AS-3654_28789_CA_LSA_20100519

I
WATERLINKS
USING THE WATER CYCLE FOR GLOBAL COOLING
May 19, 2010
Ms. Diane Eskenasy, LG
UST Section, Division of Waste Management
Sherry Ingram, Owner
Professional Geologist
MAY 20 2010 /
UST SECTION
_ Ashevme Reg-ionffl Office
Z::Cm-
North Carolina Department of Environment and Natural Resources
2090 US Highway 70
Swannanoa, NC 28778
RE: ROBO Chevron Station, Incident Number: 28789
Limited Site Assessment
In compliance with Title' 15A of the North Carolina Administrative Code,
Subchapter 2N and Subchapter 2L, the Limited Site Assessment for the release
from petroleum dispensers at the ROBO Chevron Station, Incident Number
28789, is enclosed. This report meets the requirements outlined in the North
Carolina Department of (;nvironment and Natural Resources, Division of Waste
Management, UST Section, Guidelines for Assessment and Corrective Action for
UST Releases (July 15, 2008 Version).
If you have any concerns regarding this report, please contact me at the address,
telephone, or email shown below.
Sincerely,
Sherry Ingram
North Carolina Professional Geologist Number 2129
Owner, Waterlinks, PLLC
Enclosure: Limited Site Assessment for the ROBO Chevron Station
Cc: Mr. Chip Gould, Cason Oil Companies, Inc., 203 West King Street, East
Flat Rock, NC 28786
E. Baker Jordan, Jordan Environmental, LLC, 68 Little Horse Road,
Waynesville, NC 28786
P. 0. Box 1107, Candler, NC28715-1107
Cell: 828-779-1895
[e-mail]
www.WaterLinksPLLC.com
MAY 2 o 2010
USTSECTlON
A~1h0vmo Regional Office
LIMITED SITE ASSESSMENT
REPORT
for the
ROBO CHEVRON STATION
204 East State Street
Black Mountain, NC 28711
Incident Number: 28789
May 19, 2010
Waterlinks PLLC
P. 0. Box 1107
Candler, NC 28715-1107
Project No. 00210001
Limited Site Assessment Report
ROBO Chevron Station
Black Mountain, North Carolina
LIMITED SITE ASSESSMENT REPORT
May 19, 2010
A. SITE INFORMATION
1. Site Identification
Site Name/Address:
UST Incident Number:
Geographical Data Point:
Location Method:
Latitude:
Longitude:
2. Contacts
UST/Property Owner:
Represented by:
Consultant/Contractor:
Analytical Laboratory:
3. Release Information
ROBO Chevron Station
204 East State Street
Black Mountain, NC 28711, in Buncombe County
28789
On Property
GPS
(35.619 degrees North)
(82.318 degrees West)
Greybeard Realty, LLC
204 East State Street
Black Mountain, NC 28711
Mr. John B. Gould
Cason Companies, Inc.
203 W. King Streeet
East Flat Rock, NC 28726
Telephone: [phone]
Waterlinks PLLC.
10 Quigley Drive P. 0. Box 1107
Asheville, NC 28806 Candler, NC 28715-1107
Telephone: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Black Mountain, NC28804
Telephone: [phone]
Date Release Discovered: February 4, 2010
Estimated Quantity of Release: Unknown/unquantified
Cause of Release: Off-road Diesel and Bulk Kerosene Dispensers
Source Size/Contents: Not Applicable
Signature and Seal of Certifying Professional-Geologist:
I, Sherry Ingram, a Licensed Geologist for Waterlinks, PLLC, do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
00210001 ROBO Chevron LSA May 19, 2010
Limited Site Assessment Report
ROBO Chevron Station
Black Mountain, North Carolina
Waterlinks PLLC is licensed to practice geology in North Carolina. The certification
number of the company is C-445. ~ ~
· Sh_erry Ingram, .G. #212 ,;, ..
00210001 ROBO Chevron LSA
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ii
May 19, 2010
Table of Contents
Limited Site Assessment Report
ROBO Chevron Station
Black Mountain, North Carolina
Introduction ..................................................................................................................... 1
Site History and Characterization ................................................................................. 1
Initial Abatement Activities .............................................................................................. 1
Risk Characterization .................................................................................................... 3
Receptor Information .................................................................................................... 3
Site Geology and Hydrogeology ................................................................................... 4
Sampling Results .......................................................................................................... 4
Conclusions and Recommendations ............................................................................ 5
Table
Table 1.
Table 2
Table 3
Table 4
Table 5
Table 6
Table 7
Figures
Figure 1.
Figure 2.
Figure 3
Appendices
Summary of Soil Analytical Results
Receptor Information
Property Owners/Occupants
Sensitive Land Use Features
Public Water Systems
Well Construction Details
Summary of Groundwater Analytical Results
Site Vicinity Map
Site Map
Potential Receptor Map
Appendix A: Laboratory Analytical Reports and Chain of Custody Documentation
Appendix B: Risk Classification and Land Use Form
Appendix C: Driller's Logs
00210001 ROBO Chevron LSA May 19, 2010
iii
List of Acronyms and Abbreviations
AST aboveground storage tank
bgs below ground surface
ORO Diesel Range Organics
EPA U.S. Environmental Protection Agency
EPH Extractable Petroleum Hydrocarbon
GRO Gasoline Range Organics
IAAR Initial Abatement Action Report
LSA Limited Site Assessment
Limited Site Assessment Report
ROBO Chevron Station
Black Mountain, North Carolina
MADEP Massachusetts Department of Environmental Protection
NCAC North Carolina Administrative Code
NCDENR North Carolina Department of Environment and Natural Resources
RMSCC Residential Maximum Soil Contaminant Concentration
S/GMSCC Soil-to-Groundwater Maximum Soil Contaminant Concentration
SVOC Semivolatile Organic Compound
VOC Volatile Organic Compound
VPH Volatile Petroleum Hydrocarbon
ug/L microgram per liter
UST underground storage tank
00210001 ROBO Chevron LSA May 19, 2010
iv
Introduction
Limited Site Assessment Report
ROBO Chevron Station
Black Mountain, North Carolina
This report presents the results of a Limited Site Assessment (LSA) conducted at the
ROBO Chevron Station, 204 East State Street in Black Mountain, North Carolina (NC).
The property is owned by Greybeard Realty, LLC, of 204 East State Street in Black
Mountain, NC, and the tanks onsite are owned and operated by Cason Companies,
Inc., 203 W. King Street, East Flat Rock, NC 28726, telephone: [phone],
represented by Mr. John Gould. Figure 1 shows the site location on a United States
Geological Survey topographic map, and Figure 2 presents a site map indicating the
locations of the dispensers, soil excavation areas, well locations, and samples collected.
This LSA was required by the NC Department of Environment and Natural Resources
(DENR) in a Notice of Violation (NOV) issued on April 21, 2009.
Site History and Characterization
Evidence of a suspected release (stained soil) was discovered during a compliance
inspection performed by the North Carolina Division of Waste Management
Underground Storage Tank Section, and a Notice of Violation (NOV) was issued on
April 21, 2009. Jordan Environmental, LLC, was contracted to perform a site check in
the vicinity of the location, with assessment and reporting done by Waterlinks, PLLC.
Initial Abatement Activities
On December 29, 2009, Jordan Environmental, LLC, performed the site check for the
NOV. Evidence of a fuel release (stained soil) was observed directly beneath the off
road diesel dispenser located at the second pump island and beneath the bulk fueling
area kerosene and diesel dispensers, as described in the NOV. A stainless steel hand
auger was used to collect soil samples from beneath each dispenser (Figure 2). Soil
samples were collected using latex gloves and placed in EPA-approved containers for
transport to a certified North Carolina laboratory for analysis. An Initial Abatement
Action Report (IMR) for the site was issued to DENR on May 6, 2010, by Waterlinks,
PLLC (Waterlinks).
Three soil samples (DD-1, BD-2, and BK-3 in Figure 2) were collected from directly
beneath the dispenser access openings for the fuel dispensers at a depth of 2 feet
below ground surface (bgs). The soil samples were submitted for laboratory analysis of
diesel range organics (ORO) by EPA Method 8015 with 3550 extraction and gasoline
range organics (GRO) by EPA Method 8015 with 5030 extraction.
The soil analytical results are summarized in Table 1, and a copy of the laboratory
analytical report and chain of custody documentation are included in Appendix A. The
results of the analyses indicated that concentrations of Total Petroleum Hydrocarbons
(TPH) in all three soil samples at the ROBO Chevron Station had concentrations that
exceed the action levels established by the State of North Carolina for TPH in
Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST
00210001 ROBO Chevron LSA 1 May 19, 2010
Limited Site Assessment
ROSO Chevron Station
Black Mountain, North Carolina
Releases (March 3, 2007, Version), 10 mg/kg. Because the analytical results confirmed
contamination exceeding the action level, soil around the off-road pump island diesel
dispenser was excavated (Figure 2).
On April 16, 2010, a mini-excavator was used to excavate contaminated soil
encountered in the bulk dispenser fueling area during the site check (Figure 2). The
contaminated soils were excavated to a depth of 11 feet below existing site grade. The
final excavation measured 15 feet long by 10 feet wide by 11 feet deep. The excavation
cavity was backfilled with clean suitable soil and compacted. Contaminated soil
removed from the excavation (24. 71 tons) was transported to Environmental Soils, Inc.
in Lattimore, NC, for disposal.
Five soil samples (Soil-A, Soil-8, Soil-C, Soil-D, and Soil-E in Figure 2) were collected
from the sides and bottom of the excavation on April 16, 2010, and submitted to the
laboratory for analysis of volatile petroleum hydrocarbons (VPH) and extractable
petroleum hydrocarbons (EPH) by Massachusetts Department of Environmental
Protection (MADEP) methods, volatile organic compounds (VOCs) by EPA Method
8260, and semi-volatile organic compounds (SVOCs) by EPA Method 8270. The
results of these analyses were compared with the Residential Maximum Soil
Contaminant Concentrations (RMSCCs) and the Soil-to-Groundwater Maximum Soil
Contaminant Concentrations (Soil-to-GW MSCCs) (NC Department Of Environment and
Natural Resources, Division of Waste Management, UST Section, 2008, Guidelines for
Assessment and Corrective Action for UST Releases, July 15, Table 1).
Samples Soil-A, Soil-8, Soil-C, and Soil D were collected from the side walls of the
excavation at a depth of approximately 7 feet below existing site grade. Sample Soil-E
was collected from the bottom of the excavation at a depth of approximately 11 feet
below existing site grade.
Two soil samples exceeded the Soil-to-GW MSCC for Total C9-C18 Aliphatics (540
mg/kg), and all five samples exceeded the Soil-to-GW MSCC for Total C9-C22
Aromatics (31 mg/kg), with one, sample Soil D, also exceeding the RMSCC for Total
C9-C22 Aromatics (469 mg/kg) with a concentration of 714.2 mg/kg. The VOC
Naphthalene also exceeded the Soil-to-GW MSCC (0.16 mg/kg) in samples Soil B (0.59
mg/kg), Soil D (1.1 mg/kg), and Soil E (1.1 mg/kg). Elevated soil concentration levels
above the MSCCs initiated this LSA.
Risk Characterization
As part of the LSA, the Risk Classification and Land Use Form provided in Appendix A
of the guidelines has been completed for the ROSO Chevron Station and is presented
in Appendix B.
00210001 ROSO Chevron LSA May 19, 2010
2
Receptor Information
Limited Site Assessment
ROBO Chevron Station
Black Mountain, North Carolina
Water for the site and surrounding area is provided by the Town of Black Mountain
Public Water System. Jordan completed a visual search for water supply wells within
1500 feet of the site on April 16, 2010, and identified no wells
Three unnamed tributaries, the Swannanoa River, and Lake Tomahawk are identified
as potential receptors in Table 2 and Figure 3.
Property owners and occupants within 1500 feet of the site are listed in Table 3, and the
area is highlighted in Figure 3.
Seventeen sites, mostly churches and government buildings, are presented as sensitive
land-use features in Figure 3 and Table 4.
NC SWAP info was checked to determine if the site is in a wellhead protection area,
and the Town of Black Mountain Public Water System and Community well is identified
in Figure 3 and Table 5.
The following bullets summarize other receptor information regarding this site:
• The closest surface water body is the unnamed creek approximately 230 feet
south of the source area.
• Public water supply is available in the vicinity of the site from the Town of Black
Mountain Public Water System.
• The site is not located in a wellhead protection area.
• Subsurface features at the site are shown on Figure 2.
• The risk of explosion due to the accumulation of vapors in confined space and
the threat to public health, public safety or the environment posed by vapors in
the subsurface features is considered low.
The property containing the release and the area around it are zoned commercial.
Site Geology and Hydrogeology
Based on the soils observed during the installation of the source area monitoring wells
(MW-1 and MW-2), the uppermost soils at the site consist of dark brown silty sand to a
depth of 5 feet below ground surface (bgs). From 5 feet bgs to 10 feet bgs, soil
encountered in MW-1 consisted of tan silty sand, underlain by grey silty sand to the total
depth of 24 feet bgs, while soils for MW-2 consisted of tan silty sand from 5 feet bgs to a
00210001 ROBO Chevron LSA May 19, 2010
3
Limited Site Assessment
ROSO Chevron Station
Black Mountain, North Carolina
total depth of 24 feet bgs. Well construction details are presented in Table 6, and the
driller's logs for the monitoring wells (MW-1, and MW-2) are included in Appendix C.
The depth to groundwater in both MW-1 and MW-2 was 11 feet bgs on the date of
installation, April 9, 2010. Groundwater flow is assumed to follow topography and flow
south about 230 feet and west approximately 315 feet to the unnamed tributaries.
Sampling Results
As part of this assessment, two groundwater monitoring wells (MW-1 and MW-2) were
installed adjacent to the dispensers as shown in Figure 2. The borings were advanced
to depths of 24 feet bgs, and the wells were constructed in accordance with 15A North
Carolina Administrative Code (NCAC) 2L .0404(3). MW-1 and MW-2 were installed in
the uppermost aquifer beneath the ROBO Chevron Station site on April 9, 2010. No
free product was observed in the soil cuttings or water sample taken from the well. Four
soil samples and two groundwater samples were collected during the drilling and
completion of MW-1 and MW-2.
Soil
Soil sample analytical results for the project are summarized in Table 1, and laboratory
analytical reports and chain of custody documentation are presented in Appendix A.
Soil samples MW-1-5, MW-1-10, MW-2-5, and MW-2-10 were submitted for laboratory
analysis of VPH and EPH using MADEP methods, VOCs using EPA Method 8260, and
SVOCs using EPA Method 8270. Although the Soil-to-GW MSCC for Total C9-C18
Aliphatics (31 mg/kg)' was exceeded in three of the four samples, no concentrations
were found that exceed, the RMSCC (469 mg/kg). Two SVOCs were detected in one
soil sample, but did not exceed either standard. Only the VOC Naphthalene was
detected at a concentration that exceeded the Soil-to-GW MSCC standard (0.16
mg/kg), and none exceeded the RMSCC standard (33 mg/kg).
Groundwater
Analytical results for the groundwater samples are summarized in Table 7, and
laboratory anal_ytical reports and chain of custody documentation are presented in
Appendix A. Groundwater samples MW-1 and MW-2 were collected on April 9, 2010,
and the samples were submitted for laboratory analysis of MADEP VPH and EPH
(Alkanes and Aromatics); . SVOCs using EPA Method 625 (Base Neutral and Acid
Extractables plus 1 O · Iargest non-target peaks); and VOCs using EPA 62008 (with
Xylenes, MTBE, and IPE).
Detections of the MADEP Petroleum Hydrocarbon Fraction were elevated in both the
MW-1 and MW-2 groundwater samples, but NC has not identified standards for
identifying risk. Detections of both SVOC and voe Naphthalene (15.4 ug/L and 31.5
ug/L, respectively in MW-1, and 44.1 ug/L and 183 ug/L, respectively in MW-2)
exceeded the North Carolina 2L Groundwater Quality Standards (2L) (6ug/L for both
SVOC and VOC Naphthalene), but did not exceed the Gross Contamination Level
00210001 ROSO Chevron LSA May 19, 2010
4
Limited Site Assessment
ROBO Chevron Station
Black Mountain, North Carolina
(GCL) (6000 ug/L in both SVOC and VOC Naphthalene). The only other contaminant
detected that exceeded the 2L standard, Benzene (1 ug/L), was detected at 209 ug/L in
MW-1 and 9.2 ug/L in MW-2. No detections exceeded any of the GCLs.
Conclusions and Recommendations
The results of this investigation indicate that some soil and groundwater contamination
exceeding the Soil-to-GW MSCC and 2L standards is present at the ROBO Chevron
Station from a petroleum release. Still, no concentrations exceeding the RMSCC and
GCLs were detected at the site.
The Risk Classification and Land Use Form provided in Appendix B and the risk
classification criteria detailed in the guidelines (NCDENR, 2008) have been reviewed in
regards to the site. Due to the availability of water by a provider in the area, the site
meets the criteria of the risk classification guidelines for classification as intermediate
risk.
Based on the information provided in this Limited Site Assessment, Waterlinks, PLLC,
recommends that No Further Action be approved for the ROBO Chevron Station.
00210001 ROBO Chevron LSA May 19, 2010
5
TABLES
DD-1 BD-2 BK-3 Soil-A
12/29/2009 12/29/2009 12/29/2009 4/16/2010
2 ft-bgs 2 ft-bgs 2 ft-bgs 7 ft-bgs
Diesel Range Organics
(EPA Method 8015 with 3550 extraction)
DAO 214 8550 40.7 NAn
Gasoline Range Organics
(EPA Method 8015 with 5030 extraction)
GAO 36.6 7.5 NAn
NAn NAn NAn
Petroleum Hydrocarbon Fractio
(MADEP Methods)
C9-C18 Aliphatics (EPH) 235
C9-C12 Aliphatics (VPH)
Total C9-C18 Allphatics 235
Total C19-C36 Allphatics
C9-C10 Aromatics (VPH)
C11-C22 Aromatics (EPH) 190
Total C9-C22 Aromatics 190.0
Semlvolatlle Organic Compounc NAn NAn NAn
(EPA Method 8270)
Benzo(a)anthracene
2,4-Dimethylphenol
bis(2-Ethylhexyl)phthalate 0.0051
1-Methylnaphthalene 0.024
2-Methylnap~thalene 0.023
2-Methylphenol(o-Cresol)
00210001 Robo Chev LSA T1
TABLE 1
SOIL ANAL VTICAL RES UL TS
Limited Site Assessment
Robe Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 1 of 2
Soil-8 Soll-C Soll-D Soil-E
4/16/2010 4/16/2010 4/16/2010 4/16/2010
7 ft-bgs 7 ft-bgs 7 ft-bgs 7 ft-bgs
NAn NAn NAn NAn
NAn NAn NAn NAn
319 748 825
68.6 40.4 62.4 50.1
319 748 825 0
23.0 14.0 18.2 15.9
217 395 696 280
240 409 f'""7.1_4;2;fi ;~-: 295.9
0.0070
0.0016
0.0028 0.0045
0.0088 0.012 0.044 0.056
0.0023 0.0049 0.059 0.D40
0.0022
LSA LSA LSA LSA Reportable
MW-1-5 MW-1-10 MW-2-5 MW-2-10 Concentration
4/9/2010 4/9/2010 4/9/2010 4/9/2010 (mg/kg)
NAn NAn NAn NAn 10
NAn NAn NAn NAn 10
Soil•to-GW Resldentlal
Max Soil Cont. Max Soll Cont.
Level Level
(mg/kg) (mg/kg)
112 72.2 39.4 16.6 NA NA
20.2 NA NA
132.2 72.2 39.4 16.6 540 1500
31.9 NA 31,000
NA NA
54.0 46.8 47.7 15.8 NA NA
54.0 46.8 47.7 15.8 31 469
0.41 8.2 940
0.64 312
6.6 46
NA NA
0.45 3.6 63
NA NA
May 19, 2010
DD-1 BD-2 BK-3 Soil-A
12/29/2009 12/29/2009 12/29/2009 4/16/2010
2 ft-bgs 2 ft-bgs 2 ft-bgs 7 ft-bgs
Semivolatile Organic Compounc NAn NAn NAn
(EPA Method 8270)
Naphthalene 0.0035
Phenanthrene 0.017
Pyrene 0.0018
Volatile Organic Compounds NAn NAn NAn
(EPA Method 8260)
n-Butylbenzene
sec-Butylbenzene
p-lsopropyltoluene
Naphthalene
n-Propylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
I
I
TABLE 1
SOIL ANAL VTICAL RESULTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 2 of 2
Soil-8 Soil-C Soll-D Soil-E
4/16/2010 4/16/2010 4/16/2010 4/16/2010
7 ft-bgs 7 ft-bgs 7 ft-bgs 7 ft-bgs
0.012 0.0050
0.0098 0.013 0.025 0.035
0.0014 0.0027 0.0029
0.34
0.4
0.3
0.59 1.1 1.1
0.3
0.71
0.29
Note: 1. Bolded values indicate concentrations which have exceeded at least one maximum allowable soil concentration.
bgs: below ground surface ft: feet GW: groundwater kg: kilogram mg: milligram NA: not applicable
NAn: Not analyzed ND: not detected
00210001 Robo Chev LSA T1
LSA LSA LSA LSA Soll-to-GW Residential
MW-1-5 MW-1-10 MW-2-5 MW-2-10 Max Soll Cont. Max Soll Cont.
Level Level
4/9/2010 4/9/2010 4/9/2010 4/9/2010 (mg/kg) (ma/kal
0.16 313
56 469
279 469
4.3 626
3.3 626
NA NA
0.57 0.41 0.34 0.16 313
1.7 626
8.5 782
8.3 782
May 19, 2010
A Unnamed Tributary s
B Unnamed Tributary w
C Unnamed Tributary E
D Swannanoa River SE
E Lake Tomahawk w
00210001 ROBO Chevron LSA T2
TABLE 2
RECEPTOR INFORMATION
Limited Site Assessment
ROBO Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 1 of 1
NA
NA
NA
NA
NA
NA
NA
NA
Town of Black Mountain [phone]
NA 230 Down
NA 315 Down
NA 685 Down
NA 1200 Down
Recreation 2660 Ridge Between
May 19, 2010
Parcel
Number
0619253048
0619253447
0619253930
0619254164
0619254619
0619254774
0619254944
0619255471
0619255681
0619255826
0619255861
0619256263
0619256468
0619256706
0619257099
0619257548
0619257912
0619258193
0619258322
0619258495
0619258728
0619259025
0619259197
0619259398
0619259579
0619262478
0619263055
0619263111
0619263621
0619263807
0619263928
0619264000
0619264311
0619264557
0619264580
0619264609
TABLE 3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 1 of 14
Owner/ Occupant Name
(Last, First Ml)
FLETCHER NANCY C 99999
CAROLINA FIRST BANK A SC COMP ANY 308
GAINES LAURA REAY 100
THE STEPP-NICHOLS CO INC 325
CRAWFORD SYLVIA P (TRUSTEE) 105
PERRIN TODD & DONNA M 103
SPARKS CHARLES T & CAROLYN 99999
WAGENER ALWINE 306
TOWN OF BLACK MOUNTAIN 105
SHELL RAYMOND & TILDA 111
BRINKLEY DOUGLAS C 109
STATE EMPLOYEES CREDIT UNION 319
HONEYCUTT JR WM C ETAL 304
PELLOM JOHN LAWRENCE 107
MORRIS ZEKE E 12
ASHEVILLE FEDERAL BANK FSB 300
CHRISTY WILLIAM H & DEIRDRES 110
ORR ROBERT & EVELYN A 11
STATE EMPLOYEES CREDIT UNION 313
THE BANK OF ASHEVILLE 301
DEER FIELD PROPERTIES LLC 208
ORR ROBERT & EVELYN A 99999
ORR ROBERT & EVELYN A 13
HUDSON III J RICHARD & NANCY K 101
THAI BASIL INC 227
OLIVE TREE HOSPITALITY LLC 136
MERRILL LYNCH TRUST CO OF FLORIDA 205
GRASS JAMES H TRUSTEE 207
ROZZELL W GRADY & BETTY T 101
WINGATE RICHARD B 205
EDWARD KENNETH 207
BOYD JULIE 203
POLK III DEMPSEY F 132
CALLOWAY RACHAEL S 123
WILLIAMS GEORGE M & MARIA D 121
WEBBER LYNNE & THOMAS PATTESON JR 127
Address
STATE
STATE
ORCHARD
STATE
ORCHARD
ORCHARD
DOUGHERTY
STATE
DOUGHERTY
DOUGHERTY
DOUGHERTY
STATE
STATE
DOUGHERTY
SPRING
STATE
DOUGHERTY
SPRING
STATE
STATE
STATE
SPRING
SPRING
DOUGHERTY
STATE
DOUGHERTY
DOUGHERTY
DOUGHERTY
CONNALLY
CHURCH
CHURCH
DOUGHERTY
DOUGHERTY
CHURCH
CHURCH
CHURCH
00210001 Robe Chev LSA T4
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
May 19, 2010
Parcel
Number
0619264633
0619265138
0619265389
0619265445
0619265776
0619265813
0619265917
0619265932
0619266040
0619266110
0619266335
0619266380
0619266682
0619266720
0619267225
0619267270
0619267496
0619267526
0619267560
0619268080
0619268385
0619268431
0619268722
0619269249
0619269264
0619269992
0619272487
0619273024
0619273130
0619273137
0619273315
0619273350
0619273401
0619273543
0619273661
0619273725
TABLE3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 2 of 14
Owner/ Occupant Name
(Last, First Ml)
SECREST CLAUDE D & SYLVIA 125
KENNEDY FRANCES H 124
KNIGHT EH & RUBY 117
HAIGLER POLLY C 119
TOBIN JOLAN S 124
ACK INVESTMENTS LLC 126
BOSWELL JR GEO C & MARY C 132
WATTS ROBT C & CLAUDIA K 130
BUCHANAN JOHN H & MARGARET G 112
KENNEDY FRANCES 124
GARY WELLS BALL TRUST 115
GARRISON PHILLIP B & JACKIE D 113
LINTON ANDREW M & HEIDI S 120
BRYAN HELENS 122
LOVELACE MARJORIE BOGGS 111
SCHNEPP ROGER & NANCY 109
TAYLOR JR JACKIE L & BARBARA H 114
MADDEN JERRY DAVID 118
WILSON C VAUGHN & DORIS B 116
BLACK MOUNTAIN UNITED METHODIST 101
DUARTE MARCUS P 110
TAYLOR JACKIE L & PATSY 112
BLACK MOUNTAIN PRESBYTERIAN CHURCH 117
BROUSSARD MICHAEL 108
SNEED RONALD E & PATRICIA A DEHNER 104
COGBURN INVESTMENTS LLC 128
THE STEPP NICHOLS CO INC 307
THOMAS JR EVERETT M 209
HUGHES JAS F & DONNA M 211
REED CLELAND T & NELL W TRUSTEES 213
HAYNES DOUGLAS 204
WILLIAMS HELEN C 200
THE STEPP NICHOLS CO INC 305
SURLES LEON O & ETAL 309
ELLIOTT ERIC STEPHEN 311
LIBERATOR! DENISE 102
Address
CHURCH
DOUGHERTY
CHURCH
CHURCH
CHURCH
CHURCH
CHURCH
CHURCH
DOUGHERTY
DOUGHERTY
CHURCH
CHURCH
CHURCH
CHURCH
CHURCH
CHURCH
CHURCH
CHURCH
CHURCH
CHURCH
CHURCH
CHURCH
MONTREAT
CHURCH
CHURCH
MONTREAT
CHURCH
CHURCH
CHURCH
CHURCH
LAUREL CIRCLE
LAUREL CIRCLE
CHURCH
CHURCH
CHURCH
OAKLAND
00210001 Robe Chev LSA T4
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
RD
ST
ST
RD
ST
ST
ST
ST
DR
DR
ST
ST
ST
DR
May 19, 2010
Parcel
Number
0619273941
0619274279
0619274389
0619274576
0619274990
0619275023
0619275123
0619275185
0619275374
0619275546
0619275732
0619276330
0619276380
0619276460
0619276526
0619276788
0619276792
0619276950
0619277111
0619277296
0619277523
0619277605
0619277610
0619278303
0619278420
0619278592
0619278759
0619278760
0619278940
0619279611
0619279698
0619279954
0619283281
0619283422
0619283620
0619283768
TABLE3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 3 of 14
Owner/ Occupant Name
(Last, First Ml)
STEPHENSON E W & MARY J 207
HICKS DEOBRAH A 200
HICKS JANEE 208
HAMILTON EUNICE COX & RODERICK J 106
EDWARDS ALANE & CHERYL A 205
MCCONNAUGHY JAMES 134
WILLIAMS FRANK B (LE) 136
WILLIAMS MOUNTAIN PROPERTIES INC 101
COURAGE JOHN D & RENEE B 104
KARNAS LULA HA VERTT 104
OSTEEN JAMES S & HEATHER H TRUSTEES 99999
CAPPS JULIA A & GLADYS R BROOKS 102
AZERBAEV ALSHERBAI 100
COCKRELL JR RAY W & SHEILA M 105
LAWTON THOMAS P 102
OSTEEN JAMES S & HEATHER H TRUSTEES 107
COTTLEJEAN 105
COOPER JOHN F 109
AT AND T COMMUNICATIONS 135
WELLS JR WILLIAM F 201
HALL DANIEL R ET AL 100
RENNINGER SHIRLEY A REV TRUST 103
SUMMERS JAMES R 101
EV ANS MARTHA MCREE 203
LANCE SHANE 205
SWETT JR ROBERT E & LINDA S 301
HUNLEY DONALD L & SUSAN B KASK 106
GORDON FRED M & ADRIENNE J LONG 104
MICHAUD WILLIAM A 107
RECTOR SANDRA L 303
GIBBON ASHLEY HILLYER & ANDREW H 305
BRANDON ARLENE S & KEVIN D 103
MUNSTERMAN MIKE F 203
CARREIRO JOSEPH C & LESLIE P 204
WHITE JAMES H & JULIE D 205
STONE ALLYSON A 204
Address
PINE
CHURCH
CHURCH
CONNALLY
PINE
CHURCH
CHURCH
LAUREL CIRCLE
LAUREL CIRCLE
CONNALLY
MOUNTAIN
LAUREL CIRCLE
LAUREL CIRCLE
CONNALLY
CONNALLY
MOUNTAIN
MOUNTAIN
MOUNTAIN
MONTREAT
MONTREAT
CONNALLY
MOUNTAIN
MOUNTAIN
MONTREAT
MONTREAT
MONTREAT
MOUNTAIN
MOUNTAIN
PINE
MONTREAT
MONTREAT
PINE
VIEW
VIEW
NINTH
NINTH
00210001 Robo Chev LSA T 4
ST
ST
ST
ST
ST
ST
ST
DR
DR
ST
ST
DR
DR,
ST
ST
ST
ST
ST
RD
RD
ST
ST
ST
RD
RD
RD
ST
ST
ST
RD
RD
ST
ST
ST
ST
ST
May 19, 2010
Parcel
Number
0619284008
0619284290
0619284368
0619284550
0619284728
0619285017
0619285395
0619285485
0619285573
0619285600
0619286046
0619286125
0619286222
0619287293
0619287349
0619287549
0619287551
0619287830
0619288023
0619288112
0619288461
0619288586
0619288724
0619289038
0619289213
0619289284
0619289462
0619289587
0619289713
0619294213
0619350031
0619350546
0619350644
0619350668
0619350752
0619351163
TABLE 3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 4 of 14
Owner/ Occupant Name
{Last, First Ml)
CHILDS W TRAVIS & HOLLY F 204
BALDWIN JAMES M & MARTHA J 201
GRIFFIN ill HAYNE PRESTON 202
STEPHENSON JOEY B & SUSAN M 202
WILLIAMS WHITNEY N 202
MCELHENY DONALD R 200
GARTRELL ETHELBERT H & CATHERINE Y 200
WHITE WILLIAM T & VICKIE L 301
JARRETT JULIE LYNNE 303
MILTON MACKE & LOIS R 305
MCELHENY DONALD R 201
STILES GREGORY D 205
BROUWER EDWARD W & GLENDA B 207
RANDALL JEAN M (LE) 206
BARRETTA KERRY S 108
MILTON JACK A & REBA 304
JONES LA VERNE W 302
SCHOEN SALLY A 112
MOUNTAIN PINE LLC 200
MILTON CL & TL BULLERDICK 202
JOHNSTONE DEANNA I & D C SALES IT 106
BIGGS CHARLES L & DORIS 107
BURKE HERBERT T & THOMAS JUI 110
SHARP DOUGLAS M & JAMIE A 104
BURGESS KATHERRYN D (LE) 109
GRASSPAULR 107
CHAKINMARC 104
DEGENNARO ANNE M 105
CHRISTY WILLIAM H & DEIRDRE S 108
CARSON FAMILY LP ETAL 200
ORR ROBERT & EVELYN A 29
TOWN OF BLACK MOUNTAIN 225
TOWN OF BLACK MOUNTAIN 225
AND 223
LAUDENSLAYER JOSEPH G & ALYSON R 221
WILLIAMS MOUNTAIN PROPERTIES INC 106
Address
PINE
VIEW
VIEW
VIEW
NINTH
PINE
VIEW
MOUNTAIN
MOUNTAIN
MOUNTAIN
MOUNTAIN
MOUNTAIN
MOUNTAIN
MOUNTAIN
VIEW
MOUNTAIN
MOUNTAIN
NINTH
MOUNTAIN
MOUNTAIN
VIEW
NINTH
NINTH
PINE
VIEW
VIEW
VIEW
NINTH
NINTH
NINTH
VANCE
STATE
STATE
STATE
STATE
BLACK MOUNTAIN
00210001 Robo Chev LSA T4
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST.
