22004-Witherspoon Nursury-Redevelopment Summary Report

hart � hickman
Via Email SMARTER ENVIRONMENTAL SOLUTIONS
January 30, 2023
NCDEQ — Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, NC 27699-1646
Attention: Ms. Sarah Hardison Young
Re: Annual Redevelopment Summary Report — Witherspoon Nursery West
Witherspoon Nursery
3312 Watkins Road
Durham, North Carolina
Brownfields Project No. 22004-18-032
H&H Job No. CRP-003
Dear Sarah:
On behalf of Crowne at 501, Limited Partnership (Crowne at 501), Hart & Hickman, PC (H&H)
is submitting this annual report in accordance with the executed Brownfields Agreement. A
Brownfields Agreement (Brownfields Project No. 22004-18-032) between the Prospective
Developer (PD) and the North Carolina Department of Environmental Quality (DEQ) was
executed for the Witherspoon Nursery Brownfields property on January 9, 2020. The
Brownfields property totals approximately 8.0 acres on two parcels of land, located at 3312 and
3330 Watkins Road in Durham, Durham County, North Carolina (Site or subject Site). The PD
sold 3.7 acres of the Brownfields Site (i.e., the western parcel) to Crowne at 501, Limited
Partnership (hereinafter referred to as the Witherspoon Nursery West property at 3312 Watkins
Road), and the PD retained the eastern 4.3 acres of the Brownfields Site (hereinafter referred to
as the Witherspoon Nursery East property at 3330 Watkins Road).
As it relates to the Witherspoon Nursery West property during the 2022 redevelopment time
period, this report has been prepared in accordance with Land Use Restrictions (LURs) set forth
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

Ms. Sarah Hardison Young
January 30, 2023
Page 2
in paragraph 15(c) (environmental -related reporting requirements associated with ongoing
redevelopment activities) included in the executed Brownfields Agreement for the Site.
Proposed redevelopment of the Witherspoon Nursery West property includes the construction of
residential apartments and commercial, retail, office, and open spaces. Details pertaining to
redevelopment activities for the 2021 redevelopment time period are provided in H&H's Annual
Redevelopment Summary Report — Witherspoon Nursery West dated January 28, 2022. A Site
map depicting the proposed redevelopment plan is included as Figure 2.
Redevelopment activities at the Site have been conducted in accordance with the DEQ approved
Environmental Management Plan (EMP) dated April 24, 2019, and revised on May 27, 2020.
The sections below outline activities completed to satisfy the requirements of the executed
Brownfields Agreement and DEQ approved EMP.
1.0 Environmental -Related Reporting Requirements
In accordance with LUR paragraph 15(c) in the executed Brownfields Agreement for the Site,
redevelopment activities at the Witherspoon Nursery West property are ongoing and have
included the following activities:
• Soil management during excavation and grading activities, including off -Site export; and
• Installation of hardscaped and landscaped areas.
The sections below outline activities completed to evaluate and manage Site media during
redevelopment activities.
https://hardiick.shmepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Crowne hart : h i c k m a n
Partners Inc - CRP/CRP-003 Brownfields Assistance/2022 Redevelopment Activities/Final to
DEQ/Redevelopment Summary Report_ Witherspoon.doc
SMARTER ENVIRONMENTAL SOLUTIONS

Ms. Sarah Hardison Young
January 30, 2023
Page 3
1.1 Grading, Excavation, and Stockpile Sampling Activities
During grading and excavation activities conducted in May 2022 and August 2022,
approximately 550 cubic yards (cy) of soil were stockpiled for characterization purposes. In
accordance with the DEQ-approved EMP, stockpiles were evaluated by collecting soil samples
at a frequency of one sample per approximately 1,000 cy or at minimum, one sample per
stockpile. As such, H&H mobilized to the Site on May 3, 2022, and August 31, 2022, to collect
stockpile samples (Stockpile-14 and Stockpile-15, respectively) for waste characterization
purposes to evaluate potential off -Site export disposal facilities. Note that management of soil
associated with Stockpiles-1 through 8, and Stockpile-10, was documented in H&H's Annual
Redevelopment Summary Report — Witherspoon Nursery West dated January 27, 2021, and
management of soil associated with Stockpiles 9 and 11 through 13 was documented in H&H's
Annual Redevelopment Summary Report — Witherspoon Nursery West dated January 28, 2022.
The soil samples were collected directly into laboratory supplied glassware, labeled with the
sample identification, dates, times, requested analyses and placed on ice in laboratory supplied
coolers under standard chain of custody protocols. The soil samples were submitted to Pace
Analytical (Pace) for analysis specified in the EMP: volatile organic compounds (VOCs) by EPA
Method 8260, semi-VOCs (SVOCs) by EPA Method 8270, Resource Conservation and
Recovery Act (RCRA) metals by EPA Methods 6020/7471, and organochlorine pesticides by
EPA Method 8081. Copies of the laboratory analytical reports and chain of custody records are
provided in Appendix A.
1.2 Stockpile Sampling Results
Laboratory analytical results were compared to the July 2022 DEQ Protection of Groundwater,
Residential, and Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs) and are
summarized in Table 1. In addition to the PSRGs, metals results were compared to published
background ranges for North Carolina soils published in Elements in North American Soils
authored by Dragun and Chekiri (2005).
https://hardiick.shmepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Crowne hart : h i c k m a n
Partners Inc - CRP/CRP-003 Brownfields Assistance/2022 Redevelopment Activities/Final to
DEQ/Redevelopment Summary Report_ Witherspoon.doc
SMARTER ENVIRONMENTAL SOLUTIONS

Ms. Sarah Hardison Young
January 30, 2023
Page 4
Laboratory analytical results indicated that low levels of chlorobenzene (0.0033 J mg/kg),
ethylbenzene (0.0035 J mg/kg), isopropylbenzene (0.0027 J mg/kg), total xylenes (0.011 mg/kg)
and organochlorine pesticide 4,4'-DDE (0.024 mg/kg) were detected in Stockpile-15 at
concentrations above laboratory method detection limits, but below the DEQ PSRGs
As expected, naturally occurring levels of some metals were detected at concentrations above the
laboratory method detection limits in each soil sample. Arsenic was detected at concentrations up
to 3.4 mg/kg, which exceeds the Residential PSRG of 0.68 mg/kg. However, the detections of
arsenic are consistent with published background ranges for North Carolina soils. No other
metals were detected at concentrations exceeding the DEQ PSRGs.
1.3 Export Soil Activities
On behalf of Crowne at 501, H&H submitted a soil transfer request to the DEQ Brownfields
Program on March 4, 2020, for approval to export soil to Fogleman and Fogleman Soils, Inc.
(Fogleman), a Land Clearing and Inert Debris (LCID) landfill located at 4005 Intermere Road in
Durham, North Carolina. Initial export activities to Fogleman were approved in a letter provided
by DEQ Brownfields dated March 18, 2020. Subsequent export activities to Fogleman were
approved by Fogleman in a letter provided by Smith Gardner, Inc. (S+G) on behalf of Fogleman,
dated November 30, 2020, and subsequent emails from S+G dated March 29, 2021, May 11,
2022, and September 20, 2022. In total, approximately 550 cy of soil associated with Stockpile-
14 and Stockpile-15 were exported to Fogleman's facility in Durham, North Carolina during the
months of May and October 2022. Export approval letters and emails can be provided upon
request. Copies of truck logs to Fogleman are included in Appendix B.
https://hardiick.shmepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Crowne hart : h i c k m a n
Partners Inc - CRP/CRP-003 Brownfields Assistance/2022 Redevelopment Activities/Final to
DEQ/Redevelopment Summary Report_ Witherspoon.doc
SMARTER ENVIRONMENTAL SOLUTIONS

Ms. Sarah Hardison Young
January 30, 2023
Page 5
Should you have any questions or need additional information, please do not hesitate to call me
at [phone].
Sincerely,
Hart & Hickman, PC
'30/2023
Justin Ballard, PG
Project Manager
cc: Ms. Andrea Haines (Crowne Partners)
Ms. Morgan Pendry (Crowne Partners)
Ms. Tracy Fowlkes (Crowne Partners)
Ms. Jonelle Kerins (Crowne Partners)
Attachments
https://hardiick.shmepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Crowne hart : h i c k m a n
Partners Inc - CRP/CRP-003 Brownfields Assistance/2022 Redevelopment Activities/Final to
DEQ/Redevelopment Summary Report_ Witherspoon.doc
SMARTER ENVIRONMENTAL SOLUTIONS

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Table 1 (Page 1 of 1)
Summary of Stockpile Analytical Data
Witherspoon Nursery
Durham, North Carolina
Brownfields Project No. 22004-18-032
H&H Job No. CRP-003
Industrial/
Protection of
Sample ID
Residential
Commercial
Groundwater
Regional Background
Stockpile-14
Stockpile-15
PSRG(1)
PSRG(')
PSRG(1)
Metals in Soil(2)
Sample Date
5/3/2022
8/31 /2022
VOCs in mg/kg (8260D)
Chlorobenzene
58
280
0.68
--
--
--
<0.0011
0.0033 J
Ethylbenzene
6.1
27
13
--
--
--
<0.0028
0.0035 J
Isopropylbenzene (Cumene)
410
2,100
2.3
<0.0020
0.0027 J
Total x lenes
120
530
9.9
--
--
--
<0.0034
0.011
SVOCs in mg/kg (8270E)
-
--
--
--
ALL BRL
ALL BRL
Organochlorine Pesticides in mg/kg (8081 B)
4,4'-DDD
0.38
4.9
0.47
--
--
--
<0.0011
<0.0011
4,4'-DDE
2.0
9.3
0.47
--
--
--
<0.0012
0.024
4,4'-DDT
1.9
8.5
0.67
--
--
--
<0.0011
<0.0011
RCRA Metals in mg/kg (6020B/7471B)
Arsenic
0.68
3.0
5.8
1.0-18
4.8
A
3.4
1.64
Barium
3,100
47,000
580
50-1,000
356
A
86.1
68.2
Cadmium
1.4
20
3.0
1.0-10
4.3
B
0.103
Total Chromium
23,000*
350,000*
360,000*
7.0-300
65
A
23.4
21.3
Lead
400
800
270
BRL-50
16
A
10.9
11.2
Selenium
78
1,200
2.1
<0.1-0.8
0.42
A
0.42 J
<0.14
Silver
78
1,200
3.4
BRL-5.0
NS
C
0.19 J
0.15 J
Mercury
2.3
9.7
1.0
0.03-0.52
0.121
A
0.012 J
0.089
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) (July 2022).
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.
Ref. A. North Carolina soils, B. Southeastern US soils, C. Soils of the conterminous USA
With the exception of metals, only analytes with concentrations above the laboratory method detection limits are shown.
Soil concentrations are reported in milligrams per kilogram (mg/kg).
Laboratory analytical methods are shown in parentheses.
Bold indicates concentration exceeds DEQ Residential PSRG (July 2022).
-- = not applicable; BRL = below laboratory method detection limit; * = indicates chromium III PSRG
J = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in an estimated concentration.
File: https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Crowne Partners Inc - CRP/CRP-003 Brownfields Assistance/2022 Redevelopment Activities/Stockpile Sampling Table_ Witherspoon Nursery_9-16-2022Stockpile Sampling

Appendix A
Laboratory Analytical Results

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
May 10, 2022
Justin Ballard
Hart & Hickman
3921 Sunset Ridge Rd.
Suite 301
Raleigh, NC 27607
RE: Project: CRP.003
Pace Project No.: 92602305
Dear Justin Ballard:
Enclosed are the analytical results for sample(s) received by the laboratory on May 03, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
1(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 35

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: CRP.003
Pace Project No.: 92602305
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
1800 Elm Street SE, Minneapolis, MN 55414--Satellite Air
Lab
A21-A Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009*
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014*
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
Florida Certification #: E87605*
Georgia Certification #: 959
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification M E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086*
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064*
Maryland Certification #: 322
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137*
Minnesota Dept ofAg Approval: via MN 027-053-137
Minnesota Petrofund Registration #: 1240*
Mississippi Certification #: MN00064
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
CERTIFICATIONS
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081*
New Jersey Certification #: MN002
New York Certification #: 11647*
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification (A2LA) #: R-036
North Dakota Certification (MN) #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification (1700) #: CL101
Ohio VAP Certification (1800) #: CL110*
Oklahoma Certification #: 9507*
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001*
Pennsylvania Certification #: 68-00563*
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192*
Utah Certification #: MN00064*
Vermont Certification #: VT-027053137
Virginia Certification #: 460163*
Washington Certification #: C486*
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A21-A 2926.01
USDA Permit #: P330-19-00208
*Please Note: Applicable air certifications are denoted with
an asterisk (*).
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: CRP.003
Pace Project No.: 92602305
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92602305001
92602305002
STOCK PILE-14
STOCK PILE-14C
Solid
Solid
05/03/22 11:10
05/03/22 11:10
05/03/22 13:22
05/03/22 13:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: CRP.003
Pace Project No.: 92602305
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92602305001 STOCKPILE-14
EPA 8081B
BAJ
24
PASI-C
EPA 6020E
RJS
7
PASI-M
EPA 7471 B
LMW
1
PASI-M
ASTM D2974
JDL
1
PASI-M
EPA 8270E
BPJ
75
PASI-C
SW-846
KDF
1
PASI-C
92602305002 STOCK PILE-14C
EPA 8260D
LMB
70
PASI-C
SW-846
KDF
1
PASI-C
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CRP.003
Pace Project No.: 92602305
Sample: STOCK PILE-14 Lab ID: 92602305001 Collected: 05/03/22 11:10 Received: 05/03/22 13:22 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Aldrin
ND
mg/kg
0.0025
0.0010
1
05/05/22 11:20
05/09/22 10:57
309-00-2
alpha-BHC
ND
mg/kg
0.0025
0.0011
1
05/05/22 11:20
05/09/22 10:57
319-84-6
beta-BHC
ND
mg/kg
0.0025
0.0012
1
05/05/22 11:20
05/09/22 10:57
319-85-7
delta-BHC
ND
mg/kg
0.0025
0.0012
1
05/05/22 11:20
05/09/22 10:57
319-86-8
gamma-BHC (Lindane)
ND
mg/kg
0.0025
0.0010
1
05/05/22 11:20
05/09/22 10:57
58-89-9
Chlordane (Technical)
ND
mg/kg
0.013
0.011
1
05/05/22 11:20
05/09/22 10:57
57-74-9
4,4'-DDD
ND
mg/kg
0.0025
0.0011
1
05/05/22 11:20
05/09/22 10:57
72-54-8
4,4'-DDE
ND
mg/kg
0.0025
0.0012
1
05/05/22 11:20
05/09/22 10:57
72-55-9
4,4'-DDT
ND
mg/kg
0.0025
0.0011
1
05/05/22 11:20
05/09/22 10:57
50-29-3
Dieldrin
ND
mg/kg
0.0025
0.0011
1
05/05/22 11:20
05/09/22 10:57
60-57-1
Endosulfan I
ND
mg/kg
0.0025
0.0011
1
05/05/22 11:20
05/09/22 10:57
959-98-8
Endosulfan 11
ND
mg/kg
0.0025
0.0011
1
05/05/22 11:20
05/09/22 10:57
33213-65-9
Endosulfan sulfate
ND
mg/kg
0.0025
0.0014
1
05/05/22 11:20
05/09/22 10:57
1031-07-8
Endrin
ND
mg/kg
0.0025
0.0012
1
05/05/22 11:20
05/09/22 10:57
72-20-8
Endrin aldehyde
ND
mg/kg
0.0025
0.0017
1
05/05/22 11:20
05/09/22 10:57
7421-93-4
Endrin ketone
ND
mg/kg
0.0025
0.0014
1
05/05/22 11:20
05/09/22 10:57
53494-70-5
Heptachlor
ND
mg/kg
0.0025
0.0012
1
05/05/22 11:20
05/09/22 10:57
76-44-8
Heptachlor epoxide
ND
mg/kg
0.0025
0.0010
1
05/05/22 11:20
05/09/22 10:57
1024-57-3
Hexachlorobenzene
ND
mg/kg
0.0025
0.0010
1
05/05/22 11:20
05/09/22 10:57
118-74-1
Methoxychlor
ND
mg/kg
0.0063
0.0031
1
05/05/22 11:20
05/09/22 10:57
72-43-5
Mirex
ND
mg/kg
0.0063
0.0028
1
05/05/22 11:20
05/09/22 10:57
2385-85-5
Toxaphene
ND
mg/kg
0.0088
0.0067
1
05/05/22 11:20
05/09/22 10:57
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
63
%
10-138
1
05/05/22 11:20
05/09/22 10:57
877-09-8
Decachlorobiphenyl (S)
64
%
10-150
1
05/05/22 11:20
05/09/22 10:57
2051-24-3
6020B MET ICPMS
Analytical
Method: EPA 6020E Preparation Method: EPA
3050B
Pace Analytical
Services - Minneapolis
Arsenic
3.4
mg/kg
0.63
0.14
1
05/06/2211:06
05/09/2211:38
7440-38-2
Barium
86.1
mg/kg
0.38
0.067
1
05/06/2211:06
05/09/2211:38
7440-39-3
Cadmium
0.103
mg/kg
0.10
0.040
1
05/06/2211:06
05/09/2211:38
7440-43-9
Chromium
23.4
mg/kg
2.5
0.18
1
05/06/2211:06
05/09/2211:38
7440-47-3
Lead
10.9
mg/kg
0.63
0.037
1
05/06/2211:06
05/09/2211:38
7439-92-1
Selenium
0.42J
mg/kg
0.63
0.11
1
05/06/2211:06
05/09/2211:38
7782-49-2
Silver
0.191
mg/kg
0.63
0.18
1
05/06/2211:06
05/09/2211:38
7440-22-4
7471 B Mercury
Analytical
Method: EPA 7471 B Preparation Method: EPA
7471 B
Pace Analytical
Services - Minneapolis
Mercury
0.012J
mg/kg
0.021
0.0092
1
05/06/2211:51
05/06/2213:07
7439-97-6
Dry Weight / %M by ASTM D2974
Analytical
Method: ASTM D2974
Pace Analytical
Services - Minneapolis
Percent Moisture
20.6
%
0.10
0.10
1
05/06/22 12:11
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CRP.003
Pace Project No.: 92602305
Sample: STOCK PILE-14
Lab ID:
92602305001
Collected:
05/03/22
11:10
Received: 05/03/22 13:22 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
83-32-9
Acenaphthylene
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
208-96-8
Aniline
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
62-53-3
Anthracene
ND
mg/kg
0.41
0.13
1
05/05/22 11:26
05/06/22 13:37
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
207-08-9
Benzoic Acid
ND
mg/kg
2.1
0.88
1
05/05/22 11:26
05/06/22 13:37
65-85-0
Benzyl alcohol
ND
mg/kg
0.82
0.31
1
05/05/22 11:26
05/06/22 13:37
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.41
0.17
1
05/05/22 11:26
05/06/22 13:37
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.82
0.29
1
05/05/22 11:26
05/06/22 13:37
59-50-7
4-Chloroaniline
ND
mg/kg
0.82
0.32
1
05/05/22 11:26
05/06/22 13:37
106-47-8 IL
bis(2-Chloroethoxy)methane
ND
mg/kg
0.41
0.17
1
05/05/22 11:26
05/06/22 13:37
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
91-58-7
2-Chlorophenol
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
7005-72-3
Chrysene
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
53-70-3
Dibenzofuran
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.82
0.28
1
05/05/22 11:26
05/06/22 13:37
91-94-1 IL
2,4-Dichlorophenol
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
120-83-2
Diethylphthalate
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.41
0.17
1
05/05/22 11:26
05/06/22 13:37
105-67-9
Dimethylphthalate
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.82
0.38
1
05/05/22 11:26
05/06/22 13:37
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.1
1.3
1
05/05/22 11:26
05/06/22 13:37
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
117-81-7
Fluoranthene
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
206-44-0
Fluorene
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.41
0.18
1
05/05/22 11:26
05/06/22 13:37
87-68-3
Hexachlorobenzene
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.41
0.24
1
05/05/22 11:26
05/06/22 13:37
77-47-4
Hexachloroethane
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
67-72-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CRP.003
Pace Project No.: 92602305
Sample: STOCK PILE-14
Lab ID:
92602305001
Collected:
05/03/22
11:10
Received: 05/03/22 13:22 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services
- Charlotte
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
193-39-5
Isophorone
ND
mg/kg
0.41
0.18
1
05/05/22 11:26
05/06/22 13:37
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.41
0.17
1
05/05/22 11:26
05/06/22 13:37
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.41
0.17
1
05/05/22 11:26
05/06/22 13:37
15831-10-4
Naphthalene
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
91-20-3
2-Nitroaniline
ND
mg/kg
2.1
0.34
1
05/05/22 11:26
05/06/22 13:37
88-74-4
3-Nitroaniline
ND
mg/kg
2.1
0.32
1
05/05/22 11:26
05/06/22 13:37
99-09-2 IL
4-Nitroaniline
ND
mg/kg
0.82
0.31
1
05/05/22 11:26
05/06/22 13:37
100-01-6
Nitrobenzene
ND
mg/kg
0.41
0.19
1
05/05/22 11:26
05/06/22 13:37
98-95-3
2-Nitrophenol
ND
mg/kg
0.41
0.18
1
05/05/22 11:26
05/06/22 13:37
88-75-5 v1
4-Nitrophenol
ND
mg/kg
2.1
0.79
1
05/05/22 11:26
05/06/22 13:37
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.41
0.14
1
05/05/22 11:26
05/06/22 13:37
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.41
0.15
1
05/05/22 11:26
05/06/22 13:37
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.41
0.20
1
05/05/22 11:26
05/06/22 13:37
108-60-1
Pentachlorophenol
ND
mg/kg
0.82
0.40
1
05/05/22 11:26
05/06/22 13:37
87-86-5
Phenanthrene
ND
mg/kg
0.41
0.13
1
05/05/22 11:26
05/06/22 13:37
85-01-8
Phenol
ND
mg/kg
0.41
0.18
1
05/05/22 11:26
05/06/22 13:37
108-95-2
Pyrene
ND
mg/kg
0.41
0.17
1
05/05/22 11:26
05/06/22 13:37
129-00-0
Pyridine
ND
mg/kg
0.41
0.13
1
05/05/22 11:26
05/06/22 13:37
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.41
0.16
1
05/05/22 11:26
05/06/22 13:37
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.41
0.19
1
05/05/22 11:26
05/06/22 13:37
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.41
0.17
1
05/05/22 11:26
05/06/22 13:37
88-06-2
Surrogates
Nitrobenzene-d5 (S)
68
%
21-130
1
05/05/22 11:26
05/06/22 13:37
4165-60-0
2-Fluorobiphenyl (S)
65
%
19-130
1
05/05/22 11:26
05/06/22 13:37
321-60-8
Terphenyl-d14 (S)
76
%
15-130
1
05/05/22 11:26
05/06/22 13:37
1718-51-0
Phenol-d6 (S)
69
%
18-130
1
05/05/22 11:26
05/06/22 13:37
13127-88-3
2-Fluorophenol (S)
64
%
18-130
1
05/05/22 11:26
05/06/22 13:37
367-12-4
2,4,6-Tribromophenol (S)
66
%
18-130
1
05/05/22 11:26
05/06/22 13:37
118-79-6
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
20.4
%
0.10
0.10
1
05/06/22 15:15
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CRP.003
Pace Project No.: 92602305
Sample: STOCK PILE-14C Lab ID: 92602305002 Collected: 05/03/22 11:10 Received: 05/03/22 13:22 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.12
0.038
1
05/05/22 15:50
05/05/22 17:06
67-64-1
Benzene
ND
mg/kg
0.0059
0.0024
1
05/05/22 15:50
05/05/22 17:06
71-43-2
Bromobenzene
ND
mg/kg
0.0059
0.0019
1
05/05/22 15:50
05/05/22 17:06
108-86-1
Bromochloromethane
ND
mg/kg
0.0059
0.0017
1
05/05/22 15:50
05/05/22 17:06
74-97-5
Bromodichloromethane
ND
mg/kg
0.0059
0.0023
1
05/05/22 15:50
05/05/22 17:06
75-27-4
Bromoform
ND
mg/kg
0.0059
0.0021
1
05/05/22 15:50
05/05/22 17:06
75-25-2
Bromomethane
ND
mg/kg
0.012
0.0093
1
05/05/22 15:50
05/05/22 17:06
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.12
0.028
1
05/05/22 15:50
05/05/22 17:06
78-93-3
n-Butylbenzene
ND
mg/kg
0.0059
0.0028
1
05/05/22 15:50
05/05/22 17:06
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0059
0.0026
1
05/05/22 15:50
05/05/22 17:06
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0059
0.0021
1
05/05/22 15:50
05/05/22 17:06
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0059
0.0022
1
05/05/22 15:50
05/05/22 17:06
56-23-5
Chlorobenzene
ND
mg/kg
0.0059
0.0011
1
05/05/22 15:50
05/05/22 17:06
108-90-7
Chloroethane
ND
mg/kg
0.012
0.0046
1
05/05/22 15:50
05/05/22 17:06
75-00-3
Chloroform
ND
mg/kg
0.0059
0.0036
1
05/05/22 15:50
05/05/22 17:06
67-66-3
Chloromethane
ND
mg/kg
0.012
0.0050
1
05/05/22 15:50
05/05/22 17:06
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0059
0.0021
1
05/05/22 15:50
05/05/22 17:06
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0059
0.0010
1
05/05/22 15:50
05/05/22 17:06
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0059
0.0023
1
05/05/22 15:50
05/05/22 17:06
96-12-8
Dibromochloromethane
ND
mg/kg
0.0059
0.0033
1
05/05/22 15:50
05/05/22 17:06
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0059
0.0026
1
05/05/22 15:50
05/05/22 17:06
106-93-4
Dibromomethane
ND
mg/kg
0.0059
0.0013
1
05/05/22 15:50
05/05/22 17:06
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0059
0.0021
1
05/05/22 15:50
05/05/22 17:06
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0059
0.0018
1
05/05/22 15:50
05/05/22 17:06
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0059
0.0015
1
05/05/22 15:50
05/05/22 17:06
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.012
0.0026
1
05/05/22 15:50
05/05/22 17:06
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0059
0.0024
1
05/05/22 15:50
05/05/22 17:06
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0059
0.0039
1
05/05/22 15:50
05/05/22 17:06
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0059
0.0024
1
05/05/22 15:50
05/05/22 17:06
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0059
0.0020
1
05/05/22 15:50
05/05/22 17:06
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0059
0.0021
1
05/05/22 15:50
05/05/22 17:06
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0059
0.0018
1
05/05/22 15:50
05/05/22 17:06
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0059
0.0018
1
05/05/22 15:50
05/05/22 17:06
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0059
0.0019
1
05/05/22 15:50
05/05/22 17:06
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0059
0.0028
1
05/05/22 15:50
05/05/22 17:06
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0059
0.0016
1
05/05/22 15:50
05/05/22 17:06
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0059
0.0020
1
05/05/22 15:50
05/05/22 17:06
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0059
0.0016
1
05/05/22 15:50
05/05/22 17:06
108-20-3
Ethylbenzene
ND
mg/kg
0.0059
0.0028
1
05/05/22 15:50
05/05/22 17:06
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.012
0.0097
1
05/05/22 15:50
05/05/22 17:06
87-68-3
2-Hexanone
ND
mg/kg
0.059
0.0057
1
05/05/22 15:50
05/05/22 17:06
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0059
0.0020
1
05/05/22 15:50
05/05/22 17:06
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0059
0.0029
1
05/05/22 15:50
05/05/22 17:06
99-87-6
Methylene Chloride
ND
mg/kg
0.024
0.016
1
05/05/22 15:50
05/05/22 17:06
75-09-2
REPORT OF LABORATORY ANALYSIS
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Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 35

