AS-3693_28826_CA_CAI_20210901

JUNE 2021
CORRECTIVE ACTION PERFORMANCE
REPORT

for the
THE SPOT 2267 Smokey Park Highway Candler, Buncombe County, North Carolina Incident #28826

PREPARED FOR: Theodossis Business, LLC.
1100 McMinn Road Hendersonville, NC 28792 PREPARED BY: Singleton Environmental, Inc. PO Box 604 Fletcher, NC 28732 [phone]

September 1, 2021

Singleton Environmental, Inc.

CORRECTIVE ACTION PERFORMANCE REPORT
September 1, 2021 Incident Number: 28826 Facility ID Number: 00-0-00004683 Site Name: The Spot
2267 Smokey Park Highway
Candler, NC 28705 Incident Number: 28826 Facility ID Number: 0-004683 UST Owner / Operator: Theodossis Business, LLC Contact: Jimmy Theodossis 1100 McMinn Road Hendersonville, NC 28792
Telephone: [phone]
Consultant / Contractor: Singleton Environmental, Inc. PO Box 2012 Enka, NC 28728
Telephone: [phone] Date Release Discovered: March 15, 2010 Estimated Quantity of Release: Unknown/unquantified Cause/Source of Release: Two 3,000-Gallon Gasoline USTs, One 6,000-Gallon Gasoline UST, and One 3,000-Gallon Diesel UST.
Latitude: (35° 32’ 33.14” North)
Longitude: (82° 44’ 45.11” West) Signature and Seal of Certifying Professional Engineer:
I, Christopher D. Singleton, a Professional Geologist, do certify that the information contained in this report is correct and accurate to the best of my knowledge.
____________________________________ Christopher D. Singleton, P.G. #1928

Table of Contents
Introduction ................................................................................................................................1
Field Activities…......................…………......................................... ............................................1 Sampling Results…......................…………......................................... .........................................1 Groundwater .........................................................................................................................1 Conclusions & Recommendations…..................…………......................................... ...................2
Tables Table 1. Groundwater Elevations Table 2. Historical Monitoring Wells Analytical Results Figures Figure 1. 7.5’ USGS Topographic Map Figure 2. Scaled Site Map
Figure 3. Groundwater Flow Direction
Figure 4. Groundwater Concentration Map Appendices
Appendix A: Laboratory Data Sheets

Introduction
This report presents the results of the Groundwater Monitoring Report conducted to evaluate the magnitude and extent of groundwater contamination related to a petroleum release from the former
underground storage tank (UST) system at The Spot located at 2267 Smokey Park Highway in Candler, North Carolina. Figure 1 shows the site location, and Figure 2 presents a site map showing the location of the current UST system, monitoring wells, and soil sampling locations.
Field Activities – Monitoring Wells

Eight groundwater monitoring wells and two water supply wells were sampled on June 7, 2021.
Each monitoring well was sampled following a purge of approximately three (3) well volumes and allowing the groundwater parameters to equilibrate. A new, dedicated, disposable bailer with new cotton twine lanyard was used for sampling each well to prevent cross-contamination. Each water supply well was purged for a total of 20 minutes prior to sample collection. Each groundwater
sample was transferred directly from the bailer to the appropriate sample container provided by the laboratory with Hydrochloric Acid (HCl) preservative. The samples were stored on ice and shipped to Pace Analytical in Asheville, North Carolina. All samples were submitted for laboratory analysis of Volatile Organics (VOCs) by EPA Method 6200B. A copy of the laboratory
deliverable package is included in the Appendices of this report.
Sampling Results Monitoring Wells The June 7, 2021 analytical results from The Spot are as follows:

• Laboratory analysis of the groundwater samples collected from monitoring wells MW-6, MW-7 and MW-8 did not detect targeted petroleum hydrocarbons at concentrations that exceed their respective North Carolina 2L Groundwater Quality Standards (NCAC 2L MCLS).

• Laboratory analysis of the groundwater sample collected from monitoring well MW-1 detected 1,2,4-trimethylbenzene, benzene, disopropylether, isopropylbenzene, MTBE,
naphthalene, toluene, and total xylenes at concentrations exceeding their respective NCAC
2L MCLs. Concentrations of benzene exceeded the GCLs.

• Laboratory analysis of the groundwater sample collected from monitoring well MW-2 detected benzene and naphthalene exceeding the NCAC 2L MCLs. None of the
concentrations exceeded the GCLs.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-3 detected benzene at concentrations exceeding the NCAC 2L MCLs. The concentration of
benzene did not exceed the GCLs.

• Laboratory analysis of the groundwater sample collected from monitoring well MW-4
detected benzene at concentrations exceeding their respective NCAC 2L MCLs. The
concentration of benzene did not exceed the GCLs.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-5 detected 1,2,4-trimethylbenzene, benzene, naphthalene, toluene, and total xylenes at
concentrations exceeding their respective NCAC 2L MCLs. The concentrations detected did not exceed the GCLs.
• Laboratory analysis of groundwater samples collected from water supply wells WSW-1
and WSW-2 did not detect targeted petroleum hydrocarbons at concentrations that exceed the laboratory minimum detection levels.
Free-product was not observed at the site on June 7, 2021. Groundwater analytical results are summarized in Table 2. A copy of the laboratory analytical report is included in Appendix A.
Groundwater Flow Direction
Figure 3 of this report portrays the suspected groundwater flow direction based on the depth to
water on June 7, 2021. The trend of the groundwater is to the southeast. Groundwater levels are
located in Table 2.

MMPE Performance
Recently NCDEQ asked SEI to compare the site data using a modeling program that includes natural attenuation versus MMPE. To accomplish this, SEI used Bioscreen Version 1.4 to compare the site data over the last five years (since the completion of the CSA). The highest benzene concentration of 17,500 ug/l was detected in MW-1 in May 2016. The current benzene
concentration of 9,760 ug/l was detected in MW-1 in June 2021 after three MMPE events since
2019.
While using Bioscreen Version 1.4, the following data was used in addition to the benzene concentrations for each model:
• Seepage Velocity of 12.1 ft/yr.
• Retardation Factor of 1.0t.
• Length of Model area = 200 ft.
• Width of Model area = 130 ft.
• DO = 3.3 mg/l (Lab Data).
• NO3 = 0.083 mg/l (Lab Data).
• FE2+ = 14.7 mg/l (Lab Data).
• SO4 = 3.6 mg/l (Lab Data).
• CH4 = 0.0286 mg/l (Lab Data).
Using the benzene concentrations from May 2016 and modeling a 20-year reduction, the plume
would reach MW-8 (most downgradient well) with a calculated benzene concentration of 2.257
mg/l if no degradation. Assuming 1st order decay occurs 14.9 Kg of plume mass will biodegrade.

Using the benzene concentrations from June 2021 and modeling a 20-year reduction, the plume would reach MW-8 (most downgradient well) with a calculated benzene concentration of 0.612
mg/l if no degradation. Assuming 1st order decay occurs 19.1 Kg of plume mass will biodegrade.
The model estimated there was 28.1 Kg of hydrocarbons in the groundwater in May 2016. Currently, the model estimates there is 22.3 Kg of hydrocarbons remaining. The three MMPE events along with biodegradation have reduced the levels of hydrocarbons at the site by 5.8 Kg in
5 years. The concentration levels of benzene have dropped from 17,500 ug/l to 9,760 ug/l (44.22%
drop) during the same time.
Conclusions and Recommendations
Based on the results of this report, SEI makes the following conclusions:
• The three AFVR events have potentially assisted biodegradation in reducing the levels of hydrocarbons and benzene at the site.
• Laboratory analysis of the groundwater sample collected from monitoring wells MW-1, MW-2, MW-3, MW-4, and MW-5 detected targeted compounds above their respective
NCAC 2L MCLs. MW-1 detected concentrations of benzene exceeded the GCLs.
• Mass contaminant calculation determined a mass of 22.3 Kg for the site with most of the mass concentrated around MW-1, MW-2, MW-3, MW-4 and MW-5.
Therefore, Singleton Environmental, Inc. recommends the following:
• Continue Quarterly MMPE events to attempt to remove more hydrocarbons and assist with biodegradation.
• Continue quarterly groundwater monitoring events after each MMPE event.

Tables

MW Number Top of Casing Elevation
Top of Casing
to GW Depth Groundwater Elevation
MW-1 97.67 21.35 76.32
MW-2 96.31 20.97 75.34
MW-3 94.42 19.38 75.04
MW-4 94.77 19.41 75.36
MW-5 97.02 19.35 77.67
MW-6 98.85 22.18 76.67
MW-7 100 21.85 78.15
MW-8 92.98 22.65 70.33
Table 1
Groundwater Flow Mapping Elevation Details
Candler, NC
The Spot 6-7-2021
1,2,4-
Trimeth
ylbenze
ne
1,3,5-
Trimeth
ylbenze
ne
Benzene Chlorof
orm
Diisopr
opyl
ether
Ethylbe
nzene
Isoprop
ylbenze
ne
(Cumen
e)
Methyl-
tert-
butyl
ether
Methylene Chlorid
e
Naphth
alene Toluene
Trichlor
oethene
m&p-
Xylene
n-
Propylb
enzene
o-
Xylene
Date
Collected
(mm/dd/yy)
Sample
Depth
(ft. BGS)
ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L
6/7/2021 3590 ND 9760 ND 466 3060 135 308 ND 923 1100 ND 10300 ND 4880
2/17/2021 1860 ND 10600 ND 447 2330 77 256 ND 599 9490 ND 6620 ND 3710
10/19/2020 2900 ND 10300 ND 621 2760 117 329 217 779 12200 ND 9210 ND 4630
12/4/2019 3660 923 10400 ND 612 3460 135 397 ND 792 14400 ND 12000 456 5700
04/16/2019 1860 447 12200 50.0 708 2650 76.7 373 ND 501 11700 ND 8160 230 4310
6/7/2021 3.3 ND 564 ND 12.5 ND 10.7 7.4 ND 17.8 ND ND ND ND 43.3
2/17/2021 3.2 ND 816 ND 18 ND 9.7 10.9 ND 17.5 ND ND ND ND 36.9
10/19/2020 37.2 ND 435 ND 13.4 9.3 6.8 11.4 11.2 36.1 4.8 ND 53 ND 144
12/4/2019 118 ND 778 ND 26.1 12.6 5.7 28 ND 59.8 23.4 ND 183 ND 370
04/16/2019 106 25.7 759 2.9 29.0 29.0 7.6 29.7 ND 37.9 28.3 ND 226 6.1 288
6/7/2021 ND ND 211 ND 8.6 1.7 ND 2.4 ND ND 7.6 ND 6.6 ND 2.1
2/17/2021 ND ND 154 ND 6.1 1.3 ND ND ND ND 4 ND 4.3 ND 1.5
10/19/2020 ND ND 49.3 ND 3 0.55 ND ND ND ND 2.6 ND 1.8 ND 0.65
12/4/2019 ND ND ND ND 0.63 ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND 4.5 ND ND ND ND ND ND ND 1.3 ND ND ND ND
2/17/2021 ND ND 7.7 ND ND ND ND ND ND ND 2 ND ND ND ND
10/19/2020 ND ND 0.58 ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND 0.84 ND ND ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 410 ND 58.8 ND ND 296 18.4 ND ND 113 2070 ND 1360 ND 850
2/17/2021 458 ND 108 ND ND 551 22 ND ND 156 3310 ND 1880 ND 1150
10/19/2020 900 ND 323 ND ND 1050 40 ND 126 307 7630 ND 3700 ND 2120
12/4/2019 802 184 1030 ND ND 1170 36.1 ND ND 253 8950 ND 4300 86.2 2200
04/16/2019 653 207 596 ND ND 797 30.5 ND ND 180 3000 ND 2870 80.8 1410
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND 0.59 ND ND 0.75 ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND 2 ND ND 1.9 ND ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2020 ND ND ND ND 1.9 ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND 0.61 ND ND ND
12/4/2019 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
400 400 1 70 70 600 70 20 5 6 600 3 500 70 500
28500 25000 5000 70000 70000 84500 25000 20000 5000 6000 260000 3000 85500 30000 85500
ft. BGS = feet below ground surface
mg/L = milligrams per liter
ug/L = micrograms per liter
Bold data above the MSCC (Soil to Groundwater)
2L Class GCL Standards
NOTES:
ND = Not Detected
Analytical Method
Sample ID
Constituent of Concern
2L Class GA Standards
MW-1
MW-2
MW-3
MW-4
MW-5
MW-6
MW-7
MW-8
WSW-1
WSW-2
Table # 2
Summary of Analytical Results - Water Samples
NCDEQ's Incident # 28826