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
AVE
ST
ST
ST
ST
AVE
May 19, 2010
Parcel
Number
0619351235
0619351500
0619351573
0619351795
0619351834
0619351946
0619351975
0619351979
0619352116
0619352200
0619352512
0619352554
0619352633
0619352720
0619352993
0619352999
0619353170
0619353250
0619353375
0619353526
0619353689
0619353691
0619353773
0619353779
0619353781
0619353823
0619353827
0619353907
0619353910
0619353989
0619353991
0619354293
0619354470
0619354643
0619354796
0619354843
TABLE 3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 5 of 14
Owner/ Occupant Name
(Last, First Ml)
WILLIAMS MOUNTAIN PROPERTIES INC 102
TOWN OF BLACK MOUNTAIN 99999
THE TOWN OF BLACK MOUNTAIN 99999
OTTO MARSHALL KENT 116
ROBINSON LARRY 207
MCMURRAY JR W H ETAL 203
MONTREATCOTTAGERENTALSILLC 102
VENGOECHEA ROBERTO E 100
WILLIAMS MOUNTAIN PROPERTIES INC 108
WILLIAMS MOUNTAIN PROPERTIES INC 104
D F HARVEY INC 206
RICKETTS BARRY BRUCE 204
RICKETTS BARRY BRUCE 128
RICKETTS BARRY BRUCE 118
TOWN OF BLACK MOUNTAIN 99999
CARAWAY KIM & CHERYL D 111
POMEROY JOHNS 115
PROVIDENTIALPROPERTIESLLC 105
BLUE RIDGE PROPERTY HOLDINGS LLC 101
RICKETTS BARRY BRUCE 132
ARCHAMBAULT HAROLD C & DAVID J 137
RICKETTS BARRY BRUCE 139
BLEDSOE BRENDA D 133
RICKETTS BARRY BRUCE 99999
OLD BUILDING LLC 135
HOW ARD CHANNING B 121
J &LBUTLERLLC 119
TOWN OF BLACK MOUNTAIN 99999
GREENE RAFTER ENTERPRISES 117
TOWN OF BLACK MOUNTAIN 99999
GREENE RAFTER ENTERPRISES 99999
INLAND AMERICAN ST PORTFOLIO LLC 200
THE TOWN OF BLACK MOUNTAIN 99999
SOBOL JR CT & BEYERL YB 106
ICE HOUSE CREATIONS LLC 128
MOUNTAINSPACE I.LC 120
Address
BLACK MOUNTAIN
DOUGHERTY
SUTTON
CHERRY
STATE
STATE
CHERRY
CHERRY
BLACK MOUNTAIN
BLACK MOUNTAIN
SUTTON
SUTTON
CHERRY
CHERRY
CHERRY
CHERRY
BLACK MOUNTAIN
BLACK MOUNTAIN
BLACK MOUNTAIN
CHERRY
CHERRY
CHERRY
CHERRY
CHERRY
CHERRY
CHERRY
CHERRY
CHERRY
CHERRY
BROADWAY
BROADWAY
NC9
BLACK MOUNTAIN
SUTTON
BROADWAY
BROADWAY
00210001 Robo Chev LSA T4
AVE
ST
AVE
ST
ST
ST
ST
ST
AVE
AVE
AVE
AVE
ST
ST
ST'
ST
AVE
AVE
AVE
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
HWY
AVE
AVE
ST
ST
May 19, 2010
Parcel
Number
0619354904
0619354932
0619355094
0619355488
0619355647
0619355968
0619355992
0619356828
0619356853
0619357991
0619359106
0619359589
0619359826
0619360087
0619360158
0619360200
0619360339
0619360390
0619360761
0619360881
0619361100
0619361137
0619361265
0619361799
0619362049
0619362052
0619362055
0619362057
0619362073
0619362141
0619362154
0619362175
0619362197
0619362346
0619362540
0619362638
TABLE3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 6 of 14
Owner/ Occupant Name
(Last, First Ml)
HYDER HARRY (LE) 118
MOUNTAINSPACE LLC 99999
BMRRLLC 202
THE TOWN OF BLACK MOUNTAIN 99999
GREY EAGLE LAND COMPANY LLC 100
TYSON FURNITURE CO INC 99999
BURGESS DOROTHY (LE) 131
EARLEY WILLIAMS & RICHARD R 135
HENSONTIMBERPRODUCTSCORP 139
HENSON TIMBER PRODUCTS CORP 139
MIAN REAL ESTATE LLC 203
HELEN P CAMPBELL REVOCABLE TRUST 151
. .
THE STEPP-NICHOLS COMPANY INC 117
ETHEL MINTZ HUDSON REVOCABLE TRUST 118
FA VROT JOHN CHARLES 100
MUNN BILL & CAROLYN K 102
BLACK MTN PRESBYTERIAN CHURCH 99999
MCMURRAYJRWH&MARYL 105
PACE CATHERINE V 114
F1RST STATES INVESTORS 4100B LLC 116
WELLER ROGER D 116
FOSTER PINKERTON REVOCABLE TRUST 104
SOBOL JR CT & BEYERL YB 100
REDMOND DARRELL B & BERTHA 101
MAYTIN JOHANNA TRUSTEE 111
BUELL KAREN & ROY D III 105
BLACK MOUNTAIN BOOKS LLC 103
BECKER RODNEY D & PEI-LING T 101
PELLOM JOHN LAWRENCE 107
BRANDON LAWRENCE J & RUTH 107
ROBINSON JR JAMES B & SUSAN R 105
ROBINSON JR JAMES B & SUSAN R 103
ROBINSON JR JAMES B & SUSAN R 101
THE TOWN OF BLACK MOUNTAIN 100
THE TOWN OF BLACK MOUNTAIN 102
TOWN OF BLACK MOUNTAIN 106
Address
BROADWAY
BROADWAY
NC9
NC9
SUTTON
BROADWAY
BROADWAY
BROADWAY
BROADWAY
BROADWAY
NC9
NC9
SUTTON
STATE
CHURCH
CHURCH
MONTREAT
MONTREAT
MONTREAT
MONTREAT
STATE
STATE
STATE
WEST
STATE
CHERRY
CHERRY
CHERRY
CHERRY
STATE
STATE
STATE
STATE
STATE
MONTREAT
MONTREAT
00210001 Robe Chev LSA T 4
ST
ST
HWY
HWY
AVE
ST
ST
ST
ST
ST
HWY
HWY
AVE
ST
ST ..
ST
RD
RD
RD
RD
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
RD
RD
May 19, 2010
Parcel
Number
0619362951
0619363048
0619363056
0619363064
0619363121
0619363259
0619363274
0619363853
0619363893
0619363974
0619364165
0619364213
0619364221
0619364287
0619364313
0619364387
0619364507
0619365007
0619365033
0619365421
0619365560
0619365742
0619365870
0619366183
0619366297
0619366373
0619366422
0619366831
0619366898
0619366909
0619367497
0619367554
0619367603
0619368346
0619368421
0619368641
TABLE3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 7 of 14
Owner/ Occupant Name
(Last, First Ml)
ROBBINS JAMES JEFFREY 104
RULAND AMANDA B 106
STONE RICHARD B & MURIEL 108
STONE RICHARD B & MURIEL 110
WALL IV DANIEL H & BARBARA S 104
TYSON FURNITURE COMPANY INC 104
TYSON FURNITURE CO INC 101
MCMURRAYJOHNROBERT 100
MFH PROPERTIES LLC 101
GREEN DENNISE 103
TYSON FURNITURE CO INC 109
TYSON FURNITURE CO INC 105
TYSON FURNITURE CO 107
TYSON FURNITURE CO 109
TYSON FURNITURE CO INC 112
TYSON FURNITURE CO INC 114
THE TOWN OF BLACK MOUNTAIN 102
TYSON FURNITURE CO INC 119
ATWOOD ROY LEE 121
TYSON FURNITURE CO INC 120
TYSON FURNITURE COMPANY INC 130
BLK MTN-SW ANN CHAM OF COMM INC 201
BLACK MOUNTAIN INVESTORS LLC 203
TYSON FURNITURE COMPANY INC 109
TOWN OF BLACK MOUNTAIN 99999
DA VIS JR PAUL & KATHERINE METTS TC 106
TYSON FURNITURE CO INC 99999
BLACK MOUNTAIN INVESTORS LLC 99999
GREYBEARD REALTY LLC 207
THE TOWN OF BLACK MOUNTAIN 160
BRADEN JONATHAN & MARY NOBLE 105
BEGLEY WILLIAM MICHAEL 103
BLACK MOUNTAIN SAV & LOAN ASSOC 200
CLEGG KATHERINE U & CHARLES N 109
BRADEN JONATHAN & MARY NOBLE 105
CAMPBELL FAMILY INVESTMENTS LLC 99999
Address
WEST
BROADWAY
BROADWAY
BROADWAY
BROADWAY
STATE
BROADWAY
WEST
MIDLAND
MIDLAND
BROADWAY
BROADWAY
BROADWAY
BROADWAY
STATE
STATE
STATE
BROADWAY
BROADWAY
STATE
STATE
STATE
STATE
BROADWAY
RICHARDSON
RICHARDSON
RICHARDSON
STATE
STATE
MIDLAND
RICHARDSON
RICHARDSON
STATE
RICHARDSON
RICHARDSON
RIDGEWAY
00210001 Robo Chev LSA T4
ST
ST
ST
ST
ST
ST
ST
ST
AVE
AVE
ST
ST
ST
ST
ST,.
ST
ST
ST
ST
ST
ST
ST
ST
ST
BLVD
BLVD
BLVD
ST
ST
AVE
BLVD
BLVD
ST
BLVD
BLVD
AVE
May 19, 2010
Parcel
Number
0619368701
0619368793
0619368914
0619369165
0619369206
0619369529
0619369562
0619369659
0619370706
0619370825
0619370985
0619371362
0619371675
0619372049
0619372706
0619372824
0619372984
0619373082
0619373180
0619373198
0619373654
0619373739
0619374708
0619374787
0619374926
0619374995
0619375176
0619375275
0619375383
0619375475
0619375602
0619375757
0619375974
0619376465
0619376611
0619376680
TABLE3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 8 of 14
Owner/ Occupant Name
(Last, First Ml)
GREYBEARD REALTY LLC 204
CAMPBELL FAMILY INVESTMENTS LLC 206
TOMMY K BROWN ill REVOCABLE TRUST 217
SOBOL JR CT & BEYERL YB 115
KNOPP RAYMOND C 113
BROCK DOUGLAS M 106
SMALL MICAHEL D 112
HIPPS CLAYTON J & LOIS B 100
WESTMORELAND JANIE & ARTHUR HORN 307
KRAMP ERVIN H 309
WEST EDWARD B & ETHEL M 311
FIRST BAPTIST BLACK MOUNTAIN 130
BULLERDICK HOW ARD J TRUSTEE 200
STEPP-NICHOLS COMP ANY INC 106
CLARK JAMES W 204
LOVE JOHN E & WANDA E 206
WILLIAMS KERLEE C (LE) 300
PACE SHARON D 105
STEPP-NICHOLS COMP ANY INC 107
STEPP-NICHOLS COMP ANY INC 109
HOI.i.IFIELD LUCY R 103
PRUETT BARBARA A & SUSAN E 100
CANTRELL ALLEN F & JOANN T 102
SMITH OB & SHIRLEY 104
RIO JR ROGER J & JACQUELINE R 101
WORLEY GAIL M 103
BANNERMAN ROBERT C & JANET 200
POINTS JAMES F 99999
POINTS JAMES F 204
KISSLING PAUL T ET AL 202
CURTIS TL & PATRICIA 107
KEEVER JOSEPHINE F (LE) 106
EDELMAN DIANE E 105
PROPST JOHN N & DORISE 204
RACHMAN BRADLEY S 109
WATERSFRANKW &KAYO 111
Address
STATE
STATE
STATE
RICHARDSON
RICHARDSON
RIDGEWAY
RIDGEWAY
RIDGEWAY
MONTREAT
MONTREAT
MONTREAT
MONTREAT
MONTREAT
WEST
MONTREAT
MONTREAT
MONTREAT
MIDLAND
MIDLAND
MIDLAND
FIRST
SECOND
SECOND
SECOND
SECOND
SECOND
MIDLAND
MIDLAND
MIDLAND
FIRST
FIRST
SECOND
SECOND
FIRST
FIRST
FIRST
00210001 Robo Chev LSA T 4
ST
ST
ST
BLVD
BLVD
AVE
AVE
AVE:
RD
RD
RD
RD
RD
ST
RD
RD
RD
AVE
AVE
AVE
ST
ST
ST
ST
ST
ST
AVE
AVE
AVE
ST
ST
ST
ST
ST
ST
ST
May 19, 2010
Parcel
Number
0619376736
0619376944
0619377152
0619377235
0619377322
0619377444
0619377569
0619377705
0619377785
0619377923
0619378622
0619378755
0619378922
0619379602
0619379734
0619379839
0619379949
0619380009
0619380255
0619380433
0619380587
0619380733
0619381038
0619381135
0619381273
0619381320
0619381413
0619381560
0619381740
0619382301
0619382414
0619382517
0619382618
0619382712
0619383001
0619383028
TABLE3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 9 of 14
Owner/ Occupant Name
(Last, First Ml)
KEEVER JOSEPHINE F (LE) 99999
DICKENS BLANCHE 107
SW ANNANOA VALLEY CHRIST MIN INC 101
HOMETRUST BANK 203
LEVINSON ANNIE (LE) 205
WHICKER ELIZABETH G & CHAS COTRUSTE 207
POTEAT BETTY 113
PADGETT MACK H 110
SMITH DANNYE & CHRISTINA K 112
HARRISON JAMES N & MARGARET R 109
HAMMETT LOUISE MCKINNEY (LE) 115
WELSH EMILY E 114
VITELLI STEPHEN M & DIANA M 113
WILKS DAVID ALLEN 117
STUART DAVID B 105
ALLAN WILLIAM A 99999
ALLAN WILLIAM A 99999
COUNCEMARY 102
EDWARDS CHERYL B & ABB & RB 105
PADGETT ROBERT D & TERRY 102
SHELL SHERMAN L & LENA E 103
BDK PROPERTIES INC 104
GARY WELLS BALL TRUST 401
AMMONS BOBBY R & JOYCE W 403
AMMONS BOBBY R & JOYCE W 99999
CHHAY TONG C ETAL 103
MCINTOSH SHIRLEY A & EV A 100
RANDALL DEANNA 503
MONTGOMERY YVONNE M 102
POLK ill DEMPSEY F 407
COUNCILL RY AN MICHAEL 501
LIOTTA PHILIP 505
POLING JAMES N 100
MFH PROPERTIES LLC 601
TAYLOE CARL T & JANE C 302
ANDREWS DAVID H 304
Address
SECOND
SECOND
RIDGEWAY
RIDGEWAY
RIDGEWAY
RIDGEWAY
FIRST
SECOND
SECOND
SECOND
CHARLOTTE
SECOND
SECOND
FIRST
LOUISA
LOUISA
LOUISA
PINE
VIEW
VIEW
NINTH
NINTH
MONTREAT
MONTREAT
MONTREAT
VIEW
VIEW
MONTREAT
NINTH
MONTREAT
MONTREAT
MONTREAT
NINTH
MONTREAT
MONTREAT
MONTREAT
00210001 Robo Chev LSA T4
ST
ST
AVE
AVE
AVE
AVE
ST
ST
ST
ST
ST
ST
ST
ST ..
-. ST
ST
ST
ST
ST
ST
ST
ST
RD
RD
RD
.,
ST
ST
RD
ST
RD
RD
RD
ST
RD
RD
RD
May 19, 2010
Parcel
Number
0619383145
0619383256
0619383364
0619383471
0619383488
0619383780
0619384151
0619384259
0619384474
0619385099
0619385130
0619385238
0619385443
0619385624
0619385776
0619386208
0619386287
0619386422
0619386630
0619386755
0619387008
0619387296
0619387461
0619387589
0619387610
0619387724
0619388017
0619388568
0619388744
. 0619389294
0619389299
0619389671
0619389794
0619451021
0619451929
0619453318
TABLE 3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 10 of 14
Owner/ Occupant Name
(Last, First Ml)
ANDREWS DAVID H 100
MILTON JACK A & REBA L 400
STYER RITA FA YE 402
PROPST JOHN N & DORIS E 404
CHILTON WILLIAM R 100
UNITARIAN UNIVERSALIST SW ANNANOA 500
ANDREWS DAVID H 102
MCGINNIS RICHARD A 101
BLOZAN WILLIAM F & HE ERICKSON IT 102
SIMMONS GLORIA 106
BIGGSERICW 104
MCGINNIS RICHARD A 103
CARE BRIDGE CORPORATION 99999
STAFFORD ROBIN L 103
DILLINGHAM FRED M & ANN K 102
MCGINNIS RICHARD A 105
BOX JR ROBERT R & BELINDA J 107
CARE BRIDGE CORPORATION 99999
BLANKENSIIlP RHONDA S 105
PEEK SHELBA JEAN M 104
PROSISE TOM F & JANICE E 110
PETTIT THOMAS SCOTT 111
STAFFORD MARSHA GLENN 110
GETTYS MARY HELEN 109
NANNEY STUART A 107
RAINES MICHAEL L 106
COLLINS DOROTHY C 112
BARKER JR THOMAS W & MARYE 111
SECREST MARVIN E & DONNA F 110
ROSSDAVIDF 116
ENTELIS STEVEN J & LORRAINE P 118
MASON STEPHEN C & MARY G 113
WHEELON WALTER E & EVELYN A 103
BI-LOLLC 0
SOBOL JOHN WOODROW 141
BI-LOLLC 205
Address
THIRD
MONTREAT
MONTREAT
MONTREAT
FOURTH
MONTREAT
THIRD
THIRD
FOURTH
THIRD
THIRD
THIRD
FOURTH
FOURTH
FIFTH
THIRD
THIRD
FOURTH
FOURTH
FIFTH
THIRD
THIRD
FOURTH
FOURTH
FOURTH
FIFTH
THIRD
FOURTH
FIFTH
THIRD
THIRD
FOURTH
PORTMANVIILA
NC9
RICHARDSON
NC9
00210001 Robo Chev LSA T4
ST
RD
RD
RD
ST
RD
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
ST
RD
HWY
BLVD
HWY
May 19, 2010
Parcel
Number
0619457619
0619460017
0619460285
0619460336
0619460360
0619460402
0619460858
0619460880
0619461154
0619461200
0619461652
0619461721
0619462383
0619462441
0619462505
0619462796
0619462930
0619463038
0619463233
0619463473
0619463628
0619463671
0619464114
0619464452
0619464873
0619464928
0619465108
0619465423
0619465606
0619465649
0619465696
0619465702
0619465959
0619466350
0619466562
0619466838
TABLE3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 11 of 14
Owner/ Occupant Name
(Last, First Ml)
BLACK MOUNTAIN VENTURES LLC 99999
TOWN & COUNTRY FURNISHINGS MRK INC 117
BIDDIX DONALD E 134
KNOPP RAYMOND C 122
MELTONDAVIDC 132
THOMAS CYNTHIA F1TTS 118
PAPASPYROU EV ANGELIA 306
P APSPYROU EV ANGELIA 103
WOODY MICHAEL & DEBRA CHURCH 140
ALLISON CAROLE 136
GREEN ROBERT D 107
GREEN ROBERT D 105
RESPESS SR DANIEL J & LOUISE 133
HUDGINSNAS 131
MARYS TODD TRUST 103
COOKJRRUBE 102
THE STEPP-NICHOLS CO INC 308
HAMIL GEORGE H & ELAINE B 151
LEARNED THOMAS HENRY & DONNA LYNN 137
DA VIS JERRY R 102
MELTON DOROTHY W (LE) 104
SNEEDJOHNC 106
SHOOK CARMELLA S 301
DOTSON DOROTHY MAE (LE) 104
HELGREBN JAMES NE ET AL 103
BILLIE-WORTH ENTERPRISES INC 400
SHOOK CARMELLA S 99999
DOTSON RONNIE & AUDREY 106
PRUITT CONNIE L 107
CAMPBELL JOHN DOUGLAS 111
CAMPBELL JOHN DOUGLAS 111
HALLMAN EILEEN 105
DUARTE MARCUS 404
LANDRAW I LLC 134
COSMIC KIDS LLC 130
CHHAY TONG C & SEAR M 410
Address
HEMPHILL
RICHARDSON
RIDGEWAY
RIDGEWAY
RIDGEWAY
RIDGEWAY
STATE
RIDGEWAY
RIDGEWAY
RIDGEWAY
RIDGEWAY
RIDGEWAY
RIDGEWAY
RIDGEWAY
CENTER
SCOTLAND
STATE
RIDGEWAY
RIDGEWAY
CENTER
SCOTLAND
SCOTLAND
SUTTON
CENTER
SCOTLAND
STATE
SUTTON
CENTER
SCOTLAND
CENTER
CENTER
SCOTLAND
STATE
CENTER
CENTER
STATE
00210001 Robo Chev LSA T 4
RD
BLVD
AVE
AVE
AVE
AVE
ST
AVE
AVE
AVE
AVE
AVE
AVE
AVE
AVE
ST
ST
AVE
AVE
AVE
ST
ST
AVE
AVE
ST
ST
AVE
AVE
ST
AVE
AVE
ST
ST
AVE
AVE
ST
May 19, 2010
Parcel
Number
0619467281
0619467396
0619467673
0619468855
0619470681
0619470780
0619470786
0619470892
0619470898
0619471907
0619472269
0619474537
0619474773
0619474905
0619476993
0619478177
0619478464
0619478893
0619480194
0619480305
0619480405
0619484330
0619484511
0619485049
0619486229
0619487258
0619488257
0619489007
0619489247
0619489309
0619489500
0619489519
0619489614
0619489720
0619543923
0619546910
TABLE 3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 12 of 14
Owner/ Occupant Name
(Last, First Ml)
RELIGIOUS SOCIETY OF FRIENDS 137
LANDRAW I LLC 138
ROBINSON WILLIAM D & BARBARA L 129
BLACK MOUNTAIN MINI STORAGE LLC 440
BUNC CTY BRD OF EDUCATION 99999
STUDENCWILLIAMJETAL 104
RICE REV JAMES N 106
BROWNINGJAMESE 108
BYERS WILLIAM PAUL & TRISHA K TE 110
MAIN REVOCABLE LIVING TRUST 112
BUNC CTY BRD OF EDUCATION 301
BUNC CTY BRD OF EDUCATION 99999
BROWNJOHNP 109
MAIN REVOCABLE LIVING TRUST 99999
DIERING MARK R 2
GARRETT DAVID H ET AL 401
INSPIRE CORPORATION 105
GARRETT BLAKE PET AL 103
MAIN REVOCABLE LIVING TRUST 114
HAAS IRENE 120
VADEN STERLING A 100
HART SAMUEL & KATHY 110
THE STEPP-NICHOLS CO INC 201
BLACK MOUNTAIN MASONIC LODGE# 663 105
JONES PAUL W & JOYCE ANN M 108
NIXHELENR 102
COTHERN RANDY B & DENISE B 100
EAST BLACK MOUNTAIN FREE WILL 195
CRISP MARY LOUISE 209
FOXX FORREST W 213
BARTLETT RICKY F & VANESSA 99999
BARTLETT RICKY F & VANESSA 219
MENZEL JEFFREY 221
BRUMMETT MATTHEW WELLES 223
BEGLEY RUBY B 6
BEGLEY RUBY B 99999
Address
CENTER
CENTER
CENTER
STATE
CHARLOTTE
LOUISA
LOUISA
LOUISA
LOUISA
LOUISA
STATE
CHARLOTTE
CHARLOTTE
LOUISA
VILLAGE
STATE
FLAT CREEK
FLAT CREEK
LOUISA
THIRD
PORTMAN VILLA
ROCK CHURCH
DAVIS
ROCK CHURCH
ROCK CHURCH
ROCK CHURCH
ROCK CHURCH
FLATCREEK
FLATCREEK
FLAT CREEK
FLAT CREEK
FLAT CREEK
FLATCREEK
FLAT CREEK
VANCE
VANCE
00210001 Robo Chev LSA T 4
AVE
AVE
AVE
ST
ST
ST
ST
" ST
ST
ST
ST
ST
ST
ST
WAY
ST
RD
RD
ST
ST
RD
ST
DR
ST
ST
-sT
ST
RD
RD
RD
RD
RD
RD
RD
DR
DR
May 19, 2010
Parcel
Number
0619557327
0619561528
0619562789
0619565013
0619565694
0619571281
0619573729
0619574370
0619577748
0619580296
0619580385
0619580499
0619581008
0619581107
0619581509
0619581617
0619581726
0619582142
0619582214
0619582315
0619582429
0619582631
0619582762
0619583131
0619583383
0619583580
0619583772
0619584141
0619584383
0619584590
0619584781
0619585141
0619585383
0619585499
0619585780
1
TABLE3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 13 of 14
Owner/ Occupant Name
(Last, First Ml)
HEMPHILL JR ARTHUR J & MARY R 99999
TWO CREEKS PROPERTIES 99999
WELLS WILLIAM F & WILLIAM F III 460
BLACK MOUNTAIN VENTURES LLC 99999
BLACK MOUNTAIN VENTURES LLC 99999
RICKER JR CARL H & JANIS 101
BLACK MTN HIGH SCHOOL 150
RICKER JR CARL H 133
BRADEN DONALD R & DEBORAH H 99999
RATHBONE JUSTIN & CATHY G 108
CLUBB JUDY MAMMONS 110
ANN SMITH 216
WILLIAMSON DAVID 104
QUINNLORIM 106
MORRIS ROBERT A & LORI W 220
STAFFORD WILLIAM HENRY 222
LEWIS II JAMES M & CHERYL W 224
CLOUD REX D & JEANETTE S 104
TRANTHAM ALICE WALKER 102
ANDERSON WALLACE L & ELLEN M 100
STURDNANT CYNTHIA & E WARLICK UI J 101
ST AFFORD CORA S 103
MARETT YVONNE WHITSON 105
WILMOT KATHRYN R 106
REID SANDRA M 101
BARTLETT KEVIN DEWAYNE & ASHLEY A 100
NIGHTINGALE RAYMOND PAUL 107
FOREDANNYC 108
FLYNN RONNIE B & LINDA D 103
SHOWERS CARLOS L & SHEILAH 102
WHEELER MCKINLEY R & BETTY 109
POOLE NANCY A 110
HERSEY BARBARA M 105
RICE JANELL W 104
KIENTZ CHRISTINE A 111
REITZEL PROPERTIES LLC 206
Address
SUNSET
STATE
STATE
HEMPHILL
STATE
OLDUS70
FLAT CREEK
OLDUS70
PADGETTOWN
FLATCREEK
FLAT CREEK
FLAT CREEK
FLAT CREEK
FLAT CREEK
FLAT CREEK
FLAT CREEK
FLAT CREEK
PINETREE
PINETREE
PINETREE
BEECHTREE
BEECHTREE
BEECHTREE
PINETREE
PINETREE
BEECHTREE
BEECHTREE
PINETREE
PINETREE
BEECHTREE
BEECHTREE
PINETREE
PINETREE
BEECHTREE
BEECHTREE
RIDGEWAY
00210001 Robo Chev LSA T4
DR
ST
ST
RD
ST
HWY
RD
HWY
RD
RD
RD.