leAnalyiical
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CRP.003
Pace Project No.: 92602305
Sample: STOCK PILE-14C
Lab ID:
92602305002
Collected:
05/03/22
11:10
Received: 05/03/22 13:22 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.059
0.0057
1
05/05/22 15:50
05/05/22 17:06
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0059
0.0022
1
05/05/22 15:50
05/05/22 17:06
1634-04-4
Naphthalene
ND
mg/kg
0.0059
0.0031
1
05/05/22 15:50
05/05/22 17:06
91-20-3
n-Propylbenzene
ND
mg/kg
0.0059
0.0021
1
05/05/22 15:50
05/05/22 17:06
103-65-1
Styrene
ND
mg/kg
0.0059
0.0016
1
05/05/22 15:50
05/05/22 17:06
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0059
0.0023
1
05/05/22 15:50
05/05/22 17:06
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0059
0.0016
1
05/05/22 15:50
05/05/22 17:06
79-34-5
Tetrachloroethene
ND
mg/kg
0.0059
0.0019
1
05/05/22 15:50
05/05/22 17:06
127-18-4
Toluene
ND
mg/kg
0.0059
0.0017
1
05/05/22 15:50
05/05/22 17:06
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0059
0.0048
1
05/05/22 15:50
05/05/22 17:06
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0059
0.0050
1
05/05/22 15:50
05/05/22 17:06
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0059
0.0031
1
05/05/22 15:50
05/05/22 17:06
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0059
0.0020
1
05/05/22 15:50
05/05/22 17:06
79-00-5
Trichloroethene
ND
mg/kg
0.0059
0.0015
1
05/05/22 15:50
05/05/22 17:06
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0059
0.0032
1
05/05/22 15:50
05/05/22 17:06
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0059
0.0030
1
05/05/22 15:50
05/05/22 17:06
96-18-4
1,2,4-Trimethylbenzene
ND
mg/kg
0.0059
0.0016
1
05/05/22 15:50
05/05/22 17:06
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0059
0.0020
1
05/05/22 15:50
05/05/22 17:06
108-67-8
Vinyl acetate
ND
mg/kg
0.059
0.0043
1
05/05/22 15:50
05/05/22 17:06
108-05-4
Vinyl chloride
ND
mg/kg
0.012
0.0030
1
05/05/22 15:50
05/05/22 17:06
75-01-4
Xylene (Total)
ND
mg/kg
0.012
0.0034
1
05/05/22 15:50
05/05/22 17:06
1330-20-7
m&p-Xylene
ND
mg/kg
0.012
0.0040
1
05/05/22 15:50
05/05/22 17:06
179601-23-1
o-Xylene
ND
mg/kg
0.0059
0.0026
1
05/05/22 15:50
05/05/22 17:06
95-47-6
Surrogates
Toluene-d8 (S)
98
%
70-130
1
05/05/22 15:50
05/05/22 17:06
2037-26-5
4-Bromofluorobenzene (S)
96
%
69-134
1
05/05/22 15:50
05/05/22 17:06
460-00-4
1,2-Dichloroethane-d4 (S)
89
%
70-130
1
05/05/22 15:50
05/05/22 17:06
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical Services
- Charlotte
Percent Moisture
19.1
%
0.10
0.10
1
05/06/22 15:17
N2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in
full,
Date: 05/10/2022 01:10 PM
without the written consent of Pace Analytical Services, LLC.
Page 9 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
QC Batch: 813630 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 B Mercury Solids
Laboratory: Pace Analytical Services - Minneapolis
Associated Lab Samples: 92602305001
METHOD BLANK: 4313711
Matrix:
Solid
Associated Lab Samples: 92602305001
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Mercury
mg/kg
0.0183
0.018
0.0080 05/06/2213:04
LABORATORY CONTROL SAMPLE:
4313712
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
mg/kg
0.46
0.49
107 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4313713 4313714
MS MSD
10607074001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury mg/kg ND 0.49 0.49 0.53 0.52 107 105 80-120 2 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: CRP.003
Pace Project No.: 92602305
QC Batch: 813561
QC Batch Method: EPA 3050B
Associated Lab Samples: 92602305001
QUALITY CONTROL DATA
Analysis Method: EPA 6020B
Analysis Description: 6020E Solids UPD5
Laboratory: Pace Analytical Services - Minneapolis
METHOD BLANK: 4313346
Matrix:
Solid
Associated Lab Samples: 92602305001
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Arsenic
mg/kg
0.473
0.47
0.10
05/09/2211:30
Barium
mg/kg
0.283
0.28
0.050
05/09/2211:30
Cadmium
mg/kg
0.0753
0.075
0.030
05/09/2211:30
Chromium
mg/kg
0.191
1.9
0.13
05/09/2211:30
Lead
mg/kg
0.473
0.47
0.028
05/09/2211:30
Selenium
mg/kg
0.473
0.47
0.081
05/09/2211:30
Silver
mg/kg
0.473
0.47
0.14
05/09/2211:30
LABORATORY CONTROL SAMPLE:
4313347
Parameter
Units
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Chromium
mg/kg
Lead
mg/kg
Selenium
mg/kg
Silver
mg/kg
Spike
LCS
LCS
% Rec
Conc.
Result
% Rec
Limits Qualifiers
48.5
44.2
91
80-120
48.5
43.1
89
80-120
48.5
43.8
90
80-120
48.5
46.3
95
80-120
48.5
44.8
92
80-120
48.5
48.3
99
80-120
24.3
22.3
92
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4313348
4313349
MS
MSD
92602305001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
mg/kg
3.4
62.4
62.4
60.1
58.2
91
88
75-125
3
20
Barium
mg/kg
86.1
62.4
62.4
161
159
121
117
75-125
2
20
Cadmium
mg/kg
0.103
62.4
62.4
58.9
57.2
94
92
75-125
3
20
Chromium
mg/kg
23.4
62.4
62.4
89.5
87.6
106
103
75-125
2
20
Lead
mg/kg
10.9
62.4
62.4
70.9
69.4
96
94
75-125
2
20
Selenium
mg/kg
0.42J
62.4
62.4
61.0
58.8
97
94
75-125
4
20
Silver
mg/kg
0.191
31.2
31.2
30.1
29.2
96
93
75-125
3
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
QC Batch: 813658 Analysis Method: ASTM D2974
QC Batch Method: ASTM D2974 Analysis Description: Dry Weight / %M by ASTM D2974
Laboratory: Pace Analytical Services - Minneapolis
Associated Lab Samples: 92602305001
SAMPLE DUPLICATE: 4313951
Parameter
Percent Moisture
SAMPLE DUPLICATE: 4313952
Parameter
Percent Moisture
92602305001 Dup
Units Result Result
20.6 19.7
10607223004 Dup
Units Result Result
% 15.3 18.2
Max
RPD RPD Qualifiers
4 30 N2
Max
RPD RPD Qualifiers
17 30 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 35

