26070_Wilkinson Blvd II_RSR_20240131

Redevelopment Summary
Report - 2023
Wilkinson Boulevard Brownfields Site
Brownfields ID #26070-22-060
January 31, 2024 | Terracon Project Number: 71227190
Redevelopment Summary Report – 2023
Wilkinson Boulevard Brownfields Site ■ Charlotte, North Carolina
January 31, 2024 ■ Terracon Project No. 71227190

Facilities | Environmental | Geotechnical | Materials 2
Table of Contents
1.0 PROJECT INFORMATION ............................................................... 4
2.0 FIELD ACTIVITIES ....................................................................... 4
2.1 Soil Stockpile Sampling ........................................................................ 4
3.0 ANALYTICAL RESULTS .................................................................. 5
4.0 OFF-SITE DISPOSAL OF SOILS ..................................................... 6
5.0 CLOSING .................................................................................... 6

Redevelopment Summary Report – 2023
Wilkinson Boulevard Brownfields Site ■ Charlotte, North Carolina
January 31, 2024 ■ Terracon Project No. 71227190

Facilities | Environmental | Geotechnical | Materials 3
List of Tables
Table 1 Summary of Soil Stockpile No. 1 Analytical Results

Table 2 Summary of Soil Stockpile No. 2 Analytical Results

List of Exhibits
Exhibit 1 Topographic Map

List of Appendices
Appendix A Field Documentation
Appendix B NCDEQ BRS Soil Export Approvals
Appendix C Laboratroy Analytical Reports
Appendix D Soil Export Weigh Tickets

Redevelopment Summary Report – 2023
Wilkinson Boulevard Brownfields Site ■ Charlotte, North Carolina
January 31, 2024 ■ Terracon Project No. 71227190

Facilities | Environmental | Geotechnical | Materials 4
1.0 PROJECT INFORMATION
The Wilkinson Boulevard Brownfields site is located at 2198 and 2130 and Wilkinson
Boulevard in Charlotte, Mecklenburg County, North Carolina (Exhibit 1) and consists of
an approximate 3.4-acre parcel previously developed with multiple commercial
warehouse buildings. Broadstone West End Venture, LLC (Prospective Developer or
“PD”) enrolled the site into the North Carolina Department of Environmental Quality
(NCDEQ) Brownfields Redevelopment Section (BRS) after environmental impacts were
identified as part of its due diligence activities prior to acquisition of the property.
Contaminants at the site included petroleum constituents and chlorinated solvents (e.g.
trichloroethylene and tetrachloroethylene) in groundwater and/or soil vapor. Minor
impacts from volatile organic compounds (VOCs), semi-volatile organic compounds
(SVOCs), and Resource Conservation and Recovery Act (RCRA) metals were also
identified within soil in select portions of the site.

Based on the identified contamination and the PD’s redevelopment plans, an
Environmental Management Plan (EMP) was developed and approved by the BRS on July
12, 2023. Redevelopment activities at the site began in August 2023. During the
calendar year 2023, redevelopment activities were limited to demolition of the former
site buildings and earthwork for site grading, utility installation, and deep foundation
installation. This report documents Terracon’s environmental oversight of the
redevelopment activities in accordance with the approved EMP.
2.0 FIELD ACTIVITIES
2.1 Soil Stockpile Sampling
During grading operations, the PD encountered geotechnically unsuitable soils that could
not be re-used on site. These soils were temporarily stockpiled on site as two separate
stockpiles, referred to herein as Stockpile No. 1 and Stockpile No. 2. Terracon mobilized
to collect soil samples from Stockpile No. 1 on October 16, 2023 and from Stockpile No.
2 on November 17, 2023 to determine an appropriate off-site disposal facility for export
of the soils. The PD estimated the Stockpile No. 1 to be approximately 500 cubic yards
and Stockpile No. 2 to be 2,000 cubic yards in volume. Terracon collected a total of five
composite soil samples (CS-01 through CS-05) and associated quality assurance/quality
control samples (two duplicate samples, one matrix spike/matrix spike duplicate, and
two equipment blanks) to characterize the soils for disposal.
The soils were sampled at a frequency of one sample per approximately 500 cubic yards
by advancing a decontaminated hand auger approximately two to three feet into the
stockpiles. Three boring locations (aliquots) were advanced per 500 cubic yard section of
the stockpiles. The soils from each of aliquot were divided equally with one half being
placed in a sealed plastic bag and being kept in a cooler on ice, and the other half being
placed in a sealed plastic bag and left in the sun to volatilize for approximately 5 to 10
Redevelopment Summary Report – 2023
Wilkinson Boulevard Brownfields Site ■ Charlotte, North Carolina
January 31, 2024 ■ Terracon Project No. 71227190

Facilities | Environmental | Geotechnical | Materials 5
minutes. After the volatilization period, the head space of the bag left in the sun was
screened for volatile organic vapors using a photo-ionization detector (PID). A grab
sample for VOC analysis was collected from the sealed plastic bag that had been stored
on ice from the aliquot exhibiting the highest PID reading. PID readings collected during
the stockpile sampling ranged from 1.9 to 9.8 parts per million (ppm). For composite
sample collection, soils from the sealed plastic bags placed on ice from each aliquot were
composited using a decontaminated stainless-steel bowl and spoon via the sample
homogenization procedures outlined in the U.S. Environmental Protection Agency’s
(EPA) SESDPROC-300-R3 (June 11, 2020) guidance.
The soil samples were submitted to Pace Analytical of Huntersville, North Carolina with
chain-of-custody documentation for analysis of VOCs via EPA Method 8260, SVOCs via
EPA Method 8270, RCRA 8 Metals via EPA Method 6010/7471, hexavalent chromium via
EPA Method 7199.
Terracon’s field documentation is included in Appendix A.
3.0 ANALYTICAL RESULTS
Laboratory results were compared to the NCDEQ Preliminary Soil Remediation Goals
(PSRGs; July 2023) as well as metals concentration data for the Old 27 Land Clearing
and Inert Debris (LCID) Landfill located in Mount Holly, North Carolina; the data for
which was provided by the BRS. Review of the laboratory analytical results indicated the
following:

◼ VOCs, SVOCs, and pesticides were not identified in the stockpile samples above
their most stringent PSRGs.

◼ Arsenic was identified at concentrations ranging from 0.55 to 2.6 milligrams per
kilogram (mg/kg), with some detections exceeding its residential PSRG (0.68 mg/kg).
The average arsenic concentration calculated from the five soil samples for Old 27
Landfill provided by the BRS is 1.88 mg/kg, with a maximum detected concentration of
2.7 mg/kg.

◼ Hexavalent chromium was identified at concentrations ranging from 0.0033 to 0.5
mg/kg, with one detection exceeding its residential PSRG (0.31 mg/kg). For comparison
purposes, the average hexavalent chromium concentration calculated from the five soil
samples for Old 27 Landfill provided by the BRS is 0.85 mg/kg, with a maximum
detected concentration of 2.0 mg/kg.

The analytical results from the soil sampling are summarized in Tables 1 and 2. Based
on the lack of PSRG exceedances for other compounds and the broad equivalence of the
arsenic and hexavalent chromium concentrations within the stockpiles and Old 27
Redevelopment Summary Report – 2023
Wilkinson Boulevard Brownfields Site ■ Charlotte, North Carolina
January 31, 2024 ■ Terracon Project No. 71227190

Facilities | Environmental | Geotechnical | Materials 6
Landfill, Terracon requested approval from the BRS for the PD to export the stockpiled
soils to Old 27 Landfill. The BRS provided approval on October 27 and November 27,
2023 for export of soils from Stockpile No. 1 and Stockpile No. 2, respectively. Copies of
the BRS approvals are included in Appendix B. The laboratory analytical reports are
included in Appendix C.
4.0 OFF-SITE DISPOSAL OF SOILS
Between October 30 and December 15, 2023, the PD exported the stockpiled soils to Old
27 Landfill. Copies of the gate tickets provided by Old 27 Landfill are provided in
Appendix D. It should be noted that Old 27 Landfill reportedly does not have weigh
scales. In addition, as an LCID, it does not require waste manifests.
5.0 CLOSING
Redevelopment activities are on-going at the site. Planned environmental activities at
the site during 2024 will include oversight of vapor intrusion mitigation system at the
proposed building in accordance with the approved EMP and approved Vapor Mitigation
Plan. The extent of environmental-related activities will be subject to the construction
schedule. The next annual redevelopment report is due January 31, 2024.

TABLES
Table 1 – Summary of Soil Stockpile No. 1 Analytical Results
Table 2 – Summary of Soil Stockpile No. 2 Analytical Results
Table 1
Summary of Soil Stockpile No. 1 Analytical Results
Wilkinson Boulevard Brownfields Site
Brownfields ID 26070-22-060
2198-2130 Wilkinson Boulevard
Charlotte, Mecklenburg County, North Carolina
Terracon Project No. 71227190
Sample ID CS-01 CS-DUP-01
Highest PID Reading (ppm)2.2 2.2
Volatile Organic Compounds by EPA Method 8260
Benzene 0.0049 J 0.0063 J NA 0.01 1.2 5.4
Ethylbenzene 0.0045 J 0.0083 J NA 13 6.1 27
Toluene 0.0181 0.0075 J NA 8.3 990 9,700
1,2,4-Trimethylbenzene <0.0052 0.0064 J NA 12 63 370
m&p-Xylene 0.0073 J 0.0091 J NA 9.8 120 500
Xylene (Total)0.0073 J 0.0091 J NA 9.9 120 530
Semi-Volatile Organic Compounds by EPA Method 8270
Compounds Not Detected Above Laboratory MDLs
RCRA Metals by EPA Method 6010/7471 (Chromium VI by Method 7199)
Arsenic 0.67 0.55 J 1.88 5.8 0.68 3.0
Barium 69.7 82.4 126 580 3,100 47,000
Cadmium 0.38 0.40 <0.048 3.0 1.4 20
Chromium (III)34.4 37.5 52.4 360,000 23,000 350,000
Chromium (VI)0.0033 J <0.0013 0.85 3.8 0.31 6.5
Lead 49.3 36.0 10.4 270 400 800
Mercury 0.042 0.044 0.454 NE 4.7 70
Notes:
Samples Collected on 10/16/23.
Results are shown in milligrams per kilogram (mg/kg).
PID = Photo-ionization detector
ppm - parts per million
Only compounds detected above the laboratory method detection limits are shown.
Not Applicable
NE - Not Established
Detections are indicated in bold.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
PSRG - NCDEQ Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (July 2023)
PoG - Protection of Groundwater
Old 27 Landfill Average - Average concentration from 5 samples provided by North Carolina Brownfields Redevelopment Section as
representative of consituente concentrations at Old 27 Landfill in Mount Holly, North Carolina
Shaded cells indicate the detected concentrations exceed the regulatory threshold of the corresponding color.
PoG
PSRG
Residential
PSRG
Non-Residential
PSRGOld 27 Landfill
Table 2
Summary of Soil Stockpile No. 2 Analytical Results
Wilkinson Boulevard Brownfields Site
Brownfields ID 26070-22-060
2198-2130 Wilkinson Boulevard
Charlotte, Mecklenburg County, North Carolina
Terracon Project No. 71227190
Sample ID CS-02 CS-DUP-02
(CS-02)CS-03 CS-04 CS-05
Highest PID Reading (ppm)8.2 8.2 1.9 1.9 9.8
Volatile Organic Compounds by EPA Method 8260
Ethylbenzene 0.0055 J 0.005 J 0.0061 J 0.0052 J 0.0048 J NA 13 6.1 27
Toluene 0.0113 <0.0059 <0.0067 <0.0049 <0.0055 NA 8.3 990 9,700
p-Isopropyltoluene 0.0094 0.0068 J <0.0048 <0.0035 <0.0039 NA NE NE NE
Methyl Isobutyl Ketone (MIBK)<0.0073 0.0376 J <0.0094 <0.0068 <0.0076 NA 0.45 7,000 30,000
Naphthalene 0.009 0.014 0.0283 0.0048 J <0.0042 NA 0.39 2.1 8.8
1,2,4-Trimethylbenzene 0.0045 J <0.0044 <0.0058 <0.0042 <0.0047 NA 12 63 370
m&p-Xylene 0.0115 J <0.005 0.0071 J <0.0048 0.0055 J NA 9.8 120 500
o-Xylene 0.0059 J <0.0032 <0.0043 <0.0031 <0.0035 NA 9.8 140 590
Xylene (Total)0.0174 <0.0042 0.0071 J <0.004 0.0055 J NA 9.9 120 530
Semi-Volatile Organic Compounds by EPA Method 8270
Compounds Not Detected Above Laboratory MDLs
RCRA Metals by EPA Method 6010/7471 (Chromium VI by Method 7199)
Arsenic 2.6 2.5 J 2.6 J 2.4 2.5 1.88 5.8 0.68 3.0
Barium 75.8 78.4 135 73.1 67.3 126 580 3,100 47,000
Cadmium 0.35 0.33 0.26 0.31 0.34 <0.048 3.0 1.4 20
Chromium (III)42.2 43.1 37.0 43.6 62.1 52.4 360,000 23,000 350,000
Chromium (VI)0.071 J 0.0017 J 0.10 J 0.50 J 0.005J 0.85 3.8 0.31 6.5
Lead 28.0 21.5 16.1 18.2 22.5 10.4 270 400 800
Mercury 0.060 0.052 <0.0044 0.057 0.049 0.454 NE 4.7 70
Notes:
Samples Collected on 11/7/23.
Results are shown in milligrams per kilogram (mg/kg).
PID = Photo-ionization detector
ppm - parts per million
Only compounds detected above the laboratory method detection limits are shown.
Not Applicable
NE - Not Established
Detections are indicated in bold.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
PSRG - NCDEQ Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (July 2023)
PoG - Protection of Groundwater
Old 27 Landfill Average - Average concentration from 5 samples provided by North Carolina Brownfields Redevelopment Section as
representative of consituente concentrations at Old 27 Landfill in Mount Holly, North Carolina
Shaded cells indicate the detected concentrations exceed the regulatory threshold of the corresponding color.
PoG
PSRG
Residential
PSRG
Non-Residential
PSRGOld 27 Landfill

EXHIBITS
Exhibit 1 – Topographic Map

TOPOGRAPHIC MAP
Wilkinson Boulevard Brownfields Site
2198 & 2300 Wilkinson Blvd
Charlotte, North Carolina
Brownfields ID No. 26070-22-060
TOPOGRAPHIC MAP IMAGE COURTESY OF THE U.S. GEOLOGICAL SURVEYQUADRANGLES INCLUDE: CHARLOTTE WEST, NC (1/1/1993) and CHARLOTTE EAST, NC (1/1/1988).
2701 Westport Rd
Charlotte, NC 28208-3608
71227190Project Manager:
Drawn by:
Checked by:
Approved by:
WOF
RSB
RSB
1”=2,000’
Figure 1
Jan 2024
Project No.
Scale:
File Name:
Date:
1
WOF Exhibit
APPROXIMATE
SITE BOUNDARY

APPENDIX A
Field Documentation

APPENDIX B
NCDEQ BRS Soil Export Approvals
October 27, 2023
Sent Via E-mail
Donald SantosBroadstone West End Venture, LLC
200 Providence Road, Suite 250
Charlotte, NC [e-mail]
Subject: Brownfields Soil Management Options Wilkinson Blvd. Brownfields Property
2198 and 2130 Wilkinson Boulevard
Charlotte, Mecklenburg County
Brownfields Project Number 26070-22-060
Mr. Santos:
The North Carolina Department of Environmental Quality Brownfields Redevelopment Section (DEQ Brownfields) received and reviewed the email request for soil export dated October 24,
2023 on your behalf from Terracon, to export approximately 270 cubic yards of soil
located at the above referenced Brownfields Property.
Based on our review of the data provided, the DEQ Brownfields agrees that these soils
may be exported to Old 27 Landfill located at 123 Tate Street, Mt. Holly, Gaston County, NC (permit number 36-A-LCID) as requested. Other options may be available; however,
DEQ Brownfields requires that the receiving facility be identified and approved prior to
export. The receiving facility should have metals concentrations which are consistent with
those from the Brownfields Property.
All soil export must be conducted under a DEQ Brownfields approved Environmental
Management Plan (EMP). Soils should be field screened during excavation prior to export from
the property. If unanticipated impacts are identified during excavation, please refer to the EMP
for further actions and cease transfer until appropriate characterization can be completed. In
addition, in accordance with the Wilkinson Blvd. EMP, an annual Redevelopment
Summary Report will be submitted to DEQ Brownfields. Details related to the disposition
of this soil including but not limited to, total volume, general description of field screening
efforts, etc. should be included with the Redevelopment Summary Report.
Please be advised that this approval does not waive any applicable requirement to obtain any
necessary permits, licenses or certifications which may be required from other state or local
October 27, 2023
Page 2
entities. If you have questions about this correspondence or require additional information, please
feel free to contact me by phone at 336-776- 9742 or by email at [e-mail].
Sincerely,
Seth Titley
Project Manager
Brownfields Redevelopment Section
ec: William Frazier, Terracon
November 27, 2023
Sent Via E-mail
Kristen VinesettBroadstone West End Venture, LLC
200 Providence Road, Suite 250
Charlotte, NC [e-mail]
Subject: Brownfields Soil Management Options Wilkinson Blvd. Brownfields Property
2198 and 2130 Wilkinson Boulevard
Charlotte, Mecklenburg County
Brownfields Project Number 26070-22-060
Ms. Vinesett:
The North Carolina Department of Environmental Quality Brownfields Redevelopment Section (DEQ Brownfields) received and reviewed the email request for soil export dated November 20, 2023 on your behalf from Terracon, to export approximately 2000 cubic yards of
soil located at the above referenced Brownfields Property.
Based on our review of the data provided, the DEQ Brownfields agrees that these soils
may be exported to Old 27 Landfill located at 123 Tate Street, Mt. Holly, Gaston County, NC (permit number 36-A-LCID) as requested. Other options may be available; however,
DEQ Brownfields requires that the receiving facility be identified and approved prior to
export. The receiving facility should have metals concentrations which are consistent with
those from the Brownfields Property.
All soil export must be conducted under a DEQ Brownfields approved Environmental
Management Plan (EMP). Soils should be field screened during excavation prior to export from
the property. If unanticipated impacts are identified during excavation, please refer to the EMP
for further actions and cease transfer until appropriate characterization can be completed. In
addition, in accordance with the Wilkinson Blvd. EMP, an annual Redevelopment
Summary Report will be submitted to DEQ Brownfields. Details related to the disposition
of this soil including but not limited to, total volume, general description of field screening
efforts, etc. should be included with the Redevelopment Summary Report.
Please be advised that this approval does not waive any applicable requirement to obtain any
necessary permits, licenses or certifications which may be required from other state or local
November 27, 2023
Page 2
entities. If you have questions about this correspondence or require additional information, please
feel free to contact me by phone at 336-776- 9742 or by email at [e-mail].
Sincerely,
Seth Titley
Project Manager
Brownfields Redevelopment Section
ec: William Frazier, Terracon

