AS-3731_28861_CA_TCR_20230915_IAR

INITIAL ACTIONS & ABATEMENT WITH
UST CLOSURE REPORT

For The
ONE STOP #15
146 Wiggins Road Candler, Buncombe County
North Carolina Facility # 00-0-0000021101
September 15, 2023

Singleton Environmental, Inc. Project # SEI-1361

Singleton Environmental, Inc.

INITIAL ACTIONS & ABATEMENT REPORT WITH UST CLOSURE
September 15, 2023 Incident Number: 28861 Site Name: One Stop #15 146 Wiggins Road Candler, NC 28715
Incident Number: 28861 Facility ID Number: 00-0-0000021101 UST Responsible Party: Samir Enterprises, LLC. PO Box 1272
Old Fort, NC 28762 Consultant / Contractor: Singleton Environmental, Inc. PO Box 604
Fletcher, NC 28732
Telephone: [phone] Date Release Discovered: June 6, 2012
Estimated Quantity of Release: Unknown/unquantified Cause/Source of Release: USTs and Dispenser Islands
Latitude: 35.5432° North
Longitude: -82.7530° West Signature and Seal of Certifying Professional Geologist:
I, Christopher D. Singleton, a North Carolina Professional Geologist, do certify that the information contained in this report is correct and accurate to the best of my knowledge. ____________________________________
Christopher D. Singleton, P.G. #1928
Singleton Environmental, Inc. is licensed to practice geology in North Carolina. The certification number of the company is C-443.

Table of Contents
Introduction ................................................................................................................................1
Site History…......................…………......................................... .................................................1 Brief Description of the Site…………......................................... .................................................1 Closure Procedures..............…………............................................................................................2 Source Investigation…......................…………......................................... ....................................2
Initial Abatement Activities…......................…………......................................... .........................3
Conclusions and Recommendations…..................…………......................................... ................3 Table Table 1. Soil Analytical Results – Closure Samples
Table 2. Soil Analytical Results – Risk Based Analysis Figures
Figure 1. Site Vicinity Map 7.5’ USGS Topo
Figure 2. Site Map – GRO/DRO Closure Sample Locations Figure 3. Soil Excavation Areas – Risk Based Sample Locations Figure 4. Soil Exceeding MSCCs
Appendices Appendix A: UST-2 and UST-3 Forms Appendix B: UST Disposal Manifest Appendix C: Soil Disposal Manifests
Appendix D: Laboratory Analytical Results

Introduction
This report summarizes the UST system closure and initial actions & abatement activities for the removal of four underground storage tanks (UST) at One Stop #15 located at 146
Wiggins Road in Candler, Buncombe County, North Carolina. The property is owned and operated by Samir Enterprises, LLC. Figure 1 shows the site location on a USGS topography map, and Figure 2 presents site maps showing the location of the former USTs and corresponding soil sampling locations.

Site History

The following tables summarize information about the USTs at the site:
Tank No. Volume Contents
Tank Material Use Date last used
UST removed or closed in place
Date of permanent closure
Was a release detected? When?
1 10000 Gasoline Steel Resale 6/9/23 Removed 6/9/23 Yes
2 10000 Gasoline Steel Resale 6/9/23 Removed 6/9/23 Yes
3 10000 Diesel Steel Resale 6/9/23 Removed 6/9/23 Yes
4 4000 Kerosene Steel Resale 6/9/23 Removed 6/9/23 Yes
Ownership of Tanks: Samir Enterprises, LLC.
PO Box 1272
Old Fort, NC 28762 Telephone: [phone] Brief Description of the Site

Land use at the site is commercial, and the surrounding properties are commercial and residential properties. The closest surface water body is Georges Branch located approximately 130 feet to the west of the site. Groundwater was not encountered
underneath the USTs during the soil removal activities. Bedrock was not encountered during the UST removal or soil excavation activities. Closure Procedures
On June 9, 2023, through August 2, 2023, the tank removal and initial actions and
abatement activities commenced. The USTs were located on the southern side of the
property as shown in Figure 2. Prior to the UST removal, the contents of the tanks were completely emptied by Samir Enterprises, LLC. Prior to removal, the vapors were purged from the tanks using a large quantity of dry ice. An excavator was used to remove the USTs from each respective tank cavity. The UST disposal manifest is included with
Appendix B. During the closure and excavation activities, monitoring well MW-1, PZ-1,

and PZ-4 were closed with bentonite and cement then removed during the excavation
activities. During the UST removal, soil samples were collected at the fill ports and underneath each tank. Samples were also collected underneath the product lines and dispensers at
the site. All the samples were analyzed for Gasoline Range Organics (GRO) and Diesel
Range Organics (DRO) when applicable.
Soil analytical results are summarized in Table 1 and corresponding soil sampling locations can be found in Figure 2. A high amount of petroleum odors was detected with a PID in the soils surrounding the gas and diesel USTs on the western side of the UST
tank hold, and the dispensers. Source Investigation
Twenty soil samples (see Figure 2) were collected underneath the former USTs, dispensers, and product lines on June 9, 2023. Samples FP-1 through FP-4 were collected underneath each spill bucket at a depth of approximately 2 ft/bls. Samples T-1 through T-12 were collected underneath the USTs at depths between 10 ft/bls and 14 ft/bls.
Samples D-1 through D-4 were collected underneath each dispenser at a depth of approximately 2 ft/bls. Samples L-1 through L-5 were collected underneath the product lines at a depth of approximately 3 ft/bls. Four of the soil samples (FP-2, D-1, D-2, and T-4) detected a concentration of DRO above the MSCC of 100 mg/kg and eight of the
soil samples (FP-2, FP-3, FP-4, D-1, C-2, D-3, D-4, and T-7) detected a concentration
above the MSCC of 50 mg/kg. Soil analytical results are summarized in Table 1 and the locations of the samples are shown on Figure 2. Initial Abatement Activities Once the USTs were removed, contaminated soils were excavated in six areas between June 9, 2023, and August 2, 2023. The three areas include, the USTs, each dispenser
island, and the area around monitoring well MW-1 where free-product was observed and
recovered over the last few years. The UST excavation measured approximately 35’L x 17’W x 14’D. Four small excavations were completed at each dispenser island. Each excavation measured approximately 8’L x 6’W x 5’D. These excavations were small because they were located right beside each canopy foundation footer; therefore, larger excavations would impact the structural integrity of the canopy. The last excavation
around MW-1 measured approximately 20’L x 14’W x 22’D. During the entire soil excavation activities approximately 795.52 tons of petroleum impacted soil were removed and transported to Environmental Soils, Inc. in Lattimore, NC. Soil disposal manifests are included in Appendix C.

At the completion of each soil excavation, post-excavation soil samples were collected from the sidewalls and basement of each cavity at a depth of approximately 5 ft/bls at the dispenser islands to 10 to 14 ft/bls at the UST pit, and 22 ft/bls in the area surrounding MW-1. Soil risk-based samples Soil-A through Soil-J and Soil-D-1 through Soil-D-4

(dispenser islands) were analyzed using EPA Methods 8260, 8270, and MADEP EPH/VPH with the exception of Soil-D-1, Soil-D-2, and Soil-E where EPA Method 8260 and MADEP VPH were analyzed only. The following risk-based samples detected concentrations exceeding the maximum soil contaminant concentrations (MSCCs):
• Dispenser samples Soil-D-1, Soil-D-2, Soil-D-3, and Soil-D-4 did not detect any compounds exceeding the Soil-to-Groundwater MSCCs.
• Soil samples Soil-A, Soil-B, Soil-C, Soil-D, and Soil-E detected concentrations of benzene exceeding the Soil-to-Groundwater MSCCs; however, the concentrations
of benzene did not exceed the Residential MSCC.
• Soil sample Soil-F detected concentrations of 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, benzene, ethylbenzene, methylene chloride, naphthalene, toluene, xylene, n-propylbenzene, 1-methylnaphthalene, 2-methylnaphthalene,
C5-C8 aliphatics, and C9-C10 aromatics exceeding the Soil-to-Groundwater MSCCs. The concentration of C9-C10 aromatics exceeded the Residential MSCCs. None of the detected compounds exceeded the Industrial/Commercial MSCCs.
• Soil sample Soil-G detected concentrations of benzene and naphthalene exceeding
the Soil-to-Groundwater MSCCs. None of the detected compounds exceeded the Residential MSCCs.
• Soil sample Soil-H detected a concentration of naphthalene exceeding the Soil-to-Groundwater MSCC; however, it did not exceed the Residential MSCC.
• Soil samples Soil-I and Soil-J did not detect any compounds exceeding the Soil-to-Groundwater MSCCs. Refer to Table 2 for a summary of each constituent and the detected contamination level.
Figures 3 and 4 presents the corresponding sampling locations and impacted areas,
respectively. A copy of the laboratory analytical report is included in Appendix D. On August 15, 2023, monitoring well MW-1R was installed at the site to replace MW-1. Monitoring well MW-1R was installed to a depth of 27.5 feet. To date, no free-product
has been observed in MW-1R. The well completion log and groundwater analysis will be included in the Groundwater Monitoring Report following this report. Conclusions and Recommendations
From June 9, 2023, to August 2, 2023, the subject USTs were removed and contaminated
soils were removed from the site in six on-site locations. Approximately 795.52 tons of
contaminated soil were excavated and disposed of at Environmental Soils, Inc. in Lattimore, North Carolina. The results of this investigation indicate the soil located at the site contains concentrations exceeding the Soil-to-Groundwater and Residential MSCCs. The groundwater at the site also contains compounds exceeding the NCAC 2L MCLs;
however, since the soil excavation activities, free-product has not returned to MW-1R. SEI will submit a Groundwater Monitoring Report following this report that will contain recommendations for moving forward at the site.

TABLE
EPA 8015C by EPA 8015C by Diesel Range Organics(C10-C28)Gas Range Organics (C6-C10)DateCollected(mm/dd/yy)SampleDepth(ft. BGS)mg/kg mg/kgFP-1 06/09/20232ND NDFP-2 06/09/202322330 64.6FP-3 06/09/20232N/A 1660FP-4 6/9/20232N/A 361L-1 6/16/202339.4NDL-2 6/16/20233ND NDL-3 6/16/20233ND NDL-4 6/16/20233ND NDL-5 6/16/20233ND NDD-1 6/9/2023223600 6830D-2 6/9/2023210800 1170D-3 6/9/20232N/A 34.3D-4 6/9/20232N/A 2620T-1 06/09/202310ND 11.3T-2 06/09/2023106.8 NDT-3 06/09/2023106.0 NDT-4 06/09/202312423 43.6T-5 06/09/202312ND NDT-6 06/09/202312ND NDT-7 6/9/202312N/A 316T-8 06/09/202312N/A NDT-9 06/09/202312N/A NDT-10 06/09/202312N/A NDT-11 06/09/202312N/A NDT-12 06/09/202312N/A ND100 50MSCC = Maximum Soil Contamination Concentrationft. BGS = feet below ground surfacemg/kg = milligrams per kilogramug/kg = micrograms per kilogramBold data above the 2L Class GA StandardNOTES:ND = Not DetectedAnalytical MethodSample IDConstituent of ConcernNCDEQ MSCCTable # 1Summary of Analytical Results - Solid SamplesONE STOP 15
1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneBenzeneEthylbenzeneIsopropylbenzene (Cumene)Methylene ChlorideNaphthaleneStyrene TolueneXylene (Total)p-Isopropyltoluenen-Propylbenzene1-Methylnaphthalene2-MethylnaphthaleneNaphthaleneC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 AromaticsAliphatic (C09-C18)Aliphatic (C19-C36)Aromatic (C11-C22)DateCollected(mm/dd/yy)SampleDepth(ft. BGS)mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgSOIL-A6/13/202314ND ND 0.0132ND ND ND ND ND ND ND ND ND ND ND NDND ND ND ND ND NDSOIL-B 6/13/2023140.163 0.0573 0.0113 ND ND ND 0.0538ND ND0.0351 0.0265ND ND ND NDND ND ND ND ND NDSOIL-C 6/13/2023140.0204 ND 0.0125ND ND ND ND ND ND ND ND ND ND ND NDND ND ND 20.9 ND NDSOIL-D 6/13/2023140.254 ND 0.0172 0.0138ND ND ND ND ND ND0.0801ND ND ND NDND ND ND 152 57.9 54.7Soil-D-1 6/13/20235ND ND ND ND ND ND ND ND ND ND ND ND ND ND NDND ND ND ND ND NDSoil-D-2 6/13/20235ND ND ND ND ND ND ND ND ND ND ND ND ND ND NDND ND ND ND ND NDSoil-D-3 6/13/202350.0109ND ND ND ND ND0.0072 0.0084ND ND ND NDN/A N/A N/A ND ND ND N/A N/A N/ASoil-D-4 6/13/202350.0145ND ND ND ND ND ND ND ND ND ND NDN/A N/A N/A ND ND ND N/A N/A N/ASOIL-E 6/13/2023140.034 ND 0.014ND ND ND0.0196ND ND ND ND ND ND ND NDND ND ND N/A N/A N/ASOIL-F 08/01/20232226.0 8.4 0.29 8.00.760.19 6.60.689.9 43.9ND3.4 0.912.23.2250 130 47037.6 ND 27.2SOIL-G 08/01/2023223.4 1.10.0120.21 ND ND2.90.023 0.19 1.6 ND ND ND ND ND23 21 18ND ND NDSOIL-H 08/01/2023221.1 0.34 ND 0.10 ND ND1.10.018 0.10 0.74 ND ND ND 0.500.5714 6.7 23ND ND 17.9SOIL-I 08/01/2023220.037 0.011 ND ND ND ND 0.019 ND ND 0.032 ND ND ND ND ND12 3.2 1.4ND ND NDSOIL-J 08/01/202322ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND14 2.9 1.9ND ND ND8.5 8.3 0.0056 4.9 1.7 0.02 0.16 1.5 4.36 0.121.7 0.004 3.6 0.1668 540 31540 N/A N/A782 782 18 1560 1560 85 313 3130 12003120 1560626 20 63 313625 1560 4691500 31000 N/A20400 20400 164 40000 40900 763 8180 81800 3200046700 2330016400 100 1640 81809340 23300 700040000 810000 N/Aug/kg = micrograms per kilogramBold data above the 2L Class GA StandardEPA Method 8270 MADEP VPHVPH = Volatile Petroleum Hydrocarbon - Massachusetts Department of Environmental ProtectionEPH = Extractable Petroleum Hydrocarbon - Massachusetts Department of Environmental ProtectionMSCC = Maximum Soil Contamination Concentrationft. BGS = feet below ground surfacemg/kg = milligrams per kilogramSoil to Groundwater MSCCResidential MSCCIndustrial/Commercial MSCCNOTES:ND = Not DetectedAnalytical MethodEPA Method 8260MADEP EPHSample IDConstituent of ConcernTable # 2Summary of Analytical Results - Solid SamplesONE STOP 15

FIGURES
CANTON QUADRANGLE
NORTH CAROLINA
7.5 MINUTE SERIES (TOPOGRAPHIC)
Figure 1 Site Map
One Stop #15 – Candler, NC
One Stop #15
Singleton Environmental, Inc MW-1MW-3MW-2Current USTsMW-4One Stop #15WSW-1MW-5MW-6MW-7MW-8MW-9L-1D-1D-3D-2D-4L-2L-5L-3L-4T-3FP-1T-2T-1T-4T-5T-6T-7T-8T-9T-10T-11T-12FP-4FP-2FP-3
Singleton Environmental, Inc Excavation AreasOne Stop #15WSW-1Soil-ASoil-CSoil-DSoil-ESoil-BSoil-HSoil-ISoil-JSoil-GSoil-FSoil-D-1Soil-D-2Soil-D-4Soil-D-3
Singleton Environmental, Inc Excavation AreasOne Stop #15WSW-1Soil-ASoil-CSoil-DSoil-ESoil-BSoil-HSoil-ISoil-JSoil-GSoil-FSoil-D-1Soil-D-2Soil-D-4Soil-D-3Soils Exceeding Soil-to-GW MSCCsSoils Exceeding Residential MSCCs

APPENDIX A

APPENDIX B

APPENDIX C

APPENDIX D

#=CL#
June 14, 2023
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92671719
92671719
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
105 Charlotte Highway
Asheville, NC 28803
ONE STOP 15
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on June 09, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 17
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92671719
ONE STOP 15
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92671719
ONE STOP 15
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92671719001 D-1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671719002 D-2 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671719003 D-3 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671719004 D-4 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671719005 FP-4 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671719006 T-7 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671719
ONE STOP 15
Sample:D-1 Lab ID:92671719001 Collected:06/09/23 11:40 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)23600 mg/kg 06/13/23 11:2106/10/23 12:05642125
Surrogates
n-Pentacosane (S)0 %06/13/23 11:21 629-99-2 S406/10/23 12:0510-133 125
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)6830 mg/kg 06/14/23 00:4806/12/23 14:1516320
Surrogates
4-Bromofluorobenzene (S)105 %06/14/23 00:48 460-00-406/12/23 14:1566-130 20
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 4.0 %06/12/23 12:49 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/14/2023 11:03 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671719
ONE STOP 15
Sample:D-2 Lab ID:92671719002 Collected:06/09/23 11:50 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)10800 mg/kg 06/13/23 11:2106/10/23 12:0526650
Surrogates
n-Pentacosane (S)0 %06/13/23 11:21 629-99-2 S406/10/23 12:0510-133 50
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1170 mg/kg 06/13/23 23:5206/12/23 14:1532.6 4
Surrogates
4-Bromofluorobenzene (S)105 %06/13/23 23:52 460-00-406/12/23 14:1566-130 4
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 5.4 %06/12/23 12:50 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/14/2023 11:03 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671719
ONE STOP 15
Sample:D-3 Lab ID:92671719003 Collected:06/09/23 11:55 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)34.3 mg/kg 06/13/23 21:0306/12/23 14:158.8 1
Surrogates
4-Bromofluorobenzene (S)77 %06/13/23 21:03 460-00-406/12/23 14:1566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 2.4 %06/12/23 12:50 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/14/2023 11:03 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671719
ONE STOP 15
Sample:D-4 Lab ID:92671719004 Collected:06/09/23 12:00 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)2620 mg/kg 06/14/23 00:20 D306/12/23 14:1585.8 10
Surrogates
4-Bromofluorobenzene (S)117 %06/14/23 00:20 460-00-406/12/23 14:1566-130 10
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 2.9 %06/12/23 12:50 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/14/2023 11:03 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671719
ONE STOP 15
Sample:FP-4 Lab ID:92671719005 Collected:06/09/23 13:10 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)361 mg/kg 06/13/23 21:3106/12/23 14:1513.4 1
Surrogates
4-Bromofluorobenzene (S)139 %06/13/23 21:31 460-00-4 S206/12/23 14:1566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.0 %06/12/23 12:50 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/14/2023 11:03 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671719
ONE STOP 15
Sample:T-7 Lab ID:92671719006 Collected:06/09/23 10:40 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)316 mg/kg 06/13/23 21:5906/12/23 14:157.6 1
Surrogates
4-Bromofluorobenzene (S)222 %06/13/23 21:59 460-00-4 S206/12/23 14:1566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.6 %06/12/23 12:50 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/14/2023 11:03 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92671719
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
780002
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92671719001, 92671719002, 92671719003, 92671719004, 92671719005, 92671719006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4046090
Associated Lab Samples:92671719001, 92671719002, 92671719003, 92671719004, 92671719005, 92671719006
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 06/13/23 13:06
4-Bromofluorobenzene (S)%93 66-130 06/13/23 13:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4046091LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 41.049.7 82 70-130
4-Bromofluorobenzene (S)%92 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4046093MATRIX SPIKE SAMPLE:
MSSpike
Result
92671590001
Gas Range Organics (C6-C10)mg/kg 74.890.4 82 57-154ND
4-Bromofluorobenzene (S)%97 66-130
Parameter Units
Dup
Result QualifiersRPDResult
92670552006
4046092SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%9694
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/14/2023 11:03 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
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Page 10 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92671719
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
779781
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92671719001, 92671719002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4045350
Associated Lab Samples:92671719001, 92671719002
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 4.9 06/12/23 13:40
n-Pentacosane (S)%68 10-133 06/12/23 13:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4045351LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 52.966.9 79 43-130
n-Pentacosane (S)%62 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4045352MATRIX SPIKE SAMPLE:
MSSpike
Result
92671736006
Diesel Range Organics(C10-C28)mg/kg 62.679.2 72 15-130ND
n-Pentacosane (S)%69 10-133
Parameter Units
Dup
Result QualifiersRPDResult
92671736013
4045353SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg NDND
n-Pentacosane (S)%6669
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/14/2023 11:03 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92671719
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
779974
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92671719001, 92671719002, 92671719003, 92671719004, 92671719005, 92671719006
Parameter Units
Dup
Result QualifiersRPDResult
92671736028
4045985SAMPLE DUPLICATE:
Percent Moisture %24.7 N2325.6
Parameter Units
Dup
Result QualifiersRPDResult
92670552006
4045988SAMPLE DUPLICATE:
Percent Moisture %15.4 N2814.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/14/2023 11:03 AM
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Asheville, NC 28804
[phone]
Page 12 of 17
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92671719
ONE STOP 15
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/14/2023 11:03 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 17
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92671719
ONE STOP 15
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92671719001 779781 779894D-1 EPA 3546 EPA 8015C
92671719002 779781 779894D-2 EPA 3546 EPA 8015C
92671719001 780002 780040D-1 EPA 5030B EPA 8015C
92671719002 780002 780040D-2 EPA 5030B EPA 8015C
92671719003 780002 780040D-3 EPA 5030B EPA 8015C
92671719004 780002 780040D-4 EPA 5030B EPA 8015C
92671719005 780002 780040FP-4 EPA 5030B EPA 8015C
92671719006 780002 780040T-7 EPA 5030B EPA 8015C
92671719001 779974D-1 SW-846
92671719002 779974D-2 SW-846
92671719003 779974D-3 SW-846
92671719004 779974D-4 SW-846
92671719005 779974FP-4 SW-846
92671719006 779974T-7 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/14/2023 11:03 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 17
Page 15 of 17
Page 16 of 17
Page 17 of 17
#=CL#
June 20, 2023
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92671732
92671732
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
105 Charlotte Highway
Asheville, NC 28803
ONE STOP 15
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on June 09, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92671732
ONE STOP 15
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92671732
ONE STOP 15
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92671732001 FP-1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732002 FP-2 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732003 FP-3 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732004 T-1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732005 T-2 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732006 T-3 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732007 T-4 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732008 T-5 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732009 T-6 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732010 T-8 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732011 T-9 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732012 T-10 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732013 T-11 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92671732014 T-12 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92671732
ONE STOP 15
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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2225 Riverside Dr.
Asheville, NC 28804
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:FP-1 Lab ID:92671732001 Collected:06/09/23 07:00 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/12/23 21:3406/10/23 15:005.1 1
Surrogates
n-Pentacosane (S)65 %06/12/23 21:34 629-99-206/10/23 15:0010-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/14/23 19:4906/14/23 12:068.9 1
Surrogates
4-Bromofluorobenzene (S)92 %06/14/23 19:49 460-00-406/14/23 12:0666-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 4.2 %06/12/23 13:59 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:FP-2 Lab ID:92671732002 Collected:06/09/23 08:15 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)2330 mg/kg 06/13/23 13:5106/10/23 15:0061.1 10
Surrogates
n-Pentacosane (S)0 %06/13/23 13:51 629-99-2 S406/10/23 15:0010-133 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)64.6 mg/kg 06/14/23 20:1706/14/23 12:069.2 1
Surrogates
4-Bromofluorobenzene (S)187 %06/14/23 20:17 460-00-4 S506/14/23 12:0666-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.4 %06/12/23 14:00 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:FP-3 Lab ID:92671732003 Collected:06/09/23 10:30 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1660 mg/kg 06/16/23 06:4806/15/23 11:4130.5 2
Surrogates
4-Bromofluorobenzene (S)389 %06/16/23 06:48 460-00-4 S206/15/23 11:4166-130 2
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.0 %06/12/23 14:00 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:T-1 Lab ID:92671732004 Collected:06/09/23 07:40 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/12/23 21:5506/10/23 15:007.0 1
Surrogates
n-Pentacosane (S)54 %06/12/23 21:55 629-99-206/10/23 15:0010-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)11.3 mg/kg 06/16/23 06:1906/15/23 11:4110.5 1
Surrogates
4-Bromofluorobenzene (S)100 %06/16/23 06:19 460-00-406/15/23 11:4166-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.4 %06/12/23 14:00 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:T-2 Lab ID:92671732005 Collected:06/09/23 07:45 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)6.8 mg/kg 06/13/23 14:1206/10/23 15:005.6 1
Surrogates
n-Pentacosane (S)67 %06/13/23 14:12 629-99-206/10/23 15:0010-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/15/23 17:1406/15/23 11:3516.3 1
Surrogates
4-Bromofluorobenzene (S)91 %06/15/23 17:14 460-00-406/15/23 11:3566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.7 %06/12/23 14:00 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:T-3 Lab ID:92671732006 Collected:06/09/23 07:50 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)6.0 mg/kg 06/12/23 22:1706/10/23 15:005.5 1
Surrogates
n-Pentacosane (S)75 %06/12/23 22:17 629-99-206/10/23 15:0010-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/15/23 17:4206/15/23 11:359.6 1
Surrogates
4-Bromofluorobenzene (S)96 %06/15/23 17:42 460-00-406/15/23 11:3566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 6.8 %06/12/23 14:00 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:T-4 Lab ID:92671732007 Collected:06/09/23 08:50 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)423 mg/kg 06/13/23 14:1206/10/23 15:0012.6 2
Surrogates
n-Pentacosane (S)76 %06/13/23 14:12 629-99-206/10/23 15:0010-133 2
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)43.6 mg/kg 06/14/23 22:3706/14/23 12:0611.2 1
Surrogates
4-Bromofluorobenzene (S)125 %06/14/23 22:37 460-00-406/14/23 12:0666-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.1 %06/12/23 14:00 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:T-5 Lab ID:92671732008 Collected:06/09/23 10:15 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/12/23 19:2406/12/23 10:326.2 1
Surrogates
n-Pentacosane (S)73 %06/12/23 19:24 629-99-206/12/23 10:3210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/15/23 18:1006/15/23 11:3511.8 1
Surrogates
4-Bromofluorobenzene (S)96 %06/15/23 18:10 460-00-406/15/23 11:3566-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.8 %06/12/23 14:00 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:T-6 Lab ID:92671732009 Collected:06/09/23 10:20 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/12/23 19:4606/12/23 10:325.2 1
Surrogates
n-Pentacosane (S)85 %06/12/23 19:46 629-99-206/12/23 10:3210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/14/23 23:3306/14/23 12:067.2 1
Surrogates
4-Bromofluorobenzene (S)99 %06/14/23 23:33 460-00-406/14/23 12:0666-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 3.4 %06/12/23 14:00 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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Page 13 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:T-8 Lab ID:92671732010 Collected:06/09/23 12:10 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/15/23 00:0206/14/23 12:067.8 1
Surrogates
4-Bromofluorobenzene (S)95 %06/15/23 00:02 460-00-406/14/23 12:0666-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.2 %06/12/23 14:00 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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Page 14 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:T-9 Lab ID:92671732011 Collected:06/09/23 12:20 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/15/23 00:3006/14/23 12:0611.2 1
Surrogates
4-Bromofluorobenzene (S)94 %06/15/23 00:30 460-00-406/14/23 12:0666-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.8 %06/12/23 14:00 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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Page 15 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:T-10 Lab ID:92671732012 Collected:06/09/23 13:23 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/15/23 00:5806/14/23 12:068.4 1
Surrogates
4-Bromofluorobenzene (S)97 %06/15/23 00:58 460-00-406/14/23 12:0666-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.4 %06/12/23 14:01 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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Page 16 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:T-11 Lab ID:92671732013 Collected:06/09/23 13:40 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/15/23 01:2606/14/23 12:06101
Surrogates
4-Bromofluorobenzene (S)96 %06/15/23 01:26 460-00-406/14/23 12:0666-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.7 %06/12/23 14:01 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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Page 17 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92671732
ONE STOP 15
Sample:T-12 Lab ID:92671732014 Collected:06/09/23 13:50 Received:06/09/23 14:21 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/15/23 01:5406/14/23 12:0611.2 1
Surrogates
4-Bromofluorobenzene (S)95 %06/15/23 01:54 460-00-406/14/23 12:0666-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.3 %06/12/23 14:01 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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Page 18 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92671732
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
780506
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92671732001, 92671732002, 92671732007, 92671732009, 92671732010, 92671732011, 92671732012,
92671732013, 92671732014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4048848
Associated Lab Samples:92671732001, 92671732002, 92671732007, 92671732009, 92671732010, 92671732011, 92671732012,
92671732013, 92671732014
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 06/14/23 16:04
4-Bromofluorobenzene (S)%92 66-130 06/14/23 16:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4048849LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 39.350.1 79 70-130
4-Bromofluorobenzene (S)%95 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4048851MATRIX SPIKE SAMPLE:
MSSpike
Result
92670914002
Gas Range Organics (C6-C10)mg/kg 64.874.8 86 57-154ND
4-Bromofluorobenzene (S)%101 66-130
Parameter Units
Dup
Result QualifiersRPDResult
92670914001
4048850SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%9595
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92671732
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
780779
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92671732005, 92671732006, 92671732008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4050307
Associated Lab Samples:92671732005, 92671732006, 92671732008
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 06/15/23 14:53
4-Bromofluorobenzene (S)%95 66-130 06/15/23 14:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4050308LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 37.650.4 75 70-130
4-Bromofluorobenzene (S)%98 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4050310MATRIX SPIKE SAMPLE:
MSSpike
Result
92671707001
Gas Range Organics (C6-C10)mg/kg 24.725.1 98 57-154ND
4-Bromofluorobenzene (S)%107 66-130
Parameter Units
Dup
Result QualifiersRPDResult
92672244001
4050309SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%9598
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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Asheville, NC 28804
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Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92671732
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
780780
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92671732003, 92671732004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4050322
Associated Lab Samples:92671732003, 92671732004
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 06/15/23 15:21
4-Bromofluorobenzene (S)%95 66-130 06/15/23 15:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4050323LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 37.050.4 74 70-130
4-Bromofluorobenzene (S)%95 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4050325MATRIX SPIKE SAMPLE:
MSSpike
Result
92672497005
Gas Range Organics (C6-C10)mg/kg 74.775.4 79 57-15414.7
4-Bromofluorobenzene (S)%113 66-130
Parameter Units
Dup
Result QualifiersRPDResult
92672497004
4050324SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg 23.5 422.6
4-Bromofluorobenzene (S)%106109
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92671732
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
779796
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92671732001, 92671732002, 92671732004, 92671732005, 92671732006, 92671732007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4045408
Associated Lab Samples:92671732001, 92671732002, 92671732004, 92671732005, 92671732006, 92671732007
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 06/12/23 20:29
n-Pentacosane (S)%75 10-133 06/12/23 20:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4045409LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 55.767.6 82 43-130
n-Pentacosane (S)%80 10-133
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4045410MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92671707001
4045411
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Range Organics(C10-
C28)mg/kg 85.8 41 15-13022 285.8679 714 698
n-Pentacosane (S)%S015210-133141
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92671732
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
779908
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92671732008, 92671732009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4045552
Associated Lab Samples:92671732008, 92671732009
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 06/12/23 18:20
n-Pentacosane (S)%98 10-133 06/12/23 18:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4045553LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 54.465.8 83 43-130
n-Pentacosane (S)%80 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4045554MATRIX SPIKE SAMPLE:
MSSpike
Result
92671732008
Diesel Range Organics(C10-C28)mg/kg 74.585 87 15-130ND
n-Pentacosane (S)%71 10-133
Parameter Units
Dup
Result QualifiersRPDResult
92671732009
4045555SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg NDND
n-Pentacosane (S)%7885
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92671732
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
779999
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92671732001, 92671732002, 92671732003, 92671732004, 92671732005, 92671732006, 92671732007,
92671732008, 92671732009, 92671732010, 92671732011, 92671732012, 92671732013, 92671732014
Parameter Units
Dup
Result QualifiersRPDResult
92671726006
4046069SAMPLE DUPLICATE:
Percent Moisture %15.4 N2215.7
Parameter Units
Dup
Result QualifiersRPDResult
92671732014
4046070SAMPLE DUPLICATE:
Percent Moisture %24.7 N2225.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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Asheville, NC 28804
[phone]
Page 24 of 31
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92671732
ONE STOP 15
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 31
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92671732
ONE STOP 15
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92671732001 779796 779897FP-1 EPA 3546 EPA 8015C
92671732002 779796 779897FP-2 EPA 3546 EPA 8015C
92671732004 779796 779897T-1 EPA 3546 EPA 8015C
92671732005 779796 779897T-2 EPA 3546 EPA 8015C
92671732006 779796 779897T-3 EPA 3546 EPA 8015C
92671732007 779796 779897T-4 EPA 3546 EPA 8015C
92671732008 779908 780031T-5 EPA 3546 EPA 8015C
92671732009 779908 780031T-6 EPA 3546 EPA 8015C
92671732001 780506 780523FP-1 EPA 5030B EPA 8015C
92671732002 780506 780523FP-2 EPA 5030B EPA 8015C
92671732003 780780 780804FP-3 EPA 5030B EPA 8015C
92671732004 780780 780804T-1 EPA 5030B EPA 8015C
92671732005 780779 780806T-2 EPA 5030B EPA 8015C
92671732006 780779 780806T-3 EPA 5030B EPA 8015C
92671732007 780506 780523T-4 EPA 5030B EPA 8015C
92671732008 780779 780806T-5 EPA 5030B EPA 8015C
92671732009 780506 780523T-6 EPA 5030B EPA 8015C
92671732010 780506 780523T-8 EPA 5030B EPA 8015C
92671732011 780506 780523T-9 EPA 5030B EPA 8015C
92671732012 780506 780523T-10 EPA 5030B EPA 8015C
92671732013 780506 780523T-11 EPA 5030B EPA 8015C
92671732014 780506 780523T-12 EPA 5030B EPA 8015C
92671732001 779999FP-1 SW-846
92671732002 779999FP-2 SW-846
92671732003 779999FP-3 SW-846
92671732004 779999T-1 SW-846
92671732005 779999T-2 SW-846
92671732006 779999T-3 SW-846
92671732007 779999T-4 SW-846
92671732008 779999T-5 SW-846
92671732009 779999T-6 SW-846
92671732010 779999T-8 SW-846
92671732011 779999T-9 SW-846
92671732012 779999T-10 SW-846
92671732013 779999T-11 SW-846
92671732014 779999T-12 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/20/2023 09:29 AM
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Page 26 of 31
Page 27 of 31
Page 28 of 31
Page 29 of 31
Page 30 of 31
Page 31 of 31
#=CL#
June 26, 2023
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92672500
92672500
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
105 Charlotte Highway
Asheville, NC 28803
ONE STOP 15
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on June 14, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Asheville, NC 28804
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Page 1 of 93
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92672500
ONE STOP 15
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Asheville, NC 28804
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Page 2 of 93
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92672500
ONE STOP 15
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92672500001 SOIL-D-1 MADEP EPH 7 PASI-CBAJ
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92672500002 SOIL-D-2 MADEP EPH 7 PASI-CBAJ
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92672500003 SOIL-D-3 EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92672500004 SOIL-D-4 EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92672500005 SOIL-A MADEP EPH 7 PASI-CBAJ
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92672500006 SOIL-B MADEP EPH 7 PASI-CBAJ
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92672500007 SOIL-C MADEP EPH 7 PASI-CBAJ
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92672500008 SOIL-D MADEP EPH 7 PASI-CBAJ
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92672500009 SOIL-E EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-1 Lab ID:92672500001 Collected:06/13/23 11:40 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 06/19/23 13:12 N206/18/23 11:3012.6 1
Aliphatic (C19-C36)ND mg/kg 06/19/23 13:12 N206/18/23 11:3012.6 1
Aromatic (C11-C22)ND mg/kg 06/19/23 13:12 N206/18/23 11:3012.6 1
Surrogates
1-Chlorooctadecane (S)87 %06/19/23 13:12 3386-33-206/18/23 11:3040-140 1
o-Terphenyl (S)54 %06/19/23 13:12 84-15-106/18/23 11:3040-140 1
2-Fluorobiphenyl (S)69 %06/19/23 13:12 321-60-806/18/23 11:3040-140 1
2-Bromonaphthalene (S)72 %06/19/23 13:12 580-13-206/18/23 11:3040-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/19/23 08:57 83-32-906/15/23 16:084221
Acenaphthylene ND ug/kg 06/19/23 08:57 208-96-806/15/23 16:084221
Aniline ND ug/kg 06/19/23 08:57 62-53-306/15/23 16:084221
Anthracene ND ug/kg 06/19/23 08:57 120-12-706/15/23 16:084221
Benzo(a)anthracene ND ug/kg 06/19/23 08:57 56-55-306/15/23 16:084221
Benzo(a)pyrene ND ug/kg 06/19/23 08:57 50-32-806/15/23 16:084221
Benzo(b)fluoranthene ND ug/kg 06/19/23 08:57 205-99-206/15/23 16:084221
Benzo(g,h,i)perylene ND ug/kg 06/19/23 08:57 191-24-206/15/23 16:084221
Benzo(k)fluoranthene ND ug/kg 06/19/23 08:57 207-08-906/15/23 16:084221
Benzoic Acid ND ug/kg 06/19/23 08:57 65-85-006/15/23 16:0821101
Benzyl alcohol ND ug/kg 06/19/23 08:57 100-51-606/15/23 16:088441
4-Bromophenylphenyl ether ND ug/kg 06/19/23 08:57 101-55-306/15/23 16:084221
Butylbenzylphthalate ND ug/kg 06/19/23 08:57 85-68-706/15/23 16:084221
4-Chloro-3-methylphenol ND ug/kg 06/19/23 08:57 59-50-706/15/23 16:088441
4-Chloroaniline ND ug/kg 06/19/23 08:57 106-47-806/15/23 16:088441
bis(2-Chloroethoxy)methane ND ug/kg 06/19/23 08:57 111-91-106/15/23 16:084221
bis(2-Chloroethyl) ether ND ug/kg 06/19/23 08:57 111-44-406/15/23 16:084221
2-Chloronaphthalene ND ug/kg 06/19/23 08:57 91-58-706/15/23 16:084221
2-Chlorophenol ND ug/kg 06/19/23 08:57 95-57-806/15/23 16:084221
4-Chlorophenylphenyl ether ND ug/kg 06/19/23 08:57 7005-72-306/15/23 16:084221
Chrysene ND ug/kg 06/19/23 08:57 218-01-906/15/23 16:084221
Dibenz(a,h)anthracene ND ug/kg 06/19/23 08:57 53-70-306/15/23 16:084221
Dibenzofuran ND ug/kg 06/19/23 08:57 132-64-906/15/23 16:084221
1,2-Dichlorobenzene ND ug/kg 06/19/23 08:57 95-50-106/15/23 16:084221
1,3-Dichlorobenzene ND ug/kg 06/19/23 08:57 541-73-106/15/23 16:084221
1,4-Dichlorobenzene ND ug/kg 06/19/23 08:57 106-46-706/15/23 16:084221
3,3'-Dichlorobenzidine ND ug/kg 06/19/23 08:57 91-94-106/15/23 16:088441
2,4-Dichlorophenol ND ug/kg 06/19/23 08:57 120-83-206/15/23 16:084221
Diethylphthalate ND ug/kg 06/19/23 08:57 84-66-206/15/23 16:084221
2,4-Dimethylphenol ND ug/kg 06/19/23 08:57 105-67-906/15/23 16:084221
Dimethylphthalate ND ug/kg 06/19/23 08:57 131-11-306/15/23 16:084221
Di-n-butylphthalate ND ug/kg 06/19/23 08:57 84-74-206/15/23 16:084221
4,6-Dinitro-2-methylphenol ND ug/kg 06/19/23 08:57 534-52-106/15/23 16:088441
2,4-Dinitrophenol ND ug/kg 06/19/23 08:57 51-28-506/15/23 16:0821101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-1 Lab ID:92672500001 Collected:06/13/23 11:40 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 06/19/23 08:57 121-14-206/15/23 16:084221
2,6-Dinitrotoluene ND ug/kg 06/19/23 08:57 606-20-206/15/23 16:084221
Di-n-octylphthalate ND ug/kg 06/19/23 08:57 117-84-006/15/23 16:084221
bis(2-Ethylhexyl)phthalate ND ug/kg 06/19/23 08:57 117-81-706/15/23 16:084221
Fluoranthene ND ug/kg 06/19/23 08:57 206-44-006/15/23 16:084221
Fluorene ND ug/kg 06/19/23 08:57 86-73-706/15/23 16:084221
Hexachloro-1,3-butadiene ND ug/kg 06/19/23 08:57 87-68-306/15/23 16:084221
Hexachlorobenzene ND ug/kg 06/19/23 08:57 118-74-106/15/23 16:084221
Hexachlorocyclopentadiene ND ug/kg 06/19/23 08:57 77-47-4 v206/15/23 16:084221
Hexachloroethane ND ug/kg 06/19/23 08:57 67-72-106/15/23 16:084221
Indeno(1,2,3-cd)pyrene ND ug/kg 06/19/23 08:57 193-39-506/15/23 16:084221
Isophorone ND ug/kg 06/19/23 08:57 78-59-106/15/23 16:084221
1-Methylnaphthalene ND ug/kg 06/19/23 08:57 90-12-006/15/23 16:084221
2-Methylnaphthalene ND ug/kg 06/19/23 08:57 91-57-606/15/23 16:084221
2-Methylphenol(o-Cresol)ND ug/kg 06/19/23 08:57 95-48-706/15/23 16:084221
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/19/23 08:57 15831-10-406/15/23 16:084221
Naphthalene ND ug/kg 06/19/23 08:57 91-20-306/15/23 16:084221
2-Nitroaniline ND ug/kg 06/19/23 08:57 88-74-406/15/23 16:0821101
3-Nitroaniline ND ug/kg 06/19/23 08:57 99-09-206/15/23 16:0821101
4-Nitroaniline ND ug/kg 06/19/23 08:57 100-01-606/15/23 16:088441
Nitrobenzene ND ug/kg 06/19/23 08:57 98-95-306/15/23 16:084221
2-Nitrophenol ND ug/kg 06/19/23 08:57 88-75-506/15/23 16:084221
4-Nitrophenol ND ug/kg 06/19/23 08:57 100-02-706/15/23 16:0821101
N-Nitrosodimethylamine ND ug/kg 06/19/23 08:57 62-75-906/15/23 16:084221
N-Nitroso-di-n-propylamine ND ug/kg 06/19/23 08:57 621-64-706/15/23 16:084221
N-Nitrosodiphenylamine ND ug/kg 06/19/23 08:57 86-30-606/15/23 16:084221
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/19/23 08:57 108-60-106/15/23 16:084221
Pentachlorophenol ND ug/kg 06/19/23 08:57 87-86-506/15/23 16:088441
Phenanthrene ND ug/kg 06/19/23 08:57 85-01-806/15/23 16:084221
Phenol ND ug/kg 06/19/23 08:57 108-95-206/15/23 16:084221
Pyrene ND ug/kg 06/19/23 08:57 129-00-006/15/23 16:084221
Pyridine ND ug/kg 06/19/23 08:57 110-86-106/15/23 16:084221
1,2,4-Trichlorobenzene ND ug/kg 06/19/23 08:57 120-82-106/15/23 16:084221
2,4,5-Trichlorophenol ND ug/kg 06/19/23 08:57 95-95-406/15/23 16:084221
2,4,6-Trichlorophenol ND ug/kg 06/19/23 08:57 88-06-206/15/23 16:084221
Surrogates
Nitrobenzene-d5 (S)56 %06/19/23 08:57 4165-60-006/15/23 16:0810-130 1
2-Fluorobiphenyl (S)56 %06/19/23 08:57 321-60-806/15/23 16:0810-130 1
Terphenyl-d14 (S)75 %06/19/23 08:57 1718-51-006/15/23 16:0810-130 1
Phenol-d6 (S)53 %06/19/23 08:57 13127-88-306/15/23 16:0810-130 1
2-Fluorophenol (S)49 %06/19/23 08:57 367-12-406/15/23 16:0810-130 1
2,4,6-Tribromophenol (S)62 %06/19/23 08:57 118-79-606/15/23 16:0810-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-1 Lab ID:92672500001 Collected:06/13/23 11:40 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/17/23 17:19 67-64-106/16/23 23:101811
Benzene ND ug/kg 06/17/23 17:19 71-43-206/16/23 23:109.1 1
Bromobenzene ND ug/kg 06/17/23 17:19 108-86-106/16/23 23:109.1 1
Bromochloromethane ND ug/kg 06/17/23 17:19 74-97-506/16/23 23:109.1 1
Bromodichloromethane ND ug/kg 06/17/23 17:19 75-27-406/16/23 23:109.1 1
Bromoform ND ug/kg 06/17/23 17:19 75-25-206/16/23 23:109.1 1
Bromomethane ND ug/kg 06/17/23 17:19 74-83-906/16/23 23:1036.3 1
2-Butanone (MEK)ND ug/kg 06/17/23 17:19 78-93-306/16/23 23:101811
n-Butylbenzene ND ug/kg 06/17/23 17:19 104-51-806/16/23 23:109.1 1
sec-Butylbenzene ND ug/kg 06/17/23 17:19 135-98-806/16/23 23:109.1 1
tert-Butylbenzene ND ug/kg 06/17/23 17:19 98-06-606/16/23 23:109.1 1
Carbon tetrachloride ND ug/kg 06/17/23 17:19 56-23-506/16/23 23:109.1 1
Chlorobenzene ND ug/kg 06/17/23 17:19 108-90-706/16/23 23:109.1 1
Chloroethane ND ug/kg 06/17/23 17:19 75-00-3 v106/16/23 23:1018.1 1
Chloroform ND ug/kg 06/17/23 17:19 67-66-306/16/23 23:109.1 1
Chloromethane ND ug/kg 06/17/23 17:19 74-87-3 L1,v106/16/23 23:1018.1 1
2-Chlorotoluene ND ug/kg 06/17/23 17:19 95-49-806/16/23 23:109.1 1
4-Chlorotoluene ND ug/kg 06/17/23 17:19 106-43-406/16/23 23:109.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/17/23 17:19 96-12-806/16/23 23:109.1 1
Dibromochloromethane ND ug/kg 06/17/23 17:19 124-48-106/16/23 23:109.1 1
1,2-Dibromoethane (EDB)ND ug/kg 06/17/23 17:19 106-93-406/16/23 23:109.1 1
Dibromomethane ND ug/kg 06/17/23 17:19 74-95-306/16/23 23:109.1 1
1,2-Dichlorobenzene ND ug/kg 06/17/23 17:19 95-50-106/16/23 23:109.1 1
1,3-Dichlorobenzene ND ug/kg 06/17/23 17:19 541-73-106/16/23 23:109.1 1
1,4-Dichlorobenzene ND ug/kg 06/17/23 17:19 106-46-706/16/23 23:109.1 1
Dichlorodifluoromethane ND ug/kg 06/17/23 17:19 75-71-806/16/23 23:1018.1 1
1,1-Dichloroethane ND ug/kg 06/17/23 17:19 75-34-306/16/23 23:109.1 1
1,2-Dichloroethane ND ug/kg 06/17/23 17:19 107-06-206/16/23 23:109.1 1
1,1-Dichloroethene ND ug/kg 06/17/23 17:19 75-35-406/16/23 23:109.1 1
cis-1,2-Dichloroethene ND ug/kg 06/17/23 17:19 156-59-206/16/23 23:109.1 1
trans-1,2-Dichloroethene ND ug/kg 06/17/23 17:19 156-60-506/16/23 23:109.1 1
1,2-Dichloropropane ND ug/kg 06/17/23 17:19 78-87-506/16/23 23:109.1 1
1,3-Dichloropropane ND ug/kg 06/17/23 17:19 142-28-906/16/23 23:109.1 1
2,2-Dichloropropane ND ug/kg 06/17/23 17:19 594-20-706/16/23 23:109.1 1
1,1-Dichloropropene ND ug/kg 06/17/23 17:19 563-58-606/16/23 23:109.1 1
cis-1,3-Dichloropropene ND ug/kg 06/17/23 17:19 10061-01-506/16/23 23:109.1 1
trans-1,3-Dichloropropene ND ug/kg 06/17/23 17:19 10061-02-606/16/23 23:109.1 1
Diisopropyl ether ND ug/kg 06/17/23 17:19 108-20-306/16/23 23:109.1 1
Ethylbenzene ND ug/kg 06/17/23 17:19 100-41-406/16/23 23:109.1 1
Hexachloro-1,3-butadiene ND ug/kg 06/17/23 17:19 87-68-306/16/23 23:1018.1 1
2-Hexanone ND ug/kg 06/17/23 17:19 591-78-6 v106/16/23 23:1090.7 1
Isopropylbenzene (Cumene)ND ug/kg 06/17/23 17:19 98-82-806/16/23 23:109.1 1
p-Isopropyltoluene ND ug/kg 06/17/23 17:19 99-87-606/16/23 23:109.1 1
Methylene Chloride ND ug/kg 06/17/23 17:19 75-09-206/16/23 23:1036.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/17/23 17:19 108-10-106/16/23 23:1090.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-1 Lab ID:92672500001 Collected:06/13/23 11:40 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/17/23 17:19 1634-04-406/16/23 23:109.1 1
Naphthalene ND ug/kg 06/17/23 17:19 91-20-306/16/23 23:109.1 1
n-Propylbenzene ND ug/kg 06/17/23 17:19 103-65-106/16/23 23:109.1 1
Styrene ND ug/kg 06/17/23 17:19 100-42-506/16/23 23:109.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/17/23 17:19 630-20-606/16/23 23:109.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/17/23 17:19 79-34-506/16/23 23:109.1 1
Tetrachloroethene ND ug/kg 06/17/23 17:19 127-18-406/16/23 23:109.1 1
Toluene ND ug/kg 06/17/23 17:19 108-88-306/16/23 23:109.1 1
1,2,3-Trichlorobenzene ND ug/kg 06/17/23 17:19 87-61-606/16/23 23:109.1 1
1,2,4-Trichlorobenzene ND ug/kg 06/17/23 17:19 120-82-106/16/23 23:109.1 1
1,1,1-Trichloroethane ND ug/kg 06/17/23 17:19 71-55-606/16/23 23:109.1 1
1,1,2-Trichloroethane ND ug/kg 06/17/23 17:19 79-00-506/16/23 23:109.1 1
Trichloroethene ND ug/kg 06/17/23 17:19 79-01-606/16/23 23:109.1 1
Trichlorofluoromethane ND ug/kg 06/17/23 17:19 75-69-406/16/23 23:109.1 1
1,2,3-Trichloropropane ND ug/kg 06/17/23 17:19 96-18-406/16/23 23:109.1 1
1,2,4-Trimethylbenzene ND ug/kg 06/17/23 17:19 95-63-606/16/23 23:109.1 1
1,3,5-Trimethylbenzene ND ug/kg 06/17/23 17:19 108-67-806/16/23 23:109.1 1
Vinyl acetate ND ug/kg 06/17/23 17:19 108-05-406/16/23 23:1090.7 1
Vinyl chloride ND ug/kg 06/17/23 17:19 75-01-406/16/23 23:1018.1 1
Xylene (Total)ND ug/kg 06/17/23 17:19 1330-20-706/16/23 23:1018.1 1
m&p-Xylene ND ug/kg 06/17/23 17:19 179601-23-106/16/23 23:1018.1 1
o-Xylene ND ug/kg 06/17/23 17:19 95-47-606/16/23 23:109.1 1
Surrogates
Toluene-d8 (S)101 %06/17/23 17:19 2037-26-506/16/23 23:1070-130 1
4-Bromofluorobenzene (S)106 %06/17/23 17:19 460-00-406/16/23 23:1070-130 1
1,2-Dichloroethane-d4 (S)107 %06/17/23 17:19 17060-07-006/16/23 23:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.7 %06/15/23 16:56 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-2 Lab ID:92672500002 Collected:06/13/23 11:45 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 06/19/23 13:37 N206/18/23 11:3011.1 1
Aliphatic (C19-C36)ND mg/kg 06/19/23 13:37 N206/18/23 11:3011.1 1
Aromatic (C11-C22)ND mg/kg 06/19/23 13:37 N206/18/23 11:3011.1 1
Surrogates
1-Chlorooctadecane (S)88 %06/19/23 13:37 3386-33-206/18/23 11:3040-140 1
o-Terphenyl (S)56 %06/19/23 13:37 84-15-106/18/23 11:3040-140 1
2-Fluorobiphenyl (S)81 %06/19/23 13:37 321-60-806/18/23 11:3040-140 1
2-Bromonaphthalene (S)84 %06/19/23 13:37 580-13-206/18/23 11:3040-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/19/23 09:25 83-32-906/15/23 16:083701
Acenaphthylene ND ug/kg 06/19/23 09:25 208-96-806/15/23 16:083701
Aniline ND ug/kg 06/19/23 09:25 62-53-306/15/23 16:083701
Anthracene ND ug/kg 06/19/23 09:25 120-12-706/15/23 16:083701
Benzo(a)anthracene ND ug/kg 06/19/23 09:25 56-55-306/15/23 16:083701
Benzo(a)pyrene ND ug/kg 06/19/23 09:25 50-32-806/15/23 16:083701
Benzo(b)fluoranthene ND ug/kg 06/19/23 09:25 205-99-206/15/23 16:083701
Benzo(g,h,i)perylene ND ug/kg 06/19/23 09:25 191-24-206/15/23 16:083701
Benzo(k)fluoranthene ND ug/kg 06/19/23 09:25 207-08-906/15/23 16:083701
Benzoic Acid ND ug/kg 06/19/23 09:25 65-85-006/15/23 16:0818501
Benzyl alcohol ND ug/kg 06/19/23 09:25 100-51-606/15/23 16:087401
4-Bromophenylphenyl ether ND ug/kg 06/19/23 09:25 101-55-306/15/23 16:083701
Butylbenzylphthalate ND ug/kg 06/19/23 09:25 85-68-706/15/23 16:083701
4-Chloro-3-methylphenol ND ug/kg 06/19/23 09:25 59-50-706/15/23 16:087401
4-Chloroaniline ND ug/kg 06/19/23 09:25 106-47-806/15/23 16:087401
bis(2-Chloroethoxy)methane ND ug/kg 06/19/23 09:25 111-91-106/15/23 16:083701
bis(2-Chloroethyl) ether ND ug/kg 06/19/23 09:25 111-44-406/15/23 16:083701
2-Chloronaphthalene ND ug/kg 06/19/23 09:25 91-58-706/15/23 16:083701
2-Chlorophenol ND ug/kg 06/19/23 09:25 95-57-806/15/23 16:083701
4-Chlorophenylphenyl ether ND ug/kg 06/19/23 09:25 7005-72-306/15/23 16:083701
Chrysene ND ug/kg 06/19/23 09:25 218-01-906/15/23 16:083701
Dibenz(a,h)anthracene ND ug/kg 06/19/23 09:25 53-70-306/15/23 16:083701
Dibenzofuran ND ug/kg 06/19/23 09:25 132-64-906/15/23 16:083701
1,2-Dichlorobenzene ND ug/kg 06/19/23 09:25 95-50-106/15/23 16:083701
1,3-Dichlorobenzene ND ug/kg 06/19/23 09:25 541-73-106/15/23 16:083701
1,4-Dichlorobenzene ND ug/kg 06/19/23 09:25 106-46-706/15/23 16:083701
3,3'-Dichlorobenzidine ND ug/kg 06/19/23 09:25 91-94-106/15/23 16:087401
2,4-Dichlorophenol ND ug/kg 06/19/23 09:25 120-83-206/15/23 16:083701
Diethylphthalate ND ug/kg 06/19/23 09:25 84-66-206/15/23 16:083701
2,4-Dimethylphenol ND ug/kg 06/19/23 09:25 105-67-906/15/23 16:083701
Dimethylphthalate ND ug/kg 06/19/23 09:25 131-11-306/15/23 16:083701
Di-n-butylphthalate ND ug/kg 06/19/23 09:25 84-74-206/15/23 16:083701
4,6-Dinitro-2-methylphenol ND ug/kg 06/19/23 09:25 534-52-106/15/23 16:087401
2,4-Dinitrophenol ND ug/kg 06/19/23 09:25 51-28-506/15/23 16:0818501
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-2 Lab ID:92672500002 Collected:06/13/23 11:45 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 06/19/23 09:25 121-14-206/15/23 16:083701
2,6-Dinitrotoluene ND ug/kg 06/19/23 09:25 606-20-206/15/23 16:083701
Di-n-octylphthalate ND ug/kg 06/19/23 09:25 117-84-006/15/23 16:083701
bis(2-Ethylhexyl)phthalate ND ug/kg 06/19/23 09:25 117-81-706/15/23 16:083701
Fluoranthene ND ug/kg 06/19/23 09:25 206-44-006/15/23 16:083701
Fluorene ND ug/kg 06/19/23 09:25 86-73-706/15/23 16:083701
Hexachloro-1,3-butadiene ND ug/kg 06/19/23 09:25 87-68-306/15/23 16:083701
Hexachlorobenzene ND ug/kg 06/19/23 09:25 118-74-106/15/23 16:083701
Hexachlorocyclopentadiene ND ug/kg 06/19/23 09:25 77-47-4 v206/15/23 16:083701
Hexachloroethane ND ug/kg 06/19/23 09:25 67-72-106/15/23 16:083701
Indeno(1,2,3-cd)pyrene ND ug/kg 06/19/23 09:25 193-39-506/15/23 16:083701
Isophorone ND ug/kg 06/19/23 09:25 78-59-106/15/23 16:083701
1-Methylnaphthalene ND ug/kg 06/19/23 09:25 90-12-006/15/23 16:083701
2-Methylnaphthalene ND ug/kg 06/19/23 09:25 91-57-606/15/23 16:083701
2-Methylphenol(o-Cresol)ND ug/kg 06/19/23 09:25 95-48-706/15/23 16:083701
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/19/23 09:25 15831-10-406/15/23 16:083701
Naphthalene ND ug/kg 06/19/23 09:25 91-20-306/15/23 16:083701
2-Nitroaniline ND ug/kg 06/19/23 09:25 88-74-406/15/23 16:0818501
3-Nitroaniline ND ug/kg 06/19/23 09:25 99-09-206/15/23 16:0818501
4-Nitroaniline ND ug/kg 06/19/23 09:25 100-01-606/15/23 16:087401
Nitrobenzene ND ug/kg 06/19/23 09:25 98-95-306/15/23 16:083701
2-Nitrophenol ND ug/kg 06/19/23 09:25 88-75-506/15/23 16:083701
4-Nitrophenol ND ug/kg 06/19/23 09:25 100-02-706/15/23 16:0818501
N-Nitrosodimethylamine ND ug/kg 06/19/23 09:25 62-75-906/15/23 16:083701
N-Nitroso-di-n-propylamine ND ug/kg 06/19/23 09:25 621-64-706/15/23 16:083701
N-Nitrosodiphenylamine ND ug/kg 06/19/23 09:25 86-30-606/15/23 16:083701
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/19/23 09:25 108-60-106/15/23 16:083701
Pentachlorophenol ND ug/kg 06/19/23 09:25 87-86-506/15/23 16:087401
Phenanthrene ND ug/kg 06/19/23 09:25 85-01-806/15/23 16:083701
Phenol ND ug/kg 06/19/23 09:25 108-95-206/15/23 16:083701
Pyrene ND ug/kg 06/19/23 09:25 129-00-006/15/23 16:083701
Pyridine ND ug/kg 06/19/23 09:25 110-86-106/15/23 16:083701
1,2,4-Trichlorobenzene ND ug/kg 06/19/23 09:25 120-82-106/15/23 16:083701
2,4,5-Trichlorophenol ND ug/kg 06/19/23 09:25 95-95-406/15/23 16:083701
2,4,6-Trichlorophenol ND ug/kg 06/19/23 09:25 88-06-206/15/23 16:083701
Surrogates
Nitrobenzene-d5 (S)65 %06/19/23 09:25 4165-60-006/15/23 16:0810-130 1
2-Fluorobiphenyl (S)65 %06/19/23 09:25 321-60-806/15/23 16:0810-130 1
Terphenyl-d14 (S)77 %06/19/23 09:25 1718-51-006/15/23 16:0810-130 1
Phenol-d6 (S)66 %06/19/23 09:25 13127-88-306/15/23 16:0810-130 1
2-Fluorophenol (S)60 %06/19/23 09:25 367-12-406/15/23 16:0810-130 1
2,4,6-Tribromophenol (S)71 %06/19/23 09:25 118-79-606/15/23 16:0810-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-2 Lab ID:92672500002 Collected:06/13/23 11:45 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/17/23 17:38 67-64-106/16/23 23:101701
Benzene ND ug/kg 06/17/23 17:38 71-43-206/16/23 23:108.5 1
Bromobenzene ND ug/kg 06/17/23 17:38 108-86-106/16/23 23:108.5 1
Bromochloromethane ND ug/kg 06/17/23 17:38 74-97-506/16/23 23:108.5 1
Bromodichloromethane ND ug/kg 06/17/23 17:38 75-27-406/16/23 23:108.5 1
Bromoform ND ug/kg 06/17/23 17:38 75-25-206/16/23 23:108.5 1
Bromomethane ND ug/kg 06/17/23 17:38 74-83-906/16/23 23:1034.1 1
2-Butanone (MEK)ND ug/kg 06/17/23 17:38 78-93-306/16/23 23:101701
n-Butylbenzene ND ug/kg 06/17/23 17:38 104-51-806/16/23 23:108.5 1
sec-Butylbenzene ND ug/kg 06/17/23 17:38 135-98-806/16/23 23:108.5 1
tert-Butylbenzene ND ug/kg 06/17/23 17:38 98-06-606/16/23 23:108.5 1
Carbon tetrachloride ND ug/kg 06/17/23 17:38 56-23-506/16/23 23:108.5 1
Chlorobenzene ND ug/kg 06/17/23 17:38 108-90-706/16/23 23:108.5 1
Chloroethane ND ug/kg 06/17/23 17:38 75-00-3 v106/16/23 23:1017.0 1
Chloroform ND ug/kg 06/17/23 17:38 67-66-306/16/23 23:108.5 1
Chloromethane ND ug/kg 06/17/23 17:38 74-87-3 L1,v106/16/23 23:1017.0 1
2-Chlorotoluene ND ug/kg 06/17/23 17:38 95-49-806/16/23 23:108.5 1
4-Chlorotoluene ND ug/kg 06/17/23 17:38 106-43-406/16/23 23:108.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/17/23 17:38 96-12-806/16/23 23:108.5 1
Dibromochloromethane ND ug/kg 06/17/23 17:38 124-48-106/16/23 23:108.5 1
1,2-Dibromoethane (EDB)ND ug/kg 06/17/23 17:38 106-93-406/16/23 23:108.5 1
Dibromomethane ND ug/kg 06/17/23 17:38 74-95-306/16/23 23:108.5 1
1,2-Dichlorobenzene ND ug/kg 06/17/23 17:38 95-50-106/16/23 23:108.5 1
1,3-Dichlorobenzene ND ug/kg 06/17/23 17:38 541-73-106/16/23 23:108.5 1
1,4-Dichlorobenzene ND ug/kg 06/17/23 17:38 106-46-706/16/23 23:108.5 1
Dichlorodifluoromethane ND ug/kg 06/17/23 17:38 75-71-806/16/23 23:1017.0 1
1,1-Dichloroethane ND ug/kg 06/17/23 17:38 75-34-306/16/23 23:108.5 1
1,2-Dichloroethane ND ug/kg 06/17/23 17:38 107-06-206/16/23 23:108.5 1
1,1-Dichloroethene ND ug/kg 06/17/23 17:38 75-35-406/16/23 23:108.5 1
cis-1,2-Dichloroethene ND ug/kg 06/17/23 17:38 156-59-206/16/23 23:108.5 1
trans-1,2-Dichloroethene ND ug/kg 06/17/23 17:38 156-60-506/16/23 23:108.5 1
1,2-Dichloropropane ND ug/kg 06/17/23 17:38 78-87-506/16/23 23:108.5 1
1,3-Dichloropropane ND ug/kg 06/17/23 17:38 142-28-906/16/23 23:108.5 1
2,2-Dichloropropane ND ug/kg 06/17/23 17:38 594-20-706/16/23 23:108.5 1
1,1-Dichloropropene ND ug/kg 06/17/23 17:38 563-58-606/16/23 23:108.5 1
cis-1,3-Dichloropropene ND ug/kg 06/17/23 17:38 10061-01-506/16/23 23:108.5 1
trans-1,3-Dichloropropene ND ug/kg 06/17/23 17:38 10061-02-606/16/23 23:108.5 1
Diisopropyl ether ND ug/kg 06/17/23 17:38 108-20-306/16/23 23:108.5 1
Ethylbenzene ND ug/kg 06/17/23 17:38 100-41-406/16/23 23:108.5 1
Hexachloro-1,3-butadiene ND ug/kg 06/17/23 17:38 87-68-306/16/23 23:1017.0 1
2-Hexanone ND ug/kg 06/17/23 17:38 591-78-6 v106/16/23 23:1085.2 1
Isopropylbenzene (Cumene)ND ug/kg 06/17/23 17:38 98-82-806/16/23 23:108.5 1
p-Isopropyltoluene ND ug/kg 06/17/23 17:38 99-87-606/16/23 23:108.5 1
Methylene Chloride ND ug/kg 06/17/23 17:38 75-09-206/16/23 23:1034.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/17/23 17:38 108-10-106/16/23 23:1085.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-2 Lab ID:92672500002 Collected:06/13/23 11:45 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/17/23 17:38 1634-04-406/16/23 23:108.5 1
Naphthalene ND ug/kg 06/17/23 17:38 91-20-306/16/23 23:108.5 1
n-Propylbenzene ND ug/kg 06/17/23 17:38 103-65-106/16/23 23:108.5 1
Styrene ND ug/kg 06/17/23 17:38 100-42-506/16/23 23:108.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/17/23 17:38 630-20-606/16/23 23:108.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/17/23 17:38 79-34-506/16/23 23:108.5 1
Tetrachloroethene ND ug/kg 06/17/23 17:38 127-18-406/16/23 23:108.5 1
Toluene ND ug/kg 06/17/23 17:38 108-88-306/16/23 23:108.5 1
1,2,3-Trichlorobenzene ND ug/kg 06/17/23 17:38 87-61-606/16/23 23:108.5 1
1,2,4-Trichlorobenzene ND ug/kg 06/17/23 17:38 120-82-106/16/23 23:108.5 1
1,1,1-Trichloroethane ND ug/kg 06/17/23 17:38 71-55-606/16/23 23:108.5 1
1,1,2-Trichloroethane ND ug/kg 06/17/23 17:38 79-00-506/16/23 23:108.5 1
Trichloroethene ND ug/kg 06/17/23 17:38 79-01-606/16/23 23:108.5 1
Trichlorofluoromethane ND ug/kg 06/17/23 17:38 75-69-406/16/23 23:108.5 1
1,2,3-Trichloropropane ND ug/kg 06/17/23 17:38 96-18-406/16/23 23:108.5 1
1,2,4-Trimethylbenzene ND ug/kg 06/17/23 17:38 95-63-606/16/23 23:108.5 1
1,3,5-Trimethylbenzene ND ug/kg 06/17/23 17:38 108-67-806/16/23 23:108.5 1
Vinyl acetate ND ug/kg 06/17/23 17:38 108-05-406/16/23 23:1085.2 1
Vinyl chloride ND ug/kg 06/17/23 17:38 75-01-406/16/23 23:1017.0 1
Xylene (Total)ND ug/kg 06/17/23 17:38 1330-20-706/16/23 23:1017.0 1
m&p-Xylene ND ug/kg 06/17/23 17:38 179601-23-106/16/23 23:1017.0 1
o-Xylene ND ug/kg 06/17/23 17:38 95-47-606/16/23 23:108.5 1
Surrogates
Toluene-d8 (S)102 %06/17/23 17:38 2037-26-506/16/23 23:1070-130 1
4-Bromofluorobenzene (S)104 %06/17/23 17:38 460-00-406/16/23 23:1070-130 1
1,2-Dichloroethane-d4 (S)104 %06/17/23 17:38 17060-07-006/16/23 23:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.7 %06/15/23 14:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-3 Lab ID:92672500003 Collected:06/13/23 12:35 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/17/23 17:56 67-64-106/16/23 23:101401
Benzene ND ug/kg 06/17/23 17:56 71-43-206/16/23 23:107.0 1
Bromobenzene ND ug/kg 06/17/23 17:56 108-86-106/16/23 23:107.0 1
Bromochloromethane ND ug/kg 06/17/23 17:56 74-97-506/16/23 23:107.0 1
Bromodichloromethane ND ug/kg 06/17/23 17:56 75-27-406/16/23 23:107.0 1
Bromoform ND ug/kg 06/17/23 17:56 75-25-206/16/23 23:107.0 1
Bromomethane ND ug/kg 06/17/23 17:56 74-83-906/16/23 23:1027.9 1
2-Butanone (MEK)ND ug/kg 06/17/23 17:56 78-93-306/16/23 23:101401
n-Butylbenzene ND ug/kg 06/17/23 17:56 104-51-806/16/23 23:107.0 1
sec-Butylbenzene ND ug/kg 06/17/23 17:56 135-98-806/16/23 23:107.0 1
tert-Butylbenzene ND ug/kg 06/17/23 17:56 98-06-606/16/23 23:107.0 1
Carbon tetrachloride ND ug/kg 06/17/23 17:56 56-23-506/16/23 23:107.0 1
Chlorobenzene ND ug/kg 06/17/23 17:56 108-90-706/16/23 23:107.0 1
Chloroethane ND ug/kg 06/17/23 17:56 75-00-3 v106/16/23 23:1014.0 1
Chloroform ND ug/kg 06/17/23 17:56 67-66-306/16/23 23:107.0 1
Chloromethane ND ug/kg 06/17/23 17:56 74-87-3 L1,v106/16/23 23:1014.0 1
2-Chlorotoluene ND ug/kg 06/17/23 17:56 95-49-806/16/23 23:107.0 1
4-Chlorotoluene ND ug/kg 06/17/23 17:56 106-43-406/16/23 23:107.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/17/23 17:56 96-12-806/16/23 23:107.0 1
Dibromochloromethane ND ug/kg 06/17/23 17:56 124-48-106/16/23 23:107.0 1
1,2-Dibromoethane (EDB)ND ug/kg 06/17/23 17:56 106-93-406/16/23 23:107.0 1
Dibromomethane ND ug/kg 06/17/23 17:56 74-95-306/16/23 23:107.0 1
1,2-Dichlorobenzene ND ug/kg 06/17/23 17:56 95-50-106/16/23 23:107.0 1
1,3-Dichlorobenzene ND ug/kg 06/17/23 17:56 541-73-106/16/23 23:107.0 1
1,4-Dichlorobenzene ND ug/kg 06/17/23 17:56 106-46-706/16/23 23:107.0 1
Dichlorodifluoromethane ND ug/kg 06/17/23 17:56 75-71-806/16/23 23:1014.0 1
1,1-Dichloroethane ND ug/kg 06/17/23 17:56 75-34-306/16/23 23:107.0 1
1,2-Dichloroethane ND ug/kg 06/17/23 17:56 107-06-206/16/23 23:107.0 1
1,1-Dichloroethene ND ug/kg 06/17/23 17:56 75-35-406/16/23 23:107.0 1
cis-1,2-Dichloroethene ND ug/kg 06/17/23 17:56 156-59-206/16/23 23:107.0 1
trans-1,2-Dichloroethene ND ug/kg 06/17/23 17:56 156-60-506/16/23 23:107.0 1
1,2-Dichloropropane ND ug/kg 06/17/23 17:56 78-87-506/16/23 23:107.0 1
1,3-Dichloropropane ND ug/kg 06/17/23 17:56 142-28-906/16/23 23:107.0 1
2,2-Dichloropropane ND ug/kg 06/17/23 17:56 594-20-706/16/23 23:107.0 1
1,1-Dichloropropene ND ug/kg 06/17/23 17:56 563-58-606/16/23 23:107.0 1
cis-1,3-Dichloropropene ND ug/kg 06/17/23 17:56 10061-01-506/16/23 23:107.0 1
trans-1,3-Dichloropropene ND ug/kg 06/17/23 17:56 10061-02-606/16/23 23:107.0 1
Diisopropyl ether ND ug/kg 06/17/23 17:56 108-20-306/16/23 23:107.0 1
Ethylbenzene ND ug/kg 06/17/23 17:56 100-41-406/16/23 23:107.0 1
Hexachloro-1,3-butadiene ND ug/kg 06/17/23 17:56 87-68-306/16/23 23:1014.0 1
2-Hexanone ND ug/kg 06/17/23 17:56 591-78-6 v106/16/23 23:1069.9 1
Isopropylbenzene (Cumene)ND ug/kg 06/17/23 17:56 98-82-806/16/23 23:107.0 1
p-Isopropyltoluene ND ug/kg 06/17/23 17:56 99-87-606/16/23 23:107.0 1
Methylene Chloride ND ug/kg 06/17/23 17:56 75-09-206/16/23 23:1027.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/17/23 17:56 108-10-106/16/23 23:1069.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-3 Lab ID:92672500003 Collected:06/13/23 12:35 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/17/23 17:56 1634-04-406/16/23 23:107.0 1
Naphthalene 7.2 ug/kg 06/17/23 17:56 91-20-306/16/23 23:107.0 1
n-Propylbenzene ND ug/kg 06/17/23 17:56 103-65-106/16/23 23:107.0 1
Styrene ND ug/kg 06/17/23 17:56 100-42-506/16/23 23:107.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/17/23 17:56 630-20-606/16/23 23:107.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/17/23 17:56 79-34-506/16/23 23:107.0 1
Tetrachloroethene ND ug/kg 06/17/23 17:56 127-18-406/16/23 23:107.0 1
Toluene 8.4 ug/kg 06/17/23 17:56 108-88-306/16/23 23:107.0 1
1,2,3-Trichlorobenzene ND ug/kg 06/17/23 17:56 87-61-606/16/23 23:107.0 1
1,2,4-Trichlorobenzene ND ug/kg 06/17/23 17:56 120-82-106/16/23 23:107.0 1
1,1,1-Trichloroethane ND ug/kg 06/17/23 17:56 71-55-606/16/23 23:107.0 1
1,1,2-Trichloroethane ND ug/kg 06/17/23 17:56 79-00-506/16/23 23:107.0 1
Trichloroethene ND ug/kg 06/17/23 17:56 79-01-606/16/23 23:107.0 1
Trichlorofluoromethane ND ug/kg 06/17/23 17:56 75-69-406/16/23 23:107.0 1
1,2,3-Trichloropropane ND ug/kg 06/17/23 17:56 96-18-406/16/23 23:107.0 1
1,2,4-Trimethylbenzene 10.9 ug/kg 06/17/23 17:56 95-63-606/16/23 23:107.0 1
1,3,5-Trimethylbenzene ND ug/kg 06/17/23 17:56 108-67-806/16/23 23:107.0 1
Vinyl acetate ND ug/kg 06/17/23 17:56 108-05-406/16/23 23:1069.9 1
Vinyl chloride ND ug/kg 06/17/23 17:56 75-01-406/16/23 23:1014.0 1
Xylene (Total)ND ug/kg 06/17/23 17:56 1330-20-706/16/23 23:1014.0 1
m&p-Xylene ND ug/kg 06/17/23 17:56 179601-23-106/16/23 23:1014.0 1
o-Xylene ND ug/kg 06/17/23 17:56 95-47-606/16/23 23:107.0 1
Surrogates
Toluene-d8 (S)100 %06/17/23 17:56 2037-26-506/16/23 23:1070-130 1
4-Bromofluorobenzene (S)104 %06/17/23 17:56 460-00-406/16/23 23:1070-130 1
1,2-Dichloroethane-d4 (S)107 %06/17/23 17:56 17060-07-006/16/23 23:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 9.1 %06/15/23 16:56 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-4 Lab ID:92672500004 Collected:06/13/23 12:45 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/17/23 18:15 67-64-106/16/23 23:101571
Benzene ND ug/kg 06/17/23 18:15 71-43-206/16/23 23:107.8 1
Bromobenzene ND ug/kg 06/17/23 18:15 108-86-106/16/23 23:107.8 1
Bromochloromethane ND ug/kg 06/17/23 18:15 74-97-506/16/23 23:107.8 1
Bromodichloromethane ND ug/kg 06/17/23 18:15 75-27-406/16/23 23:107.8 1
Bromoform ND ug/kg 06/17/23 18:15 75-25-206/16/23 23:107.8 1
Bromomethane ND ug/kg 06/17/23 18:15 74-83-906/16/23 23:1031.3 1
2-Butanone (MEK)ND ug/kg 06/17/23 18:15 78-93-306/16/23 23:101571
n-Butylbenzene ND ug/kg 06/17/23 18:15 104-51-806/16/23 23:107.8 1
sec-Butylbenzene ND ug/kg 06/17/23 18:15 135-98-806/16/23 23:107.8 1
tert-Butylbenzene ND ug/kg 06/17/23 18:15 98-06-606/16/23 23:107.8 1
Carbon tetrachloride ND ug/kg 06/17/23 18:15 56-23-506/16/23 23:107.8 1
Chlorobenzene ND ug/kg 06/17/23 18:15 108-90-706/16/23 23:107.8 1
Chloroethane ND ug/kg 06/17/23 18:15 75-00-3 v106/16/23 23:1015.7 1
Chloroform ND ug/kg 06/17/23 18:15 67-66-306/16/23 23:107.8 1
Chloromethane ND ug/kg 06/17/23 18:15 74-87-3 L1,v106/16/23 23:1015.7 1
2-Chlorotoluene ND ug/kg 06/17/23 18:15 95-49-806/16/23 23:107.8 1
4-Chlorotoluene ND ug/kg 06/17/23 18:15 106-43-406/16/23 23:107.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/17/23 18:15 96-12-806/16/23 23:107.8 1
Dibromochloromethane ND ug/kg 06/17/23 18:15 124-48-106/16/23 23:107.8 1
1,2-Dibromoethane (EDB)ND ug/kg 06/17/23 18:15 106-93-406/16/23 23:107.8 1
Dibromomethane ND ug/kg 06/17/23 18:15 74-95-306/16/23 23:107.8 1
1,2-Dichlorobenzene ND ug/kg 06/17/23 18:15 95-50-106/16/23 23:107.8 1
1,3-Dichlorobenzene ND ug/kg 06/17/23 18:15 541-73-106/16/23 23:107.8 1
1,4-Dichlorobenzene ND ug/kg 06/17/23 18:15 106-46-706/16/23 23:107.8 1
Dichlorodifluoromethane ND ug/kg 06/17/23 18:15 75-71-806/16/23 23:1015.7 1
1,1-Dichloroethane ND ug/kg 06/17/23 18:15 75-34-306/16/23 23:107.8 1
1,2-Dichloroethane ND ug/kg 06/17/23 18:15 107-06-206/16/23 23:107.8 1
1,1-Dichloroethene ND ug/kg 06/17/23 18:15 75-35-406/16/23 23:107.8 1
cis-1,2-Dichloroethene ND ug/kg 06/17/23 18:15 156-59-206/16/23 23:107.8 1
trans-1,2-Dichloroethene ND ug/kg 06/17/23 18:15 156-60-506/16/23 23:107.8 1
1,2-Dichloropropane ND ug/kg 06/17/23 18:15 78-87-506/16/23 23:107.8 1
1,3-Dichloropropane ND ug/kg 06/17/23 18:15 142-28-906/16/23 23:107.8 1
2,2-Dichloropropane ND ug/kg 06/17/23 18:15 594-20-706/16/23 23:107.8 1
1,1-Dichloropropene ND ug/kg 06/17/23 18:15 563-58-606/16/23 23:107.8 1
cis-1,3-Dichloropropene ND ug/kg 06/17/23 18:15 10061-01-506/16/23 23:107.8 1
trans-1,3-Dichloropropene ND ug/kg 06/17/23 18:15 10061-02-606/16/23 23:107.8 1
Diisopropyl ether ND ug/kg 06/17/23 18:15 108-20-306/16/23 23:107.8 1
Ethylbenzene ND ug/kg 06/17/23 18:15 100-41-406/16/23 23:107.8 1
Hexachloro-1,3-butadiene ND ug/kg 06/17/23 18:15 87-68-306/16/23 23:1015.7 1
2-Hexanone ND ug/kg 06/17/23 18:15 591-78-6 v106/16/23 23:1078.3 1
Isopropylbenzene (Cumene)ND ug/kg 06/17/23 18:15 98-82-806/16/23 23:107.8 1
p-Isopropyltoluene ND ug/kg 06/17/23 18:15 99-87-606/16/23 23:107.8 1
Methylene Chloride ND ug/kg 06/17/23 18:15 75-09-206/16/23 23:1031.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/17/23 18:15 108-10-106/16/23 23:1078.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D-4 Lab ID:92672500004 Collected:06/13/23 12:45 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/17/23 18:15 1634-04-406/16/23 23:107.8 1
Naphthalene ND ug/kg 06/17/23 18:15 91-20-306/16/23 23:107.8 1
n-Propylbenzene ND ug/kg 06/17/23 18:15 103-65-106/16/23 23:107.8 1
Styrene ND ug/kg 06/17/23 18:15 100-42-506/16/23 23:107.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/17/23 18:15 630-20-606/16/23 23:107.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/17/23 18:15 79-34-506/16/23 23:107.8 1
Tetrachloroethene ND ug/kg 06/17/23 18:15 127-18-406/16/23 23:107.8 1
Toluene ND ug/kg 06/17/23 18:15 108-88-306/16/23 23:107.8 1
1,2,3-Trichlorobenzene ND ug/kg 06/17/23 18:15 87-61-606/16/23 23:107.8 1
1,2,4-Trichlorobenzene ND ug/kg 06/17/23 18:15 120-82-106/16/23 23:107.8 1
1,1,1-Trichloroethane ND ug/kg 06/17/23 18:15 71-55-606/16/23 23:107.8 1
1,1,2-Trichloroethane ND ug/kg 06/17/23 18:15 79-00-506/16/23 23:107.8 1
Trichloroethene ND ug/kg 06/17/23 18:15 79-01-606/16/23 23:107.8 1
Trichlorofluoromethane ND ug/kg 06/17/23 18:15 75-69-406/16/23 23:107.8 1
1,2,3-Trichloropropane ND ug/kg 06/17/23 18:15 96-18-406/16/23 23:107.8 1
1,2,4-Trimethylbenzene 14.5 ug/kg 06/17/23 18:15 95-63-606/16/23 23:107.8 1
1,3,5-Trimethylbenzene ND ug/kg 06/17/23 18:15 108-67-806/16/23 23:107.8 1
Vinyl acetate ND ug/kg 06/17/23 18:15 108-05-406/16/23 23:1078.3 1
Vinyl chloride ND ug/kg 06/17/23 18:15 75-01-406/16/23 23:1015.7 1
Xylene (Total)ND ug/kg 06/17/23 18:15 1330-20-706/16/23 23:1015.7 1
m&p-Xylene ND ug/kg 06/17/23 18:15 179601-23-106/16/23 23:1015.7 1
o-Xylene ND ug/kg 06/17/23 18:15 95-47-606/16/23 23:107.8 1
Surrogates
Toluene-d8 (S)102 %06/17/23 18:15 2037-26-506/16/23 23:1070-130 1
4-Bromofluorobenzene (S)103 %06/17/23 18:15 460-00-406/16/23 23:1070-130 1
1,2-Dichloroethane-d4 (S)107 %06/17/23 18:15 17060-07-006/16/23 23:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.0 %06/15/23 16:56 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-A Lab ID:92672500005 Collected:06/13/23 14:00 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 06/19/23 14:03 N206/18/23 11:3011.6 1
Aliphatic (C19-C36)ND mg/kg 06/19/23 14:03 N206/18/23 11:3011.6 1
Aromatic (C11-C22)ND mg/kg 06/19/23 14:03 N206/18/23 11:3011.6 1
Surrogates
1-Chlorooctadecane (S)95 %06/19/23 14:03 3386-33-206/18/23 11:3040-140 1
o-Terphenyl (S)65 %06/19/23 14:03 84-15-106/18/23 11:3040-140 1
2-Fluorobiphenyl (S)79 %06/19/23 14:03 321-60-806/18/23 11:3040-140 1
2-Bromonaphthalene (S)80 %06/19/23 14:03 580-13-206/18/23 11:3040-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/19/23 09:52 83-32-906/15/23 16:083831
Acenaphthylene ND ug/kg 06/19/23 09:52 208-96-806/15/23 16:083831
Aniline ND ug/kg 06/19/23 09:52 62-53-306/15/23 16:083831
Anthracene ND ug/kg 06/19/23 09:52 120-12-706/15/23 16:083831
Benzo(a)anthracene ND ug/kg 06/19/23 09:52 56-55-306/15/23 16:083831
Benzo(a)pyrene ND ug/kg 06/19/23 09:52 50-32-806/15/23 16:083831
Benzo(b)fluoranthene ND ug/kg 06/19/23 09:52 205-99-206/15/23 16:083831
Benzo(g,h,i)perylene ND ug/kg 06/19/23 09:52 191-24-206/15/23 16:083831
Benzo(k)fluoranthene ND ug/kg 06/19/23 09:52 207-08-906/15/23 16:083831
Benzoic Acid ND ug/kg 06/19/23 09:52 65-85-006/15/23 16:0819101
Benzyl alcohol ND ug/kg 06/19/23 09:52 100-51-606/15/23 16:087651
4-Bromophenylphenyl ether ND ug/kg 06/19/23 09:52 101-55-306/15/23 16:083831
Butylbenzylphthalate ND ug/kg 06/19/23 09:52 85-68-706/15/23 16:083831
4-Chloro-3-methylphenol ND ug/kg 06/19/23 09:52 59-50-706/15/23 16:087651
4-Chloroaniline ND ug/kg 06/19/23 09:52 106-47-806/15/23 16:087651
bis(2-Chloroethoxy)methane ND ug/kg 06/19/23 09:52 111-91-106/15/23 16:083831
bis(2-Chloroethyl) ether ND ug/kg 06/19/23 09:52 111-44-406/15/23 16:083831
2-Chloronaphthalene ND ug/kg 06/19/23 09:52 91-58-706/15/23 16:083831
2-Chlorophenol ND ug/kg 06/19/23 09:52 95-57-806/15/23 16:083831
4-Chlorophenylphenyl ether ND ug/kg 06/19/23 09:52 7005-72-306/15/23 16:083831
Chrysene ND ug/kg 06/19/23 09:52 218-01-906/15/23 16:083831
Dibenz(a,h)anthracene ND ug/kg 06/19/23 09:52 53-70-306/15/23 16:083831
Dibenzofuran ND ug/kg 06/19/23 09:52 132-64-906/15/23 16:083831
1,2-Dichlorobenzene ND ug/kg 06/19/23 09:52 95-50-106/15/23 16:083831
1,3-Dichlorobenzene ND ug/kg 06/19/23 09:52 541-73-106/15/23 16:083831
1,4-Dichlorobenzene ND ug/kg 06/19/23 09:52 106-46-706/15/23 16:083831
3,3'-Dichlorobenzidine ND ug/kg 06/19/23 09:52 91-94-106/15/23 16:087651
2,4-Dichlorophenol ND ug/kg 06/19/23 09:52 120-83-206/15/23 16:083831
Diethylphthalate ND ug/kg 06/19/23 09:52 84-66-206/15/23 16:083831
2,4-Dimethylphenol ND ug/kg 06/19/23 09:52 105-67-906/15/23 16:083831
Dimethylphthalate ND ug/kg 06/19/23 09:52 131-11-306/15/23 16:083831
Di-n-butylphthalate ND ug/kg 06/19/23 09:52 84-74-206/15/23 16:083831
4,6-Dinitro-2-methylphenol ND ug/kg 06/19/23 09:52 534-52-106/15/23 16:087651
2,4-Dinitrophenol ND ug/kg 06/19/23 09:52 51-28-506/15/23 16:0819101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-A Lab ID:92672500005 Collected:06/13/23 14:00 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 06/19/23 09:52 121-14-206/15/23 16:083831
2,6-Dinitrotoluene ND ug/kg 06/19/23 09:52 606-20-206/15/23 16:083831
Di-n-octylphthalate ND ug/kg 06/19/23 09:52 117-84-006/15/23 16:083831
bis(2-Ethylhexyl)phthalate ND ug/kg 06/19/23 09:52 117-81-706/15/23 16:083831
Fluoranthene ND ug/kg 06/19/23 09:52 206-44-006/15/23 16:083831
Fluorene ND ug/kg 06/19/23 09:52 86-73-706/15/23 16:083831
Hexachloro-1,3-butadiene ND ug/kg 06/19/23 09:52 87-68-306/15/23 16:083831
Hexachlorobenzene ND ug/kg 06/19/23 09:52 118-74-106/15/23 16:083831
Hexachlorocyclopentadiene ND ug/kg 06/19/23 09:52 77-47-4 v206/15/23 16:083831
Hexachloroethane ND ug/kg 06/19/23 09:52 67-72-106/15/23 16:083831
Indeno(1,2,3-cd)pyrene ND ug/kg 06/19/23 09:52 193-39-506/15/23 16:083831
Isophorone ND ug/kg 06/19/23 09:52 78-59-106/15/23 16:083831
1-Methylnaphthalene ND ug/kg 06/19/23 09:52 90-12-006/15/23 16:083831
2-Methylnaphthalene ND ug/kg 06/19/23 09:52 91-57-606/15/23 16:083831
2-Methylphenol(o-Cresol)ND ug/kg 06/19/23 09:52 95-48-706/15/23 16:083831
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/19/23 09:52 15831-10-406/15/23 16:083831
Naphthalene ND ug/kg 06/19/23 09:52 91-20-306/15/23 16:083831
2-Nitroaniline ND ug/kg 06/19/23 09:52 88-74-406/15/23 16:0819101
3-Nitroaniline ND ug/kg 06/19/23 09:52 99-09-206/15/23 16:0819101
4-Nitroaniline ND ug/kg 06/19/23 09:52 100-01-606/15/23 16:087651
Nitrobenzene ND ug/kg 06/19/23 09:52 98-95-306/15/23 16:083831
2-Nitrophenol ND ug/kg 06/19/23 09:52 88-75-506/15/23 16:083831
4-Nitrophenol ND ug/kg 06/19/23 09:52 100-02-706/15/23 16:0819101
N-Nitrosodimethylamine ND ug/kg 06/19/23 09:52 62-75-906/15/23 16:083831
N-Nitroso-di-n-propylamine ND ug/kg 06/19/23 09:52 621-64-706/15/23 16:083831
N-Nitrosodiphenylamine ND ug/kg 06/19/23 09:52 86-30-606/15/23 16:083831
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/19/23 09:52 108-60-106/15/23 16:083831
Pentachlorophenol ND ug/kg 06/19/23 09:52 87-86-506/15/23 16:087651
Phenanthrene ND ug/kg 06/19/23 09:52 85-01-806/15/23 16:083831
Phenol ND ug/kg 06/19/23 09:52 108-95-206/15/23 16:083831
Pyrene ND ug/kg 06/19/23 09:52 129-00-006/15/23 16:083831
Pyridine ND ug/kg 06/19/23 09:52 110-86-106/15/23 16:083831
1,2,4-Trichlorobenzene ND ug/kg 06/19/23 09:52 120-82-106/15/23 16:083831
2,4,5-Trichlorophenol ND ug/kg 06/19/23 09:52 95-95-406/15/23 16:083831
2,4,6-Trichlorophenol ND ug/kg 06/19/23 09:52 88-06-206/15/23 16:083831
Surrogates
Nitrobenzene-d5 (S)45 %06/19/23 09:52 4165-60-006/15/23 16:0810-130 1
2-Fluorobiphenyl (S)47 %06/19/23 09:52 321-60-806/15/23 16:0810-130 1
Terphenyl-d14 (S)72 %06/19/23 09:52 1718-51-006/15/23 16:0810-130 1
Phenol-d6 (S)45 %06/19/23 09:52 13127-88-306/15/23 16:0810-130 1
2-Fluorophenol (S)42 %06/19/23 09:52 367-12-406/15/23 16:0810-130 1
2,4,6-Tribromophenol (S)58 %06/19/23 09:52 118-79-606/15/23 16:0810-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-A Lab ID:92672500005 Collected:06/13/23 14:00 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/19/23 18:13 67-64-106/19/23 14:002041
Benzene 13.2 ug/kg 06/19/23 18:13 71-43-206/19/23 14:0010.2 1
Bromobenzene ND ug/kg 06/19/23 18:13 108-86-106/19/23 14:0010.2 1
Bromochloromethane ND ug/kg 06/19/23 18:13 74-97-506/19/23 14:0010.2 1
Bromodichloromethane ND ug/kg 06/19/23 18:13 75-27-406/19/23 14:0010.2 1
Bromoform ND ug/kg 06/19/23 18:13 75-25-206/19/23 14:0010.2 1
Bromomethane ND ug/kg 06/19/23 18:13 74-83-906/19/23 14:0040.8 1
2-Butanone (MEK)ND ug/kg 06/19/23 18:13 78-93-306/19/23 14:002041
n-Butylbenzene ND ug/kg 06/19/23 18:13 104-51-806/19/23 14:0010.2 1
sec-Butylbenzene ND ug/kg 06/19/23 18:13 135-98-806/19/23 14:0010.2 1
tert-Butylbenzene ND ug/kg 06/19/23 18:13 98-06-606/19/23 14:0010.2 1
Carbon tetrachloride ND ug/kg 06/19/23 18:13 56-23-506/19/23 14:0010.2 1
Chlorobenzene ND ug/kg 06/19/23 18:13 108-90-706/19/23 14:0010.2 1
Chloroethane ND ug/kg 06/19/23 18:13 75-00-3 v106/19/23 14:0020.4 1
Chloroform ND ug/kg 06/19/23 18:13 67-66-306/19/23 14:0010.2 1
Chloromethane ND ug/kg 06/19/23 18:13 74-87-3 v106/19/23 14:0020.4 1
2-Chlorotoluene ND ug/kg 06/19/23 18:13 95-49-806/19/23 14:0010.2 1
4-Chlorotoluene ND ug/kg 06/19/23 18:13 106-43-406/19/23 14:0010.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/19/23 18:13 96-12-806/19/23 14:0010.2 1
Dibromochloromethane ND ug/kg 06/19/23 18:13 124-48-106/19/23 14:0010.2 1
1,2-Dibromoethane (EDB)ND ug/kg 06/19/23 18:13 106-93-406/19/23 14:0010.2 1
Dibromomethane ND ug/kg 06/19/23 18:13 74-95-306/19/23 14:0010.2 1
1,2-Dichlorobenzene ND ug/kg 06/19/23 18:13 95-50-106/19/23 14:0010.2 1
1,3-Dichlorobenzene ND ug/kg 06/19/23 18:13 541-73-106/19/23 14:0010.2 1
1,4-Dichlorobenzene ND ug/kg 06/19/23 18:13 106-46-706/19/23 14:0010.2 1
Dichlorodifluoromethane ND ug/kg 06/19/23 18:13 75-71-806/19/23 14:0020.4 1
1,1-Dichloroethane ND ug/kg 06/19/23 18:13 75-34-306/19/23 14:0010.2 1
1,2-Dichloroethane ND ug/kg 06/19/23 18:13 107-06-206/19/23 14:0010.2 1
1,1-Dichloroethene ND ug/kg 06/19/23 18:13 75-35-406/19/23 14:0010.2 1
cis-1,2-Dichloroethene ND ug/kg 06/19/23 18:13 156-59-206/19/23 14:0010.2 1
trans-1,2-Dichloroethene ND ug/kg 06/19/23 18:13 156-60-506/19/23 14:0010.2 1
1,2-Dichloropropane ND ug/kg 06/19/23 18:13 78-87-506/19/23 14:0010.2 1
1,3-Dichloropropane ND ug/kg 06/19/23 18:13 142-28-906/19/23 14:0010.2 1
2,2-Dichloropropane ND ug/kg 06/19/23 18:13 594-20-706/19/23 14:0010.2 1
1,1-Dichloropropene ND ug/kg 06/19/23 18:13 563-58-606/19/23 14:0010.2 1
cis-1,3-Dichloropropene ND ug/kg 06/19/23 18:13 10061-01-506/19/23 14:0010.2 1
trans-1,3-Dichloropropene ND ug/kg 06/19/23 18:13 10061-02-606/19/23 14:0010.2 1
Diisopropyl ether ND ug/kg 06/19/23 18:13 108-20-306/19/23 14:0010.2 1
Ethylbenzene ND ug/kg 06/19/23 18:13 100-41-406/19/23 14:0010.2 1
Hexachloro-1,3-butadiene ND ug/kg 06/19/23 18:13 87-68-306/19/23 14:0020.4 1
2-Hexanone ND ug/kg 06/19/23 18:13 591-78-606/19/23 14:001021
Isopropylbenzene (Cumene)ND ug/kg 06/19/23 18:13 98-82-806/19/23 14:0010.2 1
p-Isopropyltoluene ND ug/kg 06/19/23 18:13 99-87-606/19/23 14:0010.2 1
Methylene Chloride ND ug/kg 06/19/23 18:13 75-09-206/19/23 14:0040.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/19/23 18:13 108-10-106/19/23 14:001021
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-A Lab ID:92672500005 Collected:06/13/23 14:00 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/19/23 18:13 1634-04-406/19/23 14:0010.2 1
Naphthalene ND ug/kg 06/19/23 18:13 91-20-306/19/23 14:0010.2 1
n-Propylbenzene ND ug/kg 06/19/23 18:13 103-65-106/19/23 14:0010.2 1
Styrene ND ug/kg 06/19/23 18:13 100-42-506/19/23 14:0010.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/19/23 18:13 630-20-606/19/23 14:0010.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/19/23 18:13 79-34-506/19/23 14:0010.2 1
Tetrachloroethene ND ug/kg 06/19/23 18:13 127-18-406/19/23 14:0010.2 1
Toluene ND ug/kg 06/19/23 18:13 108-88-306/19/23 14:0010.2 1
1,2,3-Trichlorobenzene ND ug/kg 06/19/23 18:13 87-61-606/19/23 14:0010.2 1
1,2,4-Trichlorobenzene ND ug/kg 06/19/23 18:13 120-82-106/19/23 14:0010.2 1
1,1,1-Trichloroethane ND ug/kg 06/19/23 18:13 71-55-606/19/23 14:0010.2 1
1,1,2-Trichloroethane ND ug/kg 06/19/23 18:13 79-00-506/19/23 14:0010.2 1
Trichloroethene ND ug/kg 06/19/23 18:13 79-01-606/19/23 14:0010.2 1
Trichlorofluoromethane ND ug/kg 06/19/23 18:13 75-69-406/19/23 14:0010.2 1
1,2,3-Trichloropropane ND ug/kg 06/19/23 18:13 96-18-406/19/23 14:0010.2 1
1,2,4-Trimethylbenzene ND ug/kg 06/19/23 18:13 95-63-606/19/23 14:0010.2 1
1,3,5-Trimethylbenzene ND ug/kg 06/19/23 18:13 108-67-806/19/23 14:0010.2 1
Vinyl acetate ND ug/kg 06/19/23 18:13 108-05-406/19/23 14:001021
Vinyl chloride ND ug/kg 06/19/23 18:13 75-01-4 v106/19/23 14:0020.4 1
Xylene (Total)ND ug/kg 06/19/23 18:13 1330-20-706/19/23 14:0020.4 1
m&p-Xylene ND ug/kg 06/19/23 18:13 179601-23-106/19/23 14:0020.4 1
o-Xylene ND ug/kg 06/19/23 18:13 95-47-606/19/23 14:0010.2 1
Surrogates
Toluene-d8 (S)103 %06/19/23 18:13 2037-26-506/19/23 14:0070-130 1
4-Bromofluorobenzene (S)104 %06/19/23 18:13 460-00-406/19/23 14:0070-130 1
1,2-Dichloroethane-d4 (S)111 %06/19/23 18:13 17060-07-006/19/23 14:0070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.1 %06/15/23 14:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-B Lab ID:92672500006 Collected:06/13/23 14:15 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 06/19/23 14:28 N206/18/23 11:3011.5 1
Aliphatic (C19-C36)ND mg/kg 06/19/23 14:28 N206/18/23 11:3011.5 1
Aromatic (C11-C22)ND mg/kg 06/19/23 14:28 N206/18/23 11:3011.5 1
Surrogates
1-Chlorooctadecane (S)84 %06/19/23 14:28 3386-33-206/18/23 11:3040-140 1
o-Terphenyl (S)63 %06/19/23 14:28 84-15-106/18/23 11:3040-140 1
2-Fluorobiphenyl (S)83 %06/19/23 14:28 321-60-806/18/23 11:3040-140 1
2-Bromonaphthalene (S)84 %06/19/23 14:28 580-13-206/18/23 11:3040-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/19/23 10:20 83-32-906/15/23 16:083891
Acenaphthylene ND ug/kg 06/19/23 10:20 208-96-806/15/23 16:083891
Aniline ND ug/kg 06/19/23 10:20 62-53-306/15/23 16:083891
Anthracene ND ug/kg 06/19/23 10:20 120-12-706/15/23 16:083891
Benzo(a)anthracene ND ug/kg 06/19/23 10:20 56-55-306/15/23 16:083891
Benzo(a)pyrene ND ug/kg 06/19/23 10:20 50-32-806/15/23 16:083891
Benzo(b)fluoranthene ND ug/kg 06/19/23 10:20 205-99-206/15/23 16:083891
Benzo(g,h,i)perylene ND ug/kg 06/19/23 10:20 191-24-206/15/23 16:083891
Benzo(k)fluoranthene ND ug/kg 06/19/23 10:20 207-08-906/15/23 16:083891
Benzoic Acid ND ug/kg 06/19/23 10:20 65-85-006/15/23 16:0819401
Benzyl alcohol ND ug/kg 06/19/23 10:20 100-51-606/15/23 16:087781
4-Bromophenylphenyl ether ND ug/kg 06/19/23 10:20 101-55-306/15/23 16:083891
Butylbenzylphthalate ND ug/kg 06/19/23 10:20 85-68-706/15/23 16:083891
4-Chloro-3-methylphenol ND ug/kg 06/19/23 10:20 59-50-706/15/23 16:087781
4-Chloroaniline ND ug/kg 06/19/23 10:20 106-47-806/15/23 16:087781
bis(2-Chloroethoxy)methane ND ug/kg 06/19/23 10:20 111-91-106/15/23 16:083891
bis(2-Chloroethyl) ether ND ug/kg 06/19/23 10:20 111-44-406/15/23 16:083891
2-Chloronaphthalene ND ug/kg 06/19/23 10:20 91-58-706/15/23 16:083891
2-Chlorophenol ND ug/kg 06/19/23 10:20 95-57-806/15/23 16:083891
4-Chlorophenylphenyl ether ND ug/kg 06/19/23 10:20 7005-72-306/15/23 16:083891
Chrysene ND ug/kg 06/19/23 10:20 218-01-906/15/23 16:083891
Dibenz(a,h)anthracene ND ug/kg 06/19/23 10:20 53-70-306/15/23 16:083891
Dibenzofuran ND ug/kg 06/19/23 10:20 132-64-906/15/23 16:083891
1,2-Dichlorobenzene ND ug/kg 06/19/23 10:20 95-50-106/15/23 16:083891
1,3-Dichlorobenzene ND ug/kg 06/19/23 10:20 541-73-106/15/23 16:083891
1,4-Dichlorobenzene ND ug/kg 06/19/23 10:20 106-46-706/15/23 16:083891
3,3'-Dichlorobenzidine ND ug/kg 06/19/23 10:20 91-94-106/15/23 16:087781
2,4-Dichlorophenol ND ug/kg 06/19/23 10:20 120-83-206/15/23 16:083891
Diethylphthalate ND ug/kg 06/19/23 10:20 84-66-206/15/23 16:083891
2,4-Dimethylphenol ND ug/kg 06/19/23 10:20 105-67-906/15/23 16:083891
Dimethylphthalate ND ug/kg 06/19/23 10:20 131-11-306/15/23 16:083891
Di-n-butylphthalate ND ug/kg 06/19/23 10:20 84-74-206/15/23 16:083891
4,6-Dinitro-2-methylphenol ND ug/kg 06/19/23 10:20 534-52-106/15/23 16:087781
2,4-Dinitrophenol ND ug/kg 06/19/23 10:20 51-28-506/15/23 16:0819401
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-B Lab ID:92672500006 Collected:06/13/23 14:15 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 06/19/23 10:20 121-14-206/15/23 16:083891
2,6-Dinitrotoluene ND ug/kg 06/19/23 10:20 606-20-206/15/23 16:083891
Di-n-octylphthalate ND ug/kg 06/19/23 10:20 117-84-006/15/23 16:083891
bis(2-Ethylhexyl)phthalate ND ug/kg 06/19/23 10:20 117-81-706/15/23 16:083891
Fluoranthene ND ug/kg 06/19/23 10:20 206-44-006/15/23 16:083891
Fluorene ND ug/kg 06/19/23 10:20 86-73-706/15/23 16:083891
Hexachloro-1,3-butadiene ND ug/kg 06/19/23 10:20 87-68-306/15/23 16:083891
Hexachlorobenzene ND ug/kg 06/19/23 10:20 118-74-106/15/23 16:083891
Hexachlorocyclopentadiene ND ug/kg 06/19/23 10:20 77-47-4 v206/15/23 16:083891
Hexachloroethane ND ug/kg 06/19/23 10:20 67-72-106/15/23 16:083891
Indeno(1,2,3-cd)pyrene ND ug/kg 06/19/23 10:20 193-39-506/15/23 16:083891
Isophorone ND ug/kg 06/19/23 10:20 78-59-106/15/23 16:083891
1-Methylnaphthalene ND ug/kg 06/19/23 10:20 90-12-006/15/23 16:083891
2-Methylnaphthalene ND ug/kg 06/19/23 10:20 91-57-606/15/23 16:083891
2-Methylphenol(o-Cresol)ND ug/kg 06/19/23 10:20 95-48-706/15/23 16:083891
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/19/23 10:20 15831-10-406/15/23 16:083891
Naphthalene ND ug/kg 06/19/23 10:20 91-20-306/15/23 16:083891
2-Nitroaniline ND ug/kg 06/19/23 10:20 88-74-406/15/23 16:0819401
3-Nitroaniline ND ug/kg 06/19/23 10:20 99-09-206/15/23 16:0819401
4-Nitroaniline ND ug/kg 06/19/23 10:20 100-01-606/15/23 16:087781
Nitrobenzene ND ug/kg 06/19/23 10:20 98-95-306/15/23 16:083891
2-Nitrophenol ND ug/kg 06/19/23 10:20 88-75-506/15/23 16:083891
4-Nitrophenol ND ug/kg 06/19/23 10:20 100-02-706/15/23 16:0819401
N-Nitrosodimethylamine ND ug/kg 06/19/23 10:20 62-75-906/15/23 16:083891
N-Nitroso-di-n-propylamine ND ug/kg 06/19/23 10:20 621-64-706/15/23 16:083891
N-Nitrosodiphenylamine ND ug/kg 06/19/23 10:20 86-30-606/15/23 16:083891
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/19/23 10:20 108-60-106/15/23 16:083891
Pentachlorophenol ND ug/kg 06/19/23 10:20 87-86-506/15/23 16:087781
Phenanthrene ND ug/kg 06/19/23 10:20 85-01-806/15/23 16:083891
Phenol ND ug/kg 06/19/23 10:20 108-95-206/15/23 16:083891
Pyrene ND ug/kg 06/19/23 10:20 129-00-006/15/23 16:083891
Pyridine ND ug/kg 06/19/23 10:20 110-86-106/15/23 16:083891
1,2,4-Trichlorobenzene ND ug/kg 06/19/23 10:20 120-82-106/15/23 16:083891
2,4,5-Trichlorophenol ND ug/kg 06/19/23 10:20 95-95-406/15/23 16:083891
2,4,6-Trichlorophenol ND ug/kg 06/19/23 10:20 88-06-206/15/23 16:083891
Surrogates
Nitrobenzene-d5 (S)59 %06/19/23 10:20 4165-60-006/15/23 16:0810-130 1
2-Fluorobiphenyl (S)61 %06/19/23 10:20 321-60-806/15/23 16:0810-130 1
Terphenyl-d14 (S)88 %06/19/23 10:20 1718-51-006/15/23 16:0810-130 1
Phenol-d6 (S)57 %06/19/23 10:20 13127-88-306/15/23 16:0810-130 1
2-Fluorophenol (S)53 %06/19/23 10:20 367-12-406/15/23 16:0810-130 1
2,4,6-Tribromophenol (S)72 %06/19/23 10:20 118-79-606/15/23 16:0810-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-B Lab ID:92672500006 Collected:06/13/23 14:15 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/19/23 18:32 67-64-106/19/23 14:001781
Benzene 11.3 ug/kg 06/19/23 18:32 71-43-206/19/23 14:008.9 1
Bromobenzene ND ug/kg 06/19/23 18:32 108-86-106/19/23 14:008.9 1
Bromochloromethane ND ug/kg 06/19/23 18:32 74-97-506/19/23 14:008.9 1
Bromodichloromethane ND ug/kg 06/19/23 18:32 75-27-406/19/23 14:008.9 1
Bromoform ND ug/kg 06/19/23 18:32 75-25-206/19/23 14:008.9 1
Bromomethane ND ug/kg 06/19/23 18:32 74-83-906/19/23 14:0035.6 1
2-Butanone (MEK)ND ug/kg 06/19/23 18:32 78-93-306/19/23 14:001781
n-Butylbenzene ND ug/kg 06/19/23 18:32 104-51-806/19/23 14:008.9 1
sec-Butylbenzene ND ug/kg 06/19/23 18:32 135-98-806/19/23 14:008.9 1
tert-Butylbenzene ND ug/kg 06/19/23 18:32 98-06-606/19/23 14:008.9 1
Carbon tetrachloride ND ug/kg 06/19/23 18:32 56-23-506/19/23 14:008.9 1
Chlorobenzene ND ug/kg 06/19/23 18:32 108-90-706/19/23 14:008.9 1
Chloroethane ND ug/kg 06/19/23 18:32 75-00-3 v106/19/23 14:0017.8 1
Chloroform ND ug/kg 06/19/23 18:32 67-66-306/19/23 14:008.9 1
Chloromethane ND ug/kg 06/19/23 18:32 74-87-3 v106/19/23 14:0017.8 1
2-Chlorotoluene ND ug/kg 06/19/23 18:32 95-49-806/19/23 14:008.9 1
4-Chlorotoluene ND ug/kg 06/19/23 18:32 106-43-406/19/23 14:008.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/19/23 18:32 96-12-806/19/23 14:008.9 1
Dibromochloromethane ND ug/kg 06/19/23 18:32 124-48-106/19/23 14:008.9 1
1,2-Dibromoethane (EDB)ND ug/kg 06/19/23 18:32 106-93-406/19/23 14:008.9 1
Dibromomethane ND ug/kg 06/19/23 18:32 74-95-306/19/23 14:008.9 1
1,2-Dichlorobenzene ND ug/kg 06/19/23 18:32 95-50-106/19/23 14:008.9 1
1,3-Dichlorobenzene ND ug/kg 06/19/23 18:32 541-73-106/19/23 14:008.9 1
1,4-Dichlorobenzene ND ug/kg 06/19/23 18:32 106-46-706/19/23 14:008.9 1
Dichlorodifluoromethane ND ug/kg 06/19/23 18:32 75-71-806/19/23 14:0017.8 1
1,1-Dichloroethane ND ug/kg 06/19/23 18:32 75-34-306/19/23 14:008.9 1
1,2-Dichloroethane ND ug/kg 06/19/23 18:32 107-06-206/19/23 14:008.9 1
1,1-Dichloroethene ND ug/kg 06/19/23 18:32 75-35-406/19/23 14:008.9 1
cis-1,2-Dichloroethene ND ug/kg 06/19/23 18:32 156-59-206/19/23 14:008.9 1
trans-1,2-Dichloroethene ND ug/kg 06/19/23 18:32 156-60-506/19/23 14:008.9 1
1,2-Dichloropropane ND ug/kg 06/19/23 18:32 78-87-506/19/23 14:008.9 1
1,3-Dichloropropane ND ug/kg 06/19/23 18:32 142-28-906/19/23 14:008.9 1
2,2-Dichloropropane ND ug/kg 06/19/23 18:32 594-20-706/19/23 14:008.9 1
1,1-Dichloropropene ND ug/kg 06/19/23 18:32 563-58-606/19/23 14:008.9 1
cis-1,3-Dichloropropene ND ug/kg 06/19/23 18:32 10061-01-506/19/23 14:008.9 1
trans-1,3-Dichloropropene ND ug/kg 06/19/23 18:32 10061-02-606/19/23 14:008.9 1
Diisopropyl ether ND ug/kg 06/19/23 18:32 108-20-306/19/23 14:008.9 1
Ethylbenzene ND ug/kg 06/19/23 18:32 100-41-406/19/23 14:008.9 1
Hexachloro-1,3-butadiene ND ug/kg 06/19/23 18:32 87-68-306/19/23 14:0017.8 1
2-Hexanone ND ug/kg 06/19/23 18:32 591-78-606/19/23 14:0089.0 1
Isopropylbenzene (Cumene)ND ug/kg 06/19/23 18:32 98-82-806/19/23 14:008.9 1
p-Isopropyltoluene 26.5 ug/kg 06/19/23 18:32 99-87-606/19/23 14:008.9 1
Methylene Chloride ND ug/kg 06/19/23 18:32 75-09-206/19/23 14:0035.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/19/23 18:32 108-10-106/19/23 14:0089.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-B Lab ID:92672500006 Collected:06/13/23 14:15 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/19/23 18:32 1634-04-406/19/23 14:008.9 1
Naphthalene 53.8 ug/kg 06/19/23 18:32 91-20-306/19/23 14:008.9 1
n-Propylbenzene ND ug/kg 06/19/23 18:32 103-65-106/19/23 14:008.9 1
Styrene ND ug/kg 06/19/23 18:32 100-42-506/19/23 14:008.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/19/23 18:32 630-20-606/19/23 14:008.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/19/23 18:32 79-34-506/19/23 14:008.9 1
Tetrachloroethene ND ug/kg 06/19/23 18:32 127-18-406/19/23 14:008.9 1
Toluene ND ug/kg 06/19/23 18:32 108-88-306/19/23 14:008.9 1
1,2,3-Trichlorobenzene ND ug/kg 06/19/23 18:32 87-61-606/19/23 14:008.9 1
1,2,4-Trichlorobenzene ND ug/kg 06/19/23 18:32 120-82-106/19/23 14:008.9 1
1,1,1-Trichloroethane ND ug/kg 06/19/23 18:32 71-55-606/19/23 14:008.9 1
1,1,2-Trichloroethane ND ug/kg 06/19/23 18:32 79-00-506/19/23 14:008.9 1
Trichloroethene ND ug/kg 06/19/23 18:32 79-01-606/19/23 14:008.9 1
Trichlorofluoromethane ND ug/kg 06/19/23 18:32 75-69-406/19/23 14:008.9 1
1,2,3-Trichloropropane ND ug/kg 06/19/23 18:32 96-18-406/19/23 14:008.9 1
1,2,4-Trimethylbenzene 163 ug/kg 06/19/23 18:32 95-63-606/19/23 14:008.9 1
1,3,5-Trimethylbenzene 57.3 ug/kg 06/19/23 18:32 108-67-806/19/23 14:008.9 1
Vinyl acetate ND ug/kg 06/19/23 18:32 108-05-406/19/23 14:0089.0 1
Vinyl chloride ND ug/kg 06/19/23 18:32 75-01-4 v106/19/23 14:0017.8 1
Xylene (Total)35.1 ug/kg 06/19/23 18:32 1330-20-706/19/23 14:0017.8 1
m&p-Xylene 21.7 ug/kg 06/19/23 18:32 179601-23-106/19/23 14:0017.8 1
o-Xylene 13.4 ug/kg 06/19/23 18:32 95-47-606/19/23 14:008.9 1
Surrogates
Toluene-d8 (S)104 %06/19/23 18:32 2037-26-506/19/23 14:0070-130 1
4-Bromofluorobenzene (S)104 %06/19/23 18:32 460-00-406/19/23 14:0070-130 1
1,2-Dichloroethane-d4 (S)107 %06/19/23 18:32 17060-07-006/19/23 14:0070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.3 %06/15/23 15:23 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-C Lab ID:92672500007 Collected:06/13/23 14:30 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)20.9 mg/kg 06/19/23 14:53 N206/18/23 11:3013.1 1
Aliphatic (C19-C36)ND mg/kg 06/19/23 14:53 N206/18/23 11:3013.1 1
Aromatic (C11-C22)ND mg/kg 06/19/23 14:53 N206/18/23 11:3013.1 1
Surrogates
1-Chlorooctadecane (S)94 %06/19/23 14:53 3386-33-206/18/23 11:3040-140 1
o-Terphenyl (S)65 %06/19/23 14:53 84-15-106/18/23 11:3040-140 1
2-Fluorobiphenyl (S)85 %06/19/23 14:53 321-60-806/18/23 11:3040-140 1
2-Bromonaphthalene (S)94 %06/19/23 14:53 580-13-206/18/23 11:3040-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/19/23 10:48 83-32-906/15/23 16:084391
Acenaphthylene ND ug/kg 06/19/23 10:48 208-96-806/15/23 16:084391
Aniline ND ug/kg 06/19/23 10:48 62-53-306/15/23 16:084391
Anthracene ND ug/kg 06/19/23 10:48 120-12-706/15/23 16:084391
Benzo(a)anthracene ND ug/kg 06/19/23 10:48 56-55-306/15/23 16:084391
Benzo(a)pyrene ND ug/kg 06/19/23 10:48 50-32-806/15/23 16:084391
Benzo(b)fluoranthene ND ug/kg 06/19/23 10:48 205-99-206/15/23 16:084391
Benzo(g,h,i)perylene ND ug/kg 06/19/23 10:48 191-24-206/15/23 16:084391
Benzo(k)fluoranthene ND ug/kg 06/19/23 10:48 207-08-906/15/23 16:084391
Benzoic Acid ND ug/kg 06/19/23 10:48 65-85-006/15/23 16:0822001
Benzyl alcohol ND ug/kg 06/19/23 10:48 100-51-606/15/23 16:088781
4-Bromophenylphenyl ether ND ug/kg 06/19/23 10:48 101-55-306/15/23 16:084391
Butylbenzylphthalate ND ug/kg 06/19/23 10:48 85-68-706/15/23 16:084391
4-Chloro-3-methylphenol ND ug/kg 06/19/23 10:48 59-50-706/15/23 16:088781
4-Chloroaniline ND ug/kg 06/19/23 10:48 106-47-806/15/23 16:088781
bis(2-Chloroethoxy)methane ND ug/kg 06/19/23 10:48 111-91-106/15/23 16:084391
bis(2-Chloroethyl) ether ND ug/kg 06/19/23 10:48 111-44-406/15/23 16:084391
2-Chloronaphthalene ND ug/kg 06/19/23 10:48 91-58-706/15/23 16:084391
2-Chlorophenol ND ug/kg 06/19/23 10:48 95-57-806/15/23 16:084391
4-Chlorophenylphenyl ether ND ug/kg 06/19/23 10:48 7005-72-306/15/23 16:084391
Chrysene ND ug/kg 06/19/23 10:48 218-01-906/15/23 16:084391
Dibenz(a,h)anthracene ND ug/kg 06/19/23 10:48 53-70-306/15/23 16:084391
Dibenzofuran ND ug/kg 06/19/23 10:48 132-64-906/15/23 16:084391
1,2-Dichlorobenzene ND ug/kg 06/19/23 10:48 95-50-106/15/23 16:084391
1,3-Dichlorobenzene ND ug/kg 06/19/23 10:48 541-73-106/15/23 16:084391
1,4-Dichlorobenzene ND ug/kg 06/19/23 10:48 106-46-706/15/23 16:084391
3,3'-Dichlorobenzidine ND ug/kg 06/19/23 10:48 91-94-106/15/23 16:088781
2,4-Dichlorophenol ND ug/kg 06/19/23 10:48 120-83-206/15/23 16:084391
Diethylphthalate ND ug/kg 06/19/23 10:48 84-66-206/15/23 16:084391
2,4-Dimethylphenol ND ug/kg 06/19/23 10:48 105-67-906/15/23 16:084391
Dimethylphthalate ND ug/kg 06/19/23 10:48 131-11-306/15/23 16:084391
Di-n-butylphthalate ND ug/kg 06/19/23 10:48 84-74-206/15/23 16:084391
4,6-Dinitro-2-methylphenol ND ug/kg 06/19/23 10:48 534-52-106/15/23 16:088781
2,4-Dinitrophenol ND ug/kg 06/19/23 10:48 51-28-506/15/23 16:0822001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-C Lab ID:92672500007 Collected:06/13/23 14:30 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 06/19/23 10:48 121-14-206/15/23 16:084391
2,6-Dinitrotoluene ND ug/kg 06/19/23 10:48 606-20-206/15/23 16:084391
Di-n-octylphthalate ND ug/kg 06/19/23 10:48 117-84-006/15/23 16:084391
bis(2-Ethylhexyl)phthalate ND ug/kg 06/19/23 10:48 117-81-706/15/23 16:084391
Fluoranthene ND ug/kg 06/19/23 10:48 206-44-006/15/23 16:084391
Fluorene ND ug/kg 06/19/23 10:48 86-73-706/15/23 16:084391
Hexachloro-1,3-butadiene ND ug/kg 06/19/23 10:48 87-68-306/15/23 16:084391
Hexachlorobenzene ND ug/kg 06/19/23 10:48 118-74-106/15/23 16:084391
Hexachlorocyclopentadiene ND ug/kg 06/19/23 10:48 77-47-4 v206/15/23 16:084391
Hexachloroethane ND ug/kg 06/19/23 10:48 67-72-106/15/23 16:084391
Indeno(1,2,3-cd)pyrene ND ug/kg 06/19/23 10:48 193-39-506/15/23 16:084391
Isophorone ND ug/kg 06/19/23 10:48 78-59-106/15/23 16:084391
1-Methylnaphthalene ND ug/kg 06/19/23 10:48 90-12-006/15/23 16:084391
2-Methylnaphthalene ND ug/kg 06/19/23 10:48 91-57-606/15/23 16:084391
2-Methylphenol(o-Cresol)ND ug/kg 06/19/23 10:48 95-48-706/15/23 16:084391
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/19/23 10:48 15831-10-406/15/23 16:084391
Naphthalene ND ug/kg 06/19/23 10:48 91-20-306/15/23 16:084391
2-Nitroaniline ND ug/kg 06/19/23 10:48 88-74-406/15/23 16:0822001
3-Nitroaniline ND ug/kg 06/19/23 10:48 99-09-206/15/23 16:0822001
4-Nitroaniline ND ug/kg 06/19/23 10:48 100-01-606/15/23 16:088781
Nitrobenzene ND ug/kg 06/19/23 10:48 98-95-306/15/23 16:084391
2-Nitrophenol ND ug/kg 06/19/23 10:48 88-75-506/15/23 16:084391
4-Nitrophenol ND ug/kg 06/19/23 10:48 100-02-706/15/23 16:0822001
N-Nitrosodimethylamine ND ug/kg 06/19/23 10:48 62-75-906/15/23 16:084391
N-Nitroso-di-n-propylamine ND ug/kg 06/19/23 10:48 621-64-706/15/23 16:084391
N-Nitrosodiphenylamine ND ug/kg 06/19/23 10:48 86-30-606/15/23 16:084391
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/19/23 10:48 108-60-106/15/23 16:084391
Pentachlorophenol ND ug/kg 06/19/23 10:48 87-86-506/15/23 16:088781
Phenanthrene ND ug/kg 06/19/23 10:48 85-01-806/15/23 16:084391
Phenol ND ug/kg 06/19/23 10:48 108-95-206/15/23 16:084391
Pyrene ND ug/kg 06/19/23 10:48 129-00-006/15/23 16:084391
Pyridine ND ug/kg 06/19/23 10:48 110-86-106/15/23 16:084391
1,2,4-Trichlorobenzene ND ug/kg 06/19/23 10:48 120-82-106/15/23 16:084391
2,4,5-Trichlorophenol ND ug/kg 06/19/23 10:48 95-95-406/15/23 16:084391
2,4,6-Trichlorophenol ND ug/kg 06/19/23 10:48 88-06-206/15/23 16:084391
Surrogates
Nitrobenzene-d5 (S)39 %06/19/23 10:48 4165-60-006/15/23 16:0810-130 1
2-Fluorobiphenyl (S)40 %06/19/23 10:48 321-60-806/15/23 16:0810-130 1
Terphenyl-d14 (S)78 %06/19/23 10:48 1718-51-006/15/23 16:0810-130 1
Phenol-d6 (S)34 %06/19/23 10:48 13127-88-306/15/23 16:0810-130 1
2-Fluorophenol (S)31 %06/19/23 10:48 367-12-406/15/23 16:0810-130 1
2,4,6-Tribromophenol (S)56 %06/19/23 10:48 118-79-606/15/23 16:0810-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-C Lab ID:92672500007 Collected:06/13/23 14:30 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/19/23 18:50 67-64-106/19/23 14:002461
Benzene 12.5 ug/kg 06/19/23 18:50 71-43-206/19/23 14:0012.3 1
Bromobenzene ND ug/kg 06/19/23 18:50 108-86-106/19/23 14:0012.3 1
Bromochloromethane ND ug/kg 06/19/23 18:50 74-97-506/19/23 14:0012.3 1
Bromodichloromethane ND ug/kg 06/19/23 18:50 75-27-406/19/23 14:0012.3 1
Bromoform ND ug/kg 06/19/23 18:50 75-25-206/19/23 14:0012.3 1
Bromomethane ND ug/kg 06/19/23 18:50 74-83-906/19/23 14:0049.3 1
2-Butanone (MEK)ND ug/kg 06/19/23 18:50 78-93-306/19/23 14:002461
n-Butylbenzene ND ug/kg 06/19/23 18:50 104-51-806/19/23 14:0012.3 1
sec-Butylbenzene ND ug/kg 06/19/23 18:50 135-98-806/19/23 14:0012.3 1
tert-Butylbenzene ND ug/kg 06/19/23 18:50 98-06-606/19/23 14:0012.3 1
Carbon tetrachloride ND ug/kg 06/19/23 18:50 56-23-506/19/23 14:0012.3 1
Chlorobenzene ND ug/kg 06/19/23 18:50 108-90-706/19/23 14:0012.3 1
Chloroethane ND ug/kg 06/19/23 18:50 75-00-3 v106/19/23 14:0024.6 1
Chloroform ND ug/kg 06/19/23 18:50 67-66-306/19/23 14:0012.3 1
Chloromethane ND ug/kg 06/19/23 18:50 74-87-3 v106/19/23 14:0024.6 1
2-Chlorotoluene ND ug/kg 06/19/23 18:50 95-49-806/19/23 14:0012.3 1
4-Chlorotoluene ND ug/kg 06/19/23 18:50 106-43-406/19/23 14:0012.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/19/23 18:50 96-12-806/19/23 14:0012.3 1
Dibromochloromethane ND ug/kg 06/19/23 18:50 124-48-106/19/23 14:0012.3 1
1,2-Dibromoethane (EDB)ND ug/kg 06/19/23 18:50 106-93-406/19/23 14:0012.3 1
Dibromomethane ND ug/kg 06/19/23 18:50 74-95-306/19/23 14:0012.3 1
1,2-Dichlorobenzene ND ug/kg 06/19/23 18:50 95-50-106/19/23 14:0012.3 1
1,3-Dichlorobenzene ND ug/kg 06/19/23 18:50 541-73-106/19/23 14:0012.3 1
1,4-Dichlorobenzene ND ug/kg 06/19/23 18:50 106-46-706/19/23 14:0012.3 1
Dichlorodifluoromethane ND ug/kg 06/19/23 18:50 75-71-806/19/23 14:0024.6 1
1,1-Dichloroethane ND ug/kg 06/19/23 18:50 75-34-306/19/23 14:0012.3 1
1,2-Dichloroethane ND ug/kg 06/19/23 18:50 107-06-206/19/23 14:0012.3 1
1,1-Dichloroethene ND ug/kg 06/19/23 18:50 75-35-406/19/23 14:0012.3 1
cis-1,2-Dichloroethene ND ug/kg 06/19/23 18:50 156-59-206/19/23 14:0012.3 1
trans-1,2-Dichloroethene ND ug/kg 06/19/23 18:50 156-60-506/19/23 14:0012.3 1
1,2-Dichloropropane ND ug/kg 06/19/23 18:50 78-87-506/19/23 14:0012.3 1
1,3-Dichloropropane ND ug/kg 06/19/23 18:50 142-28-906/19/23 14:0012.3 1
2,2-Dichloropropane ND ug/kg 06/19/23 18:50 594-20-706/19/23 14:0012.3 1
1,1-Dichloropropene ND ug/kg 06/19/23 18:50 563-58-606/19/23 14:0012.3 1
cis-1,3-Dichloropropene ND ug/kg 06/19/23 18:50 10061-01-506/19/23 14:0012.3 1
trans-1,3-Dichloropropene ND ug/kg 06/19/23 18:50 10061-02-606/19/23 14:0012.3 1
Diisopropyl ether ND ug/kg 06/19/23 18:50 108-20-306/19/23 14:0012.3 1
Ethylbenzene ND ug/kg 06/19/23 18:50 100-41-406/19/23 14:0012.3 1
Hexachloro-1,3-butadiene ND ug/kg 06/19/23 18:50 87-68-306/19/23 14:0024.6 1
2-Hexanone ND ug/kg 06/19/23 18:50 591-78-606/19/23 14:001231
Isopropylbenzene (Cumene)ND ug/kg 06/19/23 18:50 98-82-806/19/23 14:0012.3 1
p-Isopropyltoluene ND ug/kg 06/19/23 18:50 99-87-606/19/23 14:0012.3 1
Methylene Chloride ND ug/kg 06/19/23 18:50 75-09-206/19/23 14:0049.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/19/23 18:50 108-10-106/19/23 14:001231
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-C Lab ID:92672500007 Collected:06/13/23 14:30 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/19/23 18:50 1634-04-406/19/23 14:0012.3 1
Naphthalene ND ug/kg 06/19/23 18:50 91-20-306/19/23 14:0012.3 1
n-Propylbenzene ND ug/kg 06/19/23 18:50 103-65-106/19/23 14:0012.3 1
Styrene ND ug/kg 06/19/23 18:50 100-42-506/19/23 14:0012.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/19/23 18:50 630-20-606/19/23 14:0012.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/19/23 18:50 79-34-506/19/23 14:0012.3 1
Tetrachloroethene ND ug/kg 06/19/23 18:50 127-18-406/19/23 14:0012.3 1
Toluene ND ug/kg 06/19/23 18:50 108-88-306/19/23 14:0012.3 1
1,2,3-Trichlorobenzene ND ug/kg 06/19/23 18:50 87-61-606/19/23 14:0012.3 1
1,2,4-Trichlorobenzene ND ug/kg 06/19/23 18:50 120-82-106/19/23 14:0012.3 1
1,1,1-Trichloroethane ND ug/kg 06/19/23 18:50 71-55-606/19/23 14:0012.3 1
1,1,2-Trichloroethane ND ug/kg 06/19/23 18:50 79-00-506/19/23 14:0012.3 1
Trichloroethene ND ug/kg 06/19/23 18:50 79-01-606/19/23 14:0012.3 1
Trichlorofluoromethane ND ug/kg 06/19/23 18:50 75-69-406/19/23 14:0012.3 1
1,2,3-Trichloropropane ND ug/kg 06/19/23 18:50 96-18-406/19/23 14:0012.3 1
1,2,4-Trimethylbenzene 20.4 ug/kg 06/19/23 18:50 95-63-606/19/23 14:0012.3 1
1,3,5-Trimethylbenzene ND ug/kg 06/19/23 18:50 108-67-806/19/23 14:0012.3 1
Vinyl acetate ND ug/kg 06/19/23 18:50 108-05-406/19/23 14:001231
Vinyl chloride ND ug/kg 06/19/23 18:50 75-01-4 v106/19/23 14:0024.6 1
Xylene (Total)ND ug/kg 06/19/23 18:50 1330-20-706/19/23 14:0024.6 1
m&p-Xylene ND ug/kg 06/19/23 18:50 179601-23-106/19/23 14:0024.6 1
o-Xylene ND ug/kg 06/19/23 18:50 95-47-606/19/23 14:0012.3 1
Surrogates
Toluene-d8 (S)102 %06/19/23 18:50 2037-26-506/19/23 14:0070-130 1
4-Bromofluorobenzene (S)104 %06/19/23 18:50 460-00-406/19/23 14:0070-130 1
1,2-Dichloroethane-d4 (S)110 %06/19/23 18:50 17060-07-006/19/23 14:0070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.6 %06/15/23 15:23 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D Lab ID:92672500008 Collected:06/13/23 14:40 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)152 mg/kg 06/20/23 16:01 N206/18/23 11:3025.8 2
Aliphatic (C19-C36)57.9 mg/kg 06/20/23 16:01 N206/18/23 11:3025.8 2
Aromatic (C11-C22)54.7 mg/kg 06/19/23 15:19 N206/18/23 11:3012.9 1
Surrogates
1-Chlorooctadecane (S)171 %06/20/23 16:01 3386-33-2 S506/18/23 11:3040-140 2
o-Terphenyl (S)106 %06/19/23 15:19 84-15-106/18/23 11:3040-140 1
2-Fluorobiphenyl (S)96 %06/19/23 15:19 321-60-806/18/23 11:3040-140 1
2-Bromonaphthalene (S)141 %06/19/23 15:19 580-13-2 S506/18/23 11:3040-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/19/23 11:16 83-32-906/15/23 16:084241
Acenaphthylene ND ug/kg 06/19/23 11:16 208-96-806/15/23 16:084241
Aniline ND ug/kg 06/19/23 11:16 62-53-306/15/23 16:084241
Anthracene ND ug/kg 06/19/23 11:16 120-12-706/15/23 16:084241
Benzo(a)anthracene ND ug/kg 06/19/23 11:16 56-55-306/15/23 16:084241
Benzo(a)pyrene ND ug/kg 06/19/23 11:16 50-32-806/15/23 16:084241
Benzo(b)fluoranthene ND ug/kg 06/19/23 11:16 205-99-206/15/23 16:084241
Benzo(g,h,i)perylene ND ug/kg 06/19/23 11:16 191-24-206/15/23 16:084241
Benzo(k)fluoranthene ND ug/kg 06/19/23 11:16 207-08-906/15/23 16:084241
Benzoic Acid ND ug/kg 06/19/23 11:16 65-85-006/15/23 16:0821201
Benzyl alcohol ND ug/kg 06/19/23 11:16 100-51-606/15/23 16:088471
4-Bromophenylphenyl ether ND ug/kg 06/19/23 11:16 101-55-306/15/23 16:084241
Butylbenzylphthalate ND ug/kg 06/19/23 11:16 85-68-706/15/23 16:084241
4-Chloro-3-methylphenol ND ug/kg 06/19/23 11:16 59-50-706/15/23 16:088471
4-Chloroaniline ND ug/kg 06/19/23 11:16 106-47-806/15/23 16:088471
bis(2-Chloroethoxy)methane ND ug/kg 06/19/23 11:16 111-91-106/15/23 16:084241
bis(2-Chloroethyl) ether ND ug/kg 06/19/23 11:16 111-44-406/15/23 16:084241
2-Chloronaphthalene ND ug/kg 06/19/23 11:16 91-58-706/15/23 16:084241
2-Chlorophenol ND ug/kg 06/19/23 11:16 95-57-806/15/23 16:084241
4-Chlorophenylphenyl ether ND ug/kg 06/19/23 11:16 7005-72-306/15/23 16:084241
Chrysene ND ug/kg 06/19/23 11:16 218-01-906/15/23 16:084241
Dibenz(a,h)anthracene ND ug/kg 06/19/23 11:16 53-70-306/15/23 16:084241
Dibenzofuran ND ug/kg 06/19/23 11:16 132-64-906/15/23 16:084241
1,2-Dichlorobenzene ND ug/kg 06/19/23 11:16 95-50-106/15/23 16:084241
1,3-Dichlorobenzene ND ug/kg 06/19/23 11:16 541-73-106/15/23 16:084241
1,4-Dichlorobenzene ND ug/kg 06/19/23 11:16 106-46-706/15/23 16:084241
3,3'-Dichlorobenzidine ND ug/kg 06/19/23 11:16 91-94-106/15/23 16:088471
2,4-Dichlorophenol ND ug/kg 06/19/23 11:16 120-83-206/15/23 16:084241
Diethylphthalate ND ug/kg 06/19/23 11:16 84-66-206/15/23 16:084241
2,4-Dimethylphenol ND ug/kg 06/19/23 11:16 105-67-906/15/23 16:084241
Dimethylphthalate ND ug/kg 06/19/23 11:16 131-11-306/15/23 16:084241
Di-n-butylphthalate ND ug/kg 06/19/23 11:16 84-74-206/15/23 16:084241
4,6-Dinitro-2-methylphenol ND ug/kg 06/19/23 11:16 534-52-106/15/23 16:088471
2,4-Dinitrophenol ND ug/kg 06/19/23 11:16 51-28-506/15/23 16:0821201
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D Lab ID:92672500008 Collected:06/13/23 14:40 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 06/19/23 11:16 121-14-206/15/23 16:084241
2,6-Dinitrotoluene ND ug/kg 06/19/23 11:16 606-20-206/15/23 16:084241
Di-n-octylphthalate ND ug/kg 06/19/23 11:16 117-84-006/15/23 16:084241
bis(2-Ethylhexyl)phthalate ND ug/kg 06/19/23 11:16 117-81-706/15/23 16:084241
Fluoranthene ND ug/kg 06/19/23 11:16 206-44-006/15/23 16:084241
Fluorene ND ug/kg 06/19/23 11:16 86-73-706/15/23 16:084241
Hexachloro-1,3-butadiene ND ug/kg 06/19/23 11:16 87-68-306/15/23 16:084241
Hexachlorobenzene ND ug/kg 06/19/23 11:16 118-74-106/15/23 16:084241
Hexachlorocyclopentadiene ND ug/kg 06/19/23 11:16 77-47-4 v206/15/23 16:084241
Hexachloroethane ND ug/kg 06/19/23 11:16 67-72-106/15/23 16:084241
Indeno(1,2,3-cd)pyrene ND ug/kg 06/19/23 11:16 193-39-506/15/23 16:084241
Isophorone ND ug/kg 06/19/23 11:16 78-59-106/15/23 16:084241
1-Methylnaphthalene ND ug/kg 06/19/23 11:16 90-12-006/15/23 16:084241
2-Methylnaphthalene ND ug/kg 06/19/23 11:16 91-57-606/15/23 16:084241
2-Methylphenol(o-Cresol)ND ug/kg 06/19/23 11:16 95-48-706/15/23 16:084241
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/19/23 11:16 15831-10-406/15/23 16:084241
Naphthalene ND ug/kg 06/19/23 11:16 91-20-306/15/23 16:084241
2-Nitroaniline ND ug/kg 06/19/23 11:16 88-74-406/15/23 16:0821201
3-Nitroaniline ND ug/kg 06/19/23 11:16 99-09-206/15/23 16:0821201
4-Nitroaniline ND ug/kg 06/19/23 11:16 100-01-606/15/23 16:088471
Nitrobenzene ND ug/kg 06/19/23 11:16 98-95-306/15/23 16:084241
2-Nitrophenol ND ug/kg 06/19/23 11:16 88-75-506/15/23 16:084241
4-Nitrophenol ND ug/kg 06/19/23 11:16 100-02-706/15/23 16:0821201
N-Nitrosodimethylamine ND ug/kg 06/19/23 11:16 62-75-906/15/23 16:084241
N-Nitroso-di-n-propylamine ND ug/kg 06/19/23 11:16 621-64-706/15/23 16:084241
N-Nitrosodiphenylamine ND ug/kg 06/19/23 11:16 86-30-606/15/23 16:084241
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/19/23 11:16 108-60-106/15/23 16:084241
Pentachlorophenol ND ug/kg 06/19/23 11:16 87-86-506/15/23 16:088471
Phenanthrene ND ug/kg 06/19/23 11:16 85-01-806/15/23 16:084241
Phenol ND ug/kg 06/19/23 11:16 108-95-206/15/23 16:084241
Pyrene ND ug/kg 06/19/23 11:16 129-00-006/15/23 16:084241
Pyridine ND ug/kg 06/19/23 11:16 110-86-106/15/23 16:084241
1,2,4-Trichlorobenzene ND ug/kg 06/19/23 11:16 120-82-106/15/23 16:084241
2,4,5-Trichlorophenol ND ug/kg 06/19/23 11:16 95-95-406/15/23 16:084241
2,4,6-Trichlorophenol ND ug/kg 06/19/23 11:16 88-06-206/15/23 16:084241
Surrogates
Nitrobenzene-d5 (S)39 %06/19/23 11:16 4165-60-006/15/23 16:0810-130 1
2-Fluorobiphenyl (S)43 %06/19/23 11:16 321-60-806/15/23 16:0810-130 1
Terphenyl-d14 (S)59 %06/19/23 11:16 1718-51-006/15/23 16:0810-130 1
Phenol-d6 (S)35 %06/19/23 11:16 13127-88-306/15/23 16:0810-130 1
2-Fluorophenol (S)32 %06/19/23 11:16 367-12-406/15/23 16:0810-130 1
2,4,6-Tribromophenol (S)47 %06/19/23 11:16 118-79-606/15/23 16:0810-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D Lab ID:92672500008 Collected:06/13/23 14:40 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/19/23 20:22 67-64-106/19/23 14:002731
Benzene 17.2 ug/kg 06/19/23 20:22 71-43-206/19/23 14:0013.6 1
Bromobenzene ND ug/kg 06/19/23 20:22 108-86-106/19/23 14:0013.6 1
Bromochloromethane ND ug/kg 06/19/23 20:22 74-97-506/19/23 14:0013.6 1
Bromodichloromethane ND ug/kg 06/19/23 20:22 75-27-406/19/23 14:0013.6 1
Bromoform ND ug/kg 06/19/23 20:22 75-25-206/19/23 14:0013.6 1
Bromomethane ND ug/kg 06/19/23 20:22 74-83-906/19/23 14:0054.6 1
2-Butanone (MEK)ND ug/kg 06/19/23 20:22 78-93-306/19/23 14:002731
n-Butylbenzene ND ug/kg 06/19/23 20:22 104-51-806/19/23 14:0013.6 1
sec-Butylbenzene ND ug/kg 06/19/23 20:22 135-98-806/19/23 14:0013.6 1
tert-Butylbenzene ND ug/kg 06/19/23 20:22 98-06-606/19/23 14:0013.6 1
Carbon tetrachloride ND ug/kg 06/19/23 20:22 56-23-506/19/23 14:0013.6 1
Chlorobenzene ND ug/kg 06/19/23 20:22 108-90-706/19/23 14:0013.6 1
Chloroethane ND ug/kg 06/19/23 20:22 75-00-3 v106/19/23 14:0027.3 1
Chloroform ND ug/kg 06/19/23 20:22 67-66-306/19/23 14:0013.6 1
Chloromethane ND ug/kg 06/19/23 20:22 74-87-3 v106/19/23 14:0027.3 1
2-Chlorotoluene ND ug/kg 06/19/23 20:22 95-49-806/19/23 14:0013.6 1
4-Chlorotoluene ND ug/kg 06/19/23 20:22 106-43-406/19/23 14:0013.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/19/23 20:22 96-12-806/19/23 14:0013.6 1
Dibromochloromethane ND ug/kg 06/19/23 20:22 124-48-106/19/23 14:0013.6 1
1,2-Dibromoethane (EDB)ND ug/kg 06/19/23 20:22 106-93-406/19/23 14:0013.6 1
Dibromomethane ND ug/kg 06/19/23 20:22 74-95-306/19/23 14:0013.6 1
1,2-Dichlorobenzene ND ug/kg 06/19/23 20:22 95-50-106/19/23 14:0013.6 1
1,3-Dichlorobenzene ND ug/kg 06/19/23 20:22 541-73-106/19/23 14:0013.6 1
1,4-Dichlorobenzene ND ug/kg 06/19/23 20:22 106-46-706/19/23 14:0013.6 1
Dichlorodifluoromethane ND ug/kg 06/19/23 20:22 75-71-806/19/23 14:0027.3 1
1,1-Dichloroethane ND ug/kg 06/19/23 20:22 75-34-306/19/23 14:0013.6 1
1,2-Dichloroethane ND ug/kg 06/19/23 20:22 107-06-206/19/23 14:0013.6 1
1,1-Dichloroethene ND ug/kg 06/19/23 20:22 75-35-406/19/23 14:0013.6 1
cis-1,2-Dichloroethene ND ug/kg 06/19/23 20:22 156-59-206/19/23 14:0013.6 1
trans-1,2-Dichloroethene ND ug/kg 06/19/23 20:22 156-60-506/19/23 14:0013.6 1
1,2-Dichloropropane ND ug/kg 06/19/23 20:22 78-87-506/19/23 14:0013.6 1
1,3-Dichloropropane ND ug/kg 06/19/23 20:22 142-28-906/19/23 14:0013.6 1
2,2-Dichloropropane ND ug/kg 06/19/23 20:22 594-20-706/19/23 14:0013.6 1
1,1-Dichloropropene ND ug/kg 06/19/23 20:22 563-58-606/19/23 14:0013.6 1
cis-1,3-Dichloropropene ND ug/kg 06/19/23 20:22 10061-01-506/19/23 14:0013.6 1
trans-1,3-Dichloropropene ND ug/kg 06/19/23 20:22 10061-02-606/19/23 14:0013.6 1
Diisopropyl ether ND ug/kg 06/19/23 20:22 108-20-306/19/23 14:0013.6 1
Ethylbenzene 13.8 ug/kg 06/19/23 20:22 100-41-406/19/23 14:0013.6 1
Hexachloro-1,3-butadiene ND ug/kg 06/19/23 20:22 87-68-306/19/23 14:0027.3 1
2-Hexanone ND ug/kg 06/19/23 20:22 591-78-606/19/23 14:001361
Isopropylbenzene (Cumene)ND ug/kg 06/19/23 20:22 98-82-806/19/23 14:0013.6 1
p-Isopropyltoluene 80.1 ug/kg 06/19/23 20:22 99-87-606/19/23 14:0013.6 1
Methylene Chloride ND ug/kg 06/19/23 20:22 75-09-206/19/23 14:0054.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/19/23 20:22 108-10-106/19/23 14:001361
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-D Lab ID:92672500008 Collected:06/13/23 14:40 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/19/23 20:22 1634-04-406/19/23 14:0013.6 1
Naphthalene ND ug/kg 06/19/23 20:22 91-20-306/19/23 14:0013.6 1
n-Propylbenzene ND ug/kg 06/19/23 20:22 103-65-106/19/23 14:0013.6 1
Styrene ND ug/kg 06/19/23 20:22 100-42-506/19/23 14:0013.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/19/23 20:22 630-20-606/19/23 14:0013.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/19/23 20:22 79-34-506/19/23 14:0013.6 1
Tetrachloroethene ND ug/kg 06/19/23 20:22 127-18-406/19/23 14:0013.6 1
Toluene ND ug/kg 06/19/23 20:22 108-88-306/19/23 14:0013.6 1
1,2,3-Trichlorobenzene ND ug/kg 06/19/23 20:22 87-61-606/19/23 14:0013.6 1
1,2,4-Trichlorobenzene ND ug/kg 06/19/23 20:22 120-82-106/19/23 14:0013.6 1
1,1,1-Trichloroethane ND ug/kg 06/19/23 20:22 71-55-606/19/23 14:0013.6 1
1,1,2-Trichloroethane ND ug/kg 06/19/23 20:22 79-00-506/19/23 14:0013.6 1
Trichloroethene ND ug/kg 06/19/23 20:22 79-01-606/19/23 14:0013.6 1
Trichlorofluoromethane ND ug/kg 06/19/23 20:22 75-69-406/19/23 14:0013.6 1
1,2,3-Trichloropropane ND ug/kg 06/19/23 20:22 96-18-406/19/23 14:0013.6 1
1,2,4-Trimethylbenzene 254 ug/kg 06/19/23 20:22 95-63-606/19/23 14:0013.6 1
1,3,5-Trimethylbenzene ND ug/kg 06/19/23 20:22 108-67-806/19/23 14:0013.6 1
Vinyl acetate ND ug/kg 06/19/23 20:22 108-05-406/19/23 14:001361
Vinyl chloride ND ug/kg 06/19/23 20:22 75-01-4 v106/19/23 14:0027.3 1
Xylene (Total)ND ug/kg 06/19/23 20:22 1330-20-706/19/23 14:0027.3 1
m&p-Xylene ND ug/kg 06/19/23 20:22 179601-23-106/19/23 14:0027.3 1
o-Xylene ND ug/kg 06/19/23 20:22 95-47-606/19/23 14:0013.6 1
Surrogates
Toluene-d8 (S)104 %06/19/23 20:22 2037-26-506/19/23 14:0070-130 1
4-Bromofluorobenzene (S)105 %06/19/23 20:22 460-00-406/19/23 14:0070-130 1
1,2-Dichloroethane-d4 (S)107 %06/19/23 20:22 17060-07-006/19/23 14:0070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.1 %06/15/23 15:23 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-E Lab ID:92672500009 Collected:06/13/23 14:55 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/19/23 20:41 67-64-106/19/23 14:002761
Benzene 14.0 ug/kg 06/19/23 20:41 71-43-206/19/23 14:0013.8 1
Bromobenzene ND ug/kg 06/19/23 20:41 108-86-106/19/23 14:0013.8 1
Bromochloromethane ND ug/kg 06/19/23 20:41 74-97-506/19/23 14:0013.8 1
Bromodichloromethane ND ug/kg 06/19/23 20:41 75-27-406/19/23 14:0013.8 1
Bromoform ND ug/kg 06/19/23 20:41 75-25-206/19/23 14:0013.8 1
Bromomethane ND ug/kg 06/19/23 20:41 74-83-906/19/23 14:0055.3 1
2-Butanone (MEK)ND ug/kg 06/19/23 20:41 78-93-306/19/23 14:002761
n-Butylbenzene ND ug/kg 06/19/23 20:41 104-51-806/19/23 14:0013.8 1
sec-Butylbenzene ND ug/kg 06/19/23 20:41 135-98-806/19/23 14:0013.8 1
tert-Butylbenzene ND ug/kg 06/19/23 20:41 98-06-606/19/23 14:0013.8 1
Carbon tetrachloride ND ug/kg 06/19/23 20:41 56-23-506/19/23 14:0013.8 1
Chlorobenzene ND ug/kg 06/19/23 20:41 108-90-706/19/23 14:0013.8 1
Chloroethane ND ug/kg 06/19/23 20:41 75-00-3 v106/19/23 14:0027.6 1
Chloroform ND ug/kg 06/19/23 20:41 67-66-306/19/23 14:0013.8 1
Chloromethane ND ug/kg 06/19/23 20:41 74-87-3 v106/19/23 14:0027.6 1
2-Chlorotoluene ND ug/kg 06/19/23 20:41 95-49-806/19/23 14:0013.8 1
4-Chlorotoluene ND ug/kg 06/19/23 20:41 106-43-406/19/23 14:0013.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/19/23 20:41 96-12-806/19/23 14:0013.8 1
Dibromochloromethane ND ug/kg 06/19/23 20:41 124-48-106/19/23 14:0013.8 1
1,2-Dibromoethane (EDB)ND ug/kg 06/19/23 20:41 106-93-406/19/23 14:0013.8 1
Dibromomethane ND ug/kg 06/19/23 20:41 74-95-306/19/23 14:0013.8 1
1,2-Dichlorobenzene ND ug/kg 06/19/23 20:41 95-50-106/19/23 14:0013.8 1
1,3-Dichlorobenzene ND ug/kg 06/19/23 20:41 541-73-106/19/23 14:0013.8 1
1,4-Dichlorobenzene ND ug/kg 06/19/23 20:41 106-46-706/19/23 14:0013.8 1
Dichlorodifluoromethane ND ug/kg 06/19/23 20:41 75-71-806/19/23 14:0027.6 1
1,1-Dichloroethane ND ug/kg 06/19/23 20:41 75-34-306/19/23 14:0013.8 1
1,2-Dichloroethane ND ug/kg 06/19/23 20:41 107-06-206/19/23 14:0013.8 1
1,1-Dichloroethene ND ug/kg 06/19/23 20:41 75-35-406/19/23 14:0013.8 1
cis-1,2-Dichloroethene ND ug/kg 06/19/23 20:41 156-59-206/19/23 14:0013.8 1
trans-1,2-Dichloroethene ND ug/kg 06/19/23 20:41 156-60-506/19/23 14:0013.8 1
1,2-Dichloropropane ND ug/kg 06/19/23 20:41 78-87-506/19/23 14:0013.8 1
1,3-Dichloropropane ND ug/kg 06/19/23 20:41 142-28-906/19/23 14:0013.8 1
2,2-Dichloropropane ND ug/kg 06/19/23 20:41 594-20-706/19/23 14:0013.8 1
1,1-Dichloropropene ND ug/kg 06/19/23 20:41 563-58-606/19/23 14:0013.8 1
cis-1,3-Dichloropropene ND ug/kg 06/19/23 20:41 10061-01-506/19/23 14:0013.8 1
trans-1,3-Dichloropropene ND ug/kg 06/19/23 20:41 10061-02-606/19/23 14:0013.8 1
Diisopropyl ether ND ug/kg 06/19/23 20:41 108-20-306/19/23 14:0013.8 1
Ethylbenzene ND ug/kg 06/19/23 20:41 100-41-406/19/23 14:0013.8 1
Hexachloro-1,3-butadiene ND ug/kg 06/19/23 20:41 87-68-306/19/23 14:0027.6 1
2-Hexanone ND ug/kg 06/19/23 20:41 591-78-606/19/23 14:001381
Isopropylbenzene (Cumene)ND ug/kg 06/19/23 20:41 98-82-806/19/23 14:0013.8 1
p-Isopropyltoluene ND ug/kg 06/19/23 20:41 99-87-606/19/23 14:0013.8 1
Methylene Chloride ND ug/kg 06/19/23 20:41 75-09-206/19/23 14:0055.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/19/23 20:41 108-10-106/19/23 14:001381
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 93
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672500
ONE STOP 15
Sample:SOIL-E Lab ID:92672500009 Collected:06/13/23 14:55 Received:06/14/23 14:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/19/23 20:41 1634-04-406/19/23 14:0013.8 1
Naphthalene 19.6 ug/kg 06/19/23 20:41 91-20-306/19/23 14:0013.8 1
n-Propylbenzene ND ug/kg 06/19/23 20:41 103-65-106/19/23 14:0013.8 1
Styrene ND ug/kg 06/19/23 20:41 100-42-506/19/23 14:0013.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/19/23 20:41 630-20-606/19/23 14:0013.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/19/23 20:41 79-34-506/19/23 14:0013.8 1
Tetrachloroethene ND ug/kg 06/19/23 20:41 127-18-406/19/23 14:0013.8 1
Toluene ND ug/kg 06/19/23 20:41 108-88-306/19/23 14:0013.8 1
1,2,3-Trichlorobenzene ND ug/kg 06/19/23 20:41 87-61-606/19/23 14:0013.8 1
1,2,4-Trichlorobenzene ND ug/kg 06/19/23 20:41 120-82-106/19/23 14:0013.8 1
1,1,1-Trichloroethane ND ug/kg 06/19/23 20:41 71-55-606/19/23 14:0013.8 1
1,1,2-Trichloroethane ND ug/kg 06/19/23 20:41 79-00-506/19/23 14:0013.8 1
Trichloroethene ND ug/kg 06/19/23 20:41 79-01-606/19/23 14:0013.8 1
Trichlorofluoromethane ND ug/kg 06/19/23 20:41 75-69-406/19/23 14:0013.8 1
1,2,3-Trichloropropane ND ug/kg 06/19/23 20:41 96-18-406/19/23 14:0013.8 1
1,2,4-Trimethylbenzene 34.0 ug/kg 06/19/23 20:41 95-63-606/19/23 14:0013.8 1
1,3,5-Trimethylbenzene ND ug/kg 06/19/23 20:41 108-67-806/19/23 14:0013.8 1
Vinyl acetate ND ug/kg 06/19/23 20:41 108-05-406/19/23 14:001381
Vinyl chloride ND ug/kg 06/19/23 20:41 75-01-4 v106/19/23 14:0027.6 1
Xylene (Total)ND ug/kg 06/19/23 20:41 1330-20-706/19/23 14:0027.6 1
m&p-Xylene ND ug/kg 06/19/23 20:41 179601-23-106/19/23 14:0027.6 1
o-Xylene ND ug/kg 06/19/23 20:41 95-47-606/19/23 14:0013.8 1
Surrogates
Toluene-d8 (S)104 %06/19/23 20:41 2037-26-506/19/23 14:0070-130 1
4-Bromofluorobenzene (S)105 %06/19/23 20:41 460-00-406/19/23 14:0070-130 1
1,2-Dichloroethane-d4 (S)108 %06/19/23 20:41 17060-07-006/19/23 14:0070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.8 %06/15/23 16:56 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
781194
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92672500001, 92672500002, 92672500003, 92672500004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4053167
Associated Lab Samples:92672500001, 92672500002, 92672500003, 92672500004
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/17/23 13:01
1,1,1-Trichloroethane ug/kg ND 5.0 06/17/23 13:01
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/17/23 13:01
1,1,2-Trichloroethane ug/kg ND 5.0 06/17/23 13:01
1,1-Dichloroethane ug/kg ND 5.0 06/17/23 13:01
1,1-Dichloroethene ug/kg ND 5.0 06/17/23 13:01
1,1-Dichloropropene ug/kg ND 5.0 06/17/23 13:01
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/17/23 13:01
1,2,3-Trichloropropane ug/kg ND 5.0 06/17/23 13:01
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/17/23 13:01
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/17/23 13:01
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/17/23 13:01
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/17/23 13:01
1,2-Dichlorobenzene ug/kg ND 5.0 06/17/23 13:01
1,2-Dichloroethane ug/kg ND 5.0 06/17/23 13:01
1,2-Dichloropropane ug/kg ND 5.0 06/17/23 13:01
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/17/23 13:01
1,3-Dichlorobenzene ug/kg ND 5.0 06/17/23 13:01
1,3-Dichloropropane ug/kg ND 5.0 06/17/23 13:01
1,4-Dichlorobenzene ug/kg ND 5.0 06/17/23 13:01
2,2-Dichloropropane ug/kg ND 5.0 06/17/23 13:01
2-Butanone (MEK)ug/kg ND 100 06/17/23 13:01
2-Chlorotoluene ug/kg ND 5.0 06/17/23 13:01
2-Hexanone ug/kg ND 50.0 v106/17/23 13:01
4-Chlorotoluene ug/kg ND 5.0 06/17/23 13:01
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/17/23 13:01
Acetone ug/kg ND 100 06/17/23 13:01
Benzene ug/kg ND 5.0 06/17/23 13:01
Bromobenzene ug/kg ND 5.0 06/17/23 13:01
Bromochloromethane ug/kg ND 5.0 06/17/23 13:01
Bromodichloromethane ug/kg ND 5.0 06/17/23 13:01
Bromoform ug/kg ND 5.0 06/17/23 13:01
Bromomethane ug/kg ND 20.0 06/17/23 13:01
Carbon tetrachloride ug/kg ND 5.0 06/17/23 13:01
Chlorobenzene ug/kg ND 5.0 06/17/23 13:01
Chloroethane ug/kg ND 10.0 v106/17/23 13:01
Chloroform ug/kg ND 5.0 06/17/23 13:01
Chloromethane ug/kg ND 10.0 v106/17/23 13:01
cis-1,2-Dichloroethene ug/kg ND 5.0 06/17/23 13:01
cis-1,3-Dichloropropene ug/kg ND 5.0 06/17/23 13:01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4053167
Associated Lab Samples:92672500001, 92672500002, 92672500003, 92672500004
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 06/17/23 13:01
Dibromomethane ug/kg ND 5.0 06/17/23 13:01
Dichlorodifluoromethane ug/kg ND 10.0 06/17/23 13:01
Diisopropyl ether ug/kg ND 5.0 06/17/23 13:01
Ethylbenzene ug/kg ND 5.0 06/17/23 13:01
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/17/23 13:01
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/17/23 13:01
m&p-Xylene ug/kg ND 10.0 06/17/23 13:01
Methyl-tert-butyl ether ug/kg ND 5.0 06/17/23 13:01
Methylene Chloride ug/kg ND 20.0 06/17/23 13:01
n-Butylbenzene ug/kg ND 5.0 06/17/23 13:01
n-Propylbenzene ug/kg ND 5.0 06/17/23 13:01
Naphthalene ug/kg ND 5.0 06/17/23 13:01
o-Xylene ug/kg ND 5.0 06/17/23 13:01
p-Isopropyltoluene ug/kg ND 5.0 06/17/23 13:01
sec-Butylbenzene ug/kg ND 5.0 06/17/23 13:01
Styrene ug/kg ND 5.0 06/17/23 13:01
tert-Butylbenzene ug/kg ND 5.0 06/17/23 13:01
Tetrachloroethene ug/kg ND 5.0 06/17/23 13:01
Toluene ug/kg ND 5.0 06/17/23 13:01
trans-1,2-Dichloroethene ug/kg ND 5.0 06/17/23 13:01
trans-1,3-Dichloropropene ug/kg ND 5.0 06/17/23 13:01
Trichloroethene ug/kg ND 5.0 06/17/23 13:01
Trichlorofluoromethane ug/kg ND 5.0 06/17/23 13:01
Vinyl acetate ug/kg ND 50.0 06/17/23 13:01
Vinyl chloride ug/kg ND 10.0 06/17/23 13:01
Xylene (Total)ug/kg ND 10.0 06/17/23 13:01
1,2-Dichloroethane-d4 (S)%116 70-130 06/17/23 13:01
4-Bromofluorobenzene (S)%102 70-130 06/17/23 13:01
Toluene-d8 (S)%104 70-130 06/17/23 13:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4053168LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 475500 95 70-130
1,1,1-Trichloroethane ug/kg 496500 99 70-130
1,1,2,2-Tetrachloroethane ug/kg 509500 102 70-130
1,1,2-Trichloroethane ug/kg 470500 94 70-130
1,1-Dichloroethane ug/kg 509500 102 70-130
1,1-Dichloroethene ug/kg 543500 109 70-130
1,1-Dichloropropene ug/kg 515500 103 70-130
1,2,3-Trichlorobenzene ug/kg 470500 94 70-130
1,2,3-Trichloropropane ug/kg 530500 106 70-130
1,2,4-Trichlorobenzene ug/kg 459500 92 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4053168LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 469500 94 70-130
1,2-Dibromo-3-chloropropane ug/kg 450500 90 67-130
1,2-Dibromoethane (EDB)ug/kg 492500 98 70-130
1,2-Dichlorobenzene ug/kg 442500 88 70-130
1,2-Dichloroethane ug/kg 512500 102 70-130
1,2-Dichloropropane ug/kg 504500 101 70-130
1,3,5-Trimethylbenzene ug/kg 476500 95 70-130
1,3-Dichlorobenzene ug/kg 498500 100 70-130
1,3-Dichloropropane ug/kg 496500 99 70-130
1,4-Dichlorobenzene ug/kg 478500 96 70-130
2,2-Dichloropropane ug/kg 443500 89 67-130
2-Butanone (MEK)ug/kg 11601000 116 66-130
2-Chlorotoluene ug/kg 486500 97 70-130
2-Hexanone ug/kg 1220 v1100012270-130
4-Chlorotoluene ug/kg 476500 95 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 11301000 113 70-130
Acetone ug/kg 11601000 116 67-130
Benzene ug/kg 479500 96 70-130
Bromobenzene ug/kg 464500 93 70-130
Bromochloromethane ug/kg 488500 98 70-130
Bromodichloromethane ug/kg 465500 93 70-130
Bromoform ug/kg 476500 95 70-130
Bromomethane ug/kg 428500 86 53-175
Carbon tetrachloride ug/kg 460500 92 70-130
Chlorobenzene ug/kg 480500 96 70-130
Chloroethane ug/kg 622 v150012470-135
Chloroform ug/kg 484500 97 70-130
Chloromethane ug/kg 718 L1,v150014464-130
cis-1,2-Dichloroethene ug/kg 506500 101 70-130
cis-1,3-Dichloropropene ug/kg 475500 95 70-130
Dibromochloromethane ug/kg 467500 93 70-130
Dibromomethane ug/kg 440500 88 70-130
Dichlorodifluoromethane ug/kg 561500 112 63-145
Diisopropyl ether ug/kg 515500 103 68-130
Ethylbenzene ug/kg 447500 89 70-130
Hexachloro-1,3-butadiene ug/kg 407500 81 70-130
Isopropylbenzene (Cumene)ug/kg 485500 97 70-130
m&p-Xylene ug/kg 9571000 96 70-130
Methyl-tert-butyl ether ug/kg 462500 92 70-130
Methylene Chloride ug/kg 580500 116 67-130
n-Butylbenzene ug/kg 454500 91 70-130
n-Propylbenzene ug/kg 474500 95 70-130
Naphthalene ug/kg 499500 100 70-130
o-Xylene ug/kg 492500 98 70-130
p-Isopropyltoluene ug/kg 471500 94 70-130
sec-Butylbenzene ug/kg 470500 94 70-130
Styrene ug/kg 494500 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4053168LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 506500 101 64-130
Tetrachloroethene ug/kg 469500 94 70-130
Toluene ug/kg 456500 91 70-130
trans-1,2-Dichloroethene ug/kg 516500 103 70-130
trans-1,3-Dichloropropene ug/kg 461500 92 70-130
Trichloroethene ug/kg 458500 92 70-130
Trichlorofluoromethane ug/kg 509500 102 70-130
Vinyl acetate ug/kg 11601000 116 70-134
Vinyl chloride ug/kg 551500 110 68-130
Xylene (Total)ug/kg 14501500 97 70-130
1,2-Dichloroethane-d4 (S)%109 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4053169MATRIX SPIKE SAMPLE:
MSSpike
Result
92672650019
1,1,1,2-Tetrachloroethane ug/kg 733899 82 58-140ND
1,1,1-Trichloroethane ug/kg 765899 85 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 712899 79 52-139ND
1,1,2-Trichloroethane ug/kg 715899 79 56-140ND
1,1-Dichloroethane ug/kg 740899 82 58-145ND
1,1-Dichloroethene ug/kg 769899 86 57-158ND
1,1-Dichloropropene ug/kg 749899 83 58-151ND
1,2,3-Trichlorobenzene ug/kg 671899 75 48-149ND
1,2,3-Trichloropropane ug/kg 727899 81 54-132ND
1,2,4-Trichlorobenzene ug/kg 642899 71 51-151ND
1,2,4-Trimethylbenzene ug/kg 673899 75 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 625899 69 44-134ND
1,2-Dibromoethane (EDB)ug/kg 717899 80 60-138ND
1,2-Dichlorobenzene ug/kg 657899 73 59-147ND
1,2-Dichloroethane ug/kg 698899 78 57-139ND
1,2-Dichloropropane ug/kg 794899 88 62-145ND
1,3,5-Trimethylbenzene ug/kg 679899 75 47-159ND
1,3-Dichlorobenzene ug/kg 720899 80 58-144ND
1,3-Dichloropropane ug/kg 719899 80 60-142ND
1,4-Dichlorobenzene ug/kg 704899 78 57-143ND
2,2-Dichloropropane ug/kg 642899 71 37-144ND
2-Butanone (MEK)ug/kg 15001800 83 28-146ND
2-Chlorotoluene ug/kg 699899 78 55-158ND
2-Hexanone ug/kg 1530 v118008544-141ND
4-Chlorotoluene ug/kg 675899 75 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 15101800 84 50-138ND
Acetone ug/kg 12601800 70 20-136ND
Benzene ug/kg 740899 82 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4053169MATRIX SPIKE SAMPLE:
MSSpike
Result
92672650019
Bromobenzene ug/kg 698899 78 59-145ND
Bromochloromethane ug/kg 717899 80 57-143ND
Bromodichloromethane ug/kg 706899 78 53-133ND
Bromoform ug/kg 698899 78 48-133ND
Bromomethane ug/kg 151899 17 10-167ND
Carbon tetrachloride ug/kg 715899 79 57-147ND
Chlorobenzene ug/kg 739899 82 61-144ND
Chloroethane ug/kg 219 v18992410-153ND
Chloroform ug/kg 709899 79 58-141ND
Chloromethane ug/kg 1060 v189911854-165ND
cis-1,2-Dichloroethene ug/kg 723899 80 59-144ND
cis-1,3-Dichloropropene ug/kg 714899 79 56-137ND
Dibromochloromethane ug/kg 690899 77 53-139ND
Dibromomethane ug/kg 693899 77 60-136ND
Dichlorodifluoromethane ug/kg 1080899 120 49-177ND
Diisopropyl ether ug/kg 757899 84 53-136ND
Ethylbenzene ug/kg 686899 76 53-150ND
Hexachloro-1,3-butadiene ug/kg 639899 71 42-186ND
Isopropylbenzene (Cumene)ug/kg 751899 83 62-154ND
m&p-Xylene ug/kg 14501800 80 49-156ND
Methyl-tert-butyl ether ug/kg 645899 72 54-133ND
Methylene Chloride ug/kg 805899 86 50-1530.036 mg/kg
n-Butylbenzene ug/kg 604899 67 44-174ND
n-Propylbenzene ug/kg 667899 74 52-157ND
Naphthalene ug/kg 682899 76 37-150ND
o-Xylene ug/kg 763899 85 54-150ND
p-Isopropyltoluene ug/kg 670899 75 50-164ND
sec-Butylbenzene ug/kg 672899 75 58-161ND
Styrene ug/kg 731899 81 60-148ND
tert-Butylbenzene ug/kg 674899 75 44-151ND
Tetrachloroethene ug/kg 676899 75 53-151ND
Toluene ug/kg 711899 79 52-148ND
trans-1,2-Dichloroethene ug/kg 708899 79 60-148ND
trans-1,3-Dichloropropene ug/kg 675899 75 55-133ND
Trichloroethene ug/kg 740899 82 60-148ND
Trichlorofluoromethane ug/kg 216899 24 10-154ND
Vinyl acetate ug/kg 14301800 80 50-149ND
Vinyl chloride ug/kg 920899 102 57-157ND
Xylene (Total)ug/kg 22102690 82 52-153ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92672650020
4053170SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg ND v1ND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg ND v1ND
Chloroform ug/kg NDND
Chloromethane ug/kg ND v1ND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 39 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92672650020
4053170SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%109108
4-Bromofluorobenzene (S)%104103
Toluene-d8 (S)%102103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 40 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
781504
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92672500005, 92672500006, 92672500007, 92672500008, 92672500009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4054590
Associated Lab Samples:92672500005, 92672500006, 92672500007, 92672500008, 92672500009
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/19/23 13:37
1,1,1-Trichloroethane ug/kg ND 5.0 06/19/23 13:37
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/19/23 13:37
1,1,2-Trichloroethane ug/kg ND 5.0 06/19/23 13:37
1,1-Dichloroethane ug/kg ND 5.0 06/19/23 13:37
1,1-Dichloroethene ug/kg ND 5.0 06/19/23 13:37
1,1-Dichloropropene ug/kg ND 5.0 06/19/23 13:37
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/19/23 13:37
1,2,3-Trichloropropane ug/kg ND 5.0 06/19/23 13:37
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/19/23 13:37
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/19/23 13:37
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/19/23 13:37
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/19/23 13:37
1,2-Dichlorobenzene ug/kg ND 5.0 06/19/23 13:37
1,2-Dichloroethane ug/kg ND 5.0 06/19/23 13:37
1,2-Dichloropropane ug/kg ND 5.0 06/19/23 13:37
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/19/23 13:37
1,3-Dichlorobenzene ug/kg ND 5.0 06/19/23 13:37
1,3-Dichloropropane ug/kg ND 5.0 06/19/23 13:37
1,4-Dichlorobenzene ug/kg ND 5.0 06/19/23 13:37
2,2-Dichloropropane ug/kg ND 5.0 06/19/23 13:37
2-Butanone (MEK)ug/kg ND 100 06/19/23 13:37
2-Chlorotoluene ug/kg ND 5.0 06/19/23 13:37
2-Hexanone ug/kg ND 50.0 06/19/23 13:37
4-Chlorotoluene ug/kg ND 5.0 06/19/23 13:37
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/19/23 13:37
Acetone ug/kg ND 100 06/19/23 13:37
Benzene ug/kg ND 5.0 06/19/23 13:37
Bromobenzene ug/kg ND 5.0 06/19/23 13:37
Bromochloromethane ug/kg ND 5.0 06/19/23 13:37
Bromodichloromethane ug/kg ND 5.0 06/19/23 13:37
Bromoform ug/kg ND 5.0 06/19/23 13:37
Bromomethane ug/kg ND 20.0 06/19/23 13:37
Carbon tetrachloride ug/kg ND 5.0 06/19/23 13:37
Chlorobenzene ug/kg ND 5.0 06/19/23 13:37
Chloroethane ug/kg ND 10.0 v106/19/23 13:37
Chloroform ug/kg ND 5.0 06/19/23 13:37
Chloromethane ug/kg ND 10.0 v106/19/23 13:37
cis-1,2-Dichloroethene ug/kg ND 5.0 06/19/23 13:37
cis-1,3-Dichloropropene ug/kg ND 5.0 06/19/23 13:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 41 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4054590
Associated Lab Samples:92672500005, 92672500006, 92672500007, 92672500008, 92672500009
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 06/19/23 13:37
Dibromomethane ug/kg ND 5.0 06/19/23 13:37
Dichlorodifluoromethane ug/kg ND 10.0 06/19/23 13:37
Diisopropyl ether ug/kg ND 5.0 06/19/23 13:37
Ethylbenzene ug/kg ND 5.0 06/19/23 13:37
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/19/23 13:37
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/19/23 13:37
m&p-Xylene ug/kg ND 10.0 06/19/23 13:37
Methyl-tert-butyl ether ug/kg ND 5.0 06/19/23 13:37
Methylene Chloride ug/kg ND 20.0 06/19/23 13:37
n-Butylbenzene ug/kg ND 5.0 06/19/23 13:37
n-Propylbenzene ug/kg ND 5.0 06/19/23 13:37
Naphthalene ug/kg ND 5.0 06/19/23 13:37
o-Xylene ug/kg ND 5.0 06/19/23 13:37
p-Isopropyltoluene ug/kg ND 5.0 06/19/23 13:37
sec-Butylbenzene ug/kg ND 5.0 06/19/23 13:37
Styrene ug/kg ND 5.0 06/19/23 13:37
tert-Butylbenzene ug/kg ND 5.0 06/19/23 13:37
Tetrachloroethene ug/kg ND 5.0 06/19/23 13:37
Toluene ug/kg ND 5.0 06/19/23 13:37
trans-1,2-Dichloroethene ug/kg ND 5.0 06/19/23 13:37
trans-1,3-Dichloropropene ug/kg ND 5.0 06/19/23 13:37
Trichloroethene ug/kg ND 5.0 06/19/23 13:37
Trichlorofluoromethane ug/kg ND 5.0 06/19/23 13:37
Vinyl acetate ug/kg ND 50.0 06/19/23 13:37
Vinyl chloride ug/kg ND 10.0 v106/19/23 13:37
Xylene (Total)ug/kg ND 10.0 06/19/23 13:37
1,2-Dichloroethane-d4 (S)%106 70-130 06/19/23 13:37
4-Bromofluorobenzene (S)%102 70-130 06/19/23 13:37
Toluene-d8 (S)%102 70-130 06/19/23 13:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4054591LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 487500 97 70-130
1,1,1-Trichloroethane ug/kg 473500 95 70-130
1,1,2,2-Tetrachloroethane ug/kg 488500 98 70-130
1,1,2-Trichloroethane ug/kg 458500 92 70-130
1,1-Dichloroethane ug/kg 472500 94 70-130
1,1-Dichloroethene ug/kg 496500 99 70-130
1,1-Dichloropropene ug/kg 496500 99 70-130
1,2,3-Trichlorobenzene ug/kg 494500 99 70-130
1,2,3-Trichloropropane ug/kg 518500 104 70-130
1,2,4-Trichlorobenzene ug/kg 497500 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 42 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4054591LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 488500 98 70-130
1,2-Dibromo-3-chloropropane ug/kg 437500 87 67-130
1,2-Dibromoethane (EDB)ug/kg 487500 97 70-130
1,2-Dichlorobenzene ug/kg 454500 91 70-130
1,2-Dichloroethane ug/kg 448500 90 70-130
1,2-Dichloropropane ug/kg 496500 99 70-130
1,3,5-Trimethylbenzene ug/kg 486500 97 70-130
1,3-Dichlorobenzene ug/kg 507500 101 70-130
1,3-Dichloropropane ug/kg 485500 97 70-130
1,4-Dichlorobenzene ug/kg 503500 101 70-130
2,2-Dichloropropane ug/kg 470500 94 67-130
2-Butanone (MEK)ug/kg 10301000 103 66-130
2-Chlorotoluene ug/kg 494500 99 70-130
2-Hexanone ug/kg 11001000 110 70-130
4-Chlorotoluene ug/kg 489500 98 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 10601000 106 70-130
Acetone ug/kg 9591000 96 67-130
Benzene ug/kg 471500 94 70-130
Bromobenzene ug/kg 478500 96 70-130
Bromochloromethane ug/kg 475500 95 70-130
Bromodichloromethane ug/kg 463500 93 70-130
Bromoform ug/kg 489500 98 70-130
Bromomethane ug/kg 420500 84 53-175
Carbon tetrachloride ug/kg 490500 98 70-130
Chlorobenzene ug/kg 493500 99 70-130
Chloroethane ug/kg 645 v150012970-135
Chloroform ug/kg 450500 90 70-130
Chloromethane ug/kg 648 v150013064-130
cis-1,2-Dichloroethene ug/kg 466500 93 70-130
cis-1,3-Dichloropropene ug/kg 481500 96 70-130
Dibromochloromethane ug/kg 480500 96 70-130
Dibromomethane ug/kg 466500 93 70-130
Dichlorodifluoromethane ug/kg 674500 135 63-145
Diisopropyl ether ug/kg 476500 95 68-130
Ethylbenzene ug/kg 463500 93 70-130
Hexachloro-1,3-butadiene ug/kg 479500 96 70-130
Isopropylbenzene (Cumene)ug/kg 514500 103 70-130
m&p-Xylene ug/kg 10101000 101 70-130
Methyl-tert-butyl ether ug/kg 416500 83 70-130
Methylene Chloride ug/kg 505500 101 67-130
n-Butylbenzene ug/kg 480500 96 70-130
n-Propylbenzene ug/kg 489500 98 70-130
Naphthalene ug/kg 481500 96 70-130
o-Xylene ug/kg 518500 104 70-130
p-Isopropyltoluene ug/kg 506500 101 70-130
sec-Butylbenzene ug/kg 484500 97 70-130
Styrene ug/kg 512500 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 43 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4054591LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 513500 103 64-130
Tetrachloroethene ug/kg 509500 102 70-130
Toluene ug/kg 466500 93 70-130
trans-1,2-Dichloroethene ug/kg 481500 96 70-130
trans-1,3-Dichloropropene ug/kg 466500 93 70-130
Trichloroethene ug/kg 484500 97 70-130
Trichlorofluoromethane ug/kg 592500 118 70-130
Vinyl acetate ug/kg 10501000 105 70-134
Vinyl chloride ug/kg 587 v150011768-130
Xylene (Total)ug/kg 15301500 102 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4054593MATRIX SPIKE SAMPLE:
MSSpike
Result
92672976004
1,1,1,2-Tetrachloroethane ug/kg 528669 79 58-140<2.6
1,1,1-Trichloroethane ug/kg 536669 80 58-144<3.5
1,1,2,2-Tetrachloroethane ug/kg 540669 81 52-139<1.8
1,1,2-Trichloroethane ug/kg 530669 79 56-140<2.2
1,1-Dichloroethane ug/kg 547669 82 58-145<2.8
1,1-Dichloroethene ug/kg 521669 78 57-158<2.8
1,1-Dichloropropene ug/kg 542669 81 58-151<3.2
1,2,3-Trichlorobenzene ug/kg 522669 78 48-149<5.4
1,2,3-Trichloropropane ug/kg 513 IK6697754-132<3.4
1,2,4-Trichlorobenzene ug/kg 448669 67 51-151<5.6
1,2,4-Trimethylbenzene ug/kg 522669 78 38-170<4.0
1,2-Dibromo-3-chloropropane ug/kg 435669 65 44-134<2.6
1,2-Dibromoethane (EDB)ug/kg 521669 78 60-138<2.9
1,2-Dichlorobenzene ug/kg 547669 82 59-147<2.4
1,2-Dichloroethane ug/kg 518669 77 57-139<4.4
1,2-Dichloropropane ug/kg 536669 80 62-145<2.0
1,3,5-Trimethylbenzene ug/kg 519669 78 47-159<2.2
1,3-Dichlorobenzene ug/kg 492669 73 58-144<2.1
1,3-Dichloropropane ug/kg 514669 77 60-142<2.1
1,4-Dichlorobenzene ug/kg 499669 75 57-143<1.7
2,2-Dichloropropane ug/kg 483669 72 37-144<5.1
2-Butanone (MEK)ug/kg 9371340 70 28-146<32.1
2-Chlorotoluene ug/kg 510669 76 55-158<2.4
2-Hexanone ug/kg 9641340 72 44-141<6.5
4-Chlorotoluene ug/kg 525669 78 55-146<3.7
4-Methyl-2-pentanone (MIBK)ug/kg 10101340 76 50-138<6.5
Acetone ug/kg 8811340 64 20-136<43.0
Benzene ug/kg 569669 85 60-145<2.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 44 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4054593MATRIX SPIKE SAMPLE:
MSSpike
Result
92672976004
Bromobenzene ug/kg 510669 76 59-145<2.2
Bromochloromethane ug/kg 555669 83 57-143<2.0
Bromodichloromethane ug/kg 520669 78 53-133<2.6
Bromoform ug/kg 510669 76 48-133<2.4
Bromomethane ug/kg 418669 62 10-167<20.7
Carbon tetrachloride ug/kg 517669 77 57-147<2.5
Chlorobenzene ug/kg 512669 76 61-144<3.8
Chloroethane ug/kg 216669 32 10-153<5.2
Chloroform ug/kg 555669 83 58-141<5.6
Chloromethane ug/kg 604669 90 54-165<5.6
cis-1,2-Dichloroethene ug/kg 556669 83 59-144<2.3
cis-1,3-Dichloropropene ug/kg 538669 80 56-137<1.8
Dibromochloromethane ug/kg 509669 76 53-139<3.8
Dibromomethane ug/kg 517669 77 60-136<1.4
Dichlorodifluoromethane ug/kg 695 IH,v166910449-177<6.8
Diisopropyl ether ug/kg 495669 74 53-136<1.8
Ethylbenzene ug/kg 541669 81 53-150<3.1
Hexachloro-1,3-butadiene ug/kg 498669 74 42-186<10.9
Isopropylbenzene (Cumene)ug/kg 541669 81 62-154<2.3
m&p-Xylene ug/kg 9821340 73 49-156<4.6
Methyl-tert-butyl ether ug/kg 469669 70 54-133<2.5
Methylene Chloride ug/kg 509 IK,v36697650-153<18.3
n-Butylbenzene ug/kg 475669 71 44-174<4.2
n-Propylbenzene ug/kg 498669 74 52-157<2.4
Naphthalene ug/kg 486669 73 37-150<3.5
o-Xylene ug/kg 507669 76 54-150<3.0
p-Isopropyltoluene ug/kg 507669 75 50-1647.6
sec-Butylbenzene ug/kg 509669 76 58-161<2.9
Styrene ug/kg 532669 80 60-148<1.8
tert-Butylbenzene ug/kg 515669 77 44-151<2.4
Tetrachloroethene ug/kg 455669 68 53-151<2.1
Toluene ug/kg 504669 75 52-148<4.6
trans-1,2-Dichloroethene ug/kg 540669 81 60-148<5.7
trans-1,3-Dichloropropene ug/kg 509669 76 55-133<2.3
Trichloroethene ug/kg 539669 81 60-148<5.4
Trichlorofluoromethane ug/kg 212669 32 10-154<3.7
Vinyl acetate ug/kg 8831340 66 50-149<13.8
Vinyl chloride ug/kg 568669 85 57-157<3.4
Xylene (Total)ug/kg 14902010 74 52-153<3.8
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 45 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92672976003
4054592SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND<2.4
1,1,1-Trichloroethane ug/kg ND<3.3
1,1,2,2-Tetrachloroethane ug/kg ND<1.7
1,1,2-Trichloroethane ug/kg ND<2.1
1,1-Dichloroethane ug/kg ND<2.6
1,1-Dichloroethene ug/kg ND<2.6
1,1-Dichloropropene ug/kg ND<3.0
1,2,3-Trichlorobenzene ug/kg ND<5.1
1,2,3-Trichloropropane ug/kg ND<3.2
1,2,4-Trichlorobenzene ug/kg ND<5.3
1,2,4-Trimethylbenzene ug/kg ND<3.8
1,2-Dibromo-3-chloropropane ug/kg ND<2.5
1,2-Dibromoethane (EDB)ug/kg ND<2.8
1,2-Dichlorobenzene ug/kg ND<2.3
1,2-Dichloroethane ug/kg ND<4.2
1,2-Dichloropropane ug/kg ND<1.9
1,3,5-Trimethylbenzene ug/kg ND<2.1
1,3-Dichlorobenzene ug/kg ND<2.0
1,3-Dichloropropane ug/kg ND<2.0
1,4-Dichlorobenzene ug/kg ND<1.6
2,2-Dichloropropane ug/kg ND<4.8
2-Butanone (MEK)ug/kg 35.5J36.9J
2-Chlorotoluene ug/kg ND<2.2
2-Hexanone ug/kg ND<6.1
4-Chlorotoluene ug/kg ND<3.5
4-Methyl-2-pentanone (MIBK)ug/kg ND<6.1
Acetone ug/kg 99.2J119J
Benzene ug/kg ND<2.5
Bromobenzene ug/kg ND<2.1
Bromochloromethane ug/kg ND<1.9
Bromodichloromethane ug/kg ND<2.4
Bromoform ug/kg ND<2.2
Bromomethane ug/kg ND<19.6
Carbon tetrachloride ug/kg ND<2.4
Chlorobenzene ug/kg ND<3.6
Chloroethane ug/kg ND v1<4.9
Chloroform ug/kg ND<5.3
Chloromethane ug/kg ND v1<5.3
cis-1,2-Dichloroethene ug/kg ND<2.2
cis-1,3-Dichloropropene ug/kg ND<1.7
Dibromochloromethane ug/kg ND<3.6
Dibromomethane ug/kg ND<1.4
Dichlorodifluoromethane ug/kg ND<6.4
Diisopropyl ether ug/kg ND<1.7
Ethylbenzene ug/kg ND<3.0
Hexachloro-1,3-butadiene ug/kg ND<10.4
Isopropylbenzene (Cumene)ug/kg ND<2.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 46 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92672976003
4054592SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND<4.3
Methyl-tert-butyl ether ug/kg ND<2.4
Methylene Chloride ug/kg ND<17.4
n-Butylbenzene ug/kg ND<4.0
n-Propylbenzene ug/kg ND<2.3
Naphthalene ug/kg ND<3.3
o-Xylene ug/kg ND<2.8
p-Isopropyltoluene ug/kg 433 1437
sec-Butylbenzene ug/kg ND<2.8
Styrene ug/kg ND<1.7
tert-Butylbenzene ug/kg ND<2.3
Tetrachloroethene ug/kg ND<2.0
Toluene ug/kg ND<4.4
trans-1,2-Dichloroethene ug/kg ND<5.4
trans-1,3-Dichloropropene ug/kg ND<2.2
Trichloroethene ug/kg ND<5.1
Trichlorofluoromethane ug/kg ND<3.5
Vinyl acetate ug/kg ND<13.0
Vinyl chloride ug/kg ND v1<3.2
Xylene (Total)ug/kg ND<3.6
1,2-Dichloroethane-d4 (S)%109112
4-Bromofluorobenzene (S)%107108
Toluene-d8 (S)%101102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 47 of 93
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
780696
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92672500001, 92672500002, 92672500005, 92672500006, 92672500007, 92672500008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4049857
Associated Lab Samples:92672500001, 92672500002, 92672500005, 92672500006, 92672500007, 92672500008
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 331 06/15/23 13:37
1,2-Dichlorobenzene ug/kg ND 331 06/15/23 13:37
1,3-Dichlorobenzene ug/kg ND 331 06/15/23 13:37
1,4-Dichlorobenzene ug/kg ND 331 06/15/23 13:37
1-Methylnaphthalene ug/kg ND 331 06/15/23 13:37
2,2'-Oxybis(1-chloropropane)ug/kg ND 331 v106/15/23 13:37
2,4,5-Trichlorophenol ug/kg ND 331 06/15/23 13:37
2,4,6-Trichlorophenol ug/kg ND 331 06/15/23 13:37
2,4-Dichlorophenol ug/kg ND 331 06/15/23 13:37
2,4-Dimethylphenol ug/kg ND 331 06/15/23 13:37
2,4-Dinitrophenol ug/kg ND 1660 06/15/23 13:37
2,4-Dinitrotoluene ug/kg ND 331 06/15/23 13:37
2,6-Dinitrotoluene ug/kg ND 331 06/15/23 13:37
2-Chloronaphthalene ug/kg ND 331 06/15/23 13:37
2-Chlorophenol ug/kg ND 331 06/15/23 13:37
2-Methylnaphthalene ug/kg ND 331 06/15/23 13:37
2-Methylphenol(o-Cresol)ug/kg ND 331 06/15/23 13:37
2-Nitroaniline ug/kg ND 1660 06/15/23 13:37
2-Nitrophenol ug/kg ND 331 06/15/23 13:37
3&4-Methylphenol(m&p Cresol)ug/kg ND 331 06/15/23 13:37
3,3'-Dichlorobenzidine ug/kg ND 662 06/15/23 13:37
3-Nitroaniline ug/kg ND 1660 06/15/23 13:37
4,6-Dinitro-2-methylphenol ug/kg ND 662 06/15/23 13:37
4-Bromophenylphenyl ether ug/kg ND 331 06/15/23 13:37
4-Chloro-3-methylphenol ug/kg ND 662 06/15/23 13:37
4-Chloroaniline ug/kg ND 662 06/15/23 13:37
4-Chlorophenylphenyl ether ug/kg ND 331 06/15/23 13:37
4-Nitroaniline ug/kg ND 662 06/15/23 13:37
4-Nitrophenol ug/kg ND 1660 06/15/23 13:37
Acenaphthene ug/kg ND 331 06/15/23 13:37
Acenaphthylene ug/kg ND 331 06/15/23 13:37
Aniline ug/kg ND 331 06/15/23 13:37
Anthracene ug/kg ND 331 06/15/23 13:37
Benzo(a)anthracene ug/kg ND 331 06/15/23 13:37
Benzo(a)pyrene ug/kg ND 331 06/15/23 13:37
Benzo(b)fluoranthene ug/kg ND 331 06/15/23 13:37
Benzo(g,h,i)perylene ug/kg ND 331 06/15/23 13:37
Benzo(k)fluoranthene ug/kg ND 331 06/15/23 13:37
Benzoic Acid ug/kg ND 1660 06/15/23 13:37
Benzyl alcohol ug/kg ND 662 06/15/23 13:37
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4049857
Associated Lab Samples:92672500001, 92672500002, 92672500005, 92672500006, 92672500007, 92672500008
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane ug/kg ND 331 06/15/23 13:37
bis(2-Chloroethyl) ether ug/kg ND 331 06/15/23 13:37
bis(2-Ethylhexyl)phthalate ug/kg ND 331 06/15/23 13:37
Butylbenzylphthalate ug/kg ND 331 06/15/23 13:37
Chrysene ug/kg ND 331 06/15/23 13:37
Di-n-butylphthalate ug/kg ND 331 06/15/23 13:37
Di-n-octylphthalate ug/kg ND 331 06/15/23 13:37
Dibenz(a,h)anthracene ug/kg ND 331 06/15/23 13:37
Dibenzofuran ug/kg ND 331 06/15/23 13:37
Diethylphthalate ug/kg ND 331 06/15/23 13:37
Dimethylphthalate ug/kg ND 331 06/15/23 13:37
Fluoranthene ug/kg ND 331 06/15/23 13:37
Fluorene ug/kg ND 331 06/15/23 13:37
Hexachloro-1,3-butadiene ug/kg ND 331 06/15/23 13:37
Hexachlorobenzene ug/kg ND 331 06/15/23 13:37
Hexachlorocyclopentadiene ug/kg ND 331 06/15/23 13:37
Hexachloroethane ug/kg ND 331 06/15/23 13:37
Indeno(1,2,3-cd)pyrene ug/kg ND 331 06/15/23 13:37
Isophorone ug/kg ND 331 06/15/23 13:37
N-Nitroso-di-n-propylamine ug/kg ND 331 06/15/23 13:37
N-Nitrosodimethylamine ug/kg ND 331 06/15/23 13:37
N-Nitrosodiphenylamine ug/kg ND 331 06/15/23 13:37
Naphthalene ug/kg ND 331 06/15/23 13:37
Nitrobenzene ug/kg ND 331 06/15/23 13:37
Pentachlorophenol ug/kg ND 662 06/15/23 13:37
Phenanthrene ug/kg ND 331 06/15/23 13:37
Phenol ug/kg ND 331 06/15/23 13:37
Pyrene ug/kg ND 331 06/15/23 13:37
Pyridine ug/kg ND 331 06/15/23 13:37
2,4,6-Tribromophenol (S)%68 10-131 06/15/23 13:37
2-Fluorobiphenyl (S)%62 10-130 06/15/23 13:37
2-Fluorophenol (S)%65 10-130 06/15/23 13:37
Nitrobenzene-d5 (S)%78 10-130 06/15/23 13:37
Phenol-d6 (S)%63 10-130 06/15/23 13:37
Terphenyl-d14 (S)%82 10-130 06/15/23 13:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4049858LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13201670 79 43-130
1,2-Dichlorobenzene ug/kg 13301670 80 43-130
1,3-Dichlorobenzene ug/kg 12901670 77 43-130
1,4-Dichlorobenzene ug/kg 12901670 77 44-130
1-Methylnaphthalene ug/kg 14901670 89 47-130
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4049858LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 1370 v116708229-130
2,4,5-Trichlorophenol ug/kg 13701670 82 47-130
2,4,6-Trichlorophenol ug/kg 13501670 81 47-130
2,4-Dichlorophenol ug/kg 14501670 87 45-130
2,4-Dimethylphenol ug/kg 20901670 125 45-130
2,4-Dinitrophenol ug/kg 69708360 83 27-140
2,4-Dinitrotoluene ug/kg 14701670 88 46-130
2,6-Dinitrotoluene ug/kg 15001670 90 48-130
2-Chloronaphthalene ug/kg 12701670 76 46-130
2-Chlorophenol ug/kg 14001670 83 43-130
2-Methylnaphthalene ug/kg 13801670 83 47-130
2-Methylphenol(o-Cresol)ug/kg 14601670 87 42-130
2-Nitroaniline ug/kg 26903340 80 41-130
2-Nitrophenol ug/kg 15501670 93 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 15801670 95 39-130
3,3'-Dichlorobenzidine ug/kg 27203340 81 41-130
3-Nitroaniline ug/kg 23803340 71 37-130
4,6-Dinitro-2-methylphenol ug/kg 31203340 93 38-141
4-Bromophenylphenyl ether ug/kg 13301670 80 47-130
4-Chloro-3-methylphenol ug/kg 30403340 91 44-130
4-Chloroaniline ug/kg 25003340 75 41-130
4-Chlorophenylphenyl ether ug/kg 13501670 81 45-130
4-Nitroaniline ug/kg 27403340 82 42-130
4-Nitrophenol ug/kg 71908360 86 39-131
Acenaphthene ug/kg 13801670 82 49-130
Acenaphthylene ug/kg 13601670 81 50-130
Aniline ug/kg 10901670 65 38-130
Anthracene ug/kg 13301670 80 49-130
Benzo(a)anthracene ug/kg 14301670 86 51-130
Benzo(a)pyrene ug/kg 18501670 111 51-130
Benzo(b)fluoranthene ug/kg 18401670 110 49-130
Benzo(g,h,i)perylene ug/kg 17601670 105 48-140
Benzo(k)fluoranthene ug/kg 19901670 119 51-130
Benzoic Acid ug/kg 38508360 46 22-130
Benzyl alcohol ug/kg 27303340 82 43-130
bis(2-Chloroethoxy)methane ug/kg 13301670 80 43-130
bis(2-Chloroethyl) ether ug/kg 13001670 77 42-130
bis(2-Ethylhexyl)phthalate ug/kg 16501670 99 43-130
Butylbenzylphthalate ug/kg 16501670 98 44-131
Chrysene ug/kg 15601670 93 51-130
Di-n-butylphthalate ug/kg 14701670 88 46-130
Di-n-octylphthalate ug/kg 16601670 99 45-130
Dibenz(a,h)anthracene ug/kg 19501670 117 48-130
Dibenzofuran ug/kg 13501670 81 10-130
Diethylphthalate ug/kg 15001670 89 48-130
Dimethylphthalate ug/kg 14601670 87 48-130
Fluoranthene ug/kg 14401670 86 48-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4049858LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 13801670 83 48-130
Hexachloro-1,3-butadiene ug/kg 13301670 80 39-130
Hexachlorobenzene ug/kg 13001670 78 47-130
Hexachlorocyclopentadiene ug/kg 9881670 59 17-130
Hexachloroethane ug/kg 13601670 81 40-130
Indeno(1,2,3-cd)pyrene ug/kg 18001670 108 50-130
Isophorone ug/kg 14801670 89 41-130
N-Nitroso-di-n-propylamine ug/kg 15001670 90 36-130
N-Nitrosodimethylamine ug/kg 12701670 76 34-130
N-Nitrosodiphenylamine ug/kg 13201670 79 48-130
Naphthalene ug/kg 13901670 83 46-130
Nitrobenzene ug/kg 13601670 81 39-130
Pentachlorophenol ug/kg 26903340 80 42-130
Phenanthrene ug/kg 14401670 86 50-130
Phenol ug/kg 15001670 89 42-130
Pyrene ug/kg 15101670 90 50-130
Pyridine ug/kg 11101670 66 26-130
2,4,6-Tribromophenol (S)%83 10-131
2-Fluorobiphenyl (S)%75 10-130
2-Fluorophenol (S)%75 10-130
Nitrobenzene-d5 (S)%80 10-130
Phenol-d6 (S)%81 10-130
Terphenyl-d14 (S)%90 10-130
Parameter Units
Dup
Result QualifiersRPDResult
92672100010
4049860SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
1-Methylnaphthalene ug/kg NDND
2,2'-Oxybis(1-chloropropane)ug/kg NDND
2,4,5-Trichlorophenol ug/kg NDND
2,4,6-Trichlorophenol ug/kg NDND
2,4-Dichlorophenol ug/kg NDND
2,4-Dimethylphenol ug/kg NDND
2,4-Dinitrophenol ug/kg NDND
2,4-Dinitrotoluene ug/kg NDND
2,6-Dinitrotoluene ug/kg NDND
2-Chloronaphthalene ug/kg NDND
2-Chlorophenol ug/kg NDND
2-Methylnaphthalene ug/kg NDND
2-Methylphenol(o-Cresol)ug/kg NDND
2-Nitroaniline ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92672100010
4049860SAMPLE DUPLICATE:
2-Nitrophenol ug/kg NDND
3&4-Methylphenol(m&p Cresol)ug/kg NDND
3,3'-Dichlorobenzidine ug/kg NDND
3-Nitroaniline ug/kg NDND
4,6-Dinitro-2-methylphenol ug/kg NDND
4-Bromophenylphenyl ether ug/kg NDND
4-Chloro-3-methylphenol ug/kg NDND
4-Chloroaniline ug/kg NDND
4-Chlorophenylphenyl ether ug/kg NDND
4-Nitroaniline ug/kg NDND
4-Nitrophenol ug/kg NDND
Acenaphthene ug/kg NDND
Acenaphthylene ug/kg NDND
Aniline ug/kg NDND
Anthracene ug/kg NDND
Benzo(a)anthracene ug/kg NDND
Benzo(a)pyrene ug/kg NDND
Benzo(b)fluoranthene ug/kg 169JND
Benzo(g,h,i)perylene ug/kg NDND
Benzo(k)fluoranthene ug/kg NDND
Benzoic Acid ug/kg NDND
Benzyl alcohol ug/kg NDND
bis(2-Chloroethoxy)methane ug/kg NDND
bis(2-Chloroethyl) ether ug/kg NDND
bis(2-Ethylhexyl)phthalate ug/kg NDND
Butylbenzylphthalate ug/kg NDND
Chrysene ug/kg NDND
Di-n-butylphthalate ug/kg NDND
Di-n-octylphthalate ug/kg NDND
Dibenz(a,h)anthracene ug/kg NDND
Dibenzofuran ug/kg NDND
Diethylphthalate ug/kg NDND
Dimethylphthalate ug/kg NDND
Fluoranthene ug/kg 200JND
Fluorene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Hexachlorobenzene ug/kg NDND
Hexachlorocyclopentadiene ug/kg ND v2ND
Hexachloroethane ug/kg NDND
Indeno(1,2,3-cd)pyrene ug/kg NDND
Isophorone ug/kg NDND
N-Nitroso-di-n-propylamine ug/kg NDND
N-Nitrosodimethylamine ug/kg NDND
N-Nitrosodiphenylamine ug/kg NDND
Naphthalene ug/kg NDND
Nitrobenzene ug/kg NDND
Pentachlorophenol ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92672100010
4049860SAMPLE DUPLICATE:
Phenanthrene ug/kg 146JND
Phenol ug/kg NDND
Pyrene ug/kg 204JND
Pyridine ug/kg NDND
2,4,6-Tribromophenol (S)%7277
2-Fluorobiphenyl (S)%6771
2-Fluorophenol (S)%6668
Nitrobenzene-d5 (S)%7274
Phenol-d6 (S)%6869
Terphenyl-d14 (S)%8590
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
781272
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92672500001, 92672500002, 92672500005, 92672500006, 92672500007, 92672500008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4053390
Associated Lab Samples:92672500001, 92672500002, 92672500005, 92672500006, 92672500007, 92672500008
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10 N206/19/23 10:15
Aliphatic (C19-C36)mg/kg ND 10 N206/19/23 10:15
Aromatic (C11-C22)mg/kg ND 10 N206/19/23 10:15
1-Chlorooctadecane (S)%125 40-140 06/19/23 10:15
2-Bromonaphthalene (S)%89 40-140 06/19/23 10:15
2-Fluorobiphenyl (S)%89 40-140 06/19/23 10:15
o-Terphenyl (S)%90 40-140 06/19/23 10:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4053391LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
4053392
Aliphatic (C09-C18)mg/kg ND N2106640-14067ND 50
Aliphatic (C19-C36)mg/kg 17.4 N213.3 130 40-14011915.7 10 50
Aromatic (C11-C22)mg/kg 20.7 N228.3 73 40-1407821.9 5 50
1-Chlorooctadecane (S)%126 40-140110
2-Bromonaphthalene (S)%61 40-14059
2-Fluorobiphenyl (S)%62 40-14062
o-Terphenyl (S)%78 40-14078
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
780828
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92672500002, 92672500005
Parameter Units
Dup
Result QualifiersRPDResult
92672319001
4050867SAMPLE DUPLICATE:
Percent Moisture %21.9 N2422.8
Parameter Units
Dup
Result QualifiersRPDResult
92672228033
4050868SAMPLE DUPLICATE:
Percent Moisture %14.2 N2114.0
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
780844
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92672500006, 92672500007, 92672500008
Parameter Units
Dup
Result QualifiersRPDResult
92672428001
4051031SAMPLE DUPLICATE:
Percent Moisture %6.8 N216.9
Parameter Units
Dup
Result QualifiersRPDResult
92672500008
4051032SAMPLE DUPLICATE:
Percent Moisture %22.7 N2322.1
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672500
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
780893
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92672500001, 92672500003, 92672500004, 92672500009
Parameter Units
Dup
Result QualifiersRPDResult
92672650001
4051270SAMPLE DUPLICATE:
Percent Moisture %21.4 N2622.8
Parameter Units
Dup
Result QualifiersRPDResult
92672438010
4051271SAMPLE DUPLICATE:
Percent Moisture %19.0 N2019.0
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92672500
ONE STOP 15
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92672500
ONE STOP 15
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92672500001 781272 781356SOIL-D-1 MADEP EPH MADEP EPH
92672500002 781272 781356SOIL-D-2 MADEP EPH MADEP EPH
92672500005 781272 781356SOIL-A MADEP EPH MADEP EPH
92672500006 781272 781356SOIL-B MADEP EPH MADEP EPH
92672500007 781272 781356SOIL-C MADEP EPH MADEP EPH
92672500008 781272 781356SOIL-D MADEP EPH MADEP EPH
92672500001 780696 780960SOIL-D-1 EPA 3546 EPA 8270E
92672500002 780696 780960SOIL-D-2 EPA 3546 EPA 8270E
92672500005 780696 780960SOIL-A EPA 3546 EPA 8270E
92672500006 780696 780960SOIL-B EPA 3546 EPA 8270E
92672500007 780696 780960SOIL-C EPA 3546 EPA 8270E
92672500008 780696 780960SOIL-D EPA 3546 EPA 8270E
92672500001 781194 781409SOIL-D-1 EPA 5035A/5030B EPA 8260D
92672500002 781194 781409SOIL-D-2 EPA 5035A/5030B EPA 8260D
92672500003 781194 781409SOIL-D-3 EPA 5035A/5030B EPA 8260D
92672500004 781194 781409SOIL-D-4 EPA 5035A/5030B EPA 8260D
92672500005 781504 781517SOIL-A EPA 5035A/5030B EPA 8260D
92672500006 781504 781517SOIL-B EPA 5035A/5030B EPA 8260D
92672500007 781504 781517SOIL-C EPA 5035A/5030B EPA 8260D
92672500008 781504 781517SOIL-D EPA 5035A/5030B EPA 8260D
92672500009 781504 781517SOIL-E EPA 5035A/5030B EPA 8260D
92672500001 780893SOIL-D-1 SW-846
92672500002 780828SOIL-D-2 SW-846
92672500003 780893SOIL-D-3 SW-846
92672500004 780893SOIL-D-4 SW-846
92672500005 780828SOIL-A SW-846
92672500006 780844SOIL-B SW-846
92672500007 780844SOIL-C SW-846
92672500008 780844SOIL-D SW-846
92672500009 780893SOIL-E SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 05:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
June 26, 2023
Matthew Brainard
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: One Stop 15
Client Job Number:
Project Number: 92672500
Laboratory Work Order Number: 23F2482
Enclosed are results of analyses for samples as received by the laboratory on June 20, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
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Sample Summary 3
Case Narrative 4
Sample Results 5
23F2482-01 5
23F2482-02 7
23F2482-03 9
23F2482-04 11
23F2482-05 13
23F2482-06 15
23F2482-07 17
23F2482-08 19
23F2482-09 21
Sample Preparation Information 23
QC Data 24
Petroleum Hydrocarbons Analyses - VPH 24
B343927 24
Flag/Qualifier Summary 26
Certifications 27
Chain of Custody/Sample Receipt 28
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ANALYTICAL SUMMARY
6/26/2023
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
ATTN: Matthew Brainard
92672500
23F2482
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
One Stop 15
SOIL-D-1 23F2482-01 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-D-2 23F2482-02 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-D-3 23F2482-03 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-D-4 23F2482-04 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-A 23F2482-05 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-B 23F2482-06 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-C 23F2482-07 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-D 23F2482-08 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-E 23F2482-09 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
[TOC_1]Sample Summary[TOC]
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CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
MADEP-VPH-Feb 2018 Rev 2.1
Qualifications:
Soil/methanol ratio does not meet method specifications. Insufficient amount of soil. Data validation is not affected since a sufficient amount
of preservative is present. Detection limits may be above useful levels.
Analyte & Samples(s) Qualified:
O-02
23F2482-05[SOIL-A], 23F2482-06[SOIL-B], 23F2482-07[SOIL-C], 23F2482-08[SOIL-D], 23F2482-09[SOIL-E]
For VPH analysis, the average of the three marker compounds passes criteria.
Analyte & Samples(s) Qualified:
V-37
Butylcyclohexane
S089561-CCV1, S089561-CCV2
SM 2540G
Qualifications:
Sample received by laboratory with insufficient time remaining to perform analysis within the recommended holding time.
Analyte & Samples(s) Qualified:
H-09
% Solids
23F2482-01[SOIL-D-1], 23F2482-02[SOIL-D-2], 23F2482-03[SOIL-D-3], 23F2482-04[SOIL-D-4], 23F2482-05[SOIL-A], 23F2482-06[SOIL-B], 23F2482-07[SOIL-C],
23F2482-08[SOIL-D], 23F2482-09[SOIL-E]
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-01
Field Sample #: SOIL-D-1
Sample Matrix: Soil
Sampled: 6/13/2023 11:40
[TOC_2]23F2482-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.07
Petroleum Hydrocarbons Analyses - VPH
ND 14 6/21/23 20:26 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 14 6/21/23 20:26 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 14 6/21/23 20:26 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 14 6/21/23 20:26 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 14 6/21/23 20:26 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)112 6/21/23 20:2670-130
2,5-Dibromotoluene (PID)118 6/21/23 20:2670-130
[TOC_1]Sample Results[TOC]
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-01
Field Sample #: SOIL-D-1
Sample Matrix: Soil
Sampled: 6/13/2023 11:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
78.9 6/22/23 6:10 WDC% Wt 6/22/23SM 2540G1H-09% Solids
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-02
Field Sample #: SOIL-D-2
Sample Matrix: Soil
Sampled: 6/13/2023 11:45
[TOC_2]23F2482-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 0.70
Petroleum Hydrocarbons Analyses - VPH
ND 18 6/21/23 21:04 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 18 6/21/23 21:04 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 18 6/21/23 21:04 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 18 6/21/23 21:04 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 18 6/21/23 21:04 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)110 6/21/23 21:0470-130
2,5-Dibromotoluene (PID)112 6/21/23 21:0470-130
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-02
Field Sample #: SOIL-D-2
Sample Matrix: Soil
Sampled: 6/13/2023 11:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
85.4 6/22/23 6:10 WDC% Wt 6/22/23SM 2540G1H-09% Solids
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-03
Field Sample #: SOIL-D-3
Sample Matrix: Soil
Sampled: 6/13/2023 12:35
[TOC_2]23F2482-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 0.79
Petroleum Hydrocarbons Analyses - VPH
ND 14 6/21/23 21:43 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 14 6/21/23 21:43 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 14 6/21/23 21:43 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 14 6/21/23 21:43 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 14 6/21/23 21:43 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)119 6/21/23 21:4370-130
2,5-Dibromotoluene (PID)120 6/21/23 21:4370-130
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-03
Field Sample #: SOIL-D-3
Sample Matrix: Soil
Sampled: 6/13/2023 12:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
92.6 6/22/23 6:10 WDC% Wt 6/22/23SM 2540G1H-09% Solids
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-04
Field Sample #: SOIL-D-4
Sample Matrix: Soil
Sampled: 6/13/2023 12:45
[TOC_2]23F2482-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 0.93
Petroleum Hydrocarbons Analyses - VPH
ND 13 6/22/23 1:33 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 13 6/22/23 1:33 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 13 6/22/23 1:33 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 13 6/22/23 1:33 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 13 6/22/23 1:33 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)118 6/22/23 1:3370-130
2,5-Dibromotoluene (PID)119 6/22/23 1:3370-130
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-04
Field Sample #: SOIL-D-4
Sample Matrix: Soil
Sampled: 6/13/2023 12:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
91.4 6/22/23 6:10 WDC% Wt 6/22/23SM 2540G1H-09% Solids
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-05
Field Sample #: SOIL-A
Sample Matrix: Soil
Sampled: 6/13/2023 14:00
[TOC_2]23F2482-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-02
Soil/Methanol Preservation Ratio: 0.57
Petroleum Hydrocarbons Analyses - VPH
ND 21 6/21/23 22:21 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 21 6/21/23 22:21 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 21 6/21/23 22:21 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 21 6/21/23 22:21 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 21 6/21/23 22:21 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)114 6/21/23 22:2170-130
2,5-Dibromotoluene (PID)114 6/21/23 22:2170-130
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-05
Field Sample #: SOIL-A
Sample Matrix: Soil
Sampled: 6/13/2023 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
88.2 6/22/23 6:10 WDC% Wt 6/22/23SM 2540G1H-09% Solids
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-06
Field Sample #: SOIL-B
Sample Matrix: Soil
Sampled: 6/13/2023 14:15
[TOC_2]23F2482-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-02
Soil/Methanol Preservation Ratio: 0.70
Petroleum Hydrocarbons Analyses - VPH
ND 22 6/21/23 22:59 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 22 6/21/23 22:59 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 22 6/21/23 22:59 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 22 6/21/23 22:59 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 22 6/21/23 22:59 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)113 6/21/23 22:5970-130
2,5-Dibromotoluene (PID)119 6/21/23 22:5970-130
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-06
Field Sample #: SOIL-B
Sample Matrix: Soil
Sampled: 6/13/2023 14:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
76.6 6/22/23 6:10 WDC% Wt 6/22/23SM 2540G1H-09% Solids
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-07
Field Sample #: SOIL-C
Sample Matrix: Soil
Sampled: 6/13/2023 14:30
[TOC_2]23F2482-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-02
Soil/Methanol Preservation Ratio: 0.68
Petroleum Hydrocarbons Analyses - VPH
ND 22 6/21/23 23:38 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 22 6/21/23 23:38 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 22 6/21/23 23:38 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 22 6/21/23 23:38 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 22 6/21/23 23:38 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)115 6/21/23 23:3870-130
2,5-Dibromotoluene (PID)120 6/21/23 23:3870-130
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-07
Field Sample #: SOIL-C
Sample Matrix: Soil
Sampled: 6/13/2023 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
77.1 6/22/23 6:10 WDC% Wt 6/22/23SM 2540G1H-09% Solids
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-08
Field Sample #: SOIL-D
Sample Matrix: Soil
Sampled: 6/13/2023 14:40
[TOC_2]23F2482-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-02
Soil/Methanol Preservation Ratio: 0.67
Petroleum Hydrocarbons Analyses - VPH
ND 22 6/22/23 0:16 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 22 6/22/23 0:16 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 22 6/22/23 0:16 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 22 6/22/23 0:16 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 22 6/22/23 0:16 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)107 6/22/23 0:1670-130
2,5-Dibromotoluene (PID)114 6/22/23 0:1670-130
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-08
Field Sample #: SOIL-D
Sample Matrix: Soil
Sampled: 6/13/2023 14:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
78.3 6/22/23 6:10 WDC% Wt 6/22/23SM 2540G1H-09% Solids
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-09
Field Sample #: SOIL-E
Sample Matrix: Soil
Sampled: 6/13/2023 14:55
[TOC_2]23F2482-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-02
Soil/Methanol Preservation Ratio: 0.66
Petroleum Hydrocarbons Analyses - VPH
ND 21 6/22/23 0:54 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 21 6/22/23 0:54 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 21 6/22/23 0:54 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 21 6/22/23 0:54 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 21 6/22/23 0:54 EEHmg/Kg dry 6/21/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)112 6/22/23 0:5470-130
2,5-Dibromotoluene (PID)118 6/22/23 0:5470-130
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Date Received: 6/20/2023
Work Order: 23F2482Sample Description:Project Location: One Stop 15
Sample ID: 23F2482-09
Field Sample #: SOIL-E
Sample Matrix: Soil
Sampled: 6/13/2023 14:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
82.6 6/22/23 6:10 WDC% Wt 6/22/23SM 2540G1H-09% Solids
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Sample Extraction Data
Prep Method:MA VPH Analytical Method:MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B343927 06/21/2310.7 12.323F2482-01 [SOIL-D-1]
B343927 06/21/237.01 11.023F2482-02 [SOIL-D-2]
B343927 06/21/237.91 10.623F2482-03 [SOIL-D-3]
B343927 06/21/239.27 10.823F2482-04 [SOIL-D-4]
B343927 06/21/235.71 10.723F2482-05 [SOIL-A]
B343927 06/21/236.96 11.623F2482-06 [SOIL-B]
B343927 06/21/236.75 11.623F2482-07 [SOIL-C]
B343927 06/21/236.74 11.523F2482-08 [SOIL-D]
B343927 06/21/236.57 11.123F2482-09 [SOIL-E]
Prep Method:% Solids Analytical Method:SM 2540G
Lab Number [Field ID]Batch Date
B344000 06/22/2323F2482-01 [SOIL-D-1]
B344000 06/22/2323F2482-02 [SOIL-D-2]
B344000 06/22/2323F2482-03 [SOIL-D-3]
B344000 06/22/2323F2482-04 [SOIL-D-4]
B344000 06/22/2323F2482-05 [SOIL-A]
B344000 06/22/2323F2482-06 [SOIL-B]
B344000 06/22/2323F2482-07 [SOIL-C]
B344000 06/22/2323F2482-08 [SOIL-D]
B344000 06/22/2323F2482-09 [SOIL-E]
[TOC_1]Sample Preparation Information[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B343927 - MA VPH
[TOC_3]B343927[TOC]
Blank (B343927-BLK1) Prepared & Analyzed: 06/21/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)11445.8
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)12349.1
LCS (B343927-BS1) Prepared & Analyzed: 06/21/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 70-13076.55.74
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 70-1301108.21
C9-C10 Aromatics mg/Kg wet10 2.50 70-13081.52.04
Benzene mg/Kg wet0.050 2.50 70-13096.52.41
Butylcyclohexane mg/Kg wet0.050 2.50 70-1301182.94
Decane mg/Kg wet0.050 2.50 70-13093.02.32
Ethylbenzene mg/Kg wet0.050 2.50 70-13084.82.12
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 70-13080.72.02
2-Methylpentane mg/Kg wet0.050 2.50 70-13072.01.80
Naphthalene mg/Kg wet0.50 2.50 70-1301162.90
Nonane mg/Kg wet0.050 2.50 30-1301182.95
Pentane mg/Kg wet0.050 2.50 70-13083.42.09
Toluene mg/Kg wet0.050 2.50 70-13083.22.08
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 70-13081.52.04
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 70-13074.21.86
m+p Xylene mg/Kg wet0.10 5.00 70-13085.04.25
o-Xylene mg/Kg wet0.050 2.50 70-13086.82.17
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12650.4
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)12951.4
[TOC_1]QC Data[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B343927 - MA VPH
LCS Dup (B343927-BSD1) Prepared & Analyzed: 06/21/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 2570-13084.7 10.26.36
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 2570-130110 0.2458.23
C9-C10 Aromatics mg/Kg wet10 2.50 2570-13082.6 1.372.07
Benzene mg/Kg wet0.050 2.50 2570-13097.8 1.342.44
Butylcyclohexane mg/Kg wet0.050 2.50 2570-130119 1.022.97
Decane mg/Kg wet0.050 2.50 2570-13094.7 1.822.37
Ethylbenzene mg/Kg wet0.050 2.50 2570-13086.9 2.482.17
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 2570-13086.5 6.982.16
2-Methylpentane mg/Kg wet0.050 2.50 2570-13076.5 6.081.91
Naphthalene mg/Kg wet0.50 2.50 2570-130110 5.282.75
Nonane mg/Kg wet0.050 2.50 2530-130116 1.812.89
Pentane mg/Kg wet0.050 2.50 2570-13099.0 17.02.47
Toluene mg/Kg wet0.050 2.50 2570-13086.4 3.802.16
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 2570-13082.6 1.372.07
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 2570-13078.8 5.961.97
m+p Xylene mg/Kg wet0.10 5.00 2570-13086.7 2.044.34
o-Xylene mg/Kg wet0.050 2.50 2570-13088.7 2.162.22
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12048.2
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)12248.6
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Sample received by laboratory with insufficient time remaining to perform analysis within the recommended
holding time.
H-09
Soil/methanol ratio does not meet method specifications. Insufficient amount of soil. Data validation is not
affected since a sufficient amount of preservative is present. Detection limits may be above useful levels.
O-02
For VPH analysis, the average of the three marker compounds passes criteria.V-37
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2025
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023
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#=CL#
August 16, 2023
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92680269
92680269
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
105 Charlotte Highway
Asheville, NC 28803
ONE STOP 15
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on August 02, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 81
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92680269
ONE STOP 15
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 81
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92680269
ONE STOP 15
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92680269001 SOIL-F MADEP EPH 7 PASI-CBAJ
EPA 8270E 72 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92680269002 SOIL-G MADEP EPH 7 PASI-CBAJ
EPA 8270E 72 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92680269003 SOIL-H MADEP EPH 7 PASI-CBAJ
EPA 8270E 72 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92680269004 SOIL-I MADEP EPH 7 PASI-CBAJ
EPA 8270E 72 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92680269005 SOIL-J MADEP EPH 7 PASI-CBAJ
EPA 8270E 72 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-F Lab ID:92680269001 Collected:08/01/23 13:30 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)37.6 mg/kg 08/09/23 19:26 N208/07/23 16:3712.3 1
Aliphatic (C19-C36)ND mg/kg 08/09/23 19:26 N208/07/23 16:3712.3 1
Aromatic (C11-C22)27.2 mg/kg 08/09/23 19:26 N208/07/23 16:3712.3 1
Surrogates
1-Chlorooctadecane (S)86 %08/09/23 19:26 3386-33-208/07/23 16:3740-140 1
o-Terphenyl (S)63 %08/09/23 19:26 84-15-108/07/23 16:3740-140 1
2-Fluorobiphenyl (S)102 %08/09/23 19:26 321-60-808/07/23 16:3740-140 1
2-Bromonaphthalene (S)104 %08/09/23 19:26 580-13-208/07/23 16:3740-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/09/23 10:11 83-32-908/07/23 13:360.41 1
Acenaphthylene ND mg/kg 08/09/23 10:11 208-96-808/07/23 13:360.41 1
Anthracene ND mg/kg 08/09/23 10:11 120-12-708/07/23 13:360.41 1
Benzo(a)anthracene ND mg/kg 08/09/23 10:11 56-55-308/07/23 13:360.41 1
Benzo(a)pyrene ND mg/kg 08/09/23 10:11 50-32-808/07/23 13:360.41 1
Benzo(b)fluoranthene ND mg/kg 08/09/23 10:11 205-99-208/07/23 13:360.41 1
Benzo(g,h,i)perylene ND mg/kg 08/09/23 10:11 191-24-208/07/23 13:360.41 1
Benzo(k)fluoranthene ND mg/kg 08/09/23 10:11 207-08-908/07/23 13:360.41 1
Benzoic Acid ND mg/kg 08/09/23 10:11 65-85-008/07/23 13:362.0 1
Benzyl alcohol ND mg/kg 08/09/23 10:11 100-51-608/07/23 13:360.82 1
4-Bromophenylphenyl ether ND mg/kg 08/09/23 10:11 101-55-308/07/23 13:360.41 1
Butylbenzylphthalate ND mg/kg 08/09/23 10:11 85-68-708/07/23 13:360.41 1
4-Chloro-3-methylphenol ND mg/kg 08/09/23 10:11 59-50-708/07/23 13:360.82 1
4-Chloroaniline ND mg/kg 08/09/23 10:11 106-47-808/07/23 13:360.82 1
bis(2-Chloroethoxy)methane ND mg/kg 08/09/23 10:11 111-91-108/07/23 13:360.41 1
bis(2-Chloroethyl) ether ND mg/kg 08/09/23 10:11 111-44-408/07/23 13:360.41 1
2-Chloronaphthalene ND mg/kg 08/09/23 10:11 91-58-708/07/23 13:360.41 1
2-Chlorophenol ND mg/kg 08/09/23 10:11 95-57-808/07/23 13:360.41 1
4-Chlorophenylphenyl ether ND mg/kg 08/09/23 10:11 7005-72-308/07/23 13:360.41 1
Chrysene ND mg/kg 08/09/23 10:11 218-01-908/07/23 13:360.41 1
Dibenz(a,h)anthracene ND mg/kg 08/09/23 10:11 53-70-308/07/23 13:360.41 1
Dibenzofuran ND mg/kg 08/09/23 10:11 132-64-908/07/23 13:360.41 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 10:11 95-50-108/07/23 13:360.41 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 10:11 541-73-108/07/23 13:360.41 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 10:11 106-46-708/07/23 13:360.41 1
3,3'-Dichlorobenzidine ND mg/kg 08/09/23 10:11 91-94-108/07/23 13:360.82 1
2,4-Dichlorophenol ND mg/kg 08/09/23 10:11 120-83-208/07/23 13:360.41 1
Diethylphthalate ND mg/kg 08/09/23 10:11 84-66-208/07/23 13:360.41 1
2,4-Dimethylphenol ND mg/kg 08/09/23 10:11 105-67-908/07/23 13:360.41 1
Dimethylphthalate ND mg/kg 08/09/23 10:11 131-11-308/07/23 13:360.41 1
Di-n-butylphthalate ND mg/kg 08/09/23 10:11 84-74-208/07/23 13:360.41 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/09/23 10:11 534-52-108/07/23 13:360.82 1
2,4-Dinitrophenol ND mg/kg 08/09/23 10:11 51-28-508/07/23 13:362.0 1
2,4-Dinitrotoluene ND mg/kg 08/09/23 10:11 121-14-208/07/23 13:360.41 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-F Lab ID:92680269001 Collected:08/01/23 13:30 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,6-Dinitrotoluene ND mg/kg 08/09/23 10:11 606-20-208/07/23 13:360.41 1
Di-n-octylphthalate ND mg/kg 08/09/23 10:11 117-84-008/07/23 13:360.41 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/09/23 10:11 117-81-708/07/23 13:360.41 1
Fluoranthene ND mg/kg 08/09/23 10:11 206-44-008/07/23 13:360.41 1
Fluorene ND mg/kg 08/09/23 10:11 86-73-708/07/23 13:360.41 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 10:11 87-68-308/07/23 13:360.41 1
Hexachlorobenzene ND mg/kg 08/09/23 10:11 118-74-108/07/23 13:360.41 1
Hexachlorocyclopentadiene ND mg/kg 08/09/23 10:11 77-47-408/07/23 13:360.41 1
Hexachloroethane ND mg/kg 08/09/23 10:11 67-72-108/07/23 13:360.41 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/09/23 10:11 193-39-508/07/23 13:360.41 1
Isophorone ND mg/kg 08/09/23 10:11 78-59-108/07/23 13:360.41 1
1-Methylnaphthalene 0.91 mg/kg 08/09/23 10:11 90-12-008/07/23 13:360.41 1
2-Methylnaphthalene 2.2 mg/kg 08/09/23 10:11 91-57-608/07/23 13:360.41 1
2-Methylphenol(o-Cresol)ND mg/kg 08/09/23 10:11 95-48-708/07/23 13:360.41 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/09/23 10:11 15831-10-408/07/23 13:360.41 1
Naphthalene 3.2 mg/kg 08/09/23 10:11 91-20-308/07/23 13:360.41 1
2-Nitroaniline ND mg/kg 08/09/23 10:11 88-74-408/07/23 13:362.0 1
3-Nitroaniline ND mg/kg 08/09/23 10:11 99-09-208/07/23 13:362.0 1
4-Nitroaniline ND mg/kg 08/09/23 10:11 100-01-608/07/23 13:360.82 1
Nitrobenzene ND mg/kg 08/09/23 10:11 98-95-308/07/23 13:360.41 1
2-Nitrophenol ND mg/kg 08/09/23 10:11 88-75-508/07/23 13:360.41 1
4-Nitrophenol ND mg/kg 08/09/23 10:11 100-02-708/07/23 13:362.0 1
N-Nitrosodimethylamine ND mg/kg 08/09/23 10:11 62-75-908/07/23 13:360.41 1
N-Nitroso-di-n-propylamine ND mg/kg 08/09/23 10:11 621-64-708/07/23 13:360.41 1
N-Nitrosodiphenylamine ND mg/kg 08/09/23 10:11 86-30-608/07/23 13:360.41 1
Pentachlorophenol ND mg/kg 08/09/23 10:11 87-86-508/07/23 13:360.82 1
Phenanthrene ND mg/kg 08/09/23 10:11 85-01-808/07/23 13:360.41 1
Phenol ND mg/kg 08/09/23 10:11 108-95-208/07/23 13:360.41 1
Pyrene ND mg/kg 08/09/23 10:11 129-00-008/07/23 13:360.41 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 10:11 120-82-108/07/23 13:360.41 1
2,4,5-Trichlorophenol ND mg/kg 08/09/23 10:11 95-95-408/07/23 13:360.41 1
2,4,6-Trichlorophenol ND mg/kg 08/09/23 10:11 88-06-208/07/23 13:360.41 1
Surrogates
Nitrobenzene-d5 (S)48 %08/09/23 10:11 4165-60-008/07/23 13:3610-130 1
2-Fluorobiphenyl (S)45 %08/09/23 10:11 321-60-808/07/23 13:3610-130 1
Terphenyl-d14 (S)44 %08/09/23 10:11 1718-51-008/07/23 13:3610-130 1
Phenol-d6 (S)47 %08/09/23 10:11 13127-88-308/07/23 13:3610-130 1
2-Fluorophenol (S)54 %08/09/23 10:11 367-12-408/07/23 13:3610-130 1
2,4,6-Tribromophenol (S)54 %08/09/23 10:11 118-79-608/07/23 13:3610-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/08/23 19:59 67-64-108/07/23 16:280.85 5
Benzene 0.29 mg/kg 08/08/23 19:59 71-43-208/07/23 16:280.042 5
Bromobenzene ND mg/kg 08/08/23 19:59 108-86-108/07/23 16:280.042 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-F Lab ID:92680269001 Collected:08/01/23 13:30 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Bromochloromethane ND mg/kg 08/08/23 19:59 74-97-508/07/23 16:280.042 5
Bromodichloromethane ND mg/kg 08/08/23 19:59 75-27-408/07/23 16:280.042 5
Bromoform ND mg/kg 08/08/23 19:59 75-25-208/07/23 16:280.042 5
Bromomethane ND mg/kg 08/08/23 19:59 74-83-908/07/23 16:280.17 5
2-Butanone (MEK)ND mg/kg 08/08/23 19:59 78-93-308/07/23 16:280.85 5
n-Butylbenzene ND mg/kg 08/08/23 19:59 104-51-808/07/23 16:280.042 5
sec-Butylbenzene ND mg/kg 08/08/23 19:59 135-98-808/07/23 16:280.042 5
tert-Butylbenzene ND mg/kg 08/08/23 19:59 98-06-608/07/23 16:280.042 5
Carbon tetrachloride ND mg/kg 08/08/23 19:59 56-23-508/07/23 16:280.042 5
Chlorobenzene ND mg/kg 08/08/23 19:59 108-90-708/07/23 16:280.042 5
Chloroethane ND mg/kg 08/08/23 19:59 75-00-308/07/23 16:280.085 5
Chloroform ND mg/kg 08/08/23 19:59 67-66-308/07/23 16:280.042 5
Chloromethane ND mg/kg 08/08/23 19:59 74-87-308/07/23 16:280.085 5
2-Chlorotoluene ND mg/kg 08/08/23 19:59 95-49-808/07/23 16:280.042 5
4-Chlorotoluene ND mg/kg 08/08/23 19:59 106-43-408/07/23 16:280.042 5
1,2-Dibromo-3-chloropropane ND mg/kg 08/08/23 19:59 96-12-808/07/23 16:280.042 5
Dibromochloromethane ND mg/kg 08/08/23 19:59 124-48-108/07/23 16:280.042 5
1,2-Dibromoethane (EDB)ND mg/kg 08/08/23 19:59 106-93-408/07/23 16:280.042 5
Dibromomethane ND mg/kg 08/08/23 19:59 74-95-308/07/23 16:280.042 5
1,2-Dichlorobenzene ND mg/kg 08/08/23 19:59 95-50-108/07/23 16:280.042 5
1,3-Dichlorobenzene ND mg/kg 08/08/23 19:59 541-73-108/07/23 16:280.042 5
1,4-Dichlorobenzene ND mg/kg 08/08/23 19:59 106-46-708/07/23 16:280.042 5
Dichlorodifluoromethane ND mg/kg 08/08/23 19:59 75-71-8 L1,v108/07/23 16:280.085 5
1,1-Dichloroethane ND mg/kg 08/08/23 19:59 75-34-308/07/23 16:280.042 5
1,2-Dichloroethane ND mg/kg 08/08/23 19:59 107-06-208/07/23 16:280.042 5
1,1-Dichloroethene ND mg/kg 08/08/23 19:59 75-35-408/07/23 16:280.042 5
cis-1,2-Dichloroethene ND mg/kg 08/08/23 19:59 156-59-208/07/23 16:280.042 5
trans-1,2-Dichloroethene ND mg/kg 08/08/23 19:59 156-60-508/07/23 16:280.042 5
1,2-Dichloropropane ND mg/kg 08/08/23 19:59 78-87-508/07/23 16:280.042 5
1,3-Dichloropropane ND mg/kg 08/08/23 19:59 142-28-908/07/23 16:280.042 5
2,2-Dichloropropane ND mg/kg 08/08/23 19:59 594-20-708/07/23 16:280.042 5
1,1-Dichloropropene ND mg/kg 08/08/23 19:59 563-58-608/07/23 16:280.042 5
cis-1,3-Dichloropropene ND mg/kg 08/08/23 19:59 10061-01-508/07/23 16:280.042 5
trans-1,3-Dichloropropene ND mg/kg 08/08/23 19:59 10061-02-608/07/23 16:280.042 5
Diisopropyl ether ND mg/kg 08/08/23 19:59 108-20-308/07/23 16:280.042 5
Ethylbenzene 8.0 mg/kg 08/08/23 19:59 100-41-408/07/23 16:280.042 5
Hexachloro-1,3-butadiene ND mg/kg 08/08/23 19:59 87-68-308/07/23 16:280.085 5
2-Hexanone ND mg/kg 08/08/23 19:59 591-78-608/07/23 16:280.42 5
Isopropylbenzene (Cumene)0.76 mg/kg 08/08/23 19:59 98-82-808/07/23 16:280.042 5
p-Isopropyltoluene ND mg/kg 08/08/23 19:59 99-87-608/07/23 16:280.042 5
Methylene Chloride 0.19 mg/kg 08/08/23 19:59 75-09-208/07/23 16:280.17 5
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/08/23 19:59 108-10-108/07/23 16:280.42 5
Methyl-tert-butyl ether ND mg/kg 08/08/23 19:59 1634-04-408/07/23 16:280.042 5
Naphthalene 6.6 mg/kg 08/08/23 19:59 91-20-308/07/23 16:280.042 5
n-Propylbenzene 3.4 mg/kg 08/08/23 19:59 103-65-108/07/23 16:280.042 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-F Lab ID:92680269001 Collected:08/01/23 13:30 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Styrene 0.68 mg/kg 08/08/23 19:59 100-42-508/07/23 16:280.042 5
1,1,1,2-Tetrachloroethane ND mg/kg 08/08/23 19:59 630-20-608/07/23 16:280.042 5
1,1,2,2-Tetrachloroethane ND mg/kg 08/08/23 19:59 79-34-508/07/23 16:280.042 5
Tetrachloroethene ND mg/kg 08/08/23 19:59 127-18-408/07/23 16:280.042 5
Toluene 9.9 mg/kg 08/08/23 19:59 108-88-308/07/23 16:280.042 5
1,2,3-Trichlorobenzene ND mg/kg 08/08/23 19:59 87-61-608/07/23 16:280.042 5
1,2,4-Trichlorobenzene ND mg/kg 08/08/23 19:59 120-82-1 IK08/07/23 16:280.042 5
1,1,1-Trichloroethane ND mg/kg 08/08/23 19:59 71-55-608/07/23 16:280.042 5
1,1,2-Trichloroethane ND mg/kg 08/08/23 19:59 79-00-508/07/23 16:280.042 5
Trichloroethene ND mg/kg 08/08/23 19:59 79-01-608/07/23 16:280.042 5
Trichlorofluoromethane ND mg/kg 08/08/23 19:59 75-69-4 v108/07/23 16:280.042 5
1,2,3-Trichloropropane ND mg/kg 08/08/23 19:59 96-18-408/07/23 16:280.042 5
1,2,4-Trimethylbenzene 26.0 mg/kg 08/08/23 19:59 95-63-608/07/23 16:280.042 5
1,3,5-Trimethylbenzene 8.4 mg/kg 08/08/23 19:59 108-67-808/07/23 16:280.042 5
Vinyl acetate ND mg/kg 08/08/23 19:59 108-05-408/07/23 16:280.42 5
Vinyl chloride ND mg/kg 08/08/23 19:59 75-01-408/07/23 16:280.085 5
Xylene (Total)43.9 mg/kg 08/08/23 19:59 1330-20-708/07/23 16:280.085 5
m&p-Xylene 30.5 mg/kg 08/08/23 19:59 179601-23-108/07/23 16:280.085 5
o-Xylene 13.4 mg/kg 08/08/23 19:59 95-47-608/07/23 16:280.042 5
Surrogates
Toluene-d8 (S)101 %08/08/23 19:59 2037-26-508/07/23 16:2870-130 5
4-Bromofluorobenzene (S)104 %08/08/23 19:59 460-00-408/07/23 16:2870-130 5
1,2-Dichloroethane-d4 (S)105 %08/08/23 19:59 17060-07-008/07/23 16:2870-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.2 %08/03/23 14:18 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-G Lab ID:92680269002 Collected:08/01/23 13:40 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 08/09/23 19:51 N208/07/23 16:3712.9 1
Aliphatic (C19-C36)ND mg/kg 08/09/23 19:51 N208/07/23 16:3712.9 1
Aromatic (C11-C22)ND mg/kg 08/09/23 19:51 N208/07/23 16:3712.9 1
Surrogates
1-Chlorooctadecane (S)68 %08/09/23 19:51 3386-33-208/07/23 16:3740-140 1
o-Terphenyl (S)61 %08/09/23 19:51 84-15-108/07/23 16:3740-140 1
2-Fluorobiphenyl (S)97 %08/09/23 19:51 321-60-808/07/23 16:3740-140 1
2-Bromonaphthalene (S)99 %08/09/23 19:51 580-13-208/07/23 16:3740-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/09/23 10:39 83-32-908/07/23 13:360.44 1
Acenaphthylene ND mg/kg 08/09/23 10:39 208-96-808/07/23 13:360.44 1
Anthracene ND mg/kg 08/09/23 10:39 120-12-708/07/23 13:360.44 1
Benzo(a)anthracene ND mg/kg 08/09/23 10:39 56-55-308/07/23 13:360.44 1
Benzo(a)pyrene ND mg/kg 08/09/23 10:39 50-32-808/07/23 13:360.44 1
Benzo(b)fluoranthene ND mg/kg 08/09/23 10:39 205-99-208/07/23 13:360.44 1
Benzo(g,h,i)perylene ND mg/kg 08/09/23 10:39 191-24-208/07/23 13:360.44 1
Benzo(k)fluoranthene ND mg/kg 08/09/23 10:39 207-08-908/07/23 13:360.44 1
Benzoic Acid ND mg/kg 08/09/23 10:39 65-85-008/07/23 13:362.2 1
Benzyl alcohol ND mg/kg 08/09/23 10:39 100-51-608/07/23 13:360.87 1
4-Bromophenylphenyl ether ND mg/kg 08/09/23 10:39 101-55-308/07/23 13:360.44 1
Butylbenzylphthalate ND mg/kg 08/09/23 10:39 85-68-708/07/23 13:360.44 1
4-Chloro-3-methylphenol ND mg/kg 08/09/23 10:39 59-50-708/07/23 13:360.87 1
4-Chloroaniline ND mg/kg 08/09/23 10:39 106-47-808/07/23 13:360.87 1
bis(2-Chloroethoxy)methane ND mg/kg 08/09/23 10:39 111-91-108/07/23 13:360.44 1
bis(2-Chloroethyl) ether ND mg/kg 08/09/23 10:39 111-44-408/07/23 13:360.44 1
2-Chloronaphthalene ND mg/kg 08/09/23 10:39 91-58-708/07/23 13:360.44 1
2-Chlorophenol ND mg/kg 08/09/23 10:39 95-57-808/07/23 13:360.44 1
4-Chlorophenylphenyl ether ND mg/kg 08/09/23 10:39 7005-72-308/07/23 13:360.44 1
Chrysene ND mg/kg 08/09/23 10:39 218-01-908/07/23 13:360.44 1
Dibenz(a,h)anthracene ND mg/kg 08/09/23 10:39 53-70-308/07/23 13:360.44 1
Dibenzofuran ND mg/kg 08/09/23 10:39 132-64-908/07/23 13:360.44 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 10:39 95-50-108/07/23 13:360.44 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 10:39 541-73-108/07/23 13:360.44 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 10:39 106-46-708/07/23 13:360.44 1
3,3'-Dichlorobenzidine ND mg/kg 08/09/23 10:39 91-94-108/07/23 13:360.87 1
2,4-Dichlorophenol ND mg/kg 08/09/23 10:39 120-83-208/07/23 13:360.44 1
Diethylphthalate ND mg/kg 08/09/23 10:39 84-66-208/07/23 13:360.44 1
2,4-Dimethylphenol ND mg/kg 08/09/23 10:39 105-67-908/07/23 13:360.44 1
Dimethylphthalate ND mg/kg 08/09/23 10:39 131-11-308/07/23 13:360.44 1
Di-n-butylphthalate ND mg/kg 08/09/23 10:39 84-74-208/07/23 13:360.44 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/09/23 10:39 534-52-108/07/23 13:360.87 1
2,4-Dinitrophenol ND mg/kg 08/09/23 10:39 51-28-508/07/23 13:362.2 1
2,4-Dinitrotoluene ND mg/kg 08/09/23 10:39 121-14-208/07/23 13:360.44 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-G Lab ID:92680269002 Collected:08/01/23 13:40 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,6-Dinitrotoluene ND mg/kg 08/09/23 10:39 606-20-208/07/23 13:360.44 1
Di-n-octylphthalate ND mg/kg 08/09/23 10:39 117-84-008/07/23 13:360.44 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/09/23 10:39 117-81-708/07/23 13:360.44 1
Fluoranthene ND mg/kg 08/09/23 10:39 206-44-008/07/23 13:360.44 1
Fluorene ND mg/kg 08/09/23 10:39 86-73-708/07/23 13:360.44 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 10:39 87-68-308/07/23 13:360.44 1
Hexachlorobenzene ND mg/kg 08/09/23 10:39 118-74-108/07/23 13:360.44 1
Hexachlorocyclopentadiene ND mg/kg 08/09/23 10:39 77-47-408/07/23 13:360.44 1
Hexachloroethane ND mg/kg 08/09/23 10:39 67-72-108/07/23 13:360.44 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/09/23 10:39 193-39-508/07/23 13:360.44 1
Isophorone ND mg/kg 08/09/23 10:39 78-59-108/07/23 13:360.44 1
1-Methylnaphthalene ND mg/kg 08/09/23 10:39 90-12-008/07/23 13:360.44 1
2-Methylnaphthalene ND mg/kg 08/09/23 10:39 91-57-608/07/23 13:360.44 1
2-Methylphenol(o-Cresol)ND mg/kg 08/09/23 10:39 95-48-708/07/23 13:360.44 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/09/23 10:39 15831-10-408/07/23 13:360.44 1
Naphthalene ND mg/kg 08/09/23 10:39 91-20-308/07/23 13:360.44 1
2-Nitroaniline ND mg/kg 08/09/23 10:39 88-74-408/07/23 13:362.2 1
3-Nitroaniline ND mg/kg 08/09/23 10:39 99-09-208/07/23 13:362.2 1
4-Nitroaniline ND mg/kg 08/09/23 10:39 100-01-608/07/23 13:360.87 1
Nitrobenzene ND mg/kg 08/09/23 10:39 98-95-308/07/23 13:360.44 1
2-Nitrophenol ND mg/kg 08/09/23 10:39 88-75-508/07/23 13:360.44 1
4-Nitrophenol ND mg/kg 08/09/23 10:39 100-02-708/07/23 13:362.2 1
N-Nitrosodimethylamine ND mg/kg 08/09/23 10:39 62-75-908/07/23 13:360.44 1
N-Nitroso-di-n-propylamine ND mg/kg 08/09/23 10:39 621-64-708/07/23 13:360.44 1
N-Nitrosodiphenylamine ND mg/kg 08/09/23 10:39 86-30-608/07/23 13:360.44 1
Pentachlorophenol ND mg/kg 08/09/23 10:39 87-86-508/07/23 13:360.87 1
Phenanthrene ND mg/kg 08/09/23 10:39 85-01-808/07/23 13:360.44 1
Phenol ND mg/kg 08/09/23 10:39 108-95-208/07/23 13:360.44 1
Pyrene ND mg/kg 08/09/23 10:39 129-00-008/07/23 13:360.44 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 10:39 120-82-108/07/23 13:360.44 1
2,4,5-Trichlorophenol ND mg/kg 08/09/23 10:39 95-95-408/07/23 13:360.44 1
2,4,6-Trichlorophenol ND mg/kg 08/09/23 10:39 88-06-208/07/23 13:360.44 1
Surrogates
Nitrobenzene-d5 (S)63 %08/09/23 10:39 4165-60-008/07/23 13:3610-130 1
2-Fluorobiphenyl (S)27 %08/09/23 10:39 321-60-808/07/23 13:3610-130 1
Terphenyl-d14 (S)23 %08/09/23 10:39 1718-51-008/07/23 13:3610-130 1
Phenol-d6 (S)65 %08/09/23 10:39 13127-88-308/07/23 13:3610-130 1
2-Fluorophenol (S)68 %08/09/23 10:39 367-12-408/07/23 13:3610-130 1
2,4,6-Tribromophenol (S)59 %08/09/23 10:39 118-79-608/07/23 13:3610-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/04/23 20:55 67-64-108/03/23 17:470.20 1
Benzene 0.012 mg/kg 08/04/23 20:55 71-43-208/03/23 17:470.0098 1
Bromobenzene ND mg/kg 08/04/23 20:55 108-86-108/03/23 17:470.0098 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-G Lab ID:92680269002 Collected:08/01/23 13:40 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Bromochloromethane ND mg/kg 08/04/23 20:55 74-97-508/03/23 17:470.0098 1
Bromodichloromethane ND mg/kg 08/04/23 20:55 75-27-408/03/23 17:470.0098 1
Bromoform ND mg/kg 08/04/23 20:55 75-25-208/03/23 17:470.0098 1
Bromomethane ND mg/kg 08/04/23 20:55 74-83-908/03/23 17:470.039 1
2-Butanone (MEK)ND mg/kg 08/04/23 20:55 78-93-308/03/23 17:470.20 1
n-Butylbenzene ND mg/kg 08/04/23 20:55 104-51-808/03/23 17:470.0098 1
sec-Butylbenzene ND mg/kg 08/04/23 20:55 135-98-808/03/23 17:470.0098 1
tert-Butylbenzene ND mg/kg 08/04/23 20:55 98-06-6 v208/03/23 17:470.0098 1
Carbon tetrachloride ND mg/kg 08/04/23 20:55 56-23-508/03/23 17:470.0098 1
Chlorobenzene ND mg/kg 08/04/23 20:55 108-90-708/03/23 17:470.0098 1
Chloroethane ND mg/kg 08/04/23 20:55 75-00-308/03/23 17:470.020 1
Chloroform ND mg/kg 08/04/23 20:55 67-66-308/03/23 17:470.0098 1
Chloromethane ND mg/kg 08/04/23 20:55 74-87-308/03/23 17:470.020 1
2-Chlorotoluene ND mg/kg 08/04/23 20:55 95-49-808/03/23 17:470.0098 1
4-Chlorotoluene ND mg/kg 08/04/23 20:55 106-43-408/03/23 17:470.0098 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/04/23 20:55 96-12-8 IK08/03/23 17:470.0098 1
Dibromochloromethane ND mg/kg 08/04/23 20:55 124-48-108/03/23 17:470.0098 1
1,2-Dibromoethane (EDB)ND mg/kg 08/04/23 20:55 106-93-408/03/23 17:470.0098 1
Dibromomethane ND mg/kg 08/04/23 20:55 74-95-308/03/23 17:470.0098 1
1,2-Dichlorobenzene ND mg/kg 08/04/23 20:55 95-50-108/03/23 17:470.0098 1
1,3-Dichlorobenzene ND mg/kg 08/04/23 20:55 541-73-108/03/23 17:470.0098 1
1,4-Dichlorobenzene ND mg/kg 08/04/23 20:55 106-46-708/03/23 17:470.0098 1
Dichlorodifluoromethane ND mg/kg 08/04/23 20:55 75-71-8 L1,v108/03/23 17:470.020 1
1,1-Dichloroethane ND mg/kg 08/04/23 20:55 75-34-308/03/23 17:470.0098 1
1,2-Dichloroethane ND mg/kg 08/04/23 20:55 107-06-208/03/23 17:470.0098 1
1,1-Dichloroethene ND mg/kg 08/04/23 20:55 75-35-408/03/23 17:470.0098 1
cis-1,2-Dichloroethene ND mg/kg 08/04/23 20:55 156-59-208/03/23 17:470.0098 1
trans-1,2-Dichloroethene ND mg/kg 08/04/23 20:55 156-60-508/03/23 17:470.0098 1
1,2-Dichloropropane ND mg/kg 08/04/23 20:55 78-87-508/03/23 17:470.0098 1
1,3-Dichloropropane ND mg/kg 08/04/23 20:55 142-28-908/03/23 17:470.0098 1
2,2-Dichloropropane ND mg/kg 08/04/23 20:55 594-20-708/03/23 17:470.0098 1
1,1-Dichloropropene ND mg/kg 08/04/23 20:55 563-58-608/03/23 17:470.0098 1
cis-1,3-Dichloropropene ND mg/kg 08/04/23 20:55 10061-01-508/03/23 17:470.0098 1
trans-1,3-Dichloropropene ND mg/kg 08/04/23 20:55 10061-02-608/03/23 17:470.0098 1
Diisopropyl ether ND mg/kg 08/04/23 20:55 108-20-308/03/23 17:470.0098 1
Ethylbenzene 0.21 mg/kg 08/04/23 20:55 100-41-408/03/23 17:470.0098 1
Hexachloro-1,3-butadiene ND mg/kg 08/04/23 20:55 87-68-308/03/23 17:470.020 1
2-Hexanone ND mg/kg 08/04/23 20:55 591-78-608/03/23 17:470.098 1
Isopropylbenzene (Cumene)ND mg/kg 08/04/23 20:55 98-82-808/03/23 17:470.0098 1
p-Isopropyltoluene ND mg/kg 08/04/23 20:55 99-87-608/03/23 17:470.0098 1
Methylene Chloride ND mg/kg 08/04/23 20:55 75-09-208/03/23 17:470.039 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/04/23 20:55 108-10-108/03/23 17:470.098 1
Methyl-tert-butyl ether ND mg/kg 08/04/23 20:55 1634-04-408/03/23 17:470.0098 1
Naphthalene 2.9 mg/kg 08/04/23 20:55 91-20-308/03/23 17:470.0098 1
n-Propylbenzene ND mg/kg 08/04/23 20:55 103-65-108/03/23 17:470.0098 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-G Lab ID:92680269002 Collected:08/01/23 13:40 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Styrene 0.023 mg/kg 08/04/23 20:55 100-42-508/03/23 17:470.0098 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/04/23 20:55 630-20-608/03/23 17:470.0098 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/04/23 20:55 79-34-508/03/23 17:470.0098 1
Tetrachloroethene ND mg/kg 08/04/23 20:55 127-18-408/03/23 17:470.0098 1
Toluene 0.19 mg/kg 08/04/23 20:55 108-88-308/03/23 17:470.0098 1
1,2,3-Trichlorobenzene ND mg/kg 08/04/23 20:55 87-61-608/03/23 17:470.0098 1
1,2,4-Trichlorobenzene ND mg/kg 08/04/23 20:55 120-82-108/03/23 17:470.0098 1
1,1,1-Trichloroethane ND mg/kg 08/04/23 20:55 71-55-608/03/23 17:470.0098 1
1,1,2-Trichloroethane ND mg/kg 08/04/23 20:55 79-00-508/03/23 17:470.0098 1
Trichloroethene ND mg/kg 08/04/23 20:55 79-01-608/03/23 17:470.0098 1
Trichlorofluoromethane ND mg/kg 08/04/23 20:55 75-69-408/03/23 17:470.0098 1
1,2,3-Trichloropropane ND mg/kg 08/04/23 20:55 96-18-408/03/23 17:470.0098 1
1,2,4-Trimethylbenzene 3.4 mg/kg 08/04/23 20:55 95-63-608/03/23 17:470.0098 1
1,3,5-Trimethylbenzene 1.1 mg/kg 08/04/23 20:55 108-67-808/03/23 17:470.0098 1
Vinyl acetate ND mg/kg 08/04/23 20:55 108-05-408/03/23 17:470.098 1
Vinyl chloride ND mg/kg 08/04/23 20:55 75-01-408/03/23 17:470.020 1
Xylene (Total)1.6 mg/kg 08/04/23 20:55 1330-20-708/03/23 17:470.020 1
m&p-Xylene 0.99 mg/kg 08/04/23 20:55 179601-23-108/03/23 17:470.020 1
o-Xylene 0.57 mg/kg 08/04/23 20:55 95-47-608/03/23 17:470.0098 1
Surrogates
Toluene-d8 (S)102 %08/04/23 20:55 2037-26-508/03/23 17:4770-130 1
4-Bromofluorobenzene (S)104 %08/04/23 20:55 460-00-408/03/23 17:4770-130 1
1,2-Dichloroethane-d4 (S)108 %08/04/23 20:55 17060-07-008/03/23 17:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.0 %08/03/23 14:18 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-H Lab ID:92680269003 Collected:08/01/23 15:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 08/09/23 20:17 N208/07/23 16:3712.0 1
Aliphatic (C19-C36)ND mg/kg 08/09/23 20:17 N208/07/23 16:3712.0 1
Aromatic (C11-C22)17.9 mg/kg 08/09/23 20:17 N208/07/23 16:3712.0 1
Surrogates
1-Chlorooctadecane (S)86 %08/09/23 20:17 3386-33-208/07/23 16:3740-140 1
o-Terphenyl (S)67 %08/09/23 20:17 84-15-108/07/23 16:3740-140 1
2-Fluorobiphenyl (S)112 %08/09/23 20:17 321-60-808/07/23 16:3740-140 1
2-Bromonaphthalene (S)115 %08/09/23 20:17 580-13-208/07/23 16:3740-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/09/23 08:20 83-32-908/07/23 13:360.40 1
Acenaphthylene ND mg/kg 08/09/23 08:20 208-96-808/07/23 13:360.40 1
Anthracene ND mg/kg 08/09/23 08:20 120-12-708/07/23 13:360.40 1
Benzo(a)anthracene ND mg/kg 08/09/23 08:20 56-55-308/07/23 13:360.40 1
Benzo(a)pyrene ND mg/kg 08/09/23 08:20 50-32-808/07/23 13:360.40 1
Benzo(b)fluoranthene ND mg/kg 08/09/23 08:20 205-99-208/07/23 13:360.40 1
Benzo(g,h,i)perylene ND mg/kg 08/09/23 08:20 191-24-208/07/23 13:360.40 1
Benzo(k)fluoranthene ND mg/kg 08/09/23 08:20 207-08-908/07/23 13:360.40 1
Benzoic Acid ND mg/kg 08/09/23 08:20 65-85-008/07/23 13:362.0 1
Benzyl alcohol ND mg/kg 08/09/23 08:20 100-51-608/07/23 13:360.80 1
4-Bromophenylphenyl ether ND mg/kg 08/09/23 08:20 101-55-308/07/23 13:360.40 1
Butylbenzylphthalate ND mg/kg 08/09/23 08:20 85-68-708/07/23 13:360.40 1
4-Chloro-3-methylphenol ND mg/kg 08/09/23 08:20 59-50-708/07/23 13:360.80 1
4-Chloroaniline ND mg/kg 08/09/23 08:20 106-47-808/07/23 13:360.80 1
bis(2-Chloroethoxy)methane ND mg/kg 08/09/23 08:20 111-91-108/07/23 13:360.40 1
bis(2-Chloroethyl) ether ND mg/kg 08/09/23 08:20 111-44-408/07/23 13:360.40 1
2-Chloronaphthalene ND mg/kg 08/09/23 08:20 91-58-708/07/23 13:360.40 1
2-Chlorophenol ND mg/kg 08/09/23 08:20 95-57-808/07/23 13:360.40 1
4-Chlorophenylphenyl ether ND mg/kg 08/09/23 08:20 7005-72-308/07/23 13:360.40 1
Chrysene ND mg/kg 08/09/23 08:20 218-01-908/07/23 13:360.40 1
Dibenz(a,h)anthracene ND mg/kg 08/09/23 08:20 53-70-308/07/23 13:360.40 1
Dibenzofuran ND mg/kg 08/09/23 08:20 132-64-908/07/23 13:360.40 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 08:20 95-50-108/07/23 13:360.40 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 08:20 541-73-108/07/23 13:360.40 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 08:20 106-46-708/07/23 13:360.40 1
3,3'-Dichlorobenzidine ND mg/kg 08/09/23 08:20 91-94-108/07/23 13:360.80 1
2,4-Dichlorophenol ND mg/kg 08/09/23 08:20 120-83-208/07/23 13:360.40 1
Diethylphthalate ND mg/kg 08/09/23 08:20 84-66-208/07/23 13:360.40 1
2,4-Dimethylphenol ND mg/kg 08/09/23 08:20 105-67-908/07/23 13:360.40 1
Dimethylphthalate ND mg/kg 08/09/23 08:20 131-11-308/07/23 13:360.40 1
Di-n-butylphthalate ND mg/kg 08/09/23 08:20 84-74-208/07/23 13:360.40 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/09/23 08:20 534-52-108/07/23 13:360.80 1
2,4-Dinitrophenol ND mg/kg 08/09/23 08:20 51-28-508/07/23 13:362.0 1
2,4-Dinitrotoluene ND mg/kg 08/09/23 08:20 121-14-208/07/23 13:360.40 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-H Lab ID:92680269003 Collected:08/01/23 15:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,6-Dinitrotoluene ND mg/kg 08/09/23 08:20 606-20-208/07/23 13:360.40 1
Di-n-octylphthalate ND mg/kg 08/09/23 08:20 117-84-008/07/23 13:360.40 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/09/23 08:20 117-81-708/07/23 13:360.40 1
Fluoranthene ND mg/kg 08/09/23 08:20 206-44-008/07/23 13:360.40 1
Fluorene ND mg/kg 08/09/23 08:20 86-73-708/07/23 13:360.40 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 08:20 87-68-308/07/23 13:360.40 1
Hexachlorobenzene ND mg/kg 08/09/23 08:20 118-74-108/07/23 13:360.40 1
Hexachlorocyclopentadiene ND mg/kg 08/09/23 08:20 77-47-408/07/23 13:360.40 1
Hexachloroethane ND mg/kg 08/09/23 08:20 67-72-108/07/23 13:360.40 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/09/23 08:20 193-39-508/07/23 13:360.40 1
Isophorone ND mg/kg 08/09/23 08:20 78-59-108/07/23 13:360.40 1
1-Methylnaphthalene ND mg/kg 08/09/23 08:20 90-12-008/07/23 13:360.40 1
2-Methylnaphthalene 0.50 mg/kg 08/09/23 08:20 91-57-608/07/23 13:360.40 1
2-Methylphenol(o-Cresol)ND mg/kg 08/09/23 08:20 95-48-708/07/23 13:360.40 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/09/23 08:20 15831-10-408/07/23 13:360.40 1
Naphthalene 0.57 mg/kg 08/09/23 08:20 91-20-308/07/23 13:360.40 1
2-Nitroaniline ND mg/kg 08/09/23 08:20 88-74-408/07/23 13:362.0 1
3-Nitroaniline ND mg/kg 08/09/23 08:20 99-09-208/07/23 13:362.0 1
4-Nitroaniline ND mg/kg 08/09/23 08:20 100-01-608/07/23 13:360.80 1
Nitrobenzene ND mg/kg 08/09/23 08:20 98-95-308/07/23 13:360.40 1
2-Nitrophenol ND mg/kg 08/09/23 08:20 88-75-508/07/23 13:360.40 1
4-Nitrophenol ND mg/kg 08/09/23 08:20 100-02-708/07/23 13:362.0 1
N-Nitrosodimethylamine ND mg/kg 08/09/23 08:20 62-75-908/07/23 13:360.40 1
N-Nitroso-di-n-propylamine ND mg/kg 08/09/23 08:20 621-64-708/07/23 13:360.40 1
N-Nitrosodiphenylamine ND mg/kg 08/09/23 08:20 86-30-608/07/23 13:360.40 1
Pentachlorophenol ND mg/kg 08/09/23 08:20 87-86-508/07/23 13:360.80 1
Phenanthrene ND mg/kg 08/09/23 08:20 85-01-808/07/23 13:360.40 1
Phenol ND mg/kg 08/09/23 08:20 108-95-208/07/23 13:360.40 1
Pyrene ND mg/kg 08/09/23 08:20 129-00-008/07/23 13:360.40 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 08:20 120-82-108/07/23 13:360.40 1
2,4,5-Trichlorophenol ND mg/kg 08/09/23 08:20 95-95-408/07/23 13:360.40 1
2,4,6-Trichlorophenol ND mg/kg 08/09/23 08:20 88-06-208/07/23 13:360.40 1
Surrogates
Nitrobenzene-d5 (S)52 %08/09/23 08:20 4165-60-008/07/23 13:3610-130 1
2-Fluorobiphenyl (S)46 %08/09/23 08:20 321-60-808/07/23 13:3610-130 1
Terphenyl-d14 (S)44 %08/09/23 08:20 1718-51-008/07/23 13:3610-130 1
Phenol-d6 (S)51 %08/09/23 08:20 13127-88-308/07/23 13:3610-130 1
2-Fluorophenol (S)52 %08/09/23 08:20 367-12-408/07/23 13:3610-130 1
2,4,6-Tribromophenol (S)57 %08/09/23 08:20 118-79-608/07/23 13:3610-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/04/23 20:36 67-64-108/03/23 17:470.19 1
Benzene ND mg/kg 08/04/23 20:36 71-43-208/03/23 17:470.0093 1
Bromobenzene ND mg/kg 08/04/23 20:36 108-86-108/03/23 17:470.0093 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-H Lab ID:92680269003 Collected:08/01/23 15:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Bromochloromethane ND mg/kg 08/04/23 20:36 74-97-508/03/23 17:470.0093 1
Bromodichloromethane ND mg/kg 08/04/23 20:36 75-27-408/03/23 17:470.0093 1
Bromoform ND mg/kg 08/04/23 20:36 75-25-208/03/23 17:470.0093 1
Bromomethane ND mg/kg 08/04/23 20:36 74-83-908/03/23 17:470.037 1
2-Butanone (MEK)ND mg/kg 08/04/23 20:36 78-93-308/03/23 17:470.19 1
n-Butylbenzene ND mg/kg 08/04/23 20:36 104-51-808/03/23 17:470.0093 1
sec-Butylbenzene ND mg/kg 08/04/23 20:36 135-98-808/03/23 17:470.0093 1
tert-Butylbenzene ND mg/kg 08/04/23 20:36 98-06-6 v208/03/23 17:470.0093 1
Carbon tetrachloride ND mg/kg 08/04/23 20:36 56-23-508/03/23 17:470.0093 1
Chlorobenzene ND mg/kg 08/04/23 20:36 108-90-708/03/23 17:470.0093 1
Chloroethane ND mg/kg 08/04/23 20:36 75-00-308/03/23 17:470.019 1
Chloroform ND mg/kg 08/04/23 20:36 67-66-308/03/23 17:470.0093 1
Chloromethane ND mg/kg 08/04/23 20:36 74-87-308/03/23 17:470.019 1
2-Chlorotoluene ND mg/kg 08/04/23 20:36 95-49-808/03/23 17:470.0093 1
4-Chlorotoluene ND mg/kg 08/04/23 20:36 106-43-408/03/23 17:470.0093 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/04/23 20:36 96-12-8 IK08/03/23 17:470.0093 1
Dibromochloromethane ND mg/kg 08/04/23 20:36 124-48-108/03/23 17:470.0093 1
1,2-Dibromoethane (EDB)ND mg/kg 08/04/23 20:36 106-93-408/03/23 17:470.0093 1
Dibromomethane ND mg/kg 08/04/23 20:36 74-95-308/03/23 17:470.0093 1
1,2-Dichlorobenzene ND mg/kg 08/04/23 20:36 95-50-108/03/23 17:470.0093 1
1,3-Dichlorobenzene ND mg/kg 08/04/23 20:36 541-73-108/03/23 17:470.0093 1
1,4-Dichlorobenzene ND mg/kg 08/04/23 20:36 106-46-708/03/23 17:470.0093 1
Dichlorodifluoromethane ND mg/kg 08/04/23 20:36 75-71-8 L1,v108/03/23 17:470.019 1
1,1-Dichloroethane ND mg/kg 08/04/23 20:36 75-34-308/03/23 17:470.0093 1
1,2-Dichloroethane ND mg/kg 08/04/23 20:36 107-06-208/03/23 17:470.0093 1
1,1-Dichloroethene ND mg/kg 08/04/23 20:36 75-35-408/03/23 17:470.0093 1
cis-1,2-Dichloroethene ND mg/kg 08/04/23 20:36 156-59-208/03/23 17:470.0093 1
trans-1,2-Dichloroethene ND mg/kg 08/04/23 20:36 156-60-508/03/23 17:470.0093 1
1,2-Dichloropropane ND mg/kg 08/04/23 20:36 78-87-508/03/23 17:470.0093 1
1,3-Dichloropropane ND mg/kg 08/04/23 20:36 142-28-908/03/23 17:470.0093 1
2,2-Dichloropropane ND mg/kg 08/04/23 20:36 594-20-708/03/23 17:470.0093 1
1,1-Dichloropropene ND mg/kg 08/04/23 20:36 563-58-608/03/23 17:470.0093 1
cis-1,3-Dichloropropene ND mg/kg 08/04/23 20:36 10061-01-508/03/23 17:470.0093 1
trans-1,3-Dichloropropene ND mg/kg 08/04/23 20:36 10061-02-608/03/23 17:470.0093 1
Diisopropyl ether ND mg/kg 08/04/23 20:36 108-20-308/03/23 17:470.0093 1
Ethylbenzene 0.10 mg/kg 08/04/23 20:36 100-41-408/03/23 17:470.0093 1
Hexachloro-1,3-butadiene ND mg/kg 08/04/23 20:36 87-68-308/03/23 17:470.019 1
2-Hexanone ND mg/kg 08/04/23 20:36 591-78-608/03/23 17:470.093 1
Isopropylbenzene (Cumene)ND mg/kg 08/04/23 20:36 98-82-808/03/23 17:470.0093 1
p-Isopropyltoluene ND mg/kg 08/04/23 20:36 99-87-608/03/23 17:470.0093 1
Methylene Chloride ND mg/kg 08/04/23 20:36 75-09-208/03/23 17:470.037 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/04/23 20:36 108-10-108/03/23 17:470.093 1
Methyl-tert-butyl ether ND mg/kg 08/04/23 20:36 1634-04-408/03/23 17:470.0093 1
Naphthalene 1.1 mg/kg 08/04/23 20:36 91-20-308/03/23 17:470.0093 1
n-Propylbenzene ND mg/kg 08/04/23 20:36 103-65-108/03/23 17:470.0093 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-H Lab ID:92680269003 Collected:08/01/23 15:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Styrene 0.018 mg/kg 08/04/23 20:36 100-42-508/03/23 17:470.0093 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/04/23 20:36 630-20-608/03/23 17:470.0093 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/04/23 20:36 79-34-508/03/23 17:470.0093 1
Tetrachloroethene ND mg/kg 08/04/23 20:36 127-18-408/03/23 17:470.0093 1
Toluene 0.10 mg/kg 08/04/23 20:36 108-88-308/03/23 17:470.0093 1
1,2,3-Trichlorobenzene ND mg/kg 08/04/23 20:36 87-61-608/03/23 17:470.0093 1
1,2,4-Trichlorobenzene ND mg/kg 08/04/23 20:36 120-82-108/03/23 17:470.0093 1
1,1,1-Trichloroethane ND mg/kg 08/04/23 20:36 71-55-608/03/23 17:470.0093 1
1,1,2-Trichloroethane ND mg/kg 08/04/23 20:36 79-00-508/03/23 17:470.0093 1
Trichloroethene ND mg/kg 08/04/23 20:36 79-01-608/03/23 17:470.0093 1
Trichlorofluoromethane ND mg/kg 08/04/23 20:36 75-69-408/03/23 17:470.0093 1
1,2,3-Trichloropropane ND mg/kg 08/04/23 20:36 96-18-408/03/23 17:470.0093 1
1,2,4-Trimethylbenzene 1.1 mg/kg 08/04/23 20:36 95-63-608/03/23 17:470.0093 1
1,3,5-Trimethylbenzene 0.34 mg/kg 08/04/23 20:36 108-67-808/03/23 17:470.0093 1
Vinyl acetate ND mg/kg 08/04/23 20:36 108-05-408/03/23 17:470.093 1
Vinyl chloride ND mg/kg 08/04/23 20:36 75-01-408/03/23 17:470.019 1
Xylene (Total)0.74 mg/kg 08/04/23 20:36 1330-20-708/03/23 17:470.019 1
m&p-Xylene 0.46 mg/kg 08/04/23 20:36 179601-23-108/03/23 17:470.019 1
o-Xylene 0.28 mg/kg 08/04/23 20:36 95-47-608/03/23 17:470.0093 1
Surrogates
Toluene-d8 (S)101 %08/04/23 20:36 2037-26-508/03/23 17:4770-130 1
4-Bromofluorobenzene (S)104 %08/04/23 20:36 460-00-408/03/23 17:4770-130 1
1,2-Dichloroethane-d4 (S)106 %08/04/23 20:36 17060-07-008/03/23 17:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.2 %08/03/23 14:18 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-I Lab ID:92680269004 Collected:08/01/23 16:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 08/09/23 20:42 N208/07/23 16:3712.5 1
Aliphatic (C19-C36)ND mg/kg 08/09/23 20:42 N208/07/23 16:3712.5 1
Aromatic (C11-C22)ND mg/kg 08/09/23 20:42 N208/07/23 16:3712.5 1
Surrogates
1-Chlorooctadecane (S)87 %08/09/23 20:42 3386-33-208/07/23 16:3740-140 1
o-Terphenyl (S)66 %08/09/23 20:42 84-15-108/07/23 16:3740-140 1
2-Fluorobiphenyl (S)100 %08/09/23 20:42 321-60-808/07/23 16:3740-140 1
2-Bromonaphthalene (S)99 %08/09/23 20:42 580-13-208/07/23 16:3740-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/09/23 09:15 83-32-908/07/23 13:360.41 1
Acenaphthylene ND mg/kg 08/09/23 09:15 208-96-808/07/23 13:360.41 1
Anthracene ND mg/kg 08/09/23 09:15 120-12-708/07/23 13:360.41 1
Benzo(a)anthracene ND mg/kg 08/09/23 09:15 56-55-308/07/23 13:360.41 1
Benzo(a)pyrene ND mg/kg 08/09/23 09:15 50-32-808/07/23 13:360.41 1
Benzo(b)fluoranthene ND mg/kg 08/09/23 09:15 205-99-208/07/23 13:360.41 1
Benzo(g,h,i)perylene ND mg/kg 08/09/23 09:15 191-24-208/07/23 13:360.41 1
Benzo(k)fluoranthene ND mg/kg 08/09/23 09:15 207-08-908/07/23 13:360.41 1
Benzoic Acid ND mg/kg 08/09/23 09:15 65-85-008/07/23 13:362.1 1
Benzyl alcohol ND mg/kg 08/09/23 09:15 100-51-608/07/23 13:360.83 1
4-Bromophenylphenyl ether ND mg/kg 08/09/23 09:15 101-55-308/07/23 13:360.41 1
Butylbenzylphthalate ND mg/kg 08/09/23 09:15 85-68-708/07/23 13:360.41 1
4-Chloro-3-methylphenol ND mg/kg 08/09/23 09:15 59-50-708/07/23 13:360.83 1
4-Chloroaniline ND mg/kg 08/09/23 09:15 106-47-808/07/23 13:360.83 1
bis(2-Chloroethoxy)methane ND mg/kg 08/09/23 09:15 111-91-108/07/23 13:360.41 1
bis(2-Chloroethyl) ether ND mg/kg 08/09/23 09:15 111-44-408/07/23 13:360.41 1
2-Chloronaphthalene ND mg/kg 08/09/23 09:15 91-58-708/07/23 13:360.41 1
2-Chlorophenol ND mg/kg 08/09/23 09:15 95-57-808/07/23 13:360.41 1
4-Chlorophenylphenyl ether ND mg/kg 08/09/23 09:15 7005-72-308/07/23 13:360.41 1
Chrysene ND mg/kg 08/09/23 09:15 218-01-908/07/23 13:360.41 1
Dibenz(a,h)anthracene ND mg/kg 08/09/23 09:15 53-70-308/07/23 13:360.41 1
Dibenzofuran ND mg/kg 08/09/23 09:15 132-64-908/07/23 13:360.41 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 09:15 95-50-108/07/23 13:360.41 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 09:15 541-73-108/07/23 13:360.41 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 09:15 106-46-708/07/23 13:360.41 1
3,3'-Dichlorobenzidine ND mg/kg 08/09/23 09:15 91-94-108/07/23 13:360.83 1
2,4-Dichlorophenol ND mg/kg 08/09/23 09:15 120-83-208/07/23 13:360.41 1
Diethylphthalate ND mg/kg 08/09/23 09:15 84-66-208/07/23 13:360.41 1
2,4-Dimethylphenol ND mg/kg 08/09/23 09:15 105-67-908/07/23 13:360.41 1
Dimethylphthalate ND mg/kg 08/09/23 09:15 131-11-308/07/23 13:360.41 1
Di-n-butylphthalate ND mg/kg 08/09/23 09:15 84-74-208/07/23 13:360.41 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/09/23 09:15 534-52-108/07/23 13:360.83 1
2,4-Dinitrophenol ND mg/kg 08/09/23 09:15 51-28-508/07/23 13:362.1 1
2,4-Dinitrotoluene ND mg/kg 08/09/23 09:15 121-14-208/07/23 13:360.41 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-I Lab ID:92680269004 Collected:08/01/23 16:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,6-Dinitrotoluene ND mg/kg 08/09/23 09:15 606-20-208/07/23 13:360.41 1
Di-n-octylphthalate ND mg/kg 08/09/23 09:15 117-84-008/07/23 13:360.41 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/09/23 09:15 117-81-708/07/23 13:360.41 1
Fluoranthene ND mg/kg 08/09/23 09:15 206-44-008/07/23 13:360.41 1
Fluorene ND mg/kg 08/09/23 09:15 86-73-708/07/23 13:360.41 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 09:15 87-68-308/07/23 13:360.41 1
Hexachlorobenzene ND mg/kg 08/09/23 09:15 118-74-108/07/23 13:360.41 1
Hexachlorocyclopentadiene ND mg/kg 08/09/23 09:15 77-47-408/07/23 13:360.41 1
Hexachloroethane ND mg/kg 08/09/23 09:15 67-72-108/07/23 13:360.41 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/09/23 09:15 193-39-508/07/23 13:360.41 1
Isophorone ND mg/kg 08/09/23 09:15 78-59-108/07/23 13:360.41 1
1-Methylnaphthalene ND mg/kg 08/09/23 09:15 90-12-008/07/23 13:360.41 1
2-Methylnaphthalene ND mg/kg 08/09/23 09:15 91-57-608/07/23 13:360.41 1
2-Methylphenol(o-Cresol)ND mg/kg 08/09/23 09:15 95-48-708/07/23 13:360.41 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/09/23 09:15 15831-10-408/07/23 13:360.41 1
Naphthalene ND mg/kg 08/09/23 09:15 91-20-308/07/23 13:360.41 1
2-Nitroaniline ND mg/kg 08/09/23 09:15 88-74-408/07/23 13:362.1 1
3-Nitroaniline ND mg/kg 08/09/23 09:15 99-09-208/07/23 13:362.1 1
4-Nitroaniline ND mg/kg 08/09/23 09:15 100-01-608/07/23 13:360.83 1
Nitrobenzene ND mg/kg 08/09/23 09:15 98-95-308/07/23 13:360.41 1
2-Nitrophenol ND mg/kg 08/09/23 09:15 88-75-508/07/23 13:360.41 1
4-Nitrophenol ND mg/kg 08/09/23 09:15 100-02-708/07/23 13:362.1 1
N-Nitrosodimethylamine ND mg/kg 08/09/23 09:15 62-75-908/07/23 13:360.41 1
N-Nitroso-di-n-propylamine ND mg/kg 08/09/23 09:15 621-64-708/07/23 13:360.41 1
N-Nitrosodiphenylamine ND mg/kg 08/09/23 09:15 86-30-608/07/23 13:360.41 1
Pentachlorophenol ND mg/kg 08/09/23 09:15 87-86-508/07/23 13:360.83 1
Phenanthrene ND mg/kg 08/09/23 09:15 85-01-808/07/23 13:360.41 1
Phenol ND mg/kg 08/09/23 09:15 108-95-208/07/23 13:360.41 1
Pyrene ND mg/kg 08/09/23 09:15 129-00-008/07/23 13:360.41 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 09:15 120-82-108/07/23 13:360.41 1
2,4,5-Trichlorophenol ND mg/kg 08/09/23 09:15 95-95-408/07/23 13:360.41 1
2,4,6-Trichlorophenol ND mg/kg 08/09/23 09:15 88-06-208/07/23 13:360.41 1
Surrogates
Nitrobenzene-d5 (S)49 %08/09/23 09:15 4165-60-008/07/23 13:3610-130 1
2-Fluorobiphenyl (S)44 %08/09/23 09:15 321-60-808/07/23 13:3610-130 1
Terphenyl-d14 (S)46 %08/09/23 09:15 1718-51-008/07/23 13:3610-130 1
Phenol-d6 (S)46 %08/09/23 09:15 13127-88-308/07/23 13:3610-130 1
2-Fluorophenol (S)47 %08/09/23 09:15 367-12-408/07/23 13:3610-130 1
2,4,6-Tribromophenol (S)51 %08/09/23 09:15 118-79-608/07/23 13:3610-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/04/23 20:18 67-64-108/03/23 17:470.15 1
Benzene ND mg/kg 08/04/23 20:18 71-43-208/03/23 17:470.0075 1
Bromobenzene ND mg/kg 08/04/23 20:18 108-86-108/03/23 17:470.0075 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-I Lab ID:92680269004 Collected:08/01/23 16:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Bromochloromethane ND mg/kg 08/04/23 20:18 74-97-508/03/23 17:470.0075 1
Bromodichloromethane ND mg/kg 08/04/23 20:18 75-27-408/03/23 17:470.0075 1
Bromoform ND mg/kg 08/04/23 20:18 75-25-208/03/23 17:470.0075 1
Bromomethane ND mg/kg 08/04/23 20:18 74-83-908/03/23 17:470.030 1
2-Butanone (MEK)ND mg/kg 08/04/23 20:18 78-93-308/03/23 17:470.15 1
n-Butylbenzene ND mg/kg 08/04/23 20:18 104-51-808/03/23 17:470.0075 1
sec-Butylbenzene ND mg/kg 08/04/23 20:18 135-98-808/03/23 17:470.0075 1
tert-Butylbenzene ND mg/kg 08/04/23 20:18 98-06-6 v208/03/23 17:470.0075 1
Carbon tetrachloride ND mg/kg 08/04/23 20:18 56-23-508/03/23 17:470.0075 1
Chlorobenzene ND mg/kg 08/04/23 20:18 108-90-708/03/23 17:470.0075 1
Chloroethane ND mg/kg 08/04/23 20:18 75-00-308/03/23 17:470.015 1
Chloroform ND mg/kg 08/04/23 20:18 67-66-308/03/23 17:470.0075 1
Chloromethane ND mg/kg 08/04/23 20:18 74-87-308/03/23 17:470.015 1
2-Chlorotoluene ND mg/kg 08/04/23 20:18 95-49-808/03/23 17:470.0075 1
4-Chlorotoluene ND mg/kg 08/04/23 20:18 106-43-408/03/23 17:470.0075 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/04/23 20:18 96-12-8 IK08/03/23 17:470.0075 1
Dibromochloromethane ND mg/kg 08/04/23 20:18 124-48-108/03/23 17:470.0075 1
1,2-Dibromoethane (EDB)ND mg/kg 08/04/23 20:18 106-93-408/03/23 17:470.0075 1
Dibromomethane ND mg/kg 08/04/23 20:18 74-95-308/03/23 17:470.0075 1
1,2-Dichlorobenzene ND mg/kg 08/04/23 20:18 95-50-108/03/23 17:470.0075 1
1,3-Dichlorobenzene ND mg/kg 08/04/23 20:18 541-73-108/03/23 17:470.0075 1
1,4-Dichlorobenzene ND mg/kg 08/04/23 20:18 106-46-708/03/23 17:470.0075 1
Dichlorodifluoromethane ND mg/kg 08/04/23 20:18 75-71-8 L1,v108/03/23 17:470.015 1
1,1-Dichloroethane ND mg/kg 08/04/23 20:18 75-34-308/03/23 17:470.0075 1
1,2-Dichloroethane ND mg/kg 08/04/23 20:18 107-06-208/03/23 17:470.0075 1
1,1-Dichloroethene ND mg/kg 08/04/23 20:18 75-35-408/03/23 17:470.0075 1
cis-1,2-Dichloroethene ND mg/kg 08/04/23 20:18 156-59-208/03/23 17:470.0075 1
trans-1,2-Dichloroethene ND mg/kg 08/04/23 20:18 156-60-508/03/23 17:470.0075 1
1,2-Dichloropropane ND mg/kg 08/04/23 20:18 78-87-508/03/23 17:470.0075 1
1,3-Dichloropropane ND mg/kg 08/04/23 20:18 142-28-908/03/23 17:470.0075 1
2,2-Dichloropropane ND mg/kg 08/04/23 20:18 594-20-708/03/23 17:470.0075 1
1,1-Dichloropropene ND mg/kg 08/04/23 20:18 563-58-608/03/23 17:470.0075 1
cis-1,3-Dichloropropene ND mg/kg 08/04/23 20:18 10061-01-508/03/23 17:470.0075 1
trans-1,3-Dichloropropene ND mg/kg 08/04/23 20:18 10061-02-608/03/23 17:470.0075 1
Diisopropyl ether ND mg/kg 08/04/23 20:18 108-20-308/03/23 17:470.0075 1
Ethylbenzene ND mg/kg 08/04/23 20:18 100-41-408/03/23 17:470.0075 1
Hexachloro-1,3-butadiene ND mg/kg 08/04/23 20:18 87-68-308/03/23 17:470.015 1
2-Hexanone ND mg/kg 08/04/23 20:18 591-78-608/03/23 17:470.075 1
Isopropylbenzene (Cumene)ND mg/kg 08/04/23 20:18 98-82-808/03/23 17:470.0075 1
p-Isopropyltoluene ND mg/kg 08/04/23 20:18 99-87-608/03/23 17:470.0075 1
Methylene Chloride ND mg/kg 08/04/23 20:18 75-09-208/03/23 17:470.030 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/04/23 20:18 108-10-108/03/23 17:470.075 1
Methyl-tert-butyl ether ND mg/kg 08/04/23 20:18 1634-04-408/03/23 17:470.0075 1
Naphthalene 0.019 mg/kg 08/04/23 20:18 91-20-308/03/23 17:470.0075 1
n-Propylbenzene ND mg/kg 08/04/23 20:18 103-65-108/03/23 17:470.0075 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-I Lab ID:92680269004 Collected:08/01/23 16:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Styrene ND mg/kg 08/04/23 20:18 100-42-508/03/23 17:470.0075 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/04/23 20:18 630-20-608/03/23 17:470.0075 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/04/23 20:18 79-34-508/03/23 17:470.0075 1
Tetrachloroethene ND mg/kg 08/04/23 20:18 127-18-408/03/23 17:470.0075 1
Toluene ND mg/kg 08/04/23 20:18 108-88-308/03/23 17:470.0075 1
1,2,3-Trichlorobenzene ND mg/kg 08/04/23 20:18 87-61-608/03/23 17:470.0075 1
1,2,4-Trichlorobenzene ND mg/kg 08/04/23 20:18 120-82-108/03/23 17:470.0075 1
1,1,1-Trichloroethane ND mg/kg 08/04/23 20:18 71-55-608/03/23 17:470.0075 1
1,1,2-Trichloroethane ND mg/kg 08/04/23 20:18 79-00-508/03/23 17:470.0075 1
Trichloroethene ND mg/kg 08/04/23 20:18 79-01-608/03/23 17:470.0075 1
Trichlorofluoromethane ND mg/kg 08/04/23 20:18 75-69-408/03/23 17:470.0075 1
1,2,3-Trichloropropane ND mg/kg 08/04/23 20:18 96-18-408/03/23 17:470.0075 1
1,2,4-Trimethylbenzene 0.037 mg/kg 08/04/23 20:18 95-63-608/03/23 17:470.0075 1
1,3,5-Trimethylbenzene 0.011 mg/kg 08/04/23 20:18 108-67-808/03/23 17:470.0075 1
Vinyl acetate ND mg/kg 08/04/23 20:18 108-05-408/03/23 17:470.075 1
Vinyl chloride ND mg/kg 08/04/23 20:18 75-01-408/03/23 17:470.015 1
Xylene (Total)0.032 mg/kg 08/04/23 20:18 1330-20-708/03/23 17:470.015 1
m&p-Xylene 0.019 mg/kg 08/04/23 20:18 179601-23-108/03/23 17:470.015 1
o-Xylene 0.013 mg/kg 08/04/23 20:18 95-47-608/03/23 17:470.0075 1
Surrogates
Toluene-d8 (S)101 %08/04/23 20:18 2037-26-508/03/23 17:4770-130 1
4-Bromofluorobenzene (S)103 %08/04/23 20:18 460-00-408/03/23 17:4770-130 1
1,2-Dichloroethane-d4 (S)111 %08/04/23 20:18 17060-07-008/03/23 17:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.5 %08/03/23 14:19 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-J Lab ID:92680269005 Collected:08/01/23 17:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 08/09/23 21:07 N208/07/23 16:3712.9 1
Aliphatic (C19-C36)ND mg/kg 08/09/23 21:07 N208/07/23 16:3712.9 1
Aromatic (C11-C22)ND mg/kg 08/09/23 21:07 N208/07/23 16:3712.9 1
Surrogates
1-Chlorooctadecane (S)75 %08/09/23 21:07 3386-33-208/07/23 16:3740-140 1
o-Terphenyl (S)56 %08/09/23 21:07 84-15-108/07/23 16:3740-140 1
2-Fluorobiphenyl (S)91 %08/09/23 21:07 321-60-808/07/23 16:3740-140 1
2-Bromonaphthalene (S)90 %08/09/23 21:07 580-13-208/07/23 16:3740-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/09/23 11:07 83-32-908/07/23 13:360.42 1
Acenaphthylene ND mg/kg 08/09/23 11:07 208-96-808/07/23 13:360.42 1
Anthracene ND mg/kg 08/09/23 11:07 120-12-708/07/23 13:360.42 1
Benzo(a)anthracene ND mg/kg 08/09/23 11:07 56-55-308/07/23 13:360.42 1
Benzo(a)pyrene ND mg/kg 08/09/23 11:07 50-32-808/07/23 13:360.42 1
Benzo(b)fluoranthene ND mg/kg 08/09/23 11:07 205-99-208/07/23 13:360.42 1
Benzo(g,h,i)perylene ND mg/kg 08/09/23 11:07 191-24-208/07/23 13:360.42 1
Benzo(k)fluoranthene ND mg/kg 08/09/23 11:07 207-08-908/07/23 13:360.42 1
Benzoic Acid ND mg/kg 08/09/23 11:07 65-85-008/07/23 13:362.1 1
Benzyl alcohol ND mg/kg 08/09/23 11:07 100-51-608/07/23 13:360.83 1
4-Bromophenylphenyl ether ND mg/kg 08/09/23 11:07 101-55-308/07/23 13:360.42 1
Butylbenzylphthalate ND mg/kg 08/09/23 11:07 85-68-708/07/23 13:360.42 1
4-Chloro-3-methylphenol ND mg/kg 08/09/23 11:07 59-50-708/07/23 13:360.83 1
4-Chloroaniline ND mg/kg 08/09/23 11:07 106-47-808/07/23 13:360.83 1
bis(2-Chloroethoxy)methane ND mg/kg 08/09/23 11:07 111-91-108/07/23 13:360.42 1
bis(2-Chloroethyl) ether ND mg/kg 08/09/23 11:07 111-44-408/07/23 13:360.42 1
2-Chloronaphthalene ND mg/kg 08/09/23 11:07 91-58-708/07/23 13:360.42 1
2-Chlorophenol ND mg/kg 08/09/23 11:07 95-57-808/07/23 13:360.42 1
4-Chlorophenylphenyl ether ND mg/kg 08/09/23 11:07 7005-72-308/07/23 13:360.42 1
Chrysene ND mg/kg 08/09/23 11:07 218-01-908/07/23 13:360.42 1
Dibenz(a,h)anthracene ND mg/kg 08/09/23 11:07 53-70-308/07/23 13:360.42 1
Dibenzofuran ND mg/kg 08/09/23 11:07 132-64-908/07/23 13:360.42 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 11:07 95-50-108/07/23 13:360.42 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 11:07 541-73-108/07/23 13:360.42 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 11:07 106-46-708/07/23 13:360.42 1
3,3'-Dichlorobenzidine ND mg/kg 08/09/23 11:07 91-94-108/07/23 13:360.83 1
2,4-Dichlorophenol ND mg/kg 08/09/23 11:07 120-83-208/07/23 13:360.42 1
Diethylphthalate ND mg/kg 08/09/23 11:07 84-66-208/07/23 13:360.42 1
2,4-Dimethylphenol ND mg/kg 08/09/23 11:07 105-67-908/07/23 13:360.42 1
Dimethylphthalate ND mg/kg 08/09/23 11:07 131-11-308/07/23 13:360.42 1
Di-n-butylphthalate ND mg/kg 08/09/23 11:07 84-74-208/07/23 13:360.42 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/09/23 11:07 534-52-108/07/23 13:360.83 1
2,4-Dinitrophenol ND mg/kg 08/09/23 11:07 51-28-508/07/23 13:362.1 1
2,4-Dinitrotoluene ND mg/kg 08/09/23 11:07 121-14-208/07/23 13:360.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-J Lab ID:92680269005 Collected:08/01/23 17:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,6-Dinitrotoluene ND mg/kg 08/09/23 11:07 606-20-208/07/23 13:360.42 1
Di-n-octylphthalate ND mg/kg 08/09/23 11:07 117-84-008/07/23 13:360.42 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/09/23 11:07 117-81-708/07/23 13:360.42 1
Fluoranthene ND mg/kg 08/09/23 11:07 206-44-008/07/23 13:360.42 1
Fluorene ND mg/kg 08/09/23 11:07 86-73-708/07/23 13:360.42 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 11:07 87-68-308/07/23 13:360.42 1
Hexachlorobenzene ND mg/kg 08/09/23 11:07 118-74-108/07/23 13:360.42 1
Hexachlorocyclopentadiene ND mg/kg 08/09/23 11:07 77-47-408/07/23 13:360.42 1
Hexachloroethane ND mg/kg 08/09/23 11:07 67-72-108/07/23 13:360.42 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/09/23 11:07 193-39-508/07/23 13:360.42 1
Isophorone ND mg/kg 08/09/23 11:07 78-59-108/07/23 13:360.42 1
1-Methylnaphthalene ND mg/kg 08/09/23 11:07 90-12-008/07/23 13:360.42 1
2-Methylnaphthalene ND mg/kg 08/09/23 11:07 91-57-608/07/23 13:360.42 1
2-Methylphenol(o-Cresol)ND mg/kg 08/09/23 11:07 95-48-708/07/23 13:360.42 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/09/23 11:07 15831-10-408/07/23 13:360.42 1
Naphthalene ND mg/kg 08/09/23 11:07 91-20-308/07/23 13:360.42 1
2-Nitroaniline ND mg/kg 08/09/23 11:07 88-74-408/07/23 13:362.1 1
3-Nitroaniline ND mg/kg 08/09/23 11:07 99-09-208/07/23 13:362.1 1
4-Nitroaniline ND mg/kg 08/09/23 11:07 100-01-608/07/23 13:360.83 1
Nitrobenzene ND mg/kg 08/09/23 11:07 98-95-308/07/23 13:360.42 1
2-Nitrophenol ND mg/kg 08/09/23 11:07 88-75-508/07/23 13:360.42 1
4-Nitrophenol ND mg/kg 08/09/23 11:07 100-02-708/07/23 13:362.1 1
N-Nitrosodimethylamine ND mg/kg 08/09/23 11:07 62-75-908/07/23 13:360.42 1
N-Nitroso-di-n-propylamine ND mg/kg 08/09/23 11:07 621-64-708/07/23 13:360.42 1
N-Nitrosodiphenylamine ND mg/kg 08/09/23 11:07 86-30-608/07/23 13:360.42 1
Pentachlorophenol ND mg/kg 08/09/23 11:07 87-86-508/07/23 13:360.83 1
Phenanthrene ND mg/kg 08/09/23 11:07 85-01-808/07/23 13:360.42 1
Phenol ND mg/kg 08/09/23 11:07 108-95-208/07/23 13:360.42 1
Pyrene ND mg/kg 08/09/23 11:07 129-00-008/07/23 13:360.42 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 11:07 120-82-108/07/23 13:360.42 1
2,4,5-Trichlorophenol ND mg/kg 08/09/23 11:07 95-95-408/07/23 13:360.42 1
2,4,6-Trichlorophenol ND mg/kg 08/09/23 11:07 88-06-208/07/23 13:360.42 1
Surrogates
Nitrobenzene-d5 (S)50 %08/09/23 11:07 4165-60-008/07/23 13:3610-130 1
2-Fluorobiphenyl (S)45 %08/09/23 11:07 321-60-808/07/23 13:3610-130 1
Terphenyl-d14 (S)51 %08/09/23 11:07 1718-51-008/07/23 13:3610-130 1
Phenol-d6 (S)47 %08/09/23 11:07 13127-88-308/07/23 13:3610-130 1
2-Fluorophenol (S)48 %08/09/23 11:07 367-12-408/07/23 13:3610-130 1
2,4,6-Tribromophenol (S)56 %08/09/23 11:07 118-79-608/07/23 13:3610-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/05/23 11:33 67-64-108/03/23 20:510.20 1
Benzene ND mg/kg 08/05/23 11:33 71-43-208/03/23 20:510.010 1
Bromobenzene ND mg/kg 08/05/23 11:33 108-86-108/03/23 20:510.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-J Lab ID:92680269005 Collected:08/01/23 17:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Bromochloromethane ND mg/kg 08/05/23 11:33 74-97-508/03/23 20:510.010 1
Bromodichloromethane ND mg/kg 08/05/23 11:33 75-27-408/03/23 20:510.010 1
Bromoform ND mg/kg 08/05/23 11:33 75-25-208/03/23 20:510.010 1
Bromomethane ND mg/kg 08/05/23 11:33 74-83-908/03/23 20:510.041 1
2-Butanone (MEK)ND mg/kg 08/05/23 11:33 78-93-308/03/23 20:510.20 1
n-Butylbenzene ND mg/kg 08/05/23 11:33 104-51-808/03/23 20:510.010 1
sec-Butylbenzene ND mg/kg 08/05/23 11:33 135-98-808/03/23 20:510.010 1
tert-Butylbenzene ND mg/kg 08/05/23 11:33 98-06-608/03/23 20:510.010 1
Carbon tetrachloride ND mg/kg 08/05/23 11:33 56-23-508/03/23 20:510.010 1
Chlorobenzene ND mg/kg 08/05/23 11:33 108-90-708/03/23 20:510.010 1
Chloroethane ND mg/kg 08/05/23 11:33 75-00-308/03/23 20:510.020 1
Chloroform ND mg/kg 08/05/23 11:33 67-66-308/03/23 20:510.010 1
Chloromethane ND mg/kg 08/05/23 11:33 74-87-308/03/23 20:510.020 1
2-Chlorotoluene ND mg/kg 08/05/23 11:33 95-49-808/03/23 20:510.010 1
4-Chlorotoluene ND mg/kg 08/05/23 11:33 106-43-408/03/23 20:510.010 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/05/23 11:33 96-12-8 IK08/03/23 20:510.010 1
Dibromochloromethane ND mg/kg 08/05/23 11:33 124-48-108/03/23 20:510.010 1
1,2-Dibromoethane (EDB)ND mg/kg 08/05/23 11:33 106-93-408/03/23 20:510.010 1
Dibromomethane ND mg/kg 08/05/23 11:33 74-95-308/03/23 20:510.010 1
1,2-Dichlorobenzene ND mg/kg 08/05/23 11:33 95-50-108/03/23 20:510.010 1
1,3-Dichlorobenzene ND mg/kg 08/05/23 11:33 541-73-108/03/23 20:510.010 1
1,4-Dichlorobenzene ND mg/kg 08/05/23 11:33 106-46-708/03/23 20:510.010 1
Dichlorodifluoromethane ND mg/kg 08/05/23 11:33 75-71-808/03/23 20:510.020 1
1,1-Dichloroethane ND mg/kg 08/05/23 11:33 75-34-308/03/23 20:510.010 1
1,2-Dichloroethane ND mg/kg 08/05/23 11:33 107-06-208/03/23 20:510.010 1
1,1-Dichloroethene ND mg/kg 08/05/23 11:33 75-35-408/03/23 20:510.010 1
cis-1,2-Dichloroethene ND mg/kg 08/05/23 11:33 156-59-208/03/23 20:510.010 1
trans-1,2-Dichloroethene ND mg/kg 08/05/23 11:33 156-60-508/03/23 20:510.010 1
1,2-Dichloropropane ND mg/kg 08/05/23 11:33 78-87-508/03/23 20:510.010 1
1,3-Dichloropropane ND mg/kg 08/05/23 11:33 142-28-908/03/23 20:510.010 1
2,2-Dichloropropane ND mg/kg 08/05/23 11:33 594-20-708/03/23 20:510.010 1
1,1-Dichloropropene ND mg/kg 08/05/23 11:33 563-58-608/03/23 20:510.010 1
cis-1,3-Dichloropropene ND mg/kg 08/05/23 11:33 10061-01-508/03/23 20:510.010 1
trans-1,3-Dichloropropene ND mg/kg 08/05/23 11:33 10061-02-608/03/23 20:510.010 1
Diisopropyl ether ND mg/kg 08/05/23 11:33 108-20-308/03/23 20:510.010 1
Ethylbenzene ND mg/kg 08/05/23 11:33 100-41-408/03/23 20:510.010 1
Hexachloro-1,3-butadiene ND mg/kg 08/05/23 11:33 87-68-308/03/23 20:510.020 1
2-Hexanone ND mg/kg 08/05/23 11:33 591-78-608/03/23 20:510.10 1
Isopropylbenzene (Cumene)ND mg/kg 08/05/23 11:33 98-82-808/03/23 20:510.010 1
p-Isopropyltoluene ND mg/kg 08/05/23 11:33 99-87-608/03/23 20:510.010 1
Methylene Chloride ND mg/kg 08/05/23 11:33 75-09-208/03/23 20:510.041 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/05/23 11:33 108-10-108/03/23 20:510.10 1
Methyl-tert-butyl ether ND mg/kg 08/05/23 11:33 1634-04-408/03/23 20:510.010 1
Naphthalene ND mg/kg 08/05/23 11:33 91-20-308/03/23 20:510.010 1
n-Propylbenzene ND mg/kg 08/05/23 11:33 103-65-108/03/23 20:510.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92680269
ONE STOP 15
Sample:SOIL-J Lab ID:92680269005 Collected:08/01/23 17:00 Received:08/02/23 08:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Styrene ND mg/kg 08/05/23 11:33 100-42-508/03/23 20:510.010 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/05/23 11:33 630-20-608/03/23 20:510.010 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/05/23 11:33 79-34-508/03/23 20:510.010 1
Tetrachloroethene ND mg/kg 08/05/23 11:33 127-18-408/03/23 20:510.010 1
Toluene ND mg/kg 08/05/23 11:33 108-88-308/03/23 20:510.010 1
1,2,3-Trichlorobenzene ND mg/kg 08/05/23 11:33 87-61-608/03/23 20:510.010 1
1,2,4-Trichlorobenzene ND mg/kg 08/05/23 11:33 120-82-108/03/23 20:510.010 1
1,1,1-Trichloroethane ND mg/kg 08/05/23 11:33 71-55-608/03/23 20:510.010 1
1,1,2-Trichloroethane ND mg/kg 08/05/23 11:33 79-00-508/03/23 20:510.010 1
Trichloroethene ND mg/kg 08/05/23 11:33 79-01-608/03/23 20:510.010 1
Trichlorofluoromethane ND mg/kg 08/05/23 11:33 75-69-408/03/23 20:510.010 1
1,2,3-Trichloropropane ND mg/kg 08/05/23 11:33 96-18-408/03/23 20:510.010 1
1,2,4-Trimethylbenzene ND mg/kg 08/05/23 11:33 95-63-608/03/23 20:510.010 1
1,3,5-Trimethylbenzene ND mg/kg 08/05/23 11:33 108-67-808/03/23 20:510.010 1
Vinyl acetate ND mg/kg 08/05/23 11:33 108-05-408/03/23 20:510.10 1
Vinyl chloride ND mg/kg 08/05/23 11:33 75-01-408/03/23 20:510.020 1
Xylene (Total)ND mg/kg 08/05/23 11:33 1330-20-708/03/23 20:510.020 1
m&p-Xylene ND mg/kg 08/05/23 11:33 179601-23-108/03/23 20:510.020 1
o-Xylene ND mg/kg 08/05/23 11:33 95-47-608/03/23 20:510.010 1
Surrogates
Toluene-d8 (S)102 %08/05/23 11:33 2037-26-508/03/23 20:5170-130 1
4-Bromofluorobenzene (S)102 %08/05/23 11:33 460-00-408/03/23 20:5170-130 1
1,2-Dichloroethane-d4 (S)117 %08/05/23 11:33 17060-07-008/03/23 20:5170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.5 %08/03/23 14:40 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
791331
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92680269002, 92680269003, 92680269004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4101122
Associated Lab Samples:92680269002, 92680269003, 92680269004
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 08/04/23 17:48
1,1,1-Trichloroethane mg/kg ND 0.0050 08/04/23 17:48
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 08/04/23 17:48
1,1,2-Trichloroethane mg/kg ND 0.0050 08/04/23 17:48
1,1-Dichloroethane mg/kg ND 0.0050 08/04/23 17:48
1,1-Dichloroethene mg/kg ND 0.0050 08/04/23 17:48
1,1-Dichloropropene mg/kg ND 0.0050 08/04/23 17:48
1,2,3-Trichlorobenzene mg/kg ND 0.0050 08/04/23 17:48
1,2,3-Trichloropropane mg/kg ND 0.0050 08/04/23 17:48
1,2,4-Trichlorobenzene mg/kg ND 0.0050 08/04/23 17:48
1,2,4-Trimethylbenzene mg/kg ND 0.0050 08/04/23 17:48
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 IK08/04/23 17:48
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 08/04/23 17:48
1,2-Dichlorobenzene mg/kg ND 0.0050 08/04/23 17:48
1,2-Dichloroethane mg/kg ND 0.0050 08/04/23 17:48
1,2-Dichloropropane mg/kg ND 0.0050 08/04/23 17:48
1,3,5-Trimethylbenzene mg/kg ND 0.0050 08/04/23 17:48
1,3-Dichlorobenzene mg/kg ND 0.0050 08/04/23 17:48
1,3-Dichloropropane mg/kg ND 0.0050 08/04/23 17:48
1,4-Dichlorobenzene mg/kg ND 0.0050 08/04/23 17:48
2,2-Dichloropropane mg/kg ND 0.0050 08/04/23 17:48
2-Butanone (MEK)mg/kg ND 0.10 08/04/23 17:48
2-Chlorotoluene mg/kg ND 0.0050 08/04/23 17:48
2-Hexanone mg/kg ND 0.050 08/04/23 17:48
4-Chlorotoluene mg/kg ND 0.0050 08/04/23 17:48
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 08/04/23 17:48
Acetone mg/kg ND 0.10 08/04/23 17:48
Benzene mg/kg ND 0.0050 08/04/23 17:48
Bromobenzene mg/kg ND 0.0050 08/04/23 17:48
Bromochloromethane mg/kg ND 0.0050 08/04/23 17:48
Bromodichloromethane mg/kg ND 0.0050 08/04/23 17:48
Bromoform mg/kg ND 0.0050 08/04/23 17:48
Bromomethane mg/kg ND 0.020 08/04/23 17:48
Carbon tetrachloride mg/kg ND 0.0050 08/04/23 17:48
Chlorobenzene mg/kg ND 0.0050 08/04/23 17:48
Chloroethane mg/kg ND 0.010 08/04/23 17:48
Chloroform mg/kg ND 0.0050 08/04/23 17:48
Chloromethane mg/kg ND 0.010 08/04/23 17:48
cis-1,2-Dichloroethene mg/kg ND 0.0050 08/04/23 17:48
cis-1,3-Dichloropropene mg/kg ND 0.0050 08/04/23 17:48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4101122
Associated Lab Samples:92680269002, 92680269003, 92680269004
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 08/04/23 17:48
Dibromomethane mg/kg ND 0.0050 08/04/23 17:48
Dichlorodifluoromethane mg/kg ND 0.010 v108/04/23 17:48
Diisopropyl ether mg/kg ND 0.0050 08/04/23 17:48
Ethylbenzene mg/kg ND 0.0050 08/04/23 17:48
Hexachloro-1,3-butadiene mg/kg ND 0.010 08/04/23 17:48
Isopropylbenzene (Cumene)mg/kg ND 0.0050 08/04/23 17:48
m&p-Xylene mg/kg ND 0.010 08/04/23 17:48
Methyl-tert-butyl ether mg/kg ND 0.0050 08/04/23 17:48
Methylene Chloride mg/kg ND 0.020 08/04/23 17:48
n-Butylbenzene mg/kg ND 0.0050 08/04/23 17:48
n-Propylbenzene mg/kg ND 0.0050 08/04/23 17:48
Naphthalene mg/kg ND 0.0050 08/04/23 17:48
o-Xylene mg/kg ND 0.0050 08/04/23 17:48
p-Isopropyltoluene mg/kg ND 0.0050 08/04/23 17:48
sec-Butylbenzene mg/kg ND 0.0050 08/04/23 17:48
Styrene mg/kg ND 0.0050 08/04/23 17:48
tert-Butylbenzene mg/kg ND 0.0050 v208/04/23 17:48
Tetrachloroethene mg/kg ND 0.0050 08/04/23 17:48
Toluene mg/kg ND 0.0050 08/04/23 17:48
trans-1,2-Dichloroethene mg/kg ND 0.0050 08/04/23 17:48
trans-1,3-Dichloropropene mg/kg ND 0.0050 08/04/23 17:48
Trichloroethene mg/kg ND 0.0050 08/04/23 17:48
Trichlorofluoromethane mg/kg ND 0.0050 08/04/23 17:48
Vinyl acetate mg/kg ND 0.050 08/04/23 17:48
Vinyl chloride mg/kg ND 0.010 08/04/23 17:48
Xylene (Total)mg/kg ND 0.010 08/04/23 17:48
1,2-Dichloroethane-d4 (S)%114 70-130 08/04/23 17:48
4-Bromofluorobenzene (S)%101 70-130 08/04/23 17:48
Toluene-d8 (S)%102 70-130 08/04/23 17:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4101123LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.480.5 95 70-130
1,1,1-Trichloroethane mg/kg 0.490.5 99 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.490.5 99 70-130
1,1,2-Trichloroethane mg/kg 0.470.5 94 70-130
1,1-Dichloroethane mg/kg 0.490.5 97 70-130
1,1-Dichloroethene mg/kg 0.520.5 104 70-130
1,1-Dichloropropene mg/kg 0.510.5 102 70-130
1,2,3-Trichlorobenzene mg/kg 0.470.5 94 70-130
1,2,3-Trichloropropane mg/kg 0.470.5 94 70-130
1,2,4-Trichlorobenzene mg/kg 0.470.5 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4101123LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 0.490.5 97 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.43 IK0.5 86 67-130
1,2-Dibromoethane (EDB)mg/kg 0.460.5 93 70-130
1,2-Dichlorobenzene mg/kg 0.460.5 92 70-130
1,2-Dichloroethane mg/kg 0.490.5 98 70-130
1,2-Dichloropropane mg/kg 0.480.5 95 70-130
1,3,5-Trimethylbenzene mg/kg 0.490.5 98 70-130
1,3-Dichlorobenzene mg/kg 0.450.5 91 70-130
1,3-Dichloropropane mg/kg 0.460.5 93 70-130
1,4-Dichlorobenzene mg/kg 0.460.5 91 70-130
2,2-Dichloropropane mg/kg 0.510.5 101 67-130
2-Butanone (MEK)mg/kg 0.941 94 66-130
2-Chlorotoluene mg/kg 0.480.5 95 70-130
2-Hexanone mg/kg 0.981 98 70-130
4-Chlorotoluene mg/kg 0.480.5 96 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.971 97 70-130
Acetone mg/kg 0.881 88 67-130
Benzene mg/kg 0.460.5 92 70-130
Bromobenzene mg/kg 0.460.5 91 70-130
Bromochloromethane mg/kg 0.480.5 97 70-130
Bromodichloromethane mg/kg 0.480.5 96 70-130
Bromoform mg/kg 0.460.5 92 70-130
Bromomethane mg/kg 0.590.5 118 53-175
Carbon tetrachloride mg/kg 0.490.5 98 70-130
Chlorobenzene mg/kg 0.480.5 97 70-130
Chloroethane mg/kg 0.490.5 99 70-135
Chloroform mg/kg 0.480.5 96 70-130
Chloromethane mg/kg 0.480.5 97 64-130
cis-1,2-Dichloroethene mg/kg 0.500.5 100 70-130
cis-1,3-Dichloropropene mg/kg 0.440.5 88 70-130
Dibromochloromethane mg/kg 0.470.5 95 70-130
Dibromomethane mg/kg 0.480.5 96 70-130
Dichlorodifluoromethane mg/kg 0.79 L1,v10.5 159 63-145
Diisopropyl ether mg/kg 0.460.5 93 68-130
Ethylbenzene mg/kg 0.450.5 89 70-130
Hexachloro-1,3-butadiene mg/kg 0.480.5 96 70-130
Isopropylbenzene (Cumene)mg/kg 0.490.5 97 70-130
m&p-Xylene mg/kg 0.961 96 70-130
Methyl-tert-butyl ether mg/kg 0.440.5 89 70-130
Methylene Chloride mg/kg 0.480.5 97 67-130
n-Butylbenzene mg/kg 0.490.5 98 70-130
n-Propylbenzene mg/kg 0.480.5 97 70-130
Naphthalene mg/kg 0.480.5 96 70-130
o-Xylene mg/kg 0.470.5 95 70-130
p-Isopropyltoluene mg/kg 0.490.5 98 70-130
sec-Butylbenzene mg/kg 0.470.5 93 70-130
Styrene mg/kg 0.490.5 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4101123LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 0.35 v30.5 70 64-130
Tetrachloroethene mg/kg 0.450.5 90 70-130
Toluene mg/kg 0.470.5 94 70-130
trans-1,2-Dichloroethene mg/kg 0.500.5 99 70-130
trans-1,3-Dichloropropene mg/kg 0.480.5 96 70-130
Trichloroethene mg/kg 0.480.5 96 70-130
Trichlorofluoromethane mg/kg 0.570.5 113 70-130
Vinyl acetate mg/kg 1.01 101 70-134
Vinyl chloride mg/kg 0.470.5 95 68-130
Xylene (Total)mg/kg 1.41.5 96 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4101124MATRIX SPIKE SAMPLE:
MSSpike
Result
92680444009
1,1,1,2-Tetrachloroethane mg/kg 1.00.83 119 58-140ND
1,1,1-Trichloroethane mg/kg 1.10.83 130 58-144ND
1,1,2,2-Tetrachloroethane mg/kg 0.950.83 113 52-139ND
1,1,2-Trichloroethane mg/kg 0.980.83 118 56-140ND
1,1-Dichloroethane mg/kg 1.00.83 121 58-145ND
1,1-Dichloroethene mg/kg 1.10.83 131 57-158ND
1,1-Dichloropropene mg/kg 1.10.83 132 58-151ND
1,2,3-Trichlorobenzene mg/kg 0.970.83 116 48-149ND
1,2,3-Trichloropropane mg/kg 0.850.83 102 54-132ND
1,2,4-Trichlorobenzene mg/kg 1.00.83 119 51-151ND
1,2,4-Trimethylbenzene mg/kg 0.970.83 116 38-170ND
1,2-Dibromo-3-chloropropane mg/kg 0.81 IK0.83 97 44-134ND
1,2-Dibromoethane (EDB)mg/kg 0.930.83 111 60-138ND
1,2-Dichlorobenzene mg/kg 0.960.83 115 59-147ND
1,2-Dichloroethane mg/kg 0.980.83 117 57-139ND
1,2-Dichloropropane mg/kg 1.00.83 121 62-145ND
1,3,5-Trimethylbenzene mg/kg 1.00.83 121 47-159ND
1,3-Dichlorobenzene mg/kg 0.930.83 111 58-144ND
1,3-Dichloropropane mg/kg 0.930.83 111 60-142ND
1,4-Dichlorobenzene mg/kg 0.940.83 113 57-143ND
2,2-Dichloropropane mg/kg 0.750.83 90 37-144ND
2-Butanone (MEK)mg/kg 1.81.6 108 28-146ND
2-Chlorotoluene mg/kg 0.970.83 116 55-158ND
2-Hexanone mg/kg 1.81.6 105 44-141ND
4-Chlorotoluene mg/kg 0.960.83 114 55-146ND
4-Methyl-2-pentanone (MIBK)mg/kg 1.81.6 106 50-138ND
Acetone mg/kg 1.31.6 74 20-136ND
Benzene mg/kg 0.980.83 118 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4101124MATRIX SPIKE SAMPLE:
MSSpike
Result
92680444009
Bromobenzene mg/kg 0.950.83 114 59-145ND
Bromochloromethane mg/kg 1.00.83 122 57-143ND
Bromodichloromethane mg/kg 0.970.83 116 53-133ND
Bromoform mg/kg 0.920.83 110 48-133ND
Bromomethane mg/kg 0.330.83 40 10-167ND
Carbon tetrachloride mg/kg 1.00.83 121 57-147ND
Chlorobenzene mg/kg 1.00.83 121 61-144ND
Chloroethane mg/kg 0.350.83 41 10-153ND
Chloroform mg/kg 1.00.83 120 58-141ND
Chloromethane mg/kg 1.10.83 127 54-165ND
cis-1,2-Dichloroethene mg/kg 1.00.83 123 59-144ND
cis-1,3-Dichloropropene mg/kg 0.870.83 104 56-137ND
Dibromochloromethane mg/kg 0.970.83 116 53-139ND
Dibromomethane mg/kg 1.00.83 120 60-136ND
Dichlorodifluoromethane mg/kg 1.6 M0,v10.83 197 49-177ND
Diisopropyl ether mg/kg 0.950.83 113 53-136ND
Ethylbenzene mg/kg 0.950.83 113 53-150ND
Hexachloro-1,3-butadiene mg/kg 1.20.83 143 42-186ND
Isopropylbenzene (Cumene)mg/kg 1.10.83 128 62-154ND
m&p-Xylene mg/kg 2.01.6 121 49-156ND
Methyl-tert-butyl ether mg/kg 0.880.83 106 54-133ND
Methylene Chloride mg/kg 0.940.83 113 50-153ND
n-Butylbenzene mg/kg 1.00.83 122 44-174ND
n-Propylbenzene mg/kg 1.00.83 120 52-157ND
Naphthalene mg/kg 0.930.83 111 37-150ND
o-Xylene mg/kg 1.00.83 121 54-150ND
p-Isopropyltoluene mg/kg 1.10.83 124 50-16439.5 ug/kg
sec-Butylbenzene mg/kg 1.00.83 121 58-161ND
Styrene mg/kg 1.00.83 123 60-148ND
tert-Butylbenzene mg/kg 0.73 v30.83 87 44-151ND
Tetrachloroethene mg/kg 0.990.83 118 53-151ND
Toluene mg/kg 1.00.83 121 52-148ND
trans-1,2-Dichloroethene mg/kg 1.00.83 120 60-148ND
trans-1,3-Dichloropropene mg/kg 0.910.83 109 55-133ND
Trichloroethene mg/kg 1.10.83 130 60-148ND
Trichlorofluoromethane mg/kg 0.510.83 61 10-154ND
Vinyl acetate mg/kg 1.71.6 103 50-149ND
Vinyl chloride mg/kg 0.960.83 114 57-157ND
Xylene (Total)mg/kg 3.02.5 121 52-153ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92680444010
4101125SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg NDND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg ND IKND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg NDND
2-Butanone (MEK)mg/kg NDND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg NDND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg NDND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg NDND
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg .013JND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg ND v1ND
Diisopropyl ether mg/kg NDND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Isopropylbenzene (Cumene)mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92680444010
4101125SAMPLE DUPLICATE:
m&p-Xylene mg/kg NDND
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg NDND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg .0087JND
o-Xylene mg/kg NDND
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg ND v2ND
Tetrachloroethene mg/kg NDND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg NDND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%122116
4-Bromofluorobenzene (S)%104104
Toluene-d8 (S)%102102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
791348
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92680269005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4101156
Associated Lab Samples:92680269005
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 08/05/23 06:15
1,1,1-Trichloroethane mg/kg ND 0.0050 08/05/23 06:15
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 08/05/23 06:15
1,1,2-Trichloroethane mg/kg ND 0.0050 08/05/23 06:15
1,1-Dichloroethane mg/kg ND 0.0050 08/05/23 06:15
1,1-Dichloroethene mg/kg ND 0.0050 08/05/23 06:15
1,1-Dichloropropene mg/kg ND 0.0050 08/05/23 06:15
1,2,3-Trichlorobenzene mg/kg ND 0.0050 08/05/23 06:15
1,2,3-Trichloropropane mg/kg ND 0.0050 08/05/23 06:15
1,2,4-Trichlorobenzene mg/kg ND 0.0050 08/05/23 06:15
1,2,4-Trimethylbenzene mg/kg ND 0.0050 08/05/23 06:15
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 IK08/05/23 06:15
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 08/05/23 06:15
1,2-Dichlorobenzene mg/kg ND 0.0050 08/05/23 06:15
1,2-Dichloroethane mg/kg ND 0.0050 08/05/23 06:15
1,2-Dichloropropane mg/kg ND 0.0050 08/05/23 06:15
1,3,5-Trimethylbenzene mg/kg ND 0.0050 08/05/23 06:15
1,3-Dichlorobenzene mg/kg ND 0.0050 08/05/23 06:15
1,3-Dichloropropane mg/kg ND 0.0050 08/05/23 06:15
1,4-Dichlorobenzene mg/kg ND 0.0050 08/05/23 06:15
2,2-Dichloropropane mg/kg ND 0.0050 08/05/23 06:15
2-Butanone (MEK)mg/kg ND 0.10 08/05/23 06:15
2-Chlorotoluene mg/kg ND 0.0050 08/05/23 06:15
2-Hexanone mg/kg ND 0.050 08/05/23 06:15
4-Chlorotoluene mg/kg ND 0.0050 08/05/23 06:15
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 08/05/23 06:15
Acetone mg/kg ND 0.10 08/05/23 06:15
Benzene mg/kg ND 0.0050 08/05/23 06:15
Bromobenzene mg/kg ND 0.0050 08/05/23 06:15
Bromochloromethane mg/kg ND 0.0050 08/05/23 06:15
Bromodichloromethane mg/kg ND 0.0050 08/05/23 06:15
Bromoform mg/kg ND 0.0050 08/05/23 06:15
Bromomethane mg/kg ND 0.020 08/05/23 06:15
Carbon tetrachloride mg/kg ND 0.0050 08/05/23 06:15
Chlorobenzene mg/kg ND 0.0050 08/05/23 06:15
Chloroethane mg/kg ND 0.010 08/05/23 06:15
Chloroform mg/kg ND 0.0050 08/05/23 06:15
Chloromethane mg/kg ND 0.010 08/05/23 06:15
cis-1,2-Dichloroethene mg/kg ND 0.0050 08/05/23 06:15
cis-1,3-Dichloropropene mg/kg ND 0.0050 08/05/23 06:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4101156
Associated Lab Samples:92680269005
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 08/05/23 06:15
Dibromomethane mg/kg ND 0.0050 08/05/23 06:15
Dichlorodifluoromethane mg/kg ND 0.010 08/05/23 06:15
Diisopropyl ether mg/kg ND 0.0050 08/05/23 06:15
Ethylbenzene mg/kg ND 0.0050 08/05/23 06:15
Hexachloro-1,3-butadiene mg/kg ND 0.010 08/05/23 06:15
Isopropylbenzene (Cumene)mg/kg ND 0.0050 08/05/23 06:15
m&p-Xylene mg/kg ND 0.010 08/05/23 06:15
Methyl-tert-butyl ether mg/kg ND 0.0050 08/05/23 06:15
Methylene Chloride mg/kg ND 0.020 08/05/23 06:15
n-Butylbenzene mg/kg ND 0.0050 08/05/23 06:15
n-Propylbenzene mg/kg ND 0.0050 08/05/23 06:15
Naphthalene mg/kg ND 0.0050 08/05/23 06:15
o-Xylene mg/kg ND 0.0050 08/05/23 06:15
p-Isopropyltoluene mg/kg ND 0.0050 08/05/23 06:15
sec-Butylbenzene mg/kg ND 0.0050 08/05/23 06:15
Styrene mg/kg ND 0.0050 08/05/23 06:15
tert-Butylbenzene mg/kg ND 0.0050 08/05/23 06:15
Tetrachloroethene mg/kg ND 0.0050 08/05/23 06:15
Toluene mg/kg ND 0.0050 08/05/23 06:15
trans-1,2-Dichloroethene mg/kg ND 0.0050 08/05/23 06:15
trans-1,3-Dichloropropene mg/kg ND 0.0050 08/05/23 06:15
Trichloroethene mg/kg ND 0.0050 08/05/23 06:15
Trichlorofluoromethane mg/kg ND 0.0050 08/05/23 06:15
Vinyl acetate mg/kg ND 0.050 08/05/23 06:15
Vinyl chloride mg/kg ND 0.010 08/05/23 06:15
Xylene (Total)mg/kg ND 0.010 08/05/23 06:15
1,2-Dichloroethane-d4 (S)%108 70-130 08/05/23 06:15
4-Bromofluorobenzene (S)%102 70-130 08/05/23 06:15
Toluene-d8 (S)%102 70-130 08/05/23 06:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4101157LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.530.5 106 70-130
1,1,1-Trichloroethane mg/kg 0.550.5 111 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.540.5 107 70-130
1,1,2-Trichloroethane mg/kg 0.540.5 108 70-130
1,1-Dichloroethane mg/kg 0.550.5 109 70-130
1,1-Dichloroethene mg/kg 0.580.5 115 70-130
1,1-Dichloropropene mg/kg 0.560.5 113 70-130
1,2,3-Trichlorobenzene mg/kg 0.530.5 106 70-130
1,2,3-Trichloropropane mg/kg 0.500.5 100 70-130
1,2,4-Trichlorobenzene mg/kg 0.530.5 106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4101157LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 0.540.5 107 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.48 IK0.5 96 67-130
1,2-Dibromoethane (EDB)mg/kg 0.530.5 105 70-130
1,2-Dichlorobenzene mg/kg 0.520.5 104 70-130
1,2-Dichloroethane mg/kg 0.540.5 107 70-130
1,2-Dichloropropane mg/kg 0.540.5 109 70-130
1,3,5-Trimethylbenzene mg/kg 0.540.5 109 70-130
1,3-Dichlorobenzene mg/kg 0.510.5 101 70-130
1,3-Dichloropropane mg/kg 0.520.5 103 70-130
1,4-Dichlorobenzene mg/kg 0.510.5 101 70-130
2,2-Dichloropropane mg/kg 0.490.5 97 67-130
2-Butanone (MEK)mg/kg 1.01 102 66-130
2-Chlorotoluene mg/kg 0.530.5 106 70-130
2-Hexanone mg/kg 1.11 106 70-130
4-Chlorotoluene mg/kg 0.530.5 106 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 1.11 107 70-130
Acetone mg/kg 0.971 97 67-130
Benzene mg/kg 0.530.5 105 70-130
Bromobenzene mg/kg 0.520.5 105 70-130
Bromochloromethane mg/kg 0.550.5 110 70-130
Bromodichloromethane mg/kg 0.530.5 106 70-130
Bromoform mg/kg 0.530.5 106 70-130
Bromomethane mg/kg 0.600.5 121 53-175
Carbon tetrachloride mg/kg 0.540.5 109 70-130
Chlorobenzene mg/kg 0.550.5 109 70-130
Chloroethane mg/kg 0.550.5 111 70-135
Chloroform mg/kg 0.530.5 106 70-130
Chloromethane mg/kg 0.550.5 109 64-130
cis-1,2-Dichloroethene mg/kg 0.550.5 110 70-130
cis-1,3-Dichloropropene mg/kg 0.480.5 96 70-130
Dibromochloromethane mg/kg 0.540.5 108 70-130
Dibromomethane mg/kg 0.550.5 110 70-130
Dichlorodifluoromethane mg/kg 0.610.5 122 63-145
Diisopropyl ether mg/kg 0.520.5 103 68-130
Ethylbenzene mg/kg 0.500.5 100 70-130
Hexachloro-1,3-butadiene mg/kg 0.560.5 111 70-130
Isopropylbenzene (Cumene)mg/kg 0.550.5 109 70-130
m&p-Xylene mg/kg 1.11 108 70-130
Methyl-tert-butyl ether mg/kg 0.490.5 98 70-130
Methylene Chloride mg/kg 0.540.5 107 67-130
n-Butylbenzene mg/kg 0.530.5 106 70-130
n-Propylbenzene mg/kg 0.540.5 108 70-130
Naphthalene mg/kg 0.540.5 107 70-130
o-Xylene mg/kg 0.540.5 108 70-130
p-Isopropyltoluene mg/kg 0.540.5 108 70-130
sec-Butylbenzene mg/kg 0.520.5 104 70-130
Styrene mg/kg 0.560.5 111 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4101157LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 0.500.5 100 64-130
Tetrachloroethene mg/kg 0.560.5 112 70-130
Toluene mg/kg 0.540.5 108 70-130
trans-1,2-Dichloroethene mg/kg 0.550.5 111 70-130
trans-1,3-Dichloropropene mg/kg 0.520.5 104 70-130
Trichloroethene mg/kg 0.560.5 113 70-130
Trichlorofluoromethane mg/kg 0.530.5 105 70-130
Vinyl acetate mg/kg 1.11 106 70-134
Vinyl chloride mg/kg 0.520.5 105 68-130
Xylene (Total)mg/kg 1.61.5 108 70-130
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4101158MATRIX SPIKE SAMPLE:
MSSpike
Result
92680208001
1,1,1,2-Tetrachloroethane mg/kg 0.900.8 112 58-140ND
1,1,1-Trichloroethane mg/kg 1.00.8 130 58-144ND
1,1,2,2-Tetrachloroethane mg/kg 0.910.8 113 52-139ND
1,1,2-Trichloroethane mg/kg 0.930.8 116 56-140ND
1,1-Dichloroethane mg/kg 1.00.8 126 58-145ND
1,1-Dichloroethene mg/kg 1.10.8 141 57-158ND
1,1-Dichloropropene mg/kg 1.10.8 135 58-151ND
1,2,3-Trichlorobenzene mg/kg 0.770.8 96 48-149ND
1,2,3-Trichloropropane mg/kg 0.840.8 105 54-132ND
1,2,4-Trichlorobenzene mg/kg 0.840.8 104 51-151ND
1,2,4-Trimethylbenzene mg/kg 0.940.8 117 38-170ND
1,2-Dibromo-3-chloropropane mg/kg 0.71 IK0.8 89 44-134ND
1,2-Dibromoethane (EDB)mg/kg 0.870.8 109 60-138ND
1,2-Dichlorobenzene mg/kg 0.880.8 110 59-147ND
1,2-Dichloroethane mg/kg 1.00.8 124 57-139ND
1,2-Dichloropropane mg/kg 0.980.8 122 62-145ND
1,3,5-Trimethylbenzene mg/kg 0.960.8 119 47-159ND
1,3-Dichlorobenzene mg/kg 0.880.8 109 58-144ND
1,3-Dichloropropane mg/kg 0.890.8 110 60-142ND
1,4-Dichlorobenzene mg/kg 0.850.8 105 57-143ND
2,2-Dichloropropane mg/kg 0.680.8 84 37-144ND
2-Butanone (MEK)mg/kg 1.91.6 116 28-146ND
2-Chlorotoluene mg/kg 0.920.8 115 55-158ND
2-Hexanone mg/kg 1.81.6 111 44-141ND
4-Chlorotoluene mg/kg 0.920.8 114 55-146ND
4-Methyl-2-pentanone (MIBK)mg/kg 1.81.6 113 50-138ND
Acetone mg/kg 1.41.6 89 20-136ND
Benzene mg/kg 0.950.8 118 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4101158MATRIX SPIKE SAMPLE:
MSSpike
Result
92680208001
Bromobenzene mg/kg 0.870.8 108 59-145ND
Bromochloromethane mg/kg 0.960.8 120 57-143ND
Bromodichloromethane mg/kg 0.920.8 114 53-133ND
Bromoform mg/kg 0.840.8 104 48-133ND
Bromomethane mg/kg 0.400.8 49 10-167ND
Carbon tetrachloride mg/kg 0.850.8 106 57-147ND
Chlorobenzene mg/kg 0.940.8 117 61-144ND
Chloroethane mg/kg 0.340.8 43 10-153ND
Chloroform mg/kg 0.980.8 122 58-141ND
Chloromethane mg/kg 1.10.8 135 54-165ND
cis-1,2-Dichloroethene mg/kg 1.00.8 126 59-144ND
cis-1,3-Dichloropropene mg/kg 0.810.8 100 56-137ND
Dibromochloromethane mg/kg 0.880.8 110 53-139ND
Dibromomethane mg/kg 0.920.8 114 60-136ND
Dichlorodifluoromethane mg/kg 1.5 M10.8 191 49-177ND
Diisopropyl ether mg/kg 0.950.8 118 53-136ND
Ethylbenzene mg/kg 0.900.8 112 53-150ND
Hexachloro-1,3-butadiene mg/kg 0.860.8 107 42-186ND
Isopropylbenzene (Cumene)mg/kg 0.990.8 123 62-154ND
m&p-Xylene mg/kg 1.91.6 120 49-156ND
Methyl-tert-butyl ether mg/kg 0.870.8 108 54-133ND
Methylene Chloride mg/kg 0.940.8 117 50-153ND
n-Butylbenzene mg/kg 0.920.8 115 44-174ND
n-Propylbenzene mg/kg 0.940.8 117 52-157ND
Naphthalene mg/kg 0.760.8 94 37-150ND
o-Xylene mg/kg 0.930.8 116 54-150ND
p-Isopropyltoluene mg/kg 0.950.8 118 50-164ND
sec-Butylbenzene mg/kg 0.950.8 118 58-161ND
Styrene mg/kg 0.950.8 118 60-148ND
tert-Butylbenzene mg/kg 0.670.8 83 44-151ND
Tetrachloroethene mg/kg 0.980.8 109 53-151101 ug/kg
Toluene mg/kg 0.960.8 119 52-148ND
trans-1,2-Dichloroethene mg/kg 1.00.8 124 60-148ND
trans-1,3-Dichloropropene mg/kg 0.840.8 105 55-133ND
Trichloroethene mg/kg 1.00.8 122 60-14811.3 ug/kg
Trichlorofluoromethane mg/kg 0.410.8 51 10-154ND
Vinyl acetate mg/kg 1.61.6 101 50-149ND
Vinyl chloride mg/kg 0.900.8 112 57-157ND
Xylene (Total)mg/kg 2.92.5 119 52-153ND
1,2-Dichloroethane-d4 (S)%114 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92680208002
4101159SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg NDND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg ND IKND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg NDND
2-Butanone (MEK)mg/kg NDND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg NDND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg NDND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg NDND
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg NDND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg NDND
Diisopropyl ether mg/kg NDND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Isopropylbenzene (Cumene)mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92680208002
4101159SAMPLE DUPLICATE:
m&p-Xylene mg/kg .016JND
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg NDND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg NDND
o-Xylene mg/kg NDND
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg NDND
Tetrachloroethene mg/kg 0.045 941.2 ug/kg
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg NDND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%109114
4-Bromofluorobenzene (S)%104103
Toluene-d8 (S)%98103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
791966
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92680269001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4103857
Associated Lab Samples:92680269001
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 08/08/23 10:45
1,1,1-Trichloroethane mg/kg ND 0.0050 08/08/23 10:45
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 08/08/23 10:45
1,1,2-Trichloroethane mg/kg ND 0.0050 08/08/23 10:45
1,1-Dichloroethane mg/kg ND 0.0050 08/08/23 10:45
1,1-Dichloroethene mg/kg ND 0.0050 08/08/23 10:45
1,1-Dichloropropene mg/kg ND 0.0050 08/08/23 10:45
1,2,3-Trichlorobenzene mg/kg ND 0.0050 08/08/23 10:45
1,2,3-Trichloropropane mg/kg ND 0.0050 08/08/23 10:45
1,2,4-Trichlorobenzene mg/kg ND 0.0050 IK08/08/23 10:45
1,2,4-Trimethylbenzene mg/kg ND 0.0050 08/08/23 10:45
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 08/08/23 10:45
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 08/08/23 10:45
1,2-Dichlorobenzene mg/kg ND 0.0050 08/08/23 10:45
1,2-Dichloroethane mg/kg ND 0.0050 08/08/23 10:45
1,2-Dichloropropane mg/kg ND 0.0050 08/08/23 10:45
1,3,5-Trimethylbenzene mg/kg ND 0.0050 08/08/23 10:45
1,3-Dichlorobenzene mg/kg ND 0.0050 08/08/23 10:45
1,3-Dichloropropane mg/kg ND 0.0050 08/08/23 10:45
1,4-Dichlorobenzene mg/kg ND 0.0050 08/08/23 10:45
2,2-Dichloropropane mg/kg ND 0.0050 08/08/23 10:45
2-Butanone (MEK)mg/kg ND 0.10 08/08/23 10:45
2-Chlorotoluene mg/kg ND 0.0050 08/08/23 10:45
2-Hexanone mg/kg ND 0.050 08/08/23 10:45
4-Chlorotoluene mg/kg ND 0.0050 08/08/23 10:45
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 08/08/23 10:45
Acetone mg/kg ND 0.10 08/08/23 10:45
Benzene mg/kg ND 0.0050 08/08/23 10:45
Bromobenzene mg/kg ND 0.0050 08/08/23 10:45
Bromochloromethane mg/kg ND 0.0050 08/08/23 10:45
Bromodichloromethane mg/kg ND 0.0050 08/08/23 10:45
Bromoform mg/kg ND 0.0050 08/08/23 10:45
Bromomethane mg/kg ND 0.020 08/08/23 10:45
Carbon tetrachloride mg/kg ND 0.0050 08/08/23 10:45
Chlorobenzene mg/kg ND 0.0050 08/08/23 10:45
Chloroethane mg/kg ND 0.010 08/08/23 10:45
Chloroform mg/kg ND 0.0050 08/08/23 10:45
Chloromethane mg/kg ND 0.010 08/08/23 10:45
cis-1,2-Dichloroethene mg/kg ND 0.0050 08/08/23 10:45
cis-1,3-Dichloropropene mg/kg ND 0.0050 08/08/23 10:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4103857
Associated Lab Samples:92680269001
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 08/08/23 10:45
Dibromomethane mg/kg ND 0.0050 08/08/23 10:45
Dichlorodifluoromethane mg/kg ND 0.010 v108/08/23 10:45
Diisopropyl ether mg/kg ND 0.0050 08/08/23 10:45
Ethylbenzene mg/kg ND 0.0050 08/08/23 10:45
Hexachloro-1,3-butadiene mg/kg ND 0.010 08/08/23 10:45
Isopropylbenzene (Cumene)mg/kg ND 0.0050 08/08/23 10:45
m&p-Xylene mg/kg ND 0.010 08/08/23 10:45
Methyl-tert-butyl ether mg/kg ND 0.0050 08/08/23 10:45
Methylene Chloride mg/kg ND 0.020 08/08/23 10:45
n-Butylbenzene mg/kg ND 0.0050 08/08/23 10:45
n-Propylbenzene mg/kg ND 0.0050 08/08/23 10:45
Naphthalene mg/kg ND 0.0050 08/08/23 10:45
o-Xylene mg/kg ND 0.0050 08/08/23 10:45
p-Isopropyltoluene mg/kg ND 0.0050 08/08/23 10:45
sec-Butylbenzene mg/kg ND 0.0050 08/08/23 10:45
Styrene mg/kg ND 0.0050 08/08/23 10:45
tert-Butylbenzene mg/kg ND 0.0050 08/08/23 10:45
Tetrachloroethene mg/kg ND 0.0050 08/08/23 10:45
Toluene mg/kg ND 0.0050 08/08/23 10:45
trans-1,2-Dichloroethene mg/kg ND 0.0050 08/08/23 10:45
trans-1,3-Dichloropropene mg/kg ND 0.0050 08/08/23 10:45
Trichloroethene mg/kg ND 0.0050 08/08/23 10:45
Trichlorofluoromethane mg/kg ND 0.0050 v108/08/23 10:45
Vinyl acetate mg/kg ND 0.050 08/08/23 10:45
Vinyl chloride mg/kg ND 0.010 08/08/23 10:45
Xylene (Total)mg/kg ND 0.010 08/08/23 10:45
1,2-Dichloroethane-d4 (S)%112 70-130 08/08/23 10:45
4-Bromofluorobenzene (S)%102 70-130 08/08/23 10:45
Toluene-d8 (S)%101 70-130 08/08/23 10:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4103858LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.480.5 95 70-130
1,1,1-Trichloroethane mg/kg 0.540.5 109 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.480.5 97 70-130
1,1,2-Trichloroethane mg/kg 0.490.5 98 70-130
1,1-Dichloroethane mg/kg 0.530.5 107 70-130
1,1-Dichloroethene mg/kg 0.580.5 116 70-130
1,1-Dichloropropene mg/kg 0.540.5 108 70-130
1,2,3-Trichlorobenzene mg/kg 0.490.5 99 70-130
1,2,3-Trichloropropane mg/kg 0.520.5 103 70-130
1,2,4-Trichlorobenzene mg/kg 0.49 IK0.5 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 39 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4103858LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 0.520.5 104 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.480.5 96 67-130
1,2-Dibromoethane (EDB)mg/kg 0.490.5 97 70-130
1,2-Dichlorobenzene mg/kg 0.470.5 95 70-130
1,2-Dichloroethane mg/kg 0.540.5 109 70-130
1,2-Dichloropropane mg/kg 0.490.5 99 70-130
1,3,5-Trimethylbenzene mg/kg 0.530.5 106 70-130
1,3-Dichlorobenzene mg/kg 0.500.5 100 70-130
1,3-Dichloropropane mg/kg 0.480.5 96 70-130
1,4-Dichlorobenzene mg/kg 0.480.5 96 70-130
2,2-Dichloropropane mg/kg 0.530.5 105 67-130
2-Butanone (MEK)mg/kg 1.11 106 66-130
2-Chlorotoluene mg/kg 0.520.5 103 70-130
2-Hexanone mg/kg 0.951 95 70-130
4-Chlorotoluene mg/kg 0.510.5 103 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.991 99 70-130
Acetone mg/kg 1.01 105 67-130
Benzene mg/kg 0.500.5 101 70-130
Bromobenzene mg/kg 0.480.5 97 70-130
Bromochloromethane mg/kg 0.490.5 97 70-130
Bromodichloromethane mg/kg 0.490.5 99 70-130
Bromoform mg/kg 0.490.5 97 70-130
Bromomethane mg/kg 0.460.5 91 53-175
Carbon tetrachloride mg/kg 0.540.5 108 70-130
Chlorobenzene mg/kg 0.480.5 96 70-130
Chloroethane mg/kg 0.560.5 113 70-135
Chloroform mg/kg 0.520.5 104 70-130
Chloromethane mg/kg 0.570.5 114 64-130
cis-1,2-Dichloroethene mg/kg 0.540.5 108 70-130
cis-1,3-Dichloropropene mg/kg 0.490.5 98 70-130
Dibromochloromethane mg/kg 0.500.5 99 70-130
Dibromomethane mg/kg 0.470.5 94 70-130
Dichlorodifluoromethane mg/kg 0.88 L1,v10.5 176 63-145
Diisopropyl ether mg/kg 0.520.5 104 68-130
Ethylbenzene mg/kg 0.500.5 99 70-130
Hexachloro-1,3-butadiene mg/kg 0.520.5 104 70-130
Isopropylbenzene (Cumene)mg/kg 0.510.5 101 70-130
m&p-Xylene mg/kg 0.971 97 70-130
Methyl-tert-butyl ether mg/kg 0.490.5 97 70-130
Methylene Chloride mg/kg 0.530.5 106 67-130
n-Butylbenzene mg/kg 0.530.5 105 70-130
n-Propylbenzene mg/kg 0.520.5 104 70-130
Naphthalene mg/kg 0.490.5 99 70-130
o-Xylene mg/kg 0.490.5 99 70-130
p-Isopropyltoluene mg/kg 0.510.5 102 70-130
sec-Butylbenzene mg/kg 0.540.5 107 70-130
Styrene mg/kg 0.500.5 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 40 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4103858LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 0.450.5 91 64-130
Tetrachloroethene mg/kg 0.470.5 94 70-130
Toluene mg/kg 0.480.5 95 70-130
trans-1,2-Dichloroethene mg/kg 0.550.5 110 70-130
trans-1,3-Dichloropropene mg/kg 0.470.5 95 70-130
Trichloroethene mg/kg 0.500.5 99 70-130
Trichlorofluoromethane mg/kg 0.64 v10.5 129 70-130
Vinyl acetate mg/kg 1.11 111 70-134
Vinyl chloride mg/kg 0.540.5 107 68-130
Xylene (Total)mg/kg 1.51.5 97 70-130
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4103859MATRIX SPIKE SAMPLE:
MSSpike
Result
92680830001
1,1,1,2-Tetrachloroethane mg/kg 1.21.2 97 58-140<12.5 ug/kg
1,1,1-Trichloroethane mg/kg 1.41.2 111 58-144<12.5 ug/kg
1,1,2,2-Tetrachloroethane mg/kg 1.21.2 97 52-139<12.5 ug/kg
1,1,2-Trichloroethane mg/kg 1.21.2 99 56-140<12.5 ug/kg
1,1-Dichloroethane mg/kg 1.41.2 111 58-145<12.5 ug/kg
1,1-Dichloroethene mg/kg 1.51.2 120 57-158<12.5 ug/kg
1,1-Dichloropropene mg/kg 1.51.2 117 58-151<12.5 ug/kg
1,2,3-Trichlorobenzene mg/kg 1.31.2 101 48-149<12.5 ug/kg
1,2,3-Trichloropropane mg/kg 1.21.2 100 54-132<12.5 ug/kg
1,2,4-Trichlorobenzene mg/kg 1.2 IK1.2 100 51-151<12.5 ug/kg
1,2,4-Trimethylbenzene mg/kg 1.41.2 113 38-17016.8 ug/kg
1,2-Dibromo-3-chloropropane mg/kg 1.01.2 84 44-134<12.5 ug/kg
1,2-Dibromoethane (EDB)mg/kg 1.21.2 96 60-138<12.5 ug/kg
1,2-Dichlorobenzene mg/kg 1.21.2 98 59-147<12.5 ug/kg
1,2-Dichloroethane mg/kg 1.31.2 103 57-139<12.5 ug/kg
1,2-Dichloropropane mg/kg 1.41.2 109 62-145<12.5 ug/kg
1,3,5-Trimethylbenzene mg/kg 1.41.2 113 47-1597.9J ug/kg
1,3-Dichlorobenzene mg/kg 1.31.2 104 58-144<12.5 ug/kg
1,3-Dichloropropane mg/kg 1.21.2 100 60-142<12.5 ug/kg
1,4-Dichlorobenzene mg/kg 1.31.2 103 57-143<12.5 ug/kg
2,2-Dichloropropane mg/kg 1.01.2 82 37-144<12.5 ug/kg
2-Butanone (MEK)mg/kg 2.42.6 95 28-146<250 ug/kg
2-Chlorotoluene mg/kg 1.41.2 109 55-158<12.5 ug/kg
2-Hexanone mg/kg 2.32.6 91 44-141<125 ug/kg
4-Chlorotoluene mg/kg 1.41.2 108 55-146<12.5 ug/kg
4-Methyl-2-pentanone (MIBK)mg/kg 2.32.6 94 50-138<125 ug/kg
Acetone mg/kg 2.32.6 92 20-136<250 ug/kg
Benzene mg/kg 1.41.2 110 60-145<12.5 ug/kg
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 41 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4103859MATRIX SPIKE SAMPLE:
MSSpike
Result
92680830001
Bromobenzene mg/kg 1.31.2 101 59-145<12.5 ug/kg
Bromochloromethane mg/kg 1.21.2 96 57-143<12.5 ug/kg
Bromodichloromethane mg/kg 1.21.2 97 53-133<12.5 ug/kg
Bromoform mg/kg 1.11.2 90 48-133<12.5 ug/kg
Bromomethane mg/kg 1.51.2 120 10-167<49.9 ug/kg
Carbon tetrachloride mg/kg 1.41.2 113 57-147<12.5 ug/kg
Chlorobenzene mg/kg 1.31.2 102 61-144<12.5 ug/kg
Chloroethane mg/kg 1.71.2 135 10-153<25.0 ug/kg
Chloroform mg/kg 1.31.2 107 58-141<12.5 ug/kg
Chloromethane mg/kg 1.61.2 129 54-165<25.0 ug/kg
cis-1,2-Dichloroethene mg/kg 1.41.2 114 59-144<12.5 ug/kg
cis-1,3-Dichloropropene mg/kg 1.21.2 98 56-137<12.5 ug/kg
Dibromochloromethane mg/kg 1.21.2 97 53-139<12.5 ug/kg
Dibromomethane mg/kg 1.21.2 93 60-136<12.5 ug/kg
Dichlorodifluoromethane mg/kg 2.4 M0,v11.2 195 49-177<25.0 ug/kg
Diisopropyl ether mg/kg 1.31.2 105 53-136<12.5 ug/kg
Ethylbenzene mg/kg 1.41.2 110 53-150<12.5 ug/kg
Hexachloro-1,3-butadiene mg/kg 1.61.2 130 42-186<25.0 ug/kg
Isopropylbenzene (Cumene)mg/kg 1.41.2 113 62-154<12.5 ug/kg
m&p-Xylene mg/kg 2.72.6 107 49-156<25.0 ug/kg
Methyl-tert-butyl ether mg/kg 1.21.2 94 54-133<12.5 ug/kg
Methylene Chloride mg/kg 1.41.2 113 50-153<49.9 ug/kg
n-Butylbenzene mg/kg 1.41.2 112 44-174<12.5 ug/kg
n-Propylbenzene mg/kg 1.41.2 111 52-157<12.5 ug/kg
Naphthalene mg/kg 1.21.2 93 37-150<12.5 ug/kg
o-Xylene mg/kg 1.31.2 107 54-150<12.5 ug/kg
p-Isopropyltoluene mg/kg 1.41.2 115 50-164<12.5 ug/kg
sec-Butylbenzene mg/kg 1.51.2 118 58-161<12.5 ug/kg
Styrene mg/kg 1.31.2 107 60-148<12.5 ug/kg
tert-Butylbenzene mg/kg 1.31.2 103 44-151<12.5 ug/kg
Tetrachloroethene mg/kg 1.21.2 97 53-151<12.5 ug/kg
Toluene mg/kg 1.31.2 101 52-148<12.5 ug/kg
trans-1,2-Dichloroethene mg/kg 1.41.2 110 60-148<12.5 ug/kg
trans-1,3-Dichloropropene mg/kg 1.11.2 89 55-133<12.5 ug/kg
Trichloroethene mg/kg 1.31.2 108 60-148<12.5 ug/kg
Trichlorofluoromethane mg/kg 1.4 v11.2 113 10-154<12.5 ug/kg
Vinyl acetate mg/kg 2.42.6 96 50-149<125 ug/kg
Vinyl chloride mg/kg 1.61.2 130 57-157<25.0 ug/kg
Xylene (Total)mg/kg 4.03.8 107 52-153<25.0 ug/kg
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 42 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92680877022
4103860SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg ND IKND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg NDND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg NDND
2-Butanone (MEK)mg/kg NDND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg NDND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg NDND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg NDND
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg NDND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg ND v1ND
Diisopropyl ether mg/kg NDND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Isopropylbenzene (Cumene)mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 43 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92680877022
4103860SAMPLE DUPLICATE:
m&p-Xylene mg/kg NDND
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg NDND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg NDND
o-Xylene mg/kg NDND
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg NDND
Tetrachloroethene mg/kg NDND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg ND v1ND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%109112
4-Bromofluorobenzene (S)%103104
Toluene-d8 (S)%102101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 44 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
791821
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92680269001, 92680269002, 92680269003, 92680269004, 92680269005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4103126
Associated Lab Samples:92680269001, 92680269002, 92680269003, 92680269004, 92680269005
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 08/09/23 07:25
1,2-Dichlorobenzene mg/kg ND 0.33 08/09/23 07:25
1,3-Dichlorobenzene mg/kg ND 0.33 08/09/23 07:25
1,4-Dichlorobenzene mg/kg ND 0.33 08/09/23 07:25
1-Methylnaphthalene mg/kg ND 0.33 08/09/23 07:25
2,4,5-Trichlorophenol mg/kg ND 0.33 08/09/23 07:25
2,4,6-Trichlorophenol mg/kg ND 0.33 08/09/23 07:25
2,4-Dichlorophenol mg/kg ND 0.33 08/09/23 07:25
2,4-Dimethylphenol mg/kg ND 0.33 08/09/23 07:25
2,4-Dinitrophenol mg/kg ND 1.6 08/09/23 07:25
2,4-Dinitrotoluene mg/kg ND 0.33 08/09/23 07:25
2,6-Dinitrotoluene mg/kg ND 0.33 08/09/23 07:25
2-Chloronaphthalene mg/kg ND 0.33 08/09/23 07:25
2-Chlorophenol mg/kg ND 0.33 08/09/23 07:25
2-Methylnaphthalene mg/kg ND 0.33 08/09/23 07:25
2-Methylphenol(o-Cresol)mg/kg ND 0.33 08/09/23 07:25
2-Nitroaniline mg/kg ND 1.6 08/09/23 07:25
2-Nitrophenol mg/kg ND 0.33 08/09/23 07:25
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 08/09/23 07:25
3,3'-Dichlorobenzidine mg/kg ND 0.65 08/09/23 07:25
3-Nitroaniline mg/kg ND 1.6 08/09/23 07:25
4,6-Dinitro-2-methylphenol mg/kg ND 0.65 08/09/23 07:25
4-Bromophenylphenyl ether mg/kg ND 0.33 08/09/23 07:25
4-Chloro-3-methylphenol mg/kg ND 0.65 08/09/23 07:25
4-Chloroaniline mg/kg ND 0.65 08/09/23 07:25
4-Chlorophenylphenyl ether mg/kg ND 0.33 08/09/23 07:25
4-Nitroaniline mg/kg ND 0.65 08/09/23 07:25
4-Nitrophenol mg/kg ND 1.6 08/09/23 07:25
Acenaphthene mg/kg ND 0.33 08/09/23 07:25
Acenaphthylene mg/kg ND 0.33 08/09/23 07:25
Anthracene mg/kg ND 0.33 08/09/23 07:25
Benzo(a)anthracene mg/kg ND 0.33 08/09/23 07:25
Benzo(a)pyrene mg/kg ND 0.33 08/09/23 07:25
Benzo(b)fluoranthene mg/kg ND 0.33 08/09/23 07:25
Benzo(g,h,i)perylene mg/kg ND 0.33 08/09/23 07:25
Benzo(k)fluoranthene mg/kg ND 0.33 08/09/23 07:25
Benzoic Acid mg/kg ND 1.6 08/09/23 07:25
Benzyl alcohol mg/kg ND 0.65 08/09/23 07:25
bis(2-Chloroethoxy)methane mg/kg ND 0.33 08/09/23 07:25
bis(2-Chloroethyl) ether mg/kg ND 0.33 08/09/23 07:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 45 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4103126
Associated Lab Samples:92680269001, 92680269002, 92680269003, 92680269004, 92680269005
Matrix:Solid
Analyzed
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 08/09/23 07:25
Butylbenzylphthalate mg/kg ND 0.33 08/09/23 07:25
Chrysene mg/kg ND 0.33 08/09/23 07:25
Di-n-butylphthalate mg/kg ND 0.33 08/09/23 07:25
Di-n-octylphthalate mg/kg ND 0.33 08/09/23 07:25
Dibenz(a,h)anthracene mg/kg ND 0.33 08/09/23 07:25
Dibenzofuran mg/kg ND 0.33 08/09/23 07:25
Diethylphthalate mg/kg ND 0.33 08/09/23 07:25
Dimethylphthalate mg/kg ND 0.33 08/09/23 07:25
Fluoranthene mg/kg ND 0.33 08/09/23 07:25
Fluorene mg/kg ND 0.33 08/09/23 07:25
Hexachloro-1,3-butadiene mg/kg ND 0.33 08/09/23 07:25
Hexachlorobenzene mg/kg ND 0.33 08/09/23 07:25
Hexachlorocyclopentadiene mg/kg ND 0.33 08/09/23 07:25
Hexachloroethane mg/kg ND 0.33 08/09/23 07:25
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 08/09/23 07:25
Isophorone mg/kg ND 0.33 08/09/23 07:25
N-Nitroso-di-n-propylamine mg/kg ND 0.33 08/09/23 07:25
N-Nitrosodimethylamine mg/kg ND 0.33 08/09/23 07:25
N-Nitrosodiphenylamine mg/kg ND 0.33 08/09/23 07:25
Naphthalene mg/kg ND 0.33 08/09/23 07:25
Nitrobenzene mg/kg ND 0.33 08/09/23 07:25
Pentachlorophenol mg/kg ND 0.65 08/09/23 07:25
Phenanthrene mg/kg ND 0.33 08/09/23 07:25
Phenol mg/kg ND 0.33 08/09/23 07:25
Pyrene mg/kg ND 0.33 08/09/23 07:25
2,4,6-Tribromophenol (S)%62 10-131 08/09/23 07:25
2-Fluorobiphenyl (S)%55 10-130 08/09/23 07:25
2-Fluorophenol (S)%61 10-130 08/09/23 07:25
Nitrobenzene-d5 (S)%61 10-130 08/09/23 07:25
Phenol-d6 (S)%59 10-130 08/09/23 07:25
Terphenyl-d14 (S)%57 10-130 08/09/23 07:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4103127LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.01.6 62 43-130
1,2-Dichlorobenzene mg/kg 1.01.6 61 43-130
1,3-Dichlorobenzene mg/kg 1.01.6 62 43-130
1,4-Dichlorobenzene mg/kg 1.01.6 62 44-130
1-Methylnaphthalene mg/kg 1.11.6 67 47-130
2,4,5-Trichlorophenol mg/kg 1.11.6 65 47-130
2,4,6-Trichlorophenol mg/kg 1.11.6 67 47-130
2,4-Dichlorophenol mg/kg 1.11.6 66 45-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 46 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4103127LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dimethylphenol mg/kg 1.11.6 67 45-130
2,4-Dinitrophenol mg/kg 4.08.2 48 27-140
2,4-Dinitrotoluene mg/kg 1.01.6 61 46-130
2,6-Dinitrotoluene mg/kg 1.01.6 62 48-130
2-Chloronaphthalene mg/kg 1.01.6 62 46-130
2-Chlorophenol mg/kg 1.21.6 71 43-130
2-Methylnaphthalene mg/kg 1.11.6 64 47-130
2-Methylphenol(o-Cresol)mg/kg 1.11.6 66 42-130
2-Nitroaniline mg/kg 2.13.3 64 41-130
2-Nitrophenol mg/kg 1.11.6 69 48-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.11.6 66 39-130
3,3'-Dichlorobenzidine mg/kg 1.93.3 58 41-130
3-Nitroaniline mg/kg 1.93.3 59 37-130
4,6-Dinitro-2-methylphenol mg/kg 1.83.3 55 38-141
4-Bromophenylphenyl ether mg/kg 1.11.6 65 47-130
4-Chloro-3-methylphenol mg/kg 2.23.3 66 44-130
4-Chloroaniline mg/kg 2.03.3 60 41-130
4-Chlorophenylphenyl ether mg/kg 1.01.6 63 45-130
4-Nitroaniline mg/kg 1.93.3 58 42-130
4-Nitrophenol mg/kg 5.48.2 66 39-131
Acenaphthene mg/kg 1.11.6 64 49-130
Acenaphthylene mg/kg 1.11.6 65 50-130
Anthracene mg/kg 1.01.6 61 49-130
Benzo(a)anthracene mg/kg 1.11.6 65 51-130
Benzo(a)pyrene mg/kg 0.901.6 55 51-130
Benzo(b)fluoranthene mg/kg 0.951.6 57 49-130
Benzo(g,h,i)perylene mg/kg 0.951.6 58 48-140
Benzo(k)fluoranthene mg/kg 0.931.6 57 51-130
Benzoic Acid mg/kg 3.48.2 41 22-130
Benzyl alcohol mg/kg 2.23.3 67 43-130
bis(2-Chloroethoxy)methane mg/kg 1.11.6 65 43-130
bis(2-Chloroethyl) ether mg/kg 1.11.6 64 42-130
bis(2-Ethylhexyl)phthalate mg/kg 0.961.6 58 43-130
Butylbenzylphthalate mg/kg 0.941.6 57 44-131
Chrysene mg/kg 1.11.6 66 51-130
Di-n-butylphthalate mg/kg 1.01.6 62 46-130
Di-n-octylphthalate mg/kg 0.991.6 60 45-130
Dibenz(a,h)anthracene mg/kg 0.921.6 56 48-130
Dibenzofuran mg/kg 1.01.6 62 10-130
Diethylphthalate mg/kg 1.01.6 61 48-130
Dimethylphthalate mg/kg 1.01.6 62 48-130
Fluoranthene mg/kg 1.11.6 66 48-130
Fluorene mg/kg 1.11.6 66 48-130
Hexachloro-1,3-butadiene mg/kg 0.991.6 60 39-130
Hexachlorobenzene mg/kg 1.11.6 65 47-130
Hexachlorocyclopentadiene mg/kg 0.701.6 42 17-130
Hexachloroethane mg/kg 1.01.6 63 40-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 47 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4103127LABORATORY CONTROL SAMPLE:
LCSSpike
Indeno(1,2,3-cd)pyrene mg/kg 0.901.6 54 50-130
Isophorone mg/kg 1.11.6 64 41-130
N-Nitroso-di-n-propylamine mg/kg 1.11.6 65 36-130
N-Nitrosodimethylamine mg/kg 1.11.6 65 34-130
N-Nitrosodiphenylamine mg/kg 1.11.6 66 48-130
Naphthalene mg/kg 1.11.6 67 46-130
Nitrobenzene mg/kg 1.11.6 64 39-130
Pentachlorophenol mg/kg 2.23.3 66 42-130
Phenanthrene mg/kg 1.11.6 66 50-130
Phenol mg/kg 1.11.6 69 42-130
Pyrene mg/kg 1.01.6 62 50-130
2,4,6-Tribromophenol (S)%70 10-131
2-Fluorobiphenyl (S)%58 10-130
2-Fluorophenol (S)%63 10-130
Nitrobenzene-d5 (S)%61 10-130
Phenol-d6 (S)%62 10-130
Terphenyl-d14 (S)%54 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4103128MATRIX SPIKE SAMPLE:
MSSpike
Result
92680269003
1,2,4-Trichlorobenzene mg/kg 1.02.1 50 16-130ND
1,2-Dichlorobenzene mg/kg 1.02.1 50 19-130ND
1,3-Dichlorobenzene mg/kg 1.02.1 49 19-130ND
1,4-Dichlorobenzene mg/kg 1.02.1 51 20-130ND
1-Methylnaphthalene mg/kg 1.42.1 58 19-130ND
2,4,5-Trichlorophenol mg/kg 1.12.1 55 19-130ND
2,4,6-Trichlorophenol mg/kg 1.22.1 57 18-130ND
2,4-Dichlorophenol mg/kg 1.12.1 53 16-130ND
2,4-Dimethylphenol mg/kg 1.22.1 56 10-130ND
2,4-Dinitrophenol mg/kg 4.610.3 45 10-143ND
2,4-Dinitrotoluene mg/kg 1.12.1 52 19-130ND
2,6-Dinitrotoluene mg/kg 1.12.1 53 22-130ND
2-Chloronaphthalene mg/kg 1.12.1 52 18-130ND
2-Chlorophenol mg/kg 1.22.1 57 20-130ND
2-Methylnaphthalene mg/kg 1.82.1 62 18-1300.50
2-Methylphenol(o-Cresol)mg/kg 1.22.1 57 13-130ND
2-Nitroaniline mg/kg 2.24.2 54 18-130ND
2-Nitrophenol mg/kg 1.12.1 54 19-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.22.1 57 13-130ND
3,3'-Dichlorobenzidine mg/kg 2.04.2 48 10-130ND
3-Nitroaniline mg/kg 2.14.2 50 22-130ND
4,6-Dinitro-2-methylphenol mg/kg 2.14.2 50 10-144ND
4-Bromophenylphenyl ether mg/kg 1.12.1 53 18-130ND
4-Chloro-3-methylphenol mg/kg 2.24.2 53 16-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
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[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4103128MATRIX SPIKE SAMPLE:
MSSpike
Result
92680269003
4-Chloroaniline mg/kg 2.04.2 48 17-130ND
4-Chlorophenylphenyl ether mg/kg 1.12.1 52 17-130ND
4-Nitroaniline mg/kg 2.04.2 48 21-130ND
4-Nitrophenol mg/kg 5.510.3 53 13-131ND
Acenaphthene mg/kg 1.12.1 55 20-130ND
Acenaphthylene mg/kg 1.12.1 55 21-130ND
Anthracene mg/kg 1.02.1 50 19-130ND
Benzo(a)anthracene mg/kg 1.02.1 51 17-130ND
Benzo(a)pyrene mg/kg 0.862.1 42 14-130ND
Benzo(b)fluoranthene mg/kg 0.892.1 43 11-134ND
Benzo(g,h,i)perylene mg/kg 0.882.1 43 12-130ND
Benzo(k)fluoranthene mg/kg 0.882.1 43 15-130ND
Benzoic Acid mg/kg 3.610.3 35 10-130ND
Benzyl alcohol mg/kg 2.34.2 56 20-130ND
bis(2-Chloroethoxy)methane mg/kg 1.12.1 54 16-130ND
bis(2-Chloroethyl) ether mg/kg 1.12.1 53 18-130ND
bis(2-Ethylhexyl)phthalate mg/kg 0.932.1 45 11-130ND
Butylbenzylphthalate mg/kg 0.972.1 47 10-130ND
Chrysene mg/kg 1.12.1 52 17-130ND
Di-n-butylphthalate mg/kg 1.02.1 50 16-130ND
Di-n-octylphthalate mg/kg 0.952.1 46 16-130ND
Dibenz(a,h)anthracene mg/kg 0.842.1 41 13-130ND
Dibenzofuran mg/kg 1.12.1 52 19-130ND
Diethylphthalate mg/kg 1.12.1 54 22-130ND
Dimethylphthalate mg/kg 1.12.1 54 23-130ND
Fluoranthene mg/kg 1.12.1 52 14-130ND
Fluorene mg/kg 1.12.1 54 19-130ND
Hexachloro-1,3-butadiene mg/kg 0.942.1 45 12-130ND
Hexachlorobenzene mg/kg 1.12.1 52 17-130ND
Hexachlorocyclopentadiene mg/kg 0.702.1 34 10-130ND
Hexachloroethane mg/kg 1.42.1 66 14-130ND
Indeno(1,2,3-cd)pyrene mg/kg 0.822.1 40 13-130ND
Isophorone mg/kg 1.12.1 52 17-130ND
N-Nitroso-di-n-propylamine mg/kg 1.22.1 56 10-130ND
N-Nitrosodimethylamine mg/kg 1.02.1 51 16-130ND
N-Nitrosodiphenylamine mg/kg 1.12.1 55 19-130ND
Naphthalene mg/kg 1.82.1 60 18-1300.57
Nitrobenzene mg/kg 1.02.1 49 15-130ND
Pentachlorophenol mg/kg 2.34.2 56 10-130ND
Phenanthrene mg/kg 1.12.1 54 17-130ND
Phenol mg/kg 1.12.1 56 15-130ND
Pyrene mg/kg 1.12.1 51 31-130ND
2,4,6-Tribromophenol (S)%57 10-131
2-Fluorobiphenyl (S)%45 10-130
2-Fluorophenol (S)%50 10-130
Nitrobenzene-d5 (S)%47 10-130
Phenol-d6 (S)%49 10-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
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2225 Riverside Dr.
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[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4103128MATRIX SPIKE SAMPLE:
MSSpike
Result
92680269003
Terphenyl-d14 (S)%39 10-130
Parameter Units
Dup
Result QualifiersRPDResult
92680269004
4103129SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
1-Methylnaphthalene mg/kg NDND
2,4,5-Trichlorophenol mg/kg NDND
2,4,6-Trichlorophenol mg/kg NDND
2,4-Dichlorophenol mg/kg NDND
2,4-Dimethylphenol mg/kg NDND
2,4-Dinitrophenol mg/kg NDND
2,4-Dinitrotoluene mg/kg NDND
2,6-Dinitrotoluene mg/kg NDND
2-Chloronaphthalene mg/kg NDND
2-Chlorophenol mg/kg NDND
2-Methylnaphthalene mg/kg NDND
2-Methylphenol(o-Cresol)mg/kg NDND
2-Nitroaniline mg/kg NDND
2-Nitrophenol mg/kg NDND
3&4-Methylphenol(m&p Cresol)mg/kg NDND
3,3'-Dichlorobenzidine mg/kg NDND
3-Nitroaniline mg/kg NDND
4,6-Dinitro-2-methylphenol mg/kg NDND
4-Bromophenylphenyl ether mg/kg NDND
4-Chloro-3-methylphenol mg/kg NDND
4-Chloroaniline mg/kg NDND
4-Chlorophenylphenyl ether mg/kg NDND
4-Nitroaniline mg/kg NDND
4-Nitrophenol mg/kg NDND
Acenaphthene mg/kg NDND
Acenaphthylene mg/kg NDND
Anthracene mg/kg NDND
Benzo(a)anthracene mg/kg NDND
Benzo(a)pyrene mg/kg NDND
Benzo(b)fluoranthene mg/kg NDND
Benzo(g,h,i)perylene mg/kg NDND
Benzo(k)fluoranthene mg/kg NDND
Benzoic Acid mg/kg NDND
Benzyl alcohol mg/kg NDND
bis(2-Chloroethoxy)methane mg/kg NDND
bis(2-Chloroethyl) ether mg/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
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Asheville, NC 28804
[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92680269004
4103129SAMPLE DUPLICATE:
bis(2-Ethylhexyl)phthalate mg/kg NDND
Butylbenzylphthalate mg/kg NDND
Chrysene mg/kg NDND
Di-n-butylphthalate mg/kg NDND
Di-n-octylphthalate mg/kg NDND
Dibenz(a,h)anthracene mg/kg NDND
Dibenzofuran mg/kg NDND
Diethylphthalate mg/kg NDND
Dimethylphthalate mg/kg NDND
Fluoranthene mg/kg NDND
Fluorene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Hexachlorobenzene mg/kg NDND
Hexachlorocyclopentadiene mg/kg NDND
Hexachloroethane mg/kg NDND
Indeno(1,2,3-cd)pyrene mg/kg NDND
Isophorone mg/kg NDND
N-Nitroso-di-n-propylamine mg/kg NDND
N-Nitrosodimethylamine mg/kg NDND
N-Nitrosodiphenylamine mg/kg NDND
Naphthalene mg/kg NDND
Nitrobenzene mg/kg NDND
Pentachlorophenol mg/kg NDND
Phenanthrene mg/kg NDND
Phenol mg/kg NDND
Pyrene mg/kg NDND
2,4,6-Tribromophenol (S)%5151
2-Fluorobiphenyl (S)%4444
2-Fluorophenol (S)%4847
Nitrobenzene-d5 (S)%4849
Phenol-d6 (S)%4846
Terphenyl-d14 (S)%4646
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 51 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
791909
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92680269001, 92680269002, 92680269003, 92680269004, 92680269005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4103605
Associated Lab Samples:92680269001, 92680269002, 92680269003, 92680269004, 92680269005
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.0 N208/09/23 12:04
Aliphatic (C19-C36)mg/kg ND 10.0 N208/09/23 12:04
Aromatic (C11-C22)mg/kg ND 10.0 N208/09/23 12:04
1-Chlorooctadecane (S)%90 40-140 08/09/23 12:04
2-Bromonaphthalene (S)%83 40-140 08/09/23 12:04
2-Fluorobiphenyl (S)%85 40-140 08/09/23 12:04
o-Terphenyl (S)%64 40-140 08/09/23 12:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4103606LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
4103607
Aliphatic (C09-C18)mg/kg ND N2105940-14063ND 50
Aliphatic (C19-C36)mg/kg 13.7 N213.4 102 40-14010814.4 5 50
Aromatic (C11-C22)mg/kg 20.7 N228.4 73 40-1408825.0 19 50
1-Chlorooctadecane (S)%98 40-140101
2-Bromonaphthalene (S)%50 40-14069
2-Fluorobiphenyl (S)%56 40-14078
o-Terphenyl (S)%69 40-14083
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
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[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
791247
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92680269001, 92680269002, 92680269003, 92680269004
Parameter Units
Dup
Result QualifiersRPDResult
92680256003
4100598SAMPLE DUPLICATE:
Percent Moisture %20.5 N2419.6
Parameter Units
Dup
Result QualifiersRPDResult
92680269004
4100599SAMPLE DUPLICATE:
Percent Moisture %19.8 N2119.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 53 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92680269
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
791258
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92680269005
Parameter Units
Dup
Result QualifiersRPDResult
92680439001
4100645SAMPLE DUPLICATE:
Percent Moisture %5.0 N224.9
Parameter Units
Dup
Result QualifiersRPDResult
92680587001
4100646SAMPLE DUPLICATE:
Percent Moisture %11.4 N2311.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
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Asheville, NC 28804
[phone]
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92680269
ONE STOP 15
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in theassociated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
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2225 Riverside Dr.
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[phone]
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92680269
ONE STOP 15
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92680269001 791909 792358SOIL-F MADEP EPH MADEP EPH
92680269002 791909 792358SOIL-G MADEP EPH MADEP EPH
92680269003 791909 792358SOIL-H MADEP EPH MADEP EPH
92680269004 791909 792358SOIL-I MADEP EPH MADEP EPH
92680269005 791909 792358SOIL-J MADEP EPH MADEP EPH
92680269001 791821 792333SOIL-F EPA 3546 EPA 8270E
92680269002 791821 792333SOIL-G EPA 3546 EPA 8270E
92680269003 791821 792333SOIL-H EPA 3546 EPA 8270E
92680269004 791821 792333SOIL-I EPA 3546 EPA 8270E
92680269005 791821 792333SOIL-J EPA 3546 EPA 8270E
92680269001 791966 792100SOIL-F EPA 5035A/5030B EPA 8260D
92680269002 791331 791571SOIL-G EPA 5035A/5030B EPA 8260D
92680269003 791331 791571SOIL-H EPA 5035A/5030B EPA 8260D
92680269004 791331 791571SOIL-I EPA 5035A/5030B EPA 8260D
92680269005 791348 791794SOIL-J EPA 5035A/5030B EPA 8260D
92680269001 791247SOIL-F SW-846
92680269002 791247SOIL-G SW-846
92680269003 791247SOIL-H SW-846
92680269004 791247SOIL-I SW-846
92680269005 791258SOIL-J SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 10:47 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 56 of 81
Page 57 of 81
Page 58 of 81
Page 59 of 81
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
August 15, 2023
Matthew Brainard
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: NC
Client Job Number:
Project Number: 92680269
Laboratory Work Order Number: 23H0909
Enclosed are results of analyses for samples as received by the laboratory on August 4, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
Page 1 of 22
Table of Contents
Page 60 of 81
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
23H0909-01 5
23H0909-02 7
23H0909-03 9
23H0909-04 11
23H0909-05 13
Sample Preparation Information 15
QC Data 16
Petroleum Hydrocarbons Analyses - VPH 16
B348077 16
B348320 16
Flag/Qualifier Summary 17
Certifications 18
Chain of Custody/Sample Receipt 19
Page 2 of 22
Table of Contents
Page 61 of 81
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
8/15/2023
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
ATTN: Matthew Brainard
92680269
23H0909
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
NC
SOIL-F 23H0909-01 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-G 23H0909-02 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-H 23H0909-03 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-I 23H0909-04 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SOIL-J 23H0909-05 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
[TOC_1]Sample Summary[TOC]
Page 3 of 22
Table of Contents
Page 62 of 81
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
MADEP-VPH-Feb 2018 Rev 2.1
Qualifications:
Soil/methanol ratio does not meet method specifications. Insufficient amount of soil. Data validation is not affected since a sufficient amount
of preservative is present. Detection limits may be above useful levels.
Analyte & Samples(s) Qualified:
O-02
23H0909-01[SOIL-F], 23H0909-02[SOIL-G], 23H0909-03[SOIL-H]
Elevated reporting limit due to high concentration of target compounds. MA CAM reporting limit not met.
Analyte & Samples(s) Qualified:
RL-05
23H0909-01[SOIL-F]
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 4 of 22
Table of Contents
Page 63 of 81
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/4/2023
Work Order: 23H0909Sample Description:Project Location: NC
Sample ID: 23H0909-01
Field Sample #: SOIL-F
Sample Matrix: Soil
Sampled: 8/1/2023 13:30
[TOC_2]23H0909-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: O-02, RL-05
Soil/Methanol Preservation Ratio: 0.62
Petroleum Hydrocarbons Analyses - VPH
280 180 8/8/23 23:45 KDKmg/Kg dry 8/8/23MADEP-VPH-Feb 2018
Rev 2.1
8Unadjusted C5-C8 Aliphatics
250 180 8/8/23 23:45 KDKmg/Kg dry 8/8/23MADEP-VPH-Feb 2018
Rev 2.1
8C5-C8 Aliphatics
780 180 8/8/23 23:45 KDKmg/Kg dry 8/8/23MADEP-VPH-Feb 2018
Rev 2.1
8Unadjusted C9-C12 Aliphatics
130 180 8/8/23 23:45 KDKmg/Kg dry 8/8/23MADEP-VPH-Feb 2018
Rev 2.1
8C9-C12 Aliphatics
470 180 8/8/23 23:45 KDKmg/Kg dry 8/8/23MADEP-VPH-Feb 2018
Rev 2.1
8C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)101 8/8/23 23:4570-130
2,5-Dibromotoluene (PID)102 8/8/23 23:4570-130
[TOC_1]Sample Results[TOC]
Page 5 of 22
Table of Contents
Page 64 of 81
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/4/2023
Work Order: 23H0909Sample Description:Project Location: NC
Sample ID: 23H0909-01
Field Sample #: SOIL-F
Sample Matrix: Soil
Sampled: 8/1/2023 13:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
79.7 8/8/23 8:22 ADB% Wt 8/8/23SM 2540G1% Solids
Page 6 of 22
Table of Contents
Page 65 of 81
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/4/2023
Work Order: 23H0909Sample Description:Project Location: NC
Sample ID: 23H0909-02
Field Sample #: SOIL-G
Sample Matrix: Soil
Sampled: 8/1/2023 13:40
[TOC_2]23H0909-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: O-02
Soil/Methanol Preservation Ratio: 0.59
Petroleum Hydrocarbons Analyses - VPH
23 24 8/7/23 21:22 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
23 24 8/7/23 21:22 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
22 24 8/7/23 21:22 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
21 24 8/7/23 21:22 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
18 24 8/7/23 21:22 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)97.0 8/7/23 21:2270-130
2,5-Dibromotoluene (PID)97.4 8/7/23 21:2270-130
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Date Received: 8/4/2023
Work Order: 23H0909Sample Description:Project Location: NC
Sample ID: 23H0909-02
Field Sample #: SOIL-G
Sample Matrix: Soil
Sampled: 8/1/2023 13:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
78.8 8/8/23 8:22 ADB% Wt 8/8/23SM 2540G1% Solids
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Date Received: 8/4/2023
Work Order: 23H0909Sample Description:Project Location: NC
Sample ID: 23H0909-03
Field Sample #: SOIL-H
Sample Matrix: Soil
Sampled: 8/1/2023 15:00
[TOC_2]23H0909-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: O-02
Soil/Methanol Preservation Ratio: 0.74
Petroleum Hydrocarbons Analyses - VPH
14 18 8/7/23 21:52 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
14 18 8/7/23 21:52 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
31 18 8/7/23 21:52 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
6.7 18 8/7/23 21:52 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
23 18 8/7/23 21:52 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)106 8/7/23 21:5270-130
2,5-Dibromotoluene (PID)107 8/7/23 21:5270-130
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Date Received: 8/4/2023
Work Order: 23H0909Sample Description:Project Location: NC
Sample ID: 23H0909-03
Field Sample #: SOIL-H
Sample Matrix: Soil
Sampled: 8/1/2023 15:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
82.9 8/8/23 8:22 ADB% Wt 8/8/23SM 2540G1% Solids
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Date Received: 8/4/2023
Work Order: 23H0909Sample Description:Project Location: NC
Sample ID: 23H0909-04
Field Sample #: SOIL-I
Sample Matrix: Soil
Sampled: 8/1/2023 16:00
[TOC_2]23H0909-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.04
Petroleum Hydrocarbons Analyses - VPH
12 21 8/7/23 22:21 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
12 21 8/7/23 22:21 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
3.2 21 8/7/23 22:21 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
3.2 21 8/7/23 22:21 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
1.4 21 8/7/23 22:21 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)87.2 8/7/23 22:2170-130
2,5-Dibromotoluene (PID)88.0 8/7/23 22:2170-130
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Date Received: 8/4/2023
Work Order: 23H0909Sample Description:Project Location: NC
Sample ID: 23H0909-04
Field Sample #: SOIL-I
Sample Matrix: Soil
Sampled: 8/1/2023 16:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
63.0 8/8/23 8:22 ADB% Wt 8/8/23SM 2540G1% Solids
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Date Received: 8/4/2023
Work Order: 23H0909Sample Description:Project Location: NC
Sample ID: 23H0909-05
Field Sample #: SOIL-J
Sample Matrix: Soil
Sampled: 8/1/2023 17:00
[TOC_2]23H0909-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.02
Petroleum Hydrocarbons Analyses - VPH
14 20 8/7/23 22:51 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
14 20 8/7/23 22:51 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
2.9 20 8/7/23 22:51 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
2.9 20 8/7/23 22:51 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
1.9 20 8/7/23 22:51 KDKmg/Kg dry 8/4/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)91.0 8/7/23 22:5170-130
2,5-Dibromotoluene (PID)93.3 8/7/23 22:5170-130
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Date Received: 8/4/2023
Work Order: 23H0909Sample Description:Project Location: NC
Sample ID: 23H0909-05
Field Sample #: SOIL-J
Sample Matrix: Soil
Sampled: 8/1/2023 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
66.0 8/8/23 8:22 ADB% Wt 8/8/23SM 2540G1% Solids
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Sample Extraction Data
Prep Method:MA VPH Analytical Method:MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B348077 08/04/235.90 11.223H0909-02 [SOIL-G]
B348077 08/04/237.39 11.323H0909-03 [SOIL-H]
B348077 08/04/2310.4 13.923H0909-04 [SOIL-I]
B348077 08/04/2310.2 13.423H0909-05 [SOIL-J]
Prep Method:MA VPH Analytical Method:MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B348320 08/08/236.21 11.323H0909-01 [SOIL-F]
Prep Method:% Solids Analytical Method:SM 2540G
Lab Number [Field ID]Batch Date
B348315 08/08/2323H0909-01 [SOIL-F]
B348315 08/08/2323H0909-02 [SOIL-G]
B348315 08/08/2323H0909-03 [SOIL-H]
B348315 08/08/2323H0909-04 [SOIL-I]
B348315 08/08/2323H0909-05 [SOIL-J]
[TOC_1]Sample Preparation Information[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B348077 - MA VPH
[TOC_3]B348077[TOC]
Blank (B348077-BLK1) Prepared: 08/04/23 Analyzed: 08/07/23
Unadjusted C5-C8 Aliphatics mg/Kg wet106.1
C5-C8 Aliphatics mg/Kg wet106.1
Unadjusted C9-C12 Aliphatics mg/Kg wet101.7
C9-C12 Aliphatics mg/Kg wet101.7
C9-C10 Aromatics mg/Kg wet100.69
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)88.935.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)88.935.5
LCS (B348077-BS1) Prepared: 08/04/23 Analyzed: 08/07/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 70-1301178.79
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 70-1301067.98
C9-C10 Aromatics mg/Kg wet10 2.50 70-1301022.54
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10241.0
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10642.3
LCS Dup (B348077-BSD1) Prepared: 08/04/23 Analyzed: 08/07/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 2570-130121 2.989.05
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 2570-130108 1.828.13
C9-C10 Aromatics mg/Kg wet10 2.50 2570-130105 3.232.62
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)99.139.6
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)99.239.7
Batch B348320 - MA VPH
[TOC_3]B348320[TOC]
Blank (B348320-BLK1) Prepared & Analyzed: 08/08/23
Unadjusted C5-C8 Aliphatics mg/Kg wet108.7
C5-C8 Aliphatics mg/Kg wet108.7
Unadjusted C9-C12 Aliphatics mg/Kg wet101.1
C9-C12 Aliphatics mg/Kg wet101.1
C9-C10 Aromatics mg/Kg wet100.59
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)93.337.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)93.037.2
LCS (B348320-BS1) Prepared & Analyzed: 08/08/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 70-1301098.16
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 70-1301047.83
C9-C10 Aromatics mg/Kg wet10 2.50 70-13097.52.44
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)97.238.9
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)97.739.1
LCS Dup (B348320-BSD1) Prepared & Analyzed: 08/08/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 2570-130109 0.04418.16
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 2570-130104 0.7727.77
C9-C10 Aromatics mg/Kg wet10 2.50 2570-13096.6 0.8942.42
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10140.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)97.338.9
[TOC_1]QC Data[TOC]
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Soil/methanol ratio does not meet method specifications. Insufficient amount of soil. Data validation is not
affected since a sufficient amount of preservative is present. Detection limits may be above useful levels.
O-02
Elevated reporting limit due to high concentration of target compounds. MA CAM reporting limit not met.RL-05
[TOC_1]Flag/Qualifier Summary[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2025
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023
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