lacieAnalyfica('
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
QC Batch: 696369 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92602305002
METHOD BLANK: 3636800
Associated Lab Samples: 92602305002
Parameter
Units
Matrix: Solid
Blank Reporting
Result Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0019
05/05/22 16:13
1,1,1-Trichloroethane
mg/kg
ND
0.0050
0.0026
05/05/22 16:13
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0013
05/05/22 16:13
1,1,2-Trichloroethane
mg/kg
ND
0.0050
0.0017
05/05/22 16:13
1,1-Dichloroethane
mg/kg
ND
0.0050
0.0021
05/05/22 16:13
1,1-Dichloroethene
mg/kg
ND
0.0050
0.0021
05/05/22 16:13
1,1-Dichloropropene
mg/kg
ND
0.0050
0.0024
05/05/22 16:13
1,2,3-Trichlorobenzene
mg/kg
ND
0.0050
0.0040
05/05/22 16:13
1,2,3-Trichloropropane
mg/kg
ND
0.0050
0.0025
05/05/22 16:13
1,2,4-Trichlorobenzene
mg/kg
ND
0.0050
0.0042
05/05/22 16:13
1,2,4-Trimethyl benzene
mg/kg
ND
0.0050
0.0014
05/05/22 16:13
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0050
0.0019
05/05/22 16:13
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0050
0.0022
05/05/22 16:13
1,2-Dichlorobenzene
mg/kg
ND
0.0050
0.0018
05/05/22 16:13
1,2-Dichloroethane
mg/kg
ND
0.0050
0.0033
05/05/22 16:13
1,2-Dichloropropane
mg/kg
ND
0.0050
0.0015
05/05/22 16:13
1,3,5-Trimethyl benzene
mg/kg
ND
0.0050
0.0017
05/05/22 16:13
1,3-Dichlorobenzene
mg/kg
ND
0.0050
0.0016
05/05/22 16:13
1,3-Dichloropropane
mg/kg
ND
0.0050
0.0016
05/05/22 16:13
1,4-Dichlorobenzene
mg/kg
ND
0.0050
0.0013
05/05/22 16:13
2,2-Dichloropropane
mg/kg
ND
0.0050
0.0016
05/05/22 16:13
2-Butanone (MEK)
mg/kg
ND
0.10
0.024
05/05/22 16:13
2-Chlorotoluene
mg/kg
ND
0.0050
0.0018
05/05/22 16:13
2-Hexanone
mg/kg
ND
0.050
0.0048
05/05/22 16:13
4-Chlorotoluene
mg/kg
ND
0.0050
0.00088
05/05/22 16:13
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.050
0.0048
05/05/22 16:13
Acetone
mg/kg
ND
0.10
0.032
05/05/22 16:13
Benzene
mg/kg
ND
0.0050
0.0020
05/05/22 16:13
Bromobenzene
mg/kg
ND
0.0050
0.0016
05/05/22 16:13
Bromochloromethane
mg/kg
ND
0.0050
0.0015
05/05/22 16:13
Bromodichloromethane
mg/kg
ND
0.0050
0.0019
05/05/22 16:13
Bromoform
mg/kg
ND
0.0050
0.0018
05/05/22 16:13
Bromomethane
mg/kg
ND
0.010
0.0079
05/05/22 16:13
Carbon tetrachloride
mg/kg
ND
0.0050
0.0019
05/05/22 16:13
Chlorobenzene
mg/kg
ND
0.0050
0.00096
05/05/22 16:13
Chloroethane
mg/kg
ND
0.010
0.0039
05/05/22 16:13
Chloroform
mg/kg
ND
0.0050
0.0030
05/05/22 16:13
Chloromethane
mg/kg
ND
0.010
0.0042
05/05/22 16:13
cis- 1,2-Dichloroethene
mg/kg
ND
0.0050
0.0017
05/05/22 16:13
cis- 1,3-Dichloropropene
mg/kg
ND
0.0050
0.0014
05/05/22 16:13
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
METHOD BLANK: 3636800
Associated Lab Samples: 92602305002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromochloromethane
mg/kg
ND
0.0050
0.0028
05/05/22 16:13
Dibromomethane
mg/kg
ND
0.0050
0.0011
05/05/22 16:13
Dichlorodifluoromethane
mg/kg
ND
0.010
0.0022
05/05/22 16:13
Diisopropyl ether
mg/kg
ND
0.0050
0.0014
05/05/22 16:13
Ethylbenzene
mg/kg
ND
0.0050
0.0023
05/05/22 16:13
Hexachloro-1,3-butadiene
mg/kg
ND
0.010
0.0082
05/05/22 16:13
Isopropylbenzene (Cumene)
mg/kg
ND
0.0050
0.0017
05/05/22 16:13
m&p-Xylene
mg/kg
ND
0.010
0.0034
05/05/22 16:13
Methyl-tert-butyl ether
mg/kg
ND
0.0050
0.0019
05/05/22 16:13
Methylene Chloride
mg/kg
ND
0.020
0.014
05/05/22 16:13
n-Butylbenzene
mg/kg
ND
0.0050
0.0024
05/05/22 16:13
n-Propylbenzene
mg/kg
ND
0.0050
0.0018
05/05/22 16:13
Naphthalene
mg/kg
ND
0.0050
0.0026
05/05/22 16:13
o-Xylene
mg/kg
ND
0.0050
0.0022
05/05/22 16:13
p-Isopropyltoluene
mg/kg
ND
0.0050
0.0025
05/05/22 16:13
sec-Butylbenzene
mg/kg
ND
0.0050
0.0022
05/05/22 16:13
Styrene
mg/kg
ND
0.0050
0.0013
05/05/22 16:13
tert-Butyl benzene
mg/kg
ND
0.0050
0.0018
05/05/22 16:13
Tetrachloroethene
mg/kg
ND
0.0050
0.0016
05/05/22 16:13
Toluene
mg/kg
ND
0.0050
0.0014
05/05/22 16:13
trans-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0018
05/05/22 16:13
trans- 1,3-Dichloropropene
mg/kg
ND
0.0050
0.0017
05/05/22 16:13
Trichloroethene
mg/kg
ND
0.0050
0.0013
05/05/22 16:13
Trichlorofluoromethane
mg/kg
ND
0.0050
0.0028
05/05/22 16:13
Vinyl acetate
mg/kg
ND
0.050
0.0036
05/05/22 16:13
Vinyl chloride
mg/kg
ND
0.010
0.0025
05/05/22 16:13
Xylene (Total)
mg/kg
ND
0.010
0.0028
05/05/22 16:13
1,2-Dichloroethane-d4 (S)
%
92
70-130
05/05/22 16:13
4-Bromofluorobenzene (S)
%
96
69-134
05/05/22 16:13
Toluene-d8 (S)
%
98
70-130
05/05/22 16:13
Qualifiers
LABORATORY CONTROL SAMPLE:
3636801
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
1.2
1.3
101
70-130
1,1,1-Trichloroethane
mg/kg
1.2
1.2
94
70-130
1,1,2,2-Tetrachloroethane
mg/kg
1.2
1.1
89
70-130
1,1,2-Trichloroethane
mg/kg
1.2
1.2
98
70-130
1,1-Dichloroethane
mg/kg
1.2
1.1
88
70-130
1,1-Dichloroethene
mg/kg
1.2
1.1
91
70-130
1,1-Dichloropropene
mg/kg
1.2
1.2
97
70-130
1,2,3-Trichlorobenzene
mg/kg
1.2
1.3
101
65-130
1,2,3-Trichloropropane
mg/kg
1.2
1.1
92
70-130
1,2,4-Trichlorobenzene
mg/kg
1.2
1.3
101
68-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
LABORATORY CONTROL SAMPLE:
Parameter
3636801
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trimethylbenzene
mg/kg
1.2
1.2
97
70-130
1,2-Dibromo-3-chloropropane
mg/kg
1.2
1.2
98
70-130
1,2-Dibromoethane (EDB)
mg/kg
1.2
1.2
98
70-130
1,2-Dichlorobenzene
mg/kg
1.2
1.2
97
70-130
1,2-Dichloroethane
mg/kg
1.2
1.1
91
63-130
1,2-Dichloropropane
mg/kg
1.2
1.2
95
70-130
1,3,5-Trimethylbenzene
mg/kg
1.2
1.2
99
70-130
1,3-Dichlorobenzene
mg/kg
1.2
1.2
95
70-130
1,3-Dichloropropane
mg/kg
1.2
1.2
93
70-130
1,4-Dichlorobenzene
mg/kg
1.2
1.2
96
70-130
2,2-Dichloropropane
mg/kg
1.2
1.2
93
66-130
2-Butanone (MEK)
mg/kg
2.5
2.1
83
70-130
2-Chlorotoluene
mg/kg
1.2
1.2
93
70-130
2-Hexanone
mg/kg
2.5
2.1
85
70-130
4-Chlorotoluene
mg/kg
1.2
1.2
92
70-130
4-Methyl-2-pentanone (MIBK)
mg/kg
2.5
2.2
89
70-130
Acetone
mg/kg
2.5
1.9
76
69-130
Benzene
mg/kg
1.2
1.2
92
70-130
Bromobenzene
mg/kg
1.2
1.3
102
70-130
Bromochloromethane
mg/kg
1.2
1.3
101
70-130
Bromodichloromethane
mg/kg
1.2
1.3
100
69-130
Bromoform
mg/kg
1.2
1.3
107
70-130
Bromomethane
mg/kg
1.2
1.4
112
52-130
Carbon tetrachloride
mg/kg
1.2
1.3
102
70-130
Chlorobenzene
mg/kg
1.2
1.3
100
70-130
Chloroethane
mg/kg
1.2
1.5
119
65-130
Chloroform
mg/kg
1.2
1.2
94
70-130
Chloromethane
mg/kg
1.2
1.1
88
55-130
cis-1,2-Dichloroethene
mg/kg
1.2
1.2
93
70-130
cis-1,3-Dichloropropene
mg/kg
1.2
1.2
98
70-130
Dibromochloromethane
mg/kg
1.2
1.3
100
70-130
Dibromomethane
mg/kg
1.2
1.3
104
70-130
Dichlorodifluoromethane
mg/kg
1.2
1.2
98
45-156
Diisopropyl ether
mg/kg
1.2
1.1
85
70-130
Ethylbenzene
mg/kg
1.2
1.2
92
70-130
Hexachloro-1,3-butadiene
mg/kg
1.2
1.4
110
66-130
Isopropylbenzene (Cumene)
mg/kg
1.2
1.2
98
70-130
m&p-Xylene
mg/kg
2.5
2.4
98
70-130
Methyl-tert-butyl ether
mg/kg
1.2
1.1
87
70-130
Methylene Chloride
mg/kg
1.2
1.0
80
65-130
n-Butylbenzene
mg/kg
1.2
1.2
100
67-130
n-Propylbenzene
mg/kg
1.2
1.2
95
70-130
Naphthalene
mg/kg
1.2
1.2
99
70-130
o-Xylene
mg/kg
1.2
1.2
99
70-130
p-Isopropyltoluene
mg/kg
1.2
1.3
103
67-130
sec-Butylbenzene
mg/kg
1.2
1.2
97
69-130
Styrene
mg/kg
1.2
1.3
104
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
LABORATORY CONTROL SAMPLE:
Parameter
3636801
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
tert-Butyl benzene
mg/kg
1.2
1.1
92
67-130
Tetrachloroethene
mg/kg
1.2
1.1
90
70-130
Toluene
mg/kg
1.2
1.2
96
70-130
trans-1,2-Dichloroethene
mg/kg
1.2
1.1
91
70-130
trans- 1,3-Dichloropropene
mg/kg
1.2
1.2
96
68-130
Trichloroethene
mg/kg
1.2
1.3
103
70-130
Trichlorofluoromethane
mg/kg
1.2
1.4
110
70-130
Vinyl acetate
mg/kg
2.5
2.2
88
70-130
Vinyl chloride
mg/kg
1.2
1.4
109
61-130
Xylene (Total)
mg/kg
3.8
3.7
98
70-130
1,2-Dichloroethane-d4 (S)
%
85
70-130
4-Bromofluorobenzene (S)
%
96
69-134
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
Parameter
3636802
Units
92602305002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.59
0.64
108
70-131
1,1,1-Trichloroethane
mg/kg
ND
0.59
0.65
111
65-133
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.59
0.53
90
66-130
1,1,2-Trichloroethane
mg/kg
ND
0.59
0.61
103
66-133
1,1-Dichloroethane
mg/kg
ND
0.59
0.59
101
65-130
1,1-Dichloroethene
mg/kg
ND
0.59
0.62
105
10-158
1,1-Dichloropropene
mg/kg
ND
0.59
0.67
113
68-133
1,2,3-Trichlorobenzene
mg/kg
ND
0.59
0.61
103
27-138
1,2,3-Trichloropropane
mg/kg
ND
0.59
0.53
90
67-130
1,2,4-Trichlorobenzene
mg/kg
ND
0.59
0.67
113
51-134
1,2,4-Trimethylbenzene
mg/kg
ND
0.59
0.67
113
63-136
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.59
0.53
90
32-130
1,2-Dibromoethane (EDB)
mg/kg
ND
0.59
0.60
102
70-130
1,2-Dichlorobenzene
mg/kg
ND
0.59
0.64
109
69-130
1,2-Dichloroethane
mg/kg
ND
0.59
0.59
99
59-130
1,2-Dichloropropane
mg/kg
ND
0.59
0.65
109
70-130
1,3,5-Trimethylbenzene
mg/kg
ND
0.59
0.66
112
65-137
1,3-Dichlorobenzene
mg/kg
ND
0.59
0.64
108
70-130
1,3-Dichloropropane
mg/kg
ND
0.59
0.59
100
70-130
1,4-Dichlorobenzene
mg/kg
ND
0.59
0.64
108
68-130
2,2-Dichloropropane
mg/kg
ND
0.59
0.61
104
32-130
2-Butanone (MEK)
mg/kg
ND
1.2
0.92
78
10-136
2-Chlorotoluene
mg/kg
ND
0.59
0.60
102
69-141
2-Hexanone
mg/kg
ND
1.2
0.93
78
10-144
4-Chlorotoluene
mg/kg
ND
0.59
0.62
104
70-132
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
1.2
1.0
84
25-143
Acetone
mg/kg
ND
1.2
0.85
72
10-130
Benzene
mg/kg
ND
0.59
0.63
108
67-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
MATRIX SPIKE SAMPLE:
Parameter
3636802
Units
92602305002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Bromobenzene
mg/kg
ND
0.59
0.66
111
70-130
Bromochloromethane
mg/kg
ND
0.59
0.64
109
69-134
Bromodichloromethane
mg/kg
ND
0.59
0.62
104
64-130
Bromoform
mg/kg
ND
0.59
0.57
96
62-130
Bromomethane
mg/kg
ND
0.59
0.43
73
20-176
Carbon tetrachloride
mg/kg
ND
0.59
0.68
116
65-140
Chlorobenzene
mg/kg
ND
0.59
0.65
110
70-130
Chloroethane
mg/kg
ND
0.59
0.38
64
10-130
Chloroform
mg/kg
ND
0.59
0.62
105
63-130
Chloromethane
mg/kg
ND
0.59
0.59
100
58-130
cis-1,2-Dichloroethene
mg/kg
ND
0.59
0.62
106
66-130
cis-1,3-Dichloropropene
mg/kg
ND
0.59
0.63
106
67-130
Dibromochloromethane
mg/kg
ND
0.59
0.57
97
67-130
Dibromomethane
mg/kg
ND
0.59
0.65
109
63-131
Dichlorodifluoromethane
mg/kg
ND
0.59
0.65
110
44-180
Diisopropyl ether
mg/kg
ND
0.59
0.57
96
63-130
Ethylbenzene
mg/kg
ND
0.59
0.62
104
66-130
Hexachloro-1,3-butadiene
mg/kg
ND
0.59
0.78
132
64-150
Isopropylbenzene (Cumene)
mg/kg
ND
0.59
0.65
110
69-135
m&p-Xylene
mg/kg
ND
1.2
1.3
110
60-133
Methyl-tert-butyl ether
mg/kg
ND
0.59
0.56
94
65-130
Methylene Chloride
mg/kg
ND
0.59
0.50
85
61-130
n-Butylbenzene
mg/kg
ND
0.59
0.67
114
65-140
n-Propylbenzene
mg/kg
ND
0.59
0.64
108
67-140
Naphthalene
mg/kg
ND
0.59
0.60
102
15-145
o-Xylene
mg/kg
ND
0.59
0.66
111
66-133
p-Isopropyltoluene
mg/kg
ND
0.59
0.69
117
56-147
sec-Butylbenzene
mg/kg
ND
0.59
0.66
113
65-139
Styrene
mg/kg
ND
0.59
0.66
112
70-132
tert-Butyl benzene
mg/kg
ND
0.59
0.64
109
62-135
Tetrachloroethene
mg/kg
ND
0.59
0.62
105
70-135
Toluene
mg/kg
ND
0.59
0.65
110
67-130
trans-1,2-Dichloroethene
mg/kg
ND
0.59
0.62
105
69-130
trans- 1,3-Dichloropropene
mg/kg
ND
0.59
0.59
100
62-130
Trichloroethene
mg/kg
ND
0.59
0.70
119
70-135
Trichlorofluoromethane
mg/kg
ND
0.59
0.39
66
10-130
Vinyl acetate
mg/kg
ND
1.2
1.1
94
53-130
Vinyl chloride
mg/kg
ND
0.59
0.69
117
61-148
Xylene (Total)
mg/kg
ND
1.7
2.0
110
63-132
1,2-Dichloroethane-d4 (S)
%
88
70-130
4-Bromofluorobenzene (S)
%
93
69-134
Toluene-d8 (S)
%
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
SAMPLE DUPLICATE: 3636803
Parameter
Units
92602811002
Result
Dup
Result RPD
Max
RPD
1,1,1,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,1-Trichloroethane
mg/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,2-Trichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethene
mg/kg
ND
ND
30
1,1-Dichloropropene
mg/kg
ND
ND
30
1,2,3-Trichlorobenzene
mg/kg
ND
ND
30
1,2,3-Trichloropropane
mg/kg
ND
ND
30
1,2,4-Trichlorobenzene
mg/kg
ND
ND
30
1,2,4-Trimethylbenzene
mg/kg
ND
ND
30
1,2-Dibromo-3-chloropropane
mg/kg
ND
ND
30
1,2-Dibromoethane (EDB)
mg/kg
ND
ND
30
1,2-Dichlorobenzene
mg/kg
ND
ND
30
1,2-Dichloroethane
mg/kg
ND
ND
30
1,2-Dichloropropane
mg/kg
ND
ND
30
1,3,5-Trimethylbenzene
mg/kg
ND
ND
30
1,3-Dichlorobenzene
mg/kg
ND
ND
30
1,3-Dichloropropane
mg/kg
ND
ND
30
1,4-Dichlorobenzene
mg/kg
ND
ND
30
2,2-Dichloropropane
mg/kg
ND
ND
30
2-Butanone (MEK)
mg/kg
ND
ND
30
2-Chlorotoluene
mg/kg
ND
ND
30
2-Hexanone
mg/kg
ND
ND
30
4-Chlorotoluene
mg/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
ND
30
Acetone
mg/kg
ND
ND
30
Benzene
mg/kg
ND
ND
30
Bromobenzene
mg/kg
ND
ND
30
Bromochloromethane
mg/kg
ND
ND
30
Bromodichloromethane
mg/kg
ND
ND
30
Bromoform
mg/kg
ND
ND
30
Bromomethane
mg/kg
ND
ND
30
Carbon tetrachloride
mg/kg
ND
ND
30
Chlorobenzene
mg/kg
3.3J ug/kg
0.0029J
30
Chloroethane
mg/kg
ND
ND
30
Chloroform
mg/kg
ND
ND
30
Chloromethane
mg/kg
ND
ND
30
cis-1,2-Dichloroethene
mg/kg
ND
ND
30
cis-1,3-Dichloropropene
mg/kg
ND
ND
30
Dibromochloromethane
mg/kg
ND
ND
30
Dibromomethane
mg/kg
ND
ND
30
Dichlorodifluoromethane
mg/kg
ND
ND
30
Diisopropyl ether
mg/kg
ND
ND
30
Ethylbenzene
mg/kg
ND
ND
30
Hexachloro-1,3-butadiene
mg/kg
ND
ND
30
Isopropylbenzene (Cumene)
mg/kg
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
SAMPLE DUPLICATE: 3636803
Parameter
Units
92602811002
Result
Dup
Result
m&p-Xylene
mg/kg
ND
ND
Methyl-tert-butyl ether
mg/kg
ND
ND
Methylene Chloride
mg/kg
ND
ND
n-Butylbenzene
mg/kg
ND
ND
n-Propylbenzene
mg/kg
ND
ND
Naphthalene
mg/kg
ND
ND
o-Xylene
mg/kg
ND
0.0058J
p-Isopropyltoluene
mg/kg
ND
ND
sec-Butylbenzene
mg/kg
ND
ND
Styrene
mg/kg
ND
ND
tert-Butyl benzene
mg/kg
ND
ND
Tetrachloroethene
mg/kg
ND
ND
Toluene
mg/kg
ND
0.0038J
trans-1,2-Dichloroethene
mg/kg
ND
ND
trans- 1,3-Dichloropropene
mg/kg
ND
ND
Trichloroethene
mg/kg
ND
ND
Trichlorofluoromethane
mg/kg
ND
ND
Vinyl acetate
mg/kg
ND
ND
Vinyl chloride
mg/kg
ND
ND
Xylene (Total)
mg/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
91
88
4-Bromofluorobenzene (S)
%
96
96
Toluene-d8 (S)
%
98
99
Max
RPD RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
QC Batch: 696200 Analysis Method: EPA 8081 B
QC Batch Method: EPA 3546 Analysis Description: 8081 GCS Pesticides
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92602305001
METHOD BLANK: 3635915
Associated Lab Samples: 92602305001
Parameter
4,4'-DDD
4,4'-DDE
4,4'-DDT
Aldrin
alpha-BHC
beta-BHC
delta-BHC
Dieldrin
Endosulfan I
Endosulfan 11
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Methoxychlor
Mirex
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
Matrix: Solid
Units
Blank
Result
Reporting
Limit
MDL
Analyzed
mg/kg
ND
0.0020
0.00090
05/09/22
11:08
mg/kg
ND
0.0020
0.00093
05/09/22
11:08
mg/kg
ND
0.0020
0.00088
05/09/22
11:08
mg/kg
ND
0.0020
0.00080
05/09/22
11:08
mg/kg
ND
0.0020
0.00086
05/09/22
11:08
mg/kg
ND
0.0020
0.00095
05/09/22
11:08
mg/kg
ND
0.0020
0.00099
05/09/22
11:08
mg/kg
ND
0.0020
0.00086
05/09/22
11:08
mg/kg
ND
0.0020
0.00085
05/09/22
11:08
mg/kg
ND
0.0020
0.00090
05/09/22
11:08
mg/kg
ND
0.0020
0.0011
05/09/22
11:08
mg/kg
ND
0.0020
0.00092
05/09/22
11:08
mg/kg
ND
0.0020
0.0013
05/09/22
11:08
mg/kg
ND
0.0020
0.0011
05/09/22
11:08
mg/kg
ND
0.0020
0.00079
05/09/22
11:08
mg/kg
ND
0.0020
0.00091
05/09/22
11:08
mg/kg
ND
0.0020
0.00079
05/09/22
11:08
mg/kg
ND
0.0020
0.00082
05/09/22
11:08
mg/kg
ND
0.0050
0.0024
05/09/22
11:08
mg/kg
ND
0.0050
0.0022
05/09/22
11:08
%
99
10-150
05/09/22
11:08
%
84
10-138
05/09/22
11:08
LABORATORY CONTROL SAMPLE: 3635916
Qualifiers
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
mg/kg
0.0084
0.0083
98
57-139
4,4'-DDE
mg/kg
0.0084
0.0080
95
53-133
4,4'-DDT
mg/kg
0.0084
0.0083
98
56-142
Aldrin
mg/kg
0.0084
0.0072
86
47-130
alpha-BHC
mg/kg
0.0084
0.0072
86
48-132
beta-BHC
mg/kg
0.0084
0.0075
89
48-136
delta-BHC
mg/kg
0.0084
0.0079
93
48-130
Dieldrin
mg/kg
0.0084
0.0078
92
53-135
Endosulfan I
mg/kg
0.0084
0.0073
87
55-130
Endosulfan II
mg/kg
0.0084
0.0075
88
58-130
Endosulfan sulfate
mg/kg
0.0084
0.0077
92
59-133
Endrin
mg/kg
0.0084
0.0081
96
60-137
Endrin aldehyde
mg/kg
0.0084
0.0066
78
52-130
Results presented on
this page are in the units indicated
by the "Units"
column except
where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
LABORATORY CONTROL SAMPLE:
Parameter
3635916
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Endrin ketone
mg/kg
0.0084
0.0077
91
52-145
gamma-BHC (Lindane)
mg/kg
0.0084
0.0077
91
50-132
Heptachlor
mg/kg
0.0084
0.0073
87
47-130
Heptachlor epoxide
mg/kg
0.0084
0.0074
88
50-130
Hexachlorobenzene
mg/kg
0.0084
0.0072
86
40-130
Methoxychlor
mg/kg
0.025
0.024
94
58-139
Mirex
mg/kg
0.025
0.023
90
58-130
Decachlorobiphenyl (S)
%
106
10-150
Tetrachloro-m-xylene (S)
%
87
10-138
MATRIX SPIKE SAMPLE:
3635917
35713844056
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
mg/kg
0.91 U ug/kg
0.0083
0.0076
91
23-158
4,4'-DDE
mg/kg
0.95U ug/kg
0.0083
0.0076
91
15-157
4,4'-DDT
mg/kg
0.89U ug/kg
0.0083
0.0083
99
24-158
Aldrin
mg/kg
0.81 U ug/kg
0.0083
0.0070
84
15-151
alpha-BHC
mg/kg
0.87U ug/kg
0.0083
0.0072
86
18-143
beta-BHC
mg/kg
0.97U ug/kg
0.0083
0.0071
85
12-163
delta-BHC
mg/kg
1.OU ug/kg
0.0083
0.0075
89
17-143
Dieldrin
mg/kg
0.87U ug/kg
0.0083
0.0074
89
10-172
EndosulfanI
mg/kg
0.86U ug/kg
0.0083
0.0069
83
21-152
Endosulfan II
mg/kg
0.91U ug/kg
0.0083
0.0071
85
21-155
Endosulfan sulfate
mg/kg
1.1 U ug/kg
0.0083
0.0083
99
26-148
Endrin
mg/kg
0.94U ug/kg
0.0083
0.0077
92
22-163
Endrin aldehyde
mg/kg
1.3U ug/kg
0.0083
0.0065
78
22-145
Endrin ketone
mg/kg
1.1 U ug/kg
0.0083
0.0075
91
15-170
gamma-BHC (Lindane)
mg/kg
0.81U ug/kg
0.0083
0.0073
88
21-144
Heptachlor
mg/kg
0.93U ug/kg
0.0083
0.0071
85
15-149
Heptachlor epoxide
mg/kg
0.80U ug/kg
0.0083
0.0070
85
19-144
Hexachlorobenzene
mg/kg
0.83U ug/kg
0.0083
0.0069
83
22-134
Methoxychlor
mg/kg
2.5U ug/kg
0.025
0.024
94
26-155
Mirex
mg/kg
2.2U ug/kg
0.025
0.022
88
12-150
Decachlorobiphenyl (S)
%
81
10-150
Tetrachloro-m-xylene (S)
%
80
10-138
SAMPLE DUPLICATE: 3635918
35713844058
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
4,4'-DDD
mg/kg
4.5U ug/kg
ND
30
4,4'-DDE
mg/kg
4.7U ug/kg
ND
30
4,4'-DDT
mg/kg
4AU ug/kg
ND
30
Aldrin
mg/kg
4.OU ug/kg
ND
30
alpha-BHC
mg/kg
4.3U ug/kg
ND
30
Results presented on this
page are in the units
indicated by the "Units" column except where an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
SAMPLE DUPLICATE: 3635918
Parameter
Units
35713844058
Result
Dup
Result
beta-BHC
mg/kg
4.8U ug/kg
ND
Chlordane (Technical)
mg/kg
43AU ug/kg
ND
delta-BHC
mg/kg
5.OU ug/kg
ND
Dieldrin
mg/kg
4.3U ug/kg
ND
Endosulfan I
mg/kg
4.3U ug/kg
ND
Endosulfan II
mg/kg
4.5U ug/kg
ND
Endosulfan sulfate
mg/kg
5.6U ug/kg
ND
Endrin
mg/kg
4.7U ug/kg
ND
Endrin aldehyde
mg/kg
6.7U ug/kg
ND
Endrin ketone
mg/kg
5.5U ug/kg
ND
gamma-BHC (Lindane)
mg/kg
4.OU ug/kg
ND
Heptachlor
mg/kg
4.6U ug/kg
ND
Heptachlor epoxide
mg/kg
4.OU ug/kg
ND
Hexachlorobenzene
mg/kg
4.1U ug/kg
ND
Methoxychlor
mg/kg
12.2U ug/kg
ND
Mirex
mg/kg
11.0U ug/kg
ND
Toxaphene
mg/kg
26.7U ug/kg
ND
Decachlorobiphenyl (S)
%
92
85
Tetrachloro-m-xylene (S)
%
85
79
Max
RPD RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
QC Batch: 696196 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92602305001
METHOD BLANK: 3635897
Associated Lab Samples: 92602305001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
mg/kg
ND
0.33
0.13
05/06/22 08:18
1,2-Dichlorobenzene
mg/kg
ND
0.33
0.12
05/06/22 08:18
1,3-Dichlorobenzene
mg/kg
ND
0.33
0.12
05/06/22 08:18
1,4-Dichlorobenzene
mg/kg
ND
0.33
0.13
05/06/22 08:18
1-Methylnaphthalene
mg/kg
ND
0.33
0.12
05/06/22 08:18
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
0.33
0.16
05/06/22 08:18
2,4,5-Trichlorophenol
mg/kg
ND
0.33
0.15
05/06/22 08:18
2,4,6-Trichlorophenol
mg/kg
ND
0.33
0.14
05/06/22 08:18
2,4-Dichlorophenol
mg/kg
ND
0.33
0.13
05/06/22 08:18
2,4-Dimethylphenol
mg/kg
ND
0.33
0.14
05/06/22 08:18
2,4-Dinitrophenol
mg/kg
ND
1.7
1.0
05/06/22 08:18
2,4-Dinitrotoluene
mg/kg
ND
0.33
0.13
05/06/22 08:18
2,6-Dinitrotoluene
mg/kg
ND
0.33
0.12
05/06/22 08:18
2-Chloronaphthalene
mg/kg
ND
0.33
0.13
05/06/22 08:18
2-Chlorophenol
mg/kg
ND
0.33
0.13
05/06/22 08:18
2-Methylnaphthalene
mg/kg
ND
0.33
0.13
05/06/22 08:18
2-Methylphenol(o-Cresol)
mg/kg
ND
0.33
0.14
05/06/22 08:18
2-Nitroaniline
mg/kg
ND
1.7
0.27
05/06/22 08:18
2-Nitrophenol
mg/kg
ND
0.33
0.14
05/06/22 08:18
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
0.33
0.13
05/06/22 08:18
3,3'-Dichlorobenzidine
mg/kg
ND
0.67
0.23
05/06/22 08:18
3-Nitroaniline
mg/kg
ND
1.7
0.26
05/06/22 08:18
4,6-Dinitro-2-methyl phenol
mg/kg
ND
0.67
0.31
05/06/22 08:18
4-Bromophenylphenyl ether
mg/kg
ND
0.33
0.13
05/06/22 08:18
4-ChIoro-3-methyl phenol
mg/kg
ND
0.67
0.24
05/06/22 08:18
4-Chloroaniline
mg/kg
ND
0.67
0.26
05/06/22 08:18
4-Chlorophenylphenyl ether
mg/kg
ND
0.33
0.12
05/06/22 08:18
4-Nitroaniline
mg/kg
ND
0.67
0.25
05/06/22 08:18
4-Nitrophenol
mg/kg
ND
1.7
0.65
05/06/22 08:18
Acenaphthene
mg/kg
ND
0.33
0.12
05/06/22 08:18
Acenaphthylene
mg/kg
ND
0.33
0.12
05/06/22 08:18
Aniline
mg/kg
ND
0.33
0.13
05/06/22 08:18
Anthracene
mg/kg
ND
0.33
0.11
05/06/22 08:18
Benzo(a)anthracene
mg/kg
ND
0.33
0.11
05/06/22 08:18
Benzo(a)pyrene
mg/kg
ND
0.33
0.12
05/06/22 08:18
Benzo(b)fluoranthene
mg/kg
ND
0.33
0.11
05/06/22 08:18
Benzo(g,h,i)perylene
mg/kg
ND
0.33
0.13
05/06/22 08:18
Benzo(k)fluoranthene
mg/kg
ND
0.33
0.12
05/06/22 08:18
Benzoic Acid
mg/kg
ND
1.7
0.72
05/06/22 08:18
Benzyl alcohol
mg/kg
ND
0.67
0.25
05/06/22 08:18
v1
IL
IL
IL
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
METHOD BLANK: 3635897
Associated Lab Samples: 92602305001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
bis(2-Chloroethoxy)methane
mg/kg
ND
0.33
0.14
05/06/22 08:18
bis(2-Chloroethyl) ether
mg/kg
ND
0.33
0.13
05/06/22 08:18
bis(2-Ethylhexyl)phthalate
mg/kg
ND
0.33
0.13
05/06/22 08:18
Butylbenzylphthalate
mg/kg
ND
0.33
0.14
05/06/22 08:18
Chrysene
mg/kg
ND
0.33
0.12
05/06/22 08:18
Di-n-butylphthalate
mg/kg
ND
0.33
0.11
05/06/22 08:18
Di-n-octylphthalate
mg/kg
ND
0.33
0.13
05/06/22 08:18
Dibenz(a,h)anthracene
mg/kg
ND
0.33
0.13
05/06/22 08:18
Dibenzofuran
mg/kg
ND
0.33
0.12
05/06/22 08:18
Diethylphthalate
mg/kg
ND
0.33
0.12
05/06/22 08:18
Dimethylphthalate
mg/kg
ND
0.33
0.12
05/06/22 08:18
Fluoranthene
mg/kg
ND
0.33
0.11
05/06/22 08:18
Fluorene
mg/kg
ND
0.33
0.12
05/06/22 08:18
Hexachloro-1,3-butadiene
mg/kg
ND
0.33
0.14
05/06/22 08:18
Hexachlorobenzene
mg/kg
ND
0.33
0.13
05/06/22 08:18
Hexachlorocyclopentadiene
mg/kg
ND
0.33
0.19
05/06/22 08:18
Hexachloroethane
mg/kg
ND
0.33
0.13
05/06/22 08:18
Indeno(1,2,3-cd)pyrene
mg/kg
ND
0.33
0.13
05/06/22 08:18
Isophorone
mg/kg
ND
0.33
0.15
05/06/22 08:18
N-Nitroso-di-n-propylamine
mg/kg
ND
0.33
0.13
05/06/22 08:18
N-Nitrosodimethylamine
mg/kg
ND
0.33
0.11
05/06/22 08:18
N-Nitrosodiphenylamine
mg/kg
ND
0.33
0.12
05/06/22 08:18
Naphthalene
mg/kg
ND
0.33
0.11
05/06/22 08:18
Nitrobenzene
mg/kg
ND
0.33
0.16
05/06/22 08:18
Pentachlorophenol
mg/kg
ND
0.67
0.33
05/06/22 08:18
Phenanthrene
mg/kg
ND
0.33
0.11
05/06/22 08:18
Phenol
mg/kg
ND
0.33
0.15
05/06/22 08:18
Pyrene
mg/kg
ND
0.33
0.14
05/06/22 08:18
Pyridine
mg/kg
ND
0.33
0.11
05/06/22 08:18
2,4,6-Tribromophenol (S)
%
71
18-130
05/06/22 08:18
2-Fluorobiphenyl (S)
%
70
19-130
05/06/22 08:18
2-Fluorophenol (S)
%
70
18-130
05/06/22 08:18
Nitrobenzene-d5 (S)
%
73
21-130
05/06/22 08:18
Phenol-d6 (S)
%
73
18-130
05/06/22 08:18
Terphenyl-d14 (S)
%
88
15-130
05/06/22 08:18
Qualifiers
LABORATORY CONTROL SAMPLE:
3635898
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
1.7
1.4
80
47-130
1,2-Dichlorobenzene
mg/kg
1.7
1.3
74
49-130
1,3-Dichlorobenzene
mg/kg
1.7
1.3
75
48-130
1,4-Dichlorobenzene
mg/kg
1.7
1.3
75
49-130
1-Methylnaphthalene
mg/kg
1.7
1.4
83
54-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
LABORATORY CONTROL SAMPLE:
Parameter
3635898
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,2'-Oxybis(1-chloropropane)
mg/kg
1.7
1.2
69
38-130
2,4,5-Trichlorophenol
mg/kg
1.7
1.6
93
49-130
2,4,6-Trichlorophenol
mg/kg
1.7
1.6
95
50-130
2,4-Dichlorophenol
mg/kg
1.7
1.5
88
51-130
2,4-Dimethylphenol
mg/kg
1.7
1.4
86
53-130
2,4-Dinitrophenol
mg/kg
8.4
8.0
95
39-130
2,4-Dinitrotoluene
mg/kg
1.7
1.6
94
53-130
2,6-Dinitrotoluene
mg/kg
1.7
1.6
95
55-130
2-Chloronaphthalene
mg/kg
1.7
1.4
85
48-130
2-Chlorophenol
mg/kg
1.7
1.4
82
54-130
2-Methylnaphthalene
mg/kg
1.7
1.4
83
57-130
2-Methylphenol(o-Cresol)
mg/kg
1.7
1.3
80
50-130
2-Nitroaniline
mg/kg
3.4
2.6
76
49-130
2-Nitrophenol
mg/kg
1.7
1.7
103
50-130 v1
3&4-Methyl phenol (m&p Cresol)
mg/kg
1.7
1.4
84
50-130
3,3'-Dichlorobenzidine
mg/kg
3.4
2.5
75
47-130IL
3-Nitroaniline
mg/kg
3.4
2.7
81
45-130IL
4,6-Dinitro-2-methyl phenol
mg/kg
3.4
3.1
91
50-142
4-Bromophenylphenyl ether
mg/kg
1.7
1.5
91
55-130
4-ChIoro-3-methyl phenol
mg/kg
3.4
3.0
89
52-130
4-Chloroaniline
mg/kg
3.4
2.7
79
49-130IL
4-Chlorophenylphenyl ether
mg/kg
1.7
1.5
88
53-130
4-Nitroaniline
mg/kg
3.4
2.8
83
51-130
4-Nitrophenol
mg/kg
8.4
7.0
83
40-130
Acenaphthene
mg/kg
1.7
1.4
82
56-130
Acenaphthylene
mg/kg
1.7
1.5
87
58-130
Aniline
mg/kg
1.7
1.1
68
44-130
Anthracene
mg/kg
1.7
1.2
72
60-130
Benzo(a)anthracene
mg/kg
1.7
1.4
85
59-130
Benzo(a)pyrene
mg/kg
1.7
1.3
80
57-130
Benzo(b)fluoranthene
mg/kg
1.7
1.3
76
54-130
Benzo(g,h,i)perylene
mg/kg
1.7
1.4
80
59-130
Benzo(k)fluoranthene
mg/kg
1.7
1.3
78
54-130
Benzoic Acid
mg/kg
8.4
6.0
71
19-130
Benzyl alcohol
mg/kg
3.4
2.8
82
50-130
bis(2-Chloroethoxy)methane
mg/kg
1.7
1.4
81
55-130
bis(2-Chloroethyl) ether
mg/kg
1.7
1.2
74
53-130
bis(2-Ethylhexyl)phthalate
mg/kg
1.7
1.5
87
58-130
Butylbenzylphthalate
mg/kg
1.7
1.5
89
46-138
Chrysene
mg/kg
1.7
1.4
84
57-130
Di-n-butylphthalate
mg/kg
1.7
1.4
83
57-130
Di-n-octylphthalate
mg/kg
1.7
1.7
101
57-130
Dibenz(a,h)anthracene
mg/kg
1.7
1.4
80
60-130
Dibenzofuran
mg/kg
1.7
1.4
85
54-130
Diethylphthalate
mg/kg
1.7
1.5
86
55-130
Dimethylphthalate
mg/kg
1.7
1.5
89
57-130
Fluoranthene
mg/kg
1.7
1.4
85
57-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
LABORATORY CONTROL SAMPLE:
3635898
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Fluorene
mg/kg
1.7
1.4
84
56-130
Hexachloro-1,3-butadiene
mg/kg
1.7
1.4
86
41-130
Hexachlorobenzene
mg/kg
1.7
1.5
92
53-130
Hexachlorocyclopentadiene
mg/kg
1.7
1.4
85
23-130
Hexachloroethane
mg/kg
1.7
1.2
73
48-130
Indeno(1,2,3-cd)pyrene
mg/kg
1.7
1.4
81
61-130
Isophorone
mg/kg
1.7
1.3
77
49-130
N-Nitroso-di-n-propylamine
mg/kg
1.7
1.3
75
52-130
N-Nitrosodimethylamine
mg/kg
1.7
1.2
72
45-130
N-Nitrosodiphenylamine
mg/kg
1.7
1.3
76
56-130
Naphthalene
mg/kg
1.7
1.4
81
56-130
Nitrobenzene
mg/kg
1.7
1.3
79
50-130
Pentachlorophenol
mg/kg
3.4
2.9
85
33-130
Phenanthrene
mg/kg
1.7
1.4
80
60-130
Phenol
mg/kg
1.7
1.4
82
54-130
Pyrene
mg/kg
1.7
1.5
87
61-130
Pyridine
mg/kg
1.7
1.1
62
35-130
2,4,6-Tribromophenol (S)
%
94
18-130
2-Fluorobiphenyl (S)
%
83
19-130
2-Fluorophenol(S)
%
81
18-130
Nitrobenzene-d5 (S)
%
78
21-130
Phenol-d6 (S)
%
84
18-130
Terphenyl-d14 (S)
%
91
15-130
MATRIX SPIKE SAMPLE:
3635899
92602206001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
ND
1.9
1.3
71
22-130
1,2-Dichlorobenzene
mg/kg
ND
1.9
1.2
68
23-130
1,3-Dichlorobenzene
mg/kg
ND
1.9
1.3
68
26-130
1,4-Dichlorobenzene
mg/kg
ND
1.9
1.2
67
27-130
1-Methylnaphthalene
mg/kg
ND
1.9
1.4
76
30-130
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
1.9
1.2
63
30-130
2,4,5-Trichlorophenol
mg/kg
ND
1.9
1.5
80
26-130
2,4,6-Trichlorophenol
mg/kg
ND
1.9
1.5
79
23-130
2,4-Dichlorophenol
mg/kg
ND
1.9
1.5
79
29-130
2,4-Dimethylphenol
mg/kg
ND
1.9
1.4
78
13-130
2,4-Dinitrophenol
mg/kg
ND
9.2
4.2
46
10-131
2,4-Dinitrotoluene
mg/kg
ND
1.9
1.6
85
28-130
2,6-Dinitrotoluene
mg/kg
ND
1.9
1.5
82
36-130
2-Chloronaphthalene
mg/kg
ND
1.9
1.3
68
27-130
2-Chlorophenol
mg/kg
ND
1.9
1.4
75
29-130
2-Methylnaphthalene
mg/kg
ND
1.9
1.4
76
29-130
2-Methylphenol(o-Cresol)
mg/kg
ND
1.9
1.3
73
20-130
2-Nitroaniline
mg/kg
ND
3.7
2.5
67
29-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 35

