25091_Lee's Truck Stop Brownfields Assessment Report_20240118

Brownfield Assessment Report
Brownfields Project Name: Lee’s Truck
Stop
Charlotte, North Carolina
S&ME Project No. 215740 REV-1
Brownfields Project No. 25091-21-060
PREPARED FOR:
100 Dalton, LLC
2100 Crescent Avenue, Suite 200
Charlotte, North Carolina 28207
PREPARED BY:
S&ME, Inc.
2016 Ayrsley Town Boulevard, Suite 2-A
Charlotte, North Carolina 28273
Corporate Registration of NC Geologists No. C-145
NC Engineering Firm No. F-0176
January 18, 2024
S&ME, Inc. | 2016 Ayrsley Town Boulevard, Suite 2-B | Charlotte, NC 28273 | p 704.523.4726 | www.smeinc.com
January 18, 2024
North Carolina Department of Environmental Quality
Division of Waste Management, Brownfields Redevelopment Section
450 West Hanes Mill Road, Suite 300
Winston Salem, North Carolina
Attention: Mr. Seth Titley via email: [e-mail]
Brownfields Project Manager
Reference: Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
Brownfields Project # 25091-21-060
Dear Mr. Titley:
S&ME, Inc. (S&ME), on behalf of our client, 100 Dalton, LLC, is submitting this Brownfields Assessment Report to
summarize assessment activities conducted at the Lee’s Truck Stop property located at Dalton Avenue and North
Tryon Street in Charlotte, Mecklenburg County, North Carolina (i.e., “subject property”) based on the approved
Work Plan for Soil and Soil Gas Assessment – Revision 1 dated October 10, 2023. This report summarized work
conducted at the subject property in October 2023.
S&ME appreciates the opportunity to provide our services on this project. Please contact us at your convenience
if there are questions regarding the information contained in this report or if we can be of further service.
Sincerely,
S&ME, Inc.
Sarah Taylor Carl H. Hewett
Staff Scientist Environmental Operations Manager
Wayne H. Watterson, P.E.
Principal Engineer
North Carolina Geology License Certification #C-145 and Engineering License Certification #F-0176.
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 i
Table of Contents
CERTIFICATION ...................................................................................................................... 1
1.0 Introduction ....................................................................................................................... 2
2.0 Project Background ........................................................................................................... 2
2.1 Project Information ........................................................................................... 2
2.2 Site Description.................................................................................................. 3
2.3 Project Description ............................................................................................ 4
3.0 Limitations.......................................................................................................................... 4
4.0 Field Activities ................................................................................................................... 5
4.1 Project Coordination ......................................................................................... 5
4.2 Underground Utility Locating Services ......................................................... 6
4.3 Soil Assessment Activities ............................................................................... 6
4.4 Soil Vapor Sampling ......................................................................................... 7
5.0 Laboratory Results ............................................................................................................ 8
5.1 Soil ....................................................................................................................... 8
5.2 Soil Gas ............................................................................................................... 8
5.3 NCDEQ Risk Calculator ................................................................................... 8
5.4 Laboratory Quality Assurance/Quality Control ........................................... 9
6.0 Investigation-Derived Waste .......................................................................................... 9
7.0 Work Plan Deviations .................................................................................................... 10
7.1 Soil ..................................................................................................................... 10
7.2 Soil Gas ............................................................................................................. 10
8.0 Summary and Conclusions ........................................................................................... 10
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 ii
8.1 Summary .......................................................................................................... 10
8.2 Conclusions ...................................................................................................... 11
9.0 Limitations........................................................................................................................ 11
Figures
Figure 1 – Vicinity Map
Figure 2 – Site Map
Figure 3 – Soil Sampling Results Map
Figure 4 – Soil-Gas Sampling Results Map
Tables
Table 1 – Soil Analytical Results
Table 2 – Soil-Gas Analytical Results
Appendices
Appendix I – Field Notes
Appendix II – Boring Logs
Appendix III – Photographs
Appendix IV – Pace Laboratory Report - Soil
Appendix V – Pace Laboratory Report – Soil-Gas
Appendix VI – NCDEQ Risk Calculator
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 2
1.0 Introduction
S&ME, on behalf of our client, 100 Dalton, LLC, has completed a soil and soil gas assessment at Lee’s Truck Stop
(subject property) located at the intersection of Dalton Avenue and North Tryon Street in Charlotte, Mecklenburg
County, North Carolina. The activities completed during this assessment were conducted in accordance with the
Work Plan for Soil and Soil Gas Assessment – Revision 1 dated October 10, 2023, and approved by the North
Carolina Department of Environmental Quality (NCDEQ) Brownfields Redevelopment Section (BRS) on
October 27, 2023. Our client, 100 Dalton, LLC, intends to develop the subject property under the NCDEQ BRS.
This report was revised on January 17, 2024 to incorporate revised risk calculator values.
2.0 Project Background
2.1 Project Information
The subject property contains approximately 1.97 acres, and it is comprised of four adjoining Mecklenburg County
tax parcels. The following tax parcel information was obtained from the Mecklenburg County Property Ownership
and Land Records System (POLARIS) website:
Parcel ID Associated Address Current
Property Owner Acreage
07901506 1601 N Tryon Street
100 Dalton Avenue
100 Dalton, LLC /
Cardon Capital, LLC 1.272
07901503 113 Sylvania Avenue 100 Dalton, LLC /
Cardon Capital, LLC 0.189
07901502 109 Sylvania Avenue 100 Dalton, LLC /
Cardon Capital, LLC 0.191
07901501
1621 N Tryon Street
1623 N Tryon Street
1625 N Tryon Street
100 Dalton, LLC /
Cardon Capital, LLC 0.297
The subject property was developed with a residential structure and a retail building in the 1930’s. A retail
gasoline station, service building, and a truck stop were constructed in the early 1950’s. The gasoline station/truck
stop facility was operated until the 2000’s. Ten petroleum underground storage tanks (USTs) were removed from
three separate tank basins in June 2008. Petroleum contamination was identified in the soil and groundwater, and
NCDEQ assigned Incident #36534 to the Lee’s Truck Stop petroleum release. No further assessment or
remediation associated with the UST release(s) was conducted after the completion of the tank removal.
S&ME has completed the following due diligence assessments with respect to the subject property:
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 3
Phase I Environmental Site Assessment (ESA) dated August 31, 2021. At the time of the Phase I ESA,
the subject property was developed with three buildings (convenience store, garage building, and retail
building). The subject property had a variety of different tenants, including an automobile body shop, a
tire store, a paint and body shop, a clothing store, a car sales facility, and a homeless encampment. The
following recognized environmental conditions (RECs) were identified during the assessment:
The 10 former petroleum USTs were removed from three separate UST basins in June 2008. A
petroleum release was identified and assigned NCDEQ Incident #36534.
Several areas of petroleum surface staining observed in the grassy area on the western portion of the
subject property, in the vicinity of two waste oil aboveground storage tanks (ASTs), at a damaged 55-
gallon drum, and adjacent to an automobile repair area.
Evidence of two former in-ground hydraulic lifts was noted in the garage service bays.
A floor drain was observed in the garage building occupied by the tire store. In addition, a metal
cover of unknown purposes was observed behind the garage building. Based on the presence of the
floor drain and the location of the metal cover, it is possible that the metal cover is associated with a
potential vault/sump that is connected with the underground drain in the garage building.
Limited Phase II Environmental Site Assessment dated February 1, 2022. S&ME completed Limited
Phase II ESA activities between November and December 2021 to assess the RECs identified during the
August 2021 Phase I ESA. Field activities performed during the assessment included underground utility
locating, soil sampling, groundwater sampling, and sub-slab vapor sampling. Petroleum impacted soil,
groundwater, and sub-slab vapors were identified during the assessment. The Limited Phase II ESA was
revised in September and October 2022 to incorporate comments from the BRS.
Additionally, S&ME conducted lead-based paint and asbestos containing materials (ACM) surveys on the site
buildings in November 2021. Three reports were prepared to document the assessment findings. The buildings
were demolished under the direction of 100 Dalton, LLC, and the site was cleared in the first half of 2022. The
subject property is currently vacant and unoccupied.
2.2 Site Description
The subject property is located northwest of the intersection of Dalton Avenue and North Tryon Street in
Charlotte, North Carolina. See Figure 1. The subject property is currently vacant. The majority of the ground
surface at the subject property is developed as a gravel parking lot. Foundations from the former buildings
remain on the subject property. For a period of time between the demolition of the site buildings and the
assessment described in this report, the subject property was used for tractor-trailer parking. A Site Map is
provided as Figure 2.
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 4
2.3 Project Description
In November 2022, Mr. Seth Titley, Project Manager with the BRS, requested that S&ME perform additional
assessments at the subject property to specifically evaluate residential use as an additional approved use under
the forthcoming Brownfields Agreement for this Brownfields Property. Mr. Titley requested the following
assessment scope of activities:
Collection of two soil samples from the northwestern corner of the subject property near soil staining that
was observed by the NCBRS during a September 2022 site visit.
Collection of one additional soil sample from an area of staining near a soil sample previously collected
during S&ME’s Phase II ESA.
Collection of six soil gas samples from areas where the proposed residential structures will be located.
The preparation of a Brownfields Work Plan to be reviewed and approved by the BRS.
A Work Plan for Soil and Soil Gas Assessment was submitted to the BRS on September 14, 2023. The Work Plan
was revised on October 10, 2023, and approved by Mr. Titley on October 27, 2023. The following Scope of Work
was proposed by S&ME and approved by the BRS:
S&ME will perform nine soil borings using either hand auger or direct-push technology. Three soil
borings will be extended to a depth two feet below ground surface (bgs) to assess surficial soil conditions,
and six soil borings will be extended up to 15 feet bgs to install soil gas implants (SGIs).
One soil sample will be collected from each of the nine soil borings for certified laboratory analysis.
S&ME will collect soil gas samples from six locations as requested by Mr. Titley.
Sampling and assessments will be conducted in general accordance with the following guidance manuals:
NCDEQ Inactive Hazardous Sites Branch (IHSB), Guidelines for Assessment and Cleanup of
Contaminated Site (July 2021)
NCDEQ Division of Waste Management, Vapor Intrusion Guidance (March 2018)
U.S. Environmental Protection Agency (EPA) Region IV Science and Ecosystem Support Division (SESD)
Field Branches Quality System and Technical Procedures
3.0 Limitations
This report and its conclusions are limited to the area where the assessment was conducted and does not
represent a comprehensive assessment of the entire site. This work does not necessarily include the level of
specificity required of technical standards that govern full characterization of the environmental conditions of the
subject property. Moreover, the assessment objectives were specific to those identified by 100 Dalton, LLC and
may not be appropriate to the needs or business objectives of others. Use of this report by any third parties will
be at such party’s sole risk except when granted under written permission by S&ME. Furthermore, this scope did
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 5
not include (and was not intended to include) the level of detail and assessment effort (and corresponding cost)
necessary to identify all potential regulated substance release sources.
Except as may have been measured by groundwater elevation or other quantifiable data, the primary direction of
groundwater flow was assumed to be dictated by topography. Additionally, except as may have been measured
by lateral delineation based on quantifiable data, the groundwater flow direction was assumed to control the
distribution of impact, if present.
S&ME's professional services have been performed using that degree of care and skill ordinarily exercised, under
similar conditions, by environmental consultants undertaking similar studies and practicing in this locality. No
other warranties, express or implied, is intended or made with respect to this report or S&ME’s services. This
assessment was not exhaustive, and users of this report should consider the scope and limitations of, and related
to, these services when developing their opinions as to environmental risks associated with the subject property.
4.0 Field Activities
4.1 Project Coordination
S&ME conducted several project management activities prior to initiating field work on this project. Preliminary
project management and coordination work included the following:
S&ME contacted the North Carolina 811 website to submit a ticket for utility locating for the subject
property. North Carolina 811 identifies public utilities and pipelines that may be located on the subject
property.
S&ME prepared a subcontract agreement with Probe Utility Locate (Probe Utility) of Huntersville, North
Carolina for underground utility locating services and coordinated a site visit for activities with Probe
Utility and S&ME personnel.
S&ME prepared a subcontract agreement with JG Drilling of Easley, South Carolina for drilling services
and coordinated a site visit for activities with JG Drilling and S&ME personnel.
S&ME obtained laboratory-provided containers, coolers, and chain of custody documentation from Pace
Analytical (Pace) located in Huntersville, North Carolina for the sampling activities to be conducted at the
site.
S&ME prepared a site-specific Health and Safety Plan (HASP) in accordance with 29 CFR 1910.120 for the
field work to be performed at the subject property.
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 6
4.2 Underground Utility Locating Services
S&ME retained Probe Utility to conduct subsurface locating using ground-penetrating radar (GPR) and
electromagnetic (EM) services to clear potential boring locations of possible subsurface utilities/interferences.
Utility locating was conducted on October 24, 2023. Ms. Sarah Taylor and Mr. Matthew Brundage of S&ME were
on site during field activities.
4.3 Soil Assessment Activities
S&ME and JG Drilling mobilized to the subject property on October 24, 2023 and collected 10 soil samples
(SB-SG-1 through SB-SG-6, SB-11 through SB-13, and SB-DUP). Soil samples were collected using a track-
mounted Geoprobe 6712DT drill rig equipped with direct push technology (DPT).
Soil samples SB-SG-1 through SB-SG-6 were collected from the soil gas implant locations. Soil profiles were
collected in five-foot intervals from each boring using Macro-Core acetate sleeves. Each five-foot interval was
split and placed into two zip top bags. One bag was placed on ice while the other bag was allowed to reach
ambient temperature before being screened for the presence of volatile organic compounds (VOCs) with a
calibrated Mini-Rae photoionization detector (PID). The five-foot interval from each boring that exhibited the
highest PID readings or contained visual and/or olfactory signs of potential contamination was selected for
laboratory analysis. Since the PID readings for the boring were relatively similar, the sample from boring SG-3 was
selected from the top five-foot interval based on the presence of signs of potential contamination rather than the
highest PID reading. The soil from the iced portion of the selected interval was placed in laboratory provided
containers and submitted for laboratory analysis.
Soil samples SB-11 and SB-12 were collected from the northwest corner of the subject property where surface
staining was observed by the BRS. Soil sample SB-13 was collected from an area of staining where a sample was
previously collected during S&ME’s Phase II. Soil profiles were collected in two-foot intervals from each sample
locating using Macro-Core acetate sleeves. Each one-foot interval was split and placed into two zip top bags.
One bag was placed on ice while the other bag was allowed to reach ambient temperature before being screened
for the presence of VOCs by a calibrated PID. The one-to-two-foot interval was selected for laboratory analysis
based on the lack of recovery from the zero-to-one-foot interval in borings SB-11 through SB-13. The soil from
the iced portion of the selected interval was placed in laboratory provided containers and submitted for
laboratory analysis. A duplicate soil sample (SB-DUP) was collected from soil boring SB-11.
The soil samples were submitted for analysis of VOCs by EPA Method 8260, semi-volatile organic compounds
(SVOCs) by EPA Method 8270, 8 RCRA Metals by EPA Method 6020/7471, and hexavalent chromium by EPA
Method 7199. Prior to sample collection, the sample containers were labeled with identification numbers,
requested analysis, sample date and time, and after collection, the sample containers were placed into a cooler
with ice. The soil samples were delivered by S&ME under chain of custody procedures to the Pace laboratory for
analytical testing.
Soil sample locations are illustrated in the Figure 3. Field notes are included in Appendix I. Boring logs are
provided in Appendix II.
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 7
4.4 Soil Vapor Sampling
On October 24, 2023, S&ME observed as JG Drilling installed six soil gas implants (SGIs) at the subject property.
Five SGIs (SG-1, 2, 3, 4 and 6) were installed to depths of 10 to 15 feet bgs as described in the approved Work Plan
(see Section 2.3). The SGI at sample location SG-5 was installed to approximately 4 feet bgs, based on observed
soil moisture at location SG-5 (see Section 7.2). Each soil gas sampling point was constructed using a Geoprobe
SGI and an anchor connected to dedicated Teflon tubing inserted into an approximate 2.23-inch diameter hole.
Medium-to-fine grained sand was placed in the annular space around the SGI and tubing to a level approximately
nine inches above the top of the screen on the SGI. The annular space above the sand pack was filled with a
bentonite seal to the ground surface.
Following installation, S&ME performed a leak test on each SGI. A plastic shroud was placed over the SGI
installation area. The tubing from the SGI was fitted through the shroud and attached to a Tedlar bag. Helium
(tracer) gas was then injected into the plastic shroud. Three volumes of air were purged from each SGI using an
air pump at a rate less than 200 milliliters per minute. Following completion of the purging process, tracer gas
was not detected at concentrations above 10% of the shroud concentration in the SGIs; therefore, the SGIs were
considered leak-free. Each SGI point was capped for at least 24 hours upon the completion of the leak tests.
On October 30, 2023, S&ME returned to the subject property to collect soil gas samples from each SGI. Prior to
sample collection, a leak test was performed on each sampling array. A brass T-connector was attached to the
end of the SGI tubing. A section of Teflon tubing was connected to one part of the T-connector while a batch-
certified one-liter summa canister was connected to the other part of the T connector. A plastic shroud was
placed overtop the sampling array and summa canister. The other section of tubing from the T-connector was
fitted through the shroud and attached to a helium detector. S&ME then injected tracer gas into the plastic
shroud. The sampling array was monitored for leaks by monitoring for the presence of helium gas concentrations
within the Teflon tubing. Tracer gas was not detected through the sampling array, and the sampling array was
considered leak free.
After successfully passing the leak test, the leak detection shroud was removed and at least three volumes of air
were purged from the sampling array using a calibrated low flow pump (similar to a personal air monitoring
pump) at a rate of approximately 200 milliliters per minute. After purging the sampling array, the valve to the
one-liter summa canister was opened to allow the collection of a soil vapor sample. The sample collection rate
was set with a one-hour regulator. Pressure readings of the summa canisters were recorded at the start and end
of collection. A residual vacuum of approximately -5 inches of mercury was left in the summa canisters upon
completion of the sampling event.
Once the soil gas samples were collected, the samples were shipped under standard chain-of-custody protocol to
Pace to by analyzed for VOCs including naphthalene by EPA Method TO-15. A duplicate sample of SG-6 was
collected for quality assurance purposes.
The locations of the SGIs are illustrated on Figure 4.
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 8
5.0 Laboratory Results
5.1 Soil
Analytical testing of the soil samples indicated the presence of arsenic in excess of its NCDEQ Residential Health-
Based Preliminary Soil Remediation Goal (PSRG) of 0.68 milligrams per kilogram (mg/kg) in eight of the 10
analyzed samples, including the duplicate sample. Arsenic concentrations also exceeded the
Industrial/Commercial PSRG of 3.0 in four of the 10 analyzed soil samples, including the duplicate sample.
Analytical testing of sample SB-SG-2 indicated the presence of hexavalent chromium in excess of its Residential
PSRG of 0.31. Analytical testing of the other soil samples indicated the presence of Hexavalent chromium at
estimated “J flagged” concentrations in excess of its Residential PRSG in eight of the nine other analyzed soil
samples, including the duplicate sample.
Several additional target metals, VOCs, and SVOCs were detected in the soil samples at concentrations greater
than the laboratory MDLs and/or at “J flagged” concentrations, but below the applicable Residential PSRGs,
Industrial/Commercial PSRGs, and the Protection of Groundwater PSRGs.
Soil analytical results are summarized in Table 1, which includes the applicable NCDEQ PSRG action levels for
comparison. A copy of the Pace soil analytical report is included in Appendix IV.
5.2 Soil Gas
Analytical testing of the soil gas samples indicated the presence of naphthalene in the seven soil gas samples,
including the duplicate sample, at concentrations in excess of the residential Vapor Intrusion Screening Level
(VISL) of 2.8 micrograms per cubic meter (µg/m3).
Total xylenes were detected in sample SG-6 at a concentration in excess of the residential VISL of 700 µg/m3.
No other target VOCs were detected in excess of their respective VISLs for residential or non-residential usage.
Soil gas analytical results are summarized in Table 2, which includes the applicable NCDEQ VISLs for comparison.
A copy of the Pace soil gas analytical report is included in Appendix V.
5.3 NCDEQ Risk Calculator
The maximum concentrations of each detected analyte in the soil and soil gas samples were input in the NCDEQ
Risk Calculator to assess the calculated risk factor for direct contact and vapor intrusion to indoor air based on the
calculated cumulative carcinogenic risk of 1x10-4 and the cumulative non-carcinogenic hazard quotient of 1. The
following table summarizes the results from the NCDEQ Risk Calculator (included as Appendix VI):
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 9
Pathway
Cumulative
Calculated
Carcinogenic
Risk
(Target 1x10-4)
Target
Carcinogenic
Risk Exceeded?
Cumulative
Calculated Non-
Carcinogenic
Hazard Quotient
(Target 1)
Target Non-
Carcinogenic
Hazard Quotient
Exceeded?
Direct Contact –
Residential Soil 1.3x10-5 No 0.22 No
Direct Contact –
Non-Residential
Worker Soil
1.8x10-6 No 0.016 No
Direct Contact –
Construction Worker
Soil
8.1x10-7 No 0.12 No
Direct Contact –
Recreator/Trespasser
Soil
7.4x10-6 No 0.12 No
Vapor Intrusion –
Resident Soil Gas to
Indoor Air
1.4x10-5 No 0.66 No
Vapor Intrusion –
Non-Residential
Worker Soil Gas to
Indoor Air
1.0x10-6 No 0.052 No
Based on the results of the NCDEQ Risk Calculator, the cumulative target carcinogenic risk and target
non-carcinogenic hazard quotient are not exceeded for direct contact with soil and for vapor intrusion.
5.4 Laboratory Quality Assurance/Quality Control
A North Carolina certified laboratory was used for the soil and soil gas analyses. Samples were handled between
S&ME and the laboratory under standard chain-of-custody procedures. The laboratory performed their analyses
according to a Level II Quality Assurance level. A duplicate soil sample was collected from soil sample SB-11. A
duplicate soil gas sample was collected from SG-6. Based on a comparison of the data sets and the similarity in
results, the soil and soil gas results appear consistent.
6.0 Investigation-Derived Waste
A limited volume of soil cuttings was generated during assessment activities. Soil cuttings were spread onsite.
Light petroleum odors were noted within a small portion of soil collected from soil boring SB-SG-3. The entire
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 10
volume of soil exhibiting odors was collected for laboratory analysis; therefore, no soil was containerized and
disposed off-site.
7.0 Work Plan Deviations
7.1 Soil
Based on the field activities completed for the soil assessment, S&ME does not report deviations from the Work
Plan.
7.2 Soil Gas
Based on the field activities completed for the soil gas assessment, S&ME does not report deviations from the
Work Plan, with the following exception:
The Work Plan states that the SGIs would be installed between 10 and 15 feet bgs. The soil boring at SG-
5 encountered wet soil conditions at approximately 7 feet bgs. No evidence of an underground storage
tank (UST), other underground structure, or evidence of a release was observed at location SG-5 during
the completion of soil boring SG-5. The source of moisture at SG-5 was not determined. The boring was
backfilled with sand and soil, and new (offset) boring SG-5 was extended to four feet bgs, where the SGI
was installed.
8.0 Summary and Conclusions
8.1 Summary
Soil and soil-gas assessment activities were conducted in October 2023. The following summarizes the work at the
subject property during this project:
S&ME collected 10 soil samples, nine record samples and one duplicate, on October 24, 2023. Arsenic
and hexavalent chromium were detected in one or more of the soil samples at concentrations greater
than the Residential PSRGs. Additionally, arsenic was detected at concentrations greater than the
Industrial/Commercial PSRGs in four of the soil samples.
S&ME collected seven soil gas samples, six record samples and one duplicate, on October 30, 2023.
Naphthalene and total xylenes were detected in one or more of the soil gas samples at concentrations
greater than the Residential VISLs. No target compounds were detected at concentrations greater than
the Non-Residential VISLs.
S&ME input the maximum reported concentrations of each detected analyte in the soil and soil gas
samples into the NCDEQ Risk Calculator to assess the calculated risk factor for direct contact and vapor
Brownfields Assessment Report
Lee’s Truck Stop
Dalton Avenue and North Tryon Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740 REV-1
January 18, 2024 11
intrusion to indoor air based on the calculated cumulative carcinogenic risk of 1x10-4 and the cumulative
non-carcinogenic hazard quotient of 1. Based on the results of the NCDEQ Risk Calculator, the cumulative
target carcinogenic risk and target non-carcinogenic hazard quotient are not exceeded for direct contact
with soil or for vapor intrusion.
8.2 Conclusions
The following conclusions are based on the field activities and findings of this assessment:
Arsenic was detected at concentrations above the Residential and Industrial/Commercial PSRGs in several
of the soil samples collected from the site. The highest detected concentration was 4.54 mg/kg in soil
sample SB-SG-5. According to the Geochemical Landscapes of the Conterminous United States – New Map
Presentations for 22 Elements prepared by the U.S. Geological Survey in 2001, arsenic is typically found at
concentrations up to 6.3 mg/kg in the Charlotte region. The assessment activities do not suggest arsenic
to be a contaminant of concern at the site related to anthropogenic causes as the detected arsenic
concentrations, while generally exceeding the Residential and Industrial Commercial PSRGs, do not appear
to be grossly elevated and generally fall within the ranges documented in the USGS paper previously
referenced.
Hexavalent chromium was detected at a concentration above the Residential PSRG in soil sample SB-SG-2.
Hexavalent chromium was also reported at “J flagged” estimated concentrations in eight of the nine other
soil samples, including the duplicate. Based on the analytical results, it appears that low concentrations of
hexavalent chromium are present in the soil at the site.
Based on the results of the NCDEQ Risk Calculator, the target carcinogenic risk and target non-
carcinogenic hazard quotient are not exceeded for direct contact with soil and for vapor intrusion.
Therefore, based on the results of the NCDEQ Risk Calculator for the data set obtained for this report,
vapor mitigation does not appear to be warranted.
9.0 Limitations
The conclusions included in this Brownfields Assessment Report are based on: S&ME’s observations of existing
site conditions; our limited understanding of the site history; and the results of a limited program of subsurface
exploration, sample screening, and chemical testing. Concentrations of contaminants reported by laboratory
analyses may not be representative of conditions between locations sampled. Conclusions about site conditions
under no circumstances comprise a warranty that conditions in all areas within the site are of the same quality as
those sampled. Further, the conclusions and opinions provided in this report are based on a proposed building
layout, as shown on Figures 3 and 4.
Figures
^_
^_PROJECT LOCATION
SCALE:
PROJECT NUMBER
FIGURE NO.
11 " = 1.0 milesDATE: 11‐22‐23
Drawing Path: T:\ENV\Projects\2021\215740_Ascent RE_Dalton Ave and N Tryon St Phase I ESA_Charlotte NC\GIS\1_vicinity.mxd plotted by DHomans 08-31-2021
VICINITY MAP
³
REFERENCE: ESRI STREETMAP USA DATASETTHIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONSDISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEYINFORMATION, UNLESS STATED OTHERWISE.
Service Layer Credits: Sources: Esri, HERE, Garmin, USGS,Intermap, INCREMENT P, NRCan, Esri Japan, METI, EsriChina (Hong Kong), Esri Korea, Esri (Thailand), NGCC, (c)
0 1 2Miles
215740
LEE'S TRUCK STOP NORTH TRYON STREET AND DALTON AVENUE CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
³●
PLYMOUTH AV
DALTON AV
N TRYON ST
DUNLOE ST
!
DRAINS●○IN-GROUND HYDRAULIC LIFTAPPROXIMATE FORMER UST LOCATIONSAPPROXIMATE EXCAVATION AREAS
SCALE:
PROJECT NUMBER
FIGURE NO
.2
1 " = 50 'DATE: 11-22-23
215740
LEE'S TRUCK STOPNORTH TRYON STREET AND DALTON AVENUECHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
SITE MAP
³
REFERENCE: 2023 AERIAL PHOTOGRAPHGIS BASE LAYERS WERE OBTAINED FROM MECKLENBURG COUNTYAND/OR DURHAM COUNTY NEARMAP. ALL FEATURE LOCATIONSDISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVILSURVEY INFORMATION, UNLESS STATED OTHERWISE.
0 50 100(FEET)
ØØØØØØØØØØØØØØ
●○Ð"I Ð"I
Ð"I
Ð"I
Ð"I
Ð"I
Ð"I
Ð"I
Ð"I
SB-11Arsenic = 2.61 mg/kg SB-12Arsenic = 2.95 mg/kg
SB-SG-4Arsenic = 3.96 mg/kg
SB-SG-5Arsenic = 4.54 mg/kg
SB-SG-6No PSRG Exceedances
SB-SG-3Arsenic = 2.12 mg/kg
SB-13No PSRG Exceedances
SB-SG-1Arsenic = 2.48 mg/kg
SB-SG-2Arsenic = 2.48 mg/kg
Ð"I SOIL SAMPLE LOCATION
APPROX. FORMER UST LOCATIONSAPPROX. EXCAVATION AREAS
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
31 " = 50 '
11-20-23
215740
LEE'S TRUCK STOPNORTH TRYON STREET AND DALTON AVENUECHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
Drawing Path: T:\charlotte-1350\Projects\2021\215740_Ascent RE_Dalton Ave and N Tryon St Phase I ESA_Charlotte NC\Phase II ESA\GIS\BFA\3_SoilResults.mxd plotted by jsherrill 11-20-2023
SOIL SAMPLING RESULTS MAP
³
REFERENCE: 2023 AERIAL PHOTOGRAPHGIS BASE LAYERS WERE OBTAINED FROM MECKLENBURG COUNTYAND/OR DURHAM COUNTY NEARMAP. SITE CONCEPT MAP FROM RBA.ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARENOT BASED ON CIVIL SURVEY INFORMATION, UNLESS STATEDOTHERWISE.
0 50 100(FEET)
NOTES:SAMPLES WERE COLLECTED ON 10/24/2023mg/kg = MILLIGRAMS PER KILOGRAMVALUES SHOWN EXCEED RESIDENTIAL HEALTH PSRGSBOLDVALUES EXCEED THE INDUSTRIAL/COMMERCIAL PSRGS.ONLY VALUES WITH AN EXCEEDANCE OF THE PSRGS ARE SHOWN ONTHIS FIGURE.TABLE 1 SUMMARIZES ALL DETECTED COMPOUNDS, AND THE FULLANALYTICAL REPORT IS INCLUDED AS APPENDIX III.
ØØØØØØØØØØØØØØ
●○
!O
!O
!O
!O
!O
!O
SG-4Naphthalene = 9.06 µg/m3
SG-5Naphthalene = 22.7 µg/m3
SG-6Naphthalene = 5.76 µg/m3Total Xylenes= 847 µg/m3
SG-3Naphthalene = 24.9 µg/m3
SG-1Naphthalene = 27.5 µg/m3
SG-2Naphthalene = 29.5 µg/m3
!O SOIL-GAS SAMPLE LOCATION
APPROX. FORMER UST LOCATIONSAPPROX. EXCAVATION AREAS
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
41 " = 50 '
11-20-23
215740
LEE'S TRUCK STOPNORTH TRYON STREET AND DALTON AVENUECHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
Drawing Path: T:\charlotte-1350\Projects\2021\215740_Ascent RE_Dalton Ave and N Tryon St Phase I ESA_Charlotte NC\Phase II ESA\GIS\BFA\4_SOILGASResults.mxd plotted by jsherrill 11-20-2023
SOIL-GAS SAMPLING RESULTS MAP
³
REFERENCE: 2023 AERIAL PHOTOGRAPHGIS BASE LAYERS WERE OBTAINED FROM MECKLENBURG COUNTYAND/OR DURHAM COUNTY NEARMAP. SITE CONCEPT MAP FROM RBA.ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARENOT BASED ON CIVIL SURVEY INFORMATION, UNLESS STATEDOTHERWISE.
0 50 100(FEET)
NOTES:SAMPLES WERE COLLECTED ON 10/30/2023µg/m3 = MICROGRAMS PER CUBIC METERVALUES SHOWN EXCEED RESIDENTIAL VAPOR INTRUSION SCREENINGLEVELS (VISLS)ONLY VALUES WITH AN EXCEEDANCE OF THE VISLS ARE SHOWN ONTHIS FIGURE. TABLE 2 SUMMARIZES ALL DETECTED COMPOUNDS, ANDTHE FULL ANALYTICAL REPORT IS INCLUDED AS APPENDIX III.
Tables
Sample Interval
(ft-bgs)
Date
Collected
0 - 5 10/24/23 2.48 37.6 < 0.106 42.7 0.94 J 42.7 7.77 0.801 J 0.0459 J 0.0066 < 0.0033 0.10 < 0.0037 < 0.0021 0.0169 J < 0.13 < 0.16
5 - 10 10/24/23 3.05 74.9 < 0.108 44.1 2.0 42.1 12.1 0.812 J 0.0364 J 0.0052 J < 0.0036 < 0.0047 < 0.0040 < 0.0023 < 0.0039 < 0.14 < 0.16
0 - 5 10/24/23 2.12 16.0 < 0.105 39.2 0.57 J 39.2 7.82 0.846 J 0.0381 J 0.0062 0.015 0.0062 0.0055 J 0.0031 J 0.0162 J < 0.13 < 0.16
5 - 10 10/24/23 3.96 14.6 < 0.120 58.4 1.0 J 58.4 6.99 1.01 J 0.0344 J 0.0059 J < 0.0040 0.012 < 0.0045 < 0.0026 0.0054 J < 0.15 < 0.18
0 - 5 10/24/23 4.54 30.5 0.372 J 44.9 0.50 J 44.9 9.80 0.723 J 0.0302 J 0.0066 J < 0.0041 0.0091 < 0.0046 < 0.0026 0.0070 J < 0.15 < 0.18
10 - 15 10/24/23 1.10 J 17.1 < 0.116 24.8 0.75 J 24.8 3.28 0.285 J < 0.0244 0.0054 J < 0.0038 < 0.0050 < 0.0043 < 0.0024 < 0.0041 < 0.15 < 0.17
1 - 2 10/24/23 2.61 11.4 < 0.107 30.0 0.58 J 30.0 4.96 0.972 J 0.0664 0.0056 J < 0.0036 < 0.0047 < 0.0041 < 0.0023 0.0054 J < 0.14 < 0.16
1 - 2 10/24/23 2.95 39.1 0.498 J 43.5 0.46 J 43.5 39.6 1.06 J 0.0739 0.0068 J < 0.0041 0.0084 < 0.0046 < 0.0026 0.0073 J 0.17 J 0.20 J
1 - 2 10/24/23 1.13 J 14.5 < 0.111 13.0 0.20 J 13.0 7.75 0.458 J 0.0250 J 0.0051 J < 0.0037 < 0.0048 < 0.0042 < 0.0024 < 0.0040 < 0.14 < 0.17
1 - 2 10/24/23 3.01 20.6 < 0.104 38.4 0.58 J 38.4 6.89 0.955 J 0.0711 0.030 < 0.0037 0.84 0.0051 J < 0.0024 0.17 < 0.14 < 0.16
Residential 0.68 3,100 1.4 NS 0.31 23,000 400 78 4.7 6.1 2.1 990 63 56 120 480 360
Industrial/Commercial 3.0 47,000 20 NS 6.5 350,000 800 1,200 70 27 8.8 9,700 370 320 530 6,000 4,500
Protection of
Groundwater 5.8 580 3.0 NS 3.8 360,000 NS 2.1 NS 13 0.39 8.3 12 11 9.9 670 440
Notes:
Concentrations are reported in milligrams per kilogram (mg/kg).
ft-bgs - feet below ground surface
NS - Not EstablishedBDL - Below laboratory detection limits
Highlighted - Value exceeds Residential Health Based PSRG Highlighted - Value exceeds Industrial/Commercial Health Based PSRG Only compounds detected in at least one sample are included in this table. The full analytical laboratory report is included in Appendix IV.
Trivalent Chromium values were calculated by subtracting the Hexavalent Chromium analytical results from the Total Chromium analytical results for the respective samples.
J - Estimated Value: analyte detected at or above the laboratory Method Detection Limit (MDL) but below the laboratory Reporting Limit (RL)
BOLD - Value detected above laboratory MDL
PSRG - Preliminary Soil Remediation Goals, July 2023 - North Carolina Department of Environmental Quality (NCDEQ)
PSRG
TABLE 1
SOIL ANALYTICAL RESULTS
Lee's Truck Stop
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740
Selenium 1,2,4-Trimethlbenzene
1,3,5-
Trimethylbenzen
e
Cadmium Fluoranthene
Semi-Volatile Organic Compounds
by EPA Method 8270E
(mg/kg)
SB-SG-3
Toluene PyreneXylenes (total)
SB-DUP
SB-SG-1
SB-SG-2
SB-12
SB-SG-4
SB-SG-5
SB-SG-6
SB-11
SB-13
Volatile Organic Compounds (VOCs) by EPA Method 8260D
(mg/kg)
Analytical Method →
(Unit)
Chromium (Total)Lead MercuryChromium (Trivalent)Chromium (Hexavalent)
Constituent →
Sample ID Barium Ethylbenzene
Metals by EPA Methods 6020/7471/7199
(mg/kg)
Arsenic Naphthalene
Date
Collected
10/30/2023 114 7.06 42.0 < 0.461 < 0.349 1.58 < 0.259 < 0.283 2.15 < 0.267 31.9 B 5.51 1.88 1.86 1.59 < 0.425 < 1.12 20.6
10/30/2023 150 6.32 120 0.571 J < 0.349 < 0.213 < 0.259 < 0.283 2.86 < 0.267 35.1 2.60 2.10 2.94 1.89 37.2 < 1.12 86.7
10/30/2023 53.9 4.25 17.5 0.462 J < 0.349 < 0.213 < 0.259 < 0.283 1.51 < 0.267 20.4 B 7.72 3.81 1.78 1.51 J 6.95 < 1.12 17.4
10/30/2023 37.5 2.12 27.1 3.14 < 0.349 1.77 < 0.259 < 0.283 0.974 < 0.267 35.3 16.3 2.26 1.75 0.623 J 4.25 < 1.12 21.0
10/30/2023 46.6 1.70 17.9 < 0.461 0.891 J 1.65 1.29 < 0.283 < 0.290 < 0.267 72.6 1.40 30.7 2.87 < 0.608 < 0.425 2.10 J 1.90 J
10/30/2023 18.9 1.82 28.2 < 0.461 < 0.349 < 0.213 < 0.259 0.539 J 0.332 J 0.311 J 17.1 B 33.5 4.20 1.80 1.32 J 45.0 < 1.12 42.7
10/30/2023 27.8 1.70 28.8 0.469 J < 0.349 < 0.213 < 0.259 0.534 J 0.330 J < 0.267 17.5 B 35.5 3.58 1.94 1.67 < 0.425 < 1.12 45.5
Residential NS 12 4,900 16 4.1 630 42,000 3.6 58 280 NS 37 NS 700 35,000 2,800 4.3 4,900
Non-Residential NS 160 61,000 200 53 7,900 88,000 47 770 9,500 NS 490 NS 8,800 44,000 35,000 56 61,000
Notes:
Concentrations are reported in microgram per cubic meter (µg/m^3).
NS - No Standard Established
Highlighted - Value exceeds Residential VISL
Highlighted - Value exceeds Industrial/Commercial Non-Residential VISL
Only compounds detected in at least one sample are included in this table. The full analytical laboratory report is included in Appendix V.
Dichlorodifluoromethane
1,1,2-Trichlorotrifluoroethane
1,2-Dichloroethane
1,1-Dichloroethane
trans-1,2-Dichloroethane
Trichlorofluoromethane
Heptane
n-Hexane
Hexachloro-1,3-butadiene
TABLE 2
SOIL-GAS ANALYTICAL RESULTS
Lee's Truck Stop
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 215740
J - Estimated Value: analyte detected at or above the method detection limit (MDL) but below the reporting Limit (RL)
TO-15Analytical Method →
Ethylbenzene
EthanolConstituent →
Acetone
Benzene
Carbon disulfide
Chloromethane
Carbon tetrachloride
BOLD - Value detected above laboratory MDL
Sample ID
SG-1
SG-2
SG-3
SG-4
SG-5
SG-6
DUP
Vapor Intrustion
Screening Levels (VISLs)
Chloroform
Cyclohexane
Date
Collected
10/30/2023 4.36 1.45 < 0.544 43.3 27.5 50.6 < 0.160 1.34 2.61 652 < 1.10 < 0.400 < 0.364 3.28 0.854 J 6.17 0.964 17.8
10/30/2023 5.41 1.58 4.02 J 150 29.5 6.76 666 1.04 17.2 39.9 < 1.10 < 0.400 < 0.364 3.07 0.717 J < 0.621 0.256 J 10.5
10/30/2023 < 0.382 1.19 < 0.544 15.8 24.9 9.76 < 0.160 < 0.335 5.49 750 < 1.10 0.475 J < 0.364 2.81 0.820 J 14.2 0.826 33.6
10/30/2023 2.05 3.14 < 0.544 5.54 9.06 6.83 < 0.160 < 0.335 4.74 189 < 1.10 < 0.400 0.421 J 3.13 0.839 J 4.91 < 0.243 67.3
10/30/2023 1.50 3.75 2.90 J 6.90 22.7 10.4 < 0.160 2.54 3.12 23.0 1.74 J < 0.400 < 0.364 2.57 0.805 J < 0.621 < 0.243 9.51
10/30/2023 < 0.382 < 0.340 < 0.544 3.42 J 5.76 7.37 < 0.160 < 0.335 8.76 1,850 < 1.10 < 0.400 < 0.364 < 0.375 < 0.382 < 0.621 < 0.243 847
10/30/2023 < 0.382 0.764 < 0.544 64.3 4.22 7.40 < 0.160 < 0.335 < 0.553 7,570 < 1.10 < 0.400 < 0.364 < 0.375 < 0.382 < 0.621 < 0.243 647
Residential 2,800 34,000 210 35,000 2.8 1,400 21,000 7,000 280 35,000 14 35,000 14 420 420 NS 5.6 700
Non-Residential 35,000 53,000 2,600 440,000 36 18,000 260,000 88,000 3,500 440,000 180 440,000 180 5,300 5,300 NS 280 8,800
Notes:
Concentrations are reported in microgram per cubic meter (µg/m^3).
NS - No Standard Established
Highlighted - Value exceeds Residential VISL
Highlighted - Value exceeds Non-Residential VISL
Only compounds detected in at least one sample are included in this table. The full analytical laboratory report is included in Appendix V.
2-Butanone (MEK)
Naphthalene
2-Propanol
(Isopropanol)Constituent →
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl Butyl Ketone
(2-Hexanone)
TABLE 2 (cont'd)
SOIL-GAS ANALYTICAL RESULTS
Lee's Truck Stop
Charlotte, Mecklenburg County, North Carolina
Tetrachloroethylene (PCE)
Toluene
Total Xylenes
2,2,4-Trimethylpentane
1,1,1-Trichloroethane
Vinyl Chloride
Propene
(Propylene)
Styrene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Trichloroethylene (TCE)
S&ME Project No. 215740
J - Estimated Value: analyte detected at or above the method detection limit but below the reporting limit
Analytical Method →TO-15
BOLD - Value detected above laboratory MDL
Sample ID
SG-1
SG-2
SG-3
SG-4
SG-5
SG-6
DUP
Vapor Intrustion
Screening Levels (VISLs)
Appendices
Appendix I – Field Notes
Environmental Field Report
Date:
10/24/2023
Job Number:
215740
Project Name:
Lee’s Truck Stop
Weather/Temperature:
75, sunny
Project Location:
100 Dalton Avenue, Charlotte, NC
Notes By:
☒
Present at the Site:
Sarah Taylor, S&ME (ST)
Matt Brundage, S&ME (MB)
Probe Utility Locating (Probe)
JG Drilling (JG)
ST arrives onsite at 0830 after picking up ice for samples. MB already onsite. Probe is clearing proposed
boring locations. JG is working on boring SG-6. ST begins describing soils while MB bags 2.5-foot
intervals and screens soils. Bagged soil is placed on ice. JG installs SGI in SG-6 at 15 ft-bgs. JG
decontaminates drilling rods.
JG moves to SG-4. ST and MB repeat soil steps. Probe finishes clearing boring locations, leaves site. JG
installs SGI in SG-4 and 15 ft-bgs and moves to collect soil samples from SB-11, SB-12, and SB-13
locations. ST describes and screens soils while MB begins leak testing SG-6 and SG-4. JG decontaminates
drilling rods.
JG moves to SG-5. Soils are wet at approximately 7 feet. Plan to set SGI above wet soils. JG puts 5 bags
of sand in boring and level of sand does not come up, indicating an unknown void below the surface. JG
offsets and sets SGI in SG-5 at approximately 4 ft-bgs to avoid reaching wet soils. ST describes and
screens soils. JG decontaminates drilling rods.
JG moves to SG-3. ST repeats soil steps. JG installs SG-3 at 15 ft-bgs. MB performs leak test on SG-5. JG
decontaminates drilling rods.
JG moves to SG-2. ST repeats soil steps. JG installs SG-2 at 15 ft-bgs. MB performs leak test on SG-3. JG
decontaminates drilling rods.
JG moves to SG-1. ST repeats soil steps. JG installs SG-1 at 12 ft-bgs due to wet soils. MB performs leak
test on SG-2. JG decontaminates drilling rods.
JG packs up Geoprobe and cleans up equipment. ST begins placing soil samples into lab-provided
sample containers. MB performs leak test on SG-1, then assists ST in sampling. JG offsite at 1300.
ST and MB finish placing soil samples in containers. ST takes photos of each sample location and SGI
while MB packs up trucks and cleans site. ST and MB offsite at 1530. ST returns to office to re-pack
samples with new ice, fill out chain of custody, and place samples in designated location for lab courier
pickup.
Equipment Used
Geoprobe
Photoionization Detector (PID)
Ground Penetrating Radar
Lee’s Truck Stop
100 Dalton Avenue, Charlotte, NC
S&ME Project No. 215740
2
PID Screening Table
Boring ID Depth (ft-bgs) PID Reading
SG-1 0 – 5 9.0*
SG-1 5 – 10 5.1
SG-1 10 – 15 1.1
SG-2 0 - 5 0.6
SG-2 5 – 10 0.8*
SG-2 10 – 15 0.7
SG-3 0 – 5 1.0**
SG-3 5 – 10 2.7
SG-3 10 – 15 2.8
SG-4 0 – 5 0.5
SG-4 5 – 10 11.5*
SG-4 10 – 15 0.6
SG-5 0 – 5 33.6*
SG-5 5 – 10 1.6
SG-5 10 – 15 12.7
SG-6 0 –5 0.3
SG-6 5 – 10 3.3
SG-6 10 – 15 11.7*
SB-11 0 – 2+ 0.3
SB-12 0 – 2+ 0.2
SB-13 0 – 2+ 1.1
Table notes:
*Soil sample collected due to highest PID reading from boring
**Soil sample collected due to petroleum odors and visible discoloration
+Top 1-foot of boring was primarily gravel; sample collected from 1’-2’ interval
Soil descriptions provided in boring logs (separate document)
Field notes completed by:
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
240 12 240 12 240 12 0 8 12 240 12
180 to 168 180 to 168 180 to 168 70 to 58 180 to 168
Date:
Notes:
Revision Date:
VOCs by TO-15 VOCs by TO-15 VOCs by TO-15
End Time 11:37 11:37 11:40 12:03
Approximate Total Time (min)75 75 60 56
Final Vacuum (inHg)-5 -5 -4 -6
12:44
-4
69
Sampler Information
10/30/2023Sampler Signature:Matthew Brundage
9/1/17 14:50
Sample Analysis VOCs by TO-15
Sampled by:
VOCs by TO-15
1. Per the NCDEQ DWM VI Guidance dated April 2014, the helium concentration detected during the leak test shall not exceed 10% of the helium concentration in the shroud.
Purge Flow Rate (mL/min)200 200 200 200
-30 -30 -27 -25
Purge Interval (3x Vol.) (min)61.9 61.9 61.9 59.1
Initial Vacuum (inHg)
10.0 10.0 8.0
Sample Collection
Start Time 10:22 10:22 10:40 11:07
Actual Purge Time (min)10.0
11:35
10.0
Volume (mL)4128 4128 4128 3942
Leak Test Passed (Yes/No)1 Yes Yes Yes Yes Yes
Purge Information
Enter
Construction Details
→
4128
Total Well Depth (in-bgs)180 180 180 70 180
He Detected in Leak Test (Y or N)No No No No No
Percent of He in the Leak Test versus the
Shroud 0.000%0.000%0.000%0.000%
He Conc. Detected in Leak Test (ppm)0 0
68 68 68
Personal Pump Personal Pump Personal Pump
Barometric Pressure (inHg)30.2 30.2
Project Number:
Canister Volume (L)1 1 1 1
Soil Gas Implant
SG-3
Regulator ID FC-3358 FC-3777
2627
FC-3326
Sample ID SG-6 DUP SG-4 SG-5
FC-3776 FC-3397
Canister ID 23766 23002
10/30/2023
SOIL VAPOR FIELD SAMPLING FORM
Location:
Lee Truck stop Property
215740
-28
30.2 30.2
0 0 0
0.000%
200
61.9
8889 2124
Sample Type Soil Gas Implant Soil Gas Implant Soil Gas Implant Soil Gas Implant
Helium Detector Serial No.:
Sample Information
Weather:
Project Name:
68
10/14/2021
Date:
Air Temp (°F):
Calibration Date:
Charlotte, North Carolina
Sunny
MGD-2002 42201
Sand Pack Interval Depth (in-bgs)
He Concentration in Shroud (%)19.5 19.5 30.1 20.2
1
72
Leak Test Information
Purge Method Personal Pump
22.8
29.8
Personal Pump
Ambient Temp (°F)68
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
240 12 240 12
180 to 168 180 to 168 to
Date:
Notes:
Revision Date:
SOIL VAPOR FIELD SAMPLING FORM
Project Name:Lee Truck stop Property
Project Number:215740
Location:Charlotte, North Carolina Date:
Sample Information
Sample Type Soil Gas Implant Soil Gas Implant Soil Gas Implant Soil Gas Implant Soil Gas Implant
10/30/2023
Weather:Sunny Air Temp (°F):68
Helium Detector Serial No.:MGD-2002 414355 Calibration Date:10/14/2021
Canister ID 24605 23696
Sample ID SG-2 SG-1
Canister Volume (L)1 1
Regulator ID 3525 3180
Barometric Pressure (inHg)30.2 30.2
Ambient Temp (°F)74 74
He Concentration in Shroud (%)27.2 20.7
Purge Method Personal Pump Personal Pump Personal Pump Personal Pump Personal Pump
He Conc. Detected in Leak Test (ppm)0 0
He Detected in Leak Test (Y or N)No No
Leak Test Passed (Yes/No)1 Yes Yes
Percent of He in the Leak Test versus the
Shroud 0.000%0.000%
Volume (mL)4128 4128
Purge Information
Enter
Construction Details
→
Sand Pack Interval Depth (in-bgs)
Total Well Depth (in-bgs)180 180
Purge Interval (3x Vol.) (min)61.9 61.9
Purge Flow Rate (mL/min)200 200
Initial Vacuum (inHg)-30 -30
Sample Collection
Start Time 12:24 12:34
Actual Purge Time (min)10.0 10.0
Final Vacuum (inHg)-5 -6
End Time 13:32 13:34
Sample Analysis VOCs by TO-15 VOCs by TO-15
Approximate Total Time (min)68 60
1. Per the NCDEQ DWM VI Guidance dated April 2014, the helium concentration detected during the leak test shall not exceed 10% of the helium concentration in the shroud.
