FA-3028_29244_CA_IAR_20230707

UST Closure and Initial Abatement Action Report July 7, 2023 i
SITE INFORMATION
1.Site Identification
Date of Report: July 7, 2023
Site Name: Love’s Travel Stop #412
Site Street Address: 3948 Hodges Chapel Road, Harnett County, NC
Geographical Data Point: Former UST Basin
GPS/confirmed with Google Earth
Latitude 35o 20’ 23.99” N and Longitude 78o 33’ 26.10’W
A site location map is included as Figure 1 to this report.
2.Information about Contacts Associated with the Leaking UST System
UST Owner/Operator: Love’s Travel Stops & Country Stores
10601 North Pennsylvania Avenue
Oklahoma City, Oklahoma 73120
Phone: [phone]
Secondary Responsible Party: Pilot Travel Centers, LLC
5508 Lonas Road
Knoxville, Tennessee 37939
Phone: [phone]
Property Owner: Love’s Travel Stops & Country Stores
10601 North Pennsylvania Avenue
Oklahoma City, Oklahoma 73120
Phone: [phone]
Property Occupant: Love’s Travel Stops & Country Stores
10601 North Pennsylvania Avenue
Oklahoma City, Oklahoma 73120
Phone: [phone]
Consultant/Contractor: Apex Companies, LLC
203 Wylderose Court
Midlothian, Virginia 23113
Phone: [phone]
Analytical Laboratory: Pace Analytical
9800 Kincey Avenue, Suite 100
Huntersville, North Carolina 28078
Phone: [phone]
Analytical Laboratory: Red Lab, LLC
105 Portwatch Way, Suite F
Wilmington, North Carolina 28412
Phone: [phone]
UST Closure and Initial Abatement Action Report July 7, 2023 iii
EXECUTIVE SUMMARY
On behalf of Love’s and Pilot, Apex has completed UST Closure and IAA Report
activities at Love’s Travel Stop #412. In accordance with NC DEQ regulatory reporting
requirements, Apex has prepared this UST Closure and IAA Report for the subject property
located at 3948 Hodges Chapel Road in Dunn, Harnett County, North Carolina.
Prior to UST closure activities, three active NC DEQ incident numbers have been
documented at the site including Incident #16993, Incident #29244, and Incident #29985. Former
owner Speedway (owner from 1987 to September 1, 2001) is listed as the responsible party for
Incident #16993. Pilot purchased the property from Speedway on September 1, 2001 and
assumed responsibility for the old incident numbers in early 2013. Under the ownership of Pilot,
a release was identified on September 22, 2004 (Incident #29244) following the detection of
free-phase petroleum product in UST basin observation well OBS-2. Pilot sold the property to
Love’s on July 19, 2010. The current Love’s Incident #29985, reported on March 31, 2016, is
the result of diesel fuel detected on the concrete surface cover in the vicinity of the most eastern
master dispenser at the truck fueling island. Upon further inspection, it was found that diesel
fuel was released to the subsurface following removal of the dispenser and surface
components/cover. In accordance with December 11, 2017, NCDEQ documentation, both the
Pilot Incident #29244 and the Love’s Incident #29985 have been combined and classified as a
comingled release.
Apex completed removal from the ground eight USTs and the non-regulated oil/water
separator. In addition to the UST removal, Apex removed both the auto and diesel fuel canopies,
fuel dispensers and fuel lines. The USTs consisted of two 20,000-gallon diesel fuel USTs, one
20,000-gallon biodiesel UST, one 10,000-gallon diesel fuel UST, two 10,000-gallon gasoline
USTs, one 8,000-gallon diesel exhaust fluid UST, and one 4,000-gallon gasoline UST at the
Love’s Travel Stop and Country Store #412 facility.
In addition to UST closure activities, Apex over excavated impacted soil associated with
the releases documented in 2004 and 2016. A total of 4,439.06 tons of petroleum contaminated
soil were excavated and hauled offsite for proper disposal during this phase. Prior to UST
removal, the USTs were cleaned using high-pressured water and a vacuum truck. A total of
14,259 gallons of remaining UST products, sludge, and tank cleaning rinsate were evacuated
from the USTs, fuel lines, and dispensers and transported offsite for proper disposal at EVO
Corporation. Additionally, 7,603 gallons of free product and water were recovered from water
within the tank basin during soil excavation activities and hauled offsite for proper disposal.
During UST removal activities, monitoring well MW-1 was abandoned due to its location within
the former tank basin and over-excavation of petroleum-impacted soil.
In accordance with NC DEQ guidelines, Apex collected 204 soil samples for total
petroleum hydrocarbons (TPH) diesel range organics and TPH gasoline range organics analyses
for submittal to Pace Analytical (20 soil samples) and onsite analysis by Red Lab Rapid
Environmental Diagnostics (184 soil samples) during the over-excavation of petroleum-impacted
soil. Additionally, a total of 16 risk-based post-excavation soil samples submitted to Pace for
volatile organic compound and semi-volatile organic compound analysis. Post-excavation soil
UST Closure and Initial Abatement Action Report July 7, 2023 iv
sampling of the basin and sidewalls yielded concentrations below commercial/industrial
Maximum Soil Contaminant Concentration Levels, indicating successful removal of petroleum-
impacted soil at the site. Free-phase petroleum product and groundwater were encountered
during UST removal. As noted above, free product was removed using a vacuum truck during
the over excavation of impacted soil from the tank basins. Based on the removal of the USTs
from the site, free product removal, and post-excavation soil sample analytical results, Apex
recommends replacement of monitoring well MW-1 and any additional wells that may be
damaged or destroyed during site redevelopment activities. Apex also recommends sampling of
all onsite monitoring wells to evaluate whether onsite groundwater concentrations are below NC
DEQ gross contaminant levels (GCLs). If petroleum concentrations in onsite monitoring wells
are confirmed to be below GCLs, Apex recommends no further action.
UST Closure and Initial Abatement Action Report July 7, 2023 v
TABLE OF CONTENTS
A.SITE HISTORY AND CHARACTERIZATION .............................................................. 3
1. UST Owner and Operator Information ............................................................................... 1 
2. UST Information ................................................................................................................. 2 
3.Non-UST Information ......................................................................................................... 2 
4.Description of the Release .................................................................................................. 2 
5.Site Characteristics .............................................................................................................. 3 
6.Summary ............................................................................................................................. 4
B.SITE CHECK REPORT ...................................................................................................... 4
1.Tank and Line Tightness Testing ........................................................................................ 4 
2.Site Check Procedure .......................................................................................................... 4 
3.Initial Response Actions ..................................................................................................... 4 
4. Soil Excavation Activities ................................................................................................... 4 
5.Site Investigation ................................................................................................................ 4 
6. Conclusions and Recommendations ................................................................................... 4
C.UST CLOSURE REPORT ................................................................................................... 5
1. Preparations for Closure ..................................................................................................... 5 
2. Closure Procedure ............................................................................................................... 5 
3. Residual Material ................................................................................................................ 6 
4.Initial Response ................................................................................................................... 6 
5. Soil Excavation ................................................................................................................... 6 
6.Site Investigation ................................................................................................................ 6 
7. Conclusions and Recommendations ................................................................................... 7
D.NAPL INVESTIGATION AND FREE PRODUCT RECOVERY REPORT ................ 7
1.Current and Historical Status .............................................................................................. 7 
2.On-Site or Off-Site Effluent Discharges ............................................................................. 7 
3. Recovery Technologies ....................................................................................................... 8 
4. Conclusions and Recommendations ................................................................................... 8
E.GROUNDWATER AND SURFACE WATER INVESTIGATION ................................ 8
1. Actions Taken ..................................................................................................................... 8 
2. Groundwater and Surface Water Investigations ................................................................. 8
F.INITIAL RESPONSE AND ABATEMENT ACTION ..................................................... 8
1.Initial Response ................................................................................................................... 8
UST Closure and Initial Abatement Action Report July 7, 2023 vi
TABLE OF CONTENTS (Cont'd.)
2. Initial Abatement Actions ................................................................................................... 8
G.EXCAVATION OF CONTAMINATED SOIL ................................................................. 8
1.Source and Estimated Extent .............................................................................................. 8 
2.Excavation Process ............................................................................................................. 9 
3.Post-Excavation .................................................................................................................. 9 
4. Soil Investigation ................................................................................................................ 9 
5.Disposal of Contaminated Soil ......................................................................................... 10 
6.Conclusions ....................................................................................................................... 10
H.CONCLUSIONS ................................................................................................................. 10 
FIGURES
Figure 1 Site Location
Figure 2 Site Plan
Figure 3 Petroleum Impacted Soil Excavation Map (4/28/2023)
Figure 4 Petroleum Impacted Soil Excavation Map (5/4/2023)
Figure 5 Petroleum Impacted Soil Excavation Map (5/5/2023)
Figure 6 Petroleum Impacted Soil Excavation Map (5/9/2023)
Figure 7 Petroleum Impacted Soil Excavation Map (5/11/2023)
Figure 8 Post-Excavation Risk-Based Sample Location Map
TABLES
Table 1 Soil TPH GRO/DRO Analytical Results
Table 2 Soil VOC/SVOC Analytical Results
Table 3 Groundwater VOC/SVOC Analytical Results
APPENDICES
Appendix A UST-3 Notice of Intent: UST Permanent Closure or Change-in-Service
Appendix B Harnett County Fire Marshal Permit Inspection Forms
Appendix C Non-Hazardous Liquid Waste Manifests
Appendix D UST Disposal Certificates
Appendix E Laboratory Certificates of Analysis and Chain of Custody Records
Appendix F Non-Hazardous Soil Waste Manifests

UST Closure and Initial Abatement Action Report July 7, 2023 1
A. SITE HISTORY AND CHARACTERIZATION

1. UST Owner and Operator Information

Name Of Current Owner/Operator Dates of Operation
Love’s Travel Stops & Country Stores July 2010 – Present
Street Address
10601 North Pennsylvania Avenue
City State Zip Telephone Number
Oklahoma City OK 73120 405-751-9000

Name of Previous Owners Dates of Operation
Speedway 1987 – September 2001
Pilot Travel Centers, LLC September 2001 – July 2010
Incident Number Responsible Party Date of Release
16993 Speedway November 21, 1996
29244 Pilot Travel Centers, LLC September 22, 2004
29985 Love’s Travel Stops March 31, 2016

UST Closure and Initial Abatement Action Report July 7, 2023 2
2. UST Information

UST
ID #
Current/
Last
Contents
Capacity
(gallons)
Construction
Details
Tank
Dimension
Description of
Associated
Piping
& Pumps
Date
Tank
Installed1
Status of
UST
Tank 1 Diesel 20,000 Steel (FC)
(SW) STIP3 120” x 34’ SW FRP 1987
Removed
from
Ground
Tank 2 Diesel 20,000 Steel (FC)
(SW) STIP3 120” x 34’ SW FRP 1987
Removed
from
Ground
Tank 3 Biodiesel 20,000 Fiberglass
(DW) 120” x 34’ SW FRP 2015
Removed
from
Ground
Tank 4 Diesel 10,000 Steel (FC)
(SW) STIP3 96” x 26’ SW FRP 1987
Removed
from
Ground
Tank 5 Gasoline 10,000 Steel (FC)
(SW) STIP3 96” x 26’ SW FRP 1987
Removed
from
Ground
Tank 6 Gasoline 10,000 Steel (FC)
(SW) STIP3 96” x 26’ SW FRP 1987
Removed
from
Ground
Tank 7
Diesel
Exhaust
Fluid
8,000 Fiberglass
(DW) 96” x 21’ DW FRP 2012
Removed
from
Ground
Tank 8 Gasoline 4,000 Steel (FC)
(SW) STIP3 60” x 24’ SW FRP 1987
Removed
from
Ground
Tank 9 Gasoline 4,000 Steel (FC)
(SW) STIP3 60” x 24’ SW FRP 1987
Removed
from
Ground

3. Non-UST Information

Not Applicable (NA)

4. Description of the Release

Three active North Carolina Department of Environmental Quality (NC
DEQ) incident numbers (Incident #16993, Incident #29244, and Incident #29985)
have been documented at the site. Former owner Speedway (owner/operator from
1987 to September 1, 2001) is listed as the responsible party for Incident #16993
(opened on November 21, 1996). Pilot Travel Centers, LLC (Pilot) purchased the
property from Speedway on September 1, 2001 and assumed responsibility for the
old incident number in 2013. Under the ownership of Pilot, a release was
identified on September 22, 2004 (Incident #29244) following the detection of
free-phase petroleum product in UST basin observation well OBS-2. Pilot sold the

UST Closure and Initial Abatement Action Report July 7, 2023 3
property to Love’s Travel Stops, LLC (Love’s) on July 19, 2010. The most
current Incident #29985 was reported on March 31, 2016 and is the result of a
leaking flex line inside the easternmost master diesel fuel dispenser at the truck
fueling island. In accordance with NC DEQ documentation dated December 11,
2017, all three active incident numbers have been combined and addressed as a
comingled release.

5. Site Characteristics

The site is located in a commercial/lightly residential area of Dunn,
Harnett County, North Carolina directly adjacent to Interstate 95. The property is
currently owned and operated by Love’s. The facility is provided potable water
and sewer services by the Harnett County Department of Public Utilities
municipal system. The site location is presented on Figure 1.

The site is currently undergoing active redevelopment. Future site
improvements include a new store building, new gasoline and diesel fuel
dispenser islands, new UST systems, concrete/asphalt access/parking areas, and
utilities. The site is bound to the north and west by Interstate 95, beyond which
are commercial properties. To the east of the site is Hodges Chapel Road, beyond
which is open farmland. Small commercial developments abut the site to the
south. The majority of area residences and businesses obtain potable water from
the Harnett County Department of Public Utilities municipal system.

During Comprehensive Site Assessment (CSA) activities in
October/November 2011, Apex identified six in-use potable supply wells within
1,500 feet of the subject site. The nearest identified supply well is associated with
the Black’s Tire and Auto Service facility addressed as 4064 Hodges Chapel Road
and located approximately 560 feet south-southeast of the former Love’s Travel
Stop #412 UST basin. Based on an interview with the Black’s Tire and Auto
Service owner performed by NC DEQ, the supply well was confirmed to no
longer be used for potable water and therefore NC DEQ revised the site ranking
from high to intermediate. A site plan depicting pertinent features of the site is
provided as Figure 2.

According to the U.S. Geological Survey 7.5-minute topographic map of
the Dunn Quadrangle, North Carolina (1997), the approximate site elevation is
240 feet above mean sea level. Site topography is characterized by low relief
sloping to the northwest. The nearest surface water body is Town Creek located
approximately 1,500 feet to the northwest from the former diesel fuel UST basin.

According to the U.S. Department of Agriculture (USDA) Online Soil
Survey of Harnett County, North Carolina, soils in the vicinity of the former UST
basin are classified under two soil types, Coxville loam to the southwest and
Norfolk loamy sand to the northeast of the site. Coxville loam is described as
“well drained soils that have a moderately high available water capacity consists

UST Closure and Initial Abatement Action Report July 7, 2023 4
of zero to two percent slope and consists of dominantly sandy clay. Norfolk
loamy sand is described as “well drained soils that have a moderately high to high
available water capacity consists of zero to two percent slope and consists of
dominantly sandy clay loam. UST closure activities indicated pea gravel and fill
material such as fine-grained clay mixed with loamy sand throughout the
excavation and excavation sidewalls. Groundwater was encountered in the former
UST basin during UST closure activities.

6. Summary

Three active NC DEQ incident numbers (#16993, #29244, and #29985)
are associated with the site. The site is currently classified by the NC DEQ as
intermediate risk. The site is currently undergoing active redevelopment and is
served with potable water and sewer services by the Harnett County Department
of Public Utilities municipal system. During UST closure activities in April/May
2023, nine USTs and the associated fuel lines and dispensers were removed.

B. Site Check Report

1. Tank and Line Tightness Testing

NA

2. Site Check Procedure

NA

3. Initial Response Actions

NA

4. Soil Excavation Activities

NA

5. Site Investigation

NA

6. Conclusions and Recommendations

NA

UST Closure and Initial Abatement Action Report July 7, 2023 5
C. UST Closure Report

1. Preparations for Closure

On March 10, 2023, Apex submitted Form UST-3 Notice of Intent: UST
Permanent Closure or Change-in-Service to NC DEQ. Additionally, Apex
contacted the Harnett County Fire Marshal’s Office prior to UST closure
activities and obtained a permit for UST removal. Apex also notified the North
Carolina One-Call service to locate and mark underground utilities prior to UST
closure activities. A copy of the completed Form UST-3 is provided in Appendix
A. Copies of the Harnett County Fire Marshal permit inspection forms for UST
removal are provided in Appendix B.

2. Closure Procedure

On April 17, 2023 Apex mobilized to the site with its partner, Evo
Corporation (EVO), to perform UST removal and site closure activities. Fuel
dispenser canopies and associated surface components such as fuel dispensers and
concrete/asphalt surface cover were removed prior to removal of the USTs.

Prior to removal of the tank systems, the USTs were degassed with dry ice
and cleaned using high pressure water and a vacuum truck to remove residual
product in the tanks. The fuel lines were purged from the dispenser sumps back to
the tanks to remove any residual product in the fuel lines. Approximately 14,259
gallons of residual product, tank rinsate, and sludge were evacuated from the
USTs, lines and dispensers and transported offsite to EVO in Winston-Salem,
North Carolina for proper disposal. Copies of the non-hazardous waste manifests
for the transportation and disposal of recovered liquids/sludge are provided in
Appendix C.

The USTs were removed after cleaning and placed on flat bed trailers for
transportation and disposal. Apex did not observe any corrosion, pitting, or holes
on any of the USTs. A representative of the Harnett County Fire Marshal’s Office
was present during UST removal activities. Seven steel USTs were transported to
Dunn Scrap and Iron in Dunn, North Carolina for proper disposal and recycling.
The fiberglass biodiesel UST and the fiberglass diesel exhaust fluid UST were
transported to GFL Environmental in Roseboro, North Carolina for proper
disposal. Copies of the UST disposal certificates are provided as Appendix D.

During UST closure activities, Apex did not observe any indications of a
new release from the USTs; however, visible free product in groundwater and
petroleum-impacted soil within the UST basin excavation were observed. The
presence of free product and petroleum-impacted soil was likely associated with
the former documented petroleum releases. An additional 7,603 gallons of free
product and petroleum-impacted groundwater were recovered from the tank basin
excavation and transported offsite for disposal at EVO. Copies of the non-

UST Closure and Initial Abatement Action Report July 7, 2023 6
hazardous waste manifests for the transportation and disposal of recovered free
product/petroleum-impacted groundwater are provided in Appendix C.

Based on discussions with NC DEQ and real-time sampling data collected
during excavation activities, a total of 3,682.04 tons of petroleum-impacted soil
was approved by NC DEQ for removal/disposal during UST removal activities.
An additional total of 757.02 tons of petroleum-impacted soil (not directed by NC
DEQ) and associated with UST overburden and considered unsuitable for re-use
was excavated from the tank basin area and dispenser islands (gasoline and diesel)
and transported offsite for disposal. During UST removal activities, monitoring
well MW-1 was abandoned due to its location within the former tank basin and
over-excavation of petroleum-impacted soil. Confirmation sampling was
performed during excavation activities to determine eligibility of petroleum-
impacted soil for NC DEQ-approved removal/disposal. Figure 3 through Figure
7 document relevant petroleum concentrations detected in soil and evaluated by
Apex and DEQ during soil over excavation activities.

In accordance with NC DEQs Guidelines for Site Checks, Tank Closure,
and Initial Response and Abatement for UST Releases, Apex collected a total of
16 risk-based soil samples at the prescribed intervals following post-excavation
activities. Apex collected 11 soil samples from the sidewalls of the tank basin just
above groundwater. The other five soil samples were collected from the four
sidewalls and the base of the excavation associated with the diesel fuel dispenser
release that occurred in 2016. Risk-based soil sample locations were based on
discussions with NC DEQ and selected to document post-excavation soil
concentrations. Samples were not collected from beneath the USTs due to the
presence of groundwater. Per discussions with NC DEQ personnel, soil samples
were not collected from beneath the product lines or the dispenser’s following
removal. Post-excavation soil sample locations are provided on Figure 8.

3. Residual Material

Described above in C.2.

4. Initial Response

Refer to Section F.

5. Soil Excavation

Refer to Section G.

6. Site Investigation

In accordance with NC DEQ guidelines, Apex collected 204 soil samples
during the excavation of impacted soil and 16 risk-based post-excavation soil

UST Closure and Initial Abatement Action Report July 7, 2023 7
samples following the removal of soil with significant petroleum impact. Figure 3
through Figure 7 document significant petroleum concentrations detected in soil
during excavation activities. Post-excavation soil sample locations are depicted on
Figure 8.

The soil samples were labeled and stored on ice in their respective
laboratory grade approved containers pending delivery to an independent
laboratory. A total of 20 soil samples were submitted to Pace Analytical (Pace) in
Raleigh, North Carolina for total petroleum hydrocarbon (TPH) diesel range
organics (DRO) and TPH gasoline range organics (GRO) analyses via method
SW846 method 8015C. An additional 16 soil samples were submitted to Pace for
volatile organic compound (VOC) and semi-volatile organic compound (SVOC)
analysis via U.S. EPA SW846 method 8260 and 8270, respectively. A total of 184
soil samples were also analyzed onsite by Red Lab Rapid Environmental
Diagnostics (Red Lab) for TPH DRO and TPH GRO analyses via method SW846
method 8015C. Strict sample security and chain-of-custody documentation were
observed during all phases of transport. Petroleum compounds were identified in
all soil samples submitted for laboratory analyses. TPH DRO and TPH GRO were
detected at maximum concentrations of 43,804 parts per million (ppm) and 9,704
ppm in soil samples 42423490-26 and 42423490-030, respectively. Soil sample
analytical results collected during excavation activities are summarized in Table
1. Post-excavation soil sample analytical results are summarized in Table 2. The
laboratory Certificate of Analysis and chain-of-custody records are provided in
Appendix E.

7. Conclusions and Recommendations

Apex has completed removal of nine USTs and associated system
components at the Love’s 412 facility. Petroleum compounds were identified in
all confirmation soil samples submitted for laboratory analyses during excavation
of petroleum-impacted soil encountered during UST closure activities. Apex
worked closely with NC DEQ the UST closure activities to determine appropriate
abatement actions including the removal of petroleum-impacted soil that was
contributing to the presence of free product at the site. Decisions made by Apex
and NC DEQ during the process were intended to move the site’s active incident
numbers toward closure.

D. NAPL Investigation and Free Product Recovery Report

1. Current and Historical Status

NA

2. On-Site or Off-Site Effluent Discharges

NA

UST Closure and Initial Abatement Action Report July 7, 2023 8

3. Recovery Technologies

NA

4. Conclusions and Recommendations

NA

E. Groundwater and Surface Water Investigation

1. Actions Taken

NA

2. Groundwater and Surface Water Investigations

NA

F. Initial Response and Abatement Action

1. Initial Response

In accordance with NC DEQ guidelines and based on site redevelopment
activities including UST closure, NC DEQ approved the excavation and disposal
of petroleum-impacted soil and groundwater associated with prior petroleum
releases onsite to promote a path forward for closure of the active NC DEQ
incident numbers associated with the site.

2. Initial Abatement Actions

Refer to Section G.

G. Excavation of Contaminated Soil

1. Source and Estimated Extent

During UST Closure activities, Apex detected both visual and olfactory
evidence of the previously documented petroleum releases at the site. Apex did
not observe indications of a new release from the UST systems as no corrosion,
pitting, or holes were observed in the USTs or product lines removed; however,
petroleum-impacted soil and visible free product was confirmed within the UST
basin excavation, Soil analytical results are documented in Table 1. Soil sample
locations are presented on Figure 3 through Figure 8.

UST Closure and Initial Abatement Action Report July 7, 2023 9
2. Excavation Process

In accordance with NC DEQ requirements, Apex performed excavation of
petroleum-impacted soil following UST closure. Apex over-excavated the tank
basin in order to remove soil with significant petroleum impact. Apex utilized
Red Lab to perform real-time analysis of petroleum-impacted soil in addition to a
PID to determine the extent of over-excavation activities. The excavation for the
tank basin measured approximately 85 feet wide by 121 feet long and ranged in
depth from 10 feet to 14 feet deep. The excavation addressing the diesel fuel
dispenser release that occurred in 2016 measured approximately 26 feet wide by
35 feet long by nine feet deep. A total of 4,439.06 tons of petroleum-impacted soil
was removed from the excavations and hauled offsite for proper disposal.
Excavation activities were limited vertically by groundwater encountered in the
tank basins and horizontally when field observations indicated significant
reduction in petroleum-impacted soil concentrations. Groundwater and free-phase
petroleum product were encountered during over-excavation activities. Free phase
petroleum product was skimmed from the surface water within the tank basin on
four occasions with a vacuum truck. A total of 7,603 gallons of free-phase
petroleum product and petroleum-impacted groundwater was recovered from
surface water within the basin. One groundwater sample (a total of four) was
collected for each load of liquids recovered by the vacuum truck from the
excavation and transported offsite for disposal. Groundwater samples were
submitted to Pace for volatile and semi-volatile analysis via U.S. EPA SW846
method 6200B and 625. A summary of groundwater analytical data is included in
Table 3. The laboratory Certificate of Analysis and chain-of-custody
documentation are included as Appendix E.

3. Post-Excavation

In accordance with NC DEQ regulations and based on discussions with
NC DEQ, risk-based post-excavation soil samples were collected from the basin
(10.0 feet below ground surface) and sidewalls (seven to eight feet below ground
surface) of the over-excavation. Soil sample locations are depicted on Figure 8.

4. Soil Investigation

The soil samples were labeled and stored on ice in their respective
laboratory grade approved containers pending delivery to an independent
laboratory. The soil samples were submitted to Pace for VOC analysis via U.S.
EPA SW-846 method 8260B and SVOC analyses via U.S. EPA method 8270
analysis. Strict sample security and chain-of-custody documentation were
observed during all phases of transport. Petroleum compounds were identified in
all post-excavation samples; however, all petroleum concentrations detected are
significantly less than the NC DEQ Maximum Soil Contaminant Concentration
Levels (MSCCs) for commercial/industrial sites. Post-excavation samples
indicated a significant reduction in petroleum concentrations detected in onsite

UST Closure and Initial Abatement Action Report July 7, 2023 10
soil. Soil sample analytical results are summarized in Table 1 and Table 2. The
soil laboratory Certificate of Analysis and chain-of-custody records are provided
in Appendix E. Photographic documentation of the UST closure and soil
excavation activities is provided as Appendix F.

5. Disposal of Contaminated Soil

A total of 4,439.06 tons of petroleum-impacted soil was removed from the
excavations and transported offsite for disposal. Of the total volume of soil
removed for disposal, 3,682.04 tons was approved by NC DEQ for
removal/disposal and the remaining 757.02 tons (not directed by NC DEQ) was
associated with UST overburden and considered unsuitable for re-use. All soil
was transported offsite for disposal under non-hazardous waste manifest to EVO
in Winston-Salem, North Carolina, E S & J Enterprise Inc in Autryville, North
Carolina, and Triangle Area Earth Corporation in Zebulon, North Carolina. At the
conclusion of excavation activities, EVO backfilled the excavation with clean
stone and fill to ground surface. Copies of the certificate of disposal and non-
hazardous waste manifests/weight tickets are provided in Appendix G.

6. Conclusions

A total of 4,439.06 tons of petroleum contaminated soil were removed
from the excavation for proper disposal during this phase. Petroleum compounds
were identified in all post-excavation samples; however, all petroleum
concentrations detected are significantly less than the NC DEQ MSCCs for
commercial/industrial sites. Post-excavation samples indicated a successful
reduction of petroleum contaminated soil at the site.

H. Conclusions

Apex has completed removal of nine USTs and associated fuel lines and dispensers at the
Love’s Travel Stop and Country Store # 412 facility in Dunn, North Carolina. Based on
documented incident reports for the site. Apex excavated a total of 4,439.06 tons of petroleum
contaminated soil from the site. Post-excavation sampling yielded concentrations below MSCCs
for commercial/industrial sites. Approximately 7,603 gallons of free-phase petroleum product
and groundwater were recovered from surface water within the basin during this phase. Based
on the removal of the USTs from the site, free product removal, and post-excavation soil sample
analytical results, Apex recommends replacement of monitoring well MW-1 and any additional
wells that may be damaged or destroyed during site redevelopment activities. Apex also
recommends sampling of all onsite monitoring wells to evaluate whether onsite groundwater
concentrations are below NC DEQ gross contaminant levels (GCLs). If petroleum
concentrations in onsite monitoring wells are confirmed to be below GCLs, Apex recommends
no further action.

FIGURES
FIGURE 1
Site Location Map
Love’s Travel Stop #412
3948 Hodges Chapel Road
Dunn, Harnett County, North Carolina
APEX COMPANIES, LLC.
203 WYLDEROSE COURT
MIDLOTHIAN, VIRGINIA 23113
[phone]
DUNN, NORTH CAROLINA
Source: U.S.G.S. Topographic Map of the
Dunn Quadrangle, North Carolina,
7.5 Minute Series (1997)
Scale: 1:24,000 Contour Interval: 10 Feet
Vertical Datum: National Geodetic
Vertical Datum 1929
Horizontal Datum: North American Datum1927
Project: UST Closure Report
Latitude:
035O 20’ 24.31” N
Longitude:
-078O 33’ 25.83” W
Client: Love’s Travel Stops
Apex Job #: 23004903
Date: June 2023
SITE
REV
0
Site Plan
Love's Travel Stop #412
3948 Hodges Chapel Road
Dunn, Harnett County, North Carolina
DRAWING TITLE
DRAWING NUMBER
FIGURE No. 2BY DATEREV
DR.: CMR
CK.:
APP'D.: CLC
SCALE: 1" = 40'
APEX PROJ. NO.: 23004903
GRAPHIC SCALE
1" = 40'NEW
40'0'20'40'60'80'DATE: June 2023 Truck
Parking
Truck
Parking Truck
ParkingTruck
Parking www.apexcos.com
UST Closure
and
Initial
Abatement
Action Report
Love's Travel Stop
#412
OBS-2OBS-1 MW-1
Truck Dispenser
Islands
Diesel Canopy
Auto Dispenser
Islands
HODGES CHAPEL
ROAD
HODGES CHAPEL
ROAD
MW-4
Closed MW-3
MW-2
MW-5
MW-6
Closed
U
U
U
Auto Canopy
DEFMW-L3
MW-L1
MW-L2
Dispenser
Release
Location
BioDieselPremiumGasolineGasoline DieselDieselDieselMW-L4
Oil Water
Separator
17
18 19 20
21 22 23
24 25
APEX COMPANIES, LLC.
203 WYLDEROSE COURT
MIDLOTHIAN, VIRGINIA 23113
[phone]
U
Monitoring Well Locations
LEGEND
Catch Basin
Utility Pole
Overhead Electrical
REV
0
Petroleum Impacted Soil Excavation Map (4/28/23)
Love's Travel Stop #412
3948 Hodges Chapel Road
Dunn, Harnett County, North Carolina
DRAWING TITLE
DRAWING NUMBER
FIGURE No. 3BY DATEREV
DR.: CMR
CK.:
APP'D.: CLC
SCALE: 1" = 40'
APEX PROJ. NO.: 23004903
GRAPHIC SCALE
1" = 40'NEW
40'0'20'40'60'80'DATE: June 2023 www.apexcos.com
UST Closure
and
Initial
Abatement
Action Report
Love's Travel Stop
#412
MW-1 (Free product present)
HODGES CHAPEL
ROAD
HODGES CHAPEL
ROAD
MW-3 MW-2
MW-5
U
U
MW-L3 MW-L1
MW-L2
Dispenser
Release
Location
MW-L4
425234903-52
DRO - 2,296
GRO - 208.6
425234903-53
DRO - 20,884 ppm
GRO - 2,506 ppm
Gasoline and Diesel
Basin
Biodiesel Basin
DEF
Basin
426234903-56
DRO - 21,936 ppm
GRO - 3,991 ppm
426234903-59
DRO - 6,706 ppm
GRO - 1,567 ppm
Sanitary
Sewer
426234903-69
DRO - 11,270
GRO - 1,904
426234903-71
DRO - 8,157 ppm
GRO - 1,197 ppm
424234903-35
DRO - 5,322 ppm
GRO - <61.6 ppm
425234903-37
DRO - 18,959 ppm
GRO - 3,155 ppm
427234903-77
DRO - 10,769 ppm
GRO - 1,926 ppm
427234903-73
DRO - 4,098 ppm
GRO - 602.5 ppm
420234903-16
Pending analytical
from offsite lab
420234903-18
Pending analytical
from offsite lab
427234903-75
DRO - 21,542 ppm
GRO - 2,643 ppm
Avg. DRO 8,666 ppm
Avg. GRO 1,372 ppm
Avg. DRO 14,649 ppm
Avg. GRO 2,089 ppm
Avg. DRO & GRO
Additional data pending offsite
laboratory analytical results DEF Basin
Dispenser Release
Avg. DRO 8,201 ppm
Avg. GRO 1,214 ppm
426234903-63
DRO - 79.8
GRO - 10.4
*All numerical data presented by Red Labs mobile laboratory
APEX COMPANIES, LLC.
203 WYLDEROSE COURT
MIDLOTHIAN, VIRGINIA 23113(804) 897-2718
Truck Dispenser
Islands
Diesel Canopy
Auto Dispenser
Islands
Auto Canopy
U
Monitoring Well Locations
Soil Sample Locations
Limits of Excavation
Sanitary Sewer
LEGEND
Catch Basin
U Utility Pole
Overhead Electrical
Demolished Structure
REV
0
DRAWING TITLE
DRAWING NUMBER
FIGURE No. 4BY DATEREV
DR.: CMR
CK.:
APP'D.: CLC
SCALE: 1" = 40'
APEX PROJ. NO.: 23004903
GRAPHIC SCALE
1" = 40'NEW
40'0'20'40'60'80'DATE: June 2023 www.apexcos.com
Petroleum Impacted Soil Excavation Map (5/4/23)
Love's Travel Stop #412
3948 Hodges Chapel Road
Dunn, Harnett County, North Carolina
UST Closure
and
Initial
Abatement
Action Report
Love's Travel Stop
#412
MW-1 (Removed)
HODGES CHAPEL
ROAD
HODGES CHAPEL
ROAD
MW-3 MW-2
MW-5
U
U
MW-L3 MW-L1
MW-L2
Dispenser
Release
Location
MW-L4
52234903-95
DRO - 4,143
GRO - 5,320
54234903-131
DRO - 8,481 ppm
GRO - 1,169 ppm
Gasoline and Diesel
Basin
Biodiesel Basin
DEF
Basin
54234903-134
DRO - 5,101 ppm
GRO - 712.8 ppm
54234903-135
DRO - 19,477 ppm
GRO - 3,647 ppm
Sanitary
Sewer
53234903-116
DRO - 537.7
GRO - 44.3
Post-Excavation
52234903-96
DRO - 1,977 ppm
GRO - 664.2 ppm
52234903-93
DRO - 303 ppm
GRO - 42.0 ppm
Post-Excavation
53234903-115
DRO - 1,685 ppm
GRO - 181 ppm
420234903-16
DRO - 6,830 ppm
GRO - 387 ppm
420234903-18
DRO - 5,480 ppm
GRO - 311 ppm
5234903-92
DRO - 1,286 ppm
GRO - 474.7 ppm
Post-Excavation
Avg. DRO - 4,853 ppm
Avg. GRO - 317.3
*All numerical data presented by Red Labs mobile laboratory and Pace Analytial.
54234903-133
DRO - 1,900 ppm
GRO - 253 ppm
Blue shaded area has been excavated to a
final depth of approximately 10' BGS
(Limited due to groundwater)
Green shaded area has been
excavated to a depth ranging from
approximately 4-5' BGS. Additional
excavation is needed in this area to
remove impacted soil with visible
staining.
52234903-90
DRO - 61.6 ppm
GRO - 27.7 ppm
Post-Excavation
52234903-91
DRO - 47.5 ppm
GRO - 5.8 ppm
Post-Excavation
Biodiesel tank pit required addition
excavation due to free product being
trapped in the backfill and
surrounding soil.
Yellow shaded area has been
excavated to a depth of
approximately 14' BGS. The diesel
side of the basin has only been
excavated to approximately 11' BGS.
The gasoline and diesel basin is
currently under water.
APEX COMPANIES, LLC.
203 WYLDEROSE COURTMIDLOTHIAN, VIRGINIA 23113(804) 897-2718
Truck Dispenser
Islands
Diesel Canopy
Auto Dispenser
Islands
Auto Canopy
U
Monitoring Well Locations
Soil Sample Locations
Limits of Excavation
Sanitary Sewer
LEGEND
Catch Basin
U Utility Pole
Overhead Electrical
Demolished Structure
REV
0
DRAWING TITLE
DRAWING NUMBER
FIGURE No. 5BY DATEREV
DR.: CMR
CK.:
APP'D.: CLC
SCALE: 1" = 40'
APEX PROJ. NO.: 23004903
GRAPHIC SCALE
1" = 40'NEW
40'0'20'40'60'80'DATE: June 2023 www.apexcos.com
UST Closure
and
Initial
Abatement
Action Report
Petroleum Impacted Soil Excavation Map (5/5/23)
Love's Travel Stop #412
3948 Hodges Chapel Road
Dunn, Harnett County, North Carolina
Love's Travel Stop
#412
MW-1 (Removed)
HODGES CHAPEL
ROAD
HODGES CHAPEL
ROAD
MW-3 MW-2
MW-5
U
MW-L3 MW-L1
MW-L2
Dispenser
Release
Location
MW-L4
52234903-94
DRO - 4,143
GRO - 5,320
55234903-1348
DRO - 331 ppm
GRO - 66.0 ppm
Gasoline and Diesel
Basin
DEF
Basin
55234903-145
DRO - 8,071 ppm
GRO - 1,191 ppm
55234903-142
DRO - 1,753 ppm
GRO - 237 ppm
Sanitary
Sewer
53234903-116
DRO - 537.7
GRO - 44.3
Post-Excavation
52234903-96
DRO - 1,977 ppm
GRO - 664.2 ppm
52234903-93
DRO - 303 ppm
GRO - 42.0 ppm
Post-Excavation
53234903-115
DRO - 1,685 ppm
GRO - 181 ppm
420234903-16
DRO - 6,830 ppm
GRO - 387 ppm
420234903-18
DRO - 5,480 ppm
GRO - 311 ppm
5234903-92
DRO - 1,286 ppm
GRO - 474.7 ppm
Post-Excavation
Avg. DRO - 4,853 ppm
Avg. GRO - 317.3
*All numerical data presented by Red Labs mobile laboratory and Pace Analytial.
55234903-147
DRO - 1,952 ppm
GRO - 361 ppm
Blue shaded area has been excavated to a
final depth of approximately 10' BGS
(Limited due to groundwater)
Green shaded area has been
excavated to a depth ranging from
approximately 4-5' BGS. Additional
excavation is needed in this area to
remove impacted soil with visible
staining.
52234903-90
DRO - 61.6 ppm
GRO - 27.7 ppm
Post-Excavation
52234903-91
DRO - 47.5 ppm
GRO - 5.8 ppm
Post-Excavation
Biodiesel tank pit required addition
excavation due to free product being
trapped in the backfill and
surrounding soil.
Yellow shaded area has been
excavated to a depth of
approximately 14' BGS. The diesel
side of the basin has only been
excavated to approximately 11' BGS.
The gasoline and diesel basin is
currently under water.
55234903-146
DRO - 7,986 ppm
GRO - 2,190 ppm
55234903-144
DRO - 8,827 ppm
GRO - 1,566 ppm
55234903-143
DRO - 6,970 ppm
GRO - 966 ppm
Red shaded area has not been excavated
and will likely require removal.
APEX COMPANIES, LLC.
203 WYLDEROSE COURT
MIDLOTHIAN, VIRGINIA 23113(804) 897-2718
Truck Dispenser
Islands
Diesel Canopy
Auto Dispenser
Islands
Auto Canopy
U
U
Monitoring Well Locations
Soil Sample Locations
Limits of Excavation
Sanitary Sewer
LEGEND
Catch Basin
U Utility Pole
Overhead Electrical
Demolished Structure
Biodiesel Basin
UST Closure
and
Initial
Abatement
Action Report REV
0
DRAWING TITLE
DRAWING NUMBER
FIGURE No. 6BY DATEREV
DR.: CMR
CK.:
APP'D.: CLC
SCALE: 1" = 40'
APEX PROJ. NO.: 23004903
GRAPHIC SCALE
1" = 40'NEW
40'0'20'40'60'80'DATE: 5/9/2023 www.apexcos.com
Petroleum Impacted Soil Excavation Map (5/9/23)
Love's Travel Stop #412
3948 Hodges Chapel Road
Dunn, Harnett County, North Carolina
Gasoline and Diesel
BasinBlue shaded areas have been fully
excavated and require no additional
excavation.
Love's Travel Stop
#412
MW-1 (Removed)
HODGES CHAPEL
ROAD
HODGES CHAPEL
ROAD
MW-3 MW-2
MW-5
U
U
MW-L3 MW-L1
MW-L2
Dispenser
Release
Location
MW-L4
52234903-94
DRO - 4,143
GRO - 5,320
55234903-1348
DRO - 331 ppm
GRO - 66.0 ppm
Biodiesel Basin
DEF
Basin
55234903-145
DRO - 8,071 ppm
GRO - 1,191 ppm
55234903-142
DRO - 1,753 ppm
GRO - 237 ppm
Sanitary
Sewer
52234903-96
DRO - 1,977 ppm
GRO - 664.2 ppm
52234903-93
DRO - 303 ppm
GRO - 42.0 ppm
Post-Excavation
53234903-115
DRO - 1,685 ppm
GRO - 181 ppm
59234903-196
DRO - 2,598 ppm
GRO - 274.2 ppm
420234903-199
DRO - 1,510 ppm
GRO - 126.2 ppm
5234903-92
DRO - 1,286 ppm
GRO - 474.7 ppm
Post-Excavation
Avg. DRO - 4,853 ppm
Avg. GRO - 317.3
*All numerical data presented by Red Labs mobile laboratory and Pace Analytial.
55234903-147
DRO - 1,952 ppm
GRO - 361 ppm
Yellow shaded area has been excavated to
a depth of approximately 6'-10' BGS and
could use additional excavation to remove
soil that may be trapping free product based
on analytical data and visual free product
on surface water in the DEF basin.
Green shaded areas could use
additional excavation to remove
impacted soil based on analytical
data and visible staining.
52234903-90
DRO - 61.6 ppm
GRO - 27.7 ppm
Post-Excavation
52234903-91
DRO - 47.5 ppm
GRO - 5.8 ppm
Post-Excavation
55234903-146
DRO - 7,986 ppm
GRO - 2,190 ppm
55234903-144
DRO - 8,827 ppm
GRO - 1,566 ppm
55234903-143
DRO - 6,970 ppm
GRO - 966 ppm
Red shaded area has not been excavated
and will likely require removal based on
analytical data.
59234903-198
DRO - 4,364 ppm
GRO - 437.7 ppm
420234903-197
DRO -9,432 ppm
GRO - 1,286 ppm
59234903-201
DRO - 17,595 ppm
GRO - 2,159 ppm
59234903-195
DRO - 9,261 ppm
GRO - 1,103 ppm
59234903-200
DRO - 3,167 ppm
GRO - 306.6 ppm
Red dotted line shows the
current limits of excavation
APEX COMPANIES, LLC.
203 WYLDEROSE COURT
MIDLOTHIAN, VIRGINIA 23113(804) 897-2718
Truck Dispenser
Islands
Diesel Canopy
Auto Dispenser
Islands
Auto Canopy
U
Monitoring Well Locations
Soil Sample Locations
Limits of Excavation
Sanitary Sewer
LEGEND
Catch Basin
U Utility Pole
Overhead Electrical
Demolished Structure
REV
0
DRAWING TITLE
DRAWING NUMBER
FIGURE No. 7BY DATEREV
DR.: CMR
CK.:
APP'D.: CLC
SCALE: 1" = 40'
APEX PROJ. NO.: 23004903
GRAPHIC SCALE
1" = 40'NEW
40'0'20'40'60'80'DATE: June 2023 www.apexcos.com
UST Closure
and
Initial
Abatement
Action Report
Petroleum Impacted Soil Excavation Map (5/11/23)
Love's Travel Stop #412
3948 Hodges Chapel Road
Dunn, Harnett County, North Carolina Gasoline and Diesel
BasinBlue shaded areas have been fully
excavated and require no additional
excavation.
Love's Travel Stop
#412
MW-1 (Removed)
HODGES CHAPEL
ROAD
HODGES CHAPEL
ROAD
MW-3 MW-2
MW-5
U
U
MW-L3 MW-L1
MW-L2
Dispenser
Release
Location
MW-L4
52234903-94
DRO - 4,143
GRO - 5,320
55234903-1348
DRO - 331 ppm
GRO - 66.0 ppm
Biodiesel Basin
DEF
Basin
55234903-145
DRO - 8,071 ppm
GRO - 1,191 ppm
55234903-142
DRO - 1,753 ppm
GRO - 237 ppm
Sanitary
Sewer
52234903-96
DRO - 1,977 ppm
GRO - 664.2 ppm
52234903-93
DRO - 303 ppm
GRO - 42.0 ppm
Post-Excavation
53234903-115
DRO - 1,685 ppm
GRO - 181 ppm
59234903-196
DRO - 2,598 ppm
GRO - 274.2 ppm
420234903-199
DRO - 1,510 ppm
GRO - 126.2 ppm
5234903-92
DRO - 1,286 ppm
GRO - 474.7 ppm
Post-Excavation
Avg. DRO - 4,853 ppm
Avg. GRO - 317.3
*All numerical data presented by Red Labs mobile laboratory and Pace Analytial.
55234903-147
DRO - 1,952 ppm
GRO - 361 ppm
52234903-90
DRO - 61.6 ppm
GRO - 27.7 ppm
Post-Excavation
52234903-91
DRO - 47.5 ppm
GRO - 5.8 ppm
Post-Excavation
55234903-146
DRO - 7,986 ppm
GRO - 2,190 ppm
55234903-144
DRO - 8,827 ppm
GRO - 1,566 ppm
55234903-143
DRO - 6,970 ppm
GRO - 966 ppm
59234903-198
DRO - 4,364 ppm
GRO - 437.7 ppm 420234903-197
DRO -9,432 ppm
GRO - 1,286 ppm
59234903-212
DRO - 1,423 ppm
GRO - 177.4 ppm
59234903-195
DRO - 9,261 ppm
GRO - 1,103 ppm
59234903-200
DRO - 3,167 ppm
GRO - 306.6 ppm
Red dotted line shows the
limits of excavation
APEX COMPANIES, LLC.
203 WYLDEROSE COURTMIDLOTHIAN, VIRGINIA 23113(804) 897-2718
Truck Dispenser
Islands
Diesel Canopy
Auto Dispenser
Islands
Auto Canopy
U
Monitoring Well Locations
Soil Sample Locations
Limits of Excavation
Sanitary Sewer
LEGEND
Catch Basin
U Utility Pole
Overhead Electrical
Demolished Structure
REV
0
Post-Excavation Risk-Based Sample Location Map
Travel Stop #412
3948 Hodges Chapel Road
Dunn, Harnett County, North Carolina
DRAWING TITLE
DRAWING NUMBER
FIGURE No. 8BY DATEREV
DR.: CMR
CK.:
APP'D.: CLC
SCALE: 1" = 40'
APEX PROJ. NO.: 23004903
GRAPHIC SCALE
1" = 40'NEW
40'0'20'40'60'80'DATE: June 2023 203 WYLDEROSE COURT
MIDLOTHIAN, VIRGINIA 23113(804) 897-2718
APEX COMPANIES, LLC.
www.apexcos.com
UST Closure
and
Initial
Abatement
Action Report
Former UST Basin
Love's Travel Stop
#412
MW-1 (Removed)
HODGES CHAPEL
ROAD
HODGES CHAPEL
ROAD
MW-3 MW-2
MW-5
U
MW-L3 MW-L1
MW-L2
Dispenser
Release
Location
MW-L4
Sanitary
Sewer
Limits of excavation
S-217 S-218
S-219
S-125S-126S-132
S-216
S-220
S-221S-222
S-223
S-109
S-106
S-108
S-110
S-107
Truck Dispenser
Islands
Diesel Canopy
Auto Dispenser
Islands
Auto Canopy
U
U
Monitoring Well Locations
Soil Sample Locations
Limits of Excavation
Sanitary Sewer
LEGEND
Catch Basin
U Utility Pole
Overhead Electrical
Demolished Structure

TABLES

Table 1
Soil TPH GRO/DRO Analytical Results
Love's Travel Stop 412
Dunn, North Carolina
Date Sample ID Sample Location PID     
(ppm)
TPH GRO 
(ppm)
TPH DRO 
(ppm)
Soil Disposal 
Load #Manifest #Tons
4/19/2023 419234903‐1  Gasoline tank #1 and fill ports 261.7 119.0 2,380 S19‐11 17437 23.29
4/19/2023 419234903‐2 Gasoline tanks 404.5 466.0 12,400 S19‐2 17438 18.3
4/19/2023 419234903‐3 Gasoline tanks 388.7 485.0 4,320 S19‐3 17439 22.83
4/19/2023 419234903‐4 Gasoline tanks 452.4 280.0 6,410 S19‐4 17440 20.94
4/19/2023 419234903‐5 Gasoline tanks 207.3 188.0 3,090 S19‐5 17441 22.9
4/19/2023 419234903‐6 Gasoline tanks 383.2 187.0 3,410 S19‐6 17443 14.31
4/19/2023 419234903‐7 Gasoline tanks 587.5 185.0 3,070 S19‐7 17442 22.72
4/20/2023 420234903‐8Diesel tank pumps 379.4 257.0 3,820 S20‐1 17444 24.23
4/20/2023 420234903‐9Diesel tank pumps 221.7 276.0 1,930 S20‐2 17445 18.43
4/20/2023 420234903‐10 Gasoline and diesel fill ports 260.3 208.0 2,940 S20‐3 17446 19.55
4/20/2023 420234903‐11 Biodiesel tank 230.2 183.0 10,200 S20‐4 17447 14.35
4/20/2023 420234903‐12 Diesel fill ports 353.2 240.0 2,190 S20‐5 17448 21.82
4/20/2023 420234903‐13 Diesel tank pumps 340.2 83.5 1,790 S20‐6 17449 23.2
4/20/2023 420234903‐14 Diesel tank pumps 490 212.0 13,700 S20‐7 17450 13.89
4/20/2023 420234903‐15 Gasoline tank #1 627.8 908.0 5,430 S20‐8 17451 25.43
4/20/2023 420234903‐16 Diesel tank pumps 393.8 387.0 6,830 S20‐9 17452 20.34
4/20/2023 420234903‐17 Gasoline tank #2 fill port 345.6 220.0 2,200 S20‐10 17453 22.67
4/21/2023 421234903‐18 Gasoline tank #2 fill port 557 331.0 5,480 S21‐1 17454 21.18
4/21/2023 421234903‐19 Gasoline tank #2 fill port 561.3 869.0 4,750 S21‐2 17455 22.66
4/21/2023 421234903‐20 Gasoline tank #1 256.3 283.0 721.0 S21‐3 17456 16.25
4/24/2023 42423490‐21 Gasoline tank #1 220.4 347.6 3,646 S24‐1 17518 24.15
4/24/2023 42423490‐22 Gasoline tank #1 199.8 1,458.0 12,483 S24‐2 17520 22.1
4/24/2023 42423490‐23 Gasoline tank #1 214.7 73.2 637.2 S24‐3 17519 18.21
4/24/2023 42423490‐24 Gasoline tank #1 719.3 749.2 5,294 S24‐4 17521 24.65
4/24/2023 42423490‐25 Beneath gasoline tanks #1 and #2 254.4 3,542.0 38,722 S24‐5 17522 23.76
4/24/2023 42423490‐26 Beneath gasoline tanks #1 and #2 306.7 2,241.0 43,804 S24‐6 17523 20.18
4/24/2023 42423490‐27 Beneath gasoline tanks #1 and #2 299.1 1,676.0 14,620 S24‐7 17524 24.62
4/24/2023 42423490‐28 Beneath gasoline tanks #1 and #2 160.3 492.1 5,793 S24‐8 17525 23.83
4/24/2023 42423490‐29 Beneath gasoline tanks #1 and #2 436 4,169.0 41,704 S24‐9 17526 21.69
4/24/2023 42423490‐30 Beneath gasoline tanks #1 and #2 963.5 9,704.0 34,410 S24‐10 17527 20.22
4/24/2023 42423490‐31 Beneath gasoline tanks #1 and #2 398.3 2,201.0 24,789 S24‐11 17528 24.68
4/24/2023 42423490‐32 Beneath gasoline tanks #1 and #2 618.8 2,145.0 25,165 S24‐12 17529 26.57
4/24/2023 42423490‐33 Biodiesel basin 151.1 172.6 1,660 S24‐13 17530 23.82
4/24/2023 42423490‐34 Biodiesel basin 386.5 1,875.0 9,481 S24‐14 17531 22.40
4/24/2023 42423490‐35 DEF tank 143.9 <61.6 5,322 S24‐15 17532 23.65
4/24/2023 42423490‐36 DEF tank 277.7 259.2 683.0 S24‐16 17533 19.49
4/25/2023 42523490‐37 DEF tank 135.8 3,155.0 18,959 S25‐1 17534 19.30
Table 1
Soil TPH GRO/DRO Analytical Results
Love's Travel Stop 412
Dunn, North Carolina
Date Sample ID Sample Location PID     
(ppm)
TPH GRO 
(ppm)
TPH DRO 
(ppm)
Soil Disposal 
Load #Manifest #Tons
4/25/2023 42523490‐38 Gasoline tanks #1 and #2 98.4 373.4 3,479 S25‐2 17535 22.85
4/25/2023 42523490‐39 Gasoline tanks #1 and #2 358.6 1,436.0 17,572 S25‐3 17536 24.19
4/25/2023 42523490‐40 Gasoline tanks #1 and #2 161.5 603.0 6,013 S25‐4 17537 20.67
4/25/2023 425234903‐41 Gasoline tanks #1 and #2 342.2 1,298.0 7,425 S25‐5 17538 22.00
4/25/2023 425234903‐42 Gasoline tanks #1 and #2 456.6 1,969.0 20,675 S25‐6 17539 22.88
4/25/2023 424234903‐43 Gasoline tanks #1 and #2 and diesel tank #3 594.2 4,583.0 37,374 S25‐7 17540 21.56
4/25/2023 424234903‐44 Gasoline tanks #1 and #2 and diesel tank #3 397.6 687.6 3,145 S25‐8 17541 22.31
4/25/2023 424234903‐45 Gasoline tanks #1 and #2 and diesel tank #3 163.2 151.7 1,143 S25‐9 17542 20.43
4/25/2023 425234903‐47 Biodiesel basin 229.3 1,559.0 11,783 S25‐10 17543 22.58
4/25/2023 425234903‐48 Biodiesel basin 282.9 5,414.0 36,571 S25‐11 17544 22.88
4/25/2023 425234903‐49 Biodiesel basin 275.5 2,409.0 13,227 S25‐12 17545 23.44
4/25/2023 425234903‐50 Biodiesel basin 181.7 <51.1 13,667 S25‐13 17546 23.97
4/25/2023 425234903‐51 Biodiesel basin 164.8 150.3 1,395 S25‐14 17457 22.53
4/25/2023 425234903‐52 Biodiesel basin 212.4 208.6 2,292 S25‐15 17458 23.76
4/25/2023 425234903‐53 Biodiesel basin 340 2,506.0 20,884 S25‐16 17547 23.8
4/25/2023 425234903‐54 Biodiesel basin 326.9 3,765.0 18,815 S25‐17 17459 24.11
4/25/2023 425234903‐55 Biodiesel basin 334.4 2,743.0 13,207 S25‐18 17460 18.03
4/26/2023 426234903‐56 Biodiesel basin 284.6 3,991.0 21,936 S26‐1 17461 22.77
4/26/2023 426234903‐57 Biodiesel basin 230.7 3,978.0 25,263 S26‐2 17462 23.67
4/26/2023 426234903‐58 Biodiesel basin 340.9 1,661.0 8,042 S26‐3 17463 23.23
4/26/2023 426234903‐59 Biodiesel basin 181.3 1,567.0 6,706 S26‐4 17569 23.41
4/26/2023 426234903‐60 Biodiesel basin 320.7 2,658.0 19,277 S26‐5 17464 15.10
4/26/2023 426234903‐61 DEF tank basin 151.1 2,015.0 9,700 S26‐6 17570 21.73
4/26/2023 426234903‐62 Side wall of gasoline tank #1 126.2 74.5 546 S26‐7 17465 24.23
4/26/2023 426234903‐63 Side wall of gasoline tank #1 83.9 10.4 80 S26‐82 17466 21.67
4/26/2023 426234903‐64 Biodiesel basin 248.1 939.0 6,660 S26‐9 17467 20.49
4/26/2023 426234903‐65 Biodiesel basin 285.3 3,238.0 16,801 S26‐10 17468 18.63
4/26/2023 426234903‐66 Biodiesel basin 117.7 379.9 2,853 S26‐11 17571 23.24
4/26/2023 426234903‐67 Biodiesel basin 275.3 492.2 3,577 S26‐12 16783 23.72
4/26/2023 426234903‐68 Biodiesel basin 104.7 1,620.0 7,377 S26‐13 16782 23.65
4/26/2023 426234903‐69 Biodiesel basin 318.3 1,904.0 11,270 S26‐14 17587 16.29
4/26/2023 426234903‐70 Biodiesel basin 133.5 326.2 2,488 S26‐15 17588 23.29
4/26/2023 426234903‐71 Biodiesel basin 136.4 1,197.0 8,157 S26‐16 16784 22.30
4/27/2023 427234903‐73 East wall of diesel basin 100.6 602.5 4,098 S27‐1 16785 22.65
4/27/2023 427234903‐74 Stockpile Sample Dispenser 24 134.3 379.9 3,356 S27‐2N/A N/A
4/27/2023 427234903‐75 Stockpile Sample Dispenser 24 156.6 2,643.0 21,542 S27‐3N/A N/A
4/27/2023 427234903‐76 Dispenser 24 173.3 1,426.0 10,757 S27‐4 17549 22.49
Table 1
Soil TPH GRO/DRO Analytical Results
Love's Travel Stop 412
Dunn, North Carolina
Date Sample ID Sample Location PID     
(ppm)
TPH GRO 
(ppm)
TPH DRO 
(ppm)
Soil Disposal 
Load #Manifest #Tons
4/27/2023 427234903‐77 Dispenser 24 178.8 1,926.0 10,769 S27‐5 17550 16.82
4/27/2023 427234903‐78 Stockpile Sample Dispenser 24 142.7 996.7 6,983 S27‐6N/A N/A
4/27/2023 42723490‐79 Dispenser 24 260.2 1,349.0 7,095 S27‐7 16788 22.31
4/27/2023 42723490‐80 Dispenser 24 73.4 188.3 1,081 S27‐8 16787 19.62
4/27/2023 42723490‐81 Stockpile Sample Dispenser 24 90.2 809.3 4,029 S27‐9N/A N/A
5/1/2023 427234903‐78 Dispenser 24 Stockpile 142.7 996.7 6,983 S1‐1/S27‐6 17657 23.29
5/1/2023 427234903‐74 Dispenser 24 Stockpile 134.3 379.9 3,356 S1‐2/S27‐2 17658 22.96
5/1/2023 427234903‐75 Dispenser 24 Stockpile 156.6 2,643.0 21,542 S1‐3/S27‐3 17659 19.73
5/2/2023 427234903‐81 Dispenser 24 Stockpile 90.2 809.3 4,029 S2‐1 17548 20.77
5/2/2023 52234903‐82 Dispenser 24 Stockpile 87.5 686.2 2,423 S2‐2 17551 20.59
5/2/2023 52234903‐83 Dispenser 24 Stockpile 81.2 295.4 1,807 S2‐3 17552 20.39
5/2/2023 52234903‐84 Biodiesel Stockpile 47.2 24.9 133.4 S2‐4 17473 21.37
5/2/2023 52234903‐85 Dispenser 24 108.5 298.0 713.3 S2‐5 17553 20.5
5/2/2023 52234903‐86 Dispenser 24 74.4 692.1 1,501 S2‐6 17554 20.2
5/2/2023 52234903‐87 Dispenser 24 120.2 651.8 957.1 S2‐7 17555 23.64
5/2/2023 52234903‐88 Dispenser 24 41.0 42.0 166.4 S2‐8 17556 20.57
5/2/2023 52234903‐89 Dispenser 24 62.8 40.0 224.3 S2‐9 17557 20.9
5/2/2023 52234903‐84 Biodiesel surface cover stockpile 47.2 24.9 133.4 S2‐10 17559 15.48
5/2/2023 52234903‐84 Biodiesel surface cover stockpile 47.2 24.9 133.4 S2‐11 17558 21.96
5/2/2023 52234903‐90 Side wall test sample North Wall Dispenser 24 51.2 27.7 61.6 N/A N/A N/A
5/2/2023 52234903‐91 Side wall test sample South Wall Dispenser 24 20.2 5.8 47.5 N/A N/A N/A
5/2/2023 52234903‐92 Side wall test sample East Wall Dispenser 24 248.7 474.7 1,286 N/A N/A N/A
5/2/2023 52234903‐93 Side wall test sample West Wall Dispenser 24 86.7 42.0 303.0 N/A N/A N/A
5/2/2023 52234903‐94 Side wall test sample North Wall Biodiesel Tank Pit 246.8 5,320.0 4,143 N/A N/A N/A
5/2/2023 52234903‐95 Side wall test sample West Wall Biodiesel Tank Pit 243.9 3,128.0 6,823 N/A N/A N/A
5/2/2023 52234903‐96 Side wall test sample South Wall DEF Tank Pit 193.0 664.2 1,977 N/A N/A N/A
5/2/2023 52234903‐84 Biodiesel surface cover stockpile 47.2 24.9 133.4 S2‐12 17474 21.93
5/3/2023 53234903‐097 Strip between Bio and Main Tank Pits 117.8 673.3 3,827 S3‐1 17475 21.75
5/3/2023 53234903‐098 Strip between Bio and Main Tank Pits 119.4 522.1 2,996 S3‐2 17560 22.06
5/3/2023 53234903‐099 Strip between Bio and Main Tank Pits 238.1 768.7 5,057 S3‐3 17561 15.44
5/3/2023 53234903‐100 Strip between Bio and Main Tank Pits 164.4 1,134.0 8,176 S3‐4 17562 21.02
5/3/2023 53234903‐101 Strip between Bio and Main Tank Pits 215.1 2,369.0 14,925 S3‐5 17563 14.05
5/3/2023 53234903‐102 Strip between Bio and Main Tank Pits 155.2 804.9 4,228 S3‐6 17476 20.61
5/3/2023 53234903‐103 Strip between Bio and Main Tank Pits 129.7 1,354.0 9,977 S3‐7 17564 17.34
5/3/2023 53234903‐104 Strip between Bio and Main Tank Pits 285.4 5,692.0 29,246 S3‐8 17565 20.38
5/3/2023 53234903‐105 Strip between Bio and Main Tank Pits 130 925.6 6,132 S3‐9 17477 22.72
5/3/2023 53234903‐111 Strip between Bio and Main Tank Pits 183.2 1,158.0 8,935 S3‐10 17566 23.71
Table 1
Soil TPH GRO/DRO Analytical Results
Love's Travel Stop 412
Dunn, North Carolina
Date Sample ID Sample Location PID     
(ppm)
TPH GRO 
(ppm)
TPH DRO 
(ppm)
Soil Disposal 
Load #Manifest #Tons
5/3/2023 53234903‐112 Strip between Bio and Main Tank Pits 102.7 832.8 4,224 S3‐11 17478 20.69
5/3/2023 53234903‐113 Strip between Bio and Main Tank Pits 124.4 587.4 4,475 S3‐12 17567 18.29
5/3/2023 53234903‐114 Strip between Bio and Main Tank Pits 128.3 907.1 6,505 S3‐13 17572 23.52
5/3/2023 53234903‐115 Eastern wall Main Tank Basin Diesel Side (Test Sample) 142.6 181.0 1,685 N/A N/A N/A
5/3/2023 53234903‐116 Strip between Bio and Main Tank Pits (Test Sample) 138.2 44.3 537.7 N/A N/A N/A
5/4/2023 54234903‐117 Strip between Bio and Main Tank Pits 129.4 877.8 5,890 S4‐1 17479 23.97
5/4/2023 54234903‐118 Overburden Stockpile (Test Sample) 1.2 30.2 153.8 N/A N/A N/A
5/4/2023 54234903‐119 Overburden Stockpile (Test Sample) 1.7 <0.8 147.5 S4‐7 17575 23.32
5/4/2023 54234903‐120 Strip between Bio and Main Tank Pits 132.6 1,257.0 6,842 S4‐2 17480 20.86
5/4/2023 54234903‐121 Strip between Bio and Main Tank Pits 117.1 573.2 2,567 S4‐3 17573 18.94
5/4/2023 54234903‐122 Strip between Bio and Main Tank Pits 97.9 878.8 4,159 S4‐4 17574 21.10
5/4/2023 54234903‐123 Strip between Bio and Main Tank Pits 239.5 594.3 4,693 S4‐5 17481 22.95
5/4/2023 54234903‐124 Strip between Bio and Main Tank Pits 97.6 136.2 962.4 S4‐6 17482 22.56
5/4/2023 54234903‐127 Strip between Bio and Main Tank Pits 101.4 74.7 763.9 S4‐8 17576 21.38
5/4/2023 54234903‐128 Overburden from Strip 10.7 74.4 690.1 S4‐9 17577 19.82
5/4/2023 54234903‐129 Strip between Bio and Main Tank Pits 232.4 519.6 3,985 S4‐10 17483 24.76
5/4/2023 54234903‐130 Strip between Bio and Main Tank Pits 170.2 743.2 5,501 S4‐11 17578 22.54
5/4/2023 54234903‐131 Biodiesel floor West Side 232.2 1,169.0 8,481 S4‐12 17484 21.12
5/4/2023 54234903‐133 Biodiesel floor West Side 111.7 1,900.0 2,153 S4‐13 17579 16.97
5/4/2023 54234903‐134 Biodiesel floor West Side 123.6 712.8 5,101 S4‐14 17580 24.24
5/4/2023 54234903‐135 Biodiesel floor West Side 228 3,647.0 19,477 S4‐15 17485 24.05
5/4/2023 54234903‐136 Stockpile from Strip 114.6 656.4 3,336 S4‐16 17581 16.94
5/4/2023 54234903‐137 Stockpile from Strip 118.5 612.1 4,911 S4‐17 17488 21.66
5/4/2023 54234903‐138 Stockpile from Strip 116.8 562.4 4,381 S4‐18 17489 20.93
5/4/2023 54234903‐139 Stockpile from Strip 120.4 430.2 3,102 S4‐19 17582 20.88
5/4/2023 54234903‐140 Stockpile from Strip 137.4 688.6 4,702 S4‐20 17583 16.04
5/5/2023 55234903‐141 Stockpile from Strip 35.9 289.3 2,284 S5‐1 17584 13.75
5/5/2023 55234903‐142 Biodiesel West Wall (Test Sample) 155.9 237.0 1,753 N/A N/A N/A
5/5/2023 55234903‐143 Biodiesel West Wall (Test Sample) 225.9 966.0 6,970 N/A N/A N/A
5/5/2023 55234903‐144 Biodiesel West Wall (Test Sample) 194.4 1,566.0 8,827 N/A N/A N/A
5/5/2023 55234903‐145 Biodiesel West Wall (Test Sample) 264.5 1,191.0 8,071 N/A N/A N/A
5/5/2023 55234903‐146 Biodiesel West Wall (Test Sample) 449.2 2,190.0 7,986 N/A N/A N/A
5/5/2023 55234903‐147 Biodiesel West Wall (Test Sample) 225.7 361.0 1,952 N/A N/A N/A
5/5/2023 55234903‐148 Biodiesel West Wall (Test Sample) 94.7 66.0 331.0 N/A N/A N/A
5/5/2023 55234903‐149 Strip between Bio and Main Tank Pits 170.1 458.1 2,829 S5‐2 17490 22.49
5/5/2023 55234903‐150 Strip between Bio and Main Tank Pits 121.9 615.0 3,662 S5‐3 17491 20.88
5/5/2023 55234903‐151 Strip between Bio and Main Tank Pits 153.8 532.2 6,382 S5‐4 17492 24.42
Table 1
Soil TPH GRO/DRO Analytical Results
Love's Travel Stop 412
Dunn, North Carolina
Date Sample ID Sample Location PID     
(ppm)
TPH GRO 
(ppm)
TPH DRO 
(ppm)
Soil Disposal 
Load #Manifest #Tons
5/5/2023 55234903‐152 Strip between Bio and Main Tank Pits 271 430.3 3,756 S5‐5 17596 15.24
5/5/2023 55234903‐153 Strip between Bio and Main Tank Pits 95.5 636.0 3,058 S5‐6 17597 20.94
5/5/2023 55234903‐154 Strip between Bio and Main Tank Pits 288.8 637.9 3,572 S5‐7 17598 18.58
5/5/2023 55234903‐155 Strip between Bio and Main Tank Pits 210.1 1,510.0 10,914 S5‐8 17493 23.18
5/5/2023 55234903‐156 Strip between Bio and Main Tank Pits 157.3 501.6 2,896 S5‐9 17494 22.56
5/5/2023 55234903‐157 Strip between Bio and Main Tank Pits 179.9 241.3 2,200 S5‐10 17495 22.47
5/5/2023 55234903‐158 Strip between Bio and Main Tank Pits 204.2 118.9 1,322 S5‐11 17599 22.04
5/5/2023 55234903‐159 Strip between Bio and Main Tank Pits 75.6 239.1 2,411 S5‐12 17600 19.19
5/8/2023 58234903‐161 Strip between Bio and Main Tank Pits 245.0 1,222.0 8,926 S8‐1 17601 16.63
5/8/2023 58234903‐162 Strip between Bio and Main Tank Pits 241.1 639.6 4,800 S8‐2 17602 23.65
5/8/2023 58234903‐163 Strip between Bio and Main Tank Pits 296.5 1,389.0 12,767 S8‐3 17496 22.11
5/8/2023 58234903‐164 Strip between Bio and Main Tank Pits 263.2 <18.8 2,223 S8‐4 17497 24.40
5/8/2023 58234903‐165 Strip between Bio and Main Tank Pits 430.7 507.0 4,310 S8‐5 17498 23.52
5/8/2023 58234903‐166 Strip between Bio and Main Tank Pits 85.1 387.5 2,799 S8‐6 17603 21.00
5/8/2023 58234903‐167 Strip between Bio and Main Tank Pits 228.5 1,811.0 11,758 S8‐7 17471 23.30
5/8/2023 58234903‐168 Strip between Bio and Main Tank Pits 137.8 1,276.0 9,511 S8‐8 17499 22.68
5/8/2023 58234903‐169 Strip between Bio and Main Tank Pits 135.6 <23 3,879 S8‐9 17604 20.65
5/8/2023 58234903‐170 Strip between Bio and Main Tank Pits 80.4 789.3 6,752 S8‐10 17500 23.16
5/8/2023 58234903‐171 Surface Gravel from between Main and Bio Tank Pits 
(Stockpile)1.9 15.1 47.5 N/A N/A N/A
5/8/2023 58234903‐172 Surface Gravel from between Main and Bio Tank Pits 
(Stockpile)5.1 21.1 52.5 N/A N/A N/A
5/8/2023 54234903‐118 Gravel Overburden Stockpile 1.6 30.2 153.8 S8‐11 17605 21.01
5/8/2023 54234903‐119 Gravel Overburden Stockpile 1.7 <0.8 147.5 S8‐12 17501 22.14
5/8/2023 58234903‐173 Strip between Bio and Main Tank Pits 96.4 280.1 2,307 S8‐13 17606 25.97
5/8/2023 58234903‐174 Strip between Bio and Main Tank Pits 34.7 523.5 4,458 S8‐14 17607 20.09
5/8/2023 58234903‐175 Strip between Bio and Main Tank Pits 44.4 161.8 977.9 S8‐15 17502 21.44
5/8/2023 58234903‐176 Strip between Bio and Main Tank Pits 95.8 666.4 3,738 S8‐16 17503 22.75
5/8/2023 58234903‐177 Strip between Bio and Main Tank Pits 101.3 585.6 3,753 S8‐17 17608 20.30
5/8/2023 58234903‐178 Strip between Bio and Main Tank Pits 143.3 397.9 3,601 S8‐18 17609 22.61
5/8/2023 58234903‐179 Strip between Bio and Main Tank Pits 149.2 351.5 2,885 S8‐19 17504 22.70
5/8/2023 58234903‐180 Strip between Bio and Main Tank Pits 410.1 1,065.0 9,140 S8‐20 17505 23.00
5/8/2023 58234903‐181 Strip between Bio and Main Tank Pits 126.7 667.9 6,134 S8‐21 17506 21.13
5/9/2023 59234903‐182 Strip between Bio and Main Tank Pits 178.5 290.3 2,336 S9‐1 17486 23.08
5/9/2023 59234903‐183 Strip between Bio and Main Tank Pits 165.8 <23.2 1,238 S9‐2 17507 21.04
5/9/2023 59234903‐184 Strip between Bio and Main Tank Pits 122 454.2 2,890 S9‐3 17610 21.86
5/9/2023 59234903‐185 Strip between Bio and Main Tank Pits 149.6 472.1 4,216 S9‐4 17611 21.2
5/9/2023 59234903‐186 Strip between Bio and Main Tank Pits 76.53 342.3 3,173 S9‐5 17508 21.47
5/9/2023 59234903‐187 Strip between Bio and Main Tank Pits 111.5 264.3 2,356 S9‐6 17509 23.63
Table 1
Soil TPH GRO/DRO Analytical Results
Love's Travel Stop 412
Dunn, North Carolina
Date Sample ID Sample Location PID     
(ppm)
TPH GRO 
(ppm)
TPH DRO 
(ppm)
Soil Disposal 
Load #Manifest #Tons
5/9/2023 59234903‐188 Strip between Bio and Main Tank Pits 170.5 442.0 3,956 S9‐7 17612 23.01
5/9/2023 59234903‐189 DEF Tank Pit 315.9 593.4 3,938 S9‐8 17613 21.06
5/9/2023 59234903‐190 DEF Tank Pit 297.1 928.1 7,074 S9‐9 17510 22.21
5/9/2023 59234903‐191 DEF Tank Pit 273.8 920.4 8,621 S9‐10 17511 19.98
5/9/2023 59234903‐192 DEF Tank Pit 339.4 1,360.0 10,223 S9‐11 17512 21.08
5/9/2023 59234903‐193 DEF Tank Pit 203.6 2,069.0 14,985 S9‐12 17614 22.25
5/9/2023 59234903‐194 DEF Tank Pit (Stockpile) 171.2 601.8 4,676 N/A N/A N/A
5/9/2023 59234903‐195 DEF Tanl Pit East Wall (Test Sample) 186.1 1,103.0 9,261 N/A N/A N/A
5/9/2023 59234903‐196 Biodiesel Tank Pit South Wall (Test Sample) 193.3 274.2 2,598 N/A N/A N/A
5/9/2023 59234903‐197 Biodiesel Tank Pit South Wall (Test Sample) 336.6 1,286.0 9,432 N/A N/A N/A
5/9/2023 59234903‐198 Biodiesel and Main Tank Pit North Wall (Test Sample) 483.2 437.7 4,364 N/A N/A N/A
5/9/2023 59234903‐199 Biodiesel and Main Tank Pit North Wall (Test Sample) 286 126.2 1,510 N/A N/A N/A
5/9/2023 59234903‐200 Main Tank Pit South Wall (Test Sample) 185.6 306.6 3,167 N/A N/A N/A
5/9/2023 59234903‐201 Biodiesel Tank Pit East Wall (Test Sample) 342.6 2,159.0 17,595 N/A N/A N/A
5/10/2023 59234903‐194 DEF Tank Pit Stockpile 171.2 601.8 4,676 S10‐1 17615 23.67
5/11/2023 511234903‐202 North Wall Main Tank Pit 81.1 <21.8 924 S11‐1 17513 22.65
5/11/2023 511234903‐203 East Wall Main Tank Pit 123.9 4,850.0 27,110 S11‐2 17514 23.77
5/11/2023 511234903‐204 DEF Tank Pit 68.6 141.3 1,266 S11‐3 17515 22.81
5/11/2023 N/A Diesel Fuel Line 103.7 N/A N/A S11‐4 17674 22.97
5/11/2023 N/A Diesel Fuel Line 158.4 N/A N/A S11‐5 17675 21.62
5/11/2023 N/A Diesel Fuel Line 138.1 N/A N/A S11‐6 17516 20.65
5/11/2023 511234903‐205 Biodiesel North Wall (Test Pit) 195.3 1,026.0 6,261 S11‐7 17676 22.48
5/11/2023 511234903‐206 Biodiesel North Wall Test Pit 61.0 <9.9 493.6 S11‐8 17641 18.8
5/11/2023 N/A Diesel Fuel Line 148.2 N/A N/A S11‐9 17677 22.59
5/11/2023 511234903‐207 Diesel Fuel Line 129.2 1,352.0 6,203 S11‐10 17654 21.83
5/11/2023 511234903‐209 DEF Tank Pit 60.6 106.2 1,025 S11‐11 17643 22.41
5/11/2023 511234903‐210 DEF Tank Pit 189.1 1,075.0 7,783 S11‐12 17644 23.76
5/11/2023 511234903‐211 Biodiesel Tank Pit South Wall and Floor 227.9 204.2 1,609 S11‐13 17645 21.75
5/11/2023 511234903‐212 Biodiesel Tank Pit East Wall 183.6 177.4 1,423 S11‐14 17678 22.27
5/11/2023 511234903‐213 Biodiesel and DEF Tank Pit South Wall 128.9 212.2 1,619 S11‐15 17679 22.45
5/11/2023 511234903‐215 Diesel Dispenser Release Area 113.8 221.0 2,408 S11‐16 17517 25.09
Table 1
Soil TPH GRO/DRO Analytical Results
Love's Travel Stop 412
Dunn, North Carolina
Date Sample ID Sample Location PID     
(ppm)
TPH GRO 
(ppm)
TPH DRO 
(ppm)
Soil Disposal 
Load #Manifest #Tons
5/12/2023 N/A Diesel Fuel Line 137.4 N/A N/A S12‐1 17680 24.40
5/12/2023 N/A Diesel Fuel Line 163.8 N/A N/A S12‐2 17681 23.33
5/12/2023 N/A Diesel Fuel Line 141.7 N/A N/A S12‐3 17682 21.08
S25‐1 17639 22.16
S25‐2 17640 21.82
S25‐3 17616 22.06
S25‐4 17617 22.86
S25‐5 17619 22.92
S25‐6 17618 21.78
S25‐7 17623 23.12
S25‐8 17620 14.38
S25‐9 17621 23.61
S25‐10 17622 22.31
S26‐1 17625 22.92
S26‐2 17624 18.58
S26‐3 17626 23.45
S26‐4 17627 25.8
S26‐5 17628 23.37
S26‐6 17629 14.29
S26‐7 17630 21.59
S26‐8 17631 23.01
TOTAL 4,439.06
2Non‐Directed Soil Disposal Totals Are Shaded (757.02 Tons)
<6.2
Gasoline Dispenser Islands ‐ Soil Stockpile 15/25/2023 524234903‐225 N/A 22.4 6.3
524234903‐2245/25/2023 N/A <10.2Gasoline Dispenser Islands ‐ Soil Stockpile 2
1DEQ‐Directed Soil Disposal Totals Are Not Shaded (3,682.04 Tons)
Table 2
Soil VOC/SVOC Analytical Results
Loves Travel Stop #412
Dunn, North Carolina
Sample Location S-106 S-107 S-108 S-109 S-110 S-125 S-126 S-132 S-216 S-217 S-218 S-219 S-220 S-221 S-222 S-223
Sample ID 53234903-
106
53234903-
107
53234903-
108
53234903-
109
53234903-
106
54234903-
125
54234903-
126
54234903-
132
512234903-
216
512234903-
217
512234903-
218
512234903-
219
512234903-
220
512234903-
221
512234903-
222
512234903-
223
Date
5/3/2023 5/3/2023 5/3/2023 5/3/2023 5/3/2023 5/4/2023 5/4/2023 5/4/2023 5/12/2023 5/12/2023 5/12/2023 5/12/2023 5/12/2023 5/12/2023 5/12/2023 5/12/2023Benzene <RL <RL <RL 7.0 18.2 <RL 56.3 201 <RL <RL <RL <RL <RL <RL <RL <RL 59,400
Ethylbenzene <RL <RL <RL <RL 18.7 802 402 132 15.7 119 2,160 60.3 8.9 <RL <RL <RL 297,000
Xylenes, Total <RL <RL <RL <RL <RL <RL <RL 425 <RL <RL 4,060 <RL <RL <RL <RL <RL 46,700,000
Isopropylbenzene <RL <RL <RL 33.3 14.4 550 577 239 649 1,440 1,340 1,440 451 111 <RL <RL 23,300,000
n-Propylbenzene <RL <RL <RL 57.7 25.8 1,240 1,300 459 1,690 3,320 2,830 2,980 1,140 184 <RL <RL 23,300,000
1,3,5-Trimethylbenzene <RL <RL <RL 58.5 <RL 621 852 408 <RL <RL 4,010 <RL <RL <RL <RL <RL 2,330,000
1,2,4-Trimethylbenzene <RL <RL <RL 339 32.0 977 2,440 1,160 <RL <RL 11,200 <RL <RL <RL <RL <RL 2,330,000
sec-Butylbenzene 29.5 <RL <RL 93.1 17.0 983 1,170 1,610 2,780 2,120 2,330 1,220 1,030 16.4 10.7 23,300,000
p-Isopropyltoluene <RL <RL <RL 193 <RL <RL <RL 554 <RL <RL 3,700 <RL <RL <RL <RL <RL 23,300,000
n-Butylbenzene <RL <RL <RL 87.1 <RL 1,230 1,440 673 1,650 2,660 1,980 1,900 1,180 514 <RL <RL 11,600,000
1-Methylnaphthalene <RL <RL <RL <RL <RL 808 2,200 1,120 1,060 7,560 8,520 1,220 <RL <RL <RL <RL 112,000
2-Methylnaphthalene <RL <RL <RL <RL <RL 1,240 3,340 1,740 1,150 11,700 13,100 1,830 403 <RL <RL <RL 934,000
1,1,2-Trichloroethane <RL <RL <RL <RL <RL <RL <RL <RL 321 <RL <RL <RL <RL <RL <RL <RL 125,000
Styrene <RL <RL <RL <RL <RL 32.4 <RL <RL <RL <RL <RL <RL <RL <RL <RL <RL 46,700,000
Naphthalene <RL <RL <RL 93.3 <RL 2,140 2,500 962 1,800 5,550 5,130 4,580 <RL <RL <RL <RL 27,000
MTBE <RL <RL <RL <RL <RL <RL <RL <RL <RL <RL <RL <RL <RL <RL <RL 5.9 1,810,000
Chloromethane 19,500 20,700 8,870 <RL 7,890 18,300 19,400 13.4 4,400 <RL 3,930 14,700 <RL <RL <RL <RL 251,000
Fluorene <RL <RL <RL <RL <RL <RL 441 <RL <RL <RL <RL <RL <RL <RL <RL <RL 9,340,000
Phenanthrene <RL <RL <RL <RL <RL <RL 662 435 599 <RL <RL 386 <RL <RL <RL <RL 7,000,000
Notes:
1 All samples analyzed via U.S. EPA SW-846 methods 8260D (VOCs) and 8270E (SVOCs), reported in micrograms per kilogram (µg/kg).
2 Industrial/Commercial MSCC's reported in micrograms per kilogram (ug/kg). MSCC screening levels have been converted from milligrams per kilogram (mg/kg) as originally reported by NC DEQ dated September 7, 2022.
Industrial/
Commercial
MSCC's
3 <RL = Constituent not detected above laboratory reporting limit.
Table 3
Groundwater VOC/SVOC Analytical Results
Loves Travel Stop #412
Dunn, North Carolina
Sample Location
Biodiesel and
Main Tank
Basin
Biodiesel Tank
Basin
Biodiesel and
Main Tank
Basin
Main Tank
Basin
Sample ID 425234903-46 426234903-72 55234903-160 511234903-214
Date 4/25/23 4/26/23 5/5/23 5/11/23
Benzene 2.0 2.0 <RL 1.7
Ethylbenzene 1.1 2.1 29.7 1.0
Xylenes, Total 4.4 8.4 <RL 1.4
Isopropylbenzene 1.1 2.2 136 1.3
n-Propylbenzene 1.7 3.3 352 2.2
1,3,5-Trimethylbenzene 2.2 3.8 <RL 4.2
1,2,4-Trimethylbenzene 4.2 5.7 <RL 3.6
sec-Butylbenzene 29.5 <RL 587 <RL
n-Butylbenzene <RL <RL 789 <RL
Toluene 5.7 8.6 <RL <RL
Naphthalene 30.4 37.3 522 13.6
Pyrene <RL <RL 3,930 <RL
Phenanthrene <RL <RL 3,500 <RL
Notes:
1 All samples analyzed via U.S. EPA SW-846 methods 6200B (VOCs) and 625.1 (SVOCs), reported in micrograms per liter (µg/L).
3 <RL = Constituent not detected above laboratory reporting limit.

