25008_North Hills Expansion_redevelopmnt_20230920

REDEVELOPMENT SUMMARY REPORT
NORTH HILLS EXPANSION (NHX)
LASSITER MILL ROAD
RALEIGH, NORTH CAROLINA
BROWNFIELDS PROJECT NUMBER: 25008-21-092

Prepared for:

NC Department of Environmental Quality
Division of Waste Management
Brownfields Program
217 W Jones St.
Raleigh, NC 27699

Prepared by:

Aptus Management, PLLC
162 Mystic Lane
Pittsboro, NC 27312

NC Firm Engineering License # P-1130

John Gallagher, P.E.

September 20, 2023

Table of Contents
1.0 General Information ........................................................................................................... Error! Bookmark not defined.
1.1 Introduction ............................................................................................................................................................... 1
1.2 Objective ..................................................................................................................................................................... 1
2.0 Field Activities ................................................................................................................................................................... 1
2.1 In-Situ Soil Assessment ............................................................................................................................................. 1
2.2 Heating Oil UST Removal ........................................................................................................................................ 2
2.3 Exported Soil .............................................................................................................................................................. 2
2.4 Vapor Intrusion Mitigation System ......................................................................................................................... 2
3.0 Conclusion .......................................................................................................................................................................... 2

Appendices

Appendix A Drawings
Appendix B Heating Oil UST Closure Oversight Summary
Appendix C Brownfield Soil Export Log

1 | Page

1.0 GENERAL INFORMATION

1.1 INTRODUCTION

The North Hills Expansion site (“subject site”) consists of four parcels and totals 8.63 acres of land located in North
Hills Mall on Lassiter Mill Road in Raleigh, North Carolina (Drawings 1 and 2). The subject site was formerly a vacant
JC Penney department store with adjacent parking lots and decks. The subject site is enrolled as a DEQ-designated
Brownfield Property (BPN#25008-21-092) and the Environmental Management Plan (EMP) was approved in April
2021.

Data collected during assessment activities associated with a nearby Brothers Cleaners dry cleaning operation and
a nearby Exxon gas station indicate that groundwater at the subject site had been impacted by releases originating
from these sites. The contaminants released from these sites were volatile organic compounds (VOCs) including
chlorinated solvents and petroleum compounds. Assessment activities conducted in association with the dry
cleaners by the Dry-Cleaning Solvent Cleanup Act Program have identified VOCs in soil gas at properties adjacent to
the subject site. A Soil Gas Assessment Report was authored by Mid-Atlantic in June 2021 included sub-slab and
exterior soil gas testing to provide ‘baseline’ data related to the potential for vapor intrusion and to help direct the
design of VI mitigation measures. This assessment identified the tetrachloroethylene (PCE) groundwater plume to
be moving to the southeast beneath the subject site.

The redevelopment of the site involves the construction of five structures known as Building P (parking),
Buildings U, T, Y (commercial office) and Building W (mixed use retail and residential) (Drawing 2). Buildings P,
U, T and Y are used for either parking or commercial office. There are no residential uses in these structures.
Building W has ground floor retail/leasing space with residential use on the floors above. Buildings P, U, T, and
Y have completed construction activities and pre-occupancy testing (Post-Construction/Pre-Occupancy VIMS
Report authored by Mid-Atlantic; August 9, 2023). Building W is still under construction and scheduled for
occupancy in first quarter 2024.

1.2 OBJECTIVE

In accordance with the approved EMP, this report documents environmentally-related activities since
redevelopment activities began.

2.0 FIELD ACTIVITIES

2.1 IN-SITU SOIL ASSESSMENT

Proctor Environmental Services, Inc. authored a Report of In-Situ Soil Assessment dated May 10, 2021 that detailed
soil assessment activities at the northwestern portion of the subject site. A total of 42 soil borings were sampled
over a four-day period on February 27, March 10, and April 5 and 6, 2021. The assessment found that the limited
and low-level detections of VOCs, SVOCs, and reported detections of arsenic and hexavalent chromium were
indicative of naturally occurring background concentrations and the soil is not expected to pose an unacceptable
risk with redevelopment of the site. The report indicated that excess fill from grading and construction activities may
be beneficially re-used at NCDOT project sites, NCDEQ approved off-site commercial/industrial locations, other
Brownfield sites, and municipal solid waste (MSW), construction/demolition (C&D), or land clearing/inert debris
(LCID) landfills.

2 | Page

2.2 HEATING OIL UST REMOVAL

During soil grading activities conducted at the southwestern portion of the site in September 2021, a heating oil UST
was encountered. The heating oil UST was removed on September 21, 2021 (Heating Oil UST Closure Oversight
Summary; Attachment A). A total of 267.42 tons of petroleum-impacted soil was excavated from under and around
the former heating oil UST and transported to Triangle Area Earth in Zebulon, North Carolina for disposal. A
representative soil sample was collected from the bottom of the excavation and submitted for laboratory analysis.
The soil sample was analyzed for VOCs according to Method 8260, semi-volatile organic compounds (SVOCs)
according to Method 8270, the Resource Conservation and Recovery Act (RCRA) metals, and total petroleum
hydrocarbons (TPH) diesel-range and gasoline-range organics (DRO and GRO respectively) by Method 8015C. None
of the concentrations detected in the soil sample exceed their respective IHSB Industrial/Commercial Preliminary
Soil Remediation Goals (PSRGs). Subsequent to the removal of the impacted soil and based upon the absence of
staining, petroleum odors, and the lack of PID (photoionization detector) readings in excess of 5 ppm (parts per
million) from the in-situ pit bottom soil, it was concluded that no residual heating oil contamination remains at the
site.

2.3 EXPORTED SOIL

Soil was exported from the subject site from June 2021 through October 2022. Exported soils were transported to
the Haul Brownfield Landfill (C&D landfill; 102,480 cubic yards [yd3]), Red Rock Disposal (C&D landfill; 2,592 yd3),
516 Cabarrus Street (Brownfield site; 7,138 yd3), Seaboard Station (Brownfield site; 1,752 yd3), East End Market
(Brownfield site; 10,622 yd3), and Triangle Area Earth (bioremediation soil farm; 192 yd3). A copy of the soil export
log is included as Attachment B.

2.4 VAPOR INTRUSION MITIGATION SYSTEM

In May 2021, sub-slab soil gas sampling activities were conducted at the subject site. These sampling activities are
summarized in the report Soil Gas Assessment Report, dated June 23, 2021 and authored by Mid-Atlantic Associates,
Inc. The presence and concentrations of the VOCs detected in soil gas and groundwater on and near the subject site
suggest that a vapor encroachment condition exists at the site. Therefore, a Vapor Intrusion Mitigation System
(VIMS) was constructed in conjunction with redevelopment of the subject site. The VIMS was constructed in
accordance with the Vapor Intrusion Mitigation System Design Submittal, Revision 3 dated December 21, 2021 (VIMS
Plan). This VIMS Plan was approved by the Brownfields Program (now known as Brownfields Redevelopment Section
(BRS)) on December 29, 2021. Addendum 1 to the VIMS Plan dated May 25, 2023 detailed the additional activities
associated with the indoor air sampling. This addendum was approved by the BRS on June 22, 2023. Mid-Atlantic
authored a Post-Construction/Pre-Occupancy VIMS Report dated August 9, 2023 summarizing activities associated
with the VIMS for portions of buildings P (partial), U, T and Y. Buildings P (partial), U, T, and Y received approval for
occupancy by the BRS on September 11, 2023.

3.0 CONCLUSION

This Redevelopment Summary report documents environmental activities conducted at the site since
redevelopment activities began and satisfies the requirements of the EMP. As summarized, these activities
include in-situ soil assessment, exporting soil, the removal of a heating oil UST, and the implementation of the
VIMS.

´
TOPOGRAPHIC SITE MAPJC PENNY NORTH HILLS REDEVELOPMENTLASSITER MILL ROADRALEIGH, NORTH CAROLINA
DRAWN BY:DATE:
ENG. CHECK:
JOB NO:
APPROVAL:
DRAFTCHECK:GIS NO:
DWG NO:
REFERENCES:
SCALE:
JUNE 2021
000R3746.02
3G-R3746.02-11
1. RALEIGH WEST, NC DIGITAL RASTER GRAPHICS, USGS. SCANNED FROM 1:24,000-SCALE WAKE, NC TOPOGRAPHIC MAPS, PUBLISHED 2019, USGS.2. INSET MAP DIGITAL DATA FROM 2002 NATIONAL TRANSPORTATION ATLAS, BUREAU OF TRANSPORTATION STATISTICS, WASHINGTON, D.C.3. PROPERTY BOUNDARY DATA FROM WAKE COUNTY GIS.
CONTOUR INTERVAL = 10 FEET
0 600 1,200Feet
SITE
1:12,000
KRC§¨¦I440§¨¦U70 §¨¦I40
§¨¦U64
WAKE
AREA SHOWNWITHIN WAKE COUNTY
DHN
DHNDHN
Lassiter Mill RoadRockingham StreetNCCGIA, NC911 Board
´
DRAWN BY:
DRAFT CHECK BY:
ENGINEER CHECK BY:
APPROVED BY:
BROWNFIELDS PROPERTY MAPNORTH HILLS EXPANSIONLASSITER MILL ROADRALEIGH, NORTH CAROLINA
REFERENCE: DATA FROM WAKE COUNTY GIS, NC ONEMAP, NCDOT.
DATE: JUNE 2021
JOB NO.: R3746.02
GIS NO.: 3G-R3746.02-2
DRAWING NO.: 2
Legend
Subject Property
Parcel Boundaries
1:1,200
0 100 200 Feet
DHN
DHN
DHN
KRC
5113 Yachtsman Court
Raleigh, North Carolina 27615
919-630-0721 January 23, 2023 Mr. John Gallagher Aptus Management 109 Amber Court Carrboro, North Carolina 27510 Subject: HEATING OIL UST CLOSURE OVERSIGHT SUMMARY NORTH HILLS EXPANSION PROJECT 1261, 4217, 0 AND 4381 LASSITER MILL ROAD RALEIGH, WAKE COUNTY, NORTH CAROLINA
BROWNFIELDS PROJECT NO. 25008-21-092
Dear Mr. Gallagher,
The North Hills Expansion redevelopment site (the Subject Site) consists of some or all of four (4) parcels and a total of 8.63 acres of land. This summary report is associated with the southwestern portion of the Subject Site, which consisted primarily of asphalt-covered parking areas for the former JC Penney’s department store. This limited assessment report provides the results of the in-situ soil assessment and impacted soil removal activities associated with a former heating oil underground storage tank (UST) encountered during planned Brownfield’s redevelopment activities associated with the above-referenced site. During soil grading activities conducted in the southwestern portion of the redevelopment project in September of 2021, a heating oil UST, likely associated with one of the former residences which once occupied that area of the site, was encountered. Upon removal of the UST, as shown in the photographs in Appendix A, petroleum odors were noted and Proctor Environmental Services, Inc. was contacted to oversee the removal and disposal of the adversely impacted soil. On September 21, 2021, sixteen (16) loads of petroleum-impacted soil were excavated from under and around the former heating oil UST and transported to Triangle Area Earth (NCDEQ Permit SRU600082) in Zebulon, North Carolina for disposal by land application. Soil transportation and disposal manifests are contained in Appendix B.
Heating Oil UST Closure Activities January 23, 2023 North Hills Expansion Project Page 2
Lassiter Mill Road
Raleigh, North Carolina

Subsequent to removal of the impacted soil, a representative soil sample, HO-UST-PB, was collected from the bottom of the excavation for laboratory analysis. The soil sample was placed in laboratory-provided glassware and shipped by overnight courier to Waypoint Analytical in Charlotte, North Carolina. In the laboratory the soil sample was analyzed for volatile organic compounds (VOCs) according to Method 8260, semi-volatile organic compounds (SVOCs) according to Method 8270, the RCRA metals and total petroleum hydrocarbons (TPH) diesel-range and gasoline-range organics (DRO and GRO respectively) by Analytical Method 8015C. As documented in Appendix C, the pit bottom soil sample exhibited 1.34 mg/Kg of TPH identified as gasoline range organics and 0.003 mg/Kg of naphthalene. In addition, arsenic was detected at a concentration of 1.59 mg/Kg, barium at 67.0 mg/Kg, chromium at 5.37 mg/Kg, lead at 9.75 mg/Kg and selenium at a concentration of 6.90 mg/Kg. None of these concentrations exceed their IHSB Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs).
Subsequent to the removal of the impacted soil and based upon the absence of staining, petroleum odors, the lack of PID readings in excess of 5 ppm from the in-situ pit bottom soil, it is our professional opinion that no residual heating oil contamination remains at the site. Therefore, no further assessment or remediation is necessary, and the site can be used for its intended purpose as a commercial property.
We appreciate the opportunity to provide our services. If you have any questions or need additional information, please feel free to contact me at [phone]. Best Regards,
PROCTOR ENVIRONMENTAL SERVICES, INC.
Thomas A. Proctor, P.G., RSM President Attachments: Appendix A - Site Photographs Appendix B –Soil Disposal Tickets Appendix C - Laboratory Analytical Results

APPENDIX A

HEATING OIL UST REMOVAL PHOTOGRAPHS

Photolog of Heating Oil UST Removal September 2021
North Hills Expansion Project Page 1
Raleigh, North Carolina

#1 – Heating Oil UST Wrapped in Plastic #2 – Removal of UST from Excavation
#3 – Heating Oil UST and Adjacent Retaining Wall #4 – Excavation of Impacted Soil by Retaining Wall
Photolog of Heating Oil UST Removal September 2021
North Hills Expansion Project Page 2
Raleigh, North Carolina

#5 – Vertical Soil Excavation to Check for Depth of Impacted Soil #6 – Dark Stained Soil, Indicating Heating Oil Impact
#7 – Excavation of Impacted Soil #8 – Loading of Trucks for Off-Site Disposal
Photolog of Heating Oil UST Removal September 2021
North Hills Expansion Project Page 3
Raleigh, North Carolina

#9 – Backfilling Excavation with Imported Fill Material #10 - Backfilling Excavation, Retaining Wall in Background
#11 – Backfilling Excavation. Lassiter Mill Road in Background #12 – Compacting Backfill and Bringing Excavation to Grade