9/1/17 14:50
Sampler Information
Sampled by:Matthew Brundage Sampler Signature:10/30/2023
Appendix II – Boring Logs
S&ME Project No. 215740
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:
WATER LEVEL
SAMPLE
OVA READINGS
(PPM)
Sample Time /
1st 6in
2nd 6in
3rd 6in
N VALUE
9.0
5.1
1.1
30
25
20
15 Boring Terminated at 15 Ft-BGS
Clayey Silt, Red, Tan,
10 No
Sandy Silt, Soft, Tan, Mottled Yellow and red minerals,
Sandy Silt, Brown, Fine, Medium, Some Organics,
5 Sandy Silt, Stiff, Tan, Fine, No
Sandy Silt, Red, Tan, Fine, Medium,
DEPTH
(feet)
GRAPHIC
LOG MATERIAL DESCRIPTION
LABORATORY
ANALYSES
Fill, Sand/gravel, Yes
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: JG Drilling
HAMMER TYPE: Not Applicable S. Taylor
DATE DRILLED:Tuesday, October 24, 2023 15
DRILL RIG: Geoprobe 6712DT
PROJECT:Lee's Truck Stop
BORING LOG: SG-1Charlotte, North Carolina
S&ME Project No. 215740
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:
WATER LEVEL
SAMPLE
OVA READINGS
(PPM)
Sample Time /
1st 6in
2nd 6in
3rd 6in
N VALUE
0.6
0.8
0.7
DATE DRILLED:Tuesday, October 24, 2023 15
DRILL RIG: Geoprobe 6712DT
PROJECT:Lee's Truck Stop
BORING LOG: SG-2Charlotte, North Carolina
DEPTH
(feet)
GRAPHIC
LOG MATERIAL DESCRIPTION
LABORATORY
ANALYSES
Sand, Tan, Grey, Coarse, Medium, No
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: JG Drilling
HAMMER TYPE: Not Applicable S. Taylor
5 Yes
Clayey Silt, Red, Brown,
10 No
Clayey Silt, Tan, Some Medium Sand,
Clayey Silt, Brown,
15 Boring Terminated at 15 Ft-BGS
20
25
30
S&ME Project No. 215740
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:
WATER LEVEL
SAMPLE
OVA READINGS
(PPM)
Sample Time /
1st 6in
2nd 6in
3rd 6in
N VALUE
1.0
2.7
2.8
DATE DRILLED:Tuesday, October 24, 2023 15
DRILL RIG: Geoprobe 6712DT
PROJECT:Lee's Truck Stop
BORING LOG: SG-3Charlotte, North Carolina
DEPTH
(feet)
GRAPHIC
LOG MATERIAL DESCRIPTION
LABORATORY
ANALYSES
Sandy Silt, Stiff, Red, Brown, Fine, Medium, Yes
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: JG Drilling
HAMMER TYPE: Not Applicable S. Taylor
Sandy Silt, Red, Tan, Mottled Red and yellow minerals,
5 No
10 No
15 Boring Terminated at 15 Ft-BGS
Clayey Silt, Red, Mottled Red and yellow minerals,
20
25
30
S&ME Project No. 215740
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:
WATER LEVEL
SAMPLE
OVA READINGS
(PPM)
Sample Time /
1st 6in
2nd 6in
3rd 6in
N VALUE
0.5
11.5
0.6
DATE DRILLED:Tuesday, October 24, 2023 15
DRILL RIG: Geoprobe 6712DT
PROJECT:Lee's Truck Stop
BORING LOG: SG-4Charlotte, North Carolina
DEPTH
(feet)
GRAPHIC
LOG MATERIAL DESCRIPTION
LABORATORY
ANALYSES
Silty Sand, Red, Tan, Fine, No
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: JG Drilling
HAMMER TYPE: Not Applicable S. Taylor
5 Silt, Red brown, Yes
10 No
15 Boring Terminated at 15 Ft-BGS
Sandy Silt, Red brown, Mottled Yellow and black minerals,
20
25
30
S&ME Project No. 215740
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:
WATER LEVEL
SAMPLE
OVA READINGS
(PPM)
Sample Time /
1st 6in
2nd 6in
3rd 6in
N VALUE
33.6
1.6
12.7
DATE DRILLED:Tuesday, October 24, 2023 15
DRILL RIG: Geoprobe 6712DT
PROJECT:Lee's Truck Stop
BORING LOG: SG-5Charlotte, North Carolina
DEPTH
(feet)
GRAPHIC
LOG MATERIAL DESCRIPTION
LABORATORY
ANALYSES
Silt and gravel, Yes
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: JG Drilling
HAMMER TYPE: Not Applicable S. Taylor
5 No
Concrete, Silt, Red, Tan, Mottled Yellow and red minerals,
10 No
Sandy Silt, Red, Tan, Fine, Medium, Mottled Yellow and red minerals,
15 Boring Terminated at 15 Ft-BGS
20
25
30
S&ME Project No. 215740
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:
WATER LEVEL
SAMPLE
OVA READINGS
(PPM)
Sample Time /
1st 6in
2nd 6in
3rd 6in
N VALUE
0.3
3.3
11.7
30
25
20
15 Boring Terminated at 15 Ft-BGS
Silt, Red, Brown, Mottled Yellow, red, and black minerals,
10 Yes
5 Silt, Red, Brown, No
DEPTH
(feet)
GRAPHIC
LOG MATERIAL DESCRIPTION
LABORATORY
ANALYSES
Sandy Silt, Red, Brown, Fine, No
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: JG Drilling
HAMMER TYPE: Not Applicable S. Taylor
DATE DRILLED:Tuesday, October 24, 2023 15
DRILL RIG: Geoprobe 6712DT
PROJECT:Lee's Truck Stop
BORING LOG: SG-6Charlotte, North Carolina
S&ME Project No. 215740
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:
WATER LEVEL
SAMPLE
OVA READINGS
(PPM)
Sample Time /
1st 6in
2nd 6in
3rd 6in
N VALUE
0.3
30
25
20
15
10
5
Boring Terminated at 2 Ft-BGS
Silty Clay, Stiff, Red, Brown, Yes
DEPTH
(feet)
GRAPHIC
LOG MATERIAL DESCRIPTION
LABORATORY
ANALYSES
Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: JG Drilling
HAMMER TYPE: Not Applicable S. Taylor
DATE DRILLED:Tuesday, October 24, 2023 2
DRILL RIG: Geoprobe 6712DT
PROJECT:Lee's Truck Stop
BORING LOG: SB-11Charlotte, North Carolina
S&ME Project No. 215740
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:
WATER LEVEL
SAMPLE
OVA READINGS
(PPM)
Sample Time /
1st 6in
2nd 6in
3rd 6in
N VALUE
0.2
30
25
20
15
10
5
Boring Terminated at 2 Ft-BGS
Silt, Red, Mottled yellow Yes
DEPTH
(feet)
GRAPHIC
LOG MATERIAL DESCRIPTION
LABORATORY
ANALYSES
Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: JG Drilling
HAMMER TYPE: Not Applicable S. Taylor
DATE DRILLED:Tuesday, October 24, 2023 2
DRILL RIG: Geoprobe 6712DT
PROJECT:Lee's Truck Stop
BORING LOG: SB-12Charlotte, North Carolina
S&ME Project No. 215740
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:
WATER LEVEL
SAMPLE
OVA READINGS
(PPM)
Sample Time /
1st 6in
2nd 6in
3rd 6in
N VALUE
1.1
30
25
20
15
10
5
Boring Terminated at 2 Ft-BGS
Sandy Silt, Brown, Organic, glass fragments Yes
DEPTH
(feet)
GRAPHIC
LOG MATERIAL DESCRIPTION
LABORATORY
ANALYSES
Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: JG Drilling
HAMMER TYPE: Not Applicable S. Taylor
DATE DRILLED:Tuesday, October 24, 2023 2
DRILL RIG: Geoprobe 6712DT
PROJECT:Lee's Truck Stop
BORING LOG: SB-13Charlotte, North Carolina
Appendix III – Photographs
Brownfields Assessment Report
Lee's Truck Stop
Charlotte, North Carolina
S&ME Project No. 215740
November 22, 2023
Date: 10/24/2023
Photographer: S.
Taylor
Location / Orientation View of the subject property facing east
Remarks SG-1 location
Date: 10/24/2023
Photographer: S. Taylor
Location / Orientation View of the subject property facing south
Remarks SG-2 location
Brownfields Assessment Report
Lee's Truck Stop
Charlotte, North Carolina
S&ME Project No. 215740
November 22, 2023
Date: 10/24/2023
Photographer: S. Taylor
Location / Orientation View of the subject property facing north
Remarks SG-3 location
Date: 10/24/2023
Photographer: S. Taylor
Location / Orientation View of the subject property facing northwest
Remarks SG-4 location
Brownfields Assessment Report
Lee's Truck Stop
Charlotte, North Carolina
S&ME Project No. 215740
November 22, 2023
Date: 10/24/2023
Photographer: S. Taylor
Location / Orientation View of the subject property facing south
Remarks SG-5 location
Date: 10/24/2023
Photographer: S. Taylor
Location / Orientation View of the subject property facing west
Remarks SG-6 location
Brownfields Assessment Report
Lee's Truck Stop
Charlotte, North Carolina
S&ME Project No. 215740
November 22, 2023
Date: 10/24/2023
Photographer: S. Taylor
Location / Orientation View of the subject property facing north
Remarks SB-11 location
Date: 10/24/2023
Photographer: S. Taylor
Location / Orientation View of the subject property facing east
Remarks SB-12 location
Brownfields Assessment Report
Lee's Truck Stop
Charlotte, North Carolina
S&ME Project No. 215740
November 22, 2023
Date: 10/24/2023
Photographer: S. Taylor
Location / Orientation View of the subject property facing north
Remarks SB-13 location
Date: 10/30/2023
Photographer: S. Taylor
Location / Orientation View of the subject property at SG-6 location
Remarks Typical soil gas sampling array with duplicate
Appendix IV – Pace Laboratory Report - Soil
#=CL#
November 15, 2023
LIMS USE: FR - JOHN SHERRILL, P.G.
LIMS OBJECT ID: 92695355
92695355
Project:
Pace Project No.:
RE:
John L. Sherrill, P.G.
S&ME, Inc.
2016 Ayrsley Town Blvd
Suite 2-A
Charlotte, NC 28273
LEE'S TRUCK STOP-215740
Dear John Sherrill, P.G.:
Enclosed are the analytical results for sample(s) received by the laboratory on October 25, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
A revised report is being submitted on 11/15/23 to include MDLs and applicable J values, per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
612-473-6801
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 88
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 88
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Lab ID Sample ID Matrix Date Collected Date Received
92695355001 SB-SG-1 Solid 10/24/23 13:00 10/25/23 07:20
92695355002 SB-SG-2 Solid 10/24/23 13:20 10/25/23 07:20
92695355003 SB-SG-3 Solid 10/24/23 13:30 10/25/23 07:20
92695355004 SB-SG-4 Solid 10/24/23 13:40 10/25/23 07:20
92695355005 SB-SG-5 Solid 10/24/23 13:45 10/25/23 07:20
92695355006 SB-SG-6 Solid 10/24/23 14:00 10/25/23 07:20
92695355007 SB-11 Solid 10/24/23 14:10 10/25/23 07:20
92695355008 SB-12 Solid 10/24/23 14:20 10/25/23 07:20
92695355009 SB-13 Solid 10/24/23 14:40 10/25/23 07:20
92695355010 SB-DUP Solid 10/24/23 00:00 10/25/23 07:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 88
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92695355001 SB-SG-1 EPA 7199 1 PASI-CSMS1
EPA 6020B 7 PANJPD
EPA 7471B 1 PANAKB
EPA 8270E 93 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92695355002 SB-SG-2 EPA 7199 1 PASI-CSMS1
EPA 6020B 7 PANJPD
EPA 7471B 1 PANAKB
EPA 8270E 93 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92695355003 SB-SG-3 EPA 7199 1 PASI-CSMS1
EPA 6020B 7 PANJPD
EPA 7471B 1 PANAKB
EPA 8270E 93 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92695355004 SB-SG-4 EPA 7199 1 PASI-CSMS1
EPA 6020B 7 PANJPD
EPA 7471B 1 PANAKB
EPA 8270E 93 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92695355005 SB-SG-5 EPA 7199 1 PASI-CSMS1
EPA 6020B 7 PANJPD
EPA 7471B 1 PANAKB
EPA 8270E 93 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92695355006 SB-SG-6 EPA 7199 1 PASI-CSMS1
EPA 6020B 7 PANJPD
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 88
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7471B 1 PANAKB
EPA 8270E 93 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92695355007 SB-11 EPA 7199 1 PASI-CSMS1
EPA 6020B 7 PANJPD
EPA 7471B 1 PANAKB
EPA 8270E 93 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92695355008 SB-12 EPA 7199 1 PASI-CSMS1
EPA 6020B 7 PANJPD
EPA 7471B 1 PANAKB
EPA 8270E 93 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92695355009 SB-13 EPA 7199 1 PASI-CSMS1
EPA 6020B 7 PANJPD
EPA 7471B 1 PANAKB
EPA 8270E 93 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92695355010 SB-DUP EPA 7199 1 PASI-CSMS1
EPA 6020B 7 PANJPD
EPA 7471B 1 PANAKB
EPA 8270E 93 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-1 Lab ID:92695355001 Collected:10/24/23 13:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.94J mg/kg 10/27/23 17:23 18540-29-910/27/23 09:451.2 0.0012 1
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.48 mg/kg 11/02/23 12:19 7440-38-211/01/23 07:521.24 0.124 5
Barium 37.6 mg/kg 11/02/23 12:19 7440-39-311/01/23 07:523.11 0.189 5
Cadmium ND mg/kg 11/02/23 12:19 7440-43-911/01/23 07:521.24 0.106 5
Chromium 42.7 mg/kg 11/02/23 12:19 7440-47-311/01/23 07:526.22 0.368 5
Lead 7.77 mg/kg 11/02/23 12:19 7439-92-111/01/23 07:522.49 0.123 5
Selenium 0.801J mg/kg 11/02/23 12:19 7782-49-2 J11/01/23 07:523.11 0.224 5
Silver ND mg/kg 11/02/23 12:19 7440-22-411/01/23 07:520.622 0.108 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0459J mg/kg 11/01/23 18:12 7439-97-6 J10/31/23 22:140.0498 0.0224 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/30/23 11:21 83-32-910/27/23 11:220.39 0.14 1
Acenaphthylene ND mg/kg 10/30/23 11:21 208-96-810/27/23 11:220.39 0.14 1
Acetophenone ND mg/kg 10/30/23 11:21 98-86-210/27/23 11:220.39 0.10 1
Aniline ND mg/kg 10/30/23 11:21 62-53-310/27/23 11:220.39 0.15 1
Atrazine ND mg/kg 10/30/23 11:21 1912-24-910/27/23 11:220.39 0.12 1
Benzaldehyde ND mg/kg 10/30/23 11:21 100-52-710/27/23 11:220.39 0.13 1
Benzidine ND mg/kg 10/30/23 11:21 92-87-510/27/23 11:221.9 0.32 1
Benzo(a)anthracene ND mg/kg 10/30/23 11:21 56-55-310/27/23 11:220.39 0.13 1
Benzo(a)pyrene ND mg/kg 10/30/23 11:21 50-32-810/27/23 11:220.39 0.13 1
Benzo(b)fluoranthene ND mg/kg 10/30/23 11:21 205-99-210/27/23 11:220.39 0.13 1
Benzo(g,h,i)perylene ND mg/kg 10/30/23 11:21 191-24-210/27/23 11:220.39 0.15 1
Benzo(k)fluoranthene ND mg/kg 10/30/23 11:21 207-08-910/27/23 11:220.39 0.14 1
Benzoic Acid ND mg/kg 10/30/23 11:21 65-85-010/27/23 11:221.9 0.83 1
Benzophenone ND mg/kg 10/30/23 11:21 119-61-910/27/23 11:220.39 0.18 1
Benzyl alcohol ND mg/kg 10/30/23 11:21 100-51-610/27/23 11:220.78 0.29 1
Biphenyl (Diphenyl)ND mg/kg 10/30/23 11:21 92-52-410/27/23 11:220.39 0.092 1
4-Bromophenylphenyl ether ND mg/kg 10/30/23 11:21 101-55-310/27/23 11:220.39 0.15 1
Butylbenzylphthalate ND mg/kg 10/30/23 11:21 85-68-710/27/23 11:220.39 0.16 1
Caprolactam ND mg/kg 10/30/23 11:21 105-60-210/27/23 11:220.39 0.21 1
Carbazole ND mg/kg 10/30/23 11:21 86-74-810/27/23 11:220.39 0.13 1
4-Chloro-3-methylphenol ND mg/kg 10/30/23 11:21 59-50-710/27/23 11:220.78 0.27 1
4-Chloroaniline ND mg/kg 10/30/23 11:21 106-47-810/27/23 11:220.78 0.30 1
Chlorobenzilate ND mg/kg 10/30/23 11:21 510-15-610/27/23 11:220.39 0.077 1
bis(2-Chloroethoxy)methane ND mg/kg 10/30/23 11:21 111-91-110/27/23 11:220.39 0.16 1
bis(2-Chloroethyl) ether ND mg/kg 10/30/23 11:21 111-44-410/27/23 11:220.39 0.15 1
2-Chloronaphthalene ND mg/kg 10/30/23 11:21 91-58-710/27/23 11:220.39 0.15 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-1 Lab ID:92695355001 Collected:10/24/23 13:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2-Chlorophenol ND mg/kg 10/30/23 11:21 95-57-810/27/23 11:220.39 0.15 1
4-Chlorophenylphenyl ether ND mg/kg 10/30/23 11:21 7005-72-310/27/23 11:220.39 0.14 1
Chrysene ND mg/kg 10/30/23 11:21 218-01-910/27/23 11:220.39 0.14 1
Dibenz(a,h)anthracene ND mg/kg 10/30/23 11:21 53-70-310/27/23 11:220.39 0.15 1
Dibenzo(a,e)pyrene ND mg/kg 10/30/23 11:21 192-65-410/27/23 11:221.2 0.26 1
Dibenzofuran ND mg/kg 10/30/23 11:21 132-64-910/27/23 11:220.39 0.14 1
1,2-Dichlorobenzene ND mg/kg 10/30/23 11:21 95-50-110/27/23 11:220.39 0.14 1
1,3-Dichlorobenzene ND mg/kg 10/30/23 11:21 541-73-110/27/23 11:220.39 0.14 1
1,4-Dichlorobenzene ND mg/kg 10/30/23 11:21 106-46-710/27/23 11:220.39 0.15 1
3,3'-Dichlorobenzidine ND mg/kg 10/30/23 11:21 91-94-1 L210/27/23 11:220.78 0.26 1
2,4-Dichlorophenol ND mg/kg 10/30/23 11:21 120-83-210/27/23 11:220.39 0.15 1
2,6-Dichlorophenol ND mg/kg 10/30/23 11:21 87-65-0 L210/27/23 11:220.39 0.099 1
2,3-Dichloroaniline ND mg/kg 10/30/23 11:21 608-27-510/27/23 11:220.39 0.19 1
Diethylphthalate ND mg/kg 10/30/23 11:21 84-66-210/27/23 11:220.39 0.14 1
3,3'-Dimethylbenzidine ND mg/kg 10/30/23 11:21 119-93-7 IL10/27/23 11:220.78 0.35 1
2,4-Dimethylphenol ND mg/kg 10/30/23 11:21 105-67-910/27/23 11:220.39 0.16 1
Dimethylphthalate ND mg/kg 10/30/23 11:21 131-11-310/27/23 11:220.39 0.14 1
Di-n-butylphthalate ND mg/kg 10/30/23 11:21 84-74-210/27/23 11:220.39 0.13 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/30/23 11:21 534-52-110/27/23 11:220.78 0.36 1
1,3-Dinitrobenzene ND mg/kg 10/30/23 11:21 99-65-0 L210/27/23 11:220.39 0.087 1
1,4-Dinitrobenzene ND mg/kg 10/30/23 11:21 100-25-4 L210/27/23 11:220.39 0.11 1
2,4-Dinitrophenol ND mg/kg 10/30/23 11:21 51-28-510/27/23 11:221.9 1.2 1
2,4-Dinitrotoluene ND mg/kg 10/30/23 11:21 121-14-210/27/23 11:220.39 0.15 1
2,6-Dinitrotoluene ND mg/kg 10/30/23 11:21 606-20-210/27/23 11:220.39 0.14 1
Di-n-octylphthalate ND mg/kg 10/30/23 11:21 117-84-010/27/23 11:220.39 0.15 1
1,2-Diphenylhydrazine ND mg/kg 10/30/23 11:21 122-66-710/27/23 11:220.39 0.15 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/30/23 11:21 117-81-710/27/23 11:220.39 0.15 1
Fluoranthene ND mg/kg 10/30/23 11:21 206-44-010/27/23 11:220.39 0.13 1
Fluorene ND mg/kg 10/30/23 11:21 86-73-710/27/23 11:220.39 0.14 1
Hexachloro-1,3-butadiene ND mg/kg 10/30/23 11:21 87-68-310/27/23 11:220.39 0.17 1
Hexachlorobenzene ND mg/kg 10/30/23 11:21 118-74-110/27/23 11:220.39 0.15 1
Hexachlorocyclopentadiene ND mg/kg 10/30/23 11:21 77-47-410/27/23 11:220.39 0.22 1
Hexachloroethane ND mg/kg 10/30/23 11:21 67-72-110/27/23 11:220.39 0.15 1
Hexachlorophene ND mg/kg 10/30/23 11:21 70-30-4 IH,v210/27/23 11:223.9 2.3 1
Hexachloropropene ND mg/kg 10/30/23 11:21 1888-71-710/27/23 11:220.39 0.11 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/30/23 11:21 193-39-510/27/23 11:220.39 0.15 1
Isodrin ND mg/kg 10/30/23 11:21 465-73-610/27/23 11:220.39 0.092 1
1-Methylnaphthalene ND mg/kg 10/30/23 11:21 90-12-010/27/23 11:220.39 0.14 1
2-Methylnaphthalene ND mg/kg 10/30/23 11:21 91-57-610/27/23 11:220.39 0.16 1
2-Methyl-5-nitroaniline ND mg/kg 10/30/23 11:21 99-55-810/27/23 11:220.39 0.12 1
2-Methylphenol(o-Cresol)ND mg/kg 10/30/23 11:21 95-48-710/27/23 11:220.39 0.16 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/30/23 11:21 15831-10-410/27/23 11:220.39 0.16 1
1-Naphthalenamine ND mg/kg 10/30/23 11:21 134-32-710/27/23 11:220.78 0.13 1
2-Naphthalenamine ND mg/kg 10/30/23 11:21 91-59-810/27/23 11:220.78 0.15 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-1 Lab ID:92695355001 Collected:10/24/23 13:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Naphthalene ND mg/kg 10/30/23 11:21 91-20-310/27/23 11:220.39 0.13 1
2-Nitroaniline ND mg/kg 10/30/23 11:21 88-74-410/27/23 11:221.9 0.32 1
3-Nitroaniline ND mg/kg 10/30/23 11:21 99-09-210/27/23 11:221.9 0.30 1
4-Nitroaniline ND mg/kg 10/30/23 11:21 100-01-610/27/23 11:220.78 0.30 1
Nitrobenzene ND mg/kg 10/30/23 11:21 98-95-310/27/23 11:220.39 0.18 1
2-Nitrophenol ND mg/kg 10/30/23 11:21 88-75-510/27/23 11:220.39 0.17 1
4-Nitrophenol ND mg/kg 10/30/23 11:21 100-02-710/27/23 11:221.9 0.75 1
N-Nitroso-di-n-propylamine ND mg/kg 10/30/23 11:21 621-64-710/27/23 11:220.39 0.15 1
Pentachlorophenol ND mg/kg 10/30/23 11:21 87-86-510/27/23 11:220.78 0.38 1
Phenanthrene ND mg/kg 10/30/23 11:21 85-01-810/27/23 11:220.39 0.13 1
Phenol ND mg/kg 10/30/23 11:21 108-95-210/27/23 11:220.39 0.17 1
Pyrene ND mg/kg 10/30/23 11:21 129-00-010/27/23 11:220.39 0.16 1
Pyridine ND mg/kg 10/30/23 11:21 110-86-1 v110/27/23 11:220.39 0.12 1
1,2,4,5-Tetrachlorobenzene ND mg/kg 10/30/23 11:21 95-94-310/27/23 11:220.39 0.095 1
2,3,4,6-Tetrachlorophenol ND mg/kg 10/30/23 11:21 58-90-210/27/23 11:220.39 0.097 1
2,4,5-Trichlorophenol ND mg/kg 10/30/23 11:21 95-95-410/27/23 11:220.39 0.18 1
2,4,6-Trichlorophenol ND mg/kg 10/30/23 11:21 88-06-210/27/23 11:220.39 0.16 1
Surrogates
2-Fluorobiphenyl (S)42 %10/30/23 11:21 321-60-810/27/23 11:2210-130 1
Terphenyl-d14 (S)50 %10/30/23 11:21 1718-51-010/27/23 11:2210-130 1
Phenol-d6 (S)39 %10/30/23 11:21 13127-88-310/27/23 11:2210-130 1
2-Fluorophenol (S)40 %10/30/23 11:21 367-12-410/27/23 11:2210-130 1
2,4,6-Tribromophenol (S)36 %10/30/23 11:21 118-79-610/27/23 11:2210-130 1
Nitrobenzene-d5 (S)45 %10/30/23 11:21 4165-60-010/27/23 11:2210-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/27/23 20:12 67-64-110/27/23 12:430.12 0.040 1
Benzene ND mg/kg 10/27/23 20:12 71-43-210/27/23 12:430.0062 0.0025 1
Bromobenzene ND mg/kg 10/27/23 20:12 108-86-110/27/23 12:430.0062 0.0020 1
Bromochloromethane ND mg/kg 10/27/23 20:12 74-97-510/27/23 12:430.0062 0.0018 1
Bromodichloromethane ND mg/kg 10/27/23 20:12 75-27-410/27/23 12:430.0062 0.0024 1
Bromoform ND mg/kg 10/27/23 20:12 75-25-210/27/23 12:430.0062 0.0022 1
Bromomethane ND mg/kg 10/27/23 20:12 74-83-9 IK,v110/27/23 12:430.025 0.019 1
2-Butanone (MEK)ND mg/kg 10/27/23 20:12 78-93-310/27/23 12:430.12 0.030 1
n-Butylbenzene ND mg/kg 10/27/23 20:12 104-51-810/27/23 12:430.0062 0.0039 1
sec-Butylbenzene ND mg/kg 10/27/23 20:12 135-98-810/27/23 12:430.0062 0.0027 1
tert-Butylbenzene ND mg/kg 10/27/23 20:12 98-06-610/27/23 12:430.0062 0.0022 1
Carbon tetrachloride ND mg/kg 10/27/23 20:12 56-23-510/27/23 12:430.0062 0.0023 1
Chlorobenzene ND mg/kg 10/27/23 20:12 108-90-710/27/23 12:430.0062 0.0036 1
Chloroethane ND mg/kg 10/27/23 20:12 75-00-310/27/23 12:430.012 0.0048 1
Chloroform ND mg/kg 10/27/23 20:12 67-66-310/27/23 12:430.0062 0.0052 1
Chloromethane ND mg/kg 10/27/23 20:12 74-87-310/27/23 12:430.012 0.0052 1
2-Chlorotoluene ND mg/kg 10/27/23 20:12 95-49-810/27/23 12:430.0062 0.0022 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-1 Lab ID:92695355001 Collected:10/24/23 13:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Chlorotoluene ND mg/kg 10/27/23 20:12 106-43-410/27/23 12:430.0062 0.0034 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/27/23 20:12 96-12-810/27/23 12:430.0062 0.0024 1
Dibromochloromethane ND mg/kg 10/27/23 20:12 124-48-110/27/23 12:430.0062 0.0035 1
1,2-Dibromoethane (EDB)ND mg/kg 10/27/23 20:12 106-93-410/27/23 12:430.0062 0.0027 1
Dibromomethane ND mg/kg 10/27/23 20:12 74-95-310/27/23 12:430.0062 0.0013 1
1,2-Dichlorobenzene ND mg/kg 10/27/23 20:12 95-50-110/27/23 12:430.0062 0.0022 1
1,3-Dichlorobenzene ND mg/kg 10/27/23 20:12 541-73-110/27/23 12:430.0062 0.0019 1
1,4-Dichlorobenzene ND mg/kg 10/27/23 20:12 106-46-710/27/23 12:430.0062 0.0016 1
Dichlorodifluoromethane ND mg/kg 10/27/23 20:12 75-71-810/27/23 12:430.012 0.0063 1
1,1-Dichloroethane ND mg/kg 10/27/23 20:12 75-34-310/27/23 12:430.0062 0.0026 1
1,2-Dichloroethane ND mg/kg 10/27/23 20:12 107-06-210/27/23 12:430.0062 0.0041 1
1,1-Dichloroethene ND mg/kg 10/27/23 20:12 75-35-410/27/23 12:430.0062 0.0026 1
cis-1,2-Dichloroethene ND mg/kg 10/27/23 20:12 156-59-210/27/23 12:430.0062 0.0021 1
trans-1,2-Dichloroethene ND mg/kg 10/27/23 20:12 156-60-510/27/23 12:430.0062 0.0053 1
1,2-Dichloropropane ND mg/kg 10/27/23 20:12 78-87-510/27/23 12:430.0062 0.0019 1
1,3-Dichloropropane ND mg/kg 10/27/23 20:12 142-28-910/27/23 12:430.0062 0.0019 1
2,2-Dichloropropane ND mg/kg 10/27/23 20:12 594-20-710/27/23 12:430.0062 0.0047 1
1,1-Dichloropropene ND mg/kg 10/27/23 20:12 563-58-610/27/23 12:430.0062 0.0030 1
cis-1,3-Dichloropropene ND mg/kg 10/27/23 20:12 10061-01-510/27/23 12:430.0062 0.0017 1
trans-1,3-Dichloropropene ND mg/kg 10/27/23 20:12 10061-02-610/27/23 12:430.0062 0.0021 1
Diisopropyl ether ND mg/kg 10/27/23 20:12 108-20-310/27/23 12:430.0062 0.0017 1
Ethylbenzene 0.0066 mg/kg 10/27/23 20:12 100-41-410/27/23 12:430.0062 0.0029 1
Hexachloro-1,3-butadiene ND mg/kg 10/27/23 20:12 87-68-310/27/23 12:430.012 0.010 1
2-Hexanone ND mg/kg 10/27/23 20:12 591-78-610/27/23 12:430.062 0.0060 1
Isopropylbenzene (Cumene)ND mg/kg 10/27/23 20:12 98-82-810/27/23 12:430.0062 0.0021 1
p-Isopropyltoluene ND mg/kg 10/27/23 20:12 99-87-610/27/23 12:430.0062 0.0030 1
Methylene Chloride ND mg/kg 10/27/23 20:12 75-09-210/27/23 12:430.025 0.017 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/27/23 20:12 108-10-110/27/23 12:430.062 0.0060 1
Methyl-tert-butyl ether ND mg/kg 10/27/23 20:12 1634-04-410/27/23 12:430.0062 0.0023 1
Naphthalene ND mg/kg 10/27/23 20:12 91-20-310/27/23 12:430.0062 0.0033 1
n-Propylbenzene ND mg/kg 10/27/23 20:12 103-65-110/27/23 12:430.0062 0.0022 1
Styrene ND mg/kg 10/27/23 20:12 100-42-510/27/23 12:430.0062 0.0016 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/27/23 20:12 630-20-610/27/23 12:430.0062 0.0024 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/27/23 20:12 79-34-510/27/23 12:430.0062 0.0016 1
Tetrachloroethene ND mg/kg 10/27/23 20:12 127-18-410/27/23 12:430.0062 0.0020 1
Toluene 0.10 mg/kg 10/27/23 20:12 108-88-310/27/23 12:430.0062 0.0043 1
1,2,3-Trichlorobenzene ND mg/kg 10/27/23 20:12 87-61-610/27/23 12:430.0062 0.0050 1
1,2,4-Trichlorobenzene ND mg/kg 10/27/23 20:12 120-82-110/27/23 12:430.0062 0.0052 1
1,1,1-Trichloroethane ND mg/kg 10/27/23 20:12 71-55-610/27/23 12:430.0062 0.0032 1
1,1,2-Trichloroethane ND mg/kg 10/27/23 20:12 79-00-510/27/23 12:430.0062 0.0021 1
Trichloroethene ND mg/kg 10/27/23 20:12 79-01-610/27/23 12:430.0062 0.0050 1
Trichlorofluoromethane ND mg/kg 10/27/23 20:12 75-69-410/27/23 12:430.0062 0.0034 1
1,2,3-Trichloropropane ND mg/kg 10/27/23 20:12 96-18-410/27/23 12:430.0062 0.0031 1
1,2,4-Trimethylbenzene ND mg/kg 10/27/23 20:12 95-63-610/27/23 12:430.0062 0.0037 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-1 Lab ID:92695355001 Collected:10/24/23 13:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3,5-Trimethylbenzene ND mg/kg 10/27/23 20:12 108-67-810/27/23 12:430.0062 0.0021 1
Vinyl acetate ND mg/kg 10/27/23 20:12 108-05-410/27/23 12:430.062 0.013 1
Vinyl chloride ND mg/kg 10/27/23 20:12 75-01-410/27/23 12:430.012 0.0031 1
Xylene (Total)ND mg/kg 10/27/23 20:12 1330-20-710/27/23 12:430.012 0.0035 1
m&p-Xylene 0.012J mg/kg 10/27/23 20:12 179601-23-110/27/23 12:430.012 0.0042 1
o-Xylene 0.0049J mg/kg 10/27/23 20:12 95-47-610/27/23 12:430.0062 0.0027 1
Surrogates
Toluene-d8 (S)100 %10/27/23 20:12 2037-26-510/27/23 12:4370-130 1
4-Bromofluorobenzene (S)100 %10/27/23 20:12 460-00-410/27/23 12:4370-130 1
1,2-Dichloroethane-d4 (S)101 %10/27/23 20:12 17060-07-010/27/23 12:4370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.4 %10/26/23 17:15 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 80.3 %11/01/23 10:2011/01/23 10:141
Sample:SB-SG-2 Lab ID:92695355002 Collected:10/24/23 13:20 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 2.0 mg/kg 10/27/23 17:59 18540-29-910/27/23 09:451.3 0.0013 1
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 3.05 mg/kg 11/02/23 12:22 7440-38-211/01/23 07:521.26 0.126 5
Barium 74.9 mg/kg 11/02/23 12:22 7440-39-311/01/23 07:523.15 0.191 5
Cadmium ND mg/kg 11/02/23 12:22 7440-43-911/01/23 07:521.26 0.108 5
Chromium 44.1 mg/kg 11/02/23 12:22 7440-47-311/01/23 07:526.30 0.373 5
Lead 12.1 mg/kg 11/02/23 12:22 7439-92-111/01/23 07:522.52 0.125 5
Selenium 0.812J mg/kg 11/02/23 12:22 7782-49-2 J11/01/23 07:523.15 0.227 5
Silver ND mg/kg 11/02/23 12:22 7440-22-411/01/23 07:520.630 0.109 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0364J mg/kg 11/01/23 18:15 7439-97-6 J10/31/23 22:140.0504 0.0227 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-2 Lab ID:92695355002 Collected:10/24/23 13:20 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/30/23 11:49 83-32-910/27/23 11:220.40 0.14 1
Acenaphthylene ND mg/kg 10/30/23 11:49 208-96-810/27/23 11:220.40 0.14 1
Acetophenone ND mg/kg 10/30/23 11:49 98-86-210/27/23 11:220.40 0.10 1
Aniline ND mg/kg 10/30/23 11:49 62-53-310/27/23 11:220.40 0.16 1
Atrazine ND mg/kg 10/30/23 11:49 1912-24-910/27/23 11:220.40 0.13 1
Benzaldehyde ND mg/kg 10/30/23 11:49 100-52-710/27/23 11:220.40 0.13 1
Benzidine ND mg/kg 10/30/23 11:49 92-87-510/27/23 11:222.0 0.33 1
Benzo(a)anthracene ND mg/kg 10/30/23 11:49 56-55-310/27/23 11:220.40 0.13 1
Benzo(a)pyrene ND mg/kg 10/30/23 11:49 50-32-810/27/23 11:220.40 0.14 1
Benzo(b)fluoranthene ND mg/kg 10/30/23 11:49 205-99-210/27/23 11:220.40 0.13 1
Benzo(g,h,i)perylene ND mg/kg 10/30/23 11:49 191-24-210/27/23 11:220.40 0.15 1
Benzo(k)fluoranthene ND mg/kg 10/30/23 11:49 207-08-910/27/23 11:220.40 0.14 1
Benzoic Acid ND mg/kg 10/30/23 11:49 65-85-010/27/23 11:222.0 0.86 1
Benzophenone ND mg/kg 10/30/23 11:49 119-61-910/27/23 11:220.40 0.18 1
Benzyl alcohol ND mg/kg 10/30/23 11:49 100-51-610/27/23 11:220.80 0.30 1
Biphenyl (Diphenyl)ND mg/kg 10/30/23 11:49 92-52-410/27/23 11:220.40 0.095 1
4-Bromophenylphenyl ether ND mg/kg 10/30/23 11:49 101-55-310/27/23 11:220.40 0.15 1
Butylbenzylphthalate ND mg/kg 10/30/23 11:49 85-68-710/27/23 11:220.40 0.17 1
Caprolactam ND mg/kg 10/30/23 11:49 105-60-210/27/23 11:220.40 0.21 1
Carbazole ND mg/kg 10/30/23 11:49 86-74-810/27/23 11:220.40 0.14 1
4-Chloro-3-methylphenol ND mg/kg 10/30/23 11:49 59-50-710/27/23 11:220.80 0.28 1
4-Chloroaniline ND mg/kg 10/30/23 11:49 106-47-810/27/23 11:220.80 0.31 1
Chlorobenzilate ND mg/kg 10/30/23 11:49 510-15-610/27/23 11:220.40 0.079 1
bis(2-Chloroethoxy)methane ND mg/kg 10/30/23 11:49 111-91-110/27/23 11:220.40 0.17 1
bis(2-Chloroethyl) ether ND mg/kg 10/30/23 11:49 111-44-410/27/23 11:220.40 0.15 1
2-Chloronaphthalene ND mg/kg 10/30/23 11:49 91-58-710/27/23 11:220.40 0.16 1
2-Chlorophenol ND mg/kg 10/30/23 11:49 95-57-810/27/23 11:220.40 0.15 1
4-Chlorophenylphenyl ether ND mg/kg 10/30/23 11:49 7005-72-310/27/23 11:220.40 0.15 1
Chrysene ND mg/kg 10/30/23 11:49 218-01-910/27/23 11:220.40 0.15 1
Dibenz(a,h)anthracene ND mg/kg 10/30/23 11:49 53-70-310/27/23 11:220.40 0.15 1
Dibenzo(a,e)pyrene ND mg/kg 10/30/23 11:49 192-65-410/27/23 11:221.2 0.27 1
Dibenzofuran ND mg/kg 10/30/23 11:49 132-64-910/27/23 11:220.40 0.14 1
1,2-Dichlorobenzene ND mg/kg 10/30/23 11:49 95-50-110/27/23 11:220.40 0.14 1
1,3-Dichlorobenzene ND mg/kg 10/30/23 11:49 541-73-110/27/23 11:220.40 0.14 1
1,4-Dichlorobenzene ND mg/kg 10/30/23 11:49 106-46-710/27/23 11:220.40 0.15 1
3,3'-Dichlorobenzidine ND mg/kg 10/30/23 11:49 91-94-1 L210/27/23 11:220.80 0.27 1
2,4-Dichlorophenol ND mg/kg 10/30/23 11:49 120-83-210/27/23 11:220.40 0.16 1
2,6-Dichlorophenol ND mg/kg 10/30/23 11:49 87-65-0 L210/27/23 11:220.40 0.10 1
2,3-Dichloroaniline ND mg/kg 10/30/23 11:49 608-27-510/27/23 11:220.40 0.19 1
Diethylphthalate ND mg/kg 10/30/23 11:49 84-66-210/27/23 11:220.40 0.15 1
3,3'-Dimethylbenzidine ND mg/kg 10/30/23 11:49 119-93-7 IL10/27/23 11:220.80 0.36 1
2,4-Dimethylphenol ND mg/kg 10/30/23 11:49 105-67-910/27/23 11:220.40 0.17 1
Dimethylphthalate ND mg/kg 10/30/23 11:49 131-11-310/27/23 11:220.40 0.15 1
Di-n-butylphthalate ND mg/kg 10/30/23 11:49 84-74-210/27/23 11:220.40 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-2 Lab ID:92695355002 Collected:10/24/23 13:20 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
4,6-Dinitro-2-methylphenol ND mg/kg 10/30/23 11:49 534-52-110/27/23 11:220.80 0.37 1
1,3-Dinitrobenzene ND mg/kg 10/30/23 11:49 99-65-0 L210/27/23 11:220.40 0.090 1
1,4-Dinitrobenzene ND mg/kg 10/30/23 11:49 100-25-4 L210/27/23 11:220.40 0.12 1
2,4-Dinitrophenol ND mg/kg 10/30/23 11:49 51-28-510/27/23 11:222.0 1.2 1
2,4-Dinitrotoluene ND mg/kg 10/30/23 11:49 121-14-210/27/23 11:220.40 0.15 1
2,6-Dinitrotoluene ND mg/kg 10/30/23 11:49 606-20-210/27/23 11:220.40 0.15 1
Di-n-octylphthalate ND mg/kg 10/30/23 11:49 117-84-010/27/23 11:220.40 0.16 1
1,2-Diphenylhydrazine ND mg/kg 10/30/23 11:49 122-66-710/27/23 11:220.40 0.16 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/30/23 11:49 117-81-710/27/23 11:220.40 0.15 1
Fluoranthene ND mg/kg 10/30/23 11:49 206-44-010/27/23 11:220.40 0.14 1
Fluorene ND mg/kg 10/30/23 11:49 86-73-710/27/23 11:220.40 0.14 1
Hexachloro-1,3-butadiene ND mg/kg 10/30/23 11:49 87-68-310/27/23 11:220.40 0.17 1
Hexachlorobenzene ND mg/kg 10/30/23 11:49 118-74-110/27/23 11:220.40 0.16 1
Hexachlorocyclopentadiene ND mg/kg 10/30/23 11:49 77-47-410/27/23 11:220.40 0.23 1
Hexachloroethane ND mg/kg 10/30/23 11:49 67-72-110/27/23 11:220.40 0.15 1
Hexachlorophene ND mg/kg 10/30/23 11:49 70-30-4 IH,v210/27/23 11:224.0 2.3 1
Hexachloropropene ND mg/kg 10/30/23 11:49 1888-71-710/27/23 11:220.40 0.11 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/30/23 11:49 193-39-510/27/23 11:220.40 0.16 1
Isodrin ND mg/kg 10/30/23 11:49 465-73-610/27/23 11:220.40 0.095 1
1-Methylnaphthalene ND mg/kg 10/30/23 11:49 90-12-010/27/23 11:220.40 0.14 1
2-Methylnaphthalene ND mg/kg 10/30/23 11:49 91-57-610/27/23 11:220.40 0.16 1
2-Methyl-5-nitroaniline ND mg/kg 10/30/23 11:49 99-55-810/27/23 11:220.40 0.12 1
2-Methylphenol(o-Cresol)ND mg/kg 10/30/23 11:49 95-48-710/27/23 11:220.40 0.16 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/30/23 11:49 15831-10-410/27/23 11:220.40 0.16 1
1-Naphthalenamine ND mg/kg 10/30/23 11:49 134-32-710/27/23 11:220.80 0.13 1
2-Naphthalenamine ND mg/kg 10/30/23 11:49 91-59-810/27/23 11:220.80 0.15 1
Naphthalene ND mg/kg 10/30/23 11:49 91-20-310/27/23 11:220.40 0.14 1
2-Nitroaniline ND mg/kg 10/30/23 11:49 88-74-410/27/23 11:222.0 0.33 1
3-Nitroaniline ND mg/kg 10/30/23 11:49 99-09-210/27/23 11:222.0 0.31 1
4-Nitroaniline ND mg/kg 10/30/23 11:49 100-01-610/27/23 11:220.80 0.30 1
Nitrobenzene ND mg/kg 10/30/23 11:49 98-95-310/27/23 11:220.40 0.19 1
2-Nitrophenol ND mg/kg 10/30/23 11:49 88-75-510/27/23 11:220.40 0.17 1
4-Nitrophenol ND mg/kg 10/30/23 11:49 100-02-710/27/23 11:222.0 0.77 1
N-Nitroso-di-n-propylamine ND mg/kg 10/30/23 11:49 621-64-710/27/23 11:220.40 0.15 1
Pentachlorophenol ND mg/kg 10/30/23 11:49 87-86-510/27/23 11:220.80 0.39 1
Phenanthrene ND mg/kg 10/30/23 11:49 85-01-810/27/23 11:220.40 0.13 1
Phenol ND mg/kg 10/30/23 11:49 108-95-210/27/23 11:220.40 0.18 1
Pyrene ND mg/kg 10/30/23 11:49 129-00-010/27/23 11:220.40 0.16 1
Pyridine ND mg/kg 10/30/23 11:49 110-86-1 v110/27/23 11:220.40 0.13 1
1,2,4,5-Tetrachlorobenzene ND mg/kg 10/30/23 11:49 95-94-310/27/23 11:220.40 0.097 1
2,3,4,6-Tetrachlorophenol ND mg/kg 10/30/23 11:49 58-90-210/27/23 11:220.40 0.10 1
2,4,5-Trichlorophenol ND mg/kg 10/30/23 11:49 95-95-410/27/23 11:220.40 0.18 1
2,4,6-Trichlorophenol ND mg/kg 10/30/23 11:49 88-06-210/27/23 11:220.40 0.16 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-2 Lab ID:92695355002 Collected:10/24/23 13:20 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorobiphenyl (S)22 %10/30/23 11:49 321-60-810/27/23 11:2210-130 1
Terphenyl-d14 (S)29 %10/30/23 11:49 1718-51-010/27/23 11:2210-130 1
Phenol-d6 (S)27 %10/30/23 11:49 13127-88-310/27/23 11:2210-130 1
2-Fluorophenol (S)26 %10/30/23 11:49 367-12-410/27/23 11:2210-130 1
2,4,6-Tribromophenol (S)17 %10/30/23 11:49 118-79-610/27/23 11:2210-130 1
Nitrobenzene-d5 (S)34 %10/30/23 11:49 4165-60-010/27/23 11:2210-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/27/23 20:30 67-64-110/27/23 14:400.14 0.044 1
Benzene ND mg/kg 10/27/23 20:30 71-43-2 M110/27/23 14:400.0068 0.0027 1
Bromobenzene ND mg/kg 10/27/23 20:30 108-86-1 M110/27/23 14:400.0068 0.0022 1
Bromochloromethane ND mg/kg 10/27/23 20:30 74-97-5 M110/27/23 14:400.0068 0.0020 1
Bromodichloromethane ND mg/kg 10/27/23 20:30 75-27-4 M110/27/23 14:400.0068 0.0026 1
Bromoform ND mg/kg 10/27/23 20:30 75-25-2 M110/27/23 14:400.0068 0.0024 1
Bromomethane ND mg/kg 10/27/23 20:30 74-83-9 IK,M1,
v1
10/27/23 14:400.027 0.021 1
2-Butanone (MEK)ND mg/kg 10/27/23 20:30 78-93-310/27/23 14:400.14 0.033 1
n-Butylbenzene ND mg/kg 10/27/23 20:30 104-51-810/27/23 14:400.0068 0.0043 1
sec-Butylbenzene ND mg/kg 10/27/23 20:30 135-98-8 M110/27/23 14:400.0068 0.0030 1
tert-Butylbenzene ND mg/kg 10/27/23 20:30 98-06-6 M110/27/23 14:400.0068 0.0024 1
Carbon tetrachloride ND mg/kg 10/27/23 20:30 56-23-5 M110/27/23 14:400.0068 0.0025 1
Chlorobenzene ND mg/kg 10/27/23 20:30 108-90-7 M110/27/23 14:400.0068 0.0039 1
Chloroethane ND mg/kg 10/27/23 20:30 75-00-3 M110/27/23 14:400.014 0.0052 1
Chloroform ND mg/kg 10/27/23 20:30 67-66-3 M110/27/23 14:400.0068 0.0057 1
Chloromethane ND mg/kg 10/27/23 20:30 74-87-3 M110/27/23 14:400.014 0.0057 1
2-Chlorotoluene ND mg/kg 10/27/23 20:30 95-49-8 M110/27/23 14:400.0068 0.0024 1
4-Chlorotoluene ND mg/kg 10/27/23 20:30 106-43-4 M110/27/23 14:400.0068 0.0038 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/27/23 20:30 96-12-810/27/23 14:400.0068 0.0026 1
Dibromochloromethane ND mg/kg 10/27/23 20:30 124-48-1 M110/27/23 14:400.0068 0.0038 1
1,2-Dibromoethane (EDB)ND mg/kg 10/27/23 20:30 106-93-4 M110/27/23 14:400.0068 0.0030 1
Dibromomethane ND mg/kg 10/27/23 20:30 74-95-3 M110/27/23 14:400.0068 0.0015 1
1,2-Dichlorobenzene ND mg/kg 10/27/23 20:30 95-50-1 M110/27/23 14:400.0068 0.0024 1
1,3-Dichlorobenzene ND mg/kg 10/27/23 20:30 541-73-1 M110/27/23 14:400.0068 0.0021 1
1,4-Dichlorobenzene ND mg/kg 10/27/23 20:30 106-46-7 M110/27/23 14:400.0068 0.0018 1
Dichlorodifluoromethane ND mg/kg 10/27/23 20:30 75-71-810/27/23 14:400.014 0.0069 1
1,1-Dichloroethane ND mg/kg 10/27/23 20:30 75-34-3 M110/27/23 14:400.0068 0.0028 1
1,2-Dichloroethane ND mg/kg 10/27/23 20:30 107-06-2 M110/27/23 14:400.0068 0.0045 1
1,1-Dichloroethene ND mg/kg 10/27/23 20:30 75-35-4 M110/27/23 14:400.0068 0.0028 1
cis-1,2-Dichloroethene ND mg/kg 10/27/23 20:30 156-59-2 M110/27/23 14:400.0068 0.0023 1
trans-1,2-Dichloroethene ND mg/kg 10/27/23 20:30 156-60-5 M110/27/23 14:400.0068 0.0058 1
1,2-Dichloropropane ND mg/kg 10/27/23 20:30 78-87-5 M110/27/23 14:400.0068 0.0020 1
1,3-Dichloropropane ND mg/kg 10/27/23 20:30 142-28-9 M110/27/23 14:400.0068 0.0021 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-2 Lab ID:92695355002 Collected:10/24/23 13:20 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND mg/kg 10/27/23 20:30 594-20-710/27/23 14:400.0068 0.0051 1
1,1-Dichloropropene ND mg/kg 10/27/23 20:30 563-58-6 M110/27/23 14:400.0068 0.0033 1
cis-1,3-Dichloropropene ND mg/kg 10/27/23 20:30 10061-01-5 M110/27/23 14:400.0068 0.0018 1
trans-1,3-Dichloropropene ND mg/kg 10/27/23 20:30 10061-02-6 M110/27/23 14:400.0068 0.0023 1
Diisopropyl ether ND mg/kg 10/27/23 20:30 108-20-3 M110/27/23 14:400.0068 0.0018 1
Ethylbenzene 0.0052J mg/kg 10/27/23 20:30 100-41-4 M110/27/23 14:400.0068 0.0032 1
Hexachloro-1,3-butadiene ND mg/kg 10/27/23 20:30 87-68-310/27/23 14:400.014 0.011 1
2-Hexanone ND mg/kg 10/27/23 20:30 591-78-6 M110/27/23 14:400.068 0.0065 1
Isopropylbenzene (Cumene)ND mg/kg 10/27/23 20:30 98-82-8 M110/27/23 14:400.0068 0.0023 1
p-Isopropyltoluene ND mg/kg 10/27/23 20:30 99-87-610/27/23 14:400.0068 0.0033 1