APPENDIX C
Laboratory Analytical Reports
#=CL#
October 20, 2023
LIMS USE: FR - WILL FRAZIER
LIMS OBJECT ID: 92693461
92693461
Project:
Pace Project No.:
RE:
Will Frazier
Terracon
2701 Westport Rd
Charlotte, NC 28208
BROADSTONE WEST END - 71227190
Dear Will Frazier:
Enclosed are the analytical results for sample(s) received by the laboratory on October 16, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
704-977-0943
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 50
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 50
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Lab ID Sample ID Matrix Date Collected Date Received
92693461001 CS-01 Solid 10/16/23 11:25 10/16/23 14:42
92693461002 CS-DUP-01 Solid 10/16/23 11:30 10/16/23 14:42
92693461003 EB-01 Water 10/16/23 12:00 10/16/23 14:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 50
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92693461001 CS-01 EPA 7199 1 PASI-CSMS1
EPA 6010 7 PASI-OTMA
EPA 7471 1 PASI-OJNK
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92693461002 CS-DUP-01 EPA 7199 1 PASI-CSMS1
EPA 6010 7 PASI-OTMA
EPA 7471 1 PASI-OJNK
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92693461003 EB-01 EPA 8260D 63 PASI-CTMH
PASI-C = Pace Analytical Services - Charlotte
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Sample:CS-01 Lab ID:92693461001 Collected:10/16/23 11:25 Received:10/16/23 14:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.0033J mg/kg 10/19/23 17:31 18540-29-9 B10/19/23 09:551.2 0.0012 1
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - Ormond Beach
6010 MET ICP
Arsenic 0.67 mg/kg 10/19/23 15:22 7440-38-210/18/23 10:390.66 0.33 1
Barium 69.7 mg/kg 10/19/23 15:22 7440-39-310/18/23 10:390.66 0.11 1
Cadmium 0.38 mg/kg 10/19/23 15:22 7440-43-910/18/23 10:390.066 0.033 1
Chromium 34.4 mg/kg 10/19/23 15:22 7440-47-310/18/23 10:390.33 0.17 1
Lead 49.3 mg/kg 10/19/23 15:22 7439-92-110/18/23 10:390.66 0.33 1
Selenium ND mg/kg 10/19/23 15:22 7782-49-210/18/23 10:390.99 0.50 1
Silver ND mg/kg 10/19/23 15:22 7440-22-410/18/23 10:390.33 0.073 1
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
7471 Mercury
Mercury 0.042 mg/kg 10/19/23 13:21 7439-97-610/18/23 15:450.011 0.0057 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 10/18/23 15:34 83-32-910/17/23 16:304011411
Acenaphthylene ND ug/kg 10/18/23 15:34 208-96-810/17/23 16:304011411
Aniline ND ug/kg 10/18/23 15:34 62-53-3 v110/17/23 16:304011571
Anthracene ND ug/kg 10/18/23 15:34 120-12-710/17/23 16:304011311
Benzo(a)anthracene ND ug/kg 10/18/23 15:34 56-55-310/17/23 16:304011341
Benzo(a)pyrene ND ug/kg 10/18/23 15:34 50-32-810/17/23 16:304011381
Benzo(b)fluoranthene ND ug/kg 10/18/23 15:34 205-99-210/17/23 16:304011341
Benzo(g,h,i)perylene ND ug/kg 10/18/23 15:34 191-24-210/17/23 16:304011551
Benzo(k)fluoranthene ND ug/kg 10/18/23 15:34 207-08-910/17/23 16:304011411
Benzoic Acid ND ug/kg 10/18/23 15:34 65-85-0 v110/17/23 16:3020008611
Benzyl alcohol ND ug/kg 10/18/23 15:34 100-51-610/17/23 16:308013031
4-Bromophenylphenyl ether ND ug/kg 10/18/23 15:34 101-55-310/17/23 16:304011541
Butylbenzylphthalate ND ug/kg 10/18/23 15:34 85-68-710/17/23 16:304011691
4-Chloro-3-methylphenol ND ug/kg 10/18/23 15:34 59-50-710/17/23 16:308012821
4-Chloroaniline ND ug/kg 10/18/23 15:34 106-47-810/17/23 16:308013141
bis(2-Chloroethoxy)methane ND ug/kg 10/18/23 15:34 111-91-110/17/23 16:304011661
bis(2-Chloroethyl) ether ND ug/kg 10/18/23 15:34 111-44-410/17/23 16:304011511
2-Chloronaphthalene ND ug/kg 10/18/23 15:34 91-58-710/17/23 16:304011591
2-Chlorophenol ND ug/kg 10/18/23 15:34 95-57-810/17/23 16:304011511
4-Chlorophenylphenyl ether ND ug/kg 10/18/23 15:34 7005-72-310/17/23 16:304011491
Chrysene ND ug/kg 10/18/23 15:34 218-01-910/17/23 16:304011461
Dibenz(a,h)anthracene ND ug/kg 10/18/23 15:34 53-70-310/17/23 16:304011541
Dibenzofuran ND ug/kg 10/18/23 15:34 132-64-910/17/23 16:304011441
1,2-Dichlorobenzene ND ug/kg 10/18/23 15:34 95-50-110/17/23 16:304011441
1,3-Dichlorobenzene ND ug/kg 10/18/23 15:34 541-73-110/17/23 16:304011421
1,4-Dichlorobenzene ND ug/kg 10/18/23 15:34 106-46-710/17/23 16:304011531
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Sample:CS-01 Lab ID:92693461001 Collected:10/16/23 11:25 Received:10/16/23 14:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 10/18/23 15:34 91-94-110/17/23 16:308012711
2,4-Dichlorophenol ND ug/kg 10/18/23 15:34 120-83-210/17/23 16:304011571
Diethylphthalate ND ug/kg 10/18/23 15:34 84-66-210/17/23 16:304011471
2,4-Dimethylphenol ND ug/kg 10/18/23 15:34 105-67-910/17/23 16:304011661
Dimethylphthalate ND ug/kg 10/18/23 15:34 131-11-310/17/23 16:304011461
Di-n-butylphthalate ND ug/kg 10/18/23 15:34 84-74-210/17/23 16:304011351
4,6-Dinitro-2-methylphenol ND ug/kg 10/18/23 15:34 534-52-110/17/23 16:308013741
2,4-Dinitrophenol ND ug/kg 10/18/23 15:34 51-28-5 v110/17/23 16:30200012401
2,4-Dinitrotoluene ND ug/kg 10/18/23 15:34 121-14-210/17/23 16:304011541
2,6-Dinitrotoluene ND ug/kg 10/18/23 15:34 606-20-210/17/23 16:304011471
Di-n-octylphthalate ND ug/kg 10/18/23 15:34 117-84-010/17/23 16:304011581
bis(2-Ethylhexyl)phthalate ND ug/kg 10/18/23 15:34 117-81-710/17/23 16:304011551
Fluoranthene ND ug/kg 10/18/23 15:34 206-44-010/17/23 16:304011371
Fluorene ND ug/kg 10/18/23 15:34 86-73-710/17/23 16:304011411
Hexachloro-1,3-butadiene ND ug/kg 10/18/23 15:34 87-68-310/17/23 16:304011741
Hexachlorobenzene ND ug/kg 10/18/23 15:34 118-74-110/17/23 16:304011571
Hexachlorocyclopentadiene ND ug/kg 10/18/23 15:34 77-47-4 v210/17/23 16:304012291
Hexachloroethane ND ug/kg 10/18/23 15:34 67-72-110/17/23 16:304011531
Indeno(1,2,3-cd)pyrene ND ug/kg 10/18/23 15:34 193-39-510/17/23 16:304011581
Isophorone ND ug/kg 10/18/23 15:34 78-59-110/17/23 16:304011781
1-Methylnaphthalene ND ug/kg 10/18/23 15:34 90-12-010/17/23 16:304011411
2-Methylnaphthalene ND ug/kg 10/18/23 15:34 91-57-610/17/23 16:304011601
2-Methylphenol(o-Cresol)ND ug/kg 10/18/23 15:34 95-48-710/17/23 16:304011641
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/18/23 15:34 15831-10-410/17/23 16:304011611
Naphthalene ND ug/kg 10/18/23 15:34 91-20-310/17/23 16:304011361
2-Nitroaniline ND ug/kg 10/18/23 15:34 88-74-410/17/23 16:3020003281
3-Nitroaniline ND ug/kg 10/18/23 15:34 99-09-210/17/23 16:3020003141
4-Nitroaniline ND ug/kg 10/18/23 15:34 100-01-6 v110/17/23 16:308013051
Nitrobenzene ND ug/kg 10/18/23 15:34 98-95-310/17/23 16:304011861
2-Nitrophenol ND ug/kg 10/18/23 15:34 88-75-510/17/23 16:304011741
4-Nitrophenol ND ug/kg 10/18/23 15:34 100-02-710/17/23 16:3020007741
N-Nitrosodimethylamine ND ug/kg 10/18/23 15:34 62-75-910/17/23 16:304011351
N-Nitroso-di-n-propylamine ND ug/kg 10/18/23 15:34 621-64-710/17/23 16:304011511
N-Nitrosodiphenylamine ND ug/kg 10/18/23 15:34 86-30-610/17/23 16:304011421
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/18/23 15:34 108-60-110/17/23 16:304011911
Pentachlorophenol ND ug/kg 10/18/23 15:34 87-86-510/17/23 16:308013921
Phenanthrene ND ug/kg 10/18/23 15:34 85-01-810/17/23 16:304011311
Phenol ND ug/kg 10/18/23 15:34 108-95-210/17/23 16:304011781
Pyrene ND ug/kg 10/18/23 15:34 129-00-010/17/23 16:304011631
Pyridine ND ug/kg 10/18/23 15:34 110-86-1 v110/17/23 16:304011261
1,2,4-Trichlorobenzene ND ug/kg 10/18/23 15:34 120-82-110/17/23 16:304011581
2,4,5-Trichlorophenol ND ug/kg 10/18/23 15:34 95-95-410/17/23 16:304011831
2,4,6-Trichlorophenol ND ug/kg 10/18/23 15:34 88-06-210/17/23 16:304011651
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Sample:CS-01 Lab ID:92693461001 Collected:10/16/23 11:25 Received:10/16/23 14:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)53 %10/18/23 15:34 4165-60-010/17/23 16:3010-130 1
2-Fluorobiphenyl (S)48 %10/18/23 15:34 321-60-810/17/23 16:3010-130 1
Terphenyl-d14 (S)59 %10/18/23 15:34 1718-51-010/17/23 16:3010-130 1
Phenol-d6 (S)55 %10/18/23 15:34 13127-88-310/17/23 16:3010-130 1
2-Fluorophenol (S)51 %10/18/23 15:34 367-12-410/17/23 16:3010-130 1
2,4,6-Tribromophenol (S)60 %10/18/23 15:34 118-79-610/17/23 16:3010-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 10/18/23 22:52 67-64-110/16/23 18:2317556.1 1
Benzene 4.9J ug/kg 10/18/23 22:52 71-43-2 M110/16/23 18:238.7 3.5 1
Bromobenzene ND ug/kg 10/18/23 22:52 108-86-110/16/23 18:238.7 2.8 1
Bromochloromethane ND ug/kg 10/18/23 22:52 74-97-510/16/23 18:238.7 2.6 1
Bromodichloromethane ND ug/kg 10/18/23 22:52 75-27-410/16/23 18:238.7 3.4 1
Bromoform ND ug/kg 10/18/23 22:52 75-25-210/16/23 18:238.7 3.1 1
Bromomethane ND ug/kg 10/18/23 22:52 74-83-9 IH10/16/23 18:2334.9 27.1 1
2-Butanone (MEK)ND ug/kg 10/18/23 22:52 78-93-310/16/23 18:2317541.9 1
n-Butylbenzene ND ug/kg 10/18/23 22:52 104-51-810/16/23 18:238.7 5.5 1
sec-Butylbenzene ND ug/kg 10/18/23 22:52 135-98-810/16/23 18:238.7 3.8 1
tert-Butylbenzene ND ug/kg 10/18/23 22:52 98-06-610/16/23 18:238.7 3.1 1
Carbon tetrachloride ND ug/kg 10/18/23 22:52 56-23-510/16/23 18:238.7 3.3 1
Chlorobenzene ND ug/kg 10/18/23 22:52 108-90-710/16/23 18:238.7 5.0 1
Chloroethane ND ug/kg 10/18/23 22:52 75-00-310/16/23 18:2317.5 6.7 1
Chloroform ND ug/kg 10/18/23 22:52 67-66-310/16/23 18:238.7 7.3 1
Chloromethane ND ug/kg 10/18/23 22:52 74-87-310/16/23 18:2317.5 7.3 1
2-Chlorotoluene ND ug/kg 10/18/23 22:52 95-49-810/16/23 18:238.7 3.1 1
4-Chlorotoluene ND ug/kg 10/18/23 22:52 106-43-410/16/23 18:238.7 4.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/18/23 22:52 96-12-810/16/23 18:238.7 3.4 1
Dibromochloromethane ND ug/kg 10/18/23 22:52 124-48-110/16/23 18:238.7 4.9 1
1,2-Dibromoethane (EDB)ND ug/kg 10/18/23 22:52 106-93-4 M110/16/23 18:238.7 3.8 1
Dibromomethane ND ug/kg 10/18/23 22:52 74-95-3 M110/16/23 18:238.7 1.9 1
1,2-Dichlorobenzene ND ug/kg 10/18/23 22:52 95-50-110/16/23 18:238.7 3.1 1
1,3-Dichlorobenzene ND ug/kg 10/18/23 22:52 541-73-110/16/23 18:238.7 2.7 1
1,4-Dichlorobenzene ND ug/kg 10/18/23 22:52 106-46-710/16/23 18:238.7 2.3 1
Dichlorodifluoromethane ND ug/kg 10/18/23 22:52 75-71-8 IH,v110/16/23 18:2317.5 8.9 1
1,1-Dichloroethane ND ug/kg 10/18/23 22:52 75-34-310/16/23 18:238.7 3.6 1
1,2-Dichloroethane ND ug/kg 10/18/23 22:52 107-06-210/16/23 18:238.7 5.8 1
1,1-Dichloroethene ND ug/kg 10/18/23 22:52 75-35-410/16/23 18:238.7 3.6 1
cis-1,2-Dichloroethene ND ug/kg 10/18/23 22:52 156-59-2 M110/16/23 18:238.7 3.0 1
trans-1,2-Dichloroethene ND ug/kg 10/18/23 22:52 156-60-510/16/23 18:238.7 7.4 1
1,2-Dichloropropane ND ug/kg 10/18/23 22:52 78-87-5 M110/16/23 18:238.7 2.6 1
1,3-Dichloropropane ND ug/kg 10/18/23 22:52 142-28-910/16/23 18:238.7 2.7 1
2,2-Dichloropropane ND ug/kg 10/18/23 22:52 594-20-710/16/23 18:238.7 6.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Sample:CS-01 Lab ID:92693461001 Collected:10/16/23 11:25 Received:10/16/23 14:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 10/18/23 22:52 563-58-610/16/23 18:238.7 4.2 1
cis-1,3-Dichloropropene ND ug/kg 10/18/23 22:52 10061-01-510/16/23 18:238.7 2.4 1
trans-1,3-Dichloropropene ND ug/kg 10/18/23 22:52 10061-02-610/16/23 18:238.7 3.0 1
Diisopropyl ether ND ug/kg 10/18/23 22:52 108-20-310/16/23 18:238.7 2.4 1
Ethylbenzene 4.5J ug/kg 10/18/23 22:52 100-41-410/16/23 18:238.7 4.1 1
Hexachloro-1,3-butadiene ND ug/kg 10/18/23 22:52 87-68-310/16/23 18:2317.5 14.3 1
2-Hexanone ND ug/kg 10/18/23 22:52 591-78-610/16/23 18:2387.4 8.4 1
Isopropylbenzene (Cumene)ND ug/kg 10/18/23 22:52 98-82-810/16/23 18:238.7 3.0 1
p-Isopropyltoluene ND ug/kg 10/18/23 22:52 99-87-610/16/23 18:238.7 4.3 1
Methylene Chloride ND ug/kg 10/18/23 22:52 75-09-210/16/23 18:2334.9 23.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/18/23 22:52 108-10-110/16/23 18:2387.4 8.4 1
Methyl-tert-butyl ether ND ug/kg 10/18/23 22:52 1634-04-4 M110/16/23 18:238.7 3.3 1
Naphthalene ND ug/kg 10/18/23 22:52 91-20-310/16/23 18:238.7 4.6 1
n-Propylbenzene ND ug/kg 10/18/23 22:52 103-65-110/16/23 18:238.7 3.1 1
Styrene ND ug/kg 10/18/23 22:52 100-42-510/16/23 18:238.7 2.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/18/23 22:52 630-20-610/16/23 18:238.7 3.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/18/23 22:52 79-34-510/16/23 18:238.7 2.3 1
Tetrachloroethene ND ug/kg 10/18/23 22:52 127-18-410/16/23 18:238.7 2.8 1
Toluene 18.1 ug/kg 10/18/23 22:52 108-88-310/16/23 18:238.7 6.0 1
1,2,3-Trichlorobenzene ND ug/kg 10/18/23 22:52 87-61-610/16/23 18:238.7 7.1 1
1,2,4-Trichlorobenzene ND ug/kg 10/18/23 22:52 120-82-110/16/23 18:238.7 7.3 1
1,1,1-Trichloroethane ND ug/kg 10/18/23 22:52 71-55-610/16/23 18:238.7 4.5 1
1,1,2-Trichloroethane ND ug/kg 10/18/23 22:52 79-00-510/16/23 18:238.7 2.9 1
Trichloroethene ND ug/kg 10/18/23 22:52 79-01-610/16/23 18:238.7 7.0 1
Trichlorofluoromethane ND ug/kg 10/18/23 22:52 75-69-410/16/23 18:238.7 4.8 1
1,2,3-Trichloropropane ND ug/kg 10/18/23 22:52 96-18-410/16/23 18:238.7 4.4 1
1,2,4-Trimethylbenzene ND ug/kg 10/18/23 22:52 95-63-610/16/23 18:238.7 5.2 1
1,3,5-Trimethylbenzene ND ug/kg 10/18/23 22:52 108-67-810/16/23 18:238.7 2.9 1
Vinyl acetate ND ug/kg 10/18/23 22:52 108-05-410/16/23 18:2387.4 18.0 1
Vinyl chloride ND ug/kg 10/18/23 22:52 75-01-410/16/23 18:2317.5 4.4 1
Xylene (Total)7.3J ug/kg 10/18/23 22:52 1330-20-710/16/23 18:2317.5 5.0 1
m&p-Xylene 7.3J ug/kg 10/18/23 22:52 179601-23-110/16/23 18:2317.5 6.0 1
o-Xylene ND ug/kg 10/18/23 22:52 95-47-610/16/23 18:238.7 3.9 1
Surrogates
Toluene-d8 (S)102 %10/18/23 22:52 2037-26-510/16/23 18:2370-130 1
4-Bromofluorobenzene (S)101 %10/18/23 22:52 460-00-410/16/23 18:2370-130 1
1,2-Dichloroethane-d4 (S)100 %10/18/23 22:52 17060-07-010/16/23 18:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.3 %10/17/23 17:44 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Sample:CS-DUP-01 Lab ID:92693461002 Collected:10/16/23 11:30 Received:10/16/23 14:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent ND mg/kg 10/19/23 17:48 18540-29-910/19/23 09:551.3 0.0013 1
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - Ormond Beach
6010 MET ICP
Arsenic 0.55J mg/kg 10/19/23 15:26 7440-38-210/18/23 10:390.66 0.33 1
Barium 82.4 mg/kg 10/19/23 15:26 7440-39-310/18/23 10:390.66 0.11 1
Cadmium 0.40 mg/kg 10/19/23 15:26 7440-43-910/18/23 10:390.066 0.033 1
Chromium 37.5 mg/kg 10/19/23 15:26 7440-47-310/18/23 10:390.33 0.16 1
Lead 36.0 mg/kg 10/19/23 15:26 7439-92-110/18/23 10:390.66 0.33 1
Selenium ND mg/kg 10/19/23 15:26 7782-49-210/18/23 10:390.98 0.49 1
Silver ND mg/kg 10/19/23 15:26 7440-22-410/18/23 10:390.33 0.072 1
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
7471 Mercury
Mercury 0.044 mg/kg 10/19/23 13:23 7439-97-610/18/23 15:450.011 0.0055 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 10/19/23 08:35 83-32-910/18/23 14:184001411
Acenaphthylene ND ug/kg 10/19/23 08:35 208-96-810/18/23 14:184001411
Aniline ND ug/kg 10/19/23 08:35 62-53-310/18/23 14:184001571
Anthracene ND ug/kg 10/19/23 08:35 120-12-710/18/23 14:184001311
Benzo(a)anthracene ND ug/kg 10/19/23 08:35 56-55-310/18/23 14:184001331
Benzo(a)pyrene ND ug/kg 10/19/23 08:35 50-32-810/18/23 14:184001381
Benzo(b)fluoranthene ND ug/kg 10/19/23 08:35 205-99-210/18/23 14:184001331
Benzo(g,h,i)perylene ND ug/kg 10/19/23 08:35 191-24-210/18/23 14:184001551
Benzo(k)fluoranthene ND ug/kg 10/19/23 08:35 207-08-910/18/23 14:184001411
Benzoic Acid ND ug/kg 10/19/23 08:35 65-85-0 v110/18/23 14:1820008601
Benzyl alcohol ND ug/kg 10/19/23 08:35 100-51-610/18/23 14:188013031
4-Bromophenylphenyl ether ND ug/kg 10/19/23 08:35 101-55-310/18/23 14:184001541
Butylbenzylphthalate ND ug/kg 10/19/23 08:35 85-68-710/18/23 14:184001691
4-Chloro-3-methylphenol ND ug/kg 10/19/23 08:35 59-50-710/18/23 14:188012821
4-Chloroaniline ND ug/kg 10/19/23 08:35 106-47-810/18/23 14:188013141
bis(2-Chloroethoxy)methane ND ug/kg 10/19/23 08:35 111-91-110/18/23 14:184001661
bis(2-Chloroethyl) ether ND ug/kg 10/19/23 08:35 111-44-410/18/23 14:184001501
2-Chloronaphthalene ND ug/kg 10/19/23 08:35 91-58-710/18/23 14:184001591
2-Chlorophenol ND ug/kg 10/19/23 08:35 95-57-810/18/23 14:184001501
4-Chlorophenylphenyl ether ND ug/kg 10/19/23 08:35 7005-72-310/18/23 14:184001491
Chrysene ND ug/kg 10/19/23 08:35 218-01-910/18/23 14:184001461
Dibenz(a,h)anthracene ND ug/kg 10/19/23 08:35 53-70-310/18/23 14:184001541
Dibenzofuran ND ug/kg 10/19/23 08:35 132-64-910/18/23 14:184001441
1,2-Dichlorobenzene ND ug/kg 10/19/23 08:35 95-50-110/18/23 14:184001441
1,3-Dichlorobenzene ND ug/kg 10/19/23 08:35 541-73-110/18/23 14:184001421
1,4-Dichlorobenzene ND ug/kg 10/19/23 08:35 106-46-710/18/23 14:184001531
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Sample:CS-DUP-01 Lab ID:92693461002 Collected:10/16/23 11:30 Received:10/16/23 14:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 10/19/23 08:35 91-94-1 L210/18/23 14:188012711
2,4-Dichlorophenol ND ug/kg 10/19/23 08:35 120-83-210/18/23 14:184001571
Diethylphthalate ND ug/kg 10/19/23 08:35 84-66-210/18/23 14:184001471
2,4-Dimethylphenol ND ug/kg 10/19/23 08:35 105-67-910/18/23 14:184001661
Dimethylphthalate ND ug/kg 10/19/23 08:35 131-11-310/18/23 14:184001461
Di-n-butylphthalate ND ug/kg 10/19/23 08:35 84-74-210/18/23 14:184001351
4,6-Dinitro-2-methylphenol ND ug/kg 10/19/23 08:35 534-52-110/18/23 14:188013741
2,4-Dinitrophenol ND ug/kg 10/19/23 08:35 51-28-510/18/23 14:18200012401
2,4-Dinitrotoluene ND ug/kg 10/19/23 08:35 121-14-210/18/23 14:184001541
2,6-Dinitrotoluene ND ug/kg 10/19/23 08:35 606-20-210/18/23 14:184001471
Di-n-octylphthalate ND ug/kg 10/19/23 08:35 117-84-010/18/23 14:184001581
bis(2-Ethylhexyl)phthalate ND ug/kg 10/19/23 08:35 117-81-710/18/23 14:184001551
Fluoranthene ND ug/kg 10/19/23 08:35 206-44-010/18/23 14:184001371
Fluorene ND ug/kg 10/19/23 08:35 86-73-710/18/23 14:184001411
Hexachloro-1,3-butadiene ND ug/kg 10/19/23 08:35 87-68-310/18/23 14:184001741
Hexachlorobenzene ND ug/kg 10/19/23 08:35 118-74-110/18/23 14:184001571
Hexachlorocyclopentadiene ND ug/kg 10/19/23 08:35 77-47-410/18/23 14:184002291
Hexachloroethane ND ug/kg 10/19/23 08:35 67-72-110/18/23 14:184001531
Indeno(1,2,3-cd)pyrene ND ug/kg 10/19/23 08:35 193-39-510/18/23 14:184001581
Isophorone ND ug/kg 10/19/23 08:35 78-59-110/18/23 14:184001781
1-Methylnaphthalene ND ug/kg 10/19/23 08:35 90-12-010/18/23 14:184001411
2-Methylnaphthalene ND ug/kg 10/19/23 08:35 91-57-610/18/23 14:184001601
2-Methylphenol(o-Cresol)ND ug/kg 10/19/23 08:35 95-48-710/18/23 14:184001641
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/19/23 08:35 15831-10-410/18/23 14:184001611
Naphthalene ND ug/kg 10/19/23 08:35 91-20-310/18/23 14:184001361
2-Nitroaniline ND ug/kg 10/19/23 08:35 88-74-410/18/23 14:1820003281
3-Nitroaniline ND ug/kg 10/19/23 08:35 99-09-210/18/23 14:1820003141
4-Nitroaniline ND ug/kg 10/19/23 08:35 100-01-610/18/23 14:188013051
Nitrobenzene ND ug/kg 10/19/23 08:35 98-95-310/18/23 14:184001861
2-Nitrophenol ND ug/kg 10/19/23 08:35 88-75-510/18/23 14:184001741
4-Nitrophenol ND ug/kg 10/19/23 08:35 100-02-710/18/23 14:1820007741
N-Nitrosodimethylamine ND ug/kg 10/19/23 08:35 62-75-910/18/23 14:184001351
N-Nitroso-di-n-propylamine ND ug/kg 10/19/23 08:35 621-64-710/18/23 14:184001501
N-Nitrosodiphenylamine ND ug/kg 10/19/23 08:35 86-30-610/18/23 14:184001421
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/19/23 08:35 108-60-110/18/23 14:184001901
Pentachlorophenol ND ug/kg 10/19/23 08:35 87-86-510/18/23 14:188013921
Phenanthrene ND ug/kg 10/19/23 08:35 85-01-810/18/23 14:184001311
Phenol ND ug/kg 10/19/23 08:35 108-95-210/18/23 14:184001781
Pyrene ND ug/kg 10/19/23 08:35 129-00-010/18/23 14:184001631
Pyridine ND ug/kg 10/19/23 08:35 110-86-110/18/23 14:184001261
1,2,4-Trichlorobenzene ND ug/kg 10/19/23 08:35 120-82-110/18/23 14:184001581
2,4,5-Trichlorophenol ND ug/kg 10/19/23 08:35 95-95-410/18/23 14:184001831
2,4,6-Trichlorophenol ND ug/kg 10/19/23 08:35 88-06-210/18/23 14:184001651
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Sample:CS-DUP-01 Lab ID:92693461002 Collected:10/16/23 11:30 Received:10/16/23 14:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)46 %10/19/23 08:35 4165-60-010/18/23 14:1810-130 1
2-Fluorobiphenyl (S)50 %10/19/23 08:35 321-60-810/18/23 14:1810-130 1
Terphenyl-d14 (S)64 %10/19/23 08:35 1718-51-010/18/23 14:1810-130 1
Phenol-d6 (S)46 %10/19/23 08:35 13127-88-310/18/23 14:1810-130 1
2-Fluorophenol (S)42 %10/19/23 08:35 367-12-410/18/23 14:1810-130 1
2,4,6-Tribromophenol (S)72 %10/19/23 08:35 118-79-610/18/23 14:1810-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 10/17/23 03:25 67-64-110/16/23 18:2319562.7 1
Benzene 6.3J ug/kg 10/17/23 03:25 71-43-210/16/23 18:239.8 3.9 1
Bromobenzene ND ug/kg 10/17/23 03:25 108-86-110/16/23 18:239.8 3.2 1
Bromochloromethane ND ug/kg 10/17/23 03:25 74-97-510/16/23 18:239.8 2.9 1
Bromodichloromethane ND ug/kg 10/17/23 03:25 75-27-410/16/23 18:239.8 3.8 1
Bromoform ND ug/kg 10/17/23 03:25 75-25-210/16/23 18:239.8 3.4 1
Bromomethane ND ug/kg 10/17/23 03:25 74-83-910/16/23 18:2339.1 30.3 1
2-Butanone (MEK)ND ug/kg 10/17/23 03:25 78-93-310/16/23 18:2319546.9 1
n-Butylbenzene ND ug/kg 10/17/23 03:25 104-51-810/16/23 18:239.8 6.2 1
sec-Butylbenzene ND ug/kg 10/17/23 03:25 135-98-810/16/23 18:239.8 4.3 1
tert-Butylbenzene ND ug/kg 10/17/23 03:25 98-06-610/16/23 18:239.8 3.5 1
Carbon tetrachloride ND ug/kg 10/17/23 03:25 56-23-510/16/23 18:239.8 3.7 1
Chlorobenzene ND ug/kg 10/17/23 03:25 108-90-710/16/23 18:239.8 5.6 1
Chloroethane ND ug/kg 10/17/23 03:25 75-00-310/16/23 18:2319.5 7.5 1
Chloroform ND ug/kg 10/17/23 03:25 67-66-310/16/23 18:239.8 8.2 1
Chloromethane ND ug/kg 10/17/23 03:25 74-87-310/16/23 18:2319.5 8.2 1
2-Chlorotoluene ND ug/kg 10/17/23 03:25 95-49-810/16/23 18:239.8 3.5 1
4-Chlorotoluene ND ug/kg 10/17/23 03:25 106-43-410/16/23 18:239.8 5.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/17/23 03:25 96-12-810/16/23 18:239.8 3.8 1
Dibromochloromethane ND ug/kg 10/17/23 03:25 124-48-110/16/23 18:239.8 5.5 1
1,2-Dibromoethane (EDB)ND ug/kg 10/17/23 03:25 106-93-410/16/23 18:239.8 4.3 1
Dibromomethane ND ug/kg 10/17/23 03:25 74-95-310/16/23 18:239.8 2.1 1
1,2-Dichlorobenzene ND ug/kg 10/17/23 03:25 95-50-110/16/23 18:239.8 3.5 1
1,3-Dichlorobenzene ND ug/kg 10/17/23 03:25 541-73-110/16/23 18:239.8 3.0 1
1,4-Dichlorobenzene ND ug/kg 10/17/23 03:25 106-46-710/16/23 18:239.8 2.5 1
Dichlorodifluoromethane ND ug/kg 10/17/23 03:25 75-71-8 IH,v110/16/23 18:2319.5 9.9 1
1,1-Dichloroethane ND ug/kg 10/17/23 03:25 75-34-310/16/23 18:239.8 4.0 1
1,2-Dichloroethane ND ug/kg 10/17/23 03:25 107-06-210/16/23 18:239.8 6.5 1
1,1-Dichloroethene ND ug/kg 10/17/23 03:25 75-35-410/16/23 18:239.8 4.0 1
cis-1,2-Dichloroethene ND ug/kg 10/17/23 03:25 156-59-210/16/23 18:239.8 3.3 1
trans-1,2-Dichloroethene ND ug/kg 10/17/23 03:25 156-60-510/16/23 18:239.8 8.3 1
1,2-Dichloropropane ND ug/kg 10/17/23 03:25 78-87-510/16/23 18:239.8 2.9 1
1,3-Dichloropropane ND ug/kg 10/17/23 03:25 142-28-910/16/23 18:239.8 3.0 1
2,2-Dichloropropane ND ug/kg 10/17/23 03:25 594-20-710/16/23 18:239.8 7.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Sample:CS-DUP-01 Lab ID:92693461002 Collected:10/16/23 11:30 Received:10/16/23 14:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 10/17/23 03:25 563-58-610/16/23 18:239.8 4.7 1
cis-1,3-Dichloropropene ND ug/kg 10/17/23 03:25 10061-01-510/16/23 18:239.8 2.7 1
trans-1,3-Dichloropropene ND ug/kg 10/17/23 03:25 10061-02-610/16/23 18:239.8 3.4 1
Diisopropyl ether ND ug/kg 10/17/23 03:25 108-20-310/16/23 18:239.8 2.6 1
Ethylbenzene 8.3J ug/kg 10/17/23 03:25 100-41-410/16/23 18:239.8 4.6 1
Hexachloro-1,3-butadiene ND ug/kg 10/17/23 03:25 87-68-310/16/23 18:2319.5 16.0 1
2-Hexanone ND ug/kg 10/17/23 03:25 591-78-610/16/23 18:2397.7 9.4 1
Isopropylbenzene (Cumene)ND ug/kg 10/17/23 03:25 98-82-810/16/23 18:239.8 3.3 1
p-Isopropyltoluene ND ug/kg 10/17/23 03:25 99-87-610/16/23 18:239.8 4.8 1
Methylene Chloride ND ug/kg 10/17/23 03:25 75-09-210/16/23 18:2339.1 26.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/17/23 03:25 108-10-110/16/23 18:2397.7 9.4 1
Methyl-tert-butyl ether ND ug/kg 10/17/23 03:25 1634-04-410/16/23 18:239.8 3.7 1
Naphthalene ND ug/kg 10/17/23 03:25 91-20-310/16/23 18:239.8 5.1 1
n-Propylbenzene ND ug/kg 10/17/23 03:25 103-65-110/16/23 18:239.8 3.5 1
Styrene ND ug/kg 10/17/23 03:25 100-42-510/16/23 18:239.8 2.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/17/23 03:25 630-20-610/16/23 18:239.8 3.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/17/23 03:25 79-34-510/16/23 18:239.8 2.6 1
Tetrachloroethene ND ug/kg 10/17/23 03:25 127-18-410/16/23 18:239.8 3.1 1
Toluene 7.5J ug/kg 10/17/23 03:25 108-88-310/16/23 18:239.8 6.7 1
1,2,3-Trichlorobenzene ND ug/kg 10/17/23 03:25 87-61-610/16/23 18:239.8 7.9 1
1,2,4-Trichlorobenzene ND ug/kg 10/17/23 03:25 120-82-110/16/23 18:239.8 8.2 1
1,1,1-Trichloroethane ND ug/kg 10/17/23 03:25 71-55-610/16/23 18:239.8 5.1 1
1,1,2-Trichloroethane ND ug/kg 10/17/23 03:25 79-00-510/16/23 18:239.8 3.2 1
Trichloroethene ND ug/kg 10/17/23 03:25 79-01-610/16/23 18:239.8 7.9 1
Trichlorofluoromethane ND ug/kg 10/17/23 03:25 75-69-410/16/23 18:239.8 5.4 1
1,2,3-Trichloropropane ND ug/kg 10/17/23 03:25 96-18-410/16/23 18:239.8 4.9 1
1,2,4-Trimethylbenzene 6.4J ug/kg 10/17/23 03:25 95-63-610/16/23 18:239.8 5.8 1
1,3,5-Trimethylbenzene ND ug/kg 10/17/23 03:25 108-67-810/16/23 18:239.8 3.3 1
Vinyl acetate ND ug/kg 10/17/23 03:25 108-05-410/16/23 18:2397.7 20.1 1
Vinyl chloride ND ug/kg 10/17/23 03:25 75-01-410/16/23 18:2319.5 5.0 1
Xylene (Total)9.1J ug/kg 10/17/23 03:25 1330-20-710/16/23 18:2319.5 5.6 1
m&p-Xylene 9.1J ug/kg 10/17/23 03:25 179601-23-110/16/23 18:2319.5 6.7 1
o-Xylene ND ug/kg 10/17/23 03:25 95-47-610/16/23 18:239.8 4.3 1
Surrogates
Toluene-d8 (S)101 %10/17/23 03:25 2037-26-510/16/23 18:2370-130 1
4-Bromofluorobenzene (S)97 %10/17/23 03:25 460-00-410/16/23 18:2370-130 1
1,2-Dichloroethane-d4 (S)101 %10/17/23 03:25 17060-07-010/16/23 18:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.4 %10/17/23 17:44 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Sample:EB-01 Lab ID:92693461003 Collected:10/16/23 12:00 Received:10/16/23 14:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/17/23 07:56 67-64-125.0 5.1 1
Benzene ND ug/L 10/17/23 07:56 71-43-21.0 0.34 1
Bromobenzene ND ug/L 10/17/23 07:56 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 10/17/23 07:56 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/17/23 07:56 75-27-41.0 0.31 1
Bromoform ND ug/L 10/17/23 07:56 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/17/23 07:56 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/17/23 07:56 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 10/17/23 07:56 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/17/23 07:56 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/17/23 07:56 75-00-31.0 0.65 1
Chloroform ND ug/L 10/17/23 07:56 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/17/23 07:56 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/17/23 07:56 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 10/17/23 07:56 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/17/23 07:56 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/17/23 07:56 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/17/23 07:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/17/23 07:56 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/17/23 07:56 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 10/17/23 07:56 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/17/23 07:56 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 10/17/23 07:56 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/17/23 07:56 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/17/23 07:56 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/17/23 07:56 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/17/23 07:56 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/17/23 07:56 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/17/23 07:56 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 10/17/23 07:56 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 10/17/23 07:56 594-20-7 v21.0 0.39 1
