AS-3731_28861_CA_MRP_20230915

AUGUST 2023
GROUNDWATER
MONITORING REPORT

for the
ONE STOP #15 146 Wiggins Road Candler, Buncombe County, North Carolina Incident #28861

PREPARED FOR: Samir Enterprises, LLC.
PO Box 1272 Old Fort, NC 28762 PREPARED BY: Singleton Environmental, Inc. PO Box 604 Fletcher, NC 28732 [phone]

September 15, 2023

Singleton Environmental, Inc.
Groundwater Monitoring Report with MMPE One Stop #15 Candler, North Carolina

GROUNDWATER MONITORING REPORT September 15, 2023
Incident Number: 28861 Site Name: One Stop #15 146 Wiggins Road Candler, NC 28715
Incident Number: 28861 Facility ID Number: 0-0021101 UST Responsible Party: Samir Enterprises, LLC.
PO Box 1272
Old Fort, NC 28762 Consultant / Contractor: Singleton Environmental, Inc. PO Box 604
Fletcher, NC 28732
Telephone: [phone] Date Release Discovered: June 6, 2012
Estimated Quantity of Release: Unknown/unquantified Cause/Source of Release: Dispenser Islands
Latitude: 35.5432° North
Longitude: -82.7530° West Signature and Seal of Certifying Professional Engineer:
I, Christopher D. Singleton, a North Carolina Professional Geologist, do certify that the
information contained in this report is correct and accurate to the best of my knowledge. ____________________________________ Christopher D. Singleton, P.G. #1928
Singleton Environmental, Inc. is licensed to practice geology in North Carolina. The
certification number of the company is C-443.

Groundwater Monitoring Report with MMPE One Stop #15 Candler, North Carolina

Table of Contents Introduction ..................................................................................................................................... 1 Site History and Source Characterization…......................…………......................................... .... 1 Summary of USTs …......................…………......................................... ................................ 1
Source of Release…......................…………......................................... .................................. 1
Summary of Assessment Activities and Corrective Actions……......................................... .. 1 Receptor Information…......................…………......................................... ................................... 2 Site Geology and Hydrogeology…......................…………......................................... .................. 2 MW-1R Installation Activities…......................…………......................................... ..................... 2
Post Excavation Groundwater Sampling Activities ...............………….........................................3
Conclusions and Recommendations…..................…………......................................... ................ 4 Tables
Table 1. Groundwater Levels
Table 2. Groundwater Analytical Results Figures
Figure 1. Site Vicinity Map
Figure 2. Site Map Figure 3. Groundwater Elevation Contour Map Figure 4. Groundwater Sampling Locations with MCLs and GCLs
Appendices
Appendix A. Field Notes and Monitoring Well MW-1R Records Appendix B. Laboratory Analytical Report

Introduction This report presents the results of the Groundwater Monitoring Report conducted to evaluate the groundwater contamination post UST removal and soil excavation activities related to a petroleum
release from the previous underground storage tank (UST) system at the One Stop #15, located at
146 Wiggins Road in Candler, North Carolina. Figure 1 shows the site location, and Figure 2 presents a site map showing the location of the current UST system, monitoring wells, and soil sampling locations.
Site History and Source Characterization
Summary of USTs The following table summarizes information about the USTs at the site:
Tank No.
Volume (gallons)
Contents (i.e., gasoline, diesel, kerosene, heating oil, waste oil, etc.)
Use (resale, heating building, distribution, farm or residential, etc.)
Date last used
Indicate whether UST has been removed or closed in place
Date of permanent closure (if applicable)
Was a release detected from this UST system? If yes, give date.
1 10,000 Gasoline Resale 6/9/23 Removed 6/9/23 No
2 10,000 Gasoline Resale 6/9/23 Removed 6/9/23 Yes 6/9/23
3 10,000 Diesel Resale 6/9/23 Removed 6/9/23 Yes 6/9/23
4 4,000 Kerosene Resale 6/9/23 Removed 6/9/23 No

Responsible Party: Samir Enterprises, LLC.
PO Box 1272
Old Fort, NC 28762
Source of Release
The source of the release is a dispenser located adjacent to MW-1 that is currently a part of the active UST system at the Site. The UST system is currently used as a petroleum retail station. During the June 2023 UST removal activities, a release was confirmed underneath the previous gas and diesel USTs.
Summary of Assessment Activities and Corrective Actions The petroleum release at the One Stop #15 was confirmed during a June 2012 Site Check.

To date, nine groundwater monitoring wells (MW-1R through MW-9) are located at the Site. Historically free-product has been observed in monitoring well MW-1 and dissolved phase

petroleum compounds above the State 2L standards have been detected in monitoring wells MW-2, MW-3, MW-4, MW-8, and MW-9.
From June 2023 through August 2023, the previous UST system was removed from the site and replaced with a completely new system that included a new compartmentalized UST, new product lines and new dispensers. Approximately 795 tons of contaminated soil were removed during the activities and monitoring well MW-1 was replaced with MW-1R. Receptor Information

Singleton Environmental completed a receptor survey in the area within a 1,500-foot radius of the site in November 2017 as part of the LSA. The following bullets summarize the receptor information for the site:
• A water supply well survey was performed near the site by identifying water meter connections and searching for well houses. Nine water supply wells were identified within 1,000 feet of the source area.
• Georges Branch is located in a buried culvert approximately 130 feet to the west of MW-1R underneath the TA Travel Center parking lot across Wiggins Road.
• Public water supply is not available in the vicinity of the site.

• The site is not located within a wellhead protection area. The property containing the release is currently an active convenience store. Therefore, land use
at the Site is commercial. The surrounding properties are a commercial and residential mix. Site Geology and Hydrogeology

According to the Geologic Map of North Carolina (1985), the local geology consists of Muscovite - Biotite Gneiss which is a part of the Ashe Metamorphic Suite and Tallulah Falls Formation inside the Blue Ridge Belt.
On August 21, 2023, the average depth to groundwater was 23.54 ft-bgs. Groundwater flow was
calculated to be flowing directly to the southeast. MW-1R Installation Activities On August 15, 2023, monitoring well MW-1R was installed to replace MW-1 that was closed and removed during the soil excavation activities in July 2023 and August 2023. The monitoring well
was installed to 27.5 feet with 15 feet of screen. To date, free product has not returned to the area.

Post Excavation Groundwater Sampling Activities
SEI was on-site on August 21, 2023, to collect post-excavation groundwater samples from the
monitoring wells. Monitoring wells MW-1R through MW-9, and WSW-1 were sampled as part
of the sampling event. Prior to sampling, the monitoring wells were developed by purging three casing volumes of water prior to sampling and the water supply well was purged for approximately 20 minutes prior to sampling.
The groundwater samples were collected in laboratory-supplied bottles and placed into a cooler
packed with ice. The cooler was delivered under chain-of-custody to Pace Analytical in Asheville, North Carolina for testing. Pace analyzed the groundwater samples for VOCs by Standard Method 6200B. A summary of the groundwater sample analytical results is included in Table 3.
• Laboratory analysis of the groundwater samples collected from monitoring wells MW-5, MW-6, MW-7, and water supply well WSW-1 did not detect targeted petroleum hydrocarbons at concentrations that exceed their respective North Carolina 2L Groundwater Quality Standards (NCAC 2L MCLs).
• Laboratory analysis of the groundwater sample collected from monitoring well MW-1R detected 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, benzene, ethylbenzene, MTBE, naphthalene, styrene, toluene, n-propylbenzene, and total xylenes at concentrations exceeding the NCAC 2L MCLs. Concentrations of benzene and toluene exceeded the
NCAC 10x2B Concentrations Levels. None of the detected concentrations exceeded the
Gross Contamination Levels (GCLs).
• Laboratory analysis of the groundwater sample collected from monitoring well MW-2
detected benzene, 1,2-dichloroethane, MTBE, and naphthalene at concentrations
exceeding the NCAC 2L MCLs. None of the detected concentrations exceeded the NCAC 10x2B Concentration Levels or the GCLs.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-3
detected MTBE at concentrations exceeding the NCAC 2L MCLs. None of the detected concentrations exceeded the NCAC 10x2B Concentration Levels or the GCLs.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-4
detected 1,2,3-trichloropropane, 1,2,4-trimethylbenzene, EDB, benzene, 1,2-
dichloroethane, diisopropylether, MTBE, naphthalene, toluene, and total xylenes at concentrations exceeding the NCAC 2L MCLs. Concentrations of toluene exceeded the NCAC 10x2B Concentration Levels. None of the detected concentrations exceeded the GCLs.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-8 detected benzene and naphthalene at concentrations exceeding the NCAC 2L MCLS. None of the detected concentrations exceeded the NCAC 10x2B Concentration Levels or the GCLs.

• Laboratory analysis of the groundwater sample collected from monitoring well MW-9
detected naphthalene at concentrations exceeding the NCAC 2L MCLS. None of the detected concentrations exceeded the NCAC 10x2B Concentration Levels or the GCLs. The laboratory analytical reports for the groundwater samples are provided in Appendix B. The
laboratory test results are summarized on Table 2. A map depicting the plume is included on Figure
4.
CONCLUSIONS
Based on the results of the groundwater sampling event, SEI makes the following conclusions:
• Laboratory analysis of the groundwater samples collected from monitoring wells WSW-1,
MW-5, MW-6, and MW-7 did not detect targeted compounds exceeding their respective
NCAC 2L MCLS.
• Laboratory analysis of the groundwater samples collected from monitoring wells MW-1R, MW-2, MW-3, MW-4, MW-8, and MW-9 detected targeted compounds exceeding their
respective NCAC 2L MCLs.
• Laboratory analysis of the groundwater samples collected from monitoring wells MW-1R and MW-4 detected targeted compounds exceeding the NCAC 10x2B Concentration Levels.
• Free product was not observed in monitoring well MW-1R.
Based on the remaining concentrations in select groundwater samples exceeding their respective NCAC 2L MCLS, GCLs, and 10x2B SEI recommends the following:
SEI recommends sampling all monitoring wells and the water supply well in November 2023.

TABLES

MW Number Date
Top of Casing Elevation (Ft) and
(screened interval)Top of Casing to Free Product
Top of Casing
to GW Depth Groundwater Elevation (ft)
MW-1R 8/21/2023 98.36 (12' to 27')ND 22.85 75.51
12/4/2019 21.90 (0.1 Ft)22.00 76.69
11/5/2020 21.52 (1.5 Ft)23.02 75.679/9/2021 20.53 (0.25 Ft)20.78 77.9112/10/2021 22.27 (0.17 Ft)22.44 76.25
7/8/2022 21.28 (0.02Ft)21.30 77.39
12/4/2019 ND 23.18 75.26
11/5/2020 ND 22.54 75.90
9/9/2021 ND 22.40 76.04
1210/22 ND 23.35 75.09
7/8/2022 ND 22.97 75.47
8/21/2023 ND 24.06 74.3812/4/2019 ND 25.10 74.7411/5/2020 ND 22.74 77.10
9/9/2021 ND 23.77 76.07
12/10/2022 ND 25.00 74.84
7/8/2022 ND 23.96 75.88
8/21/2023 ND 25.80 74.04
12/4/2019 ND 21.07 78.93
11/5/2020 ND 19.31 80.699/9/2021 ND 20.61 79.3912/10/2022 ND 21.29 78.71
7/8/2022 ND 20.92 79.08
8/21/2023 ND 21.69 78.31
12/4/2019 ND 25.30 73.32
11/5/2020 ND 22.93 75.69
9/9/2021 ND 24.21 74.41
12/10/2022 ND 25.33 73.29
7/8/2022 ND 24.56 74.068/21/2023 ND 26.07 72.5512/4/2019 ND 25.28 74.82
11/5/2020 ND 23.48 76.62
9/9/2021 ND 25.00 75.10
12/10/2022 ND 26.05 74.05
7/8/2022 ND 24.81 75.29
8/21/2023 ND 26.79 73.31
12/4/2019 ND 20.05 79.9811/5/2020 ND 19.94 80.099/9/2021 ND 19.68 80.35
12/10/2022 ND 20.32 79.71
7/8/2022 ND 20.00 80.03
8/21/2023 ND 20.80 79.23
12/4/2019 ND 21.45 77.02
98.62 (20' to 30')
100.1 (10' to 30')
100.03 (10' to 30')
MW-2
MW-3
MW-4
MW-5
MW-1 98.69 (15' to 30')
Table 1
Groundwater Flow Mapping Elevation Details
One Stop #15 - Nov-2020
Candler, NC
UST Incident # 28861
146 Wiggins Road

MW-6
MW-7
98.44 (15' to 30')
99.84 (15' to 30')
100 (15' to 30')
11/5/2020 ND 18.75 79.729/9/2021 ND 20.26 78.21
12/10/2022 ND 20.82 77.65
7/8/2022 ND 20.56 77.91
8/21/2023 ND 21.22 77.25
12/4/2019 ND 21.26 75.90
11/5/2020 ND 19.25 77.91
9/9/2021 ND 21.26 75.90
12/10/2022 ND 22.14 75.027/8/2022 ND 21.93 75.238/21/2023 ND 22.54 74.62
MW-8
MW-9
98.47 (10' to 30')
97.16 (10' to 30')
1,2,3-
Trichlor
opropa
ne
1,2,4-
Trimeth
ylbenze
ne
1,2-
Dibrom
oethane
(EDB)
1,2-
Dichlor
oethane
1,3,5-
Trimeth
ylbenze
ne
Benzen
e
Diisopro
pyl
ether
Ethylbe
nzene
Isoprop
ylbenze
ne
(Cumen
e)
Methyl-
tert-
butyl
ether
Naphth
alene
Styren
e Toluene m&p-
Xylene
n-
Butylbe
nzene
n-
Propylb
enzene
o-
Xylene
Date
Collected
(mm/dd/yy)
Sample
Depth
(ft. BGS)
ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L
MW-1R 8/21/2023 ND 1550 ND ND 489 937 36.7 1290 35.2 79 437 149 6300 5230 ND 114 2910
12/04/2019 ND 17.5 ND 1.9 6.8 198 22.0 ND ND 85.8 8.5 ND 1.1 35.9 ND ND 31.3
11/5/2020 ND 5.3 ND ND 2.9 65.5 5.2 0.58 ND 13.5 2.4 ND ND 10.3 ND ND 10.3
9/9/2021 ND 15.3 ND 1.3 7 190 23.1 ND ND 51 9.6 ND 1.3 35.5 ND ND 36.5
12/10/2021 ND 2.8 0.57 1.6 7.9 15.8 31.2 ND 1 87.2 ND ND ND 7.6 ND ND 14.5
7/8/2022 ND 22.9 ND 1.7 11 279 33.8 2.5 ND 78.3 14.5 ND 1.7 51.1 ND ND 57.4
8/21/2023 ND 11.9 ND 1.9 8.7 142 36.8 0.65 0.91 71.6 6.1 ND 0.56 27.2 ND ND 33.6
12/04/2019 ND 238 ND ND 49.9 21.4 2.5 70.6 7.7 76.7 53.1 ND 250 310 ND 27.8 158
11/5/2020 ND 3 ND ND ND ND 0.97 1.1 ND 74 ND ND 2.7 4.6 ND ND 2.3
9/9/2021 ND 0.68 ND ND ND ND 0.62 ND ND 42.4 ND ND ND ND ND ND 0.57
12/10/2021 ND 1.5 ND ND ND ND 1.2 ND ND 59.5 ND ND ND ND ND ND ND
7/8/2022 ND ND ND ND ND ND 0.79 ND ND 53.8 ND ND ND ND ND ND ND
8/21/2023 ND ND ND ND ND ND 0.63 ND ND 44.5 ND ND ND ND ND ND ND
12/04/2019 ND 378 12.2 36.4 ND 296 90.2 138 9.7 507 99.4 ND 551 1220 ND ND 625
11/5/2020 ND 644 17.4 47.1 ND 426 124 267 18.2 720 181 ND 1380 2160 ND ND 1100
9/9/2021 ND 449 9 43.3 ND 332 112 225 15.8 602 156 ND 1090 1580 ND ND 826
12/10/2021 ND 449 7.9 19.3 ND 201 52 180 14.8 299 165 ND 653 1350 ND ND 663
7/8/2022 ND 495 10.9 29.2 131 256 93 208 15.4 534 137 ND 850 1760 ND 29 837
8/21/2023 15.9 620 8.1 39.1 169 268 127 244 19.1 704 196 ND 784 2050 ND 38.1 904
12/04/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
11/5/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/9/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/10/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
7/8/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
8/21/2023 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/04/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
11/5/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/9/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/10/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
7/8/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
8/21/2023 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/04/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Analytical Method
Sample ID
Constituent of Concern
MW-3
MW-4
MW-5
MW-6
MW-2
Table # 2
Summary of Analytical Results - Water Samples
ONE STOP #15
11/5/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/9/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/10/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
7/8/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
8/21/2023 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/04/2019 ND ND ND ND 72.9 34.2 3.8 35.7 16.9 10.2 87.7 ND 13.2 59.2 ND 47.7 202
11/5/2020 ND 90.6 ND ND 72.5 25.4 3.6 21.6 19.1 9.1 65.8 ND 5.1 54.8 ND 40.2 181
9/9/2021 ND 92.9 ND ND ND 24.3 4.4 29.6 19.4 9.4 97.6 ND 12.3 86 ND ND 201
12/10/2021 ND 54.4 ND ND 75.3 23.9 4.2 33.6 23.3 10.1 109 ND 10 33.4 26.8 56.6 250
7/8/2022 ND ND ND ND 65.7 18.6 3.4 25.3 23 7.7 91.7 ND 9.4 19.4 ND 46 194
8/21/2023 ND ND ND ND 62.5 22.7 4.2 60.2 27.4 8.3 97.1 ND 19.2 18.5 ND 69.5 186
12/04/2019 ND 67.6 ND ND 21.7 ND ND 11.5 2.5 ND 9.2 ND 2.9 79.3 2.8 4.6 24.4
11/5/2020 ND 3.3 ND ND 2.3 ND ND ND ND ND ND ND ND ND 2 ND 0.57
9/9/2021 ND 42.3 ND ND 15.8 ND ND 0.54 1.6 ND 2.3 ND ND 21.7 2.5 ND 5.4
12/10/2021 ND 179 ND ND 60.2 ND ND 11.4 5.8 ND 16.3 ND 1.7 151 12.1 6.6 46.7
7/8/2022 ND 192 ND ND 68.6 ND ND 6 7.5 ND 22.8 ND 1.6 155 ND 5.3 53.9
8/21/2023 ND 300 ND ND 102 ND ND 28.3 11 ND 27.2 1.3 4.6 351 ND 13.3 113
12/04/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
11/5/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/9/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/10/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
7/8/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
8/21/2023 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
0.005 400 0.02 0.4 400 1 70 600 70 20 6 70 600 500 70 70 500
N/A N/A N/A N/A N/A 510 N/A N/A N/A N/A N/A N/A 110 N/A N/A N/A N/A
N/A 28500 50 400 25000 5000 70000 84500 25000 20000 6000 70000 260000 85500 6900 30000 85500
10 X NCAC 2B Standards
ft. BGS = feet below ground surface
mg/L = milligrams per liter
ug/L = micrograms per liter
Bold data above the MSCC (Soil to Groundwater)
2L Class GCL Standards
NOTES:
ND = Not Detected
2L Class GA Standards
MW-7
MW-8
MW-9
WSW-1

FIGURES

CANTON QUADRANGLE
NORTH CAROLINA
7.5 MINUTE SERIES (TOPOGRAPHIC)
Figure 1 Site Map
One Stop #15 – Candler, NC
One Stop #15
Singleton Environmental, Inc MW-1RMW-3MW-2Previous USTsMW-4One Stop #15WSW-1MW-5MW-6MW-7MW-8MW-9
Singleton Environmental, Inc MW-1RMW-3MW-2Previous USTsMW-4One Stop #15WSW-1MW-5MW-6MW-7MW-8MW-979.23'75.51'74.38'74.04'78.31'72.55'73.31'77.25'74.62'G W F l o w
Singleton Environmental, Inc MW-1RMW-3MW-2Previous USTsMW-4One Stop #15WSW-1MW-5MW-6MW-7MW-8MW-9GW Exceeding 2LGW Exceeding 10x2B

APPENDIX A
Field Notes and Monitoring Well MW-1R Records

PROJECT NUMBER BORING NUMBERMW-1R SHEET 1 OF 1
SOIL BORING LOG
PROJECT :One Stop #15 LOCATION :Candler, NC
ELEVATION :N/A DRILLING CONTRACTOR 3D Investigations
DRILLING METHOD AND EQUIPMENT USED :Hollow Stem Auger
WATER LEVEL :22.85 DATE:8/15/2023 LOGGER : Chris Singleton
DEPTH BELOW SURFACE (FT)STANDARD DESCRIPTION COMMENTS
INTERVAL (FT)PENETRATION
RECOVERY (IN)TEST SOIL NAME, USCS GROUP SYMBOL, COLOR, DEPTH OF CASING, DRILLING RATE,
#/TYPE RESULTS MOISTURE CONTENT, RELATIVE DENSITY, DRILLING FLUID LOSS,
6"-6"-6"-6" OR CONSISTENCY, SOIL STRUCTURE, TESTS, AND INSTRUMENTATION.
(N) MINERALOGY.
_0.0 to 22.0 feet: Gravel Fill Material _Concrete 0-4 Casing 0-12.5 _
___
___
___
5 ______
__Bent. 4-10 _
___
___
___
10 ____Sand 10-27.5 __
___
___
___
___
15 ______
__screen 12.5-27 _
___
___
___
20 ______
___
__GW _
_22 to 27.5 feet: Brown Clayey Silt __
___
25 ____
__
___
___
_Well set at 27.5 feet.__
30 ______
___
___
___
___
35 ______
___
___
___
___
40 ______
__
__
__
_
SEI-1362
MW-1R Boring Log

APPENDIX B

Laboratory Analytical Reports

#=CL#
August 31, 2023
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92683799
92683799
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
105 Charlotte Highway
Asheville, NC 28803
ONE STOP 15
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on August 22, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 53
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92683799
ONE STOP 15
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 53
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92683799
ONE STOP 15
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92683799001 WSW-1 SM 6200B 63 PASI-CSAS
92683799002 MW-1R SM 6200B 63 PASI-CJJK
92683799003 MW-2 SM 6200B 63 PASI-CJJK
92683799004 MW-3 SM 6200B 63 PASI-CSAS
92683799005 MW-4 SM 6200B 63 PASI-CJJK
92683799006 MW-5 SM 6200B 63 PASI-CSAS
92683799007 MW-6 SM 6200B 63 PASI-CSAS
92683799008 MW-7 SM 6200B 63 PASI-CSAS
92683799009 MW-8 SM 6200B 63 PASI-CSAS
92683799010 MW-9 SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:WSW-1 Lab ID:92683799001 Collected:08/21/23 11:15 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 08/24/23 03:10 71-43-20.50 1
Bromobenzene ND ug/L 08/24/23 03:10 108-86-10.50 1
Bromochloromethane ND ug/L 08/24/23 03:10 74-97-50.50 1
Bromodichloromethane ND ug/L 08/24/23 03:10 75-27-40.50 1
Bromoform ND ug/L 08/24/23 03:10 75-25-20.50 1
Bromomethane ND ug/L 08/24/23 03:10 74-83-95.0 1
n-Butylbenzene ND ug/L 08/24/23 03:10 104-51-80.50 1
sec-Butylbenzene ND ug/L 08/24/23 03:10 135-98-80.50 1
tert-Butylbenzene ND ug/L 08/24/23 03:10 98-06-60.50 1
Carbon tetrachloride ND ug/L 08/24/23 03:10 56-23-50.50 1
Chlorobenzene ND ug/L 08/24/23 03:10 108-90-70.50 1
Chloroethane ND ug/L 08/24/23 03:10 75-00-31.0 1
Chloroform ND ug/L 08/24/23 03:10 67-66-30.50 1
Chloromethane ND ug/L 08/24/23 03:10 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/23 03:10 95-49-80.50 1
4-Chlorotoluene ND ug/L 08/24/23 03:10 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/23 03:10 96-12-81.0 1
Dibromochloromethane ND ug/L 08/24/23 03:10 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/23 03:10 106-93-40.50 1
Dibromomethane ND ug/L 08/24/23 03:10 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 08/24/23 03:10 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 08/24/23 03:10 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 08/24/23 03:10 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 08/24/23 03:10 75-71-80.50 1
1,1-Dichloroethane ND ug/L 08/24/23 03:10 75-34-30.50 1
1,2-Dichloroethane ND ug/L 08/24/23 03:10 107-06-20.50 1
1,1-Dichloroethene ND ug/L 08/24/23 03:10 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 08/24/23 03:10 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 08/24/23 03:10 156-60-50.50 1
1,2-Dichloropropane ND ug/L 08/24/23 03:10 78-87-50.50 1
1,3-Dichloropropane ND ug/L 08/24/23 03:10 142-28-90.50 1
2,2-Dichloropropane ND ug/L 08/24/23 03:10 594-20-70.50 1
1,1-Dichloropropene ND ug/L 08/24/23 03:10 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 08/24/23 03:10 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 08/24/23 03:10 10061-02-60.50 1
Diisopropyl ether ND ug/L 08/24/23 03:10 108-20-30.50 1
Ethylbenzene ND ug/L 08/24/23 03:10 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 08/24/23 03:10 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/23 03:10 98-82-80.50 1
Methylene Chloride ND ug/L 08/24/23 03:10 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 08/24/23 03:10 1634-04-40.50 1
Naphthalene ND ug/L 08/24/23 03:10 91-20-32.0 1
n-Propylbenzene ND ug/L 08/24/23 03:10 103-65-10.50 1
Styrene ND ug/L 08/24/23 03:10 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/23 03:10 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/23 03:10 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:WSW-1 Lab ID:92683799001 Collected:08/21/23 11:15 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 08/24/23 03:10 127-18-40.50 1
Toluene ND ug/L 08/24/23 03:10 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 08/24/23 03:10 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/23 03:10 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 08/24/23 03:10 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 08/24/23 03:10 79-00-50.50 1
Trichloroethene ND ug/L 08/24/23 03:10 79-01-60.50 1
Trichlorofluoromethane ND ug/L 08/24/23 03:10 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/23 03:10 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 08/24/23 03:10 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 08/24/23 03:10 108-67-80.50 1
Vinyl chloride ND ug/L 08/24/23 03:10 75-01-41.0 1
m&p-Xylene ND ug/L 08/24/23 03:10 179601-23-11.0 1
o-Xylene ND ug/L 08/24/23 03:10 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)111 %08/24/23 03:10 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %08/24/23 03:10 460-00-470-130 1
Toluene-d8 (S)97 %08/24/23 03:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-1R Lab ID:92683799002 Collected:08/21/23 11:00 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 937 ug/L 08/24/23 07:46 71-43-225.0 50
Bromobenzene ND ug/L 08/24/23 07:46 108-86-125.0 50
Bromochloromethane ND ug/L 08/24/23 07:46 74-97-525.0 50
Bromodichloromethane ND ug/L 08/24/23 07:46 75-27-425.0 50
Bromoform ND ug/L 08/24/23 07:46 75-25-225.0 50
Bromomethane ND ug/L 08/24/23 07:46 74-83-925050
n-Butylbenzene ND ug/L 08/24/23 07:46 104-51-825.0 50
sec-Butylbenzene ND ug/L 08/24/23 07:46 135-98-825.0 50
tert-Butylbenzene ND ug/L 08/24/23 07:46 98-06-625.0 50
Carbon tetrachloride ND ug/L 08/24/23 07:46 56-23-525.0 50
Chlorobenzene ND ug/L 08/24/23 07:46 108-90-725.0 50
Chloroethane ND ug/L 08/24/23 07:46 75-00-350.0 50
Chloroform ND ug/L 08/24/23 07:46 67-66-325.0 50
Chloromethane ND ug/L 08/24/23 07:46 74-87-350.0 50
2-Chlorotoluene ND ug/L 08/24/23 07:46 95-49-825.0 50
4-Chlorotoluene ND ug/L 08/24/23 07:46 106-43-425.0 50
1,2-Dibromo-3-chloropropane ND ug/L 08/24/23 07:46 96-12-850.0 50
Dibromochloromethane ND ug/L 08/24/23 07:46 124-48-125.0 50
1,2-Dibromoethane (EDB)ND ug/L 08/24/23 07:46 106-93-425.0 50
Dibromomethane ND ug/L 08/24/23 07:46 74-95-325.0 50
1,2-Dichlorobenzene ND ug/L 08/24/23 07:46 95-50-125.0 50
1,3-Dichlorobenzene ND ug/L 08/24/23 07:46 541-73-125.0 50
1,4-Dichlorobenzene ND ug/L 08/24/23 07:46 106-46-725.0 50
Dichlorodifluoromethane ND ug/L 08/24/23 07:46 75-71-825.0 50
1,1-Dichloroethane ND ug/L 08/24/23 07:46 75-34-325.0 50
1,2-Dichloroethane ND ug/L 08/24/23 07:46 107-06-225.0 50
1,1-Dichloroethene ND ug/L 08/24/23 07:46 75-35-425.0 50
cis-1,2-Dichloroethene ND ug/L 08/24/23 07:46 156-59-225.0 50
trans-1,2-Dichloroethene ND ug/L 08/24/23 07:46 156-60-525.0 50
1,2-Dichloropropane ND ug/L 08/24/23 07:46 78-87-525.0 50
1,3-Dichloropropane ND ug/L 08/24/23 07:46 142-28-925.0 50
2,2-Dichloropropane ND ug/L 08/24/23 07:46 594-20-725.0 50
1,1-Dichloropropene ND ug/L 08/24/23 07:46 563-58-625.0 50
cis-1,3-Dichloropropene ND ug/L 08/24/23 07:46 10061-01-525.0 50
trans-1,3-Dichloropropene ND ug/L 08/24/23 07:46 10061-02-625.0 50
Diisopropyl ether 36.7 ug/L 08/24/23 07:46 108-20-325.0 50
Ethylbenzene 1290 ug/L 08/24/23 07:46 100-41-425.0 50
Hexachloro-1,3-butadiene ND ug/L 08/24/23 07:46 87-68-310050
Isopropylbenzene (Cumene)35.2 ug/L 08/24/23 07:46 98-82-825.0 50
Methylene Chloride ND ug/L 08/24/23 07:46 75-09-210050
Methyl-tert-butyl ether 79.0 ug/L 08/24/23 07:46 1634-04-425.0 50
Naphthalene 437 ug/L 08/24/23 07:46 91-20-310050
n-Propylbenzene 114 ug/L 08/24/23 07:46 103-65-125.0 50
Styrene 149 ug/L 08/24/23 07:46 100-42-525.0 50
1,1,1,2-Tetrachloroethane ND ug/L 08/24/23 07:46 630-20-625.0 50
1,1,2,2-Tetrachloroethane ND ug/L 08/24/23 07:46 79-34-525.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-1R Lab ID:92683799002 Collected:08/21/23 11:00 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 08/24/23 07:46 127-18-425.0 50
Toluene 6300 ug/L 08/24/23 07:46 108-88-325.0 50
1,2,3-Trichlorobenzene ND ug/L 08/24/23 07:46 87-61-610050
1,2,4-Trichlorobenzene ND ug/L 08/24/23 07:46 120-82-110050
1,1,1-Trichloroethane ND ug/L 08/24/23 07:46 71-55-625.0 50
1,1,2-Trichloroethane ND ug/L 08/24/23 07:46 79-00-525.0 50
Trichloroethene ND ug/L 08/24/23 07:46 79-01-625.0 50
Trichlorofluoromethane ND ug/L 08/24/23 07:46 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 08/24/23 07:46 96-18-425.0 50
1,2,4-Trimethylbenzene 1550 ug/L 08/24/23 07:46 95-63-625.0 50
1,3,5-Trimethylbenzene 489 ug/L 08/24/23 07:46 108-67-825.0 50
Vinyl chloride ND ug/L 08/24/23 07:46 75-01-450.0 50
m&p-Xylene 5230 ug/L 08/24/23 07:46 179601-23-150.0 50
o-Xylene 2910 ug/L 08/24/23 07:46 95-47-625.0 50
Surrogates
1,2-Dichloroethane-d4 (S)105 %08/24/23 07:46 17060-07-070-130 50
4-Bromofluorobenzene (S)97 %08/24/23 07:46 460-00-470-130 50
Toluene-d8 (S)100 %08/24/23 07:46 2037-26-570-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-2 Lab ID:92683799003 Collected:08/21/23 08:40 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 142 ug/L 08/24/23 20:38 71-43-20.50 1
Bromobenzene ND ug/L 08/24/23 20:38 108-86-10.50 1
Bromochloromethane ND ug/L 08/24/23 20:38 74-97-50.50 1
Bromodichloromethane ND ug/L 08/24/23 20:38 75-27-40.50 1
Bromoform ND ug/L 08/24/23 20:38 75-25-20.50 1
Bromomethane ND ug/L 08/24/23 20:38 74-83-95.0 1
n-Butylbenzene ND ug/L 08/24/23 20:38 104-51-80.50 1
sec-Butylbenzene ND ug/L 08/24/23 20:38 135-98-80.50 1
tert-Butylbenzene ND ug/L 08/24/23 20:38 98-06-60.50 1
Carbon tetrachloride ND ug/L 08/24/23 20:38 56-23-50.50 1
Chlorobenzene ND ug/L 08/24/23 20:38 108-90-70.50 1
Chloroethane ND ug/L 08/24/23 20:38 75-00-31.0 1
Chloroform ND ug/L 08/24/23 20:38 67-66-30.50 1
Chloromethane ND ug/L 08/24/23 20:38 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/23 20:38 95-49-80.50 1
4-Chlorotoluene ND ug/L 08/24/23 20:38 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/23 20:38 96-12-81.0 1
Dibromochloromethane ND ug/L 08/24/23 20:38 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/23 20:38 106-93-40.50 1
Dibromomethane ND ug/L 08/24/23 20:38 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 08/24/23 20:38 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 08/24/23 20:38 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 08/24/23 20:38 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 08/24/23 20:38 75-71-8 L10.50 1
1,1-Dichloroethane ND ug/L 08/24/23 20:38 75-34-30.50 1
1,2-Dichloroethane 1.9 ug/L 08/24/23 20:38 107-06-20.50 1
1,1-Dichloroethene ND ug/L 08/24/23 20:38 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 08/24/23 20:38 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 08/24/23 20:38 156-60-50.50 1
1,2-Dichloropropane ND ug/L 08/24/23 20:38 78-87-50.50 1
1,3-Dichloropropane ND ug/L 08/24/23 20:38 142-28-90.50 1
2,2-Dichloropropane ND ug/L 08/24/23 20:38 594-20-70.50 1
1,1-Dichloropropene ND ug/L 08/24/23 20:38 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 08/24/23 20:38 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 08/24/23 20:38 10061-02-60.50 1
Diisopropyl ether 36.8 ug/L 08/24/23 20:38 108-20-30.50 1
Ethylbenzene 0.65 ug/L 08/24/23 20:38 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 08/24/23 20:38 87-68-32.0 1
Isopropylbenzene (Cumene)0.91 ug/L 08/24/23 20:38 98-82-80.50 1
Methylene Chloride ND ug/L 08/24/23 20:38 75-09-22.0 1
Methyl-tert-butyl ether 71.6 ug/L 08/24/23 20:38 1634-04-40.50 1
Naphthalene 6.1 ug/L 08/24/23 20:38 91-20-32.0 1
n-Propylbenzene ND ug/L 08/24/23 20:38 103-65-10.50 1
Styrene ND ug/L 08/24/23 20:38 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/23 20:38 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/23 20:38 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-2 Lab ID:92683799003 Collected:08/21/23 08:40 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 08/24/23 20:38 127-18-40.50 1
Toluene 0.56 ug/L 08/24/23 20:38 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 08/24/23 20:38 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/23 20:38 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 08/24/23 20:38 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 08/24/23 20:38 79-00-50.50 1
Trichloroethene ND ug/L 08/24/23 20:38 79-01-60.50 1
Trichlorofluoromethane ND ug/L 08/24/23 20:38 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/23 20:38 96-18-40.50 1
1,2,4-Trimethylbenzene 11.9 ug/L 08/24/23 20:38 95-63-60.50 1
1,3,5-Trimethylbenzene 8.7 ug/L 08/24/23 20:38 108-67-80.50 1
Vinyl chloride ND ug/L 08/24/23 20:38 75-01-41.0 1
m&p-Xylene 27.2 ug/L 08/24/23 20:38 179601-23-11.0 1
o-Xylene 33.6 ug/L 08/24/23 20:38 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %08/24/23 20:38 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %08/24/23 20:38 460-00-470-130 1
Toluene-d8 (S)101 %08/24/23 20:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-3 Lab ID:92683799004 Collected:08/21/23 09:00 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 08/24/23 03:29 71-43-20.50 1
Bromobenzene ND ug/L 08/24/23 03:29 108-86-10.50 1
Bromochloromethane ND ug/L 08/24/23 03:29 74-97-50.50 1
Bromodichloromethane ND ug/L 08/24/23 03:29 75-27-40.50 1
Bromoform ND ug/L 08/24/23 03:29 75-25-20.50 1
Bromomethane ND ug/L 08/24/23 03:29 74-83-95.0 1
n-Butylbenzene ND ug/L 08/24/23 03:29 104-51-80.50 1
sec-Butylbenzene ND ug/L 08/24/23 03:29 135-98-80.50 1
tert-Butylbenzene ND ug/L 08/24/23 03:29 98-06-60.50 1
Carbon tetrachloride ND ug/L 08/24/23 03:29 56-23-50.50 1
Chlorobenzene ND ug/L 08/24/23 03:29 108-90-70.50 1
Chloroethane ND ug/L 08/24/23 03:29 75-00-31.0 1
Chloroform ND ug/L 08/24/23 03:29 67-66-30.50 1
Chloromethane ND ug/L 08/24/23 03:29 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/23 03:29 95-49-80.50 1
4-Chlorotoluene ND ug/L 08/24/23 03:29 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/23 03:29 96-12-81.0 1
Dibromochloromethane ND ug/L 08/24/23 03:29 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/23 03:29 106-93-40.50 1
Dibromomethane ND ug/L 08/24/23 03:29 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 08/24/23 03:29 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 08/24/23 03:29 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 08/24/23 03:29 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 08/24/23 03:29 75-71-80.50 1
1,1-Dichloroethane ND ug/L 08/24/23 03:29 75-34-30.50 1
1,2-Dichloroethane ND ug/L 08/24/23 03:29 107-06-20.50 1
1,1-Dichloroethene ND ug/L 08/24/23 03:29 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 08/24/23 03:29 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 08/24/23 03:29 156-60-50.50 1
1,2-Dichloropropane ND ug/L 08/24/23 03:29 78-87-50.50 1
1,3-Dichloropropane ND ug/L 08/24/23 03:29 142-28-90.50 1
2,2-Dichloropropane ND ug/L 08/24/23 03:29 594-20-70.50 1
1,1-Dichloropropene ND ug/L 08/24/23 03:29 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 08/24/23 03:29 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 08/24/23 03:29 10061-02-60.50 1
Diisopropyl ether 0.63 ug/L 08/24/23 03:29 108-20-30.50 1
Ethylbenzene ND ug/L 08/24/23 03:29 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 08/24/23 03:29 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/23 03:29 98-82-80.50 1
Methylene Chloride ND ug/L 08/24/23 03:29 75-09-22.0 1
Methyl-tert-butyl ether 44.5 ug/L 08/24/23 03:29 1634-04-40.50 1
Naphthalene ND ug/L 08/24/23 03:29 91-20-32.0 1
n-Propylbenzene ND ug/L 08/24/23 03:29 103-65-10.50 1
Styrene ND ug/L 08/24/23 03:29 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/23 03:29 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/23 03:29 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-3 Lab ID:92683799004 Collected:08/21/23 09:00 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 08/24/23 03:29 127-18-40.50 1
Toluene ND ug/L 08/24/23 03:29 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 08/24/23 03:29 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/23 03:29 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 08/24/23 03:29 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 08/24/23 03:29 79-00-50.50 1
Trichloroethene ND ug/L 08/24/23 03:29 79-01-60.50 1
Trichlorofluoromethane ND ug/L 08/24/23 03:29 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/23 03:29 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 08/24/23 03:29 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 08/24/23 03:29 108-67-80.50 1
Vinyl chloride ND ug/L 08/24/23 03:29 75-01-41.0 1
m&p-Xylene ND ug/L 08/24/23 03:29 179601-23-11.0 1
o-Xylene ND ug/L 08/24/23 03:29 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)110 %08/24/23 03:29 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %08/24/23 03:29 460-00-470-130 1
Toluene-d8 (S)97 %08/24/23 03:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-4 Lab ID:92683799005 Collected:08/21/23 10:45 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 268 ug/L 08/25/23 00:34 71-43-25.0 10
Bromobenzene ND ug/L 08/25/23 00:34 108-86-15.0 10
Bromochloromethane ND ug/L 08/25/23 00:34 74-97-55.0 10
Bromodichloromethane ND ug/L 08/25/23 00:34 75-27-45.0 10
Bromoform ND ug/L 08/25/23 00:34 75-25-25.0 10
Bromomethane ND ug/L 08/25/23 00:34 74-83-950.0 10
n-Butylbenzene ND ug/L 08/25/23 00:34 104-51-85.0 10
sec-Butylbenzene ND ug/L 08/25/23 00:34 135-98-85.0 10
tert-Butylbenzene ND ug/L 08/25/23 00:34 98-06-65.0 10
Carbon tetrachloride ND ug/L 08/25/23 00:34 56-23-55.0 10
Chlorobenzene ND ug/L 08/25/23 00:34 108-90-75.0 10
Chloroethane ND ug/L 08/25/23 00:34 75-00-310.0 10
Chloroform ND ug/L 08/25/23 00:34 67-66-35.0 10
Chloromethane ND ug/L 08/25/23 00:34 74-87-310.0 10
2-Chlorotoluene ND ug/L 08/25/23 00:34 95-49-85.0 10
4-Chlorotoluene ND ug/L 08/25/23 00:34 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 08/25/23 00:34 96-12-810.0 10
Dibromochloromethane ND ug/L 08/25/23 00:34 124-48-15.0 10
1,2-Dibromoethane (EDB)8.1 ug/L 08/25/23 00:34 106-93-45.0 10
Dibromomethane ND ug/L 08/25/23 00:34 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 08/25/23 00:34 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 08/25/23 00:34 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 08/25/23 00:34 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 08/25/23 00:34 75-71-8 L15.0 10
1,1-Dichloroethane ND ug/L 08/25/23 00:34 75-34-35.0 10
1,2-Dichloroethane 39.1 ug/L 08/25/23 00:34 107-06-25.0 10
1,1-Dichloroethene ND ug/L 08/25/23 00:34 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 08/25/23 00:34 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 08/25/23 00:34 156-60-55.0 10
1,2-Dichloropropane ND ug/L 08/25/23 00:34 78-87-55.0 10
1,3-Dichloropropane ND ug/L 08/25/23 00:34 142-28-95.0 10
2,2-Dichloropropane ND ug/L 08/25/23 00:34 594-20-75.0 10
1,1-Dichloropropene ND ug/L 08/25/23 00:34 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 08/25/23 00:34 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 08/25/23 00:34 10061-02-65.0 10
Diisopropyl ether 127 ug/L 08/25/23 00:34 108-20-35.0 10
Ethylbenzene 244 ug/L 08/25/23 00:34 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 08/25/23 00:34 87-68-320.0 10
Isopropylbenzene (Cumene)19.1 ug/L 08/25/23 00:34 98-82-85.0 10
Methylene Chloride ND ug/L 08/25/23 00:34 75-09-220.0 10
Methyl-tert-butyl ether 704 ug/L 08/25/23 00:34 1634-04-45.0 10
Naphthalene 196 ug/L 08/25/23 00:34 91-20-320.0 10
n-Propylbenzene 38.1 ug/L 08/25/23 00:34 103-65-15.0 10
Styrene ND ug/L 08/25/23 00:34 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 08/25/23 00:34 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 08/25/23 00:34 79-34-55.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-4 Lab ID:92683799005 Collected:08/21/23 10:45 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 08/25/23 00:34 127-18-45.0 10
Toluene 784 ug/L 08/25/23 00:34 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 08/25/23 00:34 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 08/25/23 00:34 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 08/25/23 00:34 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 08/25/23 00:34 79-00-55.0 10
Trichloroethene ND ug/L 08/25/23 00:34 79-01-65.0 10
Trichlorofluoromethane ND ug/L 08/25/23 00:34 75-69-410.0 10
1,2,3-Trichloropropane 15.9 ug/L 08/25/23 00:34 96-18-45.0 10
1,2,4-Trimethylbenzene 620 ug/L 08/25/23 00:34 95-63-65.0 10
1,3,5-Trimethylbenzene 169 ug/L 08/25/23 00:34 108-67-85.0 10
Vinyl chloride ND ug/L 08/25/23 00:34 75-01-410.0 10
m&p-Xylene 2050 ug/L 08/25/23 00:34 179601-23-110.0 10
o-Xylene 904 ug/L 08/25/23 00:34 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)112 %08/25/23 00:34 17060-07-070-130 10
4-Bromofluorobenzene (S)104 %08/25/23 00:34 460-00-470-130 10
Toluene-d8 (S)101 %08/25/23 00:34 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-5 Lab ID:92683799006 Collected:08/21/23 08:15 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 08/24/23 01:02 71-43-20.50 1
Bromobenzene ND ug/L 08/24/23 01:02 108-86-10.50 1
Bromochloromethane ND ug/L 08/24/23 01:02 74-97-50.50 1
Bromodichloromethane ND ug/L 08/24/23 01:02 75-27-40.50 1
Bromoform ND ug/L 08/24/23 01:02 75-25-20.50 1
Bromomethane ND ug/L 08/24/23 01:02 74-83-95.0 1
n-Butylbenzene ND ug/L 08/24/23 01:02 104-51-80.50 1
sec-Butylbenzene ND ug/L 08/24/23 01:02 135-98-80.50 1
tert-Butylbenzene ND ug/L 08/24/23 01:02 98-06-60.50 1
Carbon tetrachloride ND ug/L 08/24/23 01:02 56-23-50.50 1
Chlorobenzene ND ug/L 08/24/23 01:02 108-90-70.50 1
Chloroethane ND ug/L 08/24/23 01:02 75-00-31.0 1
Chloroform ND ug/L 08/24/23 01:02 67-66-30.50 1
Chloromethane ND ug/L 08/24/23 01:02 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/23 01:02 95-49-80.50 1
4-Chlorotoluene ND ug/L 08/24/23 01:02 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/23 01:02 96-12-81.0 1
Dibromochloromethane ND ug/L 08/24/23 01:02 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/23 01:02 106-93-40.50 1
Dibromomethane ND ug/L 08/24/23 01:02 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 08/24/23 01:02 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 08/24/23 01:02 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 08/24/23 01:02 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 08/24/23 01:02 75-71-80.50 1
1,1-Dichloroethane ND ug/L 08/24/23 01:02 75-34-30.50 1
1,2-Dichloroethane ND ug/L 08/24/23 01:02 107-06-20.50 1
1,1-Dichloroethene ND ug/L 08/24/23 01:02 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 08/24/23 01:02 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 08/24/23 01:02 156-60-50.50 1
1,2-Dichloropropane ND ug/L 08/24/23 01:02 78-87-50.50 1
1,3-Dichloropropane ND ug/L 08/24/23 01:02 142-28-90.50 1
2,2-Dichloropropane ND ug/L 08/24/23 01:02 594-20-70.50 1
1,1-Dichloropropene ND ug/L 08/24/23 01:02 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 08/24/23 01:02 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 08/24/23 01:02 10061-02-60.50 1
Diisopropyl ether ND ug/L 08/24/23 01:02 108-20-30.50 1
Ethylbenzene ND ug/L 08/24/23 01:02 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 08/24/23 01:02 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/23 01:02 98-82-80.50 1
Methylene Chloride ND ug/L 08/24/23 01:02 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 08/24/23 01:02 1634-04-40.50 1
Naphthalene ND ug/L 08/24/23 01:02 91-20-32.0 1
n-Propylbenzene ND ug/L 08/24/23 01:02 103-65-10.50 1
Styrene ND ug/L 08/24/23 01:02 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/23 01:02 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/23 01:02 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-5 Lab ID:92683799006 Collected:08/21/23 08:15 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 08/24/23 01:02 127-18-40.50 1
Toluene ND ug/L 08/24/23 01:02 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 08/24/23 01:02 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/23 01:02 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 08/24/23 01:02 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 08/24/23 01:02 79-00-50.50 1
Trichloroethene ND ug/L 08/24/23 01:02 79-01-60.50 1
Trichlorofluoromethane ND ug/L 08/24/23 01:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/23 01:02 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 08/24/23 01:02 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 08/24/23 01:02 108-67-80.50 1
Vinyl chloride ND ug/L 08/24/23 01:02 75-01-41.0 1
m&p-Xylene ND ug/L 08/24/23 01:02 179601-23-11.0 1
o-Xylene ND ug/L 08/24/23 01:02 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)111 %08/24/23 01:02 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %08/24/23 01:02 460-00-470-130 1
Toluene-d8 (S)96 %08/24/23 01:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-6 Lab ID:92683799007 Collected:08/21/23 07:45 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 08/24/23 01:21 71-43-20.50 1
Bromobenzene ND ug/L 08/24/23 01:21 108-86-10.50 1
Bromochloromethane ND ug/L 08/24/23 01:21 74-97-50.50 1
Bromodichloromethane ND ug/L 08/24/23 01:21 75-27-40.50 1
Bromoform ND ug/L 08/24/23 01:21 75-25-20.50 1
Bromomethane ND ug/L 08/24/23 01:21 74-83-95.0 1
n-Butylbenzene ND ug/L 08/24/23 01:21 104-51-80.50 1
sec-Butylbenzene ND ug/L 08/24/23 01:21 135-98-80.50 1
tert-Butylbenzene ND ug/L 08/24/23 01:21 98-06-60.50 1
Carbon tetrachloride ND ug/L 08/24/23 01:21 56-23-50.50 1
Chlorobenzene ND ug/L 08/24/23 01:21 108-90-70.50 1
Chloroethane ND ug/L 08/24/23 01:21 75-00-31.0 1
Chloroform ND ug/L 08/24/23 01:21 67-66-30.50 1
Chloromethane ND ug/L 08/24/23 01:21 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/23 01:21 95-49-80.50 1
4-Chlorotoluene ND ug/L 08/24/23 01:21 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/23 01:21 96-12-81.0 1
Dibromochloromethane ND ug/L 08/24/23 01:21 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/23 01:21 106-93-40.50 1
Dibromomethane ND ug/L 08/24/23 01:21 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 08/24/23 01:21 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 08/24/23 01:21 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 08/24/23 01:21 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 08/24/23 01:21 75-71-80.50 1
1,1-Dichloroethane ND ug/L 08/24/23 01:21 75-34-30.50 1
1,2-Dichloroethane ND ug/L 08/24/23 01:21 107-06-20.50 1
1,1-Dichloroethene ND ug/L 08/24/23 01:21 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 08/24/23 01:21 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 08/24/23 01:21 156-60-50.50 1
1,2-Dichloropropane ND ug/L 08/24/23 01:21 78-87-50.50 1
1,3-Dichloropropane ND ug/L 08/24/23 01:21 142-28-90.50 1
2,2-Dichloropropane ND ug/L 08/24/23 01:21 594-20-70.50 1
1,1-Dichloropropene ND ug/L 08/24/23 01:21 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 08/24/23 01:21 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 08/24/23 01:21 10061-02-60.50 1
Diisopropyl ether ND ug/L 08/24/23 01:21 108-20-30.50 1
Ethylbenzene ND ug/L 08/24/23 01:21 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 08/24/23 01:21 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/23 01:21 98-82-80.50 1
Methylene Chloride ND ug/L 08/24/23 01:21 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 08/24/23 01:21 1634-04-40.50 1
Naphthalene ND ug/L 08/24/23 01:21 91-20-32.0 1
n-Propylbenzene ND ug/L 08/24/23 01:21 103-65-10.50 1
Styrene ND ug/L 08/24/23 01:21 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/23 01:21 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/23 01:21 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-6 Lab ID:92683799007 Collected:08/21/23 07:45 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 08/24/23 01:21 127-18-40.50 1
Toluene ND ug/L 08/24/23 01:21 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 08/24/23 01:21 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/23 01:21 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 08/24/23 01:21 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 08/24/23 01:21 79-00-50.50 1
Trichloroethene ND ug/L 08/24/23 01:21 79-01-60.50 1
Trichlorofluoromethane ND ug/L 08/24/23 01:21 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/23 01:21 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 08/24/23 01:21 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 08/24/23 01:21 108-67-80.50 1
Vinyl chloride ND ug/L 08/24/23 01:21 75-01-41.0 1
m&p-Xylene ND ug/L 08/24/23 01:21 179601-23-11.0 1
o-Xylene ND ug/L 08/24/23 01:21 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)111 %08/24/23 01:21 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %08/24/23 01:21 460-00-470-130 1
Toluene-d8 (S)97 %08/24/23 01:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-7 Lab ID:92683799008 Collected:08/21/23 10:00 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 08/24/23 01:39 71-43-20.50 1
Bromobenzene ND ug/L 08/24/23 01:39 108-86-10.50 1
Bromochloromethane ND ug/L 08/24/23 01:39 74-97-50.50 1
Bromodichloromethane ND ug/L 08/24/23 01:39 75-27-40.50 1
Bromoform ND ug/L 08/24/23 01:39 75-25-20.50 1
Bromomethane ND ug/L 08/24/23 01:39 74-83-95.0 1
n-Butylbenzene ND ug/L 08/24/23 01:39 104-51-80.50 1
sec-Butylbenzene ND ug/L 08/24/23 01:39 135-98-80.50 1
tert-Butylbenzene ND ug/L 08/24/23 01:39 98-06-60.50 1
Carbon tetrachloride ND ug/L 08/24/23 01:39 56-23-50.50 1
Chlorobenzene ND ug/L 08/24/23 01:39 108-90-70.50 1
Chloroethane ND ug/L 08/24/23 01:39 75-00-31.0 1
Chloroform ND ug/L 08/24/23 01:39 67-66-30.50 1
Chloromethane ND ug/L 08/24/23 01:39 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/23 01:39 95-49-80.50 1
4-Chlorotoluene ND ug/L 08/24/23 01:39 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/23 01:39 96-12-81.0 1
Dibromochloromethane ND ug/L 08/24/23 01:39 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/23 01:39 106-93-40.50 1
Dibromomethane ND ug/L 08/24/23 01:39 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 08/24/23 01:39 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 08/24/23 01:39 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 08/24/23 01:39 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 08/24/23 01:39 75-71-80.50 1
1,1-Dichloroethane ND ug/L 08/24/23 01:39 75-34-30.50 1
1,2-Dichloroethane ND ug/L 08/24/23 01:39 107-06-20.50 1
1,1-Dichloroethene ND ug/L 08/24/23 01:39 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 08/24/23 01:39 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 08/24/23 01:39 156-60-50.50 1
1,2-Dichloropropane ND ug/L 08/24/23 01:39 78-87-50.50 1
1,3-Dichloropropane ND ug/L 08/24/23 01:39 142-28-90.50 1
2,2-Dichloropropane ND ug/L 08/24/23 01:39 594-20-70.50 1
1,1-Dichloropropene ND ug/L 08/24/23 01:39 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 08/24/23 01:39 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 08/24/23 01:39 10061-02-60.50 1
Diisopropyl ether ND ug/L 08/24/23 01:39 108-20-30.50 1
Ethylbenzene ND ug/L 08/24/23 01:39 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 08/24/23 01:39 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/23 01:39 98-82-80.50 1
Methylene Chloride ND ug/L 08/24/23 01:39 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 08/24/23 01:39 1634-04-40.50 1
Naphthalene ND ug/L 08/24/23 01:39 91-20-32.0 1
n-Propylbenzene ND ug/L 08/24/23 01:39 103-65-10.50 1
Styrene ND ug/L 08/24/23 01:39 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/23 01:39 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/23 01:39 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
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[phone]
Page 18 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-7 Lab ID:92683799008 Collected:08/21/23 10:00 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 08/24/23 01:39 127-18-40.50 1
Toluene ND ug/L 08/24/23 01:39 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 08/24/23 01:39 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/23 01:39 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 08/24/23 01:39 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 08/24/23 01:39 79-00-50.50 1
Trichloroethene ND ug/L 08/24/23 01:39 79-01-60.50 1
Trichlorofluoromethane ND ug/L 08/24/23 01:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/23 01:39 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 08/24/23 01:39 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 08/24/23 01:39 108-67-80.50 1
Vinyl chloride ND ug/L 08/24/23 01:39 75-01-41.0 1
m&p-Xylene ND ug/L 08/24/23 01:39 179601-23-11.0 1
o-Xylene ND ug/L 08/24/23 01:39 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)111 %08/24/23 01:39 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %08/24/23 01:39 460-00-470-130 1
Toluene-d8 (S)97 %08/24/23 01:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-8 Lab ID:92683799009 Collected:08/21/23 10:30 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 22.7 ug/L 08/31/23 05:47 71-43-21.0 2
Bromobenzene ND ug/L 08/31/23 05:47 108-86-11.0 2
Bromochloromethane ND ug/L 08/31/23 05:47 74-97-51.0 2
Bromodichloromethane ND ug/L 08/31/23 05:47 75-27-41.0 2
Bromoform ND ug/L 08/31/23 05:47 75-25-21.0 2
Bromomethane ND ug/L 08/31/23 05:47 74-83-910.0 2
n-Butylbenzene ND ug/L 08/31/23 05:47 104-51-81.0 2
sec-Butylbenzene ND ug/L 08/31/23 05:47 135-98-81.0 2
tert-Butylbenzene ND ug/L 08/31/23 05:47 98-06-61.0 2
Carbon tetrachloride ND ug/L 08/31/23 05:47 56-23-51.0 2
Chlorobenzene ND ug/L 08/31/23 05:47 108-90-71.0 2
Chloroethane ND ug/L 08/31/23 05:47 75-00-32.0 2
Chloroform ND ug/L 08/31/23 05:47 67-66-31.0 2
Chloromethane ND ug/L 08/31/23 05:47 74-87-32.0 2
2-Chlorotoluene ND ug/L 08/31/23 05:47 95-49-81.0 2
4-Chlorotoluene ND ug/L 08/31/23 05:47 106-43-41.0 2
1,2-Dibromo-3-chloropropane ND ug/L 08/31/23 05:47 96-12-82.0 2
Dibromochloromethane ND ug/L 08/31/23 05:47 124-48-11.0 2
1,2-Dibromoethane (EDB)ND ug/L 08/31/23 05:47 106-93-41.0 2
Dibromomethane ND ug/L 08/31/23 05:47 74-95-31.0 2
1,2-Dichlorobenzene ND ug/L 08/31/23 05:47 95-50-11.0 2
1,3-Dichlorobenzene ND ug/L 08/31/23 05:47 541-73-11.0 2
1,4-Dichlorobenzene ND ug/L 08/31/23 05:47 106-46-71.0 2
Dichlorodifluoromethane ND ug/L 08/31/23 05:47 75-71-81.0 2
1,1-Dichloroethane ND ug/L 08/31/23 05:47 75-34-31.0 2
1,2-Dichloroethane ND ug/L 08/31/23 05:47 107-06-21.0 2
1,1-Dichloroethene ND ug/L 08/31/23 05:47 75-35-41.0 2
cis-1,2-Dichloroethene ND ug/L 08/31/23 05:47 156-59-21.0 2
trans-1,2-Dichloroethene ND ug/L 08/31/23 05:47 156-60-51.0 2
1,2-Dichloropropane ND ug/L 08/31/23 05:47 78-87-51.0 2
1,3-Dichloropropane ND ug/L 08/31/23 05:47 142-28-91.0 2
2,2-Dichloropropane ND ug/L 08/31/23 05:47 594-20-71.0 2
1,1-Dichloropropene ND ug/L 08/31/23 05:47 563-58-61.0 2
cis-1,3-Dichloropropene ND ug/L 08/31/23 05:47 10061-01-51.0 2
trans-1,3-Dichloropropene ND ug/L 08/31/23 05:47 10061-02-61.0 2
Diisopropyl ether 4.2 ug/L 08/31/23 05:47 108-20-31.0 2
Ethylbenzene 60.2 ug/L 08/31/23 05:47 100-41-41.0 2
Hexachloro-1,3-butadiene ND ug/L 08/31/23 05:47 87-68-34.0 2
Isopropylbenzene (Cumene)27.4 ug/L 08/31/23 05:47 98-82-81.0 2
Methylene Chloride ND ug/L 08/31/23 05:47 75-09-24.0 2
Methyl-tert-butyl ether 8.3 ug/L 08/31/23 05:47 1634-04-41.0 2
Naphthalene 97.1 ug/L 08/31/23 05:47 91-20-34.0 2
n-Propylbenzene 69.5 ug/L 08/31/23 05:47 103-65-11.0 2
Styrene ND ug/L 08/31/23 05:47 100-42-51.0 2
1,1,1,2-Tetrachloroethane ND ug/L 08/31/23 05:47 630-20-61.0 2
1,1,2,2-Tetrachloroethane ND ug/L 08/31/23 05:47 79-34-51.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-8 Lab ID:92683799009 Collected:08/21/23 10:30 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 08/31/23 05:47 127-18-41.0 2
Toluene 19.2 ug/L 08/31/23 05:47 108-88-31.0 2
1,2,3-Trichlorobenzene ND ug/L 08/31/23 05:47 87-61-64.0 2
1,2,4-Trichlorobenzene ND ug/L 08/31/23 05:47 120-82-14.0 2
1,1,1-Trichloroethane ND ug/L 08/31/23 05:47 71-55-61.0 2
1,1,2-Trichloroethane ND ug/L 08/31/23 05:47 79-00-51.0 2
Trichloroethene ND ug/L 08/31/23 05:47 79-01-61.0 2
Trichlorofluoromethane ND ug/L 08/31/23 05:47 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 08/31/23 05:47 96-18-41.0 2
1,2,4-Trimethylbenzene ND ug/L 08/31/23 05:47 95-63-61.0 2
1,3,5-Trimethylbenzene 62.5 ug/L 08/31/23 05:47 108-67-81.0 2
Vinyl chloride ND ug/L 08/31/23 05:47 75-01-42.0 2
m&p-Xylene 18.5 ug/L 08/31/23 05:47 179601-23-12.0 2
o-Xylene 186 ug/L 08/31/23 05:47 95-47-61.0 2
Surrogates
1,2-Dichloroethane-d4 (S)111 %08/31/23 05:47 17060-07-070-130 2
4-Bromofluorobenzene (S)97 %08/31/23 05:47 460-00-470-130 2
Toluene-d8 (S)97 %08/31/23 05:47 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-9 Lab ID:92683799010 Collected:08/21/23 09:30 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 08/25/23 06:49 71-43-21.2 2.5
Bromobenzene ND ug/L 08/25/23 06:49 108-86-11.2 2.5
Bromochloromethane ND ug/L 08/25/23 06:49 74-97-51.2 2.5
Bromodichloromethane ND ug/L 08/25/23 06:49 75-27-41.2 2.5
Bromoform ND ug/L 08/25/23 06:49 75-25-21.2 2.5
Bromomethane ND ug/L 08/25/23 06:49 74-83-912.5 2.5
n-Butylbenzene ND ug/L 08/25/23 06:49 104-51-81.2 2.5
sec-Butylbenzene ND ug/L 08/25/23 06:49 135-98-81.2 2.5
tert-Butylbenzene ND ug/L 08/25/23 06:49 98-06-61.2 2.5
Carbon tetrachloride ND ug/L 08/25/23 06:49 56-23-51.2 2.5
Chlorobenzene ND ug/L 08/25/23 06:49 108-90-71.2 2.5
Chloroethane ND ug/L 08/25/23 06:49 75-00-32.5 2.5
Chloroform ND ug/L 08/25/23 06:49 67-66-31.2 2.5
Chloromethane ND ug/L 08/25/23 06:49 74-87-32.5 2.5
2-Chlorotoluene ND ug/L 08/25/23 06:49 95-49-81.2 2.5
4-Chlorotoluene ND ug/L 08/25/23 06:49 106-43-41.2 2.5
1,2-Dibromo-3-chloropropane ND ug/L 08/25/23 06:49 96-12-82.5 2.5
Dibromochloromethane ND ug/L 08/25/23 06:49 124-48-11.2 2.5
1,2-Dibromoethane (EDB)ND ug/L 08/25/23 06:49 106-93-41.2 2.5
Dibromomethane ND ug/L 08/25/23 06:49 74-95-31.2 2.5
1,2-Dichlorobenzene ND ug/L 08/25/23 06:49 95-50-11.2 2.5
1,3-Dichlorobenzene ND ug/L 08/25/23 06:49 541-73-11.2 2.5
1,4-Dichlorobenzene ND ug/L 08/25/23 06:49 106-46-71.2 2.5
Dichlorodifluoromethane ND ug/L 08/25/23 06:49 75-71-81.2 2.5
1,1-Dichloroethane ND ug/L 08/25/23 06:49 75-34-31.2 2.5
1,2-Dichloroethane ND ug/L 08/25/23 06:49 107-06-21.2 2.5
1,1-Dichloroethene ND ug/L 08/25/23 06:49 75-35-41.2 2.5
cis-1,2-Dichloroethene ND ug/L 08/25/23 06:49 156-59-21.2 2.5
trans-1,2-Dichloroethene ND ug/L 08/25/23 06:49 156-60-51.2 2.5
1,2-Dichloropropane ND ug/L 08/25/23 06:49 78-87-51.2 2.5
1,3-Dichloropropane ND ug/L 08/25/23 06:49 142-28-91.2 2.5
2,2-Dichloropropane ND ug/L 08/25/23 06:49 594-20-71.2 2.5
1,1-Dichloropropene ND ug/L 08/25/23 06:49 563-58-61.2 2.5
cis-1,3-Dichloropropene ND ug/L 08/25/23 06:49 10061-01-51.2 2.5
trans-1,3-Dichloropropene ND ug/L 08/25/23 06:49 10061-02-61.2 2.5
Diisopropyl ether ND ug/L 08/25/23 06:49 108-20-31.2 2.5
Ethylbenzene 28.3 ug/L 08/25/23 06:49 100-41-41.2 2.5
Hexachloro-1,3-butadiene ND ug/L 08/25/23 06:49 87-68-35.0 2.5
Isopropylbenzene (Cumene)11.0 ug/L 08/25/23 06:49 98-82-81.2 2.5
Methylene Chloride ND ug/L 08/25/23 06:49 75-09-25.0 2.5
Methyl-tert-butyl ether ND ug/L 08/25/23 06:49 1634-04-41.2 2.5
Naphthalene 27.2 ug/L 08/25/23 06:49 91-20-35.0 2.5
n-Propylbenzene 13.3 ug/L 08/25/23 06:49 103-65-11.2 2.5
Styrene 1.3 ug/L 08/25/23 06:49 100-42-51.2 2.5
1,1,1,2-Tetrachloroethane ND ug/L 08/25/23 06:49 630-20-61.2 2.5
1,1,2,2-Tetrachloroethane ND ug/L 08/25/23 06:49 79-34-51.2 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683799
ONE STOP 15
Sample:MW-9 Lab ID:92683799010 Collected:08/21/23 09:30 Received:08/22/23 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 08/25/23 06:49 127-18-41.2 2.5
Toluene 4.6 ug/L 08/25/23 06:49 108-88-31.2 2.5
1,2,3-Trichlorobenzene ND ug/L 08/25/23 06:49 87-61-65.0 2.5
1,2,4-Trichlorobenzene ND ug/L 08/25/23 06:49 120-82-15.0 2.5
1,1,1-Trichloroethane ND ug/L 08/25/23 06:49 71-55-61.2 2.5
1,1,2-Trichloroethane ND ug/L 08/25/23 06:49 79-00-51.2 2.5
Trichloroethene ND ug/L 08/25/23 06:49 79-01-61.2 2.5
Trichlorofluoromethane ND ug/L 08/25/23 06:49 75-69-42.5 2.5
1,2,3-Trichloropropane ND ug/L 08/25/23 06:49 96-18-41.2 2.5
1,2,4-Trimethylbenzene 300 ug/L 08/25/23 06:49 95-63-61.2 2.5
1,3,5-Trimethylbenzene 102 ug/L 08/25/23 06:49 108-67-81.2 2.5
Vinyl chloride ND ug/L 08/25/23 06:49 75-01-42.5 2.5
m&p-Xylene 351 ug/L 08/25/23 06:49 179601-23-12.5 2.5
o-Xylene 113 ug/L 08/25/23 06:49 95-47-61.2 2.5
Surrogates
1,2-Dichloroethane-d4 (S)107 %08/25/23 06:49 17060-07-070-130 2.5
4-Bromofluorobenzene (S)96 %08/25/23 06:49 460-00-470-130 2.5
Toluene-d8 (S)97 %08/25/23 06:49 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
795441
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683799001, 92683799004, 92683799006, 92683799007, 92683799008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4121623
Associated Lab Samples:92683799001, 92683799004, 92683799006, 92683799007, 92683799008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/23/23 22:00
1,1,1-Trichloroethane ug/L ND 0.50 08/23/23 22:00
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/23/23 22:00
1,1,2-Trichloroethane ug/L ND 0.50 08/23/23 22:00
1,1-Dichloroethane ug/L ND 0.50 08/23/23 22:00
1,1-Dichloroethene ug/L ND 0.50 08/23/23 22:00
1,1-Dichloropropene ug/L ND 0.50 08/23/23 22:00
1,2,3-Trichlorobenzene ug/L ND 2.0 08/23/23 22:00
1,2,3-Trichloropropane ug/L ND 0.50 08/23/23 22:00
1,2,4-Trichlorobenzene ug/L ND 2.0 08/23/23 22:00
1,2,4-Trimethylbenzene ug/L ND 0.50 08/23/23 22:00
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/23/23 22:00
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/23/23 22:00
1,2-Dichlorobenzene ug/L ND 0.50 08/23/23 22:00
1,2-Dichloroethane ug/L ND 0.50 08/23/23 22:00
1,2-Dichloropropane ug/L ND 0.50 08/23/23 22:00
1,3,5-Trimethylbenzene ug/L ND 0.50 08/23/23 22:00
1,3-Dichlorobenzene ug/L ND 0.50 08/23/23 22:00
1,3-Dichloropropane ug/L ND 0.50 08/23/23 22:00
1,4-Dichlorobenzene ug/L ND 0.50 08/23/23 22:00
2,2-Dichloropropane ug/L ND 0.50 08/23/23 22:00
2-Chlorotoluene ug/L ND 0.50 08/23/23 22:00
4-Chlorotoluene ug/L ND 0.50 08/23/23 22:00
Benzene ug/L ND 0.50 08/23/23 22:00
Bromobenzene ug/L ND 0.50 08/23/23 22:00
Bromochloromethane ug/L ND 0.50 08/23/23 22:00
Bromodichloromethane ug/L ND 0.50 08/23/23 22:00
Bromoform ug/L ND 0.50 08/23/23 22:00
Bromomethane ug/L ND 5.0 08/23/23 22:00
Carbon tetrachloride ug/L ND 0.50 08/23/23 22:00
Chlorobenzene ug/L ND 0.50 08/23/23 22:00
Chloroethane ug/L ND 1.0 08/23/23 22:00
Chloroform ug/L ND 0.50 08/23/23 22:00
Chloromethane ug/L ND 1.0 08/23/23 22:00
cis-1,2-Dichloroethene ug/L ND 0.50 08/23/23 22:00
cis-1,3-Dichloropropene ug/L ND 0.50 08/23/23 22:00
Dibromochloromethane ug/L ND 0.50 08/23/23 22:00
Dibromomethane ug/L ND 0.50 08/23/23 22:00
Dichlorodifluoromethane ug/L ND 0.50 08/23/23 22:00
Diisopropyl ether ug/L ND 0.50 08/23/23 22:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4121623
Associated Lab Samples:92683799001, 92683799004, 92683799006, 92683799007, 92683799008
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 08/23/23 22:00
Hexachloro-1,3-butadiene ug/L ND 2.0 08/23/23 22:00
Isopropylbenzene (Cumene)ug/L ND 0.50 08/23/23 22:00
m&p-Xylene ug/L ND 1.0 08/23/23 22:00
Methyl-tert-butyl ether ug/L ND 0.50 08/23/23 22:00
Methylene Chloride ug/L ND 2.0 08/23/23 22:00
n-Butylbenzene ug/L ND 0.50 08/23/23 22:00
n-Propylbenzene ug/L ND 0.50 08/23/23 22:00
Naphthalene ug/L ND 2.0 08/23/23 22:00
o-Xylene ug/L ND 0.50 08/23/23 22:00
sec-Butylbenzene ug/L ND 0.50 08/23/23 22:00
Styrene ug/L ND 0.50 08/23/23 22:00
tert-Butylbenzene ug/L ND 0.50 08/23/23 22:00
Tetrachloroethene ug/L ND 0.50 08/23/23 22:00
Toluene ug/L ND 0.50 08/23/23 22:00
trans-1,2-Dichloroethene ug/L ND 0.50 08/23/23 22:00
trans-1,3-Dichloropropene ug/L ND 0.50 08/23/23 22:00
Trichloroethene ug/L ND 0.50 08/23/23 22:00
Trichlorofluoromethane ug/L ND 1.0 08/23/23 22:00
Vinyl chloride ug/L ND 1.0 08/23/23 22:00
1,2-Dichloroethane-d4 (S)%110 70-130 08/23/23 22:00
4-Bromofluorobenzene (S)%95 70-130 08/23/23 22:00
Toluene-d8 (S)%97 70-130 08/23/23 22:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4121624LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.420 102 60-140
1,1,1-Trichloroethane ug/L 19.620 98 60-140
1,1,2,2-Tetrachloroethane ug/L 22.820 114 60-140
1,1,2-Trichloroethane ug/L 21.220 106 60-140
1,1-Dichloroethane ug/L 21.120 105 60-140
1,1-Dichloroethene ug/L 21.920 110 60-140
1,1-Dichloropropene ug/L 22.120 110 60-140
1,2,3-Trichlorobenzene ug/L 18.620 93 60-140
1,2,3-Trichloropropane ug/L 21.920 109 60-140
1,2,4-Trichlorobenzene ug/L 19.020 95 60-140
1,2,4-Trimethylbenzene ug/L 20.720 103 60-140
1,2-Dibromo-3-chloropropane ug/L 17.820 89 60-140
1,2-Dibromoethane (EDB)ug/L 21.420 107 60-140
1,2-Dichlorobenzene ug/L 21.520 108 60-140
1,2-Dichloroethane ug/L 21.420 107 60-140
1,2-Dichloropropane ug/L 21.820 109 60-140
1,3,5-Trimethylbenzene ug/L 21.020 105 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4121624LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 21.020 105 60-140
1,3-Dichloropropane ug/L 21.620 108 60-140
1,4-Dichlorobenzene ug/L 21.220 106 60-140
2,2-Dichloropropane ug/L 17.320 86 60-140
2-Chlorotoluene ug/L 21.120 106 60-140
4-Chlorotoluene ug/L 21.020 105 60-140
Benzene ug/L 21.220 106 60-140
Bromobenzene ug/L 21.120 106 60-140
Bromochloromethane ug/L 20.220 101 60-140
Bromodichloromethane ug/L 19.020 95 60-140
Bromoform ug/L 18.120 91 60-140
Bromomethane ug/L 27.620 138 60-140
Carbon tetrachloride ug/L 19.220 96 60-140
Chlorobenzene ug/L 21.220 106 60-140
Chloroethane ug/L 27.920 139 60-140
Chloroform ug/L 20.720 104 60-140
Chloromethane ug/L 20.320 101 60-140
cis-1,2-Dichloroethene ug/L 20.720 103 60-140
cis-1,3-Dichloropropene ug/L 18.920 95 60-140
Dibromochloromethane ug/L 19.220 96 60-140
Dibromomethane ug/L 19.720 98 60-140
Dichlorodifluoromethane ug/L 23.320 116 60-140
Diisopropyl ether ug/L 21.320 107 60-140
Ethylbenzene ug/L 21.020 105 60-140
Hexachloro-1,3-butadiene ug/L 19.520 98 60-140
Isopropylbenzene (Cumene)ug/L 20.920 105 60-140
m&p-Xylene ug/L 42.040 105 60-140
Methyl-tert-butyl ether ug/L 19.120 95 60-140
Methylene Chloride ug/L 21.120 105 60-140
n-Butylbenzene ug/L 21.020 105 60-140
n-Propylbenzene ug/L 21.020 105 60-140
Naphthalene ug/L 20.020 100 60-140
o-Xylene ug/L 20.720 103 60-140
sec-Butylbenzene ug/L 20.920 104 60-140
Styrene ug/L 21.220 106 60-140
tert-Butylbenzene ug/L 17.120 85 60-140
Tetrachloroethene ug/L 20.120 101 60-140
Toluene ug/L 19.520 97 60-140
trans-1,2-Dichloroethene ug/L 21.320 107 60-140
trans-1,3-Dichloropropene ug/L 18.520 92 60-140
Trichloroethene ug/L 20.620 103 60-140
Trichlorofluoromethane ug/L 23.620 118 60-140
Vinyl chloride ug/L 20.220 101 60-140
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4121625MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92683581013
4121626
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 121 60-140117 420ND24.2 23.3
1,1,1-Trichloroethane ug/L 20 121 60-140120 120ND24.1 24.0
1,1,2,2-Tetrachloroethane ug/L 20 127 60-140126 020ND25.4 25.3
1,1,2-Trichloroethane ug/L 20 111 60-140112 120ND22.2 22.4
1,1-Dichloroethane ug/L 20 136 60-140134 120ND27.1 26.9
1,1-Dichloroethene ug/L M12015060-140150 020ND29.9 30.0
1,1-Dichloropropene ug/L M12014960-140145 220ND29.7 29.1
1,2,3-Trichlorobenzene ug/L 20 114 60-140111 320ND22.8 22.1
1,2,3-Trichloropropane ug/L 20 120 60-140119 020ND24.0 23.9
1,2,4-Trichlorobenzene ug/L 20 122 60-140111 920ND24.3 22.2
1,2,4-Trimethylbenzene ug/L 20 129 60-140125 320ND25.9 25.0
1,2-Dibromo-3-chloropropane ug/L 20 102 60-140101 120ND20.4 20.2
1,2-Dibromoethane (EDB)ug/L 20 121 60-140120 020ND24.1 24.1
1,2-Dichlorobenzene ug/L 20 127 60-140124 220ND25.5 24.9
1,2-Dichloroethane ug/L 20 119 60-140118 020ND23.7 23.6
1,2-Dichloropropane ug/L 20 135 60-140133 220ND27.0 26.5
1,3,5-Trimethylbenzene ug/L 20 134 60-140130 320ND26.8 25.9
1,3-Dichlorobenzene ug/L 20 127 60-140125 220ND25.5 25.0
1,3-Dichloropropane ug/L 20 124 60-140123 120ND24.8 24.5
1,4-Dichlorobenzene ug/L 20 127 60-140125 120ND25.4 25.1
2,2-Dichloropropane ug/L 20 118 60-140117 120ND23.5 23.4
2-Chlorotoluene ug/L 20 128 60-140127 220ND25.7 25.3
4-Chlorotoluene ug/L 20 128 60-140127 120ND25.7 25.4
Benzene ug/L 20 135 60-140133 220ND27.0 26.6
Bromobenzene ug/L 20 125 60-140122 220ND25.0 24.4
Bromochloromethane ug/L 20 120 60-140119 120ND24.1 23.8
Bromodichloromethane ug/L 20 109 60-140108 120ND21.9 21.7
Bromoform ug/L 20 105 60-140101 420ND21.0 20.1
Bromomethane ug/L 20 139 60-140138 020ND27.7 27.7
Carbon tetrachloride ug/L 20 119 60-140116 220ND23.7 23.3
Chlorobenzene ug/L 20 128 60-140126 120ND25.5 25.2
Chloroethane ug/L M12015760-140151 420ND31.3 30.2
Chloroform ug/L 20 123 60-140121 2200.79 25.5 25.1
Chloromethane ug/L 20 123 60-140108 1320ND24.6 21.6
cis-1,2-Dichloroethene ug/L 20 129 60-140129 020ND25.9 25.9
cis-1,3-Dichloropropene ug/L 20 104 60-140102 220ND20.8 20.4
Dibromochloromethane ug/L 20 110 60-140109 020ND21.9 21.9
Dibromomethane ug/L 20 112 60-140108 320ND22.3 21.7
Dichlorodifluoromethane ug/L M12014960-140139 720ND29.9 27.9
Diisopropyl ether ug/L 20 137 60-140135 120ND27.3 27.0
Ethylbenzene ug/L 20 129 60-140126 220ND25.7 25.2
Hexachloro-1,3-butadiene ug/L M12014660-140133 920ND29.3 26.6
Isopropylbenzene (Cumene)ug/L 20 132 60-140129 220ND26.4 25.9
m&p-Xylene ug/L 40 129 60-140127 240ND51.7 50.7
Methyl-tert-butyl ether ug/L 20 113 60-140111 220ND22.7 22.2
Methylene Chloride ug/L 20 125 60-140122 220ND25.0 24.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4121625MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92683581013
4121626
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L M12014460-140141 220ND28.8 28.1
n-Propylbenzene ug/L 20 137 60-140133 320ND27.3 26.6
Naphthalene ug/L 20 116 60-140109 620ND23.1 21.9
o-Xylene ug/L 20 129 60-140121 620ND25.7 24.3
sec-Butylbenzene ug/L 20 138 60-140133 320ND27.6 26.7
Styrene ug/L 20 132 60-140124 620ND26.5 24.9
tert-Butylbenzene ug/L 20 110 60-140106 320ND21.9 21.3
Tetrachloroethene ug/L 20 129 60-140127 120ND25.7 25.4
Toluene ug/L 20 113 60-140111 220ND22.6 22.2
trans-1,2-Dichloroethene ug/L 20 140 60-140139 120ND28.0 27.9
trans-1,3-Dichloropropene ug/L 20 101 60-140101 020ND20.2 20.2
Trichloroethene ug/L 20 127 60-140125 120ND25.3 25.0
Trichlorofluoromethane ug/L 20 136 60-140133 320ND27.3 26.6
Vinyl chloride ug/L 20 124 60-140108 1420ND24.9 21.6
1,2-Dichloroethane-d4 (S)%99 70-130100
4-Bromofluorobenzene (S)%99 70-13098
Toluene-d8 (S)%91 70-13091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
795442
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683799002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4121630
Associated Lab Samples:92683799002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/24/23 00:11
1,1,1-Trichloroethane ug/L ND 0.50 08/24/23 00:11
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/24/23 00:11
1,1,2-Trichloroethane ug/L ND 0.50 08/24/23 00:11
1,1-Dichloroethane ug/L ND 0.50 08/24/23 00:11
1,1-Dichloroethene ug/L ND 0.50 08/24/23 00:11
1,1-Dichloropropene ug/L ND 0.50 08/24/23 00:11
1,2,3-Trichlorobenzene ug/L ND 2.0 08/24/23 00:11
1,2,3-Trichloropropane ug/L ND 0.50 08/24/23 00:11
1,2,4-Trichlorobenzene ug/L ND 2.0 08/24/23 00:11
1,2,4-Trimethylbenzene ug/L ND 0.50 08/24/23 00:11
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/24/23 00:11
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/24/23 00:11
1,2-Dichlorobenzene ug/L ND 0.50 08/24/23 00:11
1,2-Dichloroethane ug/L ND 0.50 08/24/23 00:11
1,2-Dichloropropane ug/L ND 0.50 08/24/23 00:11
1,3,5-Trimethylbenzene ug/L ND 0.50 08/24/23 00:11
1,3-Dichlorobenzene ug/L ND 0.50 08/24/23 00:11
1,3-Dichloropropane ug/L ND 0.50 08/24/23 00:11
1,4-Dichlorobenzene ug/L ND 0.50 08/24/23 00:11
2,2-Dichloropropane ug/L ND 0.50 08/24/23 00:11
2-Chlorotoluene ug/L ND 0.50 08/24/23 00:11
4-Chlorotoluene ug/L ND 0.50 08/24/23 00:11
Benzene ug/L ND 0.50 08/24/23 00:11
Bromobenzene ug/L ND 0.50 08/24/23 00:11
Bromochloromethane ug/L ND 0.50 08/24/23 00:11
Bromodichloromethane ug/L ND 0.50 08/24/23 00:11
Bromoform ug/L ND 0.50 08/24/23 00:11
Bromomethane ug/L ND 5.0 08/24/23 00:11
Carbon tetrachloride ug/L ND 0.50 08/24/23 00:11
Chlorobenzene ug/L ND 0.50 08/24/23 00:11
Chloroethane ug/L ND 1.0 08/24/23 00:11
Chloroform ug/L ND 0.50 08/24/23 00:11
Chloromethane ug/L ND 1.0 08/24/23 00:11
cis-1,2-Dichloroethene ug/L ND 0.50 08/24/23 00:11
cis-1,3-Dichloropropene ug/L ND 0.50 08/24/23 00:11
Dibromochloromethane ug/L ND 0.50 08/24/23 00:11
Dibromomethane ug/L ND 0.50 08/24/23 00:11
Dichlorodifluoromethane ug/L ND 0.50 08/24/23 00:11
Diisopropyl ether ug/L ND 0.50 08/24/23 00:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4121630
Associated Lab Samples:92683799002
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 08/24/23 00:11
Hexachloro-1,3-butadiene ug/L ND 2.0 08/24/23 00:11
Isopropylbenzene (Cumene)ug/L ND 0.50 08/24/23 00:11
m&p-Xylene ug/L ND 1.0 08/24/23 00:11
Methyl-tert-butyl ether ug/L ND 0.50 08/24/23 00:11
Methylene Chloride ug/L ND 2.0 08/24/23 00:11
n-Butylbenzene ug/L ND 0.50 08/24/23 00:11
n-Propylbenzene ug/L ND 0.50 08/24/23 00:11
Naphthalene ug/L ND 2.0 08/24/23 00:11
o-Xylene ug/L ND 0.50 08/24/23 00:11
sec-Butylbenzene ug/L ND 0.50 08/24/23 00:11
Styrene ug/L ND 0.50 08/24/23 00:11
tert-Butylbenzene ug/L ND 0.50 08/24/23 00:11
Tetrachloroethene ug/L ND 0.50 08/24/23 00:11
Toluene ug/L ND 0.50 08/24/23 00:11
trans-1,2-Dichloroethene ug/L ND 0.50 08/24/23 00:11
trans-1,3-Dichloropropene ug/L ND 0.50 08/24/23 00:11
Trichloroethene ug/L ND 0.50 08/24/23 00:11
Trichlorofluoromethane ug/L ND 1.0 08/24/23 00:11
Vinyl chloride ug/L ND 1.0 08/24/23 00:11
1,2-Dichloroethane-d4 (S)%107 70-130 08/24/23 00:11
4-Bromofluorobenzene (S)%97 70-130 08/24/23 00:11
Toluene-d8 (S)%99 70-130 08/24/23 00:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4121631LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.120 100 60-140
1,1,1-Trichloroethane ug/L 20.620 103 60-140
1,1,2,2-Tetrachloroethane ug/L 20.220 101 60-140
1,1,2-Trichloroethane ug/L 21.020 105 60-140
1,1-Dichloroethane ug/L 20.020 100 60-140
1,1-Dichloroethene ug/L 21.820 109 60-140
1,1-Dichloropropene ug/L 21.720 108 60-140
1,2,3-Trichlorobenzene ug/L 20.220 101 60-140
1,2,3-Trichloropropane ug/L 19.320 97 60-140
1,2,4-Trichlorobenzene ug/L 19.520 98 60-140
1,2,4-Trimethylbenzene ug/L 20.220 101 60-140
1,2-Dibromo-3-chloropropane ug/L 19.720 98 60-140
1,2-Dibromoethane (EDB)ug/L 20.920 105 60-140
1,2-Dichlorobenzene ug/L 20.020 100 60-140
1,2-Dichloroethane ug/L 20.920 105 60-140
1,2-Dichloropropane ug/L 19.620 98 60-140
1,3,5-Trimethylbenzene ug/L 19.820 99 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4121631LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 20.220 101 60-140
1,3-Dichloropropane ug/L 19.920 100 60-140
1,4-Dichlorobenzene ug/L 19.020 95 60-140
2,2-Dichloropropane ug/L 20.520 103 60-140
2-Chlorotoluene ug/L 19.620 98 60-140
4-Chlorotoluene ug/L 19.320 97 60-140
Benzene ug/L 19.720 98 60-140
Bromobenzene ug/L 19.520 98 60-140
Bromochloromethane ug/L 21.520 107 60-140
Bromodichloromethane ug/L 19.920 100 60-140
Bromoform ug/L 20.220 101 60-140
Bromomethane ug/L 19.820 99 60-140
Carbon tetrachloride ug/L 19.820 99 60-140
Chlorobenzene ug/L 19.720 98 60-140
Chloroethane ug/L 19.920 99 60-140
Chloroform ug/L 20.120 101 60-140
Chloromethane ug/L 18.020 90 60-140
cis-1,2-Dichloroethene ug/L 20.220 101 60-140
cis-1,3-Dichloropropene ug/L 20.220 101 60-140
Dibromochloromethane ug/L 20.120 100 60-140
Dibromomethane ug/L 20.620 103 60-140
Dichlorodifluoromethane ug/L 22.520 113 60-140
Diisopropyl ether ug/L 19.320 96 60-140
Ethylbenzene ug/L 19.220 96 60-140
Hexachloro-1,3-butadiene ug/L 20.120 100 60-140
Isopropylbenzene (Cumene)ug/L 20.120 100 60-140
m&p-Xylene ug/L 39.040 97 60-140
Methyl-tert-butyl ether ug/L 19.520 98 60-140
Methylene Chloride ug/L 20.920 105 60-140
n-Butylbenzene ug/L 19.720 98 60-140
n-Propylbenzene ug/L 19.620 98 60-140
Naphthalene ug/L 21.120 105 60-140
o-Xylene ug/L 19.820 99 60-140
sec-Butylbenzene ug/L 19.720 98 60-140
Styrene ug/L 20.220 101 60-140
tert-Butylbenzene ug/L 18.320 92 60-140
Tetrachloroethene ug/L 19.720 99 60-140
Toluene ug/L 19.020 95 60-140
trans-1,2-Dichloroethene ug/L 20.820 104 60-140
trans-1,3-Dichloropropene ug/L 20.320 101 60-140
Trichloroethene ug/L 20.420 102 60-140
Trichlorofluoromethane ug/L 19.620 98 60-140
Vinyl chloride ug/L 16.320 81 60-140
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4121632MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92683950001
4121633
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 114 60-140121 620ND22.9 24.3
1,1,1-Trichloroethane ug/L 20 127 60-140134 520ND25.4 26.7
1,1,2,2-Tetrachloroethane ug/L 20 114 60-140120 520ND22.9 24.1
1,1,2-Trichloroethane ug/L 20 119 60-140124 420ND23.7 24.7
1,1-Dichloroethane ug/L 20 121 60-140126 420ND24.2 25.2
1,1-Dichloroethene ug/L M12014060-140145 420ND27.9 29.1
1,1-Dichloropropene ug/L 20 134 60-140139 320ND26.9 27.8
1,2,3-Trichlorobenzene ug/L 20 118 60-140122 320ND23.7 24.4
1,2,3-Trichloropropane ug/L 20 110 60-140116 520ND22.1 23.2
1,2,4-Trichlorobenzene ug/L 20 122 60-140120 220ND24.4 24.0
1,2,4-Trimethylbenzene ug/L 20 120 60-140125 420ND24.0 24.9
1,2-Dibromo-3-chloropropane ug/L 20 111 60-140112 120ND22.2 22.5
1,2-Dibromoethane (EDB)ug/L 20 117 60-140124 620ND23.5 24.9
1,2-Dichlorobenzene ug/L 20 114 60-140119 520ND22.7 23.8
1,2-Dichloroethane ug/L 20 121 60-140128 620ND24.2 25.6
1,2-Dichloropropane ug/L 20 116 60-140124 620ND23.3 24.8
1,3,5-Trimethylbenzene ug/L 20 120 60-140124 320ND23.9 24.7
1,3-Dichlorobenzene ug/L 20 118 60-140123 420ND23.6 24.5
1,3-Dichloropropane ug/L 20 115 60-140120 520ND23.0 24.1
1,4-Dichlorobenzene ug/L 20 113 60-140115 120ND22.7 23.0
2,2-Dichloropropane ug/L 20 132 60-140137 420ND26.5 27.5
2-Chlorotoluene ug/L 20 119 60-140122 320ND23.8 24.4
4-Chlorotoluene ug/L 20 115 60-140120 420ND23.0 24.0
Benzene ug/L 20 116 60-140121 420ND23.2 24.1
Bromobenzene ug/L 20 114 60-140117 320ND22.8 23.5
Bromochloromethane ug/L 20 121 60-140129 720ND24.2 25.8
Bromodichloromethane ug/L 20 117 60-140121 320ND23.4 24.2
Bromoform ug/L 20 113 60-140119 520ND22.5 23.7
Bromomethane ug/L 20 116 60-140127 920ND23.3 25.5
Carbon tetrachloride ug/L 20 126 60-140130 320ND25.2 26.1
Chlorobenzene ug/L 20 115 60-140119 320ND23.1 23.9
Chloroethane ug/L 20 118 60-140124 520ND23.6 24.9
Chloroform ug/L 20 124 60-140123 120ND24.9 24.6
Chloromethane ug/L 20 117 60-140121 320ND23.5 24.3
cis-1,2-Dichloroethene ug/L 20 121 60-140125 320ND24.1 24.9
cis-1,3-Dichloropropene ug/L 20 115 60-140121 520ND23.1 24.2
Dibromochloromethane ug/L 20 116 60-140120 420ND23.3 24.1
Dibromomethane ug/L 20 115 60-140117 120ND23.1 23.3
Dichlorodifluoromethane ug/L M12017260-140179 320ND34.5 35.7
Diisopropyl ether ug/L 20 113 60-140119 520ND22.6 23.8
Ethylbenzene ug/L 20 116 60-140121 420ND23.2 24.1
Hexachloro-1,3-butadiene ug/L 20 126 60-140132 520ND25.1 26.5
Isopropylbenzene (Cumene)ug/L 20 121 60-140126 420ND24.2 25.3
m&p-Xylene ug/L 40 116 60-140122 540ND46.6 48.8
Methyl-tert-butyl ether ug/L 20 110 60-140117 620ND22.1 23.4
Methylene Chloride ug/L 20 121 60-140125 420ND24.1 25.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4121632MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92683950001
4121633
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 122 60-140130 620ND24.4 25.9
n-Propylbenzene ug/L 20 120 60-140122 220ND23.9 24.4
Naphthalene ug/L 20 111 60-140121 920ND22.1 24.2
o-Xylene ug/L 20 114 60-140119 420ND22.9 23.7
sec-Butylbenzene ug/L 20 121 60-140126 420ND24.3 25.3
Styrene ug/L 20 120 60-140124 320ND23.9 24.8
tert-Butylbenzene ug/L 20 97 60-140100 320ND19.5 20.1
Tetrachloroethene ug/L 20 114 60-140121 620ND22.7 24.1
Toluene ug/L 20 115 60-140120 420ND22.9 24.0
trans-1,2-Dichloroethene ug/L 20 127 60-140133 420ND25.4 26.6
trans-1,3-Dichloropropene ug/L 20 116 60-140124 720ND23.2 24.8
Trichloroethene ug/L 20 122 60-140130 620ND24.4 26.0
Trichlorofluoromethane ug/L 20 133 60-140139 420ND26.6 27.7
Vinyl chloride ug/L 20 108 60-140113 420ND21.7 22.5
1,2-Dichloroethane-d4 (S)%106 70-130105
4-Bromofluorobenzene (S)%100 70-13099
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
795496
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683799010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4121925
Associated Lab Samples:92683799010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/25/23 01:02
1,1,1-Trichloroethane ug/L ND 0.50 08/25/23 01:02
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/25/23 01:02
1,1,2-Trichloroethane ug/L ND 0.50 08/25/23 01:02
1,1-Dichloroethane ug/L ND 0.50 08/25/23 01:02
1,1-Dichloroethene ug/L ND 0.50 08/25/23 01:02
1,1-Dichloropropene ug/L ND 0.50 08/25/23 01:02
1,2,3-Trichlorobenzene ug/L ND 2.0 08/25/23 01:02
1,2,3-Trichloropropane ug/L ND 0.50 08/25/23 01:02
1,2,4-Trichlorobenzene ug/L ND 2.0 08/25/23 01:02
1,2,4-Trimethylbenzene ug/L ND 0.50 08/25/23 01:02
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/25/23 01:02
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/25/23 01:02
1,2-Dichlorobenzene ug/L ND 0.50 08/25/23 01:02
1,2-Dichloroethane ug/L ND 0.50 08/25/23 01:02
1,2-Dichloropropane ug/L ND 0.50 08/25/23 01:02
1,3,5-Trimethylbenzene ug/L ND 0.50 08/25/23 01:02
1,3-Dichlorobenzene ug/L ND 0.50 08/25/23 01:02
1,3-Dichloropropane ug/L ND 0.50 08/25/23 01:02
1,4-Dichlorobenzene ug/L ND 0.50 08/25/23 01:02
2,2-Dichloropropane ug/L ND 0.50 08/25/23 01:02
2-Chlorotoluene ug/L ND 0.50 08/25/23 01:02
4-Chlorotoluene ug/L ND 0.50 08/25/23 01:02
Benzene ug/L ND 0.50 08/25/23 01:02
Bromobenzene ug/L ND 0.50 08/25/23 01:02
Bromochloromethane ug/L ND 0.50 08/25/23 01:02
Bromodichloromethane ug/L ND 0.50 08/25/23 01:02
Bromoform ug/L ND 0.50 08/25/23 01:02
Bromomethane ug/L ND 5.0 08/25/23 01:02
Carbon tetrachloride ug/L ND 0.50 08/25/23 01:02
Chlorobenzene ug/L ND 0.50 08/25/23 01:02
Chloroethane ug/L ND 1.0 08/25/23 01:02
Chloroform ug/L ND 0.50 08/25/23 01:02
Chloromethane ug/L ND 1.0 08/25/23 01:02
cis-1,2-Dichloroethene ug/L ND 0.50 08/25/23 01:02
cis-1,3-Dichloropropene ug/L ND 0.50 08/25/23 01:02
Dibromochloromethane ug/L ND 0.50 08/25/23 01:02
Dibromomethane ug/L ND 0.50 08/25/23 01:02
Dichlorodifluoromethane ug/L ND 0.50 08/25/23 01:02
Diisopropyl ether ug/L ND 0.50 08/25/23 01:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4121925
Associated Lab Samples:92683799010
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 08/25/23 01:02
Hexachloro-1,3-butadiene ug/L ND 2.0 08/25/23 01:02
Isopropylbenzene (Cumene)ug/L ND 0.50 08/25/23 01:02
m&p-Xylene ug/L ND 1.0 08/25/23 01:02
Methyl-tert-butyl ether ug/L ND 0.50 08/25/23 01:02
Methylene Chloride ug/L ND 2.0 08/25/23 01:02
n-Butylbenzene ug/L ND 0.50 08/25/23 01:02
n-Propylbenzene ug/L ND 0.50 08/25/23 01:02
Naphthalene ug/L ND 2.0 08/25/23 01:02
o-Xylene ug/L ND 0.50 08/25/23 01:02
sec-Butylbenzene ug/L ND 0.50 08/25/23 01:02
Styrene ug/L ND 0.50 08/25/23 01:02
tert-Butylbenzene ug/L ND 0.50 08/25/23 01:02
Tetrachloroethene ug/L ND 0.50 08/25/23 01:02
Toluene ug/L ND 0.50 08/25/23 01:02
trans-1,2-Dichloroethene ug/L ND 0.50 08/25/23 01:02
trans-1,3-Dichloropropene ug/L ND 0.50 08/25/23 01:02
Trichloroethene ug/L ND 0.50 08/25/23 01:02
Trichlorofluoromethane ug/L ND 1.0 08/25/23 01:02
Vinyl chloride ug/L ND 1.0 08/25/23 01:02
1,2-Dichloroethane-d4 (S)%112 70-130 08/25/23 01:02
4-Bromofluorobenzene (S)%95 70-130 08/25/23 01:02
Toluene-d8 (S)%96 70-130 08/25/23 01:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4121926LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.720 103 60-140
1,1,1-Trichloroethane ug/L 20.120 101 60-140
1,1,2,2-Tetrachloroethane ug/L 23.120 115 60-140
1,1,2-Trichloroethane ug/L 21.420 107 60-140
1,1-Dichloroethane ug/L 21.920 110 60-140
1,1-Dichloroethene ug/L 24.920 124 60-140
1,1-Dichloropropene ug/L 22.820 114 60-140
1,2,3-Trichlorobenzene ug/L 18.120 91 60-140
1,2,3-Trichloropropane ug/L 21.920 109 60-140
1,2,4-Trichlorobenzene ug/L 18.820 94 60-140
1,2,4-Trimethylbenzene ug/L 21.520 107 60-140
1,2-Dibromo-3-chloropropane ug/L 18.220 91 60-140
1,2-Dibromoethane (EDB)ug/L 21.820 109 60-140
1,2-Dichlorobenzene ug/L 22.220 111 60-140
1,2-Dichloroethane ug/L 21.520 107 60-140
1,2-Dichloropropane ug/L 22.520 113 60-140
1,3,5-Trimethylbenzene ug/L 22.220 111 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4121926LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 21.920 110 60-140
1,3-Dichloropropane ug/L 22.220 111 60-140
1,4-Dichlorobenzene ug/L 22.520 112 60-140
2,2-Dichloropropane ug/L 17.020 85 60-140
2-Chlorotoluene ug/L 22.320 111 60-140
4-Chlorotoluene ug/L 22.020 110 60-140
Benzene ug/L 21.920 109 60-140
Bromobenzene ug/L 21.920 110 60-140
Bromochloromethane ug/L 20.620 103 60-140
Bromodichloromethane ug/L 19.320 97 60-140
Bromoform ug/L 17.720 89 60-140
Bromomethane ug/L 24.420 122 60-140
Carbon tetrachloride ug/L 19.220 96 60-140
Chlorobenzene ug/L 21.920 110 60-140
Chloroethane ug/L 24.720 124 60-140
Chloroform ug/L 21.420 107 60-140
Chloromethane ug/L 18.020 90 60-140
cis-1,2-Dichloroethene ug/L 21.220 106 60-140
cis-1,3-Dichloropropene ug/L 19.120 95 60-140
Dibromochloromethane ug/L 19.420 97 60-140
Dibromomethane ug/L 19.920 99 60-140
Dichlorodifluoromethane ug/L 22.320 111 60-140
Diisopropyl ether ug/L 21.620 108 60-140
Ethylbenzene ug/L 21.520 108 60-140
Hexachloro-1,3-butadiene ug/L 19.920 99 60-140
Isopropylbenzene (Cumene)ug/L 21.420 107 60-140
m&p-Xylene ug/L 43.140 108 60-140
Methyl-tert-butyl ether ug/L 20.820 104 60-140
Methylene Chloride ug/L 23.120 115 60-140
n-Butylbenzene ug/L 21.920 109 60-140
n-Propylbenzene ug/L 22.120 110 60-140
Naphthalene ug/L 19.320 96 60-140
o-Xylene ug/L 21.320 106 60-140
sec-Butylbenzene ug/L 21.820 109 60-140
Styrene ug/L 21.820 109 60-140
tert-Butylbenzene ug/L 17.820 89 60-140
Tetrachloroethene ug/L 20.220 101 60-140
Toluene ug/L 20.220 101 60-140
trans-1,2-Dichloroethene ug/L 24.220 121 60-140
trans-1,3-Dichloropropene ug/L 18.320 92 60-140
Trichloroethene ug/L 20.720 103 60-140
Trichlorofluoromethane ug/L 20.920 105 60-140
Vinyl chloride ug/L 17.420 87 60-140
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4121927MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92684064001
4121928
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 132 60-140122 820<0.091 26.4 24.4
1,1,1-Trichloroethane ug/L 20 137 60-140127 720<0.11 27.3 25.4
1,1,2,2-Tetrachloroethane ug/L M12015460-140127 1920<0.074 30.8 25.5
1,1,2-Trichloroethane ug/L 20 136 60-140126 820<0.096 27.3 25.2
1,1-Dichloroethane ug/L M12014660-140135 820<0.056 29.3 27.1
1,1-Dichloroethene ug/L M12016960-140160 520<0.079 33.7 32.1
1,1-Dichloropropene ug/L M12016060-140146 920<0.066 31.9 29.2
1,2,3-Trichlorobenzene ug/L 20 113 60-140113 020<0.12 22.6 22.5
1,2,3-Trichloropropane ug/L M12014360-140122 1620<0.17 28.6 24.3
1,2,4-Trichlorobenzene ug/L 20 114 60-140115 120<0.16 22.7 23.0
1,2,4-Trimethylbenzene ug/L M12014460-140131 1020<0.031 28.9 26.2
1,2-Dibromo-3-chloropropane ug/L 20 110 60-140110 020<0.18 21.9 22.0
1,2-Dibromoethane (EDB)ug/L 20 135 60-140121 1120<0.15 27.0 24.2
1,2-Dichlorobenzene ug/L 20 136 60-140130 520<0.094 27.2 26.0
1,2-Dichloroethane ug/L 20 136 60-140126 820<0.11 27.3 25.2
1,2-Dichloropropane ug/L M12014760-140138 620<0.14 29.4 27.6
1,3,5-Trimethylbenzene ug/L M12015160-140136 1120<0.071 30.2 27.2
1,3-Dichlorobenzene ug/L 20 137 60-140130 620<0.098 27.5 25.9
1,3-Dichloropropane ug/L 20 140 60-140124 1120<0.085 27.9 24.9
1,4-Dichlorobenzene ug/L 20 136 60-140131 420<0.090 27.3 26.2
2,2-Dichloropropane ug/L 20 131 60-140122 820<0.12 26.3 24.4
2-Chlorotoluene ug/L M12014960-140134 1120<0.13 29.8 26.7
4-Chlorotoluene ug/L M12014760-140133 1020<0.096 29.4 26.6
Benzene ug/L M12014560-140134 820<0.079 29.1 26.8
Bromobenzene ug/L 20 140 60-140130 720<0.14 28.0 26.0
Bromochloromethane ug/L 20 132 60-140124 620<0.094 26.3 24.8
Bromodichloromethane ug/L 20 126 60-140116 820<0.17 25.2 23.2
Bromoform ug/L 20 114 60-140101 1220<0.20 22.8 20.2
Bromomethane ug/L M12017160-140155 1020<0.22 34.2 30.9
Carbon tetrachloride ug/L 20 133 60-140125 620<0.17 26.6 25.0
Chlorobenzene ug/L 20 139 60-140129 720<0.085 27.8 25.9
Chloroethane ug/L M12017260-140163 520<0.17 34.3 32.5
Chloroform ug/L 20 138 60-140125 1020<0.069 27.6 24.9
Chloromethane ug/L 20 122 60-140125 320<0.18 24.4 25.0
cis-1,2-Dichloroethene ug/L M12014160-140131 720<0.11 28.2 26.3
cis-1,3-Dichloropropene ug/L 20 123 60-140115 720<0.090 24.6 22.9
Dibromochloromethane ug/L 20 124 60-140110 1220<0.15 24.8 22.0
Dibromomethane ug/L 20 126 60-140116 820<0.19 25.2 23.3
Dichlorodifluoromethane ug/L M12014960-140141 520<0.12 29.8 28.2
Diisopropyl ether ug/L M12014660-140134 920<0.072 29.2 26.7
Ethylbenzene ug/L M12014160-140133 620<0.081 28.1 26.5
Hexachloro-1,3-butadiene ug/L 20 135 60-140130 420<0.35 27.0 26.0
Isopropylbenzene (Cumene)ug/L M12015360-140126 1920<0.11 30.5 25.3
m&p-Xylene ug/L 40 140 60-140131 740<0.094 56.1 52.5
Methyl-tert-butyl ether ug/L 20 124 60-140116 720<0.053 24.8 23.1
Methylene Chloride ug/L 20 134 60-140125 720<1.9 26.7 25.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4121927MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92684064001
4121928
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L M12015460-140142 920<0.066 30.9 28.3
n-Propylbenzene ug/L M12015460-140139 1020<0.10 30.7 27.7
Naphthalene ug/L 20 117 60-140115 220<0.10 23.3 23.0
o-Xylene ug/L 20 134 60-140121 1020<0.14 26.7 24.1
sec-Butylbenzene ug/L M12015160-140137 1020<0.085 30.3 27.5
Styrene ug/L 20 138 60-140122 1220<0.14 27.5 24.4
tert-Butylbenzene ug/L 20 121 60-140110 1020<0.086 24.2 22.0
Tetrachloroethene ug/L 20 138 60-140123 1220<0.086 27.7 24.6
Toluene ug/L 20 136 60-140124 920<0.090 27.1 24.9
trans-1,2-Dichloroethene ug/L M12014960-140139 720<0.10 29.7 27.8
trans-1,3-Dichloropropene ug/L 20 123 60-140114 720<0.13 24.5 22.8
Trichloroethene ug/L M12014160-140130 820<0.17 28.1 25.9
Trichlorofluoromethane ug/L M12015160-140145 420<0.14 30.2 29.0
Vinyl chloride ug/L 20 124 60-140126 120<0.15 24.9 25.2
1,2-Dichloroethane-d4 (S)%104 70-130105
4-Bromofluorobenzene (S)%107 70-13094
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
795737
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683799003, 92683799005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4123216
Associated Lab Samples:92683799003, 92683799005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/24/23 15:48
1,1,1-Trichloroethane ug/L ND 0.50 08/24/23 15:48
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/24/23 15:48
1,1,2-Trichloroethane ug/L ND 0.50 08/24/23 15:48
1,1-Dichloroethane ug/L ND 0.50 08/24/23 15:48
1,1-Dichloroethene ug/L ND 0.50 08/24/23 15:48
1,1-Dichloropropene ug/L ND 0.50 08/24/23 15:48
1,2,3-Trichlorobenzene ug/L ND 2.0 08/24/23 15:48
1,2,3-Trichloropropane ug/L ND 0.50 08/24/23 15:48
1,2,4-Trichlorobenzene ug/L ND 2.0 08/24/23 15:48
1,2,4-Trimethylbenzene ug/L ND 0.50 08/24/23 15:48
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/24/23 15:48
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/24/23 15:48
1,2-Dichlorobenzene ug/L ND 0.50 08/24/23 15:48
1,2-Dichloroethane ug/L ND 0.50 08/24/23 15:48
1,2-Dichloropropane ug/L ND 0.50 08/24/23 15:48
1,3,5-Trimethylbenzene ug/L ND 0.50 08/24/23 15:48
1,3-Dichlorobenzene ug/L ND 0.50 08/24/23 15:48
1,3-Dichloropropane ug/L ND 0.50 08/24/23 15:48
1,4-Dichlorobenzene ug/L ND 0.50 08/24/23 15:48
2,2-Dichloropropane ug/L ND 0.50 08/24/23 15:48
2-Chlorotoluene ug/L ND 0.50 08/24/23 15:48
4-Chlorotoluene ug/L ND 0.50 08/24/23 15:48
Benzene ug/L ND 0.50 08/24/23 15:48
Bromobenzene ug/L ND 0.50 08/24/23 15:48
Bromochloromethane ug/L ND 0.50 08/24/23 15:48
Bromodichloromethane ug/L ND 0.50 08/24/23 15:48
Bromoform ug/L ND 0.50 08/24/23 15:48
Bromomethane ug/L ND 5.0 08/24/23 15:48
Carbon tetrachloride ug/L ND 0.50 08/24/23 15:48
Chlorobenzene ug/L ND 0.50 08/24/23 15:48
Chloroethane ug/L ND 1.0 08/24/23 15:48
Chloroform ug/L ND 0.50 08/24/23 15:48
Chloromethane ug/L ND 1.0 08/24/23 15:48
cis-1,2-Dichloroethene ug/L ND 0.50 08/24/23 15:48
cis-1,3-Dichloropropene ug/L ND 0.50 08/24/23 15:48
Dibromochloromethane ug/L ND 0.50 08/24/23 15:48
Dibromomethane ug/L ND 0.50 08/24/23 15:48
Dichlorodifluoromethane ug/L ND 0.50 08/24/23 15:48
Diisopropyl ether ug/L ND 0.50 08/24/23 15:48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 39 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4123216
Associated Lab Samples:92683799003, 92683799005
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 08/24/23 15:48
Hexachloro-1,3-butadiene ug/L ND 2.0 08/24/23 15:48
Isopropylbenzene (Cumene)ug/L ND 0.50 08/24/23 15:48
m&p-Xylene ug/L ND 1.0 08/24/23 15:48
Methyl-tert-butyl ether ug/L ND 0.50 08/24/23 15:48
Methylene Chloride ug/L ND 2.0 08/24/23 15:48
n-Butylbenzene ug/L ND 0.50 08/24/23 15:48
n-Propylbenzene ug/L ND 0.50 08/24/23 15:48
Naphthalene ug/L ND 2.0 08/24/23 15:48
o-Xylene ug/L ND 0.50 08/24/23 15:48
sec-Butylbenzene ug/L ND 0.50 08/24/23 15:48
Styrene ug/L ND 0.50 08/24/23 15:48
tert-Butylbenzene ug/L ND 0.50 08/24/23 15:48
Tetrachloroethene ug/L ND 0.50 08/24/23 15:48
Toluene ug/L ND 0.50 08/24/23 15:48
trans-1,2-Dichloroethene ug/L ND 0.50 08/24/23 15:48
trans-1,3-Dichloropropene ug/L ND 0.50 08/24/23 15:48
Trichloroethene ug/L ND 0.50 08/24/23 15:48
Trichlorofluoromethane ug/L ND 1.0 08/24/23 15:48
Vinyl chloride ug/L ND 1.0 08/24/23 15:48
1,2-Dichloroethane-d4 (S)%101 70-130 08/24/23 15:48
4-Bromofluorobenzene (S)%101 70-130 08/24/23 15:48
Toluene-d8 (S)%101 70-130 08/24/23 15:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4123217LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 24.520 122 60-140
1,1,1-Trichloroethane ug/L 24.320 122 60-140
1,1,2,2-Tetrachloroethane ug/L 22.920 115 60-140
1,1,2-Trichloroethane ug/L 23.420 117 60-140
1,1-Dichloroethane ug/L 23.020 115 60-140
1,1-Dichloroethene ug/L 24.420 122 60-140
1,1-Dichloropropene ug/L 25.220 126 60-140
1,2,3-Trichlorobenzene ug/L 24.620 123 60-140
1,2,3-Trichloropropane ug/L 22.220 111 60-140
1,2,4-Trichlorobenzene ug/L 22.720 114 60-140
1,2,4-Trimethylbenzene ug/L 23.020 115 60-140
1,2-Dibromo-3-chloropropane ug/L 23.920 119 60-140
1,2-Dibromoethane (EDB)ug/L 23.120 115 60-140
1,2-Dichlorobenzene ug/L 23.120 116 60-140
1,2-Dichloroethane ug/L 22.420 112 60-140
1,2-Dichloropropane ug/L 23.620 118 60-140
1,3,5-Trimethylbenzene ug/L 23.220 116 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 40 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4123217LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 23.920 119 60-140
1,3-Dichloropropane ug/L 21.920 109 60-140
1,4-Dichlorobenzene ug/L 22.420 112 60-140
2,2-Dichloropropane ug/L 23.320 117 60-140
2-Chlorotoluene ug/L 22.420 112 60-140
4-Chlorotoluene ug/L 23.020 115 60-140
Benzene ug/L 22.220 111 60-140
Bromobenzene ug/L 22.520 113 60-140
Bromochloromethane ug/L 24.320 122 60-140
Bromodichloromethane ug/L 23.220 116 60-140
Bromoform ug/L 21.020 105 60-140
Bromomethane ug/L 21.320 106 60-140
Carbon tetrachloride ug/L 25.120 125 60-140
Chlorobenzene ug/L 22.120 111 60-140
Chloroethane ug/L 22.720 113 60-140
Chloroform ug/L 23.220 116 60-140
Chloromethane ug/L 21.120 105 60-140
cis-1,2-Dichloroethene ug/L 24.020 120 60-140
cis-1,3-Dichloropropene ug/L 24.320 121 60-140
Dibromochloromethane ug/L 21.120 106 60-140
Dibromomethane ug/L 24.720 124 60-140
Dichlorodifluoromethane ug/L 30.5 L12015360-140
Diisopropyl ether ug/L 23.120 116 60-140
Ethylbenzene ug/L 21.820 109 60-140
Hexachloro-1,3-butadiene ug/L 23.420 117 60-140
Isopropylbenzene (Cumene)ug/L 23.920 120 60-140
m&p-Xylene ug/L 44.340 111 60-140
Methyl-tert-butyl ether ug/L 21.620 108 60-140
Methylene Chloride ug/L 21.820 109 60-140
n-Butylbenzene ug/L 23.420 117 60-140
n-Propylbenzene ug/L 22.220 111 60-140
Naphthalene ug/L 24.020 120 60-140
o-Xylene ug/L 22.020 110 60-140
sec-Butylbenzene ug/L 23.020 115 60-140
Styrene ug/L 23.220 116 60-140
tert-Butylbenzene ug/L 22.120 110 60-140
Tetrachloroethene ug/L 24.520 123 60-140
Toluene ug/L 21.820 109 60-140
trans-1,2-Dichloroethene ug/L 24.320 122 60-140
trans-1,3-Dichloropropene ug/L 23.720 118 60-140
Trichloroethene ug/L 24.720 123 60-140
Trichlorofluoromethane ug/L 24.220 121 60-140
Vinyl chloride ug/L 20.520 103 60-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 41 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4123218MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92684314002
4123219
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 125 60-140133 620ND25.0 26.5
1,1,1-Trichloroethane ug/L 20 126 60-140136 820ND25.3 27.3
1,1,2,2-Tetrachloroethane ug/L 20 115 60-140124 820ND22.9 24.8
1,1,2-Trichloroethane ug/L 20 121 60-140128 520ND24.3 25.6
1,1-Dichloroethane ug/L 20 118 60-140126 620ND23.6 25.1
1,1-Dichloroethene ug/L M12013260-140142 720ND26.5 28.4
1,1-Dichloropropene ug/L 20 131 60-140137 520ND26.2 27.5
1,2,3-Trichlorobenzene ug/L 20 115 60-140123 720ND23.0 24.7
1,2,3-Trichloropropane ug/L 20 105 60-140111 620ND21.0 22.3
1,2,4-Trichlorobenzene ug/L 20 114 60-140119 420ND22.9 23.8
1,2,4-Trimethylbenzene ug/L 20 120 60-140129 720ND24.1 25.8
1,2-Dibromo-3-chloropropane ug/L 20 112 60-140119 620ND22.4 23.9
1,2-Dibromoethane (EDB)ug/L 20 119 60-140129 820ND23.8 25.9
1,2-Dichlorobenzene ug/L 20 116 60-140123 620ND23.2 24.7
1,2-Dichloroethane ug/L 20 115 60-140123 720ND22.9 24.5
1,2-Dichloropropane ug/L 20 121 60-140127 420ND24.2 25.3
1,3,5-Trimethylbenzene ug/L 20 121 60-140126 420ND24.2 25.3
1,3-Dichlorobenzene ug/L 20 118 60-140126 720ND23.5 25.2
1,3-Dichloropropane ug/L 20 115 60-140124 720ND23.1 24.9
1,4-Dichlorobenzene ug/L 20 114 60-140123 820ND22.7 24.6
2,2-Dichloropropane ug/L 20 131 60-140135 220ND26.3 26.9
2-Chlorotoluene ug/L 20 117 60-140125 620ND23.4 25.0
4-Chlorotoluene ug/L 20 119 60-140128 720ND23.9 25.6
Benzene ug/L 20 121 60-140128 520ND24.3 25.6
Bromobenzene ug/L 20 119 60-140127 720ND23.7 25.3
Bromochloromethane ug/L 20 120 60-140128 620ND24.1 25.5
Bromodichloromethane ug/L 20 116 60-140125 720ND23.3 25.0
Bromoform ug/L 20 114 60-140127 1120ND22.7 25.4
Bromomethane ug/L 20 106 60-140112 620ND21.1 22.4
Carbon tetrachloride ug/L 20 130 60-140138 520ND26.1 27.5
Chlorobenzene ug/L 20 116 60-140125 820ND23.1 25.0
Chloroethane ug/L 20 104 60-140110 620ND20.7 22.1
Chloroform ug/L 20 112 60-140123 920ND22.4 24.6
Chloromethane ug/L 20 102 60-140108 620ND20.3 21.6
cis-1,2-Dichloroethene ug/L 20 116 60-140126 820ND23.3 25.2
cis-1,3-Dichloropropene ug/L 20 119 60-140129 820ND23.8 25.7
Dibromochloromethane ug/L 20 119 60-140129 820ND23.8 25.8
Dibromomethane ug/L 20 117 60-140121 320ND23.4 24.2
Dichlorodifluoromethane ug/L M02013960-140146 520ND27.8 29.2
Diisopropyl ether ug/L 20 109 60-140118 720ND21.9 23.6
Ethylbenzene ug/L 20 118 60-140125 620ND23.5 25.0
Hexachloro-1,3-butadiene ug/L 20 120 60-140128 720ND23.9 25.7
Isopropylbenzene (Cumene)ug/L 20 122 60-140130 720ND24.4 26.1
m&p-Xylene ug/L 40 119 60-140125 540ND47.8 50.2
Methyl-tert-butyl ether ug/L 20 104 60-140110 620ND21.1 22.5
Methylene Chloride ug/L 20 106 60-140113 620ND21.3 22.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 42 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4123218MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92684314002
4123219
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 125 60-140131 520ND25.0 26.2
n-Propylbenzene ug/L 20 118 60-140125 620ND23.5 24.9
Naphthalene ug/L 20 113 60-140122 720ND22.8 24.5
o-Xylene ug/L 20 115 60-140125 820ND23.0 25.0
sec-Butylbenzene ug/L 20 122 60-140128 520ND24.4 25.6
Styrene ug/L 20 120 60-140128 720ND24.0 25.7
tert-Butylbenzene ug/L 20 99 60-140105 620ND19.8 20.9
Tetrachloroethene ug/L 20 121 60-140128 620ND24.1 25.5
Toluene ug/L 20 116 60-140122 520ND23.2 24.4
trans-1,2-Dichloroethene ug/L 20 128 60-140137 720ND25.7 27.5
trans-1,3-Dichloropropene ug/L 20 117 60-140124 620ND23.5 24.8
Trichloroethene ug/L 20 126 60-140132 520ND25.2 26.4
Trichlorofluoromethane ug/L 20 121 60-140130 720ND24.2 25.9
Vinyl chloride ug/L 20 101 60-140109 820ND20.1 21.8
1,2-Dichloroethane-d4 (S)%95 70-13095
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 43 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
796841
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683799009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4128226
Associated Lab Samples:92683799009
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/31/23 00:00
1,1,1-Trichloroethane ug/L ND 0.50 08/31/23 00:00
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/31/23 00:00
1,1,2-Trichloroethane ug/L ND 0.50 08/31/23 00:00
1,1-Dichloroethane ug/L ND 0.50 08/31/23 00:00
1,1-Dichloroethene ug/L ND 0.50 08/31/23 00:00
1,1-Dichloropropene ug/L ND 0.50 08/31/23 00:00
1,2,3-Trichlorobenzene ug/L ND 2.0 08/31/23 00:00
1,2,3-Trichloropropane ug/L ND 0.50 08/31/23 00:00
1,2,4-Trichlorobenzene ug/L ND 2.0 08/31/23 00:00
1,2,4-Trimethylbenzene ug/L ND 0.50 08/31/23 00:00
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/31/23 00:00
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/31/23 00:00
1,2-Dichlorobenzene ug/L ND 0.50 08/31/23 00:00
1,2-Dichloroethane ug/L ND 0.50 08/31/23 00:00
1,2-Dichloropropane ug/L ND 0.50 08/31/23 00:00
1,3,5-Trimethylbenzene ug/L ND 0.50 08/31/23 00:00
1,3-Dichlorobenzene ug/L ND 0.50 08/31/23 00:00
1,3-Dichloropropane ug/L ND 0.50 08/31/23 00:00
1,4-Dichlorobenzene ug/L ND 0.50 08/31/23 00:00
2,2-Dichloropropane ug/L ND 0.50 08/31/23 00:00
2-Chlorotoluene ug/L ND 0.50 08/31/23 00:00
4-Chlorotoluene ug/L ND 0.50 08/31/23 00:00
Benzene ug/L ND 0.50 08/31/23 00:00
Bromobenzene ug/L ND 0.50 08/31/23 00:00
Bromochloromethane ug/L ND 0.50 08/31/23 00:00
Bromodichloromethane ug/L ND 0.50 08/31/23 00:00
Bromoform ug/L ND 0.50 08/31/23 00:00
Bromomethane ug/L ND 5.0 08/31/23 00:00
Carbon tetrachloride ug/L ND 0.50 08/31/23 00:00
Chlorobenzene ug/L ND 0.50 08/31/23 00:00
Chloroethane ug/L ND 1.0 08/31/23 00:00
Chloroform ug/L ND 0.50 08/31/23 00:00
Chloromethane ug/L ND 1.0 08/31/23 00:00
cis-1,2-Dichloroethene ug/L ND 0.50 08/31/23 00:00
cis-1,3-Dichloropropene ug/L ND 0.50 08/31/23 00:00
Dibromochloromethane ug/L ND 0.50 08/31/23 00:00
Dibromomethane ug/L ND 0.50 08/31/23 00:00
Dichlorodifluoromethane ug/L ND 0.50 08/31/23 00:00
Diisopropyl ether ug/L ND 0.50 08/31/23 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 44 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4128226
Associated Lab Samples:92683799009
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 08/31/23 00:00
Hexachloro-1,3-butadiene ug/L ND 2.0 08/31/23 00:00
Isopropylbenzene (Cumene)ug/L ND 0.50 08/31/23 00:00
m&p-Xylene ug/L ND 1.0 08/31/23 00:00
Methyl-tert-butyl ether ug/L ND 0.50 08/31/23 00:00
Methylene Chloride ug/L ND 2.0 08/31/23 00:00
n-Butylbenzene ug/L ND 0.50 08/31/23 00:00
n-Propylbenzene ug/L ND 0.50 08/31/23 00:00
Naphthalene ug/L ND 2.0 08/31/23 00:00
o-Xylene ug/L ND 0.50 08/31/23 00:00
sec-Butylbenzene ug/L ND 0.50 08/31/23 00:00
Styrene ug/L ND 0.50 08/31/23 00:00
tert-Butylbenzene ug/L ND 0.50 08/31/23 00:00
Tetrachloroethene ug/L ND 0.50 08/31/23 00:00
Toluene ug/L ND 0.50 08/31/23 00:00
trans-1,2-Dichloroethene ug/L ND 0.50 08/31/23 00:00
trans-1,3-Dichloropropene ug/L ND 0.50 08/31/23 00:00
Trichloroethene ug/L ND 0.50 08/31/23 00:00
Trichlorofluoromethane ug/L ND 1.0 08/31/23 00:00
Vinyl chloride ug/L ND 1.0 08/31/23 00:00
1,2-Dichloroethane-d4 (S)%114 70-130 08/31/23 00:00
4-Bromofluorobenzene (S)%95 70-130 08/31/23 00:00
Toluene-d8 (S)%98 70-130 08/31/23 00:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4128227LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.720 104 60-140
1,1,1-Trichloroethane ug/L 20.420 102 60-140
1,1,2,2-Tetrachloroethane ug/L 23.920 120 60-140
1,1,2-Trichloroethane ug/L 21.920 110 60-140
1,1-Dichloroethane ug/L 22.920 115 60-140
1,1-Dichloroethene ug/L 23.720 118 60-140
1,1-Dichloropropene ug/L 23.720 118 60-140
1,2,3-Trichlorobenzene ug/L 18.220 91 60-140
1,2,3-Trichloropropane ug/L 22.720 113 60-140
1,2,4-Trichlorobenzene ug/L 18.520 92 60-140
1,2,4-Trimethylbenzene ug/L 21.920 109 60-140
1,2-Dibromo-3-chloropropane ug/L 19.020 95 60-140
1,2-Dibromoethane (EDB)ug/L 21.820 109 60-140
1,2-Dichlorobenzene ug/L 22.120 110 60-140
1,2-Dichloroethane ug/L 22.120 111 60-140
1,2-Dichloropropane ug/L 23.320 116 60-140
1,3,5-Trimethylbenzene ug/L 22.420 112 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 45 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4128227LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 21.820 109 60-140
1,3-Dichloropropane ug/L 22.620 113 60-140
1,4-Dichlorobenzene ug/L 22.020 110 60-140
2,2-Dichloropropane ug/L 18.220 91 60-140
2-Chlorotoluene ug/L 22.320 111 60-140
4-Chlorotoluene ug/L 22.120 110 60-140
Benzene ug/L 22.320 111 60-140
Bromobenzene ug/L 21.820 109 60-140
Bromochloromethane ug/L 21.020 105 60-140
Bromodichloromethane ug/L 19.620 98 60-140
Bromoform ug/L 18.620 93 60-140
Bromomethane ug/L 20.220 101 60-140
Carbon tetrachloride ug/L 19.120 96 60-140
Chlorobenzene ug/L 21.920 110 60-140
Chloroethane ug/L 25.920 129 60-140
Chloroform ug/L 21.720 108 60-140
Chloromethane ug/L 16.520 82 60-140
cis-1,2-Dichloroethene ug/L 22.120 110 60-140
cis-1,3-Dichloropropene ug/L 19.920 99 60-140
Dibromochloromethane ug/L 19.320 96 60-140
Dibromomethane ug/L 19.520 98 60-140
Dichlorodifluoromethane ug/L 19.120 96 60-140
Diisopropyl ether ug/L 22.820 114 60-140
Ethylbenzene ug/L 22.120 110 60-140
Hexachloro-1,3-butadiene ug/L 18.920 95 60-140
Isopropylbenzene (Cumene)ug/L 21.920 109 60-140
m&p-Xylene ug/L 43.540 109 60-140
Methyl-tert-butyl ether ug/L 19.920 99 60-140
Methylene Chloride ug/L 21.220 106 60-140
n-Butylbenzene ug/L 22.420 112 60-140
n-Propylbenzene ug/L 22.720 114 60-140
Naphthalene ug/L 20.020 100 60-140
o-Xylene ug/L 21.220 106 60-140
sec-Butylbenzene ug/L 21.920 110 60-140
Styrene ug/L 22.020 110 60-140
tert-Butylbenzene ug/L 17.920 89 60-140
Tetrachloroethene ug/L 19.820 99 60-140
Toluene ug/L 20.320 101 60-140
trans-1,2-Dichloroethene ug/L 22.720 113 60-140
trans-1,3-Dichloropropene ug/L 19.020 95 60-140
Trichloroethene ug/L 20.820 104 60-140
Trichlorofluoromethane ug/L 20.720 104 60-140
Vinyl chloride ug/L 17.920 89 60-140
1,2-Dichloroethane-d4 (S)%109 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 46 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4128228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92685018001
4128229
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L M12013760-140145 620ND27.4 29.0
1,1,1-Trichloroethane ug/L M12014360-140147 320ND28.6 29.4
1,1,2,2-Tetrachloroethane ug/L M12015260-140159 520ND30.4 31.9
1,1,2-Trichloroethane ug/L M12014060-140146 420ND28.0 29.3
1,1-Dichloroethane ug/L M12015860-140162 320ND31.5 32.4
1,1-Dichloroethene ug/L M12016960-140173 220ND33.8 34.6
1,1-Dichloropropene ug/L M12016960-140173 220ND33.8 34.5
1,2,3-Trichlorobenzene ug/L 20 114 60-140124 820ND22.8 24.8
1,2,3-Trichloropropane ug/L M12014460-140150 520ND28.7 30.1
1,2,4-Trichlorobenzene ug/L 20 118 60-140128 820ND23.7 25.6
1,2,4-Trimethylbenzene ug/L M12014860-140155 520ND29.7 31.0
1,2-Dibromo-3-chloropropane ug/L 20 118 60-140123 420ND23.6 24.6
1,2-Dibromoethane (EDB)ug/L M12014160-140148 520ND28.2 29.6
1,2-Dichlorobenzene ug/L M12014260-140150 520ND28.4 30.0
1,2-Dichloroethane ug/L M12014760-140152 320ND29.4 30.3
1,2-Dichloropropane ug/L M12015560-140163 520ND30.9 32.6
1,3,5-Trimethylbenzene ug/L M12015260-140161 620ND30.4 32.1
1,3-Dichlorobenzene ug/L M12014560-140152 420ND29.0 30.3
1,3-Dichloropropane ug/L M12014860-140153 320ND29.6 30.5
1,4-Dichlorobenzene ug/L M12014660-140151 420ND29.1 30.2
2,2-Dichloropropane ug/L M12013660-140143 520ND27.2 28.7
2-Chlorotoluene ug/L M12015160-140160 520ND30.3 31.9
4-Chlorotoluene ug/L M12014960-140158 620ND29.9 31.7
Benzene ug/L M12015260-140157 320ND30.4 31.4
Bromobenzene ug/L M12014160-140149 620ND28.2 29.8
Bromochloromethane ug/L M12014060-140145 420ND28.0 29.1
Bromodichloromethane ug/L 20 131 60-140136 420ND26.2 27.3
Bromoform ug/L 20 117 60-140125 620ND23.5 25.0
Bromomethane ug/L M12014560-140153 520ND29.0 30.5
Carbon tetrachloride ug/L 20 137 60-140140 320ND27.3 28.1
Chlorobenzene ug/L M12014660-140153 520ND29.3 30.7
Chloroethane ug/L M12017560-140180 220ND35.1 35.9
Chloroform ug/L M12014660-140151 4200.26J 29.4 30.5
Chloromethane ug/L 20 96 60-140101 420ND19.3 20.1
cis-1,2-Dichloroethene ug/L M12015160-140156 420ND30.2 31.3
cis-1,3-Dichloropropene ug/L 20 130 60-140135 420ND25.9 27.0
Dibromochloromethane ug/L 20 129 60-140134 420ND25.8 26.8
Dibromomethane ug/L 20 124 60-140128 420ND24.7 25.6
Dichlorodifluoromethane ug/L 20 87 60-14088 220ND17.3 17.7
Diisopropyl ether ug/L M12015160-140158 420ND30.2 31.5
Ethylbenzene ug/L M12014860-140156 620ND29.6 31.3
Hexachloro-1,3-butadiene ug/L M12014560-140151 420ND29.0 30.3
Isopropylbenzene (Cumene)ug/L M12014960-140158 620ND29.7 31.7
m&p-Xylene ug/L M14014760-140155 540ND58.7 61.9
Methyl-tert-butyl ether ug/L 20 126 60-140133 520ND25.3 26.6
Methylene Chloride ug/L M12014260-140148 420ND28.3 29.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 47 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683799
ONE STOP 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4128228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92685018001
4128229
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L M12016760-140171 220ND33.4 34.2
n-Propylbenzene ug/L M12015860-140165 420ND31.6 33.0
Naphthalene ug/L 20 115 60-140129 1120ND23.0 25.7
o-Xylene ug/L M12013960-140148 620ND27.8 29.5
sec-Butylbenzene ug/L M12015860-140165 420ND31.6 33.0
Styrene ug/L M12014460-140154 720ND28.8 30.9
tert-Butylbenzene ug/L 20 125 60-140131 520ND24.9 26.3
Tetrachloroethene ug/L M12013960-140145 520ND27.8 29.1
Toluene ug/L M12013960-140143 320ND27.7 28.7
trans-1,2-Dichloroethene ug/L M12016060-140164 320ND32.0 32.9
trans-1,3-Dichloropropene ug/L 20 127 60-140133 420ND25.5 26.5
Trichloroethene ug/L M12014060-140148 520ND28.0 29.5
Trichlorofluoromethane ug/L M12015260-140155 220ND30.4 30.9
Vinyl chloride ug/L 20 110 60-140116 620ND22.0 23.3
1,2-Dichloroethane-d4 (S)%110 70-130110
4-Bromofluorobenzene (S)%98 70-130100
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 48 of 53
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92683799
ONE STOP 15
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 49 of 53
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92683799
ONE STOP 15
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92683799001 795441WSW-1 SM 6200B
92683799002 795442MW-1R SM 6200B
92683799003 795737MW-2 SM 6200B
92683799004 795441MW-3 SM 6200B
92683799005 795737MW-4 SM 6200B
92683799006 795441MW-5 SM 6200B
92683799007 795441MW-6 SM 6200B
92683799008 795441MW-7 SM 6200B
92683799009 796841MW-8 SM 6200B
92683799010 795496MW-9 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/31/2023 03:23 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 50 of 53
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