515.650.217<0.217µg/m3m,p-Xylene
11/30/23 10:514-Bromofluorobenzene (S)95.5 70-130
LCS-V40763Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
11313.511.9µg/m3Acetone 70-130
92.514.816.0µg/m3Benzene 70-130
10226.425.9µg/m3Benzyl Chloride 70-130
93.131.233.5µg/m3Bromodichloromethane 70-130
10051.751.7µg/m3Bromoform 70-130
12123.519.4µg/m3Bromomethane 70-130
11412.711.1µg/m31,3-Butadiene 70-130
12219.115.6µg/m3Carbon Disulfide 70-130
92.629.231.5µg/m3Carbon Tetrachloride 70-130
10323.823.0µg/m3Chlorobenzene 70-130
10142.942.6µg/m3Chlorodibromomethane 70-130
11515.213.2µg/m3Chloroethane 70-130
10225.024.4µg/m3Chloroform 70-130
97.010.010.3µg/m3Chloromethane 70-130
84.814.617.2µg/m3Cyclohexane 70-130
Page 3 of 5Date:12/01/2023 03:30 PM
Page 25 of 30
Quality Control Data
23-326-0001Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
V40771QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V40763
LCS-V40763Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10439.838.4µg/m31,2-Dibromoethane 70-130
10932.930.1µg/m31,2-Dichlorobenzene 70-130
11233.630.1µg/m31,3-Dichlorobenzene 70-130
11233.830.1µg/m31,4-Dichlorobenzene 70-130
11127.524.7µg/m3Dichlorodifluoromethane 70-130
12024.220.2µg/m31,1-Dichloroethane 70-130
93.518.920.2µg/m31,2-Dichloroethane 70-130
12224.119.8µg/m31,1-Dichloroethene 70-130
12123.919.8µg/m3cis-1,2-Dichloroethene 70-130
12124.019.8µg/m3trans-1,2-Dichloroethene 70-130
83.919.423.1µg/m31,2-Dichloropropane 70-130
11339.435.0µg/m31,2-Dichlorotetrafluoroethane 70-130
10323.422.7µg/m3cis-1,3-Dichloropropene 70-130
10323.322.7µg/m3trans-1,3-Dichloropropene 70-130
87.715.818.0µg/m31,4-Dioxane 70-130
11420.618.0µg/m3Ethyl Acetate 70-130
10122.021.7µg/m3Ethylbenzene 70-130
10726.224.6µg/m34-Ethyltoluene 70-130
12347.138.3µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 70-130
10221.020.5µg/m3Heptane 70-130
10254.153.3µg/m3Hexachlorobutadiene 70-130
11820.817.6µg/m3n-Hexane 70-130
99.520.420.5µg/m32-Hexanone 70-130
11714.412.3µg/m3Isopropyl Alcohol 70-130
11517.014.8µg/m3Methyl Ethyl Ketone (MEK)70-130
11721.118.0µg/m3Methyl tert-butyl ether (MTBE)70-130
10120.820.5µg/m34-Methyl-2-Pentanone 70-130
Page 4 of 5Date:12/01/2023 03:30 PM
Page 26 of 30
Quality Control Data
23-326-0001Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
V40771QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V40763
LCS-V40763Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
11119.317.4µg/m3Methylene Chloride 70-130
10828.426.2µg/m3Naphthalene 70-130
99.18.548.61µg/m3Propene 70-130
99.521.221.3µg/m3Styrene 70-130
10234.934.3µg/m31,1,2,2-Tetrachloroethane 70-130
10435.433.9µg/m3 70-130
97.914.414.7µg/m3 70-130
10319.418.8µg/m3 70-130
10940.537.1µg/m31,2,4-Trichlorobenzene 70-130
96.726.427.3µg/m31,1,1-Trichloroethane 70-130
10328.227.3µg/m31,1,2-Trichloroethane 70-130
10127.226.9µg/m3 70-130
12334.628.1µg/m3 70-130
11127.324.6µg/m31,2,4-Trimethylbenzene 70-130
10926.724.6µg/m31,3,5-Trimethylbenzene 70-130
11620.417.6µg/m3Vinyl Acetate 70-130
11815.112.8µg/m3Vinyl Chloride 70-130
10222.221.7µg/m3o-Xylene 70-130
10244.443.4µg/m3m,p-Xylene 70-130
1014-Bromofluorobenzene (S)70-130
Page 5 of 5Date:12/01/2023 03:30 PM
Page 27 of 30
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-326-0001
Mid-Atlantic Associates, Inc. - Charlotte
01138
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:N/A
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:11/22/2023 10:08:51
Special precautions or instructions included?
Comments:
Page 28 of 30
Page 29 of 30
Page 30 of 30

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

2/16/2024
Mid-Atlantic Associates, Inc. - Charlotte Shane Sisco
1125 E. Morehead Street, Suite 104 Charlotte, NC, 28204
Ref: Analytical Testing
Lab Report Number: 24-039-0035 Client Project Description: Former Winston Container
Dear Shane Sisco:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 2/8/2024 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 38
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2024402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/24-039-0035
Page 2 of 38
Report Number:
Sample Summary Table
Client Project Description:
24-039-0035
Former Winston Container
Lab No Client Sample ID Matrix Date Collected Date Received
02/07/2024 13:40Aqueous 96217 MW-1 02/08/2024 14:29
02/07/2024 14:00Aqueous 96218 MW-2 02/08/2024 14:29
Page 3 of 38
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-039-0035
Report Limit
Project:Former Winston Container
V 96217MW-1
0.129 02/09/2024 21:516010DBariummg/L 0.003
J0.003 02/09/2024 21:516010DChromiummg/L 0.002
J0.003 02/09/2024 21:516010DLeadmg/L 0.003
J0.855 02/10/2024 07:138260DMethyl Ethyl Ketone (MEK)µg/L 0.710
J6.56 02/14/2024 13:148270EBenzoic Acid µg/L 1.10
6.82 02/14/2024 13:148270EDibenz(a,h)anthracene µg/L 0.434
J4.70 02/14/2024 13:148270EDi-n-Octyl Phthalate µg/L 1.65
6.70 02/14/2024 13:148270EIndeno(1,2,3-cd)pyrene µg/L 0.477
5.07 02/14/2024 13:148270EPentachlorophenolµg/L 1.43
V 96218MW-2
0.145 02/09/2024 21:566010DBariummg/L 0.003
J0.004 02/09/2024 21:566010DChromiummg/L 0.002
1.19 02/10/2024 07:378260DChloroformµg/L 0.220
6.64 02/10/2024 07:378260Dcis-1,2-Dichloroethene µg/L 0.200
J0.835 02/10/2024 07:378260DMethyl Ethyl Ketone (MEK)µg/L 0.710
24.3 02/10/2024 07:378260DTetrachloroetheneµg/L 0.220
3.10 02/10/2024 07:378260DTrichloroetheneµg/L 0.180
Page 4 of 38

Client: Mid-Atlantic Associates, Inc. - Charlotte CASE NARRATIVE
Project: Former Winston Container Lab Report Number: 24-039-0035
Date: 2/16/2024
Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: Pyridine QC Batch No: V43550/V43522
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: Pyridine QC Batch No: V43550/V43522
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 5 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-1
96217 Matrix:
2/7/2024 13:40
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.004 mg/L 0.004 0.010Arsenic 1 02/09/24 21:51 6010DJKC
0.129 mg/L 0.003 0.010Barium 1 02/09/24 21:51 6010DJKC
<0.0005 mg/L 0.0005 0.0020Cadmium 1 02/09/24 21:51 6010DJKC
0.003 J mg/L 0.002 0.005Chromium 1 02/09/24 21:51 6010DJKC
0.003 J mg/L 0.003 0.006Lead 1 02/09/24 21:51 6010DJKC
<0.00007 mg/L 0.00007 0.00020Mercury (Total)1 02/15/24 18:17 7470AJKC
<0.007 mg/L 0.007 0.020Selenium 1 02/09/24 21:51 6010DJKC
<0.0007 mg/L 0.0007 0.0050Silver 1 02/09/24 21:51 6010DJKC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 6 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-1
96217 Matrix:
2/7/2024 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43450 02/09/24 14:00
<1.80 µg/L 1.80 5.00Acetone 1 02/10/24 07:13 V43451MSA