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
MATRIX SPIKE SAMPLE:
3635899
92602206001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Nitrophenol
mg/kg
ND
1.9
1.7
91
26-130 v1
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
1.9
1.4
75
10-176
3,3'-Dichlorobenzidine
mg/kg
ND
3.7
2.7
72
15-130IL
3-Nitroaniline
mg/kg
ND
3.7
2.8
76
28-130IL
4,6-Dinitro-2-methyl phenol
mg/kg
ND
3.7
2.2
60
15-132
4-Bromophenylphenyl ether
mg/kg
ND
1.9
1.4
74
35-130
4-Chloro-3-methylphenol
mg/kg
ND
3.7
3.2
86
30-130
4-Chloroaniline
mg/kg
ND
3.7
2.6
71
28-130IL
4-Chlorophenylphenyl ether
mg/kg
ND
1.9
1.4
76
32-130
4-Nitroaniline
mg/kg
ND
3.7
2.8
77
30-130
4-Nitrophenol
mg/kg
ND
9.2
7.0
76
17-130
Acenaphthene
mg/kg
ND
1.9
1.3
73
29-130
Acenaphthylene
mg/kg
ND
1.9
1.4
73
31-130
Aniline
mg/kg
ND
1.9
1.1
61
10-130
Anthracene
mg/kg
ND
1.9
1.2
62
33-130
Benzo(a)anthracene
mg/kg
ND
1.9
1.7
86
32-130
Benzo(a)pyrene
mg/kg
ND
1.9
1.5
73
32-130
Benzo(b)fluoranthene
mg/kg
ND
1.9
1.6
77
33-130
Benzo(g,h,i)perylene
mg/kg
ND
1.9
1.3
66
28-130
Benzo(k)fluoranthene
mg/kg
ND
1.9
1.4
70
31-130
Benzoic Acid
mg/kg
ND
9.2
1.5J
16
10-130
Benzyl alcohol
mg/kg
ND
3.7
2.7
72
31-130
bis(2-Chloroethoxy)methane
mg/kg
ND
1.9
1.3
70
30-130
bis(2-Chloroethyl) ether
mg/kg
ND
1.9
1.2
67
68-130 M1
bis(2-Ethylhexyl)phthalate
mg/kg
ND
1.9
1.4
73
40-130
Butylbenzylphthalate
mg/kg
ND
1.9
1.4
74
40-130
Chrysene
mg/kg
ND
1.9
1.6
80
30-130
Di-n-butylphthalate
mg/kg
ND
1.9
1.3
71
41-130
Di-n-octylphthalate
mg/kg
ND
1.9
1.6
87
42-130
Dibenz(a,h)anthracene
mg/kg
ND
1.9
1.2
63
27-130
Dibenzofuran
mg/kg
ND
1.9
1.4
75
32-130
Diethylphthalate
mg/kg
ND
1.9
1.4
75
40-130
Dimethylphthalate
mg/kg
ND
1.9
1.4
75
37-130
Fluoranthene
mg/kg
ND
1.9
2.5
126
26-130
Fluorene
mg/kg
ND
1.9
1.4
77
31-130
Hexachloro-1,3-butadiene
mg/kg
ND
1.9
1.4
76
20-130
Hexachlorobenzene
mg/kg
ND
1.9
1.4
76
29-130
Hexachlorocyclopentadiene
mg/kg
ND
1.9
0.89
48
10-130
Hexachloroethane
mg/kg
ND
1.9
1.3
68
21-130
Indeno(1,2,3-cd)pyrene
mg/kg
ND
1.9
1.3
66
28-130
Isophorone
mg/kg
ND
1.9
1.3
68
32-130
N-Nitroso-di-n-propylamine
mg/kg
ND
1.9
1.2
66
31-130
N-Nitrosodimethylamine
mg/kg
ND
1.9
1.1
61
20-130
N-Nitrosodiphenylamine
mg/kg
ND
1.9
1.2
65
32-130
Naphthalene
mg/kg
ND
1.9
1.4
74
30-130
Nitrobenzene
mg/kg
ND
1.9
1.3
70
25-130
Pentachlorophenol
mg/kg
ND
3.7
2.8
75
10-130
Results presented on this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 35

