27049_Nisbet Marine_Phase II_20221026 rev 20231213

October 26, 2022
Revised: December 13, 2023

Mr. Kevin Christiansen Catalyst Capital Partners 1600 Camden Road, Suite 200 Charlotte, North Carolina 28203 Reference: Report of Environmental Assessment Services, Revision 1 1320/1328 South Tryon Street Property 1320 and 1328 South Tryon Street Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:17700-A Dear Mr. Christiansen: ECS Southeast, LLP (ECS) is pleased to provide Catalyst Capital Partners (Catalyst) with the results of our environmental assessment for the above-referenced site. ECS’s services were provided in accordance with ECS proposal No. 49:32612P authorized on August 17, 2022. This report was initially submitted to Catalyst on October 26, 2022, and subsequently submitted to the North Carolina Department of Environmental Quality, Brownfields Redevelopment Section (BRS) as part of a Brownfields Property Application dated September 18, 2023. After review by the BRS, comments and requested edits to the report were received from Ms. Carolyn Minnich of the BRS via email on December 12, 2023. This revised version incorporates those comments and edits. ECS appreciates the opportunity to provide our services to you. If there are questions regarding this report, or a need for further information, please contact us. Respectfully submitted, ECS SOUTHEAST, LLP
Scott Young, P.G. Roger A. Smith, P.G.
Senior Environmental Project Manager Senior Principal Geologist
[e-mail] [e-mail]
704-525-5152 704-525-5152

NC Corporate Geology License #C-553

Report of Environmental Assessment Services, Revision 1.0
1320/1328 South Tryon Street Property
1320 and 1328 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:17700-A
December 13, 2023

1
TABLE OF CONTENTS
1.0 PROJECT INFORMATION .................................................................................................................... 1
2.0 SCOPE OF SERVICES ............................................................................................................................ 2
2.1 Utility Locate ....................................................................................................................................... 2
2.2 Soil Boring Activities ............................................................................................................................ 2
2.3 Soil Sample Collection ......................................................................................................................... 3
2.4 Temporary Monitoring Well Installation ............................................................................................. 3
2.5 Groundwater Sample Collection ......................................................................................................... 3
2.6 Soil Gas Boring and Sample Collection Activities ................................................................................ 4
3.0 RESULTS .............................................................................................................................................. 5
3.1 Soil Samples Analytical Results............................................................................................................ 5
3.2 Groundwater Samples Analytical Results ............................................................................................ 5
3.3 Soil Gas Samples Analytical Results ..................................................................................................... 5
4.0 CONCLUSIONS .................................................................................................................................... 6
5.0 RECOMMENDATIONS ......................................................................................................................... 7
6.0 QUALIFICATIONS OF REPORT ............................................................................................................. 7
FIGURES Figure 1 USGS Topographic Map Figure 2 Sample Location Map TABLES Table 1 Summary of Soil Samples Analytical Results Table 2 Summary of Groundwater Samples Analytical Results Table 3 Summary of Soil Gas Samples Analytical Results APPENDICES Appendix A Boring Logs and Well Construction/Abandonment Forms Appendix B Laboratory Analytical Report and Chain of Custody Record Appendix C NCDEQ Risk Calculator Output
Report of Environmental Assessment Services, Revision 1.0
1320/1328 South Tryon Street Property
1320 and 1328 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:17700-A
December 13, 2023

1
1.0 PROJECT INFORMATION

The subject property is located at 1320 and 1328 South Tryon Street, Charlotte, Mecklenburg County,
North Carolina (Figure 1) identified by Mecklenburg County GIS as Parcel Identification Numbers
07307206 and 07307205 and owned by Driggers Electric & Control Company, Inc. The approximate 0.63-
acre subject property consists of fenced in vacant land that appears to be utilized as parking for
construction vehicles. ECS previously conducted a Phase I Environmental Site Assessment (Phase I ESA)
for the subject property (ECS Project No. 49:17700 dated July 15, 2022). As noted in the Phase I ESA, the
following Recognized Environmental Conditions (RECs) was identified:

• City Directory listings from the 1930s up to the late 1970s for the subject property included Nisbet
Company Fuel Burning Equipment and Marine Mart. Due to the unknown nature of the business
this listing is considered a REC.
• American Dry-Cleaning Company, 1406 South Tryon Street - This facility is the southern adjacent
property across West Bland Street. This facility is in a presumed downgradient hydrogeological
position from the subject property. According to the EDR report this facility operated as a
drycleaning company and rug and carpet cleaners in 1925. Based on the proximity to the subject
property and the nature of dry-cleaning chemicals to impact subsurface conditions or pose a
vapor concern, ECS believes issues at this facility would result in a REC for the subject property.
• Wright Cleaning Company Incorporated, 1414 South Tryon Street - This facility is the southern
adjacent property across West Bland Street. This facility is in a presumed upgradient
hydrogeological position from the subject property. According to the EDR report, this facility listed
as Wright Cleaning Company Incorporated/Laundries Steam from 1953 up until 1975. Based on
the proximity to the subject property, the duration of operations, and the nature of dry-cleaning
chemicals to impact subsurface conditions or pose a vapor concern, ECS believes issues at this
facility would result in a REC for the subject property.
• Carroll Aligning Service Company, 1305 South Tryon Street -This facility is located approximately
250 feet north and is situated in a presumed downgradient hydrogeological position relative to
the subject property. According to the EDR report, an incident occurred on October 23, 2006. The
facility was issued a Notice of Regulatory Requirement (NORR) on November 30, 2006. According
to the EDR report, the incident was closed out on January 29, 2007. Based on the proximity to the
subject property and the duration of auto service operations, ECS has identified this listing as a
REC for the subject property.
• Tarheel Custom Cycles, 1304 South Tryon Street - This facility is approximately 130 feet north and
in a presumed downgradient hydrogeological position from the subject property. According to
the EDR report, this facility operated as a Motorcycle Dealer and Repair in 1979, 1982, 1983, 1985,
1986 ,1987, 1988, 1989, 1990, 1991, 1995, 1993, 1994, 1995, 1996, 1997, 1998, 1999, and 2000.
Based on the proximity to the subject property and the duration of auto service operations, ECS
has identified this listing as a REC for the subject property.
• Baldwin Algie, 1235 South Tryon Street - This facility is approximately 240 feet northeast and in a
presumed downgradient hydrogeological position from the subject property. According to the
EDR report, this facility operated as a service station and gasoline and oil service station in 1937,
1944, 1953, 1993, 1994, 1995, 1996, 1997, 1998, and 1999. Based on the proximity to the subject
Report of Environmental Assessment Services, Revision 1.0
1320/1328 South Tryon Street Property
1320 and 1328 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:17700-A
December 13, 2023

2
property and the duration of auto service operations, ECS has identified this listing as a REC for
the subject property.
• The subject property was utilized as a boat storage, sales, and repair facility and included onsite
painting (1962 Sanborn Map) from at least the 1960's through the late 1970's. Due to the potential
for a release, the former onsite boat repair facility is considered a REC.
• The south adjoining properties were utilized as used car sales facilities throughout the 1960s.
Onsite activities have the potential to have included car repair activities. The former south
adjoining used automotive sales facilities are considered a REC.
• The northwest adjoining property was utilized as a printing facility in the 1960s. The former
northwest adjoining printing facility is considered a REC.

In an effort to determine if the subject property has been adversely affected by the identified RECs, ECS
was requested to conduct environmental assessment services at the site. Our understanding of the
project is based on information included in the above referenced Phase I ESA report.

2.0 SCOPE OF SERVICES

The assessment included the collection and laboratory analysis of soil, groundwater, and soil gas samples.
Drilling activities were conducted using a Geoprobe® Direct Push Technology (DPT) drill rig. The drilling
subcontractor used for this assessment was Environmental Drilling and Probing Services, LLC (EDPS).
Drilling and sampling activities were between October 6 and 7, 2022.

2.1 Utility Locate

Prior to commencing with field activities, ECS contacted North Carolina One-Call to locate/mark public
utilities at the site. Required separation distances between subsurface activities and marked utilities
(typically 30-inches) were maintained during the field activities. In addition, ECS contracted with Priority
Underground Locating to evaluate the boring areas of underground private utilities.

2.2 Soil Boring Activities

Four soil borings (SB-1 through SB-4) were advanced at the site by the DPT drill rig. The locations of the
soil borings are indicated on Figure 2.

The soil borings were advanced by hydraulically driving a five-foot long, 1.5-inch diameter soil sampling
probe into the soil to depths of approximately 15 feet below the ground surface (bgs). The soil sampling
probe was lined with a dedicated disposable clear liner for each sampling interval. After the soil sampling
probe was driven, the liner filled with soil was removed from the probe and cut open to expose the soil.
Soils were collected continuously from the ground surface to the termination depth at each of the soil
boring locations. ECS visually classified the soil collected from each boring and screened the soils for
evidence of staining, odors, as well as relative levels of volatile organic vapors using a photoionization
detector (PID). Boring logs for each soil boring are included in Appendix A.

Report of Environmental Assessment Services, Revision 1.0
1320/1328 South Tryon Street Property
1320 and 1328 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:17700-A
December 13, 2023

3
2.3 Soil Sample Collection

The soil samples from soil borings SS-1 through SS-4 were collected by a sampler from the liner retrieved
from the soil sample probe and placed directly into laboratory provided containers. Based upon the field
screening results, the grab soil samples selected from soil borings SS-3 and SS-4 were collected from the
five to 10 feet bgs interval, and the grab soil samples selected from soil borings SS-1 and SS-2 were
collected from the 10 to 15 feet bgs intervals.

The soil sample containers were labeled with ECS project number, sample identification, sample date and
time, and requested analytical analysis. The containers were placed into a cooler with ice to maintain the
samples at approximately four degrees Celsius. The soil samples were submitted to Pace Analytical
Services, LLC (Pace), a North Carolina certified laboratory located in Huntersville, North Carolina, for
analysis for volatile organic compounds (VOCs) by EPA Method 8260, semi-volatile organic compounds
(SVOCs) by EPA Method 8270, RCRA Metals by EPA Methods 6010 and 7470, and hexavalent chromium
by EPA Method 7199. ECS maintained chain-of-custody (COC) procedures throughout the sample
collection and transportation process. A copy of the COC is included in Appendix B.

2.4 Temporary Monitoring Well Installation

ECS observed the advancement of eight borings (GW-1 through GW-8) for the installation of temporary
monitoring wells. The borings were advanced to depths of approximately 35 feet bgs. The locations of
groundwater samples are shown on Figure 2.

The temporary monitoring wells were constructed of approximately 10 feet of one-inch Schedule 40 PVC
slotted screen and sufficient one-inch Schedule 40 PVC casing to bring the temporary monitoring well to
the approximate ground surface. Filter sand was placed in the boring from the base of the boring to
approximately two feet above the screen and approximately two feet of bentonite seal was placed above
the sand filter pack. Boring logs including well construction details are included in Appendix A.

2.5 Groundwater Sample Collection

The groundwater samples were collected using a peristaltic pump and dedicated tubing. The groundwater
sample containers were labeled with ECS project number, sample identification, sample date and time,
and requested analytical analysis. The containers were placed into a cooler with ice to maintain the
samples at approximately four degrees Celsius. The groundwater samples were submitted to Pace for
analysis for VOCs by EPA Method 8260, SVOCs by EPA Method 8270, Total and Dissolved RCRA Metals by
EPA Methods 6010 and 7470, and hexavalent chromium by EPA Method 7199. ECS maintained chain-of-
custody (COC) procedures throughout the sample collection and transportation process. A copy of the
COC is included in Appendix B.

Following the completion of the groundwater sampling activities, the groundwater sample points were
abandoned by the North Carolina certified driller. Copies of the construction and abandonment records
are included in Appendix A.

Report of Environmental Assessment Services, Revision 1.0
1320/1328 South Tryon Street Property
1320 and 1328 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:17700-A
December 13, 2023

4
2.6 Soil Gas Boring and Sample Collection Activities
ECS observed the installation of five soil gas points (SG-1 through SG-5) at the locations shown on Figure
2. The soil gas sample points were constructed by advancing a boring to a depth of five feet bgs using the
DPT type drill rig. A vapor implant consisting of a porous air filter connected to a length of Nylaflow tubing
was positioned in near the base of each boring. The annular space around, and approximately 6 inches
above, the porous air filter was backfilled with clean filter sand and bentonite was placed in the remaining
annular space. Distilled water was poured into the bentonite and allowed to hydrate for at least 30
minutes before sampling was performed. Boring logs, including sampling point construction details, are
included in Appendix A.

Prior to collecting the soil gas samples, a sample train consisting of non-reactive tubing and microvalves
as connected to the Nylaflow tubing at each sample point and to a Summa canister. The sample train was
used to purge the sample lines and direct flow to the Summa canister being used to collect the sample at
each point. A shut-in test was performed on the sample train at each sample point to confirm that leaks
were not present in the sampling train. A micro-valve at the connection between the sampling train and
the Nylaflow tubing was closed, and a vacuum was applied to the sampling train using a disposable
syringe. The vacuum gauge on the Summa canister was monitored for declining vacuum indicative of a
leak.

Following the sample train construction and prior to collecting the soil gas samples, a helium shroud leak
test was performed at each of the sample points to confirm the integrity of the subsurface bentonite seal.
The shroud was placed and sealed over the sampling point. The vapor implant sample tubing and tracer
gas tubing was routed through small diameter holes in the wall of the shroud. The cylinder was flooded
with helium from a compressed gas tank through tracer gas tubing routed through the shroud wall. The
helium gas concentration inside the cylinder was measured with a helium gas detector. After the helium
gas concentration inside the canister reached a minimum of 20 percent, a soil gas sample was extracted
and measured with the helium detector. No leaks were noted during leak testing in any of the sample
points.

Following successful shut-in and helium shroud tests, ECS collected a soil gas sample from each sample
point. ECS collected the soil gas samples in a 1 liter-Summa canisters from Con-test, a commercial
laboratory that follows National Environmental Laboratory Accreditation Conference (NELAC) standards.
Each canister was pre-cleaned and pre-evacuated so that it is under negative pressure (i.e., under
vacuum). The canisters were individually certified by the laboratory. Each Summa canister was outfitted
with a flow regulator set to 200 milliliters per minute and a vacuum gauge. ECS opened the valve on the
Summa canister and soil gas flowed into the canister. ECS noted the time the valve was opened and the
initial vacuum. When the vacuum decreased to approximately 5 inches of mercury, ECS shut the valve and
recorded the time and final vacuum pressure.

Following sample collection, the canisters were labeled and shipped to Pace to be analyzed for VOCs using
EPA Method TO-15. ECS followed chain-of-custody procedures throughout the sample collection and
transportation process. A copy of the chain-of-custody form is included in Appendix B.

Report of Environmental Assessment Services, Revision 1.0
1320/1328 South Tryon Street Property
1320 and 1328 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:17700-A
December 13, 2023

5
3.0 RESULTS

3.1 Soil Samples Analytical Results

Review of the laboratory analytical results for the soil samples collected indicated methylene chloride in
the SS-2 and SS-4 soil samples at concentrations greater than its Protection of Groundwater Preliminary
Soil Remediation Goal (PSRG), but less than its Residential and Industrial/Commercial PSRGs. In addition,
one or more VOCs were detected in each soil sample collected at concentrations greater than the
laboratory method detection limit, but less than their respective PSRGs.

Hexavalent chromium was detected in each of the soil samples collected at concentrations greater than
its Residential PSRG, but less than its Protection of Groundwater and Industrial/Commercial PSRGs. Based
on the concentrations of total chromium and hexavalent chromium detected in each soil sample collected,
the concentrations of trivalent chromium in each soil sample collected were below its PSRGs. Additional
metals were detected in each soil sample collected at concentrations greater than the laboratory method
detection limits, but less than their respective PSRGs.

The soil samples analytical results are summarized in Table 1. A copy of the laboratory analytical report
is included in Appendix B.

3.2 Groundwater Samples Analytical Results

Review of the laboratory analytical results for the groundwater samples collected indicated
concentrations of total metals in each sample collected at concentrations greater than the laboratory
method reporting limit, including barium in the GW-2 and GW-3 groundwater samples, total chromium in
the GW-2, GW-3, GW-4, and GW-8 groundwater samples, and lead in the GW-1, GW-2, GW-3, GW-4, and
GW-8 groundwater samples at concentrations greater than their respective North Carolina 2L
Groundwater Quality Standards (NC2LGWQS). However, only concentrations of dissolved barium were
greater than the laboratory method reporting limits, but less than its NC2LGWQS, in each of the
groundwater samples. Additional dissolved metals were not detected at concentrations greater than the
laboratory method reporting limits in any of the groundwater samples collected.

VOCs and SVOCs were not detected in any of the groundwater samples collected at concentrations greater
than the laboratory method reporting limits. The groundwater samples analytical results are summarized
in Table 2. A copy of the laboratory analytical report is included in Appendix B.

3.3 Soil Gas Samples Analytical Results

Review of the laboratory analytical results for the soil gas samples collected indicated several VOCs at
concentrations greater than the laboratory method detection limits in each of the samples collected, with
the concentrations of benzene and 1,3-butadiene detected in each of the soil gas samples collected and
naphthalene in the SG-1 soil gas sample greater than their respective Residential Vapor Intrusion
Screening Levels (VISLs), but less than their respective Non-Residential VISLs. The detections of 1,3-
butadiene may be related to the fact that the soil gas sample points were only allowed to stabilize for
approximately 30 minutes prior to sample collection.
Report of Environmental Assessment Services, Revision 1.0
1320/1328 South Tryon Street Property
1320 and 1328 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:17700-A
December 13, 2023

6

In light of the soil gas sample results, ECS input the laboratory analytical results of the highest
concentration of each compound detected in soil gas samples collected into the NCDEQ Risk Calculator.
Based on the results of the NCDEQ Risk Calculator, the concentrations in the soil gas samples did not
exceed the risk thresholds for Resident or Non-Residential Worker classifications. Output from the result
of the NCDEQ Risk Calculator are presented in Appendix C.

The soil gas analytical results are summarized on Table 3. A copy of the laboratory analytical report is
included in Appendix B.

4.0 CONCLUSIONS

Based on the results of the environmental assessment, ECS concludes the following:

• Review of the laboratory analytical results for the soil samples collected indicated methylene
chloride in the SS-2 and SS-4 soil samples at concentrations greater than its Protection of
Groundwater PSRG, but less than its Residential and Industrial/Commercial PSRGs. However,
methylene chloride is a common laboratory contaminant and was not detected at concentrations
greater than the laboratory method reporting limit in any of the groundwater samples collected.
Therefore, the detections of methylene chloride in the SS-2 and SS-4 soil samples is not considered
to indicate a release.
• Hexavalent chromium was detected in each of the soil samples collected at concentrations
greater than its Residential PSRG, but less than its Protection of Groundwater and
Industrial/Commercial PSRGs. Based on the concentrations of total chromium and hexavalent
chromium detected in each soil sample collected, the concentrations of trivalent chromium in
each soil sample collected were below its PSRGs.
• Results of the total RCRA Metals analysis of the groundwater samples collected indicated barium,
total chromium, and lead in one or more groundwater samples collected at concentrations
greater than their respective NC2LGWQS; however, results of the dissolved metals analysis for
these same metals did not indicate exceedances of their respective NC2LGWQS. Therefore, the
detections of barium, total chromium, and lead in the total RCRA Metals analysis are believed to
be a result of the turbidity of the groundwater samples collected and not an indication of release.
• Several VOCs were detected in the soil gas samples at concentrations greater than the laboratory
method detection limits in each of the samples collected, with the concentrations of 1,3-
butadiene detected in each of the samples collected greater than its Residential VISLs, but less
than its Non-Residential VISLs. The additional compounds detected were not present at
concentrations greater than their respective VISLs. Detections of 1,3-butadiene are often a result
of the installation process of the soil gas sampling point and not indicative of a release.
• ECS input the laboratory analytical results of the soil gas samples into the NCDEQ Risk Calculator.
The results of the NCDEQ Risk Calculator indicated the concentrations detected in the soil gas
samples did not exceed the risk thresholds for Resident or Non-Residential Worker classifications.

Report of Environmental Assessment Services, Revision 1.0
1320/1328 South Tryon Street Property
1320 and 1328 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:17700-A
December 13, 2023

7
5.0 RECOMMENDATIONS

Based on the results of the environmental assessment, ECS recommends the following:

• ECS recommends that a copy of this report be maintained for your records.
• ECS does not recommend any additional sampling at this time.
• ECS understands that Catalyst Capital Partners wishes to enter the property into the NCDEQ
Brownfields Program. While this assessment did not reveal evidence of a release, due to the
history of the area in which the property is located and the presence of Brownfields sites in the
area, it is possible that contaminants may migrate onto the property in the future; therefore, it is
expected that this site would qualify for entry into the Brownfields Program.

6.0 QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this environmental assessment are consistent with those
normally employed in environmental soil and groundwater assessment projects of this type. Our
evaluation of site conditions has been based on our understanding of the site project information
determined during previous environmental assessments and the data obtained during our field activities.

This report was prepared for the express use of Catalyst Capital Partners. Use of this report by other
individuals or companies implies their acceptance of the General Conditions of Service of the original
contract.

FIGURES

SOURCE:
USGS TOPOGRAPHIC 7.5’ QUADRANGLE
CHARLOTTE EAST NC
SCALE:
AS SHOWN
FIGURE 1
USGS TOPOGRAPHIC MAP
1320/1328 SOUTH TRYON STREET SITE
1320 and 1328 SOUTH TRYON STREET
CHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:17700-A
SITE
Carroll Aligning
Service Company
(REC)
Tarheel Custom
Cycles (REC)
Baldwin Algie
(REC)
Former Printing
Facility (REC)
American Dry-
Cleaning Company
and Wright Cleaning
Company, Inc. (REC)
GW-6
GW-5
GW-4 SS-4
SS-3
SS-2
SS-1
SG-5
SG-4SG-3
SG-2
SG-1
FIGURE 2SAMPLE LOCATION MAP
1320/1328 SOUTH TRYON STREET SITE1320 and 1328 SOUTH TRYON STREETCHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:17700-A
SOURCE:
CHARLOTTE MECKLNEBURG COUNTY GIS WEBSITE
ACCESSED JULY 18, 2022
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
APPROXIMATE SOIL SAMPLE LOCATION
APPROXIMATE GROUNDWATER BORING LOCATION
APPROXIMATE SOIL GAS SAMPLE LOCATION
GW-7
GW-8
GW-1GW-2
GW-3