APPENDIX B

SOIL DISPOSAL MANIFESTS

TRIANGLE AREA EARTH
CORPORATION
Certificate of Disposal
NCDEQ Permit SRU600082
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
Triangle Area Earth Corporation, operating under Permit SRU600082, hereby
acknowledges the receipt of 26 7 .42 tons of soil contaminated with petroleum
hydrocarbons ~and will properly execute the disposal of this soil in the prescribed manner
set forth by the North Carolina Department of Environmental Quality, Division of Waste
Management in accordance with the requirements of SRU600082.
CLIENT
GENERATOR
TRANSPORTER
DATE(S) ACCEPTED
CERTIFICATION BY
TRIANGLE AREA
EARTH CORPORATION
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
Site: 4000 Center at North Hills
Raleigh, NC 27609
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
September 21, 2021
Laura Buchanan 9/21/2021
Printed Name Date
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESORIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE non-hazardous
CLASS/FICA T/ON
DOT HAZARD CLASS non-regulated
TRUCK 15412
CONTAMINANT heating oil
GENERATOR
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
SITE
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
CLIENT
NAME Sullivan Eastern, Inc.
ADDRESS 2860 C Slater Road
Morrisville, NC 27560
PHONE [phone] .
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 1
GROSS(LBS) 67340
TARE (LBS) 27480
NET(LBS) 39860
TONS 19.93
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE non-hazardous
CLASS/FICA TION
DOT HAZARD CLASS non-regulated
TRUCK 15410
CONTAMINANT heating oil
GENERATOR
NAME
ADDRESS
SITE
NAME
ADDRESS
CLIENT
NAME
ADDRESS
PHONE
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
[phone]
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 2
GROSS (LBS) 64220
TARE (LBS) 28020
NET(LBS) 36200
TONS 18.10
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 c Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE. non-hazardous
CLASS/FICA TION
DOT HAZARD CLASS non-regulated
TRUCK 15415
CONTAMINANT heating oil
GENERATOR
NAME
ADDRESS
SITE
NAME
ADDRESS
CLIENT
NAME
ADDRESS
PHONE
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
[phone]
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 3
GROSS(LBS) 70500
TARE (LBS) 27960
NET(LBS) 42540
TONS 21.27
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
~~Ci3~
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE
CLASS/FICA TION
non-hazardous
DOT HAZARD CLASS non-regulated
TRUCK 15402
CONTAMINANT heating oil
GENERATOR
NAME NHX Heating Oil UST Site
ADDRESS • 4000 Center at North Hills
SITE
NAME
ADDRESS
CLIENT
NAME
ADDRESS
PHONE
Raleigh, NC 27609
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
• [phone]
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 4
GROSS(LBS) 70720
TARE (LBS) 30220
NET(LBS) 40500
TONS 20.25
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE
CLASS/FICA TION
non-hazardous
DOT HAZARD CLASS non-regulated
TRUCK 15415
CONTAMINANT heating oil
GENERATOR
NAME ,. NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
SITE
NAME
ADDRESS
CLIENT
NAME
ADDRESS
PHONE
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
[phone]
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 5
GROSS (LBS) 66160
TARE (LBS) 27960
NET(LBS) 38200
TONS 19.10
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
~~CE>~
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE
CLASSIFICATION
non-hazardous
DOT HAZARD CLASS non-regulated
TRUCK 15412
CONTAMINANT heating oil
GENERATOR
NAME
ADDRESS
SITE
NAME
ADDRESS
CLIENT
NAME
ADDRESS
PHONE
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
[phone]
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 6
GROSS(LBS) 60420
TARE (LBS) 27480
NET(LBS) 32940
TONS 16.47
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021 ..
EPA WASTE non-hazardous
CLASS/FICA TION
DOT HAZARD CLASS non-regulated
TRUCK 15410
CONTAMINANT heating oil
GENERATOR
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
.
SITE
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
CLIENT
NAME Sullivan Eastern, Inc.
ADDRESS 2860 C Slater Road
Morrisville, NC 27560
PHONE [phone]
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 7
GROSS(LBS) 63060
TARE (LBS) 28020
NET(LBS) 35040
TONS 17.52
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE non-hazardous
CLASS/FICA TION
DOT HAZARD CLASS non-regulated
TRUCK 15402
CONTAMINANT heating oil
GENERATOR
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
SITE
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
CLIENT
NAME Sullivan Eastern, Inc.
ADDRESS 2860 C Slater Road
Morrisville, NC 27560
PHONE [phone]
{919) 980-6200
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 8
GROSS(LBS) 65520
TARE (LBS) 30220
NET(LBS) 35300
TONS 17.65
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
~~Ci3~
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE non-hazardous
CLASS/FICA TION
DOT HAZARD CLASS non-regulated
TRUCK 15415
CONTAMINANT heating oil
GENERATOR
NAME
ADDRESS
SITE
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
CLIENT
NAME
ADDRESS
PHONE
• Raleigh, NC 27609
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
[phone]
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 9
GROSS (LBS) . 54920
TARE (LBS) 27960
NET (LBS) 26960
TONS 13.48
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE
CLASS/FICA TION
non-hazardous
DOT HAZARD CLASS non-regulated
TRUCK 15412
CONTAMINANT heating oil
GENERATOR
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
• Raleigh, NC 27609
SITE
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
CLIENT
NAME Sullivan Eastern, Inc.
ADDRESS 2860 C Slater Road
Morrisville, NC 27560
PHONE (919} 484-0142
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 10
GROSS(LBS) 54620
TARE (LBS) 27480
NET(LBS) 27140
TONS 13.57
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
,.
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/218/21
EPA WASTE non-hazardous
CLASS/FICA TION
DOT HAZARD CLASS non-regulated
TRUCK 15410
CONTAMINANT heating oil
GENERATOR
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
SITE
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
CLIENT
NAME • Sullivan Eastern, Inc.
ADDRESS 2860 C Slater Road
Morrisville, NC 27560
PHONE [phone]
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 11
GROSS(LBS) 55620
TARE (LBS) 28020
NET(LBS) 27600
TONS 13.80
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
SIGNATURE
Laura Buchanan
PRINTED NAME
9/218/21
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE
CLASS/FICA TION
non-hazardous
..
DOT HAZARD CLASS non-regulated
TRUCK 15402
CONTAMINANT heating oil
GENERATOR
NAME
ADDRESS
SITE
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
NAME • NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
CLIENT
NAME
ADDRESS
PHONE
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
[phone]
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 12
GROSS(LBS) 63980
TARE (LBS) 30220
NET(LBS) 33760
TONS 16.88
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE non-hazardous
CLASS/FICA TION
DOT HAZARD CLASS non-regulated
TRUCK 15415
CONTAMINANT heating oil
GENERATOR
NAME • NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
SITE
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
CLIENT
NAME Sullivan Eastern, Inc.
ADDRESS 2860 C Slater Road
Morrisville, NC 27560
PHONE [phone]
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 13
GROSS(LBS) 55580
TARE (LBS) 27960
NET(LBS) 27620
TONS 13.81
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc .
2860 C Slater Road
Morrisville, NC 27560
CONSUtTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE non-hazardous
CLASS/FICA TION
DOT HAZARD CLASS non-regulated
TRUCK 15410
CONTAMINANT heating oil
GENERATOR
NAME
ADDRESS
SITE
NAME
ADDRESS
CLIENT
NAME
ADDRESS
PHONE
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
NHX Heating Oil UST Site
4000 Center at North Hills
Raleigh, NC 27609
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
[phone]
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 14
GROSS(LBS) 57360
TARE (LBS) 28020
NET(LBS) 29340
TONS 14.67
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
~~Cb~
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE non-hazardous
CLASS/FICA T/ON
DOT HAZARD CLASS non-regulated
TRUCK 15402
CONTAMINANT heating oil
GENERATOR
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
SITE
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
CLIENT
NAME Sullivan Eastern, Inc.
ADDRESS 2860 C Slater Road
Morrisville, NC 27560
PHONE {919) 484-0142
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 15
GROSS(LBS) 61680
TARE (LBS) 30220
NET(LBS) 31460
TONS 15.73
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
~0-ut\_oJCB~
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
Manifest •
NCDEQ Permit SRU600082
WASTE DESCRIPTION Petroleum-Contaminated Soil
DATE 9/21/2021
EPA WASTE non-hazardous
CLASS/FICA TION
DOT HAZARD CLASS non-regulated
TRUCK 15412
CONTAMINANT heating oil
GENERATOR
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
SITE
NAME NHX Heating Oil UST Site
ADDRESS 4000 Center at North Hills
Raleigh, NC 27609
CLIENT
NAME Sullivan Eastern, Inc.
ADDRESS 2860 C Slater Road
• Morrisville, NC 27560
PHONE {919) 484-0142
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST 16
GROSS(LBS) 57860
TARE (LBS) 27480
NET(LBS) 30380
TONS 15.19
TRANSPORTER
NAME
ADDRESS
Sullivan Eastern, Inc.
2860 C Slater Road
Morrisville, NC 27560
CONSULTANT
NAME
ADDRESS
Proctor Environmental Svcs.
5113 Yachtsman Court
Raleigh, NC 27615
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area Earth
Corporation:
~~Cb~
SIGNATURE
Laura Buchanan
PRINTED NAME
9/21/2021
DATE
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Custom~r
_ J5L/JZ EW
Suni,Ja-0
Job
NORTH CAR.OUN.A
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
UWRA BUCHANAN 31739
INVALID UNLESS SIGNED
A
A T!R
~,~1ma-:tftJR'1nlD ·2022
266
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
{I)
67340 lb t3R
09/21/21 08: 56am
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
. PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
EW
.Transporter -'-~"""-~~ ......... ~....,..+-11-
Job ,~~~ t Us
NORTH CAROLIN.A
PUBLIC WElGHMASTER
LICENSE EXPIRES JUNE 30. 2022
LAURABUCHANAN 31739
INVALID UNLESS SIGNED
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
64220 lb GR
09/21/21 08:58am
NORTH CAROLINA -
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
Job
NORTH CAROUJ\I.A
PUBLIC WEIGHMASiER
LICENSE EXPIRES JUNE 30. 2022
LAURA BUCHANAN 31739
INVALID UNLESS stGNED
MOrtTH CAROLINA
R
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
0)
70500 lb GR
09/21i21 09:02.am
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL .W267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
L51/0z-EW Truck
Custorner :Se I I, v!2:£:;. &,d-
. Transporter ..&.,...l::~t:.:.7'.L..IA~~~~'-':---1
Job
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
IAURABUCHANAN 31739
INVALID UNLESS SIGNED
NOf.l.TH CAROt.lNA
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
70720 lb GR
09/21/21 09:21.am
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL .W267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck /,54J5 EW
Customer /5a!/l(IO.,f)&.J
Transporter cS1.2 ~ i!Pa/4.J
Job $)1J GJec tJ, tb'/ls
NORTH CAR.OUN.A
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
LAURA BUCHANAN 31739
INVALID UNLESS SIGNED
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
66160 lb GR
09/21/21 10:40am
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck ~
Customer S1 J I L v'c:::z::t) ~
.Transporterc5ul&,~~ _;/
Job 1-/faJ WJ/-ec rJ./+, lds
NORTH CAROLIN.A
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
LAURA BUCHANAN 31739
INVALID UNLESS SIGNED
•Or.tTH CAROLINA
H ST!R
J11ffl'l;;..~,2022
4'2"
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
60420 lb GR
09/21/21 10: 45arr1
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4'267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck /.c5 i/fJ EW
Customer S~IY-'11 Z cz:sf
Transporter ;i1../bCU2:E:a :sf , .(
Job //la!) CeA:ec N.~lls
NORTH CAROLIN.A
PUBLIC WEJGHMASTER
LICENSE EXPIRES JUNE 30, 2022,
LAURA BUCHANAN 31739
INVALID UNLESS SIGNED
A
R
0,2022
4'266
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
63060 lb GR
09/21/21 10: 48aro
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 44267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck t.5~EW
Customer S.a//41/<UJ &:I
.Transporter c:"5c,(u;.'1-t:J &J
Job i/td) Gnle.c N, ~1k
NORTH CAR.OUN.A
PUBLIC WEIGHMAS1'ER
LICENSE EXPIRES JUNE 30, 2022
lAURABUCHANAN 31739
INVALID UNLESS SlGNED
NOFtTH CAROl.lNA
2022
266
D
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
65520 lb GR
09/21/21 10: 58am
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck l54JS EW ·
Customer £d
Job
NORTH CAROLIN.A
PUBLICWEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022·
lJ\lJRA BUCHANAN 31739
INVALID UNLESS SIGNED
A
·-----·, 2022
~~fo,lt"I!'~ 4'2t6
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
54920 lb GR
09/21/21 12: 12Pni
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4'267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Trllck ~ EW
Customer cSuJ/w<J/1 &.,f
Job
NORTH CAROLIN.A
PUBUCWBGHMASTER
LICENSE EXPIRES JUNE 30. 2022
LAURABUCHANAN 31739
INVALID UNLESSSlGNED
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
<[i)
54620 lb GR
09/21/21 12: lE,Pm
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck t54tDEw
Customer S,//4;04 kl-
.Transporter 8,J//Wll} £:d ,/
J0b '/aft2 Gdec ,J, if Us
NORTH CAROLIN.A
PUBUCWEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
LAURA BUCHANAN 31739
INVALID UNLESSSlGNED
A
T!R
2
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
5~620 lb GR
1)9/21/21 12: 17Plfl
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
.Transporter :s,Jl;.,1fVt Zaer/
lftW Cedec cl.~~ Job
NORTH CAROLIN.A
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
LAURA BUCHANAN 31739
INVALID UNLESS SIGNED
NOftTH CAROLINA ,we !IOHMAST!R
Rttt::b1Rl:ll I ES JU E 30, 2022
,ROlft~IAtiDEi!rCM 4'266
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
63980 lb GR
09/21/21 12:32P~
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL iM267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck l~l/(J EW
Customer .-5, ,llt tho Co,5i
.Transporter 3v:lld0f\ CA:sf
Job ¼ft> G,,Jec N. fl"Jb
NORTH CAROLIN.A
PUBUCWEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
IAURABUCHANAN 31739
INVALID UNLESS SlGNED
NOr.tTH CAROt.lNA
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
55580 lb GR
09/21/21 02: IJ2Pll'I
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4'267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck l~YtD EW
Customer Sal/ata11 E4s./
.Transporter c)c,rl/4vaa Ca'il
J0b f&$t9Gdec ;J. J/11
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
57360 lb GR
09/21/21 02: 04Plf1
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Job
NORTH CAR.OUN.A
PUBLIC WEtGHMASTER
LICENSE EXPIRES JUNE 30. 2022·
uUJRABUCHANAN 31739
INVALID UNLESS SIGNED
NOF<TH CAROLINA
R
t 2022
4'266
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
61680 lb GR
09/21/21 02: 07Pf1
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck lt,'tfd EW
Customer SJ/4v(l,/'\ &o.-f:. ,
.Transporter Sul\ 1~d
Job 'flrl)Gri fe.r tJ , JJk
NORTH CAROLIN.A
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
LAURA BUCHANAN 31739
INVALID UNLESS SIGNED
MOftTH CAROt.lNA
R
0,2022
.. IC.a'!Tftlol 4'2ff
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
57860 lb GR
09/21/21 02: 29Pffl
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
TriJck //SL//@
Customer 3~ &0f ··
Job
NOR11i CAROLIN.A
PUBUCWEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
u\URABUCHANAN 31739
INVAIJDUNLESS SIGNED
NCDEQ Permit SRU6OOO82
[phone]
434 Denton Ln, Zebulon, NC 27597
27480 lb SR
09/21/21 09:04.am
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
.TransportercSt?Zu~ !;as/ .,/
JOb 1-tavCkder N.~1ts
NORTH CAR.OUN.A
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
IAURABUCHANAN 31739
INVALID UNLESS SIGNED
'
NOrtTH CAROLINA
R
022
2ff
NCDEQ Permit SRU600082
[phone] .
434 Denton Ln, Zebulon, NC 27597
27960 lb GR
0'3/21/21 09: 15arri
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4'267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer Jiiiic::~v,~~~-+-"----=::;;;__,;;;y....~
.Transporter s udi v'@(J c4
JOb t/fr[) Gd-er N • 1J.tk
NORTH CAROLINA
PUBUCWEIGHMASTER
LICENSE EXPIRES JUNE 30. 2022
LAURA BUCHANAN 31739
INVALID UNLESS SlGNED
R
, 2022
"*
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
28020 lb GR
09i21/21 09:12am
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Job
NORTH CAROLIN.A
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30. 2022
LAURA BUCHANAN 31739
INVALID UNLESS SIGNED
R
22
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
30220 lb GR
09/21/21 09: 30aw,
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED

APPENDIX C

ANALYTICAL LABORATORY REPORT

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/1/2021
Proctor Environmental Services, Inc. Tom Proctor
5113 Yachtsman Ct. Raleigh, NC, 27615
Ref: Analytical Testing
Lab Report Number: 21-265-0007 Client Project Description: NHX, Raleigh
Dear Tom Proctor:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/22/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 99
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-265-0007
Page 2 of 99
Report Number:
Sample Summary Table
Client Project Description:
21-265-0007
NHX, Raleigh
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
09/21/2021 09:00Solids 95801 B-83 09/22/2021 12:06
09/21/2021 10:30Solids 95802 B-90 09/22/2021 12:06
09/21/2021 11:25Solids 95803 B-94 09/22/2021 12:06
09/21/2021 09:00Solids 95805 A5(9)2'-3'09/22/2021 12:06 7199
09/21/2021 09:00Solids 95805 A5(9)2'-3'09/22/2021 12:06
09/21/2021 10:30Solids 95806 A5(8)2'-3'09/22/2021 12:06
09/21/2021 11:25Solids 95807 A5(7)2'-3'09/22/2021 12:06
09/21/2021 13:30Solids 95808 A5(4)2'-3'09/22/2021 12:06
09/21/2021 14:00Solids 95809 HO-UST-PB 09/22/2021 12:06
09/21/2021 11:25Solids 95975 B-73 09/22/2021 12:06
: Pace Analytical - Columbia, SC (Shealy), West Columbia, SC
Page 3 of 99
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-265-0007
Report Limit
Project:NHX, Raleigh
V 95801B-83
J0.008 09/23/2021 10:428260DAcetonemg/Kg - dry 0.003
0.008 09/23/2021 10:428260DTetrachloroethenemg/Kg - dry 0.001
21.2 09/23/2021 16:37SW-DRYWT Moisture %
V 95802B-90
J0.011 09/23/2021 11:108260DAcetonemg/Kg - dry 0.003
J0.0010 09/23/2021 11:108260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.002 09/23/2021 11:108260DTetrachloroethenemg/Kg - dry 0.001
23.5 09/23/2021 16:37SW-DRYWT Moisture %
V 95803B-94
0.032 09/23/2021 11:378260DAcetonemg/Kg - dry 0.002
J0.001 09/23/2021 11:378260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
19.9 09/23/2021 16:37SW-DRYWT Moisture %
V 95805A5(9)2'-3'
2.46 09/23/2021 21:086020BArsenicmg/Kg - dry 0.119
30.7 09/23/2021 21:086020BBariummg/Kg - dry 1.77
24.7 09/23/2021 21:086020BChromiummg/Kg - dry 0.366
14.9 09/23/2021 21:086020BLeadmg/Kg - dry 0.177
J1.91 09/23/2021 21:086020BSeleniummg/Kg - dry 1.14
0.0811 09/24/2021 15:207471BMercury (Total)mg/Kg - dry 0.0152
20.8 09/23/2021 13:48SW-DRYWT Moisture %
V 95806A5(8)2'-3'
1.41 09/23/2021 22:256020BArsenicmg/Kg - dry 0.125
39.9 09/23/2021 22:256020BBariummg/Kg - dry 1.86
13.1 09/23/2021 22:256020BChromiummg/Kg - dry 0.384
14.3 09/23/2021 22:256020BLeadmg/Kg - dry 0.186
4.10 09/23/2021 22:256020BSeleniummg/Kg - dry 1.19
24.6 09/23/2021 13:48SW-DRYWT Moisture %
V 95807A5(7)2'-3'
2.51 09/23/2021 22:316020BArsenicmg/Kg - dry 0.118
32.9 09/23/2021 22:316020BBariummg/Kg - dry 1.75
22.4 09/23/2021 22:316020BChromiummg/Kg - dry 0.362
18.4 09/23/2021 22:316020BLeadmg/Kg - dry 0.175
J2.20 09/23/2021 22:316020BSeleniummg/Kg - dry 1.13
Page 4 of 99
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-265-0007
Report Limit
Project:NHX, Raleigh
V 95807A5(7)2'-3'
20.0 09/23/2021 13:48SW-DRYWT Moisture %
V 95808A5(4)2'-3'
1.86 09/23/2021 22:386020BArsenicmg/Kg - dry 0.118
20.9 09/23/2021 22:386020BBariummg/Kg - dry 1.75
16.8 09/23/2021 22:386020BChromiummg/Kg - dry 0.362
35.8 09/23/2021 22:386020BLeadmg/Kg - dry 0.175
J1.22 09/23/2021 22:386020BSeleniummg/Kg - dry 1.13
20.1 09/23/2021 13:48SW-DRYWT Moisture %
V 95809HO-UST-PB
1.59 09/23/2021 22:576020BArsenicmg/Kg - dry 0.112
67.0 09/23/2021 22:576020BBariummg/Kg - dry 1.67
5.37 09/23/2021 22:576020BChromiummg/Kg - dry 0.346
9.75 09/23/2021 22:576020BLeadmg/Kg - dry 0.167
6.90 09/23/2021 22:576020BSeleniummg/Kg - dry 1.08
JB1.34 09/24/2021 09:498015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 0.064
J0.003 09/23/2021 12:058260DAcetonemg/Kg - dry 0.002
J0.001 09/23/2021 12:058260DMethylene Chloride mg/Kg - dry 0.001
J0.003 09/23/2021 12:058260DNaphthalenemg/Kg - dry 0.001
16.4 09/23/2021 13:48SW-DRYWT Moisture %
V 95975B-73
1.03 09/23/2021 12:338260DBenzenemg/Kg - dry 0.021
5.93 09/23/2021 12:338260Dn-Butylbenzene mg/Kg - dry 0.018
5.91 09/23/2021 12:338260Dsec-Butyl benzene mg/Kg - dry 0.020
9.30 09/23/2021 12:338260DEthylbenzenemg/Kg - dry 0.021
3.24 09/23/2021 12:338260Dn-Hexane mg/Kg - dry 0.024
4.97 09/23/2021 12:338260DIsopropylbenzenemg/Kg - dry 0.016
5.38 09/23/2021 12:338260D4-Isopropyl toluene mg/Kg - dry 0.048
5.98 09/23/2021 12:338260DNaphthalenemg/Kg - dry 0.036
9.31 09/23/2021 12:338260Dn-Propylbenzene mg/Kg - dry 0.020
J0.050 09/23/2021 12:338260DTetrachloroethenemg/Kg - dry 0.033
13.5 09/23/2021 12:338260DToluenemg/Kg - dry 0.024
22.2 09/23/2021 13:018260D1,3,5-Trimethylbenzene mg/Kg - dry 0.200
17.1 09/23/2021 13:018260Do-Xylene mg/Kg - dry 0.185
33.0 09/23/2021 13:018260Dm,p-Xylene mg/Kg - dry 0.464
50.1 09/23/2021 13:018260DXylene (Total)mg/Kg - dry 0.185
Page 5 of 99
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-265-0007
Report Limit
Project:NHX, Raleigh
V 95975B-73
28.8 09/23/2021 16:37SW-DRYWT Moisture %
Page 6 of 99

Client: Proctor Environmental Services, Inc. CASE NARRATIVE
Project: NHX, Raleigh Lab Report Number: 21-265-0007
Date: 9/24/2021
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Ethyl Tertiary Butyl Ether QC Batch No: V9216/V9210
Analyte flagged for 0% recovery in LCS and/or LCSD due to the result being below the MQL. The actual results were 96.901ug/ and 92.785ug/L which calculates to a recovery of 97% and 93% which is within the acceptable
recovery range. Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: 2,4-Dinitrophenol
QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
1430 ug/kg which calculates to a recovery of 85.6% which is within the acceptable recovery range.
Sample 95746 Analyte: 2,4-Dinitrophenol
QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1440 ug/kg which calculates to a recovery of 86.6% which is within the acceptable recovery range.
Analyte: 2,4-Dinitrophenol QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1420 ug/kg which calculates to a recovery of 85% which is within the acceptable recovery range.
Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
1390 ug/kg which calculates to a recovery of 83.2% which is within the acceptable recovery range. Sample 95746 Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1340 ug/kg which calculates to a recovery of 80.6% which is within the acceptable recovery range. Analyte: 4,6-Dinitro-2-methylphenol QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1350 ug/kg which calculates to a recovery of 81% which is within the acceptable recovery range.
Analyte: 4-Nitrophenol QC Batch No: V9259/V9195 MS/MSD Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: 4-Nitrophenol
Page 7 of 99

QC Batch No: V9259/V9195
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 148 ug/kg which calculates to a recovery of 9% which is below the acceptable recovery range.
Analyte: Aniline
QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was
651 ug/kg which calculates to a recovery of 39% which is within the acceptable recovery range.
Analyte: Aniline QC Batch No: V9259/V9195
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 659 ug/kg which calculates to a recovery of 39.4% which is within the acceptable recovery range.
Analyte: Benzoic Acid
QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
1010 ug/kg which calculates to a recovery of 60.8% which is within the acceptable recovery range.
Sample 95746 Analyte: Benzoic Acid
QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1210 ug/kg which calculates to a recovery of 72.4% which is within the acceptable recovery range.
Analyte: Benzoic Acid QC Batch No: V9259/V9195
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 1180 ug/kg which calculates to a recovery of 70.6% which is within the acceptable recovery range. Analyte: Dibenz(a,h)anthracene QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
655 ug/kg which calculates to a recovery of 38.2% which is below the acceptable recovery range.
Sample 95746 Analyte: Dibenz(a,h)anthracene QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 632 ug/kg which calculates to a recovery of 37.8% which is below the acceptable recovery range.
Analyte: Dibenz(a,h)anthracene QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 624 ug/kg which calculates to a recovery of 37.4% which is within the acceptable recovery range. Analyte: Pyridine QC Batch No: V9259/V9195 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 188 ug/kg which calculates to a recovery of 11.2% which is within the acceptable recovery range. Analyte: Pyridine QC Batch No: V9259/V9195
Page 8 of 99

Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
175 ug/kg which calculates to a recovery of 10.5% which is within the acceptable recovery range.