Methylene Chloride ND mg/kg 10/27/23 20:30 75-09-210/27/23 14:400.027 0.019 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/27/23 20:30 108-10-1 M110/27/23 14:400.068 0.0065 1
Methyl-tert-butyl ether ND mg/kg 10/27/23 20:30 1634-04-4 M110/27/23 14:400.0068 0.0025 1
Naphthalene ND mg/kg 10/27/23 20:30 91-20-310/27/23 14:400.0068 0.0036 1
n-Propylbenzene ND mg/kg 10/27/23 20:30 103-65-110/27/23 14:400.0068 0.0024 1
Styrene ND mg/kg 10/27/23 20:30 100-42-5 M110/27/23 14:400.0068 0.0018 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/27/23 20:30 630-20-6 M110/27/23 14:400.0068 0.0026 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/27/23 20:30 79-34-5 M110/27/23 14:400.0068 0.0018 1
Tetrachloroethene ND mg/kg 10/27/23 20:30 127-18-410/27/23 14:400.0068 0.0021 1
Toluene ND mg/kg 10/27/23 20:30 108-88-3 M110/27/23 14:400.0068 0.0047 1
1,2,3-Trichlorobenzene ND mg/kg 10/27/23 20:30 87-61-6 M110/27/23 14:400.0068 0.0055 1
1,2,4-Trichlorobenzene ND mg/kg 10/27/23 20:30 120-82-110/27/23 14:400.0068 0.0057 1
1,1,1-Trichloroethane ND mg/kg 10/27/23 20:30 71-55-6 M110/27/23 14:400.0068 0.0035 1
1,1,2-Trichloroethane ND mg/kg 10/27/23 20:30 79-00-5 M110/27/23 14:400.0068 0.0023 1
Trichloroethene ND mg/kg 10/27/23 20:30 79-01-6 M110/27/23 14:400.0068 0.0055 1
Trichlorofluoromethane ND mg/kg 10/27/23 20:30 75-69-4 M110/27/23 14:400.0068 0.0037 1
1,2,3-Trichloropropane ND mg/kg 10/27/23 20:30 96-18-4 M110/27/23 14:400.0068 0.0034 1
1,2,4-Trimethylbenzene ND mg/kg 10/27/23 20:30 95-63-610/27/23 14:400.0068 0.0040 1
1,3,5-Trimethylbenzene ND mg/kg 10/27/23 20:30 108-67-8 M110/27/23 14:400.0068 0.0023 1
Vinyl acetate ND mg/kg 10/27/23 20:30 108-05-410/27/23 14:400.068 0.014 1
Vinyl chloride ND mg/kg 10/27/23 20:30 75-01-4 M110/27/23 14:400.014 0.0034 1
Xylene (Total)ND mg/kg 10/27/23 20:30 1330-20-7 MS10/27/23 14:400.014 0.0039 1
m&p-Xylene ND mg/kg 10/27/23 20:30 179601-23-1 M110/27/23 14:400.014 0.0046 1
o-Xylene ND mg/kg 10/27/23 20:30 95-47-6 M110/27/23 14:400.0068 0.0030 1
Surrogates
Toluene-d8 (S)101 %10/27/23 20:30 2037-26-510/27/23 14:4070-130 1
4-Bromofluorobenzene (S)100 %10/27/23 20:30 460-00-410/27/23 14:4070-130 1
1,2-Dichloroethane-d4 (S)102 %10/27/23 20:30 17060-07-010/27/23 14:4070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.9 %10/26/23 17:15 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-2 Lab ID:92695355002 Collected:10/24/23 13:20 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 79.4 %11/01/23 10:2011/01/23 10:141
Sample:SB-SG-3 Lab ID:92695355003 Collected:10/24/23 13:30 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.57J mg/kg 10/27/23 18:34 18540-29-910/27/23 09:451.1 0.0011 1
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.12 mg/kg 11/02/23 12:25 7440-38-211/01/23 07:521.22 0.122 5
Barium 16.0 mg/kg 11/02/23 12:25 7440-39-311/01/23 07:523.06 0.186 5
Cadmium ND mg/kg 11/02/23 12:25 7440-43-911/01/23 07:521.22 0.105 5
Chromium 39.4 mg/kg 11/02/23 12:25 7440-47-311/01/23 07:526.12 0.362 5
Lead 7.82 mg/kg 11/02/23 12:25 7439-92-111/01/23 07:522.45 0.121 5
Selenium 0.846J mg/kg 11/02/23 12:25 7782-49-2 J11/01/23 07:523.06 0.220 5
Silver ND mg/kg 11/02/23 12:25 7440-22-411/01/23 07:520.612 0.106 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0381J mg/kg 11/01/23 18:17 7439-97-6 J10/31/23 22:140.0490 0.0220 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/30/23 12:17 83-32-910/27/23 11:220.39 0.14 1
Acenaphthylene ND mg/kg 10/30/23 12:17 208-96-810/27/23 11:220.39 0.14 1
Acetophenone ND mg/kg 10/30/23 12:17 98-86-210/27/23 11:220.39 0.10 1
Aniline ND mg/kg 10/30/23 12:17 62-53-310/27/23 11:220.39 0.15 1
Atrazine ND mg/kg 10/30/23 12:17 1912-24-910/27/23 11:220.39 0.12 1
Benzaldehyde ND mg/kg 10/30/23 12:17 100-52-710/27/23 11:220.39 0.13 1
Benzidine ND mg/kg 10/30/23 12:17 92-87-510/27/23 11:221.9 0.32 1
Benzo(a)anthracene ND mg/kg 10/30/23 12:17 56-55-310/27/23 11:220.39 0.13 1
Benzo(a)pyrene ND mg/kg 10/30/23 12:17 50-32-810/27/23 11:220.39 0.13 1
Benzo(b)fluoranthene ND mg/kg 10/30/23 12:17 205-99-210/27/23 11:220.39 0.13 1
Benzo(g,h,i)perylene ND mg/kg 10/30/23 12:17 191-24-210/27/23 11:220.39 0.15 1
Benzo(k)fluoranthene ND mg/kg 10/30/23 12:17 207-08-910/27/23 11:220.39 0.14 1
Benzoic Acid ND mg/kg 10/30/23 12:17 65-85-010/27/23 11:221.9 0.83 1
Benzophenone ND mg/kg 10/30/23 12:17 119-61-910/27/23 11:220.39 0.18 1
Benzyl alcohol ND mg/kg 10/30/23 12:17 100-51-610/27/23 11:220.78 0.29 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-3 Lab ID:92695355003 Collected:10/24/23 13:30 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Biphenyl (Diphenyl)ND mg/kg 10/30/23 12:17 92-52-410/27/23 11:220.39 0.092 1
4-Bromophenylphenyl ether ND mg/kg 10/30/23 12:17 101-55-310/27/23 11:220.39 0.15 1
Butylbenzylphthalate ND mg/kg 10/30/23 12:17 85-68-710/27/23 11:220.39 0.16 1
Caprolactam ND mg/kg 10/30/23 12:17 105-60-210/27/23 11:220.39 0.21 1
Carbazole ND mg/kg 10/30/23 12:17 86-74-810/27/23 11:220.39 0.13 1
4-Chloro-3-methylphenol ND mg/kg 10/30/23 12:17 59-50-710/27/23 11:220.78 0.27 1
4-Chloroaniline ND mg/kg 10/30/23 12:17 106-47-810/27/23 11:220.78 0.30 1
Chlorobenzilate ND mg/kg 10/30/23 12:17 510-15-610/27/23 11:220.39 0.077 1
bis(2-Chloroethoxy)methane ND mg/kg 10/30/23 12:17 111-91-110/27/23 11:220.39 0.16 1
bis(2-Chloroethyl) ether ND mg/kg 10/30/23 12:17 111-44-410/27/23 11:220.39 0.15 1
2-Chloronaphthalene ND mg/kg 10/30/23 12:17 91-58-710/27/23 11:220.39 0.15 1
2-Chlorophenol ND mg/kg 10/30/23 12:17 95-57-810/27/23 11:220.39 0.15 1
4-Chlorophenylphenyl ether ND mg/kg 10/30/23 12:17 7005-72-310/27/23 11:220.39 0.14 1
Chrysene ND mg/kg 10/30/23 12:17 218-01-910/27/23 11:220.39 0.14 1
Dibenz(a,h)anthracene ND mg/kg 10/30/23 12:17 53-70-310/27/23 11:220.39 0.15 1
Dibenzo(a,e)pyrene ND mg/kg 10/30/23 12:17 192-65-410/27/23 11:221.2 0.26 1
Dibenzofuran ND mg/kg 10/30/23 12:17 132-64-910/27/23 11:220.39 0.14 1
1,2-Dichlorobenzene ND mg/kg 10/30/23 12:17 95-50-110/27/23 11:220.39 0.14 1
1,3-Dichlorobenzene ND mg/kg 10/30/23 12:17 541-73-110/27/23 11:220.39 0.14 1
1,4-Dichlorobenzene ND mg/kg 10/30/23 12:17 106-46-710/27/23 11:220.39 0.15 1
3,3'-Dichlorobenzidine ND mg/kg 10/30/23 12:17 91-94-1 L210/27/23 11:220.78 0.26 1
2,4-Dichlorophenol ND mg/kg 10/30/23 12:17 120-83-210/27/23 11:220.39 0.15 1
2,6-Dichlorophenol ND mg/kg 10/30/23 12:17 87-65-0 L210/27/23 11:220.39 0.099 1
2,3-Dichloroaniline ND mg/kg 10/30/23 12:17 608-27-510/27/23 11:220.39 0.19 1
Diethylphthalate ND mg/kg 10/30/23 12:17 84-66-210/27/23 11:220.39 0.14 1
3,3'-Dimethylbenzidine ND mg/kg 10/30/23 12:17 119-93-7 IL10/27/23 11:220.78 0.35 1
2,4-Dimethylphenol ND mg/kg 10/30/23 12:17 105-67-910/27/23 11:220.39 0.16 1
Dimethylphthalate ND mg/kg 10/30/23 12:17 131-11-310/27/23 11:220.39 0.14 1
Di-n-butylphthalate ND mg/kg 10/30/23 12:17 84-74-210/27/23 11:220.39 0.13 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/30/23 12:17 534-52-110/27/23 11:220.78 0.36 1
1,3-Dinitrobenzene ND mg/kg 10/30/23 12:17 99-65-0 L210/27/23 11:220.39 0.087 1
1,4-Dinitrobenzene ND mg/kg 10/30/23 12:17 100-25-4 L210/27/23 11:220.39 0.11 1
2,4-Dinitrophenol ND mg/kg 10/30/23 12:17 51-28-510/27/23 11:221.9 1.2 1
2,4-Dinitrotoluene ND mg/kg 10/30/23 12:17 121-14-210/27/23 11:220.39 0.15 1
2,6-Dinitrotoluene ND mg/kg 10/30/23 12:17 606-20-210/27/23 11:220.39 0.14 1
Di-n-octylphthalate ND mg/kg 10/30/23 12:17 117-84-010/27/23 11:220.39 0.15 1
1,2-Diphenylhydrazine ND mg/kg 10/30/23 12:17 122-66-710/27/23 11:220.39 0.15 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/30/23 12:17 117-81-710/27/23 11:220.39 0.15 1
Fluoranthene ND mg/kg 10/30/23 12:17 206-44-010/27/23 11:220.39 0.13 1
Fluorene ND mg/kg 10/30/23 12:17 86-73-710/27/23 11:220.39 0.14 1
Hexachloro-1,3-butadiene ND mg/kg 10/30/23 12:17 87-68-310/27/23 11:220.39 0.17 1
Hexachlorobenzene ND mg/kg 10/30/23 12:17 118-74-110/27/23 11:220.39 0.15 1
Hexachlorocyclopentadiene ND mg/kg 10/30/23 12:17 77-47-410/27/23 11:220.39 0.22 1
Hexachloroethane ND mg/kg 10/30/23 12:17 67-72-110/27/23 11:220.39 0.15 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-3 Lab ID:92695355003 Collected:10/24/23 13:30 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Hexachlorophene ND mg/kg 10/30/23 12:17 70-30-4 IH,v210/27/23 11:223.9 2.3 1
Hexachloropropene ND mg/kg 10/30/23 12:17 1888-71-710/27/23 11:220.39 0.11 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/30/23 12:17 193-39-510/27/23 11:220.39 0.15 1
Isodrin ND mg/kg 10/30/23 12:17 465-73-610/27/23 11:220.39 0.092 1
1-Methylnaphthalene ND mg/kg 10/30/23 12:17 90-12-010/27/23 11:220.39 0.14 1
2-Methylnaphthalene ND mg/kg 10/30/23 12:17 91-57-610/27/23 11:220.39 0.16 1
2-Methyl-5-nitroaniline ND mg/kg 10/30/23 12:17 99-55-810/27/23 11:220.39 0.12 1
2-Methylphenol(o-Cresol)ND mg/kg 10/30/23 12:17 95-48-710/27/23 11:220.39 0.16 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/30/23 12:17 15831-10-410/27/23 11:220.39 0.16 1
1-Naphthalenamine ND mg/kg 10/30/23 12:17 134-32-710/27/23 11:220.78 0.13 1
2-Naphthalenamine ND mg/kg 10/30/23 12:17 91-59-810/27/23 11:220.78 0.15 1
Naphthalene ND mg/kg 10/30/23 12:17 91-20-310/27/23 11:220.39 0.13 1
2-Nitroaniline ND mg/kg 10/30/23 12:17 88-74-410/27/23 11:221.9 0.32 1
3-Nitroaniline ND mg/kg 10/30/23 12:17 99-09-210/27/23 11:221.9 0.30 1
4-Nitroaniline ND mg/kg 10/30/23 12:17 100-01-610/27/23 11:220.78 0.30 1
Nitrobenzene ND mg/kg 10/30/23 12:17 98-95-310/27/23 11:220.39 0.18 1
2-Nitrophenol ND mg/kg 10/30/23 12:17 88-75-510/27/23 11:220.39 0.17 1
4-Nitrophenol ND mg/kg 10/30/23 12:17 100-02-710/27/23 11:221.9 0.75 1
N-Nitroso-di-n-propylamine ND mg/kg 10/30/23 12:17 621-64-710/27/23 11:220.39 0.15 1
Pentachlorophenol ND mg/kg 10/30/23 12:17 87-86-510/27/23 11:220.78 0.38 1
Phenanthrene ND mg/kg 10/30/23 12:17 85-01-810/27/23 11:220.39 0.13 1
Phenol ND mg/kg 10/30/23 12:17 108-95-210/27/23 11:220.39 0.17 1
Pyrene ND mg/kg 10/30/23 12:17 129-00-010/27/23 11:220.39 0.16 1
Pyridine ND mg/kg 10/30/23 12:17 110-86-1 v110/27/23 11:220.39 0.12 1
1,2,4,5-Tetrachlorobenzene ND mg/kg 10/30/23 12:17 95-94-310/27/23 11:220.39 0.095 1
2,3,4,6-Tetrachlorophenol ND mg/kg 10/30/23 12:17 58-90-210/27/23 11:220.39 0.097 1
2,4,5-Trichlorophenol ND mg/kg 10/30/23 12:17 95-95-410/27/23 11:220.39 0.18 1
2,4,6-Trichlorophenol ND mg/kg 10/30/23 12:17 88-06-210/27/23 11:220.39 0.16 1
Surrogates
2-Fluorobiphenyl (S)31 %10/30/23 12:17 321-60-810/27/23 11:2210-130 1
Terphenyl-d14 (S)35 %10/30/23 12:17 1718-51-010/27/23 11:2210-130 1
Phenol-d6 (S)41 %10/30/23 12:17 13127-88-310/27/23 11:2210-130 1
2-Fluorophenol (S)45 %10/30/23 12:17 367-12-410/27/23 11:2210-130 1
2,4,6-Tribromophenol (S)42 %10/30/23 12:17 118-79-610/27/23 11:2210-130 1
Nitrobenzene-d5 (S)46 %10/30/23 12:17 4165-60-010/27/23 11:2210-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/27/23 22:21 67-64-110/27/23 14:400.12 0.038 1
Benzene ND mg/kg 10/27/23 22:21 71-43-210/27/23 14:400.0059 0.0023 1
Bromobenzene ND mg/kg 10/27/23 22:21 108-86-110/27/23 14:400.0059 0.0019 1
Bromochloromethane ND mg/kg 10/27/23 22:21 74-97-510/27/23 14:400.0059 0.0017 1
Bromodichloromethane ND mg/kg 10/27/23 22:21 75-27-410/27/23 14:400.0059 0.0023 1
Bromoform ND mg/kg 10/27/23 22:21 75-25-210/27/23 14:400.0059 0.0021 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-3 Lab ID:92695355003 Collected:10/24/23 13:30 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Bromomethane ND mg/kg 10/27/23 22:21 74-83-9 IK,v110/27/23 14:400.024 0.018 1
2-Butanone (MEK)ND mg/kg 10/27/23 22:21 78-93-310/27/23 14:400.12 0.028 1
n-Butylbenzene ND mg/kg 10/27/23 22:21 104-51-810/27/23 14:400.0059 0.0037 1
sec-Butylbenzene ND mg/kg 10/27/23 22:21 135-98-810/27/23 14:400.0059 0.0026 1
tert-Butylbenzene ND mg/kg 10/27/23 22:21 98-06-610/27/23 14:400.0059 0.0021 1
Carbon tetrachloride ND mg/kg 10/27/23 22:21 56-23-510/27/23 14:400.0059 0.0022 1
Chlorobenzene ND mg/kg 10/27/23 22:21 108-90-710/27/23 14:400.0059 0.0034 1
Chloroethane ND mg/kg 10/27/23 22:21 75-00-310/27/23 14:400.012 0.0045 1
Chloroform ND mg/kg 10/27/23 22:21 67-66-310/27/23 14:400.0059 0.0049 1
Chloromethane ND mg/kg 10/27/23 22:21 74-87-310/27/23 14:400.012 0.0049 1
2-Chlorotoluene ND mg/kg 10/27/23 22:21 95-49-810/27/23 14:400.0059 0.0021 1
4-Chlorotoluene ND mg/kg 10/27/23 22:21 106-43-410/27/23 14:400.0059 0.0033 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/27/23 22:21 96-12-810/27/23 14:400.0059 0.0023 1
Dibromochloromethane ND mg/kg 10/27/23 22:21 124-48-110/27/23 14:400.0059 0.0033 1
1,2-Dibromoethane (EDB)ND mg/kg 10/27/23 22:21 106-93-410/27/23 14:400.0059 0.0026 1
Dibromomethane ND mg/kg 10/27/23 22:21 74-95-310/27/23 14:400.0059 0.0013 1
1,2-Dichlorobenzene ND mg/kg 10/27/23 22:21 95-50-110/27/23 14:400.0059 0.0021 1
1,3-Dichlorobenzene ND mg/kg 10/27/23 22:21 541-73-110/27/23 14:400.0059 0.0018 1
1,4-Dichlorobenzene ND mg/kg 10/27/23 22:21 106-46-710/27/23 14:400.0059 0.0015 1
Dichlorodifluoromethane ND mg/kg 10/27/23 22:21 75-71-810/27/23 14:400.012 0.0060 1
1,1-Dichloroethane ND mg/kg 10/27/23 22:21 75-34-310/27/23 14:400.0059 0.0024 1
1,2-Dichloroethane ND mg/kg 10/27/23 22:21 107-06-210/27/23 14:400.0059 0.0039 1
1,1-Dichloroethene ND mg/kg 10/27/23 22:21 75-35-410/27/23 14:400.0059 0.0024 1
cis-1,2-Dichloroethene ND mg/kg 10/27/23 22:21 156-59-210/27/23 14:400.0059 0.0020 1
trans-1,2-Dichloroethene ND mg/kg 10/27/23 22:21 156-60-510/27/23 14:400.0059 0.0050 1
1,2-Dichloropropane ND mg/kg 10/27/23 22:21 78-87-510/27/23 14:400.0059 0.0018 1
1,3-Dichloropropane ND mg/kg 10/27/23 22:21 142-28-910/27/23 14:400.0059 0.0018 1
2,2-Dichloropropane ND mg/kg 10/27/23 22:21 594-20-710/27/23 14:400.0059 0.0045 1
1,1-Dichloropropene ND mg/kg 10/27/23 22:21 563-58-610/27/23 14:400.0059 0.0028 1
cis-1,3-Dichloropropene ND mg/kg 10/27/23 22:21 10061-01-510/27/23 14:400.0059 0.0016 1
trans-1,3-Dichloropropene ND mg/kg 10/27/23 22:21 10061-02-610/27/23 14:400.0059 0.0020 1
Diisopropyl ether ND mg/kg 10/27/23 22:21 108-20-310/27/23 14:400.0059 0.0016 1
Ethylbenzene 0.0062 mg/kg 10/27/23 22:21 100-41-410/27/23 14:400.0059 0.0027 1
Hexachloro-1,3-butadiene ND mg/kg 10/27/23 22:21 87-68-310/27/23 14:400.012 0.0096 1
2-Hexanone ND mg/kg 10/27/23 22:21 591-78-610/27/23 14:400.059 0.0057 1
Isopropylbenzene (Cumene)ND mg/kg 10/27/23 22:21 98-82-810/27/23 14:400.0059 0.0020 1
p-Isopropyltoluene ND mg/kg 10/27/23 22:21 99-87-610/27/23 14:400.0059 0.0029 1
Methylene Chloride ND mg/kg 10/27/23 22:21 75-09-210/27/23 14:400.024 0.016 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/27/23 22:21 108-10-110/27/23 14:400.059 0.0057 1
Methyl-tert-butyl ether ND mg/kg 10/27/23 22:21 1634-04-410/27/23 14:400.0059 0.0022 1
Naphthalene 0.015 mg/kg 10/27/23 22:21 91-20-310/27/23 14:400.0059 0.0031 1
n-Propylbenzene ND mg/kg 10/27/23 22:21 103-65-110/27/23 14:400.0059 0.0021 1
Styrene ND mg/kg 10/27/23 22:21 100-42-510/27/23 14:400.0059 0.0016 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/27/23 22:21 630-20-610/27/23 14:400.0059 0.0023 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-3 Lab ID:92695355003 Collected:10/24/23 13:30 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2,2-Tetrachloroethane ND mg/kg 10/27/23 22:21 79-34-510/27/23 14:400.0059 0.0016 1
Tetrachloroethene ND mg/kg 10/27/23 22:21 127-18-410/27/23 14:400.0059 0.0019 1
Toluene 0.0062 mg/kg 10/27/23 22:21 108-88-310/27/23 14:400.0059 0.0041 1
1,2,3-Trichlorobenzene ND mg/kg 10/27/23 22:21 87-61-610/27/23 14:400.0059 0.0048 1
1,2,4-Trichlorobenzene ND mg/kg 10/27/23 22:21 120-82-110/27/23 14:400.0059 0.0049 1
1,1,1-Trichloroethane ND mg/kg 10/27/23 22:21 71-55-610/27/23 14:400.0059 0.0031 1
1,1,2-Trichloroethane ND mg/kg 10/27/23 22:21 79-00-510/27/23 14:400.0059 0.0020 1
Trichloroethene ND mg/kg 10/27/23 22:21 79-01-610/27/23 14:400.0059 0.0047 1
Trichlorofluoromethane ND mg/kg 10/27/23 22:21 75-69-410/27/23 14:400.0059 0.0032 1
1,2,3-Trichloropropane ND mg/kg 10/27/23 22:21 96-18-410/27/23 14:400.0059 0.0030 1
1,2,4-Trimethylbenzene 0.0055J mg/kg 10/27/23 22:21 95-63-610/27/23 14:400.0059 0.0035 1
1,3,5-Trimethylbenzene 0.0031J mg/kg 10/27/23 22:21 108-67-810/27/23 14:400.0059 0.0020 1
Vinyl acetate ND mg/kg 10/27/23 22:21 108-05-410/27/23 14:400.059 0.012 1
Vinyl chloride ND mg/kg 10/27/23 22:21 75-01-410/27/23 14:400.012 0.0030 1
Xylene (Total)ND mg/kg 10/27/23 22:21 1330-20-710/27/23 14:400.012 0.0034 1
m&p-Xylene 0.011J mg/kg 10/27/23 22:21 179601-23-110/27/23 14:400.012 0.0040 1
o-Xylene 0.0052J mg/kg 10/27/23 22:21 95-47-610/27/23 14:400.0059 0.0026 1
Surrogates
Toluene-d8 (S)101 %10/27/23 22:21 2037-26-510/27/23 14:4070-130 1
4-Bromofluorobenzene (S)99 %10/27/23 22:21 460-00-410/27/23 14:4070-130 1
1,2-Dichloroethane-d4 (S)99 %10/27/23 22:21 17060-07-010/27/23 14:4070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.7 %10/26/23 17:15 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 81.7 %11/01/23 10:2011/01/23 10:141
Sample:SB-SG-4 Lab ID:92695355004 Collected:10/24/23 13:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 1.0J mg/kg 10/27/23 18:52 18540-29-910/27/23 09:451.3 0.0013 1
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 3.96 mg/kg 11/02/23 12:29 7440-38-211/01/23 07:521.41 0.141 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-4 Lab ID:92695355004 Collected:10/24/23 13:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Barium 14.6 mg/kg 11/02/23 12:29 7440-39-311/01/23 07:523.52 0.214 5
Cadmium ND mg/kg 11/02/23 12:29 7440-43-911/01/23 07:521.41 0.120 5
Chromium 58.4 mg/kg 11/02/23 12:29 7440-47-311/01/23 07:527.04 0.417 5
Lead 6.99 mg/kg 11/02/23 12:29 7439-92-111/01/23 07:522.82 0.139 5
Selenium 1.01J mg/kg 11/02/23 12:29 7782-49-2 J11/01/23 07:523.52 0.254 5
Silver ND mg/kg 11/02/23 12:29 7440-22-411/01/23 07:520.704 0.122 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0344J mg/kg 11/01/23 18:20 7439-97-6 J10/31/23 22:140.0564 0.0254 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/30/23 12:45 83-32-910/27/23 11:220.45 0.16 1
Acenaphthylene ND mg/kg 10/30/23 12:45 208-96-810/27/23 11:220.45 0.16 1
Acetophenone ND mg/kg 10/30/23 12:45 98-86-210/27/23 11:220.45 0.12 1
Aniline ND mg/kg 10/30/23 12:45 62-53-310/27/23 11:220.45 0.18 1
Atrazine ND mg/kg 10/30/23 12:45 1912-24-910/27/23 11:220.45 0.14 1
Benzaldehyde ND mg/kg 10/30/23 12:45 100-52-710/27/23 11:220.45 0.15 1
Benzidine ND mg/kg 10/30/23 12:45 92-87-510/27/23 11:222.3 0.37 1
Benzo(a)anthracene ND mg/kg 10/30/23 12:45 56-55-310/27/23 11:220.45 0.15 1
Benzo(a)pyrene ND mg/kg 10/30/23 12:45 50-32-810/27/23 11:220.45 0.16 1
Benzo(b)fluoranthene ND mg/kg 10/30/23 12:45 205-99-210/27/23 11:220.45 0.15 1
Benzo(g,h,i)perylene ND mg/kg 10/30/23 12:45 191-24-210/27/23 11:220.45 0.17 1
Benzo(k)fluoranthene ND mg/kg 10/30/23 12:45 207-08-910/27/23 11:220.45 0.16 1
Benzoic Acid ND mg/kg 10/30/23 12:45 65-85-010/27/23 11:222.3 0.97 1
Benzophenone ND mg/kg 10/30/23 12:45 119-61-910/27/23 11:220.45 0.20 1
Benzyl alcohol ND mg/kg 10/30/23 12:45 100-51-610/27/23 11:220.90 0.34 1
Biphenyl (Diphenyl)ND mg/kg 10/30/23 12:45 92-52-410/27/23 11:220.45 0.11 1
4-Bromophenylphenyl ether ND mg/kg 10/30/23 12:45 101-55-310/27/23 11:220.45 0.17 1
Butylbenzylphthalate ND mg/kg 10/30/23 12:45 85-68-710/27/23 11:220.45 0.19 1
Caprolactam ND mg/kg 10/30/23 12:45 105-60-210/27/23 11:220.45 0.24 1
Carbazole ND mg/kg 10/30/23 12:45 86-74-810/27/23 11:220.45 0.15 1
4-Chloro-3-methylphenol ND mg/kg 10/30/23 12:45 59-50-710/27/23 11:220.90 0.32 1
4-Chloroaniline ND mg/kg 10/30/23 12:45 106-47-810/27/23 11:220.90 0.35 1
Chlorobenzilate ND mg/kg 10/30/23 12:45 510-15-610/27/23 11:220.45 0.089 1
bis(2-Chloroethoxy)methane ND mg/kg 10/30/23 12:45 111-91-110/27/23 11:220.45 0.19 1
bis(2-Chloroethyl) ether ND mg/kg 10/30/23 12:45 111-44-410/27/23 11:220.45 0.17 1
2-Chloronaphthalene ND mg/kg 10/30/23 12:45 91-58-710/27/23 11:220.45 0.18 1
2-Chlorophenol ND mg/kg 10/30/23 12:45 95-57-810/27/23 11:220.45 0.17 1
4-Chlorophenylphenyl ether ND mg/kg 10/30/23 12:45 7005-72-310/27/23 11:220.45 0.17 1
Chrysene ND mg/kg 10/30/23 12:45 218-01-910/27/23 11:220.45 0.16 1
Dibenz(a,h)anthracene ND mg/kg 10/30/23 12:45 53-70-310/27/23 11:220.45 0.17 1
Dibenzo(a,e)pyrene ND mg/kg 10/30/23 12:45 192-65-410/27/23 11:221.4 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-4 Lab ID:92695355004 Collected:10/24/23 13:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dibenzofuran ND mg/kg 10/30/23 12:45 132-64-910/27/23 11:220.45 0.16 1
1,2-Dichlorobenzene ND mg/kg 10/30/23 12:45 95-50-110/27/23 11:220.45 0.16 1
1,3-Dichlorobenzene ND mg/kg 10/30/23 12:45 541-73-110/27/23 11:220.45 0.16 1
1,4-Dichlorobenzene ND mg/kg 10/30/23 12:45 106-46-710/27/23 11:220.45 0.17 1
3,3'-Dichlorobenzidine ND mg/kg 10/30/23 12:45 91-94-1 L210/27/23 11:220.90 0.30 1
2,4-Dichlorophenol ND mg/kg 10/30/23 12:45 120-83-210/27/23 11:220.45 0.18 1
2,6-Dichlorophenol ND mg/kg 10/30/23 12:45 87-65-0 L210/27/23 11:220.45 0.12 1
2,3-Dichloroaniline ND mg/kg 10/30/23 12:45 608-27-510/27/23 11:220.45 0.22 1
Diethylphthalate ND mg/kg 10/30/23 12:45 84-66-210/27/23 11:220.45 0.17 1
3,3'-Dimethylbenzidine ND mg/kg 10/30/23 12:45 119-93-7 IL10/27/23 11:220.90 0.40 1
2,4-Dimethylphenol ND mg/kg 10/30/23 12:45 105-67-910/27/23 11:220.45 0.19 1
Dimethylphthalate ND mg/kg 10/30/23 12:45 131-11-310/27/23 11:220.45 0.16 1
Di-n-butylphthalate ND mg/kg 10/30/23 12:45 84-74-210/27/23 11:220.45 0.15 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/30/23 12:45 534-52-110/27/23 11:220.90 0.42 1
1,3-Dinitrobenzene ND mg/kg 10/30/23 12:45 99-65-0 L210/27/23 11:220.45 0.10 1
1,4-Dinitrobenzene ND mg/kg 10/30/23 12:45 100-25-4 L210/27/23 11:220.45 0.13 1
2,4-Dinitrophenol ND mg/kg 10/30/23 12:45 51-28-510/27/23 11:222.3 1.4 1
2,4-Dinitrotoluene ND mg/kg 10/30/23 12:45 121-14-210/27/23 11:220.45 0.17 1
2,6-Dinitrotoluene ND mg/kg 10/30/23 12:45 606-20-210/27/23 11:220.45 0.17 1
Di-n-octylphthalate ND mg/kg 10/30/23 12:45 117-84-010/27/23 11:220.45 0.18 1
1,2-Diphenylhydrazine ND mg/kg 10/30/23 12:45 122-66-710/27/23 11:220.45 0.18 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/30/23 12:45 117-81-710/27/23 11:220.45 0.17 1
Fluoranthene ND mg/kg 10/30/23 12:45 206-44-010/27/23 11:220.45 0.15 1
Fluorene ND mg/kg 10/30/23 12:45 86-73-710/27/23 11:220.45 0.16 1
Hexachloro-1,3-butadiene ND mg/kg 10/30/23 12:45 87-68-310/27/23 11:220.45 0.20 1
Hexachlorobenzene ND mg/kg 10/30/23 12:45 118-74-110/27/23 11:220.45 0.18 1
Hexachlorocyclopentadiene ND mg/kg 10/30/23 12:45 77-47-410/27/23 11:220.45 0.26 1
Hexachloroethane ND mg/kg 10/30/23 12:45 67-72-110/27/23 11:220.45 0.17 1
Hexachlorophene ND mg/kg 10/30/23 12:45 70-30-4 IH,v210/27/23 11:224.5 2.6 1
Hexachloropropene ND mg/kg 10/30/23 12:45 1888-71-710/27/23 11:220.45 0.12 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/30/23 12:45 193-39-510/27/23 11:220.45 0.18 1
Isodrin ND mg/kg 10/30/23 12:45 465-73-610/27/23 11:220.45 0.11 1
1-Methylnaphthalene ND mg/kg 10/30/23 12:45 90-12-010/27/23 11:220.45 0.16 1
2-Methylnaphthalene ND mg/kg 10/30/23 12:45 91-57-610/27/23 11:220.45 0.18 1
2-Methyl-5-nitroaniline ND mg/kg 10/30/23 12:45 99-55-810/27/23 11:220.45 0.14 1
2-Methylphenol(o-Cresol)ND mg/kg 10/30/23 12:45 95-48-710/27/23 11:220.45 0.18 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/30/23 12:45 15831-10-410/27/23 11:220.45 0.18 1
1-Naphthalenamine ND mg/kg 10/30/23 12:45 134-32-710/27/23 11:220.90 0.15 1
2-Naphthalenamine ND mg/kg 10/30/23 12:45 91-59-810/27/23 11:220.90 0.17 1
Naphthalene ND mg/kg 10/30/23 12:45 91-20-310/27/23 11:220.45 0.15 1
2-Nitroaniline ND mg/kg 10/30/23 12:45 88-74-410/27/23 11:222.3 0.37 1
3-Nitroaniline ND mg/kg 10/30/23 12:45 99-09-210/27/23 11:222.3 0.35 1
4-Nitroaniline ND mg/kg 10/30/23 12:45 100-01-610/27/23 11:220.90 0.34 1
Nitrobenzene ND mg/kg 10/30/23 12:45 98-95-310/27/23 11:220.45 0.21 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-4 Lab ID:92695355004 Collected:10/24/23 13:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2-Nitrophenol ND mg/kg 10/30/23 12:45 88-75-510/27/23 11:220.45 0.20 1
4-Nitrophenol ND mg/kg 10/30/23 12:45 100-02-710/27/23 11:222.3 0.87 1
N-Nitroso-di-n-propylamine ND mg/kg 10/30/23 12:45 621-64-710/27/23 11:220.45 0.17 1
Pentachlorophenol ND mg/kg 10/30/23 12:45 87-86-510/27/23 11:220.90 0.44 1
Phenanthrene ND mg/kg 10/30/23 12:45 85-01-810/27/23 11:220.45 0.15 1
Phenol ND mg/kg 10/30/23 12:45 108-95-210/27/23 11:220.45 0.20 1
Pyrene ND mg/kg 10/30/23 12:45 129-00-010/27/23 11:220.45 0.18 1
Pyridine ND mg/kg 10/30/23 12:45 110-86-1 v110/27/23 11:220.45 0.14 1
1,2,4,5-Tetrachlorobenzene ND mg/kg 10/30/23 12:45 95-94-310/27/23 11:220.45 0.11 1
2,3,4,6-Tetrachlorophenol ND mg/kg 10/30/23 12:45 58-90-210/27/23 11:220.45 0.11 1
2,4,5-Trichlorophenol ND mg/kg 10/30/23 12:45 95-95-410/27/23 11:220.45 0.21 1
2,4,6-Trichlorophenol ND mg/kg 10/30/23 12:45 88-06-210/27/23 11:220.45 0.19 1
Surrogates
2-Fluorobiphenyl (S)44 %10/30/23 12:45 321-60-810/27/23 11:2210-130 1
Terphenyl-d14 (S)49 %10/30/23 12:45 1718-51-010/27/23 11:2210-130 1
Phenol-d6 (S)41 %10/30/23 12:45 13127-88-310/27/23 11:2210-130 1
2-Fluorophenol (S)44 %10/30/23 12:45 367-12-410/27/23 11:2210-130 1
2,4,6-Tribromophenol (S)36 %10/30/23 12:45 118-79-610/27/23 11:2210-130 1
Nitrobenzene-d5 (S)49 %10/30/23 12:45 4165-60-010/27/23 11:2210-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/27/23 22:39 67-64-110/27/23 14:400.15 0.049 1
Benzene ND mg/kg 10/27/23 22:39 71-43-210/27/23 14:400.0077 0.0030 1
Bromobenzene ND mg/kg 10/27/23 22:39 108-86-110/27/23 14:400.0077 0.0025 1
Bromochloromethane ND mg/kg 10/27/23 22:39 74-97-510/27/23 14:400.0077 0.0023 1
Bromodichloromethane ND mg/kg 10/27/23 22:39 75-27-410/27/23 14:400.0077 0.0030 1
Bromoform ND mg/kg 10/27/23 22:39 75-25-210/27/23 14:400.0077 0.0027 1
Bromomethane ND mg/kg 10/27/23 22:39 74-83-9 IK,v110/27/23 14:400.031 0.024 1
2-Butanone (MEK)ND mg/kg 10/27/23 22:39 78-93-310/27/23 14:400.15 0.037 1
n-Butylbenzene ND mg/kg 10/27/23 22:39 104-51-810/27/23 14:400.0077 0.0048 1
sec-Butylbenzene ND mg/kg 10/27/23 22:39 135-98-810/27/23 14:400.0077 0.0034 1
tert-Butylbenzene ND mg/kg 10/27/23 22:39 98-06-610/27/23 14:400.0077 0.0027 1
Carbon tetrachloride ND mg/kg 10/27/23 22:39 56-23-510/27/23 14:400.0077 0.0029 1
Chlorobenzene ND mg/kg 10/27/23 22:39 108-90-710/27/23 14:400.0077 0.0044 1
Chloroethane ND mg/kg 10/27/23 22:39 75-00-310/27/23 14:400.015 0.0059 1
Chloroform ND mg/kg 10/27/23 22:39 67-66-310/27/23 14:400.0077 0.0064 1
Chloromethane ND mg/kg 10/27/23 22:39 74-87-310/27/23 14:400.015 0.0064 1
2-Chlorotoluene ND mg/kg 10/27/23 22:39 95-49-810/27/23 14:400.0077 0.0027 1
4-Chlorotoluene ND mg/kg 10/27/23 22:39 106-43-410/27/23 14:400.0077 0.0043 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/27/23 22:39 96-12-810/27/23 14:400.0077 0.0030 1
Dibromochloromethane ND mg/kg 10/27/23 22:39 124-48-110/27/23 14:400.0077 0.0043 1
1,2-Dibromoethane (EDB)ND mg/kg 10/27/23 22:39 106-93-410/27/23 14:400.0077 0.0034 1
Dibromomethane ND mg/kg 10/27/23 22:39 74-95-310/27/23 14:400.0077 0.0016 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-4 Lab ID:92695355004 Collected:10/24/23 13:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichlorobenzene ND mg/kg 10/27/23 22:39 95-50-110/27/23 14:400.0077 0.0028 1
1,3-Dichlorobenzene ND mg/kg 10/27/23 22:39 541-73-110/27/23 14:400.0077 0.0024 1
1,4-Dichlorobenzene ND mg/kg 10/27/23 22:39 106-46-710/27/23 14:400.0077 0.0020 1
Dichlorodifluoromethane ND mg/kg 10/27/23 22:39 75-71-810/27/23 14:400.015 0.0078 1
1,1-Dichloroethane ND mg/kg 10/27/23 22:39 75-34-310/27/23 14:400.0077 0.0032 1
1,2-Dichloroethane ND mg/kg 10/27/23 22:39 107-06-210/27/23 14:400.0077 0.0051 1
1,1-Dichloroethene ND mg/kg 10/27/23 22:39 75-35-410/27/23 14:400.0077 0.0032 1
cis-1,2-Dichloroethene ND mg/kg 10/27/23 22:39 156-59-210/27/23 14:400.0077 0.0026 1
trans-1,2-Dichloroethene ND mg/kg 10/27/23 22:39 156-60-510/27/23 14:400.0077 0.0065 1
1,2-Dichloropropane ND mg/kg 10/27/23 22:39 78-87-510/27/23 14:400.0077 0.0023 1
1,3-Dichloropropane ND mg/kg 10/27/23 22:39 142-28-910/27/23 14:400.0077 0.0024 1
2,2-Dichloropropane ND mg/kg 10/27/23 22:39 594-20-710/27/23 14:400.0077 0.0058 1
1,1-Dichloropropene ND mg/kg 10/27/23 22:39 563-58-610/27/23 14:400.0077 0.0037 1
cis-1,3-Dichloropropene ND mg/kg 10/27/23 22:39 10061-01-510/27/23 14:400.0077 0.0021 1
trans-1,3-Dichloropropene ND mg/kg 10/27/23 22:39 10061-02-610/27/23 14:400.0077 0.0026 1
Diisopropyl ether ND mg/kg 10/27/23 22:39 108-20-310/27/23 14:400.0077 0.0021 1
Ethylbenzene 0.0059J mg/kg 10/27/23 22:39 100-41-410/27/23 14:400.0077 0.0036 1
Hexachloro-1,3-butadiene ND mg/kg 10/27/23 22:39 87-68-310/27/23 14:400.015 0.013 1
2-Hexanone ND mg/kg 10/27/23 22:39 591-78-610/27/23 14:400.077 0.0074 1
Isopropylbenzene (Cumene)ND mg/kg 10/27/23 22:39 98-82-810/27/23 14:400.0077 0.0026 1
p-Isopropyltoluene ND mg/kg 10/27/23 22:39 99-87-610/27/23 14:400.0077 0.0038 1
Methylene Chloride ND mg/kg 10/27/23 22:39 75-09-210/27/23 14:400.031 0.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/27/23 22:39 108-10-110/27/23 14:400.077 0.0074 1
Methyl-tert-butyl ether ND mg/kg 10/27/23 22:39 1634-04-410/27/23 14:400.0077 0.0029 1
Naphthalene ND mg/kg 10/27/23 22:39 91-20-310/27/23 14:400.0077 0.0040 1
n-Propylbenzene ND mg/kg 10/27/23 22:39 103-65-110/27/23 14:400.0077 0.0027 1
Styrene ND mg/kg 10/27/23 22:39 100-42-510/27/23 14:400.0077 0.0020 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/27/23 22:39 630-20-610/27/23 14:400.0077 0.0029 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/27/23 22:39 79-34-510/27/23 14:400.0077 0.0020 1
Tetrachloroethene ND mg/kg 10/27/23 22:39 127-18-410/27/23 14:400.0077 0.0024 1
Toluene 0.012 mg/kg 10/27/23 22:39 108-88-310/27/23 14:400.0077 0.0053 1
1,2,3-Trichlorobenzene ND mg/kg 10/27/23 22:39 87-61-610/27/23 14:400.0077 0.0062 1
1,2,4-Trichlorobenzene ND mg/kg 10/27/23 22:39 120-82-110/27/23 14:400.0077 0.0064 1
1,1,1-Trichloroethane ND mg/kg 10/27/23 22:39 71-55-610/27/23 14:400.0077 0.0040 1
1,1,2-Trichloroethane ND mg/kg 10/27/23 22:39 79-00-510/27/23 14:400.0077 0.0025 1
Trichloroethene ND mg/kg 10/27/23 22:39 79-01-610/27/23 14:400.0077 0.0062 1
Trichlorofluoromethane ND mg/kg 10/27/23 22:39 75-69-410/27/23 14:400.0077 0.0042 1
1,2,3-Trichloropropane ND mg/kg 10/27/23 22:39 96-18-410/27/23 14:400.0077 0.0039 1
1,2,4-Trimethylbenzene ND mg/kg 10/27/23 22:39 95-63-610/27/23 14:400.0077 0.0045 1
1,3,5-Trimethylbenzene ND mg/kg 10/27/23 22:39 108-67-810/27/23 14:400.0077 0.0026 1
Vinyl acetate ND mg/kg 10/27/23 22:39 108-05-410/27/23 14:400.077 0.016 1
Vinyl chloride ND mg/kg 10/27/23 22:39 75-01-410/27/23 14:400.015 0.0039 1
Xylene (Total)ND mg/kg 10/27/23 22:39 1330-20-710/27/23 14:400.015 0.0044 1
m&p-Xylene 0.0054J mg/kg 10/27/23 22:39 179601-23-110/27/23 14:400.015 0.0052 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-4 Lab ID:92695355004 Collected:10/24/23 13:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
o-Xylene ND mg/kg 10/27/23 22:39 95-47-610/27/23 14:400.0077 0.0034 1
Surrogates
Toluene-d8 (S)100 %10/27/23 22:39 2037-26-510/27/23 14:4070-130 1
4-Bromofluorobenzene (S)100 %10/27/23 22:39 460-00-410/27/23 14:4070-130 1
1,2-Dichloroethane-d4 (S)104 %10/27/23 22:39 17060-07-010/27/23 14:4070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.2 %10/26/23 17:15 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 71.0 %11/01/23 10:2011/01/23 10:141
Sample:SB-SG-5 Lab ID:92695355005 Collected:10/24/23 13:45 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.50J mg/kg 10/27/23 19:09 18540-29-910/27/23 09:451.3 0.0013 1
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 4.54 mg/kg 11/02/23 12:32 7440-38-211/01/23 07:521.46 0.146 5
Barium 30.5 mg/kg 11/02/23 12:32 7440-39-311/01/23 07:523.66 0.223 5
Cadmium 0.372J mg/kg 11/02/23 12:32 7440-43-9 J11/01/23 07:521.46 0.125 5
Chromium 44.9 mg/kg 11/02/23 12:32 7440-47-311/01/23 07:527.32 0.433 5
Lead 9.80 mg/kg 11/02/23 12:32 7439-92-111/01/23 07:522.93 0.145 5
Selenium 0.723J mg/kg 11/02/23 12:32 7782-49-2 J11/01/23 07:523.66 0.264 5
Silver ND mg/kg 11/02/23 12:32 7440-22-411/01/23 07:520.732 0.127 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0302J mg/kg 11/01/23 18:22 7439-97-6 J10/31/23 22:140.0586 0.0264 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/30/23 13:13 83-32-910/27/23 11:220.44 0.16 1
Acenaphthylene ND mg/kg 10/30/23 13:13 208-96-810/27/23 11:220.44 0.16 1
Acetophenone ND mg/kg 10/30/23 13:13 98-86-210/27/23 11:220.44 0.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-5 Lab ID:92695355005 Collected:10/24/23 13:45 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Aniline ND mg/kg 10/30/23 13:13 62-53-310/27/23 11:220.44 0.17 1
Atrazine ND mg/kg 10/30/23 13:13 1912-24-910/27/23 11:220.44 0.14 1
Benzaldehyde ND mg/kg 10/30/23 13:13 100-52-710/27/23 11:220.44 0.15 1
Benzidine ND mg/kg 10/30/23 13:13 92-87-510/27/23 11:222.2 0.37 1
Benzo(a)anthracene ND mg/kg 10/30/23 13:13 56-55-310/27/23 11:220.44 0.15 1
Benzo(a)pyrene ND mg/kg 10/30/23 13:13 50-32-810/27/23 11:220.44 0.15 1
Benzo(b)fluoranthene ND mg/kg 10/30/23 13:13 205-99-210/27/23 11:220.44 0.15 1
Benzo(g,h,i)perylene ND mg/kg 10/30/23 13:13 191-24-210/27/23 11:220.44 0.17 1
Benzo(k)fluoranthene ND mg/kg 10/30/23 13:13 207-08-910/27/23 11:220.44 0.16 1
Benzoic Acid ND mg/kg 10/30/23 13:13 65-85-010/27/23 11:222.2 0.96 1
Benzophenone ND mg/kg 10/30/23 13:13 119-61-910/27/23 11:220.44 0.20 1
Benzyl alcohol ND mg/kg 10/30/23 13:13 100-51-610/27/23 11:220.89 0.34 1
Biphenyl (Diphenyl)ND mg/kg 10/30/23 13:13 92-52-410/27/23 11:220.44 0.11 1
4-Bromophenylphenyl ether ND mg/kg 10/30/23 13:13 101-55-310/27/23 11:220.44 0.17 1
Butylbenzylphthalate ND mg/kg 10/30/23 13:13 85-68-710/27/23 11:220.44 0.19 1
Caprolactam ND mg/kg 10/30/23 13:13 105-60-210/27/23 11:220.44 0.24 1
Carbazole ND mg/kg 10/30/23 13:13 86-74-810/27/23 11:220.44 0.15 1
4-Chloro-3-methylphenol ND mg/kg 10/30/23 13:13 59-50-710/27/23 11:220.89 0.31 1
4-Chloroaniline ND mg/kg 10/30/23 13:13 106-47-810/27/23 11:220.89 0.35 1
Chlorobenzilate ND mg/kg 10/30/23 13:13 510-15-610/27/23 11:220.44 0.088 1
bis(2-Chloroethoxy)methane ND mg/kg 10/30/23 13:13 111-91-110/27/23 11:220.44 0.18 1
bis(2-Chloroethyl) ether ND mg/kg 10/30/23 13:13 111-44-410/27/23 11:220.44 0.17 1
2-Chloronaphthalene ND mg/kg 10/30/23 13:13 91-58-710/27/23 11:220.44 0.18 1
2-Chlorophenol ND mg/kg 10/30/23 13:13 95-57-810/27/23 11:220.44 0.17 1
4-Chlorophenylphenyl ether ND mg/kg 10/30/23 13:13 7005-72-310/27/23 11:220.44 0.17 1
Chrysene ND mg/kg 10/30/23 13:13 218-01-910/27/23 11:220.44 0.16 1
Dibenz(a,h)anthracene ND mg/kg 10/30/23 13:13 53-70-310/27/23 11:220.44 0.17 1
Dibenzo(a,e)pyrene ND mg/kg 10/30/23 13:13 192-65-410/27/23 11:221.3 0.30 1
Dibenzofuran ND mg/kg 10/30/23 13:13 132-64-910/27/23 11:220.44 0.16 1
1,2-Dichlorobenzene ND mg/kg 10/30/23 13:13 95-50-110/27/23 11:220.44 0.16 1
1,3-Dichlorobenzene ND mg/kg 10/30/23 13:13 541-73-110/27/23 11:220.44 0.16 1
1,4-Dichlorobenzene ND mg/kg 10/30/23 13:13 106-46-710/27/23 11:220.44 0.17 1
3,3'-Dichlorobenzidine ND mg/kg 10/30/23 13:13 91-94-1 L210/27/23 11:220.89 0.30 1
2,4-Dichlorophenol ND mg/kg 10/30/23 13:13 120-83-210/27/23 11:220.44 0.17 1
2,6-Dichlorophenol ND mg/kg 10/30/23 13:13 87-65-0 L210/27/23 11:220.44 0.11 1
2,3-Dichloroaniline ND mg/kg 10/30/23 13:13 608-27-510/27/23 11:220.44 0.22 1
Diethylphthalate ND mg/kg 10/30/23 13:13 84-66-210/27/23 11:220.44 0.16 1
3,3'-Dimethylbenzidine ND mg/kg 10/30/23 13:13 119-93-7 IL10/27/23 11:220.89 0.40 1
2,4-Dimethylphenol ND mg/kg 10/30/23 13:13 105-67-910/27/23 11:220.44 0.18 1
Dimethylphthalate ND mg/kg 10/30/23 13:13 131-11-310/27/23 11:220.44 0.16 1
Di-n-butylphthalate ND mg/kg 10/30/23 13:13 84-74-210/27/23 11:220.44 0.15 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/30/23 13:13 534-52-110/27/23 11:220.89 0.41 1
1,3-Dinitrobenzene ND mg/kg 10/30/23 13:13 99-65-0 L210/27/23 11:220.44 0.10 1
1,4-Dinitrobenzene ND mg/kg 10/30/23 13:13 100-25-4 L210/27/23 11:220.44 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-5 Lab ID:92695355005 Collected:10/24/23 13:45 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 10/30/23 13:13 51-28-510/27/23 11:222.2 1.4 1
2,4-Dinitrotoluene ND mg/kg 10/30/23 13:13 121-14-210/27/23 11:220.44 0.17 1
2,6-Dinitrotoluene ND mg/kg 10/30/23 13:13 606-20-210/27/23 11:220.44 0.16 1
Di-n-octylphthalate ND mg/kg 10/30/23 13:13 117-84-010/27/23 11:220.44 0.18 1
1,2-Diphenylhydrazine ND mg/kg 10/30/23 13:13 122-66-710/27/23 11:220.44 0.18 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/30/23 13:13 117-81-710/27/23 11:220.44 0.17 1
Fluoranthene ND mg/kg 10/30/23 13:13 206-44-010/27/23 11:220.44 0.15 1
Fluorene ND mg/kg 10/30/23 13:13 86-73-710/27/23 11:220.44 0.16 1
Hexachloro-1,3-butadiene ND mg/kg 10/30/23 13:13 87-68-310/27/23 11:220.44 0.19 1
Hexachlorobenzene ND mg/kg 10/30/23 13:13 118-74-110/27/23 11:220.44 0.17 1
Hexachlorocyclopentadiene ND mg/kg 10/30/23 13:13 77-47-410/27/23 11:220.44 0.25 1
Hexachloroethane ND mg/kg 10/30/23 13:13 67-72-110/27/23 11:220.44 0.17 1
Hexachlorophene ND mg/kg 10/30/23 13:13 70-30-4 IH,v210/27/23 11:224.4 2.6 1
Hexachloropropene ND mg/kg 10/30/23 13:13 1888-71-710/27/23 11:220.44 0.12 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/30/23 13:13 193-39-510/27/23 11:220.44 0.18 1
Isodrin ND mg/kg 10/30/23 13:13 465-73-610/27/23 11:220.44 0.11 1