TABLES

Table 1
Summary of Soil Samples Analytical Results
1320/1328 South Tryon Street Property
1320 and 1328 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No.: 49:17700-A
SS-1 SS-2 SS-3 SS-4
10/06/22 10/06/22 10/06/22 10/06/22
10 - 15 10 - 15 5 - 10 5 - 10
Chlorobenzene <0.0020 <0.0016 0.0061 J 0.0067 J 0.68 58 280
Chloromethane <0.0086 0.0099 J 0.010 J 0.011 J 0.015 23 99
Ethylbenzene <0.0048 <0.0038 0.0068 J 0.0084 J 13 6.1 27
Methylene Chloride <0.028 0.041 <0.023 0.083 0.025 58 650
Toluene <0.0029 <0.0023 0.0058 J <0.0029 8.3 990 9,700
Trichloroethene <0.0026 <0.0021 <0.0022 <0.0027 0.021 0.87 4.0
Total Xylenes 0.0057 J <0.0046 0.021 0.023 9.9 120 530
SVOCs by EPA Method 8270All Compounds BDL BDL BDL BDL Various Various Various
Arsenic <3.0 <2.7 <2.6 <2.8 5.8 0.68 3.0
Barium 52.8 3.7 37.5 11.2 580 3,100 47,000
Cadmium <0.42 <0.37 <0.37 <0.38 3.0 1.4 20
Total Chromium 36.5 12.2 17.3 23.0 NE NE NE
Hexavalent Chromium 1.54 0.435 J 0.437 J 0.690 J 3.8 0.31 6.5
Trivalent Chromium 35.0 11.8 16.9 22.3 360,000 23,000 350,000
Lead 19.2 10.6 20.0 13.8 250 400 800
Mercury 0.081 J 0.014 J <0.013 0.11 J 4.7 70 9.7
Selenium <30.5 <27.2 <26.7 <28.0 2.1 78 1,200
Silver <0.58 <0.51 <0.50 <0.53 3.4 78 1,200
Notes:
All results presented in milligrams per kilogram (mg/kg)J = Estimated concentration detected between laboratory method reporting limit and method detection limit
Compounds not shown were not detected NE = Not Established
ft bgs = feet below ground surface VALUE = concentration greater than the laboratory method detection limit
VOCs = Volatile Organic Compounds VALUE = concentration greater than the Protection of Groundwater PSRG
SVOCs = Semi-volatile Organic Compounds VALUE = concentration greater than the Residential PSRG
PSRG = Preliminary Soil Remediation Goal (July 2023)
Value to right of “<” symbol are laboratory method detection limits. Laboratory method reporting limits may be found in the laboraotry report.
Sample Date
Sample Depth
Total RCRA Metals by EPA Method 6460/7471/7199VOCs by EPA Method 8260Industrial/
Commercial
PSRG
Residential
PSRG
Protection of
Groundwater
PSRG
Sample ID
Table 2
Summary of Groundwater Samples Analytical Results
1320/1328 South Tryon Street Property
1320 and 1328 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No.: 49:17700-A
GW-1 GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8
10/07/22 10/07/22 10/07/22 10/07/22 10/07/22 10/07/22 10/07/22 10/07/22
VOCs by EPA
Method 8260 All Compounds BDL BDL BDL BDL BDL BDL BDL BDL Various Various Various
SVOCs by EPA
Method 8270 All Compounds BDL BDL BDL BDL BDL BDL BDL BDL Various Various Various
Arsenic <26.2 <26.2 <26.2 <26.2 <26.2 <26.2 <26.2 <26.2 10 NV NV
Barium 123 1,480 784 271 88.7 80.5 143 499 700 NV NV
Cadmium <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 2 NV NV
Total Chromium 3.7 J 42.3 17.9 11.5 <3.6 <3.6 <3.6 10.6 10 NV NV
Hexavalent Chromium 0.776 0.165 J <0.150 <0.150 <0.150 <0.150 <0.150 <0.150 NE NV NV
Trivalent Chromium 2.9 42.1 17.9 11.5 <3.6 <3.6 <3.6 10.6 NE NE NE
Lead 23.4 94.5 61.8 199 <19.0 <19.0 <19.0 37.4 15 NV NV
Mercury <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 1 0.18 0.75
Selenium <31.1 <31.1 <31.1 <31.1 <31.1 <31.1 <31.1 <31.1 20 NV NV
Silver <4.6 <4.6 <4.6 <4.6 <4.6 <4.6 <4.6 <4.6 20 NE NE
Arsenic <26.2 <26.2 <26.2 <26.2 <26.2 <26.2 <26.2 <26.2 10 NV NV
Barium 28.6 58.4 45.9 41.2 52.2 59.8 66.2 62.7 700 NV NV
Cadmium <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 2 NV NV
Total Chromium <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 10 NV NV
Lead <19.0 <19.0 <19.0 <19.0 <19.0 <19.0 <19.0 <19.0 15 NV NV
Mercury <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 1 0.18 0.75
Selenium <31.1 <31.1 <31.1 <31.1 <31.1 <31.1 <31.1 <31.1 20 NV NV
Silver <4.6 <4.6 <4.6 <4.6 <4.6 <4.6 <4.6 <4.6 20 NE NE
Notes:
All results presented in micrograms per liter (µg/L)NV = Not volatile
Compounds not shown were not detected NE = Not established
VOCs = Volatile Organic Compounds BDL = Below detection limit
SVOCs = Semi-volatile Organic Compounds Value to right of “<” symbol are laboratory method detection limits. Laboratory method reporting limits may be found in the laboraotry report.
NC2LGWQS = North Carolina 2L Groundwater Quality Standards (April 2022)VALUE = concentration greater than the laboratory method detection limit
VISL = Groundwater Vapor Instrusion Screening Level (July 2023)VALUE = concentration greater than the NC2LGWQSDissolved RCRA Metals by EPA Method 6010, 7471, & 7199Total RCRA Metals by EPA Method 6010, 7471, & 7199Non-Residential
VISLResidenital VISLNC2LGWQSSample ID
Sample Date
Table 3
Summary of Soil Gas Samples Analytical Results
1320/1328 South Tryon Street Property
1320 and 1328 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No.: 49:17700-A
Sample ID SG-1 SG-2 SG-3 SG-4 SG-5
Sample Date 10/06/22 10/06/22 10/06/22 10/06/22 10/06/22
Sample Probe Depth (ft bgs) 5 5 5 5 5
Benzene 28 15 20 44 28 12 160
Bromomethane <0.52 0.64 J <0.52 <0.52 <0.52 35 440
1,3-Butadiene 37 15 13 32 19 3.1 41
2-Butanone (MEK)26 8.6 J 24 24 J 26 35,000 440,000
Carbon Disulfide 79 16 110 55 11 4,900 61,000
Chloroethane <0.47 0.88 <0.47 <0.47 <0.47 NE NE
Chloroform <0.93 1.2 <0.93 <0.93 <0.93 4.1 53
Chloromethane 1.8 2.5 2.5 2.1 2.4 630 7,900
Cyclohexane 120 16 22 11 19 42,000 530,000
Dichlorodifluoromethane 2.8 2.7 2.5 2.7 2.3 700 8,800
Ethanol 35 26 23 26 21 NE NE
Ethylbenzene 5.7 0.96 4.3 6.2 8.4 37 490
4-Ethyltoluene 1.8 <0.60 1.4 1.2 5.2 NE NE
n-Heptane 38 5.7 610 27 27 2,800 35,000
n-Hexane 120 19 J 850 66 56 4,900 61,000
Isopropanol <3.4 35 4.9 J 5.0 J <3.4 1,400 18,000
Naphthalene 3.4 <0.79 <0.79 <0.79 <0.79 2.8 36
Propylene 1,400 570 750 660 920 21,000 260,000
Styrene 0.72 J 0.70 J 1.7 1.8 1.1 7,000 88,000
Toluene 47 12 25 43 45 35,000 440,000
Trichloroethene <0.72 <0.72 <0.72 <0.72 <0.72 14 180
Trichlorofluoromethane 1.4 J 1.8 J <1.3 <1.3 <1.3 NE NE
1,2,4-Trimethylbenzene 4.7 <0.43 2.9 1.9 8.1 420 5,300
1,3,5-Trimethylbenzene 2.5 <0.52 1.5 1.1 3.8 420 5,300
Vinyl Chloride <0.46 <0.46 <0.46 0.92 <0.46 5.6 280
Total Xylenes 27.0 4.4 17.3 18.3 52.0 700 8,800
Notes:
Concentrations presented in micrograms per cubic meter (µg/m3)NE = No Standard Established
Compounds not shown were not detected VALUE = concentration greater than the laboratory method detection limit
ft bgs = feet below ground surface VALUE = concentration greater than the Residential Vapor Instrusion Screening Level
VISL = Sub-slab and Exterior Vapor Instrusion Screening Level (July 2023)VALUE = concentration greater than the Non-Residential Vapor Instrusion Screening Level
Value to right of “<” symbol are laboratory method detection limits. Laboratory method reporting limits may be found in the laboraotry report.
J = Estimated concentration detected between laboratory method reporting limit and detection limitVolatile Organic Compounds by EPA Method TO-15Residential VISLs Non-Residential
VISLs
APPENDIX A
Boring Logs and Well Construction/Abadonment
Forms
Depth/
5
10
15
20
25
30
35
40
ElevaƟon
-5
-10
-15
-20
-25
-30
-35 PID ReadingSample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
ML
ML
Water
DescripƟon
Red/Brown Clayey Silt
Red/Brown Silt
Light Brown Silt
Water
Refusal encountered at 35.0 feet.END OF DRILLING AT 35.0 FT
WELL CONSTRUCTION
Pipe SƟckup: 1.8 Ō
PVC Riser
PVC Screen
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-1
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)23.68 Boring Started:Oct 06 2022
WL (CompleƟon)23.78 Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
Depth/
5
10
15
20
25
30
35
40
ElevaƟon
-5
-10
-15
-20
-25
-30
-35 PID ReadingSample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon DescripƟon
No Lithology Recorded
Refusal encountered at 35.0 feet.END OF DRILLING AT 35.0 FT
WELL CONSTRUCTION
Pipe SƟckup: 1.26 Ō
PVC Riser
PVC Screen
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-2
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)23.91 Boring Started:Oct 06 2022
WL (CompleƟon)23.99 Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
Depth/
5
10
15
20
25
30
35
40
ElevaƟon
-5
-10
-15
-20
-25
-30
-35 PID ReadingSample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon DescripƟon
No Lithology Recorded
Refusal encountered at 35.0 feet.END OF DRILLING AT 35.0 FT
WELL CONSTRUCTION
Pipe SƟckup: 1.47 Ō
PVC Riser
PVC Screen
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-3
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)24.53 Boring Started:Oct 06 2022
WL (CompleƟon)25.03 Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
Depth/
5
10
15
20
25
30
35
40
ElevaƟon
-5
-10
-15
-20
-25
-30
-35 PID ReadingSample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon DescripƟon
No Lithology Recorded
Refusal encountered at 35.0 feet.END OF DRILLING AT 35.0 FT
WELL CONSTRUCTION
Pipe SƟckup: 1.42 Ō
PVC Riser
PVC Screen
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-4
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)25.68 Boring Started:Oct 06 2022
WL (CompleƟon)25.74 Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
Depth/
5
10
15
20
25
30
35
40
ElevaƟon
-5
-10
-15
-20
-25
-30
-35 PID ReadingSample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon DescripƟon
No Lithology Recorded
Refusal encountered at 35.0 feet.END OF DRILLING AT 35.0 FT
WELL CONSTRUCTION
Pipe SƟckup: 3 Ō
PVC Riser
PVC Screen
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-5
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)25.81 Boring Started:Oct 06 2022
WL (CompleƟon)25.89 Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
Depth/
5
10
15
20
25
30
35
40
ElevaƟon
-5
-10
-15
-20
-25
-30
-35 PID ReadingSample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon DescripƟon
No Lithology Recorded
Refusal encountered at 35.0 feet.END OF DRILLING AT 35.0 FT
WELL CONSTRUCTION
Pipe SƟckup: 0.6 Ō
PVC Riser
PVC Screen
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-6
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)25.38 Boring Started:Oct 06 2022
WL (CompleƟon)24.22 Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
Depth/
5
10
15
20
25
30
35
40
ElevaƟon
-5
-10
-15
-20
-25
-30
-35 PID ReadingSample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon DescripƟon
No Lithology Recorded
Refusal encountered at 35.0 feet.END OF DRILLING AT 35.0 FT
WELL CONSTRUCTION
Pipe SƟckup: 1.24 Ō
PVC Riser
PVC Screen
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-7
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)24.32 Boring Started:Oct 06 2022
WL (CompleƟon)23.87 Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
Depth/
5
10
15
20
25
30
35
40
ElevaƟon
-5
-10
-15
-20
-25
-30
-35 PID ReadingSample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon DescripƟon
No Lithology Recorded
Refusal encountered at 35.0 feet.END OF DRILLING AT 35.0 FT
WELL CONSTRUCTION
Pipe SƟckup: 1.2 Ō
PVC Riser
PVC Screen
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-8
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)24.66 Boring Started:Oct 06 2022
WL (CompleƟon)24.40 Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25
-30 PID Reading7.2
7.0
7.3 Sample NumberSS-1 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
ML
ML
DescripƟon
Brown Clayey Silt
Red Brown Silt
Brown Silt
Refusal encountered at 15.0 feet.END OF DRILLING AT 15.0 FT
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:SS-1
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
WL (First Encountered)Boring Started:Oct 06 2022
WL (CompleƟon)Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25
-30 PID Reading6.9
7.1
7.0 Sample NumberSS-2 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
ML
ML
DescripƟon
Red/Brown Clayey Silt
Red/Brown Silt
Brown Silt
Refusal encountered at 15.0 feet.END OF DRILLING AT 15.0 FT
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:SS-2
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
WL (First Encountered)Boring Started:Oct 06 2022
WL (CompleƟon)Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25
-30 PID Reading6.9
7.3
6.9 Sample NumberSS-3 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML
ML
DescripƟon
Red/Brown Silt
Brown Silt
Refusal encountered at 15.0 feet.END OF DRILLING AT 15.0 FT
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:SS-3
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
WL (First Encountered)Boring Started:Oct 06 2022
WL (CompleƟon)Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25
-30 PID Reading6.7
8.2
7.1 Sample NumberSS-4 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
ML/CL
ML
DescripƟon
Red/Brown Clayey Silt
Red Clayey Silt
Brown Silt
Refusal encountered at 15.0 feet.END OF DRILLING AT 15.0 FT
Project Name:Two Vacant Parcels -CharloƩe
Environmental Assessment
Client:Catalyst Capital Partners
Site LocaƟon:1320/1328 South Tryon Street, CharloƩe, NC
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:SS-4
Project No.:17700-A
Driller:EDPS Drill Rig:GeoProbe
WL (First Encountered)Boring Started:Oct 06 2022
WL (CompleƟon)Boring Completed:Oct 06 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Seth Greene
Roger Smith
APPENDIX B
Laboratory Analytical Report
Chain-of-Custody
#=CL#
October 18, 2022
LIMS USE: FR - SCOTT YOUNG
LIMS OBJECT ID: 92630074
92630074
Project:
Pace Project No.:
RE:
Scott Young
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
S TRYON 17700-A
Dear Scott Young:
Enclosed are the analytical results for sample(s) received by the laboratory on October 07, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sara Poulson
[e-mail]
Project Manager
[phone]
Enclosures
cc:ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 55
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 55
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Lab ID Sample ID Matrix Date Collected Date Received
92630074001 SS-1 Solid 10/06/22 12:10 10/07/22 10:30
92630074002 SS-2 Solid 10/06/22 12:20 10/07/22 10:30
92630074003 SS-3 Solid 10/06/22 12:30 10/07/22 10:30
92630074004 SS-4 Solid 10/06/22 12:40 10/07/22 10:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 55
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92630074001 SS-1 EPA 6010D 7 PASI-GAKH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANARD
92630074002 SS-2 EPA 6010D 7 PASI-GAKH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANARD
92630074003 SS-3 EPA 6010D 7 PASI-GAKH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANARD
92630074004 SS-4 EPA 6010D 7 PASI-GAKH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANARD
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 55
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92630074001 SS-1
Barium 52.8 mg/kg 10/13/22 22:471.4EPA 6010D
Chromium 36.5 mg/kg 10/13/22 22:471.4EPA 6010D
Lead 19.2 mg/kg 10/13/22 22:473.5EPA 6010D
Mercury 0.081J mg/kg 10/14/22 12:30 M10.37EPA 7471B
o-Xylene 0.0057J mg/kg 10/14/22 13:560.010EPA 8260D
Percent Moisture 34.4 %10/10/22 16:49 N20.10SW-846
Total Solids 65.3 %10/14/22 17:09SM 2540G
Chromium, Hexavalent 1.54 mg/kg 10/17/22 12:061.53EPA 7199
92630074002 SS-2
Barium 3.7 mg/kg 10/13/22 23:011.3EPA 6010D
Chromium 12.2 mg/kg 10/13/22 23:011.3EPA 6010D
Lead 10.6 mg/kg 10/13/22 23:013.1EPA 6010D
Mercury 0.014J mg/kg 10/14/22 12:420.31EPA 7471B
Chloromethane 0.0099J mg/kg 10/13/22 21:560.016EPA 8260D
Methylene Chloride 0.041 mg/kg 10/13/22 21:56 C9,D60.032EPA 8260D
Percent Moisture 23.5 %10/10/22 16:49 N20.10SW-846
Total Solids 62.0 %10/14/22 17:09SM 2540G
Chromium, Hexavalent 0.435J mg/kg 10/17/22 12:11 J1.61EPA 7199
92630074003 SS-3
Barium 37.5 mg/kg 10/13/22 23:061.2EPA 6010D
Chromium 17.3 mg/kg 10/13/22 23:061.2EPA 6010D
Lead 20.0 mg/kg 10/13/22 23:063.1EPA 6010D
Chlorobenzene 0.0061J mg/kg 10/13/22 22:140.0084EPA 8260D
Chloromethane 0.010J mg/kg 10/13/22 22:140.017EPA 8260D
Ethylbenzene 0.0068J mg/kg 10/13/22 22:140.0084EPA 8260D
Toluene 0.0058J mg/kg 10/13/22 22:140.0084EPA 8260D
Xylene (Total)0.021 mg/kg 10/13/22 22:140.017EPA 8260D
m&p-Xylene 0.011J mg/kg 10/13/22 22:140.017EPA 8260D
o-Xylene 0.0094 mg/kg 10/13/22 22:140.0084EPA 8260D
Percent Moisture 24.9 %10/10/22 16:49 N20.10SW-846
Total Solids 61.5 %10/14/22 17:09SM 2540G
Chromium, Hexavalent 0.437J mg/kg 10/17/22 12:17 J1.62EPA 7199
92630074004 SS-4
Barium 11.2 mg/kg 10/13/22 23:101.3EPA 6010D
Chromium 23.0 mg/kg 10/13/22 23:101.3EPA 6010D
Lead 13.8 mg/kg 10/13/22 23:103.2EPA 6010D
Mercury 0.11J mg/kg 10/14/22 12:530.32EPA 7471B
Chlorobenzene 0.0067J mg/kg 10/13/22 22:330.010EPA 8260D
Chloromethane 0.011J mg/kg 10/13/22 22:330.021EPA 8260D
Ethylbenzene 0.0084J mg/kg 10/13/22 22:330.010EPA 8260D
Methylene Chloride 0.083 mg/kg 10/13/22 22:33 C90.041EPA 8260D
Xylene (Total)0.023 mg/kg 10/13/22 22:330.021EPA 8260D
m&p-Xylene 0.012J mg/kg 10/13/22 22:330.021EPA 8260D
o-Xylene 0.011 mg/kg 10/13/22 22:330.010EPA 8260D
Percent Moisture 25.7 %10/10/22 16:50 N20.10SW-846
Total Solids 70.2 %10/14/22 17:09SM 2540G
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 55
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92630074004 SS-4
Chromium, Hexavalent 0.690J mg/kg 10/17/22 12:22 J1.42EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-1 Lab ID:92630074001 Collected:10/06/22 12:10 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 10/13/22 22:47 7440-38-210/13/22 09:244.2 3.0 1
Barium 52.8 mg/kg 10/13/22 22:47 7440-39-310/13/22 09:241.4 0.58 1
Cadmium ND mg/kg 10/13/22 22:47 7440-43-910/13/22 09:241.4 0.42 1
Chromium 36.5 mg/kg 10/13/22 22:47 7440-47-310/13/22 09:241.4 1.3 1
Lead 19.2 mg/kg 10/13/22 22:47 7439-92-110/13/22 09:243.5 2.2 1
Selenium ND mg/kg 10/14/22 14:50 7782-49-2 D310/13/22 09:2435.3 30.5 5
Silver ND mg/kg 10/13/22 22:47 7440-22-410/13/22 09:241.4 0.58 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.081J mg/kg 10/14/22 12:30 7439-97-6 M110/14/22 08:000.37 0.016 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/14/22 10:44 83-32-910/12/22 17:090.50 0.18 1
Acenaphthylene ND mg/kg 10/14/22 10:44 208-96-810/12/22 17:090.50 0.18 1
Aniline ND mg/kg 10/14/22 10:44 62-53-310/12/22 17:090.50 0.20 1
Anthracene ND mg/kg 10/14/22 10:44 120-12-710/12/22 17:090.50 0.17 1
Benzo(a)anthracene ND mg/kg 10/14/22 10:44 56-55-310/12/22 17:090.50 0.17 1
Benzo(a)pyrene ND mg/kg 10/14/22 10:44 50-32-810/12/22 17:090.50 0.17 1
Benzo(b)fluoranthene ND mg/kg 10/14/22 10:44 205-99-210/12/22 17:090.50 0.17 1
Benzo(g,h,i)perylene ND mg/kg 10/14/22 10:44 191-24-210/12/22 17:090.50 0.20 1
Benzo(k)fluoranthene ND mg/kg 10/14/22 10:44 207-08-910/12/22 17:090.50 0.18 1
Benzoic Acid ND mg/kg 10/14/22 10:44 65-85-010/12/22 17:092.5 1.1 1
Benzyl alcohol ND mg/kg 10/14/22 10:44 100-51-610/12/22 17:091.0 0.38 1
4-Bromophenylphenyl ether ND mg/kg 10/14/22 10:44 101-55-310/12/22 17:090.50 0.19 1
Butylbenzylphthalate ND mg/kg 10/14/22 10:44 85-68-710/12/22 17:090.50 0.21 1
4-Chloro-3-methylphenol ND mg/kg 10/14/22 10:44 59-50-710/12/22 17:091.0 0.35 1
4-Chloroaniline ND mg/kg 10/14/22 10:44 106-47-810/12/22 17:091.0 0.40 1
bis(2-Chloroethoxy)methane ND mg/kg 10/14/22 10:44 111-91-110/12/22 17:090.50 0.21 1
bis(2-Chloroethyl) ether ND mg/kg 10/14/22 10:44 111-44-410/12/22 17:090.50 0.19 1
2-Chloronaphthalene ND mg/kg 10/14/22 10:44 91-58-710/12/22 17:090.50 0.20 1
2-Chlorophenol ND mg/kg 10/14/22 10:44 95-57-810/12/22 17:090.50 0.19 1
4-Chlorophenylphenyl ether ND mg/kg 10/14/22 10:44 7005-72-310/12/22 17:090.50 0.19 1
Chrysene ND mg/kg 10/14/22 10:44 218-01-910/12/22 17:090.50 0.18 1
Dibenz(a,h)anthracene ND mg/kg 10/14/22 10:44 53-70-310/12/22 17:090.50 0.19 1
Dibenzofuran ND mg/kg 10/14/22 10:44 132-64-910/12/22 17:090.50 0.18 1
1,2-Dichlorobenzene ND mg/kg 10/14/22 10:44 95-50-110/12/22 17:090.50 0.18 1
1,3-Dichlorobenzene ND mg/kg 10/14/22 10:44 541-73-110/12/22 17:090.50 0.18 1
1,4-Dichlorobenzene ND mg/kg 10/14/22 10:44 106-46-710/12/22 17:090.50 0.19 1
3,3'-Dichlorobenzidine ND mg/kg 10/14/22 10:44 91-94-110/12/22 17:091.0 0.34 1
2,4-Dichlorophenol ND mg/kg 10/14/22 10:44 120-83-210/12/22 17:090.50 0.20 1
Diethylphthalate ND mg/kg 10/14/22 10:44 84-66-210/12/22 17:090.50 0.19 1
2,4-Dimethylphenol ND mg/kg 10/14/22 10:44 105-67-910/12/22 17:090.50 0.21 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-1 Lab ID:92630074001 Collected:10/06/22 12:10 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 10/14/22 10:44 131-11-310/12/22 17:090.50 0.18 1
Di-n-butylphthalate ND mg/kg 10/14/22 10:44 84-74-210/12/22 17:090.50 0.17 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/14/22 10:44 534-52-110/12/22 17:091.0 0.47 1
2,4-Dinitrophenol ND mg/kg 10/14/22 10:44 51-28-510/12/22 17:092.5 1.6 1
2,4-Dinitrotoluene ND mg/kg 10/14/22 10:44 121-14-210/12/22 17:090.50 0.19 1
2,6-Dinitrotoluene ND mg/kg 10/14/22 10:44 606-20-210/12/22 17:090.50 0.19 1
Di-n-octylphthalate ND mg/kg 10/14/22 10:44 117-84-010/12/22 17:090.50 0.20 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/14/22 10:44 117-81-710/12/22 17:090.50 0.20 1
Fluoranthene ND mg/kg 10/14/22 10:44 206-44-010/12/22 17:090.50 0.17 1
Fluorene ND mg/kg 10/14/22 10:44 86-73-710/12/22 17:090.50 0.18 1
Hexachloro-1,3-butadiene ND mg/kg 10/14/22 10:44 87-68-3 v110/12/22 17:090.50 0.22 1
Hexachlorobenzene ND mg/kg 10/14/22 10:44 118-74-110/12/22 17:090.50 0.20 1
Hexachlorocyclopentadiene ND mg/kg 10/14/22 10:44 77-47-410/12/22 17:090.50 0.29 1
Hexachloroethane ND mg/kg 10/14/22 10:44 67-72-110/12/22 17:090.50 0.19 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/14/22 10:44 193-39-510/12/22 17:090.50 0.20 1
Isophorone ND mg/kg 10/14/22 10:44 78-59-110/12/22 17:090.50 0.22 1
1-Methylnaphthalene ND mg/kg 10/14/22 10:44 90-12-010/12/22 17:090.50 0.18 1
2-Methylnaphthalene ND mg/kg 10/14/22 10:44 91-57-610/12/22 17:090.50 0.20 1
2-Methylphenol(o-Cresol)ND mg/kg 10/14/22 10:44 95-48-710/12/22 17:090.50 0.21 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/14/22 10:44 15831-10-410/12/22 17:090.50 0.20 1
Naphthalene ND mg/kg 10/14/22 10:44 91-20-310/12/22 17:090.50 0.17 1
2-Nitroaniline ND mg/kg 10/14/22 10:44 88-74-410/12/22 17:092.5 0.41 1
3-Nitroaniline ND mg/kg 10/14/22 10:44 99-09-210/12/22 17:092.5 0.40 1
4-Nitroaniline ND mg/kg 10/14/22 10:44 100-01-610/12/22 17:091.0 0.38 1
Nitrobenzene ND mg/kg 10/14/22 10:44 98-95-310/12/22 17:090.50 0.23 1
2-Nitrophenol ND mg/kg 10/14/22 10:44 88-75-510/12/22 17:090.50 0.22 1
4-Nitrophenol ND mg/kg 10/14/22 10:44 100-02-710/12/22 17:092.5 0.98 1
N-Nitrosodimethylamine ND mg/kg 10/14/22 10:44 62-75-910/12/22 17:090.50 0.17 1
N-Nitroso-di-n-propylamine ND mg/kg 10/14/22 10:44 621-64-710/12/22 17:090.50 0.19 1
N-Nitrosodiphenylamine ND mg/kg 10/14/22 10:44 86-30-610/12/22 17:090.50 0.18 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 10/14/22 10:44 108-60-1 v210/12/22 17:090.50 0.24 1
Pentachlorophenol ND mg/kg 10/14/22 10:44 87-86-510/12/22 17:091.0 0.49 1
Phenanthrene ND mg/kg 10/14/22 10:44 85-01-810/12/22 17:090.50 0.17 1
Phenol ND mg/kg 10/14/22 10:44 108-95-210/12/22 17:090.50 0.22 1
Pyrene ND mg/kg 10/14/22 10:44 129-00-010/12/22 17:090.50 0.20 1
Pyridine ND mg/kg 10/14/22 10:44 110-86-110/12/22 17:090.50 0.16 1
1,2,4-Trichlorobenzene ND mg/kg 10/14/22 10:44 120-82-110/12/22 17:090.50 0.20 1
2,4,5-Trichlorophenol ND mg/kg 10/14/22 10:44 95-95-410/12/22 17:090.50 0.23 1
2,4,6-Trichlorophenol ND mg/kg 10/14/22 10:44 88-06-210/12/22 17:090.50 0.21 1
Surrogates
Nitrobenzene-d5 (S)81 %10/14/22 10:44 4165-60-010/12/22 17:0910-130 1
2-Fluorobiphenyl (S)66 %10/14/22 10:44 321-60-810/12/22 17:0910-130 1
Terphenyl-d14 (S)57 %10/14/22 10:44 1718-51-010/12/22 17:0910-130 1
Phenol-d6 (S)65 %10/14/22 10:44 13127-88-310/12/22 17:0910-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-1 Lab ID:92630074001 Collected:10/06/22 12:10 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)66 %10/14/22 10:44 367-12-410/12/22 17:0910-130 1
2,4,6-Tribromophenol (S)81 %10/14/22 10:44 118-79-610/12/22 17:0910-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/14/22 13:56 67-64-110/14/22 13:250.20 0.065 1
Benzene ND mg/kg 10/14/22 13:56 71-43-210/14/22 13:250.010 0.0041 1
Bromobenzene ND mg/kg 10/14/22 13:56 108-86-110/14/22 13:250.010 0.0033 1
Bromochloromethane ND mg/kg 10/14/22 13:56 74-97-510/14/22 13:250.010 0.0030 1
Bromodichloromethane ND mg/kg 10/14/22 13:56 75-27-410/14/22 13:250.010 0.0039 1
Bromoform ND mg/kg 10/14/22 13:56 75-25-210/14/22 13:250.010 0.0036 1
Bromomethane ND mg/kg 10/14/22 13:56 74-83-9 IK,v110/14/22 13:250.020 0.016 1
2-Butanone (MEK)ND mg/kg 10/14/22 13:56 78-93-310/14/22 13:250.20 0.049 1
n-Butylbenzene ND mg/kg 10/14/22 13:56 104-51-810/14/22 13:250.010 0.0048 1
sec-Butylbenzene ND mg/kg 10/14/22 13:56 135-98-810/14/22 13:250.010 0.0045 1
tert-Butylbenzene ND mg/kg 10/14/22 13:56 98-06-610/14/22 13:250.010 0.0036 1
Carbon tetrachloride ND mg/kg 10/14/22 13:56 56-23-510/14/22 13:250.010 0.0038 1
Chlorobenzene ND mg/kg 10/14/22 13:56 108-90-710/14/22 13:250.010 0.0020 1
Chloroethane ND mg/kg 10/14/22 13:56 75-00-310/14/22 13:250.020 0.0079 1
Chloroform ND mg/kg 10/14/22 13:56 67-66-310/14/22 13:250.010 0.0062 1
Chloromethane ND mg/kg 10/14/22 13:56 74-87-310/14/22 13:250.020 0.0086 1
2-Chlorotoluene ND mg/kg 10/14/22 13:56 95-49-810/14/22 13:250.010 0.0036 1
4-Chlorotoluene ND mg/kg 10/14/22 13:56 106-43-410/14/22 13:250.010 0.0018 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/14/22 13:56 96-12-810/14/22 13:250.010 0.0040 1
Dibromochloromethane ND mg/kg 10/14/22 13:56 124-48-110/14/22 13:250.010 0.0057 1
1,2-Dibromoethane (EDB)ND mg/kg 10/14/22 13:56 106-93-410/14/22 13:250.010 0.0045 1
Dibromomethane ND mg/kg 10/14/22 13:56 74-95-310/14/22 13:250.010 0.0022 1
1,2-Dichlorobenzene ND mg/kg 10/14/22 13:56 95-50-110/14/22 13:250.010 0.0037 1
1,3-Dichlorobenzene ND mg/kg 10/14/22 13:56 541-73-110/14/22 13:250.010 0.0032 1
1,4-Dichlorobenzene ND mg/kg 10/14/22 13:56 106-46-710/14/22 13:250.010 0.0027 1
Dichlorodifluoromethane ND mg/kg 10/14/22 13:56 75-71-810/14/22 13:250.020 0.0044 1
1,1-Dichloroethane ND mg/kg 10/14/22 13:56 75-34-310/14/22 13:250.010 0.0042 1
1,2-Dichloroethane ND mg/kg 10/14/22 13:56 107-06-210/14/22 13:250.010 0.0068 1
1,1-Dichloroethene ND mg/kg 10/14/22 13:56 75-35-410/14/22 13:250.010 0.0042 1
cis-1,2-Dichloroethene ND mg/kg 10/14/22 13:56 156-59-210/14/22 13:250.010 0.0035 1
trans-1,2-Dichloroethene ND mg/kg 10/14/22 13:56 156-60-510/14/22 13:250.010 0.0036 1
1,2-Dichloropropane ND mg/kg 10/14/22 13:56 78-87-510/14/22 13:250.010 0.0031 1
1,3-Dichloropropane ND mg/kg 10/14/22 13:56 142-28-910/14/22 13:250.010 0.0032 1
2,2-Dichloropropane ND mg/kg 10/14/22 13:56 594-20-710/14/22 13:250.010 0.0033 1
1,1-Dichloropropene ND mg/kg 10/14/22 13:56 563-58-610/14/22 13:250.010 0.0049 1
cis-1,3-Dichloropropene ND mg/kg 10/14/22 13:56 10061-01-510/14/22 13:250.010 0.0028 1
trans-1,3-Dichloropropene ND mg/kg 10/14/22 13:56 10061-02-610/14/22 13:250.010 0.0035 1
Diisopropyl ether ND mg/kg 10/14/22 13:56 108-20-310/14/22 13:250.010 0.0028 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-1 Lab ID:92630074001 Collected:10/06/22 12:10 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 10/14/22 13:56 100-41-410/14/22 13:250.010 0.0048 1
Hexachloro-1,3-butadiene ND mg/kg 10/14/22 13:56 87-68-310/14/22 13:250.020 0.017 1
2-Hexanone ND mg/kg 10/14/22 13:56 591-78-610/14/22 13:250.10 0.0098 1
Isopropylbenzene (Cumene)ND mg/kg 10/14/22 13:56 98-82-810/14/22 13:250.010 0.0035 1
p-Isopropyltoluene ND mg/kg 10/14/22 13:56 99-87-610/14/22 13:250.010 0.0050 1
Methylene Chloride ND mg/kg 10/14/22 13:56 75-09-210/14/22 13:250.041 0.028 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/14/22 13:56 108-10-110/14/22 13:250.10 0.0098 1
Methyl-tert-butyl ether ND mg/kg 10/14/22 13:56 1634-04-410/14/22 13:250.010 0.0038 1
Naphthalene ND mg/kg 10/14/22 13:56 91-20-310/14/22 13:250.010 0.0054 1
n-Propylbenzene ND mg/kg 10/14/22 13:56 103-65-110/14/22 13:250.010 0.0036 1
Styrene ND mg/kg 10/14/22 13:56 100-42-510/14/22 13:250.010 0.0027 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/14/22 13:56 630-20-610/14/22 13:250.010 0.0039 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/14/22 13:56 79-34-510/14/22 13:250.010 0.0027 1
Tetrachloroethene ND mg/kg 10/14/22 13:56 127-18-410/14/22 13:250.010 0.0032 1
Toluene ND mg/kg 10/14/22 13:56 108-88-310/14/22 13:250.010 0.0029 1
1,2,3-Trichlorobenzene ND mg/kg 10/14/22 13:56 87-61-610/14/22 13:250.010 0.0082 1
1,2,4-Trichlorobenzene ND mg/kg 10/14/22 13:56 120-82-110/14/22 13:250.010 0.0086 1
1,1,1-Trichloroethane ND mg/kg 10/14/22 13:56 71-55-610/14/22 13:250.010 0.0053 1
1,1,2-Trichloroethane ND mg/kg 10/14/22 13:56 79-00-510/14/22 13:250.010 0.0034 1
Trichloroethene ND mg/kg 10/14/22 13:56 79-01-610/14/22 13:250.010 0.0026 1
Trichlorofluoromethane ND mg/kg 10/14/22 13:56 75-69-410/14/22 13:250.010 0.0056 1
1,2,3-Trichloropropane ND mg/kg 10/14/22 13:56 96-18-410/14/22 13:250.010 0.0052 1
1,2,4-Trimethylbenzene ND mg/kg 10/14/22 13:56 95-63-610/14/22 13:250.010 0.0028 1
1,3,5-Trimethylbenzene ND mg/kg 10/14/22 13:56 108-67-810/14/22 13:250.010 0.0034 1
Vinyl acetate ND mg/kg 10/14/22 13:56 108-05-410/14/22 13:250.10 0.0074 1
Vinyl chloride ND mg/kg 10/14/22 13:56 75-01-410/14/22 13:250.020 0.0052 1
Xylene (Total)ND mg/kg 10/14/22 13:56 1330-20-710/14/22 13:250.020 0.0058 1
m&p-Xylene ND mg/kg 10/14/22 13:56 179601-23-110/14/22 13:250.020 0.0070 1
o-Xylene 0.0057J mg/kg 10/14/22 13:56 95-47-610/14/22 13:250.010 0.0045 1
Surrogates
Toluene-d8 (S)101 %10/14/22 13:56 2037-26-510/14/22 13:2570-130 1
4-Bromofluorobenzene (S)103 %10/14/22 13:56 460-00-410/14/22 13:2570-130 1
1,2-Dichloroethane-d4 (S)112 %10/14/22 13:56 17060-07-010/14/22 13:2570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 34.4 %10/10/22 16:49 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 65.3 %10/14/22 17:0910/14/22 16:541
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-1 Lab ID:92630074001 Collected:10/06/22 12:10 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.54 mg/kg 10/17/22 12:06 18540-29-910/12/22 00:591.53 0.391 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-2 Lab ID:92630074002 Collected:10/06/22 12:20 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 10/13/22 23:01 7440-38-210/13/22 09:243.8 2.7 1
Barium 3.7 mg/kg 10/13/22 23:01 7440-39-310/13/22 09:241.3 0.52 1
Cadmium ND mg/kg 10/13/22 23:01 7440-43-910/13/22 09:241.3 0.37 1
Chromium 12.2 mg/kg 10/13/22 23:01 7440-47-310/13/22 09:241.3 1.1 1
Lead 10.6 mg/kg 10/13/22 23:01 7439-92-110/13/22 09:243.1 2.0 1
Selenium ND mg/kg 10/14/22 14:55 7782-49-2 D310/13/22 09:2431.4 27.2 5
Silver ND mg/kg 10/13/22 23:01 7440-22-410/13/22 09:241.3 0.51 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.014J mg/kg 10/14/22 12:42 7439-97-610/14/22 08:000.31 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/14/22 11:12 83-32-910/12/22 17:094.3 1.5 10
Acenaphthylene ND mg/kg 10/14/22 11:12 208-96-810/12/22 17:094.3 1.5 10
Aniline ND mg/kg 10/14/22 11:12 62-53-310/12/22 17:094.3 1.7 10
Anthracene ND mg/kg 10/14/22 11:12 120-12-710/12/22 17:094.3 1.4 10
Benzo(a)anthracene ND mg/kg 10/14/22 11:12 56-55-310/12/22 17:094.3 1.4 10
Benzo(a)pyrene ND mg/kg 10/14/22 11:12 50-32-810/12/22 17:094.3 1.5 10
Benzo(b)fluoranthene ND mg/kg 10/14/22 11:12 205-99-210/12/22 17:094.3 1.4 10
Benzo(g,h,i)perylene ND mg/kg 10/14/22 11:12 191-24-210/12/22 17:094.3 1.7 10
Benzo(k)fluoranthene ND mg/kg 10/14/22 11:12 207-08-910/12/22 17:094.3 1.5 10
Benzoic Acid ND mg/kg 10/14/22 11:12 65-85-010/12/22 17:0921.7 9.3 10
Benzyl alcohol ND mg/kg 10/14/22 11:12 100-51-610/12/22 17:098.7 3.3 10
4-Bromophenylphenyl ether ND mg/kg 10/14/22 11:12 101-55-310/12/22 17:094.3 1.7 10
Butylbenzylphthalate ND mg/kg 10/14/22 11:12 85-68-710/12/22 17:094.3 1.8 10
4-Chloro-3-methylphenol ND mg/kg 10/14/22 11:12 59-50-710/12/22 17:098.7 3.1 10
4-Chloroaniline ND mg/kg 10/14/22 11:12 106-47-810/12/22 17:098.7 3.4 10
bis(2-Chloroethoxy)methane ND mg/kg 10/14/22 11:12 111-91-110/12/22 17:094.3 1.8 10
bis(2-Chloroethyl) ether ND mg/kg 10/14/22 11:12 111-44-410/12/22 17:094.3 1.6 10
2-Chloronaphthalene ND mg/kg 10/14/22 11:12 91-58-710/12/22 17:094.3 1.7 10
2-Chlorophenol ND mg/kg 10/14/22 11:12 95-57-810/12/22 17:094.3 1.6 10
4-Chlorophenylphenyl ether ND mg/kg 10/14/22 11:12 7005-72-310/12/22 17:094.3 1.6 10
Chrysene ND mg/kg 10/14/22 11:12 218-01-910/12/22 17:094.3 1.6 10
Dibenz(a,h)anthracene ND mg/kg 10/14/22 11:12 53-70-310/12/22 17:094.3 1.7 10
Dibenzofuran ND mg/kg 10/14/22 11:12 132-64-910/12/22 17:094.3 1.6 10
1,2-Dichlorobenzene ND mg/kg 10/14/22 11:12 95-50-110/12/22 17:094.3 1.6 10
1,3-Dichlorobenzene ND mg/kg 10/14/22 11:12 541-73-110/12/22 17:094.3 1.5 10
1,4-Dichlorobenzene ND mg/kg 10/14/22 11:12 106-46-710/12/22 17:094.3 1.7 10
3,3'-Dichlorobenzidine ND mg/kg 10/14/22 11:12 91-94-110/12/22 17:098.7 2.9 10
2,4-Dichlorophenol ND mg/kg 10/14/22 11:12 120-83-210/12/22 17:094.3 1.7 10
Diethylphthalate ND mg/kg 10/14/22 11:12 84-66-210/12/22 17:094.3 1.6 10
2,4-Dimethylphenol ND mg/kg 10/14/22 11:12 105-67-910/12/22 17:094.3 1.8 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-2 Lab ID:92630074002 Collected:10/06/22 12:20 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 10/14/22 11:12 131-11-310/12/22 17:094.3 1.6 10
Di-n-butylphthalate ND mg/kg 10/14/22 11:12 84-74-210/12/22 17:094.3 1.5 10
4,6-Dinitro-2-methylphenol ND mg/kg 10/14/22 11:12 534-52-110/12/22 17:098.7 4.1 10
2,4-Dinitrophenol ND mg/kg 10/14/22 11:12 51-28-510/12/22 17:0921.7 13.4 10
2,4-Dinitrotoluene ND mg/kg 10/14/22 11:12 121-14-210/12/22 17:094.3 1.7 10
2,6-Dinitrotoluene ND mg/kg 10/14/22 11:12 606-20-210/12/22 17:094.3 1.6 10
Di-n-octylphthalate ND mg/kg 10/14/22 11:12 117-84-010/12/22 17:094.3 1.7 10
bis(2-Ethylhexyl)phthalate ND mg/kg 10/14/22 11:12 117-81-710/12/22 17:094.3 1.7 10
Fluoranthene ND mg/kg 10/14/22 11:12 206-44-010/12/22 17:094.3 1.5 10
Fluorene ND mg/kg 10/14/22 11:12 86-73-710/12/22 17:094.3 1.5 10
Hexachloro-1,3-butadiene ND mg/kg 10/14/22 11:12 87-68-3 v110/12/22 17:094.3 1.9 10
Hexachlorobenzene ND mg/kg 10/14/22 11:12 118-74-110/12/22 17:094.3 1.7 10
Hexachlorocyclopentadiene ND mg/kg 10/14/22 11:12 77-47-4 v210/12/22 17:094.3 2.5 10
Hexachloroethane ND mg/kg 10/14/22 11:12 67-72-110/12/22 17:094.3 1.7 10
Indeno(1,2,3-cd)pyrene ND mg/kg 10/14/22 11:12 193-39-510/12/22 17:094.3 1.7 10
Isophorone ND mg/kg 10/14/22 11:12 78-59-110/12/22 17:094.3 1.9 10
1-Methylnaphthalene ND mg/kg 10/14/22 11:12 90-12-010/12/22 17:094.3 1.5 10
2-Methylnaphthalene ND mg/kg 10/14/22 11:12 91-57-610/12/22 17:094.3 1.7 10
2-Methylphenol(o-Cresol)ND mg/kg 10/14/22 11:12 95-48-710/12/22 17:094.3 1.8 10
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/14/22 11:12 15831-10-410/12/22 17:094.3 1.7 10
Naphthalene ND mg/kg 10/14/22 11:12 91-20-310/12/22 17:094.3 1.5 10
2-Nitroaniline ND mg/kg 10/14/22 11:12 88-74-410/12/22 17:0921.7 3.6 10
3-Nitroaniline ND mg/kg 10/14/22 11:12 99-09-210/12/22 17:0921.7 3.4 10
4-Nitroaniline ND mg/kg 10/14/22 11:12 100-01-610/12/22 17:098.7 3.3 10
Nitrobenzene ND mg/kg 10/14/22 11:12 98-95-310/12/22 17:094.3 2.0 10
2-Nitrophenol ND mg/kg 10/14/22 11:12 88-75-510/12/22 17:094.3 1.9 10
4-Nitrophenol ND mg/kg 10/14/22 11:12 100-02-7 v210/12/22 17:0921.7 8.4 10
N-Nitrosodimethylamine ND mg/kg 10/14/22 11:12 62-75-910/12/22 17:094.3 1.5 10
N-Nitroso-di-n-propylamine ND mg/kg 10/14/22 11:12 621-64-710/12/22 17:094.3 1.6 10
N-Nitrosodiphenylamine ND mg/kg 10/14/22 11:12 86-30-610/12/22 17:094.3 1.5 10
2,2'-Oxybis(1-chloropropane)ND mg/kg 10/14/22 11:12 108-60-110/12/22 17:094.3 2.1 10
Pentachlorophenol ND mg/kg 10/14/22 11:12 87-86-5 v210/12/22 17:098.7 4.2 10
Phenanthrene ND mg/kg 10/14/22 11:12 85-01-810/12/22 17:094.3 1.4 10
Phenol ND mg/kg 10/14/22 11:12 108-95-210/12/22 17:094.3 1.9 10
Pyrene ND mg/kg 10/14/22 11:12 129-00-010/12/22 17:094.3 1.8 10
Pyridine ND mg/kg 10/14/22 11:12 110-86-110/12/22 17:094.3 1.4 10
1,2,4-Trichlorobenzene ND mg/kg 10/14/22 11:12 120-82-110/12/22 17:094.3 1.7 10
2,4,5-Trichlorophenol ND mg/kg 10/14/22 11:12 95-95-410/12/22 17:094.3 2.0 10
2,4,6-Trichlorophenol ND mg/kg 10/14/22 11:12 88-06-210/12/22 17:094.3 1.8 10
Surrogates
Nitrobenzene-d5 (S)0 %10/14/22 11:12 4165-60-0 D3,S410/12/22 17:0910-130 10
2-Fluorobiphenyl (S)0 %10/14/22 11:12 321-60-8 S410/12/22 17:0910-130 10
Terphenyl-d14 (S)0 %10/14/22 11:12 1718-51-0 S410/12/22 17:0910-130 10
Phenol-d6 (S)0 %10/14/22 11:12 13127-88-3 S410/12/22 17:0910-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-2 Lab ID:92630074002 Collected:10/06/22 12:20 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)0 %10/14/22 11:12 367-12-4 S410/12/22 17:0910-130 10
2,4,6-Tribromophenol (S)0 %10/14/22 11:12 118-79-6 S410/12/22 17:0910-131 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/13/22 21:56 67-64-110/13/22 16:370.16 0.052 1
Benzene ND mg/kg 10/13/22 21:56 71-43-210/13/22 16:370.0081 0.0032 1
Bromobenzene ND mg/kg 10/13/22 21:56 108-86-110/13/22 16:370.0081 0.0026 1
Bromochloromethane ND mg/kg 10/13/22 21:56 74-97-510/13/22 16:370.0081 0.0024 1
Bromodichloromethane ND mg/kg 10/13/22 21:56 75-27-410/13/22 16:370.0081 0.0031 1
Bromoform ND mg/kg 10/13/22 21:56 75-25-210/13/22 16:370.0081 0.0029 1
Bromomethane ND mg/kg 10/13/22 21:56 74-83-9 IK10/13/22 16:370.016 0.013 1
2-Butanone (MEK)ND mg/kg 10/13/22 21:56 78-93-310/13/22 16:370.16 0.039 1
n-Butylbenzene ND mg/kg 10/13/22 21:56 104-51-810/13/22 16:370.0081 0.0038 1
sec-Butylbenzene ND mg/kg 10/13/22 21:56 135-98-810/13/22 16:370.0081 0.0036 1
tert-Butylbenzene ND mg/kg 10/13/22 21:56 98-06-610/13/22 16:370.0081 0.0029 1
Carbon tetrachloride ND mg/kg 10/13/22 21:56 56-23-510/13/22 16:370.0081 0.0030 1
Chlorobenzene ND mg/kg 10/13/22 21:56 108-90-710/13/22 16:370.0081 0.0016 1
Chloroethane ND mg/kg 10/13/22 21:56 75-00-310/13/22 16:370.016 0.0063 1
Chloroform ND mg/kg 10/13/22 21:56 67-66-310/13/22 16:370.0081 0.0049 1
Chloromethane 0.0099J mg/kg 10/13/22 21:56 74-87-310/13/22 16:370.016 0.0068 1
2-Chlorotoluene ND mg/kg 10/13/22 21:56 95-49-810/13/22 16:370.0081 0.0029 1
4-Chlorotoluene ND mg/kg 10/13/22 21:56 106-43-410/13/22 16:370.0081 0.0014 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/13/22 21:56 96-12-810/13/22 16:370.0081 0.0031 1
Dibromochloromethane ND mg/kg 10/13/22 21:56 124-48-110/13/22 16:370.0081 0.0046 1
1,2-Dibromoethane (EDB)ND mg/kg 10/13/22 21:56 106-93-410/13/22 16:370.0081 0.0036 1
Dibromomethane ND mg/kg 10/13/22 21:56 74-95-310/13/22 16:370.0081 0.0017 1
1,2-Dichlorobenzene ND mg/kg 10/13/22 21:56 95-50-110/13/22 16:370.0081 0.0029 1
1,3-Dichlorobenzene ND mg/kg 10/13/22 21:56 541-73-110/13/22 16:370.0081 0.0025 1
1,4-Dichlorobenzene ND mg/kg 10/13/22 21:56 106-46-710/13/22 16:370.0081 0.0021 1
Dichlorodifluoromethane ND mg/kg 10/13/22 21:56 75-71-8 v110/13/22 16:370.016 0.0035 1
1,1-Dichloroethane ND mg/kg 10/13/22 21:56 75-34-310/13/22 16:370.0081 0.0033 1
1,2-Dichloroethane ND mg/kg 10/13/22 21:56 107-06-210/13/22 16:370.0081 0.0054 1
1,1-Dichloroethene ND mg/kg 10/13/22 21:56 75-35-410/13/22 16:370.0081 0.0033 1
cis-1,2-Dichloroethene ND mg/kg 10/13/22 21:56 156-59-210/13/22 16:370.0081 0.0028 1
trans-1,2-Dichloroethene ND mg/kg 10/13/22 21:56 156-60-510/13/22 16:370.0081 0.0028 1
1,2-Dichloropropane ND mg/kg 10/13/22 21:56 78-87-510/13/22 16:370.0081 0.0024 1
1,3-Dichloropropane ND mg/kg 10/13/22 21:56 142-28-910/13/22 16:370.0081 0.0025 1
2,2-Dichloropropane ND mg/kg 10/13/22 21:56 594-20-710/13/22 16:370.0081 0.0026 1
1,1-Dichloropropene ND mg/kg 10/13/22 21:56 563-58-610/13/22 16:370.0081 0.0039 1
cis-1,3-Dichloropropene ND mg/kg 10/13/22 21:56 10061-01-510/13/22 16:370.0081 0.0022 1
trans-1,3-Dichloropropene ND mg/kg 10/13/22 21:56 10061-02-610/13/22 16:370.0081 0.0028 1
Diisopropyl ether ND mg/kg 10/13/22 21:56 108-20-310/13/22 16:370.0081 0.0022 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-2 Lab ID:92630074002 Collected:10/06/22 12:20 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 10/13/22 21:56 100-41-410/13/22 16:370.0081 0.0038 1
Hexachloro-1,3-butadiene ND mg/kg 10/13/22 21:56 87-68-310/13/22 16:370.016 0.013 1
2-Hexanone ND mg/kg 10/13/22 21:56 591-78-610/13/22 16:370.081 0.0078 1
Isopropylbenzene (Cumene)ND mg/kg 10/13/22 21:56 98-82-810/13/22 16:370.0081 0.0028 1
p-Isopropyltoluene ND mg/kg 10/13/22 21:56 99-87-610/13/22 16:370.0081 0.0040 1
Methylene Chloride 0.041 mg/kg 10/13/22 21:56 75-09-2 C9,D610/13/22 16:370.032 0.022 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/13/22 21:56 108-10-110/13/22 16:370.081 0.0078 1
Methyl-tert-butyl ether ND mg/kg 10/13/22 21:56 1634-04-410/13/22 16:370.0081 0.0030 1
Naphthalene ND mg/kg 10/13/22 21:56 91-20-310/13/22 16:370.0081 0.0043 1
n-Propylbenzene ND mg/kg 10/13/22 21:56 103-65-110/13/22 16:370.0081 0.0029 1
Styrene ND mg/kg 10/13/22 21:56 100-42-510/13/22 16:370.0081 0.0021 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/13/22 21:56 630-20-610/13/22 16:370.0081 0.0031 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/13/22 21:56 79-34-510/13/22 16:370.0081 0.0021 1
Tetrachloroethene ND mg/kg 10/13/22 21:56 127-18-410/13/22 16:370.0081 0.0026 1
Toluene ND mg/kg 10/13/22 21:56 108-88-310/13/22 16:370.0081 0.0023 1
1,2,3-Trichlorobenzene ND mg/kg 10/13/22 21:56 87-61-610/13/22 16:370.0081 0.0066 1
1,2,4-Trichlorobenzene ND mg/kg 10/13/22 21:56 120-82-110/13/22 16:370.0081 0.0068 1
1,1,1-Trichloroethane ND mg/kg 10/13/22 21:56 71-55-610/13/22 16:370.0081 0.0042 1
1,1,2-Trichloroethane ND mg/kg 10/13/22 21:56 79-00-510/13/22 16:370.0081 0.0027 1
Trichloroethene ND mg/kg 10/13/22 21:56 79-01-610/13/22 16:370.0081 0.0021 1
Trichlorofluoromethane ND mg/kg 10/13/22 21:56 75-69-410/13/22 16:370.0081 0.0045 1
1,2,3-Trichloropropane ND mg/kg 10/13/22 21:56 96-18-410/13/22 16:370.0081 0.0041 1
1,2,4-Trimethylbenzene ND mg/kg 10/13/22 21:56 95-63-610/13/22 16:370.0081 0.0022 1
1,3,5-Trimethylbenzene ND mg/kg 10/13/22 21:56 108-67-810/13/22 16:370.0081 0.0027 1