<2.00 µg/L 2.00 5.00Acrolein 1 02/10/24 07:13 V43451MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 02/10/24 07:13 V43451MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/10/24 07:13 V43451MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/10/24 07:13 V43451MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/10/24 07:13 V43451MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/10/24 07:13 V43451MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/10/24 07:13 V43451MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/10/24 07:13 V43451MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 02/10/24 07:13 V43451MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/10/24 07:13 V43451MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/10/24 07:13 V43451MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 02/10/24 07:13 V43451MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/10/24 07:13 V43451MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/10/24 07:13 V43451MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/10/24 07:13 V43451MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/10/24 07:13 V43451MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/10/24 07:13 V43451MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 02/10/24 07:13 V43451MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/10/24 07:13 V43451MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/10/24 07:13 V43451MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 02/10/24 07:13 V43451MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 7 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-1
96217 Matrix:
2/7/2024 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43450 02/09/24 14:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/10/24 07:13 V43451MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/10/24 07:13 V43451MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/10/24 07:13 V43451MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/10/24 07:13 V43451MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/10/24 07:13 V43451MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/10/24 07:13 V43451MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/10/24 07:13 V43451MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/10/24 07:13 V43451MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/10/24 07:13 V43451MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/10/24 07:13 V43451MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/10/24 07:13 V43451MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/10/24 07:13 V43451MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/10/24 07:13 V43451MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/10/24 07:13 V43451MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/10/24 07:13 V43451MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/10/24 07:13 V43451MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/10/24 07:13 V43451MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/10/24 07:13 V43451MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/10/24 07:13 V43451MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 02/10/24 07:13 V43451MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 02/10/24 07:13 V43451MSA
<1.30 µg/L 1.30 10.0n-Hexane 1 02/10/24 07:13 V43451MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 8 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-1
96217 Matrix:
2/7/2024 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43450 02/09/24 14:00
<0.380 µg/L 0.380 5.002-Hexanone 1 02/10/24 07:13 V43451MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 02/10/24 07:13 V43451MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/10/24 07:13 V43451MSA
0.855 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/10/24 07:13 V43451MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 02/10/24 07:13 V43451MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 02/10/24 07:13 V43451MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 02/10/24 07:13 V43451MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/10/24 07:13 V43451MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/10/24 07:13 V43451MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/10/24 07:13 V43451MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/10/24 07:13 V43451MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/10/24 07:13 V43451MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/10/24 07:13 V43451MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/10/24 07:13 V43451MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 02/10/24 07:13 V43451MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 02/10/24 07:13 V43451MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/10/24 07:13 V43451MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/10/24 07:13 V43451MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/10/24 07:13 V43451MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/10/24 07:13 V43451MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 02/10/24 07:13 V43451MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/10/24 07:13 V43451MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 9 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-1
96217 Matrix:
2/7/2024 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43450 02/09/24 14:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 02/10/24 07:13 V43451MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/10/24 07:13 V43451MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 02/10/24 07:13 V43451MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/10/24 07:13 V43451MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/10/24 07:13 V43451
Surrogate: 4-Bromofluorobenzene 103 Limits: 80-124%02/10/24 07:131 MSA V43451
Surrogate: Dibromofluoromethane 97.0 Limits: 75-129%02/10/24 07:131 MSA V43451
Surrogate: 1,2-Dichloroethane - d4 97.6 Limits: 63-136%02/10/24 07:131 MSA V43451
Surrogate: Toluene-d8 101 Limits: 77-123%02/10/24 07:131 MSA V43451
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43522 02/13/24 11:24
<0.302 µg/L 0.302 2.00Acenaphthene 1 02/14/24 13:14 V43550AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 02/14/24 13:14 V43550AMP
<2.05 µg/L 2.05 5.00Aniline 1 02/14/24 13:14 V43550AMP
<0.836 µg/L 0.836 2.00Anthracene 1 02/14/24 13:14 V43550AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 02/14/24 13:14 V43550AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 02/14/24 13:14 V43550AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 02/14/24 13:14 V43550AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 02/14/24 13:14 V43550AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 02/14/24 13:14 V43550AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 10 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-1
96217 Matrix:
2/7/2024 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43522 02/13/24 11:24
6.56 J µg/L 1.10 10.0Benzoic Acid 1 02/14/24 13:14 V43550AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 02/14/24 13:14 V43550AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 02/14/24 13:14 V43550AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 02/14/24 13:14 V43550AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 02/14/24 13:14 V43550AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 02/14/24 13:14 V43550AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 02/14/24 13:14 V43550AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 02/14/24 13:14 V43550AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 02/14/24 13:14 V43550AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 02/14/24 13:14 V43550AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 02/14/24 13:14 V43550AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 02/14/24 13:14 V43550AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 02/14/24 13:14 V43550AMP