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
MATRIX SPIKE SAMPLE:
Parameter
3635899
Units
92602206001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Phenanthrene
mg/kg
ND
1.9
1.9
96
34-130
Phenol
mg/kg
ND
1.9
1.4
74
14-130
Pyrene
mg/kg
ND
1.9
2.1
94
31-130
Pyridine
mg/kg
ND
1.9
1.0
55
10-130
2,4,6-Tribromophenol (S)
%
77
18-130
2-Fluorobiphenyl (S)
%
64
19-130
2-Fluorophenol (S)
%
70
18-130
Nitrobenzene-d5 (S)
%
67
21-130
Phenol-d6 (S)
%
73
18-130
Terphenyl-d14 (S)
%
70
15-130
SAMPLE DUPLICATE: 3635900
Parameter
Units
92602206002
Result
Dup
Result RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzene
mg/kg
ND
ND
30
1,2-Dichlorobenzene
mg/kg
ND
ND
30
1,3-Dichlorobenzene
mg/kg
ND
ND
30
1,4-Dichlorobenzene
mg/kg
ND
ND
30
1-Methylnaphthalene
mg/kg
ND
ND
30
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
ND
30
2,4,5-Trichlorophenol
mg/kg
ND
ND
30
2,4,6-Trichlorophenol
mg/kg
ND
ND
30
2,4-Dichlorophenol
mg/kg
ND
ND
30
2,4-Dimethylphenol
mg/kg
ND
ND
30
2,4-Dinitrophenol
mg/kg
ND
ND
30
2,4-Dinitrotoluene
mg/kg
ND
ND
30
2,6-Dinitrotoluene
mg/kg
ND
ND
30
2-Chloronaphthalene
mg/kg
ND
ND
30
2-Chlorophenol
mg/kg
ND
ND
30
2-Methylnaphthalene
mg/kg
ND
ND
30
2-Methylphenol(o-Cresol)
mg/kg
ND
ND
30
2-Nitroaniline
mg/kg
ND
ND
30
2-Nitrophenol
mg/kg
ND
ND
30 v1
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
ND
30
3,3'-Dichlorobenzidine
mg/kg
ND
ND
30 IL
3-Nitroaniline
mg/kg
ND
ND
30 IL
4,6-Dinitro-2-methyl phenol
mg/kg
ND
ND
30
4-Bromophenylphenyl ether
mg/kg
ND
ND
30
4-ChIoro-3-methyl phenol
mg/kg
ND
ND
30
4-Chloroaniline
mg/kg
ND
ND
30 IL
4-Chlorophenylphenyl ether
mg/kg
ND
ND
30
4-Nitroaniline
mg/kg
ND
ND
30
4-Nitrophenol
mg/kg
ND
ND
30
Acenaphthene
mg/kg
ND
ND
30
Acenaphthylene
mg/kg
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: CRP.003
Pace Project No.: 92602305
SAMPLE DUPLICATE: 3635900
Parameter
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
Units
92602206002 Dup
Result Result
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
%
62
%
59
60
%
62
63
%
83
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
60
59
61
64
66
68
Max
RPD RPD
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92602305
QC Batch: 696657 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92602305001, 92602305002
SAMPLE DUPLICATE: 3638104
92602305001
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Percent Moisture
%
20.4
20.0
2 25 N2
SAMPLE DUPLICATE: 3638105
92602811003
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Percent Moisture
%
17.2
16.1
6 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: CRP.003
Pace Project No.: 92602305
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/10/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
CRP.003
92602305
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92602305001
STOCK PILE-14
EPA 3546
696200
EPA 8081 B
696465
92602305001
STOCK PILE-14
EPA 3050B
813561
EPA 6020B
813698
92602305001
STOCK PILE-14
EPA 7471 B
813630
EPA 7471 B
813676
92602305001
STOCK PILE-14
ASTM D2974
813658
92602305001
STOCK PILE-14
EPA 3546
696196
EPA 8270E
696460
92602305002
STOCK PILE-14C
EPA 5035A/5030B
696369
EPA 8260D
696392
92602305001
STOCK PILE-14
SW-846
696657
92602305002
STOCK PILE-14C
SW-846
696657
Date: 05/10/2022 01:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 32 of 35

Document Name;
Document Revised: November. 15, 202!
s
JW
Sample Condition Upon Recet (SOUR}
Pa e 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.0411
Pace Caroltnas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville ❑ Ra1e1gh[3"1Mechanicsvl11e❑ Atlanta[] Kernersvillte❑
Client Name:Upon Receipt Project #•Wo : 92602345
/�
Courier. ❑Fed Ex ❑lFPS ❑LISPS ocilent
❑ Commercial ❑Pace ,.� ❑Other:
Custody Seal Present? ❑E,Yes No Seals Intact? QYes No SZ602'305 }},,
Date/InkialsPenfln EYaminingContents(•.3.
Packing Material: ❑Bumble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: []Yes []No ENTA
❑ IR Gun ID: �� 6js ❑Wet []Blue []None
Type of Ice:
Q C� Correction Factor.
Cooler Temp: ems-- 9 — Add/Subtract ('C) d • 0 Temp should be above freezing to VC
[]Samples outof temp criteria. Samples on ice, cooling process
Cooler Temp Corrected ('C ; (� , c7 has begun
USDA Regulated Soil (PN/A, water sample)
Did samples orl ate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationally,
1.,__ � 1-1-11-14awaii and Puerto Ricol? r1VPs P-ma—
u•
-
Comments/Dtscrepa ncy:
Chain of Custody Present?
es
[]No
EINLA
i.
Samples Arrived within Hold Time?
Efy,
EIN.
❑N/A
2.
Short Hold Time Ana is (02 hr.)?
Yes
eTNo
NIA
3.
Rush Turn Around Time Requested?
Elyes
[JNo
NIA
4.
Sufficient Volume?
No
❑N/A
5.
Correct Contal ners Used?
-Pace Containers Used?
,Yes
es
PY6
❑No
[]No
❑N/A
N/A
6.
Containers Intact?
No
❑N/A
7.
Dissolved analysis. Samples Fteid Fiitered7
[]Yes
❑No
/A
8.
Sample labels Klatch CDC?
-Includes Date/Prnr/ID/Anal sis Matrk
r2M
❑No
❑N/A
9.
Headspace in VOA Vlals >5-6mm)?
[]Yes
QNo
ON/A
10.
Trip Stank Present?
Trip Blank Custody Seals Present?
❑Yes
Yes
❑No
Na
[]NIA
N A
!L
COMMENTS/SAMPLE DISCREPANCY Field Data Required? Des ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Date/Tlrne:
Project Meneger SCURF Review:
Project Manager SRF Review.
Date: _ I
I !
Date: }
i s
i .
Page 33 of 35

Document Name.
Sample Condition Upon Free
Document No.:
*Check mark top haif.of box if PH and/or dechlorination is
verified and within the acceptance range for preservation
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Eneptlom: VOA, Conform, TOC, OA and Grease, DRO/8015 {water} DOC, LLHg
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Page 34 of 35

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Page 35 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 14, 2022
Justin Ballard
Hart & Hickman
3921 Sunset Ridge Rd.
Suite 301
Raleigh, NC 27607
RE: Project: CRP.003
Pace Project No.: 92623549
Dear Justin Ballard:
Enclosed are the analytical results for sample(s) received by the laboratory on September 01, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Gulf Coast
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
1(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 33

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: CRP.003
Pace Project No.: 92623549
Pace Analytical Gulf Coast
7979 Innovation Park Drive, Baton Rouge, LA 70820
Arkansas Certification #: 88-0655
DoD ELAP Certification #: 6429-01
Florida Certification #: E87854
Illinois Certification #: 004585
Kansas Certification #: E-10354
Louisiana/LELAP Certification #: 01955
North Carolina Certification #: 618
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
CERTIFICATIONS
North Dakota Certification #: R-195
Oklahoma Certification #: 2019-101
South Carolina Certification #: 73006001
Texas Certification #: T104704178-19-11
USDA Soil Permit # P330-19-00209
Virginia Certification #: 460215
Washington Certification #: C929
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: CRP.003
Pace Project No.: 92623549
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92623549001
92623549002
Stock Pile-15
Stock Pile-1513
Solid
Solid
08/31/22 14:10
08/31/22 14:10
09/01/22 10:45
09/01/22 10:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: CRP.003
Pace Project No.: 92623549
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92623549001 Stock Pile-15
EPA 8081 B
SEM
24
PASI-C
EPA 6020E
LWZ
7
GCLA
EPA 7471 B
LWZ
1
GCLA
EPA 8270E
BPJ
75
PASI-C
SW-846
KDF
1
PASI-C
92623549002 Stock Pile-1513
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
GCLA = Pace Analytical Gulf Coast
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CRP.003
Pace Project No.: 92623549
Sample: Stock Pile-15 Lab ID: 92623549001 Collected: 08/31/22 14:10 Received: 09/01/22 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Aldrin
ND
mg/kg
0.0024
0.00096
1
09/07/22 16:04
09/08/22 09:41
309-00-2
alpha-BHC
ND
mg/kg
0.0024
0.0010
1
09/07/22 16:04
09/08/22 09:41
319-84-6
beta-BHC
ND
mg/kg
0.0024
0.0011
1
09/07/22 16:04
09/08/22 09:41
319-85-7
delta-BHC
ND
mg/kg
0.0024
0.0012
1
09/07/22 16:04
09/08/22 09:41
319-86-8
gamma-BHC (Lindane)
ND
mg/kg
0.0024
0.00095
1
09/07/22 16:04
09/08/22 09:41
58-89-9
Chlordane (Technical)
ND
mg/kg
0.012
0.010
1
09/07/22 16:04
09/08/22 09:41
57-74-9
4,4'-DDD
ND
mg/kg
0.0024
0.0011
1
09/07/22 16:04
09/08/22 09:41
72-54-8
4,4'-DDE
0.024
mg/kg
0.0024
0.0011
1
09/07/22 16:04
09/08/22 09:41
72-55-9
4,4'-DDT
ND
mg/kg
0.0024
0.0011
1
09/07/22 16:04
09/08/22 09:41
50-29-3
Dieldrin
ND
mg/kg
0.0024
0.0010
1
09/07/22 16:04
09/08/22 09:41
60-57-1
Endosulfan I
ND
mg/kg
0.0024
0.0010
1
09/07/22 16:04
09/08/22 09:41
959-98-8
Endosulfan 11
ND
mg/kg
0.0024
0.0011
1
09/07/22 16:04
09/08/22 09:41
33213-65-9
Endosulfan sulfate
ND
mg/kg
0.0024
0.0013
1
09/07/22 16:04
09/08/22 09:41
1031-07-8
Endrin
ND
mg/kg
0.0024
0.0011
1
09/07/22 16:04
09/08/22 09:41
72-20-8
Endrin aldehyde
ND
mg/kg
0.0024
0.0016
1
09/07/22 16:04
09/08/22 09:41
7421-93-4
Endrin ketone
ND
mg/kg
0.0024
0.0013
1
09/07/22 16:04
09/08/22 09:41
53494-70-5
Heptachlor
ND
mg/kg
0.0024
0.0011
1
09/07/22 16:04
09/08/22 09:41
76-44-8
Heptachlor epoxide
ND
mg/kg
0.0024
0.00094
1
09/07/22 16:04
09/08/22 09:41
1024-57-3
Hexachlorobenzene
ND
mg/kg
0.0024
0.00098
1
09/07/22 16:04
09/08/22 09:41
118-74-1
Methoxychlor
ND
mg/kg
0.0059
0.0029
1
09/07/22 16:04
09/08/22 09:41
72-43-5
Mirex
ND
mg/kg
0.0059
0.0026
1
09/07/22 16:04
09/08/22 09:41
2385-85-5
Toxaphene
ND
mg/kg
0.0083
0.0063
1
09/07/22 16:04
09/08/22 09:41
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
73
%
10-133
1
09/07/22 16:04
09/08/22 09:41
877-09-8
Decachlorobiphenyl (S)
78
%
10-146
1
09/07/22 16:04
09/08/22 09:41
2051-24-3
EPA 6020B
Analytical
Method: EPA 6020E Preparation Method: EPA 3050B
Pace Analytical
Gulf Coast
Arsenic
1.64
mg/kg
0.54
0.14
10
09/06/22 09:15
09/07/22 19:05
7440-38-2
Barium
68.2
mg/kg
0.54
0.14
10
09/06/22 09:15
09/07/22 19:05
7440-39-3
Cadmium
ND
mg/kg
0.54
0.14
10
09/06/22 09:15
09/07/22 19:05
7440-43-9
Chromium
21.3
mg/kg
0.54
0.14
10
09/06/22 09:15
09/07/22 19:05
7440-47-3
Lead
11.2
mg/kg
0.54
0.14
10
09/06/22 09:15
09/07/22 19:05
7439-92-1
Selenium
ND
mg/kg
0.54
0.14
10
09/06/22 09:15
09/07/22 19:05
7782-49-2
Silver
0.15J
mg/kg
0.54
0.14
10
09/06/22 09:15
09/07/22 19:05
7440-22-4
EPA 7471 B
Analytical
Method: EPA 7471 B Preparation Method:
METHOD
Pace Analytical
Gulf Coast
Mercury
0.089
mg/kg
0.015
0.0059
1
09/03/2214:15
09/07/2211:52
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method:
EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
0.39
0.14
1
09/07/2213:28
09/08/2210:59
83-32-9
Acenaphthylene
ND
mg/kg
0.39
0.14
1
09/07/2213:28
09/08/2210:59
208-96-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CRP.003
Pace Project No.: 92623549
Sample: Stock Pile-15 Lab ID: 92623549001 Collected: 08/31/22 14:10 Received: 09/01/22 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Aniline
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
62-53-3
Anthracene
ND
mg/kg
0.39
0.13
1
09/07/22 13:28
09/08/22 10:59
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.39
0.13
1
09/07/22 13:28
09/08/22 10:59
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.39
0.13
1
09/07/22 13:28
09/08/22 10:59
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.39
0.13
1
09/07/22 13:28
09/08/22 10:59
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.39
0.14
1
09/07/22 13:28
09/08/22 10:59
207-08-9
Benzoic Acid
ND
mg/kg
1.9
0.84
1
09/07/22 13:28
09/08/22 10:59
65-85-0
Benzyl alcohol
ND
mg/kg
0.78
0.29
1
09/07/22 13:28
09/08/22 10:59
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.39
0.16
1
09/07/22 13:28
09/08/22 10:59
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.78
0.27
1
09/07/22 13:28
09/08/22 10:59
59-50-7
4-Chloroaniline
ND
mg/kg
0.78
0.31
1
09/07/22 13:28
09/08/22 10:59
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.39
0.16
1
09/07/22 13:28
09/08/22 10:59
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
91-58-7
2-Chlorophenol
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
7005-72-3
Chrysene
ND
mg/kg
0.39
0.14
1
09/07/22 13:28
09/08/22 10:59
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
53-70-3
Dibenzofuran
ND
mg/kg
0.39
0.14
1
09/07/22 13:28
09/08/22 10:59
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.39
0.14
1
09/07/22 13:28
09/08/22 10:59
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.39
0.14
1
09/07/22 13:28
09/08/22 10:59
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.78
0.26
1
09/07/22 13:28
09/08/22 10:59
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
120-83-2
Diethylphthalate
ND
mg/kg
0.39
0.14
1
09/07/22 13:28
09/08/22 10:59
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.39
0.16
1
09/07/22 13:28
09/08/22 10:59
105-67-9
Dimethylphthalate
ND
mg/kg
0.39
0.14
1
09/07/22 13:28
09/08/22 10:59
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.39
0.13
1
09/07/22 13:28
09/08/22 10:59
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.78
0.36
1
09/07/22 13:28
09/08/22 10:59
534-52-1
2,4-Dinitrophenol
ND
mg/kg
1.9
1.2
1
09/07/22 13:28
09/08/22 10:59
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.39
0.14
1
09/07/22 13:28
09/08/22 10:59
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
117-81-7
Fluoranthene
ND
mg/kg
0.39
0.13
1
09/07/22 13:28
09/08/22 10:59
206-44-0
Fluorene
ND
mg/kg
0.39
0.14
1
09/07/22 13:28
09/08/22 10:59
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.39
0.17
1
09/07/22 13:28
09/08/22 10:59
87-68-3
Hexachlorobenzene
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.39
0.22
1
09/07/22 13:28
09/08/22 10:59
77-47-4
Hexachloroethane
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
193-39-5
Isophorone
ND
mg/kg
0.39
0.17
1
09/07/22 13:28
09/08/22 10:59
78-59-1
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC.
Page 6 of 33

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CRP.003
Pace Project No.: 92623549
Sample: Stock Pile-15
Lab ID:
92623549001
Collected:
08/31/22
14:10
Received: 09/01/22 10:45 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services
- Charlotte
1-Methylnaphthalene
ND
mg/kg
0.39
0.14
1
09/07/22 13:28
09/08/22 10:59
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.39
0.16
1
09/07/22 13:28
09/08/22 10:59
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.39
0.16
1
09/07/22 13:28
09/08/22 10:59
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.39
0.16
1
09/07/22 13:28
09/08/22 10:59
15831-10-4
Naphthalene
ND
mg/kg
0.39
0.13
1
09/07/22 13:28
09/08/22 10:59
91-20-3
2-Nitroaniline
ND
mg/kg
1.9
0.32
1
09/07/22 13:28
09/08/22 10:59
88-74-4
3-Nitroaniline
ND
mg/kg
1.9
0.31
1
09/07/22 13:28
09/08/22 10:59
99-09-2
4-Nitroaniline
ND
mg/kg
0.78
0.30
1
09/07/22 13:28
09/08/22 10:59
100-01-6
Nitrobenzene
ND
mg/kg
0.39
0.18
1
09/07/22 13:28
09/08/22 10:59
98-95-3
2-Nitrophenol
ND
mg/kg
0.39
0.17
1
09/07/22 13:28
09/08/22 10:59
88-75-5
4-Nitrophenol
ND
mg/kg
1.9
0.75
1
09/07/22 13:28
09/08/22 10:59
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.39
0.13
1
09/07/22 13:28
09/08/22 10:59
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.39
0.14
1
09/07/22 13:28
09/08/22 10:59
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.39
0.19
1
09/07/22 13:28
09/08/22 10:59
108-60-1
Pentachlorophenol
ND
mg/kg
0.78
0.38
1
09/07/22 13:28
09/08/22 10:59
87-86-5
Phenanthrene
ND
mg/kg
0.39
0.13
1
09/07/22 13:28
09/08/22 10:59
85-01-8
Phenol
ND
mg/kg
0.39
0.17
1
09/07/22 13:28
09/08/22 10:59
108-95-2
Pyrene
ND
mg/kg
0.39
0.16
1
09/07/22 13:28
09/08/22 10:59
129-00-0
Pyridine
ND
mg/kg
0.39
0.12
1
09/07/22 13:28
09/08/22 10:59
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.39
0.15
1
09/07/22 13:28
09/08/22 10:59
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.39
0.18
1
09/07/22 13:28
09/08/22 10:59
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.39
0.16
1
09/07/22 13:28
09/08/22 10:59
88-06-2
Surrogates
Nitrobenzene-d5 (S)
63
%
10-130
1
09/07/22 13:28
09/08/22 10:59
4165-60-0
2-Fluorobiphenyl (S)
58
%
10-130
1
09/07/22 13:28
09/08/22 10:59
321-60-8
Terphenyl-d14 (S)
81
%
10-130
1
09/07/22 13:28
09/08/22 10:59
1718-51-0
Phenol-d6 (S)
62
%
10-130
1
09/07/22 13:28
09/08/22 10:59
13127-88-3
2-Fluorophenol (S)
62
%
10-130
1
09/07/22 13:28
09/08/22 10:59
367-12-4
2,4,6-Tribromophenol (S)
73
%
10-131
1
09/07/22 13:28
09/08/22 10:59
118-79-6
Percent Moisture
Analytical
Method: SW-846
Pace Analytical Services
- Charlotte
Percent Moisture
14.9
%
0.10
0.10
1
09/07/22 17:11
N2
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM
without the written
consent of Pace Analytical Services, LLC.
Page 7 of 33