Vinyl acetate ND mg/kg 10/13/22 21:56 108-05-410/13/22 16:370.081 0.0059 1
Vinyl chloride ND mg/kg 10/13/22 21:56 75-01-4 v110/13/22 16:370.016 0.0041 1
Xylene (Total)ND mg/kg 10/13/22 21:56 1330-20-710/13/22 16:370.016 0.0046 1
m&p-Xylene ND mg/kg 10/13/22 21:56 179601-23-110/13/22 16:370.016 0.0056 1
o-Xylene ND mg/kg 10/13/22 21:56 95-47-610/13/22 16:370.0081 0.0036 1
Surrogates
Toluene-d8 (S)102 %10/13/22 21:56 2037-26-510/13/22 16:3770-130 1
4-Bromofluorobenzene (S)103 %10/13/22 21:56 460-00-410/13/22 16:3770-130 1
1,2-Dichloroethane-d4 (S)109 %10/13/22 21:56 17060-07-010/13/22 16:3770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.5 %10/10/22 16:49 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 62.0 %10/14/22 17:0910/14/22 16:541
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-2 Lab ID:92630074002 Collected:10/06/22 12:20 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.435J mg/kg 10/17/22 12:11 18540-29-9 J10/12/22 00:591.61 0.411 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-3 Lab ID:92630074003 Collected:10/06/22 12:30 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 10/13/22 23:06 7440-38-210/13/22 09:243.7 2.6 1
Barium 37.5 mg/kg 10/13/22 23:06 7440-39-310/13/22 09:241.2 0.51 1
Cadmium ND mg/kg 10/13/22 23:06 7440-43-910/13/22 09:241.2 0.37 1
Chromium 17.3 mg/kg 10/13/22 23:06 7440-47-310/13/22 09:241.2 1.1 1
Lead 20.0 mg/kg 10/13/22 23:06 7439-92-110/13/22 09:243.1 1.9 1
Selenium ND mg/kg 10/14/22 14:59 7782-49-2 D310/13/22 09:2430.8 26.7 5
Silver ND mg/kg 10/13/22 23:06 7440-22-410/13/22 09:241.2 0.50 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 10/14/22 12:45 7439-97-610/14/22 08:000.30 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/14/22 11:40 83-32-910/12/22 17:094.4 1.6 10
Acenaphthylene ND mg/kg 10/14/22 11:40 208-96-810/12/22 17:094.4 1.6 10
Aniline ND mg/kg 10/14/22 11:40 62-53-310/12/22 17:094.4 1.7 10
Anthracene ND mg/kg 10/14/22 11:40 120-12-710/12/22 17:094.4 1.4 10
Benzo(a)anthracene ND mg/kg 10/14/22 11:40 56-55-310/12/22 17:094.4 1.5 10
Benzo(a)pyrene ND mg/kg 10/14/22 11:40 50-32-810/12/22 17:094.4 1.5 10
Benzo(b)fluoranthene ND mg/kg 10/14/22 11:40 205-99-210/12/22 17:094.4 1.5 10
Benzo(g,h,i)perylene ND mg/kg 10/14/22 11:40 191-24-210/12/22 17:094.4 1.7 10
Benzo(k)fluoranthene ND mg/kg 10/14/22 11:40 207-08-910/12/22 17:094.4 1.6 10
Benzoic Acid ND mg/kg 10/14/22 11:40 65-85-010/12/22 17:0922.1 9.5 10
Benzyl alcohol ND mg/kg 10/14/22 11:40 100-51-610/12/22 17:098.8 3.4 10
4-Bromophenylphenyl ether ND mg/kg 10/14/22 11:40 101-55-310/12/22 17:094.4 1.7 10
Butylbenzylphthalate ND mg/kg 10/14/22 11:40 85-68-710/12/22 17:094.4 1.9 10
4-Chloro-3-methylphenol ND mg/kg 10/14/22 11:40 59-50-710/12/22 17:098.8 3.1 10
4-Chloroaniline ND mg/kg 10/14/22 11:40 106-47-810/12/22 17:098.8 3.5 10
bis(2-Chloroethoxy)methane ND mg/kg 10/14/22 11:40 111-91-110/12/22 17:094.4 1.8 10
bis(2-Chloroethyl) ether ND mg/kg 10/14/22 11:40 111-44-410/12/22 17:094.4 1.7 10
2-Chloronaphthalene ND mg/kg 10/14/22 11:40 91-58-710/12/22 17:094.4 1.8 10
2-Chlorophenol ND mg/kg 10/14/22 11:40 95-57-810/12/22 17:094.4 1.7 10
4-Chlorophenylphenyl ether ND mg/kg 10/14/22 11:40 7005-72-310/12/22 17:094.4 1.6 10
Chrysene ND mg/kg 10/14/22 11:40 218-01-910/12/22 17:094.4 1.6 10
Dibenz(a,h)anthracene ND mg/kg 10/14/22 11:40 53-70-310/12/22 17:094.4 1.7 10
Dibenzofuran ND mg/kg 10/14/22 11:40 132-64-910/12/22 17:094.4 1.6 10
1,2-Dichlorobenzene ND mg/kg 10/14/22 11:40 95-50-110/12/22 17:094.4 1.6 10
1,3-Dichlorobenzene ND mg/kg 10/14/22 11:40 541-73-110/12/22 17:094.4 1.6 10
1,4-Dichlorobenzene ND mg/kg 10/14/22 11:40 106-46-710/12/22 17:094.4 1.7 10
3,3'-Dichlorobenzidine ND mg/kg 10/14/22 11:40 91-94-110/12/22 17:098.8 3.0 10
2,4-Dichlorophenol ND mg/kg 10/14/22 11:40 120-83-210/12/22 17:094.4 1.7 10
Diethylphthalate ND mg/kg 10/14/22 11:40 84-66-210/12/22 17:094.4 1.6 10
2,4-Dimethylphenol ND mg/kg 10/14/22 11:40 105-67-910/12/22 17:094.4 1.8 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-3 Lab ID:92630074003 Collected:10/06/22 12:30 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 10/14/22 11:40 131-11-310/12/22 17:094.4 1.6 10
Di-n-butylphthalate ND mg/kg 10/14/22 11:40 84-74-210/12/22 17:094.4 1.5 10
4,6-Dinitro-2-methylphenol ND mg/kg 10/14/22 11:40 534-52-110/12/22 17:098.8 4.1 10
2,4-Dinitrophenol ND mg/kg 10/14/22 11:40 51-28-510/12/22 17:0922.1 13.7 10
2,4-Dinitrotoluene ND mg/kg 10/14/22 11:40 121-14-210/12/22 17:094.4 1.7 10
2,6-Dinitrotoluene ND mg/kg 10/14/22 11:40 606-20-210/12/22 17:094.4 1.6 10
Di-n-octylphthalate ND mg/kg 10/14/22 11:40 117-84-010/12/22 17:094.4 1.7 10
bis(2-Ethylhexyl)phthalate ND mg/kg 10/14/22 11:40 117-81-710/12/22 17:094.4 1.7 10
Fluoranthene ND mg/kg 10/14/22 11:40 206-44-010/12/22 17:094.4 1.5 10
Fluorene ND mg/kg 10/14/22 11:40 86-73-710/12/22 17:094.4 1.6 10
Hexachloro-1,3-butadiene ND mg/kg 10/14/22 11:40 87-68-3 v110/12/22 17:094.4 1.9 10
Hexachlorobenzene ND mg/kg 10/14/22 11:40 118-74-110/12/22 17:094.4 1.7 10
Hexachlorocyclopentadiene ND mg/kg 10/14/22 11:40 77-47-4 v210/12/22 17:094.4 2.5 10
Hexachloroethane ND mg/kg 10/14/22 11:40 67-72-110/12/22 17:094.4 1.7 10
Indeno(1,2,3-cd)pyrene ND mg/kg 10/14/22 11:40 193-39-510/12/22 17:094.4 1.7 10
Isophorone ND mg/kg 10/14/22 11:40 78-59-110/12/22 17:094.4 2.0 10
1-Methylnaphthalene ND mg/kg 10/14/22 11:40 90-12-010/12/22 17:094.4 1.6 10
2-Methylnaphthalene ND mg/kg 10/14/22 11:40 91-57-610/12/22 17:094.4 1.8 10
2-Methylphenol(o-Cresol)ND mg/kg 10/14/22 11:40 95-48-710/12/22 17:094.4 1.8 10
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/14/22 11:40 15831-10-410/12/22 17:094.4 1.8 10
Naphthalene ND mg/kg 10/14/22 11:40 91-20-310/12/22 17:094.4 1.5 10
2-Nitroaniline ND mg/kg 10/14/22 11:40 88-74-410/12/22 17:0922.1 3.6 10
3-Nitroaniline ND mg/kg 10/14/22 11:40 99-09-210/12/22 17:0922.1 3.5 10
4-Nitroaniline ND mg/kg 10/14/22 11:40 100-01-610/12/22 17:098.8 3.4 10
Nitrobenzene ND mg/kg 10/14/22 11:40 98-95-310/12/22 17:094.4 2.1 10
2-Nitrophenol ND mg/kg 10/14/22 11:40 88-75-510/12/22 17:094.4 1.9 10
4-Nitrophenol ND mg/kg 10/14/22 11:40 100-02-7 v210/12/22 17:0922.1 8.6 10
N-Nitrosodimethylamine ND mg/kg 10/14/22 11:40 62-75-910/12/22 17:094.4 1.5 10
N-Nitroso-di-n-propylamine ND mg/kg 10/14/22 11:40 621-64-710/12/22 17:094.4 1.7 10
N-Nitrosodiphenylamine ND mg/kg 10/14/22 11:40 86-30-610/12/22 17:094.4 1.6 10
2,2'-Oxybis(1-chloropropane)ND mg/kg 10/14/22 11:40 108-60-110/12/22 17:094.4 2.1 10
Pentachlorophenol ND mg/kg 10/14/22 11:40 87-86-5 v210/12/22 17:098.8 4.3 10
Phenanthrene ND mg/kg 10/14/22 11:40 85-01-810/12/22 17:094.4 1.4 10
Phenol ND mg/kg 10/14/22 11:40 108-95-210/12/22 17:094.4 2.0 10
Pyrene ND mg/kg 10/14/22 11:40 129-00-010/12/22 17:094.4 1.8 10
Pyridine ND mg/kg 10/14/22 11:40 110-86-110/12/22 17:094.4 1.4 10
1,2,4-Trichlorobenzene ND mg/kg 10/14/22 11:40 120-82-110/12/22 17:094.4 1.7 10
2,4,5-Trichlorophenol ND mg/kg 10/14/22 11:40 95-95-410/12/22 17:094.4 2.0 10
2,4,6-Trichlorophenol ND mg/kg 10/14/22 11:40 88-06-210/12/22 17:094.4 1.8 10
Surrogates
Nitrobenzene-d5 (S)0 %10/14/22 11:40 4165-60-0 D3,S410/12/22 17:0910-130 10
2-Fluorobiphenyl (S)0 %10/14/22 11:40 321-60-8 S410/12/22 17:0910-130 10
Terphenyl-d14 (S)0 %10/14/22 11:40 1718-51-0 S410/12/22 17:0910-130 10
Phenol-d6 (S)0 %10/14/22 11:40 13127-88-3 S410/12/22 17:0910-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-3 Lab ID:92630074003 Collected:10/06/22 12:30 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)0 %10/14/22 11:40 367-12-4 S410/12/22 17:0910-130 10
2,4,6-Tribromophenol (S)0 %10/14/22 11:40 118-79-6 S410/12/22 17:0910-131 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/13/22 22:14 67-64-110/13/22 16:370.17 0.054 1
Benzene ND mg/kg 10/13/22 22:14 71-43-210/13/22 16:370.0084 0.0033 1
Bromobenzene ND mg/kg 10/13/22 22:14 108-86-110/13/22 16:370.0084 0.0027 1
Bromochloromethane ND mg/kg 10/13/22 22:14 74-97-510/13/22 16:370.0084 0.0025 1
Bromodichloromethane ND mg/kg 10/13/22 22:14 75-27-410/13/22 16:370.0084 0.0032 1
Bromoform ND mg/kg 10/13/22 22:14 75-25-210/13/22 16:370.0084 0.0029 1
Bromomethane ND mg/kg 10/13/22 22:14 74-83-9 IK10/13/22 16:370.017 0.013 1
2-Butanone (MEK)ND mg/kg 10/13/22 22:14 78-93-310/13/22 16:370.17 0.040 1
n-Butylbenzene ND mg/kg 10/13/22 22:14 104-51-810/13/22 16:370.0084 0.0040 1
sec-Butylbenzene ND mg/kg 10/13/22 22:14 135-98-810/13/22 16:370.0084 0.0037 1
tert-Butylbenzene ND mg/kg 10/13/22 22:14 98-06-610/13/22 16:370.0084 0.0030 1
Carbon tetrachloride ND mg/kg 10/13/22 22:14 56-23-510/13/22 16:370.0084 0.0031 1
Chlorobenzene 0.0061J mg/kg 10/13/22 22:14 108-90-710/13/22 16:370.0084 0.0016 1
Chloroethane ND mg/kg 10/13/22 22:14 75-00-310/13/22 16:370.017 0.0065 1
Chloroform ND mg/kg 10/13/22 22:14 67-66-310/13/22 16:370.0084 0.0051 1
Chloromethane 0.010J mg/kg 10/13/22 22:14 74-87-310/13/22 16:370.017 0.0070 1
2-Chlorotoluene ND mg/kg 10/13/22 22:14 95-49-810/13/22 16:370.0084 0.0030 1
4-Chlorotoluene ND mg/kg 10/13/22 22:14 106-43-410/13/22 16:370.0084 0.0015 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/13/22 22:14 96-12-810/13/22 16:370.0084 0.0033 1
Dibromochloromethane ND mg/kg 10/13/22 22:14 124-48-110/13/22 16:370.0084 0.0047 1
1,2-Dibromoethane (EDB)ND mg/kg 10/13/22 22:14 106-93-410/13/22 16:370.0084 0.0037 1
Dibromomethane ND mg/kg 10/13/22 22:14 74-95-310/13/22 16:370.0084 0.0018 1
1,2-Dichlorobenzene ND mg/kg 10/13/22 22:14 95-50-110/13/22 16:370.0084 0.0030 1
1,3-Dichlorobenzene ND mg/kg 10/13/22 22:14 541-73-110/13/22 16:370.0084 0.0026 1
1,4-Dichlorobenzene ND mg/kg 10/13/22 22:14 106-46-710/13/22 16:370.0084 0.0022 1
Dichlorodifluoromethane ND mg/kg 10/13/22 22:14 75-71-8 v110/13/22 16:370.017 0.0036 1
1,1-Dichloroethane ND mg/kg 10/13/22 22:14 75-34-310/13/22 16:370.0084 0.0035 1
1,2-Dichloroethane ND mg/kg 10/13/22 22:14 107-06-210/13/22 16:370.0084 0.0055 1
1,1-Dichloroethene ND mg/kg 10/13/22 22:14 75-35-410/13/22 16:370.0084 0.0035 1
cis-1,2-Dichloroethene ND mg/kg 10/13/22 22:14 156-59-210/13/22 16:370.0084 0.0029 1
trans-1,2-Dichloroethene ND mg/kg 10/13/22 22:14 156-60-510/13/22 16:370.0084 0.0029 1
1,2-Dichloropropane ND mg/kg 10/13/22 22:14 78-87-510/13/22 16:370.0084 0.0025 1
1,3-Dichloropropane ND mg/kg 10/13/22 22:14 142-28-910/13/22 16:370.0084 0.0026 1
2,2-Dichloropropane ND mg/kg 10/13/22 22:14 594-20-710/13/22 16:370.0084 0.0027 1
1,1-Dichloropropene ND mg/kg 10/13/22 22:14 563-58-610/13/22 16:370.0084 0.0040 1
cis-1,3-Dichloropropene ND mg/kg 10/13/22 22:14 10061-01-510/13/22 16:370.0084 0.0023 1
trans-1,3-Dichloropropene ND mg/kg 10/13/22 22:14 10061-02-610/13/22 16:370.0084 0.0029 1
Diisopropyl ether ND mg/kg 10/13/22 22:14 108-20-310/13/22 16:370.0084 0.0023 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-3 Lab ID:92630074003 Collected:10/06/22 12:30 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene 0.0068J mg/kg 10/13/22 22:14 100-41-410/13/22 16:370.0084 0.0039 1
Hexachloro-1,3-butadiene ND mg/kg 10/13/22 22:14 87-68-310/13/22 16:370.017 0.014 1
2-Hexanone ND mg/kg 10/13/22 22:14 591-78-610/13/22 16:370.084 0.0081 1
Isopropylbenzene (Cumene)ND mg/kg 10/13/22 22:14 98-82-810/13/22 16:370.0084 0.0028 1
p-Isopropyltoluene ND mg/kg 10/13/22 22:14 99-87-610/13/22 16:370.0084 0.0041 1
Methylene Chloride ND mg/kg 10/13/22 22:14 75-09-210/13/22 16:370.034 0.023 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/13/22 22:14 108-10-110/13/22 16:370.084 0.0081 1
Methyl-tert-butyl ether ND mg/kg 10/13/22 22:14 1634-04-410/13/22 16:370.0084 0.0031 1
Naphthalene ND mg/kg 10/13/22 22:14 91-20-3 M110/13/22 16:370.0084 0.0044 1
n-Propylbenzene ND mg/kg 10/13/22 22:14 103-65-110/13/22 16:370.0084 0.0030 1
Styrene ND mg/kg 10/13/22 22:14 100-42-510/13/22 16:370.0084 0.0022 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/13/22 22:14 630-20-610/13/22 16:370.0084 0.0032 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/13/22 22:14 79-34-510/13/22 16:370.0084 0.0022 1
Tetrachloroethene ND mg/kg 10/13/22 22:14 127-18-410/13/22 16:370.0084 0.0026 1
Toluene 0.0058J mg/kg 10/13/22 22:14 108-88-310/13/22 16:370.0084 0.0024 1
1,2,3-Trichlorobenzene ND mg/kg 10/13/22 22:14 87-61-6 M110/13/22 16:370.0084 0.0068 1
1,2,4-Trichlorobenzene ND mg/kg 10/13/22 22:14 120-82-110/13/22 16:370.0084 0.0070 1
1,1,1-Trichloroethane ND mg/kg 10/13/22 22:14 71-55-610/13/22 16:370.0084 0.0044 1
1,1,2-Trichloroethane ND mg/kg 10/13/22 22:14 79-00-510/13/22 16:370.0084 0.0028 1
Trichloroethene ND mg/kg 10/13/22 22:14 79-01-610/13/22 16:370.0084 0.0022 1
Trichlorofluoromethane ND mg/kg 10/13/22 22:14 75-69-410/13/22 16:370.0084 0.0046 1
1,2,3-Trichloropropane ND mg/kg 10/13/22 22:14 96-18-410/13/22 16:370.0084 0.0042 1
1,2,4-Trimethylbenzene ND mg/kg 10/13/22 22:14 95-63-610/13/22 16:370.0084 0.0023 1
1,3,5-Trimethylbenzene ND mg/kg 10/13/22 22:14 108-67-810/13/22 16:370.0084 0.0028 1
Vinyl acetate ND mg/kg 10/13/22 22:14 108-05-410/13/22 16:370.084 0.0061 1
Vinyl chloride ND mg/kg 10/13/22 22:14 75-01-4 v110/13/22 16:370.017 0.0043 1
Xylene (Total)0.021 mg/kg 10/13/22 22:14 1330-20-710/13/22 16:370.017 0.0048 1
m&p-Xylene 0.011J mg/kg 10/13/22 22:14 179601-23-110/13/22 16:370.017 0.0057 1
o-Xylene 0.0094 mg/kg 10/13/22 22:14 95-47-610/13/22 16:370.0084 0.0037 1
Surrogates
Toluene-d8 (S)101 %10/13/22 22:14 2037-26-510/13/22 16:3770-130 1
4-Bromofluorobenzene (S)103 %10/13/22 22:14 460-00-410/13/22 16:3770-130 1
1,2-Dichloroethane-d4 (S)110 %10/13/22 22:14 17060-07-010/13/22 16:3770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.9 %10/10/22 16:49 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 61.5 %10/14/22 17:0910/14/22 16:541
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-3 Lab ID:92630074003 Collected:10/06/22 12:30 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.437J mg/kg 10/17/22 12:17 18540-29-9 J10/12/22 00:591.62 0.414 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-4 Lab ID:92630074004 Collected:10/06/22 12:40 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 10/13/22 23:10 7440-38-210/13/22 09:243.9 2.8 1
Barium 11.2 mg/kg 10/13/22 23:10 7440-39-310/13/22 09:241.3 0.54 1
Cadmium ND mg/kg 10/13/22 23:10 7440-43-910/13/22 09:241.3 0.38 1
Chromium 23.0 mg/kg 10/13/22 23:10 7440-47-310/13/22 09:241.3 1.2 1
Lead 13.8 mg/kg 10/13/22 23:10 7439-92-110/13/22 09:243.2 2.0 1
Selenium ND mg/kg 10/14/22 15:04 7782-49-2 D310/13/22 09:2432.3 28.0 5
Silver ND mg/kg 10/13/22 23:10 7440-22-410/13/22 09:241.3 0.53 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.11J mg/kg 10/14/22 12:53 7439-97-610/14/22 08:000.32 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/14/22 12:07 83-32-910/12/22 17:094.4 1.5 10
Acenaphthylene ND mg/kg 10/14/22 12:07 208-96-810/12/22 17:094.4 1.5 10
Aniline ND mg/kg 10/14/22 12:07 62-53-310/12/22 17:094.4 1.7 10
Anthracene ND mg/kg 10/14/22 12:07 120-12-710/12/22 17:094.4 1.4 10
Benzo(a)anthracene ND mg/kg 10/14/22 12:07 56-55-310/12/22 17:094.4 1.5 10
Benzo(a)pyrene ND mg/kg 10/14/22 12:07 50-32-810/12/22 17:094.4 1.5 10
Benzo(b)fluoranthene ND mg/kg 10/14/22 12:07 205-99-210/12/22 17:094.4 1.5 10
Benzo(g,h,i)perylene ND mg/kg 10/14/22 12:07 191-24-210/12/22 17:094.4 1.7 10
Benzo(k)fluoranthene ND mg/kg 10/14/22 12:07 207-08-910/12/22 17:094.4 1.5 10
Benzoic Acid ND mg/kg 10/14/22 12:07 65-85-010/12/22 17:0921.8 9.4 10
Benzyl alcohol ND mg/kg 10/14/22 12:07 100-51-610/12/22 17:098.7 3.3 10
4-Bromophenylphenyl ether ND mg/kg 10/14/22 12:07 101-55-310/12/22 17:094.4 1.7 10
Butylbenzylphthalate ND mg/kg 10/14/22 12:07 85-68-710/12/22 17:094.4 1.8 10
4-Chloro-3-methylphenol ND mg/kg 10/14/22 12:07 59-50-710/12/22 17:098.7 3.1 10
4-Chloroaniline ND mg/kg 10/14/22 12:07 106-47-810/12/22 17:098.7 3.4 10
bis(2-Chloroethoxy)methane ND mg/kg 10/14/22 12:07 111-91-110/12/22 17:094.4 1.8 10
bis(2-Chloroethyl) ether ND mg/kg 10/14/22 12:07 111-44-410/12/22 17:094.4 1.6 10
2-Chloronaphthalene ND mg/kg 10/14/22 12:07 91-58-710/12/22 17:094.4 1.7 10
2-Chlorophenol ND mg/kg 10/14/22 12:07 95-57-810/12/22 17:094.4 1.6 10
4-Chlorophenylphenyl ether ND mg/kg 10/14/22 12:07 7005-72-310/12/22 17:094.4 1.6 10
Chrysene ND mg/kg 10/14/22 12:07 218-01-910/12/22 17:094.4 1.6 10
Dibenz(a,h)anthracene ND mg/kg 10/14/22 12:07 53-70-310/12/22 17:094.4 1.7 10
Dibenzofuran ND mg/kg 10/14/22 12:07 132-64-910/12/22 17:094.4 1.6 10
1,2-Dichlorobenzene ND mg/kg 10/14/22 12:07 95-50-110/12/22 17:094.4 1.6 10
1,3-Dichlorobenzene ND mg/kg 10/14/22 12:07 541-73-110/12/22 17:094.4 1.5 10
1,4-Dichlorobenzene ND mg/kg 10/14/22 12:07 106-46-710/12/22 17:094.4 1.7 10
3,3'-Dichlorobenzidine ND mg/kg 10/14/22 12:07 91-94-110/12/22 17:098.7 3.0 10
2,4-Dichlorophenol ND mg/kg 10/14/22 12:07 120-83-210/12/22 17:094.4 1.7 10
Diethylphthalate ND mg/kg 10/14/22 12:07 84-66-210/12/22 17:094.4 1.6 10
2,4-Dimethylphenol ND mg/kg 10/14/22 12:07 105-67-910/12/22 17:094.4 1.8 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-4 Lab ID:92630074004 Collected:10/06/22 12:40 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 10/14/22 12:07 131-11-310/12/22 17:094.4 1.6 10
Di-n-butylphthalate ND mg/kg 10/14/22 12:07 84-74-210/12/22 17:094.4 1.5 10
4,6-Dinitro-2-methylphenol ND mg/kg 10/14/22 12:07 534-52-110/12/22 17:098.7 4.1 10
2,4-Dinitrophenol ND mg/kg 10/14/22 12:07 51-28-510/12/22 17:0921.8 13.5 10
2,4-Dinitrotoluene ND mg/kg 10/14/22 12:07 121-14-210/12/22 17:094.4 1.7 10
2,6-Dinitrotoluene ND mg/kg 10/14/22 12:07 606-20-210/12/22 17:094.4 1.6 10
Di-n-octylphthalate ND mg/kg 10/14/22 12:07 117-84-010/12/22 17:094.4 1.7 10
bis(2-Ethylhexyl)phthalate ND mg/kg 10/14/22 12:07 117-81-710/12/22 17:094.4 1.7 10
Fluoranthene ND mg/kg 10/14/22 12:07 206-44-010/12/22 17:094.4 1.5 10
Fluorene ND mg/kg 10/14/22 12:07 86-73-710/12/22 17:094.4 1.5 10
Hexachloro-1,3-butadiene ND mg/kg 10/14/22 12:07 87-68-3 v110/12/22 17:094.4 1.9 10
Hexachlorobenzene ND mg/kg 10/14/22 12:07 118-74-110/12/22 17:094.4 1.7 10
Hexachlorocyclopentadiene ND mg/kg 10/14/22 12:07 77-47-4 v210/12/22 17:094.4 2.5 10
Hexachloroethane ND mg/kg 10/14/22 12:07 67-72-110/12/22 17:094.4 1.7 10
Indeno(1,2,3-cd)pyrene ND mg/kg 10/14/22 12:07 193-39-510/12/22 17:094.4 1.7 10
Isophorone ND mg/kg 10/14/22 12:07 78-59-110/12/22 17:094.4 1.9 10
1-Methylnaphthalene ND mg/kg 10/14/22 12:07 90-12-010/12/22 17:094.4 1.5 10
2-Methylnaphthalene ND mg/kg 10/14/22 12:07 91-57-610/12/22 17:094.4 1.7 10
2-Methylphenol(o-Cresol)ND mg/kg 10/14/22 12:07 95-48-710/12/22 17:094.4 1.8 10
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/14/22 12:07 15831-10-410/12/22 17:094.4 1.8 10
Naphthalene ND mg/kg 10/14/22 12:07 91-20-310/12/22 17:094.4 1.5 10
2-Nitroaniline ND mg/kg 10/14/22 12:07 88-74-410/12/22 17:0921.8 3.6 10
3-Nitroaniline ND mg/kg 10/14/22 12:07 99-09-210/12/22 17:0921.8 3.4 10
4-Nitroaniline ND mg/kg 10/14/22 12:07 100-01-610/12/22 17:098.7 3.3 10
Nitrobenzene ND mg/kg 10/14/22 12:07 98-95-310/12/22 17:094.4 2.0 10
2-Nitrophenol ND mg/kg 10/14/22 12:07 88-75-510/12/22 17:094.4 1.9 10
4-Nitrophenol ND mg/kg 10/14/22 12:07 100-02-7 v210/12/22 17:0921.8 8.4 10
N-Nitrosodimethylamine ND mg/kg 10/14/22 12:07 62-75-910/12/22 17:094.4 1.5 10
N-Nitroso-di-n-propylamine ND mg/kg 10/14/22 12:07 621-64-710/12/22 17:094.4 1.6 10
N-Nitrosodiphenylamine ND mg/kg 10/14/22 12:07 86-30-610/12/22 17:094.4 1.5 10
2,2'-Oxybis(1-chloropropane)ND mg/kg 10/14/22 12:07 108-60-110/12/22 17:094.4 2.1 10
Pentachlorophenol ND mg/kg 10/14/22 12:07 87-86-5 v210/12/22 17:098.7 4.3 10
Phenanthrene ND mg/kg 10/14/22 12:07 85-01-810/12/22 17:094.4 1.4 10
Phenol ND mg/kg 10/14/22 12:07 108-95-210/12/22 17:094.4 1.9 10
Pyrene ND mg/kg 10/14/22 12:07 129-00-010/12/22 17:094.4 1.8 10
Pyridine ND mg/kg 10/14/22 12:07 110-86-110/12/22 17:094.4 1.4 10
1,2,4-Trichlorobenzene ND mg/kg 10/14/22 12:07 120-82-110/12/22 17:094.4 1.7 10
2,4,5-Trichlorophenol ND mg/kg 10/14/22 12:07 95-95-410/12/22 17:094.4 2.0 10
2,4,6-Trichlorophenol ND mg/kg 10/14/22 12:07 88-06-210/12/22 17:094.4 1.8 10
Surrogates
Nitrobenzene-d5 (S)0 %10/14/22 12:07 4165-60-0 D3,S410/12/22 17:0910-130 10
2-Fluorobiphenyl (S)0 %10/14/22 12:07 321-60-8 S410/12/22 17:0910-130 10
Terphenyl-d14 (S)0 %10/14/22 12:07 1718-51-0 S410/12/22 17:0910-130 10
Phenol-d6 (S)0 %10/14/22 12:07 13127-88-3 S410/12/22 17:0910-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-4 Lab ID:92630074004 Collected:10/06/22 12:40 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)0 %10/14/22 12:07 367-12-4 S410/12/22 17:0910-130 10
2,4,6-Tribromophenol (S)0 %10/14/22 12:07 118-79-6 S410/12/22 17:0910-131 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/13/22 22:33 67-64-110/13/22 16:370.21 0.067 1
Benzene ND mg/kg 10/13/22 22:33 71-43-210/13/22 16:370.010 0.0041 1
Bromobenzene ND mg/kg 10/13/22 22:33 108-86-110/13/22 16:370.010 0.0034 1
Bromochloromethane ND mg/kg 10/13/22 22:33 74-97-510/13/22 16:370.010 0.0031 1
Bromodichloromethane ND mg/kg 10/13/22 22:33 75-27-410/13/22 16:370.010 0.0040 1
Bromoform ND mg/kg 10/13/22 22:33 75-25-210/13/22 16:370.010 0.0037 1
Bromomethane ND mg/kg 10/13/22 22:33 74-83-9 IK10/13/22 16:370.021 0.016 1
2-Butanone (MEK)ND mg/kg 10/13/22 22:33 78-93-310/13/22 16:370.21 0.050 1
n-Butylbenzene ND mg/kg 10/13/22 22:33 104-51-810/13/22 16:370.010 0.0049 1
sec-Butylbenzene ND mg/kg 10/13/22 22:33 135-98-810/13/22 16:370.010 0.0046 1
tert-Butylbenzene ND mg/kg 10/13/22 22:33 98-06-610/13/22 16:370.010 0.0037 1
Carbon tetrachloride ND mg/kg 10/13/22 22:33 56-23-510/13/22 16:370.010 0.0039 1
Chlorobenzene 0.0067J mg/kg 10/13/22 22:33 108-90-710/13/22 16:370.010 0.0020 1
Chloroethane ND mg/kg 10/13/22 22:33 75-00-310/13/22 16:370.021 0.0080 1
Chloroform ND mg/kg 10/13/22 22:33 67-66-310/13/22 16:370.010 0.0063 1
Chloromethane 0.011J mg/kg 10/13/22 22:33 74-87-310/13/22 16:370.021 0.0087 1
2-Chlorotoluene ND mg/kg 10/13/22 22:33 95-49-810/13/22 16:370.010 0.0037 1
4-Chlorotoluene ND mg/kg 10/13/22 22:33 106-43-410/13/22 16:370.010 0.0018 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/13/22 22:33 96-12-810/13/22 16:370.010 0.0040 1
Dibromochloromethane ND mg/kg 10/13/22 22:33 124-48-110/13/22 16:370.010 0.0058 1
1,2-Dibromoethane (EDB)ND mg/kg 10/13/22 22:33 106-93-410/13/22 16:370.010 0.0046 1
Dibromomethane ND mg/kg 10/13/22 22:33 74-95-310/13/22 16:370.010 0.0022 1
1,2-Dichlorobenzene ND mg/kg 10/13/22 22:33 95-50-110/13/22 16:370.010 0.0037 1
1,3-Dichlorobenzene ND mg/kg 10/13/22 22:33 541-73-110/13/22 16:370.010 0.0032 1
1,4-Dichlorobenzene ND mg/kg 10/13/22 22:33 106-46-710/13/22 16:370.010 0.0027 1
Dichlorodifluoromethane ND mg/kg 10/13/22 22:33 75-71-8 v110/13/22 16:370.021 0.0045 1
1,1-Dichloroethane ND mg/kg 10/13/22 22:33 75-34-310/13/22 16:370.010 0.0043 1
1,2-Dichloroethane ND mg/kg 10/13/22 22:33 107-06-210/13/22 16:370.010 0.0069 1
1,1-Dichloroethene ND mg/kg 10/13/22 22:33 75-35-410/13/22 16:370.010 0.0043 1
cis-1,2-Dichloroethene ND mg/kg 10/13/22 22:33 156-59-210/13/22 16:370.010 0.0035 1
trans-1,2-Dichloroethene ND mg/kg 10/13/22 22:33 156-60-510/13/22 16:370.010 0.0036 1
1,2-Dichloropropane ND mg/kg 10/13/22 22:33 78-87-510/13/22 16:370.010 0.0031 1
1,3-Dichloropropane ND mg/kg 10/13/22 22:33 142-28-910/13/22 16:370.010 0.0032 1
2,2-Dichloropropane ND mg/kg 10/13/22 22:33 594-20-710/13/22 16:370.010 0.0034 1
1,1-Dichloropropene ND mg/kg 10/13/22 22:33 563-58-610/13/22 16:370.010 0.0050 1
cis-1,3-Dichloropropene ND mg/kg 10/13/22 22:33 10061-01-510/13/22 16:370.010 0.0028 1
trans-1,3-Dichloropropene ND mg/kg 10/13/22 22:33 10061-02-610/13/22 16:370.010 0.0036 1
Diisopropyl ether ND mg/kg 10/13/22 22:33 108-20-310/13/22 16:370.010 0.0028 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-4 Lab ID:92630074004 Collected:10/06/22 12:40 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene 0.0084J mg/kg 10/13/22 22:33 100-41-410/13/22 16:370.010 0.0048 1
Hexachloro-1,3-butadiene ND mg/kg 10/13/22 22:33 87-68-310/13/22 16:370.021 0.017 1
2-Hexanone ND mg/kg 10/13/22 22:33 591-78-610/13/22 16:370.10 0.010 1
Isopropylbenzene (Cumene)ND mg/kg 10/13/22 22:33 98-82-810/13/22 16:370.010 0.0035 1
p-Isopropyltoluene ND mg/kg 10/13/22 22:33 99-87-610/13/22 16:370.010 0.0051 1
Methylene Chloride 0.083 mg/kg 10/13/22 22:33 75-09-2 C910/13/22 16:370.041 0.028 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/13/22 22:33 108-10-110/13/22 16:370.10 0.010 1
Methyl-tert-butyl ether ND mg/kg 10/13/22 22:33 1634-04-410/13/22 16:370.010 0.0039 1
Naphthalene ND mg/kg 10/13/22 22:33 91-20-310/13/22 16:370.010 0.0055 1
n-Propylbenzene ND mg/kg 10/13/22 22:33 103-65-110/13/22 16:370.010 0.0037 1
Styrene ND mg/kg 10/13/22 22:33 100-42-510/13/22 16:370.010 0.0027 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/13/22 22:33 630-20-610/13/22 16:370.010 0.0040 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/13/22 22:33 79-34-510/13/22 16:370.010 0.0027 1
Tetrachloroethene ND mg/kg 10/13/22 22:33 127-18-410/13/22 16:370.010 0.0033 1
Toluene ND mg/kg 10/13/22 22:33 108-88-310/13/22 16:370.010 0.0029 1
1,2,3-Trichlorobenzene ND mg/kg 10/13/22 22:33 87-61-610/13/22 16:370.010 0.0084 1
1,2,4-Trichlorobenzene ND mg/kg 10/13/22 22:33 120-82-110/13/22 16:370.010 0.0087 1
1,1,1-Trichloroethane ND mg/kg 10/13/22 22:33 71-55-610/13/22 16:370.010 0.0054 1
1,1,2-Trichloroethane ND mg/kg 10/13/22 22:33 79-00-510/13/22 16:370.010 0.0034 1
Trichloroethene ND mg/kg 10/13/22 22:33 79-01-610/13/22 16:370.010 0.0027 1
Trichlorofluoromethane ND mg/kg 10/13/22 22:33 75-69-410/13/22 16:370.010 0.0057 1
1,2,3-Trichloropropane ND mg/kg 10/13/22 22:33 96-18-410/13/22 16:370.010 0.0052 1
1,2,4-Trimethylbenzene ND mg/kg 10/13/22 22:33 95-63-610/13/22 16:370.010 0.0028 1
1,3,5-Trimethylbenzene ND mg/kg 10/13/22 22:33 108-67-810/13/22 16:370.010 0.0035 1
Vinyl acetate ND mg/kg 10/13/22 22:33 108-05-410/13/22 16:370.10 0.0076 1
Vinyl chloride ND mg/kg 10/13/22 22:33 75-01-4 v110/13/22 16:370.021 0.0053 1
Xylene (Total)0.023 mg/kg 10/13/22 22:33 1330-20-710/13/22 16:370.021 0.0059 1
m&p-Xylene 0.012J mg/kg 10/13/22 22:33 179601-23-110/13/22 16:370.021 0.0071 1
o-Xylene 0.011 mg/kg 10/13/22 22:33 95-47-610/13/22 16:370.010 0.0046 1
Surrogates
Toluene-d8 (S)101 %10/13/22 22:33 2037-26-510/13/22 16:3770-130 1
4-Bromofluorobenzene (S)105 %10/13/22 22:33 460-00-410/13/22 16:3770-130 1
1,2-Dichloroethane-d4 (S)107 %10/13/22 22:33 17060-07-010/13/22 16:3770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.7 %10/10/22 16:50 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 70.2 %10/14/22 17:0910/14/22 16:541
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Sample:SS-4 Lab ID:92630074004 Collected:10/06/22 12:40 Received:10/07/22 10:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.690J mg/kg 10/17/22 12:22 18540-29-9 J10/12/22 00:591.42 0.363 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729759
EPA 3050B
EPA 6010D
6010D ATL
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3799979
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 3.0 10/13/22 22:132.1
Barium mg/kg ND 1.0 10/13/22 22:130.41
Cadmium mg/kg ND 1.0 10/13/22 22:130.30
Chromium mg/kg ND 1.0 10/13/22 22:130.91
Lead mg/kg ND 2.5 10/13/22 22:131.6
Selenium mg/kg ND 5.0 10/13/22 22:134.3
Silver mg/kg ND 1.0 10/13/22 22:130.41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799980LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 99.8100 100 80-120
Barium mg/kg 106100 106 80-120
Cadmium mg/kg 104100 104 80-120
Chromium mg/kg 106100 106 80-120
Lead mg/kg 105100 105 80-120
Selenium mg/kg 95.4100 95 80-120
Silver mg/kg 103100 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799981MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92628711001
3799982
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg M11307775-12573 5 20130ND10296.4
Barium mg/kg M11305375-12552 0 20130213281280
Cadmium mg/kg 130 82 75-12578 5 20130ND107101
Chromium mg/kg M11307875-12574 4 2013025.8 126 121
Lead mg/kg 130 83 75-12577 6 2013022.4 130 123
Selenium mg/kg M11307375-12569 6 20130ND98.0 92.6
Silver mg/kg 130 80 75-12577 5 201302.9 107 102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
730046
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3801453
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.24 10/14/22 12:110.0099
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3801454LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.310.33 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3801455MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630074001
3801456
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg M10.44 74 75-12579 13 200.490.081J 0.41 0.47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
730115
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92630074002, 92630074003, 92630074004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3801867
Associated Lab Samples:92630074002, 92630074003, 92630074004
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 10/13/22 20:220.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 10/13/22 20:220.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 10/13/22 20:220.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 10/13/22 20:220.0017
1,1-Dichloroethane mg/kg ND 0.0050 10/13/22 20:220.0021
1,1-Dichloroethene mg/kg ND 0.0050 10/13/22 20:220.0021
1,1-Dichloropropene mg/kg ND 0.0050 10/13/22 20:220.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 10/13/22 20:220.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 10/13/22 20:220.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 10/13/22 20:220.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 10/13/22 20:220.0014
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 10/13/22 20:220.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 10/13/22 20:220.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 10/13/22 20:220.0018
1,2-Dichloroethane mg/kg ND 0.0050 10/13/22 20:220.0033
1,2-Dichloropropane mg/kg ND 0.0050 10/13/22 20:220.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 10/13/22 20:220.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 10/13/22 20:220.0016
1,3-Dichloropropane mg/kg ND 0.0050 10/13/22 20:220.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 10/13/22 20:220.0013
2,2-Dichloropropane mg/kg ND 0.0050 10/13/22 20:220.0016
2-Butanone (MEK)mg/kg ND 0.10 10/13/22 20:220.024
2-Chlorotoluene mg/kg ND 0.0050 10/13/22 20:220.0018
2-Hexanone mg/kg ND 0.050 10/13/22 20:220.0048
4-Chlorotoluene mg/kg ND 0.0050 10/13/22 20:220.00088
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 10/13/22 20:220.0048
Acetone mg/kg ND 0.10 10/13/22 20:220.032
Benzene mg/kg ND 0.0050 10/13/22 20:220.0020
Bromobenzene mg/kg ND 0.0050 10/13/22 20:220.0016
Bromochloromethane mg/kg ND 0.0050 10/13/22 20:220.0015
Bromodichloromethane mg/kg ND 0.0050 10/13/22 20:220.0019
Bromoform mg/kg ND 0.0050 10/13/22 20:220.0018
Bromomethane mg/kg ND 0.010 IK10/13/22 20:220.0079
Carbon tetrachloride mg/kg ND 0.0050 10/13/22 20:220.0019
Chlorobenzene mg/kg ND 0.0050 10/13/22 20:220.00096
Chloroethane mg/kg ND 0.010 10/13/22 20:220.0039
Chloroform mg/kg ND 0.0050 10/13/22 20:220.0030
Chloromethane mg/kg ND 0.010 10/13/22 20:220.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 10/13/22 20:220.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 10/13/22 20:220.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3801867
Associated Lab Samples:92630074002, 92630074003, 92630074004
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 10/13/22 20:220.0028
Dibromomethane mg/kg ND 0.0050 10/13/22 20:220.0011
Dichlorodifluoromethane mg/kg ND 0.010 v110/13/22 20:220.0022
Diisopropyl ether mg/kg ND 0.0050 10/13/22 20:220.0014
Ethylbenzene mg/kg ND 0.0050 10/13/22 20:220.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 10/13/22 20:220.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 10/13/22 20:220.0017
m&p-Xylene mg/kg ND 0.010 10/13/22 20:220.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 10/13/22 20:220.0019
Methylene Chloride mg/kg ND 0.020 10/13/22 20:220.014
n-Butylbenzene mg/kg ND 0.0050 10/13/22 20:220.0024
n-Propylbenzene mg/kg ND 0.0050 10/13/22 20:220.0018
Naphthalene mg/kg ND 0.0050 10/13/22 20:220.0026
o-Xylene mg/kg ND 0.0050 10/13/22 20:220.0022
p-Isopropyltoluene mg/kg ND 0.0050 10/13/22 20:220.0025
sec-Butylbenzene mg/kg ND 0.0050 10/13/22 20:220.0022
Styrene mg/kg ND 0.0050 10/13/22 20:220.0013
tert-Butylbenzene mg/kg ND 0.0050 10/13/22 20:220.0018
Tetrachloroethene mg/kg ND 0.0050 10/13/22 20:220.0016
Toluene mg/kg ND 0.0050 10/13/22 20:220.0014
trans-1,2-Dichloroethene mg/kg ND 0.0050 10/13/22 20:220.0018
trans-1,3-Dichloropropene mg/kg ND 0.0050 10/13/22 20:220.0017
Trichloroethene mg/kg ND 0.0050 10/13/22 20:220.0013
Trichlorofluoromethane mg/kg ND 0.0050 10/13/22 20:220.0028
Vinyl acetate mg/kg ND 0.050 10/13/22 20:220.0036
Vinyl chloride mg/kg ND 0.010 v110/13/22 20:220.0025
Xylene (Total)mg/kg ND 0.010 10/13/22 20:220.0028
1,2-Dichloroethane-d4 (S)%100 70-130 10/13/22 20:22
4-Bromofluorobenzene (S)%101 70-130 10/13/22 20:22
Toluene-d8 (S)%101 70-130 10/13/22 20:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3801868LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.31.2 102 70-130
1,1,1-Trichloroethane mg/kg 1.31.2 101 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.11.2 91 70-130
1,1,2-Trichloroethane mg/kg 1.21.2 94 70-130
1,1-Dichloroethane mg/kg 1.31.2 102 70-130
1,1-Dichloroethene mg/kg 1.31.2 106 70-130
1,1-Dichloropropene mg/kg 1.31.2 108 70-130
1,2,3-Trichlorobenzene mg/kg 1.21.2 96 70-130
1,2,3-Trichloropropane mg/kg 1.11.2 90 70-130
1,2,4-Trichlorobenzene mg/kg 1.21.2 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3801868LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.21.2 97 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.21.2 93 67-130
1,2-Dibromoethane (EDB)mg/kg 1.21.2 98 70-130
1,2-Dichlorobenzene mg/kg 1.21.2 97 70-130
1,2-Dichloroethane mg/kg 1.31.2 103 70-130
1,2-Dichloropropane mg/kg 1.31.2 103 70-130
1,3,5-Trimethylbenzene mg/kg 1.21.2 98 70-130
1,3-Dichlorobenzene mg/kg 1.21.2 99 70-130
1,3-Dichloropropane mg/kg 1.21.2 97 70-130
1,4-Dichlorobenzene mg/kg 1.21.2 97 70-130
2,2-Dichloropropane mg/kg 1.21.2 95 67-130
2-Butanone (MEK)mg/kg 2.52.5 101 66-130
2-Chlorotoluene mg/kg 1.21.2 95 70-130
2-Hexanone mg/kg 2.42.5 95 70-130
4-Chlorotoluene mg/kg 1.21.2 97 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.42.5 97 70-130
Acetone mg/kg 2.22.5 88 67-130
Benzene mg/kg 1.21.2 96 70-130
Bromobenzene mg/kg 1.21.2 97 70-130
Bromochloromethane mg/kg 1.31.2 106 70-130
Bromodichloromethane mg/kg 1.21.2 99 70-130
Bromoform mg/kg 1.31.2 103 70-130
Bromomethane mg/kg 1.3 IK1.2 108 53-175
Carbon tetrachloride mg/kg 1.31.2 103 70-130
Chlorobenzene mg/kg 1.21.2 99 70-130
Chloroethane mg/kg 1.41.2 111 70-135
Chloroform mg/kg 1.21.2 95 70-130
Chloromethane mg/kg 1.41.2 110 64-130
cis-1,2-Dichloroethene mg/kg 1.31.2 101 70-130
cis-1,3-Dichloropropene mg/kg 1.31.2 100 70-130
Dibromochloromethane mg/kg 1.21.2 98 70-130
Dibromomethane mg/kg 1.31.2 101 70-130
Dichlorodifluoromethane mg/kg 1.5 v11.2 123 63-145
Diisopropyl ether mg/kg 1.31.2 102 68-130
Ethylbenzene mg/kg 1.11.2 91 70-130
Hexachloro-1,3-butadiene mg/kg 1.21.2 98 70-130
Isopropylbenzene (Cumene)mg/kg 1.21.2 96 70-130
m&p-Xylene mg/kg 2.52.5 98 70-130
Methyl-tert-butyl ether mg/kg 1.31.2 102 70-130
Methylene Chloride mg/kg 1.21.2 98 67-130
n-Butylbenzene mg/kg 1.21.2 98 70-130
n-Propylbenzene mg/kg 1.21.2 98 70-130
Naphthalene mg/kg 1.21.2 96 70-130
o-Xylene mg/kg 1.21.2 100 70-130
p-Isopropyltoluene mg/kg 1.21.2 98 70-130
sec-Butylbenzene mg/kg 1.21.2 96 70-130
Styrene mg/kg 1.31.2 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3801868LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.31.2 103 64-130
Tetrachloroethene mg/kg 1.31.2 104 70-130
Toluene mg/kg 1.21.2 96 70-130
trans-1,2-Dichloroethene mg/kg 1.31.2 106 70-130
trans-1,3-Dichloropropene mg/kg 1.31.2 101 70-130
Trichloroethene mg/kg 1.31.2 104 70-130
Trichlorofluoromethane mg/kg 1.31.2 108 70-130
Vinyl acetate mg/kg 2.92.5 116 70-134
Vinyl chloride mg/kg 1.5 v11.2 120 68-130
Xylene (Total)mg/kg 3.73.8 99 70-130
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3803147MATRIX SPIKE SAMPLE:
MSSpike
Result
92630074003
1,1,1,2-Tetrachloroethane mg/kg 0.910.84 109 58-140ND
1,1,1-Trichloroethane mg/kg 0.920.84 110 58-144ND
1,1,2,2-Tetrachloroethane mg/kg 0.770.84 92 52-139ND
1,1,2-Trichloroethane mg/kg 0.830.84 100 56-140ND
1,1-Dichloroethane mg/kg 0.930.84 110 58-145ND
1,1-Dichloroethene mg/kg 1.00.84 123 57-158ND
1,1-Dichloropropene mg/kg 1.00.84 119 58-151ND
1,2,3-Trichlorobenzene mg/kg 0.16 M10.84 19 48-149ND
1,2,3-Trichloropropane mg/kg 0.770.84 92 54-132ND
1,2,4-Trichlorobenzene mg/kg 0.450.84 53 51-151ND
1,2,4-Trimethylbenzene mg/kg 0.910.84 108 38-170ND
1,2-Dibromo-3-chloropropane mg/kg 0.470.84 56 44-134ND
1,2-Dibromoethane (EDB)mg/kg 0.850.84 101 60-138ND
1,2-Dichlorobenzene mg/kg 0.870.84 104 59-147ND
1,2-Dichloroethane mg/kg 0.920.84 110 57-139ND
1,2-Dichloropropane mg/kg 0.930.84 111 62-145ND
1,3,5-Trimethylbenzene mg/kg 0.900.84 107 47-159ND
1,3-Dichlorobenzene mg/kg 0.900.84 108 58-144ND
1,3-Dichloropropane mg/kg 0.860.84 102 60-142ND
1,4-Dichlorobenzene mg/kg 0.860.84 103 57-143ND
2,2-Dichloropropane mg/kg 0.810.84 97 37-144ND
2-Butanone (MEK)mg/kg 1.51.7 87 28-146ND
2-Chlorotoluene mg/kg 0.860.84 103 55-158ND
2-Hexanone mg/kg 1.41.7 82 44-141ND
4-Chlorotoluene mg/kg 0.880.84 105 55-146ND
4-Methyl-2-pentanone (MIBK)mg/kg 1.51.7 92 50-138ND
Acetone mg/kg 1.21.7 74 20-136ND
Benzene mg/kg 0.870.84 104 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3803147MATRIX SPIKE SAMPLE:
MSSpike
Result
92630074003
Bromobenzene mg/kg 0.830.84 99 59-145ND
Bromochloromethane mg/kg 0.920.84 110 57-143ND
Bromodichloromethane mg/kg 0.870.84 104 53-133ND
Bromoform mg/kg 0.860.84 103 48-133ND
Bromomethane mg/kg 0.59 IK,v10.84 71 10-167ND
Carbon tetrachloride mg/kg 0.940.84 112 57-147ND
Chlorobenzene mg/kg 0.900.84 107 61-1440.0061J
Chloroethane mg/kg 0.140.84 17 10-153ND
Chloroform mg/kg 0.880.84 105 58-141ND
Chloromethane mg/kg 1.10.84 132 54-1650.010J
cis-1,2-Dichloroethene mg/kg 0.930.84 111 59-144ND
cis-1,3-Dichloropropene mg/kg 0.890.84 106 56-137ND
Dibromochloromethane mg/kg 0.860.84 102 53-139ND
Dibromomethane mg/kg 0.830.84 100 60-136ND
Dichlorodifluoromethane mg/kg 1.40.84 163 49-177ND
Diisopropyl ether mg/kg 0.870.84 103 53-136ND
Ethylbenzene mg/kg 0.850.84 100 53-1500.0068J
Hexachloro-1,3-butadiene mg/kg 0.850.84 102 42-186ND
Isopropylbenzene (Cumene)mg/kg 0.930.84 111 62-154ND
m&p-Xylene mg/kg 1.81.7 108 49-1560.011J
Methyl-tert-butyl ether mg/kg 0.850.84 101 54-133ND
Methylene Chloride mg/kg 0.820.84 98 50-153ND
n-Butylbenzene mg/kg 0.960.84 115 44-174ND
n-Propylbenzene mg/kg 0.920.84 110 52-157ND
Naphthalene mg/kg 0.14 M10.84 17 37-150ND
o-Xylene mg/kg 0.930.84 109 54-1500.0094
p-Isopropyltoluene mg/kg 0.930.84 111 50-164ND
sec-Butylbenzene mg/kg 0.950.84 113 58-161ND
Styrene mg/kg 0.910.84 109 60-148ND
tert-Butylbenzene mg/kg 0.910.84 109 44-151ND
Tetrachloroethene mg/kg 0.920.84 110 53-151ND
Toluene mg/kg 0.880.84 104 52-1480.0058J
trans-1,2-Dichloroethene mg/kg 0.950.84 113 60-148ND
trans-1,3-Dichloropropene mg/kg 0.880.84 105 55-133ND
Trichloroethene mg/kg 0.940.84 112 60-148ND
Trichlorofluoromethane mg/kg 0.150.84 18 10-154ND
Vinyl acetate mg/kg 1.71.7 103 50-149ND
Vinyl chloride mg/kg 1.20.84 143 57-157ND
Xylene (Total)mg/kg 2.82.5 109 52-1530.021
1,2-Dichloroethane-d4 (S)%121 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92630074002
3801870SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg 0.0042J 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND IK30ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg 0.0095J 300.0099J
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND v130ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92630074002
3801870SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg 0.083 C9,D668300.041
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND v130ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%105109
4-Bromofluorobenzene (S)%102103
Toluene-d8 (S)%100102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
730403
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92630074001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3803134
Associated Lab Samples:92630074001
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 10/14/22 13:000.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 10/14/22 13:000.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 10/14/22 13:000.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 10/14/22 13:000.0017
1,1-Dichloroethane mg/kg ND 0.0050 10/14/22 13:000.0021
1,1-Dichloroethene mg/kg ND 0.0050 10/14/22 13:000.0021
1,1-Dichloropropene mg/kg ND 0.0050 10/14/22 13:000.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 10/14/22 13:000.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 10/14/22 13:000.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 10/14/22 13:000.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 10/14/22 13:000.0014
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 10/14/22 13:000.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 10/14/22 13:000.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 10/14/22 13:000.0018
1,2-Dichloroethane mg/kg ND 0.0050 10/14/22 13:000.0033
1,2-Dichloropropane mg/kg ND 0.0050 10/14/22 13:000.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 10/14/22 13:000.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 10/14/22 13:000.0016
1,3-Dichloropropane mg/kg ND 0.0050 10/14/22 13:000.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 10/14/22 13:000.0013
2,2-Dichloropropane mg/kg ND 0.0050 10/14/22 13:000.0016
2-Butanone (MEK)mg/kg ND 0.10 10/14/22 13:000.024
2-Chlorotoluene mg/kg ND 0.0050 10/14/22 13:000.0018
2-Hexanone mg/kg ND 0.050 10/14/22 13:000.0048
4-Chlorotoluene mg/kg ND 0.0050 10/14/22 13:000.00088
