AS-3327_28491_CA_MRP_20190506_ALL

7606 Whitehall Executive Center Drive, Suite 800
Charlotte, NC 28273
Tel: [phone]
Fax: [phone]
www.atcgroupservices.com
N.C. Engineering License No. C-1598

1

May 6, 2019

Mr. Dan Murphy
North Carolina Department of Environmental Quality
Asheville Regional Office
Division of Waste Management - UST Section
2090 US Highway 70
Swannanoa, North Carolina 28778

Re: Groundwater Sampling Letter Report
Yogi Foods
4018 Highway 321A
Hudson, Caldwell County
Facility ID No. 0-0 7809
NCDEQ Incident No. 28491

Dear Mr. Murphy:

ATC Associates of North Carolina, P.C. (ATC), on behalf of Cary Oil Company, is submitting a summary of
groundwater sampling activities conducted on April 18, 2019. The groundwater sampling event was
performed in accordance with Task Authorization Number 10, approved April 3, 2019. The activities
included the sampling of two groundwater monitoring wells (MW-1 and MW-5) at the site. A site location
map is provided as Figure 1 and a site map is provided as Figure 2.

The groundwater analytical results, summarized in Table B-4, indicated the presence of volatile organic
hydrocarbons in the sampled monitoring well on-site. The results indicate that groundwater from well MW-1
well contained EDB concentrations above the North Carolina Gross Contamination Levels (GCL). Historical
groundwater data is provided in Table B-4A. The laboratory analytical report is provided in Appendix A.

ATC recommends an additional sparge-enhanced AFVR event at the site. If you have any questions or
comments, please contact us at [phone].

Sincerely,

ATC Associates of North Carolina, P.C.

Michael D. Shaw, P.G.
NC Licensed Geologist #1338

cc: Cary Oil Company

Attachments:
Yogi Foods – Groundwater Sampling Letter Report May 6, 2019
NCDEQ Incident No. 28491 ATC Project No. CARYOGI006

2

TABLES
Table B-4: Summary of Groundwater Sampling Results
Revision Date: 5/6/19 Incident Number and Name: 28491/Yogi Foods Facility ID #: 0-007809
504.1
Well ID Date Collected Sample ID
Incident
Phase
MW-1 4/18/2019 MW-1 Monitoring 5,410 15,900 649 8,590 < 63 < 63 < 63 253 396 74.1 J < 100 152 J 1,890 540 296
MW-5 4/18/2019 MW-5 Monitoring 277 901 81 1,110 < 3.1 8.2 J 5.8 J 11.1 J 89.6 18.2 28.7 J 47.6 484 141 11.8
1 600 600 500 20 70 70 0.4 6 70 5 70 400 400 0.02
5,000 260,000 84,500 85,500 20,000 6,900 8,500 400 6,000 25,000 5,000 30,000 28,500 25,000 50
Results in ug/L
Concentrations in bold exceeded the 2L Standard
Concentrations in bold and italics exceeded the GCL
J = Estimated Value
NE = Not Established
ED
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GCL = gross contamination level
Contaminant of Concern
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Table B-4A: Summary of Historical Groundwater Sampling Results
Revision Date: 5/6/19 Incident Number and Name: 28491/Yogi Foods Facility ID #: 0-007809
625 504.1 3030C
Well ID Date Collected Sample ID
Incident
Phase
MW-1 8/11/2006 MW-1 Phase I LSA 6,300 11,000 580 4,400 <100 NR NR NR <20 NR <100 <100 NR NR NR NR NR <20 <40 <20 NR NR 38,000 5,300 12,000 NR NR NR NR NR NR 555
MW-1 8/6/2014 MW-1 Phase II LSA 13,500 26,900 1,120 6,910 <100 <100 <100 <100 950 <100 180 454 <100 <400 167 1,160 356 <100 <1,000 <100 <200 353 87,300 <25,000 <25,000 <100 <100 533 ND 533 701 228
MW-1 3/24/2016 MW-1 Pre-CAP 13,000 34,500 1,430 9,210 <125 <125 <125 <125 634 <125 161 542 109 J <500 267 1,710 451 <125 <1,250 <125 <250 NR NR NR NR NR NR NR NR NR 902 NR
MW-1 11/2/2016 MW-1 Pre-CAP 5,820 17,800 986 6,090 <62.5 <62.5 <62.5 <62.5 168 <62.5 37.0 J 357 68.8 228 J 199 1,300 340 <62.5 <625 <62.5 <125 NR NR NR NR NR NR NR NR NR 162 NR
MW-1 4/20/2017 MW-1 Pre-CAP 627 1,170 105 2,260 <5.0 <5.0 <5.0 <5.0 29.7 <5.0 5.1 117 42.7 <20.0 <5.0 769 <5.0 <5.0 <50.0 <5.0 <10.0 NR NR NR NR NR NR NR NR NR 30.9 NR
MW-1 11/16/2017 MW-1 Monitoring 6,560 12,200 536 6,780 <50.0 28.9 J <50.0 <50.0 246 <50.0 77.2 384 55.6 <200 <50.0 1,300 <50.0 <50.0 <500 <50.0 <100 NR NR NR NR NR NR NR NR NR 230 NR
MW-1 4/13/2018 MW-1 Monitoring 3,920 13,000 671 5,000 <50 <50 <50 <50 116 <50 <50 388 45.8 J <200 <50 1,020 <50 <50 <50 <50 <100 NR NR NR NR NR NR NR NR NR 262 NR
MW-1 4/18/2019 MW-1 Monitoring 5,410 15,900 649 8,590 < 63 < 63 < 63 < 63 253 < 63 < 63 396 74.1 J < 500 152 J 1,890 540 < 63 < 63 < 63 < 100 NR NR NR NR NR NR NR NR NR 296 NR
MW-2 8/6/2014 MW-2 Phase II LSA 279 1,720 944 4,030 19.5 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 724 70.6 <40.0 120 814 201 <10.0 <100 <10.0 <20.0 404 5,370 <5,000 19,600 <100 <100 710 19,600 710 0.075 1,900
MW-2 11/16/2017 MW-2 Monitoring 6.5 0.33 J 17.0 0.72 J <0.50 <0.50 4.5 0.97 <0.50 <0.50 <0.50 22.4 16.6 <2.0 12.8 <0.50 <0.50 <0.50 <5.0 0.90 <1.0 NR NR NR NR NR NR NR NR NR <0.019 NR
MW-3 8/6/2014 MW-3 Phase II LSA <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <0.50 <0.50 0.66 5.0 6.5 <1.0 <6.2 <50.0 <50.0 <50.0 <100 <100 <100 ND ND <0.022 617
MW-3 11/16/2017 MW-3 Monitoring <0.50 <0.50 <0.50 <1.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <5.0 <0.50 <1.0 NR NR NR NR NR NR NR NR NR <0.019 NR
MW-4 8/6/2014 MW-4 Phase II LSA 36.4 35.1 651 1,101 <5.0 <5.0 28.0 <5.0 74.8 <5.0 11.9 584 161 <20.0 420 1,440 654 <5.0 <50.0 <5.0 <10.0 342 9,470 4,720 16,200 197 <100 744 16,397 5,464 0.054 1,680
MW-4 11/16/2017 MW-4 Monitoring <0.50 0.65 11.2 <1.50 <0.50 43.8 36.6 <0.50 <0.50 0.83 <0.50 19.3 67.8 <2.0 157 <0.50 68.9 <0.50 <5.0 0.65 0.54 J NR NR NR NR NR NR NR NR NR <0.019 NR
MW-5 11/2/2016 MW-5 Pre-CAP 1,830 5,420 399 4,190 <25.0 <25.0 <25.0 <25.0 50.2 <25.0 <25.0 238 55.8 135 162 1,140 290 <25.0 <250 <25.0 <50.0 NR NR NR NR NR NR NR NR NR 29.1 NR
MW-5 4/20/2017 MW-5 Pre-CAP 550 1,390 125 1,857 <5.0 29.5 <5.0 <5.0 25.5 <5.0 3.8 J 87.5 40.8 <20.0 <5.0 745 <5.0 <5.0 <50.0 <5.0 <10.0 NR NR NR NR NR NR NR NR NR 29.1 NR
MW-5 11/16/2017 MW-5 Monitoring 1,090 3,360 243 2,423 <12.5 <12.5 <12.5 <12.5 <12.5 <12.5 <12.5 221 39.3 <50.0 <12.5 791 <12.5 <12.5 <125 <12.5 <25.0 NR NR NR NR NR NR NR NR NR 28.5 NR
MW-5 4/13/2018 MW-5 Monitoring 171 580 54.8 488 <2.0 <2.0 <2.0 <2.0 5.9 <2.0 <2.0 39.4 9.1 <8.0 28.6 189 49.5 <2.0 <20 <2.0 <4.0 NR NR NR NR NR NR NR NR NR 8.6 NR
MW-5 4/18/2019 MW-5 Monitoring 277 901 81.3 1,110 < 3.1 8.2 J 5.8 J 11 11.1 J < 3.1 < 3.1 89.6 18.2 28.7 J 47.6 484 141.0 < 3.1 < 3.1 < 3.1 < 5.0 NR NR NR NR NR NR NR NR NR 11.8 NR
1 600 600 500 20 70 70 70 0.4 6 70 6 70 5 70 400 400 NE 100 70 3 6 400 NE NE NE 10,000 NE 700 200 0.02 15
5,000 260,000 84,500 85,500 20,000 6,900 8,500 15,000 400 6,000 70,000 6,000 25,000 5,000 30,000 28,500 25,000 NE 100,000 70,000 3,000 6,000 NE NE NE NE NE NE NE NE 50 15,000
Results in ug/L
Concentrations in bold exceeded the 2L Standard
Concentrations in bold and italics exceeded the GCL
J = Estimated Value
NE = Not Established
NR = Not Requested
ND = Not Detected
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Table B-7: Monitoring Well Construction Information
Revision Date: 5/6/18 Incident Number and Name: 28491/Yogi Foods Facility ID #: 0-007809
Well ID
Date
Installed
Date GW
Measured
Casing
Diameter
(in.)
Casing
Depth (ft)
Screened
Interval
Total
Depth
TOC
Elevation*
Depth to
Water
from TOC
Free Product
Thickness**
Groundwater
Elevation*
Comments
dO (ppm)/pH
8/11/2006 26.82 0.00 67.68 Unknown
8/6/2014 22.27 0.00 72.23 7.44/4.94
3/24/2016 19.32 0.00 75.18 Not Recorded
11/2/2016 24.46 0.00 70.04 2.79/4.28
4/20/2017 26.40 0.00 68.10 Not Recorded
11/16/2017 23.30 0.00 71.20 2.93/4.73
4/13/2018 22.42 0.00 72.08 5.47/3.13
4/18/2019 17.94 0.00 76.56 Not Recorded
8/6/2014 23.05 0.00 71.55 2.38/5.44
11/16/2017 23.66 0.00 70.94 2.89/5.06
8/6/2014 22.40 0.00 72.38 1.75/6.07
11/16/2017 23.63 0.00 71.15 3.96/5.34
8/6/2014 15.55 0.00 71.47 1.70/5.98
11/16/2017 16.13 0.00 70.89 1.64/6.29
11/2/2016 24.19 0.00 70.06 2.71/3.92
4/20/2017 26.03 0.00 68.22 1.27/5.06
11/16/2017 22.91 0.00 71.34 1.71/4.40
4/13/2018 22.50 0.00 71.75 4.51/3.08
4/18/2019 17.63 0.00 76.62 0.53/4.51
** If free product is present in well, groundwater elevation is calculated by [Top of Casing Elevation-Depth to Water]+[free product thickness x 0.8581]
TOC = Top of Casing
* All measurements are feet Below Ground Surface (ft. BGS).
NS = Not Surveyed
MW-1 8/10/2006 1 13 13-28
30 94.78
MW-4 8/5/2014 2 15 15-30 30 87.02
MW-3 8/5/2014 2 15 15-30
MW-2 8/5/2014 2 15 15-30 30 94.60
MW-5 8/23/2016 4 15 15-30 30 94.25
28 94.50
Yogi Foods – Groundwater Sampling Letter Report May 6, 2019
NCDEQ Incident No. 28491 ATC Project No. CARYOGI006

3

FIGURES
CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
TITLE
DATE
SITE
DIR
T

R
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D
DISPENSER
CANOPY
STORE
STORE
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BASIN
GRASS
ASPHALT
CONCRETE
GRASS
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MW-2
MW-3
MW-4
KEROSENE
DISPENSER
KEROSENE
UST
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W
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TYPE II MONITORING WELL
E ELECTRIC LINE
W WATER LINE
TELEPHONE/TV LINE
S SEWER LINE
CATHODIC PROTECTION
PRODUCT PIPING
Yogi Foods – Groundwater Sampling Letter Report May 6, 2019
NCDEQ Incident No. 28491 ATC Project No. CARYOGI006

4

APPENDIX A

04/29/19
Technical Report for
ATC Group Services LLC
Yogi Foods; Hudson, NC
89.03451.104.3
SGS Job Number: FA63492
Sampling Date: 04/18/19
Report to:
ATC Group Services LLC.
7606 Whitehall Executive Center Dr. Suite 800
Charlotte, NC 28273
[e-mail]; [e-mail]
ATTN: Mike Shaw
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc.  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone]  fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 04/29/19
e-Hardcopy 2.0
Automated Report
32
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 32
FA63492
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA63492-1: MW-1 ........................................................................................................6
3.2: FA63492-2: MW-5 ........................................................................................................10
Section 4: Misc. Forms ............................................................................................................14
4.1: Chain of Custody ...........................................................................................................15
Section 5: MS Volatiles - QC Data Summaries .....................................................................17
5.1: Method Blank Summary ................................................................................................18
5.2: Blank Spike Summary ...................................................................................................21
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................24
Section 6: GC Volatiles - QC Data Summaries .....................................................................27
6.1: Method Blank Summary ................................................................................................28
6.2: Blank Spike Summary ...................................................................................................29
6.3: Matrix Spike Summary ..................................................................................................31
6.4: Duplicate Summary .......................................................................................................32
1
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3
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6
2 of 32
FA63492
SGS North America Inc.
Sample Summary
ATC Group Services LLC
Job No:FA63492
Yogi Foods; Hudson, NC
Project No: 89.03451.104.3
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA63492-1 04/18/19 11:30 EG 04/20/19 AQ Ground Water MW-1
FA63492-2 04/18/19 12:00 EG 04/20/19 AQ Ground Water MW-5
3 of 32
FA63492
1
Summary of Hits Page 1 of 1
Job Number:FA63492
Account:ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Collected:04/18/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA63492-1 MW-1
Benzene 5410 250 63 ug/l SM 6200B
o-Chlorotoluene 74.7 J 250 63 ug/l SM 6200B
1,2-Dibromoethane 386 250 63 ug/l SM 6200B
1,2-Dichloroethane 253 250 63 ug/l SM 6200B
Ethylbenzene 649 250 63 ug/l SM 6200B
Isopropylbenzene 74.1 J 250 63 ug/l SM 6200B
Naphthalene 396 250 63 ug/l SM 6200B
n-Propylbenzene 152 J 250 63 ug/l SM 6200B
Toluene 15900 250 63 ug/l SM 6200B
1,2,4-Trimethylbenzene 1890 250 63 ug/l SM 6200B
1,3,5-Trimethylbenzene 540 250 63 ug/l SM 6200B
m,p-Xylene 5290 500 63 ug/l SM 6200B
o-Xylene 3300 250 63 ug/l SM 6200B
Xylene (total)8590 750 130 ug/l SM 6200B
1,2-Dibromoethane a 296 19 9.4 ug/l EPA 504.1
FA63492-2 MW-5
Benzene 277 13 3.1 ug/l SM 6200B
n-Butylbenzene 8.2 J 13 3.1 ug/l SM 6200B
sec-Butylbenzene 5.8 J 13 3.1 ug/l SM 6200B
o-Chlorotoluene 15.6 13 3.1 ug/l SM 6200B
1,2-Dibromoethane 14.6 13 3.1 ug/l SM 6200B
1,2-Dichloroethane 11.1 J 13 3.1 ug/l SM 6200B
Ethylbenzene 81.3 13 3.1 ug/l SM 6200B
Isopropylbenzene 18.2 13 3.1 ug/l SM 6200B
p-Isopropyltoluene 3.8 J 13 3.1 ug/l SM 6200B
Methylene Chloride b 28.7 J 50 25 ug/l SM 6200B
Naphthalene 89.6 13 3.1 ug/l SM 6200B
n-Propylbenzene 47.6 13 3.1 ug/l SM 6200B
Toluene 901 13 3.1 ug/l SM 6200B
1,2,4-Trimethylbenzene 484 13 3.1 ug/l SM 6200B
1,3,5-Trimethylbenzene 141 13 3.1 ug/l SM 6200B
m,p-Xylene 624 25 3.1 ug/l SM 6200B
o-Xylene 482 13 3.1 ug/l SM 6200B
Xylene (total)1110 38 6.3 ug/l SM 6200B
1,2-Dibromoethane a 11.8 0.47 0.23 ug/l EPA 504.1
(a) All hits confirmed by dual column analysis.
(b) Suspected laboratory contaminant.
4 of 32
FA63492
2
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
5 of 32
FA63492
3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:FA63492-1 Date Sampled:04/18/19
Matrix:AQ - Ground Water Date Received:04/20/19
Method:SM 6200B Percent Solids:n/a
Project:Yogi Foods; Hudson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E098844.D 500 04/26/19 10:54 AB n/a n/a VE2113
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 5000 1000 ug/l
71-43-2 Benzene 5410 250 63 ug/l
108-86-1 Bromobenzene ND 250 63 ug/l
74-97-5 Bromochloromethane ND 250 63 ug/l
75-27-4 Bromodichloromethane ND 250 63 ug/l
75-25-2 Bromoform ND 250 63 ug/l
78-93-3 2-Butanone (MEK)ND 1300 630 ug/l
104-51-8 n-Butylbenzene ND 250 63 ug/l
135-98-8 sec-Butylbenzene ND 250 63 ug/l
98-06-6 tert-Butylbenzene ND 250 63 ug/l
56-23-5 Carbon Tetrachloride ND 250 63 ug/l
108-90-7 Chlorobenzene ND 250 63 ug/l
75-00-3 Chloroethane ND 250 100 ug/l
67-66-3 Chloroform ND 250 63 ug/l
95-49-8 o-Chlorotoluene 74.7 250 63 ug/l J
106-43-4 p-Chlorotoluene ND 250 63 ug/l
124-48-1 Dibromochloromethane ND 250 63 ug/l
106-93-4 1,2-Dibromoethane 386 250 63 ug/l
75-71-8 Dichlorodifluoromethane a ND 250 100 ug/l
95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l
541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l
106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l
75-34-3 1,1-Dichloroethane ND 250 63 ug/l
107-06-2 1,2-Dichloroethane 253 250 63 ug/l
75-35-4 1,1-Dichloroethylene ND 250 63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 250 63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 250 63 ug/l
78-87-5 1,2-Dichloropropane ND 250 63 ug/l
142-28-9 1,3-Dichloropropane ND 250 63 ug/l
594-20-7 2,2-Dichloropropane ND 250 63 ug/l
563-58-6 1,1-Dichloropropene ND 250 63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 250 63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:FA63492-1 Date Sampled:04/18/19
Matrix:AQ - Ground Water Date Received:04/20/19
Method:SM 6200B Percent Solids:n/a
Project:Yogi Foods; Hudson, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l
108-20-3 Di-Isopropyl Ether ND 250 63 ug/l
64-17-5 Ethyl Alcohol b ND 50000 33000 ug/l
100-41-4 Ethylbenzene 649 250 63 ug/l
591-78-6 2-Hexanone ND 2500 500 ug/l
98-82-8 Isopropylbenzene 74.1 250 63 ug/l J
99-87-6 p-Isopropyltoluene ND 250 63 ug/l
74-83-9 Methyl Bromide ND 250 100 ug/l
74-87-3 Methyl Chloride ND 250 100 ug/l
75-09-2 Methylene Chloride ND 1000 500 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 1300 630 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 250 63 ug/l
91-20-3 Naphthalene 396 250 63 ug/l
103-65-1 n-Propylbenzene 152 250 63 ug/l J
100-42-5 Styrene ND 250 63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 250 63 ug/l
127-18-4 Tetrachloroethylene ND 250 63 ug/l
108-88-3 Toluene 15900 250 63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 250 63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 250 63 ug/l
71-55-6 1,1,1-Trichloroethane ND 250 63 ug/l
79-00-5 1,1,2-Trichloroethane ND 250 63 ug/l
79-01-6 Trichloroethylene ND 250 63 ug/l
75-69-4 Trichlorofluoromethane ND 250 100 ug/l
96-18-4 1,2,3-Trichloropropane ND 250 63 ug/l
95-63-6 1,2,4-Trimethylbenzene 1890 250 63 ug/l
108-67-8 1,3,5-Trimethylbenzene 540 250 63 ug/l
108-05-4 Vinyl Acetate ND 2500 500 ug/l
75-01-4 Vinyl Chloride ND 250 63 ug/l
m,p-Xylene 5290 500 63 ug/l
95-47-6 o-Xylene 3300 250 63 ug/l
1330-20-7 Xylene (total)8590 750 130 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 94%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:FA63492-1 Date Sampled:04/18/19
Matrix:AQ - Ground Water Date Received:04/20/19
Method:SM 6200B Percent Solids:n/a
Project:Yogi Foods; Hudson, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated Initial Calibration outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FA63492-1 Date Sampled:04/18/19
Matrix:AQ - Ground Water Date Received:04/20/19
Method:EPA 504.1 EPA 504.1 Percent Solids:n/a
Project:Yogi Foods; Hudson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a DD106068.D 1000 04/29/19 12:48 NJ 04/24/19 12:45 OP74738 GDD3060
Run #2
Initial Volume Final Volume
Run #1 37.3 ml 2.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane 296 19 9.4 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 0% b 63-137%
(a) All hits confirmed by dual column analysis.
(b) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-5
Lab Sample ID:FA63492-2 Date Sampled:04/18/19
Matrix:AQ - Ground Water Date Received:04/20/19
Method:SM 6200B Percent Solids:n/a
Project:Yogi Foods; Hudson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E098846.D 25 04/26/19 11:44 AB n/a n/a VE2113
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 250 50 ug/l
71-43-2 Benzene 277 13 3.1 ug/l
108-86-1 Bromobenzene ND 13 3.1 ug/l
74-97-5 Bromochloromethane ND 13 3.1 ug/l
75-27-4 Bromodichloromethane ND 13 3.1 ug/l
75-25-2 Bromoform ND 13 3.1 ug/l
78-93-3 2-Butanone (MEK)ND 63 31 ug/l
104-51-8 n-Butylbenzene 8.2 13 3.1 ug/l J
135-98-8 sec-Butylbenzene 5.8 13 3.1 ug/l J
98-06-6 tert-Butylbenzene ND 13 3.1 ug/l
56-23-5 Carbon Tetrachloride ND 13 3.1 ug/l
108-90-7 Chlorobenzene ND 13 3.1 ug/l
75-00-3 Chloroethane ND 13 5.0 ug/l
67-66-3 Chloroform ND 13 3.1 ug/l
95-49-8 o-Chlorotoluene 15.6 13 3.1 ug/l
106-43-4 p-Chlorotoluene ND 13 3.1 ug/l
124-48-1 Dibromochloromethane ND 13 3.1 ug/l
106-93-4 1,2-Dibromoethane 14.6 13 3.1 ug/l
75-71-8 Dichlorodifluoromethane a ND 13 5.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 13 3.1 ug/l
541-73-1 1,3-Dichlorobenzene ND 13 3.1 ug/l
106-46-7 1,4-Dichlorobenzene ND 13 3.1 ug/l
75-34-3 1,1-Dichloroethane ND 13 3.1 ug/l
107-06-2 1,2-Dichloroethane 11.1 13 3.1 ug/l J
75-35-4 1,1-Dichloroethylene ND 13 3.1 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 3.1 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 3.1 ug/l
78-87-5 1,2-Dichloropropane ND 13 3.1 ug/l
142-28-9 1,3-Dichloropropane ND 13 3.1 ug/l
594-20-7 2,2-Dichloropropane ND 13 3.1 ug/l
563-58-6 1,1-Dichloropropene ND 13 3.1 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 13 3.1 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-5
Lab Sample ID:FA63492-2 Date Sampled:04/18/19
Matrix:AQ - Ground Water Date Received:04/20/19
Method:SM 6200B Percent Solids:n/a
Project:Yogi Foods; Hudson, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 13 3.1 ug/l
108-20-3 Di-Isopropyl Ether ND 13 3.1 ug/l
64-17-5 Ethyl Alcohol b ND 2500 1600 ug/l
100-41-4 Ethylbenzene 81.3 13 3.1 ug/l
591-78-6 2-Hexanone ND 130 25 ug/l
98-82-8 Isopropylbenzene 18.2 13 3.1 ug/l
99-87-6 p-Isopropyltoluene 3.8 13 3.1 ug/l J
74-83-9 Methyl Bromide ND 13 5.0 ug/l
74-87-3 Methyl Chloride ND 13 5.0 ug/l
75-09-2 Methylene Chloride c 28.7 50 25 ug/l J
108-10-1 4-Methyl-2-pentanone (MIBK)ND 63 31 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 13 3.1 ug/l
91-20-3 Naphthalene 89.6 13 3.1 ug/l
103-65-1 n-Propylbenzene 47.6 13 3.1 ug/l
100-42-5 Styrene ND 13 3.1 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.1 ug/l
127-18-4 Tetrachloroethylene ND 13 3.1 ug/l
108-88-3 Toluene 901 13 3.1 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 3.1 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 3.1 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 3.1 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 3.1 ug/l
79-01-6 Trichloroethylene ND 13 3.1 ug/l
75-69-4 Trichlorofluoromethane ND 13 5.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.1 ug/l
95-63-6 1,2,4-Trimethylbenzene 484 13 3.1 ug/l
108-67-8 1,3,5-Trimethylbenzene 141 13 3.1 ug/l
108-05-4 Vinyl Acetate ND 130 25 ug/l
75-01-4 Vinyl Chloride ND 13 3.1 ug/l
m,p-Xylene 624 25 3.1 ug/l
95-47-6 o-Xylene 482 13 3.1 ug/l
1330-20-7 Xylene (total)1110 38 6.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 94%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-5
Lab Sample ID:FA63492-2 Date Sampled:04/18/19
Matrix:AQ - Ground Water Date Received:04/20/19
Method:SM 6200B Percent Solids:n/a
Project:Yogi Foods; Hudson, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated Initial Calibration outside control limits.
(c) Suspected laboratory contaminant.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-5
Lab Sample ID:FA63492-2 Date Sampled:04/18/19
Matrix:AQ - Ground Water Date Received:04/20/19
Method:EPA 504.1 EPA 504.1 Percent Solids:n/a
Project:Yogi Foods; Hudson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a DD106069.D 25 04/29/19 13:06 NJ 04/24/19 12:45 OP74738 GDD3060
Run #2
Initial Volume Final Volume
Run #1 37.4 ml 2.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane 11.8 0.47 0.23 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 0% b 63-137%
(a) All hits confirmed by dual column analysis.
(b) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
 Chain of Custody
Orlando, FL
Section 4
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FA63492: Chain of Custody
Page 1 of 2
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Job Number:FA63492 Client:ATC
Date / Time Received:4/20/2019 9:00:00 AM Delivery Method:FX
Project:YOGI FOODS
Airbill #'s:78675958028
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (2.2);
Cooler 1: (2.6);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:BRANDYK Date:Date:4/20/2019 9:00:00 AM
FA63492: Chain of Custody
Page 2 of 2
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MS Volatiles
QC Data Summaries
Includes the following where applicable:
 Method Blank Summaries
 Blank Spike Summaries
 Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
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Method Blank Summary Page 1 of 3
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2113-MB E098842.D 1 04/26/19 AB n/a n/a VE2113
The QC reported here applies to the following samples:Method: SM 6200B
FA63492-1, FA63492-2
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
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Method Blank Summary Page 2 of 3
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2113-MB E098842.D 1 04/26/19 AB n/a n/a VE2113
The QC reported here applies to the following samples:Method: SM 6200B
FA63492-1, FA63492-2
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 95%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 102%70-130%
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Method Blank Summary Page 3 of 3
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2113-MB E098842.D 1 04/26/19 AB n/a n/a VE2113
The QC reported here applies to the following samples:Method: SM 6200B
FA63492-1, FA63492-2
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 102%70-130%
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Blank Spike Summary Page 1 of 3
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2113-BS E098840.D 1 04/26/19 AB n/a n/a VE2113
The QC reported here applies to the following samples:Method: SM 6200B
FA63492-1, FA63492-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 50 48.3 97 70-130
71-43-2 Benzene 10 9.0 90 70-130
108-86-1 Bromobenzene 10 9.9 99 70-130
74-97-5 Bromochloromethane 10 8.3 83 70-130
75-27-4 Bromodichloromethane 10 9.2 92 70-130
75-25-2 Bromoform 10 9.3 93 70-130
78-93-3 2-Butanone (MEK)50 43.9 88 70-130
104-51-8 n-Butylbenzene 10 10.2 102 70-130
135-98-8 sec-Butylbenzene 10 11.0 110 70-130
98-06-6 tert-Butylbenzene 10 10.4 104 70-130
56-23-5 Carbon Tetrachloride 10 9.9 99 70-130
108-90-7 Chlorobenzene 10 9.6 96 70-130
75-00-3 Chloroethane 10 8.1 81 60-140
67-66-3 Chloroform 10 9.0 90 70-130
95-49-8 o-Chlorotoluene 10 10.2 102 70-130
106-43-4 p-Chlorotoluene 10 10.1 101 70-130
124-48-1 Dibromochloromethane 10 9.6 96 70-130
106-93-4 1,2-Dibromoethane 10 9.3 93 70-130
75-71-8 Dichlorodifluoromethane 10 10.9 109 60-140
95-50-1 1,2-Dichlorobenzene 10 9.9 99 70-130
541-73-1 1,3-Dichlorobenzene 10 10.3 103 70-130
106-46-7 1,4-Dichlorobenzene 10 9.8 98 70-130
75-34-3 1,1-Dichloroethane 10 9.4 94 70-130
107-06-2 1,2-Dichloroethane 10 8.7 87 70-130
75-35-4 1,1-Dichloroethylene 10 9.3 93 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.1 91 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.1 91 70-130
78-87-5 1,2-Dichloropropane 10 9.1 91 70-130
142-28-9 1,3-Dichloropropane 10 9.2 92 70-130
594-20-7 2,2-Dichloropropane 10 10.2 102 70-130
563-58-6 1,1-Dichloropropene 10 9.6 96 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.3 83 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.4 94 70-130
108-20-3 Di-Isopropyl Ether 10 8.2 82 70-130
64-17-5 Ethyl Alcohol 500 403 81 70-130
100-41-4 Ethylbenzene 10 10.2 102 70-130
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 3
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2113-BS E098840.D 1 04/26/19 AB n/a n/a VE2113
The QC reported here applies to the following samples:Method: SM 6200B
FA63492-1, FA63492-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
591-78-6 2-Hexanone 50 51.8 104 70-130
98-82-8 Isopropylbenzene 10 10.9 109 70-130
99-87-6 p-Isopropyltoluene 10 11.0 110 70-130
74-83-9 Methyl Bromide 10 8.4 84 60-140
74-87-3 Methyl Chloride 10 9.4 94 60-140
75-09-2 Methylene Chloride 10 9.0 90 70-130
108-10-1 4-Methyl-2-pentanone (MIBK)50 54.1 108 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.2 82 70-130
91-20-3 Naphthalene 10 10.3 103 70-130
103-65-1 n-Propylbenzene 10 10.5 105 70-130
100-42-5 Styrene 10 9.3 93 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.0 100 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.3 103 70-130
127-18-4 Tetrachloroethylene 10 10.4 104 70-130
108-88-3 Toluene 10 9.8 98 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.5 105 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.3 103 70-130
71-55-6 1,1,1-Trichloroethane 10 9.3 93 70-130
79-00-5 1,1,2-Trichloroethane 10 9.8 98 70-130
79-01-6 Trichloroethylene 10 9.1 91 70-130
75-69-4 Trichlorofluoromethane 10 8.5 85 60-140
96-18-4 1,2,3-Trichloropropane 10 9.8 98 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.1 101 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.6 106 70-130
108-05-4 Vinyl Acetate 50 39.3 79 70-130
75-01-4 Vinyl Chloride 10 9.4 94 60-140
m,p-Xylene 20 20.3 102 70-130
95-47-6 o-Xylene 10 10.0 100 70-130
1330-20-7 Xylene (total)30 30.3 101 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 104%70-130%
* = Outside of Control Limits.
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Blank Spike Summary Page 3 of 3
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2113-BS E098840.D 1 04/26/19 AB n/a n/a VE2113
The QC reported here applies to the following samples:Method: SM 6200B
FA63492-1, FA63492-2
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA63492-2MS E098848.D 100 04/26/19 AB n/a n/a VE2113
FA63492-2MSD E098849.D 100 04/26/19 AB n/a n/a VE2113
FA63492-2 E098846.D 25 04/26/19 AB n/a n/a VE2113
The QC reported here applies to the following samples:Method: SM 6200B
FA63492-1, FA63492-2
FA63492-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 5000 4640 93 5000 4720 94 2 70-130/20
71-43-2 Benzene 277 1000 1200 92 1000 1170 89 3 70-130/20
108-86-1 Bromobenzene ND 1000 992 99 1000 979 98 1 70-130/20
74-97-5 Bromochloromethane ND 1000 818 82 1000 789 79 4 70-130/20
75-27-4 Bromodichloromethane ND 1000 922 92 1000 887 89 4 70-130/20
75-25-2 Bromoform ND 1000 933 93 1000 944 94 1 70-130/20
78-93-3 2-Butanone (MEK)ND 5000 4220 84 5000 4350 87 3 70-130/20
104-51-8 n-Butylbenzene 8.2 J 1000 1030 102 1000 1010 100 2 70-130/20
135-98-8 sec-Butylbenzene 5.8 J 1000 1120 111 1000 1080 107 4 70-130/20
98-06-6 tert-Butylbenzene ND 1000 1060 106 1000 1030 103 3 70-130/20
56-23-5 Carbon Tetrachloride ND 1000 966 97 1000 939 94 3 70-130/20
108-90-7 Chlorobenzene ND 1000 961 96 1000 932 93 3 70-130/20
75-00-3 Chloroethane ND 1000 741 74 1000 871 87 16 60-140/20
67-66-3 Chloroform ND 1000 902 90 1000 878 88 3 70-130/20
95-49-8 o-Chlorotoluene 15.6 1000 1030 101 1000 1030 101 0 70-130/20
106-43-4 p-Chlorotoluene ND 1000 1010 101 1000 993 99 2 70-130/20
124-48-1 Dibromochloromethane ND 1000 941 94 1000 936 94 1 70-130/20
106-93-4 1,2-Dibromoethane 14.6 1000 947 93 1000 936 92 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 1010 101 1000 1170 117 15 60-140/20
95-50-1 1,2-Dichlorobenzene ND 1000 997 100 1000 970 97 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 1000 1030 103 1000 1010 101 2 70-130/20
106-46-7 1,4-Dichlorobenzene ND 1000 968 97 1000 943 94 3 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 934 93 1000 903 90 3 70-130/20
107-06-2 1,2-Dichloroethane 11.1 J 1000 873 86 1000 850 84 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 925 93 1000 897 90 3 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 897 90 1000 870 87 3 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 899 90 1000 872 87 3 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 884 88 1000 860 86 3 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 919 92 1000 891 89 3 70-130/20
594-20-7 2,2-Dichloropropane ND 1000 949 95 1000 921 92 3 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 946 95 1000 918 92 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 808 81 1000 793 79 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 915 92 1000 909 91 1 70-130/20
108-20-3 Di-Isopropyl Ether ND 1000 814 81 1000 789 79 3 70-130/20
64-17-5 Ethyl Alcohol ND 50000 43000 86 50000 41800 84 3 70-130/20
100-41-4 Ethylbenzene 81.3 1000 1090 101 1000 1070 99 2 70-130/20
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA63492-2MS E098848.D 100 04/26/19 AB n/a n/a VE2113
FA63492-2MSD E098849.D 100 04/26/19 AB n/a n/a VE2113
FA63492-2 E098846.D 25 04/26/19 AB n/a n/a VE2113
The QC reported here applies to the following samples:Method: SM 6200B
FA63492-1, FA63492-2
FA63492-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 5000 4800 96 5000 4990 100 4 70-130/20
98-82-8 Isopropylbenzene 18.2 1000 1100 108 1000 1070 105 3 70-130/20
99-87-6 p-Isopropyltoluene 3.8 J 1000 1110 111 1000 1090 109 2 70-130/20
74-83-9 Methyl Bromide ND 1000 766 77 1000 914 91 18 60-140/20
74-87-3 Methyl Chloride ND 1000 895 90 1000 999 100 11 60-140/20
75-09-2 Methylene Chloride 28.7 J 1000 913 88 1000 877 85 4 70-130/20
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5000 5220 104 5000 5350 107 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 1000 807 81 1000 791 79 2 70-130/20
91-20-3 Naphthalene 89.6 1000 1120 103 1000 1090 100 3 70-130/20
103-65-1 n-Propylbenzene 47.6 1000 1100 105 1000 1080 103 2 70-130/20
100-42-5 Styrene ND 1000 921 92 1000 911 91 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 976 98 1000 965 97 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 1010 101 1000 1010 101 0 70-130/20
127-18-4 Tetrachloroethylene ND 1000 1020 102 1000 1000 100 2 70-130/20
108-88-3 Toluene 901 1000 1890 99 1000 1880 98 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 1000 987 99 1000 977 98 1 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 1000 1010 101 1000 978 98 3 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 920 92 1000 891 89 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 1000 957 96 1000 944 94 1 70-130/20
79-01-6 Trichloroethylene ND 1000 905 91 1000 870 87 4 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 788 79 1000 908 91 14 60-140/20
96-18-4 1,2,3-Trichloropropane ND 1000 961 96 1000 967 97 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene 484 1000 1520 104 1000 1500 102 1 70-130/20
108-67-8 1,3,5-Trimethylbenzene 141 1000 1220 108 1000 1190 105 2 70-130/20
108-05-4 Vinyl Acetate ND 5000 3770 75 5000 3850 77 2 70-130/20
75-01-4 Vinyl Chloride ND 1000 867 87 1000 1020 102 16 60-140/20
m,p-Xylene 624 2000 2670 102 2000 2630 100 2 70-130/20
95-47-6 o-Xylene 482 1000 1500 102 1000 1470 99 2 70-130/20
1330-20-7 Xylene (total)1110 3000 4160 102 3000 4100 100 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA63492-2 Limits
1868-53-7 Dibromofluoromethane 99%97%94%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%101%98%70-130%
2037-26-5 Toluene-D8 104%104%103%70-130%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA63492-2MS E098848.D 100 04/26/19 AB n/a n/a VE2113
FA63492-2MSD E098849.D 100 04/26/19 AB n/a n/a VE2113
FA63492-2 E098846.D 25 04/26/19 AB n/a n/a VE2113
The QC reported here applies to the following samples:Method: SM 6200B
FA63492-1, FA63492-2
CAS No.Surrogate Recoveries MS MSD FA63492-2 Limits
460-00-4 4-Bromofluorobenzene 100%102%101%70-130%
* = Outside of Control Limits.
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SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
 Method Blank Summaries
 Blank Spike Summaries
 Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
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Method Blank Summary Page 1 of 1
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP74738-MB DD106042.D 1 04/24/19 NM 04/24/19 OP74738 GDD3059
The QC reported here applies to the following samples:Method: EPA 504.1
FA63492-1, FA63492-2
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane ND 0.020 0.010 ug/l
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 95%63-137%
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Blank Spike Summary Page 1 of 1
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP74738-BS DD106040.D 1 04/24/19 NM 04/24/19 OP74738 GDD3059
The QC reported here applies to the following samples:Method: EPA 504.1
FA63492-1, FA63492-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
106-93-4 1,2-Dibromoethane 0.25 0.26 104 70-130
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 91%63-137%
* = Outside of Control Limits.
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Blank Spike Summary Page 1 of 1
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP74738-BS2 DD106041.D 1 04/24/19 NM 04/24/19 OP74738 GDD3059
The QC reported here applies to the following samples:Method: EPA 504.1
FA63492-1, FA63492-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
106-93-4 1,2-Dibromoethane 0.25 0.27 108 70-130
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 90%63-137%
* = Outside of Control Limits.
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Matrix Spike Summary Page 1 of 1
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP74738-MS DD106046.D 1 04/24/19 NM 04/24/19 OP74738 GDD3059
FA63517-1 DD106045.D 1 04/24/19 NM 04/24/19 OP74738 GDD3059
The QC reported here applies to the following samples:Method: EPA 504.1
FA63492-1, FA63492-2
FA63517-1 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
106-93-4 1,2-Dibromoethane ND 0.231 0.16 69*70-130
CAS No.Surrogate Recoveries MS FA63517-1 Limits
460-00-4 4-Bromofluorobenzene 61%* a 72%63-137%
460-00-4 4-Bromofluorobenzene 78%63-137%
(a) Outside control limits.
* = Outside of Control Limits.
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Duplicate Summary Page 1 of 1
Job Number:FA63492
Account:ATCNCC ATC Group Services LLC
Project:Yogi Foods; Hudson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP74738-DUP DD106048.D 1 04/24/19 NM 04/24/19 OP74738 GDD3059
FA63517-2 DD106047.D 1 04/24/19 NM 04/24/19 OP74738 GDD3059
The QC reported here applies to the following samples:Method: EPA 504.1
FA63492-1, FA63492-2
FA63517-2 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
106-93-4 1,2-Dibromoethane ND ND nc 25
CAS No.Surrogate Recoveries DUP FA63517-2 Limits
460-00-4 4-Bromofluorobenzene 91%87%63-137%
* = Outside of Control Limits.
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MONITORING REPORT
Yogi Foods
4018 Highway 321A
Hudson, Caldwell County, North Carolina 28638
ATC Project No. CARYOGI
NCDEQ Incident No. 28491
NCDEQ Facility ID No. 0-007809
NCDEQ Risk Classification: Intermediate (I130D)

October 1, 2019

7606 Whitehall Executive Center Drive
Suite 800
Charlotte, NC 28273
Tel: [phone]
Fax: [phone]
www.atcgroupservices.com
N.C. Engineering License No. C-1598

October 1, 2019

Mr. Dan Murphy
North Carolina Department of Environmental Quality
Asheville Regional Office
Division of Waste Management - UST Section
2090 US Highway 70
Swannanoa, North Carolina 28778

RE: Monitoring Report
Yogi Foods
4018 Highway 321A
Hudson, Caldwell County, North Carolina 28638
ATC Project No. CARYOGI
NCDEQ Incident No. 28491
NCDEQ Facility ID No. 0-007809
NCDEQ Risk Classification: Intermediate (I130D)

Dear Mr. Murphy:

ATC Associates of North Carolina, P.C., on behalf of Cary Oil Company, is submitting the
enclosed Monitoring Report for the referenced site. The report includes information pertaining
to an Aggressive Fluid Vapor Recovery event and subsquent groundwater monitoring event
conducted in July and August 2019.

If you have any questions or require additional information, please contact us at [phone].

Sincerely,
ATC Associates of North Carolina, P.C.

Erin E. Greene Mike Shaw
Project Manager Senior Project Manager

cc: Mr. Glenn Petti, Cary Oil Company

Monitoring Report
Yogi Foods
4018 Highway 321A
Hudson, Caldwell County, North Carolina 28638
ATC Project No. CARYOGI
NCDEQ Incident No. 28491
NCDEQ Facility ID No. 0-007809
NCDEQ Risk Classification: Intermediate (I130D)

Prepared By: Submitted To:

North Carolina Department of
Environmental Quality
Erin. E. Greene Asheville Regional Office
Project Manager Division of Waste Management - UST Section
2090 US Highway 70
Swannanoa, North Carolina 28778

___________________________ Submitted By:
Mike Shaw, P.G.
NC Professional Geologist #1338
ATC Associates of North Carolina, P.C.
7606 Whitehall Executive Center Drive
Suite 800
Charlotte, North Carolina 28273
Phone: [phone]
Fax: [phone]

On Behalf Of:

Cary Oil Company
110 Mackenan Drive, Suite 300
Cary, North Carolina 27511
Phone: [phone]

October 1, 2019

Site Identification:
Date of Report: 10/1/19 Site Risk: Intermediate (I130D)
Facility I.D.: 0-007809 UST Incident Number (if known): 28491
Site Name: Yogi Foods
Site Street Address: 4018 Highway 321A
City/Town: Hudson Zip Code: 28638 County: Caldwell
Description of Geographical Data Point (e.g., diesel fill port): UST Basin
Location Method (GPS, topographical map, other): Google Earth
Latitude (decimal degrees): 35.827182° N Longitude (decimal degrees): -81.476007° W

Information about Contacts Associated with the Release:
UST Owner: Cary Oil Company
Address: 110 Mackenan Drive, Suite 300, Cary, NC 27511 Phone: [phone]
UST Operator: AJ Patel
Address: 4018 Highway 321A, Hudson, NC 28638 Phone: [phone]
Property Owner: HHA Development LLC
Address: PO Box 190, Taylorsville, NC 28681 Phone: Unknown
Property Occupant: Shell Service Station/Market Basket Convenience Store
Address: 4018 Highway 321A, Hudson, NC 28638 Phone: Unknown
Consultant/Contractor: ATC Associates of North Carolina, P.C.
Address:7606 Whitehall Executive Center Dr, Charlotte, NC 28273 Phone: [phone]
Analytical Laboratory: Pace Analytical Services, Inc. State Certification No.: 5342
Address: 9800 Kincey Ave., Suite 100, Huntersville, NC 28078 Phone: [phone]

Information about Release:
Date Discovered: July 14, 2006
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release (Dispenser/Piping/UST): Gasoline/diesel UST system
Sizes and contents of UST system(s) from which the release occurred: Two 8,000-gallon gasoline USTs, one
8,000-gallon diesel UST, and one-2,000 gallon kerosene UST and associated piping and dispensers.

TABLE OF CONTENTS

1.0 EXECUTIVE SUMMARY ............................................................................................................. 1
2.0 SITE HISTORY AND CHARACTERIZATION ......................................................................... 1
3.0 RECEPTOR INFORMATION ....................................................................................................... 3
3.1 Water Supply Wells ............................................................................................................ 3
3.2 Public Water Supplies ......................................................................................................... 3
3.3 Surface Water ...................................................................................................................... 3
4.0 SITE CHARACTERISTICS ........................................................................................................... 4
4.1 Regional and Site Geology ................................................................................................. 4
4.2 Regional and Site Hydrogeology ........................................................................................ 4
5.0 AFVR EVENT .................................................................................................................................. 5
6.0 GROUNDWATER MONITORING .............................................................................................. 6
7.0 CONCLUSIONS AND RECOMMENDATIONS ......................................................................... 7
8.0 LIMITATIONS AND CERTIFICATIONS ................................................................................... 7

TABLES

Table B-1 Site History - UST System and Other Release Information
Table B-2 Site History - UST Owner/Operator and Other Responsible Party Information
Table B-4 Summary of Groundwater Sampling Results
Table B-4A Summary of Historical Groundwater Sampling Results
Table B-5 Public and Private Water Supply Well and Other Receptor Information
Table B-7 Monitoring Well Construction Information
Table B-8 Free Product Recovery Information

FIGURES

Figure 1 Site Topographic Map
Figure 2 Site Map
Figure 3 Constituents of Concern Map

APPENDICES

Appendix A AFVR Data
Appendix B Laboratory Analytical Reports

Yogi Foods October 1, 2019
Monitoring Report Page 1

1.0 EXECUTIVE SUMMARY

ATC Associates of North Carolina, P.C. (ATC), on behalf of Cary Oil Company (Cary Oil), has prepared
a Monitoring Report for the Yogi Foods facility located in Hudson, Caldwell County, North Carolina.
This report includes information summarizing field activities conducted in July and August 2019. A
United States Geological Survey (USGS) topographic map that shows topographic contours, site location,
surface water bodies, buildings, and adjacent roads in the site vicinity is included as Figure 1.

A North Carolina Department of Environmental Quality (NCDEQ) Notice of Regulatory Requirements
(NORR) dated June 7, 2019, required remediation and assessment activities be conducted at the Yogi Foods
site. ATC conducted an Aggressive Fluid Vapor Recovery (AFVR) event on July 30, 2019, and a
groundwater monitoring event on August 29, 2019. The findings of the field activities and results of the
analytical results indicate the following:
 Free product was not detected in the gauged monitoring wells during any of the field activities
conducted in July and August 2019.
 Benzene, 1,2-DCA, and EDB exceeded GCLs in MW-1 prior to the AFVR event.
 The AFVR event removed approximately 278 gallons of petroleum-impacted groundwater, and was
calculated to recover 54.28 pounds (8.69 gallons) of petroleum as vapor.
 Approximately 30 days after the AFVR event, well MW-1 contained benzene above the GCL, and
reduced by approximately 78%.
A comprehensive groundwater monitoring event has not been conducted at the site since 2017. ATC
recommends a comprehensive monitoring event be conducted approximately six months after the AFVR
(February 2020). The sampling event will evaluate the extents of the contamination plume and should
specifically utilize low-flow sampling methods to obtain an accurate and representative sample from 1-inch
monitoring well MW-1.

2.0 SITE HISTORY AND CHARACTERIZATION

The subject site is identified as the Yogi Foods facility (Facility ID No. 0-007809) and is located at 4018
Highway 321A in Hudson, Caldwell County, North Carolina. The site is accessible from Highway 321A
to the west and Adams Drive to the southeast. Properties within 1,500 feet of the site are mainly commercial
and residential on the east side Highway 321A and mainly industrial on the west side of Highway 321A. A
site map that indicates monitoring well locations and other site features is included as Figure 2.
Yogi Foods October 1, 2019
Monitoring Report Page 2

The subject property currently operates as a Shell service station with retail fuel sales and a convenience
store called Market Basket. Two 8,000-gallon gasoline underground storage tanks (USTs) and one 8,000-
gallon diesel UST were installed in April 1985 and are currently in use at the site. A separate basin
contains one 2,000-gallon kerosene UST, which was installed in February 1976 and is also currently in
use. UST system and owner/operator information is provided in Tables B-1 and B-2. The site also
contains a single-story convenience store building and fuel dispensers associated with the USTs. Surface
cover at the site consists mostly of asphalt and concrete in the fueling and driveway areas. The surface
cover on the east portion of the property, behind the convenience store building, consists mostly of grass.

A due diligence investigation was conducted at the site on June 30, 2006. Soil samples were collected at nine
locations and submitted for laboratory analysis of total petroleum hydrocarbons – gasoline range organics
(TPH – GRO). Laboratory analytical results of a soil sample collected adjacent to a gasoline and diesel
dispenser indicated a TPH – GRO concentration that exceeded the historical North Carolina Department of
Environment and Natural Resources (NCDENR, currently the NCDEQ) action limit of 10 mg/kg. Cary Oil
submitted a 24-Hour Release and UST Leak Reporting Form (UST-61) to the NCDEQ on July 14, 2006.

ATC conducted a Phase II LSA in August 2014 and collected groundwater samples from wells MW-1
through MW-4. Petroleum compounds were reported above NCDEQ 2L Standards in wells MW-1, MW-2,
and MW-4. Concentrations of lead were reported above the 2L Standard in wells MW-1 through MW-4. The
concentrations of benzene and EDB reported in well MW-1 exceeded their respective GCLs.

A limited groundwater monitoring event was conducted at the site on March 24, 2016, following two AFVR
events. Petroleum compounds were reported above 2L Standards in well MW-1. The concentrations of
benzene, 1,2-dichloroethane (DCA), and EDB reported in well MW-1 exceeded their respective GCLs.

A large diameter well (MW-5) and two air sparge wells (AS-1 and AS-2) were installed at the site in August
2016. A limited groundwater monitoring event was conducted at the site on November 2, 2016, following a
sparge-enhanced AFVR event. Concentrations of petroleum hydrocarbons were detected above GCLs in
monitoring well MW-1, but were significantly decreased compared to historical levels and MW-5 did not
contain contaminant concentrations above GCLs.

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On April 20, 2017, ATC performed a limited groundwater gauging and sampling event at the site to
identify effectiveness of a sparge-enhanced AFVR event. According to the analytical results,
concentrations of petroleum hydrocarbons were not detected above GCLs in monitoring wells MW-1 and
MW-5.

Since that time, ATC conducted limited groundwater sampling events in April 2018, and April 2019. The
analytical results from both sampling events indicated that groundwater from well MW-1 well contained
EDB concentrations above the GCL.

3.0 RECEPTOR INFORMATION
3.1 Water Supply Wells

An updated receptor survey was conducted at the site in 2012, which provided supplemental information
to an initial receptor survey conducted during a Phase I Limited Site Assessment (LSA) in 2006. One
private well (WSW-4) was identified as being used for irrigation purposes and is located approximately 315
feet from the source area. Thirteen additional water supply wells were identified within 1,500 feet of the site
but are not in use. A large concrete cover was observed at the property located at 2338 Adams Drive and
adjacent to the subject site, and was identified as a potential water supply well. The property at 2338 Adams
Drive, is supplied municipal water by the Town of Sawmills. The NCDEQ decided in December 2015 that
the potential water supply well was considered abandoned, and the site risk ranking was reduced from high to
intermediate. The receptor information is provided as Table B-5.

3.2 Public Water Supplies

Potable water is provided to the area by the Town of Sawmills and the City of Lenoir. The public water
source (Lake Rhodhiss) is not located within 1,500 feet of the subject site.

3.3 Surface Water

ATC reviewed a USGS 7.5-Minute Quadrangle Topographic Map (Figure 1) to identify surface water
bodies in the site vicinity. In addition, ATC conducted a visual reconnaissance for surface water bodies
in the area. Poplar Fish Lake is located approximately 1,100 feet to the east of the subject site.

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Monitoring Report Page 4

4.0 SITE CHARACTERISTICS
4.1 Regional and Site Geology

According to the Geologic Map of North Carolina, produced by the State of North Carolina in 1985, the
site lies in the Inner Piedmont Belt of the Piedmont Physiographic Province of North Carolina. The rock
types of the Inner Piedmont have been identified as predominatly mica schist with a variety of other rock
types depending on location. The Inner Piedmont is characterized as crystalline meta-sedimantary rock.
The shallow subsurface in most areas of the Piedmont contains residual soil overburden, including
structure-free residuum, saprolite, and partially weathered rock (PWR) that derive from in-place
weathering of the crystalline bedrock. Occasional areas containing recent deposits of alluvium in the
uppermost subsurface are found near streams and rivers. Saprolite and PWR typically contain some relict
structures from the original rock material. Depth to rock ranges from ground surface at occasional
outcrops to depths of greater than 100 feet in areas of easily weathered rock.

Shallow subsurface soils observed during drilling activities at the site were described as sandy and silty clay
and sandy and clayey silt to a termination depth of approximately 35 feet below grade.

4.2 Regional and Site Hydrogeology

The shallow aquifer occurrence varies in depth from ground surface at springs, creeks, and rivers to as
deep as 50 feet or more beneath upland surfaces in some parts of the Piedmont. Water in the alluvium or
unconsolidated residual material, including saprolite and PWR, usually behaves as an unconfined aquifer,
or water table, and will yield water with head elevation equivalent to the first elevation where water was
encountered. Permeability varies with lithology and is typically relatively low in residual soils, with
higher permeability in saprolite or PWR due to relict rock texture and variable susceptibility to
weathering exhibited by different minerals in the rock. Groundwater flow in residual soils or alluvium is
usually in rough concurrence with local topographic conditions and is toward local drainage features.

The bedrock fractures or other planar features of the Piedmont Physiographic Province generally
constitute the bedrock aquifer, with the surrounding rock material being effectively impermeable. Along
with fractures, contacts between rock bodies probably constitute zones of significant groundwater
occurrence in the bedrock. The surrounding material and overlying residuum tend to make the bedrock
aquifer a semi-confined aquifer. That is, the overlying water and soil weight normally results in pressure
that causes water in a borehole, which intersects a fracture or other feature, to rise above the elevation of
Yogi Foods October 1, 2019
Monitoring Report Page 5

the fracture or feature. Modern water supply wells in the Piedmont, likely including those in the site
vicinity, are typically installed with a surface casing through the unconsolidated material, and an open
borehole into the bedrock where water-bearing fractures are encountered.

Based on data collected in November 2017, groundwater flow away from the site appears to be generally
towards the east at an average horizontal hydraulic gradient of 0.008 along a flow path that crosses the
release source area. Depth to groundwater in site monitoring wells ranged from 16.13 feet to 23.66 feet
below top of casing (TOC) on November 16, 2017. Free product was not observed in the gauged wells
and has not historically been identified on-site.

5.0 AFVR EVENT

On July 30, 2019, an 8-hour AFVR event was conducted at well MW-5. AFVR services were provided by
Contaminant Control, Inc. (CCI), with oversight provided by ATC. Prior to and at the completion of the
AFVR event, wells MW-1, MW-5, AS-1, and AS-2 were gauged using an oil/water interface probe. Free
product was not measured in gauged wells. ATC collected one groundwater sample for laboratory analysis
from well MW-1. The groundwater sample was analyzed for volatile organic compounds (VOCs) via
Standard Method 6200B, and ethylene dibromide (EDB) via method 504.1. The analytical results are
discussed in Section 6.0.

During AFVR activities, a liquid ring vacuum pump unit is plumbed to the designated extraction
point, and a drop pipe is extended into the well through an airtight seal at the top of the well
casing (TOC) and into the water column. Throughout the AFVR process, a cone of depression
forms around the designated recovery point by drawing down the groundwater surface levels,
thus causing impacted water surrounding the recovery point to be extracted. Petroleum-impacted
soil vapor within the cone of depression and the overlying vadose zone is removed as part of the
AFVR extraction process.

Approximately 278 gallons of petroleum-impacted groundwater were recovered from monitoring well MW-
5 during the July 30, 2019, AFVR event. Measurable free product was not observed in the vacuum truck tank
following the event. Based on calculated recovery volumes, approximately 54.28 pounds (8.69 gallons) of
petroleum were recovered as vapor. Monitoring data, the waste disposal manifest, and emissions and
Yogi Foods October 1, 2019
Monitoring Report Page 6

recovery calculations for this AFVR emissions are included in Appendix A. Free product recovery
information is provided in Table B-8.

6.0 GROUNDWATER MONITORING

On July 30, 2019, prior to the AFVR event, ATC collected one grab sample from monitoring well MW-1.
The sample was collected with a new, disposable bailer, and poured directly into laboratory-provided
containers with appropriate preservatives. The sample was placed into a chilled cooler and submitted to
North Carolina-accredited Pace Analytical Services, Inc. (Pace), of Huntersville, North Carolina using proper
chain-of-custody procedures for laboratory analyses. The sample was analyzed by SM 6200B for VOCs and
EPA Method 504.1 for EDB. Laboratory analysis of the sample collected from well MW-1 prior to the
AFVR event indicated the following:
 Benzene (11,400 ug/L), 1,2-DCA (510 ug/L), and EDB (953 ug/L via EPA 504.1) were detected
above their respective GCL.
 Nine additional petroleum constituents were detected above their respective 2L Standard.

On August 29, 2019, ATC gauged and sampled monitoring wells MW-1 and MW-5 to assess the
effectiveness of the AFVR event. Groundwater elevation data for the August 2019 sampling event is
summarized in Table B-7. Prior to sampling, each well was purged of three standing water columns, or until
the well was purged dry. Samples were then collected with new disposable bailers and poured directly into
laboratory-provided containers with appropriate preservatives. The samples were placed into a chilled cooler
and submitted to Pace using proper chain-of-custody procedures for laboratory analyses. The samples were
analyzed by SM 6200B for VOCs and EPA Method 504.1 for EDB. Laboratory analysis of the samples
collected indicated the following:
 Well MW-1 contained EDB (200ug/L via SM6200) above the GCL, and nine additional
petroleum constituents above their respective 2L Standard.
 Well MW-5 contained four petroleum constituents above their respective 2L Standard.

The laboratory analytical reports are included in Appendix B. Current groundwater sampling results are
summarized in Table B-4, historical analytical results are included in Table B-4A. A map depicting a
summary of the constituents of concern from the July and August 2019 sampling events is included as
Figure 3.

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Groundwater impact above GCLs has historically been identified in wells MW-1 and MW-5 located near the
product dispensers. The July 2019 AFVR appears to have been effective at reducing the concentrations of
petroleum constituents in well MW-1 as follows: benzene by approximately 65%, toluene by 53%, 1,2-DCA
by 78%, and EDB by 78%.

7.0 CONCLUSIONS AND RECOMMENDATIONS

Groundwater impact above GCLs has historically been identified in wells MW-1 and MW-5 located near the
product dispensers. ATC conducted an Aggressive Fluid Vapor Recovery (AFVR) event on July 30, 2019,
and a groundwater monitoring event on August 29, 2019. The findings of the field activities and results of the
analytical results indicate the following:
 Free product was not detected in the gauged monitoring wells during any of the field activities
conducted in July and August 2019.
 Benzene, 1,2-DCA, and EDB exceeded GCLs in MW-1 prior to the AFVR event.
 The AFVR event removed approximately 278 gallons of petroleum-impacted groundwater, and was
calculated to recover 54.28 pounds (8.69 gallons) of petroleum as vapor.
 Approximately 30 days after the AFVR event, well MW-1 contained benzene above the GCL, and
reduced by approximately 78%.

A comprehensive groundwater monitoring event has not been conducted at the site since 2017. ATC
recommends a comprehensive monitoring event be conducted approximately six months after the AFVR
(February 2020). The sampling event will evaluate the extents of the contamination plume and should
specifically utilize low-flow sampling methods to obtain an accurate and representative sample from 1-inch
monitoring well MW-1.

8.0 LIMITATIONS AND CERTIFICATIONS

This investigation is intended to be a non-biased assessment of on-site environmental conditions
proximate to the location of the former and/or current UST system. Subsurface investigative and remedial
methodologies were performed in general accordance with applicable state and federal regulatory
requirements. The information presented in this report is based upon site-specific observations, generally
accepted geological and environmental consulting practices, and analytical results for environmental
samples collected at the time the field investigation was performed. The data presented in this report are
Yogi Foods October 1, 2019
Monitoring Report Page 8

believed to represent subsurface conditions at the facility; however, data may not be completely
representative of subsurface conditions at every location. ATC assumes no liability arising from
environmental impact to, or from, the site, regardless of the date of impact occurrence or findings.

1 Enter the date the monitoring report was due. N/A. Will this report be submitted after
the established due date? N/A
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to
explain what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule
approved in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)
N/A
4 Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source?
YES NO
IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions
recommended to further assess or clean up this known or suspected source. (This should be described in
more detail in the report text above.)
6 Certification:
I, Mike Shaw, a Licensed Geologist for ATC Associates of North Carolina, P.C., do certify that the
information contained in this report is correct and accurate to the best of my knowledge.

ATC Associates of North Carolina, P.C. is licensed to practice engineering and geology in North Carolina.
The certification numbers of the company or corporation are C-1598 (engineering) and C-274 (geology).

TABLES
Table B-1: Site History - UST System and Other Release Information
Revision Date: 9/19/14 Incident Number and Name: 28491/Yogi Foods
UST ID Number Current/Last Contents Previous Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Description of
Associated Piping and
Pumps
Date Tank
Installed Status of UST
Was Release
Associated with
the UST System?
A1 Gasoline Gasoline 8,000 Steel unknown DW Steel/FRP 4/30/1985 In Use Unknown
A2 Gasoline Gasoline 8,000 Steel unknown DW Steel/FRP 4/30/1985 In Use Unknown
A3 Diesel Diesel 8,000 Steel unknown DW Steel/FRP 4/30/1985 In Use Unknown
A4 Kerosene Kerosene 2,000 Steel unknown DW Steel/FRP 2/5/1976 In Use No
AST ID Number Current/Last Contents Previous Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Description of
Associated Piping and
Pumps
Date Tank
Installed Status of AST
Was Release
Associated with
the AST System?
None Associated With This Site
Table B-2: Site History - UST Owner/Operator and Other Responsible Party Information
Revision Date: 10/8/14 Incident Number and Name: 28491/Yogi Foods
UST ID Number A1, A2, A3, A4 Facility ID Number 0-007809
City State Zip Telephone Number
Unknown Unknown Unknown Unknown
City State Zip Telephone Number
Hudson NC 28638 919-460-3195
UST ID Number A1, A2, A3, A4 Facility ID Number 0-007809
City State Zip Telephone Number
North Wilkesboro NC 28659 336-667-9453
City State Zip Telephone Number
North Wilkesboro NC 28659 336-667-9453
UST ID Number A1, A2, A3, A4 Facility ID Number 0-007809
City State Zip Telephone Number
Cary NC 27511 919-462-1100
City State Zip Telephone Number
Cary NC 27511 919-462-1100
UST ID Number A1, A2, A3, A4 Facility ID Number 0-007809
City State Zip Telephone Number
Lenoir NC 28645 828-758-4401
City State Zip Telephone Number
Lenoir NC 28645 828-758-4401
UST ID Number A1, A2, A3, A4 Facility ID Number 0-007809
City State Zip Telephone Number
Cliffside NC 28024 704-453-7351
City State Zip Telephone Number
Cliffside NC 28024 704-453-7351
Dates of Operation (MM/DD/YY to MM/DD/YY)Name of Owner
Unknown Date to Present
Name of Operator
AJ Patel
HHA Development LLC Unknown Date to Present
4018 Highway 321A
Street Address
Unknown
Street Address
Name of Owner Dates of Operation (MM/DD/YY to MM/DD/YY)
Dates of Operation (MM/DD/YY to MM/DD/YY)
Tar Heel Oil II, Inc.05/18/2009 to Unknown Date
Street Address
320 9th Street, PO Box 608
Tar Heel Oil II, Inc.05/18/2009 to Unknown Date
Street Address
320 9th Street, PO Box 608
Name of Operator Dates of Operation (MM/DD/YY to MM/DD/YY)
Name of Owner Dates of Operation (MM/DD/YY to MM/DD/YY)
Cary Oil Company 04/05/2005 to 05/17/2009
Street Address
110 Mackenan Drive, Suite 300
Name of Operator Dates of Operation (MM/DD/YY to MM/DD/YY)
Cary Oil Company 04/05/2005 to 05/17/2009
Street Address
110 Mackenan Drive, Suite 300
Name of Owner Dates of Operation (MM/DD/YY to MM/DD/YY)
Beall Oil Company/Blue Ridge Energies LLC 03/31/1997 to 04/04/2005
Street Address
110 Nuway Circle
Name of Operator Dates of Operation (MM/DD/YY to MM/DD/YY)
Beall Oil Company/Blue Ridge Energies LLC 03/31/1997 to 04/04/2005
Street Address
110 Nuway Circle
Name of Owner Dates of Operation (MM/DD/YY to MM/DD/YY)
Petroleum World, Inc.04/30/1986 to 03/30/1997
Street Address
PO Box 307, Highway 120
Street Address
PO Box 307, Highway 120
Name of Operator Dates of Operation (MM/DD/YY to MM/DD/YY)
Petroleum World, Inc.04/30/1986 to 03/30/1997
Table B-4: Summary of Groundwater Sampling Results
Revision Date: 9/27/19 Incident Number and Name: 28491/Yogi Foods Facility ID #: 0-007809
Standard Method 6200B 504.1
Well ID Date Collected Sample ID
Incident
Phase
MW-1 7/30/2019 MW-1 Pre-AFVR 11,400 28,100 849 11,700 <50.0 <50.0 <50.0 <50.0 510 <50.0 105 594 92.4 J <200 179 2,460 611 879 953
MW-1 8/29/2019 MW-1 Monitoring 3,990 13,200 731 6,430 ND ND ND 111 111 57.4 ND 449 57.4 ND ND 1,470 ND 200 193
MW-5 8/29/2019 MW-5 Monitoring 112 402 31 312 ND ND ND 3.5 3.5 5.3 ND 24.2 5.3 ND ND 110 ND 5.2 4.9
1 600 600 500 20 70 70 70 0.4 6 70 6 70 5 70 400 400 0.02 0.02
5,000 260,000 84,500 85,500 20,000 6,900 8,500 15,000 400 6,000 70,000 6,000 25,000 5,000 30,000 28,500 25,000 50 50
Results in ug/L
Concentrations in bold exceeded the 2L Standard
Concentrations in bold and italics exceeded the GCL
J = Estimated Value
NE = Not Established
Analytical Method (e.g. EPA 601)
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Table B-4A: Summary of Historical Groundwater Sampling Results
Revision Date: 9/27/19 Incident Number and Name: 28491/Yogi Foods
504.1
Well ID Date Collected Sample ID
Incident
Phase
MW-1 8/11/2006 MW-1 Phase I LSA 6,300 11,000 580 4,400 <100 NR NR NR <20 NR <100 <100 NR NR NR NR NR <20 <40 <20 NR NR
MW-1 8/6/2014 MW-1 Phase II LSA 13,500 26,900 1,120 6,910 <100 <100 <100 <100 950 <100 180 454 <100 <400 167 1,160 356 <100 <1,000 <100 <200 701
MW-1 3/24/2016 MW-1 Pre-CAP 13,000 34,500 1,430 9,210 <125 <125 <125 <125 634 <125 161 542 109 J <500 267 1,710 451 <125 <1,250 <125 <250 902
MW-1 11/2/2016 MW-1 Pre-CAP 5,820 17,800 986 6,090 <62.5 <62.5 <62.5 <62.5 168 <62.5 37.0 J 357 68.8 228 J 199 1,300 340 <62.5 <625 <62.5 <125 162
MW-1 4/20/2017 MW-1 Pre-CAP 627 1,170 105 2,260 <5.0 <5.0 <5.0 <5.0 29.7 <5.0 5.1 117 42.7 <20.0 <5.0 769 <5.0 <5.0 <50.0 <5.0 <10.0 30.9
MW-1 11/16/2017 MW-1 Monitoring 6,560 12,200 536 6,780 <50.0 28.9 J <50.0 <50.0 246 <50.0 77.2 384 55.6 <200 <50.0 1,300 <50.0 <50.0 <500 <50.0 <100 230
MW-1 4/13/2018 MW-1 Monitoring 3,920 13,000 671 5,000 <50 <50 <50 <50 116 <50 <50 388 45.8 J <200 <50 1,020 <50 <50 <50 <50 <100 262
MW-1 4/18/2019 MW-1 Monitoring 5,410 15,900 649 8,590 < 63 < 63 < 63 < 63 253 < 63 < 63 396 74.1 J < 500 152 J 1,890 540 < 63 < 63 < 63 < 100 296
MW-1 7/30/2019 MW-1 Pre-AFVR 11400 28100 849 11700 <50.0 <50.0 <50.0 <50.0 510 <50.0 105 594 92.4 J <200 179 2460 611 <50.0 <500 <500 <100 953
MW-1 8/29/2019 MW-1 Monitoring 3990 13200 731 6430 ND ND ND ND 111 ND 26.2J 449 57.4 ND ND 1,470 ND ND ND ND ND 193
MW-2 8/6/2014 MW-2 Phase II LSA 279 1,720 944 4,030 19.5 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 724 70.6 <40.0 120 814 201 <10.0 <100 <10.0 <20.0 0.075
MW-2 11/16/2017 MW-2 Monitoring 6.5 0.33 J 17.0 0.72 J <0.50 <0.50 4.5 0.97 <0.50 <0.50 <0.50 22.4 16.6 <2.0 12.8 <0.50 <0.50 <0.50 <5.0 0.90 <1.0 <0.019
MW-3 8/6/2014 MW-3 Phase II LSA <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <0.50 <0.50 0.66 5.0 6.5 <1.0 <0.022
MW-3 11/16/2017 MW-3 Monitoring <0.50 <0.50 <0.50 <1.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <5.0 <0.50 <1.0 <0.019
MW-4 8/6/2014 MW-4 Phase II LSA 36.4 35.1 651 1,101 <5.0 <5.0 28.0 <5.0 74.8 <5.0 11.9 584 161 <20.0 420 1,440 654 <5.0 <50.0 <5.0 <10.0 0.054
MW-4 11/16/2017 MW-4 Monitoring <0.50 0.65 11.2 <1.50 <0.50 43.8 36.6 <0.50 <0.50 0.83 <0.50 19.3 67.8 <2.0 157 <0.50 68.9 <0.50 <5.0 0.65 0.54 J <0.019
MW-5 11/2/2016 MW-5 Pre-CAP 1,830 5,420 399 4,190 <25.0 <25.0 <25.0 <25.0 50.2 <25.0 <25.0 238 55.8 135 162 1,140 290 <25.0 <250 <25.0 <50.0 29.1
MW-5 4/20/2017 MW-5 Pre-CAP 550 1,390 125 1,857 <5.0 29.5 <5.0 <5.0 25.5 <5.0 3.8 J 87.5 40.8 <20.0 <5.0 745 <5.0 <5.0 <50.0 <5.0 <10.0 29.1
MW-5 11/16/2017 MW-5 Monitoring 1,090 3,360 243 2,423 <12.5 <12.5 <12.5 <12.5 <12.5 <12.5 <12.5 221 39.3 <50.0 <12.5 791 <12.5 <12.5 <125 <12.5 <25.0 28.5
MW-5 4/13/2018 MW-5 Monitoring 171 580 54.8 488 <2.0 <2.0 <2.0 <2.0 5.9 <2.0 <2.0 39.4 9.1 <8.0 28.6 189 49.5 <2.0 <20 <2.0 <4.0 8.6
MW-5 4/18/2019 MW-5 Monitoring 277 901 81.3 1,110 < 3.1 8.2 J 5.8 J 11 11.1 J < 3.1 < 3.1 89.6 18.2 28.7 J 47.6 484 141.0 < 3.1 < 3.1 < 3.1 < 5.0 11.8
MW-5 8/29/2019 MW-5 Monitoring 112 402 30.5 312 ND ND ND ND 3.5 ND ND 24.2 5.3 ND ND 110 ND ND ND ND ND 4.9
1 600 600 500 20 70 70 70 0.4 6 70 6 70 5 70 400 400 NE 100 70 3 0.02
5,000 260,000 84,500 85,500 20,000 6,900 8,500 15,000 400 6,000 70,000 6,000 25,000 5,000 30,000 28,500 25,000 NE 100,000 70,000 3,000 50
Results in ug/L
Concentrations in bold exceeded the 2L Standard
Concentrations in bold and italics exceeded the GCL
J = Estimated Value
NE = Not Established
NR = Not Requested
ND = Not Detected
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Contaminant of Concern
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Analytical Method (e.g. EPA 601)EPA Method 624/6200B
Table B-5: Public and Private Water Supply Well and Other Receptor Information
Revision Date: 11/11/16 Incident Number and Name: 28491/Yogi Foods Facility ID #: 0-007809
Gene and Sandra Duncan
5124 Bloomfield Dr, Granite Falls, NC 28630
Jake and Hilda Fletcher
2342 Adams Dr, Hudson, NC 28638
Cora Novella Adams
PO Box 322, Granite Falls, NC 28630
Criss and Loretta Wilson
2343 Adams Dr, Hudson, NC 28638
Iona Baldwin
2347 Adams Dr, Hudson, NC 28638
George and Ila Wilcox
2335 Adams Dr, Hudson, NC 28638
Charles Gragg
4002 US Hwy 321A, Hudson, NC 28638
Charles Gragg
4002 US Hwy 321A, Hudson, NC 28638
Mr. and Mrs. Benfield
4102 US Hwy 321A, Granite Falls, NC 28630
Paul Dishman
2049 Jessica Ln, Hudson, NC 28638
Floyd and Theresa Annas
3968 US Hwy 321A, Hudson, NC 28638
Gladys Greene
2624 Mission Rd, Hudson, NC 28638
Casey Wallace
PO Box 152, Granite Falls, NC 28630
Charles Chester
4110 Ardmore Ln, Hudson, NC 28638
Earnest and Diana Harris
612 S Government St, Lincolnton, NC 28092
Poplar Fish Lake Not Applicable 4243 Poplar Lake Drive Not Available Not Applicable Not Applicable Not Applicable 1,100 -
Receptor survey conducted on 9/19/2012
Well not in use
Well not in use
WSW-15 4101 Ardmore Lane Not Available Inactive Unknown Unknown 1,470
1,155 Well not in use
WSW-14 4110 Ardmore Lane Not Available Inactive Unknown Unknown 1,260
WSW-13 2630 Mission Road Not Available Inactive Unknown Unknown
WSW-12 2624 Mission Road Not Available Inactive Unknown Unknown 1,040 Well not in use; pump removed; well house used for
storage
WSW-11 3968 US Hwy 321A Not Available Inactive Unknown Unknown 1,310 Well not in use; pump removed; well under brick patio
715 Well not in use; house used as rental
WSW-10 4303 Helena Street Not Available Inactive Unknown Unknown 970
WSW-9 4253 Helena Street Not Available Inactive Unknown Unknown
Well not in use
WSW-8 4002 US Hwy 321A 828-612-6653 Inactive ~120 Unknown 535 Well not in use; potential future use for irrigation
WSW-7 4002 US Hwy 321A 828-612-6653 Inactive Unknown Unknown 495 Well not in use; pump removed; well located under
house and filled with dirt and rocks
430 Well not in use
WSW-6 2335 Adams Drive Not Available Inactive Unknown Unknown 430
WSW-5 2347 Adams Drive Not Available Inactive Unknown Unknown
Well not in use
WSW-4 2343 Adams Drive 828-396-1540 Active Unknown Unknown 315 Well used for irrigation only
WSW-3 2339 Adams Drive 828-396-3815 Inactive 28 3-28 255 Well not in use
WSW-2 2342 Adams Drive Not Available Inactive Unknown Unknown 300 Well not in use
Well Screen
Interval
Approx. distance
from source area of
release (ft)Comments
WSW-1 2338 Adams Drive 828-728-9694 Inactive Unknown Unknown
Supply Well ID Property Owner Contact Information Property Address Phone Number Well Use
Well Depth (ft
bgs)
190 Unknown object with significant surface cover resulting
in no access (deemed abandoned by DEQ)
Table B-7: Monitoring Well Construction Information
Revision Date: 9/27/19 Incident Number and Name: 28491/Yogi Foods Facility ID #: 0-007809
Well ID
Date
Installed
Date GW
Measured
Casing
Diameter
(in.)
Casing
Depth (ft)
Screened
Interval
Total
Depth
TOC
Elevation*
Depth to
Water
from TOC
Free Product
Thickness**
Groundwater
Elevation*
Comments
dO (ppm)/pH
8/11/2006 26.82 0.00 67.68 Unknown
8/6/2014 22.27 0.00 72.23 7.44/4.94
3/24/2016 19.32 0.00 75.18 Not Recorded
11/2/2016 24.46 0.00 70.04 2.79/4.28
4/20/2017 26.40 0.00 68.10 Not Recorded
11/16/2017 23.30 0.00 71.20 2.93/4.73
4/13/2018 22.42 0.00 72.08 5.47/3.13
4/18/2019 17.94 0.00 76.56 Not Recorded
7/30/2019 18.37 0.00 76.13 Not Recorded
8/29/2019 19.13 0.00 75.37 1.20 / 4.89
8/6/2014 23.05 0.00 71.55 2.38/5.44
11/16/2017 23.66 0.00 70.94 2.89/5.06
8/6/2014 22.40 0.00 72.38 1.75/6.07
11/16/2017 23.63 0.00 71.15 3.96/5.34
8/6/2014 15.55 0.00 71.47 1.70/5.98
11/16/2017 16.13 0.00 70.89 1.64/6.29
11/2/2016 24.19 0.00 70.06 2.71/3.92
4/20/2017 26.03 0.00 68.22 1.27/5.06
11/16/2017 22.91 0.00 71.34 1.71/4.40
4/13/2018 22.50 0.00 71.75 4.51/3.08
4/18/2019 17.63 0.00 76.62 0.53/4.51
7/30/2019 18.12 0.00 76.13 Not Sampled
8/29/2019 18.84 0.00 75.41 1.03 / 4.73
** If free product is present in well, groundwater elevation is calculated by [Top of Casing Elevation-Depth to Water]+[free product thickness x 0.8581]
TOC = Top of Casing
* All measurements are feet Below Ground Surface (ft. BGS).
NS = Not Surveyed
30 94.25
94.502813-28
MW-5 8/23/2016 4 15 15-30
MW-1 8/10/2006 131
30 94.78
MW-4 8/5/2014 2 15 15-30 30 87.02
MW-3 8/5/2014 2 15 15-30
30 94.60MW-2 8/5/2014 2 15 15-30
Table B-8: Free Product Recovery Information
Revision Date: 9/27/17 Incident Number and Name: 28491/Yogi Foods Facility ID #: 0-007809
Date Recovery Well ID
Product
Type
Free
Product
Recovery
Method
Product
Thickness
before
Recovery
(feet)
Product
Thickness
after
Recovery
(feet)
Volume of
Vaporized
Product
(gallons)
Volume of
Liquid (Water
and Product)
(gallons)
Volume of
Liquid
Product
(gallons)
Total Volume
of Product
Recovered
(gallons)
1/26/2016 MW-1 Gasoline AFVR 0 0 1.18 175 0 1.18
2/26/2016 MW-1 Gasoline AFVR 0 0 1.31 75 0 1.31
10/6/2016 MW-5 Gasoline AFVR 0 0 6.92 353 0 6.92
3/23/2017 MW-5 Gasoline AFVR 0 0 7.20 188 0 7.20
7/30/2019 MW-5 Gasoline AFVR 0 0 8.69 278 0 8.69
Totals:25.3 1,069 0 25.30

FIGURES
CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
TITLE
DATE
SITE
DIR
T

R
O
A
D
DISPENSER
CANOPY
STORE
STORE
UST
BASIN
GRASS
ASPHALT
CONCRETE
GRASS
MW-1
MW-2
MW-3
MW-4
KEROSENE
DISPENSER
KEROSENE
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W
W
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W
W
W
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W
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W
W
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E ELECTRIC LINE
W WATER LINE
TELEPHONE/TV LINE
S SEWER LINE
CATHODIC PROTECTION
PRODUCT PIPING
DIR
T

R
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A
D
STORE
STORE
UST
BASIN
GRASS
ASPHALT
CONCRETE
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MW-3
MW-4
KEROSENE
DISPENSER
KEROSENE
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W
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W
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W
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W
W
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W WATER LINE
TELEPHONE/TV LINE
S SEWER LINE
CATHODIC PROTECTION
PRODUCT PIPING
CO
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DISPENSER
CANOPY
MW-1

APPENDIX A

AFVR DATA
Site: Yogi Foods, 4018 Highway 321A, Hudson, NC Date: August 30, 2019
8:45 30 NA
9:15 30 NA
9:45 30 NA
10:15 30 NA
10:45 30 NA
11:45 60 NA
12:45 60 NA
13:45 60 NA
14:45 60 NA
15:45 60 NA
16:45 60 NA
PPMmea = Measured VOC concentration from OVA/TVA (PPMv)Total emissions, pounds
Velocity = Measured velocity (fpm)Total emissions, gallons (6.25 lb/gal)
Temp = Measured temperature (0F)
RH = Measured relative humidity (%) - Not Recorded
Flow = Actual Flow Volume (cfm)
Specific Humidity = data from psychrometric chart at measured Temp and RH (lb water/lb dry air) (lbW / lbDA)
Water Vapor = % water vapor on a volume basis = (Specific Humidity / 18 lb-mole H2O) / [(1 / 28.84 lb-mole dry air) + (Specific Humidity / 18 lb-mole H2O)]
Qstd = Flow volume on a dry basis at a standard temperature of 680 F = (1-Water Vapor) (Flow) [528 0R / (Temp +460)]
Dry Conc = PPMv VOC on a dry basis = [PPMmea / (1-Water Vapor)]
Response Factor of OVA/TVA meter; 1 if response factor is unknown
Corrected Conc = Dry Conc PPMv VOC corrected by Response Factor = (Dry Conc) (Response Factor)
Mass Conc (mg/m3) = Mass concentration VOC as gasoline dry basis at standard temperature = (Corrected Conc) (128 mg/mg-mole / 24.07 m3/mg-mole)
Mass Conc (lb/ft3) = [Mass Conc (mg/m3)] [(6.243 * 10-8)(lb/ft3)/(mg/m3)]
Mass Removed (lb) = [Mass Conc (lb/ft3)] [Qstd (dscfm)] [Time Interval (min)]
1211 0.000076
Response
Factor
Dry
Conc
(PPMv)
Temp
(0 F)
RH
(%)
Specific
Humidity
(lbW / lbDA)
Mass Conc
(mg/m3)
196.3 43.9/138.1 218.0 --2280.138
Corrected
Conc
(PPMv)
0.100
0.100
1 2281800
1
1
278
1208
1800
0.138
AFVR Data Sheet - Emissions Data & Calculation
Water
Vapor
(vol %)
Qstd
(dscfm)
PPMmea
(PPMv)
Pre-
carbon
Velocity
(fpm)
Flow
(cfm)
PPMmea
(PPMv)
Post
carbon
Mass
Removed
(lb)
1800
0.100
0.100
0.100
0.100
0.1001800
1800
1800
1800
1124
1125
1800
277
0.138
286
2830.138 1
1
1
1
245.1
254.1
247.6
248.2
243.1
259.8
239.9
239.0
--
--
266.0
269.0
50.1/176.6
105.2/176.3
106.7/171.8
111.1/168.2
103.2/144.3
266.0
104.3/139.6
107.2/143.5
238.0
246.0
258.0
264.0
105.2/139.4
--
269.0
--
--
--
--
269.0
--
1800
--
0.138
0.100
1128
1128
0.100
0.138
0.138
0.138
0.138
0.138
1174
1160
1141
1131
1124
1124
0.138
282
1
1
1
287
282
0.000095 3.32
284
301
1568
1528
1531
1500
1
3.27
Mass Conc
(lb/ft3)
3.450.000098
2.74
1800
1800
0.100
0.100268.0 --
88.9/136.2
87.1/103.8
246.1
243.6
288 0.000096
1518 0.000095
301 0.000100
0.000094 3.18
278 0.000092 6.261480
6.39
277 0.000092 6.231475
284 0.000094 6.371512
286
6.751603
283 1503 0.000094 6.33
8.69
54.28
Time (hh:mm)
De
l
t
a

T
i
m
e
(m
i
n
)
295295
287
288

APPENDIX B

LABORATORY ANALYTICAL REPORT

#=CL#
August 07, 2019
LIMS USE: FR - ERIN GREENE
LIMS OBJECT ID: 92439219
92439219
Project:
Pace Project No.:
RE:
Erin Greene
ATC Group
7606 Whitehall Executive Cente
Suite 800
Charlotte, NC 28273
YOGI FOODS
Dear Erin Greene:
Enclosed are the analytical results for sample(s) received by the laboratory on July 31, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 17
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92439219
YOGI FOODS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 17
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92439219
YOGI FOODS
Lab ID Sample ID Matrix Date Collected Date Received
92439219001 MW-1 Water 07/30/19 08:30 07/31/19 08:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 17
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92439219
YOGI FOODS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92439219001 MW-1 EPA 504.1 2 PASI-CBAJ
SM 6200B 66 PASI-CCL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439219
YOGI FOODS
Sample:MW-1 Lab ID:92439219001 Collected:07/30/19 08:30 Received:07/31/19 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)953 ug/L 08/06/19 13:08 106-93-408/05/19 10:2338.5 21.3 2000
Surrogates
1-Chloro-2-bromopropane (S)0 %08/06/19 13:08 301-79-56 S408/05/19 10:2370-130 2000
Analytical Method: SM 6200B6200B MSV
Benzene 11400 ug/L 08/06/19 01:21 71-43-210050.0 200
Bromobenzene ND ug/L 08/06/19 01:21 108-86-110050.0 200
Bromochloromethane ND ug/L 08/06/19 01:21 74-97-510050.0 200
Bromodichloromethane ND ug/L 08/06/19 01:21 75-27-410050.0 200
Bromoform ND ug/L 08/06/19 01:21 75-25-210050.0 200
Bromomethane ND ug/L 08/06/19 01:21 74-83-91000500200
2-Butanone (MEK)ND ug/L 08/06/19 01:21 78-93-310001000200
n-Butylbenzene ND ug/L 08/06/19 01:21 104-51-810050.0 200
sec-Butylbenzene ND ug/L 08/06/19 01:21 135-98-810050.0 200
tert-Butylbenzene ND ug/L 08/06/19 01:21 98-06-610050.0 200
Carbon tetrachloride ND ug/L 08/06/19 01:21 56-23-510050.0 200
Chlorobenzene ND ug/L 08/06/19 01:21 108-90-710050.0 200
Chloroethane ND ug/L 08/06/19 01:21 75-00-3200100200
Chloroform ND ug/L 08/06/19 01:21 67-66-31000500200
Chloromethane ND ug/L 08/06/19 01:21 74-87-3200100200
2-Chlorotoluene ND ug/L 08/06/19 01:21 95-49-810050.0 200
4-Chlorotoluene ND ug/L 08/06/19 01:21 106-43-410050.0 200
1,2-Dibromo-3-chloropropane ND ug/L 08/06/19 01:21 96-12-8200100200
Dibromochloromethane ND ug/L 08/06/19 01:21 124-48-110050.0 200
1,2-Dibromoethane (EDB)879 ug/L 08/06/19 01:21 106-93-410050.0 200
Dibromomethane ND ug/L 08/06/19 01:21 74-95-310050.0 200
1,2-Dichlorobenzene ND ug/L 08/06/19 01:21 95-50-110050.0 200
1,3-Dichlorobenzene ND ug/L 08/06/19 01:21 541-73-110050.0 200
1,4-Dichlorobenzene ND ug/L 08/06/19 01:21 106-46-710050.0 200
Dichlorodifluoromethane ND ug/L 08/06/19 01:21 75-71-810050.0 200
1,1-Dichloroethane ND ug/L 08/06/19 01:21 75-34-310050.0 200
1,2-Dichloroethane 510 ug/L 08/06/19 01:21 107-06-210050.0 200
1,1-Dichloroethene ND ug/L 08/06/19 01:21 75-35-410050.0 200
cis-1,2-Dichloroethene ND ug/L 08/06/19 01:21 156-59-210050.0 200
trans-1,2-Dichloroethene ND ug/L 08/06/19 01:21 156-60-510050.0 200
1,2-Dichloropropane ND ug/L 08/06/19 01:21 78-87-510050.0 200
1,3-Dichloropropane ND ug/L 08/06/19 01:21 142-28-910050.0 200
2,2-Dichloropropane ND ug/L 08/06/19 01:21 594-20-710050.0 200
1,1-Dichloropropene ND ug/L 08/06/19 01:21 563-58-610050.0 200
cis-1,3-Dichloropropene ND ug/L 08/06/19 01:21 10061-01-510050.0 200
trans-1,3-Dichloropropene ND ug/L 08/06/19 01:21 10061-02-610050.0 200
Diisopropyl ether 105 ug/L 08/06/19 01:21 108-20-310050.0 200
Ethylbenzene 849 ug/L 08/06/19 01:21 100-41-410050.0 200
Hexachloro-1,3-butadiene ND ug/L 08/06/19 01:21 87-68-3400200200
2-Hexanone ND ug/L 08/06/19 01:21 591-78-610001000200
Isopropylbenzene (Cumene)92.4J ug/L 08/06/19 01:21 98-82-810050.0 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/07/2019 12:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439219
YOGI FOODS
Sample:MW-1 Lab ID:92439219001 Collected:07/30/19 08:30 Received:07/31/19 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Methylene Chloride ND ug/L 08/06/19 01:21 75-09-2400200200
Methyl-tert-butyl ether ND ug/L 08/06/19 01:21 1634-04-410050.0 200
Naphthalene 594 ug/L 08/06/19 01:21 91-20-3400200200
n-Propylbenzene 179 ug/L 08/06/19 01:21 103-65-110050.0 200
Styrene ND ug/L 08/06/19 01:21 100-42-510050.0 200
1,1,1,2-Tetrachloroethane ND ug/L 08/06/19 01:21 630-20-610050.0 200
1,1,2,2-Tetrachloroethane ND ug/L 08/06/19 01:21 79-34-510050.0 200
Tetrachloroethene ND ug/L 08/06/19 01:21 127-18-410050.0 200
Toluene 28100 ug/L 08/06/19 01:21 108-88-310050.0 200
1,2,3-Trichlorobenzene ND ug/L 08/06/19 01:21 87-61-6400200200
1,2,4-Trichlorobenzene ND ug/L 08/06/19 01:21 120-82-1400200200
1,1,1-Trichloroethane ND ug/L 08/06/19 01:21 71-55-610050.0 200
1,1,2-Trichloroethane ND ug/L 08/06/19 01:21 79-00-510050.0 200
Trichloroethene ND ug/L 08/06/19 01:21 79-01-610050.0 200
Trichlorofluoromethane ND ug/L 08/06/19 01:21 75-69-4200100200
1,2,3-Trichloropropane ND ug/L 08/06/19 01:21 96-18-410050.0 200
1,2,4-Trimethylbenzene 2460 ug/L 08/06/19 01:21 95-63-610050.0 200
1,3,5-Trimethylbenzene 611 ug/L 08/06/19 01:21 108-67-810050.0 200
Vinyl chloride ND ug/L 08/06/19 01:21 75-01-4200100200
Xylene (Total)11700 ug/L 08/06/19 01:21 1330-20-7200100200
m&p-Xylene 7150 ug/L 08/06/19 01:21 179601-23-1200100200
o-Xylene 4520 ug/L 08/06/19 01:21 95-47-610050.0 200
Surrogates
1,2-Dichloroethane-d4 (S)97 %08/06/19 01:21 17060-07-070-130 200
4-Bromofluorobenzene (S)99 %08/06/19 01:21 460-00-470-130 200
Toluene-d8 (S)99 %08/06/19 01:21 2037-26-570-130 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/07/2019 12:24 PM
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Huntersville, NC 28078
[phone]
Page 6 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439219
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
490366
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92439219001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2645561
Associated Lab Samples:92439219001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/05/19 15:420.25
1,1,1-Trichloroethane ug/L ND 0.50 08/05/19 15:420.25
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/05/19 15:420.25
1,1,2-Trichloroethane ug/L ND 0.50 08/05/19 15:420.25
1,1-Dichloroethane ug/L ND 0.50 08/05/19 15:420.25
1,1-Dichloroethene ug/L ND 0.50 08/05/19 15:420.25
1,1-Dichloropropene ug/L ND 0.50 08/05/19 15:420.25
1,2,3-Trichlorobenzene ug/L ND 2.0 08/05/19 15:421.0
1,2,3-Trichloropropane ug/L ND 0.50 08/05/19 15:420.25
1,2,4-Trichlorobenzene ug/L ND 2.0 08/05/19 15:421.0
1,2,4-Trimethylbenzene ug/L ND 0.50 08/05/19 15:420.25
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/05/19 15:420.50
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/05/19 15:420.25
1,2-Dichlorobenzene ug/L ND 0.50 08/05/19 15:420.25
1,2-Dichloroethane ug/L ND 0.50 08/05/19 15:420.25
1,2-Dichloropropane ug/L ND 0.50 08/05/19 15:420.25
1,3,5-Trimethylbenzene ug/L ND 0.50 08/05/19 15:420.25
1,3-Dichlorobenzene ug/L ND 0.50 08/05/19 15:420.25
1,3-Dichloropropane ug/L ND 0.50 08/05/19 15:420.25
1,4-Dichlorobenzene ug/L ND 0.50 08/05/19 15:420.25
2,2-Dichloropropane ug/L ND 0.50 08/05/19 15:420.25
2-Butanone (MEK)ug/L ND 5.0 08/05/19 15:425.0
2-Chlorotoluene ug/L ND 0.50 08/05/19 15:420.25
2-Hexanone ug/L ND 5.0 08/05/19 15:425.0
4-Chlorotoluene ug/L ND 0.50 08/05/19 15:420.25
Benzene ug/L ND 0.50 08/05/19 15:420.25
Bromobenzene ug/L ND 0.50 08/05/19 15:420.25
Bromochloromethane ug/L ND 0.50 08/05/19 15:420.25
Bromodichloromethane ug/L ND 0.50 08/05/19 15:420.25
Bromoform ug/L ND 0.50 08/05/19 15:420.25
Bromomethane ug/L ND 5.0 08/05/19 15:422.5
Carbon tetrachloride ug/L ND 0.50 08/05/19 15:420.25
Chlorobenzene ug/L ND 0.50 08/05/19 15:420.25
Chloroethane ug/L ND 1.0 08/05/19 15:420.50
Chloroform ug/L ND 5.0 08/05/19 15:422.5
Chloromethane ug/L ND 1.0 08/05/19 15:420.50
cis-1,2-Dichloroethene ug/L ND 0.50 08/05/19 15:420.25
cis-1,3-Dichloropropene ug/L ND 0.50 08/05/19 15:420.25
Dibromochloromethane ug/L ND 0.50 08/05/19 15:420.25
Dibromomethane ug/L ND 0.50 08/05/19 15:420.25
Dichlorodifluoromethane ug/L ND 0.50 08/05/19 15:420.25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/07/2019 12:24 PM
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Page 7 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439219
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2645561
Associated Lab Samples:92439219001
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 0.50 08/05/19 15:420.25
Ethylbenzene ug/L ND 0.50 08/05/19 15:420.25
Hexachloro-1,3-butadiene ug/L ND 2.0 08/05/19 15:421.0
Isopropylbenzene (Cumene)ug/L ND 0.50 08/05/19 15:420.25
m&p-Xylene ug/L ND 1.0 08/05/19 15:420.50
Methyl-tert-butyl ether ug/L ND 0.50 08/05/19 15:420.25
Methylene Chloride ug/L ND 2.0 08/05/19 15:421.0
n-Butylbenzene ug/L ND 0.50 08/05/19 15:420.25
n-Propylbenzene ug/L ND 0.50 08/05/19 15:420.25
Naphthalene ug/L ND 2.0 08/05/19 15:421.0
o-Xylene ug/L ND 0.50 08/05/19 15:420.25
sec-Butylbenzene ug/L ND 0.50 08/05/19 15:420.25
Styrene ug/L ND 0.50 08/05/19 15:420.25
tert-Butylbenzene ug/L ND 0.50 08/05/19 15:420.25
Tetrachloroethene ug/L ND 0.50 08/05/19 15:420.25
Toluene ug/L ND 0.50 08/05/19 15:420.25
trans-1,2-Dichloroethene ug/L ND 0.50 08/05/19 15:420.25
trans-1,3-Dichloropropene ug/L ND 0.50 08/05/19 15:420.25
Trichloroethene ug/L ND 0.50 08/05/19 15:420.25
Trichlorofluoromethane ug/L ND 1.0 08/05/19 15:420.50
Vinyl chloride ug/L ND 1.0 08/05/19 15:420.50
Xylene (Total)ug/L ND 1.0 08/05/19 15:420.50
1,2-Dichloroethane-d4 (S)%98 70-130 08/05/19 15:42
4-Bromofluorobenzene (S)%96 70-130 08/05/19 15:42
Toluene-d8 (S)%98 70-130 08/05/19 15:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2645562LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.450 99 60-140
1,1,1-Trichloroethane ug/L 50.050 100 60-140
1,1,2,2-Tetrachloroethane ug/L 48.750 97 60-140
1,1,2-Trichloroethane ug/L 51.950 104 60-140
1,1-Dichloroethane ug/L 47.950 96 60-140
1,1-Dichloroethene ug/L 49.650 99 60-140
1,1-Dichloropropene ug/L 51.450 103 60-140
1,2,3-Trichlorobenzene ug/L 59.450 119 60-140
1,2,3-Trichloropropane ug/L 48.950 98 60-140
1,2,4-Trichlorobenzene ug/L 52.950 106 60-140
1,2,4-Trimethylbenzene ug/L 45.550 91 60-140
1,2-Dibromo-3-chloropropane ug/L 57.050 114 60-140
1,2-Dibromoethane (EDB)ug/L 50.850 102 60-140
1,2-Dichlorobenzene ug/L 47.050 94 60-140
1,2-Dichloroethane ug/L 52.150 104 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/07/2019 12:24 PM
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[phone]
Page 8 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439219
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2645562LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 48.550 97 60-140
1,3,5-Trimethylbenzene ug/L 45.750 91 60-140
1,3-Dichlorobenzene ug/L 46.450 93 60-140
1,3-Dichloropropane ug/L 49.250 98 60-140
1,4-Dichlorobenzene ug/L 46.150 92 60-140
2,2-Dichloropropane ug/L 49.650 99 60-140
2-Butanone (MEK)ug/L 101100 101 60-140
2-Chlorotoluene ug/L 44.350 89 60-140
2-Hexanone ug/L 99.6100 100 60-140
4-Chlorotoluene ug/L 45.750 91 60-140
Benzene ug/L 48.850 98 60-140
Bromobenzene ug/L 47.450 95 60-140
Bromochloromethane ug/L 50.250 100 60-140
Bromodichloromethane ug/L 53.450 107 60-140
Bromoform ug/L 55.750 111 60-140
Bromomethane ug/L 47.050 94 60-140
Carbon tetrachloride ug/L 48.550 97 60-140
Chlorobenzene ug/L 46.050 92 60-140
Chloroethane ug/L 48.150 96 60-140
Chloroform ug/L 46.750 93 60-140
Chloromethane ug/L 57.250 114 60-140
cis-1,2-Dichloroethene ug/L 47.150 94 60-140
cis-1,3-Dichloropropene ug/L 53.750 107 60-140
Dibromochloromethane ug/L 51.750 103 60-140
Dibromomethane ug/L 54.450 109 60-140
Dichlorodifluoromethane ug/L 55.750 111 60-140
Diisopropyl ether ug/L 49.450 99 60-140
Ethylbenzene ug/L 46.650 93 60-140
Hexachloro-1,3-butadiene ug/L 48.150 96 60-140
Isopropylbenzene (Cumene)ug/L 47.150 94 60-140
m&p-Xylene ug/L 94.2100 94 60-140
Methyl-tert-butyl ether ug/L 50.250 100 60-140
Methylene Chloride ug/L 45.850 92 60-140
n-Butylbenzene ug/L 44.150 88 60-140
n-Propylbenzene ug/L 45.550 91 60-140
Naphthalene ug/L 56.650 113 60-140
o-Xylene ug/L 47.550 95 60-140
sec-Butylbenzene ug/L 47.050 94 60-140
Styrene ug/L 47.950 96 60-140
tert-Butylbenzene ug/L 40.150 80 60-140
Tetrachloroethene ug/L 48.550 97 60-140
Toluene ug/L 46.150 92 60-140
trans-1,2-Dichloroethene ug/L 48.450 97 60-140
trans-1,3-Dichloropropene ug/L 54.250 108 60-140
Trichloroethene ug/L 48.750 97 60-140
Trichlorofluoromethane ug/L 52.350 105 60-140
Vinyl chloride ug/L 56.050 112 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/07/2019 12:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439219
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2645562LABORATORY CONTROL SAMPLE:
LCSSpike
Xylene (Total)ug/L 142150 94 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2645563MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92439127002
2645564
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 100 91 60-140106 15 30100ND91.4 106
1,1,1-Trichloroethane ug/L 100 97 60-140114 16 30100ND97.1 114
1,1,2,2-Tetrachloroethane ug/L 100 91 60-140103 13 30100ND90.7 103
1,1,2-Trichloroethane ug/L 100 96 60-140108 11 30100ND96.3 108
1,1-Dichloroethane ug/L 100 97 60-140109 12 30100ND96.9 109
1,1-Dichloroethene ug/L 100 102 60-140115 12 30100ND102115
1,1-Dichloropropene ug/L 100 104 60-140117 12 30100ND104117
1,2,3-Trichlorobenzene ug/L 100 78 60-140106 30 30100ND78.1 106
1,2,3-Trichloropropane ug/L 100 88 60-140108 20 30100ND88.1 108
1,2,4-Trichlorobenzene ug/L 100 85 60-140101 17 30100ND85.1 101
1,2,4-Trimethylbenzene ug/L M11006060-14037 4 30100585645622
1,2-Dibromo-3-
chloropropane ug/L 100 89 60-140108 19 30100ND88.7 108
1,2-Dibromoethane (EDB)ug/L 100 90 60-140104 14 30100ND89.7 104
1,2-Dichlorobenzene ug/L 100 86 60-14098 13 30100ND85.9 98.3
1,2-Dichloroethane ug/L 100 99 60-140115 15 30100ND98.5 115
1,2-Dichloropropane ug/L 100 94 60-140101 7 30100ND94.4 101
1,3,5-Trimethylbenzene ug/L M110020360-140205 1 30100ND203205
1,3-Dichlorobenzene ug/L 100 86 60-14098 14 30100ND85.6 98.4
1,3-Dichloropropane ug/L 100 92 60-140103 11 30100ND91.7 103
1,4-Dichlorobenzene ug/L 100 85 60-14099 15 30100ND85.3 98.6
2,2-Dichloropropane ug/L 100 83 60-14096 15 30100ND82.7 96.2
2-Butanone (MEK)ug/L 200 96 60-140108 12 30200ND192216
2-Chlorotoluene ug/L 100 91 60-140104 14 30100ND91.1 104
2-Hexanone ug/L 200 88 60-140104 16 30200ND176208
4-Chlorotoluene ug/L 100 86 60-14096 11 30100ND85.6 95.5
Benzene ug/L 100 95 60-140106 9 3010018.3 113 124
Bromobenzene ug/L 100 88 60-14099 12 30100ND87.8 98.6
Bromochloromethane ug/L 100 96 60-140109 13 30100ND95.9 109
Bromodichloromethane ug/L 100 98 60-140111 13 30100ND97.8 111
Bromoform ug/L 100 91 60-140109 18 30100ND91.1 109
Bromomethane ug/L 100 78 60-140105 29 30100ND78.3 105
Carbon tetrachloride ug/L 100 96 60-140108 12 30100ND95.7 108
Chlorobenzene ug/L 100 88 60-140102 15 30100ND88.2 102
Chloroethane ug/L 100 119 60-140132 10 30100ND119132
Chloroform ug/L 100 95 60-140107 11 30100ND95.3 107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/07/2019 12:24 PM
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Page 10 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439219
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2645563MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92439127002
2645564
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloromethane ug/L 100 102 60-140115 12 30100ND102115
cis-1,2-Dichloroethene ug/L 100 95 60-140108 13 30100ND94.9 108
cis-1,3-Dichloropropene ug/L 100 98 60-140110 11 30100ND98.4 110
Dibromochloromethane ug/L 100 89 60-140106 17 30100ND89.2 106
Dibromomethane ug/L 100 106 60-140118 11 30100ND106118
Dichlorodifluoromethane ug/L 100 98 60-140110 12 30100ND97.9 110
Diisopropyl ether ug/L 100 93 60-140108 13 3010011.2 104 119
Ethylbenzene ug/L 100 88 60-14066 4 30100436524503
Hexachloro-1,3-butadiene ug/L 100 87 60-14091 4 30100ND87.4 91.1
Isopropylbenzene
(Cumene)
ug/L 100 92 60-140103 9 3010020.9 113 124
m&p-Xylene ug/L M12007960-14046 5 30200124014001330
Methyl-tert-butyl ether ug/L 100 93 60-140108 15 30100ND92.8 108
Methylene Chloride ug/L 100 95 60-140107 12 30100ND95.2 107
n-Butylbenzene ug/L 100 91 60-140103 12 30100ND91.0 103
n-Propylbenzene ug/L M110015360-140159 4 30100ND153159
Naphthalene ug/L 100 76 60-140105 15 3010098.4 174 203
o-Xylene ug/L 100 80 60-14075 1 30100368448442
sec-Butylbenzene ug/L 100 96 60-140103 8 30100ND95.5 103
Styrene ug/L 100 93 60-140108 15 30100ND93.4 108
tert-Butylbenzene ug/L 100 78 60-14088 12 30100ND77.9 87.5
Tetrachloroethene ug/L 100 93 60-140106 14 30100ND92.5 106
Toluene ug/L 100 96 60-140100 2 3010087.3 183 187
trans-1,2-Dichloroethene ug/L 100 99 60-140111 12 30100ND98.7 111
trans-1,3-Dichloropropene ug/L 100 98 60-140109 11 30100ND97.8 109
Trichloroethene ug/L 100 94 60-140104 10 30100ND94.3 104
Trichlorofluoromethane ug/L 100 111 60-140128 14 30100ND111128
Vinyl chloride ug/L 100 111 60-140128 14 30100ND111128
Xylene (Total)ug/L MS3008060-14056 4 30300161018401770
1,2-Dichloroethane-d4 (S)%96 70-13096
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%101 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/07/2019 12:24 PM
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[phone]
Page 11 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439219
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
490318
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Associated Lab Samples:92439219001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2645088
Associated Lab Samples:92439219001
Matrix:Water
AnalyzedMDL
1,2-Dibromoethane (EDB)ug/L ND 0.020 08/05/19 16:040.011
1-Chloro-2-bromopropane (S)%96 70-130 08/05/19 16:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2645089LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2645090
1,2-Dibromoethane (EDB)ug/L 0.230.25 95 70-130980.25 6 20
1-Chloro-2-bromopropane (S)%91 70-13094
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2645092MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92439394004
2645093
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dibromoethane (EDB)ug/L 0.25 103 65-135104 1 200.25ND 0.26 0.26
1-Chloro-2-bromopropane
(S)
%98 70-13098
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 12 of 17
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92439219
YOGI FOODS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/07/2019 12:24 PM
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Page 13 of 17
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92439219
YOGI FOODS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92439219001 490318 490414MW-1 EPA 504.1 EPA 504.1
92439219001 490366MW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/07/2019 12:24 PM
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9800 Kincey Ave. Suite 100
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Page 14 of 17
Page 15 of 17
Page 16 of 17
Page 17 of 17
#=CL#
September 09, 2019
LIMS USE: FR - ERIN GREENE
LIMS OBJECT ID: 92443707
92443707
Project:
Pace Project No.:
RE:
Erin Greene
ATC Group
7606 Whitehall Executive Cente
Suite 800
Charlotte, NC 28273
YOGI FOODS
Dear Erin Greene:
Enclosed are the analytical results for sample(s) received by the laboratory on August 30, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 24
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92443707
YOGI FOODS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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[phone]
Page 2 of 24
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92443707
YOGI FOODS
Lab ID Sample ID Matrix Date Collected Date Received
92443707001 MW-1 Water 08/29/19 13:58 08/30/19 11:00
92443707002 MW-5 Water 08/29/19 14:47 08/30/19 11:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Page 3 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92443707
YOGI FOODS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92443707001 MW-1 EPA 504.1 2 PASI-CBAJ
SM 6200B 66 PASI-CSAS
92443707002 MW-5 EPA 504.1 2 PASI-CBAJ
SM 6200B 66 PASI-CSAS
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 4 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92443707
YOGI FOODS
Sample:MW-1 Lab ID:92443707001 Collected:08/29/19 13:58 Received:08/30/19 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)193 ug/L 09/09/19 14:22 106-93-409/09/19 10:217.9 4.4 400
Surrogates
1-Chloro-2-bromopropane (S)0 %09/09/19 14:22 301-79-56 S409/09/19 10:2170-130 400
Analytical Method: SM 6200B6200B MSV
Benzene 3990 ug/L 09/06/19 12:23 71-43-250.0 25.0 100
Bromobenzene ND ug/L 09/06/19 12:23 108-86-150.0 25.0 100
Bromochloromethane ND ug/L 09/06/19 12:23 74-97-550.0 25.0 100
Bromodichloromethane ND ug/L 09/06/19 12:23 75-27-450.0 25.0 100
Bromoform ND ug/L 09/06/19 12:23 75-25-250.0 25.0 100
Bromomethane ND ug/L 09/06/19 12:23 74-83-9500250100
2-Butanone (MEK)ND ug/L 09/06/19 12:23 78-93-3500500100
n-Butylbenzene ND ug/L 09/06/19 12:23 104-51-850.0 25.0 100
sec-Butylbenzene ND ug/L 09/06/19 12:23 135-98-850.0 25.0 100
tert-Butylbenzene ND ug/L 09/06/19 12:23 98-06-650.0 25.0 100
Carbon tetrachloride ND ug/L 09/06/19 12:23 56-23-550.0 25.0 100
Chlorobenzene ND ug/L 09/06/19 12:23 108-90-750.0 25.0 100
Chloroethane ND ug/L 09/06/19 12:23 75-00-310050.0 100
Chloroform ND ug/L 09/06/19 12:23 67-66-3500250100
Chloromethane ND ug/L 09/06/19 12:23 74-87-310050.0 100
2-Chlorotoluene ND ug/L 09/06/19 12:23 95-49-850.0 25.0 100
4-Chlorotoluene ND ug/L 09/06/19 12:23 106-43-450.0 25.0 100
1,2-Dibromo-3-chloropropane ND ug/L 09/06/19 12:23 96-12-810050.0 100
Dibromochloromethane ND ug/L 09/06/19 12:23 124-48-150.0 25.0 100
1,2-Dibromoethane (EDB)200 ug/L 09/06/19 12:23 106-93-450.0 25.0 100
Dibromomethane ND ug/L 09/06/19 12:23 74-95-350.0 25.0 100
1,2-Dichlorobenzene ND ug/L 09/06/19 12:23 95-50-150.0 25.0 100
1,3-Dichlorobenzene ND ug/L 09/06/19 12:23 541-73-150.0 25.0 100
1,4-Dichlorobenzene ND ug/L 09/06/19 12:23 106-46-750.0 25.0 100
Dichlorodifluoromethane ND ug/L 09/06/19 12:23 75-71-850.0 25.0 100
1,1-Dichloroethane ND ug/L 09/06/19 12:23 75-34-350.0 25.0 100
1,2-Dichloroethane 111 ug/L 09/06/19 12:23 107-06-250.0 25.0 100
1,1-Dichloroethene ND ug/L 09/06/19 12:23 75-35-450.0 25.0 100
cis-1,2-Dichloroethene ND ug/L 09/06/19 12:23 156-59-250.0 25.0 100
trans-1,2-Dichloroethene ND ug/L 09/06/19 12:23 156-60-550.0 25.0 100
1,2-Dichloropropane ND ug/L 09/06/19 12:23 78-87-550.0 25.0 100
1,3-Dichloropropane ND ug/L 09/06/19 12:23 142-28-950.0 25.0 100
2,2-Dichloropropane ND ug/L 09/06/19 12:23 594-20-750.0 25.0 100
1,1-Dichloropropene ND ug/L 09/06/19 12:23 563-58-650.0 25.0 100
cis-1,3-Dichloropropene ND ug/L 09/06/19 12:23 10061-01-550.0 25.0 100
trans-1,3-Dichloropropene ND ug/L 09/06/19 12:23 10061-02-650.0 25.0 100
Diisopropyl ether 26.2J ug/L 09/06/19 12:23 108-20-350.0 25.0 100
Ethylbenzene 731 ug/L 09/06/19 12:23 100-41-450.0 25.0 100
Hexachloro-1,3-butadiene ND ug/L 09/06/19 12:23 87-68-3200100100
2-Hexanone ND ug/L 09/06/19 12:23 591-78-6500500100
Isopropylbenzene (Cumene)57.4 ug/L 09/06/19 12:23 98-82-850.0 25.0 100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
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Page 5 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92443707
YOGI FOODS
Sample:MW-1 Lab ID:92443707001 Collected:08/29/19 13:58 Received:08/30/19 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Methylene Chloride ND ug/L 09/06/19 12:23 75-09-2200100100
Methyl-tert-butyl ether ND ug/L 09/06/19 12:23 1634-04-450.0 25.0 100
Naphthalene 449 ug/L 09/06/19 12:23 91-20-3200100100
n-Propylbenzene ND ug/L 09/06/19 12:23 103-65-150.0 25.0 100
Styrene ND ug/L 09/06/19 12:23 100-42-550.0 25.0 100
1,1,1,2-Tetrachloroethane ND ug/L 09/06/19 12:23 630-20-650.0 25.0 100
1,1,2,2-Tetrachloroethane ND ug/L 09/06/19 12:23 79-34-550.0 25.0 100
Tetrachloroethene ND ug/L 09/06/19 12:23 127-18-450.0 25.0 100
Toluene 13200 ug/L 09/06/19 12:23 108-88-350.0 25.0 100
1,2,3-Trichlorobenzene ND ug/L 09/06/19 12:23 87-61-6200100100
1,2,4-Trichlorobenzene ND ug/L 09/06/19 12:23 120-82-1200100100
1,1,1-Trichloroethane ND ug/L 09/06/19 12:23 71-55-650.0 25.0 100
1,1,2-Trichloroethane ND ug/L 09/06/19 12:23 79-00-550.0 25.0 100
Trichloroethene ND ug/L 09/06/19 12:23 79-01-650.0 25.0 100
Trichlorofluoromethane ND ug/L 09/06/19 12:23 75-69-410050.0 100
1,2,3-Trichloropropane ND ug/L 09/06/19 12:23 96-18-450.0 25.0 100
1,2,4-Trimethylbenzene 1470 ug/L 09/06/19 12:23 95-63-650.0 25.0 100
1,3,5-Trimethylbenzene ND ug/L 09/06/19 12:23 108-67-850.0 25.0 100
Vinyl chloride ND ug/L 09/06/19 12:23 75-01-410050.0 100
Xylene (Total)6430 ug/L 09/06/19 12:23 1330-20-710050.0 100
m&p-Xylene 4080 ug/L 09/06/19 12:23 179601-23-110050.0 100
o-Xylene 2350 ug/L 09/06/19 12:23 95-47-650.0 25.0 100
Surrogates
1,2-Dichloroethane-d4 (S)79 %09/06/19 12:23 17060-07-070-130 100
4-Bromofluorobenzene (S)96 %09/06/19 12:23 460-00-470-130 100
Toluene-d8 (S)101 %09/06/19 12:23 2037-26-570-130 100
Sample:MW-5 Lab ID:92443707002 Collected:08/29/19 14:47 Received:08/30/19 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)4.9 ug/L 09/09/19 14:40 106-93-409/09/19 10:210.20 0.11 10
Surrogates
1-Chloro-2-bromopropane (S)0 %09/09/19 14:40 301-79-56 S409/09/19 10:2170-130 10
Analytical Method: SM 6200B6200B MSV
Benzene 112 ug/L 09/04/19 20:52 71-43-22.0 1.0 4
Bromobenzene ND ug/L 09/04/19 20:52 108-86-12.0 1.0 4
Bromochloromethane ND ug/L 09/04/19 20:52 74-97-52.0 1.0 4
Bromodichloromethane ND ug/L 09/04/19 20:52 75-27-42.0 1.0 4
Bromoform ND ug/L 09/04/19 20:52 75-25-22.0 1.0 4
Bromomethane ND ug/L 09/04/19 20:52 74-83-920.0 10.0 4
2-Butanone (MEK)ND ug/L 09/04/19 20:52 78-93-320.0 20.0 4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
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Page 6 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92443707
YOGI FOODS
Sample:MW-5 Lab ID:92443707002 Collected:08/29/19 14:47 Received:08/30/19 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
n-Butylbenzene ND ug/L 09/04/19 20:52 104-51-82.0 1.0 4
sec-Butylbenzene ND ug/L 09/04/19 20:52 135-98-82.0 1.0 4
tert-Butylbenzene ND ug/L 09/04/19 20:52 98-06-62.0 1.0 4
Carbon tetrachloride ND ug/L 09/04/19 20:52 56-23-52.0 1.0 4
Chlorobenzene ND ug/L 09/04/19 20:52 108-90-72.0 1.0 4
Chloroethane ND ug/L 09/04/19 20:52 75-00-34.0 2.0 4
Chloroform ND ug/L 09/04/19 20:52 67-66-320.0 10.0 4
Chloromethane ND ug/L 09/04/19 20:52 74-87-34.0 2.0 4
2-Chlorotoluene ND ug/L 09/04/19 20:52 95-49-82.0 1.0 4
4-Chlorotoluene ND ug/L 09/04/19 20:52 106-43-42.0 1.0 4
1,2-Dibromo-3-chloropropane ND ug/L 09/04/19 20:52 96-12-84.0 2.0 4
Dibromochloromethane ND ug/L 09/04/19 20:52 124-48-12.0 1.0 4
1,2-Dibromoethane (EDB)5.2 ug/L 09/04/19 20:52 106-93-42.0 1.0 4
Dibromomethane ND ug/L 09/04/19 20:52 74-95-32.0 1.0 4
1,2-Dichlorobenzene ND ug/L 09/04/19 20:52 95-50-12.0 1.0 4
1,3-Dichlorobenzene ND ug/L 09/04/19 20:52 541-73-12.0 1.0 4
1,4-Dichlorobenzene ND ug/L 09/04/19 20:52 106-46-72.0 1.0 4
Dichlorodifluoromethane ND ug/L 09/04/19 20:52 75-71-82.0 1.0 4
1,1-Dichloroethane ND ug/L 09/04/19 20:52 75-34-32.0 1.0 4
1,2-Dichloroethane 3.5 ug/L 09/04/19 20:52 107-06-22.0 1.0 4
1,1-Dichloroethene ND ug/L 09/04/19 20:52 75-35-42.0 1.0 4
cis-1,2-Dichloroethene ND ug/L 09/04/19 20:52 156-59-22.0 1.0 4
trans-1,2-Dichloroethene ND ug/L 09/04/19 20:52 156-60-52.0 1.0 4
1,2-Dichloropropane ND ug/L 09/04/19 20:52 78-87-52.0 1.0 4
1,3-Dichloropropane ND ug/L 09/04/19 20:52 142-28-92.0 1.0 4
2,2-Dichloropropane ND ug/L 09/04/19 20:52 594-20-72.0 1.0 4
1,1-Dichloropropene ND ug/L 09/04/19 20:52 563-58-62.0 1.0 4
cis-1,3-Dichloropropene ND ug/L 09/04/19 20:52 10061-01-52.0 1.0 4
trans-1,3-Dichloropropene ND ug/L 09/04/19 20:52 10061-02-62.0 1.0 4
Diisopropyl ether ND ug/L 09/04/19 20:52 108-20-32.0 1.0 4
Ethylbenzene 30.5 ug/L 09/04/19 20:52 100-41-42.0 1.0 4
Hexachloro-1,3-butadiene ND ug/L 09/04/19 20:52 87-68-38.0 4.0 4
2-Hexanone ND ug/L 09/04/19 20:52 591-78-620.0 20.0 4
Isopropylbenzene (Cumene)5.3 ug/L 09/04/19 20:52 98-82-82.0 1.0 4
Methylene Chloride ND ug/L 09/04/19 20:52 75-09-28.0 4.0 4
Methyl-tert-butyl ether ND ug/L 09/04/19 20:52 1634-04-42.0 1.0 4
Naphthalene 24.2 ug/L 09/04/19 20:52 91-20-38.0 4.0 4
n-Propylbenzene ND ug/L 09/04/19 20:52 103-65-12.0 1.0 4
Styrene ND ug/L 09/04/19 20:52 100-42-52.0 1.0 4
1,1,1,2-Tetrachloroethane ND ug/L 09/04/19 20:52 630-20-62.0 1.0 4
1,1,2,2-Tetrachloroethane ND ug/L 09/04/19 20:52 79-34-52.0 1.0 4
Tetrachloroethene ND ug/L 09/04/19 20:52 127-18-42.0 1.0 4
Toluene 402 ug/L 09/04/19 20:52 108-88-32.0 1.0 4
1,2,3-Trichlorobenzene ND ug/L 09/04/19 20:52 87-61-68.0 4.0 4
1,2,4-Trichlorobenzene ND ug/L 09/04/19 20:52 120-82-18.0 4.0 4
1,1,1-Trichloroethane ND ug/L 09/04/19 20:52 71-55-62.0 1.0 4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
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Huntersville, NC 28078
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Page 7 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92443707
YOGI FOODS
Sample:MW-5 Lab ID:92443707002 Collected:08/29/19 14:47 Received:08/30/19 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
1,1,2-Trichloroethane ND ug/L 09/04/19 20:52 79-00-52.0 1.0 4
Trichloroethene ND ug/L 09/04/19 20:52 79-01-62.0 1.0 4
Trichlorofluoromethane ND ug/L 09/04/19 20:52 75-69-44.0 2.0 4
1,2,3-Trichloropropane ND ug/L 09/04/19 20:52 96-18-42.0 1.0 4
1,2,4-Trimethylbenzene 110 ug/L 09/04/19 20:52 95-63-62.0 1.0 4
1,3,5-Trimethylbenzene ND ug/L 09/04/19 20:52 108-67-82.0 1.0 4
Vinyl chloride ND ug/L 09/04/19 20:52 75-01-44.0 2.0 4
Xylene (Total)312 ug/L 09/04/19 20:52 1330-20-74.0 2.0 4
m&p-Xylene 164 ug/L 09/04/19 20:52 179601-23-14.0 2.0 4
o-Xylene 148 ug/L 09/04/19 20:52 95-47-62.0 1.0 4
Surrogates
1,2-Dichloroethane-d4 (S)81 %09/04/19 20:52 17060-07-070-130 4
4-Bromofluorobenzene (S)100 %09/04/19 20:52 460-00-470-130 4
Toluene-d8 (S)100 %09/04/19 20:52 2037-26-570-130 4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
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[phone]
Page 8 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92443707
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
495920
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92443707002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2671436
Associated Lab Samples:92443707002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/04/19 18:130.25
1,1,1-Trichloroethane ug/L ND 0.50 09/04/19 18:130.25
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/04/19 18:130.25
1,1,2-Trichloroethane ug/L ND 0.50 09/04/19 18:130.25
1,1-Dichloroethane ug/L ND 0.50 09/04/19 18:130.25
1,1-Dichloroethene ug/L ND 0.50 09/04/19 18:130.25
1,1-Dichloropropene ug/L ND 0.50 09/04/19 18:130.25
1,2,3-Trichlorobenzene ug/L ND 2.0 09/04/19 18:131.0
1,2,3-Trichloropropane ug/L ND 0.50 09/04/19 18:130.25
1,2,4-Trichlorobenzene ug/L ND 2.0 09/04/19 18:131.0
1,2,4-Trimethylbenzene ug/L ND 0.50 09/04/19 18:130.25
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/04/19 18:130.50
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/04/19 18:130.25
1,2-Dichlorobenzene ug/L ND 0.50 09/04/19 18:130.25
1,2-Dichloroethane ug/L ND 0.50 09/04/19 18:130.25
1,2-Dichloropropane ug/L ND 0.50 09/04/19 18:130.25
1,3,5-Trimethylbenzene ug/L ND 0.50 09/04/19 18:130.25
1,3-Dichlorobenzene ug/L ND 0.50 09/04/19 18:130.25
1,3-Dichloropropane ug/L ND 0.50 09/04/19 18:130.25
1,4-Dichlorobenzene ug/L ND 0.50 09/04/19 18:130.25
2,2-Dichloropropane ug/L ND 0.50 09/04/19 18:130.25
2-Butanone (MEK)ug/L ND 5.0 09/04/19 18:135.0
2-Chlorotoluene ug/L ND 0.50 09/04/19 18:130.25
2-Hexanone ug/L ND 5.0 09/04/19 18:135.0
4-Chlorotoluene ug/L ND 0.50 09/04/19 18:130.25
Benzene ug/L ND 0.50 09/04/19 18:130.25
Bromobenzene ug/L ND 0.50 09/04/19 18:130.25
Bromochloromethane ug/L ND 0.50 09/04/19 18:130.25
Bromodichloromethane ug/L ND 0.50 09/04/19 18:130.25
Bromoform ug/L ND 0.50 09/04/19 18:130.25
Bromomethane ug/L ND 5.0 09/04/19 18:132.5
Carbon tetrachloride ug/L ND 0.50 09/04/19 18:130.25
Chlorobenzene ug/L ND 0.50 09/04/19 18:130.25
Chloroethane ug/L ND 1.0 09/04/19 18:130.50
Chloroform ug/L ND 5.0 09/04/19 18:132.5
Chloromethane ug/L ND 1.0 09/04/19 18:130.50
cis-1,2-Dichloroethene ug/L ND 0.50 09/04/19 18:130.25
cis-1,3-Dichloropropene ug/L ND 0.50 09/04/19 18:130.25
Dibromochloromethane ug/L ND 0.50 09/04/19 18:130.25
Dibromomethane ug/L ND 0.50 09/04/19 18:130.25
Dichlorodifluoromethane ug/L ND 0.50 09/04/19 18:130.25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 9 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92443707
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2671436
Associated Lab Samples:92443707002
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 0.50 09/04/19 18:130.25
Ethylbenzene ug/L ND 0.50 09/04/19 18:130.25
Hexachloro-1,3-butadiene ug/L ND 2.0 09/04/19 18:131.0
Isopropylbenzene (Cumene)ug/L ND 0.50 09/04/19 18:130.25
m&p-Xylene ug/L ND 1.0 09/04/19 18:130.50
Methyl-tert-butyl ether ug/L ND 0.50 09/04/19 18:130.25
Methylene Chloride ug/L ND 2.0 09/04/19 18:131.0
n-Butylbenzene ug/L ND 0.50 09/04/19 18:130.25
n-Propylbenzene ug/L ND 0.50 09/04/19 18:130.25
Naphthalene ug/L ND 2.0 09/04/19 18:131.0
o-Xylene ug/L ND 0.50 09/04/19 18:130.25
sec-Butylbenzene ug/L ND 0.50 09/04/19 18:130.25
Styrene ug/L ND 0.50 09/04/19 18:130.25
tert-Butylbenzene ug/L ND 0.50 09/04/19 18:130.25
Tetrachloroethene ug/L ND 0.50 09/04/19 18:130.25
Toluene ug/L ND 0.50 09/04/19 18:130.25
trans-1,2-Dichloroethene ug/L ND 0.50 09/04/19 18:130.25
trans-1,3-Dichloropropene ug/L ND 0.50 09/04/19 18:130.25
Trichloroethene ug/L ND 0.50 09/04/19 18:130.25
Trichlorofluoromethane ug/L ND 1.0 09/04/19 18:130.50
Vinyl chloride ug/L ND 1.0 09/04/19 18:130.50
Xylene (Total)ug/L ND 1.0 09/04/19 18:130.50
1,2-Dichloroethane-d4 (S)%81 70-130 09/04/19 18:13
4-Bromofluorobenzene (S)%103 70-130 09/04/19 18:13
Toluene-d8 (S)%103 70-130 09/04/19 18:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2671437LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.550 105 60-140
1,1,1-Trichloroethane ug/L 49.250 98 60-140
1,1,2,2-Tetrachloroethane ug/L 54.450 109 60-140
1,1,2-Trichloroethane ug/L 55.850 112 60-140
1,1-Dichloroethane ug/L 46.650 93 60-140
1,1-Dichloroethene ug/L 45.550 91 60-140
1,1-Dichloropropene ug/L 41.550 83 60-140
1,2,3-Trichlorobenzene ug/L 52.750 105 60-140
1,2,3-Trichloropropane ug/L 56.850 114 60-140
1,2,4-Trichlorobenzene ug/L 51.950 104 60-140
1,2,4-Trimethylbenzene ug/L 49.950 100 60-140
1,2-Dibromo-3-chloropropane ug/L 56.050 112 60-140
1,2-Dibromoethane (EDB)ug/L 55.150 110 60-140
1,2-Dichlorobenzene ug/L 50.950 102 60-140
1,2-Dichloroethane ug/L 44.050 88 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92443707
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2671437LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 54.550 109 60-140
1,3,5-Trimethylbenzene ug/L 51.650 103 60-140
1,3-Dichlorobenzene ug/L 50.750 101 60-140
1,3-Dichloropropane ug/L 58.450 117 60-140
1,4-Dichlorobenzene ug/L 48.150 96 60-140
2,2-Dichloropropane ug/L 46.750 93 60-140
2-Butanone (MEK)ug/L 92.2100 92 60-140
2-Chlorotoluene ug/L 49.450 99 60-140
2-Hexanone ug/L 114100 114 60-140
4-Chlorotoluene ug/L 49.450 99 60-140
Benzene ug/L 52.350 105 60-140
Bromobenzene ug/L 50.650 101 60-140
Bromochloromethane ug/L 48.550 97 60-140
Bromodichloromethane ug/L 54.650 109 60-140
Bromoform ug/L 56.450 113 60-140
Bromomethane ug/L 41.950 84 60-140
Carbon tetrachloride ug/L 51.150 102 60-140
Chlorobenzene ug/L 49.050 98 60-140
Chloroethane ug/L 49.450 99 60-140
Chloroform ug/L 44.450 89 60-140
Chloromethane ug/L 43.550 87 60-140
cis-1,2-Dichloroethene ug/L 46.050 92 60-140
cis-1,3-Dichloropropene ug/L 59.650 119 60-140
Dibromochloromethane ug/L 56.950 114 60-140
Dibromomethane ug/L 51.250 102 60-140
Dichlorodifluoromethane ug/L 38.450 77 60-140
Diisopropyl ether ug/L 52.550 105 60-140
Ethylbenzene ug/L 48.350 97 60-140
Hexachloro-1,3-butadiene ug/L 52.750 105 60-140
Isopropylbenzene (Cumene)ug/L 50.150 100 60-140
m&p-Xylene ug/L 99.4100 99 60-140
Methyl-tert-butyl ether ug/L 45.450 91 60-140
Methylene Chloride ug/L 43.950 88 60-140
n-Butylbenzene ug/L 50.350 101 60-140
n-Propylbenzene ug/L 49.450 99 60-140
Naphthalene ug/L 56.150 112 60-140
o-Xylene ug/L 49.850 100 60-140
sec-Butylbenzene ug/L 51.950 104 60-140
Styrene ug/L 51.950 104 60-140
tert-Butylbenzene ug/L 46.150 92 60-140
Tetrachloroethene ug/L 51.250 102 60-140
Toluene ug/L 47.650 95 60-140
trans-1,2-Dichloroethene ug/L 46.350 93 60-140
trans-1,3-Dichloropropene ug/L 57.250 114 60-140
Trichloroethene ug/L 54.750 109 60-140
Trichlorofluoromethane ug/L 43.750 87 60-140
Vinyl chloride ug/L 43.850 88 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92443707
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2671437LABORATORY CONTROL SAMPLE:
LCSSpike
Xylene (Total)ug/L 149150 100 60-140
1,2-Dichloroethane-d4 (S)%88 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2672141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92443184011
2672142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2500 120 60-140118 1 302500ND29902950
1,1,1-Trichloroethane ug/L 2500 118 60-140118 0 302500ND29602960
1,1,2,2-Tetrachloroethane ug/L 2500 118 60-140112 5 302500ND29602800
1,1,2-Trichloroethane ug/L 2500 125 60-140117 6 302500ND31202930
1,1-Dichloroethane ug/L 2500 116 60-140115 1 302500ND29102880
1,1-Dichloroethene ug/L 2500 117 60-140115 2 302500ND29202860
1,1-Dichloropropene ug/L 2500 101 60-140100 1 302500ND25202510
1,2,3-Trichlorobenzene ug/L 2500 121 60-140120 1 302500ND30102990
1,2,3-Trichloropropane ug/L 2500 119 60-140118 1 302500ND29702940
1,2,4-Trichlorobenzene ug/L 2500 118 60-140120 2 302500ND29503000
1,2,4-Trimethylbenzene ug/L 2500 118 60-140123 2 302500317061306240
1,2-Dibromo-3-
chloropropane ug/L 2500 116 60-140122 5 302500ND29103040
1,2-Dibromoethane (EDB)ug/L 2500 119 60-140121 1 302500ND29803020
1,2-Dichlorobenzene ug/L 2500 114 60-140115 1 302500ND28402870
1,2-Dichloroethane ug/L 2500 103 60-140100 3 30250089.2 2670 2590
1,2-Dichloropropane ug/L 2500 120 60-140120 0 302500ND30003000
1,3,5-Trimethylbenzene ug/L M1250015260-140160 5 302500ND37904010
1,3-Dichlorobenzene ug/L 2500 117 60-140115 2 302500ND29302880
1,3-Dichloropropane ug/L 2500 127 60-140125 2 302500ND31703120
1,4-Dichlorobenzene ug/L 2500 110 60-140114 3 302500ND27502840
2,2-Dichloropropane ug/L 2500 112 60-140110 2 302500ND28102750
2-Butanone (MEK)ug/L 5000 98 60-14095 3 305000ND48804750
2-Chlorotoluene ug/L 2500 123 60-140127 3 302500ND30903170
2-Hexanone ug/L 5000 112 60-140109 2 305000ND55905470
4-Chlorotoluene ug/L 2500 115 60-140116 1 302500ND28702900
Benzene ug/L M1250014460-140142 0 30250088401240012400
Bromobenzene ug/L 2500 119 60-140120 0 302500ND29802990
Bromochloromethane ug/L 2500 116 60-140114 2 302500ND29102860
Bromodichloromethane ug/L 2500 122 60-140121 1 302500ND30403030
Bromoform ug/L 2500 117 60-140116 1 302500ND29202890
Bromomethane ug/L 2500 75 60-14087 15 302500ND18802180
Carbon tetrachloride ug/L 2500 122 60-140122 0 302500ND30603050
Chlorobenzene ug/L 2500 116 60-140116 0 302500ND29002900
Chloroethane ug/L 2500 103 60-140107 4 302500ND25702670
Chloroform ug/L 2500 110 60-140108 1 302500ND27502710
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92443707
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2672141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92443184011
2672142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloromethane ug/L 2500 104 60-140108 4 302500ND26002700
cis-1,2-Dichloroethene ug/L 2500 111 60-140110 1 302500ND27802760
cis-1,3-Dichloropropene ug/L 2500 128 60-140127 1 302500ND32103160
Dibromochloromethane ug/L 2500 121 60-140120 0 302500ND30203010
Dibromomethane ug/L 2500 122 60-140118 3 302500ND30402950
Dichlorodifluoromethane ug/L 2500 93 60-14092 1 302500ND23302300
Diisopropyl ether ug/L 2500 118 60-140115 2 302500ND29402880
Ethylbenzene ug/L 2500 112 60-140121 3 302500355063506570
Hexachloro-1,3-butadiene ug/L 2500 130 60-140124 5 302500ND32503110
Isopropylbenzene
(Cumene)
ug/L 2500 121 60-140122 1 30250015031603210
m&p-Xylene ug/L 5000 104 60-140120 4 305000131001830019100
Methyl-tert-butyl ether ug/L 2500 117 60-140111 3 302500171046504500
Methylene Chloride ug/L 2500 108 60-140109 1 302500ND26902720
n-Butylbenzene ug/L 2500 124 60-140125 1 302500ND30903130
n-Propylbenzene ug/L 2500 129 60-140134 4 302500ND32403360
Naphthalene ug/L 2500 123 60-140119 2 30250083939003820
o-Xylene ug/L 2500 107 60-140116 3 302500607087408970
sec-Butylbenzene ug/L 2500 124 60-140127 3 302500ND30903170
Styrene ug/L 2500 131 60-140132 1 302500ND32703290
tert-Butylbenzene ug/L 2500 112 60-140115 2 302500ND28102870
Tetrachloroethene ug/L 2500 124 60-140126 2 302500ND30903150
Toluene ug/L E25009260-14080 1 302500243002660026300
trans-1,2-Dichloroethene ug/L 2500 112 60-140112 0 302500ND28002790
trans-1,3-Dichloropropene ug/L 2500 123 60-140121 2 302500ND30903020
Trichloroethene ug/L 2500 125 60-140127 2 302500ND31103180
Trichlorofluoromethane ug/L 2500 106 60-140107 1 302500ND26402680
Vinyl chloride ug/L 2500 110 60-140109 1 302500ND27502740
Xylene (Total)ug/L 7500 105 60-140119 4 307500192002700028100
1,2-Dichloroethane-d4 (S)%93 70-13091
4-Bromofluorobenzene (S)%97 70-13099
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92443707
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
496396
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92443707001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2673402
Associated Lab Samples:92443707001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/06/19 10:550.25
1,1,1-Trichloroethane ug/L ND 0.50 09/06/19 10:550.25
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/06/19 10:550.25
1,1,2-Trichloroethane ug/L ND 0.50 09/06/19 10:550.25
1,1-Dichloroethane ug/L ND 0.50 09/06/19 10:550.25
1,1-Dichloroethene ug/L ND 0.50 09/06/19 10:550.25
1,1-Dichloropropene ug/L ND 0.50 09/06/19 10:550.25
1,2,3-Trichlorobenzene ug/L ND 2.0 09/06/19 10:551.0
1,2,3-Trichloropropane ug/L ND 0.50 09/06/19 10:550.25
1,2,4-Trichlorobenzene ug/L ND 2.0 09/06/19 10:551.0
1,2,4-Trimethylbenzene ug/L ND 0.50 09/06/19 10:550.25
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/06/19 10:550.50
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/06/19 10:550.25
1,2-Dichlorobenzene ug/L ND 0.50 09/06/19 10:550.25
1,2-Dichloroethane ug/L ND 0.50 09/06/19 10:550.25
1,2-Dichloropropane ug/L ND 0.50 09/06/19 10:550.25
1,3,5-Trimethylbenzene ug/L ND 0.50 09/06/19 10:550.25
1,3-Dichlorobenzene ug/L ND 0.50 09/06/19 10:550.25
1,3-Dichloropropane ug/L ND 0.50 09/06/19 10:550.25
1,4-Dichlorobenzene ug/L ND 0.50 09/06/19 10:550.25
2,2-Dichloropropane ug/L ND 0.50 09/06/19 10:550.25
2-Butanone (MEK)ug/L ND 5.0 09/06/19 10:555.0
2-Chlorotoluene ug/L ND 0.50 09/06/19 10:550.25
2-Hexanone ug/L ND 5.0 09/06/19 10:555.0
4-Chlorotoluene ug/L ND 0.50 09/06/19 10:550.25
Benzene ug/L ND 0.50 09/06/19 10:550.25
Bromobenzene ug/L ND 0.50 09/06/19 10:550.25
Bromochloromethane ug/L ND 0.50 09/06/19 10:550.25
Bromodichloromethane ug/L ND 0.50 09/06/19 10:550.25
Bromoform ug/L ND 0.50 09/06/19 10:550.25
Bromomethane ug/L ND 5.0 09/06/19 10:552.5
Carbon tetrachloride ug/L ND 0.50 09/06/19 10:550.25
Chlorobenzene ug/L ND 0.50 09/06/19 10:550.25
Chloroethane ug/L ND 1.0 09/06/19 10:550.50
Chloroform ug/L ND 5.0 09/06/19 10:552.5
Chloromethane ug/L ND 1.0 09/06/19 10:550.50
cis-1,2-Dichloroethene ug/L ND 0.50 09/06/19 10:550.25
cis-1,3-Dichloropropene ug/L ND 0.50 09/06/19 10:550.25
Dibromochloromethane ug/L ND 0.50 09/06/19 10:550.25
Dibromomethane ug/L ND 0.50 09/06/19 10:550.25
Dichlorodifluoromethane ug/L ND 0.50 09/06/19 10:550.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92443707
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2673402
Associated Lab Samples:92443707001
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 0.50 09/06/19 10:550.25
Ethylbenzene ug/L ND 0.50 09/06/19 10:550.25
Hexachloro-1,3-butadiene ug/L ND 2.0 09/06/19 10:551.0
Isopropylbenzene (Cumene)ug/L ND 0.50 09/06/19 10:550.25
m&p-Xylene ug/L ND 1.0 09/06/19 10:550.50
Methyl-tert-butyl ether ug/L ND 0.50 09/06/19 10:550.25
Methylene Chloride ug/L ND 2.0 09/06/19 10:551.0
n-Butylbenzene ug/L ND 0.50 09/06/19 10:550.25
n-Propylbenzene ug/L ND 0.50 09/06/19 10:550.25
Naphthalene ug/L ND 2.0 09/06/19 10:551.0
o-Xylene ug/L ND 0.50 09/06/19 10:550.25
sec-Butylbenzene ug/L ND 0.50 09/06/19 10:550.25
Styrene ug/L ND 0.50 09/06/19 10:550.25
tert-Butylbenzene ug/L ND 0.50 09/06/19 10:550.25
Tetrachloroethene ug/L ND 0.50 09/06/19 10:550.25
Toluene ug/L ND 0.50 09/06/19 10:550.25
trans-1,2-Dichloroethene ug/L ND 0.50 09/06/19 10:550.25
trans-1,3-Dichloropropene ug/L ND 0.50 09/06/19 10:550.25
Trichloroethene ug/L ND 0.50 09/06/19 10:550.25
Trichlorofluoromethane ug/L ND 1.0 09/06/19 10:550.50
Vinyl chloride ug/L ND 1.0 09/06/19 10:550.50
Xylene (Total)ug/L ND 1.0 09/06/19 10:550.50
1,2-Dichloroethane-d4 (S)%75 70-130 09/06/19 10:55
4-Bromofluorobenzene (S)%101 70-130 09/06/19 10:55
Toluene-d8 (S)%104 70-130 09/06/19 10:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2673403LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 57.250 114 60-140
1,1,1-Trichloroethane ug/L 53.550 107 60-140
1,1,2,2-Tetrachloroethane ug/L 56.350 113 60-140
1,1,2-Trichloroethane ug/L 58.950 118 60-140
1,1-Dichloroethane ug/L 51.750 103 60-140
1,1-Dichloroethene ug/L 51.750 103 60-140
1,1-Dichloropropene ug/L 45.650 91 60-140
1,2,3-Trichlorobenzene ug/L 56.650 113 60-140
1,2,3-Trichloropropane ug/L 59.350 119 60-140
1,2,4-Trichlorobenzene ug/L 56.050 112 60-140
1,2,4-Trimethylbenzene ug/L 54.650 109 60-140
1,2-Dibromo-3-chloropropane ug/L 59.050 118 60-140
1,2-Dibromoethane (EDB)ug/L 60.150 120 60-140
1,2-Dichlorobenzene ug/L 54.150 108 60-140
1,2-Dichloroethane ug/L 47.550 95 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92443707
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2673403LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 58.850 118 60-140
1,3,5-Trimethylbenzene ug/L 55.250 110 60-140
1,3-Dichlorobenzene ug/L 54.450 109 60-140
1,3-Dichloropropane ug/L 62.250 124 60-140
1,4-Dichlorobenzene ug/L 50.850 102 60-140
2,2-Dichloropropane ug/L 52.550 105 60-140
2-Butanone (MEK)ug/L 92.3100 92 60-140
2-Chlorotoluene ug/L 52.050 104 60-140
2-Hexanone ug/L 113100 113 60-140
4-Chlorotoluene ug/L 53.350 107 60-140
Benzene ug/L 56.650 113 60-140
Bromobenzene ug/L 55.250 110 60-140
Bromochloromethane ug/L 55.150 110 60-140
Bromodichloromethane ug/L 58.750 117 60-140
Bromoform ug/L 61.450 123 60-140
Bromomethane ug/L 46.650 93 60-140
Carbon tetrachloride ug/L 56.550 113 60-140
Chlorobenzene ug/L 54.050 108 60-140
Chloroethane ug/L 55.250 110 60-140
Chloroform ug/L 50.650 101 60-140
Chloromethane ug/L 49.350 99 60-140
cis-1,2-Dichloroethene ug/L 51.750 103 60-140
cis-1,3-Dichloropropene ug/L 64.250 128 60-140
Dibromochloromethane ug/L 63.050 126 60-140
Dibromomethane ug/L 57.850 116 60-140
Dichlorodifluoromethane ug/L 47.250 94 60-140
Diisopropyl ether ug/L 56.250 112 60-140
Ethylbenzene ug/L 53.250 106 60-140
Hexachloro-1,3-butadiene ug/L 60.550 121 60-140
Isopropylbenzene (Cumene)ug/L 55.750 111 60-140
m&p-Xylene ug/L 110100 110 60-140
Methyl-tert-butyl ether ug/L 47.550 95 60-140
Methylene Chloride ug/L 49.550 99 60-140
n-Butylbenzene ug/L 55.450 111 60-140
n-Propylbenzene ug/L 53.450 107 60-140
Naphthalene ug/L 57.750 115 60-140
o-Xylene ug/L 56.150 112 60-140
sec-Butylbenzene ug/L 55.250 110 60-140
Styrene ug/L 57.050 114 60-140
tert-Butylbenzene ug/L 49.750 99 60-140
Tetrachloroethene ug/L 55.950 112 60-140
Toluene ug/L 51.550 103 60-140
trans-1,2-Dichloroethene ug/L 52.550 105 60-140
trans-1,3-Dichloropropene ug/L 61.150 122 60-140
Trichloroethene ug/L 59.150 118 60-140
Trichlorofluoromethane ug/L 48.750 97 60-140
Vinyl chloride ug/L 50.550 101 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92443707
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2673403LABORATORY CONTROL SAMPLE:
LCSSpike
Xylene (Total)ug/L 166150 111 60-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2673404MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92443184008
2673405
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 10000 124 60-140118 5 3010000ND1240011800
1,1,1-Trichloroethane ug/L 10000 119 60-140111 7 3010000ND1190011100
1,1,2,2-Tetrachloroethane ug/L 10000 122 60-140115 5 3010000ND1220011500
1,1,2-Trichloroethane ug/L 10000 128 60-140121 6 3010000ND1280012100
1,1-Dichloroethane ug/L 10000 117 60-140112 4 3010000ND1170011200
1,1-Dichloroethene ug/L 10000 118 60-140113 4 3010000ND1180011300
1,1-Dichloropropene ug/L 10000 100 60-14097 2 3010000ND99609720
1,2,3-Trichlorobenzene ug/L 10000 126 60-140118 7 3010000ND1260011800
1,2,3-Trichloropropane ug/L 10000 128 60-140123 4 3010000ND1280012300
1,2,4-Trichlorobenzene ug/L 10000 123 60-140115 6 3010000ND1230011500
1,2,4-Trimethylbenzene ug/L 10000 123 60-140116 5 301000024101480014000
1,2-Dibromo-3-
chloropropane ug/L 10000 131 60-140117 11 3010000ND1310011700
1,2-Dibromoethane (EDB)ug/L 10000 125 60-140119 5 3010000ND1250011900
1,2-Dichlorobenzene ug/L 10000 122 60-140114 7 3010000ND1220011400
1,2-Dichloroethane ug/L 10000 102 60-140102 0 3010000ND1020010200
1,2-Dichloropropane ug/L 10000 128 60-140122 5 3010000ND1280012200
1,3,5-Trimethylbenzene ug/L 10000 129 60-140123 5 3010000ND1290012300
1,3-Dichlorobenzene ug/L 10000 124 60-140115 8 3010000ND1240011500
1,3-Dichloropropane ug/L 10000 131 60-140128 2 3010000ND1310012800
1,4-Dichlorobenzene ug/L 10000 113 60-140110 3 3010000ND1130011000
2,2-Dichloropropane ug/L 10000 110 60-140106 3 3010000ND1100010600
2-Butanone (MEK)ug/L 20000 103 60-14095 8 3020000ND2070019000
2-Chlorotoluene ug/L 10000 118 60-140112 5 3010000ND1180011200
2-Hexanone ug/L 20000 126 60-140117 7 3020000ND2510023400
4-Chlorotoluene ug/L 10000 118 60-140112 5 3010000ND1180011200
Benzene ug/L M11000014560-140129 5 3010000149002940027800
Bromobenzene ug/L 10000 124 60-140112 10 3010000ND1240011200
Bromochloromethane ug/L 10000 117 60-140114 2 3010000ND1170011400
Bromodichloromethane ug/L 10000 130 60-140122 6 3010000ND1300012200
Bromoform ug/L 10000 124 60-140117 5 3010000ND1240011700
Bromomethane ug/L 10000 110 60-140109 1 3010000ND1100010900
Carbon tetrachloride ug/L 10000 127 60-140118 7 3010000ND1270011800
Chlorobenzene ug/L 10000 120 60-140116 4 3010000ND1200011600
Chloroethane ug/L 10000 112 60-140106 6 3010000ND1120010600
Chloroform ug/L 10000 110 60-140110 0 3010000ND1100011000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92443707
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2673404MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92443184008
2673405
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloromethane ug/L 10000 114 60-140107 7 3010000ND1140010700
cis-1,2-Dichloroethene ug/L 10000 114 60-140110 3 3010000ND1140011000
cis-1,3-Dichloropropene ug/L 10000 134 60-140126 6 3010000ND1340012600
Dibromochloromethane ug/L 10000 129 60-140123 5 3010000ND1290012300
Dibromomethane ug/L 10000 131 60-140118 10 3010000ND1310011800
Dichlorodifluoromethane ug/L 10000 101 60-14099 2 3010000ND101009870
Diisopropyl ether ug/L 10000 119 60-140116 3 3010000ND1190011600
Ethylbenzene ug/L 10000 125 60-140120 3 301000033801590015300
Hexachloro-1,3-butadiene ug/L 10000 135 60-140122 10 3010000ND1350012200
Isopropylbenzene
(Cumene)
ug/L 10000 129 60-140123 5 3010000ND1290012300
m&p-Xylene ug/L 20000 124 60-140120 2 3020000119003670035900
Methyl-tert-butyl ether ug/L 10000 101 60-14095 6 30100009271110010500
Methylene Chloride ug/L 10000 115 60-140107 7 3010000ND1150010700
n-Butylbenzene ug/L 10000 122 60-140113 7 3010000ND1220011300
n-Propylbenzene ug/L 10000 124 60-140118 4 3010000ND1240011800
Naphthalene ug/L 10000 125 60-140116 7 3010000ND1340012500
o-Xylene ug/L 10000 126 60-140122 2 301000057101830017900
sec-Butylbenzene ug/L 10000 129 60-140118 9 3010000ND1290011800
Styrene ug/L 10000 131 60-140127 3 3010000ND1310012700
tert-Butylbenzene ug/L 10000 113 60-140106 6 3010000ND1130010600
Tetrachloroethene ug/L 10000 132 60-140125 5 3010000ND1320012500
Toluene ug/L 10000 95 60-14084 2 3010000383004780046800
trans-1,2-Dichloroethene ug/L 10000 116 60-140112 3 3010000ND1160011200
trans-1,3-Dichloropropene ug/L 10000 129 60-140121 6 3010000ND1290012100
Trichloroethene ug/L 10000 134 60-140123 9 3010000ND1340012300
Trichlorofluoromethane ug/L 10000 112 60-140108 4 3010000ND1120010800
Vinyl chloride ug/L 10000 117 60-140112 5 3010000ND1170011200
Xylene (Total)ug/L 30000 125 60-140121 2 3030000176005500053800
1,2-Dichloroethane-d4 (S)%86 70-13092
4-Bromofluorobenzene (S)%98 70-130101
Toluene-d8 (S)%97 70-13098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92443707
YOGI FOODS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
496706
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Associated Lab Samples:92443707001, 92443707002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2674883
Associated Lab Samples:92443707001, 92443707002
Matrix:Water
AnalyzedMDL
1,2-Dibromoethane (EDB)ug/L ND 0.020 09/09/19 13:270.011
1-Chloro-2-bromopropane (S)%103 70-130 09/09/19 13:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2674884LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2674923
1,2-Dibromoethane (EDB)ug/L 0.240.25 97 70-130940.23 4 20
1-Chloro-2-bromopropane (S)%99 70-13098
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92444509001
2674887SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L 0.23 8 200.25
1-Chloro-2-bromopropane (S)%102108
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 24
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92443707
YOGI FOODS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 24
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92443707
YOGI FOODS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92443707001 496706 496748MW-1 EPA 504.1 EPA 504.1
92443707002 496706 496748MW-5 EPA 504.1 EPA 504.1
92443707001 496396MW-1 SM 6200B
92443707002 495920MW-5 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/09/2019 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 24
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