<0.405 µg/L 0.405 2.00Chrysene 1 02/14/24 13:14 V43550AMP
6.82 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 02/14/24 13:14 V43550AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 02/14/24 13:14 V43550AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 02/14/24 13:14 V43550AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 02/14/24 13:14 V43550AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 02/14/24 13:14 V43550AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 02/14/24 13:14 V43550AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 02/14/24 13:14 V43550AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 02/14/24 13:14 V43550AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 11 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-1
96217 Matrix:
2/7/2024 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43522 02/13/24 11:24
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 02/14/24 13:14 V43550AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 02/14/24 13:14 V43550AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 02/14/24 13:14 V43550AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 02/14/24 13:14 V43550AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 02/14/24 13:14 V43550AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 02/14/24 13:14 V43550AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 02/14/24 13:14 V43550AMP
4.70 J µg/L 1.65 5.00Di-n-Octyl Phthalate 1 02/14/24 13:14 V43550AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 02/14/24 13:14 V43550AMP
<0.807 µg/L 0.807 2.00Fluorene 1 02/14/24 13:14 V43550AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 02/14/24 13:14 V43550AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 02/14/24 13:14 V43550AMP
<2.05 µg/L 2.05 5.00SPLP Hexachlorocyclopentadiene 1 02/14/24 13:14 V43550AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 02/14/24 13:14 V43550AMP
6.70 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 02/14/24 13:14 V43550AMP
<0.444 µg/L 0.444 5.00Isophorone 1 02/14/24 13:14 V43550AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 02/14/24 13:14 V43550AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 02/14/24 13:14 V43550AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 02/14/24 13:14 V43550AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 02/14/24 13:14 V43550AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 02/14/24 13:14 V43550AMP
<1.39 µg/L 1.39 5.002-Nitroaniline 1 02/14/24 13:14 V43550AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 12 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-1
96217 Matrix:
2/7/2024 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43522 02/13/24 11:24
<1.39 µg/L 1.39 5.003-Nitroaniline 1 02/14/24 13:14 V43550AMP
<1.53 µg/L 1.53 5.004-Nitroaniline 1 02/14/24 13:14 V43550AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 02/14/24 13:14 V43550AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 02/14/24 13:14 V43550AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 02/14/24 13:14 V43550AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 02/14/24 13:14 V43550AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 02/14/24 13:14 V43550AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 02/14/24 13:14 V43550AMP
5.07 µg/L 1.43 5.00Pentachlorophenol 1 02/14/24 13:14 V43550AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 02/14/24 13:14 V43550AMP
<0.651 µg/L 0.651 5.00Phenol 1 02/14/24 13:14 V43550AMP
<0.434 µg/L 0.434 2.00Pyrene 1 02/14/24 13:14 V43550AMP
<1.20 M µg/L 1.20 5.00Pyridine 1 02/14/24 13:14 V43550AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 02/14/24 13:14 V43550AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 02/14/24 13:14 V43550AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 02/14/24 13:14 V43550AMP
8270ESurrogate: Phenol-d5 29.2 Limits: 11-100%02/14/24 13:141 AMP
Surrogate: 2-Fluorobiphenyl 62.6 Limits: 44-119%02/14/24 13:141 AMP V43550
Surrogate: 2-Fluorophenol 41.5 Limits: 19-119%02/14/24 13:141 AMP V43550
Surrogate: Nitrobenzene-d5 64.2 Limits: 44-120%02/14/24 13:141 AMP V43550
Surrogate: 4-Terphenyl-d14 76.8 Limits: 50-134%02/14/24 13:141 AMP V43550
Surrogate: 2,4,6-Tribromophenol 79.0 Limits: 43-140%02/14/24 13:141 AMP V43550
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 13 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-2
96218 Matrix:
2/7/2024 14:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.004 mg/L 0.004 0.010Arsenic 1 02/09/24 21:56 6010DJKC
0.145 mg/L 0.003 0.010Barium 1 02/09/24 21:56 6010DJKC
<0.0005 mg/L 0.0005 0.0020Cadmium 1 02/09/24 21:56 6010DJKC
0.004 J mg/L 0.002 0.005Chromium 1 02/09/24 21:56 6010DJKC
<0.003 mg/L 0.003 0.006Lead 1 02/09/24 21:56 6010DJKC
<0.00007 mg/L 0.00007 0.00020Mercury (Total)1 02/15/24 18:33 7470AJKC
<0.007 mg/L 0.007 0.020Selenium 1 02/09/24 21:56 6010DJKC
<0.0007 mg/L 0.0007 0.0050Silver 1 02/09/24 21:56 6010DJKC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 14 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-2
96218 Matrix:
2/7/2024 14:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43450 02/09/24 14:00
<1.80 µg/L 1.80 5.00Acetone 1 02/10/24 07:37 V43451MSA
<2.00 µg/L 2.00 5.00Acrolein 1 02/10/24 07:37 V43451MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 02/10/24 07:37 V43451MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/10/24 07:37 V43451MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/10/24 07:37 V43451MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/10/24 07:37 V43451MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/10/24 07:37 V43451MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/10/24 07:37 V43451MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/10/24 07:37 V43451MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 02/10/24 07:37 V43451MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/10/24 07:37 V43451MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/10/24 07:37 V43451MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 02/10/24 07:37 V43451MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/10/24 07:37 V43451MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/10/24 07:37 V43451MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/10/24 07:37 V43451MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/10/24 07:37 V43451MSA
1.19 µg/L 0.220 0.500Chloroform 1 02/10/24 07:37 V43451MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 02/10/24 07:37 V43451MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/10/24 07:37 V43451MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/10/24 07:37 V43451MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 02/10/24 07:37 V43451MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 15 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-2