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 10/14/22 13:000.0048
Acetone mg/kg ND 0.10 10/14/22 13:000.032
Benzene mg/kg ND 0.0050 10/14/22 13:000.0020
Bromobenzene mg/kg ND 0.0050 10/14/22 13:000.0016
Bromochloromethane mg/kg ND 0.0050 10/14/22 13:000.0015
Bromodichloromethane mg/kg ND 0.0050 10/14/22 13:000.0019
Bromoform mg/kg ND 0.0050 10/14/22 13:000.0018
Bromomethane mg/kg ND 0.010 IK,v110/14/22 13:000.0079
Carbon tetrachloride mg/kg ND 0.0050 10/14/22 13:000.0019
Chlorobenzene mg/kg ND 0.0050 10/14/22 13:000.00096
Chloroethane mg/kg ND 0.010 10/14/22 13:000.0039
Chloroform mg/kg ND 0.0050 10/14/22 13:000.0030
Chloromethane mg/kg ND 0.010 10/14/22 13:000.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 10/14/22 13:000.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 10/14/22 13:000.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3803134
Associated Lab Samples:92630074001
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 10/14/22 13:000.0028
Dibromomethane mg/kg ND 0.0050 10/14/22 13:000.0011
Dichlorodifluoromethane mg/kg ND 0.010 10/14/22 13:000.0022
Diisopropyl ether mg/kg ND 0.0050 10/14/22 13:000.0014
Ethylbenzene mg/kg ND 0.0050 10/14/22 13:000.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 10/14/22 13:000.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 10/14/22 13:000.0017
m&p-Xylene mg/kg ND 0.010 10/14/22 13:000.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 10/14/22 13:000.0019
Methylene Chloride mg/kg ND 0.020 10/14/22 13:000.014
n-Butylbenzene mg/kg ND 0.0050 10/14/22 13:000.0024
n-Propylbenzene mg/kg ND 0.0050 10/14/22 13:000.0018
Naphthalene mg/kg ND 0.0050 10/14/22 13:000.0026
o-Xylene mg/kg ND 0.0050 10/14/22 13:000.0022
p-Isopropyltoluene mg/kg ND 0.0050 10/14/22 13:000.0025
sec-Butylbenzene mg/kg ND 0.0050 10/14/22 13:000.0022
Styrene mg/kg ND 0.0050 10/14/22 13:000.0013
tert-Butylbenzene mg/kg ND 0.0050 10/14/22 13:000.0018
Tetrachloroethene mg/kg ND 0.0050 10/14/22 13:000.0016
Toluene mg/kg ND 0.0050 10/14/22 13:000.0014
trans-1,2-Dichloroethene mg/kg ND 0.0050 10/14/22 13:000.0018
trans-1,3-Dichloropropene mg/kg ND 0.0050 10/14/22 13:000.0017
Trichloroethene mg/kg ND 0.0050 10/14/22 13:000.0013
Trichlorofluoromethane mg/kg ND 0.0050 10/14/22 13:000.0028
Vinyl acetate mg/kg ND 0.050 10/14/22 13:000.0036
Vinyl chloride mg/kg ND 0.010 10/14/22 13:000.0025
Xylene (Total)mg/kg ND 0.010 10/14/22 13:000.0028
1,2-Dichloroethane-d4 (S)%101 70-130 10/14/22 13:00
4-Bromofluorobenzene (S)%98 70-130 10/14/22 13:00
Toluene-d8 (S)%101 70-130 10/14/22 13:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3803135LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.41.2 111 70-130
1,1,1-Trichloroethane mg/kg 1.31.2 107 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.21.2 96 70-130
1,1,2-Trichloroethane mg/kg 1.31.2 100 70-130
1,1-Dichloroethane mg/kg 1.31.2 108 70-130
1,1-Dichloroethene mg/kg 1.41.2 113 70-130
1,1-Dichloropropene mg/kg 1.51.2 116 70-130
1,2,3-Trichlorobenzene mg/kg 1.31.2 107 70-130
1,2,3-Trichloropropane mg/kg 1.21.2 94 70-130
1,2,4-Trichlorobenzene mg/kg 1.31.2 108 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3803135LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.31.2 108 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.21.2 98 67-130
1,2-Dibromoethane (EDB)mg/kg 1.31.2 105 70-130
1,2-Dichlorobenzene mg/kg 1.31.2 106 70-130
1,2-Dichloroethane mg/kg 1.41.2 108 70-130
1,2-Dichloropropane mg/kg 1.41.2 111 70-130
1,3,5-Trimethylbenzene mg/kg 1.31.2 106 70-130
1,3-Dichlorobenzene mg/kg 1.31.2 107 70-130
1,3-Dichloropropane mg/kg 1.31.2 103 70-130
1,4-Dichlorobenzene mg/kg 1.31.2 107 70-130
2,2-Dichloropropane mg/kg 1.21.2 92 67-130
2-Butanone (MEK)mg/kg 2.52.5 100 66-130
2-Chlorotoluene mg/kg 1.31.2 103 70-130
2-Hexanone mg/kg 2.52.5 99 70-130
4-Chlorotoluene mg/kg 1.31.2 106 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.52.5 102 70-130
Acetone mg/kg 2.32.5 90 67-130
Benzene mg/kg 1.31.2 104 70-130
Bromobenzene mg/kg 1.31.2 105 70-130
Bromochloromethane mg/kg 1.41.2 109 70-130
Bromodichloromethane mg/kg 1.31.2 106 70-130
Bromoform mg/kg 1.41.2 109 70-130
Bromomethane mg/kg 1.7 IK,v11.2 135 53-175
Carbon tetrachloride mg/kg 1.41.2 115 70-130
Chlorobenzene mg/kg 1.41.2 109 70-130
Chloroethane mg/kg 1.51.2 120 70-135
Chloroform mg/kg 1.31.2 100 70-130
Chloromethane mg/kg 1.51.2 117 64-130
cis-1,2-Dichloroethene mg/kg 1.31.2 107 70-130
cis-1,3-Dichloropropene mg/kg 1.31.2 106 70-130
Dibromochloromethane mg/kg 1.31.2 106 70-130
Dibromomethane mg/kg 1.31.2 107 70-130
Dichlorodifluoromethane mg/kg 1.81.2 143 63-145
Diisopropyl ether mg/kg 1.31.2 105 68-130
Ethylbenzene mg/kg 1.21.2 100 70-130
Hexachloro-1,3-butadiene mg/kg 1.31.2 103 70-130
Isopropylbenzene (Cumene)mg/kg 1.31.2 105 70-130
m&p-Xylene mg/kg 2.72.5 108 70-130
Methyl-tert-butyl ether mg/kg 1.31.2 104 70-130
Methylene Chloride mg/kg 1.21.2 98 67-130
n-Butylbenzene mg/kg 1.41.2 109 70-130
n-Propylbenzene mg/kg 1.31.2 108 70-130
Naphthalene mg/kg 1.31.2 105 70-130
o-Xylene mg/kg 1.41.2 109 70-130
p-Isopropyltoluene mg/kg 1.31.2 107 70-130
sec-Butylbenzene mg/kg 1.31.2 105 70-130
Styrene mg/kg 1.41.2 109 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3803135LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.41.2 110 64-130
Tetrachloroethene mg/kg 1.51.2 118 70-130
Toluene mg/kg 1.31.2 105 70-130
trans-1,2-Dichloroethene mg/kg 1.41.2 111 70-130
trans-1,3-Dichloropropene mg/kg 1.31.2 105 70-130
Trichloroethene mg/kg 1.41.2 113 70-130
Trichlorofluoromethane mg/kg 1.51.2 122 70-130
Vinyl acetate mg/kg 3.02.5 120 70-134
Vinyl chloride mg/kg 1.61.2 129 68-130
Xylene (Total)mg/kg 4.13.8 108 70-130
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3803137MATRIX SPIKE SAMPLE:
MSSpike
Result
92630561001
1,1,1,2-Tetrachloroethane mg/kg 1.51.5 107 58-140ND
1,1,1-Trichloroethane mg/kg 1.51.5 107 58-144ND
1,1,2,2-Tetrachloroethane mg/kg 1.41.5 98 52-139ND
1,1,2-Trichloroethane mg/kg 1.51.5 101 56-140ND
1,1-Dichloroethane mg/kg 1.51.5 106 58-145ND
1,1-Dichloroethene mg/kg 1.61.5 113 57-158ND
1,1-Dichloropropene mg/kg 1.61.5 113 58-151ND
1,2,3-Trichlorobenzene mg/kg 0.781.5 54 48-149ND
1,2,3-Trichloropropane mg/kg 1.41.5 97 54-132ND
1,2,4-Trichlorobenzene mg/kg 1.21.5 85 51-151ND
1,2,4-Trimethylbenzene mg/kg 10.61.5 92 38-1709.3
1,2-Dibromo-3-chloropropane mg/kg 1.21.5 84 44-134ND
1,2-Dibromoethane (EDB)mg/kg 1.41.5 100 60-138ND
1,2-Dichlorobenzene mg/kg 1.51.5 106 59-147ND
1,2-Dichloroethane mg/kg 1.51.5 105 57-139ND
1,2-Dichloropropane mg/kg 1.51.5 107 62-145ND
1,3,5-Trimethylbenzene mg/kg 3.91.5 100 47-1592.5
1,3-Dichlorobenzene mg/kg 1.51.5 106 58-144ND
1,3-Dichloropropane mg/kg 1.41.5 99 60-142ND
1,4-Dichlorobenzene mg/kg 1.51.5 101 57-143ND
2,2-Dichloropropane mg/kg 1.51.5 103 37-144ND
2-Butanone (MEK)mg/kg 2.72.8 94 28-146ND
2-Chlorotoluene mg/kg 1.71.5 116 55-158ND
2-Hexanone mg/kg 2.82.8 97 44-141ND
4-Chlorotoluene mg/kg 1.51.5 102 55-146ND
4-Methyl-2-pentanone (MIBK)mg/kg 2.92.8 97 50-138ND
Acetone mg/kg 2.22.8 77 20-136ND
Benzene mg/kg 1.41.5 99 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3803137MATRIX SPIKE SAMPLE:
MSSpike
Result
92630561001
Bromobenzene mg/kg 1.41.5 97 59-145ND
Bromochloromethane mg/kg 1.51.5 106 57-143ND
Bromodichloromethane mg/kg 1.51.5 104 53-133ND
Bromoform mg/kg 1.51.5 104 48-133ND
Bromomethane mg/kg 1.1 IK,v11.5 77 10-167ND
Carbon tetrachloride mg/kg 1.61.5 113 57-147ND
Chlorobenzene mg/kg 1.51.5 104 61-1440.017
Chloroethane mg/kg 0.281.5 20 10-153ND
Chloroform mg/kg 1.41.5 100 58-141ND
Chloromethane mg/kg 1.81.5 125 54-165ND
cis-1,2-Dichloroethene mg/kg 1.51.5 106 59-144ND
cis-1,3-Dichloropropene mg/kg 1.51.5 103 56-137ND
Dibromochloromethane mg/kg 1.41.5 100 53-139ND
Dibromomethane mg/kg 1.51.5 101 60-136ND
Dichlorodifluoromethane mg/kg 2.11.5 149 49-177ND
Diisopropyl ether mg/kg 1.41.5 100 53-136ND
Ethylbenzene mg/kg 3.11.5 97 53-1501.7
Hexachloro-1,3-butadiene mg/kg 1.51.5 107 42-186ND
Isopropylbenzene (Cumene)mg/kg 2.01.5 111 62-1540.40
m&p-Xylene mg/kg 5.42.8 105 49-1562.3
Methyl-tert-butyl ether mg/kg 1.41.5 97 54-133ND
Methylene Chloride mg/kg 1.61.5 103 50-1530.089
n-Butylbenzene mg/kg 2.41.5 124 44-1740.64
n-Propylbenzene mg/kg 2.91.5 98 52-1571.5
Naphthalene mg/kg 2.31.5 67 37-1501.3
o-Xylene mg/kg 1.81.5 109 54-1500.27
p-Isopropyltoluene mg/kg 2.01.5 108 50-1640.44
sec-Butylbenzene mg/kg 1.81.5 125 58-161ND
Styrene mg/kg 1.51.5 107 60-148ND
tert-Butylbenzene mg/kg 1.71.5 115 44-151ND
Tetrachloroethene mg/kg 1.51.5 104 53-151ND
Toluene mg/kg 1.51.5 103 52-148ND
trans-1,2-Dichloroethene mg/kg 1.61.5 110 60-148ND
trans-1,3-Dichloropropene mg/kg 1.51.5 103 55-133ND
Trichloroethene mg/kg 1.51.5 107 60-148ND
Trichlorofluoromethane mg/kg 0.431.5 30 10-154ND
Vinyl acetate mg/kg 3.22.8 111 50-149ND
Vinyl chloride mg/kg 2.01.5 137 57-157ND
Xylene (Total)mg/kg 7.24.3 107 52-1532.6
1,2-Dichloroethane-d4 (S)%120 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92630074001
3803136SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND IK,v130ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92630074001
3803136SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg 0.0054J 300.0057J
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%108112
4-Bromofluorobenzene (S)%101103
Toluene-d8 (S)%100101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729746
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3799933
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.32 10/13/22 15:070.13
1,2-Dichlorobenzene mg/kg ND 0.32 10/13/22 15:070.12
1,3-Dichlorobenzene mg/kg ND 0.32 10/13/22 15:070.12
1,4-Dichlorobenzene mg/kg ND 0.32 10/13/22 15:070.12
1-Methylnaphthalene mg/kg ND 0.32 10/13/22 15:070.11
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.32 v210/13/22 15:070.15
2,4,5-Trichlorophenol mg/kg ND 0.32 10/13/22 15:070.15
2,4,6-Trichlorophenol mg/kg ND 0.32 10/13/22 15:070.13
2,4-Dichlorophenol mg/kg ND 0.32 10/13/22 15:070.13
2,4-Dimethylphenol mg/kg ND 0.32 10/13/22 15:070.13
2,4-Dinitrophenol mg/kg ND 1.6 10/13/22 15:071.0
2,4-Dinitrotoluene mg/kg ND 0.32 10/13/22 15:070.12
2,6-Dinitrotoluene mg/kg ND 0.32 10/13/22 15:070.12
2-Chloronaphthalene mg/kg ND 0.32 10/13/22 15:070.13
2-Chlorophenol mg/kg ND 0.32 10/13/22 15:070.12
2-Methylnaphthalene mg/kg ND 0.32 10/13/22 15:070.13
2-Methylphenol(o-Cresol)mg/kg ND 0.32 10/13/22 15:070.13
2-Nitroaniline mg/kg ND 1.6 10/13/22 15:070.27
2-Nitrophenol mg/kg ND 0.32 10/13/22 15:070.14
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.32 10/13/22 15:070.13
3,3'-Dichlorobenzidine mg/kg ND 0.65 10/13/22 15:070.22
3-Nitroaniline mg/kg ND 1.6 10/13/22 15:070.25
4,6-Dinitro-2-methylphenol mg/kg ND 0.65 10/13/22 15:070.30
4-Bromophenylphenyl ether mg/kg ND 0.32 v110/13/22 15:070.12
4-Chloro-3-methylphenol mg/kg ND 0.65 10/13/22 15:070.23
4-Chloroaniline mg/kg ND 0.65 10/13/22 15:070.25
4-Chlorophenylphenyl ether mg/kg ND 0.32 10/13/22 15:070.12
4-Nitroaniline mg/kg ND 0.65 v210/13/22 15:070.25
4-Nitrophenol mg/kg ND 1.6 10/13/22 15:070.63
Acenaphthene mg/kg ND 0.32 10/13/22 15:070.11
Acenaphthylene mg/kg ND 0.32 10/13/22 15:070.11
Aniline mg/kg ND 0.32 10/13/22 15:070.13
Anthracene mg/kg ND 0.32 10/13/22 15:070.11
Benzo(a)anthracene mg/kg ND 0.32 10/13/22 15:070.11
Benzo(a)pyrene mg/kg ND 0.32 10/13/22 15:070.11
Benzo(b)fluoranthene mg/kg ND 0.32 10/13/22 15:070.11
Benzo(g,h,i)perylene mg/kg ND 0.32 10/13/22 15:070.13
Benzo(k)fluoranthene mg/kg ND 0.32 10/13/22 15:070.11
Benzoic Acid mg/kg ND 1.6 10/13/22 15:070.70
Benzyl alcohol mg/kg ND 0.65 10/13/22 15:070.25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3799933
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane mg/kg ND 0.32 10/13/22 15:070.13
bis(2-Chloroethyl) ether mg/kg ND 0.32 10/13/22 15:070.12
bis(2-Ethylhexyl)phthalate mg/kg ND 0.32 10/13/22 15:070.13
Butylbenzylphthalate mg/kg ND 0.32 10/13/22 15:070.14
Chrysene mg/kg ND 0.32 10/13/22 15:070.12
Di-n-butylphthalate mg/kg ND 0.32 10/13/22 15:070.11
Di-n-octylphthalate mg/kg ND 0.32 10/13/22 15:070.13
Dibenz(a,h)anthracene mg/kg ND 0.32 10/13/22 15:070.12
Dibenzofuran mg/kg ND 0.32 10/13/22 15:070.12
Diethylphthalate mg/kg ND 0.32 10/13/22 15:070.12
Dimethylphthalate mg/kg ND 0.32 10/13/22 15:070.12
Fluoranthene mg/kg ND 0.32 10/13/22 15:070.11
Fluorene mg/kg ND 0.32 10/13/22 15:070.11
Hexachloro-1,3-butadiene mg/kg ND 0.32 v110/13/22 15:070.14
Hexachlorobenzene mg/kg ND 0.32 10/13/22 15:070.13
Hexachlorocyclopentadiene mg/kg ND 0.32 10/13/22 15:070.19
Hexachloroethane mg/kg ND 0.32 10/13/22 15:070.12
Indeno(1,2,3-cd)pyrene mg/kg ND 0.32 10/13/22 15:070.13
Isophorone mg/kg ND 0.32 10/13/22 15:070.14
N-Nitroso-di-n-propylamine mg/kg ND 0.32 10/13/22 15:070.12
N-Nitrosodimethylamine mg/kg ND 0.32 10/13/22 15:070.11
N-Nitrosodiphenylamine mg/kg ND 0.32 10/13/22 15:070.12
Naphthalene mg/kg ND 0.32 10/13/22 15:070.11
Nitrobenzene mg/kg ND 0.32 10/13/22 15:070.15
Pentachlorophenol mg/kg ND 0.65 10/13/22 15:070.32
Phenanthrene mg/kg ND 0.32 10/13/22 15:070.11
Phenol mg/kg ND 0.32 10/13/22 15:070.14
Pyrene mg/kg ND 0.32 10/13/22 15:070.13
Pyridine mg/kg ND 0.32 10/13/22 15:070.10
2,4,6-Tribromophenol (S)%70 10-131 10/13/22 15:07
2-Fluorobiphenyl (S)%60 10-130 10/13/22 15:07
2-Fluorophenol (S)%56 10-130 10/13/22 15:07
Nitrobenzene-d5 (S)%63 10-130 10/13/22 15:07
Phenol-d6 (S)%55 10-130 10/13/22 15:07
Terphenyl-d14 (S)%69 10-130 10/13/22 15:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799934LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.41.7 82 43-130
1,2-Dichlorobenzene mg/kg 1.11.7 69 43-130
1,3-Dichlorobenzene mg/kg 1.11.7 66 43-130
1,4-Dichlorobenzene mg/kg 1.11.7 67 44-130
1-Methylnaphthalene mg/kg 1.31.7 77 47-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799934LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 0.67 v21.7 41 29-130
2,4,5-Trichlorophenol mg/kg 1.31.7 77 47-130
2,4,6-Trichlorophenol mg/kg 1.41.7 82 47-130
2,4-Dichlorophenol mg/kg 1.31.7 82 45-130
2,4-Dimethylphenol mg/kg 1.51.7 90 45-130
2,4-Dinitrophenol mg/kg 6.28.3 75 27-140
2,4-Dinitrotoluene mg/kg 1.31.7 79 46-130
2,6-Dinitrotoluene mg/kg 1.31.7 78 48-130
2-Chloronaphthalene mg/kg 1.21.7 75 46-130
2-Chlorophenol mg/kg 1.11.7 65 43-130
2-Methylnaphthalene mg/kg 1.21.7 74 47-130
2-Methylphenol(o-Cresol)mg/kg 1.11.7 68 42-130
2-Nitroaniline mg/kg 2.53.3 76 41-130
2-Nitrophenol mg/kg 1.21.7 73 48-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.11.7 67 39-130
3,3'-Dichlorobenzidine mg/kg 2.43.3 72 41-130
3-Nitroaniline mg/kg 2.13.3 63 37-130
4,6-Dinitro-2-methylphenol mg/kg 2.73.3 81 38-141
4-Bromophenylphenyl ether mg/kg 1.5 v11.7 89 47-130
4-Chloro-3-methylphenol mg/kg 2.73.3 83 44-130
4-Chloroaniline mg/kg 2.33.3 69 41-130
4-Chlorophenylphenyl ether mg/kg 1.51.7 89 45-130
4-Nitroaniline mg/kg 2.1 v23.3 63 42-130
4-Nitrophenol mg/kg 7.28.3 87 39-131
Acenaphthene mg/kg 1.21.7 75 49-130
Acenaphthylene mg/kg 1.31.7 78 50-130
Aniline mg/kg 0.951.7 58 38-130
Anthracene mg/kg 1.21.7 73 49-130
Benzo(a)anthracene mg/kg 1.31.7 81 51-130
Benzo(a)pyrene mg/kg 1.41.7 86 51-130
Benzo(b)fluoranthene mg/kg 1.31.7 81 49-130
Benzo(g,h,i)perylene mg/kg 1.11.7 69 48-140
Benzo(k)fluoranthene mg/kg 1.31.7 78 51-130
Benzoic Acid mg/kg 3.48.3 41 22-130
Benzyl alcohol mg/kg 2.43.3 73 43-130
bis(2-Chloroethoxy)methane mg/kg 1.21.7 71 43-130
bis(2-Chloroethyl) ether mg/kg 1.11.7 65 42-130
bis(2-Ethylhexyl)phthalate mg/kg 1.21.7 74 43-130
Butylbenzylphthalate mg/kg 1.21.7 74 44-131
Chrysene mg/kg 1.31.7 80 51-130
Di-n-butylphthalate mg/kg 1.21.7 71 46-130
Di-n-octylphthalate mg/kg 1.21.7 75 45-130
Dibenz(a,h)anthracene mg/kg 1.21.7 72 48-130
Dibenzofuran mg/kg 1.41.7 84 10-130
Diethylphthalate mg/kg 1.31.7 77 48-130
Dimethylphthalate mg/kg 1.31.7 76 48-130
Fluoranthene mg/kg 1.31.7 80 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799934LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.31.7 80 48-130
Hexachloro-1,3-butadiene mg/kg 1.3 v11.7 80 39-130
Hexachlorobenzene mg/kg 1.41.7 85 47-130
Hexachlorocyclopentadiene mg/kg 1.21.7 73 17-130
Hexachloroethane mg/kg 1.11.7 66 40-130
Indeno(1,2,3-cd)pyrene mg/kg 1.21.7 72 50-130
Isophorone mg/kg 1.21.7 73 41-130
N-Nitroso-di-n-propylamine mg/kg 1.31.7 76 36-130
N-Nitrosodimethylamine mg/kg 1.11.7 67 34-130
N-Nitrosodiphenylamine mg/kg 1.31.7 78 48-130
Naphthalene mg/kg 1.21.7 70 46-130
Nitrobenzene mg/kg 1.31.7 81 39-130
Pentachlorophenol mg/kg 2.43.3 72 42-130
Phenanthrene mg/kg 1.31.7 78 50-130
Phenol mg/kg 1.11.7 66 42-130
Pyrene mg/kg 1.41.7 84 50-130
Pyridine mg/kg 0.961.7 58 26-130
2,4,6-Tribromophenol (S)%80 10-131
2-Fluorobiphenyl (S)%75 10-130
2-Fluorophenol (S)%68 10-130
Nitrobenzene-d5 (S)%77 10-130
Phenol-d6 (S)%70 10-130
Terphenyl-d14 (S)%77 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92629052001
3799936SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
1-Methylnaphthalene mg/kg ND 30ND
2,2'-Oxybis(1-chloropropane)mg/kg ND v230ND
2,4,5-Trichlorophenol mg/kg ND 30ND
2,4,6-Trichlorophenol mg/kg ND 30ND
2,4-Dichlorophenol mg/kg ND 30ND
2,4-Dimethylphenol mg/kg ND 30ND
2,4-Dinitrophenol mg/kg ND 30ND
2,4-Dinitrotoluene mg/kg ND 30ND
2,6-Dinitrotoluene mg/kg ND 30ND
2-Chloronaphthalene mg/kg ND 30ND
2-Chlorophenol mg/kg ND 30ND
2-Methylnaphthalene mg/kg ND 30ND
2-Methylphenol(o-Cresol)mg/kg ND 30ND
2-Nitroaniline mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92629052001
3799936SAMPLE DUPLICATE:
2-Nitrophenol mg/kg ND 30ND
3&4-Methylphenol(m&p Cresol)mg/kg ND 30ND
3,3'-Dichlorobenzidine mg/kg ND 30ND
3-Nitroaniline mg/kg ND 30ND
4,6-Dinitro-2-methylphenol mg/kg ND 30ND
4-Bromophenylphenyl ether mg/kg ND 30ND
4-Chloro-3-methylphenol mg/kg ND 30ND
4-Chloroaniline mg/kg ND 30ND
4-Chlorophenylphenyl ether mg/kg ND 30ND
4-Nitroaniline mg/kg ND 30ND
4-Nitrophenol mg/kg ND 30ND
Acenaphthene mg/kg ND 30ND
Acenaphthylene mg/kg ND 30ND
Aniline mg/kg ND 30ND
Anthracene mg/kg ND 30ND
Benzo(a)anthracene mg/kg ND 30ND
Benzo(a)pyrene mg/kg ND 30ND
Benzo(b)fluoranthene mg/kg ND 30ND
Benzo(g,h,i)perylene mg/kg ND 30ND
Benzo(k)fluoranthene mg/kg ND 30ND
Benzoic Acid mg/kg ND 30ND
Benzyl alcohol mg/kg ND 30ND
bis(2-Chloroethoxy)methane mg/kg ND 30ND
bis(2-Chloroethyl) ether mg/kg ND 30ND
bis(2-Ethylhexyl)phthalate mg/kg ND 30ND
Butylbenzylphthalate mg/kg ND 30ND
Chrysene mg/kg ND 30ND
Di-n-butylphthalate mg/kg ND 30ND
Di-n-octylphthalate mg/kg ND 30ND
Dibenz(a,h)anthracene mg/kg ND 30ND
Dibenzofuran mg/kg ND 30ND
Diethylphthalate mg/kg ND 30ND
Dimethylphthalate mg/kg ND 30ND
Fluoranthene mg/kg ND 30ND
Fluorene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND v130ND
Hexachlorobenzene mg/kg ND 30ND
Hexachlorocyclopentadiene mg/kg ND 30ND
Hexachloroethane mg/kg ND 30ND
Indeno(1,2,3-cd)pyrene mg/kg ND 30ND
Isophorone mg/kg ND 30ND
N-Nitroso-di-n-propylamine mg/kg ND 30ND
N-Nitrosodimethylamine mg/kg ND 30ND
N-Nitrosodiphenylamine mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
Nitrobenzene mg/kg ND 30ND
Pentachlorophenol mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92629052001
3799936SAMPLE DUPLICATE:
Phenanthrene mg/kg ND 30ND
Phenol mg/kg ND 30ND
Pyrene mg/kg ND 30ND
Pyridine mg/kg ND 30ND
2,4,6-Tribromophenol (S)%6064
2-Fluorobiphenyl (S)%6256
2-Fluorophenol (S)%6451
Nitrobenzene-d5 (S)%7765
Phenol-d6 (S)%6351
Terphenyl-d14 (S)%6062
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729163
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92629957001
3797307SAMPLE DUPLICATE:
Percent Moisture %24.6 N222525.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92629995007
3797308SAMPLE DUPLICATE:
Percent Moisture %14.6 N2122516.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1941315
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3849123-1
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Matrix:Solid
AnalyzedMDL
Total Solids %0.00200 10/14/22 17:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3849123-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1541197-07
R3849123-3SAMPLE DUPLICATE:
Total Solids %70.8 0.777 1070.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1941157
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3849603-1
Associated Lab Samples:92630074001, 92630074002, 92630074003, 92630074004
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 10/17/22 10:550.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3849603-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.610.0 106 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3849603-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1545162-06
R3849603-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 20.0 99.5 75.0-12599.3 0.212 2020.0ND 19.9 19.9
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3849603-7MATRIX SPIKE SAMPLE:
MSSpike
Result
L1545162-06
Chromium, Hexavalent mg/kg 709631 112 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1544665-02
R3849603-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1545162-07
R3849603-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
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[phone]
Page 51 of 55
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92630074
S TRYON 17700-A
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
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Page 52 of 55
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92630074
S TRYON 17700-A
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92630074001 729759 730008SS-1 EPA 3050B EPA 6010D
92630074002 729759 730008SS-2 EPA 3050B EPA 6010D
92630074003 729759 730008SS-3 EPA 3050B EPA 6010D
92630074004 729759 730008SS-4 EPA 3050B EPA 6010D
92630074001 730046 730251SS-1 EPA 7471B EPA 7471B
92630074002 730046 730251SS-2 EPA 7471B EPA 7471B
92630074003 730046 730251SS-3 EPA 7471B EPA 7471B
92630074004 730046 730251SS-4 EPA 7471B EPA 7471B
92630074001 729746 730025SS-1 EPA 3546 EPA 8270E
92630074002 729746 730025SS-2 EPA 3546 EPA 8270E
92630074003 729746 730025SS-3 EPA 3546 EPA 8270E
92630074004 729746 730025SS-4 EPA 3546 EPA 8270E
92630074001 730403 730407SS-1 EPA 5035A/5030B EPA 8260D
92630074002 730115 730364SS-2 EPA 5035A/5030B EPA 8260D
92630074003 730115 730364SS-3 EPA 5035A/5030B EPA 8260D
92630074004 730115 730364SS-4 EPA 5035A/5030B EPA 8260D
92630074001 729163SS-1 SW-846
92630074002 729163SS-2 SW-846
92630074003 729163SS-3 SW-846
92630074004 729163SS-4 SW-846
92630074001 1941315 1941315SS-1 SM 2540 G SM 2540G
92630074002 1941315 1941315SS-2 SM 2540 G SM 2540G
92630074003 1941315 1941315SS-3 SM 2540 G SM 2540G
92630074004 1941315 1941315SS-4 SM 2540 G SM 2540G
92630074001 1941157 1941157SS-1 3060A EPA 7199
92630074002 1941157 1941157SS-2 3060A EPA 7199
92630074003 1941157 1941157SS-3 3060A EPA 7199
92630074004 1941157 1941157SS-4 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 01:47 PM
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Page 53 of 55
Page 54 of 55
Page 55 of 55
#=CL#
October 21, 2022
LIMS USE: FR - SCOTT YOUNG
LIMS OBJECT ID: 92630198
92630198
Project:
Pace Project No.:
RE:
Scott Young
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
TWO VACANT PARCELS/SOUTH TRYON
Dear Scott Young:
Enclosed are the analytical results for sample(s) received by the laboratory on October 10, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sara Poulson
[e-mail]
Project Manager
[phone]
Enclosures
cc:ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 67
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
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A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
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South Carolina Laboratory ID: 99006
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Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
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North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 67
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Lab ID Sample ID Matrix Date Collected Date Received
92630198001 GW-1 Water 10/07/22 10:10 10/10/22 08:17
92630198002 GW-2 Water 10/07/22 10:50 10/10/22 08:17
92630198003 GW-3 Water 10/07/22 11:50 10/10/22 08:17
92630198004 GW-4 Water 10/07/22 13:15 10/10/22 08:17
92630198005 GW-5 Water 10/07/22 14:00 10/10/22 08:17
92630198006 GW-6 Water 10/07/22 14:45 10/10/22 08:17
92630198007 GW-7 Water 10/07/22 15:30 10/10/22 08:17
92630198008 GW-8 Water 10/07/22 16:30 10/10/22 08:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Page 3 of 67
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92630198001 GW-1 EPA 6010D 7 PASI-GAKH
EPA 6010D 7 PASI-GAKH
EPA 7470A 1 PASI-GAVB
EPA 7470A 1 PASI-GAVB
EPA 8270E 75 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANARD
92630198002 GW-2 EPA 6010D 7 PASI-GAKH
EPA 6010D 7 PASI-GAKH
EPA 7470A 1 PASI-GAVB
EPA 7470A 1 PASI-GAVB
EPA 8270E 75 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANARD
92630198003 GW-3 EPA 6010D 7 PASI-GAKH
EPA 6010D 7 PASI-GAKH
EPA 7470A 1 PASI-GAVB
EPA 7470A 1 PASI-GAVB
EPA 8270E 75 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANARD
92630198004 GW-4 EPA 6010D 7 PASI-GAKH
EPA 6010D 7 PASI-GAKH
EPA 7470A 1 PASI-GAVB
EPA 7470A 1 PASI-GAVB
EPA 8270E 75 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANARD
92630198005 GW-5 EPA 6010D 7 PASI-GAKH
EPA 6010D 7 PASI-GAKH
EPA 7470A 1 PASI-GAVB
EPA 7470A 1 PASI-GAVB
EPA 8270E 75 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANARD
92630198006 GW-6 EPA 6010D 7 PASI-GAKH
EPA 6010D 7 PASI-GAKH
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
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[phone]
Page 4 of 67
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7470A 1 PASI-GAVB
EPA 7470A 1 PASI-GAVB
EPA 8270E 75 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANARD
92630198007 GW-7 EPA 6010D 7 PASI-GAKH
EPA 6010D 7 PASI-GAKH
EPA 7470A 1 PASI-GAVB
EPA 7470A 1 PASI-GAVB
EPA 8270E 75 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANARD
92630198008 GW-8 EPA 6010D 7 PASI-GAKH
EPA 6010D 7 PASI-GAKH
EPA 7470A 1 PASI-GAVB
EPA 7470A 1 PASI-GAVB
EPA 8270E 75 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANARD
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 5 of 67
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92630198001 GW-1
Barium 123 ug/L 10/13/22 20:2910.0EPA 6010D
Chromium 3.7J ug/L 10/13/22 20:2910.0EPA 6010D
Lead 23.4 ug/L 10/13/22 20:2920.0EPA 6010D
Barium, Dissolved 28.6 ug/L 10/14/22 19:0810.0EPA 6010D
Chromium, Hexavalent 0.776 ug/L 10/19/22 09:070.500EPA 7199
92630198002 GW-2
Barium 1480 ug/L 10/13/22 20:4810.0EPA 6010D
Chromium 42.3 ug/L 10/13/22 20:4810.0EPA 6010D
Lead 94.5 ug/L 10/13/22 20:4820.0EPA 6010D
Barium, Dissolved 58.4 ug/L 10/14/22 19:1310.0EPA 6010D
Chromium, Hexavalent 0.165J ug/L 10/19/22 09:15 J0.500EPA 7199
92630198003 GW-3
Barium 784 ug/L 10/13/22 20:5310.0EPA 6010D
Chromium 17.9 ug/L 10/13/22 20:5310.0EPA 6010D
Lead 61.8 ug/L 10/13/22 20:5320.0EPA 6010D
Barium, Dissolved 45.9 ug/L 10/14/22 19:1810.0EPA 6010D
92630198004 GW-4
Barium 271 ug/L 10/13/22 20:5710.0EPA 6010D
Chromium 11.5 ug/L 10/13/22 20:5710.0EPA 6010D
Lead 199 ug/L 10/13/22 20:5720.0EPA 6010D
Barium, Dissolved 41.2 ug/L 10/14/22 19:3210.0EPA 6010D
92630198005 GW-5
Barium 88.7 ug/L 10/13/22 21:1210.0EPA 6010D
Barium, Dissolved 52.2 ug/L 10/14/22 19:3710.0EPA 6010D
92630198006 GW-6
Barium 80.5 ug/L 10/13/22 21:1610.0EPA 6010D
Barium, Dissolved 59.8 ug/L 10/14/22 19:4110.0EPA 6010D
92630198007 GW-7
Barium 143 ug/L 10/13/22 21:2110.0EPA 6010D
Barium, Dissolved 66.2 ug/L 10/14/22 19:4610.0EPA 6010D
92630198008 GW-8
Barium 499 ug/L 10/13/22 21:2610.0EPA 6010D
Chromium 10.6 ug/L 10/13/22 21:2610.0EPA 6010D
Lead 37.4 ug/L 10/13/22 21:2620.0EPA 6010D
Barium, Dissolved 62.7 ug/L 10/14/22 19:5110.0EPA 6010D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 6 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-1 Lab ID:92630198001 Collected:10/07/22 10:10 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND ug/L 10/13/22 20:29 7440-38-210/13/22 15:1430.0 26.2 1
Barium 123 ug/L 10/13/22 20:29 7440-39-310/13/22 15:1410.0 1.3 1
Cadmium ND ug/L 10/13/22 20:29 7440-43-910/13/22 15:1410.0 2.7 1
Chromium 3.7J ug/L 10/13/22 20:29 7440-47-310/13/22 15:1410.0 3.6 1
Silver ND ug/L 10/13/22 20:29 7440-22-410/13/22 15:1410.0 4.6 1
Lead 23.4 ug/L 10/13/22 20:29 7439-92-110/13/22 15:1420.0 19.0 1
Selenium ND ug/L 10/13/22 20:29 7782-49-210/13/22 15:1440.0 31.1 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010 MET ICP, Dissolved
Arsenic, Dissolved ND ug/L 10/14/22 19:08 7440-38-210/14/22 10:5830.0 26.2 1
Barium, Dissolved 28.6 ug/L 10/14/22 19:08 7440-39-310/14/22 10:5810.0 1.3 1
Cadmium, Dissolved ND ug/L 10/14/22 19:08 7440-43-910/14/22 10:5810.0 2.7 1
Chromium, Dissolved ND ug/L 10/14/22 19:08 7440-47-310/14/22 10:5810.0 3.6 1
Lead, Dissolved ND ug/L 10/14/22 19:08 7439-92-110/14/22 10:5820.0 19.0 1
Selenium, Dissolved ND ug/L 10/14/22 19:08 7782-49-210/14/22 10:5840.0 31.1 1
Silver, Dissolved ND ug/L 10/14/22 19:08 7440-22-410/14/22 10:5810.0 4.6 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 10/18/22 09:53 7439-97-610/17/22 16:050.20 0.13 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/17/22 15:15 7439-97-6 M110/17/22 14:100.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 10/13/22 20:59 83-32-910/12/22 16:179.1 1.8 1
Acenaphthylene ND ug/L 10/13/22 20:59 208-96-810/12/22 16:179.1 1.8 1
Aniline ND ug/L 10/13/22 20:59 62-53-310/12/22 16:179.1 1.5 1
Anthracene ND ug/L 10/13/22 20:59 120-12-710/12/22 16:179.1 2.1 1
Benzo(a)anthracene ND ug/L 10/13/22 20:59 56-55-310/12/22 16:179.1 2.4 1
Benzo(a)pyrene ND ug/L 10/13/22 20:59 50-32-810/12/22 16:179.1 2.5 1
Benzo(b)fluoranthene ND ug/L 10/13/22 20:59 205-99-210/12/22 16:179.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 10/13/22 20:59 191-24-210/12/22 16:179.1 2.6 1
Benzo(k)fluoranthene ND ug/L 10/13/22 20:59 207-08-910/12/22 16:179.1 2.5 1
Benzoic Acid ND ug/L 10/13/22 20:59 65-85-010/12/22 16:1745.5 20.0 1
Benzyl alcohol ND ug/L 10/13/22 20:59 100-51-610/12/22 16:1718.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 10/13/22 20:59 101-55-310/12/22 16:179.1 1.6 1
Butylbenzylphthalate ND ug/L 10/13/22 20:59 85-68-710/12/22 16:179.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 10/13/22 20:59 59-50-710/12/22 16:179.1 3.0 1
4-Chloroaniline ND ug/L 10/13/22 20:59 106-47-810/12/22 16:1718.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 10/13/22 20:59 111-91-110/12/22 16:179.1 1.7 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
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Page 7 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-1 Lab ID:92630198001 Collected:10/07/22 10:10 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
bis(2-Chloroethyl) ether ND ug/L 10/13/22 20:59 111-44-410/12/22 16:179.1 1.7 1
2-Chloronaphthalene ND ug/L 10/13/22 20:59 91-58-710/12/22 16:179.1 1.6 1
2-Chlorophenol ND ug/L 10/13/22 20:59 95-57-810/12/22 16:179.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 10/13/22 20:59 7005-72-310/12/22 16:179.1 1.8 1
Chrysene ND ug/L 10/13/22 20:59 218-01-910/12/22 16:179.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 10/13/22 20:59 53-70-310/12/22 16:179.1 2.7 1
Dibenzofuran ND ug/L 10/13/22 20:59 132-64-910/12/22 16:179.1 1.9 1
1,2-Dichlorobenzene ND ug/L 10/13/22 20:59 95-50-110/12/22 16:179.1 1.6 1
1,3-Dichlorobenzene ND ug/L 10/13/22 20:59 541-73-110/12/22 16:179.1 1.5 1
1,4-Dichlorobenzene ND ug/L 10/13/22 20:59 106-46-710/12/22 16:179.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 10/13/22 20:59 91-94-110/12/22 16:1718.2 7.4 1
2,4-Dichlorophenol ND ug/L 10/13/22 20:59 120-83-210/12/22 16:179.1 1.3 1
Diethylphthalate ND ug/L 10/13/22 20:59 84-66-210/12/22 16:179.1 1.9 1
2,4-Dimethylphenol ND ug/L 10/13/22 20:59 105-67-910/12/22 16:179.1 1.5 1
Dimethylphthalate ND ug/L 10/13/22 20:59 131-11-310/12/22 16:179.1 1.9 1
Di-n-butylphthalate ND ug/L 10/13/22 20:59 84-74-210/12/22 16:179.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 10/13/22 20:59 534-52-110/12/22 16:1718.2 7.1 1
2,4-Dinitrophenol ND ug/L 10/13/22 20:59 51-28-510/12/22 16:1745.5 23.6 1
2,4-Dinitrotoluene ND ug/L 10/13/22 20:59 121-14-210/12/22 16:179.1 1.5 1
2,6-Dinitrotoluene ND ug/L 10/13/22 20:59 606-20-210/12/22 16:179.1 1.6 1
Di-n-octylphthalate ND ug/L 10/13/22 20:59 117-84-010/12/22 16:179.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/13/22 20:59 117-81-710/12/22 16:175.5 3.4 1
Fluoranthene ND ug/L 10/13/22 20:59 206-44-010/12/22 16:179.1 2.0 1
Fluorene ND ug/L 10/13/22 20:59 86-73-710/12/22 16:179.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 20:59 87-68-310/12/22 16:179.1 1.6 1
Hexachlorobenzene ND ug/L 10/13/22 20:59 118-74-110/12/22 16:179.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 10/13/22 20:59 77-47-410/12/22 16:179.1 1.4 1
Hexachloroethane ND ug/L 10/13/22 20:59 67-72-110/12/22 16:179.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/13/22 20:59 193-39-510/12/22 16:179.1 2.6 1
Isophorone ND ug/L 10/13/22 20:59 78-59-110/12/22 16:179.1 1.5 1
1-Methylnaphthalene ND ug/L 10/13/22 20:59 90-12-010/12/22 16:179.1 1.8 1
2-Methylnaphthalene ND ug/L 10/13/22 20:59 91-57-610/12/22 16:179.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 10/13/22 20:59 95-48-710/12/22 16:179.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/13/22 20:59 15831-10-410/12/22 16:179.1 1.1 1
Naphthalene ND ug/L 10/13/22 20:59 91-20-310/12/22 16:179.1 1.9 1
2-Nitroaniline ND ug/L 10/13/22 20:59 88-74-410/12/22 16:1718.2 2.7 1
3-Nitroaniline ND ug/L 10/13/22 20:59 99-09-210/12/22 16:1718.2 3.4 1
4-Nitroaniline ND ug/L 10/13/22 20:59 100-01-610/12/22 16:1718.2 4.6 1
Nitrobenzene ND ug/L 10/13/22 20:59 98-95-310/12/22 16:179.1 1.7 1
2-Nitrophenol ND ug/L 10/13/22 20:59 88-75-510/12/22 16:179.1 1.3 1
4-Nitrophenol ND ug/L 10/13/22 20:59 100-02-710/12/22 16:1745.5 6.0 1
N-Nitrosodimethylamine ND ug/L 10/13/22 20:59 62-75-910/12/22 16:179.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 10/13/22 20:59 621-64-710/12/22 16:179.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 10/13/22 20:59 86-30-610/12/22 16:179.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/13/22 20:59 108-60-1 v110/12/22 16:179.1 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-1 Lab ID:92630198001 Collected:10/07/22 10:10 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Pentachlorophenol ND ug/L 10/13/22 20:59 87-86-510/12/22 16:1718.2 3.4 1
Phenanthrene ND ug/L 10/13/22 20:59 85-01-810/12/22 16:179.1 1.8 1
Phenol ND ug/L 10/13/22 20:59 108-95-210/12/22 16:179.1 1.2 1
Pyrene ND ug/L 10/13/22 20:59 129-00-010/12/22 16:179.1 2.0 1
Pyridine ND ug/L 10/13/22 20:59 110-86-110/12/22 16:179.1 2.4 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 20:59 120-82-110/12/22 16:179.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 10/13/22 20:59 95-95-410/12/22 16:179.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 10/13/22 20:59 88-06-210/12/22 16:179.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)15 %10/13/22 20:59 4165-60-010/12/22 16:1710-144 1
2-Fluorobiphenyl (S)6 %10/13/22 20:59 321-60-8 S010/12/22 16:1710-130 1
Terphenyl-d14 (S)111 %10/13/22 20:59 1718-51-010/12/22 16:1734-163 1
Phenol-d6 (S)10 %10/13/22 20:59 13127-88-310/12/22 16:1710-130 1
2-Fluorophenol (S)11 %10/13/22 20:59 367-12-410/12/22 16:1710-130 1
2,4,6-Tribromophenol (S)67 %10/13/22 20:59 118-79-610/12/22 16:1710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/13/22 20:29 67-64-125.0 5.1 1
Benzene ND ug/L 10/13/22 20:29 71-43-21.0 0.34 1
Bromobenzene ND ug/L 10/13/22 20:29 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 10/13/22 20:29 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/13/22 20:29 75-27-41.0 0.31 1
Bromoform ND ug/L 10/13/22 20:29 75-25-2 IK1.0 0.34 1
Bromomethane ND ug/L 10/13/22 20:29 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/13/22 20:29 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 10/13/22 20:29 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/13/22 20:29 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/13/22 20:29 75-00-31.0 0.65 1
Chloroform ND ug/L 10/13/22 20:29 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/13/22 20:29 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/13/22 20:29 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 10/13/22 20:29 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/22 20:29 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/13/22 20:29 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/22 20:29 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/13/22 20:29 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/13/22 20:29 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/13/22 20:29 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/13/22 20:29 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/13/22 20:29 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/13/22 20:29 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/13/22 20:29 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/13/22 20:29 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/13/22 20:29 156-59-21.0 0.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-1 Lab ID:92630198001 Collected:10/07/22 10:10 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
trans-1,2-Dichloroethene ND ug/L 10/13/22 20:29 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/13/22 20:29 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 10/13/22 20:29 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 10/13/22 20:29 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 10/13/22 20:29 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/13/22 20:29 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/13/22 20:29 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 10/13/22 20:29 108-20-3 IK1.0 0.31 1
Ethylbenzene ND ug/L 10/13/22 20:29 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 20:29 87-68-32.0 1.5 1
2-Hexanone ND ug/L 10/13/22 20:29 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 10/13/22 20:29 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 10/13/22 20:29 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/22 20:29 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/13/22 20:29 1634-04-41.0 0.42 1
Naphthalene ND ug/L 10/13/22 20:29 91-20-31.0 0.64 1
Styrene ND ug/L 10/13/22 20:29 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/22 20:29 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/22 20:29 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/13/22 20:29 127-18-41.0 0.29 1
Toluene ND ug/L 10/13/22 20:29 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/13/22 20:29 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 20:29 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/13/22 20:29 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/13/22 20:29 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/13/22 20:29 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/13/22 20:29 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/13/22 20:29 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/13/22 20:29 108-05-4 IK2.0 1.3 1
Vinyl chloride ND ug/L 10/13/22 20:29 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/13/22 20:29 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 10/13/22 20:29 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/13/22 20:29 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)91 %10/13/22 20:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)86 %10/13/22 20:29 17060-07-070-130 1
Toluene-d8 (S)111 %10/13/22 20:29 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.776 ug/L 10/19/22 09:07 18540-29-910/19/22 09:070.500 0.150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-2 Lab ID:92630198002 Collected:10/07/22 10:50 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND ug/L 10/13/22 20:48 7440-38-210/13/22 15:1430.0 26.2 1
Barium 1480 ug/L 10/13/22 20:48 7440-39-310/13/22 15:1410.0 1.3 1
Cadmium ND ug/L 10/13/22 20:48 7440-43-910/13/22 15:1410.0 2.7 1
Chromium 42.3 ug/L 10/13/22 20:48 7440-47-310/13/22 15:1410.0 3.6 1
Silver ND ug/L 10/13/22 20:48 7440-22-410/13/22 15:1410.0 4.6 1
Lead 94.5 ug/L 10/13/22 20:48 7439-92-110/13/22 15:1420.0 19.0 1
Selenium ND ug/L 10/13/22 20:48 7782-49-210/13/22 15:1440.0 31.1 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010 MET ICP, Dissolved
Arsenic, Dissolved ND ug/L 10/14/22 19:13 7440-38-210/14/22 10:5830.0 26.2 1
Barium, Dissolved 58.4 ug/L 10/14/22 19:13 7440-39-310/14/22 10:5810.0 1.3 1
Cadmium, Dissolved ND ug/L 10/14/22 19:13 7440-43-910/14/22 10:5810.0 2.7 1
Chromium, Dissolved ND ug/L 10/14/22 19:13 7440-47-310/14/22 10:5810.0 3.6 1
Lead, Dissolved ND ug/L 10/14/22 19:13 7439-92-110/14/22 10:5820.0 19.0 1
Selenium, Dissolved ND ug/L 10/14/22 19:13 7782-49-210/14/22 10:5840.0 31.1 1
Silver, Dissolved ND ug/L 10/14/22 19:13 7440-22-410/14/22 10:5810.0 4.6 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 10/18/22 09:56 7439-97-610/17/22 16:050.20 0.13 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/17/22 15:26 7439-97-610/17/22 14:100.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 10/14/22 18:10 83-32-9 L110/14/22 13:419.1 1.8 1
Acenaphthylene ND ug/L 10/14/22 18:10 208-96-8 L110/14/22 13:419.1 1.8 1
Aniline ND ug/L 10/14/22 18:10 62-53-310/14/22 13:419.1 1.5 1
Anthracene ND ug/L 10/14/22 18:10 120-12-710/14/22 13:419.1 2.1 1
Benzo(a)anthracene ND ug/L 10/14/22 18:10 56-55-3 L110/14/22 13:419.1 2.4 1
Benzo(a)pyrene ND ug/L 10/14/22 18:10 50-32-810/14/22 13:419.1 2.5 1
Benzo(b)fluoranthene ND ug/L 10/14/22 18:10 205-99-2 L110/14/22 13:419.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 10/14/22 18:10 191-24-2 L110/14/22 13:419.1 2.6 1
Benzo(k)fluoranthene ND ug/L 10/14/22 18:10 207-08-910/14/22 13:419.1 2.5 1
Benzoic Acid ND ug/L 10/14/22 18:10 65-85-0 v110/14/22 13:4145.5 20.0 1
