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Home My WebLink About25027_Pharr Yarns Brownfields Assessment Report_20230915#C-1269 Engineering #C-245 Geology Brownfields Assessment Report Pharr Yarns – Lowell 700 West 1st Street Lowell, North Carolina Brownfields Project No. 25027-21-036 H&H Job No. HNY-001 September 15, 2023 i https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc Brownfields Assessment Report Pharr Yarns – Lowell 700 West 1st Street Lowell, North Carolina Brownfields Project No. 25027-21-036 H&H Job No. HNY-001 Table of Contents 1.0 Introduction and Background ...............................................................................................1 1.1 Site Background Information ................................................................................................1 1.2 Previous Assessment Activities .............................................................................................2 1.3 Brownfields Activities ...........................................................................................................4 2.0 July 2023 Brownfields Assessment ........................................................................................5 3.0 Soil Assessment Activities .......................................................................................................6 3.1 Soil Sampling Methodology ..................................................................................................6 3.2 Soil Analytical Results ..........................................................................................................8 4.0 Groundwater Assessment Activities ....................................................................................10 4.1 Temporary Monitoring Well Installation and Groundwater Sampling Methodology .........10 4.2 Groundwater Analytical Results ..........................................................................................12 5.0 Vapor Assessment Activities ................................................................................................14 5.1 Soil Gas Sampling Methodology .........................................................................................14 5.2 Soil Gas Analytical Results .................................................................................................16 5.3 Vapor Intrusion Evaluation .................................................................................................17 6.0 Quality Assurance – Quality Control ..................................................................................19 6.1 Trip Blank ............................................................................................................................19 6.2 Field Duplicates ...................................................................................................................19 7.0 Receptor Survey ....................................................................................................................21 8.0 Summary and Conclusions ..................................................................................................23 ii https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc List of Tables Table 1 Summary of Soil Analytical Data Table 2 Summary of Well Construction and Depth to Groundwater Data Table 3 Summary of Groundwater Analytical Data Table 4 Summary of Exterior Soil Gas Analytical Data List of Figures Figure 1 Site Location Map Figure 2 Site Map Figure 3 Sample Location Map Figure 4 Soil Impacts Above PSRGs Figure 5 Shallow Groundwater Potentiometric Surface Map Figure 6 Groundwater Impacts Above NC 2L Standards Figure 7 Summary of Vapor Intrusion Risk Figure 8 Receptor Survey Map List of Appendices Appendix A Boring Logs Appendix B Laboratory Analytical Reports Appendix C Groundwater and Soil Gas Sampling Forms Appendix D DEQ Risk Calculator Input/Output Forms Appendix E Receptor Survey Form 1 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc Brownfields Assessment Report Pharr Yarns – Lowell 700 West 1st Street Lowell, North Carolina Brownfields Project No. 25027-21-036 H&H Job No. HNY-001 1.0 Introduction and Background On behalf of Lowell OZB, LLC (Prospective Developer or PD), Hart & Hickman, PC (H&H) has prepared this Brownfields Assessment Report for the Pharr Yarns – Lowell Brownfields property (Brownfields Project No. 25027-21-036) located at 700 West 1st Street in Lowell, Gaston County, North Carolina (Site). A Site location map is provided as Figure 1. The Site consists of three contiguous parcels of land (Gaston County Parcel Identification Nos. 306362, 306363, and 127737) that total approximately 17.45 acres. The southeastern portion of the Site is developed with a small garage structure. A former roadway crosses the east-central portion of the Site, and an overhead electrical right-of-way crosses the western and northern portions of the Site. West 1st Street bisects the northern and southern portions of the subject Site. The Site and surrounding area are depicted on Figure 2. 1.1 Site Background Information The northern portion of the Site was developed with the Lowell Yarn Mill and ancillary structures/residences in the earliest historical resource reviewed, a 1914 topographic map. The mill was subsequently operated by United Spinners and Pharr Mills. Mill operations consisted of carding, spinning, and winding of cotton yarns. The mill facility consisted of two main mill buildings, a cotton warehouse building, a water reservoir, multiple storage buildings, and administrative offices. By the 1930s, several unidentified stores were developed in the southern portion of the Site. The mill operations ceased in the early 2000s, and the mill buildings were razed by 2004. The administrative offices remained in the eastern portion of the Site until the office building was razed in 2018. The subject Site has remained predominately vacant land since that time. 2 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc 1.2 Previous Assessment Activities In November and December 2020, H&H performed a Phase I Environmental Site Assessment (ESA) of the Site. The following Recognized Environmental Conditions (RECs) were identified:  historical textile mill operations and associated areas of potential concern including a machine shop, a coal trestle and nearby chimney (presumably used to burn coal), and an electrical substation;  two former 1,000-gallon fuel oil underground storage tanks (USTs) and two 5,000-gallon fuel oil USTs that were reportedly removed near the former mill buildings; and  a suspect UST located adjacent to the garage structure in the southeastern portion of the subject Site. Although not identified as a REC, two open trash bags of cementitious building materials and an unidentified black building material that were considered suspect asbestos-containing materials (ACMs) were observed in the northeastern portion of the Site. H&H identified the suspect asbestos-containing debris as a potential environmental concern. In January 2021, H&H provided oversight during a ground-penetrating radar (GPR) survey and performed soil and groundwater sampling activities at the Site to evaluate potential environmental impacts associated with the RECs noted above. In addition, H&H collected samples of the suspect asbestos-containing debris. A summary of the results of the Phase II ESA is provided below. GPR Survey  Results of the GPR survey indicated evidence of two former UST basins (reportedly containing two fuel oil USTs in each basin) in the northern portion of the Site and one former UST basin in the southern portion of the Site.  An existing UST (reportedly containing fuel oil) was identified in the eastern portion of the Site during the GPR survey. The former Site owner subsequently removed this UST. 3 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc Soil  Soil analytical data did not indicate the presence of Total Petroleum Hydrocarbons-Diesel Range Organics (TPH-DRO) or Total Petroleum Hydrocarbons-Gasoline Range Organics (TPH-GRO) at concentrations above the North Carolina Department of Environmental Quality (DEQ) UST Section Action Levels in samples collected adjacent to former USTs.  Tetrachloroethene (PCE) was detected in samples SB-4 (11-13 ft) and SB-5 (3-5 ft) at concentrations above the Protection of Groundwater Preliminary Soil Remediation Goal (PSRG) but below the Residential and Industrial/Commercial PSRGs. Sample SB-4 (11-13 ft) was collected adjacent to the former coal trestle/machine shop, and sample SB-5 (3-5 ft) was collected within the former machine shop.  Multiple polynuclear aromatic hydrocarbons (PAHs) were detected in samples SB-5 (3-5 ft) and SB-13 (1-3 ft), which were collected within the former machine shop and the former carpentry shop, respectively. The detected benzo(a)anthracene concentration in sample SB-5 (3-5 ft) exceeds the Protection of Groundwater PSRG. The detected benzo(a)pyrene concentrations in samples SB-5 (3-5 ft) and SB-13 (1-3 ft) exceed the Protection of Groundwater and Residential PSRGs.  No polychlorinated biphenyls (PCBs) were detected above the laboratory method detection limits (MDLs) in sample SB-3 (1-3 ft), which was collected at the former electrical substation. Groundwater  Groundwater analytical data indicate that PCE and trichloroethene (TCE) were detected in temporary well sample TMW-2 at concentrations above the respective North Carolina 2L Groundwater Standards (2L Standards). The detected PCE and TCE concentrations in TMW-2 also exceed the respective Non-Residential Vapor Intrusion Groundwater Screening Levels (GWSLs). Sample TMW-2 was collected downgradient of the former machine shop.  PCE was also detected in samples TMW-3, TMW-4, and TMW-6 at concentrations greater than or equal to the 2L Standard. These samples were collected in the northeastern, eastern, and southern portions of the Site, respectively. 4 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc Suspect Asbestos Debris  Results of asbestos analysis did not indicate the presence of asbestos in the debris samples collected from the Site. Phase II ESA soil and groundwater data are summarized in Tables 1 and 2, respectively, and sample locations are shown on Figure 3. 1.3 Brownfields Activities To address environmental impacts on the Site, a Brownfields Property Application was submitted for the Site on March 29, 2021. A Letter of Eligibility was received from the DEQ Brownfields Redevelopment Section on August 5, 2021. Brownfields redevelopment plans include the construction of three warehouse buildings north of West 1st Street and two commercial flex buildings south of West 1st Street. The industrial/commercial complex will also include paved ground level parking lots, loading areas, and driveways. H&H prepared a Brownfields Assessment Work Plan dated June 20, 2023 (Work Plan) to perform additional assessment to address data gaps identified during a Brownfields kick-off meeting in October 2021. DEQ approved the Work Plan on July 17, 2023. H&H conducted Brownfields assessment activities in July 2023. Details of the Brownfields assessment activities are described in the following sections. 5 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc 2.0 July 2023 Brownfields Assessment Brownfields assessment activities were completed in July 2023 and included the collection of soil, groundwater, and soil gas samples to further evaluate potential impacts associated with historical on-Site operations and to evaluate risk associated with proposed commercial/industrial redevelopment of the Site. In addition, H&H performed a receptor survey in accordance with DEQ Brownfields Redevelopment Section guidelines. As part of the assessment activities, soil borings were advanced in primary areas of planned soil disturbance during grading and construction activities. H&H also completed groundwater assessment activities in the northern, central, and southern portions of the Site. To evaluate the potential for structural vapor intrusion into the proposed industrial/commercial buildings, H&H conducted soil gas assessment activities within the footprint of each of the proposed buildings. Prior to conducting field activities, H&H contacted North Carolina 811, the public utility locator, to mark subsurface utilities at the Site. H&H also contracted with a private utility locator to mark utilities which were not identified by the public locator using GPR and electromagnetic methods. In addition, H&H directed the drilling contractor to hand clear each boring to a depth of approximately 5 feet below ground surface (ft bgs) to further screen the boring locations for the presence of subsurface utilities prior to utilizing mechanical drilling equipment. The assessment activities were performed in general accordance with the DEQ Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup of Contaminated Sites (Guidelines) dated September 2022, the DEQ Division of Waste Management (DWM) Vapor Intrusion Guidance (VI Guidance) dated March 2018, the most recent versions of the U.S. Environmental Protection Agency (EPA) Region IV Lab Services and Applied Sciences Division (LSASD) Field Branches Quality System and Technical Procedures guidance, and the DEQ- approved Work Plan. 6 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc 3.0 Soil Assessment Activities To assist in management of soil generated during grading activities and to further evaluate potential soil impacts at the Site, Innovative Environmental Technologies (IET) advanced 23 soil borings for the collection of composite soil samples within proposed building footprints. Additionally, IET advanced three background soil borings in the western portion of the Site for evaluation of naturally occurring metals. Locations of the soil borings are shown on Figure 3. A discussion of the soil sampling activities and results is provided in the following sections. 3.1 Soil Sampling Methodology IET used a decontaminated stainless steel hand auger to advance 26 soil borings to approximately 5.5 ft bgs in locations shown on Figure 3 and described below.  Four soil borings (CS-1A through CS-1D) were advanced within the footprint of proposed Building A in the northern portion of the Site.  Three soil borings (CS-2A through CS-2C) were advanced within the northern portion of proposed Building B in the northern portion of the Site.  Three soil borings (CS-3A through CS-3C) were advanced within the southern portion of proposed Building B in the northern portion of the Site.  Four soil borings (CS-4A through CS-4D) were advanced within the footprint of proposed Building C in the northern portion of the Site.  Three soil borings (CS-5A through CS-5C) were advanced within the footprint of proposed Building A in the southern portion of the Site.  Three soil borings (CS-6A through CS-6C) were advanced within the western portion of proposed Building B in the southern portion of the Site.  Three soil borings (CS-7A through CS-7C) were advanced within the eastern portion of proposed Building B in the southern portion of the Site. 7 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc  Three background soil borings (BG-1 through BG-3) were advanced in an undeveloped area in the western portion of the Site to evaluate naturally occurring metals concentrations. For each evaluation area, continuous soil samples were collected from each of the soil borings and were logged for lithological description and field screened for indication of potential impacts by observation for staining, unusual odors, and the presence of volatile organic vapors using a calibrated photoionization detector (PID). No obvious evidence of soil impacts was identified by field personnel during field screening. Therefore, the soil sample aliquots from each composite soil sample area were combined in the field to create representative composite soil samples for the 0-2 ft depth interval. Boring logs including lithologic descriptions and field screening results for each soil boring are provided in Appendix A. H&H collected one soil sample from each of the composite soil sample area for laboratory analysis of semi-volatile organic compounds (SVOCs) by EPA Method 8270E and Resource Conservation and Recovery Act (RCRA) metals by EPA Methods 6020B/7471B, and hexavalent chromium by EPA Method 7199. A grab soil sample was collected from one soil boring within each composite soil sample area based on field screening results. The grab soil samples were collected from undisturbed portions of soil for laboratory analysis of VOCs by EPA Method 8260D. One background soil sample was collected from each background boring from the 0-2 ft interval for laboratory analysis of RCRA Metals by EPA Methods 6020B/7471B and hexavalent chromium by EPA Method 7199. The soil samples selected for laboratory analysis were collected directly into dedicated laboratory-supplied sample containers, labeled with the date, time, and sample identification, placed in a laboratory supplied sample cooler with ice, and submitted to Pace Analytical Services, LLC (Pace) under standard chain of custody protocols. Each soil boring location was estimated using a hand-held global positioning system (GPS) unit. Based on the lack of obvious evidence of significant soil impacts, soil cuttings were spread on- Site in the vicinity of the borings. 8 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc 3.2 Soil Analytical Results A tabular summary of the soil analytical results is presented in Table 1. The laboratory analytical report and chain of custody record are provided in Appendix B. The laboratory analytical results were compared to the DEQ Inactive Hazardous Sites Branch (IHSB) Residential and Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs) dated July 2023. Metals concentrations were also compared to Site-specific background levels identified in samples BG-1 through BG-3 and regional background levels published in Elements in North American Soils by Dragun and Chekiri (2005). A discussion of the soil analytical results is provided below. VOCs Trace levels of various VOCs including petroleum constituents and PCE were detected in at least one grab soil sample at concentrations above the MDLs. However, none of the detected VOC concentrations exceed the Residential or Industrial/Commercial PSRGs. TCE was not detected above the MDLs in any of the soil samples. SVOCs The PAHs benzo(a)anthracene (up to 12.3 mg/kg), benzo(a)pyrene (up to 9.14 mg/kg), benzo(b)fluoranthene (up to 13.2 mg/kg), and dibenz(a,h)anthracene (up to 2.27 mg/kg), and/or indeno(1,2,3-cd)pyrene (5.63 mg/kg) were detected above the Residential PSRGs in samples CS-1, CS-2/SB-DUP, and CS-7. The detected concentrations of benzo(a)pyrene and dibenz(a,h)anthracene in sample CS-1 also exceed the Industrial/Commercial PSRG of 2.1 mg/kg for both compounds. No SVOCs were detected above the MDLs in samples CS-3 through CS-5. A summary of SVOCs in soil samples at concentrations above PSRGs is depicted as Figure 4. Metals Arsenic was detected in samples CS-1 through CS-7 at concentrations ranging from 6.01 mg/kg to 11.8 mg/kg, which exceed the Industrial/Commercial PSRG of 3.0 mg/kg. The detected 9 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc arsenic concentrations are generally consistent with the range of Site-specific background concentrations of 3.29-8.42 mg/kg and within the published range of background concentrations of 1.0-18 mg/kg for North Carolina soils. Therefore, arsenic detections in composite soil samples are likely naturally occurring. Hexavalent chromium was detected in samples CS-1 through CS-7 at concentrations ranging from 0.512 J mg/kg to 1.44 mg/kg, which exceed the Residential PSRG of 0.31 mg/kg but are below the Industrial/Commercial PSRG of 6.5 mg/kg. The “J flag” indicates an estimated concentration that is above the MDL but below the laboratory reporting limit. Hexavalent chromium was also detected above the Residential PSRG in background soil samples BG-2 and BG-3 at concentrations of 0.527 J mg/kg ad 0.380 J mg/kg, respectively. Although these detections of hexavalent chromium exceed the Residential PSRG, the detections are generally consistent with concentrations detected at numerous properties across North Carolina, including undeveloped properties, and are likely naturally occurring. The remaining metals detections are below Residential and Industrial/Commercial PSRGs or generally consistent with Site-specific and/or published regional background levels. 10 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc 4.0 Groundwater Assessment Activities H&H provided oversight during installation of six temporary groundwater monitoring wells (TMW-7 through TMW-12) at the Site. Groundwater samples were collected for laboratory analysis from each temporary monitoring well to evaluate groundwater conditions. Locations of the temporary monitoring wells are depicted on Figure 3 and described below.  Two temporary wells (TMW-7 and TMW-8) were installed in the northern (downgradient) portion of the Site to assess the potential for off-Site migration of groundwater contaminants.  One temporary well (TMW-9) was installed in the footprint of proposed Building A in the northern portion of the Site.  One temporary well (TMW-10) was installed in the footprint of proposed Building B in the northern portion of the Site.  One temporary well (TMW-11) was installed in the footprint of proposed Building A in the southern portion of the Site.  One temporary well (TMW-12) was installed in the footprint of proposed Building B in the southern portion of the Site. Details of the groundwater sampling activities and results are provided in the following sections. 4.1 Temporary Monitoring Well Installation and Groundwater Sampling Methodology The temporary well borings were advanced beyond the water table utilizing direct push technology (DPT) drilling techniques to depths ranging from approximately 25 to 30 ft bgs. Continuous soil samples were collected from the temporary monitoring well borings and logged for lithologic description, observed for obvious evidence of staining and unusual odors, and field screened for the presence of volatile organic vapors using a calibrated PID. No obvious evidence of impacts was observed during field screening. 11 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc Temporary monitoring wells were constructed of 2-inch diameter PVC with 15 ft of pre-packed well screen set to bracket the water table and 2-inch diameter PVC well casing to the ground surface. A filter sand pack was installed from the bottom of each temporary well boring to approximately 2 ft above each well screen, and a hydrated bentonite seal was installed above the filter sand pack. Temporary monitoring well boring logs with well construction details are provided in Appendix A. Following installation of the temporary monitoring wells, the wells were allowed to equilibrate to static conditions, and a decontaminated electronic water level indicator was used to measure the depth to the water table relative to the top of casing. Groundwater was measured at depths ranging from approximately 20.00 ft below top of casing (TMW-8) in the northern portion of the Site to approximately 29.12 ft below top of casing (TMW-10) in the east-central portion of the Site. To evaluate groundwater flow at the Site, H&H surveyed the top of casing elevations for TMW-7, TMW-8, and TMW-10 relative to an arbitrary datum of 100 ft set for a known benchmark on the Site. The top of casing elevations for the remaining wells were not surveyed due to the presence of dense vegetation at the well locations. Based on the depth to groundwater data collected for TMW-7, TMW-8, and TMW-10 on July 20, 2023, shallow aquifer groundwater flow in the northern portion of the Site is to the north-northwest, which is away from the proposed buildings. A tabular summary of well construction details and depth to groundwater measurements is provided as Table 3. A potentiometric surface map is included as Figure 5. Once depth to water measurements were collected, the temporary wells were developed by removing a minimum of 3 to 5 volumes and until field parameters stabilized (pH± 0.1 Standard Units [SU] and conductivity varied no more than 5%) and development water was visibly clear of suspended sediment. Following development, wells were allowed to equilibrate to static conditions and a groundwater sample was collected for laboratory analysis from each temporary monitoring well utilizing low flow/low stress purging techniques using a peristaltic pump and dedicated polyethylene tubing. During purging and sampling, the intake point of the pump tubing was placed in the approximate 12 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc mid-portion of the screened interval of the well, and groundwater was removed at a rate no greater than 200 milliliters per minute. H&H utilized a calibrated water quality meter to collect measurements of pH, temperature, dissolved oxygen, oxidation reduction potential, turbidity, and specific conductivity at three to five-minute intervals during the purging process. Purging was considered complete when the field parameters stabilized (pH ± 0.1 SU, conductivity varied no more than 5%) and, when achievable, turbidity was less than 10 Nephelometric Turbidity Units (NTUs). Groundwater sampling forms completed by sampling personnel are provided in Appendix C. Once groundwater parameters stabilized, groundwater samples for analysis of SVOCs and RCRA metals were collected directly into laboratory-supplied glassware directly from the sample tubing discharge. The groundwater samples submitted for VOC analysis were collected directly into laboratory supplied sample containers using the “soda straw” method to eliminate the potential for volatile compound loss through the pump head. The sample containers were labeled with the sample identification, date, time, and requested analysis, and placed in a laboratory supplied cooler with ice. The groundwater samples were delivered to Pace under standard chain of custody protocols for analyses of VOCs by EPA Method 8260D, SVOCs by EPA Method 8270E, and RCRA metals by EPA Methods 6020B/7470A. The groundwater sample locations were estimated using a hand-held GPS unit. Following sampling activities, the temporary monitoring wells were properly abandoned by IET. Based on the lack of obvious impacts identified during drilling and sampling, well development/purge water and soil cuttings were spread on-Site near the boring locations. 4.2 Groundwater Analytical Results A tabular summary of the groundwater analytical results is presented in Table 3. A copy of the laboratory analytical report and chain of custody record is provided in Appendix B. Groundwater analytical data were compared to the DEQ 2L Standards dated April 2022 and the DEQ DWM Residential and Non-Residential GWSLs dated July 2023. 13 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc VOCs Chloromethane was detected in samples TMW-9 (43.4 µg/L) and TMW-11 (57.6 µg/L) at concentrations above the 2L Standard of 3.0 µg/L. The detection in sample TMW-11 also exceeds the Residential GWSL of 52 µg/L but is below the Non-Residential SGSL of 220 µg/L. PCE was detected in samples TMW-7/TMW-DUP (307/327 µg/L) and TMW-8 (71.8 µg/L) at concentrations above the 2L Standard of 0.7 µg/L and the Non-Residential GWSL of 48 µg/L. TCE was detected in sample TMW-8 at a concentration of 6.1 µg/L, which exceeds the 2L Standard of 3.0 µg/L. The detected concentration of 1.1 J µg/L in sample TMW-DUP exceeds the Residential GWSL of 1.0 µg/L, and the detected concentration in sample TMW-8 exceeds the Non-Residential GWSL of 4.4 µg/L. Methylene chloride was detected in the TMW-7 duplicate sample TMW-DUP at a concentration of 5.3 J µg/L, which is slightly above the 2L Standard of 5.0 µg/L. Methylene chloride, which is a common laboratory contaminant, was not detected above the MDL in the remaining samples including TMW-5, the parent sample for TMW-DUP. Based on these data, the methylene chloride detection in sample TMW-DUP is likely a laboratory artifact and not representative of groundwater conditions at the Site. VOCs that were detected in groundwater samples at concentrations above the 2L Standards are depicted on Figure 6. SVOCs The SVOCs benzoic acid and diethyl phthalate were detected in one or more samples at concentrations above the MDLs but well below the 2L Standards. Metals Low levels of the metals arsenic (up to 0.79 J µg/L), barium (up to 128 µg/L), cadmium (up to 0.38 µg/L), chromium (up to 94 J µg/L), lead (up to 0.91 J µg/L), and selenium (up to 2.4 µg/L) were detected in one or more groundwater samples at concentrations above the MDLs but below the 2L Standards. 14 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc 5.0 Vapor Assessment Activities To evaluate the potential for structural vapor intrusion into the proposed industrial/commercial buildings, H&H installed and sampled 23 temporary soil gas monitoring points (SG-1 through SG-23) at boring locations noted in Section 3.1 which are within the footprints of the proposed buildings. The soil gas sample locations are shown on Figure 3 and described below.  Four soil gas sampling points (SG-1 through SG-4) were installed in the footprint of proposed Building A in the northern portion of the Site.  Six soil gas sampling points (SG-5 through SG-10) were installed in the footprint of proposed Building B in the northern portion of the Site.  Four soil gas sampling points (SG-11 through SG-14) were installed in the footprint of proposed Building C in the northern portion of the Site.  Three soil gas sampling points (SG-15 through SG-17) were installed in the footprint of proposed Building A in the southern portion of the Site.  Six soil gas sampling points (SG-18 through SG-23) were installed in the footprint of proposed Building B in the southern portion of the Site. Details of the soil gas sampling activities and results are provided in the following sections. 5.1 Soil Gas Sampling Methodology Soil Gas Sample Point Installation The soil gas monitoring points were installed at depths of approximately 5.5 ft bgs using a stainless-steel hand auger. Continuous soil samples were collected from the hand auger bucket and logged for lithologic description, observed for obvious evidence of staining and unusual odors, and field screened for the presence of volatile organic vapors using a calibrated PID. Field screening results did not indicate obvious evidence of potential impacts in the soil gas monitoring point borings. Boring logs including lithologic descriptions and field screening results are provided in Appendix A. 15 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc Once at target depth, a six-inch stainless steel vapor implant screen attached to a length of Teflon® tubing was installed at the base of each borehole. Filter sand was then placed within the annulus of the boring from the base of the boring to a depth of approximately 6 inches above the top of the vapor screen. The sampling points were completed by placing hydrated bentonite from the top of the filter sand to the ground surface. Soil Gas Sampling Each soil gas sample was collected utilizing a batch certified laboratory-supplied 1.0-liter Summa® canister connected to an air-flow regulator calibrated by the laboratory to collect the soil gas sample at a rate of approximately 100 milliliters per minute. Prior to collection of the soil gas samples, “shut-in” tests were conducted on the sampling train and helium leak checks were conducted at each sampling point. A description of the shut-in test and helium leak testing procedures is provided below. The shut-in test was conducted by connecting the flow regulator with the vacuum gauge to the Summa® canister and sealing the flow regulator with the laboratory provided brass cap. Once the sampling train was “closed”, the sample valve on the Summa® canister was opened and the reading on the vacuum gauge was recorded. The Summa® canister sample valve was then closed, and the vacuum gauge was observed to ensure no vacuum loss occurred. Following the successful shut-in test, the Summa® canister was connected to the sample point via Teflon® sample tubing using a brass nut and ferrule assembly to create an air-tight seal. A leak check was then performed by constructing a shroud over the sampling train and flooding the shroud with helium gas. Helium concentrations inside the shroud were measured using a helium gas detector and maintained at concentrations ranging from approximately 10% to 12%. Once helium concentrations stabilized within the shroud, the sample tubing was purged outside of the shroud using a syringe and a three-way valve to collect purged soil gas into a Tedlar® bag. The purged soil gas was then analyzed using the helium gas detector to ensure that helium concentrations in the soil gas samples were less than 10% of the helium concentrations measured within the shroud. Each soil gas sampling point passed the helium leak check criteria. Soil gas sampling forms are included in Appendix C. 16 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc Following successful leak checks and an equilibration time of at least 24 hours, the soil gas samples were collected by opening the intake valve on the Summa® canister. Vacuum readings on the Summa® canister were recorded prior to and following the sampling period to ensure adequate sample volume was collected. A vacuum of approximately 5 inches of mercury was maintained within the canisters at the conclusion of the sampling event in accordance with DEQ DWM guidance. Following sample collection, the Summa® canisters were shipped to Pace under standard chain-of-custody protocols for analysis of VOCs by EPA Method TO-15. Upon receipt of the samples, the laboratory recorded the final received vacuum pressure for each Summa® canister. After sampling was completed, the soil gas sample locations were estimated using a hand-held GPS unit. The borings were properly abandoned using hydrated bentonite. 5.2 Soil Gas Analytical Results Soil gas analytical data were compared to the DEQ DWM Residential and Non-Residential Soil Gas Screening Levels (SGSLs) dated July 2023. A summary of the analytical results is provided as Table 4, and the laboratory analytical data report and chain of custody records are included in Appendix B. Laboratory analytical results for the soil gas samples indicated the presence of the VOCs benzene (up to 77.3 µg/m3), chloroform (up to 43 µg/m3), ethylbenzene (up to 72 µg/m3), isopropyl alcohol (32,400 µg/m3), PCE (up to 605 µg/m3), and TCE (27.8 µg/m3) in one or more soil gas samples at concentrations above Residential SGSLs. The detected concentration of isopropyl alcohol (32,400 µg/m3) in sample SG-22 also exceeds the Non-Residential SGSL of 18,000 µg/m3. TCE was not detected above the MDL in soil gas samples SG-1 through SG-20 and SG-22. 17 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc 5.3 Vapor Intrusion Evaluation DEQ DWM Vapor Intrusion SGSLs are conservative and based upon a cumulative lifetime incremental carcinogenic risk (LICR) of 1 x 10-6 for potential carcinogenic effects and a cumulative hazard quotient (HQ) of 0.2 for potential non-carcinogenic effects. Vapor intrusion mitigation or additional assessment is not typically warranted if the calculated cumulative LICR is 1 x 10-4 or less and the non-carcinogenic hazard index (HI) is 1.0 or less. The HI is the sum of HQs for each detected compound. H&H utilized the DEQ Risk Calculator (July 2023) to further evaluate potential cumulative risks for the soil gas to indoor air vapor intrusion pathway for the proposed industrial/commercial buildings. H&H calculated the cumulative risks using the highest concentration of each compound detected in any soil gas sample collected within each of the proposed building areas. Therefore, one cumulative risk calculation was performed for each proposed building. A summary of the results of risk calculations is provided in the table below. Land Use Scenario Calculated Cumulative LICR Calculated Cumulative HI Calculated LICR or HI Exceeds Acceptable Risk Levels? Exposure Unit 1 – Proposed Building A (North) Residential 9.7 x 10-6 0.35 No Non-Residential Worker 7.4 x 10-7 0.028 No Exposure Unit 2 – Proposed Building B (North) Residential 1.0 x 10-5 0.66 No Non-Residential Worker 7.7 x 10-7 0.053 No Exposure Unit 3 – Proposed Building C (North) Residential 2.0 x 10-5 0.65 No Non-Residential Worker 1.5 x 10-6 0.052 No Exposure Unit 4 – Proposed Building A (South) Residential 1.2 x 10-5 0.18 No Non-Residential Worker 9.2 x 10-7 0.015 No 18 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc Land Use Scenario Calculated Cumulative LICR Calculated Cumulative HI Calculated LICR or HI Exceeds Acceptable Risk Levels? Exposure Unit 5 – Proposed Building B (South) Residential 1.5 x 10-5 5.8 Yes Non-Residential Worker 1.1 x 10-6 0.46 No The results of risk calculations indicate that the cumulative carcinogenic and non-carcinogenic risk levels for each of the proposed buildings are below DEQ acceptable levels for the proposed industrial/commercial use. These data indicate that vapor intrusion is not a significant concern at the Site. Calculated carcinogenic and non-carcinogenic risk levels are shown on Figure 7, and risk calculator input/output forms are provided in Appendix D. 19 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc 6.0 Quality Assurance – Quality Control For quality assurance and quality control purposes (QA/QC), non-dedicated equipment and tools were decontaminated prior to use at each boring or sampling location or following exposure to soil or groundwater. Field QA/QC samples were analyzed along with the investigative samples to determine potential variability introduced in sampling, handling, shipping, and analysis. One trip blank was submitted for analysis of VOCs by EPA Method 8260D. In addition, H&H collected duplicate soil, groundwater, and soil gas samples to evaluate the ability of the laboratory to reproduce sample results. Duplicate samples were submitted to the laboratory for the same analysis as the corresponding parent sample. 6.1 Trip Blank The trip blank was prepared by the laboratory and consisted of certified-clean sample containers filled with analyte-free water. The trip blank accompanied the empty laboratory sample containers to the Site, remained within the sample cooler during sampling, and traveled back to the laboratory with field samples. The purpose of a trip blank is to evaluate sample handling conditions and the potential for external contaminants to compromise investigative samples during transit. A trip blank accompanied the field VOC groundwater samples and was submitted for laboratory analysis of VOCs by EPA Method 8260D. Laboratory analytical results of the trip blank sample did not indicate the presence of VOCs at concentrations above the MDLs. Laboratory analytical results of the trip blank are included in the laboratory analytical report in Appendix B. 6.2 Field Duplicates Duplicate samples were collected to evaluate the precision of the field sampling procedures, sample matrix variability, and analytical reproducibility. Duplicate soil and groundwater samples were collected directly into individual laboratory-supplied sample containers using sampling methodologies described in previous sections. The duplicate soil gas samples were 20 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc collected concurrently with the parent samples using a laboratory-supplied T-fitting, which allows for collection of two soil gas samples from one soil gas sampling point simultaneously. The samples were analyzed for the same parameters as the parent samples, and the analytical results were compared with those of the parent samples. The analytical results of the parent samples and the duplicate samples were used to evaluate the cumulative precision of the analytical method, sample matrix, and sample collection techniques. Duplicate sample laboratory analytical results for sample media are presented in the summary tables (Table 1 for soil, Table 2 for groundwater, and Table 4 for soil gas). Review of the duplicate sample results for the soil, groundwater, and soil gas samples did not indicate significant variability compared with the results of the parent samples. 21 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc 7.0 Receptor Survey In July 2023, H&H conducted a receptor survey at the Site and surrounding area in accordance with DEQ Brownfields Redevelopment Section guidance. Receptor survey activities included a pedestrian and vehicular survey to obtain information about land use, water supply, basements, underground utilities, and surface water bodies within a 1,500-ft radius of the Site. In addition, H&H obtained land use and zoning information in the area of the Site using available Gaston County online resources. A receptor survey map is provided as Figure 8, and a copy of the completed DEQ Brownfields Property Receptor Survey form is provided as Appendix E. Results of the receptor survey activities are summarized below. Zoning The Site and an adjacent property to the east are zoned industrial. Adjacent properties to the north, south, and west are zoned mixed-use or residential. An adjacent property to the northwest that is occupied by a church is zoned for civic use. Municipal Water Availability Municipal water supplied by the City of Lowell is available to the Site and surrounding area. H&H did not identify sources of public drinking water within 1,500 ft of the Site based on the DEQ Source Water Assessment Program’s GIS map. Based on the Drinking Water Quality Report published by the City of Lowell, the City of Lowell purchases water from Two Rivers Utilities, which obtains water from Mountain Island Lake. Mountain Island Lake is located approximately 7.5 miles northeast of the Site. Water Supply Wells H&H identified one inactive water supply well in the west-central portion of the Site that appears to have historically provided industrial process water to the former Pharr Yarns facility. This well will be abandoned prior to redevelopment of the Site. No other water supply wells were identified within a 1,500-ft radius of the Site. Additionally, water meters and fire hydrants were observed within the survey area. 22 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc Surface Water Bodies The closest surface water body to the Site is an unnamed pond located approximately 800 ft south of the Site. The pond drains to an unnamed tributary of Duharts Creek. Based on information obtained from the DEQ Division of Water Resources (DWR) Surface Water Classifications GIS map, the subject Site is not located within a protected water supply watershed area. Subsurface Utilities and Structures H&H contacted North Carolina 811, the public utility locator, and contracted a private utility locator to mark subsurface utilities located on the Site. H&H personnel also conducted a visual reconnaissance in the Site area to identify potential subsurface structures within 100 ft of the subject Site. H&H observed evidence of subsurface utilities including sanitary sewer, storm sewer, municipal water, and natural gas adjacent to the Site. An unknown utility line and a sanitary sewer line were identified in the northern portion of the Site. No obvious basements were observed during the visual reconnaissance. Approximate locations of subsurface utilities located in the immediate vicinity of the Site are shown on Figure 8. 23 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc 8.0 Summary and Conclusions H&H completed Brownfields assessment activities at the Pharr Yarns – Lowell Brownfields property located in Lowell, Gaston County, North Carolina. Brownfields assessment activities included a receptor survey and collection of soil, groundwater, and soil gas samples for laboratory analysis to further evaluate potential risks associated with the Site and to assist in management of Site media during future redevelopment activities. A brief summary of the Brownfields assessment activities performed in July 2023 is provided below. Soil  No VOCs were detected in composite soil samples CS-1 through CS-7 at concentrations above the Residential or Industrial/Commercial PSRGs. TCE was not detected above the MDLs in any of the soil samples.  The PAHs benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, and dibenz(a,h)anthracene, and/or indeno(1,2,3-cd)pyrene were detected above the Residential PSRGs in samples CS-1, CS-2/SB-DUP, and CS-7.  The metal hexavalent chromium was detected in samples CS-1 through CS-7 at concentrations above the Residential PSRG but below the Industrial/Commercial PSRG. Arsenic was detected in samples CS-1 through CS-7 at concentrations which exceed the Industrial/Commercial PSRG. The detected arsenic concentrations are generally consistent with the Site-specific background concentrations and are within the published range of background concentrations for North Carolina soils. No published background range was available for hexavalent chromium. Although the detections of hexavalent chromium exceed the Residential PSRG, the detections are generally consistent with concentrations detected at numerous properties across North Carolina, including undeveloped properties. The arsenic and hexavalent chromium detections are likely naturally occurring. Groundwater  Results of groundwater assessment activities indicate the presence of the VOC chloromethane in samples TMW-9 and TMW-11 at concentrations above the 2L 24 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc Standard. PCE was detected above the 2L Standard in samples TMW-7/TMW-DUP, and PCE and TCE were detected above the 2L Standard in sample TMW-8. Based on groundwater elevation data, samples TMW-7/TMW-DUP and TMW-8 were collected downgradient of proposed Buildings A, B, and C in the northern portion of the site.  No other VOCs, SVOCs, or metals were detected at concentrations above the 2L Standards or GWSLs in the groundwater samples. TCE was not detected above the MDL in groundwater samples collected from the southern portion of the Site. Soil Gas  Results of the soil gas assessment activities completed within the footprints of the proposed industrial/commercial buildings indicate the presence of the VOCs benzene, chloroform, ethylbenzene, isopropyl alcohol, PCE, and TCE in one or more samples at concentrations above Residential SGSLs. Additionally, the detected concentration of isopropyl alcohol in one sample (SG-22) exceeds the Non-Residential SGSL.  TCE was not detected above the MDL in samples SG-1 through SG-20 or SG-22.  H&H calculated the cumulative risks using the highest concentration of each compound detected in any soil gas sample collected within each of the proposed building areas. The results of risk calculations indicate that the cumulative carcinogenic and non- carcinogenic risk levels for each of the proposed buildings are below DEQ acceptable levels for the proposed industrial/commercial use. These data indicate that vapor intrusion is not a significant concern at the Site. Receptor Survey  H&H identified one inactive water supply well in the west-central portion of the Site that appears to have historically provided industrial process water to the former Pharr Yarns facility. This well will be abandoned prior to redevelopment of the Site. No other water supply wells were identified within a 1,500-ft radius of the Site.  No surface water bodies or other sensitive receptors were identified of obvious concern in connection with the Site. 25 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/henley capital llc (hny)/hny-001 - lowell, nc esa/brownfields assessment/report/brownfields assessment report - pharr yarns-lowell (9-15-23).doc Based on results of the Brownfields assessment activities, no further soil, groundwater, or soil gas sampling is warranted. Environmental impacts at the Site can be managed in accordance with a DEQ Brownfields-approved Environmental Management Plan (EMP). In addition, soil removed from areas of cut can likely be re-used as fill on-Site or can be considered for transport and disposal at facilities other than a Municipal Solid Waste landfill such as other Brownfields properties, construction and demolition (C&D) debris landfills, and/or land clearing and inert debris (LCID) landfills. The results of soil gas sampling and associated risk calculations do not indicate a significant vapor intrusion concern for the proposed industrial/commercial buildings. Therefore, no vapor intrusion mitigation is warranted based on the proposed industrial/commercial use of the buildings. The TCE impacts in the northern portion of the Site were identified in groundwater sample TMW-2, which is in relatively close proximity to Building B (north). However, TMW-2 is located approximately 260 ft from Building A (north) and approximately 220 ft from Building C (north), and groundwater flow in the vicinity of TMW-2 is to the north-northwest, which is away from Building A (north) and Building C (north). Based on this information, H&H considers Building A (north) and Building C (north) to be in separate exposure units from Building B (north). Based on this information and the calculated non-residential HI in the northern portion of the Site (0.028 to 0.053), pre-occupancy and post-occupancy vapor monitoring is not warranted for Building A (north) and Building C (north) but is warranted for Building B (north). In the southern portion of the Site, TCE was detected in soil gas samples SG-22 and SG-23, which were collected in the eastern portion of proposed Building B (south) and at least 450 ft east and topographically cross-gradient of proposed Building A (south). No TCE was detected in soil or groundwater samples collected from the southern portion of the Site. Based on this information, H&H considers Building A (south) to be in a separate exposure unit from Building B (south). Based on this information and the calculated non-residential HI of 0.015 for Building A (south), pre-occupancy and post-occupancy vapor monitoring is not warranted for Building A (south) but is warranted for Building B (south). Table 1 Summary of Soil Analytical DataPharr Yarns - LowellLowell, North CarolinaH&H Job No. HNY-001Evaluation AreaFormer Electrical SubstationFormer Carpentry ShopSample IDBG-1 BG-2 BG-3 SB-1 SB-2 SB-3 SB-5 SB-6 SB-7 SB-8 SB-9 SB-10 SB-11 SB-12 SB-13DateDepth (ft bgs)11-131-3Sample Type Range Mean TPH (EPA Method 8015C)Diesel Range Organics-- --100-- -- -- -- --4.4 J<3.5 NA NA NA NA NA <3.0 <3.1 <3.23.9 J<2.8 <2.7 NAGasoline Range Organics-- --50-- -- -- -- -- <1.8 <1.8 NA NA NA NA NA <1.4 <1.8 <1.8 <2.1 <1.4 <1.0 NAVOCs (8260D)Acetone14,000 210,000------------NANANANA <0.0018 <0.0013 <0.0012 NANANANANANA0.021Benzene1.25.4------------NANANANA <0.0011 <0.00078 <0.00076 NANANANANANA <0.00079Chloromethane2399------------NANANANA <0.0021 <0.0015 <0.0015 NANANANANANA <0.0015Ethylbenzene6.127------------NANANANA <0.0010 <0.00075 <0.00073 NANANANANANA <0.00076p-IsopropyltolueneNENE------------NANANANA <0.0017 <0.0013 <0.0012 NANANANANANA <0.0013Isopropylbenzene (Cumene)410 2,100------------NANANANA <0.00080 <0.00058 <0.00057 NANANANANANA <0.00059Naphthalene2.18.8------------NANANANA <0.00070 <0.00050 <0.00049 NANANANANANA <0.00051Tetrachloroethylene1782------------NANANANA0.0085 0.018 0.0015 JNANANANANANA <0.00092Toluene990 9,700------------NANANANA <0.0011 <0.00079 <0.00077 NANANANANANA <0.000811,2,4-Trimethylbenzene63370------------NANANANA <0.00073 <0.00053 <0.00052 NANANANANANA <0.00054m&p-Xylene120500------------NANANANA <0.0018 <0.0013 <0.0012 NANANANANANA <0.0013o-Xylene140590------------NANANANA <0.00073 <0.00053 <0.00052 NANANANANANA <0.00054Xylene (Total)120530------------NANANANA <0.0025 <0.0018 <0.0018 NANANANANANA <0.0018SVOCs (8270E)Acenaphthene720 9,000------------NANANA <0.020 NA0.064 J<0.020 NANANANANANA0.027 JAcenaphthyleneNENE------------NANANA <0.017 NA <0.017 <0.017 NANANANANANA <0.016Anthracene3,600 45,000------------NANANA <0.0097 NA0.18 J<0.0094 NANANANANANA0.097 JBenzo(a)anthracene1.121------------NANANA <0.011 NA0.67 J<0.010 NANANANANANA0.29 JBenzo(a)pyrene0.112.1------------NANANA <0.0079 NA0.68 J<0.0076 NANANANANANA0.25 JBenzo(b)fluoranthene1.121------------NANANA <0.0081 NA0.79 J<0.0079 NANANANANANA0.31 JBenzo(g,h,i)peryleneNENE------------NANANA <0.0087 NA0.37 J<0.0084 NANANANANANA0.14 JBenzo(k)fluoranthene11210------------NANANA <0.0093 NA0.25 J<0.0090 NANANANANANA0.10 JChrysene110 2,100------------NANANA <0.010 NA0.62 J<0.010 NANANANANANA0.26 JDibenzo(a,h)anthracene0.112.1------------NANANA <0.025 NA0.11 J<0.025 NANANANANANA0.038 JDibenzofuran16230------------NANANANANANANANANANANANANANAFluoranthene480 6,000------------NANANA<0.01 NA1.3<0.0097 NANANANANANA0.59 JFluorene480 6,000------------NANANA <0.015 NA0.062 J<0.015 NANANANANANA0.029 JIndeno(1,2,3-cd)pyrene1.121------------NANANA <0.025 NA0.42 J<0.024 NANANANANANA0.15 J1-Methylnaphthalene1873------------NANANA <0.013 NA0.092 J<0.013 NANANANANANA <0.0132-Methylnaphthalene48600------------NANANA <0.017 NA0.13 J<0.017 NANANANANANA <0.016Naphthalene2.18.8------------NANANA <0.019 NA0.099 J<0.018 NANANANANANA <0.018PhenanthreneNENE------------NANANA <0.0096 NA0.80 J<0.0093 NANANANANANA0.43 JPyrene360 4,500------------NANANA <0.013 NA1.1<0.012 NANANANANANA0.48 JPCBs (EPA Method 8082A)PCB-1016 (Aroclor 1016)0.8210------------NANA <0.0073 NANANANANANANANANANANAPCB-1221 (Aroclor 1221)0.20 0.84------------NANA <0.053 NANANANANANANANANANANAPCB-1232 (Aroclor 1232)0.18 0.73------------NANA <0.017 NANANANANANANANANANANAPCB-1242 (Aroclor 1242)0.23 0.95------------NANA <0.018 NANANANANANANANANANANAPCB-1248 (Aroclor 1248)0.23 0.94------------NANA <0.013 NANANANANANANANANANANAPCB-1254 (Aroclor 1254)0.23 0.97------------NANA <0.016 NANANANANANANANANANANAPCB-1254 (Aroclor 1260)0.24 0.99------------NANA <0.0084 NANANANANANANANANANANARCRA Metals (6020B/7471B/7199)Arsenic0.683.0--1.0 - 18 4.8 8.42 7.87 3.29NANANANANANANANANANANANANANABarium3,100 47,000--50 - 1,000 356 72.5 79.9 108NANANANANANANANANANANANANANACadmium 1.420--1.0 - 10 (4)4.3 (4)0.186 J<0.09890.452 JNA NA NA NA NA NA NA NA NA NA NA NA NA NAChromium (total) (6)NENE--7.0 - 300 6582.3 52.2 21.6NANANANANANANANANANANANANANAChromium, Hexavalent 0.316.5--NSNS<0.3030.527 J 0.380 JNANANANANANANANANANANANANANAChromium, Trivalent (7)23,000 350,000--NS NS 82.3 51.7 21.2NA NA NA NA NA NA NA NA NA NA NA NA NA NALead 400 800--ND - 50 1643.7 20.6 68.4NANANANANANANANANANANANANANAMercury4.770--0.03 - 0.52 0.121 0.236 0.0708 0.112NANANANANANANANANANANANANANASelenium78 1,200--<0.1 - 0.8 0.42 1.13 J 1.36 J 0.552 JNANANANANANANANANANANANANANASilver78 1,200--ND - 5.0 (5)NS<0.103 <0.100 <0.0952 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2023.2) Action Levels obtained from the NC DEQ Division of Waste Management (DWM) Underground Storage Tank (UST) Section Guidance for Site Checks, Tank Closure, and Initial Reponse and Abatement (May 2021).3) Range and mean values for regional background metals are published in Elements in North American Soils by Dragun and Chekiri dated 2005.4) North Carolina background levels are not specified; therefore, background values are reported for soils of the southeastern United States.5) North Carolina background levels are not specified; therefore, background values are reported for soils of the conterminous United States.6) Chromium PSRGs are not specified for total chromium. Refer to speciated chromium for PSRGs.7) Trivalent chromium concentrations were calculated by subtracting hexavalent chromium from total chromium concentrations.Bold values exceed the Residential PSRG. Underlined values exceed the Industrial/Commercial PSRGs. Metals detections that are generally consistent with published or site-specific background concentrations are not shown in bold.Compound concentrations are reported to the laboratory detection limits.With the exception of metals, only constituents detected in at least one sample are shown.Compound concentrations are reported in milligrams per kilogram (mg/kg)Laboratory analytical methods are shown in parentheses.VOCs = volatile organic compounds; SVOCs = semi-VOCs; RCRA = Resource Conservation and Recovery Act; TPH = total petroleum hydrocarbons; PCBs = polychlorinated biphenylsUST = underground storage tank; NS = not specified; NA = not analyzed; NE = not established; -- = not applicable; ND = non-detect; ft bgs = feet below ground surfaceJ = estimated concentration between the laboratory method detection limit and the laboratory reporting limit.GrabGrab10-12 1-3 3-5 10-121/11/2021Former Office Building UST LocationMill Building No. 1 Former Fuel Oil USTsIndustrial/ Commercial PSRGs (1)Screening CriteriaRegional Background Metals in Soil (3)Residential PSRGs (1)DEQ UST Section Action Levels (2)Former UST0-2GrabSite-Specific Background7/17/2023Mill Building No. 2 Former Fuel Oil USTsMill Building No. 1 Former Coal TrestleMill Building No. 1 Machine ShopSB-41/11/2021https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Henley Capital LLC (HNY)/HNY‐001 ‐ Lowell, NC ESA/EMP/Tables/Data Tables ‐ EMPTable 1 (Page 1 of 2)Hart & Hickman, PC Table 1 Summary of Soil Analytical DataPharr Yarns - LowellLowell, North CarolinaH&H Job No. HNY-001Evaluation AreaProposed Buidling A - NorthProposed Building C - NorthProposed Building A - SouthSample IDCS-1 CS-3 CS-4 CS-5 CS-6 CS-7DateDepth (ft bgs)Sample Type Range MeanTPH (EPA Method 8015C)Diesel Range Organics-- --100-- -- NA NA NA NA NA NA NA NAGasoline Range Organics-- --50-- -- NA NA NA NA NA NA NA NAVOCs (8260D)Acetone14,000 210,000------ <0.0382 <0.0452 <0.0443 <0.0498 <0.0465 <0.0505 <0.0539 <0.0492Benzene1.25.4------<0.0024 <0.0028 <0.0027 <0.0031 <0.0029 <0.0031 <0.00330.0044 JChloromethane2399--0.0055 J<0.0059 <0.0058 <0.00650.0061 J<0.0066 <0.00710.0070 JEthylbenzene6.127------ <0.0028 <0.0033 <0.00320.0154<0.0034 <0.0037 <0.00390.0159p-IsopropyltolueneNENE------ <0.0029 <0.0035 <0.00340.0039 J<0.0036 <0.0039 <0.0041 <0.0038Isopropylbenzene (Cumene)410 2,100------ <0.0020 <0.0024 <0.00230.0083<0.0025 <0.0027 <0.00290.0048 JNaphthalene2.18.8------0.111 0.0098 0.0063 J 0.13<0.00380.0054 J 0.0097 0.0472Tetrachloroethylene1782------ <0.0019 <0.0022 <0.0022 <0.0025 <0.0023 <0.0025 <0.0027 <0.0024Toluene990 9,700------0.0057 J<0.0049 <0.00480.0225<0.00500.0073 J 0.0059 J 0.02621,2,4-Trimethylbenzene63370------0.0039 J<0.0042 <0.00410.0289<0.0043 <0.0047 <0.00500.0193m&p-Xylene120500------0.0064 J<0.0048 <0.00470.0956<0.00500.0069 J<0.00570.0622o-Xylene140590------0.0032 J<0.0031 <0.00300.0648<0.0032 <0.0035 <0.00370.0424Xylene (Total)120530------0.0096 J<0.0040 <0.00390.16<0.00410.0069 J<0.00480.105SVOCs (8270E)720 9,000------2.05 0.246 J 0.174 J<0.153 <0.148 <0.143 <0.142 <0.140NENE------0.464<0.144<0.141 <0.153 <0.148 <0.143 <0.142 <0.1403,600 45,000------5.84 0.4850.408<0.142 <0.138 <0.133 <0.1320.295 J1.121------12.3 1.36 1.32<0.145 <0.141 <0.136 <0.1340.9010.112.1------9.141.21 1.15<0.150 <0.146 <0.140 <0.1390.741.121------13.2 1.68 1.52<0.145 <0.141 <0.136 <0.1341.01NENE------6.38 0.925 0.871<0.168 <0.164 <0.158 <0.1560.55611210------5.00 0.704 0.584<0.153 <0.148 <0.143 <0.1420.353 J110 2,100------12.6 1.53 1.42<0.158 <0.153 <0.148 <0.1460.9150.112.1------2.270.27 J 0.256 J<0.167 <0.162 <0.157 <0.1550.15716230------1.75 0.192 J<0.145 <0.157 <0.152 <0.147 <0.145 <0.143480 6,000------24.1 2.98 2.64<0.149 <0.144 <0.1390.177 J 1.74480 6,000------2.42 0.194 J<0.141 <0.153 <0.148 <0.143 <0.142 <0.140Acenaphthene Acenaphthylene AnthraceneBenzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene ChryseneDibenz(a,h)anthracene Dibenzofuran Fluoranthene FluoreneIndeno(1,2,3-cd)pyrene1.121------5.630.829 0.757<0.171 <0.166 <0.160 <0.1590.4851-Methylnaphthalene1873------0.478<0.144 <0.141 <0.153 <0.148 <0.143 <0.142 <0.1402-Methylnaphthalene48600------0.683<0.164 <0.161 <0.174 <0.169 <0.163 <0.161 <0.159Naphthalene2.18.8------1.39<0.139 <0.137 <0.147 <0.143 <0.138 <0.137 <0.135PhenanthreneNENE------22.5 2.85 1.96<0.142 <0.138 <0.1330.258 J 1.17Pyrene360 4,500------20.5 2.63 2.49<0.176 <0.171 <0.165 <0.1641.58PCBs (EPA Method 8082A)PCB-1016 (Aroclor 1016)0.8210------NANANANANANANANAPCB-1221 (Aroclor 1221)0.20 0.84------NANANANANANANANAPCB-1232 (Aroclor 1232)0.18 0.73------NANANANANANANANAPCB-1242 (Aroclor 1242)0.23 0.95------NANANANANANANANAPCB-1248 (Aroclor 1248)0.23 0.94------NANANANANANANANAPCB-1254 (Aroclor 1254)0.23 0.97------NANANANANANANANAPCB-1254 (Aroclor 1260)0.24 0.99------NANANANANANANANARCRA Metals (6020B/7471B/7199)Arsenic0.683.0--1.0 - 18 4.88.65 6.01 11.8 6.766.87.09 7.32 9.14Barium3,100 47,000--50 - 1,000 356109 34.9 27.1 50.4 36.8 61.6 79.4 69.9Cadmium1.420--1.0 - 10 (4)4.3 (4)0.433 J 0.145 J 0.211 J<0.109 <0.112 <0.1050.127 J 0.170 JChromium (total) (6)NENE--7.0 - 300 6535.4 29.6 31.3 30.1 28.1 26.5 21.4 25.1Chromium, Hexavalent 0.316.5--NSNS 0.512 J 0.969 J 1.44 1.34 0.922 J 0.936 J 0.648 J 0.953 JChromium, Trivalent (7)23,000 350,000--NS NS 34.9 28.6 29.9 28.8 27.2 25.6 20.8 24.1Lead 400 800--ND - 50 1652.0 22.1 11.8 16.1 11.2 33.1 39.3 45.4Mercury4.770--0.03 - 0.52 0.121 0.0815 0.0251 J 0.0698 0.0273 J 0.120 0.119 0.124 0.113Selenium78 1,200--<0.1 - 0.8 0.42 1.40 J 1.07 J 2.14 J 1.23 J 1.57 J 1.17 J 1.24 J 1.21 JSilver78 1,200--ND - 5.0 (5)NS<0.101 <0.104 <0.109 <0.111 <0.113 <0.106 <0.108 <0.101 Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2023.2) Action Levels obtained from the NC DEQ Division of Waste Management (DWM) Underground Storage Tank (UST) Section Guidance for Site Checks, Tank Closure, and Initial Reponse and Abatement (May 2021).3) Range and mean values for regional background metals are published in Elements in North American Soils by Dragun and Chekiri dated 2005.4) North Carolina background levels are not specified; therefore, background values are reported for soils of the southeastern United States.5) North Carolina background levels are not specified; therefore, background values are reported for soils of the conterminous United States.6) Chromium PSRGs are not specified for total chromium. Refer to speciated chromium for PSRGs.7) Trivalent chromium concentrations were calculated by subtracting hexavalent chromium from total chromium concentrations.Bold values exceed the Residential PSRG. Underlined values exceed the Industrial/Commercial PSRGs. Metals detections that are generally consistent with published or site-specific background concentrations are not shown in bold.Compound concentrations are reported to the laboratory detection limits.With the exception of metals, only constituents detected in at least one sample are shown.Compound concentrations are reported in milligrams per kilogram (mg/kg)Laboratory analytical methods are shown in parentheses.VOCs = volatile organic compounds; SVOCs = semi-VOCs; RCRA = Resource Conservation and Recovery Act; TPH = total petroleum hydrocarbons; PCBs = polychlorinated biphenylsUST = underground storage tank; NS = not specified; NA = not analyzed; NE = not established; -- = not applicable; ND = non-detect; ft bgs = feet below ground surfaceJ = estimated concentration between the laboratory method detection limit and the laboratory reporting limit.Composite0-27/18/2023Regional Background Metals in Soil (3)Screening CriteriaResidential PSRGs (1)Industrial/ Commercial PSRGs (1)DEQ UST Section Action Levels (2)Proposed Building B - NorthProposed Building B - South7/19/2023CS-2/SB-DUPhttps://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Henley Capital LLC (HNY)/HNY‐001 ‐ Lowell, NC ESA/EMP/Tables/Data Tables ‐ EMPTable 1 (Page 2 of 2)Hart & Hickman, PC Table 2 Summary of Groundwater Analytical Data Pharr Yarns - LowellLowell, North CarolinaH&H Job No. HNY-001Evaluation AreaMill Building No. 2 Former Fuel Oil USTsMill Building No. 1 Former Coal Trestle/Downgradient of former Machine ShopMill Building No. 1 Former Fuel Oil USTsFormer Office Building UST Location Former USTFormer Carpentry ShopSample IDTMW-1TMW-2TMW-3TMW-4TMW-5TMW-6Sample DateVOCs (8260D)Acetone6,000 NE NE<0.31 <3.1 <0.31 <0.31 <0.31 <0.31Chloroform70 0.813.6<0.076 <0.76 <0.076 <0.076 <0.076 <0.076Chloromethane352220<0.079 <0.79 <0.079 <0.079 <0.079 <0.0791,2-Dichlorobenzene20 5302,200<0.076 <0.760.51<0.076 <0.076 <0.0762-Hexanone40 1,6006,900<0.065 <0.65 <0.065 <0.065 <0.065 <0.065Methylene Chloride5 7604,000<0.083 <0.83 <0.083 <0.083 <0.083 <0.083Methyl tert-butyl ether (MTBE)20 4502,000<0.042 <0.42 <0.042 <0.042 <0.042 <0.042Naphthalene64.620 3.0<3.0 <0.30 <0.30 <0.30 <0.30Tetrachloroethylene0.7 1248<0.0982,100 6.6 5.6<0.0980.70Toluene600 3,80016,000<0.044 <0.44 <0.044 <0.044 <0.044 <0.044Trichloroethylene314.4<0.0787.9<0.078 <0.078 <0.078 <0.078Trichlorofluoromethane2,000 NENE<0.062 <0.62 <0.062 <0.062 <0.062 <0.0621,2,4-Trimethylbenzene400 502100.84<0.54 <0.054 <0.054 <0.054 <0.0541,3,5-Trimethylbenzene400 351500.22 J<0.76 <0.076 <0.076 <0.076 <0.076m,p-Xylene500 71 3000.30 J<1.2 <0.12 <0.12 <0.12 <0.12Xylene (total)500 773200.30 J<1.5 <0.15 <0.15 <0.15 <0.15SVOCs (8270E)Benzoic Acid30,000NENENANANANANANADiethyl Phthalate6,000NENENANANANANANANaphthalene64.6201.6 J<1.3<2.7<1.3<1.3<1.4RCRA Metals (6020B/7470A)Arsenic10NENENANANANANANABarium700NENENANANANANANACadmium2NENENANANANANANAChromium (Total)10NENENANANANANANALead15NENENANANANANANAMercury10.180.75NANANANANANASelenium20NENENANANANANANASilver20NENENANANANANANANotes:1)North Carolina Department of Environmental Quality (NCDEQ or DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) or Interim Maximum Allowable Concentrations (IMACs), dated April 2022.2)DEQ Department of Waste Management (DWM) Residential and Non Residential Vapor Intrusion Ground Water Screening Levels (GWSLs), TCR=1E-6; THQ=0.2, dated July 2023.Bold values exceed the DEQ 2L Standard.Underlined values exceed the Residential GWSL.Bold and Underlined concentrations exceed the 2L Standard and Residential GWSL.Compound concentrations are reported to the laboratory detection limits.Concentrations are reported in micrograms per liter (µg/L).Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown.VOCs = volatile organic compounds; SVOCs = semi-VOCs; RCRA = Resource Conservation and Recovery Act;J = estimated concentration between the laboratory method detection limit and the laboratory reporting limitNE = not established; NA = not analyzed; TCR = target cancer risk; THQ = target hazard quotient; UST = underground storage tankBold and Highlighted values exceed the 2L Standard and Non-Residential GWSL.Screening Criteria 2L Standards (1) Residential GWSLs (2)Non-Residential GWSLs (2)1/12/2021https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Henley Capital LLC (HNY)/HNY‐001 ‐ Lowell, NC ESA/EMP/Tables/Data Tables ‐ EMP9/7/2023Table 2 (Page 1 of 2)Hart & Hickman, PC Table 3 Summary of Groundwater Analytical DataPharr Yarns - LowellLowell, North CarolinaH&H Job No. HNY-001Evaluation AreaProposed Building A - NorthProposed Building B - NorthProposed Building A - SouthProposed Building B - SouthSample IDTMW-8 TMW-9 TMW-10 TMW-11 TMW-12Sample Date7/21/2023 7/20/2023VOCs (8260D)Acetone6,000 NE NE<12.8 <12.8 <5.1 <5.18.3 J<5.1 <5.1Chloroform70 0.813.6<1.1 <1.10.51 J<0.43 <0.431.6<0.43Chloromethane352220<1.4 <1.40.74 J43.40.80 J57.61.61,2-Dichlorobenzene20 5302,200<0.85 <0.85 <0.34 <0.34 <0.34 <0.34 <0.342-Hexanone40 1,6006,900<1.2 <1.2 <0.480.55 J0.59 J<0.48<0.48Methylene Chloride57604,000<4.95.3 J<2.0<2.0<2.0<2.0<2.0Methyl tert-butyl ether (MTBE) 204502,000<1.1<1.1<0.42<0.42<0.424.0<0.42Naphthalene64.620<1.6<1.6<0.64<0.64<0.64<0.64<0.64Tetrachloroethylene0.7124830732771.8<0.29<0.29<0.29<0.29Toluene6003,80016,000<0.60<0.60<0.24<0.24<0.24<0.24<0.24Trichloroethylene314.4<0.961.1 J6.1<0.38 <0.38 <0.38 <0.38Trichlorofluoromethane2,000 NENE<0.74 <0.742.8<0.30 <0.30 <0.30 <0.301,2,4-Trimethylbenzene400 50210NA NA NA NA NA NA NA1,3,5-Trimethylbenzene400 35150NA NA NA NA NA NA NAm,p-Xylene500 71 300<1.8 <1.8 <0.71 <0.71 <0.71 <0.71 <0.71Xylene (total)500 77320<0.84 <0.84 <0.34 <0.34 <0.34 <0.34 <0.34SVOCs (8270E)Benzoic Acid30,000NENE41.2 J22.0 J47.3 J46.0 J<22.0<20.041.3 JDiethyl Phthalate6,000NENE<1.8<1.8<2.03.8 J5.1 J<1.9<1.7Naphthalene64.620<1.8<1.8<2.1<2.1<2.1<1.9<1.7RCRA Metals (6020B/7470A)Arsenic10NENE0.74 J0.79 J0.17 J0.28 J0.29 J0.17 J0.18 JBarium700NENE53.346.761.112780.512819.0Cadmium2NENE0.370.380.080 J0.10 J0.067 J0.085 J0.060 JChromium (Total)10NENE0.62 J0.71 J<0.500.61 J0.69 J0.94 J0.92 JLead15NENE<0.0770.079 J<0.0770.091 J<0.077<0.0770.25 JMercury10.180.75<0.12<0.12<0.12<0.12<0.12<0.12<0.12Selenium20NENE2.22.20.86 J2.40.28 J<0.072<0.072Silver20NENE<0.070<0.070<0.070<0.070<0.070<0.070<0.070Notes:1) North Carolina Department of Environmental Quality (NCDEQ or DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) or Interim Maximum Allowable Concentrations (IMACs), dated April 2022.2) DEQ Department of Waste Management (DWM) Residential and Non Residential Vapor Intrusion Ground Water Screening Levels (GWSLs), TCR=1E-6; THQ=0.2, dated July 2023.Bold values exceed the DEQ 2L Standard.Underlined values exceed the Residential GWSL.Bold and Underlined concentrations exceed the 2L Standard and Residential GWSL.Bold and Highlighted values exceed the 2L Standard and Non-Residential GWSL.Compound concentrations are reported to the laboratory detection limits.Concentrations are reported in micrograms per liter (µg/L). Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown.VOCs = volatile organic compounds; SVOCs = semi-VOCs; RCRA = Resource Conservation and Recovery Act; J = estimated concentration between the laboratory method detection limit and the laboratory reporting limitNE = not established; NA = not analyzed; TCR = target cancer risk; THQ = target hazard quotient; UST = underground storage tank7/20/2023TMW-7/TMW-DUPNorthern Site Boundary2L Standards (1) Residential GWSLs (2) Non-Residential GWSLs (2)Screening Criteria https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Henley Capital LLC (HNY)/HNY‐001 ‐ Lowell, NC ESA/EMP/Tables/Data Tables ‐ EMP9/7/2023Table 3 (Page 2 of 2)Hart & Hickman, PC Table 3Summary of Well Construction and Depth to Groundwater Data Pharr Yarns - LowellLowell, North CarolinaH&H Job No. HNY-001Well IDDate of DTW MeasurementTotal Depth (ft bgs)Screen Interval (ft bgs)Ground Surface Elevation (ft)TOC Elevation (ft)Depth to Groundwater Below TOCGroundwater Elevation (ft)TMW-73015-3093.3793.2822.5170.77TMW-83015-3089.6089.3520.0069.35TMW-92510-25NMNM23.16NMTMW-103015-30105.31 104.9829.1275.86TMW-117/21/20233015-30NMNM23.20NMTMW-127/20/20233015-30NMNM21.88NMNotes:Top of casing (TOC)/ground surface elevations were surveyed by H&H relative to an arbitrary datum of 100 ft set at an on-site benchmark.ft bgs = feet below ground surface; DTW = depth to water; NM = not measured due to the presence of dense vegetation7/20/2023https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Henley Capital LLC (HNY)/HNY-001 - Lowell, NC ESA/Brownfields Assessment/Tables/Data Tables (08-18-23) DJH QC9/6/2023Table 3 (Page 1 of 1)Hart & Hickman, PC Table 4Summary of Exterior Soil Gas Analytical DataPharr Yarns - LowellLowell, North CarolinaH&H Job No. HNY-001Evaluation AreaSample IDSG-1 SG-2 SG-3 SG-4 SG-5 SG-6 SG-7 SG-8 SG-9 SG-10 SG-11 SG-12 SG-13 SG-14 SG-15 SG-16 SG-17 SG-18 SG-20 SG-21 SG-22 SG-23Sample DateVOCs (TO-15)AcetoneNENE15.4 58.0 25.053.237.1 23.1 34.9 51.8 54.7 30.4 17.2 28.8 30.7 17.8 18.9 18.0 14.6 13.3 30.4 J 28.5 J 19.1 28.8 1,570 21.0Benzene121607.0938.3 14.7 30.6 20.27.8615.9 31.7 53.7 77.3 27.8 25.7 28.9 68.46.0413.6 15.4 15.7 17.2 18.29.5834.5 54.6 J 30.4Bromodichloromethane2.533<0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.4711.39<0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <47.1 <0.4711,3-Butadiene3.141<0.230 <0.230 <0.230 <0.230 <0.230 <0.230 <0.230 <0.230 <0.230 <0.230 <0.230 <0.2301.88 J<0.230 <0.230 <0.230 <0.230 <0.230 <0.230 <0.230 <0.230 <0.230 <23.0 <0.230Carbon Disulfide4,90061,000 5.98 58.5 33.3 167 59.1<0.31734.2 77.8 183 208<0.317201<0.317166 6.44 17.1 13.8 30.2 28.7 30.0 25.0 129 43.4 J 54.2Carbon Tetrachloride16200<0.461 <0.461 <0.461 <0.461 <0.461 <0.4610.585 J<0.461 <0.461 <0.461 <0.461 <0.461 <0.4610.642 J<0.461 <0.461 <0.461 <0.461 <0.461 <0.461 <0.4610.584 J<46.1 <0.461Chlorobenzene3504,400<0.385 <0.385 <0.385 <0.385 <0.385 <0.385 <0.3850.568 J<0.385 <0.385 <0.385 <0.385 <0.385 <0.385 <0.385 <0.385 <0.385 <0.385 <0.385 <0.385 <0.385 <0.385 <38.5 <0.385Chloroethane28,000 350,000<0.263 <0.263 <0.263 <0.2630.353 J<0.2630.327 J 0.353 J 0.351 J 0.372 J 0.372 J 0.514 J<0.2630.493 J<0.263 <0.263 <0.263 <0.263 <0.263 <0.263 <0.263 <0.263 <26.3 <0.263Chloroform4.1532.64 1.5916.1<0.3499.59 9.931.336.91 11.0 31.8 4.744.0819.7 43.0 17.1 9.10 37.3 22.6<0.349 <0.3490.579 J<0.349 <34.9 <0.349Chloromethane6307,900 1.35 0.314 J 0.547 1.04 1.18 0.795 1.68 0.717 0.872 0.568 0.483 0.671 0.500 0.341 J<0.2130.374 J 0.628<0.213 <0.213 <0.2132.01 5.87<21.30.921Cyclohexane42,000 530,000 1.18 18.9 6.20 59.2 10.8 3.58 11.2 16.5 54.4 38.6 23.3 23.7 17.9 27.2 1.35 10.9 6.99 14.7<0.259 <0.2593.65<0.25980.2<0.259Dichlorodifluoromethane7008,800 0.989 J 1.96 1.58 2.07 1.59 1.06 2.00 1.86 1.90 1.84 1.58 2.64 1.85<0.6781.29 1.77 1.70 1.71<0.678 <0.6781.22 2.71<67.82.431,1-Dichloroethane58770<0.290 <0.2900.291 J<0.290 <0.2900.323 J<0.2900.513 J<0.290 <0.290 <0.290 <0.290 <0.290 <0.290 <0.290 <0.290 <0.290 <0.290 <0.290 <0.290 <0.290 <0.290 <29.0 <0.2901,1-Dichloroethene1,40018,000<0.302 <0.302 <0.302 <0.302 <0.302 <0.302 <0.302 <0.302 <0.302 <0.302 <0.302 <0.302 <0.302 <0.302 <0.3020.472 J<0.302 <0.302 <0.302 <0.302 <0.302 <0.302 <30.2 <0.302cis-1,2-Dichloroethene2803,500<0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.311 <0.3110.749 J<31.1 <0.311trans-1,2-Dichloroethene2803,500<0.2671.32<0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.267 <0.2670.307 J<0.267 <26.7 <0.267EthanolNENE27.5 26.8 42.8 79.2 99.9 32.4 25.3 32.1 76.9 74.3 23.9 70.0 33.9 15.0 36.6 21.9 69.8 53.5 27.0 JB 57.7 27.7 108 2,920 76.2Ethyl acetate4906,100<0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.360 <0.3601.62<36.01.01Ethylbenzene374906.50 27.3 12.8 35.2 18.4 6.55<0.36221.143.8 72.024.8 25.3 27.768.123.6 13.8 20.0 9.06 22.9 25.2 B 21.1 36.663.3 J32.24-EthyltolueneNENE1.29 3.80 2.38 5.06 5.20 1.70 2.46 3.21 7.21 11.4 3.95 3.71 4.09 12.7 6.18 2.19 4.45 1.31<0.384 <0.3844.08 5.20<38.45.45n-Heptane2,80035,000 9.86 198 52.8 274 87.9 31.2 56.4 113 275 386 344 355 252 182 13.2 83.4 90.0 141 99.4 95.3 63.0 203 285 163n-Hexane4,90061,000 2.93 76.5 16.6 93.1 36.0 7.97 23.1 98.0 106 145 104 94.8 70.9 36.7 2.49 38.8 22.8 45.5<0.72612.0 J 7.54 62.4 4,340 58.22-Hexanone2102,600<0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <0.544 <54.44.54 JIsopropylbenzene (Cumene)2,80035,000 1.44 4.76 2.32 7.18 7.82 4.43 1.21 2.50 14.9 10.1 5.01 5.41 5,41 9.14 3.80 4.02 3.89 3.26<0.382 <0.3823.55<0.382 <38.2 <0.382Isopropyl Alcohol (2-Propanol)1,40018,000 6.10 5.75 5.53 16.5 18.5 5.51 5.41<0.6499.29 9.86 4.52 17.1 5.46 4.50 5.48 2.88 J 7.52 6.10<0.64910.7 J 6.83 19.332,400 E10.12-Butanone (MEK)35,000 440,000 3.39 J 14.7 4.84 10.5 5.93 3.98 4.42 7.55 10.5 4.04 2.82 J<0.2406.72 3.39 J 2.95 J 5.51 2.36 J 2.77 J 9.61 J 4.84 J 7.73 6.61 174 J 5.284-Methyl-2-pentanone (MIBK)21,000 260,000<0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313226 J<0.313Methylene Chloride3,400 53,000 0.712 1.08<0.3408.65 3.14<0.3401.14 1.51 1.50 1.38<0.3402.97 1.73 0.990 1.21 0.833 4.13 3.58<0.340 <0.3400.819 3.24 270 1.78Methyl methacrylate4,900 61,000<0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359 <0.359647<0.359Naphthalene2.8 36<1.832.37 J<1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <1.83 <183 <1.83Propylene21,000 260,000<0.1609.68 1.84 J 115 14.6<0.16016.1 84.2 52.0 55.8 27.4 53.0 22.0 7.06<0.1605.06 1.83 J<0.160 <0.160 <0.160 <0.16029.6<16.012.3Styrene7,000 88,000<0.3350.766 J 0.570 J 1.15 1.56 0.966 0.506 J 1.82 2.18 1.24 0.944 1.15 0.863 0.659 J 0.424 J 0.519 J 0.425 J 1.33<0.335 <0.3350.966<0.33569.8 J 7.53Tetrachloroethene280 3,500 97.8 277 143 267 111 88.9 94.4 227384 605273 226284 551109 99.1 139 151292 327208363 355243Tetrahydrofuran14,000 180,000 0.455 J 1.52<0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <0.216 <21.6 <0.216Toluene35,000 440,000 67.1 246 123 277 148 67.4 112 182 372 505 209 213 241 512 127 113 142 98.7 217 225 149 268 433 2161,1,1-Trichloroethane35,000 440,000<0.400 <0.400 <0.400 <0.400 <0.4001.51<0.400 <0.400 <0.400 <0.400 <0.400 <0.400 <0.400 <0.400 <0.4001.82<0.400 <0.400 <0.400 <0.400 <0.4000.480 J<40.0 <0.400Trichloroethene14 180<0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.364 <0.36427.8<36.42.75TrichlorofluoromethaneNE NE 32.5 10.6 120 127 34.1 26.1 2.03 487 10.7 2.23 9.33 2.17 3.43 1.57 1.35 1.43 1.48 51.4<0.460 <0.4601.29 7.14<46.07.471,1,2-Trichlorotrifluoroethane35,000 440,000<0.608 <0.608 <0.608 <0.608 <0.6081200<0.608 <0.608 <0.608 <0.6081200<0.608600<0.608 <0.608 <0.608 <0.608 <0.608 <0.608 <0.608 <0.6081.02 J<60.80.742 J1,2,4-Trimethylbenzene4205,300 4.31 11.29.1817.7 17.9 6.82 8.83 11.6 26.8 30.0 10.7 11.8 11.6 35.4 26.3 7.71 13.1 4.15<0.37513.8 12.1 22.7 86.4 J 20.91,3,5-Trimethylbenzene4205,300 1.48 3.21 2.97 6.38 5.25 1.63 2.44 3.96 7.75 9.96 3.50 3.71 3.79 12.4 7.71 2.52 4.50 1.40<0.3823.90 J 3.29 6.38<38.27.412,2,4-TrimethylpentaneNENE4.09 134 40.6 157 64.9 19.3 51.4 94.8 221 307 221 212 168 64.5 5.56 60.7 56.5 81.3 41.9 39.7 26.2 122 144 99.5Vinyl acetate1,40018,000<0.408 <0.408 <0.408 <0.408 <0.4088.13<0.40874.3<0.408 <0.408 <0.408 <0.408 <0.408 <0.408 <0.408 <0.408 <0.408 <0.408 <0.408 <0.408 <0.408 <0.408 <40.8 <0.408o-Xylene7008,800 7.98 25.7 14.0 31.1 19.3 8.06 12.4 22.3 47.3 61.6 22.1 20.0 25.5 65.0 27.6 13.0 18.9 8.89 24.5 23.3 20.4 34.1 76.3 J 30.9m&p-Xylene7008,800 20.6 70.7 38.6 95.4 55.9 20.3 34.6 65.5 124 194 68.5 65.0 75.4 188 72.0 37.8 56.8 25.4 61.6 73.7 58.1 104 215 93.2DEQ Cumulative Risk Calculations Residential LICRResidential Non-Carcinogenic HINon-Residential LICR Non-Residential Non-Carcinogenic HI Notes:1) North Carolina Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Sub-Slab & Exterior Soil Gas Screening Levels (SGSLs), TCR = 1E-6; THQ=0.2, dated July 2023. Bold values exceed the Residential SGSL or acceptable risk level.Bold and underlined values exceed the Non-Residential SGSL.Compound concentrations are reported to the laboratory method detection limits.Only constituents detected in at least one sample are shown.Compound concentrations are reported in micrograms per cubic meter (μg/m3).Laboratory analytical methods are shown in parentheses.VOCs = volatile organic compounds; LICR = lifetime incremental cancer risk; HI = hazard index; THQ = target cancer risk; THQ = target hazard quotient; NE = not establishedJ = estimated concentration between the laboratory method detection limit and the laboratory reporting limitB = analyte was detected in the associated method blankE = analyte concentration exceeded the laboratory calibration range. The reported result is estimated.0.461.1 x 10-65.81.5 x 10-50.0159.2 x 10 -70.181.2 x 10-5SG-19/SG-DUP7/20/20237/20/20237/21/2023Screening CriteriaResidential SGSLs (1)Non-Residential SGSLs (1)Proposed Building A - SouthProposed Building B - SouthProposed Building A - NorthProposed Building B - NorthProposed Building C - North9.7x10-60.357.4x10-70.0280.0537.7x10-70.661.0x10-50.0521.5 x 10-60.652.0 x 10-5<1.0 x 10-4<1.0Acceptable Risk Levels<1.0 x 10-4<1.0https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Henley Capital LLC (HNY)/HNY‐001 ‐ Lowell, NC ESA/Brownfields Assessment/Tables/Data Tables (08‐18‐23) DJH QC9/7/2023Table 4 (Page 1 of 1)Hart & Hickman, PC REVISION NO. 0 JOB NO. HNY-001 DATE: 9-8-23 FIGURE NO. 2 PHARR YARNS - LOWELL700 WEST 1ST STREET LOWELL, NORTH CAROLINA SITE MAP LEGEND BROWNFIELDS BOUNDARYPROPERTY PARCEL BOUNDARY RAILROAD HISTORIC BUILDING FOOTPRINT PROPOSED BUILDING FOOTPRINT FORMER UNDERGROUNDSTORAGE TANK LOCATION VENT PIPE POLE-MOUNTED TRANSFORMER 2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology WE S T 1 S T S T R E E TNORTH CLAY STREETBIRCH STREETP O T T S S T R E E T NOTES: 1. PARCEL DATA OBTAINED FROM GASTON COUNTY GISDEPARTMENT, 2022. 2. AERIAL IMAGERY OBTAINED FROM ESRI GIS SERVICES,2019. RESIDENTIAL RESIDENTIAL FORMER TOWNOF LOWELLWATER TOWER FORMER OFFICEBUILDING NON-POTABLEWATER SUPPLY WELL FORMER DUKEPOWER SUB-STATION FORMERWASTE HOUSE MILL BUILDINGNO. 2 MILL BUILDINGNO. 1 COTTONWAREHOUSE COTTONWAREHOUSE HIGHWAY 7 COOL JUNK(607 WEST 1ST STREET) MULTI-TENANT COMMERCIAL(510 WEST 1ST STREET) LOWELL CHURCH OF GOD(800 WEST 1ST STREET) FORMERWATERRESERVOIR RAI L R O A D S T R E E T ASH STREETPHILLIPS STREETFORMER MACHINE SHOP FORMER CARPENTER SHOP FORMERRESIDENTIALPROPERTIES FORMERRESIDENTIAL PROPERTIES FORMER STORES BUILDING B BUILDING CBUILDING A BUILDING B RESIDENTIAL FORMERMACHINESHOP FORMER COALTRESTLEBUILDING A S:\AAA-Master Projects\Henley Capital LLC (HNY)\HNY-001 - Lowell, NC ESA\Brownfields Assessment\Figures\HNY.001-5 20230908.dwg, FIG 2, 9/15/2023 6:25:43 AM, shaynes SB-12/TMW-5 SB-9 SB-10/TMW-4 SB-8/TMW-3 SB-6 SB-5 SB-4/TMW-2 SB-2 SB-3 SB-13/TMW-6 SB-1/TMW-1 SB-7 SB-11 REVISION NO. 0 JOB NO. HNY-001 DATE: 9-11-23 FIGURE NO. 3 PHARR YARNS - LOWELL700 WEST 1ST STREET LOWELL, NORTH CAROLINA SAMPLE LOCATION MAP LEGEND BROWNFIELDS PROPERTYBOUNDARY PARCEL BOUNDARY RAILROAD PROPOSED BUILDING FOOTPRINT FORMER UNDERGROUNDSTORAGE TANK LOCATION (UST) VENT PIPE POLE-MOUNTED TRANSFORMER TEMPORARY MONITORING WELLLOCATION BACKGROUND SOIL BORINGLOCATION CO-LOCATED TEMPORARYMONITORING WELL AND SOILBORING LOCATION CO-LOCATED SOIL BORING ANDSOIL GAS SAMPLE LOCATION SOIL BORING SAMPLE LOCATION 2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology WE S T 1 S T S T R E E TNORTH CLAY STREETP O T T S S T R E E T NOTES: 1. PARCEL DATA OBTAINED FROM GASTON COUNTY GISDEPARTMENT, 2022.2. AERIAL IMAGERY OBTAINED FROM ESRI GIS SERVICES, 2019.3. PROPOSED REDEVELOPMENT PLAN BASED ON SITE PLAN PREPARED BY DESIGN RESOURCE GROUPDATED APRIL 21, 2022. 4. GROUNDWATER SAMPLES TMW-1 THROUGH TMW-6COLLECTED BY H&H IN JANUARY 2021.GROUNDWATER SAMPLES TMW-7 THROUGH TMW-12COLLECTED BY H&H ON JULY 20 & 21, 2023.5. SOIL SAMPLES SB-1 THROUGH SB-13 COLLECTED BYH&H IN JANUARY 2021. SOIL SAMPLES CS-1 THROUGHCS-7 AND BG-1 THROUGH BG-3 COLLECTED BY H&HBETWEEN JULY 17 AND 19, 2023.6. SOIL GAS SAMPLES SG-1 THROUGH SG-23 COLLECTEDBY H&H ON JULY 20 AND 21, 2023. RESIDENTIAL RESIDENTIAL HIGHWAY 7 COOL JUNK(607 WEST 1ST STREET) LOWELL CHURCH OF GOD(800 WEST 1ST STREET) RAI L R O A D S T R E E T ASH STREETPHILLIPS STREETCS-2 CS-3 CS-3C /SG-10 CS-3B /SG-9 CS-3A /SG-8 CS-2A /SG-5 CS-2B /SG-6 CS-2C /SG-7 CS-1C /SG-3 CS-1A /SG-1 CS-1B /SG-2 CS-1D /SG-4CS-1 CS-4A /SG-11 CS-4B /SG-12 CS-4D / SG-14 CS-4C /SG-13 CS-4 CS-7C /SG-23 CS-7B /SG-22 CS-7A /SG-21 CS-6C /SG-20 CS-6B / SG-19 CS-6A /SG-18 CS-5A /SG-15 CS-5B /SG-16 CS-5C / SG-17 CS-5 CS-6 CS-7 BUILDING A BUILDING B BUILDING CBUILDING A BUILDING B TMW-7 TMW-8 TMW-11 TMW-12 TMW-10 TMW-9 RESIDENTIAL MULTI-TENANTCOMMERCIAL(510 WEST 1ST STREET)BIRCH STREETFORMER DUKEPOWER SUB-STATION FORMERMACHINESHOP FORMER COALTRESTLE BG-3 BG-2 BG-1 S:\AAA-Master Projects\Henley Capital LLC (HNY)\HNY-001 - Lowell, NC ESA\Brownfields Assessment\Figures\HNY.001-5 20230908.dwg, FIG 3, 9/15/2023 6:28:48 AM, shaynes SB-6 SB-5 SB-2 SB-3 SB-11 REVISION NO. 0 JOB NO. HNY-001 DATE: 8-25-23 FIGURE NO. 4 PHARR YARNS - LOWELL 700 WEST 1ST STREET LOWELL, NORTH CAROLINA SOIL IMPACTS ABOVE PSRGs LEGEND BROWNFIELDS PROPERTYBOUNDARY PARCEL BOUNDARY RAILROAD PROPOSED BUILDING FOOTPRINT FORMER UNDERGROUNDSTORAGE TANK LOCATION (UST) VENT PIPE POLE-MOUNTED TRANSFORMER BACKGROUND SOIL BORINGLOCATION SOIL BORING LOCATION 2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 GeologyWE S T 1 S T S T R E E TNORTH CLAY STREETP O T T S S T R E E T NOTES: 1. PARCEL DATA OBTAINED FROM GASTON COUNTY GIS DEPARTMENT, 2022.2. AERIAL IMAGERY OBTAINED FROM ESRI GIS SERVICES,2019.3.BOLD VALUES EXCEED THE RESIDENTIAL PSRG. BOLDAND UNDERLINED VALUES EXCEED THEINDUSTRIAL/COMMERCIAL PSRGs.4. mg/kg = MILLIGRAMS PER KILOGRAMFT = FEET5. J = LABORATORY ESTIMATED CONCENTRATION6. PSRG = PRELIMINARY SOIL REMEDIATION GOAL RESIDENTIAL RESIDENTIAL HIGHWAY 7 COOL JUNK(607 WEST 1ST STREET) MULTI-TENANT COMMERCIAL(510 WEST 1ST STREET) LOWELL CHURCH OF GOD(800 WEST 1ST STREET) R A I LRO AD S T R E E T ASH STREETPHILLIPS STREETBG-3 BG-2 BG-1 CS-3 CS-3C CS-3B CS-3A CS-2A CS-2B CS-2C CS-1C CS-1A CS-1B CS-1D CS-4A CS-4B CS-4D CS-4C CS-4 CS-7C CS-7B CS-7A CS-6C CS-6B CS-6A CS-5A CS-5B CS-5C CS-5 CS-6 CS-1 (0-2 FT)7/19/23 BENZO(A)ANTHRACENE 12.3 BENZO(A)PYRENE 9.14 BENZO(B)FLUORANTHENE 13.2 DIBENZO(A,H)ANTHRACENE 2.27 INDENO(1,2,3-CD)PYRENE 5.63 CONSTITUENT CONCENTRATION(mg/kg) SAMPLE ID & DATE CS-1 (0-2 FT)7/19/23 BENZO(A)ANTHRACENE 12.3 BENZO(A)PYRENE 9.14 BENZO(B)FLUORANTHENE 13.2 DIBENZO(A,H)ANTHRACENE 2.27 INDENO(1,2,3-CD)PYRENE 5.63 CS-1 CS-2/SB-DUP (0-2 FT)7/19/23 BENZO(A)ANTHRACENE 1.36; 1.32 BENZO(A)PYRENE 1.21; 1.15 BENZO(B)FLUORANTHENE 1.68; 1.52 DIBENZO(A,H)ANTHRACENE 0.27J; 0.256J CS-2 CS-7 (0-2 FT)7/18/23 BENZO(A)PYRENE 0.74 DIBENZO(A,H)ANTHRACENE 0.157 CS-7 COMPOUND RESIDENTIALPSRG INDUSTRIAL/COMMERCIALPSRG BENZO(A)ANTHRACENE 1.1 21 BENZO(A)PYRENE 0.11 2.1 BENZO(B)FLUORANTHENE 1.1 21 DIBENZO(A,H)ANTHRACENE 0.11 2.1 INDENO(1,2,3-CD)PYRENE 1.1 21 SB-1 SB-4 SB-8 SB-10 SB-12 SB-13 BUILDING A BUILDING B BUILDING CBUILDING A BUILDING B SB-9 SB-7 BIRCH STREETSB-5 (3-5 FT)1/11/21 BENZO(A)PYRENE 0.58J S:\AAA-Master Projects\Henley Capital LLC (HNY)\HNY-001 - Lowell, NC ESA\Brownfields Assessment\Figures\FIG5-6_20230829.dwg, FIG 4, 9/14/2023 12:56:39 PM, draburn REVISION NO. 0 JOB NO. HNY-001 DATE: 9-11-23 FIGURE NO. 5 PHARR YARNS - LOWELL 700 WEST 1ST STREET LOWELL, NORTH CAROLINA SHALLOW GROUNDWATER POTENTIOMETRIC SURFACE MAP LEGEND BROWNFIELDS PROPERTY BOUNDARY PARCEL BOUNDARY RAILROAD PROPOSED BUILDING FOOTPRINT TEMPORARY MONITORING WELL LOCATION GROUNDWATER ELEVATION (FT) GROUNDWATER ELEVATION CONTOUR (FT) INFERRED GROUNDWATER FLOW DIRECTION 2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 GeologyWE S T 1 S T S T R E E TNORTH CLAY STREETP O T T S S T R E E T NOTES: 1.PARCEL DATA OBTAINED FROM GASTON COUNTY GIS DEPARTMENT, 2022. 2.AERIAL IMAGERY OBTAINED FROM ESRI GIS SERVICES, 2019. 3.PROPOSED REDEVELOPMENT PLAN BASED ON SITE PLAN PREPARED BY DESIGN RESOURCE GROUP DATED APRIL 21, 2022. 4.GROUNDWATER ELEVATIONS ARE BASED ON DEPTH TO GROUNDWATER MEASUREMENTS ON JULY 20, 2023. 5.GROUNDWATER ELEVATION BASED ON ARBITRARY SITE DATUM. 6.TOP OF CASING ELEVATIONS WERE NOT SURVEYED FOR TEMPORARY WELLS TMW-1 THROUGH TMW-5, TMW-9, AND TMW-10 THROUGH TMW-12 DUE TO THE PRESENCE OF DENSE VEGETATION AND/OR LIMITED PHASE II ESA SCOPE. 7.NM = NOT MEASURED RESIDENTIAL RESIDENTIAL HIGHWAY 7 COOL JUNK(607 WEST 1ST STREET) MULTI-TENANT COMMERCIAL(510 WEST 1ST STREET) LOWELL CHURCH OF GOD(800 WEST 1ST STREET) R A I LRO AD S T R E E T ASH STREETPHILLIPS STREETTMW-8 TMW-7 TMW-10 TMW-9 TMW-12 TMW-11 70 (69.35)(69.35) (70.77) (75.86) 70 70 72 72 74 74 RESIDENTIAL TMW-1 TMW-2 TMW-3 TMW-4 TMW-5 TMW-6 BUILDING A BUILDING B BUILDING CBUILDING A BUILDING B NMNM NM NM NM NM NM NM NM BIRCH STREETS:\AAA-Master Projects\Henley Capital LLC (HNY)\HNY-001 - Lowell, NC ESA\Brownfields Assessment\Figures\Site Map.dwg, FIG 5, 9/14/2023 12:53:32 PM, draburn REVISION NO. 0 JOB NO. HNY-001 DATE: 9-11-23 FIGURE NO. 6 PHARR YARNS - LOWELL 700 WEST 1ST STREET LOWELL, NORTH CAROLINA GROUNDWATER IMPACTS ABOVE NC 2L STANDARDS LEGEND BROWNFIELDS PROPERTYBOUNDARY PARCEL BOUNDARY RAILROAD PROPOSED BUILDING FOOTPRINT TEMPORARY MONITORING WELLLOCATION 2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 GeologyWE S T 1 S T S T R E E TNORTH CLAY STREETBIRCH STREETP O T T S S T R E E T NOTES: 1. PARCEL DATA OBTAINED FROM GASTON COUNTY GISDEPARTMENT, 2022.2. AERIAL IMAGERY OBTAINED FROM ESRI GISSERVICES, 2019.3.BOLD VALUES EXCEED THE 2L STANDARDS OR IMACs.4. μg/L = MICROGRAMS PER LITER5. J FLAG INDICATES AN ESTIMATED CONCENTRATIONBETWEEN THE LABORATORY METHOD DETECTIONLIMIT AND THE LABORATORY REPORTING LIMIT. RESIDENTIAL RESIDENTIAL HIGHWAY 7 COOL JUNK(607 WEST 1ST STREET) MULTI-TENANT COMMERCIAL(510 WEST 1ST STREET) LOWELL CHURCH OF GOD(800 WEST 1ST STREET) R A I LRO AD S T R E E T ASH STREETPHILLIPS STREETTMW-8 TMW-7 TMW-10 TMW-9 TMW-12 TMW-11 TMW-5 TMW-4 TMW-3TMW-2 TMW-6 TMW-1 TMW-2 1/12/21 TETRACHLOROETHYLENE 2,100 TRICHLOROETHYLENE 7.9CONSTITUENT CONCENTRATION (µg/L) SAMPLE ID & DATE COMPOUND NC 2L STANDARD CHLOROMETHANE 3 METHYLENE CHLORIDE 5 TETRACHLOROETHYLENE 0.7 TRICHLOROETHYLENE 3 TMW-2 1/12/21 TETRACHLOROETHYLENE 2,100 TRICHLOROETHYLENE 7.9 TMW-3 1/12/21 TETRACHLOROETHYLENE 6.6 TMW-4 1/12/21 TETRACHLOROETHYLENE 5.6 TMW-7/TMW-DUP 7/20/23 METHYLENE CHLORIDE <4.9; 5.3 J TETRACHLOROETHYLENE 307; 327 TMW-8 7/20/23 ETRACHLOROETHYLENE 71.8 TRICHLOROETHYLENE 6.1 TMW-9 7/20/23 CHLOROMETHANE 43.4 TMW-11 7/21/23 CHLOROMETHANE 57.6 BUILDING A BUILDING B BUILDING C BUILDING A BUILDING B BIRCH STREETS:\AAA-Master Projects\Henley Capital LLC (HNY)\HNY-001 - Lowell, NC ESA\Brownfields Assessment\Figures\FIG5-6_20230829.dwg, FIG 6, 9/14/2023 12:57:09 PM, draburn REVISION NO. 0 JOB NO. HNY-001 DATE: 9-11-23 FIGURE NO. 7 PHARR YARNS - LOWELL 700 WEST 1ST STREET LOWELL, NORTH CAROLINA SUMMARY OF VAPOR INTRUSION RISK LEGEND SITE PROPERTY BOUNDARY PARCEL BOUNDARY RAILROAD PROPOSED BUILDING FOOTPRINT 2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 GeologyWE S T 1 S T S T R E E TNORTH CLAY STREETBIRCH STREETP O T T S S T R E E T NOTES: 1. PARCEL DATA OBTAINED FROM GASTON COUNTY GISDEPARTMENT, 2022. 2. AERIAL IMAGERY OBTAINED FROM ESRI GISSERVICES, 2019. 3. VAPOR INTRUSION RISK CALCULATED USING THE DEQRISK CALCULATOR (JULY 2023 VERSION). 4. LICR = LIFETIME INCREMENTAL CANCER RISK; HI =HAZARD INDEX. 5. THE DEQ ACCEPTABLE LICR IS 1.0 X 10 -4 OR LESS, ANDTHE DEQ ACCEPTABLE HI IS 1.0 OR LESS. BOLDVALUES EXCEED THE DEQ ACCEPTABLE RISK LEVEL. RESIDENTIAL RESIDENTIAL HIGHWAY 7 COOL JUNK(607 WEST 1ST STREET) MULTI-TENANT COMMERCIAL(510 WEST 1ST STREET) LOWELL CHURCH OF GOD(800 WEST 1ST STREET) R A I LRO AD S T R E E T ASH STREETPHILLIPS STREETBUILDING A - SOUTH LICR (WORST-CASE RESIDENTIAL)1.2x10-5 NON-CARCINOGENIC HI (WORST-CASE RESIDENTIAL)0.18 LICR (WORST-CASE NON-RESIDENTIAL)9.2x10-7 NON-CARCINOGENIC HI (WORST-CASE NON-RESIDENTIAL)0.015 BUILDING B - SOUTH LICR (WORST-CASE RESIDENTIAL)1.5x10-5 NON-CARCINOGENIC HI (WORST-CASE RESIDENTIAL)5.8 LICR (WORST-CASE NON-RESIDENTIAL)1.1x10-6 NON-CARCINOGENIC HI (WORST-CASE NON-RESIDENTIAL)0.46 BUILDING A - NORTH LICR (WORST-CASE RESIDENTIAL)9.7x10-6 NON-CARCINOGENIC HI (WORST-CASE RESIDENTIAL)0.35 LICR (WORST-CASE NON-RESIDENTIAL)7.4x10-7 NON-CARCINOGENIC HI (WORST-CASE NON-RESIDENTIAL)0.028 BUILDING B - NORTH LICR (WORST-CASE RESIDENTIAL)1.0x10-5 NON-CARCINOGENIC HI (WORST-CASE RESIDENTIAL)0.66 LICR (WORST-CASE NON-RESIDENTIAL)7.7x10-7 NON-CARCINOGENIC HI (WORST-CASE NON-RESIDENTIAL)0.053 BUILDING C - NORTH LICR (WORST-CASE RESIDENTIAL)2.0x10-5 NON-CARCINOGENIC HI (WORST-CASE RESIDENTIAL)0.65 LICR (WORST-CASE NON-RESIDENTIAL)1.5x10-6 NON-CARCINOGENIC HI (WORST-CASE NON-RESIDENTIAL)0.052 S:\AAA-Master Projects\Henley Capital LLC (HNY)\HNY-001 - Lowell, NC ESA\Brownfields Assessment\Figures\FIG5-6_20230829.dwg, FIG 7, 9/14/2023 12:57:42 PM, draburn Appendix A Boring Logs NOTES: SVOC grab sample for CS-1 (0-2) taken from CS-1A (0-2). generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC SOIL GAS LOG Well No. Page: CS-1A (SG-1) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/19/2023 7/19/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR GR GR (0') SILT (ML); few coarse gravel, soft, dry, light brown (1') Lean CLAY (CL); few coarse gravel, some silt, stiff, dry, light brown/ light orange/dark orange (2') Lean CLAY (CL); few coarse gravel, some silt, stiff, moist, light orange, few mica (5.5') Boring terminated 8.0 8.9 5.4 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC SOIL GAS LOG Well No. Page: CS-1B (SG-2) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/19/2023 7/19/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') SILT (ML); soft, dry, tan (1') Lean CLAY (CL); few coarse gravel, some silt, soft, dry, orange (4') Lean CLAY (CL); some silt, soft, moist, light orange (5.5') Boring terminated 7.7 10.6 5.7 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC SOIL GAS LOG Well No. Page: CS-1C (SG-3) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/19/2023 7/19/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') Lean CLAY (CL); some silt, soft, dry, light brown, some mica (2') Lean CLAY (CL); some silt, soft, moist, light orange, some mica (3') Lean CLAY (CL); some silt, stiff, moist, light orange, some mica (4') Lean CLAY (CL); some silt, soft, moist, light brown (5.5') Boring terminated 4.4 5.9 9.9 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC SOIL GAS LOG Well No. Page: CS-1D (SG-4) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/19/2023 7/19/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') ORGANIC SOIL (OL); few fine-coarse gravel, brick debris (0.5') SILT (ML); some medium sand, little clay, soft, moist, brown/red (2') Lean CLAY (CL); some silt, stiff, moist, brown/red (4') Quartz layer (4.5') Lean CLAY (CL); some silt, stiff, moist, brown/red 6.1 7.1 5.0 0 5 10 5.5 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC SOIL GAS LOG Well No. Page: CS-2A (SG-5) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/19/2023 7/19/2023 IET Hand Auger Hand Auger TR White DJH Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') ORGANIC SOIL (OL); asphalt and brick debris (0.5') SILT (ML); some fine-coarse gravel, medium stiff, moist, light brown/white (1') SILT (ML); some clay, medium stiff, moist, brown/red/yellow (5.5') Boring terminated 2.4 5.5 4.6 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC SOIL GAS LOG Well No. Page: CS-2B (SG-6) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/19/2023 7/19/2023 IET Hand Auger Hand Auger TR White DJH Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') ORGANIC SOIL (OL) (0.5') Lean CLAY (CL); some silt, medium stiff, moist, brown/red (4') SILT (ML); little clay, medium stiff, moist, brown/red/white (5.5') Boring terminated 2.6 3.7 3.0 0 5 10 NOTES: VOC grab sample for CS-2 (0-2) taken from CS-2C (0-2). generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC SOIL GAS LOG Well No. Page: CS-2C (SG-7) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/19/2023 7/19/2023 IET Hand Auger Hand Auger TR White DJH Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') ORGANIC SOIL (OL); little fine-coarse gravel (0.5') Lean CLAY (CL); some fine-coarse gravel, little medium sand, some silt, very stiff, moist, brown/red (1.5') Lean CLAY (CL); some silt, stiff, moist, brown/red (5.5') Boring terminated 7.6 8.2 8.1 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC SOIL GAS LOG Well No. Page: CS-3A (SG-8) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/19/2023 7/19/2023 IET Direct Push AMS Power Probe 9520 TR White DJH Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') ORGANIC SOIL (OL); little fine-coarse gravel, brick debris (0.5') SILT (ML); some fine-coarse gravel, some clay, stiff, moist, brown (1') SILT (ML); some clay, stiff, moist, brown/red/yellow (4') As Above: trace sand and gravel (5.5') Boring terminated 5.6 5.0 3.9 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC SOIL GAS LOG Well No. Page: CS-3B (SG-9) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/19/2023 7/19/2023 IET Hand Auger Hand Auger TR White DJH Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') ORGANIC SOIL (OL); some coarse gravel, asphalt debris (0.5') Lean CLAY (CL); some silt, medium stiff, moist, brown/red, asphalt debris (2') Lean CLAY (CL); some silt, stiff, moist, brown/red (5.5') Boring terminated 4.0 4.7 5.6 0 5 10 NOTES: VOC grab sample for CS-3 (0-2) taken from CS-3C (0-2). generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC SOIL GAS LOG Well No. Page: CS-3C (SG-10) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/19/2023 7/19/2023 IET Hand Auger Hand Auger TR White DJH Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') ORGANIC SOIL (OL); some fine-coarse gravel (0.5') SILT (ML); some fine-coarse gravel, some medium sand, stiff, moist, light brown/pink (1') Lean CLAY (CL); some silt, stiff, moist, brown/red (5.5') Boring terminated 6.4 8.6 8.6 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC SOIL GAS LOG Well No. Page: CS-4A (SG-11) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/19/2023 7/19/2023 IET Hand Auger Hand Auger TR White DJH Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') ORGANIC SOIL (OL) (0.5') Lean CLAY (CL); some silt, stiff, moist, brown/light brown/red (2') As Above: brown/red (4.5') SILT (ML); some clay, medium stiff, moist, brown/red/yellow (5.5') Boring terminated 6.6 7.1 8.8 0 5 10 NOTES: VOC grab sample for CS-4 (0-2) taken from CS-4B (0-2). generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: CS-4B (SG-12) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/19/2023 07/19/2023 IET Hand Auger Hand Auger TR White DJH Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') ORGANIC SOIL (OL); some fine gravel (0.5') Lean CLAY (CL); few fine gravel, some silt, medium plasticity, stiff, moist, red brown (1') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, red brown/yellow (4') As Above: w/ gravel (5.5') Boring terminated 8.1 9.9 7.1 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: CS-4C (SG-13) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/19/2023 07/19/2023 IET Hand Auger Hand Auger TR White DJH Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') ORGANIC SOIL (OL) (0.5') Lean CLAY (CL); some silt, medium plasticity, very stiff, moist, red brown (5.5') Boring terminated 4.5 3.7 5.5 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: CS-4D (SG-14) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/19/2023 07/19/2023 IET Hand Auger Hand Auger TR White DJH Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') ORGANIC SOIL (OL); few fine gravel (0.5') SILT (ML); some clay, medium stiff, moist, red brown (4') SILT (ML); few fine sand, some clay, medium stiff, moist, red brown/brown/light brown (5.5') Boring terminated 5.4 3.2 2.6 0 5 10 NOTES: SG-15 installed at 0935. generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: CS-5A (SG-15) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/18/2023 07/18/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') Lean CLAY (CL); medium plasticity, soft, dry, orange (2') Lean CLAY (CL); few silt, medium plasticity, soft, moist, orange/grey, w/ few rock (4') As Above: but no rock (5.5') Boring terminated 3.7 4.6 4.6 0 5 10 NOTES: VOC grab sample for CS-5 (0-2) taken from CS-5B (0-2). generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: CS-5B (SG-16) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/18/2023 07/18/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') Lean CLAY (CL); medium plasticity, soft, dry, orange (2') Lean CLAY (CL); few fine-coarse sand, medium plasticity, soft, moist, orange (5.5') Boring terminated 5.0 5.4 5.8 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: CS-5C (SG-17) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/18/2023 07/18/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') Lean CLAY (CL); medium plasticity, soft, dry, red orange (2') Lean CLAY (CL); medium plasticity, medium stiff, moist, red orange (5.5') Boring terminated 4.5 4.1 3.3 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: CS-6A (SG-18) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/18/2023 07/18/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') SILT (ML); some clay, soft, dry, brown/orange (2') SILT (ML); some clay, soft, moist, orange (4') As Above: but light brown (5.5') Boring terminated 7.7 4.3 9.3 0 5 10 NOTES: VOC grab sample for CS-6 (0-2) taken from CS-6B (0-2). generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: CS-6B (SG-19) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/18/2023 07/18/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') Lean CLAY (CL); some silt, medium plasticity, stiff, dry, orange (2') As Above (4') As Above: but light orange (5.5') Boring terminated 49.8 13.1 13.4 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: CS-6C (SG-20) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/18/2023 07/18/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') SILT (ML); some clay, soft, moist, red orange (2') As Above (5.5') Boring terminated 5.1 4.5 5.7 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: SG-7A (SG-21) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/19/2023 07/19/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') SILT (ML); soft, dry, light brown, w/few rocks (1') Lean CLAY (CL); medium plasticity, soft, dry, orange/red orange (4') Lean CLAY (CL); few fine sand, medium plasticity, soft, dry, orange/red orange (5.5') Boring terminated 4.8 5.1 4.4 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: CS-7B (SG-22) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/19/2023 07/19/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') Lean CLAY (CL); few fine-coarse sand, medium plasticity, stiff, dry, red orange (4') Lean CLAY (CL); few fine-coarse sand, medium plasticity, soft, moist, light orange (5.5') Boring terminated 11.4 6.9 3.5 0 5 10 NOTES: VOC grab sample for CS-7 (0-2) taken from CS-7C (0-2). generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: CS-7C (SG-23) 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/19/2023 07/19/2023 IET Hand Auger Hand Auger Joe Tynan SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 5.5 3.25 Composite Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 5.5 0.25 0.600 Teflon Tubing Stainless Steel Wire Wrap Bent. Powder Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR (0') SILT (ML); few fine-coarse sand, soft, dry, light brown (3') As Above: w/ few rock (4') Lean CLAY (CL); medium plasticity, stiff, moist, orange (5.5') Boring terminated 18.4 9.7 3.3 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC BORING LOG Boring No. Page: BG-1 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/17/2023 07/17/2023 IET Hand Auger Hand Auger TR White SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 5.0 3.25 Grab DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR GR GR (0') ORGANIC SOIL (OL) (0.5') SILT (ML); soft, dry, orange/red (5') Boring terminated 1.5 0.4 0.4 0.3 0.3 BG-1(0-2) 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC BORING LOG Boring No. Page: BG-2 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/17/2023 07/17/2023 IET Hand Auger Hand Auger TR White SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 5.0 3.25 Grab DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR GR GR GR (0') SILT (ML); soft, dry, light brown (1') As Above: orange/red (5') Boring terminated 0.2 0.2 0.2 0.2 0.1 BG-2(0-2) 0 5 10 NOTES: generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC BORING LOG Boring No. Page: BG-3 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 07/17/2023 07/17/2023 IET Hand Auger Hand Auger TR White SMT Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 3.0 3.25 Grab DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 GR GR (0') SILT (ML); soft, dry, gray, gravel (1') SILT (ML); soft, dry, orange, gravel (3') Refusal 0.0 0.0 BG-3(0-2) 0 5 10 NOTES: Hand augered to 5' bgs. generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: TMW-7 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/17/23 7/17/23 IET Hollow Stem Auger AMS PowerProbe 9520 TR White Derek Haskell Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 30.0 8.00 DP, GR 22.51 Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 30.0 2.0 0.010 Sch 40 PVC PVC Prepack Bent. Chips Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 15 20 25 30 35 GR DP DP DP DP DP 5.00 5.00 5.00 5.00 5.00 5.00 (0') ORGANIC SOIL (OL) (0.5') Lean CLAY (CL); little coarse gravel, some silt, medium plasticity, medium stiff, moist, red-brown (5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, red-brown and yellow (9') Lean CLAY (CL); some fine-coarse sand, some silt, medium plasticity, medium stiff, moist, red-brown and yellow (10') SILT (ML); some clay, medium stiff, moist, red-brown and yellow (13') As Above: also black (18') SILT (ML); some clay, medium stiff, wet, light brown and black (19.5') As Above: some gravel (20') SILT (ML); trace fine-coarse sand, some clay, soft, wet, light brown and black (23') As Above: also red-brown (30') Boring terminated 1.1 2.2 3.5 4.7 5.0 4.7 5.3 4.6 4.7 6.4 6.3 4.2 0 5 10 15 20 25 30 35 NOTES: Hand augered to 5' bgs. generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: TMW-8 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/17/23 7/17/23 IET Hollow Stem Auger AMS PowerProbe 9520 TR White Derek Haskell Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 30.0 8.00 DP, GR 20.00 Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 30.0 2.0 0.010 Sch 40 PVC PVC Prepack Bent. Chips Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 15 20 25 30 35 GR DP DP DP DP DP 5.00 5.00 5.00 5.00 2.50 5.00 (0') ORGANIC SOIL (OL) (0.5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, red-brown (4') SILT (ML); some clay, medium stiff, moist, red-brown and yellow (9') As Above: also white (11') SILT (ML); little clay, medium stiff, moist, light red-brown/yellow/white/black (19') SILT (ML); medium stiff, moist, white/black/tan/pink, saprolite (22') As Above: wet (25') SILT (ML); some clay, soft, wet, white/black/tan/pink, saprolite (30') Boring terminated 3.4 4.7 4.5 3.0 3.9 3.9 3.4 3.6 3.0 4.4 4.3 2.0 0 5 10 15 20 25 30 35 NOTES: Hand augered to 5' bgs. generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: TMW-9 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/17/23 7/17/23 IET Hollow Stem Auger AMS PowerProbe 9520 TR White Derek Haskell Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 25.0 8.00 DP, GR 23.16 Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 25.0 2.0 0.010 Sch 40 PVC PVC Prepack Bent. Chips Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 15 20 25 30 GR DP DP DP DP 5.00 5.00 5.00 5.00 5.00 (0') ORGANIC SOIL (OL) (0.5') SILT (ML); some clay, medium stiff, moist, red-brown (4') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, red-brown (9') As Above: few gravel (13') Lean CLAY (CL); few fine-coarse gravel, some silt, medium plasticity, medium stiff, wet, red-brown/yellow/black (15') As Above: no gravel (25') Boring terminated 1.7 4.9 5.6 5.9 5.0 4.9 5.0 0.6 3.5 4.1 1.4 0 5 10 15 20 25 30 NOTES: Hand augered to 5' bgs. generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: TMW-10 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/18/23 7/18/23 IET Hollow Stem Auger AMS PowerProbe 9520 TR White Derek Haskell Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 30.0 8.00 DP, GR 29.12 Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 30.0 2.0 0.010 Sch 40 PVC PVC Prepack Bent. Chips Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 15 20 25 30 35 GR DP DP DP DP DP 5.00 5.00 5.00 2.00 5.00 5.00 (0') Asphalt (0.5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, red-brown and yellow (10') SILT (ML); few clay, medium stiff, moist, red-brown/yellow/white/black (14') As Above: some fine-coarse gravel (14.5') As Above: no gravel (18') SILT (ML); few clay, soft, moist, red-brown/yellow/white/black (20') White Rock (20.5') SILT (ML); little clay, soft, moist, red-brown/yellow/white/black (24') As Above: wet (30') Boring terminated 2.5 3.4 3.6 4.2 5.1 5.0 5.0 4.6 4.6 4.2 2.2 0.6 0 5 10 15 20 25 30 35 NOTES: Hand augered to 5' bgs. generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: TMW-11 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/18/23 7/18/23 IET Hollow Stem Auger AMS PowerProbe 9520 TR White Derek Haskell Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 30.0 8.00 DP, GR 23.20 Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 30.0 2.0 0.010 Sch 40 PVC PVC Prepack Bent. Chips Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 15 20 25 30 35 GR DP DP DP DP DP 5.00 3.00 5.00 5.00 5.00 5.00 (0') ORGANIC SOIL (OL) (0.5') SILT (ML); little fine-coarse gravel, medium stiff, moist, red-brown/black/brown (2') Silty SAND with gravel (SM); some fine-coarse gravel, loose, moist, brown and black (4') SILT (ML); some clay, medium stiff, moist, red-brown/yellow/white (7') SILT (ML); few clay, medium stiff, moist, light brown/pink/yellow/white/black (13') As Above: relic structures, saprolite (18') As Above: wet, no relic structures (30') Boring terminated 5.7 8.6 8.3 9.4 9.0 9.8 9.1 9.3 7.9 6.9 5.3 4.1 0 5 10 15 20 25 30 35 NOTES: Hand augered to 5' bgs. generated using GroundLogs.online Client: Project: Address: Lowell OZB, LLC HNY-001 700 West 1st Street, Lowell, NC WELL LOG Well No. Page: TMW-12 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 7/18/23 7/18/23 IET Hollow Stem Auger AMS PowerProbe 9520 TR White Derek Haskell Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Top of Casing Elev. (ft): Location (X,Y): 30.0 8.00 DP, GR 21.88 Well Depth (ft): Well Diameter (in): Screen Slot (in): Riser Material: Screen Material: Seal Material(s): Filter Pack: 30.0 2.0 0.010 Sch 40 PVC PVC Prepack Bent. Chips Sand Pack DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 15 20 25 30 35 GR DP DP DP DP DP 5.00 5.00 5.00 3.00 5.00 5.00 (0') ORGANIC SOIL (OL) (0.5') Lean CLAY (CL); little fine-coarse sand, some silt, medium plasticity, medium stiff, moist, red-brown/brown/tan (1') Lean CLAY (CL); trace fine-coarse gravel, some silt, medium plasticity, medium stiff, moist, red-brown (10') Lean CLAY (CL); trace fine-coarse sand, some silt, medium plasticity, medium stiff, moist, red-brown/yellow/black (14') SILT (ML); some clay, soft, wet, red-brown/yellow/black (18') SILT (ML); little clay, stiff, wet, red-brown/pink/yellow/white/black, saprolite (23') Sandy SILT (ML); medium stiff, moist, gray and white (23.5') SILT (ML); some clay, medium stiff, wet, red-brown/light brown/black/white, saprolite (30') Boring terminated 1.7 4.6 6.8 6.6 7.3 6.5 5.7 5.6 3.5 8.1 8.4 7.6 0 5 10 15 20 25 30 35 NOTES: BORING AND WELL LOG LEGEND LITHOLOGYWATER LEVELWELL/BORINGCOMPLETIONSample TypeDESCRIPTION GR EN SS SH CO DP ID ASPHALT CONCRETE BEDROCK IGNEOUS Rock METAMORPHIC Rock SEDIMENTARY Rock Well-graded GRAVEL (GW) Poorly graded GRAVEL (GP) Silty GRAVEL (GM) Clayey GRAVEL (GC) Well-graded GRAVEL with silt (GW-GM) Poorly graded GRAVEL with silt (GP-GM) Well-graded GRAVEL with clay (GW-GC) Poorly graded GRAVEL with clay (GP-GC) Well-graded SAND (SW) Poorly graded SAND (SP) Silty SAND (SM) Clayey SAND (SC) Well-graded SAND with silt (SW-SM) Poorly graded SAND with silt (SP-SM) Well-graded SAND with clay (SW-SC) Poorly graded SAND with clay (SP-SC) SILT (ML) Lean CLAY (CL) Organic SOIL (OL) Elastic SILT (MH) Fat CLAY (CH) Organic SOIL (OH) Organic SOIL (OL/OH) PEAT (PT) Volume Descriptors: Trace = <5% Few = 5-10% Little = 15-25% Some = 30-45% Mostly = >=50% Water Level During Drilling Water Level at End of Drilling/in Completed Well Cap Riser Screen End Plug Annular Seal (Bentonite-Cement Grout, Bentonite Slurry/Chips/Pellets/Powder, Other) Sanitary Seal (Bentonite Slurry/Chips/Pellets/Powder, Other) Filter Pack (Sand, Gravel, Other) Backfill Grab Encore Split Spoon Shelby Tube Core Barrel Direct Push Lab Sample and ID Appendix B Laboratory Analytical Reports #=CL# August 02, 2023 LIMS USE: FR - BO CAPPLEMAN LIMS OBJECT ID: 92678743 92678743 Project: Pace Project No.: RE: Bo Cappleman Hart & Hickman 2923 South Tryon Street Charlotte, NC 28203 HNY-001 Dear Bo Cappleman: Enclosed are the analytical results for sample(s) received by the laboratory on July 21, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor M Cannon taylor.cannon@pacelabs.com Project Manager (704)875-9092 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 147 #=CP# CERTIFICATIONS Pace Project No.: Project: 92678743 HNY-001 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: AI30792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TN003 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification #: CERT0086 Nebraska Certification #: NE-OS-15-05 Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TN002 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LAO00356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Mold Certification #: LAB0152 Texas Certification #: T 104704245-17-14 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A2LA 2926.01 A2LA-ISO 17025 Certification #: 1461.01 A2LA-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 147 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92678743 HNY-001 Lab ID Sample ID Matrix Date Collected Date Received 92678743001 BG-1 (0-2)Solid 07/17/23 13:30 07/21/23 16:37 92678743002 BG-2 (0-2)Solid 07/17/23 13:00 07/21/23 16:37 92678743003 BG-3 (0-2)Solid 07/17/23 12:30 07/21/23 16:37 92678743004 CS-1 (0-2)Solid 07/19/23 14:55 07/21/23 16:37 92678743005 CS-2 (0-2)Solid 07/19/23 12:05 07/21/23 16:37 92678743006 CS-3 (0-2)Solid 07/19/23 12:20 07/21/23 16:37 92678743007 CS-4 (0-2)Solid 07/19/23 14:35 07/21/23 16:37 92678743008 CS-5 (0-2)Solid 07/18/23 16:00 07/21/23 16:37 92678743009 CS-6 (0-2)Solid 07/18/23 12:00 07/21/23 16:37 92678743010 CS-7 (0-2)Solid 07/18/23 16:15 07/21/23 16:37 92678743011 TMW-7 Water 07/20/23 15:40 07/21/23 16:37 92678743012 TMW-8 Water 07/20/23 16:45 07/21/23 16:37 92678743013 TMW-9 Water 07/19/23 16:20 07/21/23 16:37 92678743014 TMW-10 Water 07/20/23 10:05 07/21/23 16:37 92678743015 TMW-11 Water 07/21/23 09:45 07/21/23 16:37 92678743016 TMW-12 Water 07/20/23 14:15 07/21/23 16:37 92678743017 TMW-DUP Water 07/20/23 00:00 07/21/23 16:37 92678743018 SB-DUP Solid 07/19/23 00:00 07/21/23 16:37 92678743019 TRIP BLANK Water 07/19/23 00:00 07/21/23 16:37 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 147 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92678743 HNY-001 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92678743001 BG-1 (0-2)EPA 6020B 7 PANLD EPA 7471B 1 PANNDL SM 2540G 1 PANCMK EPA 7199 1 PANSET 92678743002 BG-2 (0-2)EPA 6020B 7 PANLD EPA 7471B 1 PANNDL SM 2540G 1 PANCMK EPA 7199 1 PANSET 92678743003 BG-3 (0-2)EPA 6020B 7 PANLD EPA 7471B 1 PANNDL SM 2540G 1 PANCMK EPA 7199 1 PANSET 92678743004 CS-1 (0-2)EPA 6020B 7 PANLD EPA 7471B 1 PANNDL EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CSAS SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANSET 92678743005 CS-2 (0-2)EPA 6020B 7 PANLD EPA 7471B 1 PANNDL EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CSAS SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANSET 92678743006 CS-3 (0-2)EPA 6020B 7 PANLD EPA 7471B 1 PANNDL EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CSAS SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANSET 92678743007 CS-4 (0-2)EPA 6020B 7 PANLD EPA 7471B 1 PANNDL EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CSAS REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 147 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92678743 HNY-001 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANSET 92678743008 CS-5 (0-2)EPA 6020B 7 PANLD EPA 7471B 1 PANNDL EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CSAS SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANSET 92678743009 CS-6 (0-2)EPA 6020B 7 PANLD EPA 7471B 1 PANNDL EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CSAS SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANSET 92678743010 CS-7 (0-2)EPA 6020B 7 PANLD EPA 7471B 1 PANNDL EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CSAS SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANSET 92678743011 TMW-7 EPA 6020B 7 PASI-AKRL EPA 7470A 1 PASI-ANMP EPA 8270E 74 PASI-CPKS EPA 8260D 63 PASI-CJJK 92678743012 TMW-8 EPA 6020B 7 PASI-AKRL EPA 7470A 1 PASI-ANMP EPA 8270E 74 PASI-CPKS EPA 8260D 63 PASI-CJJK 92678743013 TMW-9 EPA 6020B 7 PASI-AKRL EPA 7470A 1 PASI-ANMP EPA 8270E 74 PASI-CPKS EPA 8260D 63 PASI-CJJK 92678743014 TMW-10 EPA 6020B 7 PASI-AKRL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 147 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92678743 HNY-001 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts EPA 7470A 1 PASI-ANMP EPA 8270E 74 PASI-CPKS EPA 8260D 63 PASI-CJJK 92678743015 TMW-11 EPA 6020B 7 PASI-AKRL EPA 7470A 1 PASI-ANMP EPA 8270E 74 PASI-CPKS EPA 8260D 63 PASI-CJJK 92678743016 TMW-12 EPA 6020B 7 PASI-AKRL EPA 7470A 1 PASI-ANMP EPA 8270E 74 PASI-CPKS EPA 8260D 63 PASI-CJJK 92678743017 TMW-DUP EPA 6020B 7 PASI-AKRL EPA 7470A 1 PASI-ANMP EPA 8270E 74 PASI-CPKS EPA 8260D 63 PASI-CJJK 92678743018 SB-DUP EPA 6020B 7 PANLD EPA 7471B 1 PANNDL EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CSAS SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANSET 92678743019 TRIP BLANK EPA 8260D 63 PASI-CTMH PAN = Pace National - Mt. Juliet PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: BG-1 (0-2)Lab ID: 92678743001 Collected: 07/17/23 13:30 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: 3050B Pace National - Mt. Juliet Metals (ICPMS) 6020B Arsenic 8.42 mg/kg 08/01/23 17:10 7440-38-207/27/23 03:221.19 0.119 5 Barium 72.5 mg/kg 08/01/23 17:10 7440-39-307/27/23 03:222.97 0.181 5 Cadmium 0.186J mg/kg 08/01/23 17:10 7440-43-9 J07/27/23 03:221.19 0.102 5 Chromium 82.3 mg/kg 08/01/23 17:10 7440-47-307/27/23 03:225.94 0.352 5 Lead 43.7 mg/kg 08/01/23 17:10 7439-92-107/27/23 03:222.38 0.118 5 Selenium 1.13J mg/kg 08/01/23 17:10 7782-49-2 J07/27/23 03:222.97 0.214 5 Silver ND mg/kg 08/01/23 17:10 7440-22-407/27/23 03:220.594 0.103 5 Analytical Method: EPA 7471B Preparation Method: 7471A Pace National - Mt. Juliet Mercury 7471B Mercury 0.236 mg/kg 07/30/23 18:17 7439-97-607/28/23 10:460.0475 0.0214 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 84.2 %07/27/23 12:4607/27/23 12:321 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent ND mg/kg 07/28/23 14:34 18540-29-907/28/23 10:001.19 0.303 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: BG-2 (0-2)Lab ID: 92678743002 Collected: 07/17/23 13:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: 3050B Pace National - Mt. Juliet Metals (ICPMS) 6020B Arsenic 7.87 mg/kg 08/01/23 17:13 7440-38-207/27/23 03:221.16 0.116 5 Barium 79.9 mg/kg 08/01/23 17:13 7440-39-307/27/23 03:222.89 0.176 5 Cadmium ND mg/kg 08/01/23 17:13 7440-43-907/27/23 03:221.16 0.0989 5 Chromium 52.2 mg/kg 08/01/23 17:13 7440-47-307/27/23 03:225.78 0.342 5 Lead 20.6 mg/kg 08/01/23 17:13 7439-92-107/27/23 03:222.31 0.114 5 Selenium 1.36J mg/kg 08/01/23 17:13 7782-49-2 J07/27/23 03:222.89 0.208 5 Silver ND mg/kg 08/01/23 17:13 7440-22-407/27/23 03:220.578 0.100 5 Analytical Method: EPA 7471B Preparation Method: 7471A Pace National - Mt. Juliet Mercury 7471B Mercury 0.0708 mg/kg 07/30/23 18:20 7439-97-607/28/23 10:460.0463 0.0208 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 86.5 %07/27/23 12:4607/27/23 12:321 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.527J mg/kg 07/28/23 14:55 18540-29-9 J07/28/23 10:001.16 0.295 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: BG-3 (0-2)Lab ID: 92678743003 Collected: 07/17/23 12:30 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: 3050B Pace National - Mt. Juliet Metals (ICPMS) 6020B Arsenic 3.29 mg/kg 08/01/23 17:17 7440-38-207/27/23 03:221.10 0.110 5 Barium 108 mg/kg 08/01/23 17:17 7440-39-307/27/23 03:222.75 0.167 5 Cadmium 0.452J mg/kg 08/01/23 17:17 7440-43-9 J07/27/23 03:221.10 0.0941 5 Chromium 21.6 mg/kg 08/01/23 17:17 7440-47-307/27/23 03:225.50 0.326 5 Lead 68.4 mg/kg 08/01/23 17:17 7439-92-107/27/23 03:222.20 0.109 5 Selenium 0.552J mg/kg 08/01/23 17:17 7782-49-2 J07/27/23 03:222.75 0.198 5 Silver ND mg/kg 08/01/23 17:17 7440-22-407/27/23 03:220.550 0.0952 5 Analytical Method: EPA 7471B Preparation Method: 7471A Pace National - Mt. Juliet Mercury 7471B Mercury 0.112 mg/kg 07/30/23 18:22 7439-97-607/28/23 10:460.0440 0.0198 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 90.9 %07/27/23 12:4607/27/23 12:321 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.380J mg/kg 07/28/23 15:00 18540-29-9 J07/28/23 10:001.10 0.281 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-1 (0-2)Lab ID: 92678743004 Collected: 07/19/23 14:55 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: 3050B Pace National - Mt. Juliet Metals (ICPMS) 6020B Arsenic 8.65 mg/kg 08/01/23 17:20 7440-38-207/27/23 03:221.17 0.117 5 Barium 109 mg/kg 08/01/23 17:49 7440-39-307/27/23 03:225.83 0.354 10 Cadmium 0.433J mg/kg 08/01/23 17:20 7440-43-9 J07/27/23 03:221.17 0.0997 5 Chromium 35.4 mg/kg 08/01/23 17:20 7440-47-307/27/23 03:225.83 0.345 5 Lead 52.0 mg/kg 08/01/23 17:20 7439-92-107/27/23 03:222.33 0.115 5 Selenium 1.40J mg/kg 08/01/23 17:20 7782-49-2 J07/27/23 03:222.91 0.210 5 Silver ND mg/kg 08/01/23 17:20 7440-22-407/27/23 03:220.583 0.101 5 Analytical Method: EPA 7471B Preparation Method: 7471A Pace National - Mt. Juliet Mercury 7471B Mercury 0.0815 mg/kg 07/30/23 18:25 7439-97-607/28/23 10:460.0466 0.0210 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene 2050 ug/kg 07/30/23 12:58 83-32-907/27/23 18:30392 138 1 Acenaphthylene 464 ug/kg 07/30/23 12:58 208-96-807/27/23 18:30392 138 1 Aniline ND ug/kg 07/30/23 12:58 62-53-307/27/23 18:30392 153 1 Anthracene 5840 ug/kg 07/31/23 09:44 120-12-707/27/23 18:303920 1280 10 Benzo(a)anthracene 12300 ug/kg 07/31/23 09:44 56-55-307/27/23 18:303920 1310 10 Benzo(a)pyrene 9140 ug/kg 07/31/23 09:44 50-32-807/27/23 18:303920 1360 10 Benzo(b)fluoranthene 13200 ug/kg 07/31/23 09:44 205-99-207/27/23 18:303920 1310 10 Benzo(g,h,i)perylene 6380 ug/kg 07/31/23 09:44 191-24-207/27/23 18:303920 1520 10 Benzo(k)fluoranthene 5000 ug/kg 07/31/23 09:44 207-08-907/27/23 18:303920 1380 10 Benzoic Acid ND ug/kg 07/30/23 12:58 65-85-007/27/23 18:301960 843 1 Benzyl alcohol ND ug/kg 07/30/23 12:58 100-51-607/27/23 18:30785 297 1 4-Bromophenylphenyl ether ND ug/kg 07/30/23 12:58 101-55-307/27/23 18:30392 151 1 Butylbenzylphthalate ND ug/kg 07/30/23 12:58 85-68-707/27/23 18:30392 165 1 4-Chloro-3-methylphenol ND ug/kg 07/30/23 12:58 59-50-707/27/23 18:30785 276 1 4-Chloroaniline ND ug/kg 07/30/23 12:58 106-47-807/27/23 18:30785 308 1 bis(2-Chloroethoxy)methane ND ug/kg 07/30/23 12:58 111-91-107/27/23 18:30392 163 1 bis(2-Chloroethyl) ether ND ug/kg 07/30/23 12:58 111-44-407/27/23 18:30392 147 1 2-Chloronaphthalene ND ug/kg 07/30/23 12:58 91-58-707/27/23 18:30392 156 1 2-Chlorophenol ND ug/kg 07/30/23 12:58 95-57-807/27/23 18:30392 147 1 4-Chlorophenylphenyl ether ND ug/kg 07/30/23 12:58 7005-72-307/27/23 18:30392 146 1 Chrysene 12600 ug/kg 07/31/23 09:44 218-01-907/27/23 18:303920 1430 10 Dibenz(a,h)anthracene 2270 ug/kg 07/30/23 12:58 53-70-307/27/23 18:30392 151 1 Dibenzofuran 1750 ug/kg 07/30/23 12:58 132-64-907/27/23 18:30392 142 1 1,2-Dichlorobenzene ND ug/kg 07/30/23 12:58 95-50-107/27/23 18:30392 142 1 1,3-Dichlorobenzene ND ug/kg 07/30/23 12:58 541-73-107/27/23 18:30392 139 1 1,4-Dichlorobenzene ND ug/kg 07/30/23 12:58 106-46-707/27/23 18:30392 150 1 3,3'-Dichlorobenzidine ND ug/kg 07/30/23 12:58 91-94-107/27/23 18:30785 265 1 2,4-Dichlorophenol ND ug/kg 07/30/23 12:58 120-83-207/27/23 18:30392 153 1 Diethylphthalate ND ug/kg 07/30/23 12:58 84-66-207/27/23 18:30392 144 1 2,4-Dimethylphenol ND ug/kg 07/30/23 12:58 105-67-9 v107/27/23 18:30392 163 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-1 (0-2)Lab ID: 92678743004 Collected: 07/19/23 14:55 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 07/30/23 12:58 131-11-307/27/23 18:30392 143 1 Di-n-butylphthalate ND ug/kg 07/30/23 12:58 84-74-207/27/23 18:30392 132 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/30/23 12:58 534-52-107/27/23 18:30785 366 1 2,4-Dinitrophenol ND ug/kg 07/30/23 12:58 51-28-507/27/23 18:301960 1210 1 2,4-Dinitrotoluene ND ug/kg 07/30/23 12:58 121-14-207/27/23 18:30392 151 1 2,6-Dinitrotoluene ND ug/kg 07/30/23 12:58 606-20-207/27/23 18:30392 144 1 Di-n-octylphthalate ND ug/kg 07/30/23 12:58 117-84-007/27/23 18:30392 155 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/30/23 12:58 117-81-707/27/23 18:30392 152 1 Fluoranthene 24100 ug/kg 07/31/23 09:44 206-44-007/27/23 18:303920 1340 10 Fluorene 2420 ug/kg 07/30/23 12:58 86-73-707/27/23 18:30392 138 1 Hexachloro-1,3-butadiene ND ug/kg 07/30/23 12:58 87-68-307/27/23 18:30392 170 1 Hexachlorobenzene ND ug/kg 07/30/23 12:58 118-74-107/27/23 18:30392 153 1 Hexachlorocyclopentadiene ND ug/kg 07/30/23 12:58 77-47-4 v207/27/23 18:30392 225 1 Hexachloroethane ND ug/kg 07/30/23 12:58 67-72-107/27/23 18:30392 150 1 Indeno(1,2,3-cd)pyrene 5630 ug/kg 07/31/23 09:44 193-39-507/27/23 18:303920 1550 10 Isophorone ND ug/kg 07/30/23 12:58 78-59-107/27/23 18:30392 175 1 1-Methylnaphthalene 478 ug/kg 07/30/23 12:58 90-12-007/27/23 18:30392 138 1 2-Methylnaphthalene 683 ug/kg 07/30/23 12:58 91-57-607/27/23 18:30392 157 1 2-Methylphenol(o-Cresol)ND ug/kg 07/30/23 12:58 95-48-707/27/23 18:30392 161 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/30/23 12:58 15831-10-407/27/23 18:30392 158 1 Naphthalene 1390 ug/kg 07/30/23 12:58 91-20-307/27/23 18:30392 133 1 2-Nitroaniline ND ug/kg 07/30/23 12:58 88-74-407/27/23 18:301960 321 1 3-Nitroaniline ND ug/kg 07/30/23 12:58 99-09-207/27/23 18:301960 308 1 4-Nitroaniline ND ug/kg 07/30/23 12:58 100-01-607/27/23 18:30785 299 1 Nitrobenzene ND ug/kg 07/30/23 12:58 98-95-307/27/23 18:30392 182 1 2-Nitrophenol ND ug/kg 07/30/23 12:58 88-75-507/27/23 18:30392 170 1 4-Nitrophenol ND ug/kg 07/30/23 12:58 100-02-7 v207/27/23 18:301960 759 1 N-Nitrosodimethylamine ND ug/kg 07/30/23 12:58 62-75-907/27/23 18:30392 132 1 N-Nitroso-di-n-propylamine ND ug/kg 07/30/23 12:58 621-64-707/27/23 18:30392 147 1 N-Nitrosodiphenylamine ND ug/kg 07/30/23 12:58 86-30-607/27/23 18:30392 139 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/30/23 12:58 108-60-107/27/23 18:30392 187 1 Pentachlorophenol ND ug/kg 07/30/23 12:58 87-86-5 v207/27/23 18:30785 384 1 Phenanthrene 22500 ug/kg 07/31/23 09:44 85-01-807/27/23 18:303920 1280 10 Phenol ND ug/kg 07/30/23 12:58 108-95-207/27/23 18:30392 175 1 Pyrene 20500 ug/kg 07/31/23 09:44 129-00-007/27/23 18:303920 1590 10 Pyridine ND ug/kg 07/30/23 12:58 110-86-107/27/23 18:30392 124 1 1,2,4-Trichlorobenzene ND ug/kg 07/30/23 12:58 120-82-107/27/23 18:30392 155 1 2,4,5-Trichlorophenol ND ug/kg 07/30/23 12:58 95-95-407/27/23 18:30392 180 1 2,4,6-Trichlorophenol ND ug/kg 07/30/23 12:58 88-06-207/27/23 18:30392 162 1 Surrogates Nitrobenzene-d5 (S)52 %07/30/23 12:58 4165-60-007/27/23 18:3010-130 1 2-Fluorobiphenyl (S)57 %07/30/23 12:58 321-60-807/27/23 18:3010-130 1 Terphenyl-d14 (S)55 %07/30/23 12:58 1718-51-007/27/23 18:3010-130 1 Phenol-d6 (S)46 %07/30/23 12:58 13127-88-307/27/23 18:3010-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-1 (0-2)Lab ID: 92678743004 Collected: 07/19/23 14:55 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)42 %07/30/23 12:58 367-12-407/27/23 18:3010-130 1 2,4,6-Tribromophenol (S)53 %07/30/23 12:58 118-79-607/27/23 18:3010-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 07/25/23 17:33 67-64-107/25/23 14:48119 38.2 1 Benzene ND ug/kg 07/25/23 17:33 71-43-207/25/23 14:486.0 2.4 1 Bromobenzene ND ug/kg 07/25/23 17:33 108-86-107/25/23 14:486.0 1.9 1 Bromochloromethane ND ug/kg 07/25/23 17:33 74-97-507/25/23 14:486.0 1.8 1 Bromodichloromethane ND ug/kg 07/25/23 17:33 75-27-407/25/23 14:486.0 2.3 1 Bromoform ND ug/kg 07/25/23 17:33 75-25-207/25/23 14:486.0 2.1 1 Bromomethane ND ug/kg 07/25/23 17:33 74-83-9 IH07/25/23 14:4823.8 18.4 1 2-Butanone (MEK)ND ug/kg 07/25/23 17:33 78-93-307/25/23 14:48119 28.6 1 n-Butylbenzene ND ug/kg 07/25/23 17:33 104-51-807/25/23 14:486.0 3.7 1 sec-Butylbenzene ND ug/kg 07/25/23 17:33 135-98-807/25/23 14:486.0 2.6 1 tert-Butylbenzene ND ug/kg 07/25/23 17:33 98-06-607/25/23 14:486.0 2.1 1 Carbon tetrachloride ND ug/kg 07/25/23 17:33 56-23-507/25/23 14:486.0 2.2 1 Chlorobenzene ND ug/kg 07/25/23 17:33 108-90-707/25/23 14:486.0 3.4 1 Chloroethane ND ug/kg 07/25/23 17:33 75-00-307/25/23 14:4811.9 4.6 1 Chloroform ND ug/kg 07/25/23 17:33 67-66-307/25/23 14:486.0 5.0 1 Chloromethane 5.5J ug/kg 07/25/23 17:33 74-87-307/25/23 14:4811.9 5.0 1 2-Chlorotoluene ND ug/kg 07/25/23 17:33 95-49-807/25/23 14:486.0 2.1 1 4-Chlorotoluene ND ug/kg 07/25/23 17:33 106-43-407/25/23 14:486.0 3.3 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/25/23 17:33 96-12-807/25/23 14:486.0 2.3 1 Dibromochloromethane ND ug/kg 07/25/23 17:33 124-48-107/25/23 14:486.0 3.3 1 1,2-Dibromoethane (EDB)ND ug/kg 07/25/23 17:33 106-93-407/25/23 14:486.0 2.6 1 Dibromomethane ND ug/kg 07/25/23 17:33 74-95-307/25/23 14:486.0 1.3 1 1,2-Dichlorobenzene ND ug/kg 07/25/23 17:33 95-50-107/25/23 14:486.0 2.1 1 1,3-Dichlorobenzene ND ug/kg 07/25/23 17:33 541-73-107/25/23 14:486.0 1.8 1 1,4-Dichlorobenzene ND ug/kg 07/25/23 17:33 106-46-707/25/23 14:486.0 1.5 1 Dichlorodifluoromethane ND ug/kg 07/25/23 17:33 75-71-807/25/23 14:4811.9 6.1 1 1,1-Dichloroethane ND ug/kg 07/25/23 17:33 75-34-307/25/23 14:486.0 2.5 1 1,2-Dichloroethane ND ug/kg 07/25/23 17:33 107-06-207/25/23 14:486.0 3.9 1 1,1-Dichloroethene ND ug/kg 07/25/23 17:33 75-35-407/25/23 14:486.0 2.5 1 cis-1,2-Dichloroethene ND ug/kg 07/25/23 17:33 156-59-207/25/23 14:486.0 2.0 1 trans-1,2-Dichloroethene ND ug/kg 07/25/23 17:33 156-60-507/25/23 14:486.0 5.1 1 1,2-Dichloropropane ND ug/kg 07/25/23 17:33 78-87-507/25/23 14:486.0 1.8 1 1,3-Dichloropropane ND ug/kg 07/25/23 17:33 142-28-907/25/23 14:486.0 1.9 1 2,2-Dichloropropane ND ug/kg 07/25/23 17:33 594-20-7 v207/25/23 14:486.0 4.5 1 1,1-Dichloropropene ND ug/kg 07/25/23 17:33 563-58-607/25/23 14:486.0 2.9 1 cis-1,3-Dichloropropene ND ug/kg 07/25/23 17:33 10061-01-507/25/23 14:486.0 1.6 1 trans-1,3-Dichloropropene ND ug/kg 07/25/23 17:33 10061-02-607/25/23 14:486.0 2.0 1 Diisopropyl ether ND ug/kg 07/25/23 17:33 108-20-307/25/23 14:486.0 1.6 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-1 (0-2)Lab ID: 92678743004 Collected: 07/19/23 14:55 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene ND ug/kg 07/25/23 17:33 100-41-407/25/23 14:486.0 2.8 1 Hexachloro-1,3-butadiene ND ug/kg 07/25/23 17:33 87-68-307/25/23 14:4811.9 9.7 1 2-Hexanone ND ug/kg 07/25/23 17:33 591-78-607/25/23 14:4859.5 5.7 1 Isopropylbenzene (Cumene)ND ug/kg 07/25/23 17:33 98-82-807/25/23 14:486.0 2.0 1 p-Isopropyltoluene ND ug/kg 07/25/23 17:33 99-87-607/25/23 14:486.0 2.9 1 Methylene Chloride ND ug/kg 07/25/23 17:33 75-09-207/25/23 14:4823.8 16.3 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/25/23 17:33 108-10-107/25/23 14:4859.5 5.7 1 Methyl-tert-butyl ether ND ug/kg 07/25/23 17:33 1634-04-4 v207/25/23 14:486.0 2.2 1 Naphthalene 111 ug/kg 07/25/23 17:33 91-20-307/25/23 14:486.0 3.1 1 n-Propylbenzene ND ug/kg 07/25/23 17:33 103-65-107/25/23 14:486.0 2.1 1 Styrene ND ug/kg 07/25/23 17:33 100-42-507/25/23 14:486.0 1.6 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/25/23 17:33 630-20-607/25/23 14:486.0 2.3 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/25/23 17:33 79-34-507/25/23 14:486.0 1.6 1 Tetrachloroethene ND ug/kg 07/25/23 17:33 127-18-407/25/23 14:486.0 1.9 1 Toluene 5.7J ug/kg 07/25/23 17:33 108-88-307/25/23 14:486.0 4.1 1 1,2,3-Trichlorobenzene ND ug/kg 07/25/23 17:33 87-61-607/25/23 14:486.0 4.8 1 1,2,4-Trichlorobenzene ND ug/kg 07/25/23 17:33 120-82-107/25/23 14:486.0 5.0 1 1,1,1-Trichloroethane ND ug/kg 07/25/23 17:33 71-55-607/25/23 14:486.0 3.1 1 1,1,2-Trichloroethane ND ug/kg 07/25/23 17:33 79-00-507/25/23 14:486.0 2.0 1 Trichloroethene ND ug/kg 07/25/23 17:33 79-01-607/25/23 14:486.0 4.8 1 Trichlorofluoromethane ND ug/kg 07/25/23 17:33 75-69-407/25/23 14:486.0 3.3 1 1,2,3-Trichloropropane ND ug/kg 07/25/23 17:33 96-18-407/25/23 14:486.0 3.0 1 1,2,4-Trimethylbenzene 3.9J ug/kg 07/25/23 17:33 95-63-607/25/23 14:486.0 3.5 1 1,3,5-Trimethylbenzene ND ug/kg 07/25/23 17:33 108-67-807/25/23 14:486.0 2.0 1 Vinyl acetate ND ug/kg 07/25/23 17:33 108-05-407/25/23 14:4859.5 12.2 1 Vinyl chloride ND ug/kg 07/25/23 17:33 75-01-4 v207/25/23 14:4811.9 3.0 1 Xylene (Total)9.6J ug/kg 07/25/23 17:33 1330-20-707/25/23 14:4811.9 3.4 1 m&p-Xylene 6.4J ug/kg 07/25/23 17:33 179601-23-107/25/23 14:4811.9 4.1 1 o-Xylene 3.2J ug/kg 07/25/23 17:33 95-47-607/25/23 14:486.0 2.6 1 Surrogates Toluene-d8 (S)101 %07/25/23 17:33 2037-26-507/25/23 14:4870-130 1 4-Bromofluorobenzene (S)101 %07/25/23 17:33 460-00-407/25/23 14:4870-130 1 1,2-Dichloroethane-d4 (S)106 %07/25/23 17:33 17060-07-007/25/23 14:4870-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 14.8 %07/24/23 14:06 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 85.8 %07/27/23 12:4607/27/23 12:321 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-1 (0-2)Lab ID: 92678743004 Collected: 07/19/23 14:55 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.512J mg/kg 07/28/23 15:06 18540-29-9 J07/28/23 10:001.17 0.297 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-2 (0-2)Lab ID: 92678743005 Collected: 07/19/23 12:05 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: 3050B Pace National - Mt. Juliet Metals (ICPMS) 6020B Arsenic 6.01 mg/kg 08/01/23 15:39 7440-38-207/27/23 03:221.20 0.120 5 Barium 34.9 mg/kg 08/01/23 15:39 7440-39-307/27/23 03:222.99 0.182 5 Cadmium 0.145J mg/kg 08/01/23 15:39 7440-43-9 J07/27/23 03:221.20 0.102 5 Chromium 29.6 mg/kg 08/01/23 15:39 7440-47-307/27/23 03:225.98 0.354 5 Lead 22.1 mg/kg 08/01/23 15:39 7439-92-107/27/23 03:222.39 0.119 5 Selenium 1.07J mg/kg 08/01/23 15:39 7782-49-2 J07/27/23 03:222.99 0.215 5 Silver ND mg/kg 08/01/23 15:39 7440-22-407/27/23 03:220.598 0.104 5 Analytical Method: EPA 7471B Preparation Method: 7471A Pace National - Mt. Juliet Mercury 7471B Mercury 0.0251J mg/kg 07/30/23 18:27 7439-97-6 J07/28/23 10:460.0479 0.0215 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene 246J ug/kg 07/30/23 12:31 83-32-907/27/23 18:30411 144 1 Acenaphthylene ND ug/kg 07/30/23 12:31 208-96-807/27/23 18:30411 144 1 Aniline ND ug/kg 07/30/23 12:31 62-53-307/27/23 18:30411 161 1 Anthracene 485 ug/kg 07/30/23 12:31 120-12-707/27/23 18:30411 134 1 Benzo(a)anthracene 1360 ug/kg 07/30/23 12:31 56-55-307/27/23 18:30411 137 1 Benzo(a)pyrene 1210 ug/kg 07/30/23 12:31 50-32-807/27/23 18:30411 142 1 Benzo(b)fluoranthene 1680 ug/kg 07/30/23 12:31 205-99-207/27/23 18:30411 137 1 Benzo(g,h,i)perylene 925 ug/kg 07/30/23 12:31 191-24-207/27/23 18:30411 159 1 Benzo(k)fluoranthene 704 ug/kg 07/30/23 12:31 207-08-907/27/23 18:30411 144 1 Benzoic Acid ND ug/kg 07/30/23 12:31 65-85-007/27/23 18:302050 882 1 Benzyl alcohol ND ug/kg 07/30/23 12:31 100-51-607/27/23 18:30821 311 1 4-Bromophenylphenyl ether ND ug/kg 07/30/23 12:31 101-55-307/27/23 18:30411 158 1 Butylbenzylphthalate ND ug/kg 07/30/23 12:31 85-68-707/27/23 18:30411 173 1 4-Chloro-3-methylphenol ND ug/kg 07/30/23 12:31 59-50-707/27/23 18:30821 289 1 4-Chloroaniline ND ug/kg 07/30/23 12:31 106-47-807/27/23 18:30821 322 1 bis(2-Chloroethoxy)methane ND ug/kg 07/30/23 12:31 111-91-107/27/23 18:30411 170 1 bis(2-Chloroethyl) ether ND ug/kg 07/30/23 12:31 111-44-407/27/23 18:30411 154 1 2-Chloronaphthalene ND ug/kg 07/30/23 12:31 91-58-707/27/23 18:30411 163 1 2-Chlorophenol ND ug/kg 07/30/23 12:31 95-57-807/27/23 18:30411 154 1 4-Chlorophenylphenyl ether ND ug/kg 07/30/23 12:31 7005-72-307/27/23 18:30411 153 1 Chrysene 1530 ug/kg 07/30/23 12:31 218-01-907/27/23 18:30411 149 1 Dibenz(a,h)anthracene 270J ug/kg 07/30/23 12:31 53-70-307/27/23 18:30411 158 1 Dibenzofuran 192J ug/kg 07/30/23 12:31 132-64-907/27/23 18:30411 148 1 1,2-Dichlorobenzene ND ug/kg 07/30/23 12:31 95-50-107/27/23 18:30411 148 1 1,3-Dichlorobenzene ND ug/kg 07/30/23 12:31 541-73-107/27/23 18:30411 146 1 1,4-Dichlorobenzene ND ug/kg 07/30/23 12:31 106-46-707/27/23 18:30411 157 1 3,3'-Dichlorobenzidine ND ug/kg 07/30/23 12:31 91-94-107/27/23 18:30821 278 1 2,4-Dichlorophenol ND ug/kg 07/30/23 12:31 120-83-207/27/23 18:30411 161 1 Diethylphthalate ND ug/kg 07/30/23 12:31 84-66-207/27/23 18:30411 151 1 2,4-Dimethylphenol ND ug/kg 07/30/23 12:31 105-67-9 v107/27/23 18:30411 170 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-2 (0-2)Lab ID: 92678743005 Collected: 07/19/23 12:05 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 07/30/23 12:31 131-11-307/27/23 18:30411 149 1 Di-n-butylphthalate ND ug/kg 07/30/23 12:31 84-74-207/27/23 18:30411 138 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/30/23 12:31 534-52-107/27/23 18:30821 383 1 2,4-Dinitrophenol ND ug/kg 07/30/23 12:31 51-28-507/27/23 18:302050 1270 1 2,4-Dinitrotoluene ND ug/kg 07/30/23 12:31 121-14-207/27/23 18:30411 158 1 2,6-Dinitrotoluene ND ug/kg 07/30/23 12:31 606-20-207/27/23 18:30411 151 1 Di-n-octylphthalate ND ug/kg 07/30/23 12:31 117-84-007/27/23 18:30411 162 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/30/23 12:31 117-81-707/27/23 18:30411 159 1 Fluoranthene 2980 ug/kg 07/30/23 12:31 206-44-007/27/23 18:30411 141 1 Fluorene 194J ug/kg 07/30/23 12:31 86-73-707/27/23 18:30411 144 1 Hexachloro-1,3-butadiene ND ug/kg 07/30/23 12:31 87-68-307/27/23 18:30411 178 1 Hexachlorobenzene ND ug/kg 07/30/23 12:31 118-74-107/27/23 18:30411 161 1 Hexachlorocyclopentadiene ND ug/kg 07/30/23 12:31 77-47-4 v207/27/23 18:30411 235 1 Hexachloroethane ND ug/kg 07/30/23 12:31 67-72-107/27/23 18:30411 157 1 Indeno(1,2,3-cd)pyrene 829 ug/kg 07/30/23 12:31 193-39-507/27/23 18:30411 162 1 Isophorone ND ug/kg 07/30/23 12:31 78-59-107/27/23 18:30411 183 1 1-Methylnaphthalene ND ug/kg 07/30/23 12:31 90-12-007/27/23 18:30411 144 1 2-Methylnaphthalene ND ug/kg 07/30/23 12:31 91-57-607/27/23 18:30411 164 1 2-Methylphenol(o-Cresol)ND ug/kg 07/30/23 12:31 95-48-707/27/23 18:30411 168 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/30/23 12:31 15831-10-407/27/23 18:30411 166 1 Naphthalene ND ug/kg 07/30/23 12:31 91-20-307/27/23 18:30411 139 1 2-Nitroaniline ND ug/kg 07/30/23 12:31 88-74-407/27/23 18:302050 336 1 3-Nitroaniline ND ug/kg 07/30/23 12:31 99-09-207/27/23 18:302050 322 1 4-Nitroaniline ND ug/kg 07/30/23 12:31 100-01-607/27/23 18:30821 312 1 Nitrobenzene ND ug/kg 07/30/23 12:31 98-95-307/27/23 18:30411 190 1 2-Nitrophenol ND ug/kg 07/30/23 12:31 88-75-507/27/23 18:30411 178 1 4-Nitrophenol ND ug/kg 07/30/23 12:31 100-02-7 v207/27/23 18:302050 794 1 N-Nitrosodimethylamine ND ug/kg 07/30/23 12:31 62-75-907/27/23 18:30411 138 1 N-Nitroso-di-n-propylamine ND ug/kg 07/30/23 12:31 621-64-707/27/23 18:30411 154 1 N-Nitrosodiphenylamine ND ug/kg 07/30/23 12:31 86-30-607/27/23 18:30411 146 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/30/23 12:31 108-60-107/27/23 18:30411 195 1 Pentachlorophenol ND ug/kg 07/30/23 12:31 87-86-5 v207/27/23 18:30821 402 1 Phenanthrene 2850 ug/kg 07/30/23 12:31 85-01-807/27/23 18:30411 134 1 Phenol ND ug/kg 07/30/23 12:31 108-95-207/27/23 18:30411 183 1 Pyrene 2630 ug/kg 07/30/23 12:31 129-00-007/27/23 18:30411 167 1 Pyridine ND ug/kg 07/30/23 12:31 110-86-107/27/23 18:30411 129 1 1,2,4-Trichlorobenzene ND ug/kg 07/30/23 12:31 120-82-107/27/23 18:30411 162 1 2,4,5-Trichlorophenol ND ug/kg 07/30/23 12:31 95-95-407/27/23 18:30411 188 1 2,4,6-Trichlorophenol ND ug/kg 07/30/23 12:31 88-06-207/27/23 18:30411 169 1 Surrogates Nitrobenzene-d5 (S)49 %07/30/23 12:31 4165-60-007/27/23 18:3010-130 1 2-Fluorobiphenyl (S)51 %07/30/23 12:31 321-60-807/27/23 18:3010-130 1 Terphenyl-d14 (S)50 %07/30/23 12:31 1718-51-007/27/23 18:3010-130 1 Phenol-d6 (S)43 %07/30/23 12:31 13127-88-307/27/23 18:3010-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-2 (0-2)Lab ID: 92678743005 Collected: 07/19/23 12:05 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)41 %07/30/23 12:31 367-12-407/27/23 18:3010-130 1 2,4,6-Tribromophenol (S)49 %07/30/23 12:31 118-79-607/27/23 18:3010-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 07/25/23 17:52 67-64-107/25/23 14:48141 45.2 1 Benzene ND ug/kg 07/25/23 17:52 71-43-207/25/23 14:487.0 2.8 1 Bromobenzene ND ug/kg 07/25/23 17:52 108-86-107/25/23 14:487.0 2.3 1 Bromochloromethane ND ug/kg 07/25/23 17:52 74-97-507/25/23 14:487.0 2.1 1 Bromodichloromethane ND ug/kg 07/25/23 17:52 75-27-407/25/23 14:487.0 2.7 1 Bromoform ND ug/kg 07/25/23 17:52 75-25-207/25/23 14:487.0 2.5 1 Bromomethane ND ug/kg 07/25/23 17:52 74-83-9 IH07/25/23 14:4828.2 21.8 1 2-Butanone (MEK)ND ug/kg 07/25/23 17:52 78-93-307/25/23 14:48141 33.8 1 n-Butylbenzene ND ug/kg 07/25/23 17:52 104-51-807/25/23 14:487.0 4.4 1 sec-Butylbenzene ND ug/kg 07/25/23 17:52 135-98-807/25/23 14:487.0 3.1 1 tert-Butylbenzene ND ug/kg 07/25/23 17:52 98-06-607/25/23 14:487.0 2.5 1 Carbon tetrachloride ND ug/kg 07/25/23 17:52 56-23-507/25/23 14:487.0 2.6 1 Chlorobenzene ND ug/kg 07/25/23 17:52 108-90-707/25/23 14:487.0 4.0 1 Chloroethane ND ug/kg 07/25/23 17:52 75-00-307/25/23 14:4814.1 5.4 1 Chloroform ND ug/kg 07/25/23 17:52 67-66-307/25/23 14:487.0 5.9 1 Chloromethane ND ug/kg 07/25/23 17:52 74-87-307/25/23 14:4814.1 5.9 1 2-Chlorotoluene ND ug/kg 07/25/23 17:52 95-49-807/25/23 14:487.0 2.5 1 4-Chlorotoluene ND ug/kg 07/25/23 17:52 106-43-407/25/23 14:487.0 3.9 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/25/23 17:52 96-12-807/25/23 14:487.0 2.7 1 Dibromochloromethane ND ug/kg 07/25/23 17:52 124-48-107/25/23 14:487.0 4.0 1 1,2-Dibromoethane (EDB)ND ug/kg 07/25/23 17:52 106-93-407/25/23 14:487.0 3.1 1 Dibromomethane ND ug/kg 07/25/23 17:52 74-95-307/25/23 14:487.0 1.5 1 1,2-Dichlorobenzene ND ug/kg 07/25/23 17:52 95-50-107/25/23 14:487.0 2.5 1 1,3-Dichlorobenzene ND ug/kg 07/25/23 17:52 541-73-107/25/23 14:487.0 2.2 1 1,4-Dichlorobenzene ND ug/kg 07/25/23 17:52 106-46-707/25/23 14:487.0 1.8 1 Dichlorodifluoromethane ND ug/kg 07/25/23 17:52 75-71-807/25/23 14:4814.1 7.2 1 1,1-Dichloroethane ND ug/kg 07/25/23 17:52 75-34-307/25/23 14:487.0 2.9 1 1,2-Dichloroethane ND ug/kg 07/25/23 17:52 107-06-207/25/23 14:487.0 4.7 1 1,1-Dichloroethene ND ug/kg 07/25/23 17:52 75-35-407/25/23 14:487.0 2.9 1 cis-1,2-Dichloroethene ND ug/kg 07/25/23 17:52 156-59-207/25/23 14:487.0 2.4 1 trans-1,2-Dichloroethene ND ug/kg 07/25/23 17:52 156-60-507/25/23 14:487.0 6.0 1 1,2-Dichloropropane ND ug/kg 07/25/23 17:52 78-87-507/25/23 14:487.0 2.1 1 1,3-Dichloropropane ND ug/kg 07/25/23 17:52 142-28-907/25/23 14:487.0 2.2 1 2,2-Dichloropropane ND ug/kg 07/25/23 17:52 594-20-7 v207/25/23 14:487.0 5.3 1 1,1-Dichloropropene ND ug/kg 07/25/23 17:52 563-58-607/25/23 14:487.0 3.4 1 cis-1,3-Dichloropropene ND ug/kg 07/25/23 17:52 10061-01-507/25/23 14:487.0 1.9 1 trans-1,3-Dichloropropene ND ug/kg 07/25/23 17:52 10061-02-607/25/23 14:487.0 2.4 1 Diisopropyl ether ND ug/kg 07/25/23 17:52 108-20-307/25/23 14:487.0 1.9 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-2 (0-2)Lab ID: 92678743005 Collected: 07/19/23 12:05 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene ND ug/kg 07/25/23 17:52 100-41-407/25/23 14:487.0 3.3 1 Hexachloro-1,3-butadiene ND ug/kg 07/25/23 17:52 87-68-307/25/23 14:4814.1 11.5 1 2-Hexanone ND ug/kg 07/25/23 17:52 591-78-607/25/23 14:4870.4 6.8 1 Isopropylbenzene (Cumene)ND ug/kg 07/25/23 17:52 98-82-807/25/23 14:487.0 2.4 1 p-Isopropyltoluene ND ug/kg 07/25/23 17:52 99-87-607/25/23 14:487.0 3.5 1 Methylene Chloride ND ug/kg 07/25/23 17:52 75-09-207/25/23 14:4828.2 19.3 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/25/23 17:52 108-10-107/25/23 14:4870.4 6.8 1 Methyl-tert-butyl ether ND ug/kg 07/25/23 17:52 1634-04-4 v207/25/23 14:487.0 2.6 1 Naphthalene 9.8 ug/kg 07/25/23 17:52 91-20-307/25/23 14:487.0 3.7 1 n-Propylbenzene ND ug/kg 07/25/23 17:52 103-65-107/25/23 14:487.0 2.5 1 Styrene ND ug/kg 07/25/23 17:52 100-42-507/25/23 14:487.0 1.9 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/25/23 17:52 630-20-607/25/23 14:487.0 2.7 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/25/23 17:52 79-34-507/25/23 14:487.0 1.9 1 Tetrachloroethene ND ug/kg 07/25/23 17:52 127-18-407/25/23 14:487.0 2.2 1 Toluene ND ug/kg 07/25/23 17:52 108-88-307/25/23 14:487.0 4.9 1 1,2,3-Trichlorobenzene ND ug/kg 07/25/23 17:52 87-61-607/25/23 14:487.0 5.7 1 1,2,4-Trichlorobenzene ND ug/kg 07/25/23 17:52 120-82-107/25/23 14:487.0 5.9 1 1,1,1-Trichloroethane ND ug/kg 07/25/23 17:52 71-55-607/25/23 14:487.0 3.7 1 1,1,2-Trichloroethane ND ug/kg 07/25/23 17:52 79-00-507/25/23 14:487.0 2.3 1 Trichloroethene ND ug/kg 07/25/23 17:52 79-01-607/25/23 14:487.0 5.7 1 Trichlorofluoromethane ND ug/kg 07/25/23 17:52 75-69-407/25/23 14:487.0 3.9 1 1,2,3-Trichloropropane ND ug/kg 07/25/23 17:52 96-18-407/25/23 14:487.0 3.6 1 1,2,4-Trimethylbenzene ND ug/kg 07/25/23 17:52 95-63-607/25/23 14:487.0 4.2 1 1,3,5-Trimethylbenzene ND ug/kg 07/25/23 17:52 108-67-807/25/23 14:487.0 2.4 1 Vinyl acetate ND ug/kg 07/25/23 17:52 108-05-407/25/23 14:4870.4 14.5 1 Vinyl chloride ND ug/kg 07/25/23 17:52 75-01-4 v207/25/23 14:4814.1 3.6 1 Xylene (Total)ND ug/kg 07/25/23 17:52 1330-20-707/25/23 14:4814.1 4.0 1 m&p-Xylene ND ug/kg 07/25/23 17:52 179601-23-107/25/23 14:4814.1 4.8 1 o-Xylene ND ug/kg 07/25/23 17:52 95-47-607/25/23 14:487.0 3.1 1 Surrogates Toluene-d8 (S)101 %07/25/23 17:52 2037-26-507/25/23 14:4870-130 1 4-Bromofluorobenzene (S)104 %07/25/23 17:52 460-00-407/25/23 14:4870-130 1 1,2-Dichloroethane-d4 (S)110 %07/25/23 17:52 17060-07-007/25/23 14:4870-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 18.8 %07/24/23 14:07 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 83.5 %07/27/23 12:4607/27/23 12:321 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-2 (0-2)Lab ID: 92678743005 Collected: 07/19/23 12:05 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.969J mg/kg 07/28/23 15:11 18540-29-9 J07/28/23 10:001.20 0.305 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-3 (0-2)Lab ID: 92678743006 Collected: 07/19/23 12:20 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: 3050B Pace National - Mt. Juliet Metals (ICPMS) 6020B Arsenic 6.76 mg/kg 08/01/23 15:42 7440-38-207/27/23 03:221.28 0.128 5 Barium 50.4 mg/kg 08/01/23 15:42 7440-39-307/27/23 03:223.20 0.194 5 Cadmium ND mg/kg 08/01/23 15:42 7440-43-907/27/23 03:221.28 0.109 5 Chromium 30.1 mg/kg 08/01/23 15:42 7440-47-307/27/23 03:226.40 0.379 5 Lead 16.1 mg/kg 08/01/23 15:42 7439-92-107/27/23 03:222.56 0.127 5 Selenium 1.23J mg/kg 08/01/23 15:42 7782-49-2 J07/27/23 03:223.20 0.230 5 Silver ND mg/kg 08/01/23 15:42 7440-22-407/27/23 03:220.640 0.111 5 Analytical Method: EPA 7471B Preparation Method: 7471A Pace National - Mt. Juliet Mercury 7471B Mercury 0.0273J mg/kg 07/30/23 18:30 7439-97-6 J07/28/23 10:460.0512 0.0230 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 07/30/23 10:40 83-32-907/27/23 18:30434 153 1 Acenaphthylene ND ug/kg 07/30/23 10:40 208-96-807/27/23 18:30434 153 1 Aniline ND ug/kg 07/30/23 10:40 62-53-307/27/23 18:30434 170 1 Anthracene ND ug/kg 07/30/23 10:40 120-12-707/27/23 18:30434 142 1 Benzo(a)anthracene ND ug/kg 07/30/23 10:40 56-55-307/27/23 18:30434 145 1 Benzo(a)pyrene ND ug/kg 07/30/23 10:40 50-32-807/27/23 18:30434 150 1 Benzo(b)fluoranthene ND ug/kg 07/30/23 10:40 205-99-207/27/23 18:30434 145 1 Benzo(g,h,i)perylene ND ug/kg 07/30/23 10:40 191-24-207/27/23 18:30434 168 1 Benzo(k)fluoranthene ND ug/kg 07/30/23 10:40 207-08-907/27/23 18:30434 153 1 Benzoic Acid ND ug/kg 07/30/23 10:40 65-85-007/27/23 18:302170 933 1 Benzyl alcohol ND ug/kg 07/30/23 10:40 100-51-607/27/23 18:30868 329 1 4-Bromophenylphenyl ether ND ug/kg 07/30/23 10:40 101-55-307/27/23 18:30434 167 1 Butylbenzylphthalate ND ug/kg 07/30/23 10:40 85-68-707/27/23 18:30434 183 1 4-Chloro-3-methylphenol ND ug/kg 07/30/23 10:40 59-50-707/27/23 18:30868 305 1 4-Chloroaniline ND ug/kg 07/30/23 10:40 106-47-807/27/23 18:30868 341 1 bis(2-Chloroethoxy)methane ND ug/kg 07/30/23 10:40 111-91-107/27/23 18:30434 180 1 bis(2-Chloroethyl) ether ND ug/kg 07/30/23 10:40 111-44-407/27/23 18:30434 163 1 2-Chloronaphthalene ND ug/kg 07/30/23 10:40 91-58-707/27/23 18:30434 172 1 2-Chlorophenol ND ug/kg 07/30/23 10:40 95-57-807/27/23 18:30434 163 1 4-Chlorophenylphenyl ether ND ug/kg 07/30/23 10:40 7005-72-307/27/23 18:30434 162 1 Chrysene ND ug/kg 07/30/23 10:40 218-01-907/27/23 18:30434 158 1 Dibenz(a,h)anthracene ND ug/kg 07/30/23 10:40 53-70-307/27/23 18:30434 167 1 Dibenzofuran ND ug/kg 07/30/23 10:40 132-64-907/27/23 18:30434 157 1 1,2-Dichlorobenzene ND ug/kg 07/30/23 10:40 95-50-107/27/23 18:30434 157 1 1,3-Dichlorobenzene ND ug/kg 07/30/23 10:40 541-73-107/27/23 18:30434 154 1 1,4-Dichlorobenzene ND ug/kg 07/30/23 10:40 106-46-707/27/23 18:30434 166 1 3,3'-Dichlorobenzidine ND ug/kg 07/30/23 10:40 91-94-107/27/23 18:30868 293 1 2,4-Dichlorophenol ND ug/kg 07/30/23 10:40 120-83-207/27/23 18:30434 170 1 Diethylphthalate ND ug/kg 07/30/23 10:40 84-66-207/27/23 18:30434 159 1 2,4-Dimethylphenol ND ug/kg 07/30/23 10:40 105-67-9 v107/27/23 18:30434 180 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-3 (0-2)Lab ID: 92678743006 Collected: 07/19/23 12:20 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 07/30/23 10:40 131-11-307/27/23 18:30434 158 1 Di-n-butylphthalate ND ug/kg 07/30/23 10:40 84-74-207/27/23 18:30434 146 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/30/23 10:40 534-52-107/27/23 18:30868 405 1 2,4-Dinitrophenol ND ug/kg 07/30/23 10:40 51-28-507/27/23 18:302170 1340 1 2,4-Dinitrotoluene ND ug/kg 07/30/23 10:40 121-14-207/27/23 18:30434 167 1 2,6-Dinitrotoluene ND ug/kg 07/30/23 10:40 606-20-207/27/23 18:30434 159 1 Di-n-octylphthalate ND ug/kg 07/30/23 10:40 117-84-007/27/23 18:30434 171 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/30/23 10:40 117-81-707/27/23 18:30434 168 1 Fluoranthene ND ug/kg 07/30/23 10:40 206-44-007/27/23 18:30434 149 1 Fluorene ND ug/kg 07/30/23 10:40 86-73-707/27/23 18:30434 153 1 Hexachloro-1,3-butadiene ND ug/kg 07/30/23 10:40 87-68-307/27/23 18:30434 188 1 Hexachlorobenzene ND ug/kg 07/30/23 10:40 118-74-107/27/23 18:30434 170 1 Hexachlorocyclopentadiene ND ug/kg 07/30/23 10:40 77-47-4 v207/27/23 18:30434 249 1 Hexachloroethane ND ug/kg 07/30/23 10:40 67-72-107/27/23 18:30434 166 1 Indeno(1,2,3-cd)pyrene ND ug/kg 07/30/23 10:40 193-39-507/27/23 18:30434 171 1 Isophorone ND ug/kg 07/30/23 10:40 78-59-107/27/23 18:30434 193 1 1-Methylnaphthalene ND ug/kg 07/30/23 10:40 90-12-007/27/23 18:30434 153 1 2-Methylnaphthalene ND ug/kg 07/30/23 10:40 91-57-607/27/23 18:30434 174 1 2-Methylphenol(o-Cresol)ND ug/kg 07/30/23 10:40 95-48-707/27/23 18:30434 178 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/30/23 10:40 15831-10-407/27/23 18:30434 175 1 Naphthalene ND ug/kg 07/30/23 10:40 91-20-307/27/23 18:30434 147 1 2-Nitroaniline ND ug/kg 07/30/23 10:40 88-74-407/27/23 18:302170 355 1 3-Nitroaniline ND ug/kg 07/30/23 10:40 99-09-207/27/23 18:302170 341 1 4-Nitroaniline ND ug/kg 07/30/23 10:40 100-01-607/27/23 18:30868 330 1 Nitrobenzene ND ug/kg 07/30/23 10:40 98-95-307/27/23 18:30434 201 1 2-Nitrophenol ND ug/kg 07/30/23 10:40 88-75-507/27/23 18:30434 188 1 4-Nitrophenol ND ug/kg 07/30/23 10:40 100-02-7 v207/27/23 18:302170 839 1 N-Nitrosodimethylamine ND ug/kg 07/30/23 10:40 62-75-907/27/23 18:30434 146 1 N-Nitroso-di-n-propylamine ND ug/kg 07/30/23 10:40 621-64-707/27/23 18:30434 163 1 N-Nitrosodiphenylamine ND ug/kg 07/30/23 10:40 86-30-607/27/23 18:30434 154 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/30/23 10:40 108-60-107/27/23 18:30434 207 1 Pentachlorophenol ND ug/kg 07/30/23 10:40 87-86-5 v207/27/23 18:30868 425 1 Phenanthrene ND ug/kg 07/30/23 10:40 85-01-807/27/23 18:30434 142 1 Phenol ND ug/kg 07/30/23 10:40 108-95-207/27/23 18:30434 193 1 Pyrene ND ug/kg 07/30/23 10:40 129-00-007/27/23 18:30434 176 1 Pyridine ND ug/kg 07/30/23 10:40 110-86-107/27/23 18:30434 137 1 1,2,4-Trichlorobenzene ND ug/kg 07/30/23 10:40 120-82-107/27/23 18:30434 171 1 2,4,5-Trichlorophenol ND ug/kg 07/30/23 10:40 95-95-407/27/23 18:30434 199 1 2,4,6-Trichlorophenol ND ug/kg 07/30/23 10:40 88-06-207/27/23 18:30434 179 1 Surrogates Nitrobenzene-d5 (S)65 %07/30/23 10:40 4165-60-007/27/23 18:3010-130 1 2-Fluorobiphenyl (S)62 %07/30/23 10:40 321-60-807/27/23 18:3010-130 1 Terphenyl-d14 (S)64 %07/30/23 10:40 1718-51-007/27/23 18:3010-130 1 Phenol-d6 (S)57 %07/30/23 10:40 13127-88-307/27/23 18:3010-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-3 (0-2)Lab ID: 92678743006 Collected: 07/19/23 12:20 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)59 %07/30/23 10:40 367-12-407/27/23 18:3010-130 1 2,4,6-Tribromophenol (S)59 %07/30/23 10:40 118-79-607/27/23 18:3010-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 07/25/23 18:29 67-64-107/25/23 14:48155 49.8 1 Benzene ND ug/kg 07/25/23 18:29 71-43-207/25/23 14:487.8 3.1 1 Bromobenzene ND ug/kg 07/25/23 18:29 108-86-107/25/23 14:487.8 2.5 1 Bromochloromethane ND ug/kg 07/25/23 18:29 74-97-507/25/23 14:487.8 2.3 1 Bromodichloromethane ND ug/kg 07/25/23 18:29 75-27-407/25/23 14:487.8 3.0 1 Bromoform ND ug/kg 07/25/23 18:29 75-25-207/25/23 14:487.8 2.7 1 Bromomethane ND ug/kg 07/25/23 18:29 74-83-9 IH07/25/23 14:4831.1 24.1 1 2-Butanone (MEK)ND ug/kg 07/25/23 18:29 78-93-307/25/23 14:48155 37.3 1 n-Butylbenzene ND ug/kg 07/25/23 18:29 104-51-807/25/23 14:487.8 4.9 1 sec-Butylbenzene ND ug/kg 07/25/23 18:29 135-98-807/25/23 14:487.8 3.4 1 tert-Butylbenzene ND ug/kg 07/25/23 18:29 98-06-607/25/23 14:487.8 2.8 1 Carbon tetrachloride ND ug/kg 07/25/23 18:29 56-23-507/25/23 14:487.8 2.9 1 Chlorobenzene ND ug/kg 07/25/23 18:29 108-90-707/25/23 14:487.8 4.5 1 Chloroethane ND ug/kg 07/25/23 18:29 75-00-307/25/23 14:4815.5 6.0 1 Chloroform ND ug/kg 07/25/23 18:29 67-66-307/25/23 14:487.8 6.5 1 Chloromethane ND ug/kg 07/25/23 18:29 74-87-307/25/23 14:4815.5 6.5 1 2-Chlorotoluene ND ug/kg 07/25/23 18:29 95-49-807/25/23 14:487.8 2.7 1 4-Chlorotoluene ND ug/kg 07/25/23 18:29 106-43-407/25/23 14:487.8 4.3 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/25/23 18:29 96-12-807/25/23 14:487.8 3.0 1 Dibromochloromethane ND ug/kg 07/25/23 18:29 124-48-107/25/23 14:487.8 4.4 1 1,2-Dibromoethane (EDB)ND ug/kg 07/25/23 18:29 106-93-407/25/23 14:487.8 3.4 1 Dibromomethane ND ug/kg 07/25/23 18:29 74-95-307/25/23 14:487.8 1.7 1 1,2-Dichlorobenzene ND ug/kg 07/25/23 18:29 95-50-107/25/23 14:487.8 2.8 1 1,3-Dichlorobenzene ND ug/kg 07/25/23 18:29 541-73-107/25/23 14:487.8 2.4 1 1,4-Dichlorobenzene ND ug/kg 07/25/23 18:29 106-46-707/25/23 14:487.8 2.0 1 Dichlorodifluoromethane ND ug/kg 07/25/23 18:29 75-71-807/25/23 14:4815.5 7.9 1 1,1-Dichloroethane ND ug/kg 07/25/23 18:29 75-34-307/25/23 14:487.8 3.2 1 1,2-Dichloroethane ND ug/kg 07/25/23 18:29 107-06-207/25/23 14:487.8 5.1 1 1,1-Dichloroethene ND ug/kg 07/25/23 18:29 75-35-407/25/23 14:487.8 3.2 1 cis-1,2-Dichloroethene ND ug/kg 07/25/23 18:29 156-59-207/25/23 14:487.8 2.7 1 trans-1,2-Dichloroethene ND ug/kg 07/25/23 18:29 156-60-507/25/23 14:487.8 6.6 1 1,2-Dichloropropane ND ug/kg 07/25/23 18:29 78-87-507/25/23 14:487.8 2.3 1 1,3-Dichloropropane ND ug/kg 07/25/23 18:29 142-28-907/25/23 14:487.8 2.4 1 2,2-Dichloropropane ND ug/kg 07/25/23 18:29 594-20-7 v207/25/23 14:487.8 5.9 1 1,1-Dichloropropene ND ug/kg 07/25/23 18:29 563-58-607/25/23 14:487.8 3.7 1 cis-1,3-Dichloropropene ND ug/kg 07/25/23 18:29 10061-01-507/25/23 14:487.8 2.1 1 trans-1,3-Dichloropropene ND ug/kg 07/25/23 18:29 10061-02-607/25/23 14:487.8 2.7 1 Diisopropyl ether ND ug/kg 07/25/23 18:29 108-20-307/25/23 14:487.8 2.1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-3 (0-2)Lab ID: 92678743006 Collected: 07/19/23 12:20 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene 15.4 ug/kg 07/25/23 18:29 100-41-407/25/23 14:487.8 3.6 1 Hexachloro-1,3-butadiene ND ug/kg 07/25/23 18:29 87-68-307/25/23 14:4815.5 12.7 1 2-Hexanone ND ug/kg 07/25/23 18:29 591-78-607/25/23 14:4877.6 7.5 1 Isopropylbenzene (Cumene)8.3 ug/kg 07/25/23 18:29 98-82-807/25/23 14:487.8 2.6 1 p-Isopropyltoluene 3.9J ug/kg 07/25/23 18:29 99-87-607/25/23 14:487.8 3.8 1 Methylene Chloride ND ug/kg 07/25/23 18:29 75-09-207/25/23 14:4831.1 21.3 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/25/23 18:29 108-10-107/25/23 14:4877.6 7.5 1 Methyl-tert-butyl ether ND ug/kg 07/25/23 18:29 1634-04-4 v207/25/23 14:487.8 2.9 1 Naphthalene 130 ug/kg 07/25/23 18:29 91-20-307/25/23 14:487.8 4.1 1 n-Propylbenzene ND ug/kg 07/25/23 18:29 103-65-107/25/23 14:487.8 2.8 1 Styrene ND ug/kg 07/25/23 18:29 100-42-507/25/23 14:487.8 2.0 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/25/23 18:29 630-20-607/25/23 14:487.8 3.0 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/25/23 18:29 79-34-507/25/23 14:487.8 2.0 1 Tetrachloroethene ND ug/kg 07/25/23 18:29 127-18-407/25/23 14:487.8 2.5 1 Toluene 22.5 ug/kg 07/25/23 18:29 108-88-307/25/23 14:487.8 5.4 1 1,2,3-Trichlorobenzene ND ug/kg 07/25/23 18:29 87-61-607/25/23 14:487.8 6.3 1 1,2,4-Trichlorobenzene ND ug/kg 07/25/23 18:29 120-82-107/25/23 14:487.8 6.5 1 1,1,1-Trichloroethane ND ug/kg 07/25/23 18:29 71-55-607/25/23 14:487.8 4.0 1 1,1,2-Trichloroethane ND ug/kg 07/25/23 18:29 79-00-507/25/23 14:487.8 2.6 1 Trichloroethene ND ug/kg 07/25/23 18:29 79-01-607/25/23 14:487.8 6.3 1 Trichlorofluoromethane ND ug/kg 07/25/23 18:29 75-69-407/25/23 14:487.8 4.3 1 1,2,3-Trichloropropane ND ug/kg 07/25/23 18:29 96-18-407/25/23 14:487.8 3.9 1 1,2,4-Trimethylbenzene 28.9 ug/kg 07/25/23 18:29 95-63-607/25/23 14:487.8 4.6 1 1,3,5-Trimethylbenzene ND ug/kg 07/25/23 18:29 108-67-807/25/23 14:487.8 2.6 1 Vinyl acetate ND ug/kg 07/25/23 18:29 108-05-407/25/23 14:4877.6 16.0 1 Vinyl chloride ND ug/kg 07/25/23 18:29 75-01-4 v207/25/23 14:4815.5 3.9 1 Xylene (Total)160 ug/kg 07/25/23 18:29 1330-20-707/25/23 14:4815.5 4.4 1 m&p-Xylene 95.6 ug/kg 07/25/23 18:29 179601-23-107/25/23 14:4815.5 5.3 1 o-Xylene 64.8 ug/kg 07/25/23 18:29 95-47-607/25/23 14:487.8 3.4 1 Surrogates Toluene-d8 (S)101 %07/25/23 18:29 2037-26-507/25/23 14:4870-130 1 4-Bromofluorobenzene (S)100 %07/25/23 18:29 460-00-407/25/23 14:4870-130 1 1,2-Dichloroethane-d4 (S)107 %07/25/23 18:29 17060-07-007/25/23 14:4870-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 22.7 %07/24/23 14:07 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 78.2 %07/27/23 12:4607/27/23 12:321 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-3 (0-2)Lab ID: 92678743006 Collected: 07/19/23 12:20 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 1.34 mg/kg 07/28/23 15:16 18540-29-907/28/23 10:001.28 0.326 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-4 (0-2)Lab ID: 92678743007 Collected: 07/19/23 14:35 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: 3050B Pace National - Mt. Juliet Metals (ICPMS) 6020B Arsenic 6.80 mg/kg 08/01/23 15:46 7440-38-207/27/23 03:221.30 0.130 5 Barium 36.8 mg/kg 08/01/23 15:46 7440-39-307/27/23 03:223.26 0.198 5 Cadmium ND mg/kg 08/01/23 15:46 7440-43-907/27/23 03:221.30 0.112 5 Chromium 28.1 mg/kg 08/01/23 15:46 7440-47-307/27/23 03:226.52 0.386 5 Lead 11.2 mg/kg 08/01/23 15:46 7439-92-107/27/23 03:222.61 0.129 5 Selenium 1.57J mg/kg 08/01/23 15:46 7782-49-2 J07/27/23 03:223.26 0.235 5 Silver ND mg/kg 08/01/23 15:46 7440-22-407/27/23 03:220.652 0.113 5 Analytical Method: EPA 7471B Preparation Method: 7471A Pace National - Mt. Juliet Mercury 7471B Mercury 0.120 mg/kg 07/30/23 18:32 7439-97-607/28/23 10:460.0522 0.0235 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 07/30/23 11:07 83-32-907/27/23 18:30422 148 1 Acenaphthylene ND ug/kg 07/30/23 11:07 208-96-807/27/23 18:30422 148 1 Aniline ND ug/kg 07/30/23 11:07 62-53-307/27/23 18:30422 165 1 Anthracene ND ug/kg 07/30/23 11:07 120-12-707/27/23 18:30422 138 1 Benzo(a)anthracene ND ug/kg 07/30/23 11:07 56-55-307/27/23 18:30422 141 1 Benzo(a)pyrene ND ug/kg 07/30/23 11:07 50-32-807/27/23 18:30422 146 1 Benzo(b)fluoranthene ND ug/kg 07/30/23 11:07 205-99-207/27/23 18:30422 141 1 Benzo(g,h,i)perylene ND ug/kg 07/30/23 11:07 191-24-207/27/23 18:30422 164 1 Benzo(k)fluoranthene ND ug/kg 07/30/23 11:07 207-08-907/27/23 18:30422 148 1 Benzoic Acid ND ug/kg 07/30/23 11:07 65-85-007/27/23 18:302110 906 1 Benzyl alcohol ND ug/kg 07/30/23 11:07 100-51-607/27/23 18:30843 319 1 4-Bromophenylphenyl ether ND ug/kg 07/30/23 11:07 101-55-307/27/23 18:30422 162 1 Butylbenzylphthalate ND ug/kg 07/30/23 11:07 85-68-707/27/23 18:30422 178 1 4-Chloro-3-methylphenol ND ug/kg 07/30/23 11:07 59-50-707/27/23 18:30843 296 1 4-Chloroaniline ND ug/kg 07/30/23 11:07 106-47-807/27/23 18:30843 331 1 bis(2-Chloroethoxy)methane ND ug/kg 07/30/23 11:07 111-91-107/27/23 18:30422 175 1 bis(2-Chloroethyl) ether ND ug/kg 07/30/23 11:07 111-44-407/27/23 18:30422 158 1 2-Chloronaphthalene ND ug/kg 07/30/23 11:07 91-58-707/27/23 18:30422 167 1 2-Chlorophenol ND ug/kg 07/30/23 11:07 95-57-807/27/23 18:30422 158 1 4-Chlorophenylphenyl ether ND ug/kg 07/30/23 11:07 7005-72-307/27/23 18:30422 157 1 Chrysene ND ug/kg 07/30/23 11:07 218-01-907/27/23 18:30422 153 1 Dibenz(a,h)anthracene ND ug/kg 07/30/23 11:07 53-70-307/27/23 18:30422 162 1 Dibenzofuran ND ug/kg 07/30/23 11:07 132-64-907/27/23 18:30422 152 1 1,2-Dichlorobenzene ND ug/kg 07/30/23 11:07 95-50-107/27/23 18:30422 152 1 1,3-Dichlorobenzene ND ug/kg 07/30/23 11:07 541-73-107/27/23 18:30422 150 1 1,4-Dichlorobenzene ND ug/kg 07/30/23 11:07 106-46-707/27/23 18:30422 161 1 3,3'-Dichlorobenzidine ND ug/kg 07/30/23 11:07 91-94-107/27/23 18:30843 285 1 2,4-Dichlorophenol ND ug/kg 07/30/23 11:07 120-83-207/27/23 18:30422 165 1 Diethylphthalate ND ug/kg 07/30/23 11:07 84-66-207/27/23 18:30422 155 1 2,4-Dimethylphenol ND ug/kg 07/30/23 11:07 105-67-9 v107/27/23 18:30422 175 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-4 (0-2)Lab ID: 92678743007 Collected: 07/19/23 14:35 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 07/30/23 11:07 131-11-307/27/23 18:30422 153 1 Di-n-butylphthalate ND ug/kg 07/30/23 11:07 84-74-207/27/23 18:30422 142 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/30/23 11:07 534-52-107/27/23 18:30843 394 1 2,4-Dinitrophenol ND ug/kg 07/30/23 11:07 51-28-507/27/23 18:302110 1300 1 2,4-Dinitrotoluene ND ug/kg 07/30/23 11:07 121-14-207/27/23 18:30422 162 1 2,6-Dinitrotoluene ND ug/kg 07/30/23 11:07 606-20-207/27/23 18:30422 155 1 Di-n-octylphthalate ND ug/kg 07/30/23 11:07 117-84-007/27/23 18:30422 166 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/30/23 11:07 117-81-707/27/23 18:30422 164 1 Fluoranthene ND ug/kg 07/30/23 11:07 206-44-007/27/23 18:30422 144 1 Fluorene ND ug/kg 07/30/23 11:07 86-73-707/27/23 18:30422 148 1 Hexachloro-1,3-butadiene ND ug/kg 07/30/23 11:07 87-68-307/27/23 18:30422 183 1 Hexachlorobenzene ND ug/kg 07/30/23 11:07 118-74-107/27/23 18:30422 165 1 Hexachlorocyclopentadiene ND ug/kg 07/30/23 11:07 77-47-4 v207/27/23 18:30422 242 1 Hexachloroethane ND ug/kg 07/30/23 11:07 67-72-107/27/23 18:30422 161 1 Indeno(1,2,3-cd)pyrene ND ug/kg 07/30/23 11:07 193-39-507/27/23 18:30422 166 1 Isophorone ND ug/kg 07/30/23 11:07 78-59-107/27/23 18:30422 188 1 1-Methylnaphthalene ND ug/kg 07/30/23 11:07 90-12-007/27/23 18:30422 148 1 2-Methylnaphthalene ND ug/kg 07/30/23 11:07 91-57-607/27/23 18:30422 169 1 2-Methylphenol(o-Cresol)ND ug/kg 07/30/23 11:07 95-48-707/27/23 18:30422 173 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/30/23 11:07 15831-10-407/27/23 18:30422 170 1 Naphthalene ND ug/kg 07/30/23 11:07 91-20-307/27/23 18:30422 143 1 2-Nitroaniline ND ug/kg 07/30/23 11:07 88-74-407/27/23 18:302110 345 1 3-Nitroaniline ND ug/kg 07/30/23 11:07 99-09-207/27/23 18:302110 331 1 4-Nitroaniline ND ug/kg 07/30/23 11:07 100-01-607/27/23 18:30843 321 1 Nitrobenzene ND ug/kg 07/30/23 11:07 98-95-307/27/23 18:30422 196 1 2-Nitrophenol ND ug/kg 07/30/23 11:07 88-75-507/27/23 18:30422 183 1 4-Nitrophenol ND ug/kg 07/30/23 11:07 100-02-7 v207/27/23 18:302110 815 1 N-Nitrosodimethylamine ND ug/kg 07/30/23 11:07 62-75-907/27/23 18:30422 142 1 N-Nitroso-di-n-propylamine ND ug/kg 07/30/23 11:07 621-64-707/27/23 18:30422 158 1 N-Nitrosodiphenylamine ND ug/kg 07/30/23 11:07 86-30-607/27/23 18:30422 150 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/30/23 11:07 108-60-107/27/23 18:30422 201 1 Pentachlorophenol ND ug/kg 07/30/23 11:07 87-86-5 v207/27/23 18:30843 413 1 Phenanthrene ND ug/kg 07/30/23 11:07 85-01-807/27/23 18:30422 138 1 Phenol ND ug/kg 07/30/23 11:07 108-95-207/27/23 18:30422 188 1 Pyrene ND ug/kg 07/30/23 11:07 129-00-007/27/23 18:30422 171 1 Pyridine ND ug/kg 07/30/23 11:07 110-86-107/27/23 18:30422 133 1 1,2,4-Trichlorobenzene ND ug/kg 07/30/23 11:07 120-82-107/27/23 18:30422 166 1 2,4,5-Trichlorophenol ND ug/kg 07/30/23 11:07 95-95-407/27/23 18:30422 193 1 2,4,6-Trichlorophenol ND ug/kg 07/30/23 11:07 88-06-207/27/23 18:30422 174 1 Surrogates Nitrobenzene-d5 (S)57 %07/30/23 11:07 4165-60-007/27/23 18:3010-130 1 2-Fluorobiphenyl (S)61 %07/30/23 11:07 321-60-807/27/23 18:3010-130 1 Terphenyl-d14 (S)56 %07/30/23 11:07 1718-51-007/27/23 18:3010-130 1 Phenol-d6 (S)51 %07/30/23 11:07 13127-88-307/27/23 18:3010-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-4 (0-2)Lab ID: 92678743007 Collected: 07/19/23 14:35 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)52 %07/30/23 11:07 367-12-407/27/23 18:3010-130 1 2,4,6-Tribromophenol (S)56 %07/30/23 11:07 118-79-607/27/23 18:3010-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 07/25/23 18:48 67-64-107/25/23 14:48145 46.5 1 Benzene ND ug/kg 07/25/23 18:48 71-43-207/25/23 14:487.2 2.9 1 Bromobenzene ND ug/kg 07/25/23 18:48 108-86-107/25/23 14:487.2 2.4 1 Bromochloromethane ND ug/kg 07/25/23 18:48 74-97-507/25/23 14:487.2 2.1 1 Bromodichloromethane ND ug/kg 07/25/23 18:48 75-27-407/25/23 14:487.2 2.8 1 Bromoform ND ug/kg 07/25/23 18:48 75-25-207/25/23 14:487.2 2.6 1 Bromomethane ND ug/kg 07/25/23 18:48 74-83-9 IH07/25/23 14:4829.0 22.5 1 2-Butanone (MEK)ND ug/kg 07/25/23 18:48 78-93-307/25/23 14:48145 34.8 1 n-Butylbenzene ND ug/kg 07/25/23 18:48 104-51-807/25/23 14:487.2 4.6 1 sec-Butylbenzene ND ug/kg 07/25/23 18:48 135-98-807/25/23 14:487.2 3.2 1 tert-Butylbenzene ND ug/kg 07/25/23 18:48 98-06-607/25/23 14:487.2 2.6 1 Carbon tetrachloride ND ug/kg 07/25/23 18:48 56-23-507/25/23 14:487.2 2.7 1 Chlorobenzene ND ug/kg 07/25/23 18:48 108-90-707/25/23 14:487.2 4.2 1 Chloroethane ND ug/kg 07/25/23 18:48 75-00-307/25/23 14:4814.5 5.6 1 Chloroform ND ug/kg 07/25/23 18:48 67-66-307/25/23 14:487.2 6.1 1 Chloromethane 6.1J ug/kg 07/25/23 18:48 74-87-307/25/23 14:4814.5 6.1 1 2-Chlorotoluene ND ug/kg 07/25/23 18:48 95-49-807/25/23 14:487.2 2.6 1 4-Chlorotoluene ND ug/kg 07/25/23 18:48 106-43-407/25/23 14:487.2 4.0 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/25/23 18:48 96-12-807/25/23 14:487.2 2.8 1 Dibromochloromethane ND ug/kg 07/25/23 18:48 124-48-107/25/23 14:487.2 4.1 1 1,2-Dibromoethane (EDB)ND ug/kg 07/25/23 18:48 106-93-407/25/23 14:487.2 3.2 1 Dibromomethane ND ug/kg 07/25/23 18:48 74-95-307/25/23 14:487.2 1.6 1 1,2-Dichlorobenzene ND ug/kg 07/25/23 18:48 95-50-107/25/23 14:487.2 2.6 1 1,3-Dichlorobenzene ND ug/kg 07/25/23 18:48 541-73-107/25/23 14:487.2 2.2 1 1,4-Dichlorobenzene ND ug/kg 07/25/23 18:48 106-46-707/25/23 14:487.2 1.9 1 Dichlorodifluoromethane ND ug/kg 07/25/23 18:48 75-71-807/25/23 14:4814.5 7.4 1 1,1-Dichloroethane ND ug/kg 07/25/23 18:48 75-34-307/25/23 14:487.2 3.0 1 1,2-Dichloroethane ND ug/kg 07/25/23 18:48 107-06-207/25/23 14:487.2 4.8 1 1,1-Dichloroethene ND ug/kg 07/25/23 18:48 75-35-407/25/23 14:487.2 3.0 1 cis-1,2-Dichloroethene ND ug/kg 07/25/23 18:48 156-59-207/25/23 14:487.2 2.5 1 trans-1,2-Dichloroethene ND ug/kg 07/25/23 18:48 156-60-507/25/23 14:487.2 6.2 1 1,2-Dichloropropane ND ug/kg 07/25/23 18:48 78-87-507/25/23 14:487.2 2.2 1 1,3-Dichloropropane ND ug/kg 07/25/23 18:48 142-28-907/25/23 14:487.2 2.3 1 2,2-Dichloropropane ND ug/kg 07/25/23 18:48 594-20-7 v207/25/23 14:487.2 5.5 1 1,1-Dichloropropene ND ug/kg 07/25/23 18:48 563-58-607/25/23 14:487.2 3.5 1 cis-1,3-Dichloropropene ND ug/kg 07/25/23 18:48 10061-01-507/25/23 14:487.2 2.0 1 trans-1,3-Dichloropropene ND ug/kg 07/25/23 18:48 10061-02-607/25/23 14:487.2 2.5 1 Diisopropyl ether ND ug/kg 07/25/23 18:48 108-20-307/25/23 14:487.2 2.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-4 (0-2)Lab ID: 92678743007 Collected: 07/19/23 14:35 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene ND ug/kg 07/25/23 18:48 100-41-407/25/23 14:487.2 3.4 1 Hexachloro-1,3-butadiene ND ug/kg 07/25/23 18:48 87-68-307/25/23 14:4814.5 11.9 1 2-Hexanone ND ug/kg 07/25/23 18:48 591-78-607/25/23 14:4872.5 7.0 1 Isopropylbenzene (Cumene)ND ug/kg 07/25/23 18:48 98-82-807/25/23 14:487.2 2.5 1 p-Isopropyltoluene ND ug/kg 07/25/23 18:48 99-87-607/25/23 14:487.2 3.6 1 Methylene Chloride ND ug/kg 07/25/23 18:48 75-09-207/25/23 14:4829.0 19.9 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/25/23 18:48 108-10-107/25/23 14:4872.5 7.0 1 Methyl-tert-butyl ether ND ug/kg 07/25/23 18:48 1634-04-4 v207/25/23 14:487.2 2.7 1 Naphthalene ND ug/kg 07/25/23 18:48 91-20-307/25/23 14:487.2 3.8 1 n-Propylbenzene ND ug/kg 07/25/23 18:48 103-65-107/25/23 14:487.2 2.6 1 Styrene ND ug/kg 07/25/23 18:48 100-42-507/25/23 14:487.2 1.9 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/25/23 18:48 630-20-607/25/23 14:487.2 2.8 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/25/23 18:48 79-34-507/25/23 14:487.2 1.9 1 Tetrachloroethene ND ug/kg 07/25/23 18:48 127-18-407/25/23 14:487.2 2.3 1 Toluene ND ug/kg 07/25/23 18:48 108-88-307/25/23 14:487.2 5.0 1 1,2,3-Trichlorobenzene ND ug/kg 07/25/23 18:48 87-61-607/25/23 14:487.2 5.9 1 1,2,4-Trichlorobenzene ND ug/kg 07/25/23 18:48 120-82-107/25/23 14:487.2 6.1 1 1,1,1-Trichloroethane ND ug/kg 07/25/23 18:48 71-55-607/25/23 14:487.2 3.8 1 1,1,2-Trichloroethane ND ug/kg 07/25/23 18:48 79-00-507/25/23 14:487.2 2.4 1 Trichloroethene ND ug/kg 07/25/23 18:48 79-01-607/25/23 14:487.2 5.8 1 Trichlorofluoromethane ND ug/kg 07/25/23 18:48 75-69-407/25/23 14:487.2 4.0 1 1,2,3-Trichloropropane ND ug/kg 07/25/23 18:48 96-18-407/25/23 14:487.2 3.7 1 1,2,4-Trimethylbenzene ND ug/kg 07/25/23 18:48 95-63-607/25/23 14:487.2 4.3 1 1,3,5-Trimethylbenzene ND ug/kg 07/25/23 18:48 108-67-807/25/23 14:487.2 2.4 1 Vinyl acetate ND ug/kg 07/25/23 18:48 108-05-407/25/23 14:4872.5 14.9 1 Vinyl chloride ND ug/kg 07/25/23 18:48 75-01-4 v207/25/23 14:4814.5 3.7 1 Xylene (Total)ND ug/kg 07/25/23 18:48 1330-20-707/25/23 14:4814.5 4.1 1 m&p-Xylene ND ug/kg 07/25/23 18:48 179601-23-107/25/23 14:4814.5 5.0 1 o-Xylene ND ug/kg 07/25/23 18:48 95-47-607/25/23 14:487.2 3.2 1 Surrogates Toluene-d8 (S)102 %07/25/23 18:48 2037-26-507/25/23 14:4870-130 1 4-Bromofluorobenzene (S)103 %07/25/23 18:48 460-00-407/25/23 14:4870-130 1 1,2-Dichloroethane-d4 (S)110 %07/25/23 18:48 17060-07-007/25/23 14:4870-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 21.2 %07/24/23 14:07 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 76.6 %07/27/23 12:4607/27/23 12:321 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-4 (0-2)Lab ID: 92678743007 Collected: 07/19/23 14:35 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.922J mg/kg 07/28/23 15:21 18540-29-9 D8,J07/28/23 10:001.30 0.333 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 29 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-5 (0-2)Lab ID: 92678743008 Collected: 07/18/23 16:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: 3050B Pace National - Mt. Juliet Metals (ICPMS) 6020B Arsenic 7.09 mg/kg 08/01/23 15:49 7440-38-207/27/23 03:221.23 0.123 5 Barium 61.6 mg/kg 08/01/23 15:49 7440-39-307/27/23 03:223.07 0.187 5 Cadmium ND mg/kg 08/01/23 15:49 7440-43-907/27/23 03:221.23 0.105 5 Chromium 26.5 mg/kg 08/01/23 15:49 7440-47-307/27/23 03:226.15 0.364 5 Lead 33.1 mg/kg 08/01/23 15:49 7439-92-107/27/23 03:222.46 0.122 5 Selenium 1.17J mg/kg 08/01/23 15:49 7782-49-2 J07/27/23 03:223.07 0.221 5 Silver ND mg/kg 08/01/23 15:49 7440-22-407/27/23 03:220.615 0.106 5 Analytical Method: EPA 7471B Preparation Method: 7471A Pace National - Mt. Juliet Mercury 7471B Mercury 0.119 mg/kg 07/30/23 18:40 7439-97-607/28/23 10:460.0492 0.0221 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 07/30/23 11:35 83-32-907/27/23 18:30407 143 1 Acenaphthylene ND ug/kg 07/30/23 11:35 208-96-807/27/23 18:30407 143 1 Aniline ND ug/kg 07/30/23 11:35 62-53-307/27/23 18:30407 159 1 Anthracene ND ug/kg 07/30/23 11:35 120-12-707/27/23 18:30407 133 1 Benzo(a)anthracene ND ug/kg 07/30/23 11:35 56-55-307/27/23 18:30407 136 1 Benzo(a)pyrene ND ug/kg 07/30/23 11:35 50-32-807/27/23 18:30407 140 1 Benzo(b)fluoranthene ND ug/kg 07/30/23 11:35 205-99-207/27/23 18:30407 136 1 Benzo(g,h,i)perylene ND ug/kg 07/30/23 11:35 191-24-207/27/23 18:30407 158 1 Benzo(k)fluoranthene ND ug/kg 07/30/23 11:35 207-08-907/27/23 18:30407 143 1 Benzoic Acid ND ug/kg 07/30/23 11:35 65-85-007/27/23 18:302030 874 1 Benzyl alcohol ND ug/kg 07/30/23 11:35 100-51-607/27/23 18:30813 308 1 4-Bromophenylphenyl ether ND ug/kg 07/30/23 11:35 101-55-307/27/23 18:30407 157 1 Butylbenzylphthalate ND ug/kg 07/30/23 11:35 85-68-707/27/23 18:30407 171 1 4-Chloro-3-methylphenol ND ug/kg 07/30/23 11:35 59-50-707/27/23 18:30813 286 1 4-Chloroaniline ND ug/kg 07/30/23 11:35 106-47-807/27/23 18:30813 319 1 bis(2-Chloroethoxy)methane ND ug/kg 07/30/23 11:35 111-91-107/27/23 18:30407 169 1 bis(2-Chloroethyl) ether ND ug/kg 07/30/23 11:35 111-44-407/27/23 18:30407 153 1 2-Chloronaphthalene ND ug/kg 07/30/23 11:35 91-58-707/27/23 18:30407 161 1 2-Chlorophenol ND ug/kg 07/30/23 11:35 95-57-807/27/23 18:30407 153 1 4-Chlorophenylphenyl ether ND ug/kg 07/30/23 11:35 7005-72-307/27/23 18:30407 152 1 Chrysene ND ug/kg 07/30/23 11:35 218-01-907/27/23 18:30407 148 1 Dibenz(a,h)anthracene ND ug/kg 07/30/23 11:35 53-70-307/27/23 18:30407 157 1 Dibenzofuran ND ug/kg 07/30/23 11:35 132-64-907/27/23 18:30407 147 1 1,2-Dichlorobenzene ND ug/kg 07/30/23 11:35 95-50-107/27/23 18:30407 147 1 1,3-Dichlorobenzene ND ug/kg 07/30/23 11:35 541-73-107/27/23 18:30407 144 1 1,4-Dichlorobenzene ND ug/kg 07/30/23 11:35 106-46-707/27/23 18:30407 155 1 3,3'-Dichlorobenzidine ND ug/kg 07/30/23 11:35 91-94-107/27/23 18:30813 275 1 2,4-Dichlorophenol ND ug/kg 07/30/23 11:35 120-83-207/27/23 18:30407 159 1 Diethylphthalate ND ug/kg 07/30/23 11:35 84-66-207/27/23 18:30407 149 1 2,4-Dimethylphenol ND ug/kg 07/30/23 11:35 105-67-9 v107/27/23 18:30407 169 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 30 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-5 (0-2)Lab ID: 92678743008 Collected: 07/18/23 16:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 07/30/23 11:35 131-11-307/27/23 18:30407 148 1 Di-n-butylphthalate ND ug/kg 07/30/23 11:35 84-74-207/27/23 18:30407 137 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/30/23 11:35 534-52-107/27/23 18:30813 380 1 2,4-Dinitrophenol ND ug/kg 07/30/23 11:35 51-28-507/27/23 18:302030 1260 1 2,4-Dinitrotoluene ND ug/kg 07/30/23 11:35 121-14-207/27/23 18:30407 157 1 2,6-Dinitrotoluene ND ug/kg 07/30/23 11:35 606-20-207/27/23 18:30407 149 1 Di-n-octylphthalate ND ug/kg 07/30/23 11:35 117-84-007/27/23 18:30407 160 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/30/23 11:35 117-81-707/27/23 18:30407 158 1 Fluoranthene ND ug/kg 07/30/23 11:35 206-44-007/27/23 18:30407 139 1 Fluorene ND ug/kg 07/30/23 11:35 86-73-707/27/23 18:30407 143 1 Hexachloro-1,3-butadiene ND ug/kg 07/30/23 11:35 87-68-307/27/23 18:30407 176 1 Hexachlorobenzene ND ug/kg 07/30/23 11:35 118-74-107/27/23 18:30407 159 1 Hexachlorocyclopentadiene ND ug/kg 07/30/23 11:35 77-47-4 v207/27/23 18:30407 233 1 Hexachloroethane ND ug/kg 07/30/23 11:35 67-72-107/27/23 18:30407 155 1 Indeno(1,2,3-cd)pyrene ND ug/kg 07/30/23 11:35 193-39-507/27/23 18:30407 160 1 Isophorone ND ug/kg 07/30/23 11:35 78-59-107/27/23 18:30407 181 1 1-Methylnaphthalene ND ug/kg 07/30/23 11:35 90-12-007/27/23 18:30407 143 1 2-Methylnaphthalene ND ug/kg 07/30/23 11:35 91-57-607/27/23 18:30407 163 1 2-Methylphenol(o-Cresol)ND ug/kg 07/30/23 11:35 95-48-707/27/23 18:30407 166 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/30/23 11:35 15831-10-407/27/23 18:30407 164 1 Naphthalene ND ug/kg 07/30/23 11:35 91-20-307/27/23 18:30407 138 1 2-Nitroaniline ND ug/kg 07/30/23 11:35 88-74-407/27/23 18:302030 333 1 3-Nitroaniline ND ug/kg 07/30/23 11:35 99-09-207/27/23 18:302030 319 1 4-Nitroaniline ND ug/kg 07/30/23 11:35 100-01-607/27/23 18:30813 309 1 Nitrobenzene ND ug/kg 07/30/23 11:35 98-95-307/27/23 18:30407 189 1 2-Nitrophenol ND ug/kg 07/30/23 11:35 88-75-507/27/23 18:30407 176 1 4-Nitrophenol ND ug/kg 07/30/23 11:35 100-02-7 v207/27/23 18:302030 786 1 N-Nitrosodimethylamine ND ug/kg 07/30/23 11:35 62-75-907/27/23 18:30407 137 1 N-Nitroso-di-n-propylamine ND ug/kg 07/30/23 11:35 621-64-707/27/23 18:30407 153 1 N-Nitrosodiphenylamine ND ug/kg 07/30/23 11:35 86-30-607/27/23 18:30407 144 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/30/23 11:35 108-60-107/27/23 18:30407 193 1 Pentachlorophenol ND ug/kg 07/30/23 11:35 87-86-5 v207/27/23 18:30813 398 1 Phenanthrene ND ug/kg 07/30/23 11:35 85-01-807/27/23 18:30407 133 1 Phenol ND ug/kg 07/30/23 11:35 108-95-207/27/23 18:30407 181 1 Pyrene ND ug/kg 07/30/23 11:35 129-00-007/27/23 18:30407 165 1 Pyridine ND ug/kg 07/30/23 11:35 110-86-107/27/23 18:30407 128 1 1,2,4-Trichlorobenzene ND ug/kg 07/30/23 11:35 120-82-107/27/23 18:30407 160 1 2,4,5-Trichlorophenol ND ug/kg 07/30/23 11:35 95-95-407/27/23 18:30407 186 1 2,4,6-Trichlorophenol ND ug/kg 07/30/23 11:35 88-06-207/27/23 18:30407 168 1 Surrogates Nitrobenzene-d5 (S)56 %07/30/23 11:35 4165-60-007/27/23 18:3010-130 1 2-Fluorobiphenyl (S)59 %07/30/23 11:35 321-60-807/27/23 18:3010-130 1 Terphenyl-d14 (S)57 %07/30/23 11:35 1718-51-007/27/23 18:3010-130 1 Phenol-d6 (S)45 %07/30/23 11:35 13127-88-307/27/23 18:3010-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 31 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-5 (0-2)Lab ID: 92678743008 Collected: 07/18/23 16:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)46 %07/30/23 11:35 367-12-407/27/23 18:3010-130 1 2,4,6-Tribromophenol (S)53 %07/30/23 11:35 118-79-607/27/23 18:3010-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 07/25/23 19:06 67-64-107/25/23 14:48157 50.5 1 Benzene ND ug/kg 07/25/23 19:06 71-43-207/25/23 14:487.9 3.1 1 Bromobenzene ND ug/kg 07/25/23 19:06 108-86-107/25/23 14:487.9 2.6 1 Bromochloromethane ND ug/kg 07/25/23 19:06 74-97-507/25/23 14:487.9 2.3 1 Bromodichloromethane ND ug/kg 07/25/23 19:06 75-27-407/25/23 14:487.9 3.0 1 Bromoform ND ug/kg 07/25/23 19:06 75-25-207/25/23 14:487.9 2.8 1 Bromomethane ND ug/kg 07/25/23 19:06 74-83-9 IH07/25/23 14:4831.5 24.4 1 2-Butanone (MEK)ND ug/kg 07/25/23 19:06 78-93-307/25/23 14:48157 37.7 1 n-Butylbenzene ND ug/kg 07/25/23 19:06 104-51-807/25/23 14:487.9 5.0 1 sec-Butylbenzene ND ug/kg 07/25/23 19:06 135-98-807/25/23 14:487.9 3.5 1 tert-Butylbenzene ND ug/kg 07/25/23 19:06 98-06-607/25/23 14:487.9 2.8 1 Carbon tetrachloride ND ug/kg 07/25/23 19:06 56-23-507/25/23 14:487.9 2.9 1 Chlorobenzene ND ug/kg 07/25/23 19:06 108-90-707/25/23 14:487.9 4.5 1 Chloroethane ND ug/kg 07/25/23 19:06 75-00-307/25/23 14:4815.7 6.1 1 Chloroform ND ug/kg 07/25/23 19:06 67-66-307/25/23 14:487.9 6.6 1 Chloromethane ND ug/kg 07/25/23 19:06 74-87-307/25/23 14:4815.7 6.6 1 2-Chlorotoluene ND ug/kg 07/25/23 19:06 95-49-807/25/23 14:487.9 2.8 1 4-Chlorotoluene ND ug/kg 07/25/23 19:06 106-43-407/25/23 14:487.9 4.4 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/25/23 19:06 96-12-807/25/23 14:487.9 3.1 1 Dibromochloromethane ND ug/kg 07/25/23 19:06 124-48-107/25/23 14:487.9 4.4 1 1,2-Dibromoethane (EDB)ND ug/kg 07/25/23 19:06 106-93-407/25/23 14:487.9 3.5 1 Dibromomethane ND ug/kg 07/25/23 19:06 74-95-307/25/23 14:487.9 1.7 1 1,2-Dichlorobenzene ND ug/kg 07/25/23 19:06 95-50-107/25/23 14:487.9 2.8 1 1,3-Dichlorobenzene ND ug/kg 07/25/23 19:06 541-73-107/25/23 14:487.9 2.4 1 1,4-Dichlorobenzene ND ug/kg 07/25/23 19:06 106-46-707/25/23 14:487.9 2.0 1 Dichlorodifluoromethane ND ug/kg 07/25/23 19:06 75-71-807/25/23 14:4815.7 8.0 1 1,1-Dichloroethane ND ug/kg 07/25/23 19:06 75-34-307/25/23 14:487.9 3.2 1 1,2-Dichloroethane ND ug/kg 07/25/23 19:06 107-06-207/25/23 14:487.9 5.2 1 1,1-Dichloroethene ND ug/kg 07/25/23 19:06 75-35-407/25/23 14:487.9 3.2 1 cis-1,2-Dichloroethene ND ug/kg 07/25/23 19:06 156-59-207/25/23 14:487.9 2.7 1 trans-1,2-Dichloroethene ND ug/kg 07/25/23 19:06 156-60-507/25/23 14:487.9 6.7 1 1,2-Dichloropropane ND ug/kg 07/25/23 19:06 78-87-507/25/23 14:487.9 2.4 1 1,3-Dichloropropane ND ug/kg 07/25/23 19:06 142-28-907/25/23 14:487.9 2.5 1 2,2-Dichloropropane ND ug/kg 07/25/23 19:06 594-20-7 v207/25/23 14:487.9 6.0 1 1,1-Dichloropropene ND ug/kg 07/25/23 19:06 563-58-607/25/23 14:487.9 3.8 1 cis-1,3-Dichloropropene ND ug/kg 07/25/23 19:06 10061-01-507/25/23 14:487.9 2.1 1 trans-1,3-Dichloropropene ND ug/kg 07/25/23 19:06 10061-02-607/25/23 14:487.9 2.7 1 Diisopropyl ether ND ug/kg 07/25/23 19:06 108-20-307/25/23 14:487.9 2.1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 32 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-5 (0-2)Lab ID: 92678743008 Collected: 07/18/23 16:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene ND ug/kg 07/25/23 19:06 100-41-407/25/23 14:487.9 3.7 1 Hexachloro-1,3-butadiene ND ug/kg 07/25/23 19:06 87-68-307/25/23 14:4815.7 12.9 1 2-Hexanone ND ug/kg 07/25/23 19:06 591-78-607/25/23 14:4878.6 7.6 1 Isopropylbenzene (Cumene)ND ug/kg 07/25/23 19:06 98-82-807/25/23 14:487.9 2.7 1 p-Isopropyltoluene ND ug/kg 07/25/23 19:06 99-87-607/25/23 14:487.9 3.9 1 Methylene Chloride ND ug/kg 07/25/23 19:06 75-09-207/25/23 14:4831.5 21.5 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/25/23 19:06 108-10-107/25/23 14:4878.6 7.6 1 Methyl-tert-butyl ether ND ug/kg 07/25/23 19:06 1634-04-4 v207/25/23 14:487.9 2.9 1 Naphthalene 5.4J ug/kg 07/25/23 19:06 91-20-307/25/23 14:487.9 4.1 1 n-Propylbenzene ND ug/kg 07/25/23 19:06 103-65-107/25/23 14:487.9 2.8 1 Styrene ND ug/kg 07/25/23 19:06 100-42-507/25/23 14:487.9 2.1 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/25/23 19:06 630-20-607/25/23 14:487.9 3.0 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/25/23 19:06 79-34-507/25/23 14:487.9 2.1 1 Tetrachloroethene ND ug/kg 07/25/23 19:06 127-18-407/25/23 14:487.9 2.5 1 Toluene 7.3J ug/kg 07/25/23 19:06 108-88-307/25/23 14:487.9 5.4 1 1,2,3-Trichlorobenzene ND ug/kg 07/25/23 19:06 87-61-607/25/23 14:487.9 6.4 1 1,2,4-Trichlorobenzene ND ug/kg 07/25/23 19:06 120-82-107/25/23 14:487.9 6.6 1 1,1,1-Trichloroethane ND ug/kg 07/25/23 19:06 71-55-607/25/23 14:487.9 4.1 1 1,1,2-Trichloroethane ND ug/kg 07/25/23 19:06 79-00-507/25/23 14:487.9 2.6 1 Trichloroethene ND ug/kg 07/25/23 19:06 79-01-607/25/23 14:487.9 6.3 1 Trichlorofluoromethane ND ug/kg 07/25/23 19:06 75-69-407/25/23 14:487.9 4.3 1 1,2,3-Trichloropropane ND ug/kg 07/25/23 19:06 96-18-407/25/23 14:487.9 4.0 1 1,2,4-Trimethylbenzene ND ug/kg 07/25/23 19:06 95-63-607/25/23 14:487.9 4.7 1 1,3,5-Trimethylbenzene ND ug/kg 07/25/23 19:06 108-67-807/25/23 14:487.9 2.6 1 Vinyl acetate ND ug/kg 07/25/23 19:06 108-05-407/25/23 14:4878.6 16.2 1 Vinyl chloride ND ug/kg 07/25/23 19:06 75-01-4 v207/25/23 14:4815.7 4.0 1 Xylene (Total)6.9J ug/kg 07/25/23 19:06 1330-20-707/25/23 14:4815.7 4.5 1 m&p-Xylene 6.9J ug/kg 07/25/23 19:06 179601-23-107/25/23 14:4815.7 5.4 1 o-Xylene ND ug/kg 07/25/23 19:06 95-47-607/25/23 14:487.9 3.5 1 Surrogates Toluene-d8 (S)102 %07/25/23 19:06 2037-26-507/25/23 14:4870-130 1 4-Bromofluorobenzene (S)104 %07/25/23 19:06 460-00-407/25/23 14:4870-130 1 1,2-Dichloroethane-d4 (S)109 %07/25/23 19:06 17060-07-007/25/23 14:4870-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 18.0 %07/24/23 14:07 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 81.3 %07/27/23 12:4607/27/23 12:321 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 33 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-5 (0-2)Lab ID: 92678743008 Collected: 07/18/23 16:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.936J mg/kg 07/28/23 15:32 18540-29-9 J07/28/23 10:001.23 0.314 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 34 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-6 (0-2)Lab ID: 92678743009 Collected: 07/18/23 12:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: 3050B Pace National - Mt. Juliet Metals (ICPMS) 6020B Arsenic 7.32 mg/kg 08/01/23 15:53 7440-38-207/27/23 03:221.25 0.125 5 Barium 79.4 mg/kg 08/01/23 15:53 7440-39-307/27/23 03:223.13 0.190 5 Cadmium 0.127J mg/kg 08/01/23 15:53 7440-43-9 J07/27/23 03:221.25 0.107 5 Chromium 21.4 mg/kg 08/01/23 15:53 7440-47-307/27/23 03:226.25 0.370 5 Lead 39.3 mg/kg 08/01/23 15:53 7439-92-107/27/23 03:222.50 0.124 5 Selenium 1.24J mg/kg 08/01/23 15:53 7782-49-2 J07/27/23 03:223.13 0.225 5 Silver ND mg/kg 08/01/23 15:53 7440-22-407/27/23 03:220.625 0.108 5 Analytical Method: EPA 7471B Preparation Method: 7471A Pace National - Mt. Juliet Mercury 7471B Mercury 0.124 mg/kg 07/30/23 18:42 7439-97-607/28/23 10:460.0500 0.0225 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 07/30/23 12:03 83-32-907/27/23 18:30403 142 1 Acenaphthylene ND ug/kg 07/30/23 12:03 208-96-807/27/23 18:30403 142 1 Aniline ND ug/kg 07/30/23 12:03 62-53-307/27/23 18:30403 157 1 Anthracene ND ug/kg 07/30/23 12:03 120-12-707/27/23 18:30403 132 1 Benzo(a)anthracene ND ug/kg 07/30/23 12:03 56-55-307/27/23 18:30403 134 1 Benzo(a)pyrene ND ug/kg 07/30/23 12:03 50-32-807/27/23 18:30403 139 1 Benzo(b)fluoranthene ND ug/kg 07/30/23 12:03 205-99-207/27/23 18:30403 134 1 Benzo(g,h,i)perylene ND ug/kg 07/30/23 12:03 191-24-207/27/23 18:30403 156 1 Benzo(k)fluoranthene ND ug/kg 07/30/23 12:03 207-08-907/27/23 18:30403 142 1 Benzoic Acid ND ug/kg 07/30/23 12:03 65-85-007/27/23 18:302010 865 1 Benzyl alcohol ND ug/kg 07/30/23 12:03 100-51-607/27/23 18:30805 305 1 4-Bromophenylphenyl ether ND ug/kg 07/30/23 12:03 101-55-307/27/23 18:30403 155 1 Butylbenzylphthalate ND ug/kg 07/30/23 12:03 85-68-707/27/23 18:30403 170 1 4-Chloro-3-methylphenol ND ug/kg 07/30/23 12:03 59-50-707/27/23 18:30805 283 1 4-Chloroaniline ND ug/kg 07/30/23 12:03 106-47-807/27/23 18:30805 316 1 bis(2-Chloroethoxy)methane ND ug/kg 07/30/23 12:03 111-91-107/27/23 18:30403 167 1 bis(2-Chloroethyl) ether ND ug/kg 07/30/23 12:03 111-44-407/27/23 18:30403 151 1 2-Chloronaphthalene ND ug/kg 07/30/23 12:03 91-58-707/27/23 18:30403 160 1 2-Chlorophenol ND ug/kg 07/30/23 12:03 95-57-807/27/23 18:30403 151 1 4-Chlorophenylphenyl ether ND ug/kg 07/30/23 12:03 7005-72-307/27/23 18:30403 150 1 Chrysene ND ug/kg 07/30/23 12:03 218-01-907/27/23 18:30403 146 1 Dibenz(a,h)anthracene ND ug/kg 07/30/23 12:03 53-70-307/27/23 18:30403 155 1 Dibenzofuran ND ug/kg 07/30/23 12:03 132-64-907/27/23 18:30403 145 1 1,2-Dichlorobenzene ND ug/kg 07/30/23 12:03 95-50-107/27/23 18:30403 145 1 1,3-Dichlorobenzene ND ug/kg 07/30/23 12:03 541-73-107/27/23 18:30403 143 1 1,4-Dichlorobenzene ND ug/kg 07/30/23 12:03 106-46-707/27/23 18:30403 154 1 3,3'-Dichlorobenzidine ND ug/kg 07/30/23 12:03 91-94-107/27/23 18:30805 272 1 2,4-Dichlorophenol ND ug/kg 07/30/23 12:03 120-83-207/27/23 18:30403 157 1 Diethylphthalate ND ug/kg 07/30/23 12:03 84-66-207/27/23 18:30403 148 1 2,4-Dimethylphenol ND ug/kg 07/30/23 12:03 105-67-9 v107/27/23 18:30403 167 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 35 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-6 (0-2)Lab ID: 92678743009 Collected: 07/18/23 12:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 07/30/23 12:03 131-11-307/27/23 18:30403 146 1 Di-n-butylphthalate ND ug/kg 07/30/23 12:03 84-74-207/27/23 18:30403 135 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/30/23 12:03 534-52-107/27/23 18:30805 376 1 2,4-Dinitrophenol ND ug/kg 07/30/23 12:03 51-28-507/27/23 18:302010 1240 1 2,4-Dinitrotoluene ND ug/kg 07/30/23 12:03 121-14-207/27/23 18:30403 155 1 2,6-Dinitrotoluene ND ug/kg 07/30/23 12:03 606-20-207/27/23 18:30403 148 1 Di-n-octylphthalate ND ug/kg 07/30/23 12:03 117-84-007/27/23 18:30403 159 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/30/23 12:03 117-81-707/27/23 18:30403 156 1 Fluoranthene 177J ug/kg 07/30/23 12:03 206-44-007/27/23 18:30403 138 1 Fluorene ND ug/kg 07/30/23 12:03 86-73-707/27/23 18:30403 142 1 Hexachloro-1,3-butadiene ND ug/kg 07/30/23 12:03 87-68-307/27/23 18:30403 175 1 Hexachlorobenzene ND ug/kg 07/30/23 12:03 118-74-107/27/23 18:30403 157 1 Hexachlorocyclopentadiene ND ug/kg 07/30/23 12:03 77-47-4 v207/27/23 18:30403 231 1 Hexachloroethane ND ug/kg 07/30/23 12:03 67-72-107/27/23 18:30403 154 1 Indeno(1,2,3-cd)pyrene ND ug/kg 07/30/23 12:03 193-39-507/27/23 18:30403 159 1 Isophorone ND ug/kg 07/30/23 12:03 78-59-107/27/23 18:30403 179 1 1-Methylnaphthalene ND ug/kg 07/30/23 12:03 90-12-007/27/23 18:30403 142 1 2-Methylnaphthalene ND ug/kg 07/30/23 12:03 91-57-607/27/23 18:30403 161 1 2-Methylphenol(o-Cresol)ND ug/kg 07/30/23 12:03 95-48-707/27/23 18:30403 165 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/30/23 12:03 15831-10-407/27/23 18:30403 162 1 Naphthalene ND ug/kg 07/30/23 12:03 91-20-307/27/23 18:30403 137 1 2-Nitroaniline ND ug/kg 07/30/23 12:03 88-74-407/27/23 18:302010 330 1 3-Nitroaniline ND ug/kg 07/30/23 12:03 99-09-207/27/23 18:302010 316 1 4-Nitroaniline ND ug/kg 07/30/23 12:03 100-01-607/27/23 18:30805 306 1 Nitrobenzene ND ug/kg 07/30/23 12:03 98-95-307/27/23 18:30403 187 1 2-Nitrophenol ND ug/kg 07/30/23 12:03 88-75-507/27/23 18:30403 175 1 4-Nitrophenol ND ug/kg 07/30/23 12:03 100-02-7 v207/27/23 18:302010 779 1 N-Nitrosodimethylamine ND ug/kg 07/30/23 12:03 62-75-907/27/23 18:30403 135 1 N-Nitroso-di-n-propylamine ND ug/kg 07/30/23 12:03 621-64-707/27/23 18:30403 151 1 N-Nitrosodiphenylamine ND ug/kg 07/30/23 12:03 86-30-607/27/23 18:30403 143 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/30/23 12:03 108-60-107/27/23 18:30403 192 1 Pentachlorophenol ND ug/kg 07/30/23 12:03 87-86-5 v207/27/23 18:30805 394 1 Phenanthrene 258J ug/kg 07/30/23 12:03 85-01-807/27/23 18:30403 132 1 Phenol ND ug/kg 07/30/23 12:03 108-95-207/27/23 18:30403 179 1 Pyrene ND ug/kg 07/30/23 12:03 129-00-007/27/23 18:30403 164 1 Pyridine ND ug/kg 07/30/23 12:03 110-86-107/27/23 18:30403 127 1 1,2,4-Trichlorobenzene ND ug/kg 07/30/23 12:03 120-82-107/27/23 18:30403 159 1 2,4,5-Trichlorophenol ND ug/kg 07/30/23 12:03 95-95-407/27/23 18:30403 184 1 2,4,6-Trichlorophenol ND ug/kg 07/30/23 12:03 88-06-207/27/23 18:30403 166 1 Surrogates Nitrobenzene-d5 (S)57 %07/30/23 12:03 4165-60-007/27/23 18:3010-130 1 2-Fluorobiphenyl (S)57 %07/30/23 12:03 321-60-807/27/23 18:3010-130 1 Terphenyl-d14 (S)57 %07/30/23 12:03 1718-51-007/27/23 18:3010-130 1 Phenol-d6 (S)47 %07/30/23 12:03 13127-88-307/27/23 18:3010-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 36 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-6 (0-2)Lab ID: 92678743009 Collected: 07/18/23 12:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)45 %07/30/23 12:03 367-12-407/27/23 18:3010-130 1 2,4,6-Tribromophenol (S)53 %07/30/23 12:03 118-79-607/27/23 18:3010-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 07/25/23 19:25 67-64-107/25/23 14:48168 53.9 1 Benzene ND ug/kg 07/25/23 19:25 71-43-207/25/23 14:488.4 3.3 1 Bromobenzene ND ug/kg 07/25/23 19:25 108-86-107/25/23 14:488.4 2.7 1 Bromochloromethane ND ug/kg 07/25/23 19:25 74-97-507/25/23 14:488.4 2.5 1 Bromodichloromethane ND ug/kg 07/25/23 19:25 75-27-407/25/23 14:488.4 3.2 1 Bromoform ND ug/kg 07/25/23 19:25 75-25-207/25/23 14:488.4 3.0 1 Bromomethane ND ug/kg 07/25/23 19:25 74-83-9 IH07/25/23 14:4833.6 26.0 1 2-Butanone (MEK)ND ug/kg 07/25/23 19:25 78-93-307/25/23 14:48168 40.3 1 n-Butylbenzene ND ug/kg 07/25/23 19:25 104-51-807/25/23 14:488.4 5.3 1 sec-Butylbenzene ND ug/kg 07/25/23 19:25 135-98-807/25/23 14:488.4 3.7 1 tert-Butylbenzene ND ug/kg 07/25/23 19:25 98-06-607/25/23 14:488.4 3.0 1 Carbon tetrachloride ND ug/kg 07/25/23 19:25 56-23-507/25/23 14:488.4 3.1 1 Chlorobenzene ND ug/kg 07/25/23 19:25 108-90-707/25/23 14:488.4 4.8 1 Chloroethane ND ug/kg 07/25/23 19:25 75-00-307/25/23 14:4816.8 6.5 1 Chloroform ND ug/kg 07/25/23 19:25 67-66-307/25/23 14:488.4 7.0 1 Chloromethane ND ug/kg 07/25/23 19:25 74-87-307/25/23 14:4816.8 7.1 1 2-Chlorotoluene ND ug/kg 07/25/23 19:25 95-49-807/25/23 14:488.4 3.0 1 4-Chlorotoluene ND ug/kg 07/25/23 19:25 106-43-407/25/23 14:488.4 4.7 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/25/23 19:25 96-12-807/25/23 14:488.4 3.3 1 Dibromochloromethane ND ug/kg 07/25/23 19:25 124-48-107/25/23 14:488.4 4.7 1 1,2-Dibromoethane (EDB)ND ug/kg 07/25/23 19:25 106-93-407/25/23 14:488.4 3.7 1 Dibromomethane ND ug/kg 07/25/23 19:25 74-95-307/25/23 14:488.4 1.8 1 1,2-Dichlorobenzene ND ug/kg 07/25/23 19:25 95-50-107/25/23 14:488.4 3.0 1 1,3-Dichlorobenzene ND ug/kg 07/25/23 19:25 541-73-107/25/23 14:488.4 2.6 1 1,4-Dichlorobenzene ND ug/kg 07/25/23 19:25 106-46-707/25/23 14:488.4 2.2 1 Dichlorodifluoromethane ND ug/kg 07/25/23 19:25 75-71-807/25/23 14:4816.8 8.5 1 1,1-Dichloroethane ND ug/kg 07/25/23 19:25 75-34-307/25/23 14:488.4 3.5 1 1,2-Dichloroethane ND ug/kg 07/25/23 19:25 107-06-207/25/23 14:488.4 5.6 1 1,1-Dichloroethene ND ug/kg 07/25/23 19:25 75-35-407/25/23 14:488.4 3.5 1 cis-1,2-Dichloroethene ND ug/kg 07/25/23 19:25 156-59-207/25/23 14:488.4 2.9 1 trans-1,2-Dichloroethene ND ug/kg 07/25/23 19:25 156-60-507/25/23 14:488.4 7.1 1 1,2-Dichloropropane ND ug/kg 07/25/23 19:25 78-87-507/25/23 14:488.4 2.5 1 1,3-Dichloropropane ND ug/kg 07/25/23 19:25 142-28-907/25/23 14:488.4 2.6 1 2,2-Dichloropropane ND ug/kg 07/25/23 19:25 594-20-7 v207/25/23 14:488.4 6.4 1 1,1-Dichloropropene ND ug/kg 07/25/23 19:25 563-58-607/25/23 14:488.4 4.0 1 cis-1,3-Dichloropropene ND ug/kg 07/25/23 19:25 10061-01-507/25/23 14:488.4 2.3 1 trans-1,3-Dichloropropene ND ug/kg 07/25/23 19:25 10061-02-607/25/23 14:488.4 2.9 1 Diisopropyl ether ND ug/kg 07/25/23 19:25 108-20-307/25/23 14:488.4 2.3 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 37 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-6 (0-2)Lab ID: 92678743009 Collected: 07/18/23 12:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene ND ug/kg 07/25/23 19:25 100-41-407/25/23 14:488.4 3.9 1 Hexachloro-1,3-butadiene ND ug/kg 07/25/23 19:25 87-68-307/25/23 14:4816.8 13.7 1 2-Hexanone ND ug/kg 07/25/23 19:25 591-78-607/25/23 14:4884.0 8.1 1 Isopropylbenzene (Cumene)ND ug/kg 07/25/23 19:25 98-82-807/25/23 14:488.4 2.9 1 p-Isopropyltoluene ND ug/kg 07/25/23 19:25 99-87-607/25/23 14:488.4 4.1 1 Methylene Chloride ND ug/kg 07/25/23 19:25 75-09-207/25/23 14:4833.6 23.0 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/25/23 19:25 108-10-107/25/23 14:4884.0 8.1 1 Methyl-tert-butyl ether ND ug/kg 07/25/23 19:25 1634-04-4 v207/25/23 14:488.4 3.1 1 Naphthalene 9.7 ug/kg 07/25/23 19:25 91-20-307/25/23 14:488.4 4.4 1 n-Propylbenzene ND ug/kg 07/25/23 19:25 103-65-107/25/23 14:488.4 3.0 1 Styrene ND ug/kg 07/25/23 19:25 100-42-507/25/23 14:488.4 2.2 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/25/23 19:25 630-20-607/25/23 14:488.4 3.2 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/25/23 19:25 79-34-507/25/23 14:488.4 2.2 1 Tetrachloroethene ND ug/kg 07/25/23 19:25 127-18-407/25/23 14:488.4 2.7 1 Toluene 5.9J ug/kg 07/25/23 19:25 108-88-307/25/23 14:488.4 5.8 1 1,2,3-Trichlorobenzene ND ug/kg 07/25/23 19:25 87-61-607/25/23 14:488.4 6.8 1 1,2,4-Trichlorobenzene ND ug/kg 07/25/23 19:25 120-82-107/25/23 14:488.4 7.1 1 1,1,1-Trichloroethane ND ug/kg 07/25/23 19:25 71-55-607/25/23 14:488.4 4.4 1 1,1,2-Trichloroethane ND ug/kg 07/25/23 19:25 79-00-507/25/23 14:488.4 2.8 1 Trichloroethene ND ug/kg 07/25/23 19:25 79-01-607/25/23 14:488.4 6.8 1 Trichlorofluoromethane ND ug/kg 07/25/23 19:25 75-69-407/25/23 14:488.4 4.6 1 1,2,3-Trichloropropane ND ug/kg 07/25/23 19:25 96-18-407/25/23 14:488.4 4.2 1 1,2,4-Trimethylbenzene ND ug/kg 07/25/23 19:25 95-63-607/25/23 14:488.4 5.0 1 1,3,5-Trimethylbenzene ND ug/kg 07/25/23 19:25 108-67-807/25/23 14:488.4 2.8 1 Vinyl acetate ND ug/kg 07/25/23 19:25 108-05-407/25/23 14:4884.0 17.3 1 Vinyl chloride ND ug/kg 07/25/23 19:25 75-01-4 v207/25/23 14:4816.8 4.3 1 Xylene (Total)ND ug/kg 07/25/23 19:25 1330-20-707/25/23 14:4816.8 4.8 1 m&p-Xylene ND ug/kg 07/25/23 19:25 179601-23-107/25/23 14:4816.8 5.7 1 o-Xylene ND ug/kg 07/25/23 19:25 95-47-607/25/23 14:488.4 3.7 1 Surrogates Toluene-d8 (S)101 %07/25/23 19:25 2037-26-507/25/23 14:4870-130 1 4-Bromofluorobenzene (S)101 %07/25/23 19:25 460-00-407/25/23 14:4870-130 1 1,2-Dichloroethane-d4 (S)105 %07/25/23 19:25 17060-07-007/25/23 14:4870-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 17.0 %07/24/23 14:07 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 80.0 %07/27/23 12:4607/27/23 12:321 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 38 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-6 (0-2)Lab ID: 92678743009 Collected: 07/18/23 12:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.648J mg/kg 07/28/23 15:37 18540-29-9 J07/28/23 10:001.25 0.319 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 39 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-7 (0-2)Lab ID: 92678743010 Collected: 07/18/23 16:15 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: 3050B Pace National - Mt. Juliet Metals (ICPMS) 6020B Arsenic 9.14 mg/kg 08/01/23 15:56 7440-38-207/27/23 03:221.17 0.117 5 Barium 69.9 mg/kg 08/01/23 15:56 7440-39-307/27/23 03:222.93 0.178 5 Cadmium 0.170J mg/kg 08/01/23 15:56 7440-43-9 J07/27/23 03:221.17 0.100 5 Chromium 25.1 mg/kg 08/01/23 15:56 7440-47-307/27/23 03:225.85 0.346 5 Lead 45.4 mg/kg 08/01/23 15:56 7439-92-107/27/23 03:222.34 0.116 5 Selenium 1.21J mg/kg 08/01/23 15:56 7782-49-2 J07/27/23 03:222.93 0.211 5 Silver ND mg/kg 08/01/23 15:56 7440-22-407/27/23 03:220.585 0.101 5 Analytical Method: EPA 7471B Preparation Method: 7471A Pace National - Mt. Juliet Mercury 7471B Mercury 0.113 mg/kg 07/30/23 18:45 7439-97-607/28/23 10:460.0468 0.0211 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 07/30/23 13:26 83-32-907/27/23 18:30397 140 1 Acenaphthylene ND ug/kg 07/30/23 13:26 208-96-807/27/23 18:30397 140 1 Aniline ND ug/kg 07/30/23 13:26 62-53-307/27/23 18:30397 155 1 Anthracene 295J ug/kg 07/30/23 13:26 120-12-707/27/23 18:30397 130 1 Benzo(a)anthracene 901 ug/kg 07/30/23 13:26 56-55-307/27/23 18:30397 132 1 Benzo(a)pyrene 740 ug/kg 07/30/23 13:26 50-32-807/27/23 18:30397 137 1 Benzo(b)fluoranthene 1010 ug/kg 07/30/23 13:26 205-99-207/27/23 18:30397 132 1 Benzo(g,h,i)perylene 556 ug/kg 07/30/23 13:26 191-24-207/27/23 18:30397 154 1 Benzo(k)fluoranthene 353J ug/kg 07/30/23 13:26 207-08-907/27/23 18:30397 140 1 Benzoic Acid ND ug/kg 07/30/23 13:26 65-85-007/27/23 18:301980 853 1 Benzyl alcohol ND ug/kg 07/30/23 13:26 100-51-607/27/23 18:30794 301 1 4-Bromophenylphenyl ether ND ug/kg 07/30/23 13:26 101-55-307/27/23 18:30397 153 1 Butylbenzylphthalate ND ug/kg 07/30/23 13:26 85-68-707/27/23 18:30397 167 1 4-Chloro-3-methylphenol ND ug/kg 07/30/23 13:26 59-50-707/27/23 18:30794 279 1 4-Chloroaniline ND ug/kg 07/30/23 13:26 106-47-807/27/23 18:30794 311 1 bis(2-Chloroethoxy)methane ND ug/kg 07/30/23 13:26 111-91-107/27/23 18:30397 165 1 bis(2-Chloroethyl) ether ND ug/kg 07/30/23 13:26 111-44-407/27/23 18:30397 149 1 2-Chloronaphthalene ND ug/kg 07/30/23 13:26 91-58-707/27/23 18:30397 158 1 2-Chlorophenol ND ug/kg 07/30/23 13:26 95-57-807/27/23 18:30397 149 1 4-Chlorophenylphenyl ether ND ug/kg 07/30/23 13:26 7005-72-307/27/23 18:30397 148 1 Chrysene 915 ug/kg 07/30/23 13:26 218-01-907/27/23 18:30397 144 1 Dibenz(a,h)anthracene 157J ug/kg 07/30/23 13:26 53-70-307/27/23 18:30397 153 1 Dibenzofuran ND ug/kg 07/30/23 13:26 132-64-907/27/23 18:30397 143 1 1,2-Dichlorobenzene ND ug/kg 07/30/23 13:26 95-50-107/27/23 18:30397 143 1 1,3-Dichlorobenzene ND ug/kg 07/30/23 13:26 541-73-107/27/23 18:30397 141 1 1,4-Dichlorobenzene ND ug/kg 07/30/23 13:26 106-46-707/27/23 18:30397 152 1 3,3'-Dichlorobenzidine ND ug/kg 07/30/23 13:26 91-94-107/27/23 18:30794 268 1 2,4-Dichlorophenol ND ug/kg 07/30/23 13:26 120-83-207/27/23 18:30397 155 1 Diethylphthalate ND ug/kg 07/30/23 13:26 84-66-207/27/23 18:30397 146 1 2,4-Dimethylphenol ND ug/kg 07/30/23 13:26 105-67-9 v107/27/23 18:30397 165 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 40 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-7 (0-2)Lab ID: 92678743010 Collected: 07/18/23 16:15 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 07/30/23 13:26 131-11-307/27/23 18:30397 144 1 Di-n-butylphthalate ND ug/kg 07/30/23 13:26 84-74-207/27/23 18:30397 133 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/30/23 13:26 534-52-107/27/23 18:30794 370 1 2,4-Dinitrophenol ND ug/kg 07/30/23 13:26 51-28-507/27/23 18:301980 1230 1 2,4-Dinitrotoluene ND ug/kg 07/30/23 13:26 121-14-207/27/23 18:30397 153 1 2,6-Dinitrotoluene ND ug/kg 07/30/23 13:26 606-20-207/27/23 18:30397 146 1 Di-n-octylphthalate ND ug/kg 07/30/23 13:26 117-84-007/27/23 18:30397 156 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/30/23 13:26 117-81-707/27/23 18:30397 154 1 Fluoranthene 1740 ug/kg 07/30/23 13:26 206-44-007/27/23 18:30397 136 1 Fluorene ND ug/kg 07/30/23 13:26 86-73-707/27/23 18:30397 140 1 Hexachloro-1,3-butadiene ND ug/kg 07/30/23 13:26 87-68-307/27/23 18:30397 172 1 Hexachlorobenzene ND ug/kg 07/30/23 13:26 118-74-107/27/23 18:30397 155 1 Hexachlorocyclopentadiene ND ug/kg 07/30/23 13:26 77-47-4 v207/27/23 18:30397 227 1 Hexachloroethane ND ug/kg 07/30/23 13:26 67-72-107/27/23 18:30397 152 1 Indeno(1,2,3-cd)pyrene 485 ug/kg 07/30/23 13:26 193-39-507/27/23 18:30397 156 1 Isophorone ND ug/kg 07/30/23 13:26 78-59-107/27/23 18:30397 177 1 1-Methylnaphthalene ND ug/kg 07/30/23 13:26 90-12-007/27/23 18:30397 140 1 2-Methylnaphthalene ND ug/kg 07/30/23 13:26 91-57-607/27/23 18:30397 159 1 2-Methylphenol(o-Cresol)ND ug/kg 07/30/23 13:26 95-48-707/27/23 18:30397 162 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/30/23 13:26 15831-10-407/27/23 18:30397 160 1 Naphthalene ND ug/kg 07/30/23 13:26 91-20-307/27/23 18:30397 135 1 2-Nitroaniline ND ug/kg 