96218 Matrix:
2/7/2024 14:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43450 02/09/24 14:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/10/24 07:37 V43451MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/10/24 07:37 V43451MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/10/24 07:37 V43451MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/10/24 07:37 V43451MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/10/24 07:37 V43451MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/10/24 07:37 V43451MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/10/24 07:37 V43451MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/10/24 07:37 V43451MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/10/24 07:37 V43451MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/10/24 07:37 V43451MSA
6.64 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/10/24 07:37 V43451MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/10/24 07:37 V43451MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/10/24 07:37 V43451MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/10/24 07:37 V43451MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/10/24 07:37 V43451MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/10/24 07:37 V43451MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/10/24 07:37 V43451MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/10/24 07:37 V43451MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/10/24 07:37 V43451MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 02/10/24 07:37 V43451MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 02/10/24 07:37 V43451MSA
<1.30 µg/L 1.30 10.0n-Hexane 1 02/10/24 07:37 V43451MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 16 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-2
96218 Matrix:
2/7/2024 14:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43450 02/09/24 14:00
<0.380 µg/L 0.380 5.002-Hexanone 1 02/10/24 07:37 V43451MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 02/10/24 07:37 V43451MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/10/24 07:37 V43451MSA
0.835 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/10/24 07:37 V43451MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 02/10/24 07:37 V43451MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 02/10/24 07:37 V43451MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 02/10/24 07:37 V43451MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/10/24 07:37 V43451MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/10/24 07:37 V43451MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/10/24 07:37 V43451MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/10/24 07:37 V43451MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/10/24 07:37 V43451MSA
24.3 µg/L 0.220 0.500Tetrachloroethene 1 02/10/24 07:37 V43451MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/10/24 07:37 V43451MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 02/10/24 07:37 V43451MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 02/10/24 07:37 V43451MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/10/24 07:37 V43451MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/10/24 07:37 V43451MSA
3.10 µg/L 0.180 0.500Trichloroethene 1 02/10/24 07:37 V43451MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/10/24 07:37 V43451MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 02/10/24 07:37 V43451MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/10/24 07:37 V43451MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 17 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-2
96218 Matrix:
2/7/2024 14:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43450 02/09/24 14:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 02/10/24 07:37 V43451MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/10/24 07:37 V43451MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 02/10/24 07:37 V43451MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/10/24 07:37 V43451MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/10/24 07:37 V43451
Surrogate: 4-Bromofluorobenzene 102 Limits: 80-124%02/10/24 07:371 MSA V43451
Surrogate: Dibromofluoromethane 96.2 Limits: 75-129%02/10/24 07:371 MSA V43451
Surrogate: 1,2-Dichloroethane - d4 95.0 Limits: 63-136%02/10/24 07:371 MSA V43451
Surrogate: Toluene-d8 99.6 Limits: 77-123%02/10/24 07:371 MSA V43451
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43522 02/13/24 11:24
<0.302 µg/L 0.302 2.00Acenaphthene 1 02/14/24 13:38 V43550AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 02/14/24 13:38 V43550AMP
<2.05 µg/L 2.05 5.00Aniline 1 02/14/24 13:38 V43550AMP
<0.836 µg/L 0.836 2.00Anthracene 1 02/14/24 13:38 V43550AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 02/14/24 13:38 V43550AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 02/14/24 13:38 V43550AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 02/14/24 13:38 V43550AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 02/14/24 13:38 V43550AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 02/14/24 13:38 V43550AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 18 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-2
96218 Matrix:
2/7/2024 14:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43522 02/13/24 11:24
<1.10 µg/L 1.10 10.0Benzoic Acid 1 02/14/24 13:38 V43550AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 02/14/24 13:38 V43550AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 02/14/24 13:38 V43550AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 02/14/24 13:38 V43550AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 02/14/24 13:38 V43550AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 02/14/24 13:38 V43550AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 02/14/24 13:38 V43550AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 02/14/24 13:38 V43550AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 02/14/24 13:38 V43550AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 02/14/24 13:38 V43550AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 02/14/24 13:38 V43550AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 02/14/24 13:38 V43550AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 02/14/24 13:38 V43550AMP
<0.405 µg/L 0.405 2.00Chrysene 1 02/14/24 13:38 V43550AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 02/14/24 13:38 V43550AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 02/14/24 13:38 V43550AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 02/14/24 13:38 V43550AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 02/14/24 13:38 V43550AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 02/14/24 13:38 V43550AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 02/14/24 13:38 V43550AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 02/14/24 13:38 V43550AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 02/14/24 13:38 V43550AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 19 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-2