Benzyl alcohol ND ug/L 10/14/22 18:10 100-51-610/14/22 13:4118.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 10/14/22 18:10 101-55-3 L110/14/22 13:419.1 1.6 1
Butylbenzylphthalate ND ug/L 10/14/22 18:10 85-68-7 L110/14/22 13:419.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 10/14/22 18:10 59-50-710/14/22 13:419.1 3.0 1
4-Chloroaniline ND ug/L 10/14/22 18:10 106-47-810/14/22 13:4118.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 10/14/22 18:10 111-91-110/14/22 13:419.1 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-2 Lab ID:92630198002 Collected:10/07/22 10:50 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
bis(2-Chloroethyl) ether ND ug/L 10/14/22 18:10 111-44-410/14/22 13:419.1 1.7 1
2-Chloronaphthalene ND ug/L 10/14/22 18:10 91-58-7 L110/14/22 13:419.1 1.6 1
2-Chlorophenol ND ug/L 10/14/22 18:10 95-57-810/14/22 13:419.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 10/14/22 18:10 7005-72-310/14/22 13:419.1 1.8 1
Chrysene ND ug/L 10/14/22 18:10 218-01-9 L110/14/22 13:419.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 10/14/22 18:10 53-70-3 L110/14/22 13:419.1 2.7 1
Dibenzofuran ND ug/L 10/14/22 18:10 132-64-9 L110/14/22 13:419.1 1.9 1
1,2-Dichlorobenzene ND ug/L 10/14/22 18:10 95-50-110/14/22 13:419.1 1.6 1
1,3-Dichlorobenzene ND ug/L 10/14/22 18:10 541-73-110/14/22 13:419.1 1.5 1
1,4-Dichlorobenzene ND ug/L 10/14/22 18:10 106-46-710/14/22 13:419.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 10/14/22 18:10 91-94-1 L110/14/22 13:4118.2 7.4 1
2,4-Dichlorophenol ND ug/L 10/14/22 18:10 120-83-210/14/22 13:419.1 1.3 1
Diethylphthalate ND ug/L 10/14/22 18:10 84-66-2 L110/14/22 13:419.1 1.9 1
2,4-Dimethylphenol ND ug/L 10/14/22 18:10 105-67-9 L110/14/22 13:419.1 1.5 1
Dimethylphthalate ND ug/L 10/14/22 18:10 131-11-3 L110/14/22 13:419.1 1.9 1
Di-n-butylphthalate ND ug/L 10/14/22 18:10 84-74-2 L110/14/22 13:419.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 10/14/22 18:10 534-52-110/14/22 13:4118.2 7.1 1
2,4-Dinitrophenol ND ug/L 10/14/22 18:10 51-28-510/14/22 13:4145.5 23.6 1
2,4-Dinitrotoluene ND ug/L 10/14/22 18:10 121-14-2 L110/14/22 13:419.1 1.5 1
2,6-Dinitrotoluene ND ug/L 10/14/22 18:10 606-20-2 L110/14/22 13:419.1 1.6 1
Di-n-octylphthalate ND ug/L 10/14/22 18:10 117-84-0 v110/14/22 13:419.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/14/22 18:10 117-81-710/14/22 13:415.5 3.4 1
Fluoranthene ND ug/L 10/14/22 18:10 206-44-010/14/22 13:419.1 2.0 1
Fluorene ND ug/L 10/14/22 18:10 86-73-710/14/22 13:419.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 10/14/22 18:10 87-68-310/14/22 13:419.1 1.6 1
Hexachlorobenzene ND ug/L 10/14/22 18:10 118-74-1 L110/14/22 13:419.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 10/14/22 18:10 77-47-4 L110/14/22 13:419.1 1.4 1
Hexachloroethane ND ug/L 10/14/22 18:10 67-72-110/14/22 13:419.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/14/22 18:10 193-39-5 L110/14/22 13:419.1 2.6 1
Isophorone ND ug/L 10/14/22 18:10 78-59-1 L110/14/22 13:419.1 1.5 1
1-Methylnaphthalene ND ug/L 10/14/22 18:10 90-12-010/14/22 13:419.1 1.8 1
2-Methylnaphthalene ND ug/L 10/14/22 18:10 91-57-610/14/22 13:419.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 10/14/22 18:10 95-48-710/14/22 13:419.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/14/22 18:10 15831-10-410/14/22 13:419.1 1.1 1
Naphthalene ND ug/L 10/14/22 18:10 91-20-310/14/22 13:419.1 1.9 1
2-Nitroaniline ND ug/L 10/14/22 18:10 88-74-4 L110/14/22 13:4118.2 2.7 1
3-Nitroaniline ND ug/L 10/14/22 18:10 99-09-2 L110/14/22 13:4118.2 3.4 1
4-Nitroaniline ND ug/L 10/14/22 18:10 100-01-6 L110/14/22 13:4118.2 4.6 1
Nitrobenzene ND ug/L 10/14/22 18:10 98-95-3 L110/14/22 13:419.1 1.7 1
2-Nitrophenol ND ug/L 10/14/22 18:10 88-75-5 L110/14/22 13:419.1 1.3 1
4-Nitrophenol ND ug/L 10/14/22 18:10 100-02-710/14/22 13:4145.5 6.0 1
N-Nitrosodimethylamine ND ug/L 10/14/22 18:10 62-75-910/14/22 13:419.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 10/14/22 18:10 621-64-710/14/22 13:419.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 10/14/22 18:10 86-30-6 L110/14/22 13:419.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/14/22 18:10 108-60-1 v110/14/22 13:419.1 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-2 Lab ID:92630198002 Collected:10/07/22 10:50 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Pentachlorophenol ND ug/L 10/14/22 18:10 87-86-510/14/22 13:4118.2 3.4 1
Phenanthrene ND ug/L 10/14/22 18:10 85-01-8 L110/14/22 13:419.1 1.8 1
Phenol ND ug/L 10/14/22 18:10 108-95-210/14/22 13:419.1 1.2 1
Pyrene ND ug/L 10/14/22 18:10 129-00-0 L110/14/22 13:419.1 2.0 1
Pyridine ND ug/L 10/14/22 18:10 110-86-110/14/22 13:419.1 2.4 1
1,2,4-Trichlorobenzene ND ug/L 10/14/22 18:10 120-82-110/14/22 13:419.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 10/14/22 18:10 95-95-4 L110/14/22 13:419.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 10/14/22 18:10 88-06-2 L110/14/22 13:419.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)34 %10/14/22 18:10 4165-60-010/14/22 13:4110-144 1
2-Fluorobiphenyl (S)18 %10/14/22 18:10 321-60-810/14/22 13:4110-130 1
Terphenyl-d14 (S)67 %10/14/22 18:10 1718-51-010/14/22 13:4134-163 1
Phenol-d6 (S)19 %10/14/22 18:10 13127-88-310/14/22 13:4110-130 1
2-Fluorophenol (S)22 %10/14/22 18:10 367-12-410/14/22 13:4110-130 1
2,4,6-Tribromophenol (S)39 %10/14/22 18:10 118-79-610/14/22 13:4110-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/13/22 20:47 67-64-125.0 5.1 1
Benzene ND ug/L 10/13/22 20:47 71-43-21.0 0.34 1
Bromobenzene ND ug/L 10/13/22 20:47 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 10/13/22 20:47 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/13/22 20:47 75-27-41.0 0.31 1
Bromoform ND ug/L 10/13/22 20:47 75-25-2 IK1.0 0.34 1
Bromomethane ND ug/L 10/13/22 20:47 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/13/22 20:47 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 10/13/22 20:47 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/13/22 20:47 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/13/22 20:47 75-00-31.0 0.65 1
Chloroform ND ug/L 10/13/22 20:47 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/13/22 20:47 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/13/22 20:47 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 10/13/22 20:47 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/22 20:47 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/13/22 20:47 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/22 20:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/13/22 20:47 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/13/22 20:47 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/13/22 20:47 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/13/22 20:47 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/13/22 20:47 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/13/22 20:47 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/13/22 20:47 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/13/22 20:47 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/13/22 20:47 156-59-21.0 0.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-2 Lab ID:92630198002 Collected:10/07/22 10:50 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
trans-1,2-Dichloroethene ND ug/L 10/13/22 20:47 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/13/22 20:47 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 10/13/22 20:47 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 10/13/22 20:47 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 10/13/22 20:47 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/13/22 20:47 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/13/22 20:47 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 10/13/22 20:47 108-20-3 IK1.0 0.31 1
Ethylbenzene ND ug/L 10/13/22 20:47 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 20:47 87-68-32.0 1.5 1
2-Hexanone ND ug/L 10/13/22 20:47 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 10/13/22 20:47 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 10/13/22 20:47 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/22 20:47 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/13/22 20:47 1634-04-41.0 0.42 1
Naphthalene ND ug/L 10/13/22 20:47 91-20-31.0 0.64 1
Styrene ND ug/L 10/13/22 20:47 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/22 20:47 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/22 20:47 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/13/22 20:47 127-18-41.0 0.29 1
Toluene ND ug/L 10/13/22 20:47 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/13/22 20:47 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 20:47 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/13/22 20:47 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/13/22 20:47 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/13/22 20:47 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/13/22 20:47 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/13/22 20:47 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/13/22 20:47 108-05-4 IK2.0 1.3 1
Vinyl chloride ND ug/L 10/13/22 20:47 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/13/22 20:47 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 10/13/22 20:47 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/13/22 20:47 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)89 %10/13/22 20:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %10/13/22 20:47 17060-07-070-130 1
Toluene-d8 (S)110 %10/13/22 20:47 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.165J ug/L 10/19/22 09:15 18540-29-9 J10/19/22 09:150.500 0.150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-3 Lab ID:92630198003 Collected:10/07/22 11:50 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND ug/L 10/13/22 20:53 7440-38-210/13/22 15:1430.0 26.2 1
Barium 784 ug/L 10/13/22 20:53 7440-39-310/13/22 15:1410.0 1.3 1
Cadmium ND ug/L 10/13/22 20:53 7440-43-910/13/22 15:1410.0 2.7 1
Chromium 17.9 ug/L 10/13/22 20:53 7440-47-310/13/22 15:1410.0 3.6 1
Silver ND ug/L 10/13/22 20:53 7440-22-410/13/22 15:1410.0 4.6 1
Lead 61.8 ug/L 10/13/22 20:53 7439-92-110/13/22 15:1420.0 19.0 1
Selenium ND ug/L 10/13/22 20:53 7782-49-210/13/22 15:1440.0 31.1 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010 MET ICP, Dissolved
Arsenic, Dissolved ND ug/L 10/14/22 19:18 7440-38-210/14/22 10:5830.0 26.2 1
Barium, Dissolved 45.9 ug/L 10/14/22 19:18 7440-39-310/14/22 10:5810.0 1.3 1
Cadmium, Dissolved ND ug/L 10/14/22 19:18 7440-43-910/14/22 10:5810.0 2.7 1
Chromium, Dissolved ND ug/L 10/14/22 19:18 7440-47-310/14/22 10:5810.0 3.6 1
Lead, Dissolved ND ug/L 10/14/22 19:18 7439-92-110/14/22 10:5820.0 19.0 1
Selenium, Dissolved ND ug/L 10/14/22 19:18 7782-49-210/14/22 10:5840.0 31.1 1
Silver, Dissolved ND ug/L 10/14/22 19:18 7440-22-410/14/22 10:5810.0 4.6 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 10/18/22 09:59 7439-97-610/17/22 16:050.20 0.13 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/17/22 15:29 7439-97-610/17/22 14:100.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 10/13/22 21:51 83-32-910/12/22 16:179.1 1.8 1
Acenaphthylene ND ug/L 10/13/22 21:51 208-96-810/12/22 16:179.1 1.8 1
Aniline ND ug/L 10/13/22 21:51 62-53-310/12/22 16:179.1 1.5 1
Anthracene ND ug/L 10/13/22 21:51 120-12-710/12/22 16:179.1 2.1 1
Benzo(a)anthracene ND ug/L 10/13/22 21:51 56-55-310/12/22 16:179.1 2.4 1
Benzo(a)pyrene ND ug/L 10/13/22 21:51 50-32-810/12/22 16:179.1 2.5 1
Benzo(b)fluoranthene ND ug/L 10/13/22 21:51 205-99-210/12/22 16:179.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 10/13/22 21:51 191-24-210/12/22 16:179.1 2.6 1
Benzo(k)fluoranthene ND ug/L 10/13/22 21:51 207-08-910/12/22 16:179.1 2.5 1
Benzoic Acid ND ug/L 10/13/22 21:51 65-85-010/12/22 16:1745.5 20.0 1
Benzyl alcohol ND ug/L 10/13/22 21:51 100-51-610/12/22 16:1718.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 10/13/22 21:51 101-55-310/12/22 16:179.1 1.6 1
Butylbenzylphthalate ND ug/L 10/13/22 21:51 85-68-710/12/22 16:179.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 10/13/22 21:51 59-50-710/12/22 16:179.1 3.0 1
4-Chloroaniline ND ug/L 10/13/22 21:51 106-47-810/12/22 16:1718.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 10/13/22 21:51 111-91-110/12/22 16:179.1 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-3 Lab ID:92630198003 Collected:10/07/22 11:50 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
bis(2-Chloroethyl) ether ND ug/L 10/13/22 21:51 111-44-410/12/22 16:179.1 1.7 1
2-Chloronaphthalene ND ug/L 10/13/22 21:51 91-58-710/12/22 16:179.1 1.6 1
2-Chlorophenol ND ug/L 10/13/22 21:51 95-57-810/12/22 16:179.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 10/13/22 21:51 7005-72-310/12/22 16:179.1 1.8 1
Chrysene ND ug/L 10/13/22 21:51 218-01-910/12/22 16:179.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 10/13/22 21:51 53-70-310/12/22 16:179.1 2.7 1
Dibenzofuran ND ug/L 10/13/22 21:51 132-64-910/12/22 16:179.1 1.9 1
1,2-Dichlorobenzene ND ug/L 10/13/22 21:51 95-50-110/12/22 16:179.1 1.6 1
1,3-Dichlorobenzene ND ug/L 10/13/22 21:51 541-73-110/12/22 16:179.1 1.5 1
1,4-Dichlorobenzene ND ug/L 10/13/22 21:51 106-46-710/12/22 16:179.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 10/13/22 21:51 91-94-110/12/22 16:1718.2 7.4 1
2,4-Dichlorophenol ND ug/L 10/13/22 21:51 120-83-210/12/22 16:179.1 1.3 1
Diethylphthalate ND ug/L 10/13/22 21:51 84-66-210/12/22 16:179.1 1.9 1
2,4-Dimethylphenol ND ug/L 10/13/22 21:51 105-67-910/12/22 16:179.1 1.5 1
Dimethylphthalate ND ug/L 10/13/22 21:51 131-11-310/12/22 16:179.1 1.9 1
Di-n-butylphthalate ND ug/L 10/13/22 21:51 84-74-210/12/22 16:179.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 10/13/22 21:51 534-52-110/12/22 16:1718.2 7.1 1
2,4-Dinitrophenol ND ug/L 10/13/22 21:51 51-28-510/12/22 16:1745.5 23.6 1
2,4-Dinitrotoluene ND ug/L 10/13/22 21:51 121-14-210/12/22 16:179.1 1.5 1
2,6-Dinitrotoluene ND ug/L 10/13/22 21:51 606-20-210/12/22 16:179.1 1.6 1
Di-n-octylphthalate ND ug/L 10/13/22 21:51 117-84-010/12/22 16:179.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/13/22 21:51 117-81-710/12/22 16:175.5 3.4 1
Fluoranthene ND ug/L 10/13/22 21:51 206-44-010/12/22 16:179.1 2.0 1
Fluorene ND ug/L 10/13/22 21:51 86-73-710/12/22 16:179.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 21:51 87-68-310/12/22 16:179.1 1.6 1
Hexachlorobenzene ND ug/L 10/13/22 21:51 118-74-110/12/22 16:179.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 10/13/22 21:51 77-47-410/12/22 16:179.1 1.4 1
Hexachloroethane ND ug/L 10/13/22 21:51 67-72-110/12/22 16:179.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/13/22 21:51 193-39-510/12/22 16:179.1 2.6 1
Isophorone ND ug/L 10/13/22 21:51 78-59-110/12/22 16:179.1 1.5 1
1-Methylnaphthalene ND ug/L 10/13/22 21:51 90-12-010/12/22 16:179.1 1.8 1
2-Methylnaphthalene ND ug/L 10/13/22 21:51 91-57-610/12/22 16:179.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 10/13/22 21:51 95-48-710/12/22 16:179.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/13/22 21:51 15831-10-410/12/22 16:179.1 1.1 1
Naphthalene ND ug/L 10/13/22 21:51 91-20-310/12/22 16:179.1 1.9 1
2-Nitroaniline ND ug/L 10/13/22 21:51 88-74-410/12/22 16:1718.2 2.7 1
3-Nitroaniline ND ug/L 10/13/22 21:51 99-09-210/12/22 16:1718.2 3.4 1
4-Nitroaniline ND ug/L 10/13/22 21:51 100-01-610/12/22 16:1718.2 4.6 1
Nitrobenzene ND ug/L 10/13/22 21:51 98-95-310/12/22 16:179.1 1.7 1
2-Nitrophenol ND ug/L 10/13/22 21:51 88-75-510/12/22 16:179.1 1.3 1
4-Nitrophenol ND ug/L 10/13/22 21:51 100-02-710/12/22 16:1745.5 6.0 1
N-Nitrosodimethylamine ND ug/L 10/13/22 21:51 62-75-910/12/22 16:179.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 10/13/22 21:51 621-64-710/12/22 16:179.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 10/13/22 21:51 86-30-610/12/22 16:179.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/13/22 21:51 108-60-1 v110/12/22 16:179.1 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-3 Lab ID:92630198003 Collected:10/07/22 11:50 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Pentachlorophenol ND ug/L 10/13/22 21:51 87-86-510/12/22 16:1718.2 3.4 1
Phenanthrene ND ug/L 10/13/22 21:51 85-01-810/12/22 16:179.1 1.8 1
Phenol ND ug/L 10/13/22 21:51 108-95-210/12/22 16:179.1 1.2 1
Pyrene ND ug/L 10/13/22 21:51 129-00-010/12/22 16:179.1 2.0 1
Pyridine ND ug/L 10/13/22 21:51 110-86-110/12/22 16:179.1 2.4 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 21:51 120-82-110/12/22 16:179.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 10/13/22 21:51 95-95-410/12/22 16:179.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 10/13/22 21:51 88-06-210/12/22 16:179.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)24 %10/13/22 21:51 4165-60-010/12/22 16:1710-144 1
2-Fluorobiphenyl (S)9 %10/13/22 21:51 321-60-8 S010/12/22 16:1710-130 1
Terphenyl-d14 (S)122 %10/13/22 21:51 1718-51-010/12/22 16:1734-163 1
Phenol-d6 (S)12 %10/13/22 21:51 13127-88-310/12/22 16:1710-130 1
2-Fluorophenol (S)14 %10/13/22 21:51 367-12-410/12/22 16:1710-130 1
2,4,6-Tribromophenol (S)45 %10/13/22 21:51 118-79-610/12/22 16:1710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/13/22 21:04 67-64-125.0 5.1 1
Benzene ND ug/L 10/13/22 21:04 71-43-21.0 0.34 1
Bromobenzene ND ug/L 10/13/22 21:04 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 10/13/22 21:04 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/13/22 21:04 75-27-41.0 0.31 1
Bromoform ND ug/L 10/13/22 21:04 75-25-2 IK1.0 0.34 1
Bromomethane ND ug/L 10/13/22 21:04 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/13/22 21:04 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 10/13/22 21:04 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/13/22 21:04 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/13/22 21:04 75-00-31.0 0.65 1
Chloroform ND ug/L 10/13/22 21:04 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/13/22 21:04 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/13/22 21:04 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 10/13/22 21:04 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/22 21:04 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/13/22 21:04 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/22 21:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/13/22 21:04 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/13/22 21:04 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/13/22 21:04 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/13/22 21:04 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/13/22 21:04 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/13/22 21:04 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/13/22 21:04 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/13/22 21:04 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/13/22 21:04 156-59-21.0 0.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-3 Lab ID:92630198003 Collected:10/07/22 11:50 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
trans-1,2-Dichloroethene ND ug/L 10/13/22 21:04 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/13/22 21:04 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 10/13/22 21:04 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 10/13/22 21:04 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 10/13/22 21:04 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/13/22 21:04 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/13/22 21:04 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 10/13/22 21:04 108-20-3 IK1.0 0.31 1
Ethylbenzene ND ug/L 10/13/22 21:04 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 21:04 87-68-32.0 1.5 1
2-Hexanone ND ug/L 10/13/22 21:04 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 10/13/22 21:04 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 10/13/22 21:04 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/22 21:04 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/13/22 21:04 1634-04-41.0 0.42 1
Naphthalene ND ug/L 10/13/22 21:04 91-20-31.0 0.64 1
Styrene ND ug/L 10/13/22 21:04 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/22 21:04 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/22 21:04 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/13/22 21:04 127-18-41.0 0.29 1
Toluene ND ug/L 10/13/22 21:04 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/13/22 21:04 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 21:04 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/13/22 21:04 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/13/22 21:04 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/13/22 21:04 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/13/22 21:04 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/13/22 21:04 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/13/22 21:04 108-05-4 IK2.0 1.3 1
Vinyl chloride ND ug/L 10/13/22 21:04 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/13/22 21:04 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 10/13/22 21:04 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/13/22 21:04 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)90 %10/13/22 21:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %10/13/22 21:04 17060-07-070-130 1
Toluene-d8 (S)113 %10/13/22 21:04 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 10/19/22 09:38 18540-29-910/19/22 09:380.500 0.150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-4 Lab ID:92630198004 Collected:10/07/22 13:15 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND ug/L 10/13/22 20:57 7440-38-210/13/22 15:1430.0 26.2 1
Barium 271 ug/L 10/13/22 20:57 7440-39-310/13/22 15:1410.0 1.3 1
Cadmium ND ug/L 10/13/22 20:57 7440-43-910/13/22 15:1410.0 2.7 1
Chromium 11.5 ug/L 10/13/22 20:57 7440-47-310/13/22 15:1410.0 3.6 1
Silver ND ug/L 10/13/22 20:57 7440-22-410/13/22 15:1410.0 4.6 1
Lead 199 ug/L 10/13/22 20:57 7439-92-110/13/22 15:1420.0 19.0 1
Selenium ND ug/L 10/13/22 20:57 7782-49-210/13/22 15:1440.0 31.1 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010 MET ICP, Dissolved
Arsenic, Dissolved ND ug/L 10/14/22 19:32 7440-38-210/14/22 10:5830.0 26.2 1
Barium, Dissolved 41.2 ug/L 10/14/22 19:32 7440-39-310/14/22 10:5810.0 1.3 1
Cadmium, Dissolved ND ug/L 10/14/22 19:32 7440-43-910/14/22 10:5810.0 2.7 1
Chromium, Dissolved ND ug/L 10/14/22 19:32 7440-47-310/14/22 10:5810.0 3.6 1
Lead, Dissolved ND ug/L 10/14/22 19:32 7439-92-110/14/22 10:5820.0 19.0 1
Selenium, Dissolved ND ug/L 10/14/22 19:32 7782-49-210/14/22 10:5840.0 31.1 1
Silver, Dissolved ND ug/L 10/14/22 19:32 7440-22-410/14/22 10:5810.0 4.6 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 10/18/22 10:01 7439-97-610/17/22 16:050.20 0.13 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/17/22 15:32 7439-97-610/17/22 14:100.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 10/13/22 22:16 83-32-910/12/22 16:179.1 1.8 1
Acenaphthylene ND ug/L 10/13/22 22:16 208-96-810/12/22 16:179.1 1.8 1
Aniline ND ug/L 10/13/22 22:16 62-53-310/12/22 16:179.1 1.5 1
Anthracene ND ug/L 10/13/22 22:16 120-12-710/12/22 16:179.1 2.1 1
Benzo(a)anthracene ND ug/L 10/13/22 22:16 56-55-310/12/22 16:179.1 2.4 1
Benzo(a)pyrene ND ug/L 10/13/22 22:16 50-32-810/12/22 16:179.1 2.5 1
Benzo(b)fluoranthene ND ug/L 10/13/22 22:16 205-99-210/12/22 16:179.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 10/13/22 22:16 191-24-210/12/22 16:179.1 2.6 1
Benzo(k)fluoranthene ND ug/L 10/13/22 22:16 207-08-910/12/22 16:179.1 2.5 1
Benzoic Acid ND ug/L 10/13/22 22:16 65-85-010/12/22 16:1745.5 20.0 1
Benzyl alcohol ND ug/L 10/13/22 22:16 100-51-610/12/22 16:1718.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 10/13/22 22:16 101-55-310/12/22 16:179.1 1.6 1
Butylbenzylphthalate ND ug/L 10/13/22 22:16 85-68-710/12/22 16:179.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 10/13/22 22:16 59-50-710/12/22 16:179.1 3.0 1
4-Chloroaniline ND ug/L 10/13/22 22:16 106-47-810/12/22 16:1718.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 10/13/22 22:16 111-91-110/12/22 16:179.1 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-4 Lab ID:92630198004 Collected:10/07/22 13:15 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
bis(2-Chloroethyl) ether ND ug/L 10/13/22 22:16 111-44-410/12/22 16:179.1 1.7 1
2-Chloronaphthalene ND ug/L 10/13/22 22:16 91-58-710/12/22 16:179.1 1.6 1
2-Chlorophenol ND ug/L 10/13/22 22:16 95-57-810/12/22 16:179.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 10/13/22 22:16 7005-72-310/12/22 16:179.1 1.8 1
Chrysene ND ug/L 10/13/22 22:16 218-01-910/12/22 16:179.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 10/13/22 22:16 53-70-310/12/22 16:179.1 2.7 1
Dibenzofuran ND ug/L 10/13/22 22:16 132-64-910/12/22 16:179.1 1.9 1
1,2-Dichlorobenzene ND ug/L 10/13/22 22:16 95-50-110/12/22 16:179.1 1.6 1
1,3-Dichlorobenzene ND ug/L 10/13/22 22:16 541-73-110/12/22 16:179.1 1.5 1
1,4-Dichlorobenzene ND ug/L 10/13/22 22:16 106-46-710/12/22 16:179.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 10/13/22 22:16 91-94-110/12/22 16:1718.2 7.4 1
2,4-Dichlorophenol ND ug/L 10/13/22 22:16 120-83-210/12/22 16:179.1 1.3 1
Diethylphthalate ND ug/L 10/13/22 22:16 84-66-210/12/22 16:179.1 1.9 1
2,4-Dimethylphenol ND ug/L 10/13/22 22:16 105-67-910/12/22 16:179.1 1.5 1
Dimethylphthalate ND ug/L 10/13/22 22:16 131-11-310/12/22 16:179.1 1.9 1
Di-n-butylphthalate ND ug/L 10/13/22 22:16 84-74-210/12/22 16:179.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 10/13/22 22:16 534-52-110/12/22 16:1718.2 7.1 1
2,4-Dinitrophenol ND ug/L 10/13/22 22:16 51-28-510/12/22 16:1745.5 23.6 1
2,4-Dinitrotoluene ND ug/L 10/13/22 22:16 121-14-210/12/22 16:179.1 1.5 1
2,6-Dinitrotoluene ND ug/L 10/13/22 22:16 606-20-210/12/22 16:179.1 1.6 1
Di-n-octylphthalate ND ug/L 10/13/22 22:16 117-84-010/12/22 16:179.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/13/22 22:16 117-81-710/12/22 16:175.5 3.4 1
Fluoranthene ND ug/L 10/13/22 22:16 206-44-010/12/22 16:179.1 2.0 1
Fluorene ND ug/L 10/13/22 22:16 86-73-710/12/22 16:179.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 22:16 87-68-310/12/22 16:179.1 1.6 1
Hexachlorobenzene ND ug/L 10/13/22 22:16 118-74-110/12/22 16:179.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 10/13/22 22:16 77-47-410/12/22 16:179.1 1.4 1
Hexachloroethane ND ug/L 10/13/22 22:16 67-72-110/12/22 16:179.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/13/22 22:16 193-39-510/12/22 16:179.1 2.6 1
Isophorone ND ug/L 10/13/22 22:16 78-59-110/12/22 16:179.1 1.5 1
1-Methylnaphthalene ND ug/L 10/13/22 22:16 90-12-010/12/22 16:179.1 1.8 1
2-Methylnaphthalene ND ug/L 10/13/22 22:16 91-57-610/12/22 16:179.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 10/13/22 22:16 95-48-710/12/22 16:179.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/13/22 22:16 15831-10-410/12/22 16:179.1 1.1 1
Naphthalene ND ug/L 10/13/22 22:16 91-20-310/12/22 16:179.1 1.9 1
2-Nitroaniline ND ug/L 10/13/22 22:16 88-74-410/12/22 16:1718.2 2.7 1
3-Nitroaniline ND ug/L 10/13/22 22:16 99-09-210/12/22 16:1718.2 3.4 1
4-Nitroaniline ND ug/L 10/13/22 22:16 100-01-610/12/22 16:1718.2 4.6 1
Nitrobenzene ND ug/L 10/13/22 22:16 98-95-310/12/22 16:179.1 1.7 1
2-Nitrophenol ND ug/L 10/13/22 22:16 88-75-510/12/22 16:179.1 1.3 1
4-Nitrophenol ND ug/L 10/13/22 22:16 100-02-710/12/22 16:1745.5 6.0 1
N-Nitrosodimethylamine ND ug/L 10/13/22 22:16 62-75-910/12/22 16:179.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 10/13/22 22:16 621-64-710/12/22 16:179.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 10/13/22 22:16 86-30-610/12/22 16:179.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/13/22 22:16 108-60-1 v110/12/22 16:179.1 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-4 Lab ID:92630198004 Collected:10/07/22 13:15 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Pentachlorophenol ND ug/L 10/13/22 22:16 87-86-510/12/22 16:1718.2 3.4 1
Phenanthrene ND ug/L 10/13/22 22:16 85-01-810/12/22 16:179.1 1.8 1
Phenol ND ug/L 10/13/22 22:16 108-95-210/12/22 16:179.1 1.2 1
Pyrene ND ug/L 10/13/22 22:16 129-00-010/12/22 16:179.1 2.0 1
Pyridine ND ug/L 10/13/22 22:16 110-86-110/12/22 16:179.1 2.4 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 22:16 120-82-110/12/22 16:179.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 10/13/22 22:16 95-95-410/12/22 16:179.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 10/13/22 22:16 88-06-210/12/22 16:179.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)30 %10/13/22 22:16 4165-60-010/12/22 16:1710-144 1
2-Fluorobiphenyl (S)12 %10/13/22 22:16 321-60-810/12/22 16:1710-130 1
Terphenyl-d14 (S)133 %10/13/22 22:16 1718-51-010/12/22 16:1734-163 1
Phenol-d6 (S)40 %10/13/22 22:16 13127-88-310/12/22 16:1710-130 1
2-Fluorophenol (S)24 %10/13/22 22:16 367-12-410/12/22 16:1710-130 1
2,4,6-Tribromophenol (S)98 %10/13/22 22:16 118-79-610/12/22 16:1710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/13/22 21:21 67-64-125.0 5.1 1
Benzene ND ug/L 10/13/22 21:21 71-43-21.0 0.34 1
Bromobenzene ND ug/L 10/13/22 21:21 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 10/13/22 21:21 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/13/22 21:21 75-27-41.0 0.31 1
Bromoform ND ug/L 10/13/22 21:21 75-25-2 IK1.0 0.34 1
Bromomethane ND ug/L 10/13/22 21:21 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/13/22 21:21 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 10/13/22 21:21 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/13/22 21:21 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/13/22 21:21 75-00-31.0 0.65 1
Chloroform ND ug/L 10/13/22 21:21 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/13/22 21:21 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/13/22 21:21 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 10/13/22 21:21 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/22 21:21 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/13/22 21:21 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/22 21:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/13/22 21:21 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/13/22 21:21 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/13/22 21:21 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/13/22 21:21 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/13/22 21:21 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/13/22 21:21 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/13/22 21:21 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/13/22 21:21 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/13/22 21:21 156-59-21.0 0.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-4 Lab ID:92630198004 Collected:10/07/22 13:15 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
trans-1,2-Dichloroethene ND ug/L 10/13/22 21:21 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/13/22 21:21 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 10/13/22 21:21 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 10/13/22 21:21 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 10/13/22 21:21 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/13/22 21:21 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/13/22 21:21 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 10/13/22 21:21 108-20-3 IK1.0 0.31 1
Ethylbenzene ND ug/L 10/13/22 21:21 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 21:21 87-68-32.0 1.5 1
2-Hexanone ND ug/L 10/13/22 21:21 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 10/13/22 21:21 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 10/13/22 21:21 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/22 21:21 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/13/22 21:21 1634-04-41.0 0.42 1
Naphthalene ND ug/L 10/13/22 21:21 91-20-31.0 0.64 1
Styrene ND ug/L 10/13/22 21:21 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/22 21:21 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/22 21:21 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/13/22 21:21 127-18-41.0 0.29 1
Toluene ND ug/L 10/13/22 21:21 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/13/22 21:21 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 21:21 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/13/22 21:21 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/13/22 21:21 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/13/22 21:21 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/13/22 21:21 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/13/22 21:21 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/13/22 21:21 108-05-4 IK2.0 1.3 1
Vinyl chloride ND ug/L 10/13/22 21:21 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/13/22 21:21 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 10/13/22 21:21 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/13/22 21:21 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)92 %10/13/22 21:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)84 %10/13/22 21:21 17060-07-070-130 1
Toluene-d8 (S)112 %10/13/22 21:21 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 10/19/22 09:46 18540-29-910/19/22 09:460.500 0.150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-5 Lab ID:92630198005 Collected:10/07/22 14:00 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND ug/L 10/13/22 21:12 7440-38-210/13/22 15:1430.0 26.2 1
Barium 88.7 ug/L 10/13/22 21:12 7440-39-310/13/22 15:1410.0 1.3 1
Cadmium ND ug/L 10/13/22 21:12 7440-43-910/13/22 15:1410.0 2.7 1
Chromium ND ug/L 10/13/22 21:12 7440-47-310/13/22 15:1410.0 3.6 1
Silver ND ug/L 10/13/22 21:12 7440-22-410/13/22 15:1410.0 4.6 1
Lead ND ug/L 10/13/22 21:12 7439-92-110/13/22 15:1420.0 19.0 1
Selenium ND ug/L 10/13/22 21:12 7782-49-210/13/22 15:1440.0 31.1 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010 MET ICP, Dissolved
Arsenic, Dissolved ND ug/L 10/14/22 19:37 7440-38-210/14/22 10:5830.0 26.2 1
Barium, Dissolved 52.2 ug/L 10/14/22 19:37 7440-39-310/14/22 10:5810.0 1.3 1
Cadmium, Dissolved ND ug/L 10/14/22 19:37 7440-43-910/14/22 10:5810.0 2.7 1
Chromium, Dissolved ND ug/L 10/14/22 19:37 7440-47-310/14/22 10:5810.0 3.6 1
Lead, Dissolved ND ug/L 10/14/22 19:37 7439-92-110/14/22 10:5820.0 19.0 1
Selenium, Dissolved ND ug/L 10/14/22 19:37 7782-49-210/14/22 10:5840.0 31.1 1
Silver, Dissolved ND ug/L 10/14/22 19:37 7440-22-410/14/22 10:5810.0 4.6 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 10/18/22 10:09 7439-97-610/17/22 16:050.20 0.13 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/17/22 15:34 7439-97-610/17/22 14:100.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 10/13/22 22:42 83-32-910/12/22 16:179.1 1.8 1
Acenaphthylene ND ug/L 10/13/22 22:42 208-96-810/12/22 16:179.1 1.8 1
Aniline ND ug/L 10/13/22 22:42 62-53-310/12/22 16:179.1 1.5 1
Anthracene ND ug/L 10/13/22 22:42 120-12-710/12/22 16:179.1 2.1 1
Benzo(a)anthracene ND ug/L 10/13/22 22:42 56-55-310/12/22 16:179.1 2.4 1
Benzo(a)pyrene ND ug/L 10/13/22 22:42 50-32-810/12/22 16:179.1 2.5 1
Benzo(b)fluoranthene ND ug/L 10/13/22 22:42 205-99-210/12/22 16:179.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 10/13/22 22:42 191-24-210/12/22 16:179.1 2.6 1
Benzo(k)fluoranthene ND ug/L 10/13/22 22:42 207-08-910/12/22 16:179.1 2.5 1
Benzoic Acid ND ug/L 10/13/22 22:42 65-85-010/12/22 16:1745.5 20.0 1
Benzyl alcohol ND ug/L 10/13/22 22:42 100-51-610/12/22 16:1718.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 10/13/22 22:42 101-55-310/12/22 16:179.1 1.6 1
Butylbenzylphthalate ND ug/L 10/13/22 22:42 85-68-710/12/22 16:179.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 10/13/22 22:42 59-50-710/12/22 16:179.1 3.0 1
4-Chloroaniline ND ug/L 10/13/22 22:42 106-47-810/12/22 16:1718.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 10/13/22 22:42 111-91-110/12/22 16:179.1 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-5 Lab ID:92630198005 Collected:10/07/22 14:00 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
bis(2-Chloroethyl) ether ND ug/L 10/13/22 22:42 111-44-410/12/22 16:179.1 1.7 1
2-Chloronaphthalene ND ug/L 10/13/22 22:42 91-58-710/12/22 16:179.1 1.6 1
2-Chlorophenol ND ug/L 10/13/22 22:42 95-57-810/12/22 16:179.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 10/13/22 22:42 7005-72-310/12/22 16:179.1 1.8 1
Chrysene ND ug/L 10/13/22 22:42 218-01-910/12/22 16:179.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 10/13/22 22:42 53-70-310/12/22 16:179.1 2.7 1
Dibenzofuran ND ug/L 10/13/22 22:42 132-64-910/12/22 16:179.1 1.9 1
1,2-Dichlorobenzene ND ug/L 10/13/22 22:42 95-50-110/12/22 16:179.1 1.6 1
1,3-Dichlorobenzene ND ug/L 10/13/22 22:42 541-73-110/12/22 16:179.1 1.5 1
1,4-Dichlorobenzene ND ug/L 10/13/22 22:42 106-46-710/12/22 16:179.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 10/13/22 22:42 91-94-110/12/22 16:1718.2 7.4 1
2,4-Dichlorophenol ND ug/L 10/13/22 22:42 120-83-210/12/22 16:179.1 1.3 1
Diethylphthalate ND ug/L 10/13/22 22:42 84-66-210/12/22 16:179.1 1.9 1
2,4-Dimethylphenol ND ug/L 10/13/22 22:42 105-67-910/12/22 16:179.1 1.5 1
Dimethylphthalate ND ug/L 10/13/22 22:42 131-11-310/12/22 16:179.1 1.9 1
Di-n-butylphthalate ND ug/L 10/13/22 22:42 84-74-210/12/22 16:179.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 10/13/22 22:42 534-52-110/12/22 16:1718.2 7.1 1
2,4-Dinitrophenol ND ug/L 10/13/22 22:42 51-28-510/12/22 16:1745.5 23.6 1
2,4-Dinitrotoluene ND ug/L 10/13/22 22:42 121-14-210/12/22 16:179.1 1.5 1
2,6-Dinitrotoluene ND ug/L 10/13/22 22:42 606-20-210/12/22 16:179.1 1.6 1
Di-n-octylphthalate ND ug/L 10/13/22 22:42 117-84-010/12/22 16:179.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/13/22 22:42 117-81-710/12/22 16:175.5 3.4 1
Fluoranthene ND ug/L 10/13/22 22:42 206-44-010/12/22 16:179.1 2.0 1
Fluorene ND ug/L 10/13/22 22:42 86-73-710/12/22 16:179.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 22:42 87-68-310/12/22 16:179.1 1.6 1
Hexachlorobenzene ND ug/L 10/13/22 22:42 118-74-110/12/22 16:179.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 10/13/22 22:42 77-47-410/12/22 16:179.1 1.4 1
Hexachloroethane ND ug/L 10/13/22 22:42 67-72-110/12/22 16:179.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/13/22 22:42 193-39-510/12/22 16:179.1 2.6 1
Isophorone ND ug/L 10/13/22 22:42 78-59-110/12/22 16:179.1 1.5 1
1-Methylnaphthalene ND ug/L 10/13/22 22:42 90-12-010/12/22 16:179.1 1.8 1
2-Methylnaphthalene ND ug/L 10/13/22 22:42 91-57-610/12/22 16:179.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 10/13/22 22:42 95-48-710/12/22 16:179.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/13/22 22:42 15831-10-410/12/22 16:179.1 1.1 1
Naphthalene ND ug/L 10/13/22 22:42 91-20-310/12/22 16:179.1 1.9 1
2-Nitroaniline ND ug/L 10/13/22 22:42 88-74-410/12/22 16:1718.2 2.7 1
3-Nitroaniline ND ug/L 10/13/22 22:42 99-09-210/12/22 16:1718.2 3.4 1
4-Nitroaniline ND ug/L 10/13/22 22:42 100-01-610/12/22 16:1718.2 4.6 1
Nitrobenzene ND ug/L 10/13/22 22:42 98-95-310/12/22 16:179.1 1.7 1
2-Nitrophenol ND ug/L 10/13/22 22:42 88-75-510/12/22 16:179.1 1.3 1
4-Nitrophenol ND ug/L 10/13/22 22:42 100-02-710/12/22 16:1745.5 6.0 1
N-Nitrosodimethylamine ND ug/L 10/13/22 22:42 62-75-910/12/22 16:179.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 10/13/22 22:42 621-64-710/12/22 16:179.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 10/13/22 22:42 86-30-610/12/22 16:179.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/13/22 22:42 108-60-1 v110/12/22 16:179.1 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-5 Lab ID:92630198005 Collected:10/07/22 14:00 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Pentachlorophenol ND ug/L 10/13/22 22:42 87-86-510/12/22 16:1718.2 3.4 1
Phenanthrene ND ug/L 10/13/22 22:42 85-01-810/12/22 16:179.1 1.8 1
Phenol ND ug/L 10/13/22 22:42 108-95-210/12/22 16:179.1 1.2 1
Pyrene ND ug/L 10/13/22 22:42 129-00-010/12/22 16:179.1 2.0 1
Pyridine ND ug/L 10/13/22 22:42 110-86-110/12/22 16:179.1 2.4 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 22:42 120-82-110/12/22 16:179.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 10/13/22 22:42 95-95-410/12/22 16:179.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 10/13/22 22:42 88-06-210/12/22 16:179.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)14 %10/13/22 22:42 4165-60-010/12/22 16:1710-144 1
2-Fluorobiphenyl (S)6 %10/13/22 22:42 321-60-8 S010/12/22 16:1710-130 1
Terphenyl-d14 (S)103 %10/13/22 22:42 1718-51-010/12/22 16:1734-163 1
Phenol-d6 (S)10 %10/13/22 22:42 13127-88-310/12/22 16:1710-130 1
2-Fluorophenol (S)13 %10/13/22 22:42 367-12-410/12/22 16:1710-130 1
2,4,6-Tribromophenol (S)68 %10/13/22 22:42 118-79-610/12/22 16:1710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/13/22 21:39 67-64-125.0 5.1 1
Benzene ND ug/L 10/13/22 21:39 71-43-21.0 0.34 1
Bromobenzene ND ug/L 10/13/22 21:39 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 10/13/22 21:39 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/13/22 21:39 75-27-41.0 0.31 1
Bromoform ND ug/L 10/13/22 21:39 75-25-2 IK1.0 0.34 1
Bromomethane ND ug/L 10/13/22 21:39 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/13/22 21:39 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 10/13/22 21:39 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/13/22 21:39 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/13/22 21:39 75-00-31.0 0.65 1
Chloroform ND ug/L 10/13/22 21:39 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/13/22 21:39 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/13/22 21:39 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 10/13/22 21:39 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/22 21:39 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/13/22 21:39 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/22 21:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/13/22 21:39 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/13/22 21:39 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/13/22 21:39 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/13/22 21:39 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/13/22 21:39 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/13/22 21:39 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/13/22 21:39 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/13/22 21:39 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/13/22 21:39 156-59-21.0 0.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-5 Lab ID:92630198005 Collected:10/07/22 14:00 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
trans-1,2-Dichloroethene ND ug/L 10/13/22 21:39 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/13/22 21:39 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 10/13/22 21:39 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 10/13/22 21:39 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 10/13/22 21:39 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/13/22 21:39 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/13/22 21:39 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 10/13/22 21:39 108-20-3 IK1.0 0.31 1
Ethylbenzene ND ug/L 10/13/22 21:39 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 21:39 87-68-32.0 1.5 1
2-Hexanone ND ug/L 10/13/22 21:39 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 10/13/22 21:39 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 10/13/22 21:39 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/22 21:39 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/13/22 21:39 1634-04-41.0 0.42 1
Naphthalene ND ug/L 10/13/22 21:39 91-20-31.0 0.64 1
Styrene ND ug/L 10/13/22 21:39 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/22 21:39 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/22 21:39 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/13/22 21:39 127-18-41.0 0.29 1
Toluene ND ug/L 10/13/22 21:39 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/13/22 21:39 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 21:39 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/13/22 21:39 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/13/22 21:39 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/13/22 21:39 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/13/22 21:39 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/13/22 21:39 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/13/22 21:39 108-05-4 IK2.0 1.3 1
Vinyl chloride ND ug/L 10/13/22 21:39 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/13/22 21:39 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 10/13/22 21:39 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/13/22 21:39 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)92 %10/13/22 21:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %10/13/22 21:39 17060-07-070-130 1
Toluene-d8 (S)112 %10/13/22 21:39 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 10/19/22 09:54 18540-29-910/19/22 09:540.500 0.150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-6 Lab ID:92630198006 Collected:10/07/22 14:45 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND ug/L 10/13/22 21:16 7440-38-210/13/22 15:1430.0 26.2 1
Barium 80.5 ug/L 10/13/22 21:16 7440-39-310/13/22 15:1410.0 1.3 1
Cadmium ND ug/L 10/13/22 21:16 7440-43-910/13/22 15:1410.0 2.7 1
Chromium ND ug/L 10/13/22 21:16 7440-47-310/13/22 15:1410.0 3.6 1
Silver ND ug/L 10/13/22 21:16 7440-22-410/13/22 15:1410.0 4.6 1
Lead ND ug/L 10/13/22 21:16 7439-92-110/13/22 15:1420.0 19.0 1
Selenium ND ug/L 10/13/22 21:16 7782-49-210/13/22 15:1440.0 31.1 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010 MET ICP, Dissolved
Arsenic, Dissolved ND ug/L 10/14/22 19:41 7440-38-210/14/22 10:5830.0 26.2 1
Barium, Dissolved 59.8 ug/L 10/14/22 19:41 7440-39-310/14/22 10:5810.0 1.3 1
Cadmium, Dissolved ND ug/L 10/14/22 19:41 7440-43-910/14/22 10:5810.0 2.7 1
Chromium, Dissolved ND ug/L 10/14/22 19:41 7440-47-310/14/22 10:5810.0 3.6 1
Lead, Dissolved ND ug/L 10/14/22 19:41 7439-92-110/14/22 10:5820.0 19.0 1
Selenium, Dissolved ND ug/L 10/14/22 19:41 7782-49-210/14/22 10:5840.0 31.1 1
Silver, Dissolved ND ug/L 10/14/22 19:41 7440-22-410/14/22 10:5810.0 4.6 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 10/18/22 10:12 7439-97-610/17/22 16:050.20 0.13 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/17/22 15:42 7439-97-610/17/22 14:100.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 10/13/22 23:07 83-32-910/12/22 16:179.1 1.8 1
Acenaphthylene ND ug/L 10/13/22 23:07 208-96-810/12/22 16:179.1 1.8 1
Aniline ND ug/L 10/13/22 23:07 62-53-310/12/22 16:179.1 1.5 1
Anthracene ND ug/L 10/13/22 23:07 120-12-710/12/22 16:179.1 2.1 1
Benzo(a)anthracene ND ug/L 10/13/22 23:07 56-55-310/12/22 16:179.1 2.4 1
Benzo(a)pyrene ND ug/L 10/13/22 23:07 50-32-810/12/22 16:179.1 2.5 1
Benzo(b)fluoranthene ND ug/L 10/13/22 23:07 205-99-210/12/22 16:179.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 10/13/22 23:07 191-24-210/12/22 16:179.1 2.6 1
Benzo(k)fluoranthene ND ug/L 10/13/22 23:07 207-08-910/12/22 16:179.1 2.5 1
Benzoic Acid ND ug/L 10/13/22 23:07 65-85-010/12/22 16:1745.5 20.0 1
Benzyl alcohol ND ug/L 10/13/22 23:07 100-51-610/12/22 16:1718.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 10/13/22 23:07 101-55-310/12/22 16:179.1 1.6 1
Butylbenzylphthalate ND ug/L 10/13/22 23:07 85-68-710/12/22 16:179.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 10/13/22 23:07 59-50-710/12/22 16:179.1 3.0 1
4-Chloroaniline ND ug/L 10/13/22 23:07 106-47-810/12/22 16:1718.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 10/13/22 23:07 111-91-110/12/22 16:179.1 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-6 Lab ID:92630198006 Collected:10/07/22 14:45 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
bis(2-Chloroethyl) ether ND ug/L 10/13/22 23:07 111-44-410/12/22 16:179.1 1.7 1
2-Chloronaphthalene ND ug/L 10/13/22 23:07 91-58-710/12/22 16:179.1 1.6 1
2-Chlorophenol ND ug/L 10/13/22 23:07 95-57-810/12/22 16:179.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 10/13/22 23:07 7005-72-310/12/22 16:179.1 1.8 1
Chrysene ND ug/L 10/13/22 23:07 218-01-910/12/22 16:179.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 10/13/22 23:07 53-70-310/12/22 16:179.1 2.7 1
Dibenzofuran ND ug/L 10/13/22 23:07 132-64-910/12/22 16:179.1 1.9 1
1,2-Dichlorobenzene ND ug/L 10/13/22 23:07 95-50-110/12/22 16:179.1 1.6 1
1,3-Dichlorobenzene ND ug/L 10/13/22 23:07 541-73-110/12/22 16:179.1 1.5 1
1,4-Dichlorobenzene ND ug/L 10/13/22 23:07 106-46-710/12/22 16:179.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 10/13/22 23:07 91-94-110/12/22 16:1718.2 7.4 1
2,4-Dichlorophenol ND ug/L 10/13/22 23:07 120-83-210/12/22 16:179.1 1.3 1
Diethylphthalate ND ug/L 10/13/22 23:07 84-66-210/12/22 16:179.1 1.9 1
2,4-Dimethylphenol ND ug/L 10/13/22 23:07 105-67-910/12/22 16:179.1 1.5 1
Dimethylphthalate ND ug/L 10/13/22 23:07 131-11-310/12/22 16:179.1 1.9 1
Di-n-butylphthalate ND ug/L 10/13/22 23:07 84-74-210/12/22 16:179.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 10/13/22 23:07 534-52-110/12/22 16:1718.2 7.1 1
2,4-Dinitrophenol ND ug/L 10/13/22 23:07 51-28-510/12/22 16:1745.5 23.6 1
2,4-Dinitrotoluene ND ug/L 10/13/22 23:07 121-14-210/12/22 16:179.1 1.5 1
2,6-Dinitrotoluene ND ug/L 10/13/22 23:07 606-20-210/12/22 16:179.1 1.6 1
Di-n-octylphthalate ND ug/L 10/13/22 23:07 117-84-010/12/22 16:179.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/13/22 23:07 117-81-710/12/22 16:175.5 3.4 1
Fluoranthene ND ug/L 10/13/22 23:07 206-44-010/12/22 16:179.1 2.0 1
Fluorene ND ug/L 10/13/22 23:07 86-73-710/12/22 16:179.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 23:07 87-68-310/12/22 16:179.1 1.6 1
Hexachlorobenzene ND ug/L 10/13/22 23:07 118-74-110/12/22 16:179.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 10/13/22 23:07 77-47-410/12/22 16:179.1 1.4 1
Hexachloroethane ND ug/L 10/13/22 23:07 67-72-110/12/22 16:179.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/13/22 23:07 193-39-510/12/22 16:179.1 2.6 1
Isophorone ND ug/L 10/13/22 23:07 78-59-110/12/22 16:179.1 1.5 1
1-Methylnaphthalene ND ug/L 10/13/22 23:07 90-12-010/12/22 16:179.1 1.8 1
2-Methylnaphthalene ND ug/L 10/13/22 23:07 91-57-610/12/22 16:179.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 10/13/22 23:07 95-48-710/12/22 16:179.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/13/22 23:07 15831-10-410/12/22 16:179.1 1.1 1
Naphthalene ND ug/L 10/13/22 23:07 91-20-310/12/22 16:179.1 1.9 1
2-Nitroaniline ND ug/L 10/13/22 23:07 88-74-410/12/22 16:1718.2 2.7 1
3-Nitroaniline ND ug/L 10/13/22 23:07 99-09-210/12/22 16:1718.2 3.4 1
4-Nitroaniline ND ug/L 10/13/22 23:07 100-01-610/12/22 16:1718.2 4.6 1
Nitrobenzene ND ug/L 10/13/22 23:07 98-95-310/12/22 16:179.1 1.7 1
2-Nitrophenol ND ug/L 10/13/22 23:07 88-75-510/12/22 16:179.1 1.3 1
4-Nitrophenol ND ug/L 10/13/22 23:07 100-02-710/12/22 16:1745.5 6.0 1
N-Nitrosodimethylamine ND ug/L 10/13/22 23:07 62-75-910/12/22 16:179.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 10/13/22 23:07 621-64-710/12/22 16:179.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 10/13/22 23:07 86-30-610/12/22 16:179.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/13/22 23:07 108-60-1 v110/12/22 16:179.1 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-6 Lab ID:92630198006 Collected:10/07/22 14:45 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Pentachlorophenol ND ug/L 10/13/22 23:07 87-86-510/12/22 16:1718.2 3.4 1
Phenanthrene ND ug/L 10/13/22 23:07 85-01-810/12/22 16:179.1 1.8 1
Phenol ND ug/L 10/13/22 23:07 108-95-210/12/22 16:179.1 1.2 1
Pyrene ND ug/L 10/13/22 23:07 129-00-010/12/22 16:179.1 2.0 1
Pyridine ND ug/L 10/13/22 23:07 110-86-110/12/22 16:179.1 2.4 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 23:07 120-82-110/12/22 16:179.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 10/13/22 23:07 95-95-410/12/22 16:179.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 10/13/22 23:07 88-06-210/12/22 16:179.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)21 %10/13/22 23:07 4165-60-010/12/22 16:1710-144 1
2-Fluorobiphenyl (S)7 %10/13/22 23:07 321-60-8 S010/12/22 16:1710-130 1
Terphenyl-d14 (S)119 %10/13/22 23:07 1718-51-010/12/22 16:1734-163 1
Phenol-d6 (S)16 %10/13/22 23:07 13127-88-310/12/22 16:1710-130 1
2-Fluorophenol (S)17 %10/13/22 23:07 367-12-410/12/22 16:1710-130 1
2,4,6-Tribromophenol (S)71 %10/13/22 23:07 118-79-610/12/22 16:1710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/13/22 21:56 67-64-125.0 5.1 1
Benzene ND ug/L 10/13/22 21:56 71-43-21.0 0.34 1
Bromobenzene ND ug/L 10/13/22 21:56 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 10/13/22 21:56 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/13/22 21:56 75-27-41.0 0.31 1
Bromoform ND ug/L 10/13/22 21:56 75-25-2 IK1.0 0.34 1
Bromomethane ND ug/L 10/13/22 21:56 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/13/22 21:56 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 10/13/22 21:56 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/13/22 21:56 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/13/22 21:56 75-00-31.0 0.65 1
Chloroform ND ug/L 10/13/22 21:56 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/13/22 21:56 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/13/22 21:56 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 10/13/22 21:56 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/22 21:56 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/13/22 21:56 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/22 21:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/13/22 21:56 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/13/22 21:56 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/13/22 21:56 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/13/22 21:56 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/13/22 21:56 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/13/22 21:56 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/13/22 21:56 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/13/22 21:56 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/13/22 21:56 156-59-21.0 0.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-6 Lab ID:92630198006 Collected:10/07/22 14:45 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
trans-1,2-Dichloroethene ND ug/L 10/13/22 21:56 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/13/22 21:56 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 10/13/22 21:56 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 10/13/22 21:56 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 10/13/22 21:56 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/13/22 21:56 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/13/22 21:56 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 10/13/22 21:56 108-20-3 IK1.0 0.31 1
Ethylbenzene ND ug/L 10/13/22 21:56 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 21:56 87-68-32.0 1.5 1
2-Hexanone ND ug/L 10/13/22 21:56 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 10/13/22 21:56 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 10/13/22 21:56 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/22 21:56 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/13/22 21:56 1634-04-41.0 0.42 1
Naphthalene ND ug/L 10/13/22 21:56 91-20-31.0 0.64 1
Styrene ND ug/L 10/13/22 21:56 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/22 21:56 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/22 21:56 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/13/22 21:56 127-18-41.0 0.29 1
Toluene ND ug/L 10/13/22 21:56 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/13/22 21:56 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 21:56 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/13/22 21:56 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/13/22 21:56 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/13/22 21:56 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/13/22 21:56 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/13/22 21:56 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/13/22 21:56 108-05-4 IK2.0 1.3 1
Vinyl chloride ND ug/L 10/13/22 21:56 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/13/22 21:56 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 10/13/22 21:56 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/13/22 21:56 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)90 %10/13/22 21:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)83 %10/13/22 21:56 17060-07-070-130 1
Toluene-d8 (S)114 %10/13/22 21:56 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 10/19/22 10:01 18540-29-910/19/22 10:010.500 0.150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-7 Lab ID:92630198007 Collected:10/07/22 15:30 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND ug/L 10/13/22 21:21 7440-38-210/13/22 15:1430.0 26.2 1
Barium 143 ug/L 10/13/22 21:21 7440-39-310/13/22 15:1410.0 1.3 1
Cadmium ND ug/L 10/13/22 21:21 7440-43-910/13/22 15:1410.0 2.7 1
Chromium ND ug/L 10/13/22 21:21 7440-47-310/13/22 15:1410.0 3.6 1
Silver ND ug/L 10/13/22 21:21 7440-22-410/13/22 15:1410.0 4.6 1
Lead ND ug/L 10/13/22 21:21 7439-92-110/13/22 15:1420.0 19.0 1
Selenium ND ug/L 10/13/22 21:21 7782-49-210/13/22 15:1440.0 31.1 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010 MET ICP, Dissolved
Arsenic, Dissolved ND ug/L 10/14/22 19:46 7440-38-210/14/22 10:5830.0 26.2 1
Barium, Dissolved 66.2 ug/L 10/14/22 19:46 7440-39-310/14/22 10:5810.0 1.3 1
Cadmium, Dissolved ND ug/L 10/14/22 19:46 7440-43-910/14/22 10:5810.0 2.7 1
Chromium, Dissolved ND ug/L 10/14/22 19:46 7440-47-310/14/22 10:5810.0 3.6 1
Lead, Dissolved ND ug/L 10/14/22 19:46 7439-92-110/14/22 10:5820.0 19.0 1
Selenium, Dissolved ND ug/L 10/14/22 19:46 7782-49-210/14/22 10:5840.0 31.1 1
Silver, Dissolved ND ug/L 10/14/22 19:46 7440-22-410/14/22 10:5810.0 4.6 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 10/18/22 10:14 7439-97-610/17/22 16:050.20 0.13 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/17/22 15:45 7439-97-610/17/22 14:100.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 10/14/22 18:35 83-32-9 L110/14/22 13:419.1 1.8 1
Acenaphthylene ND ug/L 10/14/22 18:35 208-96-8 L110/14/22 13:419.1 1.8 1
Aniline ND ug/L 10/14/22 18:35 62-53-310/14/22 13:419.1 1.5 1
Anthracene ND ug/L 10/14/22 18:35 120-12-710/14/22 13:419.1 2.1 1
Benzo(a)anthracene ND ug/L 10/14/22 18:35 56-55-3 L110/14/22 13:419.1 2.4 1
Benzo(a)pyrene ND ug/L 10/14/22 18:35 50-32-810/14/22 13:419.1 2.5 1
Benzo(b)fluoranthene ND ug/L 10/14/22 18:35 205-99-2 L110/14/22 13:419.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 10/14/22 18:35 191-24-2 L110/14/22 13:419.1 2.6 1
Benzo(k)fluoranthene ND ug/L 10/14/22 18:35 207-08-910/14/22 13:419.1 2.5 1
Benzoic Acid ND ug/L 10/14/22 18:35 65-85-0 v110/14/22 13:4145.5 20.0 1
Benzyl alcohol ND ug/L 10/14/22 18:35 100-51-610/14/22 13:4118.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 10/14/22 18:35 101-55-3 L110/14/22 13:419.1 1.6 1
Butylbenzylphthalate ND ug/L 10/14/22 18:35 85-68-7 L110/14/22 13:419.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 10/14/22 18:35 59-50-710/14/22 13:419.1 3.0 1
4-Chloroaniline ND ug/L 10/14/22 18:35 106-47-810/14/22 13:4118.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 10/14/22 18:35 111-91-110/14/22 13:419.1 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-7 Lab ID:92630198007 Collected:10/07/22 15:30 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
bis(2-Chloroethyl) ether ND ug/L 10/14/22 18:35 111-44-410/14/22 13:419.1 1.7 1
2-Chloronaphthalene ND ug/L 10/14/22 18:35 91-58-7 L110/14/22 13:419.1 1.6 1
2-Chlorophenol ND ug/L 10/14/22 18:35 95-57-810/14/22 13:419.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 10/14/22 18:35 7005-72-310/14/22 13:419.1 1.8 1
Chrysene ND ug/L 10/14/22 18:35 218-01-9 L110/14/22 13:419.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 10/14/22 18:35 53-70-3 L110/14/22 13:419.1 2.7 1
Dibenzofuran ND ug/L 10/14/22 18:35 132-64-9 L110/14/22 13:419.1 1.9 1
1,2-Dichlorobenzene ND ug/L 10/14/22 18:35 95-50-110/14/22 13:419.1 1.6 1
1,3-Dichlorobenzene ND ug/L 10/14/22 18:35 541-73-110/14/22 13:419.1 1.5 1
1,4-Dichlorobenzene ND ug/L 10/14/22 18:35 106-46-710/14/22 13:419.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 10/14/22 18:35 91-94-1 L110/14/22 13:4118.2 7.4 1
2,4-Dichlorophenol ND ug/L 10/14/22 18:35 120-83-210/14/22 13:419.1 1.3 1
Diethylphthalate ND ug/L 10/14/22 18:35 84-66-2 L110/14/22 13:419.1 1.9 1
2,4-Dimethylphenol ND ug/L 10/14/22 18:35 105-67-9 L110/14/22 13:419.1 1.5 1
Dimethylphthalate ND ug/L 10/14/22 18:35 131-11-3 L110/14/22 13:419.1 1.9 1
Di-n-butylphthalate ND ug/L 10/14/22 18:35 84-74-2 L110/14/22 13:419.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 10/14/22 18:35 534-52-110/14/22 13:4118.2 7.1 1
2,4-Dinitrophenol ND ug/L 10/14/22 18:35 51-28-510/14/22 13:4145.5 23.6 1
2,4-Dinitrotoluene ND ug/L 10/14/22 18:35 121-14-2 L110/14/22 13:419.1 1.5 1
2,6-Dinitrotoluene ND ug/L 10/14/22 18:35 606-20-2 L110/14/22 13:419.1 1.6 1
Di-n-octylphthalate ND ug/L 10/14/22 18:35 117-84-0 v110/14/22 13:419.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/14/22 18:35 117-81-710/14/22 13:415.5 3.4 1
Fluoranthene ND ug/L 10/14/22 18:35 206-44-010/14/22 13:419.1 2.0 1
Fluorene ND ug/L 10/14/22 18:35 86-73-710/14/22 13:419.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 10/14/22 18:35 87-68-310/14/22 13:419.1 1.6 1
Hexachlorobenzene ND ug/L 10/14/22 18:35 118-74-1 L110/14/22 13:419.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 10/14/22 18:35 77-47-4 L110/14/22 13:419.1 1.4 1
Hexachloroethane ND ug/L 10/14/22 18:35 67-72-110/14/22 13:419.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/14/22 18:35 193-39-5 L110/14/22 13:419.1 2.6 1
Isophorone ND ug/L 10/14/22 18:35 78-59-1 L110/14/22 13:419.1 1.5 1
1-Methylnaphthalene ND ug/L 10/14/22 18:35 90-12-010/14/22 13:419.1 1.8 1
2-Methylnaphthalene ND ug/L 10/14/22 18:35 91-57-610/14/22 13:419.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 10/14/22 18:35 95-48-710/14/22 13:419.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/14/22 18:35 15831-10-410/14/22 13:419.1 1.1 1
Naphthalene ND ug/L 10/14/22 18:35 91-20-310/14/22 13:419.1 1.9 1
2-Nitroaniline ND ug/L 10/14/22 18:35 88-74-4 L110/14/22 13:4118.2 2.7 1
3-Nitroaniline ND ug/L 10/14/22 18:35 99-09-2 L110/14/22 13:4118.2 3.4 1
4-Nitroaniline ND ug/L 10/14/22 18:35 100-01-6 L110/14/22 13:4118.2 4.6 1
Nitrobenzene ND ug/L 10/14/22 18:35 98-95-3 L110/14/22 13:419.1 1.7 1
2-Nitrophenol ND ug/L 10/14/22 18:35 88-75-5 L110/14/22 13:419.1 1.3 1
4-Nitrophenol ND ug/L 10/14/22 18:35 100-02-710/14/22 13:4145.5 6.0 1
N-Nitrosodimethylamine ND ug/L 10/14/22 18:35 62-75-910/14/22 13:419.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 10/14/22 18:35 621-64-710/14/22 13:419.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 10/14/22 18:35 86-30-6 L110/14/22 13:419.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/14/22 18:35 108-60-1 v110/14/22 13:419.1 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-7 Lab ID:92630198007 Collected:10/07/22 15:30 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Pentachlorophenol ND ug/L 10/14/22 18:35 87-86-510/14/22 13:4118.2 3.4 1
Phenanthrene ND ug/L 10/14/22 18:35 85-01-8 L110/14/22 13:419.1 1.8 1
Phenol ND ug/L 10/14/22 18:35 108-95-210/14/22 13:419.1 1.2 1
Pyrene ND ug/L 10/14/22 18:35 129-00-0 L110/14/22 13:419.1 2.0 1
Pyridine ND ug/L 10/14/22 18:35 110-86-110/14/22 13:419.1 2.4 1
1,2,4-Trichlorobenzene ND ug/L 10/14/22 18:35 120-82-110/14/22 13:419.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 10/14/22 18:35 95-95-4 L110/14/22 13:419.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 10/14/22 18:35 88-06-2 L110/14/22 13:419.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)41 %10/14/22 18:35 4165-60-010/14/22 13:4110-144 1
2-Fluorobiphenyl (S)18 %10/14/22 18:35 321-60-810/14/22 13:4110-130 1
Terphenyl-d14 (S)85 %10/14/22 18:35 1718-51-010/14/22 13:4134-163 1
Phenol-d6 (S)15 %10/14/22 18:35 13127-88-310/14/22 13:4110-130 1
2-Fluorophenol (S)15 %10/14/22 18:35 367-12-410/14/22 13:4110-130 1
2,4,6-Tribromophenol (S)27 %10/14/22 18:35 118-79-610/14/22 13:4110-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/13/22 22:14 67-64-125.0 5.1 1
Benzene ND ug/L 10/13/22 22:14 71-43-21.0 0.34 1
Bromobenzene ND ug/L 10/13/22 22:14 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 10/13/22 22:14 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/13/22 22:14 75-27-41.0 0.31 1
Bromoform ND ug/L 10/13/22 22:14 75-25-2 IK1.0 0.34 1
Bromomethane ND ug/L 10/13/22 22:14 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/13/22 22:14 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 10/13/22 22:14 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/13/22 22:14 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/13/22 22:14 75-00-31.0 0.65 1
Chloroform ND ug/L 10/13/22 22:14 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/13/22 22:14 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/13/22 22:14 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 10/13/22 22:14 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/22 22:14 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/13/22 22:14 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/22 22:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/13/22 22:14 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/13/22 22:14 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/13/22 22:14 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/13/22 22:14 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/13/22 22:14 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/13/22 22:14 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/13/22 22:14 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/13/22 22:14 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/13/22 22:14 156-59-21.0 0.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-7 Lab ID:92630198007 Collected:10/07/22 15:30 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
trans-1,2-Dichloroethene ND ug/L 10/13/22 22:14 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/13/22 22:14 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 10/13/22 22:14 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 10/13/22 22:14 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 10/13/22 22:14 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/13/22 22:14 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/13/22 22:14 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 10/13/22 22:14 108-20-3 IK1.0 0.31 1
Ethylbenzene ND ug/L 10/13/22 22:14 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 22:14 87-68-32.0 1.5 1
2-Hexanone ND ug/L 10/13/22 22:14 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 10/13/22 22:14 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 10/13/22 22:14 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/22 22:14 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/13/22 22:14 1634-04-41.0 0.42 1
Naphthalene ND ug/L 10/13/22 22:14 91-20-31.0 0.64 1
Styrene ND ug/L 10/13/22 22:14 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/22 22:14 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/22 22:14 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/13/22 22:14 127-18-41.0 0.29 1
Toluene ND ug/L 10/13/22 22:14 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/13/22 22:14 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 22:14 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/13/22 22:14 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/13/22 22:14 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/13/22 22:14 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/13/22 22:14 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/13/22 22:14 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/13/22 22:14 108-05-4 IK2.0 1.3 1
Vinyl chloride ND ug/L 10/13/22 22:14 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/13/22 22:14 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 10/13/22 22:14 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/13/22 22:14 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)90 %10/13/22 22:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)86 %10/13/22 22:14 17060-07-070-130 1
Toluene-d8 (S)112 %10/13/22 22:14 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 10/19/22 10:09 18540-29-910/19/22 10:090.500 0.150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-8 Lab ID:92630198008 Collected:10/07/22 16:30 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND ug/L 10/13/22 21:26 7440-38-210/13/22 15:1430.0 26.2 1
Barium 499 ug/L 10/13/22 21:26 7440-39-310/13/22 15:1410.0 1.3 1
Cadmium ND ug/L 10/13/22 21:26 7440-43-910/13/22 15:1410.0 2.7 1
Chromium 10.6 ug/L 10/13/22 21:26 7440-47-310/13/22 15:1410.0 3.6 1
Silver ND ug/L 10/13/22 21:26 7440-22-410/13/22 15:1410.0 4.6 1
Lead 37.4 ug/L 10/13/22 21:26 7439-92-110/13/22 15:1420.0 19.0 1
Selenium ND ug/L 10/13/22 21:26 7782-49-210/13/22 15:1440.0 31.1 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010 MET ICP, Dissolved
Arsenic, Dissolved ND ug/L 10/14/22 19:51 7440-38-210/14/22 10:5830.0 26.2 1
Barium, Dissolved 62.7 ug/L 10/14/22 19:51 7440-39-310/14/22 10:5810.0 1.3 1
Cadmium, Dissolved ND ug/L 10/14/22 19:51 7440-43-910/14/22 10:5810.0 2.7 1
Chromium, Dissolved ND ug/L 10/14/22 19:51 7440-47-310/14/22 10:5810.0 3.6 1
Lead, Dissolved ND ug/L 10/14/22 19:51 7439-92-110/14/22 10:5820.0 19.0 1
Selenium, Dissolved ND ug/L 10/14/22 19:51 7782-49-210/14/22 10:5840.0 31.1 1
Silver, Dissolved ND ug/L 10/14/22 19:51 7440-22-410/14/22 10:5810.0 4.6 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 10/18/22 10:17 7439-97-610/17/22 16:050.20 0.13 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, Dissolved
Mercury, Dissolved ND ug/L 10/17/22 15:47 7439-97-610/17/22 14:100.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 10/13/22 23:58 83-32-910/12/22 16:179.1 1.8 1
Acenaphthylene ND ug/L 10/13/22 23:58 208-96-810/12/22 16:179.1 1.8 1
Aniline ND ug/L 10/13/22 23:58 62-53-310/12/22 16:179.1 1.5 1
Anthracene ND ug/L 10/13/22 23:58 120-12-710/12/22 16:179.1 2.1 1
Benzo(a)anthracene ND ug/L 10/13/22 23:58 56-55-310/12/22 16:179.1 2.4 1
Benzo(a)pyrene ND ug/L 10/13/22 23:58 50-32-810/12/22 16:179.1 2.5 1
Benzo(b)fluoranthene ND ug/L 10/13/22 23:58 205-99-210/12/22 16:179.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 10/13/22 23:58 191-24-210/12/22 16:179.1 2.6 1
Benzo(k)fluoranthene ND ug/L 10/13/22 23:58 207-08-910/12/22 16:179.1 2.5 1
Benzoic Acid ND ug/L 10/13/22 23:58 65-85-010/12/22 16:1745.5 20.0 1
Benzyl alcohol ND ug/L 10/13/22 23:58 100-51-610/12/22 16:1718.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 10/13/22 23:58 101-55-310/12/22 16:179.1 1.6 1
Butylbenzylphthalate ND ug/L 10/13/22 23:58 85-68-710/12/22 16:179.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 10/13/22 23:58 59-50-710/12/22 16:179.1 3.0 1
4-Chloroaniline ND ug/L 10/13/22 23:58 106-47-810/12/22 16:1718.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 10/13/22 23:58 111-91-110/12/22 16:179.1 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-8 Lab ID:92630198008 Collected:10/07/22 16:30 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
bis(2-Chloroethyl) ether ND ug/L 10/13/22 23:58 111-44-410/12/22 16:179.1 1.7 1
2-Chloronaphthalene ND ug/L 10/13/22 23:58 91-58-710/12/22 16:179.1 1.6 1
2-Chlorophenol ND ug/L 10/13/22 23:58 95-57-810/12/22 16:179.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 10/13/22 23:58 7005-72-310/12/22 16:179.1 1.8 1
Chrysene ND ug/L 10/13/22 23:58 218-01-910/12/22 16:179.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 10/13/22 23:58 53-70-310/12/22 16:179.1 2.7 1
Dibenzofuran ND ug/L 10/13/22 23:58 132-64-910/12/22 16:179.1 1.9 1
1,2-Dichlorobenzene ND ug/L 10/13/22 23:58 95-50-110/12/22 16:179.1 1.6 1
1,3-Dichlorobenzene ND ug/L 10/13/22 23:58 541-73-110/12/22 16:179.1 1.5 1
1,4-Dichlorobenzene ND ug/L 10/13/22 23:58 106-46-710/12/22 16:179.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 10/13/22 23:58 91-94-110/12/22 16:1718.2 7.4 1
2,4-Dichlorophenol ND ug/L 10/13/22 23:58 120-83-210/12/22 16:179.1 1.3 1
Diethylphthalate ND ug/L 10/13/22 23:58 84-66-210/12/22 16:179.1 1.9 1
2,4-Dimethylphenol ND ug/L 10/13/22 23:58 105-67-910/12/22 16:179.1 1.5 1
Dimethylphthalate ND ug/L 10/13/22 23:58 131-11-310/12/22 16:179.1 1.9 1
Di-n-butylphthalate ND ug/L 10/13/22 23:58 84-74-210/12/22 16:179.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 10/13/22 23:58 534-52-110/12/22 16:1718.2 7.1 1
2,4-Dinitrophenol ND ug/L 10/13/22 23:58 51-28-510/12/22 16:1745.5 23.6 1
2,4-Dinitrotoluene ND ug/L 10/13/22 23:58 121-14-210/12/22 16:179.1 1.5 1
2,6-Dinitrotoluene ND ug/L 10/13/22 23:58 606-20-210/12/22 16:179.1 1.6 1
Di-n-octylphthalate ND ug/L 10/13/22 23:58 117-84-010/12/22 16:179.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/13/22 23:58 117-81-710/12/22 16:175.5 3.4 1
Fluoranthene ND ug/L 10/13/22 23:58 206-44-010/12/22 16:179.1 2.0 1
Fluorene ND ug/L 10/13/22 23:58 86-73-710/12/22 16:179.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 23:58 87-68-310/12/22 16:179.1 1.6 1
Hexachlorobenzene ND ug/L 10/13/22 23:58 118-74-110/12/22 16:179.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 10/13/22 23:58 77-47-410/12/22 16:179.1 1.4 1
Hexachloroethane ND ug/L 10/13/22 23:58 67-72-110/12/22 16:179.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/13/22 23:58 193-39-510/12/22 16:179.1 2.6 1
Isophorone ND ug/L 10/13/22 23:58 78-59-110/12/22 16:179.1 1.5 1
1-Methylnaphthalene ND ug/L 10/13/22 23:58 90-12-010/12/22 16:179.1 1.8 1
2-Methylnaphthalene ND ug/L 10/13/22 23:58 91-57-610/12/22 16:179.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 10/13/22 23:58 95-48-710/12/22 16:179.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/13/22 23:58 15831-10-410/12/22 16:179.1 1.1 1
Naphthalene ND ug/L 10/13/22 23:58 91-20-310/12/22 16:179.1 1.9 1
2-Nitroaniline ND ug/L 10/13/22 23:58 88-74-410/12/22 16:1718.2 2.7 1
3-Nitroaniline ND ug/L 10/13/22 23:58 99-09-210/12/22 16:1718.2 3.4 1
4-Nitroaniline ND ug/L 10/13/22 23:58 100-01-610/12/22 16:1718.2 4.6 1
Nitrobenzene ND ug/L 10/13/22 23:58 98-95-310/12/22 16:179.1 1.7 1
2-Nitrophenol ND ug/L 10/13/22 23:58 88-75-510/12/22 16:179.1 1.3 1
4-Nitrophenol ND ug/L 10/13/22 23:58 100-02-710/12/22 16:1745.5 6.0 1
N-Nitrosodimethylamine ND ug/L 10/13/22 23:58 62-75-910/12/22 16:179.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 10/13/22 23:58 621-64-710/12/22 16:179.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 10/13/22 23:58 86-30-610/12/22 16:179.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/13/22 23:58 108-60-1 v110/12/22 16:179.1 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-8 Lab ID:92630198008 Collected:10/07/22 16:30 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Pentachlorophenol ND ug/L 10/13/22 23:58 87-86-510/12/22 16:1718.2 3.4 1
Phenanthrene ND ug/L 10/13/22 23:58 85-01-810/12/22 16:179.1 1.8 1
Phenol ND ug/L 10/13/22 23:58 108-95-210/12/22 16:179.1 1.2 1
Pyrene ND ug/L 10/13/22 23:58 129-00-010/12/22 16:179.1 2.0 1
Pyridine ND ug/L 10/13/22 23:58 110-86-110/12/22 16:179.1 2.4 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 23:58 120-82-110/12/22 16:179.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 10/13/22 23:58 95-95-410/12/22 16:179.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 10/13/22 23:58 88-06-210/12/22 16:179.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)16 %10/13/22 23:58 4165-60-010/12/22 16:1710-144 1
2-Fluorobiphenyl (S)7 %10/13/22 23:58 321-60-8 S010/12/22 16:1710-130 1
Terphenyl-d14 (S)139 %10/13/22 23:58 1718-51-010/12/22 16:1734-163 1
Phenol-d6 (S)17 %10/13/22 23:58 13127-88-310/12/22 16:1710-130 1
2-Fluorophenol (S)16 %10/13/22 23:58 367-12-410/12/22 16:1710-130 1
2,4,6-Tribromophenol (S)97 %10/13/22 23:58 118-79-610/12/22 16:1710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/13/22 22:31 67-64-125.0 5.1 1
Benzene ND ug/L 10/13/22 22:31 71-43-21.0 0.34 1
Bromobenzene ND ug/L 10/13/22 22:31 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 10/13/22 22:31 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/13/22 22:31 75-27-41.0 0.31 1
Bromoform ND ug/L 10/13/22 22:31 75-25-2 IK1.0 0.34 1
Bromomethane ND ug/L 10/13/22 22:31 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/13/22 22:31 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 10/13/22 22:31 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/13/22 22:31 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/13/22 22:31 75-00-31.0 0.65 1
Chloroform ND ug/L 10/13/22 22:31 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/13/22 22:31 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/13/22 22:31 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 10/13/22 22:31 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/22 22:31 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/13/22 22:31 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/22 22:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/13/22 22:31 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/13/22 22:31 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/13/22 22:31 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/13/22 22:31 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/13/22 22:31 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/13/22 22:31 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/13/22 22:31 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/13/22 22:31 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/13/22 22:31 156-59-21.0 0.38 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Sample:GW-8 Lab ID:92630198008 Collected:10/07/22 16:30 Received:10/10/22 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
trans-1,2-Dichloroethene ND ug/L 10/13/22 22:31 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/13/22 22:31 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 10/13/22 22:31 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 10/13/22 22:31 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 10/13/22 22:31 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/13/22 22:31 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/13/22 22:31 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 10/13/22 22:31 108-20-3 IK1.0 0.31 1
Ethylbenzene ND ug/L 10/13/22 22:31 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/13/22 22:31 87-68-32.0 1.5 1
2-Hexanone ND ug/L 10/13/22 22:31 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 10/13/22 22:31 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 10/13/22 22:31 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/22 22:31 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/13/22 22:31 1634-04-41.0 0.42 1
Naphthalene ND ug/L 10/13/22 22:31 91-20-31.0 0.64 1
Styrene ND ug/L 10/13/22 22:31 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/22 22:31 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/22 22:31 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/13/22 22:31 127-18-41.0 0.29 1
Toluene ND ug/L 10/13/22 22:31 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/13/22 22:31 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/13/22 22:31 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/13/22 22:31 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/13/22 22:31 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/13/22 22:31 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/13/22 22:31 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/13/22 22:31 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/13/22 22:31 108-05-4 IK2.0 1.3 1
Vinyl chloride ND ug/L 10/13/22 22:31 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/13/22 22:31 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 10/13/22 22:31 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/13/22 22:31 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)89 %10/13/22 22:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)85 %10/13/22 22:31 17060-07-070-130 1
Toluene-d8 (S)111 %10/13/22 22:31 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 10/19/22 10:17 18540-29-910/19/22 10:170.500 0.150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
730072
EPA 3010A
EPA 6010D
6010D ATL
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3801632
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 30.0 10/13/22 20:1926.2
Barium ug/L ND 10.0 10/13/22 20:191.3
Cadmium ug/L ND 10.0 10/13/22 20:192.7
Chromium ug/L ND 10.0 10/13/22 20:193.6
Lead ug/L ND 20.0 10/13/22 20:1919.0
Selenium ug/L ND 40.0 10/13/22 20:1931.1
Silver ug/L ND 10.0 10/13/22 20:194.6
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3801633LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 10501000 105 80-120
Barium ug/L 10501000 105 80-120
Cadmium ug/L 10601000 106 80-120
Chromium ug/L 10701000 107 80-120
Lead ug/L 10501000 105 80-120
Selenium ug/L 10701000 107 80-120
Silver ug/L 10401000 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3801634MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630198001
3801635
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 1000 105 75-125101 4 201000ND10501010
Barium ug/L 1000 106 75-125104 1 20100028.6 1180 1160
Cadmium ug/L 1000 105 75-125102 3 201000ND10501020
Chromium ug/L 1000 107 75-125105 1 201000ND10701060
Lead ug/L 1000 107 75-125105 2 201000ND10901070
Selenium ug/L 1000 106 75-125105 1 201000ND10601050
Silver ug/L 1000 102 75-125100 2 201000ND10201000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
730284
EPA 3010A
EPA 6010D
6010 MET Filtered Diss.
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3802525
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Matrix:Water
AnalyzedMDL
Arsenic, Dissolved ug/L ND 30.0 10/14/22 18:4926.2
Barium, Dissolved ug/L ND 10.0 10/14/22 18:491.3
Cadmium, Dissolved ug/L ND 10.0 10/14/22 18:492.7
Chromium, Dissolved ug/L ND 10.0 10/14/22 18:493.6
Lead, Dissolved ug/L ND 20.0 10/14/22 18:4919.0
Selenium, Dissolved ug/L ND 40.0 10/14/22 18:4931.1
Silver, Dissolved ug/L ND 10.0 10/14/22 18:494.6
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3802544
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Matrix:Water
AnalyzedMDL
Arsenic, Dissolved ug/L ND 30.0 10/14/22 18:5926.2
Barium, Dissolved ug/L ND 10.0 10/14/22 18:591.3
Cadmium, Dissolved ug/L ND 10.0 10/14/22 18:592.7
Chromium, Dissolved ug/L ND 10.0 10/14/22 18:593.6
Lead, Dissolved ug/L ND 20.0 10/14/22 18:5919.0
Selenium, Dissolved ug/L ND 40.0 10/14/22 18:5931.1
Silver, Dissolved ug/L ND 10.0 10/14/22 18:594.6
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3802526LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic, Dissolved ug/L 10201000 102 80-120
Barium, Dissolved ug/L 9911000 99 80-120
Cadmium, Dissolved ug/L 10301000 103 80-120
Chromium, Dissolved ug/L 10001000 100 80-120
Lead, Dissolved ug/L 9941000 99 80-120
Selenium, Dissolved ug/L 9971000 100 80-120
Silver, Dissolved ug/L 9871000 99 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3802545LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic, Dissolved ug/L 10101000 101 80-120
Barium, Dissolved ug/L 9971000 100 80-120
Cadmium, Dissolved ug/L 10201000 102 80-120
Chromium, Dissolved ug/L 10101000 101 80-120
Lead, Dissolved ug/L 10001000 100 80-120
Selenium, Dissolved ug/L 9951000 99 80-120
Silver, Dissolved ug/L 9861000 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3802542MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630341002
3802543