RD
RD
RD
RD'
RD
RD
DR
DR
DR
DR
DR
DR
DR
DR
DR
DR
DR
DR
DR
DR
DR
DR
DR
DR
AVE
May 19, 2010
Parcel
Number
2'
3'
4'
5'
6'
TABLE3
PROPERTY OWNERS/OCCUPANTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 14 of 14
Owner/ Occupant Name
(Last, First Ml)
CAMPBEIL FAMILY INVESTMENTS LLC 206
ARSENAULT ASSETS LLC 206
GREYBEARD REALTY ILC 206
REITZEL PROPERTIES ILC 206
CAMPBEIL FAMILY INVESTMENTS ILC 206
Address
RIDGEWAY
RIDGEWAY
RIDGEWAY
RIDGEWAY
RIDGEWAY
00210001 Robo Chev LSA T 4
AVE
AVE
AVE
AVE
AVE
May 19, 2010
1 0619466562
2 0619467281
3 0619470681
4 0619472269
5 0619474537
6 0619465959
7 0619485049
8 0619489007
9 0619573729
10 0619574370
11 0619268080
12 0619268722
13 0619371362
14 0619360339
15 0619377152
16 0619369659
17 0619368793
TABLE 4
SENSITIVE LAND-USE FEATURES
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 1 of 1
COSMIC KIDS LLC C-2
RELIGIOUS SOCIETY OF FRIENDS C-2
BUNC CTY BRO OF EDUCATION Govt Owned R-10
BUNG CTY BRO OF EDUCATION Govt Owned C-2
BUNC CTY BRO OF EDUCATION Govt Owned C-2
DUARTE MARCUS Diner C-2
Moose, E ks,
BLACK MOUNTAIN MASONIC LODGE# 663 Veterans C-2
EAST BLACK MOUNTAIN FREE WILL Church Bldg C-2
BLACK MTN HIGH SCHOOL Govt Owned C-2
RICKER JR CARL H Strip Shop Ctr C-2
BLACK MOUNTAIN UNITED METHODIST Church Bldg C-1, C-2, R-10
BLACK MOUNTA N PRESBYTER AN
CHURCH Church Bldg C-2
FIRST BAPTIST BLACK MOUNTAIN Church Bldg C-2
BLACK MTN PRESBYTERIAN CHURCH Religious C-1
SWANNANOA VALLEY CHRIST MIN INC Charity/Welfare C-1, C-2
HIPPS CLAYTON J & LOIS B Restaurant C-1
CAMPBELL FAMILY INVESTMENTS LLC Condominiums C-1
00210001 Robo Chev LSA T4
5/12/2010 560 e
5/12/2010 1225 e
5/12/2010 1370 ne
5/12/2010 850 ne
5/12/2010 1525 ne
5/12/2010 1225 ene
5/12/2010 1700 nne
5/12/2010 1550 ne
5/12/2010 1625 ne
. 5/12/2010 1540 ene
5/12/2010 1610 SW
5/12/2010 1130 wnw
5/12/2010 980 nw
5/12/2010 840 WSW
5/12/2010 450 feet n
5/12/2010 150 feet se
5/12/2010 adjacent e
May 19, 2010
00210001 ROBO Chev LSA TS
TABLE 5
PUBLIC WATER SYSTEMS
Limited Site Assessment
ROBO Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 1 of 1
May 19, 2010
MW-2 4/9/2010
TABLE 6
WELL CONSTRUCTION DETAILS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 1 of 1
* Reference Point for Elevation Measurements: Estimated from USGS topographic map
bgs = below ground surface
00210001 Robo Chev LSA T6
11 0 2374
May 19, 2010
TABLE 7
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
Limited Site Assessment
Robo Chevron Station
Black Mountain, North Carolina
Incident No. 28789
Page 1 of 1
LSA LSA 2L Groundwater Gross
MW-1 MW-2 Quality Contamination
4/9/2010 4/9/2010 Standards Level
Petroleum Hydrocarbon Fractions (ug/L) (ug/L) (ug/L) (ug/L)
(MADEP Methods)
C05-C08 Aliphatics (VPH) NA NA
C09-C12 Aliphatics (VPI-2,120 1,060 NA NA
C9-C18 Aliphatics (EPH) 292 3820 NA NA
Total C9-C18 Aliphatics 2412 4880 NA NA
C19-C36 Aliphatics (EPH) 648 NA NA
C9-C10 Aromatics (VPH 353 NA NA
C11-C22 Aromatics (EP~ 911 3600 NA NA
Total C9-C22 Aromatic! 911 3953 NA NA
Semivolatile Organic Compounds
(EPA Method 625)
Fluorene 10.8 300 990
Naphthalene 15.4 44.1 6 6000
Phenanthrene 8.9 200 410
I
Volatile Organic Compounds
(EPA Method 62008)
Benzene 209 9.2 1 5000
n-Butylbenzene 3.6 8.3 70 6900
sec-Butyl benzene 6.3 17.8 70 8500
tert-Butylbenzene 2.6 70 15000
Diisopropyl ether 4.5 70 70000
Ethylbenzene 58.6 46.9 600 84500
lsopropylbenzene 8.5 24.0 70 25000
Methyl-tert-butyl ether 1.5 3.4 20 20000
Naphthalene 31.5 183 6 6000
n-Propylbenzene 10.1 27.3 70 30000
Toluene 44.1 600 260000
1,2,4-Trimethylbenzene 6.2 400 28500
1,3,5-Trimethylbenzene 1.1 400 25000
m&p-Xylene 37.4 1.2 500 85500 a-Xylene 3.2
00210001 Robo Chev LSA T7 May 19, 2010
FIGURES
!COO
BLACK MOUNTAIN QUADRANGLE
NORTH CAROLINA
7 .5 MINUTE SERIES (TOPOGRAPIITC)
0
I i"
1000
..
SCALE 1:24 000
0
2000 4000 5000 6000.
I MILE
7000 FEET
I .5
~ F3
3000
0 I KILOMETER
JORDAN ENVIRONMENTAL, LLC
68 Little Horse Road
Waynesville, NC 28786
f-+-3 f
CONTOUR INTERVAL 20 FEET
NATIONAL GEODETIC VERTICAL DATUM OF 1929
Figure 1
Site Map
Robo Chevron Station-Black Mountain, NC
~ ~Walodinll~ ~✓
P. 0. Box 1107
Candler, NC 28715-1107
WaterllnksPLLC.com
East State Street US HWY 70
SCALE
1 inch= 15 feet
0
Soil-D I BK-3
BD-\ • J
sc1fc'•••7
15
Asphalt
I
I
I
L
L• ~oil-E •,S~ Bulk Dispenser
_._ Fueling Shed
Soil-B
0MW-1
Soil Excavation
Area
Jordan Environmental, LLC
68 Little Horse Rd
Waynesville, NC 28786
Asphalt
UST Location
,{
I
, • DD-1
_j0MW-2
Asphalt
Figure 2
Site Map
Canopy
Robo Chevron
Station
Car Wash
LEGEND
>--
• Soil Sample Location
0 Monitoring Well Location
en (')
0 tt
Q)
::::l a.
en -co
CD -
~ ~ Waterlink~
Office [phone] Robo Chevron Station -Black Mountain, NC
~✓
P. 0. Box 1107
Candler, NC 28715-1107
WaterlinksPLLC.com
Jordan Environmental, LLC
68 Little Horse Rd
Waynesville, NC 28786
Figure 3
POTENTIAL RECEPTOR MAP
ROBO Chevron Station-Black Mountain, NC
Receptor
~ ~ Waterlinh%
'-.p~¥"'
P. o. Box 1107
Candler, NC 28715-1107
WaterlinksPLLC.com
N
APPENDIX A
Laboratory Analytical Reports and Chain of Custody Documentation
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
April 30, 201 O
Mr. Baker Jordan
Jordan Environmental, LLC
68 Little Horse Road
Waynesville, NC 28786
RE: Project: Robo Chevron
Pace Project No.: 9267551
Dear Mr. Jordan:
Enclosed are the analytical results for sample(s) received by the laboratory on April 16, 2010. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All.
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
o-f~-~
Lorri Patton
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
O '" ACco,,,D
~ -i 1
Page 1 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Charlotte Certification IDs
Kentucky UST Certification #: 84
Louisiana/LELAP Certification #: 04034
Connecticut Certification#: PH-0104
Pace Analytical Services, Inc.
2225 Riverside Dr.
CERTIFICATIONS
Asheville, NC 28804
[phone]
South Carolina Certification#: 99006001
Pennsylvania Certification #: 68-00784
North Carolina Wastewater Certification#: 12
9800 Kincey' Ave. -Ste 100 Huntersville, NC 28078 North Caronna Field Services Certification #: 5342
North Carolina Drinking Water Certification #: 37706
New Jersey Certification#: NC012
West Virginia Certification #: 357
Virginia Certification#: 00213
Tennessee Certification #: 04010
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
------·-----------------------
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-A
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551001 Collected: 04/16/10 10:30 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Nonatriacontane (S)
o-Terphenyl (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
VPH NC Soil
Aliphatic (C05-C08)
Aliphatic (C09-C12)
Aromatic (C09-C10)
2,5-Dibromotoluene (PID)(S)
2,5-Dibromotoluene (FID)(S)
8270 MSSV Microwave
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Date: 04/30/2010 06:21 PM
Results Units Report Limit OF Prepared Analyzed
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
235 mg/kg 63.3 5 04/19/10 14:55 04/21/10 10:46
ND mg/kg 63.3 5 04/19/10 14:55 04/21/10 10:46
190 mg/kg 25.3 2 04/19/10 14:55 04/21/10 10:46
0% 40-140 5 04/19/10 14:55 04/21/10 10:46
151 % 40-140 2 04/19/10 14:55 04/21/10 10:46
188 % 40-140 2 04/19/10 14:55 04/21/10 10:46
457 % 40-140 2 04/19/10 14:55 04/21/10 10:46
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
ND mg/kg
ND mg/kg
ND mg/kg
100 %
114 %
Analytical Method: EPA 8270
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
· 0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
o.o mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
9.8
9.8
9.8
70-130
70-130
1
1
1
1
1
1
1
04/19/10 13:31 04/19/10 19:46
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04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
04/29/10 18:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
GAS No. Qual
7194-86-7 S4
84-15-1 S5
321-60-8 S5
580-13-2 S5
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
101-55-3
85-68-7
59-50-7
10647-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
95-50-1
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
Page 3 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-A
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551001 Collected: 04/16/10 10:30 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV Microwave
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol( o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
8260/5035A Volatile Organics
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Date: 04/30/2010 06:21 PM
Results Units
Analytical Method: EPA 8270
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0051 mg/kg
0.0 mg/kg
0.0073 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.024 mg/kg
0.023 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0035 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.017 mg/kg
0.0 mg/kg
0.0018 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
Analytical Method: EPA 8260
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
Report Limit OF Prepared
4.7 50
0.24 50
0.24 50
0.24 50
0.24 50
0.24 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
'I) \1' ACConb
~ -~ ~ ~ ~
Analyzed CAS No. Qual
04/29/10 18:28 105-67-9
04/29/10 18:28 131-11-3
04/29/10 18:28 84-74-2
04/29/10 18:28 534-52-1
04/29/10 18:28 51-28-5
04/29/10 18:28 121-14-2
04/29/10 18:28 606-20-2
04/29/10 18:28 117-84-0
04/29/10 18:28 117-81-7
04/29/10 18:28 206-44-0
04/29/10 18:28 86-73-7
04/29/10 18:28 87-68-3
04/29/10 18:28 118-74-1
04/29/10 18:28 77-47-4
04/29/10 18:28 67-72-1
04/29/10 18:28 193-39-5
04/29/10 18:28 78-59-1
04/29/10 18:28 90-12-0
04/29/10 18:28 91-57-6
04/29/10 18:28 95-48-7
04/29/10 18:28
04/29/10 18:28 91-20-3
04/29/10 18:28 88-74-4
04/29/10 18:28 99-09-2
04/29/10 18:28 100-01-6
04/29/10 18:28 98-95-3
04/29/10 18:28 88-75-5
04/29/10 18:28 100-02-7
04/29/10 18:28 62-75-9
04/29/10 18:28 621-64-7
04/29/10 18:28 86-30-6
04/29/10 18:28 87-86-5
04/29/10 18:28 85-01-8
04/29/10 18:28 108-95-2
04/29/10 18:28 129-00-0
04/29/10 18:28 120-82-1
04/29/10 18:28 95-95-4
04/29/10 18:28 88-06-2
04/20/10 18:30 67-64-1
04/20/10 18:30 71-43-2
04/20/10 18:30 108-86-1
04/20/10 18:30 74-97-5
04/20/10 18:30 75-27-4
04/20/10 18:30 75-25-2
Page 4 of38
wwvv.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-A Lab ID:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
9267551001 Collected: 04/16/10 10:30 Received: 04/16/10 14:55
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CASNo. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromomethane ND mg/kg 0.47 50 04/20/10 18:30 74-83-9
2-Butanone (MEK) ND mg/kg 4.7 50 04/20/10 18:30 78-93-3
n-Butylbenzene ND mg/kg 0.24 50 04/20/10 18:30 104-51-8
sec-Butyl benzene ND mg/kg 0.24 50 04/20/10 18:30 135-98-8
tert-Butylbenzene ND mg/kg 0.24 50 04/20/10 18:30 98-06-6
Carbon tetrachloride ND mg/kg. 0.24 50 04/20/10 18:30 56-23-5
Chlorobenzene ND mg/kg 0.24 50 04/20/10 18:30 108-90-7
Chloroethane ND mg/kg 0.47 50 04/20/10 18:30 75-00-3
Chloroform ND mg/kg 0.24 50 04/20/10 18:30 67-66-3
Chloromethane ND mg/kg 0.47 50 04/20/10 18:30 74-87-3
2-Chlorotoluene ND mg/kg 0.24 50 04/20/10 18:30 95-49-8
-4-Chlorotoluene ND mg/kg 0.24 50 04/20/10 18:30 106-43-4
1,2-Dibromo-3-chloropropane ND mg/kg 0.24 50 04/20/10 18:30 96-12-8
Dibromochloromethane ND mg/kg 0.24 50 04/20/10 18:30 124-48-1
1,2-Dibromoethane (EDB) ND mg/kg 0.24 50 04/20/10 18:30 106-93-4
Dibromomethane ND mg/kg 0.24 50 04/20/10 18:30 74-95-3
1,2-Dichlorobenzene ND mg/kg 0.24 50 04/20/10-18:30 95-50-1
1,3-Dichlorobenzene ND mg/kg 0.24 50 04/20/10 18:30 541-73-1
1,4-Dichlorobenzene ND mg/kg 0.24 50 04/20/10 18:30 106-46-7
Dichlorodifluoromethane ND mg/kg 0.47 50 04/20/10 18:30 75-71-8. D3
1 , 1-Dichloroethane ND mg/kg 0.24 50 04/20/10 18:30 75-34-3,
1,2-Dichloroethane ND mg/kg 0.24 50 04/20/10 18:30 107-06-2
1, 1-Dichloroethene ND mg/kg 0.24 50 04/20/10 18:30 75-35-4
cis-1,2-Dichloroethene ND mg/kg 0.24 50 04/20/10 18:30 156.,59-2
trans-1,2-Dichloroethene ND mg/kg 0.24 50 04/20/10 18:30 156-60-5
1,2-Dichloropropane ND mg/kg 0.24 50 04/20/10 18:30 78-87-5
1,3-Dichloropropane ND mg/kg 0.24 50 04/20/10 18:30 142-28-9
2,2-Dichloropropane ND mg/kg 0.24 50 04/20/10 18:30 594-20-7
1, 1-Dichloropropene ND mg/kg 0.24 50 04/20/10 18:30 563-58-6
cis-1,3-Dichloropropene ND mg/kg 0.24 50 04/20/10 18:30 10061-01-5
trans-1,3-Dichloropropene ND mg/kg 0.24 50 04/20/10 18:30 10061-02-6
Diisopropyl ether ND mg/kg 0.24 50 04/20/10 18:30 108-20-3
Ethyl benzene ND mg/kg 0.24 50 04/20/10 18:30 100-41-4
Hexachloro-1,3-butadiene ND mg/kg 0.24 50 04/20/10 18:30 87-68-3
2-Hexanone ND mg/kg 2.4 50 04/20/10 18:30 591-78-6
lsopropylbenzene (Cumene) ND mg/kg 0.24 50 04/20/10 18:30 98-82-8
p-lsopropyltoluene ND mg/kg 0.24 50 04/20/10 18:30 99-87-6
Methylene Chloride ND mg/kg 0.95 50 04/20/10 18:30 75-09-2
4-Methyl-2-pentanone (MIBK) ND mg/kg 2.4 50 04/20/10 18:30 108-10-1
Methyl-tert-butyl ether ND mg/kg 0.24 50 04/20/10 18:30 1634-04-4
Naphthalene ND mg/kg 0.24 50 04/20/10 18:30 91-20-3
n-Propylbenzene ND mg/kg 0.24 50 04/20/10 18:30 103-65-1
Styrene ND mg/kg 0.24 50 04/20/10 18:30 100-42-5
1, 1, 1,2-Tetrachloroethane ND mg/kg 0.24 50 04/20/10 18:30 630-20-6
1, 1,2,2-Tetrachloroethane ND mg/kg 0.24 50 04/20/10 18:30 79-34-5
Tetrachloroethene ND mg/kg 0.24 50 04/20/10 18:30 127-18-4
Date: 04/30/2010 06:21 PM REPORT OF LABORATORY ANALYSIS Page 5 of38
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
0 ~ ~ -i 1
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-A Lab ID:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
9267551001 Collected: 04/16/10 10:30 Received: 04/16/10 14:55
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260/5035A Volatile Organics
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
T richloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
a-Xylene
Dibromofluoromethane (S)
Toluene-dB (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 04/30/2010 06:21 PM
Results Units Report Limit DF Prepared
Analytical Method: EPA 8260
ND mg/kg 0.24 50
ND mg/kg 0.24 50
ND mg/kg 0.24 50
ND mg/kg 0.24 50
ND mg/kg 0.24 50
ND mg/kg 0.24 50
ND mg/kg 0.24 50
ND mg/kg 0.24 50
ND mg/kg 0.24 50
ND mg/kg 0.24 50
ND mg/kg 2.4 50
ND mg/kg 0.47 50
ND mg/kg 0.47 50
ND mg/kg 0.24 50
90 % 79-116 50
99 % 88-110 50
101 % 74-115 50
86 % 69-121 50
Analytical Method: ASTM D2974-87
21.0 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
0 ,• ,cco•o
~ i ;
Analyzed CASNo. Qual
04/20/10 18:30 108-88-3
04/20/10 18:30 87-61-6
04/20/10 18:30 120-82-1
04/20/10 18:30 71-55-6
04/20/10 18:30 79-00-5
04/20/10 18:30 79-01-6
04/20/10 18:30 75-69-4
04/20/10 18:30 96-18-4
04/20/10 18:30 95-63-6
04/20/10 18:30 108-67-8
04/20/10 18:30 108-05-4
04/20/10 18:30 75-01-4
04/20/10 18:30 1330-20-7
04/20/10 18:30 95-47-6
04/20/10 18:30 1868-53-7
04/20/10 18:30 2037-26-5
04/20/10 18:30 460-00-4
04/20/10 18:30 17060-07-0
04/23/10 13:44
Page 6 of38
l'.WW.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-B
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551002 Collected: 04/16/10 10:45 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Nonatriacontane (S)
o-Terphenyl (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
VPH NC Soil
Aliphatic (Cci5-C08)
Aliphatic (C09-C12)
Aromatic (C09-C1 0)
2,5-Dibromotoluene (PID)(S)
2,5-Dibromotoluene (FID)(S)
8270 MSSV Microwave
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
BenzoicAcid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Date: 04/30/2010 06:21 PM
Results Units Report Limit DF Prepared
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
319 mg/kg 123 10 04/19/10 14:55
ND mg/kg 123 10 04/19/10 14:55
217 mg/kg 24.6 2 04/19/10 14:55
0% 40-140 10 04/19/10 14:55
154 % 40-140 2 04/19/10 14:55
222 % 40-140 2 04/19/10 14:55
251 % 40-140 2 04/19/10 14:55
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
ND mg/kg
68.6 mg/kg
23.0 mg/kg
152 %
262 %
Analytical Method: EPA 8270
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
9.1
9.1
9.1
70-130
70-130
04/19/10 13:31
04/19/10 13:31
04/19/.10 13:31
04/19/10 13:31
04/19/10 13:31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed GAS No. Qual
04/21/10 11 :22
04/21/10 11 :22
04/21/10 11 :22
04/21/10 11:22 7194-86-7 S4
04/21/10 11:22 84-15-1 S5
04/21/10 11:22 321-60-8 S5
04/21/10 11:22 580-13-2 S5
04/19/10 20:10
04/19/10 20:10
04/19/10 20: 10
04/19/10 20:10 S5
04/19/10 20:10 S5
04/29/10 18:56 83-32-9
04/29/10 18:56 208-96-8
04/29/10 18:56 120-12-7
04/29/10 18:56 56-55-3.