96218 Matrix:
2/7/2024 14:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43522 02/13/24 11:24
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 02/14/24 13:38 V43550AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 02/14/24 13:38 V43550AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 02/14/24 13:38 V43550AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 02/14/24 13:38 V43550AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 02/14/24 13:38 V43550AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 02/14/24 13:38 V43550AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 02/14/24 13:38 V43550AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 02/14/24 13:38 V43550AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 02/14/24 13:38 V43550AMP
<0.807 µg/L 0.807 2.00Fluorene 1 02/14/24 13:38 V43550AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 02/14/24 13:38 V43550AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 02/14/24 13:38 V43550AMP
<2.05 µg/L 2.05 5.00SPLP Hexachlorocyclopentadiene 1 02/14/24 13:38 V43550AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 02/14/24 13:38 V43550AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 02/14/24 13:38 V43550AMP
<0.444 µg/L 0.444 5.00Isophorone 1 02/14/24 13:38 V43550AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 02/14/24 13:38 V43550AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 02/14/24 13:38 V43550AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 02/14/24 13:38 V43550AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 02/14/24 13:38 V43550AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 02/14/24 13:38 V43550AMP
<1.39 µg/L 1.39 5.002-Nitroaniline 1 02/14/24 13:38 V43550AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 20 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-039-0035
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 02/08/2024
Former Winston Container
Report Date : 02/16/2024
Sample ID :
Lab No :
Sampled:MW-2
96218 Matrix:
2/7/2024 14:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43522 02/13/24 11:24
<1.39 µg/L 1.39 5.003-Nitroaniline 1 02/14/24 13:38 V43550AMP
<1.53 µg/L 1.53 5.004-Nitroaniline 1 02/14/24 13:38 V43550AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 02/14/24 13:38 V43550AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 02/14/24 13:38 V43550AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 02/14/24 13:38 V43550AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 02/14/24 13:38 V43550AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 02/14/24 13:38 V43550AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 02/14/24 13:38 V43550AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 02/14/24 13:38 V43550AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 02/14/24 13:38 V43550AMP
<0.651 µg/L 0.651 5.00Phenol 1 02/14/24 13:38 V43550AMP
<0.434 µg/L 0.434 2.00Pyrene 1 02/14/24 13:38 V43550AMP
<1.20 M µg/L 1.20 5.00Pyridine 1 02/14/24 13:38 V43550AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 02/14/24 13:38 V43550AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 02/14/24 13:38 V43550AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 02/14/24 13:38 V43550AMP
8270ESurrogate: Phenol-d5 33.6 Limits: 11-100%02/14/24 13:381 AMP
Surrogate: 2-Fluorobiphenyl 61.4 Limits: 44-119%02/14/24 13:381 AMP V43550
Surrogate: 2-Fluorophenol 46.4 Limits: 19-119%02/14/24 13:381 AMP V43550
Surrogate: Nitrobenzene-d5 62.6 Limits: 44-120%02/14/24 13:381 AMP V43550
Surrogate: 4-Terphenyl-d14 77.8 Limits: 50-134%02/14/24 13:381 AMP V43550
Surrogate: 2,4,6-Tribromophenol 79.1 Limits: 43-140%02/14/24 13:381 AMP V43550
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 21 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Metals Analysis
6010D
V43459QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V43397
Associated Lab Samples: 96217, 96218
LRB-V43397 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
02/09/24 20:190.0100.004<0.004mg/LArsenic
02/09/24 20:190.0100.003<0.003mg/LBarium
02/09/24 20:190.00200.0005<0.0005mg/LCadmium
02/09/24 20:190.0050.002<0.002mg/LChromium
02/09/24 20:190.0060.003<0.003mg/LLead
02/09/24 20:190.0200.007<0.007mg/LSelenium
02/09/24 20:190.00500.0007<0.0007mg/LSilver
LCS-V43397Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1040.1040.100mg/LArsenic 80-120
1151.151.00mg/LBarium 80-120
1110.1110.100mg/LCadmium 80-120
1161.161.00mg/LChromium 80-120
1140.1140.100mg/LLead 80-120
1120.1120.100mg/LSelenium 80-120
1130.1130.100mg/LSilver 80-120
V 95764-MS-V43397 V 95764-MSD-V43397Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.104 1040.1100.1000.100< 0.004mg/LArsenic 110 75-125 5.6 20.0
1.19 1171.191.001.000.024mg/LBarium 117 75-125 0.0 20.0
0.112 1120.1120.1000.100< 0.0005mg/LCadmium 112 75-125 0.0 20.0
1.15 1151.151.001.00< 0.002mg/LChromium 115 75-125 0.0 20.0
Page 1 of 15Date:02/16/2024 12:29 PM
Page 22 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Metals Analysis
6010D
V43459QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V43397
V 95764-MS-V43397 V 95764-MSD-V43397Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.116 1130.1150.1000.1000.003mg/LLead 112 75-125 0.8 20.0
0.107 1070.1100.1000.100< 0.007mg/LSelenium 110 75-125 2.7 20.0
0.112 1120.1110.1000.100< 0.0007mg/LSilver 111 75-125 0.8 20.0
V 95764-PDS-V43397Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
02/09/24 21:031070.268mg/LArsenic
02/09/24 21:031152.89mg/LBarium
02/09/24 21:031120.281mg/LCadmium
02/09/24 21:031132.83mg/LChromium
02/09/24 21:031140.286mg/LLead
02/09/24 21:031090.271mg/LSelenium
02/09/24 21:031130.282mg/LSilver
Page 2 of 15Date:02/16/2024 12:29 PM
Page 23 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Total Aqueous Mercury Analysis - CVAA
7470A
V43713QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7470A
QC Prep:V43644
Associated Lab Samples: 96217, 96218
LRB-V43644 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
02/15/24 18:110.000200.00007<0.00007mg/LMercury (Total)
LCS-V43644Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1030.004820.00468mg/LMercury (Total)80-120
V 96217-MS-V43644 V 96217-MSD-V43644Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.00448 96.00.004440.004680.00468< 0.00007mg/LMercury (Total)95.0 80-120 0.8 20.0
V 96217-PDS-V43644Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
02/15/24 18:1996.00.00226mg/LMercury (Total)
Page 3 of 15Date:02/16/2024 12:29 PM
Page 24 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43451QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43450
Associated Lab Samples: 96217, 96218
LRB-V43450 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/10/24 02:425.001.80<1.80µg/LAcetone
02/10/24 02:425.002.00<2.00µg/LAcrolein
02/10/24 02:425.000.230<0.230µg/LAcrylonitrile
02/10/24 02:420.5000.180<0.180µg/LBenzene
02/10/24 02:420.5000.210<0.210µg/LBromobenzene
02/10/24 02:421.000.420<0.420µg/LBromochloromethane
02/10/24 02:420.5000.160<0.160µg/LBromodichloromethane