Page 9 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-83
95801 Matrix:
9/21/2021 9:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.2 %Moisture 1 09/23/21 16:37 SW-DRYWTEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 10 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-83
95801 Matrix:
9/21/2021 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
0.008 J mg/Kg - dry 0.003 0.025Acetone 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.025
Acrolein 1 09/23/21 10:42 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 09/23/21 10:42 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/23/21 10:42 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/23/21 10:42 V9211TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/23/21 10:42 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/23/21 10:42 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/23/21 10:42 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/23/21 10:42 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/23/21 10:42 V9211TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/23/21 10:42 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/23/21 10:42 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/23/21 10:42 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/23/21 10:42 V9211TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/23/21 10:42 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/23/21 10:42 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-83
95801 Matrix:
9/21/2021 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/23/21 10:42 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 09/23/21 10:42 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/23/21 10:42 V9211TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/23/21 10:42 V9211TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/23/21 10:42 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/23/21 10:42 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/23/21 10:42 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/23/21 10:42 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/23/21 10:42 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 09/23/21 10:42 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/23/21 10:42 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 09/23/21 10:42 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/23/21 10:42 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-83
95801 Matrix:
9/21/2021 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/23/21 10:42 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Isopropylbenzene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/23/21 10:42 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/23/21 10:42 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/23/21 10:42 V9211TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 09/23/21 10:42 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/23/21 10:42 V9211TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/23/21 10:42 V9211TBL
0.008 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/23/21 10:42 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/23/21 10:42 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/23/21 10:42 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/23/21 10:42 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/23/21 10:42 V9211TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/23/21 10:42 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/23/21 10:42 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/23/21 10:42 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-83
95801 Matrix:
9/21/2021 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/23/21 10:42 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 09/23/21 10:42 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/23/21 10:42 V9211TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/23/21 10:42 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/23/21 10:42 V9211
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%09/23/21 10:421 TBL V9211
Surrogate: Dibromofluoromethane 103 Limits: 84-123%09/23/21 10:421 TBL V9211
Surrogate: Toluene-d8 99.0 Limits: 76-129%09/23/21 10:421 TBL V9211
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-90
95802 Matrix:
9/21/2021 10:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.5 %Moisture 1 09/23/21 16:37 SW-DRYWTEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 15 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-90
95802 Matrix:
9/21/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
0.011 J mg/Kg - dry 0.003 0.026Acetone 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.026
Acrolein 1 09/23/21 11:10 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 09/23/21 11:10 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/23/21 11:10 V9211TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 09/23/21 11:10 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 09/23/21 11:10 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/23/21 11:10 V9211TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/23/21 11:10 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/23/21 11:10 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 09/23/21 11:10 V9211TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/23/21 11:10 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 09/23/21 11:10 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-90
95802 Matrix:
9/21/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 09/23/21 11:10 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/23/21 11:10 V9211TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/23/21 11:10 V9211TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/23/21 11:10 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/23/21 11:10 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/23/21 11:10 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/23/21 11:10 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/23/21 11:10 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 09/23/21 11:10 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 09/23/21 11:10 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-90
95802 Matrix:
9/21/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 09/23/21 11:10 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Isopropylbenzene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/23/21 11:10 V9211TBL
0.0010 J mg/Kg - dry 0.0008 0.026Methyl Ethyl Ketone (MEK)1 09/23/21 11:10 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/23/21 11:10 V9211TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/23/21 11:10 V9211TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/23/21 11:10 V9211TBL
0.002 J mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/23/21 11:10 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 09/23/21 11:10 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/23/21 11:10 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/23/21 11:10 V9211TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 09/23/21 11:10 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/23/21 11:10 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-90
95802 Matrix:
9/21/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 09/23/21 11:10 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Chloride 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 09/23/21 11:10 V9211TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 09/23/21 11:10 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 09/23/21 11:10 V9211
Surrogate: 4-Bromofluorobenzene 95.0 Limits: 70-130%09/23/21 11:101 TBL V9211
Surrogate: Dibromofluoromethane 101 Limits: 84-123%09/23/21 11:101 TBL V9211
Surrogate: Toluene-d8 101 Limits: 76-129%09/23/21 11:101 TBL V9211
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-94
95803 Matrix:
9/21/2021 11:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.9 %Moisture 1 09/23/21 16:37 SW-DRYWTEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 20 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-94
95803 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
0.032 mg/Kg - dry 0.002 0.024Acetone 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 09/23/21 11:37 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 09/23/21 11:37 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/23/21 11:37 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/23/21 11:37 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/23/21 11:37 V9211TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/23/21 11:37 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/23/21 11:37 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/23/21 11:37 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/23/21 11:37 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 09/23/21 11:37 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/23/21 11:37 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/23/21 11:37 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/23/21 11:37 V9211TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/23/21 11:37 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/23/21 11:37 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-94
95803 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 09/23/21 11:37 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 09/23/21 11:37 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/23/21 11:37 V9211TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/23/21 11:37 V9211TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/23/21 11:37 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/23/21 11:37 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/23/21 11:37 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/23/21 11:37 V9211TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 09/23/21 11:37 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/23/21 11:37 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 09/23/21 11:37 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/23/21 11:37 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 09/23/21 11:37 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 09/23/21 11:37 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 09/23/21 11:37 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/23/21 11:37 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-94
95803 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 09/23/21 11:37 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Isopropylbenzene 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/23/21 11:37 V9211TBL
0.001 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 09/23/21 11:37 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/23/21 11:37 V9211TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 09/23/21 11:37 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/23/21 11:37 V9211TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/23/21 11:37 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/23/21 11:37 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/23/21 11:37 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/23/21 11:37 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/23/21 11:37 V9211TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/23/21 11:37 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/23/21 11:37 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/23/21 11:37 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-94
95803 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/23/21 11:37 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 09/23/21 11:37 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/23/21 11:37 V9211TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/23/21 11:37 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/23/21 11:37 V9211
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/23/21 11:371 TBL V9211
Surrogate: Dibromofluoromethane 101 Limits: 84-123%09/23/21 11:371 TBL V9211
Surrogate: Toluene-d8 98.4 Limits: 76-129%09/23/21 11:371 TBL V9211
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(9)2'-3'
95805 Matrix:
9/21/2021 9:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.8 %Moisture 1 09/23/21 13:48 SW-DRYWTBAM
2.46 mg/Kg - dry 0.119 1.26Arsenic 10 09/23/21 21:08 6020BEDV
30.7 mg/Kg - dry 1.77 12.6Barium 10 09/23/21 21:08 6020BEDV
<0.0694 mg/Kg - dry 0.0694 0.631Cadmium 10 09/23/21 21:08 6020BEDV
24.7 mg/Kg - dry 0.366 1.26Chromium 10 09/23/21 21:08 6020BEDV
14.9 mg/Kg - dry 0.177 1.26
Lead 10 09/23/21 21:08 6020BEDV
0.0811 mg/Kg - dry 0.0152 0.0379Mercury (Total)1 09/24/21 15:20 7471BEDV
1.91 J mg/Kg - dry 1.14 2.53Selenium 10 09/23/21 21:08 6020BEDV
<0.0517 mg/Kg - dry 0.0517 0.631Silver 10 09/23/21 21:08 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 25 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(9)2'-3'
95805 Matrix:
9/21/2021 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.146 mg/Kg - dry 0.146 0.834Acenaphthene 1 09/23/21 20:29 V9259JMV
<0.132 mg/Kg - dry 0.132 0.834
Acenaphthylene 1 09/23/21 20:29 V9259JMV
<0.191 mg/Kg - dry 0.191 0.834Aniline 1 09/23/21 20:29 V9259JMV
<0.180 mg/Kg - dry 0.180 0.834Anthracene 1 09/23/21 20:29 V9259JMV
<0.175 mg/Kg - dry 0.175 0.834Benzo(a)anthracene 1 09/23/21 20:29 V9259JMV
<0.185 mg/Kg - dry 0.185 0.834Benzo(a)pyrene 1 09/23/21 20:29 V9259JMV
<0.184 mg/Kg - dry 0.184 0.834Benzo(b)fluoranthene 1 09/23/21 20:29 V9259JMV
<0.171 mg/Kg - dry 0.171 0.834Benzo(g,h,i)perylene 1 09/23/21 20:29 V9259JMV
<0.172 mg/Kg - dry 0.172 0.834
Benzo(k)fluoranthene 1 09/23/21 20:29 V9259JMV
<0.732 mg/Kg - dry 0.732 2.53Benzoic Acid 1 09/23/21 20:29 V9259JMV
<0.132 mg/Kg - dry 0.132 0.834Benzyl alcohol 1 09/23/21 20:29 V9259JMV
<0.148 mg/Kg - dry 0.148 0.834Bis(2-Chloroethoxy)methane 1 09/23/21 20:29 V9259JMV
<0.135 mg/Kg - dry 0.135 0.834Bis(2-Chloroethyl)ether 1 09/23/21 20:29 V9259JMV
<0.171 mg/Kg - dry 0.171 0.416Bis(2-Chloroisopropyl)ether 1 09/23/21 20:29 V9259JMV
<0.151 mg/Kg - dry 0.151 0.834Bis(2-ethylhexyl)phthalate 1 09/23/21 20:29 V9259JMV
<0.137 mg/Kg - dry 0.137 0.8344-Bromophenyl phenyl ether 1 09/23/21 20:29 V9259JMV
<0.142 mg/Kg - dry 0.142 0.416Butyl benzyl phthalate 1 09/23/21 20:29 V9259JMV
<0.116 mg/Kg - dry 0.116 0.8344-Chloro-3-methylphenol 1 09/23/21 20:29 V9259JMV
<0.141 mg/Kg - dry 0.141 0.4164-Chloroaniline 1 09/23/21 20:29 V9259JMV
<0.146 mg/Kg - dry 0.146 0.8342-Chloronaphthalene 1 09/23/21 20:29 V9259JMV
<0.124 mg/Kg - dry 0.124 0.8342-Chlorophenol 1 09/23/21 20:29 V9259JMV
<0.159 mg/Kg - dry 0.159 1.264-Chlorophenyl phenyl ether 1 09/23/21 20:29 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(9)2'-3'
95805 Matrix:
9/21/2021 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.179 mg/Kg - dry 0.179 0.834Chrysene 1 09/23/21 20:29 V9259JMV
<0.290 mg/Kg - dry 0.290 0.834
Dibenz(a,h)anthracene 1 09/23/21 20:29 V9259JMV
<0.150 mg/Kg - dry 0.150 0.834Dibenzofuran 1 09/23/21 20:29 V9259JMV
<0.119 mg/Kg - dry 0.119 0.8341,2-Dichlorobenzene 1 09/23/21 20:29 V9259JMV
<0.122 mg/Kg - dry 0.122 0.8341,3-Dichlorobenzene 1 09/23/21 20:29 V9259JMV
<0.123 mg/Kg - dry 0.123 0.4161,4-Dichlorobenzene 1 09/23/21 20:29 V9259JMV
<0.185 mg/Kg - dry 0.185 0.8343,3'-Dichlorobenzidine 1 09/23/21 20:29 V9259JMV
<0.121 mg/Kg - dry 0.121 0.8342,4-Dichlorophenol 1 09/23/21 20:29 V9259JMV
<0.227 mg/Kg - dry 0.227 0.834
Diethyl phthalate 1 09/23/21 20:29 V9259JMV
<0.219 mg/Kg - dry 0.219 0.834Dimethyl phthalate 1 09/23/21 20:29 V9259JMV
<0.136 mg/Kg - dry 0.136 0.4162,4-Dimethylphenol 1 09/23/21 20:29 V9259JMV
<0.135 mg/Kg - dry 0.135 0.834Di-n-butyl phthalate 1 09/23/21 20:29 V9259JMV
<0.303 mg/Kg - dry 0.303 1.894,6-Dinitro-2-methylphenol 1 09/23/21 20:29 V9259JMV
<0.656 mg/Kg - dry 0.656 1.892,4-Dinitrophenol 1 09/23/21 20:29 V9259JMV
<0.122 mg/Kg - dry 0.122 0.8342,4-Dinitrotoluene 1 09/23/21 20:29 V9259JMV
<0.136 mg/Kg - dry 0.136 0.8342,6-Dinitrotoluene 1 09/23/21 20:29 V9259JMV
<0.180 mg/Kg - dry 0.180 0.416Di-n-Octyl Phthalate 1 09/23/21 20:29 V9259JMV
<0.155 mg/Kg - dry 0.155 0.834Fluoranthene 1 09/23/21 20:29 V9259JMV
<0.161 mg/Kg - dry 0.161 0.834Fluorene 1 09/23/21 20:29 V9259JMV
<0.133 mg/Kg - dry 0.133 0.834Hexachlorobenzene 1 09/23/21 20:29 V9259JMV
<0.123 mg/Kg - dry 0.123 0.834Hexachlorobutadiene 1 09/23/21 20:29 V9259JMV
<0.198 mg/Kg - dry 0.198 0.834Hexachlorocyclopentadiene 1 09/23/21 20:29 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(9)2'-3'
95805 Matrix:
9/21/2021 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.100 mg/Kg - dry 0.100 0.834Hexachloroethane 1 09/23/21 20:29 V9259JMV
<0.226 mg/Kg - dry 0.226 0.834
Indeno(1,2,3-cd)pyrene 1 09/23/21 20:29 V9259JMV
<0.241 mg/Kg - dry 0.241 0.834Isophorone 1 09/23/21 20:29 V9259JMV
<0.133 mg/Kg - dry 0.133 0.8341-Methylnaphthalene 1 09/23/21 20:29 V9259JMV
<0.126 mg/Kg - dry 0.126 0.8342-Methylnaphthalene 1 09/23/21 20:29 V9259JMV
<0.122 mg/Kg - dry 0.122 0.8342-Methylphenol 1 09/23/21 20:29 V9259JMV
<0.107 mg/Kg - dry 0.107 0.8343&4 Methylphenol 1 09/23/21 20:29 V9259JMV
<0.181 mg/Kg - dry 0.181 0.834Naphthalene 1 09/23/21 20:29 V9259JMV
<0.122 mg/Kg - dry 0.122 0.834
2-Nitroaniline 1 09/23/21 20:29 V9259JMV
<0.151 mg/Kg - dry 0.151 0.8343-Nitroaniline 1 09/23/21 20:29 V9259JMV
<0.117 mg/Kg - dry 0.117 0.4164-Nitroaniline 1 09/23/21 20:29 V9259JMV
<0.146 mg/Kg - dry 0.146 0.416Nitrobenzene 1 09/23/21 20:29 V9259JMV
<0.112 mg/Kg - dry 0.112 0.8342-Nitrophenol 1 09/23/21 20:29 V9259JMV
<0.147 mg/Kg - dry 0.147 0.8344-Nitrophenol 1 09/23/21 20:29 V9259JMV
<0.332 mg/Kg - dry 0.332 0.834N-Nitrosodimethylamine 1 09/23/21 20:29 V9259JMV
<0.228 mg/Kg - dry 0.228 0.834N-Nitrosodiphenylamine 1 09/23/21 20:29 V9259JMV
<0.148 mg/Kg - dry 0.148 0.834N-Nitroso-di-n-propylamine 1 09/23/21 20:29 V9259JMV
<0.438 mg/Kg - dry 0.438 1.26Pentachlorophenol 1 09/23/21 20:29 V9259JMV
<0.262 mg/Kg - dry 0.262 0.834Phenanthrene 1 09/23/21 20:29 V9259JMV
<0.141 mg/Kg - dry 0.141 0.834Phenol 1 09/23/21 20:29 V9259JMV
<0.169 mg/Kg - dry 0.169 0.834Pyrene 1 09/23/21 20:29 V9259JMV
<0.100 mg/Kg - dry 0.100 0.416Pyridine 1 09/23/21 20:29 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(9)2'-3'
95805 Matrix:
9/21/2021 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.135 mg/Kg - dry 0.135 0.8341,2,4-Trichlorobenzene 1 09/23/21 20:29 V9259JMV
<0.121 mg/Kg - dry 0.121 0.834
2,4,5-Trichlorophenol 1 09/23/21 20:29 V9259JMV
<0.122 mg/Kg - dry 0.122 0.8342,4,6-Trichlorophenol 1 09/23/21 20:29 V9259JMV
Surrogate: Phenol-d5 64.1 Limits: 34-121%09/23/21 20:291 JMV V9259
Surrogate: 2-Fluorobiphenyl 74.3 Limits: 44-115%09/23/21 20:291 JMV V9259
Surrogate: 2-Fluorophenol 65.6 Limits: 35-115%09/23/21 20:291 JMV V9259
Surrogate: Nitrobenzene-d5 64.1 Limits: 37-122%09/23/21 20:291 JMV V9259
Surrogate: 4-Terphenyl-d14 76.0 Limits: 54-127%09/23/21 20:291 JMV V9259
Surrogate: 2,4,6-Tribromophenol 101 Limits: 39-132%09/23/21 20:291 JMV V9259
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(8)2'-3'
95806 Matrix:
9/21/2021 10:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
24.6 %Moisture 1 09/23/21 13:48 SW-DRYWTBAM
1.41 mg/Kg - dry 0.125 1.33Arsenic 10 09/23/21 22:25 6020BEDV
39.9 mg/Kg - dry 1.86 13.3Barium 10 09/23/21 22:25 6020BEDV
<0.0729 mg/Kg - dry 0.0729 0.663Cadmium 10 09/23/21 22:25 6020BEDV
13.1 mg/Kg - dry 0.384 1.33Chromium 10 09/23/21 22:25 6020BEDV
14.3 mg/Kg - dry 0.186 1.33
Lead 10 09/23/21 22:25 6020BEDV
<0.0159 mg/Kg - dry 0.0159 0.0398Mercury (Total)1 09/24/21 15:52 7471BEDV
4.10 mg/Kg - dry 1.19 2.65Selenium 10 09/23/21 22:25 6020BEDV
<0.0543 mg/Kg - dry 0.0543 0.663Silver 10 09/23/21 22:25 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 30 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(8)2'-3'
95806 Matrix:
9/21/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.153 mg/Kg - dry 0.153 0.875Acenaphthene 1 09/23/21 20:51 V9259JMV
<0.139 mg/Kg - dry 0.139 0.875
Acenaphthylene 1 09/23/21 20:51 V9259JMV
<0.201 mg/Kg - dry 0.201 0.875Aniline 1 09/23/21 20:51 V9259JMV
