FA-1015_19070_CA_MRP_20220207_FRP

February 7, 2022 Mr. James Brown North Carolina Department of Environmental Quality Division of Waste Management, UST Section
225 Green Street, Suite 714 Fayetteville, North Carolina 28301 Subject: FREE PRODUCT RECOVERY AND GROUNDWATER MONITORING REPORT
FOOD LION DISTRIBUTION CENTER #4 INCIDENT 19070 2940 ARROWHEAD ROAD DUNN, NORTH CAROLINA Dear Mr. Brown: Wood Environment & Infrastructure Solutions, Inc. (Wood) is pleased to submit the attached Free product Recovery and Groundwater Monitoring Report for the Food Lion Distribution Center #4 located in Dunn, North Carolina. The report provides the results of three quarterly groundwater gauging and free product recovery events as well as a comprehensive groundwater sampling event performed in 2021. Based on the presence and volume of free product encountered in 2021, in conjunction with quarterly gauging, Wood recommends performing mobile multi-phase extraction (MMPE) or similar, as suggested by NCDEQ, at select recovery wells in 2022. If you have any questions concerning this report, please contact Anthony Kellogg at [phone] or [e-mail]. Sincerely, Wood Environment & Infrastructure Solutions, Inc. Anthony Kellogg Senior 1 Project Manager cc: Danny Matthews – Delhaize America Attachment: Free Product Recovery and Groundwater Monitoring Report
Page i
TABLE OF CONTENTS
1.0 INTRODUCTION ...................................................................................................................................1
2.0 SITE BACKGROUND ..............................................................................................................................1
3.0 RECEPTOR SURVEYS .............................................................................................................................2
4.0 FIELD METHODOLOGY ..........................................................................................................................3
4.1 GROUNDWATER AND FREE PRODUCT GAUGING .................................................................................................... 3
4.2 FREE PRODUCT RECOVERY ................................................................................................................................. 3
4.3 GROUNDWATER SAMPLING ................................................................................................................................ 3
5.0 RESULTS ..............................................................................................................................................4
5.1 GAUGING AND FREE PRODUCT RECOVERY RESULTS ................................................................................................ 4
5.2 GROUNDWATER ANALYTICAL RESULTS ................................................................................................................. 5
6.0 CONCLUSIONS AND RECOMMENDATIONS ............................................................................................6
FIGURES Figure 1 Site Location Map Figure 2 Site Layout and Well Location Map Figure 3 Potential Water Supply Well Location Map Figure 4 Groundwater Flow Map – March 17, 2021 Figure 5 Groundwater Exceedances Tag Map – March 17, 2021
TABLES Table 1 Summary of Monitoring and Remediation Well Construction Information Table 2 Water Supply Wells and Other Receptors Table 3 Summary of Groundwater Elevations and Free Product Thicknesses Table 4 Cumulative Volume of Free Product Recovered from Site Table 5 Summary of Groundwater Analytical Results Table 6 Summary of Groundwater Field Parameters
APPENDICIES Appendix A Groundwater Sampling Logs Appendix B Waste Disposal Documentation Appendix C Laboratory Analytical Reports
Page 1
Free Product Recovery and Groundwater Monitoring Report
Food Lion Distribution Center #4 Dunn, North Carolina
February 2022
1.0 INTRODUCTION Wood Environment & Infrastructure Solutions, Inc. (Wood) has prepared this Free Product Recovery and Groundwater Monitoring Report for the Food Lion Distribution Center #4 facility located at 2940 Arrowhead Road, near Highway 301 in Dunn, Harnett County, North Carolina (Site; Figure 1). The Site is owned by Delhaize America, the parent company of Food Lion, Inc. (Food Lion), and is utilized as a product distribution center for Food Lion. The Site currently consists of a distribution center/warehouse, truck maintenance facility, refueling station for trucks supplied by above ground storage tanks (ASTs), and parking lots. Historically, diesel fuel was stored in two former 25,000-gallon underground storage tanks (USTs). The Site is located in a rural area consisting of properties used for both residential and commercial purposes. Site features are illustrated in Figure 2.
2.0 SITE BACKGROUND Several assessments have been performed at the Site to identify the extent of soil and groundwater impacts resulting from releases associated with two former 25,000-gal diesel USTs and associated product piping. During initial assessment and abatement activities, free product was observed, and four recovery wells were installed in May 1998 to facilitate free product recovery. Well locations are shown in Figure 2. Well Construction information is provided in Table 1.
The Site is classified as intermediate risk based on the presence of free product. In September 1998, the two 25,000-gal USTs were removed and replaced with ASTs. Following the removal of the USTs, a Limited Site Assessment (LSA) Report was prepared in February 1999 and a Corrective Action Plan (CAP) was prepared in June 2000. The proposed corrective action included free product removal followed by monitored natural attenuation (MNA) for the impacted groundwater beneath the Site.
Following submittal of the CAP, a free product recovery system using pneumatic pumps was installed. Records regarding the length of time the system operated or how much product was removed are not available. The location of the former system is illustrated on Figure 2. Four aggressive fluid vapor recovery (AFVR) events were performed in the summer of 1998 which removed 1,699 gallons of free product from the recovery wells.
On July 8, 2010, the North Carolina Department of Environmental Quality (NCDEQ), UST Section issued a Notice of Regulatory Requirement (NORR) requiring a Free Product Evaluation. In August 2010, the free product recovery system was restarted, but was later deactivated because operation became impractical. In August 2012, Amec Foster Wheeler was retained by Delhaize America to prepare a free product recovery plan and conduct free product recovery in accordance with a May 31, 2011 NORR issued by NCDENR. Amec Foster Wheeler used Laser Induced Fluorescence/Ultraviolet Optical Screening Tool (LIF/UVOST) technology to assess the free product at the Site. The LIF/UVOST assessment was performed in December 2012, and a Free Product Recovery System Specification Report (System Specification Report) was submitted to the UST Section on April 5, 2013. The Report recommended the installation of five supplementary recovery wells and product recovery using AFVR. The additional recovery wells were installed in July 2013, followed by AFVR events in September 2013, January 2014, April 2014, and July 2014. Approximately 692 gallons of free product were recovered during these four AFVR events. Four additional AFVR events, performed at six recovery wells (RW-2, RW-3, RW-4, RW-6, RW-8, and RW-9), were conducted in November 2014, February 2015, July 2015, and February 2016.
Free Product Recovery and Groundwater Monitoring Report
Food Lion Distribution Center #4 Dunn, North Carolina
February 2022
Page 2
Approximately 100 gallons of free product were recovered as a result of the additional AFVR events; however, only 9-gallons of free product were recovered over the course of the final two events combined (July 2015 and February 2016).
Based on the decreased volumes of free product recovered during the July 2015 and February 2016 AFVR events, the March 11, 2016 Free Product Recovery Report recommended changing the free product recovery method for the Site to passive collection via oil-absorbent socks suspended in the recovery wells. The UST Section agreed with the recommendation to replace AFVR with oil-absorbent socks as the primary method for free product recovery. As such, following completion of the February 2016 AFVR event, absorbent socks were deployed within the recovery wells for the passive removal of free product. Between 2016 and 2019, a total of approximately 2.85 gallons of free product was recovered via absorbent socks. No Site work was performed in 2018 or 2020.
On August 14, 2020, the NCDEQ issued a NORR recommending the completion of a comprehensive groundwater sampling event and the continuation of quarterly free product recovery via absorbent sock deployment/maintenance, as necessary. Results of the 2021 comprehensive groundwater sampling and free product recovery is discussed in Sections 4.0 and 5.0.
Additionally, in January 2021, an estimated 700-gallons of diesel fuel was released as a result of a piping failure at one of the two existing 20,000-gallon above ground storage tanks (AST). Fuel was discharged to the ground surface surrounding the ASTs and asphalt pavement, flowing topographically downgradient towards the on-Site drainage ditch to the south of the ASTs. The release was reported to the NCDEQ and incident #95947 was assigned. An Initial Assessment Report, dated February 3, 2020, detailing assessment and abatement activities, was prepared and submitted to the NCDEQ by Highlands Environmental Solutions, Inc. (Highlands) on behalf of AUDUSA Distribution, LLC (i.e., Food Lion). Mitigation activities, consisting of soil excavation and free product recovery via absorbents, were performed in conjunction with the assessment. A total of 337.45 tons of petroleum impacted soil was excavated and disposed of off-Site as result of abatement activities. Confirmation soil sampling was performed within the excavation area, indicating soil cleanup to less than applicable total petroleum hydrocarbon (TPH) action levels. A no further action (NFA) letter was issued from the NCDEQ on February 12, 2021 and the incident was closed.
3.0 RECEPTOR SURVEYS A receptor survey conducted in 1998 identified five water-supply wells within 1,500 feet of the Site, located hydraulically upgradient and or cross-gradient of the source area, and indicated municipal water was available to those properties. The receptor survey was updated in 2019 to reassess off-Site receptor risks considering the potential for Incident closure following the completion of free product removal/recovery at the Site. During the update, three potential water supply wells were identified within 1,500 feet upgradient of the Site. The potential wells are illustrated on Figure 3 and owner information is summarized in Table 2. Municipal water was confirmed to be provided to the area.
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Free Product Recovery and Groundwater Monitoring Report
Food Lion Distribution Center #4 Dunn, North Carolina
February 2022
4.0 FIELD METHODOLOGY 4.1 Groundwater and Free Product Gauging During each quarterly event, groundwater levels and free product thicknesses, if present, were measured at each well using a water level meter and/or oil-water interface probe. An attempt was made to measure free product thickness and depth to water in each recovery well prior to removing the sock, if socks were present. If the sock prevented access by the interface probe, these measurements were collected once the sock was removed and levels in the well were allowed to equilibrate. Depth to groundwater and free phase product were measured relative to the top of casing elevation (TOC). Based on the groundwater elevations (corrected groundwater elevations if free phase product was present), groundwater flow at the Site was determined to be predominately towards the west. Depth to water and groundwater elevations obtained during the March 17, 2021 gauging event are summarized in Table 1. Historical groundwater gauging data, including each of the three events performed in 2021, is presented in Table 3.A shallow groundwater potentiometric map is presented on Figure 4.
4.2 Free Product Recovery Free product recovery was performed by hanging oil-absorbent socks within recovery wells exhibiting the presence of free product. The socks were suspended across the water table in order to absorb free product floating on the surface. Each sock measured 3 inches in diameter and 48 inches in length and was rated to absorb up to 0.75-gallons of oil. Following the completion of 2019 free product recovery, absorbent socks were left in recovery wells RW-2 and RW-8. As such, during the first quarterly gauging event (March 2021), recovery wells RW-2 and RW-8 initially contained absorbent socks. During each 2021 quarterly event, absorbent socks were deployed as needed based on the presence of free product. Sock deployment for each quarterly was as follows:
•Q1: March 2021 - Replaced socks in RW-2 and RW-8 and installed a sock in RW-7.
•Q2: June 2021 – Eliminated the sock in RW-2, replaced socks in RW-7 and RW-8, and installed asock in RW-6.
•Q3: August 2021 – Eliminated the sock in RW-6 and replaced the socks in RW-7 and RW-8.
•Q4: Quarterly Event Not Performed
Additionally, due to the thickness of free product measured in recovery wells RW-7 and RW-8, free product was also pumped from these wells during the second and third quarterly event via a peristaltic pump. All free phase product recovered, including the absorbent socks, were placed in a 55-gallon steel drum and staged on-Site prior to off-site disposal. The cumulative volume of free product recovered from the Site is summarized in Table 4.
Based on product thicknesses observed in recovery wells RW-7 and RW-8 during the first three quarterly events in 2021, the NCDEQ Trust Fund opted to eliminate the 4th quarter sock deployment and requested a more aggressive remedial approach be utilized, resuming in 2022, to recover the free product.
4.3 Groundwater Sampling On March 17, 2021, Wood completed a comprehensive groundwater sampling event to evaluate current Site groundwater conditions. During the sampling event, three monitoring wells (MW-1, MW-2, and MW-3) and six recovery wells (RW-1, RW-3, RW-4, RW-5, RW-6, and RW-9) were purged and sampled
Free Product Recovery and Groundwater Monitoring Report
Food Lion Distribution Center #4 Dunn, North Carolina
February 2022
Page 4
utilizing low-flow methodology. An obstruction was encountered in monitoring well MW-4 and free phase product was observed in recovery wells RW-2, RW-7, and RW-8; therefore, those wells were not sampled. Each well was purged and sampled utilizing a peristaltic pump and new disposable tubing. During purging, groundwater geochemical parameters, including temperature, conductivity, dissolved oxygen (DO), pH, turbidity (NTU), and oxidation/reduction potential (ORP), were monitored for stabilization utilizing a multi-parameter water quality meter prior to sampling.
After well stabilization, the flow through cell was disconnected and groundwater samples were collected by filling the laboratory-supplied bottle ware directly from the pump discharge tubing. Groundwater samples were collected and analyzed for the following parameters:
•Volatile Organic Compounds (VOCs) by Standard Method (SM) 6200B;
•Volatile Petroleum Hydrocarbons (VPH) by Massachusetts Department of EnvironmentalProtection (MADEP) VPH method.
•Extractable Petroleum Hydrocarbons (EPH) by Massachusetts Department of EnvironmentalProtection (MADEP) EPH method; and
•Semi-Volatile Organic Compounds (SVOCs) by Standard Method (SM) 625
Once collected, the samples were immediately placed on ice until delivery to Con-Test Analytical Laboratory of East Longmeadow, Massachusetts. Chain of custody documentation was completed for groundwater samples collected at the Site and accompanied the samples to the laboratory. Groundwater monitoring data sheets generated during this sampling event are included in Appendix A.
Groundwater sampling equipment, including the water level meter, oil-water interface probe, and pump, were properly decontaminated prior to use at each monitoring well. In accordance with the Guidelines, purge water generated during well purging and sampling was discharged directly to the ground surface.
5.0 RESULTS 5.1 Gauging and Free Product Recovery Results Free product was measured in select recovery wells during each of the gauging events. Results of the gauging and free product recovery were as follows:
•Q1: March 2021 - Free product observed in RW-2 (0.01’) RW-7 (4.53’) and RW-8 (5.37’). Anegligible amount of free product was recovered. No pumping was performed during this event.
•Q2: June 2021 – Free product observed in RW-6 (0.10’) RW-7 (3.35) and RW-8 (4.17). A total of14-gallons of free product was recovered via absorbent socks and low flow pumping.
•Q3: August 2021 – Free product observed in RW-7 (3.49) and RW-8 (5.16). A total of 15-gallonsof free product was recovered via absorbent socks and low flow pumping.
•Q4: Not Performed per NCDEQ.
Historically, free phase product had not been measured in recovery well RW-7. Additionally, free phase product hadn’t been measured in recovery well RW-8 since early 2016. One 55-gallon drum, consisting of used absorbent socks and recovered product, was transported and disposed of off-Site by Contaminant Control, Inc. (CCI), of Salisbury, North Carolina. Gauging data is summarized in Table 3
Free Product Recovery and Groundwater Monitoring Report
Food Lion Distribution Center #4 Dunn, North Carolina
February 2022
Page 5
and cumulative free product recovery is summarized in Table 4. Waste documentation is provided in Appendix B.
5.2 Groundwater Analytical Results Laboratory analytical results from the nine groundwater samples collected indicate that petroleum hydrocarbon concentrations exceed their respective 2L Standards in samples from recovery wells RW-1, RW-3, RW-4, RW-5, RW-6, and RW-9. Petroleum constituents were not identified in excess of the 2L Standard in samples collected from monitoring wells MW-1, MW-2, or MW-3.
VPH exceedances of the 2L Standards were identified for:
•Aliphatics C9-C18 [2L Standard 700 micrograms per liter (ug/L)] in wells RW-4 (1,030 ug/L) andRW-6 (740 ug/L).
•Aromatics C9-C22 (C9-C10) (2L Standard 200 ug/L) in RW-1 (250 ug/L), RW-3 (1,040 ug/L), RW-4 (1,680 ug/L), RW-5 (420 ug/L), RW-6 (1,090 ug/L), and RW-9 (420 ug/L).
VOC exceedances of the 2L Standards were identified for:
•Benzene (2L Standard 1 µg/L) in recovery wells RW-3 (3.6 ug/L), RW-4 (10 ug/L), RW-5 (5.4 ug/L),and RW-6 (6.1 ug/L).
SVOC exceedances of the 2L Standards were identified for:
•Naphthalene (2L Standard 6 µg/L) in recovery wells RW-3 (13.6 ug/L), RW-4 (39.8 ug/L), RW-5(8.73 ug/L), and RW-6 (21.3 ug/L).
•2-Methylnaphthalene (2L Standard 30 µg/L) in recovery wells RW-4 (45.3 ug/L) and RW-6 (37.6ug/L).
Groundwater impacts were not identified at concentrations exceeding their respective Gross Contaminant Levels (GCLs). Laboratory groundwater analytical results are summarized in Table 5. Groundwater contaminant concentrations are depicted on Figure 5. Laboratory analytical reports are included in Appendix C.
Based on groundwater geochemistry data collected during sampling, with the exception of recovery well RW-3, ORP is generally positive suggesting an aerobic environment. Typically, ORP readings will be lower (i.e., approaching negative readings) in areas of higher concentrations and dissolved oxygen concentrations will be low as oxygen is utilized; and the area becomes more anaerobic. However, since DO could not be accurately measured at the site due to an instrument malfunction, trends in DO concentrations as related to ORP are not clear. Groundwater trends will be evaluated once sufficient data is obtained. Groundwater geochemistry results are summarized in Table 6.
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Free Product Recovery and Groundwater Monitoring Report
Food Lion Distribution Center #4 Dunn, North Carolina
February 2022
6.0 CONCLUSIONS AND RECOMMENDATIONS Based on the information gathered during the 2021 comprehensive groundwater sampling and quarterly gauging events, Wood understands the following:
•As reported by Highlands, a surface release from the existing on-Site diesel ASTs occurred inJanuary 2020 (incident #95947), which released an estimated 700-gallons of diesel fuel to theground and asphalt surrounding the AST. The soil was remediated in accordance with NCDEQguidelines, and an NFA was issued for the incident in February 2020.
•Based on the gauging results/free product thicknesses measured in recovery wells RW-7 andRW-8 during the first three quarters of 2021, the NCDEQ eliminated the fourth quarter sockdeployment and recommended pursing a more aggressive remedial strategy [i.e., mobile multi-phase extraction (MMPE)] to address the volume of free phase product observed, beginning in2022.
With this understanding, Wood concludes the following:
•Groundwater gauging indicated free phase product in four wells (RW-2, RW-6, RW-7 and/orRW-8) at thicknesses ranging between 0.01’ (RW-2) and 5.37’ (RW-8). Historical gauging datadoes not indicate product had previously been measured in recovery well RW-7 and indicatesproduct hasn’t been observed in RW-8 since 2016. The cause of the product in recovery wellsRW-7 and RW-8 is unclear; however, recovery wells RW-7 and RW-8 are located east of theASTs and immediately adjacent to the product distribution lines that supply the fuel dispensers.
•Approximately 29-gallons of free product was recovered via absorbent socks and low flowpumping during 2021 remedial efforts at the Site.
•Groundwater elevation data indicated groundwater flow predominately to the west.
•VPH carbon ranges and petroleum-related VOCs are the primary dissolved phase contaminantsof concern and concentrations exceed the 2L Standards in samples from six recovery wells(RW-1, RW-3, RW-4, RW-5, RW-6, RW-9). Samples were not collected form RW-2, RW-7, orRW-8 due to the presence of free phase product at the time of sampling.
•Groundwater contaminants indicative of petroleum hydrocarbons were not detected or werenot present above the 2L Standards in upgradient monitoring well MW-3, or downgradientmonitoring wells MW-1 and MW-2.
•An obstruction was identified in deep monitoring well MW-4 which prevented sampling.
•Groundwater impacts were not identified at concentrations exceeding the GCLs.
Based on the results of the 2021 gauging, the NCDEQ requested implementing a more aggressive approach in 2022. As such, Wood recommends performing MMPE or similar, as suggested by NCDEQ, at recovery wells RW-7 and RW-8 for remediating free phase product measured in 2021. Additionally, Wood recommends continuing absorbent sock deployment at wells exhibiting de minimis amounts (i.e., less than 0.2’) of free phase product.
TABLES
Table 1
Summary of Monitoring Well and Remediation Well Construction Information
Food Lion Distribution Center #4
Dunn, North Carolina
Location
Northing
Location
Easting
Top of Casing
Elevation
(feet NAVD 88)
MW-1 11/16/98 555,522.75 2,110,041.08 170.22 2 15 5-15 15 03/17/21 - - - 3.76 - - - No 166.46
MW-2 11/16/98 555,306.26 2,110,091.14 172.88 2 15 5-15 15 03/17/21 - - - 6.24 - - - No 166.64
MW-3 11/16/98 555,570.96 2,110,496.71 172.72 2 15 5-15 15 03/17/21 - - - 1.40 - - - No 171.32
MW-4 11/17/98 555,475.34 2,110,282.35 173.80 2 50 40-50 50 03/17/21 - - - 0.00* - - - No 173.80
RW-1 05/05/98 555,514.18 2,110,151.53 172.28 4 13.5 3.5-13.5 13.5 03/17/21 - - - 5.40 - - -No 166.88
RW-2 05/05/98 555,471.42 2,110,281.62 173.53 4 14.5 4.5-14.5 14.5 03/17/21 5.21 5.22 0.01 Yes 168.32
RW-3 05/05/98 555,473.39 2,110,346.48 173.44 4 14.5 4.5-14.5 14.5 03/17/21 - - - 4.14 - - -No 169.30
RW-4 05/05/98 555,485.91 2,110,222.20 173.14 4 14 4-14 14 03/17/21 - - - 5.37 - - - No 167.77
RW-5 07/09/13 555,467.02 2,110,177.66 173.06 4 13 3-13 13 03/17/21 - - - 5.84 - - - No 167.22
RW-6 07/09/13 555,449.25 2,110,220.85 173.64 4 18 3-18 18 03/17/21 - - - 5.89 - - - No 167.75
RW-7 07/09/13 555,521.35 2,110,263.81 173.52 4 18 3-18 18 03/17/21 4.76 9.29 4.53 Yes 168.12
RW-8 07/09/13 555,505.03 2,110,307.87 173.71 4 14 4-14 14 03/17/21 4.35 9.72 5.37 Yes 168.60
RW-9 07/09/13 555,540.31 2,110,319.95 173.38 4 14.5 4-14.5 14.5 03/17/21 - - - 4.79 - - -No 168.59
Notes:
bgs = below ground surface, btoc = below top of casing * = Obstruction observed in well at time of gauging.
ft NAVD 88 = Feet according to the North American Vertical Datum of 1988 ** = Based on direct measurment or presence of free product on absorbent sock.
- - - = Free product not measured *** = elevations were corrected for the presence of free product:
Survey data from KCI survey of 7/26/2013, based on NC State Plane NAD '83 and NAVD '88
Corrected Groundwater Surface Elevation = [Top of Casing elevation – Depth to water table] + [free-product thickness * 0.8581 (specific gravity of diesel)]
Completed By: DB Date: 3/30/2021 Reviewed By: AK Date: 4/13/2021
RECOVERY WELLS
Corrected Groundwater
Surface Elevation***
(feet NAVD 88)
MONITORING WELLS
Well ID
Date
Installed
Survey Data Well
Casing
Diameter
(inches)
Well
Casing
Depth
(feet bgs)
Screened
Interval
(feet bgs)
Depth
of Well
(feet bgs)
Date Water
Level
Measured
Depth to
Product
(feet btoc)
Depth to
Water
(feet btoc)
Absorbent
Sock Present
in Well **
(Yes/No)
Apparent
Product
Thickness
(feet)
Table 2
Water Supply Wells and Other Receptors
Food Lion Distribution Center #4
Dunn, North Carolina
Property Owner Well Use Well Depth
(feet bgs)
Type of
Well
Distance from
source area
(feet)
Up or down
gradient
E C Edgerton JR LLC Unknown Unknown Unknown 1,000 Up
Dwarka and Arani Ramphal Unknown Unknown Unknown 1,300 Up
Jerry and Shirly Ammons Unknown Unknown Unknown 1,200 Up
Municipal water is available to listed properties.
Potential Public and Private Water Supply Wells
Property Address
93 Long Branch Rd., Dunn, NC 2833
1445 Ammons Rd., Dunn, NC 2833
1473 Ammons Rd., Dunn, NC 2833
Page 2 of 12
Table 3
Summary of Groundwater Elevations and Free Product Thicknesses 
Food Lion Distribution Center #4
Dunn, North Carolina
Well ID
Date
Measured
Screened
Interval
(feet bgs)
Top of Casing
Elevation*
(feet AMSL)
Depth to
Water (feet
btc)
Depth to Free
Product (feet
btc)
Free Product
Thickness
(feet)

Water
Corrected for
Free Product
Thickness**
(feet btc)
Groundwater
Surface
Elevation***
(feet AMSL)
MW-1 11/17/98 5-15 170.22 5.58 NA 0 5.58 164.64
MW-1 10/19/10 5-15 170.22 4.08 NA 0 4.08 166.14
MW-1 09/09/13 5-15 170.22 4.02 NA 0 4.02 166.20
MW-1 01/15/14 5-15 170.22 3.74 NA 0 3.74 166.48
MW-1 07/28/14 5-15 170.22 3.90 NA 0 3.90 166.32
MW-1 04/23/14 5-15 170.22 4.18 NA 0 4.18 166.04
MW-1 11/25/14 5-15 170.22 4.21 NA 0 4.21 166.01
MW-1 02/25/15 5-15 170.22 3.99 NA 0 3.99 166.23
MW-1 07/21/15 5-15 170.22 4.30 NA 0 4.30 165.92
MW-1 02/04/16 5-15 170.22 3.68 NA 0 3.68 166.54
MW-1 04/29/16 5-15 170.22 4.01 NA 0 4.01 166.21
MW-1 08/09/16 5-15 170.22 4.18 NA 0 4.18 166.04
MW-1 10/21/16 5-15 170.22 3.93 NA 0 3.93 166.29
MW-1 03/03/17 5-15 170.22 4.20 NA 0 4.20 166.02
MW-1 05/17/17 5-15 170.22 3.98 NA 0 3.98 166.24
MW-1 08/22/17 5-15 170.22 4.27 NA 0 4.27 165.95
MW-1 11/21/17 5-15 170.22 4.32 NA 0 4.32 165.90
MW-1 02/07/19 5-15 170.22 3.77 NA 0 3.77 166.45
MW-1 05/21/19 5-15 170.22 3.96 NA 0 3.96 166.26
MW-1 09/23/19 5-15 170.22 4.09 NA 0 4.09 166.13
MW-1 12/20/19 5-15 170.22 3.79 NA 0 3.79 166.43
MW-1 03/17/21 5-15 170.22 3.76 NA 0 3.76 166.46
MW-1 05/27/21 5-15 170.22 3.97 NA 0 3.97 166.25
MW-1 08/05/21 5-15 170.22 3.79 NA 0 3.79 166.43
MW-2 11/17/98 5-15 172.88 7.73 NA 0 7.73 165.15
MW-2 10/19/10 5-15 172.88 6.76 NA 0 6.76 166.12
MW-2 12/07/12 5-15 172.88 8.35 NA 0 8.35 164.53
MW-2 09/09/13 5-15 172.88 6.76 NA 0 6.76 166.12
MW-2 01/15/14 5-15 172.88 6.19 NA 0 6.19 166.69
MW-2 04/23/14 5-15 172.88 5.93 NA 0 5.93 166.95
MW-2 07/28/14 5-15 172.88 6.05 NA 0 6.05 166.83
MW-2 11/25/14 5-15 172.88 6.14 NA 0 6.14 166.74
MW-2 02/25/15 5-15 172.88 6.42 NA 0 6.42 166.46
MW-2 07/21/15 5-15 172.88 7.18 NA 0 7.18 165.70
MW-2 02/04/16 5-15 172.88 5.87 NA 0 5.87 167.01
MW-2 04/29/16 5-15 172.88 6.42 NA 0 6.42 166.46
MW-2 08/09/16 5-15 172.88 6.99 NA 0 6.99 165.89
MW-2 10/21/16 5-15 172.88 6.24 NA 0 6.24 166.64
MW-2 03/03/17 5-15 172.88 6.96 NA 0 6.96 165.92
MW-2 05/17/17 5-15 172.88 6.75 NA 0 6.75 166.13
MW-2 11/21/17 5-15 172.88 NS NA 0 NA NA
MW-2 08/22/17 5-15 172.88 7.78 NA 0 7.78 165.10
MW-2 11/21/17 5-15 172.88 NS NA 0 NA NA
MW-2 02/07/19 5-15 172.88 6.30 NA 0 NA NA
MW-2 05/21/19 5-15 172.88 7.01 NA 0 NA NA
MW-2 09/23/19 5-15 172.88 7.38 NA 0 NA NA
MW-2 12/20/19 5-15 172.88 6.43 NA 0 6.43 166.45
MW-2 03/17/21 5-15 172.88 6.24 NA 0 6.24 166.64
MW-2 05/27/21 5-15 172.88 7.58 NA 0 7.58 165.30
MW-2 08/05/21 5-15 172.88 6.39 NA 0 6.39 166.49
Table 3
Summary of Groundwater Elevations and Free Product Thicknesses 
Food Lion Distribution Center #4
Dunn, North Carolina
Well ID
Date
Measured
Screened
Interval
(feet bgs)
Top of Casing
Elevation*
(feet AMSL)
Depth to
Water (feet
btc)
Depth to Free
Product (feet
btc)
Free Product
Thickness
(feet)

Water
Corrected for
Free Product
Thickness**
(feet btc)
Groundwater
Surface
Elevation***
(feet AMSL)
MW-3 11/18/98 5-15 172.72 NA 0 0.00 172.72
MW-3 10/19/10 5-15 172.72 4.00 NA 0 4.00 168.72
MW-3 12/07/12 5-15 172.72 7.16 NA 0 7.16 165.56
MW-3 09/09/13 5-15 172.72 3.63 NA 0 3.63 169.09
MW-3 01/15/14 5-15 172.72 1.13 NA 0 1.13 171.59
MW-3 04/23/14 5-15 172.72 1.63 NA 0 1.63 171.09
MW-3 07/28/14 5-15 172.72 4.13 NA 0 4.13 168.59
MW-3 11/25/14 5-15 172.72 4.18 NA 0 4.18 168.54
MW-3 02/25/15 5-15 172.72 2.44 NA 0 2.44 170.28
MW-3 07/21/15 5-15 172.72 4.68 NA 0 4.68 168.04
MW-3 02/04/16 5-15 172.72 1.34 NA 0 1.34 171.38
MW-3 04/29/16 5-15 172.72 2.94 NA 0 2.94 169.78
MW-3 08/09/16 5-15 172.72 4.78 NA 0 4.78 167.94
MW-3 10/21/16 5-15 172.72 2.19 NA 0 2.19 170.53
MW-3 03/03/17 5-15 172.72 4.28 NA 0 4.28 168.44
MW-3 05/17/17 5-15 172.72 3.05 NA 0 3.05 169.67
MW-3 08/22/17 5-15 172.72 5.92 NA 0 5.92 166.80
MW-3 11/21/17 5-15 172.72 5.71 NA 0 5.71 167.01
MW-3 02/07/19 5-15 172.72 2.50 NA 0 2.50 170.22
MW-3 05/21/19 5-15 172.72 3.96 NA 0 3.96 168.76
MW-3 09/23/19 5-15 172.72 5.25 NA 0 5.25 167.47
MW-3 12/20/19 5-15 172.72 1.40 NA 0 1.40 171.32
MW-3 03/17/21 5-15 172.72 1.40 NA 0 1.40 171.32
MW-3 05/27/21 5-15 172.72 3.42 NA 0 3.42 169.30
MW-3 08/05/21 5-15 172.72 2.11 NA 0 2.11 170.61
MW-4 11/19/98 45-50 173.80 28.91 NA 0 28.91 144.89
MW-4 10/19/10 45-50 173.80 10.81 NA 0 10.81 162.99
MW-4 09/09/13 45-50 173.80 11.97 NA 0 11.97 161.83
MW-4 01/15/14 45-50 173.80 NM NM NM NA NA
MW-4 04/23/14 45-50 173.80 NM NM NM NA NA
MW-4 07/28/14 45-50 173.80 NM NM NM NA NA
MW-4 11/25/14 45-50 173.80 NM NM NM NA NA
MW-4 02/25/15 45-50 173.80 NM NM NM NA NA
MW-4 07/21/15 45-50 173.80 0.21 NA 0 0.21 173.59
MW-4 02/04/16 45-50 173.80 0.35 NA 0 0.35 173.45
MW-4 04/29/16 45-50 173.80 1.34 NA 0 1.34 172.46
MW-4 08/09/16 45-50 173.80 4.29 NA 0 4.29 169.51
MW-4 10/21/16 45-50 173.80 5.51 NA 0 5.51 168.29
MW-4 03/03/17 45-50 173.80 7.30 NA 0 7.30 166.50
MW-4 05/17/17 45-50 173.80 13.45 NA 0 13.45 160.35
MW-4 08/22/17 45-50 173.80 10.20 NA 0 10.20 163.60
MW-4 11/21/17 45-50 173.80 9.53 NA 0 9.53 164.27
MW-4 02/07/19 45-50 173.80 8.82 NA 0 8.82 164.98
MW-4 05/21/19 45-50 173.80 6.88 NA 0 6.88 166.92
MW-4 09/23/19 45-50 173.80 11.00 NA 0 11.00 162.80
MW-4 12/20/19 45-50 173.80 8.81 NA 0 8.81 164.99
MW-4 03/17/21 45-50 173.80 0.00 NA 0 0.00 173.80
MW-4 05/27/21 45-50 173.80 4.88 NA 0 4.88 168.92
MW-4 08/05/21 45-50 173.80 0.02 NA 0 0.02 173.78
Table 3
Summary of Groundwater Elevations and Free Product Thicknesses 
Food Lion Distribution Center #4
Dunn, North Carolina
Well ID
Date
Measured
Screened
Interval
(feet bgs)
Top of Casing
Elevation*
(feet AMSL)
Depth to
Water (feet
btc)
Depth to Free
Product (feet
btc)
Free Product
Thickness
(feet)

Water
Corrected for
Free Product
Thickness**
(feet btc)
Groundwater
Surface
Elevation***
(feet AMSL)
RW-1 11/11/98 3.5-13.5 172.28 7.75 6.95 0.80 7.06 165.22
RW-1 10/19/10 3.5-13.5 172.28 6.80 5.95 0.85 6.07 166.21
RW-1 12/03/12 3.5-13.5 172.28 7.19 6.80 0.39 6.86 165.42
RW-1 09/09/13 3.5-13.5 172.28 6.31 5.46 0.85 5.58 166.70
RW-1 01/15/14 3.5-13.5 172.28 6.13 5.81 0.32 5.86 166.42
RW-1 04/23/14 3.5-13.5 172.28 5.95 5.81 0.14 5.83 166.45
RW-1 07/28/14 3.5-13.5 172.28 6.15 NA 0 6.15 166.13
RW-1 11/25/14 3.5-13.5 172.28 6.21 NA 0 6.21 166.07
RW-1 02/25/15 3.5-13.5 172.28 5.99 NA 0 5.99 166.29
RW-1 07/21/15 3.5-13.5 172.28 6.21 NA 0 6.21 166.07
RW-1 02/04/16 3.5-13.5 172.28 5.71 NA 0 5.71 166.57
RW-1 04/29/16 3.5-13.5 172.28 6.06 NA 0 6.06 166.22
RW-1 08/09/16 3.5-13.5 172.28 6.14 NA 0 6.14 166.14
RW-1 10/21/16 3.5-13.5 172.28 5.84 NA 0 5.84 166.44
RW-1 03/03/17 3.5-13.6 172.28 6.17 NA 0 6.17 166.11
RW-1 05/17/17 3.5-13.6 172.28 6.24 NA 0 6.24 166.04
RW-1 08/22/17 3.5-13.6 172.28 6.24 NA 0 6.24 166.04
RW-1 11/21/17 3.5-13.6 172.28 6.30 NA 0 6.30 165.98
RW-1 02/07/19 3.5-13.6 172.28 5.64 NA 0 5.64 166.64
RW-1 05/21/19 3.5-13.6 172.28 5.85 NA 0 5.85 166.43
RW-1 09/23/19 3.5-13.6 172.28 6.17 NA 0 6.17 166.11
RW-1 12/20/19 3.5-13.6 172.28 5.61 NA 0 5.61 166.67
RW-1 03/17/21 3.5-13.6 172.28 5.40 NA 0 5.40 166.88
RW-1 05/27/21 3.5-13.6 172.28 5.72 NA 0 5.72 166.56
RW-1 08/05/21 3.5-13.6 172.28 5.67 NA 0 5.67 166.61
RW-2 11/11/98 4.5-14.5 173.53 11.65 8.10 3.55 8.60 164.93
RW-2 10/19/10 4.5-14.5 173.53 8.15 6.15 2.00 6.43 167.10
RW-2 12/03/12 4.5-14.5 173.53 10.35 8.02 2.33 8.35 165.18
RW-2 09/09/13 4.5-14.5 173.53 8.12 6.11 2.01 6.40 167.13
RW-2 01/15/14 4.5-14.5 173.53 5.69 5.00 0.69 5.10 168.43
RW-2 04/23/14 4.5-14.5 173.53 5.72 5.17 0.55 5.25 168.28
RW-2 07/28/14 4.5-14.5 173.53 6.90 6.51 0.39 6.57 166.96
RW-2 11/25/14 4.5-14.5 173.53 7.16 6.69 0.47 6.76 166.77
RW-2 02/25/15 4.5-14.5 173.53 5.80 5.63 0.17 5.65 167.88
RW-2 07/21/15 4.5-14.5 173.53 7.14 6.84 0.30 6.88 166.65
RW-2 02/04/16 4.5-14.5 173.53 5.16 5.04 0.12 5.06 168.47
RW-2 04/29/16 4.5-14.5 173.53 5.85 5.84 0.01 5.84 167.69
RW-2 08/09/16 4.5-14.5 173.53 6.99 6.93 0.06 6.94 166.59
RW-2 10/21/16 4.5-14.5 173.53 5.39 NA 0 5.39 168.14
RW-2 03/03/17 4.5-14.6 173.53 6.58 NA 0 6.58 166.95
RW-2 05/17/17 4.5-14.6 173.53 5.91 NA 0 5.91 167.62
RW-2 08/22/17 4.5-14.6 173.53 7.53 NA 0 7.53 166.00
RW-2 11/21/17 4.5-14.6 173.53 7.53 NA 0 7.53 166.00
RW-2 02/07/19 4.5-14.6 173.53 5.75 NA 0 5.75 167.78
RW-2 05/21/19 4.5-14.6 173.53 NM NA 0 NM NM
RW-2 09/23/19 4.5-14.6 173.53 7.20 NA 0 7.20 166.33
RW-2 12/20/19 4.5-14.6 173.53 5.17 NA 0 5.17 168.36
RW-2 03/17/21 4.5-14.6 173.53 5.22 5.21 0.01 5.21 168.32
RW-2 05/27/21 4.5-14.6 173.53 6.98 NA 0 6.98 166.55
RW-2 08/05/21 4.5-14.6 173.53 5.36 NA 0 5.36 168.17
Table 3
Summary of Groundwater Elevations and Free Product Thicknesses 
Food Lion Distribution Center #4
Dunn, North Carolina
Well ID
Date
Measured
Screened
Interval
(feet bgs)
Top of Casing
Elevation*
(feet AMSL)
Depth to
Water (feet
btc)
Depth to Free
Product (feet
btc)
Free Product
Thickness
(feet)

Water
Corrected for
Free Product
Thickness**
(feet btc)
Groundwater
Surface
Elevation***
(feet AMSL)
RW-3 11/11/98 4.5-14.5 173.44 10.70 7.95 2.75 8.34 165.10
RW-3 10/19/10 4.5-14.5 173.44 7.65 5.39 2.26 5.71 167.73
RW-3 12/03/12 4.5-14.5 173.44 9.93 7.64 2.29 7.96 165.48
RW-3 09/09/13 4.5-14.5 173.44 7.55 5.36 2.19 5.67 167.77
RW-3 01/15/14 4.5-14.5 173.44 3.97 3.47 0.50 3.54 169.90
RW-3 04/23/14 4.5-14.5 173.44 4.70 4.09 0.61 4.18 169.26
RW-3 07/28/14 4.5-14.5 173.44 6.31 5.92 0.39 5.98 167.46
RW-3 11/25/14 4.5-14.5 173.44 5.88 5.68 0.20 5.71 167.73
RW-3 02/25/15 4.5-14.5 173.44 4.90 4.76 0.14 4.78 168.66
RW-3 07/21/15 4.5-14.5 173.44 6.47 6.40 0.07 6.41 167.03
RW-3 02/04/16 4.5-14.5 173.44 4.08 NA 0 4.08 169.36
RW-3 04/29/16 4.5-14.5 173.44 5.12 NA 0 5.12 168.32
RW-3 08/09/16 4.5-14.5 173.44 6.49 NA 0 6.49 166.95
RW-3 10/21/16 4.5-14.5 173.44 4.44 NA 0 4.44 169.00
RW-3 03/03/17 4.5-14.6 173.44 6.01 NA 0 6.01 167.43
RW-3 05/17/17 4.5-14.6 173.44 5.15 NA 0 5.15 168.29
RW-3 08/22/17 4.5-14.6 173.44 7.28 NA 0 7.28 166.16
RW-3 11/21/17 4.5-14.6 173.44 7.06 NA 0 7.06 166.38
RW-3 02/07/19 4.5-14.6 173.44 4.90 NA 0 4.90 168.54
RW-3 05/21/19 4.5-14.6 173.44 5.92 NA 0 5.92 167.52
RW-3 09/23/19 4.5-14.6 173.44 6.77 NA 0 6.77 166.67
RW-3 12/20/19 4.5-14.6 173.44 4.13 NA 0 4.13 169.31
RW-3 03/17/21 4.5-14.6 173.44 4.14 NA 0 4.14 169.30
RW-3 05/27/21 4.5-14.6 173.44 6.53 NA 0 6.53 166.91
RW-3 08/05/21 4.5-14.6 173.44 4.55 NA 0 4.55 168.89
RW-4 11/11/98 4-14 173.14 11.00 7.65 3.35 8.13 165.01
RW-4 10/19/10 4-14 173.14 8.65 5.85 2.80 6.25 166.89
RW-4 12/03/12 4-14 173.14 10.00 7.50 2.50 7.85 165.29
RW-4 09/09/13 4-14 173.14 8.40 5.86 2.54 6.22 166.92
RW-4 01/15/14 4-14 173.14 5.71 5.12 0.59 5.20 167.94
RW-4 04/23/14 4-14 173.14 6.04 5.31 0.73 5.41 167.73
RW-4 07/28/14 4-14 173.14 7.90 6.30 1.60 6.53 166.61
RW-4 11/25/14 4-14 173.14 6.87 6.50 0.37 6.55 166.59
RW-4 02/25/15 4-14 173.14 5.90 5.70 0.20 5.73 167.41
RW-4 07/21/15 4-14 173.14 6.86 6.61 0.25 6.65 166.49
RW-4 02/04/16 4-14 173.14 5.40 5.34 0.06 5.35 167.79
RW-4 04/29/16 4-14 173.14 6.02 6.00 0.02 6.00 167.14
RW-4 08/09/16 4-14 173.14 6.78 NA 0 6.78 166.36
RW-4 10/21/16 4-14 173.14 5.65 NA 0 5.65 167.49
RW-4 03/03/17 4-14 173.14 6.61 NA 0 6.61 166.53
RW-4 05/17/17 4-14 173.14 6.05 NA 0 6.05 167.09
RW-4 08/22/17 4-14 173.14 7.23 NA 0 7.23 165.91
RW-4 11/21/17 4-14 173.14 7.10 NA 0 7.10 166.04
RW-4 02/07/19 4-14 173.14 5.91 NA 0 5.91 167.23
RW-4 05/21/19 4-14 173.14 7.39 NA 0 7.39 165.75
RW-4 09/23/19 4-14 173.14 6.87 NA 0 6.87 166.27
RW-4 12/20/19 4-14 173.14 5.61 NA 0 5.61 167.53
RW-4 03/17/21 4-14 173.14 5.37 NA 0 5.37 167.77
RW-4 05/27/21 4-14 173.14 6.53 NA 0 6.53 166.61
RW-4 08/05/21 4-14 173.14 5.73 NA 0 5.73 167.41
Table 3
Summary of Groundwater Elevations and Free Product Thicknesses 
Food Lion Distribution Center #4
Dunn, North Carolina
Well ID
Date
Measured
Screened
Interval
(feet bgs)
Top of Casing
Elevation*
(feet AMSL)
Depth to
Water (feet
btc)
Depth to Free
Product (feet
btc)
Free Product
Thickness
(feet)

Water
Corrected for
Free Product
Thickness**
(feet btc)
Groundwater
Surface
Elevation***
(feet AMSL)
RW-5 09/09/13 3-13 173.06 6.57 NA 0 6.57 166.49
RW-5 01/15/14 3-13 173.06 6.00 NA 0 6.00 167.06
RW-5 04/23/14 3-13 173.06 6.09 NA 0 6.09 166.97
RW-5 07/28/14 3-13 173.06 6.81 NA 0 6.81 166.25
RW-5 11/25/14 3-13 173.06 NM NM NM NA NA
RW-5 02/25/15 3-13 173.06 6.30 NA 0 6.30 166.76
RW-5 07/21/15 3-13 173.06 6.92 NA 0 6.92 166.14
RW-5 02/04/16 3-13 173.06 5.98 NA 0 5.98 167.08
RW-5 04/29/16 3-13 173.06 6.52 NA 0 6.52 166.54
RW-5 08/09/16 3-13 173.06 6.90 NA 0 6.90 166.16
RW-5 10/21/16 3-13 173.06 6.16 NA 0 6.16 166.90
RW-5 03/03/17 3-14 173.06 6.80 NA 0 6.80 166.26
RW-5 05/17/17 3-14 173.06 6.52 NA 0 6.52 166.54
RW-5 08/22/17 3-14 173.06 7.17 NA 0 7.17 165.89
RW-5 11/21/17 3-14 173.06 7.11 NA 0 7.11 165.95
RW-5 02/07/19 3-14 173.06 6.09 NA 0 6.09 166.97
RW-5 05/21/19 3-14 173.06 6.48 NA 0 6.48 166.58
RW-5 09/23/19 3-14 173.06 7.00 NA 0 7.00 166.06
RW-5 12/20/19 3-14 173.06 5.94 NA 0 5.94 167.12
RW-5 03/17/21 3-14 173.06 5.84 NA 0 5.84 167.22
RW-5 05/27/21 3-14 173.06 6.67 NA 0 6.67 166.39
RW-5 08/05/21 3-14 173.06 6.13 NA 0 6.13 166.93
RW-6 09/09/13 3-18 173.64 8.39 6.57 1.82 6.83 166.81
RW-6 01/15/14 3-18 173.64 7.08 5.73 1.35 5.92 167.72
RW-6 04/23/14 3-18 173.64 6.31 6.05 0.26 6.09 167.55
RW-6 07/28/14 3-18 173.64 7.61 6.95 0.66 7.04 166.60
RW-6 11/25/14 3-18 173.64 8.20 6.99 1.21 7.16 166.48
RW-6 02/25/15 3-18 173.64 6.48 6.36 0.12 6.38 167.26
RW-6 07/21/15 3-18 173.64 8.00 7.19 0.81 7.30 166.34
RW-6 02/04/16 3-18 173.64 6.35 5.88 0.47 5.95 167.69
RW-6 04/29/16 3-18 173.64 6.68 6.60 0.08 6.61 167.03
RW-6 08/09/16 3-18 173.64 7.57 7.27 0.30 7.31 166.33
RW-6 10/21/16 3-18 173.64 6.22 6.20 0.02 6.20 167.44
RW-6 03/03/17 3-18 173.64 7.10 NA 0 7.10 166.54
RW-6 05/17/17 3-18 173.64 6.67 NA 0 6.67 166.97
RW-6 08/22/17 3-18 173.64 8.19 7.76 0.43 7.82 165.82
RW-6 11/21/17 3-18 173.64 7.86 NA 0 7.86 165.78
RW-6 02/07/19 3-18 173.64 6.51 6.50 0.01 6.50 167.14
RW-6 05/21/19 3-18 173.64 7.10 NA 0 7.10 166.54
RW-6 09/23/19 3-18 173.64 7.72 7.63 0.09 7.64 166.00
RW-6 12/20/19 3-18 173.64 6.38 NA 0 6.38 167.26
RW-6 03/17/21 3-18 173.64 5.89 NA 0 5.89 167.75
RW-6 05/27/21 3-18 173.64 7.31 7.21 0.10 7.22 166.42
RW-6 08/05/21 3-18 173.64 6.35 NA 0 6.35 167.29
Table 3
Summary of Groundwater Elevations and Free Product Thicknesses 
Food Lion Distribution Center #4
Dunn, North Carolina
Well ID
Date
Measured
Screened
Interval
(feet bgs)
Top of Casing
Elevation*
(feet AMSL)
Depth to
Water (feet
btc)
Depth to Free
Product (feet
btc)
Free Product
Thickness
(feet)

Water
Corrected for
Free Product
Thickness**
(feet btc)
Groundwater
Surface
Elevation***
(feet AMSL)
RW-7 09/09/13 3-18 173.52 6.50 NA 0 6.50 167.02
RW-7 01/15/14 3-18 173.52 5.49 NA 0 5.49 168.03
RW-7 04/23/14 3-18 173.52 5.62 NA 0 5.62 167.90
RW-7 07/28/14 3-18 173.52 6.75 NA 0 6.75 166.77
RW-7 11/25/14 3-18 173.52 6.82 NA 0 6.82 166.70
RW-7 02/25/15 3-18 173.52 6.97 NA 0 6.97 166.55
RW-7 07/21/15 3-18 173.52 6.98 NA 0 6.98 166.54
RW-7 02/04/16 3-18 173.52 5.61 NA 0 5.61 167.91
RW-7 04/29/16 3-18 173.52 6.32 NA 0 6.32 167.20
RW-7 08/09/16 3-18 173.52 7.02 NA 0 7.02 166.50
RW-7 10/21/16 3-18 173.52 5.77 NA 0 5.77 167.75
RW-7 03/03/17 3-18 173.52 6.79 NA 0 6.79 166.73
RW-7 05/17/17 3-18 173.52 6.28 NA 0 6.28 167.24
RW-7 08/22/17 3-18 173.52 7.44 NA 0 7.44 166.08
RW-7 11/21/17 3-18 173.52 7.33 NA 0 7.33 166.19
RW-7 02/07/19 3-18 173.52 5.88 NA 0 5.88 167.64
RW-7 05/21/19 3-18 173.52 6.56 NA 0 6.56 166.96
RW-7 09/23/19 3-18 173.52 7.17 NA 0 7.17 166.35
RW-7 12/20/19 3-18 173.52 5.58 NA 0 5.58 167.94
RW-7 03/17/21 3-18 173.52 9.29 4.76 4.53 5.40 168.12
RW-7 05/27/21 3-18 173.52 9.85 6.5 3.35 6.98 166.54
RW-7 08/05/21 3-18 173.52 8.87 5.38 3.49 5.88 167.64
RW-8 09/09/13 4-14 173.71 6.81 6.27 0.54 6.35 167.36
RW-8 01/15/14 4-14 173.71 5.21 5.00 0.21 5.03 168.68
RW-8 04/23/14 4-14 173.71 5.26 5.21 0.05 5.22 168.49
RW-8 07/28/14 4-14 173.71 6.92 6.62 0.30 6.66 167.05
RW-8 11/25/14 4-14 173.71 6.59 6.36 0.23 6.39 167.32
RW-8 02/25/15 4-14 173.71 5.68 5.67 0.01 5.67 168.04
RW-8 07/21/15 4-14 173.71 7.41 6.87 0.54 6.95 166.76
RW-8 02/04/16 4-14 173.71 5.50 5.18 0.32 5.23 168.48
RW-8 04/29/16 4-14 173.71 6.05 NA 0 6.05 167.66
RW-8 08/09/16 4-14 173.71 6.98 NA 0 6.98 166.73
RW-8 10/21/16 4-14 173.71 5.45 NA 0 5.45 168.26
RW-8 03/03/17 4-15 173.71 6.75 NA 0 6.75 166.96
RW-8 05/17/17 4-15 173.71 6.00 NA 0 6.00 167.71
RW-8 08/22/17 4-15 173.71 7.60 NA 0 7.60 166.11
RW-8 11/21/17 4-15 173.71 7.70 NA 0 7.70 166.01
RW-8 02/07/19 4-15 173.71 5.74 NA 0 5.74 167.97
RW-8 05/21/19 4-15 173.71 6.92 NA 0 6.92 166.79
RW-8 09/23/19 4-15 173.71 7.55 NA 0 7.55 166.16
RW-8 12/20/19 4-15 173.71 5.24 NA 0 5.24 168.47
RW-8 03/17/21 4-15 173.71 9.72 4.35 5.37 5.11 168.60
RW-8 05/27/21 4-15 173.71 10.70 6.53 4.17 7.12 166.59
RW-8 08/05/21 4-15 173.71 9.79 4.63 5.16 5.36 168.35
Table 3
Summary of Groundwater Elevations and Free Product Thicknesses 
Food Lion Distribution Center #4
Dunn, North Carolina
Well ID
Date
Measured
Screened
Interval
(feet bgs)
Top of Casing
Elevation*
(feet AMSL)
Depth to
Water (feet
btc)
Depth to Free
Product (feet
btc)
Free Product
Thickness
(feet)

Water
Corrected for
Free Product
Thickness**
(feet btc)
Groundwater
Surface
Elevation***
(feet AMSL)
RW-9 09/09/13 4-14.5 173.38 6.78 6.51 0.27 6.55 166.83
RW-9 01/15/14 4-14.5 173.38 5.59 5.56 0.03 5.56 167.82
RW-9 04/23/14 4-14.5 173.38 4.89 4.80 0.09 4.81 168.57
RW-9 07/28/14 4-14.5 173.38 6.40 6.30 0.10 6.31 167.07
RW-9 11/25/14 4-14.5 173.38 6.04 6.02 0.02 6.02 167.36
RW-9 02/25/15 4-14.5 173.38 5.28 NA 0 5.28 168.10
RW-9 07/21/15 4-14.5 173.38 6.63 6.56 0.07 6.57 166.81
RW-9 02/04/16 4-14.5 173.38 4.90 4.89 0.01 4.89 168.49
RW-9 04/29/16 4-14.5 173.38 5.74 NA 0 5.74 167.64
RW-9 08/09/16 4-14.5 173.38 6.63 NA 0 6.63 166.75
RW-9 10/21/16 4-14.5 173.38 5.15 NA 0 5.15 168.23
RW-9 03/03/17 4-14.6 173.38 6.31 NA 0 6.31 167.07
RW-9 05/17/17 4-14.6 173.38 5.65 NA 0 5.65 167.73
RW-9 08/22/17 4-14.6 173.38 7.26 NA 0 7.26 166.12
RW-9 11/21/17 4-14.6 173.38 7.10 NA 0 7.10 166.28
RW-9 02/07/19 4-14.6 173.38 5.40 NA 0 5.40 167.98
RW-9 05/21/19 4-14.6 173.38 6.14 NA 0 6.14 167.24
RW-9 09/23/19 4-14.6 173.38 6.90 NA 0 6.90 166.48
RW-9 12/20/19 4-14.6 173.38 4.89 NA 0 4.89 168.49
RW-9 03/17/21 4-14.6 173.38 4.79 NA 0 4.79 168.59
RW-9 05/27/21 4-14.6 173.38 6.50 NA 0 6.50 166.88
RW-9 08/05/21 4-14.6 173.38 5.06 NA 0 5.06 168.32
Notes:
*Well locations and casing elevations surveyed 7/26/2013 to NC State Plane NAD '83 and NAVD '88
***Groundwater elevation is calculated using corrected depths to water
AMSL = above mean sea level
bgs = below ground surface btc = below top of casing
NA = Not Applicable NM = Not Measured
** Corrected Groundwater Surface Elevation = [Top of Casing elevation – Depth to water table] +
[free-product thickness * 0.8581 (specific gravity of diesel)]
Table 4
Cumulative Volume of Free Product Recovered from Site
Food Lion Distribution Center #4
Dunn, North Carolina
Date of Recovery Event
Total Volume Recovered from Site
During Current Recovery Event
(gallons)
Cumulative Total of Volume Recovered
to Date from All Recovery Events
(gallons)
05/08/98 (Historical AFVR)326 326
06/12/98 (Historical AFVR)524 850
07/06/98 (Historical AFVR)523 1373
07/22/98 (Historical AFVR)326 1699
09/09/13 - 09/11/13 (1st AFVR Event)192 1891
01/15/14 - 01/17/14 (2nd AFVR Event)190 2081
04/23/14 - 04/25/14 (3rd AFVR Event)179 2260
07/28/14 - 07/30-14 (4th AFVR Event)131 2391
11/25/14 - 11/26/14 (5th AFVR Event)81 2472
2/25/15 (6th AFVR Event)10 2482
07/21/15 - 07/22/15 (7th AFVR Event)4 2486
02/04/16 - 02/05/16 (8th AFVR Event)5 2491
04/29/16 (Socks)0.50 2491.50
08/09/16 (Socks)0.75 2492.25
10/21/16 (Socks)0.25 2492.50
03/03/17 (Socks)0*2492.50
05/17/17 (Socks)0*2492.50
08/22/17 (Socks)0.50 2493.00
11/21/17 (Socks)0.50 2493.50
2/7/19 (Socks)0.1 2493.60
5/21/19 (Socks)0*2493.60
9/23/19 (Socks)0.25 2493.60
12/20/19 (Socks)0*2493.60
3/17/2021 (Socks)0**2493.60
5/27/2021 (Socks + Low Flow Pump)14 2507.60
8/5/2021 (Socks + Low Flow Pump)15 2522.60
Notes:
AFVR = Aggressive Fluid Vapor Recovery
Socks = recovery via oil-only absorbent socks
Volumes less than one gallon are rounded to the nearest quarter gallon.
* negligible volume
** Several feet of free product was observed in recovery wells RW7 amd RW8. Free product was not removed but absorbent socks were deployed.
Table 5
Summary of Groundwater Analytical Results
Food Lion Distribution Center #4
Dunn, North Carolina
MW-1 MW-2 MW-3 MW-4* RW-1 RW-2**
C5-C8 Aliphatics MADEP VPH µg/L NE 400 ND ND ND NS <100 NS <100 <100 <100 <100 NS NS <100
C9-C18 Aliphatics MADEP EPH/VPH µg/L NE 700 ND ND ND NS 270 NS 640 1,030 220 740 NS NS 170
C19-C36 Aliphatics MADEH EPH µg/L NE 10,000 ND ND ND NS 230 NS 200 220 <100 <100 NS NS <97
C9-C22 Aromatics MADEP EPH/VPH µg/L NE 200 ND ND ND NS 250 NS 1,040 1,680 420 1,090 NS NS 420
C9-C18 Aliphatics MADEP EPH µg/L NE NE <100 <100 <100 NS 270 NS 280 370 <100 130 NS NS <97
C19-C36 Aliphatics MADEP EPH µg/L NE NE <100 <100 <100 NS 230 NS 200 220 <100 <100 NS NS <97
Unadjusted C11-C22 Aromatics MADEP EPH µg/L NE NE <100 <100 <100 NS 250 NS 750 1,100 230 580 NS NS 270
C11-C22 Aromatics MADEP EPH µg/L NE NE <100 <100 <100 NS 250 NS 700 950 210 500 NS NS 260
Unadjusted C5-C8 Aliphatics MADEP VPH µg/L NE NE <100 <100 <100 NS <100 NS <100 <100 <100 <100 NS NS <100
C5-C8 Aliphatics MADEP VPH µg/L NE NE <100 <100 <100 NS <100 NS <100 <100 <100 <100 NS NS <100
Unadjusted C9-C12 Aliphatics MADEP VPH µg/L NE NE <100 <100 <100 NS <100 NS 360 660 220 610 NS NS 170
C9-C12 Aliphatics MADEP VPH µg/L NE NE <100 <100 <100 NS <100 NS <100 <100 <100 <100 NS NS <100
C9-C10 Aromatics MADEP VPH µg/L NE NE <100 <100 <100 NS <100 NS 290 580 190 510 NS NS 150
Benzene SM 6200B µg/L 5,000 1 <0.13 <0.13 <0.13 NS <0.13 NS 3.6 10 5.4 6.1 NS NS 0.66
Ethylbenzene SM 6200B µg/L 84,500 600 <0.090 <0.090 <0.090 NS <0.090 NS 2.2 9.5 8 11 NS NS 1
Methyl-tert-butyl ether (MTBE)SM 6200B µg/L 20,000 20 <0.17 <0.17 <0.17 NS <0.17 NS 0.95 2.1 0.39 J <0.17 NS NS <0.17
Toluene SM 6200B µg/L 260,000 600 <0.11 <0.11 <0.11 NS <0.11 NS <0.11 0.13 J <0.11 0.12 J NS NS <0.11
m,p-Xylene SM 6200B µg/L 85,500 500 <0.18 <0.18 <0.18 NS <0.18 NS 1.2 4.8 2.2 20 NS NS 0.47 J
o-Xylene SM 6200B µg/L 85,500 500 <0.090 <0.090 <0.090 NS <0.090 NS 0.17 J 0.32 J <0.090 2.8 NS NS <0.090
Acenaphthene 625.1 µg/L 1,950 80 <0.222 <0.222 <0.222 NS <0.222 NS 1.27 J 1.59 J 0.476 J 1.37 J NS NS 0.42 J
Diethylphthalate 625.1 µg/L NE 6,000 <0.216 <0.216 <0.216 NS <0.216 NS <0.217 <0.218 <0.218 0.312 J NS NS <0.225
2,4-Dimethylphenol 625.1 µg/L 100,000 100 <0.764 <0.764 <0.764 NS <0.764 NS <0.768 0.913 J <0.772 <0.776 NS NS <0.795
Bis(2-Ethylhexyl)phthalate 625.1 µg/L 135 3 <0.499 0.702 J <0.499 NS <0.499 NS <0.501 <0.504 <0.504 <0.506 NS NS <0.519
Fluorene 625.1 µg/L 845 300 <0.236 <0.236 <0.236 NS <0.236 NS 1.92 J 3.31 J 1.34 J 3.38 J NS NS 1.33 J
Naphthalene 625.1 µg/L 6,000 6 <0.425 <0.425 <0.425 NS <0.425 NS 13.6 39.8 8.73 21.3 NS NS 1.43 J
2-Methylnaphthalene 625.1 µg/L 12,000 30 <0.256 <0.256 <0.256 NS <0.256 NS 19.2 45.3 5.85 37.6 NS NS 4.51 J
Phenanthrene 625.1 µg/L 550 200 <0.276 <0.276 <0.276 NS <0.276 NS 1.69 J 3.02 J 1.03 J 3.53 J NS NS 1.82 J
2-Methylphenol 625.1 µg/L 400,000 400 <0.438 <0.438 <0.438 NS <0.438 NS <0.441 0.573 J <0.443 <0.445 NS NS <0.456
Phenol 625.1 µg/L 30,000 30 <0.190 <0.190 <0.190 NS <0.190 NS <0.191 0.388 J <0.192 <0.193 NS NS <0.198
3/4-Methylphenol 625.1 µg/L NE 40 <0.196 <0.196 <0.196 NS <0.196 NS <0.197 0.544 J <0.198 <0.199 NS NS <0.204
Pyrene 625.1 µg/L 200 200 <0.245 <0.245 <0.245 NS <0.245 NS 0.57 J 0.563 J <0.248 0.312 J NS NS <0.255
2,4,6-Trichlorophenol 625.1 µg/L 4,000 4 <0.320 <0.320 <0.320 NS <0.320 NS 1.01 J 1.19 J <0.323 <0.325 NS NS <0.333
.beta.-Naphthaleneacetic acid 625.1 µg/L NE NE NM NM NM NS NM NS NM 17 NM NM NS NS NM
1H-Indene, 2,3-dihydro-1,2-...625.1 µg/L NE NE NM NM NM NS NM NS 8.8 NM NM NM NS NS NM
1H-Indene, 2,3-dihydro-4,6-...625.1 µg/L NE NE NM NM NM NS NM NS NM NM NM 6 NS NS NM
1H-Indene, 2,3-dihydro-4,7-...625.1 µg/L NE NE NM NM NM NS NM NS NM 23 NM NM NS NS NM
1H-Indene, 2,3-dihydro-4-me...625.1 µg/L NE NE NM NM NM NS NM NS NM NM 11 NM NS NS NM
1-Phenyl-1-butene 625.1 µg/L NE NE NM NM NM NS NM NS 25 NM NM 24 NS NS NM
3-Pentenoic acid, 4-phenyl-625.1 µg/L NE NE NM NM NM NS NM NS NM 110 NM NM NS NS NM
Benzene, 1,2,3,4-tetramethyl-625.1 µg/L NE NE NM NM NM NS NM NS NM NM 4 5.9 NS NS NM
Benzene, 1,2,3-trimethyl-625.1 µg/L NE NE NM NM NM NS NM NS NM 20 NM 35 NS NS NM
Benzene, 1,2,4,5-tetramethyl-625.1 µg/L NE NE NM NM NM NS NM NS 7.9 13 NM 8.3 NS NS NM
Benzene, 1-ethyl-2,3-dimethyl-625.1 µg/L NE NE NM NM NM NS NM NS 5.2 NM NM NM NS NS NM
Biphenyl 625.1 µg/L NE NE NM NM NM NS NM NS NM NM 4 9.4 NS NS NM
Indane 625.1 µg/L NE NE NM NM NM NS NM NS 6.7 NM 7.7 6.7 NS NS NM
Mesitylacetic acid 625.1 µg/L NE NE NM NM NM NS NM NS 8 NM NM NM NS NS NM
Naphthalene, 1,2,3,4-tetrah...625.1 µg/L NE NE NM NM NM NS NM NS NM NM NM NM NS NS 5.1
Naphthalene, 1,2,3,4-tetrah... (01)625.1 µg/L NE NE NM NM NM NS NM NS 17 39 7.3 NM NS NS NM
Naphthalene, 1,2,3,4-tetrah... (02)625.1 µg/L NE NE NM NM NM NS NM NS 8.2 14 5.9 NM NS NS NM
Naphthalene, 1,2,3,4-tetrah... (04)625.1 µg/L NE NE NM NM NM NS NM NS NM NM NM 13 NS NS NM
Naphthalene, 1,2-dimethyl-625.1 µg/L NE NE NM NM NM NS NM NS NM NM NM NM NS NS 4.6
Naphthalene, 1,3-dimethyl-625.1 µg/L NE NE NM NM NM NS NM NS NM NM NM 13 NS NS 4
Naphthalene, 1,8-dimethyl-625.1 µg/L NE NE NM NM NM NS NM NS NM NM 8.7 NM NS NS NM
Naphthalene, 2,3,6-trimethyl-625.1 µg/L NE NE NM NM NM NS NM NS 7.1 NM NM NM NS NS NM
Naphthalene, 2,3-dimethyl-625.1 µg/L NE NE NM NM NM NS NM NS NM NM NM 23 NS NS NM
Notes:
ug/L = micrograms per liter
mg/L = milligrams per liter
"<0.19" = Compound not detected above the laboratory Method Detection Limit
2L Groundwater Standard = North Carolina 15A NCAC 2L .0202 Groundwater Standard
Groundwater GCLs = North Carolina 15A NCAC 2L Gross Contaminant Levels for Groundwater
Shaded values indicate concentration exceeding 2L Standard
HT = Sample received and analyzed out of hold time
J = Estimated value below the laboratory reporting limit
* = Well not sampled due to obstruction
** = Well not sampled due to the presence of free product
MADEP VPH= Massachusetts Department of Environmental Protection Volatile Petroleum Hydrocarbons
NE = No value established, ND = No detection, NS = Not Sampled
Completed By: DB Date: 3/30/2021 Reviewed By: AK Date: 4/13/2021
Compound Analytical Method Units
Groundwater
GCLs
(µg/L)
2L
Groundwater
Standard
(µg/L)03/17/21 03/17/21 03/17/21 03/17/21 03/17/21 03/17/21
RW-5 RW-6 RW-9RW-7**
Semi-Volatile Organic Compounds - Tentatively Identified Compounds (TICs)
03/17/21
Sample Identification and Date
03/17/21
Semi-Volatile Organic Compounds
Petroleum Hydrocarbon Fractions
RW-8**
03/17/21 03/17/21 03/17/21 03/17/21
Calculated Petroleum Hydrocarbon Fractions
Volatile Organic Compounds
RW-3
03/17/21
RW-4
Table 6
Summary of Groundwater Field Parameters
Food Lion Distribution Center #4
Dunn, North Carolina
Monitoring
Well ID Date Temperature
(°C)
pH
(SU)
Specific
Conductance
(µS/cm)
DO
(mg/L)
Oxidation /
Reduction Potential
(mV)
Turbidity (NTU)
MW-1 3/17/2021 17.55 4.36 768 NM 434.0 8.10
MW-2 3/17/2021 15.60 5.42 105 NM 284.0 3.20
MW-3 3/17/2021 18.66 5.09 300 NM 378.0 0.00
MW-4 3/17/2021
RW-1 3/17/2021 16.14 6.03 34 NM 72.0 14.60
RW-2 3/17/2021
RW-3 3/17/2021 19.07 6.33 173 NM -44.0 5.90
RW-4 3/17/2021 16.06 5.69 169 NM 30.0 3.30
RW-5 3/17/2021 16.17 5.41 110 NM 78.0 0.00
RW-6 3/17/2021 16.96 5.20 84 NM 124.0 0.00
RW-7 3/17/2021
RW-8 3/17/2021
RW-9 3/17/2021 16.43 5.32 73 NM 85.0 3.80
Notes:
Field measurements conducted by Wood using a YSI 556/Professional Plus Multi-Probe System
NM = Not measurable due to equipment malfunction SU = Standard Units
mS/cm = milli-Siemens per centimeter °C = Degrees Celcius mg/L = milligrams per liter mV = millivolts DO = dissolved oxygen
Completed By: DB Date: 3/30/2021 Reviewed By: AK Date: 4/13/2021
NOT SAMPLED DUE TO OBSTRUCTION
NOT SAMPLED DUE TO FREE PHASE PRODUC
NOT SAMPLED DUE TO FREE PHASE PRODUC
NOT SAMPLED DUE TO FREE PHASE PRODUC
FIGURES
Copyright:© 2013 National Geographic Society, i-cubed
³
0 2,4001,200 Feet
FOOD LION DISTRIBUTION CENTER #4
2940 Arrowhead Road, Dunn, North Carolina
Figure
DR:CHK:
DATE:
SITE LOCATION MAP
1
D.Young A. Kellogg
01/13/2022
CLIENT:
PROJ.: 6228210058
TITLE:
SCALE:SITE:
LOCATION: P:\Comm-Ind\Projects\Clients A to F\Food Lion\6228210058 - 2021 LNAPL Recovery\07 GIS
FOOD LION, INC.
1 "=1,200 '
SITE
Wood Environment &
Infrastructure Solutions, Inc.
4021 Stirrup Creek Drive, Suite 100
Durham, NC 27703
[phone]
Legend
Site Boundary
!(
!(
!(#7
#7 #7
#7
#7
#7
#7
#7
#7
"D
Diesel ASTs
Former Location
of USTs
Product Pipeline
Pump Islands
Former
Treatment System
Highwa
y 301
RW-9
RW-8
RW-7
RW-6
RW-5
RW-4
RW-3
RW-2
RW-1MW-1
MW-3
MW-2
MW-4
NC Center for Geographic Information & Analysis
Legend
"D Deep Monitoring Well
!(Monitoring Well
#7 Recovery Well
³
0 8040Feet
FOOD LION DISTRIBUTION CENTER #4
2940 Arrowhead Road, Dunn, North Carolina
Figure
DR:CHK:
DATE:
SITE LAYOUT AND
WELL LOCATION MAP 2
D.Young A.Kellogg
01/13/2022
CLIENT:
PROJ.: 6228210058
TITLE:
SCALE:SITE:
LOCATION: P:\Comm-Ind\Projects\Clients A to F\Food Lion\6228210058 - 2021 LNAPL Recovery\07 GIS
FOOD LION, INC.
1 "=40 '
Wood Environment &
& Infrastructure, Inc.
4021 Stirrup Creek Drive, Suite 100
Durham, NC 27703
[phone]
!(
!(!(#0 #0 #0#0#0#0
#0#0#0
"D
!?!?
!?
Source: Esri, Maxar, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community
Figure:
3A. Kellogg S. Knox
01/13/2022 62282100584021 Stirrup Creek Drive, Suite 100Durham, NC 27703(919) 381-9900 P:\Comm-Ind\Projects\Clients A to F\Food Lion\6228210058 - 2021 LNAPL Recovery\07 GIS
1 " = 400 '
³
0 400 800
Feet
!?Water Supply Wells Within 1,500 Feet
"D Deep Monitoring Well
!(Monitoring Well
#0 Recovery Well
Drainage Ditch
Roadways
Site Boundary
1,500-Foot Buffer
Harnett County Parcels
2940 Arrowhead Road, Dunn, North Carolina
1473 Ammons Rd.
1445 Ammons Rd.
93 Longbranch Rd.
RetentionPond
!(
!(
!(#0
#0 #0
#0
#0
#0
#0
#0
#0
"D
Source: Esri, Maxar, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community
Notes:* Well not used for contouringOBS = Obstruction in well
Figure:
DR:CHK:DATE:
GROUNDWATER FLOW MAPMARCH 17, 2021
CLIENT:
PROJ.:
TITLE:
SCALE:SITE:
Wood Environment & Infrastructure Solutions, Inc.
LOCATION:
FOOD LION, INC.
³
Legend
"D
!(
#0
FOOD LION DISTRIBUTION CENTER #4
171
170169
168167
!(
!(
!(#0
#0 #0
#0
#0
#0
#0
#0
#0
"D
Source: Esri, Maxar, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community
Notes:All values are in micrograms per liter (ug/L)Only values exceeding the 15A NCAC 2L .0202 Groundwater Standards are shownNE = No 2L exceedances detectedNSP = Well not sampled due to the presence of free phase productNSO = Well not sampled due to an obstruction.
Figure:
DR:CHK:DATE:
GROUNDWATER EXCEEDANCES TAG MAPMARCH 17, 2021
CLIENT:
PROJ.:
TITLE:
SCALE:SITE:
Wood Environment & Infrastructure Solutions, Inc.
LOCATION:
FOOD LION, INC.
³
Legend
"D
!(
#0
FOOD LION DISTRIBUTION CENTER #4
APPENDIX A
GROUNDWATER SAMPLING LOGS
Site Name:Food Lion
Sampler Name:Forrest Hayward
Well ID MW-1
Date:3/17/2021
Depth to Water:3.76
TOC Elevation 170.22
Top of Sceen:0.00
WL Elevation 166.46
Well Depth 15.00
Time ms/cm %∆DO (mg/L)%∆pH ∆ORP (mV)∆
Turbidity
(NTU)%∆Qual Temp (Co)∆DTW (feet)∆
1205
1220 0.8 #DIV/0!#DIV/0!4.41 ##############3.98
0.1%#DIV/0!0.01 1.00 38%-0.06 0.00
Limits 3%10%0.1 10 <10.00 0.50
Purge Stop time 1232 Sampler Signature:
Sample Time 1235
Total Purge Time 27
Total Purge Volume (L)7.5
Average Flow Rate (L/min)0.278
Sampling Device Peri
Number of Bottles 8
Other Notes and Comments
Site Name:Food Lion
Sampler Name:Forrest Hayward
Well ID MW-2
Date:3/17/2021
Depth to Water:6.24
TOC Elevation 172.88
Top of Sceen:0.00
WL Elevation 166.64
Well Depth 15.00
Time ms/cm %∆DO (mg/L)%∆pH ∆ORP (mV)∆
Turbidity
(NTU)%∆Qual Temp (Co)∆DTW (feet)∆
1052
1110 0.1 #DIV/0!0.00 #DIV/0!5.37 5.37 256.0 #####5.52 #####15.42 ####6.24 6.24
1113 0.1 1.8%0.00 #DIV/0!5.37 0.00 257.0 1.00 5.20 6%15.61 0.19 6.24 0.00
1116 0.1 -1.7%0.00 #DIV/0!5.37 0.00 256.0 1.00 6.10 17%15.73 0.12 6.25 0.01
1119 0.1 -4.4%0.00 #DIV/0!5.38 0.01 263.0 7.00 5.40 11%15.77 0.04 6.26 0.01
1122 0.1 1.8%0.00 #DIV/0!5.39 0.01 269.0 6.00 4.20 22%15.70 -0.07 6.25 -0.01
1125 0.1 0.9%0.00 #DIV/0!5.39 0.00 277.0 8.00 3.80 10%15.68 -0.02 6.25 0.00
1128 0.1 0.9%0.00 #DIV/0!5.40 0.01 281.0 4.00 3.30 13%15.63 -0.05 6.25 0.00
1131 0.1 0.0%0.00 #DIV/0!5.42 0.02 284.0 3.00 3.20 3%15.60 -0.03 6.25 0.00
Limits 3%10%0.1 10 <10.00 0.50
Purge Stop time 1131 Sampler Signature:
Sample Time 1135
Total Purge Time 39
Total Purge Volume (L)5.5
Average Flow Rate (L/min)0.141
Sampling Device peri pump
Number of Bottles 8
Other Notes and Comments
Site Name:Food Lion
Sampler Name:Forrest Hayward
Well ID MW-3
Date:3/17/2021
Depth to Water:1.40
TOC Elevation 172.72
Top of Sceen:0.00
WL Elevation 171.32
Well Depth 15.00
Time ms/cm %∆DO (mg/L)%∆pH ∆ORP (mV)∆
Turbidity
(NTU)%∆Qual Temp (Co)∆DTW (feet)∆
1310
1322 0.3 #DIV/0!#DIV/0!5.05 ##############1.54
0.0%#DIV/0!0.00 1.00 100%-0.02 0.00
Limits 3%10%0.1 10 <10.00 0.50
Purge Stop time 1334 Sampler Signature:
Sample Time 1340
Total Purge Time 24
Total Purge Volume (L)9
Average Flow Rate (L/min)0.375
Sampling Device peri pump
Number of Bottles 8
Other Notes and Comments
Site Name:Food Lion
Sampler Name:Forrest Hayward
Well ID RW-1
Date:3/17/2021
Depth to Water:5.45
TOC Elevation 172.28
Top of Sceen:0.00
WL Elevation 166.83
Well Depth 13.50
Time ms/cm %∆DO (mg/L)%∆pH ∆ORP (mV)∆
Turbidity
(NTU)%∆Qual Temp (Co)∆DTW (feet)∆
1410
1420 0.039 #DIV/0!#DIV/0!5.89 61.00 #########5.45
0.0%23%0.01 1.00 6%0.02 0.00
0.0%11%0.01 1.00 4%0.02 0.00
Limits 3%10%0.1 10 <10.00 0.50
Purge Stop time 1500 Sampler Signature:
Sample Time 1505
Total Purge Time 50
Total Purge Volume (L)8.2
Average Flow Rate (L/min)0.164
Sampling Device peri pump
Number of Bottles 8
Other Notes and Comments
Site Name:Food Lion
Sampler Name:Forrest Hayward
Well ID RW-3
Date:3/17/2021
Depth to Water:4.14
TOC Elevation 173.44
Top of Sceen:0.00
WL Elevation 169.30
Well Depth 14.50
Time ms/cm %∆DO (mg/L)%∆pH ∆ORP (mV)∆
Turbidity
(NTU)%∆Qual Temp (Co)∆DTW (feet)∆
1405
1430 0.2 #DIV/0!#DIV/0!6.35 39.00 #########4.18
0.6%#DIV/0!0.00 0.00 3%0.09 0.00
Limits 3%10%0.1 10 <10.00 0.50
Purge Stop time 1445 Sampler Signature:
Sample Time 1450
Total Purge Time 40
Total Purge Volume (L)11
Average Flow Rate (L/min)0.275
Sampling Device peri pump
Number of Bottles 8
Other Notes and Comments
Site Name:Food Lion
Sampler Name:Forrest Hayward
Well ID RW-4
Date:3/17/2021
Depth to Water:5.37
TOC Elevation 173.14
Top of Sceen:0.00
WL Elevation 167.77
Well Depth 14.00
Time ms/cm %∆DO (mg/L)%∆pH ∆ORP (mV)∆
Turbidity
(NTU)%∆Qual Temp (Co)∆DTW (feet)∆
920
930 0.162 #DIV/0!5.90 #DIV/0!6.20 6.20 50.0 50.00 3.50 #####17.40 ####5.43 5.43
935 0.177 9.3%0.00 100%5.63 0.57 38.0 12.00 3.30 6%16.64 -0.76 5.50 0.07
940 0.175 -1.1%0.00 #DIV/0!5.61 0.02 37.0 1.00 3.50 6%16.43 -0.21 5.50 0.00
945 0.171 -2.3%0.00 #DIV/0!5.66 0.05 31.0 6.00 3.50 0%16.37 -0.06 5.45 -0.05
950 0.169 1.2%0.00 #DIV/0!5.69 0.03 30.0 1.00 3.30 6%16.06 -0.31 5.45 0.00
Limits 3%10%0.1 10 <10.00 0.50
Purge Stop time 950 Sampler Signature:
Sample Time 955
Total Purge Time 30
Total Purge Volume (L)4
Average Flow Rate (L/min)0.133
Sampling Device Peri pump
Number of Bottles 8
Other Notes and Comments
Site Name:Food Lion
Sampler Name:Forrest Hayward
Well ID RW-5
Date:3/17/2021
Depth to Water:5.85
TOC Elevation 173.06
Top of Sceen:0.00
WL Elevation 167.21
Well Depth 13.00
Time ms/cm %∆DO (mg/L)%∆pH ∆ORP (mV)∆
Turbidity
(NTU)%∆Qual Temp (Co)∆DTW (feet)∆
1025
1035 0.111 #DIV/0!#DIV/0!5.30 74.00 #########5.90
Limits 3%10%0.1 10 <10.00 0.50
Purge Stop time 1050 Sampler Signature:
Sample Time 1055
Total Purge Time 25
Total Purge Volume (L)4.4
Average Flow Rate (L/min)0.176
Sampling Device peri pump
Number of Bottles 8
Other Notes and Comments
Site Name:Food Lion
Sampler Name:Forrest Hayward
Well ID RW-6
Date:3/17/2021
Depth to Water:5.88
TOC Elevation 173.64
Top of Sceen:0.00
WL Elevation 167.76
Well Depth 18.00
Time ms/cm %∆DO (mg/L)%∆pH ∆ORP (mV)∆
Turbidity
(NTU)%∆Qual Temp (Co)∆DTW (feet)∆
1125
1135 0.084 #DIV/0!#DIV/0!5.17 ##############6.05
0.0%#DIV/0!0.00 2.00 #####0.02 0.00
Limits 3%10%0.1 10 <10.00 0.50
Purge Stop time 1150 Sampler Signature:
Sample Time 1155
Total Purge Time 24
Total Purge Volume (L)4.5
Average Flow Rate (L/min)0.188
Sampling Device peri pump
Number of Bottles 8
Other Notes and Comments
Site Name:Food Lion
Sampler Name:Forrest Hayward
Well ID RW-9
Date:3/17/2021
Depth to Water:4.80
TOC Elevation 173.38
Top of Sceen:0.00
WL Elevation 168.58
Well Depth 14.50
Time ms/cm %∆DO (mg/L)%∆pH ∆ORP (mV)∆
Turbidity
(NTU)%∆Qual Temp (Co)∆DTW (feet)∆
1320
1330 0.076 #DIV/0!#DIV/0!5.41 60.00 #########4.81
0.0%#DIV/0!0.00 1.00 0%0.05 0.01
Limits 3%10%0.1 10 <10.00 0.50
Purge Stop time 1342 Sampler Signature:
Sample Time 1345
Total Purge Time 22
Total Purge Volume (L)3.9
Average Flow Rate (L/min)0.177
Sampling Device peri pump
Number of Bottles 8
Other Notes and Comments

APPENDIX B WASTE DISPOSAL DOCUMENTATION

APPENDIX C LABORATORY ANALYTICAL REPORTS
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 29, 2021
Anthony Kellogg
Wood PLC - Durham, NC
4021 Stirrup Creek Drive, Suite 100
Durham, NC 27703
Project Location: Dunn, NC
Client Job Number:
Project Number: 6228-21-0058
Laboratory Work Order Number: 21C0992
Enclosed are results of analyses for samples received by the laboratory on March 18, 2021. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 85
Table of Contents
Table of Contents
Sample Summary 4
Case Narrative 6
Sample Results 9
21C0992-01 9
21C0992-02 15
21C0992-03 21
21C0992-04 27
21C0992-05 33
21C0992-06 39
21C0992-07 45
21C0992-08 51
21C0992-09 57
Sample Preparation Information 63
QC Data 64
Volatile Organic Compounds by GC/MS 64
B278468 64
Semivolatile Organic Compounds by - GC/MS 65
B278676 65
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED) 69
B278676 69
Petroleum Hydrocarbons Analyses - EPH 70
B278778 70
Petroleum Hydrocarbons Analyses - VPH 72
B278407 72
Flag/Qualifier Summary 74
Page 2 of 85
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Table of Contents (continued)
Certifications 75
Chain of Custody/Sample Receipt 79
Page 3 of 85
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/29/2021
Wood PLC - Durham, NC
4021 Stirrup Creek Drive, Suite 100
Durham, NC 27703
ATTN: Anthony Kellogg
6228-21-0058
21C0992
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Dunn, NC
MW-2 21C0992-01 Ground Water 625.1
MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM21-22 6200B
MW-1 21C0992-02 Ground Water 625.1
MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM21-22 6200B
MW-3 21C0992-03 Ground Water 625.1
MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM21-22 6200B
RW-3 21C0992-04 Ground Water 625.1
MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM21-22 6200B
RW-4 21C0992-05 Ground Water 625.1
MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM21-22 6200B
RW-5 21C0992-06 Ground Water 625.1
MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM21-22 6200B
RW-6 21C0992-07 Ground Water 625.1
MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM21-22 6200B
RW-9 21C0992-08 Ground Water 625.1
MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 4 of 85
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/29/2021
Wood PLC - Durham, NC
4021 Stirrup Creek Drive, Suite 100
Durham, NC 27703
ATTN: Anthony Kellogg
6228-21-0058
21C0992
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Dunn, NC
RW-1 21C0992-09 Ground Water 625.1
MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM21-22 6200B
Page 5 of 85
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
For method MA EPH, only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
Page 6 of 85
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
625.1
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Benzidine
21C0992-01[MW-2], 21C0992-02[MW-1], 21C0992-03[MW-3], 21C0992-04[RW-3], 21C0992-05[RW-4], 21C0992-06[RW-5], 21C0992-07[RW-6], 21C0992-08[RW-9],
21C0992-09[RW-1], B278676-BLK1, B278676-BS1, B278676-BSD1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
Benzidine
21C0992-01[MW-2], 21C0992-02[MW-1], 21C0992-03[MW-3], 21C0992-04[RW-3], 21C0992-05[RW-4], 21C0992-06[RW-5], 21C0992-07[RW-6], 21C0992-08[RW-9],
21C0992-09[RW-1], B278676-BLK1, B278676-BS1, B278676-BSD1
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-04
Benzidine
21C0992-01[MW-2], 21C0992-02[MW-1], 21C0992-03[MW-3], 21C0992-04[RW-3], 21C0992-05[RW-4], 21C0992-06[RW-5], 21C0992-07[RW-6], 21C0992-08[RW-9],
21C0992-09[RW-1], S058195-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
Benzidine
21C0992-01[MW-2], 21C0992-02[MW-1], 21C0992-03[MW-3], 21C0992-04[RW-3], 21C0992-05[RW-4], 21C0992-06[RW-5], 21C0992-07[RW-6], 21C0992-08[RW-9],
21C0992-09[RW-1], B278676-BLK1, B278676-BS1, B278676-BSD1, S058195-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
Benzidine
21C0992-01[MW-2], 21C0992-02[MW-1], 21C0992-03[MW-3], 21C0992-04[RW-3], 21C0992-05[RW-4], 21C0992-06[RW-5], 21C0992-07[RW-6], 21C0992-08[RW-9],
21C0992-09[RW-1], S058195-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-35
Benzidine
B278676-BLK1, B278676-BS1, B278676-BSD1
MADEP-VPH-Feb 2018 Rev 2.1
Qualifications:
Surrogate recovery outside of control limits due to suspected sample matrix interference. Chromatogram(s) is attached.
Analyte & Samples(s) Qualified:
S-15
2,5-Dibromotoluene (PID)
21C0992-04[RW-3], 21C0992-05[RW-4], 21C0992-06[RW-5], 21C0992-07[RW-6]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Bromomethane
S058052-CCV1
Page 7 of 85
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Chloromethane
S058052-CCV1
Naphthalene
S058052-CCV1
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain-of-custody
form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 8 of 85
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-01
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:35
[TOC_2]21C0992-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/22/21 14:39 LBDµg/L0.13 3/22/21SM21-22 6200B1Benzene
ND 0.50 3/22/21 14:39 LBDµg/L0.080 3/22/21SM21-22 6200B1Chlorobenzene
ND 0.50 3/22/21 14:39 LBDµg/L0.10 3/22/21SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/22/21 14:39 LBDµg/L0.090 3/22/21SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/22/21 14:39 LBDµg/L0.11 3/22/21SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/22/21 14:39 LBDµg/L0.090 3/22/21SM21-22 6200B1Ethylbenzene
ND 0.50 3/22/21 14:39 LBDµg/L0.17 3/22/21SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 0.50 3/22/21 14:39 LBDµg/L0.11 3/22/21SM21-22 6200B1Toluene
ND 1.0 3/22/21 14:39 LBDµg/L0.18 3/22/21SM21-22 6200B1m+p Xylene
ND 0.50 3/22/21 14:39 LBDµg/L0.090 3/22/21SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.0 3/22/21 14:3970-130
Toluene-d8 98.4 3/22/21 14:3970-130
4-Bromofluorobenzene 92.8 3/22/21 14:3970-130
[TOC_1]Sample Results[TOC]
Page 9 of 85
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-01
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.222 4.81 3/26/21 9:42 BGLµg/L0.222 3/24/21625.11Acenaphthene
<0.222 4.81 3/26/21 9:42 BGLµg/L0.222 3/24/21625.11Acenaphthylene
<0.194 4.81 3/26/21 9:42 BGLµg/L0.194 3/24/21625.11Anthracene
<15.8 19.2 3/26/21 9:42 BGLµg/L15.8 3/24/21625.11V-04, V-05, L-04,
R-05, V-34
Benzidine
<0.242 4.81 3/26/21 9:42 BGLµg/L0.242 3/24/21625.11Benzo(a)anthracene
<0.284 4.81 3/26/21 9:42 BGLµg/L0.284 3/24/21625.11Benzo(a)pyrene
<0.243 4.81 3/26/21 9:42 BGLµg/L0.243 3/24/21625.11Benzo(b)fluoranthene
<0.381 4.81 3/26/21 9:42 BGLµg/L0.381 3/24/21625.11Benzo(g,h,i)perylene
<0.267 4.81 3/26/21 9:42 BGLµg/L0.267 3/24/21625.11Benzo(k)fluoranthene
<0.285 9.62 3/26/21 9:42 BGLµg/L0.285 3/24/21625.114-Bromophenylphenylether
<0.284 9.62 3/26/21 9:42 BGLµg/L0.284 3/24/21625.11Butylbenzylphthalate
<0.462 9.62 3/26/21 9:42 BGLµg/L0.462 3/24/21625.114-Chloro-3-methylphenol
<0.453 9.62 3/26/21 9:42 BGLµg/L0.453 3/24/21625.11Bis(2-chloroethoxy)methane
<0.492 9.62 3/26/21 9:42 BGLµg/L0.492 3/24/21625.11Bis(2-chloroethyl)ether
<0.701 9.62 3/26/21 9:42 BGLµg/L0.701 3/24/21625.11Bis(2-chloroisopropyl)ether
<0.437 9.62 3/26/21 9:42 BGLµg/L0.437 3/24/21625.112-Chloronaphthalene
<0.362 9.62 3/26/21 9:42 BGLµg/L0.362 3/24/21625.112-Chlorophenol
<0.302 9.62 3/26/21 9:42 BGLµg/L0.302 3/24/21625.114-Chlorophenylphenylether
<0.209 4.81 3/26/21 9:42 BGLµg/L0.209 3/24/21625.11Chrysene
<0.438 4.81 3/26/21 9:42 BGLµg/L0.438 3/24/21625.11Dibenz(a,h)anthracene
<0.440 9.62 3/26/21 9:42 BGLµg/L0.440 3/24/21625.11Di-n-butylphthalate
<0.445 4.81 3/26/21 9:42 BGLµg/L0.445 3/24/21625.111,3-Dichlorobenzene
<0.368 4.81 3/26/21 9:42 BGLµg/L0.368 3/24/21625.111,4-Dichlorobenzene
<0.441 4.81 3/26/21 9:42 BGLµg/L0.441 3/24/21625.111,2-Dichlorobenzene
<0.345 9.62 3/26/21 9:42 BGLµg/L0.345 3/24/21625.113,3-Dichlorobenzidine
<0.288 9.62 3/26/21 9:42 BGLµg/L0.288 3/24/21625.112,4-Dichlorophenol
<0.216 9.62 3/26/21 9:42 BGLµg/L0.216 3/24/21625.11Diethylphthalate
<0.764 9.62 3/26/21 9:42 BGLµg/L0.764 3/24/21625.112,4-Dimethylphenol
<0.295 9.62 3/26/21 9:42 BGLµg/L0.295 3/24/21625.11Dimethylphthalate
<1.88 9.62 3/26/21 9:42 BGLµg/L1.88 3/24/21625.114,6-Dinitro-2-methylphenol
<1.57 9.62 3/26/21 9:42 BGLµg/L1.57 3/24/21625.112,4-Dinitrophenol
<0.314 9.62 3/26/21 9:42 BGLµg/L0.314 3/24/21625.112,4-Dinitrotoluene
<0.333 9.62 3/26/21 9:42 BGLµg/L0.333 3/24/21625.112,6-Dinitrotoluene
<0.502 9.62 3/26/21 9:42 BGLµg/L0.502 3/24/21625.11Di-n-octylphthalate
<0.361 9.62 3/26/21 9:42 BGLµg/L0.361 3/24/21625.111,2-Diphenylhydrazine/Azobenzene
0.702 9.62 3/26/21 9:42 BGLµg/L0.499 3/24/21625.11JBis(2-Ethylhexyl)phthalate
<0.286 4.81 3/26/21 9:42 BGLµg/L0.286 3/24/21625.11Fluoranthene
<0.236 4.81 3/26/21 9:42 BGLµg/L0.236 3/24/21625.11Fluorene
<0.416 9.62 3/26/21 9:42 BGLµg/L0.416 3/24/21625.11Hexachlorobenzene
<0.569 9.62 3/26/21 9:42 BGLµg/L0.569 3/24/21625.11Hexachlorobutadiene
<4.62 9.62 3/26/21 9:42 BGLµg/L4.62 3/24/21625.11Hexachlorocyclopentadiene
<0.509 9.62 3/26/21 9:42 BGLµg/L0.509 3/24/21625.11Hexachloroethane
<0.494 4.81 3/26/21 9:42 BGLµg/L0.494 3/24/21625.11Indeno(1,2,3-cd)pyrene
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-01
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.288 9.62 3/26/21 9:42 BGLµg/L0.288 3/24/21625.11Isophorone
<0.425 4.81 3/26/21 9:42 BGLµg/L0.425 3/24/21625.11Naphthalene
<0.394 9.62 3/26/21 9:42 BGLµg/L0.394 3/24/21625.11Nitrobenzene
<0.399 9.62 3/26/21 9:42 BGLµg/L0.399 3/24/21625.112-Nitrophenol
<0.603 9.62 3/26/21 9:42 BGLµg/L0.603 3/24/21625.114-Nitrophenol
<1.76 9.62 3/26/21 9:42 BGLµg/L1.76 3/24/21625.11N-Nitrosodimethylamine
<0.283 9.62 3/26/21 9:42 BGLµg/L0.283 3/24/21625.11N-Nitrosodiphenylamine/Diphenylamine
<0.498 9.62 3/26/21 9:42 BGLµg/L0.498 3/24/21625.11N-Nitrosodi-n-propylamine
<0.319 9.62 3/26/21 9:42 BGLµg/L0.319 3/24/21625.11Pentachlorophenol
<0.256 4.81 3/26/21 9:42 BGLµg/L0.256 3/24/21625.112-Methylnaphthalene
<0.276 4.81 3/26/21 9:42 BGLµg/L0.276 3/24/21625.11Phenanthrene
<0.438 9.62 3/26/21 9:42 BGLµg/L0.438 3/24/21625.112-Methylphenol
<0.190 9.62 3/26/21 9:42 BGLµg/L0.190 3/24/21625.11Phenol
<0.196 19.2 3/26/21 9:42 BGLµg/L0.196 3/24/21625.113/4-Methylphenol
<0.245 4.81 3/26/21 9:42 BGLµg/L0.245 3/24/21625.11Pyrene
<0.537 4.81 3/26/21 9:42 BGLµg/L0.537 3/24/21625.111,2,4-Trichlorobenzene
<0.320 9.62 3/26/21 9:42 BGLµg/L0.320 3/24/21625.112,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 54.8 3/26/21 9:4215-110
Phenol-d6 42.7 3/26/21 9:4215-110
Nitrobenzene-d5 85.3 3/26/21 9:4230-130
2-Fluorobiphenyl 88.3 3/26/21 9:4230-130
2,4,6-Tribromophenol 89.9 3/26/21 9:4215-110
p-Terphenyl-d14 118 3/26/21 9:4230-130
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-01
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:35
Analyte MethodResponseDFUnitsRTResults
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)
Date
AnalystAnalyzed
Date/Time
PreparedCAS #Q#
No TICs Found 0.0 µg/L 1 625.1 3/24/21 BGL3/26/21 9:42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-01
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 100 3/29/21 14:41 RDDµg/L 3/25/21MADEP EPH rev 2.11C9-C18 Aliphatics
ND 100 3/29/21 14:41 RDDµg/L 3/25/21MADEP EPH rev 2.11C19-C36 Aliphatics
ND 100 3/29/21 14:41 RDDµg/L 3/25/21MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
ND 100 3/29/21 14:41 RDDµg/L 3/25/21MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)54.4 3/29/21 14:4140-140
o-Terphenyl (OTP)67.1 3/29/21 14:4140-140
2-Bromonaphthalene 77.8 3/29/21 14:4140-140
2-Fluorobiphenyl 102 3/29/21 14:4140-140
Page 13 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-01
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 3/20/21 4:57 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 3/20/21 4:57 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 3/20/21 4:57 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 3/20/21 4:57 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 3/20/21 4:57 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)97.6 3/20/21 4:5770-130
2,5-Dibromotoluene (PID)107 3/20/21 4:5770-130
Page 14 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 12:35
[TOC_2]21C0992-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/22/21 13:48 LBDµg/L0.13 3/22/21SM21-22 6200B1Benzene
ND 0.50 3/22/21 13:48 LBDµg/L0.080 3/22/21SM21-22 6200B1Chlorobenzene
ND 0.50 3/22/21 13:48 LBDµg/L0.10 3/22/21SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/22/21 13:48 LBDµg/L0.090 3/22/21SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/22/21 13:48 LBDµg/L0.11 3/22/21SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/22/21 13:48 LBDµg/L0.090 3/22/21SM21-22 6200B1Ethylbenzene
ND 0.50 3/22/21 13:48 LBDµg/L0.17 3/22/21SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 0.50 3/22/21 13:48 LBDµg/L0.11 3/22/21SM21-22 6200B1Toluene
ND 1.0 3/22/21 13:48 LBDµg/L0.18 3/22/21SM21-22 6200B1m+p Xylene
ND 0.50 3/22/21 13:48 LBDµg/L0.090 3/22/21SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.0 3/22/21 13:4870-130
Toluene-d8 97.5 3/22/21 13:4870-130
4-Bromofluorobenzene 96.2 3/22/21 13:4870-130
Page 15 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 12:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.222 4.81 3/26/21 10:06 BGLµg/L0.222 3/24/21625.11Acenaphthene
<0.222 4.81 3/26/21 10:06 BGLµg/L0.222 3/24/21625.11Acenaphthylene
<0.194 4.81 3/26/21 10:06 BGLµg/L0.194 3/24/21625.11Anthracene
<15.8 19.2 3/26/21 10:06 BGLµg/L15.8 3/24/21625.11L-04, R-05, V-04,
V-05, V-34
Benzidine
<0.242 4.81 3/26/21 10:06 BGLµg/L0.242 3/24/21625.11Benzo(a)anthracene
<0.284 4.81 3/26/21 10:06 BGLµg/L0.284 3/24/21625.11Benzo(a)pyrene
<0.243 4.81 3/26/21 10:06 BGLµg/L0.243 3/24/21625.11Benzo(b)fluoranthene
<0.381 4.81 3/26/21 10:06 BGLµg/L0.381 3/24/21625.11Benzo(g,h,i)perylene
<0.267 4.81 3/26/21 10:06 BGLµg/L0.267 3/24/21625.11Benzo(k)fluoranthene
<0.285 9.62 3/26/21 10:06 BGLµg/L0.285 3/24/21625.114-Bromophenylphenylether
<0.284 9.62 3/26/21 10:06 BGLµg/L0.284 3/24/21625.11Butylbenzylphthalate
<0.462 9.62 3/26/21 10:06 BGLµg/L0.462 3/24/21625.114-Chloro-3-methylphenol
<0.453 9.62 3/26/21 10:06 BGLµg/L0.453 3/24/21625.11Bis(2-chloroethoxy)methane
<0.492 9.62 3/26/21 10:06 BGLµg/L0.492 3/24/21625.11Bis(2-chloroethyl)ether
<0.701 9.62 3/26/21 10:06 BGLµg/L0.701 3/24/21625.11Bis(2-chloroisopropyl)ether
<0.437 9.62 3/26/21 10:06 BGLµg/L0.437 3/24/21625.112-Chloronaphthalene
<0.362 9.62 3/26/21 10:06 BGLµg/L0.362 3/24/21625.112-Chlorophenol
<0.302 9.62 3/26/21 10:06 BGLµg/L0.302 3/24/21625.114-Chlorophenylphenylether
<0.209 4.81 3/26/21 10:06 BGLµg/L0.209 3/24/21625.11Chrysene
<0.438 4.81 3/26/21 10:06 BGLµg/L0.438 3/24/21625.11Dibenz(a,h)anthracene
<0.440 9.62 3/26/21 10:06 BGLµg/L0.440 3/24/21625.11Di-n-butylphthalate
<0.445 4.81 3/26/21 10:06 BGLµg/L0.445 3/24/21625.111,3-Dichlorobenzene
<0.368 4.81 3/26/21 10:06 BGLµg/L0.368 3/24/21625.111,4-Dichlorobenzene
<0.441 4.81 3/26/21 10:06 BGLµg/L0.441 3/24/21625.111,2-Dichlorobenzene
<0.345 9.62 3/26/21 10:06 BGLµg/L0.345 3/24/21625.113,3-Dichlorobenzidine
<0.288 9.62 3/26/21 10:06 BGLµg/L0.288 3/24/21625.112,4-Dichlorophenol
<0.216 9.62 3/26/21 10:06 BGLµg/L0.216 3/24/21625.11Diethylphthalate
<0.764 9.62 3/26/21 10:06 BGLµg/L0.764 3/24/21625.112,4-Dimethylphenol
<0.295 9.62 3/26/21 10:06 BGLµg/L0.295 3/24/21625.11Dimethylphthalate
<1.88 9.62 3/26/21 10:06 BGLµg/L1.88 3/24/21625.114,6-Dinitro-2-methylphenol
<1.57 9.62 3/26/21 10:06 BGLµg/L1.57 3/24/21625.112,4-Dinitrophenol
<0.314 9.62 3/26/21 10:06 BGLµg/L0.314 3/24/21625.112,4-Dinitrotoluene
<0.333 9.62 3/26/21 10:06 BGLµg/L0.333 3/24/21625.112,6-Dinitrotoluene
<0.502 9.62 3/26/21 10:06 BGLµg/L0.502 3/24/21625.11Di-n-octylphthalate
<0.361 9.62 3/26/21 10:06 BGLµg/L0.361 3/24/21625.111,2-Diphenylhydrazine/Azobenzene
<0.499 9.62 3/26/21 10:06 BGLµg/L0.499 3/24/21625.11Bis(2-Ethylhexyl)phthalate
<0.286 4.81 3/26/21 10:06 BGLµg/L0.286 3/24/21625.11Fluoranthene
<0.236 4.81 3/26/21 10:06 BGLµg/L0.236 3/24/21625.11Fluorene
<0.416 9.62 3/26/21 10:06 BGLµg/L0.416 3/24/21625.11Hexachlorobenzene
<0.569 9.62 3/26/21 10:06 BGLµg/L0.569 3/24/21625.11Hexachlorobutadiene
<4.62 9.62 3/26/21 10:06 BGLµg/L4.62 3/24/21625.11Hexachlorocyclopentadiene
<0.509 9.62 3/26/21 10:06 BGLµg/L0.509 3/24/21625.11Hexachloroethane
<0.494 4.81 3/26/21 10:06 BGLµg/L0.494 3/24/21625.11Indeno(1,2,3-cd)pyrene
Page 16 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 12:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.288 9.62 3/26/21 10:06 BGLµg/L0.288 3/24/21625.11Isophorone
<0.425 4.81 3/26/21 10:06 BGLµg/L0.425 3/24/21625.11Naphthalene
<0.394 9.62 3/26/21 10:06 BGLµg/L0.394 3/24/21625.11Nitrobenzene
<0.399 9.62 3/26/21 10:06 BGLµg/L0.399 3/24/21625.112-Nitrophenol
<0.603 9.62 3/26/21 10:06 BGLµg/L0.603 3/24/21625.114-Nitrophenol
<1.76 9.62 3/26/21 10:06 BGLµg/L1.76 3/24/21625.11N-Nitrosodimethylamine
<0.283 9.62 3/26/21 10:06 BGLµg/L0.283 3/24/21625.11N-Nitrosodiphenylamine/Diphenylamine
<0.498 9.62 3/26/21 10:06 BGLµg/L0.498 3/24/21625.11N-Nitrosodi-n-propylamine
<0.319 9.62 3/26/21 10:06 BGLµg/L0.319 3/24/21625.11Pentachlorophenol
<0.256 4.81 3/26/21 10:06 BGLµg/L0.256 3/24/21625.112-Methylnaphthalene
<0.276 4.81 3/26/21 10:06 BGLµg/L0.276 3/24/21625.11Phenanthrene
<0.438 9.62 3/26/21 10:06 BGLµg/L0.438 3/24/21625.112-Methylphenol
<0.190 9.62 3/26/21 10:06 BGLµg/L0.190 3/24/21625.11Phenol
<0.196 19.2 3/26/21 10:06 BGLµg/L0.196 3/24/21625.113/4-Methylphenol
<0.245 4.81 3/26/21 10:06 BGLµg/L0.245 3/24/21625.11Pyrene
<0.537 4.81 3/26/21 10:06 BGLµg/L0.537 3/24/21625.111,2,4-Trichlorobenzene
<0.320 9.62 3/26/21 10:06 BGLµg/L0.320 3/24/21625.112,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 44.0 3/26/21 10:0615-110
Phenol-d6 34.2 3/26/21 10:0615-110
Nitrobenzene-d5 70.4 3/26/21 10:0630-130
2-Fluorobiphenyl 73.7 3/26/21 10:0630-130
2,4,6-Tribromophenol 78.9 3/26/21 10:0615-110
p-Terphenyl-d14 90.2 3/26/21 10:0630-130
Page 17 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 12:35
Analyte MethodResponseDFUnitsRTResults
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)
Date
AnalystAnalyzed
Date/Time
PreparedCAS #Q#
No TICs Found 0.0 µg/L 1 625.1 3/24/21 BGL3/26/21 10:06
Page 18 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 12:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 100 3/29/21 12:59 RDDµg/L 3/25/21MADEP EPH rev 2.11C9-C18 Aliphatics
ND 100 3/29/21 12:59 RDDµg/L 3/25/21MADEP EPH rev 2.11C19-C36 Aliphatics
ND 100 3/29/21 12:59 RDDµg/L 3/25/21MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
ND 100 3/29/21 12:59 RDDµg/L 3/25/21MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)57.6 3/29/21 12:5940-140
o-Terphenyl (OTP)71.5 3/29/21 12:5940-140
2-Bromonaphthalene 78.2 3/29/21 12:5940-140
2-Fluorobiphenyl 102 3/29/21 12:5940-140
Page 19 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 12:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 3/20/21 7:27 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 3/20/21 7:27 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 3/20/21 7:27 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 3/20/21 7:27 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 3/20/21 7:27 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)112 3/20/21 7:2770-130
2,5-Dibromotoluene (PID)119 3/20/21 7:2770-130
Page 20 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:40
[TOC_2]21C0992-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/22/21 15:05 LBDµg/L0.13 3/22/21SM21-22 6200B1Benzene
ND 0.50 3/22/21 15:05 LBDµg/L0.080 3/22/21SM21-22 6200B1Chlorobenzene
ND 0.50 3/22/21 15:05 LBDµg/L0.10 3/22/21SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/22/21 15:05 LBDµg/L0.090 3/22/21SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/22/21 15:05 LBDµg/L0.11 3/22/21SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/22/21 15:05 LBDµg/L0.090 3/22/21SM21-22 6200B1Ethylbenzene
ND 0.50 3/22/21 15:05 LBDµg/L0.17 3/22/21SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 0.50 3/22/21 15:05 LBDµg/L0.11 3/22/21SM21-22 6200B1Toluene
ND 1.0 3/22/21 15:05 LBDµg/L0.18 3/22/21SM21-22 6200B1m+p Xylene
ND 0.50 3/22/21 15:05 LBDµg/L0.090 3/22/21SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.7 3/22/21 15:0570-130
Toluene-d8 97.7 3/22/21 15:0570-130
4-Bromofluorobenzene 92.0 3/22/21 15:0570-130
Page 21 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.222 4.81 3/26/21 10:30 BGLµg/L0.222 3/24/21625.11Acenaphthene
<0.222 4.81 3/26/21 10:30 BGLµg/L0.222 3/24/21625.11Acenaphthylene
<0.194 4.81 3/26/21 10:30 BGLµg/L0.194 3/24/21625.11Anthracene
<15.8 19.2 3/26/21 10:30 BGLµg/L15.8 3/24/21625.11L-04, R-05, V-04,
V-05, V-34
Benzidine
<0.242 4.81 3/26/21 10:30 BGLµg/L0.242 3/24/21625.11Benzo(a)anthracene
<0.284 4.81 3/26/21 10:30 BGLµg/L0.284 3/24/21625.11Benzo(a)pyrene
<0.243 4.81 3/26/21 10:30 BGLµg/L0.243 3/24/21625.11Benzo(b)fluoranthene
<0.381 4.81 3/26/21 10:30 BGLµg/L0.381 3/24/21625.11Benzo(g,h,i)perylene
<0.267 4.81 3/26/21 10:30 BGLµg/L0.267 3/24/21625.11Benzo(k)fluoranthene
<0.285 9.62 3/26/21 10:30 BGLµg/L0.285 3/24/21625.114-Bromophenylphenylether
<0.284 9.62 3/26/21 10:30 BGLµg/L0.284 3/24/21625.11Butylbenzylphthalate
<0.462 9.62 3/26/21 10:30 BGLµg/L0.462 3/24/21625.114-Chloro-3-methylphenol
<0.453 9.62 3/26/21 10:30 BGLµg/L0.453 3/24/21625.11Bis(2-chloroethoxy)methane
<0.492 9.62 3/26/21 10:30 BGLµg/L0.492 3/24/21625.11Bis(2-chloroethyl)ether
<0.701 9.62 3/26/21 10:30 BGLµg/L0.701 3/24/21625.11Bis(2-chloroisopropyl)ether
<0.437 9.62 3/26/21 10:30 BGLµg/L0.437 3/24/21625.112-Chloronaphthalene
<0.362 9.62 3/26/21 10:30 BGLµg/L0.362 3/24/21625.112-Chlorophenol
<0.302 9.62 3/26/21 10:30 BGLµg/L0.302 3/24/21625.114-Chlorophenylphenylether
<0.209 4.81 3/26/21 10:30 BGLµg/L0.209 3/24/21625.11Chrysene
<0.438 4.81 3/26/21 10:30 BGLµg/L0.438 3/24/21625.11Dibenz(a,h)anthracene
<0.440 9.62 3/26/21 10:30 BGLµg/L0.440 3/24/21625.11Di-n-butylphthalate
<0.445 4.81 3/26/21 10:30 BGLµg/L0.445 3/24/21625.111,3-Dichlorobenzene
<0.368 4.81 3/26/21 10:30 BGLµg/L0.368 3/24/21625.111,4-Dichlorobenzene
<0.441 4.81 3/26/21 10:30 BGLµg/L0.441 3/24/21625.111,2-Dichlorobenzene
<0.345 9.62 3/26/21 10:30 BGLµg/L0.345 3/24/21625.113,3-Dichlorobenzidine
<0.288 9.62 3/26/21 10:30 BGLµg/L0.288 3/24/21625.112,4-Dichlorophenol
<0.216 9.62 3/26/21 10:30 BGLµg/L0.216 3/24/21625.11Diethylphthalate
<0.764 9.62 3/26/21 10:30 BGLµg/L0.764 3/24/21625.112,4-Dimethylphenol
<0.295 9.62 3/26/21 10:30 BGLµg/L0.295 3/24/21625.11Dimethylphthalate
<1.88 9.62 3/26/21 10:30 BGLµg/L1.88 3/24/21625.114,6-Dinitro-2-methylphenol
<1.57 9.62 3/26/21 10:30 BGLµg/L1.57 3/24/21625.112,4-Dinitrophenol
<0.314 9.62 3/26/21 10:30 BGLµg/L0.314 3/24/21625.112,4-Dinitrotoluene
<0.333 9.62 3/26/21 10:30 BGLµg/L0.333 3/24/21625.112,6-Dinitrotoluene
<0.502 9.62 3/26/21 10:30 BGLµg/L0.502 3/24/21625.11Di-n-octylphthalate
<0.361 9.62 3/26/21 10:30 BGLµg/L0.361 3/24/21625.111,2-Diphenylhydrazine/Azobenzene
<0.499 9.62 3/26/21 10:30 BGLµg/L0.499 3/24/21625.11Bis(2-Ethylhexyl)phthalate
<0.286 4.81 3/26/21 10:30 BGLµg/L0.286 3/24/21625.11Fluoranthene
<0.236 4.81 3/26/21 10:30 BGLµg/L0.236 3/24/21625.11Fluorene
<0.416 9.62 3/26/21 10:30 BGLµg/L0.416 3/24/21625.11Hexachlorobenzene
<0.569 9.62 3/26/21 10:30 BGLµg/L0.569 3/24/21625.11Hexachlorobutadiene
<4.62 9.62 3/26/21 10:30 BGLµg/L4.62 3/24/21625.11Hexachlorocyclopentadiene
<0.509 9.62 3/26/21 10:30 BGLµg/L0.509 3/24/21625.11Hexachloroethane
<0.494 4.81 3/26/21 10:30 BGLµg/L0.494 3/24/21625.11Indeno(1,2,3-cd)pyrene
Page 22 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.288 9.62 3/26/21 10:30 BGLµg/L0.288 3/24/21625.11Isophorone
<0.425 4.81 3/26/21 10:30 BGLµg/L0.425 3/24/21625.11Naphthalene
<0.394 9.62 3/26/21 10:30 BGLµg/L0.394 3/24/21625.11Nitrobenzene
<0.399 9.62 3/26/21 10:30 BGLµg/L0.399 3/24/21625.112-Nitrophenol
<0.603 9.62 3/26/21 10:30 BGLµg/L0.603 3/24/21625.114-Nitrophenol
<1.76 9.62 3/26/21 10:30 BGLµg/L1.76 3/24/21625.11N-Nitrosodimethylamine
<0.283 9.62 3/26/21 10:30 BGLµg/L0.283 3/24/21625.11N-Nitrosodiphenylamine/Diphenylamine
<0.498 9.62 3/26/21 10:30 BGLµg/L0.498 3/24/21625.11N-Nitrosodi-n-propylamine
<0.319 9.62 3/26/21 10:30 BGLµg/L0.319 3/24/21625.11Pentachlorophenol
<0.256 4.81 3/26/21 10:30 BGLµg/L0.256 3/24/21625.112-Methylnaphthalene
<0.276 4.81 3/26/21 10:30 BGLµg/L0.276 3/24/21625.11Phenanthrene
<0.438 9.62 3/26/21 10:30 BGLµg/L0.438 3/24/21625.112-Methylphenol
<0.190 9.62 3/26/21 10:30 BGLµg/L0.190 3/24/21625.11Phenol
<0.196 19.2 3/26/21 10:30 BGLµg/L0.196 3/24/21625.113/4-Methylphenol
<0.245 4.81 3/26/21 10:30 BGLµg/L0.245 3/24/21625.11Pyrene
<0.537 4.81 3/26/21 10:30 BGLµg/L0.537 3/24/21625.111,2,4-Trichlorobenzene
<0.320 9.62 3/26/21 10:30 BGLµg/L0.320 3/24/21625.112,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 38.9 3/26/21 10:3015-110
Phenol-d6 31.4 3/26/21 10:3015-110
Nitrobenzene-d5 61.3 3/26/21 10:3030-130
2-Fluorobiphenyl 70.0 3/26/21 10:3030-130
2,4,6-Tribromophenol 76.8 3/26/21 10:3015-110
p-Terphenyl-d14 88.9 3/26/21 10:3030-130
Page 23 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:40
Analyte MethodResponseDFUnitsRTResults
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)
Date
AnalystAnalyzed
Date/Time
PreparedCAS #Q#
No TICs Found 0.0 µg/L 1 625.1 3/24/21 BGL3/26/21 10:30
Page 24 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 100 3/26/21 18:38 RDDµg/L 3/25/21MADEP EPH rev 2.11C9-C18 Aliphatics
ND 100 3/26/21 18:38 RDDµg/L 3/25/21MADEP EPH rev 2.11C19-C36 Aliphatics
ND 100 3/26/21 18:38 RDDµg/L 3/25/21MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
ND 100 3/26/21 18:38 RDDµg/L 3/25/21MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)79.5 3/26/21 18:3840-140
o-Terphenyl (OTP)89.9 3/26/21 18:3840-140
2-Bromonaphthalene 110 3/26/21 18:3840-140
2-Fluorobiphenyl 135 3/26/21 18:3840-140
Page 25 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 3/20/21 5:35 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 3/20/21 5:35 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 3/20/21 5:35 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 3/20/21 5:35 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 3/20/21 5:35 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)104 3/20/21 5:3570-130
2,5-Dibromotoluene (PID)116 3/20/21 5:3570-130
Page 26 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-04
Field Sample #: RW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 14:50
[TOC_2]21C0992-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
3.6 0.50 3/22/21 17:41 LBDµg/L0.13 3/22/21SM21-22 6200B1Benzene
ND 0.50 3/22/21 17:41 LBDµg/L0.080 3/22/21SM21-22 6200B1Chlorobenzene
ND 0.50 3/22/21 17:41 LBDµg/L0.10 3/22/21SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/22/21 17:41 LBDµg/L0.090 3/22/21SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/22/21 17:41 LBDµg/L0.11 3/22/21SM21-22 6200B11,4-Dichlorobenzene
2.2 0.50 3/22/21 17:41 LBDµg/L0.090 3/22/21SM21-22 6200B1Ethylbenzene
0.95 0.50 3/22/21 17:41 LBDµg/L0.17 3/22/21SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 0.50 3/22/21 17:41 LBDµg/L0.11 3/22/21SM21-22 6200B1Toluene
1.2 1.0 3/22/21 17:41 LBDµg/L0.18 3/22/21SM21-22 6200B1m+p Xylene
0.17 0.50 3/22/21 17:41 LBDµg/L0.090 3/22/21SM21-22 6200B1Jo-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.6 3/22/21 17:4170-130
Toluene-d8 105 3/22/21 17:4170-130
4-Bromofluorobenzene 93.9 3/22/21 17:4170-130
Page 27 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-04
Field Sample #: RW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 14:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
1.27 4.83 3/26/21 10:53 BGLµg/L0.223 3/24/21625.11JAcenaphthene
<0.223 4.83 3/26/21 10:53 BGLµg/L0.223 3/24/21625.11Acenaphthylene
<0.195 4.83 3/26/21 10:53 BGLµg/L0.195 3/24/21625.11Anthracene
<15.8 19.3 3/26/21 10:53 BGLµg/L15.8 3/24/21625.11L-04, R-05, V-04,
V-05, V-34
Benzidine
<0.243 4.83 3/26/21 10:53 BGLµg/L0.243 3/24/21625.11Benzo(a)anthracene
<0.285 4.83 3/26/21 10:53 BGLµg/L0.285 3/24/21625.11Benzo(a)pyrene
<0.244 4.83 3/26/21 10:53 BGLµg/L0.244 3/24/21625.11Benzo(b)fluoranthene
<0.383 4.83 3/26/21 10:53 BGLµg/L0.383 3/24/21625.11Benzo(g,h,i)perylene
<0.269 4.83 3/26/21 10:53 BGLµg/L0.269 3/24/21625.11Benzo(k)fluoranthene
<0.286 9.66 3/26/21 10:53 BGLµg/L0.286 3/24/21625.114-Bromophenylphenylether
<0.285 9.66 3/26/21 10:53 BGLµg/L0.285 3/24/21625.11Butylbenzylphthalate
<0.465 9.66 3/26/21 10:53 BGLµg/L0.465 3/24/21625.114-Chloro-3-methylphenol
<0.455 9.66 3/26/21 10:53 BGLµg/L0.455 3/24/21625.11Bis(2-chloroethoxy)methane
<0.495 9.66 3/26/21 10:53 BGLµg/L0.495 3/24/21625.11Bis(2-chloroethyl)ether
<0.704 9.66 3/26/21 10:53 BGLµg/L0.704 3/24/21625.11Bis(2-chloroisopropyl)ether
<0.439 9.66 3/26/21 10:53 BGLµg/L0.439 3/24/21625.112-Chloronaphthalene
<0.363 9.66 3/26/21 10:53 BGLµg/L0.363 3/24/21625.112-Chlorophenol
<0.303 9.66 3/26/21 10:53 BGLµg/L0.303 3/24/21625.114-Chlorophenylphenylether
<0.210 4.83 3/26/21 10:53 BGLµg/L0.210 3/24/21625.11Chrysene
<0.440 4.83 3/26/21 10:53 BGLµg/L0.440 3/24/21625.11Dibenz(a,h)anthracene
<0.443 9.66 3/26/21 10:53 BGLµg/L0.443 3/24/21625.11Di-n-butylphthalate
<0.447 4.83 3/26/21 10:53 BGLµg/L0.447 3/24/21625.111,3-Dichlorobenzene
<0.370 4.83 3/26/21 10:53 BGLµg/L0.370 3/24/21625.111,4-Dichlorobenzene
<0.443 4.83 3/26/21 10:53 BGLµg/L0.443 3/24/21625.111,2-Dichlorobenzene
<0.347 9.66 3/26/21 10:53 BGLµg/L0.347 3/24/21625.113,3-Dichlorobenzidine
<0.290 9.66 3/26/21 10:53 BGLµg/L0.290 3/24/21625.112,4-Dichlorophenol
<0.217 9.66 3/26/21 10:53 BGLµg/L0.217 3/24/21625.11Diethylphthalate
<0.768 9.66 3/26/21 10:53 BGLµg/L0.768 3/24/21625.112,4-Dimethylphenol
<0.297 9.66 3/26/21 10:53 BGLµg/L0.297 3/24/21625.11Dimethylphthalate
<1.88 9.66 3/26/21 10:53 BGLµg/L1.88 3/24/21625.114,6-Dinitro-2-methylphenol
<1.57 9.66 3/26/21 10:53 BGLµg/L1.57 3/24/21625.112,4-Dinitrophenol
<0.316 9.66 3/26/21 10:53 BGLµg/L0.316 3/24/21625.112,4-Dinitrotoluene
<0.334 9.66 3/26/21 10:53 BGLµg/L0.334 3/24/21625.112,6-Dinitrotoluene
<0.504 9.66 3/26/21 10:53 BGLµg/L0.504 3/24/21625.11Di-n-octylphthalate
<0.362 9.66 3/26/21 10:53 BGLµg/L0.362 3/24/21625.111,2-Diphenylhydrazine/Azobenzene
<0.501 9.66 3/26/21 10:53 BGLµg/L0.501 3/24/21625.11Bis(2-Ethylhexyl)phthalate
<0.287 4.83 3/26/21 10:53 BGLµg/L0.287 3/24/21625.11Fluoranthene
1.92 4.83 3/26/21 10:53 BGLµg/L0.237 3/24/21625.11JFluorene
<0.418 9.66 3/26/21 10:53 BGLµg/L0.418 3/24/21625.11Hexachlorobenzene
<0.572 9.66 3/26/21 10:53 BGLµg/L0.572 3/24/21625.11Hexachlorobutadiene
<4.64 9.66 3/26/21 10:53 BGLµg/L4.64 3/24/21625.11Hexachlorocyclopentadiene
<0.511 9.66 3/26/21 10:53 BGLµg/L0.511 3/24/21625.11Hexachloroethane
<0.497 4.83 3/26/21 10:53 BGLµg/L0.497 3/24/21625.11Indeno(1,2,3-cd)pyrene
Page 28 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-04
Field Sample #: RW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 14:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.290 9.66 3/26/21 10:53 BGLµg/L0.290 3/24/21625.11Isophorone
13.6 4.83 3/26/21 10:53 BGLµg/L0.427 3/24/21625.11Naphthalene
<0.396 9.66 3/26/21 10:53 BGLµg/L0.396 3/24/21625.11Nitrobenzene
<0.401 9.66 3/26/21 10:53 BGLµg/L0.401 3/24/21625.112-Nitrophenol
<0.606 9.66 3/26/21 10:53 BGLµg/L0.606 3/24/21625.114-Nitrophenol
<1.77 9.66 3/26/21 10:53 BGLµg/L1.77 3/24/21625.11N-Nitrosodimethylamine
<0.284 9.66 3/26/21 10:53 BGLµg/L0.284 3/24/21625.11N-Nitrosodiphenylamine/Diphenylamine
<0.500 9.66 3/26/21 10:53 BGLµg/L0.500 3/24/21625.11N-Nitrosodi-n-propylamine
<0.321 9.66 3/26/21 10:53 BGLµg/L0.321 3/24/21625.11Pentachlorophenol
19.2 4.83 3/26/21 10:53 BGLµg/L0.257 3/24/21625.112-Methylnaphthalene
1.69 4.83 3/26/21 10:53 BGLµg/L0.277 3/24/21625.11JPhenanthrene
<0.441 9.66 3/26/21 10:53 BGLµg/L0.441 3/24/21625.112-Methylphenol
<0.191 9.66 3/26/21 10:53 BGLµg/L0.191 3/24/21625.11Phenol
<0.197 19.3 3/26/21 10:53 BGLµg/L0.197 3/24/21625.113/4-Methylphenol
0.570 4.83 3/26/21 10:53 BGLµg/L0.246 3/24/21625.11JPyrene
<0.539 4.83 3/26/21 10:53 BGLµg/L0.539 3/24/21625.111,2,4-Trichlorobenzene
1.01 9.66 3/26/21 10:53 BGLµg/L0.322 3/24/21625.11J2,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 36.3 3/26/21 10:5315-110
Phenol-d6 30.4 3/26/21 10:5315-110
Nitrobenzene-d5 60.9 3/26/21 10:5330-130
2-Fluorobiphenyl 66.9 3/26/21 10:5330-130
2,4,6-Tribromophenol 90.9 3/26/21 10:5315-110
p-Terphenyl-d14 82.3 3/26/21 10:5330-130
Page 29 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-04
Field Sample #: RW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 14:50
Analyte MethodResponseDFUnitsRTResults
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)
Date
AnalystAnalyzed
Date/Time
PreparedCAS #Q#
1H-Indene, 2,3-dihydro-1,2-...8.8 µg/L 14.40589071 017057-82-8 625.1 3/24/21 BGL3/26/21 10:5393
1-Phenyl-1-butene 25 µg/L 14.02253374 000824-90-8 625.1 3/24/21 BGL3/26/21 10:5393
Benzene, 1,2,4,5-tetramethyl-7.9 µg/L 13.88379867 000095-93-2 625.1 3/24/21 BGL3/26/21 10:5397
Benzene, 1-ethyl-2,3-dimethyl-5.2 µg/L 13.81852622 000933-98-2 625.1 3/24/21 BGL3/26/21 10:5395
Indane 6.7 µg/L 13.54546844 000496-11-7 625.1 3/24/21 BGL3/26/21 10:5391
Mesitylacetic acid 8.0 µg/L 15.41497137 004408-60-0 625.1 3/24/21 BGL3/26/21 10:5386
Naphthalene, 1,2,3,4-tetrah... (01)17 µg/L 14.085167631 000119-64-2 625.1 3/24/21 BGL3/26/21 10:5393
Naphthalene, 1,2,3,4-tetrah... (02)8.2 µg/L 14.32483676 001559-81-5 625.1 3/24/21 BGL3/26/21 10:5396
Naphthalene, 2,3,6-trimethyl-7.1 µg/L 15.45186298 000829-26-5 625.1 3/24/21 BGL3/26/21 10:5384
Page 30 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-04
Field Sample #: RW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 14:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
280 100 3/26/21 18:59 RDDµg/L 3/25/21MADEP EPH rev 2.11C9-C18 Aliphatics
200 100 3/26/21 18:59 RDDµg/L 3/25/21MADEP EPH rev 2.11C19-C36 Aliphatics
750 100 3/26/21 18:59 RDDµg/L 3/25/21MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
700 100 3/26/21 18:59 RDDµg/L 3/25/21MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)75.5 3/26/21 18:5940-140
o-Terphenyl (OTP)88.0 3/26/21 18:5940-140
2-Bromonaphthalene 109 3/26/21 18:5940-140
2-Fluorobiphenyl 140 3/26/21 18:5940-140
Page 31 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-04
Field Sample #: RW-3
Sample Matrix: Ground Water
Sampled: 3/17/2021 14:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 3/20/21 15:30 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 3/20/21 15:30 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
360 100 3/20/21 15:30 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 3/20/21 15:30 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
290 100 3/20/21 15:30 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)125 3/20/21 15:3070-130
2,5-Dibromotoluene (PID)160 3/20/21 15:30*S-1570-130
Page 32 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-05
Field Sample #: RW-4
Sample Matrix: Ground Water
Sampled: 3/17/2021 09:55
[TOC_2]21C0992-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
10 0.50 3/22/21 18:07 LBDµg/L0.13 3/22/21SM21-22 6200B1Benzene
ND 0.50 3/22/21 18:07 LBDµg/L0.080 3/22/21SM21-22 6200B1Chlorobenzene
ND 0.50 3/22/21 18:07 LBDµg/L0.10 3/22/21SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/22/21 18:07 LBDµg/L0.090 3/22/21SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/22/21 18:07 LBDµg/L0.11 3/22/21SM21-22 6200B11,4-Dichlorobenzene
9.5 0.50 3/22/21 18:07 LBDµg/L0.090 3/22/21SM21-22 6200B1Ethylbenzene
2.1 0.50 3/22/21 18:07 LBDµg/L0.17 3/22/21SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
0.13 0.50 3/22/21 18:07 LBDµg/L0.11 3/22/21SM21-22 6200B1JToluene
4.8 1.0 3/22/21 18:07 LBDµg/L0.18 3/22/21SM21-22 6200B1m+p Xylene
0.32 0.50 3/22/21 18:07 LBDµg/L0.090 3/22/21SM21-22 6200B1Jo-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.4 3/22/21 18:0770-130
Toluene-d8 96.9 3/22/21 18:0770-130
4-Bromofluorobenzene 89.2 3/22/21 18:0770-130
Page 33 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-05
Field Sample #: RW-4
Sample Matrix: Ground Water
Sampled: 3/17/2021 09:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
1.59 4.85 3/26/21 11:17 BGLµg/L0.224 3/24/21625.11JAcenaphthene
<0.224 4.85 3/26/21 11:17 BGLµg/L0.224 3/24/21625.11Acenaphthylene
<0.196 4.85 3/26/21 11:17 BGLµg/L0.196 3/24/21625.11Anthracene
<15.9 19.4 3/26/21 11:17 BGLµg/L15.9 3/24/21625.11L-04, R-05, V-04,
V-05, V-34
Benzidine
<0.245 4.85 3/26/21 11:17 BGLµg/L0.245 3/24/21625.11Benzo(a)anthracene
<0.286 4.85 3/26/21 11:17 BGLµg/L0.286 3/24/21625.11Benzo(a)pyrene
<0.246 4.85 3/26/21 11:17 BGLµg/L0.246 3/24/21625.11Benzo(b)fluoranthene
<0.384 4.85 3/26/21 11:17 BGLµg/L0.384 3/24/21625.11Benzo(g,h,i)perylene
<0.270 4.85 3/26/21 11:17 BGLµg/L0.270 3/24/21625.11Benzo(k)fluoranthene
<0.287 9.71 3/26/21 11:17 BGLµg/L0.287 3/24/21625.114-Bromophenylphenylether
<0.286 9.71 3/26/21 11:17 BGLµg/L0.286 3/24/21625.11Butylbenzylphthalate
<0.467 9.71 3/26/21 11:17 BGLµg/L0.467 3/24/21625.114-Chloro-3-methylphenol
<0.457 9.71 3/26/21 11:17 BGLµg/L0.457 3/24/21625.11Bis(2-chloroethoxy)methane
<0.497 9.71 3/26/21 11:17 BGLµg/L0.497 3/24/21625.11Bis(2-chloroethyl)ether
<0.708 9.71 3/26/21 11:17 BGLµg/L0.708 3/24/21625.11Bis(2-chloroisopropyl)ether
<0.441 9.71 3/26/21 11:17 BGLµg/L0.441 3/24/21625.112-Chloronaphthalene
<0.365 9.71 3/26/21 11:17 BGLµg/L0.365 3/24/21625.112-Chlorophenol
<0.305 9.71 3/26/21 11:17 BGLµg/L0.305 3/24/21625.114-Chlorophenylphenylether
<0.211 4.85 3/26/21 11:17 BGLµg/L0.211 3/24/21625.11Chrysene
<0.442 4.85 3/26/21 11:17 BGLµg/L0.442 3/24/21625.11Dibenz(a,h)anthracene
<0.445 9.71 3/26/21 11:17 BGLµg/L0.445 3/24/21625.11Di-n-butylphthalate
<0.450 4.85 3/26/21 11:17 BGLµg/L0.450 3/24/21625.111,3-Dichlorobenzene
<0.372 4.85 3/26/21 11:17 BGLµg/L0.372 3/24/21625.111,4-Dichlorobenzene
<0.446 4.85 3/26/21 11:17 BGLµg/L0.446 3/24/21625.111,2-Dichlorobenzene
<0.349 9.71 3/26/21 11:17 BGLµg/L0.349 3/24/21625.113,3-Dichlorobenzidine
<0.291 9.71 3/26/21 11:17 BGLµg/L0.291 3/24/21625.112,4-Dichlorophenol
<0.218 9.71 3/26/21 11:17 BGLµg/L0.218 3/24/21625.11Diethylphthalate
0.913 9.71 3/26/21 11:17 BGLµg/L0.772 3/24/21625.11J2,4-Dimethylphenol
<0.298 9.71 3/26/21 11:17 BGLµg/L0.298 3/24/21625.11Dimethylphthalate
<1.89 9.71 3/26/21 11:17 BGLµg/L1.89 3/24/21625.114,6-Dinitro-2-methylphenol
<1.58 9.71 3/26/21 11:17 BGLµg/L1.58 3/24/21625.112,4-Dinitrophenol
<0.317 9.71 3/26/21 11:17 BGLµg/L0.317 3/24/21625.112,4-Dinitrotoluene
<0.336 9.71 3/26/21 11:17 BGLµg/L0.336 3/24/21625.112,6-Dinitrotoluene
<0.507 9.71 3/26/21 11:17 BGLµg/L0.507 3/24/21625.11Di-n-octylphthalate
<0.364 9.71 3/26/21 11:17 BGLµg/L0.364 3/24/21625.111,2-Diphenylhydrazine/Azobenzene
<0.504 9.71 3/26/21 11:17 BGLµg/L0.504 3/24/21625.11Bis(2-Ethylhexyl)phthalate
<0.288 4.85 3/26/21 11:17 BGLµg/L0.288 3/24/21625.11Fluoranthene
3.31 4.85 3/26/21 11:17 BGLµg/L0.238 3/24/21625.11JFluorene
<0.420 9.71 3/26/21 11:17 BGLµg/L0.420 3/24/21625.11Hexachlorobenzene
<0.575 9.71 3/26/21 11:17 BGLµg/L0.575 3/24/21625.11Hexachlorobutadiene
<4.66 9.71 3/26/21 11:17 BGLµg/L4.66 3/24/21625.11Hexachlorocyclopentadiene
<0.514 9.71 3/26/21 11:17 BGLµg/L0.514 3/24/21625.11Hexachloroethane
<0.499 4.85 3/26/21 11:17 BGLµg/L0.499 3/24/21625.11Indeno(1,2,3-cd)pyrene
Page 34 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-05
Field Sample #: RW-4
Sample Matrix: Ground Water
Sampled: 3/17/2021 09:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.291 9.71 3/26/21 11:17 BGLµg/L0.291 3/24/21625.11Isophorone
39.8 4.85 3/26/21 11:17 BGLµg/L0.429 3/24/21625.11Naphthalene
<0.398 9.71 3/26/21 11:17 BGLµg/L0.398 3/24/21625.11Nitrobenzene
<0.403 9.71 3/26/21 11:17 BGLµg/L0.403 3/24/21625.112-Nitrophenol
<0.609 9.71 3/26/21 11:17 BGLµg/L0.609 3/24/21625.114-Nitrophenol
<1.78 9.71 3/26/21 11:17 BGLµg/L1.78 3/24/21625.11N-Nitrosodimethylamine
<0.285 9.71 3/26/21 11:17 BGLµg/L0.285 3/24/21625.11N-Nitrosodiphenylamine/Diphenylamine
<0.503 9.71 3/26/21 11:17 BGLµg/L0.503 3/24/21625.11N-Nitrosodi-n-propylamine
<0.322 9.71 3/26/21 11:17 BGLµg/L0.322 3/24/21625.11Pentachlorophenol
45.3 4.85 3/26/21 11:17 BGLµg/L0.258 3/24/21625.112-Methylnaphthalene
3.02 4.85 3/26/21 11:17 BGLµg/L0.279 3/24/21625.11JPhenanthrene
0.573 9.71 3/26/21 11:17 BGLµg/L0.443 3/24/21625.11J2-Methylphenol
0.388 9.71 3/26/21 11:17 BGLµg/L0.192 3/24/21625.11JPhenol
0.544 19.4 3/26/21 11:17 BGLµg/L0.198 3/24/21625.11J3/4-Methylphenol
0.563 4.85 3/26/21 11:17 BGLµg/L0.248 3/24/21625.11JPyrene
<0.542 4.85 3/26/21 11:17 BGLµg/L0.542 3/24/21625.111,2,4-Trichlorobenzene
1.19 9.71 3/26/21 11:17 BGLµg/L0.323 3/24/21625.11J2,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 35.4 3/26/21 11:1715-110
Phenol-d6 28.5 3/26/21 11:1715-110
Nitrobenzene-d5 62.4 3/26/21 11:1730-130
2-Fluorobiphenyl 57.9 3/26/21 11:1730-130
2,4,6-Tribromophenol 78.6 3/26/21 11:1715-110
p-Terphenyl-d14 80.4 3/26/21 11:1730-130
Page 35 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-05
Field Sample #: RW-4
Sample Matrix: Ground Water
Sampled: 3/17/2021 09:55
Analyte MethodResponseDFUnitsRTResults
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)
Date
AnalystAnalyzed
Date/Time
PreparedCAS #Q#
.beta.-Naphthaleneacetic acid 17 µg/L 16.143140549 000581-96-4 625.1 3/24/21 BGL3/26/21 11:1793
1H-Indene, 2,3-dihydro-4,7-...23 µg/L 14.408249495 006682-71-9 625.1 3/24/21 BGL3/26/21 11:1796
3-Pentenoic acid, 4-phenyl-110 µg/L 15.867888090 053774-19-9 625.1 3/24/21 BGL3/26/21 11:1790
Benzene, 1,2,3-trimethyl-20 µg/L 13.346138365 000526-73-8 625.1 3/24/21 BGL3/26/21 11:1795
Benzene, 1,2,4,5-tetramethyl-13 µg/L 13.883140552 000095-93-2 625.1 3/24/21 BGL3/26/21 11:1797
Naphthalene, 1,2,3,4-tetrah... (01)39 µg/L 14.085422865 000119-64-2 625.1 3/24/21 BGL3/26/21 11:1797
Naphthalene, 1,2,3,4-tetrah... (02)14 µg/L 14.296148110 003877-19-8 625.1 3/24/21 BGL3/26/21 11:1790
Page 36 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-05
Field Sample #: RW-4
Sample Matrix: Ground Water
Sampled: 3/17/2021 09:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
370 100 3/26/21 19:19 RDDµg/L 3/25/21MADEP EPH rev 2.11C9-C18 Aliphatics
220 100 3/26/21 19:19 RDDµg/L 3/25/21MADEP EPH rev 2.11C19-C36 Aliphatics
1100 100 3/26/21 19:19 RDDµg/L 3/25/21MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
950 100 3/26/21 19:19 RDDµg/L 3/25/21MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)69.3 3/26/21 19:1940-140
o-Terphenyl (OTP)79.3 3/26/21 19:1940-140
2-Bromonaphthalene 106 3/26/21 19:1940-140
2-Fluorobiphenyl 138 3/26/21 19:1940-140
Page 37 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-05
Field Sample #: RW-4
Sample Matrix: Ground Water
Sampled: 3/17/2021 09:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 3/20/21 16:07 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 3/20/21 16:07 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
660 100 3/20/21 16:07 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 3/20/21 16:07 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
580 100 3/20/21 16:07 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)117 3/20/21 16:0770-130
2,5-Dibromotoluene (PID)144 3/20/21 16:07*S-1570-130
Page 38 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-06
Field Sample #: RW-5
Sample Matrix: Ground Water
Sampled: 3/17/2021 10:55
[TOC_2]21C0992-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
5.4 0.50 3/22/21 15:32 LBDµg/L0.13 3/22/21SM21-22 6200B1Benzene
ND 0.50 3/22/21 15:32 LBDµg/L0.080 3/22/21SM21-22 6200B1Chlorobenzene
ND 0.50 3/22/21 15:32 LBDµg/L0.10 3/22/21SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/22/21 15:32 LBDµg/L0.090 3/22/21SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/22/21 15:32 LBDµg/L0.11 3/22/21SM21-22 6200B11,4-Dichlorobenzene
8.0 0.50 3/22/21 15:32 LBDµg/L0.090 3/22/21SM21-22 6200B1Ethylbenzene
0.39 0.50 3/22/21 15:32 LBDµg/L0.17 3/22/21SM21-22 6200B1JMethyl tert-Butyl Ether (MTBE)
ND 0.50 3/22/21 15:32 LBDµg/L0.11 3/22/21SM21-22 6200B1Toluene
2.2 1.0 3/22/21 15:32 LBDµg/L0.18 3/22/21SM21-22 6200B1m+p Xylene
ND 0.50 3/22/21 15:32 LBDµg/L0.090 3/22/21SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 96.3 3/22/21 15:3270-130
Toluene-d8 97.7 3/22/21 15:3270-130
4-Bromofluorobenzene 97.2 3/22/21 15:3270-130
Page 39 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-06
Field Sample #: RW-5
Sample Matrix: Ground Water
Sampled: 3/17/2021 10:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
0.476 4.85 3/26/21 11:41 BGLµg/L0.224 3/24/21625.11JAcenaphthene
<0.224 4.85 3/26/21 11:41 BGLµg/L0.224 3/24/21625.11Acenaphthylene
<0.196 4.85 3/26/21 11:41 BGLµg/L0.196 3/24/21625.11Anthracene
<15.9 19.4 3/26/21 11:41 BGLµg/L15.9 3/24/21625.11L-04, R-05, V-04,
V-05, V-34
Benzidine
<0.245 4.85 3/26/21 11:41 BGLµg/L0.245 3/24/21625.11Benzo(a)anthracene
<0.286 4.85 3/26/21 11:41 BGLµg/L0.286 3/24/21625.11Benzo(a)pyrene
<0.246 4.85 3/26/21 11:41 BGLµg/L0.246 3/24/21625.11Benzo(b)fluoranthene
<0.384 4.85 3/26/21 11:41 BGLµg/L0.384 3/24/21625.11Benzo(g,h,i)perylene
<0.270 4.85 3/26/21 11:41 BGLµg/L0.270 3/24/21625.11Benzo(k)fluoranthene
<0.287 9.71 3/26/21 11:41 BGLµg/L0.287 3/24/21625.114-Bromophenylphenylether
<0.286 9.71 3/26/21 11:41 BGLµg/L0.286 3/24/21625.11Butylbenzylphthalate
<0.467 9.71 3/26/21 11:41 BGLµg/L0.467 3/24/21625.114-Chloro-3-methylphenol
<0.457 9.71 3/26/21 11:41 BGLµg/L0.457 3/24/21625.11Bis(2-chloroethoxy)methane
<0.497 9.71 3/26/21 11:41 BGLµg/L0.497 3/24/21625.11Bis(2-chloroethyl)ether
<0.708 9.71 3/26/21 11:41 BGLµg/L0.708 3/24/21625.11Bis(2-chloroisopropyl)ether
<0.441 9.71 3/26/21 11:41 BGLµg/L0.441 3/24/21625.112-Chloronaphthalene
<0.365 9.71 3/26/21 11:41 BGLµg/L0.365 3/24/21625.112-Chlorophenol
<0.305 9.71 3/26/21 11:41 BGLµg/L0.305 3/24/21625.114-Chlorophenylphenylether
<0.211 4.85 3/26/21 11:41 BGLµg/L0.211 3/24/21625.11Chrysene
<0.442 4.85 3/26/21 11:41 BGLµg/L0.442 3/24/21625.11Dibenz(a,h)anthracene
<0.445 9.71 3/26/21 11:41 BGLµg/L0.445 3/24/21625.11Di-n-butylphthalate
<0.450 4.85 3/26/21 11:41 BGLµg/L0.450 3/24/21625.111,3-Dichlorobenzene
<0.372 4.85 3/26/21 11:41 BGLµg/L0.372 3/24/21625.111,4-Dichlorobenzene
<0.446 4.85 3/26/21 11:41 BGLµg/L0.446 3/24/21625.111,2-Dichlorobenzene
<0.349 9.71 3/26/21 11:41 BGLµg/L0.349 3/24/21625.113,3-Dichlorobenzidine
<0.291 9.71 3/26/21 11:41 BGLµg/L0.291 3/24/21625.112,4-Dichlorophenol
<0.218 9.71 3/26/21 11:41 BGLµg/L0.218 3/24/21625.11Diethylphthalate
<0.772 9.71 3/26/21 11:41 BGLµg/L0.772 3/24/21625.112,4-Dimethylphenol
<0.298 9.71 3/26/21 11:41 BGLµg/L0.298 3/24/21625.11Dimethylphthalate
<1.89 9.71 3/26/21 11:41 BGLµg/L1.89 3/24/21625.114,6-Dinitro-2-methylphenol
<1.58 9.71 3/26/21 11:41 BGLµg/L1.58 3/24/21625.112,4-Dinitrophenol
<0.317 9.71 3/26/21 11:41 BGLµg/L0.317 3/24/21625.112,4-Dinitrotoluene
<0.336 9.71 3/26/21 11:41 BGLµg/L0.336 3/24/21625.112,6-Dinitrotoluene
<0.507 9.71 3/26/21 11:41 BGLµg/L0.507 3/24/21625.11Di-n-octylphthalate
<0.364 9.71 3/26/21 11:41 BGLµg/L0.364 3/24/21625.111,2-Diphenylhydrazine/Azobenzene
<0.504 9.71 3/26/21 11:41 BGLµg/L0.504 3/24/21625.11Bis(2-Ethylhexyl)phthalate
<0.288 4.85 3/26/21 11:41 BGLµg/L0.288 3/24/21625.11Fluoranthene
1.34 4.85 3/26/21 11:41 BGLµg/L0.238 3/24/21625.11JFluorene
<0.420 9.71 3/26/21 11:41 BGLµg/L0.420 3/24/21625.11Hexachlorobenzene
<0.575 9.71 3/26/21 11:41 BGLµg/L0.575 3/24/21625.11Hexachlorobutadiene
<4.66 9.71 3/26/21 11:41 BGLµg/L4.66 3/24/21625.11Hexachlorocyclopentadiene
<0.514 9.71 3/26/21 11:41 BGLµg/L0.514 3/24/21625.11Hexachloroethane
<0.499 4.85 3/26/21 11:41 BGLµg/L0.499 3/24/21625.11Indeno(1,2,3-cd)pyrene
Page 40 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-06
Field Sample #: RW-5
Sample Matrix: Ground Water
Sampled: 3/17/2021 10:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.291 9.71 3/26/21 11:41 BGLµg/L0.291 3/24/21625.11Isophorone
8.73 4.85 3/26/21 11:41 BGLµg/L0.429 3/24/21625.11Naphthalene
<0.398 9.71 3/26/21 11:41 BGLµg/L0.398 3/24/21625.11Nitrobenzene
<0.403 9.71 3/26/21 11:41 BGLµg/L0.403 3/24/21625.112-Nitrophenol
<0.609 9.71 3/26/21 11:41 BGLµg/L0.609 3/24/21625.114-Nitrophenol
<1.78 9.71 3/26/21 11:41 BGLµg/L1.78 3/24/21625.11N-Nitrosodimethylamine
<0.285 9.71 3/26/21 11:41 BGLµg/L0.285 3/24/21625.11N-Nitrosodiphenylamine/Diphenylamine
<0.503 9.71 3/26/21 11:41 BGLµg/L0.503 3/24/21625.11N-Nitrosodi-n-propylamine
<0.322 9.71 3/26/21 11:41 BGLµg/L0.322 3/24/21625.11Pentachlorophenol
5.85 4.85 3/26/21 11:41 BGLµg/L0.258 3/24/21625.112-Methylnaphthalene
1.03 4.85 3/26/21 11:41 BGLµg/L0.279 3/24/21625.11JPhenanthrene
<0.443 9.71 3/26/21 11:41 BGLµg/L0.443 3/24/21625.112-Methylphenol
<0.192 9.71 3/26/21 11:41 BGLµg/L0.192 3/24/21625.11Phenol
<0.198 19.4 3/26/21 11:41 BGLµg/L0.198 3/24/21625.113/4-Methylphenol
<0.248 4.85 3/26/21 11:41 BGLµg/L0.248 3/24/21625.11Pyrene
<0.542 4.85 3/26/21 11:41 BGLµg/L0.542 3/24/21625.111,2,4-Trichlorobenzene
<0.323 9.71 3/26/21 11:41 BGLµg/L0.323 3/24/21625.112,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 36.4 3/26/21 11:4115-110
Phenol-d6 31.8 3/26/21 11:4115-110
Nitrobenzene-d5 61.3 3/26/21 11:4130-130
2-Fluorobiphenyl 70.5 3/26/21 11:4130-130
2,4,6-Tribromophenol 82.7 3/26/21 11:4115-110
p-Terphenyl-d14 87.7 3/26/21 11:4130-130
Page 41 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-06
Field Sample #: RW-5
Sample Matrix: Ground Water
Sampled: 3/17/2021 10:55
Analyte MethodResponseDFUnitsRTResults
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)
Date
AnalystAnalyzed
Date/Time
PreparedCAS #Q#
1H-Indene, 2,3-dihydro-4-me...11 µg/L 14.0289427 000824-22-6 625.1 3/24/21 BGL3/26/21 11:4193
Benzene, 1,2,3,4-tetramethyl-4.0 µg/L 13.88332482 000488-23-3 625.1 3/24/21 BGL3/26/21 11:4195
Biphenyl 4.0 µg/L 14.89236901 000092-52-4 625.1 3/24/21 BGL3/26/21 11:4193
Indane 7.7 µg/L 13.54544081 000496-11-7 625.1 3/24/21 BGL3/26/21 11:4191
Naphthalene, 1,2,3,4-tetrah... (01)7.3 µg/L 14.08559777 000119-64-2 625.1 3/24/21 BGL3/26/21 11:4197
Naphthalene, 1,2,3,4-tetrah... (02)5.9 µg/L 14.48247999 001680-51-9 625.1 3/24/21 BGL3/26/21 11:4198
Naphthalene, 1,8-dimethyl-8.7 µg/L 15.04180083 000569-41-5 625.1 3/24/21 BGL3/26/21 11:4198
Page 42 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-06
Field Sample #: RW-5
Sample Matrix: Ground Water
Sampled: 3/17/2021 10:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 100 3/29/21 13:20 RDDµg/L 3/25/21MADEP EPH rev 2.11C9-C18 Aliphatics
ND 100 3/29/21 13:20 RDDµg/L 3/25/21MADEP EPH rev 2.11C19-C36 Aliphatics
230 100 3/29/21 13:20 RDDµg/L 3/25/21MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
210 100 3/29/21 13:20 RDDµg/L 3/25/21MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)52.5 3/29/21 13:2040-140
o-Terphenyl (OTP)61.7 3/29/21 13:2040-140
2-Bromonaphthalene 62.4 3/29/21 13:2040-140
2-Fluorobiphenyl 88.3 3/29/21 13:2040-140
Page 43 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-06
Field Sample #: RW-5
Sample Matrix: Ground Water
Sampled: 3/17/2021 10:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 3/20/21 6:12 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 3/20/21 6:12 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
220 100 3/20/21 6:12 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 3/20/21 6:12 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
190 100 3/20/21 6:12 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)120 3/20/21 6:1270-130
2,5-Dibromotoluene (PID)137 3/20/21 6:12*S-1570-130
Page 44 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-07
Field Sample #: RW-6
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:55
[TOC_2]21C0992-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
6.1 0.50 3/22/21 18:59 LBDµg/L0.13 3/22/21SM21-22 6200B1Benzene
ND 0.50 3/22/21 18:59 LBDµg/L0.080 3/22/21SM21-22 6200B1Chlorobenzene
ND 0.50 3/22/21 18:59 LBDµg/L0.10 3/22/21SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/22/21 18:59 LBDµg/L0.090 3/22/21SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/22/21 18:59 LBDµg/L0.11 3/22/21SM21-22 6200B11,4-Dichlorobenzene
11 0.50 3/22/21 18:59 LBDµg/L0.090 3/22/21SM21-22 6200B1Ethylbenzene
ND 0.50 3/22/21 18:59 LBDµg/L0.17 3/22/21SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
0.12 0.50 3/22/21 18:59 LBDµg/L0.11 3/22/21SM21-22 6200B1JToluene
20 1.0 3/22/21 18:59 LBDµg/L0.18 3/22/21SM21-22 6200B1m+p Xylene
2.8 0.50 3/22/21 18:59 LBDµg/L0.090 3/22/21SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.4 3/22/21 18:5970-130
Toluene-d8 97.4 3/22/21 18:5970-130
4-Bromofluorobenzene 97.7 3/22/21 18:5970-130
Page 45 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-07
Field Sample #: RW-6
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
1.37 4.88 3/26/21 12:05 BGLµg/L0.225 3/24/21625.11JAcenaphthene
<0.225 4.88 3/26/21 12:05 BGLµg/L0.225 3/24/21625.11Acenaphthylene
<0.197 4.88 3/26/21 12:05 BGLµg/L0.197 3/24/21625.11Anthracene
<16.0 19.5 3/26/21 12:05 BGLµg/L16.0 3/24/21625.11L-04, R-05, V-04,
V-05, V-34
Benzidine
<0.246 4.88 3/26/21 12:05 BGLµg/L0.246 3/24/21625.11Benzo(a)anthracene
<0.288 4.88 3/26/21 12:05 BGLµg/L0.288 3/24/21625.11Benzo(a)pyrene
<0.247 4.88 3/26/21 12:05 BGLµg/L0.247 3/24/21625.11Benzo(b)fluoranthene
<0.386 4.88 3/26/21 12:05 BGLµg/L0.386 3/24/21625.11Benzo(g,h,i)perylene
<0.271 4.88 3/26/21 12:05 BGLµg/L0.271 3/24/21625.11Benzo(k)fluoranthene
<0.289 9.76 3/26/21 12:05 BGLµg/L0.289 3/24/21625.114-Bromophenylphenylether
<0.288 9.76 3/26/21 12:05 BGLµg/L0.288 3/24/21625.11Butylbenzylphthalate
<0.469 9.76 3/26/21 12:05 BGLµg/L0.469 3/24/21625.114-Chloro-3-methylphenol
<0.460 9.76 3/26/21 12:05 BGLµg/L0.460 3/24/21625.11Bis(2-chloroethoxy)methane
<0.500 9.76 3/26/21 12:05 BGLµg/L0.500 3/24/21625.11Bis(2-chloroethyl)ether
<0.711 9.76 3/26/21 12:05 BGLµg/L0.711 3/24/21625.11Bis(2-chloroisopropyl)ether
<0.443 9.76 3/26/21 12:05 BGLµg/L0.443 3/24/21625.112-Chloronaphthalene
<0.367 9.76 3/26/21 12:05 BGLµg/L0.367 3/24/21625.112-Chlorophenol
<0.306 9.76 3/26/21 12:05 BGLµg/L0.306 3/24/21625.114-Chlorophenylphenylether
<0.212 4.88 3/26/21 12:05 BGLµg/L0.212 3/24/21625.11Chrysene
<0.444 4.88 3/26/21 12:05 BGLµg/L0.444 3/24/21625.11Dibenz(a,h)anthracene
<0.447 9.76 3/26/21 12:05 BGLµg/L0.447 3/24/21625.11Di-n-butylphthalate
<0.452 4.88 3/26/21 12:05 BGLµg/L0.452 3/24/21625.111,3-Dichlorobenzene
<0.374 4.88 3/26/21 12:05 BGLµg/L0.374 3/24/21625.111,4-Dichlorobenzene
<0.448 4.88 3/26/21 12:05 BGLµg/L0.448 3/24/21625.111,2-Dichlorobenzene
<0.350 9.76 3/26/21 12:05 BGLµg/L0.350 3/24/21625.113,3-Dichlorobenzidine
<0.293 9.76 3/26/21 12:05 BGLµg/L0.293 3/24/21625.112,4-Dichlorophenol
0.312 9.76 3/26/21 12:05 BGLµg/L0.220 3/24/21625.11JDiethylphthalate
<0.776 9.76 3/26/21 12:05 BGLµg/L0.776 3/24/21625.112,4-Dimethylphenol
<0.300 9.76 3/26/21 12:05 BGLµg/L0.300 3/24/21625.11Dimethylphthalate
<1.90 9.76 3/26/21 12:05 BGLµg/L1.90 3/24/21625.114,6-Dinitro-2-methylphenol
<1.59 9.76 3/26/21 12:05 BGLµg/L1.59 3/24/21625.112,4-Dinitrophenol
<0.319 9.76 3/26/21 12:05 BGLµg/L0.319 3/24/21625.112,4-Dinitrotoluene
<0.338 9.76 3/26/21 12:05 BGLµg/L0.338 3/24/21625.112,6-Dinitrotoluene
<0.509 9.76 3/26/21 12:05 BGLµg/L0.509 3/24/21625.11Di-n-octylphthalate
<0.366 9.76 3/26/21 12:05 BGLµg/L0.366 3/24/21625.111,2-Diphenylhydrazine/Azobenzene
<0.506 9.76 3/26/21 12:05 BGLµg/L0.506 3/24/21625.11Bis(2-Ethylhexyl)phthalate
<0.290 4.88 3/26/21 12:05 BGLµg/L0.290 3/24/21625.11Fluoranthene
3.38 4.88 3/26/21 12:05 BGLµg/L0.239 3/24/21625.11JFluorene
<0.422 9.76 3/26/21 12:05 BGLµg/L0.422 3/24/21625.11Hexachlorobenzene
<0.578 9.76 3/26/21 12:05 BGLµg/L0.578 3/24/21625.11Hexachlorobutadiene
<4.68 9.76 3/26/21 12:05 BGLµg/L4.68 3/24/21625.11Hexachlorocyclopentadiene
<0.516 9.76 3/26/21 12:05 BGLµg/L0.516 3/24/21625.11Hexachloroethane
<0.501 4.88 3/26/21 12:05 BGLµg/L0.501 3/24/21625.11Indeno(1,2,3-cd)pyrene
Page 46 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-07
Field Sample #: RW-6
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.293 9.76 3/26/21 12:05 BGLµg/L0.293 3/24/21625.11Isophorone
21.3 4.88 3/26/21 12:05 BGLµg/L0.431 3/24/21625.11Naphthalene
<0.400 9.76 3/26/21 12:05 BGLµg/L0.400 3/24/21625.11Nitrobenzene
<0.405 9.76 3/26/21 12:05 BGLµg/L0.405 3/24/21625.112-Nitrophenol
<0.612 9.76 3/26/21 12:05 BGLµg/L0.612 3/24/21625.114-Nitrophenol
<1.79 9.76 3/26/21 12:05 BGLµg/L1.79 3/24/21625.11N-Nitrosodimethylamine
<0.287 9.76 3/26/21 12:05 BGLµg/L0.287 3/24/21625.11N-Nitrosodiphenylamine/Diphenylamine
<0.505 9.76 3/26/21 12:05 BGLµg/L0.505 3/24/21625.11N-Nitrosodi-n-propylamine
<0.324 9.76 3/26/21 12:05 BGLµg/L0.324 3/24/21625.11Pentachlorophenol
37.6 4.88 3/26/21 12:05 BGLµg/L0.260 3/24/21625.112-Methylnaphthalene
3.53 4.88 3/26/21 12:05 BGLµg/L0.280 3/24/21625.11JPhenanthrene
<0.445 9.76 3/26/21 12:05 BGLµg/L0.445 3/24/21625.112-Methylphenol
<0.193 9.76 3/26/21 12:05 BGLµg/L0.193 3/24/21625.11Phenol
<0.199 19.5 3/26/21 12:05 BGLµg/L0.199 3/24/21625.113/4-Methylphenol
0.312 4.88 3/26/21 12:05 BGLµg/L0.249 3/24/21625.11JPyrene
<0.544 4.88 3/26/21 12:05 BGLµg/L0.544 3/24/21625.111,2,4-Trichlorobenzene
<0.325 9.76 3/26/21 12:05 BGLµg/L0.325 3/24/21625.112,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 32.2 3/26/21 12:0515-110
Phenol-d6 24.4 3/26/21 12:0515-110
Nitrobenzene-d5 49.4 3/26/21 12:0530-130
2-Fluorobiphenyl 55.9 3/26/21 12:0530-130
2,4,6-Tribromophenol 80.5 3/26/21 12:0515-110
p-Terphenyl-d14 85.1 3/26/21 12:0530-130
Page 47 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-07
Field Sample #: RW-6
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:55
Analyte MethodResponseDFUnitsRTResults
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)
Date
AnalystAnalyzed
Date/Time
PreparedCAS #Q#
1H-Indene, 2,3-dihydro-4,6-...6.0 µg/L 14.53261587 001685-82-1 625.1 3/24/21 BGL3/26/21 12:0586
1-Phenyl-1-butene 24 µg/L 14.02246670 000824-90-8 625.1 3/24/21 BGL3/26/21 12:0587
Benzene, 1,2,3,4-tetramethyl-5.9 µg/L 13.86860717 000488-23-3 625.1 3/24/21 BGL3/26/21 12:0594
Benzene, 1,2,3-trimethyl-35 µg/L 13.346239703 000526-73-8 625.1 3/24/21 BGL3/26/21 12:0595
Benzene, 1,2,4,5-tetramethyl-8.3 µg/L 13.88385179 000095-93-2 625.1 3/24/21 BGL3/26/21 12:0595
Biphenyl 9.4 µg/L 14.892107204 000092-52-4 625.1 3/24/21 BGL3/26/21 12:0594
Indane 6.7 µg/L 13.54546072 000496-11-7 625.1 3/24/21 BGL3/26/21 12:0593
Naphthalene, 1,2,3,4-tetrah... (04)13 µg/L 14.479135915 002809-64-5 625.1 3/24/21 BGL3/26/21 12:0596
Naphthalene, 1,3-dimethyl-13 µg/L 15.116144935 000575-41-7 625.1 3/24/21 BGL3/26/21 12:0597
Naphthalene, 2,3-dimethyl-23 µg/L 15.044258435 000581-40-8 625.1 3/24/21 BGL3/26/21 12:0597
Page 48 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-07
Field Sample #: RW-6
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
130 100 3/29/21 13:40 RDDµg/L 3/25/21MADEP EPH rev 2.11C9-C18 Aliphatics
ND 100 3/29/21 13:40 RDDµg/L 3/25/21MADEP EPH rev 2.11C19-C36 Aliphatics
580 100 3/29/21 13:40 RDDµg/L 3/25/21MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
500 100 3/29/21 13:40 RDDµg/L 3/25/21MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)55.4 3/29/21 13:4040-140
o-Terphenyl (OTP)65.3 3/29/21 13:4040-140
2-Bromonaphthalene 75.4 3/29/21 13:4040-140
2-Fluorobiphenyl 99.3 3/29/21 13:4040-140
Page 49 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-07
Field Sample #: RW-6
Sample Matrix: Ground Water
Sampled: 3/17/2021 11:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 3/20/21 6:49 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 3/20/21 6:49 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
610 100 3/20/21 6:49 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 3/20/21 6:49 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
510 100 3/20/21 6:49 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)120 3/20/21 6:4970-130
2,5-Dibromotoluene (PID)138 3/20/21 6:49*S-1570-130
Page 50 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-08
Field Sample #: RW-9
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:45
[TOC_2]21C0992-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.66 0.50 3/22/21 14:13 LBDµg/L0.13 3/22/21SM21-22 6200B1Benzene
ND 0.50 3/22/21 14:13 LBDµg/L0.080 3/22/21SM21-22 6200B1Chlorobenzene
ND 0.50 3/22/21 14:13 LBDµg/L0.10 3/22/21SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/22/21 14:13 LBDµg/L0.090 3/22/21SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/22/21 14:13 LBDµg/L0.11 3/22/21SM21-22 6200B11,4-Dichlorobenzene
1.0 0.50 3/22/21 14:13 LBDµg/L0.090 3/22/21SM21-22 6200B1Ethylbenzene
ND 0.50 3/22/21 14:13 LBDµg/L0.17 3/22/21SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 0.50 3/22/21 14:13 LBDµg/L0.11 3/22/21SM21-22 6200B1Toluene
0.47 1.0 3/22/21 14:13 LBDµg/L0.18 3/22/21SM21-22 6200B1Jm+p Xylene
ND 0.50 3/22/21 14:13 LBDµg/L0.090 3/22/21SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 95.0 3/22/21 14:1370-130
Toluene-d8 98.4 3/22/21 14:1370-130
4-Bromofluorobenzene 97.4 3/22/21 14:1370-130
Page 51 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-08
Field Sample #: RW-9
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
0.420 5.00 3/26/21 12:30 BGLµg/L0.231 3/24/21625.11JAcenaphthene
<0.231 5.00 3/26/21 12:30 BGLµg/L0.231 3/24/21625.11Acenaphthylene
<0.202 5.00 3/26/21 12:30 BGLµg/L0.202 3/24/21625.11Anthracene
<16.4 20.0 3/26/21 12:30 BGLµg/L16.4 3/24/21625.11L-04, R-05, V-04,
V-05, V-34
Benzidine
<0.252 5.00 3/26/21 12:30 BGLµg/L0.252 3/24/21625.11Benzo(a)anthracene
<0.295 5.00 3/26/21 12:30 BGLµg/L0.295 3/24/21625.11Benzo(a)pyrene
<0.253 5.00 3/26/21 12:30 BGLµg/L0.253 3/24/21625.11Benzo(b)fluoranthene
<0.396 5.00 3/26/21 12:30 BGLµg/L0.396 3/24/21625.11Benzo(g,h,i)perylene
<0.278 5.00 3/26/21 12:30 BGLµg/L0.278 3/24/21625.11Benzo(k)fluoranthene
<0.296 10.0 3/26/21 12:30 BGLµg/L0.296 3/24/21625.114-Bromophenylphenylether
<0.295 10.0 3/26/21 12:30 BGLµg/L0.295 3/24/21625.11Butylbenzylphthalate
<0.481 10.0 3/26/21 12:30 BGLµg/L0.481 3/24/21625.114-Chloro-3-methylphenol
<0.471 10.0 3/26/21 12:30 BGLµg/L0.471 3/24/21625.11Bis(2-chloroethoxy)methane
<0.512 10.0 3/26/21 12:30 BGLµg/L0.512 3/24/21625.11Bis(2-chloroethyl)ether
<0.729 10.0 3/26/21 12:30 BGLµg/L0.729 3/24/21625.11Bis(2-chloroisopropyl)ether
<0.454 10.0 3/26/21 12:30 BGLµg/L0.454 3/24/21625.112-Chloronaphthalene
<0.376 10.0 3/26/21 12:30 BGLµg/L0.376 3/24/21625.112-Chlorophenol
<0.314 10.0 3/26/21 12:30 BGLµg/L0.314 3/24/21625.114-Chlorophenylphenylether
<0.217 5.00 3/26/21 12:30 BGLµg/L0.217 3/24/21625.11Chrysene
<0.455 5.00 3/26/21 12:30 BGLµg/L0.455 3/24/21625.11Dibenz(a,h)anthracene
<0.458 10.0 3/26/21 12:30 BGLµg/L0.458 3/24/21625.11Di-n-butylphthalate
<0.463 5.00 3/26/21 12:30 BGLµg/L0.463 3/24/21625.111,3-Dichlorobenzene
<0.383 5.00 3/26/21 12:30 BGLµg/L0.383 3/24/21625.111,4-Dichlorobenzene
<0.459 5.00 3/26/21 12:30 BGLµg/L0.459 3/24/21625.111,2-Dichlorobenzene
<0.359 10.0 3/26/21 12:30 BGLµg/L0.359 3/24/21625.113,3-Dichlorobenzidine
<0.300 10.0 3/26/21 12:30 BGLµg/L0.300 3/24/21625.112,4-Dichlorophenol
<0.225 10.0 3/26/21 12:30 BGLµg/L0.225 3/24/21625.11Diethylphthalate
<0.795 10.0 3/26/21 12:30 BGLµg/L0.795 3/24/21625.112,4-Dimethylphenol
<0.307 10.0 3/26/21 12:30 BGLµg/L0.307 3/24/21625.11Dimethylphthalate
<1.95 10.0 3/26/21 12:30 BGLµg/L1.95 3/24/21625.114,6-Dinitro-2-methylphenol
<1.63 10.0 3/26/21 12:30 BGLµg/L1.63 3/24/21625.112,4-Dinitrophenol
<0.327 10.0 3/26/21 12:30 BGLµg/L0.327 3/24/21625.112,4-Dinitrotoluene
<0.346 10.0 3/26/21 12:30 BGLµg/L0.346 3/24/21625.112,6-Dinitrotoluene
<0.522 10.0 3/26/21 12:30 BGLµg/L0.522 3/24/21625.11Di-n-octylphthalate
<0.375 10.0 3/26/21 12:30 BGLµg/L0.375 3/24/21625.111,2-Diphenylhydrazine/Azobenzene
<0.519 10.0 3/26/21 12:30 BGLµg/L0.519 3/24/21625.11Bis(2-Ethylhexyl)phthalate
<0.297 5.00 3/26/21 12:30 BGLµg/L0.297 3/24/21625.11Fluoranthene
1.33 5.00 3/26/21 12:30 BGLµg/L0.245 3/24/21625.11JFluorene
<0.433 10.0 3/26/21 12:30 BGLµg/L0.433 3/24/21625.11Hexachlorobenzene
<0.592 10.0 3/26/21 12:30 BGLµg/L0.592 3/24/21625.11Hexachlorobutadiene
<4.80 10.0 3/26/21 12:30 BGLµg/L4.80 3/24/21625.11Hexachlorocyclopentadiene
<0.529 10.0 3/26/21 12:30 BGLµg/L0.529 3/24/21625.11Hexachloroethane
<0.514 5.00 3/26/21 12:30 BGLµg/L0.514 3/24/21625.11Indeno(1,2,3-cd)pyrene
Page 52 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-08
Field Sample #: RW-9
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.300 10.0 3/26/21 12:30 BGLµg/L0.300 3/24/21625.11Isophorone
1.43 5.00 3/26/21 12:30 BGLµg/L0.442 3/24/21625.11JNaphthalene
<0.410 10.0 3/26/21 12:30 BGLµg/L0.410 3/24/21625.11Nitrobenzene
<0.415 10.0 3/26/21 12:30 BGLµg/L0.415 3/24/21625.112-Nitrophenol
<0.627 10.0 3/26/21 12:30 BGLµg/L0.627 3/24/21625.114-Nitrophenol
<1.83 10.0 3/26/21 12:30 BGLµg/L1.83 3/24/21625.11N-Nitrosodimethylamine
<0.294 10.0 3/26/21 12:30 BGLµg/L0.294 3/24/21625.11N-Nitrosodiphenylamine/Diphenylamine
<0.518 10.0 3/26/21 12:30 BGLµg/L0.518 3/24/21625.11N-Nitrosodi-n-propylamine
<0.332 10.0 3/26/21 12:30 BGLµg/L0.332 3/24/21625.11Pentachlorophenol
4.51 5.00 3/26/21 12:30 BGLµg/L0.266 3/24/21625.11J2-Methylnaphthalene
1.82 5.00 3/26/21 12:30 BGLµg/L0.287 3/24/21625.11JPhenanthrene
<0.456 10.0 3/26/21 12:30 BGLµg/L0.456 3/24/21625.112-Methylphenol
<0.198 10.0 3/26/21 12:30 BGLµg/L0.198 3/24/21625.11Phenol
<0.204 20.0 3/26/21 12:30 BGLµg/L0.204 3/24/21625.113/4-Methylphenol
<0.255 5.00 3/26/21 12:30 BGLµg/L0.255 3/24/21625.11Pyrene
<0.558 5.00 3/26/21 12:30 BGLµg/L0.558 3/24/21625.111,2,4-Trichlorobenzene
<0.333 10.0 3/26/21 12:30 BGLµg/L0.333 3/24/21625.112,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 29.7 3/26/21 12:3015-110
Phenol-d6 24.2 3/26/21 12:3015-110
Nitrobenzene-d5 47.0 3/26/21 12:3030-130
2-Fluorobiphenyl 59.0 3/26/21 12:3030-130
2,4,6-Tribromophenol 72.0 3/26/21 12:3015-110
p-Terphenyl-d14 75.0 3/26/21 12:3030-130
Page 53 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-08
Field Sample #: RW-9
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:45
Analyte MethodResponseDFUnitsRTResults
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)
Date
AnalystAnalyzed
Date/Time
PreparedCAS #Q#
Naphthalene, 1,2,3,4-tetrah...5.1 µg/L 14.47946200 002809-64-5 625.1 3/24/21 BGL3/26/21 12:3097
Naphthalene, 1,2-dimethyl-4.6 µg/L 15.11645639 000573-98-8 625.1 3/24/21 BGL3/26/21 12:3095
Naphthalene, 1,3-dimethyl-4.0 µg/L 15.0639581 000575-41-7 625.1 3/24/21 BGL3/26/21 12:3090
Page 54 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-08
Field Sample #: RW-9
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 97 3/29/21 14:00 RDDµg/L 3/25/21MADEP EPH rev 2.11C9-C18 Aliphatics
ND 97 3/29/21 14:00 RDDµg/L 3/25/21MADEP EPH rev 2.11C19-C36 Aliphatics
270 97 3/29/21 14:00 RDDµg/L 3/25/21MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
260 97 3/29/21 14:00 RDDµg/L 3/25/21MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)55.2 3/29/21 14:0040-140
o-Terphenyl (OTP)64.0 3/29/21 14:0040-140
2-Bromonaphthalene 63.8 3/29/21 14:0040-140
2-Fluorobiphenyl 91.7 3/29/21 14:0040-140
Page 55 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-08
Field Sample #: RW-9
Sample Matrix: Ground Water
Sampled: 3/17/2021 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 3/20/21 8:05 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 3/20/21 8:05 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
170 100 3/20/21 8:05 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 3/20/21 8:05 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
150 100 3/20/21 8:05 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)111 3/20/21 8:0570-130
2,5-Dibromotoluene (PID)126 3/20/21 8:0570-130
Page 56 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-09
Field Sample #: RW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 15:05
[TOC_2]21C0992-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/22/21 15:57 LBDµg/L0.13 3/22/21SM21-22 6200B1Benzene
ND 0.50 3/22/21 15:57 LBDµg/L0.080 3/22/21SM21-22 6200B1Chlorobenzene
ND 0.50 3/22/21 15:57 LBDµg/L0.10 3/22/21SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/22/21 15:57 LBDµg/L0.090 3/22/21SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/22/21 15:57 LBDµg/L0.11 3/22/21SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/22/21 15:57 LBDµg/L0.090 3/22/21SM21-22 6200B1Ethylbenzene
ND 0.50 3/22/21 15:57 LBDµg/L0.17 3/22/21SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 0.50 3/22/21 15:57 LBDµg/L0.11 3/22/21SM21-22 6200B1Toluene
ND 1.0 3/22/21 15:57 LBDµg/L0.18 3/22/21SM21-22 6200B1m+p Xylene
ND 0.50 3/22/21 15:57 LBDµg/L0.090 3/22/21SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 95.6 3/22/21 15:5770-130
Toluene-d8 97.2 3/22/21 15:5770-130
4-Bromofluorobenzene 94.5 3/22/21 15:5770-130
Page 57 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-09
Field Sample #: RW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 15:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.222 4.81 3/26/21 12:54 BGLµg/L0.222 3/24/21625.11Acenaphthene
<0.222 4.81 3/26/21 12:54 BGLµg/L0.222 3/24/21625.11Acenaphthylene
<0.194 4.81 3/26/21 12:54 BGLµg/L0.194 3/24/21625.11Anthracene
<15.8 19.2 3/26/21 12:54 BGLµg/L15.8 3/24/21625.11L-04, R-05, V-04,
V-05, V-34
Benzidine
<0.242 4.81 3/26/21 12:54 BGLµg/L0.242 3/24/21625.11Benzo(a)anthracene
<0.284 4.81 3/26/21 12:54 BGLµg/L0.284 3/24/21625.11Benzo(a)pyrene
<0.243 4.81 3/26/21 12:54 BGLµg/L0.243 3/24/21625.11Benzo(b)fluoranthene
<0.381 4.81 3/26/21 12:54 BGLµg/L0.381 3/24/21625.11Benzo(g,h,i)perylene
<0.267 4.81 3/26/21 12:54 BGLµg/L0.267 3/24/21625.11Benzo(k)fluoranthene
<0.285 9.62 3/26/21 12:54 BGLµg/L0.285 3/24/21625.114-Bromophenylphenylether
<0.284 9.62 3/26/21 12:54 BGLµg/L0.284 3/24/21625.11Butylbenzylphthalate
<0.462 9.62 3/26/21 12:54 BGLµg/L0.462 3/24/21625.114-Chloro-3-methylphenol
<0.453 9.62 3/26/21 12:54 BGLµg/L0.453 3/24/21625.11Bis(2-chloroethoxy)methane
<0.492 9.62 3/26/21 12:54 BGLµg/L0.492 3/24/21625.11Bis(2-chloroethyl)ether
<0.701 9.62 3/26/21 12:54 BGLµg/L0.701 3/24/21625.11Bis(2-chloroisopropyl)ether
<0.437 9.62 3/26/21 12:54 BGLµg/L0.437 3/24/21625.112-Chloronaphthalene
<0.362 9.62 3/26/21 12:54 BGLµg/L0.362 3/24/21625.112-Chlorophenol
<0.302 9.62 3/26/21 12:54 BGLµg/L0.302 3/24/21625.114-Chlorophenylphenylether
<0.209 4.81 3/26/21 12:54 BGLµg/L0.209 3/24/21625.11Chrysene
<0.438 4.81 3/26/21 12:54 BGLµg/L0.438 3/24/21625.11Dibenz(a,h)anthracene
<0.440 9.62 3/26/21 12:54 BGLµg/L0.440 3/24/21625.11Di-n-butylphthalate
<0.445 4.81 3/26/21 12:54 BGLµg/L0.445 3/24/21625.111,3-Dichlorobenzene
<0.368 4.81 3/26/21 12:54 BGLµg/L0.368 3/24/21625.111,4-Dichlorobenzene
<0.441 4.81 3/26/21 12:54 BGLµg/L0.441 3/24/21625.111,2-Dichlorobenzene
<0.345 9.62 3/26/21 12:54 BGLµg/L0.345 3/24/21625.113,3-Dichlorobenzidine
<0.288 9.62 3/26/21 12:54 BGLµg/L0.288 3/24/21625.112,4-Dichlorophenol
<0.216 9.62 3/26/21 12:54 BGLµg/L0.216 3/24/21625.11Diethylphthalate
<0.764 9.62 3/26/21 12:54 BGLµg/L0.764 3/24/21625.112,4-Dimethylphenol
<0.295 9.62 3/26/21 12:54 BGLµg/L0.295 3/24/21625.11Dimethylphthalate
<1.88 9.62 3/26/21 12:54 BGLµg/L1.88 3/24/21625.114,6-Dinitro-2-methylphenol
<1.57 9.62 3/26/21 12:54 BGLµg/L1.57 3/24/21625.112,4-Dinitrophenol
<0.314 9.62 3/26/21 12:54 BGLµg/L0.314 3/24/21625.112,4-Dinitrotoluene
<0.333 9.62 3/26/21 12:54 BGLµg/L0.333 3/24/21625.112,6-Dinitrotoluene
<0.502 9.62 3/26/21 12:54 BGLµg/L0.502 3/24/21625.11Di-n-octylphthalate
<0.361 9.62 3/26/21 12:54 BGLµg/L0.361 3/24/21625.111,2-Diphenylhydrazine/Azobenzene
<0.499 9.62 3/26/21 12:54 BGLµg/L0.499 3/24/21625.11Bis(2-Ethylhexyl)phthalate
<0.286 4.81 3/26/21 12:54 BGLµg/L0.286 3/24/21625.11Fluoranthene
<0.236 4.81 3/26/21 12:54 BGLµg/L0.236 3/24/21625.11Fluorene
<0.416 9.62 3/26/21 12:54 BGLµg/L0.416 3/24/21625.11Hexachlorobenzene
<0.569 9.62 3/26/21 12:54 BGLµg/L0.569 3/24/21625.11Hexachlorobutadiene
<4.62 9.62 3/26/21 12:54 BGLµg/L4.62 3/24/21625.11Hexachlorocyclopentadiene
<0.509 9.62 3/26/21 12:54 BGLµg/L0.509 3/24/21625.11Hexachloroethane
<0.494 4.81 3/26/21 12:54 BGLµg/L0.494 3/24/21625.11Indeno(1,2,3-cd)pyrene
Page 58 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-09
Field Sample #: RW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 15:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.288 9.62 3/26/21 12:54 BGLµg/L0.288 3/24/21625.11Isophorone
<0.425 4.81 3/26/21 12:54 BGLµg/L0.425 3/24/21625.11Naphthalene
<0.394 9.62 3/26/21 12:54 BGLµg/L0.394 3/24/21625.11Nitrobenzene
<0.399 9.62 3/26/21 12:54 BGLµg/L0.399 3/24/21625.112-Nitrophenol
<0.603 9.62 3/26/21 12:54 BGLµg/L0.603 3/24/21625.114-Nitrophenol
<1.76 9.62 3/26/21 12:54 BGLµg/L1.76 3/24/21625.11N-Nitrosodimethylamine
<0.283 9.62 3/26/21 12:54 BGLµg/L0.283 3/24/21625.11N-Nitrosodiphenylamine/Diphenylamine
<0.498 9.62 3/26/21 12:54 BGLµg/L0.498 3/24/21625.11N-Nitrosodi-n-propylamine
<0.319 9.62 3/26/21 12:54 BGLµg/L0.319 3/24/21625.11Pentachlorophenol
<0.256 4.81 3/26/21 12:54 BGLµg/L0.256 3/24/21625.112-Methylnaphthalene
<0.276 4.81 3/26/21 12:54 BGLµg/L0.276 3/24/21625.11Phenanthrene
<0.438 9.62 3/26/21 12:54 BGLµg/L0.438 3/24/21625.112-Methylphenol
<0.190 9.62 3/26/21 12:54 BGLµg/L0.190 3/24/21625.11Phenol
<0.196 19.2 3/26/21 12:54 BGLµg/L0.196 3/24/21625.113/4-Methylphenol
<0.245 4.81 3/26/21 12:54 BGLµg/L0.245 3/24/21625.11Pyrene
<0.537 4.81 3/26/21 12:54 BGLµg/L0.537 3/24/21625.111,2,4-Trichlorobenzene
<0.320 9.62 3/26/21 12:54 BGLµg/L0.320 3/24/21625.112,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 31.9 3/26/21 12:5415-110
Phenol-d6 27.7 3/26/21 12:5415-110
Nitrobenzene-d5 47.1 3/26/21 12:5430-130
2-Fluorobiphenyl 54.4 3/26/21 12:5430-130
2,4,6-Tribromophenol 57.8 3/26/21 12:5415-110
p-Terphenyl-d14 63.0 3/26/21 12:5430-130
Page 59 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-09
Field Sample #: RW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 15:05
Analyte MethodResponseDFUnitsRTResults
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)
Date
AnalystAnalyzed
Date/Time
PreparedCAS #Q#
No TICs Found 0.0 µg/L 1 625.1 3/24/21 BGL3/26/21 12:54
Page 60 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-09
Field Sample #: RW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 15:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
270 96 3/27/21 0:04 RDDµg/L 3/25/21MADEP EPH rev 2.11C9-C18 Aliphatics
230 96 3/27/21 0:04 RDDµg/L 3/25/21MADEP EPH rev 2.11C19-C36 Aliphatics
250 96 3/27/21 0:04 RDDµg/L 3/25/21MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
250 96 3/27/21 0:04 RDDµg/L 3/25/21MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)52.8 3/27/21 0:0440-140
o-Terphenyl (OTP)68.8 3/27/21 0:0440-140
2-Bromonaphthalene 60.6 3/27/21 0:0440-140
2-Fluorobiphenyl 49.1 3/27/21 0:0440-140
Page 61 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/18/2021
Work Order: 21C0992Sample Description:Project Location: Dunn, NC
Sample ID: 21C0992-09
Field Sample #: RW-1
Sample Matrix: Ground Water
Sampled: 3/17/2021 15:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 3/20/21 9:58 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 3/20/21 9:58 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 3/20/21 9:58 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 3/20/21 9:58 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 3/20/21 9:58 KMBµg/L 3/19/21MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)126 3/20/21 9:5870-130
2,5-Dibromotoluene (PID)130 3/20/21 9:5870-130
Page 62 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3510C Analytical Method: 625.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B278676 03/24/2110401.0021C0992-01 [MW-2]
B278676 03/24/2110401.0021C0992-02 [MW-1]
B278676 03/24/2110401.0021C0992-03 [MW-3]
B278676 03/24/2110401.0021C0992-04 [RW-3]
B278676 03/24/2110301.0021C0992-05 [RW-4]
B278676 03/24/2110301.0021C0992-06 [RW-5]
B278676 03/24/2110201.0021C0992-07 [RW-6]
B278676 03/24/2110001.0021C0992-08 [RW-9]
B278676 03/24/2110401.0021C0992-09 [RW-1]
Prep Method: SW-846 3510C Analytical Method: MADEP EPH rev 2.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B278778 03/25/2110002.0021C0992-01 [MW-2]
B278778 03/25/2110002.0021C0992-02 [MW-1]
B278778 03/25/219902.0021C0992-03 [MW-3]
B278778 03/25/219902.0021C0992-04 [RW-3]
B278778 03/25/219902.0021C0992-05 [RW-4]
B278778 03/25/219752.0021C0992-06 [RW-5]
B278778 03/25/219752.0021C0992-07 [RW-6]
B278778 03/25/2110302.0021C0992-08 [RW-9]
B278778 03/25/2110402.0021C0992-09 [RW-1]
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B278407 03/19/2155.0021C0992-01 [MW-2]
B278407 03/19/2155.0021C0992-02 [MW-1]
B278407 03/19/2155.0021C0992-03 [MW-3]
B278407 03/19/2155.0021C0992-04 [RW-3]
B278407 03/19/2155.0021C0992-05 [RW-4]
B278407 03/19/2155.0021C0992-06 [RW-5]
B278407 03/19/2155.0021C0992-07 [RW-6]
B278407 03/19/2155.0021C0992-08 [RW-9]
B278407 03/19/2155.0021C0992-09 [RW-1]
Prep Method: SW-846 5030B Analytical Method: SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B278468 03/22/2155.0021C0992-01 [MW-2]
B278468 03/22/2155.0021C0992-02 [MW-1]
B278468 03/22/2155.0021C0992-03 [MW-3]
B278468 03/22/2155.0021C0992-04 [RW-3]
B278468 03/22/2155.0021C0992-05 [RW-4]
B278468 03/22/2155.0021C0992-06 [RW-5]
B278468 03/22/2155.0021C0992-07 [RW-6]
B278468 03/22/2155.0021C0992-08 [RW-9]
B278468 03/22/2155.0021C0992-09 [RW-1]
[TOC_1]Sample Preparation Information[TOC]
Page 63 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B278468 - SW-846 5030B
[TOC_3]B278468[TOC]
Blank (B278468-BLK1) Prepared & Analyzed: 03/22/21
Benzene µg/L0.50ND
Chlorobenzene µg/L0.50ND
1,2-Dichlorobenzene µg/L0.50ND
1,3-Dichlorobenzene µg/L0.50ND
1,4-Dichlorobenzene µg/L0.50ND
Ethylbenzene µg/L0.50ND
Methyl tert-Butyl Ether (MTBE)µg/L0.50ND
Toluene µg/L0.50ND
m+p Xylene µg/L1.0ND
o-Xylene µg/L0.50ND
µg/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 93.223.3
µg/L 25.0 70-130Surrogate: Toluene-d8 95.824.0
µg/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 94.323.6
LCS (B278468-BS1) Prepared & Analyzed: 03/22/21
Benzene µg/L0.50 10.0 70-13096.59.65
Chlorobenzene µg/L0.50 10.0 70-13010510.5
1,2-Dichlorobenzene µg/L0.50 10.0 70-13096.89.68
1,3-Dichlorobenzene µg/L0.50 10.0 70-13095.29.52
1,4-Dichlorobenzene µg/L0.50 10.0 70-13098.79.87
Ethylbenzene µg/L0.50 10.0 70-13010210.2
Methyl tert-Butyl Ether (MTBE)µg/L0.50 10.0 70-13010110.1
Toluene µg/L0.50 10.0 70-13010210.2
m+p Xylene µg/L1.0 20.0 70-13010520.9
o-Xylene µg/L0.50 10.0 70-13010010.0
µg/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 91.322.8
µg/L 25.0 70-130Surrogate: Toluene-d8 98.724.7
µg/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.224.0
LCS Dup (B278468-BSD1) Prepared & Analyzed: 03/22/21
Benzene µg/L0.50 10.0 2570-130104 7.7710.4
Chlorobenzene µg/L0.50 10.0 2570-130108 2.7210.8
1,2-Dichlorobenzene µg/L0.50 10.0 2570-13098.9 2.159.89
1,3-Dichlorobenzene µg/L0.50 10.0 2570-13099.4 4.329.94
1,4-Dichlorobenzene µg/L0.50 10.0 2570-130100 1.8110.0
Ethylbenzene µg/L0.50 10.0 2570-130107 4.7010.7
Methyl tert-Butyl Ether (MTBE)µg/L0.50 10.0 2570-13097.1 3.549.71
Toluene µg/L0.50 10.0 2570-130105 3.4810.5
m+p Xylene µg/L1.0 20.0 2570-130109 3.8421.7
o-Xylene µg/L0.50 10.0 2570-130104 3.6310.4
µg/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 92.823.2
µg/L 25.0 70-130Surrogate: Toluene-d8 98.124.5
µg/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 94.923.7
[TOC_1]QC Data[TOC]
Page 64 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by - GC/MS[TOC]
Batch B278676 - SW-846 3510C
[TOC_3]B278676[TOC]
Blank (B278676-BLK1) Prepared: 03/24/21 Analyzed: 03/25/21
Acenaphthene µg/L5.00ND
Acenaphthylene µg/L5.00ND
Anthracene µg/L5.00ND
Benzidine µg/L20.0 L-04, R-05, V-05,
V-35
ND
Benzo(a)anthracene µg/L5.00ND
Benzo(a)pyrene µg/L5.00ND
Benzo(b)fluoranthene µg/L5.00ND
Benzo(g,h,i)perylene µg/L5.00ND
Benzo(k)fluoranthene µg/L5.00ND
4-Bromophenylphenylether µg/L10.0ND
Butylbenzylphthalate µg/L10.0ND
4-Chloro-3-methylphenol µg/L10.0ND
Bis(2-chloroethoxy)methane µg/L10.0ND
Bis(2-chloroethyl)ether µg/L10.0ND
Bis(2-chloroisopropyl)ether µg/L10.0ND
2-Chloronaphthalene µg/L10.0ND
2-Chlorophenol µg/L10.0ND
4-Chlorophenylphenylether µg/L10.0ND
Chrysene µg/L5.00ND
Dibenz(a,h)anthracene µg/L5.00ND
Di-n-butylphthalate µg/L10.0ND
1,3-Dichlorobenzene µg/L5.00ND
1,4-Dichlorobenzene µg/L5.00ND
1,2-Dichlorobenzene µg/L5.00ND
3,3-Dichlorobenzidine µg/L10.0ND
2,4-Dichlorophenol µg/L10.0ND
Diethylphthalate µg/L10.0ND
2,4-Dimethylphenol µg/L10.0ND
Dimethylphthalate µg/L10.0ND
4,6-Dinitro-2-methylphenol µg/L10.0ND
2,4-Dinitrophenol µg/L10.0ND
2,4-Dinitrotoluene µg/L10.0ND
2,6-Dinitrotoluene µg/L10.0ND
Di-n-octylphthalate µg/L10.0ND
1,2-Diphenylhydrazine/Azobenzene µg/L10.0ND
Bis(2-Ethylhexyl)phthalate µg/L10.0ND
Fluoranthene µg/L5.00ND
Fluorene µg/L5.00ND
Hexachlorobenzene µg/L10.0ND
Hexachlorobutadiene µg/L10.0ND
Hexachlorocyclopentadiene µg/L10.0ND
Hexachloroethane µg/L10.0ND
Indeno(1,2,3-cd)pyrene µg/L5.00ND
Isophorone µg/L10.0ND
Naphthalene µg/L5.00ND
Nitrobenzene µg/L10.0ND
2-Nitrophenol µg/L10.0ND
4-Nitrophenol µg/L10.0ND
N-Nitrosodimethylamine µg/L10.0ND
N-Nitrosodiphenylamine/Diphenylamine µg/L10.0ND
N-Nitrosodi-n-propylamine µg/L10.0ND
Pentachlorophenol µg/L10.0ND
Page 65 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B278676 - SW-846 3510C
Blank (B278676-BLK1) Prepared: 03/24/21 Analyzed: 03/25/21
2-Methylnaphthalene µg/L5.00ND
Phenanthrene µg/L5.00ND
2-Methylphenol µg/L10.0ND
Phenol µg/L10.0ND
3/4-Methylphenol µg/L20.0ND
Pyrene µg/L5.00ND
1,2,4-Trichlorobenzene µg/L5.00ND
2,4,6-Trichlorophenol µg/L10.0ND
µg/L 200 15-110Surrogate: 2-Fluorophenol 58.5117
µg/L 200 15-110Surrogate: Phenol-d6 44.388.6
µg/L 100 30-130Surrogate: Nitrobenzene-d5 86.686.6
µg/L 100 30-130Surrogate: 2-Fluorobiphenyl 86.386.3
µg/L 100 15-110Surrogate: 2,4,6-Tribromophenol 90.590.5
µg/L 100 30-130Surrogate: p-Terphenyl-d14 99.799.7
LCS (B278676-BS1) Prepared: 03/24/21 Analyzed: 03/25/21
Acenaphthene µg/L5.00 50.0 47-14574.037.0
Acenaphthylene µg/L5.00 50.0 33-14572.536.3
Anthracene µg/L5.00 50.0 27-13378.039.0
Benzidine µg/L20.0 50.0 V-05, L-04, R-05,
V-35, J
40-14014.3 *7.16
Benzo(a)anthracene µg/L5.00 50.0 33-14377.238.6
Benzo(a)pyrene µg/L5.00 50.0 17-16372.836.4
Benzo(b)fluoranthene µg/L5.00 50.0 24-15977.939.0
Benzo(g,h,i)perylene µg/L5.00 50.0 10-21962.531.2
Benzo(k)fluoranthene µg/L5.00 50.0 11-16278.039.0
4-Bromophenylphenylether µg/L10.0 50.0 53-12769.634.8
Butylbenzylphthalate µg/L10.0 50.0 10-15281.340.7
4-Chloro-3-methylphenol µg/L10.0 50.0 22-14776.738.4
Bis(2-chloroethoxy)methane µg/L10.0 50.0 33-18470.535.3
Bis(2-chloroethyl)ether µg/L10.0 50.0 12-15863.931.9
Bis(2-chloroisopropyl)ether µg/L10.0 50.0 36-16679.239.6
2-Chloronaphthalene µg/L10.0 50.0 60-12064.132.0
2-Chlorophenol µg/L10.0 50.0 23-13461.430.7
4-Chlorophenylphenylether µg/L10.0 50.0 25-15872.836.4
Chrysene µg/L5.00 50.0 17-16876.738.3
Dibenz(a,h)anthracene µg/L5.00 50.0 10-22758.829.4
Di-n-butylphthalate µg/L10.0 50.0 10-12081.240.6
1,3-Dichlorobenzene µg/L5.00 50.0 10-17249.724.8
1,4-Dichlorobenzene µg/L5.00 50.0 20-12450.625.3
1,2-Dichlorobenzene µg/L5.00 50.0 32-12951.725.8
3,3-Dichlorobenzidine µg/L10.0 50.0 10-26284.442.2
2,4-Dichlorophenol µg/L10.0 50.0 39-13572.136.1
Diethylphthalate µg/L10.0 50.0 10-12077.638.8
2,4-Dimethylphenol µg/L10.0 50.0 32-12070.635.3
Dimethylphthalate µg/L10.0 50.0 10-12077.138.5
4,6-Dinitro-2-methylphenol µg/L10.0 50.0 10-18179.539.8
2,4-Dinitrophenol µg/L10.0 50.0 10-19182.641.3
2,4-Dinitrotoluene µg/L10.0 50.0 39-13980.540.2
2,6-Dinitrotoluene µg/L10.0 50.0 50-15879.940.0
Di-n-octylphthalate µg/L10.0 50.0 4-14688.344.2
1,2-Diphenylhydrazine/Azobenzene µg/L10.0 50.0 40-14079.239.6
Bis(2-Ethylhexyl)phthalate µg/L10.0 50.0 8-15882.341.1
Page 66 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B278676 - SW-846 3510C
LCS (B278676-BS1) Prepared: 03/24/21 Analyzed: 03/25/21
Fluoranthene µg/L5.00 50.0 26-13780.940.5
Fluorene µg/L5.00 50.0 59-12177.438.7
Hexachlorobenzene µg/L10.0 50.0 10-15268.634.3
Hexachlorobutadiene µg/L10.0 50.0 24-12052.826.4
Hexachlorocyclopentadiene µg/L10.0 50.0 40-14053.927.0
Hexachloroethane µg/L10.0 50.0 40-12049.124.6
Indeno(1,2,3-cd)pyrene µg/L5.00 50.0 10-17164.932.4
Isophorone µg/L10.0 50.0 21-19678.039.0
Naphthalene µg/L5.00 50.0 21-13363.731.9
Nitrobenzene µg/L10.0 50.0 35-18065.232.6
2-Nitrophenol µg/L10.0 50.0 29-18268.234.1
4-Nitrophenol µg/L10.0 50.0 10-13241.520.7
N-Nitrosodimethylamine µg/L10.0 50.0 40-14042.221.1
N-Nitrosodiphenylamine/Diphenylamine µg/L10.0 50.0 40-14087.243.6
N-Nitrosodi-n-propylamine µg/L10.0 50.0 10-23068.634.3
Pentachlorophenol µg/L10.0 50.0 14-17668.534.2
2-Methylnaphthalene µg/L5.00 50.0 40-14075.938.0
Phenanthrene µg/L5.00 50.0 54-12078.239.1
2-Methylphenol µg/L10.0 50.0 40-14063.331.7
Phenol µg/L10.0 50.0 5-12031.515.8
3/4-Methylphenol µg/L20.0 50.0 40-14062.231.1
Pyrene µg/L5.00 50.0 52-12083.341.7
1,2,4-Trichlorobenzene µg/L5.00 50.0 44-14257.528.7
2,4,6-Trichlorophenol µg/L10.0 50.0 37-14473.536.8
µg/L 200 15-110Surrogate: 2-Fluorophenol 44.789.4
µg/L 200 15-110Surrogate: Phenol-d6 36.873.5
µg/L 100 30-130Surrogate: Nitrobenzene-d5 72.772.7
µg/L 100 30-130Surrogate: 2-Fluorobiphenyl 78.978.9
µg/L 100 15-110Surrogate: 2,4,6-Tribromophenol 80.780.7
µg/L 100 30-130Surrogate: p-Terphenyl-d14 88.388.3
LCS Dup (B278676-BSD1) Prepared: 03/24/21 Analyzed: 03/25/21
Acenaphthene µg/L5.00 50.0 4847-14579.7 7.3939.8
Acenaphthylene µg/L5.00 50.0 7433-14578.6 8.0239.3
Anthracene µg/L5.00 50.0 6627-13384.5 8.0042.3
Benzidine µg/L20.0 50.0 30 L-04, R-05, V-05,
V-35, J
40-14034.6 82.9**17.3
Benzo(a)anthracene µg/L5.00 50.0 5333-14381.6 5.4440.8
Benzo(a)pyrene µg/L5.00 50.0 7217-16376.4 4.8838.2
Benzo(b)fluoranthene µg/L5.00 50.0 7124-15981.7 4.6940.8
Benzo(g,h,i)perylene µg/L5.00 50.0 9710-21967.9 8.2233.9
Benzo(k)fluoranthene µg/L5.00 50.0 6311-16281.4 4.3440.7
4-Bromophenylphenylether µg/L10.0 50.0 4353-12775.4 8.1137.7
Butylbenzylphthalate µg/L10.0 50.0 6010-15284.2 3.4342.1
4-Chloro-3-methylphenol µg/L10.0 50.0 7322-14783.5 8.4741.7
Bis(2-chloroethoxy)methane µg/L10.0 50.0 5433-18481.0 13.840.5
Bis(2-chloroethyl)ether µg/L10.0 50.0 10812-15873.2 13.636.6
Bis(2-chloroisopropyl)ether µg/L10.0 50.0 7636-16691.5 14.445.8
2-Chloronaphthalene µg/L10.0 50.0 2460-12068.6 6.9034.3
2-Chlorophenol µg/L10.0 50.0 6123-13471.3 14.935.7
4-Chlorophenylphenylether µg/L10.0 50.0 6125-15877.2 5.7938.6
Chrysene µg/L5.00 50.0 8717-16880.5 4.8440.2
Dibenz(a,h)anthracene µg/L5.00 50.0 12610-22762.6 6.3631.3
Page 67 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B278676 - SW-846 3510C
LCS Dup (B278676-BSD1) Prepared: 03/24/21 Analyzed: 03/25/21
Di-n-butylphthalate µg/L10.0 50.0 4710-12084.2 3.5842.1
1,3-Dichlorobenzene µg/L5.00 50.0 3010-17257.2 14.128.6
1,4-Dichlorobenzene µg/L5.00 50.0 3020-12458.4 14.329.2
1,2-Dichlorobenzene µg/L5.00 50.0 3032-12960.5 15.730.2
3,3-Dichlorobenzidine µg/L10.0 50.0 10810-26289.8 6.2244.9
2,4-Dichlorophenol µg/L10.0 50.0 5039-13581.4 12.040.7
Diethylphthalate µg/L10.0 50.0 10010-12079.3 2.1239.6
2,4-Dimethylphenol µg/L10.0 50.0 5832-12072.2 2.1836.1
Dimethylphthalate µg/L10.0 50.0 18310-12079.7 3.3439.8
4,6-Dinitro-2-methylphenol µg/L10.0 50.0 20310-18185.0 6.7142.5
2,4-Dinitrophenol µg/L10.0 50.0 13210-19186.4 4.4043.2
2,4-Dinitrotoluene µg/L10.0 50.0 4239-13983.8 4.0941.9
2,6-Dinitrotoluene µg/L10.0 50.0 4850-15883.6 4.5241.8
Di-n-octylphthalate µg/L10.0 50.0 694-14691.1 3.1245.6
1,2-Diphenylhydrazine/Azobenzene µg/L10.0 50.0 3040-14086.2 8.4443.1
Bis(2-Ethylhexyl)phthalate µg/L10.0 50.0 828-15885.2 3.4642.6
Fluoranthene µg/L5.00 50.0 6626-13784.1 3.9042.1
Fluorene µg/L5.00 50.0 3859-12181.3 4.8940.6
Hexachlorobenzene µg/L10.0 50.0 5510-15274.4 8.0837.2
Hexachlorobutadiene µg/L10.0 50.0 6224-12061.1 14.630.6
Hexachlorocyclopentadiene µg/L10.0 50.0 3040-14059.8 10.329.9
Hexachloroethane µg/L10.0 50.0 5240-12056.5 14.028.3
Indeno(1,2,3-cd)pyrene µg/L5.00 50.0 9910-17170.4 8.2235.2
Isophorone µg/L10.0 50.0 9321-19687.7 11.743.8
Naphthalene µg/L5.00 50.0 6521-13372.3 12.636.1
Nitrobenzene µg/L10.0 50.0 6235-18074.8 13.637.4
2-Nitrophenol µg/L10.0 50.0 5529-18279.6 15.439.8
4-Nitrophenol µg/L10.0 50.0 13110-13244.9 7.8822.4
N-Nitrosodimethylamine µg/L10.0 50.0 3040-14050.1 17.125.0
N-Nitrosodiphenylamine/Diphenylamine µg/L10.0 50.0 3040-14093.3 6.6946.6
N-Nitrosodi-n-propylamine µg/L10.0 50.0 8710-23080.2 15.640.1
Pentachlorophenol µg/L10.0 50.0 8614-17663.9 6.8932.0
2-Methylnaphthalene µg/L5.00 50.0 3040-14084.2 10.342.1
Phenanthrene µg/L5.00 50.0 3954-12083.6 6.5841.8
2-Methylphenol µg/L10.0 50.0 3040-14070.7 11.035.4
Phenol µg/L10.0 50.0 645-12036.9 15.818.5
3/4-Methylphenol µg/L20.0 50.0 3040-14071.4 13.735.7
Pyrene µg/L5.00 50.0 4952-12081.2 2.6340.6
1,2,4-Trichlorobenzene µg/L5.00 50.0 5044-14266.3 14.333.1
2,4,6-Trichlorophenol µg/L10.0 50.0 5837-14478.1 6.0439.0
µg/L 200 15-110Surrogate: 2-Fluorophenol 53.2106
µg/L 200 15-110Surrogate: Phenol-d6 42.484.7
µg/L 100 30-130Surrogate: Nitrobenzene-d5 79.979.9
µg/L 100 30-130Surrogate: 2-Fluorobiphenyl 85.285.2
µg/L 100 15-110Surrogate: 2,4,6-Tribromophenol 83.783.7
µg/L 100 30-130Surrogate: p-Terphenyl-d14 91.391.3
Page 68 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED) - Quality Control
QUALITY CONTROL
entatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)[TOC]
Batch B278676 - SW-846 3510C
[TOC_3]B278676[TOC]
Blank (B278676-BLK1) Prepared: 03/24/21 Analyzed: 03/25/21
No TICs Found µg/L0.0
Page 69 of 85
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - EPH[TOC]
Batch B278778 - SW-846 3510C
[TOC_3]B278778[TOC]
Blank (B278778-BLK1) Prepared: 03/25/21 Analyzed: 03/26/21
C9-C18 Aliphatics µg/L100ND
C19-C36 Aliphatics µg/L100ND
Unadjusted C11-C22 Aromatics µg/L100ND
C11-C22 Aromatics µg/L100ND
Acenaphthene µg/L2.0ND
Acenaphthylene µg/L2.0ND
Anthracene µg/L2.0ND
Benzo(a)anthracene µg/L2.0ND
Benzo(a)pyrene µg/L2.0ND
Benzo(b)fluoranthene µg/L2.0ND
Benzo(g,h,i)perylene µg/L2.0ND
Benzo(k)fluoranthene µg/L2.0ND
Chrysene µg/L2.0ND
Dibenz(a,h)anthracene µg/L2.0ND
Fluoranthene µg/L2.0ND
Fluorene µg/L2.0ND
Indeno(1,2,3-cd)pyrene µg/L2.0ND
2-Methylnaphthalene µg/L2.0ND
Naphthalene µg/L2.0ND
Phenanthrene µg/L2.0ND
Pyrene µg/L2.0ND
Naphthalene-aliphatic fraction µg/L2.0ND
2-Methylnaphthalene-aliphatic fraction µg/L2.0ND
µg/L 100 40-140Surrogate: Chlorooctadecane (COD)72.372.3
µg/L 100 40-140Surrogate: o-Terphenyl (OTP)84.584.5
µg/L 100 40-140Surrogate: 2-Bromonaphthalene 105105
µg/L 100 40-140Surrogate: 2-Fluorobiphenyl 132132
LCS (B278778-BS1) Prepared: 03/25/21 Analyzed: 03/26/21
C9-C18 Aliphatics µg/L100 600 40-14071.9432
C19-C36 Aliphatics µg/L100 800 40-14095.4763
Unadjusted C11-C22 Aromatics µg/L100 1700 40-14083.61420
Acenaphthene µg/L2.0 100 40-14076.876.8
Acenaphthylene µg/L2.0 100 40-14066.266.2
Anthracene µg/L2.0 100 40-14082.682.6
Benzo(a)anthracene µg/L2.0 100 40-14085.485.4
Benzo(a)pyrene µg/L2.0 100 40-14083.783.7
Benzo(b)fluoranthene µg/L2.0 100 40-14082.482.4
Benzo(g,h,i)perylene µg/L2.0 100 40-14080.480.4
Benzo(k)fluoranthene µg/L2.0 100 40-14086.186.1
Chrysene µg/L2.0 100 40-14088.088.0
Dibenz(a,h)anthracene µg/L2.0 100 40-14081.481.4
Fluoranthene µg/L2.0 100 40-14085.185.1
Fluorene µg/L2.0 100 40-14075.975.9
Indeno(1,2,3-cd)pyrene µg/L2.0 100 40-14072.472.4
2-Methylnaphthalene µg/L2.0 100 40-14062.062.0
Naphthalene µg/L2.0 100 40-14057.757.7
Phenanthrene µg/L2.0 100 40-14080.780.7
Pyrene µg/L2.0 100 40-14087.687.6
Naphthalene-aliphatic fraction µg/L2.0 100 0-5ND
2-Methylnaphthalene-aliphatic fraction µg/L2.0 100 0-5ND
µg/L 100 40-140Surrogate: Chlorooctadecane (COD)74.974.9
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B278778 - SW-846 3510C
LCS (B278778-BS1) Prepared: 03/25/21 Analyzed: 03/26/21
µg/L 100 40-140Surrogate: o-Terphenyl (OTP)84.784.7
µg/L 100 40-140Surrogate: 2-Bromonaphthalene 96.396.3
µg/L 100 40-140Surrogate: 2-Fluorobiphenyl 127127
LCS Dup (B278778-BSD1) Prepared: 03/25/21 Analyzed: 03/26/21
C9-C18 Aliphatics µg/L100 600 2540-14078.6 8.81471
C19-C36 Aliphatics µg/L100 800 2540-14098.6 3.32789
Unadjusted C11-C22 Aromatics µg/L100 1700 2540-14084.8 1.421440
Acenaphthene µg/L2.0 100 2540-14080.2 4.3880.2
Acenaphthylene µg/L2.0 100 2540-14070.1 5.7070.1
Anthracene µg/L2.0 100 2540-14083.0 0.43083.0
Benzo(a)anthracene µg/L2.0 100 2540-14085.5 0.091385.5
Benzo(a)pyrene µg/L2.0 100 2540-14082.9 0.88682.9
Benzo(b)fluoranthene µg/L2.0 100 2540-14082.2 0.23882.2
Benzo(g,h,i)perylene µg/L2.0 100 2540-14080.4 0.019980.4
Benzo(k)fluoranthene µg/L2.0 100 2540-14085.7 0.44985.7
Chrysene µg/L2.0 100 2540-14087.9 0.079687.9
Dibenz(a,h)anthracene µg/L2.0 100 2540-14081.3 0.046781.3
Fluoranthene µg/L2.0 100 2540-14084.9 0.22484.9
Fluorene µg/L2.0 100 2540-14078.3 3.0978.3
Indeno(1,2,3-cd)pyrene µg/L2.0 100 2540-14072.5 0.19372.5
2-Methylnaphthalene µg/L2.0 100 2540-14065.0 4.6965.0
Naphthalene µg/L2.0 100 2540-14060.8 5.2360.8
Phenanthrene µg/L2.0 100 2540-14081.2 0.69481.2
Pyrene µg/L2.0 100 2540-14087.4 0.25187.4
Naphthalene-aliphatic fraction µg/L2.0 100 0-5ND
2-Methylnaphthalene-aliphatic fraction µg/L2.0 100 0-5ND
µg/L 100 40-140Surrogate: Chlorooctadecane (COD)79.979.9
µg/L 100 40-140Surrogate: o-Terphenyl (OTP)84.184.1
µg/L 100 40-140Surrogate: 2-Bromonaphthalene 93.093.0
µg/L 100 40-140Surrogate: 2-Fluorobiphenyl 124124
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B278407 - MA VPH
[TOC_3]B278407[TOC]
Blank (B278407-BLK1) Prepared: 03/19/21 Analyzed: 03/20/21
Unadjusted C5-C8 Aliphatics µg/L100ND
C5-C8 Aliphatics µg/L100ND
Unadjusted C9-C12 Aliphatics µg/L100ND
C9-C12 Aliphatics µg/L100ND
C9-C10 Aromatics µg/L100ND
Benzene µg/L1.0ND
Butylcyclohexane µg/L1.0ND
Decane µg/L1.0ND
Ethylbenzene µg/L1.0ND
Methyl tert-Butyl Ether (MTBE)µg/L1.0ND
2-Methylpentane µg/L1.0ND
Naphthalene µg/L5.0ND
Nonane µg/L1.0ND
Pentane µg/L1.0ND
Toluene µg/L1.0ND
1,2,4-Trimethylbenzene µg/L1.0ND
2,2,4-Trimethylpentane µg/L1.0ND
m+p Xylene µg/L2.0ND
o-Xylene µg/L1.0ND
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)94.137.6
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10843.2
LCS (B278407-BS1) Prepared: 03/19/21 Analyzed: 03/20/21
Benzene µg/L1.0 50.0 70-13096.548.3
Butylcyclohexane µg/L1.0 50.0 70-13012663.0
Decane µg/L1.0 50.0 70-13010351.4
Ethylbenzene µg/L1.0 50.0 70-13097.348.6
Methyl tert-Butyl Ether (MTBE)µg/L1.0 50.0 70-13010552.4
2-Methylpentane µg/L1.0 50.0 70-13079.839.9
Naphthalene µg/L5.0 50.0 70-13010250.9
Nonane µg/L1.0 50.0 70-13012462.2
Pentane µg/L1.0 50.0 70-13080.440.2
Toluene µg/L1.0 50.0 70-13096.748.4
1,2,4-Trimethylbenzene µg/L1.0 50.0 70-13096.848.4
2,2,4-Trimethylpentane µg/L1.0 50.0 70-13080.940.4
m+p Xylene µg/L2.0 100 70-13097.997.9
o-Xylene µg/L1.0 50.0 70-13010150.4
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12349.4
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)12750.9
LCS Dup (B278407-BSD1) Prepared: 03/19/21 Analyzed: 03/20/21
Benzene µg/L1.0 50.0 2570-130100 3.9650.2
Butylcyclohexane µg/L1.0 50.0 2570-130127 0.47463.3
Decane µg/L1.0 50.0 2570-130101 1.7950.5
Ethylbenzene µg/L1.0 50.0 2570-130101 4.0150.6
Methyl tert-Butyl Ether (MTBE)µg/L1.0 50.0 2570-130104 0.48652.1
2-Methylpentane µg/L1.0 50.0 2570-13087.5 9.1243.7
Naphthalene µg/L5.0 50.0 2570-130108 6.1154.1
Nonane µg/L1.0 50.0 2570-130124 0.77661.8
Pentane µg/L1.0 50.0 2570-13090.1 11.445.1
Toluene µg/L1.0 50.0 2570-130102 5.6551.2
1,2,4-Trimethylbenzene µg/L1.0 50.0 2570-13099.1 2.3549.6
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B278407 - MA VPH
LCS Dup (B278407-BSD1) Prepared: 03/19/21 Analyzed: 03/20/21
2,2,4-Trimethylpentane µg/L1.0 50.0 2570-13081.9 1.2841.0
m+p Xylene µg/L2.0 100 2570-130102 3.63102
o-Xylene µg/L1.0 50.0 2570-130104 2.9651.9
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12851.2
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)13052.0
Page 73 of 85
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
†Wide recovery limits established for difficult compound.
‡Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Surrogate recovery outside of control limits due to suspected sample matrix interference. Chromatogram(s) is
attached.
S-15
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-04
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this
compound. Reported result is estimated.
V-35
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
625.1 in Water
CT,MA,NH,NY,NC,RI,ME,VAAcenaphthene
CT,MA,NH,NY,NC,RI,ME,VAAcenaphthylene
CT,MA,NH,NY,NC,RI,ME,VAAnthracene
CT,MA,NH,NY,NC,RI,ME,VABenzidine
CT,MA,NH,NY,NC,RI,ME,VABenzo(a)anthracene
CT,MA,NH,NY,NC,RI,ME,VABenzo(a)pyrene
CT,MA,NH,NY,NC,RI,ME,VABenzo(b)fluoranthene
CT,MA,NH,NY,NC,RI,ME,VABenzo(g,h,i)perylene
CT,MA,NH,NY,NC,RI,ME,VABenzo(k)fluoranthene
CT,MA,NH,NY,NC,RI,ME,VA4-Bromophenylphenylether
CT,MA,NH,NY,NC,RI,ME,VAButylbenzylphthalate
CT,MA,NH,NY,NC,RI,VA4-Chloro-3-methylphenol
CT,MA,NH,NY,NC,RI,ME,VABis(2-chloroethoxy)methane
CT,MA,NH,NY,NC,RI,ME,VABis(2-chloroethyl)ether
CT,MA,NH,NY,NC,RI,ME,VABis(2-chloroisopropyl)ether
CT,MA,NH,NY,NC,RI,ME,VA2-Chloronaphthalene
CT,MA,NH,NY,NC,RI,ME,VA2-Chlorophenol
CT,MA,NH,NY,NC,RI,ME,VA4-Chlorophenylphenylether
CT,MA,NH,NY,NC,RI,ME,VAChrysene
CT,MA,NH,NY,NC,RI,ME,VADibenz(a,h)anthracene
CT,MA,NH,NY,NC,RI,ME,VADi-n-butylphthalate
MA,NC1,3-Dichlorobenzene
MA,NC1,4-Dichlorobenzene
MA,NC1,2-Dichlorobenzene
CT,MA,NH,NY,NC,RI,ME,VA3,3-Dichlorobenzidine
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dichlorophenol
CT,MA,NH,NY,NC,RI,ME,VADiethylphthalate
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dimethylphenol
CT,MA,NH,NY,NC,RI,ME,VADimethylphthalate
CT,MA,NH,NY,NC,RI,ME,VA4,6-Dinitro-2-methylphenol
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dinitrophenol
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dinitrotoluene
CT,MA,NH,NY,NC,RI,ME,VA2,6-Dinitrotoluene
CT,MA,NH,NY,NC,RI,ME,VADi-n-octylphthalate
NC1,2-Diphenylhydrazine/Azobenzene
CT,MA,NH,NY,NC,RI,ME,VABis(2-Ethylhexyl)phthalate
CT,MA,NH,NY,NC,RI,ME,VAFluoranthene
CT,MA,NH,NY,NC,RI,ME,VAFluorene
CT,MA,NH,NY,NC,RI,ME,VAHexachlorobenzene
CT,MA,NH,NY,NC,RI,ME,VAHexachlorobutadiene
CT,MA,NH,NY,NC,RI,ME,VAHexachlorocyclopentadiene
CT,MA,NH,NY,NC,RI,ME,VAHexachloroethane
CT,MA,NH,NY,NC,RI,ME,VAIndeno(1,2,3-cd)pyrene
CT,MA,NH,NY,NC,RI,ME,VAIsophorone
CT,MA,NH,NY,NC,RI,ME,VANaphthalene
CT,MA,NH,NY,NC,RI,ME,VANitrobenzene
CT,MA,NH,NY,NC,RI,ME,VA2-Nitrophenol
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
625.1 in Water
CT,MA,NH,NY,NC,RI,ME,VA4-Nitrophenol
CT,MA,NH,NY,NC,RI,ME,VAN-Nitrosodimethylamine
CT,MA,NH,NY,NC,RI,ME,VAN-Nitrosodi-n-propylamine
CT,MA,NH,NY,NC,RI,ME,VAPentachlorophenol
NC2-Methylnaphthalene
CT,MA,NH,NY,NC,RI,ME,VAPhenanthrene
NY,NC2-Methylphenol
CT,MA,NH,NY,NC,RI,ME,VAPhenol
NY,NC3/4-Methylphenol
CT,MA,NH,NY,NC,RI,ME,VAPyrene
CT,MA,NH,NY,NC,RI,ME,VA1,2,4-Trichlorobenzene
CT,MA,NH,NY,NC,RI,ME,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
MADEP EPH rev 2.1 in Soil
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
CT,NC,ME,NH-PAcenaphthene
CT,NC,ME,NH-PAcenaphthylene
CT,NC,ME,NH-PAnthracene
CT,NC,ME,NH-PBenzo(a)anthracene
CT,NC,ME,NH-PBenzo(a)pyrene
CT,NC,ME,NH-PBenzo(b)fluoranthene
CT,NC,ME,NH-PBenzo(g,h,i)perylene
CT,NC,ME,NH-PBenzo(k)fluoranthene
CT,NC,ME,NH-PChrysene
CT,NC,ME,NH-PDibenz(a,h)anthracene
CT,NC,ME,NH-PFluoranthene
CT,NC,MEFluorene
CT,NC,ME,NH-PIndeno(1,2,3-cd)pyrene
CT,NC,ME2-Methylnaphthalene
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PPhenanthrene
CT,NC,ME,NH-PPyrene
MADEP EPH rev 2.1 in Water
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
CT,NC,ME,NH-PAcenaphthene
CT,NC,ME,NH-PAcenaphthylene
CT,NC,ME,NH-PAnthracene
CT,NC,ME,NH-PBenzo(a)anthracene
CT,NC,ME,NH-PBenzo(a)pyrene
CT,NC,ME,NH-PBenzo(b)fluoranthene
Page 76 of 85
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP EPH rev 2.1 in Water
CT,NC,ME,NH-PBenzo(g,h,i)perylene
CT,NC,ME,NH-PBenzo(k)fluoranthene
CT,NC,ME,NH-PChrysene
CT,NC,ME,NH-PDibenz(a,h)anthracene
CT,NC,ME,NH-PFluoranthene
CT,NC,MEFluorene
CT,NC,ME,NH-PIndeno(1,2,3-cd)pyrene
CT,NC,ME2-Methylnaphthalene
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PPhenanthrene
CT,NC,ME,NH-PPyrene
MADEP-VPH-Feb 2018 Rev 2.1 in Water
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
CT,NC,ME,NH-PBenzene
CT,NC,ME,NH-PEthylbenzene
CT,NC,ME,NH-PMethyl tert-Butyl Ether (MTBE)
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PToluene
CT,NC,ME,NH-Pm+p Xylene
CT,NC,ME,NH-Po-Xylene
SM21-22 6200B in Water
NCBenzene
NCChlorobenzene
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCEthylbenzene
NCMethyl tert-Butyl Ether (MTBE)
NCNaphthalene
NCToluene
NC1,2,4-Trichlorobenzene
NCm+p Xylene
NCo-Xylene
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Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2021
PH-0165Connecticut Department of Publilc HealthCT 12/31/2022
10899 NELAPNew York State Department of HealthNY 04/1/2021
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2022
LAO00112Rhode Island Department of HealthRI 12/30/2021
652North Carolina Div. of Water QualityNC 12/31/2021
MA007 NELAPNew Jersey DEPNJ 06/30/2021
E871027 NELAPFlorida Department of HealthFL 06/30/2021
LL720741Vermont Department of Health Lead LaboratoryVT 07/30/2021
MA00100State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2021
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2021
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2021
25703North Carolina Department of HealthNC-DW 07/31/2021
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2021
9100Dept. of Env, Great Lakes, and EnergyMI 09/6/2021
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