1,1-Dichloropropene ND ug/L 10/17/23 07:56 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/17/23 07:56 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/17/23 07:56 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 10/17/23 07:56 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 10/17/23 07:56 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/17/23 07:56 87-68-32.0 1.5 1
2-Hexanone ND ug/L 10/17/23 07:56 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 10/17/23 07:56 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 10/17/23 07:56 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/17/23 07:56 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 10/17/23 07:56 1634-04-41.0 0.42 1
Naphthalene ND ug/L 10/17/23 07:56 91-20-31.0 0.64 1
Styrene ND ug/L 10/17/23 07:56 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/17/23 07:56 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Sample:EB-01 Lab ID:92693461003 Collected:10/16/23 12:00 Received:10/16/23 14:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 10/17/23 07:56 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/17/23 07:56 127-18-41.0 0.29 1
Toluene ND ug/L 10/17/23 07:56 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/17/23 07:56 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/17/23 07:56 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/17/23 07:56 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/17/23 07:56 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/17/23 07:56 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/17/23 07:56 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/17/23 07:56 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/17/23 07:56 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 10/17/23 07:56 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/17/23 07:56 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 10/17/23 07:56 179601-23-12.0 0.71 1
o-Xylene ND ug/L 10/17/23 07:56 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %10/17/23 07:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %10/17/23 07:56 17060-07-070-130 1
Toluene-d8 (S)100 %10/17/23 07:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
959027
EPA 7471
EPA 7471
7471 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92693461001, 92693461002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5274117
Associated Lab Samples:92693461001, 92693461002
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0092 10/19/23 12:510.0046
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5274118LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0950.091 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5274119MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35834641002
5274120
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.105 105 80-120103 2 200.1080.011 0.12 0.12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
959043
EPA 3050
EPA 6010
6010 MET Solid
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92693461001, 92693461002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5274141
Associated Lab Samples:92693461001, 92693461002
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 0.53 10/19/23 13:500.27
Barium mg/kg ND 0.53 10/19/23 13:500.089
Cadmium mg/kg ND 0.053 10/19/23 13:500.027
Chromium mg/kg ND 0.27 10/19/23 13:500.13
Lead mg/kg ND 0.53 10/19/23 13:500.27
Selenium mg/kg ND 0.80 10/19/23 13:500.40
Silver mg/kg ND 0.27 10/19/23 13:500.059
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5274142LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 13.314.1 95 80-120
Barium mg/kg 15.414.1 109 80-120
Cadmium mg/kg 1.41.4 102 80-120
Chromium mg/kg 14.914.1 106 80-120
Lead mg/kg 14.914.1 106 80-120
Selenium mg/kg 13.414.1 95 80-120
Silver mg/kg 1.41.4 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5274143MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35832720001
5274144
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 13.9 83 75-12583 6 2014.70.28U 11.5 12.2
Barium mg/kg M113.9 158 75-125135 7 2014.77.7 29.6 27.5
Cadmium mg/kg 1.4 97 75-12596 5 201.510.028U 1.4 1.4
Chromium mg/kg M113.9 128 75-125118 2 2014.74.7 22.5 22.1
Lead mg/kg 13.9 106 75-125105 3 2014.74.6 19.3 20.0
Selenium mg/kg 13.9 89 75-12588 5 2014.70.43U 12.4 13.0
Silver mg/kg 1.4 94 75-12592 4 201.510.062U 1.3 1.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
806725
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693461001, 92693461002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4177609
Associated Lab Samples:92693461001, 92693461002
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 10/16/23 22:141.9
1,1,1-Trichloroethane ug/kg ND 5.0 10/16/23 22:142.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 10/16/23 22:141.3
1,1,2-Trichloroethane ug/kg ND 5.0 10/16/23 22:141.7
1,1-Dichloroethane ug/kg ND 5.0 10/16/23 22:142.1
1,1-Dichloroethene ug/kg ND 5.0 10/16/23 22:142.1
1,1-Dichloropropene ug/kg ND 5.0 10/16/23 22:142.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 10/16/23 22:144.0
1,2,3-Trichloropropane ug/kg ND 5.0 10/16/23 22:142.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 10/16/23 22:144.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 10/16/23 22:143.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 10/16/23 22:141.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 10/16/23 22:142.2
1,2-Dichlorobenzene ug/kg ND 5.0 10/16/23 22:141.8
1,2-Dichloroethane ug/kg ND 5.0 10/16/23 22:143.3
1,2-Dichloropropane ug/kg ND 5.0 10/16/23 22:141.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 10/16/23 22:141.7
1,3-Dichlorobenzene ug/kg ND 5.0 10/16/23 22:141.6
1,3-Dichloropropane ug/kg ND 5.0 10/16/23 22:141.6
1,4-Dichlorobenzene ug/kg ND 5.0 10/16/23 22:141.3
2,2-Dichloropropane ug/kg ND 5.0 10/16/23 22:143.8
2-Butanone (MEK)ug/kg ND 100 10/16/23 22:1424.0
2-Chlorotoluene ug/kg ND 5.0 10/16/23 22:141.8
2-Hexanone ug/kg ND 50.0 10/16/23 22:144.8
4-Chlorotoluene ug/kg ND 5.0 10/16/23 22:142.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 10/16/23 22:144.8
Acetone ug/kg ND 100 10/16/23 22:1432.1
Benzene ug/kg ND 5.0 10/16/23 22:142.0
Bromobenzene ug/kg ND 5.0 10/16/23 22:141.6
Bromochloromethane ug/kg ND 5.0 10/16/23 22:141.5
Bromodichloromethane ug/kg ND 5.0 10/16/23 22:141.9
Bromoform ug/kg ND 5.0 10/16/23 22:141.8
Bromomethane ug/kg ND 20.0 10/16/23 22:1415.5
Carbon tetrachloride ug/kg ND 5.0 10/16/23 22:141.9
Chlorobenzene ug/kg ND 5.0 10/16/23 22:142.9
Chloroethane ug/kg ND 10.0 10/16/23 22:143.9
Chloroform ug/kg ND 5.0 10/16/23 22:144.2
Chloromethane ug/kg ND 10.0 10/16/23 22:144.2
cis-1,2-Dichloroethene ug/kg ND 5.0 10/16/23 22:141.7
cis-1,3-Dichloropropene ug/kg ND 5.0 10/16/23 22:141.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4177609
Associated Lab Samples:92693461001, 92693461002
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 10/16/23 22:142.8
Dibromomethane ug/kg ND 5.0 10/16/23 22:141.1
Dichlorodifluoromethane ug/kg ND 10.0 IH,v110/16/23 22:145.1
Diisopropyl ether ug/kg ND 5.0 10/16/23 22:141.4
Ethylbenzene ug/kg ND 5.0 10/16/23 22:142.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 10/16/23 22:148.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 10/16/23 22:141.7
m&p-Xylene ug/kg ND 10.0 10/16/23 22:143.4
Methyl-tert-butyl ether ug/kg ND 5.0 10/16/23 22:141.9
Methylene Chloride ug/kg ND 20.0 10/16/23 22:1413.7
n-Butylbenzene ug/kg ND 5.0 10/16/23 22:143.2
n-Propylbenzene ug/kg ND 5.0 10/16/23 22:141.8
Naphthalene ug/kg ND 5.0 10/16/23 22:142.6
o-Xylene ug/kg ND 5.0 10/16/23 22:142.2
p-Isopropyltoluene ug/kg ND 5.0 10/16/23 22:142.5
sec-Butylbenzene ug/kg ND 5.0 10/16/23 22:142.2
Styrene ug/kg ND 5.0 10/16/23 22:141.3
tert-Butylbenzene ug/kg ND 5.0 10/16/23 22:141.8
Tetrachloroethene ug/kg ND 5.0 10/16/23 22:141.6
Toluene ug/kg ND 5.0 10/16/23 22:143.4
trans-1,2-Dichloroethene ug/kg ND 5.0 10/16/23 22:144.2
trans-1,3-Dichloropropene ug/kg ND 5.0 10/16/23 22:141.7
Trichloroethene ug/kg ND 5.0 10/16/23 22:144.0
Trichlorofluoromethane ug/kg ND 5.0 10/16/23 22:142.8
Vinyl acetate ug/kg ND 50.0 10/16/23 22:1410.3
Vinyl chloride ug/kg ND 10.0 10/16/23 22:142.5
Xylene (Total)ug/kg ND 10.0 10/16/23 22:142.8
1,2-Dichloroethane-d4 (S)%103 70-130 10/16/23 22:14
4-Bromofluorobenzene (S)%96 70-130 10/16/23 22:14
Toluene-d8 (S)%100 70-130 10/16/23 22:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4177610LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 482500 96 70-130
1,1,1-Trichloroethane ug/kg 446500 89 70-130
1,1,2,2-Tetrachloroethane ug/kg 472500 94 70-130
1,1,2-Trichloroethane ug/kg 446500 89 70-130
1,1-Dichloroethane ug/kg 442500 88 70-130
1,1-Dichloroethene ug/kg 462500 92 70-132
1,1-Dichloropropene ug/kg 448500 90 70-130
1,2,3-Trichlorobenzene ug/kg 480500 96 62-136
1,2,3-Trichloropropane ug/kg 452500 90 70-130
1,2,4-Trichlorobenzene ug/kg 503500 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4177610LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 482500 96 70-130
1,2-Dibromo-3-chloropropane ug/kg 434500 87 65-130
1,2-Dibromoethane (EDB)ug/kg 442500 88 70-130
1,2-Dichlorobenzene ug/kg 493500 99 70-130
1,2-Dichloroethane ug/kg 422500 84 70-130
1,2-Dichloropropane ug/kg 454500 91 70-130
1,3,5-Trimethylbenzene ug/kg 478500 96 70-130
1,3-Dichlorobenzene ug/kg 472500 94 70-130
1,3-Dichloropropane ug/kg 453500 91 70-130
1,4-Dichlorobenzene ug/kg 476500 95 70-130
2,2-Dichloropropane ug/kg 427500 85 60-130
2-Butanone (MEK)ug/kg 8021000 80 66-130
2-Chlorotoluene ug/kg 492500 98 70-130
2-Hexanone ug/kg 9361000 94 68-130
4-Chlorotoluene ug/kg 475500 95 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 9141000 91 70-130
Acetone ug/kg 7371000 74 60-130
Benzene ug/kg 439500 88 70-130
Bromobenzene ug/kg 473500 95 70-130
Bromochloromethane ug/kg 441500 88 70-130
Bromodichloromethane ug/kg 440500 88 70-130
Bromoform ug/kg 444500 89 70-130
Bromomethane ug/kg 492500 98 43-175
Carbon tetrachloride ug/kg 446500 89 70-130
Chlorobenzene ug/kg 447500 89 70-130
Chloroethane ug/kg 454500 91 70-145
Chloroform ug/kg 433500 87 70-130
Chloromethane ug/kg 450500 90 66-146
cis-1,2-Dichloroethene ug/kg 429500 86 70-130
cis-1,3-Dichloropropene ug/kg 422500 84 70-130
Dibromochloromethane ug/kg 464500 93 70-130
Dibromomethane ug/kg 439500 88 70-130
Dichlorodifluoromethane ug/kg 478 IH,v15009642-197
Diisopropyl ether ug/kg 432500 86 68-130
Ethylbenzene ug/kg 422500 84 70-130
Hexachloro-1,3-butadiene ug/kg 488500 98 70-130
Isopropylbenzene (Cumene)ug/kg 466500 93 70-130
m&p-Xylene ug/kg 9251000 92 70-130
Methyl-tert-butyl ether ug/kg 411500 82 70-130
Methylene Chloride ug/kg 454500 91 65-130
n-Butylbenzene ug/kg 463500 93 70-130
n-Propylbenzene ug/kg 475500 95 70-130
Naphthalene ug/kg 489500 98 65-135
o-Xylene ug/kg 452500 90 70-130
p-Isopropyltoluene ug/kg 478500 96 70-130
sec-Butylbenzene ug/kg 472500 94 70-130
Styrene ug/kg 455500 91 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4177610LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 450500 90 70-130
Tetrachloroethene ug/kg 468500 94 70-130
Toluene ug/kg 435500 87 70-130
trans-1,2-Dichloroethene ug/kg 452500 90 70-130
trans-1,3-Dichloropropene ug/kg 408500 82 70-130
Trichloroethene ug/kg 440500 88 70-130
Trichlorofluoromethane ug/kg 410500 82 62-140
Vinyl acetate ug/kg 9631000 96 70-140
Vinyl chloride ug/kg 413500 83 70-152
Xylene (Total)ug/kg 13801500 92 70-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4177611MATRIX SPIKE SAMPLE:
MSSpike
Result
92693461001
1,1,1,2-Tetrachloroethane ug/kg 259874 30 22-166ND
1,1,1-Trichloroethane ug/kg 240874 27 23-172ND
1,1,2,2-Tetrachloroethane ug/kg 238874 27 21-158ND
1,1,2-Trichloroethane ug/kg 234874 27 25-160ND
1,1-Dichloroethane ug/kg 244874 28 22-166ND
1,1-Dichloroethene ug/kg 268874 31 18-183ND
1,1-Dichloropropene ug/kg 255874 29 20-181ND
1,2,3-Trichlorobenzene ug/kg 235874 27 10-161ND
1,2,3-Trichloropropane ug/kg 226874 26 21-147ND
1,2,4-Trichlorobenzene ug/kg 259874 30 10-159ND
1,2,4-Trimethylbenzene ug/kg 257874 29 17-170ND
1,2-Dibromo-3-chloropropane ug/kg 215874 25 10-135ND
1,2-Dibromoethane (EDB)ug/kg 237 M18742730-154ND
1,2-Dichlorobenzene ug/kg 273874 31 26-162ND
1,2-Dichloroethane ug/kg 236874 27 23-161ND
1,2-Dichloropropane ug/kg 247 M18742829-165ND
1,3,5-Trimethylbenzene ug/kg 258874 30 20-172ND
1,3-Dichlorobenzene ug/kg 253874 29 22-164ND
1,3-Dichloropropane ug/kg 252874 29 27-156ND
1,4-Dichlorobenzene ug/kg 252874 29 20-161ND
2,2-Dichloropropane ug/kg 214874 24 10-159ND
2-Butanone (MEK)ug/kg 4551740 26 13-143ND
2-Chlorotoluene ug/kg 265874 30 21-166ND
2-Hexanone ug/kg 4541740 26 19-145ND
4-Chlorotoluene ug/kg 250874 29 19-163ND
4-Methyl-2-pentanone (MIBK)ug/kg 4461740 26 21-151ND
Acetone ug/kg 3531740 19 10-133ND
Benzene ug/kg 246 M18742829-1564.9J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4177611MATRIX SPIKE SAMPLE:
MSSpike
Result
92693461001
Bromobenzene ug/kg 254874 29 25-161ND
Bromochloromethane ug/kg 253874 29 27-158ND
Bromodichloromethane ug/kg 222874 25 23-158ND
Bromoform ug/kg 212874 24 19-152ND
Bromomethane ug/kg 126874 14 10-152ND
Carbon tetrachloride ug/kg 232874 27 18-172ND
Chlorobenzene ug/kg 244874 28 26-166ND
Chloroethane ug/kg 142874 16 10-130ND
Chloroform ug/kg 243874 28 25-161ND
Chloromethane ug/kg 287874 33 27-197ND
cis-1,2-Dichloroethene ug/kg 239 M18742728-165ND
cis-1,3-Dichloropropene ug/kg 224874 26 23-159ND
Dibromochloromethane ug/kg 231874 26 21-151ND
Dibromomethane ug/kg 229 M18742638-158ND
Dichlorodifluoromethane ug/kg 319 IH,v18743610-200ND
Diisopropyl ether ug/kg 225874 26 23-160ND
Ethylbenzene ug/kg 232874 26 22-1634.5J
Hexachloro-1,3-butadiene ug/kg 260874 30 10-192ND
Isopropylbenzene (Cumene)ug/kg 259874 30 24-173ND
m&p-Xylene ug/kg 5031740 28 22-1717.3J
Methyl-tert-butyl ether ug/kg 210 M18742425-153ND
Methylene Chloride ug/kg 210874 24 10-165ND
n-Butylbenzene ug/kg 237874 27 10-186ND
n-Propylbenzene ug/kg 255874 29 16-171ND
Naphthalene ug/kg 257874 29 10-159ND
o-Xylene ug/kg 244874 28 23-171ND
p-Isopropyltoluene ug/kg 251874 29 13-184ND
sec-Butylbenzene ug/kg 256874 29 16-182ND
Styrene ug/kg 237874 27 25-169ND
tert-Butylbenzene ug/kg 245874 28 20-174ND
Tetrachloroethene ug/kg 227874 26 14-171ND
Toluene ug/kg 235874 25 24-16618.1
trans-1,2-Dichloroethene ug/kg 243874 28 24-170ND
trans-1,3-Dichloropropene ug/kg 200874 23 22-157ND
Trichloroethene ug/kg 235874 27 23-176ND
Trichlorofluoromethane ug/kg 163874 19 10-138ND
Vinyl acetate ug/kg 3031740 17 11-166ND
Vinyl chloride ug/kg 219874 25 21-200ND
Xylene (Total)ug/kg 7472630 28 23-1707.3J
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693461002
4177612SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg 6.3J 306.4J
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg 8.3J 306.3J
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND IH,v130ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg 8.2J 308.3J
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693461002
4177612SAMPLE DUPLICATE:
m&p-Xylene ug/kg 10.4J 309.1J
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg 8.7J 307.5J
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 309.1J
1,2-Dichloroethane-d4 (S)%101101
4-Bromofluorobenzene (S)%9897
Toluene-d8 (S)%100101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
806753
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693461003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4177801
Associated Lab Samples:92693461003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/17/23 07:210.31
1,1,1-Trichloroethane ug/L ND 1.0 10/17/23 07:210.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/17/23 07:210.22
1,1,2-Trichloroethane ug/L ND 1.0 10/17/23 07:210.32
1,1-Dichloroethane ug/L ND 1.0 10/17/23 07:210.37
1,1-Dichloroethene ug/L ND 1.0 10/17/23 07:210.35
1,1-Dichloropropene ug/L ND 1.0 10/17/23 07:210.43
1,2,3-Trichlorobenzene ug/L ND 1.0 10/17/23 07:210.81
1,2,3-Trichloropropane ug/L ND 1.0 10/17/23 07:210.26
1,2,4-Trichlorobenzene ug/L ND 1.0 10/17/23 07:210.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/17/23 07:210.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/17/23 07:210.27
1,2-Dichlorobenzene ug/L ND 1.0 10/17/23 07:210.34
1,2-Dichloroethane ug/L ND 1.0 10/17/23 07:210.32
1,2-Dichloropropane ug/L ND 1.0 10/17/23 07:210.36
1,3-Dichlorobenzene ug/L ND 1.0 10/17/23 07:210.34
1,3-Dichloropropane ug/L ND 1.0 10/17/23 07:210.28
1,4-Dichlorobenzene ug/L ND 1.0 10/17/23 07:210.33
2,2-Dichloropropane ug/L ND 1.0 v210/17/23 07:210.39
2-Butanone (MEK)ug/L ND 5.0 10/17/23 07:214.0
2-Chlorotoluene ug/L ND 1.0 10/17/23 07:210.32
2-Hexanone ug/L ND 5.0 10/17/23 07:210.48
4-Chlorotoluene ug/L ND 1.0 10/17/23 07:210.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/17/23 07:212.7
Acetone ug/L ND 25.0 10/17/23 07:215.1
Benzene ug/L ND 1.0 10/17/23 07:210.34
Bromobenzene ug/L ND 1.0 10/17/23 07:210.29
Bromochloromethane ug/L ND 1.0 10/17/23 07:210.47
Bromodichloromethane ug/L ND 1.0 10/17/23 07:210.31
Bromoform ug/L ND 1.0 10/17/23 07:210.34
Bromomethane ug/L ND 2.0 10/17/23 07:211.7
Carbon tetrachloride ug/L ND 1.0 10/17/23 07:210.33
Chlorobenzene ug/L ND 1.0 10/17/23 07:210.28
Chloroethane ug/L ND 1.0 10/17/23 07:210.65
Chloroform ug/L ND 1.0 10/17/23 07:210.43
Chloromethane ug/L ND 1.0 10/17/23 07:210.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/17/23 07:210.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/17/23 07:210.36
Dibromochloromethane ug/L ND 1.0 10/17/23 07:210.36
Dibromomethane ug/L ND 1.0 10/17/23 07:210.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4177801
Associated Lab Samples:92693461003
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 10/17/23 07:210.35
Diisopropyl ether ug/L ND 1.0 10/17/23 07:210.31
Ethylbenzene ug/L ND 1.0 10/17/23 07:210.30
Hexachloro-1,3-butadiene ug/L ND 2.0 10/17/23 07:211.5
m&p-Xylene ug/L ND 2.0 10/17/23 07:210.71
Methyl-tert-butyl ether ug/L ND 1.0 10/17/23 07:210.42
Methylene Chloride ug/L ND 5.0 10/17/23 07:212.0
Naphthalene ug/L ND 1.0 10/17/23 07:210.64
o-Xylene ug/L ND 1.0 10/17/23 07:210.34
p-Isopropyltoluene ug/L ND 1.0 10/17/23 07:210.41
Styrene ug/L ND 1.0 10/17/23 07:210.29
Tetrachloroethene ug/L ND 1.0 10/17/23 07:210.29
Toluene ug/L ND 1.0 10/17/23 07:210.24
trans-1,2-Dichloroethene ug/L ND 1.0 10/17/23 07:210.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/17/23 07:210.36
Trichloroethene ug/L ND 1.0 10/17/23 07:210.38
Trichlorofluoromethane ug/L ND 1.0 10/17/23 07:210.30
Vinyl acetate ug/L ND 2.0 10/17/23 07:211.3
Vinyl chloride ug/L ND 1.0 10/17/23 07:210.39
Xylene (Total)ug/L ND 1.0 10/17/23 07:210.34
1,2-Dichloroethane-d4 (S)%104 70-130 10/17/23 07:21
4-Bromofluorobenzene (S)%98 70-130 10/17/23 07:21
Toluene-d8 (S)%99 70-130 10/17/23 07:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4177802LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.520 102 70-130
1,1,1-Trichloroethane ug/L 19.120 95 70-130
1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130
1,1,2-Trichloroethane ug/L 19.620 98 70-130
1,1-Dichloroethane ug/L 20.220 101 70-130
1,1-Dichloroethene ug/L 22.120 110 69-131
1,1-Dichloropropene ug/L 20.320 102 70-132
1,2,3-Trichlorobenzene ug/L 18.320 91 70-132
1,2,3-Trichloropropane ug/L 19.520 98 70-130
1,2,4-Trichlorobenzene ug/L 18.320 91 70-130
1,2-Dibromo-3-chloropropane ug/L 17.820 89 70-130
1,2-Dibromoethane (EDB)ug/L 20.520 102 70-130
1,2-Dichlorobenzene ug/L 19.720 98 70-130
1,2-Dichloroethane ug/L 19.320 96 70-130
1,2-Dichloropropane ug/L 20.020 100 70-130
1,3-Dichlorobenzene ug/L 19.820 99 70-130
1,3-Dichloropropane ug/L 20.220 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4177802LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 19.420 97 70-130
2,2-Dichloropropane ug/L 14.9 v3207569-130
2-Butanone (MEK)ug/L 37.140 93 67-133
2-Chlorotoluene ug/L 20.620 103 70-130
2-Hexanone ug/L 39.640 99 70-133
4-Chlorotoluene ug/L 20.220 101 70-130
4-Methyl-2-pentanone (MIBK)ug/L 37.640 94 70-130
Acetone ug/L 38.840 97 67-130
Benzene ug/L 19.220 96 70-130
Bromobenzene ug/L 20.020 100 70-130
Bromochloromethane ug/L 20.020 100 70-130
Bromodichloromethane ug/L 18.720 94 70-130
Bromoform ug/L 18.220 91 70-133
Bromomethane ug/L 16.020 80 41-148
Carbon tetrachloride ug/L 19.820 99 70-130
Chlorobenzene ug/L 19.620 98 70-130
Chloroethane ug/L 21.320 107 41-157
Chloroform ug/L 19.320 96 70-130
Chloromethane ug/L 18.020 90 59-141
cis-1,2-Dichloroethene ug/L 19.920 99 70-130
cis-1,3-Dichloropropene ug/L 18.320 91 70-130
Dibromochloromethane ug/L 19.520 97 70-130
Dibromomethane ug/L 18.520 92 70-130
Dichlorodifluoromethane ug/L 25.420 127 54-147
Diisopropyl ether ug/L 18.220 91 70-130
Ethylbenzene ug/L 19.820 99 70-130
Hexachloro-1,3-butadiene ug/L 17.220 86 70-134
m&p-Xylene ug/L 38.940 97 70-130
Methyl-tert-butyl ether ug/L 17.620 88 70-130
Methylene Chloride ug/L 19.720 99 62-130
Naphthalene ug/L 19.720 98 70-135
o-Xylene ug/L 19.920 100 70-130
p-Isopropyltoluene ug/L 19.220 96 70-130
Styrene ug/L 19.820 99 70-130
Tetrachloroethene ug/L 18.820 94 70-130
Toluene ug/L 18.720 94 70-130
trans-1,2-Dichloroethene ug/L 20.720 103 70-130
trans-1,3-Dichloropropene ug/L 18.120 90 70-130
Trichloroethene ug/L 19.620 98 70-130
Trichlorofluoromethane ug/L 18.620 93 57-130
Vinyl acetate ug/L 38.040 95 70-141
Vinyl chloride ug/L 17.620 88 66-140
Xylene (Total)ug/L 58.860 98 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4177804MATRIX SPIKE SAMPLE:
MSSpike
Result
92693069003
1,1,1,2-Tetrachloroethane ug/L 23.320 116 70-146ND
1,1,1-Trichloroethane ug/L 22.220 111 70-150ND
1,1,2,2-Tetrachloroethane ug/L 22.620 113 66-144ND
1,1,2-Trichloroethane ug/L 22.820 114 70-142ND
1,1-Dichloroethane ug/L 23.120 116 68-150ND
1,1-Dichloroethene ug/L 24.220 121 64-162ND
1,1-Dichloropropene ug/L 23.620 118 70-160ND
1,2,3-Trichlorobenzene ug/L 20.320 102 66-151ND
1,2,3-Trichloropropane ug/L 22.220 111 66-144ND
1,2,4-Trichlorobenzene ug/L 20.720 103 69-147ND
1,2-Dibromo-3-chloropropane ug/L 20.320 101 62-146ND
1,2-Dibromoethane (EDB)ug/L 23.520 118 70-143ND
1,2-Dichlorobenzene ug/L 20.920 104 70-142ND
1,2-Dichloroethane ug/L 21.920 109 68-145ND
1,2-Dichloropropane ug/L 23.820 119 70-144ND
1,3-Dichlorobenzene ug/L 21.220 106 70-142ND
1,3-Dichloropropane ug/L 23.420 117 70-141ND
1,4-Dichlorobenzene ug/L 21.520 108 70-140ND
2,2-Dichloropropane ug/L 22.520 113 58-160ND
2-Butanone (MEK)ug/L 43.740 109 57-156ND
2-Chlorotoluene ug/L 22.320 112 70-148ND
2-Hexanone ug/L 45.640 114 62-153ND
4-Chlorotoluene ug/L 22.120 110 70-144ND
4-Methyl-2-pentanone (MIBK)ug/L 44.240 111 65-144ND
Acetone ug/L 61.940 119 49-162ND
Benzene ug/L 22.520 113 68-144ND
Bromobenzene ug/L 21.820 109 70-144ND
Bromochloromethane ug/L 22.320 111 70-148ND
Bromodichloromethane ug/L 21.420 107 70-141ND
Bromoform ug/L 20.020 100 59-144ND
Bromomethane ug/L 18.3 v3209223-190ND
Carbon tetrachloride ug/L 22.520 112 70-147ND
Chlorobenzene ug/L 21.720 109 70-143ND
Chloroethane ug/L 22.920 115 55-190ND
Chloroform ug/L 22.520 113 67-148ND
Chloromethane ug/L 19.620 98 38-180ND
cis-1,2-Dichloroethene ug/L 22.620 113 67-151ND
cis-1,3-Dichloropropene ug/L 21.920 110 70-142ND
Dibromochloromethane ug/L 21.920 109 68-140ND
Dibromomethane ug/L 21.820 109 70-142ND
Dichlorodifluoromethane ug/L 23.920 119 15-200ND
Diisopropyl ether ug/L 21.320 106 62-149ND
Ethylbenzene ug/L 21.820 109 70-145ND
Hexachloro-1,3-butadiene ug/L 21.420 107 64-164ND
m&p-Xylene ug/L 43.340 108 70-148ND
Methyl-tert-butyl ether ug/L 20.320 102 64-146ND
Methylene Chloride ug/L 22.620 113 54-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4177804MATRIX SPIKE SAMPLE:
MSSpike
Result
92693069003
Naphthalene ug/L 21.020 105 62-154ND
o-Xylene ug/L 21.620 108 70-145ND
p-Isopropyltoluene ug/L 21.720 109 70-153ND
Styrene ug/L 21.220 106 70-147ND
Tetrachloroethene ug/L 20.820 104 70-145ND
Toluene ug/L 24.120 91 65-1465.9
trans-1,2-Dichloroethene ug/L 24.320 121 69-155ND
trans-1,3-Dichloropropene ug/L 21.920 109 70-142ND
Trichloroethene ug/L 22.920 114 70-152ND
Trichlorofluoromethane ug/L 20.920 105 60-158ND
Vinyl acetate ug/L 44.740 112 56-157ND
Vinyl chloride ug/L 19.420 97 51-178ND
Xylene (Total)ug/L 65.060 108 70-146ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693069002
4177803SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693069002
4177803SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%103104
4-Bromofluorobenzene (S)%9897
Toluene-d8 (S)%10099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807491
EPA 7199
EPA 7199
7199 Chromium, Hexavalent
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693461001, 92693461002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4181263
Associated Lab Samples:92693461001, 92693461002
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg 0.14J 1.0 10/19/23 16:340.0010
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4181264LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.09.6 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4181265MATRIX SPIKE SAMPLE:
MSSpike
Result
92693294001
Chromium, Hexavalent mg/kg 0.46J M1982075-1250.80J
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4181266MATRIX SPIKE SAMPLE:
MSSpike
Result
92693851015
Chromium, Hexavalent mg/kg 0.030J M110.4 0 75-1250.040J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
806980
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693461001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4178822
Associated Lab Samples:92693461001
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 326 10/18/23 08:39128
1,2-Dichlorobenzene ug/kg ND 326 10/18/23 08:39117
1,3-Dichlorobenzene ug/kg ND 326 10/18/23 08:39115
1,4-Dichlorobenzene ug/kg ND 326 10/18/23 08:39124
1-Methylnaphthalene ug/kg ND 326 10/18/23 08:39114
2,2'-Oxybis(1-chloropropane)ug/kg ND 326 10/18/23 08:39155
2,4,5-Trichlorophenol ug/kg ND 326 10/18/23 08:39149
2,4,6-Trichlorophenol ug/kg ND 326 10/18/23 08:39134
2,4-Dichlorophenol ug/kg ND 326 10/18/23 08:39127
2,4-Dimethylphenol ug/kg ND 326 10/18/23 08:39135
2,4-Dinitrophenol ug/kg ND 1630 v110/18/23 08:391010
2,4-Dinitrotoluene ug/kg ND 326 10/18/23 08:39125
2,6-Dinitrotoluene ug/kg ND 326 10/18/23 08:39119
2-Chloronaphthalene ug/kg ND 326 10/18/23 08:39129
2-Chlorophenol ug/kg ND 326 10/18/23 08:39122
2-Methylnaphthalene ug/kg ND 326 10/18/23 08:39130
2-Methylphenol(o-Cresol)ug/kg ND 326 10/18/23 08:39133
2-Nitroaniline ug/kg ND 1630 10/18/23 08:39266
2-Nitrophenol ug/kg ND 326 10/18/23 08:39141
3&4-Methylphenol(m&p Cresol)ug/kg ND 326 10/18/23 08:39131
3,3'-Dichlorobenzidine ug/kg ND 651 10/18/23 08:39220
3-Nitroaniline ug/kg ND 1630 10/18/23 08:39256
4,6-Dinitro-2-methylphenol ug/kg ND 651 10/18/23 08:39304
4-Bromophenylphenyl ether ug/kg ND 326 10/18/23 08:39125
4-Chloro-3-methylphenol ug/kg ND 651 10/18/23 08:39229
4-Chloroaniline ug/kg ND 651 10/18/23 08:39256
4-Chlorophenylphenyl ether ug/kg ND 326 10/18/23 08:39121
4-Nitroaniline ug/kg ND 651 v110/18/23 08:39248
4-Nitrophenol ug/kg ND 1630 10/18/23 08:39630
Acenaphthene ug/kg ND 326 10/18/23 08:39114
Acenaphthylene ug/kg ND 326 10/18/23 08:39114
Aniline ug/kg ND 326 v110/18/23 08:39127
Anthracene ug/kg ND 326 10/18/23 08:39107
Benzo(a)anthracene ug/kg ND 326 10/18/23 08:39109
Benzo(a)pyrene ug/kg ND 326 10/18/23 08:39112
Benzo(b)fluoranthene ug/kg ND 326 10/18/23 08:39109
Benzo(g,h,i)perylene ug/kg ND 326 10/18/23 08:39126
Benzo(k)fluoranthene ug/kg ND 326 10/18/23 08:39114
Benzoic Acid ug/kg ND 1630 v110/18/23 08:39700
Benzyl alcohol ug/kg ND 651 10/18/23 08:39247
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4178822
Associated Lab Samples:92693461001
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 326 10/18/23 08:39135
bis(2-Chloroethyl) ether ug/kg ND 326 10/18/23 08:39122