Figures

ASHEVILLE QUADRANGLE NORTH CAROLINA 7.5 MINUTE SERIES (TOPOGRAPHIC)
Figure 1 Site Map
The Spot – Candler, NC
THE SPOT
Singleton Environmental, Inc
Singleton Environmental, Inc
Singleton Environmental, Inc

Bioscreen Version 1.4 Data

DISSOLVED HYDROCARBON CONCENTRATION ALONG PLUME CENTERLINE (mg/L at Z=0)Distance from Source (ft)TYPE OF MODEL0 20 40 60 80 100 120 140 160 180 200No Degradation9.760 2.649 1.902 1.559 1.345 1.188 1.058 0.942 0.831 0.721 0.6121st Order Decay9.760 0.171 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000Inst. Reaction9.760 2.641 1.885 1.526 1.284 1.082 0.882 0.664 0.414 0.126 0.000Field Data from Site9.760 0.564Time:20 YearsNext TimestepPrev TimestepCalculateAnimationRecalculate This 0.0002.0004.0006.0008.00010.00012.0000 50 100 150 200 250Concentration(mg/L)Distance From Source (ft)1st Order DecayInstantaneous ReactionNo DegradationField Data from SiteReturn to
TransverseDISSOLVED HYDROCARBON CONCENTRATIONS IN PLUME (mg/L at Z=0)Distance (ft) Distance from Source (ft)Model to Display:0 20 40 60 80 100 120 140 160 180 20041 0.059 0.051 0.040 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.00021 0.059 0.109 0.309 0.436 0.482 0.466 0.397 0.275 0.099 0.000 0.0000 9.760 2.641 1.885 1.526 1.284 1.082 0.882 0.664 0.414 0.126 0.000-21 0.059 0.109 0.309 0.436 0.4820.466 0.397 0.275 0.099 0.000 0.000-41 0.059 0.051 0.040 0.018 0.0000.000 0.000 0.000 0.000 0.000 0.000MASS1.6E+2 1.7E+2 1.5E+2 1.4E+2 1.3E+2 1.2E+2 9.6E+1 7.0E+1 3.5E+1 7.2E+0 0.0E+0FLUX(mg/day)Time:20 YearsTarget Level: 0.001 mg/L Displayed Model: Inst. ReactionPlume and Source Masses (Order-of-Magnitude Accuracy)Plume Mass if No Biodegradation22.3(Kg)- Actual Plume Mass3.1(Kg)= Plume Mass Removed by Biodeg19.1(Kg)(86 %)Change in Electron Acceptor/Byproduct Masses:Oxygen Nitrate Iron II Sulfate Methane-24.8 -0.6 +110.5 -27.1 +0.2(Kg)Contam. Mass in Source (t=0 Years) Infinite(Kg)Contam. Mass in Source Now (t=20Years) Infinite(Kg) Current Volume of Groundwater in Plume 1.0(ac-ft) Flowrate of Water Through Source Zone 0.336(ac-ft/yr)410-410.0001.0002.0003.0004.0005.0006.0007.0008.0009.00010.000020406080100120140160180(ft)Concentration (mg/L)(ft)Recalculate No Degradation 1st Order Decay Instantaneous Plot All DataPlot Data > TargetMass HELP
DISSOLVED HYDROCARBON CONCENTRATION ALONG PLUME CENTERLINE (mg/L at Z=0)Distance from Source (ft)TYPE OF MODEL0 20 40 60 80 100 120 140 160 180 200No Degradation17.370 6.070 4.878 4.323 3.964 3.683 3.428 3.169 2.891 2.587 2.2571st Order Decay17.370 0.392 0.020 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000Inst. Reaction17.030 5.966 4.795 4.239 3.864 3.545 3.226 2.872 2.460 1.983 1.444Field Data from Site17.500 1.920Time:20 YearsNext TimestepPrev TimestepCalculateAnimationRecalculate This 0.0005.00010.00015.00020.0000 50 100 150 200 250Concentration(mg/L)Distance From Source (ft)1st Order DecayInstantaneous ReactionNo DegradationField Data from SiteReturn to
TransverseDISSOLVED HYDROCARBON CONCENTRATIONS IN PLUME (mg/L at Z=0)Distance (ft) Distance from Source (ft)Model to Display:0 20 40 60 80 100 120 140 160 180 20041 1.937 1.925 1.909 1.873 1.814 1.726 1.595 1.408 1.157 0.839 0.46221 1.937 2.017 2.331 2.531 2.603 2.576 2.460 2.255 1.959 1.576 1.1160 17.030 5.966 4.795 4.239 3.864 3.545 3.226 2.872 2.460 1.983 1.444-21 1.937 2.017 2.331 2.531 2.6032.576 2.460 2.255 1.959 1.576 1.116-41 1.937 1.925 1.909 1.873 1.8141.726 1.595 1.408 1.157 0.839 0.462MASS1.0E+3 8.0E+2 7.6E+2 7.5E+2 7.3E+2 7.0E+2 6.5E+2 5.9E+2 5.0E+2 3.9E+2 2.6E+2FLUX(mg/day)Time:20 YearsTarget Level: 0.001 mg/L Displayed Model: Inst. ReactionPlume and Source Masses (Order-of-Magnitude Accuracy)Plume Mass if No Biodegradation28.1(Kg)- Actual Plume Mass13.2(Kg)= Plume Mass Removed by Biodeg14.9(Kg)(53 %)Change in Electron Acceptor/Byproduct Masses:Oxygen Nitrate Iron II Sulfate Methane-19.3 -0.5 +85.9 -21.0 +0.2(Kg)Contam. Mass in Source (t=0 Years) 1000.0(Kg)Contam. Mass in Source Now (t=20Years) 971.9(Kg) Current Volume of Groundwater in Plume 1.6(ac-ft) Flowrate of Water Through Source Zone 0.336(ac-ft/yr)410-410.0002.0004.0006.0008.00010.00012.00014.00016.00018.000020406080100120140160180(ft)Concentration (mg/L)(ft)Recalculate No Degradation 1st Order Decay Instantaneous Plot All DataPlot Data > TargetMass HELP