<0.189 mg/Kg - dry 0.189 0.875Anthracene 1 09/23/21 20:51 V9259JMV
<0.184 mg/Kg - dry 0.184 0.875Benzo(a)anthracene 1 09/23/21 20:51 V9259JMV
<0.194 mg/Kg - dry 0.194 0.875Benzo(a)pyrene 1 09/23/21 20:51 V9259JMV
<0.193 mg/Kg - dry 0.193 0.875Benzo(b)fluoranthene 1 09/23/21 20:51 V9259JMV
<0.180 mg/Kg - dry 0.180 0.875Benzo(g,h,i)perylene 1 09/23/21 20:51 V9259JMV
<0.181 mg/Kg - dry 0.181 0.875
Benzo(k)fluoranthene 1 09/23/21 20:51 V9259JMV
<0.769 mg/Kg - dry 0.769 2.65Benzoic Acid 1 09/23/21 20:51 V9259JMV
<0.139 mg/Kg - dry 0.139 0.875Benzyl alcohol 1 09/23/21 20:51 V9259JMV
<0.156 mg/Kg - dry 0.156 0.875Bis(2-Chloroethoxy)methane 1 09/23/21 20:51 V9259JMV
<0.141 mg/Kg - dry 0.141 0.875Bis(2-Chloroethyl)ether 1 09/23/21 20:51 V9259JMV
<0.180 mg/Kg - dry 0.180 0.437Bis(2-Chloroisopropyl)ether 1 09/23/21 20:51 V9259JMV
<0.159 mg/Kg - dry 0.159 0.875Bis(2-ethylhexyl)phthalate 1 09/23/21 20:51 V9259JMV
<0.144 mg/Kg - dry 0.144 0.8754-Bromophenyl phenyl ether 1 09/23/21 20:51 V9259JMV
<0.149 mg/Kg - dry 0.149 0.437Butyl benzyl phthalate 1 09/23/21 20:51 V9259JMV
<0.122 mg/Kg - dry 0.122 0.8754-Chloro-3-methylphenol 1 09/23/21 20:51 V9259JMV
<0.148 mg/Kg - dry 0.148 0.4374-Chloroaniline 1 09/23/21 20:51 V9259JMV
<0.153 mg/Kg - dry 0.153 0.8752-Chloronaphthalene 1 09/23/21 20:51 V9259JMV
<0.130 mg/Kg - dry 0.130 0.8752-Chlorophenol 1 09/23/21 20:51 V9259JMV
<0.167 mg/Kg - dry 0.167 1.334-Chlorophenyl phenyl ether 1 09/23/21 20:51 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(8)2'-3'
95806 Matrix:
9/21/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.188 mg/Kg - dry 0.188 0.875Chrysene 1 09/23/21 20:51 V9259JMV
<0.305 mg/Kg - dry 0.305 0.875
Dibenz(a,h)anthracene 1 09/23/21 20:51 V9259JMV
<0.157 mg/Kg - dry 0.157 0.875Dibenzofuran 1 09/23/21 20:51 V9259JMV
<0.125 mg/Kg - dry 0.125 0.8751,2-Dichlorobenzene 1 09/23/21 20:51 V9259JMV
<0.129 mg/Kg - dry 0.129 0.8751,3-Dichlorobenzene 1 09/23/21 20:51 V9259JMV
<0.129 mg/Kg - dry 0.129 0.4371,4-Dichlorobenzene 1 09/23/21 20:51 V9259JMV
<0.194 mg/Kg - dry 0.194 0.8753,3'-Dichlorobenzidine 1 09/23/21 20:51 V9259JMV
<0.127 mg/Kg - dry 0.127 0.8752,4-Dichlorophenol 1 09/23/21 20:51 V9259JMV
<0.238 mg/Kg - dry 0.238 0.875
Diethyl phthalate 1 09/23/21 20:51 V9259JMV
<0.230 mg/Kg - dry 0.230 0.875Dimethyl phthalate 1 09/23/21 20:51 V9259JMV
<0.143 mg/Kg - dry 0.143 0.4372,4-Dimethylphenol 1 09/23/21 20:51 V9259JMV
<0.141 mg/Kg - dry 0.141 0.875Di-n-butyl phthalate 1 09/23/21 20:51 V9259JMV
<0.318 mg/Kg - dry 0.318 1.994,6-Dinitro-2-methylphenol 1 09/23/21 20:51 V9259JMV
<0.689 mg/Kg - dry 0.689 1.992,4-Dinitrophenol 1 09/23/21 20:51 V9259JMV
<0.128 mg/Kg - dry 0.128 0.8752,4-Dinitrotoluene 1 09/23/21 20:51 V9259JMV
<0.143 mg/Kg - dry 0.143 0.8752,6-Dinitrotoluene 1 09/23/21 20:51 V9259JMV
<0.189 mg/Kg - dry 0.189 0.437Di-n-Octyl Phthalate 1 09/23/21 20:51 V9259JMV
<0.163 mg/Kg - dry 0.163 0.875Fluoranthene 1 09/23/21 20:51 V9259JMV
<0.169 mg/Kg - dry 0.169 0.875Fluorene 1 09/23/21 20:51 V9259JMV
<0.140 mg/Kg - dry 0.140 0.875Hexachlorobenzene 1 09/23/21 20:51 V9259JMV
<0.129 mg/Kg - dry 0.129 0.875Hexachlorobutadiene 1 09/23/21 20:51 V9259JMV
<0.208 mg/Kg - dry 0.208 0.875Hexachlorocyclopentadiene 1 09/23/21 20:51 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 32 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(8)2'-3'
95806 Matrix:
9/21/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.105 mg/Kg - dry 0.105 0.875Hexachloroethane 1 09/23/21 20:51 V9259JMV
<0.237 mg/Kg - dry 0.237 0.875
Indeno(1,2,3-cd)pyrene 1 09/23/21 20:51 V9259JMV
<0.253 mg/Kg - dry 0.253 0.875Isophorone 1 09/23/21 20:51 V9259JMV
<0.140 mg/Kg - dry 0.140 0.8751-Methylnaphthalene 1 09/23/21 20:51 V9259JMV
<0.132 mg/Kg - dry 0.132 0.8752-Methylnaphthalene 1 09/23/21 20:51 V9259JMV
<0.128 mg/Kg - dry 0.128 0.8752-Methylphenol 1 09/23/21 20:51 V9259JMV
<0.112 mg/Kg - dry 0.112 0.8753&4 Methylphenol 1 09/23/21 20:51 V9259JMV
<0.190 mg/Kg - dry 0.190 0.875Naphthalene 1 09/23/21 20:51 V9259JMV
<0.128 mg/Kg - dry 0.128 0.875
2-Nitroaniline 1 09/23/21 20:51 V9259JMV
<0.159 mg/Kg - dry 0.159 0.8753-Nitroaniline 1 09/23/21 20:51 V9259JMV
<0.123 mg/Kg - dry 0.123 0.4374-Nitroaniline 1 09/23/21 20:51 V9259JMV
<0.153 mg/Kg - dry 0.153 0.437Nitrobenzene 1 09/23/21 20:51 V9259JMV
<0.117 mg/Kg - dry 0.117 0.8752-Nitrophenol 1 09/23/21 20:51 V9259JMV
<0.155 mg/Kg - dry 0.155 0.8754-Nitrophenol 1 09/23/21 20:51 V9259JMV
<0.348 mg/Kg - dry 0.348 0.875N-Nitrosodimethylamine 1 09/23/21 20:51 V9259JMV
<0.240 mg/Kg - dry 0.240 0.875N-Nitrosodiphenylamine 1 09/23/21 20:51 V9259JMV
<0.156 mg/Kg - dry 0.156 0.875N-Nitroso-di-n-propylamine 1 09/23/21 20:51 V9259JMV
<0.460 mg/Kg - dry 0.460 1.33Pentachlorophenol 1 09/23/21 20:51 V9259JMV
<0.275 mg/Kg - dry 0.275 0.875Phenanthrene 1 09/23/21 20:51 V9259JMV
<0.148 mg/Kg - dry 0.148 0.875Phenol 1 09/23/21 20:51 V9259JMV
<0.177 mg/Kg - dry 0.177 0.875Pyrene 1 09/23/21 20:51 V9259JMV
<0.105 mg/Kg - dry 0.105 0.437Pyridine 1 09/23/21 20:51 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 33 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(8)2'-3'
95806 Matrix:
9/21/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.141 mg/Kg - dry 0.141 0.8751,2,4-Trichlorobenzene 1 09/23/21 20:51 V9259JMV
<0.127 mg/Kg - dry 0.127 0.875
2,4,5-Trichlorophenol 1 09/23/21 20:51 V9259JMV
<0.128 mg/Kg - dry 0.128 0.8752,4,6-Trichlorophenol 1 09/23/21 20:51 V9259JMV
Surrogate: Phenol-d5 69.1 Limits: 34-121%09/23/21 20:511 JMV V9259
Surrogate: 2-Fluorobiphenyl 82.0 Limits: 44-115%09/23/21 20:511 JMV V9259
Surrogate: 2-Fluorophenol 72.1 Limits: 35-115%09/23/21 20:511 JMV V9259
Surrogate: Nitrobenzene-d5 72.5 Limits: 37-122%09/23/21 20:511 JMV V9259
Surrogate: 4-Terphenyl-d14 89.2 Limits: 54-127%09/23/21 20:511 JMV V9259
Surrogate: 2,4,6-Tribromophenol 115 Limits: 39-132%09/23/21 20:511 JMV V9259
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 34 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(7)2'-3'
95807 Matrix:
9/21/2021 11:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.0 %Moisture 1 09/23/21 13:48 SW-DRYWTBAM
2.51 mg/Kg - dry 0.118 1.25Arsenic 10 09/23/21 22:31 6020BEDV
32.9 mg/Kg - dry 1.75 12.5Barium 10 09/23/21 22:31 6020BEDV
<0.0687 mg/Kg - dry 0.0687 0.625Cadmium 10 09/23/21 22:31 6020BEDV
22.4 mg/Kg - dry 0.362 1.25Chromium 10 09/23/21 22:31 6020BEDV
18.4 mg/Kg - dry 0.175 1.25
Lead 10 09/23/21 22:31 6020BEDV
<0.0150 mg/Kg - dry 0.0150 0.0375Mercury (Total)1 09/24/21 17:01 7471BEDV
2.20 J mg/Kg - dry 1.13 2.50Selenium 10 09/23/21 22:31 6020BEDV
<0.0512 mg/Kg - dry 0.0512 0.625Silver 10 09/23/21 22:31 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 35 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(7)2'-3'
95807 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.145 mg/Kg - dry 0.145 0.825Acenaphthene 1 09/23/21 21:13 V9259JMV
<0.131 mg/Kg - dry 0.131 0.825
Acenaphthylene 1 09/23/21 21:13 V9259JMV
<0.190 mg/Kg - dry 0.190 0.825Aniline 1 09/23/21 21:13 V9259JMV
<0.178 mg/Kg - dry 0.178 0.825Anthracene 1 09/23/21 21:13 V9259JMV
<0.173 mg/Kg - dry 0.173 0.825Benzo(a)anthracene 1 09/23/21 21:13 V9259JMV
<0.183 mg/Kg - dry 0.183 0.825Benzo(a)pyrene 1 09/23/21 21:13 V9259JMV
<0.182 mg/Kg - dry 0.182 0.825Benzo(b)fluoranthene 1 09/23/21 21:13 V9259JMV
<0.170 mg/Kg - dry 0.170 0.825Benzo(g,h,i)perylene 1 09/23/21 21:13 V9259JMV
<0.171 mg/Kg - dry 0.171 0.825
Benzo(k)fluoranthene 1 09/23/21 21:13 V9259JMV
<0.725 mg/Kg - dry 0.725 2.50Benzoic Acid 1 09/23/21 21:13 V9259JMV
<0.131 mg/Kg - dry 0.131 0.825Benzyl alcohol 1 09/23/21 21:13 V9259JMV
<0.147 mg/Kg - dry 0.147 0.825Bis(2-Chloroethoxy)methane 1 09/23/21 21:13 V9259JMV
<0.133 mg/Kg - dry 0.133 0.825Bis(2-Chloroethyl)ether 1 09/23/21 21:13 V9259JMV
<0.170 mg/Kg - dry 0.170 0.412Bis(2-Chloroisopropyl)ether 1 09/23/21 21:13 V9259JMV
<0.150 mg/Kg - dry 0.150 0.825Bis(2-ethylhexyl)phthalate 1 09/23/21 21:13 V9259JMV
<0.136 mg/Kg - dry 0.136 0.8254-Bromophenyl phenyl ether 1 09/23/21 21:13 V9259JMV
<0.141 mg/Kg - dry 0.141 0.412Butyl benzyl phthalate 1 09/23/21 21:13 V9259JMV
<0.115 mg/Kg - dry 0.115 0.8254-Chloro-3-methylphenol 1 09/23/21 21:13 V9259JMV
<0.140 mg/Kg - dry 0.140 0.4124-Chloroaniline 1 09/23/21 21:13 V9259JMV
<0.145 mg/Kg - dry 0.145 0.8252-Chloronaphthalene 1 09/23/21 21:13 V9259JMV
<0.122 mg/Kg - dry 0.122 0.8252-Chlorophenol 1 09/23/21 21:13 V9259JMV
<0.157 mg/Kg - dry 0.157 1.254-Chlorophenyl phenyl ether 1 09/23/21 21:13 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 36 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(7)2'-3'
95807 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.177 mg/Kg - dry 0.177 0.825Chrysene 1 09/23/21 21:13 V9259JMV
<0.287 mg/Kg - dry 0.287 0.825
Dibenz(a,h)anthracene 1 09/23/21 21:13 V9259JMV
<0.148 mg/Kg - dry 0.148 0.825Dibenzofuran 1 09/23/21 21:13 V9259JMV
<0.118 mg/Kg - dry 0.118 0.8251,2-Dichlorobenzene 1 09/23/21 21:13 V9259JMV
<0.121 mg/Kg - dry 0.121 0.8251,3-Dichlorobenzene 1 09/23/21 21:13 V9259JMV
<0.121 mg/Kg - dry 0.121 0.4121,4-Dichlorobenzene 1 09/23/21 21:13 V9259JMV
<0.183 mg/Kg - dry 0.183 0.8253,3'-Dichlorobenzidine 1 09/23/21 21:13 V9259JMV
<0.119 mg/Kg - dry 0.119 0.8252,4-Dichlorophenol 1 09/23/21 21:13 V9259JMV
<0.225 mg/Kg - dry 0.225 0.825
Diethyl phthalate 1 09/23/21 21:13 V9259JMV
<0.217 mg/Kg - dry 0.217 0.825Dimethyl phthalate 1 09/23/21 21:13 V9259JMV
<0.135 mg/Kg - dry 0.135 0.4122,4-Dimethylphenol 1 09/23/21 21:13 V9259JMV
<0.133 mg/Kg - dry 0.133 0.825Di-n-butyl phthalate 1 09/23/21 21:13 V9259JMV
<0.300 mg/Kg - dry 0.300 1.884,6-Dinitro-2-methylphenol 1 09/23/21 21:13 V9259JMV
<0.650 mg/Kg - dry 0.650 1.882,4-Dinitrophenol 1 09/23/21 21:13 V9259JMV
<0.120 mg/Kg - dry 0.120 0.8252,4-Dinitrotoluene 1 09/23/21 21:13 V9259JMV
<0.135 mg/Kg - dry 0.135 0.8252,6-Dinitrotoluene 1 09/23/21 21:13 V9259JMV
<0.178 mg/Kg - dry 0.178 0.412Di-n-Octyl Phthalate 1 09/23/21 21:13 V9259JMV
<0.153 mg/Kg - dry 0.153 0.825Fluoranthene 1 09/23/21 21:13 V9259JMV
<0.160 mg/Kg - dry 0.160 0.825Fluorene 1 09/23/21 21:13 V9259JMV
<0.132 mg/Kg - dry 0.132 0.825Hexachlorobenzene 1 09/23/21 21:13 V9259JMV
<0.122 mg/Kg - dry 0.122 0.825Hexachlorobutadiene 1 09/23/21 21:13 V9259JMV
<0.196 mg/Kg - dry 0.196 0.825Hexachlorocyclopentadiene 1 09/23/21 21:13 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 37 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(7)2'-3'
95807 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.099 mg/Kg - dry 0.099 0.825Hexachloroethane 1 09/23/21 21:13 V9259JMV
<0.223 mg/Kg - dry 0.223 0.825
Indeno(1,2,3-cd)pyrene 1 09/23/21 21:13 V9259JMV
<0.238 mg/Kg - dry 0.238 0.825Isophorone 1 09/23/21 21:13 V9259JMV
<0.132 mg/Kg - dry 0.132 0.8251-Methylnaphthalene 1 09/23/21 21:13 V9259JMV
<0.125 mg/Kg - dry 0.125 0.8252-Methylnaphthalene 1 09/23/21 21:13 V9259JMV
<0.121 mg/Kg - dry 0.121 0.8252-Methylphenol 1 09/23/21 21:13 V9259JMV
<0.106 mg/Kg - dry 0.106 0.8253&4 Methylphenol 1 09/23/21 21:13 V9259JMV
<0.180 mg/Kg - dry 0.180 0.825Naphthalene 1 09/23/21 21:13 V9259JMV
<0.120 mg/Kg - dry 0.120 0.825
2-Nitroaniline 1 09/23/21 21:13 V9259JMV
<0.150 mg/Kg - dry 0.150 0.8253-Nitroaniline 1 09/23/21 21:13 V9259JMV
<0.116 mg/Kg - dry 0.116 0.4124-Nitroaniline 1 09/23/21 21:13 V9259JMV
<0.145 mg/Kg - dry 0.145 0.412Nitrobenzene 1 09/23/21 21:13 V9259JMV
<0.111 mg/Kg - dry 0.111 0.8252-Nitrophenol 1 09/23/21 21:13 V9259JMV
<0.146 mg/Kg - dry 0.146 0.8254-Nitrophenol 1 09/23/21 21:13 V9259JMV
<0.328 mg/Kg - dry 0.328 0.825N-Nitrosodimethylamine 1 09/23/21 21:13 V9259JMV
<0.226 mg/Kg - dry 0.226 0.825N-Nitrosodiphenylamine 1 09/23/21 21:13 V9259JMV
<0.147 mg/Kg - dry 0.147 0.825N-Nitroso-di-n-propylamine 1 09/23/21 21:13 V9259JMV
<0.433 mg/Kg - dry 0.433 1.25Pentachlorophenol 1 09/23/21 21:13 V9259JMV
<0.260 mg/Kg - dry 0.260 0.825Phenanthrene 1 09/23/21 21:13 V9259JMV
<0.140 mg/Kg - dry 0.140 0.825Phenol 1 09/23/21 21:13 V9259JMV
<0.167 mg/Kg - dry 0.167 0.825Pyrene 1 09/23/21 21:13 V9259JMV
<0.099 mg/Kg - dry 0.099 0.412Pyridine 1 09/23/21 21:13 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 38 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(7)2'-3'
95807 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.133 mg/Kg - dry 0.133 0.8251,2,4-Trichlorobenzene 1 09/23/21 21:13 V9259JMV
<0.120 mg/Kg - dry 0.120 0.825
2,4,5-Trichlorophenol 1 09/23/21 21:13 V9259JMV
<0.120 mg/Kg - dry 0.120 0.8252,4,6-Trichlorophenol 1 09/23/21 21:13 V9259JMV
Surrogate: Phenol-d5 66.7 Limits: 34-121%09/23/21 21:131 JMV V9259
Surrogate: 2-Fluorobiphenyl 80.8 Limits: 44-115%09/23/21 21:131 JMV V9259
Surrogate: 2-Fluorophenol 70.0 Limits: 35-115%09/23/21 21:131 JMV V9259
Surrogate: Nitrobenzene-d5 69.5 Limits: 37-122%09/23/21 21:131 JMV V9259
Surrogate: 4-Terphenyl-d14 82.6 Limits: 54-127%09/23/21 21:131 JMV V9259
Surrogate: 2,4,6-Tribromophenol 108 Limits: 39-132%09/23/21 21:131 JMV V9259
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 39 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(4)2'-3'
95808 Matrix:
9/21/2021 13:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.1 %Moisture 1 09/23/21 13:48 SW-DRYWTBAM
1.86 mg/Kg - dry 0.118 1.25Arsenic 10 09/23/21 22:38 6020BEDV
20.9 mg/Kg - dry 1.75 12.5Barium 10 09/23/21 22:38 6020BEDV
<0.0688 mg/Kg - dry 0.0688 0.626Cadmium 10 09/23/21 22:38 6020BEDV
16.8 mg/Kg - dry 0.362 1.25Chromium 10 09/23/21 22:38 6020BEDV
35.8 mg/Kg - dry 0.175 1.25
Lead 10 09/23/21 22:38 6020BEDV
<0.0150 mg/Kg - dry 0.0150 0.0375Mercury (Total)1 09/24/21 15:55 7471BEDV
1.22 J mg/Kg - dry 1.13 2.50Selenium 10 09/23/21 22:38 6020BEDV
<0.0513 mg/Kg - dry 0.0513 0.626Silver 10 09/23/21 22:38 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 40 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(4)2'-3'
95808 Matrix:
9/21/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.145 mg/Kg - dry 0.145 0.826Acenaphthene 1 09/23/21 21:36 V9259JMV
<0.131 mg/Kg - dry 0.131 0.826
Acenaphthylene 1 09/23/21 21:36 V9259JMV
<0.190 mg/Kg - dry 0.190 0.826Aniline 1 09/23/21 21:36 V9259JMV
<0.178 mg/Kg - dry 0.178 0.826Anthracene 1 09/23/21 21:36 V9259JMV
<0.173 mg/Kg - dry 0.173 0.826Benzo(a)anthracene 1 09/23/21 21:36 V9259JMV
<0.183 mg/Kg - dry 0.183 0.826Benzo(a)pyrene 1 09/23/21 21:36 V9259JMV
<0.182 mg/Kg - dry 0.182 0.826Benzo(b)fluoranthene 1 09/23/21 21:36 V9259JMV
<0.170 mg/Kg - dry 0.170 0.826Benzo(g,h,i)perylene 1 09/23/21 21:36 V9259JMV
<0.171 mg/Kg - dry 0.171 0.826
Benzo(k)fluoranthene 1 09/23/21 21:36 V9259JMV
<0.725 mg/Kg - dry 0.725 2.50Benzoic Acid 1 09/23/21 21:36 V9259JMV
<0.131 mg/Kg - dry 0.131 0.826Benzyl alcohol 1 09/23/21 21:36 V9259JMV
<0.147 mg/Kg - dry 0.147 0.826Bis(2-Chloroethoxy)methane 1 09/23/21 21:36 V9259JMV
<0.133 mg/Kg - dry 0.133 0.826Bis(2-Chloroethyl)ether 1 09/23/21 21:36 V9259JMV
<0.170 mg/Kg - dry 0.170 0.413Bis(2-Chloroisopropyl)ether 1 09/23/21 21:36 V9259JMV
<0.150 mg/Kg - dry 0.150 0.826Bis(2-ethylhexyl)phthalate 1 09/23/21 21:36 V9259JMV
<0.136 mg/Kg - dry 0.136 0.8264-Bromophenyl phenyl ether 1 09/23/21 21:36 V9259JMV
<0.141 mg/Kg - dry 0.141 0.413Butyl benzyl phthalate 1 09/23/21 21:36 V9259JMV
<0.115 mg/Kg - dry 0.115 0.8264-Chloro-3-methylphenol 1 09/23/21 21:36 V9259JMV
<0.140 mg/Kg - dry 0.140 0.4134-Chloroaniline 1 09/23/21 21:36 V9259JMV
<0.145 mg/Kg - dry 0.145 0.8262-Chloronaphthalene 1 09/23/21 21:36 V9259JMV
<0.122 mg/Kg - dry 0.122 0.8262-Chlorophenol 1 09/23/21 21:36 V9259JMV
<0.157 mg/Kg - dry 0.157 1.254-Chlorophenyl phenyl ether 1 09/23/21 21:36 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 41 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(4)2'-3'
95808 Matrix:
9/21/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.177 mg/Kg - dry 0.177 0.826Chrysene 1 09/23/21 21:36 V9259JMV
<0.287 mg/Kg - dry 0.287 0.826
Dibenz(a,h)anthracene 1 09/23/21 21:36 V9259JMV
<0.148 mg/Kg - dry 0.148 0.826Dibenzofuran 1 09/23/21 21:36 V9259JMV
<0.118 mg/Kg - dry 0.118 0.8261,2-Dichlorobenzene 1 09/23/21 21:36 V9259JMV
<0.121 mg/Kg - dry 0.121 0.8261,3-Dichlorobenzene 1 09/23/21 21:36 V9259JMV
<0.122 mg/Kg - dry 0.122 0.4131,4-Dichlorobenzene 1 09/23/21 21:36 V9259JMV
<0.183 mg/Kg - dry 0.183 0.8263,3'-Dichlorobenzidine 1 09/23/21 21:36 V9259JMV
<0.119 mg/Kg - dry 0.119 0.8262,4-Dichlorophenol 1 09/23/21 21:36 V9259JMV
<0.225 mg/Kg - dry 0.225 0.826
Diethyl phthalate 1 09/23/21 21:36 V9259JMV
<0.217 mg/Kg - dry 0.217 0.826Dimethyl phthalate 1 09/23/21 21:36 V9259JMV
<0.135 mg/Kg - dry 0.135 0.4132,4-Dimethylphenol 1 09/23/21 21:36 V9259JMV
<0.133 mg/Kg - dry 0.133 0.826Di-n-butyl phthalate 1 09/23/21 21:36 V9259JMV
<0.300 mg/Kg - dry 0.300 1.884,6-Dinitro-2-methylphenol 1 09/23/21 21:36 V9259JMV
<0.650 mg/Kg - dry 0.650 1.882,4-Dinitrophenol 1 09/23/21 21:36 V9259JMV
<0.120 mg/Kg - dry 0.120 0.8262,4-Dinitrotoluene 1 09/23/21 21:36 V9259JMV
<0.135 mg/Kg - dry 0.135 0.8262,6-Dinitrotoluene 1 09/23/21 21:36 V9259JMV
<0.178 mg/Kg - dry 0.178 0.413Di-n-Octyl Phthalate 1 09/23/21 21:36 V9259JMV
<0.153 mg/Kg - dry 0.153 0.826Fluoranthene 1 09/23/21 21:36 V9259JMV
<0.160 mg/Kg - dry 0.160 0.826Fluorene 1 09/23/21 21:36 V9259JMV
<0.132 mg/Kg - dry 0.132 0.826Hexachlorobenzene 1 09/23/21 21:36 V9259JMV
<0.122 mg/Kg - dry 0.122 0.826Hexachlorobutadiene 1 09/23/21 21:36 V9259JMV
<0.196 mg/Kg - dry 0.196 0.826Hexachlorocyclopentadiene 1 09/23/21 21:36 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 42 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(4)2'-3'
95808 Matrix:
9/21/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.099 mg/Kg - dry 0.099 0.826Hexachloroethane 1 09/23/21 21:36 V9259JMV
<0.224 mg/Kg - dry 0.224 0.826
Indeno(1,2,3-cd)pyrene 1 09/23/21 21:36 V9259JMV
<0.239 mg/Kg - dry 0.239 0.826Isophorone 1 09/23/21 21:36 V9259JMV
<0.132 mg/Kg - dry 0.132 0.8261-Methylnaphthalene 1 09/23/21 21:36 V9259JMV
<0.125 mg/Kg - dry 0.125 0.8262-Methylnaphthalene 1 09/23/21 21:36 V9259JMV
<0.121 mg/Kg - dry 0.121 0.8262-Methylphenol 1 09/23/21 21:36 V9259JMV
<0.106 mg/Kg - dry 0.106 0.8263&4 Methylphenol 1 09/23/21 21:36 V9259JMV
<0.180 mg/Kg - dry 0.180 0.826Naphthalene 1 09/23/21 21:36 V9259JMV
<0.121 mg/Kg - dry 0.121 0.826
2-Nitroaniline 1 09/23/21 21:36 V9259JMV
<0.150 mg/Kg - dry 0.150 0.8263-Nitroaniline 1 09/23/21 21:36 V9259JMV
<0.116 mg/Kg - dry 0.116 0.4134-Nitroaniline 1 09/23/21 21:36 V9259JMV
<0.145 mg/Kg - dry 0.145 0.413Nitrobenzene 1 09/23/21 21:36 V9259JMV
<0.111 mg/Kg - dry 0.111 0.8262-Nitrophenol 1 09/23/21 21:36 V9259JMV
<0.146 mg/Kg - dry 0.146 0.8264-Nitrophenol 1 09/23/21 21:36 V9259JMV
<0.329 mg/Kg - dry 0.329 0.826N-Nitrosodimethylamine 1 09/23/21 21:36 V9259JMV
<0.226 mg/Kg - dry 0.226 0.826N-Nitrosodiphenylamine 1 09/23/21 21:36 V9259JMV
<0.147 mg/Kg - dry 0.147 0.826N-Nitroso-di-n-propylamine 1 09/23/21 21:36 V9259JMV
<0.434 mg/Kg - dry 0.434 1.25Pentachlorophenol 1 09/23/21 21:36 V9259JMV
<0.260 mg/Kg - dry 0.260 0.826Phenanthrene 1 09/23/21 21:36 V9259JMV
<0.140 mg/Kg - dry 0.140 0.826Phenol 1 09/23/21 21:36 V9259JMV
<0.167 mg/Kg - dry 0.167 0.826Pyrene 1 09/23/21 21:36 V9259JMV
<0.099 mg/Kg - dry 0.099 0.413Pyridine 1 09/23/21 21:36 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 43 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:A5(4)2'-3'
95808 Matrix:
9/21/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.133 mg/Kg - dry 0.133 0.8261,2,4-Trichlorobenzene 1 09/23/21 21:36 V9259JMV
<0.120 mg/Kg - dry 0.120 0.826
2,4,5-Trichlorophenol 1 09/23/21 21:36 V9259JMV
<0.120 mg/Kg - dry 0.120 0.8262,4,6-Trichlorophenol 1 09/23/21 21:36 V9259JMV
Surrogate: Phenol-d5 69.7 Limits: 34-121%09/23/21 21:361 JMV V9259
Surrogate: 2-Fluorobiphenyl 84.4 Limits: 44-115%09/23/21 21:361 JMV V9259
Surrogate: 2-Fluorophenol 72.1 Limits: 35-115%09/23/21 21:361 JMV V9259
Surrogate: Nitrobenzene-d5 71.3 Limits: 37-122%09/23/21 21:361 JMV V9259
Surrogate: 4-Terphenyl-d14 86.2 Limits: 54-127%09/23/21 21:361 JMV V9259
Surrogate: 2,4,6-Tribromophenol 111 Limits: 39-132%09/23/21 21:361 JMV V9259
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 44 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:HO-UST-PB