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CRP.003
Pace Project No.: 92623549
Sample: Stock Pile-15B
Lab ID:
92623549002
Collected:
08/31/22
14:10
Received: 09/01/22 10:45 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
Acetone
ND
mg/kg
0.11
0.035
1
09/06/22 15:20
09/08/22 05:37
67-64-1
Benzene
ND
mg/kg
0.0054
0.0022
1
09/06/22 15:20
09/08/22 05:37
71-43-2
Bromobenzene
ND
mg/kg
0.0054
0.0018
1
09/06/22 15:20
09/08/22 05:37
108-86-1
Bromochloromethane
ND
mg/kg
0.0054
0.0016
1
09/06/22 15:20
09/08/22 05:37
74-97-5
Bromodichloromethane
ND
mg/kg
0.0054
0.0021
1
09/06/22 15:20
09/08/22 05:37
75-27-4
Bromoform
ND
mg/kg
0.0054
0.0019
1
09/06/22 15:20
09/08/22 05:37
75-25-2
Bromomethane
ND
mg/kg
0.011
0.0086
1
09/06/22 15:20
09/08/22 05:37
74-83-9 IK
2-Butanone (MEK)
ND
mg/kg
0.11
0.026
1
09/06/22 15:20
09/08/22 05:37
78-93-3
n-Butylbenzene
ND
mg/kg
0.0054
0.0026
1
09/06/22 15:20
09/08/22 05:37
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0054
0.0024
1
09/06/22 15:20
09/08/22 05:37
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0054
0.0019
1
09/06/22 15:20
09/08/22 05:37
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0054
0.0020
1
09/06/22 15:20
09/08/22 05:37
56-23-5
Chlorobenzene
0.0033J
mg/kg
0.0054
0.0010
1
09/06/22 15:20
09/08/22 05:37
108-90-7
Chloroethane
ND
mg/kg
0.011
0.0042
1
09/06/22 15:20
09/08/22 05:37
75-00-3
Chloroform
ND
mg/kg
0.0054
0.0033
1
09/06/22 15:20
09/08/22 05:37
67-66-3
Chloromethane
ND
mg/kg
0.011
0.0046
1
09/06/22 15:20
09/08/22 05:37
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0054
0.0019
1
09/06/22 15:20
09/08/22 05:37
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0054
0.00096
1
09/06/22 15:20
09/08/22 05:37
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0054
0.0021
1
09/06/22 15:20
09/08/22 05:37
96-12-8
Dibromochloromethane
ND
mg/kg
0.0054
0.0030
1
09/06/22 15:20
09/08/22 05:37
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0054
0.0024
1
09/06/22 15:20
09/08/22 05:37
106-93-4
Dibromomethane
ND
mg/kg
0.0054
0.0012
1
09/06/22 15:20
09/08/22 05:37
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0054
0.0020
1
09/06/22 15:20
09/08/22 05:37
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0054
0.0017
1
09/06/22 15:20
09/08/22 05:37
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0054
0.0014
1
09/06/22 15:20
09/08/22 05:37
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.011
0.0024
1
09/06/22 15:20
09/08/22 05:37
75-71-8 IK
1,1-Dichloroethane
ND
mg/kg
0.0054
0.0022
1
09/06/22 15:20
09/08/22 05:37
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0054
0.0036
1
09/06/22 15:20
09/08/22 05:37
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0054
0.0022
1
09/06/22 15:20
09/08/22 05:37
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0054
0.0019
1
09/06/22 15:20
09/08/22 05:37
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0054
0.0019
1
09/06/22 15:20
09/08/22 05:37
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0054
0.0016
1
09/06/22 15:20
09/08/22 05:37
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0054
0.0017
1
09/06/22 15:20
09/08/22 05:37
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0054
0.0018
1
09/06/22 15:20
09/08/22 05:37
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0054
0.0026
1
09/06/22 15:20
09/08/22 05:37
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0054
0.0015
1
09/06/22 15:20
09/08/22 05:37
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0054
0.0019
1
09/06/22 15:20
09/08/22 05:37
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0054
0.0015
1
09/06/22 15:20
09/08/22 05:37
108-20-3
Ethylbenzene
0.0035J
mg/kg
0.0054
0.0025
1
09/06/22 15:20
09/08/22 05:37
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.011
0.0089
1
09/06/22 15:20
09/08/22 05:37
87-68-3
2-Hexanone
ND
mg/kg
0.054
0.0052
1
09/06/22 15:20
09/08/22 05:37
591-78-6
Isopropylbenzene (Cumene)
0.0027J
mg/kg
0.0054
0.0018
1
09/06/22 15:20
09/08/22 05:37
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0054
0.0027
1
09/06/22 15:20
09/08/22 05:37
99-87-6
Methylene Chloride
ND
mg/kg
0.022
0.015
1
09/06/22 15:20
09/08/22 05:37
75-09-2 IK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 33

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CRP.003
Pace Project No.: 92623549
Sample: Stock Pile-1513
Lab ID:
92623549002
Collected:
08/31/22
14:10
Received: 09/01/22 10:45 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.054
0.0052
1
09/06/22 15:20
09/08/22 05:37
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0054
0.0020
1
09/06/22 15:20
09/08/22 05:37
1634-04-4
Naphthalene
ND
mg/kg
0.0054
0.0029
1
09/06/22 15:20
09/08/22 05:37
91-20-3
n-Propylbenzene
ND
mg/kg
0.0054
0.0019
1
09/06/22 15:20
09/08/22 05:37
103-65-1
Styrene
ND
mg/kg
0.0054
0.0014
1
09/06/22 15:20
09/08/22 05:37
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0054
0.0021
1
09/06/22 15:20
09/08/22 05:37
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0054
0.0014
1
09/06/22 15:20
09/08/22 05:37
79-34-5
Tetrachloroethene
ND
mg/kg
0.0054
0.0017
1
09/06/22 15:20
09/08/22 05:37
127-18-4
Toluene
ND
mg/kg
0.0054
0.0015
1
09/06/22 15:20
09/08/22 05:37
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0054
0.0044
1
09/06/22 15:20
09/08/22 05:37
87-61-6 IK,L2,v2
1,2,4-Trichlorobenzene
ND
mg/kg
0.0054
0.0046
1
09/06/22 15:20
09/08/22 05:37
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0054
0.0028
1
09/06/22 15:20
09/08/22 05:37
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0054
0.0018
1
09/06/22 15:20
09/08/22 05:37
79-00-5
Trichloroethene
ND
mg/kg
0.0054
0.0014
1
09/06/22 15:20
09/08/22 05:37
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0054
0.0030
1
09/06/22 15:20
09/08/22 05:37
75-69-4 IK
1,2,3-Trichloropropane
ND
mg/kg
0.0054
0.0027
1
09/06/22 15:20
09/08/22 05:37
96-18-4
1,2,4-Trimethylbenzene
ND
mg/kg
0.0054
0.0015
1
09/06/22 15:20
09/08/22 05:37
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0054
0.0018
1
09/06/22 15:20
09/08/22 05:37
108-67-8
Vinyl acetate
ND
mg/kg
0.054
0.0039
1
09/06/22 15:20
09/08/22 05:37
108-05-4
Vinyl chloride
ND
mg/kg
0.011
0.0028
1
09/06/22 15:20
09/08/22 05:37
75-01-4
Xylene (Total)
0.011
mg/kg
0.011
0.0031
1
09/06/22 15:20
09/08/22 05:37
1330-20-7
m&p-Xylene
0.0054J
mg/kg
0.011
0.0037
1
09/06/22 15:20
09/08/22 05:37
179601-23-1
o-Xylene
0.0060
mg/kg
0.0054
0.0024
1
09/06/22 15:20
09/08/22 05:37
95-47-6
Surrogates
Toluene-d8 (S)
101
%
70-130
1
09/06/22 15:20
09/08/22 05:37
2037-26-5
4-Bromofluorobenzene (S)
102
%
70-130
1
09/06/22 15:20
09/08/22 05:37
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
09/06/22 15:20
09/08/22 05:37
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
11.7
%
0.10
0.10
1
09/07/22 17:11
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
QC Batch: 748987 Analysis Method: EPA 6020B
QC Batch Method: EPA 3050E Analysis Description: EPA 6020
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92623549001
METHOD BLANK: 2391600
Matrix:
Solid
Associated Lab Samples: 92623549001
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Arsenic
mg/kg
ND
0.040
0.010
09/07/2217:59
Barium
mg/kg
ND
0.040
0.010
09/07/2217:59
Cadmium
mg/kg
ND
0.040
0.010
09/07/2217:59
Chromium
mg/kg
ND
0.040
0.010
09/07/2217:59
Lead
mg/kg
ND
0.040
0.010
09/07/2217:59
Selenium
mg/kg
ND
0.040
0.010
09/07/2217:59
Silver
mg/kg
ND
0.040
0.010
09/07/2217:59
LABORATORY CONTROL SAMPLE:
2391601
Parameter
Units
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Chromium
mg/kg
Lead
mg/kg
Selenium
mg/kg
Silver
mg/kg
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2
1.91
96
80-120
2
2.03
101
80-120
2
1.92
96
80-120
2
2.06
103
80-120
2
2.16
108
80-120
0.4
0.39
98
80-120
2
2.03
102
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
QC Batch: 749043 Analysis Method: EPA 7471 B
QC Batch Method: METHOD Analysis Description: EPA 7471 B
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92623549001
METHOD BLANK: 2392018
Matrix:
Solid
Associated Lab Samples: 92623549001
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Mercury
mg/kg
ND
0.010
0.0040 09/07/2213:51
LABORATORY CONTROL SAMPLE:
2392019
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
mg/kg
0.25
0.25
99 80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
QC Batch: 721612 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92623549002
METHOD BLANK: 3759718
Associated Lab Samples: 92623549002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0019
09/08/22 01:52
1,1,1-Trichloroethane
mg/kg
ND
0.0050
0.0026
09/08/22 01:52
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0013
09/08/22 01:52
1,1,2-Trichloroethane
mg/kg
ND
0.0050
0.0017
09/08/22 01:52
1,1-Dichloroethane
mg/kg
ND
0.0050
0.0021
09/08/22 01:52
1,1-Dichloroethene
mg/kg
ND
0.0050
0.0021
09/08/22 01:52
1,1-Dichloropropene
mg/kg
ND
0.0050
0.0024
09/08/22 01:52
1,2,3-Trichlorobenzene
mg/kg
ND
0.0050
0.0040
09/08/22 01:52 IL,v2
1,2,3-Trichloropropane
mg/kg
ND
0.0050
0.0025
09/08/22 01:52
1,2,4-Trichlorobenzene
mg/kg
ND
0.0050
0.0042
09/08/22 01:52
1,2,4-Trimethylbenzene
mg/kg
ND
0.0050
0.0014
09/08/22 01:52
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0050
0.0019
09/08/22 01:52
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0050
0.0022
09/08/22 01:52
1,2-Dichlorobenzene
mg/kg
ND
0.0050
0.0018
09/08/22 01:52
1,2-Dichloroethane
mg/kg
ND
0.0050
0.0033
09/08/22 01:52
1,2-Dichloropropane
mg/kg
ND
0.0050
0.0015
09/08/22 01:52
1,3,5-Trimethylbenzene
mg/kg
ND
0.0050
0.0017
09/08/22 01:52
1,3-Dichlorobenzene
mg/kg
ND
0.0050
0.0016
09/08/22 01:52
1,3-Dichloropropane
mg/kg
ND
0.0050
0.0016
09/08/22 01:52
1,4-Dichlorobenzene
mg/kg
ND
0.0050
0.0013
09/08/22 01:52
2,2-Dichloropropane
mg/kg
ND
0.0050
0.0016
09/08/22 01:52
2-Butanone (MEK)
mg/kg
ND
0.10
0.024
09/08/22 01:52
2-Chlorotoluene
mg/kg
ND
0.0050
0.0018
09/08/22 01:52
2-Hexanone
mg/kg
ND
0.050
0.0048
09/08/22 01:52
4-Chlorotoluene
mg/kg
ND
0.0050
0.00088
09/08/22 01:52
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.050
0.0048
09/08/22 01:52
Acetone
mg/kg
ND
0.10
0.032
09/08/22 01:52
Benzene
mg/kg
ND
0.0050
0.0020
09/08/22 01:52
Bromobenzene
mg/kg
ND
0.0050
0.0016
09/08/22 01:52
Bromochloromethane
mg/kg
ND
0.0050
0.0015
09/08/22 01:52
Bromodichloromethane
mg/kg
ND
0.0050
0.0019
09/08/22 01:52
Bromoform
mg/kg
ND
0.0050
0.0018
09/08/22 01:52
Bromomethane
mg/kg
ND
0.010
0.0079
09/08/22 01:52 IK
Carbon tetrachloride
mg/kg
ND
0.0050
0.0019
09/08/22 01:52
Chlorobenzene
mg/kg
ND
0.0050
0.00096
09/08/22 01:52
Chloroethane
mg/kg
ND
0.010
0.0039
09/08/22 01:52
Chloroform
mg/kg
ND
0.0050
0.0030
09/08/22 01:52
Chloromethane
mg/kg
ND
0.010
0.0042
09/08/22 01:52
cis-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0017
09/08/22 01:52
cis-1,3-Dichloropropene
mg/kg
ND
0.0050
0.0014
09/08/22 01:52
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 33

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
METHOD BLANK: 3759718
Associated Lab Samples: 92623549002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromochloromethane
mg/kg
ND
0.0050
0.0028
09/08/22 01:52
Dibromomethane
mg/kg
ND
0.0050
0.0011
09/08/22 01:52
Dichlorodifluoromethane
mg/kg
ND
0.010
0.0022
09/08/22 01:52
Diisopropyl ether
mg/kg
ND
0.0050
0.0014
09/08/22 01:52
Ethylbenzene
mg/kg
ND
0.0050
0.0023
09/08/22 01:52
Hexachloro-1,3-butadiene
mg/kg
ND
0.010
0.0082
09/08/22 01:52
Isopropylbenzene (Cumene)
mg/kg
ND
0.0050
0.0017
09/08/22 01:52
m&p-Xylene
mg/kg
ND
0.010
0.0034
09/08/22 01:52
Methyl-tert-butyl ether
mg/kg
ND
0.0050
0.0019
09/08/22 01:52
Methylene Chloride
mg/kg
ND
0.020
0.014
09/08/22 01:52
n-Butylbenzene
mg/kg
ND
0.0050
0.0024
09/08/22 01:52
n-Propylbenzene
mg/kg
ND
0.0050
0.0018
09/08/22 01:52
Naphthalene
mg/kg
ND
0.0050
0.0026
09/08/22 01:52
o-Xylene
mg/kg
ND
0.0050
0.0022
09/08/22 01:52
p-Isopropyltoluene
mg/kg
ND
0.0050
0.0025
09/08/22 01:52
sec-Butylbenzene
mg/kg
ND
0.0050
0.0022
09/08/22 01:52
Styrene
mg/kg
ND
0.0050
0.0013
09/08/22 01:52
tert-Butyl benzene
mg/kg
ND
0.0050
0.0018
09/08/22 01:52
Tetrachloroethene
mg/kg
ND
0.0050
0.0016
09/08/22 01:52
Toluene
mg/kg
ND
0.0050
0.0014
09/08/22 01:52
trans-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0018
09/08/22 01:52
trans- 1,3-Dichloropropene
mg/kg
ND
0.0050
0.0017
09/08/22 01:52
Trichloroethene
mg/kg
ND
0.0050
0.0013
09/08/22 01:52
Trichlorofluoromethane
mg/kg
ND
0.0050
0.0028
09/08/22 01:52
Vinyl acetate
mg/kg
ND
0.050
0.0036
09/08/22 01:52
Vinyl chloride
mg/kg
ND
0.010
0.0025
09/08/22 01:52
Xylene (Total)
mg/kg
ND
0.010
0.0028
09/08/22 01:52
1,2-Dichloroethane-d4 (S)
%
99
70-130
09/08/22 01:52
4-Bromofluorobenzene (S)
%
100
70-130
09/08/22 01:52
Toluene-d8(S)
%
100
70-130
09/08/22 01:52
LABORATORY CONTROL SAMPLE: 3759719
Parameter
Qualifiers
IK
IK
IK
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
1.2
1.3
105
70-130
1,1,1-Trichloroethane
mg/kg
1.2
1.4
113
70-130
1,1,2,2-Tetrachloroethane
mg/kg
1.2
1.1
89
70-130
1,1,2-Trichloroethane
mg/kg
1.2
1.2
99
70-130
1,1-Dichloroethane
mg/kg
1.2
1.4
108
70-130
1,1-Dichloroethene
mg/kg
1.2
1.5
119
70-130
1,1-Dichloropropene
mg/kg
1.2
1.5
118
70-130
1,2,3-Trichlorobenzene
mg/kg
1.2
0.69
55
70-1301L,L2,v3
1,2,3-Trichloropropane
mg/kg
1.2
1.2
92
70-130
1,2,4-Trichlorobenzene
mg/kg
1.2
0.94
75
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
LABORATORY CONTROL SAMPLE:
Parameter
3759719
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trimethylbenzene
mg/kg
1.2
1.3
104
70-130
1,2-Dibromo-3-chloropropane
mg/kg
1.2
0.94
75
67-130
1,2-Dibromoethane (EDB)
mg/kg
1.2
1.2
96
70-130
1,2-Dichlorobenzene
mg/kg
1.2
1.2
99
70-130
1,2-Dichloroethane
mg/kg
1.2
1.3
102
70-130
1,2-Dichloropropane
mg/kg
1.2
1.3
103
70-130
1,3,5-Trimethylbenzene
mg/kg
1.2
1.4
109
70-130
1,3-Dichlorobenzene
mg/kg
1.2
1.3
102
70-130
1,3-Dichloropropane
mg/kg
1.2
1.2
96
70-130
1,4-Dichlorobenzene
mg/kg
1.2
1.2
100
70-130
2,2-Dichloropropane
mg/kg
1.2
1.3
106
67-130
2-Butanone (MEK)
mg/kg
2.5
2.2
89
66-130
2-Chlorotoluene
mg/kg
1.2
1.3
107
70-130
2-Hexanone
mg/kg
2.5
2.3
92
70-130
4-Chlorotoluene
mg/kg
1.2
1.3
105
70-130
4-Methyl-2-pentanone (MIBK)
mg/kg
2.5
2.3
93
70-130
Acetone
mg/kg
2.5
2.1
83
67-130
Benzene
mg/kg
1.2
1.2
97
70-130
Bromobenzene
mg/kg
1.2
1.3
103
70-130
Bromochloromethane
mg/kg
1.2
1.4
109
70-130
Bromodichloromethane
mg/kg
1.2
1.3
103
70-130
Bromoform
mg/kg
1.2
1.3
101
70-130
Bromomethane
mg/kg
1.2
1.6
126
53-175IK
Carbon tetrachloride
mg/kg
1.2
1.3
107
70-130
Chlorobenzene
mg/kg
1.2
1.3
103
70-130
Chloroethane
mg/kg
1.2
1.5
121
70-135
Chloroform
mg/kg
1.2
1.3
107
70-130
Chloromethane
mg/kg
1.2
1.5
122
64-130
cis-1,2-Dichloroethene
mg/kg
1.2
1.4
111
70-130
cis-1,3-Dichloropropene
mg/kg
1.2
1.3
103
70-130
Dibromochloromethane
mg/kg
1.2
1.3
101
70-130
Dibromomethane
mg/kg
1.2
1.2
98
70-130
Dichlorodifluoromethane
mg/kg
1.2
1.5
117
63-145IK
Diisopropyl ether
mg/kg
1.2
1.4
111
68-130
Ethylbenzene
mg/kg
1.2
1.2
98
70-130
Hexachloro-1,3-butadiene
mg/kg
1.2
1.2
98
70-130
Isopropylbenzene (Cumene)
mg/kg
1.2
1.3
103
70-130
m&p-Xylene
mg/kg
2.5
2.7
106
70-130
Methyl-tert-butyl ether
mg/kg
1.2
1.3
104
70-130
Methylene Chloride
mg/kg
1.2
1.2
96
67-130 IK
n-Butylbenzene
mg/kg
1.2
1.4
109
70-130
n-Propylbenzene
mg/kg
1.2
1.3
108
70-130
Naphthalene
mg/kg
1.2
0.97
77
70-130
o-Xylene
mg/kg
1.2
1.3
107
70-130
p-Isopropyltoluene
mg/kg
1.2
1.4
109
70-130
sec-Butylbenzene
mg/kg
1.2
1.3
107
70-130
Styrene
mg/kg
1.2
1.4
112
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
LABORATORY CONTROL SAMPLE:
Parameter
3759719
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
tert-Butyl benzene
mg/kg
1.2
1.4
112
64-130
Tetrachloroethene
mg/kg
1.2
1.3
103
70-130
Toluene
mg/kg
1.2
1.2
99
70-130
trans-1,2-Dichloroethene
mg/kg
1.2
1.4
114
70-130
trans- 1,3-Dichloropropene
mg/kg
1.2
1.3
102
70-130
Trichloroethene
mg/kg
1.2
1.3
105
70-130
Trichlorofluoromethane
mg/kg
1.2
1.3
108
70-1301K
Vinyl acetate
mg/kg
2.5
2.7
110
70-134
Vinyl chloride
mg/kg
1.2
1.6
125
68-130
Xylene (Total)
mg/kg
3.8
4.0
107
70-130
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
102
70-130
MATRIX SPIKE SAMPLE:
Parameter
3759720
Units
92623615001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.68
0.67
98
58-140
1,1,1-Trichloroethane
mg/kg
ND
0.68
0.73
108
58-144
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.68
0.56
83
52-139
1,1,2-Trichloroethane
mg/kg
ND
0.68
0.63
93
56-140
1,1-Dichloroethane
mg/kg
ND
0.68
0.67
99
58-145
1,1-Dichloroethene
mg/kg
ND
0.68
0.81
119
57-158
1,1-Dichloropropene
mg/kg
ND
0.68
0.76
112
58-151
1,2,3-Trichlorobenzene
mg/kg
ND
0.68
0.27
39
48-1491L,MO,v3
1,2,3-Trichloropropane
mg/kg
ND
0.68
0.56
83
54-132
1,2,4-Trichlorobenzene
mg/kg
ND
0.68
0.48
71
51-151
1,2,4-Trimethylbenzene
mg/kg
ND
0.68
0.67
99
38-170
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.68
0.48
70
44-134
1,2-Dibromoethane (EDB)
mg/kg
ND
0.68
0.59
87
60-138
1,2-Dichlorobenzene
mg/kg
ND
0.68
0.65
96
59-147
1,2-Dichloroethane
mg/kg
ND
0.68
0.61
90
57-139
1,2-Dichloropropane
mg/kg
ND
0.68
0.67
99
62-145
1,3,5-Trimethylbenzene
mg/kg
ND
0.68
0.70
103
47-159
1,3-Dichlorobenzene
mg/kg
ND
0.68
0.69
101
58-144
1,3-Dichloropropane
mg/kg
ND
0.68
0.61
90
60-142
1,4-Dichlorobenzene
mg/kg
ND
0.68
0.64
95
57-143
2,2-Dichloropropane
mg/kg
ND
0.68
0.48
71
37-144
2-Butanone (MEK)
mg/kg
ND
1.4
0.99
71
28-146
2-Chlorotoluene
mg/kg
ND
0.68
0.68
100
55-158
2-Hexanone
mg/kg
ND
1.4
1.0
75
44-141
4-Chlorotoluene
mg/kg
ND
0.68
0.66
98
55-146
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
1.4
1.1
78
50-138
Acetone
mg/kg
ND
1.4
0.96
71
20-136
Benzene
mg/kg
ND
0.68
0.67
99
60-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
MATRIX SPIKE SAMPLE:
3759720
92623615001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromobenzene
mg/kg
ND
0.68
0.63
93
59-145
Bromochloromethane
mg/kg
ND
0.68
0.64
94
57-143
Bromodichloromethane
mg/kg
ND
0.68
0.65
96
53-133
Bromoform
mg/kg
ND
0.68
0.60
88
48-133
Bromomethane
mg/kg
ND
0.68
0.22
33
10-1671K
Carbon tetrachloride
mg/kg
ND
0.68
0.74
109
57-147
Chlorobenzene
mg/kg
ND
0.68
0.68
100
61-144
Chloroethane
mg/kg
ND
0.68
0.20
29
10-153
Chloroform
mg/kg
ND
0.68
0.67
99
58-141
Chloromethane
mg/kg
ND
0.68
0.82
121
54-165
cis-1,2-Dichloroethene
mg/kg
ND
0.68
0.68
100
59-144
cis-1,3-Dichloropropene
mg/kg
ND
0.68
0.62
91
56-137
Dibromochloromethane
mg/kg
ND
0.68
0.61
90
53-139
Dibromomethane
mg/kg
ND
0.68
0.62
91
60-136
Dichlorodifluoromethane
mg/kg
ND
0.68
0.89
132
49-1771K
Diisopropyl ether
mg/kg
ND
0.68
0.65
95
53-136
Ethylbenzene
mg/kg
ND
0.68
0.64
94
53-150
Hexachloro-1,3-butadiene
mg/kg
ND
0.68
0.77
113
42-186
Isopropylbenzene (Cumene)
mg/kg
ND
0.68
0.69
101
62-154
m&p-Xylene
mg/kg
ND
1.4
1.4
101
49-156
Methyl-tert-butyl ether
mg/kg
ND
0.68
0.59
87
54-133
Methylene Chloride
mg/kg
ND
0.68
0.47
70
50-153 IK
n-Butylbenzene
mg/kg
ND
0.68
0.72
106
44-174
n-Propylbenzene
mg/kg
ND
0.68
0.70
103
52-157
Naphthalene
mg/kg
ND
0.68
0.34
51
37-150
o-Xylene
mg/kg
ND
0.68
0.69
102
54-150
p-Isopropyltoluene
mg/kg
ND
0.68
0.72
106
50-164
sec-Butylbenzene
mg/kg
ND
0.68
0.73
108
58-161
Styrene
mg/kg
ND
0.68
0.68
100
60-148
tert-Butyl benzene
mg/kg
ND
0.68
0.70
102
44-151
Tetrachloroethene
mg/kg
ND
0.68
0.66
97
53-151
Toluene
mg/kg
ND
0.68
0.66
98
52-148
trans-1,2-Dichloroethene
mg/kg
ND
0.68
0.73
108
60-148
trans- 1,3-Dichloropropene
mg/kg
ND
0.68
0.60
88
55-133
Trichloroethene
mg/kg
ND
0.68
0.72
105
60-148
Trichlorofluoromethane
mg/kg
ND
0.68
0.36
52
10-1541K
Vinyl acetate
mg/kg
ND
1.4
1.1
85
50-149
Vinyl chloride
mg/kg
ND
0.68
0.77
113
57-157
Xylene (Total)
mg/kg
ND
2
2.1
101
52-153
1,2-Dichloroethane-d4 (S)
%
89
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
SAMPLE DUPLICATE: 3759721
92623615002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,1-Trichloroethane
mg/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,2-Trichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethene
mg/kg
ND
ND
30
1,1-Dichloropropene
mg/kg
ND
ND
30
1,2,3-Trichlorobenzene
mg/kg
ND
ND
301L,v2
1,2,3-Trichloropropane
mg/kg
ND
ND
30
1,2,4-Trichlorobenzene
mg/kg
ND
ND
30
1,2,4-Trimethylbenzene
mg/kg
ND
ND
30
1,2-Dibromo-3-chloropropane
mg/kg
ND
ND
30
1,2-Dibromoethane (EDB)
mg/kg
ND
ND
30
1,2-Dichlorobenzene
mg/kg
ND
ND
30
1,2-Dichloroethane
mg/kg
ND
ND
30
1,2-Dichloropropane
mg/kg
ND
ND
30
1,3,5-Trimethylbenzene
mg/kg
ND
ND
30
1,3-Dichlorobenzene
mg/kg
ND
ND
30
1,3-Dichloropropane
mg/kg
ND
ND
30
1,4-Dichlorobenzene
mg/kg
ND
ND
30
2,2-Dichloropropane
mg/kg
ND
ND
30
2-Butanone (MEK)
mg/kg
ND
ND
30
2-Chlorotoluene
mg/kg
ND
ND
30
2-Hexanone
mg/kg
ND
ND
30
4-Chlorotoluene
mg/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
ND
30
Acetone
mg/kg
ND
ND
30
Benzene
mg/kg
ND
ND
30
Bromobenzene
mg/kg
ND
ND
30
Bromochloromethane
mg/kg
ND
ND
30
Bromodichloromethane
mg/kg
ND
ND
30
Bromoform
mg/kg
ND
ND
30
Bromomethane
mg/kg
ND
ND
301K
Carbon tetrachloride
mg/kg
ND
ND
30
Chlorobenzene
mg/kg
ND
ND
30
Chloroethane
mg/kg
ND
ND
30
Chloroform
mg/kg
ND
ND
30
Chloromethane
mg/kg
ND
ND
30
cis-1,2-Dichloroethene
mg/kg
ND
ND
30
cis-1,3-Dichloropropene
mg/kg
ND
ND
30
Dibromochloromethane
mg/kg
ND
ND
30
Dibromomethane
mg/kg
ND
ND
30
Dichlorodifluoromethane
mg/kg
ND
ND
301K
Diisopropyl ether
mg/kg
ND
ND
30
Ethylbenzene
mg/kg
ND
ND
30
Hexachloro-1,3-butadiene
mg/kg
ND
ND
30
Isopropylbenzene (Cumene)
mg/kg
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 33

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
SAMPLE DUPLICATE: 3759721
Parameter
Units
92623615002
Result
Dup
Result
m&p-Xylene
mg/kg
ND
ND
Methyl-tert-butyl ether
mg/kg
ND
ND
Methylene Chloride
mg/kg
ND
ND
n-Butylbenzene
mg/kg
ND
ND
n-Propylbenzene
mg/kg
ND
ND
Naphthalene
mg/kg
ND
ND
o-Xylene
mg/kg
ND
ND
p-Isopropyltoluene
mg/kg
ND
ND
sec-Butylbenzene
mg/kg
ND
ND
Styrene
mg/kg
ND
ND
tert-Butyl benzene
mg/kg
ND
ND
Tetrachloroethene
mg/kg
ND
ND
Toluene
mg/kg
ND
ND
trans-1,2-Dichloroethene
mg/kg
ND
ND
trans- 1,3-Dichloropropene
mg/kg
ND
ND
Trichloroethene
mg/kg
ND
ND
Trichlorofluoromethane
mg/kg
ND
ND
Vinyl acetate
mg/kg
ND
ND
Vinyl chloride
mg/kg
ND
ND
Xylene (Total)
mg/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
96
95
4-Bromofluorobenzene (S)
%
102
101
Toluene-d8 (S)
%
100
100
Max
RPD RPD Qualifiers
30
30
30 I K
30
30
30
30
30
30
30
30
30
30
30
30
30
30 I K
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
QC Batch: 721862 Analysis Method: EPA 8081 B
QC Batch Method: EPA 3546 Analysis Description: 8081 GCS Pesticides
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92623549001
METHOD BLANK: 3761093
Associated Lab Samples: 92623549001
Parameter
4,4'-DDD
4,4'-DDE
4,4'-DDT
Aldrin
alpha-BHC
beta-BHC
Chlordane (Technical)
delta-BHC
Dieldrin
Endosulfan I
Endosulfan 11
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Methoxychlor
Mirex
Toxaphene
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
Matrix: Solid
Units
Blank
Result
Reporting
Limit
MDL
Analyzed
mg/kg
ND
0.0020
0.00090
09/08/22 09:18
mg/kg
ND
0.0020
0.00094
09/08/22 09:18
mg/kg
ND
0.0020
0.00089
09/08/22 09:18
mg/kg
ND
0.0020
0.00081
09/08/22 09:18
mg/kg
ND
0.0020
0.00087
09/08/22 09:18
mg/kg
ND
0.0020
0.00096
09/08/22 09:18
mg/kg
ND
0.010
0.0087
09/08/22 09:18
mg/kg
ND
0.0020
0.00099
09/08/22 09:18
mg/kg
ND
0.0020
0.00087
09/08/22 09:18
mg/kg
ND
0.0020
0.00086
09/08/22 09:18
mg/kg
ND
0.0020
0.00090
09/08/22 09:18
mg/kg
ND
0.0020
0.0011
09/08/22 09:18
mg/kg
ND
0.0020
0.00093
09/08/22 09:18
mg/kg
ND
0.0020
0.0013
09/08/22 09:18
mg/kg
ND
0.0020
0.0011
09/08/22 09:18
mg/kg
ND
0.0020
0.00080
09/08/22 09:18
mg/kg
ND
0.0020
0.00092
09/08/22 09:18
mg/kg
ND
0.0020
0.00079
09/08/22 09:18
mg/kg
ND
0.0020
0.00082
09/08/22 09:18
mg/kg
ND
0.0050
0.0024
09/08/22 09:18
mg/kg
ND
0.0050
0.0022
09/08/22 09:18
mg/kg
ND
0.0070
0.0053
09/08/22 09:18
%
71
10-146
09/08/22 09:18
%
70
10-133
09/08/22 09:18
LABORATORY CONTROL SAMPLE: 3761094
Qualifiers
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
mg/kg
0.0082
0.0092
111
40-160
4,4'-DDE
mg/kg
0.0082
0.0091
110
41-154
4,4'-DDT
mg/kg
0.0082
0.0096
117
34-163
Aldrin
mg/kg
0.0082
0.0065
79
39-144
alpha-BHC
mg/kg
0.0082
0.0073
89
36-145
beta-BHC
mg/kg
0.0082
0.0068
83
39-152
delta-BHC
mg/kg
0.0082
0.0071
87
41-147
Dieldrin
mg/kg
0.0082
0.0092
112
42-153
Endosulfan I
mg/kg
0.0082
0.0069
84
39-148
Endosulfan II
mg/kg
0.0082
0.0069
84
40-147
Endosulfan sulfate
mg/kg
0.0082
0.0072
87
40-148
Results presented on
this page are in the units indicated
by the "Units"
column except
where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC.
Page 19 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: CRP.003
Pace Project No.: 92623549
LABORATORY CONTROL SAMPLE: 3761094
Parameter
Endrin
Endrin aldehyde
Endrin ketone
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Methoxychlor
Mirex
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
I•r_11IVp1=11u111WfMLb1»:1
Parameter
4,4'-DDD
4,4'-DDE
4,4'-DDT
Aldrin
alpha-BHC
beta-BHC
delta-BHC
Dieldrin
Endosulfan I
Endosulfan 11
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Methoxychlor
Mirex
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
011-1111*11
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
QUALITY CONTROL DATA
Spike
Conc.
0.0082
0.0082
0.0082
0.0082
0.0082
0.0082
0.0082
0.025
0.025
LCS
Result
0.0096
0.0066
0.0073
0.0067
0.0069
0.0069
0.0067
0.021
0.021
92623549001
Result
ND
0.024
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Spike
Conc.
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.0099
0.029
0.029
LCS
% Rec
117
80
88
81
83
84
82
86
86
96
76
MS
Result
0.016
0.040
0.016
0.0076
0.0086
0.0081
0.0088
0.012
0.0078
0.0079
0.0081
0.012
0.0076
0.0088
0.0081
0.0081
0.0087
0.0076
0.025
0.024
% Rec
Limits
42-158
39-130
39-159
38-146
39-144
40-143
33-139
32-146
39-141
10-146
10-133
MS
% Rec
159
165
162
77
88
82
90
119
80
81
82
117
77
89
82
83
89
78
86
82
79
76
Qualifiers
% Rec
Limits
10-160
10-170
10-194
10-143
10-144
10-152
10-147
10-181
10-147
11-149
10-153
10-160
10-134
11-155
10-152
10-149
10-142
10-140
10-147
11-139
10-146
10-133
SAMPLE DUPLICATE: 3761096
92623697002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
4,4'-DDD mg/kg ND ND 30
4,4'-DDE mg/kg 90.4 ug/kg 0.084 8 30
4,4'-DDT mg/kg 110 ug/kg 0.11 0 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 20 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
SAMPLE DUPLICATE: 3761096
Parameter
Units
92623697002
Result
Dup
Result
Aldrin
mg/kg
ND
ND
alpha-BHC
mg/kg
ND
ND
beta-BHC
mg/kg
ND
ND
Chlordane (Technical)
mg/kg
ND
ND
delta-BHC
mg/kg
ND
ND
Dieldrin
mg/kg
ND
ND
Endosulfan I
mg/kg
ND
ND
Endosulfan II
mg/kg
ND
ND
Endosulfan sulfate
mg/kg
ND
ND
Endrin
mg/kg
19.9 ug/kg
0.020
Endrin aldehyde
mg/kg
ND
ND
Endrin ketone
mg/kg
ND
0.00901
gamma-BHC (Lindane)
mg/kg
ND
ND
Heptachlor
mg/kg
ND
ND
Heptachlor epoxide
mg/kg
ND
ND
Hexachlorobenzene
mg/kg
ND
ND
Methoxychlor
mg/kg
ND
ND
Mirex
mg/kg
ND
ND
Toxaphene
mg/kg
ND
ND
Decachlorobiphenyl (S)
%
113
127
Tetrachloro-m-xylene (S)
%
86
79
lVV
0
Max
RPD
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC.
Page 21 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
QC Batch: 721805 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92623549001
METHOD BLANK: 3760695
Associated Lab Samples: 92623549001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
mg/kg
ND
0.33
0.13
09/09/22 11:53
1,2-Dichlorobenzene
mg/kg
ND
0.33
0.12
09/09/22 11:53
1,3-Dichlorobenzene
mg/kg
ND
0.33
0.12
09/09/22 11:53
1,4-Dichlorobenzene
mg/kg
ND
0.33
0.12
09/09/22 11:53
1-Methylnaphthalene
mg/kg
ND
0.33
0.11
09/09/22 11:53
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
0.33
0.15
09/09/22 11:53
2,4,5-Trichlorophenol
mg/kg
ND
0.33
0.15
09/09/22 11:53
2,4,6-Trichlorophenol
mg/kg
ND
0.33
0.13
09/09/22 11:53
2,4-Dichlorophenol
mg/kg
ND
0.33
0.13
09/09/22 11:53
2,4-Dimethylphenol
mg/kg
ND
0.33
0.14
09/09/22 11:53
2,4-Dinitrophenol
mg/kg
ND
1.6
1.0
09/09/22 11:53
2,4-Dinitrotoluene
mg/kg
ND
0.33
0.13
09/09/22 11:53
2,6-Dinitrotoluene
mg/kg
ND
0.33
0.12
09/09/22 11:53
2-Chloronaphthalene
mg/kg
ND
0.33
0.13
09/09/22 11:53
2-Chlorophenol
mg/kg
ND
0.33
0.12
09/09/22 11:53
2-Methylnaphthalene
mg/kg
ND
0.33
0.13
09/09/22 11:53
2-Methylphenol(o-Cresol)
mg/kg
ND
0.33
0.13
09/09/22 11:53
2-Nitroaniline
mg/kg
ND
1.6
0.27
09/09/22 11:53
2-Nitrophenol
mg/kg
ND
0.33
0.14
09/09/22 11:53
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
0.33
0.13
09/09/22 11:53
3,3'-Dichlorobenzidine
mg/kg
ND
0.65
0.22
09/09/22 11:53
3-Nitroaniline
mg/kg
ND
1.6
0.26
09/09/22 11:53
4,6-Dinitro-2-methyl phenol
mg/kg
ND
0.65
0.30
09/09/22 11:53
4-Bromophenylphenyl ether
mg/kg
ND
0.33
0.13
09/09/22 11:53
4-ChIoro-3-methyl phenol
mg/kg
ND
0.65
0.23
09/09/22 11:53
4-Chloroaniline
mg/kg
ND
0.65
0.26
09/09/22 11:53
4-Chlorophenylphenyl ether
mg/kg
ND
0.33
0.12
09/09/22 11:53
4-Nitroaniline
mg/kg
ND
0.65
0.25
09/09/22 11:53
4-Nitrophenol
mg/kg
ND
1.6
0.63
09/09/22 11:53
Acenaphthene
mg/kg
ND
0.33
0.11
09/09/22 11:53
Acenaphthylene
mg/kg
ND
0.33
0.11
09/09/22 11:53
Aniline
mg/kg
ND
0.33
0.13
09/09/22 11:53
Anthracene
mg/kg
ND
0.33
0.11
09/09/22 11:53
Benzo(a)anthracene
mg/kg
ND
0.33
0.11
09/09/22 11:53
Benzo(a)pyrene
mg/kg
ND
0.33
0.11
09/09/22 11:53
Benzo(b)fluoranthene
mg/kg
ND
0.33
0.11
09/09/22 11:53
Benzo(g,h,i)perylene
mg/kg
ND
0.33
0.13
09/09/22 11:53
Benzo(k)fluoranthene
mg/kg
ND
0.33
0.11
09/09/22 11:53
Benzoic Acid
mg/kg
ND
1.6
0.70
09/09/22 11:53
Benzyl alcohol
mg/kg
ND
0.65
0.25
09/09/22 11:53
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
METHOD BLANK: 3760695
Associated Lab Samples: 92623549001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
bis(2-Chloroethoxy)methane
mg/kg
ND
0.33
0.14
09/09/22 11:53
bis(2-Chloroethyl) ether
mg/kg
ND
0.33
0.12
09/09/22 11:53
bis(2-Ethylhexyl)phthalate
mg/kg
ND
0.33
0.13
09/09/22 11:53
Butylbenzylphthalate
mg/kg
ND
0.33
0.14
09/09/22 11:53
Chrysene
mg/kg
ND
0.33
0.12
09/09/22 11:53
Di-n-butylphthalate
mg/kg
ND
0.33
0.11
09/09/22 11:53
Di-n-octylphthalate
mg/kg
ND
0.33
0.13
09/09/22 11:53
Dibenz(a,h)anthracene
mg/kg
ND
0.33
0.13
09/09/22 11:53
Dibenzofuran
mg/kg
ND
0.33
0.12
09/09/22 11:53
Diethylphthalate
mg/kg
ND
0.33
0.12
09/09/22 11:53
Dimethylphthalate
mg/kg
ND
0.33
0.12
09/09/22 11:53
Fluoranthene
mg/kg
ND
0.33
0.11
09/09/22 11:53
Fluorene
mg/kg
ND
0.33
0.11
09/09/22 11:53
Hexachloro-1,3-butadiene
mg/kg
ND
0.33
0.14
09/09/22 11:53
Hexachlorobenzene
mg/kg
ND
0.33
0.13
09/09/22 11:53
Hexachlorocyclopentadiene
mg/kg
ND
0.33
0.19
09/09/22 11:53
Hexachloroethane
mg/kg
ND
0.33
0.12
09/09/22 11:53
Indeno(1,2,3-cd)pyrene
mg/kg
ND
0.33
0.13
09/09/22 11:53
Isophorone
mg/kg
ND
0.33
0.15
09/09/22 11:53
N-Nitroso-di-n-propylamine
mg/kg
ND
0.33
0.12
09/09/22 11:53
N-Nitrosodimethylamine
mg/kg
ND
0.33
0.11
09/09/22 11:53
N-Nitrosodiphenylamine
mg/kg
ND
0.33
0.12
09/09/22 11:53
Naphthalene
mg/kg
ND
0.33
0.11
09/09/22 11:53
Nitrobenzene
mg/kg
ND
0.33
0.15
09/09/22 11:53
Pentachlorophenol
mg/kg
ND
0.65
0.32
09/09/22 11:53
Phenanthrene
mg/kg
ND
0.33
0.11
09/09/22 11:53
Phenol
mg/kg
ND
0.33
0.15
09/09/22 11:53
Pyrene
mg/kg
ND
0.33
0.13
09/09/22 11:53
Pyridine
mg/kg
ND
0.33
0.10
09/09/22 11:53
2,4,6-Tribromophenol (S)
%
74
10-131
09/09/22 11:53
2-Fluorobiphenyl (S)
%
59
10-130
09/09/22 11:53
2-Fluorophenol(S)
%
55
10-130
09/09/22 11:53
Nitrobenzene-d5 (S)
%
56
10-130
09/09/22 11:53
Phenol-d6 (S)
%
53
10-130
09/09/22 11:53
Terphenyl-d14 (S)
%
87
10-130
09/09/22 11:53
Qualifiers
LABORATORY CONTROL SAMPLE:
3760696
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
1.7
1.2
74
43-130
1,2-Dichlorobenzene
mg/kg
1.7
1.2
70
43-130
1,3-Dichlorobenzene
mg/kg
1.7
1.2
71
43-130
1,4-Dichlorobenzene
mg/kg
1.7
1.1
69
44-130
1-Methylnaphthalene
mg/kg
1.7
1.3
81
47-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
LABORATORY CONTROL SAMPLE:
Parameter
3760696
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,2'-Oxybis(1-chloropropane)
mg/kg
1.7
1.2
75
29-130
2,4,5-Trichlorophenol
mg/kg
1.7
1.4
86
47-130
2,4,6-Trichlorophenol
mg/kg
1.7
1.4
82
47-130
2,4-Dichlorophenol
mg/kg
1.7
1.3
79
45-130
2,4-Dimethylphenol
mg/kg
1.7
1.5
90
45-130
2,4-Dinitrophenol
mg/kg
8.3
6.3
76
27-140
2,4-Dinitrotoluene
mg/kg
1.7
1.4
87
46-130
2,6-Dinitrotoluene
mg/kg
1.7
1.5
88
48-130
2-Chloronaphthalene
mg/kg
1.7
1.3
76
46-130
2-Chlorophenol
mg/kg
1.7
1.3
76
43-130
2-Methylnaphthalene
mg/kg
1.7
1.3
78
47-130
2-Methylphenol(o-Cresol)
mg/kg
1.7
1.2
73
42-130
2-Nitroaniline
mg/kg
3.3
2.9
86
41-130
2-Nitrophenol
mg/kg
1.7
1.4
84
48-130
3&4-Methyl phenol (m&p Cresol)
mg/kg
1.7
1.2
70
39-130
3,3'-Dichlorobenzidine
mg/kg
3.3
2.4
72
41-130
3-Nitroaniline
mg/kg
3.3
2.8
84
37-130
4,6-Dinitro-2-methyl phenol
mg/kg
3.3
2.5
77
38-141
4-Bromophenylphenyl ether
mg/kg
1.7
1.5
91
47-130
4-ChIoro-3-methyl phenol
mg/kg
3.3
2.9
88
44-130
4-Chloroaniline
mg/kg
3.3
2.5
75
41-130
4-Chlorophenylphenyl ether
mg/kg
1.7
1.4
83
45-130
4-Nitroaniline
mg/kg
3.3
2.6
79
42-130
4-Nitrophenol
mg/kg
8.3
6.7
80
39-131
Acenaphthene
mg/kg
1.7
1.3
76
49-130
Acenaphthylene
mg/kg
1.7
1.4
86
50-130
Aniline
mg/kg
1.7
1.2
71
38-130
Anthracene
mg/kg
1.7
1.2
73
49-130
Benzo(a)anthracene
mg/kg
1.7
1.3
80
51-130
Benzo(a)pyrene
mg/kg
1.7
1.6
94
51-130
Benzo(b)fluoranthene
mg/kg
1.7
1.6
95
49-130
Benzo(g,h,i)perylene
mg/kg
1.7
1.4
84
48-140
Benzo(k)fluoranthene
mg/kg
1.7
1.4
85
51-130
Benzoic Acid
mg/kg
8.3
4.6
56
22-130
Benzyl alcohol
mg/kg
3.3
2.6
78
43-130
bis(2-Chloroethoxy)methane
mg/kg
1.7
1.3
76
43-130
bis(2-Chloroethyl) ether
mg/kg
1.7
1.2
73
42-130
bis(2-Ethylhexyl)phthalate
mg/kg
1.7
1.1
68
43-130 v3
Butylbenzylphthalate
mg/kg
1.7
1.4
84
44-131
Chrysene
mg/kg
1.7
1.4
87
51-130
Di-n-butylphthalate
mg/kg
1.7
1.3
76
46-130
Di-n-octylphthalate
mg/kg
1.7
1.5
90
45-130
Dibenz(a,h)anthracene
mg/kg
1.7
1.4
86
48-130
Dibenzofuran
mg/kg
1.7
1.4
83
10-130
Diethylphthalate
mg/kg
1.7
1.3
81
48-130
Dimethylphthalate
mg/kg
1.7
1.4
84
48-130
Fluoranthene
mg/kg
1.7
1.5
89
48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
LABORATORY CONTROL SAMPLE:
Parameter
3760696
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Fluorene
mg/kg
1.7
1.3
81
48-130
Hexachloro-1,3-butadiene
mg/kg
1.7
1.3
77
39-130
Hexachlorobenzene
mg/kg
1.7
1.4
85
47-130
Hexachlorocyclopentadiene
mg/kg
1.7
1.1
69
17-130
Hexachloroethane
mg/kg
1.7
1.1
67
40-130
Indeno(1,2,3-cd)pyrene
mg/kg
1.7
1.4
87
50-130
Isophorone
mg/kg
1.7
1.3
80
41-130
N-Nitroso-di-n-propylamine
mg/kg
1.7
1.2
72
36-130
N-Nitrosodimethylamine
mg/kg
1.7
0.96
58
34-130
N-Nitrosodiphenylamine
mg/kg
1.7
1.3
77
48-130
Naphthalene
mg/kg
1.7
1.2
74
46-130
Nitrobenzene
mg/kg
1.7
1.3
77
39-130
Pentachlorophenol
mg/kg
3.3
2.5
74
42-130
Phenanthrene
mg/kg
1.7
1.4
82
50-130
Phenol
mg/kg
1.7
1.4
88
42-130
Pyrene
mg/kg
1.7
1.4
87
50-130
Pyridine
mg/kg
1.7
0.77
46
26-130
2,4,6-Tribromophenol (S)
%
85
10-131
2-Fluorobiphenyl (S)
%
71
10-130
2-Fluorophenol (S)
%
77
10-130
Nitrobenzene-d5 (S)
%
73
10-130
Phenol-d6 (S)
%
77
10-130
Terphenyl-d14 (S)
%
81
10-130
Qualifiers
SAMPLE DUPLICATE: 3760698
Parameter
Units
92623619005
Result
Dup
Result RPD
Max
RPD
1,2,4-Trichlorobenzene
mg/kg
ND
ND
30
1,2-Dichlorobenzene
mg/kg
ND
ND
30
1,3-Dichlorobenzene
mg/kg
ND
ND
30
1,4-Dichlorobenzene
mg/kg
ND
ND
30
1-Methylnaphthalene
mg/kg
ND
ND
30
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
ND
30
2,4,5-Trichlorophenol
mg/kg
ND
ND
30
2,4,6-Trichlorophenol
mg/kg
ND
ND
30
2,4-Dichlorophenol
mg/kg
ND
ND
30
2,4-Dimethylphenol
mg/kg
ND
ND
30
2,4-Dinitrophenol
mg/kg
ND
ND
30
2,4-Dinitrotoluene
mg/kg
ND
ND
30
2,6-Dinitrotoluene
mg/kg
ND
ND
30
2-Chloronaphthalene
mg/kg
ND
ND
30
2-Chlorophenol
mg/kg
ND
ND
30
2-Methylnaphthalene
mg/kg
ND
ND
30
2-Methylphenol(o-Cresol)
mg/kg
ND
ND
30
2-Nitroaniline
mg/kg
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
SAMPLE DUPLICATE: 3760698
Parameter
Units
92623619005
Result
Dup
Result RPD
Max
RPD Qualifiers
2-Nitrophenol
mg/kg
ND
ND
30
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
ND
30
3,3'-Dichlorobenzidine
mg/kg
ND
ND
30
3-Nitroaniline
mg/kg
ND
ND
30
4,6-Dinitro-2-methyl phenol
mg/kg
ND
ND
30
4-Bromophenylphenyl ether
mg/kg
ND
ND
30
4-Chloro-3-methylphenol
mg/kg
ND
ND
30
4-Chloroaniline
mg/kg
ND
ND
30
4-Chlorophenylphenyl ether
mg/kg
ND
ND
30
4-Nitroaniline
mg/kg
ND
ND
30
4-Nitrophenol
mg/kg
ND
ND
30
Acenaphthene
mg/kg
ND
ND
30
Acenaphthylene
mg/kg
ND
ND
30
Aniline
mg/kg
ND
ND
30
Anthracene
mg/kg
ND
ND
30
Benzo(a)anthracene
mg/kg
ND
ND
30
Benzo(a)pyrene
mg/kg
ND
ND
30
Benzo(b)fluoranthene
mg/kg
ND
ND
30
Benzo(g,h,i)perylene
mg/kg
ND
ND
30
Benzo(k)fluoranthene
mg/kg
ND
ND
30
Benzoic Acid
mg/kg
ND
ND
30
Benzyl alcohol
mg/kg
ND
ND
30
bis(2-Chloroethoxy)methane
mg/kg
ND
ND
30
bis(2-Chloroethyl) ether
mg/kg
ND
ND
30
bis(2-Ethylhexyl)phthalate
mg/kg
ND
ND
30 v2
Butylbenzylphthalate
mg/kg
ND
ND
30
Chrysene
mg/kg
ND
ND
30
Di-n-butylphthalate
mg/kg
ND
ND
30
Di-n-octylphthalate
mg/kg
ND
ND
30
Dibenz(a,h)anthracene
mg/kg
ND
ND
30
Dibenzofuran
mg/kg
ND
ND
30
Diethylphthalate
mg/kg
ND
ND
30
Dimethylphthalate
mg/kg
ND
ND
30
Fluoranthene
mg/kg
ND
ND
30
Fluorene
mg/kg
ND
ND
30
Hexachloro-1,3-butadiene
mg/kg
ND
ND
30
Hexachlorobenzene
mg/kg
ND
ND
30
Hexachlorocyclopentadiene
mg/kg
ND
ND
30
Hexachloroethane
mg/kg
ND
ND
30
Indeno(1,2,3-cd)pyrene
mg/kg
ND
ND
30
Isophorone
mg/kg
ND
ND
30
N-Nitroso-di-n-propylamine
mg/kg
ND
ND
30
N-Nitrosodimethylamine
mg/kg
ND
ND
30
N-Nitrosodiphenylamine
mg/kg
ND
ND
30
Naphthalene
mg/kg
ND
ND
30
Nitrobenzene
mg/kg
ND
ND
30
Pentachlorophenol
mg/kg
ND
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: CRP.003
Pace Project No.: 92623549
SAMPLE DUPLICATE: 3760698
Parameter
Phenanthrene
Phenol
Pyrene
Pyridine
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
Units
92623619005
Result
Dup
Result
mg/kg
ND
ND
mg/kg
ND
ND
mg/kg
ND
ND
mg/kg
ND
ND
%
66
45
%
66
63
%
50
41
%
57
56
%
56
52
%
70
68
Max
RPD RPD Qualifiers
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC.
Page 27 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CRP.003
Pace Project No.: 92623549
QC Batch: 721884 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92623549001, 92623549002
SAMPLE DUPLICATE: 3761243
Parameter
Percent Moisture
SAMPLE DUPLICATE: 3761246
Parameter
Percent Moisture
92623950001 Dup
Units Result Result
37.4 37.8
92624000001 Dup
Units Result Result
% 76.6 76.3
Max
RPD RPD Qualifiers
1 25 N2
Max
RPD RPD Qualifiers
0 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 33