bis(2-Ethylhexyl)phthalate ug/kg ND 326 10/18/23 08:39126
Butylbenzylphthalate ug/kg ND 326 10/18/23 08:39137
Chrysene ug/kg ND 326 10/18/23 08:39118
Di-n-butylphthalate ug/kg ND 326 10/18/23 08:39110
Di-n-octylphthalate ug/kg ND 326 10/18/23 08:39128
Dibenz(a,h)anthracene ug/kg ND 326 10/18/23 08:39125
Dibenzofuran ug/kg ND 326 10/18/23 08:39117
Diethylphthalate ug/kg ND 326 10/18/23 08:39119
Dimethylphthalate ug/kg ND 326 10/18/23 08:39118
Fluoranthene ug/kg ND 326 10/18/23 08:39112
Fluorene ug/kg ND 326 10/18/23 08:39114
Hexachloro-1,3-butadiene ug/kg ND 326 10/18/23 08:39141
Hexachlorobenzene ug/kg ND 326 10/18/23 08:39127
Hexachlorocyclopentadiene ug/kg ND 326 v210/18/23 08:39187
Hexachloroethane ug/kg ND 326 10/18/23 08:39124
Indeno(1,2,3-cd)pyrene ug/kg ND 326 10/18/23 08:39128
Isophorone ug/kg ND 326 10/18/23 08:39145
N-Nitroso-di-n-propylamine ug/kg ND 326 10/18/23 08:39122
N-Nitrosodimethylamine ug/kg ND 326 10/18/23 08:39110
N-Nitrosodiphenylamine ug/kg ND 326 10/18/23 08:39115
Naphthalene ug/kg ND 326 10/18/23 08:39111
Nitrobenzene ug/kg ND 326 10/18/23 08:39151
Pentachlorophenol ug/kg ND 651 10/18/23 08:39319
Phenanthrene ug/kg ND 326 10/18/23 08:39107
Phenol ug/kg ND 326 10/18/23 08:39145
Pyrene ug/kg ND 326 10/18/23 08:39132
Pyridine ug/kg ND 326 v110/18/23 08:39103
2,4,6-Tribromophenol (S)%56 10-130 10/18/23 08:39
2-Fluorobiphenyl (S)%52 10-130 10/18/23 08:39
2-Fluorophenol (S)%52 10-130 10/18/23 08:39
Nitrobenzene-d5 (S)%57 10-130 10/18/23 08:39
Phenol-d6 (S)%57 10-130 10/18/23 08:39
Terphenyl-d14 (S)%67 10-130 10/18/23 08:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4178823LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10201660 61 40-130
1,2-Dichlorobenzene ug/kg 10201660 62 37-130
1,3-Dichlorobenzene ug/kg 9811660 59 36-130
1,4-Dichlorobenzene ug/kg 9841660 59 36-130
1-Methylnaphthalene ug/kg 11001660 66 46-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4178823LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 9961660 60 12-130
2,4,5-Trichlorophenol ug/kg 11201660 68 49-130
2,4,6-Trichlorophenol ug/kg 11001660 66 48-130
2,4-Dichlorophenol ug/kg 10501660 63 45-130
2,4-Dimethylphenol ug/kg 10901660 66 45-130
2,4-Dinitrophenol ug/kg 6220 v183107523-130
2,4-Dinitrotoluene ug/kg 12301660 74 50-130
2,6-Dinitrotoluene ug/kg 11901660 72 53-130
2-Chloronaphthalene ug/kg 9961660 60 46-130
2-Chlorophenol ug/kg 11101660 67 39-130
2-Methylnaphthalene ug/kg 11101660 67 45-130
2-Methylphenol(o-Cresol)ug/kg 11301660 68 38-130
2-Nitroaniline ug/kg 22903320 69 43-130
2-Nitrophenol ug/kg 10601660 64 43-130
3&4-Methylphenol(m&p Cresol)ug/kg 11101660 67 34-130
3,3'-Dichlorobenzidine ug/kg 22503320 68 68-130
3-Nitroaniline ug/kg 23503320 71 36-130
4,6-Dinitro-2-methylphenol ug/kg 25903320 78 38-130
4-Bromophenylphenyl ether ug/kg 12401660 75 52-130
4-Chloro-3-methylphenol ug/kg 23203320 70 45-130
4-Chloroaniline ug/kg 22803320 69 41-130
4-Chlorophenylphenyl ether ug/kg 12401660 74 46-130
4-Nitroaniline ug/kg 2490 v133207540-130
4-Nitrophenol ug/kg 59208310 71 34-130
Acenaphthene ug/kg 11001660 66 47-130
Acenaphthylene ug/kg 11101660 67 50-130
Aniline ug/kg 1090 v116606633-130
Anthracene ug/kg 11801660 71 46-130
Benzo(a)anthracene ug/kg 12201660 73 49-130
Benzo(a)pyrene ug/kg 13001660 78 45-130
Benzo(b)fluoranthene ug/kg 13401660 81 45-130
Benzo(g,h,i)perylene ug/kg 10801660 65 44-130
Benzo(k)fluoranthene ug/kg 13301660 80 46-130
Benzoic Acid ug/kg 5390 v183106514-130
Benzyl alcohol ug/kg 21803320 66 39-130
bis(2-Chloroethoxy)methane ug/kg 10701660 65 41-130
bis(2-Chloroethyl) ether ug/kg 10401660 63 34-130
bis(2-Ethylhexyl)phthalate ug/kg 11501660 69 39-130
Butylbenzylphthalate ug/kg 11301660 68 48-130
Chrysene ug/kg 12301660 74 50-130
Di-n-butylphthalate ug/kg 12101660 73 46-130
Di-n-octylphthalate ug/kg 11301660 68 49-130
Dibenz(a,h)anthracene ug/kg 11801660 71 46-130
Dibenzofuran ug/kg 11201660 67 49-130
Diethylphthalate ug/kg 12301660 74 49-130
Dimethylphthalate ug/kg 12001660 72 50-130
Fluoranthene ug/kg 13001660 78 49-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4178823LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 12101660 73 47-130
Hexachloro-1,3-butadiene ug/kg 10601660 64 36-130
Hexachlorobenzene ug/kg 12101660 73 52-130
Hexachlorocyclopentadiene ug/kg 816 v316604910-130
Hexachloroethane ug/kg 9671660 58 36-130
Indeno(1,2,3-cd)pyrene ug/kg 11001660 66 44-130
Isophorone ug/kg 10801660 65 40-130
N-Nitroso-di-n-propylamine ug/kg 11301660 68 34-130
N-Nitrosodimethylamine ug/kg 9501660 57 29-130
N-Nitrosodiphenylamine ug/kg 11801660 71 47-130
Naphthalene ug/kg 10601660 64 43-130
Nitrobenzene ug/kg 9861660 59 41-130
Pentachlorophenol ug/kg 22003320 66 35-130
Phenanthrene ug/kg 12201660 74 50-130
Phenol ug/kg 11501660 69 39-130
Pyrene ug/kg 12101660 73 51-130
Pyridine ug/kg 868 v116605221-130
2,4,6-Tribromophenol (S)%77 10-130
2-Fluorobiphenyl (S)%62 10-130
2-Fluorophenol (S)%62 10-130
Nitrobenzene-d5 (S)%62 10-130
Phenol-d6 (S)%65 10-130
Terphenyl-d14 (S)%75 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4178824MATRIX SPIKE SAMPLE:
MSSpike
Result
92693214007
1,2,4-Trichlorobenzene ug/kg 6022080 29 22-130ND
1,2-Dichlorobenzene ug/kg 6742080 32 22-130ND
1,3-Dichlorobenzene ug/kg 6502080 31 22-130ND
1,4-Dichlorobenzene ug/kg 6622080 32 21-130ND
1-Methylnaphthalene ug/kg 6432080 31 27-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 6932080 33 10-130ND
2,4,5-Trichlorophenol ug/kg 8052080 39 18-130ND
2,4,6-Trichlorophenol ug/kg 7402080 36 17-130ND
2,4-Dichlorophenol ug/kg 6972080 34 19-130ND
2,4-Dimethylphenol ug/kg 7432080 36 17-130ND
2,4-Dinitrophenol ug/kg 6490 v1104006310-130ND
2,4-Dinitrotoluene ug/kg 11202080 54 31-130ND
2,6-Dinitrotoluene ug/kg 9962080 48 33-130ND
2-Chloronaphthalene ug/kg 6162080 30 26-130ND
2-Chlorophenol ug/kg 8242080 40 19-130ND
2-Methylnaphthalene ug/kg 6532080 31 26-130ND
2-Methylphenol(o-Cresol)ug/kg 8562080 41 19-130ND
2-Nitroaniline ug/kg 20604150 50 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4178824MATRIX SPIKE SAMPLE:
MSSpike
Result
92693214007
2-Nitrophenol ug/kg 7022080 34 16-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 8382080 40 14-130ND
3,3'-Dichlorobenzidine ug/kg 19604150 47 16-130ND
3-Nitroaniline ug/kg 24104150 58 28-130ND
4,6-Dinitro-2-methylphenol ug/kg 25804150 62 10-131ND
4-Bromophenylphenyl ether ug/kg 9192080 44 32-130ND
4-Chloro-3-methylphenol ug/kg 16304150 39 26-130ND
4-Chloroaniline ug/kg 15704150 38 19-130ND
4-Chlorophenylphenyl ether ug/kg 8602080 41 29-130ND
4-Nitroaniline ug/kg 2570 v141506222-130ND
4-Nitrophenol ug/kg 627010400 60 10-130ND
Acenaphthene ug/kg 6892080 33 29-130ND
Acenaphthylene ug/kg 6882080 33 27-130ND
Aniline ug/kg 757 v120803610-130ND
Anthracene ug/kg 9762080 47 26-130ND
Benzo(a)anthracene ug/kg 10402080 50 31-130ND
Benzo(a)pyrene ug/kg 10402080 50 24-130ND
Benzo(b)fluoranthene ug/kg 10602080 51 12-137ND
Benzo(g,h,i)perylene ug/kg 9272080 45 16-130ND
Benzo(k)fluoranthene ug/kg 11002080 53 27-130ND
Benzoic Acid ug/kg 3750 v1104003610-130ND
Benzyl alcohol ug/kg 16604150 40 25-130ND
bis(2-Chloroethoxy)methane ug/kg 7062080 34 26-130ND
bis(2-Chloroethyl) ether ug/kg 8422080 41 23-130ND
bis(2-Ethylhexyl)phthalate ug/kg 9942080 48 20-130ND
Butylbenzylphthalate ug/kg 9532080 46 28-130ND
Chrysene ug/kg 10502080 51 29-130ND
Di-n-butylphthalate ug/kg 10402080 50 29-130ND
Di-n-octylphthalate ug/kg 9972080 48 30-130ND
Dibenz(a,h)anthracene ug/kg 10002080 48 27-130ND
Dibenzofuran ug/kg 7282080 35 33-130ND
Diethylphthalate ug/kg 10702080 51 34-130ND
Dimethylphthalate ug/kg 10902080 52 35-130ND
Fluoranthene ug/kg 11002080 53 26-130ND
Fluorene ug/kg 8612080 41 27-130ND
Hexachloro-1,3-butadiene ug/kg 5902080 28 19-130ND
Hexachlorobenzene ug/kg 9312080 45 31-130ND
Hexachlorocyclopentadiene ug/kg 370J v320801810-130ND
Hexachloroethane ug/kg 6062080 29 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 9572080 46 16-130ND
Isophorone ug/kg 7402080 36 29-130ND
N-Nitroso-di-n-propylamine ug/kg 8402080 40 22-130ND
N-Nitrosodimethylamine ug/kg 7302080 35 15-130ND
N-Nitrosodiphenylamine ug/kg 9502080 46 30-130ND
Naphthalene ug/kg 6372080 31 24-130ND
Nitrobenzene ug/kg 6662080 32 25-130ND
Pentachlorophenol ug/kg 21604150 52 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4178824MATRIX SPIKE SAMPLE:
MSSpike
Result
92693214007
Phenanthrene ug/kg 9982080 48 28-130ND
Phenol ug/kg 8692080 42 18-130ND
Pyrene ug/kg 10102080 49 27-130ND
Pyridine ug/kg 553 v120802710-130ND
2,4,6-Tribromophenol (S)%31 10-130
2-Fluorobiphenyl (S)%17 10-130
2-Fluorophenol (S)%31 10-130
Nitrobenzene-d5 (S)%26 10-130
Phenol-d6 (S)%34 10-130
Terphenyl-d14 (S)%32 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693214010
4178825SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND v130ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND v130ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693214010
4178825SAMPLE DUPLICATE:
Aniline ug/kg ND v130ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND v130ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND v230ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND v130ND
2,4,6-Tribromophenol (S)%6665
2-Fluorobiphenyl (S)%5249
2-Fluorophenol (S)%6156
Nitrobenzene-d5 (S)%6358
Phenol-d6 (S)%6762
Terphenyl-d14 (S)%5553
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807174
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693461002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4179587
Associated Lab Samples:92693461002
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 326 10/19/23 08:03128
1,2-Dichlorobenzene ug/kg ND 326 10/19/23 08:03117
1,3-Dichlorobenzene ug/kg ND 326 10/19/23 08:03115
1,4-Dichlorobenzene ug/kg ND 326 10/19/23 08:03124
1-Methylnaphthalene ug/kg ND 326 10/19/23 08:03114
2,2'-Oxybis(1-chloropropane)ug/kg ND 326 10/19/23 08:03155
2,4,5-Trichlorophenol ug/kg ND 326 10/19/23 08:03149
2,4,6-Trichlorophenol ug/kg ND 326 10/19/23 08:03134
2,4-Dichlorophenol ug/kg ND 326 10/19/23 08:03127
2,4-Dimethylphenol ug/kg ND 326 10/19/23 08:03135
2,4-Dinitrophenol ug/kg ND 1630 10/19/23 08:031010
2,4-Dinitrotoluene ug/kg ND 326 10/19/23 08:03125
2,6-Dinitrotoluene ug/kg ND 326 10/19/23 08:03119
2-Chloronaphthalene ug/kg ND 326 10/19/23 08:03129
2-Chlorophenol ug/kg ND 326 10/19/23 08:03122
2-Methylnaphthalene ug/kg ND 326 10/19/23 08:03130
2-Methylphenol(o-Cresol)ug/kg ND 326 10/19/23 08:03133
2-Nitroaniline ug/kg ND 1630 10/19/23 08:03266
2-Nitrophenol ug/kg ND 326 10/19/23 08:03141
3&4-Methylphenol(m&p Cresol)ug/kg ND 326 10/19/23 08:03131
3,3'-Dichlorobenzidine ug/kg ND 651 10/19/23 08:03220
3-Nitroaniline ug/kg ND 1630 10/19/23 08:03256
4,6-Dinitro-2-methylphenol ug/kg ND 651 10/19/23 08:03304
4-Bromophenylphenyl ether ug/kg ND 326 10/19/23 08:03125
4-Chloro-3-methylphenol ug/kg ND 651 10/19/23 08:03229
4-Chloroaniline ug/kg ND 651 10/19/23 08:03256
4-Chlorophenylphenyl ether ug/kg ND 326 10/19/23 08:03121
4-Nitroaniline ug/kg ND 651 10/19/23 08:03248
4-Nitrophenol ug/kg ND 1630 10/19/23 08:03630
Acenaphthene ug/kg ND 326 10/19/23 08:03114
Acenaphthylene ug/kg ND 326 10/19/23 08:03114
Aniline ug/kg ND 326 10/19/23 08:03127
Anthracene ug/kg ND 326 10/19/23 08:03107
Benzo(a)anthracene ug/kg ND 326 10/19/23 08:03109
Benzo(a)pyrene ug/kg ND 326 10/19/23 08:03112
Benzo(b)fluoranthene ug/kg ND 326 10/19/23 08:03109
Benzo(g,h,i)perylene ug/kg ND 326 10/19/23 08:03126
Benzo(k)fluoranthene ug/kg ND 326 10/19/23 08:03114
Benzoic Acid ug/kg ND 1630 10/19/23 08:03700
Benzyl alcohol ug/kg ND 651 10/19/23 08:03247
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4179587
Associated Lab Samples:92693461002
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 326 10/19/23 08:03135
bis(2-Chloroethyl) ether ug/kg ND 326 10/19/23 08:03122
bis(2-Ethylhexyl)phthalate ug/kg ND 326 10/19/23 08:03126
Butylbenzylphthalate ug/kg ND 326 10/19/23 08:03137
Chrysene ug/kg ND 326 10/19/23 08:03118
Di-n-butylphthalate ug/kg ND 326 10/19/23 08:03110
Di-n-octylphthalate ug/kg ND 326 10/19/23 08:03128
Dibenz(a,h)anthracene ug/kg ND 326 10/19/23 08:03125
Dibenzofuran ug/kg ND 326 10/19/23 08:03117
Diethylphthalate ug/kg ND 326 10/19/23 08:03119
Dimethylphthalate ug/kg ND 326 10/19/23 08:03118
Fluoranthene ug/kg ND 326 10/19/23 08:03112
Fluorene ug/kg ND 326 10/19/23 08:03114
Hexachloro-1,3-butadiene ug/kg ND 326 10/19/23 08:03141
Hexachlorobenzene ug/kg ND 326 10/19/23 08:03127
Hexachlorocyclopentadiene ug/kg ND 326 10/19/23 08:03187
Hexachloroethane ug/kg ND 326 10/19/23 08:03124
Indeno(1,2,3-cd)pyrene ug/kg ND 326 10/19/23 08:03128
Isophorone ug/kg ND 326 10/19/23 08:03145
N-Nitroso-di-n-propylamine ug/kg ND 326 10/19/23 08:03122
N-Nitrosodimethylamine ug/kg ND 326 10/19/23 08:03110
N-Nitrosodiphenylamine ug/kg ND 326 10/19/23 08:03115
Naphthalene ug/kg ND 326 10/19/23 08:03111
Nitrobenzene ug/kg ND 326 10/19/23 08:03151
Pentachlorophenol ug/kg ND 651 10/19/23 08:03319
Phenanthrene ug/kg ND 326 10/19/23 08:03107
Phenol ug/kg ND 326 10/19/23 08:03145
Pyrene ug/kg ND 326 10/19/23 08:03132
Pyridine ug/kg ND 326 10/19/23 08:03103
2,4,6-Tribromophenol (S)%47 10-130 10/19/23 08:03
2-Fluorobiphenyl (S)%49 10-130 10/19/23 08:03
2-Fluorophenol (S)%52 10-130 10/19/23 08:03
Nitrobenzene-d5 (S)%52 10-130 10/19/23 08:03
Phenol-d6 (S)%54 10-130 10/19/23 08:03
Terphenyl-d14 (S)%63 10-130 10/19/23 08:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4179588LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 8091640 49 40-130
1,2-Dichlorobenzene ug/kg 8221640 50 37-130
1,3-Dichlorobenzene ug/kg 7971640 49 36-130
1,4-Dichlorobenzene ug/kg 8081640 49 36-130
1-Methylnaphthalene ug/kg 8981640 55 46-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4179588LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 8121640 50 12-130
2,4,5-Trichlorophenol ug/kg 10401640 63 49-130
2,4,6-Trichlorophenol ug/kg 9751640 59 48-130
2,4-Dichlorophenol ug/kg 8891640 54 45-130
2,4-Dimethylphenol ug/kg 9011640 55 45-130
2,4-Dinitrophenol ug/kg 55608200 68 23-130
2,4-Dinitrotoluene ug/kg 11401640 70 50-130
2,6-Dinitrotoluene ug/kg 11201640 68 53-130
2-Chloronaphthalene ug/kg 8651640 53 46-130
2-Chlorophenol ug/kg 9071640 55 39-130
2-Methylnaphthalene ug/kg 8951640 55 45-130
2-Methylphenol(o-Cresol)ug/kg 9251640 56 38-130
2-Nitroaniline ug/kg 21603280 66 43-130
2-Nitrophenol ug/kg 8741640 53 43-130
3&4-Methylphenol(m&p Cresol)ug/kg 9581640 58 34-130
3,3'-Dichlorobenzidine ug/kg 2040 L232806268-130
3-Nitroaniline ug/kg 23503280 72 36-130
4,6-Dinitro-2-methylphenol ug/kg 23603280 72 38-130
4-Bromophenylphenyl ether ug/kg 10701640 65 52-130
4-Chloro-3-methylphenol ug/kg 20803280 64 45-130
4-Chloroaniline ug/kg 19803280 60 41-130
4-Chlorophenylphenyl ether ug/kg 10801640 66 46-130
4-Nitroaniline ug/kg 24903280 76 40-130
4-Nitrophenol ug/kg 59508200 73 34-130
Acenaphthene ug/kg 10001640 61 47-130
Acenaphthylene ug/kg 9951640 61 50-130
Aniline ug/kg 9121640 56 33-130
Anthracene ug/kg 12001640 73 46-130
Benzo(a)anthracene ug/kg 11101640 67 49-130
Benzo(a)pyrene ug/kg 11801640 72 45-130
Benzo(b)fluoranthene ug/kg 12301640 75 45-130
Benzo(g,h,i)perylene ug/kg 9841640 60 44-130
Benzo(k)fluoranthene ug/kg 12101640 74 46-130
Benzoic Acid ug/kg 48008200 59 14-130
Benzyl alcohol ug/kg 18503280 56 39-130
bis(2-Chloroethoxy)methane ug/kg 8971640 55 41-130
bis(2-Chloroethyl) ether ug/kg 9001640 55 34-130
bis(2-Ethylhexyl)phthalate ug/kg 13201640 81 39-130
Butylbenzylphthalate ug/kg 11501640 70 48-130
Chrysene ug/kg 12901640 78 50-130
Di-n-butylphthalate ug/kg 12401640 76 46-130
Di-n-octylphthalate ug/kg 12301640 75 49-130
Dibenz(a,h)anthracene ug/kg 10901640 66 46-130
Dibenzofuran ug/kg 10101640 62 49-130
Diethylphthalate ug/kg 11301640 69 49-130
Dimethylphthalate ug/kg 11201640 68 50-130
Fluoranthene ug/kg 11801640 72 49-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4179588LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 11101640 68 47-130
Hexachloro-1,3-butadiene ug/kg 8121640 50 36-130
Hexachlorobenzene ug/kg 10201640 62 52-130
Hexachlorocyclopentadiene ug/kg 6751640 41 10-130
Hexachloroethane ug/kg 7631640 47 36-130
Indeno(1,2,3-cd)pyrene ug/kg 10301640 63 44-130
Isophorone ug/kg 9651640 59 40-130
N-Nitroso-di-n-propylamine ug/kg 10301640 63 34-130
N-Nitrosodimethylamine ug/kg 8161640 50 29-130
N-Nitrosodiphenylamine ug/kg 11601640 71 47-130
Naphthalene ug/kg 8521640 52 43-130
Nitrobenzene ug/kg 8121640 50 41-130
Pentachlorophenol ug/kg 20803280 63 35-130
Phenanthrene ug/kg 12001640 73 50-130
Phenol ug/kg 10101640 62 39-130
Pyrene ug/kg 11001640 67 51-130
Pyridine ug/kg 7661640 47 21-130
2,4,6-Tribromophenol (S)%65 10-130
2-Fluorobiphenyl (S)%51 10-130
2-Fluorophenol (S)%53 10-130
Nitrobenzene-d5 (S)%50 10-130
Phenol-d6 (S)%55 10-130
Terphenyl-d14 (S)%62 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4179589MATRIX SPIKE SAMPLE:
MSSpike
Result
92693690001
1,2,4-Trichlorobenzene ug/kg 7132340 30 22-130ND
1,2-Dichlorobenzene ug/kg 7502340 32 22-130ND
1,3-Dichlorobenzene ug/kg 7362340 31 22-130ND
1,4-Dichlorobenzene ug/kg 7392340 31 21-130ND
1-Methylnaphthalene ug/kg 7232340 31 27-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 7332340 31 10-130ND
2,4,5-Trichlorophenol ug/kg 8922340 38 18-130ND
2,4,6-Trichlorophenol ug/kg 8542340 36 17-130ND
2,4-Dichlorophenol ug/kg 7072340 30 19-130ND
2,4-Dimethylphenol ug/kg 7192340 31 17-130ND
2,4-Dinitrophenol ug/kg 349011700 30 10-130ND
2,4-Dinitrotoluene ug/kg 9792340 42 31-130ND
2,6-Dinitrotoluene ug/kg 9842340 42 33-130ND
2-Chloronaphthalene ug/kg 7752340 33 26-130ND
2-Chlorophenol ug/kg 7822340 33 19-130ND
2-Methylnaphthalene ug/kg 7252340 31 26-130ND
2-Methylphenol(o-Cresol)ug/kg 7462340 32 19-130ND
2-Nitroaniline ug/kg 1950J4700 42 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4179589MATRIX SPIKE SAMPLE:
MSSpike
Result
92693690001
2-Nitrophenol ug/kg 7362340 31 16-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 7432340 32 14-130ND
3,3'-Dichlorobenzidine ug/kg 19004700 40 16-130ND
3-Nitroaniline ug/kg 1990J4700 42 28-130ND
4,6-Dinitro-2-methylphenol ug/kg 21004700 45 10-131ND
4-Bromophenylphenyl ether ug/kg 10202340 44 32-130ND
4-Chloro-3-methylphenol ug/kg 15104700 32 26-130ND
4-Chloroaniline ug/kg 15904700 34 19-130ND
4-Chlorophenylphenyl ether ug/kg 9152340 39 29-130ND
4-Nitroaniline ug/kg 19004700 40 22-130ND
4-Nitrophenol ug/kg 428011700 36 10-130ND
Acenaphthene ug/kg 8352340 36 29-130ND
Acenaphthylene ug/kg 8432340 36 27-130ND
Aniline ug/kg 7942340 34 10-130ND
Anthracene ug/kg 9792340 42 26-130ND
Benzo(a)anthracene ug/kg 10302340 44 31-130ND
Benzo(a)pyrene ug/kg 10602340 45 24-130ND
Benzo(b)fluoranthene ug/kg 10402340 44 12-137ND
Benzo(g,h,i)perylene ug/kg 10902340 46 16-130ND
Benzo(k)fluoranthene ug/kg 10402340 44 27-130ND
Benzoic Acid ug/kg ND M1,v111700610-130ND
Benzyl alcohol ug/kg 15304700 33 25-130ND
bis(2-Chloroethoxy)methane ug/kg 7362340 31 26-130ND
bis(2-Chloroethyl) ether ug/kg 7562340 32 23-130ND
bis(2-Ethylhexyl)phthalate ug/kg 8962340 38 20-130ND
Butylbenzylphthalate ug/kg 9382340 40 28-130ND
Chrysene ug/kg 10602340 45 29-130ND
Di-n-butylphthalate ug/kg 9442340 40 29-130ND
Di-n-octylphthalate ug/kg 9122340 39 30-130ND
Dibenz(a,h)anthracene ug/kg 10202340 44 27-130ND
Dibenzofuran ug/kg 8602340 37 33-130ND
Diethylphthalate ug/kg 9842340 42 34-130ND
Dimethylphthalate ug/kg 10302340 44 35-130ND
Fluoranthene ug/kg 9292340 40 26-130ND
Fluorene ug/kg 9072340 39 27-130ND
Hexachloro-1,3-butadiene ug/kg 7152340 30 19-130ND
Hexachlorobenzene ug/kg 10102340 43 31-130ND
Hexachlorocyclopentadiene ug/kg 301J2340 13 10-130ND
Hexachloroethane ug/kg 6692340 28 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 10502340 45 16-130ND
Isophorone ug/kg 7552340 32 29-130ND
N-Nitroso-di-n-propylamine ug/kg 7792340 33 22-130ND
N-Nitrosodimethylamine ug/kg 7622340 32 15-130ND
N-Nitrosodiphenylamine ug/kg 10402340 44 30-130ND
Naphthalene ug/kg 7312340 31 24-130ND
Nitrobenzene ug/kg 7192340 31 25-130ND
Pentachlorophenol ug/kg 19504700 41 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4179589MATRIX SPIKE SAMPLE:
MSSpike
Result
92693690001
Phenanthrene ug/kg 10202340 44 28-130ND
Phenol ug/kg 7952340 34 18-130ND
Pyrene ug/kg 11002340 47 27-130ND
Pyridine ug/kg 7282340 31 10-130ND
2,4,6-Tribromophenol (S)%47 10-130
2-Fluorobiphenyl (S)%32 10-130
2-Fluorophenol (S)%32 10-130
Nitrobenzene-d5 (S)%32 10-130
Phenol-d6 (S)%32 10-130
Terphenyl-d14 (S)%46 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693690002
4179590SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693690002
4179590SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND v130ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6039
2-Fluorobiphenyl (S)%4531
2-Fluorophenol (S)%5535
Nitrobenzene-d5 (S)%5738
Phenol-d6 (S)%5535
Terphenyl-d14 (S)%4137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807072
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693461001, 92693461002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693333001
4179152SAMPLE DUPLICATE:
Percent Moisture %19.0 N252520.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693497005
4179153SAMPLE DUPLICATE:
Percent Moisture %20.7 N2212516.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 50
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in theassociated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 50
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92693461
BROADSTONE WEST END - 71227190
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92693461001 807491 807640CS-01 EPA 7199 EPA 7199
92693461002 807491 807640CS-DUP-01 EPA 7199 EPA 7199
92693461001 959043 959185CS-01 EPA 3050 EPA 6010
92693461002 959043 959185CS-DUP-01 EPA 3050 EPA 6010
92693461001 959027 959334CS-01 EPA 7471 EPA 7471
92693461002 959027 959334CS-DUP-01 EPA 7471 EPA 7471
92693461001 806980 807143CS-01 EPA 3546 EPA 8270E
92693461002 807174 807482CS-DUP-01 EPA 3546 EPA 8270E
92693461001 806725 806785CS-01 EPA 5035A/5030B EPA 8260D
92693461002 806725 806785CS-DUP-01 EPA 5035A/5030B EPA 8260D
92693461003 806753EB-01 EPA 8260D
92693461001 807072CS-01 SW-846
92693461002 807072CS-DUP-01 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2023 05:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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#=CL#
November 20, 2023
LIMS USE: FR - WILL FRAZIER
LIMS OBJECT ID: 92697661
92697661
Project:
Pace Project No.:
RE:
Will Frazier
Terracon
2701 Westport Rd
Charlotte, NC 28208
71227190
Dear Will Frazier:
Enclosed are the analytical results for sample(s) received by the laboratory on November 08, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
704-977-0943
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 61
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92697661
71227190
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 61
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92697661
71227190
Lab ID Sample ID Matrix Date Collected Date Received
92697661001 CS-02 Solid 11/07/23 16:20 11/08/23 10:05
92697661002 CS-03 Solid 11/07/23 16:50 11/08/23 10:05
92697661003 CS-04 Solid 11/07/23 17:15 11/08/23 10:05
92697661004 CS-05 Solid 11/07/23 17:30 11/08/23 10:05
92697661005 CS-DUP-02 Solid 11/07/23 16:25 11/08/23 10:05
92697661006 EB-02 Water 11/07/23 17:40 11/08/23 15:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 61
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92697661
71227190
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92697661001 CS-02 EPA 7199 1 PASI-CICO
EPA 6010D 7 PASI-ASBW
EPA 7471B 1 PASI-ABM
EPA 8270E 75 PASI-CPKS
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92697661002 CS-03 EPA 7199 1 PASI-CICO
EPA 6010D 7 PASI-ASBW
EPA 7471B 1 PASI-ABM
EPA 8270E 75 PASI-CPKS
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92697661003 CS-04 EPA 7199 1 PASI-CICO
EPA 6010D 7 PASI-ASBW
EPA 7471B 1 PASI-ABM
EPA 8270E 75 PASI-CPKS
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92697661004 CS-05 EPA 7199 1 PASI-CICO
EPA 6010D 7 PASI-ASBW
EPA 7471B 1 PASI-ABM
EPA 8270E 75 PASI-CPKS
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92697661005 CS-DUP-02 EPA 7199 1 PASI-CICO
EPA 6010D 7 PASI-ASBW
EPA 7471B 1 PASI-ABM
EPA 8270E 75 PASI-CPKS
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92697661006 EB-02 EPA 8260D 63 PASI-CLMB
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-02 Lab ID:92697661001 Collected:11/07/23 16:20 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.071J mg/kg 11/09/23 19:32 18540-29-9 B11/09/23 10:471.2 0.0012 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 2.6 mg/kg 11/15/23 12:54 7440-38-211/14/23 15:442.1 0.35 1
Barium 75.8 mg/kg 11/15/23 12:54 7440-39-311/14/23 15:440.86 0.097 1
Cadmium 0.35 mg/kg 11/15/23 12:54 7440-43-911/14/23 15:440.086 0.022 1
Chromium 42.3 mg/kg 11/15/23 12:54 7440-47-311/14/23 15:440.43 0.064 1
Lead 28.0 mg/kg 11/15/23 12:54 7439-92-111/14/23 15:440.86 0.22 1
Selenium ND mg/kg 11/16/23 15:09 7782-49-211/14/23 15:444.3 3.3 5
Silver ND mg/kg 11/15/23 12:54 7440-22-411/14/23 15:440.43 0.040 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.060 mg/kg 11/15/23 14:48 7439-97-611/14/23 12:410.0071 0.0044 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 11/12/23 17:35 83-32-911/11/23 12:1220007025
Acenaphthylene ND ug/kg 11/12/23 17:35 208-96-811/11/23 12:1220007025
Aniline ND ug/kg 11/12/23 17:35 62-53-311/11/23 12:1220007805
Anthracene ND ug/kg 11/12/23 17:35 120-12-711/11/23 12:1220006535
Benzo(a)anthracene ND ug/kg 11/12/23 17:35 56-55-311/11/23 12:1220006655
Benzo(a)pyrene ND ug/kg 11/12/23 17:35 50-32-811/11/23 12:1220006905
Benzo(b)fluoranthene ND ug/kg 11/12/23 17:35 205-99-211/11/23 12:1220006655
Benzo(g,h,i)perylene ND ug/kg 11/12/23 17:35 191-24-211/11/23 12:1220007745
Benzo(k)fluoranthene ND ug/kg 11/12/23 17:35 207-08-911/11/23 12:1220007025
Benzoic Acid ND ug/kg 11/12/23 17:35 65-85-011/11/23 12:12998042905
Benzyl alcohol ND ug/kg 11/12/23 17:35 100-51-611/11/23 12:12399015105
4-Bromophenylphenyl ether ND ug/kg 11/12/23 17:35 101-55-311/11/23 12:1220007685
Butylbenzylphthalate ND ug/kg 11/12/23 17:35 85-68-711/11/23 12:1220008415
4-Chloro-3-methylphenol ND ug/kg 11/12/23 17:35 59-50-711/11/23 12:12399014005
4-Chloroaniline ND ug/kg 11/12/23 17:35 106-47-811/11/23 12:12399015705
bis(2-Chloroethoxy)methane ND ug/kg 11/12/23 17:35 111-91-111/11/23 12:1220008295
bis(2-Chloroethyl) ether ND ug/kg 11/12/23 17:35 111-44-411/11/23 12:1220007505
2-Chloronaphthalene ND ug/kg 11/12/23 17:35 91-58-711/11/23 12:1220007925
2-Chlorophenol ND ug/kg 11/12/23 17:35 95-57-811/11/23 12:1220007505
4-Chlorophenylphenyl ether ND ug/kg 11/12/23 17:35 7005-72-311/11/23 12:1220007445
Chrysene ND ug/kg 11/12/23 17:35 218-01-911/11/23 12:1220007265
Dibenz(a,h)anthracene ND ug/kg 11/12/23 17:35 53-70-311/11/23 12:1220007685
Dibenzofuran ND ug/kg 11/12/23 17:35 132-64-911/11/23 12:1220007205
1,2-Dichlorobenzene ND ug/kg 11/12/23 17:35 95-50-111/11/23 12:1220007205
1,3-Dichlorobenzene ND ug/kg 11/12/23 17:35 541-73-111/11/23 12:1220007085
1,4-Dichlorobenzene ND ug/kg 11/12/23 17:35 106-46-711/11/23 12:1220007625
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-02 Lab ID:92697661001 Collected:11/07/23 16:20 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 11/12/23 17:35 91-94-1 L211/11/23 12:12399013505
2,4-Dichlorophenol ND ug/kg 11/12/23 17:35 120-83-211/11/23 12:1220007805
Diethylphthalate ND ug/kg 11/12/23 17:35 84-66-211/11/23 12:1220007325
2,4-Dimethylphenol ND ug/kg 11/12/23 17:35 105-67-911/11/23 12:1220008295
Dimethylphthalate ND ug/kg 11/12/23 17:35 131-11-311/11/23 12:1220007265
Di-n-butylphthalate ND ug/kg 11/12/23 17:35 84-74-211/11/23 12:1220006715
4,6-Dinitro-2-methylphenol ND ug/kg 11/12/23 17:35 534-52-111/11/23 12:12399018605
2,4-Dinitrophenol ND ug/kg 11/12/23 17:35 51-28-511/11/23 12:12998061705
2,4-Dinitrotoluene ND ug/kg 11/12/23 17:35 121-14-211/11/23 12:1220007685