95809 Matrix:
9/21/2021 14:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.4 %Moisture 1 09/23/21 13:48 SW-DRYWTBAM
1.59 mg/Kg - dry 0.112 1.20Arsenic 10 09/23/21 22:57 6020BEDV
67.0 mg/Kg - dry 1.67 12.0Barium 10 09/23/21 22:57 6020BEDV
<0.0657 mg/Kg - dry 0.0657 0.598Cadmium 10 09/23/21 22:57 6020BEDV
5.37 mg/Kg - dry 0.346 1.20Chromium 10 09/23/21 22:57 6020BEDV
9.75 mg/Kg - dry 0.167 1.20
Lead 10 09/23/21 22:57 6020BEDV
<0.0144 mg/Kg - dry 0.0144 0.0359Mercury (Total)1 09/24/21 15:57 7471BEDV
6.90 mg/Kg - dry 1.08 2.39Selenium 10 09/23/21 22:57 6020BEDV
<0.0490 mg/Kg - dry 0.0490 0.598Silver 10 09/23/21 22:57 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 45 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:HO-UST-PB
95809 Matrix:
9/21/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V9156 09/22/21 13:00
<5.62 mg/Kg - dry 5.62 12.1Diesel Range Organics (C10-C28)1 09/22/21 23:10 V9181ZRC
Surrogate: OTP Surrogate 66.7 Limits: 31-123%09/22/21 23:101 ZRC V9181
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V9212 09/24/21 08:00
1.34 JB mg/Kg - dry 0.064 7.81Gasoline Range Organics (C6-C10)50 09/24/21 09:49 V9213TBL
Surrogate: a,a,a-Trifluorotoluene 127 Limits: 50-137%09/24/21 09:4950 TBL V9213
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
0.003 J mg/Kg - dry 0.002 0.023Acetone 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 09/23/21 12:05 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 09/23/21 12:05 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 09/23/21 12:05 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.005Bromochloromethane 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 09/23/21 12:05 V9211TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 09/23/21 12:05 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 46 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:HO-UST-PB
95809 Matrix:
9/21/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 09/23/21 12:05 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.005
sec-Butyl benzene 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 09/23/21 12:05 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 09/23/21 12:05 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 09/23/21 12:05 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.011Chloromethane 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 09/23/21 12:05 V9211TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 09/23/21 12:05 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 09/23/21 12:05 V9211TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 09/23/21 12:05 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 09/23/21 12:05 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 09/23/21 12:05 V9211TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 09/23/21 12:05 V9211TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,3-Dichlorobenzene 1 09/23/21 12:05 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 09/23/21 12:05 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 09/23/21 12:05 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 47 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:HO-UST-PB
95809 Matrix:
9/21/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 09/23/21 12:05 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.005
cis-1,2-Dichloroethene 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 09/23/21 12:05 V9211TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 09/23/21 12:05 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 09/23/21 12:05 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 09/23/21 12:05 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.005
trans-1,3-Dichloropropene 1 09/23/21 12:05 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 09/23/21 12:05 V9211TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 09/23/21 12:05 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 09/23/21 12:05 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 09/23/21 12:05 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.005Isopropylbenzene 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 09/23/21 12:05 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 09/23/21 12:05 V9211TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 09/23/21 12:05 V9211TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 09/23/21 12:05 V9211TBL
0.001 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 09/23/21 12:05 V9211TBL
0.003 J mg/Kg - dry 0.001 0.011Naphthalene 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 09/23/21 12:05 V9211TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 48 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:HO-UST-PB
95809 Matrix:
9/21/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9210 09/23/21 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.005
1,1,1,2-Tetrachloroethane 1 09/23/21 12:05 V9211TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 09/23/21 12:05 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 09/23/21 12:05 V9211TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,1,2-Trichloroethane 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 09/23/21 12:05 V9211TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 09/23/21 12:05 V9211TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Acetate 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 09/23/21 12:05 V9211TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 09/23/21 12:05 V9211TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 09/23/21 12:05 V9211
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/23/21 12:051 TBL V9211
Surrogate: Dibromofluoromethane 101 Limits: 84-123%09/23/21 12:051 TBL V9211
Surrogate: Toluene-d8 98.1 Limits: 76-129%09/23/21 12:051 TBL V9211
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 49 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:HO-UST-PB
95809 Matrix:
9/21/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.138 mg/Kg - dry 0.138 0.790Acenaphthene 1 09/24/21 14:29 V9259JMV
<0.125 mg/Kg - dry 0.125 0.790
Acenaphthylene 1 09/24/21 14:29 V9259JMV
<0.181 mg/Kg - dry 0.181 0.790Aniline 1 09/24/21 14:29 V9259JMV
<0.171 mg/Kg - dry 0.171 0.790Anthracene 1 09/24/21 14:29 V9259JMV
<0.166 mg/Kg - dry 0.166 0.790Benzo(a)anthracene 1 09/24/21 14:29 V9259JMV
<0.175 mg/Kg - dry 0.175 0.790Benzo(a)pyrene 1 09/24/21 14:29 V9259JMV
<0.174 mg/Kg - dry 0.174 0.790Benzo(b)fluoranthene 1 09/24/21 14:29 V9259JMV
<0.162 mg/Kg - dry 0.162 0.790Benzo(g,h,i)perylene 1 09/24/21 14:29 V9259JMV
<0.163 mg/Kg - dry 0.163 0.790
Benzo(k)fluoranthene 1 09/24/21 14:29 V9259JMV
<0.693 mg/Kg - dry 0.693 2.39Benzoic Acid 1 09/24/21 14:29 V9259JMV
<0.125 mg/Kg - dry 0.125 0.790Benzyl alcohol 1 09/24/21 14:29 V9259JMV
<0.141 mg/Kg - dry 0.141 0.790Bis(2-Chloroethoxy)methane 1 09/24/21 14:29 V9259JMV
<0.127 mg/Kg - dry 0.127 0.790Bis(2-Chloroethyl)ether 1 09/24/21 14:29 V9259JMV
<0.162 mg/Kg - dry 0.162 0.394Bis(2-Chloroisopropyl)ether 1 09/24/21 14:29 V9259JMV
<0.143 mg/Kg - dry 0.143 0.790Bis(2-ethylhexyl)phthalate 1 09/24/21 14:29 V9259JMV
<0.130 mg/Kg - dry 0.130 0.7904-Bromophenyl phenyl ether 1 09/24/21 14:29 V9259JMV
<0.135 mg/Kg - dry 0.135 0.394Butyl benzyl phthalate 1 09/24/21 14:29 V9259JMV
<0.110 mg/Kg - dry 0.110 0.7904-Chloro-3-methylphenol 1 09/24/21 14:29 V9259JMV
<0.133 mg/Kg - dry 0.133 0.3944-Chloroaniline 1 09/24/21 14:29 V9259JMV
<0.138 mg/Kg - dry 0.138 0.7902-Chloronaphthalene 1 09/24/21 14:29 V9259JMV
<0.117 mg/Kg - dry 0.117 0.7902-Chlorophenol 1 09/24/21 14:29 V9259JMV
<0.150 mg/Kg - dry 0.150 1.204-Chlorophenyl phenyl ether 1 09/24/21 14:29 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 50 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:HO-UST-PB
95809 Matrix:
9/21/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.169 mg/Kg - dry 0.169 0.790Chrysene 1 09/24/21 14:29 V9259JMV
<0.275 mg/Kg - dry 0.275 0.790
Dibenz(a,h)anthracene 1 09/24/21 14:29 V9259JMV
<0.142 mg/Kg - dry 0.142 0.790Dibenzofuran 1 09/24/21 14:29 V9259JMV
<0.113 mg/Kg - dry 0.113 0.7901,2-Dichlorobenzene 1 09/24/21 14:29 V9259JMV
<0.116 mg/Kg - dry 0.116 0.7901,3-Dichlorobenzene 1 09/24/21 14:29 V9259JMV
<0.116 mg/Kg - dry 0.116 0.3941,4-Dichlorobenzene 1 09/24/21 14:29 V9259JMV
<0.175 mg/Kg - dry 0.175 0.7903,3'-Dichlorobenzidine 1 09/24/21 14:29 V9259JMV
<0.114 mg/Kg - dry 0.114 0.7902,4-Dichlorophenol 1 09/24/21 14:29 V9259JMV
<0.215 mg/Kg - dry 0.215 0.790
Diethyl phthalate 1 09/24/21 14:29 V9259JMV
<0.208 mg/Kg - dry 0.208 0.790Dimethyl phthalate 1 09/24/21 14:29 V9259JMV
<0.129 mg/Kg - dry 0.129 0.3942,4-Dimethylphenol 1 09/24/21 14:29 V9259JMV
<0.127 mg/Kg - dry 0.127 0.790Di-n-butyl phthalate 1 09/24/21 14:29 V9259JMV
<0.287 mg/Kg - dry 0.287 1.794,6-Dinitro-2-methylphenol 1 09/24/21 14:29 V9259JMV
<0.622 mg/Kg - dry 0.622 1.792,4-Dinitrophenol 1 09/24/21 14:29 V9259JMV
<0.115 mg/Kg - dry 0.115 0.7902,4-Dinitrotoluene 1 09/24/21 14:29 V9259JMV
<0.129 mg/Kg - dry 0.129 0.7902,6-Dinitrotoluene 1 09/24/21 14:29 V9259JMV
<0.171 mg/Kg - dry 0.171 0.394Di-n-Octyl Phthalate 1 09/24/21 14:29 V9259JMV
<0.147 mg/Kg - dry 0.147 0.790Fluoranthene 1 09/24/21 14:29 V9259JMV
<0.153 mg/Kg - dry 0.153 0.790Fluorene 1 09/24/21 14:29 V9259JMV
<0.126 mg/Kg - dry 0.126 0.790Hexachlorobenzene 1 09/24/21 14:29 V9259JMV
<0.116 mg/Kg - dry 0.116 0.790Hexachlorobutadiene 1 09/24/21 14:29 V9259JMV
<0.187 mg/Kg - dry 0.187 0.790Hexachlorocyclopentadiene 1 09/24/21 14:29 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 51 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:HO-UST-PB
95809 Matrix:
9/21/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.094 mg/Kg - dry 0.094 0.790Hexachloroethane 1 09/24/21 14:29 V9259JMV
<0.214 mg/Kg - dry 0.214 0.790
Indeno(1,2,3-cd)pyrene 1 09/24/21 14:29 V9259JMV
<0.228 mg/Kg - dry 0.228 0.790Isophorone 1 09/24/21 14:29 V9259JMV
<0.126 mg/Kg - dry 0.126 0.7901-Methylnaphthalene 1 09/24/21 14:29 V9259JMV
<0.119 mg/Kg - dry 0.119 0.7902-Methylnaphthalene 1 09/24/21 14:29 V9259JMV
<0.116 mg/Kg - dry 0.116 0.7902-Methylphenol 1 09/24/21 14:29 V9259JMV
<0.101 mg/Kg - dry 0.101 0.7903&4 Methylphenol 1 09/24/21 14:29 V9259JMV
<0.172 mg/Kg - dry 0.172 0.790Naphthalene 1 09/24/21 14:29 V9259JMV
<0.115 mg/Kg - dry 0.115 0.790
2-Nitroaniline 1 09/24/21 14:29 V9259JMV
<0.143 mg/Kg - dry 0.143 0.7903-Nitroaniline 1 09/24/21 14:29 V9259JMV
<0.111 mg/Kg - dry 0.111 0.3944-Nitroaniline 1 09/24/21 14:29 V9259JMV
<0.138 mg/Kg - dry 0.138 0.394Nitrobenzene 1 09/24/21 14:29 V9259JMV
<0.106 mg/Kg - dry 0.106 0.7902-Nitrophenol 1 09/24/21 14:29 V9259JMV
<0.139 mg/Kg - dry 0.139 0.7904-Nitrophenol 1 09/24/21 14:29 V9259JMV
<0.314 mg/Kg - dry 0.314 0.790N-Nitrosodimethylamine 1 09/24/21 14:29 V9259JMV
<0.216 mg/Kg - dry 0.216 0.790N-Nitrosodiphenylamine 1 09/24/21 14:29 V9259JMV
<0.141 mg/Kg - dry 0.141 0.790N-Nitroso-di-n-propylamine 1 09/24/21 14:29 V9259JMV
<0.415 mg/Kg - dry 0.415 1.20Pentachlorophenol 1 09/24/21 14:29 V9259JMV
<0.248 mg/Kg - dry 0.248 0.790Phenanthrene 1 09/24/21 14:29 V9259JMV
<0.133 mg/Kg - dry 0.133 0.790Phenol 1 09/24/21 14:29 V9259JMV
<0.160 mg/Kg - dry 0.160 0.790Pyrene 1 09/24/21 14:29 V9259JMV
<0.094 mg/Kg - dry 0.094 0.394Pyridine 1 09/24/21 14:29 V9259JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 52 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:HO-UST-PB
95809 Matrix:
9/21/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9195 09/23/21 11:50
<0.127 mg/Kg - dry 0.127 0.7901,2,4-Trichlorobenzene 1 09/24/21 14:29 V9259JMV
<0.115 mg/Kg - dry 0.115 0.790
2,4,5-Trichlorophenol 1 09/24/21 14:29 V9259JMV
<0.115 mg/Kg - dry 0.115 0.7902,4,6-Trichlorophenol 1 09/24/21 14:29 V9259JMV
Surrogate: Phenol-d5 50.9 Limits: 34-121%09/24/21 14:291 JMV V9259
Surrogate: 2-Fluorobiphenyl 63.5 Limits: 44-115%09/24/21 14:291 JMV V9259
Surrogate: 2-Fluorophenol 54.5 Limits: 35-115%09/24/21 14:291 JMV V9259
Surrogate: Nitrobenzene-d5 52.9 Limits: 37-122%09/24/21 14:291 JMV V9259
Surrogate: 4-Terphenyl-d14 63.5 Limits: 54-127%09/24/21 14:291 JMV V9259
Surrogate: 2,4,6-Tribromophenol 83.2 Limits: 39-132%09/24/21 14:291 JMV V9259
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 53 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-73
95975 Matrix:
9/21/2021 11:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.8 %Moisture 1 09/23/21 16:37 SW-DRYWTEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 54 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-73
95975 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V9215 09/23/21 08:00
<0.088 mg/Kg - dry 0.088 0.738Acetone 50 09/23/21 12:33 V9216TBL
<0.044 mg/Kg - dry 0.044 0.738
Acrolein 50 09/23/21 12:33 V9216TBL
<0.027 mg/Kg - dry 0.027 0.738Acrylonitrile 50 09/23/21 12:33 V9216TBL
1.03 mg/Kg - dry 0.021 0.185Benzene 50 09/23/21 12:33 V9216TBL
<0.018 mg/Kg - dry 0.018 0.185Bromobenzene 50 09/23/21 12:33 V9216TBL
<0.029 mg/Kg - dry 0.029 0.185Bromochloromethane 50 09/23/21 12:33 V9216TBL
<0.044 mg/Kg - dry 0.044 0.185Bromodichloromethane 50 09/23/21 12:33 V9216TBL
<0.037 mg/Kg - dry 0.037 0.185Bromoform 50 09/23/21 12:33 V9216TBL
<0.067 mg/Kg - dry 0.067 0.369
Bromomethane 50 09/23/21 12:33 V9216TBL
5.93 mg/Kg - dry 0.018 0.185n-Butylbenzene 50 09/23/21 12:33 V9216TBL
5.91 mg/Kg - dry 0.020 0.185sec-Butyl benzene 50 09/23/21 12:33 V9216TBL
<0.018 mg/Kg - dry 0.018 0.185tert-Butyl benzene 50 09/23/21 12:33 V9216TBL
<0.023 mg/Kg - dry 0.023 0.185Carbon Disulfide 50 09/23/21 12:33 V9216TBL
<0.058 mg/Kg - dry 0.058 0.185Carbon Tetrachloride 50 09/23/21 12:33 V9216TBL
<0.024 mg/Kg - dry 0.024 0.185Chlorobenzene 50 09/23/21 12:33 V9216TBL
<0.033 mg/Kg - dry 0.033 0.185Chlorodibromomethane 50 09/23/21 12:33 V9216TBL
<0.032 mg/Kg - dry 0.032 0.369Chloroethane 50 09/23/21 12:33 V9216TBL
<0.038 mg/Kg - dry 0.038 0.185Chloroform 50 09/23/21 12:33 V9216TBL
<0.023 mg/Kg - dry 0.023 0.369Chloromethane 50 09/23/21 12:33 V9216TBL
<0.018 mg/Kg - dry 0.018 0.1852-Chlorotoluene 50 09/23/21 12:33 V9216TBL
<0.014 mg/Kg - dry 0.014 0.1854-Chlorotoluene 50 09/23/21 12:33 V9216TBL
<0.027 mg/Kg - dry 0.027 0.185Di-Isopropyl Ether (DIPE)50 09/23/21 12:33 V9216TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 55 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-73
95975 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V9215 09/23/21 08:00
<0.016 mg/Kg - dry 0.016 0.3691,2-Dibromo-3-Chloropropane 50 09/23/21 12:33 V9216TBL
<0.021 mg/Kg - dry 0.021 0.185
1,2-Dibromoethane 50 09/23/21 12:33 V9216TBL
<0.036 mg/Kg - dry 0.036 0.185Dibromomethane 50 09/23/21 12:33 V9216TBL
<0.011 mg/Kg - dry 0.011 0.1851,2-Dichlorobenzene 50 09/23/21 12:33 V9216TBL
<0.014 mg/Kg - dry 0.014 0.1851,3-Dichlorobenzene 50 09/23/21 12:33 V9216TBL
<0.022 mg/Kg - dry 0.022 0.1851,4-Dichlorobenzene 50 09/23/21 12:33 V9216TBL
<0.048 mg/Kg - dry 0.048 0.369Dichlorodifluoromethane 50 09/23/21 12:33 V9216TBL
<0.030 mg/Kg - dry 0.030 0.1851,1-Dichloroethane 50 09/23/21 12:33 V9216TBL
<0.051 mg/Kg - dry 0.051 0.185
1,2-Dichloroethane 50 09/23/21 12:33 V9216TBL
<0.027 mg/Kg - dry 0.027 0.1851,1-Dichloroethene 50 09/23/21 12:33 V9216TBL
<0.029 mg/Kg - dry 0.029 0.185cis-1,2-Dichloroethene 50 09/23/21 12:33 V9216TBL
<0.038 mg/Kg - dry 0.038 0.185trans-1,2-Dichloroethene 50 09/23/21 12:33 V9216TBL
<0.016 mg/Kg - dry 0.016 0.1851,2-Dichloropropane 50 09/23/21 12:33 V9216TBL
<0.020 mg/Kg - dry 0.020 0.1851,3-Dichloropropane 50 09/23/21 12:33 V9216TBL
<0.047 mg/Kg - dry 0.047 0.1852,2-Dichloropropane 50 09/23/21 12:33 V9216TBL
<0.028 mg/Kg - dry 0.028 0.1851,1-Dichloropropene 50 09/23/21 12:33 V9216TBL
<0.020 mg/Kg - dry 0.020 0.185cis-1,3-Dichloropropene 50 09/23/21 12:33 V9216TBL
<0.029 mg/Kg - dry 0.029 0.185trans-1,3-Dichloropropene 50 09/23/21 12:33 V9216TBL
9.30 mg/Kg - dry 0.021 0.185Ethylbenzene 50 09/23/21 12:33 V9216TBL
<0.030 mg/Kg - dry 0.030 3.69Ethyl Tertiary Butyl Ether (ETBE)50 09/23/21 12:33 V9216TBL
<0.029 mg/Kg - dry 0.029 0.369Hexachlorobutadiene 50 09/23/21 12:33 V9216TBL
3.24 mg/Kg - dry 0.024 0.369n-Hexane 50 09/23/21 12:33 V9216TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 56 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-73
95975 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V9215 09/23/21 08:00
<0.022 mg/Kg - dry 0.022 0.7382-Hexanone 50 09/23/21 12:33 V9216TBL
4.97 mg/Kg - dry 0.016 0.185
Isopropylbenzene 50 09/23/21 12:33 V9216TBL
5.38 mg/Kg - dry 0.048 0.1854-Isopropyl toluene 50 09/23/21 12:33 V9216TBL
<0.024 mg/Kg - dry 0.024 0.738Methyl Ethyl Ketone (MEK)50 09/23/21 12:33 V9216TBL
<0.023 mg/Kg - dry 0.023 0.185Methyl tert-butyl ether (MTBE)50 09/23/21 12:33 V9216TBL
<0.554 mg/Kg - dry 0.554 0.7384-Methyl-2-Pentanone 50 09/23/21 12:33 V9216TBL
<0.054 mg/Kg - dry 0.054 0.185Methylene Chloride 50 09/23/21 12:33 V9216TBL
5.98 mg/Kg - dry 0.036 0.369Naphthalene 50 09/23/21 12:33 V9216TBL
9.31 mg/Kg - dry 0.020 0.185
n-Propylbenzene 50 09/23/21 12:33 V9216TBL
<0.052 mg/Kg - dry 0.052 0.185Styrene 50 09/23/21 12:33 V9216TBL
<0.038 mg/Kg - dry 0.038 0.1851,1,1,2-Tetrachloroethane 50 09/23/21 12:33 V9216TBL
<0.011 mg/Kg - dry 0.011 0.1851,1,2,2-Tetrachloroethane 50 09/23/21 12:33 V9216TBL
0.050 J mg/Kg - dry 0.033 0.185Tetrachloroethene 50 09/23/21 12:33 V9216TBL
13.5 mg/Kg - dry 0.024 0.185Toluene 50 09/23/21 12:33 V9216TBL
<0.019 mg/Kg - dry 0.019 0.3691,2,3-Trichlorobenzene 50 09/23/21 12:33 V9216TBL
<0.023 mg/Kg - dry 0.023 0.3691,2,4-Trichlorobenzene 50 09/23/21 12:33 V9216TBL
<0.053 mg/Kg - dry 0.053 0.1851,1,1-Trichloroethane 50 09/23/21 12:33 V9216TBL
<0.017 mg/Kg - dry 0.017 0.1851,1,2-Trichloroethane 50 09/23/21 12:33 V9216TBL
<0.034 mg/Kg - dry 0.034 0.185Trichloroethene 50 09/23/21 12:33 V9216TBL
<0.077 mg/Kg - dry 0.077 0.369Trichlorofluoromethane 50 09/23/21 12:33 V9216TBL
<0.026 mg/Kg - dry 0.026 0.1851,2,3-Trichloropropane 50 09/23/21 12:33 V9216TBL
22.2 mg/Kg - dry 0.200 1.851,3,5-Trimethylbenzene 500 09/23/21 13:01 V9216TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 57 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-265-0007
01166
Proctor Environmental Services, Inc.
5113 Yachtsman Ct.
Tom Proctor
Raleigh
Received : 09/22/2021
NHX, Raleigh
Report Date : 10/01/2021
Sample ID :
Lab No :
Sampled:B-73
95975 Matrix:
9/21/2021 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V9215 09/23/21 08:00
<0.016 mg/Kg - dry 0.016 0.369Vinyl Acetate 50 09/23/21 12:33 V9216TBL
<0.017 mg/Kg - dry 0.017 0.369
Vinyl Chloride 50 09/23/21 12:33 V9216TBL
17.1 mg/Kg - dry 0.185 1.85o-Xylene 500 09/23/21 13:01 V9216TBL
33.0 mg/Kg - dry 0.464 3.69m,p-Xylene 500 09/23/21 13:01 V9216TBL
50.1 mg/Kg - dry 0.185 1.85Xylene (Total)500 09/23/21 13:01 V9216
Surrogate: 4-Bromofluorobenzene 121 Limits: 70-130%09/23/21 12:3350 TBL V9216
Surrogate: Dibromofluoromethane 94.3 Limits: 70-130%09/23/21 12:3350 TBL V9216
Surrogate: Toluene-d8 116 Limits: 76-129%09/23/21 12:3350 TBL V9216
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%09/23/21 13:01500 TBL V9216
Surrogate: Dibromofluoromethane 97.9 Limits: 70-130%09/23/21 13:01500 TBL V9216
Surrogate: Toluene-d8 105 Limits: 76-129%09/23/21 13:01500 TBL V9216
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Page 58 of 99
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172Tel: [phone] Fax: [phone] www.pacelabs.com
Report of Analysis
Waypoint Analytical
PO Box 240543Charlotte, NC 28224Attention: Angela Overcash
Project Name: 21-265-0007
Lot Number:WI28043
Date Completed:09/30/2021
10/01/2021 10:49 AMApproved and released by:
Project Manager II:Lucas Odom
Page 1 of 11
Page 59 of 99
PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Waypoint Analytical
Lot Number: WI28043
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header informationassociated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page ordiscussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non-Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weightunless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Page 2 of 11
Page 60 of 99
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: WI28043

Sample Number Sample ID Matrix Date Sampled Date Received
001 09/21/2021 0900A5(9)2'-3'Solid 09/28/2021
(1 sample)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 11
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Waypoint Analytical
Lot Number: WI28043

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 A5(9)2'-3'Solid Hexavalent Chromium 7199 0.52 J mg/kg 5
(1 detection)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 11
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
A5(9)2'-3'
WI28043-001
09/21/2021 0900
09/28/2021
Solid
% Solids:75.8 09/28/2021 2312
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 09/29/2021 1952 AMR 09/29/2021 1152 16787
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.52 J 1mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 11
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 11
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ16787-001
16787 3060A
09/29/2021 1152Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 09/29/2021 15591.0 0.20 mg/kg1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 11
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ16787-002
16787 3060A
09/29/2021 1152Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg) (mg/kg)
Hexavalent Chromium 9.0 09/29/2021 1625901080-1201
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 11
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 11
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 11
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 11
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Metals Analyses
6020B
V9219QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V9191
Associated Lab Samples: 95805, 95806, 95807, 95808, 95809
LRB-V9191 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/23/21 20:551.000.0940<0.0940mg/KgArsenic
09/23/21 20:5510.01.40<1.40mg/KgBarium
09/23/21 20:550.5000.0550<0.0550mg/KgCadmium
09/23/21 20:551.000.290<0.290mg/KgChromium
09/23/21 20:551.000.140<0.140mg/KgLead
09/23/21 20:552.000.900<0.900mg/KgSelenium
09/23/21 20:550.5000.0410<0.0410mg/KgSilver
LCS-V9191Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.012.012.5mg/KgArsenic 80-120
10012.512.5mg/KgBarium 80-120
10212.812.5mg/KgCadmium 80-120
98.012.312.5mg/KgChromium 80-120
10112.612.5mg/KgLead 80-120
99.012.412.5mg/KgSelenium 80-120
1015.035.00mg/KgSilver 80-120
V 95805-MS-V9191 V 95805-MSD-V9191Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
12.5 84.012.812.512.51.95mg/KgArsenic 87.0 75-125 2.3 20
37.1 10235.312.512.524.3mg/KgBarium 88.0 75-125 4.9 20
12.3 98.012.412.512.5<0.0550mg/KgCadmium 99.0 75-125 0.8 20
29.6 80.030.212.512.519.6mg/KgChromium 85.0 75-125 2.0 20
Page 1 of 28Date:10/01/2021 11:03 AM
Page 70 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Metals Analyses
6020B
V9219QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V9191
V 95805-MS-V9191 V 95805-MSD-V9191Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
23.1 90.022.412.512.511.8mg/KgLead 85.0 75-125 3.0 20
13.1 10513.612.512.51.51mg/KgSelenium 109 75-125 3.7 20
4.84 97.04.865.005.00<0.0410mg/KgSilver 97.0 75-125 0.4 20
V 95805-PDS-V9191Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/23/21 21:4010213.7mg/KgArsenic
09/23/21 21:4010124.9mg/KgBarium
09/23/21 21:4010212.7mg/KgCadmium
09/23/21 21:4099.022.1mg/KgChromium
09/23/21 21:4099.018.2mg/KgLead
09/23/21 21:4010613.2mg/KgSelenium
09/23/21 21:4010212.7mg/KgSilver
Page 2 of 28Date:10/01/2021 11:03 AM
Page 71 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V9272QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V9236
Associated Lab Samples: 95805, 95806, 95807, 95808, 95809
LRB-V9236 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/24/21 15:140.03000.0120<0.0120mg/KgMercury (Total)
LCS-V9236Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
95.00.3950.417mg/KgMercury (Total)80-120
V 95805-MS-V9236 V 95805-MSD-V9236Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.484 1010.4450.4170.4170.0642mg/KgMercury (Total)91.0 80-120 8.3 20
V 95805-PDS-V9236Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/24/21 15:2994.00.227mg/KgMercury (Total)
Page 3 of 28Date:10/01/2021 11:03 AM
Page 72 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V9181QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9156
Associated Lab Samples: 95809
LRB-V9156 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/22/21 16:2310.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
09/22/21 16:23OTP Surrogate (S)74.7 31-123
LCS-V9156 LCSD-V9156Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
50.3 75.477.551.766.7mg/KgDiesel Range Organics (C10-C28)46-126 2.7 20
73.976.6OTP Surrogate (S)31-123
Page 4 of 28Date:10/01/2021 11:03 AM
Page 73 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V9213QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V9212
Associated Lab Samples: 95809
LRB-V9212 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/24/21 09:215.000.0410.617mg/KgGasoline Range Organics (C6-C10)
09/24/21 09:21a,a,a-Trifluorotoluene (S)133 50-137
LCS-V9212Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10351.450.0mg/KgGasoline Range Organics (C6-C10)41-138
127a,a,a-Trifluorotoluene (S)50-137
V 95809-MS-V9212 V 95809-MSD-V9212Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
49.0 98.048.250.050.01.12mg/KgGasoline Range Organics (C6-C10)96.4 41-138 1.6 34
122a,a,a-Trifluorotoluene (S)120 50-137
Page 5 of 28Date:10/01/2021 11:03 AM
Page 74 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9211QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9210
Associated Lab Samples: 95801, 95802, 95803, 95809
LRB-V9210 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/23/21 10:140.0200.002<0.002mg/KgAcetone
09/23/21 10:140.0200.001<0.001mg/KgAcrolein
09/23/21 10:140.0200.0008<0.0008mg/KgAcrylonitrile
09/23/21 10:140.0050.0006<0.0006mg/KgBenzene
09/23/21 10:140.0050.0005<0.0005mg/KgBromobenzene
09/23/21 10:140.0050.0008<0.0008mg/KgBromochloromethane
09/23/21 10:140.0050.001<0.001mg/KgBromodichloromethane
09/23/21 10:140.0050.001<0.001mg/KgBromoform
09/23/21 10:140.0100.001<0.001mg/KgBromomethane
09/23/21 10:140.0050.0005<0.0005mg/Kgn-Butylbenzene
09/23/21 10:140.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/23/21 10:140.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/23/21 10:140.0050.0006<0.0006mg/KgCarbon Disulfide
09/23/21 10:140.0050.001<0.001mg/KgCarbon Tetrachloride
09/23/21 10:140.0050.0007<0.0007mg/KgChlorobenzene
09/23/21 10:140.0050.0009<0.0009mg/KgChlorodibromomethane
09/23/21 10:140.0100.0009<0.0009mg/KgChloroethane
09/23/21 10:140.0050.001<0.001mg/KgChloroform
09/23/21 10:140.0100.0006<0.0006mg/KgChloromethane
09/23/21 10:140.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/23/21 10:140.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/23/21 10:140.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/23/21 10:140.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/23/21 10:140.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/23/21 10:140.0050.0006<0.0006mg/KgDibromomethane
09/23/21 10:140.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/23/21 10:140.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 6 of 28Date:10/01/2021 11:03 AM
Page 75 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9211QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9210
Associated Lab Samples: 95801, 95802, 95803, 95809
LRB-V9210 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/23/21 10:140.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/23/21 10:140.0100.001<0.001mg/KgDichlorodifluoromethane
09/23/21 10:140.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/23/21 10:140.0050.001<0.001mg/Kg1,2-Dichloroethane
09/23/21 10:140.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/23/21 10:140.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/23/21 10:140.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/23/21 10:140.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/23/21 10:140.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/23/21 10:140.0050.001<0.001mg/Kg2,2-Dichloropropane
09/23/21 10:140.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/23/21 10:140.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/23/21 10:140.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/23/21 10:140.0050.0006<0.0006mg/KgEthylbenzene
09/23/21 10:140.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/23/21 10:140.0100.0008<0.0008mg/KgHexachlorobutadiene
09/23/21 10:140.0100.0007<0.0007mg/Kgn-Hexane
09/23/21 10:140.0200.0006<0.0006mg/Kg2-Hexanone
09/23/21 10:140.0050.0005<0.0005mg/KgIsopropylbenzene
09/23/21 10:140.0050.001<0.001mg/Kg4-Isopropyl toluene
09/23/21 10:140.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/23/21 10:140.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/23/21 10:140.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/23/21 10:140.0100.001<0.001mg/KgMethylene Chloride
09/23/21 10:140.0100.0010<0.0010mg/KgNaphthalene
09/23/21 10:140.0050.0005<0.0005mg/Kgn-Propylbenzene
09/23/21 10:140.0050.001<0.001mg/KgStyrene
Page 7 of 28Date:10/01/2021 11:03 AM
Page 76 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9211QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9210
Associated Lab Samples: 95801, 95802, 95803, 95809
LRB-V9210 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/23/21 10:140.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/23/21 10:140.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/23/21 10:140.0050.0009<0.0009mg/KgTetrachloroethene
09/23/21 10:140.0050.0007<0.0007mg/KgToluene
09/23/21 10:140.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/23/21 10:140.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/23/21 10:140.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/23/21 10:140.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/23/21 10:140.0050.0009<0.0009mg/KgTrichloroethene
09/23/21 10:140.0100.002<0.002mg/KgTrichlorofluoromethane
09/23/21 10:140.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/23/21 10:140.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/23/21 10:140.0100.0005<0.0005mg/KgVinyl Acetate
09/23/21 10:140.0100.0005<0.0005mg/KgVinyl Chloride
09/23/21 10:140.0050.0005<0.0005mg/Kgo-Xylene
09/23/21 10:140.0100.001<0.001mg/Kgm,p-Xylene
09/23/21 10:144-Bromofluorobenzene (S)101 70-130
09/23/21 10:14Dibromofluoromethane (S)93.0 84-123
09/23/21 10:14Toluene-d8 (S)101 76-129
LCS-V9210 LCSD-V9210Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.116 1161110.1110.100mg/KgAcetone 29-198 4.4 20
0.101 1011000.1000.100mg/KgAcrolein 70-130 0.9 20
0.094 94.097.30.0970.100mg/KgAcrylonitrile 65-134 3.4 20
Page 8 of 28Date:10/01/2021 11:03 AM
Page 77 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9211QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9210
LCS-V9210 LCSD-V9210Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 85.692.60.0460.050mg/KgBenzene 74-127 7.8 20
0.043 86.893.60.0460.050mg/KgBromobenzene 73-125 7.5 20
0.045 91.094.20.0470.050mg/KgBromochloromethane 72-134 3.4 20
0.045 91.095.60.0470.050mg/KgBromodichloromethane 75-122 4.9 20
0.046 93.895.00.0470.050mg/KgBromoform 66-135 1.2 20
0.054 1081040.0510.050mg/KgBromomethane 20-180 4.5 20
0.042 85.493.80.0460.050mg/Kgn-Butylbenzene 65-135 9.3 20
0.042 85.294.00.0470.050mg/Kgsec-Butyl benzene 66-131 9.8 20
0.042 85.493.60.0460.050mg/Kgtert-Butyl benzene 67-132 9.1 20
0.043 86.492.00.0460.050mg/KgCarbon Disulfide 61-129 6.2 20
0.041 83.292.20.0460.050mg/KgCarbon Tetrachloride 64-143 10.2 20
0.043 87.091.80.0450.050mg/KgChlorobenzene 74-118 5.3 20
0.047 95.088.60.0440.050mg/KgChlorodibromomethane 73-122 6.9 20
0.037 75.474.00.0370.050mg/KgChloroethane 33-149 1.8 20
0.042 84.291.60.0450.050mg/KgChloroform 73-127 8.4 20
0.041 82.281.80.0400.050mg/KgChloromethane 45-143 0.4 20
0.043 86.293.40.0460.050mg/Kg2-Chlorotoluene 67-124 8.0 20
0.040 81.292.00.0460.050mg/Kg4-Chlorotoluene 71-126 12.4 20
0.044 89.694.20.0470.050mg/KgDi-Isopropyl Ether (DIPE)59-159 5.0 20
0.054 1091020.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 6.6 20
0.046 93.094.60.0470.050mg/Kg1,2-Dibromoethane 70-132 1.7 20
0.047 95.097.00.0480.050mg/KgDibromomethane 74-133 2.0 20
0.046 92.290.80.0450.050mg/Kg1,2-Dichlorobenzene 72-123 1.5 20
0.043 87.492.40.0460.050mg/Kg1,3-Dichlorobenzene 71-120 5.5 20
0.043 86.493.00.0460.050mg/Kg1,4-Dichlorobenzene 71-123 7.3 20
0.034 68.070.40.0350.050mg/KgDichlorodifluoromethane 26-146 3.4 20
Page 9 of 28Date:10/01/2021 11:03 AM
Page 78 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9211QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9210
LCS-V9210 LCSD-V9210Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 84.491.40.0450.050mg/Kg1,1-Dichloroethane 74-127 7.9 20
0.043 87.090.60.0450.050mg/Kg1,2-Dichloroethane 68-128 4.0 20
0.043 87.092.40.0460.050mg/Kg1,1-Dichloroethene 67-149 6.0 20
0.042 85.693.40.0460.050mg/Kgcis-1,2-Dichloroethene 76-134 8.7 20
0.042 85.289.20.0440.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.5 20
0.044 89.095.80.0470.050mg/Kg1,2-Dichloropropane 73-130 7.3 20
0.045 90.293.20.0460.050mg/Kg1,3-Dichloropropane 75-124 3.2 20
0.043 86.097.60.0480.050mg/Kg2,2-Dichloropropane 50-142 12.6 20
0.041 82.693.40.0460.050mg/Kg1,1-Dichloropropene 71-130 12.2 20
0.046 93.698.00.0490.050mg/Kgcis-1,3-Dichloropropene 71-125 4.5 20
0.047 95.096.40.0480.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.4 20
0.042 84.892.60.0460.050mg/KgEthylbenzene 74-128 8.7 20
0.092 92.896.90.0960.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 4.3 20
0.047 95.298.40.0490.050mg/KgHexachlorobutadiene 64-125 3.3 20
0.045 90.496.40.0480.050mg/Kgn-Hexane 70-130 6.4 20
0.054 1091080.0530.050mg/Kg2-Hexanone 61-157 0.7 20
0.042 85.294.20.0470.050mg/KgIsopropylbenzene 68-126 10.0 20
0.043 86.694.80.0470.050mg/Kg4-Isopropyl toluene 68-129 9.0 20
0.054 1091100.0550.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.4 20
0.047 95.094.40.0470.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.6 20
0.049 98.298.00.0490.050mg/Kg4-Methyl-2-Pentanone 57-162 0.2 20
0.042 85.284.20.0420.050mg/KgMethylene Chloride 74-129 1.1 20
0.051 10398.60.0490.050mg/KgNaphthalene 57-157 4.7 20
0.042 84.493.60.0460.050mg/Kgn-Propylbenzene 67-130 10.3 20
0.044 89.695.60.0470.050mg/KgStyrene 77-121 6.4 20
0.045 90.294.00.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.1 20
Page 10 of 28Date:10/01/2021 11:03 AM
Page 79 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9211QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9210
LCS-V9210 LCSD-V9210Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.693.80.0460.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 4.5 20
0.043 86.492.20.0460.050mg/KgTetrachloroethene 68-130 6.4 20
0.043 87.292.00.0460.050mg/KgToluene 71-129 5.3 20
0.049 99.697.20.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.4 20
0.049 98.697.40.0480.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.2 20
0.042 84.093.20.0460.050mg/Kg1,1,1-Trichloroethane 67-131 10.3 20
0.046 93.094.60.0470.050mg/Kg1,1,2-Trichloroethane 70-133 1.7 20
0.043 86.493.20.0460.050mg/KgTrichloroethene 75-133 7.5 20
0.042 85.289.80.0440.050mg/KgTrichlorofluoromethane 44-146 5.2 20
0.046 92.693.80.0460.050mg/Kg1,2,3-Trichloropropane 60-137 1.2 20
0.043 87.094.20.0470.050mg/Kg1,3,5-Trimethylbenzene 69-128 7.9 20
0.050 1021100.0550.050mg/KgVinyl Acetate 60-140 7.9 20
0.040 81.885.00.0420.050mg/KgVinyl Chloride 48-147 3.8 20
0.043 87.694.60.0470.050mg/Kgo-Xylene 74-126 7.6 20
0.088 88.295.40.0950.100mg/Kgm,p-Xylene 75-124 7.8 20
1001024-Bromofluorobenzene (S)70-130
97.698.4Dibromofluoromethane (S)84-123
98.8102Toluene-d8 (S)76-129
Page 11 of 28Date:10/01/2021 11:03 AM
Page 80 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9216QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V9215
Associated Lab Samples: 95975
LRB-V9215 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/23/21 10:140.0200.002<0.002mg/KgAcetone
09/23/21 10:140.0200.001<0.001mg/KgAcrolein
09/23/21 10:140.0200.0008<0.0008mg/KgAcrylonitrile
09/23/21 10:140.0050.0006<0.0006mg/KgBenzene
09/23/21 10:140.0050.0005<0.0005mg/KgBromobenzene
09/23/21 10:140.0050.0008<0.0008mg/KgBromochloromethane
09/23/21 10:140.0050.001<0.001mg/KgBromodichloromethane
09/23/21 10:140.0050.001<0.001mg/KgBromoform
09/23/21 10:140.0100.001<0.001mg/KgBromomethane
09/23/21 10:140.0050.0005<0.0005mg/Kgn-Butylbenzene
09/23/21 10:140.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/23/21 10:140.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/23/21 10:140.0050.0006<0.0006mg/KgCarbon Disulfide
09/23/21 10:140.0050.001<0.001mg/KgCarbon Tetrachloride
09/23/21 10:140.0050.0007<0.0007mg/KgChlorobenzene
09/23/21 10:140.0050.0009<0.0009mg/KgChlorodibromomethane
09/23/21 10:140.0100.0009<0.0009mg/KgChloroethane
09/23/21 10:140.0050.001<0.001mg/KgChloroform
09/23/21 10:140.0100.0006<0.0006mg/KgChloromethane
09/23/21 10:140.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/23/21 10:140.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/23/21 10:140.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/23/21 10:140.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/23/21 10:140.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/23/21 10:140.0050.0010<0.0010mg/KgDibromomethane
09/23/21 10:140.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/23/21 10:140.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 12 of 28Date:10/01/2021 11:03 AM
Page 81 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9216QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V9215
Associated Lab Samples: 95975
LRB-V9215 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/23/21 10:140.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/23/21 10:140.0100.001<0.001mg/KgDichlorodifluoromethane
09/23/21 10:140.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/23/21 10:140.0050.001<0.001mg/Kg1,2-Dichloroethane
