AS-3704_28838_CA_MRP_20230108

GROUNDWATER MONITORING REPORT

HOT SPOT 2002
704 EAST MAIN STREET, BURNSVILLE, NC 28714
GROUNDWATER INCIDENT #: 28838; FACILITY ID #: 00-0-0000006505
LATITUDE: N 35.916292o; LONGITUDE: W -82.285840o (From GPS)

JANUARY 8, 2023

UST OWNER/OPERATOR:
R.L. Jordan Oil Company of North Carolina, Inc., 1451 Fernwood Glendale Road
Spartanburg, SC 29307; Phone Number: [phone]

PROPERTY OWNER:
Owner: R.L. RJOC Holdings Co., 1451 Fernwood Glendale Rd, Spartanburg, SC 29307
Phone Number: [phone]; Occupant: Unoccupied

CONSULTANT:
Henry Nemargut Engineering Services, 2211 Chestnut Street, Wilmington, NC 28405 Phone Number: [phone]

LABORATORY:
Pace Analytical Services, Inc., 9800 Kincey Ave, Suite 100, Huntersville, NC 28078
Phone Number: [phone]; State Certification #12

RELEASE INFORMATION:
Date Discovered: 4/14/2010; Estimated Quantity of Release: Unknown Cause of Release: Unknown; Source of Release: UST System Size-Contents: (2) 8,000 Gal + (1) 6,000 Gal Gasoline USTs; (1) 8,000 Gal Diesel UST; (1) 4,000 Gal Kerosene; + (1) 4000 & (1) 3000 Gal Unregistered Gasoline USTs

The Monitoring Report for this site has been prepared by Henry Nemargut Engineering
Services. All engineering work performed on this project was conducted under my direct
supervision:

Henry Nemargut, P.E.
Henry Nemargut Engineering Services
North Carolina License #17669

January 8, 2023

Mr. Troy Knox
R.L. Jordan Oil Company of North Carolina, Inc.
1451 Fernwood Glendale Road
Spartanburg, SC 29307

Reference: Groundwater Monitoring Report
Hot Spot 2002
704 East Main Street
Burnsville, Yancey County, North Carolina 28714
Groundwater Incident #28838
Facility ID # 00-0-0000006505

Dear Mr. Knox:

In accordance with an approved Task Authorization Form (TAF) from the North Carolina Department of Environmental Quality (NCDEQ), contained herein is a Groundwater Monitoring Report for the release which occurred at the above referenced facility. The field activities for this project consisted of sampling of existing monitoring and water supply wells. All activities were conducted in accordance with the NCDEQ guidelines and the requirements of 15A NCAC 2L .0115.

Mr. Knox, please contact me at [phone] if you have questions regarding this report.

Sincerely,

Henry Nemargut, P.E.
Henry Nemargut Engineering Services
B. EXECUTIVE SUMMARY
1. Free Product: Free product has not been observed at this site during the only 2 sampling/gauging events conducted since approved soil/free product remedial excavation was conducted in September-October, 2021 and completed in March, 2022. Free product at the site has apparently been remediated via the (2) soil remediation projects conducted at this site based on post-excavation monitoring.
2. Contaminant Mass: Contaminant mass calculations cannot be completed at this time since the residual contamination which remains in place is predominantly situated beneath the former store building prohibiting the definition of the vertical and horizontal extent of contamination; however, dissolved constituent concentrations observed in the installed monitoring network have decreased significantly since the final soil excavation and placement of biodegradation materials conducted at the site on March 8, 2022. 3. Maximum Concentrations of Dissolved Groundwater Contaminants:

Current Groundwater Maximums:
Contaminant Result Well ID 2L Standard Benzene 66.1 ug/L (MW-5R) 1 ug/L Toluene 15.8 ug/L (MW-2R) 600 ug/L Ethylbenzene 122 ug/L (MW-2R) 600 ug/L Naphthalene 62.7 ug/L (MW-8) 6 ug/L MTBE 71 ug/L (MW-5R) 20 ug/L Total 6200B 585 ug/L (MW-2R) NSE (3) compounds exceeded 2L Standards for 6200B compounds during the latest groundwater monitoring event for this site. No GCL violations were noted. No compounds exceeded 10X 15 NCAC 2B Standards applicable for this release site. 4. Extent of Dissolved Groundwater Contamination: The plume of dissolved groundwater contamination has not been defined horizontally or vertically at this site. Additional monitoring wells will be required to more accurately assess the extent of 2L exceedances at this site. 5. Maximum Soil Contaminant Concentrations (Post IAA Excavation): Contaminant Result Sample ID Lowest MSCC Benzene 1.030 mg/kg (UB2) 0.0072 mg/kg Toluene 27.0 mg/kg (UB2) 5.4 mg/kg Ethylbenzene 16.1 mg/kg (UB2) 8.0 mg/kg Xylenes 92.5 mg/kg (UB2) 6.0 mg/kg Naphthalene 7.83 mg/kg (UB2) 0.2 mg/kg Isopropylbenzene 1.98 mg/kg (UB2) 1.3 mg/kg n-Propylbenzene 6.98 mg/kg (UB2) 1.4 mg/kg 1,2,4-Trimethylbenzene 44.9 mg/kg (UB2) 6.6 mg/kg 1,3,5-Trimethylbenzene 12.9 mg/kg (UB2) 6.6 mg/kg C5-C8 Aliphatics 639 mg/kg (UB2) 68 mg/kg C9-C18 Aliphatics 1072 mg/kg (UB2) 540 mg/kg C9-C22 Aromatics 506 mg/kg (UB2) 31 mg/kg
Based on the site use, Commercial/Industrial MSCC standards apply for this site. 3 compounds/compound groups exceed Residential MSCCs; however, no soil concentrations are noted to exceed Commercial/Industrial standards. 6. Remedial Action Plan:
Soil remediation and biological treatment activities have been conducted at this site as follows:  2,722.76 tons of soil/free product were excavated from September-October, 2021 at this site and transported for off-site disposal.  117.27 tons of soil/free product were excavated on March 8, 2022 at this site and transported for off-site disposal.  Nutrients, straw, and concentrated bio-degradation liquids were placed back into the remedial excavation prior to and during backfill of the 3/8/22 remedial excavation to accelerate natural processes in the UST release source area of this site.

7. Impacted Receptors:
No water supply wells are located within 1000’ of the release source at this facility. Little Crabtree Creek borders the southern edge of the property. This creek was tested several times by Terry Environmental Services throughout the monitoring history of this site and has failed to indicate any impact from the petroleum release originating at the Hot Spot 2002 facility. A monitoring well network installed at the site in 2010- 2012 included (3) monitoring wells which were situated along Crabtree Creek and are located between the UST source area and this receptor. None of these wells, (MW-12, MW-22 and MW-23), have ever indicated any 6200B compounds (including benzene and toluene) above laboratory detection limits throughout the 10+ years of site monitoring. Since source area free product has been remediated, and dissolved benzene/toluene have been remediated to < 10X 15 NCAC 2B Standards, it is highly unlikely that this surface water receptor will ever receive groundwater impact as a result from the petroleum release at the former Hot Spot 2002 facility. Groundwater flow velocity was estimated at 7 ft/year by Terry Environmental during CSA activities.
TABLE OF CONTENTS

Section Page 1.0 Site History and Characterization 1.1 Introduction .................................................................... 1 1.2 Scope of Services ........................................................... 2 2.0 Presentation of Current Site Assessment Information / Comparison to Historical Assessment Information 2.1 Historical Soil Assessment Information ........................ 2 2.2 Groundwater Flow Direction and Gradient ................... 3 2.3 Monitor Well Sampling and Analyses ........................... 3 2.4 Regional / Site Geology and Hydrogeology .................. 4 2.5 Plume Development ....................................................... 5 3.0 Monitored Natural Attenuation 3.1 Natural Source Zone Depletion Status ........................... 5 4.0 Conclusions 4.1 General Summary .......................................................... 6 4.2 Recommendations .......................................................... 6 4.3 Limitations ..................................................................... 7 5.0 Statements and Certification 5.1 Statements ...................................................................... 8 5.2 Certification ................................................................... 8

LIST OF FIGURES Figure 1: Project Location Figure 2: Site Layout, UST & Monitor Well Locations Figure 3: Post-Remediation Soil Concentrations Map Figure 4: Shallow Well Potentiometric Surface Map (11/26/22) Figure 5: Benzene Isoconcentration Map Figure 6: Toluene Isoconcentration Map Figure 7: Naphthalene Isoconcentration Map Figure 8: Total 6200B Compounds Concentration Map – 11/26/22 Figure 8H: Historical Total 6200B Compounds Concentration Map – 2/3/22

LIST OF TABLES Table 1: Site History Table 2: Summary of Risk-Based Soil Analytical Data
Table 3: Monitoring Well Information and Groundwater Elevations
Table 4: Summary of Current Groundwater Analytical Results
Table 5: Historical Groundwater Summary

APPENDICES Appendix A: Laboratory Analytical Results
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GROUNDWATER MONITORING REPORT Hot Spot 2002 704 East Main Street, Burnsville, NC 28714

1.0 Site History and Characterization

1.1 Introduction

R.L. Jordan Oil Company of North Carolina, Inc. owned USTs which were operated at
the Hot Spot 2002 facility located at 704 East Main Street in Burnsville, North Carolina.
Figure 1 illustrates the location of this facility on the Burnsville Quadrangle U.S.G.S.
Topo Map. This facility contains one permanent structure which is currently un-
occupied. The site formerly contained (5) registered and (2) unregistered USTs which
were last used at this facility between 1971 (unregistered USTs) and 2019 (registered
USTs). On June 19, 2019, the registered USTs were put into temporary closure. During
closure of the regulated USTs on September 29, 2021, the (2) unregistered USTs were
discovered at the Hot Spot 2002 facility. It is believed that the (2) unregistered USTs
were last used around April, 1971 when the registered USTs were installed (April 25,
1971). Figure 2 illustrates the overall layout of this site and the UST locations. Table 1
summarizes the UST history for the Hot Spot 2002 site.

The original release from the UST system was reported to NCDEQ around May 14, 2010
upon receipt of analytical results from soil samples collected during a site check
conducted on 4/27/2021. Groundwater and free product were observed during soil
remediation activities. The site and adjacent properties are used for commercial
purposes. Municipal water supplies are available to all properties within 1,500’. A
surface stream is located within 500’ of the release source at this facility.

With NCDEQ approval, the (7) USTs and 2,722.76 tons of soil/free product were
excavated from September-October, 2021 at this site and transported for off-site disposal.
Based on recurring free product in replacement well MW-1A subsequent to the 2021
remedial excavation, 117.27 tons of soil/free product were excavated at the site on March
8, 2022 at this site and transported for off-site disposal. Nutrients, straw, and
concentrated bio-degradation liquids were placed back into the remedial excavation prior
to and during backfill of the 3/8/22 remedial excavation to accelerate natural processes in
the UST release source area of this site.
1.2 Scope of Services

Contained herein are the results of a groundwater sampling event as approved by the
NCDEQ. This Groundwater Monitoring Report contains documentation concerning the
following activities which have been conducted at this facility: o Sampling/gauging of (12) existing monitoring wells conducted by Henry Nemargut Engineering on November 26, 2022.
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o Laboratory analyses of groundwater samples conducted by Pace Analytical, Inc. of Huntersville, NC. 2.0 Presentation of Current Site Assessment Information / Comparison to Historical Assessment Information 2.1 Historical Soil Assessment Information
The soils at the project site consist of sand, clay, & silt of varying proportions. Soil
boring logs are contained on well construction records included as Appendix A.

On October 14 & 19, 2021, following remedial excavation, soil samples were collected
from the perimeter of the remedial excavation above the shallow water table to obtain
risk-based analytical data for the site. The soil samples collected at 704 East Main Street
were labeled with sample location, depth, and date collected. The soil samples were
obtained as specified in the collection, preservation, and handling section of the specific
method. Each container was labeled with sample location, analyses to be performed,
time, date, and the sampler's name. They were then placed in a cooler and chilled with
ice to approximately 4oC in preparation for transportation to the analytical laboratory
utilizing EPA approved chain of custody procedures.

Samples collected at the limits of excavation were above current lowest MSCCs for
sample UB2 for (11) compounds/compound groups, with C9-C22 aromatics noted above
Residential MSCCs. These soils are located under the on-site structure and cannot be
remediated without demolition of the building. Sample S1 collected near the retaining
wall on the southern boundary of the remedial excavation contained C9-C22 Aromatic
compounds above lowest MSCCs. No other perimeter soil samples obtained exhibited
contaminants above lowest MSCCs. It should be noted that none of the wall samples
collected were obtained from beneath the high seasonal water table at this site. Figure 3
illustrates the locations of the excavation perimeter soil samples collected at the subject
site following remedial excavation activities. Table 2 summarizes the laboratory results
for the soil samples from 704 East Main Street in Burnsville, NC. A copy of the soil
analytical report and the chain of custody records for the risk-based soil samples
collected at 704 East Main Street is contained in the previously submitted IAA report.
2.2 Ground Water Flow Direction and Gradient

In order to estimate the groundwater flow direction in the vicinity of the petroleum
release, elevations of the monitor well casings were measured using surveying
equipment. During the November 26, 2022 sampling event, static water levels were
obtained from the monitor wells (see Table 3) and the data was used to compute a
potentiometric surface map. Figure 4 illustrates the current potentiometric surface map
as calculated based on the measurements obtained on November 26, 2022.

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Groundwater data and monitoring well information were also used to estimate the
hydraulic gradient at the project site. Using the horizontal distance between the monitor
wells and the static water levels, the groundwater was calculated to flow toward the
southeast with a hydraulic gradient of approximately 0.0175 ft/ft.

2.3 Monitor Well Sampling and Analyses

On November 26, 2022, monitor wells MW-1B, 2R, 4R, 5R, 6, 7, 8, 10R, 11, 20, 21R, &
MW-23 were sampled for analyses utilizing Standard Method 6200B + oxygenates.
Gauging of these wells failed to indicate the presence of free in any of the monitoring
wells formerly containing free product or their replacement monitoring wells. Before
collecting the samples, the monitor wells were purged by removing a minimum of three
well volumes to ensure that the samples were representative of the actual groundwater
conditions. The wells were developed using disposable plastic bailers suspended with
unused nylon string.
All samples were placed in laboratory supplied glassware, labeled with sample location,
analysis to be performed, time, date and sampler's name. The sample jars were then
immediately placed in a cooler, chilled with ice to approximately 4oC in preparation of
transportation to an analytical laboratory utilizing EPA approved chain-of-custody
procedures.

Laboratory analytical results indicate the presence of (3) compounds above the current
listed 2L Standards in the monitor well network. Benzene was detected at a maximum
concentration of 66.1 ug/l in MW-5R, above its 2L standard of 1 ug/l. Naphthalene was
detected at a maximum concentration of 62.7 ug/l in MW-8, above its 2L standard of 6
ug/l. MTBE was detected at a maximum concentration of 71 ug/l, above its 2L Standard
of 20 ug/l. No GCL violations were noted during this monitoring event. Toluene was
detected at a maximum concentration of 15.8 ug/l in MW-2R, below its 2L Standard and
also at a concentration of < 10X 15 NCAC 2B Standard. No compounds were detected at
concentrations > 10X 15 NCAC 2B Standards. Table 4 summarizes the laboratory
analytical results, and Appendix A contains a copy of the laboratory analytical report and
chain of custody records. Figure 5 contains a benzene concentration map, Figure 6
contains a toluene concentration map, Figure 7 contains a Naphthalene concentration
map, and Figure 8 contains a total 6200B concentration map. Figure 8H contains the
baseline historical Total 6200B concentration map as measured on 2/3/2022. 2.4 Regional / Site Geology and Hydrogeology
The site is situated in the Blue Ridge Geologic Province. According to the Geological
Map of North Carolina local geology of the region is comprised of a series of thrust
sheets. According to Terry Environmental, Saprolite was encountered at a depth of 38
feet below surface, but competent bedrock was not encountered to a depth of 50’, which
was the maximum depth explored during subsurface investigations at this site. Soils
encountered at the site during the CSA consisted of clayey silt and silty clay.
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The partial Burnsville Quadrangle U.S.G.S. Topographic Map included as Figure 1
indicates that the release site is located at an approximate elevation of 3282’ amsl.
Surface waters in the vicinity of the release area generally drain south towards Little
Crabtree Creek which borders the southern boundary of the Hot Spot 2002 parcel.

During CSA activities, slug tests performed by Terry Environmental indicated an average
hydraulic conductivity of 0.41 ft/day, with an estimated ground water flow velocity of 7
ft/year at the Hot Spot 2002 release site.

2.5 Plume Development

The monitoring well network at this release site was installed between 2010 and 2012,
with replacement free product area wells installed in February, 2022 following
completion of October, 2021 initial excavation, and again in March, 2022 following the
MW-1A area IAA excavation. In the only prior comprehensive sampling event
conducted at the site following the October, 2021 soil excavation project, 2L violations
for (8) 6200B compounds were noted in monitor wells MW-1A, MW-2R or MW-5R.
The site maximum Total 6200B level was noted in MW-1A on February 3, 2022 was
observed at a concentration of 4,862 ug/l. Both benzene and toluene were present in
MW-1A on that date at a concentration > 10X 15 NCAC 2B; however, no other
monitoring wells at the site were noted to exceed 10X the surface water standards.

Following additional MW-1A/MW-2R area excavation at the site on March 8, 2022,
nutrients, straw, and concentrated bio-degradation liquids were placed back into the
remedial excavation prior to and during backfill to accelerate natural processes in the
UST release source area of this site. The second MW-1 replacement well, MW-1B, was
installed on March 9, 2022 and sampled on March 10, 2022 and was found to contain
significantly reduced benzene and toluene concentrations significantly < 10X 2B
Standards.