2,6-Dinitrotoluene ND ug/kg 11/12/23 17:35 606-20-211/11/23 12:1220007325
Di-n-octylphthalate ND ug/kg 11/12/23 17:35 117-84-011/11/23 12:1220007865
bis(2-Ethylhexyl)phthalate ND ug/kg 11/12/23 17:35 117-81-711/11/23 12:1220007745
Fluoranthene ND ug/kg 11/12/23 17:35 206-44-011/11/23 12:1220006845
Fluorene ND ug/kg 11/12/23 17:35 86-73-711/11/23 12:1220007025
Hexachloro-1,3-butadiene ND ug/kg 11/12/23 17:35 87-68-311/11/23 12:1220008655
Hexachlorobenzene ND ug/kg 11/12/23 17:35 118-74-111/11/23 12:1220007805
Hexachlorocyclopentadiene ND ug/kg 11/12/23 17:35 77-47-411/11/23 12:12200011405
Hexachloroethane ND ug/kg 11/12/23 17:35 67-72-111/11/23 12:1220007625
Indeno(1,2,3-cd)pyrene ND ug/kg 11/12/23 17:35 193-39-511/11/23 12:1220007865
Isophorone ND ug/kg 11/12/23 17:35 78-59-111/11/23 12:1220008895
1-Methylnaphthalene ND ug/kg 11/12/23 17:35 90-12-011/11/23 12:1220007025
2-Methylnaphthalene ND ug/kg 11/12/23 17:35 91-57-611/11/23 12:1220007985
2-Methylphenol(o-Cresol)ND ug/kg 11/12/23 17:35 95-48-711/11/23 12:1220008175
3&4-Methylphenol(m&p Cresol)ND ug/kg 11/12/23 17:35 15831-10-411/11/23 12:1220008055
Naphthalene ND ug/kg 11/12/23 17:35 91-20-311/11/23 12:1220006775
2-Nitroaniline ND ug/kg 11/12/23 17:35 88-74-411/11/23 12:12998016305
3-Nitroaniline ND ug/kg 11/12/23 17:35 99-09-211/11/23 12:12998015705
4-Nitroaniline ND ug/kg 11/12/23 17:35 100-01-611/11/23 12:12399015205
Nitrobenzene ND ug/kg 11/12/23 17:35 98-95-311/11/23 12:1220009255
2-Nitrophenol ND ug/kg 11/12/23 17:35 88-75-511/11/23 12:1220008655
4-Nitrophenol ND ug/kg 11/12/23 17:35 100-02-711/11/23 12:12998038605
N-Nitrosodimethylamine ND ug/kg 11/12/23 17:35 62-75-911/11/23 12:1220006715
N-Nitroso-di-n-propylamine ND ug/kg 11/12/23 17:35 621-64-711/11/23 12:1220007505
N-Nitrosodiphenylamine ND ug/kg 11/12/23 17:35 86-30-611/11/23 12:1220007085
2,2'-Oxybis(1-chloropropane)ND ug/kg 11/12/23 17:35 108-60-111/11/23 12:1220009505
Pentachlorophenol ND ug/kg 11/12/23 17:35 87-86-511/11/23 12:12399019505
Phenanthrene ND ug/kg 11/12/23 17:35 85-01-811/11/23 12:1220006535
Phenol ND ug/kg 11/12/23 17:35 108-95-211/11/23 12:1220008895
Pyrene ND ug/kg 11/12/23 17:35 129-00-011/11/23 12:1220008115
Pyridine ND ug/kg 11/12/23 17:35 110-86-111/11/23 12:1220006295
1,2,4-Trichlorobenzene ND ug/kg 11/12/23 17:35 120-82-111/11/23 12:1220007865
2,4,5-Trichlorophenol ND ug/kg 11/12/23 17:35 95-95-411/11/23 12:1220009135
2,4,6-Trichlorophenol ND ug/kg 11/12/23 17:35 88-06-211/11/23 12:1220008235
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-02 Lab ID:92697661001 Collected:11/07/23 16:20 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)62 %11/12/23 17:35 4165-60-0 D311/11/23 12:1210-130 5
2-Fluorobiphenyl (S)52 %11/12/23 17:35 321-60-811/11/23 12:1210-130 5
Terphenyl-d14 (S)63 %11/12/23 17:35 1718-51-011/11/23 12:1210-130 5
Phenol-d6 (S)50 %11/12/23 17:35 13127-88-311/11/23 12:1210-130 5
2-Fluorophenol (S)45 %11/12/23 17:35 367-12-411/11/23 12:1210-130 5
2,4,6-Tribromophenol (S)52 %11/12/23 17:35 118-79-611/11/23 12:1210-130 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 11/11/23 10:09 67-64-111/10/23 16:0015148.4 1
Benzene ND ug/kg 11/11/23 10:09 71-43-211/10/23 16:007.5 3.0 1
Bromobenzene ND ug/kg 11/11/23 10:09 108-86-111/10/23 16:007.5 2.5 1
Bromochloromethane ND ug/kg 11/11/23 10:09 74-97-511/10/23 16:007.5 2.2 1
Bromodichloromethane ND ug/kg 11/11/23 10:09 75-27-411/10/23 16:007.5 2.9 1
Bromoform ND ug/kg 11/11/23 10:09 75-25-211/10/23 16:007.5 2.7 1
Bromomethane ND ug/kg 11/11/23 10:09 74-83-911/10/23 16:0030.2 23.4 1
2-Butanone (MEK)ND ug/kg 11/11/23 10:09 78-93-311/10/23 16:0015136.2 1
n-Butylbenzene ND ug/kg 11/11/23 10:09 104-51-811/10/23 16:007.5 4.8 1
sec-Butylbenzene ND ug/kg 11/11/23 10:09 135-98-811/10/23 16:007.5 3.3 1
tert-Butylbenzene ND ug/kg 11/11/23 10:09 98-06-611/10/23 16:007.5 2.7 1
Carbon tetrachloride ND ug/kg 11/11/23 10:09 56-23-511/10/23 16:007.5 2.8 1
Chlorobenzene ND ug/kg 11/11/23 10:09 108-90-711/10/23 16:007.5 4.3 1
Chloroethane ND ug/kg 11/11/23 10:09 75-00-311/10/23 16:0015.1 5.8 1
Chloroform ND ug/kg 11/11/23 10:09 67-66-311/10/23 16:007.5 6.3 1
Chloromethane ND ug/kg 11/11/23 10:09 74-87-311/10/23 16:0015.1 6.3 1
2-Chlorotoluene ND ug/kg 11/11/23 10:09 95-49-811/10/23 16:007.5 2.7 1
4-Chlorotoluene ND ug/kg 11/11/23 10:09 106-43-411/10/23 16:007.5 4.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/11/23 10:09 96-12-811/10/23 16:007.5 2.9 1
Dibromochloromethane ND ug/kg 11/11/23 10:09 124-48-111/10/23 16:007.5 4.2 1
1,2-Dibromoethane (EDB)ND ug/kg 11/11/23 10:09 106-93-411/10/23 16:007.5 3.3 1
Dibromomethane ND ug/kg 11/11/23 10:09 74-95-311/10/23 16:007.5 1.6 1
1,2-Dichlorobenzene ND ug/kg 11/11/23 10:09 95-50-111/10/23 16:007.5 2.7 1
1,3-Dichlorobenzene ND ug/kg 11/11/23 10:09 541-73-111/10/23 16:007.5 2.3 1
1,4-Dichlorobenzene ND ug/kg 11/11/23 10:09 106-46-711/10/23 16:007.5 2.0 1
Dichlorodifluoromethane ND ug/kg 11/11/23 10:09 75-71-811/10/23 16:0015.1 7.7 1
1,1-Dichloroethane ND ug/kg 11/11/23 10:09 75-34-311/10/23 16:007.5 3.1 1
1,2-Dichloroethane ND ug/kg 11/11/23 10:09 107-06-211/10/23 16:007.5 5.0 1
1,1-Dichloroethene ND ug/kg 11/11/23 10:09 75-35-411/10/23 16:007.5 3.1 1
cis-1,2-Dichloroethene ND ug/kg 11/11/23 10:09 156-59-211/10/23 16:007.5 2.6 1
trans-1,2-Dichloroethene ND ug/kg 11/11/23 10:09 156-60-511/10/23 16:007.5 6.4 1
1,2-Dichloropropane ND ug/kg 11/11/23 10:09 78-87-511/10/23 16:007.5 2.3 1
1,3-Dichloropropane ND ug/kg 11/11/23 10:09 142-28-911/10/23 16:007.5 2.4 1
2,2-Dichloropropane ND ug/kg 11/11/23 10:09 594-20-711/10/23 16:007.5 5.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-02 Lab ID:92697661001 Collected:11/07/23 16:20 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 11/11/23 10:09 563-58-611/10/23 16:007.5 3.6 1
cis-1,3-Dichloropropene ND ug/kg 11/11/23 10:09 10061-01-511/10/23 16:007.5 2.1 1
trans-1,3-Dichloropropene ND ug/kg 11/11/23 10:09 10061-02-611/10/23 16:007.5 2.6 1
Diisopropyl ether ND ug/kg 11/11/23 10:09 108-20-311/10/23 16:007.5 2.0 1
Ethylbenzene 5.5J ug/kg 11/11/23 10:09 100-41-411/10/23 16:007.5 3.5 1
Hexachloro-1,3-butadiene ND ug/kg 11/11/23 10:09 87-68-311/10/23 16:0015.1 12.3 1
2-Hexanone ND ug/kg 11/11/23 10:09 591-78-611/10/23 16:0075.4 7.3 1
Isopropylbenzene (Cumene)ND ug/kg 11/11/23 10:09 98-82-811/10/23 16:007.5 2.6 1
p-Isopropyltoluene 9.4 ug/kg 11/11/23 10:09 99-87-611/10/23 16:007.5 3.7 1
Methylene Chloride ND ug/kg 11/11/23 10:09 75-09-211/10/23 16:0030.2 20.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/11/23 10:09 108-10-111/10/23 16:0075.4 7.3 1
Methyl-tert-butyl ether ND ug/kg 11/11/23 10:09 1634-04-411/10/23 16:007.5 2.8 1
Naphthalene 9.0 ug/kg 11/11/23 10:09 91-20-311/10/23 16:007.5 4.0 1
n-Propylbenzene ND ug/kg 11/11/23 10:09 103-65-111/10/23 16:007.5 2.7 1
Styrene ND ug/kg 11/11/23 10:09 100-42-511/10/23 16:007.5 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/11/23 10:09 630-20-611/10/23 16:007.5 2.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/11/23 10:09 79-34-511/10/23 16:007.5 2.0 1
Tetrachloroethene ND ug/kg 11/11/23 10:09 127-18-411/10/23 16:007.5 2.4 1
Toluene 11.3 ug/kg 11/11/23 10:09 108-88-311/10/23 16:007.5 5.2 1
1,2,3-Trichlorobenzene ND ug/kg 11/11/23 10:09 87-61-611/10/23 16:007.5 6.1 1
1,2,4-Trichlorobenzene ND ug/kg 11/11/23 10:09 120-82-111/10/23 16:007.5 6.3 1
1,1,1-Trichloroethane ND ug/kg 11/11/23 10:09 71-55-611/10/23 16:007.5 3.9 1
1,1,2-Trichloroethane ND ug/kg 11/11/23 10:09 79-00-511/10/23 16:007.5 2.5 1
Trichloroethene ND ug/kg 11/11/23 10:09 79-01-611/10/23 16:007.5 6.1 1
Trichlorofluoromethane ND ug/kg 11/11/23 10:09 75-69-411/10/23 16:007.5 4.1 1
1,2,3-Trichloropropane ND ug/kg 11/11/23 10:09 96-18-411/10/23 16:007.5 3.8 1
1,2,4-Trimethylbenzene 4.5J ug/kg 11/11/23 10:09 95-63-611/10/23 16:007.5 4.5 1
1,3,5-Trimethylbenzene ND ug/kg 11/11/23 10:09 108-67-811/10/23 16:007.5 2.5 1
Vinyl acetate ND ug/kg 11/11/23 10:09 108-05-411/10/23 16:0075.4 15.5 1
Vinyl chloride ND ug/kg 11/11/23 10:09 75-01-411/10/23 16:0015.1 3.8 1
Xylene (Total)17.4 ug/kg 11/11/23 10:09 1330-20-711/10/23 16:0015.1 4.3 1
m&p-Xylene 11.5J ug/kg 11/11/23 10:09 179601-23-111/10/23 16:0015.1 5.2 1
o-Xylene 5.9J ug/kg 11/11/23 10:09 95-47-611/10/23 16:007.5 3.3 1
Surrogates
Toluene-d8 (S)98 %11/11/23 10:09 2037-26-511/10/23 16:0070-130 1
4-Bromofluorobenzene (S)96 %11/11/23 10:09 460-00-411/10/23 16:0070-130 1
1,2-Dichloroethane-d4 (S)86 %11/11/23 10:09 17060-07-011/10/23 16:0070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.7 %11/09/23 13:49 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-03 Lab ID:92697661002 Collected:11/07/23 16:50 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.10J mg/kg 11/09/23 19:49 18540-29-9 B,M111/09/23 10:471.2 0.0012 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 2.6J mg/kg 11/15/23 12:56 7440-38-211/14/23 15:443.0 0.50 1
Barium 135 mg/kg 11/15/23 12:56 7440-39-3 M111/14/23 15:441.2 0.14 1
Cadmium 0.26 mg/kg 11/15/23 12:56 7440-43-911/14/23 15:440.12 0.032 1
Chromium 37.1 mg/kg 11/15/23 12:56 7440-47-311/14/23 15:440.61 0.091 1
Lead 16.1 mg/kg 11/15/23 12:56 7439-92-111/14/23 15:441.2 0.32 1
Selenium ND mg/kg 11/16/23 15:11 7782-49-211/14/23 15:446.1 4.7 5
Silver ND mg/kg 11/15/23 12:56 7440-22-411/14/23 15:440.61 0.057 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury ND mg/kg 11/15/23 14:50 7439-97-611/14/23 12:410.0071 0.0044 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 11/12/23 18:00 83-32-911/11/23 12:1220307125
Acenaphthylene ND ug/kg 11/12/23 18:00 208-96-811/11/23 12:1220307125
Aniline ND ug/kg 11/12/23 18:00 62-53-311/11/23 12:1220307925
Anthracene ND ug/kg 11/12/23 18:00 120-12-711/11/23 12:1220306635
Benzo(a)anthracene ND ug/kg 11/12/23 18:00 56-55-311/11/23 12:1220306755
Benzo(a)pyrene ND ug/kg 11/12/23 18:00 50-32-811/11/23 12:1220307005
Benzo(b)fluoranthene ND ug/kg 11/12/23 18:00 205-99-211/11/23 12:1220306755
Benzo(g,h,i)perylene ND ug/kg 11/12/23 18:00 191-24-211/11/23 12:1220307865
Benzo(k)fluoranthene ND ug/kg 11/12/23 18:00 207-08-911/11/23 12:1220307125
Benzoic Acid ND ug/kg 11/12/23 18:00 65-85-0 M111/11/23 12:121010043505
Benzyl alcohol ND ug/kg 11/12/23 18:00 100-51-611/11/23 12:12405015305
4-Bromophenylphenyl ether ND ug/kg 11/12/23 18:00 101-55-311/11/23 12:1220307805
Butylbenzylphthalate ND ug/kg 11/12/23 18:00 85-68-711/11/23 12:1220308535
4-Chloro-3-methylphenol ND ug/kg 11/12/23 18:00 59-50-711/11/23 12:12405014205
4-Chloroaniline ND ug/kg 11/12/23 18:00 106-47-811/11/23 12:12405015905
bis(2-Chloroethoxy)methane ND ug/kg 11/12/23 18:00 111-91-111/11/23 12:1220308415
bis(2-Chloroethyl) ether ND ug/kg 11/12/23 18:00 111-44-411/11/23 12:1220307615
2-Chloronaphthalene ND ug/kg 11/12/23 18:00 91-58-711/11/23 12:1220308045
2-Chlorophenol ND ug/kg 11/12/23 18:00 95-57-811/11/23 12:1220307615
4-Chlorophenylphenyl ether ND ug/kg 11/12/23 18:00 7005-72-311/11/23 12:1220307555
Chrysene ND ug/kg 11/12/23 18:00 218-01-911/11/23 12:1220307375
Dibenz(a,h)anthracene ND ug/kg 11/12/23 18:00 53-70-311/11/23 12:1220307805
Dibenzofuran ND ug/kg 11/12/23 18:00 132-64-911/11/23 12:1220307305
1,2-Dichlorobenzene ND ug/kg 11/12/23 18:00 95-50-111/11/23 12:1220307305
1,3-Dichlorobenzene ND ug/kg 11/12/23 18:00 541-73-111/11/23 12:1220307185
1,4-Dichlorobenzene ND ug/kg 11/12/23 18:00 106-46-711/11/23 12:1220307735
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-03 Lab ID:92697661002 Collected:11/07/23 16:50 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 11/12/23 18:00 91-94-1 L211/11/23 12:12405013705
2,4-Dichlorophenol ND ug/kg 11/12/23 18:00 120-83-211/11/23 12:1220307925
Diethylphthalate ND ug/kg 11/12/23 18:00 84-66-211/11/23 12:1220307435
2,4-Dimethylphenol ND ug/kg 11/12/23 18:00 105-67-911/11/23 12:1220308415
Dimethylphthalate ND ug/kg 11/12/23 18:00 131-11-311/11/23 12:1220307375
Di-n-butylphthalate ND ug/kg 11/12/23 18:00 84-74-211/11/23 12:1220306815
4,6-Dinitro-2-methylphenol ND ug/kg 11/12/23 18:00 534-52-111/11/23 12:12405018905
2,4-Dinitrophenol ND ug/kg 11/12/23 18:00 51-28-511/11/23 12:121010062605
2,4-Dinitrotoluene ND ug/kg 11/12/23 18:00 121-14-211/11/23 12:1220307805
2,6-Dinitrotoluene ND ug/kg 11/12/23 18:00 606-20-211/11/23 12:1220307435
Di-n-octylphthalate ND ug/kg 11/12/23 18:00 117-84-011/11/23 12:1220307985
bis(2-Ethylhexyl)phthalate ND ug/kg 11/12/23 18:00 117-81-711/11/23 12:1220307865
Fluoranthene ND ug/kg 11/12/23 18:00 206-44-011/11/23 12:1220306945
Fluorene ND ug/kg 11/12/23 18:00 86-73-711/11/23 12:1220307125
Hexachloro-1,3-butadiene ND ug/kg 11/12/23 18:00 87-68-311/11/23 12:1220308785
Hexachlorobenzene ND ug/kg 11/12/23 18:00 118-74-111/11/23 12:1220307925
Hexachlorocyclopentadiene ND ug/kg 11/12/23 18:00 77-47-411/11/23 12:12203011605
Hexachloroethane ND ug/kg 11/12/23 18:00 67-72-111/11/23 12:1220307735
Indeno(1,2,3-cd)pyrene ND ug/kg 11/12/23 18:00 193-39-511/11/23 12:1220307985
Isophorone ND ug/kg 11/12/23 18:00 78-59-111/11/23 12:1220309025
1-Methylnaphthalene ND ug/kg 11/12/23 18:00 90-12-011/11/23 12:1220307125
2-Methylnaphthalene ND ug/kg 11/12/23 18:00 91-57-611/11/23 12:1220308105
2-Methylphenol(o-Cresol)ND ug/kg 11/12/23 18:00 95-48-711/11/23 12:1220308295
3&4-Methylphenol(m&p Cresol)ND ug/kg 11/12/23 18:00 15831-10-411/11/23 12:1220308165
Naphthalene ND ug/kg 11/12/23 18:00 91-20-311/11/23 12:1220306885
2-Nitroaniline ND ug/kg 11/12/23 18:00 88-74-411/11/23 12:121010016605
3-Nitroaniline ND ug/kg 11/12/23 18:00 99-09-211/11/23 12:121010015905
4-Nitroaniline ND ug/kg 11/12/23 18:00 100-01-611/11/23 12:12405015405
Nitrobenzene ND ug/kg 11/12/23 18:00 98-95-311/11/23 12:1220309395
2-Nitrophenol ND ug/kg 11/12/23 18:00 88-75-511/11/23 12:1220308785
4-Nitrophenol ND ug/kg 11/12/23 18:00 100-02-711/11/23 12:121010039205
N-Nitrosodimethylamine ND ug/kg 11/12/23 18:00 62-75-911/11/23 12:1220306815
N-Nitroso-di-n-propylamine ND ug/kg 11/12/23 18:00 621-64-711/11/23 12:1220307615
N-Nitrosodiphenylamine ND ug/kg 11/12/23 18:00 86-30-611/11/23 12:1220307185
2,2'-Oxybis(1-chloropropane)ND ug/kg 11/12/23 18:00 108-60-111/11/23 12:1220309645
Pentachlorophenol ND ug/kg 11/12/23 18:00 87-86-511/11/23 12:12405019805
Phenanthrene ND ug/kg 11/12/23 18:00 85-01-811/11/23 12:1220306635
Phenol ND ug/kg 11/12/23 18:00 108-95-211/11/23 12:1220309025
Pyrene ND ug/kg 11/12/23 18:00 129-00-011/11/23 12:1220308235
Pyridine ND ug/kg 11/12/23 18:00 110-86-111/11/23 12:1220306385
1,2,4-Trichlorobenzene ND ug/kg 11/12/23 18:00 120-82-111/11/23 12:1220307985
2,4,5-Trichlorophenol ND ug/kg 11/12/23 18:00 95-95-411/11/23 12:1220309275
2,4,6-Trichlorophenol ND ug/kg 11/12/23 18:00 88-06-211/11/23 12:1220308355
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-03 Lab ID:92697661002 Collected:11/07/23 16:50 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)58 %11/12/23 18:00 4165-60-0 D311/11/23 12:1210-130 5
2-Fluorobiphenyl (S)51 %11/12/23 18:00 321-60-811/11/23 12:1210-130 5
Terphenyl-d14 (S)60 %11/12/23 18:00 1718-51-011/11/23 12:1210-130 5
Phenol-d6 (S)48 %11/12/23 18:00 13127-88-311/11/23 12:1210-130 5
2-Fluorophenol (S)43 %11/12/23 18:00 367-12-411/11/23 12:1210-130 5
2,4,6-Tribromophenol (S)45 %11/12/23 18:00 118-79-611/11/23 12:1210-130 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 11/10/23 08:16 67-64-1 R1,v2,
v311/09/23 22:5719562.6 1
Benzene ND ug/kg 11/10/23 08:16 71-43-211/09/23 22:579.7 3.9 1
Bromobenzene ND ug/kg 11/10/23 08:16 108-86-111/09/23 22:579.7 3.2 1
Bromochloromethane ND ug/kg 11/10/23 08:16 74-97-511/09/23 22:579.7 2.9 1
Bromodichloromethane ND ug/kg 11/10/23 08:16 75-27-411/09/23 22:579.7 3.8 1
Bromoform ND ug/kg 11/10/23 08:16 75-25-211/09/23 22:579.7 3.4 1
Bromomethane ND ug/kg 11/10/23 08:16 74-83-9 IK11/09/23 22:5739.0 30.2 1
2-Butanone (MEK)ND ug/kg 11/10/23 08:16 78-93-3 v2,v311/09/23 22:5719546.8 1
n-Butylbenzene ND ug/kg 11/10/23 08:16 104-51-811/09/23 22:579.7 6.1 1
sec-Butylbenzene ND ug/kg 11/10/23 08:16 135-98-811/09/23 22:579.7 4.3 1
tert-Butylbenzene ND ug/kg 11/10/23 08:16 98-06-611/09/23 22:579.7 3.5 1
Carbon tetrachloride ND ug/kg 11/10/23 08:16 56-23-511/09/23 22:579.7 3.6 1
Chlorobenzene ND ug/kg 11/10/23 08:16 108-90-711/09/23 22:579.7 5.6 1
Chloroethane ND ug/kg 11/10/23 08:16 75-00-311/09/23 22:5719.5 7.5 1
Chloroform ND ug/kg 11/10/23 08:16 67-66-311/09/23 22:579.7 8.1 1
Chloromethane ND ug/kg 11/10/23 08:16 74-87-311/09/23 22:5719.5 8.2 1
2-Chlorotoluene ND ug/kg 11/10/23 08:16 95-49-811/09/23 22:579.7 3.5 1
4-Chlorotoluene ND ug/kg 11/10/23 08:16 106-43-411/09/23 22:579.7 5.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/10/23 08:16 96-12-811/09/23 22:579.7 3.8 1
Dibromochloromethane ND ug/kg 11/10/23 08:16 124-48-111/09/23 22:579.7 5.5 1
1,2-Dibromoethane (EDB)ND ug/kg 11/10/23 08:16 106-93-411/09/23 22:579.7 4.3 1
Dibromomethane ND ug/kg 11/10/23 08:16 74-95-311/09/23 22:579.7 2.1 1
1,2-Dichlorobenzene ND ug/kg 11/10/23 08:16 95-50-111/09/23 22:579.7 3.5 1
1,3-Dichlorobenzene ND ug/kg 11/10/23 08:16 541-73-111/09/23 22:579.7 3.0 1
1,4-Dichlorobenzene ND ug/kg 11/10/23 08:16 106-46-711/09/23 22:579.7 2.5 1
Dichlorodifluoromethane ND ug/kg 11/10/23 08:16 75-71-811/09/23 22:5719.5 9.9 1
1,1-Dichloroethane ND ug/kg 11/10/23 08:16 75-34-311/09/23 22:579.7 4.0 1
1,2-Dichloroethane ND ug/kg 11/10/23 08:16 107-06-211/09/23 22:579.7 6.5 1
1,1-Dichloroethene ND ug/kg 11/10/23 08:16 75-35-4 R111/09/23 22:579.7 4.0 1
cis-1,2-Dichloroethene ND ug/kg 11/10/23 08:16 156-59-211/09/23 22:579.7 3.3 1
trans-1,2-Dichloroethene ND ug/kg 11/10/23 08:16 156-60-5 R111/09/23 22:579.7 8.3 1
1,2-Dichloropropane ND ug/kg 11/10/23 08:16 78-87-511/09/23 22:579.7 2.9 1
1,3-Dichloropropane ND ug/kg 11/10/23 08:16 142-28-911/09/23 22:579.7 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-03 Lab ID:92697661002 Collected:11/07/23 16:50 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 11/10/23 08:16 594-20-711/09/23 22:579.7 7.4 1
1,1-Dichloropropene ND ug/kg 11/10/23 08:16 563-58-611/09/23 22:579.7 4.7 1
cis-1,3-Dichloropropene ND ug/kg 11/10/23 08:16 10061-01-511/09/23 22:579.7 2.7 1
trans-1,3-Dichloropropene ND ug/kg 11/10/23 08:16 10061-02-611/09/23 22:579.7 3.4 1
Diisopropyl ether ND ug/kg 11/10/23 08:16 108-20-311/09/23 22:579.7 2.6 1
Ethylbenzene 6.1J ug/kg 11/10/23 08:16 100-41-411/09/23 22:579.7 4.5 1
Hexachloro-1,3-butadiene ND ug/kg 11/10/23 08:16 87-68-311/09/23 22:5719.5 15.9 1
2-Hexanone ND ug/kg 11/10/23 08:16 591-78-611/09/23 22:5797.5 9.4 1
Isopropylbenzene (Cumene)ND ug/kg 11/10/23 08:16 98-82-811/09/23 22:579.7 3.3 1
p-Isopropyltoluene ND ug/kg 11/10/23 08:16 99-87-611/09/23 22:579.7 4.8 1
Methylene Chloride ND ug/kg 11/10/23 08:16 75-09-2 R111/09/23 22:5739.0 26.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/10/23 08:16 108-10-111/09/23 22:5797.5 9.4 1
Methyl-tert-butyl ether ND ug/kg 11/10/23 08:16 1634-04-411/09/23 22:579.7 3.6 1
Naphthalene 28.3 ug/kg 11/10/23 08:16 91-20-3 R111/09/23 22:579.7 5.1 1
n-Propylbenzene ND ug/kg 11/10/23 08:16 103-65-111/09/23 22:579.7 3.5 1
Styrene ND ug/kg 11/10/23 08:16 100-42-511/09/23 22:579.7 2.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/10/23 08:16 630-20-611/09/23 22:579.7 3.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/10/23 08:16 79-34-511/09/23 22:579.7 2.6 1
Tetrachloroethene ND ug/kg 11/10/23 08:16 127-18-411/09/23 22:579.7 3.1 1
Toluene ND ug/kg 11/10/23 08:16 108-88-311/09/23 22:579.7 6.7 1
1,2,3-Trichlorobenzene ND ug/kg 11/10/23 08:16 87-61-6 R111/09/23 22:579.7 7.9 1
1,2,4-Trichlorobenzene ND ug/kg 11/10/23 08:16 120-82-1 IK11/09/23 22:579.7 8.2 1
1,1,1-Trichloroethane ND ug/kg 11/10/23 08:16 71-55-611/09/23 22:579.7 5.1 1
1,1,2-Trichloroethane ND ug/kg 11/10/23 08:16 79-00-511/09/23 22:579.7 3.2 1
Trichloroethene ND ug/kg 11/10/23 08:16 79-01-611/09/23 22:579.7 7.9 1
Trichlorofluoromethane ND ug/kg 11/10/23 08:16 75-69-411/09/23 22:579.7 5.4 1
1,2,3-Trichloropropane ND ug/kg 11/10/23 08:16 96-18-411/09/23 22:579.7 4.9 1
1,2,4-Trimethylbenzene ND ug/kg 11/10/23 08:16 95-63-611/09/23 22:579.7 5.8 1
1,3,5-Trimethylbenzene ND ug/kg 11/10/23 08:16 108-67-811/09/23 22:579.7 3.3 1
Vinyl acetate ND ug/kg 11/10/23 08:16 108-05-411/09/23 22:5797.5 20.1 1
Vinyl chloride ND ug/kg 11/10/23 08:16 75-01-411/09/23 22:5719.5 5.0 1
Xylene (Total)7.1J ug/kg 11/10/23 08:16 1330-20-711/09/23 22:5719.5 5.6 1
m&p-Xylene 7.1J ug/kg 11/10/23 08:16 179601-23-111/09/23 22:5719.5 6.7 1
o-Xylene ND ug/kg 11/10/23 08:16 95-47-611/09/23 22:579.7 4.3 1
Surrogates
Toluene-d8 (S)98 %11/10/23 08:16 2037-26-511/09/23 22:5770-130 1
4-Bromofluorobenzene (S)97 %11/10/23 08:16 460-00-411/09/23 22:5770-130 1
1,2-Dichloroethane-d4 (S)86 %11/10/23 08:16 17060-07-011/09/23 22:5770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.3 %11/09/23 13:49 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-04 Lab ID:92697661003 Collected:11/07/23 17:15 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.50J mg/kg 11/09/23 22:29 18540-29-9 B11/09/23 10:471.2 0.0012 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 2.4 mg/kg 11/15/23 13:08 7440-38-211/14/23 15:441.8 0.29 1
Barium 73.1 mg/kg 11/15/23 13:08 7440-39-311/14/23 15:440.71 0.080 1
Cadmium 0.31 mg/kg 11/15/23 13:08 7440-43-911/14/23 15:440.071 0.018 1
Chromium 44.1 mg/kg 11/15/23 13:08 7440-47-311/14/23 15:440.35 0.053 1
Lead 18.2 mg/kg 11/15/23 13:08 7439-92-111/14/23 15:440.71 0.18 1
Selenium ND mg/kg 11/16/23 15:23 7782-49-211/14/23 15:443.5 2.7 5
Silver ND mg/kg 11/15/23 13:08 7440-22-411/14/23 15:440.35 0.033 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.057 mg/kg 11/15/23 14:56 7439-97-611/14/23 12:410.0067 0.0041 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 11/13/23 12:19 83-32-911/11/23 12:1219606895
Acenaphthylene ND ug/kg 11/13/23 12:19 208-96-811/11/23 12:1219606895
Aniline ND ug/kg 11/13/23 12:19 62-53-311/11/23 12:1219607665
Anthracene ND ug/kg 11/13/23 12:19 120-12-711/11/23 12:1219606415
Benzo(a)anthracene ND ug/kg 11/13/23 12:19 56-55-311/11/23 12:1219606535
Benzo(a)pyrene ND ug/kg 11/13/23 12:19 50-32-811/11/23 12:1219606775
Benzo(b)fluoranthene ND ug/kg 11/13/23 12:19 205-99-211/11/23 12:1219606535
Benzo(g,h,i)perylene ND ug/kg 11/13/23 12:19 191-24-211/11/23 12:1219607605
Benzo(k)fluoranthene ND ug/kg 11/13/23 12:19 207-08-911/11/23 12:1219606895
Benzoic Acid ND ug/kg 11/13/23 12:19 65-85-011/11/23 12:12979042105
Benzyl alcohol ND ug/kg 11/13/23 12:19 100-51-611/11/23 12:12392014805
4-Bromophenylphenyl ether ND ug/kg 11/13/23 12:19 101-55-311/11/23 12:1219607545
Butylbenzylphthalate ND ug/kg 11/13/23 12:19 85-68-711/11/23 12:1219608255
4-Chloro-3-methylphenol ND ug/kg 11/13/23 12:19 59-50-711/11/23 12:12392013805
4-Chloroaniline ND ug/kg 11/13/23 12:19 106-47-811/11/23 12:12392015405
bis(2-Chloroethoxy)methane ND ug/kg 11/13/23 12:19 111-91-111/11/23 12:1219608135
bis(2-Chloroethyl) ether ND ug/kg 11/13/23 12:19 111-44-411/11/23 12:1219607365
2-Chloronaphthalene ND ug/kg 11/13/23 12:19 91-58-711/11/23 12:1219607785
2-Chlorophenol ND ug/kg 11/13/23 12:19 95-57-811/11/23 12:1219607365
4-Chlorophenylphenyl ether ND ug/kg 11/13/23 12:19 7005-72-311/11/23 12:1219607305
Chrysene ND ug/kg 11/13/23 12:19 218-01-911/11/23 12:1219607125
Dibenz(a,h)anthracene ND ug/kg 11/13/23 12:19 53-70-311/11/23 12:1219607545
Dibenzofuran ND ug/kg 11/13/23 12:19 132-64-911/11/23 12:1219607065
1,2-Dichlorobenzene ND ug/kg 11/13/23 12:19 95-50-111/11/23 12:1219607065
1,3-Dichlorobenzene ND ug/kg 11/13/23 12:19 541-73-111/11/23 12:1219606945
1,4-Dichlorobenzene ND ug/kg 11/13/23 12:19 106-46-711/11/23 12:1219607485
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-04 Lab ID:92697661003 Collected:11/07/23 17:15 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 11/13/23 12:19 91-94-1 L211/11/23 12:12392013205
2,4-Dichlorophenol ND ug/kg 11/13/23 12:19 120-83-211/11/23 12:1219607665
Diethylphthalate ND ug/kg 11/13/23 12:19 84-66-211/11/23 12:1219607185
2,4-Dimethylphenol ND ug/kg 11/13/23 12:19 105-67-911/11/23 12:1219608135
Dimethylphthalate ND ug/kg 11/13/23 12:19 131-11-311/11/23 12:1219607125
Di-n-butylphthalate ND ug/kg 11/13/23 12:19 84-74-211/11/23 12:1219606595
4,6-Dinitro-2-methylphenol ND ug/kg 11/13/23 12:19 534-52-111/11/23 12:12392018305
2,4-Dinitrophenol ND ug/kg 11/13/23 12:19 51-28-511/11/23 12:12979060505
2,4-Dinitrotoluene ND ug/kg 11/13/23 12:19 121-14-211/11/23 12:1219607545
2,6-Dinitrotoluene ND ug/kg 11/13/23 12:19 606-20-211/11/23 12:1219607185
Di-n-octylphthalate ND ug/kg 11/13/23 12:19 117-84-011/11/23 12:1219607725
bis(2-Ethylhexyl)phthalate ND ug/kg 11/13/23 12:19 117-81-711/11/23 12:1219607605
Fluoranthene ND ug/kg 11/13/23 12:19 206-44-011/11/23 12:1219606715
Fluorene ND ug/kg 11/13/23 12:19 86-73-711/11/23 12:1219606895
Hexachloro-1,3-butadiene ND ug/kg 11/13/23 12:19 87-68-311/11/23 12:1219608495
Hexachlorobenzene ND ug/kg 11/13/23 12:19 118-74-111/11/23 12:1219607665
Hexachlorocyclopentadiene ND ug/kg 11/13/23 12:19 77-47-411/11/23 12:12196011205
Hexachloroethane ND ug/kg 11/13/23 12:19 67-72-111/11/23 12:1219607485
Indeno(1,2,3-cd)pyrene ND ug/kg 11/13/23 12:19 193-39-511/11/23 12:1219607725
Isophorone ND ug/kg 11/13/23 12:19 78-59-111/11/23 12:1219608735
1-Methylnaphthalene ND ug/kg 11/13/23 12:19 90-12-011/11/23 12:1219606895
2-Methylnaphthalene ND ug/kg 11/13/23 12:19 91-57-611/11/23 12:1219607835
2-Methylphenol(o-Cresol)ND ug/kg 11/13/23 12:19 95-48-711/11/23 12:1219608015
3&4-Methylphenol(m&p Cresol)ND ug/kg 11/13/23 12:19 15831-10-411/11/23 12:1219607895
Naphthalene ND ug/kg 11/13/23 12:19 91-20-311/11/23 12:1219606655
2-Nitroaniline ND ug/kg 11/13/23 12:19 88-74-411/11/23 12:12979016005
3-Nitroaniline ND ug/kg 11/13/23 12:19 99-09-211/11/23 12:12979015405
4-Nitroaniline ND ug/kg 11/13/23 12:19 100-01-611/11/23 12:12392014905
Nitrobenzene ND ug/kg 11/13/23 12:19 98-95-311/11/23 12:1219609085
2-Nitrophenol ND ug/kg 11/13/23 12:19 88-75-511/11/23 12:1219608495
4-Nitrophenol ND ug/kg 11/13/23 12:19 100-02-711/11/23 12:12979037905
N-Nitrosodimethylamine ND ug/kg 11/13/23 12:19 62-75-911/11/23 12:1219606595
N-Nitroso-di-n-propylamine ND ug/kg 11/13/23 12:19 621-64-711/11/23 12:1219607365
N-Nitrosodiphenylamine ND ug/kg 11/13/23 12:19 86-30-611/11/23 12:1219606945
2,2'-Oxybis(1-chloropropane)ND ug/kg 11/13/23 12:19 108-60-111/11/23 12:1219609325
Pentachlorophenol ND ug/kg 11/13/23 12:19 87-86-511/11/23 12:12392019205
Phenanthrene ND ug/kg 11/13/23 12:19 85-01-811/11/23 12:1219606415
Phenol ND ug/kg 11/13/23 12:19 108-95-211/11/23 12:1219608735
Pyrene ND ug/kg 11/13/23 12:19 129-00-011/11/23 12:1219607955
Pyridine ND ug/kg 11/13/23 12:19 110-86-111/11/23 12:1219606175
1,2,4-Trichlorobenzene ND ug/kg 11/13/23 12:19 120-82-111/11/23 12:1219607725
2,4,5-Trichlorophenol ND ug/kg 11/13/23 12:19 95-95-411/11/23 12:1219608965
2,4,6-Trichlorophenol ND ug/kg 11/13/23 12:19 88-06-211/11/23 12:1219608075
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-04 Lab ID:92697661003 Collected:11/07/23 17:15 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)52 %11/13/23 12:19 4165-60-011/11/23 12:1210-130 5
2-Fluorobiphenyl (S)49 %11/13/23 12:19 321-60-811/11/23 12:1210-130 5
Terphenyl-d14 (S)50 %11/13/23 12:19 1718-51-011/11/23 12:1210-130 5
Phenol-d6 (S)47 %11/13/23 12:19 13127-88-311/11/23 12:1210-130 5
2-Fluorophenol (S)43 %11/13/23 12:19 367-12-411/11/23 12:1210-130 5
2,4,6-Tribromophenol (S)52 %11/13/23 12:19 118-79-611/11/23 12:1210-130 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 11/10/23 08:34 67-64-1 v211/09/23 22:5714145.4 1
Benzene ND ug/kg 11/10/23 08:34 71-43-211/09/23 22:577.1 2.8 1
Bromobenzene ND ug/kg 11/10/23 08:34 108-86-111/09/23 22:577.1 2.3 1
Bromochloromethane ND ug/kg 11/10/23 08:34 74-97-511/09/23 22:577.1 2.1 1
Bromodichloromethane ND ug/kg 11/10/23 08:34 75-27-411/09/23 22:577.1 2.7 1
Bromoform ND ug/kg 11/10/23 08:34 75-25-211/09/23 22:577.1 2.5 1
Bromomethane ND ug/kg 11/10/23 08:34 74-83-9 IK11/09/23 22:5728.3 21.9 1
2-Butanone (MEK)ND ug/kg 11/10/23 08:34 78-93-3 v211/09/23 22:5714133.9 1
n-Butylbenzene ND ug/kg 11/10/23 08:34 104-51-811/09/23 22:577.1 4.5 1
sec-Butylbenzene ND ug/kg 11/10/23 08:34 135-98-811/09/23 22:577.1 3.1 1
tert-Butylbenzene ND ug/kg 11/10/23 08:34 98-06-611/09/23 22:577.1 2.5 1
Carbon tetrachloride ND ug/kg 11/10/23 08:34 56-23-511/09/23 22:577.1 2.6 1
Chlorobenzene ND ug/kg 11/10/23 08:34 108-90-711/09/23 22:577.1 4.1 1
Chloroethane ND ug/kg 11/10/23 08:34 75-00-311/09/23 22:5714.1 5.5 1
Chloroform ND ug/kg 11/10/23 08:34 67-66-311/09/23 22:577.1 5.9 1
Chloromethane ND ug/kg 11/10/23 08:34 74-87-311/09/23 22:5714.1 5.9 1
2-Chlorotoluene ND ug/kg 11/10/23 08:34 95-49-811/09/23 22:577.1 2.5 1
4-Chlorotoluene ND ug/kg 11/10/23 08:34 106-43-411/09/23 22:577.1 3.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/10/23 08:34 96-12-811/09/23 22:577.1 2.7 1
Dibromochloromethane ND ug/kg 11/10/23 08:34 124-48-111/09/23 22:577.1 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 11/10/23 08:34 106-93-411/09/23 22:577.1 3.1 1
Dibromomethane ND ug/kg 11/10/23 08:34 74-95-311/09/23 22:577.1 1.5 1
1,2-Dichlorobenzene ND ug/kg 11/10/23 08:34 95-50-111/09/23 22:577.1 2.5 1
1,3-Dichlorobenzene ND ug/kg 11/10/23 08:34 541-73-111/09/23 22:577.1 2.2 1
1,4-Dichlorobenzene ND ug/kg 11/10/23 08:34 106-46-711/09/23 22:577.1 1.8 1
Dichlorodifluoromethane ND ug/kg 11/10/23 08:34 75-71-811/09/23 22:5714.1 7.2 1
1,1-Dichloroethane ND ug/kg 11/10/23 08:34 75-34-311/09/23 22:577.1 2.9 1
1,2-Dichloroethane ND ug/kg 11/10/23 08:34 107-06-211/09/23 22:577.1 4.7 1
1,1-Dichloroethene ND ug/kg 11/10/23 08:34 75-35-411/09/23 22:577.1 2.9 1
cis-1,2-Dichloroethene ND ug/kg 11/10/23 08:34 156-59-211/09/23 22:577.1 2.4 1
trans-1,2-Dichloroethene ND ug/kg 11/10/23 08:34 156-60-511/09/23 22:577.1 6.0 1
1,2-Dichloropropane ND ug/kg 11/10/23 08:34 78-87-511/09/23 22:577.1 2.1 1
1,3-Dichloropropane ND ug/kg 11/10/23 08:34 142-28-911/09/23 22:577.1 2.2 1
2,2-Dichloropropane ND ug/kg 11/10/23 08:34 594-20-711/09/23 22:577.1 5.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-04 Lab ID:92697661003 Collected:11/07/23 17:15 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 11/10/23 08:34 563-58-611/09/23 22:577.1 3.4 1
cis-1,3-Dichloropropene ND ug/kg 11/10/23 08:34 10061-01-511/09/23 22:577.1 1.9 1
trans-1,3-Dichloropropene ND ug/kg 11/10/23 08:34 10061-02-611/09/23 22:577.1 2.4 1
Diisopropyl ether ND ug/kg 11/10/23 08:34 108-20-311/09/23 22:577.1 1.9 1
Ethylbenzene 5.2J ug/kg 11/10/23 08:34 100-41-411/09/23 22:577.1 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 11/10/23 08:34 87-68-311/09/23 22:5714.1 11.6 1
2-Hexanone ND ug/kg 11/10/23 08:34 591-78-611/09/23 22:5770.7 6.8 1
Isopropylbenzene (Cumene)ND ug/kg 11/10/23 08:34 98-82-811/09/23 22:577.1 2.4 1
p-Isopropyltoluene ND ug/kg 11/10/23 08:34 99-87-611/09/23 22:577.1 3.5 1
Methylene Chloride ND ug/kg 11/10/23 08:34 75-09-211/09/23 22:5728.3 19.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/10/23 08:34 108-10-111/09/23 22:5770.7 6.8 1
Methyl-tert-butyl ether ND ug/kg 11/10/23 08:34 1634-04-411/09/23 22:577.1 2.6 1
Naphthalene 4.8J ug/kg 11/10/23 08:34 91-20-311/09/23 22:577.1 3.7 1
n-Propylbenzene ND ug/kg 11/10/23 08:34 103-65-111/09/23 22:577.1 2.5 1
Styrene ND ug/kg 11/10/23 08:34 100-42-511/09/23 22:577.1 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/10/23 08:34 630-20-611/09/23 22:577.1 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/10/23 08:34 79-34-511/09/23 22:577.1 1.9 1
Tetrachloroethene ND ug/kg 11/10/23 08:34 127-18-411/09/23 22:577.1 2.2 1
Toluene ND ug/kg 11/10/23 08:34 108-88-311/09/23 22:577.1 4.9 1
1,2,3-Trichlorobenzene ND ug/kg 11/10/23 08:34 87-61-611/09/23 22:577.1 5.7 1
1,2,4-Trichlorobenzene ND ug/kg 11/10/23 08:34 120-82-1 IK11/09/23 22:577.1 5.9 1
1,1,1-Trichloroethane ND ug/kg 11/10/23 08:34 71-55-611/09/23 22:577.1 3.7 1
1,1,2-Trichloroethane ND ug/kg 11/10/23 08:34 79-00-511/09/23 22:577.1 2.3 1
Trichloroethene ND ug/kg 11/10/23 08:34 79-01-611/09/23 22:577.1 5.7 1
Trichlorofluoromethane ND ug/kg 11/10/23 08:34 75-69-411/09/23 22:577.1 3.9 1
1,2,3-Trichloropropane ND ug/kg 11/10/23 08:34 96-18-411/09/23 22:577.1 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 11/10/23 08:34 95-63-611/09/23 22:577.1 4.2 1
1,3,5-Trimethylbenzene ND ug/kg 11/10/23 08:34 108-67-811/09/23 22:577.1 2.4 1
Vinyl acetate ND ug/kg 11/10/23 08:34 108-05-411/09/23 22:5770.7 14.6 1
Vinyl chloride ND ug/kg 11/10/23 08:34 75-01-411/09/23 22:5714.1 3.6 1
Xylene (Total)ND ug/kg 11/10/23 08:34 1330-20-711/09/23 22:5714.1 4.0 1
m&p-Xylene ND ug/kg 11/10/23 08:34 179601-23-111/09/23 22:5714.1 4.8 1
o-Xylene ND ug/kg 11/10/23 08:34 95-47-611/09/23 22:577.1 3.1 1
Surrogates
Toluene-d8 (S)98 %11/10/23 08:34 2037-26-511/09/23 22:5770-130 1
4-Bromofluorobenzene (S)96 %11/10/23 08:34 460-00-411/09/23 22:5770-130 1
1,2-Dichloroethane-d4 (S)83 %11/10/23 08:34 17060-07-011/09/23 22:5770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.3 %11/09/23 13:49 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-05 Lab ID:92697661004 Collected:11/07/23 17:30 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.0050J mg/kg 11/09/23 22:47 18540-29-9 B11/09/23 10:471.2 0.0012 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 2.5 mg/kg 11/15/23 13:10 7440-38-211/14/23 15:442.0 0.33 1
Barium 67.3 mg/kg 11/15/23 13:10 7440-39-311/14/23 15:440.80 0.091 1
Cadmium 0.34 mg/kg 11/15/23 13:10 7440-43-911/14/23 15:440.080 0.021 1
Chromium 62.1 mg/kg 11/15/23 13:10 7440-47-311/14/23 15:440.40 0.060 1
Lead 22.5 mg/kg 11/15/23 13:10 7439-92-111/14/23 15:440.80 0.21 1
Selenium ND mg/kg 11/16/23 15:26 7782-49-211/14/23 15:444.0 3.1 5
Silver ND mg/kg 11/15/23 13:10 7440-22-411/14/23 15:440.40 0.038 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.049 mg/kg 11/15/23 14:58 7439-97-611/14/23 12:410.0067 0.0041 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 11/13/23 12:46 83-32-911/11/23 12:123961391
Acenaphthylene ND ug/kg 11/13/23 12:46 208-96-811/11/23 12:123961391
Aniline ND ug/kg 11/13/23 12:46 62-53-311/11/23 12:123961551
Anthracene ND ug/kg 11/13/23 12:46 120-12-711/11/23 12:123961301
Benzo(a)anthracene ND ug/kg 11/13/23 12:46 56-55-311/11/23 12:123961321
Benzo(a)pyrene ND ug/kg 11/13/23 12:46 50-32-811/11/23 12:123961371
Benzo(b)fluoranthene ND ug/kg 11/13/23 12:46 205-99-211/11/23 12:123961321
Benzo(g,h,i)perylene ND ug/kg 11/13/23 12:46 191-24-211/11/23 12:123961541
Benzo(k)fluoranthene ND ug/kg 11/13/23 12:46 207-08-911/11/23 12:123961391
Benzoic Acid ND ug/kg 11/13/23 12:46 65-85-011/11/23 12:1219808511
Benzyl alcohol ND ug/kg 11/13/23 12:46 100-51-611/11/23 12:127933001
4-Bromophenylphenyl ether ND ug/kg 11/13/23 12:46 101-55-311/11/23 12:123961531
Butylbenzylphthalate ND ug/kg 11/13/23 12:46 85-68-711/11/23 12:123961671
4-Chloro-3-methylphenol ND ug/kg 11/13/23 12:46 59-50-711/11/23 12:127932791
4-Chloroaniline ND ug/kg 11/13/23 12:46 106-47-811/11/23 12:127933111
bis(2-Chloroethoxy)methane ND ug/kg 11/13/23 12:46 111-91-111/11/23 12:123961651
bis(2-Chloroethyl) ether ND ug/kg 11/13/23 12:46 111-44-411/11/23 12:123961491
2-Chloronaphthalene ND ug/kg 11/13/23 12:46 91-58-711/11/23 12:123961571
2-Chlorophenol ND ug/kg 11/13/23 12:46 95-57-811/11/23 12:123961491
4-Chlorophenylphenyl ether ND ug/kg 11/13/23 12:46 7005-72-311/11/23 12:123961481
Chrysene ND ug/kg 11/13/23 12:46 218-01-911/11/23 12:123961441
Dibenz(a,h)anthracene ND ug/kg 11/13/23 12:46 53-70-311/11/23 12:123961531
Dibenzofuran ND ug/kg 11/13/23 12:46 132-64-911/11/23 12:123961431
1,2-Dichlorobenzene ND ug/kg 11/13/23 12:46 95-50-111/11/23 12:123961431
1,3-Dichlorobenzene ND ug/kg 11/13/23 12:46 541-73-111/11/23 12:123961401
1,4-Dichlorobenzene ND ug/kg 11/13/23 12:46 106-46-711/11/23 12:123961511
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-05 Lab ID:92697661004 Collected:11/07/23 17:30 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 11/13/23 12:46 91-94-1 L211/11/23 12:127932681
2,4-Dichlorophenol ND ug/kg 11/13/23 12:46 120-83-211/11/23 12:123961551
Diethylphthalate ND ug/kg 11/13/23 12:46 84-66-211/11/23 12:123961451
2,4-Dimethylphenol ND ug/kg 11/13/23 12:46 105-67-911/11/23 12:123961651
Dimethylphthalate ND ug/kg 11/13/23 12:46 131-11-311/11/23 12:123961441
Di-n-butylphthalate ND ug/kg 11/13/23 12:46 84-74-211/11/23 12:123961331
4,6-Dinitro-2-methylphenol ND ug/kg 11/13/23 12:46 534-52-111/11/23 12:127933701
2,4-Dinitrophenol ND ug/kg 11/13/23 12:46 51-28-511/11/23 12:12198012201
2,4-Dinitrotoluene ND ug/kg 11/13/23 12:46 121-14-211/11/23 12:123961531
2,6-Dinitrotoluene ND ug/kg 11/13/23 12:46 606-20-211/11/23 12:123961451
Di-n-octylphthalate ND ug/kg 11/13/23 12:46 117-84-011/11/23 12:123961561
bis(2-Ethylhexyl)phthalate ND ug/kg 11/13/23 12:46 117-81-711/11/23 12:123961541
Fluoranthene ND ug/kg 11/13/23 12:46 206-44-011/11/23 12:123961361
Fluorene ND ug/kg 11/13/23 12:46 86-73-711/11/23 12:123961391
Hexachloro-1,3-butadiene ND ug/kg 11/13/23 12:46 87-68-311/11/23 12:123961721
Hexachlorobenzene ND ug/kg 11/13/23 12:46 118-74-111/11/23 12:123961551
Hexachlorocyclopentadiene ND ug/kg 11/13/23 12:46 77-47-411/11/23 12:123962271
Hexachloroethane ND ug/kg 11/13/23 12:46 67-72-111/11/23 12:123961511
Indeno(1,2,3-cd)pyrene ND ug/kg 11/13/23 12:46 193-39-511/11/23 12:123961561
Isophorone ND ug/kg 11/13/23 12:46 78-59-111/11/23 12:123961771
1-Methylnaphthalene ND ug/kg 11/13/23 12:46 90-12-011/11/23 12:123961391
2-Methylnaphthalene ND ug/kg 11/13/23 12:46 91-57-611/11/23 12:123961591
2-Methylphenol(o-Cresol)ND ug/kg 11/13/23 12:46 95-48-711/11/23 12:123961621
3&4-Methylphenol(m&p Cresol)ND ug/kg 11/13/23 12:46 15831-10-411/11/23 12:123961601
Naphthalene ND ug/kg 11/13/23 12:46 91-20-311/11/23 12:123961341
2-Nitroaniline ND ug/kg 11/13/23 12:46 88-74-411/11/23 12:1219803241
3-Nitroaniline ND ug/kg 11/13/23 12:46 99-09-211/11/23 12:1219803111
4-Nitroaniline ND ug/kg 11/13/23 12:46 100-01-611/11/23 12:127933011
Nitrobenzene ND ug/kg 11/13/23 12:46 98-95-311/11/23 12:123961841
2-Nitrophenol ND ug/kg 11/13/23 12:46 88-75-511/11/23 12:123961721
4-Nitrophenol ND ug/kg 11/13/23 12:46 100-02-711/11/23 12:1219807661
N-Nitrosodimethylamine ND ug/kg 11/13/23 12:46 62-75-911/11/23 12:123961331
N-Nitroso-di-n-propylamine ND ug/kg 11/13/23 12:46 621-64-711/11/23 12:123961491
N-Nitrosodiphenylamine ND ug/kg 11/13/23 12:46 86-30-611/11/23 12:123961401
2,2'-Oxybis(1-chloropropane)ND ug/kg 11/13/23 12:46 108-60-111/11/23 12:123961891
Pentachlorophenol ND ug/kg 11/13/23 12:46 87-86-511/11/23 12:127933881
Phenanthrene ND ug/kg 11/13/23 12:46 85-01-811/11/23 12:123961301
Phenol ND ug/kg 11/13/23 12:46 108-95-211/11/23 12:123961771
Pyrene ND ug/kg 11/13/23 12:46 129-00-011/11/23 12:123961611
Pyridine ND ug/kg 11/13/23 12:46 110-86-111/11/23 12:123961251
1,2,4-Trichlorobenzene ND ug/kg 11/13/23 12:46 120-82-111/11/23 12:123961561
2,4,5-Trichlorophenol ND ug/kg 11/13/23 12:46 95-95-411/11/23 12:123961811
2,4,6-Trichlorophenol ND ug/kg 11/13/23 12:46 88-06-211/11/23 12:123961631
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-05 Lab ID:92697661004 Collected:11/07/23 17:30 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)57 %11/13/23 12:46 4165-60-011/11/23 12:1210-130 1
2-Fluorobiphenyl (S)50 %11/13/23 12:46 321-60-811/11/23 12:1210-130 1
Terphenyl-d14 (S)51 %11/13/23 12:46 1718-51-011/11/23 12:1210-130 1
Phenol-d6 (S)51 %11/13/23 12:46 13127-88-311/11/23 12:1210-130 1
2-Fluorophenol (S)50 %11/13/23 12:46 367-12-411/11/23 12:1210-130 1
2,4,6-Tribromophenol (S)60 %11/13/23 12:46 118-79-611/11/23 12:1210-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 11/10/23 08:53 67-64-1 v211/09/23 22:5715950.9 1
Benzene ND ug/kg 11/10/23 08:53 71-43-211/09/23 22:577.9 3.2 1
Bromobenzene ND ug/kg 11/10/23 08:53 108-86-111/09/23 22:577.9 2.6 1
Bromochloromethane ND ug/kg 11/10/23 08:53 74-97-511/09/23 22:577.9 2.3 1
Bromodichloromethane ND ug/kg 11/10/23 08:53 75-27-411/09/23 22:577.9 3.1 1
Bromoform ND ug/kg 11/10/23 08:53 75-25-211/09/23 22:577.9 2.8 1
Bromomethane ND ug/kg 11/10/23 08:53 74-83-9 IK11/09/23 22:5731.7 24.6 1
2-Butanone (MEK)ND ug/kg 11/10/23 08:53 78-93-3 v211/09/23 22:5715938.1 1
n-Butylbenzene ND ug/kg 11/10/23 08:53 104-51-811/09/23 22:577.9 5.0 1
sec-Butylbenzene ND ug/kg 11/10/23 08:53 135-98-811/09/23 22:577.9 3.5 1
tert-Butylbenzene ND ug/kg 11/10/23 08:53 98-06-611/09/23 22:577.9 2.8 1
Carbon tetrachloride ND ug/kg 11/10/23 08:53 56-23-511/09/23 22:577.9 3.0 1
Chlorobenzene ND ug/kg 11/10/23 08:53 108-90-711/09/23 22:577.9 4.6 1
Chloroethane ND ug/kg 11/10/23 08:53 75-00-311/09/23 22:5715.9 6.1 1
Chloroform ND ug/kg 11/10/23 08:53 67-66-311/09/23 22:577.9 6.6 1
Chloromethane ND ug/kg 11/10/23 08:53 74-87-311/09/23 22:5715.9 6.7 1
2-Chlorotoluene ND ug/kg 11/10/23 08:53 95-49-811/09/23 22:577.9 2.8 1
4-Chlorotoluene ND ug/kg 11/10/23 08:53 106-43-411/09/23 22:577.9 4.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/10/23 08:53 96-12-811/09/23 22:577.9 3.1 1
Dibromochloromethane ND ug/kg 11/10/23 08:53 124-48-111/09/23 22:577.9 4.5 1
1,2-Dibromoethane (EDB)ND ug/kg 11/10/23 08:53 106-93-411/09/23 22:577.9 3.5 1
Dibromomethane ND ug/kg 11/10/23 08:53 74-95-311/09/23 22:577.9 1.7 1
1,2-Dichlorobenzene ND ug/kg 11/10/23 08:53 95-50-111/09/23 22:577.9 2.9 1
1,3-Dichlorobenzene ND ug/kg 11/10/23 08:53 541-73-111/09/23 22:577.9 2.5 1
1,4-Dichlorobenzene ND ug/kg 11/10/23 08:53 106-46-711/09/23 22:577.9 2.1 1
Dichlorodifluoromethane ND ug/kg 11/10/23 08:53 75-71-811/09/23 22:5715.9 8.1 1
1,1-Dichloroethane ND ug/kg 11/10/23 08:53 75-34-311/09/23 22:577.9 3.3 1
1,2-Dichloroethane ND ug/kg 11/10/23 08:53 107-06-211/09/23 22:577.9 5.3 1
1,1-Dichloroethene ND ug/kg 11/10/23 08:53 75-35-411/09/23 22:577.9 3.3 1
cis-1,2-Dichloroethene ND ug/kg 11/10/23 08:53 156-59-211/09/23 22:577.9 2.7 1
trans-1,2-Dichloroethene ND ug/kg 11/10/23 08:53 156-60-511/09/23 22:577.9 6.7 1
1,2-Dichloropropane ND ug/kg 11/10/23 08:53 78-87-511/09/23 22:577.9 2.4 1
1,3-Dichloropropane ND ug/kg 11/10/23 08:53 142-28-911/09/23 22:577.9 2.5 1
2,2-Dichloropropane ND ug/kg 11/10/23 08:53 594-20-711/09/23 22:577.9 6.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-05 Lab ID:92697661004 Collected:11/07/23 17:30 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 11/10/23 08:53 563-58-611/09/23 22:577.9 3.8 1
cis-1,3-Dichloropropene ND ug/kg 11/10/23 08:53 10061-01-511/09/23 22:577.9 2.2 1
trans-1,3-Dichloropropene ND ug/kg 11/10/23 08:53 10061-02-611/09/23 22:577.9 2.7 1
Diisopropyl ether ND ug/kg 11/10/23 08:53 108-20-311/09/23 22:577.9 2.1 1
Ethylbenzene 4.8J ug/kg 11/10/23 08:53 100-41-411/09/23 22:577.9 3.7 1
Hexachloro-1,3-butadiene ND ug/kg 11/10/23 08:53 87-68-311/09/23 22:5715.9 13.0 1
2-Hexanone ND ug/kg 11/10/23 08:53 591-78-611/09/23 22:5779.3 7.6 1
Isopropylbenzene (Cumene)ND ug/kg 11/10/23 08:53 98-82-811/09/23 22:577.9 2.7 1
p-Isopropyltoluene ND ug/kg 11/10/23 08:53 99-87-611/09/23 22:577.9 3.9 1
Methylene Chloride ND ug/kg 11/10/23 08:53 75-09-211/09/23 22:5731.7 21.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/10/23 08:53 108-10-111/09/23 22:5779.3 7.6 1
Methyl-tert-butyl ether ND ug/kg 11/10/23 08:53 1634-04-411/09/23 22:577.9 3.0 1
Naphthalene ND ug/kg 11/10/23 08:53 91-20-311/09/23 22:577.9 4.2 1
n-Propylbenzene ND ug/kg 11/10/23 08:53 103-65-111/09/23 22:577.9 2.8 1
Styrene ND ug/kg 11/10/23 08:53 100-42-511/09/23 22:577.9 2.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/10/23 08:53 630-20-611/09/23 22:577.9 3.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/10/23 08:53 79-34-511/09/23 22:577.9 2.1 1
Tetrachloroethene ND ug/kg 11/10/23 08:53 127-18-411/09/23 22:577.9 2.5 1
Toluene ND ug/kg 11/10/23 08:53 108-88-311/09/23 22:577.9 5.5 1
1,2,3-Trichlorobenzene ND ug/kg 11/10/23 08:53 87-61-611/09/23 22:577.9 6.4 1
1,2,4-Trichlorobenzene ND ug/kg 11/10/23 08:53 120-82-1 IK11/09/23 22:577.9 6.7 1
1,1,1-Trichloroethane ND ug/kg 11/10/23 08:53 71-55-611/09/23 22:577.9 4.1 1
1,1,2-Trichloroethane ND ug/kg 11/10/23 08:53 79-00-511/09/23 22:577.9 2.6 1
Trichloroethene ND ug/kg 11/10/23 08:53 79-01-611/09/23 22:577.9 6.4 1
Trichlorofluoromethane ND ug/kg 11/10/23 08:53 75-69-411/09/23 22:577.9 4.4 1
1,2,3-Trichloropropane ND ug/kg 11/10/23 08:53 96-18-411/09/23 22:577.9 4.0 1
1,2,4-Trimethylbenzene ND ug/kg 11/10/23 08:53 95-63-611/09/23 22:577.9 4.7 1
1,3,5-Trimethylbenzene ND ug/kg 11/10/23 08:53 108-67-811/09/23 22:577.9 2.7 1
Vinyl acetate ND ug/kg 11/10/23 08:53 108-05-411/09/23 22:5779.3 16.3 1
Vinyl chloride ND ug/kg 11/10/23 08:53 75-01-411/09/23 22:5715.9 4.0 1
Xylene (Total)5.5J ug/kg 11/10/23 08:53 1330-20-711/09/23 22:5715.9 4.5 1
m&p-Xylene 5.5J ug/kg 11/10/23 08:53 179601-23-111/09/23 22:5715.9 5.4 1
o-Xylene ND ug/kg 11/10/23 08:53 95-47-611/09/23 22:577.9 3.5 1
Surrogates
Toluene-d8 (S)100 %11/10/23 08:53 2037-26-511/09/23 22:5770-130 1
4-Bromofluorobenzene (S)95 %11/10/23 08:53 460-00-411/09/23 22:5770-130 1
1,2-Dichloroethane-d4 (S)121 %11/10/23 08:53 17060-07-011/09/23 22:5770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.6 %11/09/23 13:49 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-DUP-02 Lab ID:92697661005 Collected:11/07/23 16:25 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: EPA 7199
Pace Analytical Services - Charlotte
7199 Chromium, Hexavalent
Chromium, Hexavalent 0.0017J mg/kg 11/09/23 23:04 18540-29-9 B11/09/23 10:471.2 0.0012 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 2.5J mg/kg 11/15/23 13:19 7440-38-211/14/23 15:442.7 0.44 1
Barium 78.4 mg/kg 11/15/23 13:19 7440-39-311/14/23 15:441.1 0.12 1
Cadmium 0.33 mg/kg 11/15/23 13:19 7440-43-911/14/23 15:440.11 0.028 1
Chromium 43.1 mg/kg 11/15/23 13:19 7440-47-311/14/23 15:440.54 0.081 1
Lead 21.5 mg/kg 11/15/23 13:19 7439-92-111/14/23 15:441.1 0.28 1
Selenium ND mg/kg 11/16/23 15:28 7782-49-211/14/23 15:445.4 4.1 5
Silver ND mg/kg 11/15/23 13:19 7440-22-411/14/23 15:440.54 0.051 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.052 mg/kg 11/15/23 15:00 7439-97-611/14/23 12:410.0063 0.0039 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 11/13/23 13:13 83-32-911/11/23 12:1220307145
Acenaphthylene ND ug/kg 11/13/23 13:13 208-96-811/11/23 12:1220307145
Aniline ND ug/kg 11/13/23 13:13 62-53-311/11/23 12:1220307945
Anthracene ND ug/kg 11/13/23 13:13 120-12-711/11/23 12:1220306655
Benzo(a)anthracene ND ug/kg 11/13/23 13:13 56-55-311/11/23 12:1220306775
Benzo(a)pyrene ND ug/kg 11/13/23 13:13 50-32-811/11/23 12:1220307025
Benzo(b)fluoranthene ND ug/kg 11/13/23 13:13 205-99-211/11/23 12:1220306775
Benzo(g,h,i)perylene ND ug/kg 11/13/23 13:13 191-24-211/11/23 12:1220307885
Benzo(k)fluoranthene ND ug/kg 11/13/23 13:13 207-08-911/11/23 12:1220307145
Benzoic Acid ND ug/kg 11/13/23 13:13 65-85-011/11/23 12:121020043705
Benzyl alcohol ND ug/kg 11/13/23 13:13 100-51-611/11/23 12:12406015405
4-Bromophenylphenyl ether ND ug/kg 11/13/23 13:13 101-55-311/11/23 12:1220307825
Butylbenzylphthalate ND ug/kg 11/13/23 13:13 85-68-711/11/23 12:1220308565
4-Chloro-3-methylphenol ND ug/kg 11/13/23 13:13 59-50-711/11/23 12:12406014305
4-Chloroaniline ND ug/kg 11/13/23 13:13 106-47-811/11/23 12:12406016005
bis(2-Chloroethoxy)methane ND ug/kg 11/13/23 13:13 111-91-111/11/23 12:1220308445
bis(2-Chloroethyl) ether ND ug/kg 11/13/23 13:13 111-44-411/11/23 12:1220307645
2-Chloronaphthalene ND ug/kg 11/13/23 13:13 91-58-711/11/23 12:1220308075
2-Chlorophenol ND ug/kg 11/13/23 13:13 95-57-811/11/23 12:1220307645
4-Chlorophenylphenyl ether ND ug/kg 11/13/23 13:13 7005-72-311/11/23 12:1220307575
Chrysene ND ug/kg 11/13/23 13:13 218-01-911/11/23 12:1220307395
Dibenz(a,h)anthracene ND ug/kg 11/13/23 13:13 53-70-311/11/23 12:1220307825
Dibenzofuran ND ug/kg 11/13/23 13:13 132-64-911/11/23 12:1220307335
1,2-Dichlorobenzene ND ug/kg 11/13/23 13:13 95-50-111/11/23 12:1220307335
1,3-Dichlorobenzene ND ug/kg 11/13/23 13:13 541-73-111/11/23 12:1220307215
1,4-Dichlorobenzene ND ug/kg 11/13/23 13:13 106-46-711/11/23 12:1220307765
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-DUP-02 Lab ID:92697661005 Collected:11/07/23 16:25 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 11/13/23 13:13 91-94-1 L211/11/23 12:12406013705
2,4-Dichlorophenol ND ug/kg 11/13/23 13:13 120-83-211/11/23 12:1220307945
Diethylphthalate ND ug/kg 11/13/23 13:13 84-66-211/11/23 12:1220307455
2,4-Dimethylphenol ND ug/kg 11/13/23 13:13 105-67-911/11/23 12:1220308445
Dimethylphthalate ND ug/kg 11/13/23 13:13 131-11-311/11/23 12:1220307395
Di-n-butylphthalate ND ug/kg 11/13/23 13:13 84-74-211/11/23 12:1220306845
4,6-Dinitro-2-methylphenol ND ug/kg 11/13/23 13:13 534-52-111/11/23 12:12406019005
2,4-Dinitrophenol ND ug/kg 11/13/23 13:13 51-28-511/11/23 12:121020062805
2,4-Dinitrotoluene ND ug/kg 11/13/23 13:13 121-14-211/11/23 12:1220307825
2,6-Dinitrotoluene ND ug/kg 11/13/23 13:13 606-20-211/11/23 12:1220307455
Di-n-octylphthalate ND ug/kg 11/13/23 13:13 117-84-011/11/23 12:1220308015
bis(2-Ethylhexyl)phthalate ND ug/kg 11/13/23 13:13 117-81-711/11/23 12:1220307885
Fluoranthene ND ug/kg 11/13/23 13:13 206-44-011/11/23 12:1220306965
Fluorene ND ug/kg 11/13/23 13:13 86-73-711/11/23 12:1220307145
Hexachloro-1,3-butadiene ND ug/kg 11/13/23 13:13 87-68-311/11/23 12:1220308815
Hexachlorobenzene ND ug/kg 11/13/23 13:13 118-74-111/11/23 12:1220307945
Hexachlorocyclopentadiene ND ug/kg 11/13/23 13:13 77-47-411/11/23 12:12203011605
Hexachloroethane ND ug/kg 11/13/23 13:13 67-72-111/11/23 12:1220307765
Indeno(1,2,3-cd)pyrene ND ug/kg 11/13/23 13:13 193-39-511/11/23 12:1220308015
Isophorone ND ug/kg 11/13/23 13:13 78-59-111/11/23 12:1220309055
1-Methylnaphthalene ND ug/kg 11/13/23 13:13 90-12-011/11/23 12:1220307145
2-Methylnaphthalene ND ug/kg 11/13/23 13:13 91-57-611/11/23 12:1220308135
2-Methylphenol(o-Cresol)ND ug/kg 11/13/23 13:13 95-48-711/11/23 12:1220308315
3&4-Methylphenol(m&p Cresol)ND ug/kg 11/13/23 13:13 15831-10-411/11/23 12:1220308195
Naphthalene ND ug/kg 11/13/23 13:13 91-20-311/11/23 12:1220306905
2-Nitroaniline ND ug/kg 11/13/23 13:13 88-74-411/11/23 12:121020016605
3-Nitroaniline ND ug/kg 11/13/23 13:13 99-09-211/11/23 12:121020016005
4-Nitroaniline ND ug/kg 11/13/23 13:13 100-01-611/11/23 12:12406015505
Nitrobenzene ND ug/kg 11/13/23 13:13 98-95-311/11/23 12:1220309425
2-Nitrophenol ND ug/kg 11/13/23 13:13 88-75-511/11/23 12:1220308815
4-Nitrophenol ND ug/kg 11/13/23 13:13 100-02-711/11/23 12:121020039305
N-Nitrosodimethylamine ND ug/kg 11/13/23 13:13 62-75-911/11/23 12:1220306845
N-Nitroso-di-n-propylamine ND ug/kg 11/13/23 13:13 621-64-711/11/23 12:1220307645
N-Nitrosodiphenylamine ND ug/kg 11/13/23 13:13 86-30-611/11/23 12:1220307215
2,2'-Oxybis(1-chloropropane)ND ug/kg 11/13/23 13:13 108-60-111/11/23 12:1220309675
Pentachlorophenol ND ug/kg 11/13/23 13:13 87-86-511/11/23 12:12406019905
Phenanthrene ND ug/kg 11/13/23 13:13 85-01-811/11/23 12:1220306655
Phenol ND ug/kg 11/13/23 13:13 108-95-211/11/23 12:1220309055
Pyrene ND ug/kg 11/13/23 13:13 129-00-011/11/23 12:1220308255
Pyridine ND ug/kg 11/13/23 13:13 110-86-111/11/23 12:1220306405
1,2,4-Trichlorobenzene ND ug/kg 11/13/23 13:13 120-82-111/11/23 12:1220308015
2,4,5-Trichlorophenol ND ug/kg 11/13/23 13:13 95-95-411/11/23 12:1220309305
2,4,6-Trichlorophenol ND ug/kg 11/13/23 13:13 88-06-211/11/23 12:1220308385
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
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Page 22 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-DUP-02 Lab ID:92697661005 Collected:11/07/23 16:25 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)57 %11/13/23 13:13 4165-60-011/11/23 12:1210-130 5
2-Fluorobiphenyl (S)51 %11/13/23 13:13 321-60-811/11/23 12:1210-130 5
Terphenyl-d14 (S)59 %11/13/23 13:13 1718-51-011/11/23 12:1210-130 5
Phenol-d6 (S)52 %11/13/23 13:13 13127-88-311/11/23 12:1210-130 5
2-Fluorophenol (S)48 %11/13/23 13:13 367-12-411/11/23 12:1210-130 5
2,4,6-Tribromophenol (S)56 %11/13/23 13:13 118-79-611/11/23 12:1210-130 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 11/10/23 09:11 67-64-1 v211/09/23 22:5714747.1 1
Benzene ND ug/kg 11/10/23 09:11 71-43-211/09/23 22:577.3 2.9 1
Bromobenzene ND ug/kg 11/10/23 09:11 108-86-111/09/23 22:577.3 2.4 1
Bromochloromethane ND ug/kg 11/10/23 09:11 74-97-511/09/23 22:577.3 2.2 1
Bromodichloromethane ND ug/kg 11/10/23 09:11 75-27-411/09/23 22:577.3 2.8 1
Bromoform ND ug/kg 11/10/23 09:11 75-25-211/09/23 22:577.3 2.6 1
Bromomethane ND ug/kg 11/10/23 09:11 74-83-9 IK11/09/23 22:5729.3 22.7 1
2-Butanone (MEK)ND ug/kg 11/10/23 09:11 78-93-3 v211/09/23 22:5714735.2 1
n-Butylbenzene ND ug/kg 11/10/23 09:11 104-51-811/09/23 22:577.3 4.6 1
sec-Butylbenzene ND ug/kg 11/10/23 09:11 135-98-811/09/23 22:577.3 3.2 1
tert-Butylbenzene ND ug/kg 11/10/23 09:11 98-06-611/09/23 22:577.3 2.6 1
Carbon tetrachloride ND ug/kg 11/10/23 09:11 56-23-511/09/23 22:577.3 2.7 1
Chlorobenzene ND ug/kg 11/10/23 09:11 108-90-711/09/23 22:577.3 4.2 1
Chloroethane ND ug/kg 11/10/23 09:11 75-00-311/09/23 22:5714.7 5.7 1
Chloroform ND ug/kg 11/10/23 09:11 67-66-311/09/23 22:577.3 6.1 1
Chloromethane ND ug/kg 11/10/23 09:11 74-87-311/09/23 22:5714.7 6.2 1
2-Chlorotoluene ND ug/kg 11/10/23 09:11 95-49-811/09/23 22:577.3 2.6 1
4-Chlorotoluene ND ug/kg 11/10/23 09:11 106-43-411/09/23 22:577.3 4.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/10/23 09:11 96-12-811/09/23 22:577.3 2.8 1
Dibromochloromethane ND ug/kg 11/10/23 09:11 124-48-111/09/23 22:577.3 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 11/10/23 09:11 106-93-411/09/23 22:577.3 3.2 1
Dibromomethane ND ug/kg 11/10/23 09:11 74-95-311/09/23 22:577.3 1.6 1
1,2-Dichlorobenzene ND ug/kg 11/10/23 09:11 95-50-111/09/23 22:577.3 2.6 1
1,3-Dichlorobenzene ND ug/kg 11/10/23 09:11 541-73-111/09/23 22:577.3 2.3 1
1,4-Dichlorobenzene ND ug/kg 11/10/23 09:11 106-46-711/09/23 22:577.3 1.9 1
Dichlorodifluoromethane ND ug/kg 11/10/23 09:11 75-71-811/09/23 22:5714.7 7.5 1
1,1-Dichloroethane ND ug/kg 11/10/23 09:11 75-34-311/09/23 22:577.3 3.0 1
1,2-Dichloroethane ND ug/kg 11/10/23 09:11 107-06-211/09/23 22:577.3 4.9 1
1,1-Dichloroethene ND ug/kg 11/10/23 09:11 75-35-411/09/23 22:577.3 3.0 1
cis-1,2-Dichloroethene ND ug/kg 11/10/23 09:11 156-59-211/09/23 22:577.3 2.5 1
trans-1,2-Dichloroethene ND ug/kg 11/10/23 09:11 156-60-511/09/23 22:577.3 6.2 1
1,2-Dichloropropane ND ug/kg 11/10/23 09:11 78-87-511/09/23 22:577.3 2.2 1
1,3-Dichloropropane ND ug/kg 11/10/23 09:11 142-28-911/09/23 22:577.3 2.3 1
2,2-Dichloropropane ND ug/kg 11/10/23 09:11 594-20-711/09/23 22:577.3 5.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
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Page 23 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:CS-DUP-02 Lab ID:92697661005 Collected:11/07/23 16:25 Received:11/08/23 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 11/10/23 09:11 563-58-611/09/23 22:577.3 3.5 1
cis-1,3-Dichloropropene ND ug/kg 11/10/23 09:11 10061-01-511/09/23 22:577.3 2.0 1
trans-1,3-Dichloropropene ND ug/kg 11/10/23 09:11 10061-02-611/09/23 22:577.3 2.5 1
Diisopropyl ether ND ug/kg 11/10/23 09:11 108-20-311/09/23 22:577.3 2.0 1
Ethylbenzene 5.0J ug/kg 11/10/23 09:11 100-41-411/09/23 22:577.3 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 11/10/23 09:11 87-68-311/09/23 22:5714.7 12.0 1
2-Hexanone ND ug/kg 11/10/23 09:11 591-78-611/09/23 22:5773.3 7.1 1
Isopropylbenzene (Cumene)ND ug/kg 11/10/23 09:11 98-82-811/09/23 22:577.3 2.5 1
p-Isopropyltoluene 6.8J ug/kg 11/10/23 09:11 99-87-611/09/23 22:577.3 3.6 1
Methylene Chloride ND ug/kg 11/10/23 09:11 75-09-211/09/23 22:5729.3 20.1 1
4-Methyl-2-pentanone (MIBK)37.6J ug/kg 11/10/23 09:11 108-10-111/09/23 22:5773.3 7.1 1
Methyl-tert-butyl ether ND ug/kg 11/10/23 09:11 1634-04-411/09/23 22:577.3 2.7 1
Naphthalene 10.4 ug/kg 11/10/23 09:11 91-20-311/09/23 22:577.3 3.9 1
n-Propylbenzene ND ug/kg 11/10/23 09:11 103-65-111/09/23 22:577.3 2.6 1
Styrene ND ug/kg 11/10/23 09:11 100-42-511/09/23 22:577.3 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/10/23 09:11 630-20-611/09/23 22:577.3 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/10/23 09:11 79-34-511/09/23 22:577.3 1.9 1
Tetrachloroethene ND ug/kg 11/10/23 09:11 127-18-411/09/23 22:577.3 2.3 1
Toluene ND ug/kg 11/10/23 09:11 108-88-311/09/23 22:577.3 5.1 1
1,2,3-Trichlorobenzene ND ug/kg 11/10/23 09:11 87-61-611/09/23 22:577.3 5.9 1
1,2,4-Trichlorobenzene ND ug/kg 11/10/23 09:11 120-82-1 IK11/09/23 22:577.3 6.2 1
1,1,1-Trichloroethane ND ug/kg 11/10/23 09:11 71-55-611/09/23 22:577.3 3.8 1
1,1,2-Trichloroethane ND ug/kg 11/10/23 09:11 79-00-511/09/23 22:577.3 2.4 1
Trichloroethene ND ug/kg 11/10/23 09:11 79-01-611/09/23 22:577.3 5.9 1
Trichlorofluoromethane ND ug/kg 11/10/23 09:11 75-69-411/09/23 22:577.3 4.0 1
1,2,3-Trichloropropane ND ug/kg 11/10/23 09:11 96-18-411/09/23 22:577.3 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 11/10/23 09:11 95-63-611/09/23 22:577.3 4.4 1
1,3,5-Trimethylbenzene ND ug/kg 11/10/23 09:11 108-67-811/09/23 22:577.3 2.5 1
Vinyl acetate ND ug/kg 11/10/23 09:11 108-05-411/09/23 22:5773.3 15.1 1
Vinyl chloride ND ug/kg 11/10/23 09:11 75-01-411/09/23 22:5714.7 3.7 1
Xylene (Total)ND ug/kg 11/10/23 09:11 1330-20-711/09/23 22:5714.7 4.2 1
m&p-Xylene ND ug/kg 11/10/23 09:11 179601-23-111/09/23 22:5714.7 5.0 1
o-Xylene ND ug/kg 11/10/23 09:11 95-47-611/09/23 22:577.3 3.2 1
Surrogates
Toluene-d8 (S)98 %11/10/23 09:11 2037-26-511/09/23 22:5770-130 1
4-Bromofluorobenzene (S)99 %11/10/23 09:11 460-00-411/09/23 22:5770-130 1
1,2-Dichloroethane-d4 (S)107 %11/10/23 09:11 17060-07-011/09/23 22:5770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.3 %11/09/23 13:49 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:EB-02 Lab ID:92697661006 Collected:11/07/23 17:40 Received:11/08/23 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 11/11/23 02:29 67-64-1 v225.0 5.1 1
Benzene ND ug/L 11/11/23 02:29 71-43-21.0 0.34 1
Bromobenzene ND ug/L 11/11/23 02:29 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 11/11/23 02:29 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 11/11/23 02:29 75-27-41.0 0.31 1
Bromoform ND ug/L 11/11/23 02:29 75-25-21.0 0.34 1
Bromomethane ND ug/L 11/11/23 02:29 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 11/11/23 02:29 78-93-3 v25.0 4.0 1
Carbon tetrachloride ND ug/L 11/11/23 02:29 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 11/11/23 02:29 108-90-71.0 0.28 1
Chloroethane ND ug/L 11/11/23 02:29 75-00-31.0 0.65 1
Chloroform ND ug/L 11/11/23 02:29 67-66-31.0 0.43 1
Chloromethane ND ug/L 11/11/23 02:29 74-87-3 v21.0 0.54 1
2-Chlorotoluene ND ug/L 11/11/23 02:29 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 11/11/23 02:29 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 11/11/23 02:29 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 11/11/23 02:29 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 11/11/23 02:29 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/11/23 02:29 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 11/11/23 02:29 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 11/11/23 02:29 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 11/11/23 02:29 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 11/11/23 02:29 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 11/11/23 02:29 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 11/11/23 02:29 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 11/11/23 02:29 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 11/11/23 02:29 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 11/11/23 02:29 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 11/11/23 02:29 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 11/11/23 02:29 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 11/11/23 02:29 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 11/11/23 02:29 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 11/11/23 02:29 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 11/11/23 02:29 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 11/11/23 02:29 108-20-3 v21.0 0.31 1
Ethylbenzene ND ug/L 11/11/23 02:29 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 11/11/23 02:29 87-68-32.0 1.5 1
2-Hexanone ND ug/L 11/11/23 02:29 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 11/11/23 02:29 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 11/11/23 02:29 75-09-2 v25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/11/23 02:29 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 11/11/23 02:29 1634-04-4 v21.0 0.42 1
Naphthalene ND ug/L 11/11/23 02:29 91-20-31.0 0.64 1
Styrene ND ug/L 11/11/23 02:29 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 11/11/23 02:29 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92697661
71227190
Sample:EB-02 Lab ID:92697661006 Collected:11/07/23 17:40 Received:11/08/23 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 11/11/23 02:29 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 11/11/23 02:29 127-18-41.0 0.29 1
Toluene ND ug/L 11/11/23 02:29 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/11/23 02:29 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 11/11/23 02:29 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 11/11/23 02:29 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 11/11/23 02:29 79-00-51.0 0.32 1
Trichloroethene ND ug/L 11/11/23 02:29 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 11/11/23 02:29 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 11/11/23 02:29 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 11/11/23 02:29 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 11/11/23 02:29 75-01-4 v21.0 0.39 1
Xylene (Total)ND ug/L 11/11/23 02:29 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 11/11/23 02:29 179601-23-12.0 0.71 1
o-Xylene ND ug/L 11/11/23 02:29 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %11/11/23 02:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %11/11/23 02:29 17060-07-070-130 1
Toluene-d8 (S)100 %11/11/23 02:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
813005
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92697661001, 92697661002, 92697661003, 92697661004, 92697661005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4209521
Associated Lab Samples:92697661001, 92697661002, 92697661003, 92697661004, 92697661005
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 11/15/23 14:410.0037
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4209522LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0920.083 110 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4209523MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697661002
4209524
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.095 110 75-125115 1 200.093ND 0.11 0.11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
813148
EPA 3050B
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92697661001, 92697661002, 92697661003, 92697661004, 92697661005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4210199
Associated Lab Samples:92697661001, 92697661002, 92697661003, 92697661004, 92697661005
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 2.5 11/16/23 15:030.41
Barium mg/kg ND 1.0 11/16/23 15:030.11
Cadmium mg/kg ND 0.10 11/16/23 15:030.026
Chromium mg/kg ND 0.50 11/16/23 15:030.075
Lead mg/kg ND 1.0 11/16/23 15:030.26
Selenium mg/kg ND 1.0 11/16/23 15:030.77
Silver mg/kg ND 0.50 11/16/23 15:030.047
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4210200LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 48.550 97 80-120
Barium mg/kg 53.850 108 80-120
Cadmium mg/kg 49.250 98 80-120
Chromium mg/kg 50.850 102 80-120
Lead mg/kg 49.250 98 80-120
Selenium mg/kg 45.550 91 80-120
Silver mg/kg 25.025 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4210201MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697661002
4210202
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 60.7 88 75-12589 1 2061.12.6J 56.0 56.7
Barium mg/kg M160.7 21 75-12523 1 2061.1135 147 149
Cadmium mg/kg 60.7 92 75-12593 1 2061.10.26 56.3 56.8
Chromium mg/kg 60.7 104 75-125105 1 2061.137.1 100 101
Lead mg/kg 60.7 94 75-12594 1 2061.116.1 73.2 73.8
Selenium mg/kg 60.7 84 75-12586 3 2061.1ND 51.0 52.8
Silver mg/kg 30.3 96 75-12597 1 2030.6ND 29.1 29.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
812291
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92697661002, 92697661003, 92697661004, 92697661005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4206168
Associated Lab Samples:92697661002, 92697661003, 92697661004, 92697661005
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 11/10/23 07:581.9
1,1,1-Trichloroethane ug/kg ND 5.0 11/10/23 07:582.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 11/10/23 07:581.3
1,1,2-Trichloroethane ug/kg ND 5.0 11/10/23 07:581.7
1,1-Dichloroethane ug/kg ND 5.0 11/10/23 07:582.1
1,1-Dichloroethene ug/kg ND 5.0 11/10/23 07:582.1
1,1-Dichloropropene ug/kg ND 5.0 11/10/23 07:582.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 11/10/23 07:584.0
1,2,3-Trichloropropane ug/kg ND 5.0 11/10/23 07:582.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 IK11/10/23 07:584.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 11/10/23 07:583.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 11/10/23 07:581.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 11/10/23 07:582.2
1,2-Dichlorobenzene ug/kg ND 5.0 11/10/23 07:581.8
1,2-Dichloroethane ug/kg ND 5.0 11/10/23 07:583.3
1,2-Dichloropropane ug/kg ND 5.0 11/10/23 07:581.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 11/10/23 07:581.7
1,3-Dichlorobenzene ug/kg ND 5.0 11/10/23 07:581.6
1,3-Dichloropropane ug/kg ND 5.0 11/10/23 07:581.6
1,4-Dichlorobenzene ug/kg ND 5.0 11/10/23 07:581.3
2,2-Dichloropropane ug/kg ND 5.0 11/10/23 07:583.8
2-Butanone (MEK)ug/kg ND 100 v211/10/23 07:5824.0
2-Chlorotoluene ug/kg ND 5.0 11/10/23 07:581.8
2-Hexanone ug/kg ND 50.0 11/10/23 07:584.8
4-Chlorotoluene ug/kg ND 5.0 11/10/23 07:582.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 11/10/23 07:584.8
Acetone ug/kg ND 100 v211/10/23 07:5832.1
Benzene ug/kg ND 5.0 11/10/23 07:582.0
Bromobenzene ug/kg ND 5.0 11/10/23 07:581.6
Bromochloromethane ug/kg ND 5.0 11/10/23 07:581.5
Bromodichloromethane ug/kg ND 5.0 11/10/23 07:581.9
Bromoform ug/kg ND 5.0 11/10/23 07:581.8
Bromomethane ug/kg ND 20.0 IK11/10/23 07:5815.5
Carbon tetrachloride ug/kg ND 5.0 11/10/23 07:581.9
Chlorobenzene ug/kg ND 5.0 11/10/23 07:582.9
Chloroethane ug/kg ND 10.0 11/10/23 07:583.9
Chloroform ug/kg ND 5.0 11/10/23 07:584.2
Chloromethane ug/kg ND 10.0 11/10/23 07:584.2
cis-1,2-Dichloroethene ug/kg ND 5.0 11/10/23 07:581.7
cis-1,3-Dichloropropene ug/kg ND 5.0 11/10/23 07:581.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4206168
Associated Lab Samples:92697661002, 92697661003, 92697661004, 92697661005
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 11/10/23 07:582.8
Dibromomethane ug/kg ND 5.0 11/10/23 07:581.1
Dichlorodifluoromethane ug/kg ND 10.0 11/10/23 07:585.1
Diisopropyl ether ug/kg ND 5.0 11/10/23 07:581.4
Ethylbenzene ug/kg ND 5.0 11/10/23 07:582.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 11/10/23 07:588.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 11/10/23 07:581.7
m&p-Xylene ug/kg ND 10.0 11/10/23 07:583.4
Methyl-tert-butyl ether ug/kg ND 5.0 11/10/23 07:581.9
Methylene Chloride ug/kg ND 20.0 11/10/23 07:5813.7
n-Butylbenzene ug/kg ND 5.0 11/10/23 07:583.2
n-Propylbenzene ug/kg ND 5.0 11/10/23 07:581.8
Naphthalene ug/kg ND 5.0 11/10/23 07:582.6
o-Xylene ug/kg ND 5.0 11/10/23 07:582.2
p-Isopropyltoluene ug/kg ND 5.0 11/10/23 07:582.5
sec-Butylbenzene ug/kg ND 5.0 11/10/23 07:582.2
Styrene ug/kg ND 5.0 11/10/23 07:581.3
tert-Butylbenzene ug/kg ND 5.0 11/10/23 07:581.8
Tetrachloroethene ug/kg ND 5.0 11/10/23 07:581.6
Toluene ug/kg ND 5.0 11/10/23 07:583.4
trans-1,2-Dichloroethene ug/kg ND 5.0 11/10/23 07:584.2
trans-1,3-Dichloropropene ug/kg ND 5.0 11/10/23 07:581.7
Trichloroethene ug/kg ND 5.0 11/10/23 07:584.0
Trichlorofluoromethane ug/kg ND 5.0 11/10/23 07:582.8
Vinyl acetate ug/kg ND 50.0 11/10/23 07:5810.3
Vinyl chloride ug/kg ND 10.0 11/10/23 07:582.5
Xylene (Total)ug/kg ND 10.0 11/10/23 07:582.8
1,2-Dichloroethane-d4 (S)%85 70-130 11/10/23 07:58
4-Bromofluorobenzene (S)%98 70-130 11/10/23 07:58
Toluene-d8 (S)%97 70-130 11/10/23 07:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4206169LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 490500 98 70-130
1,1,1-Trichloroethane ug/kg 440500 88 70-130
1,1,2,2-Tetrachloroethane ug/kg 454500 91 70-130
1,1,2-Trichloroethane ug/kg 469500 94 70-130
1,1-Dichloroethane ug/kg 416500 83 70-130
1,1-Dichloroethene ug/kg 436500 87 70-132
1,1-Dichloropropene ug/kg 445500 89 70-130
1,2,3-Trichlorobenzene ug/kg 496500 99 62-136
1,2,3-Trichloropropane ug/kg 440500 88 70-130
1,2,4-Trichlorobenzene ug/kg 482 IK5009670-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4206169LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 467500 93 70-130
1,2-Dibromo-3-chloropropane ug/kg 428500 86 65-130
1,2-Dibromoethane (EDB)ug/kg 470500 94 70-130
1,2-Dichlorobenzene ug/kg 472500 94 70-130
1,2-Dichloroethane ug/kg 405500 81 70-130
1,2-Dichloropropane ug/kg 440500 88 70-130
1,3,5-Trimethylbenzene ug/kg 468500 94 70-130
1,3-Dichlorobenzene ug/kg 467500 93 70-130
1,3-Dichloropropane ug/kg 428500 86 70-130
1,4-Dichlorobenzene ug/kg 463500 93 70-130
2,2-Dichloropropane ug/kg 398500 80 60-130
2-Butanone (MEK)ug/kg 764 v310007666-130
2-Chlorotoluene ug/kg 448500 90 70-130
2-Hexanone ug/kg 8201000 82 68-130
4-Chlorotoluene ug/kg 446500 89 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 8361000 84 70-130
Acetone ug/kg 729 v310007360-130
Benzene ug/kg 457500 91 70-130
Bromobenzene ug/kg 494500 99 70-130
Bromochloromethane ug/kg 471500 94 70-130
Bromodichloromethane ug/kg 444500 89 70-130
Bromoform ug/kg 499500 100 70-130
Bromomethane ug/kg 499 IK50010043-175
Carbon tetrachloride ug/kg 476500 95 70-130
Chlorobenzene ug/kg 467500 93 70-130
Chloroethane ug/kg 415500 83 70-145
Chloroform ug/kg 432500 86 70-130
Chloromethane ug/kg 429500 86 66-146
cis-1,2-Dichloroethene ug/kg 419500 84 70-130
cis-1,3-Dichloropropene ug/kg 421500 84 70-130
Dibromochloromethane ug/kg 473500 95 70-130
Dibromomethane ug/kg 519500 104 70-130
Dichlorodifluoromethane ug/kg 485500 97 42-197
Diisopropyl ether ug/kg 388500 78 68-130
Ethylbenzene ug/kg 427500 85 70-130
Hexachloro-1,3-butadiene ug/kg 511500 102 70-130
Isopropylbenzene (Cumene)ug/kg 481500 96 70-130
m&p-Xylene ug/kg 9311000 93 70-130
Methyl-tert-butyl ether ug/kg 399500 80 70-130
Methylene Chloride ug/kg 408500 82 65-130
n-Butylbenzene ug/kg 440500 88 70-130
n-Propylbenzene ug/kg 447500 89 70-130
Naphthalene ug/kg 479500 96 65-135
o-Xylene ug/kg 484500 97 70-130
p-Isopropyltoluene ug/kg 467500 93 70-130
sec-Butylbenzene ug/kg 450500 90 70-130
Styrene ug/kg 491500 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4206169LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 468500 94 70-130
Tetrachloroethene ug/kg 510500 102 70-130
Toluene ug/kg 462500 92 70-130
trans-1,2-Dichloroethene ug/kg 412500 82 70-130
trans-1,3-Dichloropropene ug/kg 407500 81 70-130
Trichloroethene ug/kg 500500 100 70-130
Trichlorofluoromethane ug/kg 449500 90 62-140
Vinyl acetate ug/kg 8021000 80 70-140
Vinyl chloride ug/kg 390500 78 70-152
Xylene (Total)ug/kg 14101500 94 70-130
1,2-Dichloroethane-d4 (S)%82 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4206170MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697661002
4206171
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg 975 51 22-16658 13 30975ND501567
1,1,1-Trichloroethane ug/kg 975 43 23-17247 9 30975ND416457
1,1,2,2-Tetrachloroethane ug/kg 975 45 21-15854 18 30975ND441530
1,1,2-Trichloroethane ug/kg 975 52 25-16061 15 30975ND511595
1,1-Dichloroethane ug/kg 975 39 22-16645 14 30975ND377434
1,1-Dichloroethene ug/kg R19752918-18341 37 30975ND278404
1,1-Dichloropropene ug/kg 975 36 20-18140 12 30975ND347393
1,2,3-Trichlorobenzene ug/kg R19752210-16111 67 30975ND219109
1,2,3-Trichloropropane ug/kg 975 43 21-14752 18 30975ND418502
1,2,4-Trichlorobenzene ug/kg IK9752910-15929 0 30975ND279280
1,2,4-Trimethylbenzene ug/kg 975 39 17-17043 10 30975ND384424
1,2-Dibromo-3-
chloropropane ug/kg 975 39 10-13544 11 30975ND380425
1,2-Dibromoethane (EDB)ug/kg 975 50 30-15460 18 30975ND487581
1,2-Dichlorobenzene ug/kg 975 43 26-16251 17 30975ND422498
1,2-Dichloroethane ug/kg 975 40 23-16146 13 30975ND394450
1,2-Dichloropropane ug/kg 975 45 29-16550 11 30975ND437490
1,3,5-Trimethylbenzene ug/kg 975 39 20-17243 9 30975ND377415
1,3-Dichlorobenzene ug/kg 975 40 22-16444 9 30975ND391427
1,3-Dichloropropane ug/kg 975 45 27-15652 14 30975ND442506
1,4-Dichlorobenzene ug/kg 975 38 20-16146 19 30975ND368445
2,2-Dichloropropane ug/kg 975 36 10-15940 9 30975ND353387
2-Butanone (MEK)ug/kg v319503313-14336 9 301950ND650709
2-Chlorotoluene ug/kg 975 38 21-16643 12 30975ND374423
2-Hexanone ug/kg 1950 35 19-14540 13 301950ND679771
4-Chlorotoluene ug/kg 975 37 19-16342 14 30975ND357410
4-Methyl-2-pentanone
(MIBK)ug/kg 1950 40 21-15147 17 301950ND772914
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4206170MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697661002
4206171
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acetone ug/kg R1,v319502110-13332 38 301950ND445653
Benzene ug/kg 975 46 29-15651 11 30975ND447501
Bromobenzene ug/kg 975 48 25-16156 15 30975ND468541
Bromochloromethane ug/kg 975 49 27-15856 13 30975ND480546
Bromodichloromethane ug/kg 975 46 23-15853 14 30975ND445514
Bromoform ug/kg 975 53 19-15263 17 30975ND514611
Bromomethane ug/kg IK9752610-15229 11 30975ND251281
Carbon tetrachloride ug/kg 975 42 18-17246 11 30975ND407453
Chlorobenzene ug/kg 975 45 26-16652 15 30975ND435505
Chloroethane ug/kg 975 19 10-13019 2 30975ND184188
Chloroform ug/kg 975 42 25-16148 12 30975ND413465
Chloromethane ug/kg 975 39 27-19745 14 30975ND380438
cis-1,2-Dichloroethene ug/kg 975 39 28-16544 12 30975ND381432
cis-1,3-Dichloropropene ug/kg 975 43 23-15949 12 30975ND421473
Dibromochloromethane ug/kg 975 50 21-15158 16 30975ND487569
Dibromomethane ug/kg 975 59 38-15869 17 30975ND572675
Dichlorodifluoromethane ug/kg 975 43 10-20046 5 30975ND422445
Diisopropyl ether ug/kg 975 36 23-16040 10 30975ND350385
Ethylbenzene ug/kg 975 36 22-16343 16 309756.1J 361 422
Hexachloro-1,3-butadiene ug/kg 975 34 10-19235 1 30975ND334337
Isopropylbenzene
(Cumene)ug/kg 975 42 24-17347 12 30975ND406460
m&p-Xylene ug/kg 1950 39 22-17145 15 3019507.1J 765 888
Methyl-tert-butyl ether ug/kg 975 34 25-15344 28 30975ND327434
Methylene Chloride ug/kg R19753210-16545 33 30975ND310434
n-Butylbenzene ug/kg 975 29 10-18632 11 30975ND283315
n-Propylbenzene ug/kg 975 35 16-17140 13 30975ND340389
Naphthalene ug/kg R19752610-15911 67 3097528.3 278 139
o-Xylene ug/kg 975 44 23-17152 15 30975ND434504
p-Isopropyltoluene ug/kg 975 36 13-18438 7 30975ND350375
sec-Butylbenzene ug/kg 975 36 16-18240 10 30975ND356392
Styrene ug/kg 975 44 25-16951 14 30975ND433498
tert-Butylbenzene ug/kg 975 33 20-17437 10 30975ND326361
Tetrachloroethene ug/kg 975 37 14-17141 11 30975ND360401
Toluene ug/kg 975 44 24-16650 13 30975ND429487
trans-1,2-Dichloroethene ug/kg R19752724-17037 32 30975ND264364
trans-1,3-Dichloropropene ug/kg 975 41 22-15748 15 30975ND399463
Trichloroethene ug/kg 975 46 23-17652 13 30975ND445509
Trichlorofluoromethane ug/kg 975 19 10-13823 15 30975ND190221
Vinyl acetate ug/kg 1950 36 11-16641 13 301950ND697795
Vinyl chloride ug/kg 975 36 21-20042 17 30975ND347410
Xylene (Total)ug/kg 2920 41 23-17047 15 3029207.1J 1200 1390
1,2-Dichloroethane-d4 (S)%76 70-13078
4-Bromofluorobenzene (S)%94 70-13094
Toluene-d8 (S)%96 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
812545
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92697661001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4207194
Associated Lab Samples:92697661001
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 11/11/23 09:521.9
1,1,1-Trichloroethane ug/kg ND 5.0 11/11/23 09:522.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 11/11/23 09:521.3
1,1,2-Trichloroethane ug/kg ND 5.0 11/11/23 09:521.7
1,1-Dichloroethane ug/kg ND 5.0 11/11/23 09:522.1
1,1-Dichloroethene ug/kg ND 5.0 11/11/23 09:522.1
1,1-Dichloropropene ug/kg ND 5.0 11/11/23 09:522.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 11/11/23 09:524.0
1,2,3-Trichloropropane ug/kg ND 5.0 11/11/23 09:522.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 11/11/23 09:524.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 11/11/23 09:523.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 11/11/23 09:521.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 11/11/23 09:522.2
1,2-Dichlorobenzene ug/kg ND 5.0 11/11/23 09:521.8
1,2-Dichloroethane ug/kg ND 5.0 11/11/23 09:523.3
1,2-Dichloropropane ug/kg ND 5.0 11/11/23 09:521.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 11/11/23 09:521.7
1,3-Dichlorobenzene ug/kg ND 5.0 11/11/23 09:521.6
1,3-Dichloropropane ug/kg ND 5.0 11/11/23 09:521.6
1,4-Dichlorobenzene ug/kg ND 5.0 11/11/23 09:521.3
2,2-Dichloropropane ug/kg ND 5.0 11/11/23 09:523.8
2-Butanone (MEK)ug/kg ND 100 11/11/23 09:5224.0
2-Chlorotoluene ug/kg ND 5.0 11/11/23 09:521.8
2-Hexanone ug/kg ND 50.0 11/11/23 09:524.8
4-Chlorotoluene ug/kg ND 5.0 11/11/23 09:522.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 11/11/23 09:524.8
Acetone ug/kg ND 100 11/11/23 09:5232.1
Benzene ug/kg ND 5.0 11/11/23 09:522.0
Bromobenzene ug/kg ND 5.0 11/11/23 09:521.6
Bromochloromethane ug/kg ND 5.0 11/11/23 09:521.5
Bromodichloromethane ug/kg ND 5.0 11/11/23 09:521.9
Bromoform ug/kg ND 5.0 11/11/23 09:521.8
Bromomethane ug/kg ND 20.0 11/11/23 09:5215.5
Carbon tetrachloride ug/kg ND 5.0 11/11/23 09:521.9
Chlorobenzene ug/kg ND 5.0 11/11/23 09:522.9
Chloroethane ug/kg ND 10.0 11/11/23 09:523.9
Chloroform ug/kg ND 5.0 11/11/23 09:524.2
Chloromethane ug/kg ND 10.0 11/11/23 09:524.2
cis-1,2-Dichloroethene ug/kg ND 5.0 11/11/23 09:521.7
cis-1,3-Dichloropropene ug/kg ND 5.0 11/11/23 09:521.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4207194
Associated Lab Samples:92697661001
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 11/11/23 09:522.8
Dibromomethane ug/kg ND 5.0 11/11/23 09:521.1
Dichlorodifluoromethane ug/kg ND 10.0 11/11/23 09:525.1
Diisopropyl ether ug/kg ND 5.0 11/11/23 09:521.4
Ethylbenzene ug/kg ND 5.0 11/11/23 09:522.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 11/11/23 09:528.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 11/11/23 09:521.7
m&p-Xylene ug/kg ND 10.0 11/11/23 09:523.4
Methyl-tert-butyl ether ug/kg ND 5.0 11/11/23 09:521.9
Methylene Chloride ug/kg ND 20.0 11/11/23 09:5213.7
n-Butylbenzene ug/kg ND 5.0 11/11/23 09:523.2
n-Propylbenzene ug/kg ND 5.0 11/11/23 09:521.8
Naphthalene ug/kg ND 5.0 11/11/23 09:522.6
o-Xylene ug/kg ND 5.0 11/11/23 09:522.2
p-Isopropyltoluene ug/kg ND 5.0 11/11/23 09:522.5
sec-Butylbenzene ug/kg ND 5.0 11/11/23 09:522.2
Styrene ug/kg ND 5.0 11/11/23 09:521.3
tert-Butylbenzene ug/kg ND 5.0 11/11/23 09:521.8
Tetrachloroethene ug/kg ND 5.0 11/11/23 09:521.6
Toluene ug/kg ND 5.0 11/11/23 09:523.4
trans-1,2-Dichloroethene ug/kg ND 5.0 11/11/23 09:524.2
trans-1,3-Dichloropropene ug/kg ND 5.0 11/11/23 09:521.7
Trichloroethene ug/kg ND 5.0 11/11/23 09:524.0
Trichlorofluoromethane ug/kg ND 5.0 11/11/23 09:522.8
Vinyl acetate ug/kg ND 50.0 11/11/23 09:5210.3
Vinyl chloride ug/kg ND 10.0 11/11/23 09:522.5
Xylene (Total)ug/kg ND 10.0 11/11/23 09:522.8
1,2-Dichloroethane-d4 (S)%86 70-130 11/11/23 09:52
4-Bromofluorobenzene (S)%94 70-130 11/11/23 09:52
Toluene-d8 (S)%97 70-130 11/11/23 09:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4207195LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 539500 108 70-130
1,1,1-Trichloroethane ug/kg 514500 103 70-130
1,1,2,2-Tetrachloroethane ug/kg 535500 107 70-130
1,1,2-Trichloroethane ug/kg 536500 107 70-130
1,1-Dichloroethane ug/kg 487500 97 70-130
1,1-Dichloroethene ug/kg 518500 104 70-132
1,1-Dichloropropene ug/kg 516500 103 70-130
1,2,3-Trichlorobenzene ug/kg 463500 93 62-136
1,2,3-Trichloropropane ug/kg 515500 103 70-130
1,2,4-Trichlorobenzene ug/kg 447500 89 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4207195LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 453500 91 70-130
1,2-Dibromo-3-chloropropane ug/kg 574500 115 65-130
1,2-Dibromoethane (EDB)ug/kg 536500 107 70-130
1,2-Dichlorobenzene ug/kg 507500 101 70-130
1,2-Dichloroethane ug/kg 469500 94 70-130
1,2-Dichloropropane ug/kg 500500 100 70-130
1,3,5-Trimethylbenzene ug/kg 469500 94 70-130
1,3-Dichlorobenzene ug/kg 507500 101 70-130
1,3-Dichloropropane ug/kg 494500 99 70-130
1,4-Dichlorobenzene ug/kg 515500 103 70-130
2,2-Dichloropropane ug/kg 465500 93 60-130
2-Butanone (MEK)ug/kg 9161000 92 66-130
2-Chlorotoluene ug/kg 473500 95 70-130
2-Hexanone ug/kg 9981000 100 68-130
4-Chlorotoluene ug/kg 499500 100 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 9711000 97 70-130
Acetone ug/kg 8901000 89 60-130
Benzene ug/kg 515500 103 70-130
Bromobenzene ug/kg 531500 106 70-130
Bromochloromethane ug/kg 541500 108 70-130
Bromodichloromethane ug/kg 505500 101 70-130
Bromoform ug/kg 536500 107 70-130
Bromomethane ug/kg 496500 99 43-175
Carbon tetrachloride ug/kg 583500 117 70-130
Chlorobenzene ug/kg 526500 105 70-130
Chloroethane ug/kg 568500 114 70-145
Chloroform ug/kg 504500 101 70-130
Chloromethane ug/kg 526500 105 66-146
cis-1,2-Dichloroethene ug/kg 473500 95 70-130
cis-1,3-Dichloropropene ug/kg 512500 102 70-130
Dibromochloromethane ug/kg 530500 106 70-130
Dibromomethane ug/kg 590500 118 70-130
Dichlorodifluoromethane ug/kg 586500 117 42-197
Diisopropyl ether ug/kg 432500 86 68-130
Ethylbenzene ug/kg 500500 100 70-130
Hexachloro-1,3-butadiene ug/kg 582500 116 70-130
Isopropylbenzene (Cumene)ug/kg 497500 99 70-130
m&p-Xylene ug/kg 9741000 97 70-130
Methyl-tert-butyl ether ug/kg 456500 91 70-130
Methylene Chloride ug/kg 467500 93 65-130
n-Butylbenzene ug/kg 424500 85 70-130
n-Propylbenzene ug/kg 478500 96 70-130
Naphthalene ug/kg 409500 82 65-135
o-Xylene ug/kg 519500 104 70-130
p-Isopropyltoluene ug/kg 481500 96 70-130
sec-Butylbenzene ug/kg 478500 96 70-130
Styrene ug/kg 508500 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4207195LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 526500 105 70-130
Tetrachloroethene ug/kg 576500 115 70-130
Toluene ug/kg 505500 101 70-130
trans-1,2-Dichloroethene ug/kg 502500 100 70-130
trans-1,3-Dichloropropene ug/kg 509500 102 70-130
Trichloroethene ug/kg 558500 112 70-130
Trichlorofluoromethane ug/kg 563500 113 62-140
Vinyl acetate ug/kg 11001000 110 70-140
Vinyl chloride ug/kg 546500 109 70-152
Xylene (Total)ug/kg 14901500 100 70-130
1,2-Dichloroethane-d4 (S)%86 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4207196MATRIX SPIKE SAMPLE:
MSSpike
Result
92696830006
1,1,1,2-Tetrachloroethane ug/kg 268916 29 22-166ND
1,1,1-Trichloroethane ug/kg 283916 31 23-172ND
1,1,2,2-Tetrachloroethane ug/kg 701916 77 21-158ND
1,1,2-Trichloroethane ug/kg 300916 33 25-160ND
1,1-Dichloroethane ug/kg 304916 33 22-166ND
1,1-Dichloroethene ug/kg 338916 37 18-183ND
1,1-Dichloropropene ug/kg 298916 32 20-181ND
1,2,3-Trichlorobenzene ug/kg 401916 44 10-161ND
1,2,3-Trichloropropane ug/kg 294916 32 21-147ND
1,2,4-Trichlorobenzene ug/kg 274916 30 10-159ND
1,2,4-Trimethylbenzene ug/kg 254916 28 17-170ND
1,2-Dibromo-3-chloropropane ug/kg 319916 35 10-135ND
1,2-Dibromoethane (EDB)ug/kg 311916 34 30-154ND
1,2-Dichlorobenzene ug/kg 259916 28 26-162ND
1,2-Dichloroethane ug/kg 305916 33 23-161ND
1,2-Dichloropropane ug/kg 278916 30 29-165ND
1,3,5-Trimethylbenzene ug/kg 218916 24 20-172ND
1,3-Dichlorobenzene ug/kg 237916 26 22-164ND
1,3-Dichloropropane ug/kg 286916 31 27-156ND
1,4-Dichlorobenzene ug/kg 249916 27 20-161ND
2,2-Dichloropropane ug/kg 243916 27 10-159ND
2-Butanone (MEK)ug/kg 5951830 32 13-143ND
2-Chlorotoluene ug/kg 224916 24 21-166ND
2-Hexanone ug/kg 5441830 30 19-145ND
4-Chlorotoluene ug/kg 254916 28 19-163ND
4-Methyl-2-pentanone (MIBK)ug/kg 5391830 29 21-151ND
Acetone ug/kg 7171830 33 10-133114J
Benzene ug/kg 303916 33 29-156ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4207196MATRIX SPIKE SAMPLE:
MSSpike
Result
92696830006
Bromobenzene ug/kg 274916 30 25-161ND
Bromochloromethane ug/kg 343916 37 27-158ND
Bromodichloromethane ug/kg 273916 30 23-158ND
Bromoform ug/kg 273916 30 19-152ND
Bromomethane ug/kg 63.4 M1916710-152ND
Carbon tetrachloride ug/kg 274916 30 18-172ND
Chlorobenzene ug/kg 293916 32 26-166ND
Chloroethane ug/kg 63.3 M1916710-130ND
Chloroform ug/kg 308916 34 25-161ND
Chloromethane ug/kg 441916 48 27-197ND
cis-1,2-Dichloroethene ug/kg 314916 34 28-165ND
cis-1,3-Dichloropropene ug/kg 284916 31 23-159ND
Dibromochloromethane ug/kg 269916 29 21-151ND
Dibromomethane ug/kg 343 M19163738-158ND
Dichlorodifluoromethane ug/kg 369916 40 10-200ND
Diisopropyl ether ug/kg 231916 25 23-160ND
Ethylbenzene ug/kg 263916 28 22-1636.5J
Hexachloro-1,3-butadiene ug/kg 177916 19 10-192ND
Isopropylbenzene (Cumene)ug/kg 225916 25 24-173ND
m&p-Xylene ug/kg 5031830 27 22-17112.4J
Methyl-tert-butyl ether ug/kg 261916 28 25-153ND
Methylene Chloride ug/kg 435916 36 10-165102
n-Butylbenzene ug/kg 199916 22 10-186ND
n-Propylbenzene ug/kg 207916 23 16-171ND
Naphthalene ug/kg 192916 21 10-159ND
o-Xylene ug/kg 257916 28 23-171ND
p-Isopropyltoluene ug/kg 199916 22 13-184ND
sec-Butylbenzene ug/kg 186916 20 16-182ND
Styrene ug/kg 256916 28 25-169ND
tert-Butylbenzene ug/kg 185916 20 20-174ND
Tetrachloroethene ug/kg 259916 28 14-171ND
Toluene ug/kg 279916 29 24-16611.2
trans-1,2-Dichloroethene ug/kg 330916 36 24-170ND
trans-1,3-Dichloropropene ug/kg 282916 31 22-157ND
Trichloroethene ug/kg 304916 33 23-176ND
Trichlorofluoromethane ug/kg 87.1916 10 10-138ND
Vinyl acetate ug/kg 5951830 32 11-166ND
Vinyl chloride ug/kg 344916 38 21-200ND
Xylene (Total)ug/kg 7602750 27 23-17012.4J
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92696830007
4207197SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 76.8J 3096.5J
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92696830007
4207197SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 305.7J
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg 33.5 7 3031.3
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 308.9
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 305.7J
1,2-Dichloroethane-d4 (S)%8786
4-Bromofluorobenzene (S)%9697
Toluene-d8 (S)%9898
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
812422
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92697661006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4206537
Associated Lab Samples:92697661006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/11/23 01:000.31
1,1,1-Trichloroethane ug/L ND 1.0 11/11/23 01:000.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/11/23 01:000.22
1,1,2-Trichloroethane ug/L ND 1.0 11/11/23 01:000.32
1,1-Dichloroethane ug/L ND 1.0 11/11/23 01:000.37
1,1-Dichloroethene ug/L ND 1.0 11/11/23 01:000.35
1,1-Dichloropropene ug/L ND 1.0 11/11/23 01:000.43
1,2,3-Trichlorobenzene ug/L ND 1.0 11/11/23 01:000.81
1,2,3-Trichloropropane ug/L ND 1.0 11/11/23 01:000.26
1,2,4-Trichlorobenzene ug/L ND 1.0 11/11/23 01:000.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/11/23 01:000.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/11/23 01:000.27
1,2-Dichlorobenzene ug/L ND 1.0 11/11/23 01:000.34
1,2-Dichloroethane ug/L ND 1.0 11/11/23 01:000.32
1,2-Dichloropropane ug/L ND 1.0 11/11/23 01:000.36
1,3-Dichlorobenzene ug/L ND 1.0 11/11/23 01:000.34
1,3-Dichloropropane ug/L ND 1.0 11/11/23 01:000.28
1,4-Dichlorobenzene ug/L ND 1.0 11/11/23 01:000.33
2,2-Dichloropropane ug/L ND 1.0 11/11/23 01:000.39
2-Butanone (MEK)ug/L ND 5.0 v211/11/23 01:004.0
2-Chlorotoluene ug/L ND 1.0 11/11/23 01:000.32
2-Hexanone ug/L ND 5.0 11/11/23 01:000.48
4-Chlorotoluene ug/L ND 1.0 11/11/23 01:000.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/11/23 01:002.7
Acetone ug/L ND 25.0 v211/11/23 01:005.1
Benzene ug/L ND 1.0 11/11/23 01:000.34
Bromobenzene ug/L ND 1.0 11/11/23 01:000.29
Bromochloromethane ug/L ND 1.0 11/11/23 01:000.47
Bromodichloromethane ug/L ND 1.0 11/11/23 01:000.31
Bromoform ug/L ND 1.0 11/11/23 01:000.34
Bromomethane ug/L ND 2.0 v211/11/23 01:001.7
Carbon tetrachloride ug/L ND 1.0 11/11/23 01:000.33
Chlorobenzene ug/L ND 1.0 11/11/23 01:000.28
Chloroethane ug/L ND 1.0 11/11/23 01:000.65
Chloroform ug/L ND 1.0 11/11/23 01:000.43
Chloromethane ug/L ND 1.0 v211/11/23 01:000.54
cis-1,2-Dichloroethene ug/L ND 1.0 11/11/23 01:000.38
cis-1,3-Dichloropropene ug/L ND 1.0 11/11/23 01:000.36
Dibromochloromethane ug/L ND 1.0 11/11/23 01:000.36
Dibromomethane ug/L ND 1.0 11/11/23 01:000.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4206537
Associated Lab Samples:92697661006
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 11/11/23 01:000.35
Diisopropyl ether ug/L ND 1.0 v211/11/23 01:000.31
Ethylbenzene ug/L ND 1.0 11/11/23 01:000.30
Hexachloro-1,3-butadiene ug/L ND 2.0 11/11/23 01:001.5
m&p-Xylene ug/L ND 2.0 11/11/23 01:000.71
Methyl-tert-butyl ether ug/L ND 1.0 v211/11/23 01:000.42
Methylene Chloride ug/L ND 5.0 v211/11/23 01:002.0
Naphthalene ug/L ND 1.0 11/11/23 01:000.64
o-Xylene ug/L ND 1.0 11/11/23 01:000.34
p-Isopropyltoluene ug/L ND 1.0 11/11/23 01:000.41
Styrene ug/L ND 1.0 11/11/23 01:000.29
Tetrachloroethene ug/L ND 1.0 11/11/23 01:000.29
Toluene ug/L ND 1.0 11/11/23 01:000.24
trans-1,2-Dichloroethene ug/L ND 1.0 11/11/23 01:000.40
trans-1,3-Dichloropropene ug/L ND 1.0 11/11/23 01:000.36
Trichloroethene ug/L ND 1.0 11/11/23 01:000.38
Trichlorofluoromethane ug/L ND 1.0 11/11/23 01:000.30
Vinyl acetate ug/L ND 2.0 v211/11/23 01:001.3
Vinyl chloride ug/L ND 1.0 v211/11/23 01:000.39
Xylene (Total)ug/L ND 1.0 11/11/23 01:000.34
1,2-Dichloroethane-d4 (S)%98 70-130 11/11/23 01:00
4-Bromofluorobenzene (S)%99 70-130 11/11/23 01:00
Toluene-d8 (S)%98 70-130 11/11/23 01:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4206538LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 18.720 93 70-130
1,1,1-Trichloroethane ug/L 17.820 89 70-130
1,1,2,2-Tetrachloroethane ug/L 18.820 94 70-130
1,1,2-Trichloroethane ug/L 17.720 89 70-130
1,1-Dichloroethane ug/L 17.220 86 70-130
1,1-Dichloroethene ug/L 18.220 91 69-131
1,1-Dichloropropene ug/L 19.420 97 70-132
1,2,3-Trichlorobenzene ug/L 20.520 102 70-132
1,2,3-Trichloropropane ug/L 19.620 98 70-130
1,2,4-Trichlorobenzene ug/L 20.220 101 70-130
1,2-Dibromo-3-chloropropane ug/L 17.720 88 70-130
1,2-Dibromoethane (EDB)ug/L 19.220 96 70-130
1,2-Dichlorobenzene ug/L 19.920 100 70-130
1,2-Dichloroethane ug/L 17.320 87 70-130
1,2-Dichloropropane ug/L 17.720 88 70-130
1,3-Dichlorobenzene ug/L 20.120 101 70-130
1,3-Dichloropropane ug/L 18.820 94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4206538LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 20.220 101 70-130
2,2-Dichloropropane ug/L 17.020 85 69-130
2-Butanone (MEK)ug/L 31.1 v3407867-133
2-Chlorotoluene ug/L 20.020 100 70-130
2-Hexanone ug/L 35.140 88 70-133
4-Chlorotoluene ug/L 19.820 99 70-130
4-Methyl-2-pentanone (MIBK)ug/L 32.240 80 70-130
Acetone ug/L 30.0 v3407567-130
Benzene ug/L 18.620 93 70-130
Bromobenzene ug/L 19.220 96 70-130
Bromochloromethane ug/L 17.920 90 70-130
Bromodichloromethane ug/L 16.620 83 70-130
Bromoform ug/L 16.920 85 70-133
Bromomethane ug/L 15.2 v3207641-148
Carbon tetrachloride ug/L 19.720 98 70-130
Chlorobenzene ug/L 19.420 97 70-130
Chloroethane ug/L 16.620 83 41-157
Chloroform ug/L 17.220 86 70-130
Chloromethane ug/L 15.6 v3207859-141
cis-1,2-Dichloroethene ug/L 17.020 85 70-130
cis-1,3-Dichloropropene ug/L 16.920 85 70-130
Dibromochloromethane ug/L 17.320 87 70-130
Dibromomethane ug/L 18.020 90 70-130
Dichlorodifluoromethane ug/L 20.320 101 54-147
Diisopropyl ether ug/L 14.8 v3207470-130
Ethylbenzene ug/L 19.720 98 70-130
Hexachloro-1,3-butadiene ug/L 19.920 99 70-134
m&p-Xylene ug/L 38.840 97 70-130
Methyl-tert-butyl ether ug/L 15.8 v3207970-130
Methylene Chloride ug/L 15.9 v3207962-130
Naphthalene ug/L 21.420 107 70-135
o-Xylene ug/L 19.520 97 70-130
p-Isopropyltoluene ug/L 20.920 105 70-130
Styrene ug/L 18.820 94 70-130
Tetrachloroethene ug/L 20.720 104 70-130
Toluene ug/L 17.720 89 70-130
trans-1,2-Dichloroethene ug/L 17.220 86 70-130
trans-1,3-Dichloropropene ug/L 17.120 86 70-130
Trichloroethene ug/L 18.720 94 70-130
Trichlorofluoromethane ug/L 19.320 96 57-130
Vinyl acetate ug/L 30.5 v3407670-141
Vinyl chloride ug/L 15.4 v3207766-140
Xylene (Total)ug/L 58.260 97 70-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4206539MATRIX SPIKE SAMPLE:
MSSpike
Result
92696989001
1,1,1,2-Tetrachloroethane ug/L 21.020 105 70-146ND
1,1,1-Trichloroethane ug/L 21.320 107 70-150ND
1,1,2,2-Tetrachloroethane ug/L 20.520 102 66-144ND
1,1,2-Trichloroethane ug/L 19.420 97 70-142ND
1,1-Dichloroethane ug/L 19.420 97 68-150ND
1,1-Dichloroethene ug/L 21.120 105 64-162ND
1,1-Dichloropropene ug/L 23.120 115 70-160ND
1,2,3-Trichlorobenzene ug/L 24.520 122 66-151ND
1,2,3-Trichloropropane ug/L 20.620 103 66-144ND
1,2,4-Trichlorobenzene ug/L 24.520 122 69-147ND
1,2-Dibromo-3-chloropropane ug/L 18.520 92 62-146ND
1,2-Dibromoethane (EDB)ug/L 21.320 107 70-143ND
1,2-Dichlorobenzene ug/L 22.520 113 70-142ND
1,2-Dichloroethane ug/L 19.220 96 68-145ND
1,2-Dichloropropane ug/L 19.620 98 70-144ND
1,3-Dichlorobenzene ug/L 22.820 114 70-142ND
1,3-Dichloropropane ug/L 20.720 103 70-141ND
1,4-Dichlorobenzene ug/L 22.720 113 70-140ND
2,2-Dichloropropane ug/L 20.220 101 58-160ND
2-Butanone (MEK)ug/L 33.540 84 57-156ND
2-Chlorotoluene ug/L 23.120 116 70-148ND
2-Hexanone ug/L 37.340 93 62-153ND
4-Chlorotoluene ug/L 22.720 114 70-144ND
4-Methyl-2-pentanone (MIBK)ug/L 34.340 86 65-144ND
Acetone ug/L 32.340 81 49-162ND
Benzene ug/L 20.820 104 68-144ND
Bromobenzene ug/L 21.720 108 70-144ND
Bromochloromethane ug/L 20.120 101 70-148ND
Bromodichloromethane ug/L 18.420 92 70-141ND
Bromoform ug/L 18.720 93 59-144ND
Bromomethane ug/L 19.2 v3209623-190ND
Carbon tetrachloride ug/L 21.920 109 70-147ND
Chlorobenzene ug/L 21.920 110 70-143ND
Chloroethane ug/L 18.920 94 55-190ND
Chloroform ug/L 19.620 98 67-148ND
Chloromethane ug/L 16.320 82 38-180ND
cis-1,2-Dichloroethene ug/L 19.620 98 67-151ND
cis-1,3-Dichloropropene ug/L 19.120 95 70-142ND
Dibromochloromethane ug/L 19.720 98 68-140ND
Dibromomethane ug/L 20.320 101 70-142ND
Dichlorodifluoromethane ug/L 18.220 91 15-200ND
Diisopropyl ether ug/L 16.320 81 62-149ND
Ethylbenzene ug/L 22.220 111 70-145ND
Hexachloro-1,3-butadiene ug/L 25.120 125 64-164ND
m&p-Xylene ug/L 43.840 110 70-148ND
Methyl-tert-butyl ether ug/L 17.120 85 64-146ND
Methylene Chloride ug/L 17.620 88 54-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4206539MATRIX SPIKE SAMPLE:
MSSpike
Result
92696989001
Naphthalene ug/L 25.020 122 62-154ND
o-Xylene ug/L 21.620 108 70-145ND
p-Isopropyltoluene ug/L 25.120 126 70-153ND
Styrene ug/L 21.220 106 70-147ND
Tetrachloroethene ug/L 30.620 116 70-1457.3
Toluene ug/L 20.020 100 65-146ND
trans-1,2-Dichloroethene ug/L 19.620 98 69-155ND
trans-1,3-Dichloropropene ug/L 19.420 97 70-142ND
Trichloroethene ug/L 22.220 107 70-1520.79J
Trichlorofluoromethane ug/L 22.420 112 60-158ND
Vinyl acetate ug/L 33.3 v3408356-157ND
Vinyl chloride ug/L 17.320 86 51-178ND
Xylene (Total)ug/L 65.460 109 70-146ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92696989002
4206540SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92696989002
4206540SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L 3.0 4 303.1
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.79J 300.82J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 4.0 12 304.5
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND v230ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%9999
4-Bromofluorobenzene (S)%9898
Toluene-d8 (S)%10099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
812045
EPA 7199
EPA 7199
7199 Chromium, Hexavalent
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92697661001, 92697661002, 92697661003, 92697661004, 92697661005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4204525
Associated Lab Samples:92697661001, 92697661002, 92697661003, 92697661004, 92697661005
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg 0.071J 0.96 11/09/23 17:250.00096
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4204526LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.110 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4204527MATRIX SPIKE SAMPLE:
MSSpike
Result
92697269002
Chromium, Hexavalent mg/kg 15101490 101 75-1250.77J
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4204528MATRIX SPIKE SAMPLE:
MSSpike
Result
92697661002
Chromium, Hexavalent mg/kg 3.5 M112.2 27 75-1250.10J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
812661
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92697661001, 92697661002, 92697661003, 92697661004, 92697661005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4207829
Associated Lab Samples:92697661001, 92697661002, 92697661003, 92697661004, 92697661005
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 327 11/12/23 14:12129
1,2-Dichlorobenzene ug/kg ND 327 11/12/23 14:12118
1,3-Dichlorobenzene ug/kg ND 327 11/12/23 14:12116
1,4-Dichlorobenzene ug/kg ND 327 11/12/23 14:12125
1-Methylnaphthalene ug/kg ND 327 11/12/23 14:12115
2,2'-Oxybis(1-chloropropane)ug/kg ND 327 11/12/23 14:12155
2,4,5-Trichlorophenol ug/kg ND 327 11/12/23 14:12150
2,4,6-Trichlorophenol ug/kg ND 327 11/12/23 14:12135
2,4-Dichlorophenol ug/kg ND 327 11/12/23 14:12128
2,4-Dimethylphenol ug/kg ND 327 11/12/23 14:12136
2,4-Dinitrophenol ug/kg ND 1630 11/12/23 14:121010
2,4-Dinitrotoluene ug/kg ND 327 11/12/23 14:12126
2,6-Dinitrotoluene ug/kg ND 327 11/12/23 14:12120
2-Chloronaphthalene ug/kg ND 327 11/12/23 14:12130
2-Chlorophenol ug/kg ND 327 11/12/23 14:12123
2-Methylnaphthalene ug/kg ND 327 11/12/23 14:12131
2-Methylphenol(o-Cresol)ug/kg ND 327 11/12/23 14:12134
2-Nitroaniline ug/kg ND 1630 11/12/23 14:12267
2-Nitrophenol ug/kg ND 327 11/12/23 14:12142
3&4-Methylphenol(m&p Cresol)ug/kg ND 327 11/12/23 14:12132
3,3'-Dichlorobenzidine ug/kg ND 653 11/12/23 14:12221
3-Nitroaniline ug/kg ND 1630 11/12/23 14:12256
4,6-Dinitro-2-methylphenol ug/kg ND 653 11/12/23 14:12305
4-Bromophenylphenyl ether ug/kg ND 327 11/12/23 14:12126
4-Chloro-3-methylphenol ug/kg ND 653 11/12/23 14:12230
4-Chloroaniline ug/kg ND 653 11/12/23 14:12256
4-Chlorophenylphenyl ether ug/kg ND 327 11/12/23 14:12122
4-Nitroaniline ug/kg ND 653 11/12/23 14:12249
4-Nitrophenol ug/kg ND 1630 11/12/23 14:12632
Acenaphthene ug/kg ND 327 11/12/23 14:12115
Acenaphthylene ug/kg ND 327 11/12/23 14:12115
Aniline ug/kg ND 327 11/12/23 14:12128
Anthracene ug/kg ND 327 11/12/23 14:12107
Benzo(a)anthracene ug/kg ND 327 11/12/23 14:12109
Benzo(a)pyrene ug/kg ND 327 11/12/23 14:12113
Benzo(b)fluoranthene ug/kg ND 327 11/12/23 14:12109
Benzo(g,h,i)perylene ug/kg ND 327 11/12/23 14:12127
Benzo(k)fluoranthene ug/kg ND 327 11/12/23 14:12115
Benzoic Acid ug/kg ND 1630 11/12/23 14:12702
Benzyl alcohol ug/kg ND 653 11/12/23 14:12248
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4207829
Associated Lab Samples:92697661001, 92697661002, 92697661003, 92697661004, 92697661005
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 327 11/12/23 14:12136
bis(2-Chloroethyl) ether ug/kg ND 327 11/12/23 14:12123
bis(2-Ethylhexyl)phthalate ug/kg ND 327 11/12/23 14:12127
Butylbenzylphthalate ug/kg ND 327 11/12/23 14:12138
Chrysene ug/kg ND 327 11/12/23 14:12119
Di-n-butylphthalate ug/kg ND 327 11/12/23 14:12110
Di-n-octylphthalate ug/kg ND 327 11/12/23 14:12129
Dibenz(a,h)anthracene ug/kg ND 327 11/12/23 14:12126
Dibenzofuran ug/kg ND 327 11/12/23 14:12118
Diethylphthalate ug/kg ND 327 11/12/23 14:12120
Dimethylphthalate ug/kg ND 327 11/12/23 14:12119
Fluoranthene ug/kg ND 327 11/12/23 14:12112
Fluorene ug/kg ND 327 11/12/23 14:12115
Hexachloro-1,3-butadiene ug/kg ND 327 11/12/23 14:12142
Hexachlorobenzene ug/kg ND 327 11/12/23 14:12128
Hexachlorocyclopentadiene ug/kg ND 327 11/12/23 14:12187
Hexachloroethane ug/kg ND 327 11/12/23 14:12125
Indeno(1,2,3-cd)pyrene ug/kg ND 327 11/12/23 14:12129
Isophorone ug/kg ND 327 11/12/23 14:12146
N-Nitroso-di-n-propylamine ug/kg ND 327 11/12/23 14:12123
N-Nitrosodimethylamine ug/kg ND 327 11/12/23 14:12110
N-Nitrosodiphenylamine ug/kg ND 327 11/12/23 14:12116
Naphthalene ug/kg ND 327 11/12/23 14:12111
Nitrobenzene ug/kg ND 327 11/12/23 14:12151
Pentachlorophenol ug/kg ND 653 11/12/23 14:12320
Phenanthrene ug/kg ND 327 11/12/23 14:12107
Phenol ug/kg ND 327 11/12/23 14:12146
Pyrene ug/kg ND 327 11/12/23 14:12133
Pyridine ug/kg ND 327 11/12/23 14:12103
2,4,6-Tribromophenol (S)%55 10-130 11/12/23 14:12
2-Fluorobiphenyl (S)%56 10-130 11/12/23 14:12
2-Fluorophenol (S)%61 10-130 11/12/23 14:12
Nitrobenzene-d5 (S)%63 10-130 11/12/23 14:12
Phenol-d6 (S)%61 10-130 11/12/23 14:12
Terphenyl-d14 (S)%78 10-130 11/12/23 14:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4207830LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 9641640 59 40-130
1,2-Dichlorobenzene ug/kg 9551640 58 37-130
1,3-Dichlorobenzene ug/kg 9451640 58 36-130
1,4-Dichlorobenzene ug/kg 9401640 57 36-130
1-Methylnaphthalene ug/kg 10801640 66 46-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4207830LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 10601640 65 12-130
2,4,5-Trichlorophenol ug/kg 9881640 60 49-130
2,4,6-Trichlorophenol ug/kg 9761640 60 48-130
2,4-Dichlorophenol ug/kg 10301640 63 45-130
2,4-Dimethylphenol ug/kg 10701640 65 45-130
2,4-Dinitrophenol ug/kg 45008200 55 23-130
2,4-Dinitrotoluene ug/kg 10601640 65 50-130
2,6-Dinitrotoluene ug/kg 10701640 65 53-130
2-Chloronaphthalene ug/kg 9561640 58 46-130
2-Chlorophenol ug/kg 10201640 63 39-130
2-Methylnaphthalene ug/kg 10801640 66 45-130
2-Methylphenol(o-Cresol)ug/kg 10401640 63 38-130
2-Nitroaniline ug/kg 20303280 62 43-130
2-Nitrophenol ug/kg 10601640 65 43-130
3&4-Methylphenol(m&p Cresol)ug/kg 10301640 63 34-130
3,3'-Dichlorobenzidine ug/kg 2060 L232806368-130
3-Nitroaniline ug/kg 18703280 57 36-130
4,6-Dinitro-2-methylphenol ug/kg 22303280 68 38-130
4-Bromophenylphenyl ether ug/kg 11501640 70 52-130
4-Chloro-3-methylphenol ug/kg 21903280 67 45-130
4-Chloroaniline ug/kg 21603280 66 41-130
4-Chlorophenylphenyl ether ug/kg 10601640 65 46-130
4-Nitroaniline ug/kg 19403280 59 40-130
4-Nitrophenol ug/kg 50208200 61 34-130
Acenaphthene ug/kg 10701640 65 47-130
Acenaphthylene ug/kg 10801640 66 50-130
Aniline ug/kg 10101640 62 33-130
Anthracene ug/kg 11801640 72 46-130
Benzo(a)anthracene ug/kg 11601640 71 49-130
Benzo(a)pyrene ug/kg 10401640 63 45-130
Benzo(b)fluoranthene ug/kg 10101640 62 45-130
Benzo(g,h,i)perylene ug/kg 10801640 66 44-130
Benzo(k)fluoranthene ug/kg 10801640 66 46-130
Benzoic Acid ug/kg 22608200 28 14-130
Benzyl alcohol ug/kg 20903280 64 39-130
bis(2-Chloroethoxy)methane ug/kg 10701640 65 41-130
bis(2-Chloroethyl) ether ug/kg 10301640 63 34-130
bis(2-Ethylhexyl)phthalate ug/kg 13901640 85 39-130
Butylbenzylphthalate ug/kg 13201640 80 48-130
Chrysene ug/kg 12301640 75 50-130
Di-n-butylphthalate ug/kg 12201640 75 46-130
Di-n-octylphthalate ug/kg 13801640 84 49-130
Dibenz(a,h)anthracene ug/kg 10401640 64 46-130
Dibenzofuran ug/kg 10501640 64 49-130
Diethylphthalate ug/kg 11001640 67 49-130
Dimethylphthalate ug/kg 10501640 64 50-130
Fluoranthene ug/kg 11601640 71 49-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4207830LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 11101640 68 47-130
Hexachloro-1,3-butadiene ug/kg 9831640 60 36-130
Hexachlorobenzene ug/kg 10901640 67 52-130
Hexachlorocyclopentadiene ug/kg 7761640 47 10-130
Hexachloroethane ug/kg 9551640 58 36-130
Indeno(1,2,3-cd)pyrene ug/kg 10501640 64 44-130
Isophorone ug/kg 11501640 70 40-130
N-Nitroso-di-n-propylamine ug/kg 10901640 67 34-130
N-Nitrosodimethylamine ug/kg 9831640 60 29-130
N-Nitrosodiphenylamine ug/kg 11601640 71 47-130
Naphthalene ug/kg 10901640 67 43-130
Nitrobenzene ug/kg 10601640 65 41-130
Pentachlorophenol ug/kg 18803280 57 35-130
Phenanthrene ug/kg 12001640 73 50-130
Phenol ug/kg 11001640 67 39-130
Pyrene ug/kg 12701640 77 51-130
Pyridine ug/kg 8361640 51 21-130
2,4,6-Tribromophenol (S)%69 10-130
2-Fluorobiphenyl (S)%60 10-130
2-Fluorophenol (S)%62 10-130
Nitrobenzene-d5 (S)%67 10-130
Phenol-d6 (S)%65 10-130
Terphenyl-d14 (S)%75 10-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4207831MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697661002
4207832
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 2020 38 22-13042 302010NDND833J
1,2-Dichlorobenzene ug/kg 2020 41 22-13044 302010ND823J885J
1,3-Dichlorobenzene ug/kg 2020 41 22-13043 302010ND823J871J
1,4-Dichlorobenzene ug/kg 2020 40 21-13043 302010ND802J872J
1-Methylnaphthalene ug/kg 2020 42 27-13048 302010ND847J967J
2,2'-Oxybis(1-
chloropropane)ug/kg 2020 49 10-13055 302010ND990J1100J
2,4,5-Trichlorophenol ug/kg 2020 37 18-13041 302010NDNDND
2,4,6-Trichlorophenol ug/kg 2020 38 17-13039 302010NDNDND
2,4-Dichlorophenol ug/kg 2020 37 19-13044 302010NDND880J
2,4-Dimethylphenol ug/kg 2020 22 17-13024 302010NDNDND
2,4-Dinitrophenol ug/kg 10100 19 10-13022 3010000NDNDND
2,4-Dinitrotoluene ug/kg 2020 36 31-13043 302010NDND857J
2,6-Dinitrotoluene ug/kg 2020 39 33-13044 302010ND794J887J
2-Chloronaphthalene ug/kg 2020 38 26-13040 302010NDND808J
2-Chlorophenol ug/kg 2020 43 19-13048 302010ND864J957J
2-Methylnaphthalene ug/kg 2020 43 26-13046 302010ND864J928J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4207831MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697661002
4207832
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Methylphenol(o-Cresol)ug/kg 2020 34 19-13038 302010NDNDND
2-Nitroaniline ug/kg 4040 42 29-13045 304010ND1710J1810J
2-Nitrophenol ug/kg 2020 42 16-13045 302010NDND906J
3&4-Methylphenol(m&p
Cresol)ug/kg 2020 35 14-13038 302010NDNDND
3,3'-Dichlorobenzidine ug/kg 4040 30 16-13033 304010NDNDND
3-Nitroaniline ug/kg 4040 36 28-13041 304010NDND1630J
4,6-Dinitro-2-methylphenol ug/kg 4040 33 10-13136 304010NDNDND
4-Bromophenylphenyl ether ug/kg 2020 41 32-13047 302010ND826J933J
4-Chloro-3-methylphenol ug/kg 4040 40 26-13046 304010ND1630J1840J
4-Chloroaniline ug/kg 4040 35 19-13039 304010NDNDND
4-Chlorophenylphenyl ether ug/kg 2020 37 29-13042 302010ND751J835J
4-Nitroaniline ug/kg 4040 32 22-13036 304010NDNDND
4-Nitrophenol ug/kg 10100 30 10-13039 3010000NDND3880J
Acenaphthene ug/kg 2020 42 29-13045 302010ND839J899J
Acenaphthylene ug/kg 2020 43 27-13046 302010ND869J929J
Aniline ug/kg 2020 27 10-13026 302010NDNDND
Anthracene ug/kg 2020 44 26-13049 302010ND894J988J
Benzo(a)anthracene ug/kg 2020 36 31-13041 302010ND941J1030J
Benzo(a)pyrene ug/kg 2020 37 24-13045 302010ND738J894J
Benzo(b)fluoranthene ug/kg 2020 40 12-13743 302010ND804J870J
Benzo(g,h,i)perylene ug/kg 2020 41 16-13045 302010ND831J908J
Benzo(k)fluoranthene ug/kg 2020 34 27-13039 302010NDND792J
Benzoic Acid ug/kg M110100710-13010 3010000NDNDND
Benzyl alcohol ug/kg 4040 43 25-13044 304010ND1730J1750J
bis(2-
Chloroethoxy)methane ug/kg 2020 46 26-13052 302010ND934J1050J
bis(2-Chloroethyl) ether ug/kg 2020 43 23-13047 302010ND863J944J
bis(2-Ethylhexyl)phthalate ug/kg 2020 50 20-13053 302010ND1020J1070J
Butylbenzylphthalate ug/kg 2020 50 28-13052 302010ND1010J1040J
Chrysene ug/kg 2020 49 29-13055 302010ND983J1100J
Di-n-butylphthalate ug/kg 2020 42 29-13047 302010ND854J941J
Di-n-octylphthalate ug/kg 2020 50 30-13051 302010ND1010J1030J
Dibenz(a,h)anthracene ug/kg 2020 33 27-13033 302010NDNDND
Dibenzofuran ug/kg 2020 39 33-13043 302010ND791J854J
Diethylphthalate ug/kg 2020 41 34-13047 302010ND825J940J
Dimethylphthalate ug/kg 2020 42 35-13047 302010ND850J946J
Fluoranthene ug/kg 2020 33 26-13040 302010ND1030J1170J
Fluorene ug/kg 2020 41 27-13045 302010ND829J893J
Hexachloro-1,3-butadiene ug/kg 2020 37 19-13040 302010NDNDND
Hexachlorobenzene ug/kg 2020 38 31-13044 302010NDND891J
Hexachlorocyclopentadiene ug/kg 2020 12 10-13012 302010NDNDND
Hexachloroethane ug/kg 2020 40 21-13043 302010ND812J866J
Indeno(1,2,3-cd)pyrene ug/kg 2020 37 16-13043 302010NDND863J
Isophorone ug/kg 2020 50 29-13055 302010ND1020J1100J
N-Nitroso-di-n-propylamine ug/kg 2020 50 22-13055 302010ND1010J1100J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4207831MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697661002
4207832
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodimethylamine ug/kg 2020 37 15-13040 302010ND749J793J
N-Nitrosodiphenylamine ug/kg 2020 43 30-13048 302010ND877J966J
Naphthalene ug/kg 2020 46 24-13049 302010ND920J985J
Nitrobenzene ug/kg 2020 45 25-13048 302010NDND966J
Pentachlorophenol ug/kg 4040 28 10-13036 304010NDNDND
Phenanthrene ug/kg 2020 50 28-13057 302010ND1010J1150J
Phenol ug/kg 2020 42 18-13047 302010NDND940J
Pyrene ug/kg 2020 43 27-13049 302010ND1220J1330J
Pyridine ug/kg 2020 39 10-13039 302010ND788J773J
2,4,6-Tribromophenol (S)%41 10-13045
2-Fluorobiphenyl (S)%43 10-13044
2-Fluorophenol (S)%39 10-13038
Nitrobenzene-d5 (S)%D34910-13049
Phenol-d6 (S)%41 10-13044
Terphenyl-d14 (S)%45 10-13041
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92697661
71227190
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
812157
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92697661001, 92697661002, 92697661003, 92697661004, 92697661005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92697068001
4205285SAMPLE DUPLICATE:
Percent Moisture %12.5 N212512.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92697178001
4205286SAMPLE DUPLICATE:
Percent Moisture %41.6 N2172535.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 61
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92697661
71227190
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 61
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92697661
71227190
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92697661001 812045 812240CS-02 EPA 7199 EPA 7199
92697661002 812045 812240CS-03 EPA 7199 EPA 7199
92697661003 812045 812240CS-04 EPA 7199 EPA 7199
92697661004 812045 812240CS-05 EPA 7199 EPA 7199
92697661005 812045 812240CS-DUP-02 EPA 7199 EPA 7199
92697661001 813148 813230CS-02 EPA 3050B EPA 6010D
92697661002 813148 813230CS-03 EPA 3050B EPA 6010D
92697661003 813148 813230CS-04 EPA 3050B EPA 6010D
92697661004 813148 813230CS-05 EPA 3050B EPA 6010D
92697661005 813148 813230CS-DUP-02 EPA 3050B EPA 6010D
92697661001 813005 813137CS-02 EPA 7471B EPA 7471B
92697661002 813005 813137CS-03 EPA 7471B EPA 7471B
92697661003 813005 813137CS-04 EPA 7471B EPA 7471B
92697661004 813005 813137CS-05 EPA 7471B EPA 7471B
92697661005 813005 813137CS-DUP-02 EPA 7471B EPA 7471B
92697661001 812661 812725CS-02 EPA 3546 EPA 8270E
92697661002 812661 812725CS-03 EPA 3546 EPA 8270E
92697661003 812661 812725CS-04 EPA 3546 EPA 8270E
92697661004 812661 812725CS-05 EPA 3546 EPA 8270E
92697661005 812661 812725CS-DUP-02 EPA 3546 EPA 8270E
92697661001 812545 812735CS-02 EPA 5035A/5030B EPA 8260D
92697661002 812291 812440CS-03 EPA 5035A/5030B EPA 8260D
92697661003 812291 812440CS-04 EPA 5035A/5030B EPA 8260D
92697661004 812291 812440CS-05 EPA 5035A/5030B EPA 8260D
92697661005 812291 812440CS-DUP-02 EPA 5035A/5030B EPA 8260D
92697661006 812422EB-02 EPA 8260D
92697661001 812157CS-02 SW-846
92697661002 812157CS-03 SW-846
92697661003 812157CS-04 SW-846
92697661004 812157CS-05 SW-846
92697661005 812157CS-DUP-02 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 61
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Page 61 of 61

APPENDIX D
Soil Export Weigh Tickets