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic, Dissolved ug/L 1000 100 75-125103 3 201000ND9961030
Barium, Dissolved ug/L 1000 99 75-125101 2 20100086.1 1080 1100
Cadmium, Dissolved ug/L 1000 100 75-125103 3 201000ND9991030
Chromium, Dissolved ug/L 1000 98 75-125100 2 201000ND9851000
Lead, Dissolved ug/L 1000 97 75-125100 3 201000ND9811010
Selenium, Dissolved ug/L 1000 98 75-125100 2 201000ND9851000
Silver, Dissolved ug/L 1000 96 75-12599 2 201000ND962985
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
730765
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3804947
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/18/22 09:220.13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3804948LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.22.5 86 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3804949MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630865003
3804950
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 82 75-12579 4 202.5ND 2.1 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
730657
EPA 7470A
EPA 7470A
7470 Mercury Dissolved
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3804156
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Matrix:Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 10/17/22 15:100.13
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3804160
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Matrix:Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 10/17/22 16:030.13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3804157LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.22.5 89 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3804161LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.12.5 85 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3804158MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630198001
3804159
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L M12.5 74 75-12574 0 202.5ND 1.9 1.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729189
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3797515
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/13/22 19:550.31
1,1,1-Trichloroethane ug/L ND 1.0 10/13/22 19:550.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/13/22 19:550.22
1,1,2-Trichloroethane ug/L ND 1.0 10/13/22 19:550.32
1,1-Dichloroethane ug/L ND 1.0 10/13/22 19:550.37
1,1-Dichloroethene ug/L ND 1.0 10/13/22 19:550.35
1,1-Dichloropropene ug/L ND 1.0 10/13/22 19:550.43
1,2,3-Trichlorobenzene ug/L ND 1.0 10/13/22 19:550.81
1,2,3-Trichloropropane ug/L ND 1.0 10/13/22 19:550.26
1,2,4-Trichlorobenzene ug/L ND 1.0 10/13/22 19:550.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/13/22 19:550.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/13/22 19:550.27
1,2-Dichlorobenzene ug/L ND 1.0 10/13/22 19:550.34
1,2-Dichloroethane ug/L ND 1.0 10/13/22 19:550.32
1,2-Dichloropropane ug/L ND 1.0 10/13/22 19:550.36
1,3-Dichlorobenzene ug/L ND 1.0 10/13/22 19:550.34
1,3-Dichloropropane ug/L ND 1.0 10/13/22 19:550.28
1,4-Dichlorobenzene ug/L ND 1.0 10/13/22 19:550.33
2,2-Dichloropropane ug/L ND 1.0 10/13/22 19:550.39
2-Butanone (MEK)ug/L ND 5.0 10/13/22 19:554.0
2-Chlorotoluene ug/L ND 1.0 10/13/22 19:550.32
2-Hexanone ug/L ND 5.0 10/13/22 19:550.48
4-Chlorotoluene ug/L ND 1.0 10/13/22 19:550.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/13/22 19:552.7
Acetone ug/L ND 25.0 10/13/22 19:555.1
Benzene ug/L ND 1.0 10/13/22 19:550.34
Bromobenzene ug/L ND 1.0 10/13/22 19:550.29
Bromochloromethane ug/L ND 1.0 10/13/22 19:550.47
Bromodichloromethane ug/L ND 1.0 10/13/22 19:550.31
Bromoform ug/L ND 1.0 IK10/13/22 19:550.34
Bromomethane ug/L ND 2.0 10/13/22 19:551.7
Carbon tetrachloride ug/L ND 1.0 10/13/22 19:550.33
Chlorobenzene ug/L ND 1.0 10/13/22 19:550.28
Chloroethane ug/L ND 1.0 10/13/22 19:550.65
Chloroform ug/L ND 1.0 10/13/22 19:550.43
Chloromethane ug/L ND 1.0 10/13/22 19:550.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/13/22 19:550.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/13/22 19:550.36
Dibromochloromethane ug/L ND 1.0 10/13/22 19:550.36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3797515
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 1.0 10/13/22 19:550.39
Dichlorodifluoromethane ug/L ND 1.0 10/13/22 19:550.35
Diisopropyl ether ug/L ND 1.0 IK10/13/22 19:550.31
Ethylbenzene ug/L ND 1.0 10/13/22 19:550.30
Hexachloro-1,3-butadiene ug/L ND 2.0 10/13/22 19:551.5
m&p-Xylene ug/L ND 2.0 10/13/22 19:550.71
Methyl-tert-butyl ether ug/L ND 1.0 10/13/22 19:550.42
Methylene Chloride ug/L 2.9J 5.0 10/13/22 19:552.0
Naphthalene ug/L ND 1.0 10/13/22 19:550.64
o-Xylene ug/L ND 1.0 10/13/22 19:550.34
p-Isopropyltoluene ug/L ND 1.0 10/13/22 19:550.41
Styrene ug/L ND 1.0 10/13/22 19:550.29
Tetrachloroethene ug/L ND 1.0 10/13/22 19:550.29
Toluene ug/L ND 1.0 10/13/22 19:550.24
trans-1,2-Dichloroethene ug/L ND 1.0 10/13/22 19:550.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/13/22 19:550.36
Trichloroethene ug/L ND 1.0 10/13/22 19:550.38
Trichlorofluoromethane ug/L ND 1.0 10/13/22 19:550.30
Vinyl acetate ug/L ND 2.0 IK10/13/22 19:551.3
Vinyl chloride ug/L ND 1.0 10/13/22 19:550.39
Xylene (Total)ug/L ND 1.0 10/13/22 19:550.34
1,2-Dichloroethane-d4 (S)%85 70-130 10/13/22 19:55
4-Bromofluorobenzene (S)%89 70-130 10/13/22 19:55
Toluene-d8 (S)%109 70-130 10/13/22 19:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3797516LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.950 108 70-130
1,1,1-Trichloroethane ug/L 51.350 103 70-130
1,1,2,2-Tetrachloroethane ug/L 48.950 98 70-130
1,1,2-Trichloroethane ug/L 51.550 103 70-130
1,1-Dichloroethane ug/L 46.250 92 70-130
1,1-Dichloroethene ug/L 44.650 89 70-130
1,1-Dichloropropene ug/L 53.450 107 70-130
1,2,3-Trichlorobenzene ug/L 57.150 114 70-130
1,2,3-Trichloropropane ug/L 48.250 96 70-130
1,2,4-Trichlorobenzene ug/L 55.050 110 70-130
1,2-Dibromo-3-chloropropane ug/L 50.350 101 70-131
1,2-Dibromoethane (EDB)ug/L 54.550 109 70-130
1,2-Dichlorobenzene ug/L 52.150 104 70-130
1,2-Dichloroethane ug/L 50.050 100 70-130
1,2-Dichloropropane ug/L 51.450 103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3797516LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 51.450 103 70-130
1,3-Dichloropropane ug/L 54.450 109 70-130
1,4-Dichlorobenzene ug/L 49.150 98 70-130
2,2-Dichloropropane ug/L 53.450 107 68-135
2-Butanone (MEK)ug/L 96.2100 96 70-134
2-Chlorotoluene ug/L 49.250 98 70-130
2-Hexanone ug/L 97.1100 97 70-131
4-Chlorotoluene ug/L 50.050 100 70-130
4-Methyl-2-pentanone (MIBK)ug/L 91.3100 91 70-130
Acetone ug/L 88.6100 89 70-133
Benzene ug/L 49.350 99 70-130
Bromobenzene ug/L 48.350 97 70-130
Bromochloromethane ug/L 49.350 99 70-130
Bromodichloromethane ug/L 54.150 108 70-130
Bromoform ug/L 57.5 IK5011570-130
Bromomethane ug/L 64.850 130 45-151
Carbon tetrachloride ug/L 52.150 104 70-130
Chlorobenzene ug/L 50.150 100 70-130
Chloroethane ug/L 49.450 99 39-152
Chloroform ug/L 48.650 97 70-130
Chloromethane ug/L 46.950 94 58-130
cis-1,2-Dichloroethene ug/L 46.150 92 70-130
cis-1,3-Dichloropropene ug/L 55.750 111 70-130
Dibromochloromethane ug/L 56.750 113 70-130
Dibromomethane ug/L 49.750 99 70-130
Dichlorodifluoromethane ug/L 43.550 87 54-133
Diisopropyl ether ug/L 45.4 IK509170-130
Ethylbenzene ug/L 50.050 100 70-130
Hexachloro-1,3-butadiene ug/L 50.550 101 70-135
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 54.650 109 70-130
Methylene Chloride ug/L 46.250 92 66-130
Naphthalene ug/L 58.850 118 70-130
o-Xylene ug/L 49.750 99 70-130
p-Isopropyltoluene ug/L 51.050 102 70-130
Styrene ug/L 53.350 107 70-130
Tetrachloroethene ug/L 49.650 99 70-130
Toluene ug/L 45.250 90 70-130
trans-1,2-Dichloroethene ug/L 45.950 92 70-130
trans-1,3-Dichloropropene ug/L 54.150 108 70-130
Trichloroethene ug/L 53.750 107 70-130
Trichlorofluoromethane ug/L 43.750 87 62-130
Vinyl acetate ug/L 89.5 IK1008970-144
Vinyl chloride ug/L 44.850 90 62-130
Xylene (Total)ug/L 151150 100 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3797516LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%92 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3801930MATRIX SPIKE SAMPLE:
MSSpike
Result
92629993005
1,1,1,2-Tetrachloroethane ug/L 14.020 70 70-141ND
1,1,1-Trichloroethane ug/L 16.120 80 70-150ND
1,1,2,2-Tetrachloroethane ug/L 14.720 74 69-142ND
1,1,2-Trichloroethane ug/L 15.320 76 70-138ND
1,1-Dichloroethane ug/L 16.320 81 70-150ND
1,1-Dichloroethene ug/L 16.220 81 70-156ND
1,1-Dichloropropene ug/L 15.420 77 70-150ND
1,2,3-Trichlorobenzene ug/L 16.220 81 70-148ND
1,2,3-Trichloropropane ug/L 13.7 M1206970-140ND
1,2,4-Trichlorobenzene ug/L 16.020 80 70-146ND
1,2-Dibromo-3-chloropropane ug/L 15.220 76 68-146ND
1,2-Dibromoethane (EDB)ug/L 14.320 71 70-138ND
1,2-Dichlorobenzene ug/L 16.720 83 70-141ND
1,2-Dichloroethane ug/L 16.220 81 69-143ND
1,2-Dichloropropane ug/L 15.220 76 68-156ND
1,3-Dichlorobenzene ug/L 16.920 84 70-143ND
1,3-Dichloropropane ug/L 14.720 73 70-138ND
1,4-Dichlorobenzene ug/L 15.720 79 70-142ND
2,2-Dichloropropane ug/L 13.820 69 52-170ND
2-Butanone (MEK)ug/L 28.740 72 60-157ND
2-Chlorotoluene ug/L 15.820 79 70-147ND
2-Hexanone ug/L 26.8 M1406768-146ND
4-Chlorotoluene ug/L 15.520 78 70-142ND
4-Methyl-2-pentanone (MIBK)ug/L 26.5 M1406670-141ND
Acetone ug/L 32.640 81 58-157ND
Benzene ug/L 15.620 78 70-142ND
Bromobenzene ug/L 15.220 76 70-143ND
Bromochloromethane ug/L 17.720 88 70-146ND
Bromodichloromethane ug/L 16.120 80 70-139ND
Bromoform ug/L 14.0 IK207064-140ND
Bromomethane ug/L 20.5 v12010228-192ND
Carbon tetrachloride ug/L 17.320 87 70-148ND
Chlorobenzene ug/L 15.520 77 70-141ND
Chloroethane ug/L 17.820 89 58-191ND
Chloroform ug/L 15.920 80 70-148ND
Chloromethane ug/L 14.020 70 43-162ND
cis-1,2-Dichloroethene ug/L 16.420 82 68-151ND
cis-1,3-Dichloropropene ug/L 13.920 70 70-139ND
Dibromochloromethane ug/L 14.120 71 70-144ND
Dibromomethane ug/L 16.720 84 70-139ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3801930MATRIX SPIKE SAMPLE:
MSSpike
Result
92629993005
Dichlorodifluoromethane ug/L 14.720 74 39-171ND
Diisopropyl ether ug/L 13.1 IK,M1206667-142ND
Ethylbenzene ug/L 15.520 78 70-143ND
Hexachloro-1,3-butadiene ug/L 15.920 79 64-163ND
m&p-Xylene ug/L 30.940 77 70-144ND
Methyl-tert-butyl ether ug/L 13.620 68 65-143ND
Methylene Chloride ug/L 17.020 85 62-149ND
Naphthalene ug/L 15.620 78 67-147ND
o-Xylene ug/L 14.920 75 70-145ND
p-Isopropyltoluene ug/L 16.120 80 70-147ND
Styrene ug/L 15.720 78 70-143ND
Tetrachloroethene ug/L 15.220 76 70-145ND
Toluene ug/L 16.320 82 70-142ND
trans-1,2-Dichloroethene ug/L 16.720 84 70-151ND
trans-1,3-Dichloropropene ug/L 13.6 M1206870-139ND
Trichloroethene ug/L 16.420 82 62-146ND
Trichlorofluoromethane ug/L 16.020 80 63-153ND
Vinyl acetate ug/L 21.4 IK,M1405361-162ND
Vinyl chloride ug/L 16.120 81 61-163ND
Xylene (Total)ug/L 45.860 76 70-143ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92629993007
3801929SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92629993007
3801929SAMPLE DUPLICATE:
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND IK30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND IK30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L 1.0J 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L 0.49J 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND IK30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%8387
4-Bromofluorobenzene (S)%8988
Toluene-d8 (S)%112107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729659
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92630198001, 92630198003, 92630198004, 92630198005, 92630198006, 92630198008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3799430
Associated Lab Samples:92630198001, 92630198003, 92630198004, 92630198005, 92630198006, 92630198008
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 10/13/22 16:431.7
1,2-Dichlorobenzene ug/L ND 10.0 10/13/22 16:431.8
1,3-Dichlorobenzene ug/L ND 10.0 10/13/22 16:431.6
1,4-Dichlorobenzene ug/L ND 10.0 10/13/22 16:431.7
1-Methylnaphthalene ug/L ND 10.0 10/13/22 16:432.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 v110/13/22 16:431.2
2,4,5-Trichlorophenol ug/L ND 10.0 10/13/22 16:431.4
2,4,6-Trichlorophenol ug/L ND 10.0 10/13/22 16:431.6
2,4-Dichlorophenol ug/L ND 10.0 10/13/22 16:431.4
2,4-Dimethylphenol ug/L ND 10.0 10/13/22 16:431.7
2,4-Dinitrophenol ug/L ND 50.0 10/13/22 16:4326.0
2,4-Dinitrotoluene ug/L ND 10.0 10/13/22 16:431.6
2,6-Dinitrotoluene ug/L ND 10.0 10/13/22 16:431.7
2-Chloronaphthalene ug/L ND 10.0 10/13/22 16:431.7
2-Chlorophenol ug/L ND 10.0 10/13/22 16:431.2
2-Methylnaphthalene ug/L ND 10.0 10/13/22 16:431.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 10/13/22 16:431.9
2-Nitroaniline ug/L ND 20.0 10/13/22 16:433.0
2-Nitrophenol ug/L ND 10.0 10/13/22 16:431.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 10/13/22 16:431.2
3,3'-Dichlorobenzidine ug/L ND 20.0 10/13/22 16:438.1
3-Nitroaniline ug/L ND 20.0 10/13/22 16:433.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 10/13/22 16:437.8
4-Bromophenylphenyl ether ug/L ND 10.0 10/13/22 16:431.8
4-Chloro-3-methylphenol ug/L ND 10.0 10/13/22 16:433.3
4-Chloroaniline ug/L ND 20.0 10/13/22 16:433.6
4-Chlorophenylphenyl ether ug/L ND 10.0 10/13/22 16:432.0
4-Nitroaniline ug/L ND 20.0 10/13/22 16:435.1
4-Nitrophenol ug/L ND 50.0 10/13/22 16:436.6
Acenaphthene ug/L ND 10.0 10/13/22 16:432.0
Acenaphthylene ug/L ND 10.0 10/13/22 16:432.0
Aniline ug/L ND 10.0 10/13/22 16:431.6
Anthracene ug/L ND 10.0 10/13/22 16:432.3
Benzo(a)anthracene ug/L ND 10.0 10/13/22 16:432.7
Benzo(a)pyrene ug/L ND 10.0 10/13/22 16:432.8
Benzo(b)fluoranthene ug/L ND 10.0 10/13/22 16:432.6
Benzo(g,h,i)perylene ug/L ND 10.0 10/13/22 16:432.8
Benzo(k)fluoranthene ug/L ND 10.0 10/13/22 16:432.7
Benzoic Acid ug/L ND 50.0 10/13/22 16:4322.0
Benzyl alcohol ug/L ND 20.0 10/13/22 16:432.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3799430
Associated Lab Samples:92630198001, 92630198003, 92630198004, 92630198005, 92630198006, 92630198008
Matrix:Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 10/13/22 16:431.8
bis(2-Chloroethyl) ether ug/L ND 10.0 10/13/22 16:431.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 10/13/22 16:433.7
Butylbenzylphthalate ug/L ND 10.0 10/13/22 16:433.1
Chrysene ug/L ND 10.0 10/13/22 16:432.8
Di-n-butylphthalate ug/L ND 10.0 10/13/22 16:432.2
Di-n-octylphthalate ug/L ND 10.0 10/13/22 16:433.9
Dibenz(a,h)anthracene ug/L ND 10.0 10/13/22 16:433.0
Dibenzofuran ug/L ND 10.0 10/13/22 16:432.1
Diethylphthalate ug/L ND 10.0 10/13/22 16:432.0
Dimethylphthalate ug/L ND 10.0 10/13/22 16:432.1
Fluoranthene ug/L ND 10.0 10/13/22 16:432.2
Fluorene ug/L ND 10.0 10/13/22 16:432.1
Hexachloro-1,3-butadiene ug/L ND 10.0 10/13/22 16:431.8
Hexachlorobenzene ug/L ND 10.0 10/13/22 16:432.2
Hexachlorocyclopentadiene ug/L ND 10.0 10/13/22 16:431.6
Hexachloroethane ug/L ND 10.0 10/13/22 16:431.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 10/13/22 16:432.9
Isophorone ug/L ND 10.0 10/13/22 16:431.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 10/13/22 16:431.3
N-Nitrosodimethylamine ug/L ND 10.0 10/13/22 16:431.9
N-Nitrosodiphenylamine ug/L ND 10.0 10/13/22 16:433.0
Naphthalene ug/L ND 10.0 10/13/22 16:432.1
Nitrobenzene ug/L ND 10.0 10/13/22 16:431.9
Pentachlorophenol ug/L ND 20.0 10/13/22 16:433.8
Phenanthrene ug/L ND 10.0 10/13/22 16:432.0
Phenol ug/L ND 10.0 10/13/22 16:431.4
Pyrene ug/L ND 10.0 10/13/22 16:432.2
Pyridine ug/L ND 10.0 10/13/22 16:432.6
2,4,6-Tribromophenol (S)%84 10-144 10/13/22 16:43
2-Fluorobiphenyl (S)%74 10-130 10/13/22 16:43
2-Fluorophenol (S)%61 10-130 10/13/22 16:43
Nitrobenzene-d5 (S)%83 10-144 10/13/22 16:43
Phenol-d6 (S)%45 10-130 10/13/22 16:43
Terphenyl-d14 (S)%105 34-163 10/13/22 16:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799431LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 34.550 69 18-130
1,2-Dichlorobenzene ug/L 29.450 59 20-130
1,3-Dichlorobenzene ug/L 25.950 52 18-130
1,4-Dichlorobenzene ug/L 26.550 53 18-130
1-Methylnaphthalene ug/L 43.450 87 29-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
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Page 51 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799431LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 45.9 v1509228-130
2,4,5-Trichlorophenol ug/L 46.350 93 35-130
2,4,6-Trichlorophenol ug/L 45.750 91 31-130
2,4-Dichlorophenol ug/L 43.950 88 35-130
2,4-Dimethylphenol ug/L 50.250 100 34-130
2,4-Dinitrophenol ug/L 195250 78 10-153
2,4-Dinitrotoluene ug/L 51.050 102 37-136
2,6-Dinitrotoluene ug/L 50.550 101 33-136
2-Chloronaphthalene ug/L 44.150 88 26-130
2-Chlorophenol ug/L 39.950 80 37-130
2-Methylnaphthalene ug/L 42.350 85 29-130
2-Methylphenol(o-Cresol)ug/L 39.350 79 35-130
2-Nitroaniline ug/L 90.6100 91 37-130
2-Nitrophenol ug/L 41.650 83 32-130
3&4-Methylphenol(m&p Cresol)ug/L 38.250 76 34-130
3,3'-Dichlorobenzidine ug/L 90.4100 90 34-136
3-Nitroaniline ug/L 97.6100 98 37-138
4,6-Dinitro-2-methylphenol ug/L 94.7100 95 21-157
4-Bromophenylphenyl ether ug/L 44.450 89 38-130
4-Chloro-3-methylphenol ug/L 89.5100 89 37-130
4-Chloroaniline ug/L 87.9100 88 38-130
4-Chlorophenylphenyl ether ug/L 44.150 88 33-130
4-Nitroaniline ug/L 94.1100 94 42-137
4-Nitrophenol ug/L 145250 58 10-130
Acenaphthene ug/L 46.350 93 33-130
Acenaphthylene ug/L 45.550 91 35-130
Aniline ug/L 35.550 71 22-130
Anthracene ug/L 43.950 88 48-130
Benzo(a)anthracene ug/L 47.150 94 48-137
Benzo(a)pyrene ug/L 48.050 96 49-138
Benzo(b)fluoranthene ug/L 48.850 98 52-138
Benzo(g,h,i)perylene ug/L 49.350 99 48-140
Benzo(k)fluoranthene ug/L 48.750 97 48-139
Benzoic Acid ug/L 96.6250 39 10-130
Benzyl alcohol ug/L 80.7100 81 35-130
bis(2-Chloroethoxy)methane ug/L 42.350 85 34-130
bis(2-Chloroethyl) ether ug/L 41.350 83 36-130
bis(2-Ethylhexyl)phthalate ug/L 51.850 104 32-165
Butylbenzylphthalate ug/L 53.150 106 34-161
Chrysene ug/L 47.750 95 47-131
Di-n-butylphthalate ug/L 47.950 96 39-144
Di-n-octylphthalate ug/L 52.850 106 30-170
Dibenz(a,h)anthracene ug/L 47.750 95 49-138
Dibenzofuran ug/L 46.650 93 33-130
Diethylphthalate ug/L 49.050 98 38-131
Dimethylphthalate ug/L 47.150 94 37-130
Fluoranthene ug/L 49.050 98 46-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
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Huntersville, NC 28078
[phone]
Page 52 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799431LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/L 48.350 97 37-130
Hexachloro-1,3-butadiene ug/L 29.150 58 11-130
Hexachlorobenzene ug/L 44.550 89 38-130
Hexachlorocyclopentadiene ug/L 33.650 67 10-130
Hexachloroethane ug/L 26.050 52 14-130
Indeno(1,2,3-cd)pyrene ug/L 49.950 100 41-130
Isophorone ug/L 45.550 91 33-130
N-Nitroso-di-n-propylamine ug/L 46.250 92 36-130
N-Nitrosodimethylamine ug/L 36.550 73 34-130
N-Nitrosodiphenylamine ug/L 47.950 96 37-130
Naphthalene ug/L 37.050 74 30-130
Nitrobenzene ug/L 41.650 83 36-130
Pentachlorophenol ug/L 92.0100 92 23-149
Phenanthrene ug/L 48.550 97 44-130
Phenol ug/L 28.550 57 18-130
Pyrene ug/L 50.350 101 47-134
Pyridine ug/L 32.750 65 10-130
2,4,6-Tribromophenol (S)%107 10-144
2-Fluorobiphenyl (S)%91 10-130
2-Fluorophenol (S)%71 10-130
Nitrobenzene-d5 (S)%92 10-144
Phenol-d6 (S)%60 10-130
Terphenyl-d14 (S)%113 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799432MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92627310005
3799433
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 50 10-13059 16 3050ND25.0 29.4
1,2-Dichlorobenzene ug/L 50 39 10-13047 21 3050ND19.3 23.7
1,3-Dichlorobenzene ug/L 50 34 10-13041 19 3050ND16.8 20.3
1,4-Dichlorobenzene ug/L 50 35 10-13042 19 3050ND17.4 21.1
1-Methylnaphthalene ug/L 50 62 10-13071 13 3050ND31.0 35.4
2,2'-Oxybis(1-
chloropropane)ug/L 50 58 12-14266 13 3050ND28.8 33.0
2,4,5-Trichlorophenol ug/L R1503310-14345 32 3050ND16.3 22.6
2,4,6-Trichlorophenol ug/L 50 17 10-14724 3050ND8.3J 12.1
2,4-Dichlorophenol ug/L 50 45 10-13858 26 3050ND22.4 29.0
2,4-Dimethylphenol ug/L 50 85 25-130104 19 3050ND42.6 51.8
2,4-Dinitrophenol ug/L M1250010-1650 30250NDNDND
2,4-Dinitrotoluene ug/L 50 85 29-148102 19 3050ND42.4 51.1
2,6-Dinitrotoluene ug/L 50 86 26-146102 18 3050ND42.9 51.2
2-Chloronaphthalene ug/L 50 73 11-13079 9 3050ND36.4 39.7
2-Chlorophenol ug/L 50 44 10-13357 25 3050ND22.1 28.4
2-Methylnaphthalene ug/L 50 61 13-13069 12 3050ND30.6 34.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799432MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92627310005
3799433
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Methylphenol(o-Cresol)ug/L 50 57 20-13070 20 3050ND28.6 35.2
2-Nitroaniline ug/L 100 80 24-13695 18 30100ND79.5 95.2
2-Nitrophenol ug/L 50 52 10-15367 24 3050ND26.2 33.4
3&4-Methylphenol(m&p
Cresol)ug/L 50 53 16-13067 24 3050ND26.4 33.7
3,3'-Dichlorobenzidine ug/L 100 73 10-153100 30 30100ND73.4 99.8
3-Nitroaniline ug/L 100 67 22-15191 30 30100ND67.5 91.1
4,6-Dinitro-2-methylphenol ug/L M1100710-1809 30100NDND8.9J
4-Bromophenylphenyl ether ug/L 50 78 25-13087 11 3050ND38.8 43.3
4-Chloro-3-methylphenol ug/L 100 66 25-13380 20 30100ND65.8 80.2
4-Chloroaniline ug/L 100 50 14-13265 26 30100ND50.2 65.0
4-Chlorophenylphenyl ether ug/L 50 74 19-13088 18 3050ND36.8 44.0
4-Nitroaniline ug/L 100 65 29-15089 30 30100ND65.4 88.9
4-Nitrophenol ug/L M1250010-1300 30250NDNDND
Acenaphthene ug/L 50 73 16-13084 13 3050ND36.7 41.9
Acenaphthylene ug/L 50 74 15-13783 12 3050ND36.8 41.7
Aniline ug/L R1503210-13045 33 3050ND16.0 22.4
Anthracene ug/L 50 72 37-13686 18 3050ND36.0 43.0
Benzo(a)anthracene ug/L 50 87 40-145100 14 3050ND43.5 50.1
Benzo(a)pyrene ug/L 50 88 41-146100 13 3050ND44.1 50.2
Benzo(b)fluoranthene ug/L 50 86 39-151100 15 3050ND43.0 50.0
Benzo(g,h,i)perylene ug/L 50 111 40-147131 17 3050ND55.3 65.6
Benzo(k)fluoranthene ug/L 50 87 40-14695 9 3050ND43.6 47.6
Benzoic Acid ug/L M1250010-1300 30250NDNDND
Benzyl alcohol ug/L 100 58 25-13069 17 30100ND58.1 68.6
bis(2-
Chloroethoxy)methane ug/L 50 60 23-13070 15 3050ND30.1 34.9
bis(2-Chloroethyl) ether ug/L 50 56 25-13067 18 3050ND27.9 33.4
bis(2-Ethylhexyl)phthalate ug/L 50 109 28-166119 9 3050ND54.3 59.6
Butylbenzylphthalate ug/L 50 111 33-165123 10 3050ND55.7 61.7
Chrysene ug/L 50 87 38-141102 15 3050ND43.5 50.8
Di-n-butylphthalate ug/L 50 96 32-153112 16 3050ND47.8 55.9
Di-n-octylphthalate ug/L 50 103 30-175114 10 3050ND51.4 57.1
Dibenz(a,h)anthracene ug/L 50 104 39-148125 19 3050ND52.0 62.7
Dibenzofuran ug/L 50 73 20-13087 18 3050ND36.6 43.7
Diethylphthalate ug/L 50 87 28-142101 15 3050ND43.3 50.5
Dimethylphthalate ug/L 50 80 26-13696 18 3050ND40.0 47.9
Fluoranthene ug/L 50 87 39-143102 16 3050ND43.4 50.9
Fluorene ug/L 50 78 24-13290 15 3050ND38.9 45.2
Hexachloro-1,3-butadiene ug/L 50 43 10-13049 12 3050ND21.6 24.4
Hexachlorobenzene ug/L 50 78 29-13089 13 3050ND39.0 44.4
Hexachlorocyclopentadiene ug/L 50 33 10-13037 11 3050ND16.3 18.3
Hexachloroethane ug/L 50 32 10-13040 20 3050ND16.2 19.9
Indeno(1,2,3-cd)pyrene ug/L 50 106 39-148132 21 3050ND53.1 65.8
Isophorone ug/L 50 70 23-13079 13 3050ND34.8 39.7
N-Nitroso-di-n-propylamine ug/L 50 67 25-13078 14 3050ND33.7 38.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799432MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92627310005
3799433
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodimethylamine ug/L 50 55 22-13066 18 3050ND27.5 32.8
N-Nitrosodiphenylamine ug/L 50 72 26-13488 20 3050ND36.1 44.2
Naphthalene ug/L 50 56 14-13064 14 3050ND27.8 31.9
Nitrobenzene ug/L 50 66 25-13075 14 3050ND32.8 37.6
Pentachlorophenol ug/L M1100010-1752 30100NDNDND
Phenanthrene ug/L 50 81 36-13394 14 3050ND40.6 46.9
Phenol ug/L 50 37 10-13048 27 3050ND18.4 24.2
Pyrene ug/L 50 85 40-14395 11 3050ND42.6 47.6
Pyridine ug/L 50 52 10-13055 6 3050ND25.8 27.4
2,4,6-Tribromophenol (S)%29 10-14440
2-Fluorobiphenyl (S)%65 10-13072
2-Fluorophenol (S)%26 10-13037
Nitrobenzene-d5 (S)%67 10-14476
Phenol-d6 (S)%38 10-13049
Terphenyl-d14 (S)%98 34-163109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
730273
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92630198002, 92630198007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3802401
Associated Lab Samples:92630198002, 92630198007
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 10/14/22 15:181.7
1,2-Dichlorobenzene ug/L ND 10.0 10/14/22 15:181.8
1,3-Dichlorobenzene ug/L ND 10.0 10/14/22 15:181.6
1,4-Dichlorobenzene ug/L ND 10.0 10/14/22 15:181.7
1-Methylnaphthalene ug/L ND 10.0 10/14/22 15:182.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 10/14/22 15:181.2
2,4,5-Trichlorophenol ug/L ND 10.0 10/14/22 15:181.4
2,4,6-Trichlorophenol ug/L ND 10.0 10/14/22 15:181.6
2,4-Dichlorophenol ug/L ND 10.0 10/14/22 15:181.4
2,4-Dimethylphenol ug/L ND 10.0 10/14/22 15:181.7
2,4-Dinitrophenol ug/L ND 50.0 10/14/22 15:1826.0
2,4-Dinitrotoluene ug/L ND 10.0 10/14/22 15:181.6
2,6-Dinitrotoluene ug/L ND 10.0 10/14/22 15:181.7
2-Chloronaphthalene ug/L ND 10.0 10/14/22 15:181.7
2-Chlorophenol ug/L ND 10.0 10/14/22 15:181.2
2-Methylnaphthalene ug/L ND 10.0 10/14/22 15:181.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 10/14/22 15:181.9
2-Nitroaniline ug/L ND 20.0 10/14/22 15:183.0
2-Nitrophenol ug/L ND 10.0 v110/14/22 15:181.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 10/14/22 15:181.2
3,3'-Dichlorobenzidine ug/L ND 20.0 10/14/22 15:188.1
3-Nitroaniline ug/L ND 20.0 10/14/22 15:183.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 10/14/22 15:187.8
4-Bromophenylphenyl ether ug/L ND 10.0 10/14/22 15:181.8
4-Chloro-3-methylphenol ug/L ND 10.0 10/14/22 15:183.3
4-Chloroaniline ug/L ND 20.0 10/14/22 15:183.6
4-Chlorophenylphenyl ether ug/L ND 10.0 10/14/22 15:182.0
4-Nitroaniline ug/L ND 20.0 10/14/22 15:185.1
4-Nitrophenol ug/L ND 50.0 10/14/22 15:186.6
Acenaphthene ug/L ND 10.0 10/14/22 15:182.0
Acenaphthylene ug/L ND 10.0 10/14/22 15:182.0
Aniline ug/L ND 10.0 10/14/22 15:181.6
Anthracene ug/L ND 10.0 10/14/22 15:182.3
Benzo(a)anthracene ug/L ND 10.0 10/14/22 15:182.7
Benzo(a)pyrene ug/L ND 10.0 10/14/22 15:182.8
Benzo(b)fluoranthene ug/L ND 10.0 10/14/22 15:182.6
Benzo(g,h,i)perylene ug/L ND 10.0 10/14/22 15:182.8
Benzo(k)fluoranthene ug/L ND 10.0 10/14/22 15:182.7
Benzoic Acid ug/L ND 50.0 10/14/22 15:1822.0
Benzyl alcohol ug/L ND 20.0 10/14/22 15:182.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
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Huntersville, NC 28078
[phone]
Page 56 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3802401
Associated Lab Samples:92630198002, 92630198007
Matrix:Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 10/14/22 15:181.8
bis(2-Chloroethyl) ether ug/L ND 10.0 10/14/22 15:181.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 10/14/22 15:183.7
Butylbenzylphthalate ug/L ND 10.0 v110/14/22 15:183.1
Chrysene ug/L ND 10.0 10/14/22 15:182.8
Di-n-butylphthalate ug/L ND 10.0 10/14/22 15:182.2
Di-n-octylphthalate ug/L ND 10.0 10/14/22 15:183.9
Dibenz(a,h)anthracene ug/L ND 10.0 10/14/22 15:183.0
Dibenzofuran ug/L ND 10.0 10/14/22 15:182.1
Diethylphthalate ug/L ND 10.0 10/14/22 15:182.0
Dimethylphthalate ug/L ND 10.0 10/14/22 15:182.1
Fluoranthene ug/L ND 10.0 10/14/22 15:182.2
Fluorene ug/L ND 10.0 10/14/22 15:182.1
Hexachloro-1,3-butadiene ug/L ND 10.0 10/14/22 15:181.8
Hexachlorobenzene ug/L ND 10.0 10/14/22 15:182.2
Hexachlorocyclopentadiene ug/L ND 10.0 10/14/22 15:181.6
Hexachloroethane ug/L ND 10.0 10/14/22 15:181.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 10/14/22 15:182.9
Isophorone ug/L ND 10.0 10/14/22 15:181.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 10/14/22 15:181.3
N-Nitrosodimethylamine ug/L ND 10.0 10/14/22 15:181.9
N-Nitrosodiphenylamine ug/L ND 10.0 10/14/22 15:183.0
Naphthalene ug/L ND 10.0 10/14/22 15:182.1
Nitrobenzene ug/L ND 10.0 10/14/22 15:181.9
Pentachlorophenol ug/L ND 20.0 10/14/22 15:183.8
Phenanthrene ug/L ND 10.0 10/14/22 15:182.0
Phenol ug/L ND 10.0 10/14/22 15:181.4
Pyrene ug/L ND 10.0 10/14/22 15:182.2
Pyridine ug/L ND 10.0 10/14/22 15:182.6
2,4,6-Tribromophenol (S)%94 10-144 10/14/22 15:18
2-Fluorobiphenyl (S)%51 10-130 10/14/22 15:18
2-Fluorophenol (S)%60 10-130 10/14/22 15:18
Nitrobenzene-d5 (S)%78 10-144 10/14/22 15:18
Phenol-d6 (S)%48 10-130 10/14/22 15:18
Terphenyl-d14 (S)%102 34-163 10/14/22 15:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3802402LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 53.750 107 18-130
1,2-Dichlorobenzene ug/L 48.950 98 20-130
1,3-Dichlorobenzene ug/L 43.850 88 18-130
1,4-Dichlorobenzene ug/L 45.450 91 18-130
1-Methylnaphthalene ug/L 60.450 121 29-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3802402LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 58.950 118 28-130
2,4,5-Trichlorophenol ug/L 67.9 L15013635-130
2,4,6-Trichlorophenol ug/L 70.8 L15014231-130
2,4-Dichlorophenol ug/L 61.750 123 35-130
2,4-Dimethylphenol ug/L 86.4 L15017334-130
2,4-Dinitrophenol ug/L 328250 131 10-153
2,4-Dinitrotoluene ug/L 74.7 L15014937-136
2,6-Dinitrotoluene ug/L 78.3 L15015733-136
2-Chloronaphthalene ug/L 69.6 L15013926-130
2-Chlorophenol ug/L 57.750 115 37-130
2-Methylnaphthalene ug/L 59.950 120 29-130
2-Methylphenol(o-Cresol)ug/L 57.250 114 35-130
2-Nitroaniline ug/L 145 L110014537-130
2-Nitrophenol ug/L 71.3 L15014332-130
3&4-Methylphenol(m&p Cresol)ug/L 58.750 117 34-130
3,3'-Dichlorobenzidine ug/L 147 L110014734-136
3-Nitroaniline ug/L 153 L110015337-138
4,6-Dinitro-2-methylphenol ug/L 139100 139 21-157
4-Bromophenylphenyl ether ug/L 65.8 L15013238-130
4-Chloro-3-methylphenol ug/L 121100 121 37-130
4-Chloroaniline ug/L 126100 126 38-130
4-Chlorophenylphenyl ether ug/L 62.250 124 33-130
4-Nitroaniline ug/L 141 L110014142-137
4-Nitrophenol ug/L 203250 81 10-130
Acenaphthene ug/L 67.4 L15013533-130
Acenaphthylene ug/L 66.8 L15013435-130
Aniline ug/L 54.350 109 22-130
Anthracene ug/L 60.650 121 48-130
Benzo(a)anthracene ug/L 69.7 L15013948-137
Benzo(a)pyrene ug/L 67.750 135 49-138
Benzo(b)fluoranthene ug/L 77.6 L15015552-138
Benzo(g,h,i)perylene ug/L 74.6 L15014948-140
Benzo(k)fluoranthene ug/L 68.950 138 48-139
Benzoic Acid ug/L 193250 77 10-130
Benzyl alcohol ug/L 117100 117 35-130
bis(2-Chloroethoxy)methane ug/L 61.750 123 34-130
bis(2-Chloroethyl) ether ug/L 58.250 116 36-130
bis(2-Ethylhexyl)phthalate ug/L 80.250 160 32-165
Butylbenzylphthalate ug/L 86.7 L15017334-161
Chrysene ug/L 66.4 L15013347-131
Di-n-butylphthalate ug/L 74.2 L15014839-144
Di-n-octylphthalate ug/L 74.950 150 30-170
Dibenz(a,h)anthracene ug/L 74.0 L15014849-138
Dibenzofuran ug/L 65.8 L15013233-130
Diethylphthalate ug/L 67.0 L15013438-131
Dimethylphthalate ug/L 67.5 L15013537-130
Fluoranthene ug/L 64.250 128 46-137
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3802402LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/L 65.250 130 37-130
Hexachloro-1,3-butadiene ug/L 50.150 100 11-130
Hexachlorobenzene ug/L 66.6 L15013338-130
Hexachlorocyclopentadiene ug/L 68.3 L15013710-130
Hexachloroethane ug/L 44.750 89 14-130
Indeno(1,2,3-cd)pyrene ug/L 76.2 L15015241-130
Isophorone ug/L 65.7 L15013133-130
N-Nitroso-di-n-propylamine ug/L 63.950 128 36-130
N-Nitrosodimethylamine ug/L 54.650 109 34-130
N-Nitrosodiphenylamine ug/L 69.3 L15013937-130
Naphthalene ug/L 57.550 115 30-130
Nitrobenzene ug/L 66.7 L15013336-130
Pentachlorophenol ug/L 139100 139 23-149
Phenanthrene ug/L 65.4 L15013144-130
Phenol ug/L 42.350 85 18-130
Pyrene ug/L 68.5 L15013747-134
Pyridine ug/L 45.350 91 10-130
2,4,6-Tribromophenol (S)%139 10-144
2-Fluorobiphenyl (S)%117 10-130
2-Fluorophenol (S)%89 10-130
Nitrobenzene-d5 (S)%122 10-144
Phenol-d6 (S)%72 10-130
Terphenyl-d14 (S)%134 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3802403MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92627310008
3802404
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L R183.3 32 10-13046 38 3083.3ND 26.4 38.6
1,2-Dichlorobenzene ug/L 83.3 16 10-13030 3083.3ND 13.2J 24.6
1,3-Dichlorobenzene ug/L 83.3 12 10-13025 3083.3ND 9.9J 20.5
1,4-Dichlorobenzene ug/L 83.3 13 10-13027 3083.3ND 11.1J 22.2
1-Methylnaphthalene ug/L 83.3 58 10-13072 21 3083.3ND 48.7 60.2
2,2'-Oxybis(1-
chloropropane)ug/L 83.3 41 12-14254 28 3083.3ND 34.2 45.4
2,4,5-Trichlorophenol ug/L 83.3 82 10-14365 23 3083.3ND 68.0 54.2
2,4,6-Trichlorophenol ug/L R183.3 86 10-14749 55 3083.3ND 71.3 40.4
2,4-Dichlorophenol ug/L 83.3 68 10-13864 6 3083.3ND 56.6 53.3
2,4-Dimethylphenol ug/L 83.3 88 25-130105 18 3083.3ND 73.5 87.6
2,4-Dinitrophenol ug/L 417 73 10-16513 30417ND30655.8J
2,4-Dinitrotoluene ug/L 83.3 98 29-148114 15 3083.3ND 81.8 94.9
2,6-Dinitrotoluene ug/L 83.3 96 26-146116 19 3083.3ND 80.3 97.0
2-Chloronaphthalene ug/L 83.3 74 11-13087 16 3083.3ND 61.5 72.3
2-Chlorophenol ug/L 83.3 48 10-13352 8 3083.3ND 39.8 43.1
2-Methylnaphthalene ug/L 83.3 54 13-13066 21 3083.3ND 44.7 55.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3802403MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92627310008
3802404
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Methylphenol(o-Cresol)ug/L 83.3 56 20-13069 20 3083.3ND 46.5 57.1
2-Nitroaniline ug/L 167 90 24-136107 17 30167ND150178
2-Nitrophenol ug/L v183.3 64 10-15361 5 3083.3ND 53.3 50.7
3&4-Methylphenol(m&p
Cresol)ug/L 83.3 62 16-13078 24 3083.3ND 51.3 65.2
3,3'-Dichlorobenzidine ug/L 167 73 10-15399 30 30167ND122164
3-Nitroaniline ug/L 167 92 22-151112 20 30167ND153187
4,6-Dinitro-2-methylphenol ug/L R11678710-18029 100 30167ND14448.0
4-Bromophenylphenyl ether ug/L 83.3 83 25-13099 18 3083.3ND 68.9 82.4
4-Chloro-3-methylphenol ug/L 167 74 25-13389 17 30167ND124148
4-Chloroaniline ug/L 167 61 14-13279 26 30167ND102131
4-Chlorophenylphenyl ether ug/L 83.3 77 19-13091 17 3083.3ND 64.3 76.2
4-Nitroaniline ug/L 167 87 29-150102 16 30167ND145170
4-Nitrophenol ug/L 417 46 10-13014 30417ND19256.3J
Acenaphthene ug/L 83.3 77 16-13091 17 3083.3ND 64.2 75.8
Acenaphthylene ug/L 83.3 77 15-13793 19 3083.3ND 63.9 77.1
Aniline ug/L R183.3 39 10-13055 34 3083.3ND 32.9 46.2
Anthracene ug/L 83.3 77 37-13694 21 3083.3ND 63.9 78.6
Benzo(a)anthracene ug/L 83.3 90 40-145109 19 3083.3ND 74.9 90.9
Benzo(a)pyrene ug/L 83.3 90 41-146108 18 3083.3ND 74.8 89.7
Benzo(b)fluoranthene ug/L 83.3 91 39-151119 27 3083.3ND 75.8 99.2
Benzo(g,h,i)perylene ug/L 83.3 89 40-147110 21 3083.3ND 74.0 91.8
Benzo(k)fluoranthene ug/L 83.3 88 40-146107 19 3083.3ND 73.7 89.5
Benzoic Acid ug/L M14172210-1305 30417ND91.4 ND
Benzyl alcohol ug/L 167 60 25-13076 23 30167ND100127
bis(2-
Chloroethoxy)methane ug/L 83.3 58 23-13069 19 3083.3ND 48.0 57.8
bis(2-Chloroethyl) ether ug/L 83.3 46 25-13057 23 3083.3ND 38.0 47.9
bis(2-Ethylhexyl)phthalate ug/L 83.3 104 28-166125 19 3083.3ND 86.6 105
Butylbenzylphthalate ug/L v183.3 110 33-165132 18 3083.3ND 91.5 110
Chrysene ug/L 83.3 89 38-141106 17 3083.3ND 74.5 88.0
Di-n-butylphthalate ug/L 83.3 94 32-153110 16 3083.3ND 78.1 91.8
Di-n-octylphthalate ug/L 83.3 98 30-175115 16 3083.3ND 81.8 96.2
Dibenz(a,h)anthracene ug/L 83.3 91 39-148112 21 3083.3ND 75.6 93.0
Dibenzofuran ug/L 83.3 80 20-13095 16 3083.3ND 67.0 78.8
Diethylphthalate ug/L 83.3 88 28-142104 16 3083.3ND 73.4 86.5
Dimethylphthalate ug/L 83.3 87 26-136101 14 3083.3ND 72.8 84.0
Fluoranthene ug/L 83.3 81 39-14394 15 3083.3ND 67.8 78.6
Fluorene ug/L 83.3 82 24-13295 15 3083.3ND 68.2 79.3
Hexachloro-1,3-butadiene ug/L R183.3 20 10-13034 51 3083.3ND 16.8 28.3
Hexachlorobenzene ug/L 83.3 88 29-130105 18 3083.3ND 72.9 87.1
Hexachlorocyclopentadiene ug/L R183.3 37 10-13064 53 3083.3ND 31.1 53.6
Hexachloroethane ug/L 83.3 10 10-13022 3083.3ND 8.0J 18.7
Indeno(1,2,3-cd)pyrene ug/L 83.3 93 39-148112 18 3083.3ND 77.8 93.3
Isophorone ug/L 83.3 68 23-13081 18 3083.3ND 56.3 67.3
N-Nitroso-di-n-propylamine ug/L 83.3 64 25-13082 24 3083.3ND 53.6 68.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
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Page 60 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3802403MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92627310008
3802404
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodimethylamine ug/L 83.3 51 22-13063 21 3083.3ND 42.5 52.7
N-Nitrosodiphenylamine ug/L 83.3 85 26-134103 19 3083.3ND 70.6 85.8
Naphthalene ug/L 83.3 40 14-13053 28 3083.3ND 33.7 44.5
Nitrobenzene ug/L 83.3 53 25-13066 22 3083.3ND 44.4 55.4
Pentachlorophenol ug/L R11677910-17529 93 30167ND13248.1
Phenanthrene ug/L 83.3 85 36-13399 15 3083.3ND 70.7 82.3
Phenol ug/L 83.3 40 10-13047 18 3083.3ND 33.0 39.4
Pyrene ug/L 83.3 89 40-143113 23 3083.3ND 74.2 93.9
Pyridine ug/L 83.3 40 10-13052 26 3083.3ND 33.3 43.4
2,4,6-Tribromophenol (S)%92 10-14473
2-Fluorobiphenyl (S)%50 10-13067
2-Fluorophenol (S)%45 10-13037
Nitrobenzene-d5 (S)%57 10-14470
Phenol-d6 (S)%43 10-13048
Terphenyl-d14 (S)%92 34-163116
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 61 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1941872
7199
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3850992-1
Associated Lab Samples:92630198001, 92630198002, 92630198003, 92630198004, 92630198005, 92630198006, 92630198007,
92630198008
Matrix:Water
AnalyzedMDL
Chromium, Hexavalent ug/L ND 0.500 10/19/22 06:270.150
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3850992-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent ug/L 2.042.00 102 90.0-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3850992-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1543866-01
R3850992-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent ug/L 50.0 101 90.0-110101 0.154 2050.0ND 50.4 50.3
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3850992-7MATRIX SPIKE SAMPLE:
MSSpike
Result
L1545350-01
Chromium, Hexavalent ug/L 49.250.0 98.4 90.0-110ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1544015-02
R3850992-5SAMPLE DUPLICATE:
Chromium, Hexavalent ug/L 0.684 3.94 200.658
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1545344-01
R3850992-6SAMPLE DUPLICATE:
Chromium, Hexavalent ug/L 27.2 0.163 2027.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
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Page 62 of 67
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
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Page 63 of 67
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92630198001 730072 730140GW-1 EPA 3010A EPA 6010D
92630198002 730072 730140GW-2 EPA 3010A EPA 6010D
92630198003 730072 730140GW-3 EPA 3010A EPA 6010D
92630198004 730072 730140GW-4 EPA 3010A EPA 6010D
92630198005 730072 730140GW-5 EPA 3010A EPA 6010D
92630198006 730072 730140GW-6 EPA 3010A EPA 6010D
92630198007 730072 730140GW-7 EPA 3010A EPA 6010D
92630198008 730072 730140GW-8 EPA 3010A EPA 6010D
92630198001 730284 730376GW-1 EPA 3010A EPA 6010D
92630198002 730284 730376GW-2 EPA 3010A EPA 6010D
92630198003 730284 730376GW-3 EPA 3010A EPA 6010D
92630198004 730284 730376GW-4 EPA 3010A EPA 6010D
92630198005 730284 730376GW-5 EPA 3010A EPA 6010D
92630198006 730284 730376GW-6 EPA 3010A EPA 6010D
92630198007 730284 730376GW-7 EPA 3010A EPA 6010D
92630198008 730284 730376GW-8 EPA 3010A EPA 6010D
92630198001 730765 730893GW-1 EPA 7470A EPA 7470A
92630198002 730765 730893GW-2 EPA 7470A EPA 7470A
92630198003 730765 730893GW-3 EPA 7470A EPA 7470A
92630198004 730765 730893GW-4 EPA 7470A EPA 7470A
92630198005 730765 730893GW-5 EPA 7470A EPA 7470A
92630198006 730765 730893GW-6 EPA 7470A EPA 7470A
92630198007 730765 730893GW-7 EPA 7470A EPA 7470A
92630198008 730765 730893GW-8 EPA 7470A EPA 7470A
92630198001 730657 730741GW-1 EPA 7470A EPA 7470A
92630198002 730657 730741GW-2 EPA 7470A EPA 7470A
92630198003 730657 730741GW-3 EPA 7470A EPA 7470A
92630198004 730657 730741GW-4 EPA 7470A EPA 7470A
92630198005 730657 730741GW-5 EPA 7470A EPA 7470A
92630198006 730657 730741GW-6 EPA 7470A EPA 7470A
92630198007 730657 730741GW-7 EPA 7470A EPA 7470A
92630198008 730657 730741GW-8 EPA 7470A EPA 7470A
92630198001 729659 730120GW-1 EPA 3510C EPA 8270E
92630198002 730273 730458GW-2 EPA 3510C EPA 8270E
92630198003 729659 730120GW-3 EPA 3510C EPA 8270E
92630198004 729659 730120GW-4 EPA 3510C EPA 8270E
92630198005 729659 730120GW-5 EPA 3510C EPA 8270E
92630198006 729659 730120GW-6 EPA 3510C EPA 8270E
92630198007 730273 730458GW-7 EPA 3510C EPA 8270E
92630198008 729659 730120GW-8 EPA 3510C EPA 8270E
92630198001 729189GW-1 EPA 8260D
92630198002 729189GW-2 EPA 8260D
92630198003 729189GW-3 EPA 8260D
92630198004 729189GW-4 EPA 8260D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
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Page 64 of 67
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92630198
TWO VACANT PARCELS/SOUTH TRYON
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92630198005 729189GW-5 EPA 8260D
92630198006 729189GW-6 EPA 8260D
92630198007 729189GW-7 EPA 8260D
92630198008 729189GW-8 EPA 8260D
92630198001 1941872 1941872GW-1 7199 EPA 7199
92630198002 1941872 1941872GW-2 7199 EPA 7199
92630198003 1941872 1941872GW-3 7199 EPA 7199
92630198004 1941872 1941872GW-4 7199 EPA 7199
92630198005 1941872 1941872GW-5 7199 EPA 7199
92630198006 1941872 1941872GW-6 7199 EPA 7199
92630198007 1941872 1941872GW-7 7199 EPA 7199
92630198008 1941872 1941872GW-8 7199 EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/21/2022 02:07 PM
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[phone]
Page 65 of 67
Page 66 of 67
Page 67 of 67
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
October 14, 2022
Scott Young
ECS Southeast - Charlotte, NC
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project Location: Charlotte, NC
Client Job Number:
Project Number: 17700A
Laboratory Work Order Number: 22J1275
Enclosed are results of analyses for samples as received by the laboratory on October 8, 2022. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
10/14/2022ECS Southeast - Charlotte, NC
1812 Center Park Drive, Suite D
Charlotte, NC 28217
ATTN: Scott Young
17700A
22J1275
The results of analyses performed on the following samples submitted to Con-Test, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