During the latest sampling event conducted on November 26, 2022, natural processes
appear to be reducing both the benzene and toluene source area concentrations, with the
maximum toluene concentration at the site noted in MW-2R at 15.8 ug/l, and the
maximum benzene concentration level noted in MW-5R at a level of 66.1 ug/l. Both the
benzene and toluene values are currently significantly < 10X 2B standards.

3.0 Monitored Natural Attenuation 3.1 Natural Source Zone Depletion Status
Historically, 2L violations for 8 compounds were observed at this site in MW-1A/MW-
2R during the only previous comprehensive sampling event conducted on February 3,
2022. Only (3) compounds were noted above 2L Standards during the latest post soil
remediation monitoring event, with no 10X 2B exceedences. Due to the low
groundwater flow velocity (7 ft/yr), the absence of free product, and no compounds >
10X 2B Standards, the risk of impact to Crabtree Creek is considered to be de minimis.
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4.0 Conclusions
4.1 General Summary
A Groundwater Monitoring event at Hot Spot 2002 located at 704 East Main Street in Burnsville, NC has been completed. From a review of all information gathered during this monitoring project, Henry Nemargut Engineering makes the following conclusions:

o On November 26, 2022, monitor wells MW-1B, 2R, 4R, 5R, 6, 7, 8, 10R, 11, 20,
21R, & MW-23 were sampled for analyses utilizing Standard Method 6200B +
oxygenates. Gauging of these wells failed to indicate the presence of free in any
of the monitoring wells formerly containing free product or their replacement
monitoring wells.

o Laboratory analytical results indicate the presence of (3) compounds above the
current listed 2L Standards in the monitor well network. Benzene was detected at
a maximum concentration of 66.1 ug/l in MW-5R, above its 2L standard of 1 ug/l.
Naphthalene was detected at a maximum concentration of 62.7 ug/l in MW-8,
above its 2L standard of 6 ug/l. MTBE was detected at a maximum concentration
of 71 ug/l, above its 2L Standard of 20 ug/l.

o No GCL violations were noted during this monitoring event. Toluene was
detected at a maximum concentration of 15.8 ug/l in MW-2R, below its 2L
Standard and also at a concentration of < 10X 15 NCAC 2B Standard. No
compounds were detected at concentrations > 10X 15 NCAC 2B Standards.

o Only (3) compounds were noted above 2L Standards during the latest post soil
remediation monitoring event, with no 10X 2B exceedences. Due to the low
groundwater flow velocity (7 ft/yr), the absence of free product, and no
compounds > 10X 2B Standards, the risk of impact to Crabtree Creek is
considered to be de minimis.

4.2 Recommendations
Based on information obtained during this sampling event, Henry Nemargut Engineering Services makes the following recommendations for this site:
o The release at this facility should be considered for closure since soil excavation
activities have resulted in free product and 10X 2B groundwater remediation.

A copy of this monitoring report has been forwarded to the following address:
Ms. Maura Clark NCDEQ – UST Section 20909 US Highway 70 Swannanoa, NC 28778 4.3 Limitations
This report has been prepared for the exclusive use of R.L. Jordan Oil Company of North Carolina, Inc. for the specific application to the referenced site located in Yancey County, North Carolina. The assessment was conducted based on the scope of work and level of
Page - 6
effort desired by the client. Our findings have been developed in accordance with generally accepted standards in the practice of Groundwater Monitoring Reports in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied. 5.0 Statements and Certification 5.1 Statements The monitoring report was due n January, 2023. Will this report be submitted after the established due date? No Was any required information from the template missing from this report? No If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? Not Applicable, no CAP has been prepared for this site. Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? No Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? No 5.2 Certification I, Henry Nemargut, a Professional Engineer, do certify that the information contained in this report is correct and accurate to the best of my knowledge.
Henry Nemargut, P.E.
Henry Nemargut Engineering Services
North Carolina License #17669

FIGURES

FIGURE 1: PROJECT LOCATION - USGS TOPO MAP
Project Location

TABLES

TABLE 1: SITE HISTORY
HOT SPOT 2002
704 E. MAIN STREET, BURNSVILLE, NC 28714

Property Ownership:

RLJOC Holdings Co., Inc.
1451 Fernwood Glendale Road
Spartanburg, NC 29307

UST Ownership:

R.L. Jordan Oil Company of North Carolina, Inc
1451 Fernwood Glendale Road
Spartanburg, NC 29307

UST Information:

Tank Inst. Size Closure UST Tank
No Date (Gal) Date Status Contents

T1 4/25/71 8,000 9/29/21 Removed Gasoline
T2 4/25/71 8,000 9/29/21 Removed Gasoline
T3 4/25/71 8,000 9/29/21 Removed Gasoline
T4 4/25/71 6,000 9/29/21 Removed Diesel
T5 4/25/71 4,000 9/29/21 Removed Diesel
T6 Unknown 4,000 10/13/21 Removed Gravel*
T7 Unknown 3,000 10/13/21 Removed Gravel*

* Previously contained gasoline based on UVF analyses

Hot Spot- HIST
Sample Location UB1 UB2 W1 N1 N2 S1 Lowest MSCC Residential MSCC Ind/Comm MSCCDate10/14/2021 10/14/2021 10/14/2021 10/14/2021 10/14/2021 10/14/2021 (note units) (note units) (note units)Sample depth10' 10' 10' 10' 10' 4' Method 8260 (ug/kg)Benzene 21,0301 2 2 BDL 7.2 12,000.0 59,400Methylene Chloride BDL 770 BDL BDL BDL BDL 23 93,800 140,000n-Butylbenzene 1 2,020 7 BDL BDL 1 2,400 782,000 11,600,000sec-Butylbenzene 1 728 4 BDL BDL BDL 2,200 1,560,000 23,300,000Ethylbenzene 416,10022 BDL BDL BDL 8,000 60,300 297,0002-Hexanone BDL BDL BDL 30 BDL BDL 170 11,600,000 78,200Carbon Disulfide 1 BDL 5 BDL BDL 1 3,700 1,560,000 23,000,000n-Hexane 4 6,930 40 BDL 1 BDL NSE NSE NSEIsopropylbenzene 11,9805 BDL BDL BDL 1,300 1,560,000 23,300,000p-Isopropyltoluene BDL BDL 2 BDL BDL BDL NSE NSE NSENaphthalene 117,83045 BDL 2 BDL 200 5500 27,000Acetone 140 BDL 49 214 51 50 24,000 14,000,000 360,000,000Methyl Ethyl Ketone (MEK) 47 BDL BDL 115 9 13 16,000 31,200,000 467,000,000n-Propylbenzene 26,98022 BDL BDL BDL 1,400 1,560,000 23,300,000Toluene 327,00027 2 3 2 5,400 1,250,000 18,600,0001,2,4-Trimethylbenzene 2544,900223 BDL 4 BDL 6,600 156,000 233,000,0001,3,5-Trimethylbenzene 1512,90081 BDL 1 BDL 6,600 156,000 233,000,000MTBE BDL BDL BDL BDL 1 BDL 85 156,000 1,810,000sec-butylbenzene BDL BDL BDL BDL BDL BDL 3,400 626,000 16,350,000Xylenes (total) 2492,500183 8 21 BDL 6,000 3,120,000 46,700,000Method 8270 (ug/kg)FluoreneBDLBDLBDLBDLBDLBDL47,000620,00016,400,000Fluoranthene BDL BDL BDL BDL BDL BDL 290,000 620,000 16,400,000Pyrene BDL BDL BDL BDL BDL BDL 270,000 469,000 12,264,0001-Methylnaphthalene BDL BDL BDL BDL BDL BDL 4 20,000 100,0002-Methylnaphthalene BDL BDL BDL BDL BDL BDL 3,600 63,000 1,635,000Naphthalene BDL BDL BDL BDL BDL BDL 160 313000 8,176,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL6398.35 BDL BDL BDL 68 625 9,340C9 - C12 Volatile Aliphatics 7.66 979 52.6 BDL BDL 20.9 NSE NSE NSEC9-C18 Extractable Aliphatics BDL 93.2 BDL BDL BDL 281 NSE NSE NSEC9-C18 Aliphatics (total) 7.661072.252.6 0 0 301.9 540 1,560 23,300C19-C36 Extractable AliphaticsBDLBDLBDLBDLBDL60.2NSE31,200467,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDL43622.1BDLBDL4.19NSENSENSEC11 - C22 Extractable Aromatics BDL 70.1 BDL BDL BDL 59.9 NSE NSE NSEC9 - C22 Aromatics (total)0506.122.10064.09314697000BDL = below detection limits NR = analyses not requestedNSE = no standard establishedTABLE 2Laboratory Analytical Results - Risk Based Soil SamplesHot Spot 2002, 704 E. Main St, Burnsville, NC 28714
Sample Location S2 SE N3 N4 N5 E1 Lowest MSCC Ind/Comm MSCC Residential MSCCDate10/14/2021 10/14/2021 10/19/2021 10/19/2021 10/19/2021 10/19/2021 (note units) (note units) (note units)Sample depth2' 2' 10' 8' 5' 2' Method 8260 (ug/kg)Benzene BDL BDL BDL BDL 1 BDL 7.2 12,000.0 59,400Methylene Chloride 2 BDL BDL BDL BDL BDL 23 93,800 140,000n-Butylbenzene BDL BDL BDL BDL BDL BDL 2,400 782,000 11,600,000sec-Butylbenzene BDL BDL BDL BDL BDL BDL 2,200 1,560,000 23,300,000Ethylbenzene BDL BDL BDL BDL BDL BDL 8,000 60,300 297,000Isopropylbenzene BDL BDL BDL BDL BDL BDL 1,300 1,560,000 23,300,000p-Isopropyltoluene BDL BDL BDL BDL BDL BDL NSE NSE NSENaphthalene BDL BDL BDL BDL BDL BDL 200 5500 27,000Acetone 37 21 40 81 41 26 24,000 14,000,000 360,000,000Methyl Ethyl Ketone (MEK) 73325316,00031,200,000 467,000,000n-Propylbenzene BDL BDL BDL BDL BDL BDL 1,400 1,560,000 23,300,000Di-isopropyl ether (DIPE BDL 2 BDL BDL BDL BDL 320 2,330,000 NSEToluene BDL 1 BDL BDL BDL BDL 5,400 1,250,000 18,600,0001,2,4-Trimethylbenzene BDL BDL BDL BDL BDL BDL 6,600 156,000 233,000,0001,3,5-Trimethylbenzene BDL BDL BDL BDL BDL BDL 6,600 156,000 233,000,000MTBE BDL 3 BDL BDL BDL BDL 85 156,000 1,810,000sec-butylbenzene BDL BDL BDL BDL BDL BDL 3,400 626,000 16,350,000Xylenes (total) BDL BDL BDL BDL BDL BDL 6,000 3,120,000 46,700,000Method 8270 (ug/kg)FluoreneBDLBDLBDLBDLBDLBDL47,00016,400,000620,000Fluoranthene BDL BDL BDL BDL BDL BDL 290,000 16,400,000 620,000Pyrene BDL BDL BDL BDL BDL BDL 270,000 12,264,000 469,0001-Methylnaphthalene BDL BDL BDL BDL BDL BDL 4 100,000 20,0002-Methylnaphthalene BDL BDL BDL BDL BDL BDL 3,600 1,635,000 63,000Naphthalene BDL BDL BDL BDL BDL BDL 160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL BDL BDL BDL BDL BDL 68 625 9,340C9 - C12 Volatile Aliphatics BDL BDL BDL BDL BDL BDL NSE NSE NSEC9-C18 Extractable Aliphatics 166 BDL BDL BDL 154 BDL NSE NSE NSEC9-C18 Aliphatics (total) 1660001540540 1,560 23,300C19-C36 Extractable Aliphatics29.5BDLBDLBDL51.1BDLNSE31,200467,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDLBDLBDLBDLBDLBDLNSENSENSEC11 - C22 Extractable Aromatics BDL BDL BDL BDL 21 BDL NSE NSE NSEC9 - C22 Aromatics (total)000021.20314697000BDL = below detection limits NR = analyses not requestedNSE = no standard establishedTABLE 2 (Continued)Laboratory Analytical Results - Risk Based Soil SamplesHot Spot 2002, 704 E. Main St, Burnsville, NC 28714
Sample Location E2 Lowest MSCC Ind/Comm MSCC Residential MSCCDate10/19/2021 (note units) (note units) (note units)Sample depth2' Method 8260 (ug/kg)Benzene BDL7.2 12,000.0 59,400Methylene Chloride BDL23 93,800 140,000n-Butylbenzene BDL2,400 782,000 11,600,000sec-Butylbenzene BDL2,200 1,560,000 23,300,000Ethylbenzene BDL8,000 60,300 297,000Isopropylbenzene BDL1,300 1,560,000 23,300,000p-Isopropyltoluene BDLNSE NSE NSENaphthalene BDL200 5500 27,000Acetone 3724,000 14,000,000 360,000,000Methyl Ethyl Ketone (MEK) 516,000 31,200,000 467,000,000n-Propylbenzene BDL1,400 1,560,000 23,300,000Di-isopropyl ether (DIPE BDL320 2,330,000 NSEToluene BDL5,400 1,250,000 18,600,0001,2,4-Trimethylbenzene BDL6,600 156,000 233,000,0001,3,5-Trimethylbenzene BDL6,600 156,000 233,000,000MTBE BDL85 156,000 1,810,000sec-butylbenzene BDL3,400 626,000 16,350,000Xylenes (total) BDL6,000 3,120,000 46,700,000Method 8270 (ug/kg)FluoreneBDL47,00016,400,000620,000Fluoranthene BDL290,000 16,400,000 620,000Pyrene BDL270,000 12,264,000 469,0001-Methylnaphthalene BDL4 100,000 20,0002-Methylnaphthalene BDL3,600 1,635,000 63,000Naphthalene BDL160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL68 625 9,340C9 - C12 Volatile Aliphatics BDLNSE NSE NSEC9-C18 Extractable Aliphatics BDLNSE NSE NSEC9-C18 Aliphatics (total)0540 1,560 23,300C19-C36 Extractable AliphaticsBDLNSE31,200467,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDLNSENSENSEC11 - C22 Extractable Aromatics BDLNSE NSE NSEC9 - C22 Aromatics (total)0314697000BDL = below detection limits NR = analyses not requestedNSE = no standard establishedTABLE 2 (Continued)Laboratory Analytical Results - Risk Based Soil SamplesHot Spot 2002, 704 E. Main St, Burnsville, NC 28714
Well Number Top of Casing Elev Top of Screen Elev Bottom of Screen Elev Depth to FP Depth to Water GH2O Elevation FP ThicknessMW-1B 98.63 87.63 77.63 11.71 86.92MW-2R 99.69 89.69 79.69 12.72 86.97MW-4R 97.23 89.23 79.23 11.09 86.14MW-5R 90.73 86.73 71.73 4.39 86.34MW-6 97.98 88.98 78.98 10.94 87.04MW-7 99.83 89.83 79.83 13.10 86.73MW-8 97.18 89.18 79.18 10.38 86.80MW-10R 89.49 86.99 76.99 4.25 85.24MW-11 90.78 87.78 77.78 4.53 86.25MW-12 99.20 92.20 82.20 NMMW-13 100.21 90.21 80.21 NMMW-14 100.05 91.05 81.05 NMMW-15 99.47 90.47 80.47 NMMW-16 106.22 91.22 81.22 NMMW-17 97.39 89.59 79.59 NMMW-18 95.15 86.75 76.75 NMMW-20 95.95 88.15 78.15 10.09 85.86MW-21R 89.16 86.66 76.66 3.62 85.54MW-23 92.06 86.46 76.46 7.18 84.88NM = Not measuredDensity of Gasoline = 0.77All measurements taken in feet and based on an arbitrary benchmark of 100 ft. established at Groundwater levels measured on 11/26/2022TABLE 3Monitoring Well Information and Groundwater ElevationsHot Spt 2002, 704 East Main Street, Burnsville, NC 28714
Constituent MW-1B MW-2R MW-4R MW-5R 10X 2B GCL 2L Standard