1-Methylnaphthalene ND mg/kg 10/30/23 13:13 90-12-010/27/23 11:220.44 0.16 1
2-Methylnaphthalene ND mg/kg 10/30/23 13:13 91-57-610/27/23 11:220.44 0.18 1
2-Methyl-5-nitroaniline ND mg/kg 10/30/23 13:13 99-55-810/27/23 11:220.44 0.13 1
2-Methylphenol(o-Cresol)ND mg/kg 10/30/23 13:13 95-48-710/27/23 11:220.44 0.18 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/30/23 13:13 15831-10-410/27/23 11:220.44 0.18 1
1-Naphthalenamine ND mg/kg 10/30/23 13:13 134-32-710/27/23 11:220.89 0.15 1
2-Naphthalenamine ND mg/kg 10/30/23 13:13 91-59-810/27/23 11:220.89 0.17 1
Naphthalene ND mg/kg 10/30/23 13:13 91-20-310/27/23 11:220.44 0.15 1
2-Nitroaniline ND mg/kg 10/30/23 13:13 88-74-410/27/23 11:222.2 0.36 1
3-Nitroaniline ND mg/kg 10/30/23 13:13 99-09-210/27/23 11:222.2 0.35 1
4-Nitroaniline ND mg/kg 10/30/23 13:13 100-01-610/27/23 11:220.89 0.34 1
Nitrobenzene ND mg/kg 10/30/23 13:13 98-95-310/27/23 11:220.44 0.21 1
2-Nitrophenol ND mg/kg 10/30/23 13:13 88-75-510/27/23 11:220.44 0.19 1
4-Nitrophenol ND mg/kg 10/30/23 13:13 100-02-710/27/23 11:222.2 0.86 1
N-Nitroso-di-n-propylamine ND mg/kg 10/30/23 13:13 621-64-710/27/23 11:220.44 0.17 1
Pentachlorophenol ND mg/kg 10/30/23 13:13 87-86-510/27/23 11:220.89 0.44 1
Phenanthrene ND mg/kg 10/30/23 13:13 85-01-810/27/23 11:220.44 0.15 1
Phenol ND mg/kg 10/30/23 13:13 108-95-210/27/23 11:220.44 0.20 1
Pyrene ND mg/kg 10/30/23 13:13 129-00-010/27/23 11:220.44 0.18 1
Pyridine ND mg/kg 10/30/23 13:13 110-86-1 v110/27/23 11:220.44 0.14 1
1,2,4,5-Tetrachlorobenzene ND mg/kg 10/30/23 13:13 95-94-310/27/23 11:220.44 0.11 1
2,3,4,6-Tetrachlorophenol ND mg/kg 10/30/23 13:13 58-90-210/27/23 11:220.44 0.11 1
2,4,5-Trichlorophenol ND mg/kg 10/30/23 13:13 95-95-410/27/23 11:220.44 0.20 1
2,4,6-Trichlorophenol ND mg/kg 10/30/23 13:13 88-06-210/27/23 11:220.44 0.18 1
Surrogates
2-Fluorobiphenyl (S)53 %10/30/23 13:13 321-60-810/27/23 11:2210-130 1
Terphenyl-d14 (S)60 %10/30/23 13:13 1718-51-010/27/23 11:2210-130 1
Phenol-d6 (S)53 %10/30/23 13:13 13127-88-310/27/23 11:2210-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-5 Lab ID:92695355005 Collected:10/24/23 13:45 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)50 %10/30/23 13:13 367-12-410/27/23 11:2210-130 1
2,4,6-Tribromophenol (S)46 %10/30/23 13:13 118-79-610/27/23 11:2210-130 1
Nitrobenzene-d5 (S)60 %10/30/23 13:13 4165-60-010/27/23 11:2210-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/27/23 18:40 67-64-110/27/23 12:430.16 0.050 1
Benzene ND mg/kg 10/27/23 18:40 71-43-210/27/23 12:430.0078 0.0031 1
Bromobenzene ND mg/kg 10/27/23 18:40 108-86-110/27/23 12:430.0078 0.0025 1
Bromochloromethane ND mg/kg 10/27/23 18:40 74-97-510/27/23 12:430.0078 0.0023 1
Bromodichloromethane ND mg/kg 10/27/23 18:40 75-27-410/27/23 12:430.0078 0.0030 1
Bromoform ND mg/kg 10/27/23 18:40 75-25-210/27/23 12:430.0078 0.0027 1
Bromomethane ND mg/kg 10/27/23 18:40 74-83-9 IK,v110/27/23 12:430.031 0.024 1
2-Butanone (MEK)ND mg/kg 10/27/23 18:40 78-93-310/27/23 12:430.16 0.037 1
n-Butylbenzene ND mg/kg 10/27/23 18:40 104-51-810/27/23 12:430.0078 0.0049 1
sec-Butylbenzene ND mg/kg 10/27/23 18:40 135-98-810/27/23 12:430.0078 0.0034 1
tert-Butylbenzene ND mg/kg 10/27/23 18:40 98-06-610/27/23 12:430.0078 0.0028 1
Carbon tetrachloride ND mg/kg 10/27/23 18:40 56-23-510/27/23 12:430.0078 0.0029 1
Chlorobenzene ND mg/kg 10/27/23 18:40 108-90-710/27/23 12:430.0078 0.0045 1
Chloroethane ND mg/kg 10/27/23 18:40 75-00-310/27/23 12:430.016 0.0060 1
Chloroform ND mg/kg 10/27/23 18:40 67-66-310/27/23 12:430.0078 0.0065 1
Chloromethane ND mg/kg 10/27/23 18:40 74-87-310/27/23 12:430.016 0.0065 1
2-Chlorotoluene ND mg/kg 10/27/23 18:40 95-49-810/27/23 12:430.0078 0.0027 1
4-Chlorotoluene ND mg/kg 10/27/23 18:40 106-43-410/27/23 12:430.0078 0.0043 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/27/23 18:40 96-12-810/27/23 12:430.0078 0.0030 1
Dibromochloromethane ND mg/kg 10/27/23 18:40 124-48-110/27/23 12:430.0078 0.0044 1
1,2-Dibromoethane (EDB)ND mg/kg 10/27/23 18:40 106-93-410/27/23 12:430.0078 0.0034 1
Dibromomethane ND mg/kg 10/27/23 18:40 74-95-310/27/23 12:430.0078 0.0017 1
1,2-Dichlorobenzene ND mg/kg 10/27/23 18:40 95-50-110/27/23 12:430.0078 0.0028 1
1,3-Dichlorobenzene ND mg/kg 10/27/23 18:40 541-73-110/27/23 12:430.0078 0.0024 1
1,4-Dichlorobenzene ND mg/kg 10/27/23 18:40 106-46-710/27/23 12:430.0078 0.0020 1
Dichlorodifluoromethane ND mg/kg 10/27/23 18:40 75-71-810/27/23 12:430.016 0.0079 1
1,1-Dichloroethane ND mg/kg 10/27/23 18:40 75-34-310/27/23 12:430.0078 0.0032 1
1,2-Dichloroethane ND mg/kg 10/27/23 18:40 107-06-210/27/23 12:430.0078 0.0051 1
1,1-Dichloroethene ND mg/kg 10/27/23 18:40 75-35-410/27/23 12:430.0078 0.0032 1
cis-1,2-Dichloroethene ND mg/kg 10/27/23 18:40 156-59-210/27/23 12:430.0078 0.0027 1
trans-1,2-Dichloroethene ND mg/kg 10/27/23 18:40 156-60-510/27/23 12:430.0078 0.0066 1
1,2-Dichloropropane ND mg/kg 10/27/23 18:40 78-87-510/27/23 12:430.0078 0.0023 1
1,3-Dichloropropane ND mg/kg 10/27/23 18:40 142-28-910/27/23 12:430.0078 0.0024 1
2,2-Dichloropropane ND mg/kg 10/27/23 18:40 594-20-710/27/23 12:430.0078 0.0059 1
1,1-Dichloropropene ND mg/kg 10/27/23 18:40 563-58-610/27/23 12:430.0078 0.0037 1
cis-1,3-Dichloropropene ND mg/kg 10/27/23 18:40 10061-01-510/27/23 12:430.0078 0.0021 1
trans-1,3-Dichloropropene ND mg/kg 10/27/23 18:40 10061-02-610/27/23 12:430.0078 0.0027 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-5 Lab ID:92695355005 Collected:10/24/23 13:45 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Diisopropyl ether ND mg/kg 10/27/23 18:40 108-20-310/27/23 12:430.0078 0.0021 1
Ethylbenzene 0.0066J mg/kg 10/27/23 18:40 100-41-410/27/23 12:430.0078 0.0036 1
Hexachloro-1,3-butadiene ND mg/kg 10/27/23 18:40 87-68-310/27/23 12:430.016 0.013 1
2-Hexanone ND mg/kg 10/27/23 18:40 591-78-610/27/23 12:430.078 0.0075 1
Isopropylbenzene (Cumene)ND mg/kg 10/27/23 18:40 98-82-810/27/23 12:430.0078 0.0026 1
p-Isopropyltoluene ND mg/kg 10/27/23 18:40 99-87-610/27/23 12:430.0078 0.0038 1
Methylene Chloride ND mg/kg 10/27/23 18:40 75-09-210/27/23 12:430.031 0.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/27/23 18:40 108-10-110/27/23 12:430.078 0.0075 1
Methyl-tert-butyl ether ND mg/kg 10/27/23 18:40 1634-04-410/27/23 12:430.0078 0.0029 1
Naphthalene ND mg/kg 10/27/23 18:40 91-20-310/27/23 12:430.0078 0.0041 1
n-Propylbenzene ND mg/kg 10/27/23 18:40 103-65-110/27/23 12:430.0078 0.0028 1
Styrene ND mg/kg 10/27/23 18:40 100-42-510/27/23 12:430.0078 0.0020 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/27/23 18:40 630-20-610/27/23 12:430.0078 0.0030 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/27/23 18:40 79-34-510/27/23 12:430.0078 0.0020 1
Tetrachloroethene ND mg/kg 10/27/23 18:40 127-18-410/27/23 12:430.0078 0.0025 1
Toluene 0.0091 mg/kg 10/27/23 18:40 108-88-310/27/23 12:430.0078 0.0054 1
1,2,3-Trichlorobenzene ND mg/kg 10/27/23 18:40 87-61-610/27/23 12:430.0078 0.0063 1
1,2,4-Trichlorobenzene ND mg/kg 10/27/23 18:40 120-82-110/27/23 12:430.0078 0.0065 1
1,1,1-Trichloroethane ND mg/kg 10/27/23 18:40 71-55-610/27/23 12:430.0078 0.0040 1
1,1,2-Trichloroethane ND mg/kg 10/27/23 18:40 79-00-510/27/23 12:430.0078 0.0026 1
Trichloroethene ND mg/kg 10/27/23 18:40 79-01-610/27/23 12:430.0078 0.0063 1
Trichlorofluoromethane ND mg/kg 10/27/23 18:40 75-69-410/27/23 12:430.0078 0.0043 1
1,2,3-Trichloropropane ND mg/kg 10/27/23 18:40 96-18-410/27/23 12:430.0078 0.0039 1
1,2,4-Trimethylbenzene ND mg/kg 10/27/23 18:40 95-63-610/27/23 12:430.0078 0.0046 1
1,3,5-Trimethylbenzene ND mg/kg 10/27/23 18:40 108-67-810/27/23 12:430.0078 0.0026 1
Vinyl acetate ND mg/kg 10/27/23 18:40 108-05-410/27/23 12:430.078 0.016 1
Vinyl chloride ND mg/kg 10/27/23 18:40 75-01-410/27/23 12:430.016 0.0039 1
Xylene (Total)ND mg/kg 10/27/23 18:40 1330-20-710/27/23 12:430.016 0.0044 1
m&p-Xylene 0.0070J mg/kg 10/27/23 18:40 179601-23-110/27/23 12:430.016 0.0053 1
o-Xylene ND mg/kg 10/27/23 18:40 95-47-610/27/23 12:430.0078 0.0034 1
Surrogates
Toluene-d8 (S)100 %10/27/23 18:40 2037-26-510/27/23 12:4370-130 1
4-Bromofluorobenzene (S)101 %10/27/23 18:40 460-00-410/27/23 12:4370-130 1
1,2-Dichloroethane-d4 (S)100 %10/27/23 18:40 17060-07-010/27/23 12:4370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.8 %10/26/23 17:16 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 68.3 %11/01/23 10:2011/01/23 10:141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-6 Lab ID:92695355006 Collected:10/24/23 14:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.75J mg/kg 10/27/23 19:27 18540-29-910/27/23 09:451.4 0.0014 1
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 1.10J mg/kg 11/02/23 12:35 7440-38-2 J11/01/23 07:521.36 0.136 5
Barium 17.1 mg/kg 11/02/23 12:35 7440-39-311/01/23 07:523.39 0.206 5
Cadmium ND mg/kg 11/02/23 12:35 7440-43-911/01/23 07:521.36 0.116 5
Chromium 24.8 mg/kg 11/02/23 12:35 7440-47-311/01/23 07:526.78 0.401 5
Lead 3.28 mg/kg 11/02/23 12:35 7439-92-111/01/23 07:522.71 0.134 5
Selenium 0.285J mg/kg 11/02/23 12:35 7782-49-2 J11/01/23 07:523.39 0.244 5
Silver ND mg/kg 11/02/23 12:35 7440-22-411/01/23 07:520.678 0.117 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 11/01/23 18:25 7439-97-610/31/23 22:140.0543 0.0244 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/30/23 13:41 83-32-910/27/23 11:220.43 0.15 1
Acenaphthylene ND mg/kg 10/30/23 13:41 208-96-810/27/23 11:220.43 0.15 1
Acetophenone ND mg/kg 10/30/23 13:41 98-86-210/27/23 11:220.43 0.11 1
Aniline ND mg/kg 10/30/23 13:41 62-53-310/27/23 11:220.43 0.17 1
Atrazine ND mg/kg 10/30/23 13:41 1912-24-910/27/23 11:220.43 0.14 1
Benzaldehyde ND mg/kg 10/30/23 13:41 100-52-710/27/23 11:220.43 0.14 1
Benzidine ND mg/kg 10/30/23 13:41 92-87-510/27/23 11:222.2 0.35 1
Benzo(a)anthracene ND mg/kg 10/30/23 13:41 56-55-310/27/23 11:220.43 0.14 1
Benzo(a)pyrene ND mg/kg 10/30/23 13:41 50-32-810/27/23 11:220.43 0.15 1
Benzo(b)fluoranthene ND mg/kg 10/30/23 13:41 205-99-210/27/23 11:220.43 0.14 1
Benzo(g,h,i)perylene ND mg/kg 10/30/23 13:41 191-24-210/27/23 11:220.43 0.17 1
Benzo(k)fluoranthene ND mg/kg 10/30/23 13:41 207-08-910/27/23 11:220.43 0.15 1
Benzoic Acid ND mg/kg 10/30/23 13:41 65-85-010/27/23 11:222.2 0.93 1
Benzophenone ND mg/kg 10/30/23 13:41 119-61-910/27/23 11:220.43 0.20 1
Benzyl alcohol ND mg/kg 10/30/23 13:41 100-51-610/27/23 11:220.86 0.33 1
Biphenyl (Diphenyl)ND mg/kg 10/30/23 13:41 92-52-410/27/23 11:220.43 0.10 1
4-Bromophenylphenyl ether ND mg/kg 10/30/23 13:41 101-55-310/27/23 11:220.43 0.17 1
Butylbenzylphthalate ND mg/kg 10/30/23 13:41 85-68-710/27/23 11:220.43 0.18 1
Caprolactam ND mg/kg 10/30/23 13:41 105-60-210/27/23 11:220.43 0.23 1
Carbazole ND mg/kg 10/30/23 13:41 86-74-810/27/23 11:220.43 0.15 1
4-Chloro-3-methylphenol ND mg/kg 10/30/23 13:41 59-50-710/27/23 11:220.86 0.30 1
4-Chloroaniline ND mg/kg 10/30/23 13:41 106-47-810/27/23 11:220.86 0.34 1
Chlorobenzilate ND mg/kg 10/30/23 13:41 510-15-610/27/23 11:220.43 0.085 1
bis(2-Chloroethoxy)methane ND mg/kg 10/30/23 13:41 111-91-110/27/23 11:220.43 0.18 1
bis(2-Chloroethyl) ether ND mg/kg 10/30/23 13:41 111-44-410/27/23 11:220.43 0.16 1
2-Chloronaphthalene ND mg/kg 10/30/23 13:41 91-58-710/27/23 11:220.43 0.17 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-6 Lab ID:92695355006 Collected:10/24/23 14:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2-Chlorophenol ND mg/kg 10/30/23 13:41 95-57-810/27/23 11:220.43 0.16 1
4-Chlorophenylphenyl ether ND mg/kg 10/30/23 13:41 7005-72-310/27/23 11:220.43 0.16 1
Chrysene ND mg/kg 10/30/23 13:41 218-01-910/27/23 11:220.43 0.16 1
Dibenz(a,h)anthracene ND mg/kg 10/30/23 13:41 53-70-310/27/23 11:220.43 0.17 1
Dibenzo(a,e)pyrene ND mg/kg 10/30/23 13:41 192-65-410/27/23 11:221.3 0.29 1
Dibenzofuran ND mg/kg 10/30/23 13:41 132-64-910/27/23 11:220.43 0.16 1
1,2-Dichlorobenzene ND mg/kg 10/30/23 13:41 95-50-110/27/23 11:220.43 0.16 1
1,3-Dichlorobenzene ND mg/kg 10/30/23 13:41 541-73-110/27/23 11:220.43 0.15 1
1,4-Dichlorobenzene ND mg/kg 10/30/23 13:41 106-46-710/27/23 11:220.43 0.16 1
3,3'-Dichlorobenzidine ND mg/kg 10/30/23 13:41 91-94-1 L210/27/23 11:220.86 0.29 1
2,4-Dichlorophenol ND mg/kg 10/30/23 13:41 120-83-210/27/23 11:220.43 0.17 1
2,6-Dichlorophenol ND mg/kg 10/30/23 13:41 87-65-0 L210/27/23 11:220.43 0.11 1
2,3-Dichloroaniline ND mg/kg 10/30/23 13:41 608-27-510/27/23 11:220.43 0.21 1
Diethylphthalate ND mg/kg 10/30/23 13:41 84-66-210/27/23 11:220.43 0.16 1
3,3'-Dimethylbenzidine ND mg/kg 10/30/23 13:41 119-93-7 IL10/27/23 11:220.86 0.38 1
2,4-Dimethylphenol ND mg/kg 10/30/23 13:41 105-67-910/27/23 11:220.43 0.18 1
Dimethylphthalate ND mg/kg 10/30/23 13:41 131-11-310/27/23 11:220.43 0.16 1
Di-n-butylphthalate ND mg/kg 10/30/23 13:41 84-74-210/27/23 11:220.43 0.14 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/30/23 13:41 534-52-110/27/23 11:220.86 0.40 1
1,3-Dinitrobenzene ND mg/kg 10/30/23 13:41 99-65-0 L210/27/23 11:220.43 0.097 1
1,4-Dinitrobenzene ND mg/kg 10/30/23 13:41 100-25-4 L210/27/23 11:220.43 0.13 1
2,4-Dinitrophenol ND mg/kg 10/30/23 13:41 51-28-510/27/23 11:222.2 1.3 1
2,4-Dinitrotoluene ND mg/kg 10/30/23 13:41 121-14-210/27/23 11:220.43 0.17 1
2,6-Dinitrotoluene ND mg/kg 10/30/23 13:41 606-20-210/27/23 11:220.43 0.16 1
Di-n-octylphthalate ND mg/kg 10/30/23 13:41 117-84-010/27/23 11:220.43 0.17 1
1,2-Diphenylhydrazine ND mg/kg 10/30/23 13:41 122-66-710/27/23 11:220.43 0.17 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/30/23 13:41 117-81-710/27/23 11:220.43 0.17 1
Fluoranthene ND mg/kg 10/30/23 13:41 206-44-010/27/23 11:220.43 0.15 1
Fluorene ND mg/kg 10/30/23 13:41 86-73-710/27/23 11:220.43 0.15 1
Hexachloro-1,3-butadiene ND mg/kg 10/30/23 13:41 87-68-310/27/23 11:220.43 0.19 1
Hexachlorobenzene ND mg/kg 10/30/23 13:41 118-74-110/27/23 11:220.43 0.17 1
Hexachlorocyclopentadiene ND mg/kg 10/30/23 13:41 77-47-410/27/23 11:220.43 0.25 1
Hexachloroethane ND mg/kg 10/30/23 13:41 67-72-110/27/23 11:220.43 0.16 1
Hexachlorophene ND mg/kg 10/30/23 13:41 70-30-4 IH,v210/27/23 11:224.3 2.5 1
Hexachloropropene ND mg/kg 10/30/23 13:41 1888-71-710/27/23 11:220.43 0.12 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/30/23 13:41 193-39-510/27/23 11:220.43 0.17 1
Isodrin ND mg/kg 10/30/23 13:41 465-73-610/27/23 11:220.43 0.10 1
1-Methylnaphthalene ND mg/kg 10/30/23 13:41 90-12-010/27/23 11:220.43 0.15 1
2-Methylnaphthalene ND mg/kg 10/30/23 13:41 91-57-610/27/23 11:220.43 0.17 1
2-Methyl-5-nitroaniline ND mg/kg 10/30/23 13:41 99-55-810/27/23 11:220.43 0.13 1
2-Methylphenol(o-Cresol)ND mg/kg 10/30/23 13:41 95-48-710/27/23 11:220.43 0.18 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/30/23 13:41 15831-10-410/27/23 11:220.43 0.17 1
1-Naphthalenamine ND mg/kg 10/30/23 13:41 134-32-710/27/23 11:220.86 0.14 1
2-Naphthalenamine ND mg/kg 10/30/23 13:41 91-59-810/27/23 11:220.86 0.17 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-6 Lab ID:92695355006 Collected:10/24/23 14:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Naphthalene ND mg/kg 10/30/23 13:41 91-20-310/27/23 11:220.43 0.15 1
2-Nitroaniline ND mg/kg 10/30/23 13:41 88-74-410/27/23 11:222.2 0.35 1
3-Nitroaniline ND mg/kg 10/30/23 13:41 99-09-210/27/23 11:222.2 0.34 1
4-Nitroaniline ND mg/kg 10/30/23 13:41 100-01-610/27/23 11:220.86 0.33 1
Nitrobenzene ND mg/kg 10/30/23 13:41 98-95-310/27/23 11:220.43 0.20 1
2-Nitrophenol ND mg/kg 10/30/23 13:41 88-75-510/27/23 11:220.43 0.19 1
4-Nitrophenol ND mg/kg 10/30/23 13:41 100-02-710/27/23 11:222.2 0.83 1
N-Nitroso-di-n-propylamine ND mg/kg 10/30/23 13:41 621-64-710/27/23 11:220.43 0.16 1
Pentachlorophenol ND mg/kg 10/30/23 13:41 87-86-510/27/23 11:220.86 0.42 1
Phenanthrene ND mg/kg 10/30/23 13:41 85-01-810/27/23 11:220.43 0.14 1
Phenol ND mg/kg 10/30/23 13:41 108-95-210/27/23 11:220.43 0.19 1
Pyrene ND mg/kg 10/30/23 13:41 129-00-010/27/23 11:220.43 0.17 1
Pyridine ND mg/kg 10/30/23 13:41 110-86-1 v110/27/23 11:220.43 0.14 1
1,2,4,5-Tetrachlorobenzene ND mg/kg 10/30/23 13:41 95-94-310/27/23 11:220.43 0.10 1
2,3,4,6-Tetrachlorophenol ND mg/kg 10/30/23 13:41 58-90-210/27/23 11:220.43 0.11 1
2,4,5-Trichlorophenol ND mg/kg 10/30/23 13:41 95-95-410/27/23 11:220.43 0.20 1
2,4,6-Trichlorophenol ND mg/kg 10/30/23 13:41 88-06-210/27/23 11:220.43 0.18 1
Surrogates
2-Fluorobiphenyl (S)49 %10/30/23 13:41 321-60-810/27/23 11:2210-130 1
Terphenyl-d14 (S)50 %10/30/23 13:41 1718-51-010/27/23 11:2210-130 1
Phenol-d6 (S)50 %10/30/23 13:41 13127-88-310/27/23 11:2210-130 1
2-Fluorophenol (S)52 %10/30/23 13:41 367-12-410/27/23 11:2210-130 1
2,4,6-Tribromophenol (S)45 %10/30/23 13:41 118-79-610/27/23 11:2210-130 1
Nitrobenzene-d5 (S)55 %10/30/23 13:41 4165-60-010/27/23 11:2210-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/27/23 18:58 67-64-110/27/23 12:430.15 0.047 1
Benzene ND mg/kg 10/27/23 18:58 71-43-210/27/23 12:430.0073 0.0029 1
Bromobenzene ND mg/kg 10/27/23 18:58 108-86-110/27/23 12:430.0073 0.0024 1
Bromochloromethane ND mg/kg 10/27/23 18:58 74-97-510/27/23 12:430.0073 0.0021 1
Bromodichloromethane ND mg/kg 10/27/23 18:58 75-27-410/27/23 12:430.0073 0.0028 1
Bromoform ND mg/kg 10/27/23 18:58 75-25-210/27/23 12:430.0073 0.0026 1
Bromomethane ND mg/kg 10/27/23 18:58 74-83-9 IK,v110/27/23 12:430.029 0.022 1
2-Butanone (MEK)ND mg/kg 10/27/23 18:58 78-93-310/27/23 12:430.15 0.035 1
n-Butylbenzene ND mg/kg 10/27/23 18:58 104-51-810/27/23 12:430.0073 0.0046 1
sec-Butylbenzene ND mg/kg 10/27/23 18:58 135-98-810/27/23 12:430.0073 0.0032 1
tert-Butylbenzene ND mg/kg 10/27/23 18:58 98-06-610/27/23 12:430.0073 0.0026 1
Carbon tetrachloride ND mg/kg 10/27/23 18:58 56-23-510/27/23 12:430.0073 0.0027 1
Chlorobenzene ND mg/kg 10/27/23 18:58 108-90-710/27/23 12:430.0073 0.0042 1
Chloroethane ND mg/kg 10/27/23 18:58 75-00-310/27/23 12:430.015 0.0056 1
Chloroform ND mg/kg 10/27/23 18:58 67-66-310/27/23 12:430.0073 0.0061 1
Chloromethane ND mg/kg 10/27/23 18:58 74-87-310/27/23 12:430.015 0.0061 1
2-Chlorotoluene ND mg/kg 10/27/23 18:58 95-49-810/27/23 12:430.0073 0.0026 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-6 Lab ID:92695355006 Collected:10/24/23 14:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Chlorotoluene ND mg/kg 10/27/23 18:58 106-43-410/27/23 12:430.0073 0.0040 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/27/23 18:58 96-12-810/27/23 12:430.0073 0.0028 1
Dibromochloromethane ND mg/kg 10/27/23 18:58 124-48-110/27/23 12:430.0073 0.0041 1
1,2-Dibromoethane (EDB)ND mg/kg 10/27/23 18:58 106-93-410/27/23 12:430.0073 0.0032 1
Dibromomethane ND mg/kg 10/27/23 18:58 74-95-310/27/23 12:430.0073 0.0016 1
1,2-Dichlorobenzene ND mg/kg 10/27/23 18:58 95-50-110/27/23 12:430.0073 0.0026 1
1,3-Dichlorobenzene ND mg/kg 10/27/23 18:58 541-73-110/27/23 12:430.0073 0.0022 1
1,4-Dichlorobenzene ND mg/kg 10/27/23 18:58 106-46-710/27/23 12:430.0073 0.0019 1
Dichlorodifluoromethane ND mg/kg 10/27/23 18:58 75-71-810/27/23 12:430.015 0.0074 1
1,1-Dichloroethane ND mg/kg 10/27/23 18:58 75-34-310/27/23 12:430.0073 0.0030 1
1,2-Dichloroethane ND mg/kg 10/27/23 18:58 107-06-210/27/23 12:430.0073 0.0048 1
1,1-Dichloroethene ND mg/kg 10/27/23 18:58 75-35-410/27/23 12:430.0073 0.0030 1
cis-1,2-Dichloroethene ND mg/kg 10/27/23 18:58 156-59-210/27/23 12:430.0073 0.0025 1
trans-1,2-Dichloroethene ND mg/kg 10/27/23 18:58 156-60-510/27/23 12:430.0073 0.0062 1
1,2-Dichloropropane ND mg/kg 10/27/23 18:58 78-87-510/27/23 12:430.0073 0.0022 1
1,3-Dichloropropane ND mg/kg 10/27/23 18:58 142-28-910/27/23 12:430.0073 0.0023 1
2,2-Dichloropropane ND mg/kg 10/27/23 18:58 594-20-710/27/23 12:430.0073 0.0055 1
1,1-Dichloropropene ND mg/kg 10/27/23 18:58 563-58-610/27/23 12:430.0073 0.0035 1
cis-1,3-Dichloropropene ND mg/kg 10/27/23 18:58 10061-01-510/27/23 12:430.0073 0.0020 1
trans-1,3-Dichloropropene ND mg/kg 10/27/23 18:58 10061-02-610/27/23 12:430.0073 0.0025 1
Diisopropyl ether ND mg/kg 10/27/23 18:58 108-20-310/27/23 12:430.0073 0.0020 1
Ethylbenzene 0.0054J mg/kg 10/27/23 18:58 100-41-410/27/23 12:430.0073 0.0034 1
Hexachloro-1,3-butadiene ND mg/kg 10/27/23 18:58 87-68-310/27/23 12:430.015 0.012 1
2-Hexanone ND mg/kg 10/27/23 18:58 591-78-610/27/23 12:430.073 0.0070 1
Isopropylbenzene (Cumene)ND mg/kg 10/27/23 18:58 98-82-810/27/23 12:430.0073 0.0025 1
p-Isopropyltoluene ND mg/kg 10/27/23 18:58 99-87-610/27/23 12:430.0073 0.0036 1
Methylene Chloride ND mg/kg 10/27/23 18:58 75-09-210/27/23 12:430.029 0.020 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/27/23 18:58 108-10-110/27/23 12:430.073 0.0070 1
Methyl-tert-butyl ether ND mg/kg 10/27/23 18:58 1634-04-410/27/23 12:430.0073 0.0027 1
Naphthalene ND mg/kg 10/27/23 18:58 91-20-310/27/23 12:430.0073 0.0038 1
n-Propylbenzene ND mg/kg 10/27/23 18:58 103-65-110/27/23 12:430.0073 0.0026 1
Styrene ND mg/kg 10/27/23 18:58 100-42-510/27/23 12:430.0073 0.0019 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/27/23 18:58 630-20-610/27/23 12:430.0073 0.0028 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/27/23 18:58 79-34-510/27/23 12:430.0073 0.0019 1
Tetrachloroethene ND mg/kg 10/27/23 18:58 127-18-410/27/23 12:430.0073 0.0023 1
Toluene ND mg/kg 10/27/23 18:58 108-88-310/27/23 12:430.0073 0.0050 1
1,2,3-Trichlorobenzene ND mg/kg 10/27/23 18:58 87-61-610/27/23 12:430.0073 0.0059 1
1,2,4-Trichlorobenzene ND mg/kg 10/27/23 18:58 120-82-110/27/23 12:430.0073 0.0061 1
1,1,1-Trichloroethane ND mg/kg 10/27/23 18:58 71-55-610/27/23 12:430.0073 0.0038 1
1,1,2-Trichloroethane ND mg/kg 10/27/23 18:58 79-00-510/27/23 12:430.0073 0.0024 1
Trichloroethene ND mg/kg 10/27/23 18:58 79-01-610/27/23 12:430.0073 0.0058 1
Trichlorofluoromethane ND mg/kg 10/27/23 18:58 75-69-410/27/23 12:430.0073 0.0040 1
1,2,3-Trichloropropane ND mg/kg 10/27/23 18:58 96-18-410/27/23 12:430.0073 0.0037 1
1,2,4-Trimethylbenzene ND mg/kg 10/27/23 18:58 95-63-610/27/23 12:430.0073 0.0043 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-SG-6 Lab ID:92695355006 Collected:10/24/23 14:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3,5-Trimethylbenzene ND mg/kg 10/27/23 18:58 108-67-810/27/23 12:430.0073 0.0024 1
Vinyl acetate ND mg/kg 10/27/23 18:58 108-05-410/27/23 12:430.073 0.015 1
Vinyl chloride ND mg/kg 10/27/23 18:58 75-01-410/27/23 12:430.015 0.0037 1
Xylene (Total)ND mg/kg 10/27/23 18:58 1330-20-710/27/23 12:430.015 0.0041 1
m&p-Xylene ND mg/kg 10/27/23 18:58 179601-23-110/27/23 12:430.015 0.0050 1
o-Xylene ND mg/kg 10/27/23 18:58 95-47-610/27/23 12:430.0073 0.0032 1
Surrogates
Toluene-d8 (S)100 %10/27/23 18:58 2037-26-510/27/23 12:4370-130 1
4-Bromofluorobenzene (S)101 %10/27/23 18:58 460-00-410/27/23 12:4370-130 1
1,2-Dichloroethane-d4 (S)103 %10/27/23 18:58 17060-07-010/27/23 12:4370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.6 %10/26/23 18:54 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 73.7 %11/01/23 10:2011/01/23 10:141
Sample:SB-11 Lab ID:92695355007 Collected:10/24/23 14:10 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.58J mg/kg 10/27/23 21:31 18540-29-910/27/23 09:451.2 0.0012 1
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.61 mg/kg 11/02/23 12:39 7440-38-211/01/23 07:521.25 0.125 5
Barium 11.4 mg/kg 11/02/23 12:39 7440-39-311/01/23 07:523.13 0.190 5
Cadmium ND mg/kg 11/02/23 12:39 7440-43-911/01/23 07:521.25 0.107 5
Chromium 30.0 mg/kg 11/02/23 12:39 7440-47-311/01/23 07:526.26 0.370 5
Lead 4.96 mg/kg 11/02/23 12:39 7439-92-111/01/23 07:522.50 0.124 5
Selenium 0.972J mg/kg 11/02/23 12:39 7782-49-2 J11/01/23 07:523.13 0.225 5
Silver ND mg/kg 11/02/23 12:39 7440-22-411/01/23 07:520.626 0.108 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0664 mg/kg 11/01/23 18:27 7439-97-610/31/23 22:140.0500 0.0225 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-11 Lab ID:92695355007 Collected:10/24/23 14:10 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/30/23 14:10 83-32-910/27/23 11:220.40 0.14 1
Acenaphthylene ND mg/kg 10/30/23 14:10 208-96-810/27/23 11:220.40 0.14 1
Acetophenone ND mg/kg 10/30/23 14:10 98-86-210/27/23 11:220.40 0.10 1
Aniline ND mg/kg 10/30/23 14:10 62-53-310/27/23 11:220.40 0.16 1
Atrazine ND mg/kg 10/30/23 14:10 1912-24-910/27/23 11:220.40 0.13 1
Benzaldehyde ND mg/kg 10/30/23 14:10 100-52-710/27/23 11:220.40 0.13 1
Benzidine ND mg/kg 10/30/23 14:10 92-87-510/27/23 11:222.0 0.33 1
Benzo(a)anthracene ND mg/kg 10/30/23 14:10 56-55-310/27/23 11:220.40 0.13 1
Benzo(a)pyrene ND mg/kg 10/30/23 14:10 50-32-810/27/23 11:220.40 0.14 1
Benzo(b)fluoranthene ND mg/kg 10/30/23 14:10 205-99-210/27/23 11:220.40 0.13 1
Benzo(g,h,i)perylene ND mg/kg 10/30/23 14:10 191-24-210/27/23 11:220.40 0.16 1
Benzo(k)fluoranthene ND mg/kg 10/30/23 14:10 207-08-910/27/23 11:220.40 0.14 1
Benzoic Acid ND mg/kg 10/30/23 14:10 65-85-010/27/23 11:222.0 0.86 1
Benzophenone ND mg/kg 10/30/23 14:10 119-61-910/27/23 11:220.40 0.18 1
Benzyl alcohol ND mg/kg 10/30/23 14:10 100-51-610/27/23 11:220.80 0.30 1
Biphenyl (Diphenyl)ND mg/kg 10/30/23 14:10 92-52-410/27/23 11:220.40 0.095 1
4-Bromophenylphenyl ether ND mg/kg 10/30/23 14:10 101-55-310/27/23 11:220.40 0.15 1
Butylbenzylphthalate ND mg/kg 10/30/23 14:10 85-68-710/27/23 11:220.40 0.17 1
Caprolactam ND mg/kg 10/30/23 14:10 105-60-210/27/23 11:220.40 0.21 1
Carbazole ND mg/kg 10/30/23 14:10 86-74-810/27/23 11:220.40 0.14 1
4-Chloro-3-methylphenol ND mg/kg 10/30/23 14:10 59-50-710/27/23 11:220.80 0.28 1
4-Chloroaniline ND mg/kg 10/30/23 14:10 106-47-810/27/23 11:220.80 0.31 1
Chlorobenzilate ND mg/kg 10/30/23 14:10 510-15-610/27/23 11:220.40 0.079 1
bis(2-Chloroethoxy)methane ND mg/kg 10/30/23 14:10 111-91-110/27/23 11:220.40 0.17 1
bis(2-Chloroethyl) ether ND mg/kg 10/30/23 14:10 111-44-410/27/23 11:220.40 0.15 1
2-Chloronaphthalene ND mg/kg 10/30/23 14:10 91-58-710/27/23 11:220.40 0.16 1
2-Chlorophenol ND mg/kg 10/30/23 14:10 95-57-810/27/23 11:220.40 0.15 1
4-Chlorophenylphenyl ether ND mg/kg 10/30/23 14:10 7005-72-310/27/23 11:220.40 0.15 1
Chrysene ND mg/kg 10/30/23 14:10 218-01-910/27/23 11:220.40 0.15 1
Dibenz(a,h)anthracene ND mg/kg 10/30/23 14:10 53-70-310/27/23 11:220.40 0.15 1
Dibenzo(a,e)pyrene ND mg/kg 10/30/23 14:10 192-65-410/27/23 11:221.2 0.27 1
Dibenzofuran ND mg/kg 10/30/23 14:10 132-64-910/27/23 11:220.40 0.14 1
1,2-Dichlorobenzene ND mg/kg 10/30/23 14:10 95-50-110/27/23 11:220.40 0.14 1
1,3-Dichlorobenzene ND mg/kg 10/30/23 14:10 541-73-110/27/23 11:220.40 0.14 1
1,4-Dichlorobenzene ND mg/kg 10/30/23 14:10 106-46-710/27/23 11:220.40 0.15 1
3,3'-Dichlorobenzidine ND mg/kg 10/30/23 14:10 91-94-1 L210/27/23 11:220.80 0.27 1
2,4-Dichlorophenol ND mg/kg 10/30/23 14:10 120-83-210/27/23 11:220.40 0.16 1
2,6-Dichlorophenol ND mg/kg 10/30/23 14:10 87-65-0 L210/27/23 11:220.40 0.10 1
2,3-Dichloroaniline ND mg/kg 10/30/23 14:10 608-27-510/27/23 11:220.40 0.19 1
Diethylphthalate ND mg/kg 10/30/23 14:10 84-66-210/27/23 11:220.40 0.15 1
3,3'-Dimethylbenzidine ND mg/kg 10/30/23 14:10 119-93-7 IL10/27/23 11:220.80 0.36 1
2,4-Dimethylphenol ND mg/kg 10/30/23 14:10 105-67-910/27/23 11:220.40 0.17 1
Dimethylphthalate ND mg/kg 10/30/23 14:10 131-11-310/27/23 11:220.40 0.15 1
Di-n-butylphthalate ND mg/kg 10/30/23 14:10 84-74-210/27/23 11:220.40 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-11 Lab ID:92695355007 Collected:10/24/23 14:10 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
4,6-Dinitro-2-methylphenol ND mg/kg 10/30/23 14:10 534-52-110/27/23 11:220.80 0.37 1
1,3-Dinitrobenzene ND mg/kg 10/30/23 14:10 99-65-0 L210/27/23 11:220.40 0.090 1
1,4-Dinitrobenzene ND mg/kg 10/30/23 14:10 100-25-4 L210/27/23 11:220.40 0.12 1
2,4-Dinitrophenol ND mg/kg 10/30/23 14:10 51-28-510/27/23 11:222.0 1.2 1
2,4-Dinitrotoluene ND mg/kg 10/30/23 14:10 121-14-210/27/23 11:220.40 0.15 1
2,6-Dinitrotoluene ND mg/kg 10/30/23 14:10 606-20-210/27/23 11:220.40 0.15 1
Di-n-octylphthalate ND mg/kg 10/30/23 14:10 117-84-010/27/23 11:220.40 0.16 1
1,2-Diphenylhydrazine ND mg/kg 10/30/23 14:10 122-66-710/27/23 11:220.40 0.16 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/30/23 14:10 117-81-710/27/23 11:220.40 0.16 1
Fluoranthene ND mg/kg 10/30/23 14:10 206-44-010/27/23 11:220.40 0.14 1
Fluorene ND mg/kg 10/30/23 14:10 86-73-710/27/23 11:220.40 0.14 1
Hexachloro-1,3-butadiene ND mg/kg 10/30/23 14:10 87-68-310/27/23 11:220.40 0.17 1
Hexachlorobenzene ND mg/kg 10/30/23 14:10 118-74-110/27/23 11:220.40 0.16 1
Hexachlorocyclopentadiene ND mg/kg 10/30/23 14:10 77-47-410/27/23 11:220.40 0.23 1
Hexachloroethane ND mg/kg 10/30/23 14:10 67-72-110/27/23 11:220.40 0.15 1
Hexachlorophene ND mg/kg 10/30/23 14:10 70-30-4 IH,v210/27/23 11:224.0 2.3 1
Hexachloropropene ND mg/kg 10/30/23 14:10 1888-71-710/27/23 11:220.40 0.11 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/30/23 14:10 193-39-510/27/23 11:220.40 0.16 1
Isodrin ND mg/kg 10/30/23 14:10 465-73-610/27/23 11:220.40 0.095 1
1-Methylnaphthalene ND mg/kg 10/30/23 14:10 90-12-010/27/23 11:220.40 0.14 1
2-Methylnaphthalene ND mg/kg 10/30/23 14:10 91-57-610/27/23 11:220.40 0.16 1
2-Methyl-5-nitroaniline ND mg/kg 10/30/23 14:10 99-55-810/27/23 11:220.40 0.12 1
2-Methylphenol(o-Cresol)ND mg/kg 10/30/23 14:10 95-48-710/27/23 11:220.40 0.16 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/30/23 14:10 15831-10-410/27/23 11:220.40 0.16 1
1-Naphthalenamine ND mg/kg 10/30/23 14:10 134-32-710/27/23 11:220.80 0.13 1
2-Naphthalenamine ND mg/kg 10/30/23 14:10 91-59-810/27/23 11:220.80 0.15 1
Naphthalene ND mg/kg 10/30/23 14:10 91-20-310/27/23 11:220.40 0.14 1
2-Nitroaniline ND mg/kg 10/30/23 14:10 88-74-410/27/23 11:222.0 0.33 1
3-Nitroaniline ND mg/kg 10/30/23 14:10 99-09-210/27/23 11:222.0 0.31 1
4-Nitroaniline ND mg/kg 10/30/23 14:10 100-01-610/27/23 11:220.80 0.30 1
Nitrobenzene ND mg/kg 10/30/23 14:10 98-95-310/27/23 11:220.40 0.19 1
2-Nitrophenol ND mg/kg 10/30/23 14:10 88-75-510/27/23 11:220.40 0.17 1
4-Nitrophenol ND mg/kg 10/30/23 14:10 100-02-710/27/23 11:222.0 0.77 1
N-Nitroso-di-n-propylamine ND mg/kg 10/30/23 14:10 621-64-710/27/23 11:220.40 0.15 1
Pentachlorophenol ND mg/kg 10/30/23 14:10 87-86-510/27/23 11:220.80 0.39 1
Phenanthrene ND mg/kg 10/30/23 14:10 85-01-810/27/23 11:220.40 0.13 1
Phenol ND mg/kg 10/30/23 14:10 108-95-210/27/23 11:220.40 0.18 1
Pyrene ND mg/kg 10/30/23 14:10 129-00-010/27/23 11:220.40 0.16 1
Pyridine ND mg/kg 10/30/23 14:10 110-86-1 v110/27/23 11:220.40 0.13 1
1,2,4,5-Tetrachlorobenzene ND mg/kg 10/30/23 14:10 95-94-310/27/23 11:220.40 0.097 1
2,3,4,6-Tetrachlorophenol ND mg/kg 10/30/23 14:10 58-90-210/27/23 11:220.40 0.10 1
2,4,5-Trichlorophenol ND mg/kg 10/30/23 14:10 95-95-410/27/23 11:220.40 0.18 1
2,4,6-Trichlorophenol ND mg/kg 10/30/23 14:10 88-06-210/27/23 11:220.40 0.16 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-11 Lab ID:92695355007 Collected:10/24/23 14:10 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorobiphenyl (S)37 %10/30/23 14:10 321-60-810/27/23 11:2210-130 1
Terphenyl-d14 (S)57 %10/30/23 14:10 1718-51-010/27/23 11:2210-130 1
Phenol-d6 (S)38 %10/30/23 14:10 13127-88-310/27/23 11:2210-130 1
2-Fluorophenol (S)40 %10/30/23 14:10 367-12-410/27/23 11:2210-130 1
2,4,6-Tribromophenol (S)42 %10/30/23 14:10 118-79-610/27/23 11:2210-130 1
Nitrobenzene-d5 (S)41 %10/30/23 14:10 4165-60-010/27/23 11:2210-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/27/23 19:17 67-64-110/27/23 12:430.14 0.044 1
Benzene ND mg/kg 10/27/23 19:17 71-43-210/27/23 12:430.0069 0.0027 1
Bromobenzene ND mg/kg 10/27/23 19:17 108-86-110/27/23 12:430.0069 0.0022 1
Bromochloromethane ND mg/kg 10/27/23 19:17 74-97-510/27/23 12:430.0069 0.0020 1
Bromodichloromethane ND mg/kg 10/27/23 19:17 75-27-410/27/23 12:430.0069 0.0027 1
Bromoform ND mg/kg 10/27/23 19:17 75-25-210/27/23 12:430.0069 0.0024 1
Bromomethane ND mg/kg 10/27/23 19:17 74-83-9 IK,v110/27/23 12:430.027 0.021 1
2-Butanone (MEK)ND mg/kg 10/27/23 19:17 78-93-310/27/23 12:430.14 0.033 1
n-Butylbenzene ND mg/kg 10/27/23 19:17 104-51-810/27/23 12:430.0069 0.0043 1
sec-Butylbenzene ND mg/kg 10/27/23 19:17 135-98-810/27/23 12:430.0069 0.0030 1
tert-Butylbenzene ND mg/kg 10/27/23 19:17 98-06-610/27/23 12:430.0069 0.0024 1
Carbon tetrachloride ND mg/kg 10/27/23 19:17 56-23-510/27/23 12:430.0069 0.0026 1
Chlorobenzene ND mg/kg 10/27/23 19:17 108-90-710/27/23 12:430.0069 0.0039 1
Chloroethane ND mg/kg 10/27/23 19:17 75-00-310/27/23 12:430.014 0.0053 1
Chloroform ND mg/kg 10/27/23 19:17 67-66-310/27/23 12:430.0069 0.0057 1
Chloromethane ND mg/kg 10/27/23 19:17 74-87-310/27/23 12:430.014 0.0058 1
2-Chlorotoluene ND mg/kg 10/27/23 19:17 95-49-810/27/23 12:430.0069 0.0024 1
4-Chlorotoluene ND mg/kg 10/27/23 19:17 106-43-410/27/23 12:430.0069 0.0038 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/27/23 19:17 96-12-810/27/23 12:430.0069 0.0027 1
Dibromochloromethane ND mg/kg 10/27/23 19:17 124-48-110/27/23 12:430.0069 0.0039 1
1,2-Dibromoethane (EDB)ND mg/kg 10/27/23 19:17 106-93-410/27/23 12:430.0069 0.0030 1
Dibromomethane ND mg/kg 10/27/23 19:17 74-95-310/27/23 12:430.0069 0.0015 1
1,2-Dichlorobenzene ND mg/kg 10/27/23 19:17 95-50-110/27/23 12:430.0069 0.0025 1
1,3-Dichlorobenzene ND mg/kg 10/27/23 19:17 541-73-110/27/23 12:430.0069 0.0021 1
1,4-Dichlorobenzene ND mg/kg 10/27/23 19:17 106-46-710/27/23 12:430.0069 0.0018 1
Dichlorodifluoromethane ND mg/kg 10/27/23 19:17 75-71-810/27/23 12:430.014 0.0070 1
1,1-Dichloroethane ND mg/kg 10/27/23 19:17 75-34-310/27/23 12:430.0069 0.0028 1
1,2-Dichloroethane ND mg/kg 10/27/23 19:17 107-06-210/27/23 12:430.0069 0.0045 1
1,1-Dichloroethene ND mg/kg 10/27/23 19:17 75-35-410/27/23 12:430.0069 0.0028 1
cis-1,2-Dichloroethene ND mg/kg 10/27/23 19:17 156-59-210/27/23 12:430.0069 0.0023 1
trans-1,2-Dichloroethene ND mg/kg 10/27/23 19:17 156-60-510/27/23 12:430.0069 0.0058 1
1,2-Dichloropropane ND mg/kg 10/27/23 19:17 78-87-510/27/23 12:430.0069 0.0021 1
1,3-Dichloropropane ND mg/kg 10/27/23 19:17 142-28-910/27/23 12:430.0069 0.0021 1
2,2-Dichloropropane ND mg/kg 10/27/23 19:17 594-20-710/27/23 12:430.0069 0.0052 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-11 Lab ID:92695355007 Collected:10/24/23 14:10 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND mg/kg 10/27/23 19:17 563-58-610/27/23 12:430.0069 0.0033 1
cis-1,3-Dichloropropene ND mg/kg 10/27/23 19:17 10061-01-510/27/23 12:430.0069 0.0019 1
trans-1,3-Dichloropropene ND mg/kg 10/27/23 19:17 10061-02-610/27/23 12:430.0069 0.0024 1
Diisopropyl ether ND mg/kg 10/27/23 19:17 108-20-310/27/23 12:430.0069 0.0019 1
Ethylbenzene 0.0056J mg/kg 10/27/23 19:17 100-41-410/27/23 12:430.0069 0.0032 1
Hexachloro-1,3-butadiene ND mg/kg 10/27/23 19:17 87-68-310/27/23 12:430.014 0.011 1
2-Hexanone ND mg/kg 10/27/23 19:17 591-78-610/27/23 12:430.069 0.0066 1
Isopropylbenzene (Cumene)ND mg/kg 10/27/23 19:17 98-82-810/27/23 12:430.0069 0.0023 1
p-Isopropyltoluene ND mg/kg 10/27/23 19:17 99-87-610/27/23 12:430.0069 0.0034 1
Methylene Chloride ND mg/kg 10/27/23 19:17 75-09-210/27/23 12:430.027 0.019 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/27/23 19:17 108-10-110/27/23 12:430.069 0.0066 1
Methyl-tert-butyl ether ND mg/kg 10/27/23 19:17 1634-04-410/27/23 12:430.0069 0.0026 1
Naphthalene ND mg/kg 10/27/23 19:17 91-20-310/27/23 12:430.0069 0.0036 1
n-Propylbenzene ND mg/kg 10/27/23 19:17 103-65-110/27/23 12:430.0069 0.0024 1
Styrene ND mg/kg 10/27/23 19:17 100-42-510/27/23 12:430.0069 0.0018 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/27/23 19:17 630-20-610/27/23 12:430.0069 0.0026 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/27/23 19:17 79-34-510/27/23 12:430.0069 0.0018 1
Tetrachloroethene ND mg/kg 10/27/23 19:17 127-18-410/27/23 12:430.0069 0.0022 1
Toluene ND mg/kg 10/27/23 19:17 108-88-310/27/23 12:430.0069 0.0047 1
1,2,3-Trichlorobenzene ND mg/kg 10/27/23 19:17 87-61-610/27/23 12:430.0069 0.0055 1
1,2,4-Trichlorobenzene ND mg/kg 10/27/23 19:17 120-82-110/27/23 12:430.0069 0.0058 1
1,1,1-Trichloroethane ND mg/kg 10/27/23 19:17 71-55-610/27/23 12:430.0069 0.0036 1
1,1,2-Trichloroethane ND mg/kg 10/27/23 19:17 79-00-510/27/23 12:430.0069 0.0023 1
Trichloroethene ND mg/kg 10/27/23 19:17 79-01-610/27/23 12:430.0069 0.0055 1
Trichlorofluoromethane ND mg/kg 10/27/23 19:17 75-69-410/27/23 12:430.0069 0.0038 1
1,2,3-Trichloropropane ND mg/kg 10/27/23 19:17 96-18-410/27/23 12:430.0069 0.0035 1
1,2,4-Trimethylbenzene ND mg/kg 10/27/23 19:17 95-63-610/27/23 12:430.0069 0.0041 1
1,3,5-Trimethylbenzene ND mg/kg 10/27/23 19:17 108-67-810/27/23 12:430.0069 0.0023 1
Vinyl acetate ND mg/kg 10/27/23 19:17 108-05-410/27/23 12:430.069 0.014 1
Vinyl chloride ND mg/kg 10/27/23 19:17 75-01-410/27/23 12:430.014 0.0035 1
Xylene (Total)ND mg/kg 10/27/23 19:17 1330-20-710/27/23 12:430.014 0.0039 1
m&p-Xylene 0.0054J mg/kg 10/27/23 19:17 179601-23-110/27/23 12:430.014 0.0047 1
o-Xylene ND mg/kg 10/27/23 19:17 95-47-610/27/23 12:430.0069 0.0030 1
Surrogates
Toluene-d8 (S)100 %10/27/23 19:17 2037-26-510/27/23 12:4370-130 1
4-Bromofluorobenzene (S)100 %10/27/23 19:17 460-00-410/27/23 12:4370-130 1
1,2-Dichloroethane-d4 (S)101 %10/27/23 19:17 17060-07-010/27/23 12:4370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.5 %10/26/23 18:54 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-11 Lab ID:92695355007 Collected:10/24/23 14:10 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 79.9 %11/01/23 10:2011/01/23 10:141
Sample:SB-12 Lab ID:92695355008 Collected:10/24/23 14:20 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.46J mg/kg 10/27/23 21:49 18540-29-910/27/23 09:451.3 0.0013 1