APPENDIX A

#=CL#
June 10, 2021
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92542712
92542712
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
P.O. Box 2012
Enka, NC 28728
The Spot 6/7/21
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on June 07, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 38
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 38
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92542712001 WSW-1 SM 6200B 63 PASI-CPM1
92542712002 WSW-2 SM 6200B 63 PASI-CPM1
92542712003 MW-1 SM 6200B 63 PASI-CPM1
92542712004 MW-2 SM 6200B 63 PASI-CPM1
92542712005 MW-3 SM 6200B 63 PASI-CSAS
92542712006 MW-4 SM 6200B 63 PASI-CPM1
92542712007 MW-5 SM 6200B 63 PASI-CPM1
92542712008 MW-6 SM 6200B 63 PASI-CPM1
92542712009 MW-7 SM 6200B 63 PASI-CPM1
92542712010 MW-8 SM 6200B 63 PASI-CPM1
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:WSW-1 Lab ID:92542712001 Collected:06/07/21 12:00 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 06/08/21 15:29 71-43-20.50 1
Bromobenzene ND ug/L 06/08/21 15:29 108-86-10.50 1
Bromochloromethane ND ug/L 06/08/21 15:29 74-97-50.50 1
Bromodichloromethane ND ug/L 06/08/21 15:29 75-27-40.50 1
Bromoform ND ug/L 06/08/21 15:29 75-25-20.50 1
Bromomethane ND ug/L 06/08/21 15:29 74-83-95.0 1
n-Butylbenzene ND ug/L 06/08/21 15:29 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/08/21 15:29 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/08/21 15:29 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/08/21 15:29 56-23-50.50 1
Chlorobenzene ND ug/L 06/08/21 15:29 108-90-70.50 1
Chloroethane ND ug/L 06/08/21 15:29 75-00-31.0 1
Chloroform ND ug/L 06/08/21 15:29 67-66-30.50 1
Chloromethane ND ug/L 06/08/21 15:29 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/08/21 15:29 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/08/21 15:29 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/08/21 15:29 96-12-81.0 1
Dibromochloromethane ND ug/L 06/08/21 15:29 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/08/21 15:29 106-93-40.50 1
Dibromomethane ND ug/L 06/08/21 15:29 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/08/21 15:29 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/08/21 15:29 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/08/21 15:29 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/08/21 15:29 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/08/21 15:29 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/08/21 15:29 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/08/21 15:29 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/08/21 15:29 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/08/21 15:29 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/08/21 15:29 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/08/21 15:29 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/08/21 15:29 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/08/21 15:29 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/08/21 15:29 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/08/21 15:29 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/08/21 15:29 108-20-30.50 1
Ethylbenzene ND ug/L 06/08/21 15:29 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/08/21 15:29 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/08/21 15:29 98-82-80.50 1
Methylene Chloride ND ug/L 06/08/21 15:29 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/08/21 15:29 1634-04-40.50 1
Naphthalene ND ug/L 06/08/21 15:29 91-20-32.0 1
n-Propylbenzene ND ug/L 06/08/21 15:29 103-65-10.50 1
Styrene ND ug/L 06/08/21 15:29 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/08/21 15:29 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/08/21 15:29 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:WSW-1 Lab ID:92542712001 Collected:06/07/21 12:00 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 06/08/21 15:29 127-18-40.50 1
Toluene ND ug/L 06/08/21 15:29 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/08/21 15:29 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/08/21 15:29 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/08/21 15:29 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/08/21 15:29 79-00-50.50 1
Trichloroethene ND ug/L 06/08/21 15:29 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/08/21 15:29 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/08/21 15:29 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/08/21 15:29 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/08/21 15:29 108-67-80.50 1
Vinyl chloride ND ug/L 06/08/21 15:29 75-01-41.0 1
m&p-Xylene ND ug/L 06/08/21 15:29 179601-23-11.0 1
o-Xylene ND ug/L 06/08/21 15:29 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %06/08/21 15:29 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %06/08/21 15:29 460-00-470-130 1
Toluene-d8 (S)99 %06/08/21 15:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:WSW-2 Lab ID:92542712002 Collected:06/07/21 12:20 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 06/08/21 15:47 71-43-20.50 1
Bromobenzene ND ug/L 06/08/21 15:47 108-86-10.50 1
Bromochloromethane ND ug/L 06/08/21 15:47 74-97-50.50 1
Bromodichloromethane ND ug/L 06/08/21 15:47 75-27-40.50 1
Bromoform ND ug/L 06/08/21 15:47 75-25-20.50 1
Bromomethane ND ug/L 06/08/21 15:47 74-83-95.0 1
n-Butylbenzene ND ug/L 06/08/21 15:47 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/08/21 15:47 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/08/21 15:47 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/08/21 15:47 56-23-50.50 1
Chlorobenzene ND ug/L 06/08/21 15:47 108-90-70.50 1
Chloroethane ND ug/L 06/08/21 15:47 75-00-31.0 1
Chloroform ND ug/L 06/08/21 15:47 67-66-30.50 1
Chloromethane ND ug/L 06/08/21 15:47 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/08/21 15:47 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/08/21 15:47 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/08/21 15:47 96-12-81.0 1
Dibromochloromethane ND ug/L 06/08/21 15:47 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/08/21 15:47 106-93-40.50 1
Dibromomethane ND ug/L 06/08/21 15:47 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/08/21 15:47 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/08/21 15:47 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/08/21 15:47 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/08/21 15:47 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/08/21 15:47 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/08/21 15:47 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/08/21 15:47 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/08/21 15:47 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/08/21 15:47 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/08/21 15:47 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/08/21 15:47 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/08/21 15:47 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/08/21 15:47 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/08/21 15:47 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/08/21 15:47 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/08/21 15:47 108-20-30.50 1
Ethylbenzene ND ug/L 06/08/21 15:47 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/08/21 15:47 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/08/21 15:47 98-82-80.50 1
Methylene Chloride ND ug/L 06/08/21 15:47 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/08/21 15:47 1634-04-40.50 1
Naphthalene ND ug/L 06/08/21 15:47 91-20-32.0 1
n-Propylbenzene ND ug/L 06/08/21 15:47 103-65-10.50 1
Styrene ND ug/L 06/08/21 15:47 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/08/21 15:47 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/08/21 15:47 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:WSW-2 Lab ID:92542712002 Collected:06/07/21 12:20 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 06/08/21 15:47 127-18-40.50 1
Toluene ND ug/L 06/08/21 15:47 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/08/21 15:47 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/08/21 15:47 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/08/21 15:47 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/08/21 15:47 79-00-50.50 1
Trichloroethene ND ug/L 06/08/21 15:47 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/08/21 15:47 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/08/21 15:47 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/08/21 15:47 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/08/21 15:47 108-67-80.50 1
Vinyl chloride ND ug/L 06/08/21 15:47 75-01-41.0 1
m&p-Xylene ND ug/L 06/08/21 15:47 179601-23-11.0 1
o-Xylene ND ug/L 06/08/21 15:47 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %06/08/21 15:47 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/08/21 15:47 460-00-470-130 1
Toluene-d8 (S)100 %06/08/21 15:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-1 Lab ID:92542712003 Collected:06/07/21 09:45 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 9760 ug/L 06/08/21 20:35 71-43-250.0 100
Bromobenzene ND ug/L 06/08/21 20:35 108-86-150.0 100
Bromochloromethane ND ug/L 06/08/21 20:35 74-97-550.0 100
Bromodichloromethane ND ug/L 06/08/21 20:35 75-27-450.0 100
Bromoform ND ug/L 06/08/21 20:35 75-25-250.0 100
Bromomethane ND ug/L 06/08/21 20:35 74-83-9500100
n-Butylbenzene ND ug/L 06/08/21 20:35 104-51-850.0 100
sec-Butylbenzene ND ug/L 06/08/21 20:35 135-98-850.0 100
tert-Butylbenzene ND ug/L 06/08/21 20:35 98-06-650.0 100
Carbon tetrachloride ND ug/L 06/08/21 20:35 56-23-550.0 100
Chlorobenzene ND ug/L 06/08/21 20:35 108-90-750.0 100
Chloroethane ND ug/L 06/08/21 20:35 75-00-3100100
Chloroform ND ug/L 06/08/21 20:35 67-66-350.0 100
Chloromethane ND ug/L 06/08/21 20:35 74-87-3100100
2-Chlorotoluene ND ug/L 06/08/21 20:35 95-49-850.0 100
4-Chlorotoluene ND ug/L 06/08/21 20:35 106-43-450.0 100
1,2-Dibromo-3-chloropropane ND ug/L 06/08/21 20:35 96-12-8100100
Dibromochloromethane ND ug/L 06/08/21 20:35 124-48-150.0 100
1,2-Dibromoethane (EDB)ND ug/L 06/08/21 20:35 106-93-450.0 100
Dibromomethane ND ug/L 06/08/21 20:35 74-95-350.0 100
1,2-Dichlorobenzene ND ug/L 06/08/21 20:35 95-50-150.0 100
1,3-Dichlorobenzene ND ug/L 06/08/21 20:35 541-73-150.0 100
1,4-Dichlorobenzene ND ug/L 06/08/21 20:35 106-46-750.0 100
Dichlorodifluoromethane ND ug/L 06/08/21 20:35 75-71-850.0 100
1,1-Dichloroethane ND ug/L 06/08/21 20:35 75-34-350.0 100
1,2-Dichloroethane ND ug/L 06/08/21 20:35 107-06-250.0 100
1,1-Dichloroethene ND ug/L 06/08/21 20:35 75-35-450.0 100
cis-1,2-Dichloroethene ND ug/L 06/08/21 20:35 156-59-250.0 100
trans-1,2-Dichloroethene ND ug/L 06/08/21 20:35 156-60-550.0 100
1,2-Dichloropropane ND ug/L 06/08/21 20:35 78-87-550.0 100
1,3-Dichloropropane ND ug/L 06/08/21 20:35 142-28-950.0 100
2,2-Dichloropropane ND ug/L 06/08/21 20:35 594-20-750.0 100
1,1-Dichloropropene ND ug/L 06/08/21 20:35 563-58-650.0 100
cis-1,3-Dichloropropene ND ug/L 06/08/21 20:35 10061-01-550.0 100
trans-1,3-Dichloropropene ND ug/L 06/08/21 20:35 10061-02-650.0 100
Diisopropyl ether 466 ug/L 06/08/21 20:35 108-20-350.0 100
Ethylbenzene 3060 ug/L 06/08/21 20:35 100-41-450.0 100
Hexachloro-1,3-butadiene ND ug/L 06/08/21 20:35 87-68-3200100
Isopropylbenzene (Cumene)135 ug/L 06/08/21 20:35 98-82-850.0 100
Methylene Chloride ND ug/L 06/08/21 20:35 75-09-2200100
Methyl-tert-butyl ether 308 ug/L 06/08/21 20:35 1634-04-450.0 100
Naphthalene 923 ug/L 06/08/21 20:35 91-20-3200100
n-Propylbenzene ND ug/L 06/08/21 20:35 103-65-150.0 100
Styrene ND ug/L 06/08/21 20:35 100-42-550.0 100
1,1,1,2-Tetrachloroethane ND ug/L 06/08/21 20:35 630-20-650.0 100
1,1,2,2-Tetrachloroethane ND ug/L 06/08/21 20:35 79-34-550.0 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-1 Lab ID:92542712003 Collected:06/07/21 09:45 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 06/08/21 20:35 127-18-450.0 100
Toluene 11000 ug/L 06/08/21 20:35 108-88-350.0 100
1,2,3-Trichlorobenzene ND ug/L 06/08/21 20:35 87-61-6200100
1,2,4-Trichlorobenzene ND ug/L 06/08/21 20:35 120-82-1200100
1,1,1-Trichloroethane ND ug/L 06/08/21 20:35 71-55-650.0 100
1,1,2-Trichloroethane ND ug/L 06/08/21 20:35 79-00-550.0 100
Trichloroethene ND ug/L 06/08/21 20:35 79-01-650.0 100
Trichlorofluoromethane ND ug/L 06/08/21 20:35 75-69-4100100
1,2,3-Trichloropropane ND ug/L 06/08/21 20:35 96-18-450.0 100
1,2,4-Trimethylbenzene 3590 ug/L 06/08/21 20:35 95-63-650.0 100
1,3,5-Trimethylbenzene ND ug/L 06/08/21 20:35 108-67-8 M150.0 100
Vinyl chloride ND ug/L 06/08/21 20:35 75-01-4100100
m&p-Xylene 10300 ug/L 06/08/21 20:35 179601-23-1100100
o-Xylene 4880 ug/L 06/08/21 20:35 95-47-650.0 100
Surrogates
1,2-Dichloroethane-d4 (S)99 %06/08/21 20:35 17060-07-070-130 100
4-Bromofluorobenzene (S)97 %06/08/21 20:35 460-00-470-130 100
Toluene-d8 (S)97 %06/08/21 20:35 2037-26-570-130 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-2 Lab ID:92542712004 Collected:06/07/21 10:05 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 564 ug/L 06/08/21 19:23 71-43-22.5 5
Bromobenzene ND ug/L 06/08/21 19:23 108-86-12.5 5
Bromochloromethane ND ug/L 06/08/21 19:23 74-97-52.5 5
Bromodichloromethane ND ug/L 06/08/21 19:23 75-27-42.5 5
Bromoform ND ug/L 06/08/21 19:23 75-25-22.5 5
Bromomethane ND ug/L 06/08/21 19:23 74-83-925.0 5
n-Butylbenzene ND ug/L 06/08/21 19:23 104-51-82.5 5
sec-Butylbenzene ND ug/L 06/08/21 19:23 135-98-82.5 5
tert-Butylbenzene ND ug/L 06/08/21 19:23 98-06-62.5 5
Carbon tetrachloride ND ug/L 06/08/21 19:23 56-23-52.5 5
Chlorobenzene ND ug/L 06/08/21 19:23 108-90-72.5 5
Chloroethane ND ug/L 06/08/21 19:23 75-00-35.0 5
Chloroform ND ug/L 06/08/21 19:23 67-66-32.5 5
Chloromethane ND ug/L 06/08/21 19:23 74-87-35.0 5
2-Chlorotoluene ND ug/L 06/08/21 19:23 95-49-82.5 5
4-Chlorotoluene ND ug/L 06/08/21 19:23 106-43-42.5 5
1,2-Dibromo-3-chloropropane ND ug/L 06/08/21 19:23 96-12-85.0 5
Dibromochloromethane ND ug/L 06/08/21 19:23 124-48-12.5 5
1,2-Dibromoethane (EDB)ND ug/L 06/08/21 19:23 106-93-42.5 5
Dibromomethane ND ug/L 06/08/21 19:23 74-95-32.5 5
1,2-Dichlorobenzene ND ug/L 06/08/21 19:23 95-50-12.5 5
1,3-Dichlorobenzene ND ug/L 06/08/21 19:23 541-73-12.5 5
1,4-Dichlorobenzene ND ug/L 06/08/21 19:23 106-46-72.5 5
Dichlorodifluoromethane ND ug/L 06/08/21 19:23 75-71-82.5 5
1,1-Dichloroethane ND ug/L 06/08/21 19:23 75-34-32.5 5
1,2-Dichloroethane ND ug/L 06/08/21 19:23 107-06-22.5 5
1,1-Dichloroethene ND ug/L 06/08/21 19:23 75-35-42.5 5
cis-1,2-Dichloroethene ND ug/L 06/08/21 19:23 156-59-22.5 5
trans-1,2-Dichloroethene ND ug/L 06/08/21 19:23 156-60-52.5 5
1,2-Dichloropropane ND ug/L 06/08/21 19:23 78-87-52.5 5
1,3-Dichloropropane ND ug/L 06/08/21 19:23 142-28-92.5 5
2,2-Dichloropropane ND ug/L 06/08/21 19:23 594-20-72.5 5
1,1-Dichloropropene ND ug/L 06/08/21 19:23 563-58-62.5 5
cis-1,3-Dichloropropene ND ug/L 06/08/21 19:23 10061-01-52.5 5
trans-1,3-Dichloropropene ND ug/L 06/08/21 19:23 10061-02-62.5 5
Diisopropyl ether 12.5 ug/L 06/08/21 19:23 108-20-32.5 5
Ethylbenzene ND ug/L 06/08/21 19:23 100-41-42.5 5
Hexachloro-1,3-butadiene ND ug/L 06/08/21 19:23 87-68-310.0 5
Isopropylbenzene (Cumene)10.7 ug/L 06/08/21 19:23 98-82-82.5 5
Methylene Chloride ND ug/L 06/08/21 19:23 75-09-210.0 5
Methyl-tert-butyl ether 7.4 ug/L 06/08/21 19:23 1634-04-42.5 5
Naphthalene 17.8 ug/L 06/08/21 19:23 91-20-310.0 5
n-Propylbenzene ND ug/L 06/08/21 19:23 103-65-12.5 5
Styrene ND ug/L 06/08/21 19:23 100-42-52.5 5
1,1,1,2-Tetrachloroethane ND ug/L 06/08/21 19:23 630-20-62.5 5
1,1,2,2-Tetrachloroethane ND ug/L 06/08/21 19:23 79-34-52.5 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-2 Lab ID:92542712004 Collected:06/07/21 10:05 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 06/08/21 19:23 127-18-42.5 5
Toluene ND ug/L 06/08/21 19:23 108-88-32.5 5
1,2,3-Trichlorobenzene ND ug/L 06/08/21 19:23 87-61-610.0 5
1,2,4-Trichlorobenzene ND ug/L 06/08/21 19:23 120-82-110.0 5
1,1,1-Trichloroethane ND ug/L 06/08/21 19:23 71-55-62.5 5
1,1,2-Trichloroethane ND ug/L 06/08/21 19:23 79-00-52.5 5
Trichloroethene ND ug/L 06/08/21 19:23 79-01-62.5 5
Trichlorofluoromethane ND ug/L 06/08/21 19:23 75-69-45.0 5
1,2,3-Trichloropropane ND ug/L 06/08/21 19:23 96-18-42.5 5
1,2,4-Trimethylbenzene 3.3 ug/L 06/08/21 19:23 95-63-62.5 5
1,3,5-Trimethylbenzene ND ug/L 06/08/21 19:23 108-67-82.5 5
Vinyl chloride ND ug/L 06/08/21 19:23 75-01-45.0 5
m&p-Xylene ND ug/L 06/08/21 19:23 179601-23-15.0 5
o-Xylene 43.3 ug/L 06/08/21 19:23 95-47-62.5 5
Surrogates
1,2-Dichloroethane-d4 (S)101 %06/08/21 19:23 17060-07-070-130 5
4-Bromofluorobenzene (S)99 %06/08/21 19:23 460-00-470-130 5
Toluene-d8 (S)101 %06/08/21 19:23 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-3 Lab ID:92542712005 Collected:06/07/21 10:20 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 211 ug/L 06/10/21 03:27 71-43-21.0 2
Bromobenzene ND ug/L 06/10/21 03:27 108-86-11.0 2
Bromochloromethane ND ug/L 06/10/21 03:27 74-97-51.0 2
Bromodichloromethane ND ug/L 06/10/21 03:27 75-27-41.0 2
Bromoform ND ug/L 06/10/21 03:27 75-25-21.0 2
Bromomethane ND ug/L 06/10/21 03:27 74-83-910.0 2
n-Butylbenzene ND ug/L 06/10/21 03:27 104-51-81.0 2
sec-Butylbenzene ND ug/L 06/10/21 03:27 135-98-81.0 2
tert-Butylbenzene ND ug/L 06/10/21 03:27 98-06-61.0 2
Carbon tetrachloride ND ug/L 06/10/21 03:27 56-23-51.0 2
Chlorobenzene ND ug/L 06/10/21 03:27 108-90-71.0 2
Chloroethane ND ug/L 06/10/21 03:27 75-00-32.0 2
Chloroform ND ug/L 06/10/21 03:27 67-66-31.0 2
Chloromethane ND ug/L 06/10/21 03:27 74-87-32.0 2
2-Chlorotoluene ND ug/L 06/10/21 03:27 95-49-81.0 2
4-Chlorotoluene ND ug/L 06/10/21 03:27 106-43-41.0 2
1,2-Dibromo-3-chloropropane ND ug/L 06/10/21 03:27 96-12-82.0 2
Dibromochloromethane ND ug/L 06/10/21 03:27 124-48-11.0 2
1,2-Dibromoethane (EDB)ND ug/L 06/10/21 03:27 106-93-41.0 2
Dibromomethane ND ug/L 06/10/21 03:27 74-95-31.0 2
1,2-Dichlorobenzene ND ug/L 06/10/21 03:27 95-50-11.0 2
1,3-Dichlorobenzene ND ug/L 06/10/21 03:27 541-73-11.0 2
1,4-Dichlorobenzene ND ug/L 06/10/21 03:27 106-46-71.0 2
Dichlorodifluoromethane ND ug/L 06/10/21 03:27 75-71-81.0 2
1,1-Dichloroethane ND ug/L 06/10/21 03:27 75-34-31.0 2
1,2-Dichloroethane ND ug/L 06/10/21 03:27 107-06-21.0 2
1,1-Dichloroethene ND ug/L 06/10/21 03:27 75-35-41.0 2
cis-1,2-Dichloroethene ND ug/L 06/10/21 03:27 156-59-21.0 2
trans-1,2-Dichloroethene ND ug/L 06/10/21 03:27 156-60-51.0 2
1,2-Dichloropropane ND ug/L 06/10/21 03:27 78-87-51.0 2
1,3-Dichloropropane ND ug/L 06/10/21 03:27 142-28-91.0 2
2,2-Dichloropropane ND ug/L 06/10/21 03:27 594-20-71.0 2
1,1-Dichloropropene ND ug/L 06/10/21 03:27 563-58-61.0 2
cis-1,3-Dichloropropene ND ug/L 06/10/21 03:27 10061-01-51.0 2
trans-1,3-Dichloropropene ND ug/L 06/10/21 03:27 10061-02-61.0 2
Diisopropyl ether 8.6 ug/L 06/10/21 03:27 108-20-31.0 2
Ethylbenzene 1.7 ug/L 06/10/21 03:27 100-41-41.0 2
Hexachloro-1,3-butadiene ND ug/L 06/10/21 03:27 87-68-34.0 2
Isopropylbenzene (Cumene)ND ug/L 06/10/21 03:27 98-82-81.0 2
Methylene Chloride ND ug/L 06/10/21 03:27 75-09-24.0 2
Methyl-tert-butyl ether 2.4 ug/L 06/10/21 03:27 1634-04-41.0 2
Naphthalene ND ug/L 06/10/21 03:27 91-20-34.0 2
n-Propylbenzene ND ug/L 06/10/21 03:27 103-65-11.0 2
Styrene ND ug/L 06/10/21 03:27 100-42-51.0 2
1,1,1,2-Tetrachloroethane ND ug/L 06/10/21 03:27 630-20-61.0 2
1,1,2,2-Tetrachloroethane ND ug/L 06/10/21 03:27 79-34-51.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-3 Lab ID:92542712005 Collected:06/07/21 10:20 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 06/10/21 03:27 127-18-41.0 2
Toluene 7.6 ug/L 06/10/21 03:27 108-88-31.0 2
1,2,3-Trichlorobenzene ND ug/L 06/10/21 03:27 87-61-64.0 2
1,2,4-Trichlorobenzene ND ug/L 06/10/21 03:27 120-82-14.0 2
1,1,1-Trichloroethane ND ug/L 06/10/21 03:27 71-55-61.0 2
1,1,2-Trichloroethane ND ug/L 06/10/21 03:27 79-00-51.0 2
Trichloroethene ND ug/L 06/10/21 03:27 79-01-61.0 2
Trichlorofluoromethane ND ug/L 06/10/21 03:27 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 06/10/21 03:27 96-18-41.0 2
1,2,4-Trimethylbenzene ND ug/L 06/10/21 03:27 95-63-61.0 2
1,3,5-Trimethylbenzene ND ug/L 06/10/21 03:27 108-67-81.0 2
Vinyl chloride ND ug/L 06/10/21 03:27 75-01-42.0 2
m&p-Xylene 6.6 ug/L 06/10/21 03:27 179601-23-12.0 2
o-Xylene 2.1 ug/L 06/10/21 03:27 95-47-61.0 2
Surrogates
1,2-Dichloroethane-d4 (S)108 %06/10/21 03:27 17060-07-070-130 2
4-Bromofluorobenzene (S)100 %06/10/21 03:27 460-00-470-130 2
Toluene-d8 (S)102 %06/10/21 03:27 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-4 Lab ID:92542712006 Collected:06/07/21 10:40 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 4.5 ug/L 06/08/21 16:59 71-43-20.50 1
Bromobenzene ND ug/L 06/08/21 16:59 108-86-10.50 1
Bromochloromethane ND ug/L 06/08/21 16:59 74-97-50.50 1
Bromodichloromethane ND ug/L 06/08/21 16:59 75-27-40.50 1
Bromoform ND ug/L 06/08/21 16:59 75-25-20.50 1
Bromomethane ND ug/L 06/08/21 16:59 74-83-95.0 1
n-Butylbenzene ND ug/L 06/08/21 16:59 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/08/21 16:59 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/08/21 16:59 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/08/21 16:59 56-23-50.50 1
Chlorobenzene ND ug/L 06/08/21 16:59 108-90-70.50 1
Chloroethane ND ug/L 06/08/21 16:59 75-00-31.0 1
Chloroform ND ug/L 06/08/21 16:59 67-66-30.50 1
Chloromethane ND ug/L 06/08/21 16:59 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/08/21 16:59 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/08/21 16:59 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/08/21 16:59 96-12-81.0 1
Dibromochloromethane ND ug/L 06/08/21 16:59 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/08/21 16:59 106-93-40.50 1
Dibromomethane ND ug/L 06/08/21 16:59 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/08/21 16:59 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/08/21 16:59 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/08/21 16:59 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/08/21 16:59 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/08/21 16:59 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/08/21 16:59 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/08/21 16:59 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/08/21 16:59 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/08/21 16:59 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/08/21 16:59 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/08/21 16:59 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/08/21 16:59 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/08/21 16:59 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/08/21 16:59 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/08/21 16:59 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/08/21 16:59 108-20-30.50 1
Ethylbenzene ND ug/L 06/08/21 16:59 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/08/21 16:59 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/08/21 16:59 98-82-80.50 1
Methylene Chloride ND ug/L 06/08/21 16:59 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/08/21 16:59 1634-04-40.50 1
Naphthalene ND ug/L 06/08/21 16:59 91-20-32.0 1
n-Propylbenzene ND ug/L 06/08/21 16:59 103-65-10.50 1
Styrene ND ug/L 06/08/21 16:59 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/08/21 16:59 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/08/21 16:59 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-4 Lab ID:92542712006 Collected:06/07/21 10:40 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 06/08/21 16:59 127-18-40.50 1
Toluene 1.3 ug/L 06/08/21 16:59 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/08/21 16:59 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/08/21 16:59 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/08/21 16:59 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/08/21 16:59 79-00-50.50 1
Trichloroethene ND ug/L 06/08/21 16:59 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/08/21 16:59 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/08/21 16:59 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/08/21 16:59 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/08/21 16:59 108-67-80.50 1
Vinyl chloride ND ug/L 06/08/21 16:59 75-01-41.0 1
m&p-Xylene ND ug/L 06/08/21 16:59 179601-23-11.0 1
o-Xylene ND ug/L 06/08/21 16:59 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %06/08/21 16:59 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %06/08/21 16:59 460-00-470-130 1
Toluene-d8 (S)100 %06/08/21 16:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-5 Lab ID:92542712007 Collected:06/07/21 11:00 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 58.8 ug/L 06/08/21 20:17 71-43-210.0 20
Bromobenzene ND ug/L 06/08/21 20:17 108-86-110.0 20
Bromochloromethane ND ug/L 06/08/21 20:17 74-97-510.0 20
Bromodichloromethane ND ug/L 06/08/21 20:17 75-27-410.0 20
Bromoform ND ug/L 06/08/21 20:17 75-25-210.0 20
Bromomethane ND ug/L 06/08/21 20:17 74-83-910020
n-Butylbenzene ND ug/L 06/08/21 20:17 104-51-810.0 20
sec-Butylbenzene ND ug/L 06/08/21 20:17 135-98-810.0 20
tert-Butylbenzene ND ug/L 06/08/21 20:17 98-06-610.0 20
Carbon tetrachloride ND ug/L 06/08/21 20:17 56-23-510.0 20
Chlorobenzene ND ug/L 06/08/21 20:17 108-90-710.0 20
Chloroethane ND ug/L 06/08/21 20:17 75-00-320.0 20
Chloroform ND ug/L 06/08/21 20:17 67-66-310.0 20
Chloromethane ND ug/L 06/08/21 20:17 74-87-320.0 20
2-Chlorotoluene ND ug/L 06/08/21 20:17 95-49-810.0 20
4-Chlorotoluene ND ug/L 06/08/21 20:17 106-43-410.0 20
1,2-Dibromo-3-chloropropane ND ug/L 06/08/21 20:17 96-12-820.0 20
Dibromochloromethane ND ug/L 06/08/21 20:17 124-48-110.0 20
1,2-Dibromoethane (EDB)ND ug/L 06/08/21 20:17 106-93-410.0 20
Dibromomethane ND ug/L 06/08/21 20:17 74-95-310.0 20
1,2-Dichlorobenzene ND ug/L 06/08/21 20:17 95-50-110.0 20
1,3-Dichlorobenzene ND ug/L 06/08/21 20:17 541-73-110.0 20
1,4-Dichlorobenzene ND ug/L 06/08/21 20:17 106-46-710.0 20
Dichlorodifluoromethane ND ug/L 06/08/21 20:17 75-71-810.0 20
1,1-Dichloroethane ND ug/L 06/08/21 20:17 75-34-310.0 20
1,2-Dichloroethane ND ug/L 06/08/21 20:17 107-06-210.0 20
1,1-Dichloroethene ND ug/L 06/08/21 20:17 75-35-410.0 20
cis-1,2-Dichloroethene ND ug/L 06/08/21 20:17 156-59-210.0 20
trans-1,2-Dichloroethene ND ug/L 06/08/21 20:17 156-60-510.0 20
1,2-Dichloropropane ND ug/L 06/08/21 20:17 78-87-510.0 20
1,3-Dichloropropane ND ug/L 06/08/21 20:17 142-28-910.0 20
2,2-Dichloropropane ND ug/L 06/08/21 20:17 594-20-710.0 20
1,1-Dichloropropene ND ug/L 06/08/21 20:17 563-58-610.0 20
cis-1,3-Dichloropropene ND ug/L 06/08/21 20:17 10061-01-510.0 20
trans-1,3-Dichloropropene ND ug/L 06/08/21 20:17 10061-02-610.0 20
Diisopropyl ether ND ug/L 06/08/21 20:17 108-20-310.0 20
Ethylbenzene 296 ug/L 06/08/21 20:17 100-41-410.0 20
Hexachloro-1,3-butadiene ND ug/L 06/08/21 20:17 87-68-340.0 20
Isopropylbenzene (Cumene)18.4 ug/L 06/08/21 20:17 98-82-810.0 20
Methylene Chloride ND ug/L 06/08/21 20:17 75-09-240.0 20
Methyl-tert-butyl ether ND ug/L 06/08/21 20:17 1634-04-410.0 20
Naphthalene 113 ug/L 06/08/21 20:17 91-20-340.0 20
n-Propylbenzene ND ug/L 06/08/21 20:17 103-65-110.0 20
Styrene ND ug/L 06/08/21 20:17 100-42-510.0 20
1,1,1,2-Tetrachloroethane ND ug/L 06/08/21 20:17 630-20-610.0 20
1,1,2,2-Tetrachloroethane ND ug/L 06/08/21 20:17 79-34-510.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-5 Lab ID:92542712007 Collected:06/07/21 11:00 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 06/08/21 20:17 127-18-410.0 20
Toluene 2070 ug/L 06/08/21 20:17 108-88-310.0 20
1,2,3-Trichlorobenzene ND ug/L 06/08/21 20:17 87-61-640.0 20
1,2,4-Trichlorobenzene ND ug/L 06/08/21 20:17 120-82-140.0 20
1,1,1-Trichloroethane ND ug/L 06/08/21 20:17 71-55-610.0 20
1,1,2-Trichloroethane ND ug/L 06/08/21 20:17 79-00-510.0 20
Trichloroethene ND ug/L 06/08/21 20:17 79-01-610.0 20
Trichlorofluoromethane ND ug/L 06/08/21 20:17 75-69-420.0 20
1,2,3-Trichloropropane ND ug/L 06/08/21 20:17 96-18-410.0 20
1,2,4-Trimethylbenzene 410 ug/L 06/08/21 20:17 95-63-610.0 20
1,3,5-Trimethylbenzene ND ug/L 06/08/21 20:17 108-67-810.0 20
Vinyl chloride ND ug/L 06/08/21 20:17 75-01-420.0 20
m&p-Xylene 1360 ug/L 06/08/21 20:17 179601-23-120.0 20
o-Xylene 850 ug/L 06/08/21 20:17 95-47-610.0 20
Surrogates
1,2-Dichloroethane-d4 (S)100 %06/08/21 20:17 17060-07-070-130 20
4-Bromofluorobenzene (S)99 %06/08/21 20:17 460-00-470-130 20
Toluene-d8 (S)100 %06/08/21 20:17 2037-26-570-130 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-6 Lab ID:92542712008 Collected:06/07/21 11:15 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 06/08/21 16:05 71-43-20.50 1
Bromobenzene ND ug/L 06/08/21 16:05 108-86-10.50 1
Bromochloromethane ND ug/L 06/08/21 16:05 74-97-50.50 1
Bromodichloromethane ND ug/L 06/08/21 16:05 75-27-40.50 1
Bromoform ND ug/L 06/08/21 16:05 75-25-20.50 1
Bromomethane ND ug/L 06/08/21 16:05 74-83-95.0 1
n-Butylbenzene ND ug/L 06/08/21 16:05 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/08/21 16:05 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/08/21 16:05 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/08/21 16:05 56-23-50.50 1
Chlorobenzene ND ug/L 06/08/21 16:05 108-90-70.50 1
Chloroethane ND ug/L 06/08/21 16:05 75-00-31.0 1
Chloroform ND ug/L 06/08/21 16:05 67-66-30.50 1
Chloromethane ND ug/L 06/08/21 16:05 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/08/21 16:05 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/08/21 16:05 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/08/21 16:05 96-12-81.0 1
Dibromochloromethane ND ug/L 06/08/21 16:05 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/08/21 16:05 106-93-40.50 1
Dibromomethane ND ug/L 06/08/21 16:05 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/08/21 16:05 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/08/21 16:05 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/08/21 16:05 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/08/21 16:05 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/08/21 16:05 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/08/21 16:05 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/08/21 16:05 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/08/21 16:05 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/08/21 16:05 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/08/21 16:05 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/08/21 16:05 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/08/21 16:05 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/08/21 16:05 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/08/21 16:05 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/08/21 16:05 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/08/21 16:05 108-20-30.50 1
Ethylbenzene ND ug/L 06/08/21 16:05 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/08/21 16:05 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/08/21 16:05 98-82-80.50 1
Methylene Chloride ND ug/L 06/08/21 16:05 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/08/21 16:05 1634-04-40.50 1
Naphthalene ND ug/L 06/08/21 16:05 91-20-32.0 1
n-Propylbenzene ND ug/L 06/08/21 16:05 103-65-10.50 1
Styrene ND ug/L 06/08/21 16:05 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/08/21 16:05 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/08/21 16:05 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-6 Lab ID:92542712008 Collected:06/07/21 11:15 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 06/08/21 16:05 127-18-40.50 1
Toluene ND ug/L 06/08/21 16:05 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/08/21 16:05 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/08/21 16:05 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/08/21 16:05 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/08/21 16:05 79-00-50.50 1
Trichloroethene ND ug/L 06/08/21 16:05 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/08/21 16:05 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/08/21 16:05 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/08/21 16:05 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/08/21 16:05 108-67-80.50 1
Vinyl chloride ND ug/L 06/08/21 16:05 75-01-41.0 1
m&p-Xylene ND ug/L 06/08/21 16:05 179601-23-11.0 1
o-Xylene ND ug/L 06/08/21 16:05 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %06/08/21 16:05 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/08/21 16:05 460-00-470-130 1
Toluene-d8 (S)98 %06/08/21 16:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-7 Lab ID:92542712009 Collected:06/07/21 11:35 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 06/08/21 16:23 71-43-20.50 1
Bromobenzene ND ug/L 06/08/21 16:23 108-86-10.50 1
Bromochloromethane ND ug/L 06/08/21 16:23 74-97-50.50 1
Bromodichloromethane ND ug/L 06/08/21 16:23 75-27-40.50 1
Bromoform ND ug/L 06/08/21 16:23 75-25-20.50 1
Bromomethane ND ug/L 06/08/21 16:23 74-83-95.0 1
n-Butylbenzene ND ug/L 06/08/21 16:23 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/08/21 16:23 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/08/21 16:23 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/08/21 16:23 56-23-50.50 1
Chlorobenzene ND ug/L 06/08/21 16:23 108-90-70.50 1
Chloroethane ND ug/L 06/08/21 16:23 75-00-31.0 1
Chloroform ND ug/L 06/08/21 16:23 67-66-30.50 1
Chloromethane ND ug/L 06/08/21 16:23 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/08/21 16:23 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/08/21 16:23 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/08/21 16:23 96-12-81.0 1
Dibromochloromethane ND ug/L 06/08/21 16:23 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/08/21 16:23 106-93-40.50 1
Dibromomethane ND ug/L 06/08/21 16:23 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/08/21 16:23 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/08/21 16:23 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/08/21 16:23 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/08/21 16:23 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/08/21 16:23 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/08/21 16:23 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/08/21 16:23 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/08/21 16:23 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/08/21 16:23 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/08/21 16:23 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/08/21 16:23 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/08/21 16:23 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/08/21 16:23 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/08/21 16:23 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/08/21 16:23 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/08/21 16:23 108-20-30.50 1
Ethylbenzene ND ug/L 06/08/21 16:23 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/08/21 16:23 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/08/21 16:23 98-82-80.50 1
Methylene Chloride ND ug/L 06/08/21 16:23 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/08/21 16:23 1634-04-40.50 1
Naphthalene ND ug/L 06/08/21 16:23 91-20-32.0 1
n-Propylbenzene ND ug/L 06/08/21 16:23 103-65-10.50 1
Styrene ND ug/L 06/08/21 16:23 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/08/21 16:23 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/08/21 16:23 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-7 Lab ID:92542712009 Collected:06/07/21 11:35 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 06/08/21 16:23 127-18-40.50 1
Toluene ND ug/L 06/08/21 16:23 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/08/21 16:23 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/08/21 16:23 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/08/21 16:23 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/08/21 16:23 79-00-50.50 1
Trichloroethene ND ug/L 06/08/21 16:23 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/08/21 16:23 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/08/21 16:23 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/08/21 16:23 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/08/21 16:23 108-67-80.50 1
Vinyl chloride ND ug/L 06/08/21 16:23 75-01-41.0 1
m&p-Xylene ND ug/L 06/08/21 16:23 179601-23-11.0 1
o-Xylene ND ug/L 06/08/21 16:23 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %06/08/21 16:23 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %06/08/21 16:23 460-00-470-130 1
Toluene-d8 (S)99 %06/08/21 16:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-8 Lab ID:92542712010 Collected:06/07/21 11:50 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 06/08/21 16:41 71-43-20.50 1
Bromobenzene ND ug/L 06/08/21 16:41 108-86-10.50 1
Bromochloromethane ND ug/L 06/08/21 16:41 74-97-50.50 1
Bromodichloromethane ND ug/L 06/08/21 16:41 75-27-40.50 1
Bromoform ND ug/L 06/08/21 16:41 75-25-20.50 1
Bromomethane ND ug/L 06/08/21 16:41 74-83-95.0 1
n-Butylbenzene ND ug/L 06/08/21 16:41 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/08/21 16:41 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/08/21 16:41 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/08/21 16:41 56-23-50.50 1
Chlorobenzene ND ug/L 06/08/21 16:41 108-90-70.50 1
Chloroethane ND ug/L 06/08/21 16:41 75-00-31.0 1
Chloroform ND ug/L 06/08/21 16:41 67-66-30.50 1
Chloromethane ND ug/L 06/08/21 16:41 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/08/21 16:41 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/08/21 16:41 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/08/21 16:41 96-12-81.0 1
Dibromochloromethane ND ug/L 06/08/21 16:41 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/08/21 16:41 106-93-40.50 1
Dibromomethane ND ug/L 06/08/21 16:41 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/08/21 16:41 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/08/21 16:41 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/08/21 16:41 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/08/21 16:41 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/08/21 16:41 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/08/21 16:41 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/08/21 16:41 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/08/21 16:41 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/08/21 16:41 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/08/21 16:41 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/08/21 16:41 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/08/21 16:41 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/08/21 16:41 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/08/21 16:41 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/08/21 16:41 10061-02-60.50 1
Diisopropyl ether 0.59 ug/L 06/08/21 16:41 108-20-30.50 1
Ethylbenzene ND ug/L 06/08/21 16:41 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/08/21 16:41 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/08/21 16:41 98-82-80.50 1
Methylene Chloride ND ug/L 06/08/21 16:41 75-09-22.0 1
Methyl-tert-butyl ether 0.75 ug/L 06/08/21 16:41 1634-04-40.50 1
Naphthalene ND ug/L 06/08/21 16:41 91-20-32.0 1
n-Propylbenzene ND ug/L 06/08/21 16:41 103-65-10.50 1
Styrene ND ug/L 06/08/21 16:41 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/08/21 16:41 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/08/21 16:41 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Sample:MW-8 Lab ID:92542712010 Collected:06/07/21 11:50 Received:06/07/21 12:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 06/08/21 16:41 127-18-40.50 1
Toluene ND ug/L 06/08/21 16:41 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/08/21 16:41 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/08/21 16:41 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/08/21 16:41 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/08/21 16:41 79-00-50.50 1
Trichloroethene ND ug/L 06/08/21 16:41 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/08/21 16:41 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/08/21 16:41 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/08/21 16:41 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/08/21 16:41 108-67-80.50 1
Vinyl chloride ND ug/L 06/08/21 16:41 75-01-41.0 1
m&p-Xylene ND ug/L 06/08/21 16:41 179601-23-11.0 1
o-Xylene ND ug/L 06/08/21 16:41 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %06/08/21 16:41 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/08/21 16:41 460-00-470-130 1
Toluene-d8 (S)98 %06/08/21 16:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
625574
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92542712001, 92542712002, 92542712003, 92542712004, 92542712006, 92542712007, 92542712008,
92542712009, 92542712010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3289530
Associated Lab Samples:92542712001, 92542712002, 92542712003, 92542712004, 92542712006, 92542712007, 92542712008,
92542712009, 92542712010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/08/21 14:17
1,1,1-Trichloroethane ug/L ND 0.50 06/08/21 14:17
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/08/21 14:17
1,1,2-Trichloroethane ug/L ND 0.50 06/08/21 14:17
1,1-Dichloroethane ug/L ND 0.50 06/08/21 14:17
1,1-Dichloroethene ug/L ND 0.50 06/08/21 14:17
1,1-Dichloropropene ug/L ND 0.50 06/08/21 14:17
1,2,3-Trichlorobenzene ug/L ND 2.0 06/08/21 14:17
1,2,3-Trichloropropane ug/L ND 0.50 06/08/21 14:17
1,2,4-Trichlorobenzene ug/L ND 2.0 06/08/21 14:17
1,2,4-Trimethylbenzene ug/L ND 0.50 06/08/21 14:17
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/08/21 14:17
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/08/21 14:17
1,2-Dichlorobenzene ug/L ND 0.50 06/08/21 14:17
1,2-Dichloroethane ug/L ND 0.50 06/08/21 14:17
1,2-Dichloropropane ug/L ND 0.50 06/08/21 14:17
1,3,5-Trimethylbenzene ug/L ND 0.50 06/08/21 14:17
1,3-Dichlorobenzene ug/L ND 0.50 06/08/21 14:17
1,3-Dichloropropane ug/L ND 0.50 06/08/21 14:17
1,4-Dichlorobenzene ug/L ND 0.50 06/08/21 14:17
2,2-Dichloropropane ug/L ND 0.50 06/08/21 14:17
2-Chlorotoluene ug/L ND 0.50 06/08/21 14:17
4-Chlorotoluene ug/L ND 0.50 06/08/21 14:17
Benzene ug/L ND 0.50 06/08/21 14:17
Bromobenzene ug/L ND 0.50 06/08/21 14:17
Bromochloromethane ug/L ND 0.50 06/08/21 14:17
Bromodichloromethane ug/L ND 0.50 06/08/21 14:17
Bromoform ug/L ND 0.50 06/08/21 14:17
Bromomethane ug/L ND 5.0 06/08/21 14:17
Carbon tetrachloride ug/L ND 0.50 06/08/21 14:17
Chlorobenzene ug/L ND 0.50 06/08/21 14:17
Chloroethane ug/L ND 1.0 06/08/21 14:17
Chloroform ug/L ND 0.50 06/08/21 14:17
Chloromethane ug/L ND 1.0 06/08/21 14:17
cis-1,2-Dichloroethene ug/L ND 0.50 06/08/21 14:17
cis-1,3-Dichloropropene ug/L ND 0.50 06/08/21 14:17
Dibromochloromethane ug/L ND 0.50 06/08/21 14:17
Dibromomethane ug/L ND 0.50 06/08/21 14:17
Dichlorodifluoromethane ug/L ND 0.50 06/08/21 14:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3289530
Associated Lab Samples:92542712001, 92542712002, 92542712003, 92542712004, 92542712006, 92542712007, 92542712008,
92542712009, 92542712010
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 0.50 06/08/21 14:17
Ethylbenzene ug/L ND 0.50 06/08/21 14:17
Hexachloro-1,3-butadiene ug/L ND 2.0 06/08/21 14:17
Isopropylbenzene (Cumene)ug/L ND 0.50 06/08/21 14:17
m&p-Xylene ug/L ND 1.0 06/08/21 14:17
Methyl-tert-butyl ether ug/L ND 0.50 06/08/21 14:17
Methylene Chloride ug/L ND 2.0 06/08/21 14:17
n-Butylbenzene ug/L ND 0.50 06/08/21 14:17
n-Propylbenzene ug/L ND 0.50 06/08/21 14:17
Naphthalene ug/L ND 2.0 06/08/21 14:17
o-Xylene ug/L ND 0.50 06/08/21 14:17
sec-Butylbenzene ug/L ND 0.50 06/08/21 14:17
Styrene ug/L ND 0.50 06/08/21 14:17
tert-Butylbenzene ug/L ND 0.50 06/08/21 14:17
Tetrachloroethene ug/L ND 0.50 06/08/21 14:17
Toluene ug/L ND 0.50 06/08/21 14:17
trans-1,2-Dichloroethene ug/L ND 0.50 06/08/21 14:17
trans-1,3-Dichloropropene ug/L ND 0.50 06/08/21 14:17
Trichloroethene ug/L ND 0.50 06/08/21 14:17
Trichlorofluoromethane ug/L ND 1.0 06/08/21 14:17
Vinyl chloride ug/L ND 1.0 06/08/21 14:17
1,2-Dichloroethane-d4 (S)%100 70-130 06/08/21 14:17
4-Bromofluorobenzene (S)%101 70-130 06/08/21 14:17
Toluene-d8 (S)%101 70-130 06/08/21 14:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3289531LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.150 102 60-140
1,1,1-Trichloroethane ug/L 48.750 97 60-140
1,1,2,2-Tetrachloroethane ug/L 49.850 100 60-140
1,1,2-Trichloroethane ug/L 49.150 98 60-140
1,1-Dichloroethane ug/L 50.150 100 60-140
1,1-Dichloroethene ug/L 50.150 100 60-140
1,1-Dichloropropene ug/L 50.650 101 60-140
1,2,3-Trichlorobenzene ug/L 52.550 105 60-140
1,2,3-Trichloropropane ug/L 48.150 96 60-140
1,2,4-Trichlorobenzene ug/L 52.150 104 60-140
1,2,4-Trimethylbenzene ug/L 50.950 102 60-140
1,2-Dibromo-3-chloropropane ug/L 52.150 104 60-140
1,2-Dibromoethane (EDB)ug/L 51.150 102 60-140
1,2-Dichlorobenzene ug/L 50.750 101 60-140
1,2-Dichloroethane ug/L 43.850 88 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3289531LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 48.850 98 60-140
1,3,5-Trimethylbenzene ug/L 50.850 102 60-140
1,3-Dichlorobenzene ug/L 50.450 101 60-140
1,3-Dichloropropane ug/L 51.050 102 60-140
1,4-Dichlorobenzene ug/L 50.150 100 60-140
2,2-Dichloropropane ug/L 53.050 106 60-140
2-Chlorotoluene ug/L 52.850 106 60-140
4-Chlorotoluene ug/L 51.050 102 60-140
Benzene ug/L 48.050 96 60-140
Bromobenzene ug/L 50.150 100 60-140
Bromochloromethane ug/L 47.250 94 60-140
Bromodichloromethane ug/L 47.350 95 60-140
Bromoform ug/L 53.050 106 60-140
Bromomethane ug/L 43.750 87 60-140
Carbon tetrachloride ug/L 47.750 95 60-140
Chlorobenzene ug/L 48.350 97 60-140
Chloroethane ug/L 41.550 83 60-140
Chloroform ug/L 46.550 93 60-140
Chloromethane ug/L 43.750 87 60-140
cis-1,2-Dichloroethene ug/L 46.550 93 60-140
cis-1,3-Dichloropropene ug/L 51.850 104 60-140
Dibromochloromethane ug/L 53.150 106 60-140
Dibromomethane ug/L 47.050 94 60-140
Dichlorodifluoromethane ug/L 32.750 65 60-140
Diisopropyl ether ug/L 49.950 100 60-140
Ethylbenzene ug/L 49.150 98 60-140
Hexachloro-1,3-butadiene ug/L 49.750 99 60-140
Isopropylbenzene (Cumene)ug/L 50.250 100 60-140
m&p-Xylene ug/L 96.9100 97 60-140
Methyl-tert-butyl ether ug/L 49.050 98 60-140
Methylene Chloride ug/L 50.150 100 60-140
n-Butylbenzene ug/L 52.750 105 60-140
n-Propylbenzene ug/L 51.650 103 60-140
Naphthalene ug/L 53.950 108 60-140
o-Xylene ug/L 48.250 96 60-140
sec-Butylbenzene ug/L 50.350 101 60-140
Styrene ug/L 50.250 100 60-140
tert-Butylbenzene ug/L 42.250 84 60-140
Tetrachloroethene ug/L 47.250 94 60-140
Toluene ug/L 48.150 96 60-140
trans-1,2-Dichloroethene ug/L 49.650 99 60-140
trans-1,3-Dichloropropene ug/L 51.350 103 60-140
Trichloroethene ug/L 48.550 97 60-140
Trichlorofluoromethane ug/L 37.850 76 60-140
Vinyl chloride ug/L 41.650 83 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3289531LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3289532MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92542712003
3289533
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2000 112 60-140112 02000ND22402250
1,1,1-Trichloroethane ug/L 2000 115 60-140119 42000ND22902380
1,1,2,2-Tetrachloroethane ug/L 2000 108 60-140105 22000ND21502110
1,1,2-Trichloroethane ug/L 2000 106 60-140111 52000ND21102210
1,1-Dichloroethane ug/L 2000 116 60-140117 12000ND23102350
1,1-Dichloroethene ug/L 2000 120 60-140121 12000ND24002420
1,1-Dichloropropene ug/L 2000 122 60-140123 12000ND24402470
1,2,3-Trichlorobenzene ug/L 2000 109 60-140103 52000ND21802070
1,2,3-Trichloropropane ug/L 2000 108 60-140104 32000ND21502080
1,2,4-Trichlorobenzene ug/L 2000 112 60-140104 72000ND22302090
1,2,4-Trimethylbenzene ug/L 2000 114 60-140106 22000359058605720
1,2-Dibromo-3-chloropropane ug/L 2000 98 60-140101 42000ND19502030
1,2-Dibromoethane (EDB)ug/L 2000 115 60-140107 72000ND22902140
1,2-Dichlorobenzene ug/L 2000 113 60-140108 52000ND22702160
1,2-Dichloroethane ug/L 2000 98 60-14099 22000ND19501980
1,2-Dichloropropane ug/L 2000 112 60-140114 22000ND22502280
1,3,5-Trimethylbenzene ug/L M1200016060-140156 32000ND32103110
1,3-Dichlorobenzene ug/L 2000 113 60-140109 32000ND22502170
1,3-Dichloropropane ug/L 2000 114 60-140110 32000ND22902210
1,4-Dichlorobenzene ug/L 2000 112 60-140106 62000ND22302110
2,2-Dichloropropane ug/L 2000 106 60-140106 02000ND21102120
2-Chlorotoluene ug/L 2000 124 60-140118 52000ND24802360
4-Chlorotoluene ug/L 2000 117 60-140110 62000ND23402210
Benzene ug/L 2000 122 60-140125 1200097601220012300
Bromobenzene ug/L 2000 112 60-140108 32000ND22402160
Bromochloromethane ug/L 2000 109 60-140110 12000ND21902200
Bromodichloromethane ug/L 2000 103 60-140105 22000ND20702100
Bromoform ug/L 2000 102 60-14099 32000ND20501980
Bromomethane ug/L 2000 98 60-140103 52000ND19602060
Carbon tetrachloride ug/L 2000 114 60-140111 32000ND22802220
Chlorobenzene ug/L 2000 113 60-140109 32000ND22602190
Chloroethane ug/L 2000 102 60-140105 22000ND20502100
Chloroform ug/L 2000 109 60-140112 32000ND21802240
Chloromethane ug/L 2000 95 60-14093 22000ND19301900
cis-1,2-Dichloroethene ug/L 2000 108 60-140110 22000ND21602200
cis-1,3-Dichloropropene ug/L 2000 112 60-140112 02000ND22502240
Dibromochloromethane ug/L 2000 112 60-140105 62000ND22402110
Dibromomethane ug/L 2000 102 60-140102 12000ND20302050
Dichlorodifluoromethane ug/L 2000 82 60-14082 02000ND16401640
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3289532MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92542712003
3289533
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diisopropyl ether ug/L 2000 107 60-140109 1200046626102640
Ethylbenzene ug/L 2000 120 60-140112 32000306054605290
Hexachloro-1,3-butadiene ug/L 2000 112 60-140101 102000ND22502030
Isopropylbenzene (Cumene)ug/L 2000 118 60-140110 7200013525002330
m&p-Xylene ug/L 4000 121 60-140111 34000103001520014800
Methyl-tert-butyl ether ug/L 2000 108 60-140109 1200030824602490
Methylene Chloride ug/L 2000 116 60-140116 02000ND23302320
n-Butylbenzene ug/L 2000 123 60-140115 72000ND24602290
n-Propylbenzene ug/L 2000 137 60-140134 32000ND27502670
Naphthalene ug/L 2000 107 60-140105 1200092330703030
o-Xylene ug/L 2000 121 60-140115 22000488073007180
sec-Butylbenzene ug/L 2000 117 60-140111 52000ND23402230
Styrene ug/L 2000 117 60-140112 42000ND23602260
tert-Butylbenzene ug/L 2000 97 60-14092 52000ND19401840
Tetrachloroethene ug/L 2000 111 60-140104 72000ND22202070
Toluene ug/L 2000 115 60-140115 02000110001330013300
trans-1,2-Dichloroethene ug/L 2000 118 60-140118 02000ND23502360
trans-1,3-Dichloropropene ug/L 2000 109 60-140107 22000ND21802140
Trichloroethene ug/L 2000 111 60-140113 22000ND22102270
Trichlorofluoromethane ug/L 2000 98 60-14098 02000ND19601970
Vinyl chloride ug/L 2000 96 60-14099 32000ND19101970
1,2-Dichloroethane-d4 (S)%97 70-13098
4-Bromofluorobenzene (S)%100 70-13099
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
625887
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92542712005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3290960
Associated Lab Samples:92542712005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/09/21 22:02
1,1,1-Trichloroethane ug/L ND 0.50 06/09/21 22:02
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/09/21 22:02
1,1,2-Trichloroethane ug/L ND 0.50 06/09/21 22:02
1,1-Dichloroethane ug/L ND 0.50 06/09/21 22:02
1,1-Dichloroethene ug/L ND 0.50 06/09/21 22:02
1,1-Dichloropropene ug/L ND 0.50 06/09/21 22:02
1,2,3-Trichlorobenzene ug/L ND 2.0 06/09/21 22:02
1,2,3-Trichloropropane ug/L ND 0.50 06/09/21 22:02
1,2,4-Trichlorobenzene ug/L ND 2.0 06/09/21 22:02
1,2,4-Trimethylbenzene ug/L ND 0.50 06/09/21 22:02
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/09/21 22:02
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/09/21 22:02
1,2-Dichlorobenzene ug/L ND 0.50 06/09/21 22:02
1,2-Dichloroethane ug/L ND 0.50 06/09/21 22:02
1,2-Dichloropropane ug/L ND 0.50 06/09/21 22:02
1,3,5-Trimethylbenzene ug/L ND 0.50 06/09/21 22:02
1,3-Dichlorobenzene ug/L ND 0.50 06/09/21 22:02
1,3-Dichloropropane ug/L ND 0.50 06/09/21 22:02
1,4-Dichlorobenzene ug/L ND 0.50 06/09/21 22:02
2,2-Dichloropropane ug/L ND 0.50 06/09/21 22:02
2-Chlorotoluene ug/L ND 0.50 06/09/21 22:02
4-Chlorotoluene ug/L ND 0.50 06/09/21 22:02
Benzene ug/L ND 0.50 06/09/21 22:02
Bromobenzene ug/L ND 0.50 06/09/21 22:02
Bromochloromethane ug/L ND 0.50 06/09/21 22:02
Bromodichloromethane ug/L ND 0.50 06/09/21 22:02
Bromoform ug/L ND 0.50 06/09/21 22:02
Bromomethane ug/L ND 5.0 06/09/21 22:02
Carbon tetrachloride ug/L ND 0.50 06/09/21 22:02
Chlorobenzene ug/L ND 0.50 06/09/21 22:02
Chloroethane ug/L ND 1.0 06/09/21 22:02
Chloroform ug/L ND 0.50 06/09/21 22:02
Chloromethane ug/L ND 1.0 06/09/21 22:02
cis-1,2-Dichloroethene ug/L ND 0.50 06/09/21 22:02
cis-1,3-Dichloropropene ug/L ND 0.50 06/09/21 22:02
Dibromochloromethane ug/L ND 0.50 06/09/21 22:02
Dibromomethane ug/L ND 0.50 06/09/21 22:02
Dichlorodifluoromethane ug/L ND 0.50 06/09/21 22:02
Diisopropyl ether ug/L ND 0.50 06/09/21 22:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3290960
Associated Lab Samples:92542712005
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 06/09/21 22:02
Hexachloro-1,3-butadiene ug/L ND 2.0 06/09/21 22:02
Isopropylbenzene (Cumene)ug/L ND 0.50 06/09/21 22:02
m&p-Xylene ug/L ND 1.0 06/09/21 22:02
Methyl-tert-butyl ether ug/L ND 0.50 06/09/21 22:02
Methylene Chloride ug/L ND 2.0 06/09/21 22:02
n-Butylbenzene ug/L ND 0.50 06/09/21 22:02
n-Propylbenzene ug/L ND 0.50 06/09/21 22:02
Naphthalene ug/L ND 2.0 06/09/21 22:02
o-Xylene ug/L ND 0.50 06/09/21 22:02
sec-Butylbenzene ug/L ND 0.50 06/09/21 22:02
Styrene ug/L ND 0.50 06/09/21 22:02
tert-Butylbenzene ug/L ND 0.50 06/09/21 22:02
Tetrachloroethene ug/L ND 0.50 06/09/21 22:02
Toluene ug/L ND 0.50 06/09/21 22:02
trans-1,2-Dichloroethene ug/L ND 0.50 06/09/21 22:02
trans-1,3-Dichloropropene ug/L ND 0.50 06/09/21 22:02
Trichloroethene ug/L ND 0.50 06/09/21 22:02
Trichlorofluoromethane ug/L ND 1.0 06/09/21 22:02
Vinyl chloride ug/L ND 1.0 06/09/21 22:02
1,2-Dichloroethane-d4 (S)%111 70-130 06/09/21 22:02
4-Bromofluorobenzene (S)%102 70-130 06/09/21 22:02
Toluene-d8 (S)%102 70-130 06/09/21 22:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3290961LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.850 98 60-140
1,1,1-Trichloroethane ug/L 50.050 100 60-140
1,1,2,2-Tetrachloroethane ug/L 50.650 101 60-140
1,1,2-Trichloroethane ug/L 48.650 97 60-140
1,1-Dichloroethane ug/L 49.250 98 60-140
1,1-Dichloroethene ug/L 49.850 100 60-140
1,1-Dichloropropene ug/L 49.350 99 60-140
1,2,3-Trichlorobenzene ug/L 54.950 110 60-140
1,2,3-Trichloropropane ug/L 52.250 104 60-140
1,2,4-Trichlorobenzene ug/L 54.050 108 60-140
1,2,4-Trimethylbenzene ug/L 51.250 102 60-140
1,2-Dibromo-3-chloropropane ug/L 54.550 109 60-140
1,2-Dibromoethane (EDB)ug/L 50.950 102 60-140
1,2-Dichlorobenzene ug/L 50.150 100 60-140
1,2-Dichloroethane ug/L 46.450 93 60-140
1,2-Dichloropropane ug/L 47.250 94 60-140
1,3,5-Trimethylbenzene ug/L 49.950 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3290961LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 49.950 100 60-140
1,3-Dichloropropane ug/L 51.250 102 60-140
1,4-Dichlorobenzene ug/L 50.250 100 60-140
2,2-Dichloropropane ug/L 52.450 105 60-140
2-Chlorotoluene ug/L 51.150 102 60-140
4-Chlorotoluene ug/L 49.950 100 60-140
Benzene ug/L 46.450 93 60-140
Bromobenzene ug/L 47.950 96 60-140
Bromochloromethane ug/L 47.350 95 60-140
Bromodichloromethane ug/L 45.150 90 60-140
Bromoform ug/L 50.450 101 60-140
Bromomethane ug/L 48.650 97 60-140
Carbon tetrachloride ug/L 48.650 97 60-140
Chlorobenzene ug/L 48.350 97 60-140
Chloroethane ug/L 40.850 82 60-140
Chloroform ug/L 47.950 96 60-140
Chloromethane ug/L 44.250 88 60-140
cis-1,2-Dichloroethene ug/L 47.750 95 60-140
cis-1,3-Dichloropropene ug/L 49.050 98 60-140
Dibromochloromethane ug/L 53.150 106 60-140
Dibromomethane ug/L 46.950 94 60-140
Dichlorodifluoromethane ug/L 51.750 103 60-140
Diisopropyl ether ug/L 48.350 97 60-140
Ethylbenzene ug/L 48.950 98 60-140
Hexachloro-1,3-butadiene ug/L 51.050 102 60-140
Isopropylbenzene (Cumene)ug/L 51.050 102 60-140
m&p-Xylene ug/L 99.5100 99 60-140
Methyl-tert-butyl ether ug/L 49.650 99 60-140
Methylene Chloride ug/L 50.350 101 60-140
n-Butylbenzene ug/L 51.950 104 60-140
n-Propylbenzene ug/L 49.450 99 60-140
Naphthalene ug/L 57.750 115 60-140
o-Xylene ug/L 48.450 97 60-140
sec-Butylbenzene ug/L 49.950 100 60-140
Styrene ug/L 50.450 101 60-140
tert-Butylbenzene ug/L 42.450 85 60-140
Tetrachloroethene ug/L 47.550 95 60-140
Toluene ug/L 46.250 92 60-140
trans-1,2-Dichloroethene ug/L 49.250 98 60-140
trans-1,3-Dichloropropene ug/L 50.450 101 60-140
Trichloroethene ug/L 46.850 94 60-140
Trichlorofluoromethane ug/L 43.950 88 60-140
Vinyl chloride ug/L 43.950 88 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3291132MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92542668038
3291133
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 102 60-140102 0200ND203204
1,1,1-Trichloroethane ug/L 200 111 60-140112 1200ND221224
1,1,2,2-Tetrachloroethane ug/L 200 100 60-140101 1200ND201202
1,1,2-Trichloroethane ug/L 200 102 60-140102 0200ND204204
1,1-Dichloroethane ug/L 200 110 60-140109 1200ND221219
1,1-Dichloroethene ug/L 200 115 60-140115 1200ND230231
1,1-Dichloropropene ug/L 200 110 60-140111 1200ND221222
1,2,3-Trichlorobenzene ug/L 200 96 60-140121 23200ND193242
1,2,3-Trichloropropane ug/L 200 101 60-140103 2200ND202207
1,2,4-Trichlorobenzene ug/L 200 98 60-140115 16200ND196231
1,2,4-Trimethylbenzene ug/L 200 104 60-140107 220029.0 237 243
1,2-Dibromo-3-chloropropane ug/L 200 93 60-14097 5200ND186194
1,2-Dibromoethane (EDB)ug/L 200 100 60-140103 3200ND201207
1,2-Dichlorobenzene ug/L 200 98 60-140101 3200ND196202
1,2-Dichloroethane ug/L 200 98 60-14097 1200ND196194
1,2-Dichloropropane ug/L 200 104 60-140105 1200ND208211
1,3,5-Trimethylbenzene ug/L 200 111 60-140113 2200ND221225
1,3-Dichlorobenzene ug/L 200 99 60-140101 2200ND199202
1,3-Dichloropropane ug/L 200 107 60-140107 1200ND215213
1,4-Dichlorobenzene ug/L 200 99 60-140101 3200ND197203
2,2-Dichloropropane ug/L 200 84 60-14082 3200ND169163
2-Chlorotoluene ug/L 200 106 60-140107 1200ND213214
4-Chlorotoluene ug/L 200 103 60-140104 0200ND207207
Benzene ug/L 200 111 60-140109 0200100012201220
Bromobenzene ug/L 200 98 60-14099 0200ND196197
Bromochloromethane ug/L 200 102 60-140101 1200ND204202
Bromodichloromethane ug/L 200 96 60-14097 0200ND193193
Bromoform ug/L 200 93 60-14097 4200ND187194
Bromomethane ug/L 200 109 60-140122 11200ND219243
Carbon tetrachloride ug/L 200 111 60-140107 3200ND222215
Chlorobenzene ug/L 200 103 60-140103 0200ND207206
Chloroethane ug/L 200 103 60-140105 2200ND206210
Chloroform ug/L 200 104 60-140103 0200ND207207
Chloromethane ug/L 200 103 60-140103 0200ND206206
cis-1,2-Dichloroethene ug/L 200 107 60-140106 1200ND214211
cis-1,3-Dichloropropene ug/L 200 96 60-14097 0200ND193193
Dibromochloromethane ug/L 200 106 60-140107 1200ND212214
Dibromomethane ug/L 200 97 60-14099 2200ND194198
Dichlorodifluoromethane ug/L 200 105 60-140105 0200ND210209
Diisopropyl ether ug/L 200 107 60-140106 0200356569568
Ethylbenzene ug/L 200 107 60-140108 1200110325326
Hexachloro-1,3-butadiene ug/L 200 98 60-140116 17200ND196232
Isopropylbenzene (Cumene)ug/L 200 111 60-140112 12007.2 228 231
m&p-Xylene ug/L 400 106 60-140106 040047.8 471 472
Methyl-tert-butyl ether ug/L 200 103 60-140101 12007.5 213 210
Methylene Chloride ug/L 200 113 60-140109 3200ND226219
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3291132MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92542668038
3291133
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 200 103 60-140111 8200ND206222
n-Propylbenzene ug/L 200 103 60-140104 120016.9 223 224
Naphthalene ug/L 200 95 60-140120 1920044.4 234 283
o-Xylene ug/L 200 103 60-140104 120029.2 236 238
sec-Butylbenzene ug/L 200 106 60-140110 3200ND213220
Styrene ug/L 200 103 60-140104 0200ND207207
tert-Butylbenzene ug/L 200 91 60-14093 2200ND182185
Tetrachloroethene ug/L 200 104 60-140103 1200ND209207
Toluene ug/L 200 101 60-140101 020025.8 228 227
trans-1,2-Dichloroethene ug/L 200 111 60-140109 2200ND222218
trans-1,3-Dichloropropene ug/L 200 95 60-14096 2200ND190193
Trichloroethene ug/L 200 103 60-140103 0200ND206206
Trichlorofluoromethane ug/L 200 112 60-140109 2200ND224219
Vinyl chloride ug/L 200 98 60-14099 1200ND197198
1,2-Dichloroethane-d4 (S)%110 70-130110
4-Bromofluorobenzene (S)%103 70-130104
Toluene-d8 (S)%102 70-130102
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92542712
The Spot 6/7/21
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
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Page 34 of 38
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92542712
The Spot 6/7/21
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92542712001 625574WSW-1 SM 6200B
92542712002 625574WSW-2 SM 6200B
92542712003 625574MW-1 SM 6200B
92542712004 625574MW-2 SM 6200B
92542712005 625887MW-3 SM 6200B
92542712006 625574MW-4 SM 6200B
92542712007 625574MW-5 SM 6200B
92542712008 625574MW-6 SM 6200B
92542712009 625574MW-7 SM 6200B
92542712010 625574MW-8 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/10/2021 04:16 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 38
Page 36 of 38
Page 37 of 38
Page 38 of 38
#=CL#
July 19, 2021
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92548822
92548822
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
P.O. Box 2012
Enka, NC 28728
The Spot
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on July 12, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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2225 Riverside Dr.
Asheville, NC 28804
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Page 1 of 13
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92548822
The Spot
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 13
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92548822
The Spot
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92548822001 MW-1 RSK 175 Modified 1 PASI-CMAD
SM 3500-Fe B-2011 1 PASI-ADMN
EPA 300.0 Rev 2.1 1993 1 PASI-AMDW
EPA 353.2 Rev 2.0 1993 1 PASI-AMFO
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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2225 Riverside Dr.
Asheville, NC 28804
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Page 3 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548822
The Spot
Sample:MW-1 Lab ID:92548822001 Collected:07/12/21 09:15 Received:07/12/21 10:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: RSK 175 Modified
Pace Analytical Services - Charlotte
RSK 175 Headspace
Methane 28.6 ug/L 07/14/21 20:13 74-82-810.0 1
Analytical Method: SM 3500-Fe B-2011
Pace Analytical Services - Asheville
Iron, Ferrous
Iron, Ferrous 14.7 mg/L 07/14/21 14:35 H3,N25.0 10
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 3.6 mg/L 07/15/21 15:33 14808-79-81.0 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 0.083 mg/L 07/14/21 00:50 14797-55-80.040 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 04:51 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548822
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
633472
RSK 175 Modified
RSK 175 Modified
RSK 175 HEADSPACE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92548822001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3327443
Associated Lab Samples:92548822001
Matrix:Water
Analyzed
Methane ug/L ND 10.0 07/14/21 17:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3327444LABORATORY CONTROL SAMPLE:
LCSSpike
Methane ug/L 361396 91 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3331345MATRIX SPIKE SAMPLE:
MSSpike
Result
92548708022
Methane ug/L 699396 102 70-130297
Parameter Units
Dup
Result QualifiersRPDResult
92548708023
3331344SAMPLE DUPLICATE:
Methane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 04:51 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548822
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
633288
SM 3500-Fe B-2011
SM 3500-Fe B-2011
Iron, Ferrous
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92548822001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3326310
Associated Lab Samples:92548822001
Matrix:Water
Analyzed
Iron, Ferrous mg/L ND 0.50 N207/14/21 12:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3326311LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Ferrous mg/L 1.6 N21.5 103 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92548708010
3326312SAMPLE DUPLICATE:
Iron, Ferrous mg/L 2.6 H3,N2102.8
Parameter Units
Dup
Result QualifiersRPDResult
92548708003
3326313SAMPLE DUPLICATE:
Iron, Ferrous mg/L 2.1 H3,N232.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 04:51 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548822
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
633482
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92548822001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3327474
Associated Lab Samples:92548822001
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 07/15/21 07:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3327475LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 51.250 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3327476MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92547812001
3327477
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 99 90-11098 05023.9 73.3 73.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3327478MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92548763003
3327479
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L M1508990-11090 050150194195
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 04:51 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548822
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
633186
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite, Unpres.
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92548822001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3326067
Associated Lab Samples:92548822001
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.040 07/14/21 00:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3326068LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 1.51.5 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3326069MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92549069001
3326070
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 104 90-110103 11.50.38 1.9 1.9
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3326071MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92549261006
3326072
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 101 90-110101 01.50.047 1.6 1.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 04:51 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 13
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92548822
The Spot
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 04:51 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 13
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92548822
The Spot
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92548822001 633472MW-1 RSK 175 Modified
92548822001 633288MW-1 SM 3500-Fe B-2011
92548822001 633482MW-1 EPA 300.0 Rev 2.1 1993
92548822001 633186MW-1 EPA 353.2 Rev 2.0 1993
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 04:51 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 13
Page 11 of 13
Page 12 of 13
Page 13 of 13