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: CRP.003
Pace Project No.: 92623549
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2022 11:28 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: CRP.003
Pace Project No.: 92623549
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92623549001
Stock
Pile-15
EPA 3546
721862
EPA 8081 B
721983
92623549001
Stock
Pile-15
EPA 3050B
748987
EPA 6020B
749259
92623549001
Stock
Pile-15
METHOD
749043
EPA 7471 B
749197
92623549001
Stock
Pile-15
EPA 3546
721805
EPA 8270E
721980
92623549002
Stock
Pile-15B
EPA 5035A/5030B
721612
EPA 8260D
722046
92623549001
Stock
Pile-15
SW-846
721884
92623549002
Stock
Pile-15B
SW-846
721884
Date: 09/14/2022 11:28 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 30 of 33

DC# Title: &NV FIRM-HUNI.00" v0i Tech Spec Sample Condition 1
Upon Receipt
Effective Date: OSlI 0 22
I �
Uboratory receiving samples:
Asheville ❑Eden ❑ Greenwood ❑ Nentersvilfe ❑ Raleigh Mechanicsville❑ Atianta❑ Kamersville❑ ;
Sample condition upon Client Name:
Receipt
Project #:
92623549
❑ commercial ace Elmer:
:
Carrier Tracking Number:
Custody Seal Present? ❑Yes 16No Seals intact? ❑Yes oateftitiais Person Examining Contents:
Packing Material: ❑Bubbfe Wrap 21Bubble Bags ❑None �❑ Other Biological Tissue Fro n? y
Thermometer: ❑ IR Gun 1D: S Type of fes: Efw'et []Blue
Cooler Temp ('C }:. 3 Correction Factor: Add / Subtract ('C }
Corrected Cooler Temp ('C)-
USDA Regulated Soil (Z'N/A, water sample)
Did samples ginate in a quarantine zone within the united States: CA, NY, or SC (check maps)?
❑Yes nNo
[]Yes []No VIA
❑ iYone
Temp shoufd be above freezing to 6'C
❑5anples out of temp criteria. Samples on ice, coaling process
has begun
Did samples originate from a foreign source (€nternatlonally,
including Hawaii and Puerto Rico)? []Yes �o
Comments/Discrepancy:
iri;of
es
1
-S�ilPle3`ATri4�Withi€iFtel�"€'1mE?-4—°-
_.��_�..�,_ �,_�❑No-. .[]�/A _
�-
Short Hoid Tlme,Analys€s i<72 hr.1?
- - OYes
o
❑N/.a
3
Rush Turn Around Time Requested?
Yes
o
❑ N/A
4.
Sufficient Volume?
A fC
ONO
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
Yes
❑No
Na
❑N/A
N/A
6.
ontainen 7
es
ON.
❑N/A
7.
Dissolved anaiys€s: Samples Field Filtered? ❑Yes
❑No
N/A
S.
Sample Labels Match COC?
-includes Date�me/iD/Anafysis
]?es
k
Matrix: 5 L
❑ Na
❑N/A
9.
Headspace in VOA Vials ?S-6mm}?
❑Yes
ON.
N/A
10.
Trip Blank Present?
Trip Blank. CustodySeals Present?
❑Yes
Yee
ONO
No
A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Temp tog: Temp must be maintained
at <& C during fagin; record temp
every 2© minutes.
Tiine opened; Teinp:
Time.. not;" Cooler
Time:. Tetnp:
Person Contacted: Date/Troe:
Project Manager SCURF Review: slate: --
Field Data Required? ❑Yes ❑Ho
Project Manager SRF Review
Lot iD of spilt containers:
CLIENT NOTIFICATION/RESOLUTION
Date:
Qualtrax Document ID: 70677 Page 1 of 2
II
s
I
3
i

DC# Tifle: ENV-FRM-HUNT-0084 01 Tech Spec Sample Condition
Upon Receipt
i Effective Date: 05M21202
*Check mark top ha!€ of box if pH and/or dechlorination Project #
Is verified and within the acceptance range for
preservation samples.
Eueptions: VOA, Coiiiarm, TOC, Oil and Grease, OROISDIS (water) DOC, LLHg
***Check all unpreserviad Nitrates for chlorine
92623549
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pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot ii
777
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy qr mrs roan will Lie sane io the worm aroma utnr+n Lerrnicaaan urnee ti.e.
Out of hold, incorrect preservative, out of temp, incorrect containers}
Qualtrax Document R 70677 Page 2 of 2

ITEM #
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(Y/N)
Page 33 of 33

Appendix B
Export Soil Truck Logs

Tw"
(919)-270-7010
info @ fc 11-t rucking.ca m
Date: _ Truek#: _
Customef Name; _ �l
Dump Site
lart Ttme,. #PM End Time. —*A
MatwWs Hauled: Cad Dirt
Load u nt'
Ld Times:
Notes:
Myers ignalure; _N� ,_
Fomm n's Sign@ U -
TICKETS MUSY BE SIGNE a BY $08 FOREMAN AND
TUIRNEDIN CAILY
�E

1040
114p1l11
F- 11
(-9191'270-7010
info@fC11-truCki ng. Co m
Dab.. --' Truk#;
Cusummr Name:
Lod.site , _ 4 :-
dark Tme: M End Tara, �Ah
MaWals Muled; W
oskm (type)
OIhar_
Low Cwnt e4 I,
kLOW RM,

------------------
1
r
'
■:ri�+lliiirll
�
N EYNRJ: Cep vlf- 520 M
STONE TYPE HAULED}
RICDLXT HAULM WjFd l7 �R ASPHALT USM4
FO REMM'5SIGNATl,J� 4 _ .
DAVER 5 51 ATUK; �-
CMCIE GNE; � UINT-AXLE TWAXLE CWD-AXLE TRKTOR
�O�I+IMFNTS:
7fCI.KAR kV-ELiCW) OFF

0
Ila-
$1
ST[MET FE FrAULEat --
FORDAWS SWAATURE:
CIRCLEONE; CMKF-�L 7�AXU QUAD -AXLE 1RMM-a
COhWENT
COhfT'R+�T�IR 1Rl�C 'KELL�+YM

r f �

02475
T{A1ViE OF OMTAACTM
PLTmAwff PtTMARRY K$ I 100
MWya VffPAM-Of i AMMIL DEPARTURE
kl�
IFWCK
SIGN WnMt., .0 e2
SIGN TIME: -00 y M
WNCIH: SAL HAS:
COWENTS
JOB NAJtiiEIkUM9ER:k
5TONET► RE HAULEI}
PFlGDLF.7H LlLED: [CIRCLECNJQ GIRT MILLING ASPIOLT BRUSH
F0RENM'; 5KJM7URE;
ORMFrk G
NATtiFlF_ s
EIRCLIE (0147-AML! tffi-AXLE QUAD -AXLE Tfk u(*
C ENTS-

twz�-,-L
070
1�Mf 0� C�91IT5iA�T�fI
4
W TAM I JLO4Y
'��U kj-;j L
#IGIY i14�00SPWOu7
$�FamNU:5►ppHArAfPt —
pq HAEjLM fCJRCLEOW
F� 509HATURE.
DArnNs LMRJ� —COCLEONE
DiHT MLLJI*G * pE#�41T BRUSH
TFdJXLf
QUAD -AXLE

+ KLT &la PC
a —
PlI-OJAHxr r4ra �h AA JOB
Uvk, IET 14;s� Itly� OdP�pT1x� J
u
I
1+
h'F
1*
I.,
T
�q
�G
27
$TO ETYFF!•AU4EJY. —
pADOLiC71HAUL E0: {CIRCLE 0NC1
FOREMAN'S SFGNAIVn:
DA"A-S PI NATUK.
CACtE # Imo'
C=;V
�T)
MM.1*. G 'r MW'u -L do
er r,r m�WI

2843
Fc=1 I
TnuCKinGs
NOMJ
(919)-270-7010
i nfo@fc11-trucki ng, com
Date: Z� Truck# -
Customer Name: CA .1 1/1'
Load Site.`
Dump Site
Start Time
Materials �
ElStone (type)
Other:
Load fount:
Load Times -
Notes:
Drivers Signature4.
Foreman's Signature:
W-I
I
TICKETS M UST BE SIGN ED BY JOB FORE MAN AN D
TURNED IN DAILY

2360
P
Date: l,�%
(919)-270-7010
t nfo@fc11-trucking. c0m
0
Truck#.- --L�
Customer Name:�11 �
Load Site
Dumb Site
Start Time: � DJ M
Materials Hauled: 1k, irt
Ir
End Time: t
[]Stone (type)
Other:
Load Count.
Load Times:
Notes:
7
DhveTs Signature.,
Forernan's Sign ure;
1
0
4
TICKETS MUST BE SIGNED BY JAB FIREMAN AND
TURNED IN DAISY