09/23/21 10:140.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/23/21 10:140.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/23/21 10:140.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/23/21 10:140.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/23/21 10:140.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/23/21 10:140.0050.001<0.001mg/Kg2,2-Dichloropropane
09/23/21 10:140.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/23/21 10:140.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/23/21 10:140.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/23/21 10:140.0050.0006<0.0006mg/KgEthylbenzene
09/23/21 10:140.1000.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/23/21 10:140.0100.0008<0.0008mg/KgHexachlorobutadiene
09/23/21 10:140.0100.0007<0.0007mg/Kgn-Hexane
09/23/21 10:140.0200.0006<0.0006mg/Kg2-Hexanone
09/23/21 10:140.0050.0005<0.0005mg/KgIsopropylbenzene
09/23/21 10:140.0050.001<0.001mg/Kg4-Isopropyl toluene
09/23/21 10:140.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/23/21 10:140.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/23/21 10:140.0050.001<0.001mg/KgMethylene Chloride
09/23/21 10:140.0100.0010<0.0010mg/KgNaphthalene
09/23/21 10:140.0050.0005<0.0005mg/Kgn-Propylbenzene
09/23/21 10:140.0050.001<0.001mg/KgStyrene
09/23/21 10:140.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
Page 13 of 28Date:10/01/2021 11:03 AM
Page 82 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9216QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V9215
Associated Lab Samples: 95975
LRB-V9215 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/23/21 10:140.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/23/21 10:140.0050.0009<0.0009mg/KgTetrachloroethene
09/23/21 10:140.0050.0007<0.0007mg/KgToluene
09/23/21 10:140.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/23/21 10:140.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/23/21 10:140.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/23/21 10:140.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/23/21 10:140.0050.0009<0.0009mg/KgTrichloroethene
09/23/21 10:140.0100.002<0.002mg/KgTrichlorofluoromethane
09/23/21 10:140.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/23/21 10:140.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/23/21 10:140.0100.0005<0.0005mg/KgVinyl Acetate
09/23/21 10:140.0100.0005<0.0005mg/KgVinyl Chloride
09/23/21 10:140.0050.0005<0.0005mg/Kgo-Xylene
09/23/21 10:140.0100.001<0.001mg/Kgm,p-Xylene
09/23/21 10:144-Bromofluorobenzene (S)101 70-130
09/23/21 10:14Dibromofluoromethane (S)93.0 70-130
09/23/21 10:14Toluene-d8 (S)101 76-129
LCS-V9215 LCSD-V9215Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.116 1161110.1110.100mg/KgAcetone 29-198 4.4 20
0.101 1011000.1000.100mg/KgAcrolein 70-130 0.9 20
0.094 94.097.30.0970.100mg/KgAcrylonitrile 65-134 3.4 20
0.042 85.692.60.0460.050mg/KgBenzene 74-127 7.8 20
Page 14 of 28Date:10/01/2021 11:03 AM
Page 83 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9216QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V9215
LCS-V9215 LCSD-V9215Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.043 86.893.60.0460.050mg/KgBromobenzene 73-125 7.5 20
0.045 91.094.20.0470.050mg/KgBromochloromethane 72-134 3.4 20
0.045 91.095.60.0470.050mg/KgBromodichloromethane 75-122 4.9 20
0.046 93.895.00.0470.050mg/KgBromoform 66-135 1.2 20
0.054 1081040.0510.050mg/KgBromomethane 20-180 4.5 20
0.042 85.493.80.0460.050mg/Kgn-Butylbenzene 65-135 9.3 20
0.042 85.294.00.0470.050mg/Kgsec-Butyl benzene 66-131 9.8 20
0.042 85.493.60.0460.050mg/Kgtert-Butyl benzene 67-132 9.1 20
0.043 86.492.00.0460.050mg/KgCarbon Disulfide 61-129 6.2 20
0.041 83.292.20.0460.050mg/KgCarbon Tetrachloride 64-143 10.2 20
0.043 87.091.80.0450.050mg/KgChlorobenzene 74-118 5.3 20
0.047 95.088.60.0440.050mg/KgChlorodibromomethane 73-122 6.9 20
0.037 75.474.00.0370.050mg/KgChloroethane 33-149 1.8 20
0.042 84.291.60.0450.050mg/KgChloroform 73-127 8.4 20
0.041 82.281.80.0400.050mg/KgChloromethane 45-143 0.4 20
0.043 86.293.40.0460.050mg/Kg2-Chlorotoluene 67-124 8.0 20
0.040 81.292.00.0460.050mg/Kg4-Chlorotoluene 71-126 12.4 20
0.044 89.694.20.0470.050mg/KgDi-Isopropyl Ether (DIPE)59-159 5.0 20
0.054 1091020.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 6.6 20
0.046 93.094.60.0470.050mg/Kg1,2-Dibromoethane 70-132 1.7 20
0.047 95.097.00.0480.050mg/KgDibromomethane 74-133 2.0 20
0.046 92.290.80.0450.050mg/Kg1,2-Dichlorobenzene 72-123 1.5 20
0.043 87.492.40.0460.050mg/Kg1,3-Dichlorobenzene 71-120 5.5 20
0.043 86.493.00.0460.050mg/Kg1,4-Dichlorobenzene 71-123 7.3 20
0.034 68.070.40.0350.050mg/KgDichlorodifluoromethane 26-146 3.4 20
0.042 84.491.40.0450.050mg/Kg1,1-Dichloroethane 74-127 7.9 20
Page 15 of 28Date:10/01/2021 11:03 AM
Page 84 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9216QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V9215
LCS-V9215 LCSD-V9215Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.043 87.090.60.0450.050mg/Kg1,2-Dichloroethane 68-128 4.0 20
0.043 87.092.40.0460.050mg/Kg1,1-Dichloroethene 67-149 6.0 20
0.042 85.693.40.0460.050mg/Kgcis-1,2-Dichloroethene 76-134 8.7 20
0.042 85.289.20.0440.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.5 20
0.044 89.095.80.0470.050mg/Kg1,2-Dichloropropane 73-130 7.3 20
0.045 90.293.20.0460.050mg/Kg1,3-Dichloropropane 75-124 3.2 20
0.043 86.097.60.0480.050mg/Kg2,2-Dichloropropane 50-142 12.6 20
0.041 82.693.40.0460.050mg/Kg1,1-Dichloropropene 71-130 12.2 20
0.046 93.698.00.0490.050mg/Kgcis-1,3-Dichloropropene 71-125 4.5 20
0.047 95.096.40.0480.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.4 20
0.042 84.892.60.0460.050mg/KgEthylbenzene 74-128 8.7 20
0.092 0.0*0.0*0.0960.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.0 20
0.047 95.298.40.0490.050mg/KgHexachlorobutadiene 64-125 3.3 20
0.045 90.496.40.0480.050mg/Kgn-Hexane 70-130 6.4 20
0.054 1091080.0530.050mg/Kg2-Hexanone 61-157 0.7 20
0.042 85.294.20.0470.050mg/KgIsopropylbenzene 68-126 10.0 20
0.043 86.694.80.0470.050mg/Kg4-Isopropyl toluene 68-129 9.0 20
0.054 1091100.0550.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.4 20
0.047 95.094.40.0470.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.6 20
0.042 85.284.20.0420.050mg/KgMethylene Chloride 74-129 1.1 20
0.051 10398.60.0490.050mg/KgNaphthalene 57-157 4.7 20
0.042 84.493.60.0460.050mg/Kgn-Propylbenzene 67-130 10.3 20
0.044 89.695.60.0470.050mg/KgStyrene 77-121 6.4 20
0.045 90.294.00.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.1 20
0.044 89.693.80.0460.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 4.5 20
0.043 86.492.20.0460.050mg/KgTetrachloroethene 68-130 6.4 20
Page 16 of 28* QC Fail Date:10/01/2021 11:03 AM
Page 85 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9216QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V9215
LCS-V9215 LCSD-V9215Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.043 87.292.00.0460.050mg/KgToluene 71-129 5.3 20
0.049 99.697.20.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.4 20
0.049 98.697.40.0480.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.2 20
0.042 84.093.20.0460.050mg/Kg1,1,1-Trichloroethane 67-131 10.3 20
0.046 93.094.60.0470.050mg/Kg1,1,2-Trichloroethane 70-133 1.7 20
0.043 86.493.20.0460.050mg/KgTrichloroethene 75-133 7.5 20
0.042 85.289.80.0440.050mg/KgTrichlorofluoromethane 44-146 5.2 20
0.046 92.693.80.0460.050mg/Kg1,2,3-Trichloropropane 60-137 1.2 20
0.043 87.094.20.0470.050mg/Kg1,3,5-Trimethylbenzene 69-128 7.9 20
0.050 1021100.0550.050mg/KgVinyl Acetate 60-140 7.9 20
0.040 81.885.00.0420.050mg/KgVinyl Chloride 48-147 3.8 20
0.043 87.694.60.0470.050mg/Kgo-Xylene 74-126 7.6 20
0.088 88.295.40.0950.100mg/Kgm,p-Xylene 75-124 7.8 20
1001024-Bromofluorobenzene (S)70-130
97.698.4Dibromofluoromethane (S)70-130
98.8102Toluene-d8 (S)76-129
Page 17 of 28Date:10/01/2021 11:03 AM
Page 86 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9259QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9195
Associated Lab Samples: 95805, 95806, 95807, 95808, 95809
LRB-V9195 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/23/21 17:080.6600.116<0.116mg/KgAcenaphthene
09/23/21 17:080.6600.105<0.105mg/KgAcenaphthylene
09/23/21 17:080.6600.152<0.152mg/KgAniline
09/23/21 17:080.6600.143<0.143mg/KgAnthracene
09/23/21 17:080.6600.139<0.139mg/KgBenzo(a)anthracene
09/23/21 17:080.6600.147<0.147mg/KgBenzo(a)pyrene
09/23/21 17:080.6600.146<0.146mg/KgBenzo(b)fluoranthene
09/23/21 17:080.6600.136<0.136mg/KgBenzo(g,h,i)perylene
09/23/21 17:080.6600.137<0.137mg/KgBenzo(k)fluoranthene
09/23/21 17:082.000.580<0.580mg/KgBenzoic Acid
09/23/21 17:080.6600.105<0.105mg/KgBenzyl alcohol
09/23/21 17:080.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
09/23/21 17:080.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
09/23/21 17:080.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
09/23/21 17:080.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
09/23/21 17:080.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
09/23/21 17:080.3300.113<0.113mg/KgButyl benzyl phthalate
09/23/21 17:080.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
09/23/21 17:080.3300.112<0.112mg/Kg4-Chloroaniline
09/23/21 17:080.6600.116<0.116mg/Kg2-Chloronaphthalene
09/23/21 17:080.6600.098<0.098mg/Kg2-Chlorophenol
09/23/21 17:081.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
09/23/21 17:080.6600.142<0.142mg/KgChrysene
09/23/21 17:080.6600.230<0.230mg/KgDibenz(a,h)anthracene
09/23/21 17:080.6600.119<0.119mg/KgDibenzofuran
09/23/21 17:080.6600.094<0.094mg/Kg1,2-Dichlorobenzene
09/23/21 17:080.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 18 of 28Date:10/01/2021 11:03 AM
Page 87 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9259QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9195
Associated Lab Samples: 95805, 95806, 95807, 95808, 95809
LRB-V9195 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/23/21 17:080.3300.097<0.097mg/Kg1,4-Dichlorobenzene
09/23/21 17:080.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
09/23/21 17:080.6600.095<0.095mg/Kg2,4-Dichlorophenol
09/23/21 17:080.6600.180<0.180mg/KgDiethyl phthalate
09/23/21 17:080.6600.174<0.174mg/KgDimethyl phthalate
09/23/21 17:080.3300.108<0.108mg/Kg2,4-Dimethylphenol
09/23/21 17:080.6600.107<0.107mg/KgDi-n-butyl phthalate
09/23/21 17:081.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
09/23/21 17:081.500.520<0.520mg/Kg2,4-Dinitrophenol
09/23/21 17:080.6600.096<0.096mg/Kg2,4-Dinitrotoluene
09/23/21 17:080.6600.108<0.108mg/Kg2,6-Dinitrotoluene
09/23/21 17:080.3300.143<0.143mg/KgDi-n-Octyl Phthalate
09/23/21 17:080.6600.123<0.123mg/KgFluoranthene
09/23/21 17:080.6600.128<0.128mg/KgFluorene
09/23/21 17:080.6600.106<0.106mg/KgHexachlorobenzene
09/23/21 17:080.6600.097<0.097mg/KgHexachlorobutadiene
09/23/21 17:080.6600.157<0.157mg/KgHexachlorocyclopentadiene
09/23/21 17:080.6600.079<0.079mg/KgHexachloroethane
09/23/21 17:080.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
09/23/21 17:080.6600.191<0.191mg/KgIsophorone
09/23/21 17:080.6600.106<0.106mg/Kg1-Methylnaphthalene
09/23/21 17:080.6600.100<0.100mg/Kg2-Methylnaphthalene
09/23/21 17:080.6600.097<0.097mg/Kg2-Methylphenol
09/23/21 17:080.6600.084<0.084mg/Kg3&4 Methylphenol
09/23/21 17:080.6600.144<0.144mg/KgNaphthalene
09/23/21 17:080.6600.096<0.096mg/Kg2-Nitroaniline
09/23/21 17:080.6600.120<0.120mg/Kg3-Nitroaniline
Page 19 of 28Date:10/01/2021 11:03 AM
Page 88 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9259QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9195
Associated Lab Samples: 95805, 95806, 95807, 95808, 95809
LRB-V9195 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/23/21 17:080.3300.093<0.093mg/Kg4-Nitroaniline
09/23/21 17:080.3300.116<0.116mg/KgNitrobenzene
09/23/21 17:080.6600.088<0.088mg/Kg2-Nitrophenol
09/23/21 17:080.6600.117<0.117mg/Kg4-Nitrophenol
09/23/21 17:080.6600.263<0.263mg/KgN-Nitrosodimethylamine
09/23/21 17:080.6600.181<0.181mg/KgN-Nitrosodiphenylamine
09/23/21 17:080.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
09/23/21 17:081.000.347<0.347mg/KgPentachlorophenol
09/23/21 17:080.6600.208<0.208mg/KgPhenanthrene
09/23/21 17:080.6600.112<0.112mg/KgPhenol
09/23/21 17:080.6600.134<0.134mg/KgPyrene
09/23/21 17:080.3300.079<0.079mg/KgPyridine
09/23/21 17:080.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
09/23/21 17:080.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
09/23/21 17:080.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
09/23/21 17:082-Fluorobiphenyl (S)63.4 44-115
09/23/21 17:082-Fluorophenol (S)53.1 35-115
09/23/21 17:08Nitrobenzene-d5 (S)54.9 37-122
09/23/21 17:084-Terphenyl-d14 (S)67.0 54-127
09/23/21 17:082,4,6-Tribromophenol (S)76.5 39-132
09/23/21 17:08Phenol-d5 (S)53.4 34-121
LCS-V9195Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
80.21.341.67mg/KgAcenaphthene 40-123
83.21.391.67mg/KgAcenaphthylene 32-132
Page 20 of 28Date:10/01/2021 11:03 AM
Page 89 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9259QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9195
LCS-V9195Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
71.21.191.67mg/KgAniline 12-197
80.81.351.67mg/KgAnthracene 47-123
79.01.321.67mg/KgBenzo(a)anthracene 49-126
94.01.571.67mg/KgBenzo(a)pyrene 45-129
84.41.411.67mg/KgBenzo(b)fluoranthene 45-132
82.01.371.67mg/KgBenzo(g,h,i)perylene 43-134
83.81.401.67mg/KgBenzo(k)fluoranthene 47-132
0.0*1.011.67mg/KgBenzoic Acid 10-83
68.81.151.67mg/KgBenzyl alcohol 29-122
71.81.201.67mg/KgBis(2-Chloroethoxy)methane 36-121
65.21.091.67mg/KgBis(2-Chloroethyl)ether 31-120
55.60.9301.67mg/KgBis(2-Chloroisopropyl)ether 33-131
78.41.311.67mg/KgBis(2-ethylhexyl)phthalate 51-133
88.61.481.67mg/Kg4-Bromophenyl phenyl ether 46-124
70.61.181.67mg/KgButyl benzyl phthalate 48-132
79.01.321.67mg/Kg4-Chloro-3-methylphenol 45-122
61.01.021.67mg/Kg4-Chloroaniline 17-106
79.61.331.67mg/Kg2-Chloronaphthalene 41-114
75.41.261.67mg/Kg2-Chlorophenol 34-121
88.01.471.67mg/Kg4-Chlorophenyl phenyl ether 45-121
80.21.341.67mg/KgChrysene 50-124
0.0*0.6551.67mg/KgDibenz(a,h)anthracene 45-134
81.41.361.67mg/KgDibenzofuran 44-120
68.81.151.67mg/Kg1,2-Dichlorobenzene 33-117
68.21.141.67mg/Kg1,3-Dichlorobenzene 30-115
66.41.111.67mg/Kg1,4-Dichlorobenzene 31-115
70.61.181.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 21 of 28* QC Fail Date:10/01/2021 11:03 AM
Page 90 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9259QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9195
LCS-V9195Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
77.21.291.67mg/Kg2,4-Dichlorophenol 40-122
83.81.401.67mg/KgDiethyl phthalate 50-124
81.41.361.67mg/KgDimethyl phthalate 48-124
79.61.331.67mg/Kg2,4-Dimethylphenol 30-127
86.21.441.67mg/KgDi-n-butyl phthalate 51-128
0.0*1.391.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
0.0*1.431.67mg/Kg2,4-Dinitrophenol 27-129
92.81.551.67mg/Kg2,4-Dinitrotoluene 48-126
91.61.531.67mg/Kg2,6-Dinitrotoluene 46-124
73.01.221.67mg/KgDi-n-Octyl Phthalate 45-140
86.21.441.67mg/KgFluoranthene 50-127
82.01.371.67mg/KgFluorene 43-125
94.01.571.67mg/KgHexachlorobenzene 45-122
78.41.311.67mg/KgHexachlorobutadiene 32-123
71.81.201.67mg/KgHexachlorocyclopentadiene 32-117
65.81.101.67mg/KgHexachloroethane 28-117
80.21.341.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
54.50.9111.67mg/KgIsophorone 30-122
70.01.171.67mg/Kg1-Methylnaphthalene 40-119
70.61.181.67mg/Kg2-Methylnaphthalene 38-122
75.41.261.67mg/Kg2-Methylphenol 32-122
67.61.131.67mg/Kg3&4 Methylphenol 34-119
65.21.091.67mg/KgNaphthalene 35-123
80.21.341.67mg/Kg2-Nitroaniline 44-127
76.61.281.67mg/Kg3-Nitroaniline 33-119
86.21.441.67mg/Kg4-Nitroaniline 63-147
64.61.081.67mg/KgNitrobenzene 34-122
Page 22 of 28* QC Fail Date:10/01/2021 11:03 AM
Page 91 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9259QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9195
LCS-V9195Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
70.01.171.67mg/Kg2-Nitrophenol 36-123
83.21.391.67mg/Kg4-Nitrophenol 30-132
46.20.7721.67mg/KgN-Nitrosodimethylamine 10-146
94.01.571.67mg/KgN-Nitrosodiphenylamine 38-127
68.81.151.67mg/KgN-Nitroso-di-n-propylamine 36-120
1131.891.67mg/KgPentachlorophenol 25-133
81.41.361.67mg/KgPhenanthrene 50-121
71.21.191.67mg/KgPhenol 34-121
79.61.331.67mg/KgPyrene 47-127
36.80.6151.67mg/KgPyridine 10-80
71.21.191.67mg/Kg1,2,4-Trichlorobenzene 34-118
85.01.421.67mg/Kg2,4,5-Trichlorophenol 41-124
89.21.491.67mg/Kg2,4,6-Trichlorophenol 39-126
77.82-Fluorobiphenyl (S)44-115
70.82-Fluorophenol (S)35-115
61.6Nitrobenzene-d5 (S)37-122
82.64-Terphenyl-d14 (S)54-127
1082,4,6-Tribromophenol (S)39-132
68.4Phenol-d5 (S)34-121
V 95746-MS-V9195 V 95746-MSD-V9195Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.28 76.61.321.671.67<0.116mg/KgAcenaphthene 79.0 40-123 3.0 20
1.30 77.81.351.671.67<0.105mg/KgAcenaphthylene 80.8 32-132 3.7 20
0.659 0.0*0.6511.671.67<0.152mg/KgAniline 0.0*12-197 0.0 20
Page 23 of 28* QC Fail Date:10/01/2021 11:03 AM
Page 92 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9259QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9195
V 95746-MS-V9195 V 95746-MSD-V9195Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.31 78.41.301.671.67<0.143mg/KgAnthracene 77.8 47-123 0.7 20
1.26 75.41.261.671.67<0.139mg/KgBenzo(a)anthracene 75.4 49-126 0.0 20
1.50 89.81.541.671.67<0.147mg/KgBenzo(a)pyrene 92.2 45-129 2.6 20
1.34 80.21.361.671.67<0.146mg/KgBenzo(b)fluoranthene 81.4 45-132 1.4 20
1.31 78.41.321.671.67<0.136mg/KgBenzo(g,h,i)perylene 79.0 43-134 0.7 20
1.34 80.21.341.671.67<0.137mg/KgBenzo(k)fluoranthene 80.2 47-132 0.0 20
1.18 0.0*1.211.671.67<0.580mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.07 64.01.111.671.67<0.105mg/KgBenzyl alcohol 66.4 29-122 3.6 20
1.15 68.81.201.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 71.8 36-121 4.2 20
1.24 74.21.281.671.67<0.107mg/KgBis(2-Chloroethyl)ether 76.6 31-120 3.1 20
0.880 52.60.9021.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 54.0 33-131 2.4 20
1.25 74.81.341.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 80.2 51-133 6.9 20
1.45 86.81.441.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 86.2 46-124 0.6 20
1.13 67.61.151.671.67<0.113mg/KgButyl benzyl phthalate 68.8 48-132 1.7 20
1.28 76.61.321.671.67<0.092mg/Kg4-Chloro-3-methylphenol 79.0 45-122 3.0 20
0.991 59.31.011.671.67<0.112mg/Kg4-Chloroaniline 60.4 17-106 1.8 20
1.27 76.01.311.671.67<0.116mg/Kg2-Chloronaphthalene 78.4 41-114 3.1 20
1.20 71.81.241.671.67<0.098mg/Kg2-Chlorophenol 74.2 34-121 3.2 20
1.38 82.61.411.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 84.4 45-121 2.1 20
1.29 77.21.291.671.67<0.142mg/KgChrysene 77.2 50-124 0.0 20
0.624 0.0*0.6321.671.67<0.230mg/KgDibenz(a,h)anthracene 0.0*45-134 0.0 20
1.29 77.21.321.671.67<0.119mg/KgDibenzofuran 79.0 44-120 2.2 20
1.11 66.41.141.671.67<0.094mg/Kg1,2-Dichlorobenzene 68.2 33-117 2.6 20
1.10 65.81.121.671.67<0.097mg/Kg1,3-Dichlorobenzene 67.0 30-115 1.8 20
1.07 64.01.111.671.67<0.097mg/Kg1,4-Dichlorobenzene 66.4 31-115 3.6 20
1.02 61.01.031.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 61.6 22-121 0.9 20
Page 24 of 28* QC Fail Date:10/01/2021 11:03 AM
Page 93 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9259QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9195
V 95746-MS-V9195 V 95746-MSD-V9195Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.24 74.21.261.671.67<0.095mg/Kg2,4-Dichlorophenol 75.4 40-122 1.6 20
1.36 81.41.381.671.67<0.180mg/KgDiethyl phthalate 82.6 50-124 1.4 20
1.31 78.41.341.671.67<0.174mg/KgDimethyl phthalate 80.2 48-124 2.2 30
1.24 74.21.301.671.67<0.108mg/Kg2,4-Dimethylphenol 77.8 30-127 4.7 20
1.35 80.81.371.671.67<0.107mg/KgDi-n-butyl phthalate 82.0 51-128 1.4 20
1.34 0.0*1.351.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
1.44 0.0*1.421.671.67<0.520mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.49 89.21.501.671.67<0.096mg/Kg2,4-Dinitrotoluene 89.8 48-126 0.6 20
1.47 88.01.521.671.67<0.108mg/Kg2,6-Dinitrotoluene 91.0 46-124 3.3 20
1.15 68.81.161.671.67<0.143mg/KgDi-n-Octyl Phthalate 69.4 45-140 0.8 20
1.38 82.61.381.671.67<0.123mg/KgFluoranthene 82.6 50-127 0.0 20
1.32 79.01.361.671.67<0.128mg/KgFluorene 81.4 43-125 2.9 20
1.49 89.21.521.671.67<0.106mg/KgHexachlorobenzene 91.0 45-122 1.9 20
1.26 75.41.321.671.67<0.097mg/KgHexachlorobutadiene 79.0 32-123 4.6 20
1.16 69.41.191.671.67<0.157mg/KgHexachlorocyclopentadiene 71.2 32-117 2.5 20
1.08 64.61.101.671.67<0.079mg/KgHexachloroethane 65.8 28-117 1.8 20
1.30 77.81.321.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 79.0 45-133 1.5 20
0.874 52.30.9091.671.67<0.191mg/KgIsophorone 54.4 30-122 3.9 20
1.11 66.41.141.671.67<0.106mg/Kg1-Methylnaphthalene 68.2 40-119 2.6 20
1.09 65.21.151.671.67<0.100mg/Kg2-Methylnaphthalene 68.8 38-122 5.3 20
1.22 73.01.271.671.67<0.097mg/Kg2-Methylphenol 76.0 32-122 4.0 20
1.08 64.61.091.671.67<0.084mg/Kg3&4 Methylphenol 65.2 34-119 0.9 20
1.04 62.21.081.671.67<0.144mg/KgNaphthalene 64.6 35-123 3.7 20
1.31 78.41.321.671.67<0.096mg/Kg2-Nitroaniline 79.0 44-127 0.7 20
1.25 74.81.271.671.67<0.120mg/Kg3-Nitroaniline 76.0 33-119 1.5 20
1.39 83.21.411.671.67<0.093mg/Kg4-Nitroaniline 84.4 63-147 1.4 20
Page 25 of 28* QC Fail Date:10/01/2021 11:03 AM
Page 94 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9259QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9195
V 95746-MS-V9195 V 95746-MSD-V9195Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.03 61.61.071.671.67<0.116mg/KgNitrobenzene 64.0 34-122 3.8 20
1.12 67.01.181.671.67<0.088mg/Kg2-Nitrophenol 70.6 32-123 5.2 20
1.32 79.00.1481.671.67<0.117mg/Kg4-Nitrophenol 0.0*30-132 66.6*20
0.744 44.50.7531.671.67<0.263mg/KgN-Nitrosodimethylamine 45.0 10-146 1.2 30
1.48 88.61.481.671.67<0.181mg/KgN-Nitrosodiphenylamine 88.6 38-127 0.0 20
1.09 65.21.131.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 67.6 36-120 3.6 20
1.87 1121.881.671.67<0.347mg/KgPentachlorophenol 113 25-133 0.5 20
1.31 78.41.291.671.67<0.208mg/KgPhenanthrene 77.2 50-121 1.5 20
1.06 63.41.111.671.67<0.112mg/KgPhenol 66.4 34-121 4.6 20
1.29 77.21.271.671.67<0.134mg/KgPyrene 76.0 47-127 1.5 20
0.175 0.0*0.1881.671.67<0.079mg/KgPyridine 0.0*10-80 0.0 20
1.12 67.01.171.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 70.0 34-118 4.3 20
1.38 82.61.431.671.67<0.096mg/Kg2,4,5-Trichlorophenol 85.6 41-124 3.5 20
1.45 86.81.481.671.67<0.096mg/Kg2,4,6-Trichlorophenol 88.6 39-126 2.0 20
74.82-Fluorobiphenyl (S)72.4 44-115
68.12-Fluorophenol (S)65.7 35-115
58.8Nitrobenzene-d5 (S)58.0 37-122
80.24-Terphenyl-d14 (S)76.0 54-127
1052,4,6-Tribromophenol (S)102 39-132
64.8Phenol-d5 (S)62.4 34-121
Page 26 of 28* QC Fail Date:10/01/2021 11:03 AM
Page 95 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
Dry Weight Determination
SW-DRYWT
V9193QC Analytical Batch:
Analysis Method:
Analysis Description:
V 95756-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/23/21 13:481.018.418.6%Moisture
V 95807-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/23/21 13:480.519.920.0%Moisture
Page 27 of 28Date:10/01/2021 11:03 AM
Page 96 of 99
Quality Control Data
21-265-0007Report No:
Project Description:
Client ID:Proctor Environmental Services, Inc.
NHX, Raleigh
Dry Weight Determination
SW-DRYWT
V9204QC Analytical Batch:
Analysis Method:
Analysis Description:
V 95619-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/23/21 16:373.422.523.3%Moisture
V 95803-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/23/21 16:371.519.619.9%Moisture
Page 28 of 28Date:10/01/2021 11:03 AM
Page 97 of 99
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-265-0007
Proctor Environmental Services, Inc.
01166
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 4.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Sarah J. Locklear Date & Time:09/22/2021 12:07:03
Special precautions or instructions included?
Comments:
Page 98 of 99
Page 99 of 99
Brownfield Dirt Export Log
Northhills Expansion
Date Haul Brownfield Red Rock Haul to Haul to Seaboard East End Triangle Area Earth
Location Landfill (CY) CY 516 Cabarrus (CY) Station (CY) Market (CY) (CY)
6/18/2021 Brownfield Landfill 2600 Brownfield Rd 504
6/19/2021 Brownfield Landfill 2600 Brownfield Rd 324
6/21/2021 Brownfield Landfill 2600 Brownfield Rd 552
6/22/2021 Brownfield Landfill 2600 Brownfield Rd 156
6/23/2021 Brownfield Landfill 2600 Brownfield Rd 858
6/24/2021 Brownfield Landfill 2600 Brownfield Rd 1498
6/24/2021 Yardage Correction 6-24-21 28
6/25/2021 Brownfield Landfill 2600 Brownfield Rd 1630
6/28/2021 Brownfield Landfill 2600 Brownfield Rd 1200
6/29/2021 Brownfield Landfill 2600 Brownfield Rd 1328
6/30/2021 Brownfield Landfill 2600 Brownfield Rd 1310
7/1/2021 Brownfield Landfill 2600 Brownfield Rd 1138
7/6/2021 Brownfield Landfill 2600 Brownfield Rd 1272
7/7/2021 Brownfield Landfill 2600 Brownfield Rd 1488
7/10/2021 Brownfield Landfill 2600 Brownfield Rd 866
7/12/2021 Brownfield Landfill 2600 Brownfield Rd 950
7/13/2021 Brownfield Landfill 2600 Brownfield Rd 842
7/14/2021 Brownfield Landfill 2600 Brownfield Rd 1050
7/15/2021 Brownfield Landfill 2600 Brownfield Rd 870
7/27/2021 Brownfield Landfill 2600 Brownfield Rd 264
7/27/2021 Yardage Correction 7-27-21 -2
8/9/2021 Brownfield Landfill 2600 Brownfield Rd 432
8/10/2021 Brownfield Landfill 2600 Brownfield Rd 286
8/12/2013 Brownfield Landfill 2600 Brownfield Rd 496
8/13/2021 Brownfield Landfill 2600 Brownfield Rd 124
8/23/2021 Brownfield Landfill 2600 Brownfield Rd 216
9/3/2021 516 W. Cabarrus Street 1132
9/7/2021 516 W. Cabarrus Street 412
9/8/2021 516 W. Cabarrus Street 528
9/15/2021 516 W. Cabarrus Street 612
9/16/2021 516 W. Cabarrus Street 456
9/17/2021 516 W. Cabarrus Street 468
9/20/2021 Brownfield Landfill 2600 Brownfield Rd 300
9/21/2021 Triangle Area Earth 192
9/24/2021 Brownfield Landfill 2600 Brownfield Rd 720
9/25/2021 Brownfield Landfill 2600 Brownfield Rd 504
9/27/2021 Brownfield Landfill 2600 Brownfield Rd 528
9/29/2021 Brownfield Landfill 2600 Brownfield Rd 410
9/30/2021 Brownfield Landfill 2600 Brownfield Rd 658
10/2/2021 Brownfield Landfill 2600 Brownfield Rd 902
10/4/2021 Brownfield Landfill 2600 Brownfield Rd 228
10/4/2021 Brownfield Landfill 2600 Brownfield Rd 48
10/5/2021 Brownfield Landfill 2600 Brownfield Rd 672
10/6/2021 Brownfield Landfill 2600 Brownfield Rd 458
10/6/2021 Seaboard Station 288
10/7/2021 Brownfield Landfill 2600 Brownfield Rd 644
10/7/2021 Yardage Correction 10-7-21 -14
10/7/2021 Seaboard Station 204
10/8/2021 Brownfield Landfill 2600 Brownfield Rd 608
10/8/2021 Yardage Correction 10-8-21 -10
10/8/2021 Seaboard Station 180
10/12/2021 Brownfield Landfill 2600 Brownfield Rd 1108
10/12/2021 Yardage Correction 10-12-21 -14
10/12/2021 Seaboard Station 168
10/13/2021 Brownfield Landfill 2600 Brownfield Rd 624
10/13/2021 Seaboard Station 276
10/13/2021 Cabarrus 480
10/14/2021 Brownfield Landfill 2600 Brownfield Rd 1500
10/14/2021 Yardage Correction 10-14-21 72
10/14/2021 Seaboard Station 216
10/14/2021 Cabarrus 276
10/15/2021 Cabarrus 348
10/16/2021 Brownfield Landfill 2600 Brownfield Rd 562
10/18/2021 Brownfield Landfill 2600 Brownfield Rd 204
10/18/2021 Cabarrus 468
10/18/2021 Cabarrus - Yardage Correction -10
10/19/2021 Cabarrus 626
10/20/2021 Brownfield Landfill 2600 Brownfield Rd 48
10/20/2021 Cabarrus 550
10/20/2021 Cabarrus - Yardage Correction 120
10/21/2021 Brownfield Landfill 2600 Brownfield Rd 428
10/21/2021 Cabarrus 372
10/22/2021 Brownfield Landfill 2600 Brownfield Rd 696
10/22/2021 Cabarrus 288
10/23/2021 Brownfield Landfill 2600 Brownfield Rd 612
10/25/2021 Brownfield Landfill 2600 Brownfield Rd 444
10/26/2021 Brownfield Landfill 2600 Brownfield Rd 724
Brownfield Dirt Export Log
Northhills Expansion
Date Haul Brownfield Red Rock Haul to Haul to Seaboard East End Triangle Area Earth
Location Landfill (CY) CY 516 Cabarrus (CY) Station (CY) Market (CY) (CY)
10/26/2021 Cabarrus 12
10/28/2021 Brownfield Landfill 2600 Brownfield Rd 678
10/30/2021 Brownfield Landfill 2600 Brownfield Rd 132
11/1/2021 Brownfield Landfill 2600 Brownfield Rd 1100
11/2/2021 Brownfield Landfill 2600 Brownfield Rd 850
11/3/2021 Brownfield Landfill 2600 Brownfield Rd 802
11/3/2021 Yardage Correction 11-3-21 12
11/8/2021 Brownfield Landfill 2600 Brownfield Rd 972
11/9/2021 Brownfield Landfill 2600 Brownfield Rd 820
11/9/2021 Yardage Correction 11-9-21 14
11/10/2021 Brownfield Landfill 2600 Brownfield Rd 1080
11/11/2021 Brownfield Landfill 2600 Brownfield Rd 1004
11/12/2021 Brownfield Landfill 2600 Brownfield Rd 596
11/13/2021 Brownfield Landfill 2600 Brownfield Rd 804
11/15/2021 Brownfield Landfill 2600 Brownfield Rd 826
11/16/2021 Brownfield Landfill 2600 Brownfield Rd 830
11/17/2021 Brownfield Landfill 2600 Brownfield Rd 870
11/18/2021 Brownfield Landfill 2600 Brownfield Rd 1016
11/19/2021 Brownfield Landfill 2600 Brownfield Rd 982
11/19/2021 Yardage Correction 11-19-21 60
11/20/2021 Brownfield Landfill 2600 Brownfield Rd 638
11/29/2021 Brownfield Landfill 2600 Brownfield Rd 1348
11/30/2021 Brownfield Landfill 2600 Brownfield Rd 1066
12/1/2021 Brownfield Landfill 2600 Brownfield Rd 950
12/2/2021 Brownfield Landfill 2600 Brownfield Rd 1166
12/3/2021 Brownfield Landfill 2600 Brownfield Rd 958
12/3/2021 Yardage Correction 12/3/21 14
12/4/2021 Brownfield Landfill 2600 Brownfield Rd 1480
12/6/2021 Brownfield Landfill 2600 Brownfield Rd 1214
12/7/2021 Brownfield Landfill 2600 Brownfield Rd 872
12/10/2021 Brownfield Landfill 2600 Brownfield Rd 1222
12/10/2021 Seaboard Station 300
12/11/2021 Brownfield Landfill 2600 Brownfield Rd 1718
12/13/2021 Brownfield Landfill 2600 Brownfield Rd 908
12/13/2021 Seaboard Station 120
12/14/2021 Brownfield Landfill 2600 Brownfield Rd 466
12/15/2021 Brownfield Landfill 2600 Brownfield Rd 806
12/16/2021 Brownfield Landfill 2600 Brownfield Rd 666
12/17/2021 Brownfield Landfill 2600 Brownfield Rd 576
12/18/2021 Brownfield Landfill 2600 Brownfield Rd 778
12/21/2021 Brownfield Landfill 2600 Brownfield Rd 742
12/23/2021 Brownfield Landfill 2600 Brownfield Rd 924
12/27/2021 Brownfield Landfill 2600 Brownfield Rd 1454
12/28/2021 Brownfield Landfill 2600 Brownfield Rd 1272
12/30/2021 Brownfield Landfill 2600 Brownfield Rd 12
1/8/2022 Brownfield Landfill 2600 Brownfield Rd 972
1/10/2022 Brownfield Landfill 2600 Brownfield Rd 620
1/11/2022 Brownfield Landfill 2600 Brownfield Rd 1016
1/12/2022 Brownfield Landfill 2600 Brownfield Rd 1164
1/13/2022 Brownfield Landfill 2600 Brownfield Rd 644
1/18/2022 Brownfield Landfill 2600 Brownfield Rd 0
1/19/2022 Brownfield Landfill 2600 Brownfield Rd 96
1/22/2022 Brownfield Landfill 2600 Brownfield Rd 216
1/25/2022 Brownfield Landfill 2600 Brownfield Rd 0
1/26/2022 Brownfield Landfill 2600 Brownfield Rd 420
1/27/2022 Brownfield Landfill 2600 Brownfield Rd 516
1/28/2022 Brownfield Landfill 2600 Brownfield Rd 912
1/31/2022 Brownfield Landfill 2600 Brownfield Rd 468
2/1/2022 Brownfield Landfill 2600 Brownfield Rd 898
2/2/2022 Brownfield Landfill 2600 Brownfield Rd 1130
2/3/2022 Brownfield Landfill 2600 Brownfield Rd 1322
2/3/2022 Yardage Correction 4-12-22 84
2/10/2022 Brownfield Landfill 2600 Brownfield Rd 974
2/10/2022 Yardage Correction 2-14-22 72
2/11/2022 Brownfield Landfill 2600 Brownfield Rd 946
2/11/2022 Yardage Correction 3-11-22 12
2/12/2022 Brownfield Landfill 2600 Brownfield Rd 1176
2/14/2022 Brownfield Landfill 2600 Brownfield Rd 1334
2/15/2022 Brownfield Landfill 2600 Brownfield Rd 1294
2/16/2022 Brownfield Landfill 2600 Brownfield Rd 1354
2/17/2022 Brownfield Landfill 2600 Brownfield Rd 1646
2/21/2022 Brownfield Landfill 2600 Brownfield Rd 914
2/22/2022 Brownfield Landfill 2600 Brownfield Rd 156
2/23/2022 Brownfield Landfill 2600 Brownfield Rd 332
2/24/2022 Brownfield Landfill 2600 Brownfield Rd 1340
2/24/2022 Yardage Correction 3-24-22 36
2/28/2022 Brownfield Landfill 2600 Brownfield Rd 552
Brownfield Dirt Export Log
Northhills Expansion
Date Haul Brownfield Red Rock Haul to Haul to Seaboard East End Triangle Area Earth
Location Landfill (CY) CY 516 Cabarrus (CY) Station (CY) Market (CY) (CY)
3/1/2022 Brownfield Landfill 2600 Brownfield Rd 662
3/2/2022 Brownfield Landfill 2600 Brownfield Rd 530
3/7/2022 East End Market 12
3/8/2022 East End Market 1320
3/15/2022 East End Market 1144
3/16/2022 East End Market 698
3/16/2022 Brownfield Landfill 2600 Brownfield Rd 286
3/21/2022 East End Market 1056
3/22/2022 East End Market 1516
3/23/2022 East End Market 916
3/28/2022 East End Market 1408
3/29/2022 East End Market 792
4/4/2022 East End Market 988
4/5/2022 East End Market 772
4/7/2022 Brownfield Landfill 2600 Brownfield Rd 654
4/9/2022 Brownfield Landfill 2600 Brownfield Rd 758
4/11/2022 Brownfield Landfill 2600 Brownfield Rd 304
4/12/2022 Brownfield Landfill 2600 Brownfield Rd 730
4/13/2022 Brownfield Landfill 2600 Brownfield Rd 96
4/20/2022 Brownfield Landfill 2600 Brownfield Rd 140
4/21/2022 Brownfield Landfill 2600 Brownfield Rd 346
4/22/2022 Brownfield Landfill 2600 Brownfield Rd 302
4/25/2022 Brownfield Landfill 2600 Brownfield Rd 540
4/26/2022 Brownfield Landfill 2600 Brownfield Rd 564
4/27/2022 Brownfield Landfill 2600 Brownfield Rd 192
4/30/2022 Brownfield Landfill 2600 Brownfield Rd 156
5/2/2022 Brownfield Landfill 2600 Brownfield Rd 204
5/4/2022 Brownfield Landfill 2600 Brownfield Rd 276
5/5/2022 Brownfield Landfill 2600 Brownfield Rd 88
5/11/2022 Brownfield Landfill 2600 Brownfield Rd 204
5/12/2022 Brownfield Landfill 2600 Brownfield Rd 120
5/17/2022 Brownfield Landfill 2600 Brownfield Rd 96
6/8/2022 Brownfield Landfill 2600 Brownfield Rd 186
6/9/2022 Brownfield Landfill 2600 Brownfield Rd 72
6/10/2022 Brownfield Landfill 2600 Brownfield Rd 108
6/11/2022 Brownfield Landfill 2600 Brownfield Rd 164
6/13/2022 Brownfield Landfill 2600 Brownfield Rd 36
6/14/2022 Brownfield Landfill 2600 Brownfield Rd 48
6/15/2022 Brownfield Landfill 2600 Brownfield Rd 168
6/20/2022 Brownfield Landfill 2600 Brownfield Rd 24
6/22/2022 Brownfield Landfill 2600 Brownfield Rd 48
6/23/2022 Brownfield Landfill 2600 Brownfield Rd 84
6/27/2022 Brownfield Landfill 2600 Brownfield Rd 128
7/1/2022 Brownfield Landfill 2600 Brownfield Rd 84
7/5/2022 Brownfield Landfill 2600 Brownfield Rd 72
7/6/2022 Brownfield Landfill 2600 Brownfield Rd 294
7/7/2022 Brownfield Landfill 2600 Brownfield Rd 112
7/12/2022 Brownfield Landfill 2600 Brownfield Rd 144
7/13/2022 Brownfield Landfill 2600 Brownfield Rd 240
7/14/2022 Brownfield Landfill 2600 Brownfield Rd 300
7/15/2022 Brownfield Landfill 2600 Brownfield Rd 192
7/18/2022 Brownfield Landfill 2600 Brownfield Rd 456
7/19/2022 Brownfield Landfill 2600 Brownfield Rd 384
7/20/2022 Brownfield Landfill 2600 Brownfield Rd 48
7/22/2022 Brownfield Landfill 2600 Brownfield Rd 238
7/26/2022 Brownfield Landfill 2600 Brownfield Rd 84
7/27/2022 Brownfield Landfill 2600 Brownfield Rd 24
7/29/2022 Brownfield Landfill 2600 Brownfield Rd 12
8/1/2022 Brownfield Landfill 2600 Brownfield Rd 144
8/2/2022 Brownfield Landfill 2600 Brownfield Rd 140
8/3/2022 Brownfield Landfill 2600 Brownfield Rd 168
8/4/2022 Brownfield Landfill 2600 Brownfield Rd 84
8/9/2022 Brownfield Landfill 2600 Brownfield Rd 120
8/17/2022 Brownfield Landfill 2600 Brownfield Rd 12
8/23/2022 Brownfield Landfill 2600 Brownfield Rd 60
8/24/2022 Brownfield Landfill 2600 Brownfield Rd 36
9/12/2022 Brownfield Landfill 2600 Brownfield Rd 60
9/12/2022 Red Rock 204
9/13/2022 Brownfield Landfill 2600 Brownfield Rd 204
9/14/2022 Brownfield Landfill 2600 Brownfield Rd 84
9/22/2022 Brownfield Landfill 2600 Brownfield Rd 60
9/29/2022 Red Rock 48
10/3/2022 Red Rock 120
10/4/2022 Red Rock 288
10/7/2022 Red Rock 48
10/10/2022 Red Rock 48
10/11/2022 Red Rock 12
Brownfield Dirt Export Log
Northhills Expansion
Date Haul Brownfield Red Rock Haul to Haul to Seaboard East End Triangle Area Earth
Location Landfill (CY) CY 516 Cabarrus (CY) Station (CY) Market (CY) (CY)
10/12/2022 Red Rock 50
10/14/2022 Red Rock 276
10/15/2022 Red Rock 84
10/17/2022 Red Rock 184
10/18/2022 Red Rock 312
10/19/2022 Red Rock 72
10/20/2022 Red Rock 66
10/21/2022 Red Rock 24
10/22/2022 Red Rock 408
Totals 102480 2592 7138 1752 10622 192