APPENDIX A

UST-3 Notice of Intent: UST Permanent Closure or Change-In-Service

APPENDIX B

Harnett County Fire Marshal Permit Inspection Forms

Inspection Type:306 - Fuel Tank Installation/Removal
Inspection Date:4/19/2023 By:Starling, Matthew (3590msES)
Time In:12:00 Time Out:15:00
Authorized Date:04/19/2023 By:Starling, Matthew (3590msES)
Next Inspection Date: 04/20/2023 306 - Fuel Tank Installation/Removal
Occupancy:Love’s Truck Stop
Occupancy ID:85000566
Address:3948 Hodges Chapel RD DUNN NC 28334
Additional Time Spent on Inspection:
Category Start Date / Time End Date / Time
No Additional time recordedNotes:
Total Additional Time: 0 minutes
Total Time: 180 minutes
Inspection Time: 180 minutes
Inspection Topics:
Summary:
Overall Result:Fire Code Compliance
An inspection of your facility revealed no violations of the North Carolina Fire Code.
Inspector Notes:Fuel tank removal at Love’s Truck Stop. Two gasoline tanks and one diesel tanks. All LELs
were 0 and proper markings put on rear of tanks.
Harnett County Fire Marshals Office
Form: Harnett County
General Fire Inspection
Statement of Compliance
An inspection of your facility on this date revealed no violations of the North Carolina State Fire Prevention Code. No further
inspections will need to be conducted until your next regular schedule fire inspection.
Status: PASS
Notes:
***Statement of Compliance***
Inspection Description:
Harnett County Fire Inspection
Inspector:
Name: Starling, Matthew
Rank:
Work Phone(s): None on file
Email(s): [e-mail]
Starling, Matthew:
Signature Date
Signed on: 04/19/2023 14:15
Page 1 of 2Printed on 04/19/23 at 14:51:41
Representative Signature:
Signature Date
Page 2 of 2Printed on 04/19/23 at 14:51:41
Inspection Type:306 - Fuel Tank Installation/Removal
Inspection Date:4/21/2023 By:Starling, Matthew (3590msES)
Time In:08:00 Time Out:11:00
Authorized Date:04/21/2023 By:Starling, Matthew (3590msES)
Next Inspection Date: 04/21/2024 100 - Fire Protection Inspection
Occupancy:Love’s Truck Stop
Occupancy ID:85000566
Address:3948 Hodges Chapel RD DUNN NC 28334
Additional Time Spent on Inspection:
Category Start Date / Time End Date / Time
No Additional time recordedNotes:
Total Additional Time: 0 minutes
Total Time: 180 minutes
Inspection Time: 180 minutes
Inspection Topics:
Summary:
Overall Result:Fire Code Compliance
An inspection of your facility revealed no violations of the North Carolina Fire Code.
Inspector Notes:Removal of two fuel tanks by crane. LEL levels were 0 and all other markings were wrote
on tanks prior to hauling off.
Harnett County Fire Marshals Office
Form: Harnett County
General Fire Inspection
Inspection Description:
Harnett County Fire Inspection
Inspector:
Name: Starling, Matthew
Rank:
Work Phone(s): None on file
Email(s): [e-mail]
Starling, Matthew:
Signature Date
Signed on: 04/21/2023 10:31
Representative Signature:
Signature Date
Page 1 of 1Printed on 04/21/23 at 10:32:55

APPENDIX C

Non-Hazardous Liquid Waste Manifests

APPENDIX D

UST Disposal Certificates

APPENDIX E

Laboratory Certificates of Analysis
and Chain of Custody Records

Hydrocarbon Analysis Results
Client:APEX Samples taken Monday, April 24, 2023
Address:Samples extracted Monday, April 24, 2023
Samples analysed Monday, April 24, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #412 ; PO#23004903
6 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042423 4903 - 21 0945 1055.0 <26.4 347.6 3646 3994 862.3 31 <1.1 85.7 13.4 0.9 Deg.Diesel 95.2%,(FCM)
s 042423 4903 - 22 0955 2472.0 <61.8 1458 12483 13941 1978 73.6 <2.5 86.5 12.9 0.6 Deg.Diesel 95.7%,(FCM)
s 042423 4903 - 23 1005 373.0 <9.3 73.2 637.2 710.4 82.6 <3 <0.37 91.7 8.3 0 Deg.Diesel 75.5%,(FCM)
s 042423 4903 - 24 1014 2509.0 <62.7 749.2 5294 6043 576.6 <20.1 <2.5 94.1 5.5 0.4 Deg.Diesel 84.9%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 92 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Monday, April 24, 2023
Address:Samples extracted Monday, April 24, 2023
Samples analysed Monday, April 24, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #412 ; PO#23004903
15 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042423 4903 - 25 1231 38523.0 <963.1 3542 38722 42264 6514 <308.2 <38.5 85.7 12.9 1.5 Deg.Diesel 83.8%,(FCM)
s 042423 4903 - 26 1237 32158.0 <804 2241 43804 46045 13213 475.8 <32.2 67.3 30.6 2 Deg.Diesel 82.9%,(FCM)
s 042423 4903 - 27 1240 2627.0 <65.7 1676 14620 16296 2333 86 <2.6 85.7 13.6 0.7 Deg.Diesel 79.5%,(FCM)
s 042423 4903 - 28 1245 2975.0 <74.4 492.1 5793 6285 1334 48.4 <3 83.2 15.7 1.1 Deg.Diesel 95.1%,(FCM)
s 042423 4903 - 29 1414 26228.0 <655.7 4169 41704 45873 6600 <209.8 <26.2 87.8 11.2 1 Deg.Diesel 79.7%,(FCM)
s 042423 4903 - 30 1421 81152.0 <2029 9704 34410 44114 2171 <649.2 <81.2 99.6 0.4 0 Undeg.Diesel 89.5%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 101.7 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Monday, April 24, 2023
Address:Samples extracted Monday, April 24, 2023
Samples analysed Monday, April 24, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #412 ; PO#23004903
6 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042423 4903 - 31 1622 13640.0 <341 2201 24789 26990 4360 160.5 <13.6 85 14.3 0.7 Deg.Diesel 79.9%,(FCM)
s 042423 4903 - 32 1625 11088.0 <277.2 2145 25165 27310 4918 179.1 <11.1 84.2 14.6 1.2 Deg.Diesel 83%,(FCM)
s 042423 4903 - 33 1628 2136.0 <53.4 172.6 1660 1833 142.6 <17.1 <2.1 93.5 5.8 0.7 Deg.Diesel 68.3%,(FCM)
s 042423 4903 - 34 1630 2184.0 <54.6 1875 9481 11356 817 29.6 <2.2 97.5 2.3 0.2 Undeg.Diesel 89%,(FCM)
s 042423 4903 - 35 1636 2464.0 <61.6 <61.6 5322 5322 190.2 <19.7 <2.5 0 87.4 12.6 Waste Oil 72.4%,(FCM)
s 042423 4903 - 36 1650 2002.0 <50.1 259.2 683 942.2 109 <16 <2 95.7 3.8 0.5 Deg.Diesel 73.7%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 99.5 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, April 25, 2023
Address:Samples extracted Tuesday, April 25, 2023
Samples analysed Tuesday, April 25, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #412 ; PO#23004903
6 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042523 4903 - 37 0915 1941.0 599.2 3155 18959 22114 2312 82.1 <1.9 96.3 3.4 0.2 Undeg.Diesel 86.6%,(FCM)
s 042523 4903 - 38 0942 1830.0 <45.8 373.7 3479 3853 532.4 19.9 <1.8 88.8 10.6 0.6 Deg.Diesel 95.6%,(FCM)
s 042523 4903 - 39 0950 7612.0 <190.3 1436 17572 19008 3539 128.7 <7.6 82.6 16.2 1.1 Deg.Diesel 80%,(FCM)
s 042523 4903 - 40 0957 1538.0 <38.4 603 6013 6616 1685 60.3 <1.5 83 16.1 0.8 Deg.Diesel 80%,(FCM)
s 042523 4903 - 41 1110 1732.0 238.7 1298 7425 8723 1282 46 <1.7 94.1 5.5 0.4 Deg.Diesel 87.9%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 92.2 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, April 25, 2023
Address:Samples extracted Tuesday, April 25, 2023
Samples analysed Tuesday, April 25, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #412 ; PO#23004903
11 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042523 4903 - 42 1132 9236.0 <230.9 1969 20675 22644 2770 101.9 <9.2 88.8 10.4 0.8 Deg.Diesel 81.1%,(FCM)
s 042523 4903 - 43 1150 12343.0 <308.6 4583 37374 41957 7250 261.9 <12.3 90.2 9.2 0.6 Deg.Diesel 95.4%,(FCM)
s 042523 4903 - 44 1205 1732.0 257.5 687.6 3145 3833 346 <13.9 <1.7 95.9 3.7 0.4 Deg.Diesel 92.4%,(FCM)
s 042523 4903 - 45 1231 438.0 <11 151.7 1143 1295 126.3 4.7 <0.44 93.8 5.7 0.5 Undeg.Diesel 95.3%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 102.3 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, April 25, 2023
Address:Samples extracted Tuesday, April 25, 2023
Samples analysed Tuesday, April 25, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #412 ; PO#23004903
18 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042523 4903 - 47 1410 1763.0 <44.1 1559 11783 13342 1483 55 <1.8 91.1 8.4 0.5 Undeg.Diesel 96%,(FCM)
s 042523 4903 - 48 1415 9691.0 <242.3 5414 36571 41985 4895 176.4 <9.7 95.2 4.8 0 Undeg.Diesel 81.5%,(FCM)
s 042523 4903 - 49 1435 1643.0 751.7 2409 13227 15636 1527 56.6 <1.6 93.8 5.9 0.3 Undeg.Diesel 95.4%,(FCM)
s 042523 4903 - 50 1449 2045.0 <51.1 <51.1 13667 13667 2413 89 <2 0 96.2 3.8 Undeg.Diesel 91.3%,(FCM)
s 042523 4903 - 51 1555 1830.0 <45.8 150.3 1395 1545 143.2 <14.6 <1.8 92.9 5.7 1.5 Undeg.Diesel 69%,(FCM)
s 042523 4903 - 52 1602 1780.0 <44.5 208.6 2292 2501 290.5 <14.2 <1.8 89.1 9.7 1.3 Deg.Diesel 64.7%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 105.3 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, April 25, 2023
Address:Samples extracted Tuesday, April 25, 2023
Samples analysed Tuesday, April 25, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #412 ; PO#23004903
3 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042523 4903 - 53 1625 1763.0 <44.1 2506 20884 23390 1505 55.7 <1.8 94.7 5 0.3 Undeg.Diesel 83.6%,(FCM)
s 042523 4903 - 54 1642 1478.0 <37 3765 18815 22580 1359 50.3 <1.5 96.7 3.1 0.2 Undeg.Diesel 89.7%,(FCM)
s 042523 4903 - 55 1700 1961.0 <49 2743 13207 15950 1395 49.9 <2 97.6 2.4 0 Undeg.Diesel 88.3%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 99.8 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Wednesday, April 26, 2023
Address:Samples extracted Wednesday, April 26, 2023
Samples analysed Wednesday, April 26, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #412 ; PO#23004903
6 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042623 4903 - 56 0925 1866.0 248 3991 21936 25927 2338 86.4 <1.9 94 5.7 0.3 Undeg.Diesel 94.5%,(FCM)
s 042623 4903 - 57 0928 1780.0 485.1 3978 25263 29241 1814 67.2 <1.8 95.5 4.3 0.3 Undeg.Diesel 88.9%,(FCM)
s 042623 4903 - 58 0931 2316.0 806.5 1661 8042 9703 960.8 34.8 <2.3 96.3 3.3 0.3 Undeg.Diesel 86.1%,(FCM)
s 042623 4903 - 59 0938 1780.0 774.8 1567 6706 8273 924.4 33.3 <1.8 96.5 3.3 0.3 Undeg.Diesel 91.5%,(FCM)
s 042623 4903 - 60 1015 6763.0 <169.1 2658 19277 21935 2768 100.1 <6.8 93.9 5.8 0.3 Deg.Diesel 80.8%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 103.3 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Wednesday, April 26, 2023
Address:Samples extracted Wednesday, April 26, 2023
Samples analysed Wednesday, April 26, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #421 ; PO#23004903
6 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042623 4903 - 61 1130 2403.0 <120.1 2015 9700 11715 683.6 25.4 <2.4 97.7 2.2 0.1 Undeg.Diesel 87.7%,(FCM)
s 042623 4903 - 62 1220 63.9 <1.6 74.5 546 620.5 65.5 2.4 <0.064 91.3 8.3 0.4 Undeg.Diesel 95.8%,(FCM)
s 042623 4903 - 63 1230 79.5 <2 10.4 79.8 90.2 9.2 <0.64 <0.079 93.5 6.5 0 Deg.Diesel 79.8%,(FCM)
s 042623 4903 - 64 1314 1830.0 <45.8 939 6660 7599 1409 50.4 <1.8 92.6 7.4 0 Undeg.Diesel 93.1%,(FCM)
s 042623 4903 - 65 1322 1866.0 1206 3238 16801 20039 1826 67.5 <1.9 94.6 5.2 0.3 Undeg.Diesel 95.7%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 100.6 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Wednesday, April 26, 2023
Address:Samples extracted Wednesday, April 26, 2023
Samples analysed Wednesday, April 26, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #421 ; PO#23004903
11 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042623 4903 - 66 1625 793.0 <19.8 379.9 2853 3233 536.3 19.2 <0.79 92.5 7 0.4 Undeg.Diesel 94.4%,(FCM)
s 042623 4903 - 67 1527 430.0 <10.7 492.2 3577 4069 482.5 17.8 <0.43 90.1 9.5 0.4 Undeg.Diesel 94.4%,(FCM)
s 042623 4903 - 68 1542 1903.0 570.5 1620 7377 8997 1505 53.8 <1.9 95.3 4.5 0.3 Undeg.Diesel 92.9%,(FCM)
s 042623 4903 - 69 1544 2136.0 <53.4 1904 11270 13174 997 35.8 <2.1 96.7 3 0.3 Undeg.Diesel 91.3%,(FCM)
s 042623 4903 - 70 1545 488.0 <12.2 326.2 2488 2814 579.1 20.6 <0.49 91.4 8.2 0.4 Undeg.Diesel 94.4%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 100.6 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Wednesday, April 26, 2023
Address:Samples extracted Wednesday, April 26, 2023
Samples analysed Wednesday, April 26, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #421 ; PO#23004903
1 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042623 4903 - 71 1640 1848.0 <46.2 1197 8157 9354 1484 53 <1.8 94.1 5.7 0.2 Undeg.Diesel 91.7%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 104.3 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, April 27, 2023
Address:Samples extracted Thursday, April 27, 2023
Samples analysed Thursday, April 27, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #421 ; PO#23004903
6 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042723 4903 - 73 1002 462.0 <11.5 602.5 4098 4701 418.5 15.5 <0.46 92.8 6.7 0.5 Deg.Diesel 83.9%,(FCM)
s 042723 4903 - 74 1052 1445.0 <36.1 379.9 3356 3736 403.2 15 <1.4 91.8 7.7 0.5 Deg.Diesel 78.1%,(FCM)
s 042723 4903 - 75 1105 11648.0 <291.2 2643 21542 24185 3052 113.8 <11.6 91.9 8.1 0 Deg.Diesel 77.1%,(FCM)
s 042723 4903 - 76 1118 1796.0 <44.9 1426 10757 12183 1980 70.6 <1.8 92.7 7 0.3 Deg.Diesel 82.2%,(FCM)
s 042723 4903 - 77 1149 1643.0 120.4 1926 10769 12695 1894 67.5 <1.6 94.7 5 0.3 Deg.Diesel 96.6%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 99.3 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, April 27, 2023
Address:Samples extracted Thursday, April 27, 2023
Samples analysed Thursday, April 27, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #421 ; PO#23004903
9 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042723 4903 - 78 1214 2464.0 <61.6 996.7 6983 7980 743.3 27.8 <2.5 93.8 5.7 0.5 Deg.Diesel 84.3%,(FCM)
s 042723 4903 - 79 1349 1602.0 241 1349 7095 8444 475.1 17.7 <1.6 97.3 2.5 0.2 Undeg.Diesel 90.2%,(FCM)
s 042723 4903 - 80 1357 67.4 67.8 188.3 1081 1269 68.2 2.5 <0.067 95.4 4.2 0.4 Deg.Diesel 86.1%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 97.9 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, April 27, 2023
Address:Samples extracted Thursday, April 27, 2023
Samples analysed Thursday, April 27, 2023
Contact:MARK RYLAND ; CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP #421 ; PO#23004903
10 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 042723 4903 - 81 1415 1078.0 133.2 809.3 4029 4838 253.5 <8.6 <1.1 97.4 2.3 0.4 Undeg.Diesel 89.5%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 101.6 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, May 2, 2023
Address:3948 HODGES CHAPEL ROAD Samples extracted Tuesday, May 2, 2023
DUNN, NC Samples analysed Tuesday, May 2, 2023
Contact:CRAIG RICHARDSON Operator TORI KELLY
Project:LOVE'S TRAVEL SHOP #412
4 F03640
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 52234903-82 2905.0 <72.6 686.2 2423 3109 573.1 <23.2 <2.9 94.3 5.4 0.4 Deg.Diesel 70.1%,(FCM)
s 52234903-83 1220.0 <30.5 295.4 1807 2102 560.9 21 <1.2 89.4 10.1 0.5 Deg.Diesel 97.9%,(FCM)
s 52234903-84 51.7 <1.3 24.9 133.4 158.3 44.4 1.6 <0.052 91.6 8 0.4 Undeg.Diesel 94.7%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 109.9 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, May 2, 2023
Address:3948 HODGES CHAPEL ROAD Samples extracted Tuesday, May 2, 2023
DUNN, NC Samples analysed Tuesday, May 2, 2023
Contact:CRAIG RICHARDSON Operator TORI KELLY
Project:LOVE'S TRAVEL SHOP #412
5 F03640
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 52234903-85 745.0 <18.6 298 713.3 1011.3 191 7.3 <0.74 95 4.7 0.3 Deg.Diesel 82.4%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 108.7 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, May 2, 2023
Address:3948 HODGES CHAPEL ROAD Samples extracted Tuesday, May 2, 2023
DUNN, NC Samples analysed Tuesday, May 2, 2023
Contact:CRAIG RICHARDSON Operator TORI KELLY
Project:LOVES TRAVEL SHOP #412
4 F03640
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 52234903-86 641.0 <16 692.1 1501 2193 650.3 24.1 <0.64 94.5 5.1 0.4 Deg.Diesel 91.1%,(FCM)
s 52234903-87 843.0 107 651.8 957.1 1608.9 266.9 10.1 <0.84 96.9 2.9 0.2 Deg.Diesel 92.7%,(FCM)
s 52234903-88 291.0 <7.3 42 166.4 208.4 42.5 <2.3 <0.29 91.9 7.6 0.5 Deg.Diesel 77.6%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 98.3 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, May 2, 2023
Address:3948 HODGES CHAPEL ROAD Samples extracted Tuesday, May 2, 2023
DUNN, NC Samples analysed Tuesday, May 2, 2023
Contact:CRAIG RICHARDSON Operator TORI KELLY
Project:LOVES TRAVEL SHOP #412
5 F03640
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 52234903-89 371.0 <9.3 40 224.3 264.3 57.5 <3 <0.37 90.3 9.1 0.6 Deg.Diesel 65.4%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 97.7 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, May 2, 2023
Address:3948 HODGES CHAPEL ROAD Samples extracted Tuesday, May 2, 2023
DUNN, NC Samples analysed Tuesday, May 2, 2023
Contact:CRAIG RICHARDSON Operator TORI KELLY
Project:LOVES TRAVEL SHOP #412
16 F03640
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 52234903-90 18.1 3.2 27.7 61.6 89.3 27.3 1 <0.018 95.7 4 0.3 Undeg.Diesel 94.6%,(FCM)
s 52234903-91 21.0 <0.53 5.8 47.5 53.3 17.1 0.64 <0.021 80 18.6 1.4 Deg.Diesel 78.2%,(FCM)
s 52234903-92 269.0 <6.7 474.7 1286 1761 138.8 5.2 <0.27 98.5 1.4 0.1 Undeg.Diesel 93.8%,(FCM)
s 52234903-93 189.0 <4.7 42 303 345 94.8 3.5 <0.19 85.3 13.9 0.7 Deg.Diesel 81.4%,(FCM)
s 52234903-94 8269.0 <206.7 5320 4143 9463 1298 <66.2 <8.3 98.3 1.5 0.1 Deg.Diesel 95.8%,(FCM)
s 52234903-95 4181.0 <104.5 3128 6823 9951 1519 57.9 <4.2 96.8 3 0.2 Undeg.Diesel 94.9%,(FCM)
s 52234903-96 1232.0 <30.8 664.2 1977 2641 166.5 <9.9 <1.2 98.5 1.5 0 Undeg.Diesel 93%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 96.7 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Wednesday, May 3, 2023
Address:Samples extracted Wednesday, May 3, 2023
Samples analysed Wednesday, May 3, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
3 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050323 4903 - 97 0908 741.0 <18.5 673.3 3827 4500 336.9 12.1 <0.74 97 2.7 0.2 Undeg.Diesel 93.9%,(FCM)
s 050323 4903 - 98 0913 723.0 <18.1 522.1 2996 3518 407.1 14.6 <0.72 95.7 4.1 0.2 Undeg.Diesel 85.6%,(FCM)
s 050323 4903 - 99 0928 700.0 <17.5 768.7 5057 5826 571.7 21.2 <0.7 93.2 6.4 0.4 Undeg.Diesel 94.8%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 98.1 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Wednesday, May 3, 2023
Address:Samples extracted Wednesday, May 3, 2023
Samples analysed Wednesday, May 3, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
7 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050323 4903 - 100 1115 848.0 <21.2 1134 8176 9310 884.3 32.7 <0.85 92.3 7.4 0.4 Undeg.Diesel 95.5%,(FCM)
s 050323 4903 - 101 1122 3150.0 <78.8 2369 14925 17294 2271 81.2 <3.2 95.2 4.8 0 Undeg.Diesel 82.9%,(FCM)
s 050323 4903 - 102 1131 991.0 248.9 804.9 4228 5033 581.9 20.9 <0.99 95.7 3.9 0.4 Undeg.Diesel 86.7%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 99.7 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Wednesday, May 3, 2023
Address:Samples extracted Wednesday, May 3, 2023
Samples analysed Wednesday, May 3, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
5 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050323 4903 - 103 1319 3835.0 <95.9 1354 9977 11331 1075 39.9 <3.8 94.6 5.4 0 Undeg.Diesel 78%,(FCM)
s 050323 4903 - 104 1322 6695.0 1377 5692 29246 34938 4661 167.1 <6.7 95.6 4.2 0.2 Undeg.Diesel 87.4%,(FCM)
s 050323 4903 - 105 1420 882.0 54.3 925.6 6132 7058 615.2 22.1 <0.88 96.3 3.5 0.3 Undeg.Diesel 91%,(FCM)
s 050323 4903 - 111 1510 1002.0 <25.1 1158 8935 10093 1075 39.8 <1 90.8 8.8 0.4 Undeg.Diesel 96%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 103.3 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Wednesday, May 3, 2023
Address:Samples extracted Wednesday, May 3, 2023
Samples analysed Wednesday, May 3, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
5 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050323 4903 - 112 1640 1208.0 203.7 832.8 4224 5057 551.3 19.9 <1.2 96.3 3.5 0.2 Undeg.Diesel 93.9%,(FCM)
s 050323 4903 - 113 1649 891.0 <22.3 587.4 4475 5062 807 28.8 <0.89 92.8 6.9 0.3 Undeg.Diesel 95.8%,(FCM)
s 050323 4903 - 114 1709 991.0 <24.8 907.1 6505 7412 1179 41.9 <0.99 93.6 6.1 0.2 Undeg.Diesel 94.6%,(FCM)
s 050323 4903 - 115 1710 329.0 <8.2 181 1685 1866 225 8.4 <0.33 88.6 10.8 0.6 Deg.Diesel 74.9%,(FCM)
s 050323 4903 - 116 1711 260.0 <6.5 44.3 537.7 582 113.2 4.1 <0.26 84.8 14.4 0.7 Deg.Diesel 95.4%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 102.1 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, May 4, 2023
Address:Samples extracted Thursday, May 4, 2023
Samples analysed Thursday, May 4, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
6 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050423 4903 - 117 0824 919.0 <23 877.8 5890 6768 930.5 33.1 <0.92 94.4 5.3 0.3 Undeg.Diesel 85%,(FCM)
s 050423 4903 - 118 0826 45.7 <1.1 30.2 153.8 184 32.5 1.2 <0.046 84.5 13.5 1.9 Deg.Diesel 58.5%,(FCM)
s 050423 4903 - 119 0834 32.1 <0.8 <0.8 147.5 147.5 38.7 1.4 <0.032 0 88.5 11.5 Deg.Diesel 55.7%,(FCM)
s 050423 4903 - 120 0845 824.0 514.7 1257 6842 8099 757.6 27 <0.82 96.9 2.9 0.2 Undeg.Diesel 88.8%,(FCM)
s 050423 4903 - 121 0907 943.0 226.3 573.2 2567 3140 247.3 9.2 <0.94 96.5 3.2 0.3 Undeg.Diesel 89.7%,(FCM)
s 050423 4903 - 122 0920 741.0 256.7 878.8 4159 5038 623.2 22.3 <0.74 96 3.7 0.3 Undeg.Diesel 90.3%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 106.6 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, May 4, 2023
Address:Samples extracted Thursday, May 4, 2023
Samples analysed Thursday, May 4, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
3 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050423 4903 - 123 1046 865.0 <21.6 594.3 4693 5287 937.9 33.4 <0.86 91.3 8.2 0.4 Deg.Diesel 80.3%,(FCM)
s 050423 4903 - 124 1054 969.0 <24.2 136.2 962.4 1098.6 90.9 <7.8 <0.97 95.3 4.7 0 Deg.Diesel 81%,(FCM)
s 050423 4903 - 127 1118 809.0 <20.2 74.7 763.9 838.6 97.9 <6.5 <0.81 90.9 9.1 0 Deg.Diesel 66.5%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 99 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, May 4, 2023
Address:Samples extracted Thursday, May 4, 2023
Samples analysed Thursday, May 4, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
8 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050423 4903 - 128 1252 747.0 <18.7 74.4 690.1 764.5 66.4 <6 <0.75 92.1 6.6 1.3 Deg.Diesel 70.9%,(FCM)
s 050423 4903 - 129 1307 900.0 <22.5 519.6 3985 4505 614.8 22 <0.9 93.6 6 0.4 Undeg.Diesel 95.4%,(FCM)
s 050423 4903 - 130 1330 948.0 <23.7 743.2 5501 6244 996.1 35.5 <0.95 93.2 6.5 0.3 Undeg.Diesel 95.7%,(FCM)
s 050423 4903 - 131 1345 684.0 298.5 1169 8481 9650 554.8 22 <0.68 94.9 4.7 0.4 Deg.Diesel 78.5%,(FCM)
s 050423 4903 - 133 1424 969.0 <24.2 253 1900 2153 200 <7.8 <0.97 93.7 5.7 0.6 Deg.Diesel 81%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 98 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, May 4, 2023
Address:Samples extracted Thursday, May 4, 2023
Samples analysed Thursday, May 4, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
15 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050423 4903 - 134 1520 760.0 176.4 712.8 5101 5814 463.2 16.7 <0.76 95.8 3.8 0.4 Deg.Diesel 87.8%,(FCM)
s 050423 4903 - 135 1526 5162.0 669 3647 19477 23124 1358 50.5 <5.2 97.6 2.4 0 Undeg.Diesel 87.9%,(FCM)
s 050423 4903 - 136 1553 873.0 162.1 656.4 3336 3992 440.9 15.9 <0.87 96.3 3.4 0.3 Undeg.Diesel 94.2%,(FCM)
s 050423 4903 - 137 1610 1063.0 <26.6 612.1 4911 5523 851.1 30.4 <1.1 92.5 7.1 0.4 Undeg.Diesel 78.9%,(FCM)
s 050423 4903 - 138 1655 919.0 <23 562.4 4381 4943 771 27.6 <0.92 92.6 7 0.4 Undeg.Diesel 81.5%,(FCM)
s 050423 4903 - 139 1711 1014.0 <25.3 430.2 3102 3532 469.4 16.9 <1 93.6 6 0.5 Deg.Diesel 82.2%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 103.4 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, May 4, 2023
Address:Samples extracted Thursday, May 4, 2023
Samples analysed Thursday, May 4, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
16 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050423 4903 - 140 1724 1050.0 <26.3 688.6 4702 5391 720.2 25.8 <1.1 94.2 5.4 0.4 Undeg.Diesel 85.3%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 98.2 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Friday, May 5, 2023
Address:Samples extracted Friday, May 5, 2023
Samples analysed Friday, May 5, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
14 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050523 4903 - 141 0922 339.0 <8.5 289.3 2284 2573 261.8 9.7 <0.34 91.7 7.8 0.4 Undeg.Diesel 79.5%,(FCM)
s 050523 4903 - 142 0923 486.0 <12.2 237.1 1753 1990 336.4 12.1 <0.49 92.6 7.1 0.3 Undeg.Diesel 93.9%,(FCM)
s 050523 4903 - 143 0924 909.0 <22.7 966 6970 7936 891.8 33 <0.91 91.4 8.3 0.3 Undeg.Diesel 94.2%,(FCM)
s 050523 4903 - 144 0927 788.0 675.1 1566 8827 10393 623.9 23.1 <0.79 96.4 3.4 0.2 Undeg.Diesel 93.7%,(FCM)
s 050523 4903 - 145 0929 1609.0 <40.2 1191 8071 9262 1361 48.6 <1.6 94.1 5.6 0.2 Undeg.Diesel 94.3%,(FCM)
s 050523 4903 - 146 0931 1565.0 990.2 2190 7986 10176 1419 50.7 <1.6 96.6 3.3 0.1 Undeg.Diesel 94.3%,(FCM)
s 050523 4903 - 147 0933 856.0 96.6 361.3 1952 2313 128.5 <6.9 <0.86 97.4 2.4 0.2 Undeg.Diesel 92.3%,(FCM)
s 050523 4903 - 148 0934 307.0 <15.4 66.1 331.4 397.5 33.7 <2.5 <0.31 96 3.7 0.3 Deg.Diesel 91.1%,(FCM)
s 050523 4903 - 149 0937 1002.0 162.9 458.1 2829 3287 185.1 <8 <1 97 2.8 0.2 Undeg.Diesel 89.9%,(FCM)
s 050523 4903 - 150 0938 723.0 141.8 615 3662 4277 318.5 11.5 <0.72 96.8 2.9 0.3 Undeg.Diesel 91.9%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 102 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Friday, May 5, 2023
Address:Samples extracted Friday, May 5, 2023
Samples analysed Friday, May 5, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
21 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050523 4903 - 151 0942 383.0 167.1 532.2 3682 4214 425.5 15.1 <0.38 95.9 3.8 0.3 Undeg.Diesel 85.2%,(FCM)
s 050523 4903 - 152 0944 1050.0 <26.3 430.3 3756 4186 755.3 27.2 <1.1 89.2 10 0.7 Deg.Diesel 95.5%,(FCM)
s 050523 4903 - 153 1025 809.0 72.1 636 3058 3694 358.2 13 <0.81 96.2 3.3 0.5 Deg.Diesel 89.1%,(FCM)
s 050523 4903 - 154 1027 856.0 121.7 637.9 3572 4210 526 18.9 <0.86 95.6 4.1 0.3 Undeg.Diesel 94.3%,(FCM)
s 050523 4903 - 155 1126 1609.0 <40.2 1510 10914 12424 1281 47.5 <1.6 92.7 7 0.3 Undeg.Diesel 93.5%,(FCM)
s 050523 4903 - 156 1128 1063.0 93.5 501.6 2896 3398 313.5 11.7 <1.1 95.1 4.5 0.4 Deg.Diesel 86.1%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 90.9 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Friday, May 5, 2023
Address:Samples extracted Friday, May 5, 2023
Samples analysed Friday, May 5, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
24 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050523 4903 - 157 1153 909.0 <22.7 241.3 2200 2441 375.5 13.5 <0.91 90.8 8.5 0.7 Deg.Diesel 76.3%,(FCM)
s 050523 4903 - 158 1154 948.0 <23.7 118.9 1322 1441 169.7 <7.6 <0.95 89.6 9.3 1.1 Deg.Diesel 65%,(FCM)
s 050523 4903 - 159 1213 639.0 <16 239.1 2411 2650 471.6 16.9 <0.64 89.6 9.8 0.6 Deg.Diesel 96.4%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 106.7 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Monday, May 8, 2023
Address:Samples extracted Monday, May 8, 2023
Samples analysed Monday, May 8, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
10 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050823 4903 - 161 1012 848.0 <21.2 1222 8926 10148 916.8 33.9 <0.85 92.3 7.4 0.4 Undeg.Diesel 82.7%,(FCM)
s 050823 4903 - 162 1013 1002.0 <25.1 639.6 4800 5440 755.2 27 <1 93.2 6.5 0.3 Deg.Diesel 81.4%,(FCM)
s 050823 4903 - 163 1015 909.0 <22.7 1389 12767 14156 891.1 33 <0.91 93.6 6 0.3 Undeg.Diesel 83.7%,(FCM)
s 050823 4903 - 164 1016 754.0 <18.8 <18.8 2223 2223 625.5 22.3 <0.75 0 94.3 5.7 Undeg.Diesel 93.7%,(FCM)
s 050823 4903 - 165 1018 1026.0 <25.6 507 4310 4817 873.1 31.3 <1 89.8 9.8 0.4 Deg.Diesel 79%,(FCM)
s 050823 4903 - 166 1048 1230.0 <30.8 387.5 2799 3187 286.6 <9.8 <1.2 94 5.7 0.3 Deg.Diesel 84%,(FCM)
s 050823 4903 - 167 1057 948.0 774.1 1811 11758 13569 819.7 30.4 <0.95 95.6 4.1 0.2 Undeg.Diesel 86.4%,(FCM)
s 050823 4903 - 168 1110 781.0 <19.5 1276 9511 10787 1013 37.4 <0.78 91.2 8.4 0.4 Deg.Diesel 82.7%,(FCM)
s 050823 4903 - 169 1118 919.0 <23 <23 3879 3879 716 26.5 <0.92 0 94.5 5.5 Undeg.Diesel 93.4%,(FCM)
s 050823 4903 - 170 1135 959.0 <24 789.3 5963 6752 763.5 28.4 <0.96 90.3 9.2 0.5 Deg.Diesel 84.3%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 99.9 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Monday, May 8, 2023
Address:Samples extracted Monday, May 8, 2023
Samples analysed Monday, May 8, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
16 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050823 4903 - 171 1211 35.3 <0.88 15.1 47.5 62.6 22.1 0.95 <0.035 69.2 26.6 4.2 V.Deg.Diesel 81.6%,(FCM)
s 050823 4903 - 172 1310 39.6 <0.99 21.1 52.5 73.6 25.1 1.1 <0.04 72.1 24 3.8 V.Deg.Diesel 81.5%,(FCM),(BO)
s 050823 4903 - 173 1331 809.0 <20.2 280.1 2307 2587 312.4 11.4 <0.81 92.7 6.7 0.6 Deg.Diesel 80.7%,(FCM)
s 050823 4903 - 174 1336 799.0 <20 523.5 4458 4982 577.6 22.6 <0.8 89.1 10.2 0.7 Deg.Diesel 79.5%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 95.1 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Monday, May 8, 2023
Address:Samples extracted Monday, May 8, 2023
Samples analysed Monday, May 8, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
20 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050823 4903 - 175 1400 409.0 <10.2 161.8 977.9 1139.7 106.9 4 <0.41 94.1 5.1 0.7 Deg.Diesel 92.7%,(FCM)
s 050823 4903 - 176 1401 824.0 <20.6 666.4 3738 4404 675.2 24.2 <0.82 94 5.6 0.5 Deg.Diesel 88.6%,(FCM)
s 050823 4903 - 177 1526 817.0 <20.4 585.6 3753 4339 635.4 22.9 <0.82 92.8 6.7 0.5 Deg.Diesel 82.4%,(FCM)
s 050823 4903 - 178 1545 928.0 <23.2 397.9 3601 3999 796.5 28.6 <0.93 88.1 11.3 0.6 Deg.Diesel 95.2%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 103.8 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Monday, May 8, 2023
Address:Samples extracted Monday, May 8, 2023
Samples analysed Monday, May 8, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
24 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050823 4903 - 179 1558 741.0 <18.5 351.5 2885 3237 562.9 20.2 <0.74 89.9 9.6 0.5 Deg.Diesel 82.8%,(FCM)
s 050823 4903 - 180 1603 1640.0 <41 1065 9140 10205 1412 52 <1.6 86.3 13 0.6 Deg.Diesel 85.6%,(FCM)
s 050823 4903 - 181 1621 909.0 <22.7 667.9 6134 6802 999 36.7 <0.91 84.1 15.3 0.6 Deg.Diesel 81%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 98.4 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, May 9, 2023
Address:Samples extracted Tuesday, May 9, 2023
Samples analysed Tuesday, May 9, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
3 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050923 4903 - 182 0851 635.0 <15.9 290.3 2336 2626 525 18.8 <0.63 89 10.5 0.4 Deg.Diesel 95.5%,(FCM)
s 050923 4903 - 183 0857 928.0 <23.2 <23.2 1238 1238 268.6 10 <0.93 0 95 5 Deg.Diesel 94.3%,(FCM)
s 050923 4903 - 184 0912 824.0 85.3 454.2 2890 3344 566.6 20.4 <0.82 91.7 7.8 0.5 Deg.Diesel 95%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 96.4 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, May 9, 2023
Address:Samples extracted Tuesday, May 9, 2023
Samples analysed Tuesday, May 9, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
7 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050923 4903 - 185 1104 741.0 <18.5 472.1 4216 4688 671.1 25 <0.74 85.1 14.2 0.7 Deg.Diesel 95.9%,(FCM)
s 050923 4903 - 186 1109 848.0 <21.2 342.3 3173 3515 809 29 <0.85 86.3 12.9 0.8 Deg.Diesel 95.6%,(FCM)
s 050923 4903 - 187 1129 440.0 <11 264.3 2356 2620 301.1 11.2 <0.44 88.1 11.1 0.8 Deg.Diesel 82.9%,(FCM)
s 050923 4903 - 188 1143 900.0 <22.5 442 3956 4398 255.4 9.6 <0.9 95.2 4.2 0.6 Deg.Diesel 82.8%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 96.4 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, May 9, 2023
Address:Samples extracted Tuesday, May 9, 2023
Samples analysed Tuesday, May 9, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
16 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050923 4903 - 189 1417 1038.0 254.4 593.4 3938 4531 249.9 <8.3 <1 96.5 3.2 0.3 Deg.Diesel 80.3%,(FCM)
s 050923 4903 - 190 1431 959.0 <24 928.1 7074 8002 979.5 36.4 <0.96 89 10.6 0.5 Deg.Diesel 83.2%,(FCM)
s 050923 4903 - 191 1439 1813.0 <45.3 920.4 8621 9541 1287 47.9 <1.8 86.6 12.8 0.6 Deg.Diesel 95.2%,(FCM)
s 050923 4903 - 192 1450 1739.0 <43.5 1360 10223 11583 2117 75.2 <1.7 92.3 7.4 0.4 Undeg.Diesel 95.7%,(FCM)
s 050923 4903 - 193 1504 1580.0 <39.5 2069 14985 17054 1948 72.1 <1.6 90 9.6 0.4 Deg.Diesel 96.3%,(FCM)
s 050923 4903 - 194 1600 809.0 <20.2 601.8 4676 5278 998.1 35.5 <0.81 91.5 8.1 0.4 Deg.Diesel 80.4%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 105.1 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Tuesday, May 9, 2023
Address:Samples extracted Tuesday, May 9, 2023
Samples analysed Tuesday, May 9, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
9 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 050923 4903 - 195 1629 1722.0 <43.1 1103 9261 10364 1298 48.2 <1.7 89.3 10.3 0.4 Deg.Diesel 79%,(FCM)
s 050923 4903 - 196 1631 644.0 <16.1 274.2 2598 2872 680.6 24.2 <0.64 88 11.5 0.4 Deg.Diesel 94.8%,(FCM)
s 050923 4903 - 197 1634 991.0 <24.8 1286 9432 10718 1228 45.3 <0.99 91.3 8.7 0 Undeg.Diesel 91.5%,(FCM)
s 050923 4903 - 198 1635 909.0 <22.7 437.7 4364 4802 708.4 26.4 <0.91 84.4 15 0.6 Deg.Diesel 95.9%,(FCM)
s 050923 4903 - 199 1637 684.0 <17.1 126.2 1510 1636 358 12.9 <0.68 82.9 16.4 0.7 Deg.Diesel 95.5%,(FCM)
s 050923 4903 - 200 1638 840.0 <21 306.6 3167 3474 780.2 27.8 <0.84 85.7 13.6 0.6 Deg.Diesel 80.8%,(FCM)
s 050923 4903 - 201 1640 2267.0 <56.7 2159 17595 19754 2353 87.1 <2.3 89.9 9.8 0.3 Undeg.Diesel 76.5%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 98.5 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, May 11, 2023
Address:Samples extracted Thursday, May 11, 2023
Samples analysed Thursday, May 11, 2023
Contact:ERIC RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
3 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 051123 4903 - 202 0824 873.0 <21.8 <21.8 924 924 166.2 <7 <0.87 0 93.4 6.6 Deg.Diesel 93.7%,(FCM)
s 051123 4903 - 203 0851 2949.0 1215 4850 27110 31960 3106 115.2 <2.9 93.4 6.3 0.4 Deg.Diesel 87%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 95.9 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, May 11, 2023
Address:Samples extracted Thursday, May 11, 2023
Samples analysed Thursday, May 11, 2023
Contact:ERIC RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
5 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 051123 4903 - 204 1040 840.0 <21 141.3 1266 1407 160.1 <6.7 <0.84 91.4 7.7 0.9 Deg.Diesel 78%,(FCM)
s 051123 4903 - 205 1151 1594.0 251.1 1026 6261 7287 1315 47.1 <1.6 92.4 7.1 0.5 Deg.Diesel 86.1%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 103.5 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, May 11, 2023
Address:Samples extracted Thursday, May 11, 2023
Samples analysed Thursday, May 11, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
4 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 051123 4903 - 206 1254 398.0 <9.9 <9.9 493.6 493.6 103.3 3.9 <0.4 0 94.7 5.3 Deg.Diesel 95.9%,(FCM)
s 051123 4903 - 207 1358 781.0 490.3 1352 6203 7555 744.3 27.6 <0.78 94.6 5.1 0.3 Undeg.Diesel 95.6%,(FCM)
s 051123 4903 - 208 1402 969.0 279.6 897.2 4895 5792 843.7 30.1 <0.97 95.1 4.7 0.2 Undeg.Diesel 95.1%,(FCM)
s 051123 4903 - 209 1433 374.0 <9.4 106.2 1025 1131 180.6 6.5 <0.37 90.3 9.1 0.5 Deg.Diesel 71.1%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 101.1 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, May 11, 2023
Address:Samples extracted Thursday, May 11, 2023
Samples analysed Thursday, May 11, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
6 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 051123 4903 - 210 1513 1656.0 <41.4 1075 7783 8858 1656 59.1 <1.7 92.1 7.5 0.3 Undeg.Diesel 81.1%,(FCM)
s 051123 4903 - 211 1545 268.0 <6.7 204.2 1609 1813 221 8.2 <0.27 89.9 9.7 0.4 Deg.Diesel 81.5%,(FCM)
s 051123 4903 - 212 1559 233.0 <5.8 177.4 1423 1600 180 6.7 <0.23 90.8 8.9 0.4 Deg.Diesel 96.7%,(FCM)
s 051123 4903 - 215 1630 364.0 <9.1 221 2408 2629 960.6 34 <0.36 69.7 27 3.2 Deg.Diesel 82%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 97 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:APEX Samples taken Thursday, May 11, 2023
Address:Samples extracted Thursday, May 11, 2023
Samples analysed Thursday, May 11, 2023
Contact:CRAIG RICHARDSON Operator MAX MOYER
Project:LOVE'S TRAVEL STOP ; PO#23004903
7 H09382
Matrix Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid
%
heavy
s 051123 4903 - 213 1719 236.0 <5.9 212.2 1619 1831 218.6 8.1 <0.24 89.6 9.9 0.5 Deg.Diesel 82.1%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 100.9 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
#=CL#
May 04, 2023
LIMS USE: FR - MARK RYLAND
LIMS OBJECT ID: 92663981
92663981
Project:
Pace Project No.:
RE:
Mark Ryland
Apex Companies, LLC
203 Wylderose Court
Midlothian, VA 23113
Loves 412 23004903
Dear Mark Ryland:
Enclosed are the analytical results for sample(s) received by the laboratory on April 25, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 39
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 39
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92663981
Loves 412 23004903
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92663981001 419234903-1 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981002 419234903-2 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981003 419234903-3 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981004 419234903-4 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981005 419234903-5 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981006 419234903-6 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981007 419234903-7 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981008 419234903-8 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981009 419234903-9 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981010 419234903-10 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981011 419234903-11 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981012 419234903-12 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981013 419234903-13 EPA 8015C 2 PASI-CNND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 39
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92663981
Loves 412 23004903
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981014 419234903-14 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981015 419234903-15 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981016 419234903-16 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981017 419234903-17 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981018 419234903-18 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981019 419234903-19 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92663981020 419234903-20 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-1 Lab ID: 92663981001 Collected: 04/19/23 09:50 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)2380 mg/kg 05/03/23 13:55 M104/29/23 20:0356.7 10
Surrogates
n-Pentacosane (S) 0 %05/03/23 13:55 629-99-2 S404/29/23 20:0310-133 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)119 mg/kg 04/28/23 00:0604/27/23 16:406.5 1
Surrogates
4-Bromofluorobenzene (S) 196 %04/28/23 00:06 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.7 %04/25/23 15:48 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-2 Lab ID: 92663981002 Collected: 04/19/23 13:20 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)12400 mg/kg 05/03/23 14:11 D604/29/23 20:03286 50
Surrogates
n-Pentacosane (S) 0 %05/03/23 14:11 629-99-2 S404/29/23 20:0310-133 50
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)466 mg/kg 04/28/23 00:3204/27/23 16:406.0 1
Surrogates
4-Bromofluorobenzene (S) 254 %04/28/23 00:32 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.1 %04/25/23 15:48 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-3 Lab ID: 92663981003 Collected: 04/19/23 13:30 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)4320 mg/kg 05/03/23 14:1104/29/23 20:03114 20
Surrogates
n-Pentacosane (S) 0 %05/03/23 14:11 629-99-2 S404/29/23 20:0310-133 20
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)485 mg/kg 04/28/23 00:5704/27/23 16:406.1 1
Surrogates
4-Bromofluorobenzene (S) 263 %04/28/23 00:57 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.3 %04/25/23 15:48 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-4 Lab ID: 92663981004 Collected: 04/19/23 14:30 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)6410 mg/kg 05/03/23 14:2804/29/23 20:03144 25
Surrogates
n-Pentacosane (S) 0 %05/03/23 14:28 629-99-2 S404/29/23 20:0310-133 25
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)280 mg/kg 04/28/23 01:2304/27/23 16:406.0 1
Surrogates
4-Bromofluorobenzene (S) 191 %04/28/23 01:23 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.6 %04/25/23 15:48 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-5 Lab ID: 92663981005 Collected: 04/19/23 16:20 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)3090 mg/kg 05/03/23 14:2804/29/23 20:0357.3 10
Surrogates
n-Pentacosane (S) 0 %05/03/23 14:28 629-99-2 S404/29/23 20:0310-133 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)188 mg/kg 04/28/23 01:4904/27/23 16:406.1 1
Surrogates
4-Bromofluorobenzene (S) 167 %04/28/23 01:49 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.7 %04/25/23 15:48 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-6 Lab ID: 92663981006 Collected: 04/19/23 16:30 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)3410 mg/kg 05/03/23 14:4404/29/23 20:0355.6 10
Surrogates
n-Pentacosane (S) 0 %05/03/23 14:44 629-99-2 S404/29/23 20:0310-133 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)187 mg/kg 04/28/23 02:1504/27/23 16:405.6 1
Surrogates
4-Bromofluorobenzene (S) 164 %04/28/23 02:15 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.5 %04/25/23 15:48 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-7 Lab ID: 92663981007 Collected: 04/19/23 16:40 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)3070 mg/kg 05/03/23 14:4404/29/23 20:0355.8 10
Surrogates
n-Pentacosane (S) 0 %05/03/23 14:44 629-99-2 S404/29/23 20:0310-133 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)185 mg/kg 04/28/23 02:4004/27/23 16:405.7 1
Surrogates
4-Bromofluorobenzene (S) 194 %04/28/23 02:40 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.8 %04/25/23 15:48 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-8 Lab ID: 92663981008 Collected: 04/20/23 09:30 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)3820 mg/kg 05/03/23 17:4404/29/23 20:03111 20
Surrogates
n-Pentacosane (S) 0 %05/03/23 17:44 629-99-2 S404/29/23 20:0310-133 20
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)257 mg/kg 04/28/23 03:0604/27/23 16:405.8 1
Surrogates
4-Bromofluorobenzene (S) 304 %04/28/23 03:06 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 9.4 %04/25/23 15:49 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-9 Lab ID: 92663981009 Collected: 04/20/23 09:50 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)1930 mg/kg 05/03/23 15:0004/29/23 20:0358.1 10
Surrogates
n-Pentacosane (S) 0 %05/03/23 15:00 629-99-2 S404/29/23 20:0310-133 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)276 mg/kg 04/28/23 03:3204/27/23 16:406.1 1
Surrogates
4-Bromofluorobenzene (S) 296 %04/28/23 03:32 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.4 %04/25/23 15:49 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-10 Lab ID: 92663981010 Collected: 04/20/23 09:40 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)2940 mg/kg 05/03/23 15:1704/29/23 20:0358.8 10
Surrogates
n-Pentacosane (S) 0 %05/03/23 15:17 629-99-2 S404/29/23 20:0310-133 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)208 mg/kg 04/28/23 03:5804/27/23 16:406.1 1
Surrogates
4-Bromofluorobenzene (S) 193 %04/28/23 03:58 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.5 %04/25/23 16:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-11 Lab ID: 92663981011 Collected: 04/20/23 11:30 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)10200 mg/kg 05/03/23 15:3304/29/23 20:03281 50
Surrogates
n-Pentacosane (S) 0 %05/03/23 15:33 629-99-2 S404/29/23 20:0310-133 50
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)183 mg/kg 04/28/23 04:2404/27/23 16:405.7 1
Surrogates
4-Bromofluorobenzene (S) 265 %04/28/23 04:24 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.6 %04/25/23 16:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-12 Lab ID: 92663981012 Collected: 04/20/23 11:50 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)2190 mg/kg 05/03/23 15:1704/29/23 20:0356.9 10
Surrogates
n-Pentacosane (S) 0 %05/03/23 15:17 629-99-2 S404/29/23 20:0310-133 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)240 mg/kg 04/28/23 04:5004/27/23 16:406.9 1
Surrogates
4-Bromofluorobenzene (S) 171 %04/28/23 04:50 460-00-4 S504/27/23 16:4066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.9 %04/25/23 16:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-13 Lab ID: 92663981013 Collected: 04/20/23 12:10 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)1790 mg/kg 05/03/23 17:4404/29/23 20:0354.1 10
Surrogates
n-Pentacosane (S) 0 %05/03/23 17:44 629-99-2 S404/29/23 20:0310-133 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)83.5 mg/kg 04/28/23 07:5004/27/23 16:456.4 1
Surrogates
4-Bromofluorobenzene (S) 141 %04/28/23 07:50 460-00-4 S504/27/23 16:4566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 9.1 %04/25/23 16:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-14 Lab ID: 92663981014 Collected: 04/20/23 13:30 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)13700 mg/kg 05/03/23 15:5004/29/23 20:03279 50
Surrogates
n-Pentacosane (S) 0 %05/03/23 15:50 629-99-2 S404/29/23 20:0310-133 50
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)212 mg/kg 04/28/23 08:1604/27/23 16:456.1 1
Surrogates
4-Bromofluorobenzene (S) 206 %04/28/23 08:16 460-00-4 S504/27/23 16:4566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.5 %04/25/23 16:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-15 Lab ID: 92663981015 Collected: 04/20/23 14:08 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)5430 mg/kg 05/03/23 16:3905/02/23 12:51140 25
Surrogates
n-Pentacosane (S) 0 %05/03/23 16:39 629-99-2 S405/02/23 12:5110-133 25
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)908 mg/kg 04/28/23 23:3104/28/23 16:5113.3 2
Surrogates
4-Bromofluorobenzene (S) 272 %04/28/23 23:31 460-00-4 S204/28/23 16:5166-130 2
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.6 %04/25/23 16:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-16 Lab ID: 92663981016 Collected: 04/20/23 17:15 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)6830 mg/kg 05/03/23 16:5505/02/23 12:51139 25
Surrogates
n-Pentacosane (S) 0 %05/03/23 16:55 629-99-2 S405/02/23 12:5110-133 25
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)387 mg/kg 04/28/23 09:0704/27/23 16:456.3 1
Surrogates
4-Bromofluorobenzene (S) 182 %04/28/23 09:07 460-00-4 S504/27/23 16:4566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.7 %04/25/23 16:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-17 Lab ID: 92663981017 Collected: 04/20/23 17:25 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)2200 mg/kg 05/03/23 16:5505/02/23 12:5158.7 10
Surrogates
n-Pentacosane (S) 0 %05/03/23 16:55 629-99-2 S405/02/23 12:5110-133 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)220 mg/kg 04/28/23 09:3304/27/23 16:456.7 1
Surrogates
4-Bromofluorobenzene (S) 150 %04/28/23 09:33 460-00-4 S504/27/23 16:4566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.2 %04/25/23 16:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-18 Lab ID: 92663981018 Collected: 04/21/23 09:20 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)5480 mg/kg 05/03/23 17:1205/02/23 12:51146 25
Surrogates
n-Pentacosane (S) 0 %05/03/23 17:12 629-99-2 S405/02/23 12:5110-133 25
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)311 mg/kg 04/28/23 09:5904/27/23 16:456.6 1
Surrogates
4-Bromofluorobenzene (S) 230 %04/28/23 09:59 460-00-4 S504/27/23 16:4566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.8 %04/25/23 16:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-19 Lab ID: 92663981019 Collected: 04/21/23 11:50 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)4750 mg/kg 05/03/23 17:1205/02/23 12:51144 25
Surrogates
n-Pentacosane (S) 0 %05/03/23 17:12 629-99-2 S405/02/23 12:5110-133 25
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)869 mg/kg 04/28/23 23:5704/28/23 16:5112.9 2
Surrogates
4-Bromofluorobenzene (S) 311 %04/28/23 23:57 460-00-4 S204/28/23 16:5166-130 2
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.1 %04/25/23 16:23 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 23 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663981
Loves 412 23004903
Sample: 419234903-20 Lab ID: 92663981020 Collected: 04/21/23 12:05 Received: 04/25/23 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)721 mg/kg 05/03/23 17:2805/02/23 12:5115.1 2.5
Surrogates
n-Pentacosane (S) 82 %05/03/23 17:28 629-99-205/02/23 12:5110-133 2.5
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)283 mg/kg 04/28/23 10:5004/27/23 16:457.5 1
Surrogates
4-Bromofluorobenzene (S) 177 %04/28/23 10:50 460-00-4 S504/27/23 16:4566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.6 %04/25/23 16:23 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663981
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770927
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples:92663981001, 92663981002, 92663981003, 92663981004, 92663981005, 92663981006, 92663981007,
92663981008, 92663981009, 92663981010, 92663981011, 92663981012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4002244
Associated Lab Samples: 92663981001, 92663981002, 92663981003, 92663981004, 92663981005, 92663981006, 92663981007,
92663981008, 92663981009, 92663981010, 92663981011, 92663981012
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 04/27/23 19:22
4-Bromofluorobenzene (S) % 97 66-130 04/27/23 19:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4002245LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10) mg/kg 54.949.7 111 70-130
4-Bromofluorobenzene (S) %98 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4002247MATRIX SPIKE SAMPLE:
MSSpike
Result
92664159002
Gas Range Organics (C6-C10) mg/kg 87.068.8 124 57-154ND
4-Bromofluorobenzene (S) %98 66-130
Parameter Units
Dup
Result QualifiersRPDResult
92664159001
4002246SAMPLE DUPLICATE:
Gas Range Organics (C6-C10) mg/kg 5.1JND
4-Bromofluorobenzene (S) %9799
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663981
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770928
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92663981013, 92663981014, 92663981016, 92663981017, 92663981018, 92663981020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4002264
Associated Lab Samples:92663981013, 92663981014, 92663981016, 92663981017, 92663981018, 92663981020
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 04/27/23 19:48
4-Bromofluorobenzene (S) % 97 66-130 04/27/23 19:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4002265LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10) mg/kg 54.549.7 110 70-130
4-Bromofluorobenzene (S) %98 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4002267MATRIX SPIKE SAMPLE:
MSSpike
Result
92663770001
Gas Range Organics (C6-C10) mg/kg 73.364.6 112 57-154ND
4-Bromofluorobenzene (S) %98 66-130
Parameter Units
Dup
Result QualifiersRPDResult
92663742003
4002266SAMPLE DUPLICATE:
Gas Range Organics (C6-C10) mg/kg NDND
4-Bromofluorobenzene (S) %9497
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663981
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
771194
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92663981015, 92663981019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4003622
Associated Lab Samples:92663981015, 92663981019
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 04/28/23 19:13
4-Bromofluorobenzene (S) % 97 66-130 04/28/23 19:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4003623LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10) mg/kg 54.050.1 108 70-130
4-Bromofluorobenzene (S) %97 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4003625MATRIX SPIKE SAMPLE:
MSSpike
Result
92664547002
Gas Range Organics (C6-C10) mg/kg 77.163.3 111 57-154ND
4-Bromofluorobenzene (S) %97 66-130
Parameter Units
Dup
Result QualifiersRPDResult
92664547001
4003624SAMPLE DUPLICATE:
Gas Range Organics (C6-C10) mg/kg 98.9 D6,R25755.1
4-Bromofluorobenzene (S) %187 S2158
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663981
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
771359
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples:92663981001, 92663981002, 92663981003, 92663981004, 92663981005, 92663981006, 92663981007,
92663981008, 92663981009, 92663981010, 92663981011, 92663981012, 92663981013, 92663981014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4004364
Associated Lab Samples: 92663981001, 92663981002, 92663981003, 92663981004, 92663981005, 92663981006, 92663981007,
92663981008, 92663981009, 92663981010, 92663981011, 92663981012, 92663981013, 92663981014
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 5.1 05/02/23 14:27
n-Pentacosane (S) % 78 10-133 05/02/23 14:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004365LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28) mg/kg 55.065.6 84 43-130
n-Pentacosane (S) %84 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4004366MATRIX SPIKE SAMPLE:
MSSpike
Result
92663981001
Diesel Range Organics(C10-C28) mg/kg 2870 M177.7 628 15-1302380
n-Pentacosane (S) %S5137 10-133
Parameter Units
Dup
Result QualifiersRPDResult
92663981002
4004367SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28) mg/kg 8250 D64012400
n-Pentacosane (S) %0 S40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663981
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
771767
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92663981015, 92663981016, 92663981017, 92663981018, 92663981019, 92663981020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4006263
Associated Lab Samples:92663981015, 92663981016, 92663981017, 92663981018, 92663981019, 92663981020
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 4.9 05/03/23 09:45
n-Pentacosane (S) % 71 10-133 05/03/23 09:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4006264LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28) mg/kg 52.466.2 79 43-130
n-Pentacosane (S) %78 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4006265MATRIX SPIKE SAMPLE:
MSSpike
Result
92663796007
Diesel Range Organics(C10-C28) mg/kg 19780.3 27 15-130176
n-Pentacosane (S) %57 10-133
Parameter Units
Dup
Result QualifiersRPDResult
92663796008
4006266SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28) mg/kg 4630 D6366690
n-Pentacosane (S) %0 S40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663981
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770299
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples:92663981001, 92663981002, 92663981003, 92663981004, 92663981005, 92663981006, 92663981007,
92663981008, 92663981009
Parameter Units
Dup
Result QualifiersRPDResult
92663770001
3998935SAMPLE DUPLICATE:
Percent Moisture % 13.5 N2113.3
Parameter Units
Dup
Result QualifiersRPDResult
92663981009
3998936SAMPLE DUPLICATE:
Percent Moisture % 13.7 N2912.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663981
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770319
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples:92663981010, 92663981011, 92663981012, 92663981013, 92663981014, 92663981015, 92663981016,
92663981017, 92663981018, 92663981019, 92663981020
Parameter Units
Dup
Result QualifiersRPDResult
92664026001
3999068SAMPLE DUPLICATE:
Percent Moisture % 29.8 N2129.6
Parameter Units
Dup
Result QualifiersRPDResult
92663981020
3999069SAMPLE DUPLICATE:
Percent Moisture % 20.1 N21317.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 39
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92663981
Loves 412 23004903
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
N2
RPD value was outside control limits due to matrix interferenceR2
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).
S2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 39
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92663981
Loves 412 23004903
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92663981001 771359 771478419234903-1 EPA 3546 EPA 8015C
92663981002 771359 771478419234903-2 EPA 3546 EPA 8015C
92663981003 771359 771478419234903-3 EPA 3546 EPA 8015C
92663981004 771359 771478419234903-4 EPA 3546 EPA 8015C
92663981005 771359 771478419234903-5 EPA 3546 EPA 8015C
92663981006 771359 771478419234903-6 EPA 3546 EPA 8015C
92663981007 771359 771478419234903-7 EPA 3546 EPA 8015C
92663981008 771359 771478419234903-8 EPA 3546 EPA 8015C
92663981009 771359 771478419234903-9 EPA 3546 EPA 8015C
92663981010 771359 771478419234903-10 EPA 3546 EPA 8015C
92663981011 771359 771478419234903-11 EPA 3546 EPA 8015C
92663981012 771359 771478419234903-12 EPA 3546 EPA 8015C
92663981013 771359 771478419234903-13 EPA 3546 EPA 8015C
92663981014 771359 771478419234903-14 EPA 3546 EPA 8015C
92663981015 771767 771998419234903-15 EPA 3546 EPA 8015C
92663981016 771767 771998419234903-16 EPA 3546 EPA 8015C
92663981017 771767 771998419234903-17 EPA 3546 EPA 8015C
92663981018 771767 771998419234903-18 EPA 3546 EPA 8015C
92663981019 771767 771998419234903-19 EPA 3546 EPA 8015C
92663981020 771767 771998419234903-20 EPA 3546 EPA 8015C
92663981001 770927 770952419234903-1 EPA 5030B EPA 8015C
92663981002 770927 770952419234903-2 EPA 5030B EPA 8015C
92663981003 770927 770952419234903-3 EPA 5030B EPA 8015C
92663981004 770927 770952419234903-4 EPA 5030B EPA 8015C
92663981005 770927 770952419234903-5 EPA 5030B EPA 8015C
92663981006 770927 770952419234903-6 EPA 5030B EPA 8015C
92663981007 770927 770952419234903-7 EPA 5030B EPA 8015C
92663981008 770927 770952419234903-8 EPA 5030B EPA 8015C
92663981009 770927 770952419234903-9 EPA 5030B EPA 8015C
92663981010 770927 770952419234903-10 EPA 5030B EPA 8015C
92663981011 770927 770952419234903-11 EPA 5030B EPA 8015C
92663981012 770927 770952419234903-12 EPA 5030B EPA 8015C
92663981013 770928 770954419234903-13 EPA 5030B EPA 8015C
92663981014 770928 770954419234903-14 EPA 5030B EPA 8015C
92663981015 771194 771238419234903-15 EPA 5030B EPA 8015C
92663981016 770928 770954419234903-16 EPA 5030B EPA 8015C
92663981017 770928 770954419234903-17 EPA 5030B EPA 8015C
92663981018 770928 770954419234903-18 EPA 5030B EPA 8015C
92663981019 771194 771238419234903-19 EPA 5030B EPA 8015C
92663981020 770928 770954419234903-20 EPA 5030B EPA 8015C
92663981001 770299419234903-1 SW-846
92663981002 770299419234903-2 SW-846
92663981003 770299419234903-3 SW-846
92663981004 770299419234903-4 SW-846
92663981005 770299419234903-5 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 39
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92663981
Loves 412 23004903
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92663981006 770299419234903-6 SW-846
92663981007 770299419234903-7 SW-846
92663981008 770299419234903-8 SW-846
92663981009 770299419234903-9 SW-846
92663981010 770319419234903-10 SW-846
92663981011 770319419234903-11 SW-846
92663981012 770319419234903-12 SW-846
92663981013 770319419234903-13 SW-846
92663981014 770319419234903-14 SW-846
92663981015 770319419234903-15 SW-846
92663981016 770319419234903-16 SW-846
92663981017 770319419234903-17 SW-846
92663981018 770319419234903-18 SW-846
92663981019 770319419234903-19 SW-846
92663981020 770319419234903-20 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 10:56 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 39
Page 35 of 39
Page 36 of 39
Page 37 of 39
Page 38 of 39
Page 39 of 39
#=CL#
May 04, 2023
LIMS USE: FR - MARK RYLAND
LIMS OBJECT ID: 92664200
92664200
Project:
Pace Project No.:
RE:
Mark Ryland
Apex Companies, LLC
203 Wylderose Court
Midlothian, VA 23113
Loves 412 23004903
Dear Mark Ryland:
Enclosed are the analytical results for sample(s) received by the laboratory on April 26, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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[phone]
Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92664200
Loves 412 23004903
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92664200
Loves 412 23004903
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92664200001 425234903-46 EPA 625.1 58 PASI-CPKS
SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664200
Loves 412 23004903
Sample: 425234903-46 Lab ID: 92664200001 Collected: 04/25/23 12:45 Received: 04/26/23 08:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 04/30/23 17:05 83-32-904/28/23 16:4320.8 5
Acenaphthylene ND ug/L 04/30/23 17:05 208-96-804/28/23 16:4320.8 5
Anthracene ND ug/L 04/30/23 17:05 120-12-704/28/23 16:4320.8 5
Benzo(a)anthracene ND ug/L 04/30/23 17:05 56-55-304/28/23 16:4320.8 5
Benzo(a)pyrene ND ug/L 04/30/23 17:05 50-32-804/28/23 16:4320.8 5
Benzo(b)fluoranthene ND ug/L 04/30/23 17:05 205-99-204/28/23 16:4320.8 5
Benzo(g,h,i)perylene ND ug/L 04/30/23 17:05 191-24-204/28/23 16:4320.8 5
Benzo(k)fluoranthene ND ug/L 04/30/23 17:05 207-08-904/28/23 16:4320.8 5
4-Bromophenylphenyl ether ND ug/L 04/30/23 17:05 101-55-304/28/23 16:4320.8 5
Butylbenzylphthalate ND ug/L 04/30/23 17:05 85-68-704/28/23 16:4320.8 5
4-Chloro-3-methylphenol ND ug/L 04/30/23 17:05 59-50-704/28/23 16:4320.8 5
bis(2-Chloroethoxy)methane ND ug/L 04/30/23 17:05 111-91-104/28/23 16:4341.7 5
bis(2-Chloroethyl) ether ND ug/L 04/30/23 17:05 111-44-404/28/23 16:4320.8 5
2-Chloronaphthalene ND ug/L 04/30/23 17:05 91-58-704/28/23 16:4320.8 5
2-Chlorophenol ND ug/L 04/30/23 17:05 95-57-804/28/23 16:4320.8 5
4-Chlorophenylphenyl ether ND ug/L 04/30/23 17:05 7005-72-304/28/23 16:4320.8 5
Chrysene ND ug/L 04/30/23 17:05 218-01-904/28/23 16:4320.8 5
Dibenz(a,h)anthracene ND ug/L 04/30/23 17:05 53-70-304/28/23 16:4320.8 5
3,3'-Dichlorobenzidine ND ug/L 04/30/23 17:05 91-94-104/28/23 16:4341.7 5
2,4-Dichlorophenol ND ug/L 04/30/23 17:05 120-83-204/28/23 16:4320.8 5
Diethylphthalate ND ug/L 04/30/23 17:05 84-66-204/28/23 16:4320.8 5
2,4-Dimethylphenol ND ug/L 04/30/23 17:05 105-67-9 L104/28/23 16:4341.7 5
Dimethylphthalate ND ug/L 04/30/23 17:05 131-11-304/28/23 16:4320.8 5
Di-n-butylphthalate ND ug/L 04/30/23 17:05 84-74-204/28/23 16:4320.8 5
4,6-Dinitro-2-methylphenol ND ug/L 04/30/23 17:05 534-52-104/28/23 16:4341.7 5
2,4-Dinitrophenol ND ug/L 04/30/23 17:05 51-28-504/28/23 16:43208 5
2,4-Dinitrotoluene ND ug/L 04/30/23 17:05 121-14-204/28/23 16:4320.8 5
2,6-Dinitrotoluene ND ug/L 04/30/23 17:05 606-20-204/28/23 16:4320.8 5
Di-n-octylphthalate ND ug/L 04/30/23 17:05 117-84-004/28/23 16:4320.8 5
bis(2-Ethylhexyl)phthalate ND ug/L 04/30/23 17:05 117-81-704/28/23 16:4320.8 5
Fluoranthene ND ug/L 04/30/23 17:05 206-44-004/28/23 16:4320.8 5
Fluorene ND ug/L 04/30/23 17:05 86-73-704/28/23 16:4320.8 5
Hexachloro-1,3-butadiene ND ug/L 04/30/23 17:05 87-68-304/28/23 16:4320.8 5
Hexachlorobenzene ND ug/L 04/30/23 17:05 118-74-104/28/23 16:4320.8 5
Hexachlorocyclopentadiene ND ug/L 04/30/23 17:05 77-47-404/28/23 16:4341.7 5
Hexachloroethane ND ug/L 04/30/23 17:05 67-72-104/28/23 16:4320.8 5
Indeno(1,2,3-cd)pyrene ND ug/L 04/30/23 17:05 193-39-504/28/23 16:4320.8 5
Isophorone ND ug/L 04/30/23 17:05 78-59-104/28/23 16:4341.7 5
Naphthalene ND ug/L 04/30/23 17:05 91-20-304/28/23 16:4320.8 5
Nitrobenzene ND ug/L 04/30/23 17:05 98-95-304/28/23 16:4320.8 5
2-Nitrophenol ND ug/L 04/30/23 17:05 88-75-504/28/23 16:4320.8 5
4-Nitrophenol ND ug/L 04/30/23 17:05 100-02-704/28/23 16:4341.7 5
N-Nitrosodimethylamine ND ug/L 04/30/23 17:05 62-75-904/28/23 16:4320.8 5
N-Nitroso-di-n-propylamine ND ug/L 04/30/23 17:05 621-64-704/28/23 16:4320.8 5
N-Nitrosodiphenylamine ND ug/L 04/30/23 17:05 86-30-604/28/23 16:4341.7 5
2,2'-Oxybis(1-chloropropane) ND ug/L 04/30/23 17:05 108-60-104/28/23 16:4320.8 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664200
Loves 412 23004903
Sample: 425234903-46 Lab ID: 92664200001 Collected: 04/25/23 12:45 Received: 04/26/23 08:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Pentachlorophenol ND ug/L 04/30/23 17:05 87-86-504/28/23 16:4341.7 5
Phenanthrene ND ug/L 04/30/23 17:05 85-01-804/28/23 16:4320.8 5
Phenol ND ug/L 04/30/23 17:05 108-95-204/28/23 16:4320.8 5
Pyrene ND ug/L 04/30/23 17:05 129-00-004/28/23 16:4320.8 5
1,2,4-Trichlorobenzene ND ug/L 04/30/23 17:05 120-82-104/28/23 16:4320.8 5
2,4,6-Trichlorophenol ND ug/L 04/30/23 17:05 88-06-204/28/23 16:4341.7 5
Surrogates
Nitrobenzene-d5 (S) 68 %04/30/23 17:05 4165-60-0 D304/28/23 16:4310-120 5
2-Fluorobiphenyl (S) 58 %04/30/23 17:05 321-60-804/28/23 16:4315-120 5
Terphenyl-d14 (S) 82 %04/30/23 17:05 1718-51-004/28/23 16:4311-131 5
Phenol-d6 (S) 35 %04/30/23 17:05 13127-88-304/28/23 16:4310-120 5
2-Fluorophenol (S) 39 %04/30/23 17:05 367-12-404/28/23 16:4310-120 5
2,4,6-Tribromophenol (S) 67 %04/30/23 17:05 118-79-604/28/23 16:4310-137 5
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 2.0 ug/L 05/03/23 17:08 71-43-20.50 1
Bromobenzene ND ug/L 05/03/23 17:08 108-86-10.50 1
Bromochloromethane ND ug/L 05/03/23 17:08 74-97-50.50 1
Bromodichloromethane ND ug/L 05/03/23 17:08 75-27-40.50 1
Bromoform ND ug/L 05/03/23 17:08 75-25-20.50 1
Bromomethane ND ug/L 05/03/23 17:08 74-83-95.0 1
n-Butylbenzene ND ug/L 05/03/23 17:08 104-51-80.50 1
sec-Butylbenzene ND ug/L 05/03/23 17:08 135-98-80.50 1
tert-Butylbenzene ND ug/L 05/03/23 17:08 98-06-60.50 1
Carbon tetrachloride ND ug/L 05/03/23 17:08 56-23-50.50 1
Chlorobenzene ND ug/L 05/03/23 17:08 108-90-70.50 1
Chloroethane ND ug/L 05/03/23 17:08 75-00-3 L11.0 1
Chloroform ND ug/L 05/03/23 17:08 67-66-30.50 1
Chloromethane ND ug/L 05/03/23 17:08 74-87-3 L11.0 1
2-Chlorotoluene ND ug/L 05/03/23 17:08 95-49-80.50 1
4-Chlorotoluene ND ug/L 05/03/23 17:08 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 05/03/23 17:08 96-12-81.0 1
Dibromochloromethane ND ug/L 05/03/23 17:08 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 05/03/23 17:08 106-93-40.50 1
Dibromomethane ND ug/L 05/03/23 17:08 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 05/03/23 17:08 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 05/03/23 17:08 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 05/03/23 17:08 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 05/03/23 17:08 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 05/03/23 17:08 75-34-30.50 1
1,2-Dichloroethane ND ug/L 05/03/23 17:08 107-06-20.50 1
1,1-Dichloroethene ND ug/L 05/03/23 17:08 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 05/03/23 17:08 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 05/03/23 17:08 156-60-50.50 1
1,2-Dichloropropane ND ug/L 05/03/23 17:08 78-87-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664200
Loves 412 23004903
Sample: 425234903-46 Lab ID: 92664200001 Collected: 04/25/23 12:45 Received: 04/26/23 08:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,3-Dichloropropane ND ug/L 05/03/23 17:08 142-28-90.50 1
2,2-Dichloropropane ND ug/L 05/03/23 17:08 594-20-70.50 1
1,1-Dichloropropene ND ug/L 05/03/23 17:08 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 05/03/23 17:08 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 05/03/23 17:08 10061-02-60.50 1
Diisopropyl ether ND ug/L 05/03/23 17:08 108-20-30.50 1
Ethylbenzene 1.1 ug/L 05/03/23 17:08 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 05/03/23 17:08 87-68-32.0 1
Isopropylbenzene (Cumene)1.1 ug/L 05/03/23 17:08 98-82-80.50 1
Methylene Chloride ND ug/L 05/03/23 17:08 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 05/03/23 17:08 1634-04-40.50 1
Naphthalene 30.4 ug/L 05/03/23 17:08 91-20-32.0 1
n-Propylbenzene 1.7 ug/L 05/03/23 17:08 103-65-10.50 1
Styrene ND ug/L 05/03/23 17:08 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 05/03/23 17:08 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 05/03/23 17:08 79-34-50.50 1
Tetrachloroethene ND ug/L 05/03/23 17:08 127-18-40.50 1
Toluene 5.7 ug/L 05/03/23 17:08 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 05/03/23 17:08 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 05/03/23 17:08 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 05/03/23 17:08 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 05/03/23 17:08 79-00-50.50 1
Trichloroethene ND ug/L 05/03/23 17:08 79-01-60.50 1
Trichlorofluoromethane ND ug/L 05/03/23 17:08 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/03/23 17:08 96-18-40.50 1
1,2,4-Trimethylbenzene 4.2 ug/L 05/03/23 17:08 95-63-60.50 1
1,3,5-Trimethylbenzene 2.2 ug/L 05/03/23 17:08 108-67-80.50 1
Vinyl chloride ND ug/L 05/03/23 17:08 75-01-41.0 1
m&p-Xylene 2.5 ug/L 05/03/23 17:08 179601-23-11.0 1
o-Xylene 1.9 ug/L 05/03/23 17:08 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 105 %05/03/23 17:08 17060-07-070-130 1
4-Bromofluorobenzene (S) 99 %05/03/23 17:08 460-00-470-130 1
Toluene-d8 (S) 101 %05/03/23 17:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664200
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
771970
SM 6200B
SM 6200B
6200B MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92664200001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4007426
Associated Lab Samples:92664200001
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/03/23 12:05
1,1,1-Trichloroethane ug/L ND 0.50 05/03/23 12:05
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/03/23 12:05
1,1,2-Trichloroethane ug/L ND 0.50 05/03/23 12:05
1,1-Dichloroethane ug/L ND 0.50 05/03/23 12:05
1,1-Dichloroethene ug/L ND 0.50 05/03/23 12:05
1,1-Dichloropropene ug/L ND 0.50 05/03/23 12:05
1,2,3-Trichlorobenzene ug/L ND 2.0 05/03/23 12:05
1,2,3-Trichloropropane ug/L ND 0.50 05/03/23 12:05
1,2,4-Trichlorobenzene ug/L ND 2.0 05/03/23 12:05
1,2,4-Trimethylbenzene ug/L ND 0.50 05/03/23 12:05
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/03/23 12:05
1,2-Dibromoethane (EDB) ug/L ND 0.50 05/03/23 12:05
1,2-Dichlorobenzene ug/L ND 0.50 05/03/23 12:05
1,2-Dichloroethane ug/L ND 0.50 05/03/23 12:05
1,2-Dichloropropane ug/L ND 0.50 05/03/23 12:05
1,3,5-Trimethylbenzene ug/L ND 0.50 05/03/23 12:05
1,3-Dichlorobenzene ug/L ND 0.50 05/03/23 12:05
1,3-Dichloropropane ug/L ND 0.50 05/03/23 12:05
1,4-Dichlorobenzene ug/L ND 0.50 05/03/23 12:05
2,2-Dichloropropane ug/L ND 0.50 05/03/23 12:05
2-Chlorotoluene ug/L ND 0.50 05/03/23 12:05
4-Chlorotoluene ug/L ND 0.50 05/03/23 12:05
Benzene ug/L ND 0.50 05/03/23 12:05
Bromobenzene ug/L ND 0.50 05/03/23 12:05
Bromochloromethane ug/L ND 0.50 05/03/23 12:05
Bromodichloromethane ug/L ND 0.50 05/03/23 12:05
Bromoform ug/L ND 0.50 05/03/23 12:05
Bromomethane ug/L ND 5.0 05/03/23 12:05
Carbon tetrachloride ug/L ND 0.50 05/03/23 12:05
Chlorobenzene ug/L ND 0.50 05/03/23 12:05
Chloroethane ug/L ND 1.0 05/03/23 12:05
Chloroform ug/L ND 0.50 05/03/23 12:05
Chloromethane ug/L ND 1.0 05/03/23 12:05
cis-1,2-Dichloroethene ug/L ND 0.50 05/03/23 12:05
cis-1,3-Dichloropropene ug/L ND 0.50 05/03/23 12:05
Dibromochloromethane ug/L ND 0.50 05/03/23 12:05
Dibromomethane ug/L ND 0.50 05/03/23 12:05
Dichlorodifluoromethane ug/L ND 0.50 IH05/03/23 12:05
Diisopropyl ether ug/L ND 0.50 05/03/23 12:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664200
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4007426
Associated Lab Samples:92664200001
Matrix: Water
Analyzed
Ethylbenzene ug/L ND 0.50 05/03/23 12:05
Hexachloro-1,3-butadiene ug/L ND 2.0 05/03/23 12:05
Isopropylbenzene (Cumene) ug/L ND 0.50 05/03/23 12:05
m&p-Xylene ug/L ND 1.0 05/03/23 12:05
Methyl-tert-butyl ether ug/L ND 0.50 05/03/23 12:05
Methylene Chloride ug/L ND 2.0 05/03/23 12:05
n-Butylbenzene ug/L ND 0.50 05/03/23 12:05
n-Propylbenzene ug/L ND 0.50 05/03/23 12:05
Naphthalene ug/L ND 2.0 05/03/23 12:05
o-Xylene ug/L ND 0.50 05/03/23 12:05
sec-Butylbenzene ug/L ND 0.50 05/03/23 12:05
Styrene ug/L ND 0.50 05/03/23 12:05
tert-Butylbenzene ug/L ND 0.50 05/03/23 12:05
Tetrachloroethene ug/L ND 0.50 05/03/23 12:05
Toluene ug/L ND 0.50 05/03/23 12:05
trans-1,2-Dichloroethene ug/L ND 0.50 05/03/23 12:05
trans-1,3-Dichloropropene ug/L ND 0.50 05/03/23 12:05
Trichloroethene ug/L ND 0.50 05/03/23 12:05
Trichlorofluoromethane ug/L ND 1.0 05/03/23 12:05
Vinyl chloride ug/L ND 1.0 05/03/23 12:05
1,2-Dichloroethane-d4 (S) % 108 70-130 05/03/23 12:05
4-Bromofluorobenzene (S) % 97 70-130 05/03/23 12:05
Toluene-d8 (S) % 101 70-130 05/03/23 12:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4007427LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 22.420 112 60-140
1,1,1-Trichloroethane ug/L 23.020 115 60-140
1,1,2,2-Tetrachloroethane ug/L 24.620 123 60-140
1,1,2-Trichloroethane ug/L 24.120 121 60-140
1,1-Dichloroethane ug/L 24.620 123 60-140
1,1-Dichloroethene ug/L 24.520 123 60-140
1,1-Dichloropropene ug/L 26.320 131 60-140
1,2,3-Trichlorobenzene ug/L 23.220 116 60-140
1,2,3-Trichloropropane ug/L 23.820 119 60-140
1,2,4-Trichlorobenzene ug/L 22.520 112 60-140
1,2,4-Trimethylbenzene ug/L 23.520 117 60-140
1,2-Dibromo-3-chloropropane ug/L 21.220 106 60-140
1,2-Dibromoethane (EDB) ug/L 24.020 120 60-140
1,2-Dichlorobenzene ug/L 23.120 115 60-140
1,2-Dichloroethane ug/L 24.920 124 60-140
1,2-Dichloropropane ug/L 24.320 122 60-140
1,3,5-Trimethylbenzene ug/L 23.820 119 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664200
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4007427LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 23.220 116 60-140
1,3-Dichloropropane ug/L 23.320 116 60-140
1,4-Dichlorobenzene ug/L 22.420 112 60-140
2,2-Dichloropropane ug/L 25.020 125 60-140
2-Chlorotoluene ug/L 23.020 115 60-140
4-Chlorotoluene ug/L 23.720 118 60-140
Benzene ug/L 23.720 118 60-140
Bromobenzene ug/L 22.320 111 60-140
Bromochloromethane ug/L 24.320 121 60-140
Bromodichloromethane ug/L 21.820 109 60-140
Bromoform ug/L 19.620 98 60-140
Bromomethane ug/L 22.620 113 60-140
Carbon tetrachloride ug/L 20.420 102 60-140
Chlorobenzene ug/L 23.220 116 60-140
Chloroethane ug/L 35.0 L120 175 60-140
Chloroform ug/L 23.820 119 60-140
Chloromethane ug/L 29.4 L120 147 60-140
cis-1,2-Dichloroethene ug/L 24.420 122 60-140
cis-1,3-Dichloropropene ug/L 22.920 114 60-140
Dibromochloromethane ug/L 21.720 109 60-140
Dibromomethane ug/L 22.420 112 60-140
Dichlorodifluoromethane ug/L 40.6 IH,L120 203 60-140
Diisopropyl ether ug/L 23.720 119 60-140
Ethylbenzene ug/L 22.820 114 60-140
Hexachloro-1,3-butadiene ug/L 22.620 113 60-140
Isopropylbenzene (Cumene) ug/L 22.720 114 60-140
m&p-Xylene ug/L 45.040 113 60-140
Methyl-tert-butyl ether ug/L 23.420 117 60-140
Methylene Chloride ug/L 22.920 115 60-140
n-Butylbenzene ug/L 24.820 124 60-140
n-Propylbenzene ug/L 23.020 115 60-140
Naphthalene ug/L 24.720 123 60-140
o-Xylene ug/L 22.620 113 60-140
sec-Butylbenzene ug/L 22.820 114 60-140
Styrene ug/L 23.420 117 60-140
tert-Butylbenzene ug/L 18.620 93 60-140
Tetrachloroethene ug/L 21.120 106 60-140
Toluene ug/L 22.320 112 60-140
trans-1,2-Dichloroethene ug/L 25.320 127 60-140
trans-1,3-Dichloropropene ug/L 22.520 113 60-140
Trichloroethene ug/L 23.320 117 60-140
Trichlorofluoromethane ug/L 24.620 123 60-140
Vinyl chloride ug/L 23.620 118 60-140
1,2-Dichloroethane-d4 (S) %105 70-130
4-Bromofluorobenzene (S) %101 70-130
Toluene-d8 (S) %101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664200
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4007428MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92664356019
4007429
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 107 60-140113 520ND21.5 22.6
1,1,1-Trichloroethane ug/L 20 116 60-140121 520ND23.2 24.3
1,1,2,2-Tetrachloroethane ug/L 20 110 60-140117 620ND22.0 23.4
1,1,2-Trichloroethane ug/L 20 109 60-140114 520ND21.7 22.8
1,1-Dichloroethane ug/L 20 122 60-140128 520ND24.3 25.6
1,1-Dichloroethene ug/L 20 120 60-140126 5200.52 24.4 25.7
1,1-Dichloropropene ug/L 20 132 60-140137 420ND26.3 27.4
1,2,3-Trichlorobenzene ug/L 20 92 60-140100 820ND18.4 19.9
1,2,3-Trichloropropane ug/L 20 105 60-140111 520ND20.9 22.1
1,2,4-Trichlorobenzene ug/L 20 96 60-140102 620ND19.2 20.4
1,2,4-Trimethylbenzene ug/L 20 113 60-140117 420ND22.5 23.4
1,2-Dibromo-3-chloropropane ug/L 20 89 60-14097 820ND17.8 19.3
1,2-Dibromoethane (EDB) ug/L 20 109 60-140115 520ND21.8 22.9
1,2-Dichlorobenzene ug/L 20 108 60-140113 520ND21.5 22.6
1,2-Dichloroethane ug/L 20 114 60-140120 520ND22.9 24.0
1,2-Dichloropropane ug/L 20 117 60-140123 520ND23.4 24.6
1,3,5-Trimethylbenzene ug/L 20 113 60-140119 520ND22.6 23.8
1,3-Dichlorobenzene ug/L 20 113 60-140117 420ND22.6 23.5
1,3-Dichloropropane ug/L 20 111 60-140114 220ND22.2 22.7
1,4-Dichlorobenzene ug/L 20 105 60-140110 520ND20.9 22.0
2,2-Dichloropropane ug/L 20 115 60-140119 420ND22.9 23.9
2-Chlorotoluene ug/L 20 113 60-140119 520ND22.6 23.8
4-Chlorotoluene ug/L 20 115 60-140119 320ND23.0 23.8
Benzene ug/L 20 112 60-140118 520ND22.4 23.6
Bromobenzene ug/L 20 108 60-140112 320ND21.7 22.3
Bromochloromethane ug/L 20 111 60-140116 420ND22.3 23.2
Bromodichloromethane ug/L 20 102 60-140107 420ND20.4 21.3
Bromoform ug/L 20 89 60-14093 520ND17.8 18.6
Bromomethane ug/L 20 72 60-14091 2420ND14.4 18.3
Carbon tetrachloride ug/L 20 103 60-140109 520ND20.6 21.7
Chlorobenzene ug/L 20 112 60-140118 520ND22.4 23.5
Chloroethane ug/L M020154 60-140161 420ND30.8 32.1
Chloroform ug/L 20 119 60-140126 6200.83 24.7 26.1
Chloromethane ug/L 20 85 60-14091 720ND17.0 18.2
cis-1,2-Dichloroethene ug/L 20 119 60-140125 520ND23.7 25.0
cis-1,3-Dichloropropene ug/L 20 99 60-140107 720ND19.9 21.4
Dibromochloromethane ug/L 20 102 60-140106 320ND20.5 21.1
Dibromomethane ug/L 20 103 60-140108 520ND20.5 21.6
Dichlorodifluoromethane ug/L IH2079 60-14081 320ND15.8 16.2
Diisopropyl ether ug/L 20 105 60-140112 620ND21.1 22.3
Ethylbenzene ug/L 20 111 60-140117 520ND22.2 23.4
Hexachloro-1,3-butadiene ug/L 20 101 60-140109 720ND20.2 21.7
Isopropylbenzene (Cumene) ug/L 20 111 60-140118 720ND22.2 23.7
m&p-Xylene ug/L 40 110 60-140115 440ND43.9 45.8
Methyl-tert-butyl ether ug/L 20 101 60-140106 520ND20.1 21.2
Methylene Chloride ug/L 20 104 60-140107 420ND20.7 21.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664200
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4007428MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92664356019
4007429
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 118 60-140123 420ND23.5 24.6
n-Propylbenzene ug/L 20 115 60-140121 520ND23.0 24.1
Naphthalene ug/L 20 97 60-140108 1020ND19.4 21.5
o-Xylene ug/L 20 107 60-140113 520ND21.5 22.5
sec-Butylbenzene ug/L 20 113 60-140119 520ND22.7 23.8
Styrene ug/L 20 108 60-140114 520ND21.7 22.8
tert-Butylbenzene ug/L 20 94 60-14098 520ND18.8 19.7
Tetrachloroethene ug/L 20 105 60-140109 420ND21.0 21.8
Toluene ug/L 20 106 60-140111 4200.35J 21.6 22.6
trans-1,2-Dichloroethene ug/L 20 122 60-140130 620ND24.4 26.0
trans-1,3-Dichloropropene ug/L 20 100 60-140105 520ND20.0 21.1
Trichloroethene ug/L 20 118 60-140123 3208.1 31.8 32.6
Trichlorofluoromethane ug/L 20 116 60-140120 320ND23.2 23.9
Vinyl chloride ug/L 20 86 60-14091 620ND17.2 18.2
1,2-Dichloroethane-d4 (S) %108 70-130106
4-Bromofluorobenzene (S) %98 70-13099
Toluene-d8 (S) %98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664200
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
771013
EPA 625.1
EPA 625.1
625 MSS
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92664200001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4002601
Associated Lab Samples:92664200001
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 04/30/23 11:59
2,2'-Oxybis(1-chloropropane) ug/L ND 5.0 04/30/23 11:59
2,4,6-Trichlorophenol ug/L ND 10.0 04/30/23 11:59
2,4-Dichlorophenol ug/L ND 5.0 04/30/23 11:59
2,4-Dimethylphenol ug/L ND 10.0 04/30/23 11:59
2,4-Dinitrophenol ug/L ND 50.0 04/30/23 11:59
2,4-Dinitrotoluene ug/L ND 5.0 04/30/23 11:59
2,6-Dinitrotoluene ug/L ND 5.0 04/30/23 11:59
2-Chloronaphthalene ug/L ND 5.0 04/30/23 11:59
2-Chlorophenol ug/L ND 5.0 04/30/23 11:59
2-Nitrophenol ug/L ND 5.0 04/30/23 11:59
3,3'-Dichlorobenzidine ug/L ND 10.0 04/30/23 11:59
4,6-Dinitro-2-methylphenol ug/L ND 10.0 04/30/23 11:59
4-Bromophenylphenyl ether ug/L ND 5.0 04/30/23 11:59
4-Chloro-3-methylphenol ug/L ND 5.0 04/30/23 11:59
4-Chlorophenylphenyl ether ug/L ND 5.0 04/30/23 11:59
4-Nitrophenol ug/L ND 10.0 04/30/23 11:59
Acenaphthene ug/L ND 5.0 04/30/23 11:59
Acenaphthylene ug/L ND 5.0 04/30/23 11:59
Anthracene ug/L ND 5.0 04/30/23 11:59
Benzo(a)anthracene ug/L ND 5.0 04/30/23 11:59
Benzo(a)pyrene ug/L ND 5.0 04/30/23 11:59
Benzo(b)fluoranthene ug/L ND 5.0 04/30/23 11:59
Benzo(g,h,i)perylene ug/L ND 5.0 04/30/23 11:59
Benzo(k)fluoranthene ug/L ND 5.0 04/30/23 11:59
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/30/23 11:59
bis(2-Chloroethyl) ether ug/L ND 5.0 04/30/23 11:59
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/30/23 11:59
Butylbenzylphthalate ug/L ND 5.0 04/30/23 11:59
Chrysene ug/L ND 5.0 04/30/23 11:59
Di-n-butylphthalate ug/L ND 5.0 04/30/23 11:59
Di-n-octylphthalate ug/L ND 5.0 04/30/23 11:59
Dibenz(a,h)anthracene ug/L ND 5.0 04/30/23 11:59
Diethylphthalate ug/L ND 5.0 04/30/23 11:59
Dimethylphthalate ug/L ND 5.0 04/30/23 11:59
Fluoranthene ug/L ND 5.0 04/30/23 11:59
Fluorene ug/L ND 5.0 04/30/23 11:59
Hexachloro-1,3-butadiene ug/L ND 5.0 04/30/23 11:59
Hexachlorobenzene ug/L ND 5.0 04/30/23 11:59
Hexachlorocyclopentadiene ug/L ND 10.0 04/30/23 11:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664200
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4002601
Associated Lab Samples:92664200001
Matrix: Water
Analyzed
Hexachloroethane ug/L ND 5.0 04/30/23 11:59
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 04/30/23 11:59
Isophorone ug/L ND 10.0 04/30/23 11:59
N-Nitroso-di-n-propylamine ug/L ND 5.0 04/30/23 11:59
N-Nitrosodimethylamine ug/L ND 5.0 04/30/23 11:59
N-Nitrosodiphenylamine ug/L ND 10.0 04/30/23 11:59
Naphthalene ug/L ND 5.0 04/30/23 11:59
Nitrobenzene ug/L ND 5.0 04/30/23 11:59
Pentachlorophenol ug/L ND 10.0 04/30/23 11:59
Phenanthrene ug/L ND 5.0 04/30/23 11:59
Phenol ug/L ND 5.0 04/30/23 11:59
Pyrene ug/L ND 5.0 04/30/23 11:59
2,4,6-Tribromophenol (S) % 91 10-137 04/30/23 11:59
2-Fluorobiphenyl (S) % 75 15-120 04/30/23 11:59
2-Fluorophenol (S) % 64 10-120 04/30/23 11:59
Nitrobenzene-d5 (S) % 84 10-120 04/30/23 11:59
Phenol-d6 (S) % 53 10-120 04/30/23 11:59
Terphenyl-d14 (S) % 101 11-131 04/30/23 11:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4002602LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 39.350 79 44-142
2,2'-Oxybis(1-chloropropane) ug/L 46.450 93 36-166
2,4,6-Trichlorophenol ug/L 52.150 104 37-144
2,4-Dichlorophenol ug/L 50.650 101 1-191
2,4-Dimethylphenol ug/L 84.9 L150 170 32-119
2,4-Dinitrophenol ug/L 276250 111 1-181
2,4-Dinitrotoluene ug/L 51.650 103 39-139
2,6-Dinitrotoluene ug/L 54.250 108 50-158
2-Chloronaphthalene ug/L 43.750 87 60-118
2-Chlorophenol ug/L 46.250 92 23-134
2-Nitrophenol ug/L 52.150 104 29-182
3,3'-Dichlorobenzidine ug/L 86.7100 87 1-262
4,6-Dinitro-2-methylphenol ug/L 108100 108 1-181
4-Bromophenylphenyl ether ug/L 47.450 95 53-127
4-Chloro-3-methylphenol ug/L 103100 103 22-147
4-Chlorophenylphenyl ether ug/L 45.450 91 25-158
4-Nitrophenol ug/L 145250 58 1-132
Acenaphthene ug/L 46.250 92 47-145
Acenaphthylene ug/L 47.050 94 33-145
Anthracene ug/L 44.250 88 1-166
Benzo(a)anthracene ug/L 46.450 93 33-143
Benzo(a)pyrene ug/L 47.950 96 17-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664200
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4002602LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 50.850 102 24-159
Benzo(g,h,i)perylene ug/L 35.250 70 1-219
Benzo(k)fluoranthene ug/L 51.050 102 11-162
bis(2-Chloroethoxy)methane ug/L 49.550 99 33-184
bis(2-Chloroethyl) ether ug/L 47.150 94 12-158
bis(2-Ethylhexyl)phthalate ug/L 51.650 103 8-158
Butylbenzylphthalate ug/L 55.750 111 1-152
Chrysene ug/L 45.450 91 17-168
Di-n-butylphthalate ug/L 47.450 95 1-118
Di-n-octylphthalate ug/L 48.750 97 4-146
Dibenz(a,h)anthracene ug/L 37.550 75 1-227
Diethylphthalate ug/L 46.950 94 1-114
Dimethylphthalate ug/L 47.050 94 1-112
Fluoranthene ug/L 44.150 88 26-137
Fluorene ug/L 47.350 95 59-121
Hexachloro-1,3-butadiene ug/L 36.350 73 24-116
Hexachlorobenzene ug/L 45.350 91 1-152
Hexachlorocyclopentadiene ug/L 41.750 83 25-150
Hexachloroethane ug/L 34.550 69 40-113
Indeno(1,2,3-cd)pyrene ug/L 37.950 76 1-171
Isophorone ug/L 53.450 107 21-196
N-Nitroso-di-n-propylamine ug/L 52.650 105 1-230
N-Nitrosodimethylamine ug/L 41.150 82 25-150
N-Nitrosodiphenylamine ug/L 48.750 97 25-150
Naphthalene ug/L 41.950 84 21-133
Nitrobenzene ug/L 47.550 95 35-180
Pentachlorophenol ug/L 102100 102 14-176
Phenanthrene ug/L 45.750 91 54-120
Phenol ug/L 31.350 63 5-112
Pyrene ug/L 54.350 109 52-115
2,4,6-Tribromophenol (S) %120 10-137
2-Fluorobiphenyl (S) %104 15-120
2-Fluorophenol (S) %80 10-120
Nitrobenzene-d5 (S) %109 10-120
Phenol-d6 (S) %67 10-120
Terphenyl-d14 (S) %125 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4002603MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92664142001
4002604
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L M1,R110024 44-14249 66100ND24.5 48.7
2,2'-Oxybis(1-chloropropane) ug/L 100 61 36-16676 21100ND61.4 76.1
2,4,6-Trichlorophenol ug/L 100 87 37-14496 10100ND86.9 96.2
2,4-Dichlorophenol ug/L 100 84 1-19192 9100ND84.1 92.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664200
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4002603MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92664142001
4002604
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4-Dimethylphenol ug/L M0100136 32-119150 10100ND136 150
2,4-Dinitrophenol ug/L 500 103 1-18199 4500ND514 494
2,4-Dinitrotoluene ug/L 100 84 39-13989 6100ND84.2 89.2
2,6-Dinitrotoluene ug/L 100 85 50-15897 13100ND84.6 96.6
2-Chloronaphthalene ug/L M1,R110035 60-11858 48100ND35.3 57.7
2-Chlorophenol ug/L 100 79 23-13485 8100ND78.8 85.0
2-Nitrophenol ug/L 100 90 29-18297 7100ND90.0 96.7
3,3'-Dichlorobenzidine ug/L 200 61 1-26255 10200ND123 111
4,6-Dinitro-2-methylphenol ug/L 200 93 1-18196 3200ND187 192
4-Bromophenylphenyl ether ug/L 100 73 53-12787 17100ND73.3 87.1
4-Chloro-3-methylphenol ug/L 200 90 22-14795 6200ND179 190
4-Chlorophenylphenyl ether ug/L 100 67 25-15876 12100ND66.9 75.6
4-Nitrophenol ug/L 500 56 1-13254 3500ND279 271
Acenaphthene ug/L 100 50 47-14567 29100ND49.8 66.7
Acenaphthylene ug/L R110050 33-14569 31100ND50.1 68.8
Anthracene ug/L 100 71 1-16677 8100ND70.8 76.7
Benzo(a)anthracene ug/L 100 78 33-14387 11100ND78.2 87.0
Benzo(a)pyrene ug/L 100 81 17-16385 5100ND80.8 84.6
Benzo(b)fluoranthene ug/L 100 82 24-15991 10100ND82.0 90.6
Benzo(g,h,i)perylene ug/L 100 71 1-21990 24100ND71.0 90.4
Benzo(k)fluoranthene ug/L 100 82 11-16291 9100ND82.4 90.5
bis(2-Chloroethoxy)methane ug/L 100 87 33-18488 2100ND86.6 88.5
bis(2-Chloroethyl) ether ug/L 100 81 12-15886 6100ND81.3 86.3
bis(2-Ethylhexyl)phthalate ug/L 100 84 8-158103 20100ND84.3 103
Butylbenzylphthalate ug/L 100 89 1-152110 21100ND89.1 110
Chrysene ug/L 100 79 17-16886 8100ND79.4 85.8
Di-n-butylphthalate ug/L 100 78 1-11886 9100ND78.3 85.9
Di-n-octylphthalate ug/L 100 87 4-14696 11100ND86.6 96.3
Dibenz(a,h)anthracene ug/L 100 73 1-22790 21100ND73.1 90.2
Diethylphthalate ug/L 100 76 1-11485 12100ND76.0 85.4
Dimethylphthalate ug/L 100 75 1-11285 12100ND75.2 84.5
Fluoranthene ug/L 100 78 26-13780 3100ND78.1 80.2
Fluorene ug/L 100 68 59-12180 16100ND68.2 79.7
Hexachloro-1,3-butadiene ug/L M1,R110020 24-11645 76100ND20.4 45.4
Hexachlorobenzene ug/L 100 71 1-15285 18100ND70.9 85.2
Hexachlorocyclopentadiene ug/L M1,R110021 25-15043 70100ND20.7 43.0
Hexachloroethane ug/L M1,R110022 40-11345 70100ND21.9 45.5
Indeno(1,2,3-cd)pyrene ug/L 100 74 1-17191 20100ND74.2 91.1
Isophorone ug/L 100 91 21-19694 3100ND91.0 94.2
N-Nitroso-di-n-propylamine ug/L 100 89 1-23098 10100ND88.6 98.2
N-Nitrosodimethylamine ug/L 100 82 25-15075 8100ND81.6 75.1
N-Nitrosodiphenylamine ug/L R110049 25-15076 42100ND49.5 75.7
Naphthalene ug/L R110032 21-13354 51100ND32.2 54.4
Nitrobenzene ug/L 100 79 35-18083 5100ND78.6 82.5
Pentachlorophenol ug/L 200 77 14-17692 17200ND155 184
Phenanthrene ug/L 100 75 54-12084 12100ND74.6 83.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664200
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4002603MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92664142001
4002604
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol ug/L 100 64 5-11260 7100ND64.2 60.0
Pyrene ug/L 100 81 52-115105 26100ND81.1 105
2,4,6-Tribromophenol (S) %80 10-137114
2-Fluorobiphenyl (S) %62 15-12080
2-Fluorophenol (S) %66 10-12076
Nitrobenzene-d5 (S) %86 10-12097
Phenol-d6 (S) %56 10-12065
Terphenyl-d14 (S) %84 11-131128
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92664200
Loves 412 23004903
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92664200
Loves 412 23004903
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92664200001 771013 771402425234903-46 EPA 625.1 EPA 625.1
92664200001 771970425234903-46 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 07:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 21
Page 19 of 21
Page 20 of 21
Page 21 of 21
#=CL#
May 11, 2023
LIMS USE: FR - MARK RYLAND
LIMS OBJECT ID: 92664392
92664392
Project:
Pace Project No.:
RE:
Mark Ryland
Apex Companies, LLC
203 Wylderose Court
Midlothian, VA 23113
Loves 412 23004903
Dear Mark Ryland:
Enclosed are the analytical results for sample(s) received by the laboratory on April 27, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sarah Graham for
[e-mail]
Project Manager
Angela Baioni
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92664392
Loves 412 23004903
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92664392
Loves 412 23004903
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92664392001 426234903-72 EPA 625.1 58 PASI-CPKS
SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664392
Loves 412 23004903
Sample: 426234903-72 Lab ID: 92664392001 Collected: 04/26/23 16:00 Received: 04/27/23 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 04/30/23 20:29 83-32-904/29/23 16:2121.7 5
Acenaphthylene ND ug/L 04/30/23 20:29 208-96-804/29/23 16:2121.7 5
Anthracene ND ug/L 04/30/23 20:29 120-12-704/29/23 16:2121.7 5
Benzo(a)anthracene ND ug/L 04/30/23 20:29 56-55-304/29/23 16:2121.7 5
Benzo(a)pyrene ND ug/L 04/30/23 20:29 50-32-804/29/23 16:2121.7 5
Benzo(b)fluoranthene ND ug/L 04/30/23 20:29 205-99-204/29/23 16:2121.7 5
Benzo(g,h,i)perylene ND ug/L 04/30/23 20:29 191-24-204/29/23 16:2121.7 5
Benzo(k)fluoranthene ND ug/L 04/30/23 20:29 207-08-904/29/23 16:2121.7 5
4-Bromophenylphenyl ether ND ug/L 04/30/23 20:29 101-55-304/29/23 16:2121.7 5
Butylbenzylphthalate ND ug/L 04/30/23 20:29 85-68-704/29/23 16:2121.7 5
4-Chloro-3-methylphenol ND ug/L 04/30/23 20:29 59-50-704/29/23 16:2121.7 5
bis(2-Chloroethoxy)methane ND ug/L 04/30/23 20:29 111-91-104/29/23 16:2143.5 5
bis(2-Chloroethyl) ether ND ug/L 04/30/23 20:29 111-44-404/29/23 16:2121.7 5
2-Chloronaphthalene ND ug/L 04/30/23 20:29 91-58-704/29/23 16:2121.7 5
2-Chlorophenol ND ug/L 04/30/23 20:29 95-57-804/29/23 16:2121.7 5
4-Chlorophenylphenyl ether ND ug/L 04/30/23 20:29 7005-72-304/29/23 16:2121.7 5
Chrysene ND ug/L 04/30/23 20:29 218-01-904/29/23 16:2121.7 5
Dibenz(a,h)anthracene ND ug/L 04/30/23 20:29 53-70-304/29/23 16:2121.7 5
3,3'-Dichlorobenzidine ND ug/L 04/30/23 20:29 91-94-104/29/23 16:2143.5 5
2,4-Dichlorophenol ND ug/L 04/30/23 20:29 120-83-204/29/23 16:2121.7 5
Diethylphthalate ND ug/L 04/30/23 20:29 84-66-204/29/23 16:2121.7 5
2,4-Dimethylphenol ND ug/L 04/30/23 20:29 105-67-9 L104/29/23 16:2143.5 5
Dimethylphthalate ND ug/L 04/30/23 20:29 131-11-304/29/23 16:2121.7 5
Di-n-butylphthalate ND ug/L 04/30/23 20:29 84-74-204/29/23 16:2121.7 5
4,6-Dinitro-2-methylphenol ND ug/L 04/30/23 20:29 534-52-104/29/23 16:2143.5 5
2,4-Dinitrophenol ND ug/L 04/30/23 20:29 51-28-504/29/23 16:21217 5
2,4-Dinitrotoluene ND ug/L 04/30/23 20:29 121-14-204/29/23 16:2121.7 5
2,6-Dinitrotoluene ND ug/L 04/30/23 20:29 606-20-204/29/23 16:2121.7 5
Di-n-octylphthalate ND ug/L 04/30/23 20:29 117-84-004/29/23 16:2121.7 5
bis(2-Ethylhexyl)phthalate ND ug/L 04/30/23 20:29 117-81-704/29/23 16:2121.7 5
Fluoranthene ND ug/L 04/30/23 20:29 206-44-004/29/23 16:2121.7 5
Fluorene ND ug/L 04/30/23 20:29 86-73-704/29/23 16:2121.7 5
Hexachloro-1,3-butadiene ND ug/L 04/30/23 20:29 87-68-304/29/23 16:2121.7 5
Hexachlorobenzene ND ug/L 04/30/23 20:29 118-74-104/29/23 16:2121.7 5
Hexachlorocyclopentadiene ND ug/L 04/30/23 20:29 77-47-404/29/23 16:2143.5 5
Hexachloroethane ND ug/L 04/30/23 20:29 67-72-104/29/23 16:2121.7 5
Indeno(1,2,3-cd)pyrene ND ug/L 04/30/23 20:29 193-39-504/29/23 16:2121.7 5
Isophorone ND ug/L 04/30/23 20:29 78-59-104/29/23 16:2143.5 5
Naphthalene ND ug/L 04/30/23 20:29 91-20-304/29/23 16:2121.7 5
Nitrobenzene ND ug/L 04/30/23 20:29 98-95-304/29/23 16:2121.7 5
2-Nitrophenol ND ug/L 04/30/23 20:29 88-75-504/29/23 16:2121.7 5
4-Nitrophenol ND ug/L 04/30/23 20:29 100-02-704/29/23 16:2143.5 5
N-Nitrosodimethylamine ND ug/L 04/30/23 20:29 62-75-904/29/23 16:2121.7 5
N-Nitroso-di-n-propylamine ND ug/L 04/30/23 20:29 621-64-704/29/23 16:2121.7 5
N-Nitrosodiphenylamine ND ug/L 04/30/23 20:29 86-30-604/29/23 16:2143.5 5
2,2'-Oxybis(1-chloropropane) ND ug/L 04/30/23 20:29 108-60-104/29/23 16:2121.7 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664392
Loves 412 23004903
Sample: 426234903-72 Lab ID: 92664392001 Collected: 04/26/23 16:00 Received: 04/27/23 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Pentachlorophenol ND ug/L 04/30/23 20:29 87-86-504/29/23 16:2143.5 5
Phenanthrene ND ug/L 04/30/23 20:29 85-01-804/29/23 16:2121.7 5
Phenol ND ug/L 04/30/23 20:29 108-95-204/29/23 16:2121.7 5
Pyrene ND ug/L 04/30/23 20:29 129-00-004/29/23 16:2121.7 5
1,2,4-Trichlorobenzene ND ug/L 04/30/23 20:29 120-82-104/29/23 16:2121.7 5
2,4,6-Trichlorophenol ND ug/L 04/30/23 20:29 88-06-204/29/23 16:2143.5 5
Surrogates
Nitrobenzene-d5 (S) 74 %04/30/23 20:29 4165-60-0 D304/29/23 16:2110-120 5
2-Fluorobiphenyl (S) 62 %04/30/23 20:29 321-60-804/29/23 16:2115-120 5
Terphenyl-d14 (S) 82 %04/30/23 20:29 1718-51-004/29/23 16:2111-131 5
Phenol-d6 (S) 42 %04/30/23 20:29 13127-88-304/29/23 16:2110-120 5
2-Fluorophenol (S) 49 %04/30/23 20:29 367-12-404/29/23 16:2110-120 5
2,4,6-Tribromophenol (S) 72 %04/30/23 20:29 118-79-604/29/23 16:2110-137 5
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 2.0 ug/L 05/09/23 19:54 71-43-20.50 1
Bromobenzene ND ug/L 05/09/23 19:54 108-86-10.50 1
Bromochloromethane ND ug/L 05/09/23 19:54 74-97-50.50 1
Bromodichloromethane ND ug/L 05/09/23 19:54 75-27-40.50 1
Bromoform ND ug/L 05/09/23 19:54 75-25-20.50 1
Bromomethane ND ug/L 05/09/23 19:54 74-83-95.0 1
n-Butylbenzene ND ug/L 05/09/23 19:54 104-51-80.50 1
sec-Butylbenzene ND ug/L 05/09/23 19:54 135-98-80.50 1
tert-Butylbenzene ND ug/L 05/09/23 19:54 98-06-60.50 1
Carbon tetrachloride ND ug/L 05/09/23 19:54 56-23-50.50 1
Chlorobenzene ND ug/L 05/09/23 19:54 108-90-70.50 1
Chloroethane ND ug/L 05/09/23 19:54 75-00-3 L11.0 1
Chloroform ND ug/L 05/09/23 19:54 67-66-30.50 1
Chloromethane ND ug/L 05/09/23 19:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/09/23 19:54 95-49-80.50 1
4-Chlorotoluene ND ug/L 05/09/23 19:54 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 05/09/23 19:54 96-12-81.0 1
Dibromochloromethane ND ug/L 05/09/23 19:54 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 05/09/23 19:54 106-93-40.50 1
Dibromomethane ND ug/L 05/09/23 19:54 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 05/09/23 19:54 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 05/09/23 19:54 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 05/09/23 19:54 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 05/09/23 19:54 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 05/09/23 19:54 75-34-30.50 1
1,2-Dichloroethane ND ug/L 05/09/23 19:54 107-06-20.50 1
1,1-Dichloroethene ND ug/L 05/09/23 19:54 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 05/09/23 19:54 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 05/09/23 19:54 156-60-50.50 1
1,2-Dichloropropane ND ug/L 05/09/23 19:54 78-87-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664392
Loves 412 23004903
Sample: 426234903-72 Lab ID: 92664392001 Collected: 04/26/23 16:00 Received: 04/27/23 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,3-Dichloropropane ND ug/L 05/09/23 19:54 142-28-90.50 1
2,2-Dichloropropane ND ug/L 05/09/23 19:54 594-20-70.50 1
1,1-Dichloropropene ND ug/L 05/09/23 19:54 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 05/09/23 19:54 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 05/09/23 19:54 10061-02-60.50 1
Diisopropyl ether ND ug/L 05/09/23 19:54 108-20-30.50 1
Ethylbenzene 2.1 ug/L 05/09/23 19:54 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 05/09/23 19:54 87-68-32.0 1
Isopropylbenzene (Cumene)2.2 ug/L 05/09/23 19:54 98-82-80.50 1
Methylene Chloride ND ug/L 05/09/23 19:54 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 05/09/23 19:54 1634-04-40.50 1
Naphthalene 37.3 ug/L 05/09/23 19:54 91-20-32.0 1
n-Propylbenzene 3.3 ug/L 05/09/23 19:54 103-65-10.50 1
Styrene ND ug/L 05/09/23 19:54 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 05/09/23 19:54 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 05/09/23 19:54 79-34-50.50 1
Tetrachloroethene ND ug/L 05/09/23 19:54 127-18-40.50 1
Toluene 8.6 ug/L 05/09/23 19:54 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 05/09/23 19:54 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 05/09/23 19:54 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 05/09/23 19:54 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 05/09/23 19:54 79-00-50.50 1
Trichloroethene ND ug/L 05/09/23 19:54 79-01-60.50 1
Trichlorofluoromethane ND ug/L 05/09/23 19:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/09/23 19:54 96-18-40.50 1
1,2,4-Trimethylbenzene 5.7 ug/L 05/09/23 19:54 95-63-60.50 1
1,3,5-Trimethylbenzene 3.8 ug/L 05/09/23 19:54 108-67-80.50 1
Vinyl chloride ND ug/L 05/09/23 19:54 75-01-41.0 1
m&p-Xylene 5.0 ug/L 05/09/23 19:54 179601-23-11.0 1
o-Xylene 3.4 ug/L 05/09/23 19:54 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 107 %05/09/23 19:54 17060-07-070-130 1
4-Bromofluorobenzene (S) 97 %05/09/23 19:54 460-00-470-130 1
Toluene-d8 (S) 101 %05/09/23 19:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664392
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
773195
SM 6200B
SM 6200B
6200B MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92664392001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4013171
Associated Lab Samples:92664392001
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/09/23 11:42
1,1,1-Trichloroethane ug/L ND 0.50 05/09/23 11:42
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/09/23 11:42
1,1,2-Trichloroethane ug/L ND 0.50 05/09/23 11:42
1,1-Dichloroethane ug/L ND 0.50 05/09/23 11:42
1,1-Dichloroethene ug/L ND 0.50 05/09/23 11:42
1,1-Dichloropropene ug/L ND 0.50 05/09/23 11:42
1,2,3-Trichlorobenzene ug/L ND 2.0 05/09/23 11:42
1,2,3-Trichloropropane ug/L ND 0.50 05/09/23 11:42
1,2,4-Trichlorobenzene ug/L ND 2.0 05/09/23 11:42
1,2,4-Trimethylbenzene ug/L ND 0.50 05/09/23 11:42
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/09/23 11:42
1,2-Dibromoethane (EDB) ug/L ND 0.50 05/09/23 11:42
1,2-Dichlorobenzene ug/L ND 0.50 05/09/23 11:42
1,2-Dichloroethane ug/L ND 0.50 05/09/23 11:42
1,2-Dichloropropane ug/L ND 0.50 05/09/23 11:42
1,3,5-Trimethylbenzene ug/L ND 0.50 05/09/23 11:42
1,3-Dichlorobenzene ug/L ND 0.50 05/09/23 11:42
1,3-Dichloropropane ug/L ND 0.50 05/09/23 11:42
1,4-Dichlorobenzene ug/L ND 0.50 05/09/23 11:42
2,2-Dichloropropane ug/L ND 0.50 05/09/23 11:42
2-Chlorotoluene ug/L ND 0.50 05/09/23 11:42
4-Chlorotoluene ug/L ND 0.50 05/09/23 11:42
Benzene ug/L ND 0.50 05/09/23 11:42
Bromobenzene ug/L ND 0.50 05/09/23 11:42
Bromochloromethane ug/L ND 0.50 05/09/23 11:42
Bromodichloromethane ug/L ND 0.50 05/09/23 11:42
Bromoform ug/L ND 0.50 05/09/23 11:42
Bromomethane ug/L ND 5.0 05/09/23 11:42
Carbon tetrachloride ug/L ND 0.50 05/09/23 11:42
Chlorobenzene ug/L ND 0.50 05/09/23 11:42
Chloroethane ug/L ND 1.0 05/09/23 11:42
Chloroform ug/L ND 0.50 05/09/23 11:42
Chloromethane ug/L ND 1.0 05/09/23 11:42
cis-1,2-Dichloroethene ug/L ND 0.50 05/09/23 11:42
cis-1,3-Dichloropropene ug/L ND 0.50 05/09/23 11:42
Dibromochloromethane ug/L ND 0.50 05/09/23 11:42
Dibromomethane ug/L ND 0.50 05/09/23 11:42
Dichlorodifluoromethane ug/L ND 0.50 IH05/09/23 11:42
Diisopropyl ether ug/L ND 0.50 05/09/23 11:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664392
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4013171
Associated Lab Samples:92664392001
Matrix: Water
Analyzed
Ethylbenzene ug/L ND 0.50 05/09/23 11:42
Hexachloro-1,3-butadiene ug/L ND 2.0 05/09/23 11:42
Isopropylbenzene (Cumene) ug/L ND 0.50 05/09/23 11:42
m&p-Xylene ug/L ND 1.0 05/09/23 11:42
Methyl-tert-butyl ether ug/L ND 0.50 05/09/23 11:42
Methylene Chloride ug/L ND 2.0 05/09/23 11:42
n-Butylbenzene ug/L ND 0.50 05/09/23 11:42
n-Propylbenzene ug/L ND 0.50 05/09/23 11:42
Naphthalene ug/L ND 2.0 05/09/23 11:42
o-Xylene ug/L ND 0.50 05/09/23 11:42
sec-Butylbenzene ug/L ND 0.50 05/09/23 11:42
Styrene ug/L ND 0.50 05/09/23 11:42
tert-Butylbenzene ug/L ND 0.50 05/09/23 11:42
Tetrachloroethene ug/L ND 0.50 05/09/23 11:42
Toluene ug/L ND 0.50 05/09/23 11:42
trans-1,2-Dichloroethene ug/L ND 0.50 05/09/23 11:42
trans-1,3-Dichloropropene ug/L ND 0.50 05/09/23 11:42
Trichloroethene ug/L ND 0.50 05/09/23 11:42
Trichlorofluoromethane ug/L ND 1.0 05/09/23 11:42
Vinyl chloride ug/L ND 1.0 05/09/23 11:42
1,2-Dichloroethane-d4 (S) % 108 70-130 05/09/23 11:42
4-Bromofluorobenzene (S) % 95 70-130 05/09/23 11:42
Toluene-d8 (S) % 100 70-130 05/09/23 11:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4013172LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.220 106 60-140
1,1,1-Trichloroethane ug/L 21.920 109 60-140
1,1,2,2-Tetrachloroethane ug/L 22.820 114 60-140
1,1,2-Trichloroethane ug/L 21.720 109 60-140
1,1-Dichloroethane ug/L 23.320 116 60-140
1,1-Dichloroethene ug/L 23.520 118 60-140
1,1-Dichloropropene ug/L 24.720 124 60-140
1,2,3-Trichlorobenzene ug/L 21.120 105 60-140
1,2,3-Trichloropropane ug/L 20.920 104 60-140
1,2,4-Trichlorobenzene ug/L 21.420 107 60-140
1,2,4-Trimethylbenzene ug/L 22.220 111 60-140
1,2-Dibromo-3-chloropropane ug/L 19.320 97 60-140
1,2-Dibromoethane (EDB) ug/L 22.320 111 60-140
1,2-Dichlorobenzene ug/L 21.720 108 60-140
1,2-Dichloroethane ug/L 22.720 113 60-140
1,2-Dichloropropane ug/L 22.320 111 60-140
1,3,5-Trimethylbenzene ug/L 22.120 110 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664392
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4013172LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 22.120 110 60-140
1,3-Dichloropropane ug/L 21.720 108 60-140
1,4-Dichlorobenzene ug/L 21.220 106 60-140
2,2-Dichloropropane ug/L 23.320 116 60-140
2-Chlorotoluene ug/L 22.020 110 60-140
4-Chlorotoluene ug/L 22.820 114 60-140
Benzene ug/L 21.820 109 60-140
Bromobenzene ug/L 21.220 106 60-140
Bromochloromethane ug/L 22.520 113 60-140
Bromodichloromethane ug/L 19.920 100 60-140
Bromoform ug/L 18.320 91 60-140
Bromomethane ug/L 23.120 116 60-140
Carbon tetrachloride ug/L 19.920 100 60-140
Chlorobenzene ug/L 22.020 110 60-140
Chloroethane ug/L 31.1 L120 156 60-140
Chloroform ug/L 22.820 114 60-140
Chloromethane ug/L 25.920 129 60-140
cis-1,2-Dichloroethene ug/L 22.520 112 60-140
cis-1,3-Dichloropropene ug/L 20.820 104 60-140
Dibromochloromethane ug/L 20.320 101 60-140
Dibromomethane ug/L 21.320 106 60-140
Dichlorodifluoromethane ug/L 36.2 IH,L120 181 60-140
Diisopropyl ether ug/L 21.020 105 60-140
Ethylbenzene ug/L 21.420 107 60-140
Hexachloro-1,3-butadiene ug/L 21.720 109 60-140
Isopropylbenzene (Cumene) ug/L 21.420 107 60-140
m&p-Xylene ug/L 42.540 106 60-140
Methyl-tert-butyl ether ug/L 20.720 103 60-140
Methylene Chloride ug/L 19.620 98 60-140
n-Butylbenzene ug/L 23.620 118 60-140
n-Propylbenzene ug/L 22.020 110 60-140
Naphthalene ug/L 23.320 117 60-140
o-Xylene ug/L 21.420 107 60-140
sec-Butylbenzene ug/L 21.820 109 60-140
Styrene ug/L 21.820 109 60-140
tert-Butylbenzene ug/L 18.120 90 60-140
Tetrachloroethene ug/L 20.320 102 60-140
Toluene ug/L 20.520 103 60-140
trans-1,2-Dichloroethene ug/L 23.820 119 60-140
trans-1,3-Dichloropropene ug/L 20.220 101 60-140
Trichloroethene ug/L 22.120 111 60-140
Trichlorofluoromethane ug/L 23.820 119 60-140
Vinyl chloride ug/L 21.420 107 60-140
1,2-Dichloroethane-d4 (S) %106 70-130
4-Bromofluorobenzene (S) %101 70-130
Toluene-d8 (S) %98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664392
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4013173MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92665044002
4013174
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 111 60-140113 220<0.31 22.3 22.6
1,1,1-Trichloroethane ug/L 20 119 60-140122 320<0.33 23.7 24.5
1,1,2,2-Tetrachloroethane ug/L 20 114 60-140115 120<0.22 22.9 23.1
1,1,2-Trichloroethane ug/L 20 114 60-140115 120<0.32 22.8 23.0
1,1-Dichloroethane ug/L 20 125 60-140128 220<0.37 25.0 25.5
1,1-Dichloroethene ug/L 20 128 60-140135 520<0.35 25.7 27.0
1,1-Dichloropropene ug/L M120137 60-140142 320<0.43 27.4 28.4
1,2,3-Trichlorobenzene ug/L 20 101 60-140103 120<0.81 20.3 20.5
1,2,3-Trichloropropane ug/L 20 109 60-140109 020<0.26 21.8 21.9
1,2,4-Trichlorobenzene ug/L 20 102 60-140107 520<0.64 20.3 21.5
1,2,4-Trimethylbenzene ug/L 20 117 60-140117 020<0.50 23.4 23.4
1,2-Dibromo-3-chloropropane ug/L 20 96 60-14095 120<0.34 19.2 19.0
1,2-Dibromoethane (EDB) ug/L 20 115 60-140116 120<0.27 23.0 23.2
1,2-Dichlorobenzene ug/L 20 112 60-140113 120<0.34 22.4 22.5
1,2-Dichloroethane ug/L 20 116 60-140120 420<0.32 23.2 24.1
1,2-Dichloropropane ug/L 20 119 60-140120 120<0.36 23.9 24.0
1,3,5-Trimethylbenzene ug/L 20 118 60-140119 120<0.33 23.5 23.9
1,3-Dichlorobenzene ug/L 20 114 60-140117 220<0.34 22.7 23.3
1,3-Dichloropropane ug/L 20 113 60-140114 120<0.28 22.6 22.9
1,4-Dichlorobenzene ug/L 20 108 60-140111 320<0.33 21.6 22.2
2,2-Dichloropropane ug/L 20 124 60-140129 420<0.39 24.9 25.9
2-Chlorotoluene ug/L 20 117 60-140118 220<0.32 23.3 23.7
4-Chlorotoluene ug/L 20 116 60-140119 220<0.32 23.3 23.8
Benzene ug/L 20 118 60-140121 220<0.34 23.6 24.2
Bromobenzene ug/L 20 111 60-140113 220<0.29 22.2 22.7
Bromochloromethane ug/L 20 116 60-140120 320<0.47 23.3 23.9
Bromodichloromethane ug/L 20 104 60-140108 420<0.31 20.8 21.6
Bromoform ug/L 20 93 60-14095 220<0.34 18.6 19.0
Bromomethane ug/L 20 119 60-140124 420<1.7 23.8 24.8
Carbon tetrachloride ug/L 20 107 60-140113 520<0.33 21.5 22.6
Chlorobenzene ug/L 20 116 60-140119 320<0.28 23.1 23.8
Chloroethane ug/L M020175 60-140184 520<0.65 35.1 36.9
Chloroform ug/L 20 118 60-140127 7200.80 24.3 26.2
Chloromethane ug/L M120142 60-140149 520<0.54 28.4 29.7
cis-1,2-Dichloroethene ug/L 20 121 60-140125 320<0.38 24.3 25.0
cis-1,3-Dichloropropene ug/L 20 108 60-140110 220<0.36 21.5 22.0
Dibromochloromethane ug/L 20 105 60-140107 220<0.36 21.1 21.5
Dibromomethane ug/L 20 106 60-140108 220<0.39 21.2 21.6
Dichlorodifluoromethane ug/L IH,M020206 60-140216 420<0.35 41.3 43.2
Diisopropyl ether ug/L 20 112 60-140113 120<0.31 22.4 22.6
Ethylbenzene ug/L 20 116 60-140118 220<0.30 23.2 23.7
Hexachloro-1,3-butadiene ug/L 20 112 60-140117 520<1.5 22.4 23.5
Isopropylbenzene (Cumene) ug/L 20 116 60-140121 420<0.33 23.1 24.1
m&p-Xylene ug/L 40 115 60-140118 340<0.71 45.9 47.1
Methyl-tert-butyl ether ug/L 20 108 60-140109 120<0.42 21.7 21.9
Methylene Chloride ug/L 20 111 60-140114 320<2.0 22.3 22.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664392
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4013173MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92665044002
4013174
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 122 60-140126 320<0.49 24.5 25.3
n-Propylbenzene ug/L 20 118 60-140121 220<0.34 23.6 24.2
Naphthalene ug/L 20 110 60-140110 020<0.64 22.0 22.1
o-Xylene ug/L 20 113 60-140116 320<0.34 22.5 23.2
sec-Butylbenzene ug/L 20 118 60-140120 220<0.40 23.6 24.0
Styrene ug/L 20 113 60-140117 320<0.29 22.6 23.4
tert-Butylbenzene ug/L 20 96 60-14099 220<0.32 19.3 19.7
Tetrachloroethene ug/L 20 109 60-140112 220<0.29 21.9 22.3
Toluene ug/L 20 111 60-140114 320<0.24 22.2 22.8
trans-1,2-Dichloroethene ug/L 20 129 60-140133 320<0.40 25.8 26.6
trans-1,3-Dichloropropene ug/L 20 104 60-140109 420<0.36 20.8 21.7
Trichloroethene ug/L 20 119 60-140123 320<0.38 23.8 24.6
Trichlorofluoromethane ug/L 20 130 60-140134 320<0.30 26.0 26.9
Vinyl chloride ug/L 20 124 60-140126 220<0.39 24.8 25.2
1,2-Dichloroethane-d4 (S) %105 70-130106
4-Bromofluorobenzene (S) %99 70-13099
Toluene-d8 (S) %99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664392
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
771272
EPA 625.1
EPA 625.1
625 MSS
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92664392001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4004087
Associated Lab Samples:92664392001
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 04/30/23 11:08
2,2'-Oxybis(1-chloropropane) ug/L ND 5.0 04/30/23 11:08
2,4,6-Trichlorophenol ug/L ND 10.0 04/30/23 11:08
2,4-Dichlorophenol ug/L ND 5.0 04/30/23 11:08
2,4-Dimethylphenol ug/L ND 10.0 04/30/23 11:08
2,4-Dinitrophenol ug/L ND 50.0 04/30/23 11:08
2,4-Dinitrotoluene ug/L ND 5.0 04/30/23 11:08
2,6-Dinitrotoluene ug/L ND 5.0 04/30/23 11:08
2-Chloronaphthalene ug/L ND 5.0 04/30/23 11:08
2-Chlorophenol ug/L ND 5.0 04/30/23 11:08
2-Nitrophenol ug/L ND 5.0 04/30/23 11:08
3,3'-Dichlorobenzidine ug/L ND 10.0 04/30/23 11:08
4,6-Dinitro-2-methylphenol ug/L ND 10.0 04/30/23 11:08
4-Bromophenylphenyl ether ug/L ND 5.0 04/30/23 11:08
4-Chloro-3-methylphenol ug/L ND 5.0 04/30/23 11:08
4-Chlorophenylphenyl ether ug/L ND 5.0 04/30/23 11:08
4-Nitrophenol ug/L ND 10.0 04/30/23 11:08
Acenaphthene ug/L ND 5.0 04/30/23 11:08
Acenaphthylene ug/L ND 5.0 04/30/23 11:08
Anthracene ug/L ND 5.0 04/30/23 11:08
Benzo(a)anthracene ug/L ND 5.0 04/30/23 11:08
Benzo(a)pyrene ug/L ND 5.0 04/30/23 11:08
Benzo(b)fluoranthene ug/L ND 5.0 04/30/23 11:08
Benzo(g,h,i)perylene ug/L ND 5.0 04/30/23 11:08
Benzo(k)fluoranthene ug/L ND 5.0 04/30/23 11:08
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/30/23 11:08
bis(2-Chloroethyl) ether ug/L ND 5.0 04/30/23 11:08
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/30/23 11:08
Butylbenzylphthalate ug/L ND 5.0 04/30/23 11:08
Chrysene ug/L ND 5.0 04/30/23 11:08
Di-n-butylphthalate ug/L ND 5.0 04/30/23 11:08
Di-n-octylphthalate ug/L ND 5.0 04/30/23 11:08
Dibenz(a,h)anthracene ug/L ND 5.0 04/30/23 11:08
Diethylphthalate ug/L ND 5.0 04/30/23 11:08
Dimethylphthalate ug/L ND 5.0 04/30/23 11:08
Fluoranthene ug/L ND 5.0 04/30/23 11:08
Fluorene ug/L ND 5.0 04/30/23 11:08
Hexachloro-1,3-butadiene ug/L ND 5.0 04/30/23 11:08
Hexachlorobenzene ug/L ND 5.0 04/30/23 11:08
Hexachlorocyclopentadiene ug/L ND 10.0 04/30/23 11:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664392
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4004087
Associated Lab Samples:92664392001
Matrix: Water
Analyzed
Hexachloroethane ug/L ND 5.0 04/30/23 11:08
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 04/30/23 11:08
Isophorone ug/L ND 10.0 04/30/23 11:08
N-Nitroso-di-n-propylamine ug/L ND 5.0 04/30/23 11:08
N-Nitrosodimethylamine ug/L ND 5.0 04/30/23 11:08
N-Nitrosodiphenylamine ug/L ND 10.0 04/30/23 11:08
Naphthalene ug/L ND 5.0 04/30/23 11:08
Nitrobenzene ug/L ND 5.0 04/30/23 11:08
Pentachlorophenol ug/L ND 10.0 04/30/23 11:08
Phenanthrene ug/L ND 5.0 04/30/23 11:08
Phenol ug/L ND 5.0 04/30/23 11:08
Pyrene ug/L ND 5.0 04/30/23 11:08
2,4,6-Tribromophenol (S) % 91 10-137 04/30/23 11:08
2-Fluorobiphenyl (S) % 76 15-120 04/30/23 11:08
2-Fluorophenol (S) % 63 10-120 04/30/23 11:08
Nitrobenzene-d5 (S) % 84 10-120 04/30/23 11:08
Phenol-d6 (S) % 52 10-120 04/30/23 11:08
Terphenyl-d14 (S) % 112 11-131 04/30/23 11:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004088LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 28.750 57 44-142
2,2'-Oxybis(1-chloropropane) ug/L 44.850 90 36-166
2,4,6-Trichlorophenol ug/L 50.950 102 37-144
2,4-Dichlorophenol ug/L 49.350 99 1-191
2,4-Dimethylphenol ug/L 78.5 L150 157 32-119
2,4-Dinitrophenol ug/L 291250 116 1-181
2,4-Dinitrotoluene ug/L 51.250 102 39-139
2,6-Dinitrotoluene ug/L 52.250 104 50-158
2-Chloronaphthalene ug/L 38.150 76 60-118
2-Chlorophenol ug/L 47.350 95 23-134
2-Nitrophenol ug/L 51.950 104 29-182
3,3'-Dichlorobenzidine ug/L 82.5100 83 1-262
4,6-Dinitro-2-methylphenol ug/L 106100 106 1-181
4-Bromophenylphenyl ether ug/L 44.850 90 53-127
4-Chloro-3-methylphenol ug/L 101100 101 22-147
4-Chlorophenylphenyl ether ug/L 43.350 87 25-158
4-Nitrophenol ug/L 150250 60 1-132
Acenaphthene ug/L 42.750 85 47-145
Acenaphthylene ug/L 42.750 85 33-145
Anthracene ug/L 40.250 80 1-166
Benzo(a)anthracene ug/L 43.150 86 33-143
Benzo(a)pyrene ug/L 43.250 86 17-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664392
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004088LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 48.050 96 24-159
Benzo(g,h,i)perylene ug/L 34.150 68 1-219
Benzo(k)fluoranthene ug/L 47.350 95 11-162
bis(2-Chloroethoxy)methane ug/L 48.750 97 33-184
bis(2-Chloroethyl) ether ug/L 47.150 94 12-158
bis(2-Ethylhexyl)phthalate ug/L 49.650 99 8-158
Butylbenzylphthalate ug/L 53.250 106 1-152
Chrysene ug/L 43.950 88 17-168
Di-n-butylphthalate ug/L 44.650 89 1-118
Di-n-octylphthalate ug/L 45.750 91 4-146
Dibenz(a,h)anthracene ug/L 36.550 73 1-227
Diethylphthalate ug/L 47.250 94 1-114
Dimethylphthalate ug/L 46.750 93 1-112
Fluoranthene ug/L 41.750 83 26-137
Fluorene ug/L 45.550 91 59-121
Hexachloro-1,3-butadiene ug/L 25.150 50 24-116
Hexachlorobenzene ug/L 41.950 84 1-152
Hexachlorocyclopentadiene ug/L 29.850 60 25-150
Hexachloroethane ug/L 24.050 48 40-113
Indeno(1,2,3-cd)pyrene ug/L 36.350 73 1-171
Isophorone ug/L 51.550 103 21-196
N-Nitroso-di-n-propylamine ug/L 52.950 106 1-230
N-Nitrosodimethylamine ug/L 41.350 83 25-150
N-Nitrosodiphenylamine ug/L 45.150 90 25-150
Naphthalene ug/L 34.350 69 21-133
Nitrobenzene ug/L 46.550 93 35-180
Pentachlorophenol ug/L 95.6100 96 14-176
Phenanthrene ug/L 43.150 86 54-120
Phenol ug/L 32.350 65 5-112
Pyrene ug/L 51.650 103 52-115
2,4,6-Tribromophenol (S) %97 10-137
2-Fluorobiphenyl (S) %79 15-120
2-Fluorophenol (S) %72 10-120
Nitrobenzene-d5 (S) %92 10-120
Phenol-d6 (S) %59 10-120
Terphenyl-d14 (S) %102 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4004091MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35795500001
4004092
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 83.3 47 44-14256 1683.31.4U 39.5 46.3
2,2'-Oxybis(1-chloropropane) ug/L 83.3 50 36-16660 1983.30.96U 41.3 50.1
2,4,6-Trichlorophenol ug/L 83.3 63 37-14481 2583.31.3U 52.3 67.5
2,4-Dichlorophenol ug/L 83.3 60 1-19172 1983.31.2U 49.9 60.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664392
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4004091MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35795500001
4004092
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4-Dimethylphenol ug/L M083.3 102 32-119123 1983.31.4U 84.7 103
2,4-Dinitrophenol ug/L 417 61 1-18171 1541721.7U 255 296
2,4-Dinitrotoluene ug/L 83.3 70 39-13984 1883.31.4U 58.6 70.3
2,6-Dinitrotoluene ug/L 83.3 66 50-15880 1983.31.4U 54.6 66.4
2-Chloronaphthalene ug/L M183.3 54 60-11864 1783.31.4U 45.1 53.2
2-Chlorophenol ug/L 83.3 54 23-13470 2683.31.0U 44.7 58.0
2-Nitrophenol ug/L 83.3 64 29-18275 1683.31.2U 53.3 62.7
3,3'-Dichlorobenzidine ug/L 167 61 1-26271 151676.8U 102 118
4,6-Dinitro-2-methylphenol ug/L 167 69 1-18188 241676.5U 115 147
4-Bromophenylphenyl ether ug/L R183.3 58 53-12780 3183.31.5U 48.6 66.6
4-Chloro-3-methylphenol ug/L 167 59 22-14778 281672.8U 98.1 130
4-Chlorophenylphenyl ether ug/L 83.3 54 25-15868 2383.31.7U 45.3 56.9
4-Nitrophenol ug/L 417 45 1-13247 44175.5U 187 195
Acenaphthene ug/L 83.3 54 47-14565 1883.31.7U 45.4 54.5
Acenaphthylene ug/L 83.3 55 33-14567 1983.31.6U 46.0 55.8
Anthracene ug/L 83.3 60 1-16678 2683.31.9U 49.9 64.6
Benzo(a)anthracene ug/L 83.3 77 33-14388 1383.32.2U 64.0 73.2
Benzo(a)pyrene ug/L 83.3 74 17-16384 1283.32.3U 61.9 70.2
Benzo(b)fluoranthene ug/L 83.3 77 24-15983 883.32.2U 64.2 69.5
Benzo(g,h,i)perylene ug/L 83.3 79 1-21996 2083.32.4U 65.5 79.8
Benzo(k)fluoranthene ug/L 83.3 74 11-16280 883.32.3U 61.7 66.7
bis(2-Chloroethoxy)methane ug/L 83.3 58 33-18466 1483.31.5U 48.0 55.1
bis(2-Chloroethyl) ether ug/L 83.3 54 12-15866 2083.31.6U 44.8 54.6
bis(2-Ethylhexyl)phthalate ug/L 83.3 82 8-158103 2283.33.1U 69.8 87.3
Butylbenzylphthalate ug/L 83.3 97 1-152114 1683.32.6U 81.2 95.2
Chrysene ug/L 83.3 75 17-16889 1783.32.3U 62.8 74.6
Di-n-butylphthalate ug/L 83.3 72 1-11887 1983.31.8U 59.9 72.4
Di-n-octylphthalate ug/L 83.3 79 4-14694 1783.33.3U 65.7 78.1
Dibenz(a,h)anthracene ug/L 83.3 81 1-22797 1883.32.5U 67.3 80.8
Diethylphthalate ug/L 83.3 64 1-11478 2083.31.7U 53.1 65.0
Dimethylphthalate ug/L 83.3 59 1-11274 2383.31.8U 48.9 61.6
Fluoranthene ug/L 83.3 66 26-13777 1483.31.8U 55.4 63.8
Fluorene ug/L M183.3 55 59-12169 2283.31.7U 46.0 57.4
Hexachloro-1,3-butadiene ug/L 83.3 45 24-11651 1283.31.5U 37.9 42.8
Hexachlorobenzene ug/L R183.3 58 1-15283 3583.31.8U 48.5 69.0
Hexachlorocyclopentadiene ug/L 83.3 49 25-15055 1283.31.3U 41.0 46.1
Hexachloroethane ug/L 83.3 41 40-11345 1083.31.2U 34.1 37.7
Indeno(1,2,3-cd)pyrene ug/L 83.3 80 1-17196 1883.32.4U 66.7 80.2
Isophorone ug/L 83.3 61 21-19670 1383.31.4U 51.2 58.1
N-Nitroso-di-n-propylamine ug/L 83.3 62 1-23072 1483.31.1U 52.0 59.9
N-Nitrosodimethylamine ug/L 83.3 49 25-15054 1083.31.6U 40.5 44.6
N-Nitrosodiphenylamine ug/L 83.3 60 25-15081 2983.32.5U 50.3 67.3
Naphthalene ug/L 83.3 50 21-13358 1583.31.7U 41.7 48.6
Nitrobenzene ug/L 83.3 56 35-18065 1583.31.6U 46.7 54.5
Pentachlorophenol ug/L 167 68 14-17685 211673.1U 114 141
Phenanthrene ug/L 83.3 62 54-12081 2683.31.7U 52.0 67.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
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[phone]
Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664392
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4004091MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35795500001
4004092
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol ug/L R183.3 40 5-11265 4883.31.1U 34.1 55.5
Pyrene ug/L 83.3 101 52-115113 1183.31.8U 84.5 94.3
2,4,6-Tribromophenol (S) %80 10-13797
2-Fluorobiphenyl (S) %63 15-12064
2-Fluorophenol (S) %48 10-12060
Nitrobenzene-d5 (S) %68 10-12067
Phenol-d6 (S) %41 10-12058
Terphenyl-d14 (S) %106 11-131116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
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[phone]
Page 16 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92664392
Loves 412 23004903
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 17 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92664392
Loves 412 23004903
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92664392001 771272 771404426234903-72 EPA 625.1 EPA 625.1
92664392001 773195426234903-72 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2023 07:20 PM
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[phone]
Page 18 of 21
Page 19 of 21
Page 20 of 21
Page 21 of 21
#=CL#
May 12, 2023
LIMS USE: FR - MARK RYLAND
LIMS OBJECT ID: 92666252
92666252
Project:
Pace Project No.:
RE:
Mark Ryland
Apex Companies, LLC
203 Wylderose Court
Midlothian, VA 23113
Loves 412 23004903
Dear Mark Ryland:
Enclosed are the analytical results for sample(s) received by the laboratory on May 08, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 61
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 61
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92666252
Loves 412 23004903
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92666252001 53234903 - 106 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92666252002 53234903 - 107 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92666252003 53234903 - 108 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92666252004 53234903 - 109 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92666252005 53234903 - 110 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92666252006 53234903 - 125 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92666252007 53234903 - 126 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92666252008 53234903 - 132 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 106 Lab ID: 92666252001 Collected: 05/03/23 14:30 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/11/23 08:54 83-32-905/10/23 15:09380 1
Acenaphthylene ND ug/kg 05/11/23 08:54 208-96-805/10/23 15:09380 1
Aniline ND ug/kg 05/11/23 08:54 62-53-305/10/23 15:09380 1
Anthracene ND ug/kg 05/11/23 08:54 120-12-705/10/23 15:09380 1
Benzo(a)anthracene ND ug/kg 05/11/23 08:54 56-55-305/10/23 15:09380 1
Benzo(a)pyrene ND ug/kg 05/11/23 08:54 50-32-805/10/23 15:09380 1
Benzo(b)fluoranthene ND ug/kg 05/11/23 08:54 205-99-205/10/23 15:09380 1
Benzo(g,h,i)perylene ND ug/kg 05/11/23 08:54 191-24-205/10/23 15:09380 1
Benzo(k)fluoranthene ND ug/kg 05/11/23 08:54 207-08-905/10/23 15:09380 1
Benzoic Acid ND ug/kg 05/11/23 08:54 65-85-005/10/23 15:091900 1
Benzyl alcohol ND ug/kg 05/11/23 08:54 100-51-605/10/23 15:09760 1
4-Bromophenylphenyl ether ND ug/kg 05/11/23 08:54 101-55-305/10/23 15:09380 1
Butylbenzylphthalate ND ug/kg 05/11/23 08:54 85-68-705/10/23 15:09380 1
4-Chloro-3-methylphenol ND ug/kg 05/11/23 08:54 59-50-705/10/23 15:09760 1
4-Chloroaniline ND ug/kg 05/11/23 08:54 106-47-805/10/23 15:09760 1
bis(2-Chloroethoxy)methane ND ug/kg 05/11/23 08:54 111-91-105/10/23 15:09380 1
bis(2-Chloroethyl) ether ND ug/kg 05/11/23 08:54 111-44-405/10/23 15:09380 1
2-Chloronaphthalene ND ug/kg 05/11/23 08:54 91-58-705/10/23 15:09380 1
2-Chlorophenol ND ug/kg 05/11/23 08:54 95-57-805/10/23 15:09380 1
4-Chlorophenylphenyl ether ND ug/kg 05/11/23 08:54 7005-72-305/10/23 15:09380 1
Chrysene ND ug/kg 05/11/23 08:54 218-01-905/10/23 15:09380 1
Dibenz(a,h)anthracene ND ug/kg 05/11/23 08:54 53-70-305/10/23 15:09380 1
Dibenzofuran ND ug/kg 05/11/23 08:54 132-64-905/10/23 15:09380 1
1,2-Dichlorobenzene ND ug/kg 05/11/23 08:54 95-50-105/10/23 15:09380 1
1,3-Dichlorobenzene ND ug/kg 05/11/23 08:54 541-73-105/10/23 15:09380 1
1,4-Dichlorobenzene ND ug/kg 05/11/23 08:54 106-46-705/10/23 15:09380 1
3,3'-Dichlorobenzidine ND ug/kg 05/11/23 08:54 91-94-105/10/23 15:09760 1
2,4-Dichlorophenol ND ug/kg 05/11/23 08:54 120-83-205/10/23 15:09380 1
Diethylphthalate ND ug/kg 05/11/23 08:54 84-66-205/10/23 15:09380 1
2,4-Dimethylphenol ND ug/kg 05/11/23 08:54 105-67-905/10/23 15:09380 1
Dimethylphthalate ND ug/kg 05/11/23 08:54 131-11-305/10/23 15:09380 1
Di-n-butylphthalate ND ug/kg 05/11/23 08:54 84-74-205/10/23 15:09380 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/11/23 08:54 534-52-105/10/23 15:09760 1
2,4-Dinitrophenol ND ug/kg 05/11/23 08:54 51-28-5 v105/10/23 15:091900 1
2,4-Dinitrotoluene ND ug/kg 05/11/23 08:54 121-14-205/10/23 15:09380 1
2,6-Dinitrotoluene ND ug/kg 05/11/23 08:54 606-20-205/10/23 15:09380 1
Di-n-octylphthalate ND ug/kg 05/11/23 08:54 117-84-005/10/23 15:09380 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/11/23 08:54 117-81-705/10/23 15:09380 1
Fluoranthene ND ug/kg 05/11/23 08:54 206-44-005/10/23 15:09380 1
Fluorene ND ug/kg 05/11/23 08:54 86-73-705/10/23 15:09380 1
Hexachloro-1,3-butadiene ND ug/kg 05/11/23 08:54 87-68-305/10/23 15:09380 1
Hexachlorobenzene ND ug/kg 05/11/23 08:54 118-74-105/10/23 15:09380 1
Hexachlorocyclopentadiene ND ug/kg 05/11/23 08:54 77-47-405/10/23 15:09380 1
Hexachloroethane ND ug/kg 05/11/23 08:54 67-72-105/10/23 15:09380 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/11/23 08:54 193-39-505/10/23 15:09380 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
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[phone]
Page 4 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 106 Lab ID: 92666252001 Collected: 05/03/23 14:30 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/11/23 08:54 78-59-105/10/23 15:09380 1
1-Methylnaphthalene ND ug/kg 05/11/23 08:54 90-12-005/10/23 15:09380 1
2-Methylnaphthalene ND ug/kg 05/11/23 08:54 91-57-605/10/23 15:09380 1
2-Methylphenol(o-Cresol) ND ug/kg 05/11/23 08:54 95-48-705/10/23 15:09380 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/11/23 08:54 15831-10-405/10/23 15:09380 1
Naphthalene ND ug/kg 05/11/23 08:54 91-20-305/10/23 15:09380 1
2-Nitroaniline ND ug/kg 05/11/23 08:54 88-74-405/10/23 15:091900 1
3-Nitroaniline ND ug/kg 05/11/23 08:54 99-09-205/10/23 15:091900 1
4-Nitroaniline ND ug/kg 05/11/23 08:54 100-01-605/10/23 15:09760 1
Nitrobenzene ND ug/kg 05/11/23 08:54 98-95-305/10/23 15:09380 1
2-Nitrophenol ND ug/kg 05/11/23 08:54 88-75-505/10/23 15:09380 1
4-Nitrophenol ND ug/kg 05/11/23 08:54 100-02-705/10/23 15:091900 1
N-Nitrosodimethylamine ND ug/kg 05/11/23 08:54 62-75-905/10/23 15:09380 1
N-Nitroso-di-n-propylamine ND ug/kg 05/11/23 08:54 621-64-705/10/23 15:09380 1
N-Nitrosodiphenylamine ND ug/kg 05/11/23 08:54 86-30-605/10/23 15:09380 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/11/23 08:54 108-60-105/10/23 15:09380 1
Pentachlorophenol ND ug/kg 05/11/23 08:54 87-86-505/10/23 15:09760 1
Phenanthrene ND ug/kg 05/11/23 08:54 85-01-805/10/23 15:09380 1
Phenol ND ug/kg 05/11/23 08:54 108-95-205/10/23 15:09380 1
Pyrene ND ug/kg 05/11/23 08:54 129-00-005/10/23 15:09380 1
Pyridine ND ug/kg 05/11/23 08:54 110-86-105/10/23 15:09380 1
1,2,4-Trichlorobenzene ND ug/kg 05/11/23 08:54 120-82-105/10/23 15:09380 1
2,4,5-Trichlorophenol ND ug/kg 05/11/23 08:54 95-95-405/10/23 15:09380 1
2,4,6-Trichlorophenol ND ug/kg 05/11/23 08:54 88-06-205/10/23 15:09380 1
Surrogates
Nitrobenzene-d5 (S) 45 %05/11/23 08:54 4165-60-005/10/23 15:0910-130 1
2-Fluorobiphenyl (S) 39 %05/11/23 08:54 321-60-805/10/23 15:0910-130 1
Terphenyl-d14 (S) 51 %05/11/23 08:54 1718-51-005/10/23 15:0910-130 1
Phenol-d6 (S) 45 %05/11/23 08:54 13127-88-305/10/23 15:0910-130 1
2-Fluorophenol (S) 43 %05/11/23 08:54 367-12-405/10/23 15:0910-130 1
2,4,6-Tribromophenol (S) 55 %05/11/23 08:54 118-79-605/10/23 15:0910-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/09/23 14:03 67-64-105/09/23 09:05587 5
Benzene ND ug/kg 05/09/23 14:03 71-43-205/09/23 09:0529.3 5
Bromobenzene ND ug/kg 05/09/23 14:03 108-86-105/09/23 09:0529.3 5
Bromochloromethane ND ug/kg 05/09/23 14:03 74-97-505/09/23 09:0529.3 5
Bromodichloromethane ND ug/kg 05/09/23 14:03 75-27-405/09/23 09:0529.3 5
Bromoform ND ug/kg 05/09/23 14:03 75-25-205/09/23 09:0529.3 5
Bromomethane ND ug/kg 05/09/23 14:03 74-83-9 IK,v105/09/23 09:05117 5
2-Butanone (MEK) ND ug/kg 05/09/23 14:03 78-93-305/09/23 09:05587 5
n-Butylbenzene ND ug/kg 05/09/23 14:03 104-51-805/09/23 09:0529.3 5
sec-Butylbenzene 29.5 ug/kg 05/09/23 14:03 135-98-805/09/23 09:0529.3 5
tert-Butylbenzene ND ug/kg 05/09/23 14:03 98-06-605/09/23 09:0529.3 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
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Page 5 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 106 Lab ID: 92666252001 Collected: 05/03/23 14:30 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/09/23 14:03 56-23-505/09/23 09:0529.3 5
Chlorobenzene ND ug/kg 05/09/23 14:03 108-90-705/09/23 09:0529.3 5
Chloroethane ND ug/kg 05/09/23 14:03 75-00-305/09/23 09:0558.7 5
Chloroform ND ug/kg 05/09/23 14:03 67-66-305/09/23 09:0529.3 5
Chloromethane 19500 ug/kg 05/09/23 14:03 74-87-305/09/23 09:0558.7 5
2-Chlorotoluene ND ug/kg 05/09/23 14:03 95-49-805/09/23 09:0529.3 5
4-Chlorotoluene ND ug/kg 05/09/23 14:03 106-43-405/09/23 09:0529.3 5
1,2-Dibromo-3-chloropropane ND ug/kg 05/09/23 14:03 96-12-805/09/23 09:0529.3 5
Dibromochloromethane ND ug/kg 05/09/23 14:03 124-48-105/09/23 09:0529.3 5
1,2-Dibromoethane (EDB) ND ug/kg 05/09/23 14:03 106-93-405/09/23 09:0529.3 5
Dibromomethane ND ug/kg 05/09/23 14:03 74-95-305/09/23 09:0529.3 5
1,2-Dichlorobenzene ND ug/kg 05/09/23 14:03 95-50-105/09/23 09:0529.3 5
1,3-Dichlorobenzene ND ug/kg 05/09/23 14:03 541-73-105/09/23 09:0529.3 5
1,4-Dichlorobenzene ND ug/kg 05/09/23 14:03 106-46-705/09/23 09:0529.3 5
Dichlorodifluoromethane ND ug/kg 05/09/23 14:03 75-71-8 L105/09/23 09:0558.7 5
1,1-Dichloroethane ND ug/kg 05/09/23 14:03 75-34-305/09/23 09:0529.3 5
1,2-Dichloroethane ND ug/kg 05/09/23 14:03 107-06-205/09/23 09:0529.3 5
1,1-Dichloroethene ND ug/kg 05/09/23 14:03 75-35-405/09/23 09:0529.3 5
cis-1,2-Dichloroethene ND ug/kg 05/09/23 14:03 156-59-205/09/23 09:0529.3 5
trans-1,2-Dichloroethene ND ug/kg 05/09/23 14:03 156-60-505/09/23 09:0529.3 5
1,2-Dichloropropane ND ug/kg 05/09/23 14:03 78-87-505/09/23 09:0529.3 5
1,3-Dichloropropane ND ug/kg 05/09/23 14:03 142-28-905/09/23 09:0529.3 5
2,2-Dichloropropane ND ug/kg 05/09/23 14:03 594-20-705/09/23 09:0529.3 5
1,1-Dichloropropene ND ug/kg 05/09/23 14:03 563-58-605/09/23 09:0529.3 5
cis-1,3-Dichloropropene ND ug/kg 05/09/23 14:03 10061-01-505/09/23 09:0529.3 5
trans-1,3-Dichloropropene ND ug/kg 05/09/23 14:03 10061-02-605/09/23 09:0529.3 5
Diisopropyl ether ND ug/kg 05/09/23 14:03 108-20-305/09/23 09:0529.3 5
Ethylbenzene ND ug/kg 05/09/23 14:03 100-41-405/09/23 09:0529.3 5
Hexachloro-1,3-butadiene ND ug/kg 05/09/23 14:03 87-68-305/09/23 09:0558.7 5
2-Hexanone ND ug/kg 05/09/23 14:03 591-78-605/09/23 09:05293 5
Isopropylbenzene (Cumene) ND ug/kg 05/09/23 14:03 98-82-805/09/23 09:0529.3 5
p-Isopropyltoluene ND ug/kg 05/09/23 14:03 99-87-605/09/23 09:0529.3 5
Methylene Chloride ND ug/kg 05/09/23 14:03 75-09-205/09/23 09:05117 5
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/09/23 14:03 108-10-105/09/23 09:05293 5
Methyl-tert-butyl ether ND ug/kg 05/09/23 14:03 1634-04-405/09/23 09:0529.3 5
Naphthalene ND ug/kg 05/09/23 14:03 91-20-305/09/23 09:0529.3 5
n-Propylbenzene ND ug/kg 05/09/23 14:03 103-65-105/09/23 09:0529.3 5
Styrene ND ug/kg 05/09/23 14:03 100-42-505/09/23 09:0529.3 5
1,1,1,2-Tetrachloroethane ND ug/kg 05/09/23 14:03 630-20-605/09/23 09:0529.3 5
1,1,2,2-Tetrachloroethane ND ug/kg 05/09/23 14:03 79-34-505/09/23 09:0529.3 5
Tetrachloroethene ND ug/kg 05/09/23 14:03 127-18-405/09/23 09:0529.3 5
Toluene ND ug/kg 05/09/23 14:03 108-88-305/09/23 09:0529.3 5
1,2,3-Trichlorobenzene ND ug/kg 05/09/23 14:03 87-61-605/09/23 09:0529.3 5
1,2,4-Trichlorobenzene ND ug/kg 05/09/23 14:03 120-82-105/09/23 09:0529.3 5
1,1,1-Trichloroethane ND ug/kg 05/09/23 14:03 71-55-605/09/23 09:0529.3 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 106 Lab ID: 92666252001 Collected: 05/03/23 14:30 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/09/23 14:03 79-00-505/09/23 09:0529.3 5
Trichloroethene ND ug/kg 05/09/23 14:03 79-01-605/09/23 09:0529.3 5
Trichlorofluoromethane ND ug/kg 05/09/23 14:03 75-69-405/09/23 09:0529.3 5
1,2,3-Trichloropropane ND ug/kg 05/09/23 14:03 96-18-405/09/23 09:0529.3 5
1,2,4-Trimethylbenzene ND ug/kg 05/09/23 14:03 95-63-605/09/23 09:0529.3 5
1,3,5-Trimethylbenzene ND ug/kg 05/09/23 14:03 108-67-805/09/23 09:0529.3 5
Vinyl acetate ND ug/kg 05/09/23 14:03 108-05-405/09/23 09:05293 5
Vinyl chloride ND ug/kg 05/09/23 14:03 75-01-405/09/23 09:0558.7 5
Xylene (Total) ND ug/kg 05/09/23 14:03 1330-20-705/09/23 09:0558.7 5
m&p-Xylene ND ug/kg 05/09/23 14:03 179601-23-105/09/23 09:0558.7 5
o-Xylene ND ug/kg 05/09/23 14:03 95-47-605/09/23 09:0529.3 5
Surrogates
Toluene-d8 (S) 100 %05/09/23 14:03 2037-26-505/09/23 09:0570-130 5
4-Bromofluorobenzene (S) 95 %05/09/23 14:03 460-00-405/09/23 09:0570-130 5
1,2-Dichloroethane-d4 (S) 100 %05/09/23 14:03 17060-07-005/09/23 09:0570-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.3 %05/08/23 14:45 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 107 Lab ID: 92666252002 Collected: 05/03/23 14:40 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/11/23 09:19 83-32-905/10/23 15:09405 1
Acenaphthylene ND ug/kg 05/11/23 09:19 208-96-805/10/23 15:09405 1
Aniline ND ug/kg 05/11/23 09:19 62-53-305/10/23 15:09405 1
Anthracene ND ug/kg 05/11/23 09:19 120-12-705/10/23 15:09405 1
Benzo(a)anthracene ND ug/kg 05/11/23 09:19 56-55-305/10/23 15:09405 1
Benzo(a)pyrene ND ug/kg 05/11/23 09:19 50-32-805/10/23 15:09405 1
Benzo(b)fluoranthene ND ug/kg 05/11/23 09:19 205-99-205/10/23 15:09405 1
Benzo(g,h,i)perylene ND ug/kg 05/11/23 09:19 191-24-205/10/23 15:09405 1
Benzo(k)fluoranthene ND ug/kg 05/11/23 09:19 207-08-905/10/23 15:09405 1
Benzoic Acid ND ug/kg 05/11/23 09:19 65-85-005/10/23 15:092030 1
Benzyl alcohol ND ug/kg 05/11/23 09:19 100-51-605/10/23 15:09811 1
4-Bromophenylphenyl ether ND ug/kg 05/11/23 09:19 101-55-305/10/23 15:09405 1
Butylbenzylphthalate ND ug/kg 05/11/23 09:19 85-68-705/10/23 15:09405 1
4-Chloro-3-methylphenol ND ug/kg 05/11/23 09:19 59-50-705/10/23 15:09811 1
4-Chloroaniline ND ug/kg 05/11/23 09:19 106-47-805/10/23 15:09811 1
bis(2-Chloroethoxy)methane ND ug/kg 05/11/23 09:19 111-91-105/10/23 15:09405 1
bis(2-Chloroethyl) ether ND ug/kg 05/11/23 09:19 111-44-405/10/23 15:09405 1
2-Chloronaphthalene ND ug/kg 05/11/23 09:19 91-58-705/10/23 15:09405 1
2-Chlorophenol ND ug/kg 05/11/23 09:19 95-57-805/10/23 15:09405 1
4-Chlorophenylphenyl ether ND ug/kg 05/11/23 09:19 7005-72-305/10/23 15:09405 1
Chrysene ND ug/kg 05/11/23 09:19 218-01-905/10/23 15:09405 1
Dibenz(a,h)anthracene ND ug/kg 05/11/23 09:19 53-70-305/10/23 15:09405 1
Dibenzofuran ND ug/kg 05/11/23 09:19 132-64-905/10/23 15:09405 1
1,2-Dichlorobenzene ND ug/kg 05/11/23 09:19 95-50-105/10/23 15:09405 1
1,3-Dichlorobenzene ND ug/kg 05/11/23 09:19 541-73-105/10/23 15:09405 1
1,4-Dichlorobenzene ND ug/kg 05/11/23 09:19 106-46-705/10/23 15:09405 1
3,3'-Dichlorobenzidine ND ug/kg 05/11/23 09:19 91-94-105/10/23 15:09811 1
2,4-Dichlorophenol ND ug/kg 05/11/23 09:19 120-83-205/10/23 15:09405 1
Diethylphthalate ND ug/kg 05/11/23 09:19 84-66-205/10/23 15:09405 1
2,4-Dimethylphenol ND ug/kg 05/11/23 09:19 105-67-905/10/23 15:09405 1
Dimethylphthalate ND ug/kg 05/11/23 09:19 131-11-305/10/23 15:09405 1
Di-n-butylphthalate ND ug/kg 05/11/23 09:19 84-74-205/10/23 15:09405 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/11/23 09:19 534-52-105/10/23 15:09811 1
2,4-Dinitrophenol ND ug/kg 05/11/23 09:19 51-28-5 v105/10/23 15:092030 1
2,4-Dinitrotoluene ND ug/kg 05/11/23 09:19 121-14-205/10/23 15:09405 1
2,6-Dinitrotoluene ND ug/kg 05/11/23 09:19 606-20-205/10/23 15:09405 1
Di-n-octylphthalate ND ug/kg 05/11/23 09:19 117-84-005/10/23 15:09405 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/11/23 09:19 117-81-705/10/23 15:09405 1
Fluoranthene ND ug/kg 05/11/23 09:19 206-44-005/10/23 15:09405 1
Fluorene ND ug/kg 05/11/23 09:19 86-73-705/10/23 15:09405 1
Hexachloro-1,3-butadiene ND ug/kg 05/11/23 09:19 87-68-305/10/23 15:09405 1
Hexachlorobenzene ND ug/kg 05/11/23 09:19 118-74-105/10/23 15:09405 1
Hexachlorocyclopentadiene ND ug/kg 05/11/23 09:19 77-47-405/10/23 15:09405 1
Hexachloroethane ND ug/kg 05/11/23 09:19 67-72-105/10/23 15:09405 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/11/23 09:19 193-39-505/10/23 15:09405 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 107 Lab ID: 92666252002 Collected: 05/03/23 14:40 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/11/23 09:19 78-59-105/10/23 15:09405 1
1-Methylnaphthalene ND ug/kg 05/11/23 09:19 90-12-005/10/23 15:09405 1
2-Methylnaphthalene ND ug/kg 05/11/23 09:19 91-57-605/10/23 15:09405 1
2-Methylphenol(o-Cresol) ND ug/kg 05/11/23 09:19 95-48-705/10/23 15:09405 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/11/23 09:19 15831-10-405/10/23 15:09405 1
Naphthalene ND ug/kg 05/11/23 09:19 91-20-305/10/23 15:09405 1
2-Nitroaniline ND ug/kg 05/11/23 09:19 88-74-405/10/23 15:092030 1
3-Nitroaniline ND ug/kg 05/11/23 09:19 99-09-205/10/23 15:092030 1
4-Nitroaniline ND ug/kg 05/11/23 09:19 100-01-605/10/23 15:09811 1
Nitrobenzene ND ug/kg 05/11/23 09:19 98-95-305/10/23 15:09405 1
2-Nitrophenol ND ug/kg 05/11/23 09:19 88-75-505/10/23 15:09405 1
4-Nitrophenol ND ug/kg 05/11/23 09:19 100-02-705/10/23 15:092030 1
N-Nitrosodimethylamine ND ug/kg 05/11/23 09:19 62-75-905/10/23 15:09405 1
N-Nitroso-di-n-propylamine ND ug/kg 05/11/23 09:19 621-64-705/10/23 15:09405 1
N-Nitrosodiphenylamine ND ug/kg 05/11/23 09:19 86-30-605/10/23 15:09405 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/11/23 09:19 108-60-105/10/23 15:09405 1
Pentachlorophenol ND ug/kg 05/11/23 09:19 87-86-505/10/23 15:09811 1
Phenanthrene ND ug/kg 05/11/23 09:19 85-01-805/10/23 15:09405 1
Phenol ND ug/kg 05/11/23 09:19 108-95-205/10/23 15:09405 1
Pyrene ND ug/kg 05/11/23 09:19 129-00-005/10/23 15:09405 1
Pyridine ND ug/kg 05/11/23 09:19 110-86-105/10/23 15:09405 1
1,2,4-Trichlorobenzene ND ug/kg 05/11/23 09:19 120-82-105/10/23 15:09405 1
2,4,5-Trichlorophenol ND ug/kg 05/11/23 09:19 95-95-405/10/23 15:09405 1
2,4,6-Trichlorophenol ND ug/kg 05/11/23 09:19 88-06-205/10/23 15:09405 1
Surrogates
Nitrobenzene-d5 (S) 64 %05/11/23 09:19 4165-60-005/10/23 15:0910-130 1
2-Fluorobiphenyl (S) 60 %05/11/23 09:19 321-60-805/10/23 15:0910-130 1
Terphenyl-d14 (S) 67 %05/11/23 09:19 1718-51-005/10/23 15:0910-130 1
Phenol-d6 (S) 63 %05/11/23 09:19 13127-88-305/10/23 15:0910-130 1
2-Fluorophenol (S) 60 %05/11/23 09:19 367-12-405/10/23 15:0910-130 1
2,4,6-Tribromophenol (S) 71 %05/11/23 09:19 118-79-605/10/23 15:0910-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/09/23 14:21 67-64-105/09/23 09:05609 5
Benzene ND ug/kg 05/09/23 14:21 71-43-205/09/23 09:0530.5 5
Bromobenzene ND ug/kg 05/09/23 14:21 108-86-105/09/23 09:0530.5 5
Bromochloromethane ND ug/kg 05/09/23 14:21 74-97-505/09/23 09:0530.5 5
Bromodichloromethane ND ug/kg 05/09/23 14:21 75-27-405/09/23 09:0530.5 5
Bromoform ND ug/kg 05/09/23 14:21 75-25-205/09/23 09:0530.5 5
Bromomethane ND ug/kg 05/09/23 14:21 74-83-9 IK,v105/09/23 09:05122 5
2-Butanone (MEK) ND ug/kg 05/09/23 14:21 78-93-305/09/23 09:05609 5
n-Butylbenzene ND ug/kg 05/09/23 14:21 104-51-805/09/23 09:0530.5 5
sec-Butylbenzene ND ug/kg 05/09/23 14:21 135-98-805/09/23 09:0530.5 5
tert-Butylbenzene ND ug/kg 05/09/23 14:21 98-06-605/09/23 09:0530.5 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 107 Lab ID: 92666252002 Collected: 05/03/23 14:40 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/09/23 14:21 56-23-505/09/23 09:0530.5 5
Chlorobenzene ND ug/kg 05/09/23 14:21 108-90-705/09/23 09:0530.5 5
Chloroethane ND ug/kg 05/09/23 14:21 75-00-305/09/23 09:0560.9 5
Chloroform ND ug/kg 05/09/23 14:21 67-66-305/09/23 09:0530.5 5
Chloromethane 20700 ug/kg 05/09/23 14:21 74-87-305/09/23 09:0560.9 5
2-Chlorotoluene ND ug/kg 05/09/23 14:21 95-49-805/09/23 09:0530.5 5
4-Chlorotoluene ND ug/kg 05/09/23 14:21 106-43-405/09/23 09:0530.5 5
1,2-Dibromo-3-chloropropane ND ug/kg 05/09/23 14:21 96-12-805/09/23 09:0530.5 5
Dibromochloromethane ND ug/kg 05/09/23 14:21 124-48-105/09/23 09:0530.5 5
1,2-Dibromoethane (EDB) ND ug/kg 05/09/23 14:21 106-93-405/09/23 09:0530.5 5
Dibromomethane ND ug/kg 05/09/23 14:21 74-95-305/09/23 09:0530.5 5
1,2-Dichlorobenzene ND ug/kg 05/09/23 14:21 95-50-105/09/23 09:0530.5 5
1,3-Dichlorobenzene ND ug/kg 05/09/23 14:21 541-73-105/09/23 09:0530.5 5
1,4-Dichlorobenzene ND ug/kg 05/09/23 14:21 106-46-705/09/23 09:0530.5 5
Dichlorodifluoromethane ND ug/kg 05/09/23 14:21 75-71-8 L105/09/23 09:0560.9 5
1,1-Dichloroethane ND ug/kg 05/09/23 14:21 75-34-305/09/23 09:0530.5 5
1,2-Dichloroethane ND ug/kg 05/09/23 14:21 107-06-205/09/23 09:0530.5 5
1,1-Dichloroethene ND ug/kg 05/09/23 14:21 75-35-405/09/23 09:0530.5 5
cis-1,2-Dichloroethene ND ug/kg 05/09/23 14:21 156-59-205/09/23 09:0530.5 5
trans-1,2-Dichloroethene ND ug/kg 05/09/23 14:21 156-60-505/09/23 09:0530.5 5
1,2-Dichloropropane ND ug/kg 05/09/23 14:21 78-87-505/09/23 09:0530.5 5
1,3-Dichloropropane ND ug/kg 05/09/23 14:21 142-28-905/09/23 09:0530.5 5
2,2-Dichloropropane ND ug/kg 05/09/23 14:21 594-20-705/09/23 09:0530.5 5
1,1-Dichloropropene ND ug/kg 05/09/23 14:21 563-58-605/09/23 09:0530.5 5
cis-1,3-Dichloropropene ND ug/kg 05/09/23 14:21 10061-01-505/09/23 09:0530.5 5
trans-1,3-Dichloropropene ND ug/kg 05/09/23 14:21 10061-02-605/09/23 09:0530.5 5
Diisopropyl ether ND ug/kg 05/09/23 14:21 108-20-305/09/23 09:0530.5 5
Ethylbenzene ND ug/kg 05/09/23 14:21 100-41-405/09/23 09:0530.5 5
Hexachloro-1,3-butadiene ND ug/kg 05/09/23 14:21 87-68-305/09/23 09:0560.9 5
2-Hexanone ND ug/kg 05/09/23 14:21 591-78-605/09/23 09:05305 5
Isopropylbenzene (Cumene) ND ug/kg 05/09/23 14:21 98-82-805/09/23 09:0530.5 5
p-Isopropyltoluene ND ug/kg 05/09/23 14:21 99-87-605/09/23 09:0530.5 5
Methylene Chloride ND ug/kg 05/09/23 14:21 75-09-205/09/23 09:05122 5
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/09/23 14:21 108-10-105/09/23 09:05305 5
Methyl-tert-butyl ether ND ug/kg 05/09/23 14:21 1634-04-405/09/23 09:0530.5 5
Naphthalene ND ug/kg 05/09/23 14:21 91-20-305/09/23 09:0530.5 5
n-Propylbenzene ND ug/kg 05/09/23 14:21 103-65-105/09/23 09:0530.5 5
Styrene ND ug/kg 05/09/23 14:21 100-42-505/09/23 09:0530.5 5
1,1,1,2-Tetrachloroethane ND ug/kg 05/09/23 14:21 630-20-605/09/23 09:0530.5 5
1,1,2,2-Tetrachloroethane ND ug/kg 05/09/23 14:21 79-34-505/09/23 09:0530.5 5
Tetrachloroethene ND ug/kg 05/09/23 14:21 127-18-405/09/23 09:0530.5 5
Toluene ND ug/kg 05/09/23 14:21 108-88-305/09/23 09:0530.5 5
1,2,3-Trichlorobenzene ND ug/kg 05/09/23 14:21 87-61-605/09/23 09:0530.5 5
1,2,4-Trichlorobenzene ND ug/kg 05/09/23 14:21 120-82-105/09/23 09:0530.5 5
1,1,1-Trichloroethane ND ug/kg 05/09/23 14:21 71-55-605/09/23 09:0530.5 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 107 Lab ID: 92666252002 Collected: 05/03/23 14:40 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/09/23 14:21 79-00-505/09/23 09:0530.5 5
Trichloroethene ND ug/kg 05/09/23 14:21 79-01-605/09/23 09:0530.5 5
Trichlorofluoromethane ND ug/kg 05/09/23 14:21 75-69-405/09/23 09:0530.5 5
1,2,3-Trichloropropane ND ug/kg 05/09/23 14:21 96-18-405/09/23 09:0530.5 5
1,2,4-Trimethylbenzene ND ug/kg 05/09/23 14:21 95-63-605/09/23 09:0530.5 5
1,3,5-Trimethylbenzene ND ug/kg 05/09/23 14:21 108-67-805/09/23 09:0530.5 5
Vinyl acetate ND ug/kg 05/09/23 14:21 108-05-405/09/23 09:05305 5
Vinyl chloride ND ug/kg 05/09/23 14:21 75-01-405/09/23 09:0560.9 5
Xylene (Total) ND ug/kg 05/09/23 14:21 1330-20-705/09/23 09:0560.9 5
m&p-Xylene ND ug/kg 05/09/23 14:21 179601-23-105/09/23 09:0560.9 5
o-Xylene ND ug/kg 05/09/23 14:21 95-47-605/09/23 09:0530.5 5
Surrogates
Toluene-d8 (S) 101 %05/09/23 14:21 2037-26-505/09/23 09:0570-130 5
4-Bromofluorobenzene (S) 94 %05/09/23 14:21 460-00-405/09/23 09:0570-130 5
1,2-Dichloroethane-d4 (S) 101 %05/09/23 14:21 17060-07-005/09/23 09:0570-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.9 %05/08/23 14:46 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 108 Lab ID: 92666252003 Collected: 05/03/23 14:50 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/11/23 09:45 83-32-905/10/23 15:09391 1
Acenaphthylene ND ug/kg 05/11/23 09:45 208-96-805/10/23 15:09391 1
Aniline ND ug/kg 05/11/23 09:45 62-53-305/10/23 15:09391 1
Anthracene ND ug/kg 05/11/23 09:45 120-12-705/10/23 15:09391 1
Benzo(a)anthracene ND ug/kg 05/11/23 09:45 56-55-305/10/23 15:09391 1
Benzo(a)pyrene ND ug/kg 05/11/23 09:45 50-32-805/10/23 15:09391 1
Benzo(b)fluoranthene ND ug/kg 05/11/23 09:45 205-99-205/10/23 15:09391 1
Benzo(g,h,i)perylene ND ug/kg 05/11/23 09:45 191-24-205/10/23 15:09391 1
Benzo(k)fluoranthene ND ug/kg 05/11/23 09:45 207-08-905/10/23 15:09391 1
Benzoic Acid ND ug/kg 05/11/23 09:45 65-85-005/10/23 15:091960 1
Benzyl alcohol ND ug/kg 05/11/23 09:45 100-51-605/10/23 15:09783 1
4-Bromophenylphenyl ether ND ug/kg 05/11/23 09:45 101-55-305/10/23 15:09391 1
Butylbenzylphthalate ND ug/kg 05/11/23 09:45 85-68-705/10/23 15:09391 1
4-Chloro-3-methylphenol ND ug/kg 05/11/23 09:45 59-50-705/10/23 15:09783 1
4-Chloroaniline ND ug/kg 05/11/23 09:45 106-47-805/10/23 15:09783 1
bis(2-Chloroethoxy)methane ND ug/kg 05/11/23 09:45 111-91-105/10/23 15:09391 1
bis(2-Chloroethyl) ether ND ug/kg 05/11/23 09:45 111-44-405/10/23 15:09391 1
2-Chloronaphthalene ND ug/kg 05/11/23 09:45 91-58-705/10/23 15:09391 1
2-Chlorophenol ND ug/kg 05/11/23 09:45 95-57-805/10/23 15:09391 1
4-Chlorophenylphenyl ether ND ug/kg 05/11/23 09:45 7005-72-305/10/23 15:09391 1
Chrysene ND ug/kg 05/11/23 09:45 218-01-905/10/23 15:09391 1
Dibenz(a,h)anthracene ND ug/kg 05/11/23 09:45 53-70-305/10/23 15:09391 1
Dibenzofuran ND ug/kg 05/11/23 09:45 132-64-905/10/23 15:09391 1
1,2-Dichlorobenzene ND ug/kg 05/11/23 09:45 95-50-105/10/23 15:09391 1
1,3-Dichlorobenzene ND ug/kg 05/11/23 09:45 541-73-105/10/23 15:09391 1
1,4-Dichlorobenzene ND ug/kg 05/11/23 09:45 106-46-705/10/23 15:09391 1
3,3'-Dichlorobenzidine ND ug/kg 05/11/23 09:45 91-94-105/10/23 15:09783 1
2,4-Dichlorophenol ND ug/kg 05/11/23 09:45 120-83-205/10/23 15:09391 1
Diethylphthalate ND ug/kg 05/11/23 09:45 84-66-205/10/23 15:09391 1
2,4-Dimethylphenol ND ug/kg 05/11/23 09:45 105-67-905/10/23 15:09391 1
Dimethylphthalate ND ug/kg 05/11/23 09:45 131-11-305/10/23 15:09391 1
Di-n-butylphthalate ND ug/kg 05/11/23 09:45 84-74-205/10/23 15:09391 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/11/23 09:45 534-52-105/10/23 15:09783 1
2,4-Dinitrophenol ND ug/kg 05/11/23 09:45 51-28-5 v105/10/23 15:091960 1
2,4-Dinitrotoluene ND ug/kg 05/11/23 09:45 121-14-205/10/23 15:09391 1
2,6-Dinitrotoluene ND ug/kg 05/11/23 09:45 606-20-205/10/23 15:09391 1
Di-n-octylphthalate ND ug/kg 05/11/23 09:45 117-84-005/10/23 15:09391 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/11/23 09:45 117-81-705/10/23 15:09391 1
Fluoranthene ND ug/kg 05/11/23 09:45 206-44-005/10/23 15:09391 1
Fluorene ND ug/kg 05/11/23 09:45 86-73-705/10/23 15:09391 1
Hexachloro-1,3-butadiene ND ug/kg 05/11/23 09:45 87-68-305/10/23 15:09391 1
Hexachlorobenzene ND ug/kg 05/11/23 09:45 118-74-105/10/23 15:09391 1
Hexachlorocyclopentadiene ND ug/kg 05/11/23 09:45 77-47-405/10/23 15:09391 1
Hexachloroethane ND ug/kg 05/11/23 09:45 67-72-105/10/23 15:09391 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/11/23 09:45 193-39-505/10/23 15:09391 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 108 Lab ID: 92666252003 Collected: 05/03/23 14:50 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/11/23 09:45 78-59-105/10/23 15:09391 1
1-Methylnaphthalene ND ug/kg 05/11/23 09:45 90-12-005/10/23 15:09391 1
2-Methylnaphthalene ND ug/kg 05/11/23 09:45 91-57-605/10/23 15:09391 1
2-Methylphenol(o-Cresol) ND ug/kg 05/11/23 09:45 95-48-705/10/23 15:09391 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/11/23 09:45 15831-10-405/10/23 15:09391 1
Naphthalene ND ug/kg 05/11/23 09:45 91-20-305/10/23 15:09391 1
2-Nitroaniline ND ug/kg 05/11/23 09:45 88-74-405/10/23 15:091960 1
3-Nitroaniline ND ug/kg 05/11/23 09:45 99-09-205/10/23 15:091960 1
4-Nitroaniline ND ug/kg 05/11/23 09:45 100-01-605/10/23 15:09783 1
Nitrobenzene ND ug/kg 05/11/23 09:45 98-95-305/10/23 15:09391 1
2-Nitrophenol ND ug/kg 05/11/23 09:45 88-75-505/10/23 15:09391 1
4-Nitrophenol ND ug/kg 05/11/23 09:45 100-02-705/10/23 15:091960 1
N-Nitrosodimethylamine ND ug/kg 05/11/23 09:45 62-75-905/10/23 15:09391 1
N-Nitroso-di-n-propylamine ND ug/kg 05/11/23 09:45 621-64-705/10/23 15:09391 1
N-Nitrosodiphenylamine ND ug/kg 05/11/23 09:45 86-30-605/10/23 15:09391 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/11/23 09:45 108-60-105/10/23 15:09391 1
Pentachlorophenol ND ug/kg 05/11/23 09:45 87-86-505/10/23 15:09783 1
Phenanthrene ND ug/kg 05/11/23 09:45 85-01-805/10/23 15:09391 1
Phenol ND ug/kg 05/11/23 09:45 108-95-205/10/23 15:09391 1
Pyrene ND ug/kg 05/11/23 09:45 129-00-005/10/23 15:09391 1
Pyridine ND ug/kg 05/11/23 09:45 110-86-105/10/23 15:09391 1
1,2,4-Trichlorobenzene ND ug/kg 05/11/23 09:45 120-82-105/10/23 15:09391 1
2,4,5-Trichlorophenol ND ug/kg 05/11/23 09:45 95-95-405/10/23 15:09391 1
2,4,6-Trichlorophenol ND ug/kg 05/11/23 09:45 88-06-205/10/23 15:09391 1
Surrogates
Nitrobenzene-d5 (S) 45 %05/11/23 09:45 4165-60-005/10/23 15:0910-130 1
2-Fluorobiphenyl (S) 40 %05/11/23 09:45 321-60-805/10/23 15:0910-130 1
Terphenyl-d14 (S) 56 %05/11/23 09:45 1718-51-005/10/23 15:0910-130 1
Phenol-d6 (S) 44 %05/11/23 09:45 13127-88-305/10/23 15:0910-130 1
2-Fluorophenol (S) 42 %05/11/23 09:45 367-12-405/10/23 15:0910-130 1
2,4,6-Tribromophenol (S) 56 %05/11/23 09:45 118-79-605/10/23 15:0910-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/09/23 14:58 67-64-105/09/23 09:05320 2.5
Benzene ND ug/kg 05/09/23 14:58 71-43-205/09/23 09:0516.0 2.5
Bromobenzene ND ug/kg 05/09/23 14:58 108-86-105/09/23 09:0516.0 2.5
Bromochloromethane ND ug/kg 05/09/23 14:58 74-97-505/09/23 09:0516.0 2.5
Bromodichloromethane ND ug/kg 05/09/23 14:58 75-27-405/09/23 09:0516.0 2.5
Bromoform ND ug/kg 05/09/23 14:58 75-25-205/09/23 09:0516.0 2.5
Bromomethane ND ug/kg 05/09/23 14:58 74-83-9 IK,v105/09/23 09:0563.9 2.5
2-Butanone (MEK) ND ug/kg 05/09/23 14:58 78-93-305/09/23 09:05320 2.5
n-Butylbenzene ND ug/kg 05/09/23 14:58 104-51-805/09/23 09:0516.0 2.5
sec-Butylbenzene ND ug/kg 05/09/23 14:58 135-98-805/09/23 09:0516.0 2.5
tert-Butylbenzene ND ug/kg 05/09/23 14:58 98-06-605/09/23 09:0516.0 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 108 Lab ID: 92666252003 Collected: 05/03/23 14:50 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/09/23 14:58 56-23-505/09/23 09:0516.0 2.5
Chlorobenzene ND ug/kg 05/09/23 14:58 108-90-705/09/23 09:0516.0 2.5
Chloroethane ND ug/kg 05/09/23 14:58 75-00-305/09/23 09:0532.0 2.5
Chloroform ND ug/kg 05/09/23 14:58 67-66-305/09/23 09:0516.0 2.5
Chloromethane 8870 ug/kg 05/09/23 14:58 74-87-305/09/23 09:0532.0 2.5
2-Chlorotoluene ND ug/kg 05/09/23 14:58 95-49-805/09/23 09:0516.0 2.5
4-Chlorotoluene ND ug/kg 05/09/23 14:58 106-43-405/09/23 09:0516.0 2.5
1,2-Dibromo-3-chloropropane ND ug/kg 05/09/23 14:58 96-12-805/09/23 09:0516.0 2.5
Dibromochloromethane ND ug/kg 05/09/23 14:58 124-48-105/09/23 09:0516.0 2.5
1,2-Dibromoethane (EDB) ND ug/kg 05/09/23 14:58 106-93-405/09/23 09:0516.0 2.5
Dibromomethane ND ug/kg 05/09/23 14:58 74-95-305/09/23 09:0516.0 2.5
1,2-Dichlorobenzene ND ug/kg 05/09/23 14:58 95-50-105/09/23 09:0516.0 2.5
1,3-Dichlorobenzene ND ug/kg 05/09/23 14:58 541-73-105/09/23 09:0516.0 2.5
1,4-Dichlorobenzene ND ug/kg 05/09/23 14:58 106-46-705/09/23 09:0516.0 2.5
Dichlorodifluoromethane ND ug/kg 05/09/23 14:58 75-71-8 L105/09/23 09:0532.0 2.5
1,1-Dichloroethane ND ug/kg 05/09/23 14:58 75-34-305/09/23 09:0516.0 2.5
1,2-Dichloroethane ND ug/kg 05/09/23 14:58 107-06-205/09/23 09:0516.0 2.5
1,1-Dichloroethene ND ug/kg 05/09/23 14:58 75-35-405/09/23 09:0516.0 2.5
cis-1,2-Dichloroethene ND ug/kg 05/09/23 14:58 156-59-205/09/23 09:0516.0 2.5
trans-1,2-Dichloroethene ND ug/kg 05/09/23 14:58 156-60-505/09/23 09:0516.0 2.5
1,2-Dichloropropane ND ug/kg 05/09/23 14:58 78-87-505/09/23 09:0516.0 2.5
1,3-Dichloropropane ND ug/kg 05/09/23 14:58 142-28-905/09/23 09:0516.0 2.5
2,2-Dichloropropane ND ug/kg 05/09/23 14:58 594-20-705/09/23 09:0516.0 2.5
1,1-Dichloropropene ND ug/kg 05/09/23 14:58 563-58-605/09/23 09:0516.0 2.5
cis-1,3-Dichloropropene ND ug/kg 05/09/23 14:58 10061-01-505/09/23 09:0516.0 2.5
trans-1,3-Dichloropropene ND ug/kg 05/09/23 14:58 10061-02-605/09/23 09:0516.0 2.5
Diisopropyl ether ND ug/kg 05/09/23 14:58 108-20-305/09/23 09:0516.0 2.5
Ethylbenzene ND ug/kg 05/09/23 14:58 100-41-405/09/23 09:0516.0 2.5
Hexachloro-1,3-butadiene ND ug/kg 05/09/23 14:58 87-68-305/09/23 09:0532.0 2.5
2-Hexanone ND ug/kg 05/09/23 14:58 591-78-605/09/23 09:05160 2.5
Isopropylbenzene (Cumene) ND ug/kg 05/09/23 14:58 98-82-805/09/23 09:0516.0 2.5
p-Isopropyltoluene ND ug/kg 05/09/23 14:58 99-87-605/09/23 09:0516.0 2.5
Methylene Chloride ND ug/kg 05/09/23 14:58 75-09-205/09/23 09:0563.9 2.5
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/09/23 14:58 108-10-105/09/23 09:05160 2.5
Methyl-tert-butyl ether ND ug/kg 05/09/23 14:58 1634-04-405/09/23 09:0516.0 2.5
Naphthalene ND ug/kg 05/09/23 14:58 91-20-305/09/23 09:0516.0 2.5
n-Propylbenzene ND ug/kg 05/09/23 14:58 103-65-105/09/23 09:0516.0 2.5
Styrene ND ug/kg 05/09/23 14:58 100-42-505/09/23 09:0516.0 2.5
1,1,1,2-Tetrachloroethane ND ug/kg 05/09/23 14:58 630-20-605/09/23 09:0516.0 2.5
1,1,2,2-Tetrachloroethane ND ug/kg 05/09/23 14:58 79-34-505/09/23 09:0516.0 2.5
Tetrachloroethene ND ug/kg 05/09/23 14:58 127-18-405/09/23 09:0516.0 2.5
Toluene ND ug/kg 05/09/23 14:58 108-88-305/09/23 09:0516.0 2.5
1,2,3-Trichlorobenzene ND ug/kg 05/09/23 14:58 87-61-605/09/23 09:0516.0 2.5
1,2,4-Trichlorobenzene ND ug/kg 05/09/23 14:58 120-82-105/09/23 09:0516.0 2.5
1,1,1-Trichloroethane ND ug/kg 05/09/23 14:58 71-55-605/09/23 09:0516.0 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 108 Lab ID: 92666252003 Collected: 05/03/23 14:50 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/09/23 14:58 79-00-505/09/23 09:0516.0 2.5
Trichloroethene ND ug/kg 05/09/23 14:58 79-01-605/09/23 09:0516.0 2.5
Trichlorofluoromethane ND ug/kg 05/09/23 14:58 75-69-405/09/23 09:0516.0 2.5
1,2,3-Trichloropropane ND ug/kg 05/09/23 14:58 96-18-405/09/23 09:0516.0 2.5
1,2,4-Trimethylbenzene ND ug/kg 05/09/23 14:58 95-63-605/09/23 09:0516.0 2.5
1,3,5-Trimethylbenzene ND ug/kg 05/09/23 14:58 108-67-805/09/23 09:0516.0 2.5
Vinyl acetate ND ug/kg 05/09/23 14:58 108-05-405/09/23 09:05160 2.5
Vinyl chloride ND ug/kg 05/09/23 14:58 75-01-405/09/23 09:0532.0 2.5
Xylene (Total) ND ug/kg 05/09/23 14:58 1330-20-705/09/23 09:0532.0 2.5
m&p-Xylene ND ug/kg 05/09/23 14:58 179601-23-105/09/23 09:0532.0 2.5
o-Xylene ND ug/kg 05/09/23 14:58 95-47-605/09/23 09:0516.0 2.5
Surrogates
Toluene-d8 (S) 101 %05/09/23 14:58 2037-26-505/09/23 09:0570-130 2.5
4-Bromofluorobenzene (S) 95 %05/09/23 14:58 460-00-405/09/23 09:0570-130 2.5
1,2-Dichloroethane-d4 (S) 100 %05/09/23 14:58 17060-07-005/09/23 09:0570-130 2.5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.3 %05/08/23 14:46 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 109 Lab ID: 92666252004 Collected: 05/03/23 15:00 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/11/23 10:11 83-32-905/10/23 15:09390 1
Acenaphthylene ND ug/kg 05/11/23 10:11 208-96-805/10/23 15:09390 1
Aniline ND ug/kg 05/11/23 10:11 62-53-305/10/23 15:09390 1
Anthracene ND ug/kg 05/11/23 10:11 120-12-705/10/23 15:09390 1
Benzo(a)anthracene ND ug/kg 05/11/23 10:11 56-55-305/10/23 15:09390 1
Benzo(a)pyrene ND ug/kg 05/11/23 10:11 50-32-805/10/23 15:09390 1
Benzo(b)fluoranthene ND ug/kg 05/11/23 10:11 205-99-205/10/23 15:09390 1
Benzo(g,h,i)perylene ND ug/kg 05/11/23 10:11 191-24-205/10/23 15:09390 1
Benzo(k)fluoranthene ND ug/kg 05/11/23 10:11 207-08-905/10/23 15:09390 1
Benzoic Acid ND ug/kg 05/11/23 10:11 65-85-005/10/23 15:091950 1
Benzyl alcohol ND ug/kg 05/11/23 10:11 100-51-605/10/23 15:09780 1
4-Bromophenylphenyl ether ND ug/kg 05/11/23 10:11 101-55-305/10/23 15:09390 1
Butylbenzylphthalate ND ug/kg 05/11/23 10:11 85-68-705/10/23 15:09390 1
4-Chloro-3-methylphenol ND ug/kg 05/11/23 10:11 59-50-705/10/23 15:09780 1
4-Chloroaniline ND ug/kg 05/11/23 10:11 106-47-805/10/23 15:09780 1
bis(2-Chloroethoxy)methane ND ug/kg 05/11/23 10:11 111-91-105/10/23 15:09390 1
bis(2-Chloroethyl) ether ND ug/kg 05/11/23 10:11 111-44-405/10/23 15:09390 1
2-Chloronaphthalene ND ug/kg 05/11/23 10:11 91-58-705/10/23 15:09390 1
2-Chlorophenol ND ug/kg 05/11/23 10:11 95-57-805/10/23 15:09390 1
4-Chlorophenylphenyl ether ND ug/kg 05/11/23 10:11 7005-72-305/10/23 15:09390 1
Chrysene ND ug/kg 05/11/23 10:11 218-01-905/10/23 15:09390 1
Dibenz(a,h)anthracene ND ug/kg 05/11/23 10:11 53-70-305/10/23 15:09390 1
Dibenzofuran ND ug/kg 05/11/23 10:11 132-64-905/10/23 15:09390 1
1,2-Dichlorobenzene ND ug/kg 05/11/23 10:11 95-50-105/10/23 15:09390 1
1,3-Dichlorobenzene ND ug/kg 05/11/23 10:11 541-73-105/10/23 15:09390 1
1,4-Dichlorobenzene ND ug/kg 05/11/23 10:11 106-46-705/10/23 15:09390 1
3,3'-Dichlorobenzidine ND ug/kg 05/11/23 10:11 91-94-105/10/23 15:09780 1
2,4-Dichlorophenol ND ug/kg 05/11/23 10:11 120-83-205/10/23 15:09390 1
Diethylphthalate ND ug/kg 05/11/23 10:11 84-66-205/10/23 15:09390 1
2,4-Dimethylphenol ND ug/kg 05/11/23 10:11 105-67-905/10/23 15:09390 1
Dimethylphthalate ND ug/kg 05/11/23 10:11 131-11-305/10/23 15:09390 1
Di-n-butylphthalate ND ug/kg 05/11/23 10:11 84-74-205/10/23 15:09390 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/11/23 10:11 534-52-105/10/23 15:09780 1
2,4-Dinitrophenol ND ug/kg 05/11/23 10:11 51-28-5 v105/10/23 15:091950 1
2,4-Dinitrotoluene ND ug/kg 05/11/23 10:11 121-14-205/10/23 15:09390 1
2,6-Dinitrotoluene ND ug/kg 05/11/23 10:11 606-20-205/10/23 15:09390 1
Di-n-octylphthalate ND ug/kg 05/11/23 10:11 117-84-005/10/23 15:09390 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/11/23 10:11 117-81-705/10/23 15:09390 1
Fluoranthene ND ug/kg 05/11/23 10:11 206-44-005/10/23 15:09390 1
Fluorene ND ug/kg 05/11/23 10:11 86-73-705/10/23 15:09390 1
Hexachloro-1,3-butadiene ND ug/kg 05/11/23 10:11 87-68-305/10/23 15:09390 1
Hexachlorobenzene ND ug/kg 05/11/23 10:11 118-74-105/10/23 15:09390 1
Hexachlorocyclopentadiene ND ug/kg 05/11/23 10:11 77-47-405/10/23 15:09390 1
Hexachloroethane ND ug/kg 05/11/23 10:11 67-72-105/10/23 15:09390 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/11/23 10:11 193-39-505/10/23 15:09390 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 109 Lab ID: 92666252004 Collected: 05/03/23 15:00 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/11/23 10:11 78-59-105/10/23 15:09390 1
1-Methylnaphthalene ND ug/kg 05/11/23 10:11 90-12-005/10/23 15:09390 1
2-Methylnaphthalene ND ug/kg 05/11/23 10:11 91-57-605/10/23 15:09390 1
2-Methylphenol(o-Cresol) ND ug/kg 05/11/23 10:11 95-48-705/10/23 15:09390 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/11/23 10:11 15831-10-405/10/23 15:09390 1
Naphthalene ND ug/kg 05/11/23 10:11 91-20-305/10/23 15:09390 1
2-Nitroaniline ND ug/kg 05/11/23 10:11 88-74-405/10/23 15:091950 1
3-Nitroaniline ND ug/kg 05/11/23 10:11 99-09-205/10/23 15:091950 1
4-Nitroaniline ND ug/kg 05/11/23 10:11 100-01-605/10/23 15:09780 1
Nitrobenzene ND ug/kg 05/11/23 10:11 98-95-305/10/23 15:09390 1
2-Nitrophenol ND ug/kg 05/11/23 10:11 88-75-505/10/23 15:09390 1
4-Nitrophenol ND ug/kg 05/11/23 10:11 100-02-705/10/23 15:091950 1
N-Nitrosodimethylamine ND ug/kg 05/11/23 10:11 62-75-905/10/23 15:09390 1
N-Nitroso-di-n-propylamine ND ug/kg 05/11/23 10:11 621-64-705/10/23 15:09390 1
N-Nitrosodiphenylamine ND ug/kg 05/11/23 10:11 86-30-605/10/23 15:09390 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/11/23 10:11 108-60-105/10/23 15:09390 1
Pentachlorophenol ND ug/kg 05/11/23 10:11 87-86-505/10/23 15:09780 1
Phenanthrene ND ug/kg 05/11/23 10:11 85-01-805/10/23 15:09390 1
Phenol ND ug/kg 05/11/23 10:11 108-95-205/10/23 15:09390 1
Pyrene ND ug/kg 05/11/23 10:11 129-00-005/10/23 15:09390 1
Pyridine ND ug/kg 05/11/23 10:11 110-86-105/10/23 15:09390 1
1,2,4-Trichlorobenzene ND ug/kg 05/11/23 10:11 120-82-105/10/23 15:09390 1
2,4,5-Trichlorophenol ND ug/kg 05/11/23 10:11 95-95-405/10/23 15:09390 1
2,4,6-Trichlorophenol ND ug/kg 05/11/23 10:11 88-06-205/10/23 15:09390 1
Surrogates
Nitrobenzene-d5 (S) 61 %05/11/23 10:11 4165-60-005/10/23 15:0910-130 1
2-Fluorobiphenyl (S) 57 %05/11/23 10:11 321-60-805/10/23 15:0910-130 1
Terphenyl-d14 (S) 67 %05/11/23 10:11 1718-51-005/10/23 15:0910-130 1
Phenol-d6 (S) 60 %05/11/23 10:11 13127-88-305/10/23 15:0910-130 1
2-Fluorophenol (S) 58 %05/11/23 10:11 367-12-405/10/23 15:0910-130 1
2,4,6-Tribromophenol (S) 72 %05/11/23 10:11 118-79-605/10/23 15:0910-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/09/23 13:07 67-64-1 R105/09/23 09:05123 1
Benzene 7.0 ug/kg 05/09/23 13:07 71-43-2 M1,R105/09/23 09:056.2 1
Bromobenzene ND ug/kg 05/09/23 13:07 108-86-1 M1,R105/09/23 09:056.2 1
Bromochloromethane ND ug/kg 05/09/23 13:07 74-97-5 M1,R105/09/23 09:056.2 1
Bromodichloromethane ND ug/kg 05/09/23 13:07 75-27-4 M1,R105/09/23 09:056.2 1
Bromoform ND ug/kg 05/09/23 13:07 75-25-2 M1,R105/09/23 09:056.2 1
Bromomethane ND ug/kg 05/09/23 13:07 74-83-9 IK,R1,v105/09/23 09:0524.6 1
2-Butanone (MEK) ND ug/kg 05/09/23 13:07 78-93-3 R105/09/23 09:05123 1
n-Butylbenzene 87.1 ug/kg 05/09/23 13:07 104-51-8 R105/09/23 09:056.2 1
sec-Butylbenzene 93.1 ug/kg 05/09/23 13:07 135-98-8 M1,R105/09/23 09:056.2 1
tert-Butylbenzene ND ug/kg 05/09/23 13:07 98-06-6 R105/09/23 09:056.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 109 Lab ID: 92666252004 Collected: 05/03/23 15:00 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/09/23 13:07 56-23-5 M1,R105/09/23 09:056.2 1
Chlorobenzene ND ug/kg 05/09/23 13:07 108-90-7 M1,R105/09/23 09:056.2 1
Chloroethane ND ug/kg 05/09/23 13:07 75-00-3 R105/09/23 09:0512.3 1
Chloroform ND ug/kg 05/09/23 13:07 67-66-3 M1,R105/09/23 09:056.2 1
Chloromethane ND ug/kg 05/09/23 13:07 74-87-3 R105/09/23 09:0512.3 1
2-Chlorotoluene ND ug/kg 05/09/23 13:07 95-49-8 M1,R105/09/23 09:056.2 1
4-Chlorotoluene ND ug/kg 05/09/23 13:07 106-43-4 M1,R105/09/23 09:056.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/09/23 13:07 96-12-8 M1,R105/09/23 09:056.2 1
Dibromochloromethane ND ug/kg 05/09/23 13:07 124-48-1 M1,R105/09/23 09:056.2 1
1,2-Dibromoethane (EDB) ND ug/kg 05/09/23 13:07 106-93-4 M1,R105/09/23 09:056.2 1
Dibromomethane ND ug/kg 05/09/23 13:07 74-95-3 M1,R105/09/23 09:056.2 1
1,2-Dichlorobenzene ND ug/kg 05/09/23 13:07 95-50-1 M1,R105/09/23 09:056.2 1
1,3-Dichlorobenzene ND ug/kg 05/09/23 13:07 541-73-1 M1,R105/09/23 09:056.2 1
1,4-Dichlorobenzene ND ug/kg 05/09/23 13:07 106-46-7 M1,R105/09/23 09:056.2 1
Dichlorodifluoromethane ND ug/kg 05/09/23 13:07 75-71-8 L1,R105/09/23 09:0512.3 1
1,1-Dichloroethane ND ug/kg 05/09/23 13:07 75-34-3 M1,R105/09/23 09:056.2 1
1,2-Dichloroethane ND ug/kg 05/09/23 13:07 107-06-2 M1,R105/09/23 09:056.2 1
1,1-Dichloroethene ND ug/kg 05/09/23 13:07 75-35-4 M1,R105/09/23 09:056.2 1
cis-1,2-Dichloroethene ND ug/kg 05/09/23 13:07 156-59-2 M1,R105/09/23 09:056.2 1
trans-1,2-Dichloroethene ND ug/kg 05/09/23 13:07 156-60-5 M1,R105/09/23 09:056.2 1
1,2-Dichloropropane ND ug/kg 05/09/23 13:07 78-87-5 M1,R105/09/23 09:056.2 1
1,3-Dichloropropane ND ug/kg 05/09/23 13:07 142-28-9 M1,R105/09/23 09:056.2 1
2,2-Dichloropropane ND ug/kg 05/09/23 13:07 594-20-7 R105/09/23 09:056.2 1
1,1-Dichloropropene ND ug/kg 05/09/23 13:07 563-58-6 M1,R105/09/23 09:056.2 1
cis-1,3-Dichloropropene ND ug/kg 05/09/23 13:07 10061-01-5 M1,R105/09/23 09:056.2 1
trans-1,3-Dichloropropene ND ug/kg 05/09/23 13:07 10061-02-6 M1,R105/09/23 09:056.2 1
Diisopropyl ether ND ug/kg 05/09/23 13:07 108-20-3 M1,R105/09/23 09:056.2 1
Ethylbenzene ND ug/kg 05/09/23 13:07 100-41-4 M1,R105/09/23 09:056.2 1
Hexachloro-1,3-butadiene ND ug/kg 05/09/23 13:07 87-68-3 R105/09/23 09:0512.3 1
2-Hexanone ND ug/kg 05/09/23 13:07 591-78-6 R105/09/23 09:0561.6 1
Isopropylbenzene (Cumene)33.3 ug/kg 05/09/23 13:07 98-82-8 M1,R105/09/23 09:056.2 1
p-Isopropyltoluene 193 ug/kg 05/09/23 13:07 99-87-6 R105/09/23 09:056.2 1
Methylene Chloride ND ug/kg 05/09/23 13:07 75-09-2 M1,R105/09/23 09:0524.6 1
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/09/23 13:07 108-10-1 M1,R105/09/23 09:0561.6 1
Methyl-tert-butyl ether ND ug/kg 05/09/23 13:07 1634-04-4 M1,R105/09/23 09:056.2 1
Naphthalene 93.3 ug/kg 05/09/23 13:07 91-20-3 R105/09/23 09:056.2 1
n-Propylbenzene 57.7 ug/kg 05/09/23 13:07 103-65-1 R105/09/23 09:056.2 1
Styrene ND ug/kg 05/09/23 13:07 100-42-5 M1,R105/09/23 09:056.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/09/23 13:07 630-20-6 M1,R105/09/23 09:056.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/09/23 13:07 79-34-5 R105/09/23 09:056.2 1
Tetrachloroethene ND ug/kg 05/09/23 13:07 127-18-4 R105/09/23 09:056.2 1
Toluene ND ug/kg 05/09/23 13:07 108-88-3 M1,R105/09/23 09:056.2 1
1,2,3-Trichlorobenzene ND ug/kg 05/09/23 13:07 87-61-6 R105/09/23 09:056.2 1
1,2,4-Trichlorobenzene ND ug/kg 05/09/23 13:07 120-82-1 R105/09/23 09:056.2 1
1,1,1-Trichloroethane ND ug/kg 05/09/23 13:07 71-55-6 M1,R105/09/23 09:056.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 109 Lab ID: 92666252004 Collected: 05/03/23 15:00 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/09/23 13:07 79-00-5 M1,R105/09/23 09:056.2 1
Trichloroethene ND ug/kg 05/09/23 13:07 79-01-6 M1,R105/09/23 09:056.2 1
Trichlorofluoromethane ND ug/kg 05/09/23 13:07 75-69-4 R105/09/23 09:056.2 1
1,2,3-Trichloropropane ND ug/kg 05/09/23 13:07 96-18-4 M1,R105/09/23 09:056.2 1
1,2,4-Trimethylbenzene 339 ug/kg 05/09/23 13:07 95-63-6 R105/09/23 09:056.2 1
1,3,5-Trimethylbenzene 58.5 ug/kg 05/09/23 13:07 108-67-8 R105/09/23 09:056.2 1
Vinyl acetate ND ug/kg 05/09/23 13:07 108-05-4 R105/09/23 09:0561.6 1
Vinyl chloride ND ug/kg 05/09/23 13:07 75-01-4 M1,R105/09/23 09:0512.3 1
Xylene (Total) ND ug/kg 05/09/23 13:07 1330-20-7 MS,RS05/09/23 09:0512.3 1
m&p-Xylene ND ug/kg 05/09/23 13:07 179601-23-1 M1,R105/09/23 09:0512.3 1
o-Xylene ND ug/kg 05/09/23 13:07 95-47-6 M1,R105/09/23 09:056.2 1
Surrogates
Toluene-d8 (S) 100 %05/09/23 13:07 2037-26-505/09/23 09:0570-130 1
4-Bromofluorobenzene (S) 98 %05/09/23 13:07 460-00-405/09/23 09:0570-130 1
1,2-Dichloroethane-d4 (S) 100 %05/09/23 13:07 17060-07-005/09/23 09:0570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.7 %05/08/23 14:46 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 110 Lab ID: 92666252005 Collected: 05/03/23 15:10 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/11/23 10:36 83-32-905/10/23 15:09394 1
Acenaphthylene ND ug/kg 05/11/23 10:36 208-96-805/10/23 15:09394 1
Aniline ND ug/kg 05/11/23 10:36 62-53-305/10/23 15:09394 1
Anthracene ND ug/kg 05/11/23 10:36 120-12-705/10/23 15:09394 1
Benzo(a)anthracene ND ug/kg 05/11/23 10:36 56-55-305/10/23 15:09394 1
Benzo(a)pyrene ND ug/kg 05/11/23 10:36 50-32-805/10/23 15:09394 1
Benzo(b)fluoranthene ND ug/kg 05/11/23 10:36 205-99-205/10/23 15:09394 1
Benzo(g,h,i)perylene ND ug/kg 05/11/23 10:36 191-24-205/10/23 15:09394 1
Benzo(k)fluoranthene ND ug/kg 05/11/23 10:36 207-08-905/10/23 15:09394 1
Benzoic Acid ND ug/kg 05/11/23 10:36 65-85-005/10/23 15:091970 1
Benzyl alcohol ND ug/kg 05/11/23 10:36 100-51-605/10/23 15:09788 1
4-Bromophenylphenyl ether ND ug/kg 05/11/23 10:36 101-55-305/10/23 15:09394 1
Butylbenzylphthalate ND ug/kg 05/11/23 10:36 85-68-705/10/23 15:09394 1
4-Chloro-3-methylphenol ND ug/kg 05/11/23 10:36 59-50-705/10/23 15:09788 1
4-Chloroaniline ND ug/kg 05/11/23 10:36 106-47-805/10/23 15:09788 1
bis(2-Chloroethoxy)methane ND ug/kg 05/11/23 10:36 111-91-105/10/23 15:09394 1
bis(2-Chloroethyl) ether ND ug/kg 05/11/23 10:36 111-44-405/10/23 15:09394 1
2-Chloronaphthalene ND ug/kg 05/11/23 10:36 91-58-705/10/23 15:09394 1
2-Chlorophenol ND ug/kg 05/11/23 10:36 95-57-805/10/23 15:09394 1
4-Chlorophenylphenyl ether ND ug/kg 05/11/23 10:36 7005-72-305/10/23 15:09394 1
Chrysene ND ug/kg 05/11/23 10:36 218-01-905/10/23 15:09394 1
Dibenz(a,h)anthracene ND ug/kg 05/11/23 10:36 53-70-305/10/23 15:09394 1
Dibenzofuran ND ug/kg 05/11/23 10:36 132-64-905/10/23 15:09394 1
1,2-Dichlorobenzene ND ug/kg 05/11/23 10:36 95-50-105/10/23 15:09394 1
1,3-Dichlorobenzene ND ug/kg 05/11/23 10:36 541-73-105/10/23 15:09394 1
1,4-Dichlorobenzene ND ug/kg 05/11/23 10:36 106-46-705/10/23 15:09394 1
3,3'-Dichlorobenzidine ND ug/kg 05/11/23 10:36 91-94-105/10/23 15:09788 1
2,4-Dichlorophenol ND ug/kg 05/11/23 10:36 120-83-205/10/23 15:09394 1
Diethylphthalate ND ug/kg 05/11/23 10:36 84-66-205/10/23 15:09394 1
2,4-Dimethylphenol ND ug/kg 05/11/23 10:36 105-67-905/10/23 15:09394 1
Dimethylphthalate ND ug/kg 05/11/23 10:36 131-11-305/10/23 15:09394 1
Di-n-butylphthalate ND ug/kg 05/11/23 10:36 84-74-205/10/23 15:09394 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/11/23 10:36 534-52-105/10/23 15:09788 1
2,4-Dinitrophenol ND ug/kg 05/11/23 10:36 51-28-5 v105/10/23 15:091970 1
2,4-Dinitrotoluene ND ug/kg 05/11/23 10:36 121-14-205/10/23 15:09394 1
2,6-Dinitrotoluene ND ug/kg 05/11/23 10:36 606-20-205/10/23 15:09394 1
Di-n-octylphthalate ND ug/kg 05/11/23 10:36 117-84-005/10/23 15:09394 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/11/23 10:36 117-81-705/10/23 15:09394 1
Fluoranthene ND ug/kg 05/11/23 10:36 206-44-005/10/23 15:09394 1
Fluorene ND ug/kg 05/11/23 10:36 86-73-705/10/23 15:09394 1
Hexachloro-1,3-butadiene ND ug/kg 05/11/23 10:36 87-68-305/10/23 15:09394 1
Hexachlorobenzene ND ug/kg 05/11/23 10:36 118-74-105/10/23 15:09394 1
Hexachlorocyclopentadiene ND ug/kg 05/11/23 10:36 77-47-405/10/23 15:09394 1
Hexachloroethane ND ug/kg 05/11/23 10:36 67-72-105/10/23 15:09394 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/11/23 10:36 193-39-505/10/23 15:09394 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 110 Lab ID: 92666252005 Collected: 05/03/23 15:10 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/11/23 10:36 78-59-105/10/23 15:09394 1
1-Methylnaphthalene ND ug/kg 05/11/23 10:36 90-12-005/10/23 15:09394 1
2-Methylnaphthalene ND ug/kg 05/11/23 10:36 91-57-605/10/23 15:09394 1
2-Methylphenol(o-Cresol) ND ug/kg 05/11/23 10:36 95-48-705/10/23 15:09394 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/11/23 10:36 15831-10-405/10/23 15:09394 1
Naphthalene ND ug/kg 05/11/23 10:36 91-20-305/10/23 15:09394 1
2-Nitroaniline ND ug/kg 05/11/23 10:36 88-74-405/10/23 15:091970 1
3-Nitroaniline ND ug/kg 05/11/23 10:36 99-09-205/10/23 15:091970 1
4-Nitroaniline ND ug/kg 05/11/23 10:36 100-01-605/10/23 15:09788 1
Nitrobenzene ND ug/kg 05/11/23 10:36 98-95-305/10/23 15:09394 1
2-Nitrophenol ND ug/kg 05/11/23 10:36 88-75-505/10/23 15:09394 1
4-Nitrophenol ND ug/kg 05/11/23 10:36 100-02-705/10/23 15:091970 1
N-Nitrosodimethylamine ND ug/kg 05/11/23 10:36 62-75-905/10/23 15:09394 1
N-Nitroso-di-n-propylamine ND ug/kg 05/11/23 10:36 621-64-705/10/23 15:09394 1
N-Nitrosodiphenylamine ND ug/kg 05/11/23 10:36 86-30-605/10/23 15:09394 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/11/23 10:36 108-60-105/10/23 15:09394 1
Pentachlorophenol ND ug/kg 05/11/23 10:36 87-86-505/10/23 15:09788 1
Phenanthrene ND ug/kg 05/11/23 10:36 85-01-805/10/23 15:09394 1
Phenol ND ug/kg 05/11/23 10:36 108-95-205/10/23 15:09394 1
Pyrene ND ug/kg 05/11/23 10:36 129-00-005/10/23 15:09394 1
Pyridine ND ug/kg 05/11/23 10:36 110-86-105/10/23 15:09394 1
1,2,4-Trichlorobenzene ND ug/kg 05/11/23 10:36 120-82-105/10/23 15:09394 1
2,4,5-Trichlorophenol ND ug/kg 05/11/23 10:36 95-95-405/10/23 15:09394 1
2,4,6-Trichlorophenol ND ug/kg 05/11/23 10:36 88-06-205/10/23 15:09394 1
Surrogates
Nitrobenzene-d5 (S) 58 %05/11/23 10:36 4165-60-005/10/23 15:0910-130 1
2-Fluorobiphenyl (S) 52 %05/11/23 10:36 321-60-805/10/23 15:0910-130 1
Terphenyl-d14 (S) 59 %05/11/23 10:36 1718-51-005/10/23 15:0910-130 1
Phenol-d6 (S) 56 %05/11/23 10:36 13127-88-305/10/23 15:0910-130 1
2-Fluorophenol (S) 54 %05/11/23 10:36 367-12-405/10/23 15:0910-130 1
2,4,6-Tribromophenol (S) 61 %05/11/23 10:36 118-79-605/10/23 15:0910-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/09/23 15:16 67-64-105/09/23 09:05281 2.5
Benzene 18.2 ug/kg 05/09/23 15:16 71-43-205/09/23 09:0514.1 2.5
Bromobenzene ND ug/kg 05/09/23 15:16 108-86-105/09/23 09:0514.1 2.5
Bromochloromethane ND ug/kg 05/09/23 15:16 74-97-505/09/23 09:0514.1 2.5
Bromodichloromethane ND ug/kg 05/09/23 15:16 75-27-405/09/23 09:0514.1 2.5
Bromoform ND ug/kg 05/09/23 15:16 75-25-205/09/23 09:0514.1 2.5
Bromomethane ND ug/kg 05/09/23 15:16 74-83-9 IK,v105/09/23 09:0556.2 2.5
2-Butanone (MEK) ND ug/kg 05/09/23 15:16 78-93-305/09/23 09:05281 2.5
n-Butylbenzene ND ug/kg 05/09/23 15:16 104-51-805/09/23 09:0514.1 2.5
sec-Butylbenzene 17.0 ug/kg 05/09/23 15:16 135-98-805/09/23 09:0514.1 2.5
tert-Butylbenzene ND ug/kg 05/09/23 15:16 98-06-605/09/23 09:0514.1 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 110 Lab ID: 92666252005 Collected: 05/03/23 15:10 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/09/23 15:16 56-23-505/09/23 09:0514.1 2.5
Chlorobenzene ND ug/kg 05/09/23 15:16 108-90-705/09/23 09:0514.1 2.5
Chloroethane ND ug/kg 05/09/23 15:16 75-00-305/09/23 09:0528.1 2.5
Chloroform ND ug/kg 05/09/23 15:16 67-66-305/09/23 09:0514.1 2.5
Chloromethane 7890 ug/kg 05/09/23 15:16 74-87-305/09/23 09:0528.1 2.5
2-Chlorotoluene ND ug/kg 05/09/23 15:16 95-49-805/09/23 09:0514.1 2.5
4-Chlorotoluene ND ug/kg 05/09/23 15:16 106-43-405/09/23 09:0514.1 2.5
1,2-Dibromo-3-chloropropane ND ug/kg 05/09/23 15:16 96-12-805/09/23 09:0514.1 2.5
Dibromochloromethane ND ug/kg 05/09/23 15:16 124-48-105/09/23 09:0514.1 2.5
1,2-Dibromoethane (EDB) ND ug/kg 05/09/23 15:16 106-93-405/09/23 09:0514.1 2.5
Dibromomethane ND ug/kg 05/09/23 15:16 74-95-305/09/23 09:0514.1 2.5
1,2-Dichlorobenzene ND ug/kg 05/09/23 15:16 95-50-105/09/23 09:0514.1 2.5
1,3-Dichlorobenzene ND ug/kg 05/09/23 15:16 541-73-105/09/23 09:0514.1 2.5
1,4-Dichlorobenzene ND ug/kg 05/09/23 15:16 106-46-705/09/23 09:0514.1 2.5
Dichlorodifluoromethane ND ug/kg 05/09/23 15:16 75-71-8 L105/09/23 09:0528.1 2.5
1,1-Dichloroethane ND ug/kg 05/09/23 15:16 75-34-305/09/23 09:0514.1 2.5
1,2-Dichloroethane ND ug/kg 05/09/23 15:16 107-06-205/09/23 09:0514.1 2.5
1,1-Dichloroethene ND ug/kg 05/09/23 15:16 75-35-405/09/23 09:0514.1 2.5
cis-1,2-Dichloroethene ND ug/kg 05/09/23 15:16 156-59-205/09/23 09:0514.1 2.5
trans-1,2-Dichloroethene ND ug/kg 05/09/23 15:16 156-60-505/09/23 09:0514.1 2.5
1,2-Dichloropropane ND ug/kg 05/09/23 15:16 78-87-505/09/23 09:0514.1 2.5
1,3-Dichloropropane ND ug/kg 05/09/23 15:16 142-28-905/09/23 09:0514.1 2.5
2,2-Dichloropropane ND ug/kg 05/09/23 15:16 594-20-705/09/23 09:0514.1 2.5
1,1-Dichloropropene ND ug/kg 05/09/23 15:16 563-58-605/09/23 09:0514.1 2.5
cis-1,3-Dichloropropene ND ug/kg 05/09/23 15:16 10061-01-505/09/23 09:0514.1 2.5
trans-1,3-Dichloropropene ND ug/kg 05/09/23 15:16 10061-02-605/09/23 09:0514.1 2.5
Diisopropyl ether ND ug/kg 05/09/23 15:16 108-20-305/09/23 09:0514.1 2.5
Ethylbenzene 18.7 ug/kg 05/09/23 15:16 100-41-405/09/23 09:0514.1 2.5
Hexachloro-1,3-butadiene ND ug/kg 05/09/23 15:16 87-68-305/09/23 09:0528.1 2.5
2-Hexanone ND ug/kg 05/09/23 15:16 591-78-605/09/23 09:05141 2.5
Isopropylbenzene (Cumene)14.4 ug/kg 05/09/23 15:16 98-82-805/09/23 09:0514.1 2.5
p-Isopropyltoluene ND ug/kg 05/09/23 15:16 99-87-605/09/23 09:0514.1 2.5
Methylene Chloride ND ug/kg 05/09/23 15:16 75-09-205/09/23 09:0556.2 2.5
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/09/23 15:16 108-10-105/09/23 09:05141 2.5
Methyl-tert-butyl ether ND ug/kg 05/09/23 15:16 1634-04-405/09/23 09:0514.1 2.5
Naphthalene ND ug/kg 05/09/23 15:16 91-20-305/09/23 09:0514.1 2.5
n-Propylbenzene 25.8 ug/kg 05/09/23 15:16 103-65-105/09/23 09:0514.1 2.5
Styrene ND ug/kg 05/09/23 15:16 100-42-505/09/23 09:0514.1 2.5
1,1,1,2-Tetrachloroethane ND ug/kg 05/09/23 15:16 630-20-605/09/23 09:0514.1 2.5
1,1,2,2-Tetrachloroethane ND ug/kg 05/09/23 15:16 79-34-505/09/23 09:0514.1 2.5
Tetrachloroethene ND ug/kg 05/09/23 15:16 127-18-405/09/23 09:0514.1 2.5
Toluene ND ug/kg 05/09/23 15:16 108-88-305/09/23 09:0514.1 2.5
1,2,3-Trichlorobenzene ND ug/kg 05/09/23 15:16 87-61-605/09/23 09:0514.1 2.5
1,2,4-Trichlorobenzene ND ug/kg 05/09/23 15:16 120-82-105/09/23 09:0514.1 2.5
1,1,1-Trichloroethane ND ug/kg 05/09/23 15:16 71-55-605/09/23 09:0514.1 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 110 Lab ID: 92666252005 Collected: 05/03/23 15:10 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/09/23 15:16 79-00-505/09/23 09:0514.1 2.5
Trichloroethene ND ug/kg 05/09/23 15:16 79-01-605/09/23 09:0514.1 2.5
Trichlorofluoromethane ND ug/kg 05/09/23 15:16 75-69-405/09/23 09:0514.1 2.5
1,2,3-Trichloropropane ND ug/kg 05/09/23 15:16 96-18-405/09/23 09:0514.1 2.5
1,2,4-Trimethylbenzene 32.0 ug/kg 05/09/23 15:16 95-63-605/09/23 09:0514.1 2.5
1,3,5-Trimethylbenzene ND ug/kg 05/09/23 15:16 108-67-805/09/23 09:0514.1 2.5
Vinyl acetate ND ug/kg 05/09/23 15:16 108-05-405/09/23 09:05141 2.5
Vinyl chloride ND ug/kg 05/09/23 15:16 75-01-405/09/23 09:0528.1 2.5
Xylene (Total) ND ug/kg 05/09/23 15:16 1330-20-705/09/23 09:0528.1 2.5
m&p-Xylene ND ug/kg 05/09/23 15:16 179601-23-105/09/23 09:0528.1 2.5
o-Xylene ND ug/kg 05/09/23 15:16 95-47-605/09/23 09:0514.1 2.5
Surrogates
Toluene-d8 (S) 101 %05/09/23 15:16 2037-26-505/09/23 09:0570-130 2.5
4-Bromofluorobenzene (S) 95 %05/09/23 15:16 460-00-405/09/23 09:0570-130 2.5
1,2-Dichloroethane-d4 (S) 101 %05/09/23 15:16 17060-07-005/09/23 09:0570-130 2.5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.3 %05/08/23 14:46 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 125 Lab ID: 92666252006 Collected: 05/04/23 10:30 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/11/23 11:02 83-32-905/10/23 15:09392 1
Acenaphthylene ND ug/kg 05/11/23 11:02 208-96-805/10/23 15:09392 1
Aniline ND ug/kg 05/11/23 11:02 62-53-305/10/23 15:09392 1
Anthracene ND ug/kg 05/11/23 11:02 120-12-705/10/23 15:09392 1
Benzo(a)anthracene ND ug/kg 05/11/23 11:02 56-55-305/10/23 15:09392 1
Benzo(a)pyrene ND ug/kg 05/11/23 11:02 50-32-805/10/23 15:09392 1
Benzo(b)fluoranthene ND ug/kg 05/11/23 11:02 205-99-205/10/23 15:09392 1
Benzo(g,h,i)perylene ND ug/kg 05/11/23 11:02 191-24-205/10/23 15:09392 1
Benzo(k)fluoranthene ND ug/kg 05/11/23 11:02 207-08-905/10/23 15:09392 1
Benzoic Acid ND ug/kg 05/11/23 11:02 65-85-005/10/23 15:091960 1
Benzyl alcohol ND ug/kg 05/11/23 11:02 100-51-605/10/23 15:09784 1
4-Bromophenylphenyl ether ND ug/kg 05/11/23 11:02 101-55-305/10/23 15:09392 1
Butylbenzylphthalate ND ug/kg 05/11/23 11:02 85-68-705/10/23 15:09392 1
4-Chloro-3-methylphenol ND ug/kg 05/11/23 11:02 59-50-705/10/23 15:09784 1
4-Chloroaniline ND ug/kg 05/11/23 11:02 106-47-805/10/23 15:09784 1
bis(2-Chloroethoxy)methane ND ug/kg 05/11/23 11:02 111-91-105/10/23 15:09392 1
bis(2-Chloroethyl) ether ND ug/kg 05/11/23 11:02 111-44-405/10/23 15:09392 1
2-Chloronaphthalene ND ug/kg 05/11/23 11:02 91-58-705/10/23 15:09392 1
2-Chlorophenol ND ug/kg 05/11/23 11:02 95-57-805/10/23 15:09392 1
4-Chlorophenylphenyl ether ND ug/kg 05/11/23 11:02 7005-72-305/10/23 15:09392 1
Chrysene ND ug/kg 05/11/23 11:02 218-01-905/10/23 15:09392 1
Dibenz(a,h)anthracene ND ug/kg 05/11/23 11:02 53-70-305/10/23 15:09392 1
Dibenzofuran ND ug/kg 05/11/23 11:02 132-64-905/10/23 15:09392 1
1,2-Dichlorobenzene ND ug/kg 05/11/23 11:02 95-50-105/10/23 15:09392 1
1,3-Dichlorobenzene ND ug/kg 05/11/23 11:02 541-73-105/10/23 15:09392 1
1,4-Dichlorobenzene ND ug/kg 05/11/23 11:02 106-46-705/10/23 15:09392 1
3,3'-Dichlorobenzidine ND ug/kg 05/11/23 11:02 91-94-105/10/23 15:09784 1
2,4-Dichlorophenol ND ug/kg 05/11/23 11:02 120-83-205/10/23 15:09392 1
Diethylphthalate ND ug/kg 05/11/23 11:02 84-66-205/10/23 15:09392 1
2,4-Dimethylphenol ND ug/kg 05/11/23 11:02 105-67-905/10/23 15:09392 1
Dimethylphthalate ND ug/kg 05/11/23 11:02 131-11-305/10/23 15:09392 1
Di-n-butylphthalate ND ug/kg 05/11/23 11:02 84-74-205/10/23 15:09392 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/11/23 11:02 534-52-105/10/23 15:09784 1
2,4-Dinitrophenol ND ug/kg 05/11/23 11:02 51-28-5 v105/10/23 15:091960 1
2,4-Dinitrotoluene ND ug/kg 05/11/23 11:02 121-14-205/10/23 15:09392 1
2,6-Dinitrotoluene ND ug/kg 05/11/23 11:02 606-20-205/10/23 15:09392 1
Di-n-octylphthalate ND ug/kg 05/11/23 11:02 117-84-005/10/23 15:09392 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/11/23 11:02 117-81-705/10/23 15:09392 1
Fluoranthene ND ug/kg 05/11/23 11:02 206-44-005/10/23 15:09392 1
Fluorene ND ug/kg 05/11/23 11:02 86-73-705/10/23 15:09392 1
Hexachloro-1,3-butadiene ND ug/kg 05/11/23 11:02 87-68-305/10/23 15:09392 1
Hexachlorobenzene ND ug/kg 05/11/23 11:02 118-74-105/10/23 15:09392 1
Hexachlorocyclopentadiene ND ug/kg 05/11/23 11:02 77-47-405/10/23 15:09392 1
Hexachloroethane ND ug/kg 05/11/23 11:02 67-72-105/10/23 15:09392 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/11/23 11:02 193-39-505/10/23 15:09392 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 125 Lab ID: 92666252006 Collected: 05/04/23 10:30 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/11/23 11:02 78-59-105/10/23 15:09392 1
1-Methylnaphthalene 808 ug/kg 05/11/23 11:02 90-12-005/10/23 15:09392 1
2-Methylnaphthalene 1240 ug/kg 05/11/23 11:02 91-57-605/10/23 15:09392 1
2-Methylphenol(o-Cresol) ND ug/kg 05/11/23 11:02 95-48-705/10/23 15:09392 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/11/23 11:02 15831-10-405/10/23 15:09392 1
Naphthalene 432 ug/kg 05/11/23 11:02 91-20-305/10/23 15:09392 1
2-Nitroaniline ND ug/kg 05/11/23 11:02 88-74-405/10/23 15:091960 1
3-Nitroaniline ND ug/kg 05/11/23 11:02 99-09-205/10/23 15:091960 1
4-Nitroaniline ND ug/kg 05/11/23 11:02 100-01-605/10/23 15:09784 1
Nitrobenzene ND ug/kg 05/11/23 11:02 98-95-305/10/23 15:09392 1
2-Nitrophenol ND ug/kg 05/11/23 11:02 88-75-505/10/23 15:09392 1
4-Nitrophenol ND ug/kg 05/11/23 11:02 100-02-705/10/23 15:091960 1
N-Nitrosodimethylamine ND ug/kg 05/11/23 11:02 62-75-905/10/23 15:09392 1
N-Nitroso-di-n-propylamine ND ug/kg 05/11/23 11:02 621-64-705/10/23 15:09392 1
N-Nitrosodiphenylamine ND ug/kg 05/11/23 11:02 86-30-605/10/23 15:09392 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/11/23 11:02 108-60-105/10/23 15:09392 1
Pentachlorophenol ND ug/kg 05/11/23 11:02 87-86-505/10/23 15:09784 1
Phenanthrene ND ug/kg 05/11/23 11:02 85-01-805/10/23 15:09392 1
Phenol ND ug/kg 05/11/23 11:02 108-95-205/10/23 15:09392 1
Pyrene ND ug/kg 05/11/23 11:02 129-00-005/10/23 15:09392 1
Pyridine ND ug/kg 05/11/23 11:02 110-86-105/10/23 15:09392 1
1,2,4-Trichlorobenzene ND ug/kg 05/11/23 11:02 120-82-105/10/23 15:09392 1
2,4,5-Trichlorophenol ND ug/kg 05/11/23 11:02 95-95-405/10/23 15:09392 1
2,4,6-Trichlorophenol ND ug/kg 05/11/23 11:02 88-06-205/10/23 15:09392 1
Surrogates
Nitrobenzene-d5 (S) 65 %05/11/23 11:02 4165-60-005/10/23 15:0910-130 1
2-Fluorobiphenyl (S) 50 %05/11/23 11:02 321-60-805/10/23 15:0910-130 1
Terphenyl-d14 (S) 64 %05/11/23 11:02 1718-51-005/10/23 15:0910-130 1
Phenol-d6 (S) 60 %05/11/23 11:02 13127-88-305/10/23 15:0910-130 1
2-Fluorophenol (S) 56 %05/11/23 11:02 367-12-405/10/23 15:0910-130 1
2,4,6-Tribromophenol (S) 69 %05/11/23 11:02 118-79-605/10/23 15:0910-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/09/23 15:35 67-64-105/09/23 09:05545 5
Benzene ND ug/kg 05/09/23 15:35 71-43-205/09/23 09:0527.3 5
Bromobenzene ND ug/kg 05/09/23 15:35 108-86-105/09/23 09:0527.3 5
Bromochloromethane ND ug/kg 05/09/23 15:35 74-97-505/09/23 09:0527.3 5
Bromodichloromethane ND ug/kg 05/09/23 15:35 75-27-405/09/23 09:0527.3 5
Bromoform ND ug/kg 05/09/23 15:35 75-25-205/09/23 09:0527.3 5
Bromomethane ND ug/kg 05/09/23 15:35 74-83-9 IK,v105/09/23 09:05109 5
2-Butanone (MEK) ND ug/kg 05/09/23 15:35 78-93-305/09/23 09:05545 5
n-Butylbenzene 1230 ug/kg 05/09/23 15:35 104-51-805/09/23 09:0527.3 5
sec-Butylbenzene 983 ug/kg 05/09/23 15:35 135-98-805/09/23 09:0527.3 5
tert-Butylbenzene ND ug/kg 05/09/23 15:35 98-06-605/09/23 09:0527.3 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 125 Lab ID: 92666252006 Collected: 05/04/23 10:30 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/09/23 15:35 56-23-505/09/23 09:0527.3 5
Chlorobenzene ND ug/kg 05/09/23 15:35 108-90-705/09/23 09:0527.3 5
Chloroethane ND ug/kg 05/09/23 15:35 75-00-305/09/23 09:0554.5 5
Chloroform ND ug/kg 05/09/23 15:35 67-66-305/09/23 09:0527.3 5
Chloromethane 18300 ug/kg 05/09/23 15:35 74-87-305/09/23 09:0554.5 5
2-Chlorotoluene ND ug/kg 05/09/23 15:35 95-49-805/09/23 09:0527.3 5
4-Chlorotoluene ND ug/kg 05/09/23 15:35 106-43-405/09/23 09:0527.3 5
1,2-Dibromo-3-chloropropane ND ug/kg 05/09/23 15:35 96-12-805/09/23 09:0527.3 5
Dibromochloromethane ND ug/kg 05/09/23 15:35 124-48-105/09/23 09:0527.3 5
1,2-Dibromoethane (EDB) ND ug/kg 05/09/23 15:35 106-93-405/09/23 09:0527.3 5
Dibromomethane ND ug/kg 05/09/23 15:35 74-95-305/09/23 09:0527.3 5
1,2-Dichlorobenzene ND ug/kg 05/09/23 15:35 95-50-105/09/23 09:0527.3 5
1,3-Dichlorobenzene ND ug/kg 05/09/23 15:35 541-73-105/09/23 09:0527.3 5
1,4-Dichlorobenzene ND ug/kg 05/09/23 15:35 106-46-705/09/23 09:0527.3 5
Dichlorodifluoromethane ND ug/kg 05/09/23 15:35 75-71-8 L105/09/23 09:0554.5 5
1,1-Dichloroethane ND ug/kg 05/09/23 15:35 75-34-305/09/23 09:0527.3 5
1,2-Dichloroethane ND ug/kg 05/09/23 15:35 107-06-205/09/23 09:0527.3 5
1,1-Dichloroethene ND ug/kg 05/09/23 15:35 75-35-405/09/23 09:0527.3 5
cis-1,2-Dichloroethene ND ug/kg 05/09/23 15:35 156-59-205/09/23 09:0527.3 5
trans-1,2-Dichloroethene ND ug/kg 05/09/23 15:35 156-60-505/09/23 09:0527.3 5
1,2-Dichloropropane ND ug/kg 05/09/23 15:35 78-87-505/09/23 09:0527.3 5
1,3-Dichloropropane ND ug/kg 05/09/23 15:35 142-28-905/09/23 09:0527.3 5
2,2-Dichloropropane ND ug/kg 05/09/23 15:35 594-20-705/09/23 09:0527.3 5
1,1-Dichloropropene ND ug/kg 05/09/23 15:35 563-58-605/09/23 09:0527.3 5
cis-1,3-Dichloropropene ND ug/kg 05/09/23 15:35 10061-01-505/09/23 09:0527.3 5
trans-1,3-Dichloropropene ND ug/kg 05/09/23 15:35 10061-02-605/09/23 09:0527.3 5
Diisopropyl ether ND ug/kg 05/09/23 15:35 108-20-305/09/23 09:0527.3 5
Ethylbenzene 802 ug/kg 05/09/23 15:35 100-41-405/09/23 09:0527.3 5
Hexachloro-1,3-butadiene ND ug/kg 05/09/23 15:35 87-68-305/09/23 09:0554.5 5
2-Hexanone ND ug/kg 05/09/23 15:35 591-78-605/09/23 09:05273 5
Isopropylbenzene (Cumene)550 ug/kg 05/09/23 15:35 98-82-805/09/23 09:0527.3 5
p-Isopropyltoluene ND ug/kg 05/09/23 15:35 99-87-605/09/23 09:0527.3 5
Methylene Chloride ND ug/kg 05/09/23 15:35 75-09-205/09/23 09:05109 5
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/09/23 15:35 108-10-105/09/23 09:05273 5
Methyl-tert-butyl ether ND ug/kg 05/09/23 15:35 1634-04-405/09/23 09:0527.3 5
Naphthalene 2140 ug/kg 05/09/23 15:35 91-20-305/09/23 09:0527.3 5
n-Propylbenzene 1240 ug/kg 05/09/23 15:35 103-65-105/09/23 09:0527.3 5
Styrene 32.4 ug/kg 05/09/23 15:35 100-42-505/09/23 09:0527.3 5
1,1,1,2-Tetrachloroethane ND ug/kg 05/09/23 15:35 630-20-605/09/23 09:0527.3 5
1,1,2,2-Tetrachloroethane ND ug/kg 05/09/23 15:35 79-34-505/09/23 09:0527.3 5
Tetrachloroethene ND ug/kg 05/09/23 15:35 127-18-405/09/23 09:0527.3 5
Toluene ND ug/kg 05/09/23 15:35 108-88-305/09/23 09:0527.3 5
1,2,3-Trichlorobenzene ND ug/kg 05/09/23 15:35 87-61-605/09/23 09:0527.3 5
1,2,4-Trichlorobenzene ND ug/kg 05/09/23 15:35 120-82-105/09/23 09:0527.3 5
1,1,1-Trichloroethane ND ug/kg 05/09/23 15:35 71-55-605/09/23 09:0527.3 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 125 Lab ID: 92666252006 Collected: 05/04/23 10:30 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/09/23 15:35 79-00-505/09/23 09:0527.3 5
Trichloroethene ND ug/kg 05/09/23 15:35 79-01-605/09/23 09:0527.3 5
Trichlorofluoromethane ND ug/kg 05/09/23 15:35 75-69-405/09/23 09:0527.3 5
1,2,3-Trichloropropane ND ug/kg 05/09/23 15:35 96-18-405/09/23 09:0527.3 5
1,2,4-Trimethylbenzene 977 ug/kg 05/09/23 15:35 95-63-605/09/23 09:0527.3 5
1,3,5-Trimethylbenzene 621 ug/kg 05/09/23 15:35 108-67-805/09/23 09:0527.3 5
Vinyl acetate ND ug/kg 05/09/23 15:35 108-05-405/09/23 09:05273 5
Vinyl chloride ND ug/kg 05/09/23 15:35 75-01-405/09/23 09:0554.5 5
Xylene (Total) ND ug/kg 05/09/23 15:35 1330-20-705/09/23 09:0554.5 5
m&p-Xylene ND ug/kg 05/09/23 15:35 179601-23-105/09/23 09:0554.5 5
o-Xylene ND ug/kg 05/09/23 15:35 95-47-605/09/23 09:0527.3 5
Surrogates
Toluene-d8 (S) 100 %05/09/23 15:35 2037-26-505/09/23 09:0570-130 5
4-Bromofluorobenzene (S) 100 %05/09/23 15:35 460-00-405/09/23 09:0570-130 5
1,2-Dichloroethane-d4 (S) 100 %05/09/23 15:35 17060-07-005/09/23 09:0570-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.0 %05/08/23 14:46 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 126 Lab ID: 92666252007 Collected: 05/04/23 10:45 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/11/23 11:27 83-32-905/10/23 15:09392 1
Acenaphthylene ND ug/kg 05/11/23 11:27 208-96-805/10/23 15:09392 1
Aniline ND ug/kg 05/11/23 11:27 62-53-305/10/23 15:09392 1
Anthracene ND ug/kg 05/11/23 11:27 120-12-705/10/23 15:09392 1
Benzo(a)anthracene ND ug/kg 05/11/23 11:27 56-55-305/10/23 15:09392 1
Benzo(a)pyrene ND ug/kg 05/11/23 11:27 50-32-805/10/23 15:09392 1
Benzo(b)fluoranthene ND ug/kg 05/11/23 11:27 205-99-205/10/23 15:09392 1
Benzo(g,h,i)perylene ND ug/kg 05/11/23 11:27 191-24-205/10/23 15:09392 1
Benzo(k)fluoranthene ND ug/kg 05/11/23 11:27 207-08-905/10/23 15:09392 1
Benzoic Acid ND ug/kg 05/11/23 11:27 65-85-005/10/23 15:091960 1
Benzyl alcohol ND ug/kg 05/11/23 11:27 100-51-605/10/23 15:09784 1
4-Bromophenylphenyl ether ND ug/kg 05/11/23 11:27 101-55-305/10/23 15:09392 1
Butylbenzylphthalate ND ug/kg 05/11/23 11:27 85-68-705/10/23 15:09392 1
4-Chloro-3-methylphenol ND ug/kg 05/11/23 11:27 59-50-705/10/23 15:09784 1
4-Chloroaniline ND ug/kg 05/11/23 11:27 106-47-805/10/23 15:09784 1
bis(2-Chloroethoxy)methane ND ug/kg 05/11/23 11:27 111-91-105/10/23 15:09392 1
bis(2-Chloroethyl) ether ND ug/kg 05/11/23 11:27 111-44-405/10/23 15:09392 1
2-Chloronaphthalene ND ug/kg 05/11/23 11:27 91-58-705/10/23 15:09392 1
2-Chlorophenol ND ug/kg 05/11/23 11:27 95-57-805/10/23 15:09392 1
4-Chlorophenylphenyl ether ND ug/kg 05/11/23 11:27 7005-72-305/10/23 15:09392 1
Chrysene ND ug/kg 05/11/23 11:27 218-01-905/10/23 15:09392 1
Dibenz(a,h)anthracene ND ug/kg 05/11/23 11:27 53-70-305/10/23 15:09392 1
Dibenzofuran ND ug/kg 05/11/23 11:27 132-64-905/10/23 15:09392 1
1,2-Dichlorobenzene ND ug/kg 05/11/23 11:27 95-50-105/10/23 15:09392 1
1,3-Dichlorobenzene ND ug/kg 05/11/23 11:27 541-73-105/10/23 15:09392 1
1,4-Dichlorobenzene ND ug/kg 05/11/23 11:27 106-46-705/10/23 15:09392 1
3,3'-Dichlorobenzidine ND ug/kg 05/11/23 11:27 91-94-105/10/23 15:09784 1
2,4-Dichlorophenol ND ug/kg 05/11/23 11:27 120-83-205/10/23 15:09392 1
Diethylphthalate ND ug/kg 05/11/23 11:27 84-66-205/10/23 15:09392 1
2,4-Dimethylphenol ND ug/kg 05/11/23 11:27 105-67-905/10/23 15:09392 1
Dimethylphthalate ND ug/kg 05/11/23 11:27 131-11-305/10/23 15:09392 1
Di-n-butylphthalate ND ug/kg 05/11/23 11:27 84-74-205/10/23 15:09392 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/11/23 11:27 534-52-105/10/23 15:09784 1
2,4-Dinitrophenol ND ug/kg 05/11/23 11:27 51-28-5 v105/10/23 15:091960 1
2,4-Dinitrotoluene ND ug/kg 05/11/23 11:27 121-14-205/10/23 15:09392 1
2,6-Dinitrotoluene ND ug/kg 05/11/23 11:27 606-20-205/10/23 15:09392 1
Di-n-octylphthalate ND ug/kg 05/11/23 11:27 117-84-005/10/23 15:09392 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/11/23 11:27 117-81-705/10/23 15:09392 1
Fluoranthene ND ug/kg 05/11/23 11:27 206-44-005/10/23 15:09392 1
Fluorene 441 ug/kg 05/11/23 11:27 86-73-705/10/23 15:09392 1
Hexachloro-1,3-butadiene ND ug/kg 05/11/23 11:27 87-68-305/10/23 15:09392 1
Hexachlorobenzene ND ug/kg 05/11/23 11:27 118-74-105/10/23 15:09392 1
Hexachlorocyclopentadiene ND ug/kg 05/11/23 11:27 77-47-405/10/23 15:09392 1
Hexachloroethane ND ug/kg 05/11/23 11:27 67-72-105/10/23 15:09392 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/11/23 11:27 193-39-505/10/23 15:09392 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 126 Lab ID: 92666252007 Collected: 05/04/23 10:45 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/11/23 11:27 78-59-105/10/23 15:09392 1
1-Methylnaphthalene 2200 ug/kg 05/11/23 11:27 90-12-005/10/23 15:09392 1
2-Methylnaphthalene 3340 ug/kg 05/11/23 11:27 91-57-605/10/23 15:09392 1
2-Methylphenol(o-Cresol) ND ug/kg 05/11/23 11:27 95-48-705/10/23 15:09392 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/11/23 11:27 15831-10-405/10/23 15:09392 1
Naphthalene 1070 ug/kg 05/11/23 11:27 91-20-305/10/23 15:09392 1
2-Nitroaniline ND ug/kg 05/11/23 11:27 88-74-405/10/23 15:091960 1
3-Nitroaniline ND ug/kg 05/11/23 11:27 99-09-205/10/23 15:091960 1
4-Nitroaniline ND ug/kg 05/11/23 11:27 100-01-605/10/23 15:09784 1
Nitrobenzene ND ug/kg 05/11/23 11:27 98-95-305/10/23 15:09392 1
2-Nitrophenol ND ug/kg 05/11/23 11:27 88-75-505/10/23 15:09392 1
4-Nitrophenol ND ug/kg 05/11/23 11:27 100-02-705/10/23 15:091960 1
N-Nitrosodimethylamine ND ug/kg 05/11/23 11:27 62-75-905/10/23 15:09392 1
N-Nitroso-di-n-propylamine ND ug/kg 05/11/23 11:27 621-64-705/10/23 15:09392 1
N-Nitrosodiphenylamine ND ug/kg 05/11/23 11:27 86-30-605/10/23 15:09392 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/11/23 11:27 108-60-105/10/23 15:09392 1
Pentachlorophenol ND ug/kg 05/11/23 11:27 87-86-505/10/23 15:09784 1
Phenanthrene 662 ug/kg 05/11/23 11:27 85-01-805/10/23 15:09392 1
Phenol ND ug/kg 05/11/23 11:27 108-95-205/10/23 15:09392 1
Pyrene ND ug/kg 05/11/23 11:27 129-00-005/10/23 15:09392 1
Pyridine ND ug/kg 05/11/23 11:27 110-86-105/10/23 15:09392 1
1,2,4-Trichlorobenzene ND ug/kg 05/11/23 11:27 120-82-105/10/23 15:09392 1
2,4,5-Trichlorophenol ND ug/kg 05/11/23 11:27 95-95-405/10/23 15:09392 1
2,4,6-Trichlorophenol ND ug/kg 05/11/23 11:27 88-06-205/10/23 15:09392 1
Surrogates
Nitrobenzene-d5 (S) 75 %05/11/23 11:27 4165-60-005/10/23 15:0910-130 1
2-Fluorobiphenyl (S) 56 %05/11/23 11:27 321-60-805/10/23 15:0910-130 1
Terphenyl-d14 (S) 63 %05/11/23 11:27 1718-51-005/10/23 15:0910-130 1
Phenol-d6 (S) 61 %05/11/23 11:27 13127-88-305/10/23 15:0910-130 1
2-Fluorophenol (S) 59 %05/11/23 11:27 367-12-405/10/23 15:0910-130 1
2,4,6-Tribromophenol (S) 68 %05/11/23 11:27 118-79-605/10/23 15:0910-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/09/23 16:12 67-64-105/09/23 09:05558 5
Benzene 56.3 ug/kg 05/09/23 16:12 71-43-205/09/23 09:0527.9 5
Bromobenzene ND ug/kg 05/09/23 16:12 108-86-105/09/23 09:0527.9 5
Bromochloromethane ND ug/kg 05/09/23 16:12 74-97-505/09/23 09:0527.9 5
Bromodichloromethane ND ug/kg 05/09/23 16:12 75-27-405/09/23 09:0527.9 5
Bromoform ND ug/kg 05/09/23 16:12 75-25-205/09/23 09:0527.9 5
Bromomethane ND ug/kg 05/09/23 16:12 74-83-9 IK,v105/09/23 09:05112 5
2-Butanone (MEK) ND ug/kg 05/09/23 16:12 78-93-305/09/23 09:05558 5
n-Butylbenzene 1440 ug/kg 05/09/23 16:12 104-51-805/09/23 09:0527.9 5
sec-Butylbenzene 1170 ug/kg 05/09/23 16:12 135-98-805/09/23 09:0527.9 5
tert-Butylbenzene ND ug/kg 05/09/23 16:12 98-06-605/09/23 09:0527.9 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 126 Lab ID: 92666252007 Collected: 05/04/23 10:45 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/09/23 16:12 56-23-505/09/23 09:0527.9 5
Chlorobenzene ND ug/kg 05/09/23 16:12 108-90-705/09/23 09:0527.9 5
Chloroethane ND ug/kg 05/09/23 16:12 75-00-305/09/23 09:0555.8 5
Chloroform ND ug/kg 05/09/23 16:12 67-66-305/09/23 09:0527.9 5
Chloromethane 19400 ug/kg 05/09/23 16:12 74-87-305/09/23 09:0555.8 5
2-Chlorotoluene ND ug/kg 05/09/23 16:12 95-49-805/09/23 09:0527.9 5
4-Chlorotoluene ND ug/kg 05/09/23 16:12 106-43-405/09/23 09:0527.9 5
1,2-Dibromo-3-chloropropane ND ug/kg 05/09/23 16:12 96-12-805/09/23 09:0527.9 5
Dibromochloromethane ND ug/kg 05/09/23 16:12 124-48-105/09/23 09:0527.9 5
1,2-Dibromoethane (EDB) ND ug/kg 05/09/23 16:12 106-93-405/09/23 09:0527.9 5
Dibromomethane ND ug/kg 05/09/23 16:12 74-95-305/09/23 09:0527.9 5
1,2-Dichlorobenzene ND ug/kg 05/09/23 16:12 95-50-105/09/23 09:0527.9 5
1,3-Dichlorobenzene ND ug/kg 05/09/23 16:12 541-73-105/09/23 09:0527.9 5
1,4-Dichlorobenzene ND ug/kg 05/09/23 16:12 106-46-705/09/23 09:0527.9 5
Dichlorodifluoromethane ND ug/kg 05/09/23 16:12 75-71-8 L105/09/23 09:0555.8 5
1,1-Dichloroethane ND ug/kg 05/09/23 16:12 75-34-305/09/23 09:0527.9 5
1,2-Dichloroethane ND ug/kg 05/09/23 16:12 107-06-205/09/23 09:0527.9 5
1,1-Dichloroethene ND ug/kg 05/09/23 16:12 75-35-405/09/23 09:0527.9 5
cis-1,2-Dichloroethene ND ug/kg 05/09/23 16:12 156-59-205/09/23 09:0527.9 5
trans-1,2-Dichloroethene ND ug/kg 05/09/23 16:12 156-60-505/09/23 09:0527.9 5
1,2-Dichloropropane ND ug/kg 05/09/23 16:12 78-87-505/09/23 09:0527.9 5
1,3-Dichloropropane ND ug/kg 05/09/23 16:12 142-28-905/09/23 09:0527.9 5
2,2-Dichloropropane ND ug/kg 05/09/23 16:12 594-20-705/09/23 09:0527.9 5
1,1-Dichloropropene ND ug/kg 05/09/23 16:12 563-58-605/09/23 09:0527.9 5
cis-1,3-Dichloropropene ND ug/kg 05/09/23 16:12 10061-01-505/09/23 09:0527.9 5
trans-1,3-Dichloropropene ND ug/kg 05/09/23 16:12 10061-02-605/09/23 09:0527.9 5
Diisopropyl ether ND ug/kg 05/09/23 16:12 108-20-305/09/23 09:0527.9 5
Ethylbenzene 402 ug/kg 05/09/23 16:12 100-41-405/09/23 09:0527.9 5
Hexachloro-1,3-butadiene ND ug/kg 05/09/23 16:12 87-68-305/09/23 09:0555.8 5
2-Hexanone ND ug/kg 05/09/23 16:12 591-78-605/09/23 09:05279 5
Isopropylbenzene (Cumene)577 ug/kg 05/09/23 16:12 98-82-805/09/23 09:0527.9 5
p-Isopropyltoluene ND ug/kg 05/09/23 16:12 99-87-605/09/23 09:0527.9 5
Methylene Chloride ND ug/kg 05/09/23 16:12 75-09-205/09/23 09:05112 5
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/09/23 16:12 108-10-105/09/23 09:05279 5
Methyl-tert-butyl ether ND ug/kg 05/09/23 16:12 1634-04-405/09/23 09:0527.9 5
Naphthalene 2500 ug/kg 05/09/23 16:12 91-20-305/09/23 09:0527.9 5
n-Propylbenzene 1300 ug/kg 05/09/23 16:12 103-65-105/09/23 09:0527.9 5
Styrene ND ug/kg 05/09/23 16:12 100-42-505/09/23 09:0527.9 5
1,1,1,2-Tetrachloroethane ND ug/kg 05/09/23 16:12 630-20-605/09/23 09:0527.9 5
1,1,2,2-Tetrachloroethane ND ug/kg 05/09/23 16:12 79-34-505/09/23 09:0527.9 5
Tetrachloroethene ND ug/kg 05/09/23 16:12 127-18-405/09/23 09:0527.9 5
Toluene ND ug/kg 05/09/23 16:12 108-88-305/09/23 09:0527.9 5
1,2,3-Trichlorobenzene ND ug/kg 05/09/23 16:12 87-61-605/09/23 09:0527.9 5
1,2,4-Trichlorobenzene ND ug/kg 05/09/23 16:12 120-82-105/09/23 09:0527.9 5
1,1,1-Trichloroethane ND ug/kg 05/09/23 16:12 71-55-605/09/23 09:0527.9 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 126 Lab ID: 92666252007 Collected: 05/04/23 10:45 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/09/23 16:12 79-00-505/09/23 09:0527.9 5
Trichloroethene ND ug/kg 05/09/23 16:12 79-01-605/09/23 09:0527.9 5
Trichlorofluoromethane ND ug/kg 05/09/23 16:12 75-69-405/09/23 09:0527.9 5
1,2,3-Trichloropropane ND ug/kg 05/09/23 16:12 96-18-405/09/23 09:0527.9 5
1,2,4-Trimethylbenzene 2440 ug/kg 05/09/23 16:12 95-63-605/09/23 09:0527.9 5
1,3,5-Trimethylbenzene 852 ug/kg 05/09/23 16:12 108-67-805/09/23 09:0527.9 5
Vinyl acetate ND ug/kg 05/09/23 16:12 108-05-405/09/23 09:05279 5
Vinyl chloride ND ug/kg 05/09/23 16:12 75-01-405/09/23 09:0555.8 5
Xylene (Total) ND ug/kg 05/09/23 16:12 1330-20-705/09/23 09:0555.8 5
m&p-Xylene ND ug/kg 05/09/23 16:12 179601-23-105/09/23 09:0555.8 5
o-Xylene ND ug/kg 05/09/23 16:12 95-47-605/09/23 09:0527.9 5
Surrogates
Toluene-d8 (S) 100 %05/09/23 16:12 2037-26-505/09/23 09:0570-130 5
4-Bromofluorobenzene (S) 98 %05/09/23 16:12 460-00-405/09/23 09:0570-130 5
1,2-Dichloroethane-d4 (S) 99 %05/09/23 16:12 17060-07-005/09/23 09:0570-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.2 %05/09/23 16:37 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 132 Lab ID: 92666252008 Collected: 05/04/23 14:00 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/11/23 11:53 83-32-905/10/23 15:09395 1
Acenaphthylene ND ug/kg 05/11/23 11:53 208-96-805/10/23 15:09395 1
Aniline ND ug/kg 05/11/23 11:53 62-53-305/10/23 15:09395 1
Anthracene ND ug/kg 05/11/23 11:53 120-12-705/10/23 15:09395 1
Benzo(a)anthracene ND ug/kg 05/11/23 11:53 56-55-305/10/23 15:09395 1
Benzo(a)pyrene ND ug/kg 05/11/23 11:53 50-32-805/10/23 15:09395 1
Benzo(b)fluoranthene ND ug/kg 05/11/23 11:53 205-99-205/10/23 15:09395 1
Benzo(g,h,i)perylene ND ug/kg 05/11/23 11:53 191-24-205/10/23 15:09395 1
Benzo(k)fluoranthene ND ug/kg 05/11/23 11:53 207-08-905/10/23 15:09395 1
Benzoic Acid ND ug/kg 05/11/23 11:53 65-85-005/10/23 15:091980 1
Benzyl alcohol ND ug/kg 05/11/23 11:53 100-51-605/10/23 15:09791 1
4-Bromophenylphenyl ether ND ug/kg 05/11/23 11:53 101-55-305/10/23 15:09395 1
Butylbenzylphthalate ND ug/kg 05/11/23 11:53 85-68-705/10/23 15:09395 1
4-Chloro-3-methylphenol ND ug/kg 05/11/23 11:53 59-50-705/10/23 15:09791 1
4-Chloroaniline ND ug/kg 05/11/23 11:53 106-47-805/10/23 15:09791 1
bis(2-Chloroethoxy)methane ND ug/kg 05/11/23 11:53 111-91-105/10/23 15:09395 1
bis(2-Chloroethyl) ether ND ug/kg 05/11/23 11:53 111-44-405/10/23 15:09395 1
2-Chloronaphthalene ND ug/kg 05/11/23 11:53 91-58-705/10/23 15:09395 1
2-Chlorophenol ND ug/kg 05/11/23 11:53 95-57-805/10/23 15:09395 1
4-Chlorophenylphenyl ether ND ug/kg 05/11/23 11:53 7005-72-305/10/23 15:09395 1
Chrysene ND ug/kg 05/11/23 11:53 218-01-905/10/23 15:09395 1
Dibenz(a,h)anthracene ND ug/kg 05/11/23 11:53 53-70-305/10/23 15:09395 1
Dibenzofuran ND ug/kg 05/11/23 11:53 132-64-905/10/23 15:09395 1
1,2-Dichlorobenzene ND ug/kg 05/11/23 11:53 95-50-105/10/23 15:09395 1
1,3-Dichlorobenzene ND ug/kg 05/11/23 11:53 541-73-105/10/23 15:09395 1
1,4-Dichlorobenzene ND ug/kg 05/11/23 11:53 106-46-705/10/23 15:09395 1
3,3'-Dichlorobenzidine ND ug/kg 05/11/23 11:53 91-94-105/10/23 15:09791 1
2,4-Dichlorophenol ND ug/kg 05/11/23 11:53 120-83-205/10/23 15:09395 1
Diethylphthalate ND ug/kg 05/11/23 11:53 84-66-205/10/23 15:09395 1
2,4-Dimethylphenol ND ug/kg 05/11/23 11:53 105-67-905/10/23 15:09395 1
Dimethylphthalate ND ug/kg 05/11/23 11:53 131-11-305/10/23 15:09395 1
Di-n-butylphthalate ND ug/kg 05/11/23 11:53 84-74-205/10/23 15:09395 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/11/23 11:53 534-52-105/10/23 15:09791 1
2,4-Dinitrophenol ND ug/kg 05/11/23 11:53 51-28-5 v105/10/23 15:091980 1
2,4-Dinitrotoluene ND ug/kg 05/11/23 11:53 121-14-205/10/23 15:09395 1
2,6-Dinitrotoluene ND ug/kg 05/11/23 11:53 606-20-205/10/23 15:09395 1
Di-n-octylphthalate ND ug/kg 05/11/23 11:53 117-84-005/10/23 15:09395 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/11/23 11:53 117-81-705/10/23 15:09395 1
Fluoranthene ND ug/kg 05/11/23 11:53 206-44-005/10/23 15:09395 1
Fluorene ND ug/kg 05/11/23 11:53 86-73-705/10/23 15:09395 1
Hexachloro-1,3-butadiene ND ug/kg 05/11/23 11:53 87-68-305/10/23 15:09395 1
Hexachlorobenzene ND ug/kg 05/11/23 11:53 118-74-105/10/23 15:09395 1
Hexachlorocyclopentadiene ND ug/kg 05/11/23 11:53 77-47-405/10/23 15:09395 1
Hexachloroethane ND ug/kg 05/11/23 11:53 67-72-105/10/23 15:09395 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/11/23 11:53 193-39-505/10/23 15:09395 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 132 Lab ID: 92666252008 Collected: 05/04/23 14:00 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/11/23 11:53 78-59-105/10/23 15:09395 1
1-Methylnaphthalene 1120 ug/kg 05/11/23 11:53 90-12-005/10/23 15:09395 1
2-Methylnaphthalene 1740 ug/kg 05/11/23 11:53 91-57-605/10/23 15:09395 1
2-Methylphenol(o-Cresol) ND ug/kg 05/11/23 11:53 95-48-705/10/23 15:09395 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/11/23 11:53 15831-10-405/10/23 15:09395 1
Naphthalene 559 ug/kg 05/11/23 11:53 91-20-305/10/23 15:09395 1
2-Nitroaniline ND ug/kg 05/11/23 11:53 88-74-405/10/23 15:091980 1
3-Nitroaniline ND ug/kg 05/11/23 11:53 99-09-205/10/23 15:091980 1
4-Nitroaniline ND ug/kg 05/11/23 11:53 100-01-605/10/23 15:09791 1
Nitrobenzene ND ug/kg 05/11/23 11:53 98-95-305/10/23 15:09395 1
2-Nitrophenol ND ug/kg 05/11/23 11:53 88-75-505/10/23 15:09395 1
4-Nitrophenol ND ug/kg 05/11/23 11:53 100-02-705/10/23 15:091980 1
N-Nitrosodimethylamine ND ug/kg 05/11/23 11:53 62-75-905/10/23 15:09395 1
N-Nitroso-di-n-propylamine ND ug/kg 05/11/23 11:53 621-64-705/10/23 15:09395 1
N-Nitrosodiphenylamine ND ug/kg 05/11/23 11:53 86-30-605/10/23 15:09395 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/11/23 11:53 108-60-105/10/23 15:09395 1
Pentachlorophenol ND ug/kg 05/11/23 11:53 87-86-505/10/23 15:09791 1
Phenanthrene 435 ug/kg 05/11/23 11:53 85-01-805/10/23 15:09395 1
Phenol ND ug/kg 05/11/23 11:53 108-95-205/10/23 15:09395 1
Pyrene ND ug/kg 05/11/23 11:53 129-00-005/10/23 15:09395 1
Pyridine ND ug/kg 05/11/23 11:53 110-86-105/10/23 15:09395 1
1,2,4-Trichlorobenzene ND ug/kg 05/11/23 11:53 120-82-105/10/23 15:09395 1
2,4,5-Trichlorophenol ND ug/kg 05/11/23 11:53 95-95-405/10/23 15:09395 1
2,4,6-Trichlorophenol ND ug/kg 05/11/23 11:53 88-06-205/10/23 15:09395 1
Surrogates
Nitrobenzene-d5 (S) 69 %05/11/23 11:53 4165-60-005/10/23 15:0910-130 1
2-Fluorobiphenyl (S) 59 %05/11/23 11:53 321-60-805/10/23 15:0910-130 1
Terphenyl-d14 (S) 66 %05/11/23 11:53 1718-51-005/10/23 15:0910-130 1
Phenol-d6 (S) 62 %05/11/23 11:53 13127-88-305/10/23 15:0910-130 1
2-Fluorophenol (S) 60 %05/11/23 11:53 367-12-405/10/23 15:0910-130 1
2,4,6-Tribromophenol (S) 73 %05/11/23 11:53 118-79-605/10/23 15:0910-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/08/23 22:23 67-64-105/08/23 02:50114 1
Benzene 201 ug/kg 05/08/23 22:23 71-43-205/08/23 02:505.7 1
Bromobenzene ND ug/kg 05/08/23 22:23 108-86-105/08/23 02:505.7 1
Bromochloromethane ND ug/kg 05/08/23 22:23 74-97-505/08/23 02:505.7 1
Bromodichloromethane ND ug/kg 05/08/23 22:23 75-27-405/08/23 02:505.7 1
Bromoform ND ug/kg 05/08/23 22:23 75-25-205/08/23 02:505.7 1
Bromomethane ND ug/kg 05/08/23 22:23 74-83-9 IK,v105/08/23 02:5022.7 1
2-Butanone (MEK) ND ug/kg 05/08/23 22:23 78-93-305/08/23 02:50114 1
n-Butylbenzene 673 ug/kg 05/08/23 22:23 104-51-805/08/23 02:505.7 1
sec-Butylbenzene ND ug/kg 05/08/23 22:23 135-98-805/08/23 02:505.7 1
tert-Butylbenzene ND ug/kg 05/08/23 22:23 98-06-605/08/23 02:505.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 132 Lab ID: 92666252008 Collected: 05/04/23 14:00 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/08/23 22:23 56-23-505/08/23 02:505.7 1
Chlorobenzene ND ug/kg 05/08/23 22:23 108-90-705/08/23 02:505.7 1
Chloroethane ND ug/kg 05/08/23 22:23 75-00-305/08/23 02:5011.4 1
Chloroform ND ug/kg 05/08/23 22:23 67-66-305/08/23 02:505.7 1
Chloromethane 13.4 ug/kg 05/08/23 22:23 74-87-305/08/23 02:5011.4 1
2-Chlorotoluene ND ug/kg 05/08/23 22:23 95-49-805/08/23 02:505.7 1
4-Chlorotoluene ND ug/kg 05/08/23 22:23 106-43-405/08/23 02:505.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/08/23 22:23 96-12-805/08/23 02:505.7 1
Dibromochloromethane ND ug/kg 05/08/23 22:23 124-48-105/08/23 02:505.7 1
1,2-Dibromoethane (EDB) ND ug/kg 05/08/23 22:23 106-93-405/08/23 02:505.7 1
Dibromomethane ND ug/kg 05/08/23 22:23 74-95-305/08/23 02:505.7 1
1,2-Dichlorobenzene ND ug/kg 05/08/23 22:23 95-50-105/08/23 02:505.7 1
1,3-Dichlorobenzene ND ug/kg 05/08/23 22:23 541-73-105/08/23 02:505.7 1
1,4-Dichlorobenzene ND ug/kg 05/08/23 22:23 106-46-705/08/23 02:505.7 1
Dichlorodifluoromethane ND ug/kg 05/08/23 22:23 75-71-8 L105/08/23 02:5011.4 1
1,1-Dichloroethane ND ug/kg 05/08/23 22:23 75-34-305/08/23 02:505.7 1
1,2-Dichloroethane ND ug/kg 05/08/23 22:23 107-06-205/08/23 02:505.7 1
1,1-Dichloroethene ND ug/kg 05/08/23 22:23 75-35-405/08/23 02:505.7 1
cis-1,2-Dichloroethene ND ug/kg 05/08/23 22:23 156-59-205/08/23 02:505.7 1
trans-1,2-Dichloroethene ND ug/kg 05/08/23 22:23 156-60-505/08/23 02:505.7 1
1,2-Dichloropropane ND ug/kg 05/08/23 22:23 78-87-505/08/23 02:505.7 1
1,3-Dichloropropane ND ug/kg 05/08/23 22:23 142-28-905/08/23 02:505.7 1
2,2-Dichloropropane ND ug/kg 05/08/23 22:23 594-20-705/08/23 02:505.7 1
1,1-Dichloropropene ND ug/kg 05/08/23 22:23 563-58-605/08/23 02:505.7 1
cis-1,3-Dichloropropene ND ug/kg 05/08/23 22:23 10061-01-505/08/23 02:505.7 1
trans-1,3-Dichloropropene ND ug/kg 05/08/23 22:23 10061-02-605/08/23 02:505.7 1
Diisopropyl ether ND ug/kg 05/08/23 22:23 108-20-305/08/23 02:505.7 1
Ethylbenzene 132 ug/kg 05/08/23 22:23 100-41-405/08/23 02:505.7 1
Hexachloro-1,3-butadiene ND ug/kg 05/08/23 22:23 87-68-305/08/23 02:5011.4 1
2-Hexanone ND ug/kg 05/08/23 22:23 591-78-605/08/23 02:5056.8 1
Isopropylbenzene (Cumene)239 ug/kg 05/08/23 22:23 98-82-805/08/23 02:505.7 1
p-Isopropyltoluene 554 ug/kg 05/08/23 22:23 99-87-605/08/23 02:505.7 1
Methylene Chloride ND ug/kg 05/08/23 22:23 75-09-205/08/23 02:5022.7 1
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/08/23 22:23 108-10-105/08/23 02:5056.8 1
Methyl-tert-butyl ether ND ug/kg 05/08/23 22:23 1634-04-405/08/23 02:505.7 1
Naphthalene 962 ug/kg 05/08/23 22:23 91-20-305/08/23 02:505.7 1
n-Propylbenzene 459 ug/kg 05/08/23 22:23 103-65-105/08/23 02:505.7 1
Styrene ND ug/kg 05/08/23 22:23 100-42-505/08/23 02:505.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/08/23 22:23 630-20-605/08/23 02:505.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/08/23 22:23 79-34-505/08/23 02:505.7 1
Tetrachloroethene ND ug/kg 05/08/23 22:23 127-18-405/08/23 02:505.7 1
Toluene ND ug/kg 05/08/23 22:23 108-88-305/08/23 02:505.7 1
1,2,3-Trichlorobenzene ND ug/kg 05/08/23 22:23 87-61-605/08/23 02:505.7 1
1,2,4-Trichlorobenzene ND ug/kg 05/08/23 22:23 120-82-105/08/23 02:505.7 1
1,1,1-Trichloroethane ND ug/kg 05/08/23 22:23 71-55-605/08/23 02:505.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666252
Loves 412 23004903
Sample: 53234903 - 132 Lab ID: 92666252008 Collected: 05/04/23 14:00 Received: 05/08/23 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/08/23 22:23 79-00-505/08/23 02:505.7 1
Trichloroethene ND ug/kg 05/08/23 22:23 79-01-605/08/23 02:505.7 1
Trichlorofluoromethane ND ug/kg 05/08/23 22:23 75-69-405/08/23 02:505.7 1
1,2,3-Trichloropropane ND ug/kg 05/08/23 22:23 96-18-405/08/23 02:505.7 1
1,2,4-Trimethylbenzene 1160 ug/kg 05/08/23 22:23 95-63-605/08/23 02:505.7 1
1,3,5-Trimethylbenzene 408 ug/kg 05/08/23 22:23 108-67-805/08/23 02:505.7 1
Vinyl acetate ND ug/kg 05/08/23 22:23 108-05-405/08/23 02:5056.8 1
Vinyl chloride ND ug/kg 05/08/23 22:23 75-01-405/08/23 02:5011.4 1
Xylene (Total)425 ug/kg 05/08/23 22:23 1330-20-705/08/23 02:5011.4 1
m&p-Xylene 140 ug/kg 05/08/23 22:23 179601-23-105/08/23 02:5011.4 1
o-Xylene 285 ug/kg 05/08/23 22:23 95-47-605/08/23 02:505.7 1
Surrogates
Toluene-d8 (S) 101 %05/08/23 22:23 2037-26-505/08/23 02:5070-130 1
4-Bromofluorobenzene (S) 104 %05/08/23 22:23 460-00-405/08/23 02:5070-130 1
1,2-Dichloroethane-d4 (S) 98 %05/08/23 22:23 17060-07-005/08/23 02:5070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.8 %05/09/23 16:37 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
773106
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92666252008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4012949
Associated Lab Samples:92666252008
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/08/23 16:51
1,1,1-Trichloroethane ug/kg ND 5.0 05/08/23 16:51
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/08/23 16:51
1,1,2-Trichloroethane ug/kg ND 5.0 05/08/23 16:51
1,1-Dichloroethane ug/kg ND 5.0 05/08/23 16:51
1,1-Dichloroethene ug/kg ND 5.0 05/08/23 16:51
1,1-Dichloropropene ug/kg ND 5.0 05/08/23 16:51
1,2,3-Trichlorobenzene ug/kg ND 5.0 05/08/23 16:51
1,2,3-Trichloropropane ug/kg ND 5.0 05/08/23 16:51
1,2,4-Trichlorobenzene ug/kg ND 5.0 05/08/23 16:51
1,2,4-Trimethylbenzene ug/kg ND 5.0 05/08/23 16:51
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 05/08/23 16:51
1,2-Dibromoethane (EDB) ug/kg ND 5.0 05/08/23 16:51
1,2-Dichlorobenzene ug/kg ND 5.0 05/08/23 16:51
1,2-Dichloroethane ug/kg ND 5.0 05/08/23 16:51
1,2-Dichloropropane ug/kg ND 5.0 05/08/23 16:51
1,3,5-Trimethylbenzene ug/kg ND 5.0 05/08/23 16:51
1,3-Dichlorobenzene ug/kg ND 5.0 05/08/23 16:51
1,3-Dichloropropane ug/kg ND 5.0 05/08/23 16:51
1,4-Dichlorobenzene ug/kg ND 5.0 05/08/23 16:51
2,2-Dichloropropane ug/kg ND 5.0 05/08/23 16:51
2-Butanone (MEK) ug/kg ND 100 05/08/23 16:51
2-Chlorotoluene ug/kg ND 5.0 05/08/23 16:51
2-Hexanone ug/kg ND 50.0 05/08/23 16:51
4-Chlorotoluene ug/kg ND 5.0 05/08/23 16:51
4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 05/08/23 16:51
Acetone ug/kg ND 100 05/08/23 16:51
Benzene ug/kg ND 5.0 05/08/23 16:51
Bromobenzene ug/kg ND 5.0 05/08/23 16:51
Bromochloromethane ug/kg ND 5.0 05/08/23 16:51
Bromodichloromethane ug/kg ND 5.0 05/08/23 16:51
Bromoform ug/kg ND 5.0 05/08/23 16:51
Bromomethane ug/kg ND 20.0 IK,v105/08/23 16:51
Carbon tetrachloride ug/kg ND 5.0 05/08/23 16:51
Chlorobenzene ug/kg ND 5.0 05/08/23 16:51
Chloroethane ug/kg ND 10.0 05/08/23 16:51
Chloroform ug/kg ND 5.0 05/08/23 16:51
Chloromethane ug/kg ND 10.0 05/08/23 16:51
cis-1,2-Dichloroethene ug/kg ND 5.0 05/08/23 16:51
cis-1,3-Dichloropropene ug/kg ND 5.0 05/08/23 16:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4012949
Associated Lab Samples:92666252008
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 05/08/23 16:51
Dibromomethane ug/kg ND 5.0 05/08/23 16:51
Dichlorodifluoromethane ug/kg ND 10.0 05/08/23 16:51
Diisopropyl ether ug/kg ND 5.0 05/08/23 16:51
Ethylbenzene ug/kg ND 5.0 05/08/23 16:51
Hexachloro-1,3-butadiene ug/kg ND 10.0 05/08/23 16:51
Isopropylbenzene (Cumene) ug/kg ND 5.0 05/08/23 16:51
m&p-Xylene ug/kg ND 10.0 05/08/23 16:51
Methyl-tert-butyl ether ug/kg ND 5.0 05/08/23 16:51
Methylene Chloride ug/kg ND 20.0 05/08/23 16:51
n-Butylbenzene ug/kg ND 5.0 05/08/23 16:51
n-Propylbenzene ug/kg ND 5.0 05/08/23 16:51
Naphthalene ug/kg ND 5.0 05/08/23 16:51
o-Xylene ug/kg ND 5.0 05/08/23 16:51
p-Isopropyltoluene ug/kg ND 5.0 05/08/23 16:51
sec-Butylbenzene ug/kg ND 5.0 05/08/23 16:51
Styrene ug/kg ND 5.0 05/08/23 16:51
tert-Butylbenzene ug/kg ND 5.0 05/08/23 16:51
Tetrachloroethene ug/kg ND 5.0 05/08/23 16:51
Toluene ug/kg ND 5.0 05/08/23 16:51
trans-1,2-Dichloroethene ug/kg ND 5.0 05/08/23 16:51
trans-1,3-Dichloropropene ug/kg ND 5.0 05/08/23 16:51
Trichloroethene ug/kg ND 5.0 05/08/23 16:51
Trichlorofluoromethane ug/kg ND 5.0 05/08/23 16:51
Vinyl acetate ug/kg ND 50.0 05/08/23 16:51
Vinyl chloride ug/kg ND 10.0 05/08/23 16:51
Xylene (Total) ug/kg ND 10.0 05/08/23 16:51
1,2-Dichloroethane-d4 (S) % 102 70-130 05/08/23 16:51
4-Bromofluorobenzene (S) % 92 70-130 05/08/23 16:51
Toluene-d8 (S) % 100 70-130 05/08/23 16:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4012950LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 473500 95 70-130
1,1,1-Trichloroethane ug/kg 464500 93 70-130
1,1,2,2-Tetrachloroethane ug/kg 502500 100 70-130
1,1,2-Trichloroethane ug/kg 443500 89 70-130
1,1-Dichloroethane ug/kg 494500 99 70-130
1,1-Dichloroethene ug/kg 510500 102 70-130
1,1-Dichloropropene ug/kg 502500 100 70-130
1,2,3-Trichlorobenzene ug/kg 474500 95 70-130
1,2,3-Trichloropropane ug/kg 479500 96 70-130
1,2,4-Trichlorobenzene ug/kg 493500 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4012950LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 509500 102 70-130
1,2-Dibromo-3-chloropropane ug/kg 473500 95 67-130
1,2-Dibromoethane (EDB) ug/kg 489500 98 70-130
1,2-Dichlorobenzene ug/kg 467500 93 70-130
1,2-Dichloroethane ug/kg 483500 97 70-130
1,2-Dichloropropane ug/kg 475500 95 70-130
1,3,5-Trimethylbenzene ug/kg 484500 97 70-130
1,3-Dichlorobenzene ug/kg 506500 101 70-130
1,3-Dichloropropane ug/kg 485500 97 70-130
1,4-Dichlorobenzene ug/kg 490500 98 70-130
2,2-Dichloropropane ug/kg 500500 100 67-130
2-Butanone (MEK) ug/kg 9991000 100 66-130
2-Chlorotoluene ug/kg 496500 99 70-130
2-Hexanone ug/kg 10501000 105 70-130
4-Chlorotoluene ug/kg 491500 98 70-130
4-Methyl-2-pentanone (MIBK) ug/kg 9461000 95 70-130
Acetone ug/kg 9631000 96 67-130
Benzene ug/kg 467500 93 70-130
Bromobenzene ug/kg 501500 100 70-130
Bromochloromethane ug/kg 533500 107 70-130
Bromodichloromethane ug/kg 443500 89 70-130
Bromoform ug/kg 478500 96 70-130
Bromomethane ug/kg 666 IK,v1500 133 53-175
Carbon tetrachloride ug/kg 465500 93 70-130
Chlorobenzene ug/kg 499500 100 70-130
Chloroethane ug/kg 516500 103 70-135
Chloroform ug/kg 465500 93 70-130
Chloromethane ug/kg 565500 113 64-130
cis-1,2-Dichloroethene ug/kg 510500 102 70-130
cis-1,3-Dichloropropene ug/kg 494500 99 70-130
Dibromochloromethane ug/kg 476500 95 70-130
Dibromomethane ug/kg 498500 100 70-130
Dichlorodifluoromethane ug/kg 780 L1500 156 63-145
Diisopropyl ether ug/kg 464500 93 68-130
Ethylbenzene ug/kg 457500 91 70-130
Hexachloro-1,3-butadiene ug/kg 509500 102 70-130
Isopropylbenzene (Cumene) ug/kg 482500 96 70-130
m&p-Xylene ug/kg 9281000 93 70-130
Methyl-tert-butyl ether ug/kg 446500 89 70-130
Methylene Chloride ug/kg 456500 91 67-130
n-Butylbenzene ug/kg 497500 99 70-130
n-Propylbenzene ug/kg 494500 99 70-130
Naphthalene ug/kg 486500 97 70-130
o-Xylene ug/kg 469500 94 70-130
p-Isopropyltoluene ug/kg 507500 101 70-130
sec-Butylbenzene ug/kg 485500 97 70-130
Styrene ug/kg 476500 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4012950LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 613500 123 64-130
Tetrachloroethene ug/kg 519500 104 70-130
Toluene ug/kg 464500 93 70-130
trans-1,2-Dichloroethene ug/kg 495500 99 70-130
trans-1,3-Dichloropropene ug/kg 463500 93 70-130
Trichloroethene ug/kg 478500 96 70-130
Trichlorofluoromethane ug/kg 560500 112 70-130
Vinyl acetate ug/kg 10301000 103 70-134
Vinyl chloride ug/kg 469500 94 68-130
Xylene (Total) ug/kg 14001500 93 70-130
1,2-Dichloroethane-d4 (S) %99 70-130
4-Bromofluorobenzene (S) %94 70-130
Toluene-d8 (S) %99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4012952MATRIX SPIKE SAMPLE:
MSSpike
Result
92665969003
1,1,1,2-Tetrachloroethane ug/kg 938947 99 58-140ND
1,1,1-Trichloroethane ug/kg 976947 103 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 975947 103 52-139ND
1,1,2-Trichloroethane ug/kg 915947 97 56-140ND
1,1-Dichloroethane ug/kg 1010947 106 58-145ND
1,1-Dichloroethene ug/kg 1010947 107 57-158ND
1,1-Dichloropropene ug/kg 968947 102 58-151ND
1,2,3-Trichlorobenzene ug/kg 863947 91 48-149ND
1,2,3-Trichloropropane ug/kg 930947 98 54-132ND
1,2,4-Trichlorobenzene ug/kg 888947 94 51-151ND
1,2,4-Trimethylbenzene ug/kg 900947 94 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 861947 91 44-134ND
1,2-Dibromoethane (EDB) ug/kg 976947 103 60-138ND
1,2-Dichlorobenzene ug/kg 875947 92 59-147ND
1,2-Dichloroethane ug/kg 982947 104 57-139ND
1,2-Dichloropropane ug/kg 1010947 107 62-145ND
1,3,5-Trimethylbenzene ug/kg 886947 94 47-159ND
1,3-Dichlorobenzene ug/kg 892947 94 58-144ND
1,3-Dichloropropane ug/kg 968947 102 60-142ND
1,4-Dichlorobenzene ug/kg 897947 95 57-143ND
2,2-Dichloropropane ug/kg 1030947 108 37-144ND
2-Butanone (MEK) ug/kg 18901890 100 28-146ND
2-Chlorotoluene ug/kg 915947 97 55-158ND
2-Hexanone ug/kg 19401890 102 44-141ND
4-Chlorotoluene ug/kg 881947 93 55-146ND
4-Methyl-2-pentanone (MIBK) ug/kg 19001890 100 50-138ND
Acetone ug/kg 17601890 91 20-136ND
Benzene ug/kg 971947 103 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4012952MATRIX SPIKE SAMPLE:
MSSpike
Result
92665969003
Bromobenzene ug/kg 983947 104 59-145ND
Bromochloromethane ug/kg 1080947 114 57-143ND
Bromodichloromethane ug/kg 884947 93 53-133ND
Bromoform ug/kg 933947 98 48-133ND
Bromomethane ug/kg 252 IK,v1947 27 10-167ND
Carbon tetrachloride ug/kg 721947 76 57-147ND
Chlorobenzene ug/kg 974947 103 61-144ND
Chloroethane ug/kg 232947 25 10-153ND
Chloroform ug/kg 957947 101 58-141ND
Chloromethane ug/kg 1360947 144 54-165ND
cis-1,2-Dichloroethene ug/kg 1060947 112 59-144ND
cis-1,3-Dichloropropene ug/kg 977947 103 56-137ND
Dibromochloromethane ug/kg 921947 97 53-139ND
Dibromomethane ug/kg 1010947 106 60-136ND
Dichlorodifluoromethane ug/kg 1480947 156 49-177ND
Diisopropyl ether ug/kg 979947 103 53-136ND
Ethylbenzene ug/kg 857947 90 53-150ND
Hexachloro-1,3-butadiene ug/kg 1110947 118 42-186ND
Isopropylbenzene (Cumene) ug/kg 911947 96 62-154ND
m&p-Xylene ug/kg 17401890 91 49-156ND
Methyl-tert-butyl ether ug/kg 899947 95 54-133ND
Methylene Chloride ug/kg 959947 101 50-153ND
n-Butylbenzene ug/kg 878947 93 44-174ND
n-Propylbenzene ug/kg 870947 92 52-157ND
Naphthalene ug/kg 947947 92 37-15071.7
o-Xylene ug/kg 914947 96 54-150ND
p-Isopropyltoluene ug/kg 918947 97 50-164ND
sec-Butylbenzene ug/kg 903947 95 58-161ND
Styrene ug/kg 882947 93 60-148ND
tert-Butylbenzene ug/kg 892947 94 44-151ND
Tetrachloroethene ug/kg 863947 91 53-151ND
Toluene ug/kg 934947 98 52-1489.6
trans-1,2-Dichloroethene ug/kg 959947 101 60-148ND
trans-1,3-Dichloropropene ug/kg 928947 98 55-133ND
Trichloroethene ug/kg 929947 98 60-148ND
Trichlorofluoromethane ug/kg 206947 22 10-154ND
Vinyl acetate ug/kg 19801890 105 50-149ND
Vinyl chloride ug/kg 937947 99 57-157ND
Xylene (Total) ug/kg 26502840 93 52-153ND
1,2-Dichloroethane-d4 (S) %103 70-130
4-Bromofluorobenzene (S) %95 70-130
Toluene-d8 (S) %100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92665969002
4012951SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg 23.3 123.0
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB) ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg 9.3 1410.7
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK) ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK) ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg 8.0 48.3
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IK,v1ND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 13.3 113.1
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene) ug/kg 7.1J8.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92665969002
4012951SAMPLE DUPLICATE:
m&p-Xylene ug/kg 30.0 029.9
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg 6.3J8.0
Naphthalene ug/kg 146 6155
o-Xylene ug/kg 14.7 315.1
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg 112 1113
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg 6.1JND
Toluene ug/kg 20.1 621.4
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total) ug/kg 44.6 145.0
1,2-Dichloroethane-d4 (S) %9999
4-Bromofluorobenzene (S) %9393
Toluene-d8 (S) %101101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
773232
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92666252001, 92666252002, 92666252003, 92666252004, 92666252005, 92666252006, 92666252007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4013311
Associated Lab Samples:92666252001, 92666252002, 92666252003, 92666252004, 92666252005, 92666252006, 92666252007
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/09/23 11:54
1,1,1-Trichloroethane ug/kg ND 5.0 05/09/23 11:54
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/09/23 11:54
1,1,2-Trichloroethane ug/kg ND 5.0 05/09/23 11:54
1,1-Dichloroethane ug/kg ND 5.0 05/09/23 11:54
1,1-Dichloroethene ug/kg ND 5.0 05/09/23 11:54
1,1-Dichloropropene ug/kg ND 5.0 05/09/23 11:54
1,2,3-Trichlorobenzene ug/kg ND 5.0 05/09/23 11:54
1,2,3-Trichloropropane ug/kg ND 5.0 05/09/23 11:54
1,2,4-Trichlorobenzene ug/kg ND 5.0 05/09/23 11:54
1,2,4-Trimethylbenzene ug/kg ND 5.0 05/09/23 11:54
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 05/09/23 11:54
1,2-Dibromoethane (EDB) ug/kg ND 5.0 05/09/23 11:54
1,2-Dichlorobenzene ug/kg ND 5.0 05/09/23 11:54
1,2-Dichloroethane ug/kg ND 5.0 05/09/23 11:54
1,2-Dichloropropane ug/kg ND 5.0 05/09/23 11:54
1,3,5-Trimethylbenzene ug/kg ND 5.0 05/09/23 11:54
1,3-Dichlorobenzene ug/kg ND 5.0 05/09/23 11:54
1,3-Dichloropropane ug/kg ND 5.0 05/09/23 11:54
1,4-Dichlorobenzene ug/kg ND 5.0 05/09/23 11:54
2,2-Dichloropropane ug/kg ND 5.0 05/09/23 11:54
2-Butanone (MEK) ug/kg ND 100 05/09/23 11:54
2-Chlorotoluene ug/kg ND 5.0 05/09/23 11:54
2-Hexanone ug/kg ND 50.0 05/09/23 11:54
4-Chlorotoluene ug/kg ND 5.0 05/09/23 11:54
4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 05/09/23 11:54
Acetone ug/kg ND 100 05/09/23 11:54
Benzene ug/kg ND 5.0 05/09/23 11:54
Bromobenzene ug/kg ND 5.0 05/09/23 11:54
Bromochloromethane ug/kg ND 5.0 05/09/23 11:54
Bromodichloromethane ug/kg ND 5.0 05/09/23 11:54
Bromoform ug/kg ND 5.0 05/09/23 11:54
Bromomethane ug/kg ND 20.0 IK,v105/09/23 11:54
Carbon tetrachloride ug/kg ND 5.0 05/09/23 11:54
Chlorobenzene ug/kg ND 5.0 05/09/23 11:54
Chloroethane ug/kg ND 10.0 05/09/23 11:54
Chloroform ug/kg ND 5.0 05/09/23 11:54
Chloromethane ug/kg ND 10.0 05/09/23 11:54
cis-1,2-Dichloroethene ug/kg ND 5.0 05/09/23 11:54
cis-1,3-Dichloropropene ug/kg ND 5.0 05/09/23 11:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4013311
Associated Lab Samples:92666252001, 92666252002, 92666252003, 92666252004, 92666252005, 92666252006, 92666252007
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 05/09/23 11:54
Dibromomethane ug/kg ND 5.0 05/09/23 11:54
Dichlorodifluoromethane ug/kg ND 10.0 05/09/23 11:54
Diisopropyl ether ug/kg ND 5.0 05/09/23 11:54
Ethylbenzene ug/kg ND 5.0 05/09/23 11:54
Hexachloro-1,3-butadiene ug/kg ND 10.0 05/09/23 11:54
Isopropylbenzene (Cumene) ug/kg ND 5.0 05/09/23 11:54
m&p-Xylene ug/kg ND 10.0 05/09/23 11:54
Methyl-tert-butyl ether ug/kg ND 5.0 05/09/23 11:54
Methylene Chloride ug/kg ND 20.0 05/09/23 11:54
n-Butylbenzene ug/kg ND 5.0 05/09/23 11:54
n-Propylbenzene ug/kg ND 5.0 05/09/23 11:54
Naphthalene ug/kg ND 5.0 05/09/23 11:54
o-Xylene ug/kg ND 5.0 05/09/23 11:54
p-Isopropyltoluene ug/kg ND 5.0 05/09/23 11:54
sec-Butylbenzene ug/kg ND 5.0 05/09/23 11:54
Styrene ug/kg ND 5.0 05/09/23 11:54
tert-Butylbenzene ug/kg ND 5.0 05/09/23 11:54
Tetrachloroethene ug/kg ND 5.0 05/09/23 11:54
Toluene ug/kg ND 5.0 05/09/23 11:54
trans-1,2-Dichloroethene ug/kg ND 5.0 05/09/23 11:54
trans-1,3-Dichloropropene ug/kg ND 5.0 05/09/23 11:54
Trichloroethene ug/kg ND 5.0 05/09/23 11:54
Trichlorofluoromethane ug/kg ND 5.0 05/09/23 11:54
Vinyl acetate ug/kg ND 50.0 05/09/23 11:54
Vinyl chloride ug/kg ND 10.0 05/09/23 11:54
Xylene (Total) ug/kg ND 10.0 05/09/23 11:54
1,2-Dichloroethane-d4 (S) % 100 70-130 05/09/23 11:54
4-Bromofluorobenzene (S) % 93 70-130 05/09/23 11:54
Toluene-d8 (S) % 101 70-130 05/09/23 11:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4013312LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 478500 96 70-130
1,1,1-Trichloroethane ug/kg 446500 89 70-130
1,1,2,2-Tetrachloroethane ug/kg 493500 99 70-130
1,1,2-Trichloroethane ug/kg 436500 87 70-130
1,1-Dichloroethane ug/kg 483500 97 70-130
1,1-Dichloroethene ug/kg 491500 98 70-130
1,1-Dichloropropene ug/kg 492500 98 70-130
1,2,3-Trichlorobenzene ug/kg 464500 93 70-130
1,2,3-Trichloropropane ug/kg 467500 93 70-130
1,2,4-Trichlorobenzene ug/kg 485500 97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4013312LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 495500 99 70-130
1,2-Dibromo-3-chloropropane ug/kg 426500 85 67-130
1,2-Dibromoethane (EDB) ug/kg 478500 96 70-130
1,2-Dichlorobenzene ug/kg 456500 91 70-130
1,2-Dichloroethane ug/kg 470500 94 70-130
1,2-Dichloropropane ug/kg 475500 95 70-130
1,3,5-Trimethylbenzene ug/kg 474500 95 70-130
1,3-Dichlorobenzene ug/kg 481500 96 70-130
1,3-Dichloropropane ug/kg 478500 96 70-130
1,4-Dichlorobenzene ug/kg 495500 99 70-130
2,2-Dichloropropane ug/kg 493500 99 67-130
2-Butanone (MEK) ug/kg 9221000 92 66-130
2-Chlorotoluene ug/kg 487500 97 70-130
2-Hexanone ug/kg 10101000 101 70-130
4-Chlorotoluene ug/kg 479500 96 70-130
4-Methyl-2-pentanone (MIBK) ug/kg 8991000 90 70-130
Acetone ug/kg 8601000 86 67-130
Benzene ug/kg 454500 91 70-130
Bromobenzene ug/kg 482500 96 70-130
Bromochloromethane ug/kg 516500 103 70-130
Bromodichloromethane ug/kg 436500 87 70-130
Bromoform ug/kg 472500 94 70-130
Bromomethane ug/kg 667 IK,v1500 133 53-175
Carbon tetrachloride ug/kg 464500 93 70-130
Chlorobenzene ug/kg 496500 99 70-130
Chloroethane ug/kg 493500 99 70-135
Chloroform ug/kg 453500 91 70-130
Chloromethane ug/kg 565500 113 64-130
cis-1,2-Dichloroethene ug/kg 493500 99 70-130
cis-1,3-Dichloropropene ug/kg 474500 95 70-130
Dibromochloromethane ug/kg 474500 95 70-130
Dibromomethane ug/kg 477500 95 70-130
Dichlorodifluoromethane ug/kg 752 L1500 150 63-145
Diisopropyl ether ug/kg 461500 92 68-130
Ethylbenzene ug/kg 452500 90 70-130
Hexachloro-1,3-butadiene ug/kg 484500 97 70-130
Isopropylbenzene (Cumene) ug/kg 484500 97 70-130
m&p-Xylene ug/kg 9311000 93 70-130
Methyl-tert-butyl ether ug/kg 430500 86 70-130
Methylene Chloride ug/kg 433500 87 67-130
n-Butylbenzene ug/kg 493500 99 70-130
n-Propylbenzene ug/kg 483500 97 70-130
Naphthalene ug/kg 456500 91 70-130
o-Xylene ug/kg 471500 94 70-130
p-Isopropyltoluene ug/kg 503500 101 70-130
sec-Butylbenzene ug/kg 480500 96 70-130
Styrene ug/kg 467500 93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4013312LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 607500 121 64-130
Tetrachloroethene ug/kg 510500 102 70-130
Toluene ug/kg 454500 91 70-130
trans-1,2-Dichloroethene ug/kg 490500 98 70-130
trans-1,3-Dichloropropene ug/kg 452500 90 70-130
Trichloroethene ug/kg 467500 93 70-130
Trichlorofluoromethane ug/kg 540500 108 70-130
Vinyl acetate ug/kg 9781000 98 70-134
Vinyl chloride ug/kg 456500 91 68-130
Xylene (Total) ug/kg 14001500 93 70-130
1,2-Dichloroethane-d4 (S) %98 70-130
4-Bromofluorobenzene (S) %96 70-130
Toluene-d8 (S) %99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4013313MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92666252004
4013314
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg M1,R161695 58-14049 64616ND585 301
1,1,1-Trichloroethane ug/kg M1,R161691 58-14450 58616ND560 308
1,1,2,2-Tetrachloroethane ug/kg R1616112 52-13957 66616ND692 348
1,1,2-Trichloroethane ug/kg M1,R161695 56-14049 64616ND583 300
1,1-Dichloroethane ug/kg M1,R161697 58-14553 59616ND596 326
1,1-Dichloroethene ug/kg M1,R161699 57-15855 57616ND610 338
1,1-Dichloropropene ug/kg M1,R161698 58-15154 57616ND602 334
1,2,3-Trichlorobenzene ug/kg R1616100 48-14954 61616ND616 330
1,2,3-Trichloropropane ug/kg M1,R1616100 54-13249 70616ND618 299
1,2,4-Trichlorobenzene ug/kg R1616102 51-15156 58616ND628 345
1,2,4-Trimethylbenzene ug/kg R161696 38-17050 36616339928 645
1,2-Dibromo-3-chloropropane ug/kg M1,R161699 44-13443 78616ND611 268
1,2-Dibromoethane (EDB) ug/kg M1,R1616101 60-13850 68616ND622 307
1,2-Dichlorobenzene ug/kg M1,R161693 59-14748 63616ND570 298
1,2-Dichloroethane ug/kg M1,R161698 57-13952 62616ND606 318
1,2-Dichloropropane ug/kg M1,R161698 62-14551 63616ND605 315
1,3,5-Trimethylbenzene ug/kg R161696 47-15952 5261658.5 647 381
1,3-Dichlorobenzene ug/kg M1,R161696 58-14452 59616ND590 322
1,3-Dichloropropane ug/kg M1,R1616100 60-14250 66616ND615 308
1,4-Dichlorobenzene ug/kg M1,R161697 57-14349 65616ND597 303
2,2-Dichloropropane ug/kg R161699 37-14454 59616ND609 330
2-Butanone (MEK) ug/kg R11230107 28-14647 781230ND1320 581
2-Chlorotoluene ug/kg M1,R161698 55-15852 62616ND602 319
2-Hexanone ug/kg R11230112 44-14149 791230ND1380 600
4-Chlorotoluene ug/kg M1,R161694 55-14649 63616ND580 303
4-Methyl-2-pentanone (MIBK) ug/kg M1,R11230106 50-13849 741230ND1300 601
Acetone ug/kg R1123098 20-13646 721230ND1210 568
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4013313MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92666252004
4013314
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Benzene ug/kg M1,R161693 60-14550 596167.0 580 315
Bromobenzene ug/kg M1,R161694 59-14552 57616ND576 321
Bromochloromethane ug/kg M1,R1616105 57-14355 62616ND647 340
Bromodichloromethane ug/kg M1,R161690 53-13346 65616ND552 282
Bromoform ug/kg M1,R161696 48-13347 70616ND594 287
Bromomethane ug/kg IK,R1,v161622 10-16714 48616ND137 84.1
Carbon tetrachloride ug/kg M1,R161677 57-14742 58616ND472 260
Chlorobenzene ug/kg M1,R161697 61-14452 61616ND599 320
Chloroethane ug/kg R161620 10-15313 45616ND125 78.4
Chloroform ug/kg M1,R161693 58-14150 60616ND570 307
Chloromethane ug/kg R1616126 54-16573 53616ND778 454
cis-1,2-Dichloroethene ug/kg M1,R1616102 59-14455 60616ND628 339
cis-1,3-Dichloropropene ug/kg M1,R161698 56-13752 62616ND605 318
Dibromochloromethane ug/kg M1,R161695 53-13947 67616ND583 291
Dibromomethane ug/kg M1,R1616103 60-13651 67616ND634 317
Dichlorodifluoromethane ug/kg R1616148 49-17780 60616ND913 493
Diisopropyl ether ug/kg M1,R161698 53-13650 65616ND601 307
Ethylbenzene ug/kg M1,R161687 53-15047 59616ND541 295
Hexachloro-1,3-butadiene ug/kg R1616152 42-18686 56616ND938 528
Isopropylbenzene (Cumene) ug/kg M1,R161696 62-15452 5561633.3 624 355
m&p-Xylene ug/kg M1,R1123090 49-15648 601230ND1110 594
Methyl-tert-butyl ether ug/kg M1,R161691 54-13345 67616ND562 279
Methylene Chloride ug/kg M1,R161692 50-15345 68616ND565 278
n-Butylbenzene ug/kg R1616110 44-17462 4861687.1 767 472
n-Propylbenzene ug/kg R161696 52-15752 5361657.7 650 377
Naphthalene ug/kg R1616100 37-15050 5561693.3 708 402
o-Xylene ug/kg M1,R161692 54-15050 60616ND570 306
p-Isopropyltoluene ug/kg R1616103 50-16457 42616193829 542
sec-Butylbenzene ug/kg M1,R1616102 58-16156 4961693.1 721 435
Styrene ug/kg M1,R161691 60-14848 62616ND561 294
tert-Butylbenzene ug/kg R161698 44-15153 61616ND605 323
Tetrachloroethene ug/kg R161692 53-15153 54616ND569 326
Toluene ug/kg M1,R161693 52-14850 59616ND570 309
trans-1,2-Dichloroethene ug/kg M1,R161697 60-14854 57616ND600 334
trans-1,3-Dichloropropene ug/kg M1,R161698 55-13348 69616ND602 293
Trichloroethene ug/kg M1,R161692 60-14850 59616ND568 310
Trichlorofluoromethane ug/kg R161621 10-15412 54616ND128 73.1
Vinyl acetate ug/kg R11230103 50-14952 661230ND1260 639
Vinyl chloride ug/kg M1,R161690 57-15751 55616ND552 315
Xylene (Total) ug/kg MS,RS185091 52-15349 601850ND1680 901
1,2-Dichloroethane-d4 (S) %100 70-130101
4-Bromofluorobenzene (S) %99 70-13099
Toluene-d8 (S) %100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
773599
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples:92666252001, 92666252002, 92666252003, 92666252004, 92666252005, 92666252006, 92666252007,
92666252008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4015343
Associated Lab Samples: 92666252001, 92666252002, 92666252003, 92666252004, 92666252005, 92666252006, 92666252007,
92666252008
Matrix: Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 331 05/11/23 06:21
1,2-Dichlorobenzene ug/kg ND 331 05/11/23 06:21
1,3-Dichlorobenzene ug/kg ND 331 05/11/23 06:21
1,4-Dichlorobenzene ug/kg ND 331 05/11/23 06:21
1-Methylnaphthalene ug/kg ND 331 05/11/23 06:21
2,2'-Oxybis(1-chloropropane) ug/kg ND 331 05/11/23 06:21
2,4,5-Trichlorophenol ug/kg ND 331 05/11/23 06:21
2,4,6-Trichlorophenol ug/kg ND 331 05/11/23 06:21
2,4-Dichlorophenol ug/kg ND 331 05/11/23 06:21
2,4-Dimethylphenol ug/kg ND 331 05/11/23 06:21
2,4-Dinitrophenol ug/kg ND 1660 v105/11/23 06:21
2,4-Dinitrotoluene ug/kg ND 331 05/11/23 06:21
2,6-Dinitrotoluene ug/kg ND 331 05/11/23 06:21
2-Chloronaphthalene ug/kg ND 331 05/11/23 06:21
2-Chlorophenol ug/kg ND 331 05/11/23 06:21
2-Methylnaphthalene ug/kg ND 331 05/11/23 06:21
2-Methylphenol(o-Cresol) ug/kg ND 331 05/11/23 06:21
2-Nitroaniline ug/kg ND 1660 05/11/23 06:21
2-Nitrophenol ug/kg ND 331 05/11/23 06:21
3&4-Methylphenol(m&p Cresol) ug/kg ND 331 05/11/23 06:21
3,3'-Dichlorobenzidine ug/kg ND 662 05/11/23 06:21
3-Nitroaniline ug/kg ND 1660 05/11/23 06:21
4,6-Dinitro-2-methylphenol ug/kg ND 662 05/11/23 06:21
4-Bromophenylphenyl ether ug/kg ND 331 05/11/23 06:21
4-Chloro-3-methylphenol ug/kg ND 662 05/11/23 06:21
4-Chloroaniline ug/kg ND 662 05/11/23 06:21
4-Chlorophenylphenyl ether ug/kg ND 331 05/11/23 06:21
4-Nitroaniline ug/kg ND 662 05/11/23 06:21
4-Nitrophenol ug/kg ND 1660 05/11/23 06:21
Acenaphthene ug/kg ND 331 05/11/23 06:21
Acenaphthylene ug/kg ND 331 05/11/23 06:21
Aniline ug/kg ND 331 05/11/23 06:21
Anthracene ug/kg ND 331 05/11/23 06:21
Benzo(a)anthracene ug/kg ND 331 05/11/23 06:21
Benzo(a)pyrene ug/kg ND 331 05/11/23 06:21
Benzo(b)fluoranthene ug/kg ND 331 05/11/23 06:21
Benzo(g,h,i)perylene ug/kg ND 331 05/11/23 06:21
Benzo(k)fluoranthene ug/kg ND 331 05/11/23 06:21
Benzoic Acid ug/kg ND 1660 05/11/23 06:21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4015343
Associated Lab Samples: 92666252001, 92666252002, 92666252003, 92666252004, 92666252005, 92666252006, 92666252007,
92666252008
Matrix: Solid
Analyzed
Benzyl alcohol ug/kg ND 662 05/11/23 06:21
bis(2-Chloroethoxy)methane ug/kg ND 331 05/11/23 06:21
bis(2-Chloroethyl) ether ug/kg ND 331 05/11/23 06:21
bis(2-Ethylhexyl)phthalate ug/kg ND 331 05/11/23 06:21
Butylbenzylphthalate ug/kg 432 331 05/11/23 06:21
Chrysene ug/kg ND 331 05/11/23 06:21
Di-n-butylphthalate ug/kg ND 331 05/11/23 06:21
Di-n-octylphthalate ug/kg ND 331 05/11/23 06:21
Dibenz(a,h)anthracene ug/kg ND 331 05/11/23 06:21
Dibenzofuran ug/kg ND 331 05/11/23 06:21
Diethylphthalate ug/kg ND 331 05/11/23 06:21
Dimethylphthalate ug/kg ND 331 05/11/23 06:21
Fluoranthene ug/kg ND 331 05/11/23 06:21
Fluorene ug/kg ND 331 05/11/23 06:21
Hexachloro-1,3-butadiene ug/kg ND 331 05/11/23 06:21
Hexachlorobenzene ug/kg ND 331 05/11/23 06:21
Hexachlorocyclopentadiene ug/kg ND 331 05/11/23 06:21
Hexachloroethane ug/kg ND 331 05/11/23 06:21
Indeno(1,2,3-cd)pyrene ug/kg ND 331 05/11/23 06:21
Isophorone ug/kg ND 331 05/11/23 06:21
N-Nitroso-di-n-propylamine ug/kg ND 331 05/11/23 06:21
N-Nitrosodimethylamine ug/kg ND 331 05/11/23 06:21
N-Nitrosodiphenylamine ug/kg ND 331 05/11/23 06:21
Naphthalene ug/kg ND 331 05/11/23 06:21
Nitrobenzene ug/kg ND 331 05/11/23 06:21
Pentachlorophenol ug/kg ND 662 05/11/23 06:21
Phenanthrene ug/kg ND 331 05/11/23 06:21
Phenol ug/kg ND 331 05/11/23 06:21
Pyrene ug/kg ND 331 05/11/23 06:21
Pyridine ug/kg ND 331 05/11/23 06:21
2,4,6-Tribromophenol (S) % 64 10-131 05/11/23 06:21
2-Fluorobiphenyl (S) % 55 10-130 05/11/23 06:21
2-Fluorophenol (S) % 54 10-130 05/11/23 06:21
Nitrobenzene-d5 (S) % 58 10-130 05/11/23 06:21
Phenol-d6 (S) % 58 10-130 05/11/23 06:21
Terphenyl-d14 (S) % 61 10-130 05/11/23 06:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4015344LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11101670 67 43-130
1,2-Dichlorobenzene ug/kg 10501670 63 43-130
1,3-Dichlorobenzene ug/kg 10201670 61 43-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4015344LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/kg 10401670 62 44-130
1-Methylnaphthalene ug/kg 12101670 72 47-130
2,2'-Oxybis(1-chloropropane) ug/kg 9541670 57 29-130
2,4,5-Trichlorophenol ug/kg 12501670 75 47-130
2,4,6-Trichlorophenol ug/kg 12301670 74 47-130
2,4-Dichlorophenol ug/kg 12001670 72 45-130
2,4-Dimethylphenol ug/kg 17201670 103 45-130
2,4-Dinitrophenol ug/kg 7140 v18330 86 27-140
2,4-Dinitrotoluene ug/kg 13301670 80 46-130
2,6-Dinitrotoluene ug/kg 13301670 80 48-130
2-Chloronaphthalene ug/kg 10701670 64 46-130
2-Chlorophenol ug/kg 11001670 66 43-130
2-Methylnaphthalene ug/kg 11401670 68 47-130
2-Methylphenol(o-Cresol) ug/kg 11701670 70 42-130
2-Nitroaniline ug/kg 22403330 67 41-130
2-Nitrophenol ug/kg 12601670 76 48-130
3&4-Methylphenol(m&p Cresol) ug/kg 12001670 72 39-130
3,3'-Dichlorobenzidine ug/kg 22003330 66 41-130
3-Nitroaniline ug/kg 22503330 68 37-130
4,6-Dinitro-2-methylphenol ug/kg 29903330 90 38-141
4-Bromophenylphenyl ether ug/kg 12501670 75 47-130
4-Chloro-3-methylphenol ug/kg 25703330 77 44-130
4-Chloroaniline ug/kg 21703330 65 41-130
4-Chlorophenylphenyl ether ug/kg 12301670 74 45-130
4-Nitroaniline ug/kg 23603330 71 42-130
4-Nitrophenol ug/kg 67408330 81 39-131
Acenaphthene ug/kg 11601670 70 49-130
Acenaphthylene ug/kg 11601670 70 50-130
Aniline ug/kg 8961670 54 38-130
Anthracene ug/kg 11801670 71 49-130
Benzo(a)anthracene ug/kg 12301670 74 51-130
Benzo(a)pyrene ug/kg 12401670 74 51-130
Benzo(b)fluoranthene ug/kg 12801670 77 49-130
Benzo(g,h,i)perylene ug/kg 10901670 65 48-140
Benzo(k)fluoranthene ug/kg 12901670 78 51-130
Benzoic Acid ug/kg 40608330 49 22-130
Benzyl alcohol ug/kg 22003330 66 43-130
bis(2-Chloroethoxy)methane ug/kg 10401670 62 43-130
bis(2-Chloroethyl) ether ug/kg 9791670 59 42-130
bis(2-Ethylhexyl)phthalate ug/kg 12701670 76 43-130
Butylbenzylphthalate ug/kg 12701670 76 44-131
Chrysene ug/kg 12601670 76 51-130
Di-n-butylphthalate ug/kg 12901670 78 46-130
Di-n-octylphthalate ug/kg 12701670 76 45-130
Dibenz(a,h)anthracene ug/kg 11901670 71 48-130
Dibenzofuran ug/kg 11801670 71 10-130
Diethylphthalate ug/kg 12901670 77 48-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
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Page 50 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4015344LABORATORY CONTROL SAMPLE:
LCSSpike
Dimethylphthalate ug/kg 12701670 76 48-130
Fluoranthene ug/kg 13201670 79 48-130
Fluorene ug/kg 12501670 75 48-130
Hexachloro-1,3-butadiene ug/kg 11401670 69 39-130
Hexachlorobenzene ug/kg 13101670 79 47-130
Hexachlorocyclopentadiene ug/kg 10101670 61 17-130
Hexachloroethane ug/kg 10301670 62 40-130
Indeno(1,2,3-cd)pyrene ug/kg 9201670 55 50-130
Isophorone ug/kg 11801670 71 41-130
N-Nitroso-di-n-propylamine ug/kg 11601670 69 36-130
N-Nitrosodimethylamine ug/kg 9831670 59 34-130
N-Nitrosodiphenylamine ug/kg 12001670 72 48-130
Naphthalene ug/kg 11101670 66 46-130
Nitrobenzene ug/kg 10601670 64 39-130
Pentachlorophenol ug/kg 26203330 79 42-130
Phenanthrene ug/kg 12801670 77 50-130
Phenol ug/kg 12001670 72 42-130
Pyrene ug/kg 12401670 74 50-130
Pyridine ug/kg 8071670 48 26-130
2,4,6-Tribromophenol (S) %77 10-131
2-Fluorobiphenyl (S) %59 10-130
2-Fluorophenol (S) %57 10-130
Nitrobenzene-d5 (S) %60 10-130
Phenol-d6 (S) %60 10-130
Terphenyl-d14 (S) %69 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4015345MATRIX SPIKE SAMPLE:
MSSpike
Result
92665974004
1,2,4-Trichlorobenzene ug/kg 11001900 58 16-130ND
1,2-Dichlorobenzene ug/kg 10901900 57 19-130ND
1,3-Dichlorobenzene ug/kg 10601900 56 19-130ND
1,4-Dichlorobenzene ug/kg 10701900 56 20-130ND
1-Methylnaphthalene ug/kg 12201900 64 19-130ND
2,2'-Oxybis(1-chloropropane) ug/kg 9871900 52 10-130ND
2,4,5-Trichlorophenol ug/kg 12901900 68 19-130ND
2,4,6-Trichlorophenol ug/kg 12701900 67 18-130ND
2,4-Dichlorophenol ug/kg 12301900 65 16-130ND
2,4-Dimethylphenol ug/kg 17401900 91 10-130ND
2,4-Dinitrophenol ug/kg 7820 v19520 82 10-143ND
2,4-Dinitrotoluene ug/kg 13601900 71 19-130ND
2,6-Dinitrotoluene ug/kg 13901900 73 22-130ND
2-Chloronaphthalene ug/kg 11001900 58 18-130ND
2-Chlorophenol ug/kg 11201900 59 20-130ND
2-Methylnaphthalene ug/kg 11501900 61 18-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
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Page 51 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4015345MATRIX SPIKE SAMPLE:
MSSpike
Result
92665974004
2-Methylphenol(o-Cresol) ug/kg 11901900 62 13-130ND
2-Nitroaniline ug/kg 23503810 62 18-130ND
2-Nitrophenol ug/kg 12801900 67 19-130ND
3&4-Methylphenol(m&p Cresol) ug/kg 12301900 65 13-130ND
3,3'-Dichlorobenzidine ug/kg 23403810 62 10-130ND
3-Nitroaniline ug/kg 23503810 62 22-130ND
4,6-Dinitro-2-methylphenol ug/kg 31403810 83 10-144ND
4-Bromophenylphenyl ether ug/kg 12301900 65 18-130ND
4-Chloro-3-methylphenol ug/kg 26603810 70 16-130ND
4-Chloroaniline ug/kg 22303810 59 17-130ND
4-Chlorophenylphenyl ether ug/kg 12101900 64 17-130ND
4-Nitroaniline ug/kg 24503810 64 21-130ND
4-Nitrophenol ug/kg 67409520 71 13-131ND
Acenaphthene ug/kg 11901900 63 20-130ND
Acenaphthylene ug/kg 12001900 63 21-130ND
Aniline ug/kg 8791900 46 10-130ND
Anthracene ug/kg 12001900 63 19-130ND
Benzo(a)anthracene ug/kg 12001900 63 17-130ND
Benzo(a)pyrene ug/kg 12301900 65 14-130ND
Benzo(b)fluoranthene ug/kg 12601900 66 11-134ND
Benzo(g,h,i)perylene ug/kg 11001900 58 12-130ND
Benzo(k)fluoranthene ug/kg 13001900 68 15-130ND
Benzoic Acid ug/kg 46309520 49 10-130ND
Benzyl alcohol ug/kg 22703810 60 20-130ND
bis(2-Chloroethoxy)methane ug/kg 10701900 56 16-130ND
bis(2-Chloroethyl) ether ug/kg 10101900 53 18-130ND
bis(2-Ethylhexyl)phthalate ug/kg 12201900 64 11-130ND
Butylbenzylphthalate ug/kg 12101900 64 10-130ND
Chrysene ug/kg 12301900 65 17-130ND
Di-n-butylphthalate ug/kg 12301900 64 16-130ND
Di-n-octylphthalate ug/kg 11801900 62 16-130ND
Dibenz(a,h)anthracene ug/kg 11501900 60 13-130ND
Dibenzofuran ug/kg 11901900 63 19-130ND
Diethylphthalate ug/kg 13201900 69 22-130ND
Dimethylphthalate ug/kg 13201900 69 23-130ND
Fluoranthene ug/kg 12901900 68 14-130ND
Fluorene ug/kg 12501900 66 19-130ND
Hexachloro-1,3-butadiene ug/kg 10801900 57 12-130ND
Hexachlorobenzene ug/kg 12801900 67 17-130ND
Hexachlorocyclopentadiene ug/kg 9391900 49 10-130ND
Hexachloroethane ug/kg 10501900 55 14-130ND
Indeno(1,2,3-cd)pyrene ug/kg 8891900 47 13-130ND
Isophorone ug/kg 12401900 65 17-130ND
N-Nitroso-di-n-propylamine ug/kg 12201900 64 10-130ND
N-Nitrosodimethylamine ug/kg 9971900 52 16-130ND
N-Nitrosodiphenylamine ug/kg 12601900 66 19-130ND
Naphthalene ug/kg 11301900 59 18-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
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Page 52 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4015345MATRIX SPIKE SAMPLE:
MSSpike
Result
92665974004
Nitrobenzene ug/kg 10701900 56 15-130ND
Pentachlorophenol ug/kg 27003810 71 10-130ND
Phenanthrene ug/kg 12901900 68 17-130ND
Phenol ug/kg 11901900 63 15-130ND
Pyrene ug/kg 12601900 66 31-130ND
Pyridine ug/kg 4071900 21 10-130ND
2,4,6-Tribromophenol (S) %68 10-131
2-Fluorobiphenyl (S) %48 10-130
2-Fluorophenol (S) %49 10-130
Nitrobenzene-d5 (S) %52 10-130
Phenol-d6 (S) %52 10-130
Terphenyl-d14 (S) %59 10-130
Parameter Units
Dup
Result QualifiersRPDResult
92665974005
4015346SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
1-Methylnaphthalene ug/kg NDND
2,2'-Oxybis(1-chloropropane) ug/kg NDND
2,4,5-Trichlorophenol ug/kg NDND
2,4,6-Trichlorophenol ug/kg NDND
2,4-Dichlorophenol ug/kg NDND
2,4-Dimethylphenol ug/kg NDND
2,4-Dinitrophenol ug/kg ND v1ND
2,4-Dinitrotoluene ug/kg NDND
2,6-Dinitrotoluene ug/kg NDND
2-Chloronaphthalene ug/kg NDND
2-Chlorophenol ug/kg NDND
2-Methylnaphthalene ug/kg NDND
2-Methylphenol(o-Cresol) ug/kg NDND
2-Nitroaniline ug/kg NDND
2-Nitrophenol ug/kg NDND
3&4-Methylphenol(m&p Cresol) ug/kg NDND
3,3'-Dichlorobenzidine ug/kg NDND
3-Nitroaniline ug/kg NDND
4,6-Dinitro-2-methylphenol ug/kg NDND
4-Bromophenylphenyl ether ug/kg NDND
4-Chloro-3-methylphenol ug/kg NDND
4-Chloroaniline ug/kg NDND
4-Chlorophenylphenyl ether ug/kg NDND
4-Nitroaniline ug/kg NDND
4-Nitrophenol ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
Page 53 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92665974005
4015346SAMPLE DUPLICATE:
Acenaphthene ug/kg NDND
Acenaphthylene ug/kg NDND
Aniline ug/kg NDND
Anthracene ug/kg NDND
Benzo(a)anthracene ug/kg NDND
Benzo(a)pyrene ug/kg NDND
Benzo(b)fluoranthene ug/kg NDND
Benzo(g,h,i)perylene ug/kg NDND
Benzo(k)fluoranthene ug/kg NDND
Benzoic Acid ug/kg NDND
Benzyl alcohol ug/kg NDND
bis(2-Chloroethoxy)methane ug/kg NDND
bis(2-Chloroethyl) ether ug/kg NDND
bis(2-Ethylhexyl)phthalate ug/kg NDND
Butylbenzylphthalate ug/kg NDND
Chrysene ug/kg NDND
Di-n-butylphthalate ug/kg NDND
Di-n-octylphthalate ug/kg NDND
Dibenz(a,h)anthracene ug/kg NDND
Dibenzofuran ug/kg NDND
Diethylphthalate ug/kg NDND
Dimethylphthalate ug/kg NDND
Fluoranthene ug/kg NDND
Fluorene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Hexachlorobenzene ug/kg NDND
Hexachlorocyclopentadiene ug/kg NDND
Hexachloroethane ug/kg NDND
Indeno(1,2,3-cd)pyrene ug/kg NDND
Isophorone ug/kg NDND
N-Nitroso-di-n-propylamine ug/kg NDND
N-Nitrosodimethylamine ug/kg NDND
N-Nitrosodiphenylamine ug/kg NDND
Naphthalene ug/kg NDND
Nitrobenzene ug/kg NDND
Pentachlorophenol ug/kg NDND
Phenanthrene ug/kg NDND
Phenol ug/kg NDND
Pyrene ug/kg NDND
Pyridine ug/kg NDND
2,4,6-Tribromophenol (S) %6059
2-Fluorobiphenyl (S) %5757
2-Fluorophenol (S) %5354
Nitrobenzene-d5 (S) %5960
Phenol-d6 (S) %5757
Terphenyl-d14 (S) %6663
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 54 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
773104
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92666252001, 92666252002, 92666252003, 92666252004, 92666252005, 92666252006
Parameter Units
Dup
Result QualifiersRPDResult
92666257001
4012920SAMPLE DUPLICATE:
Percent Moisture % 17.1 N2017.0
Parameter Units
Dup
Result QualifiersRPDResult
92666252006
4012921SAMPLE DUPLICATE:
Percent Moisture % 16.4 N2915.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666252
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
773361
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92666252007, 92666252008
Parameter Units
Dup
Result QualifiersRPDResult
92664914002
4014187SAMPLE DUPLICATE:
Percent Moisture % 80.6 N2080.3
Parameter Units
Dup
Result QualifiersRPDResult
92666318005
4014304SAMPLE DUPLICATE:
Percent Moisture % 25.5 N2426.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
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[phone]
Page 56 of 61
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92666252
Loves 412 23004903
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.
MS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The RPD value in one of the constituent analytes was outside the control limits.RS
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
Pace Analytical Services, LLC
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[phone]
Page 57 of 61
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92666252
Loves 412 23004903
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92666252001 773599 77371853234903 - 106 EPA 3546 EPA 8270E
92666252002 773599 77371853234903 - 107 EPA 3546 EPA 8270E
92666252003 773599 77371853234903 - 108 EPA 3546 EPA 8270E
92666252004 773599 77371853234903 - 109 EPA 3546 EPA 8270E
92666252005 773599 77371853234903 - 110 EPA 3546 EPA 8270E
92666252006 773599 77371853234903 - 125 EPA 3546 EPA 8270E
92666252007 773599 77371853234903 - 126 EPA 3546 EPA 8270E
92666252008 773599 77371853234903 - 132 EPA 3546 EPA 8270E
92666252001 773232 77324153234903 - 106 EPA 5035A/5030B EPA 8260D
92666252002 773232 77324153234903 - 107 EPA 5035A/5030B EPA 8260D
92666252003 773232 77324153234903 - 108 EPA 5035A/5030B EPA 8260D
92666252004 773232 77324153234903 - 109 EPA 5035A/5030B EPA 8260D
92666252005 773232 77324153234903 - 110 EPA 5035A/5030B EPA 8260D
92666252006 773232 77324153234903 - 125 EPA 5035A/5030B EPA 8260D
92666252007 773232 77324153234903 - 126 EPA 5035A/5030B EPA 8260D
92666252008 773106 77320253234903 - 132 EPA 5035A/5030B EPA 8260D
92666252001 77310453234903 - 106 SW-846
92666252002 77310453234903 - 107 SW-846
92666252003 77310453234903 - 108 SW-846
92666252004 77310453234903 - 109 SW-846
92666252005 77310453234903 - 110 SW-846
92666252006 77310453234903 - 125 SW-846
92666252007 77336153234903 - 126 SW-846
92666252008 77336153234903 - 132 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:37 PM
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Page 58 of 61
Page 59 of 61
Page 60 of 61
Page 61 of 61
#=CL#
May 23, 2023
LIMS USE: FR - MARK RYLAND
LIMS OBJECT ID: 92666250
92666250
Project:
Pace Project No.:
RE:
Mark Ryland
Apex Companies, LLC
203 Wylderose Court
Midlothian, VA 23113
Loves 412 23004903
Dear Mark Ryland:
Enclosed are the analytical results for sample(s) received by the laboratory on May 08, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92666250
Loves 412 23004903
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92666250
Loves 412 23004903
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92666250001 55234903-160 EPA 625.1 58 PASI-CPKS
SM 6200B 63 PASI-CLMB
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 3 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666250
Loves 412 23004903
Sample: 55234903-160 Lab ID: 92666250001 Collected: 05/05/23 12:30 Received: 05/08/23 13:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 05/12/23 01:26 83-32-905/09/23 11:032500 50
Acenaphthylene ND ug/L 05/12/23 01:26 208-96-805/09/23 11:032500 50
Anthracene ND ug/L 05/12/23 01:26 120-12-705/09/23 11:032500 50
Benzo(a)anthracene ND ug/L 05/12/23 01:26 56-55-305/09/23 11:032500 50
Benzo(a)pyrene ND ug/L 05/12/23 01:26 50-32-805/09/23 11:032500 50
Benzo(b)fluoranthene ND ug/L 05/12/23 01:26 205-99-205/09/23 11:032500 50
Benzo(g,h,i)perylene ND ug/L 05/12/23 01:26 191-24-205/09/23 11:032500 50
Benzo(k)fluoranthene ND ug/L 05/12/23 01:26 207-08-905/09/23 11:032500 50
4-Bromophenylphenyl ether ND ug/L 05/12/23 01:26 101-55-305/09/23 11:032500 50
Butylbenzylphthalate ND ug/L 05/12/23 01:26 85-68-705/09/23 11:032500 50
4-Chloro-3-methylphenol ND ug/L 05/12/23 01:26 59-50-705/09/23 11:032500 50
bis(2-Chloroethoxy)methane ND ug/L 05/12/23 01:26 111-91-105/09/23 11:035000 50
bis(2-Chloroethyl) ether ND ug/L 05/12/23 01:26 111-44-405/09/23 11:032500 50
2-Chloronaphthalene ND ug/L 05/12/23 01:26 91-58-705/09/23 11:032500 50
2-Chlorophenol ND ug/L 05/12/23 01:26 95-57-805/09/23 11:032500 50
4-Chlorophenylphenyl ether ND ug/L 05/12/23 01:26 7005-72-305/09/23 11:032500 50
Chrysene ND ug/L 05/12/23 01:26 218-01-905/09/23 11:032500 50
Dibenz(a,h)anthracene ND ug/L 05/12/23 01:26 53-70-305/09/23 11:032500 50
3,3'-Dichlorobenzidine ND ug/L 05/12/23 01:26 91-94-105/09/23 11:035000 50
2,4-Dichlorophenol ND ug/L 05/12/23 01:26 120-83-205/09/23 11:032500 50
Diethylphthalate ND ug/L 05/12/23 01:26 84-66-205/09/23 11:032500 50
2,4-Dimethylphenol ND ug/L 05/12/23 01:26 105-67-9 L105/09/23 11:035000 50
Dimethylphthalate ND ug/L 05/12/23 01:26 131-11-305/09/23 11:032500 50
Di-n-butylphthalate ND ug/L 05/12/23 01:26 84-74-205/09/23 11:032500 50
4,6-Dinitro-2-methylphenol ND ug/L 05/12/23 01:26 534-52-105/09/23 11:035000 50
2,4-Dinitrophenol ND ug/L 05/12/23 01:26 51-28-505/09/23 11:0325000 50
2,4-Dinitrotoluene ND ug/L 05/12/23 01:26 121-14-205/09/23 11:032500 50
2,6-Dinitrotoluene ND ug/L 05/12/23 01:26 606-20-205/09/23 11:032500 50
Di-n-octylphthalate ND ug/L 05/12/23 01:26 117-84-005/09/23 11:032500 50
bis(2-Ethylhexyl)phthalate ND ug/L 05/12/23 01:26 117-81-705/09/23 11:032500 50
Fluoranthene ND ug/L 05/12/23 01:26 206-44-005/09/23 11:032500 50
Fluorene ND ug/L 05/12/23 01:26 86-73-705/09/23 11:032500 50
Hexachloro-1,3-butadiene ND ug/L 05/12/23 01:26 87-68-305/09/23 11:032500 50
Hexachlorobenzene ND ug/L 05/12/23 01:26 118-74-105/09/23 11:032500 50
Hexachlorocyclopentadiene ND ug/L 05/12/23 01:26 77-47-405/09/23 11:035000 50
Hexachloroethane ND ug/L 05/12/23 01:26 67-72-105/09/23 11:032500 50
Indeno(1,2,3-cd)pyrene ND ug/L 05/12/23 01:26 193-39-505/09/23 11:032500 50
Isophorone ND ug/L 05/12/23 01:26 78-59-105/09/23 11:035000 50
Naphthalene ND ug/L 05/12/23 01:26 91-20-305/09/23 11:032500 50
Nitrobenzene ND ug/L 05/12/23 01:26 98-95-305/09/23 11:032500 50
2-Nitrophenol ND ug/L 05/12/23 01:26 88-75-505/09/23 11:032500 50
4-Nitrophenol ND ug/L 05/12/23 01:26 100-02-705/09/23 11:035000 50
N-Nitrosodimethylamine ND ug/L 05/12/23 01:26 62-75-905/09/23 11:032500 50
N-Nitroso-di-n-propylamine ND ug/L 05/12/23 01:26 621-64-705/09/23 11:032500 50
N-Nitrosodiphenylamine ND ug/L 05/12/23 01:26 86-30-605/09/23 11:035000 50
2,2'-Oxybis(1-chloropropane) ND ug/L 05/12/23 01:26 108-60-105/09/23 11:032500 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666250
Loves 412 23004903
Sample: 55234903-160 Lab ID: 92666250001 Collected: 05/05/23 12:30 Received: 05/08/23 13:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Pentachlorophenol ND ug/L 05/12/23 01:26 87-86-505/09/23 11:035000 50
Phenanthrene 3500 ug/L 05/12/23 01:26 85-01-805/09/23 11:032500 50
Phenol ND ug/L 05/12/23 01:26 108-95-205/09/23 11:032500 50
Pyrene 3930 ug/L 05/12/23 01:26 129-00-005/09/23 11:032500 50
1,2,4-Trichlorobenzene ND ug/L 05/12/23 01:26 120-82-105/09/23 11:032500 50
2,4,6-Trichlorophenol ND ug/L 05/12/23 01:26 88-06-205/09/23 11:035000 50
Surrogates
Nitrobenzene-d5 (S) 0 %05/12/23 01:26 4165-60-0 D3,S405/09/23 11:0310-120 50
2-Fluorobiphenyl (S) 0 %05/12/23 01:26 321-60-8 S405/09/23 11:0315-120 50
Terphenyl-d14 (S) 0 %05/12/23 01:26 1718-51-0 S405/09/23 11:0311-131 50
Phenol-d6 (S)0 %05/12/23 01:26 13127-88-3 S405/09/23 11:0310-120 50
2-Fluorophenol (S) 0 %05/12/23 01:26 367-12-4 S405/09/23 11:0310-120 50
2,4,6-Tribromophenol (S) 0 %05/12/23 01:26 118-79-6 S405/09/23 11:0310-137 50
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 05/22/23 15:15 71-43-2 H112.5 25
Bromobenzene ND ug/L 05/22/23 15:15 108-86-1 H112.5 25
Bromochloromethane ND ug/L 05/22/23 15:15 74-97-5 H112.5 25
Bromodichloromethane ND ug/L 05/22/23 15:15 75-27-4 H112.5 25
Bromoform ND ug/L 05/22/23 15:15 75-25-2 H112.5 25
Bromomethane ND ug/L 05/22/23 15:15 74-83-9 H1125 25
n-Butylbenzene 789 ug/L 05/22/23 15:15 104-51-8 H112.5 25
sec-Butylbenzene 587 ug/L 05/22/23 15:15 135-98-8 H112.5 25
tert-Butylbenzene ND ug/L 05/22/23 15:15 98-06-6 H112.5 25
Carbon tetrachloride ND ug/L 05/22/23 15:15 56-23-5 H112.5 25
Chlorobenzene ND ug/L 05/22/23 15:15 108-90-7 H112.5 25
Chloroethane ND ug/L 05/22/23 15:15 75-00-3 H125.0 25
Chloroform ND ug/L 05/22/23 15:15 67-66-3 H112.5 25
Chloromethane ND ug/L 05/22/23 15:15 74-87-3 H125.0 25
2-Chlorotoluene ND ug/L 05/22/23 15:15 95-49-8 H112.5 25
4-Chlorotoluene ND ug/L 05/22/23 15:15 106-43-4 H112.5 25
1,2-Dibromo-3-chloropropane ND ug/L 05/22/23 15:15 96-12-8 H125.0 25
Dibromochloromethane ND ug/L 05/22/23 15:15 124-48-1 H112.5 25
1,2-Dibromoethane (EDB) ND ug/L 05/22/23 15:15 106-93-4 H112.5 25
Dibromomethane ND ug/L 05/22/23 15:15 74-95-3 H112.5 25
1,2-Dichlorobenzene ND ug/L 05/22/23 15:15 95-50-1 H112.5 25
1,3-Dichlorobenzene ND ug/L 05/22/23 15:15 541-73-1 H112.5 25
1,4-Dichlorobenzene ND ug/L 05/22/23 15:15 106-46-7 H112.5 25
Dichlorodifluoromethane ND ug/L 05/22/23 15:15 75-71-8 H112.5 25
1,1-Dichloroethane ND ug/L 05/22/23 15:15 75-34-3 H112.5 25
1,2-Dichloroethane ND ug/L 05/22/23 15:15 107-06-2 H112.5 25
1,1-Dichloroethene ND ug/L 05/22/23 15:15 75-35-4 H112.5 25
cis-1,2-Dichloroethene ND ug/L 05/22/23 15:15 156-59-2 H112.5 25
trans-1,2-Dichloroethene ND ug/L 05/22/23 15:15 156-60-5 H112.5 25
1,2-Dichloropropane ND ug/L 05/22/23 15:15 78-87-5 H112.5 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92666250
Loves 412 23004903
Sample: 55234903-160 Lab ID: 92666250001 Collected: 05/05/23 12:30 Received: 05/08/23 13:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,3-Dichloropropane ND ug/L 05/22/23 15:15 142-28-9 H112.5 25
2,2-Dichloropropane ND ug/L 05/22/23 15:15 594-20-7 H112.5 25
1,1-Dichloropropene ND ug/L 05/22/23 15:15 563-58-6 H112.5 25
cis-1,3-Dichloropropene ND ug/L 05/22/23 15:15 10061-01-5 H112.5 25
trans-1,3-Dichloropropene ND ug/L 05/22/23 15:15 10061-02-6 H112.5 25
Diisopropyl ether ND ug/L 05/22/23 15:15 108-20-3 H112.5 25
Ethylbenzene 29.7 ug/L 05/22/23 15:15 100-41-4 H112.5 25
Hexachloro-1,3-butadiene ND ug/L 05/22/23 15:15 87-68-3 H150.0 25
Isopropylbenzene (Cumene)136 ug/L 05/22/23 15:15 98-82-8 H112.5 25
Methylene Chloride ND ug/L 05/22/23 15:15 75-09-2 H150.0 25
Methyl-tert-butyl ether ND ug/L 05/22/23 15:15 1634-04-4 H112.5 25
Naphthalene 522 ug/L 05/22/23 15:15 91-20-3 H150.0 25
n-Propylbenzene 352 ug/L 05/22/23 15:15 103-65-1 H112.5 25
Styrene ND ug/L 05/22/23 15:15 100-42-5 H112.5 25
1,1,1,2-Tetrachloroethane ND ug/L 05/22/23 15:15 630-20-6 H112.5 25
1,1,2,2-Tetrachloroethane ND ug/L 05/22/23 15:15 79-34-5 H112.5 25
Tetrachloroethene ND ug/L 05/22/23 15:15 127-18-4 H112.5 25
Toluene ND ug/L 05/22/23 15:15 108-88-3 H112.5 25
1,2,3-Trichlorobenzene ND ug/L 05/22/23 15:15 87-61-6 H150.0 25
1,2,4-Trichlorobenzene ND ug/L 05/22/23 15:15 120-82-1 H150.0 25
1,1,1-Trichloroethane ND ug/L 05/22/23 15:15 71-55-6 H112.5 25
1,1,2-Trichloroethane ND ug/L 05/22/23 15:15 79-00-5 H112.5 25
Trichloroethene ND ug/L 05/22/23 15:15 79-01-6 H112.5 25
Trichlorofluoromethane ND ug/L 05/22/23 15:15 75-69-4 H125.0 25
1,2,3-Trichloropropane ND ug/L 05/22/23 15:15 96-18-4 H112.5 25
1,2,4-Trimethylbenzene ND ug/L 05/22/23 15:15 95-63-6 H112.5 25
1,3,5-Trimethylbenzene ND ug/L 05/22/23 15:15 108-67-8 H112.5 25
Vinyl chloride ND ug/L 05/22/23 15:15 75-01-4 H125.0 25
m&p-Xylene ND ug/L 05/22/23 15:15 179601-23-1 H125.0 25
o-Xylene ND ug/L 05/22/23 15:15 95-47-6 H112.5 25
Surrogates
1,2-Dichloroethane-d4 (S) 101 %05/22/23 15:15 17060-07-0 D3,H570-130 25
4-Bromofluorobenzene (S) 128 %05/22/23 15:15 460-00-470-130 25
Toluene-d8 (S) 112 %05/22/23 15:15 2037-26-570-130 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666250
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
776053
SM 6200B
SM 6200B
6200B MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92666250001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4026368
Associated Lab Samples:92666250001
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/22/23 10:12
1,1,1-Trichloroethane ug/L ND 0.50 05/22/23 10:12
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/22/23 10:12
1,1,2-Trichloroethane ug/L ND 0.50 05/22/23 10:12
1,1-Dichloroethane ug/L ND 0.50 05/22/23 10:12
1,1-Dichloroethene ug/L ND 0.50 05/22/23 10:12
1,1-Dichloropropene ug/L ND 0.50 05/22/23 10:12
1,2,3-Trichlorobenzene ug/L ND 2.0 05/22/23 10:12
1,2,3-Trichloropropane ug/L ND 0.50 05/22/23 10:12
1,2,4-Trichlorobenzene ug/L ND 2.0 05/22/23 10:12
1,2,4-Trimethylbenzene ug/L ND 0.50 05/22/23 10:12
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/22/23 10:12
1,2-Dibromoethane (EDB) ug/L ND 0.50 05/22/23 10:12
1,2-Dichlorobenzene ug/L ND 0.50 05/22/23 10:12
1,2-Dichloroethane ug/L ND 0.50 05/22/23 10:12
1,2-Dichloropropane ug/L ND 0.50 05/22/23 10:12
1,3,5-Trimethylbenzene ug/L ND 0.50 05/22/23 10:12
1,3-Dichlorobenzene ug/L ND 0.50 05/22/23 10:12
1,3-Dichloropropane ug/L ND 0.50 05/22/23 10:12
1,4-Dichlorobenzene ug/L ND 0.50 05/22/23 10:12
2,2-Dichloropropane ug/L ND 0.50 05/22/23 10:12
2-Chlorotoluene ug/L ND 0.50 05/22/23 10:12
4-Chlorotoluene ug/L ND 0.50 05/22/23 10:12
Benzene ug/L ND 0.50 05/22/23 10:12
Bromobenzene ug/L ND 0.50 05/22/23 10:12
Bromochloromethane ug/L ND 0.50 05/22/23 10:12
Bromodichloromethane ug/L ND 0.50 05/22/23 10:12
Bromoform ug/L ND 0.50 05/22/23 10:12
Bromomethane ug/L ND 5.0 05/22/23 10:12
Carbon tetrachloride ug/L ND 0.50 05/22/23 10:12
Chlorobenzene ug/L ND 0.50 05/22/23 10:12
Chloroethane ug/L ND 1.0 05/22/23 10:12
Chloroform ug/L ND 0.50 05/22/23 10:12
Chloromethane ug/L ND 1.0 05/22/23 10:12
cis-1,2-Dichloroethene ug/L ND 0.50 05/22/23 10:12
cis-1,3-Dichloropropene ug/L ND 0.50 05/22/23 10:12
Dibromochloromethane ug/L ND 0.50 05/22/23 10:12
Dibromomethane ug/L ND 0.50 05/22/23 10:12
Dichlorodifluoromethane ug/L ND 0.50 05/22/23 10:12
Diisopropyl ether ug/L ND 0.50 05/22/23 10:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666250
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4026368
Associated Lab Samples:92666250001
Matrix: Water
Analyzed
Ethylbenzene ug/L ND 0.50 05/22/23 10:12
Hexachloro-1,3-butadiene ug/L ND 2.0 05/22/23 10:12
Isopropylbenzene (Cumene) ug/L ND 0.50 05/22/23 10:12
m&p-Xylene ug/L ND 1.0 05/22/23 10:12
Methyl-tert-butyl ether ug/L ND 0.50 05/22/23 10:12
Methylene Chloride ug/L ND 2.0 05/22/23 10:12
n-Butylbenzene ug/L ND 0.50 05/22/23 10:12
n-Propylbenzene ug/L ND 0.50 05/22/23 10:12
Naphthalene ug/L ND 2.0 05/22/23 10:12
o-Xylene ug/L ND 0.50 05/22/23 10:12
sec-Butylbenzene ug/L ND 0.50 05/22/23 10:12
Styrene ug/L ND 0.50 05/22/23 10:12
tert-Butylbenzene ug/L ND 0.50 05/22/23 10:12
Tetrachloroethene ug/L ND 0.50 05/22/23 10:12
Toluene ug/L ND 0.50 05/22/23 10:12
trans-1,2-Dichloroethene ug/L ND 0.50 05/22/23 10:12
trans-1,3-Dichloropropene ug/L ND 0.50 05/22/23 10:12
Trichloroethene ug/L ND 0.50 05/22/23 10:12
Trichlorofluoromethane ug/L ND 1.0 05/22/23 10:12
Vinyl chloride ug/L ND 1.0 05/22/23 10:12
1,2-Dichloroethane-d4 (S) % 92 70-130 05/22/23 10:12
4-Bromofluorobenzene (S) % 102 70-130 05/22/23 10:12
Toluene-d8 (S) % 99 70-130 05/22/23 10:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026369LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.420 97 60-140
1,1,1-Trichloroethane ug/L 19.620 98 60-140
1,1,2,2-Tetrachloroethane ug/L 19.820 99 60-140
1,1,2-Trichloroethane ug/L 18.420 92 60-140
1,1-Dichloroethane ug/L 19.420 97 60-140
1,1-Dichloroethene ug/L 21.520 108 60-140
1,1-Dichloropropene ug/L 21.520 107 60-140
1,2,3-Trichlorobenzene ug/L 21.320 106 60-140
1,2,3-Trichloropropane ug/L 19.520 98 60-140
1,2,4-Trichlorobenzene ug/L 22.620 113 60-140
1,2,4-Trimethylbenzene ug/L 20.720 104 60-140
1,2-Dibromo-3-chloropropane ug/L 19.420 97 60-140
1,2-Dibromoethane (EDB) ug/L 19.720 98 60-140
1,2-Dichlorobenzene ug/L 21.120 105 60-140
1,2-Dichloroethane ug/L 19.020 95 60-140
1,2-Dichloropropane ug/L 20.420 102 60-140
1,3,5-Trimethylbenzene ug/L 21.020 105 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666250
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026369LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 21.220 106 60-140
1,3-Dichloropropane ug/L 20.620 103 60-140
1,4-Dichlorobenzene ug/L 20.120 100 60-140
2,2-Dichloropropane ug/L 18.920 95 60-140
2-Chlorotoluene ug/L 21.120 105 60-140
4-Chlorotoluene ug/L 20.320 102 60-140
Benzene ug/L 20.420 102 60-140
Bromobenzene ug/L 20.120 101 60-140
Bromochloromethane ug/L 20.520 102 60-140
Bromodichloromethane ug/L 17.920 89 60-140
Bromoform ug/L 19.320 97 60-140
Bromomethane ug/L 12.020 60 60-140
Carbon tetrachloride ug/L 19.920 99 60-140
Chlorobenzene ug/L 20.720 103 60-140
Chloroethane ug/L 19.020 95 60-140
Chloroform ug/L 17.720 89 60-140
Chloromethane ug/L 21.220 106 60-140
cis-1,2-Dichloroethene ug/L 19.620 98 60-140
cis-1,3-Dichloropropene ug/L 20.020 100 60-140
Dibromochloromethane ug/L 17.920 89 60-140
Dibromomethane ug/L 18.520 92 60-140
Dichlorodifluoromethane ug/L 25.020 125 60-140
Diisopropyl ether ug/L 19.220 96 60-140
Ethylbenzene ug/L 20.820 104 60-140
Hexachloro-1,3-butadiene ug/L 22.720 113 60-140
Isopropylbenzene (Cumene) ug/L 21.220 106 60-140
m&p-Xylene ug/L 42.140 105 60-140
Methyl-tert-butyl ether ug/L 17.920 89 60-140
Methylene Chloride ug/L 20.720 104 60-140
n-Butylbenzene ug/L 22.720 113 60-140
n-Propylbenzene ug/L 21.520 107 60-140
Naphthalene ug/L 21.920 110 60-140
o-Xylene ug/L 20.320 101 60-140
sec-Butylbenzene ug/L 21.520 108 60-140
Styrene ug/L 20.420 102 60-140
tert-Butylbenzene ug/L 17.720 88 60-140
Tetrachloroethene ug/L 20.420 102 60-140
Toluene ug/L 19.220 96 60-140
trans-1,2-Dichloroethene ug/L 20.120 100 60-140
trans-1,3-Dichloropropene ug/L 18.720 93 60-140
Trichloroethene ug/L 20.020 100 60-140
Trichlorofluoromethane ug/L 18.820 94 60-140
Vinyl chloride ug/L 17.020 85 60-140
1,2-Dichloroethane-d4 (S) %98 70-130
4-Bromofluorobenzene (S) %101 70-130
Toluene-d8 (S) %98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666250
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026370MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667432001
4026371
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 87 60-140101 1620ND17.3 20.2
1,1,1-Trichloroethane ug/L 20 92 60-140102 1120ND18.4 20.4
1,1,2,2-Tetrachloroethane ug/L 20 86 60-140100 1420ND17.3 19.9
1,1,2-Trichloroethane ug/L 20 84 60-14096 1320ND16.9 19.2
1,1-Dichloroethane ug/L 20 95 60-140108 1220ND19.1 21.5
1,1-Dichloroethene ug/L 20 108 60-140118 920ND21.5 23.5
1,1-Dichloropropene ug/L 20 103 60-140114 1020ND20.6 22.8
1,2,3-Trichlorobenzene ug/L 20 91 60-140115 2420ND18.1 23.0
1,2,3-Trichloropropane ug/L 20 87 60-14094 820ND17.4 18.9
1,2,4-Trichlorobenzene ug/L 20 91 60-140115 2320ND18.2 22.9
1,2,4-Trimethylbenzene ug/L 20 93 60-140109 1520ND18.6 21.7
1,2-Dibromo-3-chloropropane ug/L 20 80 60-14092 1420ND16.1 18.5
1,2-Dibromoethane (EDB) ug/L 20 90 60-140100 1120ND18.0 20.1
1,2-Dichlorobenzene ug/L 20 94 60-140111 1720ND18.8 22.2
1,2-Dichloroethane ug/L 20 89 60-140103 1420ND17.9 20.6
1,2-Dichloropropane ug/L 20 93 60-140109 1620ND18.6 21.7
1,3,5-Trimethylbenzene ug/L 20 95 60-140111 1520ND19.1 22.2
1,3-Dichlorobenzene ug/L 20 95 60-140112 1620ND19.1 22.5
1,3-Dichloropropane ug/L 20 93 60-140104 1220ND18.5 20.8
1,4-Dichlorobenzene ug/L 20 90 60-140105 1620ND18.0 21.0
2,2-Dichloropropane ug/L 20 90 60-140100 1020ND18.1 20.0
2-Chlorotoluene ug/L 20 96 60-140110 1320ND19.3 21.9
4-Chlorotoluene ug/L 20 93 60-140106 1320ND18.6 21.2
Benzene ug/L 20 95 60-140107 1220ND19.0 21.5
Bromobenzene ug/L 20 90 60-140102 1220ND18.0 20.3
Bromochloromethane ug/L 20 96 60-140108 1220ND19.2 21.6
Bromodichloromethane ug/L 20 80 60-14090 1220ND16.0 18.0
Bromoform ug/L 20 85 60-14097 1320ND17.0 19.3
Bromomethane ug/L M12051 60-14067 2820ND10.1 13.5
Carbon tetrachloride ug/L 20 88 60-140100 1320ND17.5 20.0
Chlorobenzene ug/L 20 96 60-140105 920ND19.2 21.0
Chloroethane ug/L 20 102 60-140114 1120ND20.4 22.8
Chloroform ug/L 20 86 60-14095 920ND17.2 18.9
Chloromethane ug/L 20 102 60-140112 1020ND20.4 22.5
cis-1,2-Dichloroethene ug/L 20 93 60-140106 1320ND18.5 21.2
cis-1,3-Dichloropropene ug/L 20 87 60-14098 1220ND17.4 19.6
Dibromochloromethane ug/L 20 79 60-14091 1420ND15.9 18.2
Dibromomethane ug/L 20 84 60-14093 1020ND16.9 18.6
Dichlorodifluoromethane ug/L 20 127 60-140132 420ND25.3 26.5
Diisopropyl ether ug/L 20 90 60-140104 14201.1 19.2 22.0
Ethylbenzene ug/L 20 96 60-140106 920ND19.3 21.2
Hexachloro-1,3-butadiene ug/L 20 109 60-140125 1320ND21.8 24.9
Isopropylbenzene (Cumene) ug/L 20 99 60-140111 1120ND19.9 22.2
m&p-Xylene ug/L 40 98 60-140109 1040ND39.2 43.5
Methyl-tert-butyl ether ug/L 20 88 60-140107 112014.3 32.0 35.6
Methylene Chloride ug/L 20 100 60-140113 1220ND20.0 22.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666250
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026370MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667432001
4026371
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 103 60-140122 1620ND20.7 24.4
n-Propylbenzene ug/L 20 98 60-140112 1320ND19.7 22.4
Naphthalene ug/L 20 90 60-140112 2220ND18.0 22.3
o-Xylene ug/L 20 96 60-140104 920ND19.2 20.9
sec-Butylbenzene ug/L 20 101 60-140118 1620ND20.1 23.7
Styrene ug/L 20 94 60-140102 920ND18.7 20.4
tert-Butylbenzene ug/L 20 83 60-14094 1320ND16.6 18.9
Tetrachloroethene ug/L 20 93 60-140102 1020ND18.5 20.4
Toluene ug/L 20 91 60-140101 1120ND18.2 20.3
trans-1,2-Dichloroethene ug/L 20 94 60-140110 1520ND18.8 22.0
trans-1,3-Dichloropropene ug/L 20 82 60-14094 1420ND16.3 18.8
Trichloroethene ug/L 20 99 60-140104 520ND19.7 20.7
Trichlorofluoromethane ug/L 20 93 60-140103 1020ND18.6 20.5
Vinyl chloride ug/L 20 86 60-14094 920ND17.2 18.8
1,2-Dichloroethane-d4 (S) %97 70-130101
4-Bromofluorobenzene (S) %102 70-130101
Toluene-d8 (S) %99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666250
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
773203
EPA 625.1
EPA 625.1
625 MSS
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92666250001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4013204
Associated Lab Samples:92666250001
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 05/09/23 16:54
2,2'-Oxybis(1-chloropropane) ug/L ND 5.0 05/09/23 16:54
2,4,6-Trichlorophenol ug/L ND 10.0 05/09/23 16:54
2,4-Dichlorophenol ug/L ND 5.0 05/09/23 16:54
2,4-Dimethylphenol ug/L ND 10.0 05/09/23 16:54
2,4-Dinitrophenol ug/L ND 50.0 05/09/23 16:54
2,4-Dinitrotoluene ug/L ND 5.0 05/09/23 16:54
2,6-Dinitrotoluene ug/L ND 5.0 05/09/23 16:54
2-Chloronaphthalene ug/L ND 5.0 05/09/23 16:54
2-Chlorophenol ug/L ND 5.0 05/09/23 16:54
2-Nitrophenol ug/L ND 5.0 05/09/23 16:54
3,3'-Dichlorobenzidine ug/L ND 10.0 05/09/23 16:54
4,6-Dinitro-2-methylphenol ug/L ND 10.0 05/09/23 16:54
4-Bromophenylphenyl ether ug/L ND 5.0 05/09/23 16:54
4-Chloro-3-methylphenol ug/L ND 5.0 05/09/23 16:54
4-Chlorophenylphenyl ether ug/L ND 5.0 05/09/23 16:54
4-Nitrophenol ug/L ND 10.0 05/09/23 16:54
Acenaphthene ug/L ND 5.0 05/09/23 16:54
Acenaphthylene ug/L ND 5.0 05/09/23 16:54
Anthracene ug/L ND 5.0 05/09/23 16:54
Benzo(a)anthracene ug/L ND 5.0 05/09/23 16:54
Benzo(a)pyrene ug/L ND 5.0 05/09/23 16:54
Benzo(b)fluoranthene ug/L ND 5.0 05/09/23 16:54
Benzo(g,h,i)perylene ug/L ND 5.0 05/09/23 16:54
Benzo(k)fluoranthene ug/L ND 5.0 05/09/23 16:54
bis(2-Chloroethoxy)methane ug/L ND 10.0 05/09/23 16:54
bis(2-Chloroethyl) ether ug/L ND 5.0 05/09/23 16:54
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 05/09/23 16:54
Butylbenzylphthalate ug/L ND 5.0 05/09/23 16:54
Chrysene ug/L ND 5.0 05/09/23 16:54
Di-n-butylphthalate ug/L ND 5.0 05/09/23 16:54
Di-n-octylphthalate ug/L ND 5.0 05/09/23 16:54
Dibenz(a,h)anthracene ug/L ND 5.0 05/09/23 16:54
Diethylphthalate ug/L ND 5.0 05/09/23 16:54
Dimethylphthalate ug/L ND 5.0 05/09/23 16:54
Fluoranthene ug/L ND 5.0 05/09/23 16:54
Fluorene ug/L ND 5.0 05/09/23 16:54
Hexachloro-1,3-butadiene ug/L ND 5.0 05/09/23 16:54
Hexachlorobenzene ug/L ND 5.0 05/09/23 16:54
Hexachlorocyclopentadiene ug/L ND 10.0 05/09/23 16:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666250
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4013204
Associated Lab Samples:92666250001
Matrix: Water
Analyzed
Hexachloroethane ug/L ND 5.0 05/09/23 16:54
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 05/09/23 16:54
Isophorone ug/L ND 10.0 05/09/23 16:54
N-Nitroso-di-n-propylamine ug/L ND 5.0 05/09/23 16:54
N-Nitrosodimethylamine ug/L ND 5.0 05/09/23 16:54
N-Nitrosodiphenylamine ug/L ND 10.0 05/09/23 16:54
Naphthalene ug/L ND 5.0 05/09/23 16:54
Nitrobenzene ug/L ND 5.0 05/09/23 16:54
Pentachlorophenol ug/L ND 10.0 05/09/23 16:54
Phenanthrene ug/L ND 5.0 05/09/23 16:54
Phenol ug/L ND 5.0 05/09/23 16:54
Pyrene ug/L ND 5.0 05/09/23 16:54
2,4,6-Tribromophenol (S) % 93 10-137 05/09/23 16:54
2-Fluorobiphenyl (S) % 71 15-120 05/09/23 16:54
2-Fluorophenol (S) % 62 10-120 05/09/23 16:54
Nitrobenzene-d5 (S) % 83 10-120 05/09/23 16:54
Phenol-d6 (S) % 48 10-120 05/09/23 16:54
Terphenyl-d14 (S) % 94 11-131 05/09/23 16:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4013205LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 29.550 59 44-142
2,2'-Oxybis(1-chloropropane) ug/L 38.250 76 36-166
2,4,6-Trichlorophenol ug/L 51.550 103 37-144
2,4-Dichlorophenol ug/L 48.450 97 1-191
2,4-Dimethylphenol ug/L 73.5 L150 147 32-119
2,4-Dinitrophenol ug/L 313250 125 1-181
2,4-Dinitrotoluene ug/L 53.250 106 39-139
2,6-Dinitrotoluene ug/L 52.450 105 50-158
2-Chloronaphthalene ug/L 39.650 79 60-118
2-Chlorophenol ug/L 43.150 86 23-134
2-Nitrophenol ug/L 49.350 99 29-182
3,3'-Dichlorobenzidine ug/L 96.1100 96 1-262
4,6-Dinitro-2-methylphenol ug/L 118100 118 1-181
4-Bromophenylphenyl ether ug/L 49.950 100 53-127
4-Chloro-3-methylphenol ug/L 97.5100 97 22-147
4-Chlorophenylphenyl ether ug/L 46.850 94 25-158
4-Nitrophenol ug/L 159250 63 1-132
Acenaphthene ug/L 45.250 90 47-145
Acenaphthylene ug/L 44.950 90 33-145
Anthracene ug/L 46.750 93 1-166
Benzo(a)anthracene ug/L 49.550 99 33-143
Benzo(a)pyrene ug/L 48.450 97 17-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666250
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4013205LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 48.150 96 24-159
Benzo(g,h,i)perylene ug/L 50.350 101 1-219
Benzo(k)fluoranthene ug/L 48.150 96 11-162
bis(2-Chloroethoxy)methane ug/L 45.850 92 33-184
bis(2-Chloroethyl) ether ug/L 43.150 86 12-158
bis(2-Ethylhexyl)phthalate ug/L 51.450 103 8-158
Butylbenzylphthalate ug/L 52.350 105 1-152
Chrysene ug/L 49.650 99 17-168
Di-n-butylphthalate ug/L 51.350 103 1-118
Di-n-octylphthalate ug/L 53.050 106 4-146
Dibenz(a,h)anthracene ug/L 50.350 101 1-227
Diethylphthalate ug/L 50.150 100 1-114
Dimethylphthalate ug/L 49.550 99 1-112
Fluoranthene ug/L 52.350 105 26-137
Fluorene ug/L 48.950 98 59-121
Hexachloro-1,3-butadiene ug/L 25.850 52 24-116
Hexachlorobenzene ug/L 50.550 101 1-152
Hexachlorocyclopentadiene ug/L 30.150 60 25-150
Hexachloroethane ug/L 25.050 50 40-113
Indeno(1,2,3-cd)pyrene ug/L 51.050 102 1-171
Isophorone ug/L 48.050 96 21-196
N-Nitroso-di-n-propylamine ug/L 45.250 90 1-230
N-Nitrosodimethylamine ug/L 38.950 78 25-150
N-Nitrosodiphenylamine ug/L 48.550 97 25-150
Naphthalene ug/L 34.050 68 21-133
Nitrobenzene ug/L 42.150 84 35-180
Pentachlorophenol ug/L 107100 107 14-176
Phenanthrene ug/L 49.050 98 54-120
Phenol ug/L 31.150 62 5-112
Pyrene ug/L 49.150 98 52-115
2,4,6-Tribromophenol (S) %136 10-137
2-Fluorobiphenyl (S) %96 15-120
2-Fluorophenol (S) %78 10-120
Nitrobenzene-d5 (S) %103 10-120
Phenol-d6 (S) %63 10-120
Terphenyl-d14 (S) %113 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4013206MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92665704001
4013207
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L M1,R183.3 44 44-14226 5083.3ND 36.9 22.1
2,2'-Oxybis(1-chloropropane) ug/L M1,R183.3 47 36-16632 3883.3ND 39.4 26.7
2,4,6-Trichlorophenol ug/L R183.3 79 37-14448 4783.3ND 65.5 40.4
2,4-Dichlorophenol ug/L R183.3 72 1-19145 4783.3ND 59.8 37.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666250
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4013206MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92665704001
4013207
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4-Dimethylphenol ug/L M0,R183.3 128 32-11981 4583.3ND 107 67.7
2,4-Dinitrophenol ug/L R141790 1-18165 32417ND373 272
2,4-Dinitrotoluene ug/L 83.3 81 39-13961 2883.3ND 67.7 50.9
2,6-Dinitrotoluene ug/L M1,R183.3 77 50-15848 4683.3ND 64.3 40.1
2-Chloronaphthalene ug/L M1,R183.3 56 60-11834 4883.3ND 46.7 28.5
2-Chlorophenol ug/L R183.3 62 23-13440 4283.3ND 51.6 33.6
2-Nitrophenol ug/L R183.3 71 29-18245 4483.3ND 59.2 37.8
3,3'-Dichlorobenzidine ug/L 167 47 1-26247 1167ND78.4 78.9
4,6-Dinitro-2-methylphenol ug/L 167 83 1-18165 26167ND139 108
4-Bromophenylphenyl ether ug/L M1,R183.3 66 53-12746 3683.3ND 55.4 38.6
4-Chloro-3-methylphenol ug/L R116782 22-14751 46167ND136 85.3
4-Chlorophenylphenyl ether ug/L R183.3 69 25-15844 4483.3ND 57.2 36.7
4-Nitrophenol ug/L 417 61 1-13249 22417ND254 204
Acenaphthene ug/L M1,R183.3 60 47-14536 5183.3ND 50.1 29.8
Acenaphthylene ug/L R183.3 59 33-14536 4783.3ND 49.0 30.4
Anthracene ug/L 83.3 64 1-16649 2783.3ND 53.5 40.6
Benzo(a)anthracene ug/L 83.3 74 33-14364 1583.3ND 61.5 53.1
Benzo(a)pyrene ug/L 83.3 70 17-16358 1983.3ND 58.1 48.2
Benzo(b)fluoranthene ug/L 83.3 69 24-15959 1683.3ND 57.5 48.8
Benzo(g,h,i)perylene ug/L 83.3 76 1-21962 2183.3ND 63.7 51.8
Benzo(k)fluoranthene ug/L 83.3 69 11-16257 1983.3ND 57.6 47.5
bis(2-Chloroethoxy)methane ug/L R183.3 71 33-18445 4583.3ND 59.2 37.4
bis(2-Chloroethyl) ether ug/L R183.3 69 12-15846 4083.3ND 57.4 38.4
bis(2-Ethylhexyl)phthalate ug/L 83.3 72 8-15861 1683.3ND 59.8 51.0
Butylbenzylphthalate ug/L 83.3 76 1-15263 1983.3ND 63.2 52.3
Chrysene ug/L 83.3 76 17-16864 1683.3ND 63.2 53.6
Di-n-butylphthalate ug/L 83.3 68 1-11856 1983.3ND 56.7 46.9
Di-n-octylphthalate ug/L 83.3 74 4-14662 1783.3ND 61.6 51.9
Dibenz(a,h)anthracene ug/L 83.3 77 1-22762 2183.3ND 64.5 52.1
Diethylphthalate ug/L 83.3 71 1-11453 2983.3ND 59.4 44.1
Dimethylphthalate ug/L R183.3 68 1-11245 4083.3ND 56.5 37.6
Fluoranthene ug/L 83.3 74 26-13759 2283.3ND 61.8 49.5
Fluorene ug/L M1,R183.3 65 59-12142 4483.3ND 54.6 34.9
Hexachloro-1,3-butadiene ug/L R183.3 43 24-11626 5083.3ND 35.5 21.4
Hexachlorobenzene ug/L 83.3 64 1-15249 2683.3ND 53.3 40.9
Hexachlorocyclopentadiene ug/L R183.3 42 25-15025 5383.3ND 35.4 20.7
Hexachloroethane ug/L M1,R183.3 34 40-11320 4983.3ND 28.0 17.0
Indeno(1,2,3-cd)pyrene ug/L 83.3 77 1-17163 2083.3ND 64.4 52.8
Isophorone ug/L R183.3 78 21-19648 4783.3ND 65.4 40.3
N-Nitroso-di-n-propylamine ug/L R183.3 75 1-23049 4283.3ND 62.2 40.7
N-Nitrosodimethylamine ug/L 83.3 66 25-15050 2983.3ND 55.2 41.3
N-Nitrosodiphenylamine ug/L R183.3 67 25-15049 3183.3ND 55.9 40.8
Naphthalene ug/L R183.3 44 21-13328 4383.3ND 36.5 23.6
Nitrobenzene ug/L R183.3 76 35-18050 4183.3ND 63.4 41.6
Pentachlorophenol ug/L 167 81 14-17663 25167ND135 105
Phenanthrene ug/L M183.3 69 54-12052 2883.3ND 57.7 43.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92666250
Loves 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4013206MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92665704001
4013207
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol ug/L R183.3 52 5-11236 3883.3ND 43.4 29.6
Pyrene ug/L 83.3 72 52-11562 1583.3ND 60.4 52.1
2,4,6-Tribromophenol (S) %74 10-13748
2-Fluorobiphenyl (S) %58 15-12032
2-Fluorophenol (S) %52 10-12032
Nitrobenzene-d5 (S) %74 10-12043
Phenol-d6 (S) %45 10-12027
Terphenyl-d14 (S) %72 11-13158
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92666250
Loves 412 23004903
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analysis conducted outside the EPA method holding time.H1
Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.H5
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92666250
Loves 412 23004903
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92666250001 773203 77338555234903-160 EPA 625.1 EPA 625.1
92666250001 77605355234903-160 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 21
Page 19 of 21
Page 20 of 21
Page 21 of 21
#=CL#
May 23, 2023
LIMS USE: FR - MARK RYLAND
LIMS OBJECT ID: 92667251
92667251
Project:
Pace Project No.:
RE:
Mark Ryland
Apex Companies, LLC
203 Wylderose Court
Midlothian, VA 23113
LOVES 412 23004903
Dear Mark Ryland:
Enclosed are the analytical results for sample(s) received by the laboratory on May 12, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92667251001 511234903-214 EPA 625.1 58 PASI-CPKS
SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Sample: 511234903-214 Lab ID: 92667251001 Collected: 05/11/23 16:30 Received: 05/12/23 14:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 05/20/23 02:44 83-32-905/16/23 22:0922.7 5
Acenaphthylene ND ug/L 05/20/23 02:44 208-96-805/16/23 22:0922.7 5
Anthracene ND ug/L 05/20/23 02:44 120-12-705/16/23 22:0922.7 5
Benzo(a)anthracene ND ug/L 05/20/23 02:44 56-55-305/16/23 22:0922.7 5
Benzo(a)pyrene ND ug/L 05/20/23 02:44 50-32-805/16/23 22:0922.7 5
Benzo(b)fluoranthene ND ug/L 05/20/23 02:44 205-99-205/16/23 22:0922.7 5
Benzo(g,h,i)perylene ND ug/L 05/20/23 02:44 191-24-205/16/23 22:0922.7 5
Benzo(k)fluoranthene ND ug/L 05/20/23 02:44 207-08-905/16/23 22:0922.7 5
4-Bromophenylphenyl ether ND ug/L 05/20/23 02:44 101-55-305/16/23 22:0922.7 5
Butylbenzylphthalate ND ug/L 05/20/23 02:44 85-68-705/16/23 22:0922.7 5
4-Chloro-3-methylphenol ND ug/L 05/20/23 02:44 59-50-705/16/23 22:0922.7 5
bis(2-Chloroethoxy)methane ND ug/L 05/20/23 02:44 111-91-105/16/23 22:0945.5 5
bis(2-Chloroethyl) ether ND ug/L 05/20/23 02:44 111-44-405/16/23 22:0922.7 5
2-Chloronaphthalene ND ug/L 05/20/23 02:44 91-58-705/16/23 22:0922.7 5
2-Chlorophenol ND ug/L 05/20/23 02:44 95-57-805/16/23 22:0922.7 5
4-Chlorophenylphenyl ether ND ug/L 05/20/23 02:44 7005-72-305/16/23 22:0922.7 5
Chrysene ND ug/L 05/20/23 02:44 218-01-905/16/23 22:0922.7 5
Dibenz(a,h)anthracene ND ug/L 05/20/23 02:44 53-70-305/16/23 22:0922.7 5
3,3'-Dichlorobenzidine ND ug/L 05/20/23 02:44 91-94-105/16/23 22:0945.5 5
2,4-Dichlorophenol ND ug/L 05/20/23 02:44 120-83-205/16/23 22:0922.7 5
Diethylphthalate ND ug/L 05/20/23 02:44 84-66-205/16/23 22:0922.7 5
2,4-Dimethylphenol ND ug/L 05/20/23 02:44 105-67-9 L105/16/23 22:0945.5 5
Dimethylphthalate ND ug/L 05/20/23 02:44 131-11-305/16/23 22:0922.7 5
Di-n-butylphthalate ND ug/L 05/20/23 02:44 84-74-205/16/23 22:0922.7 5
4,6-Dinitro-2-methylphenol ND ug/L 05/20/23 02:44 534-52-105/16/23 22:0945.5 5
2,4-Dinitrophenol ND ug/L 05/20/23 02:44 51-28-505/16/23 22:09227 5
2,4-Dinitrotoluene ND ug/L 05/20/23 02:44 121-14-205/16/23 22:0922.7 5
2,6-Dinitrotoluene ND ug/L 05/20/23 02:44 606-20-205/16/23 22:0922.7 5
Di-n-octylphthalate ND ug/L 05/20/23 02:44 117-84-005/16/23 22:0922.7 5
bis(2-Ethylhexyl)phthalate ND ug/L 05/20/23 02:44 117-81-705/16/23 22:0922.7 5
Fluoranthene ND ug/L 05/20/23 02:44 206-44-005/16/23 22:0922.7 5
Fluorene ND ug/L 05/20/23 02:44 86-73-705/16/23 22:0922.7 5
Hexachloro-1,3-butadiene ND ug/L 05/20/23 02:44 87-68-305/16/23 22:0922.7 5
Hexachlorobenzene ND ug/L 05/20/23 02:44 118-74-105/16/23 22:0922.7 5
Hexachlorocyclopentadiene ND ug/L 05/20/23 02:44 77-47-405/16/23 22:0945.5 5
Hexachloroethane ND ug/L 05/20/23 02:44 67-72-105/16/23 22:0922.7 5
Indeno(1,2,3-cd)pyrene ND ug/L 05/20/23 02:44 193-39-505/16/23 22:0922.7 5
Isophorone ND ug/L 05/20/23 02:44 78-59-105/16/23 22:0945.5 5
Naphthalene ND ug/L 05/20/23 02:44 91-20-305/16/23 22:0922.7 5
Nitrobenzene ND ug/L 05/20/23 02:44 98-95-305/16/23 22:0922.7 5
2-Nitrophenol ND ug/L 05/20/23 02:44 88-75-505/16/23 22:0922.7 5
4-Nitrophenol ND ug/L 05/20/23 02:44 100-02-705/16/23 22:0945.5 5
N-Nitrosodimethylamine ND ug/L 05/20/23 02:44 62-75-905/16/23 22:0922.7 5
N-Nitroso-di-n-propylamine ND ug/L 05/20/23 02:44 621-64-705/16/23 22:0922.7 5
N-Nitrosodiphenylamine ND ug/L 05/20/23 02:44 86-30-605/16/23 22:0945.5 5
2,2'-Oxybis(1-chloropropane) ND ug/L 05/20/23 02:44 108-60-105/16/23 22:0922.7 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Sample: 511234903-214 Lab ID: 92667251001 Collected: 05/11/23 16:30 Received: 05/12/23 14:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Pentachlorophenol ND ug/L 05/20/23 02:44 87-86-505/16/23 22:0945.5 5
Phenanthrene ND ug/L 05/20/23 02:44 85-01-805/16/23 22:0922.7 5
Phenol ND ug/L 05/20/23 02:44 108-95-205/16/23 22:0922.7 5
Pyrene ND ug/L 05/20/23 02:44 129-00-005/16/23 22:0922.7 5
1,2,4-Trichlorobenzene ND ug/L 05/20/23 02:44 120-82-1 L205/16/23 22:0922.7 5
2,4,6-Trichlorophenol ND ug/L 05/20/23 02:44 88-06-205/16/23 22:0945.5 5
Surrogates
Nitrobenzene-d5 (S) 59 %05/20/23 02:44 4165-60-0 D305/16/23 22:0910-120 5
2-Fluorobiphenyl (S) 45 %05/20/23 02:44 321-60-805/16/23 22:0915-120 5
Terphenyl-d14 (S) 75 %05/20/23 02:44 1718-51-005/16/23 22:0911-131 5
Phenol-d6 (S) 34 %05/20/23 02:44 13127-88-305/16/23 22:0910-120 5
2-Fluorophenol (S) 48 %05/20/23 02:44 367-12-405/16/23 22:0910-120 5
2,4,6-Tribromophenol (S) 88 %05/20/23 02:44 118-79-605/16/23 22:0910-137 5
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 1.7 ug/L 05/23/23 02:17 71-43-20.50 1
Bromobenzene ND ug/L 05/23/23 02:17 108-86-10.50 1
Bromochloromethane ND ug/L 05/23/23 02:17 74-97-50.50 1
Bromodichloromethane ND ug/L 05/23/23 02:17 75-27-40.50 1
Bromoform ND ug/L 05/23/23 02:17 75-25-20.50 1
Bromomethane ND ug/L 05/23/23 02:17 74-83-95.0 1
n-Butylbenzene ND ug/L 05/23/23 02:17 104-51-80.50 1
sec-Butylbenzene ND ug/L 05/23/23 02:17 135-98-80.50 1
tert-Butylbenzene ND ug/L 05/23/23 02:17 98-06-60.50 1
Carbon tetrachloride ND ug/L 05/23/23 02:17 56-23-50.50 1
Chlorobenzene ND ug/L 05/23/23 02:17 108-90-70.50 1
Chloroethane ND ug/L 05/23/23 02:17 75-00-3 L11.0 1
Chloroform ND ug/L 05/23/23 02:17 67-66-30.50 1
Chloromethane ND ug/L 05/23/23 02:17 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/23/23 02:17 95-49-80.50 1
4-Chlorotoluene ND ug/L 05/23/23 02:17 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 05/23/23 02:17 96-12-81.0 1
Dibromochloromethane ND ug/L 05/23/23 02:17 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 05/23/23 02:17 106-93-40.50 1
Dibromomethane ND ug/L 05/23/23 02:17 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 05/23/23 02:17 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 05/23/23 02:17 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 05/23/23 02:17 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 05/23/23 02:17 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 05/23/23 02:17 75-34-30.50 1
1,2-Dichloroethane ND ug/L 05/23/23 02:17 107-06-20.50 1
1,1-Dichloroethene ND ug/L 05/23/23 02:17 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 05/23/23 02:17 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 05/23/23 02:17 156-60-50.50 1
1,2-Dichloropropane ND ug/L 05/23/23 02:17 78-87-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Sample: 511234903-214 Lab ID: 92667251001 Collected: 05/11/23 16:30 Received: 05/12/23 14:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,3-Dichloropropane ND ug/L 05/23/23 02:17 142-28-90.50 1
2,2-Dichloropropane ND ug/L 05/23/23 02:17 594-20-70.50 1
1,1-Dichloropropene ND ug/L 05/23/23 02:17 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 05/23/23 02:17 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 05/23/23 02:17 10061-02-60.50 1
Diisopropyl ether ND ug/L 05/23/23 02:17 108-20-30.50 1
Ethylbenzene 1.0 ug/L 05/23/23 02:17 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 05/23/23 02:17 87-68-32.0 1
Isopropylbenzene (Cumene)1.3 ug/L 05/23/23 02:17 98-82-80.50 1
Methylene Chloride ND ug/L 05/23/23 02:17 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 05/23/23 02:17 1634-04-40.50 1
Naphthalene 13.6 ug/L 05/23/23 02:17 91-20-32.0 1
n-Propylbenzene 2.2 ug/L 05/23/23 02:17 103-65-10.50 1
Styrene ND ug/L 05/23/23 02:17 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 05/23/23 02:17 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 05/23/23 02:17 79-34-50.50 1
Tetrachloroethene ND ug/L 05/23/23 02:17 127-18-40.50 1
Toluene ND ug/L 05/23/23 02:17 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 05/23/23 02:17 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 05/23/23 02:17 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 05/23/23 02:17 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 05/23/23 02:17 79-00-50.50 1
Trichloroethene ND ug/L 05/23/23 02:17 79-01-60.50 1
Trichlorofluoromethane ND ug/L 05/23/23 02:17 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/23/23 02:17 96-18-40.50 1
1,2,4-Trimethylbenzene 3.6 ug/L 05/23/23 02:17 95-63-60.50 1
1,3,5-Trimethylbenzene 4.2 ug/L 05/23/23 02:17 108-67-80.50 1
Vinyl chloride ND ug/L 05/23/23 02:17 75-01-41.0 1
m&p-Xylene ND ug/L 05/23/23 02:17 179601-23-11.0 1
o-Xylene 1.4 ug/L 05/23/23 02:17 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 121 %05/23/23 02:17 17060-07-070-130 1
4-Bromofluorobenzene (S) 99 %05/23/23 02:17 460-00-470-130 1
Toluene-d8 (S) 103 %05/23/23 02:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
776135
SM 6200B
SM 6200B
6200B MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92667251001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4026978
Associated Lab Samples:92667251001
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/22/23 23:37
1,1,1-Trichloroethane ug/L ND 0.50 05/22/23 23:37
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/22/23 23:37
1,1,2-Trichloroethane ug/L ND 0.50 05/22/23 23:37
1,1-Dichloroethane ug/L ND 0.50 05/22/23 23:37
1,1-Dichloroethene ug/L ND 0.50 05/22/23 23:37
1,1-Dichloropropene ug/L ND 0.50 05/22/23 23:37
1,2,3-Trichlorobenzene ug/L ND 2.0 05/22/23 23:37
1,2,3-Trichloropropane ug/L ND 0.50 05/22/23 23:37
1,2,4-Trichlorobenzene ug/L ND 2.0 05/22/23 23:37
1,2,4-Trimethylbenzene ug/L ND 0.50 05/22/23 23:37
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/22/23 23:37
1,2-Dibromoethane (EDB) ug/L ND 0.50 05/22/23 23:37
1,2-Dichlorobenzene ug/L ND 0.50 05/22/23 23:37
1,2-Dichloroethane ug/L ND 0.50 05/22/23 23:37
1,2-Dichloropropane ug/L ND 0.50 05/22/23 23:37
1,3,5-Trimethylbenzene ug/L ND 0.50 05/22/23 23:37
1,3-Dichlorobenzene ug/L ND 0.50 05/22/23 23:37
1,3-Dichloropropane ug/L ND 0.50 05/22/23 23:37
1,4-Dichlorobenzene ug/L ND 0.50 05/22/23 23:37
2,2-Dichloropropane ug/L ND 0.50 05/22/23 23:37
2-Chlorotoluene ug/L ND 0.50 05/22/23 23:37
4-Chlorotoluene ug/L ND 0.50 05/22/23 23:37
Benzene ug/L ND 0.50 05/22/23 23:37
Bromobenzene ug/L ND 0.50 05/22/23 23:37
Bromochloromethane ug/L ND 0.50 05/22/23 23:37
Bromodichloromethane ug/L ND 0.50 05/22/23 23:37
Bromoform ug/L ND 0.50 05/22/23 23:37
Bromomethane ug/L ND 5.0 05/22/23 23:37
Carbon tetrachloride ug/L ND 0.50 05/22/23 23:37
Chlorobenzene ug/L ND 0.50 05/22/23 23:37
Chloroethane ug/L ND 1.0 05/22/23 23:37
Chloroform ug/L ND 0.50 05/22/23 23:37
Chloromethane ug/L ND 1.0 05/22/23 23:37
cis-1,2-Dichloroethene ug/L ND 0.50 05/22/23 23:37
cis-1,3-Dichloropropene ug/L ND 0.50 05/22/23 23:37
Dibromochloromethane ug/L ND 0.50 05/22/23 23:37
Dibromomethane ug/L ND 0.50 05/22/23 23:37
Dichlorodifluoromethane ug/L ND 0.50 IH05/22/23 23:37
Diisopropyl ether ug/L ND 0.50 05/22/23 23:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4026978
Associated Lab Samples:92667251001
Matrix: Water
Analyzed
Ethylbenzene ug/L ND 0.50 05/22/23 23:37
Hexachloro-1,3-butadiene ug/L ND 2.0 05/22/23 23:37
Isopropylbenzene (Cumene) ug/L ND 0.50 05/22/23 23:37
m&p-Xylene ug/L ND 1.0 05/22/23 23:37
Methyl-tert-butyl ether ug/L ND 0.50 05/22/23 23:37
Methylene Chloride ug/L 2.0 2.0 05/22/23 23:37
n-Butylbenzene ug/L ND 0.50 05/22/23 23:37
n-Propylbenzene ug/L ND 0.50 05/22/23 23:37
Naphthalene ug/L ND 2.0 05/22/23 23:37
o-Xylene ug/L ND 0.50 05/22/23 23:37
sec-Butylbenzene ug/L ND 0.50 05/22/23 23:37
Styrene ug/L ND 0.50 05/22/23 23:37
tert-Butylbenzene ug/L ND 0.50 05/22/23 23:37
Tetrachloroethene ug/L ND 0.50 05/22/23 23:37
Toluene ug/L ND 0.50 05/22/23 23:37
trans-1,2-Dichloroethene ug/L ND 0.50 05/22/23 23:37
trans-1,3-Dichloropropene ug/L ND 0.50 05/22/23 23:37
Trichloroethene ug/L ND 0.50 05/22/23 23:37
Trichlorofluoromethane ug/L ND 1.0 05/22/23 23:37
Vinyl chloride ug/L ND 1.0 05/22/23 23:37
1,2-Dichloroethane-d4 (S) % 121 70-130 05/22/23 23:37
4-Bromofluorobenzene (S) % 97 70-130 05/22/23 23:37
Toluene-d8 (S) % 104 70-130 05/22/23 23:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026979LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.820 99 60-140
1,1,1-Trichloroethane ug/L 22.420 112 60-140
1,1,2,2-Tetrachloroethane ug/L 22.620 113 60-140
1,1,2-Trichloroethane ug/L 21.120 105 60-140
1,1-Dichloroethane ug/L 25.420 127 60-140
1,1-Dichloroethene ug/L 24.620 123 60-140
1,1-Dichloropropene ug/L 25.820 129 60-140
1,2,3-Trichlorobenzene ug/L 16.920 84 60-140
1,2,3-Trichloropropane ug/L 21.720 109 60-140
1,2,4-Trichlorobenzene ug/L 17.520 87 60-140
1,2,4-Trimethylbenzene ug/L 21.420 107 60-140
1,2-Dibromo-3-chloropropane ug/L 16.620 83 60-140
1,2-Dibromoethane (EDB) ug/L 21.420 107 60-140
1,2-Dichlorobenzene ug/L 20.320 101 60-140
1,2-Dichloroethane ug/L 24.520 123 60-140
1,2-Dichloropropane ug/L 23.120 116 60-140
1,3,5-Trimethylbenzene ug/L 21.720 108 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026979LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 20.720 103 60-140
1,3-Dichloropropane ug/L 21.920 110 60-140
1,4-Dichlorobenzene ug/L 20.020 100 60-140
2,2-Dichloropropane ug/L 22.120 111 60-140
2-Chlorotoluene ug/L 22.320 111 60-140
4-Chlorotoluene ug/L 22.820 114 60-140
Benzene ug/L 22.420 112 60-140
Bromobenzene ug/L 20.120 100 60-140
Bromochloromethane ug/L 22.520 112 60-140
Bromodichloromethane ug/L 19.920 99 60-140
Bromoform ug/L 14.920 74 60-140
Bromomethane ug/L 23.120 115 60-140
Carbon tetrachloride ug/L 18.620 93 60-140
Chlorobenzene ug/L 21.520 108 60-140
Chloroethane ug/L 35.8 L120 179 60-140
Chloroform ug/L 24.220 121 60-140
Chloromethane ug/L 27.820 139 60-140
cis-1,2-Dichloroethene ug/L 24.120 121 60-140
cis-1,3-Dichloropropene ug/L 20.420 102 60-140
Dibromochloromethane ug/L 18.420 92 60-140
Dibromomethane ug/L 18.920 94 60-140
Dichlorodifluoromethane ug/L 34.4 IH,L120 172 60-140
Diisopropyl ether ug/L 23.120 115 60-140
Ethylbenzene ug/L 21.420 107 60-140
Hexachloro-1,3-butadiene ug/L 17.020 85 60-140
Isopropylbenzene (Cumene) ug/L 20.720 103 60-140
m&p-Xylene ug/L 42.240 105 60-140
Methyl-tert-butyl ether ug/L 21.420 107 60-140
Methylene Chloride ug/L 23.720 119 60-140
n-Butylbenzene ug/L 21.920 110 60-140
n-Propylbenzene ug/L 22.020 110 60-140
Naphthalene ug/L 20.120 100 60-140
o-Xylene ug/L 20.820 104 60-140
sec-Butylbenzene ug/L 21.320 106 60-140
Styrene ug/L 21.220 106 60-140
tert-Butylbenzene ug/L 17.420 87 60-140
Tetrachloroethene ug/L 18.220 91 60-140
Toluene ug/L 20.520 102 60-140
trans-1,2-Dichloroethene ug/L 25.420 127 60-140
trans-1,3-Dichloropropene ug/L 19.120 95 60-140
Trichloroethene ug/L 20.920 105 60-140
Trichlorofluoromethane ug/L 23.120 116 60-140
Vinyl chloride ug/L 21.920 109 60-140
1,2-Dichloroethane-d4 (S) %117 70-130
4-Bromofluorobenzene (S) %101 70-130
Toluene-d8 (S) %102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026980MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667997002
4026981
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 109 60-140120 1020<0.31 21.9 24.0
1,1,1-Trichloroethane ug/L M120131 60-140142 920<0.33 26.1 28.4
1,1,2,2-Tetrachloroethane ug/L 20 116 60-140129 1120<0.22 23.2 25.8
1,1,2-Trichloroethane ug/L 20 114 60-140122 720<0.32 22.9 24.4
1,1-Dichloroethane ug/L M120146 60-140157 720<0.37 29.3 31.5
1,1-Dichloroethene ug/L M120143 60-140156 920<0.35 28.6 31.1
1,1-Dichloropropene ug/L M120151 60-140165 920<0.43 30.3 33.0
1,2,3-Trichlorobenzene ug/L 20 92 60-14097 520<0.81 18.4 19.5
1,2,3-Trichloropropane ug/L 20 111 60-140125 1220<0.26 22.2 25.0
1,2,4-Trichlorobenzene ug/L 20 98 60-140104 620<0.64 19.5 20.7
1,2,4-Trimethylbenzene ug/L 20 117 60-140128 820<0.50 23.5 25.5
1,2-Dibromo-3-chloropropane ug/L 20 87 60-14098 1220<0.34 17.4 19.6
1,2-Dibromoethane (EDB) ug/L 20 114 60-140125 920<0.27 22.8 25.0
1,2-Dichlorobenzene ug/L 20 108 60-140117 820<0.34 21.6 23.5
1,2-Dichloroethane ug/L M120133 60-140145 920<0.32 26.6 29.0
1,2-Dichloropropane ug/L M120130 60-140141 820<0.36 26.0 28.2
1,3,5-Trimethylbenzene ug/L 20 118 60-140129 920<0.33 23.7 25.8
1,3-Dichlorobenzene ug/L 20 114 60-140122 620<0.34 22.8 24.3
1,3-Dichloropropane ug/L 20 119 60-140131 920<0.28 23.8 26.1
1,4-Dichlorobenzene ug/L 20 107 60-140118 1020<0.33 21.3 23.5
2,2-Dichloropropane ug/L M120142 60-140154 820<0.39 28.4 30.8
2-Chlorotoluene ug/L 20 123 60-140134 920<0.32 24.5 26.8
4-Chlorotoluene ug/L 20 124 60-140134 820<0.32 24.9 26.8
Benzene ug/L 20 125 60-140134 720<0.34 25.0 26.8
Bromobenzene ug/L 20 110 60-140119 920<0.29 21.9 23.9
Bromochloromethane ug/L 20 123 60-140131 620<0.47 24.6 26.2
Bromodichloromethane ug/L 20 110 60-140118 720<0.31 22.0 23.6
Bromoform ug/L 20 79 60-14090 1220<0.34 15.9 17.9
Bromomethane ug/L 20 127 60-140134 620<1.7 25.3 26.9
Carbon tetrachloride ug/L 20 110 60-140119 820<0.33 22.0 23.7
Chlorobenzene ug/L 20 116 60-140127 920<0.28 23.3 25.5
Chloroethane ug/L M020187 60-140208 1020<0.65 37.5 41.5
Chloroform ug/L M120133 60-140142 620<0.43 26.7 28.4
Chloromethane ug/L M120159 60-140173 820<0.54 31.9 34.5
cis-1,2-Dichloroethene ug/L M120142 60-140151 620<0.38 28.3 30.1
cis-1,3-Dichloropropene ug/L 20 112 60-140119 620<0.36 22.4 23.8
Dibromochloromethane ug/L 20 102 60-140110 820<0.36 20.3 22.0
Dibromomethane ug/L 20 101 60-140110 820<0.39 20.3 21.9
Dichlorodifluoromethane ug/L IH,M020188 60-140200 620<0.35 37.6 40.1
Diisopropyl ether ug/L 20 127 60-140140 1020<0.31 25.4 28.0
Ethylbenzene ug/L 20 119 60-140130 1020<0.30 23.7 26.1
Hexachloro-1,3-butadiene ug/L 20 99 60-140107 820<1.5 19.8 21.5
Isopropylbenzene (Cumene) ug/L 20 116 60-140128 1020<0.33 23.2 25.7
m&p-Xylene ug/L 40 116 60-140128 1040<0.71 46.5 51.2
Methyl-tert-butyl ether ug/L 20 116 60-140127 920<0.42 23.2 25.4
Methylene Chloride ug/L 20 122 60-140133 920<2.0 24.4 26.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026980MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667997002
4026981
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 127 60-140137 820<0.49 25.4 27.5
n-Propylbenzene ug/L 20 124 60-140135 820<0.34 24.8 26.9
Naphthalene ug/L 20 110 60-140118 720<0.64 21.9 23.6
o-Xylene ug/L 20 113 60-140122 820<0.34 22.5 24.4
sec-Butylbenzene ug/L 20 121 60-140133 920<0.40 24.3 26.5
Styrene ug/L 20 115 60-140127 920<0.29 23.1 25.4
tert-Butylbenzene ug/L 20 98 60-140106 820<0.32 19.6 21.2
Tetrachloroethene ug/L 20 102 60-140113 1020<0.29 20.4 22.6
Toluene ug/L 20 112 60-140122 820<0.24 22.5 24.4
trans-1,2-Dichloroethene ug/L M120149 60-140162 820<0.40 29.8 32.3
trans-1,3-Dichloropropene ug/L 20 109 60-140116 620<0.36 21.7 23.1
Trichloroethene ug/L 20 119 60-140129 820<0.38 23.7 25.8
Trichlorofluoromethane ug/L M120134 60-140147 920<0.30 26.9 29.5
Vinyl chloride ug/L 20 124 60-140135 820<0.39 24.8 27.0
1,2-Dichloroethane-d4 (S) %119 70-130119
4-Bromofluorobenzene (S) %101 70-130103
Toluene-d8 (S) %99 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
774864
EPA 625.1
EPA 625.1
625 MSS
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92667251001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4021275
Associated Lab Samples:92667251001
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 05/17/23 12:02
2,2'-Oxybis(1-chloropropane) ug/L ND 5.0 05/17/23 12:02
2,4,6-Trichlorophenol ug/L ND 10.0 05/17/23 12:02
2,4-Dichlorophenol ug/L ND 5.0 05/17/23 12:02
2,4-Dimethylphenol ug/L ND 10.0 05/17/23 12:02
2,4-Dinitrophenol ug/L ND 50.0 05/17/23 12:02
2,4-Dinitrotoluene ug/L ND 5.0 05/17/23 12:02
2,6-Dinitrotoluene ug/L ND 5.0 05/17/23 12:02
2-Chloronaphthalene ug/L ND 5.0 05/17/23 12:02
2-Chlorophenol ug/L ND 5.0 05/17/23 12:02
2-Nitrophenol ug/L ND 5.0 05/17/23 12:02
3,3'-Dichlorobenzidine ug/L ND 10.0 05/17/23 12:02
4,6-Dinitro-2-methylphenol ug/L ND 10.0 05/17/23 12:02
4-Bromophenylphenyl ether ug/L ND 5.0 05/17/23 12:02
4-Chloro-3-methylphenol ug/L ND 5.0 05/17/23 12:02
4-Chlorophenylphenyl ether ug/L ND 5.0 05/17/23 12:02
4-Nitrophenol ug/L ND 10.0 05/17/23 12:02
Acenaphthene ug/L ND 5.0 05/17/23 12:02
Acenaphthylene ug/L ND 5.0 05/17/23 12:02
Anthracene ug/L ND 5.0 05/17/23 12:02
Benzo(a)anthracene ug/L ND 5.0 05/17/23 12:02
Benzo(a)pyrene ug/L ND 5.0 05/17/23 12:02
Benzo(b)fluoranthene ug/L ND 5.0 05/17/23 12:02
Benzo(g,h,i)perylene ug/L ND 5.0 05/17/23 12:02
Benzo(k)fluoranthene ug/L ND 5.0 05/17/23 12:02
bis(2-Chloroethoxy)methane ug/L ND 10.0 05/17/23 12:02
bis(2-Chloroethyl) ether ug/L ND 5.0 05/17/23 12:02
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 05/17/23 12:02
Butylbenzylphthalate ug/L ND 5.0 05/17/23 12:02
Chrysene ug/L ND 5.0 05/17/23 12:02
Di-n-butylphthalate ug/L ND 5.0 05/17/23 12:02
Di-n-octylphthalate ug/L ND 5.0 05/17/23 12:02
Dibenz(a,h)anthracene ug/L ND 5.0 05/17/23 12:02
Diethylphthalate ug/L ND 5.0 05/17/23 12:02
Dimethylphthalate ug/L ND 5.0 05/17/23 12:02
Fluoranthene ug/L ND 5.0 05/17/23 12:02
Fluorene ug/L ND 5.0 05/17/23 12:02
Hexachloro-1,3-butadiene ug/L ND 5.0 05/17/23 12:02
Hexachlorobenzene ug/L ND 5.0 05/17/23 12:02
Hexachlorocyclopentadiene ug/L ND 10.0 05/17/23 12:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4021275
Associated Lab Samples:92667251001
Matrix: Water
Analyzed
Hexachloroethane ug/L ND 5.0 05/17/23 12:02
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 05/17/23 12:02
Isophorone ug/L ND 10.0 05/17/23 12:02
N-Nitroso-di-n-propylamine ug/L ND 5.0 05/17/23 12:02
N-Nitrosodimethylamine ug/L ND 5.0 05/17/23 12:02
N-Nitrosodiphenylamine ug/L ND 10.0 05/17/23 12:02
Naphthalene ug/L ND 5.0 05/17/23 12:02
Nitrobenzene ug/L ND 5.0 05/17/23 12:02
Pentachlorophenol ug/L ND 10.0 05/17/23 12:02
Phenanthrene ug/L ND 5.0 05/17/23 12:02
Phenol ug/L ND 5.0 05/17/23 12:02
Pyrene ug/L ND 5.0 05/17/23 12:02
2,4,6-Tribromophenol (S) % 89 10-137 05/17/23 12:02
2-Fluorobiphenyl (S) % 56 15-120 05/17/23 12:02
2-Fluorophenol (S) % 61 10-120 05/17/23 12:02
Nitrobenzene-d5 (S) % 77 10-120 05/17/23 12:02
Phenol-d6 (S) % 51 10-120 05/17/23 12:02
Terphenyl-d14 (S) % 99 11-131 05/17/23 12:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4021276LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 21.5 L250 43 44-142
2,2'-Oxybis(1-chloropropane) ug/L 44.450 89 36-166
2,4,6-Trichlorophenol ug/L 54.450 109 37-144
2,4-Dichlorophenol ug/L 48.550 97 1-191
2,4-Dimethylphenol ug/L 84.3 L150 169 32-119
2,4-Dinitrophenol ug/L 325250 130 1-181
2,4-Dinitrotoluene ug/L 59.350 119 39-139
2,6-Dinitrotoluene ug/L 57.550 115 50-158
2-Chloronaphthalene ug/L 33.150 66 60-118
2-Chlorophenol ug/L 50.550 101 23-134
2-Nitrophenol ug/L 50.350 101 29-182
3,3'-Dichlorobenzidine ug/L 99.1100 99 1-262
4,6-Dinitro-2-methylphenol ug/L 124100 124 1-181
4-Bromophenylphenyl ether ug/L 48.250 96 53-127
4-Chloro-3-methylphenol ug/L 105100 105 22-147
4-Chlorophenylphenyl ether ug/L 44.050 88 25-158
4-Nitrophenol ug/L 190250 76 1-132
Acenaphthene ug/L 42.750 85 47-145
Acenaphthylene ug/L 41.950 84 33-145
Anthracene ug/L 46.150 92 1-166
Benzo(a)anthracene ug/L 50.550 101 33-143
Benzo(a)pyrene ug/L 50.150 100 17-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4021276LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 51.050 102 24-159
Benzo(g,h,i)perylene ug/L 49.950 100 1-219
Benzo(k)fluoranthene ug/L 50.350 101 11-162
bis(2-Chloroethoxy)methane ug/L 47.350 95 33-184
bis(2-Chloroethyl) ether ug/L 48.250 96 12-158
bis(2-Ethylhexyl)phthalate ug/L 58.850 118 8-158
Butylbenzylphthalate ug/L 59.850 120 1-152
Chrysene ug/L 49.950 100 17-168
Di-n-butylphthalate ug/L 53.950 108 1-118
Di-n-octylphthalate ug/L 60.550 121 4-146
Dibenz(a,h)anthracene ug/L 49.750 99 1-227
Diethylphthalate ug/L 55.650 111 1-114
Dimethylphthalate ug/L 53.050 106 1-112
Fluoranthene ug/L 50.750 101 26-137
Fluorene ug/L 48.950 98 59-121
Hexachloro-1,3-butadiene ug/L 20.050 40 24-116
Hexachlorobenzene ug/L 47.050 94 1-152
Hexachlorocyclopentadiene ug/L 20.350 41 25-150
Hexachloroethane ug/L 22.050 44 40-113
Indeno(1,2,3-cd)pyrene ug/L 51.050 102 1-171
Isophorone ug/L 52.050 104 21-196
N-Nitroso-di-n-propylamine ug/L 53.350 107 1-230
N-Nitrosodimethylamine ug/L 44.350 89 25-150
N-Nitrosodiphenylamine ug/L 49.950 100 25-150
Naphthalene ug/L 26.450 53 21-133
Nitrobenzene ug/L 44.550 89 35-180
Pentachlorophenol ug/L 104100 104 14-176
Phenanthrene ug/L 50.350 101 54-120
Phenol ug/L 36.050 72 5-112
Pyrene ug/L 50.450 101 52-115
2,4,6-Tribromophenol (S) %102 10-137
2-Fluorobiphenyl (S) %71 15-120
2-Fluorophenol (S) %75 10-120
Nitrobenzene-d5 (S) %86 10-120
Phenol-d6 (S) %61 10-120
Terphenyl-d14 (S) %98 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4021277MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35798781001
4021278
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L M05024 44-14222 7501.7U 11.8 11.0
2,2'-Oxybis(1-chloropropane) ug/L 50 63 36-16650 24501.2U 31.7 25.0
2,4,6-Trichlorophenol ug/L M15065 37-1449501.6U 32.6 4.5J
2,4-Dichlorophenol ug/L R15068 1-19128 82501.4U 34.0 14.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4021277MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35798781001
4021278
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4-Dimethylphenol ug/L M050120 32-11999 19501.7U 60.2 49.6
2,4-Dinitrophenol ug/L M12503 1-181025026.0U ND ND
2,4-Dinitrotoluene ug/L 50 89 39-13977 14501.6U 44.5 38.6
2,6-Dinitrotoluene ug/L 50 84 50-15876 11501.7U 42.2 37.8
2-Chloronaphthalene ug/L M15046 60-11835 27501.7U 23.2 17.7
2-Chlorophenol ug/L R15069 23-13432 74501.2U 34.4 15.9
2-Nitrophenol ug/L M1,R15071 29-18228 87501.4U 35.7 14.0
3,3'-Dichlorobenzidine ug/L 100 97 1-26282 171008.1U 97.3 82.3
4,6-Dinitro-2-methylphenol ug/L M110027 1-18101007.8U 27.5 ND
4-Bromophenylphenyl ether ug/L 50 78 53-12765 18501.8U 39.1 32.7
4-Chloro-3-methylphenol ug/L 100 73 22-14765 121003.3U 73.1 64.6
4-Chlorophenylphenyl ether ug/L 50 64 25-15854 16502.0U 32.1 27.2
4-Nitrophenol ug/L M125017 1-13202506.6U 41.9 ND
Acenaphthene ug/L M15057 47-14546 23502.0U 28.7 22.8
Acenaphthylene ug/L 50 58 33-14545 26502.0U 29.2 22.5
Anthracene ug/L 50 82 1-16674 10502.3U 40.8 36.9
Benzo(a)anthracene ug/L 50 100 33-14386 15502.7U 50.0 42.8
Benzo(a)pyrene ug/L 50 94 17-16379 18502.8U 47.0 39.4
Benzo(b)fluoranthene ug/L 50 95 24-15979 18502.6U 47.3 39.7
Benzo(g,h,i)perylene ug/L 50 92 1-21981 13502.8U 45.8 40.4
Benzo(k)fluoranthene ug/L 50 93 11-16279 16502.7U 46.6 39.6
bis(2-Chloroethoxy)methane ug/L 50 66 33-18454 21501.8U 33.2 26.9
bis(2-Chloroethyl) ether ug/L 50 69 12-15856 20501.9U 34.5 28.2
bis(2-Ethylhexyl)phthalate ug/L 50 111 8-15892 18503.7U 55.3 46.2
Butylbenzylphthalate ug/L 50 109 1-15294 15503.1U 54.4 46.8
Chrysene ug/L 50 97 17-16886 12502.8U 48.7 43.1
Di-n-butylphthalate ug/L 50 99 1-11889 12502.2U 49.7 44.3
Di-n-octylphthalate ug/L 50 118 4-14697 20503.9U 58.9 48.3
Dibenz(a,h)anthracene ug/L 50 95 1-22780 18503.0U 47.6 39.8
Diethylphthalate ug/L 50 89 1-11478 14502.0U 44.6 38.8
Dimethylphthalate ug/L 50 81 1-11267 19502.1U 40.6 33.6
Fluoranthene ug/L 50 98 26-13788 10502.2U 48.8 44.2
Fluorene ug/L M15069 59-12158 17502.1U 34.6 29.2
Hexachloro-1,3-butadiene ug/L M15017 24-11620 12501.8U 8.7 9.8
Hexachlorobenzene ug/L 50 81 1-15271 13502.2U 40.4 35.3
Hexachlorocyclopentadiene ug/L M15018 25-15015501.6U 9.1J 7.3J
Hexachloroethane ug/L M15020 40-11322 8501.4U 10.1 10.9
Indeno(1,2,3-cd)pyrene ug/L 50 95 1-17179 18502.9U 47.5 39.7
Isophorone ug/L 50 70 21-19657 21501.7U 35.1 28.3
N-Nitroso-di-n-propylamine ug/L 50 71 1-23059 19501.3U 35.6 29.3
N-Nitrosodimethylamine ug/L 50 66 25-15054 19501.9U 32.9 27.2
N-Nitrosodiphenylamine ug/L 50 84 25-15074 13503.0U 42.2 37.0
Naphthalene ug/L 50 33 21-13328 18502.1U 16.6 13.9
Nitrobenzene ug/L 50 66 35-18052 23501.9U 32.9 26.1
Pentachlorophenol ug/L M110064 14-17631003.8U 63.5 ND
Phenanthrene ug/L 50 87 54-12077 12502.0U 43.4 38.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
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Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4021277MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35798781001
4021278
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol ug/L R15050 5-11235 35501.4U 25.0 17.7
Pyrene ug/L 50 95 52-11583 13502.2U 47.6 41.7
2,4,6-Tribromophenol (S) %86 10-13722
2-Fluorobiphenyl (S) %51 15-12040
2-Fluorophenol (S) %49 10-12011
Nitrobenzene-d5 (S) %66 10-12051
Phenol-d6 (S) %43 10-12027
Terphenyl-d14 (S) %93 11-13177
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
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[phone]
Page 16 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92667251
LOVES 412 23004903
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
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[phone]
Page 17 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92667251
LOVES 412 23004903
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92667251001 774864 775032511234903-214 EPA 625.1 EPA 625.1
92667251001 776135511234903-214 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 03:49 PM
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[phone]
Page 18 of 21
Page 19 of 21
Page 20 of 21
Page 21 of 21
#=CL#
June 07, 2023
LIMS USE: FR - MARK RYLAND
LIMS OBJECT ID: 92667253
92667253
Project:
Pace Project No.:
RE:
Mark Ryland
Apex Companies, LLC
203 Wylderose Court
Midlothian, VA 23113
LOVES 412 23004903
Dear Mark Ryland:
Enclosed are the analytical results for sample(s) received by the laboratory on May 12, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
Pace Analytical Services - Charlotte
A revised report is being submitted on 6/7/23 to update the project name.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
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[phone]
Page 1 of 70
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 70
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92667253001 512234903-216 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92667253002 512234903-217 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92667253003 512234903-218 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92667253004 512234903-219 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92667253005 512234903-220 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92667253006 512234903-221 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92667253007 512234903-222 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92667253008 512234903-223 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-216 Lab ID: 92667253001 Collected: 05/12/23 08:25 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/17/23 11:39 83-32-905/16/23 14:28389 1
Acenaphthylene ND ug/kg 05/17/23 11:39 208-96-805/16/23 14:28389 1
Aniline ND ug/kg 05/17/23 11:39 62-53-305/16/23 14:28389 1
Anthracene ND ug/kg 05/17/23 11:39 120-12-705/16/23 14:28389 1
Benzo(a)anthracene ND ug/kg 05/17/23 11:39 56-55-305/16/23 14:28389 1
Benzo(a)pyrene ND ug/kg 05/17/23 11:39 50-32-805/16/23 14:28389 1
Benzo(b)fluoranthene ND ug/kg 05/17/23 11:39 205-99-205/16/23 14:28389 1
Benzo(g,h,i)perylene ND ug/kg 05/17/23 11:39 191-24-205/16/23 14:28389 1
Benzo(k)fluoranthene ND ug/kg 05/17/23 11:39 207-08-905/16/23 14:28389 1
Benzoic Acid ND ug/kg 05/17/23 11:39 65-85-005/16/23 14:281950 1
Benzyl alcohol ND ug/kg 05/17/23 11:39 100-51-605/16/23 14:28778 1
4-Bromophenylphenyl ether ND ug/kg 05/17/23 11:39 101-55-305/16/23 14:28389 1
Butylbenzylphthalate ND ug/kg 05/17/23 11:39 85-68-705/16/23 14:28389 1
4-Chloro-3-methylphenol ND ug/kg 05/17/23 11:39 59-50-705/16/23 14:28778 1
4-Chloroaniline ND ug/kg 05/17/23 11:39 106-47-805/16/23 14:28778 1
bis(2-Chloroethoxy)methane ND ug/kg 05/17/23 11:39 111-91-105/16/23 14:28389 1
bis(2-Chloroethyl) ether ND ug/kg 05/17/23 11:39 111-44-405/16/23 14:28389 1
2-Chloronaphthalene ND ug/kg 05/17/23 11:39 91-58-705/16/23 14:28389 1
2-Chlorophenol ND ug/kg 05/17/23 11:39 95-57-805/16/23 14:28389 1
4-Chlorophenylphenyl ether ND ug/kg 05/17/23 11:39 7005-72-305/16/23 14:28389 1
Chrysene ND ug/kg 05/17/23 11:39 218-01-905/16/23 14:28389 1
Dibenz(a,h)anthracene ND ug/kg 05/17/23 11:39 53-70-305/16/23 14:28389 1
Dibenzofuran ND ug/kg 05/17/23 11:39 132-64-905/16/23 14:28389 1
1,2-Dichlorobenzene ND ug/kg 05/17/23 11:39 95-50-105/16/23 14:28389 1
1,3-Dichlorobenzene ND ug/kg 05/17/23 11:39 541-73-105/16/23 14:28389 1
1,4-Dichlorobenzene ND ug/kg 05/17/23 11:39 106-46-705/16/23 14:28389 1
3,3'-Dichlorobenzidine ND ug/kg 05/17/23 11:39 91-94-105/16/23 14:28778 1
2,4-Dichlorophenol ND ug/kg 05/17/23 11:39 120-83-205/16/23 14:28389 1
Diethylphthalate ND ug/kg 05/17/23 11:39 84-66-205/16/23 14:28389 1
2,4-Dimethylphenol ND ug/kg 05/17/23 11:39 105-67-905/16/23 14:28389 1
Dimethylphthalate ND ug/kg 05/17/23 11:39 131-11-305/16/23 14:28389 1
Di-n-butylphthalate ND ug/kg 05/17/23 11:39 84-74-205/16/23 14:28389 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/23 11:39 534-52-105/16/23 14:28778 1
2,4-Dinitrophenol ND ug/kg 05/17/23 11:39 51-28-505/16/23 14:281950 1
2,4-Dinitrotoluene ND ug/kg 05/17/23 11:39 121-14-205/16/23 14:28389 1
2,6-Dinitrotoluene ND ug/kg 05/17/23 11:39 606-20-205/16/23 14:28389 1
Di-n-octylphthalate ND ug/kg 05/17/23 11:39 117-84-005/16/23 14:28389 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/23 11:39 117-81-705/16/23 14:28389 1
Fluoranthene ND ug/kg 05/17/23 11:39 206-44-005/16/23 14:28389 1
Fluorene ND ug/kg 05/17/23 11:39 86-73-705/16/23 14:28389 1
Hexachloro-1,3-butadiene ND ug/kg 05/17/23 11:39 87-68-305/16/23 14:28389 1
Hexachlorobenzene ND ug/kg 05/17/23 11:39 118-74-105/16/23 14:28389 1
Hexachlorocyclopentadiene ND ug/kg 05/17/23 11:39 77-47-405/16/23 14:28389 1
Hexachloroethane ND ug/kg 05/17/23 11:39 67-72-105/16/23 14:28389 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/23 11:39 193-39-505/16/23 14:28389 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
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Huntersville, NC 28078
[phone]
Page 4 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-216 Lab ID: 92667253001 Collected: 05/12/23 08:25 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/17/23 11:39 78-59-105/16/23 14:28389 1
1-Methylnaphthalene 1060 ug/kg 05/17/23 11:39 90-12-005/16/23 14:28389 1
2-Methylnaphthalene 1150 ug/kg 05/17/23 11:39 91-57-605/16/23 14:28389 1
2-Methylphenol(o-Cresol) ND ug/kg 05/17/23 11:39 95-48-705/16/23 14:28389 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/17/23 11:39 15831-10-405/16/23 14:28389 1
Naphthalene ND ug/kg 05/17/23 11:39 91-20-305/16/23 14:28389 1
2-Nitroaniline ND ug/kg 05/17/23 11:39 88-74-405/16/23 14:281950 1
3-Nitroaniline ND ug/kg 05/17/23 11:39 99-09-205/16/23 14:281950 1
4-Nitroaniline ND ug/kg 05/17/23 11:39 100-01-605/16/23 14:28778 1
Nitrobenzene ND ug/kg 05/17/23 11:39 98-95-305/16/23 14:28389 1
2-Nitrophenol ND ug/kg 05/17/23 11:39 88-75-505/16/23 14:28389 1
4-Nitrophenol ND ug/kg 05/17/23 11:39 100-02-705/16/23 14:281950 1
N-Nitrosodimethylamine ND ug/kg 05/17/23 11:39 62-75-905/16/23 14:28389 1
N-Nitroso-di-n-propylamine ND ug/kg 05/17/23 11:39 621-64-705/16/23 14:28389 1
N-Nitrosodiphenylamine ND ug/kg 05/17/23 11:39 86-30-605/16/23 14:28389 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/17/23 11:39 108-60-105/16/23 14:28389 1
Pentachlorophenol ND ug/kg 05/17/23 11:39 87-86-505/16/23 14:28778 1
Phenanthrene 599 ug/kg 05/17/23 11:39 85-01-805/16/23 14:28389 1
Phenol ND ug/kg 05/17/23 11:39 108-95-205/16/23 14:28389 1
Pyrene ND ug/kg 05/17/23 11:39 129-00-005/16/23 14:28389 1
Pyridine ND ug/kg 05/17/23 11:39 110-86-105/16/23 14:28389 1
1,2,4-Trichlorobenzene ND ug/kg 05/17/23 11:39 120-82-105/16/23 14:28389 1
2,4,5-Trichlorophenol ND ug/kg 05/17/23 11:39 95-95-405/16/23 14:28389 1
2,4,6-Trichlorophenol ND ug/kg 05/17/23 11:39 88-06-205/16/23 14:28389 1
Surrogates
Nitrobenzene-d5 (S) 52 %05/17/23 11:39 4165-60-005/16/23 14:2810-130 1
2-Fluorobiphenyl (S) 57 %05/17/23 11:39 321-60-805/16/23 14:2810-130 1
Terphenyl-d14 (S) 57 %05/17/23 11:39 1718-51-005/16/23 14:2810-130 1
Phenol-d6 (S) 47 %05/17/23 11:39 13127-88-305/16/23 14:2810-130 1
2-Fluorophenol (S) 50 %05/17/23 11:39 367-12-405/16/23 14:2810-130 1
2,4,6-Tribromophenol (S) 66 %05/17/23 11:39 118-79-605/16/23 14:2810-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/19/23 09:57 67-64-105/18/23 22:28112 1
Benzene ND ug/kg 05/19/23 09:57 71-43-205/18/23 22:285.6 1
Bromobenzene ND ug/kg 05/19/23 09:57 108-86-105/18/23 22:285.6 1
Bromochloromethane ND ug/kg 05/19/23 09:57 74-97-505/18/23 22:285.6 1
Bromodichloromethane ND ug/kg 05/19/23 09:57 75-27-405/18/23 22:285.6 1
Bromoform ND ug/kg 05/19/23 09:57 75-25-205/18/23 22:285.6 1
Bromomethane ND ug/kg 05/19/23 09:57 74-83-905/18/23 22:2822.4 1
2-Butanone (MEK) ND ug/kg 05/19/23 09:57 78-93-305/18/23 22:28112 1
n-Butylbenzene 1650 ug/kg 05/19/23 09:57 104-51-805/18/23 22:285.6 1
sec-Butylbenzene 1610 ug/kg 05/19/23 09:57 135-98-805/18/23 22:285.6 1
tert-Butylbenzene ND ug/kg 05/19/23 09:57 98-06-605/18/23 22:285.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
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[phone]
Page 5 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-216 Lab ID: 92667253001 Collected: 05/12/23 08:25 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/19/23 09:57 56-23-505/18/23 22:285.6 1
Chlorobenzene ND ug/kg 05/19/23 09:57 108-90-705/18/23 22:285.6 1
Chloroethane ND ug/kg 05/19/23 09:57 75-00-305/18/23 22:2811.2 1
Chloroform ND ug/kg 05/19/23 09:57 67-66-305/18/23 22:285.6 1
Chloromethane 4400 ug/kg 05/19/23 09:57 74-87-305/18/23 22:2811.2 1
2-Chlorotoluene ND ug/kg 05/19/23 09:57 95-49-805/18/23 22:285.6 1
4-Chlorotoluene ND ug/kg 05/19/23 09:57 106-43-405/18/23 22:285.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/19/23 09:57 96-12-805/18/23 22:285.6 1
Dibromochloromethane ND ug/kg 05/19/23 09:57 124-48-105/18/23 22:285.6 1
1,2-Dibromoethane (EDB) ND ug/kg 05/19/23 09:57 106-93-405/18/23 22:285.6 1
Dibromomethane ND ug/kg 05/19/23 09:57 74-95-305/18/23 22:285.6 1
1,2-Dichlorobenzene ND ug/kg 05/19/23 09:57 95-50-105/18/23 22:285.6 1
1,3-Dichlorobenzene ND ug/kg 05/19/23 09:57 541-73-105/18/23 22:285.6 1
1,4-Dichlorobenzene ND ug/kg 05/19/23 09:57 106-46-705/18/23 22:285.6 1
Dichlorodifluoromethane ND ug/kg 05/19/23 09:57 75-71-8 IH05/18/23 22:2811.2 1
1,1-Dichloroethane ND ug/kg 05/19/23 09:57 75-34-305/18/23 22:285.6 1
1,2-Dichloroethane ND ug/kg 05/19/23 09:57 107-06-205/18/23 22:285.6 1
1,1-Dichloroethene ND ug/kg 05/19/23 09:57 75-35-405/18/23 22:285.6 1
cis-1,2-Dichloroethene ND ug/kg 05/19/23 09:57 156-59-205/18/23 22:285.6 1
trans-1,2-Dichloroethene ND ug/kg 05/19/23 09:57 156-60-505/18/23 22:285.6 1
1,2-Dichloropropane ND ug/kg 05/19/23 09:57 78-87-505/18/23 22:285.6 1
1,3-Dichloropropane ND ug/kg 05/19/23 09:57 142-28-905/18/23 22:285.6 1
2,2-Dichloropropane ND ug/kg 05/19/23 09:57 594-20-705/18/23 22:285.6 1
1,1-Dichloropropene ND ug/kg 05/19/23 09:57 563-58-605/18/23 22:285.6 1
cis-1,3-Dichloropropene ND ug/kg 05/19/23 09:57 10061-01-505/18/23 22:285.6 1
trans-1,3-Dichloropropene ND ug/kg 05/19/23 09:57 10061-02-605/18/23 22:285.6 1
Diisopropyl ether ND ug/kg 05/19/23 09:57 108-20-305/18/23 22:285.6 1
Ethylbenzene 15.7 ug/kg 05/19/23 09:57 100-41-405/18/23 22:285.6 1
Hexachloro-1,3-butadiene ND ug/kg 05/19/23 09:57 87-68-305/18/23 22:2811.2 1
2-Hexanone ND ug/kg 05/19/23 09:57 591-78-605/18/23 22:2856.1 1
Isopropylbenzene (Cumene)649 ug/kg 05/19/23 09:57 98-82-805/18/23 22:285.6 1
p-Isopropyltoluene ND ug/kg 05/19/23 09:57 99-87-605/18/23 22:285.6 1
Methylene Chloride ND ug/kg 05/19/23 09:57 75-09-205/18/23 22:2822.4 1
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/19/23 09:57 108-10-105/18/23 22:2856.1 1
Methyl-tert-butyl ether ND ug/kg 05/19/23 09:57 1634-04-405/18/23 22:285.6 1
Naphthalene 1800 ug/kg 05/19/23 09:57 91-20-305/18/23 22:285.6 1
n-Propylbenzene 1690 ug/kg 05/19/23 09:57 103-65-105/18/23 22:285.6 1
Styrene ND ug/kg 05/19/23 09:57 100-42-505/18/23 22:285.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/19/23 09:57 630-20-605/18/23 22:285.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/19/23 09:57 79-34-505/18/23 22:285.6 1
Tetrachloroethene ND ug/kg 05/19/23 09:57 127-18-405/18/23 22:285.6 1
Toluene ND ug/kg 05/19/23 09:57 108-88-305/18/23 22:285.6 1
1,2,3-Trichlorobenzene ND ug/kg 05/19/23 09:57 87-61-605/18/23 22:285.6 1
1,2,4-Trichlorobenzene ND ug/kg 05/19/23 09:57 120-82-105/18/23 22:285.6 1
1,1,1-Trichloroethane ND ug/kg 05/19/23 09:57 71-55-605/18/23 22:285.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-216 Lab ID: 92667253001 Collected: 05/12/23 08:25 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane 321 ug/kg 05/19/23 09:57 79-00-505/18/23 22:285.6 1
Trichloroethene ND ug/kg 05/19/23 09:57 79-01-605/18/23 22:285.6 1
Trichlorofluoromethane ND ug/kg 05/19/23 09:57 75-69-405/18/23 22:285.6 1
1,2,3-Trichloropropane ND ug/kg 05/19/23 09:57 96-18-405/18/23 22:285.6 1
1,2,4-Trimethylbenzene ND ug/kg 05/19/23 09:57 95-63-605/18/23 22:285.6 1
1,3,5-Trimethylbenzene ND ug/kg 05/19/23 09:57 108-67-805/18/23 22:285.6 1
Vinyl acetate ND ug/kg 05/19/23 09:57 108-05-405/18/23 22:2856.1 1
Vinyl chloride ND ug/kg 05/19/23 09:57 75-01-405/18/23 22:2811.2 1
Xylene (Total) ND ug/kg 05/19/23 09:57 1330-20-705/18/23 22:2811.2 1
m&p-Xylene ND ug/kg 05/19/23 09:57 179601-23-105/18/23 22:2811.2 1
o-Xylene ND ug/kg 05/19/23 09:57 95-47-605/18/23 22:285.6 1
Surrogates
Toluene-d8 (S) 102 %05/19/23 09:57 2037-26-505/18/23 22:2870-130 1
4-Bromofluorobenzene (S) 120 %05/19/23 09:57 460-00-405/18/23 22:2870-130 1
1,2-Dichloroethane-d4 (S) 103 %05/19/23 09:57 17060-07-005/18/23 22:2870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.2 %05/15/23 13:12 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-217 Lab ID: 92667253002 Collected: 05/12/23 08:40 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/17/23 15:27 83-32-905/16/23 14:283690 10
Acenaphthylene ND ug/kg 05/17/23 15:27 208-96-805/16/23 14:283690 10
Aniline ND ug/kg 05/17/23 15:27 62-53-305/16/23 14:283690 10
Anthracene ND ug/kg 05/17/23 15:27 120-12-705/16/23 14:283690 10
Benzo(a)anthracene ND ug/kg 05/17/23 15:27 56-55-305/16/23 14:283690 10
Benzo(a)pyrene ND ug/kg 05/17/23 15:27 50-32-805/16/23 14:283690 10
Benzo(b)fluoranthene ND ug/kg 05/17/23 15:27 205-99-205/16/23 14:283690 10
Benzo(g,h,i)perylene ND ug/kg 05/17/23 15:27 191-24-205/16/23 14:283690 10
Benzo(k)fluoranthene ND ug/kg 05/17/23 15:27 207-08-905/16/23 14:283690 10
Benzoic Acid ND ug/kg 05/17/23 15:27 65-85-005/16/23 14:2818500 10
Benzyl alcohol ND ug/kg 05/17/23 15:27 100-51-605/16/23 14:287390 10
4-Bromophenylphenyl ether ND ug/kg 05/17/23 15:27 101-55-305/16/23 14:283690 10
Butylbenzylphthalate ND ug/kg 05/17/23 15:27 85-68-705/16/23 14:283690 10
4-Chloro-3-methylphenol ND ug/kg 05/17/23 15:27 59-50-705/16/23 14:287390 10
4-Chloroaniline ND ug/kg 05/17/23 15:27 106-47-805/16/23 14:287390 10
bis(2-Chloroethoxy)methane ND ug/kg 05/17/23 15:27 111-91-105/16/23 14:283690 10
bis(2-Chloroethyl) ether ND ug/kg 05/17/23 15:27 111-44-405/16/23 14:283690 10
2-Chloronaphthalene ND ug/kg 05/17/23 15:27 91-58-705/16/23 14:283690 10
2-Chlorophenol ND ug/kg 05/17/23 15:27 95-57-805/16/23 14:283690 10
4-Chlorophenylphenyl ether ND ug/kg 05/17/23 15:27 7005-72-305/16/23 14:283690 10
Chrysene ND ug/kg 05/17/23 15:27 218-01-905/16/23 14:283690 10
Dibenz(a,h)anthracene ND ug/kg 05/17/23 15:27 53-70-305/16/23 14:283690 10
Dibenzofuran ND ug/kg 05/17/23 15:27 132-64-905/16/23 14:283690 10
1,2-Dichlorobenzene ND ug/kg 05/17/23 15:27 95-50-105/16/23 14:283690 10
1,3-Dichlorobenzene ND ug/kg 05/17/23 15:27 541-73-105/16/23 14:283690 10
1,4-Dichlorobenzene ND ug/kg 05/17/23 15:27 106-46-705/16/23 14:283690 10
3,3'-Dichlorobenzidine ND ug/kg 05/17/23 15:27 91-94-105/16/23 14:287390 10
2,4-Dichlorophenol ND ug/kg 05/17/23 15:27 120-83-205/16/23 14:283690 10
Diethylphthalate ND ug/kg 05/17/23 15:27 84-66-205/16/23 14:283690 10
2,4-Dimethylphenol ND ug/kg 05/17/23 15:27 105-67-905/16/23 14:283690 10
Dimethylphthalate ND ug/kg 05/17/23 15:27 131-11-305/16/23 14:283690 10
Di-n-butylphthalate ND ug/kg 05/17/23 15:27 84-74-205/16/23 14:283690 10
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/23 15:27 534-52-105/16/23 14:287390 10
2,4-Dinitrophenol ND ug/kg 05/17/23 15:27 51-28-505/16/23 14:2818500 10
2,4-Dinitrotoluene ND ug/kg 05/17/23 15:27 121-14-205/16/23 14:283690 10
2,6-Dinitrotoluene ND ug/kg 05/17/23 15:27 606-20-205/16/23 14:283690 10
Di-n-octylphthalate ND ug/kg 05/17/23 15:27 117-84-005/16/23 14:283690 10
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/23 15:27 117-81-705/16/23 14:283690 10
Fluoranthene ND ug/kg 05/17/23 15:27 206-44-005/16/23 14:283690 10
Fluorene ND ug/kg 05/17/23 15:27 86-73-705/16/23 14:283690 10
Hexachloro-1,3-butadiene ND ug/kg 05/17/23 15:27 87-68-305/16/23 14:283690 10
Hexachlorobenzene ND ug/kg 05/17/23 15:27 118-74-105/16/23 14:283690 10
Hexachlorocyclopentadiene ND ug/kg 05/17/23 15:27 77-47-405/16/23 14:283690 10
Hexachloroethane ND ug/kg 05/17/23 15:27 67-72-105/16/23 14:283690 10
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/23 15:27 193-39-505/16/23 14:283690 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-217 Lab ID: 92667253002 Collected: 05/12/23 08:40 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/17/23 15:27 78-59-105/16/23 14:283690 10
1-Methylnaphthalene 7560 ug/kg 05/17/23 15:27 90-12-005/16/23 14:283690 10
2-Methylnaphthalene 11700 ug/kg 05/17/23 15:27 91-57-605/16/23 14:283690 10
2-Methylphenol(o-Cresol) ND ug/kg 05/17/23 15:27 95-48-705/16/23 14:283690 10
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/17/23 15:27 15831-10-405/16/23 14:283690 10
Naphthalene ND ug/kg 05/17/23 15:27 91-20-305/16/23 14:283690 10
2-Nitroaniline ND ug/kg 05/17/23 15:27 88-74-405/16/23 14:2818500 10
3-Nitroaniline ND ug/kg 05/17/23 15:27 99-09-205/16/23 14:2818500 10
4-Nitroaniline ND ug/kg 05/17/23 15:27 100-01-605/16/23 14:287390 10
Nitrobenzene ND ug/kg 05/17/23 15:27 98-95-305/16/23 14:283690 10
2-Nitrophenol ND ug/kg 05/17/23 15:27 88-75-505/16/23 14:283690 10
4-Nitrophenol ND ug/kg 05/17/23 15:27 100-02-705/16/23 14:2818500 10
N-Nitrosodimethylamine ND ug/kg 05/17/23 15:27 62-75-905/16/23 14:283690 10
N-Nitroso-di-n-propylamine ND ug/kg 05/17/23 15:27 621-64-705/16/23 14:283690 10
N-Nitrosodiphenylamine ND ug/kg 05/17/23 15:27 86-30-605/16/23 14:283690 10
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/17/23 15:27 108-60-105/16/23 14:283690 10
Pentachlorophenol ND ug/kg 05/17/23 15:27 87-86-505/16/23 14:287390 10
Phenanthrene ND ug/kg 05/17/23 15:27 85-01-805/16/23 14:283690 10
Phenol ND ug/kg 05/17/23 15:27 108-95-205/16/23 14:283690 10
Pyrene ND ug/kg 05/17/23 15:27 129-00-005/16/23 14:283690 10
Pyridine ND ug/kg 05/17/23 15:27 110-86-105/16/23 14:283690 10
1,2,4-Trichlorobenzene ND ug/kg 05/17/23 15:27 120-82-105/16/23 14:283690 10
2,4,5-Trichlorophenol ND ug/kg 05/17/23 15:27 95-95-405/16/23 14:283690 10
2,4,6-Trichlorophenol ND ug/kg 05/17/23 15:27 88-06-205/16/23 14:283690 10
Surrogates
Nitrobenzene-d5 (S) 0 %05/17/23 15:27 4165-60-0 D3,S405/16/23 14:2810-130 10
2-Fluorobiphenyl (S) 0 %05/17/23 15:27 321-60-8 S405/16/23 14:2810-130 10
Terphenyl-d14 (S) 0 %05/17/23 15:27 1718-51-0 S405/16/23 14:2810-130 10
Phenol-d6 (S)0 %05/17/23 15:27 13127-88-3 S405/16/23 14:2810-130 10
2-Fluorophenol (S) 0 %05/17/23 15:27 367-12-4 S405/16/23 14:2810-130 10
2,4,6-Tribromophenol (S) 0 %05/17/23 15:27 118-79-6 S405/16/23 14:2810-131 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/19/23 10:34 67-64-105/18/23 22:28245 2.5
Benzene ND ug/kg 05/19/23 10:34 71-43-205/18/23 22:2812.3 2.5
Bromobenzene ND ug/kg 05/19/23 10:34 108-86-105/18/23 22:2812.3 2.5
Bromochloromethane ND ug/kg 05/19/23 10:34 74-97-505/18/23 22:2812.3 2.5
Bromodichloromethane ND ug/kg 05/19/23 10:34 75-27-405/18/23 22:2812.3 2.5
Bromoform ND ug/kg 05/19/23 10:34 75-25-205/18/23 22:2812.3 2.5
Bromomethane ND ug/kg 05/19/23 10:34 74-83-905/18/23 22:2849.1 2.5
2-Butanone (MEK) ND ug/kg 05/19/23 10:34 78-93-305/18/23 22:28245 2.5
n-Butylbenzene 2660 ug/kg 05/19/23 10:34 104-51-805/18/23 22:2812.3 2.5
sec-Butylbenzene 2780 ug/kg 05/19/23 10:34 135-98-805/18/23 22:2812.3 2.5
tert-Butylbenzene ND ug/kg 05/19/23 10:34 98-06-605/18/23 22:2812.3 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-217 Lab ID: 92667253002 Collected: 05/12/23 08:40 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/19/23 10:34 56-23-505/18/23 22:2812.3 2.5
Chlorobenzene ND ug/kg 05/19/23 10:34 108-90-705/18/23 22:2812.3 2.5
Chloroethane ND ug/kg 05/19/23 10:34 75-00-305/18/23 22:2824.5 2.5
Chloroform ND ug/kg 05/19/23 10:34 67-66-305/18/23 22:2812.3 2.5
Chloromethane ND ug/kg 05/19/23 10:34 74-87-305/18/23 22:2824.5 2.5
2-Chlorotoluene ND ug/kg 05/19/23 10:34 95-49-805/18/23 22:2812.3 2.5
4-Chlorotoluene ND ug/kg 05/19/23 10:34 106-43-405/18/23 22:2812.3 2.5
1,2-Dibromo-3-chloropropane ND ug/kg 05/19/23 10:34 96-12-805/18/23 22:2812.3 2.5
Dibromochloromethane ND ug/kg 05/19/23 10:34 124-48-105/18/23 22:2812.3 2.5
1,2-Dibromoethane (EDB) ND ug/kg 05/19/23 10:34 106-93-405/18/23 22:2812.3 2.5
Dibromomethane ND ug/kg 05/19/23 10:34 74-95-305/18/23 22:2812.3 2.5
1,2-Dichlorobenzene ND ug/kg 05/19/23 10:34 95-50-105/18/23 22:2812.3 2.5
1,3-Dichlorobenzene ND ug/kg 05/19/23 10:34 541-73-105/18/23 22:2812.3 2.5
1,4-Dichlorobenzene ND ug/kg 05/19/23 10:34 106-46-705/18/23 22:2812.3 2.5
Dichlorodifluoromethane ND ug/kg 05/19/23 10:34 75-71-8 IH05/18/23 22:2824.5 2.5
1,1-Dichloroethane ND ug/kg 05/19/23 10:34 75-34-305/18/23 22:2812.3 2.5
1,2-Dichloroethane ND ug/kg 05/19/23 10:34 107-06-205/18/23 22:2812.3 2.5
1,1-Dichloroethene ND ug/kg 05/19/23 10:34 75-35-405/18/23 22:2812.3 2.5
cis-1,2-Dichloroethene ND ug/kg 05/19/23 10:34 156-59-205/18/23 22:2812.3 2.5
trans-1,2-Dichloroethene ND ug/kg 05/19/23 10:34 156-60-505/18/23 22:2812.3 2.5
1,2-Dichloropropane ND ug/kg 05/19/23 10:34 78-87-505/18/23 22:2812.3 2.5
1,3-Dichloropropane ND ug/kg 05/19/23 10:34 142-28-905/18/23 22:2812.3 2.5
2,2-Dichloropropane ND ug/kg 05/19/23 10:34 594-20-705/18/23 22:2812.3 2.5
1,1-Dichloropropene ND ug/kg 05/19/23 10:34 563-58-605/18/23 22:2812.3 2.5
cis-1,3-Dichloropropene ND ug/kg 05/19/23 10:34 10061-01-505/18/23 22:2812.3 2.5
trans-1,3-Dichloropropene ND ug/kg 05/19/23 10:34 10061-02-605/18/23 22:2812.3 2.5
Diisopropyl ether ND ug/kg 05/19/23 10:34 108-20-305/18/23 22:2812.3 2.5
Ethylbenzene 119 ug/kg 05/19/23 10:34 100-41-405/18/23 22:2812.3 2.5
Hexachloro-1,3-butadiene ND ug/kg 05/19/23 10:34 87-68-305/18/23 22:2824.5 2.5
2-Hexanone ND ug/kg 05/19/23 10:34 591-78-605/18/23 22:28123 2.5
Isopropylbenzene (Cumene)1440 ug/kg 05/19/23 10:34 98-82-805/18/23 22:2812.3 2.5
p-Isopropyltoluene ND ug/kg 05/19/23 10:34 99-87-605/18/23 22:2812.3 2.5
Methylene Chloride ND ug/kg 05/19/23 10:34 75-09-205/18/23 22:2849.1 2.5
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/19/23 10:34 108-10-105/18/23 22:28123 2.5
Methyl-tert-butyl ether ND ug/kg 05/19/23 10:34 1634-04-405/18/23 22:2812.3 2.5
Naphthalene 5550 ug/kg 05/19/23 10:34 91-20-305/18/23 22:2812.3 2.5
n-Propylbenzene 3320 ug/kg 05/19/23 10:34 103-65-105/18/23 22:2812.3 2.5
Styrene ND ug/kg 05/19/23 10:34 100-42-505/18/23 22:2812.3 2.5
1,1,1,2-Tetrachloroethane ND ug/kg 05/19/23 10:34 630-20-605/18/23 22:2812.3 2.5
1,1,2,2-Tetrachloroethane ND ug/kg 05/19/23 10:34 79-34-505/18/23 22:2812.3 2.5
Tetrachloroethene ND ug/kg 05/19/23 10:34 127-18-405/18/23 22:2812.3 2.5
Toluene ND ug/kg 05/19/23 10:34 108-88-305/18/23 22:2812.3 2.5
1,2,3-Trichlorobenzene ND ug/kg 05/19/23 10:34 87-61-605/18/23 22:2812.3 2.5
1,2,4-Trichlorobenzene ND ug/kg 05/19/23 10:34 120-82-105/18/23 22:2812.3 2.5
1,1,1-Trichloroethane ND ug/kg 05/19/23 10:34 71-55-605/18/23 22:2812.3 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-217 Lab ID: 92667253002 Collected: 05/12/23 08:40 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/19/23 10:34 79-00-505/18/23 22:2812.3 2.5
Trichloroethene ND ug/kg 05/19/23 10:34 79-01-605/18/23 22:2812.3 2.5
Trichlorofluoromethane ND ug/kg 05/19/23 10:34 75-69-405/18/23 22:2812.3 2.5
1,2,3-Trichloropropane ND ug/kg 05/19/23 10:34 96-18-405/18/23 22:2812.3 2.5
1,2,4-Trimethylbenzene ND ug/kg 05/19/23 10:34 95-63-605/18/23 22:2812.3 2.5
1,3,5-Trimethylbenzene ND ug/kg 05/19/23 10:34 108-67-805/18/23 22:2812.3 2.5
Vinyl acetate ND ug/kg 05/19/23 10:34 108-05-405/18/23 22:28123 2.5
Vinyl chloride ND ug/kg 05/19/23 10:34 75-01-405/18/23 22:2824.5 2.5
Xylene (Total) ND ug/kg 05/19/23 10:34 1330-20-705/18/23 22:2824.5 2.5
m&p-Xylene ND ug/kg 05/19/23 10:34 179601-23-105/18/23 22:2824.5 2.5
o-Xylene ND ug/kg 05/19/23 10:34 95-47-605/18/23 22:2812.3 2.5
Surrogates
Toluene-d8 (S) 101 %05/19/23 10:34 2037-26-505/18/23 22:2870-130 2.5
4-Bromofluorobenzene (S) 120 %05/19/23 10:34 460-00-405/18/23 22:2870-130 2.5
1,2-Dichloroethane-d4 (S) 102 %05/19/23 10:34 17060-07-005/18/23 22:2870-130 2.5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.1 %05/15/23 13:13 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-218 Lab ID: 92667253003 Collected: 05/12/23 08:50 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/17/23 15:55 83-32-905/16/23 14:283830 10
Acenaphthylene ND ug/kg 05/17/23 15:55 208-96-805/16/23 14:283830 10
Aniline ND ug/kg 05/17/23 15:55 62-53-305/16/23 14:283830 10
Anthracene ND ug/kg 05/17/23 15:55 120-12-705/16/23 14:283830 10
Benzo(a)anthracene ND ug/kg 05/17/23 15:55 56-55-305/16/23 14:283830 10
Benzo(a)pyrene ND ug/kg 05/17/23 15:55 50-32-805/16/23 14:283830 10
Benzo(b)fluoranthene ND ug/kg 05/17/23 15:55 205-99-205/16/23 14:283830 10
Benzo(g,h,i)perylene ND ug/kg 05/17/23 15:55 191-24-205/16/23 14:283830 10
Benzo(k)fluoranthene ND ug/kg 05/17/23 15:55 207-08-905/16/23 14:283830 10
Benzoic Acid ND ug/kg 05/17/23 15:55 65-85-005/16/23 14:2819100 10
Benzyl alcohol ND ug/kg 05/17/23 15:55 100-51-605/16/23 14:287660 10
4-Bromophenylphenyl ether ND ug/kg 05/17/23 15:55 101-55-305/16/23 14:283830 10
Butylbenzylphthalate ND ug/kg 05/17/23 15:55 85-68-705/16/23 14:283830 10
4-Chloro-3-methylphenol ND ug/kg 05/17/23 15:55 59-50-705/16/23 14:287660 10
4-Chloroaniline ND ug/kg 05/17/23 15:55 106-47-805/16/23 14:287660 10
bis(2-Chloroethoxy)methane ND ug/kg 05/17/23 15:55 111-91-105/16/23 14:283830 10
bis(2-Chloroethyl) ether ND ug/kg 05/17/23 15:55 111-44-405/16/23 14:283830 10
2-Chloronaphthalene ND ug/kg 05/17/23 15:55 91-58-705/16/23 14:283830 10
2-Chlorophenol ND ug/kg 05/17/23 15:55 95-57-805/16/23 14:283830 10
4-Chlorophenylphenyl ether ND ug/kg 05/17/23 15:55 7005-72-305/16/23 14:283830 10
Chrysene ND ug/kg 05/17/23 15:55 218-01-905/16/23 14:283830 10
Dibenz(a,h)anthracene ND ug/kg 05/17/23 15:55 53-70-305/16/23 14:283830 10
Dibenzofuran ND ug/kg 05/17/23 15:55 132-64-905/16/23 14:283830 10
1,2-Dichlorobenzene ND ug/kg 05/17/23 15:55 95-50-105/16/23 14:283830 10
1,3-Dichlorobenzene ND ug/kg 05/17/23 15:55 541-73-105/16/23 14:283830 10
1,4-Dichlorobenzene ND ug/kg 05/17/23 15:55 106-46-705/16/23 14:283830 10
3,3'-Dichlorobenzidine ND ug/kg 05/17/23 15:55 91-94-105/16/23 14:287660 10
2,4-Dichlorophenol ND ug/kg 05/17/23 15:55 120-83-205/16/23 14:283830 10
Diethylphthalate ND ug/kg 05/17/23 15:55 84-66-205/16/23 14:283830 10
2,4-Dimethylphenol ND ug/kg 05/17/23 15:55 105-67-905/16/23 14:283830 10
Dimethylphthalate ND ug/kg 05/17/23 15:55 131-11-305/16/23 14:283830 10
Di-n-butylphthalate ND ug/kg 05/17/23 15:55 84-74-205/16/23 14:283830 10
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/23 15:55 534-52-105/16/23 14:287660 10
2,4-Dinitrophenol ND ug/kg 05/17/23 15:55 51-28-505/16/23 14:2819100 10
2,4-Dinitrotoluene ND ug/kg 05/17/23 15:55 121-14-205/16/23 14:283830 10
2,6-Dinitrotoluene ND ug/kg 05/17/23 15:55 606-20-205/16/23 14:283830 10
Di-n-octylphthalate ND ug/kg 05/17/23 15:55 117-84-005/16/23 14:283830 10
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/23 15:55 117-81-705/16/23 14:283830 10
Fluoranthene ND ug/kg 05/17/23 15:55 206-44-005/16/23 14:283830 10
Fluorene ND ug/kg 05/17/23 15:55 86-73-705/16/23 14:283830 10
Hexachloro-1,3-butadiene ND ug/kg 05/17/23 15:55 87-68-305/16/23 14:283830 10
Hexachlorobenzene ND ug/kg 05/17/23 15:55 118-74-105/16/23 14:283830 10
Hexachlorocyclopentadiene ND ug/kg 05/17/23 15:55 77-47-405/16/23 14:283830 10
Hexachloroethane ND ug/kg 05/17/23 15:55 67-72-105/16/23 14:283830 10
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/23 15:55 193-39-505/16/23 14:283830 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-218 Lab ID: 92667253003 Collected: 05/12/23 08:50 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/17/23 15:55 78-59-105/16/23 14:283830 10
1-Methylnaphthalene 8520 ug/kg 05/17/23 15:55 90-12-005/16/23 14:283830 10
2-Methylnaphthalene 13100 ug/kg 05/17/23 15:55 91-57-605/16/23 14:283830 10
2-Methylphenol(o-Cresol) ND ug/kg 05/17/23 15:55 95-48-705/16/23 14:283830 10
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/17/23 15:55 15831-10-405/16/23 14:283830 10
Naphthalene 4650 ug/kg 05/17/23 15:55 91-20-305/16/23 14:283830 10
2-Nitroaniline ND ug/kg 05/17/23 15:55 88-74-405/16/23 14:2819100 10
3-Nitroaniline ND ug/kg 05/17/23 15:55 99-09-205/16/23 14:2819100 10
4-Nitroaniline ND ug/kg 05/17/23 15:55 100-01-605/16/23 14:287660 10
Nitrobenzene ND ug/kg 05/17/23 15:55 98-95-305/16/23 14:283830 10
2-Nitrophenol ND ug/kg 05/17/23 15:55 88-75-505/16/23 14:283830 10
4-Nitrophenol ND ug/kg 05/17/23 15:55 100-02-705/16/23 14:2819100 10
N-Nitrosodimethylamine ND ug/kg 05/17/23 15:55 62-75-905/16/23 14:283830 10
N-Nitroso-di-n-propylamine ND ug/kg 05/17/23 15:55 621-64-705/16/23 14:283830 10
N-Nitrosodiphenylamine ND ug/kg 05/17/23 15:55 86-30-605/16/23 14:283830 10
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/17/23 15:55 108-60-105/16/23 14:283830 10
Pentachlorophenol ND ug/kg 05/17/23 15:55 87-86-505/16/23 14:287660 10
Phenanthrene ND ug/kg 05/17/23 15:55 85-01-805/16/23 14:283830 10
Phenol ND ug/kg 05/17/23 15:55 108-95-205/16/23 14:283830 10
Pyrene ND ug/kg 05/17/23 15:55 129-00-005/16/23 14:283830 10
Pyridine ND ug/kg 05/17/23 15:55 110-86-105/16/23 14:283830 10
1,2,4-Trichlorobenzene ND ug/kg 05/17/23 15:55 120-82-105/16/23 14:283830 10
2,4,5-Trichlorophenol ND ug/kg 05/17/23 15:55 95-95-405/16/23 14:283830 10
2,4,6-Trichlorophenol ND ug/kg 05/17/23 15:55 88-06-205/16/23 14:283830 10
Surrogates
Nitrobenzene-d5 (S) 0 %05/17/23 15:55 4165-60-0 D3,S405/16/23 14:2810-130 10
2-Fluorobiphenyl (S) 0 %05/17/23 15:55 321-60-8 S405/16/23 14:2810-130 10
Terphenyl-d14 (S) 0 %05/17/23 15:55 1718-51-0 S405/16/23 14:2810-130 10
Phenol-d6 (S)0 %05/17/23 15:55 13127-88-3 S405/16/23 14:2810-130 10
2-Fluorophenol (S) 0 %05/17/23 15:55 367-12-4 S405/16/23 14:2810-130 10
2,4,6-Tribromophenol (S) 0 %05/17/23 15:55 118-79-6 S405/16/23 14:2810-131 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/23/23 12:34 67-64-105/22/23 22:22583 5
Benzene ND ug/kg 05/23/23 12:34 71-43-205/22/23 22:2229.2 5
Bromobenzene ND ug/kg 05/23/23 12:34 108-86-105/22/23 22:2229.2 5
Bromochloromethane ND ug/kg 05/23/23 12:34 74-97-505/22/23 22:2229.2 5
Bromodichloromethane ND ug/kg 05/23/23 12:34 75-27-405/22/23 22:2229.2 5
Bromoform ND ug/kg 05/23/23 12:34 75-25-205/22/23 22:2229.2 5
Bromomethane ND ug/kg 05/23/23 12:34 74-83-9 v205/22/23 22:22117 5
2-Butanone (MEK) ND ug/kg 05/23/23 12:34 78-93-305/22/23 22:22583 5
n-Butylbenzene 1980 ug/kg 05/23/23 12:34 104-51-805/22/23 22:2229.2 5
sec-Butylbenzene 2120 ug/kg 05/23/23 12:34 135-98-805/22/23 22:2229.2 5
tert-Butylbenzene ND ug/kg 05/23/23 12:34 98-06-605/22/23 22:2229.2 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-218 Lab ID: 92667253003 Collected: 05/12/23 08:50 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/23/23 12:34 56-23-505/22/23 22:2229.2 5
Chlorobenzene ND ug/kg 05/23/23 12:34 108-90-705/22/23 22:2229.2 5
Chloroethane ND ug/kg 05/23/23 12:34 75-00-305/22/23 22:2258.3 5
Chloroform ND ug/kg 05/23/23 12:34 67-66-305/22/23 22:2229.2 5
Chloromethane 3930 ug/kg 05/23/23 12:34 74-87-305/22/23 22:2258.3 5
2-Chlorotoluene ND ug/kg 05/23/23 12:34 95-49-805/22/23 22:2229.2 5
4-Chlorotoluene ND ug/kg 05/23/23 12:34 106-43-405/22/23 22:2229.2 5
1,2-Dibromo-3-chloropropane ND ug/kg 05/23/23 12:34 96-12-805/22/23 22:2229.2 5
Dibromochloromethane ND ug/kg 05/23/23 12:34 124-48-105/22/23 22:2229.2 5
1,2-Dibromoethane (EDB) ND ug/kg 05/23/23 12:34 106-93-405/22/23 22:2229.2 5
Dibromomethane ND ug/kg 05/23/23 12:34 74-95-305/22/23 22:2229.2 5
1,2-Dichlorobenzene ND ug/kg 05/23/23 12:34 95-50-105/22/23 22:2229.2 5
1,3-Dichlorobenzene ND ug/kg 05/23/23 12:34 541-73-105/22/23 22:2229.2 5
1,4-Dichlorobenzene ND ug/kg 05/23/23 12:34 106-46-705/22/23 22:2229.2 5
Dichlorodifluoromethane ND ug/kg 05/23/23 12:34 75-71-8 IH,v205/22/23 22:2258.3 5
1,1-Dichloroethane ND ug/kg 05/23/23 12:34 75-34-305/22/23 22:2229.2 5
1,2-Dichloroethane ND ug/kg 05/23/23 12:34 107-06-205/22/23 22:2229.2 5
1,1-Dichloroethene ND ug/kg 05/23/23 12:34 75-35-405/22/23 22:2229.2 5
cis-1,2-Dichloroethene ND ug/kg 05/23/23 12:34 156-59-205/22/23 22:2229.2 5
trans-1,2-Dichloroethene ND ug/kg 05/23/23 12:34 156-60-505/22/23 22:2229.2 5
1,2-Dichloropropane ND ug/kg 05/23/23 12:34 78-87-505/22/23 22:2229.2 5
1,3-Dichloropropane ND ug/kg 05/23/23 12:34 142-28-905/22/23 22:2229.2 5
2,2-Dichloropropane ND ug/kg 05/23/23 12:34 594-20-7 v205/22/23 22:2229.2 5
1,1-Dichloropropene ND ug/kg 05/23/23 12:34 563-58-605/22/23 22:2229.2 5
cis-1,3-Dichloropropene ND ug/kg 05/23/23 12:34 10061-01-505/22/23 22:2229.2 5
trans-1,3-Dichloropropene ND ug/kg 05/23/23 12:34 10061-02-605/22/23 22:2229.2 5
Diisopropyl ether ND ug/kg 05/23/23 12:34 108-20-305/22/23 22:2229.2 5
Ethylbenzene 2160 ug/kg 05/23/23 12:34 100-41-405/22/23 22:2229.2 5
Hexachloro-1,3-butadiene ND ug/kg 05/23/23 12:34 87-68-305/22/23 22:2258.3 5
2-Hexanone ND ug/kg 05/23/23 12:34 591-78-605/22/23 22:22292 5
Isopropylbenzene (Cumene)1340 ug/kg 05/23/23 12:34 98-82-805/22/23 22:2229.2 5
p-Isopropyltoluene 3700 ug/kg 05/23/23 12:34 99-87-605/22/23 22:2229.2 5
Methylene Chloride ND ug/kg 05/23/23 12:34 75-09-205/22/23 22:22117 5
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/23/23 12:34 108-10-105/22/23 22:22292 5
Methyl-tert-butyl ether ND ug/kg 05/23/23 12:34 1634-04-405/22/23 22:2229.2 5
Naphthalene 5130 ug/kg 05/23/23 12:34 91-20-305/22/23 22:2229.2 5
n-Propylbenzene 2830 ug/kg 05/23/23 12:34 103-65-105/22/23 22:2229.2 5
Styrene ND ug/kg 05/23/23 12:34 100-42-505/22/23 22:2229.2 5
1,1,1,2-Tetrachloroethane ND ug/kg 05/23/23 12:34 630-20-605/22/23 22:2229.2 5
1,1,2,2-Tetrachloroethane ND ug/kg 05/23/23 12:34 79-34-505/22/23 22:2229.2 5
Tetrachloroethene ND ug/kg 05/23/23 12:34 127-18-405/22/23 22:2229.2 5
Toluene ND ug/kg 05/23/23 12:34 108-88-305/22/23 22:2229.2 5
1,2,3-Trichlorobenzene ND ug/kg 05/23/23 12:34 87-61-605/22/23 22:2229.2 5
1,2,4-Trichlorobenzene ND ug/kg 05/23/23 12:34 120-82-105/22/23 22:2229.2 5
1,1,1-Trichloroethane ND ug/kg 05/23/23 12:34 71-55-605/22/23 22:2229.2 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-218 Lab ID: 92667253003 Collected: 05/12/23 08:50 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/23/23 12:34 79-00-505/22/23 22:2229.2 5
Trichloroethene ND ug/kg 05/23/23 12:34 79-01-605/22/23 22:2229.2 5
Trichlorofluoromethane ND ug/kg 05/23/23 12:34 75-69-405/22/23 22:2229.2 5
1,2,3-Trichloropropane ND ug/kg 05/23/23 12:34 96-18-405/22/23 22:2229.2 5
1,2,4-Trimethylbenzene 11200 ug/kg 05/23/23 12:34 95-63-605/22/23 22:2229.2 5
1,3,5-Trimethylbenzene 4010 ug/kg 05/23/23 12:34 108-67-805/22/23 22:2229.2 5
Vinyl acetate ND ug/kg 05/23/23 12:34 108-05-405/22/23 22:22292 5
Vinyl chloride ND ug/kg 05/23/23 12:34 75-01-405/22/23 22:2258.3 5
Xylene (Total)4060 ug/kg 05/23/23 12:34 1330-20-705/22/23 22:2258.3 5
m&p-Xylene 4010 ug/kg 05/23/23 12:34 179601-23-105/22/23 22:2258.3 5
o-Xylene 49.9 ug/kg 05/23/23 12:34 95-47-605/22/23 22:2229.2 5
Surrogates
Toluene-d8 (S) 102 %05/23/23 12:34 2037-26-5 D305/22/23 22:2270-130 5
4-Bromofluorobenzene (S) 110 %05/23/23 12:34 460-00-405/22/23 22:2270-130 5
1,2-Dichloroethane-d4 (S) 102 %05/23/23 12:34 17060-07-005/22/23 22:2270-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.0 %05/15/23 13:13 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-219 Lab ID: 92667253004 Collected: 05/12/23 09:00 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/17/23 13:06 83-32-905/16/23 14:28378 1
Acenaphthylene ND ug/kg 05/17/23 13:06 208-96-805/16/23 14:28378 1
Aniline ND ug/kg 05/17/23 13:06 62-53-305/16/23 14:28378 1
Anthracene ND ug/kg 05/17/23 13:06 120-12-705/16/23 14:28378 1
Benzo(a)anthracene ND ug/kg 05/17/23 13:06 56-55-305/16/23 14:28378 1
Benzo(a)pyrene ND ug/kg 05/17/23 13:06 50-32-805/16/23 14:28378 1
Benzo(b)fluoranthene ND ug/kg 05/17/23 13:06 205-99-205/16/23 14:28378 1
Benzo(g,h,i)perylene ND ug/kg 05/17/23 13:06 191-24-205/16/23 14:28378 1
Benzo(k)fluoranthene ND ug/kg 05/17/23 13:06 207-08-905/16/23 14:28378 1
Benzoic Acid ND ug/kg 05/17/23 13:06 65-85-005/16/23 14:281890 1
Benzyl alcohol ND ug/kg 05/17/23 13:06 100-51-605/16/23 14:28757 1
4-Bromophenylphenyl ether ND ug/kg 05/17/23 13:06 101-55-305/16/23 14:28378 1
Butylbenzylphthalate ND ug/kg 05/17/23 13:06 85-68-705/16/23 14:28378 1
4-Chloro-3-methylphenol ND ug/kg 05/17/23 13:06 59-50-705/16/23 14:28757 1
4-Chloroaniline ND ug/kg 05/17/23 13:06 106-47-805/16/23 14:28757 1
bis(2-Chloroethoxy)methane ND ug/kg 05/17/23 13:06 111-91-105/16/23 14:28378 1
bis(2-Chloroethyl) ether ND ug/kg 05/17/23 13:06 111-44-405/16/23 14:28378 1
2-Chloronaphthalene ND ug/kg 05/17/23 13:06 91-58-705/16/23 14:28378 1
2-Chlorophenol ND ug/kg 05/17/23 13:06 95-57-805/16/23 14:28378 1
4-Chlorophenylphenyl ether ND ug/kg 05/17/23 13:06 7005-72-305/16/23 14:28378 1
Chrysene ND ug/kg 05/17/23 13:06 218-01-905/16/23 14:28378 1
Dibenz(a,h)anthracene ND ug/kg 05/17/23 13:06 53-70-305/16/23 14:28378 1
Dibenzofuran ND ug/kg 05/17/23 13:06 132-64-905/16/23 14:28378 1
1,2-Dichlorobenzene ND ug/kg 05/17/23 13:06 95-50-105/16/23 14:28378 1
1,3-Dichlorobenzene ND ug/kg 05/17/23 13:06 541-73-105/16/23 14:28378 1
1,4-Dichlorobenzene ND ug/kg 05/17/23 13:06 106-46-705/16/23 14:28378 1
3,3'-Dichlorobenzidine ND ug/kg 05/17/23 13:06 91-94-105/16/23 14:28757 1
2,4-Dichlorophenol ND ug/kg 05/17/23 13:06 120-83-205/16/23 14:28378 1
Diethylphthalate ND ug/kg 05/17/23 13:06 84-66-205/16/23 14:28378 1
2,4-Dimethylphenol ND ug/kg 05/17/23 13:06 105-67-905/16/23 14:28378 1
Dimethylphthalate ND ug/kg 05/17/23 13:06 131-11-305/16/23 14:28378 1
Di-n-butylphthalate ND ug/kg 05/17/23 13:06 84-74-205/16/23 14:28378 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/23 13:06 534-52-105/16/23 14:28757 1
2,4-Dinitrophenol ND ug/kg 05/17/23 13:06 51-28-505/16/23 14:281890 1
2,4-Dinitrotoluene ND ug/kg 05/17/23 13:06 121-14-205/16/23 14:28378 1
2,6-Dinitrotoluene ND ug/kg 05/17/23 13:06 606-20-205/16/23 14:28378 1
Di-n-octylphthalate ND ug/kg 05/17/23 13:06 117-84-005/16/23 14:28378 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/23 13:06 117-81-705/16/23 14:28378 1
Fluoranthene ND ug/kg 05/17/23 13:06 206-44-005/16/23 14:28378 1
Fluorene ND ug/kg 05/17/23 13:06 86-73-705/16/23 14:28378 1
Hexachloro-1,3-butadiene ND ug/kg 05/17/23 13:06 87-68-305/16/23 14:28378 1
Hexachlorobenzene ND ug/kg 05/17/23 13:06 118-74-105/16/23 14:28378 1
Hexachlorocyclopentadiene ND ug/kg 05/17/23 13:06 77-47-405/16/23 14:28378 1
Hexachloroethane ND ug/kg 05/17/23 13:06 67-72-105/16/23 14:28378 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/23 13:06 193-39-505/16/23 14:28378 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-219 Lab ID: 92667253004 Collected: 05/12/23 09:00 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/17/23 13:06 78-59-105/16/23 14:28378 1
1-Methylnaphthalene 1220 ug/kg 05/17/23 13:06 90-12-005/16/23 14:28378 1
2-Methylnaphthalene 1830 ug/kg 05/17/23 13:06 91-57-605/16/23 14:28378 1
2-Methylphenol(o-Cresol) ND ug/kg 05/17/23 13:06 95-48-705/16/23 14:28378 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/17/23 13:06 15831-10-405/16/23 14:28378 1
Naphthalene 585 ug/kg 05/17/23 13:06 91-20-305/16/23 14:28378 1
2-Nitroaniline ND ug/kg 05/17/23 13:06 88-74-405/16/23 14:281890 1
3-Nitroaniline ND ug/kg 05/17/23 13:06 99-09-205/16/23 14:281890 1
4-Nitroaniline ND ug/kg 05/17/23 13:06 100-01-605/16/23 14:28757 1
Nitrobenzene ND ug/kg 05/17/23 13:06 98-95-305/16/23 14:28378 1
2-Nitrophenol ND ug/kg 05/17/23 13:06 88-75-505/16/23 14:28378 1
4-Nitrophenol ND ug/kg 05/17/23 13:06 100-02-705/16/23 14:281890 1
N-Nitrosodimethylamine ND ug/kg 05/17/23 13:06 62-75-905/16/23 14:28378 1
N-Nitroso-di-n-propylamine ND ug/kg 05/17/23 13:06 621-64-705/16/23 14:28378 1
N-Nitrosodiphenylamine ND ug/kg 05/17/23 13:06 86-30-605/16/23 14:28378 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/17/23 13:06 108-60-105/16/23 14:28378 1
Pentachlorophenol ND ug/kg 05/17/23 13:06 87-86-505/16/23 14:28757 1
Phenanthrene 386 ug/kg 05/17/23 13:06 85-01-805/16/23 14:28378 1
Phenol ND ug/kg 05/17/23 13:06 108-95-205/16/23 14:28378 1
Pyrene ND ug/kg 05/17/23 13:06 129-00-005/16/23 14:28378 1
Pyridine ND ug/kg 05/17/23 13:06 110-86-105/16/23 14:28378 1
1,2,4-Trichlorobenzene ND ug/kg 05/17/23 13:06 120-82-105/16/23 14:28378 1
2,4,5-Trichlorophenol ND ug/kg 05/17/23 13:06 95-95-405/16/23 14:28378 1
2,4,6-Trichlorophenol ND ug/kg 05/17/23 13:06 88-06-205/16/23 14:28378 1
Surrogates
Nitrobenzene-d5 (S) 69 %05/17/23 13:06 4165-60-005/16/23 14:2810-130 1
2-Fluorobiphenyl (S) 68 %05/17/23 13:06 321-60-805/16/23 14:2810-130 1
Terphenyl-d14 (S) 67 %05/17/23 13:06 1718-51-005/16/23 14:2810-130 1
Phenol-d6 (S) 60 %05/17/23 13:06 13127-88-305/16/23 14:2810-130 1
2-Fluorophenol (S) 65 %05/17/23 13:06 367-12-405/16/23 14:2810-130 1
2,4,6-Tribromophenol (S) 85 %05/17/23 13:06 118-79-605/16/23 14:2810-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/23/23 13:11 67-64-105/22/23 22:22502 5
Benzene ND ug/kg 05/23/23 13:11 71-43-205/22/23 22:2225.1 5
Bromobenzene ND ug/kg 05/23/23 13:11 108-86-105/22/23 22:2225.1 5
Bromochloromethane ND ug/kg 05/23/23 13:11 74-97-505/22/23 22:2225.1 5
Bromodichloromethane ND ug/kg 05/23/23 13:11 75-27-405/22/23 22:2225.1 5
Bromoform ND ug/kg 05/23/23 13:11 75-25-205/22/23 22:2225.1 5
Bromomethane ND ug/kg 05/23/23 13:11 74-83-9 v205/22/23 22:22100 5
2-Butanone (MEK) ND ug/kg 05/23/23 13:11 78-93-305/22/23 22:22502 5
n-Butylbenzene 1900 ug/kg 05/23/23 13:11 104-51-805/22/23 22:2225.1 5
sec-Butylbenzene 2330 ug/kg 05/23/23 13:11 135-98-805/22/23 22:2225.1 5
tert-Butylbenzene ND ug/kg 05/23/23 13:11 98-06-605/22/23 22:2225.1 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-219 Lab ID: 92667253004 Collected: 05/12/23 09:00 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/23/23 13:11 56-23-505/22/23 22:2225.1 5
Chlorobenzene ND ug/kg 05/23/23 13:11 108-90-705/22/23 22:2225.1 5
Chloroethane ND ug/kg 05/23/23 13:11 75-00-305/22/23 22:2250.2 5
Chloroform ND ug/kg 05/23/23 13:11 67-66-305/22/23 22:2225.1 5
Chloromethane 14700 ug/kg 05/23/23 13:11 74-87-305/22/23 22:2250.2 5
2-Chlorotoluene ND ug/kg 05/23/23 13:11 95-49-805/22/23 22:2225.1 5
4-Chlorotoluene ND ug/kg 05/23/23 13:11 106-43-405/22/23 22:2225.1 5
1,2-Dibromo-3-chloropropane ND ug/kg 05/23/23 13:11 96-12-805/22/23 22:2225.1 5
Dibromochloromethane ND ug/kg 05/23/23 13:11 124-48-105/22/23 22:2225.1 5
1,2-Dibromoethane (EDB) ND ug/kg 05/23/23 13:11 106-93-405/22/23 22:2225.1 5
Dibromomethane ND ug/kg 05/23/23 13:11 74-95-305/22/23 22:2225.1 5
1,2-Dichlorobenzene ND ug/kg 05/23/23 13:11 95-50-105/22/23 22:2225.1 5
1,3-Dichlorobenzene ND ug/kg 05/23/23 13:11 541-73-105/22/23 22:2225.1 5
1,4-Dichlorobenzene ND ug/kg 05/23/23 13:11 106-46-705/22/23 22:2225.1 5
Dichlorodifluoromethane ND ug/kg 05/23/23 13:11 75-71-8 IH,v205/22/23 22:2250.2 5
1,1-Dichloroethane ND ug/kg 05/23/23 13:11 75-34-305/22/23 22:2225.1 5
1,2-Dichloroethane ND ug/kg 05/23/23 13:11 107-06-205/22/23 22:2225.1 5
1,1-Dichloroethene ND ug/kg 05/23/23 13:11 75-35-405/22/23 22:2225.1 5
cis-1,2-Dichloroethene ND ug/kg 05/23/23 13:11 156-59-205/22/23 22:2225.1 5
trans-1,2-Dichloroethene ND ug/kg 05/23/23 13:11 156-60-505/22/23 22:2225.1 5
1,2-Dichloropropane ND ug/kg 05/23/23 13:11 78-87-505/22/23 22:2225.1 5
1,3-Dichloropropane ND ug/kg 05/23/23 13:11 142-28-905/22/23 22:2225.1 5
2,2-Dichloropropane ND ug/kg 05/23/23 13:11 594-20-7 v205/22/23 22:2225.1 5
1,1-Dichloropropene ND ug/kg 05/23/23 13:11 563-58-605/22/23 22:2225.1 5
cis-1,3-Dichloropropene ND ug/kg 05/23/23 13:11 10061-01-505/22/23 22:2225.1 5
trans-1,3-Dichloropropene ND ug/kg 05/23/23 13:11 10061-02-605/22/23 22:2225.1 5
Diisopropyl ether ND ug/kg 05/23/23 13:11 108-20-305/22/23 22:2225.1 5
Ethylbenzene 60.3 ug/kg 05/23/23 13:11 100-41-405/22/23 22:2225.1 5
Hexachloro-1,3-butadiene ND ug/kg 05/23/23 13:11 87-68-305/22/23 22:2250.2 5
2-Hexanone ND ug/kg 05/23/23 13:11 591-78-605/22/23 22:22251 5
Isopropylbenzene (Cumene)1440 ug/kg 05/23/23 13:11 98-82-805/22/23 22:2225.1 5
p-Isopropyltoluene ND ug/kg 05/23/23 13:11 99-87-605/22/23 22:2225.1 5
Methylene Chloride ND ug/kg 05/23/23 13:11 75-09-205/22/23 22:22100 5
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/23/23 13:11 108-10-105/22/23 22:22251 5
Methyl-tert-butyl ether ND ug/kg 05/23/23 13:11 1634-04-405/22/23 22:2225.1 5
Naphthalene 4580 ug/kg 05/23/23 13:11 91-20-305/22/23 22:2225.1 5
n-Propylbenzene 2980 ug/kg 05/23/23 13:11 103-65-105/22/23 22:2225.1 5
Styrene ND ug/kg 05/23/23 13:11 100-42-505/22/23 22:2225.1 5
1,1,1,2-Tetrachloroethane ND ug/kg 05/23/23 13:11 630-20-605/22/23 22:2225.1 5
1,1,2,2-Tetrachloroethane ND ug/kg 05/23/23 13:11 79-34-505/22/23 22:2225.1 5
Tetrachloroethene ND ug/kg 05/23/23 13:11 127-18-405/22/23 22:2225.1 5
Toluene ND ug/kg 05/23/23 13:11 108-88-305/22/23 22:2225.1 5
1,2,3-Trichlorobenzene ND ug/kg 05/23/23 13:11 87-61-605/22/23 22:2225.1 5
1,2,4-Trichlorobenzene ND ug/kg 05/23/23 13:11 120-82-105/22/23 22:2225.1 5
1,1,1-Trichloroethane ND ug/kg 05/23/23 13:11 71-55-605/22/23 22:2225.1 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-219 Lab ID: 92667253004 Collected: 05/12/23 09:00 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/23/23 13:11 79-00-505/22/23 22:2225.1 5
Trichloroethene ND ug/kg 05/23/23 13:11 79-01-605/22/23 22:2225.1 5
Trichlorofluoromethane ND ug/kg 05/23/23 13:11 75-69-405/22/23 22:2225.1 5
1,2,3-Trichloropropane ND ug/kg 05/23/23 13:11 96-18-405/22/23 22:2225.1 5
1,2,4-Trimethylbenzene ND ug/kg 05/23/23 13:11 95-63-605/22/23 22:2225.1 5
1,3,5-Trimethylbenzene ND ug/kg 05/23/23 13:11 108-67-805/22/23 22:2225.1 5
Vinyl acetate ND ug/kg 05/23/23 13:11 108-05-405/22/23 22:22251 5
Vinyl chloride ND ug/kg 05/23/23 13:11 75-01-405/22/23 22:2250.2 5
Xylene (Total) ND ug/kg 05/23/23 13:11 1330-20-705/22/23 22:2250.2 5
m&p-Xylene ND ug/kg 05/23/23 13:11 179601-23-105/22/23 22:2250.2 5
o-Xylene ND ug/kg 05/23/23 13:11 95-47-605/22/23 22:2225.1 5
Surrogates
Toluene-d8 (S) 102 %05/23/23 13:11 2037-26-505/22/23 22:2270-130 5
4-Bromofluorobenzene (S) 113 %05/23/23 13:11 460-00-405/22/23 22:2270-130 5
1,2-Dichloroethane-d4 (S) 100 %05/23/23 13:11 17060-07-005/22/23 22:2270-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.1 %05/15/23 13:13 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-220 Lab ID: 92667253005 Collected: 05/12/23 09:15 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/17/23 13:34 83-32-905/16/23 14:28389 1
Acenaphthylene ND ug/kg 05/17/23 13:34 208-96-805/16/23 14:28389 1
Aniline ND ug/kg 05/17/23 13:34 62-53-305/16/23 14:28389 1
Anthracene ND ug/kg 05/17/23 13:34 120-12-705/16/23 14:28389 1
Benzo(a)anthracene ND ug/kg 05/17/23 13:34 56-55-305/16/23 14:28389 1
Benzo(a)pyrene ND ug/kg 05/17/23 13:34 50-32-805/16/23 14:28389 1
Benzo(b)fluoranthene ND ug/kg 05/17/23 13:34 205-99-205/16/23 14:28389 1
Benzo(g,h,i)perylene ND ug/kg 05/17/23 13:34 191-24-205/16/23 14:28389 1
Benzo(k)fluoranthene ND ug/kg 05/17/23 13:34 207-08-905/16/23 14:28389 1
Benzoic Acid ND ug/kg 05/17/23 13:34 65-85-005/16/23 14:281940 1
Benzyl alcohol ND ug/kg 05/17/23 13:34 100-51-605/16/23 14:28777 1
4-Bromophenylphenyl ether ND ug/kg 05/17/23 13:34 101-55-305/16/23 14:28389 1
Butylbenzylphthalate ND ug/kg 05/17/23 13:34 85-68-705/16/23 14:28389 1
4-Chloro-3-methylphenol ND ug/kg 05/17/23 13:34 59-50-705/16/23 14:28777 1
4-Chloroaniline ND ug/kg 05/17/23 13:34 106-47-805/16/23 14:28777 1
bis(2-Chloroethoxy)methane ND ug/kg 05/17/23 13:34 111-91-105/16/23 14:28389 1
bis(2-Chloroethyl) ether ND ug/kg 05/17/23 13:34 111-44-405/16/23 14:28389 1
2-Chloronaphthalene ND ug/kg 05/17/23 13:34 91-58-705/16/23 14:28389 1
2-Chlorophenol ND ug/kg 05/17/23 13:34 95-57-805/16/23 14:28389 1
4-Chlorophenylphenyl ether ND ug/kg 05/17/23 13:34 7005-72-305/16/23 14:28389 1
Chrysene ND ug/kg 05/17/23 13:34 218-01-905/16/23 14:28389 1
Dibenz(a,h)anthracene ND ug/kg 05/17/23 13:34 53-70-305/16/23 14:28389 1
Dibenzofuran ND ug/kg 05/17/23 13:34 132-64-905/16/23 14:28389 1
1,2-Dichlorobenzene ND ug/kg 05/17/23 13:34 95-50-105/16/23 14:28389 1
1,3-Dichlorobenzene ND ug/kg 05/17/23 13:34 541-73-105/16/23 14:28389 1
1,4-Dichlorobenzene ND ug/kg 05/17/23 13:34 106-46-705/16/23 14:28389 1
3,3'-Dichlorobenzidine ND ug/kg 05/17/23 13:34 91-94-105/16/23 14:28777 1
2,4-Dichlorophenol ND ug/kg 05/17/23 13:34 120-83-205/16/23 14:28389 1
Diethylphthalate ND ug/kg 05/17/23 13:34 84-66-205/16/23 14:28389 1
2,4-Dimethylphenol ND ug/kg 05/17/23 13:34 105-67-905/16/23 14:28389 1
Dimethylphthalate ND ug/kg 05/17/23 13:34 131-11-305/16/23 14:28389 1
Di-n-butylphthalate ND ug/kg 05/17/23 13:34 84-74-205/16/23 14:28389 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/23 13:34 534-52-105/16/23 14:28777 1
2,4-Dinitrophenol ND ug/kg 05/17/23 13:34 51-28-505/16/23 14:281940 1
2,4-Dinitrotoluene ND ug/kg 05/17/23 13:34 121-14-205/16/23 14:28389 1
2,6-Dinitrotoluene ND ug/kg 05/17/23 13:34 606-20-205/16/23 14:28389 1
Di-n-octylphthalate ND ug/kg 05/17/23 13:34 117-84-005/16/23 14:28389 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/23 13:34 117-81-705/16/23 14:28389 1
Fluoranthene ND ug/kg 05/17/23 13:34 206-44-005/16/23 14:28389 1
Fluorene ND ug/kg 05/17/23 13:34 86-73-705/16/23 14:28389 1
Hexachloro-1,3-butadiene ND ug/kg 05/17/23 13:34 87-68-305/16/23 14:28389 1
Hexachlorobenzene ND ug/kg 05/17/23 13:34 118-74-105/16/23 14:28389 1
Hexachlorocyclopentadiene ND ug/kg 05/17/23 13:34 77-47-405/16/23 14:28389 1
Hexachloroethane ND ug/kg 05/17/23 13:34 67-72-105/16/23 14:28389 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/23 13:34 193-39-505/16/23 14:28389 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-220 Lab ID: 92667253005 Collected: 05/12/23 09:15 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/17/23 13:34 78-59-105/16/23 14:28389 1
1-Methylnaphthalene ND ug/kg 05/17/23 13:34 90-12-005/16/23 14:28389 1
2-Methylnaphthalene 403 ug/kg 05/17/23 13:34 91-57-605/16/23 14:28389 1
2-Methylphenol(o-Cresol) ND ug/kg 05/17/23 13:34 95-48-705/16/23 14:28389 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/17/23 13:34 15831-10-405/16/23 14:28389 1
Naphthalene ND ug/kg 05/17/23 13:34 91-20-305/16/23 14:28389 1
2-Nitroaniline ND ug/kg 05/17/23 13:34 88-74-405/16/23 14:281940 1
3-Nitroaniline ND ug/kg 05/17/23 13:34 99-09-205/16/23 14:281940 1
4-Nitroaniline ND ug/kg 05/17/23 13:34 100-01-605/16/23 14:28777 1
Nitrobenzene ND ug/kg 05/17/23 13:34 98-95-305/16/23 14:28389 1
2-Nitrophenol ND ug/kg 05/17/23 13:34 88-75-505/16/23 14:28389 1
4-Nitrophenol ND ug/kg 05/17/23 13:34 100-02-705/16/23 14:281940 1
N-Nitrosodimethylamine ND ug/kg 05/17/23 13:34 62-75-905/16/23 14:28389 1
N-Nitroso-di-n-propylamine ND ug/kg 05/17/23 13:34 621-64-705/16/23 14:28389 1
N-Nitrosodiphenylamine ND ug/kg 05/17/23 13:34 86-30-605/16/23 14:28389 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/17/23 13:34 108-60-105/16/23 14:28389 1
Pentachlorophenol ND ug/kg 05/17/23 13:34 87-86-505/16/23 14:28777 1
Phenanthrene ND ug/kg 05/17/23 13:34 85-01-805/16/23 14:28389 1
Phenol ND ug/kg 05/17/23 13:34 108-95-205/16/23 14:28389 1
Pyrene ND ug/kg 05/17/23 13:34 129-00-005/16/23 14:28389 1
Pyridine ND ug/kg 05/17/23 13:34 110-86-105/16/23 14:28389 1
1,2,4-Trichlorobenzene ND ug/kg 05/17/23 13:34 120-82-105/16/23 14:28389 1
2,4,5-Trichlorophenol ND ug/kg 05/17/23 13:34 95-95-405/16/23 14:28389 1
2,4,6-Trichlorophenol ND ug/kg 05/17/23 13:34 88-06-205/16/23 14:28389 1
Surrogates
Nitrobenzene-d5 (S) 60 %05/17/23 13:34 4165-60-005/16/23 14:2810-130 1
2-Fluorobiphenyl (S) 56 %05/17/23 13:34 321-60-805/16/23 14:2810-130 1
Terphenyl-d14 (S) 61 %05/17/23 13:34 1718-51-005/16/23 14:2810-130 1
Phenol-d6 (S) 50 %05/17/23 13:34 13127-88-305/16/23 14:2810-130 1
2-Fluorophenol (S) 53 %05/17/23 13:34 367-12-405/16/23 14:2810-130 1
2,4,6-Tribromophenol (S) 69 %05/17/23 13:34 118-79-605/16/23 14:2810-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/19/23 05:02 67-64-105/18/23 22:28106 1
Benzene ND ug/kg 05/19/23 05:02 71-43-205/18/23 22:285.3 1
Bromobenzene ND ug/kg 05/19/23 05:02 108-86-105/18/23 22:285.3 1
Bromochloromethane ND ug/kg 05/19/23 05:02 74-97-505/18/23 22:285.3 1
Bromodichloromethane ND ug/kg 05/19/23 05:02 75-27-405/18/23 22:285.3 1
Bromoform ND ug/kg 05/19/23 05:02 75-25-205/18/23 22:285.3 1
Bromomethane ND ug/kg 05/19/23 05:02 74-83-905/18/23 22:2821.3 1
2-Butanone (MEK) ND ug/kg 05/19/23 05:02 78-93-305/18/23 22:28106 1
n-Butylbenzene 1180 ug/kg 05/19/23 05:02 104-51-805/18/23 22:285.3 1
sec-Butylbenzene 1220 ug/kg 05/19/23 05:02 135-98-805/18/23 22:285.3 1
tert-Butylbenzene ND ug/kg 05/19/23 05:02 98-06-605/18/23 22:285.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-220 Lab ID: 92667253005 Collected: 05/12/23 09:15 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/19/23 05:02 56-23-505/18/23 22:285.3 1
Chlorobenzene ND ug/kg 05/19/23 05:02 108-90-705/18/23 22:285.3 1
Chloroethane ND ug/kg 05/19/23 05:02 75-00-305/18/23 22:2810.6 1
Chloroform ND ug/kg 05/19/23 05:02 67-66-305/18/23 22:285.3 1
Chloromethane ND ug/kg 05/19/23 05:02 74-87-305/18/23 22:2810.6 1
2-Chlorotoluene ND ug/kg 05/19/23 05:02 95-49-805/18/23 22:285.3 1
4-Chlorotoluene ND ug/kg 05/19/23 05:02 106-43-405/18/23 22:285.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/19/23 05:02 96-12-805/18/23 22:285.3 1
Dibromochloromethane ND ug/kg 05/19/23 05:02 124-48-105/18/23 22:285.3 1
1,2-Dibromoethane (EDB) ND ug/kg 05/19/23 05:02 106-93-405/18/23 22:285.3 1
Dibromomethane ND ug/kg 05/19/23 05:02 74-95-305/18/23 22:285.3 1
1,2-Dichlorobenzene ND ug/kg 05/19/23 05:02 95-50-105/18/23 22:285.3 1
1,3-Dichlorobenzene ND ug/kg 05/19/23 05:02 541-73-105/18/23 22:285.3 1
1,4-Dichlorobenzene ND ug/kg 05/19/23 05:02 106-46-705/18/23 22:285.3 1
Dichlorodifluoromethane ND ug/kg 05/19/23 05:02 75-71-8 IH05/18/23 22:2810.6 1
1,1-Dichloroethane ND ug/kg 05/19/23 05:02 75-34-305/18/23 22:285.3 1
1,2-Dichloroethane ND ug/kg 05/19/23 05:02 107-06-205/18/23 22:285.3 1
1,1-Dichloroethene ND ug/kg 05/19/23 05:02 75-35-405/18/23 22:285.3 1
cis-1,2-Dichloroethene ND ug/kg 05/19/23 05:02 156-59-205/18/23 22:285.3 1
trans-1,2-Dichloroethene ND ug/kg 05/19/23 05:02 156-60-505/18/23 22:285.3 1
1,2-Dichloropropane ND ug/kg 05/19/23 05:02 78-87-505/18/23 22:285.3 1
1,3-Dichloropropane ND ug/kg 05/19/23 05:02 142-28-905/18/23 22:285.3 1
2,2-Dichloropropane ND ug/kg 05/19/23 05:02 594-20-705/18/23 22:285.3 1
1,1-Dichloropropene ND ug/kg 05/19/23 05:02 563-58-605/18/23 22:285.3 1
cis-1,3-Dichloropropene ND ug/kg 05/19/23 05:02 10061-01-505/18/23 22:285.3 1
trans-1,3-Dichloropropene ND ug/kg 05/19/23 05:02 10061-02-605/18/23 22:285.3 1
Diisopropyl ether ND ug/kg 05/19/23 05:02 108-20-305/18/23 22:285.3 1
Ethylbenzene 8.9 ug/kg 05/19/23 05:02 100-41-405/18/23 22:285.3 1
Hexachloro-1,3-butadiene ND ug/kg 05/19/23 05:02 87-68-305/18/23 22:2810.6 1
2-Hexanone ND ug/kg 05/19/23 05:02 591-78-605/18/23 22:2853.2 1
Isopropylbenzene (Cumene)451 ug/kg 05/19/23 05:02 98-82-805/18/23 22:285.3 1
p-Isopropyltoluene ND ug/kg 05/19/23 05:02 99-87-605/18/23 22:285.3 1
Methylene Chloride ND ug/kg 05/19/23 05:02 75-09-205/18/23 22:2821.3 1
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/19/23 05:02 108-10-105/18/23 22:2853.2 1
Methyl-tert-butyl ether ND ug/kg 05/19/23 05:02 1634-04-405/18/23 22:285.3 1
Naphthalene ND ug/kg 05/19/23 05:02 91-20-305/18/23 22:285.3 1
n-Propylbenzene 1140 ug/kg 05/19/23 05:02 103-65-105/18/23 22:285.3 1
Styrene ND ug/kg 05/19/23 05:02 100-42-505/18/23 22:285.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/19/23 05:02 630-20-605/18/23 22:285.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/19/23 05:02 79-34-505/18/23 22:285.3 1
Tetrachloroethene ND ug/kg 05/19/23 05:02 127-18-405/18/23 22:285.3 1
Toluene ND ug/kg 05/19/23 05:02 108-88-305/18/23 22:285.3 1
1,2,3-Trichlorobenzene ND ug/kg 05/19/23 05:02 87-61-605/18/23 22:285.3 1
1,2,4-Trichlorobenzene ND ug/kg 05/19/23 05:02 120-82-105/18/23 22:285.3 1
1,1,1-Trichloroethane ND ug/kg 05/19/23 05:02 71-55-605/18/23 22:285.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-220 Lab ID: 92667253005 Collected: 05/12/23 09:15 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/19/23 05:02 79-00-505/18/23 22:285.3 1
Trichloroethene ND ug/kg 05/19/23 05:02 79-01-605/18/23 22:285.3 1
Trichlorofluoromethane ND ug/kg 05/19/23 05:02 75-69-405/18/23 22:285.3 1
1,2,3-Trichloropropane ND ug/kg 05/19/23 05:02 96-18-405/18/23 22:285.3 1
1,2,4-Trimethylbenzene ND ug/kg 05/19/23 05:02 95-63-605/18/23 22:285.3 1
1,3,5-Trimethylbenzene ND ug/kg 05/19/23 05:02 108-67-805/18/23 22:285.3 1
Vinyl acetate ND ug/kg 05/19/23 05:02 108-05-405/18/23 22:2853.2 1
Vinyl chloride ND ug/kg 05/19/23 05:02 75-01-405/18/23 22:2810.6 1
Xylene (Total) ND ug/kg 05/19/23 05:02 1330-20-705/18/23 22:2810.6 1
m&p-Xylene ND ug/kg 05/19/23 05:02 179601-23-105/18/23 22:2810.6 1
o-Xylene ND ug/kg 05/19/23 05:02 95-47-605/18/23 22:285.3 1
Surrogates
Toluene-d8 (S) 104 %05/19/23 05:02 2037-26-505/18/23 22:2870-130 1
4-Bromofluorobenzene (S) 118 %05/19/23 05:02 460-00-405/18/23 22:2870-130 1
1,2-Dichloroethane-d4 (S) 101 %05/19/23 05:02 17060-07-005/18/23 22:2870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.5 %05/15/23 14:04 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-221 Lab ID: 92667253006 Collected: 05/12/23 09:35 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/17/23 14:03 83-32-905/16/23 14:28399 1
Acenaphthylene ND ug/kg 05/17/23 14:03 208-96-805/16/23 14:28399 1
Aniline ND ug/kg 05/17/23 14:03 62-53-305/16/23 14:28399 1
Anthracene ND ug/kg 05/17/23 14:03 120-12-705/16/23 14:28399 1
Benzo(a)anthracene ND ug/kg 05/17/23 14:03 56-55-305/16/23 14:28399 1
Benzo(a)pyrene ND ug/kg 05/17/23 14:03 50-32-805/16/23 14:28399 1
Benzo(b)fluoranthene ND ug/kg 05/17/23 14:03 205-99-205/16/23 14:28399 1
Benzo(g,h,i)perylene ND ug/kg 05/17/23 14:03 191-24-205/16/23 14:28399 1
Benzo(k)fluoranthene ND ug/kg 05/17/23 14:03 207-08-905/16/23 14:28399 1
Benzoic Acid ND ug/kg 05/17/23 14:03 65-85-005/16/23 14:282000 1
Benzyl alcohol ND ug/kg 05/17/23 14:03 100-51-605/16/23 14:28798 1
4-Bromophenylphenyl ether ND ug/kg 05/17/23 14:03 101-55-305/16/23 14:28399 1
Butylbenzylphthalate ND ug/kg 05/17/23 14:03 85-68-705/16/23 14:28399 1
4-Chloro-3-methylphenol ND ug/kg 05/17/23 14:03 59-50-705/16/23 14:28798 1
4-Chloroaniline ND ug/kg 05/17/23 14:03 106-47-805/16/23 14:28798 1
bis(2-Chloroethoxy)methane ND ug/kg 05/17/23 14:03 111-91-105/16/23 14:28399 1
bis(2-Chloroethyl) ether ND ug/kg 05/17/23 14:03 111-44-405/16/23 14:28399 1
2-Chloronaphthalene ND ug/kg 05/17/23 14:03 91-58-705/16/23 14:28399 1
2-Chlorophenol ND ug/kg 05/17/23 14:03 95-57-805/16/23 14:28399 1
4-Chlorophenylphenyl ether ND ug/kg 05/17/23 14:03 7005-72-305/16/23 14:28399 1
Chrysene ND ug/kg 05/17/23 14:03 218-01-905/16/23 14:28399 1
Dibenz(a,h)anthracene ND ug/kg 05/17/23 14:03 53-70-305/16/23 14:28399 1
Dibenzofuran ND ug/kg 05/17/23 14:03 132-64-905/16/23 14:28399 1
1,2-Dichlorobenzene ND ug/kg 05/17/23 14:03 95-50-105/16/23 14:28399 1
1,3-Dichlorobenzene ND ug/kg 05/17/23 14:03 541-73-105/16/23 14:28399 1
1,4-Dichlorobenzene ND ug/kg 05/17/23 14:03 106-46-705/16/23 14:28399 1
3,3'-Dichlorobenzidine ND ug/kg 05/17/23 14:03 91-94-105/16/23 14:28798 1
2,4-Dichlorophenol ND ug/kg 05/17/23 14:03 120-83-205/16/23 14:28399 1
Diethylphthalate ND ug/kg 05/17/23 14:03 84-66-205/16/23 14:28399 1
2,4-Dimethylphenol ND ug/kg 05/17/23 14:03 105-67-905/16/23 14:28399 1
Dimethylphthalate ND ug/kg 05/17/23 14:03 131-11-305/16/23 14:28399 1
Di-n-butylphthalate ND ug/kg 05/17/23 14:03 84-74-205/16/23 14:28399 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/23 14:03 534-52-105/16/23 14:28798 1
2,4-Dinitrophenol ND ug/kg 05/17/23 14:03 51-28-505/16/23 14:282000 1
2,4-Dinitrotoluene ND ug/kg 05/17/23 14:03 121-14-205/16/23 14:28399 1
2,6-Dinitrotoluene ND ug/kg 05/17/23 14:03 606-20-205/16/23 14:28399 1
Di-n-octylphthalate ND ug/kg 05/17/23 14:03 117-84-005/16/23 14:28399 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/23 14:03 117-81-705/16/23 14:28399 1
Fluoranthene ND ug/kg 05/17/23 14:03 206-44-005/16/23 14:28399 1
Fluorene ND ug/kg 05/17/23 14:03 86-73-705/16/23 14:28399 1
Hexachloro-1,3-butadiene ND ug/kg 05/17/23 14:03 87-68-305/16/23 14:28399 1
Hexachlorobenzene ND ug/kg 05/17/23 14:03 118-74-105/16/23 14:28399 1
Hexachlorocyclopentadiene ND ug/kg 05/17/23 14:03 77-47-405/16/23 14:28399 1
Hexachloroethane ND ug/kg 05/17/23 14:03 67-72-105/16/23 14:28399 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/23 14:03 193-39-505/16/23 14:28399 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-221 Lab ID: 92667253006 Collected: 05/12/23 09:35 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/17/23 14:03 78-59-105/16/23 14:28399 1
1-Methylnaphthalene ND ug/kg 05/17/23 14:03 90-12-005/16/23 14:28399 1
2-Methylnaphthalene ND ug/kg 05/17/23 14:03 91-57-605/16/23 14:28399 1
2-Methylphenol(o-Cresol) ND ug/kg 05/17/23 14:03 95-48-705/16/23 14:28399 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/17/23 14:03 15831-10-405/16/23 14:28399 1
Naphthalene ND ug/kg 05/17/23 14:03 91-20-305/16/23 14:28399 1
2-Nitroaniline ND ug/kg 05/17/23 14:03 88-74-405/16/23 14:282000 1
3-Nitroaniline ND ug/kg 05/17/23 14:03 99-09-205/16/23 14:282000 1
4-Nitroaniline ND ug/kg 05/17/23 14:03 100-01-605/16/23 14:28798 1
Nitrobenzene ND ug/kg 05/17/23 14:03 98-95-305/16/23 14:28399 1
2-Nitrophenol ND ug/kg 05/17/23 14:03 88-75-505/16/23 14:28399 1
4-Nitrophenol ND ug/kg 05/17/23 14:03 100-02-705/16/23 14:282000 1
N-Nitrosodimethylamine ND ug/kg 05/17/23 14:03 62-75-905/16/23 14:28399 1
N-Nitroso-di-n-propylamine ND ug/kg 05/17/23 14:03 621-64-705/16/23 14:28399 1
N-Nitrosodiphenylamine ND ug/kg 05/17/23 14:03 86-30-605/16/23 14:28399 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/17/23 14:03 108-60-105/16/23 14:28399 1
Pentachlorophenol ND ug/kg 05/17/23 14:03 87-86-505/16/23 14:28798 1
Phenanthrene ND ug/kg 05/17/23 14:03 85-01-805/16/23 14:28399 1
Phenol ND ug/kg 05/17/23 14:03 108-95-205/16/23 14:28399 1
Pyrene ND ug/kg 05/17/23 14:03 129-00-005/16/23 14:28399 1
Pyridine ND ug/kg 05/17/23 14:03 110-86-105/16/23 14:28399 1
1,2,4-Trichlorobenzene ND ug/kg 05/17/23 14:03 120-82-105/16/23 14:28399 1
2,4,5-Trichlorophenol ND ug/kg 05/17/23 14:03 95-95-405/16/23 14:28399 1
2,4,6-Trichlorophenol ND ug/kg 05/17/23 14:03 88-06-205/16/23 14:28399 1
Surrogates
Nitrobenzene-d5 (S) 63 %05/17/23 14:03 4165-60-005/16/23 14:2810-130 1
2-Fluorobiphenyl (S) 64 %05/17/23 14:03 321-60-805/16/23 14:2810-130 1
Terphenyl-d14 (S) 69 %05/17/23 14:03 1718-51-005/16/23 14:2810-130 1
Phenol-d6 (S) 57 %05/17/23 14:03 13127-88-305/16/23 14:2810-130 1
2-Fluorophenol (S) 59 %05/17/23 14:03 367-12-405/16/23 14:2810-130 1
2,4,6-Tribromophenol (S) 77 %05/17/23 14:03 118-79-605/16/23 14:2810-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/19/23 05:20 67-64-105/18/23 22:28117 1
Benzene ND ug/kg 05/19/23 05:20 71-43-205/18/23 22:285.9 1
Bromobenzene ND ug/kg 05/19/23 05:20 108-86-105/18/23 22:285.9 1
Bromochloromethane ND ug/kg 05/19/23 05:20 74-97-505/18/23 22:285.9 1
Bromodichloromethane ND ug/kg 05/19/23 05:20 75-27-405/18/23 22:285.9 1
Bromoform ND ug/kg 05/19/23 05:20 75-25-205/18/23 22:285.9 1
Bromomethane ND ug/kg 05/19/23 05:20 74-83-905/18/23 22:2823.4 1
2-Butanone (MEK) ND ug/kg 05/19/23 05:20 78-93-305/18/23 22:28117 1
n-Butylbenzene 514 ug/kg 05/19/23 05:20 104-51-805/18/23 22:285.9 1
sec-Butylbenzene 1030 ug/kg 05/19/23 05:20 135-98-805/18/23 22:285.9 1
tert-Butylbenzene ND ug/kg 05/19/23 05:20 98-06-605/18/23 22:285.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-221 Lab ID: 92667253006 Collected: 05/12/23 09:35 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/19/23 05:20 56-23-505/18/23 22:285.9 1
Chlorobenzene ND ug/kg 05/19/23 05:20 108-90-705/18/23 22:285.9 1
Chloroethane ND ug/kg 05/19/23 05:20 75-00-305/18/23 22:2811.7 1
Chloroform ND ug/kg 05/19/23 05:20 67-66-305/18/23 22:285.9 1
Chloromethane ND ug/kg 05/19/23 05:20 74-87-305/18/23 22:2811.7 1
2-Chlorotoluene ND ug/kg 05/19/23 05:20 95-49-805/18/23 22:285.9 1
4-Chlorotoluene ND ug/kg 05/19/23 05:20 106-43-405/18/23 22:285.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/19/23 05:20 96-12-805/18/23 22:285.9 1
Dibromochloromethane ND ug/kg 05/19/23 05:20 124-48-105/18/23 22:285.9 1
1,2-Dibromoethane (EDB) ND ug/kg 05/19/23 05:20 106-93-405/18/23 22:285.9 1
Dibromomethane ND ug/kg 05/19/23 05:20 74-95-305/18/23 22:285.9 1
1,2-Dichlorobenzene ND ug/kg 05/19/23 05:20 95-50-105/18/23 22:285.9 1
1,3-Dichlorobenzene ND ug/kg 05/19/23 05:20 541-73-105/18/23 22:285.9 1
1,4-Dichlorobenzene ND ug/kg 05/19/23 05:20 106-46-705/18/23 22:285.9 1
Dichlorodifluoromethane ND ug/kg 05/19/23 05:20 75-71-8 IH05/18/23 22:2811.7 1
1,1-Dichloroethane ND ug/kg 05/19/23 05:20 75-34-305/18/23 22:285.9 1
1,2-Dichloroethane ND ug/kg 05/19/23 05:20 107-06-205/18/23 22:285.9 1
1,1-Dichloroethene ND ug/kg 05/19/23 05:20 75-35-405/18/23 22:285.9 1
cis-1,2-Dichloroethene ND ug/kg 05/19/23 05:20 156-59-205/18/23 22:285.9 1
trans-1,2-Dichloroethene ND ug/kg 05/19/23 05:20 156-60-505/18/23 22:285.9 1
1,2-Dichloropropane ND ug/kg 05/19/23 05:20 78-87-505/18/23 22:285.9 1
1,3-Dichloropropane ND ug/kg 05/19/23 05:20 142-28-905/18/23 22:285.9 1
2,2-Dichloropropane ND ug/kg 05/19/23 05:20 594-20-705/18/23 22:285.9 1
1,1-Dichloropropene ND ug/kg 05/19/23 05:20 563-58-605/18/23 22:285.9 1
cis-1,3-Dichloropropene ND ug/kg 05/19/23 05:20 10061-01-505/18/23 22:285.9 1
trans-1,3-Dichloropropene ND ug/kg 05/19/23 05:20 10061-02-605/18/23 22:285.9 1
Diisopropyl ether ND ug/kg 05/19/23 05:20 108-20-305/18/23 22:285.9 1
Ethylbenzene ND ug/kg 05/19/23 05:20 100-41-405/18/23 22:285.9 1
Hexachloro-1,3-butadiene ND ug/kg 05/19/23 05:20 87-68-305/18/23 22:2811.7 1
2-Hexanone ND ug/kg 05/19/23 05:20 591-78-605/18/23 22:2858.6 1
Isopropylbenzene (Cumene)111 ug/kg 05/19/23 05:20 98-82-805/18/23 22:285.9 1
p-Isopropyltoluene ND ug/kg 05/19/23 05:20 99-87-605/18/23 22:285.9 1
Methylene Chloride ND ug/kg 05/19/23 05:20 75-09-205/18/23 22:2823.4 1
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/19/23 05:20 108-10-105/18/23 22:2858.6 1
Methyl-tert-butyl ether ND ug/kg 05/19/23 05:20 1634-04-405/18/23 22:285.9 1
Naphthalene ND ug/kg 05/19/23 05:20 91-20-305/18/23 22:285.9 1
n-Propylbenzene 184 ug/kg 05/19/23 05:20 103-65-105/18/23 22:285.9 1
Styrene ND ug/kg 05/19/23 05:20 100-42-505/18/23 22:285.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/19/23 05:20 630-20-605/18/23 22:285.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/19/23 05:20 79-34-505/18/23 22:285.9 1
Tetrachloroethene ND ug/kg 05/19/23 05:20 127-18-405/18/23 22:285.9 1
Toluene ND ug/kg 05/19/23 05:20 108-88-305/18/23 22:285.9 1
1,2,3-Trichlorobenzene ND ug/kg 05/19/23 05:20 87-61-605/18/23 22:285.9 1
1,2,4-Trichlorobenzene ND ug/kg 05/19/23 05:20 120-82-105/18/23 22:285.9 1
1,1,1-Trichloroethane ND ug/kg 05/19/23 05:20 71-55-605/18/23 22:285.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-221 Lab ID: 92667253006 Collected: 05/12/23 09:35 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/19/23 05:20 79-00-505/18/23 22:285.9 1
Trichloroethene ND ug/kg 05/19/23 05:20 79-01-605/18/23 22:285.9 1
Trichlorofluoromethane ND ug/kg 05/19/23 05:20 75-69-405/18/23 22:285.9 1
1,2,3-Trichloropropane ND ug/kg 05/19/23 05:20 96-18-405/18/23 22:285.9 1
1,2,4-Trimethylbenzene ND ug/kg 05/19/23 05:20 95-63-605/18/23 22:285.9 1
1,3,5-Trimethylbenzene ND ug/kg 05/19/23 05:20 108-67-805/18/23 22:285.9 1
Vinyl acetate ND ug/kg 05/19/23 05:20 108-05-405/18/23 22:2858.6 1
Vinyl chloride ND ug/kg 05/19/23 05:20 75-01-405/18/23 22:2811.7 1
Xylene (Total) ND ug/kg 05/19/23 05:20 1330-20-705/18/23 22:2811.7 1
m&p-Xylene ND ug/kg 05/19/23 05:20 179601-23-105/18/23 22:2811.7 1
o-Xylene ND ug/kg 05/19/23 05:20 95-47-605/18/23 22:285.9 1
Surrogates
Toluene-d8 (S) 104 %05/19/23 05:20 2037-26-505/18/23 22:2870-130 1
4-Bromofluorobenzene (S) 119 %05/19/23 05:20 460-00-405/18/23 22:2870-130 1
1,2-Dichloroethane-d4 (S) 101 %05/19/23 05:20 17060-07-005/18/23 22:2870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.8 %05/15/23 14:04 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-222 Lab ID: 92667253007 Collected: 05/12/23 09:50 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/17/23 14:31 83-32-905/16/23 14:28395 1
Acenaphthylene ND ug/kg 05/17/23 14:31 208-96-805/16/23 14:28395 1
Aniline ND ug/kg 05/17/23 14:31 62-53-305/16/23 14:28395 1
Anthracene ND ug/kg 05/17/23 14:31 120-12-705/16/23 14:28395 1
Benzo(a)anthracene ND ug/kg 05/17/23 14:31 56-55-305/16/23 14:28395 1
Benzo(a)pyrene ND ug/kg 05/17/23 14:31 50-32-805/16/23 14:28395 1
Benzo(b)fluoranthene ND ug/kg 05/17/23 14:31 205-99-205/16/23 14:28395 1
Benzo(g,h,i)perylene ND ug/kg 05/17/23 14:31 191-24-205/16/23 14:28395 1
Benzo(k)fluoranthene ND ug/kg 05/17/23 14:31 207-08-905/16/23 14:28395 1
Benzoic Acid ND ug/kg 05/17/23 14:31 65-85-005/16/23 14:281980 1
Benzyl alcohol ND ug/kg 05/17/23 14:31 100-51-605/16/23 14:28791 1
4-Bromophenylphenyl ether ND ug/kg 05/17/23 14:31 101-55-305/16/23 14:28395 1
Butylbenzylphthalate ND ug/kg 05/17/23 14:31 85-68-705/16/23 14:28395 1
4-Chloro-3-methylphenol ND ug/kg 05/17/23 14:31 59-50-705/16/23 14:28791 1
4-Chloroaniline ND ug/kg 05/17/23 14:31 106-47-805/16/23 14:28791 1
bis(2-Chloroethoxy)methane ND ug/kg 05/17/23 14:31 111-91-105/16/23 14:28395 1
bis(2-Chloroethyl) ether ND ug/kg 05/17/23 14:31 111-44-405/16/23 14:28395 1
2-Chloronaphthalene ND ug/kg 05/17/23 14:31 91-58-705/16/23 14:28395 1
2-Chlorophenol ND ug/kg 05/17/23 14:31 95-57-805/16/23 14:28395 1
4-Chlorophenylphenyl ether ND ug/kg 05/17/23 14:31 7005-72-305/16/23 14:28395 1
Chrysene ND ug/kg 05/17/23 14:31 218-01-905/16/23 14:28395 1
Dibenz(a,h)anthracene ND ug/kg 05/17/23 14:31 53-70-305/16/23 14:28395 1
Dibenzofuran ND ug/kg 05/17/23 14:31 132-64-905/16/23 14:28395 1
1,2-Dichlorobenzene ND ug/kg 05/17/23 14:31 95-50-105/16/23 14:28395 1
1,3-Dichlorobenzene ND ug/kg 05/17/23 14:31 541-73-105/16/23 14:28395 1
1,4-Dichlorobenzene ND ug/kg 05/17/23 14:31 106-46-705/16/23 14:28395 1
3,3'-Dichlorobenzidine ND ug/kg 05/17/23 14:31 91-94-105/16/23 14:28791 1
2,4-Dichlorophenol ND ug/kg 05/17/23 14:31 120-83-205/16/23 14:28395 1
Diethylphthalate ND ug/kg 05/17/23 14:31 84-66-205/16/23 14:28395 1
2,4-Dimethylphenol ND ug/kg 05/17/23 14:31 105-67-905/16/23 14:28395 1
Dimethylphthalate ND ug/kg 05/17/23 14:31 131-11-305/16/23 14:28395 1
Di-n-butylphthalate ND ug/kg 05/17/23 14:31 84-74-205/16/23 14:28395 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/23 14:31 534-52-105/16/23 14:28791 1
2,4-Dinitrophenol ND ug/kg 05/17/23 14:31 51-28-505/16/23 14:281980 1
2,4-Dinitrotoluene ND ug/kg 05/17/23 14:31 121-14-205/16/23 14:28395 1
2,6-Dinitrotoluene ND ug/kg 05/17/23 14:31 606-20-205/16/23 14:28395 1
Di-n-octylphthalate ND ug/kg 05/17/23 14:31 117-84-005/16/23 14:28395 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/23 14:31 117-81-705/16/23 14:28395 1
Fluoranthene ND ug/kg 05/17/23 14:31 206-44-005/16/23 14:28395 1
Fluorene ND ug/kg 05/17/23 14:31 86-73-705/16/23 14:28395 1
Hexachloro-1,3-butadiene ND ug/kg 05/17/23 14:31 87-68-305/16/23 14:28395 1
Hexachlorobenzene ND ug/kg 05/17/23 14:31 118-74-105/16/23 14:28395 1
Hexachlorocyclopentadiene ND ug/kg 05/17/23 14:31 77-47-405/16/23 14:28395 1
Hexachloroethane ND ug/kg 05/17/23 14:31 67-72-105/16/23 14:28395 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/23 14:31 193-39-505/16/23 14:28395 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-222 Lab ID: 92667253007 Collected: 05/12/23 09:50 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/17/23 14:31 78-59-105/16/23 14:28395 1
1-Methylnaphthalene ND ug/kg 05/17/23 14:31 90-12-005/16/23 14:28395 1
2-Methylnaphthalene ND ug/kg 05/17/23 14:31 91-57-605/16/23 14:28395 1
2-Methylphenol(o-Cresol) ND ug/kg 05/17/23 14:31 95-48-705/16/23 14:28395 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/17/23 14:31 15831-10-405/16/23 14:28395 1
Naphthalene ND ug/kg 05/17/23 14:31 91-20-305/16/23 14:28395 1
2-Nitroaniline ND ug/kg 05/17/23 14:31 88-74-405/16/23 14:281980 1
3-Nitroaniline ND ug/kg 05/17/23 14:31 99-09-205/16/23 14:281980 1
4-Nitroaniline ND ug/kg 05/17/23 14:31 100-01-605/16/23 14:28791 1
Nitrobenzene ND ug/kg 05/17/23 14:31 98-95-305/16/23 14:28395 1
2-Nitrophenol ND ug/kg 05/17/23 14:31 88-75-505/16/23 14:28395 1
4-Nitrophenol ND ug/kg 05/17/23 14:31 100-02-705/16/23 14:281980 1
N-Nitrosodimethylamine ND ug/kg 05/17/23 14:31 62-75-905/16/23 14:28395 1
N-Nitroso-di-n-propylamine ND ug/kg 05/17/23 14:31 621-64-705/16/23 14:28395 1
N-Nitrosodiphenylamine ND ug/kg 05/17/23 14:31 86-30-605/16/23 14:28395 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/17/23 14:31 108-60-105/16/23 14:28395 1
Pentachlorophenol ND ug/kg 05/17/23 14:31 87-86-505/16/23 14:28791 1
Phenanthrene ND ug/kg 05/17/23 14:31 85-01-805/16/23 14:28395 1
Phenol ND ug/kg 05/17/23 14:31 108-95-205/16/23 14:28395 1
Pyrene ND ug/kg 05/17/23 14:31 129-00-005/16/23 14:28395 1
Pyridine ND ug/kg 05/17/23 14:31 110-86-105/16/23 14:28395 1
1,2,4-Trichlorobenzene ND ug/kg 05/17/23 14:31 120-82-105/16/23 14:28395 1
2,4,5-Trichlorophenol ND ug/kg 05/17/23 14:31 95-95-405/16/23 14:28395 1
2,4,6-Trichlorophenol ND ug/kg 05/17/23 14:31 88-06-205/16/23 14:28395 1
Surrogates
Nitrobenzene-d5 (S) 59 %05/17/23 14:31 4165-60-005/16/23 14:2810-130 1
2-Fluorobiphenyl (S) 59 %05/17/23 14:31 321-60-805/16/23 14:2810-130 1
Terphenyl-d14 (S) 60 %05/17/23 14:31 1718-51-005/16/23 14:2810-130 1
Phenol-d6 (S) 55 %05/17/23 14:31 13127-88-305/16/23 14:2810-130 1
2-Fluorophenol (S) 57 %05/17/23 14:31 367-12-405/16/23 14:2810-130 1
2,4,6-Tribromophenol (S) 69 %05/17/23 14:31 118-79-605/16/23 14:2810-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/17/23 18:12 67-64-105/16/23 22:24125 1
Benzene ND ug/kg 05/17/23 18:12 71-43-205/16/23 22:246.2 1
Bromobenzene ND ug/kg 05/17/23 18:12 108-86-105/16/23 22:246.2 1
Bromochloromethane ND ug/kg 05/17/23 18:12 74-97-505/16/23 22:246.2 1
Bromodichloromethane ND ug/kg 05/17/23 18:12 75-27-405/16/23 22:246.2 1
Bromoform ND ug/kg 05/17/23 18:12 75-25-205/16/23 22:246.2 1
Bromomethane ND ug/kg 05/17/23 18:12 74-83-9 v205/16/23 22:2425.0 1
2-Butanone (MEK) ND ug/kg 05/17/23 18:12 78-93-305/16/23 22:24125 1
n-Butylbenzene ND ug/kg 05/17/23 18:12 104-51-805/16/23 22:246.2 1
sec-Butylbenzene 16.4 ug/kg 05/17/23 18:12 135-98-805/16/23 22:246.2 1
tert-Butylbenzene ND ug/kg 05/17/23 18:12 98-06-605/16/23 22:246.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-222 Lab ID: 92667253007 Collected: 05/12/23 09:50 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/17/23 18:12 56-23-505/16/23 22:246.2 1
Chlorobenzene ND ug/kg 05/17/23 18:12 108-90-705/16/23 22:246.2 1
Chloroethane ND ug/kg 05/17/23 18:12 75-00-305/16/23 22:2412.5 1
Chloroform ND ug/kg 05/17/23 18:12 67-66-305/16/23 22:246.2 1
Chloromethane ND ug/kg 05/17/23 18:12 74-87-305/16/23 22:2412.5 1
2-Chlorotoluene ND ug/kg 05/17/23 18:12 95-49-805/16/23 22:246.2 1
4-Chlorotoluene ND ug/kg 05/17/23 18:12 106-43-405/16/23 22:246.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/17/23 18:12 96-12-805/16/23 22:246.2 1
Dibromochloromethane ND ug/kg 05/17/23 18:12 124-48-105/16/23 22:246.2 1
1,2-Dibromoethane (EDB) ND ug/kg 05/17/23 18:12 106-93-405/16/23 22:246.2 1
Dibromomethane ND ug/kg 05/17/23 18:12 74-95-305/16/23 22:246.2 1
1,2-Dichlorobenzene ND ug/kg 05/17/23 18:12 95-50-105/16/23 22:246.2 1
1,3-Dichlorobenzene ND ug/kg 05/17/23 18:12 541-73-105/16/23 22:246.2 1
1,4-Dichlorobenzene ND ug/kg 05/17/23 18:12 106-46-705/16/23 22:246.2 1
Dichlorodifluoromethane ND ug/kg 05/17/23 18:12 75-71-8 IH05/16/23 22:2412.5 1
1,1-Dichloroethane ND ug/kg 05/17/23 18:12 75-34-305/16/23 22:246.2 1
1,2-Dichloroethane ND ug/kg 05/17/23 18:12 107-06-205/16/23 22:246.2 1
1,1-Dichloroethene ND ug/kg 05/17/23 18:12 75-35-405/16/23 22:246.2 1
cis-1,2-Dichloroethene ND ug/kg 05/17/23 18:12 156-59-205/16/23 22:246.2 1
trans-1,2-Dichloroethene ND ug/kg 05/17/23 18:12 156-60-505/16/23 22:246.2 1
1,2-Dichloropropane ND ug/kg 05/17/23 18:12 78-87-505/16/23 22:246.2 1
1,3-Dichloropropane ND ug/kg 05/17/23 18:12 142-28-905/16/23 22:246.2 1
2,2-Dichloropropane ND ug/kg 05/17/23 18:12 594-20-7 v205/16/23 22:246.2 1
1,1-Dichloropropene ND ug/kg 05/17/23 18:12 563-58-605/16/23 22:246.2 1
cis-1,3-Dichloropropene ND ug/kg 05/17/23 18:12 10061-01-505/16/23 22:246.2 1
trans-1,3-Dichloropropene ND ug/kg 05/17/23 18:12 10061-02-605/16/23 22:246.2 1
Diisopropyl ether ND ug/kg 05/17/23 18:12 108-20-305/16/23 22:246.2 1
Ethylbenzene ND ug/kg 05/17/23 18:12 100-41-405/16/23 22:246.2 1
Hexachloro-1,3-butadiene ND ug/kg 05/17/23 18:12 87-68-305/16/23 22:2412.5 1
2-Hexanone ND ug/kg 05/17/23 18:12 591-78-605/16/23 22:2462.4 1
Isopropylbenzene (Cumene) ND ug/kg 05/17/23 18:12 98-82-805/16/23 22:246.2 1
p-Isopropyltoluene ND ug/kg 05/17/23 18:12 99-87-605/16/23 22:246.2 1
Methylene Chloride ND ug/kg 05/17/23 18:12 75-09-205/16/23 22:2425.0 1
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/17/23 18:12 108-10-105/16/23 22:2462.4 1
Methyl-tert-butyl ether ND ug/kg 05/17/23 18:12 1634-04-405/16/23 22:246.2 1
Naphthalene ND ug/kg 05/17/23 18:12 91-20-305/16/23 22:246.2 1
n-Propylbenzene ND ug/kg 05/17/23 18:12 103-65-105/16/23 22:246.2 1
Styrene ND ug/kg 05/17/23 18:12 100-42-505/16/23 22:246.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/17/23 18:12 630-20-605/16/23 22:246.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/17/23 18:12 79-34-505/16/23 22:246.2 1
Tetrachloroethene ND ug/kg 05/17/23 18:12 127-18-405/16/23 22:246.2 1
Toluene ND ug/kg 05/17/23 18:12 108-88-305/16/23 22:246.2 1
1,2,3-Trichlorobenzene ND ug/kg 05/17/23 18:12 87-61-605/16/23 22:246.2 1
1,2,4-Trichlorobenzene ND ug/kg 05/17/23 18:12 120-82-105/16/23 22:246.2 1
1,1,1-Trichloroethane ND ug/kg 05/17/23 18:12 71-55-605/16/23 22:246.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-222 Lab ID: 92667253007 Collected: 05/12/23 09:50 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/17/23 18:12 79-00-505/16/23 22:246.2 1
Trichloroethene ND ug/kg 05/17/23 18:12 79-01-605/16/23 22:246.2 1
Trichlorofluoromethane ND ug/kg 05/17/23 18:12 75-69-405/16/23 22:246.2 1
1,2,3-Trichloropropane ND ug/kg 05/17/23 18:12 96-18-405/16/23 22:246.2 1
1,2,4-Trimethylbenzene ND ug/kg 05/17/23 18:12 95-63-605/16/23 22:246.2 1
1,3,5-Trimethylbenzene ND ug/kg 05/17/23 18:12 108-67-805/16/23 22:246.2 1
Vinyl acetate ND ug/kg 05/17/23 18:12 108-05-405/16/23 22:2462.4 1
Vinyl chloride ND ug/kg 05/17/23 18:12 75-01-405/16/23 22:2412.5 1
Xylene (Total) ND ug/kg 05/17/23 18:12 1330-20-705/16/23 22:2412.5 1
m&p-Xylene ND ug/kg 05/17/23 18:12 179601-23-105/16/23 22:2412.5 1
o-Xylene ND ug/kg 05/17/23 18:12 95-47-605/16/23 22:246.2 1
Surrogates
Toluene-d8 (S) 102 %05/17/23 18:12 2037-26-505/16/23 22:2470-130 1
4-Bromofluorobenzene (S) 104 %05/17/23 18:12 460-00-405/16/23 22:2470-130 1
1,2-Dichloroethane-d4 (S) 103 %05/17/23 18:12 17060-07-005/16/23 22:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.6 %05/15/23 14:04 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-223 Lab ID: 92667253008 Collected: 05/12/23 10:05 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/17/23 14:59 83-32-905/16/23 14:28401 1
Acenaphthylene ND ug/kg 05/17/23 14:59 208-96-805/16/23 14:28401 1
Aniline ND ug/kg 05/17/23 14:59 62-53-305/16/23 14:28401 1
Anthracene ND ug/kg 05/17/23 14:59 120-12-705/16/23 14:28401 1
Benzo(a)anthracene ND ug/kg 05/17/23 14:59 56-55-305/16/23 14:28401 1
Benzo(a)pyrene ND ug/kg 05/17/23 14:59 50-32-805/16/23 14:28401 1
Benzo(b)fluoranthene ND ug/kg 05/17/23 14:59 205-99-205/16/23 14:28401 1
Benzo(g,h,i)perylene ND ug/kg 05/17/23 14:59 191-24-205/16/23 14:28401 1
Benzo(k)fluoranthene ND ug/kg 05/17/23 14:59 207-08-905/16/23 14:28401 1
Benzoic Acid ND ug/kg 05/17/23 14:59 65-85-005/16/23 14:282000 1
Benzyl alcohol ND ug/kg 05/17/23 14:59 100-51-605/16/23 14:28801 1
4-Bromophenylphenyl ether ND ug/kg 05/17/23 14:59 101-55-305/16/23 14:28401 1
Butylbenzylphthalate ND ug/kg 05/17/23 14:59 85-68-705/16/23 14:28401 1
4-Chloro-3-methylphenol ND ug/kg 05/17/23 14:59 59-50-705/16/23 14:28801 1
4-Chloroaniline ND ug/kg 05/17/23 14:59 106-47-805/16/23 14:28801 1
bis(2-Chloroethoxy)methane ND ug/kg 05/17/23 14:59 111-91-105/16/23 14:28401 1
bis(2-Chloroethyl) ether ND ug/kg 05/17/23 14:59 111-44-405/16/23 14:28401 1
2-Chloronaphthalene ND ug/kg 05/17/23 14:59 91-58-705/16/23 14:28401 1
2-Chlorophenol ND ug/kg 05/17/23 14:59 95-57-805/16/23 14:28401 1
4-Chlorophenylphenyl ether ND ug/kg 05/17/23 14:59 7005-72-305/16/23 14:28401 1
Chrysene ND ug/kg 05/17/23 14:59 218-01-905/16/23 14:28401 1
Dibenz(a,h)anthracene ND ug/kg 05/17/23 14:59 53-70-305/16/23 14:28401 1
Dibenzofuran ND ug/kg 05/17/23 14:59 132-64-905/16/23 14:28401 1
1,2-Dichlorobenzene ND ug/kg 05/17/23 14:59 95-50-105/16/23 14:28401 1
1,3-Dichlorobenzene ND ug/kg 05/17/23 14:59 541-73-105/16/23 14:28401 1
1,4-Dichlorobenzene ND ug/kg 05/17/23 14:59 106-46-705/16/23 14:28401 1
3,3'-Dichlorobenzidine ND ug/kg 05/17/23 14:59 91-94-105/16/23 14:28801 1
2,4-Dichlorophenol ND ug/kg 05/17/23 14:59 120-83-205/16/23 14:28401 1
Diethylphthalate ND ug/kg 05/17/23 14:59 84-66-205/16/23 14:28401 1
2,4-Dimethylphenol ND ug/kg 05/17/23 14:59 105-67-905/16/23 14:28401 1
Dimethylphthalate ND ug/kg 05/17/23 14:59 131-11-305/16/23 14:28401 1
Di-n-butylphthalate ND ug/kg 05/17/23 14:59 84-74-205/16/23 14:28401 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/23 14:59 534-52-105/16/23 14:28801 1
2,4-Dinitrophenol ND ug/kg 05/17/23 14:59 51-28-505/16/23 14:282000 1
2,4-Dinitrotoluene ND ug/kg 05/17/23 14:59 121-14-205/16/23 14:28401 1
2,6-Dinitrotoluene ND ug/kg 05/17/23 14:59 606-20-205/16/23 14:28401 1
Di-n-octylphthalate ND ug/kg 05/17/23 14:59 117-84-005/16/23 14:28401 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/23 14:59 117-81-705/16/23 14:28401 1
Fluoranthene ND ug/kg 05/17/23 14:59 206-44-005/16/23 14:28401 1
Fluorene ND ug/kg 05/17/23 14:59 86-73-705/16/23 14:28401 1
Hexachloro-1,3-butadiene ND ug/kg 05/17/23 14:59 87-68-305/16/23 14:28401 1
Hexachlorobenzene ND ug/kg 05/17/23 14:59 118-74-105/16/23 14:28401 1
Hexachlorocyclopentadiene ND ug/kg 05/17/23 14:59 77-47-405/16/23 14:28401 1
Hexachloroethane ND ug/kg 05/17/23 14:59 67-72-105/16/23 14:28401 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/23 14:59 193-39-505/16/23 14:28401 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-223 Lab ID: 92667253008 Collected: 05/12/23 10:05 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND ug/kg 05/17/23 14:59 78-59-105/16/23 14:28401 1
1-Methylnaphthalene ND ug/kg 05/17/23 14:59 90-12-005/16/23 14:28401 1
2-Methylnaphthalene ND ug/kg 05/17/23 14:59 91-57-605/16/23 14:28401 1
2-Methylphenol(o-Cresol) ND ug/kg 05/17/23 14:59 95-48-705/16/23 14:28401 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 05/17/23 14:59 15831-10-405/16/23 14:28401 1
Naphthalene ND ug/kg 05/17/23 14:59 91-20-305/16/23 14:28401 1
2-Nitroaniline ND ug/kg 05/17/23 14:59 88-74-405/16/23 14:282000 1
3-Nitroaniline ND ug/kg 05/17/23 14:59 99-09-205/16/23 14:282000 1
4-Nitroaniline ND ug/kg 05/17/23 14:59 100-01-605/16/23 14:28801 1
Nitrobenzene ND ug/kg 05/17/23 14:59 98-95-305/16/23 14:28401 1
2-Nitrophenol ND ug/kg 05/17/23 14:59 88-75-505/16/23 14:28401 1
4-Nitrophenol ND ug/kg 05/17/23 14:59 100-02-705/16/23 14:282000 1
N-Nitrosodimethylamine ND ug/kg 05/17/23 14:59 62-75-905/16/23 14:28401 1
N-Nitroso-di-n-propylamine ND ug/kg 05/17/23 14:59 621-64-705/16/23 14:28401 1
N-Nitrosodiphenylamine ND ug/kg 05/17/23 14:59 86-30-605/16/23 14:28401 1
2,2'-Oxybis(1-chloropropane) ND ug/kg 05/17/23 14:59 108-60-105/16/23 14:28401 1
Pentachlorophenol ND ug/kg 05/17/23 14:59 87-86-505/16/23 14:28801 1
Phenanthrene ND ug/kg 05/17/23 14:59 85-01-805/16/23 14:28401 1
Phenol ND ug/kg 05/17/23 14:59 108-95-205/16/23 14:28401 1
Pyrene ND ug/kg 05/17/23 14:59 129-00-005/16/23 14:28401 1
Pyridine ND ug/kg 05/17/23 14:59 110-86-105/16/23 14:28401 1
1,2,4-Trichlorobenzene ND ug/kg 05/17/23 14:59 120-82-105/16/23 14:28401 1
2,4,5-Trichlorophenol ND ug/kg 05/17/23 14:59 95-95-405/16/23 14:28401 1
2,4,6-Trichlorophenol ND ug/kg 05/17/23 14:59 88-06-205/16/23 14:28401 1
Surrogates
Nitrobenzene-d5 (S) 71 %05/17/23 14:59 4165-60-005/16/23 14:2810-130 1
2-Fluorobiphenyl (S) 68 %05/17/23 14:59 321-60-805/16/23 14:2810-130 1
Terphenyl-d14 (S) 65 %05/17/23 14:59 1718-51-005/16/23 14:2810-130 1
Phenol-d6 (S) 58 %05/17/23 14:59 13127-88-305/16/23 14:2810-130 1
2-Fluorophenol (S) 62 %05/17/23 14:59 367-12-405/16/23 14:2810-130 1
2,4,6-Tribromophenol (S) 76 %05/17/23 14:59 118-79-605/16/23 14:2810-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/17/23 18:30 67-64-105/16/23 22:24118 1
Benzene ND ug/kg 05/17/23 18:30 71-43-205/16/23 22:245.9 1
Bromobenzene ND ug/kg 05/17/23 18:30 108-86-105/16/23 22:245.9 1
Bromochloromethane ND ug/kg 05/17/23 18:30 74-97-505/16/23 22:245.9 1
Bromodichloromethane ND ug/kg 05/17/23 18:30 75-27-405/16/23 22:245.9 1
Bromoform ND ug/kg 05/17/23 18:30 75-25-205/16/23 22:245.9 1
Bromomethane ND ug/kg 05/17/23 18:30 74-83-9 v205/16/23 22:2423.6 1
2-Butanone (MEK) ND ug/kg 05/17/23 18:30 78-93-305/16/23 22:24118 1
n-Butylbenzene ND ug/kg 05/17/23 18:30 104-51-805/16/23 22:245.9 1
sec-Butylbenzene 10.7 ug/kg 05/17/23 18:30 135-98-805/16/23 22:245.9 1
tert-Butylbenzene ND ug/kg 05/17/23 18:30 98-06-605/16/23 22:245.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-223 Lab ID: 92667253008 Collected: 05/12/23 10:05 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND ug/kg 05/17/23 18:30 56-23-505/16/23 22:245.9 1
Chlorobenzene ND ug/kg 05/17/23 18:30 108-90-705/16/23 22:245.9 1
Chloroethane ND ug/kg 05/17/23 18:30 75-00-305/16/23 22:2411.8 1
Chloroform ND ug/kg 05/17/23 18:30 67-66-305/16/23 22:245.9 1
Chloromethane ND ug/kg 05/17/23 18:30 74-87-305/16/23 22:2411.8 1
2-Chlorotoluene ND ug/kg 05/17/23 18:30 95-49-805/16/23 22:245.9 1
4-Chlorotoluene ND ug/kg 05/17/23 18:30 106-43-405/16/23 22:245.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/17/23 18:30 96-12-805/16/23 22:245.9 1
Dibromochloromethane ND ug/kg 05/17/23 18:30 124-48-105/16/23 22:245.9 1
1,2-Dibromoethane (EDB) ND ug/kg 05/17/23 18:30 106-93-405/16/23 22:245.9 1
Dibromomethane ND ug/kg 05/17/23 18:30 74-95-305/16/23 22:245.9 1
1,2-Dichlorobenzene ND ug/kg 05/17/23 18:30 95-50-105/16/23 22:245.9 1
1,3-Dichlorobenzene ND ug/kg 05/17/23 18:30 541-73-105/16/23 22:245.9 1
1,4-Dichlorobenzene ND ug/kg 05/17/23 18:30 106-46-705/16/23 22:245.9 1
Dichlorodifluoromethane ND ug/kg 05/17/23 18:30 75-71-8 IH05/16/23 22:2411.8 1
1,1-Dichloroethane ND ug/kg 05/17/23 18:30 75-34-305/16/23 22:245.9 1
1,2-Dichloroethane ND ug/kg 05/17/23 18:30 107-06-205/16/23 22:245.9 1
1,1-Dichloroethene ND ug/kg 05/17/23 18:30 75-35-405/16/23 22:245.9 1
cis-1,2-Dichloroethene ND ug/kg 05/17/23 18:30 156-59-205/16/23 22:245.9 1
trans-1,2-Dichloroethene ND ug/kg 05/17/23 18:30 156-60-505/16/23 22:245.9 1
1,2-Dichloropropane ND ug/kg 05/17/23 18:30 78-87-505/16/23 22:245.9 1
1,3-Dichloropropane ND ug/kg 05/17/23 18:30 142-28-905/16/23 22:245.9 1
2,2-Dichloropropane ND ug/kg 05/17/23 18:30 594-20-7 v205/16/23 22:245.9 1
1,1-Dichloropropene ND ug/kg 05/17/23 18:30 563-58-605/16/23 22:245.9 1
cis-1,3-Dichloropropene ND ug/kg 05/17/23 18:30 10061-01-505/16/23 22:245.9 1
trans-1,3-Dichloropropene ND ug/kg 05/17/23 18:30 10061-02-605/16/23 22:245.9 1
Diisopropyl ether ND ug/kg 05/17/23 18:30 108-20-305/16/23 22:245.9 1
Ethylbenzene ND ug/kg 05/17/23 18:30 100-41-405/16/23 22:245.9 1
Hexachloro-1,3-butadiene ND ug/kg 05/17/23 18:30 87-68-305/16/23 22:2411.8 1
2-Hexanone ND ug/kg 05/17/23 18:30 591-78-605/16/23 22:2459.0 1
Isopropylbenzene (Cumene) ND ug/kg 05/17/23 18:30 98-82-805/16/23 22:245.9 1
p-Isopropyltoluene ND ug/kg 05/17/23 18:30 99-87-605/16/23 22:245.9 1
Methylene Chloride ND ug/kg 05/17/23 18:30 75-09-205/16/23 22:2423.6 1
4-Methyl-2-pentanone (MIBK) ND ug/kg 05/17/23 18:30 108-10-105/16/23 22:2459.0 1
Methyl-tert-butyl ether 5.9 ug/kg 05/17/23 18:30 1634-04-405/16/23 22:245.9 1
Naphthalene ND ug/kg 05/17/23 18:30 91-20-305/16/23 22:245.9 1
n-Propylbenzene ND ug/kg 05/17/23 18:30 103-65-105/16/23 22:245.9 1
Styrene ND ug/kg 05/17/23 18:30 100-42-505/16/23 22:245.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/17/23 18:30 630-20-605/16/23 22:245.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/17/23 18:30 79-34-505/16/23 22:245.9 1
Tetrachloroethene ND ug/kg 05/17/23 18:30 127-18-405/16/23 22:245.9 1
Toluene ND ug/kg 05/17/23 18:30 108-88-305/16/23 22:245.9 1
1,2,3-Trichlorobenzene ND ug/kg 05/17/23 18:30 87-61-605/16/23 22:245.9 1
1,2,4-Trichlorobenzene ND ug/kg 05/17/23 18:30 120-82-105/16/23 22:245.9 1
1,1,1-Trichloroethane ND ug/kg 05/17/23 18:30 71-55-605/16/23 22:245.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Sample: 512234903-223 Lab ID: 92667253008 Collected: 05/12/23 10:05 Received: 05/12/23 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND ug/kg 05/17/23 18:30 79-00-505/16/23 22:245.9 1
Trichloroethene ND ug/kg 05/17/23 18:30 79-01-605/16/23 22:245.9 1
Trichlorofluoromethane ND ug/kg 05/17/23 18:30 75-69-405/16/23 22:245.9 1
1,2,3-Trichloropropane ND ug/kg 05/17/23 18:30 96-18-405/16/23 22:245.9 1
1,2,4-Trimethylbenzene ND ug/kg 05/17/23 18:30 95-63-605/16/23 22:245.9 1
1,3,5-Trimethylbenzene ND ug/kg 05/17/23 18:30 108-67-805/16/23 22:245.9 1
Vinyl acetate ND ug/kg 05/17/23 18:30 108-05-405/16/23 22:2459.0 1
Vinyl chloride ND ug/kg 05/17/23 18:30 75-01-405/16/23 22:2411.8 1
Xylene (Total) ND ug/kg 05/17/23 18:30 1330-20-705/16/23 22:2411.8 1
m&p-Xylene ND ug/kg 05/17/23 18:30 179601-23-105/16/23 22:2411.8 1
o-Xylene ND ug/kg 05/17/23 18:30 95-47-605/16/23 22:245.9 1
Surrogates
Toluene-d8 (S) 102 %05/17/23 18:30 2037-26-505/16/23 22:2470-130 1
4-Bromofluorobenzene (S) 103 %05/17/23 18:30 460-00-405/16/23 22:2470-130 1
1,2-Dichloroethane-d4 (S) 105 %05/17/23 18:30 17060-07-005/16/23 22:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.1 %05/15/23 14:04 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
774899
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92667253007, 92667253008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4021409
Associated Lab Samples:92667253007, 92667253008
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/17/23 10:30
1,1,1-Trichloroethane ug/kg ND 5.0 05/17/23 10:30
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/17/23 10:30
1,1,2-Trichloroethane ug/kg ND 5.0 05/17/23 10:30
1,1-Dichloroethane ug/kg ND 5.0 05/17/23 10:30
1,1-Dichloroethene ug/kg ND 5.0 05/17/23 10:30
1,1-Dichloropropene ug/kg ND 5.0 05/17/23 10:30
1,2,3-Trichlorobenzene ug/kg ND 5.0 05/17/23 10:30
1,2,3-Trichloropropane ug/kg ND 5.0 05/17/23 10:30
1,2,4-Trichlorobenzene ug/kg ND 5.0 05/17/23 10:30
1,2,4-Trimethylbenzene ug/kg ND 5.0 05/17/23 10:30
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 05/17/23 10:30
1,2-Dibromoethane (EDB) ug/kg ND 5.0 05/17/23 10:30
1,2-Dichlorobenzene ug/kg ND 5.0 05/17/23 10:30
1,2-Dichloroethane ug/kg ND 5.0 05/17/23 10:30
1,2-Dichloropropane ug/kg ND 5.0 05/17/23 10:30
1,3,5-Trimethylbenzene ug/kg ND 5.0 05/17/23 10:30
1,3-Dichlorobenzene ug/kg ND 5.0 05/17/23 10:30
1,3-Dichloropropane ug/kg ND 5.0 05/17/23 10:30
1,4-Dichlorobenzene ug/kg ND 5.0 05/17/23 10:30
2,2-Dichloropropane ug/kg ND 5.0 v205/17/23 10:30
2-Butanone (MEK) ug/kg ND 100 05/17/23 10:30
2-Chlorotoluene ug/kg ND 5.0 05/17/23 10:30
2-Hexanone ug/kg ND 50.0 05/17/23 10:30
4-Chlorotoluene ug/kg ND 5.0 05/17/23 10:30
4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 05/17/23 10:30
Acetone ug/kg ND 100 05/17/23 10:30
Benzene ug/kg ND 5.0 05/17/23 10:30
Bromobenzene ug/kg ND 5.0 05/17/23 10:30
Bromochloromethane ug/kg ND 5.0 05/17/23 10:30
Bromodichloromethane ug/kg ND 5.0 05/17/23 10:30
Bromoform ug/kg ND 5.0 05/17/23 10:30
Bromomethane ug/kg ND 20.0 v205/17/23 10:30
Carbon tetrachloride ug/kg ND 5.0 05/17/23 10:30
Chlorobenzene ug/kg ND 5.0 05/17/23 10:30
Chloroethane ug/kg ND 10.0 05/17/23 10:30
Chloroform ug/kg ND 5.0 05/17/23 10:30
Chloromethane ug/kg ND 10.0 05/17/23 10:30
cis-1,2-Dichloroethene ug/kg ND 5.0 05/17/23 10:30
cis-1,3-Dichloropropene ug/kg ND 5.0 05/17/23 10:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4021409
Associated Lab Samples:92667253007, 92667253008
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 05/17/23 10:30
Dibromomethane ug/kg ND 5.0 05/17/23 10:30
Dichlorodifluoromethane ug/kg ND 10.0 IH05/17/23 10:30
Diisopropyl ether ug/kg ND 5.0 05/17/23 10:30
Ethylbenzene ug/kg ND 5.0 05/17/23 10:30
Hexachloro-1,3-butadiene ug/kg ND 10.0 05/17/23 10:30
Isopropylbenzene (Cumene) ug/kg ND 5.0 05/17/23 10:30
m&p-Xylene ug/kg ND 10.0 05/17/23 10:30
Methyl-tert-butyl ether ug/kg ND 5.0 05/17/23 10:30
Methylene Chloride ug/kg ND 20.0 05/17/23 10:30
n-Butylbenzene ug/kg ND 5.0 05/17/23 10:30
n-Propylbenzene ug/kg ND 5.0 05/17/23 10:30
Naphthalene ug/kg ND 5.0 05/17/23 10:30
o-Xylene ug/kg ND 5.0 05/17/23 10:30
p-Isopropyltoluene ug/kg ND 5.0 05/17/23 10:30
sec-Butylbenzene ug/kg ND 5.0 05/17/23 10:30
Styrene ug/kg ND 5.0 05/17/23 10:30
tert-Butylbenzene ug/kg ND 5.0 05/17/23 10:30
Tetrachloroethene ug/kg ND 5.0 05/17/23 10:30
Toluene ug/kg ND 5.0 05/17/23 10:30
trans-1,2-Dichloroethene ug/kg ND 5.0 05/17/23 10:30
trans-1,3-Dichloropropene ug/kg ND 5.0 05/17/23 10:30
Trichloroethene ug/kg ND 5.0 05/17/23 10:30
Trichlorofluoromethane ug/kg ND 5.0 05/17/23 10:30
Vinyl acetate ug/kg ND 50.0 05/17/23 10:30
Vinyl chloride ug/kg ND 10.0 05/17/23 10:30
Xylene (Total) ug/kg ND 10.0 05/17/23 10:30
1,2-Dichloroethane-d4 (S) % 105 70-130 05/17/23 10:30
4-Bromofluorobenzene (S) % 101 70-130 05/17/23 10:30
Toluene-d8 (S) % 101 70-130 05/17/23 10:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4021410LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 467500 93 70-130
1,1,1-Trichloroethane ug/kg 468500 94 70-130
1,1,2,2-Tetrachloroethane ug/kg 492500 98 70-130
1,1,2-Trichloroethane ug/kg 467500 93 70-130
1,1-Dichloroethane ug/kg 487500 97 70-130
1,1-Dichloroethene ug/kg 516500 103 70-130
1,1-Dichloropropene ug/kg 481500 96 70-130
1,2,3-Trichlorobenzene ug/kg 473500 95 70-130
1,2,3-Trichloropropane ug/kg 476500 95 70-130
1,2,4-Trichlorobenzene ug/kg 452500 90 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4021410LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 475500 95 70-130
1,2-Dibromo-3-chloropropane ug/kg 473500 95 67-130
1,2-Dibromoethane (EDB) ug/kg 481500 96 70-130
1,2-Dichlorobenzene ug/kg 460500 92 70-130
1,2-Dichloroethane ug/kg 478500 96 70-130
1,2-Dichloropropane ug/kg 482500 96 70-130
1,3,5-Trimethylbenzene ug/kg 479500 96 70-130
1,3-Dichlorobenzene ug/kg 447500 89 70-130
1,3-Dichloropropane ug/kg 474500 95 70-130
1,4-Dichlorobenzene ug/kg 442500 88 70-130
2,2-Dichloropropane ug/kg 383 v3500 77 67-130
2-Butanone (MEK) ug/kg 9881000 99 66-130
2-Chlorotoluene ug/kg 474500 95 70-130
2-Hexanone ug/kg 10501000 105 70-130
4-Chlorotoluene ug/kg 474500 95 70-130
4-Methyl-2-pentanone (MIBK) ug/kg 10101000 101 70-130
Acetone ug/kg 9871000 99 67-130
Benzene ug/kg 459500 92 70-130
Bromobenzene ug/kg 467500 93 70-130
Bromochloromethane ug/kg 473500 95 70-130
Bromodichloromethane ug/kg 461500 92 70-130
Bromoform ug/kg 456500 91 70-130
Bromomethane ug/kg 384 v3500 77 53-175
Carbon tetrachloride ug/kg 470500 94 70-130
Chlorobenzene ug/kg 478500 96 70-130
Chloroethane ug/kg 455500 91 70-135
Chloroform ug/kg 464500 93 70-130
Chloromethane ug/kg 529500 106 64-130
cis-1,2-Dichloroethene ug/kg 475500 95 70-130
cis-1,3-Dichloropropene ug/kg 417500 83 70-130
Dibromochloromethane ug/kg 469500 94 70-130
Dibromomethane ug/kg 469500 94 70-130
Dichlorodifluoromethane ug/kg 459 IH500 92 63-145
Diisopropyl ether ug/kg 488500 98 68-130
Ethylbenzene ug/kg 440500 88 70-130
Hexachloro-1,3-butadiene ug/kg 415500 83 70-130
Isopropylbenzene (Cumene) ug/kg 481500 96 70-130
m&p-Xylene ug/kg 9451000 94 70-130
Methyl-tert-butyl ether ug/kg 450500 90 70-130
Methylene Chloride ug/kg 525500 105 67-130
n-Butylbenzene ug/kg 451500 90 70-130
n-Propylbenzene ug/kg 465500 93 70-130
Naphthalene ug/kg 484500 97 70-130
o-Xylene ug/kg 469500 94 70-130
p-Isopropyltoluene ug/kg 470500 94 70-130
sec-Butylbenzene ug/kg 454500 91 70-130
Styrene ug/kg 479500 96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4021410LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 472500 94 64-130
Tetrachloroethene ug/kg 476500 95 70-130
Toluene ug/kg 449500 90 70-130
trans-1,2-Dichloroethene ug/kg 507500 101 70-130
trans-1,3-Dichloropropene ug/kg 451500 90 70-130
Trichloroethene ug/kg 464500 93 70-130
Trichlorofluoromethane ug/kg 402500 80 70-130
Vinyl acetate ug/kg 9711000 97 70-134
Vinyl chloride ug/kg 406500 81 68-130
Xylene (Total) ug/kg 14101500 94 70-130
1,2-Dichloroethane-d4 (S) %97 70-130
4-Bromofluorobenzene (S) %103 70-130
Toluene-d8 (S) %100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4021411MATRIX SPIKE SAMPLE:
MSSpike
Result
92667323011
1,1,1,2-Tetrachloroethane ug/kg 492574 86 58-140ND
1,1,1-Trichloroethane ug/kg 536574 93 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 502574 87 52-139ND
1,1,2-Trichloroethane ug/kg 485574 85 56-140ND
1,1-Dichloroethane ug/kg 522574 91 58-145ND
1,1-Dichloroethene ug/kg 580574 101 57-158ND
1,1-Dichloropropene ug/kg 532574 93 58-151ND
1,2,3-Trichlorobenzene ug/kg 483574 84 48-149ND
1,2,3-Trichloropropane ug/kg 466574 81 54-132ND
1,2,4-Trichlorobenzene ug/kg 473574 82 51-151ND
1,2,4-Trimethylbenzene ug/kg 486574 85 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 452574 79 44-134ND
1,2-Dibromoethane (EDB) ug/kg 484574 84 60-138ND
1,2-Dichlorobenzene ug/kg 483574 84 59-147ND
1,2-Dichloroethane ug/kg 497574 87 57-139ND
1,2-Dichloropropane ug/kg 517574 90 62-145ND
1,3,5-Trimethylbenzene ug/kg 497574 87 47-159ND
1,3-Dichlorobenzene ug/kg 470574 82 58-144ND
1,3-Dichloropropane ug/kg 484574 84 60-142ND
1,4-Dichlorobenzene ug/kg 444574 77 57-143ND
2,2-Dichloropropane ug/kg 402574 70 37-144ND
2-Butanone (MEK) ug/kg 9951150 87 28-146ND
2-Chlorotoluene ug/kg 491574 86 55-158ND
2-Hexanone ug/kg 9901150 86 44-141ND
4-Chlorotoluene ug/kg 490574 85 55-146ND
4-Methyl-2-pentanone (MIBK) ug/kg 9991150 87 50-138ND
Acetone ug/kg 9431150 82 20-136ND
Benzene ug/kg 496574 86 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4021411MATRIX SPIKE SAMPLE:
MSSpike
Result
92667323011
Bromobenzene ug/kg 483574 84 59-145ND
Bromochloromethane ug/kg 481574 84 57-143ND
Bromodichloromethane ug/kg 480574 84 53-133ND
Bromoform ug/kg 452574 79 48-133ND
Bromomethane ug/kg 84.4 v3574 15 10-167ND
Carbon tetrachloride ug/kg 424574 74 57-147ND
Chlorobenzene ug/kg 500574 87 61-144ND
Chloroethane ug/kg 98.0574 17 10-153ND
Chloroform ug/kg 504574 88 58-141ND
Chloromethane ug/kg 625574 109 54-165ND
cis-1,2-Dichloroethene ug/kg 521574 91 59-144ND
cis-1,3-Dichloropropene ug/kg 437574 76 56-137ND
Dibromochloromethane ug/kg 469574 82 53-139ND
Dibromomethane ug/kg 473574 82 60-136ND
Dichlorodifluoromethane ug/kg 653 IH574 114 49-177ND
Diisopropyl ether ug/kg 520574 91 53-136ND
Ethylbenzene ug/kg 469574 82 53-150ND
Hexachloro-1,3-butadiene ug/kg 460574 80 42-186ND
Isopropylbenzene (Cumene) ug/kg 515574 90 62-154ND
m&p-Xylene ug/kg 9871150 86 49-156ND
Methyl-tert-butyl ether ug/kg 465574 81 54-133ND
Methylene Chloride ug/kg 538574 94 50-153ND
n-Butylbenzene ug/kg 459574 80 44-174ND
n-Propylbenzene ug/kg 481574 84 52-157ND
Naphthalene ug/kg 490574 85 37-150ND
o-Xylene ug/kg 490574 85 54-150ND
p-Isopropyltoluene ug/kg 494574 86 50-164ND
sec-Butylbenzene ug/kg 493574 86 58-161ND
Styrene ug/kg 501574 87 60-148ND
tert-Butylbenzene ug/kg 477574 83 44-151ND
Tetrachloroethene ug/kg 464574 81 53-151ND
Toluene ug/kg 492574 86 52-148ND
trans-1,2-Dichloroethene ug/kg 514574 90 60-148ND
trans-1,3-Dichloropropene ug/kg 466574 81 55-133ND
Trichloroethene ug/kg 488574 85 60-148ND
Trichlorofluoromethane ug/kg 90.5574 16 10-154ND
Vinyl acetate ug/kg 9701150 85 50-149ND
Vinyl chloride ug/kg 465574 81 57-157ND
Xylene (Total) ug/kg 14801720 86 52-153ND
1,2-Dichloroethane-d4 (S) %103 70-130
4-Bromofluorobenzene (S) %105 70-130
Toluene-d8 (S) %102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92667323013
4021412SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB) ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg ND v2ND
2-Butanone (MEK) ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK) ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND v2ND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg ND IHND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene) ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92667323013
4021412SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total) ug/kg NDND
1,2-Dichloroethane-d4 (S) %105104
4-Bromofluorobenzene (S) %105104
Toluene-d8 (S) %101103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
775512
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92667253001, 92667253002, 92667253005, 92667253006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4024344
Associated Lab Samples:92667253001, 92667253002, 92667253005, 92667253006
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/19/23 02:34
1,1,1-Trichloroethane ug/kg ND 5.0 05/19/23 02:34
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/19/23 02:34
1,1,2-Trichloroethane ug/kg ND 5.0 05/19/23 02:34
1,1-Dichloroethane ug/kg ND 5.0 05/19/23 02:34
1,1-Dichloroethene ug/kg ND 5.0 05/19/23 02:34
1,1-Dichloropropene ug/kg ND 5.0 05/19/23 02:34
1,2,3-Trichlorobenzene ug/kg ND 5.0 05/19/23 02:34
1,2,3-Trichloropropane ug/kg ND 5.0 05/19/23 02:34
1,2,4-Trichlorobenzene ug/kg ND 5.0 05/19/23 02:34
1,2,4-Trimethylbenzene ug/kg ND 5.0 05/19/23 02:34
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 05/19/23 02:34
1,2-Dibromoethane (EDB) ug/kg ND 5.0 05/19/23 02:34
1,2-Dichlorobenzene ug/kg ND 5.0 05/19/23 02:34
1,2-Dichloroethane ug/kg ND 5.0 05/19/23 02:34
1,2-Dichloropropane ug/kg ND 5.0 05/19/23 02:34
1,3,5-Trimethylbenzene ug/kg ND 5.0 05/19/23 02:34
1,3-Dichlorobenzene ug/kg ND 5.0 05/19/23 02:34
1,3-Dichloropropane ug/kg ND 5.0 05/19/23 02:34
1,4-Dichlorobenzene ug/kg ND 5.0 05/19/23 02:34
2,2-Dichloropropane ug/kg ND 5.0 05/19/23 02:34
2-Butanone (MEK) ug/kg ND 100 05/19/23 02:34
2-Chlorotoluene ug/kg ND 5.0 05/19/23 02:34
2-Hexanone ug/kg ND 50.0 05/19/23 02:34
4-Chlorotoluene ug/kg ND 5.0 05/19/23 02:34
4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 05/19/23 02:34
Acetone ug/kg ND 100 05/19/23 02:34
Benzene ug/kg ND 5.0 05/19/23 02:34
Bromobenzene ug/kg ND 5.0 05/19/23 02:34
Bromochloromethane ug/kg ND 5.0 05/19/23 02:34
Bromodichloromethane ug/kg ND 5.0 05/19/23 02:34
Bromoform ug/kg ND 5.0 05/19/23 02:34
Bromomethane ug/kg ND 20.0 05/19/23 02:34
Carbon tetrachloride ug/kg ND 5.0 05/19/23 02:34
Chlorobenzene ug/kg ND 5.0 05/19/23 02:34
Chloroethane ug/kg ND 10.0 05/19/23 02:34
Chloroform ug/kg ND 5.0 05/19/23 02:34
Chloromethane ug/kg ND 10.0 05/19/23 02:34
cis-1,2-Dichloroethene ug/kg ND 5.0 05/19/23 02:34
cis-1,3-Dichloropropene ug/kg ND 5.0 05/19/23 02:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4024344
Associated Lab Samples:92667253001, 92667253002, 92667253005, 92667253006
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 05/19/23 02:34
Dibromomethane ug/kg ND 5.0 05/19/23 02:34
Dichlorodifluoromethane ug/kg ND 10.0 IH05/19/23 02:34
Diisopropyl ether ug/kg ND 5.0 05/19/23 02:34
Ethylbenzene ug/kg ND 5.0 05/19/23 02:34
Hexachloro-1,3-butadiene ug/kg ND 10.0 05/19/23 02:34
Isopropylbenzene (Cumene) ug/kg ND 5.0 05/19/23 02:34
m&p-Xylene ug/kg ND 10.0 05/19/23 02:34
Methyl-tert-butyl ether ug/kg ND 5.0 05/19/23 02:34
Methylene Chloride ug/kg ND 20.0 05/19/23 02:34
n-Butylbenzene ug/kg ND 5.0 05/19/23 02:34
n-Propylbenzene ug/kg ND 5.0 05/19/23 02:34
Naphthalene ug/kg ND 5.0 05/19/23 02:34
o-Xylene ug/kg ND 5.0 05/19/23 02:34
p-Isopropyltoluene ug/kg ND 5.0 05/19/23 02:34
sec-Butylbenzene ug/kg ND 5.0 05/19/23 02:34
Styrene ug/kg ND 5.0 05/19/23 02:34
tert-Butylbenzene ug/kg ND 5.0 05/19/23 02:34
Tetrachloroethene ug/kg ND 5.0 05/19/23 02:34
Toluene ug/kg ND 5.0 05/19/23 02:34
trans-1,2-Dichloroethene ug/kg ND 5.0 05/19/23 02:34
trans-1,3-Dichloropropene ug/kg ND 5.0 05/19/23 02:34
Trichloroethene ug/kg ND 5.0 05/19/23 02:34
Trichlorofluoromethane ug/kg ND 5.0 05/19/23 02:34
Vinyl acetate ug/kg ND 50.0 05/19/23 02:34
Vinyl chloride ug/kg ND 10.0 05/19/23 02:34
Xylene (Total) ug/kg ND 10.0 05/19/23 02:34
1,2-Dichloroethane-d4 (S) % 105 70-130 05/19/23 02:34
4-Bromofluorobenzene (S) % 105 70-130 05/19/23 02:34
Toluene-d8 (S) % 102 70-130 05/19/23 02:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4024345LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 474500 95 70-130
1,1,1-Trichloroethane ug/kg 503500 101 70-130
1,1,2,2-Tetrachloroethane ug/kg 495500 99 70-130
1,1,2-Trichloroethane ug/kg 486500 97 70-130
1,1-Dichloroethane ug/kg 532500 106 70-130
1,1-Dichloroethene ug/kg 572500 114 70-130
1,1-Dichloropropene ug/kg 541500 108 70-130
1,2,3-Trichlorobenzene ug/kg 499500 100 70-130
1,2,3-Trichloropropane ug/kg 486500 97 70-130
1,2,4-Trichlorobenzene ug/kg 492500 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4024345LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 503500 101 70-130
1,2-Dibromo-3-chloropropane ug/kg 459500 92 67-130
1,2-Dibromoethane (EDB) ug/kg 479500 96 70-130
1,2-Dichlorobenzene ug/kg 485500 97 70-130
1,2-Dichloroethane ug/kg 495500 99 70-130
1,2-Dichloropropane ug/kg 520500 104 70-130
1,3,5-Trimethylbenzene ug/kg 523500 105 70-130
1,3-Dichlorobenzene ug/kg 483500 97 70-130
1,3-Dichloropropane ug/kg 490500 98 70-130
1,4-Dichlorobenzene ug/kg 456500 91 70-130
2,2-Dichloropropane ug/kg 468500 94 67-130
2-Butanone (MEK) ug/kg 10201000 102 66-130
2-Chlorotoluene ug/kg 514500 103 70-130
2-Hexanone ug/kg 10501000 105 70-130
4-Chlorotoluene ug/kg 514500 103 70-130
4-Methyl-2-pentanone (MIBK) ug/kg 10601000 106 70-130
Acetone ug/kg 9931000 99 67-130
Benzene ug/kg 495500 99 70-130
Bromobenzene ug/kg 496500 99 70-130
Bromochloromethane ug/kg 493500 99 70-130
Bromodichloromethane ug/kg 485500 97 70-130
Bromoform ug/kg 446500 89 70-130
Bromomethane ug/kg 378500 76 53-175
Carbon tetrachloride ug/kg 500500 100 70-130
Chlorobenzene ug/kg 494500 99 70-130
Chloroethane ug/kg 528500 106 70-135
Chloroform ug/kg 499500 100 70-130
Chloromethane ug/kg 628500 126 64-130
cis-1,2-Dichloroethene ug/kg 523500 105 70-130
cis-1,3-Dichloropropene ug/kg 453500 91 70-130
Dibromochloromethane ug/kg 473500 95 70-130
Dibromomethane ug/kg 471500 94 70-130
Dichlorodifluoromethane ug/kg 630 IH500 126 63-145
Diisopropyl ether ug/kg 526500 105 68-130
Ethylbenzene ug/kg 463500 93 70-130
Hexachloro-1,3-butadiene ug/kg 485500 97 70-130
Isopropylbenzene (Cumene) ug/kg 508500 102 70-130
m&p-Xylene ug/kg 9991000 100 70-130
Methyl-tert-butyl ether ug/kg 465500 93 70-130
Methylene Chloride ug/kg 527500 105 67-130
n-Butylbenzene ug/kg 514500 103 70-130
n-Propylbenzene ug/kg 516500 103 70-130
Naphthalene ug/kg 490500 98 70-130
o-Xylene ug/kg 493500 99 70-130
p-Isopropyltoluene ug/kg 521500 104 70-130
sec-Butylbenzene ug/kg 503500 101 70-130
Styrene ug/kg 504500 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4024345LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 527500 105 64-130
Tetrachloroethene ug/kg 483500 97 70-130
Toluene ug/kg 484500 97 70-130
trans-1,2-Dichloroethene ug/kg 568500 114 70-130
trans-1,3-Dichloropropene ug/kg 485500 97 70-130
Trichloroethene ug/kg 495500 99 70-130
Trichlorofluoromethane ug/kg 460500 92 70-130
Vinyl acetate ug/kg 10401000 104 70-134
Vinyl chloride ug/kg 489500 98 68-130
Xylene (Total) ug/kg 14901500 99 70-130
1,2-Dichloroethane-d4 (S) %98 70-130
4-Bromofluorobenzene (S) %104 70-130
Toluene-d8 (S) %101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4024346MATRIX SPIKE SAMPLE:
MSSpike
Result
92667633017
1,1,1,2-Tetrachloroethane ug/kg 780705 111 58-140ND
1,1,1-Trichloroethane ug/kg 836705 119 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 805705 114 52-139ND
1,1,2-Trichloroethane ug/kg 810705 115 56-140ND
1,1-Dichloroethane ug/kg 874705 124 58-145ND
1,1-Dichloroethene ug/kg 886705 126 57-158ND
1,1-Dichloropropene ug/kg 769705 109 58-151ND
1,2,3-Trichlorobenzene ug/kg 666705 94 48-149ND
1,2,3-Trichloropropane ug/kg 757705 107 54-132ND
1,2,4-Trichlorobenzene ug/kg 606705 86 51-151ND
1,2,4-Trimethylbenzene ug/kg 781705 109 38-17012.5
1,2-Dibromo-3-chloropropane ug/kg 725705 103 44-134ND
1,2-Dibromoethane (EDB) ug/kg 789705 112 60-138ND
1,2-Dichlorobenzene ug/kg 709705 101 59-147ND
1,2-Dichloroethane ug/kg 789705 112 57-139ND
1,2-Dichloropropane ug/kg 862705 122 62-145ND
1,3,5-Trimethylbenzene ug/kg 730705 104 47-159ND
1,3-Dichlorobenzene ug/kg 625705 89 58-144ND
1,3-Dichloropropane ug/kg 793705 113 60-142ND
1,4-Dichlorobenzene ug/kg 596705 84 57-143ND
2,2-Dichloropropane ug/kg 713705 101 37-144ND
2-Butanone (MEK) ug/kg 16601410 118 28-146ND
2-Chlorotoluene ug/kg 708705 100 55-158ND
2-Hexanone ug/kg 16101410 114 44-141ND
4-Chlorotoluene ug/kg 679705 96 55-146ND
4-Methyl-2-pentanone (MIBK) ug/kg 16901410 120 50-138ND
Acetone ug/kg 14901410 105 20-136ND
Benzene ug/kg 810705 115 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4024346MATRIX SPIKE SAMPLE:
MSSpike
Result
92667633017
Bromobenzene ug/kg 725705 103 59-145ND
Bromochloromethane ug/kg 805705 114 57-143ND
Bromodichloromethane ug/kg 788705 112 53-133ND
Bromoform ug/kg 724705 103 48-133ND
Bromomethane ug/kg 132705 19 10-167ND
Carbon tetrachloride ug/kg 644705 91 57-147ND
Chlorobenzene ug/kg 736705 104 61-144ND
Chloroethane ug/kg 147705 21 10-153ND
Chloroform ug/kg 823705 117 58-141ND
Chloromethane ug/kg 1050705 149 54-165ND
cis-1,2-Dichloroethene ug/kg 851705 121 59-144ND
cis-1,3-Dichloropropene ug/kg 734705 104 56-137ND
Dibromochloromethane ug/kg 760705 108 53-139ND
Dibromomethane ug/kg 785705 111 60-136ND
Dichlorodifluoromethane ug/kg 944 IH705 134 49-177ND
Diisopropyl ether ug/kg 878705 124 53-136ND
Ethylbenzene ug/kg 663705 93 53-150ND
Hexachloro-1,3-butadiene ug/kg 567705 80 42-186ND
Isopropylbenzene (Cumene) ug/kg 732705 104 62-154ND
m&p-Xylene ug/kg 13801410 97 49-156ND
Methyl-tert-butyl ether ug/kg 782705 111 54-133ND
Methylene Chloride ug/kg 856705 121 50-153ND
n-Butylbenzene ug/kg 558705 79 44-174ND
n-Propylbenzene ug/kg 664705 94 52-157ND
Naphthalene ug/kg 742705 105 37-150ND
o-Xylene ug/kg 727705 103 54-150ND
p-Isopropyltoluene ug/kg 656705 93 50-164ND
sec-Butylbenzene ug/kg 658705 93 58-161ND
Styrene ug/kg 733705 104 60-148ND
tert-Butylbenzene ug/kg 683705 97 44-151ND
Tetrachloroethene ug/kg 576705 82 53-151ND
Toluene ug/kg 797705 106 52-14852.7
trans-1,2-Dichloroethene ug/kg 807705 114 60-148ND
trans-1,3-Dichloropropene ug/kg 777705 110 55-133ND
Trichloroethene ug/kg 727705 103 60-148ND
Trichlorofluoromethane ug/kg 119705 17 10-154ND
Vinyl acetate ug/kg 16501410 117 50-149ND
Vinyl chloride ug/kg 791705 112 57-157ND
Xylene (Total) ug/kg 21102120 100 52-153ND
1,2-Dichloroethane-d4 (S) %100 70-130
4-Bromofluorobenzene (S) %106 70-130
Toluene-d8 (S) %102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92667633002
4024347SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg 8.8 68.3
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB) ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK) ug/kg NDND
2-Chlorotoluene ug/kg 7.3JND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg 7.8ND
4-Methyl-2-pentanone (MIBK) ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg ND IHND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 5.6JND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene) ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92667633002
4024347SAMPLE DUPLICATE:
m&p-Xylene ug/kg 5.8JND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 543 4522
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total) ug/kg NDND
1,2-Dichloroethane-d4 (S) %104104
4-Bromofluorobenzene (S) %106104
Toluene-d8 (S) %102103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
776194
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92667253003, 92667253004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4027241
Associated Lab Samples:92667253003, 92667253004
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/23/23 09:11
1,1,1-Trichloroethane ug/kg ND 5.0 05/23/23 09:11
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/23/23 09:11
1,1,2-Trichloroethane ug/kg ND 5.0 05/23/23 09:11
1,1-Dichloroethane ug/kg ND 5.0 05/23/23 09:11
1,1-Dichloroethene ug/kg ND 5.0 05/23/23 09:11
1,1-Dichloropropene ug/kg ND 5.0 05/23/23 09:11
1,2,3-Trichlorobenzene ug/kg ND 5.0 05/23/23 09:11
1,2,3-Trichloropropane ug/kg ND 5.0 05/23/23 09:11
1,2,4-Trichlorobenzene ug/kg ND 5.0 05/23/23 09:11
1,2,4-Trimethylbenzene ug/kg ND 5.0 05/23/23 09:11
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 05/23/23 09:11
1,2-Dibromoethane (EDB) ug/kg ND 5.0 05/23/23 09:11
1,2-Dichlorobenzene ug/kg ND 5.0 05/23/23 09:11
1,2-Dichloroethane ug/kg ND 5.0 05/23/23 09:11
1,2-Dichloropropane ug/kg ND 5.0 05/23/23 09:11
1,3,5-Trimethylbenzene ug/kg ND 5.0 05/23/23 09:11
1,3-Dichlorobenzene ug/kg ND 5.0 05/23/23 09:11
1,3-Dichloropropane ug/kg ND 5.0 05/23/23 09:11
1,4-Dichlorobenzene ug/kg ND 5.0 05/23/23 09:11
2,2-Dichloropropane ug/kg ND 5.0 v205/23/23 09:11
2-Butanone (MEK) ug/kg ND 100 05/23/23 09:11
2-Chlorotoluene ug/kg ND 5.0 05/23/23 09:11
2-Hexanone ug/kg ND 50.0 05/23/23 09:11
4-Chlorotoluene ug/kg ND 5.0 05/23/23 09:11
4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 05/23/23 09:11
Acetone ug/kg ND 100 05/23/23 09:11
Benzene ug/kg ND 5.0 05/23/23 09:11
Bromobenzene ug/kg ND 5.0 05/23/23 09:11
Bromochloromethane ug/kg ND 5.0 05/23/23 09:11
Bromodichloromethane ug/kg ND 5.0 05/23/23 09:11
Bromoform ug/kg ND 5.0 05/23/23 09:11
Bromomethane ug/kg ND 20.0 v205/23/23 09:11
Carbon tetrachloride ug/kg ND 5.0 05/23/23 09:11
Chlorobenzene ug/kg ND 5.0 05/23/23 09:11
Chloroethane ug/kg ND 10.0 05/23/23 09:11
Chloroform ug/kg ND 5.0 05/23/23 09:11
Chloromethane ug/kg ND 10.0 05/23/23 09:11
cis-1,2-Dichloroethene ug/kg ND 5.0 05/23/23 09:11
cis-1,3-Dichloropropene ug/kg ND 5.0 05/23/23 09:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4027241
Associated Lab Samples:92667253003, 92667253004
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 05/23/23 09:11
Dibromomethane ug/kg ND 5.0 05/23/23 09:11
Dichlorodifluoromethane ug/kg ND 10.0 IH,v205/23/23 09:11
Diisopropyl ether ug/kg ND 5.0 05/23/23 09:11
Ethylbenzene ug/kg ND 5.0 05/23/23 09:11
Hexachloro-1,3-butadiene ug/kg ND 10.0 05/23/23 09:11
Isopropylbenzene (Cumene) ug/kg ND 5.0 05/23/23 09:11
m&p-Xylene ug/kg ND 10.0 05/23/23 09:11
Methyl-tert-butyl ether ug/kg ND 5.0 05/23/23 09:11
Methylene Chloride ug/kg ND 20.0 05/23/23 09:11
n-Butylbenzene ug/kg ND 5.0 05/23/23 09:11
n-Propylbenzene ug/kg ND 5.0 05/23/23 09:11
Naphthalene ug/kg ND 5.0 05/23/23 09:11
o-Xylene ug/kg ND 5.0 05/23/23 09:11
p-Isopropyltoluene ug/kg ND 5.0 05/23/23 09:11
sec-Butylbenzene ug/kg ND 5.0 05/23/23 09:11
Styrene ug/kg ND 5.0 05/23/23 09:11
tert-Butylbenzene ug/kg ND 5.0 05/23/23 09:11
Tetrachloroethene ug/kg ND 5.0 05/23/23 09:11
Toluene ug/kg ND 5.0 05/23/23 09:11
trans-1,2-Dichloroethene ug/kg ND 5.0 05/23/23 09:11
trans-1,3-Dichloropropene ug/kg ND 5.0 05/23/23 09:11
Trichloroethene ug/kg ND 5.0 05/23/23 09:11
Trichlorofluoromethane ug/kg ND 5.0 05/23/23 09:11
Vinyl acetate ug/kg ND 50.0 05/23/23 09:11
Vinyl chloride ug/kg ND 10.0 05/23/23 09:11
Xylene (Total) ug/kg ND 10.0 05/23/23 09:11
1,2-Dichloroethane-d4 (S) % 105 70-130 05/23/23 09:11
4-Bromofluorobenzene (S) % 105 70-130 05/23/23 09:11
Toluene-d8 (S) % 102 70-130 05/23/23 09:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4027242LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 398500 80 70-130
1,1,1-Trichloroethane ug/kg 401500 80 70-130
1,1,2,2-Tetrachloroethane ug/kg 418500 84 70-130
1,1,2-Trichloroethane ug/kg 395500 79 70-130
1,1-Dichloroethane ug/kg 436500 87 70-130
1,1-Dichloroethene ug/kg 451500 90 70-130
1,1-Dichloropropene ug/kg 436500 87 70-130
1,2,3-Trichlorobenzene ug/kg 423500 85 70-130
1,2,3-Trichloropropane ug/kg 407500 81 70-130
1,2,4-Trichlorobenzene ug/kg 422500 84 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4027242LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 440500 88 70-130
1,2-Dibromo-3-chloropropane ug/kg 387500 77 67-130
1,2-Dibromoethane (EDB) ug/kg 411500 82 70-130
1,2-Dichlorobenzene ug/kg 416500 83 70-130
1,2-Dichloroethane ug/kg 398500 80 70-130
1,2-Dichloropropane ug/kg 432500 86 70-130
1,3,5-Trimethylbenzene ug/kg 443500 89 70-130
1,3-Dichlorobenzene ug/kg 417500 83 70-130
1,3-Dichloropropane ug/kg 417500 83 70-130
1,4-Dichlorobenzene ug/kg 387500 77 70-130
2,2-Dichloropropane ug/kg 348 v3500 70 67-130
2-Butanone (MEK) ug/kg 8621000 86 66-130
2-Chlorotoluene ug/kg 435500 87 70-130
2-Hexanone ug/kg 8911000 89 70-130
4-Chlorotoluene ug/kg 442500 88 70-130
4-Methyl-2-pentanone (MIBK) ug/kg 8781000 88 70-130
Acetone ug/kg 8091000 81 67-130
Benzene ug/kg 402500 80 70-130
Bromobenzene ug/kg 415500 83 70-130
Bromochloromethane ug/kg 408500 82 70-130
Bromodichloromethane ug/kg 392500 78 70-130
Bromoform ug/kg 374500 75 70-130
Bromomethane ug/kg 271 v3500 54 53-175
Carbon tetrachloride ug/kg 400500 80 70-130
Chlorobenzene ug/kg 414500 83 70-130
Chloroethane ug/kg 424500 85 70-135
Chloroform ug/kg 407500 81 70-130
Chloromethane ug/kg 463500 93 64-130
cis-1,2-Dichloroethene ug/kg 435500 87 70-130
cis-1,3-Dichloropropene ug/kg 367500 73 70-130
Dibromochloromethane ug/kg 396500 79 70-130
Dibromomethane ug/kg 384500 77 70-130
Dichlorodifluoromethane ug/kg 331 IH,v3500 66 63-145
Diisopropyl ether ug/kg 449500 90 68-130
Ethylbenzene ug/kg 389500 78 70-130
Hexachloro-1,3-butadiene ug/kg 398500 80 70-130
Isopropylbenzene (Cumene) ug/kg 427500 85 70-130
m&p-Xylene ug/kg 8431000 84 70-130
Methyl-tert-butyl ether ug/kg 391500 78 70-130
Methylene Chloride ug/kg 434500 87 67-130
n-Butylbenzene ug/kg 433500 87 70-130
n-Propylbenzene ug/kg 434500 87 70-130
Naphthalene ug/kg 425500 85 70-130
o-Xylene ug/kg 412500 82 70-130
p-Isopropyltoluene ug/kg 443500 89 70-130
sec-Butylbenzene ug/kg 427500 85 70-130
Styrene ug/kg 428500 86 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4027242LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 458500 92 64-130
Tetrachloroethene ug/kg 406500 81 70-130
Toluene ug/kg 393500 79 70-130
trans-1,2-Dichloroethene ug/kg 459500 92 70-130
trans-1,3-Dichloropropene ug/kg 392500 78 70-130
Trichloroethene ug/kg 395500 79 70-130
Trichlorofluoromethane ug/kg 351500 70 70-130
Vinyl acetate ug/kg 8621000 86 70-134
Vinyl chloride ug/kg 378500 76 68-130
Xylene (Total) ug/kg 12601500 84 70-130
1,2-Dichloroethane-d4 (S) %98 70-130
4-Bromofluorobenzene (S) %105 70-130
Toluene-d8 (S) %100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4027243MATRIX SPIKE SAMPLE:
MSSpike
Result
92668398008
1,1,1,2-Tetrachloroethane ug/kg 921905 102 58-140ND
1,1,1-Trichloroethane ug/kg 951905 105 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 944905 104 52-139ND
1,1,2-Trichloroethane ug/kg 926905 102 56-140ND
1,1-Dichloroethane ug/kg 1010905 111 58-145ND
1,1-Dichloroethene ug/kg 1030905 113 57-158ND
1,1-Dichloropropene ug/kg 949905 105 58-151ND
1,2,3-Trichlorobenzene ug/kg 875905 97 48-149ND
1,2,3-Trichloropropane ug/kg 898905 99 54-132ND
1,2,4-Trichlorobenzene ug/kg 830905 92 51-151ND
1,2,4-Trimethylbenzene ug/kg 936905 103 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 881905 97 44-134ND
1,2-Dibromoethane (EDB) ug/kg 923905 102 60-138ND
1,2-Dichlorobenzene ug/kg 888905 98 59-147ND
1,2-Dichloroethane ug/kg 883905 97 57-139ND
1,2-Dichloropropane ug/kg 1010905 111 62-145ND
1,3,5-Trimethylbenzene ug/kg 923905 102 47-159ND
1,3-Dichlorobenzene ug/kg 828905 91 58-144ND
1,3-Dichloropropane ug/kg 935905 103 60-142ND
1,4-Dichlorobenzene ug/kg 765905 85 57-143ND
2,2-Dichloropropane ug/kg 783 v3905 87 37-144ND
2-Butanone (MEK) ug/kg 18501820 102 28-146ND
2-Chlorotoluene ug/kg 900905 99 55-158ND
2-Hexanone ug/kg 19001820 105 44-141ND
4-Chlorotoluene ug/kg 874905 97 55-146ND
4-Methyl-2-pentanone (MIBK) ug/kg 19201820 106 50-138ND
Acetone ug/kg 17401820 96 20-136ND
Benzene ug/kg 937905 104 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4027243MATRIX SPIKE SAMPLE:
MSSpike
Result
92668398008
Bromobenzene ug/kg 892905 98 59-145ND
Bromochloromethane ug/kg 919905 101 57-143ND
Bromodichloromethane ug/kg 888905 98 53-133ND
Bromoform ug/kg 841905 93 48-133ND
Bromomethane ug/kg 148 v3905 16 10-167ND
Carbon tetrachloride ug/kg 807905 89 57-147ND
Chlorobenzene ug/kg 907905 100 61-144ND
Chloroethane ug/kg 209905 23 10-153ND
Chloroform ug/kg 938905 104 58-141ND
Chloromethane ug/kg 1110905 123 54-165ND
cis-1,2-Dichloroethene ug/kg 984905 109 59-144ND
cis-1,3-Dichloropropene ug/kg 831905 92 56-137ND
Dibromochloromethane ug/kg 879905 97 53-139ND
Dibromomethane ug/kg 871905 96 60-136ND
Dichlorodifluoromethane ug/kg 857 IH,v3905 95 49-177ND
Diisopropyl ether ug/kg 1010905 112 53-136ND
Ethylbenzene ug/kg 843905 93 53-150ND
Hexachloro-1,3-butadiene ug/kg 952905 105 42-186ND
Isopropylbenzene (Cumene) ug/kg 932905 103 62-154ND
m&p-Xylene ug/kg 17801820 98 49-156ND
Methyl-tert-butyl ether ug/kg 873905 96 54-133ND
Methylene Chloride ug/kg 989905 109 50-153ND
n-Butylbenzene ug/kg 834905 92 44-174ND
n-Propylbenzene ug/kg 865905 96 52-157ND
Naphthalene ug/kg 921905 102 37-150ND
o-Xylene ug/kg 906905 100 54-150ND
p-Isopropyltoluene ug/kg 880905 97 50-164ND
sec-Butylbenzene ug/kg 905905 100 58-161ND
Styrene ug/kg 925905 102 60-148ND
tert-Butylbenzene ug/kg 901905 99 44-151ND
Tetrachloroethene ug/kg 768905 85 53-151ND
Toluene ug/kg 903905 100 52-148ND
trans-1,2-Dichloroethene ug/kg 964905 106 60-148ND
trans-1,3-Dichloropropene ug/kg 868905 96 55-133ND
Trichloroethene ug/kg 870905 96 60-148ND
Trichlorofluoromethane ug/kg 192905 21 10-154ND
Vinyl acetate ug/kg 18201820 101 50-149ND
Vinyl chloride ug/kg 867905 96 57-157ND
Xylene (Total) ug/kg 26802710 99 52-153ND
1,2-Dichloroethane-d4 (S) %95 70-130
4-Bromofluorobenzene (S) %106 70-130
Toluene-d8 (S) %101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92668398009
4027244SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB) ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg ND v2ND
2-Butanone (MEK) ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK) ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND v2ND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg ND IH,v2ND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene) ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92668398009
4027244SAMPLE DUPLICATE:
m&p-Xylene ug/kg 6JND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 19.1 019.0
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total) ug/kg NDND
1,2-Dichloroethane-d4 (S) %101102
4-Bromofluorobenzene (S) %105106
Toluene-d8 (S) %101102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
774649
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples:92667253001, 92667253002, 92667253003, 92667253004, 92667253005, 92667253006, 92667253007,
92667253008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4020024
Associated Lab Samples: 92667253001, 92667253002, 92667253003, 92667253004, 92667253005, 92667253006, 92667253007,
92667253008
Matrix: Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 329 05/17/23 07:56
1,2-Dichlorobenzene ug/kg ND 329 05/17/23 07:56
1,3-Dichlorobenzene ug/kg ND 329 05/17/23 07:56
1,4-Dichlorobenzene ug/kg ND 329 05/17/23 07:56
1-Methylnaphthalene ug/kg ND 329 05/17/23 07:56
2,2'-Oxybis(1-chloropropane) ug/kg ND 329 05/17/23 07:56
2,4,5-Trichlorophenol ug/kg ND 329 05/17/23 07:56
2,4,6-Trichlorophenol ug/kg ND 329 05/17/23 07:56
2,4-Dichlorophenol ug/kg ND 329 05/17/23 07:56
2,4-Dimethylphenol ug/kg ND 329 05/17/23 07:56
2,4-Dinitrophenol ug/kg ND 1640 05/17/23 07:56
2,4-Dinitrotoluene ug/kg ND 329 05/17/23 07:56
2,6-Dinitrotoluene ug/kg ND 329 05/17/23 07:56
2-Chloronaphthalene ug/kg ND 329 05/17/23 07:56
2-Chlorophenol ug/kg ND 329 05/17/23 07:56
2-Methylnaphthalene ug/kg ND 329 05/17/23 07:56
2-Methylphenol(o-Cresol) ug/kg ND 329 05/17/23 07:56
2-Nitroaniline ug/kg ND 1640 05/17/23 07:56
2-Nitrophenol ug/kg ND 329 05/17/23 07:56
3&4-Methylphenol(m&p Cresol) ug/kg ND 329 05/17/23 07:56
3,3'-Dichlorobenzidine ug/kg ND 658 05/17/23 07:56
3-Nitroaniline ug/kg ND 1640 05/17/23 07:56
4,6-Dinitro-2-methylphenol ug/kg ND 658 05/17/23 07:56
4-Bromophenylphenyl ether ug/kg ND 329 05/17/23 07:56
4-Chloro-3-methylphenol ug/kg ND 658 05/17/23 07:56
4-Chloroaniline ug/kg ND 658 05/17/23 07:56
4-Chlorophenylphenyl ether ug/kg ND 329 05/17/23 07:56
4-Nitroaniline ug/kg ND 658 05/17/23 07:56
4-Nitrophenol ug/kg ND 1640 05/17/23 07:56
Acenaphthene ug/kg ND 329 05/17/23 07:56
Acenaphthylene ug/kg ND 329 05/17/23 07:56
Aniline ug/kg ND 329 05/17/23 07:56
Anthracene ug/kg ND 329 05/17/23 07:56
Benzo(a)anthracene ug/kg ND 329 05/17/23 07:56
Benzo(a)pyrene ug/kg ND 329 05/17/23 07:56
Benzo(b)fluoranthene ug/kg ND 329 05/17/23 07:56
Benzo(g,h,i)perylene ug/kg ND 329 05/17/23 07:56
Benzo(k)fluoranthene ug/kg ND 329 05/17/23 07:56
Benzoic Acid ug/kg ND 1640 05/17/23 07:56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4020024
Associated Lab Samples: 92667253001, 92667253002, 92667253003, 92667253004, 92667253005, 92667253006, 92667253007,
92667253008
Matrix: Solid
Analyzed
Benzyl alcohol ug/kg ND 658 05/17/23 07:56
bis(2-Chloroethoxy)methane ug/kg ND 329 05/17/23 07:56
bis(2-Chloroethyl) ether ug/kg ND 329 05/17/23 07:56
bis(2-Ethylhexyl)phthalate ug/kg ND 329 05/17/23 07:56
Butylbenzylphthalate ug/kg ND 329 05/17/23 07:56
Chrysene ug/kg ND 329 05/17/23 07:56
Di-n-butylphthalate ug/kg ND 329 05/17/23 07:56
Di-n-octylphthalate ug/kg ND 329 05/17/23 07:56
Dibenz(a,h)anthracene ug/kg ND 329 05/17/23 07:56
Dibenzofuran ug/kg ND 329 05/17/23 07:56
Diethylphthalate ug/kg ND 329 05/17/23 07:56
Dimethylphthalate ug/kg ND 329 05/17/23 07:56
Fluoranthene ug/kg ND 329 05/17/23 07:56
Fluorene ug/kg ND 329 05/17/23 07:56
Hexachloro-1,3-butadiene ug/kg ND 329 05/17/23 07:56
Hexachlorobenzene ug/kg ND 329 05/17/23 07:56
Hexachlorocyclopentadiene ug/kg ND 329 05/17/23 07:56
Hexachloroethane ug/kg ND 329 05/17/23 07:56
Indeno(1,2,3-cd)pyrene ug/kg ND 329 05/17/23 07:56
Isophorone ug/kg ND 329 05/17/23 07:56
N-Nitroso-di-n-propylamine ug/kg ND 329 05/17/23 07:56
N-Nitrosodimethylamine ug/kg ND 329 05/17/23 07:56
N-Nitrosodiphenylamine ug/kg ND 329 05/17/23 07:56
Naphthalene ug/kg ND 329 05/17/23 07:56
Nitrobenzene ug/kg ND 329 05/17/23 07:56
Pentachlorophenol ug/kg ND 658 05/17/23 07:56
Phenanthrene ug/kg ND 329 05/17/23 07:56
Phenol ug/kg ND 329 05/17/23 07:56
Pyrene ug/kg ND 329 05/17/23 07:56
Pyridine ug/kg ND 329 05/17/23 07:56
2,4,6-Tribromophenol (S) % 65 10-131 05/17/23 07:56
2-Fluorobiphenyl (S) % 61 10-130 05/17/23 07:56
2-Fluorophenol (S) % 55 10-130 05/17/23 07:56
Nitrobenzene-d5 (S) % 57 10-130 05/17/23 07:56
Phenol-d6 (S) % 53 10-130 05/17/23 07:56
Terphenyl-d14 (S) % 66 10-130 05/17/23 07:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4020025LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11501690 68 43-130
1,2-Dichlorobenzene ug/kg 11001690 65 43-130
1,3-Dichlorobenzene ug/kg 11001690 65 43-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4020025LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/kg 10901690 65 44-130
1-Methylnaphthalene ug/kg 11101690 66 47-130
2,2'-Oxybis(1-chloropropane) ug/kg 8951690 53 29-130
2,4,5-Trichlorophenol ug/kg 11601690 69 47-130
2,4,6-Trichlorophenol ug/kg 11901690 70 47-130
2,4-Dichlorophenol ug/kg 11501690 68 45-130
2,4-Dimethylphenol ug/kg 15901690 94 45-130
2,4-Dinitrophenol ug/kg 54108450 64 27-140
2,4-Dinitrotoluene ug/kg 11201690 66 46-130
2,6-Dinitrotoluene ug/kg 11301690 67 48-130
2-Chloronaphthalene ug/kg 11301690 67 46-130
2-Chlorophenol ug/kg 11201690 66 43-130
2-Methylnaphthalene ug/kg 10601690 63 47-130
2-Methylphenol(o-Cresol) ug/kg 10601690 63 42-130
2-Nitroaniline ug/kg 20203380 60 41-130
2-Nitrophenol ug/kg 11401690 67 48-130
3&4-Methylphenol(m&p Cresol) ug/kg 10401690 62 39-130
3,3'-Dichlorobenzidine ug/kg 20003380 59 41-130
3-Nitroaniline ug/kg 20303380 60 37-130
4,6-Dinitro-2-methylphenol ug/kg 23703380 70 38-141
4-Bromophenylphenyl ether ug/kg 11701690 69 47-130
4-Chloro-3-methylphenol ug/kg 21603380 64 44-130
4-Chloroaniline ug/kg 20003380 59 41-130
4-Chlorophenylphenyl ether ug/kg 11001690 65 45-130
4-Nitroaniline ug/kg 20403380 60 42-130
4-Nitrophenol ug/kg 50608450 60 39-131
Acenaphthene ug/kg 11101690 66 49-130
Acenaphthylene ug/kg 11301690 67 50-130
Aniline ug/kg 8641690 51 38-130
Anthracene ug/kg 10901690 64 49-130
Benzo(a)anthracene ug/kg 11401690 68 51-130
Benzo(a)pyrene ug/kg 11401690 68 51-130
Benzo(b)fluoranthene ug/kg 11101690 66 49-130
Benzo(g,h,i)perylene ug/kg 13301690 79 48-140
Benzo(k)fluoranthene ug/kg 11801690 70 51-130
Benzoic Acid ug/kg 32908450 39 22-130
Benzyl alcohol ug/kg 19203380 57 43-130
bis(2-Chloroethoxy)methane ug/kg 9791690 58 43-130
bis(2-Chloroethyl) ether ug/kg 9681690 57 42-130
bis(2-Ethylhexyl)phthalate ug/kg 11001690 65 43-130
Butylbenzylphthalate ug/kg 10901690 64 44-131
Chrysene ug/kg 11801690 70 51-130
Di-n-butylphthalate ug/kg 10701690 64 46-130
Di-n-octylphthalate ug/kg 10501690 62 45-130
Dibenz(a,h)anthracene ug/kg 13101690 77 48-130
Dibenzofuran ug/kg 11301690 67 10-130
Diethylphthalate ug/kg 10601690 63 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4020025LABORATORY CONTROL SAMPLE:
LCSSpike
Dimethylphthalate ug/kg 10701690 63 48-130
Fluoranthene ug/kg 11301690 67 48-130
Fluorene ug/kg 11201690 67 48-130
Hexachloro-1,3-butadiene ug/kg 11801690 70 39-130
Hexachlorobenzene ug/kg 11801690 70 47-130
Hexachlorocyclopentadiene ug/kg 11001690 65 17-130
Hexachloroethane ug/kg 10801690 64 40-130
Indeno(1,2,3-cd)pyrene ug/kg 13201690 78 50-130
Isophorone ug/kg 9861690 58 41-130
N-Nitroso-di-n-propylamine ug/kg 9521690 56 36-130
N-Nitrosodimethylamine ug/kg 9941690 59 34-130
N-Nitrosodiphenylamine ug/kg 11401690 68 48-130
Naphthalene ug/kg 11401690 67 46-130
Nitrobenzene ug/kg 10601690 63 39-130
Pentachlorophenol ug/kg 18903380 56 42-130
Phenanthrene ug/kg 11801690 70 50-130
Phenol ug/kg 11401690 68 42-130
Pyrene ug/kg 12001690 71 50-130
Pyridine ug/kg 8711690 52 26-130
2,4,6-Tribromophenol (S) %72 10-131
2-Fluorobiphenyl (S) %67 10-130
2-Fluorophenol (S) %63 10-130
Nitrobenzene-d5 (S) %64 10-130
Phenol-d6 (S) %61 10-130
Terphenyl-d14 (S) %70 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4020026MATRIX SPIKE SAMPLE:
MSSpike
Result
92667337001
1,2,4-Trichlorobenzene ug/kg 12402030 61 16-130<159
1,2-Dichlorobenzene ug/kg 12202030 60 19-130<146
1,3-Dichlorobenzene ug/kg 11902030 58 19-130<143
1,4-Dichlorobenzene ug/kg 11802030 58 20-130<154
1-Methylnaphthalene ug/kg 11802030 58 19-130<142
2,2'-Oxybis(1-chloropropane) ug/kg 9692030 48 10-130<192
2,4,5-Trichlorophenol ug/kg 12602030 62 19-130<185
2,4,6-Trichlorophenol ug/kg 13202030 65 18-130<166
2,4-Dichlorophenol ug/kg 12802030 63 16-130<158
2,4-Dimethylphenol ug/kg 17502030 86 10-130<168
2,4-Dinitrophenol ug/kg 674010200 66 10-143<1250
2,4-Dinitrotoluene ug/kg 12602030 62 19-130<155
2,6-Dinitrotoluene ug/kg 12702030 62 22-130<148
2-Chloronaphthalene ug/kg 11902030 59 18-130<160
2-Chlorophenol ug/kg 12102030 60 20-130<152
2-Methylnaphthalene ug/kg 11402030 56 18-130<161
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
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Page 60 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4020026MATRIX SPIKE SAMPLE:
MSSpike
Result
92667337001
2-Methylphenol(o-Cresol) ug/kg 11902030 58 13-130<165
2-Nitroaniline ug/kg 23404070 58 18-130<330
2-Nitrophenol ug/kg 12502030 61 19-130<175
3&4-Methylphenol(m&p Cresol) ug/kg 11702030 57 13-130<163
3,3'-Dichlorobenzidine ug/kg 23404070 58 10-130<273
3-Nitroaniline ug/kg 23104070 57 22-130<317
4,6-Dinitro-2-methylphenol ug/kg 27804070 68 10-144<377
4-Bromophenylphenyl ether ug/kg 12102030 60 18-130<155
4-Chloro-3-methylphenol ug/kg 23904070 59 16-130<284
4-Chloroaniline ug/kg 22504070 55 17-130<317
4-Chlorophenylphenyl ether ug/kg 12202030 60 17-130<150
4-Nitroaniline ug/kg 23704070 58 21-130<307
4-Nitrophenol ug/kg 594010200 58 13-131<780
Acenaphthene ug/kg 12102030 59 20-130<142
Acenaphthylene ug/kg 12402030 61 21-130<142
Aniline ug/kg 9052030 45 10-130<158
Anthracene ug/kg 11902030 59 19-130<132
Benzo(a)anthracene ug/kg 12102030 60 17-130<135
Benzo(a)pyrene ug/kg 11902030 59 14-130<139
Benzo(b)fluoranthene ug/kg 11702030 57 11-134<135
Benzo(g,h,i)perylene ug/kg 14102030 69 12-130<157
Benzo(k)fluoranthene ug/kg 12102030 59 15-130<142
Benzoic Acid ug/kg 531010200 52 10-130<867
Benzyl alcohol ug/kg 21304070 52 20-130<306
bis(2-Chloroethoxy)methane ug/kg 10902030 54 16-130<168
bis(2-Chloroethyl) ether ug/kg 10702030 53 18-130<152
bis(2-Ethylhexyl)phthalate ug/kg 11302030 56 11-130<157
Butylbenzylphthalate ug/kg 11502030 56 10-130<170
Chrysene ug/kg 12502030 61 17-130<147
Di-n-butylphthalate ug/kg 11502030 56 16-130<136
Di-n-octylphthalate ug/kg 10902030 54 16-130<159
Dibenz(a,h)anthracene ug/kg 13202030 65 13-130<155
Dibenzofuran ug/kg 12102030 60 19-130<146
Diethylphthalate ug/kg 11902030 59 22-130<148
Dimethylphthalate ug/kg 12402030 61 23-130<147
Fluoranthene ug/kg 12202030 60 14-130<138
Fluorene ug/kg 12402030 61 19-130<142
Hexachloro-1,3-butadiene ug/kg 12102030 60 12-130<175
Hexachlorobenzene ug/kg 12502030 62 17-130<158
Hexachlorocyclopentadiene ug/kg 10902030 54 10-130<231
Hexachloroethane ug/kg 11602030 57 14-130<154
Indeno(1,2,3-cd)pyrene ug/kg 13802030 68 13-130<159
Isophorone ug/kg 11102030 55 17-130<180
N-Nitroso-di-n-propylamine ug/kg 10802030 53 10-130<152
N-Nitrosodimethylamine ug/kg 11102030 55 16-130<136
N-Nitrosodiphenylamine ug/kg 12802030 63 19-130<143
Naphthalene ug/kg 12302030 61 18-130<137
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4020026MATRIX SPIKE SAMPLE:
MSSpike
Result
92667337001
Nitrobenzene ug/kg 11702030 58 15-130<187
Pentachlorophenol ug/kg 22304070 55 10-130<395
Phenanthrene ug/kg 12802030 63 17-130<132
Phenol ug/kg 12402030 61 15-130<180
Pyrene ug/kg 13002030 64 31-130<164
Pyridine ug/kg 325J2030 16 10-130<127
2,4,6-Tribromophenol (S) %68 10-131
2-Fluorobiphenyl (S) %60 10-130
2-Fluorophenol (S) %58 10-130
Nitrobenzene-d5 (S) %57 10-130
Phenol-d6 (S) %54 10-130
Terphenyl-d14 (S) %62 10-130
Parameter Units
Dup
Result QualifiersRPDResult
92667337002
4020027SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND<155
1,2-Dichlorobenzene ug/kg ND<142
1,3-Dichlorobenzene ug/kg ND<140
1,4-Dichlorobenzene ug/kg ND<150
1-Methylnaphthalene ug/kg ND<138
2,2'-Oxybis(1-chloropropane) ug/kg ND<187
2,4,5-Trichlorophenol ug/kg ND<180
2,4,6-Trichlorophenol ug/kg ND<162
2,4-Dichlorophenol ug/kg ND<154
2,4-Dimethylphenol ug/kg ND<163
2,4-Dinitrophenol ug/kg ND<1220
2,4-Dinitrotoluene ug/kg ND<152
2,6-Dinitrotoluene ug/kg ND<144
2-Chloronaphthalene ug/kg ND<156
2-Chlorophenol ug/kg ND<148
2-Methylnaphthalene ug/kg ND<157
2-Methylphenol(o-Cresol) ug/kg ND<161
2-Nitroaniline ug/kg ND<322
2-Nitrophenol ug/kg ND<171
3&4-Methylphenol(m&p Cresol) ug/kg ND<159
3,3'-Dichlorobenzidine ug/kg ND<266
3-Nitroaniline ug/kg ND<309
4,6-Dinitro-2-methylphenol ug/kg ND<367
4-Bromophenylphenyl ether ug/kg ND<152
4-Chloro-3-methylphenol ug/kg ND<277
4-Chloroaniline ug/kg ND<309
4-Chlorophenylphenyl ether ug/kg ND<147
4-Nitroaniline ug/kg ND<299
4-Nitrophenol ug/kg ND<761
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92667337002
4020027SAMPLE DUPLICATE:
Acenaphthene ug/kg ND<138
Acenaphthylene ug/kg ND<138
Aniline ug/kg ND<154
Anthracene ug/kg ND<129
Benzo(a)anthracene ug/kg ND<131
Benzo(a)pyrene ug/kg ND<136
Benzo(b)fluoranthene ug/kg ND<131
Benzo(g,h,i)perylene ug/kg ND<153
Benzo(k)fluoranthene ug/kg ND<138
Benzoic Acid ug/kg ND<846
Benzyl alcohol ug/kg ND<298
bis(2-Chloroethoxy)methane ug/kg ND<163
bis(2-Chloroethyl) ether ug/kg ND<148
bis(2-Ethylhexyl)phthalate ug/kg ND<153
Butylbenzylphthalate ug/kg ND<166
Chrysene ug/kg ND<143
Di-n-butylphthalate ug/kg ND<132
Di-n-octylphthalate ug/kg ND<155
Dibenz(a,h)anthracene ug/kg ND<152
Dibenzofuran ug/kg ND<142
Diethylphthalate ug/kg ND<144
Dimethylphthalate ug/kg ND<143
Fluoranthene ug/kg ND<135
Fluorene ug/kg ND<138
Hexachloro-1,3-butadiene ug/kg ND<171
Hexachlorobenzene ug/kg ND<154
Hexachlorocyclopentadiene ug/kg ND<226
Hexachloroethane ug/kg ND<150
Indeno(1,2,3-cd)pyrene ug/kg ND<155
Isophorone ug/kg ND<175
N-Nitroso-di-n-propylamine ug/kg ND<148
N-Nitrosodimethylamine ug/kg ND<132
N-Nitrosodiphenylamine ug/kg ND<140
Naphthalene ug/kg ND<134
Nitrobenzene ug/kg ND<183
Pentachlorophenol ug/kg ND<385
Phenanthrene ug/kg ND<129
Phenol ug/kg ND<175
Pyrene ug/kg ND<160
Pyridine ug/kg ND<124
2,4,6-Tribromophenol (S) %5662
2-Fluorobiphenyl (S) %5154
2-Fluorophenol (S) %4644
Nitrobenzene-d5 (S) %4850
Phenol-d6 (S) %4443
Terphenyl-d14 (S) %5258
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
774494
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92667253001, 92667253002, 92667253003, 92667253004
Parameter Units
Dup
Result QualifiersRPDResult
92667223002
4019477SAMPLE DUPLICATE:
Percent Moisture % 18.1 N2619.2
Parameter Units
Dup
Result QualifiersRPDResult
92667253004
4019478SAMPLE DUPLICATE:
Percent Moisture % 12.8 N2213.1
REPORT OF LABORATORY ANALYSIS
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Page 64 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
774506
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92667253005, 92667253006, 92667253007, 92667253008
Parameter Units
Dup
Result QualifiersRPDResult
92667113001
4019519SAMPLE DUPLICATE:
Percent Moisture % 14.1 N2513.4
Parameter Units
Dup
Result QualifiersRPDResult
92667323015
4019520SAMPLE DUPLICATE:
Percent Moisture % 17.9 N2418.6
REPORT OF LABORATORY ANALYSIS
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Page 65 of 70
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92667253
LOVES 412 23004903
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
N2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
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Page 66 of 70
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92667253
LOVES 412 23004903
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92667253001 774649 774925512234903-216 EPA 3546 EPA 8270E
92667253002 774649 774925512234903-217 EPA 3546 EPA 8270E
92667253003 774649 774925512234903-218 EPA 3546 EPA 8270E
92667253004 774649 774925512234903-219 EPA 3546 EPA 8270E
92667253005 774649 774925512234903-220 EPA 3546 EPA 8270E
92667253006 774649 774925512234903-221 EPA 3546 EPA 8270E
92667253007 774649 774925512234903-222 EPA 3546 EPA 8270E
92667253008 774649 774925512234903-223 EPA 3546 EPA 8270E
92667253001 775512 775592512234903-216 EPA 5035A/5030B EPA 8260D
92667253002 775512 775592512234903-217 EPA 5035A/5030B EPA 8260D
92667253003 776194 776223512234903-218 EPA 5035A/5030B EPA 8260D
92667253004 776194 776223512234903-219 EPA 5035A/5030B EPA 8260D
92667253005 775512 775592512234903-220 EPA 5035A/5030B EPA 8260D
92667253006 775512 775592512234903-221 EPA 5035A/5030B EPA 8260D
92667253007 774899 774930512234903-222 EPA 5035A/5030B EPA 8260D
92667253008 774899 774930512234903-223 EPA 5035A/5030B EPA 8260D
92667253001 774494512234903-216 SW-846
92667253002 774494512234903-217 SW-846
92667253003 774494512234903-218 SW-846
92667253004 774494512234903-219 SW-846
92667253005 774506512234903-220 SW-846
92667253006 774506512234903-221 SW-846
92667253007 774506512234903-222 SW-846
92667253008 774506512234903-223 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 09:16 AM
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Page 67 of 70
Page 68 of 70
Page 69 of 70
Page 70 of 70
#=CL#
June 07, 2023
LIMS USE: FR - MARK RYLAND
LIMS OBJECT ID: 92669792
92669792
Project:
Pace Project No.:
RE:
Mark Ryland
Apex Companies, LLC
203 Wylderose Court
Midlothian, VA 23113
LOVES 412 23004903
Dear Mark Ryland:
Enclosed are the analytical results for sample(s) received by the laboratory on May 30, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 14
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92669792
LOVES 412 23004903
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 14
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92669792
LOVES 412 23004903
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92669792001 STOCK PILE 2 524237903-227 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92669792002 STOCK PILE 1 524234903-225 EPA 8015C 2 PASI-CNND
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 3 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92669792
LOVES 412 23004903
Sample: STOCK PILE 2 524237903-
227
Lab ID: 92669792001 Collected: 05/24/23 16:25 Received: 05/30/23 09:18 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28) ND mg/kg 05/31/23 21:3505/31/23 13:506.2 1
Surrogates
n-Pentacosane (S) 60 %05/31/23 21:35 629-99-205/31/23 13:5010-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10) ND mg/kg 06/02/23 16:2706/02/23 12:0010.2 1
Surrogates
4-Bromofluorobenzene (S) 98 %06/02/23 16:27 460-00-406/02/23 12:0066-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.0 %05/31/23 15:26 N20.10 1
REPORT OF LABORATORY ANALYSIS
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Page 4 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92669792
LOVES 412 23004903
Sample: STOCK PILE 1 524234903-
225
Lab ID: 92669792002 Collected: 05/24/23 16:35 Received: 05/30/23 09:18 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)6.3 mg/kg 05/31/23 21:3505/31/23 13:506.0 1
Surrogates
n-Pentacosane (S) 58 %05/31/23 21:35 629-99-205/31/23 13:5010-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)22.4 mg/kg 06/01/23 23:4606/01/23 12:379.0 1
Surrogates
4-Bromofluorobenzene (S) 106 %06/01/23 23:46 460-00-406/01/23 12:3766-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.2 %05/31/23 15:26 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 12:03 PM
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Page 5 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92669792
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
778065
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92669792002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4036157
Associated Lab Samples:92669792002
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 06/01/23 16:45
4-Bromofluorobenzene (S) % 90 66-130 06/01/23 16:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4036158LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10) mg/kg 46.449.9 93 70-130
4-Bromofluorobenzene (S) %92 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4036160MATRIX SPIKE SAMPLE:
MSSpike
Result
92669409004
Gas Range Organics (C6-C10) mg/kg 54.060.1 88 57-154ND
4-Bromofluorobenzene (S) %97 66-130
Parameter Units
Dup
Result QualifiersRPDResult
92669409003
4036159SAMPLE DUPLICATE:
Gas Range Organics (C6-C10) mg/kg 99.3 2775.7
4-Bromofluorobenzene (S) %158 S2132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 12:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92669792
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
778343
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92669792001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4037500
Associated Lab Samples:92669792001
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10) mg/kg ND 5.9 06/02/23 14:07
4-Bromofluorobenzene (S) % 95 66-130 06/02/23 14:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4037501LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10) mg/kg 41.749.5 84 70-130
4-Bromofluorobenzene (S) %93 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4037503MATRIX SPIKE SAMPLE:
MSSpike
Result
92669530001
Gas Range Organics (C6-C10) mg/kg 50.156.3 88 57-154ND
4-Bromofluorobenzene (S) %94 66-130
Parameter Units
Dup
Result QualifiersRPDResult
92669409005
4037502SAMPLE DUPLICATE:
Gas Range Organics (C6-C10) mg/kg NDND
4-Bromofluorobenzene (S) %9391
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 12:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92669792
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
777750
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92669792001, 92669792002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4034749
Associated Lab Samples:92669792001, 92669792002
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 5.0 05/31/23 20:10
n-Pentacosane (S) % 67 10-133 05/31/23 20:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4034750LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28) mg/kg 50.166 76 43-130
n-Pentacosane (S) %65 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4034751MATRIX SPIKE SAMPLE:
MSSpike
Result
92669840002
Diesel Range Organics(C10-C28) mg/kg 10900 M186.9 3790 15-1307590
n-Pentacosane (S) %S5221 10-133
Parameter Units
Dup
Result QualifiersRPDResult
92669840003
4034752SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28) mg/kg 899 7964
n-Pentacosane (S) %111163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 12:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92669792
LOVES 412 23004903
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
777801
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92669792001, 92669792002
Parameter Units
Dup
Result QualifiersRPDResult
92669764001
4035075SAMPLE DUPLICATE:
Percent Moisture % 12.9 N2412.4
Parameter Units
Dup
Result QualifiersRPDResult
92669648005
4035076SAMPLE DUPLICATE:
Percent Moisture % 20.3 N2521.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 12:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 14
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92669792
LOVES 412 23004903
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).
S2
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 12:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 14
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92669792
LOVES 412 23004903
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92669792001 777750 777982STOCK PILE 2 524237903-227 EPA 3546 EPA 8015C
92669792002 777750 777982STOCK PILE 1 524234903-225 EPA 3546 EPA 8015C
92669792001 778343 778359STOCK PILE 2 524237903-227 EPA 5030B EPA 8015C
92669792002 778065 778126STOCK PILE 1 524234903-225 EPA 5030B EPA 8015C
92669792001 777801STOCK PILE 2 524237903-227 SW-846
92669792002 777801STOCK PILE 1 524234903-225 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2023 12:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 14
Page 12 of 14
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Page 14 of 14
APPENDIX F
Non-Hazardous Soil Waste Manifests
S25-1
S25-2
S25-3
S25-4
S25-5
S25-6
S25-7
S25-8
S25-9
S25-10
S26-1
S26-2
S26-3
S26-4
S26-5
S26-6
S26-7
S26-8