04/29/10 18:56 50-32-8
04/29/10 18:56 205-99-2
04/29/10 18:56 191-24-2
04/29/10 18:56 207-08-9
04/29/10 18:56 65-85-0
04/29/10 18:56 100-51-6
04/29/10 18:56 101-55-3
04/29/10 18:56 85-68-7
04/29/10 18:56 59-50-7
04/29/10 18:56 10647-8
04/29/10 18:56 111-91-1
04/29/10 18:56 111-44-4
04/29/10 18:56 108-60-1
04/29/10 18:56 91-58-7
04/29/10 18:56 95-57-8
04/29/10 18:56 7005-72-3
04/29/10 18:56 218-01-9
04/29/10 18:56 53-70-3
04/29/10 18:56 132-64-9
04/29/10 18:56 95-50-1
04/29/10 18:56 541-73-1
04/29/10 18:56 106-46-7
04/29/10 18:56 91-94-1
04/29/10 18:56 120-83-2
04/29/10 18:56 84-66-2
Page 7 of38
IWMl.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-B
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551002 Collected: 04/16/10 10:45 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV Microwave
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno{1,2,3-cd)pyrene
lsophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-T richlorophenol
2,4,6-Trichlorophenol
8260I5035A Volatile Organics
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Date: 04/30/2010 06:21 PM
Results Units
Analytical Method: EPA 8270
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0053 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0088 mg/kg
0.0023 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0098 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
Analytical Method: EPA 8260
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
Report Limit DF Prepared
1
10.4 100
0.52 100
0.52 100
0.52 100
0.52 100
0.52 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed CASNo. Qual
04/29/10 18:56 105-67-9
04/29/10 18:56 131-11-3
04/29/10 18:56 84-74-2
04/29/10 18:56 534-52-1
04/29/10 18:56 51-28-5
04/29/10 18:56 121-14-2
04/29/10 18:56 606-20-2
04/29/10 18:56 117-84-0
04/29/10 18:56 117-81-7
04/29/10 18:56 206-44-0
04/29/10 18:56 86-73-7
04/29/10 18:56 87-68-3
04/29/10 18:56 118-74-1
04/29/10 18:56 77-47-4
04/29/10 18:56 67-72-1
04/29/10 18:56 193-39-5
04/29/10 18:56 78-59-1
04/29/10 18:56 90-12-0
04/29/10 18:56 91-57-6
04/29/10 18:56 95-48-7
04/29/10 18:56
04/29/10 18:56 91-20-3
04/29/10 18:56 88-74-4
04/29/10 18:56 99-09-2
04/29/10 18:56 100-01-6
04/29/10 18:56 98-95-3
04/29/10 18:56 88-75-5
04/29/10 18:56 100-02-7
04/29/10 18:56 62-75-9
04/29/10 18:56 621-64-7
04/29/10 18:56 86-30-6
04/29/10 18:56 87-86-5
04/29/10 18:56 85-01-8
04/29/10 18:56 108-95-2
04/29/10 18:56 129-00-0
04/29/10 18:56 120-82-1
04/29/10 18:56 95-95-4
04/29/10 18:56 88-06-2
04/21/10 03:00 67-64-1
04/21/10 03:00 71-43-2
04/21/10 03:00 108-86-1
04/21/10 03:00 74-97-5
04/21/10 03:00 75-27-4
04/21/10 03:00 75-25-2
Page 8 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-B lab ID:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
{828)254-7176
ANALYTICAL RESULTS
9267551002 Collected: 04/16/10 10:45 Received: 04/16/10 14:55
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromomethane ND mg/kg 1.0 100 04/21/10 03:00 74-83-9
2-Butanone (MEK) ND mg/kg 10.4 100 04/21/10 03:00 78-93-3
n-Butylbenzene ND mg/kg 0.52 100 04/21/10 03:00 104-51-8
sec-Butyl benzene ND mg/kg 0.52 100 04/21/10 03:00 135-98-8
tert-Butylbenzene ND mg/kg 0.52 100 04/21/10 03:00 98-06-6
Carbon tetrachloride ND mg/kg 0.52 100 04/21/10 03:00 56-23-5
Chlorobenzene ND mg/kg 0.52 100 04/21/10 03:00 108-90-7
Chloroethane ND mg/kg 1.0 100 04/21/10 03:00 75-00-3
Chloroform ND mg/kg 0.52 100 04/21/10 03:00 67-66-3
Chloromethane ND mg/kg 1.0 100 04/21/10 03:00 74-87-3
2-Chlorotoluene ND mg/kg 0.52 100 04/21/10 03:00 95-49-8
4-Chlorotoluene ND mg/kg 0.52 100 04/21/10 03:00 106-43-4
1,2-Dibromo-3-chloropropane ND mg/kg 0.52 100 04/21/10 03:00 96-12-8
Dibromochloromethane ND mg/kg 0.52 100 04/21/10 03:00 124-48-1
1,2-Dibromoethane (EDB) ND mg/kg 0.52 100 04/21/10 03:00 106-93-4
Dibromomethane ND mg/kg 0.52 100 04/21/10 03:00 74-95-3
1,2-Dichlorobenzene ND mg/kg 0.52 100 04/21/10 03:00 95-50-1
1,3-Dichlorobenzene ND mg/kg 0.52 100 04/21/10 03:00 541-73-1
1,4-Dichlorobenzene ND mg/kg 0.52 100 04/21/10 03:00 106-46-7
Dichlorodifluoromethane ND mg/kg 1.0 100 04/21/10 03:00 75-71-8 03
1, 1-Dichloroethane ND mg/kg 0.52 100 04/21/10 03:00 75-34-3
1,2-Dichloroethane ND mg/kg 0.52 100 04/21/10 03:00 107-06-2
1, 1-Dichloroethene ND mg/kg 0.52 100 04/21/10 03:00 75-35-4
.cis-1,2-Dichloroethene ND mg/kg 0.52 100 04/21/10 03:00 156-59-2
trans-1,2-Dichloroethene ND mg/kg 0.52 100 04/21/10 03:00 156-60-5
1,2-Dichloropropane ND mg/kg 0.52 100 04/21/10 03:00 78-87-5
1,3-Dichloropropane ND mg/kg 0.52 100 04/21/10 03:00 142-28-9
2,2-Dichloropropane ND mg/kg 0.52 100 04/21/10 03:00 594-20-7
1, 1-Dichloropropene ND mg/kg 0.52 100 04/21/10 03:00 563-58-6
cis-1,3-Dichloropropene ND mg/kg 0.52 100 04/21/10 03:00 10061-01-5
trans-1,3-Dichloropropene ND mg/kg 0.52 100 04/21/10 03:00 10061-02-6
Diisopropyl ether ND mg/kg 0.52 100 04/21/10 03:00 108-20-3
Ethyl benzene ND mg/kg 0.52 100 04/21/10 03:00 100-41-4
Hexachloro-1,3-butadiene ND mg/kg 0.52 100 04/21/10 03:00 87-68-3
2-Hexanone ND mg/kg 5.2 100 04/21/10 03:00 591-78-6
lsopropylbenzene (Cumene) ND mg/kg 0.52 100 04/21/10 03:00 98-82-8
p-lsopropyltoluene ND mg/kg 0.52 100 04/21/10 03:00 99-87-6
Methylene Chloride ND mg/kg 2.1 100 04/21/10 03:00 75-09-2
4-Methyl-2-pentanone (MIBK) ND mg/kg 5.2 100 04/21/10 03:00 108-10-1
Methyl-tert-butyl ether ND mg/kg 0.52 100 04/21/10 03:00 1634-04-4
Naphthalene 0.59 mg/kg 0.52 100 04/21/10 03:00 91-20-3
n-Propylbenzene ND mg/kg 0.52 100 04/21/10 03:00 103-65-1
Styrene ND mg/kg 0.52 100 04/21/10 03:00 100-42-5
1, 1, 1,2-Tetrachloroethane ND mg/kg 0.52 100 04/21/10 03:00 630-20-6
1, 1,2,2-Tetrachloroethane ND mg/kg 0.52 100 04/21/10 03:00 79-34-5
Tetrachloroethene ND mg/kg 0.52 100 04/21/10 03:00 127-18-4
Date: 04/30/2010 06:21 PM REPORT OF LABORATORY ANALYSIS Page 9 of38
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ ~ -:} ~ ~ ~
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-B
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551002 Collected: 04/16/10 10:45 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260/5035A Volatile Organics
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-T richloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Dibromofluoromethane (S)
Toluene-dB (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 04/30/2010 06:21 PM
Results Units Report Limit DF Prepared
Analytical Method: EPA 8260
ND mg/kg 0.52 100
ND mg/kg 0.52 100
ND mg/kg 0.52 100
ND mg/kg 0.52 100
ND mg/kg 0.52 100
ND mg/kg 0.52 100
ND mg/kg 0.52 100
ND mg/kg 0.52 100
ND mg/kg 0.52 100
ND mg/kg 0.52 100
ND mg/kg 5.2 100
ND mg/kg 1.0 100
ND mg/kg 1.0 100
ND mg/kg 0.52 100
104 % 79-116 100
102 % 88-110 100
100 % 74-115 100
102 % 69-121 100
Analytical Method: ASTM D2974-87
18.8 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
O '" ACColio
~ ! 1
Analyzed CAS No. Qual
04/21/10 03:00 108-88-3
04/21/10 03:00 87-61-6
04/21/10 03:00 120-82-1
04/21/10 03:00 71-55-6
04/21/10 03:00 79-00-5
04/21/10 03:00 79-01-6
04/21/10 03:00 75-69-4
04/21/10 03:00 96-18-4
04/21/10 03:00 95-63-6
04/21/10 03:00 108-67-8
04/21/10 03:00 108-05-4
04/21/10 03:00 75-01-4
04/21/10 03:00 1330-20-7
04/21/10 03:00 95-47-6
04/21/10 03:00 1868-53-7
04/21/10 03:00 2037-26-5
04/21/10 03:00 460-00-4
04/21/10 03:00 17060-07-0
04/23/10 13:45
Page 10 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-C
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551003 Collected: 04/16/10 11:00 Received: 04/16/1014:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18) 748 mg/kg 240 20 04/19/10 14:55 04/21/10 11:58
Aliphatic (C19-C36) ND mg/kg 240 20 04/19/10 14:55 04/21/10 11 :58
Aromatic (C11-C22) 395 mg/kg 60.0 5 04/19/10 14:55 04/21/1011 :58
Nonatriacontane (S) 0% 40-140 20 04/19/10 14:55 04/21/10 11:58 7194-86-7 S4
o-Terphenyl (S) 0% 40-140 5 04/19/10 14:55 04/21/10 11:58 84-15-1 S4
2-Fluorobiphenyl (S) 0% 40-140 5 04/19/10 14:55 04/21/10 11:58 321-60-8 S4
2-Bromonaphthalene (S) 0% 40-140 5 04/19/10 14:55 04/21/1011 :58 580-13-2 S4
VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (COS-COB) ND mg/kg 9.6 04/19/10 13:31 04/19/10 20:35
Aliphatic (C09-C12) 40.4 mg/kg 9.6 04/19/10 13:31 04/19/10 20:35
Aromatic (C09-C10) 14.0 mg/kg --9.6 04/19/10 13:31 04/19/10 20:35
2,5-Dibromotoluene (PID)(S) 135 % 70-130 04/19/10 13:31 04/19/10 20:35 S5
2,5-Dibromotoluene (FID)(S) 240 % 70-130 04/19/10 13:31 04/19/10 20:35 S5
8270 MSSV Microwave Analytical Method: EPA 8270
Acenaphthene 0.0 mg/kg 04/29/10 19:24 83-32-9
Acenaphthylene 0.0 mg/kg 04/29/10 19:24 208-96-8
Anthracene 0.0 mg/kg 04/29/10 19:24 120-12-7
Benzo(a)anthracene 0.0 mg/kg 04/29/10 19:24 56-55-3
Benzo(a)pyrene 0.0 mg/kg 04/29/10 19:24 50-32-8
Benzo(b)fluoranthene 0.0 mg/kg 04/29/10 19:24 205-99-2
Benzo(g,h,i)perylene 0.0 mg/kg 04/29/10 19:24 191-24-2
Benzo(k)fluoranthene 0.0 mg/kg 04/29/10 19:24 207-08-9
Benzoic Acid 0.0 mg/kg 04/29/10 19:24 65-85-0
Benzyl alcohol 0.0 mg/kg 1 04/29/10 19:24 100-51-6
4-Bromophenylphenyl ether o.o mg/kg 04/29/10 19:24 101-55-3
Butylbenzylphthalate 0.0 mg/kg 1 04/29/10 19:24 85-68-7
4-Chloro-3-methylphenol 0.0 mg/kg 1 04/29/10 19:24 59-50-7
4-Chloroaniline 0.0 mg/kg 04/29/10 19:24 106-47-8
bis(2-Chloroethoxy)methane 0.0 mg/kg 04/29/10 19:24 111-91-1
bis(2-Chloroethyl) ether 0.0 mg/kg 1 04/29/10 19:24 111-44-4
bis(2-Chloroisopropyl) ether 0.0 mg/kg 1 04/29/10 19:24 108-60-1
2-Chloronaphthalene 0.0 mg/kg 1 04/29/10 19:24 91-58-7
2-Chlorophenol 0.0 mg/kg 04/29/10 19:24 95-57-8
4-Chlorophenylphenyl ether 0.0 mg/kg 04/29/10 19:24 7005-72-3
Chrysene 0.0 mg/kg 04/29/10 19:24 218-01-9
Dibenz(a,h)anthracene 0.0 mg/kg 04/29/10 19:24 53-70-3
Dibenzofuran 0.0 mg/kg 04/29/10 19:24 132-64-9
1,2-Dichlorobenzene 0.0 mg/kg 1 04/29/10 19:24 95-50-1
1,3-Dichlorobenzene 0.0 mg/kg 1 04/29/10 19:24 541-73-1
1,4-Dichlorobenzene 0.0 mg/kg 04/29/10 19:24 106-46-7
3,3'-Dichlorobenzidine 0.0 mg/kg 1 04/29/10 19:24 91-94-1
2,4-Dichlorophenol 0.0 mg/kg 04/29/10 19:24 120-83-2
Diethylphthalate 0.0 mg/kg 04/29/10 19:24 84-66-2
Date: 04/30/2010 06:21 PM REPORT OF LABORATORY ANALYSIS Page 11 of38
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ 0 ~ ~ :t ~ :; ~
IWIW.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-C
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551003 Collected: 04/16/1011:00 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV Microwave
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
8260/5035A Volatile Organics
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Date: 04/30/2010 06:21 PM
Results Units
Analytical Method: EPA 8270
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
-0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.012 mg/kg
0.0049 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.013 mg/kg
0.0 mg/kg
0.0014 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
Analytical Method: EPA 8260
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
Report Limit OF Prepared
5.1 50
0.26 50
0.26 50
0.26 50
0.26 50
0.26 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
'I) \ti ACCo,90
~ , g i
Analyzed CASNo. Qual
04/29/10 19:24 105-67-9
04/29/10 19:24 131-11-3
04/29/10 19:24 84-74-2
04/29/10 19:24 534-52-1
04/29/10 19:24 51-28-5
04/29/10 19:24 121-14-2
04/29/10 19:24 606-20-2
04/29/10 19:24 117-84-0
04/29/10 19:24 117-81-7
04/29/10 19:24 206-44-0
04/29/10 19:24 86-73-7
04/29/10 19:24 87-68-3
04/29/10 19:24 118-74-1
04/29/10 19:24 77-47-4
04/29/10 19:24 67-72-1
04/29/10 19:24 193-39-5
04/29/10 19:24 78-59-1
04/29/10 19:24 90-12-0
04/29/10 19:24 91-57-6
04/29/10 19:24 95-48-7
04/29/10 19:24
04/29/10 19:24 91-20-3
04/29/10 19:24 88-74-4
04/29/10 19:24 99-09-2
04/29/10 19:24 100-01-6
04/29/10 19:24 98-95-3
04/29/10 19:24 88-75-5
04/29/10 19:24 100-02-7
04/29/10 19:24 62-75-9
04/29/10 19:24 621-64-7
04/29/10 19:24 86-30-6
04/29/10 19:24 87-86-5
04/29/10 19:24 85-01-8
04/29/10 19:24 108-95-2
04/29/10 19:24 129-00-0
04/29/10 19:24 120-82-1
04/29/10 19:24 95-95-4
04/29/10 19:24 88-06-2
04/20/10 18:48 67-64-1
04/20/10 18:48 71-43-2
04/20/10 18:48 108-86-1
04/20/10 18:48 74-97-5
04/20/10 18:48 75-27-4
04/20/10 18:48 75-25-2
Page 12 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-C
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551003 Collected: 04/16/10 11:00 Received: 04/16/1014:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromomethane ND mg/kg 0.51 50 04/20/10 18:48 74-83-9
2-Butanone (MEK) ND mg/kg 5.1 50 04/20/10 18:48 78-93-3
n-Butylbenzene ND mg/kg 0.26 50 04/20/10 18:48 104-51-8
sec-Butylbenzene ND mg/kg 0.26 50 04/20/10 18:48 135-98-8
tert-Butylbenzene ND mg/kg 0.26 50 04/20/10 18:48 98-06-6
Carbon tetrachloride ND mg/kg 0.26 50 04/20/10 18:48 56-23-5
Chlorobenzene ND mg/kg 0.26 50 04/20/10 18:48 108-90-7
Chloroethane ND mg/kg 0.51 50 04/20/10 18:48 75-00-3
Chloroform ND mg/kg 0.26 50 04/20/10 18:48 67-66-3
Chloromethane ND mg/kg 0.51 50 04/20/10 18:48 74-87-3
2-Chlorotoluene ND mg/kg 0.26 50 04/20/10 18:48 95-49-8
• 4-Chlorotoluene ND mg/kg 0.26 50 04/20/10 18:48 106-43-4
1,2-Dibromo-3-chloropropane ND mg/kg 0.26 50 04/20/10 18:48 96-12-8
Dibromochloromethane ND mg/kg 0.26 50 04/20/10 18:48 124-48-1
1,2-Dibromoethane (EDB) ND mg/l<g 0.26 50 04/20/10 18:48 106-93-4
Dibromomethane ND m'g/kg 0.26 50 04/20/10 18:48 74-95-3
1,2-Dichlorobenzene ND mg/kg 0.26 50 04/20/10 18:48 95-50-1
1,3-Dichlorobenzene ND mg/kg 0.26 50 04/20/10 18:48 541-73-1
1,4-Dichlorobenzene ND mg/kg 0.26 50 04/20/10 18:48 106-46-7
Dichlorodifluoromethane ND mg/kg 0.51 50 04/20/10 18:48 75-71-8 ,, D3
1, 1-Dichloroethane ND mg/kg 0.26 50 04/20/10 18:48 75-34-3.
1,2-Dichloroethane ND mg/kg 0.26 50 04/20/10 18:48 107-06-2
1, 1-Dichloroethene ND mg/kg 0.26 50 04/20/10 18:48 75-35-4
cis-1,2-Dichloroethene ND mg/kg 0.26 50 04/20/10 18:48 156-59-2
trans-1,2-Dichloroethene ND mg/kg 0.26 · 50 04/20/10 18:48 156-60-5
1,2-Dichloropropane ND mg/kg 0.26 50 04/20/10 18:48 78-87-5
1,3-Dichloropropane Nb mg/kg 0.26 50 04/20/10 18:48 142-28-9
2,2-Dichloropropane ND mg/kg 0.26 50 04/20/10 18:48 594-20-7
1, 1-Dichloropropene ND mg/kg 0.2~ 50 04/20/10 18:48 563-58-6
cis-1,3-Dichloropropene ND mg/kg 0.26 50 04/20/10 18:48 10061-01-5
trans-1,3-Dichloropropene ND mg/kg 0.26 50 04/20/10 18:48 10061-02-6
Diisopropyl ether ND mg/kg 0.26 50 04/20/10 18:48 108-20-3
Ethyl benzene ND mg/kg 0.26 50 04/20/10 18:48 100-41-4
Hexachloro-1,3-butadiene ND mg/kg 0.26 50 04/20/10 18:48 87-68-3
2-Hexanone ND mg/kg 2.6 50 04/20/10 18:48 591-78-6
lsopropylbenzene (Cumene) ND mg/kg 0.26 50 04/20/10 18:48 98-82-8
p-lsopropyltoluene ND mg/kg 0.26 50 04/20/10 18:48 99-87-6
Methylene Chloride ND mg/kg 1.0 50 04/20/10 18:48 75-09-2
4-Methyl-2-pentanone (MIBK) ND mg/kg 2.6 50 04/20/10 18:48 108-10-1
Methyl-tert-butyl ether ND mg/kg 0.26 50 04/20/10 18:48 1634-04-4
Naphthalene ND mg/kg 0.26 50 04/20/10 18:48 91-20-3
n-Propylbenzene ND mg/kg 0.26 50 04/20/10 18:48 103-65-1
Styrene ND mg/kg 0.26 50 04/20/10 18:48 100-42-5
1, 1, 1,2-Tetrachloroethane ND mg/kg 0.26 50 04/20/10 18:48 630-20-6
1, 1,2,2-Tetrachloroethane ND mg/kg 0.26 50 04/20/10 18:48 79-34-5
Tetrachloroethene ND mg/kg 0.26 50 04/20/10 18:48 127-18-4
Date: 04/30/2010 06:21 PM REPORT OF LABORATORY ANALYSIS Page 13 of38
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ ~ -:f ~ ~ ~
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-C
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 26604
[phone]
Pace Analytical Services, Inc.
9600 Kincey Ave. Suite 100
Huntersville, NC 26076
[phone]
LablD: 9267551003 Collected: 04/16/10 11:00 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260/5035A Volatile Organics
Toluene
1,2,3-Trichlorobenzene
1,2,4-T richlorobenzene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Dibromofluoromethane (S)
Toluene-dB (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 04/30/2010 06:21 PM
Results Units Report Limit DF Prepared
Analytical Method: EPA 8260
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 2.6 50
ND mg/kg 0.-51 50
ND mg/kg 0.51 50
ND mg/kg 0.26 50
92 % 79-116 50
99 % 88-110 50
101 % 74-115 50
89 % 69-121 50
Analytical Method: ASTM D2974-87
16.7 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
O \tl ACCoFft,
~ ~ :J ~ ~ ~
Analyzed CAS No. Qua!
04/20/10 18:4!! 108-88-3
04/20/10 18:48 87-61-6
04/20/10 18:48 120-82-1
04/20/10 18:48 71-55-6
04/20/10 18:48 79-00-5
04/20/10 18:48 79-01-6
04/20/10 18:48 75-69-4
04/20/10 18:48 96-18-4
04/20/10 18:48 95-63-6
04/20/10 18:48 108-67-8
04/20/10 18:48 108-05-4
04/20/10 18:48 75-01-4
04/20/10 18:48 1330-20-7
04/20/10 18:48 95-47-6
04/20/10 18:48 1868-53-7
04/20/10 18:48 2037-26-5
04/20/10 18:48 460-00-4
04/20/10 18:48 17060-07-0
04/23/10 13:44
Page 14 of38
IWIW.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-D
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551004 Collected: 04/16/10 11:15 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Nonatriacontane (S)
o-Terphenyl (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
VPH NC Soil
Aliphatic (C05-C08)
Aliphatic (C09-C12)
Aromatic (C09-C10)
2,5-Dibromotoluene (PID)(S)
2,5-Dibromotoluene (FID)(S)
8270 MSSV Microwave
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
BenzoicAcid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Date: 04/30/2010 06:21 PM
Results Units Report Limit OF Prepared Analyzed
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
825 mg/kg 308 25 04/19/10 14:55 04/21/10 12:34
ND mg/kg 308 25 04/19/10 14:55 04/21/10 12:34
696 mg/kg 123 10 04/19/10 14:55 04/21/10 12:34
0% 40-140 25 04/19/10 14:55 04/21/10 12:34
0% 40-140 10 04/19/10 14:55 04/21/10 12:34
0% 40-140 10 04/19/10 14:55 04/21/10 12:34
0% 40-140 10 04/19/10 14:55 04/21/10 12:34
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
ND mg/kg
62.4 mg/kg
18.2 mg/kg
143 %
257 %
Analytical Method: EPA 8270
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
8.7
8.7
8.7
70-130
70-130
1
1
1
1
1
1
1
1
1
04/19/10 13:31 04/19/1021 :00
04/19/10 13:31 04/19/10 21:00
04/19/10 13:31 04/19/1021 :00
04/19/1013:31 04/19/10 21:00
04/19/1013:31 04/19/1021:00
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
04/29/10 19:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
CAS No.
7194-86-7
84-15-1
321-60-8
580-13-2
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
95-50-1
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
Qual
S4
S4
S4
S4
S5
S5
Page 15 of38
www.pacetabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-D
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551004 Collected: 04/16/1011:15 Received: 04/16/1014:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units Report Limit DF Prepared
8270 MSSV Microwave
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-ccl)pyrene
lsophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
8260/5035A Volatile Organics
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Date: 04/30/2010 06:21 PM
Analytical Method: EPA 8270
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0028 mg/kg
0.0 mg/kg
0.011 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.044 mg/kg
0.059 mg/kg
0.0022 mg/kg
0.0 mg/kg
0.012 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.025 mg/kg
0.0 mg/kg
0.0027 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
Analytical Method: EPA 8260
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
1
1
1
1
1
8.7 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed CASNo.
04/29/10 19:52 105-67-9
04/29/10 19:52 131-11-3
04/29/10 19:52 84-74-2
04/29/10 19:52 534-52-1
04/29/10 19:52 51-28-5
04/29/10 19:52 121-14-2
04/29/1.0 19:52 606-20-2
04/29/10 19:52 117-84-0
04/29/10 19:52 117-81-7
04/29/10 19:52 206-44-0
04/29/10 19:52 86-73-7
04/29/10 19:52 87-68-3
04/29/1019:52 118-74-1
04/29/10 19:52 77-47-4
04/29/10 19:52 67-72-1
04/29/10 19:52 193-39-5
04/29/10 19:52 78-59-1
04/29/10 19:52 90-12-0
04/29/10 19:52 91-57-6
04/29/10 19:52 95-48-7
04/29/10 19:52
04/29/10 19:52 91-20-3
04/29/10 19:52 88-74-4
04/29/10 19:52 99-09-2
04/29/10 19:52 100-01-6
04/29/10 19:52 98-95-3
04/29/10 19:52 88-75-5
04/29/10 19:52 100-02-7
04/29/10 19:52 62-75-9
04/29/10 19:52 621-64-7
04/29/10 19:52 86-30-6
04/29/10 19:52 87-86-5
04/29/10 19:52 85-01-8
04/29/10 19:52 108-95-2
04/29/10 19:52 129-00-0
04/29/10 19:52 120-82-1
04/29/10 19:52 95-95-4
04/29/10 19:52 88-06-2
04/20/10 19:06 67-64-1
04/20/10 19:06 71-43-2
04/20/10 19:06 108-86-1
04/20/10 19:06 74-97-5
04/20/10 19:06 75-27-4
04/20/10 19:06 75-25-2
Qual
Page 16 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-D
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551004 Collected: 04/16/1011:15 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
B260/5035A Volatile Organics
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
. cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethyl benzene
Hexachloro-1,3-butadiene
2-Hexanone
lsopropylbenzene (Cumene)
p-1s opropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Date: 04/30/2010 06:21 PM
Results Units
Analytical Method: EPA 8260
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
1.1 mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
Report Limit DF Prepared
0.87 100
8.7 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.87 100
0.44 100
0.87 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.87 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
4.4 100
0.44 100
0.44 100
1.7 100
4.4 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
0.44 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed CAS No.
04/20/10 19:06 74-83-9
04/20/10 19:06 78-93-3
04/20/10 19:06 104-51-8
04/20/10 19:06 135-98-8
04/20/10 19:06 98-06-6
04/20/10 19:06 56-23-5
04/20/10 19:06 108-90-7
04/20/10 19:06 75-00-3
04/20/10 19:06 67-66-3
04/20/10 19:06 74-87-3
04/20/10 19:06 95-49-8
04/20/10 19:06 106-43-4
04/20/10 19:06 96-12-8
04/20/10 19:06 124-48-1
04/20/10 19:06 106-93-4
04/20/10 19:06 74-95-3
04/20/10 19:06 95-50-1
04/20/10 19:06 541-73-1
04/20/10 19:06 106-46-7
Qual
04/20/10 19:06 75-71-8 --D3
04/20/10 19:06 75-34-3
04/20/10 19:06 107-06-2
04/20/10 19:06 75-35-4
04/20/10 19:06 156-59-2
04/20/10 19:06 156-60-5
04/20/10 19:06 78-87-5
04/20/10 19:06 142-28-9
04/20/10 19:06 594-20-7
04/20/10 19:06 563-58-6
04/20/10 19:06 10061-01-5
04/20/10 19:06 10061-02-6
04/20/10 19:06 108-20-3
04/20/10 19:06 100-41-4
04/20/10 19:06 87-68-3 .
04/20/10 19:06 591-78-6
04/20/10 19:06 98-82-8
04/20/10 19:06 99-87-6
04/20/10 19:06 75-09-2
04/20/10 19:06 108-10-1
04/20/10 19:06 1634-04-4
04/20/10 19:06 91-20-3
04/20/10 19:06 103-65-1
04/20/10 19:06 100-42-5
04/20/10 19:06 630-20-6
04/20/10 19:06 79-34-5
04/20/10 19:06 127-18-4
Page 17 of38
wrm.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-D
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551004 Collected: 04/16/10 11:15 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260/5035A Volatile Organics
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-T richloroethane
1, 1,2-Trichloroethane
Trichloroethene
T richlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Dibromofluoromethane (S)
Toluene-dB (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 04/30/2010 06:21 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA 8260
ND mg/kg 0.44 100
ND mg/kg 0.44 100
ND mg/kg 0.44 100
ND mg/kg 0.44 100
ND mg/kg 0.44 100
ND mg/kg 0.44 100
ND mg/kg 0.44 100
ND mg/kg 0.44 100
ND mg/kg 0.44 100
ND mg/kg 0.44 100
ND mg/kg 4.4 100
ND mg/kg 0.87 100
ND mg/kg 0.87 100
ND mg/kg 0.44 100
97 % 79-116 100
101 % 88-110 100
105 % 74-115 100
91 % 69-121 100
Analytical Method: ASTM D2974-87
18.8 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
<:> \ti ACCo110
~ C i 1
Analyzed CAS No. Qual
04/20/10 19:06 108-88-3
04/20/10 19:06 87-61-6
04/20/10 19:06 120-82-1
04/20/10 19:06 71-55-6
04/20/10 19:06 79-00-5
04/20/10 19:06 79-01-6
04/20/10 19:06 75-69-4
04/20/10 19:06 96-18-4
04/20/10 19:06 95-63-6
04/20/10 19:06 108-67-8
04/20/10 19:06 108-05-4
04/20/10 19:06 75-01-4
04/20/10 19:06 1330-20-7
04/20/10 19:06 95-47-6
04/20/10 19:06 1868-53-7
04/20/10 19:06 2037-26-5
04/20/10 19:06 460-00-4
04/20/10 19:06 17060-07-0
04/23/10 13:44
Page 18 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-E
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551005 Collected: 04/16/10 11:30 Received: 04/16/1014:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Nonatriacontane (S)
o-Terphenyl (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
VPH NC Soil
Aliphatic (COS-COB)
Aliphatic (C09-C12)
Aromatic (C09-C10)
2,5-Dibromotoluene (PID)(S)
2,5-Dibromotoluene (FID)(S)
8270 MSSV Microwave
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)m_ethane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-pichlorophenol
Diethylphthalate
Date: 04/30/2010 06:21 PM
Results Units Report Limit DF Prepared Analyzed
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
381 mg/kg 120 10 04/19/10 14:55 04/21/10 13:10
ND mg/kg 120 10 04/19/10 14:55 04/21/10 13:10
280 mg/kg 59.8 5 04/19/10 14:55 04/21/10 13:10
0% 40-140 10 04/19/10 14:55 04/21/10 13:10
0% 40-140 5 04/19/10 14:55 04/21/10 13:10
0% 40-140 5 04/19/10 14:55 04/21/10 13:10
0% 40-140 5 04/19/10 14:55 04/21/10 13:10
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
ND mg/kg
50.1 mg/kg
.15.9 mg/kg
136 %
240 %
Analytical Method: EPA 8270
0.0070 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
9.1
9.1
9.1
70-130
70-130 1
1
1
1
1
1
1
f
04/19/10 13:31 04/19/10 21 :25
04/19/10 13:31 04/19/10 21 :25
04/19/10 13:31 04/19/10 21:25
04/19/10 13:31 04/19/10 21:25
04/19/10 13:31 04/19/10 21:25
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
04/29/10 20:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
CAS No.
7194-86-7
84-15-1
321-60-8
580-13-2
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8 ·
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
95-50-1
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
Qual
S4
S4
S4
S4
S5
S5
Page 19 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-E
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551005 Collected: 04/16/10 11:30 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units Report Limit DF Prepared
8270 MSSV Microwave
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n~octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
.Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
. 3-Nitroaniline
4-Nitroaniline
Nitro benzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
826015035A Volatile Organics
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Date: 04/30/2010 06:21 PM
Analytical Method: EPA 8270
0.0016 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0045 mg/kg
0.0 mg/kg
0.015 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.056 mg/kg
0.040 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0050 mg/kg
0.0 mg/kg
-0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
0.Omg/kg
0.035 mg/kg
0.0 mg/kg
0.0029 mg/kg
0.0 mg/kg
0.0 mg/kg
0.0 mg/kg
Analytical Method: EPA 8260
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
1
1
1
1
1
1
.1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
5.2 50
0.26 50
0.26 50
0.26 50
0.26 50
0.26 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed CAS No.
04/29/10 20:20 105-67-9
04/29/10 20:20 131-11-3
04/29/10 20:20 84-74-2
04/29/10 20:20 534-52-1
04/29/10 20:20 51-28-5
04/29/10 20:20 121-14-2
04/29/10 20:20 606-20-2
04/29/10 20:20 117-84-0
04/29/10 20:20 117-81-7
04/29/10 20:20 206-44-0
04/29/10 20:20 86-73-7
04/29/10 20:20 87-68-3
04/29/10 20:20 118-74-1
04/29/10 20:20 77-47-4
04/29/10 20:20 67-72-1
04/29/10 20:20 193-39-5
04/29/10 20:20 78-59-1
04/29/10 20:20 90-12-0
04/29/10 20:20 91-57-6
04/29/10 20:20 95-48-7
04/29/10 20:20
04/29/10 20:20 91-20-3
04/29/10 20:20 88-74-4
04/29/10 20:20 .99-09-2
04/29/10 20:20 100-01-6
04/29/10 20:20 98-95-3
04/29/10 20:20 88-75-5
04/29/10 20:20 100-02-7
04/29/10 20:20 62-75-9
04/29/10 20:20 621-64-7
04/29/10 20:20 86-30-6
04/29/10 20:20 87-86-5
04/29/10 20:20 85-01-8
04/29/10 20:20 108-95-2
04/29/10 20:20 129-00-0
04/29/.10 20;20 120-82-1
04/29/10 20:20 95-95-4
04/29/10 20:20 88-06-2
04/20/10 18:11 67-64-1
04/20/10 18:11 71-43-2
04/20/10 18:11 108-86-1
04/20/10 18:11 74-97-5
04/20/10 18:11 75-27-4
04/20/10 18:11 75-25-2
Qual
Page 20 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-E
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
LablD: 9267551005 Collected: 04/16/10 11:30 Received: 04/16/10 14:55
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CASNo. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromomethane ND mg/kg 0.52 50 04/20/10 18:11 74-83-9
2-Butanone (MEK) ND mg/kg 5.2 50 04/20/10 18:11 78-93-3
n-Butylbenzene 0.34 mg/kg 0.26 50 04/20/10 18:11 104-51-8
sec-Butyl benzene 0.44 mg/kg 0.26 50 04/20/10 18:11 135-98-8
tert-Butylbenzene ND mg/kg 0.26 50 04/20/10 18:11 98-06-6
Carbon tetrachloride ND mg/kg 0.26 50 04/20/10 18:11 56-23-5
Chlorobenzene ND mg/kg 0.26 50 04/20/10 18:11 108-90-7
Chloroethane ND mg/kg 0.52 50 04/20/10 18:11 75-00-3
Chloroform ND mg/kg 0.26 50 04/20/10 18:11 67-66-3
Chloromethane ND mg/kg 0.52 50 04/20/10 18:11 74-87-3
2-Chlorotoluene ND mg/kg 0.26 50 04/20/10 18:11 95-49-8
4-Chlorotoluene ND mg/kg 0.26 50 04/20/10 18:11 106-43-4
1,2-Dibromo-3-chloropropane ND mg/kg 0.26 50 04/20/10 18:11 96-12-8
Dibromochloromethane ND mg/kg 0.26 50 04/20/10 18:11 124-48-1
1,2-Dibromoethane (EDB) ND mg/kg 0.26 50 04/20/10 18:11 106-93-4
Dibromomethane ND mg/kg 0.26 50 04/20/10 18:11 74-95-3
1,2-Dichlorobenzene ND mg/kg 0.26 50 04/20/10 18:11 95-50-1
1,3-Dichlorobenzene ND mg/kg 0.26 50 04/20/10 18:11 541-73-1
1,4-Dichlorobenzene ND mg/kg 0.26 50 04/20/10 18:11 106-46-7
Dichlorodifluoromethane ND mg/kg 0.52 50 04/20/10 18:11 75-71-8 D3
1, 1-Dichloroethane ND mg/kg 0.26 50 04/20/10 18:11 75-34-3
1,2-Dichloroethane ND mg/kg 0.26 50 04/20/10 18:11 107-06-2
1, 1-Dichloroethene ND mg/kg 0.26 50 04/20/10 18: 11 75-35-4
cis-1,2-Dichloroethene ND mg/kg 0.26 50 04/20/10 18:11 156-59-2
trans-1,2-Dichloroethene ND mg/kg 0.26 50 04/20/10 18:11 156-60-5
1,2-Dichloropropane ND mg/kg 0.26 50 04/20/10 18:11 78-87-5
1,3-Dichloropropane ND mg/kg 0.26 50 04/20/10 18:11 142-28-9
2,2-Dichloropropane ND mg/kg 0.26 50 04/20/10 18:11 594-20-7
1, 1-Dichloropropene ND mg/kg 0.26 50 04/20/10 18:11 563-58-6
cis-1,3-Dichloropropene ND mg/kg 0.26 50 04/20/10 18:11 10061-01-5
trans-1,3-Dichloropropene ND mg/kg 0.26 50 04/20/10 18:11 10061-02-6
Diisopropyl ether ND mg/kg 0.26 50 04/20/10 18: 11 108-20-3
Ethyl benzene ND mg/kg 0.26 50 04/20/10 18:11 100-41-4
Hexachloro-1,3-butadiene ND mg/kg 0.26 50 04/20/10 18:11 87-68-3
2-Hexanone ND mg/kg 2.6 50 04/20/10 18:11 591-78-6
lsopropylbenzene (Cumene) ND mg/kg 0.26 50 04/20/10 18:11 98-82-8
p-lsopropyltoluene 0.30 mg/kg 0.26 50 04/20/10 18:11 99-87-6
Methylene Chloride ND mg/kg 1.0 50 04/20/10 18:11 75-09-2
4-Methyl-2-pentanone (MIBK) ND mg/kg 2.6 50 04/20/10 18:11 108-10-1
Methyl-tert-butyl ether ND mg/kg 0.26 50 04/20/10 18:11 1634-04-4
Naphthalene 1.1 mg/kg 0.26 50 04/20/10 18:11 91-20-3
n-Propylbenzene 0.28 mg/kg 0.26 50 04/20/10 18:11 103-65-1
Styrene ND mg/kg 0.26 50 04/20/10 18:11 100-42-5
1, 1, 1,2-Tetrachloroethane ND mg/kg 0.26 50 04/20/10 18:11 630-20-6
1, 1,2,2-Tetrachloroethane ND mg/kg 0.26 50 04/20/10 18:11 79-34-5
Tetrachloroethene ND mg/kg 0.26 50 04/20/10 18:11 127-18-4
Date: 04/30/2010 06:21 PM REPORT OF LABORATORY ANALYSIS Page 21 of38
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ ~ ~ ff 1
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
Sample: Soil-E
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9267551005 Collected: 04/16/10 11:30 Received: 04/16/10 14:55 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260/5035A Volatile Organics
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1, 1,2-Trichloroethane
T richloroethene
T richlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Dibromofluoromethane (S)
Toluen~8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethan~4 (S)
Percent Moisture
Percent Moisture
Date: 04/30/2010 06:21 PM
Results Units Report Limit DF Prepared
Analytical Method: EPA 8260
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
ND mg/kg 0.26 50
0.71 mg/kg 0.26 50
0.29 mg/kg 0.26 50
ND mg/kg 2.6 50
ND mg/kg 0.52 50
ND mg/kg 0.52 50
ND mg/kg 0.26 50
80 % 79-116 50
100 % 88-110 50
101 % 74-115 50
77 % 69-121 50
Analytical Method: ASTM D2974-87
16.4 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
0 \"-11,cco110
~ ~ ff 1
Analyzed GAS No. Qual
04/20/10 18:11 108-88-3
04/20/10 18:11 87-61-6
04/20/10 18:11 120-82-1
04/20/10 18:11 71-55-6
04/20/10 18:11 79-00-5
04/20/10 18:11 79-01-6
04/20/10 18:11 75-69-4
04/20/10 18:11 96-18-4
04/20/10 18:11 95-63-6
04/20/10 18:11 108-67-8
04/20/10 18:11 108-05-4
04/20/10 18:11 75-01-4
04/20/10 18:11 1330-20-7
04/20/10 18:11 95-47-6
04/20/10 18:11 1868-53-7
04/20/10 18:11 2037-26-5
04/20/10 18:11 460-00-4
04/20/10 18:11 17060-07-0
04/23/10 13:45
Page 22 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
QC Batch: OEXT/9764
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: MADEPEPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Associated Lab Samples: 9267551001, 9267551002, 9267551003, 9267551004, 9267551005
METHOD BLANK: 430714 Matrix: Solid
Associated Lab Samples: 9267551001, 9267551002, 9267551003, 9267551004, 9267551005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Aliphatic (C09-C18) mg/kg
Aliphatic (C19-C36) mg/kg
Aromatic (C11-C22) mg/kg
2-Bromonaphthalene (S) %
2-Fluorobiphenyl (S) %
Nonatriacontane (S) %
o-Terphenyl (S) %
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
Aliphatic (C09-C18) mg/kg
Aliphatic (C19-C36) mg/kg
Aromatic (C11-C22) mg/kg
2-Bromonaphthalene (S) %
2-Fluorobiphenyl (S) %
Nonatriacontane (S) %
o-Terphenyl (S) %
Date: 04/30/2010 06:21 PM
ND 10.0 04/20/10 20:47
ND 10.0 04/20/10 20:47
ND 10.0 04/20/10 20:47
103 40-140 04/20/10 20:47
98 40-140 04/20/10 20:47
76 40-140 04/20/10 20:47
88 40-140 04/20/10 20:47
430715 430716
Units
Spike LCS LCSD LCS LCSD
Cone. Result Result % Rec% Rec ----
10 ND ND 99 90
13.3 16.3 14.7 122 110
28.3 27.3 26.7 96 94
98 96
101 93
79 75
92 82
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
%Rec
Limits RPD
40-140
40-140
40-140
40-140
40-140
40-140
40-140
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPD Qualifiers
50
11 50
2 50
Page 23 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
QC Batch: GCV/39B2
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: MADEPVPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil
Associated Lab Samples: 9267551001, 9267551002, 9267551003, 9267551004, 9267551005
METHOD BLANK: 430627 Matrix: Solid
Associated Lab Samples: 9267551001, 9267551002, 9267551003, 9267551004, 9267551005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Aliphatic (COS-COB) mg/kg
Aliphatic (C09-C12) mg/kg
Aromatic (C09-C10) mg/kg
2,5-Dibromotoluene (FID)(S) %
2,5-Dibromotoluene (PID)(S) %
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
Aliphatic (COS-COB) mg/kg
Aliphatic (C09-C12) mg/kg
Aromatic (C09-C10) mg/kg
2,5-Dibromotoluene (FID)(S) %
2,5-Dibromotoluene (PID)(S) %
Date: 04/30/2010 06:21 PM
ND 10.0 04/19/10 16:03
ND 10.0 04/19/10 16:03
ND 10.0 04/19/10 16:03
126 70-130 04/19/10 16:03
119 70-130 04/19/10 16:03
430628 430629
Units
Spike LCS LCSD LCS LCSD
Cone. Result Result %Rec %Rec ----
15 15.9 15.1 106 100
15 16.4 15.7 109 105
5 ND ND 101 96
114 115
101 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
'O '"° ACCo~0
0 ~ ~ i i
%Rec
Limits RPD
70-130
30-130
70-130
70-130
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPD Qualifiers
6 25
4 25
25
Page24 of3B
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
QC Batch: MSV/10661
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 9267551001, 9267551003, 9267551004, 9267551005
METHOD BLANK: 430684 Matrix: Solid
Associated Lab Samples: 9267551001,9267551003,9267551004,9267551005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1, 1, 1,2-Tetrachloroethane mg/kg ND 0.0050 04/20/10 09:57
1, 1, 1-Trichloroethane mg/kg ND 0.0050 04/20/10 09:57
1, 1,2,2-Tetrachloroethane mg/kg ND 0.0050 04/20/10 09:57
1, 1,2-Trichloroethane mg/kg ND 0.0050 04/20/10 09:57
1, 1-Dichloroethane mg/kg ND 0.0050 04/20/10 09:57
1, 1-Dichloroethene mg/kg ND 0.0050 04/20/10 09:57
1 , 1-Dichloropropene mg/kg ND 0.0050 04/20/10 09:57
1,2,3-Trichlorobenzene mg/kg ND 0.0050 04/20/10 09:57
1,2,3-Trichloropropane mg/kg ND 0.0050 04/20/10 09:57
1,2,4-Trichlorobenzene mg/kg ND 0.0050 04/20/10 09:57
1,2,4-Trimethylbenzene mg/kg ND 0.0050 04/20/10 09:57
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 04/20/10 09:57
1,2-Dibromoethane (EDB) mg/kg ND 0.0050 04/20/10 09:57
1,2-Dichlorobenzene mg/kg ND 0.0050 04/20/10 09:57
1,2-Dichloroethane mg/kg ND 0.0050 04/20/10 09:57
1,2-Dichloropropane mg/kg ND 0.0050 04/20/10 09:57
1,3,5-Trimethylbenzene mg/kg ND 0.0050 04/20/10 09:57
1,3-Dichlorobenzene mg/kg ND 0.0050 04/20/10 09:57
1,3-Dichloropropane mg/kg ND 0.0050 04/20/10 09:57
1,4-Dichlorobenzene mg/kg ND 0.0050 04/20/10 09:57
2,2-Dichloropropane mg/kg ND 0.0050 04/20/10 09:57
2-Butanone (MEK) mg/kg ND 0.10 04/20/10 09:57
2-Chlorotoluene mg/kg ND 0.0050 04/20/10 09:57
2-Hexanone mg/kg ND 0.050 04/20/10 09:57
4-Chlorotoluene mg/kg ND 0.0050 04/20/10 09:57
4-Methyl-2-pentanone (MIBK) mg/kg ND 0.050 04/20/10 09:57
Acetone mg/kg ND 0.10 04/20/10 09:57
Benzene mg/kg ND 0.0050 04/20/10 09:57
Bro mo benzene mg/kg ND 0.0050 04/20/10 09:57
Bromochloromethane mg/kg ND 0.0050 04/20/10 09:57
Bromodichloromethane mg/kg ND 0.0050 04/20/10 09:57
Bromoform mg/kg ND .0.0050 04/20/10 09:57
Bromomethane mg/kg ND 0.010 04/20/10 09:57
Carbon tetrachloride mg/kg ND 0.0050 04/20/10 09:57
Chlorobenzene mg/kg ND 0.0050 04/20/10 09:57
Chloroethane mg/kg ND 0.010 04/20/10 09:57
Chloroform mg/kg ND 0.0050 04/20/10 09:57
Chloromethane mg/kg ND 0.010 04/20/10 09:57
cis-1,2-Dichloroethene mg/kg ND 0.0050 04/20/10 09:57
cis-1,3-Dichloropropene mg/kg ND 0.0050 04/20/10 09:57
Dibromochloromethane mg/kg ND 0.0050 04/20/10 09:57
Dibromomethane mg/kg ND 0.0050 04/20/10 09:57
Dichlorodifluoromethane mg/kg ND 0.010 04/20/10 09:57
Date: 04/30/2010 06:21 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ ~ -ff 1
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of38
Wl'IW.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
METHOD BLANK: 430684
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Matrix: Solid
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Associated Lab Samples: 9267551001,9267551003,9267551004,9267551005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Diisopropyl ether mg/kg ND 0.0050 04/20/10 09:57
Ethyl benzene mg/kg ND 0.0050 04/20/10 09:57
Hexachloro-1,3-butadiene mg/kg ND 0.0050 04/20/10 09:57
lsopropylbenzene (Cumene) mg/kg ND 0.0050 04/20/10 09:57
m&p-Xylene mg/kg ND 0.010 04/20/10 09:57
Methyl-tert-butyl ether mg/kg ND 0.0050 04/20/10 09:57
Methylene Chloride mg/kg ND 0.020 04/20/10 09:57
n-Butylbenzene mg/kg ND 0.0050 04/20/10 09:57
n-Propylbenzene mg/kg ND 0.0050 04/20/10 09:57
Naphthalene mg/kg ND 0.0050 04/20/10 09:57
a-Xylene mg/kg ND 0.0050 04/20/10 09:57
p-lsopropyltoluene mg/kg ND 0.0050 04/20/10 09:57
sec-Butyl benzene mg/kg ND 0.0050 04/20/10 09:57
Styrene mg/kg ND 0.0050 04/20/10 09:57
tert-Butylbenzene mg/kg ND 0.0050 04/20/10 09:57
Tetrachloroethene mg/kg ND 0.0050 04/20/10 09:57
Toluene mg/kg ND 0.0050 04/20/10 09:57
trans-1,2-Dichloroethene mg/kg ND 0.0050 04/20/10 09:57
trans-1,3-Dichloropropene mg/kg ND 0.0050 04/20/10 09:57
T richloroethene mg/kg ND 0.0050 04/20/10 09:57
T richlorofluoromethane mg/kg ND 0.0050 04/20/10 09:57
Vinyl acetate mg/kg ND 0.050 04/20/10 09:57
Vinyl chloride mg/kg ND 0.010 04/20/10 09:57
1,2-Dichloroethane-d4 (S) % 96 69-121 04/20/10 09:57
4-Bromofluorobenzene -{S) % 103 74-115 04/20/10 09:57
Dibromofluoromethane (S) % 100 79-116 04/20/10 09:57
Toluene-dB (S) % 99 88-110 04/20/10 09:57
LABORATORY CONTROL SAMPLE: 430685
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
1, 1, 1,2-Tetrachloroethane mg/kg .05 0.051 102 75-137
1, 1, 1-T richloroethane mg/kg .05 0.047 95 70-140
1, 1,2,2-Tetrachloroethane mg/kg .05 0.050 101 74-133
1, 1,2-Trichloroethane mg/kg .05 0.052 103 79-129
1, 1-Dichloroethane mg/kg .05 0.050 100 72-139
1, 1-Dichloroethene mg/kg .05 0.048 96 69-154
1, 1-Dichloropropene mg/kg .05 0.048 96 74-138
1,2,3-Trichlorobenzene mg/kg .05 0.058 116 71-150
1,2,3-Trichloropropane mg/kg .05 0.051 102 74-135
1,2,4-Trichlorobenzene mg/kg .05 0.061 121 68-150
1,2,4-Trimethylbenzene mg/kg .05 0.051 103 70-130
1,2-Dibromo-3-chloropropane mg/kg .05 0.050 100 65-146
1,2-Dibromoethane (EDB) mg/kg .05 0.052 104 77-136
1,2-Dichlorobenzene mg/kg .05 0.053 105 75-141
Date: 04/30/2010 06:21 PM REPORT OF LABORATORY ANALYSIS Page 26 of38
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ "'c-,.. ~~ ff i
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: Robo Chevron
Pace Project No.: 9267551
LABORATORY CONTROL SAMPLE: 430685
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
1,2-Dichloroethane mg/kg .05 0.045 91 74-134
1,2-Dichloropropane mg/kg .05 0.049 97 77-138
1,3,5-Trimethylbenzene mg/kg .05 0.052 105 65-128
1,3-Dichlorobenzene mg/kg .05 0.054 107 76-133
1,3-Dichloropropane mg/kg .05 0.050 101 79-132
1,4-Dichlorobenzene mg/kg .05 0.054 107 75-137
2,2-Dichloropropane mg/kg .05 0.050 99 73-137
2-Butanone (MEK} mg/kg .1 .098J 98 61-138
2-Chlorotoluene mg/kg .05 0.051 102 73-138
2-Hexanone mg/kg .1 0.12 115 58-159
4-Chlorotoluene mg/kg .05 0.053 107 75-136
4-Methyl-2-pentanone (MIBK} mg/kg .1 0.11 109 74-139
Acetone mg/kg .1 0.11 108 58-150
Benzene mg/kg .05 0.050 99 71-140
Bromobenzene mg/kg .05 0.051 102 72-144
Bromochloromethane mg/kg .05 0.052 103 78-133
Bromodichloromethane mg/kg .05 0.047 94 78-133
Bromoform mg/kg .05 0.050 101 74-132
Bromomethane mg/kg .05 0.047 93 63-184
Carbon tetrachloride mg/kg .05 0.051 103 73-143
Chlorobenzene mg/kg .05 0.053 106 77-137
Chloroethane mg/kg .05 0.049 98 68-146
Chloroform mg/kg .05 0.047 93 75-137
Chloromethane mg/kg .05 0.045 91 54-143
cis-1,2-Dichloroethene mg/kg .05 0.047 93 71-143
cis-1,3-Dichloropropene mg/kg .05 0.050 99 76-133
Dibromochloromethane mg/kg .05 0.050 101 77-131
Dibromomethane mg/kg .05 0.056 112 63-184
Dichlorodifluoromethane mg/kg .05 0.044 89 36-173
Diisopropyl ether mg/kg .05 0.047 93 68-144
Ethyl benzene mg/kg .05 0.053 106 69-141
Hexachloro-1,3-butadiene mg/kg .05 0.054 107 70-152
lsopropylbenzene (Cumene} mg/kg .05 0.055 110 77-143
m&p-Xylene mg/kg .1 0.11 109 72-138
Methyl-tert-butyl ether mg/kg .05 0.046 92 2-138
Methylene Chloride mg/kg .05 0.044 87 69-136
n-Butylbenzene mg/kg .05 0.055 110 65-128
n-Propylbenzene mg/kg .05 0.054 109 72-139
Naphthalene mg/kg .05 0.056 111 61-138
a-Xylene mg/kg .05 0.054 108 74-137
p-lsopropyltoluene mg/kg .05 0.054 108 66-128
sec-Butyl benzene mg/kg .05 0.054 108 72-140
Styrene mg/kg .05 0.054 107 76-137
tert-Butylbenzene mg/kg .05 0.054 107 68-141
Tetrachloroethene mg/kg .05 0.057 113 72-136
Toluene mg/kg .05 0.050 100 69-139
trans-1,2-Dichloroethene mg/kg .05 0.047 95 72-144
trans-1,3-Dichloropropene mg/kg .05 0.050 100 73-135
Date: 04/30/2010 06:21 PM REPORT OF LABORATORY ANALYSIS Page 27 of38
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ ~ ~ i 1
IWIW.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
LABORATORY CONTROL SAMPLE: 430685
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
1,2-Dichloroethane-04 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-dB (S)
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
Units
MATRIX SPIKE SAMPLE: 431482
Parameter
1, 1-Dichloroethene
Benzene
Chlorobenzene
Toluene
Trichloroethene
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-08 (S)
SAMPLE DUPLICATE: 431481
Parameter
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
1, 1, 1,2-Tetrachloroethane mg/kg
1 , 1, 1-T richloroethane mg/kg
1, 1,2,2-Tetrachloroethane mg/kg
1, 1,2-Trichloroethane mg/kg
1, 1-Dichloroethane mg/kg
1 , 1-Dichloroethene mg/kg
1, 1-Dichloropropene mg/kg
1,2,3-Trichlorobenzene mg/kg
1,2,3-Trichloropropane mg/kg
1,2,4-Trichlorobenzene mg/kg
1,2,4-Trimethylbenzene mg/kg
1,2-Dibromo-3-chloropropane mg/kg
1,2-Dibromoethane (EDB) mg/kg
1,2-Dichlorobenzene mg/kg
1,2-Dichloroethane mg/kg
1,2-Dichloropropane mg/kg
1,3,5-Trimethylbenzene mg/kg
1,3-Dichlorobenzene mg/kg
1,3-Dichloropropane mg/kg
1,4-Dichlorobenzene mg/kg
Date: 04/30/2010 06:21 PM
Units
Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike LCS LCS
Cone. Result %Rec
.05 0.052 104
.05 0.043 86
.1 0.16 163
.05 0.044 88
91
104
98
101
9267598001 Spike MS
Result Cone. Result
ND .048 0.047
ND .048 0.045
ND .048 0.046
ND .048 0.046
ND .048 0.045
· 9267499014 Dup
Result Result RPO
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
0 \It Acco,,"
~ -f 1
%Rec
Limits
75-136
69-144
50-150 L3
61-145
69-121
74-115
79-116
88-110
MS
%Rec
99
93
95
96
94
101
96
100
101
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
%Rec
Limits Qualifiers
33-158
46-143
29-159
38-145
70-130
69-121
74-115
79-116
88-110
Page 28 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
SAMPLE DUPLICATE: 431481
Parameter
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethyl benzene
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
m&p-Xylene
Methyl-tert-butyl ether
Methylene Chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
a-Xylene
p-lsopropyltoluene
sec-Butylben?ene
Styrene
tert-Butylbenzene
Tetrachloroelhene
Toluene
trans-1,2-Dichloroelhene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Date: 04/30/2010 06:21 PM
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9267499014 Dup
Result Result RPO Qualifiers ---ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND .015J
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
.ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
94 111 49
102 98 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ 0 ~ ~ i 1
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
SAMPLE DUPLICATE: 431481
Parameter
Dibromofluoromethane (S)
Toluene-dB (S)
Date: 04/30/2010 06:21 PM
%
%
Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9267499014
Result
97
100
Dup
Result
107
102
RPO
REPORT OF LABORATORY ANALYSIS
43
35
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
QC Batch: MSV/10680
QC Batch Method: EPA 8260
Associated Lab Samples: 9267551002
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA8260
Analysis Description: 8260 MSV 5035A Volatile Organics
METHOD BLANK: 431207 Matrix: Solid
Associated Lab Samples: 9267551002
Parameter
1, 1, 1,2-Tetrachloroethane
1, 1, 1-Trichloroethane
1, 1,2,2-Tetrachloroethane
1, 1,2-Trichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
1, 1-Dichloropropene
1,2,3-T richlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Date: 04/30/2010 06:21 PM
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mgtkg
mg/kg
mg/kg
mg/kg
mg/kg
-mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Units
Blank Reporting
Result Limit Analyzed
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.10 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.050 04/20/10 23:58
ND 0.10 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.010 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.010 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.010 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.010 04/20/10 23:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
METHOD BLANK: 431207
Associated Lab Samples: 9267551002
Parameter Units
Diisopropyl ether mg/kg
Ethyl benzene mg/kg
Hexachloro-1,3-butadiene mg/kg
lsopropylbenzene (Cumene) mg/kg
m&p-Xylene mg/kg
Methyl-tert-butyl ether mg/kg
Methylene Chloride mg/kg
n-Butylbenzene .mg/kg
n-Propylbenzene mg/kg
Naphthalene mg/kg
o-Xylene mg/kg
p-lsopropyltoluene mg/kg
sec-Butyl benzene mg/kg
Styrene mg/kg
tert-Butylbenzene mg/kg
Tetrachloroethene mg/kg
Toluene mg/kg
trans-1,2-Dichloroethene mg/kg
trans-1,3-Dichloropropene mg/kg
Trichloroethene mg/kg
Trichlorofluoromethane mg/kg
Vinyl acetate mg/kg
Vinyl chloride mg/kg
1,2-Dichloroethan~4 (S) %
4-Bromofluorobenzene_ (S) %
Dibromofluoromethane (S) %
Toluene-dB (S) %
LABORATORY CONTROL SAMPLE: 431208
Parameter Units
1, 1, 1,2-Tetrachloroethane mg/kg
1, 1, 1-T richloroethane mg/kg
1, 1,2,2-Tetrachloroethane mg/kg
1, 1,2-Trichloroethane mg/kg
1, 1-Dichloroethane mg/kg
1, 1-Dichloroethene mg/kg
1, 1-Dichloropropene mg/kg
1,2,3-Trichlorobenzene mg/kg
1,2,3-T richloropropane mg/kg
1,2,4-Trichlorobenzene mg/kg
1,2,4-Trimethylbenzene mg/kg
1,2-Dibromo-3-chloropropane mg/kg
1,2-Dibromoethane (EDB) mg/kg
1,2-Dichlorobenzene mg/kg
Date: 04/30/2010 06:21 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Matrix: Solid
Blank Reporting
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Result Limit Analyzed Qualifiers
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.010 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.020 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.0050 04/20/10 23:58
ND 0.050 04/20/10 23:58
ND 0.010 04/20/10 23:58
103 69-121 04/20/10 23:58
98 74-115 04/20/10 23:58
105 79-116 04/20/10 23:58
101 88-110 04/20/10 23:58
Spike LCS LCS %Rec
Cone. Result %Rec Limits Qualifiers
.05 0.051 102 75-137
.05 0.048 95 70-140
.05 0.048 95 74-133
.05 0.051 101 79-129
.05 0.052 105 72-139
.05 0.051 102 69-154
.05 0.046 92 74-138
.05 0.055 110 71-150
.05 0.050 100 74-135
.05 0.054 107 68-150
.05 0.051 103 70-130
.05 0.052 103 65-146
.05 0.050 99 77-136
.05 0.052 105 75-141
REPORT OF LABORATORY ANALYSIS Page 32 of38
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ ~ :: ~ ~ ~
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: Robo Chevron
Pace Project No.: 9267551
LABORATORY CONTROL SAMPLE: 431208
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers --
1,2-Dichloroethane mg/kg .05 0.049 99 74-134
1,2-Dichloropropane mg/kg .05 0.052 103 77-138
1,3,5-Trimethylbenzene mg/kg .05 0.052 104 65-128
1,3-Dichlorobenzene mg/kg .05 0.051 101 76-133
1,3-Dichloropropane mg/kg .05 0.050 100 79-132
1,4-Dichlorobenzene mg/kg .05 0.050 101 75-137
2,2-Dichloropropane mg/kg .05 0.051 103 73-137
2-Butanone (MEK) mg/kg .1 .087J 87 61-138
2-Chlorotoluene mg/kg .05 0.051 101 73-138
2-Hexanone mg/kg .1 0.11 108 58-159
4-Chlorotoluene mg/kg .05 0.052 104 75-136
4-Methyl-2-pentanone (MIBK) mg/kg .1 0.11 106 74-139
Acetone mg/kg .1 0.11 107 58-150
-Benzene mg/kg .05 0.050 101 71-140
Bromobenzene mg/kg .05 0.052 103 72-144
Bromochloromethane mg/kg .05 0.052 104 78-133
Bromodichloromethane mg/kg .05 0.051 101 78-133
Bromoform mg/kg .05 0.052 105 74-132
Bromomethane mg/kg .05 0.060 120 63-184
Carbon tetrachloride mg/kg .05 0.051 103 73-143
Chlorobenzene mg/kg .05 0.051 103 77-137
Chloroethane mg/kg .05 0.060 120 68-146
Chloroform mg/kg .05 0.049 99 75-137
Chloromethane mg/kg .05 0.055 111 54-143
cis-1,2-Dichloroethene mg/kg .05 0.051 102 71-143
cis-1,3-Dichloropropene -mg/kg .05 0.052 104 76-133
Dibromochloromethane mg/kg .05 0.052 103 77-131
Dibromomethane mg/kg .05 0.053 107 63-184
Dichlorodifluoromethane mg/kg .05 0.049 98 36-173
Diisopropyl ether mg/kg .05 0.050 101 68-144
Ethyl benzene mg/kg .05 0.052 103 69-141
Hexachloro-1,3-butadiene mg/kg .05 0.054 109 70-152
lsopropylbenzene (Cumene) mg/kg .05 0.054 108 77-143
m&p-Xylene mg/kg .1 0.11 106 72-138
Methyl-tert-butyl ether mg/kg .05 0.050 101 2-138
Methylene Chloride mg/kg .05 0.049 98 69-136
n-Butylbenzene mg/kg .05 0.052 105 65-128
n-Propylbenzene mg/kg .05 0.053 107 72-139
Naphthalene mg/kg .05 0.054 109 61-138
a-Xylene mg/kg .05 0.054 108 74-137
p-lsopropyltoluene mg/kg .05 0.053 106 66-128
sec-Butylbenzene mg/kg .05 0.054 107 72-140
Styrene mg/kg .05 0.054 107 76-137
tert-Butylbenzene mg/kg .05 0.055 110 68-141
Tetrachloroethene mg/kg .05 0.052 104 72-136
Toluene mg/kg .05 0.051 103 69-139
trans-1,2-Dichloroethene mg/kg .05 0.050 100 72-144
trans-1,3-Dichloropropene mg/kg .05 0.052 104 73-135
Date: 04/30/2010 06:21 PM REPORT OF LABORATORY ANALYSIS Page 33 of 38
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~~ «, +c,.,.
i ~
www.pacetabs.oom
Project: Robo Chevron
Pace Project No.: 9267551
LABORATORY CONTROL SAMPLE: 431208
Parameter
Trichloroethene
Trichlorofluoroinettiane
Vinyl acetate
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-dB (S)
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
Units
MATRIX SPIKE SAMPLE: 431570
Parameter
1, 1-Dichloroethene
Benzene
Chlorobenzene
Toluene
Trichloroethene
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-dB (S)
SAMPLE DUPLICATE: 431650
Parameter
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
1, 1, 1,2-Tetrachloroethane mg/kg
1, 1, 1-Trichloroethane mg/kg
1, 1,2,2-Tetrachloroethane mg/kg
1,1,2-Trichloroethane mg/kg
1, 1-Dichloroethane mg/kg
1, 1-Dichloroethene mg/kg
1, 1-Dichloropropene mg/kg
1,2,3-Trichlorobenzene mg/kg
1,2,3-Trichloropropane mg/kg
1,2,4-Trichlorobenzene mg/kg
1,2,4-Trimethylbenzene mg/kg
1,2-Dibromo-3-chloropropane mg/kg
1,2-Dibromoethane (EDB) mg/kg
1,2-Dichlorobenzene mg/kg
1,2-Dichloroethane mg/kg
1,2-Dichloropropane mg/kg
1,3,5-T rimethylbenzene mg/kg
1 ,3-Dichlorobenzene mg/kg
1,3-Dichloropropane mg/kg
1,4-Dichlorobenzene mg/kg
Date: 04/30/2010 06:21 PM
Units
Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike LCS LCS
Cone. Result %Rec
.05 0.052 104
.05 0.057 113
.1 0.10 104
.05 0.054 107
99
100
95
100
9267634003 Spike MS
Result Cone. Result
ND .048 0.043
ND .048 0.039
ND .048 0.035
ND .048 0.038
ND .048 0.039
9267634004-Dup
Result Result RPO
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
%Rec
Limits
75-136
69-144
50-150
61-145
69-121
74-115
79-116
88-110
MS
%Rec
89
81
73
79
80
102
96
103
100
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
%Rec
Limits Qualifiers
33-158
46-143
29-159
38-145
70-130
69-121
74-115
79-116
88-110
Page 34of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
SAMPLE DUPLICATE: 431650
Parameter
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bro mo benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethyl benzene
-Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
m&p-Xylene
Methyl-tert-butyl ether
Methylene Chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
a-Xylene
p-lsopropyltoluene
sec-Butyl benzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
T richlorofluoromethane
Vinyl acetate
Vinyl chloride
1,2-Dichloroethan~4 (S)
4-Bromofluorobenzene (S)
Date: 04/30/2010 06:21 PM
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9267634004
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
101
97
Dup
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
103
95
RPO
2
6
Qualifiers
. REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
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~ ~ ff 1
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page35 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
SAMPLE DUPLICATE: 431650
Parameter
Dibromofluoromethane {S)
Toluene-dB (S)
Date: 04/30/2010 06:21 PM
%
%
Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9267634004
Result
96
101
Dup
Result
104
101
RPO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Q \ll ACCoiib
0 ~ , i 1
3
5
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of38
www.pacelabs.com
Project: Robo Chevron
Pace Project No.: 9267551
QC Batch: PMST/3149
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9267551001, 9267551002, 9267551003, 9267551004, 9267551005
SAMPLE DUPLICATE: 432820
Parameter Units
Percent Moisture %
SAMPLE DUPLICATE: 432821
Parameter Units
Percent Moisture %
Date: 04/30/2010 06:21 PM
9267127048
Result
22.8
9267551002
Result
18.8
Dup
Result
Dup
Result
RP.D
22.1
RPO
19.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Qualifiers
3
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of38
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Robo Chevron
Pace Project No.: 9267551
DEFINITIONS
OF -Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND -Not Detected at or above adjusted reporting limit.
J -Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S -Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPO values.
LCS(D) -Laboratory Control Sample (Duplicate)
MS(D) -Matrix Spike (Duplicate)
DUP -Sample Duplicate
RPO -Relative Percent Difference
NC -Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U -Indicates the compound was analyzed for, but not detected.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).
Date: 04/30/2010 06:21 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
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~ -:} ~ !: ~
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aAnalyticaJ.
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CHAIN-OF-CUSTODY / Analytical Request Document
The Chain-of-Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C Page: \ of I
Required Client Information: Required Project Information: Invoice Information: 1294486
w~"""~v,\\e., Nr V .., ' Address: r NPDES r GROUNDWATER r DRINKINGWATER 1::--.:-::....:....:."+~=--....:...,.=:....~:....!!lo ...... _-+.:,........,--:-e......,..,----,----------1:---=-,---------------I Email To: I Purchase Order No.: A _ / _ Pace Quote ,.,._ UST r RCRA r OTHER ____ _ I:::' .-, I,, ,,., Reference: Y"I
·,6
7,
8,
10
.: I 12
SecUon D
RaqulredCllenl lnfonnallon
SAMPLE ID
(A-Z,0-9/,·)
Sample IDs MUST BE UNIQUE
Matrix Codes i 1i: M6IBl21 l QQl:!la :;; COLLECTED s 8 Drinking Water DW !!l Water WT 1l II u Waste Water WW COMPOSITE COMPOSITE 'C I START END/GRAB Product p 1 SolVSolld SL ! C) 011 OL !k, Wipe WP w Air AR C w Tissue TS 0 a.
Other OT (..l ~ !:S w I ..I a. :; ;;!j DAT: TIME DATE
Presetvatlves
5L C 1M, 10 ( ~ 1./f'.
;,[ (' 'o/q, ft ( J:.~
~ c., i.ir4 t1 l \'n
~L '("' ,:l;I~ It \\\ ~o
I
ORIGINAL PRINT Name of SAMPLER:
SIGNATURE of SAMPL,E.R_: ·
'Important Note: By signing lhla fonn you are accepting Pace's Nl:T 30 day payment tenns and agreeing to late charges of 1.6% per month ·ro, any Invoices not paid within 30 days. 1·,, '
M::NJ!l~91!8,S,!if~:~Qaly~J.tf,l!\~r!i~ :(YI~)>:;", Yi i · .. ' '
I DATE Signed
IMM/DD/YY):
jf55}/,,;. ·, ,:) I
j
SAMPLE CONDITIONS
I->
.5 0. E ~
y
F-ALL-Q-020rev.07, 15-May-2007
Sample Condition Upon Receipt
Client Name: j 0 .r:Joo< Project # __ "1_.__2___,,C.._7_,_z ____ o~
Where Received: D Huntersville ~ville D Eden
Courier: D Fed Ex D UPS D USPS ~nt D Commercial D Pace Other __ _ 0
Custody Seal on Cooler/Box Present: D yes [::;J,1io'.. Seals intact: D yes ~
Packing Material: D Bubble Wrap ~le Bags D None Dother ___ _
Thermometer Used~/ 72490786 Type of Ice:~ Blue None ~les on ice, cooling process has begun
Temp Correction Factor: Ad~ e; -V C
Corrected Cooler Temp.: ~-7 C Biological Tissue is Frozen: Yes No Date and lnitial~rso/4a~lng
contents: ~ c, · / r-.,
Temp should be above freezing to 6°C Comments:· -1/ /
Chain of Custody Present: ~·□No □NIA 1.
Chain of Custody Filled Out: ~□No □NIA 2.
Chain of Custody Relinquished: ~□No □NIA 3.
Sampler Name & Signature on COC: □Yes ~□NIA 4.
Samples Arrive_d within Hold Time: ~□No □NIA 5. -Short Hold Time Analysis (<72hr): □Yes~DN/A 6.
Rush Turn Around Time Requested: □Yes~ □NIA 7.
Sufficient Volume: ~□No □NIA 8.
Correct Containers Used: es □No □NIA 9.
-Pace Containers Used: ~□No □NIA
Containers Intact: ~No □NIA 10.
Filtered volume received for Dissolved tests □Yes □No~ 11.
Sample Labels match COC: jlIYes □No □NIA 12.
-Includes date/time/ID/Analysis Matrix: L: I ..-
All containers needing preservation have been checked. ~ □No □NIA 13.
All containers needing preservation are found to be in _pt'es □No ON/A _£--compliance with EPA recommendation.
exceptions: VOA, coliform, T0C, O&G, WI-DRO (water) □Yes~ Initial when completed
Samples checked for dechlorination: □Yes □No ~ 14.
Headspace in VOA Vials ( >6mm): □Yes □No ~A 15.
Trip Blank Present: □Yes □No ~ 16.
[)4(1:
,,,
Trip Blank Custody Seals Present □Yes □No
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution: Field Data Required? y / N
Person Contacted: Date/Time: -----------------------
Comments/ Resolution: --------------,----------------------------
Project Manager Review: f!-f Date: t.f:(,.a l to
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( Le out of hold, incorrect preservative, out of temp, incorrect containers)
Pace F-ASV-CS-03-Rev00
www:pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
April 21, 2010
Mr. Baker Jordan
Jordan Environmental, LLC
68 Little Horse Road
Waynesville, NC 28786
RE: Project: ROSO CHEVRON 04/09
Pace Project No.: 9267119
Dear Mr. Jordan:
Enclosed are the analytical results for sample(s) received by the laboratory on April 09, 2010. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
of'~-~
Lorri Patton
[e-mail]
Project Manager
Enclosures
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Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
Charlotte Certification IDs
9800 Kincey Ave. -Ste 100 Huntersville, NC 28078
Connecticut Certification#: PH-0104
Virginia Certification#: 00213
Tennessee Certification#: 04010
South Carolina Drinking Water Cert. #: 990060003
South Carolina Certification #: 990060001
Pennsylvania Certification #: 68-00784
North Carolina Wastewater Certification #: 12
Pace Analytical Services, Inc.
2225 Riverside Dr.
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[phone]
CERTIFICATIONS
North Carolina Field Services Certification #: 5342
North Carolina Drinking Water Certification #: 37706
New Jersey Certification#: NC012
Louisiana/LEL.AP Certification #: 04034
Kentucky UST Certification #: 84
Florida/NEL.AP Certification #: E87627
West Virginia Certification #: 357
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc ..
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Huntersville, NC 28078
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Page2 of21
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Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
Sample: MW-1 LablD: 9267119001 Collected: 04/09/10 13:20 Received: 04/09/10 15:18 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CASNo. Qual
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18) 292 ug/L 156 04/14/10 07:30 04/14/10 20:24
Aliphatic (C19-C36) ND ug/L 156 04/14/10 07:30 04/14/10 20:24
Aromatic (C11-C22) 911 ug/L 156 1 04/14/10 07:30 04/14/10 20:24
Nonatriacontane (S) 77 % 40-140 1 04/14/10 07:30 04/14/10 20:24 7194-86-7
o-Terphenyl (S) 78 % 40-140 1 04/14/10 07:30 04/14/10 20:24 84-15-1
2-Fluorobiphenyl (S) 109 % 40-140 1 04/14/10 07:30 04/14/10 20:24 321-60-8
2-Bromonaphthalene (S) 112 % 40-140 1 04/14/10 07:30 04/14/10 20:24 580-13-2
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (COS-COB) ND ug/L 1000 10 04/14/10 14:50
Aliphatic (C09-C12) 2120 ug/L 1000 10 04/14/10 14:50
Aromatic (C09-C10) ND ug/L 1000 10 04/14/10 14:50
2,5-Dibromotoluene (PID)(S) 122 % 70-130 10 04/14/10 14:50
2,5-Dibromotoluene (FID}(S) 177 % 70-130 10 04/14/10 14:50 S5
625MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 83-32-9
Acenaphthylene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 208-96-8
Anthracene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 120-12-7
Benzo(a)anthracene ND ug/L 7.7 1 04/12/10 08:00 04/20/10 04:26 56-55-3
Benzo(a)pyrene ND ug/L 7.7 1 04/12/10 08:00 04/20/10 04:26 50-32-8
Benzo(b )fluoranthene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 205-99-2
Benzo(g ,h,i)perylene ND ug/L 7.7 1 04/12/10 08:00 04/20/10 04:26 191-24-2
Benzo(k)fluoranthene ND ug/L 7.7 1 04/12/10 08:00 04/20/10 04:26 207-08-9
4-Bromophenylphenyl ether ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 101-55-3
Butylbenzylphthalate ND ug/L 7.7 1 04/12/10 08:00 04/20/10 04:26 85-68-7
4-Chloro-3-methylphenol ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 15.4 1 04/12/10 08:00 04/20/10 04:26 111-91-1
bis(2-Chloroethyl) ether ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 111-44-4
bis(2-Chloroisopropyl) ether ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 108-60-1
2-Chloronaphthalene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 91-58-7
2-Chlorophenol ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 95-57-8
4-Chlorophenylphenyl ether ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 7005-72-3
Chrysene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 218-01-9
Dibenz(a,h)anthracene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 53-70-3
3,3'-Dichlorobenzidine ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 91-94-1
2,4-Dichlorophenol ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 120-83-2
Diethylphthalate ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 84-66-2
2,4-Dimethylphenol ND ug/L 15.4 04/12/10 08:00 04/20/10 04:26 105-67-9
Dimethylphthalate ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 131-11-3
Di-n-butylphthalate ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 84-74-2
4,6-Dinitro-2-methylphenol ND ug/L 30.8 04/12/10 08:00 04/20/10 04:26 534-52-1
2,4-Dinitrophenol ND ug/L 76.9 1 04/12/10 08:00 04/20/10 04:26 51-28-5
2,4-Dinitrotoluene ND ug/L 7.7 1 04/12/10 08:00 04/20/10 04:26 121-14-2
2,6-Dinitrotoluene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 606-20-2
Di-n-octylphthalate ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 117-84-0
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS Page 3 of21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
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Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
Sample: MW-1 LablD: 9267119001 Collected: 04/09/10 13:20 Received: 04/09/10 15:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CASNo. Qual
625MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
bis(2-Ethylhexyl)phthalate ND ug/L 7.7 1 04/12/10 08:00 04/20/10 04:26 117-81-7
Fluoranthene ND ug/L 7.7 1 04/12/10 08:00 04/20/10 04:26 206-44-0
Fluorene 10.8 ug/L 7.7 1 04/12/10 08:00 04/20/10 04:26 86-73-7
Hexachloro-1,3-butadiene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 87-68-3
Hexachlorobenzene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 118-74-1
Hexachlorocyclopentadiene ND ug/L 15.4 04/12/10 08:00 04/20/10 04:26 77-47-4
Hexachloroethane ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 67-72-1
lndeno(1,2,3-cd)pyrene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 193-39-5
lsophorone ND ug/L 15.4 04/12/10 08:00 04/20/10 04:26 78-59-1
Naphthalene 15.4 ug/L 7.7 04/12/10 08:00 04/20/10 04:26 91-20-3
Nitro benzene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 98-95-3
2-Nitrophenol ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 88-75-5
4-Nitrophenol ND ug/L 76.9 04/12/10 08:00 04/20/10 04:26 100-02-7
N-Nitrosodimethylamine ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 62-75-9
N-Nitros0-0i-n-propylamine ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 621-64-7
N-Nitrosodiphenylamine ND ug/L 15.4 04/12/10 08:00 04/20/10 04:26 86-30-6
Pentachlorophenol ND ug/L 38.5 04/12/10 08:00 04/20/10 04:26 87-86-5
Phenanthrene 8.9 ug/L 7.7 04/12/10 08:00 04/20/10 04:26 85-01-8
Phenol ND ug/L 7.7 1 04/12/10 08:00 04/20/10 04:26 108-95-2
Pyrene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 129-00-0
1,2,4-Trichlorobenzene ND ug/L 7.7 04/12/10 08:00 04/20/10 04:26 120-82-1
2,4,6-Trichlorophenol ND ug/L 15.4 1 04/12/10 08:00 04/20/10 04:26 88-06-2
Nitrobenzene-d5 (S) 61 % 10-120 1 04/12/10 08:00 04/20/10 04:26 4165-60-0
2-Fluorobiphenyl (S) 71 % 15-120 04/12/10 08:00 04/20/10 04:26 321-60-8
Terphenyl-d14 (S) 86 % 11-131 1 04/12/10 08:00 04/20/10 04:26 1718-51-0
Phenol-d6 (S) 30 % 10-120 1 04/12/10 08:00 04/20/10 04:26 13127-88-3
2-Fluorophenol (S) 38 % 10-120 1 04/12/10 08:00 04/20/10 04:26 367-12-4
2,4,6-Tribromophenol (S) 95 % 10-137 1 04/12/10 08:00 04/20/10 04:26 118-79-6
6200BMSV Analytical Method: SM 62008
Benzene 209 ug/L 1.2 2.5 04/12/10 14:50 71-43-2
Bromobenzene ND ug/L 1.2 2.5 04/12/10 14:50 108-86-1
Bromochloromethane ND ug/L 1.2 2.5 04/12/10 14:50 74-97-5
Bromodichloromethane ND ug/L 1.2 2.5 04/12/10 14:50 75-27-4
Bromoform ND ug/L 1.2 2.5 04/12/10 14:50 75-25-2
Bromomethane ND ug/L 12.5 2.5 04/12/10 14:50 74-83-9
n-Butylbenzene 3.6 ug/L 1.2 2.5 04/12/10 14:50 104-51-8
sec-Butylbenzene 6.3 ug/L 1.2 2.5 04/12/10 14:50 135-98-8
tert-Butylbenzene ND ug/L 1.2 2.5 04/12/10 14:50 98-06-6
Carbon tetrachloride ND ug/L 1.2 2.5 04/12/10 14:50 56-23-5
Chlorobenzene ND ug/L 1.2 2.5 04/12/10 14:50 108-90-7
Chloroethane ND ug/L 2.5 2.5 04/12/10 14:50 75-00-3
Chloroform ND ug/L 1.2 2.5 04/12/10 14:50 67-66-3
Chloromethane ND ug/L 2.5 2.5 04/12/10 14:50 74-87-3
2-Chlorotoluene ND ug/L 1.2 2.5 04/12/10 14:50 95-49-8
4-Chlorotoluene ND ug/L 1.2 2.5 04/12/10 14:50 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 2.5 2.5 04/12/10 14:50 96-12-8
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS Page 4 of21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ ~ , i 1
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Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ROSO CHEVRON 04/09
Pace Project No.: 9267119
Sample: MW-1 lab ID: 9267119001 Collected: 04/09/10 13:20 Received: 04/09/10 15:18 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CASNo. Qual
6200BMSV Analytical Method: SM 62008
Dibromochloromethane ND ug/L 1.2 2.5 04/12/10 14:50 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.2 2.5 04/12/10 14:50 106-93-4
Dibromomethane ND ug/L 1.2 2.5 04/12/10 14:50 74-95-3
1,2-Dichlorobenzene ND ug/L 1.2 2.5 04/12/10 14:50 95-50-1
1,3-Dichlorobenzene ND ug/L 1.2 2.5 04/12/10 14:50 541-73-1
1,4-Dichlorobenzene ND ug/L 1.2 2.5 04/12/10 14:50 106-46-7
Dichlorodifluoromethane ND ug/L 1.2 2.5 04/12/10 14:50 75-71-8
1, 1-Dichloroethane ND ug/L 1.2 2.5 04/12/10 14:50 75-34-3
1,2-Dichloroethane ND ug/L 1.2 2.5 04/12/10 14:50 107-06-2
1, 1-Dichloroethene ND ug/L 1.2 2.5 04/12/10 14:50 75-35-4
cis-1,2-Dichloroethene ND ug/L 1.2 2.5 04/12/10 14:50 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.2 2.5 04/12/10 14:50 156-60-5
1,2-Dichloropropane ND ug/L 1.2 2.5 04/12/10 14:50 78-87-5
1,3-Dichloropropane ND ug/L 1.2 2.5 04/12/10 14:50 142-28-9
2,2-Dichloropropane ND ug/L 1.2 2.5 04/12/10 14:50 594-20-7
1, 1-Dichloropropene ND ug/L 1.2 2.5 04/12/10 14:50 563-58-6
cis-1,3-Dichloropropene ND ug/L 1.2 2.5 04/12/10 14:50 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.2 2.5 04/12/10 14:50 10061-02-6
Diisopropyl ether 4.5 ug/L 1.2 2.5 04/12/10 14:50 108-20-3
Ethylbenzene 58.6 ug/L 1.2 2.5 04/12/10 14:50 100-41-4
Hexachloro-1,3-butadiene ND ug/L 5.0 2.5 04/12/10 14:50 87-68-3
lsopropylbenzene (Cumene) 8.5 ug/L 1.2 2.5 04/12/10 14:50 98-82-8
Methylene Chloride ND ug/L 5.0 2.5 04/12/10 14:50 75-09-2
Methyl-tert-butyl ether 1.5 ug/L 1.2 2.5 04/12/10 14:50 1634-04-4
Naphthalene 31.5 ug/L 5.0 2.5 04/12/10 14:50 91-20-3
n-Propylbenzene 10.1 ug/L 1.2 2.5 04/12/10 14:50 103-65-1
Styrene ND ug/L 1.2 2.5 04/12/10 14:50 100-42-5
1, 1, 1,2-Tetrachloroethane ND ug/L 1.2 2.5 04/12/10 14:50 630-20-6
1, 1,2,2-Tetrachloroethane ND ug/L 1.2 2.5 04/12/10 14:50 79-34-5
Tetrachloroethene ND ug/L 1.2 2.5 04/12/10 14:50 127-18-4
Toluene 44.1 ug/L 1.2 2.5 04/12/10 14:50 108-88-3
1,2,3-Trichlorobenzene ND ug/L 5.0 2.5 04/12/10 14:50 87-61-6
1,2,4-T richlorobenzene ND ug/L 5.0 2.5 04/12/10 14:50 120-82-1
1, 1, 1-Trichloroethane ND ug/L 1.2 2.5 04/12/10 14:50 71-55-6
1, 1,2-Trichloroethane ND ug/L 1.2 2.5 04/12/10 14:50 79-00-5
Trichloroethene ND ug/L 1.2 2.5 04/12/10 14:50 79-01-6
Trichlorofluoromethane ND ug/L 2.5 2.5 04/12/10 14:50 75-69-4
1,2,3-Trichloropropane ND ug/L 1.2 2.5 04/12/10 14:50 96-18-4
1,2,4-Trimethylbenzene 6.2 ug/L 1.2 2.5 04/12/10 14:50 95-63-6
1,3,5-Trimethylbenzene ND ug/L 1.2 2.5 04/12/10 14:50 108-67-8
Vinyl chloride ND ug/L 2.5 2.5 04/12/10 14:50 75-01-4
m&p-Xylene 37.4 ug/L 2.5 2.5 04/12/10 14:50 1330-20-7
a-Xylene 3.2 ug/L 1.2 2.5 04/12/10 14:50 95-47-6
1,2-Dichloroethane-d4 (S) 87 % 70-130 2.5 04/12/10 14:50 17060-07-0
Dibromofluoromethane (S) 89 % 70-130 2.5 04/12/10 14:50 1868-53-7
4-Bromofluorobenzene (S) 113 % 70-130 2.5 04/12/10 14:50 460-00-4
Toluene-dB (S) 96 % 70-130 2.5 04/12/10 14:50 2037-26-5
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS Page 5 of21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
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Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
Sample: MW-2
Parameters
MADEP EPH NC Water
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Nonatriacontane (S)
o-Terphenyl (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
VPH NC Water
Aliphatic (C05-C08)
Aliphatic (C09-C12)
Aromatic (C09-C10)
2,5-Dibromotoluene (PID)(S)
2,5-Dibromotoluene (FID)(S)
625MSSV
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g ,h,i)perylene
Benzo(k)fluoranthene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
Date: 04/21/2010 02:59 PM
LablD: 9267119002 Collected: 04/09/10 12:20 Received: 04/09/10 15:18 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No.
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
3820 ug/L
648 ug/L
3600 ug/L
571 4
571 4
143 1
40-140 4
40-140 1
04/14/10 07:30 04/15/10 09:19
04/14/10 07:30 04/15/10 09:19
04/14/10 07:30 04/14/10 21:00
04/14/10 07:30 04/15/10 09:19 7194-86-7
04/14/10 07:30 04/14/10 21:00 84-15-1
Qual
92 %
110 %
153 %
153 %
40-140 1 04/14/10 07:30 04/14/10 21:00 321-60-8 S5
40-140 1 04/14/10 07:30 04/14/10 21:00 580-13-2 S5
Analytical Method: MADEP VPH
ND ug/L
1060 ug/L
353 ug/L
119 %
164 %
100 1
100 1
100 1
70-130
70-130 1
04/13/10 16:28
04/13/10 16:28
04/13/10 16:28
04/13/10 16:28
04/13/10 16:28
Analytical Method: EPA 625 Preparation Method: EPA 625
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
12.5 1
12.5 1
12.5 1
12.5
12.5
12.5
12.5
12.5
12.5
12.5 1
12.5 1
25.0 1
12.5 1
12.5 1
12.5 1
12.5 1
12.5
12.5
12.5
12.5
12.5 1
12.5 1
25.0 1
12.5 1
12.5 1
50.0 1
125 1
12.5 1
12.5 1
12.5 1
04/12/10 08:00 04/20/10 04:53 83-32-9
04/12/10 08:00 04/20/10 04:53 208-96-8
04/12/10 08:00 04/20/10 04:53 120-12-7
04/12/10 08:00 04/20/10 04:53 56-55-3
04/12/10 08:00 04/20/10 04:53 50-32-8
04/12/10 08:00 04/20/10 04:53 205-99-2
04/12/10 08:00 04/20/10 04:53 191-24-2
04/12/10 08:00 04/20/10 04:53 207-08-9
04/12/10 08:00 04/20/10 04:53 101-55-3
04/12/10 08:00 04/20/10 04:53 85-68-7
04/12/10 08:00 04/20/10 04:53 59-50-7
04/12/10 08:00 04/20/10 04:53 111-91-1
04/12/10 08:00 04/20/10 04:53 111-44-4
04/12/10 08:00 04/20/10 04:53 108-60-1
04/12/10 08:00 04/20/10 04:53 91-58-7
04/12/10 08:00 04/20/10 04:53 95-57-8
04/12/10 08:00 04/20/10 04:53 7005-72-3
04/12/10 08:00 04/20/10 04:53 218-01-9
04/12/10 08:00 04/20/10 04:53 53-70-3
04/12/10 08:00 04/20/10 04:53 91-94-1
04/12/10 08:00 04/20/10 04:53 120-83-2
04/12/10 08:00 04/20/10 04:53 84-66-2
04/12/10 08:00 04/20/10 04:53 105-67-9
04/12/10 08:00 04/20/10 04:53 131-11-3
04/12/10 08:00 04/20/10 04:53 84-74-2
04/12/10 08:00 04/20/10 04:53 534-52-1
04/12/10 08:00 04/20/10 04:53 51-28-5
04/12/10 08:00 04/20/10 04:53 121-14-2
04/12/10 08:00 04/20/10 04:53 606-20-2
04/12/10 08:00 04/20/10 04:53 117-84-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
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S5
Page 6 of21
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
Sample: MW-2 LablD: 9267119002 Collected: 04/09/10 12:20 Received: 04/09/10 15:18 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CASNo. Qual
625MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
bis(2-Ethylhexyl)phthalate ND ug/L 12.5 04/12/10 08:00 04/20/10 04:53 117-81-7
Fluoranthene ND ug/L 12.5 04/12/10 08:00 04/20/10 04:53 206-44-0
Fluorene ND ug/L 12.5 1 04/12/10 08:00 04/20/10 04:53 86-73-7
Hexachloro-1,3-butadiene ND ug/L 12.5 1 04/12/10 08:00 04/20/10 04:53 87-68-3
Hexachlorobenzene ND ug/L 12.5 04/12/10 08:00 04/20/10 04:53 118-74-1
Hexachlorocyclopentadiene ND ug/L 25.0 1 04/12/10 08:00 04/20/10 04:53 77-47-4
Hexachloroethane ND ug/L 12.5 1 04/12/10 08:00 04/20/10 04:53 67-72-1
lndeno(1,2,3-cd)pyrene ND ug/L 12.5 1 04/12/10 08:00 04/20/10 04:53 193-39-5
lsophorone ND ug/L 25.0 04/12/10 08:00 04/20/10 04:53 78-59-1
Naphthalene 44.1 ug/L 12.5 04/12/10 08:00 04/20/10 04:53 91-20-3
Nitrobenzene ND ug/L 12.5 04/12/10 08:00 04/20/10 04:53 98-95-3
2-Nitrophenol ND ug/L 12.5 04/12/10 08:00 04/20/10 04:53 88-75-5
4-Nitrophenol ND ug/L 125 04/12/10 08:00 04/20/10 04:53 100-02-7
N-Nilrosodimelhylamine ND ug/L 12.5 04/12/10 08:00 04/20/10 04:53 62-75-9
N-Nitroso-di-n-propylamine ND ug/L 12.5 1 04/12/10 08:00 04/20/10 04:53 621-64-7
N-Nilrosodiphenylamine ND ug/L 25.0 1 04/12/10 08:00 04/20/10 04:53 86-30-6
Pentachlorophenol ND ug/L 62.5 1 04/12/10 08:00 04/20/10 04:53 87-86-5
Phenanthrene ND ug/L 12.5 1 04/12/10 08:00 04/20/10 04:53 85-01-8
Phenol ND ug/L 12.5 04/12/10 08:00 04/20/10 04:53 108-95-2
Pyrene ND ug/L 12.5 04/12/10 08:00 04/20/10 04:53 129-00-0
1,2,4-Trichlorobenzene ND ug/L 12.5 04/12/10 08:00 04/20/10 04:53 120-82-1
2,4,6-Trichlorophenol ND ug/L 25.0 04/12/10 08:00 04/20/10 04:53 88-06-2
Nitrobenzene-d5 (S) 57 % 10-120 04/12/10 08:00 04/20/10 04:53 4165-60-0
2-Fluorobiphenyl (S) 63 % 15-120 04/12/10 08:00 04/20/10 04:53 321-60-8
Terphenyl-d14 (S) 82 % 11-131 04/12/10 08:00 04/20/10 04:53 1718-51-0
Phenol-d6 (S) 42 % 10-120 04/12/10 08:00 04/20/10 04:53 13127-88-3
2-Fluorophenol (S) 48 % 10-120 04/12/10 08:00 04/20/10 04:53 367-12-4
2,4,6-Tribromophenol (S) 93 % 10-137 04/12/10 08:00 04/20/10 04:53 118-79-6
6200BMSV Analytical Method: SM 6200B
Benzene 9.2 ug/L 0.50 1 04/12/10 12:58 71-43-2
Bromobenzene ND ug/L 0.50 1 04/12/10 12:58 108-86-1
Bromochloromethane ND ug/L 0.50 1 04/12/10 12:58 74-97-5
Bromodichloromethane ND ug/L 0.50 04/12/10 12:58 75-27-4
Bromoform ND ug/L 0.50 04/12/10 12:58 75-25-2
Bromomethane ND ug/L 5.0 04/12/10 12:58 74-83-9
n-Butylbenzene 8.3 ug/L 0.50 04/12/10 12:58 104-51-8
sec-Butylbenzene 17.8 ug/L 0.50 04/12/10 12:58 135-98-8
tert-Butylbenzene 2.6 ug/L 0.50 1 04/12/10 12:58 98-06-6
Carbon tetrachloride ND ug/L 0.50 1 04/12/10 12:58 56-23-5
Chlorobenzene ND ug/L 0.50 1 04/12/10 12:58 108-90-7
Chloroethane ND ug/L 1.0 04/12/10 12:58 75-00-3
Chloroform ND ug/L 0.50 04/12/10 12:58 67-66-3
Chloromethane ND ug/L 1.0 04/12/10 12:58 74-87-3
2-Chlorotoluene ND ug/L 0.50 04/12/10 12:58 95-49-8
4-Chlorotoluene ND ug/L 0.50 1 04/12/10 12:58 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 04/12/10 12:58 96-12-8
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS Page 7 of21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
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Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
Sample: MW-2
Parameters
6200B MSV
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethyl benzene
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-T richloroethane
1, 1,2-Trichloroethane
T richloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
1,2-Dichloroethane-d4 (S)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-dB (S)
Date: 04/21/2010 02:59 PM
LablD: 9267119002 Collected: 04/09/10 12:20 Received: 04/09/10 15:18 Matrix: Water
Results Units Report Limit DF Prepared
Analytical Method: SM 6200B
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
46.9 ug/L 0.50
ND ug/L 2.0
24.0 ug/L 0.50
ND ug/L 2.0
3.4 ug/L 0.50
183 ug/L 2.0
27.3 ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 2.0
ND ug/L 2.0
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 0.50
ND ug/L 1.0
ND ug/L 0.50
ND ug/L 0.50
1.1 ug/L 0.50
ND ug/L 1.0
1.2 ug/L 1.0
ND ug/L 0.50
86 % 70-130
89 % 70-130
113 % 70-130
97 % 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ ,,.. ACco,,0
~ -f 1
Analyzed CASNo.
04/12/10 12:58 124-48-1
04/12/10 12:58 106-93-4
04/12/10 12:58 74-95-3
04/12/10 12:58 95-50-1
04/12/10 12:58 541-73-1
04/12/10 12:58 106-46-7
04/12/10 12:58 75-71-8
04/12/10 12:58 75-34-3
04/12/10 12:58 107-06-2
04/12/10 12:58 75-35-4
04/12/10 12:58 156-59-2
04/12/10 12:58 156-60-5
04/12/10 12:58 78-87-5
04/12/10 12:58 142-28-9
04/12/10 12:58 594-20-7
04/12/10 12:58 563-58-6
04/12/10 12:58 10061-01-5
04/12/10 12:58 10061-02-6
04/12/10 12:58 108-20-3
04/12/10 12:58 100-41-4
04/12/10 12:58 87-68-3
04/12/10 12:58 98-82-8
04/12/10 12:58 75-09-2
04/12/10 12:58 1634-04-4
04/12/10 12:58 91-20-3
04/12/10 12:58 103-65-1
04/12/10 12:58 100-42-5
04/12/10 12:58 630-20-6
04/12/10 12:58 79-34-5
04/12/10 12:58 127-18-4
04/12/10 12:58 108-88-3
04/12/10 12:58 87-61-6
04/12/10 12:58 120-82-1
04/12/10 12:58 71-55-6
04/12/10 12:58 79-00-5
04/12/10 12:58 79-01-6
04/12/10 12:58 75-69-4
04/12/10 12:58 96-18-4
04/12/10 12:58 95-63-6
04/12/10 12:58 108-67-8
04/12/10 12:58 75-01-4
04/12/10 12:58 1330-20-7
04/12/10 12:58 95-47-6
04/12/10 12:58 17060-07-0
04/12/10 12:58 1868-53-7
04/12/10 12:58 460-00-4
04/12/10 12:58 2037-26-5
Qual
Page 8 of21
www.pacelabs.com
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
QC Batch: OEXT/9723
QC Batch Method: MADEP EPH
Associated Lab Samples: 9267119001, 9267119002
METHOD BLANK: 428191
Associated Lab Samples: 9267119001, 9267119002
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: MADEP EPH
Analysis Description: MADEP EPH NC Water
Matrix: Water
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Aliphatic (C09-C18) ug/L ND 100 04/14/10 15:02
Aliphatic (C19-C36) ug/L ND 100 04/14/10 15:02
Aromatic (C11-C22) ug/L ND 100 04/14/10 15:02
2-Bromonaphthalene (S) % 109 40-140 04/14/10 15:02
2-Fluorobiphenyl (S) % 107 40-140 04/14/10 15:02
Nonatriacontane (S) % 79 40-140 04/14/10 15:02
o-Terphenyl (S) % 87 40-140 04/14/10 15:02
LABORATORY CONTROL SAMPLE & LCSD: 428192 428193
Parameter Units
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
2-Bromonaphthalene (S)
2-Fluorobiphenyl (S)
Nonatriacontane (S)
o-Terphenyl (S)
Date: 04/21/2010 02:59 PM
ug/L
ug/L
ug/L
%
%
%
%
Spike LCS LCSD LCS LCSD
Cone. Result Result %Rec %Rec
----
300 148 187 49 62
400 289 316 72 79
850 820 822 96 97
113 106
115 109
80 85
96 91
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
%Rec
Limits RPO
40-140
40-140
40-140
40-140
40-140
40-140
40-140
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPO Qualifiers
23 50
9 50
0 50
Page 9 of21
www.pacelabs.com
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
QC Batch: GCV/3974
QC Batch Method: MADEP VPH
Associated Lab Samples: 9267119001, 9267119002
METHOD BLANK: 427801
Associated Lab Samples: 9267119001, 9267119002
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: MADEPVPH
Analysis Description: VPH NC Water
Matrix: Water
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Aliphatic (C05-C08) ug/L ND 100 04/13/10 13:35
Aliphatic (C09-C12) ug/L ND 100 04/13/10 13:35
Aromatic (C09-C10) ug/L ND 100 04/13/10 13:35
2,5-Dibromotoluene (FID)(S) % 117 70-130 04/13/10 13:35
2,5-Dibromotoluene (PID)(S) % 115 70-130 04/13/10 13:35
LABORATORY CONTROL SAMPLE & LCSD: 427802 427803
Parameter Units
Aliphatic (C05-C08) ug/L
Aliphatic (C09-C12) ug/L
Aromatic (C09-C10) ug/L
2,5-Dibromotoluene (FID)(S) %
2,5-Dibromotoluene (PID)(S) %
Date: 04/21/2010 02:59 PM
Spike LCS LCSD LCS LCSD
Cone. Result Result % Rec% Rec
----
300 302 311 101 104
300 305 323 102 108
100 ND 101 99 101
112 104
103 95
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
O \II ACC0-9b
0 l ~-r(~ • Cl.\,,,],
%Rec
Limits RPO
70-130
30-130
70-130
70-130
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPO Qualifiers
3 25
6 25
25
Page 10 of21
www.pacelabs.com
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
QC Batch: OEXT/9706
QC Batch Method: EPA625
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA625
Analysis Description: 625MSS
Associated Lab Samples: 9267119001,9267119002
METHOD BLANK: 427357 Matrix: Water
Associated Lab Samples: 9267119001,9267119002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,2,4-Trichlorobenzene ug/L ND 5.0 04/17/10 07:12
2,4,6-Trichlorophenol ug/L ND 10.0 04/17/10 07:12
2,4-Dichlorophenol ug/L ND 5.0 04/17/10 07:12
2,4-Dimethylphenol ug/L ND 10.0 04/17/10 07:12
2,4-Dinitrophenol ug/L ND 50.0 04/17/10 07:12
2,4-Dinitrotoluene ug/L ND 5.0 04/17/10 07:12
2,6-Dinitrotoluene ug/L ND 5.0 04/17/10 07:12
2-Chloronaphthalene ug/L ND 5.0 04/17/10 07:12
2-Chlorophenol ug/L ND 5.0 04/17/10 07:12
2-Nitrophenol ug/L ND 5.0 04/17/10 07:12
3,3'-Dichlorobenzidine_ ug/L ND 5.0 04/17/10 07:12
4,6-Dinitro-2-methylphenol ug/L ND 20.0 04/17/10 07:12
4-Bromophenylphenyl ether ug/L ND 5.0 04/17/10 07:12
4-Chloro-3-methylphenol ug/L ND 5.0 04/17/10 07:12
4-Chlorophenylphenyl ether ug/L ND 5.0 04/17/10 07:12
4-Nitrophenol ug/L ND 50.0 04/17/10 07:12
Acenaphthene ug/L ND 5.0 04/17/10 07:12
Acenaphthylene ug/L ND 5.0 04/17/10 07:12
Anthracene ug/L ND 5.0 04/17/10 07:12
Benzo(a)anthracene ug/L ND 5.0 04/17/10 07:12
Benzo(a)pyrene ug/L ND 5.0 04/17/10 07:12
Benzo(b )fluoranthene ug/L ND · 5.o 04/17/10 07:12
Benzo(g,h,i)perylene ug/L ND 5.0 04/17/10 07:12
Benzo(k)fluoranthene ug/L ND 5.0 04/17/10 07:12
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/17/10 07:12
bis(2-Chloroethyl) ether ug/L ND 5.0 04/17/10 07:12
bis(2-Chloroisopropyl) ether ug/L ND 5.0 04/17/10 07:12
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/17/10 07:12
Butylbenzylphthalate ug/L l\!D 5.0 04/17/10 07:12
Chrysene ug/L ND 5.0 04/17/10 07:12
Di-n-butylphthalate ug/L ND 5.0 04/17/10 07:12
Di-n-octylphthalate ug/L ND 5.0 04/17/10 07:12
Dibenz(a,h)anthracene ug/L ND 5.0 04/17/10 07:12
Diethylphthalate ug/L ND 5.0 04/17/10 07:12
Dimethylphthalate ug/L ND 5.0 04/17/10 07:12
Fluoranthene ug/L ND 5.0 04/17/10 07:12
Fluorene ug/L ND 5.0 04/17/10 07:12
Hexachloro-1,3-butadiene ug/L ND 5.0 04/17/10 07:12
Hexachlorobenzene ug/L ND 5.0 04/17/10 07:12
Hexachlorocyclopentadiene ug/L ND 10.0 04/17/10 07:12
Hexachloroethane ug/L ND 5.0 04/17/10 07:12
lndeno(1,2,3-cd)pyrene ug/L ND 5.0 04/17/10 07:12
lsophorone ug/L ND 10.0 04/17/10 07:12
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ t 0\
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 21
www.pacelabs.com
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
METHOD BLANK: 427357
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Matrix: Water
Associated Lab Samples: 9267119001,9267119002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
N-Nitroso-di-n-propylamine ug/L ND 5.0 04/17/10 07:12
N-Nitrosodimethylamine ug/L ND 5.0 04/17/10 07:12
N-Nitrosodiphenylamine ug/L ND 10.0 04/17/10 07:12
Naphthalene ug/L ND 5.0 04/17/10 07:12
Nitrobenzene ug/L ND 5.0 04/17/10 07:12
Pentachlorophenol ug/L ND 25.0 04/17/10 07:12
Phenanthrene ug/L ND 5.0 04/17/10 07:12
Phenol ug/L ND 5.0 04/17/10 07:12
Pyrene ug/L ND 5.0 04/17/10 07:12
2,4,6-Tribromophenol (S) % 88 10-137 04/17/10 07:12
2-Fluorobiphenyl (S) % 75 15-120 04/17/10 07:12
2-Fluorophenol (S) % 39 10-120 04/17/10 07:12
Nitrobenzene-d5 (S) % 71 10-120 04/17/10 07:12
Phenol-d6 (S) % 26 10-120 04/17/10 07:12
Terphenyl-d14 (S) % 90 11-131 04/17/10 07:12
LABORATORY CONTROL SAMPLE & LCSD: 427358 427359
Spike LCS LCSD LCS LCSD %Rec
Parameter Units Cone. Result Result % Rec %Rec Limits RPD ----
1,2,4-Trichlorobenzene ug/L 50 30.6 31.9 61 64 44-142
2,4,6-Trichlorophenol ug/L 50 45.0 47.6 90 95 37-144
2,4-Dichlorophenol ug/L 50 46.3 48.1 93 96 1-191
2,4-Dimethylphenol ug/L 50 36.7 37.4 73 75 32-119
2,4-Dinitrophenol ug/L 250 193 218 77 87 1-181
2,4-Dinitrotoluene ug/L 50 45.3 46.9 91 94 39-139
2,6-Dinitrotoluene ug/L 50 45.5 47.3 91 95 50-158
2-Chloronaphthalene ug/L 50 38.8 41.5 78 83 60-118
2-Chlorophenol ug/L 50 36.3 37.2 73 74 23-134
2-Nitrophenol ug/L 50 43.0 46.0 86 92 29-182
3,3'-Dichlorobenzidine ug/L 250 191 197 76 79 1-262
4,6-Dinitro-2-methylphenol ug/L 100 86.4 95.1 86 95 1-181
4-Bromophenylphenyl ether ug/L 50 41.8 44.2 84 88 53-127
4-Chloro-3-methylphenol ug/L 100 87.1 90.7 87 91 22-147
4-Chlorophenylphenyl ether ug/L 50 39.6 42.4 79 85 25-158
4-Nitrophenol ug/L 250 78.2 85.7 31 34 1-132
Acenaphthene ug/L 50 38.6 41.4 77 83 47-145
Acenaphthylene ug/L 50 38.2 40.9 76 82 33-145
Anthracene ug/L 50 40.8 42.8 82 86 1-166
Benzo(a)anthracene ug/L 50 40.3 43.5 81 87 33-143
Benzo(a)pyrene ug/L 50 35.8 37.5 72 75 17-163
Benzo(b)fluoranthene ug/L 50 37.4 39.7 75 79 24-159
Benzo(g,h,i)perylene ug/L 50 33.3 33.7 67 67 1-219
Benzo(k)fluoranthene ug/L 50 34.3 34.8 69 70 11-162
bis(2-Chloroethoxy)methane ug/L 50 35.5 37.8 71 76 33-184
bis(2-Chloroethyl) ether ug/L 50 35.5 35.7 71 71 12-158
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ ~ ~ i ~
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPD Qualifiers
4 30
6 30
4 30
2 30
12 30
4 30
4 30
7 30
2 30
7 30
3 30
10 30
6 30
4 30
7 30
9 30
7 30
7 30
5 30
8 30
5 30
6 30
1 30
1 30
6 30
0 30
Page 12 of21
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
LABORATORY CONTROL SAMPLE & LCSD: 427358 427359
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units Cone. Result Result %Rec% Rec Limits RPD RPD Qualifiers -----
bis(2-Chloroisopropyl) ether ug/L 50 29.8 30.2 60 60 36-166 1 30
bis(2-Ethylhexyl)phthalate ug/L 50 39.1 41.6 78 83 8-158 6 30
Butylbenzylphthalate ug/L 50 38.5 40.6 77 81 1-152 5 30
Chrysene ug/L 50 39.3 42.7 79 85 17-168 8 30
Di-n-butylphthalate ug/L 50 39.9 41.5 80 83 1-118 4 30
Di-n-octylphthalate ug/L 50 37.1 39.4 74 79 4-146 6 30
Dibenz(a,h)anthracene ug/L 50 35.3 36.1 71 72 1-227 2 30
Diethylphthalate ug/L 50 40.6 41.9 81 84 1-114 3 30
Dimethylphthalate ug/L 50 40.5 42.1 81 84 1-112 4 30
Fluoranthene ug/L 50 41.9 43.8 84 88 26-137 5 30
Fluorene ug/L 50 40.4 42.3 81 85 59-121 5 30
Hexachloro-1,3-butadiene ug/L 50 21.2 23.5 42 47 24-116 10 30
Hexachlorobenzene ug/L 50 47.6 49.4 95 99 1-152 4 30
Hexachlorocyclopentadiene ug/L 50 29.4 33.6 59 67 25-150 13 30
Hexachloroethane ug/L 50 18.3 19.7 37 39 40-113 7 30 L2
lndeno(1,2,3-cd)pyrene ug/L 50 33.9 36.1 68 72 1-171 6 30
lsophorone ug/L 50 39.7 42.5 79 85 21-196 7 30
N-Nitroso-di-n-propylamine ug/L 50 39.1 41.7 78 83 1-230 6 30
N-Nitrosodimethylamine ug/L 50 24.7 24.5 49 49 25-150 1 30
N-Nitrosodiphenylamine ug/L 50 44.3 46.5 89 93 25-150 5 30
Naphthalene ug/L 50 33.5 34.5 67 69 21-133 3 30
Nitrobenzene ug/L 50 38.7 40.0 77 80 35-180 3 30
Pentachlorophenol ug/L 250 206 225 82 90 14-176 9 30
Phenanthrene ug/L 50 39.5 41.2 79 82 54-120 4 30
Phenol ug/L 50 17.9 18.9 36 38 5-112 5 30
Pyrene ug/L 50 43.4 41.5 87 83 52-115 4 30
2,4,6-Tribromophenol (S) % 93 95 10-137
2-Fluorobiphenyl (S) % 73 77 15-120
2-Fluorophenol (S) % 42 43 10-120
Nitrobenzene-d5 (S) % 71 73 10-120
Phenol-cl6 (S) % 28 29 10-120
Terphenyl-d14 (S) % 84 80 11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 427360 427361
MS MSD
9266797001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual --
1,2,4-T richlorobenzene ug/L ND 100 100 65.8 52.9 66 53 44-142 22
2,4,6-Trichlorophenol ug/L ND 100 100 88.5 75.8 88 76 37-144 16
2,4-Dichlorophenol ug/L ND 100 100 96.8 74.1 97 74 1-191 27
2,4-Dimethylphenol ug/L ND 100 100 73.0 67.6 73 68 32-119 8
2,4-Dinitrophenol ug/L ND 500 500 405 367 81 73 1-181 10
2,4-Dinitrotoluene ug/L ND 100 100 92.0 72.1 92 72 39-139 24
2,6-Dinitrotoluene ug/L ND 100 100 91.8 71.0 92 71 50-158 26
2-Chloronaphthalene ug/L ND 100 100 82.4 67.6 82 68 60-118 20
2-Chlorophenol ug/L ND 100 100 81.2 56.1 81 56 23-134 37 M1,R1
2-Nitrophenol ug/L ND 100 100 84.0 68.3 84 68 29-182 21
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS Page 13 of21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ ~ -i l
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 427360 427361
MS MSD
9266797001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPO Qual -----3,3'-Dichlorobenzidine ug/L ND 500 500 387 332 77 66 1-262 15
4,6-Dinitro-2-methylphenol ug/L ND 200 200 174 165 87 82 1-181 6
4-Bromophenylphenyl ether ug/L ND 100 100 81.7 71.5 82 72 53-127 13
4-Chloro-3-methylphenol ug/L ND 200 200 189 151 95 75 22-147 22
4-Chlorophenylphenyl ether ug/L ND 100 100 81.6 68.9 82 69 25-158 17
4-Nitrophenol ug/L ND 500 500 283 257 57 51 1-132 10
Acenaphthene ug/L ND 100 100 82.4 70.0 82 70 47-145 16
Acenaphthylene ug/L ND 100 100 82.2 69.4 82 69 33-145 17
Anthracene ug/L ND 100 100 85.3 74.9 85 75 1-166 13
Benzo(a)anthracene ug/L ND 100 100 82.7 71.8 83 72 33-143 14
Benzo(a)pyrene ug/L ND 100 100 78.0 66.7 78 67 17-163 16
Benzo(b )fluoranthene ug/L ND 100 100 78.5 68.8 79 69 24-159 13
Benzo(g,h,i)perylene ug/L ND 100 100 77.2 69.8 77 70 1-219 10
Benzo{k)fluoranthene ug/L ND 100 100 78.2 64.7 78 65 11-162 19
bis(2-Chloroethoxy)methane ug/L ND 100 100 75.7 60.0 76 60 33-184 23
bis(2-Chloroethyl) ether ug/L ND 100 100 75.3 51.0 75 51 12-158 38 M1,R1
bis(2-Chloroisopropyl) ether ug/L ND 100 100 65.8 46.7 66 47 36-166 34 M1,R1
bis(2-Ethylhexyl)phthalate ug/L ND 100 100 81.5 65.4 81 65 8-158 22
Butylbenzylphthalate ug/L ND 100 100 81.4 65.3 81 65 1-152 22
Chrysene ug/L ND 100 100 80.7 70.8 81 71 17-168 13
Di-n-butylphthalate ug/L ND 100 100 83.6 66.9 84 67 1-118 22
Di-n-octylphthalate ug/L ND 100 100 89.3 70.8 89 71 4-146 23
Dibenz(a,h)anthracene ug/L ND 100 100 74.3 66.4 74 66 1-227 11
Diethylphthalate ug/L ND 100 100 83.1 66.0 83 66 1-114 23
Dimethylphthalate ug/L ND 100 100 80.5 64.7 81 65 1-112 22
Fluoranthene ug/L ND 100 100 89.2 75.7 89 76 26-137 16
Fluorene ug/L ND 100 100 85.5 72.1 85 72 59-121 17
Hexachloro-1,3-butadiene ug/L ND 100 100 56.0 46.9 56 47 24-116 18
Hexachlorobenzene ug/L ND 100 100 91.2 76.7 91 77 1-152 17
Hexachlorocyclopentadiene ug/L ND 100 100 58.0 52.2 58 52 25-150 11
Hexachloroethane ug/L ND 100 100 50.6 39.1 51 39 40-113 26 M0,M1
lndeno(1,2,3-cd)pyrene ug/L ND 100 100 73.9 66.1 74 66 1-171 11
lsophorone ug/L ND 100 100 86.7 65.5 87 66 21-196 28
N-Nitroso-di-n-propylamine ug/L ND 100 100 92.1 61.9 92 62 1-230 39 M1,R1
N-Nitrosodimethylamine ug/L ND 100 100 67.1 43.2 67 43 25-150 43 M1,R1
N-Nitrosodiphenylamine ug/L ND 100 100 89.2 75.7 89 76 25-150 16
Naphthalene ug/L ND 100 100 70.6 55.1 71 55 21-133 25
Nitrobenzene ug/L ND 100 100 76.0 54.8 76 55 35-180 33 M1,R1
Pentachlorophenol ug/L ND 500 500 391 360 78 72 14-176 8
Phenanthrene ug/L ND 100 100 82.0 71.9 82 72 54-120 13
Phenol ug/L ND 100 100 60.5 40.9 60 41 5-112 39 M1,R1
Pyrene ug/L ND 100 100 84.6 68.1 85 68 52-115 22
2,4,6-Tribromophenol (S) % 96 82 10-137
2-Fluorobiphenyl (S) % 74 66 15-120
2-Fluorophenol (S) % 61 43 10-120
Nitrobenzene-d5 (S) % 73 59 10-120
Phenol-d6 {S) % 53 37 10-120
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS Page 14 of21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
e ~ f ~\
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Pace Analytical Services, Inc.
2225 Riverside Dr.
QUALITY CONTROL DATA
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 427360 427361
Parameter
Terphenyl-d14 (S) %
Date: 04/21/2010 02:59 PM
MS MSD
9266797001 Spike MS MSD %Rec
Units Result Cone.
Spike
Cone.
MS
Result
MSD
Result % Rec % Rec Limits RPO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
() \~ ACco110
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81 70 11-131
Qual
Page 15 of21
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Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
QC Batch: MSV/10581
QC Batch Method: SM 62008
Associated Lab Samples: 9267119001, 9267119002
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
SM 62008
62008 MSV
METHOD BLANK: 427328 Matrix: Water
Associated Lab Samples: 9267119001, 9267119002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1, 1, 1,2-Tetrachloroethane ug/L ND 0.50 04/11/10 15:23
1, 1, 1-Trichloroethane ug/L ND 0.50 04/11/10 15:23
1, 1,2,2-Tetrachloroethane ug/L ND 0.50 04/11/10 15:23
1, 1,2-Trichloroethane ug/L ND 0.50 04/11/10 15:23
1, 1-Dichloroethane ug/L ND 0.50 04/11 /10 15:23
1, 1-Dichloroethene ug/L ND 0.50 04/11/10 15:23
1, 1-Dichloropropene ug/L ND 0.50 04/11/10 15:23
1,2,3-Trichlorobenzene ug/L ND 2.0 04/11/10 15:23
1,2,3-T richloropropane ug/L ND 0.50 04/11/10 15:23
1,2,4-Trichlorobenzene ug/L ND 2.0 04/11/10 15:23
1,2,4-Trimethylbenzene ug/L ND 0.50 04/11/10 15:23
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/11/10 15:23
1,2-Dibromoethane (EDB) ug/L ND 0.50 04/11/10 15:23
1,2-Dichlorobenzene ug/L ND 0.50 04/11/10 15:23
1,2-Dichloroethane ug/L ND 0.50 04/11/10 15:23
1,2-Dichloropropane ug/L ND 0.50 04/11 /10 15:23
1,3,5-Trimethylbenzene ug/L ND 0.50 04/11/10 15:23
1,3-Dichlorobenzene ug/L ND 0.50 04/11/10 15:23
1,3-Dichloropropane ug/L ND 0.50 04/11 /10 15:23
1 ,4-Dichlorobenzene ug/L ND 0.50 04/11/10 15:23
2,2-Dichloropropane ug/L ND 0.50 04/11/10 15:23
2-Chlorotoluene ug/L ,ND 0.50 04/11/10 15:23
4-Chlorotoluene ug/L I ND 0.50 04/11/10 15:23
Benzene ug/L ND 0.50 04/11/10 15:23
Bromobenzene ug/L ND 0.50 04/11/10 15:23
Bromochloromethane ug/L ND 0.50 04/11/10 15:23
Bromodichloromethane ug/L ND 0.50 04/11/10 15:23
Bromoform ug/L ND 0.50 04/11/10 15:23
Bro mo methane ug/L ND 5.0 04/11/10 15:23
Carbon tetrachloride ug/L ND 0.50 04/11 /10 15:23
Chlorobenzene ug/L ND 0.50 04/11/10 15:23
Chloroethane ug/L ND 1.0 04/11/10 15:23
Chloroform ug/L ND 0.50 04/11 /10 15:23
Chloromethane ug/L ND 1.0 04/11/10 15:23
cis-1,2-Dichloroethene ug/L ND 0.50 04/11/10 15:23
cis-1,3-Dichloropropene ug/L ND 0.50 04/11/10 15:23
Dibromochloromethane ug/L ND 0.50 04/11/10 15:23
Dibromomethane ug/L ND 0.50 04/11/10 15:23
Dichlorodifluoromethane ug/L ND 0.50 04/11/10 15:23
Diisopropyl ether ug/L ND 0.50 04/11/10 15:23
Ethylbenzene ug/L ND 0.50 04/11/10 15:23
Hexachloro-1,3-butadiene ug/L ND 2.0 04/11/10 15:23
lsopropylbenzene (Cumene) ug/L ND 0.50 04/11/10 15:23
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~ ~ ~ ? 1
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of21
W'NW.pacelabs.com
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
METHOD BLA.NK: 427328
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Matrix: Water
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Associated Lab Samples: 9267119001,9267119002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
m&p-Xylene ug/L ND 1.0 04/11/10 15:23
Methyl-tert-butyl ether ug/L ND 0.50 04/11/10 15:23
Methylene Chloride ug/L ND 2.0 04/11 /1 0 15:23
n-Butylbenzene ug/L ND 0.50 04/11/10 15:23
n-Propylbenzene ug/L ND 0.50 04/11/10 15:23
Naphthalene ug/L ND 2.0 04/11/10 15:23
o-Xylene ug/L ND 0.50 04/11/10 15:23
sec-Butylbenzene ug/L ND 0.50 04/11/10 15:23
Styrene ug/L ND 0.50 04/11/10 15:23
tert-Butylbenzene ug/L ND 0.50 04/11/10 15:23
Tetrachloroethene ug/L ND 0.50 04/11/10 15:23
Toluene ug/L ND 0.50 04/11/10 15:23
trans-1,2-Dichloroethene ug/L ND 0.50 04/11/10 15:23
trans-1,3-Dichloropropene ug/L ND 0.50 04/11/10 15:23
Trichloroethene ug/L ND 0.50 04/11/10 15:23
Trichlorofluoromethane ug/L ND 1.0 04/11/10 15:23
Vinyl chloride ug/L ND 1.0 04/11/10 15:23
1,2-Dichloroethane-d4 (S) % 89 70-130 04/11/10 15:23
4-Bromofluorobenzene (S) % 114 70-130 04/11/10 15:23
Dibromofluoromethane (S) % 90 70-130 04/11/10 15:23
Toluene-dB (S) % 97 70-130 04/11/10 15:23
LA.BORATORY CONTROL SAMPLE: 427329
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
1, 1, 1,2-Tetrachloroethane ug/L 50 55.0 110 60-140
1, 1, 1-Trichloroethane ug/L 50 44.3 89 60-140
1, 1,2,2-Tetrachloroethane ug/L 50 47.7 95 60-140
1, 1,2-Trichloroethane ug/L 50 47.5 95 60-140
1, 1-Dichloroethane ug/L 50 41.2 82 60-140
1, 1-Dichloroethene ug/L 50 38.7 77 60-140
1, 1-Dichloropropene ug/L 50 40.1 80 60-140
1,2,3-Trichlorobenzene ug/L 50 49.6 99 60-140
1,2,3-Trichloropropane ug/L 50 53.2 106 60-140
1,2,4-Trichlorobenzene ug/L 50 51.5 103 60-140
1,2,4-Trimethylbenzene ug/L 50 47.9 96 60-140
1,2-Dibromo-3-chloropropane ug/L 50 45.9 92 60-140
1,2-Dibromoethane (EDB) ug/L 50 52.5 105 60-140
1,2-Dichlorobenzene ug/L 50 49.4 99 60-140
1,2-Dichloroethane ug/L 50 42.9 86 60-140
1,2-Dichloropropane ug/L 50 42.9 86 60-140
1,3,5-Trimethylbenzene ug/L 50 48.0 96 60-140
1,3-Dichlorobenzene ug/L 50 49.3 99 60-140
1,3-Dichloropropane ug/L 50 48.6 97 60-140
1,4-Dichlorobenzene ug/L 50 48.2 96 60-140
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS Page 17 of21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
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Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
LABORATORY CONTROL SAMPLE: 427329
Parameter Units
2,2-Dichloropropane ug/L
2-Chlorotoluene ug/L
4-Chlorotoluene ug/L
Benzene ug/L
Bromobenzene ug/L
Bromochloromethane ug/L
Bromodichloromethane ug/L
Bromoform ug/L
Bromomethane ug/L
Carbon tetrachloride ug/L
Chlorobenzene ug/L
Chloroethane ug/L
Chloroform ug/L
Chloromethane ug/L
cis-1,2-Dichloroethene ug/L
cis-1,3-Dichloropropene ug/L
Dibromochloromethane ug/L
Dibromomethane ug/L
Dichlorodifluoromethane ug/L
Diisopropyl ether ug/L
Ethyl benzene ug/L
Hexachloro-1,3-butadiene ug/L
lsopropylbenzene (Cumene) ug/L
m&p-Xylene ug/L
Methyl-tert-butyl ether ug/L
Methylene Chloride ug/L
n-Butylbenzene ug/L
n-Propylbenzene ug/L
Naphthalene ug/L
a-Xylene ug/L
sec-Butyl benzene ug/L
Styrene ug/L
tert-Butylbenzene ug/L
Tetrachloroethene ug/L
Toluene ug/L
trans-1,2-Dichloroethene ug/L
trans-1,3-Dichloropropene ug/L
Trichloroethene ug/L
T richlorofluoromethane ug/L
Vinyl chloride ug/L
1,2-Dichloroethane-d4 (S) %
4-Bromofluorobenzene (S) %
Dibromofluoromethane (S) %
Toluene-dB (S) %
Date: 04/21/2010 02:59 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike LCS LCS %Rec
Cone. Result %Rec Limits
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers --
50 33.0 66 60-140 cc
50 45.8 92
50 45.5 91
50 43.9 88
50 43.2 86
50 43.5 87
50 47.6 95
50 57.0 114
50 44.2 88
50 46.7 93
50 51.2 102
50 46.3 93
50 41.4 83
50 38.8 78
50 40.2 80
50 42.0 84
50 53.7 107
50 53.7 107
50 38.4 77
50 39.1 78
50 49.8 100
50 50.8 102
50 52.6 105
100 102 102
50 51.1 102
50 38.9 78
50 44.2 88
50 45.4 91
50 47.4 95
50 50.5 101
50 47.0 94
50 52.8 106
50 48.7 97
50 54.0 108
50 46.1 92
50 39.5 79
50 42.8 86
50 50.9 102
50 42.5 85
50 38.6 77
87
115
91
98
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
70-130
70-130
70-130
70-130
Page 18 of21
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: ROSO CHEVRON 04/09
Pace Project No.: 9267119
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 427330 427331
MS MSD
9267006008 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPO Qua! --
1, 1, 1,2-Tetrachloroethane ug/L ND 20 20 22.5 24.9 113 124 60-140 10
1, 1, 1-Trichloroethane ug/L ND 20 20 20.9 21.7 105 108 60-140 3
1, 1,2,2-Tetrachloroethane ug/L ND 20 20 17.8 19.7 89 99 60-140 10
1, 1,2-Trichloroethane ug/L ND 20 20 19.9 21.4 100 107 60-140 7
1, 1-Dichloroethane ug/L ND 20 20 18.6 19.2 93 96 60-140 3
1, 1-Dichloroethene ug/L ND 20 20 18.6 18.9 93 95 60-140 2
1, 1-Dichloropropene ug/L ND 20 20 17.8 18.1 89 91 60-140 2
1,2,3-Trichlorobenzene ug/L ND 20 20 19.9 24.0 100 120 60-140 19
1,2,3-Trichloropropane ug/L ND 20 20 20.7 22.7 103 114 60-140 10
1,2,4-Trichlorobenzene ug/L ND 20 20 20.2 24.3 101 122 60-140 18
1,2,4-Trimethylbenzene ug/L ND 20 20 19.9 21.3 98 105 60-140 7
1,2-Dibromo-3-chloropropane ug/L ND 20 20 17.1 19.9 85 100 60-140 15
1,2-Dibromoethane (EDB) ug/L ND 20 20 21.0 22.7 105 114 60-140 8
1,2-Dichlorobenzene ug/L ND 20 20 20.7 22.6 103 113 60-140 9
1,2-Dichloroethane ug/L ND 20 20 18.5 19.3 93 97 60-140 4
1,2-Dichloropropane ug/L ND 20 20 18.1 19.4 90 97 60-140 7
1,3,5-Trimethylbenzene ug/L ND 20 20 20.5 22.2 103 111 60-140 8
1 ,3-Dichlorobenzene ug/L ND 20 20 20.5 22.6 103 113 60-140 10
1,3-Dichloropropane ug/L ND 20 20 19.8 21.3 99 106 60-140 7
1,4-Dichlorobenzene ug/L ND 20 20 20.4 21.8 102 109 60-140 7
2,2-Dichloropropane ug/L ND 20 20 17.6 17.2 88 86 60-140 2
2-Chlorotoluene ug/L ND 20 20 19.5 21.0 98 105 60-140 7
4-Chlorotoluene ug/L ND 20 20 20.2 21.4 101 107 60-140 5
Benzene ug/L ND 20 20 19.4 20.0 97 100 60-140 3
Bromobenzene ug/L ND 20 20 18.6 19.8 93 99 60-140 6
Bromochloromethane ug/L ND 20 20 21.5 22.0 107 110 60-140 2
Bromodichloromethane ug/L ND 20 20 20.0 21.2 100 106 60-140 6
Bromoform ug/L ND 20 20 22.2 24.4 111 122 60-140 10
Bromomethane ug/L ND 20 20 19.8 20.6 99 103 60-140 4
Carbon tetrachloride ug/L ND 20 20 26.9 27.0 135 135 60-140 0
Chlorobenzene ug/L ND 20 20 22.5 23.8 113 119 60-140 6
Chloroethane ug/L ND 20 20 22.0 22.2 110 111 60-140
Chloroform ug/L ND 20 20 17.9 18.9 89 94 60-140 5
Chloromethane ug/L ND 20 20 13.2 13.5 66 68 60-140 2
cis-1,2-Dichloroethene ug/L ND 20 20 17.8 18.7 89 94 60-140 5
cis-1,3-Dichloropropene ug/L ND 20 20 16.6 17.9 83 90 60-140 8
Dibromochloromethane ug/L ND 20 20 21.8 23.3 109 116 60-140 6
Dibromomethane ug/L ND 20 20 23.7 25.2 118 126 60-140 6
Dichlorodifluoromethane ug/L ND 20 20 18.7 18.8 93 94 60-140 1
Diisopropyl ether ug/L ND 20 20 16.1 17.6 80 88 60-140 9
Ethyl benzene ug/L ND 20 20 21.8 22.9 109 114 60-140 5
Hexachloro-1,3-butadiene ug/L ND 20 20 21.6 23.4 108 117 60-140 8
lsopropylbenzene (Cumene) ug/L ND 20 20 23.7 25.7 118 128 60-140 8
m&p-Xylene ug/L ND 40 40 46.3 48.6 115 121 60-140 5
Methyl-tert-butyl ether ug/L ND 20 20 21.2 23.1 104 113 60-140 9
Methylene Chloride ug/L ND 20 20 15.4 16.3 77 82 60-140 6
n-Butylbenzene ug/L ND 20 20 18.7 21.1 93 106 60-140 12
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS Page19of21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
i~l
Pace Analytical Services, Inc.
2225 Riverside Dr.
www.pacelabs.com Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 427330 427331
MS MSD
9267006008 Spike Spike MS MSD MS
Parameter Units
n-Propylbenzene ug/L
Naphthalene ug/L
a-Xylene ug/L
sec-Butyl benzene ug/L
Styrene ug/L
tert-Butylbenzene ug/L
Tetrachloroethene ug/L
Toluene ug/L
trans-1,2-Dichloroethene ug/L
trans-1,3-Dichloropropene ug/L
Trichloroethene ug/L
Trichlorofluoromethane ug/L
Vinyl chloride ug/L
1,2-Dichloroethane-d4 (S) %
4-Bromofluorobenzene (S) %
Dibromofluoromethane (S) %
Toluene-dB (S) %
Date: 04/21/2010 02:59 PM
Result Cone. Cone. Result Result %Rec
ND 20 20 20.5 22.1
ND 20 20 19.2 22.1
ND 20 20 22.3 23.6
ND 20 20 20.5 23.3
ND 20 20 21.1 21.9
ND 20 20 21.8 24.2
ND 20 20 24.4 25.3
ND 20 20 20.1 20.8
ND 20 20 18.0 18.1
ND 20 20 16.8 18.0
ND 20 20 22.8 23.3
ND 20 20 21.6 21.1
ND 20 20 17.2 17.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
'I) \ll ACCo-90
~ ~ i 1
102
87
111
103
106
109
122
101
90
84
114
108
86
89
116
91
98
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MSD %Rec
%Rec Limits RPO Qual
110 60-140 7
101 60-140 14
117 60-140 6
117 60-140 13
110 60-140 4
121 60-140 10
126 60-140 3
104 60-140 3
91 60-140
90 60-140 7
116 60-140 2
106 60-140 2
86 60-140 0
89 70-130
116 70-130
92 70-130
98 70-130
Page 20 of21
Wl'IW.pace/abs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: ROBO CHEVRON 04/09
Pace Project No.: 9267119
DEFINITIONS
OF -Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND -Not Detected at or above adjusted reporting limit.
J -Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S -Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPO values.
LCS(D) -Laboratory Control Sample (Duplicate)
MS(D) -Matrix Spike (Duplicate)
DUP -Sample Duplicate
RPO -Relative Percent Difference
NC -Not Calculable.
Pace Analytical is NE LAP accredited. Contact your Pace PM for the current list of accredited analytes.
U -Indicates the compound was analyzed for, but not detected.
ANALYTE QUALIFIERS
CC The continuing calibration for this compound is outside of method control limits. The result is estimated.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPO value was outside control limits.
SS Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).
Date: 04/21/2010 02:59 PM REPORT OF LABORATORY ANALYSIS
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Matrix Codes i ii:' MMBIK l ~Qtllii :;; COLLECTED J3 0 Drinking Water DW a'! u Water WT ~ II u Waste Water WW COMPOSITE COMPOSITE
Product p ~ ! START ENO/GRAB
SolVSolld SL > l C)
OIi OL ~ Wipe WP UJ Air AR Q w Tissue TS 8 ~ Other OT >< w ii: ..J D.. i ~ DATE C/l TIME DATE
· Preservatives
W"( l.t ,,,.,. -
t r/llJ la!lO
/If. :,i/iMo ltt1-"
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6
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u . ~
1-1.;.." 2~·: 1-------------------11---+-+---➔~-..,,....--+~v.,c.---+---+--+--➔--+--+-+-+--+--11--+--1~)'----t---1-1---t---t---11--1---+---t----11--1---1-------------1
;~~~~{~~.:.~~m.~:~ijp'.~)g~~t/:f~~ft:t~i1iZi:BWf :t~f~1!.~~t!t 1:i:i;~JftilitI~;ll~ Z'f1;l;~;_iff \ ?::· .. , \,:,\:.. ~:c·
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y
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Chain of Custody Present:
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Short Hold Time Anal sis (<72hr :
Rush Turn Around Time Re uested:
Sufficient Volume:
Correct Containers Used:
-Pace Containers Used:
Containers Intact:
Filtered volume received for Dissolved tests
Comments:
□NIA 1.
□NIA 2.
□NJA 8.
□NJA 9.
Date and lnltla
Sample Labels match COG:
-Includes date/time/ID/Analysis
f1....cc TIA,,o ~,,.pre f,c.rv c. A-h ,,_.,
Matrix: l.f...,s ~,,-h ~o J~f.eJs. · ~f ~
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation.
1-DRO (water)
Samples checked for dechlorination:
Headspace in VOA Vials ( >6mm):
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot# (if purchased :
Client Notification/ Resolution:
~ □No □NIA 13.
~-□No □NJA ?....
~□No Initial when completed
□Yes □No
Person Contacted: Date/Time: --------------
Comments/ Resolution:
Field Data Required? y / N
------------------------------------------
Project Manager Review: '-fP Date: 1 / fB [jn
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers)
Pace F-ASV-CS-03-Rev00
APPENDIX B
Risk Classification and Land Use Form
Limited Site Assessment Risk Classification and Land Use Form
Part I -Groundwater/Surface WaterNapor Impacts
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
High Risk
Has the release contaminated any water supply well including any well used for non-drinking purposes?
Is a water supply well used for drinking water located within 550 feet of the source area of the release?
Is a water supply well not used for drinking water ( e.g., irrigation, washing cars, industrial cooling water,
filling swimming pools) located within 250 feet of the source area of the release?
Does groundwater within 500 feet of the source area of the release have the potential for future use (there is no
other source of water supply other than the groundwater)?
Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined space
or pose any other serious threat to public health, public safety or the environment?
If yes, describe. Not Applicable.
Are there any other factors that would cause the release to pose an imminent danger to public health, public
safety, or the environment?
If yes, describe. Not Applicable.
Intermediate Risk
Is a surface water body located within 500 feet of the source area of the release?
IfYES, does the maximum groundwater contaminant concentration exceed the surface water quality standards
and criteria found in 15A NCAC 2B .0200 by a factor of 10? Unknown. I, 19 Vj { l_
Is the source area of the release located within a approved or planned wellhead protection area as defined in 42
USC 300h-7(e)?
If yes, describe. Not Applicable
Is the release located in the Coastal Plain physiographic region as designated on a map entitled "Geology of
North Carolina" published by the Department in 1985?
If YES, is the source area of the release located in an area in which there is recharge to an unconfined or semi-
confined deeper aquifer that is being used or may be used as a source of drinking water? Not Applicable.
IfYES, describe. Not Applicable
Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels
established by the Department?
NO
NO
NO
NO
NO
NO
NO
NO
NO
Part II -Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1.
2.
3.
4.
5.
6
Does the property contain one or more primary or secondary residences (permanent or temporary)?
Describe. The property consists of a gas station and convenience store.
Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing
home, or other place of public assembly?
Describe. Not Applicable.
Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial (e.g.,
manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise,
an inactive commercial or industrial enterprise, or is the land undeveloped?
Describe A bulk dispenser storage shed is located on the property.
Do children visit the property?
Explain. Occasionally.
Is access to the property reliably restricted consistent with its use ( e.g., by fences, security personnel or both)?
Explain. No restrictions are warranted.
Do pavement, buildings, or other structures cap the contaminated soil?
Describe. Access to the area of contaminated soil is restricted by the concrete parking surface.
If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will remain
capped in the foreseeable future? Not Applicable.
7. What is the zoning status of the property? The property is zoned commercial, C-1.
8. Is the use of the property likely to change in the next 20 years?
Explain. Although possible, change is not likely.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property containing
source area of the release):
1.
2.
3.
4.
What is the distance from the source area of the release to the nearest primary or secondary residence
(permanent or temporary)? 100 feet
What is the distance from the source area of the release to the nearest school, daycare center, hospital,
playground, park, recreation area, church, nursing home or other place of public assembly? The Swannanoa
Valley Christian Ministries, Inc., is approximately 450 feet north of the site.
What is the zoning status of properties in the surrounding area? The area is zoned commercial with some
residential.
Briefly characterize the use and activities of the land in the surrounding area. The area surrounding the ROBO
Chevron Station is predominantly commercial, with churches, banks, restaurants, condominiums, and a
Buncombe County Board of Education property located 850 feet northeast of the site.
NO
NO
YES
YES
YES
YES
NO
APPENDIXC
Driller's Log
NON RESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Naturnl Resources-Division of Water Quality
WELL CONTRACTOR CERTIFICATION# 3172
1. WELL CONTRACTOR:
Everard Baker Uordan
Well Contractor (lndi~ldual) Name
Jordan Envirorimental, LLC
Well Contractor Company Name
68 Little Horse !Road
Street Address I
Waynesville I
City or Town I
l (828 > 734-26~2
Area code Phone number
2. WELL INFORMATidN:
NC 28786
Stale Zip Code
WELL CONSTRUCTIO;N PERMIT# __________ _
OTHER ASSOCIATEDIPERMIT#(if applicable), _______ _
SITE WELL ID #(if appli~ble),...:M..:..:....:W-=----=-1 _______ _
3. WELL USE (Check Gne Box) Monitoring rJ/ Municipal/Public □
I lndustrial/Commerci~I □ Agricultural □ Recovery□ Injection □
Irrigation□ Other ol (list use) __________ _
DATE DRILLED 4/9/10 _,_.-='-..,_.. ____ _
4. WELL LOCATION: i
204 East StatelStreet. 28711
(Street Name, Numbers, Community. Subdivision, Lot No., Parcel, Zip Code) i
c1TY: Black Mountain couNTY Buncombe
TOPOGRAPHIC/ LAND SETTING: (check appropriate box) □Slope □Valley ~Flat □Ridge □Other. ______ _
LATITUDE 35 'i "DMSOR 35.619383 DD
I
LONGITUDE 81__0i ·---"□MSOR 82.318211 DD
Latitude/longitude soutce: ~PS oropographic map
(location of well must pe shown on a USGS topo map andattached to
this form if not using $PS)
5. FACILITY (Name of the business where the well ls located.)
l
Roho Chevron Station 0-004164
Facility Name I Factlity ID# (if applicable)
204 East State !Street
street Address · I
Black Mounta10 NC
State
28711
City orTown ! Zip Code
Chio Gould 1
Contact Name i
203 West Kina :Street
Mailing Address i
East flat Rock NC 28762.
City or Town j State Zip Code
I
( 828.ij 697-0501
Area code Phone number
------------
: d. TOP OF CASING IS _____ FT. Above Land Surface•
: ~rop of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
: e. YIELD (gpm): ____ METHOD OF TEST ____ _
: f. DISINFECTION: Type Amount ____ _
; g. WATER ZONES (depth}:
: Top 11.0 Bottom 24 0 Top'---___ Bottom. ___ _
: Top ____ Bottom ___ _ Top Bottom. ___ _
: Top Bottom. ___ _ Top Bottom. ___ _
; 7. CASING: Depth
: Top 0.0 Bottom 9.0
: Top ___ Bottom
: Top ___ Bottom
: 8. GROUT: Depth
: Top 0.0 Bottom 6.0
: Top Bottom
: Top Bottom ___
: 9. SCREEN: Depth
Diameter
Ft. 2
FL
Ft.
Material
Ft. Portland
FL
Ft.
Thickness/
Weight Material
Sch40 PVC
Method
Tremmie
Diameter Slot Size Material
: Top 9.0 Bottom 24.0 Ft._2 __ in. -1.Q_ in. _P,_V~C~--
: Top, ___ Bottom ___ Ft. __ in. in. ____ _
: Top Bottom ___ Ft __ in. in. ____ _
: 10. SAND/GRAVEL PACK:
: Depth Size Material
: Top 7.0 Bottom 24.0 Ft._2 ___ ---'S""a""n,..,,d,.__ ____ _
: Top ___ Bottom ___ Ft. __ _
: Top Bottom Ft. ____________ _
: 11. DRILLING LOG
• Top Bottom
0.0
5.0
10.0
I 5.0
/ 10.0
/ 24.0 __ _,/ ___ _
------'----/ ___ _
---/ ___ _ __ ....;/ ___ _ __ ...,/ ___ _ ___ / ___ _
----'----
: 12. REMARKS:
Formation Description
Dark Brn Silty Sand
Tan SHty Sand
Grey Silty Sand
I : I DO HEREBY CERTJfiY THAT T CTEO IN ACCORDANCE WITH 6. WELL DETAILS: I . (I~. !tCONS _ THAT A COPY OF THIS
; ; R~RDHAS J ,PTHE t:/'LOWNER.
a. TOTAL DEPTH: 24.0 : A, . ./ · . 4/14/1 O
b. DOES WELL RE,LACE EXISTING WELL? YES D NO rJ/ ! SIGNATURE O _ . 'WELL CONTRA<5'fc5R DATE
c. WATER Ll:VEL Below Top of Casing: 11 0 FT. : Everard Baker Jordan
(Use "-t-J'f Above Top of Casing) : PRINTED NAME OF PERSON CONSTRUCTING THE WELL
• Form GW-·lb
Submit within 30 ays of completion to: Division of Water Quality • lnfonnation Proce~s1ns, Rev. 2109
1617 Mail Service cJnter, Raleigh, NC 27699-161, Phone: [phone] i .
~ NON RESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources-Division of Water Quality
WELL CONTRACTOR CERTIFICATION# 3172
1. WELL CONTRACT R:
Everard Baker Uordan
Well Contractor (Individual) Name
Jordan Environ1mental, LLC
Well Contractor Company Name
68 Little Horse !Road
Street Address I
Waynesville
City or Town I
< 828 ) 734-2612
Area code Phone nurriber
2. WELL INFORMATIOIN:
NC 28786
State Zip Code
WELL CONSTRUCTION PERMIT# __________ _
I OTHER ASSOCIATED PERMIT#(if applicable) _______ _
SITE WELL ID #(if applidable),_M~W--2~--------
1
3. WELL USE (Check One Box) Monitoring 1¥ Municipal/Public □
lndustrial/CommerciJI □ Agricultural □ Recovery □ Injection □ Irrigation□ Other □ I (list use) __________ _
DATE DRtLLED_4:.:../9=Yf-'1,_.Q....._ ___ _
4. WELL LOCATION: I
204 East State Street. 28711
(Street Name. Numbers, community, SubdiVision, Lot No., Parwl, Zip Code)
c1TY: Black MouJtain couNTY Buncombe
TOPOGRAPHIC/ LAND SETTING: (check appropriate box)
□Slope □Valley !ilflat □Ridge □Other, ______ _
LATITUDE 35 ·I . ___ " OMS OR 35.619383 DD
LONGITLJDE~0 1 ___ "DMSOR 82.318211 DD
Latitudenongitude soufce: l;iJ3PS Dropographic map
(location of well must ~e shown on a USGS topo map andattached to
this form if not using GPSJ
5. FACILITY (Name of t~e business where the well is located.)
Robo ChevroJ Station 0-004164 Facility Name I Facility ID# (if applicable)
204 East State /Street
Street Address I
Black Mountain NC 28711
City or Town \1
Chin Gould
State Zip Code
contact Name /
203 West Kina f treet Mailing Address
East Flat Rack NC 28762
City or Town / State Zip Code
< 828 a 697-0501 Area code Phone number
6. WELL DETAILS: I
a. TOTAL DEPTH:_.1,._4_... • .,..Q ___ _
b. DOES WELL REPtACE EXISTING WELL? YES O NO a/
c. WATER LEVEL Below Top of Casing: 11 0 FT.
(Use"+" i' Above Top of Casing)
------------
: d. TOP OF CASING IS_,--___ FT. Above Land Surface•
: "Top of casing terminated aUor below land surface may require
: a variance in accordance with 15A NCAC 2C .0118.
: e. YIELD (gpm): ____ METHOD OF TEST ____ _
: f. DISINFECTION: Type'-------Amount ____ _
: g. WATER ZONES (depth}:
: Top 11.0 Bottom 24.0 Top ____ Bottom. ___ _
: Top ___ Bottom~---Top ____ Bottom. ___ _
: Top Bottom ____ _ Top Bottom. ___ _
Thickness/
: 7. CASING: Depth Diameter Weight Material
: Top 0.0 Bottom 9.0 Ft. 2 Sch40 PVC
: Top Bottom Ft.
: Top Bottom Ft.
: 8. GROUT: Depth Material
: Top 0.0 Bottom_§,_Q_ Ft. Portland
: Top ___ Bottom ___ Ft.. ____ _
: Top ___ Bottom ___ Ft. ____ _
Method
Tremmie
: 9. SCREEN: Depth Diameter Slot Size Material
: Top 9.0 Bottom 24.0 Ft._2 __ in. _jQ_ in. _P~V~C~--
: Top ___ Bottom ___ Ft. __ in. in. ____ _
: Top ___ Bottom~ __ Ft. __ in. in. ____ _
: 10. SAND/GRAVEL PACK:
Depth Size Material
: Top 7.0 Bottom 24.0 Ft.~2~--_S=a~od~------
: Top ___ Bottom ___ Ft. ___________ _
: Top ___ B.ottom'---__ Ft. ___________ _
: 11. DRILLING LOG
: Top Bottom
o.o , ...... s=_o __ _
s.o '~2,,_,4=.o~----''--------:'----__ __,/ ___ _
--~'------~'------~'-------''----__ ....,, ___ _
----''----
: 12. REMARKS:
Formation Description
Dark Bm Silty Sand
Tan Silty Sand
: / ,,,
: PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Submit within 30 d ys of completion to: DivisiQn of Water Quality .. Information Processing,
1617 Mall Service Ce ter, Raleigh~ NC 27699-161, Phone: [phone]
FormGW-1b
Rev. 2/09