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.95 mg/kg 11/02/23 14:18 7440-38-211/01/23 07:521.54 0.154 5
Barium 39.1 mg/kg 11/02/23 14:18 7440-39-311/01/23 07:523.86 0.234 5
Cadmium 0.498J mg/kg 11/02/23 14:18 7440-43-9 J11/01/23 07:521.54 0.132 5
Chromium 43.5 mg/kg 11/02/23 14:18 7440-47-311/01/23 07:527.71 0.457 5
Lead 39.6 mg/kg 11/02/23 14:18 7439-92-111/01/23 07:523.09 0.153 5
Selenium 1.06J mg/kg 11/02/23 14:18 7782-49-2 J11/01/23 07:523.86 0.278 5
Silver ND mg/kg 11/02/23 14:18 7440-22-411/01/23 07:520.771 0.133 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0739 mg/kg 11/01/23 18:30 7439-97-610/31/23 22:140.0617 0.0278 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/30/23 14:38 83-32-910/27/23 11:220.43 0.15 1
Acenaphthylene ND mg/kg 10/30/23 14:38 208-96-810/27/23 11:220.43 0.15 1
Acetophenone ND mg/kg 10/30/23 14:38 98-86-210/27/23 11:220.43 0.11 1
Aniline ND mg/kg 10/30/23 14:38 62-53-310/27/23 11:220.43 0.17 1
Atrazine ND mg/kg 10/30/23 14:38 1912-24-910/27/23 11:220.43 0.14 1
Benzaldehyde ND mg/kg 10/30/23 14:38 100-52-710/27/23 11:220.43 0.14 1
Benzidine ND mg/kg 10/30/23 14:38 92-87-510/27/23 11:222.2 0.36 1
Benzo(a)anthracene ND mg/kg 10/30/23 14:38 56-55-310/27/23 11:220.43 0.14 1
Benzo(a)pyrene ND mg/kg 10/30/23 14:38 50-32-810/27/23 11:220.43 0.15 1
Benzo(b)fluoranthene ND mg/kg 10/30/23 14:38 205-99-210/27/23 11:220.43 0.14 1
Benzo(g,h,i)perylene ND mg/kg 10/30/23 14:38 191-24-210/27/23 11:220.43 0.17 1
Benzo(k)fluoranthene ND mg/kg 10/30/23 14:38 207-08-910/27/23 11:220.43 0.15 1
Benzoic Acid ND mg/kg 10/30/23 14:38 65-85-010/27/23 11:222.2 0.93 1
Benzophenone ND mg/kg 10/30/23 14:38 119-61-910/27/23 11:220.43 0.20 1
Benzyl alcohol ND mg/kg 10/30/23 14:38 100-51-610/27/23 11:220.87 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-12 Lab ID:92695355008 Collected:10/24/23 14:20 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Biphenyl (Diphenyl)ND mg/kg 10/30/23 14:38 92-52-410/27/23 11:220.43 0.10 1
4-Bromophenylphenyl ether ND mg/kg 10/30/23 14:38 101-55-310/27/23 11:220.43 0.17 1
Butylbenzylphthalate ND mg/kg 10/30/23 14:38 85-68-710/27/23 11:220.43 0.18 1
Caprolactam ND mg/kg 10/30/23 14:38 105-60-210/27/23 11:220.43 0.23 1
Carbazole ND mg/kg 10/30/23 14:38 86-74-810/27/23 11:220.43 0.15 1
4-Chloro-3-methylphenol ND mg/kg 10/30/23 14:38 59-50-710/27/23 11:220.87 0.31 1
4-Chloroaniline ND mg/kg 10/30/23 14:38 106-47-810/27/23 11:220.87 0.34 1
Chlorobenzilate ND mg/kg 10/30/23 14:38 510-15-610/27/23 11:220.43 0.086 1
bis(2-Chloroethoxy)methane ND mg/kg 10/30/23 14:38 111-91-110/27/23 11:220.43 0.18 1
bis(2-Chloroethyl) ether ND mg/kg 10/30/23 14:38 111-44-410/27/23 11:220.43 0.16 1
2-Chloronaphthalene ND mg/kg 10/30/23 14:38 91-58-710/27/23 11:220.43 0.17 1
2-Chlorophenol ND mg/kg 10/30/23 14:38 95-57-810/27/23 11:220.43 0.16 1
4-Chlorophenylphenyl ether ND mg/kg 10/30/23 14:38 7005-72-310/27/23 11:220.43 0.16 1
Chrysene ND mg/kg 10/30/23 14:38 218-01-910/27/23 11:220.43 0.16 1
Dibenz(a,h)anthracene ND mg/kg 10/30/23 14:38 53-70-310/27/23 11:220.43 0.17 1
Dibenzo(a,e)pyrene ND mg/kg 10/30/23 14:38 192-65-410/27/23 11:221.3 0.29 1
Dibenzofuran ND mg/kg 10/30/23 14:38 132-64-910/27/23 11:220.43 0.16 1
1,2-Dichlorobenzene ND mg/kg 10/30/23 14:38 95-50-110/27/23 11:220.43 0.16 1
1,3-Dichlorobenzene ND mg/kg 10/30/23 14:38 541-73-110/27/23 11:220.43 0.15 1
1,4-Dichlorobenzene ND mg/kg 10/30/23 14:38 106-46-710/27/23 11:220.43 0.17 1
3,3'-Dichlorobenzidine ND mg/kg 10/30/23 14:38 91-94-1 L210/27/23 11:220.87 0.29 1
2,4-Dichlorophenol ND mg/kg 10/30/23 14:38 120-83-210/27/23 11:220.43 0.17 1
2,6-Dichlorophenol ND mg/kg 10/30/23 14:38 87-65-0 L210/27/23 11:220.43 0.11 1
2,3-Dichloroaniline ND mg/kg 10/30/23 14:38 608-27-510/27/23 11:220.43 0.21 1
Diethylphthalate ND mg/kg 10/30/23 14:38 84-66-210/27/23 11:220.43 0.16 1
3,3'-Dimethylbenzidine ND mg/kg 10/30/23 14:38 119-93-7 IL10/27/23 11:220.87 0.39 1
2,4-Dimethylphenol ND mg/kg 10/30/23 14:38 105-67-910/27/23 11:220.43 0.18 1
Dimethylphthalate ND mg/kg 10/30/23 14:38 131-11-310/27/23 11:220.43 0.16 1
Di-n-butylphthalate ND mg/kg 10/30/23 14:38 84-74-210/27/23 11:220.43 0.15 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/30/23 14:38 534-52-110/27/23 11:220.87 0.41 1
1,3-Dinitrobenzene ND mg/kg 10/30/23 14:38 99-65-0 L210/27/23 11:220.43 0.097 1
1,4-Dinitrobenzene ND mg/kg 10/30/23 14:38 100-25-4 L210/27/23 11:220.43 0.13 1
2,4-Dinitrophenol ND mg/kg 10/30/23 14:38 51-28-510/27/23 11:222.2 1.3 1
2,4-Dinitrotoluene ND mg/kg 10/30/23 14:38 121-14-210/27/23 11:220.43 0.17 1
2,6-Dinitrotoluene ND mg/kg 10/30/23 14:38 606-20-210/27/23 11:220.43 0.16 1
Di-n-octylphthalate ND mg/kg 10/30/23 14:38 117-84-010/27/23 11:220.43 0.17 1
1,2-Diphenylhydrazine ND mg/kg 10/30/23 14:38 122-66-710/27/23 11:220.43 0.17 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/30/23 14:38 117-81-710/27/23 11:220.43 0.17 1
Fluoranthene 0.17J mg/kg 10/30/23 14:38 206-44-010/27/23 11:220.43 0.15 1
Fluorene ND mg/kg 10/30/23 14:38 86-73-710/27/23 11:220.43 0.15 1
Hexachloro-1,3-butadiene ND mg/kg 10/30/23 14:38 87-68-310/27/23 11:220.43 0.19 1
Hexachlorobenzene ND mg/kg 10/30/23 14:38 118-74-110/27/23 11:220.43 0.17 1
Hexachlorocyclopentadiene ND mg/kg 10/30/23 14:38 77-47-410/27/23 11:220.43 0.25 1
Hexachloroethane ND mg/kg 10/30/23 14:38 67-72-110/27/23 11:220.43 0.17 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-12 Lab ID:92695355008 Collected:10/24/23 14:20 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Hexachlorophene ND mg/kg 10/30/23 14:38 70-30-4 IH,v210/27/23 11:224.3 2.5 1
Hexachloropropene ND mg/kg 10/30/23 14:38 1888-71-710/27/23 11:220.43 0.12 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/30/23 14:38 193-39-510/27/23 11:220.43 0.17 1
Isodrin ND mg/kg 10/30/23 14:38 465-73-610/27/23 11:220.43 0.10 1
1-Methylnaphthalene ND mg/kg 10/30/23 14:38 90-12-010/27/23 11:220.43 0.15 1
2-Methylnaphthalene ND mg/kg 10/30/23 14:38 91-57-610/27/23 11:220.43 0.17 1
2-Methyl-5-nitroaniline ND mg/kg 10/30/23 14:38 99-55-810/27/23 11:220.43 0.13 1
2-Methylphenol(o-Cresol)ND mg/kg 10/30/23 14:38 95-48-710/27/23 11:220.43 0.18 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/30/23 14:38 15831-10-410/27/23 11:220.43 0.17 1
1-Naphthalenamine ND mg/kg 10/30/23 14:38 134-32-710/27/23 11:220.87 0.15 1
2-Naphthalenamine ND mg/kg 10/30/23 14:38 91-59-810/27/23 11:220.87 0.17 1
Naphthalene ND mg/kg 10/30/23 14:38 91-20-310/27/23 11:220.43 0.15 1
2-Nitroaniline ND mg/kg 10/30/23 14:38 88-74-410/27/23 11:222.2 0.36 1
3-Nitroaniline ND mg/kg 10/30/23 14:38 99-09-210/27/23 11:222.2 0.34 1
4-Nitroaniline ND mg/kg 10/30/23 14:38 100-01-610/27/23 11:220.87 0.33 1
Nitrobenzene ND mg/kg 10/30/23 14:38 98-95-310/27/23 11:220.43 0.20 1
2-Nitrophenol ND mg/kg 10/30/23 14:38 88-75-510/27/23 11:220.43 0.19 1
4-Nitrophenol ND mg/kg 10/30/23 14:38 100-02-710/27/23 11:222.2 0.84 1
N-Nitroso-di-n-propylamine ND mg/kg 10/30/23 14:38 621-64-710/27/23 11:220.43 0.16 1
Pentachlorophenol ND mg/kg 10/30/23 14:38 87-86-510/27/23 11:220.87 0.42 1
Phenanthrene ND mg/kg 10/30/23 14:38 85-01-810/27/23 11:220.43 0.14 1
Phenol ND mg/kg 10/30/23 14:38 108-95-210/27/23 11:220.43 0.19 1
Pyrene 0.20J mg/kg 10/30/23 14:38 129-00-010/27/23 11:220.43 0.18 1
Pyridine ND mg/kg 10/30/23 14:38 110-86-1 v110/27/23 11:220.43 0.14 1
1,2,4,5-Tetrachlorobenzene ND mg/kg 10/30/23 14:38 95-94-310/27/23 11:220.43 0.11 1
2,3,4,6-Tetrachlorophenol ND mg/kg 10/30/23 14:38 58-90-210/27/23 11:220.43 0.11 1
2,4,5-Trichlorophenol ND mg/kg 10/30/23 14:38 95-95-410/27/23 11:220.43 0.20 1
2,4,6-Trichlorophenol ND mg/kg 10/30/23 14:38 88-06-210/27/23 11:220.43 0.18 1
Surrogates
2-Fluorobiphenyl (S)56 %10/30/23 14:38 321-60-810/27/23 11:2210-130 1
Terphenyl-d14 (S)60 %10/30/23 14:38 1718-51-010/27/23 11:2210-130 1
Phenol-d6 (S)49 %10/30/23 14:38 13127-88-310/27/23 11:2210-130 1
2-Fluorophenol (S)47 %10/30/23 14:38 367-12-410/27/23 11:2210-130 1
2,4,6-Tribromophenol (S)46 %10/30/23 14:38 118-79-610/27/23 11:2210-130 1
Nitrobenzene-d5 (S)58 %10/30/23 14:38 4165-60-010/27/23 11:2210-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/27/23 19:35 67-64-110/27/23 12:430.15 0.050 1
Benzene ND mg/kg 10/27/23 19:35 71-43-210/27/23 12:430.0077 0.0031 1
Bromobenzene ND mg/kg 10/27/23 19:35 108-86-110/27/23 12:430.0077 0.0025 1
Bromochloromethane ND mg/kg 10/27/23 19:35 74-97-510/27/23 12:430.0077 0.0023 1
Bromodichloromethane ND mg/kg 10/27/23 19:35 75-27-410/27/23 12:430.0077 0.0030 1
Bromoform ND mg/kg 10/27/23 19:35 75-25-210/27/23 12:430.0077 0.0027 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-12 Lab ID:92695355008 Collected:10/24/23 14:20 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Bromomethane ND mg/kg 10/27/23 19:35 74-83-9 IK,v110/27/23 12:430.031 0.024 1
2-Butanone (MEK)ND mg/kg 10/27/23 19:35 78-93-310/27/23 12:430.15 0.037 1
n-Butylbenzene ND mg/kg 10/27/23 19:35 104-51-810/27/23 12:430.0077 0.0049 1
sec-Butylbenzene ND mg/kg 10/27/23 19:35 135-98-810/27/23 12:430.0077 0.0034 1
tert-Butylbenzene ND mg/kg 10/27/23 19:35 98-06-610/27/23 12:430.0077 0.0027 1
Carbon tetrachloride ND mg/kg 10/27/23 19:35 56-23-510/27/23 12:430.0077 0.0029 1
Chlorobenzene ND mg/kg 10/27/23 19:35 108-90-710/27/23 12:430.0077 0.0044 1
Chloroethane ND mg/kg 10/27/23 19:35 75-00-310/27/23 12:430.015 0.0060 1
Chloroform ND mg/kg 10/27/23 19:35 67-66-310/27/23 12:430.0077 0.0065 1
Chloromethane ND mg/kg 10/27/23 19:35 74-87-310/27/23 12:430.015 0.0065 1
2-Chlorotoluene ND mg/kg 10/27/23 19:35 95-49-810/27/23 12:430.0077 0.0027 1
4-Chlorotoluene ND mg/kg 10/27/23 19:35 106-43-410/27/23 12:430.0077 0.0043 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/27/23 19:35 96-12-810/27/23 12:430.0077 0.0030 1
Dibromochloromethane ND mg/kg 10/27/23 19:35 124-48-110/27/23 12:430.0077 0.0043 1
1,2-Dibromoethane (EDB)ND mg/kg 10/27/23 19:35 106-93-410/27/23 12:430.0077 0.0034 1
Dibromomethane ND mg/kg 10/27/23 19:35 74-95-310/27/23 12:430.0077 0.0017 1
1,2-Dichlorobenzene ND mg/kg 10/27/23 19:35 95-50-110/27/23 12:430.0077 0.0028 1
1,3-Dichlorobenzene ND mg/kg 10/27/23 19:35 541-73-110/27/23 12:430.0077 0.0024 1
1,4-Dichlorobenzene ND mg/kg 10/27/23 19:35 106-46-710/27/23 12:430.0077 0.0020 1
Dichlorodifluoromethane ND mg/kg 10/27/23 19:35 75-71-810/27/23 12:430.015 0.0079 1
1,1-Dichloroethane ND mg/kg 10/27/23 19:35 75-34-310/27/23 12:430.0077 0.0032 1
1,2-Dichloroethane ND mg/kg 10/27/23 19:35 107-06-210/27/23 12:430.0077 0.0051 1
1,1-Dichloroethene ND mg/kg 10/27/23 19:35 75-35-410/27/23 12:430.0077 0.0032 1
cis-1,2-Dichloroethene ND mg/kg 10/27/23 19:35 156-59-210/27/23 12:430.0077 0.0026 1
trans-1,2-Dichloroethene ND mg/kg 10/27/23 19:35 156-60-510/27/23 12:430.0077 0.0066 1
1,2-Dichloropropane ND mg/kg 10/27/23 19:35 78-87-510/27/23 12:430.0077 0.0023 1
1,3-Dichloropropane ND mg/kg 10/27/23 19:35 142-28-910/27/23 12:430.0077 0.0024 1
2,2-Dichloropropane ND mg/kg 10/27/23 19:35 594-20-710/27/23 12:430.0077 0.0058 1
1,1-Dichloropropene ND mg/kg 10/27/23 19:35 563-58-610/27/23 12:430.0077 0.0037 1
cis-1,3-Dichloropropene ND mg/kg 10/27/23 19:35 10061-01-510/27/23 12:430.0077 0.0021 1
trans-1,3-Dichloropropene ND mg/kg 10/27/23 19:35 10061-02-610/27/23 12:430.0077 0.0027 1
Diisopropyl ether ND mg/kg 10/27/23 19:35 108-20-310/27/23 12:430.0077 0.0021 1
Ethylbenzene 0.0068J mg/kg 10/27/23 19:35 100-41-410/27/23 12:430.0077 0.0036 1
Hexachloro-1,3-butadiene ND mg/kg 10/27/23 19:35 87-68-310/27/23 12:430.015 0.013 1
2-Hexanone ND mg/kg 10/27/23 19:35 591-78-610/27/23 12:430.077 0.0074 1
Isopropylbenzene (Cumene)ND mg/kg 10/27/23 19:35 98-82-810/27/23 12:430.0077 0.0026 1
p-Isopropyltoluene ND mg/kg 10/27/23 19:35 99-87-610/27/23 12:430.0077 0.0038 1
Methylene Chloride ND mg/kg 10/27/23 19:35 75-09-210/27/23 12:430.031 0.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/27/23 19:35 108-10-110/27/23 12:430.077 0.0074 1
Methyl-tert-butyl ether ND mg/kg 10/27/23 19:35 1634-04-410/27/23 12:430.0077 0.0029 1
Naphthalene ND mg/kg 10/27/23 19:35 91-20-310/27/23 12:430.0077 0.0041 1
n-Propylbenzene ND mg/kg 10/27/23 19:35 103-65-110/27/23 12:430.0077 0.0027 1
Styrene ND mg/kg 10/27/23 19:35 100-42-510/27/23 12:430.0077 0.0020 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/27/23 19:35 630-20-610/27/23 12:430.0077 0.0030 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-12 Lab ID:92695355008 Collected:10/24/23 14:20 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2,2-Tetrachloroethane ND mg/kg 10/27/23 19:35 79-34-510/27/23 12:430.0077 0.0020 1
Tetrachloroethene ND mg/kg 10/27/23 19:35 127-18-410/27/23 12:430.0077 0.0024 1
Toluene 0.0084 mg/kg 10/27/23 19:35 108-88-310/27/23 12:430.0077 0.0053 1
1,2,3-Trichlorobenzene ND mg/kg 10/27/23 19:35 87-61-610/27/23 12:430.0077 0.0062 1
1,2,4-Trichlorobenzene ND mg/kg 10/27/23 19:35 120-82-110/27/23 12:430.0077 0.0065 1
1,1,1-Trichloroethane ND mg/kg 10/27/23 19:35 71-55-610/27/23 12:430.0077 0.0040 1
1,1,2-Trichloroethane ND mg/kg 10/27/23 19:35 79-00-510/27/23 12:430.0077 0.0026 1
Trichloroethene ND mg/kg 10/27/23 19:35 79-01-610/27/23 12:430.0077 0.0062 1
Trichlorofluoromethane ND mg/kg 10/27/23 19:35 75-69-410/27/23 12:430.0077 0.0042 1
1,2,3-Trichloropropane ND mg/kg 10/27/23 19:35 96-18-410/27/23 12:430.0077 0.0039 1
1,2,4-Trimethylbenzene ND mg/kg 10/27/23 19:35 95-63-610/27/23 12:430.0077 0.0046 1
1,3,5-Trimethylbenzene ND mg/kg 10/27/23 19:35 108-67-810/27/23 12:430.0077 0.0026 1
Vinyl acetate ND mg/kg 10/27/23 19:35 108-05-410/27/23 12:430.077 0.016 1
Vinyl chloride ND mg/kg 10/27/23 19:35 75-01-410/27/23 12:430.015 0.0039 1
Xylene (Total)ND mg/kg 10/27/23 19:35 1330-20-710/27/23 12:430.015 0.0044 1
m&p-Xylene 0.0073J mg/kg 10/27/23 19:35 179601-23-110/27/23 12:430.015 0.0053 1
o-Xylene ND mg/kg 10/27/23 19:35 95-47-610/27/23 12:430.0077 0.0034 1
Surrogates
Toluene-d8 (S)100 %10/27/23 19:35 2037-26-510/27/23 12:4370-130 1
4-Bromofluorobenzene (S)102 %10/27/23 19:35 460-00-410/27/23 12:4370-130 1
1,2-Dichloroethane-d4 (S)104 %10/27/23 19:35 17060-07-010/27/23 12:4370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.5 %10/26/23 18:54 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 64.8 %11/01/23 10:2011/01/23 10:141
Sample:SB-13 Lab ID:92695355009 Collected:10/24/23 14:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.20J mg/kg 10/27/23 22:07 18540-29-910/27/23 09:451.3 0.0013 1
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 1.13J mg/kg 11/02/23 14:22 7440-38-2 J11/01/23 07:521.29 0.129 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-13 Lab ID:92695355009 Collected:10/24/23 14:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Barium 14.5 mg/kg 11/02/23 14:22 7440-39-311/01/23 07:523.24 0.197 5
Cadmium ND mg/kg 11/02/23 14:22 7440-43-911/01/23 07:521.29 0.111 5
Chromium 13.0 mg/kg 11/02/23 14:22 7440-47-311/01/23 07:526.47 0.383 5
Lead 7.75 mg/kg 11/02/23 14:22 7439-92-111/01/23 07:522.59 0.128 5
Selenium 0.458J mg/kg 11/02/23 14:22 7782-49-2 J11/01/23 07:523.24 0.233 5
Silver ND mg/kg 11/02/23 14:22 7440-22-411/01/23 07:520.647 0.112 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0250J mg/kg 11/01/23 18:32 7439-97-6 J10/31/23 22:140.0518 0.0233 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/30/23 15:06 83-32-910/27/23 11:220.42 0.15 1
Acenaphthylene ND mg/kg 10/30/23 15:06 208-96-810/27/23 11:220.42 0.15 1
Acetophenone ND mg/kg 10/30/23 15:06 98-86-210/27/23 11:220.42 0.11 1
Aniline ND mg/kg 10/30/23 15:06 62-53-310/27/23 11:220.42 0.16 1
Atrazine ND mg/kg 10/30/23 15:06 1912-24-910/27/23 11:220.42 0.13 1
Benzaldehyde ND mg/kg 10/30/23 15:06 100-52-710/27/23 11:220.42 0.14 1
Benzidine ND mg/kg 10/30/23 15:06 92-87-510/27/23 11:222.1 0.34 1
Benzo(a)anthracene ND mg/kg 10/30/23 15:06 56-55-310/27/23 11:220.42 0.14 1
Benzo(a)pyrene ND mg/kg 10/30/23 15:06 50-32-810/27/23 11:220.42 0.14 1
Benzo(b)fluoranthene ND mg/kg 10/30/23 15:06 205-99-210/27/23 11:220.42 0.14 1
Benzo(g,h,i)perylene ND mg/kg 10/30/23 15:06 191-24-210/27/23 11:220.42 0.16 1
Benzo(k)fluoranthene ND mg/kg 10/30/23 15:06 207-08-910/27/23 11:220.42 0.15 1
Benzoic Acid ND mg/kg 10/30/23 15:06 65-85-010/27/23 11:222.1 0.89 1
Benzophenone ND mg/kg 10/30/23 15:06 119-61-910/27/23 11:220.42 0.19 1
Benzyl alcohol ND mg/kg 10/30/23 15:06 100-51-610/27/23 11:220.83 0.32 1
Biphenyl (Diphenyl)ND mg/kg 10/30/23 15:06 92-52-410/27/23 11:220.42 0.099 1
4-Bromophenylphenyl ether ND mg/kg 10/30/23 15:06 101-55-310/27/23 11:220.42 0.16 1
Butylbenzylphthalate ND mg/kg 10/30/23 15:06 85-68-710/27/23 11:220.42 0.18 1
Caprolactam ND mg/kg 10/30/23 15:06 105-60-210/27/23 11:220.42 0.22 1
Carbazole ND mg/kg 10/30/23 15:06 86-74-810/27/23 11:220.42 0.14 1
4-Chloro-3-methylphenol ND mg/kg 10/30/23 15:06 59-50-710/27/23 11:220.83 0.29 1
4-Chloroaniline ND mg/kg 10/30/23 15:06 106-47-810/27/23 11:220.83 0.33 1
Chlorobenzilate ND mg/kg 10/30/23 15:06 510-15-610/27/23 11:220.42 0.082 1
bis(2-Chloroethoxy)methane ND mg/kg 10/30/23 15:06 111-91-110/27/23 11:220.42 0.17 1
bis(2-Chloroethyl) ether ND mg/kg 10/30/23 15:06 111-44-410/27/23 11:220.42 0.16 1
2-Chloronaphthalene ND mg/kg 10/30/23 15:06 91-58-710/27/23 11:220.42 0.17 1
2-Chlorophenol ND mg/kg 10/30/23 15:06 95-57-810/27/23 11:220.42 0.16 1
4-Chlorophenylphenyl ether ND mg/kg 10/30/23 15:06 7005-72-310/27/23 11:220.42 0.16 1
Chrysene ND mg/kg 10/30/23 15:06 218-01-910/27/23 11:220.42 0.15 1
Dibenz(a,h)anthracene ND mg/kg 10/30/23 15:06 53-70-310/27/23 11:220.42 0.16 1
Dibenzo(a,e)pyrene ND mg/kg 10/30/23 15:06 192-65-410/27/23 11:221.3 0.28 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-13 Lab ID:92695355009 Collected:10/24/23 14:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dibenzofuran ND mg/kg 10/30/23 15:06 132-64-910/27/23 11:220.42 0.15 1
1,2-Dichlorobenzene ND mg/kg 10/30/23 15:06 95-50-110/27/23 11:220.42 0.15 1
1,3-Dichlorobenzene ND mg/kg 10/30/23 15:06 541-73-110/27/23 11:220.42 0.15 1
1,4-Dichlorobenzene ND mg/kg 10/30/23 15:06 106-46-710/27/23 11:220.42 0.16 1
3,3'-Dichlorobenzidine ND mg/kg 10/30/23 15:06 91-94-1 L210/27/23 11:220.83 0.28 1
2,4-Dichlorophenol ND mg/kg 10/30/23 15:06 120-83-210/27/23 11:220.42 0.16 1
2,6-Dichlorophenol ND mg/kg 10/30/23 15:06 87-65-0 L210/27/23 11:220.42 0.11 1
2,3-Dichloroaniline ND mg/kg 10/30/23 15:06 608-27-510/27/23 11:220.42 0.20 1
Diethylphthalate ND mg/kg 10/30/23 15:06 84-66-210/27/23 11:220.42 0.15 1
3,3'-Dimethylbenzidine ND mg/kg 10/30/23 15:06 119-93-7 IL10/27/23 11:220.83 0.37 1
2,4-Dimethylphenol ND mg/kg 10/30/23 15:06 105-67-910/27/23 11:220.42 0.17 1
Dimethylphthalate ND mg/kg 10/30/23 15:06 131-11-310/27/23 11:220.42 0.15 1
Di-n-butylphthalate ND mg/kg 10/30/23 15:06 84-74-210/27/23 11:220.42 0.14 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/30/23 15:06 534-52-110/27/23 11:220.83 0.39 1
1,3-Dinitrobenzene ND mg/kg 10/30/23 15:06 99-65-0 L210/27/23 11:220.42 0.094 1
1,4-Dinitrobenzene ND mg/kg 10/30/23 15:06 100-25-4 L210/27/23 11:220.42 0.12 1
2,4-Dinitrophenol ND mg/kg 10/30/23 15:06 51-28-510/27/23 11:222.1 1.3 1
2,4-Dinitrotoluene ND mg/kg 10/30/23 15:06 121-14-210/27/23 11:220.42 0.16 1
2,6-Dinitrotoluene ND mg/kg 10/30/23 15:06 606-20-210/27/23 11:220.42 0.15 1
Di-n-octylphthalate ND mg/kg 10/30/23 15:06 117-84-010/27/23 11:220.42 0.16 1
1,2-Diphenylhydrazine ND mg/kg 10/30/23 15:06 122-66-710/27/23 11:220.42 0.16 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/30/23 15:06 117-81-710/27/23 11:220.42 0.16 1
Fluoranthene ND mg/kg 10/30/23 15:06 206-44-010/27/23 11:220.42 0.14 1
Fluorene ND mg/kg 10/30/23 15:06 86-73-710/27/23 11:220.42 0.15 1
Hexachloro-1,3-butadiene ND mg/kg 10/30/23 15:06 87-68-310/27/23 11:220.42 0.18 1
Hexachlorobenzene ND mg/kg 10/30/23 15:06 118-74-110/27/23 11:220.42 0.16 1
Hexachlorocyclopentadiene ND mg/kg 10/30/23 15:06 77-47-410/27/23 11:220.42 0.24 1
Hexachloroethane ND mg/kg 10/30/23 15:06 67-72-110/27/23 11:220.42 0.16 1
Hexachlorophene ND mg/kg 10/30/23 15:06 70-30-4 IH,v210/27/23 11:224.2 2.4 1
Hexachloropropene ND mg/kg 10/30/23 15:06 1888-71-710/27/23 11:220.42 0.11 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/30/23 15:06 193-39-510/27/23 11:220.42 0.16 1
Isodrin ND mg/kg 10/30/23 15:06 465-73-610/27/23 11:220.42 0.099 1
1-Methylnaphthalene ND mg/kg 10/30/23 15:06 90-12-010/27/23 11:220.42 0.15 1
2-Methylnaphthalene ND mg/kg 10/30/23 15:06 91-57-610/27/23 11:220.42 0.17 1
2-Methyl-5-nitroaniline ND mg/kg 10/30/23 15:06 99-55-810/27/23 11:220.42 0.13 1
2-Methylphenol(o-Cresol)ND mg/kg 10/30/23 15:06 95-48-710/27/23 11:220.42 0.17 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/30/23 15:06 15831-10-410/27/23 11:220.42 0.17 1
1-Naphthalenamine ND mg/kg 10/30/23 15:06 134-32-710/27/23 11:220.83 0.14 1
2-Naphthalenamine ND mg/kg 10/30/23 15:06 91-59-810/27/23 11:220.83 0.16 1
Naphthalene ND mg/kg 10/30/23 15:06 91-20-310/27/23 11:220.42 0.14 1
2-Nitroaniline ND mg/kg 10/30/23 15:06 88-74-410/27/23 11:222.1 0.34 1
3-Nitroaniline ND mg/kg 10/30/23 15:06 99-09-210/27/23 11:222.1 0.33 1
4-Nitroaniline ND mg/kg 10/30/23 15:06 100-01-610/27/23 11:220.83 0.32 1
Nitrobenzene ND mg/kg 10/30/23 15:06 98-95-310/27/23 11:220.42 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-13 Lab ID:92695355009 Collected:10/24/23 14:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2-Nitrophenol ND mg/kg 10/30/23 15:06 88-75-510/27/23 11:220.42 0.18 1
4-Nitrophenol ND mg/kg 10/30/23 15:06 100-02-710/27/23 11:222.1 0.81 1
N-Nitroso-di-n-propylamine ND mg/kg 10/30/23 15:06 621-64-710/27/23 11:220.42 0.16 1
Pentachlorophenol ND mg/kg 10/30/23 15:06 87-86-510/27/23 11:220.83 0.41 1
Phenanthrene ND mg/kg 10/30/23 15:06 85-01-810/27/23 11:220.42 0.14 1
Phenol ND mg/kg 10/30/23 15:06 108-95-210/27/23 11:220.42 0.19 1
Pyrene ND mg/kg 10/30/23 15:06 129-00-010/27/23 11:220.42 0.17 1
Pyridine ND mg/kg 10/30/23 15:06 110-86-1 v110/27/23 11:220.42 0.13 1
1,2,4,5-Tetrachlorobenzene ND mg/kg 10/30/23 15:06 95-94-310/27/23 11:220.42 0.10 1
2,3,4,6-Tetrachlorophenol ND mg/kg 10/30/23 15:06 58-90-210/27/23 11:220.42 0.10 1
2,4,5-Trichlorophenol ND mg/kg 10/30/23 15:06 95-95-410/27/23 11:220.42 0.19 1
2,4,6-Trichlorophenol ND mg/kg 10/30/23 15:06 88-06-210/27/23 11:220.42 0.17 1
Surrogates
2-Fluorobiphenyl (S)49 %10/30/23 15:06 321-60-810/27/23 11:2210-130 1
Terphenyl-d14 (S)54 %10/30/23 15:06 1718-51-010/27/23 11:2210-130 1
Phenol-d6 (S)48 %10/30/23 15:06 13127-88-310/27/23 11:2210-130 1
2-Fluorophenol (S)51 %10/30/23 15:06 367-12-410/27/23 11:2210-130 1
2,4,6-Tribromophenol (S)47 %10/30/23 15:06 118-79-610/27/23 11:2210-130 1
Nitrobenzene-d5 (S)51 %10/30/23 15:06 4165-60-010/27/23 11:2210-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/27/23 19:54 67-64-110/27/23 12:430.14 0.045 1
Benzene ND mg/kg 10/27/23 19:54 71-43-210/27/23 12:430.0070 0.0028 1
Bromobenzene ND mg/kg 10/27/23 19:54 108-86-110/27/23 12:430.0070 0.0023 1
Bromochloromethane ND mg/kg 10/27/23 19:54 74-97-510/27/23 12:430.0070 0.0021 1
Bromodichloromethane ND mg/kg 10/27/23 19:54 75-27-410/27/23 12:430.0070 0.0027 1
Bromoform ND mg/kg 10/27/23 19:54 75-25-210/27/23 12:430.0070 0.0025 1
Bromomethane ND mg/kg 10/27/23 19:54 74-83-9 IK,v110/27/23 12:430.028 0.022 1
2-Butanone (MEK)ND mg/kg 10/27/23 19:54 78-93-310/27/23 12:430.14 0.034 1
n-Butylbenzene ND mg/kg 10/27/23 19:54 104-51-810/27/23 12:430.0070 0.0044 1
sec-Butylbenzene ND mg/kg 10/27/23 19:54 135-98-810/27/23 12:430.0070 0.0031 1
tert-Butylbenzene ND mg/kg 10/27/23 19:54 98-06-610/27/23 12:430.0070 0.0025 1
Carbon tetrachloride ND mg/kg 10/27/23 19:54 56-23-510/27/23 12:430.0070 0.0026 1
Chlorobenzene ND mg/kg 10/27/23 19:54 108-90-710/27/23 12:430.0070 0.0040 1
Chloroethane ND mg/kg 10/27/23 19:54 75-00-310/27/23 12:430.014 0.0054 1
Chloroform ND mg/kg 10/27/23 19:54 67-66-310/27/23 12:430.0070 0.0059 1
Chloromethane ND mg/kg 10/27/23 19:54 74-87-310/27/23 12:430.014 0.0059 1
2-Chlorotoluene ND mg/kg 10/27/23 19:54 95-49-810/27/23 12:430.0070 0.0025 1
4-Chlorotoluene ND mg/kg 10/27/23 19:54 106-43-410/27/23 12:430.0070 0.0039 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/27/23 19:54 96-12-810/27/23 12:430.0070 0.0027 1
Dibromochloromethane ND mg/kg 10/27/23 19:54 124-48-110/27/23 12:430.0070 0.0039 1
1,2-Dibromoethane (EDB)ND mg/kg 10/27/23 19:54 106-93-410/27/23 12:430.0070 0.0031 1
Dibromomethane ND mg/kg 10/27/23 19:54 74-95-310/27/23 12:430.0070 0.0015 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-13 Lab ID:92695355009 Collected:10/24/23 14:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichlorobenzene ND mg/kg 10/27/23 19:54 95-50-110/27/23 12:430.0070 0.0025 1
1,3-Dichlorobenzene ND mg/kg 10/27/23 19:54 541-73-110/27/23 12:430.0070 0.0022 1
1,4-Dichlorobenzene ND mg/kg 10/27/23 19:54 106-46-710/27/23 12:430.0070 0.0018 1
Dichlorodifluoromethane ND mg/kg 10/27/23 19:54 75-71-810/27/23 12:430.014 0.0072 1
1,1-Dichloroethane ND mg/kg 10/27/23 19:54 75-34-310/27/23 12:430.0070 0.0029 1
1,2-Dichloroethane ND mg/kg 10/27/23 19:54 107-06-210/27/23 12:430.0070 0.0047 1
1,1-Dichloroethene ND mg/kg 10/27/23 19:54 75-35-410/27/23 12:430.0070 0.0029 1
cis-1,2-Dichloroethene ND mg/kg 10/27/23 19:54 156-59-210/27/23 12:430.0070 0.0024 1
trans-1,2-Dichloroethene ND mg/kg 10/27/23 19:54 156-60-510/27/23 12:430.0070 0.0060 1
1,2-Dichloropropane ND mg/kg 10/27/23 19:54 78-87-510/27/23 12:430.0070 0.0021 1
1,3-Dichloropropane ND mg/kg 10/27/23 19:54 142-28-910/27/23 12:430.0070 0.0022 1
2,2-Dichloropropane ND mg/kg 10/27/23 19:54 594-20-710/27/23 12:430.0070 0.0053 1
1,1-Dichloropropene ND mg/kg 10/27/23 19:54 563-58-610/27/23 12:430.0070 0.0034 1
cis-1,3-Dichloropropene ND mg/kg 10/27/23 19:54 10061-01-510/27/23 12:430.0070 0.0019 1
trans-1,3-Dichloropropene ND mg/kg 10/27/23 19:54 10061-02-610/27/23 12:430.0070 0.0024 1
Diisopropyl ether ND mg/kg 10/27/23 19:54 108-20-310/27/23 12:430.0070 0.0019 1
Ethylbenzene 0.0051J mg/kg 10/27/23 19:54 100-41-410/27/23 12:430.0070 0.0033 1
Hexachloro-1,3-butadiene ND mg/kg 10/27/23 19:54 87-68-310/27/23 12:430.014 0.011 1
2-Hexanone ND mg/kg 10/27/23 19:54 591-78-610/27/23 12:430.070 0.0068 1
Isopropylbenzene (Cumene)ND mg/kg 10/27/23 19:54 98-82-810/27/23 12:430.0070 0.0024 1
p-Isopropyltoluene ND mg/kg 10/27/23 19:54 99-87-610/27/23 12:430.0070 0.0035 1
Methylene Chloride ND mg/kg 10/27/23 19:54 75-09-210/27/23 12:430.028 0.019 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/27/23 19:54 108-10-110/27/23 12:430.070 0.0068 1
Methyl-tert-butyl ether ND mg/kg 10/27/23 19:54 1634-04-410/27/23 12:430.0070 0.0026 1
Naphthalene ND mg/kg 10/27/23 19:54 91-20-310/27/23 12:430.0070 0.0037 1
n-Propylbenzene ND mg/kg 10/27/23 19:54 103-65-110/27/23 12:430.0070 0.0025 1
Styrene ND mg/kg 10/27/23 19:54 100-42-510/27/23 12:430.0070 0.0019 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/27/23 19:54 630-20-610/27/23 12:430.0070 0.0027 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/27/23 19:54 79-34-510/27/23 12:430.0070 0.0019 1
Tetrachloroethene ND mg/kg 10/27/23 19:54 127-18-410/27/23 12:430.0070 0.0022 1
Toluene ND mg/kg 10/27/23 19:54 108-88-310/27/23 12:430.0070 0.0048 1
1,2,3-Trichlorobenzene ND mg/kg 10/27/23 19:54 87-61-610/27/23 12:430.0070 0.0057 1
1,2,4-Trichlorobenzene ND mg/kg 10/27/23 19:54 120-82-110/27/23 12:430.0070 0.0059 1
1,1,1-Trichloroethane ND mg/kg 10/27/23 19:54 71-55-610/27/23 12:430.0070 0.0037 1
1,1,2-Trichloroethane ND mg/kg 10/27/23 19:54 79-00-510/27/23 12:430.0070 0.0023 1
Trichloroethene ND mg/kg 10/27/23 19:54 79-01-610/27/23 12:430.0070 0.0057 1
Trichlorofluoromethane ND mg/kg 10/27/23 19:54 75-69-410/27/23 12:430.0070 0.0039 1
1,2,3-Trichloropropane ND mg/kg 10/27/23 19:54 96-18-410/27/23 12:430.0070 0.0036 1
1,2,4-Trimethylbenzene ND mg/kg 10/27/23 19:54 95-63-610/27/23 12:430.0070 0.0042 1
1,3,5-Trimethylbenzene ND mg/kg 10/27/23 19:54 108-67-810/27/23 12:430.0070 0.0024 1
Vinyl acetate ND mg/kg 10/27/23 19:54 108-05-410/27/23 12:430.070 0.014 1
Vinyl chloride ND mg/kg 10/27/23 19:54 75-01-410/27/23 12:430.014 0.0036 1
Xylene (Total)ND mg/kg 10/27/23 19:54 1330-20-710/27/23 12:430.014 0.0040 1
m&p-Xylene ND mg/kg 10/27/23 19:54 179601-23-110/27/23 12:430.014 0.0048 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-13 Lab ID:92695355009 Collected:10/24/23 14:40 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
o-Xylene ND mg/kg 10/27/23 19:54 95-47-610/27/23 12:430.0070 0.0031 1
Surrogates
Toluene-d8 (S)100 %10/27/23 19:54 2037-26-510/27/23 12:4370-130 1
4-Bromofluorobenzene (S)99 %10/27/23 19:54 460-00-410/27/23 12:4370-130 1
1,2-Dichloroethane-d4 (S)102 %10/27/23 19:54 17060-07-010/27/23 12:4370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.8 %10/26/23 18:54 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 77.2 %11/01/23 10:1411/01/23 10:091
Sample:SB-DUP Lab ID:92695355010 Collected:10/24/23 00:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.58J mg/kg 10/27/23 22:42 18540-29-910/27/23 09:451.3 0.0013 1
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 3.01 mg/kg 11/02/23 14:25 7440-38-211/01/23 07:521.22 0.122 5
Barium 20.6 mg/kg 11/02/23 14:25 7440-39-311/01/23 07:523.05 0.185 5
Cadmium ND mg/kg 11/02/23 14:25 7440-43-911/01/23 07:521.22 0.104 5
Chromium 38.4 mg/kg 11/02/23 14:25 7440-47-311/01/23 07:526.10 0.361 5
Lead 6.89 mg/kg 11/02/23 14:25 7439-92-111/01/23 07:522.44 0.121 5
Selenium 0.955J mg/kg 11/02/23 14:25 7782-49-2 J11/01/23 07:523.05 0.220 5
Silver ND mg/kg 11/02/23 14:25 7440-22-411/01/23 07:520.610 0.105 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0711 mg/kg 11/01/23 18:39 7439-97-610/31/23 22:140.0488 0.0220 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/30/23 15:34 83-32-910/27/23 11:220.40 0.14 1
Acenaphthylene ND mg/kg 10/30/23 15:34 208-96-810/27/23 11:220.40 0.14 1
Acetophenone ND mg/kg 10/30/23 15:34 98-86-210/27/23 11:220.40 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-DUP Lab ID:92695355010 Collected:10/24/23 00:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Aniline ND mg/kg 10/30/23 15:34 62-53-310/27/23 11:220.40 0.16 1
Atrazine ND mg/kg 10/30/23 15:34 1912-24-910/27/23 11:220.40 0.13 1
Benzaldehyde ND mg/kg 10/30/23 15:34 100-52-710/27/23 11:220.40 0.13 1
Benzidine ND mg/kg 10/30/23 15:34 92-87-510/27/23 11:222.0 0.33 1
Benzo(a)anthracene ND mg/kg 10/30/23 15:34 56-55-310/27/23 11:220.40 0.13 1
Benzo(a)pyrene ND mg/kg 10/30/23 15:34 50-32-810/27/23 11:220.40 0.14 1
Benzo(b)fluoranthene ND mg/kg 10/30/23 15:34 205-99-210/27/23 11:220.40 0.13 1
Benzo(g,h,i)perylene ND mg/kg 10/30/23 15:34 191-24-210/27/23 11:220.40 0.15 1
Benzo(k)fluoranthene ND mg/kg 10/30/23 15:34 207-08-910/27/23 11:220.40 0.14 1
Benzoic Acid ND mg/kg 10/30/23 15:34 65-85-010/27/23 11:222.0 0.85 1
Benzophenone ND mg/kg 10/30/23 15:34 119-61-910/27/23 11:220.40 0.18 1
Benzyl alcohol ND mg/kg 10/30/23 15:34 100-51-610/27/23 11:220.79 0.30 1
Biphenyl (Diphenyl)ND mg/kg 10/30/23 15:34 92-52-410/27/23 11:220.40 0.094 1
4-Bromophenylphenyl ether ND mg/kg 10/30/23 15:34 101-55-310/27/23 11:220.40 0.15 1
Butylbenzylphthalate ND mg/kg 10/30/23 15:34 85-68-710/27/23 11:220.40 0.17 1
Caprolactam ND mg/kg 10/30/23 15:34 105-60-210/27/23 11:220.40 0.21 1
Carbazole ND mg/kg 10/30/23 15:34 86-74-810/27/23 11:220.40 0.14 1
4-Chloro-3-methylphenol ND mg/kg 10/30/23 15:34 59-50-710/27/23 11:220.79 0.28 1
4-Chloroaniline ND mg/kg 10/30/23 15:34 106-47-810/27/23 11:220.79 0.31 1
Chlorobenzilate ND mg/kg 10/30/23 15:34 510-15-610/27/23 11:220.40 0.078 1
bis(2-Chloroethoxy)methane ND mg/kg 10/30/23 15:34 111-91-110/27/23 11:220.40 0.16 1
bis(2-Chloroethyl) ether ND mg/kg 10/30/23 15:34 111-44-410/27/23 11:220.40 0.15 1
2-Chloronaphthalene ND mg/kg 10/30/23 15:34 91-58-710/27/23 11:220.40 0.16 1
2-Chlorophenol ND mg/kg 10/30/23 15:34 95-57-810/27/23 11:220.40 0.15 1
4-Chlorophenylphenyl ether ND mg/kg 10/30/23 15:34 7005-72-310/27/23 11:220.40 0.15 1
Chrysene ND mg/kg 10/30/23 15:34 218-01-910/27/23 11:220.40 0.14 1
Dibenz(a,h)anthracene ND mg/kg 10/30/23 15:34 53-70-310/27/23 11:220.40 0.15 1
Dibenzo(a,e)pyrene ND mg/kg 10/30/23 15:34 192-65-410/27/23 11:221.2 0.27 1
Dibenzofuran ND mg/kg 10/30/23 15:34 132-64-910/27/23 11:220.40 0.14 1
1,2-Dichlorobenzene ND mg/kg 10/30/23 15:34 95-50-110/27/23 11:220.40 0.14 1
1,3-Dichlorobenzene ND mg/kg 10/30/23 15:34 541-73-110/27/23 11:220.40 0.14 1
1,4-Dichlorobenzene ND mg/kg 10/30/23 15:34 106-46-710/27/23 11:220.40 0.15 1
3,3'-Dichlorobenzidine ND mg/kg 10/30/23 15:34 91-94-1 L210/27/23 11:220.79 0.27 1
2,4-Dichlorophenol ND mg/kg 10/30/23 15:34 120-83-210/27/23 11:220.40 0.16 1
2,6-Dichlorophenol ND mg/kg 10/30/23 15:34 87-65-0 L210/27/23 11:220.40 0.10 1
2,3-Dichloroaniline ND mg/kg 10/30/23 15:34 608-27-510/27/23 11:220.40 0.19 1
Diethylphthalate ND mg/kg 10/30/23 15:34 84-66-210/27/23 11:220.40 0.15 1
3,3'-Dimethylbenzidine ND mg/kg 10/30/23 15:34 119-93-7 IL10/27/23 11:220.79 0.35 1
2,4-Dimethylphenol ND mg/kg 10/30/23 15:34 105-67-910/27/23 11:220.40 0.16 1
Dimethylphthalate ND mg/kg 10/30/23 15:34 131-11-310/27/23 11:220.40 0.14 1
Di-n-butylphthalate ND mg/kg 10/30/23 15:34 84-74-210/27/23 11:220.40 0.13 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/30/23 15:34 534-52-110/27/23 11:220.79 0.37 1
1,3-Dinitrobenzene ND mg/kg 10/30/23 15:34 99-65-0 L210/27/23 11:220.40 0.089 1
1,4-Dinitrobenzene ND mg/kg 10/30/23 15:34 100-25-4 L210/27/23 11:220.40 0.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-DUP Lab ID:92695355010 Collected:10/24/23 00:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 10/30/23 15:34 51-28-510/27/23 11:222.0 1.2 1
2,4-Dinitrotoluene ND mg/kg 10/30/23 15:34 121-14-210/27/23 11:220.40 0.15 1
2,6-Dinitrotoluene ND mg/kg 10/30/23 15:34 606-20-210/27/23 11:220.40 0.15 1
Di-n-octylphthalate ND mg/kg 10/30/23 15:34 117-84-010/27/23 11:220.40 0.16 1
1,2-Diphenylhydrazine ND mg/kg 10/30/23 15:34 122-66-710/27/23 11:220.40 0.16 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/30/23 15:34 117-81-710/27/23 11:220.40 0.15 1
Fluoranthene ND mg/kg 10/30/23 15:34 206-44-010/27/23 11:220.40 0.14 1
Fluorene ND mg/kg 10/30/23 15:34 86-73-710/27/23 11:220.40 0.14 1
Hexachloro-1,3-butadiene ND mg/kg 10/30/23 15:34 87-68-310/27/23 11:220.40 0.17 1
Hexachlorobenzene ND mg/kg 10/30/23 15:34 118-74-110/27/23 11:220.40 0.16 1
Hexachlorocyclopentadiene ND mg/kg 10/30/23 15:34 77-47-410/27/23 11:220.40 0.23 1
Hexachloroethane ND mg/kg 10/30/23 15:34 67-72-110/27/23 11:220.40 0.15 1
Hexachlorophene ND mg/kg 10/30/23 15:34 70-30-4 IH,v210/27/23 11:224.0 2.3 1
Hexachloropropene ND mg/kg 10/30/23 15:34 1888-71-710/27/23 11:220.40 0.11 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/30/23 15:34 193-39-510/27/23 11:220.40 0.16 1
Isodrin ND mg/kg 10/30/23 15:34 465-73-610/27/23 11:220.40 0.094 1
1-Methylnaphthalene ND mg/kg 10/30/23 15:34 90-12-010/27/23 11:220.40 0.14 1
2-Methylnaphthalene ND mg/kg 10/30/23 15:34 91-57-610/27/23 11:220.40 0.16 1
2-Methyl-5-nitroaniline ND mg/kg 10/30/23 15:34 99-55-810/27/23 11:220.40 0.12 1
2-Methylphenol(o-Cresol)ND mg/kg 10/30/23 15:34 95-48-710/27/23 11:220.40 0.16 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/30/23 15:34 15831-10-410/27/23 11:220.40 0.16 1
1-Naphthalenamine ND mg/kg 10/30/23 15:34 134-32-710/27/23 11:220.79 0.13 1
2-Naphthalenamine ND mg/kg 10/30/23 15:34 91-59-810/27/23 11:220.79 0.15 1
Naphthalene ND mg/kg 10/30/23 15:34 91-20-310/27/23 11:220.40 0.13 1
2-Nitroaniline ND mg/kg 10/30/23 15:34 88-74-410/27/23 11:222.0 0.32 1
3-Nitroaniline ND mg/kg 10/30/23 15:34 99-09-210/27/23 11:222.0 0.31 1
4-Nitroaniline ND mg/kg 10/30/23 15:34 100-01-610/27/23 11:220.79 0.30 1
Nitrobenzene ND mg/kg 10/30/23 15:34 98-95-310/27/23 11:220.40 0.18 1
2-Nitrophenol ND mg/kg 10/30/23 15:34 88-75-510/27/23 11:220.40 0.17 1
4-Nitrophenol ND mg/kg 10/30/23 15:34 100-02-710/27/23 11:222.0 0.77 1
N-Nitroso-di-n-propylamine ND mg/kg 10/30/23 15:34 621-64-710/27/23 11:220.40 0.15 1
Pentachlorophenol ND mg/kg 10/30/23 15:34 87-86-510/27/23 11:220.79 0.39 1
Phenanthrene ND mg/kg 10/30/23 15:34 85-01-810/27/23 11:220.40 0.13 1
Phenol ND mg/kg 10/30/23 15:34 108-95-210/27/23 11:220.40 0.18 1
Pyrene ND mg/kg 10/30/23 15:34 129-00-010/27/23 11:220.40 0.16 1
Pyridine ND mg/kg 10/30/23 15:34 110-86-1 v110/27/23 11:220.40 0.12 1
1,2,4,5-Tetrachlorobenzene ND mg/kg 10/30/23 15:34 95-94-310/27/23 11:220.40 0.097 1
2,3,4,6-Tetrachlorophenol ND mg/kg 10/30/23 15:34 58-90-210/27/23 11:220.40 0.099 1
2,4,5-Trichlorophenol ND mg/kg 10/30/23 15:34 95-95-410/27/23 11:220.40 0.18 1
2,4,6-Trichlorophenol ND mg/kg 10/30/23 15:34 88-06-210/27/23 11:220.40 0.16 1
Surrogates
2-Fluorobiphenyl (S)47 %10/30/23 15:34 321-60-810/27/23 11:2210-130 1
Terphenyl-d14 (S)55 %10/30/23 15:34 1718-51-010/27/23 11:2210-130 1
Phenol-d6 (S)48 %10/30/23 15:34 13127-88-310/27/23 11:2210-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-DUP Lab ID:92695355010 Collected:10/24/23 00:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)50 %10/30/23 15:34 367-12-410/27/23 11:2210-130 1
2,4,6-Tribromophenol (S)45 %10/30/23 15:34 118-79-610/27/23 11:2210-130 1
Nitrobenzene-d5 (S)51 %10/30/23 15:34 4165-60-010/27/23 11:2210-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/27/23 22:58 67-64-110/27/23 14:400.14 0.045 1
Benzene ND mg/kg 10/27/23 22:58 71-43-210/27/23 14:400.0071 0.0028 1
Bromobenzene ND mg/kg 10/27/23 22:58 108-86-110/27/23 14:400.0071 0.0023 1
Bromochloromethane ND mg/kg 10/27/23 22:58 74-97-510/27/23 14:400.0071 0.0021 1
Bromodichloromethane ND mg/kg 10/27/23 22:58 75-27-410/27/23 14:400.0071 0.0027 1
Bromoform ND mg/kg 10/27/23 22:58 75-25-210/27/23 14:400.0071 0.0025 1
Bromomethane ND mg/kg 10/27/23 22:58 74-83-9 IK,v110/27/23 14:400.028 0.022 1
2-Butanone (MEK)ND mg/kg 10/27/23 22:58 78-93-310/27/23 14:400.14 0.034 1
n-Butylbenzene ND mg/kg 10/27/23 22:58 104-51-810/27/23 14:400.0071 0.0044 1
sec-Butylbenzene ND mg/kg 10/27/23 22:58 135-98-810/27/23 14:400.0071 0.0031 1
tert-Butylbenzene ND mg/kg 10/27/23 22:58 98-06-610/27/23 14:400.0071 0.0025 1
Carbon tetrachloride ND mg/kg 10/27/23 22:58 56-23-510/27/23 14:400.0071 0.0026 1
Chlorobenzene ND mg/kg 10/27/23 22:58 108-90-710/27/23 14:400.0071 0.0041 1
Chloroethane ND mg/kg 10/27/23 22:58 75-00-310/27/23 14:400.014 0.0054 1
Chloroform ND mg/kg 10/27/23 22:58 67-66-310/27/23 14:400.0071 0.0059 1
Chloromethane ND mg/kg 10/27/23 22:58 74-87-310/27/23 14:400.014 0.0059 1
2-Chlorotoluene ND mg/kg 10/27/23 22:58 95-49-810/27/23 14:400.0071 0.0025 1
4-Chlorotoluene ND mg/kg 10/27/23 22:58 106-43-410/27/23 14:400.0071 0.0039 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/27/23 22:58 96-12-810/27/23 14:400.0071 0.0027 1
Dibromochloromethane ND mg/kg 10/27/23 22:58 124-48-110/27/23 14:400.0071 0.0040 1
1,2-Dibromoethane (EDB)ND mg/kg 10/27/23 22:58 106-93-410/27/23 14:400.0071 0.0031 1
Dibromomethane ND mg/kg 10/27/23 22:58 74-95-310/27/23 14:400.0071 0.0015 1
1,2-Dichlorobenzene ND mg/kg 10/27/23 22:58 95-50-110/27/23 14:400.0071 0.0025 1
1,3-Dichlorobenzene ND mg/kg 10/27/23 22:58 541-73-110/27/23 14:400.0071 0.0022 1
1,4-Dichlorobenzene ND mg/kg 10/27/23 22:58 106-46-710/27/23 14:400.0071 0.0018 1
Dichlorodifluoromethane ND mg/kg 10/27/23 22:58 75-71-810/27/23 14:400.014 0.0072 1
1,1-Dichloroethane ND mg/kg 10/27/23 22:58 75-34-310/27/23 14:400.0071 0.0029 1
1,2-Dichloroethane ND mg/kg 10/27/23 22:58 107-06-210/27/23 14:400.0071 0.0047 1
1,1-Dichloroethene ND mg/kg 10/27/23 22:58 75-35-410/27/23 14:400.0071 0.0029 1
cis-1,2-Dichloroethene ND mg/kg 10/27/23 22:58 156-59-210/27/23 14:400.0071 0.0024 1
trans-1,2-Dichloroethene ND mg/kg 10/27/23 22:58 156-60-510/27/23 14:400.0071 0.0060 1
1,2-Dichloropropane ND mg/kg 10/27/23 22:58 78-87-510/27/23 14:400.0071 0.0021 1
1,3-Dichloropropane ND mg/kg 10/27/23 22:58 142-28-910/27/23 14:400.0071 0.0022 1
2,2-Dichloropropane ND mg/kg 10/27/23 22:58 594-20-710/27/23 14:400.0071 0.0053 1
1,1-Dichloropropene ND mg/kg 10/27/23 22:58 563-58-610/27/23 14:400.0071 0.0034 1
cis-1,3-Dichloropropene ND mg/kg 10/27/23 22:58 10061-01-510/27/23 14:400.0071 0.0019 1
trans-1,3-Dichloropropene ND mg/kg 10/27/23 22:58 10061-02-610/27/23 14:400.0071 0.0024 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 88
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Sample:SB-DUP Lab ID:92695355010 Collected:10/24/23 00:00 Received:10/25/23 07:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Diisopropyl ether ND mg/kg 10/27/23 22:58 108-20-310/27/23 14:400.0071 0.0019 1
Ethylbenzene 0.030 mg/kg 10/27/23 22:58 100-41-410/27/23 14:400.0071 0.0033 1
Hexachloro-1,3-butadiene ND mg/kg 10/27/23 22:58 87-68-310/27/23 14:400.014 0.012 1
2-Hexanone ND mg/kg 10/27/23 22:58 591-78-610/27/23 14:400.071 0.0068 1
Isopropylbenzene (Cumene)ND mg/kg 10/27/23 22:58 98-82-810/27/23 14:400.0071 0.0024 1
p-Isopropyltoluene ND mg/kg 10/27/23 22:58 99-87-610/27/23 14:400.0071 0.0035 1
Methylene Chloride ND mg/kg 10/27/23 22:58 75-09-210/27/23 14:400.028 0.019 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/27/23 22:58 108-10-110/27/23 14:400.071 0.0068 1
Methyl-tert-butyl ether ND mg/kg 10/27/23 22:58 1634-04-410/27/23 14:400.0071 0.0026 1
Naphthalene ND mg/kg 10/27/23 22:58 91-20-310/27/23 14:400.0071 0.0037 1
n-Propylbenzene ND mg/kg 10/27/23 22:58 103-65-110/27/23 14:400.0071 0.0025 1
Styrene ND mg/kg 10/27/23 22:58 100-42-510/27/23 14:400.0071 0.0019 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/27/23 22:58 630-20-610/27/23 14:400.0071 0.0027 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/27/23 22:58 79-34-510/27/23 14:400.0071 0.0019 1
Tetrachloroethene ND mg/kg 10/27/23 22:58 127-18-410/27/23 14:400.0071 0.0022 1
Toluene 0.84 mg/kg 10/27/23 22:58 108-88-310/27/23 14:400.0071 0.0049 1
1,2,3-Trichlorobenzene ND mg/kg 10/27/23 22:58 87-61-610/27/23 14:400.0071 0.0057 1
1,2,4-Trichlorobenzene ND mg/kg 10/27/23 22:58 120-82-110/27/23 14:400.0071 0.0059 1
1,1,1-Trichloroethane ND mg/kg 10/27/23 22:58 71-55-610/27/23 14:400.0071 0.0037 1
1,1,2-Trichloroethane ND mg/kg 10/27/23 22:58 79-00-510/27/23 14:400.0071 0.0023 1
Trichloroethene ND mg/kg 10/27/23 22:58 79-01-610/27/23 14:400.0071 0.0057 1
Trichlorofluoromethane ND mg/kg 10/27/23 22:58 75-69-410/27/23 14:400.0071 0.0039 1
1,2,3-Trichloropropane ND mg/kg 10/27/23 22:58 96-18-410/27/23 14:400.0071 0.0036 1
1,2,4-Trimethylbenzene 0.0051J mg/kg 10/27/23 22:58 95-63-610/27/23 14:400.0071 0.0042 1
1,3,5-Trimethylbenzene ND mg/kg 10/27/23 22:58 108-67-810/27/23 14:400.0071 0.0024 1
Vinyl acetate ND mg/kg 10/27/23 22:58 108-05-410/27/23 14:400.071 0.015 1
Vinyl chloride ND mg/kg 10/27/23 22:58 75-01-410/27/23 14:400.014 0.0036 1
Xylene (Total)0.17 mg/kg 10/27/23 22:58 1330-20-710/27/23 14:400.014 0.0040 1
m&p-Xylene 0.12 mg/kg 10/27/23 22:58 179601-23-110/27/23 14:400.014 0.0048 1
o-Xylene 0.054 mg/kg 10/27/23 22:58 95-47-610/27/23 14:400.0071 0.0031 1
Surrogates
Toluene-d8 (S)100 %10/27/23 22:58 2037-26-510/27/23 14:4070-130 1
4-Bromofluorobenzene (S)102 %10/27/23 22:58 460-00-410/27/23 14:4070-130 1
1,2-Dichloroethane-d4 (S)101 %10/27/23 22:58 17060-07-010/27/23 14:4070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.1 %10/26/23 18:54 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 82.0 %11/01/23 10:1411/01/23 10:091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2161880
3050B
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008, 92695355009, 92695355010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3994493-1
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008, 92695355009, 92695355010
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 1.00 11/02/23 11:330.100
Barium mg/kg ND 2.50 11/02/23 11:330.152
Cadmium mg/kg ND 1.00 11/02/23 11:330.0855
Chromium mg/kg ND 5.00 11/02/23 11:330.297
Lead mg/kg ND 2.00 11/02/23 11:330.0990
Selenium mg/kg ND 2.50 11/02/23 11:330.180
Silver mg/kg ND 0.500 11/02/23 11:330.0865
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3994493-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 94.9100 94.9 80.0-120
Barium mg/kg 86.4100 86.4 80.0-120
Cadmium mg/kg 97.3100 97.3 80.0-120
Chromium mg/kg 94.4100 94.4 80.0-120
Lead mg/kg 88.5100 88.5 80.0-120
Selenium mg/kg 105100 105 80.0-120
Silver mg/kg 18.820.0 93.8 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3994493-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1671516-01
R3994493-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 100 83.9 75.0-12593.9 8.40 2010030.5 114 124
Barium mg/kg 100 80.6 75.0-125103 4.63 20100401482504
Cadmium mg/kg 100 95.4 75.0-125106 10.5 201000.698 96.0 107
Chromium mg/kg 100 86.9 75.0-12599.8 10.4 2010031.0 118 131
Lead mg/kg 100 87.9 75.0-125100 10.4 2010023.7 112 124
Selenium mg/kg 100 101 75.0-125113 11.2 201001.20 102 114
Silver mg/kg 20.0 93.8 75.0-125103 9.17 2020.00.145 18.9 20.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2161803
7471A
EPA 7471B
Mercury 7471B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008, 92695355009, 92695355010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3994207-1
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008, 92695355009, 92695355010
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0400 11/01/23 17:510.0180
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3994207-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.4850.500 97.1 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3994207-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1671862-04
R3994207-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.500 87.9 75.0-12586.4 1.13 200.5000.218 0.657 0.650
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
809251
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92695355001, 92695355005, 92695355006, 92695355007, 92695355008, 92695355009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4190558
Associated Lab Samples:92695355001, 92695355005, 92695355006, 92695355007, 92695355008, 92695355009
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 10/27/23 15:180.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 10/27/23 15:180.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 10/27/23 15:180.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 10/27/23 15:180.0017
1,1-Dichloroethane mg/kg ND 0.0050 10/27/23 15:180.0021
1,1-Dichloroethene mg/kg ND 0.0050 10/27/23 15:180.0021
1,1-Dichloropropene mg/kg ND 0.0050 10/27/23 15:180.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 10/27/23 15:180.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 10/27/23 15:180.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 10/27/23 15:180.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 10/27/23 15:180.0030
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 10/27/23 15:180.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 10/27/23 15:180.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 10/27/23 15:180.0018
1,2-Dichloroethane mg/kg ND 0.0050 10/27/23 15:180.0033
1,2-Dichloropropane mg/kg ND 0.0050 10/27/23 15:180.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 10/27/23 15:180.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 10/27/23 15:180.0016
1,3-Dichloropropane mg/kg ND 0.0050 10/27/23 15:180.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 10/27/23 15:180.0013
2,2-Dichloropropane mg/kg ND 0.0050 10/27/23 15:180.0038
2-Butanone (MEK)mg/kg ND 0.10 10/27/23 15:180.024
2-Chlorotoluene mg/kg ND 0.0050 10/27/23 15:180.0018
2-Hexanone mg/kg ND 0.050 10/27/23 15:180.0048
4-Chlorotoluene mg/kg ND 0.0050 10/27/23 15:180.0028
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 10/27/23 15:180.0048
Acetone mg/kg ND 0.10 10/27/23 15:180.032
Benzene mg/kg ND 0.0050 10/27/23 15:180.0020
Bromobenzene mg/kg ND 0.0050 10/27/23 15:180.0016
Bromochloromethane mg/kg ND 0.0050 10/27/23 15:180.0015
Bromodichloromethane mg/kg ND 0.0050 10/27/23 15:180.0019
Bromoform mg/kg ND 0.0050 10/27/23 15:180.0018
Bromomethane mg/kg ND 0.020 IK,v110/27/23 15:180.016
Carbon tetrachloride mg/kg ND 0.0050 10/27/23 15:180.0019
Chlorobenzene mg/kg ND 0.0050 10/27/23 15:180.0029
Chloroethane mg/kg ND 0.010 10/27/23 15:180.0039
Chloroform mg/kg ND 0.0050 10/27/23 15:180.0042
Chloromethane mg/kg ND 0.010 10/27/23 15:180.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 10/27/23 15:180.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 10/27/23 15:180.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4190558
Associated Lab Samples:92695355001, 92695355005, 92695355006, 92695355007, 92695355008, 92695355009
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 10/27/23 15:180.0028
Dibromomethane mg/kg ND 0.0050 10/27/23 15:180.0011
Dichlorodifluoromethane mg/kg ND 0.010 10/27/23 15:180.0051
Diisopropyl ether mg/kg ND 0.0050 10/27/23 15:180.0014
Ethylbenzene mg/kg ND 0.0050 10/27/23 15:180.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 10/27/23 15:180.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 10/27/23 15:180.0017
m&p-Xylene mg/kg ND 0.010 10/27/23 15:180.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 10/27/23 15:180.0019
Methylene Chloride mg/kg ND 0.020 10/27/23 15:180.014
n-Butylbenzene mg/kg ND 0.0050 10/27/23 15:180.0032
n-Propylbenzene mg/kg ND 0.0050 10/27/23 15:180.0018
Naphthalene mg/kg ND 0.0050 10/27/23 15:180.0026
o-Xylene mg/kg ND 0.0050 10/27/23 15:180.0022
p-Isopropyltoluene mg/kg ND 0.0050 10/27/23 15:180.0025
sec-Butylbenzene mg/kg ND 0.0050 10/27/23 15:180.0022
Styrene mg/kg ND 0.0050 10/27/23 15:180.0013
tert-Butylbenzene mg/kg ND 0.0050 10/27/23 15:180.0018
Tetrachloroethene mg/kg ND 0.0050 10/27/23 15:180.0016
Toluene mg/kg ND 0.0050 10/27/23 15:180.0034
trans-1,2-Dichloroethene mg/kg ND 0.0050 10/27/23 15:180.0042
trans-1,3-Dichloropropene mg/kg ND 0.0050 10/27/23 15:180.0017
Trichloroethene mg/kg ND 0.0050 10/27/23 15:180.0040
Trichlorofluoromethane mg/kg ND 0.0050 10/27/23 15:180.0028
Vinyl acetate mg/kg ND 0.050 10/27/23 15:180.010
Vinyl chloride mg/kg ND 0.010 10/27/23 15:180.0025
Xylene (Total)mg/kg ND 0.010 10/27/23 15:180.0028
1,2-Dichloroethane-d4 (S)%106 70-130 10/27/23 15:18
4-Bromofluorobenzene (S)%98 70-130 10/27/23 15:18
Toluene-d8 (S)%100 70-130 10/27/23 15:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4190559LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.500.5 100 70-130
1,1,1-Trichloroethane mg/kg 0.510.5 102 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.500.5 100 70-130
1,1,2-Trichloroethane mg/kg 0.500.5 101 70-130
1,1-Dichloroethane mg/kg 0.510.5 102 70-130
1,1-Dichloroethene mg/kg 0.520.5 105 70-132
1,1-Dichloropropene mg/kg 0.520.5 104 70-130
1,2,3-Trichlorobenzene mg/kg 0.520.5 104 62-136
1,2,3-Trichloropropane mg/kg 0.490.5 99 70-130
1,2,4-Trichlorobenzene mg/kg 0.460.5 93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4190559LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 0.500.5 100 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.460.5 92 65-130
1,2-Dibromoethane (EDB)mg/kg 0.510.5 102 70-130
1,2-Dichlorobenzene mg/kg 0.480.5 97 70-130
1,2-Dichloroethane mg/kg 0.510.5 103 70-130
1,2-Dichloropropane mg/kg 0.500.5 100 70-130
1,3,5-Trimethylbenzene mg/kg 0.500.5 100 70-130
1,3-Dichlorobenzene mg/kg 0.490.5 98 70-130
1,3-Dichloropropane mg/kg 0.490.5 98 70-130
1,4-Dichlorobenzene mg/kg 0.470.5 93 70-130
2,2-Dichloropropane mg/kg 0.460.5 93 60-130
2-Butanone (MEK)mg/kg 0.991 99 66-130
2-Chlorotoluene mg/kg 0.500.5 100 70-130
2-Hexanone mg/kg 1.01 103 68-130
4-Chlorotoluene mg/kg 0.500.5 99 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 1.01 102 70-130
Acetone mg/kg 0.971 97 60-130
Benzene mg/kg 0.500.5 100 70-130
Bromobenzene mg/kg 0.480.5 97 70-130
Bromochloromethane mg/kg 0.510.5 103 70-130
Bromodichloromethane mg/kg 0.500.5 99 70-130
Bromoform mg/kg 0.490.5 97 70-130
Bromomethane mg/kg 0.67 IK,v10.5 133 43-175
Carbon tetrachloride mg/kg 0.510.5 102 70-130
Chlorobenzene mg/kg 0.490.5 98 70-130
Chloroethane mg/kg 0.580.5 116 70-145
Chloroform mg/kg 0.500.5 100 70-130
Chloromethane mg/kg 0.610.5 123 66-146
cis-1,2-Dichloroethene mg/kg 0.510.5 102 70-130
cis-1,3-Dichloropropene mg/kg 0.460.5 92 70-130
Dibromochloromethane mg/kg 0.500.5 100 70-130
Dibromomethane mg/kg 0.510.5 102 70-130
Dichlorodifluoromethane mg/kg 0.560.5 112 42-197
Diisopropyl ether mg/kg 0.500.5 100 68-130
Ethylbenzene mg/kg 0.460.5 92 70-130
Hexachloro-1,3-butadiene mg/kg 0.480.5 95 70-130
Isopropylbenzene (Cumene)mg/kg 0.500.5 101 70-130
m&p-Xylene mg/kg 1.01 100 70-130
Methyl-tert-butyl ether mg/kg 0.470.5 94 70-130
Methylene Chloride mg/kg 0.510.5 103 65-130
n-Butylbenzene mg/kg 0.490.5 99 70-130
n-Propylbenzene mg/kg 0.490.5 98 70-130
Naphthalene mg/kg 0.510.5 102 65-135
o-Xylene mg/kg 0.510.5 102 70-130
p-Isopropyltoluene mg/kg 0.500.5 100 70-130
sec-Butylbenzene mg/kg 0.490.5 97 70-130
Styrene mg/kg 0.520.5 104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4190559LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 0.500.5 100 70-130
Tetrachloroethene mg/kg 0.510.5 103 70-130
Toluene mg/kg 0.490.5 98 70-130
trans-1,2-Dichloroethene mg/kg 0.540.5 109 70-130
trans-1,3-Dichloropropene mg/kg 0.520.5 103 70-130
Trichloroethene mg/kg 0.520.5 105 70-130
Trichlorofluoromethane mg/kg 0.560.5 112 62-140
Vinyl acetate mg/kg 1.01 103 70-140
Vinyl chloride mg/kg 0.540.5 107 70-152
Xylene (Total)mg/kg 1.51.5 101 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4190560MATRIX SPIKE SAMPLE:
MSSpike
Result
92695390018
1,1,1,2-Tetrachloroethane mg/kg 0.360.68 53 22-166ND
1,1,1-Trichloroethane mg/kg 0.380.68 56 23-172ND
1,1,2,2-Tetrachloroethane mg/kg 0.350.68 52 21-158ND
1,1,2-Trichloroethane mg/kg 0.400.68 59 25-160ND
1,1-Dichloroethane mg/kg 0.380.68 55 22-166ND
1,1-Dichloroethene mg/kg 0.400.68 59 18-183ND
1,1-Dichloropropene mg/kg 0.390.68 57 20-181ND
1,2,3-Trichlorobenzene mg/kg 0.160.68 24 10-161ND
1,2,3-Trichloropropane mg/kg 0.350.68 52 21-147ND
1,2,4-Trichlorobenzene mg/kg 0.230.68 33 10-159ND
1,2,4-Trimethylbenzene mg/kg 0.340.68 50 17-170ND
1,2-Dibromo-3-chloropropane mg/kg 0.280.68 42 10-135ND
1,2-Dibromoethane (EDB)mg/kg 0.380.68 56 30-154ND
1,2-Dichlorobenzene mg/kg 0.330.68 49 26-162ND
1,2-Dichloroethane mg/kg 0.390.68 58 23-161ND
1,2-Dichloropropane mg/kg 0.400.68 58 29-165ND
1,3,5-Trimethylbenzene mg/kg 0.340.68 50 20-172ND
1,3-Dichlorobenzene mg/kg 0.340.68 49 22-164ND
1,3-Dichloropropane mg/kg 0.380.68 56 27-156ND
1,4-Dichlorobenzene mg/kg 0.320.68 47 20-161ND
2,2-Dichloropropane mg/kg 0.330.68 49 10-159ND
2-Butanone (MEK)mg/kg 0.731.4 54 13-143ND
2-Chlorotoluene mg/kg 0.350.68 51 21-166ND
2-Hexanone mg/kg 0.681.4 50 19-145ND
4-Chlorotoluene mg/kg 0.340.68 51 19-163ND
4-Methyl-2-pentanone (MIBK)mg/kg 0.391.4 28 21-151ND
Acetone mg/kg 0.551.4 40 10-133ND
Benzene mg/kg 0.390.68 57 29-156ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4190560MATRIX SPIKE SAMPLE:
MSSpike
Result
92695390018
Bromobenzene mg/kg 0.340.68 50 25-161ND
Bromochloromethane mg/kg 0.390.68 57 27-158ND
Bromodichloromethane mg/kg 0.380.68 55 23-158ND
Bromoform mg/kg 0.350.68 51 19-152ND
Bromomethane mg/kg ND IK,M1,v10.68 0 10-152ND
Carbon tetrachloride mg/kg 0.380.68 55 18-172ND
Chlorobenzene mg/kg 0.350.68 51 26-166ND
Chloroethane mg/kg 0.0810.68 12 10-130ND
Chloroform mg/kg 0.390.68 57 25-161ND
Chloromethane mg/kg 0.540.68 79 27-197ND
cis-1,2-Dichloroethene mg/kg 0.400.68 59 28-165ND
cis-1,3-Dichloropropene mg/kg 0.350.68 51 23-159ND
Dibromochloromethane mg/kg 0.360.68 53 21-151ND
Dibromomethane mg/kg 0.400.68 59 38-158ND
Dichlorodifluoromethane mg/kg 0.490.68 72 10-200ND
Diisopropyl ether mg/kg 0.380.68 56 23-160ND
Ethylbenzene mg/kg 0.330.68 47 22-1636.5J ug/kg
Hexachloro-1,3-butadiene mg/kg 0.300.68 43 10-192ND
Isopropylbenzene (Cumene)mg/kg 0.350.68 52 24-173ND
m&p-Xylene mg/kg 0.691.4 50 22-1715.3J ug/kg
Methyl-tert-butyl ether mg/kg 0.350.68 51 25-153ND
Methylene Chloride mg/kg 0.400.68 59 10-165ND
n-Butylbenzene mg/kg 0.320.68 46 10-18612.2 ug/kg
n-Propylbenzene mg/kg 0.340.68 50 16-1713.8J ug/kg
Naphthalene mg/kg 0.180.68 25 10-1598.7 ug/kg
o-Xylene mg/kg 0.350.68 51 23-171ND
p-Isopropyltoluene mg/kg 0.340.68 49 13-1846.0J ug/kg
sec-Butylbenzene mg/kg 0.340.68 49 16-18210.4 ug/kg
Styrene mg/kg 0.350.68 51 25-169ND
tert-Butylbenzene mg/kg 0.330.68 49 20-174ND
Tetrachloroethene mg/kg 0.320.68 47 14-171ND
Toluene mg/kg 0.370.68 53 24-166ND
trans-1,2-Dichloroethene mg/kg 0.380.68 56 24-170ND
trans-1,3-Dichloropropene mg/kg 0.380.68 56 22-157ND
Trichloroethene mg/kg 0.380.68 56 23-176ND
Trichlorofluoromethane mg/kg 0.0670.68 10 10-138ND
Vinyl acetate mg/kg 0.761.4 56 11-166ND
Vinyl chloride mg/kg 0.480.68 70 21-200ND
Xylene (Total)mg/kg 1.02.1 51 23-1705.3J ug/kg
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92695390019
4190561SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND IK,v130ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg 0.0068J 308.1J ug/kg
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92695390019
4190561SAMPLE DUPLICATE:
m&p-Xylene mg/kg 0.0062J 307.8J ug/kg
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 307.8J ug/kg
1,2-Dichloroethane-d4 (S)%102102
4-Bromofluorobenzene (S)%102101
Toluene-d8 (S)%99100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
809454
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92695355002, 92695355003, 92695355004, 92695355010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4191314
Associated Lab Samples:92695355002, 92695355003, 92695355004, 92695355010
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 10/27/23 14:590.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 10/27/23 14:590.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 10/27/23 14:590.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 10/27/23 14:590.0017
1,1-Dichloroethane mg/kg ND 0.0050 10/27/23 14:590.0021
1,1-Dichloroethene mg/kg ND 0.0050 10/27/23 14:590.0021
1,1-Dichloropropene mg/kg ND 0.0050 10/27/23 14:590.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 10/27/23 14:590.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 10/27/23 14:590.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 10/27/23 14:590.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 10/27/23 14:590.0030
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 10/27/23 14:590.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 10/27/23 14:590.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 10/27/23 14:590.0018
1,2-Dichloroethane mg/kg ND 0.0050 10/27/23 14:590.0033
1,2-Dichloropropane mg/kg ND 0.0050 10/27/23 14:590.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 10/27/23 14:590.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 10/27/23 14:590.0016
1,3-Dichloropropane mg/kg ND 0.0050 10/27/23 14:590.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 10/27/23 14:590.0013
2,2-Dichloropropane mg/kg ND 0.0050 10/27/23 14:590.0038
2-Butanone (MEK)mg/kg ND 0.10 10/27/23 14:590.024
2-Chlorotoluene mg/kg ND 0.0050 10/27/23 14:590.0018
2-Hexanone mg/kg ND 0.050 10/27/23 14:590.0048
4-Chlorotoluene mg/kg ND 0.0050 10/27/23 14:590.0028
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 10/27/23 14:590.0048
Acetone mg/kg ND 0.10 10/27/23 14:590.032
Benzene mg/kg ND 0.0050 10/27/23 14:590.0020
Bromobenzene mg/kg ND 0.0050 10/27/23 14:590.0016
Bromochloromethane mg/kg ND 0.0050 10/27/23 14:590.0015
Bromodichloromethane mg/kg ND 0.0050 10/27/23 14:590.0019
Bromoform mg/kg ND 0.0050 10/27/23 14:590.0018
Bromomethane mg/kg ND 0.020 IK,v110/27/23 14:590.016
Carbon tetrachloride mg/kg ND 0.0050 10/27/23 14:590.0019
Chlorobenzene mg/kg ND 0.0050 10/27/23 14:590.0029
Chloroethane mg/kg ND 0.010 10/27/23 14:590.0039
Chloroform mg/kg ND 0.0050 10/27/23 14:590.0042
Chloromethane mg/kg ND 0.010 10/27/23 14:590.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 10/27/23 14:590.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 10/27/23 14:590.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4191314
Associated Lab Samples:92695355002, 92695355003, 92695355004, 92695355010
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 10/27/23 14:590.0028
Dibromomethane mg/kg ND 0.0050 10/27/23 14:590.0011
Dichlorodifluoromethane mg/kg ND 0.010 10/27/23 14:590.0051
Diisopropyl ether mg/kg ND 0.0050 10/27/23 14:590.0014
Ethylbenzene mg/kg ND 0.0050 10/27/23 14:590.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 10/27/23 14:590.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 10/27/23 14:590.0017
m&p-Xylene mg/kg ND 0.010 10/27/23 14:590.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 10/27/23 14:590.0019
Methylene Chloride mg/kg ND 0.020 10/27/23 14:590.014
n-Butylbenzene mg/kg ND 0.0050 10/27/23 14:590.0032
n-Propylbenzene mg/kg ND 0.0050 10/27/23 14:590.0018
Naphthalene mg/kg ND 0.0050 10/27/23 14:590.0026
o-Xylene mg/kg ND 0.0050 10/27/23 14:590.0022
p-Isopropyltoluene mg/kg ND 0.0050 10/27/23 14:590.0025
sec-Butylbenzene mg/kg ND 0.0050 10/27/23 14:590.0022
Styrene mg/kg ND 0.0050 10/27/23 14:590.0013
tert-Butylbenzene mg/kg ND 0.0050 10/27/23 14:590.0018
Tetrachloroethene mg/kg ND 0.0050 10/27/23 14:590.0016
Toluene mg/kg ND 0.0050 10/27/23 14:590.0034
trans-1,2-Dichloroethene mg/kg ND 0.0050 10/27/23 14:590.0042
trans-1,3-Dichloropropene mg/kg ND 0.0050 10/27/23 14:590.0017
Trichloroethene mg/kg ND 0.0050 10/27/23 14:590.0040
Trichlorofluoromethane mg/kg ND 0.0050 10/27/23 14:590.0028
Vinyl acetate mg/kg ND 0.050 10/27/23 14:590.010
Vinyl chloride mg/kg ND 0.010 10/27/23 14:590.0025
Xylene (Total)mg/kg ND 0.010 10/27/23 14:590.0028
1,2-Dichloroethane-d4 (S)%106 70-130 10/27/23 14:59
4-Bromofluorobenzene (S)%99 70-130 10/27/23 14:59
Toluene-d8 (S)%99 70-130 10/27/23 14:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4191315LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.510.5 101 70-130
1,1,1-Trichloroethane mg/kg 0.500.5 99 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.510.5 101 70-130
1,1,2-Trichloroethane mg/kg 0.510.5 103 70-130
1,1-Dichloroethane mg/kg 0.500.5 100 70-130
1,1-Dichloroethene mg/kg 0.520.5 103 70-132
1,1-Dichloropropene mg/kg 0.510.5 102 70-130
1,2,3-Trichlorobenzene mg/kg 0.530.5 107 62-136
1,2,3-Trichloropropane mg/kg 0.510.5 101 70-130
1,2,4-Trichlorobenzene mg/kg 0.460.5 93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4191315LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 0.500.5 100 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.480.5 96 65-130
1,2-Dibromoethane (EDB)mg/kg 0.510.5 102 70-130
1,2-Dichlorobenzene mg/kg 0.480.5 96 70-130
1,2-Dichloroethane mg/kg 0.500.5 100 70-130
1,2-Dichloropropane mg/kg 0.500.5 100 70-130
1,3,5-Trimethylbenzene mg/kg 0.490.5 99 70-130
1,3-Dichlorobenzene mg/kg 0.480.5 96 70-130
1,3-Dichloropropane mg/kg 0.500.5 99 70-130
1,4-Dichlorobenzene mg/kg 0.470.5 94 70-130
2,2-Dichloropropane mg/kg 0.450.5 91 60-130
2-Butanone (MEK)mg/kg 1.01 102 66-130
2-Chlorotoluene mg/kg 0.500.5 99 70-130
2-Hexanone mg/kg 1.11 107 68-130
4-Chlorotoluene mg/kg 0.490.5 98 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 1.11 105 70-130
Acetone mg/kg 0.981 98 60-130
Benzene mg/kg 0.500.5 99 70-130
Bromobenzene mg/kg 0.470.5 95 70-130
Bromochloromethane mg/kg 0.510.5 101 70-130
Bromodichloromethane mg/kg 0.500.5 100 70-130
Bromoform mg/kg 0.500.5 100 70-130
Bromomethane mg/kg 0.61 IK,v10.5 121 43-175
Carbon tetrachloride mg/kg 0.510.5 102 70-130
Chlorobenzene mg/kg 0.490.5 98 70-130
Chloroethane mg/kg 0.570.5 113 70-145
Chloroform mg/kg 0.490.5 98 70-130
Chloromethane mg/kg 0.600.5 120 66-146
cis-1,2-Dichloroethene mg/kg 0.500.5 99 70-130
cis-1,3-Dichloropropene mg/kg 0.460.5 92 70-130
Dibromochloromethane mg/kg 0.500.5 100 70-130
Dibromomethane mg/kg 0.510.5 102 70-130
Dichlorodifluoromethane mg/kg 0.530.5 107 42-197
Diisopropyl ether mg/kg 0.490.5 98 68-130
Ethylbenzene mg/kg 0.460.5 92 70-130
Hexachloro-1,3-butadiene mg/kg 0.480.5 97 70-130
Isopropylbenzene (Cumene)mg/kg 0.510.5 102 70-130
m&p-Xylene mg/kg 1.01 100 70-130
Methyl-tert-butyl ether mg/kg 0.460.5 93 70-130
Methylene Chloride mg/kg 0.500.5 101 65-130
n-Butylbenzene mg/kg 0.490.5 98 70-130
n-Propylbenzene mg/kg 0.490.5 97 70-130
Naphthalene mg/kg 0.520.5 104 65-135
o-Xylene mg/kg 0.510.5 101 70-130
p-Isopropyltoluene mg/kg 0.500.5 100 70-130
sec-Butylbenzene mg/kg 0.490.5 97 70-130
Styrene mg/kg 0.520.5 104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4191315LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 0.600.5 121 70-130
Tetrachloroethene mg/kg 0.510.5 102 70-130
Toluene mg/kg 0.490.5 97 70-130
trans-1,2-Dichloroethene mg/kg 0.520.5 103 70-130
trans-1,3-Dichloropropene mg/kg 0.510.5 101 70-130
Trichloroethene mg/kg 0.510.5 102 70-130
Trichlorofluoromethane mg/kg 0.530.5 107 62-140
Vinyl acetate mg/kg 1.01 102 70-140
Vinyl chloride mg/kg 0.540.5 108 70-152
Xylene (Total)mg/kg 1.51.5 101 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4191316MATRIX SPIKE SAMPLE:
MSSpike
Result
92695355002
1,1,1,2-Tetrachloroethane mg/kg 0.056 M10.34 17 22-166ND
1,1,1-Trichloroethane mg/kg 0.053 M10.34 16 23-172ND
1,1,2,2-Tetrachloroethane mg/kg 0.054 M10.34 16 21-158ND
1,1,2-Trichloroethane mg/kg 0.057 M10.34 17 25-160ND
1,1-Dichloroethane mg/kg 0.054 M10.34 16 22-166ND
1,1-Dichloroethene mg/kg 0.054 M10.34 16 18-183ND
1,1-Dichloropropene mg/kg 0.055 M10.34 16 20-181ND
1,2,3-Trichlorobenzene mg/kg 0.027 M10.34 8 10-161ND
1,2,3-Trichloropropane mg/kg 0.052 M10.34 15 21-147ND
1,2,4-Trichlorobenzene mg/kg 0.0390.34 11 10-159ND
1,2,4-Trimethylbenzene mg/kg 0.0590.34 17 17-170ND
1,2-Dibromo-3-chloropropane mg/kg 0.0470.34 14 10-135ND
1,2-Dibromoethane (EDB)mg/kg 0.055 M10.34 16 30-154ND
1,2-Dichlorobenzene mg/kg 0.061 M10.34 18 26-162ND
1,2-Dichloroethane mg/kg 0.055 M10.34 16 23-161ND
1,2-Dichloropropane mg/kg 0.054 M10.34 16 29-165ND
1,3,5-Trimethylbenzene mg/kg 0.057 M10.34 17 20-172ND
1,3-Dichlorobenzene mg/kg 0.060 M10.34 18 22-164ND
1,3-Dichloropropane mg/kg 0.052 M10.34 15 27-156ND
1,4-Dichlorobenzene mg/kg 0.056 M10.34 17 20-161ND
2,2-Dichloropropane mg/kg 0.0520.34 15 10-159ND
2-Butanone (MEK)mg/kg 0.11J0.68 16 13-143ND
2-Chlorotoluene mg/kg 0.059 M10.34 17 21-166ND
2-Hexanone mg/kg 0.094 M10.68 14 19-145ND
4-Chlorotoluene mg/kg 0.057 M10.34 17 19-163ND
4-Methyl-2-pentanone (MIBK)mg/kg 0.11 M10.68 16 21-151ND
Acetone mg/kg 0.071J0.68 11 10-133ND
Benzene mg/kg 0.055 M10.34 16 29-156ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4191316MATRIX SPIKE SAMPLE:
MSSpike
Result
92695355002
Bromobenzene mg/kg 0.057 M10.34 17 25-161ND
Bromochloromethane mg/kg 0.054 M10.34 16 27-158ND
Bromodichloromethane mg/kg 0.050 M10.34 15 23-158ND
Bromoform mg/kg 0.050 M10.34 15 19-152ND
Bromomethane mg/kg ND IK,M1,v10.34 0 10-152ND
Carbon tetrachloride mg/kg 0.052 M10.34 15 18-172ND
Chlorobenzene mg/kg 0.054 M10.34 16 26-166ND
Chloroethane mg/kg 0.016 M10.34 5 10-130ND
Chloroform mg/kg 0.055 M10.34 16 25-161ND
Chloromethane mg/kg 0.084 M10.34 25 27-197ND
cis-1,2-Dichloroethene mg/kg 0.055 M10.34 16 28-165ND
cis-1,3-Dichloropropene mg/kg 0.052 M10.34 15 23-159ND
Dibromochloromethane mg/kg 0.057 M10.34 17 21-151ND
Dibromomethane mg/kg 0.055 M10.34 16 38-158ND
Dichlorodifluoromethane mg/kg 0.0700.34 21 10-200ND
Diisopropyl ether mg/kg 0.052 M10.34 15 23-160ND
Ethylbenzene mg/kg 0.056 M10.34 15 22-1630.0052J
Hexachloro-1,3-butadiene mg/kg 0.0450.34 13 10-192ND
Isopropylbenzene (Cumene)mg/kg 0.060 M10.34 18 24-173ND
m&p-Xylene mg/kg 0.11 M10.68 16 22-171ND
Methyl-tert-butyl ether mg/kg 0.051 M10.34 15 25-153ND
Methylene Chloride mg/kg 0.0600.34 18 10-165ND
n-Butylbenzene mg/kg 0.0520.34 15 10-186ND
n-Propylbenzene mg/kg 0.0550.34 16 16-171ND
Naphthalene mg/kg 0.0360.34 11 10-159ND
o-Xylene mg/kg 0.057 M10.34 17 23-171ND
p-Isopropyltoluene mg/kg 0.0510.34 15 13-184ND
sec-Butylbenzene mg/kg 0.052 M10.34 15 16-182ND
Styrene mg/kg 0.051 M10.34 15 25-169ND
tert-Butylbenzene mg/kg 0.060 M10.34 18 20-174ND
Tetrachloroethene mg/kg 0.0510.34 15 14-171ND
Toluene mg/kg 0.056 M10.34 16 24-166ND
trans-1,2-Dichloroethene mg/kg 0.055 M10.34 16 24-170ND
trans-1,3-Dichloropropene mg/kg 0.052 M10.34 15 22-157ND
Trichloroethene mg/kg 0.052 M10.34 15 23-176ND
Trichlorofluoromethane mg/kg 0.0069 M10.34 2 10-138ND
Vinyl acetate mg/kg 0.100.68 15 11-166ND
Vinyl chloride mg/kg 0.068 M10.34 20 21-200ND
Xylene (Total)mg/kg 0.17 MS11723-170ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92695520002
4191317SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg 0.038J 3042.8J ug/kg
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND IK,v130ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg 0.0034J 303.9J ug/kg
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92695520002
4191317SAMPLE DUPLICATE:
m&p-Xylene mg/kg 0.0047J 305.5J ug/kg
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 304.1J ug/kg
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 305.5J ug/kg
1,2-Dichloroethane-d4 (S)%100103
4-Bromofluorobenzene (S)%100101
Toluene-d8 (S)%101100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
809298
EPA 7199
EPA 7199
7199 Chromium, Hexavalent
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008, 92695355009, 92695355010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4190698
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008, 92695355009, 92695355010
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg 0.30J 1.0 10/27/23 16:380.0010
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4190699LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 11.010.4 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4190700MATRIX SPIKE SAMPLE:
MSSpike
Result
92695355001
Chromium, Hexavalent mg/kg 11.912.2 90 75-1250.94J
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4190702MATRIX SPIKE SAMPLE:
MSSpike
Result
92695355010
Chromium, Hexavalent mg/kg 14701490 98 75-1250.58J
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92695355002
4190701SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 1.9 2 202.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
809224
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008, 92695355009, 92695355010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4190506
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008, 92695355009, 92695355010
Matrix:Solid
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene mg/kg ND 0.33 10/30/23 09:330.080
1,2-Dichlorobenzene mg/kg ND 0.33 10/30/23 09:330.12
1,2-Diphenylhydrazine mg/kg ND 0.33 10/30/23 09:330.13
1,3-Dichlorobenzene mg/kg ND 0.33 10/30/23 09:330.12
1,3-Dinitrobenzene mg/kg ND 0.33 10/30/23 09:330.073
1,4-Dichlorobenzene mg/kg ND 0.33 10/30/23 09:330.12
1,4-Dinitrobenzene mg/kg ND 0.33 10/30/23 09:330.097
1-Methylnaphthalene mg/kg ND 0.33 10/30/23 09:330.11
1-Naphthalenamine mg/kg ND 0.65 10/30/23 09:330.11
2,3,4,6-Tetrachlorophenol mg/kg ND 0.33 10/30/23 09:330.082
2,3-Dichloroaniline mg/kg ND 0.33 10/30/23 09:330.16
2,4,5-Trichlorophenol mg/kg ND 0.33 10/30/23 09:330.15
2,4,6-Trichlorophenol mg/kg ND 0.33 10/30/23 09:330.13
2,4-Dichlorophenol mg/kg ND 0.33 10/30/23 09:330.13
2,4-Dimethylphenol mg/kg ND 0.33 10/30/23 09:330.14
2,4-Dinitrophenol mg/kg ND 1.6 10/30/23 09:331.0
2,4-Dinitrotoluene mg/kg ND 0.33 10/30/23 09:330.13
2,6-Dichlorophenol mg/kg ND 0.33 10/30/23 09:330.084
2,6-Dinitrotoluene mg/kg ND 0.33 10/30/23 09:330.12
2-Chloronaphthalene mg/kg ND 0.33 10/30/23 09:330.13
2-Chlorophenol mg/kg ND 0.33 10/30/23 09:330.12
2-Methyl-5-nitroaniline mg/kg ND 0.33 10/30/23 09:330.098
2-Methylnaphthalene mg/kg ND 0.33 10/30/23 09:330.13
2-Methylphenol(o-Cresol)mg/kg ND 0.33 10/30/23 09:330.13
2-Naphthalenamine mg/kg ND 0.65 10/30/23 09:330.13
2-Nitroaniline mg/kg ND 1.6 10/30/23 09:330.27
2-Nitrophenol mg/kg ND 0.33 10/30/23 09:330.14
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 10/30/23 09:330.13
3,3'-Dichlorobenzidine mg/kg ND 0.65 10/30/23 09:330.22
3,3'-Dimethylbenzidine mg/kg ND 0.65 IL10/30/23 09:330.29
3-Nitroaniline mg/kg ND 1.6 10/30/23 09:330.26
4,6-Dinitro-2-methylphenol mg/kg ND 0.65 10/30/23 09:330.30
4-Bromophenylphenyl ether mg/kg ND 0.33 10/30/23 09:330.13
4-Chloro-3-methylphenol mg/kg ND 0.65 10/30/23 09:330.23
4-Chloroaniline mg/kg ND 0.65 10/30/23 09:330.26
4-Chlorophenylphenyl ether mg/kg ND 0.33 10/30/23 09:330.12
4-Nitroaniline mg/kg ND 0.65 10/30/23 09:330.25
4-Nitrophenol mg/kg ND 1.6 10/30/23 09:330.63
Acenaphthene mg/kg ND 0.33 10/30/23 09:330.11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4190506
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008, 92695355009, 92695355010
Matrix:Solid
AnalyzedMDL
Acenaphthylene mg/kg ND 0.33 10/30/23 09:330.11
Acetophenone mg/kg ND 0.33 10/30/23 09:330.084
Aniline mg/kg ND 0.33 10/30/23 09:330.13
Atrazine mg/kg ND 0.33 10/30/23 09:330.10
Benzaldehyde mg/kg ND 0.33 10/30/23 09:330.11
Benzidine mg/kg ND 1.6 10/30/23 09:330.27
Benzo(a)anthracene mg/kg ND 0.33 10/30/23 09:330.11
Benzo(a)pyrene mg/kg ND 0.33 10/30/23 09:330.11
Benzo(b)fluoranthene mg/kg ND 0.33 10/30/23 09:330.11
Benzo(g,h,i)perylene mg/kg ND 0.33 10/30/23 09:330.13
Benzo(k)fluoranthene mg/kg ND 0.33 10/30/23 09:330.11
Benzoic Acid mg/kg ND 1.6 10/30/23 09:330.70
Benzophenone mg/kg ND 0.33 10/30/23 09:330.15
Benzyl alcohol mg/kg ND 0.65 10/30/23 09:330.25
Biphenyl (Diphenyl)mg/kg ND 0.33 10/30/23 09:330.077
bis(2-Chloroethoxy)methane mg/kg ND 0.33 10/30/23 09:330.14
bis(2-Chloroethyl) ether mg/kg ND 0.33 10/30/23 09:330.12
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 10/30/23 09:330.13
Butylbenzylphthalate mg/kg ND 0.33 10/30/23 09:330.14
Caprolactam mg/kg ND 0.33 10/30/23 09:330.18
Carbazole mg/kg ND 0.33 10/30/23 09:330.11
Chlorobenzilate mg/kg ND 0.33 10/30/23 09:330.065
Chrysene mg/kg ND 0.33 10/30/23 09:330.12
Di-n-butylphthalate mg/kg ND 0.33 10/30/23 09:330.11
Di-n-octylphthalate mg/kg ND 0.33 10/30/23 09:330.13
Dibenz(a,h)anthracene mg/kg ND 0.33 10/30/23 09:330.13
Dibenzo(a,e)pyrene mg/kg ND 0.99 10/30/23 09:330.22
Dibenzofuran mg/kg ND 0.33 10/30/23 09:330.12
Diethylphthalate mg/kg ND 0.33 10/30/23 09:330.12
Dimethylphthalate mg/kg ND 0.33 10/30/23 09:330.12
Fluoranthene mg/kg ND 0.33 10/30/23 09:330.11
Fluorene mg/kg ND 0.33 10/30/23 09:330.11
Hexachloro-1,3-butadiene mg/kg ND 0.33 10/30/23 09:330.14
Hexachlorobenzene mg/kg ND 0.33 10/30/23 09:330.13
Hexachlorocyclopentadiene mg/kg ND 0.33 10/30/23 09:330.19
Hexachloroethane mg/kg ND 0.33 10/30/23 09:330.12
Hexachlorophene mg/kg ND 3.3 IH,v210/30/23 09:331.9
Hexachloropropene mg/kg ND 0.33 10/30/23 09:330.089
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 10/30/23 09:330.13
Isodrin mg/kg ND 0.33 10/30/23 09:330.078
N-Nitroso-di-n-propylamine mg/kg ND 0.33 10/30/23 09:330.12
Naphthalene mg/kg ND 0.33 10/30/23 09:330.11
Nitrobenzene mg/kg ND 0.33 10/30/23 09:330.15
Pentachlorophenol mg/kg ND 0.65 10/30/23 09:330.32
Phenanthrene mg/kg ND 0.33 10/30/23 09:330.11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4190506
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008, 92695355009, 92695355010
Matrix:Solid
AnalyzedMDL
Phenol mg/kg ND 0.33 10/30/23 09:330.15
Pyrene mg/kg ND 0.33 10/30/23 09:330.13
Pyridine mg/kg ND 0.33 v110/30/23 09:330.10
2,4,6-Tribromophenol (S)%34 10-130 10/30/23 09:33
2-Fluorobiphenyl (S)%42 10-130 10/30/23 09:33
2-Fluorophenol (S)%43 10-130 10/30/23 09:33
Nitrobenzene-d5 (S)%43 10-130 10/30/23 09:33
Phenol-d6 (S)%40 10-130 10/30/23 09:33
Terphenyl-d14 (S)%49 10-130 10/30/23 09:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4190507LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene mg/kg 0.771.7 45 39-130
1,2-Dichlorobenzene mg/kg 0.831.7 49 37-130
1,2-Diphenylhydrazine mg/kg 1.71.7 102 45-130
1,3-Dichlorobenzene mg/kg 0.821.7 48 36-130
1,3-Dinitrobenzene mg/kg 1.1 L21.7 62 66-130
1,4-Dichlorobenzene mg/kg 0.811.7 48 36-130
1,4-Dinitrobenzene mg/kg 1.0 L21.7 62 68-130
1-Methylnaphthalene mg/kg 0.841.7 49 46-130
1-Naphthalenamine mg/kg 0.991.7 58 43-130
2,3,4,6-Tetrachlorophenol mg/kg 0.831.7 49 45-130
2,3-Dichloroaniline mg/kg 0.941.7 55 46-145
2,4,5-Trichlorophenol mg/kg 0.891.7 52 49-130
2,4,6-Trichlorophenol mg/kg 0.871.7 51 48-130
2,4-Dichlorophenol mg/kg 0.781.7 46 45-130
2,4-Dimethylphenol mg/kg 0.851.7 50 45-130
2,4-Dinitrophenol mg/kg 4.48.5 52 23-130
2,4-Dinitrotoluene mg/kg 1.01.7 59 50-130
2,6-Dichlorophenol mg/kg 0.82 L21.7 48 51-130
2,6-Dinitrotoluene mg/kg 1.01.7 60 53-130
2-Chloronaphthalene mg/kg 0.831.7 49 46-130
2-Chlorophenol mg/kg 0.861.7 51 39-130
2-Methyl-5-nitroaniline mg/kg 1.11.7 65 52-130
2-Methylnaphthalene mg/kg 0.841.7 50 45-130
2-Methylphenol(o-Cresol)mg/kg 0.841.7 50 38-130
2-Naphthalenamine mg/kg 0.67J1.7 40 34-130
2-Nitroaniline mg/kg 1.93.4 57 43-130
2-Nitrophenol mg/kg 0.831.7 49 43-130
3&4-Methylphenol(m&p Cresol)mg/kg 0.921.7 54 34-130
3,3'-Dichlorobenzidine mg/kg 2.1 L23.4 61 68-130
3,3'-Dimethylbenzidine mg/kg 3.0 IL3.4 88 68-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4190507LABORATORY CONTROL SAMPLE:
LCSSpike
3-Nitroaniline mg/kg 2.23.4 66 36-130
4,6-Dinitro-2-methylphenol mg/kg 2.03.4 60 38-130
4-Bromophenylphenyl ether mg/kg 0.941.7 56 52-130
4-Chloro-3-methylphenol mg/kg 1.83.4 54 45-130
4-Chloroaniline mg/kg 1.83.4 53 41-130
4-Chlorophenylphenyl ether mg/kg 0.931.7 55 46-130
4-Nitroaniline mg/kg 2.23.4 64 40-130
4-Nitrophenol mg/kg 4.98.5 57 34-130
Acenaphthene mg/kg 0.961.7 57 47-130
Acenaphthylene mg/kg 0.981.7 58 50-130
Acetophenone mg/kg 0.871.7 51 38-130
Aniline mg/kg 0.871.7 51 33-130
Atrazine mg/kg 0.561.7 33 10-130
Benzaldehyde mg/kg 0.661.7 39 22-130
Benzidine mg/kg 1.5J3.4 43 10-130
Benzo(a)anthracene mg/kg 1.11.7 64 49-130
Benzo(a)pyrene mg/kg 1.31.7 75 45-130
Benzo(b)fluoranthene mg/kg 1.31.7 78 45-130
Benzo(g,h,i)perylene mg/kg 1.31.7 76 44-130
Benzo(k)fluoranthene mg/kg 1.31.7 75 46-130
Benzoic Acid mg/kg 2.08.5 23 14-130
Benzophenone mg/kg 1.41.7 83 56-130
Benzyl alcohol mg/kg 1.73.4 49 39-130
Biphenyl (Diphenyl)mg/kg 0.871.7 52 49-130
bis(2-Chloroethoxy)methane mg/kg 0.871.7 51 41-130
bis(2-Chloroethyl) ether mg/kg 0.871.7 51 34-130
bis(2-Ethylhexyl)phthalate mg/kg 1.21.7 70 39-130
Butylbenzylphthalate mg/kg 1.21.7 71 48-130
Caprolactam mg/kg 0.591.7 35 10-130
Carbazole mg/kg 1.11.7 65 50-130
Chlorobenzilate mg/kg 0.941.7 55 55-130
Chrysene mg/kg 1.11.7 65 50-130
Di-n-butylphthalate mg/kg 1.11.7 64 46-130
Di-n-octylphthalate mg/kg 1.21.7 71 49-130
Dibenz(a,h)anthracene mg/kg 1.31.7 74 46-130
Dibenzo(a,e)pyrene mg/kg 1.31.7 74 49-130
Dibenzofuran mg/kg 0.931.7 55 49-130
Diethylphthalate mg/kg 1.01.7 61 49-130
Dimethylphthalate mg/kg 0.991.7 58 50-130
Fluoranthene mg/kg 1.01.7 60 49-130
Fluorene mg/kg 1.01.7 61 47-130
Hexachloro-1,3-butadiene mg/kg 0.721.7 43 36-130
Hexachlorobenzene mg/kg 0.871.7 52 52-130
Hexachlorocyclopentadiene mg/kg 0.661.7 39 10-130
Hexachloroethane mg/kg 0.811.7 48 36-130
Hexachlorophene mg/kg 7.5 IH,v316.9 44 10-130
Hexachloropropene mg/kg 0.691.7 41 40-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4190507LABORATORY CONTROL SAMPLE:
LCSSpike
Indeno(1,2,3-cd)pyrene mg/kg 1.21.7 73 44-130
Isodrin mg/kg 0.951.7 56 55-130
N-Nitroso-di-n-propylamine mg/kg 0.881.7 52 34-130
Naphthalene mg/kg 0.871.7 51 43-130
Nitrobenzene mg/kg 0.841.7 49 41-130
Pentachlorophenol mg/kg 1.83.4 52 35-130
Phenanthrene mg/kg 1.11.7 63 50-130
Phenol mg/kg 0.911.7 54 39-130
Pyrene mg/kg 1.11.7 65 51-130
Pyridine mg/kg 0.73 v11.7 43 21-130
2,4,6-Tribromophenol (S)%50 10-130
2-Fluorobiphenyl (S)%49 10-130
2-Fluorophenol (S)%51 10-130
Nitrobenzene-d5 (S)%48 10-130
Phenol-d6 (S)%50 10-130
Terphenyl-d14 (S)%59 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4190508MATRIX SPIKE SAMPLE:
MSSpike
Result
92694471001
1,2,4,5-Tetrachlorobenzene mg/kg 1.22.1 59 10-141ND
1,2-Dichlorobenzene mg/kg 1.02.1 49 22-130ND
1,2-Diphenylhydrazine mg/kg 2.9 M12.1 139 10-131ND
1,3-Dichlorobenzene mg/kg 0.982.1 47 22-130ND
1,3-Dinitrobenzene mg/kg 1.72.1 80 70-130ND
1,4-Dichlorobenzene mg/kg 1.02.1 47 21-130ND
1,4-Dinitrobenzene mg/kg 1.72.1 81 10-139ND
1-Methylnaphthalene mg/kg 1.32.1 62 27-130ND
1-Naphthalenamine mg/kg 1.3 M12.1 60 70-130ND
2,3,4,6-Tetrachlorophenol mg/kg 1.42.1 64 10-130ND
2,3-Dichloroaniline mg/kg 1.52.1 71 70-130ND
2,4,5-Trichlorophenol mg/kg 1.52.1 72 18-130ND
2,4,6-Trichlorophenol mg/kg 1.42.1 65 17-130ND
2,4-Dichlorophenol mg/kg 1.22.1 55 19-130ND
2,4-Dimethylphenol mg/kg 1.12.1 50 17-130ND
2,4-Dinitrophenol mg/kg 2.910.6 27 10-130ND
2,4-Dinitrotoluene mg/kg 1.62.1 76 31-130ND
2,6-Dichlorophenol mg/kg 1.22.1 57 10-142ND
2,6-Dinitrotoluene mg/kg 1.62.1 78 33-130ND
2-Chloronaphthalene mg/kg 1.32.1 62 26-130ND
2-Chlorophenol mg/kg 1.22.1 55 19-130ND
2-Methyl-5-nitroaniline mg/kg 1.82.1 84 70-130ND
2-Methylnaphthalene mg/kg 1.32.1 62 26-130ND
2-Methylphenol(o-Cresol)mg/kg 1.12.1 50 19-130ND
2-Naphthalenamine mg/kg 1.3 M12.1 62 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4190508MATRIX SPIKE SAMPLE:
MSSpike
Result
92694471001
2-Nitroaniline mg/kg 3.24.2 75 29-130ND
2-Nitrophenol mg/kg 1.22.1 56 16-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.32.1 59 14-130ND
3,3'-Dichlorobenzidine mg/kg 3.2 IL4.2 75 16-130ND
3,3'-Dimethylbenzidine mg/kg 3.7 IL4.2 88 70-130ND
3-Nitroaniline mg/kg 3.64.2 85 28-130ND
4,6-Dinitro-2-methylphenol mg/kg 2.64.2 61 10-131ND
4-Bromophenylphenyl ether mg/kg 1.62.1 73 32-130ND
4-Chloro-3-methylphenol mg/kg 2.94.2 68 26-130ND
4-Chloroaniline mg/kg 2.64.2 61 19-130ND
4-Chlorophenylphenyl ether mg/kg 1.52.1 71 29-130ND
4-Nitroaniline mg/kg 3.64.2 84 22-130ND
4-Nitrophenol mg/kg 7.810.6 74 10-130ND
Acenaphthene mg/kg 1.62.1 74 29-130ND
Acenaphthylene mg/kg 1.62.1 74 27-130ND
Acetophenone mg/kg 1.22.1 57 18-130ND
Aniline mg/kg 1.12.1 50 10-130ND
Atrazine mg/kg 0.692.1 32 10-130ND
Benzaldehyde mg/kg 1.12.1 53 22-130ND
Benzidine mg/kg 0.60J4.2 14 10-130ND
Benzo(a)anthracene mg/kg 1.82.1 84 31-130ND
Benzo(a)pyrene mg/kg 2.12.1 98 24-130ND
Benzo(b)fluoranthene mg/kg 2.22.1 103 12-137ND
Benzo(g,h,i)perylene mg/kg 2.12.1 100 16-130ND
Benzo(k)fluoranthene mg/kg 2.12.1 98 27-130ND
Benzoic Acid mg/kg ND M110.6 3 10-130ND
Benzophenone mg/kg 2.32.1 111 70-130ND
Benzyl alcohol mg/kg 2.54.2 58 25-130ND
Biphenyl (Diphenyl)mg/kg 1.42.1 66 32-130ND
bis(2-Chloroethoxy)methane mg/kg 1.22.1 58 26-130ND
bis(2-Chloroethyl) ether mg/kg 1.22.1 58 23-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.92.1 92 20-130ND
Butylbenzylphthalate mg/kg 2.02.1 94 28-130ND
Caprolactam mg/kg 1.12.1 51 10-130ND
Carbazole mg/kg 1.82.1 85 27-130ND
Chlorobenzilate mg/kg 1.52.1 72 70-130ND
Chrysene mg/kg 1.82.1 84 29-130ND
Di-n-butylphthalate mg/kg 1.82.1 84 29-130ND
Di-n-octylphthalate mg/kg 2.02.1 94 30-130ND
Dibenz(a,h)anthracene mg/kg 2.12.1 101 27-130ND
Dibenzo(a,e)pyrene mg/kg 2.12.1 99 70-130ND
Dibenzofuran mg/kg 1.52.1 70 33-130ND
Diethylphthalate mg/kg 1.62.1 78 34-130ND
Dimethylphthalate mg/kg 1.62.1 75 35-130ND
Fluoranthene mg/kg 1.72.1 79 26-130ND
Fluorene mg/kg 1.72.1 79 27-130ND
Hexachloro-1,3-butadiene mg/kg 1.02.1 49 19-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4190508MATRIX SPIKE SAMPLE:
MSSpike
Result
92694471001
Hexachlorobenzene mg/kg 1.52.1 71 31-130ND
Hexachlorocyclopentadiene mg/kg 0.802.1 38 10-130ND
Hexachloroethane mg/kg 1.02.1 47 21-130ND
Hexachlorophene mg/kg 10.8 IH,M1,v321.1 51 70-130ND
Hexachloropropene mg/kg 0.942.1 45 10-142ND
Indeno(1,2,3-cd)pyrene mg/kg 2.12.1 97 16-130ND
Isodrin mg/kg 1.62.1 76 70-130ND
N-Nitroso-di-n-propylamine mg/kg 1.22.1 58 22-130ND
Naphthalene mg/kg 1.32.1 60 24-130ND
Nitrobenzene mg/kg 1.22.1 56 25-130ND
Pentachlorophenol mg/kg 2.94.2 68 10-130ND
Phenanthrene mg/kg 1.82.1 83 28-130ND
Phenol mg/kg 1.22.1 58 18-130ND
Pyrene mg/kg 1.82.1 84 27-130ND
Pyridine mg/kg 1.2 v12.1 55 10-130ND
2,4,6-Tribromophenol (S)%56 10-130
2-Fluorobiphenyl (S)%40 10-130
2-Fluorophenol (S)%48 10-130
Nitrobenzene-d5 (S)%52 10-130
Phenol-d6 (S)%50 10-130
Terphenyl-d14 (S)%49 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92694471003
4190509SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Diphenylhydrazine mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dinitrobenzene mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
1,4-Dinitrobenzene mg/kg ND 30ND
1-Methylnaphthalene mg/kg ND 30ND
1-Naphthalenamine mg/kg ND 30ND
2,3,4,6-Tetrachlorophenol mg/kg ND 30ND
2,3-Dichloroaniline mg/kg ND 30ND
2,4,5-Trichlorophenol mg/kg ND 30ND
2,4,6-Trichlorophenol mg/kg ND 30ND
2,4-Dichlorophenol mg/kg ND 30ND
2,4-Dimethylphenol mg/kg ND 30ND
2,4-Dinitrophenol mg/kg ND 30ND
2,4-Dinitrotoluene mg/kg ND 30ND
2,6-Dichlorophenol mg/kg ND 30ND
2,6-Dinitrotoluene mg/kg ND 30ND
2-Chloronaphthalene mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92694471003
4190509SAMPLE DUPLICATE:
2-Chlorophenol mg/kg ND 30ND
2-Methyl-5-nitroaniline mg/kg ND 30ND
2-Methylnaphthalene mg/kg ND 30ND
2-Methylphenol(o-Cresol)mg/kg ND 30ND
2-Naphthalenamine mg/kg ND 30ND
2-Nitroaniline mg/kg ND 30ND
2-Nitrophenol mg/kg ND 30ND
3&4-Methylphenol(m&p Cresol)mg/kg ND 30ND
3,3'-Dichlorobenzidine mg/kg ND 30ND
3,3'-Dimethylbenzidine mg/kg ND IL30ND
3-Nitroaniline mg/kg ND 30ND
4,6-Dinitro-2-methylphenol mg/kg ND 30ND
4-Bromophenylphenyl ether mg/kg ND 30ND
4-Chloro-3-methylphenol mg/kg ND 30ND
4-Chloroaniline mg/kg ND 30ND
4-Chlorophenylphenyl ether mg/kg ND 30ND
4-Nitroaniline mg/kg ND 30ND
4-Nitrophenol mg/kg ND 30ND
Acenaphthene mg/kg ND 30ND
Acenaphthylene mg/kg ND 30ND
Acetophenone mg/kg ND 30ND
Aniline mg/kg ND 30ND
Atrazine mg/kg ND 30ND
Benzaldehyde mg/kg ND 30ND
Benzidine mg/kg ND 30ND
Benzo(a)anthracene mg/kg 0.74 D686301850 ug/kg
Benzo(a)pyrene mg/kg 1.0 D661301870 ug/kg
Benzo(b)fluoranthene mg/kg 0.85 D695302410 ug/kg
Benzo(g,h,i)perylene mg/kg 0.62 D667301240 ug/kg
Benzo(k)fluoranthene mg/kg 0.33J 30842 ug/kg
Benzoic Acid mg/kg ND 30ND
Benzophenone mg/kg ND 30ND
Benzyl alcohol mg/kg ND 30ND
Biphenyl (Diphenyl)mg/kg ND 30ND
bis(2-Chloroethoxy)methane mg/kg ND 30ND
bis(2-Chloroethyl) ether mg/kg ND 30ND
bis(2-Ethylhexyl)phthalate mg/kg ND 30ND
Butylbenzylphthalate mg/kg ND 30ND
Caprolactam mg/kg ND 30ND
Carbazole mg/kg ND 30674 ug/kg
Chlorobenzilate mg/kg ND 30ND
Chrysene mg/kg 0.63 D694301760 ug/kg
Di-n-butylphthalate mg/kg ND 30ND
Di-n-octylphthalate mg/kg ND 30ND
Dibenz(a,h)anthracene mg/kg ND 30ND
Dibenzo(a,e)pyrene mg/kg ND 30ND
Dibenzofuran mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92694471003
4190509SAMPLE DUPLICATE:
Diethylphthalate mg/kg ND 30ND
Dimethylphthalate mg/kg ND 30ND
Fluoranthene mg/kg 1.0 D6111303590 ug/kg
Fluorene mg/kg ND 30490 ug/kg
Hexachloro-1,3-butadiene mg/kg ND 30ND
Hexachlorobenzene mg/kg ND 30ND
Hexachlorocyclopentadiene mg/kg ND 30ND
Hexachloroethane mg/kg ND 30ND
Hexachlorophene mg/kg ND IH,v230ND
Hexachloropropene mg/kg ND 30ND
Indeno(1,2,3-cd)pyrene mg/kg 0.42J 301000 ug/kg
Isodrin mg/kg ND 30ND
N-Nitroso-di-n-propylamine mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
Nitrobenzene mg/kg ND 30ND
Pentachlorophenol mg/kg ND 30ND
Phenanthrene mg/kg 0.26J 304080 ug/kg
Phenol mg/kg ND 30ND
Pyrene mg/kg 2.0 D657303670 ug/kg
Pyridine mg/kg ND v130ND
2,4,6-Tribromophenol (S)%5049
2-Fluorobiphenyl (S)%3925
2-Fluorophenol (S)%5632
Nitrobenzene-d5 (S)%6535
Phenol-d6 (S)%6235
Terphenyl-d14 (S)%2828
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
809186
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693657001
4190208SAMPLE DUPLICATE:
Percent Moisture %19.8 N232520.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92695403008
4190209SAMPLE DUPLICATE:
Percent Moisture %21.5 N2112523.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
809208
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92695355006, 92695355007, 92695355008, 92695355009, 92695355010
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92695355006
4190353SAMPLE DUPLICATE:
Percent Moisture %24.6 N202524.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92695239015
4190354SAMPLE DUPLICATE:
Percent Moisture %8.8 N211259.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2161351
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3994280-1
Associated Lab Samples:92695355001, 92695355002, 92695355003, 92695355004, 92695355005, 92695355006, 92695355007,
92695355008
Matrix:Solid
AnalyzedMDL
Total Solids %ND 11/01/23 10:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3994280-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1671275-06
R3994280-3SAMPLE DUPLICATE:
Total Solids %83.7 0.408 1084.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 88
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2161354
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92695355009, 92695355010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3994279-1
Associated Lab Samples:92695355009, 92695355010
Matrix:Solid
AnalyzedMDL
Total Solids %0.00200 11/01/23 10:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3994279-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92695355009
R3994279-3SAMPLE DUPLICATE:
Total Solids %77.0 0.358 1077.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 88
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 88
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
ANALYTE QUALIFIERS
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 88
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92695355001 809298 809485SB-SG-1 EPA 7199 EPA 7199
92695355002 809298 809485SB-SG-2 EPA 7199 EPA 7199
92695355003 809298 809485SB-SG-3 EPA 7199 EPA 7199
92695355004 809298 809485SB-SG-4 EPA 7199 EPA 7199
92695355005 809298 809485SB-SG-5 EPA 7199 EPA 7199
92695355006 809298 809485SB-SG-6 EPA 7199 EPA 7199
92695355007 809298 809485SB-11 EPA 7199 EPA 7199
92695355008 809298 809485SB-12 EPA 7199 EPA 7199
92695355009 809298 809485SB-13 EPA 7199 EPA 7199
92695355010 809298 809485SB-DUP EPA 7199 EPA 7199
92695355001 2161880 2161880SB-SG-1 3050B EPA 6020B
92695355002 2161880 2161880SB-SG-2 3050B EPA 6020B
92695355003 2161880 2161880SB-SG-3 3050B EPA 6020B
92695355004 2161880 2161880SB-SG-4 3050B EPA 6020B
92695355005 2161880 2161880SB-SG-5 3050B EPA 6020B
92695355006 2161880 2161880SB-SG-6 3050B EPA 6020B
92695355007 2161880 2161880SB-11 3050B EPA 6020B
92695355008 2161880 2161880SB-12 3050B EPA 6020B
92695355009 2161880 2161880SB-13 3050B EPA 6020B
92695355010 2161880 2161880SB-DUP 3050B EPA 6020B
92695355001 2161803 2161803SB-SG-1 7471A EPA 7471B
92695355002 2161803 2161803SB-SG-2 7471A EPA 7471B
92695355003 2161803 2161803SB-SG-3 7471A EPA 7471B
92695355004 2161803 2161803SB-SG-4 7471A EPA 7471B
92695355005 2161803 2161803SB-SG-5 7471A EPA 7471B
92695355006 2161803 2161803SB-SG-6 7471A EPA 7471B
92695355007 2161803 2161803SB-11 7471A EPA 7471B
92695355008 2161803 2161803SB-12 7471A EPA 7471B
92695355009 2161803 2161803SB-13 7471A EPA 7471B
92695355010 2161803 2161803SB-DUP 7471A EPA 7471B
92695355001 809224 809640SB-SG-1 EPA 3546 EPA 8270E
92695355002 809224 809640SB-SG-2 EPA 3546 EPA 8270E
92695355003 809224 809640SB-SG-3 EPA 3546 EPA 8270E
92695355004 809224 809640SB-SG-4 EPA 3546 EPA 8270E
92695355005 809224 809640SB-SG-5 EPA 3546 EPA 8270E
92695355006 809224 809640SB-SG-6 EPA 3546 EPA 8270E
92695355007 809224 809640SB-11 EPA 3546 EPA 8270E
92695355008 809224 809640SB-12 EPA 3546 EPA 8270E
92695355009 809224 809640SB-13 EPA 3546 EPA 8270E
92695355010 809224 809640SB-DUP EPA 3546 EPA 8270E
92695355001 809251 809448SB-SG-1 EPA 5035A/5030B EPA 8260D
92695355002 809454 809496SB-SG-2 EPA 5035A/5030B EPA 8260D
92695355003 809454 809496SB-SG-3 EPA 5035A/5030B EPA 8260D
92695355004 809454 809496SB-SG-4 EPA 5035A/5030B EPA 8260D
92695355005 809251 809448SB-SG-5 EPA 5035A/5030B EPA 8260D
92695355006 809251 809448SB-SG-6 EPA 5035A/5030B EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 88
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92695355
LEE'S TRUCK STOP-215740
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92695355007 809251 809448SB-11 EPA 5035A/5030B EPA 8260D
92695355008 809251 809448SB-12 EPA 5035A/5030B EPA 8260D
92695355009 809251 809448SB-13 EPA 5035A/5030B EPA 8260D
92695355010 809454 809496SB-DUP EPA 5035A/5030B EPA 8260D
92695355001 809186SB-SG-1 SW-846
92695355002 809186SB-SG-2 SW-846
92695355003 809186SB-SG-3 SW-846
92695355004 809186SB-SG-4 SW-846
92695355005 809186SB-SG-5 SW-846
92695355006 809208SB-SG-6 SW-846
92695355007 809208SB-11 SW-846
92695355008 809208SB-12 SW-846
92695355009 809208SB-13 SW-846
92695355010 809208SB-DUP SW-846
92695355001 2161351 2161351SB-SG-1 SM 2540 G SM 2540G
92695355002 2161351 2161351SB-SG-2 SM 2540 G SM 2540G
92695355003 2161351 2161351SB-SG-3 SM 2540 G SM 2540G
92695355004 2161351 2161351SB-SG-4 SM 2540 G SM 2540G
92695355005 2161351 2161351SB-SG-5 SM 2540 G SM 2540G
92695355006 2161351 2161351SB-SG-6 SM 2540 G SM 2540G
92695355007 2161351 2161351SB-11 SM 2540 G SM 2540G
92695355008 2161351 2161351SB-12 SM 2540 G SM 2540G
92695355009 2161354 2161354SB-13 SM 2540 G SM 2540G
92695355010 2161354 2161354SB-DUP SM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/15/2023 06:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 88
Page 86 of 88
Page 87 of 88
Page 88 of 88
Appendix V – Pace Laboratory Report – Soil Gas
ANALYTICAL REPORT
November 14, 2023
Revised Report
S&ME Inc. - Charlotte NC
Sample Delivery Group:L1672585
Samples Received:11/01/2023
Project Number:215740
Description:Lee's Truck Stop
Report To:John Sherrill
2016 Ayrsley Town Blvd, Suite 2-A
Charlotte, NC 28273
Entire Report Reviewed By:
November 14, 2023
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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November 14, 2023
Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
SG-6 L1672585-01 5
SG-5 L1672585-02 7
SG-4 L1672585-03 9
SG-3 L1672585-04 11
SG-2 L1672585-05 13
SG-1 L1672585-06 15
DUP L1672585-07 17
Qc: Quality Control Summary 19
Volatile Organic Compounds (MS) by Method TO-15 19
Gl: Glossary of Terms 26
Al: Accreditations & Locations 27
Sc: Sample Chain of Custody 28
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SG-6 L1672585-01 Air Matthew Brundage 10/30/23 11:37 11/01/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2166112 1 11/07/23 23:13 11/07/23 23:13 JAP Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2167003 20 11/08/23 17:39 11/08/23 17:39 SDS Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2167849 50 11/09/23 19:43 11/09/23 19:43 DAH Mt. Juliet, TN
Collected by Collected date/time Received date/time
SG-5 L1672585-02 Air Matthew Brundage 10/30/23 12:03 11/01/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2166112 1 11/07/23 23:48 11/07/23 23:48 JAP Mt. Juliet, TN
Collected by Collected date/time Received date/time
SG-4 L1672585-03 Air Matthew Brundage 10/30/23 11:40 11/01/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2166112 1 11/08/23 00:22 11/08/23 00:22 JAP Mt. Juliet, TN
Collected by Collected date/time Received date/time
SG-3 L1672585-04 Air Matthew Brundage 10/30/23 12:44 11/01/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2166112 1 11/08/23 00:55 11/08/23 00:55 JAP Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2167849 20 11/09/23 17:56 11/09/23 17:56 DAH Mt. Juliet, TN
Collected by Collected date/time Received date/time
SG-2 L1672585-05 Air Matthew Brundage 10/30/23 13:32 11/01/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2166112 1 11/08/23 01:29 11/08/23 01:29 JAP Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2168835 20 11/10/23 18:10 11/10/23 18:10 DAH Mt. Juliet, TN
Collected by Collected date/time Received date/time
SG-1 L1672585-06 Air Matthew Brundage 10/30/23 13:34 11/01/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2166112 1 11/08/23 02:06 11/08/23 02:06 JAP Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2167849 10 11/09/23 16:09 11/09/23 16:09 DAH Mt. Juliet, TN
Collected by Collected date/time Received date/time
DUP L1672585-07 Air Matthew Brundage 10/30/23 11:37 11/01/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2166112 1 11/08/23 02:40 11/08/23 02:40 JAP Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2167849 20 11/09/23 17:21 11/09/23 17:21 DAH Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
Report Revision History
Level II Report - Version 1: 11/14/23 11:00
Project Narrative
Revised Report: Revised to report results to the MDL per client request. This report replaces the report issued 11/14/2023.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1672585
SG-6
Collected date/time: 10/30/23 11:37
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
Acetone 67-64-1 58.10 1.39 2.97 18.9 1 WG2166112
Allyl chloride 107-05-1 76.53 0.357 0.626 U 1 WG2166112
Benzene 71-43-2 78.10 0.228 0.639 1.82 1 WG2166112
Benzyl Chloride 100-44-7 127 0.311 1.04 U 1 WG2166112
Bromodichloromethane 75-27-4 164 0.471 1.34 U 1 WG2166112
Bromoform 75-25-2 253 0.757 6.21 U 1 WG2166112
Bromomethane 74-83-9 94.90 0.381 0.776 U 1 WG2166112
1,3-Butadiene 106-99-0 54.10 0.230 4.43 U 1 WG2166112
Carbon disulfide 75-15-0 76.10 0.317 0.622 28.2 1 WG2166112
Carbon tetrachloride 56-23-5 154 0.461 1.26 U 1 WG2166112
Chlorobenzene 108-90-7 113 0.385 0.924 U 1 WG2166112
Chloroethane 75-00-3 64.50 0.263 0.528 U 1 WG2166112
Chloroform 67-66-3 119 0.349 0.973 U 1 WG2166112
Chloromethane 74-87-3 50.50 0.213 0.413 U 1 WG2166112
2-Chlorotoluene 95-49-8 126 0.427 1.03 U 1 WG2166112
Cyclohexane 110-82-7 84.20 0.259 0.689 U 1 WG2166112
Dibromochloromethane 124-48-1 208 0.618 1.70 U 1 WG2166112
1,2-Dibromoethane 106-93-4 188 0.554 1.54 U 1 WG2166112
1,2-Dichlorobenzene 95-50-1 147 0.770 1.20 U 1 WG2166112
1,3-Dichlorobenzene 541-73-1 147 1.09 1.20 U 1 WG2166112
1,4-Dichlorobenzene 106-46-7 147 0.335 1.20 U 1 WG2166112
1,2-Dichloroethane 107-06-2 99 0.283 0.810 0.539 J 1 WG2166112
1,1-Dichloroethane 75-34-3 98 0.290 0.802 0.332 J 1 WG2166112
1,1-Dichloroethene 75-35-4 96.90 0.302 0.793 U 1 WG2166112
cis-1,2-Dichloroethene 156-59-2 96.90 0.311 0.793 U 1 WG2166112
trans-1,2-Dichloroethene 156-60-5 96.90 0.267 0.793 0.311 J 1 WG2166112
1,2-Dichloropropane 78-87-5 113 0.351 0.924 U 1 WG2166112
cis-1,3-Dichloropropene 10061-01-5 111 0.313 0.908 U 1 WG2166112
trans-1,3-Dichloropropene 10061-02-6 111 0.331 0.908 U 1 WG2166112
1,4-Dioxane 123-91-1 88.10 0.300 2.27 U 1 WG2166112
Ethanol 64-17-5 46.10 0.500 4.71 17.1 B 1 WG2166112
Ethylbenzene 100-41-4 106 0.362 0.867 33.5 1 WG2166112
4-Ethyltoluene 622-96-8 120 0.384 0.982 U 1 WG2166112
Trichlorofluoromethane 75-69-4 137.40 0.460 1.12 4.20 1 WG2166112
Dichlorodifluoromethane 75-71-8 120.92 0.678 0.989 1.80 1 WG2166112
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.608 1.53 1.32 J 1 WG2166112
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.622 1.40 U 1 WG2166112
Heptane 142-82-5 100 0.425 0.818 45.0 1 WG2166112
Hexachloro-1,3-butadiene 87-68-3 261 1.12 6.73 U 1 WG2166112
n-Hexane 110-54-3 86.20 0.726 2.22 42.7 1 WG2166112
Isopropylbenzene 98-82-8 120.20 0.382 0.983 U 1 WG2166112
Methylene Chloride 75-09-2 84.90 0.340 0.694 U 1 WG2166112
Methyl Butyl Ketone 591-78-6 100 0.544 5.11 U 1 WG2166112
2-Butanone (MEK)78-93-3 72.10 0.240 3.69 3.42 J 1 WG2166112
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 0.313 5.12 U 1 WG2166112
Methyl methacrylate 80-62-6 100.12 0.359 0.819 U 1 WG2166112
MTBE 1634-04-4 88.10 0.233 0.721 U 1 WG2166112
Naphthalene 91-20-3 128 1.83 3.30 5.76 1 WG2166112
2-Propanol 67-63-0 60.10 0.649 3.07 7.37 1 WG2166112
Propene 115-07-1 42.10 0.160 2.15 U 1 WG2166112
Styrene 100-42-5 104 0.335 0.851 U 1 WG2166112
1,1,2,2-Tetrachloroethane 79-34-5 168 0.511 1.37 U 1 WG2166112
Tetrachloroethylene 127-18-4 166 0.553 1.36 8.76 1 WG2166112
Tetrahydrofuran 109-99-9 72.10 0.216 0.590 U 1 WG2166112
Toluene 108-88-3 92.10 16.4 94.2 1850 50 WG2167849
1,2,4-Trichlorobenzene 120-82-1 181 1.10 4.66 U 1 WG2166112
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1672585
SG-6
Collected date/time: 10/30/23 11:37
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
1,1,1-Trichloroethane 71-55-6 133 0.400 1.09 U 1 WG2166112
1,1,2-Trichloroethane 79-00-5 133 0.422 1.09 U 1 WG2166112
Trichloroethylene 79-01-6 131 0.364 1.07 U 1 WG2166112
1,2,4-Trimethylbenzene 95-63-6 120 0.375 0.982 U 1 WG2166112
1,3,5-Trimethylbenzene 108-67-8 120 0.382 0.982 U 1 WG2166112
2,2,4-Trimethylpentane 540-84-1 114.22 0.621 0.934 U 1 WG2166112
Vinyl chloride 75-01-4 62.50 0.243 0.511 U 1 WG2166112
Vinyl Bromide 593-60-2 106.95 0.373 0.875 U 1 WG2166112
Vinyl acetate 108-05-4 86.10 0.408 2.22 U 1 WG2166112
Xylenes, Total 1330-20-7 106.16 11.7 52.1 847 20 WG2167003
m&p-Xylene 1330-20-7 106 0.585 1.73 61.1 1 WG2166112
o-Xylene 95-47-6 106 7.20 17.3 785 20 WG2167003
(S)
1,4-Bromofluorobenzene 460-00-4 175 374 J1 60.0-140 WG2166112
(S)
1,4-Bromofluorobenzene 460-00-4 175 201 J1 60.0-140 WG2167003
(S)
1,4-Bromofluorobenzene 460-00-4 175 110 60.0-140 WG2167849
Sample Narrative:
L1672585-01 WG2166112: Surrogate failure due to matrix interference
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 02
L1672585
SG-5
Collected date/time: 10/30/23 12:03
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
Acetone 67-64-1 58.10 1.39 2.97 46.6 1 WG2166112
Allyl chloride 107-05-1 76.53 0.357 0.626 U 1 WG2166112
Benzene 71-43-2 78.10 0.228 0.639 1.70 1 WG2166112
Benzyl Chloride 100-44-7 127 0.311 1.04 U 1 WG2166112
Bromodichloromethane 75-27-4 164 0.471 1.34 U 1 WG2166112
Bromoform 75-25-2 253 0.757 6.21 U 1 WG2166112
Bromomethane 74-83-9 94.90 0.381 0.776 U 1 WG2166112
1,3-Butadiene 106-99-0 54.10 0.230 4.43 U 1 WG2166112
Carbon disulfide 75-15-0 76.10 0.317 0.622 17.9 1 WG2166112
Carbon tetrachloride 56-23-5 154 0.461 1.26 U 1 WG2166112
Chlorobenzene 108-90-7 113 0.385 0.924 U 1 WG2166112
Chloroethane 75-00-3 64.50 0.263 0.528 U 1 WG2166112
Chloroform 67-66-3 119 0.349 0.973 0.891 J 1 WG2166112
Chloromethane 74-87-3 50.50 0.213 0.413 1.65 1 WG2166112
2-Chlorotoluene 95-49-8 126 0.427 1.03 U 1 WG2166112
Cyclohexane 110-82-7 84.20 0.259 0.689 1.29 1 WG2166112
Dibromochloromethane 124-48-1 208 0.618 1.70 U 1 WG2166112
1,2-Dibromoethane 106-93-4 188 0.554 1.54 U 1 WG2166112
1,2-Dichlorobenzene 95-50-1 147 0.770 1.20 U 1 WG2166112
1,3-Dichlorobenzene 541-73-1 147 1.09 1.20 U 1 WG2166112
1,4-Dichlorobenzene 106-46-7 147 0.335 1.20 U 1 WG2166112
1,2-Dichloroethane 107-06-2 99 0.283 0.810 U 1 WG2166112
1,1-Dichloroethane 75-34-3 98 0.290 0.802 U 1 WG2166112
1,1-Dichloroethene 75-35-4 96.90 0.302 0.793 U 1 WG2166112
cis-1,2-Dichloroethene 156-59-2 96.90 0.311 0.793 U 1 WG2166112
trans-1,2-Dichloroethene 156-60-5 96.90 0.267 0.793 U 1 WG2166112
1,2-Dichloropropane 78-87-5 113 0.351 0.924 U 1 WG2166112
cis-1,3-Dichloropropene 10061-01-5 111 0.313 0.908 U 1 WG2166112
trans-1,3-Dichloropropene 10061-02-6 111 0.331 0.908 U 1 WG2166112
1,4-Dioxane 123-91-1 88.10 0.300 2.27 U 1 WG2166112
Ethanol 64-17-5 46.10 0.500 4.71 72.6 1 WG2166112
Ethylbenzene 100-41-4 106 0.362 0.867 1.40 1 WG2166112
4-Ethyltoluene 622-96-8 120 0.384 0.982 U 1 WG2166112
Trichlorofluoromethane 75-69-4 137.40 0.460 1.12 30.7 1 WG2166112
Dichlorodifluoromethane 75-71-8 120.92 0.678 0.989 2.87 1 WG2166112
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.608 1.53 U 1 WG2166112
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.622 1.40 U 1 WG2166112
Heptane 142-82-5 100 0.425 0.818 U 1 WG2166112
Hexachloro-1,3-butadiene 87-68-3 261 1.12 6.73 2.10 J 1 WG2166112
n-Hexane 110-54-3 86.20 0.726 2.22 1.90 J 1 WG2166112
Isopropylbenzene 98-82-8 120.20 0.382 0.983 1.50 1 WG2166112
Methylene Chloride 75-09-2 84.90 0.340 0.694 3.75 1 WG2166112
Methyl Butyl Ketone 591-78-6 100 0.544 5.11 2.90 J 1 WG2166112
2-Butanone (MEK)78-93-3 72.10 0.240 3.69 6.90 1 WG2166112
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 0.313 5.12 U 1 WG2166112
Methyl methacrylate 80-62-6 100.12 0.359 0.819 U 1 WG2166112
MTBE 1634-04-4 88.10 0.233 0.721 U 1 WG2166112
Naphthalene 91-20-3 128 1.83 3.30 22.7 1 WG2166112
2-Propanol 67-63-0 60.10 0.649 3.07 10.4 1 WG2166112
Propene 115-07-1 42.10 0.160 2.15 U 1 WG2166112
Styrene 100-42-5 104 0.335 0.851 2.54 1 WG2166112
1,1,2,2-Tetrachloroethane 79-34-5 168 0.511 1.37 U 1 WG2166112
Tetrachloroethylene 127-18-4 166 0.553 1.36 3.12 1 WG2166112
Tetrahydrofuran 109-99-9 72.10 0.216 0.590 U 1 WG2166112
Toluene 108-88-3 92.10 0.328 1.88 23.0 1 WG2166112
1,2,4-Trichlorobenzene 120-82-1 181 1.10 4.66 1.74 J 1 WG2166112
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 02
L1672585
SG-5
Collected date/time: 10/30/23 12:03
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
1,1,1-Trichloroethane 71-55-6 133 0.400 1.09 U 1 WG2166112
1,1,2-Trichloroethane 79-00-5 133 0.422 1.09 U 1 WG2166112
Trichloroethylene 79-01-6 131 0.364 1.07 U 1 WG2166112
1,2,4-Trimethylbenzene 95-63-6 120 0.375 0.982 2.57 1 WG2166112
1,3,5-Trimethylbenzene 108-67-8 120 0.382 0.982 0.805 J 1 WG2166112
2,2,4-Trimethylpentane 540-84-1 114.22 0.621 0.934 U 1 WG2166112
Vinyl chloride 75-01-4 62.50 0.243 0.511 U 1 WG2166112
Vinyl Bromide 593-60-2 106.95 0.373 0.875 U 1 WG2166112
Vinyl acetate 108-05-4 86.10 0.408 2.22 U 1 WG2166112
Xylenes, Total 1330-20-7 106.16 0.586 2.61 9.51 1 WG2166112
m&p-Xylene 1330-20-7 106 0.585 1.73 6.11 1 WG2166112
o-Xylene 95-47-6 106 0.359 0.867 3.38 1 WG2166112
(S)
1,4-Bromofluorobenzene 460-00-4 175 107 60.0-140 WG2166112
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 03
L1672585
SG-4
Collected date/time: 10/30/23 11:40
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
Acetone 67-64-1 58.10 1.39 2.97 37.5 1 WG2166112
Allyl chloride 107-05-1 76.53 0.357 0.626 U 1 WG2166112
Benzene 71-43-2 78.10 0.228 0.639 2.12 1 WG2166112
Benzyl Chloride 100-44-7 127 0.311 1.04 U 1 WG2166112
Bromodichloromethane 75-27-4 164 0.471 1.34 U 1 WG2166112
Bromoform 75-25-2 253 0.757 6.21 U 1 WG2166112
Bromomethane 74-83-9 94.90 0.381 0.776 U 1 WG2166112
1,3-Butadiene 106-99-0 54.10 0.230 4.43 U 1 WG2166112
Carbon disulfide 75-15-0 76.10 0.317 0.622 27.1 1 WG2166112
Carbon tetrachloride 56-23-5 154 0.461 1.26 3.14 1 WG2166112
Chlorobenzene 108-90-7 113 0.385 0.924 U 1 WG2166112
Chloroethane 75-00-3 64.50 0.263 0.528 U 1 WG2166112
Chloroform 67-66-3 119 0.349 0.973 U 1 WG2166112
Chloromethane 74-87-3 50.50 0.213 0.413 1.77 1 WG2166112
2-Chlorotoluene 95-49-8 126 0.427 1.03 U 1 WG2166112
Cyclohexane 110-82-7 84.20 0.259 0.689 U 1 WG2166112
Dibromochloromethane 124-48-1 208 0.618 1.70 U 1 WG2166112
1,2-Dibromoethane 106-93-4 188 0.554 1.54 U 1 WG2166112
1,2-Dichlorobenzene 95-50-1 147 0.770 1.20 U 1 WG2166112
1,3-Dichlorobenzene 541-73-1 147 1.09 1.20 U 1 WG2166112
1,4-Dichlorobenzene 106-46-7 147 0.335 1.20 U 1 WG2166112
1,2-Dichloroethane 107-06-2 99 0.283 0.810 U 1 WG2166112
1,1-Dichloroethane 75-34-3 98 0.290 0.802 0.974 1 WG2166112
1,1-Dichloroethene 75-35-4 96.90 0.302 0.793 U 1 WG2166112
cis-1,2-Dichloroethene 156-59-2 96.90 0.311 0.793 U 1 WG2166112
trans-1,2-Dichloroethene 156-60-5 96.90 0.267 0.793 U 1 WG2166112
1,2-Dichloropropane 78-87-5 113 0.351 0.924 U 1 WG2166112
cis-1,3-Dichloropropene 10061-01-5 111 0.313 0.908 U 1 WG2166112
trans-1,3-Dichloropropene 10061-02-6 111 0.331 0.908 U 1 WG2166112
1,4-Dioxane 123-91-1 88.10 0.300 2.27 U 1 WG2166112
Ethanol 64-17-5 46.10 0.500 4.71 35.3 1 WG2166112
Ethylbenzene 100-41-4 106 0.362 0.867 16.3 1 WG2166112
4-Ethyltoluene 622-96-8 120 0.384 0.982 U 1 WG2166112
Trichlorofluoromethane 75-69-4 137.40 0.460 1.12 2.26 1 WG2166112
Dichlorodifluoromethane 75-71-8 120.92 0.678 0.989 1.75 1 WG2166112
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.608 1.53 0.623 J 1 WG2166112
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.622 1.40 U 1 WG2166112
Heptane 142-82-5 100 0.425 0.818 4.25 1 WG2166112
Hexachloro-1,3-butadiene 87-68-3 261 1.12 6.73 U 1 WG2166112
n-Hexane 110-54-3 86.20 0.726 2.22 21.0 1 WG2166112
Isopropylbenzene 98-82-8 120.20 0.382 0.983 2.05 1 WG2166112
Methylene Chloride 75-09-2 84.90 0.340 0.694 3.14 1 WG2166112
Methyl Butyl Ketone 591-78-6 100 0.544 5.11 U 1 WG2166112
2-Butanone (MEK)78-93-3 72.10 0.240 3.69 5.54 1 WG2166112
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 0.313 5.12 U 1 WG2166112
Methyl methacrylate 80-62-6 100.12 0.359 0.819 U 1 WG2166112
MTBE 1634-04-4 88.10 0.233 0.721 U 1 WG2166112
Naphthalene 91-20-3 128 1.83 3.30 9.06 1 WG2166112
2-Propanol 67-63-0 60.10 0.649 3.07 6.83 1 WG2166112
Propene 115-07-1 42.10 0.160 2.15 U 1 WG2166112
Styrene 100-42-5 104 0.335 0.851 U 1 WG2166112
1,1,2,2-Tetrachloroethane 79-34-5 168 0.511 1.37 U 1 WG2166112
Tetrachloroethylene 127-18-4 166 0.553 1.36 4.74 1 WG2166112
Tetrahydrofuran 109-99-9 72.10 0.216 0.590 U 1 WG2166112
Toluene 108-88-3 92.10 0.328 1.88 189 1 WG2166112
1,2,4-Trichlorobenzene 120-82-1 181 1.10 4.66 U 1 WG2166112
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Charlotte NC 215740 L1672585 11/14/23 13:04 9 of 28
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S&ME Inc. - Charlotte NC 215740 L1672585 11/14/23 13:34 9 of 28
SAMPLE RESULTS - 03
L1672585
SG-4
Collected date/time: 10/30/23 11:40
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
1,1,1-Trichloroethane 71-55-6 133 0.400 1.09 U 1 WG2166112
1,1,2-Trichloroethane 79-00-5 133 0.422 1.09 U 1 WG2166112
Trichloroethylene 79-01-6 131 0.364 1.07 0.421 J 1 WG2166112
1,2,4-Trimethylbenzene 95-63-6 120 0.375 0.982 3.13 1 WG2166112
1,3,5-Trimethylbenzene 108-67-8 120 0.382 0.982 0.839 J 1 WG2166112
2,2,4-Trimethylpentane 540-84-1 114.22 0.621 0.934 4.91 1 WG2166112
Vinyl chloride 75-01-4 62.50 0.243 0.511 U 1 WG2166112
Vinyl Bromide 593-60-2 106.95 0.373 0.875 U 1 WG2166112
Vinyl acetate 108-05-4 86.10 0.408 2.22 U 1 WG2166112
Xylenes, Total 1330-20-7 106.16 0.586 2.61 67.3 1 WG2166112
m&p-Xylene 1330-20-7 106 0.585 1.73 52.0 1 WG2166112
o-Xylene 95-47-6 106 0.359 0.867 15.0 1 WG2166112
(S)
1,4-Bromofluorobenzene 460-00-4 175 139 60.0-140 WG2166112
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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S&ME Inc. - Charlotte NC 215740 L1672585 11/14/23 13:34 10 of 28
SAMPLE RESULTS - 04
L1672585
SG-3
Collected date/time: 10/30/23 12:44
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
Acetone 67-64-1 58.10 1.39 2.97 53.9 1 WG2166112
Allyl chloride 107-05-1 76.53 0.357 0.626 U 1 WG2166112
Benzene 71-43-2 78.10 0.228 0.639 4.25 1 WG2166112
Benzyl Chloride 100-44-7 127 0.311 1.04 U 1 WG2166112
Bromodichloromethane 75-27-4 164 0.471 1.34 U 1 WG2166112
Bromoform 75-25-2 253 0.757 6.21 U 1 WG2166112
Bromomethane 74-83-9 94.90 0.381 0.776 U 1 WG2166112
1,3-Butadiene 106-99-0 54.10 0.230 4.43 U 1 WG2166112
Carbon disulfide 75-15-0 76.10 0.317 0.622 17.5 1 WG2166112
Carbon tetrachloride 56-23-5 154 0.461 1.26 0.462 J 1 WG2166112
Chlorobenzene 108-90-7 113 0.385 0.924 U 1 WG2166112
Chloroethane 75-00-3 64.50 0.263 0.528 U 1 WG2166112
Chloroform 67-66-3 119 0.349 0.973 U 1 WG2166112
Chloromethane 74-87-3 50.50 0.213 0.413 U 1 WG2166112
2-Chlorotoluene 95-49-8 126 0.427 1.03 U 1 WG2166112
Cyclohexane 110-82-7 84.20 0.259 0.689 U 1 WG2166112
Dibromochloromethane 124-48-1 208 0.618 1.70 U 1 WG2166112
1,2-Dibromoethane 106-93-4 188 0.554 1.54 U 1 WG2166112
1,2-Dichlorobenzene 95-50-1 147 0.770 1.20 U 1 WG2166112
1,3-Dichlorobenzene 541-73-1 147 1.09 1.20 U 1 WG2166112
1,4-Dichlorobenzene 106-46-7 147 0.335 1.20 U 1 WG2166112
1,2-Dichloroethane 107-06-2 99 0.283 0.810 U 1 WG2166112
1,1-Dichloroethane 75-34-3 98 0.290 0.802 1.51 1 WG2166112
1,1-Dichloroethene 75-35-4 96.90 0.302 0.793 U 1 WG2166112
cis-1,2-Dichloroethene 156-59-2 96.90 0.311 0.793 U 1 WG2166112
trans-1,2-Dichloroethene 156-60-5 96.90 0.267 0.793 U 1 WG2166112
1,2-Dichloropropane 78-87-5 113 0.351 0.924 U 1 WG2166112
cis-1,3-Dichloropropene 10061-01-5 111 0.313 0.908 U 1 WG2166112
trans-1,3-Dichloropropene 10061-02-6 111 0.331 0.908 U 1 WG2166112
1,4-Dioxane 123-91-1 88.10 0.300 2.27 U 1 WG2166112
Ethanol 64-17-5 46.10 0.500 4.71 20.4 B 1 WG2166112
Ethylbenzene 100-41-4 106 0.362 0.867 7.72 1 WG2166112
4-Ethyltoluene 622-96-8 120 0.384 0.982 U 1 WG2166112
Trichlorofluoromethane 75-69-4 137.40 0.460 1.12 3.81 1 WG2166112
Dichlorodifluoromethane 75-71-8 120.92 0.678 0.989 1.78 1 WG2166112
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.608 1.53 1.51 J 1 WG2166112
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.622 1.40 U 1 WG2166112
Heptane 142-82-5 100 0.425 0.818 6.95 1 WG2166112
Hexachloro-1,3-butadiene 87-68-3 261 1.12 6.73 U 1 WG2166112
n-Hexane 110-54-3 86.20 0.726 2.22 17.4 1 WG2166112
Isopropylbenzene 98-82-8 120.20 0.382 0.983 U 1 WG2166112
Methylene Chloride 75-09-2 84.90 0.340 0.694 1.19 1 WG2166112
Methyl Butyl Ketone 591-78-6 100 0.544 5.11 U 1 WG2166112
2-Butanone (MEK)78-93-3 72.10 0.240 3.69 15.8 1 WG2166112
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 0.313 5.12 U 1 WG2166112
Methyl methacrylate 80-62-6 100.12 0.359 0.819 U 1 WG2166112
MTBE 1634-04-4 88.10 0.233 0.721 U 1 WG2166112
Naphthalene 91-20-3 128 1.83 3.30 24.9 1 WG2166112
2-Propanol 67-63-0 60.10 0.649 3.07 9.76 1 WG2166112
Propene 115-07-1 42.10 0.160 2.15 U 1 WG2166112
Styrene 100-42-5 104 0.335 0.851 U 1 WG2166112
1,1,2,2-Tetrachloroethane 79-34-5 168 0.511 1.37 U 1 WG2166112
Tetrachloroethylene 127-18-4 166 0.553 1.36 5.49 1 WG2166112
Tetrahydrofuran 109-99-9 72.10 0.216 0.590 U 1 WG2166112
Toluene 108-88-3 92.10 6.55 37.7 750 20 WG2167849
1,2,4-Trichlorobenzene 120-82-1 181 1.10 4.66 U 1 WG2166112
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Charlotte NC 215740 L1672585 11/14/23 13:34 11 of 28
SAMPLE RESULTS - 04
L1672585
SG-3
Collected date/time: 10/30/23 12:44
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
1,1,1-Trichloroethane 71-55-6 133 0.400 1.09 0.475 J 1 WG2166112
1,1,2-Trichloroethane 79-00-5 133 0.422 1.09 U 1 WG2166112
Trichloroethylene 79-01-6 131 0.364 1.07 U 1 WG2166112
1,2,4-Trimethylbenzene 95-63-6 120 0.375 0.982 2.81 1 WG2166112
1,3,5-Trimethylbenzene 108-67-8 120 0.382 0.982 0.820 J 1 WG2166112
2,2,4-Trimethylpentane 540-84-1 114.22 0.621 0.934 14.2 1 WG2166112
Vinyl chloride 75-01-4 62.50 0.243 0.511 0.826 1 WG2166112
Vinyl Bromide 593-60-2 106.95 0.373 0.875 U 1 WG2166112
Vinyl acetate 108-05-4 86.10 0.408 2.22 U 1 WG2166112
Xylenes, Total 1330-20-7 106.16 0.586 2.61 33.6 1 WG2166112
m&p-Xylene 1330-20-7 106 0.585 1.73 20.8 1 WG2166112
o-Xylene 95-47-6 106 0.359 0.867 12.7 1 WG2166112
(S)
1,4-Bromofluorobenzene 460-00-4 175 123 60.0-140 WG2166112
(S)
1,4-Bromofluorobenzene 460-00-4 175 100 60.0-140 WG2167849
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Charlotte NC 215740 L1672585 11/14/23 13:34 12 of 28
SAMPLE RESULTS - 05
L1672585
SG-2
Collected date/time: 10/30/23 13:32
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
Acetone 67-64-1 58.10 1.39 2.97 150 1 WG2166112
Allyl chloride 107-05-1 76.53 0.357 0.626 U 1 WG2166112
Benzene 71-43-2 78.10 0.228 0.639 6.32 1 WG2166112
Benzyl Chloride 100-44-7 127 0.311 1.04 U 1 WG2166112
Bromodichloromethane 75-27-4 164 0.471 1.34 U 1 WG2166112
Bromoform 75-25-2 253 0.757 6.21 U 1 WG2166112
Bromomethane 74-83-9 94.90 0.381 0.776 U 1 WG2166112
1,3-Butadiene 106-99-0 54.10 0.230 4.43 U 1 WG2166112
Carbon disulfide 75-15-0 76.10 0.317 0.622 120 1 WG2166112
Carbon tetrachloride 56-23-5 154 0.461 1.26 0.571 J 1 WG2166112
Chlorobenzene 108-90-7 113 0.385 0.924 U 1 WG2166112
Chloroethane 75-00-3 64.50 0.263 0.528 U 1 WG2166112
Chloroform 67-66-3 119 0.349 0.973 U 1 WG2166112
Chloromethane 74-87-3 50.50 0.213 0.413 U 1 WG2166112
2-Chlorotoluene 95-49-8 126 0.427 1.03 U 1 WG2166112
Cyclohexane 110-82-7 84.20 0.259 0.689 U 1 WG2166112
Dibromochloromethane 124-48-1 208 0.618 1.70 U 1 WG2166112
1,2-Dibromoethane 106-93-4 188 0.554 1.54 U 1 WG2166112
1,2-Dichlorobenzene 95-50-1 147 0.770 1.20 U 1 WG2166112
1,3-Dichlorobenzene 541-73-1 147 1.09 1.20 U 1 WG2166112
1,4-Dichlorobenzene 106-46-7 147 0.335 1.20 U 1 WG2166112
1,2-Dichloroethane 107-06-2 99 0.283 0.810 U 1 WG2166112
1,1-Dichloroethane 75-34-3 98 0.290 0.802 2.86 1 WG2166112
1,1-Dichloroethene 75-35-4 96.90 0.302 0.793 U 1 WG2166112
cis-1,2-Dichloroethene 156-59-2 96.90 0.311 0.793 U 1 WG2166112
trans-1,2-Dichloroethene 156-60-5 96.90 0.267 0.793 U 1 WG2166112
1,2-Dichloropropane 78-87-5 113 0.351 0.924 U 1 WG2166112
cis-1,3-Dichloropropene 10061-01-5 111 0.313 0.908 U 1 WG2166112
trans-1,3-Dichloropropene 10061-02-6 111 0.331 0.908 U 1 WG2166112
1,4-Dioxane 123-91-1 88.10 0.300 2.27 U 1 WG2166112
Ethanol 64-17-5 46.10 0.500 4.71 35.1 1 WG2166112
Ethylbenzene 100-41-4 106 0.362 0.867 2.60 1 WG2166112
4-Ethyltoluene 622-96-8 120 0.384 0.982 U 1 WG2166112
Trichlorofluoromethane 75-69-4 137.40 0.460 1.12 2.10 1 WG2166112
Dichlorodifluoromethane 75-71-8 120.92 0.678 0.989 2.94 1 WG2166112
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.608 1.53 1.89 1 WG2166112
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.622 1.40 U 1 WG2166112
Heptane 142-82-5 100 0.425 0.818 37.2 1 WG2166112
Hexachloro-1,3-butadiene 87-68-3 261 1.12 6.73 U 1 WG2166112
n-Hexane 110-54-3 86.20 0.726 2.22 86.7 1 WG2166112
Isopropylbenzene 98-82-8 120.20 0.382 0.983 5.41 1 WG2166112
Methylene Chloride 75-09-2 84.90 0.340 0.694 1.58 1 WG2166112
Methyl Butyl Ketone 591-78-6 100 0.544 5.11 4.02 J 1 WG2166112
2-Butanone (MEK)78-93-3 72.10 0.240 3.69 150 1 WG2166112
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 0.313 5.12 U 1 WG2166112
Methyl methacrylate 80-62-6 100.12 0.359 0.819 U 1 WG2166112
MTBE 1634-04-4 88.10 0.233 0.721 U 1 WG2166112
Naphthalene 91-20-3 128 1.83 3.30 29.5 1 WG2166112
2-Propanol 67-63-0 60.10 0.649 3.07 6.76 1 WG2166112
Propene 115-07-1 42.10 3.20 43.0 666 20 WG2168835
Styrene 100-42-5 104 0.335 0.851 1.04 1 WG2166112
1,1,2,2-Tetrachloroethane 79-34-5 168 0.511 1.37 U 1 WG2166112
Tetrachloroethylene 127-18-4 166 0.553 1.36 17.2 1 WG2166112
Tetrahydrofuran 109-99-9 72.10 0.216 0.590 U 1 WG2166112
Toluene 108-88-3 92.10 0.328 1.88 39.9 1 WG2166112
1,2,4-Trichlorobenzene 120-82-1 181 1.10 4.66 U 1 WG2166112
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 05
L1672585
SG-2
Collected date/time: 10/30/23 13:32
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
1,1,1-Trichloroethane 71-55-6 133 0.400 1.09 U 1 WG2166112
1,1,2-Trichloroethane 79-00-5 133 0.422 1.09 U 1 WG2166112
Trichloroethylene 79-01-6 131 0.364 1.07 U 1 WG2166112
1,2,4-Trimethylbenzene 95-63-6 120 0.375 0.982 3.07 1 WG2166112
1,3,5-Trimethylbenzene 108-67-8 120 0.382 0.982 0.717 J 1 WG2166112
2,2,4-Trimethylpentane 540-84-1 114.22 0.621 0.934 U 1 WG2166112
Vinyl chloride 75-01-4 62.50 0.243 0.511 0.256 J 1 WG2166112
Vinyl Bromide 593-60-2 106.95 0.373 0.875 U 1 WG2166112
Vinyl acetate 108-05-4 86.10 0.408 2.22 U 1 WG2166112
Xylenes, Total 1330-20-7 106.16 0.586 2.61 10.5 1 WG2166112
m&p-Xylene 1330-20-7 106 0.585 1.73 7.41 1 WG2166112
o-Xylene 95-47-6 106 0.359 0.867 3.10 1 WG2166112
(S)
1,4-Bromofluorobenzene 460-00-4 175 104 60.0-140 WG2166112
(S)
1,4-Bromofluorobenzene 460-00-4 175 89.6 60.0-140 WG2168835
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 06
L1672585
SG-1
Collected date/time: 10/30/23 13:34
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
Acetone 67-64-1 58.10 1.39 2.97 114 1 WG2166112
Allyl chloride 107-05-1 76.53 0.357 0.626 U 1 WG2166112
Benzene 71-43-2 78.10 0.228 0.639 7.06 1 WG2166112
Benzyl Chloride 100-44-7 127 0.311 1.04 U 1 WG2166112
Bromodichloromethane 75-27-4 164 0.471 1.34 U 1 WG2166112
Bromoform 75-25-2 253 0.757 6.21 U 1 WG2166112
Bromomethane 74-83-9 94.90 0.381 0.776 U 1 WG2166112
1,3-Butadiene 106-99-0 54.10 0.230 4.43 U 1 WG2166112
Carbon disulfide 75-15-0 76.10 0.317 0.622 42.0 1 WG2166112
Carbon tetrachloride 56-23-5 154 0.461 1.26 U 1 WG2166112
Chlorobenzene 108-90-7 113 0.385 0.924 U 1 WG2166112
Chloroethane 75-00-3 64.50 0.263 0.528 U 1 WG2166112
Chloroform 67-66-3 119 0.349 0.973 U 1 WG2166112
Chloromethane 74-87-3 50.50 0.213 0.413 1.58 1 WG2166112
2-Chlorotoluene 95-49-8 126 0.427 1.03 U 1 WG2166112
Cyclohexane 110-82-7 84.20 0.259 0.689 U 1 WG2166112
Dibromochloromethane 124-48-1 208 0.618 1.70 U 1 WG2166112
1,2-Dibromoethane 106-93-4 188 0.554 1.54 U 1 WG2166112
1,2-Dichlorobenzene 95-50-1 147 0.770 1.20 U 1 WG2166112
1,3-Dichlorobenzene 541-73-1 147 1.09 1.20 U 1 WG2166112
1,4-Dichlorobenzene 106-46-7 147 0.335 1.20 U 1 WG2166112
1,2-Dichloroethane 107-06-2 99 0.283 0.810 U 1 WG2166112
1,1-Dichloroethane 75-34-3 98 0.290 0.802 2.15 1 WG2166112
1,1-Dichloroethene 75-35-4 96.90 0.302 0.793 U 1 WG2166112
cis-1,2-Dichloroethene 156-59-2 96.90 0.311 0.793 U 1 WG2166112
trans-1,2-Dichloroethene 156-60-5 96.90 0.267 0.793 U 1 WG2166112
1,2-Dichloropropane 78-87-5 113 0.351 0.924 U 1 WG2166112
cis-1,3-Dichloropropene 10061-01-5 111 0.313 0.908 U 1 WG2166112
trans-1,3-Dichloropropene 10061-02-6 111 0.331 0.908 U 1 WG2166112
1,4-Dioxane 123-91-1 88.10 0.300 2.27 U 1 WG2166112
Ethanol 64-17-5 46.10 0.500 4.71 31.9 B 1 WG2166112
Ethylbenzene 100-41-4 106 0.362 0.867 5.51 1 WG2166112
4-Ethyltoluene 622-96-8 120 0.384 0.982 U 1 WG2166112
Trichlorofluoromethane 75-69-4 137.40 0.460 1.12 1.88 1 WG2166112
Dichlorodifluoromethane 75-71-8 120.92 0.678 0.989 1.86 1 WG2166112
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.608 1.53 1.59 1 WG2166112
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.622 1.40 U 1 WG2166112
Heptane 142-82-5 100 0.425 0.818 U 1 WG2166112
Hexachloro-1,3-butadiene 87-68-3 261 1.12 6.73 U 1 WG2166112
n-Hexane 110-54-3 86.20 0.726 2.22 20.6 1 WG2166112
Isopropylbenzene 98-82-8 120.20 0.382 0.983 4.36 1 WG2166112
Methylene Chloride 75-09-2 84.90 0.340 0.694 1.45 1 WG2166112
Methyl Butyl Ketone 591-78-6 100 0.544 5.11 U 1 WG2166112
2-Butanone (MEK)78-93-3 72.10 0.240 3.69 43.3 1 WG2166112
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 0.313 5.12 U 1 WG2166112
Methyl methacrylate 80-62-6 100.12 0.359 0.819 U 1 WG2166112
MTBE 1634-04-4 88.10 0.233 0.721 U 1 WG2166112
Naphthalene 91-20-3 128 1.83 3.30 27.5 1 WG2166112
2-Propanol 67-63-0 60.10 0.649 3.07 50.6 1 WG2166112
Propene 115-07-1 42.10 0.160 2.15 U 1 WG2166112
Styrene 100-42-5 104 0.335 0.851 1.34 1 WG2166112
1,1,2,2-Tetrachloroethane 79-34-5 168 0.511 1.37 U 1 WG2166112
Tetrachloroethylene 127-18-4 166 0.553 1.36 2.61 1 WG2166112
Tetrahydrofuran 109-99-9 72.10 0.216 0.590 U 1 WG2166112
Toluene 108-88-3 92.10 3.28 18.8 652 10 WG2167849
1,2,4-Trichlorobenzene 120-82-1 181 1.10 4.66 U 1 WG2166112
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 06
L1672585
SG-1
Collected date/time: 10/30/23 13:34
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
1,1,1-Trichloroethane 71-55-6 133 0.400 1.09 U 1 WG2166112
1,1,2-Trichloroethane 79-00-5 133 0.422 1.09 U 1 WG2166112
Trichloroethylene 79-01-6 131 0.364 1.07 U 1 WG2166112
1,2,4-Trimethylbenzene 95-63-6 120 0.375 0.982 3.28 1 WG2166112
1,3,5-Trimethylbenzene 108-67-8 120 0.382 0.982 0.854 J 1 WG2166112
2,2,4-Trimethylpentane 540-84-1 114.22 0.621 0.934 6.17 1 WG2166112
Vinyl chloride 75-01-4 62.50 0.243 0.511 0.964 1 WG2166112
Vinyl Bromide 593-60-2 106.95 0.373 0.875 U 1 WG2166112
Vinyl acetate 108-05-4 86.10 0.408 2.22 U 1 WG2166112
Xylenes, Total 1330-20-7 106.16 0.586 2.61 17.8 1 WG2166112
m&p-Xylene 1330-20-7 106 0.585 1.73 12.4 1 WG2166112
o-Xylene 95-47-6 106 0.359 0.867 5.33 1 WG2166112
(S)
1,4-Bromofluorobenzene 460-00-4 175 106 60.0-140 WG2166112
(S)
1,4-Bromofluorobenzene 460-00-4 175 102 60.0-140 WG2167849
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 07
L1672585
DUP
Collected date/time: 10/30/23 11:37
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
Acetone 67-64-1 58.10 1.39 2.97 27.8 1 WG2166112
Allyl chloride 107-05-1 76.53 0.357 0.626 U 1 WG2166112
Benzene 71-43-2 78.10 0.228 0.639 1.70 1 WG2166112
Benzyl Chloride 100-44-7 127 0.311 1.04 U 1 WG2166112
Bromodichloromethane 75-27-4 164 0.471 1.34 U 1 WG2166112
Bromoform 75-25-2 253 0.757 6.21 U 1 WG2166112
Bromomethane 74-83-9 94.90 0.381 0.776 U 1 WG2166112
1,3-Butadiene 106-99-0 54.10 0.230 4.43 U 1 WG2166112
Carbon disulfide 75-15-0 76.10 0.317 0.622 28.8 1 WG2166112
Carbon tetrachloride 56-23-5 154 0.461 1.26 0.469 J 1 WG2166112
Chlorobenzene 108-90-7 113 0.385 0.924 U 1 WG2166112
Chloroethane 75-00-3 64.50 0.263 0.528 U 1 WG2166112
Chloroform 67-66-3 119 0.349 0.973 U 1 WG2166112
Chloromethane 74-87-3 50.50 0.213 0.413 U 1 WG2166112
2-Chlorotoluene 95-49-8 126 0.427 1.03 U 1 WG2166112
Cyclohexane 110-82-7 84.20 0.259 0.689 U 1 WG2166112
Dibromochloromethane 124-48-1 208 0.618 1.70 U 1 WG2166112
1,2-Dibromoethane 106-93-4 188 0.554 1.54 U 1 WG2166112
1,2-Dichlorobenzene 95-50-1 147 0.770 1.20 U 1 WG2166112
1,3-Dichlorobenzene 541-73-1 147 1.09 1.20 U 1 WG2166112
1,4-Dichlorobenzene 106-46-7 147 0.335 1.20 U 1 WG2166112
1,2-Dichloroethane 107-06-2 99 0.283 0.810 0.534 J 1 WG2166112
1,1-Dichloroethane 75-34-3 98 0.290 0.802 0.330 J 1 WG2166112
1,1-Dichloroethene 75-35-4 96.90 0.302 0.793 U 1 WG2166112
cis-1,2-Dichloroethene 156-59-2 96.90 0.311 0.793 U 1 WG2166112
trans-1,2-Dichloroethene 156-60-5 96.90 0.267 0.793 U 1 WG2166112
1,2-Dichloropropane 78-87-5 113 0.351 0.924 U 1 WG2166112
cis-1,3-Dichloropropene 10061-01-5 111 0.313 0.908 U 1 WG2166112
trans-1,3-Dichloropropene 10061-02-6 111 0.331 0.908 U 1 WG2166112
1,4-Dioxane 123-91-1 88.10 0.300 2.27 U 1 WG2166112
Ethanol 64-17-5 46.10 0.500 4.71 17.5 B 1 WG2166112
Ethylbenzene 100-41-4 106 0.362 0.867 35.5 1 WG2166112
4-Ethyltoluene 622-96-8 120 0.384 0.982 U 1 WG2166112
Trichlorofluoromethane 75-69-4 137.40 0.460 1.12 3.58 1 WG2166112
Dichlorodifluoromethane 75-71-8 120.92 0.678 0.989 1.94 1 WG2166112
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.608 1.53 1.67 1 WG2166112
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.622 1.40 U 1 WG2166112
Heptane 142-82-5 100 0.425 0.818 U 1 WG2166112
Hexachloro-1,3-butadiene 87-68-3 261 1.12 6.73 U 1 WG2166112
n-Hexane 110-54-3 86.20 0.726 2.22 45.5 1 WG2166112
Isopropylbenzene 98-82-8 120.20 0.382 0.983 U 1 WG2166112
Methylene Chloride 75-09-2 84.90 0.340 0.694 0.764 1 WG2166112
Methyl Butyl Ketone 591-78-6 100 0.544 5.11 U 1 WG2166112
2-Butanone (MEK)78-93-3 72.10 0.240 3.69 64.3 1 WG2166112
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 0.313 5.12 U 1 WG2166112
Methyl methacrylate 80-62-6 100.12 0.359 0.819 U 1 WG2166112
MTBE 1634-04-4 88.10 0.233 0.721 U 1 WG2166112
Naphthalene 91-20-3 128 1.83 3.30 4.22 1 WG2166112
2-Propanol 67-63-0 60.10 0.649 3.07 7.40 1 WG2166112
Propene 115-07-1 42.10 0.160 2.15 U 1 WG2166112
Styrene 100-42-5 104 0.335 0.851 U 1 WG2166112
1,1,2,2-Tetrachloroethane 79-34-5 168 0.511 1.37 U 1 WG2166112
Tetrachloroethylene 127-18-4 166 0.553 1.36 U 1 WG2166112
Tetrahydrofuran 109-99-9 72.10 0.216 0.590 U 1 WG2166112
Toluene 108-88-3 92.10 6.55 37.7 7570 20 WG2167849
1,2,4-Trichlorobenzene 120-82-1 181 1.10 4.66 U 1 WG2166112
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 07
L1672585
DUP
Collected date/time: 10/30/23 11:37
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
1,1,1-Trichloroethane 71-55-6 133 0.400 1.09 U 1 WG2166112
1,1,2-Trichloroethane 79-00-5 133 0.422 1.09 U 1 WG2166112
Trichloroethylene 79-01-6 131 0.364 1.07 U 1 WG2166112
1,2,4-Trimethylbenzene 95-63-6 120 0.375 0.982 U 1 WG2166112
1,3,5-Trimethylbenzene 108-67-8 120 0.382 0.982 U 1 WG2166112
2,2,4-Trimethylpentane 540-84-1 114.22 0.621 0.934 U 1 WG2166112
Vinyl chloride 75-01-4 62.50 0.243 0.511 U 1 WG2166112
Vinyl Bromide 593-60-2 106.95 0.373 0.875 U 1 WG2166112
Vinyl acetate 108-05-4 86.10 0.408 2.22 U 1 WG2166112
Xylenes, Total 1330-20-7 106.16 11.7 52.1 647 20 WG2167849
m&p-Xylene 1330-20-7 106 0.585 1.73 62.9 1 WG2166112
o-Xylene 95-47-6 106 7.20 17.3 585 20 WG2167849
(S)
1,4-Bromofluorobenzene 460-00-4 175 369 J1 60.0-140 WG2166112
(S)
1,4-Bromofluorobenzene 460-00-4 175 194 J1 60.0-140 WG2167849
Sample Narrative:
L1672585-07 WG2166112: Surrogate failure due to matrix interference
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2166112
Volatile Organic Compounds (MS) by Method TO-15 L1672585-01,02,03,04,05,06,07
Method Blank (MB)
(MB) R3997096-3 11/07/23 10:38
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/m3 ug/m3 ug/m3
Acetone U 1.39 2.97
Allyl chloride U 0.357 0.626
Benzene U 0.228 0.639
Benzyl Chloride U 0.311 1.04
Bromodichloromethane U 0.471 1.34
Bromoform U 0.757 6.21
Bromomethane U 0.381 0.776
1,3-Butadiene U 0.230 4.43
Carbon disulfide U 0.317 0.622
Carbon tetrachloride U 0.461 1.26
Chlorobenzene U 0.385 0.924
Chloroethane U 0.263 0.528
Chloroform U 0.349 0.973
Chloromethane U 0.213 0.413
2-Chlorotoluene U 0.427 1.03
Cyclohexane U 0.259 0.689
Dibromochloromethane U 0.618 1.70
1,2-Dibromoethane U 0.554 1.54
1,2-Dichlorobenzene U 0.770 1.20
1,3-Dichlorobenzene U 1.09 1.20
1,4-Dichlorobenzene U 0.335 1.20
1,2-Dichloroethane U 0.283 0.810
1,1-Dichloroethane U 0.290 0.802
1,1-Dichloroethene U 0.302 0.793
cis-1,2-Dichloroethene U 0.311 0.793
trans-1,2-Dichloroethene U 0.267 0.793
1,2-Dichloropropane U 0.351 0.924
cis-1,3-Dichloropropene U 0.313 0.908
trans-1,3-Dichloropropene U 0.331 0.908
1,4-Dioxane U 0.300 2.27
Ethanol 3.41 J 0.500 4.71
Ethylbenzene U 0.362 0.867
4-Ethyltoluene U 0.384 0.982
Trichlorofluoromethane U 0.460 1.12
Dichlorodifluoromethane U 0.678 0.989
1,1,2-Trichlorotrifluoroethane U 0.608 1.53
1,2-Dichlorotetrafluoroethane U 0.622 1.40
Heptane U 0.425 0.818
Hexachloro-1,3-butadiene U 1.12 6.73
n-Hexane U 0.726 2.22
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2166112
Volatile Organic Compounds (MS) by Method TO-15 L1672585-01,02,03,04,05,06,07
Method Blank (MB)
(MB) R3997096-3 11/07/23 10:38
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/m3 ug/m3 ug/m3
Isopropylbenzene U 0.382 0.983
Methylene Chloride U 0.340 0.694
Methyl Butyl Ketone U 0.544 5.11
2-Butanone (MEK)U 0.240 3.69
4-Methyl-2-pentanone (MIBK)U 0.313 5.12
Methyl methacrylate U 0.359 0.819
MTBE U 0.233 0.721
Naphthalene U 1.83 3.30
2-Propanol U 0.649 3.07
Propene U 0.160 2.15
Styrene U 0.335 0.851
1,1,2,2-Tetrachloroethane U 0.511 1.37
Tetrachloroethylene U 0.553 1.36
Tetrahydrofuran U 0.216 0.590
Toluene U 0.328 1.88
1,2,4-Trichlorobenzene U 1.10 4.66
1,1,1-Trichloroethane U 0.400 1.09
1,1,2-Trichloroethane U 0.422 1.09
Trichloroethylene U 0.364 1.07
1,2,4-Trimethylbenzene U 0.375 0.982
1,3,5-Trimethylbenzene U 0.382 0.982
2,2,4-Trimethylpentane U 0.621 0.934
Vinyl chloride U 0.243 0.511
Vinyl Bromide U 0.373 0.875
Vinyl acetate U 0.408 2.22
Xylenes, Total U 0.586 2.61
m&p-Xylene U 0.585 1.73
o-Xylene U 0.359 0.867
(S) 1,4-Bromofluorobenzene 96.7 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3997096-1 11/07/23 09:28 • (LCSD) R3997096-2 11/07/23 10:05
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
Acetone 8.91 8.74 6.82 98.1 76.5 70.0-130 24.7 25
Allyl chloride 11.7 11.8 11.9 101 101 70.0-130 0.793 25
Benzene 12.0 11.8 11.8 98.1 98.1 70.0-130 0.000 25
Benzyl Chloride 19.5 19.3 19.1 98.9 98.1 70.0-152 0.812 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2166112
Volatile Organic Compounds (MS) by Method TO-15 L1672585-01,02,03,04,05,06,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3997096-1 11/07/23 09:28 • (LCSD) R3997096-2 11/07/23 10:05
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
Bromodichloromethane 25.2 25.0 24.8 99.5 98.7 70.0-130 0.808 25
Bromoform 38.8 37.6 37.4 96.8 96.3 70.0-130 0.552 25
Bromomethane 14.6 15.3 15.0 105 103 70.0-130 2.05 25
1,3-Butadiene 8.30 8.14 7.83 98.1 94.4 70.0-130 3.88 25
Carbon disulfide 11.7 11.4 11.2 97.6 96.3 70.0-130 1.38 25
Carbon tetrachloride 23.6 23.9 23.7 101 100 70.0-130 0.795 25
Chlorobenzene 17.3 17.3 17.7 100 102 70.0-130 1.85 25
Chloroethane 9.89 9.73 9.81 98.4 99.2 70.0-130 0.810 25
Chloroform 18.3 18.1 17.9 99.2 98.1 70.0-130 1.08 25
Chloromethane 7.75 7.58 7.54 97.9 97.3 70.0-130 0.546 25
2-Chlorotoluene 19.3 19.9 20.1 103 104 70.0-130 0.772 25
Cyclohexane 12.9 13.2 12.9 102 100 70.0-130 2.11 25
Dibromochloromethane 31.9 31.7 31.3 99.5 98.1 70.0-130 1.35 25
1,2-Dibromoethane 28.8 28.8 29.0 100 101 70.0-130 0.532 25
1,2-Dichlorobenzene 22.5 22.7 21.9 101 97.3 70.0-130 3.23 25
1,3-Dichlorobenzene 22.5 22.7 22.5 101 99.7 70.0-130 0.799 25
1,4-Dichlorobenzene 22.5 22.9 22.8 102 101 70.0-130 0.526 25
1,2-Dichloroethane 15.2 14.9 14.9 97.9 97.9 70.0-130 0.000 25
1,1-Dichloroethane 15.0 14.8 15.0 98.1 99.7 70.0-130 1.62 25
1,1-Dichloroethene 14.9 13.8 14.3 92.5 96.3 70.0-130 3.95 25
cis-1,2-Dichloroethene 14.9 14.0 14.3 94.1 96.0 70.0-130 1.96 25
trans-1,2-Dichloroethene 14.9 14.5 14.7 97.9 99.2 70.0-130 1.35 25
1,2-Dichloropropane 17.3 16.6 16.5 96.0 94.9 70.0-130 1.12 25
cis-1,3-Dichloropropene 17.0 16.5 16.7 97.1 97.9 70.0-130 0.821 25
trans-1,3-Dichloropropene 17.0 16.3 17.0 95.5 100 70.0-130 4.64 25
1,4-Dioxane 13.5 13.4 13.6 98.9 101 70.0-140 1.60 25
Ethanol 7.07 9.07 9.28 128 131 55.0-148 2.26 25
Ethylbenzene 16.3 16.2 16.0 99.7 98.4 70.0-130 1.35 25
4-Ethyltoluene 18.4 19.0 18.9 103 103 70.0-130 0.776 25
Trichlorofluoromethane 21.1 21.6 21.5 103 102 70.0-130 0.521 25
Dichlorodifluoromethane 18.5 18.8 18.4 101 99.5 64.0-139 1.86 25
1,1,2-Trichlorotrifluoroethane 28.7 26.9 26.4 93.6 91.7 70.0-130 2.01 25
1,2-Dichlorotetrafluoroethane 26.2 26.3 26.0 100 99.2 70.0-130 1.07 25
Heptane 15.3 16.8 15.7 110 102 70.0-130 7.05 25
Hexachloro-1,3-butadiene 40.0 41.6 41.1 104 103 70.0-151 1.29 25
n-Hexane 13.2 13.3 13.3 101 101 70.0-130 0.265 25
Isopropylbenzene 18.4 19.1 18.9 103 102 70.0-130 1.04 25
Methylene Chloride 13.0 12.7 12.6 97.3 96.5 70.0-130 0.825 25
Methyl Butyl Ketone 15.3 14.8 14.6 96.8 95.5 70.0-149 1.39 25
2-Butanone (MEK)11.1 11.3 11.1 102 100 70.0-130 1.58 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2166112
Volatile Organic Compounds (MS) by Method TO-15 L1672585-01,02,03,04,05,06,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3997096-1 11/07/23 09:28 • (LCSD) R3997096-2 11/07/23 10:05
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
4-Methyl-2-pentanone (MIBK)15.4 15.1 15.2 98.4 98.9 70.0-139 0.541 25
Methyl methacrylate 15.4 13.9 14.4 90.7 93.6 70.0-130 3.18 25
MTBE 13.5 13.4 13.2 99.2 97.9 70.0-130 1.35 25
Naphthalene 19.6 21.6 21.8 110 111 70.0-159 0.964 25
2-Propanol 9.22 9.34 9.17 101 99.5 70.0-139 1.86 25
Propene 6.46 6.77 6.59 105 102 64.0-144 2.58 25
Styrene 16.0 16.7 16.7 105 105 70.0-130 0.000 25
1,1,2,2-Tetrachloroethane 25.8 25.0 24.9 97.1 96.5 70.0-130 0.551 25
Tetrachloroethylene 25.5 25.1 24.9 98.7 97.9 70.0-130 0.814 25
Tetrahydrofuran 11.1 10.9 11.0 98.1 99.5 70.0-137 1.35 25
Toluene 14.1 14.2 14.2 101 101 70.0-130 0.000 25
1,2,4-Trichlorobenzene 27.8 30.7 30.2 111 109 70.0-160 1.70 25
1,1,1-Trichloroethane 20.4 20.1 20.2 98.7 98.9 70.0-130 0.270 25
1,1,2-Trichloroethane 20.4 20.3 20.0 99.7 97.9 70.0-130 1.89 25
Trichloroethylene 20.1 19.5 19.6 97.1 97.6 70.0-130 0.548 25
1,2,4-Trimethylbenzene 18.4 19.2 18.8 105 102 70.0-130 2.32 25
1,3,5-Trimethylbenzene 18.4 19.7 19.3 107 105 70.0-130 2.26 25
2,2,4-Trimethylpentane 17.5 17.8 17.8 102 102 70.0-130 0.000 25
Vinyl chloride 9.59 9.76 9.59 102 100 70.0-130 1.85 25
Vinyl Bromide 16.4 17.1 16.7 104 102 70.0-130 2.07 25
Vinyl acetate 13.2 14.4 13.0 109 98.7 70.0-130 9.77 25
Xylenes, Total 49.1 49.5 49.1 101 100 70.0-130 0.881 25
m&p-Xylene 32.5 32.9 32.5 101 100 70.0-130 1.19 25
o-Xylene 16.3 16.4 16.3 101 101 70.0-130 0.265 25
(S) 1,4-Bromofluorobenzene 99.4 97.6 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2167003
Volatile Organic Compounds (MS) by Method TO-15 L1672585-01
Method Blank (MB)
(MB) R3997449-3 11/08/23 11:38
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/m3 ug/m3 ug/m3
Xylenes, Total U 0.586 2.61
o-Xylene U 0.359 0.867
(S) 1,4-Bromofluorobenzene 97.3 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3997449-1 11/08/23 10:03 • (LCSD) R3997449-2 11/08/23 10:52
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
Xylenes, Total 49.1 53.8 54.7 110 112 70.0-130 1.60 25
o-Xylene 16.3 17.7 17.9 109 110 70.0-130 1.22 25
(S) 1,4-Bromofluorobenzene 95.7 96.7 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2167849
Volatile Organic Compounds (MS) by Method TO-15 L1672585-01,04,06,07
Method Blank (MB)
(MB) R3998122-3 11/09/23 11:03
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/m3 ug/m3 ug/m3
Toluene U 0.328 1.88
Xylenes, Total U 0.586 2.61
o-Xylene U 0.359 0.867
(S) 1,4-Bromofluorobenzene 97.0 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3998122-1 11/09/23 09:46 • (LCSD) R3998122-2 11/09/23 10:25
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
Toluene 14.1 13.6 13.8 96.5 97.6 70.0-130 1.10 25
Xylenes, Total 49.1 49.5 49.1 101 100 70.0-130 0.881 25
o-Xylene 16.3 16.2 16.0 99.7 98.4 70.0-130 1.35 25
(S) 1,4-Bromofluorobenzene 98.9 98.3 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2168835
Volatile Organic Compounds (MS) by Method TO-15 L1672585-05
Method Blank (MB)
(MB) R3998517-3 11/10/23 10:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/m3 ug/m3 ug/m3
Propene U 0.160 2.15
(S) 1,4-Bromofluorobenzene 93.3 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3998517-1 11/10/23 09:24 • (LCSD) R3998517-2 11/10/23 10:03
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
Propene 6.46 6.37 6.54 98.7 101 64.0-144 2.67 25
(S) 1,4-Bromofluorobenzene 92.4 93.7 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded; values are outside upper control limits.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Appendix VI – NCDEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
C
North Carolina Department of Environmental Quality
Risk Calculator
Lee's Truck Stop
100 Dalton Avenue
Brownfields
25091-21-060
July 2023
May 2023 EPA RSL Table
11/22/2023
Prepared By:S&ME, Inc.
John L. Sherrill, P.G.
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 25091-21-060
Exposure Unit ID: C
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 25091-21-060
Exposure Unit ID: C
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 1.3E-05 2.2E-01 NO
Groundwater Use*NC NC NC
Soil 1.8E-06 1.6E-02 NO
Groundwater Use*NC NC NC
Construction Worker Soil 8.1E-07 1.2E-01 NO
Soil 7.4E-06 1.2E-01 NO
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 0.0E+00 0.0E+00 NO
Soil Gas to Indoor Air 1.4E-05 6.6E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air 0.0E+00 0.0E+00 NO
Soil Gas to Indoor Air 1.0E-06 5.2E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NM
Source Groundwater NM
Source Soil NM
Source Groundwater NM
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Sitewide Risk Output Form 1B
Version Date: July 2023 NOTE: If any changes were made, select "Update Sitewide Risk Values" to obtain updated values.
Basis: May 2023 EPA RSL Table
Site ID: 25091-21-060
Exposure Unit ID: C
Receptor Pathway
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Soil 1.3E-05 2.2E-01 1.3E-05 2.2E-01
Groundwater Use*NM NM NM NM
Soil 1.8E-06 1.6E-02 1.8E-06 1.6E-02
Groundwater Use*NM NM NM NM
Construction Worker Soil 8.1E-07 1.2E-01
Soil 7.4E-06 1.2E-01
Surface Water Use*NM NM
Groundwater to Indoor Air NM NM NM NM
Soil Gas to Indoor Air 1.4E-05 6.6E-01 1.4E-05 6.6E-01
Indoor Air NM NM NM NM
Groundwater to Indoor Air NM NM NM NM
Soil Gas to Indoor Air 1.0E-06 5.2E-02 1.0E-06 5.2E-02
Indoor Air NM NM NM NM
2.7E-05 8.8E-01 2.7E-05 8.8E-01 2.9E-06 6.8E-02 2.9E-06 6.8E-02 8.1E-07 1.2E-01 7.4E-06 1.2E-01
3. NM = Not Modeled
4. NC = Pathway not calculated
TOTAL SITEWIDE RISK FOR EACH RECEPTOR
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure.
Resident
Non-Residential Worker
Resident
Non-Residential Worker
Recreator/Trespasser
VAPOR INTRUSION CALCULATORS
DIRECT CONTACT SOIL AND WATER CALCULATORS
Non-Residential Worker - Future Scenario Construction Worker Recreator/TrespasserResident - Current Scenario Resident - Future Scenario Non-Residential Worker - Current Scenario
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 25091-21-060
Exposure Unit ID: C
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated
Non-
Carcinogenic
Hazard
Quotient
7440-38-2 Arsenic, Inorganic 4.54 4.54 4.54 5.9E-06 8.3E-07 1.2E-10 6.7E-06 1.2E-01 1.4E-02 4.9E-06 1.3E-01
7440-39-3 Barium 74.9 74.9 74.9 4.8E-03 2.4E-06 4.8E-03
7440-43-9 Cadmium (Diet)0.498 0.498 0.498 5.4E-12 5.4E-12 6.4E-02 6.0E-03 8.0E-07 7.0E-02
16065-83-1 Chromium(III), Insoluble Salts 58.4 58.4 58.4 5.0E-04 5.0E-04
18540-29-9 Chromium(VI)2 2 2 6.5E-06 2.8E-09 6.5E-06 8.5E-03 3.2E-07 8.5E-03
100-41-4 Ethylbenzene 0.03 0.03 0.03 4.7E-10 4.4E-09 4.9E-09 7.7E-06 4.8E-06 1.2E-05
7439-92-1 ~Lead and Compounds 39.6 39.6 39.6 <SL**<SL**<SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.0739 0.0739 0.0739 3.1E-03 4.0E-09 3.1E-03
206-44-0 ~Fluoranthene 0.17 0.17 0.17 5.4E-05 1.7E-05 7.1E-05
91-20-3 ~Naphthalene 0.015 0.015 0.015 2.6E-09 9.5E-10 3.7E-09 7.2E-09 9.6E-06 3.0E-06 9.7E-05 1.1E-04
129-00-0 ~Pyrene 0.2 0.2 0.2 8.5E-05 2.6E-05 1.1E-04
7782-49-2 Selenium 1.06 1.06 1.06 2.7E-03 8.6E-10 2.7E-03
108-88-3 Toluene 0.84 0.84 0.84 1.3E-04 3.5E-05 1.7E-04
95-63-6 Trimethylbenzene, 1,2,4-0.0055 0.0055 0.0055 7.0E-06 1.0E-05 1.7E-05
108-67-8 Trimethylbenzene, 1,3,5-0.0031 0.0031 0.0031 4.0E-06 7.0E-06 1.1E-05
1330-20-7 Xylenes 0.17 0.17 0.17 1.1E-05 2.7E-04 2.8E-04
Cumulative:1.3E-05 2.2E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 25091-21-060
Exposure Unit ID: C
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
7440-38-2 Arsenic, Inorganic 4.54 4.54 4.54 1.2E-06 2.6E-07 2.7E-11 1.5E-06 7.8E-03 1.6E-03 1.2E-06 9.4E-03
7440-39-3 Barium 74.9 74.9 74.9 3.2E-04 5.8E-07 3.2E-04
7440-43-9 Cadmium (Diet)0.498 0.498 0.498 1.2E-12 1.2E-12 4.3E-03 7.2E-04 1.9E-07 5.0E-03
16065-83-1 Chromium(III), Insoluble Salts 58.4 58.4 58.4 3.3E-05 3.3E-05
18540-29-9 Chromium(VI)2 2 2 3.1E-07 2.3E-10 3.1E-07 5.7E-04 7.7E-08 5.7E-04
100-41-4 Ethylbenzene 0.03 0.03 0.03 1.0E-10 1.0E-09 1.1E-09 5.1E-07 1.1E-06 1.6E-06
7439-92-1 ~Lead and Compounds 39.6 39.6 39.6 <SL**<SL**<SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.0739 0.0739 0.0739 2.1E-04 9.5E-10 2.1E-04
206-44-0 ~Fluoranthene 0.17 0.17 0.17 3.6E-06 2.0E-06 5.6E-06
91-20-3 ~Naphthalene 0.015 0.015 0.015 5.5E-10 3.0E-10 8.4E-10 1.7E-09 6.4E-07 3.5E-07 2.3E-05 2.4E-05
129-00-0 ~Pyrene 0.2 0.2 0.2 5.7E-06 3.1E-06 8.8E-06
7782-49-2 Selenium 1.06 1.06 1.06 1.8E-04 2.0E-10 1.8E-04
108-88-3 Toluene 0.84 0.84 0.84 9.0E-06 8.4E-06 1.7E-05
95-63-6 Trimethylbenzene, 1,2,4-0.0055 0.0055 0.0055 4.7E-07 2.5E-06 3.0E-06
108-67-8 Trimethylbenzene, 1,3,5-0.0031 0.0031 0.0031 2.7E-07 1.7E-06 1.9E-06
1330-20-7 Xylenes 0.17 0.17 0.17 7.3E-07 6.4E-05 6.4E-05
Cumulative:1.8E-06 1.6E-02
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Construction Worker Soil
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 25091-21-060
Exposure Unit ID: C
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
7440-38-2 Arsenic, Inorganic 4.54 4.54 4.54 1.6E-07 2.6E-08 6.0E-08 2.5E-07 2.7E-02 4.3E-03 6.8E-02 9.9E-02
7440-39-3 Barium 74.9 74.9 74.9 1.1E-03 3.4E-03 4.5E-03
7440-43-9 Cadmium (Diet)0.498 0.498 0.498 2.8E-09 2.8E-09 2.9E-03 3.8E-04 1.1E-02 1.4E-02
16065-83-1 Chromium(III), Insoluble Salts 58.4 58.4 58.4 1.1E-04 2.6E-03 2.7E-03
18540-29-9 Chromium(VI)2 2 2 4.0E-08 5.2E-07 5.6E-07 1.2E-03 1.5E-03 2.7E-03
100-41-4 Ethylbenzene 0.03 0.03 0.03 1.3E-11 1.9E-10 2.1E-10 1.8E-06 6.2E-07 2.4E-06
7439-92-1 ~Lead and Compounds 39.6 39.6 39.6 <SL**<SL**<SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.0739 0.0739 0.0739 7.3E-05 5.5E-05 1.3E-04
206-44-0 ~Fluoranthene 0.17 0.17 0.17 5.0E-06 2.1E-06 7.1E-06
91-20-3 ~Naphthalene 0.015 0.015 0.015 7.3E-11 3.0E-11 1.6E-10 2.6E-10 7.4E-08 3.1E-08 1.2E-04 1.2E-04
129-00-0 ~Pyrene 0.2 0.2 0.2 2.0E-06 8.2E-07 2.8E-06
7782-49-2 Selenium 1.06 1.06 1.06 6.2E-04 1.2E-05 6.4E-04
108-88-3 Toluene 0.84 0.84 0.84 3.1E-06 4.2E-05 4.5E-05
95-63-6 Trimethylbenzene, 1,2,4-0.0055 0.0055 0.0055 4.1E-07 3.7E-06 4.1E-06
108-67-8 Trimethylbenzene, 1,3,5-0.0031 0.0031 0.0031 2.3E-07 2.5E-06 2.7E-06
1330-20-7 Xylenes 0.17 0.17 0.17 1.3E-06 7.9E-05 8.0E-05
Cumulative:8.1E-07 1.2E-01
Output Form 2E
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800 mg/kg
for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Recreator/Trespasser Soil Output Form 2F
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 25091-21-060
Exposure Unit ID: C
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
Receptor Type:
CAS #Chemical Name:Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
7440-38-2 Arsenic, Inorganic 4.54 4.54 4.54 3.3E-06 4.6E-07 5.4E-12 3.7E-06 6.5E-02 7.7E-03 2.3E-07 7.2E-02
7440-39-3 Barium 74.9 74.9 74.9 2.7E-03 1.1E-07 2.7E-03
7440-43-9 Cadmium (Diet)0.498 0.498 0.498 2.5E-13 2.5E-13 3.5E-02 3.4E-03 3.7E-08 3.9E-02
16065-83-1 Chromium(III), Insoluble Salts 58.4 58.4 58.4 2.8E-04 2.8E-04
18540-29-9 Chromium(VI)2 2 2 3.6E-06 1.3E-10 3.6E-06 4.7E-03 1.5E-08 4.7E-03
100-41-4 Ethylbenzene 0.03 0.03 0.03 2.6E-10 2.1E-10 4.7E-10 4.3E-06 2.2E-07 4.5E-06
7439-92-1 ~Lead and Compounds 39.6 39.6 39.6 <SL**<SL**<SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.0739 0.0739 0.0739 1.8E-03 1.8E-10 1.8E-03
206-44-0 ~Fluoranthene 0.17 0.17 0.17 3.0E-05 9.3E-06 4.0E-05
91-20-3 ~Naphthalene 0.015 0.015 0.015 1.4E-09 5.3E-10 1.7E-10 2.1E-09 5.3E-06 1.6E-06 4.5E-06 1.2E-05
129-00-0 ~Pyrene 0.2 0.2 0.2 4.7E-05 1.5E-05 6.2E-05
7782-49-2 Selenium 1.06 1.06 1.06 1.5E-03 4.0E-11 1.5E-03
108-88-3 Toluene 0.84 0.84 0.84 7.5E-05 1.6E-06 7.6E-05
95-63-6 Trimethylbenzene, 1,2,4-0.0055 0.0055 0.0055 3.9E-06 4.8E-07 4.4E-06
108-67-8 Trimethylbenzene, 1,3,5-0.0031 0.0031 0.0031 2.2E-06 3.3E-07 2.5E-06
1330-20-7 Xylenes 0.17 0.17 0.17 6.1E-06 1.2E-05 1.8E-05
Cumulative:7.4E-06 1.2E-01
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400
mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 25091-21-060
Exposure Unit ID: C
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 150 4.5 --
71-43-2 Benzene 7.06 0.2118 3.6E-01 6.3E+00 5.9E-07 6.8E-03
75-15-0 Carbon Disulfide 120 3.6 -1.5E+02 4.9E-03
56-23-5 Carbon Tetrachloride 3.14 0.0942 4.7E-01 2.1E+01 2.0E-07 9.0E-04
67-66-3 Chloroform 0.891 0.02673 1.2E-01 2.0E+01 2.2E-07 2.6E-04
74-87-3 Chloromethane 1.77 0.0531 -1.9E+01 5.7E-04
98-82-8 Cumene 5.41 0.1623 -8.3E+01 3.9E-04
110-83-8 Cyclohexene 1.29 0.0387 -2.1E+02 3.7E-05
75-71-8 Dichlorodifluoromethane 2.94 0.0882 -2.1E+01 8.5E-04
75-34-3 Dichloroethane, 1,1-2.86 0.0858 1.8E+00 -4.9E-08
107-06-2 Dichloroethane, 1,2-0.539 0.01617 1.1E-01 1.5E+00 1.5E-07 2.2E-03
156-60-5 Dichloroethylene, trans-1,2-0.311 0.00933 -8.3E+00 2.2E-04
100-41-4 Ethylbenzene 35.5 1.065 1.1E+00 2.1E+02 9.5E-07 1.0E-03
142-82-5 Heptane, N-45 1.35 -8.3E+01 3.2E-03
87-68-3 Hexachlorobutadiene 2.1 0.063 1.3E-01 -4.9E-07
110-54-3 Hexane, N-86.7 2.601 -1.5E+02 3.6E-03
591-78-6 Hexanone, 2-4.02 0.1206 -6.3E+00 3.9E-03
67-63-0 Isopropanol 50.6 1.518 -4.2E+01 7.3E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone)150 4.5 -1.0E+03 8.6E-04
75-09-2 Methylene Chloride 3.75 0.1125 1.0E+02 1.3E+02 1.1E-09 1.8E-04
91-20-3 ~Naphthalene 29.5 0.885 8.3E-02 6.3E-01 1.1E-05 2.8E-01
115-07-1 Propylene 666 19.98 -6.3E+02 6.4E-03
100-42-5 Styrene 2.54 0.0762 -2.1E+02 7.3E-05
127-18-4 Tetrachloroethylene 17.2 0.516 1.1E+01 8.3E+00 4.8E-08 1.2E-02
108-88-3 Toluene 7570 227.1 -1.0E+03 4.4E-02
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-1.89 0.0567 -1.0E+03 1.1E-05
120-82-1 Trichlorobenzene, 1,2,4-1.74 0.0522 -4.2E-01 2.5E-02
71-55-6 Trichloroethane, 1,1,1-0.475 0.01425 -1.0E+03 2.7E-06
79-01-6 Trichloroethylene 0.421 0.01263 4.8E-01 4.2E-01 2.6E-08 6.1E-03
75-69-4 Trichlorofluoromethane 30.7 0.921 --
95-63-6 Trimethylbenzene, 1,2,4-3.28 0.0984 -1.3E+01 1.6E-03
108-67-8 Trimethylbenzene, 1,3,5-0.854 0.02562 -1.3E+01 4.1E-04
75-01-4 Vinyl Chloride 0.964 0.02892 1.7E-01 2.1E+01 1.7E-07 2.8E-04
1330-20-7 Xylenes 847 25.41 -2.1E+01 2.4E-01
Cumulative:1.4E-05 6.6E-01
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 25091-21-060
Exposure Unit ID: C
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 150 1.5 --
71-43-2 Benzene 7.06 0.0706 1.6E+00 2.6E+01 4.5E-08 5.4E-04
75-15-0 Carbon Disulfide 120 1.2 -6.1E+02 3.9E-04
56-23-5 Carbon Tetrachloride 3.14 0.0314 2.0E+00 8.8E+01 1.5E-08 7.2E-05
67-66-3 Chloroform 0.891 0.00891 5.3E-01 8.6E+01 1.7E-08 2.1E-05
74-87-3 Chloromethane 1.77 0.0177 -7.9E+01 4.5E-05
98-82-8 Cumene 5.41 0.0541 -3.5E+02 3.1E-05
110-83-8 Cyclohexene 1.29 0.0129 -8.8E+02 2.9E-06
75-71-8 Dichlorodifluoromethane 2.94 0.0294 -8.8E+01 6.7E-05
75-34-3 Dichloroethane, 1,1-2.86 0.0286 7.7E+00 -3.7E-09
107-06-2 Dichloroethane, 1,2-0.539 0.00539 4.7E-01 6.1E+00 1.1E-08 1.8E-04
156-60-5 Dichloroethylene, trans-1,2-0.311 0.00311 -3.5E+01 1.8E-05
100-41-4 Ethylbenzene 35.5 0.355 4.9E+00 8.8E+02 7.2E-08 8.1E-05
142-82-5 Heptane, N-45 0.45 -3.5E+02 2.6E-04
87-68-3 Hexachlorobutadiene 2.1 0.021 5.6E-01 -3.8E-08
110-54-3 Hexane, N-86.7 0.867 -6.1E+02 2.8E-04
591-78-6 Hexanone, 2-4.02 0.0402 -2.6E+01 3.1E-04
67-63-0 Isopropanol 50.6 0.506 -1.8E+02 5.8E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)150 1.5 -4.4E+03 6.8E-05
75-09-2 Methylene Chloride 3.75 0.0375 1.2E+03 5.3E+02 3.1E-11 1.4E-05
91-20-3 ~Naphthalene 29.5 0.295 3.6E-01 2.6E+00 8.2E-07 2.2E-02
115-07-1 Propylene 666 6.66 -2.6E+03 5.1E-04
100-42-5 Styrene 2.54 0.0254 -8.8E+02 5.8E-06
127-18-4 Tetrachloroethylene 17.2 0.172 4.7E+01 3.5E+01 3.6E-09 9.8E-04
108-88-3 Toluene 7570 75.7 -4.4E+03 3.5E-03
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-1.89 0.0189 -4.4E+03 8.6E-07
120-82-1 Trichlorobenzene, 1,2,4-1.74 0.0174 -1.8E+00 2.0E-03
71-55-6 Trichloroethane, 1,1,1-0.475 0.00475 -4.4E+03 2.2E-07
79-01-6 Trichloroethylene 0.421 0.00421 3.0E+00 1.8E+00 1.4E-09 4.8E-04
75-69-4 Trichlorofluoromethane 30.7 0.307 --
95-63-6 Trimethylbenzene, 1,2,4-3.28 0.0328 -5.3E+01 1.2E-04
108-67-8 Trimethylbenzene, 1,3,5-0.854 0.00854 -5.3E+01 3.2E-05
75-01-4 Vinyl Chloride 0.964 0.00964 2.8E+00 8.8E+01 3.5E-09 2.2E-05
1330-20-7 Xylenes 847 8.47 -8.8E+01 1.9E-02
Cumulative:1.0E-06 5.2E-02
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator