AS-3327_28491_CA_LSA_20141024_2

PHASE II LIMITED SITE ASSESSMENT REPORT

Yogi Foods
4018 Highway 321A
Hudson, Caldwell County, North Carolina 28638
ATC Project Number 89.03451.1043
NCDENR Incident No. 28491
NCDENR Facility Identification No. 0-007809
NCDENR Risk Classification: High (H130D)

October 24, 2014

7606 Whitehall Executive Center Drive, Suite 800
Charlotte, NC 28273
Tel: [phone]
Fax: [phone]
www.atcassociates.com
N.C. Engineering License No. C-1598

October 24, 2014

Mr. Dan Murphy
North Carolina Department of Environment and Natural Resources
Asheville Regional Office
Division of Waste Management - UST Section
2090 US Highway 70
Swannanoa, NC 28778

Re: Yogi Foods
4018 Highway 321A
Hudson, Caldwell County, North Carolina 28638
ATC Project Number 89.03451.1043
NCDENR Incident No. 28491
NCDENR Facility Identification No. 0-007809
NCDENR Risk Classification: High (H130D)

Dear Mr. Murphy:

ATC Associates of North Carolina, P.C. (ATC), on behalf of Cary Oil Company, is submitting the enclosed
Phase II Limited Site Assessment (LSA) Report for Yogi Foods site. This report includes the analytical
results obtained from assessment activities conducted in August 2014.

If you have any questions or require additional information, please contact our office at [phone].

Sincerely,

ATC Associates of North Carolina, P.C.

Christine E. Schaefer
Project Manager

cc: Mr. Glenn Petti – Cary Oil Company

Yogi Foods ATC Associates of North Carolina, P.C.
Phase II LSA Report i October 24, 2014

Site Identification:
Date of Report: 10/24/2014
Facility I.D.: 0-007809 UST Incident Number (if known): 28491 Site Risk: High (H130D)
Site Name: Yogi Foods
Site Street Address: 4018 Highway 321A
City/Town: Hudson Zip Code: 28638 County: Caldwell
Description of Geographical Data Point (e.g., diesel fill port): UST Basin
Location Method (GPS, topographical map, other): Google Earth
Latitude (decimal degrees): 35.827182° N Longitude (decimal degrees): -81.476007° W

Information about Contacts Associated with the Release:
UST Owner: Cary Oil Company
Address: 110 MacKenan Drive, Suite 300, Cary, NC 27511 Phone: [phone]
UST Operator: AJ Patel
Address: 4018 Highway 321A, Hudson, NC 28638 Phone: [phone]
Property Owner: HHA Development LLC
Address: PO Box 190, Taylorsville, NC 28681 Phone: Unknown
Property Occupant: Shell Service Station/Market Basket Convenience Store
Address: 4018 Highway 321A, Hudson, NC 28638 Phone: Unknown
Consultant/Contractor: ATC Associates of North Carolina, P.C.
Address:7606 Whitehall Executive Center Dr, Charlotte, NC 28273 Phone: [phone]
Analytical Laboratory: Pace Analytical Services, Inc. State Certification No.: 5342
Address: 9800 Kincey Ave., Suite 100, Huntersville, NC 28078 Phone: [phone]

Information about Release:
Date Discovered: July 14, 2006
Estimated Quantity of Release: unknown
Cause of Release: unknown
Source of Release (Dispenser/Piping/UST): gasoline/diesel UST system
Sizes and contents of UST system(s) from which the release occurred: Two – 8,000 gallon gasoline USTs,
one – 8,000 diesel UST, and one – 2,000 gallon kerosene UST and associated piping and dispensers

I, David A. Hunter a Licensed Geologist for ATC Associates of North Carolina,
P.C., do certify that the information contained in this report is correct and accurate to the best of my
knowledge.

ATC Associates of North Carolina, P.C. is licensed to practice geology/engineering (circle one or both) in
North Carolina. The certification number issued by the North Carolina Board for Licensing of Geologists
is C-274. The certification number issued by the North Carolina Board of Examiners for Engineers and
Surveyors is C-1598.

Yogi Foods ATC Associates of North Carolina, P.C.
Phase II LSA Report ii October 24, 2014

TABLE OF CONTENTS

1.0 INTRODUCTION ............................................................................................................................ 1
1.1 Site Description .............................................................................................................. 1
1.2 Site History ..................................................................................................................... 2
2.0 RISK CHARACTERIZATION ..................................................................................................... 3
3.0 RECEPTOR INFORMATION ...................................................................................................... 3
3.1 Water Supply Wells ........................................................................................................ 3
3.2 Public Water Supplies .................................................................................................... 4
3.3 Surface Water ................................................................................................................. 4
3.4 Wellhead Protection Areas ............................................................................................. 4
3.5 Deep Aquifers in the Coastal Plain ................................................................................. 4
3.6 Subsurface Structures ..................................................................................................... 4
3.7 Land Use ......................................................................................................................... 5
4.0 SITE CHARACTERISTICS .......................................................................................................... 5
4.1 Regional Geology ........................................................................................................... 5
4.2 Site Geology ................................................................................................................... 6
4.3 Regional Hydrogeology .................................................................................................. 6
4.4 Site Hydrogeology .......................................................................................................... 6
5.0 SUBSURFACE INVESTIGATION .............................................................................................. 7
5.1 Soil Sampling ................................................................................................................. 7
5.2 Well Installation ............................................................................................................. 7
6.0 CONCLUSIONS ............................................................................................................................... 8

Yogi Foods ATC Associates of North Carolina, P.C.
Phase II LSA Report iii October 24, 2014

TABLES

Table B-1 Site History - UST System and Other Release Information
Table B-2 Site History - UST Owner/Operator and Other Responsible Party
Table B-3 Summary of Soil Sampling Results
Table B-4 Summary of Groundwater Sampling Results
Table B-5 Public and Private Water Supply Well and Other Receptor Information
Table B-7 Monitoring Well Construction Information

FIGURES

Figure 1 Site Topographic Map
Figure 2 Site Map
Figure 3 Water Supply Well Location Map
Figure 4 Soil Analytical Data Map
Figure 5 Groundwater Elevation Map
Figure 6 Benzene Isoconcentration Map
Figure 7 Toluene Isoconcentration Map
Figure 8 Ethylbenzene Isoconcentration Map
Figure 9 Xylenes Isoconcentration Map

APPENDICES

Appendix A Limited Site Assessment Risk Classification and Land Use Form
Appendix B Soil Boring Logs and Well Records
Appendix C Laboratory Analytical Report

Yogi Foods ATC Associates of North Carolina, P.C.
Phase II LSA Report 1 October 24, 2014

1.0 INTRODUCTION

Cary Oil Company (Cary Oil) retained ATC Associates of North Carolina, P.C. (ATC) to conduct
groundwater assessment activities at the Yogi Foods site located at 4018 Highway 321A in Hudson,
Caldwell County, North Carolina. A United States Geological Survey (USGS) topographic map that
shows topographic contours, site location, surface water bodies, buildings, and adjacent roads in the site
vicinity is included as Figure 1.

1.1 Site Description

The subject site currently operates as a Shell service station with retail fuel sales and a convenience store
called Market Basket. A site map that indicates monitoring well locations and other site features is
included as Figure 2. The site is accessible from Highway 321A to the west and Adams Drive to the
southeast. Properties within 1,500 feet of the site are mainly commercial and residential on the east side
Highway 321A and mainly industrial on the west side of Highway 321A.

Two 8,000-gallon gasoline underground storage tanks (USTs) and one 8,000-gallon diesel UST were
installed in April 1985 and are currently in use at the site. A separate basin contains one 2,000-gallon
kerosene UST, which was installed in February 1976 and is also currently in use. UST system and
owner/operator information is provided in Tables B-1 and B-2. The site also consists of a single-story
convenience store building and fuel dispensers associated with the USTs. Surface cover at the site
consists mostly of asphalt and concrete in the fueling and driveway areas. The surface cover on the east
portion of the property, behind the convenience store building, consists mostly of grass.

The site and surrounding areas are supplied municipal water by the Town of Sawmills. An updated
receptor survey was conducted in 2012, which provided supplemental information to an initial receptor
survey conducted during a Phase I Limited Site Assessment (LSA) in 2006. Based on information obtained
from the updated receptor survey, one private well (WSW-4) is being used for irrigation purposes and is
located approximately 315 feet from the source area. Thirteen additional water supply wells were identified
within 1,500 feet of the site but were not in use. A large concrete cover was observed at the property adjacent
to the subject site and was identified as a potential water supply well. However, the property owner could not
provide information because the cover was there when he bought the property. Due to the size, weight, and
security (apparently cemented in place) of the cover, confirmation of whether the object was a well could not
be validated. Without the ability to confirm the object was not a potential receptor, the North Carolina

Yogi Foods ATC Associates of North Carolina, P.C.
Phase II LSA Report 2 October 24, 2014

Department of Environment and Natural Resources (NCDENR) has assigned a high risk classification to the
site based on the object’s proximity to the subject site. The property with the suspected well, located at 2338
Adams Drive, is supplied municipal water by the Town of Sawmills.

Poplar Fish Lake is located approximately 1,100 feet to the east of the subject site. The drainage feature that
supplies Poplar Fish Lake originates closer to the site but does not appear to be a perennial stream over the
closer interval.

Soils encountered during installation of monitoring wells on-site have been described as sandy clay,
sandy silt, and silty clay to a termination depth of approximately 30 feet below grade. Depth to
groundwater in site monitoring wells ranged from 15.55 feet to 23.05 feet below top of casing (TOC) on
August 6, 2014. Groundwater flow appears to be generally towards the east based on elevation data
obtained on August 6, 2014.

1.2 Site History

A due diligence investigation was conducted by Cary Oil on June 30, 2006. Soil samples were collected at
nine locations (YF-1 through YF-9) and submitted for laboratory analysis of total petroleum hydrocarbons –
gasoline range organics (TPH – GRO). Laboratory analytical results of a soil sample collected adjacent to a
gasoline and diesel dispenser (YF-4) indicated a TPH – GRO concentration that exceeded the NCDENR
action level of 10 mg/kg. Cary Oil submitted a 24-Hour Release and UST Leak Reporting Form (UST-61) to
the NCDENR on July 14, 2006.

ATC conducted a Phase I LSA on August 10 and 11, 2006, based on the results of the due diligence
investigation. Monitoring well MW-1 was installed with 1-inch diameter polyvinyl chloride (PVC) pipe to a
depth of 28 feet below grade, with a 15 foot screened section. Soil samples were collected through split spoon
samplers during well installation activities and submitted for laboratory analysis of volatile organic
compounds (VOCs) by EPA Method 8260, semi-VOCs by EPA Method 8270, and Massachusetts
Department of Environmental Protection volatile petroleum hydrocarbons (MADEP VPH). Laboratory
analytical results identified contaminant concentrations above soil-to-groundwater maximum soil
contaminant concentrations (MSCCs). A groundwater sample was collected from well MW-1 and submitted
for laboratory analysis of VOCs by EPA Method 624, MADEP VPH, and lead by EPA Method 6010.
Laboratory analytical results indicated groundwater contaminant concentrations above NCDENR 2L
Standards, and the benzene concentration exceeded the Gross Contamination Level (GCL).

Yogi Foods ATC Associates of North Carolina, P.C.
Phase II LSA Report 3 October 24, 2014

ATC recommended additional assessment to determine the extent of petroleum contaminant impact. This
report documents the results of the subsequent Phase II LSA.

2.0 RISK CHARACTERIZATION

In accordance with 15A NCAC 2L .0115, a completed Limited Site Assessment Risk Classification and
Land Use Form provided by the NCDENR is included in Appendix A. Answers and explanations
included on the form are based on information obtained by ATC during Phase I and II LSA activities.

3.0 RECEPTOR INFORMATION

3.1 Water Supply Wells

An updated receptor survey was conducted in 2012, which provided supplemental information to an
initial receptor survey conducted during a Phase I LSA in 2006. Water supply well forms were sent via
certified mail to property owners within 500 feet of the site and to owners of properties where water supply
wells had been previously identified. ATC subsequently conducted a visual site reconnaissance within a
1,500 foot radius of the site to confirm the existence of water supply wells in the area. Based on information
obtained from the updated receptor survey, one private well (WSW-4) is being used for irrigation purposes
and is located approximately 315 feet from the source area. Thirteen additional water supply wells were
identified within 1,500 feet of the site but were not in use. A large concrete cover was observed at the
property adjacent to the subject site and was identified as a potential water supply well. However, the
property owner could not provide information because the cover was there when he bought the property. Due
to the size, weight, and security (apparently cemented in place) of the cover, confirmation of whether the
object was a well could not be validated. Without the ability to confirm the object was not a potential
receptor, the NCDENR has assigned a high risk classification to the site based on the object’s proximity to
the subject site. The property with the suspected well, located at 2338 Adams Drive, is supplied municipal
water by the Town of Sawmills. The locations of identified water supply wells are indicated on Figure 3.

Poplar Fish Lake is located approximately 1,100 feet to the east of the subject site. The drainage feature that
supplies Poplar Fish Lake originates closer to the site but does not appear to be a perennial stream over the
closer interval. Receptor information is provided as Table B-5.

Yogi Foods ATC Associates of North Carolina, P.C.
Phase II LSA Report 4 October 24, 2014

3.2 Public Water Supplies

Potable water is provided to the area by the Town of Sawmills and the City of Lenoir. The public water
source (Lake Rhodhiss) is not located within 1,500 feet of the subject site.

3.3 Surface Water

ATC reviewed a USGS 7.5-Minute Quadrangle Topographic Map (Figure 1) to identify surface water
bodies in the site vicinity. In addition, ATC conducted a visual reconnaissance for surface water bodies
in the area. Poplar Fish Lake is located approximately 1,100 feet to the east of the subject site. The drainage
feature that supplies Poplar Fish Lake originates closer to the site but does not appear to be a perennial stream
over the closer interval.

3.4 Wellhead Protection Areas

According the Division of Water Quality Wellhead Protection Website, the site is not located within a
wellhead protection program area.

3.5 Deep Aquifers in the Coastal Plain

The risk classification criteria specified in Title 15A NCAC 2L .0115(d) requires an evaluation for the
presence of unconfined or semi-confined deep aquifers in the Coastal Plain region which may be used as
a source of drinking water. The site is not located in the Coastal Plain Physiographic region.

3.6 Subsurface Structures

Prior to drilling activities, a private utility locating company and One-Call of North Carolina, a public utility
locating service, were contacted to locate underground utilities at the site. Underground utilities (water,
electric, natural gas, telephone) were located on-site; however, the utilities did not intersect the water table.
Underground utility locations are identified on Figure 2.

Yogi Foods ATC Associates of North Carolina, P.C.
Phase II LSA Report 5 October 24, 2014

3.7 Land Use

The subject site is located in Caldwell County, North Carolina. The site is accessible from Highway 321A
to the west and Adams Drive to the southeast. The site operates as a retail petroleum and convenience
store, and contains two gasoline USTs, one diesel UST, and one kerosene UST. The site also consists of
a single-story convenience store building and fuel dispensers associated with the USTs. Surface cover at
the site consists mostly of asphalt and concrete in the fueling and driveway areas. The surface cover on
the east portion of the property, behind the convenience store building, consists mostly of grass. A
Limited Site Assessment Risk Classification and Land Use Form is included in Appendix A.

Properties within 1,500 feet of the site are mainly commercial and residential on the east side Highway 321A
and mainly industrial on the west side of Highway 321A. The closest residential building is located adjacent
to the northeast of the subject site. The closest place of public assembly is the Sawmills Town Hall located
approximately 1,250 feet south-southeast of the release area.

The subject property is zoned as H-B (Highway Business). Areas surrounding the site are zoned as H-B, R-
15 (Residential), and G-M (General Manufacturing).

4.0 SITE CHARACTERISTICS

4.1 Regional Geology

According to the Geologic Map of North Carolina, produced by the State of North Carolina in 1985, the
site lies in the Inner Piedmont Belt of the Piedmont Physiographic Province of North Carolina. The rock
types of the Inner Piedmont have been identified as predominatly mica shist with a variety of other rock
types depending on location. The Inner Piedmont is characterized as crystalline meta-sedimantary rock.
The shallow subsurface in most areas of the Piedmont contains residual soil overburden, including
structure-free residuum, saprolite, and partially weathered rock (PWR) that derive from in-place
weathering of the crystalline bedrock. Occasional areas containing recent deposits of alluvium in the
uppermost subsurface are found near streams and rivers. Saprolite and PWR typically contain some relict
structures from the original rock material. Depth to rock ranges from ground surface at occasional
outcrops to depths of greater than 100 feet in areas of easily weathered rock.

Yogi Foods ATC Associates of North Carolina, P.C.
Phase II LSA Report 6 October 24, 2014

4.2 Site Geology

Shallow subsurface soils observed during drilling activities were described as sandy clay, sandy silt, and
silty clay to a termination depth of approximately 30 feet below grade. Soil boring logs from the Phase II
LSA are included as Appendix B.

4.3 Regional Hydrogeology

The shallow aquifer occurrence varies in depth from ground surface at springs, creeks, and rivers to as
deep as 50 feet or more beneath upland surfaces in some parts of the Piedmont. Water in the alluvium or
unconsolidated residual material, including saprolite and PWR, usually behaves as an unconfined aquifer,
or water table, and will yield water with head elevation equivalent to the first elevation where water was
encountered. Permeability varies with lithology and is typically relatively low in residual soils, with
higher permeability in saprolite or PWR due to relict rock texture and variable susceptibility to
weathering exhibited by different minerals in the rock. Groundwater flow in residual soils or alluvium is
usually in rough concurrence with local topographic conditions and is toward local drainage features.

The bedrock fractures or other planar features of the Piedmont Physiographic Province generally
constitute the bedrock aquifer, with the surrounding rock material being effectively impermeable. Along
with fractures, contacts between rock bodies probably constitute zones of significant groundwater
occurrence in the bedrock. The surrounding material and overlying residuum tend to make the bedrock
aquifer a semi-confined aquifer. That is, the overlying water and soil weight normally results in pressure
that causes water in a borehole, which intersects a fracture or other feature, to rise above the elevation of
the fracture or feature. Modern water supply wells in the Piedmont, likely including those in the site
vicinity, are typically installed with a surface casing through the unconsolidated material, and an open
borehole into the bedrock where water-bearing fractures are encountered.

4.4 Site Hydrogeology

Depth to groundwater in site monitoring wells MW-1 through MW-4 ranged from 15.55 feet to 23.05 feet
below TOC on August 6, 2014. Free product was not observed in the site wells. Based on elevation data
obtained on August 6, 2014, groundwater flow appears to be generally towards the east at an average
horizontal hydraulic gradient of 0.009 along a flow path that crosses the source. Well construction details
and groundwater elevation data are summarized in Table B-7.

Yogi Foods ATC Associates of North Carolina, P.C.
Phase II LSA Report 7 October 24, 2014

5.0 SUBSURFACE INVESTIGATION

5.1 Soil Sampling

On June 30, 2006, soil samples were collected at nine locations (YF-1 through YF-9) and submitted for
laboratory analysis as part of a due diligence investigation. Laboratory analytical results of a soil sample
collected adjacent to a gasoline and diesel dispenser (YF-4) indicated a TPH – GRO concentration that
exceeded the NCDENR action level of 10 mg/kg. Boring locations are indicated on Figure 4 and soil
analytical results are provided in Table B-3.

On August 10, 2006, split spoon samplers were advanced at a location adjacent to the gasoline and diesel
dispenser, in the vicinity of soil sample YF-4. The boring location is indicated on Figure 4. Continuous
soil samples were collected from grade to a depth of 25 feet below grade. The soil samples were
characterized for lithology and screened with a photo-ionization detector (PID). Petroleum compounds
were reported in the soil samples at concentrations above soil-to-groundwater MSCCs. Soil analytical
results are provided in Table B-3.

Soil samples were collected on August 5, 2014, during installation of wells MW-2 through MW-4 and
characterized in the field for lithology and screened with a PID. Soil boring logs are provided in
Appendix B. Soil samples were not submitted for laboratory analysis, per NCDENR guidelines for Phase
II LSAs.

5.2 Well Installation

Three groundwater monitoring wells (MW-2 through MW-4) were installed at the subject site during the
Phase II LSA. Due to the presence of multiple underground and overhead obstructions, the location of
well MW-3 was adjusted in the field. The wells were installed to a depth of 30 feet below grade, with 15
feet of 2-inch diameter 0.010-inch slotted screen and 15 feet of PVC riser casing. The wells were secured
at the surface with steel manhole covers and concrete pads. Boring logs and well records are provided in
Appendix B.

ATC returned to the site on August 6, 2014, to gauge and collect groundwater samples from wells MW-1
through MW-4. Depths to groundwater at the site ranged from 15.55 to 23.05 feet below TOC.
Groundwater flow was generally towards the east at the site based on data obtained on August 6, 2014. A
groundwater elevation map is provided as Figure 5.

Yogi Foods ATC Associates of North Carolina, P.C.
Phase II LSA Report 8 October 24, 2014

Prior to sampling, each well was purged of three standing water columns, or until the well was purged dry.
Samples were then collected with new disposable bailers and poured directly into laboratory-provided
containers with appropriate preservatives. The samples were placed in a chilled cooler and submitted to
North Carolina-accredited Pace Analytical Services, Inc. of Huntersville, North Carolina, using proper chain-
of-custody procedures for laboratory analyses. The groundwater samples were analyzed for VOCs by EPA
Method 6200B, semi-VOCs by EPA Method 625, lead by EPA Method 6010, ethylene dibromide (EDB) by
EPA Method 504.1, and MADEP VPH and extractable petroleum hydrocarbons (EPH).

Petroleum compounds were reported above NCDENR 2L Standards in wells MW-1, MW-2, and MW-4.
Concentrations of lead were reported above the 2L Standard in wells MW-1 through MW-4. The
concentrations of benzene and EDB reported in well MW-1 exceeded their respective GCLs. Groundwater
analytical data is presented in Table B-4 and on Figures 6 through 9. The laboratory analytical report is
provided in Appendix C.

6.0 CONCLUSIONS

ATC conducted a Phase II LSA at the Yogi Foods site in August 2014 to obtain groundwater flow and
contaminant information. Groundwater contaminant concentrations were identified above 2L Standards in
site monitoring wells, and benzene and EDB were identified in monitoring well MW-1 above their
respective GCLs. Based on the concentrations of groundwater contamination, the site would be ranked as
intermediate risk. However, due to a potential water supply well located within 250 feet of the site, the
incident has been assigned a high risk. ATC recommends additional assessment to delineate the extent of
the petroleum release in soil and groundwater. Potential exists to abandon water supply wells and connect
the users to municipal supply, if not already provided, or to conduct remediation of groundwater impact to
lower site risk.

TABLES
Table B‐1: Site History ‐ UST System and Other Release Informatio
Revision Date: 9/19/14 Incident Number and Name: 28491/Yogi Foods
UST ID Number Current/Last Contents Previous Contents
Capacity 
(gallons)
Construction 
Details
Tank 
Dimensions
Description of 
Associated Piping and 
Pumps
Date Tank 
Installed Status of UST
Was Release 
Associated with 
the UST System?
A1 Gasoline Gasoline 8,000 Steel unknown DW Steel/FRP 4/30/1985 In Use Unknown
A2 Gasoline Gasoline 8,000 Steel unknown DW Steel/FRP 4/30/1985 In Use Unknown
A3 Diesel Diesel 8,000 Steel unknown DW Steel/FRP 4/30/1985 In Use Unknown
A4 Kerosene Kerosene 2,000 Steel unknown DW Steel/FRP 2/5/1976 In Use No
AST ID Number Current/Last Contents Previous Contents
Capacity 
(gallons)
Construction 
Details
Tank 
Dimensions
Description of 
Associated Piping and 
Pumps
Date Tank 
Installed Status of AST
Was Release 
Associated with 
the AST System?
None Associated With This Site
Table B‐2: Site History ‐ UST Owner/Operator and Other Responsible Party Information
Revision Date: 10/8/14 Incident Number and Name: 28491/Yogi Foods
UST ID Number A1, A2, A3, A4 Facility ID Number 0‐007809
City State Zip Telephone Number
Unknown Unknown Unknown Unknown
City State Zip Telephone Number
Hudson NC 28638 919‐460‐3195
UST ID Number A1, A2, A3, A4 Facility ID Number 0‐007809
City State Zip Telephone Number
North Wilkesboro NC 28659 336‐667‐9453
City State Zip Telephone Number
North Wilkesboro NC 28659 336‐667‐9453
UST ID Number A1, A2, A3, A4 Facility ID Number 0‐007809
City State Zip Telephone Number
Cary NC 27511 919‐462‐1100
City State Zip Telephone Number
Cary NC 27511 919‐462‐1100
UST ID Number A1, A2, A3, A4 Facility ID Number 0‐007809
City State Zip Telephone Number
Lenoir NC 28645 828‐758‐4401
City State Zip Telephone Number
Lenoir NC 28645 828‐758‐4401
UST ID Number A1, A2, A3, A4 Facility ID Number 0‐007809
City State Zip Telephone Number
Cliffside NC 28024 704‐453‐7351
City State Zip Telephone Number
Cliffside NC 28024 704‐453‐7351
Street Address
PO Box 307, Highway 120
Street Address
PO Box 307, Highway 120
Name of Operator Dates of Operation (MM/DD/YY to MM/DD/YY)
Petroleum World, Inc.04/30/1986 to 03/30/1997
Street Address
110 Nuway Circle
Name of Owner Dates of Operation (MM/DD/YY to MM/DD/YY)
Petroleum World, Inc.04/30/1986 to 03/30/1997
Street Address
110 Nuway Circle
Name of Operator Dates of Operation (MM/DD/YY to MM/DD/YY)
Beall Oil Company/Blue Ridge Energies LLC 03/31/1997 to 04/04/2005
Street Address
110 MacKenan Drive, Suite 300
Name of Owner Dates of Operation (MM/DD/YY to MM/DD/YY)
Beall Oil Company/Blue Ridge Energies LLC 03/31/1997 to 04/04/2005
110 MacKenan Drive, Suite 300
Name of Operator Dates of Operation (MM/DD/YY to MM/DD/YY)
Cary Oil Company 04/05/2005 to 05/17/2009
Name of Owner Dates of Operation (MM/DD/YY to MM/DD/YY)
Cary Oil Company 04/05/2005 to 05/17/2009
Street Address
Tar Heel Oil II, Inc.05/18/2009 to Unknown Date
Street Address
320 9th Street, PO Box 608
Tar Heel Oil II, Inc.05/18/2009 to Unknown Date
Street Address
320 9th Street, PO Box 608
Name of Operator Dates of Operation (MM/DD/YY to MM/DD/YY)
4018 Highway 321A
Street Address
Unknown
Street Address
Name of Owner Dates of Operation (MM/DD/YY to MM/DD/YY)
Dates of Operation (MM/DD/YY to MM/DD/YY)
Dates of Operation (MM/DD/YY to MM/DD/YY)Name of Owner
Unknown Date to Present
Name of Operator
AJ Patel
HHA Development LLC Unknown Date to Present
Table B‐3: Summary of Soil Sampling Results
Revision Date: 9/19/1 Incident Number and Name: 28491/Yogi Food Facility ID #: 0‐00780
8015C
Sample ID
Date 
Collected
Source 
Area
Sample 
Depth 
(ft BGS)
Incident 
Phase
YF‐1 6/30/2006 UST 10 Phase II ESA 3.6 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
YF‐2 6/30/200 US 10 Phase II ESA 3.6 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
YF‐3 6/30/200 US 10 Phase II ESA 3.1 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
YF‐4 6/30/200 Dispenser 3 Phase II ESA 11.3 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
YF‐5 6/30/200 Dispenser 3 Phase II ESA 5.0 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
YF‐6 6/30/200 Dispenser 3 Phase II ESA 3.2 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
YF‐7 6/30/200 Dispenser 3 Phase II ESA 3.8 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
YF‐8 6/30/200 US 10 Phase II ESA 3.4 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
YF‐9 6/30/200 US 10 Phase II ESA 2.7 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
MW‐1S 0‐5 8/10/200 Dispenser 0‐5 Phase I LSA NR 7.6 47 36 227 <0.0049 230 <0.0049 12 3.0 2.0 <12 32 29 22 23 60 89 54
MW‐1S 5‐1 8/10/200 Dispenser 5‐10 Phase I LSA NR <0.29 17 8.6 72 <0.29 <5.8 <0.29 1.8 2.0 0.93 <230 660 760 23 <19 230 990 68
MW‐1S 10‐15 8/10/200 Dispenser 10‐15 Phase I LSA NR 0.1 5.3.0 26 0.01 0.79 <0.0063 0.49 1.1 0.48 160 200 230 22 <20 73 303 222
MW‐1S 15‐2 8/10/200 Dispenser 15‐20 Phase I LSA NR 0.02 0.2 0.11 0.99 0.015 <4.7 <0.0047 0.58 <0.22 <0.22 27 49 59 <13 <19 14 73 49
MW‐1S 20‐25 8/10/200 Dispenser 20‐25 Phase I LSA NR 6.6 <0.0063 14 95 <0.0063 <6.3 0.0078 <0.013 0.64 0.37 60 84 110 <14 <21 <14 110 84
NE 0.0056 4.3 4.9 4.6 0.0019 24 0.02 0.36 3.6 0.16 68 NE NE NE Immobile NE 540 31
NE 18 1200 1560 3129 7 14000 49 10000 63 313 939 NE NE NE 31000 NE 1500 469
NE 164 32000 40000 81760 63 36000 440 40000 1635 8176 24528 NE NE NE 81000 NE 40000 1226
NCDENR Action Limit (mg/kg)10 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
MSCC = maximum soil contaminant concentration
ft BGS = feet below ground surfac
Results in mg/kg
NE = Not Established
NA = Not Applicabl
NR = Not Requested
Concentrations in bold exceeded the NCDENR action limit or soil‐to‐groundwater MSC
Concentrations in bold and italics exceeded the residential MSC
C9
‐C1
2
 Al
i
p
h
a
t
i
c
s
C9
‐C1
8
 Al
i
p
h
a
t
i
c
s
C9
‐C2
2
 Al
i
p
h
a
t
i
c
s
VPH/EPH
1,
2
‐Dic
h
l
o
r
o
e
t
h
a
n
e
Ch
l
o
r
o
m
e
t
h
a
n
e
EPA Method 8260B MADEP EPH
C1
1
‐C2
2
 Ar
o
m
a
t
i
c
s
C1
9
‐C3
6
 Al
i
p
h
a
t
i
c
s
C9
‐C1
8
 Al
i
p
h
a
t
i
c
s
EPA Method 8270
2‐Me
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
Na
p
h
t
h
a
l
e
n
e
Ac
e
t
o
n
e
MADEP VPH
C5
‐C8
 Al
i
p
h
a
t
i
c
s
C9
‐C1
0
 Ar
o
m
a
t
i
c
s
Vin
y
l
 Ac
e
t
a
t
e
Xy
l
e
n
e
s
Et
h
y
l
b
e
n
z
e
n
e
Analytical Method (e.g. VOC by EPA 8260)
Contaminant of Concern
To
l
u
e
n
e
Be
n
z
e
n
e
Industrial/Commercial MSCC (mg/kg)
TP
H
 GR
O
Soil‐to‐Groundwater MSCC (mg/kg)
Residential MSCC (mg/kg)
Table B‐4: Summary of Groundwater Sampling Result
Revision Date: 9/19/1 Incident Number and Name: 28491/Yogi Food Facility ID #: 0‐00780
625 504.1 3030C
Well ID Date Collected Sample ID
Incident 
Phase
MW‐1 8/11/2006 MW‐1 Phase I LSA 6,300 11,000 580 4,400 <100 NR <20 <100 <100 NR NR NR NR <20 <40 <20 NR 38,000 5,300 12,000 NR NR NR NR NR NR 555
MW‐1 8/6/2014 MW‐1 Phase II LSA 13,500 26,900 1,120 6,910 <100 <100 950 180 454 <100 167 1,160 356 <100 <1,000 <100 353 87,300 <25,000 <25,000 <100 <100 533 ND 533 701 228
MW‐2 8/6/2014 MW‐2 Phase II LSA 279 1,720 944 4,030 19.5 <10.0 <10.0 <10.0 724 70.6 120 814 201 <10.0 <100 <10.0 404 5,370 <5,000 19,600 <100 <100 710 19,600 710 0.075 1,900
MW‐3 8/6/2014 MW‐3 Phase II LSA <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 0.66 5.0 6.5 <6.2 <50.0 <50.0 <50.0 <100 <100 <100 ND ND <0.022 617
MW‐4 8/6/2014 MW‐4 Phase II LSA 36.4 35.1 651 1,101 <5.0 28.0 74.8 11.9 584 161 420 1,440 654 <5.0 <50.0 <5.0 342 9,470 4,720 16,200 197 <100 744 16,397 5,464 0.054 1,680
1 600 600 500 20 70 0.4 70 6 70 70 400 400 NE 100 70 6 400 NE NE NE 10,000 NE 700 200 0.02 15
5,000 260,000 84,500 85,500 20,000 8,500 400 70,000 6,000 25,000 30,000 28,500 25,000 NE 100,000 70,000 6,000 NE NE NE NE NE NE NE NE 50 15,000
Results in ug/L
Concentrations in bold exceeded the 2L Standar
Concentrations in bold and italics exceeded the GC
J = Estimated Value
NE = Not Established
NR = Not Requested
ND = Not Detected
Le
a
d
MADEP EPH
C9
‐C1
8
 Ali
p
h
a
t
i
c
s
Ch
l
o
r
o
f
o
r
m
ED
B
MADEP VPH
C5
‐C8
 Ali
p
h
a
t
i
c
s
C9
‐C1
0
 Ar
o
m
a
t
i
c
s
C9
‐C1
2
 Ali
p
h
a
t
i
c
s
C9
‐C1
8
 Ali
p
h
a
t
i
c
s
C9
‐C2
2
 Ar
o
m
a
t
i
c
s
VPH/EPH
C1
9
‐C3
6
 Ali
p
h
a
t
i
c
s
C1
1
‐C2
2
 Ar
o
m
a
t
i
c
s
Na
p
h
t
h
a
l
e
n
e
GCL = gross contamination level
Contaminant of Concern
1,
2
,
4
‐Tr
i
m
e
t
h
y
l
b
e
n
z
e
n
e
To
l
u
e
n
e
Xy
l
e
n
e
s
,
 To
t
a
l
Na
p
h
t
h
a
l
e
n
e
1,
2
‐Dic
h
l
o
r
o
e
t
h
a
n
e
2L Standard
n‐Pr
o
p
y
l
b
e
n
z
e
n
e
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Br
o
m
o
d
i
c
h
l
o
r
o
m
e
t
h
a
n
e
Br
o
m
o
m
e
t
h
a
n
e
Be
n
z
e
n
e
Analytical Method (e.g. EPA 601)
Dii
s
o
p
r
o
p
y
l
 et
h
e
r
MT
B
E
1,
3
,
5
‐Tr
i
m
e
t
h
y
l
b
e
n
z
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
se
c
‐Bu
t
y
l
b
e
n
z
e
n
e
EPA Method 624/6200B
Table B‐5: Public and Private Water Supply Well and Other Receptor Information
Revision Date: 9/19/14 Incident Number and Name: 28491/Yogi Foods Facility ID #: 0‐007809
Gene and Sandra Duncan
5124 Bloomfield Dr, Granite Falls, NC 28630
Jake and Hilda Fletcher
2342 Adams Dr, Hudson, NC 28638
Cora Novella Adams
PO Box 322, Granite Falls, NC 28630
Criss and Loretta Wilson
2343 Adams Dr, Hudson, NC 28638
Iona Baldwin
2347 Adams Dr, Hudson, NC 28638
George and Ila Wilcox
2335 Adams Dr, Hudson, NC 28638
Charles Gragg
4002 US Hwy 321A, Hudson, NC 28638
Charles Gragg
4002 US Hwy 321A, Hudson, NC 28638
Mr. and Mrs. Benfield
4102 US Hwy 321A, Granite Falls, NC 28630
Paul Dishman
2049 Jessica Ln, Hudson, NC 28638
Floyd and Theresa Annas
3968 US Hwy 321A, Hudson, NC 28638
Gladys Greene
2624 Mission Rd, Hudson, NC 28638
Casey Wallace
PO Box 152, Granite Falls, NC 28630
Charles Chester
4110 Ardmore Ln, Hudson, NC 28638
Earnest and Diana Harris
612 S Government St, Lincolnton, NC 28092
Poplar Fish Lake Not Applicable 4243 Poplar Lake Drive Not Available Not Applicable Not Applicable Not Applicable 1,100 ‐
Receptor survey conducted on 9/19/2012
Well not in use
Well not in use
WSW‐15 4101 Ardmore Lane Not Available Inactive Unknown Unknown 1,470
1,155 Well not in use
WSW‐14 4110 Ardmore Lane Not Available Inactive Unknown Unknown 1,260
WSW‐13 2630 Mission Road Not Available Inactive Unknown Unknown
WSW‐12 2624 Mission Road Not Available Inactive Unknown Unknown 1,040 Well not in use; pump removed; well house used for 
storage
WSW‐11 3968 US Hwy 321A Not Available Inactive Unknown Unknown 1,310 Well not in use; pump removed; well under brick patio
715 Well not in use; house used as rental
WSW‐10 4303 Helena Street Not Available Inactive Unknown Unknown 970
WSW‐9 4253 Helena Street Not Available Inactive Unknown Unknown
Well not in use
WSW‐8 4002 US Hwy 321A 828‐612‐6653 Inactive ~120 Unknown 535 Well not in use; potential future use for irrigation
WSW‐7 4002 US Hwy 321A 828‐612‐6653 Inactive Unknown Unknown 495 Well not in use; pump removed; well located under 
house and filled with dirt and rocks
430 Well not in use
WSW‐6 2335 Adams Drive Not Available Inactive Unknown Unknown 430
WSW‐5 2347 Adams Drive Not Available Inactive Unknown Unknown
Well not in use
WSW‐4 2343 Adams Drive 828‐396‐1540 Active Unknown Unknown 315 Well used for irrigation only
WSW‐3 2339 Adams Drive 828‐396‐3815 Inactive 28 3‐28 255 Well not in use
WSW‐2 2342 Adams Drive Not Available Inactive Unknown Unknown 300 Well not in use
Well Screen 
Interval
Approx. distance 
from source area of 
release (ft) Comments
WSW‐1 2338 Adams Drive 828‐728‐9694 Inactive Unknown Unknown
Supply Well ID Property Owner Contact Information Property Address Phone Number Well Use
Well Depth (ft 
bgs)
190 Potential well; not in use
Table B‐7: Monitoring Well Construction Information
Revision Date: 9/19/14 Incident Number and Name: 28491/Yogi Foods Facility ID #: 0‐007809
Well ID
Date 
Installed
Date GW 
Measured
Casing 
Diameter 
(in.)
Casing 
Depth (ft)
Screened 
Interval
Total 
Depth
TOC 
Elevation*
Depth to 
Water 
from TOC
Free Product 
Thickness**
Groundwater 
Elevation*
Comments         
dO (ppm)/pH
8/11/2006 26.82 0.00 67.68 Unknown
8/6/2014 22.27 0.00 72.23 7.44/4.94
MW‐2 8/5/2014 8/6/2014 2 15 15‐30 30 94.60 23.05 0.00 71.55 2.38/5.44
MW‐3 8/5/2014 8/6/2014 2 15 15‐30 30 94.78 22.40 0.00 72.38 1.75/6.07
MW‐4 8/5/2014 8/6/2014 2 15 15‐30 30 87.02 15.55 0.00 71.47 1.70/5.98
** If free product is present in well, groundwater elevation is calculated by [Top of Casing Elevation‐Depth to Water]+[free product thickness x 0.8581]
TOC = Top of Casing
* All measurements are feet Below Ground Surface (ft. BGS).
28 94.50MW‐1 8/10/2006 1 13 13‐28

FIGURES

US

H
I
G
H
W
A
Y

3
2
1
A
ADA
M
S

D
R
I
V
E
DIR
T

R
O
A
D
DISPENSER
CANOPY
STORE
STORE
UST
BASIN
GRASS
ASPHALT
CONCRETE
GRASS
MW-1
MW-2
MW-3
MW-4
KEROSENE
DISPENSER
KEROSENE
UST
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
S
S
S
S
S
S
S
S
S
S
S
S
E
E
E
E
E
S
S
S
S
S
S
S
S
S
S
S
E
E
E
EE
E
E
E
E
LEGEND
PR
O
J
E
C
T

N
O
.
NO
T
E
S
:
DA
T
E
TIT
L
E
SC
A
L
E
RE
V
.

B
Y
PR
E
P
.

B
Y
CA
D

F
I
L
E
DC
S
A

I
D
TYPE II MONITORING WELL
E ELECTRIC LINE
W WATER LINE
TELEPHONE/TV LINE
S SEWER LINE
CATHODIC PROTECTION
PRODUCT PIPING
500'
RADI
U
S
1,000
'
RADI
U
S
1,500
'
RADI
U
S
WSW-1
WSW-2
WSW-3
WSW-4
WSW-5
WSW-7
WSW-8
WSW-9
WSW-10
WSW-11
WSW-12
WSW-13
WSW-14
WSW-15
WSW-6
Source Area
PR
O
J
E
C
T

N
O
.
NO
T
E
S
:
DA
T
E
TIT
L
E
SC
A
L
E
RE
V
.

B
Y
PR
E
P
.

B
Y
CA
D

F
I
L
E
DC
S
A

I
D
Inactive Water Supply Well
LEGEND
Active Water Supply Well
(Used for Irrigation Only)

APPENDIX A

LIMITED SITE ASSESSMENT RISK CLASSIFICATION AND
LAND USE FORM

Site Name: Yogi Foods
NCDENR Incident No. 28491
NCDENR Facility I.D. No. 0-007809 Appendix A Page 1

Limited Site Assessment Risk Classification and Land Use Form

Part I – Groundwater/Surface Water/Vapor Impacts

High Risk
1. Has the release contaminated any water supply well including any well used for non-
drinking purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source
area of the release? NO

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars,
industrial cooling water, filling swimming pools) located within 250 feet of the
source area of the release? YES

4. Does groundwater within 500 feet of the source area of the release have the potential
for future use (there is no other source of water supply other than the groundwater)? NO

5. Do vapors from the release pose a threat of explosion because of accumulation of the
vapors in a confined space or pose any other serious threat to public health, public
safety or the environment? NO
If yes, describe. N/A

6. Are there any other factors that would cause the release to pose an imminent danger
to public health, public safety, or the environment? NO
If yes, describe. N/A

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release?
NO
If YES, does the maximum groundwater contaminant concentration exceed the
surface water quality standards and criteria found in 15A NCAC 2B .0200 by a
factor of 10? N/A

8. Is the source area of the release located within an approved or planned wellhead
protection area as defined in 42 USC 300h-7(e)? NO
If yes, describe. N/A

9. Is the release located in the Coastal Plain physiographic region as designated on a
map entitled “Geology of North Carolina” published by the Department in 1985? NO
If YES, is the source area of the release located in an area in which there is recharge
to an unconfined or semi-confined deeper aquifer that is being used or may be used
as a source of drinking water?
If YES, describe. N/A
Site Name: Yogi Foods
NCDENR Incident No. 28491
NCDENR Facility I.D. No. 0-007809 Appendix A Page 2

10. Do the levels of groundwater contamination for any contaminant exceed the gross
contamination levels (see Table 9) established by the Department? YES

Part II - Land Use

Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.

1. Does the property contain one or more primary or secondary residences (permanent
or temporary)? NO
Describe. No, the site consisted of a convenience store with petroleum retail.

2. Does the property contain a school, daycare center, hospital, playground, park,
recreation area, church, nursing home, or other place of public assembly? NO
Describe. No, the site consisted of a convenience store with petroleum retail.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business
space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and
development, chemical/petroleum bulk storage, etc.) enterprise, an inactive
commercial or industrial enterprise, or is the land undeveloped? YES
Describe. The site consisted of a convenience store with petroleum retail.

4. Do children visit the property? YES
Explain. Yes, children with their parents may visit the property.
Is access to the property reliably restricted consistent with its use (e.g., by fences,
security personnel or both)? NO
Explain.
No, the site is accessible and is not surrounded by a fence and is not secured.

5. Does pavement, buildings, or other structures cap the contaminated soil? YES
Describe. Yes, the majority of the site is covered with concrete and asphalt.

If yes, what mechanisms are in place or can be put into place to ensure that the
contaminated soil will remain capped in the foreseeable future? Contaminated soil
has been identified at the site, but the site will likely remain a petroleum service
station with concrete and asphalt cover.

6. What is the zoning status of the property? H-B (Highway Business)

Site Name: Yogi Foods
NCDENR Incident No. 28491
NCDENR Facility I.D. No. 0-007809 Appendix A Page 3

7. Is the use of the property likely to change in the next 20 years? NO
Explain. No, the site has been used as a petroleum service station and other
commercial uses for approximately 30 years and the owner does not have plans to
change the use of the property.

Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release
(excludes property containing source area of the release):

1. What is the distance from the source area of the release to the nearest primary or
secondary residence (permanent or temporary)? The nearest residence is located
adjacent to the northeast of the subject site.

2. What is the distance from the source area of the release to the nearest school,
daycare center, hospital, playground, park, recreation area, church, nursing home or
other place of public assembly? The Sawmills Town Hall is located approximately
1,250 feet south-southeast of the subject site.

3. What is the zoning status of properties in the surrounding area? H-B, R-15
(Residential), and G-M (General Manufacturing).

4. Briefly characterize the use and activities of the land in the surrounding area. The
surrounding area is used mainly for commercial and residential purposes, and an
industrial property is located on the west side of Highway 321A, directly across
from the site.

APPENDIX B

SOIL BORING LOGS AND WELL RECORDS
SOIL BORING LOG
PROJECT NAME:Yogi Foods BORING I.D.:MW-2
PROJECT NO.: 89.03451.1043 DATE(S) DRILLED: 8/5/2014
PROJECT LOCATION:4018 Highway 321A DRILLING CONTR.: Carolina Soil Investigations LLC
Hudson, NC DRILL METHOD: Hollow Stem Auger
BORING DIAMETER: ~8"
CLIENT: Cary Oil Company
LOGGED BY:JB

DESCRIPTIVE LOG (page 1 of 1)
SAMPLE PID/FID GRAPHIC DEPTH
INTERVAL (ppm) COLUMN (FT)DESCRIPTION OF MATERIAL
1.0 1.5' asphalt and 1.5' backfill then red/brown silty clay, dry, no odor
2.0
3.0
4.0
0.0 5.0
6.0 Dark brown silty clay, damp, no odor
7.0
8.0
9.0
0.0 10.0
11.0 Red brown sandy silt, damp, no odor
12.0
13.0
14.0
0.0 15.0
16.0
17.0
18.0
19.0
0.0 20.0
21.0
22.0
▼23.0
24.0
0.0 25.0
26.0 Red brown sandy silt, damp, slight odor
27.0
28.0
29.0
7.6 30.0
31.0 Boring terminated at 30 feet bgs
32.0
33.0
34.0
35.0
36.0
37.0
38.0
39.0
40.0
41.0
42.0
43.0
44.0
45.0
46.0
47.0
48.0
49.0
50.0
51.0
bgs= BELOW GROUND SURFACE
GRAPHIC COLUMN
▼DEPTH TO WATER
GROUT
SCREEN
* Samples collection interval PHC = Petroleum hrdocarbon odor SAA - Same as ab
SAMPLING METHOD/INTERVAL: Drill Cuttings/5 feet
REMARKS: Total boring depth: 30 ft bgs; screened: 15-30 ft bgs
USCS
BENTONITE
DRILLING METHODSSS-SPLIT SPOON AIR - AIR ROTARY CFA - CONTINUOUS FLIGHT AUGER DC - DRIVEN CASING HA - HAND AUGER HSA - HOLLOW STEM AUGER MD - MUD DRILLING RC - ROCK CORING WR - WATER ROTARY SAMPLING METHODSGP-GEOPROBE
SPLIT SPOON
GROUT
SAND
3417-A Trade Park Court
Charlotte, North Carolina 28217
BENTONITE
BENTONITE
GROUT
SAND
7606 Whitehall Executive Center Drive
Charlotte, North Carolina 28273
SOIL BORING LOG
PROJECT NAME:Yogi Foods BORING I.D.:MW-3
PROJECT NO.: 89.03451.1043 DATE(S) DRILLED: 8/5/2014
PROJECT LOCATION:4018 Highway 321A DRILLING CONTR.: Carolina Soil Investigations LLC
Hudson, NC DRILL METHOD: Hollow Stem Auger
BORING DIAMETER: ~8"
CLIENT: Cary Oil Company
LOGGED BY:JB

DESCRIPTIVE LOG (page 1 of 1)
SAMPLE PID/FID GRAPHIC DEPTH
INTERVAL (ppm) COLUMN (FT)DESCRIPTION OF MATERIAL
1.0 3.5' asphalt then red/brown silty clay, fine gravel, dry, no odor
2.0
3.0
4.0
0.0 5.0
6.0 Red/brown sandy silt, dry, no odor
7.0
8.0
9.0
0.0 10.0
11.0
12.0
13.0
14.0
0.0 15.0
16.0 Brown sandy silt, damp, no odor
17.0
18.0
19.0
0.0 20.0
21.0
22.0
▼23.0
24.0
0.0 25.0
26.0 Brown sandy silt, wet, no odor
27.0
28.0
29.0
0.0 30.0
31.0 Boring terminated at 30 feet bgs
32.0
33.0
34.0
35.0
36.0
37.0
38.0
39.0
40.0
41.0
42.0
43.0
44.0
45.0
46.0
47.0
48.0
49.0
50.0
51.0
bgs= BELOW GROUND SURFACE
GRAPHIC COLUMN
▼DEPTH TO WATER
GROUT
SCREEN
* Samples collection interval PHC = Petroleum hrdocarbon odor SAA - Same as ab
SAMPLING METHOD/INTERVAL: Drill Cuttings/5 feet
REMARKS: Total boring depth: 30 ft bgs; screened: 15-30 ft bgs
USCS
BENTONITE
DRILLING METHODSSS-SPLIT SPOON AIR - AIR ROTARY CFA - CONTINUOUS FLIGHT AUGER DC - DRIVEN CASING HA - HAND AUGER HSA - HOLLOW STEM AUGER MD - MUD DRILLING RC - ROCK CORING WR - WATER ROTARY SAMPLING METHODSGP-GEOPROBE
SPLIT SPOON
GROUT
SAND
3417-A Trade Park Court
Charlotte, North Carolina 28217
BENTONITE
BENTONITE
GROUT
SAND
7606 Whitehall Executive Center Drive
Charlotte, North Carolina 28273
SOIL BORING LOG
PROJECT NAME:Yogi Foods BORING I.D.:MW-4
PROJECT NO.: 89.03451.1043 DATE(S) DRILLED: 8/5/2014
PROJECT LOCATION:4018 Highway 321A DRILLING CONTR.: Carolina Soil Investigations LLC
Hudson, NC DRILL METHOD: Hollow Stem Auger
BORING DIAMETER: ~8"
CLIENT: Cary Oil Company
LOGGED BY:JB

DESCRIPTIVE LOG (page 1 of 1)
SAMPLE PID/FID GRAPHIC DEPTH
INTERVAL (ppm) COLUMN (FT)DESCRIPTION OF MATERIAL
1.0 Grass and topsoil then red/brown sandy silt, dry, no odor
2.0
3.0
4.0
0.0 5.0
6.0 Brown sandy silt, dry, no odor
7.0
8.0
9.0
0.0 10.0
11.0 Brown sandy silt, damp, no odor
12.0
13.0
14.0
0.0 15.0
▼16.0
17.0
18.0
19.0
664 20.0
21.0 Brown sandy silt, wet, no odor
22.0
23.0
24.0
358 25.0
26.0 Brown sandy silt, wet, slight odor
27.0
28.0
29.0
100 30.0
31.0 Boring terminated at 30 feet bgs
32.0
33.0
34.0
35.0
36.0
37.0
38.0
39.0
40.0
41.0
42.0
43.0
44.0
45.0
46.0
47.0
48.0
49.0
50.0
51.0
bgs= BELOW GROUND SURFACE
GRAPHIC COLUMN
▼DEPTH TO WATER
GROUT
SCREEN
* Samples collection interval PHC = Petroleum hrdocarbon odor SAA - Same as ab
SAMPLING METHOD/INTERVAL: Drill Cuttings/5 feet
REMARKS: Total boring depth: 30 ft bgs; screened: 15-30 ft bgs
USCS
BENTONITE
DRILLING METHODSSS-SPLIT SPOON AIR - AIR ROTARY CFA - CONTINUOUS FLIGHT AUGER DC - DRIVEN CASING HA - HAND AUGER HSA - HOLLOW STEM AUGER MD - MUD DRILLING RC - ROCK CORING WR - WATER ROTARY SAMPLING METHODSGP-GEOPROBE
SPLIT SPOON
GROUT
SAND
3417-A Trade Park Court
Charlotte, North Carolina 28217
BENTONITE
BENTONITE
GROUT
SAND
7606 Whitehall Executive Center Drive
Charlotte, North Carolina 28273

APPENDIX C

LABORATORY ANALYTICAL REPORT

#=CL#
August 12, 2014
LIMS USE: FR - CHRISTINE
LIMS OBJECT ID: 92212243
92212243
Project:
Pace Project No.:
RE:
Christine Schaefer
Cardno ATC
7606 Whitehall Executive Cente
Suite 800
Charlotte, NC 28273
Yogi Foods
Dear Christine Schaefer:
Enclosed are the analytical results for sample(s) received by the laboratory on August 06, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 44
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92212243
Yogi Foods
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 44
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92212243
Yogi Foods
Lab ID Sample ID Matrix Date Collected Date Received
92212243001 MW1 Water 08/06/14 09:35 08/06/14 15:30
92212243002 MW2 Water 08/06/14 10:40 08/06/14 15:30
92212243003 MW3 Water 08/06/14 11:45 08/06/14 15:30
92212243004 MW4 Water 08/06/14 11:15 08/06/14 15:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 44
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92212243
Yogi Foods
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92212243001 MW1 EPA 504.1 2 PASI-CJMC
MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 6010 1 PASI-AJMW
EPA 625 58 PASI-CRES
SM 6200B 63 PASI-CMCK
92212243002 MW2 EPA 504.1 2 PASI-CJMC
MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 6010 1 PASI-AJMW
EPA 625 58 PASI-CRES
SM 6200B 63 PASI-CMCK
92212243003 MW3 EPA 504.1 2 PASI-CJMC
MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 6010 1 PASI-AJMW
EPA 625 58 PASI-CRES
SM 6200B 63 PASI-CMCK
92212243004 MW4 EPA 504.1 2 PASI-CJMC
MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 6010 1 PASI-AJMW
EPA 625 58 PASI-CRES
SM 6200B 63 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW1 Lab ID:92212243001 Collected:08/06/14 09:35 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)701 ug/L 08/10/14 14:46 106-93-408/09/14 17:4932.3 1600
Surrogates
1-Chloro-2-bromopropane (S)0 %08/10/14 14:46 301-79-56 S408/09/14 17:4970-130 1600
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 08/12/14 00:54 N208/07/14 08:281001
Aliphatic (C19-C36)ND ug/L 08/12/14 00:54 N208/07/14 08:281001
Aromatic (C11-C22)533 ug/L 08/12/14 00:54 N208/07/14 08:281001
Surrogates
Nonatriacontane (S)51 %08/12/14 00:54 7194-86-708/07/14 08:2840-140 1
o-Terphenyl (S)50 %08/12/14 00:54 84-15-108/07/14 08:2840-140 1
2-Fluorobiphenyl (S)67 %08/12/14 00:54 321-60-808/07/14 08:2840-140 1
2-Bromonaphthalene (S)76 %08/12/14 00:54 580-13-208/07/14 08:2840-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)87300 ug/L 08/12/14 12:41 N225000500
Aliphatic (C09-C12)ND ug/L 08/12/14 12:41 1g,N225000500
Aromatic (C09-C10)ND ug/L 08/12/14 12:41 N225000500
Surrogates
4-Bromofluorobenzene (FID) (S)106 %08/12/14 12:41 460-00-470-130 500
4-Bromofluorobenzene (PID) (S)99 %08/12/14 12:41 460-00-470-130 500
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP
Lead 228 ug/L 08/09/14 00:51 7439-92-108/08/14 15:305.0 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 08/08/14 06:02 83-32-908/07/14 11:215.0 1
Acenaphthylene ND ug/L 08/08/14 06:02 208-96-808/07/14 11:215.0 1
Anthracene ND ug/L 08/08/14 06:02 120-12-708/07/14 11:215.0 1
Benzo(a)anthracene ND ug/L 08/08/14 06:02 56-55-308/07/14 11:215.0 1
Benzo(a)pyrene ND ug/L 08/08/14 06:02 50-32-808/07/14 11:215.0 1
Benzo(b)fluoranthene ND ug/L 08/08/14 06:02 205-99-208/07/14 11:215.0 1
Benzo(g,h,i)perylene ND ug/L 08/08/14 06:02 191-24-208/07/14 11:215.0 1
Benzo(k)fluoranthene ND ug/L 08/08/14 06:02 207-08-908/07/14 11:215.0 1
4-Bromophenylphenyl ether ND ug/L 08/08/14 06:02 101-55-308/07/14 11:215.0 1
Butylbenzylphthalate ND ug/L 08/08/14 06:02 85-68-708/07/14 11:215.0 1
4-Chloro-3-methylphenol ND ug/L 08/08/14 06:02 59-50-708/07/14 11:215.0 1
bis(2-Chloroethoxy)methane ND ug/L 08/08/14 06:02 111-91-108/07/14 11:2110.0 1
bis(2-Chloroethyl) ether ND ug/L 08/08/14 06:02 111-44-408/07/14 11:215.0 1
bis(2-Chloroisopropyl) ether ND ug/L 08/08/14 06:02 108-60-108/07/14 11:215.0 1
2-Chloronaphthalene ND ug/L 08/08/14 06:02 91-58-708/07/14 11:215.0 1
2-Chlorophenol ND ug/L 08/08/14 06:02 95-57-808/07/14 11:215.0 1
4-Chlorophenylphenyl ether ND ug/L 08/08/14 06:02 7005-72-308/07/14 11:215.0 1
Chrysene ND ug/L 08/08/14 06:02 218-01-908/07/14 11:215.0 1
Dibenz(a,h)anthracene ND ug/L 08/08/14 06:02 53-70-308/07/14 11:215.0 1
3,3'-Dichlorobenzidine ND ug/L 08/08/14 06:02 91-94-108/07/14 11:2125.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW1 Lab ID:92212243001 Collected:08/06/14 09:35 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
2,4-Dichlorophenol ND ug/L 08/08/14 06:02 120-83-208/07/14 11:215.0 1
Diethylphthalate ND ug/L 08/08/14 06:02 84-66-208/07/14 11:215.0 1
2,4-Dimethylphenol ND ug/L 08/08/14 06:02 105-67-908/07/14 11:2110.0 1
Dimethylphthalate ND ug/L 08/08/14 06:02 131-11-308/07/14 11:215.0 1
Di-n-butylphthalate ND ug/L 08/08/14 06:02 84-74-208/07/14 11:215.0 1
4,6-Dinitro-2-methylphenol ND ug/L 08/08/14 06:02 534-52-108/07/14 11:2120.0 1
2,4-Dinitrophenol ND ug/L 08/08/14 06:02 51-28-508/07/14 11:2150.0 1
2,4-Dinitrotoluene ND ug/L 08/08/14 06:02 121-14-208/07/14 11:215.0 1
2,6-Dinitrotoluene ND ug/L 08/08/14 06:02 606-20-208/07/14 11:215.0 1
Di-n-octylphthalate ND ug/L 08/08/14 06:02 117-84-008/07/14 11:215.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/08/14 06:02 117-81-708/07/14 11:215.0 1
Fluoranthene ND ug/L 08/08/14 06:02 206-44-008/07/14 11:215.0 1
Fluorene ND ug/L 08/08/14 06:02 86-73-708/07/14 11:215.0 1
Hexachloro-1,3-butadiene ND ug/L 08/08/14 06:02 87-68-308/07/14 11:215.0 1
Hexachlorobenzene ND ug/L 08/08/14 06:02 118-74-108/07/14 11:215.0 1
Hexachlorocyclopentadiene ND ug/L 08/08/14 06:02 77-47-408/07/14 11:2110.0 1
Hexachloroethane ND ug/L 08/08/14 06:02 67-72-108/07/14 11:215.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/08/14 06:02 193-39-508/07/14 11:215.0 1
Isophorone ND ug/L 08/08/14 06:02 78-59-108/07/14 11:2110.0 1
Naphthalene 353 ug/L 08/09/14 00:13 91-20-308/07/14 11:2120.0 4
Nitrobenzene ND ug/L 08/08/14 06:02 98-95-308/07/14 11:215.0 1
2-Nitrophenol ND ug/L 08/08/14 06:02 88-75-508/07/14 11:215.0 1
4-Nitrophenol ND ug/L 08/08/14 06:02 100-02-708/07/14 11:2150.0 1
N-Nitrosodimethylamine ND ug/L 08/08/14 06:02 62-75-908/07/14 11:215.0 1
N-Nitroso-di-n-propylamine ND ug/L 08/08/14 06:02 621-64-708/07/14 11:215.0 1
N-Nitrosodiphenylamine ND ug/L 08/08/14 06:02 86-30-608/07/14 11:2110.0 1
Pentachlorophenol ND ug/L 08/08/14 06:02 87-86-508/07/14 11:2110.0 1
Phenanthrene ND ug/L 08/08/14 06:02 85-01-808/07/14 11:215.0 1
Phenol ND ug/L 08/08/14 06:02 108-95-208/07/14 11:215.0 1
Pyrene ND ug/L 08/08/14 06:02 129-00-008/07/14 11:215.0 1
1,2,4-Trichlorobenzene ND ug/L 08/08/14 06:02 120-82-108/07/14 11:215.0 1
2,4,6-Trichlorophenol ND ug/L 08/08/14 06:02 88-06-208/07/14 11:2110.0 1
Surrogates
Nitrobenzene-d5 (S)70 %08/08/14 06:02 4165-60-008/07/14 11:2110-120 1
2-Fluorobiphenyl (S)58 %08/08/14 06:02 321-60-808/07/14 11:2115-120 1
Terphenyl-d14 (S)84 %08/08/14 06:02 1718-51-008/07/14 11:2111-131 1
Phenol-d6 (S)32 %08/08/14 06:02 13127-88-308/07/14 11:2110-120 1
2-Fluorophenol (S)47 %08/08/14 06:02 367-12-408/07/14 11:2110-120 1
2,4,6-Tribromophenol (S)90 %08/08/14 06:02 118-79-608/07/14 11:2110-137 1
Analytical Method: SM 6200B6200B MSV
Benzene 13500 ug/L 08/08/14 08:43 71-43-2100200
Bromobenzene ND ug/L 08/08/14 08:43 108-86-1100200
Bromochloromethane ND ug/L 08/08/14 08:43 74-97-5100200
Bromodichloromethane ND ug/L 08/08/14 08:43 75-27-4100200
Bromoform ND ug/L 08/08/14 08:43 75-25-2100200
Bromomethane ND ug/L 08/08/14 08:43 74-83-91000200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW1 Lab ID:92212243001 Collected:08/06/14 09:35 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
n-Butylbenzene ND ug/L 08/08/14 08:43 104-51-8100200
sec-Butylbenzene ND ug/L 08/08/14 08:43 135-98-8100200
tert-Butylbenzene ND ug/L 08/08/14 08:43 98-06-6100200
Carbon tetrachloride ND ug/L 08/08/14 08:43 56-23-5100200
Chlorobenzene ND ug/L 08/08/14 08:43 108-90-7100200
Chloroethane ND ug/L 08/08/14 08:43 75-00-3200200
Chloroform ND ug/L 08/08/14 08:43 67-66-3100200
Chloromethane ND ug/L 08/08/14 08:43 74-87-3200200
2-Chlorotoluene ND ug/L 08/08/14 08:43 95-49-8100200
4-Chlorotoluene ND ug/L 08/08/14 08:43 106-43-4100200
1,2-Dibromo-3-chloropropane ND ug/L 08/08/14 08:43 96-12-8200200
Dibromochloromethane ND ug/L 08/08/14 08:43 124-48-1100200
1,2-Dibromoethane (EDB)650 ug/L 08/08/14 08:43 106-93-4100200
Dibromomethane ND ug/L 08/08/14 08:43 74-95-3100200
1,2-Dichlorobenzene ND ug/L 08/08/14 08:43 95-50-1100200
1,3-Dichlorobenzene ND ug/L 08/08/14 08:43 541-73-1100200
1,4-Dichlorobenzene ND ug/L 08/08/14 08:43 106-46-7100200
Dichlorodifluoromethane ND ug/L 08/08/14 08:43 75-71-8100200
1,1-Dichloroethane ND ug/L 08/08/14 08:43 75-34-3100200
1,2-Dichloroethane 950 ug/L 08/08/14 08:43 107-06-2100200
1,1-Dichloroethene ND ug/L 08/08/14 08:43 75-35-4100200
cis-1,2-Dichloroethene ND ug/L 08/08/14 08:43 156-59-2100200
trans-1,2-Dichloroethene ND ug/L 08/08/14 08:43 156-60-5100200
1,2-Dichloropropane ND ug/L 08/08/14 08:43 78-87-5100200
1,3-Dichloropropane ND ug/L 08/08/14 08:43 142-28-9100200
2,2-Dichloropropane ND ug/L 08/08/14 08:43 594-20-7100200
1,1-Dichloropropene ND ug/L 08/08/14 08:43 563-58-6100200
cis-1,3-Dichloropropene ND ug/L 08/08/14 08:43 10061-01-5100200
trans-1,3-Dichloropropene ND ug/L 08/08/14 08:43 10061-02-6100200
Diisopropyl ether 180 ug/L 08/08/14 08:43 108-20-3100200
Ethylbenzene 1120 ug/L 08/08/14 08:43 100-41-4100200
Hexachloro-1,3-butadiene ND ug/L 08/08/14 08:43 87-68-3400200
Isopropylbenzene (Cumene)ND ug/L 08/08/14 08:43 98-82-8100200
Methylene Chloride ND ug/L 08/08/14 08:43 75-09-2400200
Methyl-tert-butyl ether ND ug/L 08/08/14 08:43 1634-04-4100200
Naphthalene 454 ug/L 08/08/14 08:43 91-20-3400200
n-Propylbenzene 167 ug/L 08/08/14 08:43 103-65-1100200
Styrene ND ug/L 08/08/14 08:43 100-42-5100200
1,1,1,2-Tetrachloroethane ND ug/L 08/08/14 08:43 630-20-6100200
1,1,2,2-Tetrachloroethane ND ug/L 08/08/14 08:43 79-34-5100200
Tetrachloroethene ND ug/L 08/08/14 08:43 127-18-4100200
Toluene 26900 ug/L 08/08/14 08:43 108-88-3100200
1,2,3-Trichlorobenzene ND ug/L 08/08/14 08:43 87-61-6400200
1,2,4-Trichlorobenzene ND ug/L 08/08/14 08:43 120-82-1400200
1,1,1-Trichloroethane ND ug/L 08/08/14 08:43 71-55-6100200
1,1,2-Trichloroethane ND ug/L 08/08/14 08:43 79-00-5100200
Trichloroethene ND ug/L 08/08/14 08:43 79-01-6100200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW1 Lab ID:92212243001 Collected:08/06/14 09:35 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Trichlorofluoromethane ND ug/L 08/08/14 08:43 75-69-4200200
1,2,3-Trichloropropane ND ug/L 08/08/14 08:43 96-18-4100200
1,2,4-Trimethylbenzene 1160 ug/L 08/08/14 08:43 95-63-6100200
1,3,5-Trimethylbenzene 356 ug/L 08/08/14 08:43 108-67-8100200
Vinyl chloride ND ug/L 08/08/14 08:43 75-01-4200200
m&p-Xylene 4370 ug/L 08/08/14 08:43 179601-23-1200200
o-Xylene 2540 ug/L 08/08/14 08:43 95-47-6100200
Surrogates
1,2-Dichloroethane-d4 (S)99 %08/08/14 08:43 17060-07-070-130 200
4-Bromofluorobenzene (S)98 %08/08/14 08:43 460-00-470-130 200
Toluene-d8 (S)101 %08/08/14 08:43 2037-26-570-130 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW2 Lab ID:92212243002 Collected:08/06/14 10:40 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)0.075 ug/L 08/09/14 21:26 106-93-408/09/14 17:490.020 1
Surrogates
1-Chloro-2-bromopropane (S)113 %08/09/14 21:26 301-79-5608/09/14 17:4970-130 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 08/12/14 01:26 N208/07/14 08:281001
Aliphatic (C19-C36)ND ug/L 08/12/14 01:26 N208/07/14 08:281001
Aromatic (C11-C22)710 ug/L 08/12/14 01:26 N208/07/14 08:281001
Surrogates
Nonatriacontane (S)57 %08/12/14 01:26 7194-86-708/07/14 08:2840-140 1
o-Terphenyl (S)63 %08/12/14 01:26 84-15-108/07/14 08:2840-140 1
2-Fluorobiphenyl (S)79 %08/12/14 01:26 321-60-808/07/14 08:2840-140 1
2-Bromonaphthalene (S)92 %08/12/14 01:26 580-13-208/07/14 08:2840-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)5370 ug/L 08/12/14 13:04 N25000100
Aliphatic (C09-C12)19600 ug/L 08/12/14 13:04 N25000100
Aromatic (C09-C10)ND ug/L 08/12/14 13:04 N25000100
Surrogates
4-Bromofluorobenzene (FID) (S)105 %08/12/14 13:04 460-00-470-130 100
4-Bromofluorobenzene (PID) (S)98 %08/12/14 13:04 460-00-470-130 100
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP
Lead 1900 ug/L 08/09/14 01:00 7439-92-108/08/14 15:305.0 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 08/09/14 00:41 83-32-908/07/14 11:215.6 1
Acenaphthylene ND ug/L 08/09/14 00:41 208-96-808/07/14 11:215.6 1
Anthracene ND ug/L 08/09/14 00:41 120-12-708/07/14 11:215.6 1
Benzo(a)anthracene ND ug/L 08/09/14 00:41 56-55-308/07/14 11:215.6 1
Benzo(a)pyrene ND ug/L 08/09/14 00:41 50-32-808/07/14 11:215.6 1
Benzo(b)fluoranthene ND ug/L 08/09/14 00:41 205-99-208/07/14 11:215.6 1
Benzo(g,h,i)perylene ND ug/L 08/09/14 00:41 191-24-208/07/14 11:215.6 1
Benzo(k)fluoranthene ND ug/L 08/09/14 00:41 207-08-908/07/14 11:215.6 1
4-Bromophenylphenyl ether ND ug/L 08/09/14 00:41 101-55-308/07/14 11:215.6 1
Butylbenzylphthalate ND ug/L 08/09/14 00:41 85-68-708/07/14 11:215.6 1
4-Chloro-3-methylphenol ND ug/L 08/09/14 00:41 59-50-708/07/14 11:215.6 1
bis(2-Chloroethoxy)methane ND ug/L 08/09/14 00:41 111-91-108/07/14 11:2111.1 1
bis(2-Chloroethyl) ether ND ug/L 08/09/14 00:41 111-44-408/07/14 11:215.6 1
bis(2-Chloroisopropyl) ether ND ug/L 08/09/14 00:41 108-60-108/07/14 11:215.6 1
2-Chloronaphthalene ND ug/L 08/09/14 00:41 91-58-708/07/14 11:215.6 1
2-Chlorophenol ND ug/L 08/09/14 00:41 95-57-808/07/14 11:215.6 1
4-Chlorophenylphenyl ether ND ug/L 08/09/14 00:41 7005-72-308/07/14 11:215.6 1
Chrysene ND ug/L 08/09/14 00:41 218-01-908/07/14 11:215.6 1
Dibenz(a,h)anthracene ND ug/L 08/09/14 00:41 53-70-308/07/14 11:215.6 1
3,3'-Dichlorobenzidine ND ug/L 08/09/14 00:41 91-94-108/07/14 11:2127.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW2 Lab ID:92212243002 Collected:08/06/14 10:40 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
2,4-Dichlorophenol ND ug/L 08/09/14 00:41 120-83-208/07/14 11:215.6 1
Diethylphthalate ND ug/L 08/09/14 00:41 84-66-208/07/14 11:215.6 1
2,4-Dimethylphenol ND ug/L 08/09/14 00:41 105-67-908/07/14 11:2111.1 1
Dimethylphthalate ND ug/L 08/09/14 00:41 131-11-308/07/14 11:215.6 1
Di-n-butylphthalate ND ug/L 08/09/14 00:41 84-74-208/07/14 11:215.6 1
4,6-Dinitro-2-methylphenol ND ug/L 08/09/14 00:41 534-52-108/07/14 11:2122.2 1
2,4-Dinitrophenol ND ug/L 08/09/14 00:41 51-28-508/07/14 11:2155.6 1
2,4-Dinitrotoluene ND ug/L 08/09/14 00:41 121-14-208/07/14 11:215.6 1
2,6-Dinitrotoluene ND ug/L 08/09/14 00:41 606-20-208/07/14 11:215.6 1
Di-n-octylphthalate ND ug/L 08/09/14 00:41 117-84-008/07/14 11:215.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/09/14 00:41 117-81-708/07/14 11:215.6 1
Fluoranthene ND ug/L 08/09/14 00:41 206-44-008/07/14 11:215.6 1
Fluorene ND ug/L 08/09/14 00:41 86-73-708/07/14 11:215.6 1
Hexachloro-1,3-butadiene ND ug/L 08/09/14 00:41 87-68-308/07/14 11:215.6 1
Hexachlorobenzene ND ug/L 08/09/14 00:41 118-74-108/07/14 11:215.6 1
Hexachlorocyclopentadiene ND ug/L 08/09/14 00:41 77-47-408/07/14 11:2111.1 1
Hexachloroethane ND ug/L 08/09/14 00:41 67-72-108/07/14 11:215.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/09/14 00:41 193-39-508/07/14 11:215.6 1
Isophorone ND ug/L 08/09/14 00:41 78-59-108/07/14 11:2111.1 1
Naphthalene 404 ug/L 08/09/14 01:09 91-20-308/07/14 11:2127.8 5
Nitrobenzene ND ug/L 08/09/14 00:41 98-95-308/07/14 11:215.6 1
2-Nitrophenol ND ug/L 08/09/14 00:41 88-75-508/07/14 11:215.6 1
4-Nitrophenol ND ug/L 08/09/14 00:41 100-02-708/07/14 11:2155.6 1
N-Nitrosodimethylamine ND ug/L 08/09/14 00:41 62-75-908/07/14 11:215.6 1
N-Nitroso-di-n-propylamine ND ug/L 08/09/14 00:41 621-64-708/07/14 11:215.6 1
N-Nitrosodiphenylamine ND ug/L 08/09/14 00:41 86-30-608/07/14 11:2111.1 1
Pentachlorophenol ND ug/L 08/09/14 00:41 87-86-508/07/14 11:2111.1 1
Phenanthrene ND ug/L 08/09/14 00:41 85-01-808/07/14 11:215.6 1
Phenol ND ug/L 08/09/14 00:41 108-95-208/07/14 11:215.6 1
Pyrene ND ug/L 08/09/14 00:41 129-00-008/07/14 11:215.6 1
1,2,4-Trichlorobenzene ND ug/L 08/09/14 00:41 120-82-108/07/14 11:215.6 1
2,4,6-Trichlorophenol ND ug/L 08/09/14 00:41 88-06-208/07/14 11:2111.1 1
Surrogates
Nitrobenzene-d5 (S)85 %08/09/14 00:41 4165-60-008/07/14 11:2110-120 1
2-Fluorobiphenyl (S)59 %08/09/14 00:41 321-60-808/07/14 11:2115-120 1
Terphenyl-d14 (S)85 %08/09/14 00:41 1718-51-008/07/14 11:2111-131 1
Phenol-d6 (S)39 %08/09/14 00:41 13127-88-308/07/14 11:2110-120 1
2-Fluorophenol (S)50 %08/09/14 00:41 367-12-408/07/14 11:2110-120 1
2,4,6-Tribromophenol (S)92 %08/09/14 00:41 118-79-608/07/14 11:2110-137 1
Analytical Method: SM 6200B6200B MSV
Benzene 279 ug/L 08/08/14 09:00 71-43-210.0 20
Bromobenzene ND ug/L 08/08/14 09:00 108-86-110.0 20
Bromochloromethane ND ug/L 08/08/14 09:00 74-97-510.0 20
Bromodichloromethane ND ug/L 08/08/14 09:00 75-27-410.0 20
Bromoform ND ug/L 08/08/14 09:00 75-25-210.0 20
Bromomethane ND ug/L 08/08/14 09:00 74-83-910020
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW2 Lab ID:92212243002 Collected:08/06/14 10:40 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
n-Butylbenzene ND ug/L 08/08/14 09:00 104-51-810.0 20
sec-Butylbenzene ND ug/L 08/08/14 09:00 135-98-810.0 20
tert-Butylbenzene ND ug/L 08/08/14 09:00 98-06-610.0 20
Carbon tetrachloride ND ug/L 08/08/14 09:00 56-23-510.0 20
Chlorobenzene ND ug/L 08/08/14 09:00 108-90-710.0 20
Chloroethane ND ug/L 08/08/14 09:00 75-00-320.0 20
Chloroform ND ug/L 08/08/14 09:00 67-66-310.0 20
Chloromethane ND ug/L 08/08/14 09:00 74-87-320.0 20
2-Chlorotoluene ND ug/L 08/08/14 09:00 95-49-810.0 20
4-Chlorotoluene ND ug/L 08/08/14 09:00 106-43-410.0 20
1,2-Dibromo-3-chloropropane ND ug/L 08/08/14 09:00 96-12-820.0 20
Dibromochloromethane ND ug/L 08/08/14 09:00 124-48-110.0 20
1,2-Dibromoethane (EDB)ND ug/L 08/08/14 09:00 106-93-410.0 20
Dibromomethane ND ug/L 08/08/14 09:00 74-95-310.0 20
1,2-Dichlorobenzene ND ug/L 08/08/14 09:00 95-50-110.0 20
1,3-Dichlorobenzene ND ug/L 08/08/14 09:00 541-73-110.0 20
1,4-Dichlorobenzene ND ug/L 08/08/14 09:00 106-46-710.0 20
Dichlorodifluoromethane ND ug/L 08/08/14 09:00 75-71-810.0 20
1,1-Dichloroethane ND ug/L 08/08/14 09:00 75-34-310.0 20
1,2-Dichloroethane ND ug/L 08/08/14 09:00 107-06-210.0 20
1,1-Dichloroethene ND ug/L 08/08/14 09:00 75-35-410.0 20
cis-1,2-Dichloroethene ND ug/L 08/08/14 09:00 156-59-210.0 20
trans-1,2-Dichloroethene ND ug/L 08/08/14 09:00 156-60-510.0 20
1,2-Dichloropropane ND ug/L 08/08/14 09:00 78-87-510.0 20
1,3-Dichloropropane ND ug/L 08/08/14 09:00 142-28-910.0 20
2,2-Dichloropropane ND ug/L 08/08/14 09:00 594-20-710.0 20
1,1-Dichloropropene ND ug/L 08/08/14 09:00 563-58-610.0 20
cis-1,3-Dichloropropene ND ug/L 08/08/14 09:00 10061-01-510.0 20
trans-1,3-Dichloropropene ND ug/L 08/08/14 09:00 10061-02-610.0 20
Diisopropyl ether ND ug/L 08/08/14 09:00 108-20-310.0 20
Ethylbenzene 944 ug/L 08/08/14 09:00 100-41-410.0 20
Hexachloro-1,3-butadiene ND ug/L 08/08/14 09:00 87-68-340.0 20
Isopropylbenzene (Cumene)70.6 ug/L 08/08/14 09:00 98-82-810.0 20
Methylene Chloride ND ug/L 08/08/14 09:00 75-09-240.0 20
Methyl-tert-butyl ether 19.5 ug/L 08/08/14 09:00 1634-04-410.0 20
Naphthalene 724 ug/L 08/08/14 09:00 91-20-340.0 20
n-Propylbenzene 120 ug/L 08/08/14 09:00 103-65-110.0 20
Styrene ND ug/L 08/08/14 09:00 100-42-510.0 20
1,1,1,2-Tetrachloroethane ND ug/L 08/08/14 09:00 630-20-610.0 20
1,1,2,2-Tetrachloroethane ND ug/L 08/08/14 09:00 79-34-510.0 20
Tetrachloroethene ND ug/L 08/08/14 09:00 127-18-410.0 20
Toluene 1720 ug/L 08/08/14 09:00 108-88-310.0 20
1,2,3-Trichlorobenzene ND ug/L 08/08/14 09:00 87-61-640.0 20
1,2,4-Trichlorobenzene ND ug/L 08/08/14 09:00 120-82-140.0 20
1,1,1-Trichloroethane ND ug/L 08/08/14 09:00 71-55-610.0 20
1,1,2-Trichloroethane ND ug/L 08/08/14 09:00 79-00-510.0 20
Trichloroethene ND ug/L 08/08/14 09:00 79-01-610.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW2 Lab ID:92212243002 Collected:08/06/14 10:40 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Trichlorofluoromethane ND ug/L 08/08/14 09:00 75-69-420.0 20
1,2,3-Trichloropropane ND ug/L 08/08/14 09:00 96-18-410.0 20
1,2,4-Trimethylbenzene 814 ug/L 08/08/14 09:00 95-63-610.0 20
1,3,5-Trimethylbenzene 201 ug/L 08/08/14 09:00 108-67-810.0 20
Vinyl chloride ND ug/L 08/08/14 09:00 75-01-420.0 20
m&p-Xylene 2500 ug/L 08/08/14 09:00 179601-23-120.0 20
o-Xylene 1530 ug/L 08/08/14 09:00 95-47-610.0 20
Surrogates
1,2-Dichloroethane-d4 (S)99 %08/08/14 09:00 17060-07-070-130 20
4-Bromofluorobenzene (S)99 %08/08/14 09:00 460-00-470-130 20
Toluene-d8 (S)101 %08/08/14 09:00 2037-26-570-130 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW3 Lab ID:92212243003 Collected:08/06/14 11:45 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)ND ug/L 08/09/14 21:46 106-93-408/09/14 17:490.022 1
Surrogates
1-Chloro-2-bromopropane (S)116 %08/09/14 21:46 301-79-5608/09/14 17:4970-130 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 08/12/14 01:58 N208/07/14 08:281001
Aliphatic (C19-C36)ND ug/L 08/12/14 01:58 N208/07/14 08:281001
Aromatic (C11-C22)ND ug/L 08/12/14 01:58 N208/07/14 08:281001
Surrogates
Nonatriacontane (S)48 %08/12/14 01:58 7194-86-708/07/14 08:2840-140 1
o-Terphenyl (S)75 %08/12/14 01:58 84-15-108/07/14 08:2840-140 1
2-Fluorobiphenyl (S)86 %08/12/14 01:58 321-60-808/07/14 08:2840-140 1
2-Bromonaphthalene (S)98 %08/12/14 01:58 580-13-208/07/14 08:2840-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)ND ug/L 08/11/14 13:12 N250.0 1
Aliphatic (C09-C12)ND ug/L 08/11/14 13:12 N250.0 1
Aromatic (C09-C10)ND ug/L 08/11/14 13:12 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)101 %08/11/14 13:12 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)91 %08/11/14 13:12 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP
Lead 617 ug/L 08/09/14 01:03 7439-92-108/08/14 15:305.0 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 08/08/14 06:57 83-32-908/07/14 11:216.2 1
Acenaphthylene ND ug/L 08/08/14 06:57 208-96-808/07/14 11:216.2 1
Anthracene ND ug/L 08/08/14 06:57 120-12-708/07/14 11:216.2 1
Benzo(a)anthracene ND ug/L 08/08/14 06:57 56-55-308/07/14 11:216.2 1
Benzo(a)pyrene ND ug/L 08/08/14 06:57 50-32-808/07/14 11:216.2 1
Benzo(b)fluoranthene ND ug/L 08/08/14 06:57 205-99-208/07/14 11:216.2 1
Benzo(g,h,i)perylene ND ug/L 08/08/14 06:57 191-24-208/07/14 11:216.2 1
Benzo(k)fluoranthene ND ug/L 08/08/14 06:57 207-08-908/07/14 11:216.2 1
4-Bromophenylphenyl ether ND ug/L 08/08/14 06:57 101-55-308/07/14 11:216.2 1
Butylbenzylphthalate ND ug/L 08/08/14 06:57 85-68-708/07/14 11:216.2 1
4-Chloro-3-methylphenol ND ug/L 08/08/14 06:57 59-50-708/07/14 11:216.2 1
bis(2-Chloroethoxy)methane ND ug/L 08/08/14 06:57 111-91-108/07/14 11:2112.5 1
bis(2-Chloroethyl) ether ND ug/L 08/08/14 06:57 111-44-408/07/14 11:216.2 1
bis(2-Chloroisopropyl) ether ND ug/L 08/08/14 06:57 108-60-108/07/14 11:216.2 1
2-Chloronaphthalene ND ug/L 08/08/14 06:57 91-58-708/07/14 11:216.2 1
2-Chlorophenol ND ug/L 08/08/14 06:57 95-57-808/07/14 11:216.2 1
4-Chlorophenylphenyl ether ND ug/L 08/08/14 06:57 7005-72-308/07/14 11:216.2 1
Chrysene ND ug/L 08/08/14 06:57 218-01-908/07/14 11:216.2 1
Dibenz(a,h)anthracene ND ug/L 08/08/14 06:57 53-70-308/07/14 11:216.2 1
3,3'-Dichlorobenzidine ND ug/L 08/08/14 06:57 91-94-108/07/14 11:2131.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW3 Lab ID:92212243003 Collected:08/06/14 11:45 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
2,4-Dichlorophenol ND ug/L 08/08/14 06:57 120-83-208/07/14 11:216.2 1
Diethylphthalate ND ug/L 08/08/14 06:57 84-66-208/07/14 11:216.2 1
2,4-Dimethylphenol ND ug/L 08/08/14 06:57 105-67-908/07/14 11:2112.5 1
Dimethylphthalate ND ug/L 08/08/14 06:57 131-11-308/07/14 11:216.2 1
Di-n-butylphthalate ND ug/L 08/08/14 06:57 84-74-208/07/14 11:216.2 1
4,6-Dinitro-2-methylphenol ND ug/L 08/08/14 06:57 534-52-108/07/14 11:2125.0 1
2,4-Dinitrophenol ND ug/L 08/08/14 06:57 51-28-508/07/14 11:2162.5 1
2,4-Dinitrotoluene ND ug/L 08/08/14 06:57 121-14-208/07/14 11:216.2 1
2,6-Dinitrotoluene ND ug/L 08/08/14 06:57 606-20-208/07/14 11:216.2 1
Di-n-octylphthalate ND ug/L 08/08/14 06:57 117-84-008/07/14 11:216.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/08/14 06:57 117-81-708/07/14 11:216.2 1
Fluoranthene ND ug/L 08/08/14 06:57 206-44-008/07/14 11:216.2 1
Fluorene ND ug/L 08/08/14 06:57 86-73-708/07/14 11:216.2 1
Hexachloro-1,3-butadiene ND ug/L 08/08/14 06:57 87-68-308/07/14 11:216.2 1
Hexachlorobenzene ND ug/L 08/08/14 06:57 118-74-108/07/14 11:216.2 1
Hexachlorocyclopentadiene ND ug/L 08/08/14 06:57 77-47-408/07/14 11:2112.5 1
Hexachloroethane ND ug/L 08/08/14 06:57 67-72-108/07/14 11:216.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/08/14 06:57 193-39-508/07/14 11:216.2 1
Isophorone ND ug/L 08/08/14 06:57 78-59-108/07/14 11:2112.5 1
Naphthalene ND ug/L 08/08/14 06:57 91-20-308/07/14 11:216.2 1
Nitrobenzene ND ug/L 08/08/14 06:57 98-95-308/07/14 11:216.2 1
2-Nitrophenol ND ug/L 08/08/14 06:57 88-75-508/07/14 11:216.2 1
4-Nitrophenol ND ug/L 08/08/14 06:57 100-02-708/07/14 11:2162.5 1
N-Nitrosodimethylamine ND ug/L 08/08/14 06:57 62-75-908/07/14 11:216.2 1
N-Nitroso-di-n-propylamine ND ug/L 08/08/14 06:57 621-64-708/07/14 11:216.2 1
N-Nitrosodiphenylamine ND ug/L 08/08/14 06:57 86-30-608/07/14 11:2112.5 1
Pentachlorophenol ND ug/L 08/08/14 06:57 87-86-508/07/14 11:2112.5 1
Phenanthrene ND ug/L 08/08/14 06:57 85-01-808/07/14 11:216.2 1
Phenol ND ug/L 08/08/14 06:57 108-95-208/07/14 11:216.2 1
Pyrene ND ug/L 08/08/14 06:57 129-00-008/07/14 11:216.2 1
1,2,4-Trichlorobenzene ND ug/L 08/08/14 06:57 120-82-108/07/14 11:216.2 1
2,4,6-Trichlorophenol ND ug/L 08/08/14 06:57 88-06-208/07/14 11:2112.5 1
Surrogates
Nitrobenzene-d5 (S)77 %08/08/14 06:57 4165-60-008/07/14 11:2110-120 1
2-Fluorobiphenyl (S)76 %08/08/14 06:57 321-60-808/07/14 11:2115-120 1
Terphenyl-d14 (S)87 %08/08/14 06:57 1718-51-008/07/14 11:2111-131 1
Phenol-d6 (S)41 %08/08/14 06:57 13127-88-308/07/14 11:2110-120 1
2-Fluorophenol (S)53 %08/08/14 06:57 367-12-408/07/14 11:2110-120 1
2,4,6-Tribromophenol (S)88 %08/08/14 06:57 118-79-608/07/14 11:2110-137 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 08/08/14 09:17 71-43-20.50 1
Bromobenzene ND ug/L 08/08/14 09:17 108-86-10.50 1
Bromochloromethane ND ug/L 08/08/14 09:17 74-97-50.50 1
Bromodichloromethane 0.66 ug/L 08/08/14 09:17 75-27-40.50 1
Bromoform ND ug/L 08/08/14 09:17 75-25-20.50 1
Bromomethane 5.0 ug/L 08/08/14 09:17 74-83-95.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW3 Lab ID:92212243003 Collected:08/06/14 11:45 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
n-Butylbenzene ND ug/L 08/08/14 09:17 104-51-80.50 1
sec-Butylbenzene ND ug/L 08/08/14 09:17 135-98-80.50 1
tert-Butylbenzene ND ug/L 08/08/14 09:17 98-06-60.50 1
Carbon tetrachloride ND ug/L 08/08/14 09:17 56-23-50.50 1
Chlorobenzene ND ug/L 08/08/14 09:17 108-90-70.50 1
Chloroethane ND ug/L 08/08/14 09:17 75-00-31.0 1
Chloroform 6.5 ug/L 08/08/14 09:17 67-66-30.50 1
Chloromethane ND ug/L 08/08/14 09:17 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/08/14 09:17 95-49-80.50 1
4-Chlorotoluene ND ug/L 08/08/14 09:17 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 08/08/14 09:17 96-12-81.0 1
Dibromochloromethane ND ug/L 08/08/14 09:17 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 08/08/14 09:17 106-93-40.50 1
Dibromomethane ND ug/L 08/08/14 09:17 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 08/08/14 09:17 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 08/08/14 09:17 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 08/08/14 09:17 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 08/08/14 09:17 75-71-80.50 1
1,1-Dichloroethane ND ug/L 08/08/14 09:17 75-34-30.50 1
1,2-Dichloroethane ND ug/L 08/08/14 09:17 107-06-20.50 1
1,1-Dichloroethene ND ug/L 08/08/14 09:17 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 08/08/14 09:17 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 08/08/14 09:17 156-60-50.50 1
1,2-Dichloropropane ND ug/L 08/08/14 09:17 78-87-50.50 1
1,3-Dichloropropane ND ug/L 08/08/14 09:17 142-28-90.50 1
2,2-Dichloropropane ND ug/L 08/08/14 09:17 594-20-70.50 1
1,1-Dichloropropene ND ug/L 08/08/14 09:17 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 08/08/14 09:17 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 08/08/14 09:17 10061-02-60.50 1
Diisopropyl ether ND ug/L 08/08/14 09:17 108-20-30.50 1
Ethylbenzene ND ug/L 08/08/14 09:17 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 08/08/14 09:17 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 08/08/14 09:17 98-82-80.50 1
Methylene Chloride ND ug/L 08/08/14 09:17 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 08/08/14 09:17 1634-04-40.50 1
Naphthalene ND ug/L 08/08/14 09:17 91-20-32.0 1
n-Propylbenzene ND ug/L 08/08/14 09:17 103-65-10.50 1
Styrene ND ug/L 08/08/14 09:17 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 08/08/14 09:17 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 08/08/14 09:17 79-34-50.50 1
Tetrachloroethene ND ug/L 08/08/14 09:17 127-18-40.50 1
Toluene ND ug/L 08/08/14 09:17 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 08/08/14 09:17 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 08/08/14 09:17 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 08/08/14 09:17 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 08/08/14 09:17 79-00-50.50 1
Trichloroethene ND ug/L 08/08/14 09:17 79-01-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW3 Lab ID:92212243003 Collected:08/06/14 11:45 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Trichlorofluoromethane ND ug/L 08/08/14 09:17 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/08/14 09:17 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 08/08/14 09:17 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 08/08/14 09:17 108-67-80.50 1
Vinyl chloride ND ug/L 08/08/14 09:17 75-01-41.0 1
m&p-Xylene ND ug/L 08/08/14 09:17 179601-23-11.0 1
o-Xylene ND ug/L 08/08/14 09:17 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %08/08/14 09:17 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %08/08/14 09:17 460-00-470-130 1
Toluene-d8 (S)101 %08/08/14 09:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW4 Lab ID:92212243004 Collected:08/06/14 11:15 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)0.054 ug/L 08/09/14 22:07 106-93-408/09/14 17:490.021 1
Surrogates
1-Chloro-2-bromopropane (S)104 %08/09/14 22:07 301-79-5608/09/14 17:4970-130 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)197 ug/L 08/12/14 02:31 N208/07/14 08:281001
Aliphatic (C19-C36)ND ug/L 08/12/14 02:31 N208/07/14 08:281001
Aromatic (C11-C22)744 ug/L 08/12/14 02:31 N208/07/14 08:281001
Surrogates
Nonatriacontane (S)56 %08/12/14 02:31 7194-86-708/07/14 08:2840-140 1
o-Terphenyl (S)61 %08/12/14 02:31 84-15-108/07/14 08:2840-140 1
2-Fluorobiphenyl (S)71 %08/12/14 02:31 321-60-808/07/14 08:2840-140 1
2-Bromonaphthalene (S)87 %08/12/14 02:31 580-13-208/07/14 08:2840-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)9470 ug/L 08/11/14 13:58 N250010
Aliphatic (C09-C12)16200 ug/L 08/11/14 13:58 N250010
Aromatic (C09-C10)4720 ug/L 08/11/14 13:58 N250010
Surrogates
4-Bromofluorobenzene (FID) (S)107 %08/11/14 13:58 460-00-470-130 10
4-Bromofluorobenzene (PID) (S)97 %08/11/14 13:58 460-00-470-130 10
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP
Lead 1680 ug/L 08/09/14 01:06 7439-92-108/08/14 15:305.0 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 08/08/14 07:25 83-32-908/07/14 11:215.0 1
Acenaphthylene ND ug/L 08/08/14 07:25 208-96-808/07/14 11:215.0 1
Anthracene ND ug/L 08/08/14 07:25 120-12-708/07/14 11:215.0 1
Benzo(a)anthracene ND ug/L 08/08/14 07:25 56-55-308/07/14 11:215.0 1
Benzo(a)pyrene ND ug/L 08/08/14 07:25 50-32-808/07/14 11:215.0 1
Benzo(b)fluoranthene ND ug/L 08/08/14 07:25 205-99-208/07/14 11:215.0 1
Benzo(g,h,i)perylene ND ug/L 08/08/14 07:25 191-24-208/07/14 11:215.0 1
Benzo(k)fluoranthene ND ug/L 08/08/14 07:25 207-08-908/07/14 11:215.0 1
4-Bromophenylphenyl ether ND ug/L 08/08/14 07:25 101-55-308/07/14 11:215.0 1
Butylbenzylphthalate ND ug/L 08/08/14 07:25 85-68-708/07/14 11:215.0 1
4-Chloro-3-methylphenol ND ug/L 08/08/14 07:25 59-50-708/07/14 11:215.0 1
bis(2-Chloroethoxy)methane ND ug/L 08/08/14 07:25 111-91-108/07/14 11:2110.0 1
bis(2-Chloroethyl) ether ND ug/L 08/08/14 07:25 111-44-408/07/14 11:215.0 1
bis(2-Chloroisopropyl) ether ND ug/L 08/08/14 07:25 108-60-108/07/14 11:215.0 1
2-Chloronaphthalene ND ug/L 08/08/14 07:25 91-58-708/07/14 11:215.0 1
2-Chlorophenol ND ug/L 08/08/14 07:25 95-57-808/07/14 11:215.0 1
4-Chlorophenylphenyl ether ND ug/L 08/08/14 07:25 7005-72-308/07/14 11:215.0 1
Chrysene ND ug/L 08/08/14 07:25 218-01-908/07/14 11:215.0 1
Dibenz(a,h)anthracene ND ug/L 08/08/14 07:25 53-70-308/07/14 11:215.0 1
3,3'-Dichlorobenzidine ND ug/L 08/08/14 07:25 91-94-108/07/14 11:2125.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW4 Lab ID:92212243004 Collected:08/06/14 11:15 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
2,4-Dichlorophenol ND ug/L 08/08/14 07:25 120-83-208/07/14 11:215.0 1
Diethylphthalate ND ug/L 08/08/14 07:25 84-66-208/07/14 11:215.0 1
2,4-Dimethylphenol ND ug/L 08/08/14 07:25 105-67-908/07/14 11:2110.0 1
Dimethylphthalate ND ug/L 08/08/14 07:25 131-11-308/07/14 11:215.0 1
Di-n-butylphthalate ND ug/L 08/08/14 07:25 84-74-208/07/14 11:215.0 1
4,6-Dinitro-2-methylphenol ND ug/L 08/08/14 07:25 534-52-108/07/14 11:2120.0 1
2,4-Dinitrophenol ND ug/L 08/08/14 07:25 51-28-508/07/14 11:2150.0 1
2,4-Dinitrotoluene ND ug/L 08/08/14 07:25 121-14-208/07/14 11:215.0 1
2,6-Dinitrotoluene ND ug/L 08/08/14 07:25 606-20-208/07/14 11:215.0 1
Di-n-octylphthalate ND ug/L 08/08/14 07:25 117-84-008/07/14 11:215.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/08/14 07:25 117-81-708/07/14 11:215.0 1
Fluoranthene ND ug/L 08/08/14 07:25 206-44-008/07/14 11:215.0 1
Fluorene ND ug/L 08/08/14 07:25 86-73-708/07/14 11:215.0 1
Hexachloro-1,3-butadiene ND ug/L 08/08/14 07:25 87-68-308/07/14 11:215.0 1
Hexachlorobenzene ND ug/L 08/08/14 07:25 118-74-108/07/14 11:215.0 1
Hexachlorocyclopentadiene ND ug/L 08/08/14 07:25 77-47-408/07/14 11:2110.0 1
Hexachloroethane ND ug/L 08/08/14 07:25 67-72-108/07/14 11:215.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/08/14 07:25 193-39-508/07/14 11:215.0 1
Isophorone ND ug/L 08/08/14 07:25 78-59-108/07/14 11:2110.0 1
Naphthalene 342 ug/L 08/09/14 01:37 91-20-308/07/14 11:2120.0 4
Nitrobenzene ND ug/L 08/08/14 07:25 98-95-308/07/14 11:215.0 1
2-Nitrophenol ND ug/L 08/08/14 07:25 88-75-508/07/14 11:215.0 1
4-Nitrophenol ND ug/L 08/08/14 07:25 100-02-708/07/14 11:2150.0 1
N-Nitrosodimethylamine ND ug/L 08/08/14 07:25 62-75-908/07/14 11:215.0 1
N-Nitroso-di-n-propylamine ND ug/L 08/08/14 07:25 621-64-708/07/14 11:215.0 1
N-Nitrosodiphenylamine ND ug/L 08/08/14 07:25 86-30-608/07/14 11:2110.0 1
Pentachlorophenol ND ug/L 08/08/14 07:25 87-86-508/07/14 11:2110.0 1
Phenanthrene ND ug/L 08/08/14 07:25 85-01-808/07/14 11:215.0 1
Phenol ND ug/L 08/08/14 07:25 108-95-208/07/14 11:215.0 1
Pyrene ND ug/L 08/08/14 07:25 129-00-008/07/14 11:215.0 1
1,2,4-Trichlorobenzene ND ug/L 08/08/14 07:25 120-82-108/07/14 11:215.0 1
2,4,6-Trichlorophenol ND ug/L 08/08/14 07:25 88-06-208/07/14 11:2110.0 1
Surrogates
Nitrobenzene-d5 (S)74 %08/08/14 07:25 4165-60-008/07/14 11:2110-120 1
2-Fluorobiphenyl (S)73 %08/08/14 07:25 321-60-808/07/14 11:2115-120 1
Terphenyl-d14 (S)84 %08/08/14 07:25 1718-51-008/07/14 11:2111-131 1
Phenol-d6 (S)29 %08/08/14 07:25 13127-88-308/07/14 11:2110-120 1
2-Fluorophenol (S)42 %08/08/14 07:25 367-12-408/07/14 11:2110-120 1
2,4,6-Tribromophenol (S)90 %08/08/14 07:25 118-79-608/07/14 11:2110-137 1
Analytical Method: SM 6200B6200B MSV
Benzene 36.4 ug/L 08/11/14 18:09 71-43-25.0 10
Bromobenzene ND ug/L 08/11/14 18:09 108-86-15.0 10
Bromochloromethane ND ug/L 08/11/14 18:09 74-97-55.0 10
Bromodichloromethane ND ug/L 08/11/14 18:09 75-27-45.0 10
Bromoform ND ug/L 08/11/14 18:09 75-25-25.0 10
Bromomethane ND ug/L 08/11/14 18:09 74-83-950.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW4 Lab ID:92212243004 Collected:08/06/14 11:15 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
n-Butylbenzene ND ug/L 08/11/14 18:09 104-51-85.0 10
sec-Butylbenzene 28.0 ug/L 08/11/14 18:09 135-98-85.0 10
tert-Butylbenzene ND ug/L 08/11/14 18:09 98-06-65.0 10
Carbon tetrachloride ND ug/L 08/11/14 18:09 56-23-55.0 10
Chlorobenzene ND ug/L 08/11/14 18:09 108-90-75.0 10
Chloroethane ND ug/L 08/11/14 18:09 75-00-310.0 10
Chloroform ND ug/L 08/11/14 18:09 67-66-35.0 10
Chloromethane ND ug/L 08/11/14 18:09 74-87-310.0 10
2-Chlorotoluene ND ug/L 08/11/14 18:09 95-49-85.0 10
4-Chlorotoluene ND ug/L 08/11/14 18:09 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 08/11/14 18:09 96-12-810.0 10
Dibromochloromethane ND ug/L 08/11/14 18:09 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 08/11/14 18:09 106-93-45.0 10
Dibromomethane ND ug/L 08/11/14 18:09 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 08/11/14 18:09 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 08/11/14 18:09 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 08/11/14 18:09 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 08/11/14 18:09 75-71-85.0 10
1,1-Dichloroethane ND ug/L 08/11/14 18:09 75-34-35.0 10
1,2-Dichloroethane 74.8 ug/L 08/11/14 18:09 107-06-25.0 10
1,1-Dichloroethene ND ug/L 08/11/14 18:09 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 08/11/14 18:09 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 08/11/14 18:09 156-60-55.0 10
1,2-Dichloropropane ND ug/L 08/11/14 18:09 78-87-55.0 10
1,3-Dichloropropane ND ug/L 08/11/14 18:09 142-28-95.0 10
2,2-Dichloropropane ND ug/L 08/11/14 18:09 594-20-75.0 10
1,1-Dichloropropene ND ug/L 08/11/14 18:09 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 08/11/14 18:09 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 08/11/14 18:09 10061-02-65.0 10
Diisopropyl ether 11.9 ug/L 08/11/14 18:09 108-20-35.0 10
Ethylbenzene 651 ug/L 08/11/14 18:09 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 08/11/14 18:09 87-68-320.0 10
Isopropylbenzene (Cumene)161 ug/L 08/11/14 18:09 98-82-85.0 10
Methylene Chloride ND ug/L 08/11/14 18:09 75-09-220.0 10
Methyl-tert-butyl ether ND ug/L 08/11/14 18:09 1634-04-45.0 10
Naphthalene 584 ug/L 08/11/14 18:09 91-20-320.0 10
n-Propylbenzene 420 ug/L 08/11/14 18:09 103-65-15.0 10
Styrene ND ug/L 08/11/14 18:09 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 08/11/14 18:09 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 08/11/14 18:09 79-34-55.0 10
Tetrachloroethene ND ug/L 08/11/14 18:09 127-18-45.0 10
Toluene 35.1 ug/L 08/11/14 18:09 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 08/11/14 18:09 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 08/11/14 18:09 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 08/11/14 18:09 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 08/11/14 18:09 79-00-55.0 10
Trichloroethene ND ug/L 08/11/14 18:09 79-01-65.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92212243
Yogi Foods
Sample:MW4 Lab ID:92212243004 Collected:08/06/14 11:15 Received:08/06/14 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Trichlorofluoromethane ND ug/L 08/11/14 18:09 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 08/11/14 18:09 96-18-45.0 10
1,2,4-Trimethylbenzene 1440 ug/L 08/11/14 18:09 95-63-65.0 10
1,3,5-Trimethylbenzene 654 ug/L 08/11/14 18:09 108-67-85.0 10
Vinyl chloride ND ug/L 08/11/14 18:09 75-01-410.0 10
m&p-Xylene 1040 ug/L 08/11/14 18:09 179601-23-110.0 10
o-Xylene 61.0 ug/L 08/11/14 18:09 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)102 %08/11/14 18:09 17060-07-070-130 10
4-Bromofluorobenzene (S)100 %08/11/14 18:09 460-00-470-130 10
Toluene-d8 (S)104 %08/11/14 18:09 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/8427
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:92212243003, 92212243004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1261038
Associated Lab Samples:92212243003, 92212243004
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N208/11/14 10:55
Aliphatic (C09-C12)ug/L ND 50.0 N208/11/14 10:55
Aromatic (C09-C10)ug/L ND 50.0 N208/11/14 10:55
4-Bromofluorobenzene (FID) (S)%103 70-130 08/11/14 10:55
4-Bromofluorobenzene (PID) (S)%98 70-130 08/11/14 10:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1261039LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1261040
Aliphatic (C05-C08)ug/L 303 N230010170-130102306 1 25
Aliphatic (C09-C12)ug/L 332 N230011130-130116349 5 25
Aromatic (C09-C10)ug/L 93.4 N21009370-1309594.5 1 25
4-Bromofluorobenzene (FID) (S)%104 70-130101
4-Bromofluorobenzene (PID) (S)%101 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/8433
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:92212243001, 92212243002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1261658
Associated Lab Samples:92212243001, 92212243002
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N208/12/14 11:09
Aliphatic (C09-C12)ug/L ND 50.0 N208/12/14 11:09
Aromatic (C09-C10)ug/L ND 50.0 N208/12/14 11:09
4-Bromofluorobenzene (FID) (S)%105 70-130 08/12/14 11:09
4-Bromofluorobenzene (PID) (S)%97 70-130 08/12/14 11:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1261659LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1261660
Aliphatic (C05-C08)ug/L 305 N230010270-130100299 2 25
Aliphatic (C09-C12)ug/L 344 N230011530-130118353 3 25
Aromatic (C09-C10)ug/L 94.6 N21009570-1309493.7 1 25
4-Bromofluorobenzene (FID) (S)%106 70-130107
4-Bromofluorobenzene (PID) (S)%101 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/16631
EPA 3010
EPA 6010
6010 MET
Associated Lab Samples:92212243001, 92212243002, 92212243003, 92212243004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1260143
Associated Lab Samples:92212243001, 92212243002, 92212243003, 92212243004
Matrix:Water
Analyzed
Lead ug/L ND 5.0 08/09/14 00:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1260144LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 490500 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1260145MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92212243001
1260146
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 500 98 75-12598 0 20500228716719
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27865
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92212243001, 92212243002, 92212243003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1259151
Associated Lab Samples:92212243001, 92212243002, 92212243003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/08/14 08:27
1,1,1-Trichloroethane ug/L ND 0.50 08/08/14 08:27
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/08/14 08:27
1,1,2-Trichloroethane ug/L ND 0.50 08/08/14 08:27
1,1-Dichloroethane ug/L ND 0.50 08/08/14 08:27
1,1-Dichloroethene ug/L ND 0.50 08/08/14 08:27
1,1-Dichloropropene ug/L ND 0.50 08/08/14 08:27
1,2,3-Trichlorobenzene ug/L ND 2.0 08/08/14 08:27
1,2,3-Trichloropropane ug/L ND 0.50 08/08/14 08:27
1,2,4-Trichlorobenzene ug/L ND 2.0 08/08/14 08:27
1,2,4-Trimethylbenzene ug/L ND 0.50 08/08/14 08:27
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/08/14 08:27
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/08/14 08:27
1,2-Dichlorobenzene ug/L ND 0.50 08/08/14 08:27
1,2-Dichloroethane ug/L ND 0.50 08/08/14 08:27
1,2-Dichloropropane ug/L ND 0.50 08/08/14 08:27
1,3,5-Trimethylbenzene ug/L ND 0.50 08/08/14 08:27
1,3-Dichlorobenzene ug/L ND 0.50 08/08/14 08:27
1,3-Dichloropropane ug/L ND 0.50 08/08/14 08:27
1,4-Dichlorobenzene ug/L ND 0.50 08/08/14 08:27
2,2-Dichloropropane ug/L ND 0.50 08/08/14 08:27
2-Chlorotoluene ug/L ND 0.50 08/08/14 08:27
4-Chlorotoluene ug/L ND 0.50 08/08/14 08:27
Benzene ug/L ND 0.50 08/08/14 08:27
Bromobenzene ug/L ND 0.50 08/08/14 08:27
Bromochloromethane ug/L ND 0.50 08/08/14 08:27
Bromodichloromethane ug/L ND 0.50 08/08/14 08:27
Bromoform ug/L ND 0.50 08/08/14 08:27
Bromomethane ug/L ND 5.0 08/08/14 08:27
Carbon tetrachloride ug/L ND 0.50 08/08/14 08:27
Chlorobenzene ug/L ND 0.50 08/08/14 08:27
Chloroethane ug/L ND 1.0 08/08/14 08:27
Chloroform ug/L ND 0.50 08/08/14 08:27
Chloromethane ug/L ND 1.0 08/08/14 08:27
cis-1,2-Dichloroethene ug/L ND 0.50 08/08/14 08:27
cis-1,3-Dichloropropene ug/L ND 0.50 08/08/14 08:27
Dibromochloromethane ug/L ND 0.50 08/08/14 08:27
Dibromomethane ug/L ND 0.50 08/08/14 08:27
Dichlorodifluoromethane ug/L ND 0.50 08/08/14 08:27
Diisopropyl ether ug/L ND 0.50 08/08/14 08:27
Ethylbenzene ug/L ND 0.50 08/08/14 08:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1259151
Associated Lab Samples:92212243001, 92212243002, 92212243003
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 08/08/14 08:27
Isopropylbenzene (Cumene)ug/L ND 0.50 08/08/14 08:27
m&p-Xylene ug/L ND 1.0 08/08/14 08:27
Methyl-tert-butyl ether ug/L ND 0.50 08/08/14 08:27
Methylene Chloride ug/L ND 2.0 08/08/14 08:27
n-Butylbenzene ug/L ND 0.50 08/08/14 08:27
n-Propylbenzene ug/L ND 0.50 08/08/14 08:27
Naphthalene ug/L ND 2.0 08/08/14 08:27
o-Xylene ug/L ND 0.50 08/08/14 08:27
sec-Butylbenzene ug/L ND 0.50 08/08/14 08:27
Styrene ug/L ND 0.50 08/08/14 08:27
tert-Butylbenzene ug/L ND 0.50 08/08/14 08:27
Tetrachloroethene ug/L ND 0.50 08/08/14 08:27
Toluene ug/L ND 0.50 08/08/14 08:27
trans-1,2-Dichloroethene ug/L ND 0.50 08/08/14 08:27
trans-1,3-Dichloropropene ug/L ND 0.50 08/08/14 08:27
Trichloroethene ug/L ND 0.50 08/08/14 08:27
Trichlorofluoromethane ug/L ND 1.0 08/08/14 08:27
Vinyl chloride ug/L ND 1.0 08/08/14 08:27
1,2-Dichloroethane-d4 (S)%99 70-130 08/08/14 08:27
4-Bromofluorobenzene (S)%99 70-130 08/08/14 08:27
Toluene-d8 (S)%102 70-130 08/08/14 08:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1259152LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.950 100 60-140
1,1,1-Trichloroethane ug/L 50.850 102 60-140
1,1,2,2-Tetrachloroethane ug/L 51.450 103 60-140
1,1,2-Trichloroethane ug/L 53.550 107 60-140
1,1-Dichloroethane ug/L 50.650 101 60-140
1,1-Dichloroethene ug/L 52.750 105 60-140
1,1-Dichloropropene ug/L 54.950 110 60-140
1,2,3-Trichlorobenzene ug/L 50.950 102 60-140
1,2,3-Trichloropropane ug/L 51.750 103 60-140
1,2,4-Trichlorobenzene ug/L 51.450 103 60-140
1,2,4-Trimethylbenzene ug/L 49.550 99 60-140
1,2-Dibromo-3-chloropropane ug/L 49.750 99 60-140
1,2-Dibromoethane (EDB)ug/L 51.950 104 60-140
1,2-Dichlorobenzene ug/L 49.450 99 60-140
1,2-Dichloroethane ug/L 51.050 102 60-140
1,2-Dichloropropane ug/L 54.450 109 60-140
1,3,5-Trimethylbenzene ug/L 49.650 99 60-140
1,3-Dichlorobenzene ug/L 49.250 98 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1259152LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 52.050 104 60-140
1,4-Dichlorobenzene ug/L 48.950 98 60-140
2,2-Dichloropropane ug/L 42.750 85 60-140
2-Chlorotoluene ug/L 49.550 99 60-140
4-Chlorotoluene ug/L 50.050 100 60-140
Benzene ug/L 51.050 102 60-140
Bromobenzene ug/L 49.750 99 60-140
Bromochloromethane ug/L 53.250 106 60-140
Bromodichloromethane ug/L 58.550 117 60-140
Bromoform ug/L 56.250 112 60-140
Bromomethane ug/L 42.050 84 60-140
Carbon tetrachloride ug/L 51.250 102 60-140
Chlorobenzene ug/L 50.150 100 60-140
Chloroethane ug/L 50.450 101 60-140
Chloroform ug/L 58.150 116 60-140
Chloromethane ug/L 47.450 95 60-140
cis-1,2-Dichloroethene ug/L 56.350 113 60-140
cis-1,3-Dichloropropene ug/L 56.450 113 60-140
Dibromochloromethane ug/L 60.450 121 60-140
Dibromomethane ug/L 54.050 108 60-140
Dichlorodifluoromethane ug/L 48.150 96 60-140
Diisopropyl ether ug/L 52.850 106 60-140
Ethylbenzene ug/L 50.050 100 60-140
Hexachloro-1,3-butadiene ug/L 47.850 96 60-140
Isopropylbenzene (Cumene)ug/L 53.550 107 60-140
m&p-Xylene ug/L 98.2100 98 60-140
Methyl-tert-butyl ether ug/L 51.750 103 60-140
Methylene Chloride ug/L 54.250 108 60-140
n-Butylbenzene ug/L 50.950 102 60-140
n-Propylbenzene ug/L 49.750 99 60-140
Naphthalene ug/L 54.850 110 60-140
o-Xylene ug/L 50.750 101 60-140
sec-Butylbenzene ug/L 49.950 100 60-140
Styrene ug/L 55.350 111 60-140
tert-Butylbenzene ug/L 50.450 101 60-140
Tetrachloroethene ug/L 48.450 97 60-140
Toluene ug/L 49.050 98 60-140
trans-1,2-Dichloroethene ug/L 53.450 107 60-140
trans-1,3-Dichloropropene ug/L 47.150 94 60-140
Trichloroethene ug/L 49.150 98 60-140
Trichlorofluoromethane ug/L 48.050 96 60-140
Vinyl chloride ug/L 49.050 98 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1259153MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92212276012
1259154
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 104 60-14099 5 3020ND20.9 19.8
1,1,1-Trichloroethane ug/L 20 110 60-140105 4 3020ND21.9 21.0
1,1,2,2-Tetrachloroethane ug/L 20 111 60-140104 6 3020ND22.2 20.9
1,1,2-Trichloroethane ug/L 20 117 60-140108 8 3020ND23.4 21.6
1,1-Dichloroethane ug/L 20 113 60-140107 6 3020ND22.6 21.3
1,1-Dichloroethene ug/L 20 122 60-140115 6 3020ND24.4 23.0
1,1-Dichloropropene ug/L 20 121 60-140119 2 3020ND24.3 23.9
1,2,3-Trichlorobenzene ug/L 20 108 60-140102 6 3020ND21.6 20.5
1,2,3-Trichloropropane ug/L 20 114 60-140106 8 3020ND22.9 21.2
1,2,4-Trichlorobenzene ug/L 20 108 60-140102 6 3020ND21.6 20.4
1,2,4-Trimethylbenzene ug/L 20 107 60-140100 6 3020ND21.4 20.1
1,2-Dibromo-3-chloropropane ug/L 20 103 60-14097 6 3020ND20.6 19.4
1,2-Dibromoethane (EDB)ug/L 20 111 60-140106 5 3020ND22.2 21.2
1,2-Dichlorobenzene ug/L 20 107 60-140101 6 3020ND21.4 20.2
1,2-Dichloroethane ug/L 20 114 60-140108 5 3020ND22.8 21.6
1,2-Dichloropropane ug/L 20 119 60-140112 5 3020ND23.7 22.5
1,3,5-Trimethylbenzene ug/L 20 108 60-140102 5 3020ND21.6 20.5
1,3-Dichlorobenzene ug/L 20 111 60-140101 9 3020ND22.2 20.3
1,3-Dichloropropane ug/L 20 114 60-140109 4 3020ND22.7 21.8
1,4-Dichlorobenzene ug/L 20 106 60-140101 5 3020ND21.2 20.2
2,2-Dichloropropane ug/L 20 115 60-140111 3 3020ND23.0 22.2
2-Chlorotoluene ug/L 20 107 60-140102 5 3020ND21.4 20.4
4-Chlorotoluene ug/L 20 109 60-140104 5 3020ND21.8 20.8
Benzene ug/L 20 112 60-140107 4 3020ND22.4 21.4
Bromobenzene ug/L 20 109 60-140103 5 3020ND21.8 20.7
Bromochloromethane ug/L 20 123 60-140119 4 3020ND24.6 23.7
Bromodichloromethane ug/L 20 122 60-140114 6 3020ND24.3 22.9
Bromoform ug/L 20 111 60-140103 7 3020ND22.1 20.6
Bromomethane ug/L 20 121 60-140115 5 3020ND24.3 23.0
Carbon tetrachloride ug/L 20 109 60-140101 7 3020ND21.7 20.2
Chlorobenzene ug/L 20 110 60-140103 7 3020ND22.1 20.7
Chloroethane ug/L 20 120 60-140114 5 3020ND23.9 22.8
Chloroform ug/L 20 129 60-140125 3 3020ND25.8 25.0
Chloromethane ug/L 20 114 60-140114 0 3020ND22.8 22.9
cis-1,2-Dichloroethene ug/L 20 126 60-140121 4 3020ND25.2 24.2
cis-1,3-Dichloropropene ug/L 20 119 60-140111 7 3020ND23.8 22.2
Dibromochloromethane ug/L 20 123 60-140116 6 3020ND24.6 23.1
Dibromomethane ug/L 20 115 60-140112 3 3020ND23.1 22.3
Dichlorodifluoromethane ug/L 20 124 60-140117 6 3020ND24.8 23.4
Diisopropyl ether ug/L 20 118 60-140113 4 3020ND23.6 22.7
Ethylbenzene ug/L 20 108 60-140102 6 3020ND21.6 20.3
Hexachloro-1,3-butadiene ug/L 20 105 60-140103 2 3020ND21.0 20.5
Isopropylbenzene (Cumene)ug/L 20 112 60-140106 6 3020ND22.5 21.2
m&p-Xylene ug/L 40 106 60-140102 4 3040ND42.4 40.8
Methyl-tert-butyl ether ug/L 20 117 60-140111 5 3020ND23.5 22.2
Methylene Chloride ug/L 20 115 60-140109 6 3020ND23.0 21.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1259153MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92212276012
1259154
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 108 60-140105 3 3020ND21.6 20.9
n-Propylbenzene ug/L 20 108 60-140101 6 3020ND21.6 20.3
Naphthalene ug/L 20 115 60-140108 7 3020ND23.0 21.5
o-Xylene ug/L 20 109 60-140103 6 3020ND21.9 20.6
sec-Butylbenzene ug/L 20 106 60-140101 4 3020ND21.2 20.2
Styrene ug/L 20 119 60-140113 6 3020ND23.9 22.5
tert-Butylbenzene ug/L 20 107 60-140102 5 3020ND21.5 20.5
Tetrachloroethene ug/L 20 103 60-14097 5 3020ND20.5 19.4
Toluene ug/L 20 108 60-140102 6 3020ND21.7 20.5
trans-1,2-Dichloroethene ug/L 20 121 60-140116 4 3020ND24.2 23.3
trans-1,3-Dichloropropene ug/L 20 103 60-14099 4 3020ND20.6 19.9
Trichloroethene ug/L 20 106 60-140101 5 3020ND21.2 20.2
Trichlorofluoromethane ug/L 20 112 60-140108 4 3020ND22.5 21.5
Vinyl chloride ug/L 20 119 60-140117 2 3020ND23.8 23.3
1,2-Dichloroethane-d4 (S)%97 70-13098
4-Bromofluorobenzene (S)%101 70-130100
Toluene-d8 (S)%102 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27891
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92212243004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1261146
Associated Lab Samples:92212243004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/11/14 11:49
1,1,1-Trichloroethane ug/L ND 0.50 08/11/14 11:49
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/11/14 11:49
1,1,2-Trichloroethane ug/L ND 0.50 08/11/14 11:49
1,1-Dichloroethane ug/L ND 0.50 08/11/14 11:49
1,1-Dichloroethene ug/L ND 0.50 08/11/14 11:49
1,1-Dichloropropene ug/L ND 0.50 08/11/14 11:49
1,2,3-Trichlorobenzene ug/L ND 2.0 08/11/14 11:49
1,2,3-Trichloropropane ug/L ND 0.50 08/11/14 11:49
1,2,4-Trichlorobenzene ug/L ND 2.0 08/11/14 11:49
1,2,4-Trimethylbenzene ug/L ND 0.50 08/11/14 11:49
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/11/14 11:49
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/11/14 11:49
1,2-Dichlorobenzene ug/L ND 0.50 08/11/14 11:49
1,2-Dichloroethane ug/L ND 0.50 08/11/14 11:49
1,2-Dichloropropane ug/L ND 0.50 08/11/14 11:49
1,3,5-Trimethylbenzene ug/L ND 0.50 08/11/14 11:49
1,3-Dichlorobenzene ug/L ND 0.50 08/11/14 11:49
1,3-Dichloropropane ug/L ND 0.50 08/11/14 11:49
1,4-Dichlorobenzene ug/L ND 0.50 08/11/14 11:49
2,2-Dichloropropane ug/L ND 0.50 08/11/14 11:49
2-Chlorotoluene ug/L ND 0.50 08/11/14 11:49
4-Chlorotoluene ug/L ND 0.50 08/11/14 11:49
Benzene ug/L ND 0.50 08/11/14 11:49
Bromobenzene ug/L ND 0.50 08/11/14 11:49
Bromochloromethane ug/L ND 0.50 08/11/14 11:49
Bromodichloromethane ug/L ND 0.50 08/11/14 11:49
Bromoform ug/L ND 0.50 08/11/14 11:49
Bromomethane ug/L ND 5.0 08/11/14 11:49
Carbon tetrachloride ug/L ND 0.50 08/11/14 11:49
Chlorobenzene ug/L ND 0.50 08/11/14 11:49
Chloroethane ug/L ND 1.0 08/11/14 11:49
Chloroform ug/L ND 0.50 08/11/14 11:49
Chloromethane ug/L ND 1.0 08/11/14 11:49
cis-1,2-Dichloroethene ug/L ND 0.50 08/11/14 11:49
cis-1,3-Dichloropropene ug/L ND 0.50 08/11/14 11:49
Dibromochloromethane ug/L ND 0.50 08/11/14 11:49
Dibromomethane ug/L ND 0.50 08/11/14 11:49
Dichlorodifluoromethane ug/L ND 0.50 08/11/14 11:49
Diisopropyl ether ug/L ND 0.50 08/11/14 11:49
Ethylbenzene ug/L ND 0.50 08/11/14 11:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1261146
Associated Lab Samples:92212243004
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 08/11/14 11:49
Isopropylbenzene (Cumene)ug/L ND 0.50 08/11/14 11:49
m&p-Xylene ug/L ND 1.0 08/11/14 11:49
Methyl-tert-butyl ether ug/L ND 0.50 08/11/14 11:49
Methylene Chloride ug/L ND 2.0 08/11/14 11:49
n-Butylbenzene ug/L ND 0.50 08/11/14 11:49
n-Propylbenzene ug/L ND 0.50 08/11/14 11:49
Naphthalene ug/L ND 2.0 08/11/14 11:49
o-Xylene ug/L ND 0.50 08/11/14 11:49
sec-Butylbenzene ug/L ND 0.50 08/11/14 11:49
Styrene ug/L ND 0.50 08/11/14 11:49
tert-Butylbenzene ug/L ND 0.50 08/11/14 11:49
Tetrachloroethene ug/L ND 0.50 08/11/14 11:49
Toluene ug/L ND 0.50 08/11/14 11:49
trans-1,2-Dichloroethene ug/L ND 0.50 08/11/14 11:49
trans-1,3-Dichloropropene ug/L ND 0.50 08/11/14 11:49
Trichloroethene ug/L ND 0.50 08/11/14 11:49
Trichlorofluoromethane ug/L ND 1.0 08/11/14 11:49
Vinyl chloride ug/L ND 1.0 08/11/14 11:49
1,2-Dichloroethane-d4 (S)%102 70-130 08/11/14 11:49
4-Bromofluorobenzene (S)%99 70-130 08/11/14 11:49
Toluene-d8 (S)%101 70-130 08/11/14 11:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1261147LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.350 99 60-140
1,1,1-Trichloroethane ug/L 52.650 105 60-140
1,1,2,2-Tetrachloroethane ug/L 49.650 99 60-140
1,1,2-Trichloroethane ug/L 52.850 106 60-140
1,1-Dichloroethane ug/L 52.550 105 60-140
1,1-Dichloroethene ug/L 50.250 100 60-140
1,1-Dichloropropene ug/L 51.850 104 60-140
1,2,3-Trichlorobenzene ug/L 48.250 96 60-140
1,2,3-Trichloropropane ug/L 51.150 102 60-140
1,2,4-Trichlorobenzene ug/L 49.150 98 60-140
1,2,4-Trimethylbenzene ug/L 45.750 91 60-140
1,2-Dibromo-3-chloropropane ug/L 53.750 107 60-140
1,2-Dibromoethane (EDB)ug/L 50.550 101 60-140
1,2-Dichlorobenzene ug/L 46.850 94 60-140
1,2-Dichloroethane ug/L 53.050 106 60-140
1,2-Dichloropropane ug/L 51.250 102 60-140
1,3,5-Trimethylbenzene ug/L 46.450 93 60-140
1,3-Dichlorobenzene ug/L 46.350 93 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1261147LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 49.350 99 60-140
1,4-Dichlorobenzene ug/L 45.750 91 60-140
2,2-Dichloropropane ug/L 54.850 110 60-140
2-Chlorotoluene ug/L 45.450 91 60-140
4-Chlorotoluene ug/L 46.950 94 60-140
Benzene ug/L 49.050 98 60-140
Bromobenzene ug/L 47.050 94 60-140
Bromochloromethane ug/L 55.550 111 60-140
Bromodichloromethane ug/L 54.150 108 60-140
Bromoform ug/L 54.950 110 60-140
Bromomethane ug/L 48.850 98 60-140
Carbon tetrachloride ug/L 50.250 100 60-140
Chlorobenzene ug/L 47.950 96 60-140
Chloroethane ug/L 50.350 101 60-140
Chloroform ug/L 52.450 105 60-140
Chloromethane ug/L 45.950 92 60-140
cis-1,2-Dichloroethene ug/L 51.550 103 60-140
cis-1,3-Dichloropropene ug/L 58.450 117 60-140
Dibromochloromethane ug/L 52.650 105 60-140
Dibromomethane ug/L 53.850 108 60-140
Dichlorodifluoromethane ug/L 42.950 86 60-140
Diisopropyl ether ug/L 52.550 105 60-140
Ethylbenzene ug/L 46.550 93 60-140
Hexachloro-1,3-butadiene ug/L 46.250 92 60-140
Isopropylbenzene (Cumene)ug/L 48.050 96 60-140
m&p-Xylene ug/L 92.0100 92 60-140
Methyl-tert-butyl ether ug/L 52.850 106 60-140
Methylene Chloride ug/L 51.850 104 60-140
n-Butylbenzene ug/L 46.750 93 60-140
n-Propylbenzene ug/L 45.150 90 60-140
Naphthalene ug/L 53.150 106 60-140
o-Xylene ug/L 47.250 94 60-140
sec-Butylbenzene ug/L 44.950 90 60-140
Styrene ug/L 50.750 101 60-140
tert-Butylbenzene ug/L 45.850 92 60-140
Tetrachloroethene ug/L 45.150 90 60-140
Toluene ug/L 47.150 94 60-140
trans-1,2-Dichloroethene ug/L 50.050 100 60-140
trans-1,3-Dichloropropene ug/L 50.050 100 60-140
Trichloroethene ug/L 49.450 99 60-140
Trichlorofluoromethane ug/L 47.450 95 60-140
Vinyl chloride ug/L 49.050 98 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1261621MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92212381004
1261622
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L R1207660-140112 38 3020ND15.2 22.3
1,1,1-Trichloroethane ug/L M1,R1209560-140145 42 3020ND18.9 29.0
1,1,2,2-Tetrachloroethane ug/L R1208160-140115 34 3020ND16.3 22.9
1,1,2-Trichloroethane ug/L R1209560-140133 34 3020ND19.0 26.7
1,1-Dichloroethane ug/L M1,R1209760-140144 39 3020ND19.4 28.8
1,1-Dichloroethene ug/L M1,R12010360-140159 42 3020ND20.7 31.8
1,1-Dichloropropene ug/L M1,R12010760-140165 43 3020ND21.4 33.0
1,2,3-Trichlorobenzene ug/L R1207660-140108 35 3020ND15.2 21.6
1,2,3-Trichloropropane ug/L R1208260-140118 36 3020ND16.4 23.6
1,2,4-Trichlorobenzene ug/L R1207660-140108 35 3020ND15.2 21.6
1,2,4-Trimethylbenzene ug/L R1207560-140110 37 3020ND15.1 22.0
1,2-Dibromo-3-chloropropane ug/L R1207160-140104 37 3020ND14.2 20.7
1,2-Dibromoethane (EDB)ug/L R1208160-140116 36 3020ND16.2 23.2
1,2-Dichlorobenzene ug/L R1207560-140108 36 3020ND15.1 21.7
1,2-Dichloroethane ug/L R1209560-140138 37 3020ND19.0 27.6
1,2-Dichloropropane ug/L M1,R1209860-140141 37 3020ND19.5 28.3
1,3,5-Trimethylbenzene ug/L R1207560-140111 38 3020ND15.1 22.2
1,3-Dichlorobenzene ug/L R1207560-140108 36 3020ND15.1 21.6
1,3-Dichloropropane ug/L R1208560-140119 34 3020ND16.9 23.8
1,4-Dichlorobenzene ug/L R1207660-140108 36 3020ND15.1 21.7
2,2-Dichloropropane ug/L M1,R1209560-140150 45 3020ND18.9 30.0
2-Chlorotoluene ug/L R1207660-140109 36 3020ND15.2 21.8
4-Chlorotoluene ug/L R1207760-140111 36 3020ND15.4 22.2
Benzene ug/L R1209360-140136 38 3020ND18.6 27.1
Bromobenzene ug/L R1207660-140111 37 3020ND15.3 22.3
Bromochloromethane ug/L M1,R12010760-140157 38 3020ND21.3 31.3
Bromodichloromethane ug/L M1,R1209860-140142 36 3020ND19.6 28.4
Bromoform ug/L R1207760-140116 41 3020ND15.3 23.2
Bromomethane ug/L R1208960-140128 36 3020ND17.8 25.6
Carbon tetrachloride ug/L R1208760-140136 44 3020ND17.4 27.1
Chlorobenzene ug/L R1208160-140116 35 3020ND16.3 23.2
Chloroethane ug/L M1,R12010060-140149 39 3020ND20.0 29.8
Chloroform ug/L M1,R12011260-140166 39 3020ND22.3 33.1
Chloromethane ug/L R1209560-140138 37 3020ND18.9 27.7
cis-1,2-Dichloroethene ug/L M1,R12011060-140160 37 3020ND22.0 32.0
cis-1,3-Dichloropropene ug/L R1209260-140138 40 3020ND18.4 27.6
Dibromochloromethane ug/L R1208860-140131 39 3020ND17.6 26.1
Dibromomethane ug/L R1209660-140135 34 3020ND19.2 27.0
Dichlorodifluoromethane ug/L M1,R1209960-140149 41 3020ND19.7 29.9
Diisopropyl ether ug/L M1,R12010560-140154 38 3020ND21.0 30.7
Ethylbenzene ug/L R1208060-140116 38 3020ND15.9 23.3
Hexachloro-1,3-butadiene ug/L R1207460-140112 41 3020ND14.7 22.4
Isopropylbenzene (Cumene)ug/L R1208260-140124 40 3020ND16.5 24.8
m&p-Xylene ug/L R1407960-140115 37 3040ND31.7 46.2
Methyl-tert-butyl ether ug/L M1,R12010360-140149 37 3020ND20.5 29.8
Methylene Chloride ug/L M1,R12010060-140146 38 3020ND20.0 29.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1261621MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92212381004
1261622
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Butylbenzene ug/L R1207660-140115 41 3020ND15.1 23.0
n-Propylbenzene ug/L R1207660-140114 40 3020ND15.1 22.8
Naphthalene ug/L R1207860-140114 37 3020ND15.7 22.8
o-Xylene ug/L R1208060-140116 37 3020ND15.9 23.2
sec-Butylbenzene ug/L R1207560-140114 41 3020ND15.1 22.8
Styrene ug/L R1208660-140126 37 3020ND17.2 25.1
tert-Butylbenzene ug/L R1207760-140114 39 3020ND15.3 22.8
Tetrachloroethene ug/L R1207760-140115 40 3020ND15.3 23.0
Toluene ug/L R1208960-140129 37 3020ND17.7 25.9
trans-1,2-Dichloroethene ug/L M1,R12010560-140158 40 3020ND21.0 31.6
trans-1,3-Dichloropropene ug/L R1208160-140120 39 3020ND16.1 24.0
Trichloroethene ug/L R1208860-140128 37 3020ND17.6 25.7
Trichlorofluoromethane ug/L M1,R1209860-140151 42 3020ND19.6 30.1
Vinyl chloride ug/L M1,R12010060-140150 40 3020ND20.1 30.1
1,2-Dichloroethane-d4 (S)%99 70-130101
4-Bromofluorobenzene (S)%103 70-130103
Toluene-d8 (S)%104 70-130104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/29317
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Associated Lab Samples:92212243001, 92212243002, 92212243003, 92212243004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1260885
Associated Lab Samples:92212243001, 92212243002, 92212243003, 92212243004
Matrix:Water
Analyzed
1,2-Dibromoethane (EDB)ug/L ND 0.020 08/09/14 20:04
1-Chloro-2-bromopropane (S)%105 70-130 08/09/14 20:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1260886LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1260887
1,2-Dibromoethane (EDB)ug/L 0.29.29 100 70-1301040.29 3 20
1-Chloro-2-bromopropane (S)%106 70-130102
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1260888MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92212715003
1260889
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dibromoethane (EDB)ug/L M3.28 135 65-135163 3 20.282.7 3.0 3.1
1-Chloro-2-bromopropane (S)%108 70-130111
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92212715004
1260890SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 20ND
1-Chloro-2-bromopropane (S)%112 1114
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/29257
EPA 625
EPA 625
625 MSS
Associated Lab Samples:92212243001, 92212243002, 92212243003, 92212243004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1258662
Associated Lab Samples:92212243001, 92212243002, 92212243003, 92212243004
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 08/08/14 00:27
2,4,6-Trichlorophenol ug/L ND 10.0 08/08/14 00:27
2,4-Dichlorophenol ug/L ND 5.0 08/08/14 00:27
2,4-Dimethylphenol ug/L ND 10.0 08/08/14 00:27
2,4-Dinitrophenol ug/L ND 50.0 08/08/14 00:27
2,4-Dinitrotoluene ug/L ND 5.0 08/08/14 00:27
2,6-Dinitrotoluene ug/L ND 5.0 08/08/14 00:27
2-Chloronaphthalene ug/L ND 5.0 08/08/14 00:27
2-Chlorophenol ug/L ND 5.0 08/08/14 00:27
2-Nitrophenol ug/L ND 5.0 08/08/14 00:27
3,3'-Dichlorobenzidine ug/L ND 25.0 08/08/14 00:27
4,6-Dinitro-2-methylphenol ug/L ND 20.0 08/08/14 00:27
4-Bromophenylphenyl ether ug/L ND 5.0 08/08/14 00:27
4-Chloro-3-methylphenol ug/L ND 5.0 08/08/14 00:27
4-Chlorophenylphenyl ether ug/L ND 5.0 08/08/14 00:27
4-Nitrophenol ug/L ND 50.0 08/08/14 00:27
Acenaphthene ug/L ND 5.0 08/08/14 00:27
Acenaphthylene ug/L ND 5.0 08/08/14 00:27
Anthracene ug/L ND 5.0 08/08/14 00:27
Benzo(a)anthracene ug/L ND 5.0 08/08/14 00:27
Benzo(a)pyrene ug/L ND 5.0 08/08/14 00:27
Benzo(b)fluoranthene ug/L ND 5.0 08/08/14 00:27
Benzo(g,h,i)perylene ug/L ND 5.0 08/08/14 00:27
Benzo(k)fluoranthene ug/L ND 5.0 08/08/14 00:27
bis(2-Chloroethoxy)methane ug/L ND 10.0 08/08/14 00:27
bis(2-Chloroethyl) ether ug/L ND 5.0 08/08/14 00:27
bis(2-Chloroisopropyl) ether ug/L ND 5.0 08/08/14 00:27
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 08/08/14 00:27
Butylbenzylphthalate ug/L ND 5.0 08/08/14 00:27
Chrysene ug/L ND 5.0 08/08/14 00:27
Di-n-butylphthalate ug/L ND 5.0 08/08/14 00:27
Di-n-octylphthalate ug/L ND 5.0 08/08/14 00:27
Dibenz(a,h)anthracene ug/L ND 5.0 08/08/14 00:27
Diethylphthalate ug/L ND 5.0 08/08/14 00:27
Dimethylphthalate ug/L ND 5.0 08/08/14 00:27
Fluoranthene ug/L ND 5.0 08/08/14 00:27
Fluorene ug/L ND 5.0 08/08/14 00:27
Hexachloro-1,3-butadiene ug/L ND 5.0 08/08/14 00:27
Hexachlorobenzene ug/L ND 5.0 08/08/14 00:27
Hexachlorocyclopentadiene ug/L ND 10.0 08/08/14 00:27
Hexachloroethane ug/L ND 5.0 08/08/14 00:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1258662
Associated Lab Samples:92212243001, 92212243002, 92212243003, 92212243004
Matrix:Water
Analyzed
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 08/08/14 00:27
Isophorone ug/L ND 10.0 08/08/14 00:27
N-Nitroso-di-n-propylamine ug/L ND 5.0 08/08/14 00:27
N-Nitrosodimethylamine ug/L ND 5.0 08/08/14 00:27
N-Nitrosodiphenylamine ug/L ND 10.0 08/08/14 00:27
Naphthalene ug/L ND 5.0 08/08/14 00:27
Nitrobenzene ug/L ND 5.0 08/08/14 00:27
Pentachlorophenol ug/L ND 10.0 08/08/14 00:27
Phenanthrene ug/L ND 5.0 08/08/14 00:27
Phenol ug/L ND 5.0 08/08/14 00:27
Pyrene ug/L ND 5.0 08/08/14 00:27
2,4,6-Tribromophenol (S)%84 10-137 08/08/14 00:27
2-Fluorobiphenyl (S)%78 15-120 08/08/14 00:27
2-Fluorophenol (S)%44 10-120 08/08/14 00:27
Nitrobenzene-d5 (S)%74 10-120 08/08/14 00:27
Phenol-d6 (S)%31 10-120 08/08/14 00:27
Terphenyl-d14 (S)%93 11-131 08/08/14 00:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1258663LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 36.850 74 44-142
2,4,6-Trichlorophenol ug/L 41.550 83 37-144
2,4-Dichlorophenol ug/L 46.350 93 1-191
2,4-Dimethylphenol ug/L 46.950 94 32-119
2,4-Dinitrophenol ug/L 233250 93 1-181
2,4-Dinitrotoluene ug/L 51.050 102 39-139
2,6-Dinitrotoluene ug/L 48.950 98 50-158
2-Chloronaphthalene ug/L 38.450 77 60-118
2-Chlorophenol ug/L 38.650 77 23-134
2-Nitrophenol ug/L 43.550 87 29-182
3,3'-Dichlorobenzidine ug/L 99.2100 99 1-262
4,6-Dinitro-2-methylphenol ug/L 92.4100 92 1-181
4-Bromophenylphenyl ether ug/L 43.750 87 53-127
4-Chloro-3-methylphenol ug/L 101100 101 22-147
4-Chlorophenylphenyl ether ug/L 47.250 94 25-158
4-Nitrophenol ug/L 108250 43 1-132
Acenaphthene ug/L 43.150 86 47-145
Acenaphthylene ug/L 43.350 87 33-145
Anthracene ug/L 44.650 89 1-166
Benzo(a)anthracene ug/L 42.150 84 33-143
Benzo(a)pyrene ug/L 41.750 83 17-163
Benzo(b)fluoranthene ug/L 41.850 84 24-159
Benzo(g,h,i)perylene ug/L 41.250 82 1-219
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1258663LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(k)fluoranthene ug/L 36.850 74 11-162
bis(2-Chloroethoxy)methane ug/L 43.550 87 33-184
bis(2-Chloroethyl) ether ug/L 39.650 79 12-158
bis(2-Chloroisopropyl) ether ug/L 39.250 78 36-166
bis(2-Ethylhexyl)phthalate ug/L 46.850 94 8-158
Butylbenzylphthalate ug/L 46.850 94 1-152
Chrysene ug/L 42.850 86 17-168
Di-n-butylphthalate ug/L 49.850 100 1-118
Di-n-octylphthalate ug/L 50.950 102 4-146
Dibenz(a,h)anthracene ug/L 43.250 86 1-227
Diethylphthalate ug/L 51.150 102 1-114
Dimethylphthalate ug/L 48.350 97 1-112
Fluoranthene ug/L 48.150 96 26-137
Fluorene ug/L 47.650 95 59-121
Hexachloro-1,3-butadiene ug/L 35.650 71 24-116
Hexachlorobenzene ug/L 40.250 80 1-152
Hexachlorocyclopentadiene ug/L 30.750 61 25-150
Hexachloroethane ug/L 33.050 66 40-113
Indeno(1,2,3-cd)pyrene ug/L 34.350 69 1-171
Isophorone ug/L 45.550 91 21-196
N-Nitroso-di-n-propylamine ug/L 47.950 96 1-230
N-Nitrosodimethylamine ug/L 22.350 45 25-150
N-Nitrosodiphenylamine ug/L 43.250 86 25-150
Naphthalene ug/L 40.350 81 21-133
Nitrobenzene ug/L 42.050 84 35-180
Pentachlorophenol ug/L 87.0100 87 14-176
Phenanthrene ug/L 42.350 85 54-120
Phenol ug/L 19.250 38 5-112
Pyrene ug/L 40.550 81 52-115
2,4,6-Tribromophenol (S)%93 10-137
2-Fluorobiphenyl (S)%81 15-120
2-Fluorophenol (S)%45 10-120
Nitrobenzene-d5 (S)%82 10-120
Phenol-d6 (S)%32 10-120
Terphenyl-d14 (S)%85 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1258664MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92211885001
1258665
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 100 69 44-14275 9 30100ND68.6 75.1
2,4,6-Trichlorophenol ug/L 100 78 37-14481 4 30100ND78.1 81.0
2,4-Dichlorophenol ug/L 100 94 1-19190 5 30100ND94.4 89.7
2,4-Dimethylphenol ug/L 100 95 32-11995 0 30100ND95.1 95.1
2,4-Dinitrophenol ug/L 500 101 1-18181 21 30500ND503406
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1258664MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92211885001
1258665
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4-Dinitrotoluene ug/L 100 105 39-139101 4 30100ND105101
2,6-Dinitrotoluene ug/L 100 95 50-15894 1 30100ND95.1 94.2
2-Chloronaphthalene ug/L 100 71 60-11875 6 30100ND70.7 74.8
2-Chlorophenol ug/L 100 77 23-13478 1 30100ND76.8 77.7
2-Nitrophenol ug/L 100 80 29-18287 8 30100ND80.4 86.7
3,3'-Dichlorobenzidine ug/L 200 90 1-26287 4 30200ND180174
4,6-Dinitro-2-methylphenol ug/L 200 88 1-18186 3 30200ND177172
4-Bromophenylphenyl ether ug/L 100 79 53-12788 11 30100ND78.6 88.0
4-Chloro-3-methylphenol ug/L 200 114 22-147103 10 30200ND228206
4-Chlorophenylphenyl ether ug/L 100 92 25-15894 2 30100ND91.8 93.7
4-Nitrophenol ug/L 500 69 1-13259 16 30500ND344293
Acenaphthene ug/L 100 82 47-14586 5 30100ND82.0 85.9
Acenaphthylene ug/L 100 82 33-14584 3 30100ND81.8 84.0
Anthracene ug/L 100 82 1-16686 4 30100ND82.4 85.7
Benzo(a)anthracene ug/L 100 79 33-14380 1 30100ND79.5 80.4
Benzo(a)pyrene ug/L 100 77 17-16378 1 30100ND77.4 77.8
Benzo(b)fluoranthene ug/L 100 77 24-15972 6 30100ND76.8 72.5
Benzo(g,h,i)perylene ug/L 100 75 1-21986 14 30100ND74.8 86.2
Benzo(k)fluoranthene ug/L 100 69 11-16273 5 30100ND69.5 73.3
bis(2-Chloroethoxy)methane ug/L 100 81 33-18486 6 30100ND81.1 86.0
bis(2-Chloroethyl) ether ug/L 100 74 12-15879 7 30100ND74.1 79.1
bis(2-Chloroisopropyl) ether ug/L 100 70 36-16677 10 30100ND69.7 77.3
bis(2-Ethylhexyl)phthalate ug/L 100 93 8-15895 2 30100ND93.2 95.4
Butylbenzylphthalate ug/L 100 93 1-15295 2 30100ND93.3 95.5
Chrysene ug/L 100 79 17-16881 2 30100ND79.1 81.1
Di-n-butylphthalate ug/L 100 95 1-11897 2 30100ND95.4 97.4
Di-n-octylphthalate ug/L 100 98 4-14697 1 30100ND98.5 97.2
Dibenz(a,h)anthracene ug/L 100 78 1-22788 12 30100ND78.3 88.1
Diethylphthalate ug/L 100 102 1-114101 1 30100ND102101
Dimethylphthalate ug/L 100 94 1-11297 3 30100ND93.8 97.1
Fluoranthene ug/L 100 91 26-13791 0 30100ND90.9 90.9
Fluorene ug/L 100 93 59-12194 2 30100ND93.0 94.5
Hexachloro-1,3-butadiene ug/L 100 65 24-11676 16 30100ND65.0 76.1
Hexachlorobenzene ug/L 100 75 1-15280 7 30100ND74.7 80.2
Hexachlorocyclopentadiene ug/L R11004725-15064 32 30100ND46.6 64.1
Hexachloroethane ug/L 100 62 40-11372 14 30100ND62.3 71.9
Indeno(1,2,3-cd)pyrene ug/L 100 62 1-17169 11 30100ND62.0 68.9
Isophorone ug/L 100 84 21-19696 13 30100ND83.9 96.0
N-Nitroso-di-n-propylamine ug/L 100 84 1-23090 7 30100ND84.4 90.4
N-Nitrosodimethylamine ug/L 100 49 25-15059 19 30100ND48.8 58.9
N-Nitrosodiphenylamine ug/L 100 78 25-15085 8 30100ND78.3 85.1
Naphthalene ug/L 100 76 21-13380 6 30100ND75.8 80.2
Nitrobenzene ug/L 100 76 35-18081 7 30100ND75.8 81.1
Pentachlorophenol ug/L 200 86 14-17682 4 30200ND172165
Phenanthrene ug/L 100 79 54-12082 5 30100ND78.7 82.3
Phenol ug/L 100 49 5-11249 0 30100ND49.1 49.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1258664MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92211885001
1258665
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Pyrene ug/L 100 78 52-11584 7 30100ND78.2 83.7
2,4,6-Tribromophenol (S)%86 10-13786
2-Fluorobiphenyl (S)%71 15-12076
2-Fluorophenol (S)%53 10-12056
Nitrobenzene-d5 (S)%74 10-12078
Phenol-d6 (S)%42 10-12042
Terphenyl-d14 (S)%79 11-13185
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92212243
Yogi Foods
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/29235
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:92212243001, 92212243002, 92212243003, 92212243004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1257667
Associated Lab Samples:92212243001, 92212243002, 92212243003, 92212243004
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N208/07/14 14:44
Aliphatic (C19-C36)ug/L ND 100 N208/07/14 14:44
Aromatic (C11-C22)ug/L ND 100 N208/07/14 14:44
2-Bromonaphthalene (S)%83 40-140 08/07/14 14:44
2-Fluorobiphenyl (S)%69 40-140 08/07/14 14:44
Nonatriacontane (S)%62 40-140 08/07/14 14:44
o-Terphenyl (S)%64 40-140 08/07/14 14:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1257668LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1257669
Aliphatic (C09-C18)ug/L 157 N23005240-14064193 21 50
Aliphatic (C19-C36)ug/L 253 N24006340-14076303 18 50
Aromatic (C11-C22)ug/L 675 N28507940-14070594 13 50
2-Bromonaphthalene (S)%83 40-14080
2-Fluorobiphenyl (S)%83 40-14072
Nonatriacontane (S)%54 40-14066
o-Terphenyl (S)%78 40-14066
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 44
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92212243
Yogi Foods
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
C9-C12 range is under reporting limit due to dilution made for C5-C8 range.1g
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery was outside laboratory control limits due to matrix interferences.M3
The lab does not hold TNI accreditation for this parameter.N2
RPD value was outside control limits.R1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 44
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92212243
Yogi Foods
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92212243001 OEXT/29317 GCSV/18499MW1EPA 504.1 EPA 504.1
92212243002 OEXT/29317 GCSV/18499MW2EPA 504.1 EPA 504.1
92212243003 OEXT/29317 GCSV/18499MW3EPA 504.1 EPA 504.1
92212243004 OEXT/29317 GCSV/18499MW4EPA 504.1 EPA 504.1
92212243001 OEXT/29235 GCSV/18470MW1MADEP EPH MADEP EPH
92212243002 OEXT/29235 GCSV/18470MW2MADEP EPH MADEP EPH
92212243003 OEXT/29235 GCSV/18470MW3MADEP EPH MADEP EPH
92212243004 OEXT/29235 GCSV/18470MW4MADEP EPH MADEP EPH
92212243001 GCV/8433MW1MADEP VPH
92212243002 GCV/8433MW2MADEP VPH
92212243003 GCV/8427MW3MADEP VPH
92212243004 GCV/8427MW4MADEP VPH
92212243001 MPRP/16631 ICP/15017MW1EPA 3010 EPA 6010
92212243002 MPRP/16631 ICP/15017MW2EPA 3010 EPA 6010
92212243003 MPRP/16631 ICP/15017MW3EPA 3010 EPA 6010
92212243004 MPRP/16631 ICP/15017MW4EPA 3010 EPA 6010
92212243001 OEXT/29257 MSSV/9502MW1EPA 625 EPA 625
92212243002 OEXT/29257 MSSV/9502MW2EPA 625 EPA 625
92212243003 OEXT/29257 MSSV/9502MW3EPA 625 EPA 625
92212243004 OEXT/29257 MSSV/9502MW4EPA 625 EPA 625
92212243001 MSV/27865MW1SM 6200B
92212243002 MSV/27865MW2SM 6200B
92212243003 MSV/27865MW3SM 6200B
92212243004 MSV/27891MW4SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/12/2014 04:19 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 44
Page 43 of 44
Page 44 of 44