Date 11/26/2022 11/26/2022 11/26/2022 11/26/2022
Standard Method 6200B (ug/L)
Benzene 8 30.8 60.7 66.1 510 5,000 1
Toluene BDL 15.8 1.3 0.5 110 260,000 600
Ethylbenzene 0.71 122 2.5 2.9 NSE 84,500 600
Xylenes (total) 0.63 BDL 0.56 0.78 NSE 85,500 500
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE NSE
Isopropylbenzene 0.55 14.9 5.8 3.8 NSE 25,000 70
Diisopropyl Ether (DIPE) 2.5 BDL 1.2 86.5 NSE 70,000 70
Naphthalene 3.5 44.4 4.3 5.2 NSE 6,000 6
n-propylbenzene 0.8 45.4 0.65 2.4 NSE 30,000 70
n-butylbenzene 0.58 17.7 1 1.5 NSE 6,900 70
sec-butylbenzene BDL BDL 1.3 4.1 NSE 8,800 70
tert-butylbenzene BDL BDL BDL 0.9 NSE 14,750 70
Chloroform BDL BDL BDL BDL NSE 70,000 70
Methyl-tert-butyl-ether (MTBE) 9.4 9.3 3 71 NSE 20,000 20
Tert-Amylmethyl ether (TAME) BDL BDL BDL 14.1 NSE 128,000 128
1,2,4-Trimethylbenzene 1.7 216 BDL 1.5 NSE 24,000 400
1,3,5-Trimethylbenzene BDL 68.4 BDL BDL NSE 25,000 400
TOTAL 6200B 28.37 584.7 82.31 261.28 NSE 15,000 15
Method 625 (ug/L)
Acenaphthene NR NR NR NR NSE 2,120 80
Naphthalene NR NR NR NR NSE 6,000 6
1-Methylnaphthalene NR NR NR NR NSE 1,000 1
2-Methylnaphthalene NR NR NR NR NSE 125,000 30
TOTAL TICs NR NR NR NR NSE NSE NSE
MADEP Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics NR NR NR NR NSE NSE 400
C9-C12 Volatile Aliphatics NR NR NR NR NSE NSE NSE
C9-C18 Extractable Aliphatics NR NR NR NR NSE NSE 700
C9-C18 Aliphatics (total) NR NR NR NR NSE NSE 700
C19-C36 Extractable Aliphatics NR NR NR NR NSE NSE 10,000
MADEP Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics NR NR NR NR NSE NSE NSE
C11-C22 Extractable Aromatics NR NR NR NR NSE NSE NSE
C9-C22 Aromatics (total)NR NR NR NR NSE NSE 200
NR = Analyses Not Requested Bolded values = Exceeds 2L Drinking Water Standards
BDL = Below Detection Limits Red Highlighted values = Exceeds 10X 2B Surface Water Standards
NSE = No Standard Established
TABLE 4
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
Hot Spot 2002
704 East Main St, Burnsville, NC 28714
Constituent MW-6 MW-7 MW-8 MW-10R 10X 2B GCL 2L Standard

Date 11/26/2022 11/26/2022 11/26/2022 11/26/2022
Standard Method 6200B (ug/L)
Benzene BDL BDL BDL BDL 510 5,000 1
Toluene BDL BDL BDL BDL 110 260,000 600
Ethylbenzene BDL BDL 43.6 BDL NSE 84,500 600
Xylenes (total) BDL BDL 44 BDL NSE 85,500 500
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE NSE
Isopropylbenzene BDL BDL 7.9 BDL NSE 25,000 70
Diisopropyl Ether (DIPE) BDL BDL BDL 3.4 NSE 70,000 70
Naphthalene BDL BDL 62.7 BDL NSE 6,000 6
n-propylbenzene BDL BDL 27.1 BDL NSE 30,000 70
n-butylbenzene BDL BDL 31.2 BDL NSE 6,900 70
sec-butylbenzene BDL BDL BDL BDL NSE 8,800 70
tert-butylbenzene BDL BDL BDL BDL NSE 14,750 70
Chloroform BDL BDL 1.1 BDL NSE 70,000 70
Methyl-tert-butyl-ether (MTBE) BDL BDL BDL 7.3 NSE 20,000 20
Tert-Amylmethyl ether (TAME) BDL BDL BDL BDL NSE 128,000 128
1,2,4-Trimethylbenzene BDL BDL 239 BDL NSE 24,000 400
1,3,5-Trimethylbenzene BDL BDL 42.3 BDL NSE 25,000 400
TOTAL 6200B 0 0 498.9 10.7 NSE 15,000 15
Method 625 (ug/L)
Acenaphthene NR NR NR NR NSE 2,120 80
Naphthalene NR NR NR NR NSE 6,000 6
1-Methylnaphthalene NR NR NR NR NSE 1,000 1
2-Methylnaphthalene NR NR NR NR NSE 125,000 30
TOTAL TICs NR NR NR NR NSE NSE NSE
MADEP Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics NR NR NR NR NSE NSE 400
C9-C12 Volatile Aliphatics NR NR NR NR NSE NSE NSE
C9-C18 Extractable Aliphatics NR NR NR NR NSE NSE 700
C9-C18 Aliphatics (total) NR NR NR NR NSE NSE 700
C19-C36 Extractable Aliphatics NR NR NR NR NSE NSE 10,000
MADEP Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics NR NR NR NR NSE NSE NSE
C11-C22 Extractable Aromatics NR NR NR NR NSE NSE NSE
C9-C22 Aromatics (total)NR NR NR NR NSE NSE 200
NR = Analyses Not Requested Bolded values = Exceeds 2L Drinking Water Standards
BDL = Below Detection Limits Red Highlighted values = Exceeds 10X 2B Surface Water Standards
NSE = No Standard Established
TABLE 4 (Continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
Hot Spot 2002
704 East Main St, Burnsville, NC 28714
Constituent MW-11 MW-20 MW-21R MW-23 10X 2B GCL 2L Standard

Date 11/26/2022 11/26/2022 11/26/2022 11/26/2022
Standard Method 6200B (ug/L)
Benzene BDL BDL 30.3 BDL 510 5,000 1
Toluene BDL BDL 0.93 BDL 110 260,000 600
Ethylbenzene BDL BDL 17.5 BDL NSE 84,500 600
Xylenes (total) BDL BDL 5.63 BDL NSE 85,500 500
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE NSE
Isopropylbenzene BDL BDL 4.1 BDL NSE 25,000 70
Diisopropyl Ether (DIPE) BDL BDL 5.6 BDL NSE 70,000 70
Naphthalene BDL BDL 12.4 BDL NSE 6,000 6
n-propylbenzene BDL BDL 3.7 BDL NSE 30,000 70
n-butylbenzene BDL BDL BDL BDL NSE 6,900 70
sec-butylbenzene BDL BDL 4 BDL NSE 8,800 70
tert-butylbenzene BDL BDL 0.81 BDL NSE 14,750 70
Chloroform BDL 0.84 BDL 1.1 NSE 70,000 70
Methyl-tert-butyl-ether (MTBE) BDL BDL 3.2 BDL NSE 20,000 20
Tert-Amylmethyl ether (TAME) BDL BDL BDL BDL NSE 128,000 128
1,2,4-Trimethylbenzene BDL BDL 9.2 BDL NSE 28,500 400
1,3,5-Trimethylbenzene BDL BDL BDL BDL NSE 24,100 400
TOTAL 6200B 0 0.84 97.37 1.1 NSE 15,000 15
Method 625 (ug/L)
Acenaphthene NR NR NR NR NSE 2,120 80
Naphthalene NR NR NR NR NSE 6,000 6
1-Methylnaphthalene NR NR NR NR NSE 1,000 1
2-Methylnaphthalene NR NR NR NR NSE 125,000 30
TOTAL TICs NR NR NR NR NSE NSE NSE
MADEP Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics NR NR NR NR NSE NSE 400
C9-C12 Volatile Aliphatics NR NR NR NR NSE NSE NSE
C9-C18 Extractable Aliphatics NR NR NR NR NSE NSE 700
C9-C18 Aliphatics (total) NR NR NR NR NSE NSE 700
C19-C36 Extractable Aliphatics NR NR NR NR NSE NSE 10,000
MADEP Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics NR NR NR NR NSE NSE NSE
C11-C22 Extractable Aromatics NR NR NR NR NSE NSE NSE
C9-C22 Aromatics (total)NR NR NR NR NSE NSE 200
NR = Analyses Not Requested Bolded values = Exceeds 2L Drinking Water Standards
BDL = Below Detection Limits Red Highlighted values = Exceeds 10X 2B Surface Water Standards
NSE = No Standard Established
TABLE 4 (Continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
Hot Spot 2002
704 East Main St, Burnsville, NC 28714
Constituent MW-1B MW-21R 10X 2B GCL 2L Standard

Date 3/10/2022 3/10/2022
Standard Method 6200B (ug/L)
Benzene 189 14.3 510 5,000 1
Toluene 12.2 0.54 110 260,000 600
Ethylbenzene 38.3 42.5 NSE 84,500 600
Xylenes (total) 107.5 53.1 NSE 85,500 500
p-Isopropyltoluene BDL BDL NSE NSE NSE
Isopropylbenzene 4.4 12.8 NSE 25,000 70
Diisopropyl Ether (DIPE) 13.2 6.8 NSE 70,000 70
Naphthalene 29.5 41.5 NSE 6,000 6
n-propylbenzene 11.6 34.7 NSE 30,000 70
n-butylbenzene 5.5 BDL NSE 6,900 70
sec-butylbenzene BDL BDL NSE 8,500 70
Chloroform 6 BDL NSE 70,000 70
Styrene BDL BDL NSE 70,000 70
Methyl-tert-butyl-ether (MTBE)36.7 3.1 NSE 20,000 20
Tert-Amyl Alcohol (TAA)291 BDL NSE 40,000 40
1,2,4-Trimethylbenzene 66.9 161 NSE 24,000 400
1,3,5-Trimethylbenzene 20.1 57.5 NSE 25,000 400
TOTAL 6200B 831.9 427.84 NSE 15,000 15
Method 625 (ug/L)
Acenaphthene NR NR NSE 2,120 80
Naphthalene NR NR NSE 6,000 6
1-Methylnaphthalene NR NR NSE 1,000 1
2-Methylnaphthalene NR NR NSE 125,000 30
TOTAL TICs NR NR NSE NSE NSE
MADEP Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics NR NR NSE NSE 400
C9-C12 Volatile Aliphatics NR NR NSE NSE NSE
C9-C18 Extractable Aliphatics NR NR NSE NSE 700
C9-C18 Aliphatics (total) NR NR NSE NSE 700
C19-C36 Extractable Aliphatics NR NR NSE NSE 10,000
MADEP Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics NR NR NSE NSE NSE
C11-C22 Extractable Aromatics NR NR NSE NSE NSE
C9-C22 Aromatics (total)NR NR NSE NSE 200
NR = Analyses Not Requested Bolded values = Exceeds 2L Drinking Water Standards
BDL = Below Detection Limits Red Highlighted values = Exceeds 10X 2B Surface Water Standards
NSE = No Standard Established
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
Hot Spot 2002
704 East Main St, Burnsville, NC 28714
Constituent MW-1A MW-2R MW-4R MW-5R 10X 2B GCL 2L Standard

Date 2/3/2022 2/3/2022 2/3/2022 2/3/2022
Standard Method 6200B (ug/L)
Benzene 2430 168 12 31.7 510 5,000 1
Toluene 344 95.6 5.1 1.2 110 260,000 600
Ethylbenzene 260 BDL 110 25.5 NSE 84,500 600
Xylenes (total)729 1550 293.4 7.37 NSE 85,500 500
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE NSE
Isopropylbenzene 39.3 95.4 11.1 10 NSE 25,000 70
Diisopropyl Ether (DIPE)110 BDL BDL 50.1 NSE 70,000 70
Naphthalene 302 413 53.1 32.7 NSE 6,000 6
n-propylbenzene 77.9 303 35.3 20.2 NSE 30,000 70
n-butylbenzene 69.9 BDL BDL 10 NSE 6,900 70
sec-butylbenzene BDL BDL BDL 8.1 NSE 8,500 70
Chloroform 17.5 BDL 5 BDL NSE 70,000 70
Styrene BDL BDL BDL BDL NSE 70,000 70
Methyl-tert-butyl-ether (MTBE) BDL 15.6 BDL 47.3 NSE 20,000 20
Tert-Amylmethyl ether (TAME) BDL BDL BDL 10.6 NSE 128,000 128
1,2,4-Trimethylbenzene 375 1430 223 17.2 NSE 24,000 400
1,3,5-Trimethylbenzene 107 460 60.3 4 NSE 25,000 400
TOTAL 6200B 4861.6 4530.6 808.3 275.97 NSE 15,000 15
Method 625 (ug/L)
Acenaphthene NR NR NR NR NSE 2,120 80
Naphthalene NR NR NR NR NSE 6,000 6
1-Methylnaphthalene NR NR NR NR NSE 1,000 1
2-Methylnaphthalene NR NR NR NR NSE 125,000 30
TOTAL TICs NR NR NR NR NSE NSE NSE
MADEP Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics NR NR NR NR NSE NSE 400
C9-C12 Volatile Aliphatics NR NR NR NR NSE NSE NSE
C9-C18 Extractable Aliphatics NR NR NR NR NSE NSE 700
C9-C18 Aliphatics (total) NR NR NR NR NSE NSE 700
C19-C36 Extractable Aliphatics NR NR NR NR NSE NSE 10,000
MADEP Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics NR NR NR NR NSE NSE NSE
C11-C22 Extractable Aromatics NR NR NR NR NSE NSE NSE
C9-C22 Aromatics (total)NR NR NR NR NSE NSE 200
NR = Analyses Not Requested Bolded values = Exceeds 2L Drinking Water Standards
BDL = Below Detection Limits Red Highlighted values = Exceeds 10X 2B Surface Water Standards
NSE = No Standard Established
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
Hot Spot 2002
704 East Main St, Burnsville, NC 28714
Constituent MW6 MW8 MW10R MW11 10X 2B GCL 2L Standard

Date 2/3/2022 2/3/2022 2/3/2022 2/3/2022
Standard Method 6200B (ug/L)
Benzene 1.1 BDL BDL BDL 510 5,000 1
Toluene BDL BDL BDL BDL 110 260,000 600
Ethylbenzene BDL 60.3 1.9 BDL NSE 84,500 600
Xylenes (total) BDL 70.1 3.29 BDL NSE 85,500 500
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE NSE
Isopropylbenzene BDL 7.6 1.1 BDL NSE 25,000 70
Diisopropyl Ether (DIPE) BDL BDL BDL BDL NSE 70,000 70
Naphthalene BDL 56.4 4.7 BDL NSE 6,000 6
n-propylbenzene BDL 24.1 1.8 BDL NSE 30,000 70
n-butylbenzene BDL BDL 1.8 BDL NSE 6,900 70
sec-butylbenzene BDL BDL BDL BDL NSE 8,500 70
Chloroform 1.8 5.2 2.3 0.79 NSE 70,000 70
Styrene BDL BDL BDL BDL NSE 70,000 70
Methyl-tert-butyl-ether (MTBE) BDL BDL BDL BDL NSE 20,000 20
Methylene Chloride BDL BDL BDL BDL NSE 5,000 5
1,2,4-Trimethylbenzene BDL 203 6 2.8 NSE 24,000 400
1,3,5-Trimethylbenzene BDL 45.8 2 BDL NSE 25,000 400
TOTAL 6200B 2.9 472.5 24.89 3.59 NSE 15,000 15
Method 625 (ug/L)
Acenaphthene NR NR NR NR NSE 2,120 80
Naphthalene NR NR NR NR NSE 6,000 6
1-Methylnaphthalene NR NR NR NR NSE 1,000 1
2-Methylnaphthalene NR NR NR NR NSE 125,000 30
TOTAL TICs NR NR NR NR NSE NSE NSE
MADEP Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics NR NR NR NR NSE NSE 400
C9-C12 Volatile Aliphatics NR NR NR NR NSE NSE NSE
C9-C18 Extractable Aliphatics NR NR NR NR NSE NSE 700
C9-C18 Aliphatics (total) NR NR NR NR NSE NSE 700
C19-C36 Extractable Aliphatics NR NR NR NR NSE NSE 10,000
MADEP Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics NR NR NR NR NSE NSE NSE
C11-C22 Extractable Aromatics NR NR NR NR NSE NSE NSE
C9-C22 Aromatics (total)NR NR NR NR NSE NSE 200
NR = Analyses Not Requested Bolded values = Exceeds 2L Drinking Water Standards
BDL = Below Detection Limits Red Highlighted values = Exceeds 10X 2B Surface Water Standards
NSE = No Standard Established
TABLE 5 (continued)
HISTORICAL GROUNDWATER SUMMARY
Hot Spot 2002
704 East Main St, Burnsville, NC 28714

APPENDIX A

LABORATORY

ANALYTICAL RESULTS

#=CL#
December 03, 2022
LIMS USE: FR - HENRY NEMARGUT
LIMS OBJECT ID: 92638703
92638703
Project:
Pace Project No.:
RE:
Henry Nemargut
Henry Nemargut Engineering
2211 Chestnut Street
Wilmington, NC 28405
HOT SPOT 2002
Dear Henry Nemargut:
Enclosed are the analytical results for sample(s) received by the laboratory on November 28, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 45
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 45
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Lab ID Sample ID Matrix Date Collected Date Received
92638703001 MW1B Water 11/26/22 09:10 11/28/22 11:00
92638703002 MW2R Water 11/26/22 09:30 11/28/22 11:00
92638703003 MW4R Water 11/26/22 09:50 11/28/22 11:00
92638703004 MW5R Water 11/26/22 10:15 11/28/22 11:00
92638703005 MW6 Water 11/26/22 10:30 11/28/22 11:00
92638703006 MW7 Water 11/26/22 10:50 11/28/22 11:00
92638703007 MW8 Water 11/26/22 11:05 11/28/22 11:00
92638703008 MW10R Water 11/26/22 11:25 11/28/22 11:00
92638703009 MW11 Water 11/26/22 11:45 11/28/22 11:00
92638703010 MW20 Water 11/26/22 12:00 11/28/22 11:00
92638703011 MW21R Water 11/26/22 12:20 11/28/22 11:00
92638703012 MW23 Water 11/26/22 12:35 11/28/22 11:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 45
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92638703001 MW1B SM 6200B 69 PASI-CCL
92638703002 MW2R SM 6200B 69 PASI-CCL
92638703003 MW4R SM 6200B 69 PASI-CCL
92638703004 MW5R SM 6200B 69 PASI-CCL
92638703005 MW6 SM 6200B 69 PASI-CCL
92638703006 MW7 SM 6200B 69 PASI-CCL
92638703007 MW8 SM 6200B 69 PASI-CCL
92638703008 MW10R SM 6200B 69 PASI-CCL
92638703009 MW11 SM 6200B 69 PASI-CCL
92638703010 MW20 SM 6200B 69 PASI-CCL
92638703011 MW21R SM 6200B 69 PASI-CCL
92638703012 MW23 SM 6200B 69 PASI-CCL
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 45
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92638703001 MW1B
Benzene 8.0 ug/L 12/01/22 19:260.50SM 6200B
n-Butylbenzene 0.58 ug/L 12/01/22 19:260.50SM 6200B
Diisopropyl ether 2.5 ug/L 12/01/22 19:260.50SM 6200B
Ethylbenzene 0.71 ug/L 12/01/22 19:260.50SM 6200B
Isopropylbenzene (Cumene)0.55 ug/L 12/01/22 19:260.50SM 6200B
Methyl-tert-butyl ether 9.4 ug/L 12/01/22 19:260.50SM 6200B
Naphthalene 3.5 ug/L 12/01/22 19:262.0SM 6200B
n-Propylbenzene 0.80 ug/L 12/01/22 19:260.50SM 6200B
1,2,4-Trimethylbenzene 1.7 ug/L 12/01/22 19:260.50SM 6200B
o-Xylene 0.63 ug/L 12/01/22 19:260.50SM 6200B
92638703002 MW2R
Benzene 30.8 ug/L 12/01/22 20:561.0SM 6200B
n-Butylbenzene 17.7 ug/L 12/01/22 20:561.0SM 6200B
Ethylbenzene 122 ug/L 12/01/22 20:561.0SM 6200B
Isopropylbenzene (Cumene)14.9 ug/L 12/01/22 20:561.0SM 6200B
Methyl-tert-butyl ether 9.3 ug/L 12/01/22 20:561.0SM 6200B
Naphthalene 44.4 ug/L 12/01/22 20:564.0SM 6200B
n-Propylbenzene 45.4 ug/L 12/01/22 20:561.0SM 6200B
Toluene 15.8 ug/L 12/01/22 20:561.0SM 6200B
1,2,4-Trimethylbenzene 216 ug/L 12/01/22 20:561.0SM 6200B
1,3,5-Trimethylbenzene 68.4 ug/L 12/01/22 20:561.0SM 6200B
m&p-Xylene 127 ug/L 12/01/22 20:562.0SM 6200B
o-Xylene 30.5 ug/L 12/01/22 20:561.0SM 6200B
92638703003 MW4R
Benzene 60.7 ug/L 12/01/22 19:440.50SM 6200B
n-Butylbenzene 1.0 ug/L 12/01/22 19:440.50SM 6200B
sec-Butylbenzene 1.3 ug/L 12/01/22 19:440.50SM 6200B
Diisopropyl ether 1.2 ug/L 12/01/22 19:440.50SM 6200B
Ethylbenzene 2.5 ug/L 12/01/22 19:440.50SM 6200B
Isopropylbenzene (Cumene)5.8 ug/L 12/01/22 19:440.50SM 6200B
Methyl-tert-butyl ether 3.0 ug/L 12/01/22 19:440.50SM 6200B
Naphthalene 4.3 ug/L 12/01/22 19:442.0SM 6200B
n-Propylbenzene 0.65 ug/L 12/01/22 19:440.50SM 6200B
Toluene 1.3 ug/L 12/01/22 19:440.50SM 6200B
o-Xylene 0.56 ug/L 12/01/22 19:440.50SM 6200B
92638703004 MW5R
tert-Amylmethyl ether 14.1 ug/L 11/30/22 20:4410.0SM 6200B
Benzene 66.1 ug/L 11/30/22 20:440.50SM 6200B
n-Butylbenzene 1.5 ug/L 11/30/22 20:440.50SM 6200B
sec-Butylbenzene 4.1 ug/L 11/30/22 20:440.50SM 6200B
tert-Butylbenzene 0.90 ug/L 11/30/22 20:440.50SM 6200B
Diisopropyl ether 86.5 ug/L 11/30/22 20:440.50SM 6200B
Ethylbenzene 2.9 ug/L 11/30/22 20:440.50SM 6200B
Isopropylbenzene (Cumene)3.8 ug/L 11/30/22 20:440.50SM 6200B
Methyl-tert-butyl ether 71.0 ug/L 11/30/22 20:440.50SM 6200B
Naphthalene 5.2 ug/L 11/30/22 20:442.0SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 45
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92638703004 MW5R
n-Propylbenzene 2.4 ug/L 11/30/22 20:440.50SM 6200B
Toluene 0.50 ug/L 11/30/22 20:440.50SM 6200B
1,2,4-Trimethylbenzene 1.5 ug/L 11/30/22 20:440.50SM 6200B
o-Xylene 0.78 ug/L 11/30/22 20:440.50SM 6200B
92638703007 MW8
n-Butylbenzene 31.2 ug/L 11/30/22 22:331.0SM 6200B
Chloroform 1.1 ug/L 11/30/22 22:331.0SM 6200B
Ethylbenzene 43.6 ug/L 11/30/22 22:331.0SM 6200B
Isopropylbenzene (Cumene)7.9 ug/L 11/30/22 22:331.0SM 6200B
Naphthalene 62.7 ug/L 11/30/22 22:334.0SM 6200B
n-Propylbenzene 27.1 ug/L 11/30/22 22:331.0SM 6200B
1,2,4-Trimethylbenzene 239 ug/L 11/30/22 22:331.0SM 6200B
1,3,5-Trimethylbenzene 42.3 ug/L 11/30/22 22:331.0SM 6200B
m&p-Xylene 38.9 ug/L 11/30/22 22:332.0SM 6200B
o-Xylene 5.1 ug/L 11/30/22 22:331.0SM 6200B
92638703008 MW10R
Diisopropyl ether 3.4 ug/L 11/30/22 17:430.50SM 6200B
Methyl-tert-butyl ether 7.3 ug/L 11/30/22 17:430.50SM 6200B
92638703010 MW20
Chloroform 0.84 ug/L 11/30/22 15:540.50SM 6200B
92638703011 MW21R
Benzene 30.3 ug/L 11/30/22 20:080.50SM 6200B
sec-Butylbenzene 4.0 ug/L 11/30/22 20:080.50SM 6200B
tert-Butylbenzene 0.81 ug/L 11/30/22 20:080.50SM 6200B
Diisopropyl ether 5.6 ug/L 11/30/22 20:080.50SM 6200B
Ethylbenzene 17.5 ug/L 11/30/22 20:080.50SM 6200B
Isopropylbenzene (Cumene)4.1 ug/L 11/30/22 20:080.50SM 6200B
Methyl-tert-butyl ether 3.2 ug/L 11/30/22 20:080.50SM 6200B
Naphthalene 12.4 ug/L 11/30/22 20:082.0SM 6200B
n-Propylbenzene 3.7 ug/L 11/30/22 20:080.50SM 6200B
Toluene 0.93 ug/L 11/30/22 20:080.50SM 6200B
1,2,4-Trimethylbenzene 9.2 ug/L 11/30/22 20:080.50SM 6200B
m&p-Xylene 4.7 ug/L 11/30/22 20:081.0SM 6200B
o-Xylene 0.93 ug/L 11/30/22 20:080.50SM 6200B
92638703012 MW23
Chloroform 1.1 ug/L 11/30/22 16:120.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW1B Lab ID:92638703001 Collected:11/26/22 09:10 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 12/01/22 19:26 75-85-41001
tert-Amylmethyl ether ND ug/L 12/01/22 19:26 994-05-810.0 1
Benzene 8.0 ug/L 12/01/22 19:26 71-43-20.50 1
Bromobenzene ND ug/L 12/01/22 19:26 108-86-10.50 1
Bromochloromethane ND ug/L 12/01/22 19:26 74-97-50.50 1
Bromodichloromethane ND ug/L 12/01/22 19:26 75-27-40.50 1
Bromoform ND ug/L 12/01/22 19:26 75-25-20.50 1
Bromomethane ND ug/L 12/01/22 19:26 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 12/01/22 19:26 75-65-050.0 1
n-Butylbenzene 0.58 ug/L 12/01/22 19:26 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/01/22 19:26 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/01/22 19:26 98-06-60.50 1
tert-Butyl Formate ND ug/L 12/01/22 19:26 762-75-450.0 1
Carbon tetrachloride ND ug/L 12/01/22 19:26 56-23-50.50 1
Chlorobenzene ND ug/L 12/01/22 19:26 108-90-70.50 1
Chloroethane ND ug/L 12/01/22 19:26 75-00-31.0 1
Chloroform ND ug/L 12/01/22 19:26 67-66-30.50 1
Chloromethane ND ug/L 12/01/22 19:26 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/01/22 19:26 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/01/22 19:26 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/22 19:26 96-12-81.0 1
Dibromochloromethane ND ug/L 12/01/22 19:26 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/22 19:26 106-93-40.50 1
Dibromomethane ND ug/L 12/01/22 19:26 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/01/22 19:26 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/01/22 19:26 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/01/22 19:26 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/01/22 19:26 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/01/22 19:26 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/01/22 19:26 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/01/22 19:26 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/01/22 19:26 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/01/22 19:26 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/01/22 19:26 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/01/22 19:26 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/01/22 19:26 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/01/22 19:26 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/01/22 19:26 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/01/22 19:26 10061-02-60.50 1
Diisopropyl ether 2.5 ug/L 12/01/22 19:26 108-20-30.50 1
Ethanol ND ug/L 12/01/22 19:26 64-17-52001
Ethylbenzene 0.71 ug/L 12/01/22 19:26 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 12/01/22 19:26 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 12/01/22 19:26 87-68-32.0 1
Isopropylbenzene (Cumene)0.55 ug/L 12/01/22 19:26 98-82-80.50 1
Methylene Chloride ND ug/L 12/01/22 19:26 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW1B Lab ID:92638703001 Collected:11/26/22 09:10 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 9.4 ug/L 12/01/22 19:26 1634-04-40.50 1
Naphthalene 3.5 ug/L 12/01/22 19:26 91-20-32.0 1
n-Propylbenzene 0.80 ug/L 12/01/22 19:26 103-65-10.50 1
Styrene ND ug/L 12/01/22 19:26 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/22 19:26 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/22 19:26 79-34-50.50 1
Tetrachloroethene ND ug/L 12/01/22 19:26 127-18-40.50 1
Toluene ND ug/L 12/01/22 19:26 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/01/22 19:26 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/01/22 19:26 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/01/22 19:26 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/01/22 19:26 79-00-50.50 1
Trichloroethene ND ug/L 12/01/22 19:26 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/01/22 19:26 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/01/22 19:26 96-18-40.50 1
1,2,4-Trimethylbenzene 1.7 ug/L 12/01/22 19:26 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/01/22 19:26 108-67-80.50 1
Vinyl chloride ND ug/L 12/01/22 19:26 75-01-41.0 1
m&p-Xylene ND ug/L 12/01/22 19:26 179601-23-11.0 1
o-Xylene 0.63 ug/L 12/01/22 19:26 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)84 %12/01/22 19:26 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %12/01/22 19:26 460-00-470-130 1
Toluene-d8 (S)98 %12/01/22 19:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW2R Lab ID:92638703002 Collected:11/26/22 09:30 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 12/01/22 20:56 75-85-42002
tert-Amylmethyl ether ND ug/L 12/01/22 20:56 994-05-820.0 2
Benzene 30.8 ug/L 12/01/22 20:56 71-43-21.0 2
Bromobenzene ND ug/L 12/01/22 20:56 108-86-11.0 2
Bromochloromethane ND ug/L 12/01/22 20:56 74-97-51.0 2
Bromodichloromethane ND ug/L 12/01/22 20:56 75-27-41.0 2
Bromoform ND ug/L 12/01/22 20:56 75-25-21.0 2
Bromomethane ND ug/L 12/01/22 20:56 74-83-910.0 2
tert-Butyl Alcohol ND ug/L 12/01/22 20:56 75-65-01002
n-Butylbenzene 17.7 ug/L 12/01/22 20:56 104-51-81.0 2
sec-Butylbenzene ND ug/L 12/01/22 20:56 135-98-81.0 2
tert-Butylbenzene ND ug/L 12/01/22 20:56 98-06-61.0 2
tert-Butyl Formate ND ug/L 12/01/22 20:56 762-75-41002
Carbon tetrachloride ND ug/L 12/01/22 20:56 56-23-51.0 2
Chlorobenzene ND ug/L 12/01/22 20:56 108-90-71.0 2
Chloroethane ND ug/L 12/01/22 20:56 75-00-32.0 2
Chloroform ND ug/L 12/01/22 20:56 67-66-31.0 2
Chloromethane ND ug/L 12/01/22 20:56 74-87-32.0 2
2-Chlorotoluene ND ug/L 12/01/22 20:56 95-49-81.0 2
4-Chlorotoluene ND ug/L 12/01/22 20:56 106-43-41.0 2
1,2-Dibromo-3-chloropropane ND ug/L 12/01/22 20:56 96-12-82.0 2
Dibromochloromethane ND ug/L 12/01/22 20:56 124-48-11.0 2
1,2-Dibromoethane (EDB)ND ug/L 12/01/22 20:56 106-93-41.0 2
Dibromomethane ND ug/L 12/01/22 20:56 74-95-31.0 2
1,2-Dichlorobenzene ND ug/L 12/01/22 20:56 95-50-11.0 2
1,3-Dichlorobenzene ND ug/L 12/01/22 20:56 541-73-11.0 2
1,4-Dichlorobenzene ND ug/L 12/01/22 20:56 106-46-71.0 2
Dichlorodifluoromethane ND ug/L 12/01/22 20:56 75-71-81.0 2
1,1-Dichloroethane ND ug/L 12/01/22 20:56 75-34-31.0 2
1,2-Dichloroethane ND ug/L 12/01/22 20:56 107-06-21.0 2
1,1-Dichloroethene ND ug/L 12/01/22 20:56 75-35-41.0 2
cis-1,2-Dichloroethene ND ug/L 12/01/22 20:56 156-59-21.0 2
trans-1,2-Dichloroethene ND ug/L 12/01/22 20:56 156-60-51.0 2
1,2-Dichloropropane ND ug/L 12/01/22 20:56 78-87-51.0 2
1,3-Dichloropropane ND ug/L 12/01/22 20:56 142-28-91.0 2
2,2-Dichloropropane ND ug/L 12/01/22 20:56 594-20-71.0 2
1,1-Dichloropropene ND ug/L 12/01/22 20:56 563-58-61.0 2
cis-1,3-Dichloropropene ND ug/L 12/01/22 20:56 10061-01-51.0 2
trans-1,3-Dichloropropene ND ug/L 12/01/22 20:56 10061-02-61.0 2
Diisopropyl ether ND ug/L 12/01/22 20:56 108-20-31.0 2
Ethanol ND ug/L 12/01/22 20:56 64-17-54002
Ethylbenzene 122 ug/L 12/01/22 20:56 100-41-41.0 2
Ethyl-tert-butyl ether ND ug/L 12/01/22 20:56 637-92-320.0 2
Hexachloro-1,3-butadiene ND ug/L 12/01/22 20:56 87-68-34.0 2
Isopropylbenzene (Cumene)14.9 ug/L 12/01/22 20:56 98-82-81.0 2
Methylene Chloride ND ug/L 12/01/22 20:56 75-09-24.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW2R Lab ID:92638703002 Collected:11/26/22 09:30 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 9.3 ug/L 12/01/22 20:56 1634-04-41.0 2
Naphthalene 44.4 ug/L 12/01/22 20:56 91-20-34.0 2
n-Propylbenzene 45.4 ug/L 12/01/22 20:56 103-65-11.0 2
Styrene ND ug/L 12/01/22 20:56 100-42-51.0 2
1,1,1,2-Tetrachloroethane ND ug/L 12/01/22 20:56 630-20-61.0 2
1,1,2,2-Tetrachloroethane ND ug/L 12/01/22 20:56 79-34-51.0 2
Tetrachloroethene ND ug/L 12/01/22 20:56 127-18-41.0 2
Toluene 15.8 ug/L 12/01/22 20:56 108-88-31.0 2
1,2,3-Trichlorobenzene ND ug/L 12/01/22 20:56 87-61-64.0 2
1,2,4-Trichlorobenzene ND ug/L 12/01/22 20:56 120-82-14.0 2
1,1,1-Trichloroethane ND ug/L 12/01/22 20:56 71-55-61.0 2
1,1,2-Trichloroethane ND ug/L 12/01/22 20:56 79-00-51.0 2
Trichloroethene ND ug/L 12/01/22 20:56 79-01-61.0 2
Trichlorofluoromethane ND ug/L 12/01/22 20:56 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 12/01/22 20:56 96-18-41.0 2
1,2,4-Trimethylbenzene 216 ug/L 12/01/22 20:56 95-63-61.0 2
1,3,5-Trimethylbenzene 68.4 ug/L 12/01/22 20:56 108-67-81.0 2
Vinyl chloride ND ug/L 12/01/22 20:56 75-01-42.0 2
m&p-Xylene 127 ug/L 12/01/22 20:56 179601-23-12.0 2
o-Xylene 30.5 ug/L 12/01/22 20:56 95-47-61.0 2
Surrogates
1,2-Dichloroethane-d4 (S)84 %12/01/22 20:56 17060-07-070-130 2
4-Bromofluorobenzene (S)93 %12/01/22 20:56 460-00-470-130 2
Toluene-d8 (S)97 %12/01/22 20:56 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW4R Lab ID:92638703003 Collected:11/26/22 09:50 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 12/01/22 19:44 75-85-41001
tert-Amylmethyl ether ND ug/L 12/01/22 19:44 994-05-810.0 1
Benzene 60.7 ug/L 12/01/22 19:44 71-43-20.50 1
Bromobenzene ND ug/L 12/01/22 19:44 108-86-10.50 1
Bromochloromethane ND ug/L 12/01/22 19:44 74-97-50.50 1
Bromodichloromethane ND ug/L 12/01/22 19:44 75-27-40.50 1
Bromoform ND ug/L 12/01/22 19:44 75-25-20.50 1
Bromomethane ND ug/L 12/01/22 19:44 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 12/01/22 19:44 75-65-050.0 1
n-Butylbenzene 1.0 ug/L 12/01/22 19:44 104-51-80.50 1
sec-Butylbenzene 1.3 ug/L 12/01/22 19:44 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/01/22 19:44 98-06-60.50 1
tert-Butyl Formate ND ug/L 12/01/22 19:44 762-75-450.0 1
Carbon tetrachloride ND ug/L 12/01/22 19:44 56-23-50.50 1
Chlorobenzene ND ug/L 12/01/22 19:44 108-90-70.50 1
Chloroethane ND ug/L 12/01/22 19:44 75-00-31.0 1
Chloroform ND ug/L 12/01/22 19:44 67-66-30.50 1
Chloromethane ND ug/L 12/01/22 19:44 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/01/22 19:44 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/01/22 19:44 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/22 19:44 96-12-81.0 1
Dibromochloromethane ND ug/L 12/01/22 19:44 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/22 19:44 106-93-40.50 1
Dibromomethane ND ug/L 12/01/22 19:44 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/01/22 19:44 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/01/22 19:44 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/01/22 19:44 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/01/22 19:44 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/01/22 19:44 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/01/22 19:44 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/01/22 19:44 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/01/22 19:44 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/01/22 19:44 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/01/22 19:44 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/01/22 19:44 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/01/22 19:44 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/01/22 19:44 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/01/22 19:44 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/01/22 19:44 10061-02-60.50 1
Diisopropyl ether 1.2 ug/L 12/01/22 19:44 108-20-30.50 1
Ethanol ND ug/L 12/01/22 19:44 64-17-52001
Ethylbenzene 2.5 ug/L 12/01/22 19:44 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 12/01/22 19:44 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 12/01/22 19:44 87-68-32.0 1
Isopropylbenzene (Cumene)5.8 ug/L 12/01/22 19:44 98-82-80.50 1
Methylene Chloride ND ug/L 12/01/22 19:44 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW4R Lab ID:92638703003 Collected:11/26/22 09:50 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 3.0 ug/L 12/01/22 19:44 1634-04-40.50 1
Naphthalene 4.3 ug/L 12/01/22 19:44 91-20-32.0 1
n-Propylbenzene 0.65 ug/L 12/01/22 19:44 103-65-10.50 1
Styrene ND ug/L 12/01/22 19:44 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/22 19:44 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/22 19:44 79-34-50.50 1
Tetrachloroethene ND ug/L 12/01/22 19:44 127-18-40.50 1
Toluene 1.3 ug/L 12/01/22 19:44 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/01/22 19:44 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/01/22 19:44 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/01/22 19:44 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/01/22 19:44 79-00-50.50 1
Trichloroethene ND ug/L 12/01/22 19:44 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/01/22 19:44 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/01/22 19:44 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/01/22 19:44 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/01/22 19:44 108-67-80.50 1
Vinyl chloride ND ug/L 12/01/22 19:44 75-01-41.0 1
m&p-Xylene ND ug/L 12/01/22 19:44 179601-23-11.0 1
o-Xylene 0.56 ug/L 12/01/22 19:44 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)84 %12/01/22 19:44 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %12/01/22 19:44 460-00-470-130 1
Toluene-d8 (S)98 %12/01/22 19:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW5R Lab ID:92638703004 Collected:11/26/22 10:15 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/30/22 20:44 75-85-41001
tert-Amylmethyl ether 14.1 ug/L 11/30/22 20:44 994-05-810.0 1
Benzene 66.1 ug/L 11/30/22 20:44 71-43-20.50 1
Bromobenzene ND ug/L 11/30/22 20:44 108-86-10.50 1
Bromochloromethane ND ug/L 11/30/22 20:44 74-97-50.50 1
Bromodichloromethane ND ug/L 11/30/22 20:44 75-27-40.50 1
Bromoform ND ug/L 11/30/22 20:44 75-25-20.50 1
Bromomethane ND ug/L 11/30/22 20:44 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/30/22 20:44 75-65-050.0 1
n-Butylbenzene 1.5 ug/L 11/30/22 20:44 104-51-80.50 1
sec-Butylbenzene 4.1 ug/L 11/30/22 20:44 135-98-80.50 1
tert-Butylbenzene 0.90 ug/L 11/30/22 20:44 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/30/22 20:44 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/30/22 20:44 56-23-50.50 1
Chlorobenzene ND ug/L 11/30/22 20:44 108-90-70.50 1
Chloroethane ND ug/L 11/30/22 20:44 75-00-31.0 1
Chloroform ND ug/L 11/30/22 20:44 67-66-30.50 1
Chloromethane ND ug/L 11/30/22 20:44 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/30/22 20:44 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/30/22 20:44 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/30/22 20:44 96-12-81.0 1
Dibromochloromethane ND ug/L 11/30/22 20:44 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/30/22 20:44 106-93-40.50 1
Dibromomethane ND ug/L 11/30/22 20:44 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/30/22 20:44 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/30/22 20:44 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/30/22 20:44 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/30/22 20:44 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/30/22 20:44 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/30/22 20:44 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/30/22 20:44 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/30/22 20:44 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/30/22 20:44 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/30/22 20:44 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/30/22 20:44 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/30/22 20:44 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/30/22 20:44 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/30/22 20:44 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/30/22 20:44 10061-02-60.50 1
Diisopropyl ether 86.5 ug/L 11/30/22 20:44 108-20-30.50 1
Ethanol ND ug/L 11/30/22 20:44 64-17-52001
Ethylbenzene 2.9 ug/L 11/30/22 20:44 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/30/22 20:44 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/30/22 20:44 87-68-32.0 1
Isopropylbenzene (Cumene)3.8 ug/L 11/30/22 20:44 98-82-80.50 1
Methylene Chloride ND ug/L 11/30/22 20:44 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW5R Lab ID:92638703004 Collected:11/26/22 10:15 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 71.0 ug/L 11/30/22 20:44 1634-04-40.50 1
Naphthalene 5.2 ug/L 11/30/22 20:44 91-20-32.0 1
n-Propylbenzene 2.4 ug/L 11/30/22 20:44 103-65-10.50 1
Styrene ND ug/L 11/30/22 20:44 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/30/22 20:44 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/30/22 20:44 79-34-50.50 1
Tetrachloroethene ND ug/L 11/30/22 20:44 127-18-40.50 1
Toluene 0.50 ug/L 11/30/22 20:44 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/30/22 20:44 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/30/22 20:44 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/30/22 20:44 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/30/22 20:44 79-00-50.50 1
Trichloroethene ND ug/L 11/30/22 20:44 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/30/22 20:44 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/30/22 20:44 96-18-40.50 1
1,2,4-Trimethylbenzene 1.5 ug/L 11/30/22 20:44 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/30/22 20:44 108-67-80.50 1
Vinyl chloride ND ug/L 11/30/22 20:44 75-01-41.0 1
m&p-Xylene ND ug/L 11/30/22 20:44 179601-23-11.0 1
o-Xylene 0.78 ug/L 11/30/22 20:44 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)88 %11/30/22 20:44 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %11/30/22 20:44 460-00-470-130 1
Toluene-d8 (S)96 %11/30/22 20:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW6 Lab ID:92638703005 Collected:11/26/22 10:30 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/30/22 15:36 75-85-41001
tert-Amylmethyl ether ND ug/L 11/30/22 15:36 994-05-810.0 1
Benzene ND ug/L 11/30/22 15:36 71-43-20.50 1
Bromobenzene ND ug/L 11/30/22 15:36 108-86-10.50 1
Bromochloromethane ND ug/L 11/30/22 15:36 74-97-50.50 1
Bromodichloromethane ND ug/L 11/30/22 15:36 75-27-40.50 1
Bromoform ND ug/L 11/30/22 15:36 75-25-20.50 1
Bromomethane ND ug/L 11/30/22 15:36 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/30/22 15:36 75-65-0 M150.0 1
n-Butylbenzene ND ug/L 11/30/22 15:36 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/30/22 15:36 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/30/22 15:36 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/30/22 15:36 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/30/22 15:36 56-23-50.50 1
Chlorobenzene ND ug/L 11/30/22 15:36 108-90-70.50 1
Chloroethane ND ug/L 11/30/22 15:36 75-00-3 M11.0 1
Chloroform ND ug/L 11/30/22 15:36 67-66-30.50 1
Chloromethane ND ug/L 11/30/22 15:36 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/30/22 15:36 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/30/22 15:36 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/30/22 15:36 96-12-81.0 1
Dibromochloromethane ND ug/L 11/30/22 15:36 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/30/22 15:36 106-93-40.50 1
Dibromomethane ND ug/L 11/30/22 15:36 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/30/22 15:36 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/30/22 15:36 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/30/22 15:36 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/30/22 15:36 75-71-8 M10.50 1
1,1-Dichloroethane ND ug/L 11/30/22 15:36 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/30/22 15:36 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/30/22 15:36 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/30/22 15:36 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/30/22 15:36 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/30/22 15:36 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/30/22 15:36 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/30/22 15:36 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/30/22 15:36 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/30/22 15:36 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/30/22 15:36 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/30/22 15:36 108-20-30.50 1
Ethanol ND ug/L 11/30/22 15:36 64-17-52001
Ethylbenzene ND ug/L 11/30/22 15:36 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/30/22 15:36 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/30/22 15:36 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/30/22 15:36 98-82-80.50 1
Methylene Chloride ND ug/L 11/30/22 15:36 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW6 Lab ID:92638703005 Collected:11/26/22 10:30 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 11/30/22 15:36 1634-04-40.50 1
Naphthalene ND ug/L 11/30/22 15:36 91-20-3 M12.0 1
n-Propylbenzene ND ug/L 11/30/22 15:36 103-65-10.50 1
Styrene ND ug/L 11/30/22 15:36 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/30/22 15:36 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/30/22 15:36 79-34-50.50 1
Tetrachloroethene ND ug/L 11/30/22 15:36 127-18-40.50 1
Toluene ND ug/L 11/30/22 15:36 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/30/22 15:36 87-61-6 M12.0 1
1,2,4-Trichlorobenzene ND ug/L 11/30/22 15:36 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/30/22 15:36 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/30/22 15:36 79-00-50.50 1
Trichloroethene ND ug/L 11/30/22 15:36 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/30/22 15:36 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/30/22 15:36 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/30/22 15:36 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/30/22 15:36 108-67-80.50 1
Vinyl chloride ND ug/L 11/30/22 15:36 75-01-41.0 1
m&p-Xylene ND ug/L 11/30/22 15:36 179601-23-11.0 1
o-Xylene ND ug/L 11/30/22 15:36 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)87 %11/30/22 15:36 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %11/30/22 15:36 460-00-470-130 1
Toluene-d8 (S)99 %11/30/22 15:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW7 Lab ID:92638703006 Collected:11/26/22 10:50 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 12/01/22 20:02 75-85-41001
tert-Amylmethyl ether ND ug/L 12/01/22 20:02 994-05-810.0 1
Benzene ND ug/L 12/01/22 20:02 71-43-20.50 1
Bromobenzene ND ug/L 12/01/22 20:02 108-86-10.50 1
Bromochloromethane ND ug/L 12/01/22 20:02 74-97-50.50 1
Bromodichloromethane ND ug/L 12/01/22 20:02 75-27-40.50 1
Bromoform ND ug/L 12/01/22 20:02 75-25-20.50 1
Bromomethane ND ug/L 12/01/22 20:02 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 12/01/22 20:02 75-65-050.0 1
n-Butylbenzene ND ug/L 12/01/22 20:02 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/01/22 20:02 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/01/22 20:02 98-06-60.50 1
tert-Butyl Formate ND ug/L 12/01/22 20:02 762-75-450.0 1
Carbon tetrachloride ND ug/L 12/01/22 20:02 56-23-50.50 1
Chlorobenzene ND ug/L 12/01/22 20:02 108-90-70.50 1
Chloroethane ND ug/L 12/01/22 20:02 75-00-31.0 1
Chloroform ND ug/L 12/01/22 20:02 67-66-30.50 1
Chloromethane ND ug/L 12/01/22 20:02 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/01/22 20:02 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/01/22 20:02 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/22 20:02 96-12-81.0 1
Dibromochloromethane ND ug/L 12/01/22 20:02 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/22 20:02 106-93-40.50 1
Dibromomethane ND ug/L 12/01/22 20:02 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/01/22 20:02 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/01/22 20:02 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/01/22 20:02 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/01/22 20:02 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/01/22 20:02 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/01/22 20:02 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/01/22 20:02 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/01/22 20:02 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/01/22 20:02 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/01/22 20:02 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/01/22 20:02 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/01/22 20:02 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/01/22 20:02 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/01/22 20:02 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/01/22 20:02 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/01/22 20:02 108-20-30.50 1
Ethanol ND ug/L 12/01/22 20:02 64-17-52001
Ethylbenzene ND ug/L 12/01/22 20:02 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 12/01/22 20:02 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 12/01/22 20:02 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/01/22 20:02 98-82-80.50 1
Methylene Chloride ND ug/L 12/01/22 20:02 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW7 Lab ID:92638703006 Collected:11/26/22 10:50 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 12/01/22 20:02 1634-04-40.50 1
Naphthalene ND ug/L 12/01/22 20:02 91-20-32.0 1
n-Propylbenzene ND ug/L 12/01/22 20:02 103-65-10.50 1
Styrene ND ug/L 12/01/22 20:02 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/22 20:02 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/22 20:02 79-34-50.50 1
Tetrachloroethene ND ug/L 12/01/22 20:02 127-18-40.50 1
Toluene ND ug/L 12/01/22 20:02 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/01/22 20:02 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/01/22 20:02 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/01/22 20:02 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/01/22 20:02 79-00-50.50 1
Trichloroethene ND ug/L 12/01/22 20:02 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/01/22 20:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/01/22 20:02 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/01/22 20:02 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/01/22 20:02 108-67-80.50 1
Vinyl chloride ND ug/L 12/01/22 20:02 75-01-41.0 1
m&p-Xylene ND ug/L 12/01/22 20:02 179601-23-11.0 1
o-Xylene ND ug/L 12/01/22 20:02 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)83 %12/01/22 20:02 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %12/01/22 20:02 460-00-470-130 1
Toluene-d8 (S)98 %12/01/22 20:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW8 Lab ID:92638703007 Collected:11/26/22 11:05 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/30/22 22:33 75-85-42002
tert-Amylmethyl ether ND ug/L 11/30/22 22:33 994-05-820.0 2
Benzene ND ug/L 11/30/22 22:33 71-43-21.0 2
Bromobenzene ND ug/L 11/30/22 22:33 108-86-11.0 2
Bromochloromethane ND ug/L 11/30/22 22:33 74-97-51.0 2
Bromodichloromethane ND ug/L 11/30/22 22:33 75-27-41.0 2
Bromoform ND ug/L 11/30/22 22:33 75-25-21.0 2
Bromomethane ND ug/L 11/30/22 22:33 74-83-910.0 2
tert-Butyl Alcohol ND ug/L 11/30/22 22:33 75-65-01002
n-Butylbenzene 31.2 ug/L 11/30/22 22:33 104-51-81.0 2
sec-Butylbenzene ND ug/L 11/30/22 22:33 135-98-81.0 2
tert-Butylbenzene ND ug/L 11/30/22 22:33 98-06-61.0 2
tert-Butyl Formate ND ug/L 11/30/22 22:33 762-75-41002
Carbon tetrachloride ND ug/L 11/30/22 22:33 56-23-51.0 2
Chlorobenzene ND ug/L 11/30/22 22:33 108-90-71.0 2
Chloroethane ND ug/L 11/30/22 22:33 75-00-32.0 2
Chloroform 1.1 ug/L 11/30/22 22:33 67-66-31.0 2
Chloromethane ND ug/L 11/30/22 22:33 74-87-32.0 2
2-Chlorotoluene ND ug/L 11/30/22 22:33 95-49-81.0 2
4-Chlorotoluene ND ug/L 11/30/22 22:33 106-43-41.0 2
1,2-Dibromo-3-chloropropane ND ug/L 11/30/22 22:33 96-12-82.0 2
Dibromochloromethane ND ug/L 11/30/22 22:33 124-48-11.0 2
1,2-Dibromoethane (EDB)ND ug/L 11/30/22 22:33 106-93-41.0 2
Dibromomethane ND ug/L 11/30/22 22:33 74-95-31.0 2
1,2-Dichlorobenzene ND ug/L 11/30/22 22:33 95-50-11.0 2
1,3-Dichlorobenzene ND ug/L 11/30/22 22:33 541-73-11.0 2
1,4-Dichlorobenzene ND ug/L 11/30/22 22:33 106-46-71.0 2
Dichlorodifluoromethane ND ug/L 11/30/22 22:33 75-71-81.0 2
1,1-Dichloroethane ND ug/L 11/30/22 22:33 75-34-31.0 2
1,2-Dichloroethane ND ug/L 11/30/22 22:33 107-06-21.0 2
1,1-Dichloroethene ND ug/L 11/30/22 22:33 75-35-41.0 2
cis-1,2-Dichloroethene ND ug/L 11/30/22 22:33 156-59-21.0 2
trans-1,2-Dichloroethene ND ug/L 11/30/22 22:33 156-60-51.0 2
1,2-Dichloropropane ND ug/L 11/30/22 22:33 78-87-51.0 2
1,3-Dichloropropane ND ug/L 11/30/22 22:33 142-28-91.0 2
2,2-Dichloropropane ND ug/L 11/30/22 22:33 594-20-71.0 2
1,1-Dichloropropene ND ug/L 11/30/22 22:33 563-58-61.0 2
cis-1,3-Dichloropropene ND ug/L 11/30/22 22:33 10061-01-51.0 2
trans-1,3-Dichloropropene ND ug/L 11/30/22 22:33 10061-02-61.0 2
Diisopropyl ether ND ug/L 11/30/22 22:33 108-20-31.0 2
Ethanol ND ug/L 11/30/22 22:33 64-17-54002
Ethylbenzene 43.6 ug/L 11/30/22 22:33 100-41-41.0 2
Ethyl-tert-butyl ether ND ug/L 11/30/22 22:33 637-92-320.0 2
Hexachloro-1,3-butadiene ND ug/L 11/30/22 22:33 87-68-34.0 2
Isopropylbenzene (Cumene)7.9 ug/L 11/30/22 22:33 98-82-81.0 2
Methylene Chloride ND ug/L 11/30/22 22:33 75-09-24.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW8 Lab ID:92638703007 Collected:11/26/22 11:05 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 11/30/22 22:33 1634-04-41.0 2
Naphthalene 62.7 ug/L 11/30/22 22:33 91-20-34.0 2
n-Propylbenzene 27.1 ug/L 11/30/22 22:33 103-65-11.0 2
Styrene ND ug/L 11/30/22 22:33 100-42-51.0 2
1,1,1,2-Tetrachloroethane ND ug/L 11/30/22 22:33 630-20-61.0 2
1,1,2,2-Tetrachloroethane ND ug/L 11/30/22 22:33 79-34-51.0 2
Tetrachloroethene ND ug/L 11/30/22 22:33 127-18-41.0 2
Toluene ND ug/L 11/30/22 22:33 108-88-31.0 2
1,2,3-Trichlorobenzene ND ug/L 11/30/22 22:33 87-61-64.0 2
1,2,4-Trichlorobenzene ND ug/L 11/30/22 22:33 120-82-14.0 2
1,1,1-Trichloroethane ND ug/L 11/30/22 22:33 71-55-61.0 2
1,1,2-Trichloroethane ND ug/L 11/30/22 22:33 79-00-51.0 2
Trichloroethene ND ug/L 11/30/22 22:33 79-01-61.0 2
Trichlorofluoromethane ND ug/L 11/30/22 22:33 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 11/30/22 22:33 96-18-41.0 2
1,2,4-Trimethylbenzene 239 ug/L 11/30/22 22:33 95-63-61.0 2
1,3,5-Trimethylbenzene 42.3 ug/L 11/30/22 22:33 108-67-81.0 2
Vinyl chloride ND ug/L 11/30/22 22:33 75-01-42.0 2
m&p-Xylene 38.9 ug/L 11/30/22 22:33 179601-23-12.0 2
o-Xylene 5.1 ug/L 11/30/22 22:33 95-47-61.0 2
Surrogates
1,2-Dichloroethane-d4 (S)87 %11/30/22 22:33 17060-07-070-130 2
4-Bromofluorobenzene (S)95 %11/30/22 22:33 460-00-470-130 2
Toluene-d8 (S)97 %11/30/22 22:33 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW10R Lab ID:92638703008 Collected:11/26/22 11:25 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/30/22 17:43 75-85-41001
tert-Amylmethyl ether ND ug/L 11/30/22 17:43 994-05-810.0 1
Benzene ND ug/L 11/30/22 17:43 71-43-20.50 1
Bromobenzene ND ug/L 11/30/22 17:43 108-86-10.50 1
Bromochloromethane ND ug/L 11/30/22 17:43 74-97-50.50 1
Bromodichloromethane ND ug/L 11/30/22 17:43 75-27-40.50 1
Bromoform ND ug/L 11/30/22 17:43 75-25-20.50 1
Bromomethane ND ug/L 11/30/22 17:43 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/30/22 17:43 75-65-050.0 1
n-Butylbenzene ND ug/L 11/30/22 17:43 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/30/22 17:43 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/30/22 17:43 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/30/22 17:43 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/30/22 17:43 56-23-50.50 1
Chlorobenzene ND ug/L 11/30/22 17:43 108-90-70.50 1
Chloroethane ND ug/L 11/30/22 17:43 75-00-31.0 1
Chloroform ND ug/L 11/30/22 17:43 67-66-30.50 1
Chloromethane ND ug/L 11/30/22 17:43 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/30/22 17:43 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/30/22 17:43 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/30/22 17:43 96-12-81.0 1
Dibromochloromethane ND ug/L 11/30/22 17:43 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/30/22 17:43 106-93-40.50 1
Dibromomethane ND ug/L 11/30/22 17:43 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/30/22 17:43 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/30/22 17:43 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/30/22 17:43 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/30/22 17:43 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/30/22 17:43 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/30/22 17:43 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/30/22 17:43 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/30/22 17:43 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/30/22 17:43 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/30/22 17:43 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/30/22 17:43 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/30/22 17:43 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/30/22 17:43 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/30/22 17:43 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/30/22 17:43 10061-02-60.50 1
Diisopropyl ether 3.4 ug/L 11/30/22 17:43 108-20-30.50 1
Ethanol ND ug/L 11/30/22 17:43 64-17-52001
Ethylbenzene ND ug/L 11/30/22 17:43 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/30/22 17:43 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/30/22 17:43 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/30/22 17:43 98-82-80.50 1
Methylene Chloride ND ug/L 11/30/22 17:43 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW10R Lab ID:92638703008 Collected:11/26/22 11:25 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 7.3 ug/L 11/30/22 17:43 1634-04-40.50 1
Naphthalene ND ug/L 11/30/22 17:43 91-20-32.0 1
n-Propylbenzene ND ug/L 11/30/22 17:43 103-65-10.50 1
Styrene ND ug/L 11/30/22 17:43 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/30/22 17:43 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/30/22 17:43 79-34-50.50 1
Tetrachloroethene ND ug/L 11/30/22 17:43 127-18-40.50 1
Toluene ND ug/L 11/30/22 17:43 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/30/22 17:43 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/30/22 17:43 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/30/22 17:43 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/30/22 17:43 79-00-50.50 1
Trichloroethene ND ug/L 11/30/22 17:43 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/30/22 17:43 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/30/22 17:43 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/30/22 17:43 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/30/22 17:43 108-67-80.50 1
Vinyl chloride ND ug/L 11/30/22 17:43 75-01-41.0 1
m&p-Xylene ND ug/L 11/30/22 17:43 179601-23-11.0 1
o-Xylene ND ug/L 11/30/22 17:43 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)89 %11/30/22 17:43 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %11/30/22 17:43 460-00-470-130 1
Toluene-d8 (S)99 %11/30/22 17:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW11 Lab ID:92638703009 Collected:11/26/22 11:45 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/30/22 17:24 75-85-41001
tert-Amylmethyl ether ND ug/L 11/30/22 17:24 994-05-810.0 1
Benzene ND ug/L 11/30/22 17:24 71-43-20.50 1
Bromobenzene ND ug/L 11/30/22 17:24 108-86-10.50 1
Bromochloromethane ND ug/L 11/30/22 17:24 74-97-50.50 1
Bromodichloromethane ND ug/L 11/30/22 17:24 75-27-40.50 1
Bromoform ND ug/L 11/30/22 17:24 75-25-20.50 1
Bromomethane ND ug/L 11/30/22 17:24 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/30/22 17:24 75-65-050.0 1
n-Butylbenzene ND ug/L 11/30/22 17:24 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/30/22 17:24 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/30/22 17:24 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/30/22 17:24 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/30/22 17:24 56-23-50.50 1
Chlorobenzene ND ug/L 11/30/22 17:24 108-90-70.50 1
Chloroethane ND ug/L 11/30/22 17:24 75-00-31.0 1
Chloroform ND ug/L 11/30/22 17:24 67-66-30.50 1
Chloromethane ND ug/L 11/30/22 17:24 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/30/22 17:24 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/30/22 17:24 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/30/22 17:24 96-12-81.0 1
Dibromochloromethane ND ug/L 11/30/22 17:24 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/30/22 17:24 106-93-40.50 1
Dibromomethane ND ug/L 11/30/22 17:24 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/30/22 17:24 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/30/22 17:24 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/30/22 17:24 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/30/22 17:24 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/30/22 17:24 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/30/22 17:24 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/30/22 17:24 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/30/22 17:24 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/30/22 17:24 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/30/22 17:24 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/30/22 17:24 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/30/22 17:24 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/30/22 17:24 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/30/22 17:24 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/30/22 17:24 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/30/22 17:24 108-20-30.50 1
Ethanol ND ug/L 11/30/22 17:24 64-17-52001
Ethylbenzene ND ug/L 11/30/22 17:24 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/30/22 17:24 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/30/22 17:24 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/30/22 17:24 98-82-80.50 1
Methylene Chloride ND ug/L 11/30/22 17:24 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW11 Lab ID:92638703009 Collected:11/26/22 11:45 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 11/30/22 17:24 1634-04-40.50 1
Naphthalene ND ug/L 11/30/22 17:24 91-20-32.0 1
n-Propylbenzene ND ug/L 11/30/22 17:24 103-65-10.50 1
Styrene ND ug/L 11/30/22 17:24 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/30/22 17:24 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/30/22 17:24 79-34-50.50 1
Tetrachloroethene ND ug/L 11/30/22 17:24 127-18-40.50 1
Toluene ND ug/L 11/30/22 17:24 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/30/22 17:24 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/30/22 17:24 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/30/22 17:24 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/30/22 17:24 79-00-50.50 1
Trichloroethene ND ug/L 11/30/22 17:24 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/30/22 17:24 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/30/22 17:24 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/30/22 17:24 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/30/22 17:24 108-67-80.50 1
Vinyl chloride ND ug/L 11/30/22 17:24 75-01-41.0 1
m&p-Xylene ND ug/L 11/30/22 17:24 179601-23-11.0 1
o-Xylene ND ug/L 11/30/22 17:24 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)87 %11/30/22 17:24 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %11/30/22 17:24 460-00-470-130 1
Toluene-d8 (S)99 %11/30/22 17:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW20 Lab ID:92638703010 Collected:11/26/22 12:00 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/30/22 15:54 75-85-41001
tert-Amylmethyl ether ND ug/L 11/30/22 15:54 994-05-810.0 1
Benzene ND ug/L 11/30/22 15:54 71-43-20.50 1
Bromobenzene ND ug/L 11/30/22 15:54 108-86-10.50 1
Bromochloromethane ND ug/L 11/30/22 15:54 74-97-50.50 1
Bromodichloromethane ND ug/L 11/30/22 15:54 75-27-40.50 1
Bromoform ND ug/L 11/30/22 15:54 75-25-20.50 1
Bromomethane ND ug/L 11/30/22 15:54 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/30/22 15:54 75-65-050.0 1
n-Butylbenzene ND ug/L 11/30/22 15:54 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/30/22 15:54 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/30/22 15:54 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/30/22 15:54 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/30/22 15:54 56-23-50.50 1
Chlorobenzene ND ug/L 11/30/22 15:54 108-90-70.50 1
Chloroethane ND ug/L 11/30/22 15:54 75-00-31.0 1
Chloroform 0.84 ug/L 11/30/22 15:54 67-66-30.50 1
Chloromethane ND ug/L 11/30/22 15:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/30/22 15:54 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/30/22 15:54 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/30/22 15:54 96-12-81.0 1
Dibromochloromethane ND ug/L 11/30/22 15:54 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/30/22 15:54 106-93-40.50 1
Dibromomethane ND ug/L 11/30/22 15:54 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/30/22 15:54 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/30/22 15:54 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/30/22 15:54 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/30/22 15:54 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/30/22 15:54 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/30/22 15:54 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/30/22 15:54 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/30/22 15:54 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/30/22 15:54 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/30/22 15:54 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/30/22 15:54 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/30/22 15:54 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/30/22 15:54 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/30/22 15:54 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/30/22 15:54 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/30/22 15:54 108-20-30.50 1
Ethanol ND ug/L 11/30/22 15:54 64-17-52001
Ethylbenzene ND ug/L 11/30/22 15:54 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/30/22 15:54 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/30/22 15:54 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/30/22 15:54 98-82-80.50 1
Methylene Chloride ND ug/L 11/30/22 15:54 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW20 Lab ID:92638703010 Collected:11/26/22 12:00 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 11/30/22 15:54 1634-04-40.50 1
Naphthalene ND ug/L 11/30/22 15:54 91-20-32.0 1
n-Propylbenzene ND ug/L 11/30/22 15:54 103-65-10.50 1
Styrene ND ug/L 11/30/22 15:54 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/30/22 15:54 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/30/22 15:54 79-34-50.50 1
Tetrachloroethene ND ug/L 11/30/22 15:54 127-18-40.50 1
Toluene ND ug/L 11/30/22 15:54 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/30/22 15:54 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/30/22 15:54 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/30/22 15:54 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/30/22 15:54 79-00-50.50 1
Trichloroethene ND ug/L 11/30/22 15:54 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/30/22 15:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/30/22 15:54 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/30/22 15:54 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/30/22 15:54 108-67-80.50 1
Vinyl chloride ND ug/L 11/30/22 15:54 75-01-41.0 1
m&p-Xylene ND ug/L 11/30/22 15:54 179601-23-11.0 1
o-Xylene ND ug/L 11/30/22 15:54 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)85 %11/30/22 15:54 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %11/30/22 15:54 460-00-470-130 1
Toluene-d8 (S)100 %11/30/22 15:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW21R Lab ID:92638703011 Collected:11/26/22 12:20 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/30/22 20:08 75-85-41001
tert-Amylmethyl ether ND ug/L 11/30/22 20:08 994-05-810.0 1
Benzene 30.3 ug/L 11/30/22 20:08 71-43-20.50 1
Bromobenzene ND ug/L 11/30/22 20:08 108-86-10.50 1
Bromochloromethane ND ug/L 11/30/22 20:08 74-97-50.50 1
Bromodichloromethane ND ug/L 11/30/22 20:08 75-27-40.50 1
Bromoform ND ug/L 11/30/22 20:08 75-25-20.50 1
Bromomethane ND ug/L 11/30/22 20:08 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/30/22 20:08 75-65-050.0 1
n-Butylbenzene ND ug/L 11/30/22 20:08 104-51-80.50 1
sec-Butylbenzene 4.0 ug/L 11/30/22 20:08 135-98-80.50 1
tert-Butylbenzene 0.81 ug/L 11/30/22 20:08 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/30/22 20:08 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/30/22 20:08 56-23-50.50 1
Chlorobenzene ND ug/L 11/30/22 20:08 108-90-70.50 1
Chloroethane ND ug/L 11/30/22 20:08 75-00-31.0 1
Chloroform ND ug/L 11/30/22 20:08 67-66-30.50 1
Chloromethane ND ug/L 11/30/22 20:08 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/30/22 20:08 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/30/22 20:08 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/30/22 20:08 96-12-81.0 1
Dibromochloromethane ND ug/L 11/30/22 20:08 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/30/22 20:08 106-93-40.50 1
Dibromomethane ND ug/L 11/30/22 20:08 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/30/22 20:08 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/30/22 20:08 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/30/22 20:08 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/30/22 20:08 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/30/22 20:08 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/30/22 20:08 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/30/22 20:08 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/30/22 20:08 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/30/22 20:08 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/30/22 20:08 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/30/22 20:08 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/30/22 20:08 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/30/22 20:08 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/30/22 20:08 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/30/22 20:08 10061-02-60.50 1
Diisopropyl ether 5.6 ug/L 11/30/22 20:08 108-20-30.50 1
Ethanol ND ug/L 11/30/22 20:08 64-17-52001
Ethylbenzene 17.5 ug/L 11/30/22 20:08 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/30/22 20:08 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/30/22 20:08 87-68-32.0 1
Isopropylbenzene (Cumene)4.1 ug/L 11/30/22 20:08 98-82-80.50 1
Methylene Chloride ND ug/L 11/30/22 20:08 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW21R Lab ID:92638703011 Collected:11/26/22 12:20 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 3.2 ug/L 11/30/22 20:08 1634-04-40.50 1
Naphthalene 12.4 ug/L 11/30/22 20:08 91-20-32.0 1
n-Propylbenzene 3.7 ug/L 11/30/22 20:08 103-65-10.50 1
Styrene ND ug/L 11/30/22 20:08 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/30/22 20:08 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/30/22 20:08 79-34-50.50 1
Tetrachloroethene ND ug/L 11/30/22 20:08 127-18-40.50 1
Toluene 0.93 ug/L 11/30/22 20:08 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/30/22 20:08 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/30/22 20:08 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/30/22 20:08 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/30/22 20:08 79-00-50.50 1
Trichloroethene ND ug/L 11/30/22 20:08 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/30/22 20:08 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/30/22 20:08 96-18-40.50 1
1,2,4-Trimethylbenzene 9.2 ug/L 11/30/22 20:08 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/30/22 20:08 108-67-80.50 1
Vinyl chloride ND ug/L 11/30/22 20:08 75-01-41.0 1
m&p-Xylene 4.7 ug/L 11/30/22 20:08 179601-23-11.0 1
o-Xylene 0.93 ug/L 11/30/22 20:08 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)88 %11/30/22 20:08 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %11/30/22 20:08 460-00-470-130 1
Toluene-d8 (S)96 %11/30/22 20:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW23 Lab ID:92638703012 Collected:11/26/22 12:35 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/30/22 16:12 75-85-41001
tert-Amylmethyl ether ND ug/L 11/30/22 16:12 994-05-810.0 1
Benzene ND ug/L 11/30/22 16:12 71-43-20.50 1
Bromobenzene ND ug/L 11/30/22 16:12 108-86-10.50 1
Bromochloromethane ND ug/L 11/30/22 16:12 74-97-50.50 1
Bromodichloromethane ND ug/L 11/30/22 16:12 75-27-40.50 1
Bromoform ND ug/L 11/30/22 16:12 75-25-20.50 1
Bromomethane ND ug/L 11/30/22 16:12 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/30/22 16:12 75-65-050.0 1
n-Butylbenzene ND ug/L 11/30/22 16:12 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/30/22 16:12 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/30/22 16:12 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/30/22 16:12 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/30/22 16:12 56-23-50.50 1
Chlorobenzene ND ug/L 11/30/22 16:12 108-90-70.50 1
Chloroethane ND ug/L 11/30/22 16:12 75-00-31.0 1
Chloroform 1.1 ug/L 11/30/22 16:12 67-66-30.50 1
Chloromethane ND ug/L 11/30/22 16:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/30/22 16:12 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/30/22 16:12 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/30/22 16:12 96-12-81.0 1
Dibromochloromethane ND ug/L 11/30/22 16:12 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/30/22 16:12 106-93-40.50 1
Dibromomethane ND ug/L 11/30/22 16:12 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/30/22 16:12 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/30/22 16:12 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/30/22 16:12 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/30/22 16:12 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/30/22 16:12 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/30/22 16:12 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/30/22 16:12 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/30/22 16:12 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/30/22 16:12 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/30/22 16:12 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/30/22 16:12 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/30/22 16:12 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/30/22 16:12 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/30/22 16:12 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/30/22 16:12 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/30/22 16:12 108-20-30.50 1
Ethanol ND ug/L 11/30/22 16:12 64-17-52001
Ethylbenzene ND ug/L 11/30/22 16:12 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/30/22 16:12 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/30/22 16:12 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/30/22 16:12 98-82-80.50 1
Methylene Chloride ND ug/L 11/30/22 16:12 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Sample:MW23 Lab ID:92638703012 Collected:11/26/22 12:35 Received:11/28/22 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 11/30/22 16:12 1634-04-40.50 1
Naphthalene ND ug/L 11/30/22 16:12 91-20-32.0 1
n-Propylbenzene ND ug/L 11/30/22 16:12 103-65-10.50 1
Styrene ND ug/L 11/30/22 16:12 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/30/22 16:12 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/30/22 16:12 79-34-50.50 1
Tetrachloroethene ND ug/L 11/30/22 16:12 127-18-40.50 1
Toluene ND ug/L 11/30/22 16:12 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/30/22 16:12 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/30/22 16:12 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/30/22 16:12 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/30/22 16:12 79-00-50.50 1
Trichloroethene ND ug/L 11/30/22 16:12 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/30/22 16:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/30/22 16:12 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/30/22 16:12 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/30/22 16:12 108-67-80.50 1
Vinyl chloride ND ug/L 11/30/22 16:12 75-01-41.0 1
m&p-Xylene ND ug/L 11/30/22 16:12 179601-23-11.0 1
o-Xylene ND ug/L 11/30/22 16:12 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)87 %11/30/22 16:12 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %11/30/22 16:12 460-00-470-130 1
Toluene-d8 (S)98 %11/30/22 16:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
740165
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92638703004, 92638703005, 92638703007, 92638703008, 92638703009, 92638703010, 92638703011,
92638703012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3851028
Associated Lab Samples:92638703004, 92638703005, 92638703007, 92638703008, 92638703009, 92638703010, 92638703011,
92638703012
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/30/22 14:59
1,1,1-Trichloroethane ug/L ND 0.50 11/30/22 14:59
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/30/22 14:59
1,1,2-Trichloroethane ug/L ND 0.50 11/30/22 14:59
1,1-Dichloroethane ug/L ND 0.50 11/30/22 14:59
1,1-Dichloroethene ug/L ND 0.50 11/30/22 14:59
1,1-Dichloropropene ug/L ND 0.50 11/30/22 14:59
1,2,3-Trichlorobenzene ug/L ND 2.0 11/30/22 14:59
1,2,3-Trichloropropane ug/L ND 0.50 11/30/22 14:59
1,2,4-Trichlorobenzene ug/L ND 2.0 11/30/22 14:59
1,2,4-Trimethylbenzene ug/L ND 0.50 11/30/22 14:59
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/30/22 14:59
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/30/22 14:59
1,2-Dichlorobenzene ug/L ND 0.50 11/30/22 14:59
1,2-Dichloroethane ug/L ND 0.50 11/30/22 14:59
1,2-Dichloropropane ug/L ND 0.50 11/30/22 14:59
1,3,5-Trimethylbenzene ug/L ND 0.50 11/30/22 14:59
1,3-Dichlorobenzene ug/L ND 0.50 11/30/22 14:59
1,3-Dichloropropane ug/L ND 0.50 11/30/22 14:59
1,4-Dichlorobenzene ug/L ND 0.50 11/30/22 14:59
2,2-Dichloropropane ug/L ND 0.50 11/30/22 14:59
2-Chlorotoluene ug/L ND 0.50 11/30/22 14:59
4-Chlorotoluene ug/L ND 0.50 11/30/22 14:59
Benzene ug/L ND 0.50 11/30/22 14:59
Bromobenzene ug/L ND 0.50 11/30/22 14:59
Bromochloromethane ug/L ND 0.50 11/30/22 14:59
Bromodichloromethane ug/L ND 0.50 11/30/22 14:59
Bromoform ug/L ND 0.50 11/30/22 14:59
Bromomethane ug/L ND 5.0 11/30/22 14:59
Carbon tetrachloride ug/L ND 0.50 11/30/22 14:59
Chlorobenzene ug/L ND 0.50 11/30/22 14:59
Chloroethane ug/L ND 1.0 11/30/22 14:59
Chloroform ug/L ND 0.50 11/30/22 14:59
Chloromethane ug/L ND 1.0 11/30/22 14:59
cis-1,2-Dichloroethene ug/L ND 0.50 11/30/22 14:59
cis-1,3-Dichloropropene ug/L ND 0.50 11/30/22 14:59
Dibromochloromethane ug/L ND 0.50 11/30/22 14:59
Dibromomethane ug/L ND 0.50 11/30/22 14:59
Dichlorodifluoromethane ug/L ND 0.50 11/30/22 14:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3851028
Associated Lab Samples:92638703004, 92638703005, 92638703007, 92638703008, 92638703009, 92638703010, 92638703011,
92638703012
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 0.50 11/30/22 14:59
Ethanol ug/L ND 200 11/30/22 14:59
Ethyl-tert-butyl ether ug/L ND 10.0 11/30/22 14:59
Ethylbenzene ug/L ND 0.50 11/30/22 14:59
Hexachloro-1,3-butadiene ug/L ND 2.0 11/30/22 14:59
Isopropylbenzene (Cumene)ug/L ND 0.50 11/30/22 14:59
m&p-Xylene ug/L ND 1.0 11/30/22 14:59
Methyl-tert-butyl ether ug/L ND 0.50 11/30/22 14:59
Methylene Chloride ug/L ND 2.0 11/30/22 14:59
n-Butylbenzene ug/L ND 0.50 11/30/22 14:59
n-Propylbenzene ug/L ND 0.50 11/30/22 14:59
Naphthalene ug/L ND 2.0 11/30/22 14:59
o-Xylene ug/L ND 0.50 11/30/22 14:59
sec-Butylbenzene ug/L ND 0.50 11/30/22 14:59
Styrene ug/L ND 0.50 11/30/22 14:59
tert-Amyl Alcohol ug/L ND 100 11/30/22 14:59
tert-Amylmethyl ether ug/L ND 10.0 11/30/22 14:59
tert-Butyl Alcohol ug/L ND 50.0 11/30/22 14:59
tert-Butyl Formate ug/L ND 50.0 11/30/22 14:59
tert-Butylbenzene ug/L ND 0.50 11/30/22 14:59
Tetrachloroethene ug/L ND 0.50 11/30/22 14:59
Toluene ug/L ND 0.50 11/30/22 14:59
trans-1,2-Dichloroethene ug/L ND 0.50 11/30/22 14:59
trans-1,3-Dichloropropene ug/L ND 0.50 11/30/22 14:59
Trichloroethene ug/L ND 0.50 11/30/22 14:59
Trichlorofluoromethane ug/L ND 1.0 11/30/22 14:59
Vinyl chloride ug/L ND 1.0 11/30/22 14:59
1,2-Dichloroethane-d4 (S)%87 70-130 11/30/22 14:59
4-Bromofluorobenzene (S)%97 70-130 11/30/22 14:59
Toluene-d8 (S)%99 70-130 11/30/22 14:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3851029LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.350 99 60-140
1,1,1-Trichloroethane ug/L 45.150 90 60-140
1,1,2,2-Tetrachloroethane ug/L 46.750 93 60-140
1,1,2-Trichloroethane ug/L 48.450 97 60-140
1,1-Dichloroethane ug/L 43.050 86 60-140
1,1-Dichloroethene ug/L 47.750 95 60-140
1,1-Dichloropropene ug/L 49.150 98 60-140
1,2,3-Trichlorobenzene ug/L 53.250 106 60-140
1,2,3-Trichloropropane ug/L 43.650 87 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3851029LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 51.750 103 60-140
1,2,4-Trimethylbenzene ug/L 47.250 94 60-140
1,2-Dibromo-3-chloropropane ug/L 49.550 99 60-140
1,2-Dibromoethane (EDB)ug/L 50.050 100 60-140
1,2-Dichlorobenzene ug/L 49.650 99 60-140
1,2-Dichloroethane ug/L 40.850 82 60-140
1,2-Dichloropropane ug/L 47.650 95 60-140
1,3,5-Trimethylbenzene ug/L 46.750 93 60-140
1,3-Dichlorobenzene ug/L 49.250 98 60-140
1,3-Dichloropropane ug/L 46.750 93 60-140
1,4-Dichlorobenzene ug/L 47.150 94 60-140
2,2-Dichloropropane ug/L 43.550 87 60-140
2-Chlorotoluene ug/L 45.550 91 60-140
4-Chlorotoluene ug/L 44.650 89 60-140
Benzene ug/L 46.450 93 60-140
Bromobenzene ug/L 49.650 99 60-140
Bromochloromethane ug/L 51.150 102 60-140
Bromodichloromethane ug/L 45.350 91 60-140
Bromoform ug/L 49.450 99 60-140
Bromomethane ug/L 42.350 85 60-140
Carbon tetrachloride ug/L 43.850 88 60-140
Chlorobenzene ug/L 48.450 97 60-140
Chloroethane ug/L 46.250 92 60-140
Chloroform ug/L 42.950 86 60-140
Chloromethane ug/L 49.850 100 60-140
cis-1,2-Dichloroethene ug/L 42.650 85 60-140
cis-1,3-Dichloropropene ug/L 47.250 94 60-140
Dibromochloromethane ug/L 48.150 96 60-140
Dibromomethane ug/L 54.150 108 60-140
Dichlorodifluoromethane ug/L 52.650 105 60-140
Diisopropyl ether ug/L 42.350 85 60-140
Ethanol ug/L 15602000 78 60-140
Ethyl-tert-butyl ether ug/L 85.1100 85 60-140
Ethylbenzene ug/L 45.950 92 60-140
Hexachloro-1,3-butadiene ug/L 50.950 102 60-140
Isopropylbenzene (Cumene)ug/L 46.050 92 60-140
m&p-Xylene ug/L 93.0100 93 60-140
Methyl-tert-butyl ether ug/L 47.150 94 60-140
Methylene Chloride ug/L 40.850 82 60-140
n-Butylbenzene ug/L 46.050 92 60-140
n-Propylbenzene ug/L 45.050 90 60-140
Naphthalene ug/L 55.050 110 60-140
o-Xylene ug/L 47.950 96 60-140
sec-Butylbenzene ug/L 45.150 90 60-140
Styrene ug/L 49.150 98 60-140
tert-Amyl Alcohol ug/L 8311000 83 60-140
tert-Amylmethyl ether ug/L 90.8100 91 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3851029LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butyl Alcohol ug/L 413500 83 60-140
tert-Butyl Formate ug/L 328400 82 60-140
tert-Butylbenzene ug/L 40.150 80 60-140
Tetrachloroethene ug/L 51.150 102 60-140
Toluene ug/L 45.650 91 60-140
trans-1,2-Dichloroethene ug/L 45.250 90 60-140
trans-1,3-Dichloropropene ug/L 46.550 93 60-140
Trichloroethene ug/L 51.450 103 60-140
Trichlorofluoromethane ug/L 41.350 83 60-140
Vinyl chloride ug/L 49.950 100 60-140
1,2-Dichloroethane-d4 (S)%85 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3851030MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92638703005
3851031
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 116 60-140123 6 3020ND23.2 24.6
1,1,1-Trichloroethane ug/L 20 116 60-140120 4 3020ND23.2 24.0
1,1,2,2-Tetrachloroethane ug/L 20 111 60-140118 6 3020ND22.3 23.6
1,1,2-Trichloroethane ug/L 20 116 60-140124 7 3020ND23.1 24.7
1,1-Dichloroethane ug/L 20 112 60-140115 3 3020ND22.4 23.1
1,1-Dichloroethene ug/L 20 126 60-140131 3 3020ND25.3 26.1
1,1-Dichloropropene ug/L 20 126 60-140130 3 3020ND25.3 25.9
1,2,3-Trichlorobenzene ug/L M12012760-140141 10 3020ND25.3 28.1
1,2,3-Trichloropropane ug/L 20 104 60-140110 5 3020ND20.9 21.9
1,2,4-Trichlorobenzene ug/L 20 125 60-140133 6 3020ND25.1 26.6
1,2,4-Trimethylbenzene ug/L 20 117 60-140121 4 3020ND23.4 24.3
1,2-Dibromo-3-
chloropropane ug/L 20 112 60-140121 8 3020ND22.3 24.2
1,2-Dibromoethane (EDB)ug/L 20 118 60-140125 6 3020ND23.7 25.1
1,2-Dichlorobenzene ug/L 20 119 60-140126 5 3020ND23.8 25.2
1,2-Dichloroethane ug/L 20 101 60-140106 5 3020ND20.2 21.3
1,2-Dichloropropane ug/L 20 118 60-140125 5 3020ND23.6 24.9
1,3,5-Trimethylbenzene ug/L 20 116 60-140122 5 3020ND23.2 24.4
1,3-Dichlorobenzene ug/L 20 121 60-140126 5 3020ND24.1 25.2
1,3-Dichloropropane ug/L 20 112 60-140119 5 3020ND22.5 23.7
1,4-Dichlorobenzene ug/L 20 117 60-140121 3 3020ND23.5 24.3
2,2-Dichloropropane ug/L 20 112 60-140115 3 3020ND22.3 23.1
2-Chlorotoluene ug/L 20 114 60-140116 2 3020ND22.7 23.2
4-Chlorotoluene ug/L 20 111 60-140115 4 3020ND22.2 23.1
Benzene ug/L 20 118 60-140123 4 3020ND23.5 24.5
Bromobenzene ug/L 20 123 60-140129 5 3020ND24.6 25.7
Bromochloromethane ug/L 20 127 60-140132 4 3020ND25.5 26.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3851030MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92638703005
3851031
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromodichloromethane ug/L 20 108 60-140113 5 3020ND21.5 22.7
Bromoform ug/L 20 111 60-140117 5 3020ND22.2 23.4
Bromomethane ug/L 20 124 60-140120 3 3020ND24.7 24.0
Carbon tetrachloride ug/L 20 111 60-140115 3 3020ND22.2 22.9
Chlorobenzene ug/L 20 121 60-140126 4 3020ND24.2 25.2
Chloroethane ug/L M12014560-140149 3 3020ND28.9 29.7
Chloroform ug/L 20 103 60-140111 7 3020ND20.6 22.2
Chloromethane ug/L 20 136 60-140140 3 3020ND27.2 28.1
cis-1,2-Dichloroethene ug/L 20 109 60-140113 3 3020ND21.8 22.6
cis-1,3-Dichloropropene ug/L 20 111 60-140117 6 3020ND22.1 23.4
Dibromochloromethane ug/L 20 110 60-140118 7 3020ND22.1 23.6
Dibromomethane ug/L 20 130 60-140138 6 3020ND26.1 27.7
Dichlorodifluoromethane ug/L M12014660-140148 1 3020ND29.2 29.6
Diisopropyl ether ug/L 20 103 60-140109 6 3020ND20.7 21.8
Ethanol ug/L 800 102 60-140115 11 30800ND820918
Ethyl-tert-butyl ether ug/L 40 92 60-14097 6 3040ND36.6 38.8
Ethylbenzene ug/L 20 116 60-140120 4 3020ND23.1 24.1
Hexachloro-1,3-butadiene ug/L 20 137 60-140136 1 3020ND27.4 27.3
Isopropylbenzene
(Cumene)ug/L 20 116 60-140120 3 3020ND23.2 24.0
m&p-Xylene ug/L 40 117 60-140121 3 3040ND46.6 48.2
Methyl-tert-butyl ether ug/L 20 109 60-140116 6 3020ND21.8 23.3
Methylene Chloride ug/L 20 90 60-14096 6 3020ND18.1 19.2
n-Butylbenzene ug/L 20 116 60-140122 4 3020ND23.3 24.3
n-Propylbenzene ug/L 20 114 60-140118 3 3020ND22.8 23.6
Naphthalene ug/L M12012560-140141 11 3020ND25.1 28.1
o-Xylene ug/L 20 119 60-140124 4 3020ND23.8 24.8
sec-Butylbenzene ug/L 20 117 60-140121 3 3020ND23.4 24.1
Styrene ug/L 20 116 60-140122 5 3020ND23.1 24.4
tert-Amyl Alcohol ug/L 400 96 60-140104 8 30400ND382416
tert-Amylmethyl ether ug/L 40 97 60-140103 6 3040ND38.8 41.3
tert-Butyl Alcohol ug/L M120014260-140154 8 30200ND285307
tert-Butyl Formate ug/L 160 78 60-14074 5 30160ND125119
tert-Butylbenzene ug/L 20 103 60-140106 2 3020ND20.7 21.1
Tetrachloroethene ug/L 20 130 60-140133 2 3020ND26.1 26.7
Toluene ug/L 20 114 60-140120 5 3020ND22.8 24.0
trans-1,2-Dichloroethene ug/L 20 119 60-140123 3 3020ND23.8 24.5
trans-1,3-Dichloropropene ug/L 20 108 60-140113 5 3020ND21.6 22.6
Trichloroethene ug/L 20 130 60-140138 6 3020ND26.0 27.6
Trichlorofluoromethane ug/L 20 115 60-140117 2 3020ND23.0 23.5
Vinyl chloride ug/L 20 134 60-140137 2 3020ND26.8 27.4
1,2-Dichloroethane-d4 (S)%82 70-13082
4-Bromofluorobenzene (S)%94 70-13094
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
740169
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92638703001, 92638703002, 92638703003, 92638703006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3851045
Associated Lab Samples:92638703001, 92638703002, 92638703003, 92638703006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/01/22 18:14
1,1,1-Trichloroethane ug/L ND 0.50 12/01/22 18:14
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/01/22 18:14
1,1,2-Trichloroethane ug/L ND 0.50 12/01/22 18:14
1,1-Dichloroethane ug/L ND 0.50 12/01/22 18:14
1,1-Dichloroethene ug/L ND 0.50 12/01/22 18:14
1,1-Dichloropropene ug/L ND 0.50 12/01/22 18:14
1,2,3-Trichlorobenzene ug/L ND 2.0 12/01/22 18:14
1,2,3-Trichloropropane ug/L ND 0.50 12/01/22 18:14
1,2,4-Trichlorobenzene ug/L ND 2.0 12/01/22 18:14
1,2,4-Trimethylbenzene ug/L ND 0.50 12/01/22 18:14
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/01/22 18:14
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/01/22 18:14
1,2-Dichlorobenzene ug/L ND 0.50 12/01/22 18:14
1,2-Dichloroethane ug/L ND 0.50 12/01/22 18:14
1,2-Dichloropropane ug/L ND 0.50 12/01/22 18:14
1,3,5-Trimethylbenzene ug/L ND 0.50 12/01/22 18:14
1,3-Dichlorobenzene ug/L ND 0.50 12/01/22 18:14
1,3-Dichloropropane ug/L ND 0.50 12/01/22 18:14
1,4-Dichlorobenzene ug/L ND 0.50 12/01/22 18:14
2,2-Dichloropropane ug/L ND 0.50 12/01/22 18:14
2-Chlorotoluene ug/L ND 0.50 12/01/22 18:14
4-Chlorotoluene ug/L ND 0.50 12/01/22 18:14
Benzene ug/L ND 0.50 12/01/22 18:14
Bromobenzene ug/L ND 0.50 12/01/22 18:14
Bromochloromethane ug/L ND 0.50 12/01/22 18:14
Bromodichloromethane ug/L ND 0.50 12/01/22 18:14
Bromoform ug/L ND 0.50 12/01/22 18:14
Bromomethane ug/L ND 5.0 12/01/22 18:14
Carbon tetrachloride ug/L ND 0.50 12/01/22 18:14
Chlorobenzene ug/L ND 0.50 12/01/22 18:14
Chloroethane ug/L ND 1.0 12/01/22 18:14
Chloroform ug/L ND 0.50 12/01/22 18:14
Chloromethane ug/L ND 1.0 12/01/22 18:14
cis-1,2-Dichloroethene ug/L ND 0.50 12/01/22 18:14
cis-1,3-Dichloropropene ug/L ND 0.50 12/01/22 18:14
Dibromochloromethane ug/L ND 0.50 12/01/22 18:14
Dibromomethane ug/L ND 0.50 12/01/22 18:14
Dichlorodifluoromethane ug/L ND 0.50 12/01/22 18:14
Diisopropyl ether ug/L ND 0.50 12/01/22 18:14
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3851045
Associated Lab Samples:92638703001, 92638703002, 92638703003, 92638703006
Matrix:Water
Analyzed
Ethanol ug/L ND 200 12/01/22 18:14
Ethyl-tert-butyl ether ug/L ND 10.0 12/01/22 18:14
Ethylbenzene ug/L ND 0.50 12/01/22 18:14
Hexachloro-1,3-butadiene ug/L ND 2.0 12/01/22 18:14
Isopropylbenzene (Cumene)ug/L ND 0.50 12/01/22 18:14
m&p-Xylene ug/L ND 1.0 12/01/22 18:14
Methyl-tert-butyl ether ug/L ND 0.50 12/01/22 18:14
Methylene Chloride ug/L ND 2.0 12/01/22 18:14
n-Butylbenzene ug/L ND 0.50 12/01/22 18:14
n-Propylbenzene ug/L ND 0.50 12/01/22 18:14
Naphthalene ug/L ND 2.0 12/01/22 18:14
o-Xylene ug/L ND 0.50 12/01/22 18:14
sec-Butylbenzene ug/L ND 0.50 12/01/22 18:14
Styrene ug/L ND 0.50 12/01/22 18:14
tert-Amyl Alcohol ug/L ND 100 12/01/22 18:14
tert-Amylmethyl ether ug/L ND 10.0 12/01/22 18:14
tert-Butyl Alcohol ug/L ND 50.0 12/01/22 18:14
tert-Butyl Formate ug/L ND 50.0 12/01/22 18:14
tert-Butylbenzene ug/L ND 0.50 12/01/22 18:14
Tetrachloroethene ug/L ND 0.50 12/01/22 18:14
Toluene ug/L ND 0.50 12/01/22 18:14
trans-1,2-Dichloroethene ug/L ND 0.50 12/01/22 18:14
trans-1,3-Dichloropropene ug/L ND 0.50 12/01/22 18:14
Trichloroethene ug/L ND 0.50 12/01/22 18:14
Trichlorofluoromethane ug/L ND 1.0 12/01/22 18:14
Vinyl chloride ug/L ND 1.0 12/01/22 18:14
1,2-Dichloroethane-d4 (S)%83 70-130 12/01/22 18:14
4-Bromofluorobenzene (S)%96 70-130 12/01/22 18:14
Toluene-d8 (S)%98 70-130 12/01/22 18:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3851046LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.550 101 60-140
1,1,1-Trichloroethane ug/L 46.550 93 60-140
1,1,2,2-Tetrachloroethane ug/L 48.650 97 60-140
1,1,2-Trichloroethane ug/L 51.150 102 60-140
1,1-Dichloroethane ug/L 45.550 91 60-140
1,1-Dichloroethene ug/L 49.850 100 60-140
1,1-Dichloropropene ug/L 50.650 101 60-140
1,2,3-Trichlorobenzene ug/L 54.450 109 60-140
1,2,3-Trichloropropane ug/L 45.850 92 60-140
1,2,4-Trichlorobenzene ug/L 53.050 106 60-140
1,2,4-Trimethylbenzene ug/L 47.750 95 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
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[phone]
Page 37 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3851046LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 52.850 106 60-140
1,2-Dibromoethane (EDB)ug/L 52.350 105 60-140
1,2-Dichlorobenzene ug/L 50.750 101 60-140
1,2-Dichloroethane ug/L 42.750 85 60-140
1,2-Dichloropropane ug/L 50.250 100 60-140
1,3,5-Trimethylbenzene ug/L 47.250 94 60-140
1,3-Dichlorobenzene ug/L 49.850 100 60-140
1,3-Dichloropropane ug/L 48.950 98 60-140
1,4-Dichlorobenzene ug/L 48.550 97 60-140
2,2-Dichloropropane ug/L 43.450 87 60-140
2-Chlorotoluene ug/L 46.550 93 60-140
4-Chlorotoluene ug/L 45.950 92 60-140
Benzene ug/L 48.550 97 60-140
Bromobenzene ug/L 51.150 102 60-140
Bromochloromethane ug/L 55.050 110 60-140
Bromodichloromethane ug/L 46.950 94 60-140
Bromoform ug/L 51.150 102 60-140
Bromomethane ug/L 43.750 87 60-140
Carbon tetrachloride ug/L 44.550 89 60-140
Chlorobenzene ug/L 50.550 101 60-140
Chloroethane ug/L 45.850 92 60-140
Chloroform ug/L 44.950 90 60-140
Chloromethane ug/L 54.950 110 60-140
cis-1,2-Dichloroethene ug/L 44.950 90 60-140
cis-1,3-Dichloropropene ug/L 49.150 98 60-140
Dibromochloromethane ug/L 50.350 101 60-140
Dibromomethane ug/L 57.950 116 60-140
Dichlorodifluoromethane ug/L 53.550 107 60-140
Diisopropyl ether ug/L 45.950 92 60-140
Ethanol ug/L 18002000 90 60-140
Ethyl-tert-butyl ether ug/L 81.0100 81 60-140
Ethylbenzene ug/L 47.250 94 60-140
Hexachloro-1,3-butadiene ug/L 49.750 99 60-140
Isopropylbenzene (Cumene)ug/L 47.150 94 60-140
m&p-Xylene ug/L 94.7100 95 60-140
Methyl-tert-butyl ether ug/L 49.450 99 60-140
Methylene Chloride ug/L 68.050 136 60-140
n-Butylbenzene ug/L 45.750 91 60-140
n-Propylbenzene ug/L 45.450 91 60-140
Naphthalene ug/L 57.150 114 60-140
o-Xylene ug/L 49.250 98 60-140
sec-Butylbenzene ug/L 45.450 91 60-140
Styrene ug/L 49.650 99 60-140
tert-Amyl Alcohol ug/L 8841000 88 60-140
tert-Amylmethyl ether ug/L 86.0100 86 60-140
tert-Butyl Alcohol ug/L 657500 131 60-140
tert-Butyl Formate ug/L 318400 80 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
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Page 38 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3851046LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 40.750 81 60-140
Tetrachloroethene ug/L 52.350 105 60-140
Toluene ug/L 47.650 95 60-140
trans-1,2-Dichloroethene ug/L 48.150 96 60-140
trans-1,3-Dichloropropene ug/L 47.550 95 60-140
Trichloroethene ug/L 53.950 108 60-140
Trichlorofluoromethane ug/L 41.250 82 60-140
Vinyl chloride ug/L 53.250 106 60-140
1,2-Dichloroethane-d4 (S)%85 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3851047MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92638618003
3851048
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 118 60-140115 3 3020ND23.7 23.1
1,1,1-Trichloroethane ug/L 20 111 60-140113 2 3020ND22.2 22.7
1,1,2,2-Tetrachloroethane ug/L 20 112 60-140112 0 3020ND22.4 22.4
1,1,2-Trichloroethane ug/L 20 119 60-140121 1 3020ND23.8 24.1
1,1-Dichloroethane ug/L 20 110 60-140109 1 3020ND22.0 21.8
1,1-Dichloroethene ug/L 20 123 60-140121 1 3020ND24.6 24.3
1,1-Dichloropropene ug/L 20 122 60-140123 1 3020ND24.5 24.6
1,2,3-Trichlorobenzene ug/L 20 118 60-140128 8 3020ND23.6 25.6
1,2,3-Trichloropropane ug/L 20 105 60-140106 1 3020ND21.0 21.3
1,2,4-Trichlorobenzene ug/L 20 118 60-140121 3 3020ND23.6 24.2
1,2,4-Trimethylbenzene ug/L 20 114 60-140114 0 3020ND22.9 22.8
1,2-Dibromo-3-
chloropropane ug/L 20 111 60-140115 4 3020ND22.1 23.1
1,2-Dibromoethane (EDB)ug/L 20 120 60-140119 1 3020ND24.1 23.7
1,2-Dichlorobenzene ug/L 20 119 60-140119 0 3020ND23.8 23.8
1,2-Dichloroethane ug/L 20 101 60-140100 1 3020ND20.3 20.1
1,2-Dichloropropane ug/L 20 119 60-140120 1 3020ND23.7 23.9
1,3,5-Trimethylbenzene ug/L 20 113 60-140113 1 3020ND22.7 22.5
1,3-Dichlorobenzene ug/L 20 119 60-140120 1 3020ND23.8 24.0
1,3-Dichloropropane ug/L 20 113 60-140114 0 3020ND22.7 22.8
1,4-Dichlorobenzene ug/L 20 115 60-140114 1 3020ND23.0 22.8
2,2-Dichloropropane ug/L 20 108 60-140108 0 3020ND21.6 21.5
2-Chlorotoluene ug/L 20 112 60-140113 0 3020ND22.5 22.5
4-Chlorotoluene ug/L 20 110 60-140110 0 3020ND21.9 21.9
Benzene ug/L 20 118 60-140118 0 3020ND23.5 23.6
Bromobenzene ug/L 20 121 60-140122 1 3020ND24.2 24.5
Bromochloromethane ug/L 20 127 60-140127 1 3020ND25.3 25.5
Bromodichloromethane ug/L 20 109 60-140108 0 3020ND21.7 21.7
Bromoform ug/L 20 111 60-140110 1 3020ND22.2 22.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
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[phone]
Page 39 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3851047MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92638618003
3851048
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 20 85 60-14097 14 3020ND17.0 19.5
Carbon tetrachloride ug/L 20 110 60-140109 0 3020ND21.9 21.9
Chlorobenzene ug/L 20 121 60-140120 1 3020ND24.3 24.0
Chloroethane ug/L 20 137 60-140133 3 3020ND27.5 26.7
Chloroform ug/L 20 103 60-140107 3 3020ND20.6 21.3
Chloromethane ug/L 20 124 60-140129 3 3020ND24.9 25.7
cis-1,2-Dichloroethene ug/L 20 108 60-140108 0 3020ND21.5 21.5
cis-1,3-Dichloropropene ug/L 20 110 60-140111 0 3020ND22.0 22.1
Dibromochloromethane ug/L 20 113 60-140112 2 3020ND22.7 22.3
Dibromomethane ug/L 20 134 60-140134 0 3020ND26.8 26.9
Dichlorodifluoromethane ug/L 20 136 60-140135 1 3020ND27.3 27.0
Diisopropyl ether ug/L 20 101 60-140103 1 3020ND20.2 20.5
Ethanol ug/L 800 107 60-140113 6 30800ND856906
Ethyl-tert-butyl ether ug/L 40 85 60-14086 1 3040ND34.0 34.4
Ethylbenzene ug/L 20 114 60-140114 1 3020ND22.9 22.7
Hexachloro-1,3-butadiene ug/L 20 120 60-140122 1 3020ND24.1 24.3
Isopropylbenzene
(Cumene)ug/L 20 114 60-140113 1 3020ND22.8 22.5
m&p-Xylene ug/L 40 116 60-140114 2 3040ND46.6 45.7
Methyl-tert-butyl ether ug/L 20 104 60-140105 1 3020ND20.9 21.0
Methylene Chloride ug/L 20 90 60-14088 2 3020ND18.0 17.6
n-Butylbenzene ug/L 20 109 60-140109 0 3020ND21.7 21.8
n-Propylbenzene ug/L 20 111 60-140110 1 3020ND22.3 22.0
Naphthalene ug/L 20 119 60-140132 10 3020ND23.8 26.3
o-Xylene ug/L 20 119 60-140117 2 3020ND23.8 23.3
sec-Butylbenzene ug/L 20 112 60-140111 1 3020ND22.4 22.3
Styrene ug/L 20 115 60-140113 1 3020ND23.0 22.7
tert-Amyl Alcohol ug/L 400 92 60-14098 7 30400ND366391
tert-Amylmethyl ether ug/L 40 93 60-14093 0 3040ND37.2 37.2
tert-Butyl Alcohol ug/L M120014960-140152 2 30200ND298305
tert-Butyl Formate ug/L M11605460-14045 18 30160ND87.1 72.8
tert-Butylbenzene ug/L 20 99 60-14099 1 3020ND19.9 19.7
Tetrachloroethene ug/L 20 129 60-140127 2 3020ND25.8 25.4
Toluene ug/L 20 116 60-140115 0 3020ND23.2 23.1
trans-1,2-Dichloroethene ug/L 20 115 60-140115 0 3020ND23.0 23.0
trans-1,3-Dichloropropene ug/L 20 107 60-140108 1 3020ND21.4 21.5
Trichloroethene ug/L 20 129 60-140131 1 3020ND25.9 26.1
Trichlorofluoromethane ug/L 20 113 60-140111 2 3020ND22.5 22.1
Vinyl chloride ug/L 20 127 60-140130 2 3020ND25.4 26.0
1,2-Dichloroethane-d4 (S)%83 70-13082
4-Bromofluorobenzene (S)%95 70-13095
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
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Page 40 of 45
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92638703
HOT SPOT 2002
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
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[phone]
Page 41 of 45
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92638703
HOT SPOT 2002
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92638703001 740169MW1BSM 6200B
92638703002 740169MW2RSM 6200B
92638703003 740169MW4RSM 6200B
92638703004 740165MW5RSM 6200B
92638703005 740165MW6SM 6200B
92638703006 740169MW7SM 6200B
92638703007 740165MW8SM 6200B
92638703008 740165MW10RSM 6200B
92638703009 740165MW11SM 6200B
92638703010 740165MW20SM 6200B
92638703011 740165MW21RSM 6200B
92638703012 740165MW23SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/03/2022 01:58 PM
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[phone]
Page 42 of 45
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