SG-1 22J1275-01 Soil Gas EPA TO-15
SG-2 22J1275-02 Soil Gas EPA TO-15
SG-3 22J1275-03 Soil Gas EPA TO-15
SG-4 22J1275-04 Soil Gas EPA TO-15
SG-5 22J1275-05 Soil Gas EPA TO-15
Page 2 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not
detected" for all samples in this batch for this compound and bias is on the high side.
Analyte & Samples(s) Qualified:
L-01
4-Methyl-2-pentanone (MIBK), Benzyl chloride, Methyl tert-Butyl Ether (MTBE)
B319439-BS1
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be
biased on the low side.
Analyte & Samples(s) Qualified:
L-03
Hexachlorobutadiene, Naphthalene
22J1275-01[SG-1], 22J1275-02[SG-2], 22J1275-03[SG-3], 22J1275-04[SG-4], 22J1275-05[SG-5], B319439-BLK1, B319439-BS1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
4-Methyl-2-pentanone (MIBK), Benzyl chloride, Methyl tert-Butyl Ether (MTBE)
S077732-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since
sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-36
1,2,4-Trichlorobenzene, Benzyl chloride
S077732-CCV1
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 3 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 10/8/2022
Work Order: 22J1275Sample Description/Location:
Field Sample #: SG-1
Sample ID: 22J1275-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -4.8
Sampled: 10/6/2022 13:49
Canister ID: 2421
Flow Controller ID: 4676
Sub Description/Location:
Canister Size: 3 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 15 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 8.0 10/10/22 23:00 TPHND4194.8 11
Benzene 8.6 0.20 10/10/22 23:00 TPH28 40.640.15 0.48
Benzyl chloride ND 0.40 10/10/22 23:00 TPHND42.10.18 0.91
Bromodichloromethane ND 0.20 10/10/22 23:00 TPHND41.30.14 0.94
Bromoform ND 0.20 10/10/22 23:00 TPHND42.10.14 1.4
Bromomethane ND 0.20 10/10/22 23:00 TPHND40.780.13 0.52
1,3-Butadiene 17 0.20 10/10/22 23:00 TPH37 40.440.17 0.37
2-Butanone (MEK)8.9 8.0 10/10/22 23:00 TPH26 4242.1 6.3
Carbon Disulfide 25 2.0 10/10/22 23:00 TPH79 46.20.18 0.58
Carbon Tetrachloride ND 0.20 10/10/22 23:00 TPHND41.30.16 1.0
Chlorobenzene ND 0.20 10/10/22 23:00 TPHND40.920.13 0.61
Chloroethane ND 0.20 10/10/22 23:00 TPHND40.530.18 0.47
Chloroform ND 0.20 10/10/22 23:00 TPHND40.980.19 0.93
Chloromethane 0.86 0.40 10/10/22 23:00 TPH1.8 40.830.16 0.33
Cyclohexane 33 0.20 10/10/22 23:00 TPH120 40.690.12 0.42
Dibromochloromethane ND 0.20 10/10/22 23:00 TPHND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 10/10/22 23:00 TPHND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 10/10/22 23:00 TPHND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 10/10/22 23:00 TPHND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 10/10/22 23:00 TPHND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)0.56 0.20 10/10/22 23:00 TPH2.8 40.990.20 0.97
1,1-Dichloroethane ND 0.20 10/10/22 23:00 TPHND40.810.17 0.71
1,2-Dichloroethane ND 0.20 10/10/22 23:00 TPHND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 10/10/22 23:00 TPHND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 10/10/22 23:00 TPHND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 10/10/22 23:00 TPHND40.790.16 0.62
1,2-Dichloropropane ND 0.20 10/10/22 23:00 TPHND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 10/10/22 23:00 TPHND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 10/10/22 23:00 TPHND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 10/10/22 23:00 TPHND41.40.20 1.4
1,4-Dioxane ND 2.0 10/10/22 23:00 TPHND47.20.17 0.60
Ethanol 19 8.0 10/10/22 23:00 TPH35 4153.5 6.6
Ethyl Acetate ND 2.0 10/10/22 23:00 TPHND47.21.0 3.6
Ethylbenzene 1.3 0.20 10/10/22 23:00 TPH5.7 40.870.12 0.51
4-Ethyltoluene 0.37 0.20 10/10/22 23:00 TPH1.8 40.980.12 0.60
Heptane 9.2 0.20 10/10/22 23:00 TPH38 40.820.13 0.52
Hexachlorobutadiene ND 0.20 10/10/22 23:00 TPHL-03 ND 42.10.16 1.8
Hexane 33 8.0 10/10/22 23:00 TPH120 4281.0 3.7
2-Hexanone (MBK)ND 0.20 10/10/22 23:00 TPHND40.820.10 0.41
Isopropanol ND 8.0 10/10/22 23:00 TPHND4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 10/10/22 23:00 TPHND40.720.15 0.56
Methylene Chloride ND 2.0 10/10/22 23:00 TPHND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 10/10/22 23:00 TPHND40.820.11 0.44
Naphthalene 0.64 0.20 10/10/22 23:00 TPHL-03 3.4 41.00.15 0.79
Propene 800 60 10/10/22 23:28 TPH1400 301001323
Styrene 0.17 0.20 10/10/22 23:00 TPHJ0.72 40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 10/10/22 23:00 TPHND41.40.11 0.74
Page 4 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 10/8/2022
Work Order: 22J1275Sample Description/Location:
Field Sample #: SG-1
Sample ID: 22J1275-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -4.8
Sampled: 10/6/2022 13:49
Canister ID: 2421
Flow Controller ID: 4676
Sub Description/Location:
Canister Size: 3 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 15 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 10/10/22 23:00 TPHND41.40.15 1.0
Tetrahydrofuran ND 2.0 10/10/22 23:00 TPHND45.90.33 0.97
Toluene 13 0.20 10/10/22 23:00 TPH47 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 10/10/22 23:00 TPHND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 10/10/22 23:00 TPHND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 10/10/22 23:00 TPHND41.10.14 0.77
Trichloroethylene ND 0.20 10/10/22 23:00 TPHND41.10.13 0.72
Trichlorofluoromethane (Freon 11)0.25 0.80 10/10/22 23:00 TPHJ1.4 44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 10/10/22 23:00 TPHND46.10.22 1.7
1,2,4-Trimethylbenzene 0.96 0.20 10/10/22 23:00 TPH4.7 40.980.088 0.43
1,3,5-Trimethylbenzene 0.50 0.20 10/10/22 23:00 TPH2.5 40.980.11 0.52
Vinyl Acetate ND 4.0 10/10/22 23:00 TPHND4141.1 3.8
Vinyl Chloride ND 0.20 10/10/22 23:00 TPHND40.510.18 0.46
m&p-Xylene 4.0 0.40 10/10/22 23:00 TPH17 41.70.22 0.97
o-Xylene 2.4 0.20 10/10/22 23:00 TPH10 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)86.1 10/10/22 23:2870-130
4-Bromofluorobenzene (1)91.6 10/10/22 23:0070-130
Page 5 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 10/8/2022
Work Order: 22J1275Sample Description/Location:
Field Sample #: SG-2
Sample ID: 22J1275-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.8
Sampled: 10/6/2022 14:13
Canister ID: 2261
Flow Controller ID: 4675
Sub Description/Location:
Canister Size: 3 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 15 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 8.0 10/10/22 23:57 TPHND4194.8 11
Benzene 4.8 0.20 10/10/22 23:57 TPH15 40.640.15 0.48
Benzyl chloride ND 0.40 10/10/22 23:57 TPHND42.10.18 0.91
Bromodichloromethane ND 0.20 10/10/22 23:57 TPHND41.30.14 0.94
Bromoform ND 0.20 10/10/22 23:57 TPHND42.10.14 1.4
Bromomethane 0.16 0.20 10/10/22 23:57 TPHJ0.64 40.780.13 0.52
1,3-Butadiene 6.8 0.20 10/10/22 23:57 TPH15 40.440.17 0.37
2-Butanone (MEK)2.9 8.0 10/10/22 23:57 TPHJ8.6 4242.1 6.3
Carbon Disulfide 5.1 2.0 10/10/22 23:57 TPH16 46.20.18 0.58
Carbon Tetrachloride ND 0.20 10/10/22 23:57 TPHND41.30.16 1.0
Chlorobenzene ND 0.20 10/10/22 23:57 TPHND40.920.13 0.61
Chloroethane 0.33 0.20 10/10/22 23:57 TPH0.88 40.530.18 0.47
Chloroform 0.24 0.20 10/10/22 23:57 TPH1.2 40.980.19 0.93
Chloromethane 1.2 0.40 10/10/22 23:57 TPH2.5 40.830.16 0.33
Cyclohexane 4.7 0.20 10/10/22 23:57 TPH16 40.690.12 0.42
Dibromochloromethane ND 0.20 10/10/22 23:57 TPHND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 10/10/22 23:57 TPHND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 10/10/22 23:57 TPHND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 10/10/22 23:57 TPHND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 10/10/22 23:57 TPHND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)0.56 0.20 10/10/22 23:57 TPH2.7 40.990.20 0.97
1,1-Dichloroethane ND 0.20 10/10/22 23:57 TPHND40.810.17 0.71
1,2-Dichloroethane ND 0.20 10/10/22 23:57 TPHND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 10/10/22 23:57 TPHND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 10/10/22 23:57 TPHND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 10/10/22 23:57 TPHND40.790.16 0.62
1,2-Dichloropropane ND 0.20 10/10/22 23:57 TPHND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 10/10/22 23:57 TPHND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 10/10/22 23:57 TPHND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 10/10/22 23:57 TPHND41.40.20 1.4
1,4-Dioxane ND 2.0 10/10/22 23:57 TPHND47.20.17 0.60
Ethanol 14 8.0 10/10/22 23:57 TPH26 4153.5 6.6
Ethyl Acetate ND 2.0 10/10/22 23:57 TPHND47.21.0 3.6
Ethylbenzene 0.22 0.20 10/10/22 23:57 TPH0.96 40.870.12 0.51
4-Ethyltoluene ND 0.20 10/10/22 23:57 TPHND40.980.12 0.60
Heptane 1.4 0.20 10/10/22 23:57 TPH5.7 40.820.13 0.52
Hexachlorobutadiene ND 0.20 10/10/22 23:57 TPHL-03 ND 42.10.16 1.8
Hexane 5.4 8.0 10/10/22 23:57 TPHJ19 4281.0 3.7
2-Hexanone (MBK)ND 0.20 10/10/22 23:57 TPHND40.820.10 0.41
Isopropanol 14 8.0 10/10/22 23:57 TPH35 4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 10/10/22 23:57 TPHND40.720.15 0.56
Methylene Chloride ND 2.0 10/10/22 23:57 TPHND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 10/10/22 23:57 TPHND40.820.11 0.44
Naphthalene ND 0.20 10/10/22 23:57 TPHL-03 ND 41.00.15 0.79
Propene 330 60 10/11/22 0:25 TPH570 301001323
Styrene 0.16 0.20 10/10/22 23:57 TPHJ0.70 40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 10/10/22 23:57 TPHND41.40.11 0.74
Page 6 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 10/8/2022
Work Order: 22J1275Sample Description/Location:
Field Sample #: SG-2
Sample ID: 22J1275-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.8
Sampled: 10/6/2022 14:13
Canister ID: 2261
Flow Controller ID: 4675
Sub Description/Location:
Canister Size: 3 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 15 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 10/10/22 23:57 TPHND41.40.15 1.0
Tetrahydrofuran ND 2.0 10/10/22 23:57 TPHND45.90.33 0.97
Toluene 3.2 0.20 10/10/22 23:57 TPH12 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 10/10/22 23:57 TPHND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 10/10/22 23:57 TPHND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 10/10/22 23:57 TPHND41.10.14 0.77
Trichloroethylene ND 0.20 10/10/22 23:57 TPHND41.10.13 0.72
Trichlorofluoromethane (Freon 11)0.33 0.80 10/10/22 23:57 TPHJ1.8 44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 10/10/22 23:57 TPHND46.10.22 1.7
1,2,4-Trimethylbenzene ND 0.20 10/10/22 23:57 TPHND40.980.088 0.43
1,3,5-Trimethylbenzene ND 0.20 10/10/22 23:57 TPHND40.980.11 0.52
Vinyl Acetate ND 4.0 10/10/22 23:57 TPHND4141.1 3.8
Vinyl Chloride ND 0.20 10/10/22 23:57 TPHND40.510.18 0.46
m&p-Xylene 0.58 0.40 10/10/22 23:57 TPH2.5 41.70.22 0.97
o-Xylene 0.43 0.20 10/10/22 23:57 TPH1.9 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)89.0 10/11/22 0:2570-130
4-Bromofluorobenzene (1)94.8 10/10/22 23:5770-130
Page 7 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 10/8/2022
Work Order: 22J1275Sample Description/Location:
Field Sample #: SG-3
Sample ID: 22J1275-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.2
Sampled: 10/6/2022 14:55
Canister ID: 2275
Flow Controller ID: 4747
Sub Description/Location:
Canister Size: 3 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 15 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 8.0 10/11/22 0:53 TPHND4194.8 11
Benzene 6.3 0.20 10/11/22 0:53 TPH20 40.640.15 0.48
Benzyl chloride ND 0.40 10/11/22 0:53 TPHND42.10.18 0.91
Bromodichloromethane ND 0.20 10/11/22 0:53 TPHND41.30.14 0.94
Bromoform ND 0.20 10/11/22 0:53 TPHND42.10.14 1.4
Bromomethane ND 0.20 10/11/22 0:53 TPHND40.780.13 0.52
1,3-Butadiene 6.1 0.20 10/11/22 0:53 TPH13 40.440.17 0.37
2-Butanone (MEK)8.0 8.0 10/11/22 0:53 TPH24 4242.1 6.3
Carbon Disulfide 36 2.0 10/11/22 0:53 TPH110 46.20.18 0.58
Carbon Tetrachloride ND 0.20 10/11/22 0:53 TPHND41.30.16 1.0
Chlorobenzene ND 0.20 10/11/22 0:53 TPHND40.920.13 0.61
Chloroethane ND 0.20 10/11/22 0:53 TPHND40.530.18 0.47
Chloroform ND 0.20 10/11/22 0:53 TPHND40.980.19 0.93
Chloromethane 1.2 0.40 10/11/22 0:53 TPH2.5 40.830.16 0.33
Cyclohexane 6.5 0.20 10/11/22 0:53 TPH22 40.690.12 0.42
Dibromochloromethane ND 0.20 10/11/22 0:53 TPHND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 10/11/22 0:53 TPHND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 10/11/22 0:53 TPHND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 10/11/22 0:53 TPHND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 10/11/22 0:53 TPHND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)0.51 0.20 10/11/22 0:53 TPH2.5 40.990.20 0.97
1,1-Dichloroethane ND 0.20 10/11/22 0:53 TPHND40.810.17 0.71
1,2-Dichloroethane ND 0.20 10/11/22 0:53 TPHND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 10/11/22 0:53 TPHND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 10/11/22 0:53 TPHND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 10/11/22 0:53 TPHND40.790.16 0.62
1,2-Dichloropropane ND 0.20 10/11/22 0:53 TPHND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 10/11/22 0:53 TPHND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 10/11/22 0:53 TPHND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 10/11/22 0:53 TPHND41.40.20 1.4
1,4-Dioxane ND 2.0 10/11/22 0:53 TPHND47.20.17 0.60
Ethanol 12 8.0 10/11/22 0:53 TPH23 4153.5 6.6
Ethyl Acetate ND 2.0 10/11/22 0:53 TPHND47.21.0 3.6
Ethylbenzene 1.0 0.20 10/11/22 0:53 TPH4.3 40.870.12 0.51
4-Ethyltoluene 0.28 0.20 10/11/22 0:53 TPH1.4 40.980.12 0.60
Heptane 150 0.20 10/11/22 0:53 TPH610 40.820.13 0.52
Hexachlorobutadiene ND 0.20 10/11/22 0:53 TPHL-03 ND 42.10.16 1.8
Hexane 240 60 10/11/22 1:22 TPH850 302107.8 28
2-Hexanone (MBK)ND 0.20 10/11/22 0:53 TPHND40.820.10 0.41
Isopropanol 2.0 8.0 10/11/22 0:53 TPHJ4.9 4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 10/11/22 0:53 TPHND40.720.15 0.56
Methylene Chloride ND 2.0 10/11/22 0:53 TPHND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 10/11/22 0:53 TPHND40.820.11 0.44
Naphthalene ND 0.20 10/11/22 0:53 TPHL-03 ND 41.00.15 0.79
Propene 440 60 10/11/22 1:22 TPH750 301001323
Styrene 0.39 0.20 10/11/22 0:53 TPH1.7 40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 10/11/22 0:53 TPHND41.40.11 0.74
Page 8 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 10/8/2022
Work Order: 22J1275Sample Description/Location:
Field Sample #: SG-3
Sample ID: 22J1275-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.2
Sampled: 10/6/2022 14:55
Canister ID: 2275
Flow Controller ID: 4747
Sub Description/Location:
Canister Size: 3 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 15 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 10/11/22 0:53 TPHND41.40.15 1.0
Tetrahydrofuran ND 2.0 10/11/22 0:53 TPHND45.90.33 0.97
Toluene 6.5 0.20 10/11/22 0:53 TPH25 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 10/11/22 0:53 TPHND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 10/11/22 0:53 TPHND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 10/11/22 0:53 TPHND41.10.14 0.77
Trichloroethylene ND 0.20 10/11/22 0:53 TPHND41.10.13 0.72
Trichlorofluoromethane (Freon 11)ND 0.80 10/11/22 0:53 TPHND44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 10/11/22 0:53 TPHND46.10.22 1.7
1,2,4-Trimethylbenzene 0.60 0.20 10/11/22 0:53 TPH2.9 40.980.088 0.43
1,3,5-Trimethylbenzene 0.30 0.20 10/11/22 0:53 TPH1.5 40.980.11 0.52
Vinyl Acetate ND 4.0 10/11/22 0:53 TPHND4141.1 3.8
Vinyl Chloride ND 0.20 10/11/22 0:53 TPHND40.510.18 0.46
m&p-Xylene 2.5 0.40 10/11/22 0:53 TPH11 41.70.22 0.97
o-Xylene 1.4 0.20 10/11/22 0:53 TPH6.3 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)97.6 10/11/22 0:5370-130
4-Bromofluorobenzene (1)87.9 10/11/22 1:2270-130
Page 9 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 10/8/2022
Work Order: 22J1275Sample Description/Location:
Field Sample #: SG-4
Sample ID: 22J1275-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.7
Sampled: 10/6/2022 15:34
Canister ID: 2413
Flow Controller ID: 4746
Sub Description/Location:
Canister Size: 3 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 15 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 8.0 10/11/22 1:50 TPHND4194.8 11
Benzene 14 0.20 10/11/22 1:50 TPH44 40.640.15 0.48
Benzyl chloride ND 0.40 10/11/22 1:50 TPHND42.10.18 0.91
Bromodichloromethane ND 0.20 10/11/22 1:50 TPHND41.30.14 0.94
Bromoform ND 0.20 10/11/22 1:50 TPHND42.10.14 1.4
Bromomethane ND 0.20 10/11/22 1:50 TPHND40.780.13 0.52
1,3-Butadiene 14 0.20 10/11/22 1:50 TPH32 40.440.17 0.37
2-Butanone (MEK)8.0 8.0 10/11/22 1:50 TPHJ24 4242.1 6.3
Carbon Disulfide 18 2.0 10/11/22 1:50 TPH55 46.20.18 0.58
Carbon Tetrachloride ND 0.20 10/11/22 1:50 TPHND41.30.16 1.0
Chlorobenzene ND 0.20 10/11/22 1:50 TPHND40.920.13 0.61
Chloroethane ND 0.20 10/11/22 1:50 TPHND40.530.18 0.47
Chloroform ND 0.20 10/11/22 1:50 TPHND40.980.19 0.93
Chloromethane 1.0 0.40 10/11/22 1:50 TPH2.1 40.830.16 0.33
Cyclohexane 3.3 0.20 10/11/22 1:50 TPH11 40.690.12 0.42
Dibromochloromethane ND 0.20 10/11/22 1:50 TPHND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 10/11/22 1:50 TPHND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 10/11/22 1:50 TPHND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 10/11/22 1:50 TPHND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 10/11/22 1:50 TPHND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)0.55 0.20 10/11/22 1:50 TPH2.7 40.990.20 0.97
1,1-Dichloroethane ND 0.20 10/11/22 1:50 TPHND40.810.17 0.71
1,2-Dichloroethane ND 0.20 10/11/22 1:50 TPHND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 10/11/22 1:50 TPHND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 10/11/22 1:50 TPHND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 10/11/22 1:50 TPHND40.790.16 0.62
1,2-Dichloropropane ND 0.20 10/11/22 1:50 TPHND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 10/11/22 1:50 TPHND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 10/11/22 1:50 TPHND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 10/11/22 1:50 TPHND41.40.20 1.4
1,4-Dioxane ND 2.0 10/11/22 1:50 TPHND47.20.17 0.60
Ethanol 14 8.0 10/11/22 1:50 TPH26 4153.5 6.6
Ethyl Acetate ND 2.0 10/11/22 1:50 TPHND47.21.0 3.6
Ethylbenzene 1.4 0.20 10/11/22 1:50 TPH6.2 40.870.12 0.51
4-Ethyltoluene 0.24 0.20 10/11/22 1:50 TPH1.2 40.980.12 0.60
Heptane 6.5 0.20 10/11/22 1:50 TPH27 40.820.13 0.52
Hexachlorobutadiene ND 0.20 10/11/22 1:50 TPHL-03 ND 42.10.16 1.8
Hexane 19 8.0 10/11/22 1:50 TPH66 4281.0 3.7
2-Hexanone (MBK)ND 0.20 10/11/22 1:50 TPHND40.820.10 0.41
Isopropanol 2.0 8.0 10/11/22 1:50 TPHJ5.0 4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 10/11/22 1:50 TPHND40.720.15 0.56
Methylene Chloride ND 2.0 10/11/22 1:50 TPHND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 10/11/22 1:50 TPHND40.820.11 0.44
Naphthalene ND 0.20 10/11/22 1:50 TPHL-03 ND 41.00.15 0.79
Propene 380 60 10/11/22 2:19 TPH660 301001323
Styrene 0.43 0.20 10/11/22 1:50 TPH1.8 40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 10/11/22 1:50 TPHND41.40.11 0.74
Page 10 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 10/8/2022
Work Order: 22J1275Sample Description/Location:
Field Sample #: SG-4
Sample ID: 22J1275-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.7
Sampled: 10/6/2022 15:34
Canister ID: 2413
Flow Controller ID: 4746
Sub Description/Location:
Canister Size: 3 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 15 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 10/11/22 1:50 TPHND41.40.15 1.0
Tetrahydrofuran ND 2.0 10/11/22 1:50 TPHND45.90.33 0.97
Toluene 11 0.20 10/11/22 1:50 TPH43 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 10/11/22 1:50 TPHND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 10/11/22 1:50 TPHND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 10/11/22 1:50 TPHND41.10.14 0.77
Trichloroethylene ND 0.20 10/11/22 1:50 TPHND41.10.13 0.72
Trichlorofluoromethane (Freon 11)ND 0.80 10/11/22 1:50 TPHND44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 10/11/22 1:50 TPHND46.10.22 1.7
1,2,4-Trimethylbenzene 0.39 0.20 10/11/22 1:50 TPH1.9 40.980.088 0.43
1,3,5-Trimethylbenzene 0.22 0.20 10/11/22 1:50 TPH1.1 40.980.11 0.52
Vinyl Acetate ND 4.0 10/11/22 1:50 TPHND4141.1 3.8
Vinyl Chloride 0.36 0.20 10/11/22 1:50 TPH0.92 40.510.18 0.46
m&p-Xylene 2.8 0.40 10/11/22 1:50 TPH12 41.70.22 0.97
o-Xylene 1.5 0.20 10/11/22 1:50 TPH6.3 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)90.1 10/11/22 2:1970-130
4-Bromofluorobenzene (1)95.8 10/11/22 1:5070-130
Page 11 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 10/8/2022
Work Order: 22J1275Sample Description/Location:
Field Sample #: SG-5
Sample ID: 22J1275-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.9
Sampled: 10/6/2022 16:14
Canister ID: 2604
Flow Controller ID: 4706
Sub Description/Location:
Canister Size: 3 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 15 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 8.0 10/11/22 2:47 TPHND4194.8 11
Benzene 8.8 0.20 10/11/22 2:47 TPH28 40.640.15 0.48
Benzyl chloride ND 0.40 10/11/22 2:47 TPHND42.10.18 0.91
Bromodichloromethane ND 0.20 10/11/22 2:47 TPHND41.30.14 0.94
Bromoform ND 0.20 10/11/22 2:47 TPHND42.10.14 1.4
Bromomethane ND 0.20 10/11/22 2:47 TPHND40.780.13 0.52
1,3-Butadiene 8.4 0.20 10/11/22 2:47 TPH19 40.440.17 0.37
2-Butanone (MEK)8.7 8.0 10/11/22 2:47 TPH26 4242.1 6.3
Carbon Disulfide 3.4 2.0 10/11/22 2:47 TPH11 46.20.18 0.58
Carbon Tetrachloride ND 0.20 10/11/22 2:47 TPHND41.30.16 1.0
Chlorobenzene ND 0.20 10/11/22 2:47 TPHND40.920.13 0.61
Chloroethane ND 0.20 10/11/22 2:47 TPHND40.530.18 0.47
Chloroform ND 0.20 10/11/22 2:47 TPHND40.980.19 0.93
Chloromethane 1.2 0.40 10/11/22 2:47 TPH2.4 40.830.16 0.33
Cyclohexane 5.6 0.20 10/11/22 2:47 TPH19 40.690.12 0.42
Dibromochloromethane ND 0.20 10/11/22 2:47 TPHND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 10/11/22 2:47 TPHND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 10/11/22 2:47 TPHND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 10/11/22 2:47 TPHND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 10/11/22 2:47 TPHND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)0.46 0.20 10/11/22 2:47 TPH2.3 40.990.20 0.97
1,1-Dichloroethane ND 0.20 10/11/22 2:47 TPHND40.810.17 0.71
1,2-Dichloroethane ND 0.20 10/11/22 2:47 TPHND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 10/11/22 2:47 TPHND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 10/11/22 2:47 TPHND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 10/11/22 2:47 TPHND40.790.16 0.62
1,2-Dichloropropane ND 0.20 10/11/22 2:47 TPHND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 10/11/22 2:47 TPHND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 10/11/22 2:47 TPHND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 10/11/22 2:47 TPHND41.40.20 1.4
1,4-Dioxane ND 2.0 10/11/22 2:47 TPHND47.20.17 0.60
Ethanol 11 8.0 10/11/22 2:47 TPH21 4153.5 6.6
Ethyl Acetate ND 2.0 10/11/22 2:47 TPHND47.21.0 3.6
Ethylbenzene 1.9 0.20 10/11/22 2:47 TPH8.4 40.870.12 0.51
4-Ethyltoluene 1.1 0.20 10/11/22 2:47 TPH5.2 40.980.12 0.60
Heptane 6.5 0.20 10/11/22 2:47 TPH27 40.820.13 0.52
Hexachlorobutadiene ND 0.20 10/11/22 2:47 TPHL-03 ND 42.10.16 1.8
Hexane 16 8.0 10/11/22 2:47 TPH56 4281.0 3.7
2-Hexanone (MBK)ND 0.20 10/11/22 2:47 TPHND40.820.10 0.41
Isopropanol ND 8.0 10/11/22 2:47 TPHND4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 10/11/22 2:47 TPHND40.720.15 0.56
Methylene Chloride ND 2.0 10/11/22 2:47 TPHND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 10/11/22 2:47 TPHND40.820.11 0.44
Naphthalene ND 0.20 10/11/22 2:47 TPHL-03 ND 41.00.15 0.79
Propene 530 60 10/11/22 3:15 TPH920 301001323
Styrene 0.26 0.20 10/11/22 2:47 TPH1.1 40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 10/11/22 2:47 TPHND41.40.11 0.74
Page 12 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 10/8/2022
Work Order: 22J1275Sample Description/Location:
Field Sample #: SG-5
Sample ID: 22J1275-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.9
Sampled: 10/6/2022 16:14
Canister ID: 2604
Flow Controller ID: 4706
Sub Description/Location:
Canister Size: 3 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 15 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 10/11/22 2:47 TPHND41.40.15 1.0
Tetrahydrofuran ND 2.0 10/11/22 2:47 TPHND45.90.33 0.97
Toluene 12 0.20 10/11/22 2:47 TPH45 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 10/11/22 2:47 TPHND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 10/11/22 2:47 TPHND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 10/11/22 2:47 TPHND41.10.14 0.77
Trichloroethylene ND 0.20 10/11/22 2:47 TPHND41.10.13 0.72
Trichlorofluoromethane (Freon 11)ND 0.80 10/11/22 2:47 TPHND44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 10/11/22 2:47 TPHND46.10.22 1.7
1,2,4-Trimethylbenzene 1.7 0.20 10/11/22 2:47 TPH8.1 40.980.088 0.43
1,3,5-Trimethylbenzene 0.77 0.20 10/11/22 2:47 TPH3.8 40.980.11 0.52
Vinyl Acetate ND 4.0 10/11/22 2:47 TPHND4141.1 3.8
Vinyl Chloride ND 0.20 10/11/22 2:47 TPHND40.510.18 0.46
m&p-Xylene 8.9 0.40 10/11/22 2:47 TPH38 41.70.22 0.97
o-Xylene 3.2 0.20 10/11/22 2:47 TPH14 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)92.6 10/11/22 3:1570-130
4-Bromofluorobenzene (1)96.3 10/11/22 2:4770-130
Page 13 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
22J1275-01 [SG-1]B319439 1.5 1 N/A 1000 200 75 10/10/22
22J1275-01RE1 [SG-1]B319439 1.5 1 N/A 1000 200 10 10/10/22
22J1275-02 [SG-2]B319439 1.5 1 N/A 1000 200 75 10/10/22
22J1275-02RE1 [SG-2]B319439 1.5 1 N/A 1000 200 10 10/10/22
22J1275-03 [SG-3]B319439 1.5 1 N/A 1000 200 75 10/10/22
22J1275-03RE1 [SG-3]B319439 1.5 1 N/A 1000 200 10 10/10/22
22J1275-04 [SG-4]B319439 1.5 1 N/A 1000 200 75 10/10/22
22J1275-04RE1 [SG-4]B319439 1.5 1 N/A 1000 200 10 10/10/22
22J1275-05 [SG-5]B319439 1.5 1 N/A 1000 200 75 10/10/22
22J1275-05RE1 [SG-5]B319439 1.5 1 N/A 1000 200 10 10/10/22
Page 14 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B319439 - TO-15 Prep
Blank (B319439-BLK1)Prepared & Analyzed: 10/10/22
0.80NDAcetone
0.020NDBenzene
0.020NDBenzyl chloride
0.020NDBromodichloromethane
0.020NDBromoform
0.020NDBromomethane
0.020ND1,3-Butadiene
0.80ND2-Butanone (MEK)
0.20NDCarbon Disulfide
0.020NDCarbon Tetrachloride
0.020NDChlorobenzene
0.020NDChloroethane
0.020NDChloroform
0.040NDChloromethane
0.020NDCyclohexane
0.020NDDibromochloromethane
0.020ND1,2-Dibromoethane (EDB)
0.020ND1,2-Dichlorobenzene
0.020ND1,3-Dichlorobenzene
0.020ND1,4-Dichlorobenzene
0.020NDDichlorodifluoromethane (Freon 12)
0.020ND1,1-Dichloroethane
0.020ND1,2-Dichloroethane
0.020ND1,1-Dichloroethylene
0.020NDcis-1,2-Dichloroethylene
0.020NDtrans-1,2-Dichloroethylene
0.020ND1,2-Dichloropropane
0.020NDcis-1,3-Dichloropropene
0.020NDtrans-1,3-Dichloropropene
0.020ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
0.20ND1,4-Dioxane
0.80NDEthanol
0.20NDEthyl Acetate
0.020NDEthylbenzene
0.020ND4-Ethyltoluene
0.020NDHeptane
0.020 L-03NDHexachlorobutadiene
0.80NDHexane
0.020ND2-Hexanone (MBK)
0.80NDIsopropanol
0.020NDMethyl tert-Butyl Ether (MTBE)
0.20NDMethylene Chloride
0.020ND4-Methyl-2-pentanone (MIBK)
0.020 L-03NDNaphthalene
0.80NDPropene
0.020NDStyrene
Page 15 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B319439 - TO-15 Prep
Blank (B319439-BLK1)Prepared & Analyzed: 10/10/22
0.020ND1,1,2,2-Tetrachloroethane
0.020NDTetrachloroethylene
0.20NDTetrahydrofuran
0.020NDToluene
0.020ND1,2,4-Trichlorobenzene
0.020ND1,1,1-Trichloroethane
0.020ND1,1,2-Trichloroethane
0.020NDTrichloroethylene
0.080NDTrichlorofluoromethane (Freon 11)
0.080ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.020ND1,2,4-Trimethylbenzene
0.020ND1,3,5-Trimethylbenzene
0.40NDVinyl Acetate
0.020NDVinyl Chloride
0.040NDm&p-Xylene
0.020NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)90.67.24
LCS (B319439-BS1)Prepared & Analyzed: 10/10/22
5.00 70-1301055.24Acetone
5.00 70-1301065.31Benzene
5.00 L-0170-1301437.13Benzyl chloride *
5.00 70-1301085.41Bromodichloromethane
5.00 70-1301045.22Bromoform
5.00 70-1301075.36Bromomethane
5.00 70-1301095.441,3-Butadiene
5.00 70-1301045.182-Butanone (MEK)
5.00 70-1301045.20Carbon Disulfide
5.00 70-1301145.70Carbon Tetrachloride
5.00 70-13099.74.99Chlorobenzene
5.00 70-1301115.56Chloroethane
5.00 70-1301025.10Chloroform
5.00 70-1301115.56Chloromethane
5.00 70-1301135.63Cyclohexane
5.00 70-1301095.45Dibromochloromethane
5.00 70-1301075.341,2-Dibromoethane (EDB)
5.00 70-1301035.161,2-Dichlorobenzene
5.00 70-1301045.221,3-Dichlorobenzene
5.00 70-1301115.531,4-Dichlorobenzene
5.00 70-1301105.51Dichlorodifluoromethane (Freon 12)
5.00 70-1301165.781,1-Dichloroethane
5.00 70-1301055.241,2-Dichloroethane
5.00 70-1301075.351,1-Dichloroethylene
5.00 70-13098.94.94cis-1,2-Dichloroethylene
5.00 70-1301085.40trans-1,2-Dichloroethylene
5.00 70-1301085.401,2-Dichloropropane
Page 16 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B319439 - TO-15 Prep
LCS (B319439-BS1)Prepared & Analyzed: 10/10/22
5.00 70-13089.34.47cis-1,3-Dichloropropene
5.00 70-1301155.74trans-1,3-Dichloropropene
5.00 70-1301015.061,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
5.00 70-1301025.081,4-Dioxane
5.00 70-13075.03.75Ethanol
5.00 70-1301065.31Ethyl Acetate
5.00 70-1301055.26Ethylbenzene
5.00 70-1301075.344-Ethyltoluene
5.00 70-1301185.90Heptane
5.00 L-0370-13063.53.18Hexachlorobutadiene *
5.00 70-1301085.42Hexane
5.00 70-1301135.662-Hexanone (MBK)
5.00 70-13088.54.43Isopropanol
5.00 L-0170-1301316.56Methyl tert-Butyl Ether (MTBE)*
5.00 70-1301015.06Methylene Chloride
5.00 L-0170-1301457.254-Methyl-2-pentanone (MIBK)*
5.00 L-0370-13069.93.50Naphthalene *
5.00 70-1301205.99Propene
5.00 70-1301095.44Styrene
5.00 70-1301095.441,1,2,2-Tetrachloroethane
5.00 70-13096.94.84Tetrachloroethylene
5.00 70-1301095.44Tetrahydrofuran
5.00 70-1301055.24Toluene
5.00 70-13071.23.561,2,4-Trichlorobenzene
5.00 70-1301145.721,1,1-Trichloroethane
5.00 70-1301075.371,1,2-Trichloroethane
5.00 70-1301065.29Trichloroethylene
5.00 70-1301105.50Trichlorofluoromethane (Freon 11)
5.00 70-1301125.581,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-1301085.381,2,4-Trimethylbenzene
5.00 70-1301135.631,3,5-Trimethylbenzene
5.00 70-13089.24.46Vinyl Acetate
5.00 70-1301095.47Vinyl Chloride
10.0 70-13010310.3m&p-Xylene
5.00 70-1301135.67o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)95.07.60
Page 17 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Note: Blank Subtraction is not performed unless otherwise noted
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not
affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high
side.
L-01
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this
compound is likely to be biased on the low side.
L-03
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data
validation is not affected since sample result was "not detected" for this compound.
V-36
Page 18 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYST
Thomas P. HniteckiTPH
Raisa A. PetraitisRAP
PDF Management StationSTATION
Kerry K. McGeeKKM
Page 19 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S069304-ICV1 )Lab File ID: K22A075019.D Analyzed: 03/16/22 23:55
Bromochloromethane (1)104138 2.987 104138 2.987 60 - 140100 0.0000 +/-0.50
1,4-Difluorobenzene (1)315817 3.584 315817 3.584 60 - 140100 0.0000 +/-0.50
Chlorobenzene-d5 (1)233658 5.159 233658 5.159 60 - 140100 0.0000 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S077732-CCV1 )Lab File ID: K22A283004.D Analyzed: 10/10/22 11:08
Bromochloromethane (1)84069 2.991 84069 2.991 60 - 140100 0.0000 +/-0.50
1,4-Difluorobenzene (1)221565 3.583 221565 3.583 60 - 140100 0.0000 +/-0.50
Chlorobenzene-d5 (1)168934 5.163 168934 5.163 60 - 140100 0.0000 +/-0.50
LCS (B319439-BS1 )Lab File ID: K22A283005.D Analyzed: 10/10/22 11:38
Bromochloromethane (1)85722 2.991 84069 2.991 60 - 140102 0.0000 +/-0.50
1,4-Difluorobenzene (1)228063 3.583 221565 3.583 60 - 140103 0.0000 +/-0.50
Chlorobenzene-d5 (1)169748 5.163 168934 5.163 60 - 140100 0.0000 +/-0.50
Blank (B319439-BLK1 )Lab File ID: K22A283008.D Analyzed: 10/10/22 13:21
Bromochloromethane (1)85790 2.991 84069 2.991 60 - 140102 0.0000 +/-0.50
1,4-Difluorobenzene (1)207239 3.583 221565 3.583 60 - 14094 0.0000 +/-0.50
Chlorobenzene-d5 (1)160810 5.163 168934 5.163 60 - 14095 0.0000 +/-0.50
SG-1 (22J1275-01 )Lab File ID: K22A283022.D Analyzed: 10/10/22 23:00
Bromochloromethane (1)83225 3.001 84069 2.991 60 - 14099 0.0100 +/-0.50
1,4-Difluorobenzene (1)226471 3.588 221565 3.583 60 - 140102 0.0050 +/-0.50
Chlorobenzene-d5 (1)167322 5.163 168934 5.163 60 - 14099 0.0000 +/-0.50
SG-1 (22J1275-01RE1 )Lab File ID: K22A283023.D Analyzed: 10/10/22 23:28
Bromochloromethane (1)85872 2.996 84069 2.991 60 - 140102 0.0050 +/-0.50
1,4-Difluorobenzene (1)228299 3.588 221565 3.583 60 - 140103 0.0050 +/-0.50
Chlorobenzene-d5 (1)165440 5.163 168934 5.163 60 - 14098 0.0000 +/-0.50
SG-2 (22J1275-02 )Lab File ID: K22A283024.D Analyzed: 10/10/22 23:57
Bromochloromethane (1)83921 3.001 84069 2.991 60 - 140100 0.0100 +/-0.50
1,4-Difluorobenzene (1)219779 3.588 221565 3.583 60 - 14099 0.0050 +/-0.50
Chlorobenzene-d5 (1)167824 5.163 168934 5.163 60 - 14099 0.0000 +/-0.50
SG-2 (22J1275-02RE1 )Lab File ID: K22A283025.D Analyzed: 10/11/22 00:25
Bromochloromethane (1)85036 3.001 84069 2.991 60 - 140101 0.0100 +/-0.50
1,4-Difluorobenzene (1)216745 3.588 221565 3.583 60 - 14098 0.0050 +/-0.50
Chlorobenzene-d5 (1)160933 5.163 168934 5.163 60 - 14095 0.0000 +/-0.50
Page 20 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
SG-3 (22J1275-03 )Lab File ID: K22A283026.D Analyzed: 10/11/22 00:53
Bromochloromethane (1)82887 3.001 84069 2.991 60 - 14099 0.0100 +/-0.50
1,4-Difluorobenzene (1)218443 3.593 221565 3.583 60 - 14099 0.0100 +/-0.50
Chlorobenzene-d5 (1)176376 5.163 168934 5.163 60 - 140104 0.0000 +/-0.50
SG-3 (22J1275-03RE1 )Lab File ID: K22A283027.D Analyzed: 10/11/22 01:22
Bromochloromethane (1)85486 2.996 84069 2.991 60 - 140102 0.0050 +/-0.50
1,4-Difluorobenzene (1)234162 3.588 221565 3.583 60 - 140106 0.0050 +/-0.50
Chlorobenzene-d5 (1)177151 5.163 168934 5.163 60 - 140105 0.0000 +/-0.50
SG-4 (22J1275-04 )Lab File ID: K22A283028.D Analyzed: 10/11/22 01:50
Bromochloromethane (1)88474 3.001 84069 2.991 60 - 140105 0.0100 +/-0.50
1,4-Difluorobenzene (1)241425 3.588 221565 3.583 60 - 140109 0.0050 +/-0.50
Chlorobenzene-d5 (1)184213 5.163 168934 5.163 60 - 140109 0.0000 +/-0.50
SG-4 (22J1275-04RE1 )Lab File ID: K22A283029.D Analyzed: 10/11/22 02:19
Bromochloromethane (1)87223 3.001 84069 2.991 60 - 140104 0.0100 +/-0.50
1,4-Difluorobenzene (1)239000 3.592 221565 3.583 60 - 140108 0.0090 +/-0.50
Chlorobenzene-d5 (1)177824 5.163 168934 5.163 60 - 140105 0.0000 +/-0.50
SG-5 (22J1275-05 )Lab File ID: K22A283030.D Analyzed: 10/11/22 02:47
Bromochloromethane (1)84949 3.01 84069 2.991 60 - 140101 0.0190 +/-0.50
1,4-Difluorobenzene (1)216535 3.597 221565 3.583 60 - 14098 0.0140 +/-0.50
Chlorobenzene-d5 (1)183122 5.168 168934 5.163 60 - 140108 0.0050 +/-0.50
SG-5 (22J1275-05RE1 )Lab File ID: K22A283031.D Analyzed: 10/11/22 03:15
Bromochloromethane (1)88999 3 84069 2.991 60 - 140106 0.0090 +/-0.50
1,4-Difluorobenzene (1)240852 3.592 221565 3.583 60 - 140109 0.0090 +/-0.50
Chlorobenzene-d5 (1)183191 5.163 168934 5.163 60 - 140108 0.0000 +/-0.50
Page 21 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S077732-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
1.122678A 12.1 305.60 1.0015045.00Acetone
0.7067398A 11.5 305.58 0.6337045.00Benzene
0.7193531A 62.7 *308.14 0.44210815.00Benzyl chloride
0.522949A 16.6 305.83 0.44847425.00Bromodichloromethane
0.5840482A 9.9 305.50 0.53136085.00Bromoform
0.6432621A 13.2 305.66 0.568465.00Bromomethane
0.6014678A 21.7 306.09 0.49412945.001,3-Butadiene
1.24985A 9.3 305.47 1.1433395.002-Butanone (MEK)
2.207786A 5.1 305.25 2.1010975.00Carbon Disulfide
0.4369066A 21.9 306.10 0.35837935.00Carbon Tetrachloride
0.7789551A 6.6 305.33 0.73073575.00Chlorobenzene
0.4186656A 12.3 305.61 0.37289695.00Chloroethane
1.27461A 5.7 305.28 1.2059735.00Chloroform
0.6764729A 15.8 305.79 0.58435035.00Chloromethane
0.2790477A 12.8 305.64 0.24743965.00Cyclohexane
0.6045438A 12.7 305.63 0.53656275.00Dibromochloromethane
0.5380373A 14.6 305.73 0.46964285.001,2-Dibromoethane (EDB)
0.6120923A 12.8 305.64 0.54254115.001,2-Dichlorobenzene
0.6454971A 15.7 305.79 0.55776855.001,3-Dichlorobenzene
0.5975446A 23.4 306.17 0.48416785.001,4-Dichlorobenzene
1.688727A 17.5 305.87 1.4373685.00Dichlorodifluoromethane (Freon 12)
1.184037A 19.2 305.96 0.99331175.001,1-Dichloroethane
0.8421654A 10.7 305.54 0.76049545.001,2-Dichloroethane
1.131299A 10.3 305.52 1.0254175.001,1-Dichloroethylene
0.8503872A 4.0 305.20 0.81743615.00cis-1,2-Dichloroethylene
0.9528744A 15.3 305.76 0.82655715.00trans-1,2-Dichloroethylene
0.2914395A 15.4 305.77 0.25255515.001,2-Dichloropropane
0.4027712A -0.4 304.98 0.40422685.00cis-1,3-Dichloropropene
0.3481994A 23.4 306.17 0.28217545.00trans-1,3-Dichloropropene
1.818011A 15.7 305.79 1.5711765.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.1333424A 6.5 305.32 0.12523265.001,4-Dioxane
0.2626224A 11.8 305.59 0.23481145.00Ethanol
0.2236449A 24.4 306.22 0.17977625.00Ethyl Acetate
1.298969A 11.4 305.57 1.1661035.00Ethylbenzene
1.222205A 12.0 305.60 1.0915375.004-Ethyltoluene
0.2981482A 25.7 306.29 0.23709755.00Heptane
0.3329584A -13.4 304.33 0.38469915.00Hexachlorobutadiene
0.7204939L 13.7 305.68 0.61173145.00Hexane
Page 22 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S077732-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.6334497A 19.7 305.98 0.52934325.002-Hexanone (MBK)
1.474579A 19.6 305.98 1.2331515.00Isopropanol
1.931309A 37.6 *306.88 1.4039195.00Methyl tert-Butyl Ether (MTBE)
0.8278723A 6.8 305.34 0.77496645.00Methylene Chloride
0.1545226A 49.0 *307.45 0.10367325.004-Methyl-2-pentanone (MIBK)
0.8383298A -7.5 304.62 0.90672085.00Naphthalene
0.6055788A 27.3 306.36 0.47577555.00Propene
0.7140493A 15.3 305.76 0.61955725.00Styrene
0.8862633A 15.9 305.79 0.76495215.001,1,2,2-Tetrachloroethane
0.3991618A -0.8 304.96 0.40254575.00Tetrachloroethylene
0.7375085A 19.1 305.96 0.61923625.00Tetrahydrofuran
1.040994A 8.6 305.43 0.95887535.00Toluene
0.2971101A 2.9 305.14 0.28885585.001,2,4-Trichlorobenzene
0.5016532A 25.3 306.26 0.40050755.001,1,1-Trichloroethane
0.3769709A 12.9 305.64 0.3339565.001,1,2-Trichloroethane
0.2970361A 11.3 305.56 0.26692125.00Trichloroethylene
1.547833A 13.6 305.68 1.3627485.00Trichlorofluoromethane (Freon 11)
1.515251A 15.6 305.78 1.3112435.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
1.055352A 16.0 305.80 0.91012065.001,2,4-Trimethylbenzene
1.127039A 21.1 306.06 0.93057165.001,3,5-Trimethylbenzene
1.209102A -17.0 304.15 1.4567695.00Vinyl Acetate
0.7893516A 17.8 305.89 0.67006745.00Vinyl Chloride
1.09388A 10.5 3011.0 0.990172810.0m&p-Xylene
1.054471A 17.1 305.85 0.90063785.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
Page 23 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,NY,ME,NHAcetone
AIHA,FL,NJ,NY,ME,NH,VABenzene
AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride
AIHA,NJ,NY,ME,NH,VABromodichloromethane
AIHA,NJ,NY,ME,NH,VABromoform
AIHA,FL,NJ,NY,ME,NHBromomethane
AIHA,NJ,NY,ME,NH,VA1,3-Butadiene
AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK)
AIHA,NJ,NY,ME,NH,VACarbon Disulfide
AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride
AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene
AIHA,FL,NJ,NY,ME,NH,VAChloroethane
AIHA,FL,NJ,NY,ME,NH,VAChloroform
AIHA,FL,NJ,NY,ME,NH,VAChloromethane
AIHA,NJ,NY,ME,NH,VACyclohexane
AIHA,NY,ME,NHDibromochloromethane
AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB)
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene
AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene
AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12)
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene
AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene
AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane
AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene
AIHA,NY,ME,NHtrans-1,3-Dichloropropene
AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
AIHA,NJ,NY,ME,NH,VA1,4-Dioxane
AIHAEthanol
AIHAEthyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene
AIHA,NJ4-Ethyltoluene
AIHA,NJ,NY,ME,NH,VAHeptane
AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene
AIHA,FL,NJ,NY,ME,NH,VAHexane
AIHA2-Hexanone (MBK)
AIHA,NY,ME,NHIsopropanol
AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE)
AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride
AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK)
NY,ME,NHNaphthalene
AIHAPropene
AIHA,FL,NJ,NY,ME,NH,VAStyrene
AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane
Page 24 of 28
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene
AIHATetrahydrofuran
AIHA,FL,NJ,NY,ME,NH,VAToluene
AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene
AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11)
AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene
AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride
AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene
AIHA,FL,NJ,NY,ME,NH,VAo-Xylene
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO 17025:2017AIHA 03/1/2024
10899 NELAPNew York State Department of HealthNY 04/1/2023
2516 NELAPNew Hampshire Environmental LabNH 02/5/2023
MA007 NELAPNew Jersey DEPNJ 06/30/2023
E871027 NELAPFlorida Department of HealthFL 06/30/2023
MA00100State of MaineME 06/9/2023
460217Commonwealth of VirginiaVA 12/14/2022
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APPENDIX C
NCDEQ Risk Calculator Output
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 1320/1328 South Tryon Property
Exposure Unit ID: Site Wide
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.7E-05 7.4E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.3E-06 5.8E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator