AS-3740_28869_CA_MRP_20180921

Via FedEx Overnight

September 20, 2018 North Carolina Department of
Environmental Quality
Asheville Regional Office 2090 US Highway 70 Swannanoa, NC 28778
Attention: Ms. Caroline LaFond
Re: Monitoring Report Former Dietz Trucking Terminal Hickory, North Carolina
NC DEQ Incident No. 28869
H&H Job No. ROS-001 Dear Caroline:
On behalf of Ms. Rose Dietz, Hart & Hickman, PC (H&H) is submitting the attached Monitoring
Report for the above-referenced site. If you have any questions or need further information, please do not hesitate to contact me. Sincerely,

Hart & Hickman, PC
Stephen R. Libbey, PG Project Manager

Monitoring Report
Former Dietz Trucking Terminal

8814 Dietz Avenue
Hickory, North Carolina
NC DEQ Incident No. 28869

H&H Job No. ROS-001
September 20, 2018

Title Page

Site Location:
8814 Dietz Avenue
Hickory, NC 28637
Site Owner: Rose Dietz
746 14th Avenue NW
Hickory, NC 28601

UST Owner: Dietz Motor Lines (out of business) 8814 Dietz Avenue
Hickory, NC 28602

Consultant: Hart & Hickman, PC
2923 S. Tryon Street, Ste 100 Charlotte, NC 28203 [phone]

General Site Information: Facility ID Number: 0-004348
NC DEQ Incident Number: 28869 Site Priority Ranking: High Land Use Category: Industrial
Latitude: 35.70478N Longitude: -81.43421W
Release Discovery Date: July 20, 2010
Estimated Quantity of Release: Unknown
Cause/Source of Release: Unknown/UST System Size and content of UST system: 10,000-gallon diesel
Laboratory: Prism Laboratories, Inc., NC Certification No. 402

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Monitoring Report
Former Dietz Trucking Terminal
Hickory, North Carolina
H&H Job No. ROS-001

Table of Contents Section Page No.

1.0 Site History and Source Characterization ............................................................................1
2.0 Summary of Potential Receptor Information .......................................................................4
2.1 Water Supply Wells ...............................................................................................................4
2.2 Surface Water ........................................................................................................................4
3.0 Groundwater Monitoring .......................................................................................................5
3.1 Water Levels ..........................................................................................................................5
3.2 Monitoring Well and Water Supply Well Analytical Data ....................................................5
4.0 Conclusions and Recommendations ......................................................................................7

List of Tables
Table 1 Receptor Information
Table 2 Summary of Groundwater Level Data
Table 3 Summary of Groundwater Sampling Results

List of Figures
Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Water Supply Well Survey and Adjacent Property Owners Map
Figure 4 Monitoring Well Locations and Groundwater Elevations Map

List of Appendices
Appendix A Laboratory Analytical Data

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Monitoring Report
Former Dietz Trucking Terminal
Hickory, North Carolina
H&H Job No. ROS-001

1.0 Site History and Source Characterization

On behalf of Ms. Rose Dietz, Hart & Hickman, PC (H&H) has completed this Monitoring Report
for the former Dietz trucking terminal located at 8814 Dietz Avenue in Hickory, Burke County,
North Carolina. The site is approximately 17.25 acres in area and contains an approximate
29,400 square ft office and warehouse building and an approximate 10,900 square ft former
service garage building. Currently, the site is used as a trucking terminal and is located in a
mixed commercial, industrial and residential area of Hickory, North Carolina. A site location
map is presented as Figure 1, and a site layout is depicted on Figure 2.

Underground storage tank (UST) closure activities were conducted at the site for a 10,000-gallon
diesel UST on July 20 and 21, 2010. During UST closure, approximately 112 tons of impacted
soils were excavated from around the UST and transported off-site for proper disposal. The UST
excavation was limited in extent on its western sidewall due to the existence of the former
service garage building.

The results of analyses of the post-excavation soil samples indicated that one sample (labeled
West SW) in the excavation western sidewall contained compound concentrations above soil-to-
groundwater Maximum Soil Contaminant Concentrations (MSCCs). No post-excavation soil
sample concentrations exceeded residential or commercial/industrial MSCCs.

Based on soil remaining in the excavation western sidewall above the lowest MSCCs, H&H
recommended that a Phase I Limited Site Assessment (LSA) be completed for the site in
accordance with North Carolina Department of Environmental Quality (DEQ) guidance.
Additionally, due to the close proximity of the on-site water supply well, H&H also
recommended sampling the well during the Phase I LSA. In a Notice of Regulatory

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Requirements (NORR) letter dated August 26, 2010, DEQ indicated that a Phase I LSA should
be completed for the site.

On October 27, 2010, H&H oversaw the advancement of LSA monitoring well TMW-1 adjacent
to former soil sample West SW that contained the highest compound concentrations during the
initial abatement activities. Soil samples were not collected from the TMW-1 boring because the
initial abatement excavation extended to the water table and excavation sidewall samples for
risk-based analysis were collected as part of the initial abatement. In addition, on-site water
supply well WSW-1 also was sampled.

Because the groundwater analytical results for TMW-1 indicated compound concentrations
greater than 10 times the groundwater standards, and because water supply wells were identified
within 1,000 ft, H&H conducted additional assessment activities to meet the requirements of a
Phase II LSA. On December 20, 2010, H&H oversaw the installation of monitoring wells MW-2
and MW-3 in locations anticipated to be downgradient of the former UST basin and MW-4 in a
location anticipated to be upgradient of the former UST basin.

The results of the Phase I and II LSA groundwater analyses indicated that C9-C18 aromatics,
total C9-C22 aromatics, naphthalene, and 2-methylnaphthalene were detected above the
North Carolina groundwater standards in TMW-1. Free product was not identified, and no
compound concentrations exceeded their DEQ-defined Gross Contamination Levels (GCLs). No
compound concentrations were detected above laboratory detection limits in monitoring wells
MW-2 through MW-4 and water supply well WSW-1.

Because water supply wells are located within 1,000 ft of the site, post-excavation confirmation
soil sample concentrations exceed soil-to-groundwater MSCCs, and petroleum compounds
exceed the North Carolina groundwater standards, H&H recommended that a Comprehensive
Site Assessment (CSA) be completed for the site in accordance with DEQ guidance. In a letter
dated February 8, 2011, DEQ requested that a CSA be completed in accordance with applicable

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guidelines. In subsequent phone calls between H&H and DEQ, DEQ approved limited CSA
activities based on the lack of significant soil and groundwater impacts at the site.
Limited CSA activities were conducted in August and September 2011. The activities included
installation of one deep monitoring well, sampling five groundwater monitoring wells, and
sampling the two closest downgradient water supply wells to the source area. Target compound
concentrations in groundwater samples were detected above the North Carolina groundwater
standards in shallow source area monitoring well TMW-1 only. No concentrations exceed GCLs
and no free product was detected in any of the monitoring wells. Additionally, no target
compounds were detected above laboratory detection limits in the two closest downgradient
water supply wells to the source area.

Based on the results of the limited CSA activities conducted by H&H, DEQ issued an NORR
letter dated December 5, 2011 requesting a Corrective Action Plan (CAP) be completed for the
site. H&H prepared a Natural Attenuation CAP dated August 10, 2012, which identified natural
attenuation as the most cost-effective means to remediate petroleum-impacted soil and
groundwater at the former Dietz Trucking Terminal site. The CAP was approved by DEQ in an
NORR letter dated August 20, 2012.

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2.0 Summary of Potential Receptor Information

2.1 Water Supply Wells

H&H conducted a water supply well survey for the area within a 1,500-ft radius of the former
UST basin during the Phase I and II LSA and updated during the limited CSA activities, as
necessary. The survey was conducted by performing area reconnaissance and checking for
municipal water connections. H&H also conducted an extended survey of properties within
500 ft of the UST area, which included contacts with knowledgeable personnel at those adjacent
properties with structures present.

The results of the survey indicated that city water is available to properties within a 1,500-foot
radius of the site. Eleven water supply wells were identified at or within 1,000 ft of the source
area. Of these, eight are utilized for drinking water and three are not used.

The approximate water supply well locations are depicted on Figure 3, and supply well owner
information and well specifics are presented in Table 1.

2.2 Surface Water

The closest surface water body is an unnamed intermittent stream located approximately 300 ft
southwest of the source area. Henry Fork River is located approximately 2,500 ft south of the
source area. Henry Fork River is designated as a “Class C” surface water body in the vicinity of
the site.

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3.0 Groundwater Monitoring

3.1 Water Levels

On October 19 and 20, 2017, the depths to groundwater were measured in monitoring wells
TMW-1, MW-2, MW-3, MW-4, and DMW-1 (Table 2). Depths to groundwater at the site were
approximately 14 to 14 ft below ground surface. No free product was detected in the monitoring
wells during gauging.

Calculated groundwater elevations are presented on Figure 4. Based on these data, the estimated
shallow groundwater flow is to the southwest at the subject property.

3.2 Monitoring Well and Water Supply Well Analytical Data

On October 19 and 20, 2017, groundwater samples were collected from monitoring wells TMW-
1, MW-2, MW-3, MW-4, and DMW-1. Prior to sampling, the wells were purged until pH,
temperature, and conductivity stabilized. Groundwater samples were then collected using
dedicated polyethylene bailers, poured in laboratory supplied containers marked with identifying
labels, and placed in an iced cooler for shipment under chain-of-custody protocol to a certified
laboratory for analyses.

The groundwater samples were analyzed for EPA Method 602 volatile organic compounds
(VOCs) by EPA Method 6200B and semi-VOCs by EPA Method 625. The chain-of-custody
records and laboratory analytical data sheets are provided in Appendix A.

As shown in Table 3, 1-methylnaphthalene and 2-methylnaphthalene were detected above the
groundwater standards in TMW-1. No compound concentrations exceeded their DEQ-defined
GCLs in TMW-1. Additionally, no compound concentrations were detected above the
groundwater standards in the remaining monitoring wells.

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Water supply wells WSW-1 and WSW-6 also were sampled on October 19, 2017. The supply
well samples were collected after allowing the water to run for approximately 15 minutes. The
water supply well samples were analyzed for EPA Method 602 VOCs by EPA Method 6200B
(Appendix A). No compound concentrations were detected above laboratory detection limits in
the water supply well samples (Table 3).

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4.0 Conclusions and Recommendations

Groundwater sampling activities were conducted in October 2017 at the former Dietz trucking
terminal. The activities included sampling five groundwater monitoring wells (TMW-1, MW-2
MW-3, MW-4, and DMW-1) and two water supply wells (WSW-1 and WSW-6). The sampling
results indicate:

• Petroleum compounds were detected above the North Carolina groundwater standards in
monitoring well TMW-1. No concentrations exceed GCLs and no free product was
detected in any of the monitoring wells. The horizontal and vertical extent of
groundwater impacts above standards is well defined and is limited to a small area in the
area of the former diesel UST.

• No target compounds were detected above laboratory detection limits in water supply
wells WSW-1 and WSW-6.

Based on the current and historical groundwater sampling results, H&H recommends continuing
a monitored natural attenuation approach for the subject site. Once compound concentration
degradation trends can be established, a risk-based closure should be warranted for the site. The
site monitoring wells should continue to be sampled on an annual basis for VOCs by EPA
Method 602 and semi-VOCs by EPA Method 625. In addition, the water supply wells WSW-1
and WSW-6 should be sampled for VOCs by EPA Method 602 only.

WSW-1 Rose Dietz 8814 Dietz Ave
Hickory, NC 28601
c/o Alan Dietz
800-438-8244 x3013 Yes Drinking Unknown Unknown Unknown 530 Northeast
WSW-2 Kent Anderson 3905 Brittain Street
Hickory, NC 28602 828-397-6841 Yes Drinking 20 None None 560 Northwest
WSW-3 Julia Jones 3895 Brittain Street
Hickory, NC 28602 Unknown Yes Drinking Unknown Unknown Unknown 660 North
WSW-4 Phyllis Yost 3955 Martin Fish Pond Road
Hickory, NC 28602 828-396-5717 Not since
2006 Drinking >200 Unknown Unknown 660 West
WSW-5 Dorothy Franklin 3900 Brittain Street
Hickory, NC 28602 828-397-3246 Yes Drinking 40 None None 770 Northwest
WSW-6 Boyd Lail 4130 Countryside Drive
Hickory, NC 28602 828-397-3951 Yes Drinking 52 None None 810 Southwest
WSW-7 Peter Rhyne 3945 Martin Fish Pond Road
Hickory, NC 28602 828-397-3884 Yes Drinking Unknown Unknown Unknown 820 Northwest
WSW-8 Dale Clark 4055 Martin Fish Pond Road
Hickory, NC 28602 828-397-3574 No; City
water in use Inactive Unknown Unknown Unknown 860 Southwest
WSW-9 Kenneth Baker 3890 Brittain Street
Hickory, NC 28602 828-397-2496 Yes Drinking 50 None None 870 North
WSW-10 Girthie Teague 3975 Martin Fish Pond Road
Hickory, NC 28602 828-397-3488 Yes Drinking 175 Unknown None 930 West
WSW-11 Judy Evans 8850 Dietz Avenue Hickory, NC 28602 828-495-4176 No; City water in use Inactive Uknown Unknown None 1,000 Northeast
Notes:Information taken from Burke County, NC Website and interviews with land owners.
Refer to Figure 3 for locations.
Table 1
Receptor Information
Former Dietz Trucking Terminal
Hickory, North Carolina
Figure 3
Map ID
H&H Job No. ROS-001
Location
Relative to SiteWell Owner Address Type of
Well
Well Screen
Interval (ft bgs)
Distance
from Source Area (ft)
Well Casing
Depth (ft bgs)
Well Depth
(ft bgs)Well In UsePhone Number
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9/21/2018
Table 1 (Page 1 of 1)Hart & Hickman, PC
Table 2
Summary of Groundwater Level Data
Former Dietz Trucking Terminal
Hickory, North Carolina
H&H Job No. ROS-001
Well ID Date
Installed
TOC
Elevation
Total Depth
(ft)
Screen
Length (ft)
Approximate
Screened Interval
(ft)
Depth to
Water from
TOC (ft)
GW Elevation
(ft)
10/27/10 14.66 85.34
12/03/12 15.46 84.54
02/25/14 12.35 87.65
08/12/15 12.91 87.65
10/24/16 14.40 85.60
10/20/17 13.43 86.57
12/20/10 15.03 84.29
12/03/12 15.76 83.56
02/25/14 12.66 86.66
08/12/15 13.22 86.10
10/25/16 14.83 84.49
10/19/17 13.69 85.63
12/20/10 15.66 84.70
12/03/12 16.47 83.89
02/25/14 13.27 87.09
08/12/15 13.83 86.53
10/25/16 15.53 84.83
10/19/17 14.44 85.92
12/20/10 13.91 85.71
12/03/12 14.70 84.92
02/25/14 11.79 87.83
08/12/15 12.35 87.27
10/25/16 13.74 85.88
10/19/17 12.81 86.81
08/14/11 16.88 NA
12/03/12 16.03 NA
02/25/14 12.84 NA
08/12/15 14.20 NA
10/25/16 15.08 NA
10/19/17 14.03 NA
Notes:
TOC = Top of Casing Elevation
DMW-1
MW-4
MW-3
MW-2
TMW-1
57
99.62
NM 5 52-57
7-22
27
22
15
15
1522 7-22
7-22
12-27100.00
99.32
100.36
22 15
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Table 2 (Page 1 of 1)
Hart & Hickman, PC
MADEP VPH MADEP VPH MADEP EPH MADEP VPH/EPH MADEP EPH MADEP VPH MADEP EPH MADEP VPH/EPH 602 602 602 602 625 625 625 625 625
Sample ID
Date
Collected
Incident
Phase
10/27/10 LSA 160 1,180 11,100 12,280 1,990 1,380 8,250 9,630 33.4 NA 1.13 28.8 15.8 161 30.9 NA NA
8/4/11*CSA <50 54 5,500 5,554 1,500 1,000 6,200 7,200 NA NA NA NA 15 78 33 NA NA
12/03/12 MNA <50 190 9,000 9,190 2,700 580 14,000 14,580 21 260 <1.0 4.0 18 85 31 110 150
2/25/142 MNA <100 <100 3,870 3,870 771 <100 5,440 5,440 18.3 106 <1.0 7.0 7.4 112 10.5 NA NA
08/12/15 MNA 58 340 6,300 6,640 2,300 600 7,400 8,000 25 190 <1.0 8.6 15 140 25 140 190
10/25/16 MNA NA NA NA NA NA NA NA NA 32 190 <1.0 14 12 98 16 110 140
10/20/175 MNA NA NA NA NA NA NA NA NA 61 390 <1.0 24 11 180 16 150 210
12/20/10 LSA <100 <100 <100 BDL <105 <100 <105 BDL <1 NA <1 <3 <10 <10 <10 NA <10
8/4/11*CSA <50 <50 <100 BDL <100 <50 <100 BDL NA NA NA NA <10 <10 <10 NA <10
12/03/12 MNA <50 <50 <100 BDL <100 <50 <100 BDL <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
02/25/14 MNA <50 <50 <105 BDL <105 <50 <105 BDL <1.0 <2.0 <1.0 <3.0 <5.0 <5.0 <5.0 NA NA
08/12/15 MNA <50 <50 <350 BDL <500 <50 <100 BDL <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
10/25/164 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
10/19/17 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 <11 <11 <11 <11 <11
12/20/10 LSA <100 <100 <100 BDL <100 <100 <100 BDL <1 NA <1 <3 <10 <10 <10 NA <10
8/4/2011*CSA <50 <50 <100 BDL <100 <50 <100 BDL NA NA NA NA <10 <10 <10 NA <10
12/03/12 MNA <50 <50 <100 BDL <100 <50 <100 BDL <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
02/25/14 MNA <50 <50 <112 BDL <112 <50 <112 BDL <1.0 <2.0 <1.0 <3.0 <5.0 <5.0 <5.0 NA NA
08/12/15 MNA <50 <50 <350 BDL <500 <50 <100 BDL <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
10/25/16 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
10/19/17 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 <11 <11 <11 <11 <11
420 NS NS 4,200 42,000 NS NS 210 600 6 600 500 300 6 200 1 30
NS NS NS NS NS NS NS NS 84,500 6,000 260,000 85,500 990 6,000 410 1,000 12,500
Notes:Apart from VPH and EPH, only those compounds detected are shown.Bold indicates concentration exceeds 2L standard
2L Standard = NCAC 2L groundwater quality standard GCL = gross contaminant levelMADEP = Massachusetts Department of Environmental Protection
VPH = Volatile Petroleum Hydrocarbon; EPH = Extractable Petroleum HydrocarbonNS = No Standard NA= Not Analyzed; LSA = Limited Site Assessment; CSA = Comprehensive Site Assessment; MNA = Monitored Natural Attenuation
* - Due to a laboratory error, EPA Method 625 samples collected on September 8, 2011. 1 - 37 µg/l of bis(2-ethylhexyl)phthalate also detected in well on December 3, 2012. 2 - 5.2 µg/l of isopropylbenzene also detected in well on February 25, 2014. 3 - 14 µg/l of diethyl phthalate also detected in well on August 12, 2015.
4 - 15 µg/l of pentachlorophenol also detected in well on October 28, 2016. 5 - 0.95 µg/l of benzene also detected in well on October 20, 2017.
H&H Job No. ROS-001
VPH C5-C8 Aliphatics Ethylbenzene2-MethylnaphthaleneTotal C9-C22 AromaticsMW-2 VPH C9-C10 Aromatics VPH C9-C12 Aliphatics XylenesMW-3
Table 3 (Page 1 of 2)
Summary of Groundwater Sampling Results
Former Dietz Trucking Terminal
Hickory, North Carolina
PhenanthreneAnalytical Method
TMW-1 EPH C19-C36 Aliphatics EPH C9-C18 Aliphatics GCL (µg/l)
Contaminant of Concern
2L Standard (µg/l)EPH C11-C22 Aromatics Total C9-C18 Aliphatics1-MethylnaphthaleneNaphthaleneFluoreneTolueneNaphthaleneS:\AAA-Master Projects\Dietz Trucking (ROS-001)\Sampling\0917\Table\ROS-001PreCAPTables9/21/2018
Table 3 (Page 1 of 3)
Hart & Hickman, PC
MADEP VPH MADEP VPH MADEP EPH MADEP VPH/EPH MADEP EPH MADEP VPH MADEP EPH MADEP VPH/EPH 602 602 602 602 625 625 625 625 625
Sample ID Date Collected Incident Phase
12/20/10 LSA <100 <100 <100 BDL <100 <100 <100 BDL <1 NA <1 <3 <10 <10 <10 NA <10
8/4/11*LSA <50 <50 <100 BDL <100 <50 <100 BDL NA NA NA NA <10 <10 <10 NA <10
12/03/12 MNA <50 <50 <100 BDL <100 <50 <100 BDL <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
02/25/14 MNA <50 <50 <104 BDL <104 <50 <104 BDL <1.0 <2.0 <1.0 <3.0 <5.0 <5.0 <5.0 NA NA
8/12/153 MNA <50 <50 <350 BDL <500 <50 <100 BDL <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
10/25/16 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
10/19/17 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 <11 <11 <11 <11 <11
8/4/11*LSA <50 <50 <100 BDL <100 <50 <100 BDL <1 NA <1 <3 <10 <10 <10 NA <10
12/3/121 MNA <50 <50 <100 BDL <100 <50 <100 BDL <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
02/25/14 MNA <50 <50 <110 BDL <110 <50 <110 BDL <1.0 <2.0 <1.0 <3.0 <5.0 <5.0 <5.0 NA NA
08/12/15 MNA <50 <50 <350 BDL <500 <50 <100 BDL <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
10/25/16 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 <10 <10 <10 <10 <10
10/19/17 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 <11 <11 <11 <11 <11
10/27/10 LSA <100 <100 <105 BDL <105 <100 <105 BDL <1 NA <1 <3 <10 <10 <10 NA <10
12/03/12 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 NA NA NA NA NA
02/25/14 MNA NA NA NA NA NA NA NA NA <1.0 <2.0 <1.0 <3.0 NA NA NA NA NA
08/12/15 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 NA NA NA NA NA
10/25/16 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 NA NA NA NA NA
10/19/17 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 NA NA NA NA NA
08/03/11 CSA NA NA NA NA NA NA NA NA <1 NA <1 <3 NA NA NA NA NA
02/25/14 MNA NA NA NA NA NA NA NA NA <1.0 <2.0 <1.0 <3.0 NA NA NA NA NA
08/04/11 CSA NA NA NA NA NA NA NA NA <1 NA <1 <3 NA NA NA NA NA
12/03/12 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 NA NA NA NA NA
02/25/14 MNA NA NA NA NA NA NA NA NA <1.0 <2.0 <1.0 <3.0 NA NA NA NA NA
08/12/15 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 NA NA NA NA NA
10/25/16 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 NA NA NA NA NA
10/19/17 MNA NA NA NA NA NA NA NA NA <1.0 <5.0 <1.0 <3.0 NA NA NA NA NA
420 NS NS 4,200 42,000 NS NS 210 600 6 600 500 300 6 200 1 30
NS NS NS NS NS NS NS NS 84,500 6,000 260,000 85,500 990 6,000 410 1,000 12,500
Notes:Apart from VPH and EPH, only those compounds detected are shown.Bold indicates concentration exceeds 2L standard
2L Standard = NCAC 2L groundwater quality standard GCL = gross contaminant levelMADEP = Massachusetts Department of Environmental ProtectionVPH = Volatile Petroleum Hydrocarbon; EPH = Extractable Petroleum HydrocarbonNS = No Standard NA= Not Analyzed; LSA = Limited Site Assessment; CSA = Comprehensive Site Assessment; MNA = Monitored Natural Attenuation* - Due to a laboratory error, EPA Method 625 samples collected on September 8, 2011. 1 - 37 µg/l of bis(2-ethylhexyl)phthalate also detected in well on December 3, 2012. 2 - 5.2 µg/l of isopropylbenzene also detected in well on February 25, 2014.
WSW-4
WSW-6
2L Standard (µg/l)
GCL (µg/l)
MW-4
DMW-1
WSW-1 XylenesFluoreneNaphthalenePhenanthrene1-Methylnaphthalene2-MethylnaphthaleneVPH C9-C10 Aromatics EPH C11-C22 Aromatics Total C9-C22 AromaticsEthylbenzeneNaphthaleneTolueneContaminant of Concern
VPH C5-C8 Aliphatics VPH C9-C12 Aliphatics EPH C9-C18 Aliphatics Total C9-C18 AliphaticsEPH C19-C36 Aliphatics Table 3 (Page 2 of 2)Summary of Groundwater Sampling Results
Former Dietz Trucking Terminal
Hickory, North Carolina
H&H Job No. ROS-001
Analytical Method
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Table 3 (Page 2 of 3)Hart & Hickman, PC
TITLE
PROJECT
SITE LOCATION MAP
FORMER DIETZ TRUCKING TERMINALHICKORY, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
8-28-18 0
1ROS-001
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
LONGVIEW, NC 1993
SITE
DIE
T
Z

A
V
E
I-40
E
A
S
T
B
O
U
N
D
I-40
W
E
S
T
B
O
U
N
D
SITE MAP
FORMER DIETZ TRUCKING
8814 DIETZ AVE
HICKORY, NC
TRUCKING
TERMINAL
GARAGE
ASPHALT
LOT
GRAVEL
TURN-AROUND
CONC
R
E
T
E
A
P
R
O
N
ASPHALT LOT
ASPHALT LOT
FORMER UST #2
LOCATION
WSW-1
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
S:\AAA-Master Projects\Dietz Trucking (ROS-001)\Sampling\0917\Figures\FIG-2.dwg, FIG 2, 9/21/2018 2:54:08 PM,
1000
1500
500
WATER SUPPLY WELL SURVEY AND ADJACENT
PROPERTY OWNERS MAP
FORMER DIETZ TRUCKING
8814 DIETZ AVE
HICKORY, NC
WSW-3
WSW-1
WSW-5
WSW-2WSW-7
WSW-4
WSW-6
WSW-10
WSW-9
WSW-8
WSW-11
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
S:\AAA-Master Projects\Dietz Trucking (ROS-001)\Sampling\0917\Figures\FIG-3.dwg, FIG-3B, 9/21/2018 2:54:58 PM,
MW-4
TMW-1
MW-2
MW-3
DMW-1
MONITORING WELL LOCATIONS AND
GROUNDWATER ELEVATIONS MAP
FORMER DIETZ TRUCKING
8814 DIETZ AVE
HICKORY, NC
GARAGE
ASPHALT LOT
LIMITS OF UST EXCAVATION
ASPHALT LOT
BUILDING
DIRT SLOPE
(86.81)
63.04
(86.81)
(85.92)
86.
5
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
85.0
(86.57)
(85.63)
86.
0
S:\AAA-Master Projects\Dietz Trucking (ROS-001)\Sampling\0917\Figures\FIG-4.dwg, FIG 3, 9/21/2018 2:55:44 PM,

Appendix A

Laboratory Analytical Data
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
10/30/2017
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: ROS-001 Former Dietz Trucking
Lab Submittal Date: 10/19/2017
Prism Work Order: 7100385
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash
President/Project Manager
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
L Parameter reported with possible low bias. LCS recovery below the QC limit.
SE Surrogate recovery outside the QC limits due to emulsion.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 25
Sample Receipt Summary
10/30/2017
Prism Work Order: 7100385
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7100385-01 10/19/17DMW-1 10/19/17Water
7100385-02 10/19/17MW-4 10/19/17Water
7100385-03 10/19/17MW-3 10/19/17Water
7100385-04 10/19/17MW-2 10/19/17Water
7100385-05 10/19/17WSW-1 10/19/17Water
7100385-06 10/19/17WSW-6 10/19/17Water
Samples were received in good condition at 2.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 25
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7100385
10/30/2017
Summary of Detections
13 ug/L7100385-01 DMW-1 Docosene *625
13 ug/L7100385-03 MW-3 Docosene *625
17 ug/L7100385-03 MW-3 Hexadecanoic acid *625
25 ug/L7100385-03 MW-3 Unknown 1 *625
11 ug/L7100385-04 MW-2 Hexadecanoic acid *625
350 ug/L7100385-04 MW-2 Unknown 1 *625
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: DMW-1
Prism Sample ID: 7100385-01
Prism Work Order: 7100385
Time Collected: 10/19/17 10:20
Time Submitted: 10/19/17 13:35
Semivolatile Organic Compounds by GC/MS
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.61,2,4-Trichlorobenzene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.51,2-Dichlorobenzene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.41,3-Dichlorobenzene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.51,4-Dichlorobenzene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.31-Methylnaphthalene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.02,4,6-Trichlorophenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.72,4-Dichlorophenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.32,4-Dimethylphenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.32,4-Dinitrophenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.22,4-Dinitrotoluene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.22,6-Dinitrotoluene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.52-Chloronaphthalene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.22-Chlorophenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.02-Methylnaphthalene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.52-Nitrophenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.03,3’-Dichlorobenzidine
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.23/4-Methylphenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.14,6-Dinitro-2-methylphenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.44-Bromophenyl phenyl ether
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.54-Chloro-3-methylphenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.84-Chloroaniline
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.44-Chlorophenyl phenyl ether
BRL *625 P7J043115410/24/17 22:37 JMVug/L 1.84-Nitrophenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.5Acenaphthene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.5Acenaphthylene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.4Anthracene
BRL *625 P7J0431111010/24/17 22:37 JMVug/L 15Benzidine
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.4Benzo(a)anthracene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.9Benzo(a)pyrene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.8Benzo(b)fluoranthene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.8Benzo(g,h,i)perylene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 4.2Benzo(k)fluoranthene
BRL *625 P7J0431111010/24/17 22:37 JMVug/L 0.80Benzoic Acid
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.8Benzyl alcohol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.9bis(2-Chloroethoxy)methane
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.8Bis(2-Chloroethyl)ether
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.8Bis(2-chloroisopropyl)ether
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.4Bis(2-Ethylhexyl)phthalate
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.8Butyl benzyl phthalate
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.7Chrysene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.7Dibenzo(a,h)anthracene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.5Dibenzofuran
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: DMW-1
Prism Sample ID: 7100385-01
Prism Work Order: 7100385
Time Collected: 10/19/17 10:20
Time Submitted: 10/19/17 13:35
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.5Diethyl phthalate
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.7Dimethyl phthalate
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.6Di-n-butyl phthalate
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.9Di-n-octyl phthalate
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.8Fluoranthene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.0Fluorene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.7Hexachlorobenzene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.2Hexachlorobutadiene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.8Hexachlorocyclopentadiene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.6Hexachloroethane
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.3Indeno(1,2,3-cd)pyrene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.3Isophorone
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.2Naphthalene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 1.5Nitrobenzene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 0.90N-Nitrosodimethylamine
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.2N-Nitroso-di-n-propylamine
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.2N-Nitrosodiphenylamine
BRL *625 P7J043111110/24/17 22:37 JMVug/L 2.3Pentachlorophenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.5Phenanthrene
BRL *625 P7J043111110/24/17 22:37 JMVug/L 0.52Phenol
BRL *625 P7J043111110/24/17 22:37 JMVug/L 3.8Pyrene
13 *625 P7J0431110/24/17 22:37 JMVug/LTIC: Docosene
Surrogate Recovery Control Limits
31-14469 %2,4,6-Tribromophenol
49-11870 %2-Fluorobiphenyl
22-8449 %2-Fluorophenol
43-12366 %Nitrobenzene-d5
10-6334 %Phenol-d5
49-15177 %Terphenyl-d14
Volatile Organic 602 Compounds by GC/MS
BRL *SM6200 B P7J038710.50 10/22/17 5:39 KDMug/L 0.048Benzene
BRL *SM6200 B P7J038711.0 10/22/17 5:39 KDMug/L 0.061Ethylbenzene
BRL *SM6200 B P7J038715.0 10/22/17 5:39 KDMug/L 0.050Isopropyl Ether
BRL *SM6200 B P7J038712.0 10/22/17 5:39 KDMug/L 0.12m,p-Xylenes
BRL *SM6200 B P7J038715.0 10/22/17 5:39 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P7J038715.0 10/22/17 5:39 KDMug/L 0.19Naphthalene
BRL *SM6200 B P7J038711.0 10/22/17 5:39 KDMug/L 0.044o-Xylene
BRL *SM6200 B P7J038711.0 10/22/17 5:39 KDMug/L 0.044Toluene
BRL *SM6200 B P7J038713.0 10/22/17 5:39 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-4
Prism Sample ID: 7100385-02
Prism Work Order: 7100385
Time Collected: 10/19/17 10:50
Time Submitted: 10/19/17 13:35
Semivolatile Organic Compounds by GC/MS
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.61,2,4-Trichlorobenzene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.61,2-Dichlorobenzene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.51,3-Dichlorobenzene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.51,4-Dichlorobenzene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.31-Methylnaphthalene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.02,4,6-Trichlorophenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.72,4-Dichlorophenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.32,4-Dimethylphenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.42,4-Dinitrophenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.32,4-Dinitrotoluene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.32,6-Dinitrotoluene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.62-Chloronaphthalene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.22-Chlorophenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.12-Methylnaphthalene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.52-Nitrophenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.13,3’-Dichlorobenzidine
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.33/4-Methylphenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.14,6-Dinitro-2-methylphenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.54-Bromophenyl phenyl ether
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.54-Chloro-3-methylphenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.94-Chloroaniline
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.54-Chlorophenyl phenyl ether
BRL *625 P7J043115610/24/17 23:00 JMVug/L 1.94-Nitrophenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.6Acenaphthene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.6Acenaphthylene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.5Anthracene
BRL *625 P7J0431111010/24/17 23:00 JMVug/L 15Benzidine
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.5Benzo(a)anthracene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 4.0Benzo(a)pyrene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.9Benzo(b)fluoranthene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.9Benzo(g,h,i)perylene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 4.2Benzo(k)fluoranthene
BRL *625 P7J0431111010/24/17 23:00 JMVug/L 0.82Benzoic Acid
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.8Benzyl alcohol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.0bis(2-Chloroethoxy)methane
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.8Bis(2-Chloroethyl)ether
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.9Bis(2-chloroisopropyl)ether
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.5Bis(2-Ethylhexyl)phthalate
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.9Butyl benzyl phthalate
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.8Chrysene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.8Dibenzo(a,h)anthracene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.6Dibenzofuran
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-4
Prism Sample ID: 7100385-02
Prism Work Order: 7100385
Time Collected: 10/19/17 10:50
Time Submitted: 10/19/17 13:35
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.6Diethyl phthalate
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.7Dimethyl phthalate
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.7Di-n-butyl phthalate
BRL *625 P7J043111110/24/17 23:00 JMVug/L 4.0Di-n-octyl phthalate
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.9Fluoranthene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.1Fluorene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.7Hexachlorobenzene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.3Hexachlorobutadiene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.8Hexachlorocyclopentadiene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.7Hexachloroethane
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.4Indeno(1,2,3-cd)pyrene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.4Isophorone
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.3Naphthalene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 1.5Nitrobenzene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 0.92N-Nitrosodimethylamine
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.3N-Nitroso-di-n-propylamine
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.2N-Nitrosodiphenylamine
BRL *625 P7J043111110/24/17 23:00 JMVug/L 2.3Pentachlorophenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.5Phenanthrene
BRL *625 P7J043111110/24/17 23:00 JMVug/L 0.53Phenol
BRL *625 P7J043111110/24/17 23:00 JMVug/L 3.9Pyrene
Not
Detected
*625 P7J0431110/24/17 23:00 JMVug/LTIC: Tentatively Identified Compounds
Surrogate Recovery Control Limits
31-14472 %2,4,6-Tribromophenol
49-11868 %2-Fluorobiphenyl
22-8451 %2-Fluorophenol
43-12365 %Nitrobenzene-d5
10-6334 %Phenol-d5
49-15177 %Terphenyl-d14
Volatile Organic 602 Compounds by GC/MS
BRL *SM6200 B P7J038710.50 10/22/17 6:12 KDMug/L 0.048Benzene
BRL *SM6200 B P7J038711.0 10/22/17 6:12 KDMug/L 0.061Ethylbenzene
BRL *SM6200 B P7J038715.0 10/22/17 6:12 KDMug/L 0.050Isopropyl Ether
BRL *SM6200 B P7J038712.0 10/22/17 6:12 KDMug/L 0.12m,p-Xylenes
BRL *SM6200 B P7J038715.0 10/22/17 6:12 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P7J038715.0 10/22/17 6:12 KDMug/L 0.19Naphthalene
BRL *SM6200 B P7J038711.0 10/22/17 6:12 KDMug/L 0.044o-Xylene
BRL *SM6200 B P7J038711.0 10/22/17 6:12 KDMug/L 0.044Toluene
BRL *SM6200 B P7J038713.0 10/22/17 6:12 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130108 %4-Bromofluorobenzene
70-130113 %Dibromofluoromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-4
Prism Sample ID: 7100385-02
Prism Work Order: 7100385
Time Collected: 10/19/17 10:50
Time Submitted: 10/19/17 13:35
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-3
Prism Sample ID: 7100385-03
Prism Work Order: 7100385
Time Collected: 10/19/17 11:05
Time Submitted: 10/19/17 13:35
Semivolatile Organic Compounds by GC/MS
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.61,2,4-Trichlorobenzene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.51,2-Dichlorobenzene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.41,3-Dichlorobenzene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.51,4-Dichlorobenzene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.31-Methylnaphthalene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.02,4,6-Trichlorophenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.72,4-Dichlorophenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.32,4-Dimethylphenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.32,4-Dinitrophenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.22,4-Dinitrotoluene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.22,6-Dinitrotoluene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.52-Chloronaphthalene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.22-Chlorophenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.02-Methylnaphthalene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.52-Nitrophenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.03,3’-Dichlorobenzidine
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.23/4-Methylphenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.14,6-Dinitro-2-methylphenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.44-Bromophenyl phenyl ether
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.54-Chloro-3-methylphenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.84-Chloroaniline
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.44-Chlorophenyl phenyl ether
BRL *625 P7J043115410/24/17 23:22 JMVug/L 1.84-Nitrophenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.5Acenaphthene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.5Acenaphthylene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.4Anthracene
BRL *625 P7J0431111010/24/17 23:22 JMVug/L 15Benzidine
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.4Benzo(a)anthracene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.9Benzo(a)pyrene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.8Benzo(b)fluoranthene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.8Benzo(g,h,i)perylene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 4.2Benzo(k)fluoranthene
BRL *625 P7J0431111010/24/17 23:22 JMVug/L 0.80Benzoic Acid
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.8Benzyl alcohol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.9bis(2-Chloroethoxy)methane
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.8Bis(2-Chloroethyl)ether
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.8Bis(2-chloroisopropyl)ether
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.4Bis(2-Ethylhexyl)phthalate
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.8Butyl benzyl phthalate
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.7Chrysene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.7Dibenzo(a,h)anthracene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.5Dibenzofuran
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-3
Prism Sample ID: 7100385-03
Prism Work Order: 7100385
Time Collected: 10/19/17 11:05
Time Submitted: 10/19/17 13:35
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.5Diethyl phthalate
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.7Dimethyl phthalate
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.6Di-n-butyl phthalate
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.9Di-n-octyl phthalate
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.8Fluoranthene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.0Fluorene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.7Hexachlorobenzene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.2Hexachlorobutadiene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.8Hexachlorocyclopentadiene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.6Hexachloroethane
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.3Indeno(1,2,3-cd)pyrene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.3Isophorone
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.2Naphthalene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 1.5Nitrobenzene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 0.90N-Nitrosodimethylamine
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.2N-Nitroso-di-n-propylamine
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.2N-Nitrosodiphenylamine
BRL *625 P7J043111110/24/17 23:22 JMVug/L 2.3Pentachlorophenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.5Phenanthrene
BRL *625 P7J043111110/24/17 23:22 JMVug/L 0.52Phenol
BRL *625 P7J043111110/24/17 23:22 JMVug/L 3.8Pyrene
13 *625 P7J0431110/24/17 23:22 JMVug/LTIC: Docosene
17 *625 P7J0431110/24/17 23:22 JMVug/LTIC: Hexadecanoic acid
25 *625 P7J0431110/24/17 23:22 JMVug/LTIC: Unknown 1
Surrogate Recovery Control Limits
31-14464 %2,4,6-Tribromophenol
49-11875 %2-Fluorobiphenyl
22-8455 %2-Fluorophenol
43-12373 %Nitrobenzene-d5
10-6335 %Phenol-d5
49-15180 %Terphenyl-d14
Volatile Organic 602 Compounds by GC/MS
BRL *SM6200 B P7J038710.50 10/22/17 6:46 KDMug/L 0.048Benzene
BRL *SM6200 B P7J038711.0 10/22/17 6:46 KDMug/L 0.061Ethylbenzene
BRL *SM6200 B P7J038715.0 10/22/17 6:46 KDMug/L 0.050Isopropyl Ether
BRL *SM6200 B P7J038712.0 10/22/17 6:46 KDMug/L 0.12m,p-Xylenes
BRL *SM6200 B P7J038715.0 10/22/17 6:46 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P7J038715.0 10/22/17 6:46 KDMug/L 0.19Naphthalene
BRL *SM6200 B P7J038711.0 10/22/17 6:46 KDMug/L 0.044o-Xylene
BRL *SM6200 B P7J038711.0 10/22/17 6:46 KDMug/L 0.044Toluene
BRL *SM6200 B P7J038713.0 10/22/17 6:46 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-3
Prism Sample ID: 7100385-03
Prism Work Order: 7100385
Time Collected: 10/19/17 11:05
Time Submitted: 10/19/17 13:35
70-130107 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-2
Prism Sample ID: 7100385-04
Prism Work Order: 7100385
Time Collected: 10/19/17 11:20
Time Submitted: 10/19/17 13:35
Semivolatile Organic Compounds by GC/MS
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.61,2,4-Trichlorobenzene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.51,2-Dichlorobenzene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.51,3-Dichlorobenzene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.51,4-Dichlorobenzene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.31-Methylnaphthalene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.02,4,6-Trichlorophenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.72,4-Dichlorophenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.32,4-Dimethylphenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.42,4-Dinitrophenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.22,4-Dinitrotoluene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.22,6-Dinitrotoluene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.62-Chloronaphthalene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.22-Chlorophenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.02-Methylnaphthalene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.52-Nitrophenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.03,3’-Dichlorobenzidine
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.33/4-Methylphenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.14,6-Dinitro-2-methylphenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.54-Bromophenyl phenyl ether
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.54-Chloro-3-methylphenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.84-Chloroaniline
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.44-Chlorophenyl phenyl ether
BRL *625 P7J043115510/24/17 23:45 JMVug/L 1.84-Nitrophenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.5Acenaphthene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.5Acenaphthylene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.5Anthracene
BRL *625 P7J0431111010/24/17 23:45 JMVug/L 15Benzidine
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.4Benzo(a)anthracene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 4.0Benzo(a)pyrene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.9Benzo(b)fluoranthene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.8Benzo(g,h,i)perylene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 4.2Benzo(k)fluoranthene
BRL *625 P7J0431111010/24/17 23:45 JMVug/L 0.81Benzoic Acid
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.8Benzyl alcohol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.0bis(2-Chloroethoxy)methane
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.8Bis(2-Chloroethyl)ether
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.8Bis(2-chloroisopropyl)ether
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.4Bis(2-Ethylhexyl)phthalate
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.8Butyl benzyl phthalate
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.7Chrysene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.7Dibenzo(a,h)anthracene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.5Dibenzofuran
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-2
Prism Sample ID: 7100385-04
Prism Work Order: 7100385
Time Collected: 10/19/17 11:20
Time Submitted: 10/19/17 13:35
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.5Diethyl phthalate
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.7Dimethyl phthalate
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.7Di-n-butyl phthalate
BRL *625 P7J043111110/24/17 23:45 JMVug/L 4.0Di-n-octyl phthalate
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.8Fluoranthene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.1Fluorene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.7Hexachlorobenzene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.2Hexachlorobutadiene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.8Hexachlorocyclopentadiene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.6Hexachloroethane
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.4Indeno(1,2,3-cd)pyrene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.3Isophorone
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.3Naphthalene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 1.5Nitrobenzene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 0.91N-Nitrosodimethylamine
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.2N-Nitroso-di-n-propylamine
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.2N-Nitrosodiphenylamine
BRL *625 P7J043111110/24/17 23:45 JMVug/L 2.3Pentachlorophenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.5Phenanthrene
BRL *625 P7J043111110/24/17 23:45 JMVug/L 0.53Phenol
BRL *625 P7J043111110/24/17 23:45 JMVug/L 3.8Pyrene
11 *625 P7J0431110/24/17 23:45 JMVug/LTIC: Hexadecanoic acid
350 *625 P7J0431110/24/17 23:45 JMVug/LTIC: Unknown 1
Surrogate Recovery Control Limits
31-1445 %2,4,6-Tribromophenol SE
49-11867 %2-Fluorobiphenyl
22-841 %2-Fluorophenol SE
43-12360 %Nitrobenzene-d5
10-630.7 %Phenol-d5 SE
49-15176 %Terphenyl-d14
Volatile Organic 602 Compounds by GC/MS
BRL *SM6200 B P7J038710.50 10/22/17 7:20 KDMug/L 0.048Benzene
BRL *SM6200 B P7J038711.0 10/22/17 7:20 KDMug/L 0.061Ethylbenzene
BRL *SM6200 B P7J038715.0 10/22/17 7:20 KDMug/L 0.050Isopropyl Ether
BRL *SM6200 B P7J038712.0 10/22/17 7:20 KDMug/L 0.12m,p-Xylenes
BRL *SM6200 B P7J038715.0 10/22/17 7:20 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P7J038715.0 10/22/17 7:20 KDMug/L 0.19Naphthalene
BRL *SM6200 B P7J038711.0 10/22/17 7:20 KDMug/L 0.044o-Xylene
BRL *SM6200 B P7J038711.0 10/22/17 7:20 KDMug/L 0.044Toluene
BRL *SM6200 B P7J038713.0 10/22/17 7:20 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130107 %4-Bromofluorobenzene
70-130101 %Dibromofluoromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-2
Prism Sample ID: 7100385-04
Prism Work Order: 7100385
Time Collected: 10/19/17 11:20
Time Submitted: 10/19/17 13:35
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: WSW-1
Prism Sample ID: 7100385-05
Prism Work Order: 7100385
Time Collected: 10/19/17 11:40
Time Submitted: 10/19/17 13:35
Volatile Organic 602 Compounds by GC/MS
BRL *SM6200 B P7J038710.50 10/22/17 7:53 KDMug/L 0.048Benzene
BRL *SM6200 B P7J038711.0 10/22/17 7:53 KDMug/L 0.061Ethylbenzene
BRL *SM6200 B P7J038715.0 10/22/17 7:53 KDMug/L 0.050Isopropyl Ether
BRL *SM6200 B P7J038712.0 10/22/17 7:53 KDMug/L 0.12m,p-Xylenes
BRL *SM6200 B P7J038715.0 10/22/17 7:53 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P7J038715.0 10/22/17 7:53 KDMug/L 0.19Naphthalene
BRL *SM6200 B P7J038711.0 10/22/17 7:53 KDMug/L 0.044o-Xylene
BRL *SM6200 B P7J038711.0 10/22/17 7:53 KDMug/L 0.044Toluene
BRL *SM6200 B P7J038713.0 10/22/17 7:53 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
70-130113 %Dibromofluoromethane
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 25
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz
Trucking
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: WSW-6
Prism Sample ID: 7100385-06
Prism Work Order: 7100385
Time Collected: 10/19/17 11:55
Time Submitted: 10/19/17 13:35
Volatile Organic 602 Compounds by GC/MS
BRL *SM6200 B P7J038710.50 10/22/17 8:27 KDMug/L 0.048Benzene
BRL *SM6200 B P7J038711.0 10/22/17 8:27 KDMug/L 0.061Ethylbenzene
BRL *SM6200 B P7J038715.0 10/22/17 8:27 KDMug/L 0.050Isopropyl Ether
BRL *SM6200 B P7J038712.0 10/22/17 8:27 KDMug/L 0.12m,p-Xylenes
BRL *SM6200 B P7J038715.0 10/22/17 8:27 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P7J038715.0 10/22/17 8:27 KDMug/L 0.19Naphthalene
BRL *SM6200 B P7J038711.0 10/22/17 8:27 KDMug/L 0.044o-Xylene
BRL *SM6200 B P7J038711.0 10/22/17 8:27 KDMug/L 0.044Toluene
BRL *SM6200 B P7J038713.0 10/22/17 8:27 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 25
10/30/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz TruckingHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Prism Work Order: 7100385
Time Submitted: 10/19/2017 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic 602 Compounds by GC/MS - Quality Control
Batch P7J0387 - SM6200 B
Blank (P7J0387-BLK1)Prepared: 10/21/17 Analyzed: 10/22/17
Benzene ug/LBRL0.50
Ethylbenzene ug/LBRL1.0
Isopropyl Ether ug/LBRL5.0
m,p-Xylenes ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL5.0
Naphthalene ug/LBRL5.0
o-Xylene ug/LBRL1.0
Toluene ug/LBRL1.0
Xylenes, total ug/LBRL3.0
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.4
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10351.6
ug/L 50.00 70-130Surrogate: Toluene-d8 9849.1
LCS (P7J0387-BS1)Prepared: 10/21/17 Analyzed: 10/22/17
Benzene ug/L21.2 0.50 20.00 70-130106
Ethylbenzene ug/L22.0 1.0 20.00 70-130110
Isopropyl Ether ug/L19.1 5.0 20.00 70-13096
m,p-Xylenes ug/L45.4 2.0 40.00 70-130113
Methyl-tert-Butyl Ether ug/L19.6 5.0 20.00 70-13098
Naphthalene ug/L19.9 5.0 20.00 70-13099
o-Xylene ug/L20.4 1.0 20.00 70-130102
Toluene ug/L21.8 1.0 20.00 70-130109
Xylenes, total ug/L65.7 3.0 60.00 70-130110
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9848.8
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9647.8
ug/L 50.00 70-130Surrogate: Toluene-d8 10049.8
LCS Dup (P7J0387-BSD1)Prepared: 10/21/17 Analyzed: 10/22/17
Benzene ug/L21.1 0.50 20.00 2070-130105 0.8
Ethylbenzene ug/L22.1 1.0 20.00 2070-130111 0.4
Isopropyl Ether ug/L19.2 5.0 20.00 2070-13096 0.6
m,p-Xylenes ug/L45.6 2.0 40.00 2070-130114 0.7
Methyl-tert-Butyl Ether ug/L20.1 5.0 20.00 2070-130100 2
Naphthalene ug/L20.4 5.0 20.00 2070-130102 3
o-Xylene ug/L21.2 1.0 20.00 2070-130106 4
Toluene ug/L21.7 1.0 20.00 2070-130109 0.3
Xylenes, total ug/L66.9 3.0 60.00 2070-130111 2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.8
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9849.2
ug/L 50.00 70-130Surrogate: Toluene-d8 10150.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 25
10/30/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz TruckingHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Prism Work Order: 7100385
Time Submitted: 10/19/2017 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0431 - 625
Blank (P7J0431-BLK1)Prepared & Analyzed: 10/24/17
1,2,4-Trichlorobenzene ug/LBRL10
1,2-Dichlorobenzene ug/LBRL10
1,3-Dichlorobenzene ug/LBRL10
1,4-Dichlorobenzene ug/LBRL10
1-Methylnaphthalene ug/LBRL10
2,4,6-Trichlorophenol ug/LBRL10
2,4-Dichlorophenol ug/LBRL10
2,4-Dimethylphenol ug/LBRL10
2,4-Dinitrophenol ug/LBRL10
2,4-Dinitrotoluene ug/LBRL10
2,6-Dinitrotoluene ug/LBRL10
2-Chloronaphthalene ug/LBRL10
2-Chlorophenol ug/LBRL10
2-Methylnaphthalene ug/LBRL10
2-Nitrophenol ug/LBRL10
3,3’-Dichlorobenzidine ug/LBRL10
3/4-Methylphenol ug/LBRL10
4,6-Dinitro-2-methylphenol ug/LBRL10
4-Bromophenyl phenyl ether ug/LBRL10
4-Chloro-3-methylphenol ug/LBRL10
4-Chloroaniline ug/LBRL10
4-Chlorophenyl phenyl ether ug/LBRL10
4-Nitrophenol ug/LBRL50
Acenaphthene ug/LBRL10
Acenaphthylene ug/LBRL10
Anthracene ug/LBRL10
Benzidine ug/LBRL100
Benzo(a)anthracene ug/LBRL10
Benzo(a)pyrene ug/LBRL10
Benzo(b)fluoranthene ug/LBRL10
Benzo(g,h,i)perylene ug/LBRL10
Benzo(k)fluoranthene ug/LBRL10
Benzoic Acid ug/LBRL100
Benzyl alcohol ug/LBRL10
bis(2-Chloroethoxy)methane ug/LBRL10
Bis(2-Chloroethyl)ether ug/LBRL10
Bis(2-chloroisopropyl)ether ug/LBRL10
Bis(2-Ethylhexyl)phthalate ug/LBRL10
Butyl benzyl phthalate ug/LBRL10
Chrysene ug/LBRL10
Dibenzo(a,h)anthracene ug/LBRL10
Dibenzofuran ug/LBRL10
Diethyl phthalate ug/LBRL10
Dimethyl phthalate ug/LBRL10
Di-n-butyl phthalate ug/LBRL10
Di-n-octyl phthalate ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 25
10/30/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz TruckingHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Prism Work Order: 7100385
Time Submitted: 10/19/2017 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0431 - 625
Blank (P7J0431-BLK1)Prepared & Analyzed: 10/24/17
Fluoranthene ug/LBRL10
Fluorene ug/LBRL10
Hexachlorobenzene ug/LBRL10
Hexachlorobutadiene ug/LBRL10
Hexachlorocyclopentadiene ug/LBRL10
Hexachloroethane ug/LBRL10
Indeno(1,2,3-cd)pyrene ug/LBRL10
Isophorone ug/LBRL10
Naphthalene ug/LBRL10
Nitrobenzene ug/LBRL10
N-Nitrosodimethylamine ug/LBRL10
N-Nitroso-di-n-propylamine ug/LBRL10
N-Nitrosodiphenylamine ug/LBRL10
Pentachlorophenol ug/LBRL10
Phenanthrene ug/LBRL10
Phenol ug/LBRL10
Pyrene ug/LBRL10
Tentatively Identified Compounds ug/LNot Detected
ug/L 100.0 31-144Surrogate: 2,4,6-Tribromophenol 7877.5
ug/L 50.00 49-118Surrogate: 2-Fluorobiphenyl 6532.5
ug/L 100.0 22-84Surrogate: 2-Fluorophenol 5251.8
ug/L 50.00 43-123Surrogate: Nitrobenzene-d5 6532.3
ug/L 100.0 10-63Surrogate: Phenol-d5 3433.9
ug/L 50.00 49-151Surrogate: Terphenyl-d14 8040.0
LCS (P7J0431-BS1)Prepared & Analyzed: 10/24/17
1,2,4-Trichlorobenzene ug/L53.9 10 100.0 44-14254
1,2-Dichlorobenzene ug/L54.6 10 100.0 32-12955
1,3-Dichlorobenzene ug/L51.6 10 100.0 20-12452
1,4-Dichlorobenzene ug/L51.7 10 100.0 20-12452
1-Methylnaphthalene ug/L65.0 10 100.0 40-13565
2,4,6-Trichlorophenol ug/L74.5 10 100.0 37-14474
2,4-Dichlorophenol ug/L66.2 10 100.0 39-13566
2,4-Dimethylphenol ug/L78.4 10 100.0 32-11978
2,4-Dinitrophenol ug/L74.0 10 100.0 10-19174
2,4-Dinitrotoluene ug/L80.8 10 100.0 39-13981
2,6-Dinitrotoluene ug/L80.1 10 100.0 50-15880
2-Chloronaphthalene ug/L66.4 10 100.0 60-11866
2-Chlorophenol ug/L65.6 10 100.0 23-13466
2-Methylnaphthalene ug/L61.9 10 100.0 18-12162
2-Nitrophenol ug/L66.3 10 100.0 29-18266
3,3’-Dichlorobenzidine ug/L90.8 10 100.0 10-26291
3/4-Methylphenol ug/L54.6 10 100.0 L76-10755
4,6-Dinitro-2-methylphenol ug/L86.5 10 100.0 10-18186
4-Bromophenyl phenyl ether ug/L78.0 10 100.0 53-12778
4-Chloro-3-methylphenol ug/L71.0 10 100.0 22-14771
4-Chloroaniline ug/L72.0 10 100.0 44-16372
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 25
10/30/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz TruckingHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Prism Work Order: 7100385
Time Submitted: 10/19/2017 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0431 - 625
LCS (P7J0431-BS1)Prepared & Analyzed: 10/24/17
4-Chlorophenyl phenyl ether ug/L74.8 10 100.0 25-15875
4-Nitrophenol ug/L34.8 50 100.0 10-13235
Acenaphthene ug/L73.3 10 100.0 47-14573
Acenaphthylene ug/L74.0 10 100.0 33-14574
Anthracene ug/L83.9 10 100.0 27-13384
Benzidine ug/L37.6 100 100.0 15-15038
Benzo(a)anthracene ug/L81.0 10 100.0 33-14381
Benzo(a)pyrene ug/L84.2 10 100.0 17-16384
Benzo(b)fluoranthene ug/L84.5 10 100.0 24-15985
Benzo(g,h,i)perylene ug/L84.4 10 100.0 10-21984
Benzo(k)fluoranthene ug/L81.8 10 100.0 11-16282
Benzoic Acid ug/L35.5 100 100.0 10-12536
Benzyl alcohol ug/L62.9 10 100.0 16-10763
bis(2-Chloroethoxy)methane ug/L69.0 10 100.0 33-18469
Bis(2-Chloroethyl)ether ug/L63.6 10 100.0 12-15864
Bis(2-chloroisopropyl)ether ug/L65.0 10 100.0 36-16665
Bis(2-Ethylhexyl)phthalate ug/L81.5 10 100.0 10-15881
Butyl benzyl phthalate ug/L60.7 10 100.0 10-15261
Chrysene ug/L81.6 10 100.0 17-16882
Dibenzo(a,h)anthracene ug/L59.9 10 100.0 10-22760
Dibenzofuran ug/L71.0 10 100.0 39-11471
Diethyl phthalate ug/L54.5 10 100.0 10-11454
Dimethyl phthalate ug/L25.1 10 100.0 10-11225
Di-n-butyl phthalate ug/L72.6 10 100.0 10-11873
Di-n-octyl phthalate ug/L83.2 10 100.0 10-14683
Fluoranthene ug/L83.6 10 100.0 26-13784
Fluorene ug/L77.4 10 100.0 59-12177
Hexachlorobenzene ug/L80.6 10 100.0 10-15281
Hexachlorobutadiene ug/L50.9 10 100.0 24-11651
Hexachlorocyclopentadiene ug/L47.6 10 100.0 32-11748
Hexachloroethane ug/L48.6 10 100.0 40-11349
Indeno(1,2,3-cd)pyrene ug/L96.8 10 100.0 10-17197
Isophorone ug/L68.2 10 100.0 21-19668
Naphthalene ug/L63.2 10 100.0 21-13363
Nitrobenzene ug/L60.8 10 100.0 35-18061
N-Nitrosodimethylamine ug/L45.7 10 100.0 10-11946
N-Nitroso-di-n-propylamine ug/L69.8 10 100.0 10-23070
N-Nitrosodiphenylamine ug/L99.2 10 100.0 69-15299
Pentachlorophenol ug/L87.5 10 100.0 14-17687
Phenanthrene ug/L84.3 10 100.0 54-12084
Phenol ug/L36.3 10 100.0 10-11236
Pyrene ug/L79.6 10 100.0 52-11580
ug/L 100.0 31-144Surrogate: 2,4,6-Tribromophenol 8282.4
ug/L 50.00 49-118Surrogate: 2-Fluorobiphenyl 7035.2
ug/L 100.0 22-84Surrogate: 2-Fluorophenol 4949.0
ug/L 50.00 43-123Surrogate: Nitrobenzene-d5 6733.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 25
10/30/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz TruckingHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Prism Work Order: 7100385
Time Submitted: 10/19/2017 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0431 - 625
LCS (P7J0431-BS1)Prepared & Analyzed: 10/24/17
ug/L 100.0 10-63Surrogate: Phenol-d5 3232.0
ug/L 50.00 49-151Surrogate: Terphenyl-d14 7839.0
LCS Dup (P7J0431-BSD1)Prepared & Analyzed: 10/24/17
1,2,4-Trichlorobenzene ug/L56.2 10 100.0 2044-14256 4
1,2-Dichlorobenzene ug/L58.0 10 100.0 2032-12958 6
1,3-Dichlorobenzene ug/L56.4 10 100.0 2020-12456 9
1,4-Dichlorobenzene ug/L56.6 10 100.0 2020-12457 9
1-Methylnaphthalene ug/L65.8 10 100.0 2040-13566 1
2,4,6-Trichlorophenol ug/L72.8 10 100.0 2037-14473 2
2,4-Dichlorophenol ug/L67.4 10 100.0 2039-13567 2
2,4-Dimethylphenol ug/L78.1 10 100.0 2032-11978 0.4
2,4-Dinitrophenol ug/L67.5 10 100.0 2010-19167 9
2,4-Dinitrotoluene ug/L74.7 10 100.0 2039-13975 8
2,6-Dinitrotoluene ug/L74.6 10 100.0 2050-15875 7
2-Chloronaphthalene ug/L67.3 10 100.0 2060-11867 1
2-Chlorophenol ug/L67.6 10 100.0 2023-13468 3
2-Methylnaphthalene ug/L60.8 10 100.0 2018-12161 2
2-Nitrophenol ug/L66.5 10 100.0 2029-18267 0.4
3,3’-Dichlorobenzidine ug/L81.7 10 100.0 2010-26282 11
3/4-Methylphenol ug/L53.7 10 100.0 20 L76-10754 2
4,6-Dinitro-2-methylphenol ug/L76.2 10 100.0 2010-18176 13
4-Bromophenyl phenyl ether ug/L71.1 10 100.0 2053-12771 9
4-Chloro-3-methylphenol ug/L68.1 10 100.0 2022-14768 4
4-Chloroaniline ug/L67.9 10 100.0 2044-16368 6
4-Chlorophenyl phenyl ether ug/L71.4 10 100.0 2025-15871 5
4-Nitrophenol ug/L31.2 50 100.0 2010-13231 11
Acenaphthene ug/L69.8 10 100.0 2047-14570 5
Acenaphthylene ug/L72.2 10 100.0 2033-14572 2
Anthracene ug/L76.5 10 100.0 2027-13377 9
Benzidine ug/L29.1 100 100.0 20 D15-15029 25
Benzo(a)anthracene ug/L74.5 10 100.0 2033-14374 8
Benzo(a)pyrene ug/L76.7 10 100.0 2017-16377 9
Benzo(b)fluoranthene ug/L76.3 10 100.0 2024-15976 10
Benzo(g,h,i)perylene ug/L76.6 10 100.0 2010-21977 10
Benzo(k)fluoranthene ug/L76.4 10 100.0 2011-16276 7
Benzoic Acid ug/L27.6 100 100.0 20 D10-12528 25
Benzyl alcohol ug/L62.6 10 100.0 2016-10763 0.4
bis(2-Chloroethoxy)methane ug/L67.1 10 100.0 2033-18467 3
Bis(2-Chloroethyl)ether ug/L61.2 10 100.0 2012-15861 4
Bis(2-chloroisopropyl)ether ug/L66.0 10 100.0 2036-16666 1
Bis(2-Ethylhexyl)phthalate ug/L73.1 10 100.0 2010-15873 11
Butyl benzyl phthalate ug/L55.0 10 100.0 2010-15255 10
Chrysene ug/L74.6 10 100.0 2017-16875 9
Dibenzo(a,h)anthracene ug/L54.2 10 100.0 2010-22754 10
Dibenzofuran ug/L69.6 10 100.0 2039-11470 2
Diethyl phthalate ug/L47.2 10 100.0 2010-11447 14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 25
10/30/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: ROS-001 Former Dietz TruckingHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Prism Work Order: 7100385
Time Submitted: 10/19/2017 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0431 - 625
LCS Dup (P7J0431-BSD1)Prepared & Analyzed: 10/24/17
Dimethyl phthalate ug/L20.4 10 100.0 20 D10-11220 21
Di-n-butyl phthalate ug/L64.9 10 100.0 2010-11865 11
Di-n-octyl phthalate ug/L75.2 10 100.0 2010-14675 10
Fluoranthene ug/L75.7 10 100.0 2026-13776 10
Fluorene ug/L73.2 10 100.0 2059-12173 6
Hexachlorobenzene ug/L72.9 10 100.0 2010-15273 10
Hexachlorobutadiene ug/L54.6 10 100.0 2024-11655 7
Hexachlorocyclopentadiene ug/L50.9 10 100.0 2032-11751 7
Hexachloroethane ug/L53.5 10 100.0 2040-11353 10
Indeno(1,2,3-cd)pyrene ug/L88.5 10 100.0 2010-17189 9
Isophorone ug/L65.4 10 100.0 2021-19665 4
Naphthalene ug/L64.0 10 100.0 2021-13364 1
Nitrobenzene ug/L59.9 10 100.0 2035-18060 1
N-Nitrosodimethylamine ug/L46.2 10 100.0 2010-11946 1
N-Nitroso-di-n-propylamine ug/L66.8 10 100.0 2010-23067 5
N-Nitrosodiphenylamine ug/L90.2 10 100.0 2069-15290 10
Pentachlorophenol ug/L78.4 10 100.0 2014-17678 11
Phenanthrene ug/L76.5 10 100.0 2054-12077 10
Phenol ug/L36.4 10 100.0 2010-11236 0.03
Pyrene ug/L74.1 10 100.0 2052-11574 7
ug/L 100.0 31-144Surrogate: 2,4,6-Tribromophenol 7676.4
ug/L 50.00 49-118Surrogate: 2-Fluorobiphenyl 7135.4
ug/L 100.0 22-84Surrogate: 2-Fluorophenol 5151.4
ug/L 50.00 43-123Surrogate: Nitrobenzene-d5 6633.1
ug/L 100.0 10-63Surrogate: Phenol-d5 3333.1
ug/L 50.00 49-151Surrogate: Terphenyl-d14 7135.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 25
Sample Extraction Data
Prep Method: 625
Lab Number Batch Date/TimeInitialFinal
P7J04317100385-01 10/24/17 13:159201mL mL
P7J04317100385-02 10/24/17 13:159001mL mL
P7J04317100385-03 10/24/17 13:159201mL mL
P7J04317100385-04 10/24/17 13:159101mL mL
Prep Method: SM6200 B
Lab Number Batch Date/TimeInitialFinal
P7J03877100385-01 10/21/17 14:4810 10mL mL
P7J03877100385-02 10/21/17 14:4810 10mL mL
P7J03877100385-03 10/21/17 14:4810 10mL mL
P7J03877100385-04 10/21/17 14:4810 10mL mL
P7J03877100385-05 10/21/17 14:4810 10mL mL
P7J03877100385-06 10/21/17 14:4810 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 25
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