02/10/24 02:425.001.50<1.50µg/LBromoform
02/10/24 02:421.000.280<0.280µg/LBromomethane
02/10/24 02:421.000.185<0.185µg/Ln-Butylbenzene
02/10/24 02:420.5000.200<0.200µg/Lsec-Butyl benzene
02/10/24 02:422.000.920<0.920µg/Ltert-Butyl benzene
02/10/24 02:425.000.150<0.150µg/LCarbon Disulfide
02/10/24 02:420.5000.180<0.180µg/LCarbon Tetrachloride
02/10/24 02:420.5000.190<0.190µg/LChlorobenzene
02/10/24 02:420.5000.190<0.190µg/LChlorodibromomethane
02/10/24 02:421.000.430<0.430µg/LChloroethane
02/10/24 02:420.5000.220<0.220µg/LChloroform
02/10/24 02:420.5000.220<0.220µg/LChloromethane
02/10/24 02:420.5000.200<0.200µg/L2-Chlorotoluene
02/10/24 02:420.5000.200<0.200µg/L4-Chlorotoluene
02/10/24 02:425.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
02/10/24 02:422.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
02/10/24 02:420.5000.200<0.200µg/L1,2-Dibromoethane
02/10/24 02:420.5000.230<0.230µg/LDibromomethane
02/10/24 02:420.5000.220<0.220µg/L1,2-Dichlorobenzene
02/10/24 02:420.5000.190<0.190µg/L1,3-Dichlorobenzene
Page 4 of 15Date:02/16/2024 12:29 PM
Page 25 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43451QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43450
Associated Lab Samples: 96217, 96218
LRB-V43450 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/10/24 02:420.5000.210<0.210µg/L1,4-Dichlorobenzene
02/10/24 02:425.001.20<1.20µg/LDichlorodifluoromethane
02/10/24 02:420.5000.240<0.240µg/L1,1-Dichloroethane
02/10/24 02:420.5000.150<0.150µg/L1,2-Dichloroethane
02/10/24 02:420.5000.150<0.150µg/L1,1-Dichloroethene
02/10/24 02:420.5000.200<0.200µg/Lcis-1,2-Dichloroethene
02/10/24 02:420.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
02/10/24 02:420.5000.190<0.190µg/L1,2-Dichloropropane
02/10/24 02:420.5000.130<0.130µg/L1,3-Dichloropropane
02/10/24 02:422.000.210<0.210µg/L2,2-Dichloropropane
02/10/24 02:420.5000.200<0.200µg/L1,1-Dichloropropene
02/10/24 02:420.5000.210<0.210µg/Lcis-1,3-Dichloropropene
02/10/24 02:420.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
02/10/24 02:420.5000.170<0.170µg/LEthylbenzene
02/10/24 02:4210.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
02/10/24 02:422.000.350<0.350µg/LHexachlorobutadiene
02/10/24 02:4210.01.30<1.30µg/Ln-Hexane
02/10/24 02:425.000.380<0.380µg/L2-Hexanone
02/10/24 02:425.000.180<0.180µg/LIsopropylbenzene
02/10/24 02:420.5000.089<0.089µg/L4-Isopropyl toluene
02/10/24 02:425.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
02/10/24 02:420.5000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
02/10/24 02:425.001.00<1.00µg/L4-Methyl-2-Pentanone
02/10/24 02:421.000.330<0.330µg/LMethylene Chloride
02/10/24 02:421.000.470<0.470µg/LNaphthalene
02/10/24 02:420.5000.190<0.190µg/Ln-Propylbenzene
02/10/24 02:420.5000.220<0.220µg/LStyrene
Page 5 of 15Date:02/16/2024 12:29 PM
Page 26 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43451QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43450
Associated Lab Samples: 96217, 96218
LRB-V43450 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/10/24 02:420.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
02/10/24 02:420.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
02/10/24 02:420.5000.220<0.220µg/LTetrachloroethene
02/10/24 02:420.5000.220<0.220µg/LToluene
02/10/24 02:422.000.380<0.380µg/L1,2,3-Trichlorobenzene
02/10/24 02:421.000.310<0.310µg/L1,2,4-Trichlorobenzene
02/10/24 02:420.5000.160<0.160µg/L1,1,1-Trichloroethane
02/10/24 02:420.5000.096<0.096µg/L1,1,2-Trichloroethane
02/10/24 02:420.5000.180<0.180µg/LTrichloroethene
02/10/24 02:420.5000.180<0.180µg/LTrichlorofluoromethane
02/10/24 02:421.000.270<0.270µg/L1,2,3-Trichloropropane
02/10/24 02:420.5000.180<0.180µg/L1,3,5-Trimethylbenzene
02/10/24 02:422.001.00<1.00µg/LVinyl Acetate
02/10/24 02:420.5000.170<0.170µg/LVinyl Chloride
02/10/24 02:420.5000.210<0.210µg/Lo-Xylene
02/10/24 02:421.000.420<0.420µg/Lm,p-Xylene
02/10/24 02:424-Bromofluorobenzene (S)98.4 80-124
02/10/24 02:42Dibromofluoromethane (S)96.8 75-129
02/10/24 02:421,2-Dichloroethane - d4 (S)97.6 63-136
02/10/24 02:42Toluene-d8 (S)99.2 77-123
LCS-V43450 LCSD-V43450Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.3 93.295.038.040.0µg/LAcetone 40-166 1.8 20.0
38.1 95.293.237.340.0µg/LAcrolein 70-130 2.1 20.0
Page 6 of 15Date:02/16/2024 12:29 PM
Page 27 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43451QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43450
LCS-V43450 LCSD-V43450Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
41.9 10510341.240.0µg/LAcrylonitrile 81-127 1.6 20.0
20.4 10210520.920.0µg/LBenzene 77-128 2.4 20.0
19.4 97.010621.120.0µg/LBromobenzene 78-129 8.3 20.0
20.2 10110220.420.0µg/LBromochloromethane 78-135 0.9 20.0
19.8 99.010220.320.0µg/LBromodichloromethane 76-138 2.4 20.0
19.7 98.510220.320.0µg/LBromoform 71-135 3.0 20.0
23.2 11612124.120.0µg/LBromomethane 41-168 3.8 20.0
19.5 97.510621.120.0µg/Ln-Butylbenzene 68-134 7.8 20.0
20.2 10111021.920.0µg/Lsec-Butyl benzene 71-131 8.0 20.0
19.8 99.010821.520.0µg/Ltert-Butyl benzene 70-132 8.2 20.0
20.2 10110320.520.0µg/LCarbon Disulfide 59-135 1.4 20.0
18.9 94.597.019.420.0µg/LCarbon Tetrachloride 72-142 2.6 20.0
20.1 10110320.520.0µg/LChlorobenzene 78-119 1.9 20.0
20.2 10110320.520.0µg/LChlorodibromomethane 75-134 1.4 20.0
20.9 10510921.820.0µg/LChloroethane 57-142 4.2 20.0
19.8 99.010220.320.0µg/LChloroform 77-130 2.4 20.0
19.9 99.510320.520.0µg/LChloromethane 47-145 2.9 20.0
19.6 98.010721.320.0µg/L2-Chlorotoluene 74-126 8.3 20.0
19.4 97.010621.120.0µg/L4-Chlorotoluene 78-129 8.3 20.0
20.3 10210320.520.0µg/LDi-Isopropyl Ether (DIPE)60-154 0.9 20.0
19.3 96.510721.420.0µg/L1,2-Dibromo-3-Chloropropane 63-134 10.3 20.0
19.8 99.010120.220.0µg/L1,2-Dibromoethane 77-135 2.0 20.0
20.4 10210320.620.0µg/LDibromomethane 76-138 0.9 20.0
20.1 10110721.420.0µg/L1,2-Dichlorobenzene 78-128 6.2 20.0
19.7 98.510621.120.0µg/L1,3-Dichlorobenzene 77-125 6.8 20.0
19.5 97.510520.920.0µg/L1,4-Dichlorobenzene 75-126 6.9 20.0
Page 7 of 15Date:02/16/2024 12:29 PM
Page 28 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43451QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43450
LCS-V43450 LCSD-V43450Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.6 11311723.420.0µg/LDichlorodifluoromethane 28-163 3.4 20.0
19.9 99.510420.720.0µg/L1,1-Dichloroethane 70-130 3.9 20.0
19.3 96.597.019.420.0µg/L1,2-Dichloroethane 68-131 0.5 20.0
20.0 10010220.320.0µg/L1,1-Dichloroethene 70-154 1.4 20.0
19.0 95.095.519.120.0µg/Lcis-1,2-Dichloroethene 76-141 0.5 20.0
20.2 10110320.620.0µg/Ltrans-1,2-Dichloroethene 76-135 1.9 20.0
20.1 10110320.620.0µg/L1,2-Dichloropropane 77-130 2.4 20.0
20.1 10110320.620.0µg/L1,3-Dichloropropane 76-132 2.4 20.0
17.5 87.588.017.620.0µg/L2,2-Dichloropropane 29-149 0.5 20.0
20.2 10110420.820.0µg/L1,1-Dichloropropene 71-136 2.9 20.0
20.6 10310621.120.0µg/Lcis-1,3-Dichloropropene 65-140 2.3 20.0
20.1 10110320.520.0µg/Ltrans-1,3-Dichloropropene 67-140 1.9 20.0
19.5 97.510320.520.0µg/LEthylbenzene 80-127 5.0 20.0
42.4 10610742.640.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 0.4 20.0
20.4 10210621.220.0µg/LHexachlorobutadiene 61-134 3.8 20.0
20.0 10010220.320.0µg/Ln-Hexane 70-130 1.4 20.0
19.0 95.099.019.820.0µg/L2-Hexanone 64-137 4.1 20.0
19.8 99.010821.620.0µg/LIsopropylbenzene 70-130 8.6 20.0
20.0 10010921.820.0µg/L4-Isopropyl toluene 69-132 8.6 20.0
18.3 91.595.519.120.0µg/LMethyl Ethyl Ketone (MEK)71-134 4.2 20.0
20.9 10510420.820.0µg/LMethyl tert-butyl ether (MTBE)68-135 0.4 20.0
20.2 10110320.520.0µg/L4-Methyl-2-Pentanone 69-134 1.4 20.0
19.2 96.098.519.720.0µg/LMethylene Chloride 73-131 2.5 20.0
20.1 10199.519.920.0µg/LNaphthalene 64-136 1.0 20.0
19.7 98.510721.420.0µg/Ln-Propylbenzene 72-132 8.2 20.0
20.2 10110721.420.0µg/LStyrene 78-129 5.7 20.0
Page 8 of 15Date:02/16/2024 12:29 PM
Page 29 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43451QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43450
LCS-V43450 LCSD-V43450Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.0 10010020.020.0µg/L1,1,1,2-Tetrachloroethane 79-134 0.0 20.0
19.3 96.510320.620.0µg/L1,1,2,2-Tetrachloroethane 62-127 6.5 20.0
19.7 98.510320.620.0µg/LTetrachloroethene 80-129 4.4 20.0
20.4 10210420.720.0µg/LToluene 76-131 1.4 20.0
21.5 10811122.220.0µg/L1,2,3-Trichlorobenzene 58-144 3.2 20.0
20.5 10310320.620.0µg/L1,2,4-Trichlorobenzene 66-139 0.4 20.0
19.9 99.510220.420.0µg/L1,1,1-Trichloroethane 75-135 2.4 20.0
20.4 10210520.920.0µg/L1,1,2-Trichloroethane 70-140 2.4 20.0
19.8 99.010220.420.0µg/LTrichloroethene 77-133 2.9 20.0
21.3 10711222.420.0µg/LTrichlorofluoromethane 62-148 5.0 20.0
19.3 96.510721.420.0µg/L1,2,3-Trichloropropane 71-127 10.3 20.0
19.8 99.010821.520.0µg/L1,3,5-Trimethylbenzene 75-131 8.2 20.0
21.5 10810621.220.0µg/LVinyl Acetate 34-167 1.4 20.0
20.7 10410721.420.0µg/LVinyl Chloride 57-141 3.3 20.0
20.0 10010621.120.0µg/Lo-Xylene 78-128 5.3 20.0
41.8 10511043.840.0µg/Lm,p-Xylene 77-133 4.6 20.0
99.81024-Bromofluorobenzene (S)80-124
96.494.0Dibromofluoromethane (S)75-129
94.693.81,2-Dichloroethane - d4 (S)63-136
99.899.6Toluene-d8 (S)77-123
Page 9 of 15Date:02/16/2024 12:29 PM
Page 30 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43522
Associated Lab Samples: 96217, 96218
LRB-V43522 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/14/24 11:182.000.302<0.302µg/LAcenaphthene
02/14/24 11:182.000.297<0.297µg/LAcenaphthylene
02/14/24 11:185.002.05<2.05µg/LAniline
02/14/24 11:182.000.836<0.836µg/LAnthracene
02/14/24 11:182.000.637<0.637µg/LBenzo(a)anthracene
02/14/24 11:182.001.02<1.02µg/LBenzo(a)pyrene
02/14/24 11:185.002.49<2.49µg/LBenzo(b)fluoranthene
02/14/24 11:185.001.01<1.01µg/LBenzo(g,h,i)perylene
02/14/24 11:185.001.99<1.99µg/LBenzo(k)fluoranthene
02/14/24 11:1810.01.10<1.10µg/LBenzoic Acid
02/14/24 11:185.000.684<0.684µg/LBenzyl alcohol
02/14/24 11:185.000.468<0.468µg/LBis(2-Chloroethoxy)methane
02/14/24 11:185.001.04<1.04µg/LBis(2-Chloroethyl)ether
02/14/24 11:185.001.08<1.08µg/LBis(2-Chloroisopropyl)ether
02/14/24 11:1810.03.46<3.46µg/LBis(2-ethylhexyl)phthalate
02/14/24 11:185.001.11<1.11µg/L4-Bromophenyl phenyl ether
02/14/24 11:185.001.83<1.83µg/LButyl benzyl phthalate
02/14/24 11:185.001.18<1.18µg/L4-Chloro-3-methylphenol
02/14/24 11:185.001.33<1.33µg/L4-Chloroaniline
02/14/24 11:1820.01.83<1.83µg/L2-Chloronaphthalene
02/14/24 11:1810.00.938<0.938µg/L2-Chlorophenol
02/14/24 11:185.001.71<1.71µg/L4-Chlorophenyl phenyl ether
02/14/24 11:182.000.405<0.405µg/LChrysene
02/14/24 11:182.000.434<0.434µg/LDibenz(a,h)anthracene
02/14/24 11:185.000.856<0.856µg/LDibenzofuran
02/14/24 11:185.002.00<2.00µg/L1,2-Dichlorobenzene
02/14/24 11:185.002.00<2.00µg/L1,3-Dichlorobenzene
Page 10 of 15Date:02/16/2024 12:29 PM
Page 31 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43522
Associated Lab Samples: 96217, 96218
LRB-V43522 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/14/24 11:185.002.05<2.05µg/L1,4-Dichlorobenzene
02/14/24 11:185.001.89<1.89µg/L3,3'-Dichlorobenzidine
02/14/24 11:1810.01.46<1.46µg/L2,4-Dichlorophenol
02/14/24 11:185.000.745<0.745µg/LDiethyl phthalate
02/14/24 11:185.000.939<0.939µg/LDimethyl phthalate
02/14/24 11:1820.01.57<1.57µg/L2,4-Dimethylphenol
02/14/24 11:185.002.06<2.06µg/LDi-n-butyl phthalate
02/14/24 11:1810.02.07<2.07µg/L4,6-Dinitro-2-methylphenol
02/14/24 11:1810.01.92<1.92µg/L2,4-Dinitrophenol
02/14/24 11:185.001.11<1.11µg/L2,4-Dinitrotoluene
02/14/24 11:185.000.809<0.809µg/L2,6-Dinitrotoluene
02/14/24 11:185.001.65<1.65µg/LDi-n-Octyl Phthalate
02/14/24 11:182.000.250<0.250µg/LFluoranthene
02/14/24 11:182.000.807<0.807µg/LFluorene
02/14/24 11:185.000.979<0.979µg/LHexachlorobenzene
02/14/24 11:185.002.73<2.73µg/LHexachlorobutadiene
02/14/24 11:185.002.05<2.05µg/LSPLP Hexachlorocyclopentadiene
02/14/24 11:185.001.76<1.76µg/LHexachloroethane
02/14/24 11:182.000.477<0.477µg/LIndeno(1,2,3-cd)pyrene
02/14/24 11:185.000.444<0.444µg/LIsophorone
02/14/24 11:182.001.14<1.14µg/L1-Methylnaphthalene
02/14/24 11:182.000.666<0.666µg/L2-Methylnaphthalene
02/14/24 11:185.001.15<1.15µg/L2-Methylphenol
02/14/24 11:1810.00.880<0.880µg/L3&4 Methylphenol
02/14/24 11:182.000.728<0.728µg/LNaphthalene
02/14/24 11:185.001.39<1.39µg/L2-Nitroaniline
02/14/24 11:185.001.39<1.39µg/L3-Nitroaniline
Page 11 of 15Date:02/16/2024 12:29 PM
Page 32 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43522
Associated Lab Samples: 96217, 96218
LRB-V43522 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/14/24 11:185.001.53<1.53µg/L4-Nitroaniline
02/14/24 11:185.000.905<0.905µg/LNitrobenzene
02/14/24 11:185.000.493<0.493µg/L2-Nitrophenol
02/14/24 11:1810.01.23<1.23µg/L4-Nitrophenol
02/14/24 11:185.000.450<0.450µg/LN-Nitrosodimethylamine
02/14/24 11:185.001.10<1.10µg/LN-Nitrosodiphenylamine
02/14/24 11:185.000.641<0.641µg/LN-Nitroso-di-n-propylamine
02/14/24 11:185.001.43<1.43µg/LPentachlorophenol
02/14/24 11:182.000.428<0.428µg/LPhenanthrene
02/14/24 11:185.000.651<0.651µg/LPhenol
02/14/24 11:182.000.434<0.434µg/LPyrene
02/14/24 11:185.001.20<1.20µg/LPyridine
02/14/24 11:185.002.21<2.21µg/L1,2,4-Trichlorobenzene
02/14/24 11:185.001.31<1.31µg/L2,4,5-Trichlorophenol
02/14/24 11:185.001.32<1.32µg/L2,4,6-Trichlorophenol
02/14/24 11:182-Fluorobiphenyl (S)68.4 44-119
02/14/24 11:182-Fluorophenol (S)47.6 19-119
02/14/24 11:18Nitrobenzene-d5 (S)72.2 44-120
02/14/24 11:184-Terphenyl-d14 (S)80.0 50-134
02/14/24 11:182,4,6-Tribromophenol (S)82.6 43-140
02/14/24 11:18Phenol-d5 (S)32.3 11-100
LCS-V43522 LCSD-V43522Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
31.3 62.668.834.450.0µg/LAcenaphthene 38-117 9.4 20.0
Page 12 of 15Date:02/16/2024 12:29 PM
Page 33 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43522
LCS-V43522 LCSD-V43522Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
31.3 62.668.234.150.0µg/LAcenaphthylene 41-130 8.5 20.0
36.3 72.676.038.050.0µg/LAniline 12-197 4.5 20.0
37.8 75.681.440.750.0µg/LAnthracene 57-123 7.3 20.0
37.6 75.277.038.550.0µg/LBenzo(a)anthracene 58-125 2.3 20.0
49.9 99.810351.750.0µg/LBenzo(a)pyrene 54-128 3.5 20.0
46.3 92.694.647.350.0µg/LBenzo(b)fluoranthene 53-131 2.1 20.0
43.8 87.689.644.850.0µg/LBenzo(g,h,i)perylene 50-134 2.2 20.0
38.7 77.482.041.050.0µg/LBenzo(k)fluoranthene 53-131 5.7 20.0
19.1 38.240.420.250.0µg/LBenzoic Acid 10-125 5.5 20.0
31.9 63.870.035.050.0µg/LBenzyl alcohol 31-112 9.2 20.0
29.9 59.865.432.750.0µg/LBis(2-Chloroethoxy)methane 48-120 8.9 20.0
30.4 60.867.833.950.0µg/LBis(2-Chloroethyl)ether 43-118 10.8 20.0
23.6 47.253.426.750.0µg/LBis(2-Chloroisopropyl)ether 37-130 12.3 20.0
44.2 88.492.246.150.0µg/LBis(2-ethylhexyl)phthalate 55-135 4.2 20.0
31.5 63.065.032.550.0µg/L4-Bromophenyl phenyl ether 55-124 3.1 20.0
46.8 93.697.048.550.0µg/LButyl benzyl phthalate 53-134 3.5 20.0
34.0 68.072.636.350.0µg/L4-Chloro-3-methylphenol 52-119 6.5 20.0
35.7 71.472.836.450.0µg/L4-Chloroaniline 33-117 1.9 20.0
28.2 56.462.831.450.0µg/L2-Chloronaphthalene 40-116 10.7 20.0
32.3 64.673.036.550.0µg/L2-Chlorophenol 38-117 12.2 20.0
31.2 62.467.433.750.0µg/L4-Chlorophenyl phenyl ether 53-121 7.7 20.0
36.0 72.074.837.450.0µg/LChrysene 59-123 3.8 20.0
30.4 60.862.831.450.0µg/LDibenz(a,h)anthracene 51-134 3.2 20.0
32.8 65.670.835.450.0µg/LDibenzofuran 53-118 7.6 20.0
22.9 45.850.625.350.0µg/L1,2-Dichlorobenzene 32-111 9.9 20.0
22.1 44.249.024.550.0µg/L1,3-Dichlorobenzene 28-110 10.3 20.0
Page 13 of 15Date:02/16/2024 12:29 PM
Page 34 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43522
LCS-V43522 LCSD-V43522Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.3 42.647.423.750.0µg/L1,4-Dichlorobenzene 29-112 10.6 20.0
36.7 73.477.438.750.0µg/L3,3'-Dichlorobenzidine 27-129 5.3 20.0
30.1 60.264.632.350.0µg/L2,4-Dichlorophenol 47-121 7.0 20.0
36.8 73.677.238.650.0µg/LDiethyl phthalate 56-125 4.7 20.0
36.8 73.678.039.050.0µg/LDimethyl phthalate 45-127 5.8 20.0
42.1 84.293.046.550.0µg/L2,4-Dimethylphenol 31-124 9.9 20.0
41.1 82.288.044.050.0µg/LDi-n-butyl phthalate 59-127 6.8 20.0
37.9 75.880.040.050.0µg/L4,6-Dinitro-2-methylphenol 44-137 5.3 20.0
40.5 81.084.042.050.0µg/L2,4-Dinitrophenol 23-143 3.6 20.0
42.1 84.287.043.550.0µg/L2,4-Dinitrotoluene 57-128 3.2 20.0
42.1 84.289.444.750.0µg/L2,6-Dinitrotoluene 57-124 5.9 20.0
46.2 92.496.848.450.0µg/LDi-n-Octyl Phthalate 51-140 4.6 20.0
37.0 74.078.439.250.0µg/LFluoranthene 57-128 5.7 20.0
34.2 68.474.037.050.0µg/LFluorene 52-124 7.8 20.0
32.5 65.068.234.150.0µg/LHexachlorobenzene 53-125 4.8 20.0
20.9 41.846.023.050.0µg/LHexachlorobutadiene 22-124 9.5 20.0
17.8 35.638.819.450.0µg/LSPLP Hexachlorocyclopentadiene 32-117 8.6 20.0
23.5 47.052.026.050.0µg/LHexachloroethane 21-115 10.1 20.0
42.0 84.086.043.050.0µg/LIndeno(1,2,3-cd)pyrene 52-134 2.3 20.0
30.7 61.464.432.250.0µg/LIsophorone 42-124 4.7 20.0
23.7 47.452.826.450.0µg/L1-Methylnaphthalene 41-119 10.7 20.0
23.3 46.651.225.650.0µg/L2-Methylnaphthalene 40-121 9.4 20.0
31.9 63.870.635.350.0µg/L2-Methylphenol 30-117 10.1 20.0
26.3 52.656.628.350.0µg/L3&4 Methylphenol 29-110 7.3 20.0
24.8 49.654.827.450.0µg/LNaphthalene 40-121 9.9 20.0
40.6 81.286.243.150.0µg/L2-Nitroaniline 55-127 5.9 20.0
Page 14 of 15Date:02/16/2024 12:29 PM
Page 35 of 38
Quality Control Data
24-039-0035Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Former Winston Container
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43522
LCS-V43522 LCSD-V43522Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.6 81.286.243.150.0µg/L3-Nitroaniline 41-128 5.9 20.0
38.7 77.482.641.350.0µg/L4-Nitroaniline 45-135 6.5 20.0
28.2 56.461.630.850.0µg/LNitrobenzene 45-121 8.8 20.0
29.5 59.061.630.850.0µg/L2-Nitrophenol 47-123 4.3 20.0
15.3 30.635.817.950.0µg/L4-Nitrophenol 10-105 15.6 20.0
19.6 39.243.421.750.0µg/LN-Nitrosodimethylamine 10-119 10.1 20.0
43.2 86.493.246.650.0µg/LN-Nitrosodiphenylamine 51-123 7.5 20.0
35.4 70.877.838.950.0µg/LN-Nitroso-di-n-propylamine 49-119 9.4 20.0
38.5 77.081.640.850.0µg/LPentachlorophenol 35-138 5.8 20.0
36.3 72.677.638.850.0µg/LPhenanthrene 59-120 6.6 20.0
13.5 27.030.215.150.0µg/LPhenol 12-58 11.1 20.0
38.7 77.481.840.950.0µg/LPyrene 57-126 5.5 20.0
7.87 15.79.2*4.6150.0µg/LPyridine 10-80 52.2*20.0
21.4 42.846.623.350.0µg/L1,2,4-Trichlorobenzene 29-126 8.5 20.0
35.3 70.677.638.850.0µg/L2,4,5-Trichlorophenol 53-123 9.4 20.0
32.7 65.472.236.150.0µg/L2,4,6-Trichlorophenol 50-125 9.8 20.0
62.068.02-Fluorobiphenyl (S)44-119
42.046.42-Fluorophenol (S)19-119
58.062.6Nitrobenzene-d5 (S)44-120
71.076.04-Terphenyl-d14 (S)50-134
78.784.92,4,6-Tribromophenol (S)43-140
27.931.0Phenol-d5 (S)11-100
Page 15 of 15* QC Fail Date:02/16/2024 12:29 PM
Page 36 of 38
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:24-039-0035
Mid-Atlantic Associates, Inc. - Charlotte
01138
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.6C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:02/08/2024 17:20:44
Special precautions or instructions included?
Comments:
Page 37 of 38
Page 38 of 38

APPENDIX E
NCDEQ Risk Calculator (February 2024)

Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
12/19/2023
Prepared By:Shane Sisco, P.G.
Mid-Atlantic Associates, Inc.
Greg Icenhour, P.G.
Soil Vapor (Highest Concentrations)
Former Winston Container
4901 Winston Container Road, Charlotte, North Carolina
Brownfields
27003-23-060
July 2023
May 2023 EPA RSL Table
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 27003-23-060
Exposure Unit ID: Soil Vapor (Highest Concentrations)
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 27003-23-060
Exposure Unit ID: Soil Vapor (Highest Concentrations)
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2023
Basis: May 2023 EPA RSL TableSite ID: 27003-23-060
Exposure Unit ID: Soil Vapor (Highest Concentrations)
Description of Exposure Point Concentration Selection:
Exposure Point Concentration
(ug/m3)Notes:CAS Number Chemical Minimum Concentration (Qualifier)
Maximum Concentration (Qualifier)
Units Location of Maximum Concentration
Detection Frequency
Range of Detection Limits
Concentration Used for Screening
Background Value
Screening Toxicity Value (Screening Level) (n/c)
Potential ARAR/TBC Value
Potential ARAR/TBC Source
COPC Flag (Y/N)
Rationale for Selection or Deletion
30.6 67-64-1 Acetone
17.5 71-43-2 Benzene
2.34 106-99-0 Butadiene, 1,3-0.868 75-15-0 Carbon Disulfide
16.6 110-82-7 Cyclohexane
2.86 75-71-8 Dichlorodifluoromethane
24 141-78-6 Ethyl Acetate
18.7 100-41-4 Ethylbenzene
19.4 142-82-5 Heptane, N-
56.2 110-54-3 Hexane, N-
9.43 67-63-0 Isopropanol7.11 78-93-3 Methyl Ethyl Ketone (2-Butanone)
1.35 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)
2.64 75-09-2 Methylene Chloride
13.9 115-07-1 Propylene
1.51 100-42-5 Styrene
3.32 127-18-4 Tetrachloroethylene
99.3 108-88-3 Toluene
0.766 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-1.31 71-55-6 Trichloroethane, 1,1,1-
415 75-69-4 Trichlorofluoromethane
8.9 95-63-6 Trimethylbenzene, 1,2,4-
2.92 108-67-8 Trimethylbenzene, 1,3,5-
70.8 1330-20-7 Xylenes
Input Form 2D
Soil Gas Exposure Point Concentration Table
Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 27003-23-060
Exposure Unit ID: Soil Vapor (Highest Concentrations)
Receptor Pathway Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.1E-07 7.6E-03 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
Surface Water
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
North Carolina DEQ Risk Calculator