07/30/23 13:26 88-74-407/27/23 18:301980 325 1 3-Nitroaniline ND ug/kg 07/30/23 13:26 99-09-207/27/23 18:301980 311 1 4-Nitroaniline ND ug/kg 07/30/23 13:26 100-01-607/27/23 18:30794 302 1 Nitrobenzene ND ug/kg 07/30/23 13:26 98-95-307/27/23 18:30397 184 1 2-Nitrophenol ND ug/kg 07/30/23 13:26 88-75-507/27/23 18:30397 172 1 4-Nitrophenol ND ug/kg 07/30/23 13:26 100-02-7 v207/27/23 18:301980 767 1 N-Nitrosodimethylamine ND ug/kg 07/30/23 13:26 62-75-907/27/23 18:30397 133 1 N-Nitroso-di-n-propylamine ND ug/kg 07/30/23 13:26 621-64-707/27/23 18:30397 149 1 N-Nitrosodiphenylamine ND ug/kg 07/30/23 13:26 86-30-607/27/23 18:30397 141 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/30/23 13:26 108-60-107/27/23 18:30397 189 1 Pentachlorophenol ND ug/kg 07/30/23 13:26 87-86-5 v207/27/23 18:30794 388 1 Phenanthrene 1170 ug/kg 07/30/23 13:26 85-01-807/27/23 18:30397 130 1 Phenol ND ug/kg 07/30/23 13:26 108-95-207/27/23 18:30397 177 1 Pyrene 1580 ug/kg 07/30/23 13:26 129-00-007/27/23 18:30397 161 1 Pyridine ND ug/kg 07/30/23 13:26 110-86-107/27/23 18:30397 125 1 1,2,4-Trichlorobenzene ND ug/kg 07/30/23 13:26 120-82-107/27/23 18:30397 156 1 2,4,5-Trichlorophenol ND ug/kg 07/30/23 13:26 95-95-407/27/23 18:30397 182 1 2,4,6-Trichlorophenol ND ug/kg 07/30/23 13:26 88-06-207/27/23 18:30397 164 1 Surrogates Nitrobenzene-d5 (S)48 %07/30/23 13:26 4165-60-007/27/23 18:3010-130 1 2-Fluorobiphenyl (S)50 %07/30/23 13:26 321-60-807/27/23 18:3010-130 1 Terphenyl-d14 (S)50 %07/30/23 13:26 1718-51-007/27/23 18:3010-130 1 Phenol-d6 (S)38 %07/30/23 13:26 13127-88-307/27/23 18:3010-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 41 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-7 (0-2)Lab ID: 92678743010 Collected: 07/18/23 16:15 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)38 %07/30/23 13:26 367-12-407/27/23 18:3010-130 1 2,4,6-Tribromophenol (S)49 %07/30/23 13:26 118-79-607/27/23 18:3010-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 07/25/23 19:44 67-64-107/25/23 18:31153 49.2 1 Benzene 4.4J ug/kg 07/25/23 19:44 71-43-207/25/23 18:317.7 3.0 1 Bromobenzene ND ug/kg 07/25/23 19:44 108-86-107/25/23 18:317.7 2.5 1 Bromochloromethane ND ug/kg 07/25/23 19:44 74-97-507/25/23 18:317.7 2.3 1 Bromodichloromethane ND ug/kg 07/25/23 19:44 75-27-407/25/23 18:317.7 3.0 1 Bromoform ND ug/kg 07/25/23 19:44 75-25-207/25/23 18:317.7 2.7 1 Bromomethane ND ug/kg 07/25/23 19:44 74-83-9 IH07/25/23 18:3130.6 23.7 1 2-Butanone (MEK)ND ug/kg 07/25/23 19:44 78-93-307/25/23 18:31153 36.8 1 n-Butylbenzene ND ug/kg 07/25/23 19:44 104-51-807/25/23 18:317.7 4.8 1 sec-Butylbenzene ND ug/kg 07/25/23 19:44 135-98-807/25/23 18:317.7 3.4 1 tert-Butylbenzene ND ug/kg 07/25/23 19:44 98-06-607/25/23 18:317.7 2.7 1 Carbon tetrachloride ND ug/kg 07/25/23 19:44 56-23-507/25/23 18:317.7 2.9 1 Chlorobenzene ND ug/kg 07/25/23 19:44 108-90-707/25/23 18:317.7 4.4 1 Chloroethane ND ug/kg 07/25/23 19:44 75-00-307/25/23 18:3115.3 5.9 1 Chloroform ND ug/kg 07/25/23 19:44 67-66-307/25/23 18:317.7 6.4 1 Chloromethane 7.0J ug/kg 07/25/23 19:44 74-87-307/25/23 18:3115.3 6.4 1 2-Chlorotoluene ND ug/kg 07/25/23 19:44 95-49-807/25/23 18:317.7 2.7 1 4-Chlorotoluene ND ug/kg 07/25/23 19:44 106-43-407/25/23 18:317.7 4.3 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/25/23 19:44 96-12-807/25/23 18:317.7 3.0 1 Dibromochloromethane ND ug/kg 07/25/23 19:44 124-48-107/25/23 18:317.7 4.3 1 1,2-Dibromoethane (EDB)ND ug/kg 07/25/23 19:44 106-93-407/25/23 18:317.7 3.4 1 Dibromomethane ND ug/kg 07/25/23 19:44 74-95-307/25/23 18:317.7 1.6 1 1,2-Dichlorobenzene ND ug/kg 07/25/23 19:44 95-50-107/25/23 18:317.7 2.8 1 1,3-Dichlorobenzene ND ug/kg 07/25/23 19:44 541-73-107/25/23 18:317.7 2.4 1 1,4-Dichlorobenzene ND ug/kg 07/25/23 19:44 106-46-707/25/23 18:317.7 2.0 1 Dichlorodifluoromethane ND ug/kg 07/25/23 19:44 75-71-8 M107/25/23 18:3115.3 7.8 1 1,1-Dichloroethane ND ug/kg 07/25/23 19:44 75-34-307/25/23 18:317.7 3.2 1 1,2-Dichloroethane ND ug/kg 07/25/23 19:44 107-06-207/25/23 18:317.7 5.1 1 1,1-Dichloroethene ND ug/kg 07/25/23 19:44 75-35-407/25/23 18:317.7 3.2 1 cis-1,2-Dichloroethene ND ug/kg 07/25/23 19:44 156-59-207/25/23 18:317.7 2.6 1 trans-1,2-Dichloroethene ND ug/kg 07/25/23 19:44 156-60-507/25/23 18:317.7 6.5 1 1,2-Dichloropropane ND ug/kg 07/25/23 19:44 78-87-507/25/23 18:317.7 2.3 1 1,3-Dichloropropane ND ug/kg 07/25/23 19:44 142-28-907/25/23 18:317.7 2.4 1 2,2-Dichloropropane ND ug/kg 07/25/23 19:44 594-20-7 v207/25/23 18:317.7 5.8 1 1,1-Dichloropropene ND ug/kg 07/25/23 19:44 563-58-607/25/23 18:317.7 3.7 1 cis-1,3-Dichloropropene ND ug/kg 07/25/23 19:44 10061-01-507/25/23 18:317.7 2.1 1 trans-1,3-Dichloropropene ND ug/kg 07/25/23 19:44 10061-02-607/25/23 18:317.7 2.6 1 Diisopropyl ether ND ug/kg 07/25/23 19:44 108-20-307/25/23 18:317.7 2.1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 42 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-7 (0-2)Lab ID: 92678743010 Collected: 07/18/23 16:15 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene 15.9 ug/kg 07/25/23 19:44 100-41-407/25/23 18:317.7 3.6 1 Hexachloro-1,3-butadiene ND ug/kg 07/25/23 19:44 87-68-307/25/23 18:3115.3 12.5 1 2-Hexanone ND ug/kg 07/25/23 19:44 591-78-607/25/23 18:3176.6 7.4 1 Isopropylbenzene (Cumene)4.8J ug/kg 07/25/23 19:44 98-82-807/25/23 18:317.7 2.6 1 p-Isopropyltoluene ND ug/kg 07/25/23 19:44 99-87-607/25/23 18:317.7 3.8 1 Methylene Chloride ND ug/kg 07/25/23 19:44 75-09-207/25/23 18:3130.6 21.0 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/25/23 19:44 108-10-107/25/23 18:3176.6 7.4 1 Methyl-tert-butyl ether ND ug/kg 07/25/23 19:44 1634-04-4 v207/25/23 18:317.7 2.9 1 Naphthalene 47.2 ug/kg 07/25/23 19:44 91-20-307/25/23 18:317.7 4.0 1 n-Propylbenzene ND ug/kg 07/25/23 19:44 103-65-107/25/23 18:317.7 2.7 1 Styrene ND ug/kg 07/25/23 19:44 100-42-507/25/23 18:317.7 2.0 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/25/23 19:44 630-20-607/25/23 18:317.7 2.9 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/25/23 19:44 79-34-507/25/23 18:317.7 2.0 1 Tetrachloroethene ND ug/kg 07/25/23 19:44 127-18-407/25/23 18:317.7 2.4 1 Toluene 26.2 ug/kg 07/25/23 19:44 108-88-307/25/23 18:317.7 5.3 1 1,2,3-Trichlorobenzene ND ug/kg 07/25/23 19:44 87-61-607/25/23 18:317.7 6.2 1 1,2,4-Trichlorobenzene ND ug/kg 07/25/23 19:44 120-82-107/25/23 18:317.7 6.4 1 1,1,1-Trichloroethane ND ug/kg 07/25/23 19:44 71-55-607/25/23 18:317.7 4.0 1 1,1,2-Trichloroethane ND ug/kg 07/25/23 19:44 79-00-507/25/23 18:317.7 2.5 1 Trichloroethene ND ug/kg 07/25/23 19:44 79-01-607/25/23 18:317.7 6.2 1 Trichlorofluoromethane ND ug/kg 07/25/23 19:44 75-69-407/25/23 18:317.7 4.2 1 1,2,3-Trichloropropane ND ug/kg 07/25/23 19:44 96-18-407/25/23 18:317.7 3.9 1 1,2,4-Trimethylbenzene 19.3 ug/kg 07/25/23 19:44 95-63-607/25/23 18:317.7 4.5 1 1,3,5-Trimethylbenzene ND ug/kg 07/25/23 19:44 108-67-807/25/23 18:317.7 2.6 1 Vinyl acetate ND ug/kg 07/25/23 19:44 108-05-407/25/23 18:3176.6 15.8 1 Vinyl chloride ND ug/kg 07/25/23 19:44 75-01-4 v207/25/23 18:3115.3 3.9 1 Xylene (Total)105 ug/kg 07/25/23 19:44 1330-20-707/25/23 18:3115.3 4.4 1 m&p-Xylene 62.2 ug/kg 07/25/23 19:44 179601-23-107/25/23 18:3115.3 5.2 1 o-Xylene 42.4 ug/kg 07/25/23 19:44 95-47-607/25/23 18:317.7 3.4 1 Surrogates Toluene-d8 (S)101 %07/25/23 19:44 2037-26-507/25/23 18:3170-130 1 4-Bromofluorobenzene (S)103 %07/25/23 19:44 460-00-407/25/23 18:3170-130 1 1,2-Dichloroethane-d4 (S)108 %07/25/23 19:44 17060-07-007/25/23 18:3170-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 15.7 %07/24/23 14:07 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 85.5 %07/27/23 12:4607/27/23 12:321 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 43 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: CS-7 (0-2)Lab ID: 92678743010 Collected: 07/18/23 16:15 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.953J mg/kg 07/28/23 15:52 18540-29-9 J07/28/23 10:001.17 0.298 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 44 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-7 Lab ID: 92678743011 Collected: 07/20/23 15:40 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3010A Pace Analytical Services - Asheville 6020 MET ICPMS Arsenic 0.74J ug/L 07/27/23 02:12 7440-38-207/26/23 11:461.0 0.087 1 Barium 53.3 ug/L 07/27/23 02:12 7440-39-307/26/23 11:461.0 0.21 1 Cadmium 0.37 ug/L 07/27/23 02:12 7440-43-907/26/23 11:460.20 0.060 1 Chromium 0.62J ug/L 07/27/23 02:12 7440-47-307/26/23 11:461.0 0.50 1 Lead ND ug/L 07/27/23 02:12 7439-92-107/26/23 11:461.0 0.077 1 Selenium 2.2 ug/L 07/27/23 02:12 7782-49-207/26/23 11:462.0 0.072 1 Silver ND ug/L 07/27/23 02:12 7440-22-407/26/23 11:460.40 0.070 1 Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services - Asheville 7470 Mercury Mercury ND ug/L 07/31/23 14:14 7439-97-607/31/23 09:370.20 0.12 1 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Acenaphthene ND ug/L 07/25/23 21:44 83-32-907/25/23 11:228.7 1.7 1 Acenaphthylene ND ug/L 07/25/23 21:44 208-96-807/25/23 11:228.7 1.7 1 Aniline ND ug/L 07/25/23 21:44 62-53-307/25/23 11:228.7 1.4 1 Anthracene ND ug/L 07/25/23 21:44 120-12-707/25/23 11:228.7 2.0 1 Benzo(a)anthracene ND ug/L 07/25/23 21:44 56-55-307/25/23 11:228.7 2.3 1 Benzo(a)pyrene ND ug/L 07/25/23 21:44 50-32-807/25/23 11:228.7 2.4 1 Benzo(b)fluoranthene ND ug/L 07/25/23 21:44 205-99-207/25/23 11:228.7 2.3 1 Benzo(g,h,i)perylene ND ug/L 07/25/23 21:44 191-24-207/25/23 11:228.7 2.5 1 Benzo(k)fluoranthene ND ug/L 07/25/23 21:44 207-08-907/25/23 11:228.7 2.4 1 Benzoic Acid 41.2J ug/L 07/25/23 21:44 65-85-0 C707/25/23 11:2243.5 19.1 1 Benzyl alcohol ND ug/L 07/25/23 21:44 100-51-607/25/23 11:2217.4 2.5 1 4-Bromophenylphenyl ether ND ug/L 07/25/23 21:44 101-55-307/25/23 11:228.7 1.5 1 Butylbenzylphthalate ND ug/L 07/25/23 21:44 85-68-707/25/23 11:228.7 2.7 1 4-Chloro-3-methylphenol ND ug/L 07/25/23 21:44 59-50-707/25/23 11:228.7 2.9 1 4-Chloroaniline ND ug/L 07/25/23 21:44 106-47-807/25/23 11:2217.4 3.2 1 bis(2-Chloroethoxy)methane ND ug/L 07/25/23 21:44 111-91-107/25/23 11:228.7 1.6 1 bis(2-Chloroethyl) ether ND ug/L 07/25/23 21:44 111-44-407/25/23 11:228.7 1.7 1 2-Chloronaphthalene ND ug/L 07/25/23 21:44 91-58-707/25/23 11:228.7 1.5 1 2-Chlorophenol ND ug/L 07/25/23 21:44 95-57-807/25/23 11:228.7 1.0 1 4-Chlorophenylphenyl ether ND ug/L 07/25/23 21:44 7005-72-307/25/23 11:228.7 1.7 1 Chrysene ND ug/L 07/25/23 21:44 218-01-907/25/23 11:228.7 2.4 1 Dibenz(a,h)anthracene ND ug/L 07/25/23 21:44 53-70-307/25/23 11:228.7 2.6 1 Dibenzofuran ND ug/L 07/25/23 21:44 132-64-907/25/23 11:228.7 1.8 1 1,2-Dichlorobenzene ND ug/L 07/25/23 21:44 95-50-107/25/23 11:228.7 1.6 1 1,3-Dichlorobenzene ND ug/L 07/25/23 21:44 541-73-107/25/23 11:228.7 1.4 1 1,4-Dichlorobenzene ND ug/L 07/25/23 21:44 106-46-707/25/23 11:228.7 1.5 1 3,3'-Dichlorobenzidine ND ug/L 07/25/23 21:44 91-94-107/25/23 11:2217.4 7.1 1 2,4-Dichlorophenol ND ug/L 07/25/23 21:44 120-83-207/25/23 11:228.7 1.2 1 Diethylphthalate ND ug/L 07/25/23 21:44 84-66-207/25/23 11:228.7 1.8 1 2,4-Dimethylphenol ND ug/L 07/25/23 21:44 105-67-9 v107/25/23 11:228.7 1.5 1 Dimethylphthalate ND ug/L 07/25/23 21:44 131-11-307/25/23 11:228.7 1.9 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 45 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-7 Lab ID: 92678743011 Collected: 07/20/23 15:40 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Di-n-butylphthalate ND ug/L 07/25/23 21:44 84-74-207/25/23 11:228.7 1.9 1 4,6-Dinitro-2-methylphenol ND ug/L 07/25/23 21:44 534-52-107/25/23 11:2217.4 6.8 1 2,4-Dinitrophenol ND ug/L 07/25/23 21:44 51-28-507/25/23 11:2243.5 22.6 1 2,4-Dinitrotoluene ND ug/L 07/25/23 21:44 121-14-207/25/23 11:228.7 1.4 1 2,6-Dinitrotoluene ND ug/L 07/25/23 21:44 606-20-207/25/23 11:228.7 1.5 1 Di-n-octylphthalate ND ug/L 07/25/23 21:44 117-84-007/25/23 11:228.7 3.4 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/25/23 21:44 117-81-707/25/23 11:225.2 3.2 1 Fluoranthene ND ug/L 07/25/23 21:44 206-44-007/25/23 11:228.7 1.9 1 Fluorene ND ug/L 07/25/23 21:44 86-73-707/25/23 11:228.7 1.8 1 Hexachloro-1,3-butadiene ND ug/L 07/25/23 21:44 87-68-307/25/23 11:228.7 1.5 1 Hexachlorobenzene ND ug/L 07/25/23 21:44 118-74-107/25/23 11:228.7 1.9 1 Hexachlorocyclopentadiene ND ug/L 07/25/23 21:44 77-47-407/25/23 11:228.7 1.4 1 Hexachloroethane ND ug/L 07/25/23 21:44 67-72-107/25/23 11:228.7 1.2 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/25/23 21:44 193-39-507/25/23 11:228.7 2.5 1 Isophorone ND ug/L 07/25/23 21:44 78-59-107/25/23 11:228.7 1.4 1 1-Methylnaphthalene ND ug/L 07/25/23 21:44 90-12-007/25/23 11:228.7 1.8 1 2-Methylnaphthalene ND ug/L 07/25/23 21:44 91-57-607/25/23 11:228.7 1.6 1 2-Methylphenol(o-Cresol)ND ug/L 07/25/23 21:44 95-48-707/25/23 11:228.7 1.6 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/25/23 21:44 15831-10-407/25/23 11:228.7 1.1 1 Naphthalene ND ug/L 07/25/23 21:44 91-20-307/25/23 11:228.7 1.8 1 2-Nitroaniline ND ug/L 07/25/23 21:44 88-74-407/25/23 11:2217.4 2.6 1 3-Nitroaniline ND ug/L 07/25/23 21:44 99-09-207/25/23 11:2217.4 3.3 1 4-Nitroaniline ND ug/L 07/25/23 21:44 100-01-607/25/23 11:2217.4 4.4 1 Nitrobenzene ND ug/L 07/25/23 21:44 98-95-307/25/23 11:228.7 1.6 1 2-Nitrophenol ND ug/L 07/25/23 21:44 88-75-507/25/23 11:228.7 1.2 1 4-Nitrophenol ND ug/L 07/25/23 21:44 100-02-707/25/23 11:2243.5 5.7 1 N-Nitrosodimethylamine ND ug/L 07/25/23 21:44 62-75-9 v107/25/23 11:228.7 1.6 1 N-Nitroso-di-n-propylamine ND ug/L 07/25/23 21:44 621-64-707/25/23 11:228.7 1.2 1 N-Nitrosodiphenylamine ND ug/L 07/25/23 21:44 86-30-607/25/23 11:228.7 2.6 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/25/23 21:44 108-60-1 v107/25/23 11:228.7 1.0 1 Pentachlorophenol ND ug/L 07/25/23 21:44 87-86-507/25/23 11:2217.4 3.3 1 Phenanthrene ND ug/L 07/25/23 21:44 85-01-807/25/23 11:228.7 1.7 1 Phenol ND ug/L 07/25/23 21:44 108-95-207/25/23 11:228.7 1.2 1 Pyrene ND ug/L 07/25/23 21:44 129-00-007/25/23 11:228.7 1.9 1 1,2,4-Trichlorobenzene ND ug/L 07/25/23 21:44 120-82-107/25/23 11:228.7 1.5 1 2,4,5-Trichlorophenol ND ug/L 07/25/23 21:44 95-95-407/25/23 11:228.7 1.2 1 2,4,6-Trichlorophenol ND ug/L 07/25/23 21:44 88-06-207/25/23 11:228.7 1.3 1 Surrogates Nitrobenzene-d5 (S)52 %07/25/23 21:44 4165-60-007/25/23 11:2210-138 1 2-Fluorobiphenyl (S)38 %07/25/23 21:44 321-60-807/25/23 11:2210-130 1 Terphenyl-d14 (S)114 %07/25/23 21:44 1718-51-007/25/23 11:2219-191 1 Phenol-d6 (S)20 %07/25/23 21:44 13127-88-307/25/23 11:2210-130 1 2-Fluorophenol (S)34 %07/25/23 21:44 367-12-407/25/23 11:2210-130 1 2,4,6-Tribromophenol (S)97 %07/25/23 21:44 118-79-607/25/23 11:2210-164 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 46 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-7 Lab ID: 92678743011 Collected: 07/20/23 15:40 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level Acetone ND ug/L 07/27/23 07:12 67-64-162.5 12.8 2.5 Benzene ND ug/L 07/27/23 07:12 71-43-22.5 0.86 2.5 Bromobenzene ND ug/L 07/27/23 07:12 108-86-12.5 0.72 2.5 Bromochloromethane ND ug/L 07/27/23 07:12 74-97-52.5 1.2 2.5 Bromodichloromethane ND ug/L 07/27/23 07:12 75-27-42.5 0.77 2.5 Bromoform ND ug/L 07/27/23 07:12 75-25-22.5 0.85 2.5 Bromomethane ND ug/L 07/27/23 07:12 74-83-95.0 4.2 2.5 2-Butanone (MEK)ND ug/L 07/27/23 07:12 78-93-312.5 9.9 2.5 Carbon tetrachloride ND ug/L 07/27/23 07:12 56-23-52.5 0.83 2.5 Chlorobenzene ND ug/L 07/27/23 07:12 108-90-72.5 0.71 2.5 Chloroethane ND ug/L 07/27/23 07:12 75-00-32.5 1.6 2.5 Chloroform ND ug/L 07/27/23 07:12 67-66-32.5 1.1 2.5 Chloromethane ND ug/L 07/27/23 07:12 74-87-32.5 1.4 2.5 2-Chlorotoluene ND ug/L 07/27/23 07:12 95-49-82.5 0.80 2.5 4-Chlorotoluene ND ug/L 07/27/23 07:12 106-43-42.5 0.81 2.5 1,2-Dibromo-3-chloropropane ND ug/L 07/27/23 07:12 96-12-85.0 0.85 2.5 Dibromochloromethane ND ug/L 07/27/23 07:12 124-48-12.5 0.90 2.5 1,2-Dibromoethane (EDB)ND ug/L 07/27/23 07:12 106-93-42.5 0.68 2.5 Dibromomethane ND ug/L 07/27/23 07:12 74-95-32.5 0.98 2.5 1,2-Dichlorobenzene ND ug/L 07/27/23 07:12 95-50-12.5 0.85 2.5 1,3-Dichlorobenzene ND ug/L 07/27/23 07:12 541-73-12.5 0.85 2.5 1,4-Dichlorobenzene ND ug/L 07/27/23 07:12 106-46-72.5 0.83 2.5 Dichlorodifluoromethane ND ug/L 07/27/23 07:12 75-71-82.5 0.86 2.5 1,1-Dichloroethane ND ug/L 07/27/23 07:12 75-34-32.5 0.92 2.5 1,2-Dichloroethane ND ug/L 07/27/23 07:12 107-06-22.5 0.80 2.5 1,1-Dichloroethene ND ug/L 07/27/23 07:12 75-35-42.5 0.87 2.5 cis-1,2-Dichloroethene ND ug/L 07/27/23 07:12 156-59-22.5 0.96 2.5 trans-1,2-Dichloroethene ND ug/L 07/27/23 07:12 156-60-52.5 0.99 2.5 1,2-Dichloropropane ND ug/L 07/27/23 07:12 78-87-52.5 0.89 2.5 1,3-Dichloropropane ND ug/L 07/27/23 07:12 142-28-92.5 0.71 2.5 2,2-Dichloropropane ND ug/L 07/27/23 07:12 594-20-72.5 0.97 2.5 1,1-Dichloropropene ND ug/L 07/27/23 07:12 563-58-62.5 1.1 2.5 cis-1,3-Dichloropropene ND ug/L 07/27/23 07:12 10061-01-52.5 0.91 2.5 trans-1,3-Dichloropropene ND ug/L 07/27/23 07:12 10061-02-62.5 0.91 2.5 Diisopropyl ether ND ug/L 07/27/23 07:12 108-20-32.5 0.77 2.5 Ethylbenzene ND ug/L 07/27/23 07:12 100-41-42.5 0.76 2.5 Hexachloro-1,3-butadiene ND ug/L 07/27/23 07:12 87-68-35.0 3.8 2.5 2-Hexanone ND ug/L 07/27/23 07:12 591-78-612.5 1.2 2.5 p-Isopropyltoluene ND ug/L 07/27/23 07:12 99-87-62.5 1.0 2.5 Methylene Chloride ND ug/L 07/27/23 07:12 75-09-212.5 4.9 2.5 4-Methyl-2-pentanone (MIBK)ND ug/L 07/27/23 07:12 108-10-112.5 6.8 2.5 Methyl-tert-butyl ether ND ug/L 07/27/23 07:12 1634-04-42.5 1.1 2.5 Naphthalene ND ug/L 07/27/23 07:12 91-20-32.5 1.6 2.5 Styrene ND ug/L 07/27/23 07:12 100-42-52.5 0.73 2.5 1,1,1,2-Tetrachloroethane ND ug/L 07/27/23 07:12 630-20-62.5 0.78 2.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 47 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-7 Lab ID: 92678743011 Collected: 07/20/23 15:40 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level 1,1,2,2-Tetrachloroethane ND ug/L 07/27/23 07:12 79-34-52.5 0.56 2.5 Tetrachloroethene 307 ug/L 07/27/23 07:12 127-18-42.5 0.73 2.5 Toluene ND ug/L 07/27/23 07:12 108-88-32.5 0.60 2.5 1,2,3-Trichlorobenzene ND ug/L 07/27/23 07:12 87-61-62.5 2.0 2.5 1,2,4-Trichlorobenzene ND ug/L 07/27/23 07:12 120-82-12.5 1.6 2.5 1,1,1-Trichloroethane ND ug/L 07/27/23 07:12 71-55-62.5 0.83 2.5 1,1,2-Trichloroethane ND ug/L 07/27/23 07:12 79-00-52.5 0.81 2.5 Trichloroethene ND ug/L 07/27/23 07:12 79-01-62.5 0.96 2.5 Trichlorofluoromethane ND ug/L 07/27/23 07:12 75-69-42.5 0.74 2.5 1,2,3-Trichloropropane ND ug/L 07/27/23 07:12 96-18-42.5 0.65 2.5 Vinyl acetate ND ug/L 07/27/23 07:12 108-05-45.0 3.3 2.5 Vinyl chloride ND ug/L 07/27/23 07:12 75-01-42.5 0.96 2.5 Xylene (Total)ND ug/L 07/27/23 07:12 1330-20-72.5 0.84 2.5 m&p-Xylene ND ug/L 07/27/23 07:12 179601-23-15.0 1.8 2.5 o-Xylene ND ug/L 07/27/23 07:12 95-47-62.5 0.84 2.5 Surrogates 4-Bromofluorobenzene (S)99 %07/27/23 07:12 460-00-470-130 2.5 1,2-Dichloroethane-d4 (S)102 %07/27/23 07:12 17060-07-070-130 2.5 Toluene-d8 (S)98 %07/27/23 07:12 2037-26-570-130 2.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 48 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-8 Lab ID: 92678743012 Collected: 07/20/23 16:45 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3010A Pace Analytical Services - Asheville 6020 MET ICPMS Arsenic 0.17J ug/L 07/27/23 02:17 7440-38-207/26/23 11:461.0 0.087 1 Barium 61.1 ug/L 07/27/23 02:17 7440-39-307/26/23 11:461.0 0.21 1 Cadmium 0.080J ug/L 07/27/23 02:17 7440-43-907/26/23 11:460.20 0.060 1 Chromium ND ug/L 07/27/23 02:17 7440-47-307/26/23 11:461.0 0.50 1 Lead ND ug/L 07/27/23 02:17 7439-92-107/26/23 11:461.0 0.077 1 Selenium 0.86J ug/L 07/27/23 02:17 7782-49-207/26/23 11:462.0 0.072 1 Silver ND ug/L 07/27/23 02:17 7440-22-407/26/23 11:460.40 0.070 1 Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services - Asheville 7470 Mercury Mercury ND ug/L 07/31/23 14:21 7439-97-607/31/23 09:370.20 0.12 1 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Acenaphthene ND ug/L 07/25/23 22:10 83-32-907/25/23 11:2210.0 2.0 1 Acenaphthylene ND ug/L 07/25/23 22:10 208-96-807/25/23 11:2210.0 2.0 1 Aniline ND ug/L 07/25/23 22:10 62-53-307/25/23 11:2210.0 1.6 1 Anthracene ND ug/L 07/25/23 22:10 120-12-707/25/23 11:2210.0 2.3 1 Benzo(a)anthracene ND ug/L 07/25/23 22:10 56-55-307/25/23 11:2210.0 2.7 1 Benzo(a)pyrene ND ug/L 07/25/23 22:10 50-32-807/25/23 11:2210.0 2.8 1 Benzo(b)fluoranthene ND ug/L 07/25/23 22:10 205-99-207/25/23 11:2210.0 2.6 1 Benzo(g,h,i)perylene ND ug/L 07/25/23 22:10 191-24-207/25/23 11:2210.0 2.8 1 Benzo(k)fluoranthene ND ug/L 07/25/23 22:10 207-08-907/25/23 11:2210.0 2.7 1 Benzoic Acid 47.3J ug/L 07/25/23 22:10 65-85-0 C707/25/23 11:2250.0 22.0 1 Benzyl alcohol ND ug/L 07/25/23 22:10 100-51-607/25/23 11:2220.0 2.9 1 4-Bromophenylphenyl ether ND ug/L 07/25/23 22:10 101-55-307/25/23 11:2210.0 1.8 1 Butylbenzylphthalate ND ug/L 07/25/23 22:10 85-68-707/25/23 11:2210.0 3.1 1 4-Chloro-3-methylphenol ND ug/L 07/25/23 22:10 59-50-707/25/23 11:2210.0 3.3 1 4-Chloroaniline ND ug/L 07/25/23 22:10 106-47-807/25/23 11:2220.0 3.6 1 bis(2-Chloroethoxy)methane ND ug/L 07/25/23 22:10 111-91-107/25/23 11:2210.0 1.8 1 bis(2-Chloroethyl) ether ND ug/L 07/25/23 22:10 111-44-407/25/23 11:2210.0 1.9 1 2-Chloronaphthalene ND ug/L 07/25/23 22:10 91-58-707/25/23 11:2210.0 1.7 1 2-Chlorophenol ND ug/L 07/25/23 22:10 95-57-807/25/23 11:2210.0 1.2 1 4-Chlorophenylphenyl ether ND ug/L 07/25/23 22:10 7005-72-307/25/23 11:2210.0 2.0 1 Chrysene ND ug/L 07/25/23 22:10 218-01-907/25/23 11:2210.0 2.8 1 Dibenz(a,h)anthracene ND ug/L 07/25/23 22:10 53-70-307/25/23 11:2210.0 3.0 1 Dibenzofuran ND ug/L 07/25/23 22:10 132-64-907/25/23 11:2210.0 2.1 1 1,2-Dichlorobenzene ND ug/L 07/25/23 22:10 95-50-107/25/23 11:2210.0 1.8 1 1,3-Dichlorobenzene ND ug/L 07/25/23 22:10 541-73-107/25/23 11:2210.0 1.6 1 1,4-Dichlorobenzene ND ug/L 07/25/23 22:10 106-46-707/25/23 11:2210.0 1.7 1 3,3'-Dichlorobenzidine ND ug/L 07/25/23 22:10 91-94-107/25/23 11:2220.0 8.1 1 2,4-Dichlorophenol ND ug/L 07/25/23 22:10 120-83-207/25/23 11:2210.0 1.4 1 Diethylphthalate ND ug/L 07/25/23 22:10 84-66-207/25/23 11:2210.0 2.0 1 2,4-Dimethylphenol ND ug/L 07/25/23 22:10 105-67-9 v107/25/23 11:2210.0 1.7 1 Dimethylphthalate ND ug/L 07/25/23 22:10 131-11-307/25/23 11:2210.0 2.1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 49 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-8 Lab ID: 92678743012 Collected: 07/20/23 16:45 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Di-n-butylphthalate ND ug/L 07/25/23 22:10 84-74-207/25/23 11:2210.0 2.2 1 4,6-Dinitro-2-methylphenol ND ug/L 07/25/23 22:10 534-52-107/25/23 11:2220.0 7.8 1 2,4-Dinitrophenol ND ug/L 07/25/23 22:10 51-28-507/25/23 11:2250.0 26.0 1 2,4-Dinitrotoluene ND ug/L 07/25/23 22:10 121-14-207/25/23 11:2210.0 1.6 1 2,6-Dinitrotoluene ND ug/L 07/25/23 22:10 606-20-207/25/23 11:2210.0 1.7 1 Di-n-octylphthalate ND ug/L 07/25/23 22:10 117-84-007/25/23 11:2210.0 3.9 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/25/23 22:10 117-81-707/25/23 11:226.0 3.7 1 Fluoranthene ND ug/L 07/25/23 22:10 206-44-007/25/23 11:2210.0 2.2 1 Fluorene ND ug/L 07/25/23 22:10 86-73-707/25/23 11:2210.0 2.1 1 Hexachloro-1,3-butadiene ND ug/L 07/25/23 22:10 87-68-307/25/23 11:2210.0 1.8 1 Hexachlorobenzene ND ug/L 07/25/23 22:10 118-74-107/25/23 11:2210.0 2.2 1 Hexachlorocyclopentadiene ND ug/L 07/25/23 22:10 77-47-407/25/23 11:2210.0 1.6 1 Hexachloroethane ND ug/L 07/25/23 22:10 67-72-107/25/23 11:2210.0 1.4 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/25/23 22:10 193-39-507/25/23 11:2210.0 2.9 1 Isophorone ND ug/L 07/25/23 22:10 78-59-107/25/23 11:2210.0 1.7 1 1-Methylnaphthalene ND ug/L 07/25/23 22:10 90-12-007/25/23 11:2210.0 2.0 1 2-Methylnaphthalene ND ug/L 07/25/23 22:10 91-57-607/25/23 11:2210.0 1.9 1 2-Methylphenol(o-Cresol)ND ug/L 07/25/23 22:10 95-48-707/25/23 11:2210.0 1.9 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/25/23 22:10 15831-10-407/25/23 11:2210.0 1.2 1 Naphthalene ND ug/L 07/25/23 22:10 91-20-307/25/23 11:2210.0 2.1 1 2-Nitroaniline ND ug/L 07/25/23 22:10 88-74-407/25/23 11:2220.0 3.0 1 3-Nitroaniline ND ug/L 07/25/23 22:10 99-09-207/25/23 11:2220.0 3.8 1 4-Nitroaniline ND ug/L 07/25/23 22:10 100-01-607/25/23 11:2220.0 5.1 1 Nitrobenzene ND ug/L 07/25/23 22:10 98-95-307/25/23 11:2210.0 1.9 1 2-Nitrophenol ND ug/L 07/25/23 22:10 88-75-507/25/23 11:2210.0 1.4 1 4-Nitrophenol ND ug/L 07/25/23 22:10 100-02-707/25/23 11:2250.0 6.6 1 N-Nitrosodimethylamine ND ug/L 07/25/23 22:10 62-75-9 v107/25/23 11:2210.0 1.9 1 N-Nitroso-di-n-propylamine ND ug/L 07/25/23 22:10 621-64-707/25/23 11:2210.0 1.3 1 N-Nitrosodiphenylamine ND ug/L 07/25/23 22:10 86-30-607/25/23 11:2210.0 3.0 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/25/23 22:10 108-60-1 v107/25/23 11:2210.0 1.2 1 Pentachlorophenol ND ug/L 07/25/23 22:10 87-86-507/25/23 11:2220.0 3.8 1 Phenanthrene ND ug/L 07/25/23 22:10 85-01-807/25/23 11:2210.0 2.0 1 Phenol ND ug/L 07/25/23 22:10 108-95-207/25/23 11:2210.0 1.4 1 Pyrene ND ug/L 07/25/23 22:10 129-00-007/25/23 11:2210.0 2.2 1 1,2,4-Trichlorobenzene ND ug/L 07/25/23 22:10 120-82-107/25/23 11:2210.0 1.7 1 2,4,5-Trichlorophenol ND ug/L 07/25/23 22:10 95-95-407/25/23 11:2210.0 1.4 1 2,4,6-Trichlorophenol ND ug/L 07/25/23 22:10 88-06-207/25/23 11:2210.0 1.6 1 Surrogates Nitrobenzene-d5 (S)97 %07/25/23 22:10 4165-60-007/25/23 11:2210-138 1 2-Fluorobiphenyl (S)75 %07/25/23 22:10 321-60-807/25/23 11:2210-130 1 Terphenyl-d14 (S)123 %07/25/23 22:10 1718-51-007/25/23 11:2219-191 1 Phenol-d6 (S)41 %07/25/23 22:10 13127-88-307/25/23 11:2210-130 1 2-Fluorophenol (S)58 %07/25/23 22:10 367-12-407/25/23 11:2210-130 1 2,4,6-Tribromophenol (S)114 %07/25/23 22:10 118-79-607/25/23 11:2210-164 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 50 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-8 Lab ID: 92678743012 Collected: 07/20/23 16:45 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level Acetone ND ug/L 07/27/23 06:00 67-64-125.0 5.1 1 Benzene ND ug/L 07/27/23 06:00 71-43-21.0 0.34 1 Bromobenzene ND ug/L 07/27/23 06:00 108-86-11.0 0.29 1 Bromochloromethane ND ug/L 07/27/23 06:00 74-97-51.0 0.47 1 Bromodichloromethane ND ug/L 07/27/23 06:00 75-27-41.0 0.31 1 Bromoform ND ug/L 07/27/23 06:00 75-25-21.0 0.34 1 Bromomethane ND ug/L 07/27/23 06:00 74-83-92.0 1.7 1 2-Butanone (MEK)ND ug/L 07/27/23 06:00 78-93-35.0 4.0 1 Carbon tetrachloride ND ug/L 07/27/23 06:00 56-23-51.0 0.33 1 Chlorobenzene ND ug/L 07/27/23 06:00 108-90-71.0 0.28 1 Chloroethane ND ug/L 07/27/23 06:00 75-00-31.0 0.65 1 Chloroform 0.51J ug/L 07/27/23 06:00 67-66-31.0 0.43 1 Chloromethane 0.74J ug/L 07/27/23 06:00 74-87-31.0 0.54 1 2-Chlorotoluene ND ug/L 07/27/23 06:00 95-49-81.0 0.32 1 4-Chlorotoluene ND ug/L 07/27/23 06:00 106-43-41.0 0.32 1 1,2-Dibromo-3-chloropropane ND ug/L 07/27/23 06:00 96-12-82.0 0.34 1 Dibromochloromethane ND ug/L 07/27/23 06:00 124-48-11.0 0.36 1 1,2-Dibromoethane (EDB)ND ug/L 07/27/23 06:00 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/27/23 06:00 74-95-31.0 0.39 1 1,2-Dichlorobenzene ND ug/L 07/27/23 06:00 95-50-11.0 0.34 1 1,3-Dichlorobenzene ND ug/L 07/27/23 06:00 541-73-11.0 0.34 1 1,4-Dichlorobenzene ND ug/L 07/27/23 06:00 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/27/23 06:00 75-71-81.0 0.35 1 1,1-Dichloroethane ND ug/L 07/27/23 06:00 75-34-31.0 0.37 1 1,2-Dichloroethane ND ug/L 07/27/23 06:00 107-06-21.0 0.32 1 1,1-Dichloroethene ND ug/L 07/27/23 06:00 75-35-41.0 0.35 1 cis-1,2-Dichloroethene ND ug/L 07/27/23 06:00 156-59-21.0 0.38 1 trans-1,2-Dichloroethene ND ug/L 07/27/23 06:00 156-60-51.0 0.40 1 1,2-Dichloropropane ND ug/L 07/27/23 06:00 78-87-51.0 0.36 1 1,3-Dichloropropane ND ug/L 07/27/23 06:00 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/27/23 06:00 594-20-71.0 0.39 1 1,1-Dichloropropene ND ug/L 07/27/23 06:00 563-58-61.0 0.43 1 cis-1,3-Dichloropropene ND ug/L 07/27/23 06:00 10061-01-51.0 0.36 1 trans-1,3-Dichloropropene ND ug/L 07/27/23 06:00 10061-02-61.0 0.36 1 Diisopropyl ether ND ug/L 07/27/23 06:00 108-20-31.0 0.31 1 Ethylbenzene ND ug/L 07/27/23 06:00 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/27/23 06:00 87-68-32.0 1.5 1 2-Hexanone ND ug/L 07/27/23 06:00 591-78-65.0 0.48 1 p-Isopropyltoluene ND ug/L 07/27/23 06:00 99-87-61.0 0.41 1 Methylene Chloride ND ug/L 07/27/23 06:00 75-09-25.0 2.0 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/27/23 06:00 108-10-15.0 2.7 1 Methyl-tert-butyl ether ND ug/L 07/27/23 06:00 1634-04-41.0 0.42 1 Naphthalene ND ug/L 07/27/23 06:00 91-20-31.0 0.64 1 Styrene ND ug/L 07/27/23 06:00 100-42-51.0 0.29 1 1,1,1,2-Tetrachloroethane ND ug/L 07/27/23 06:00 630-20-61.0 0.31 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 51 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-8 Lab ID: 92678743012 Collected: 07/20/23 16:45 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level 1,1,2,2-Tetrachloroethane ND ug/L 07/27/23 06:00 79-34-51.0 0.22 1 Tetrachloroethene 71.8 ug/L 07/27/23 06:00 127-18-41.0 0.29 1 Toluene ND ug/L 07/27/23 06:00 108-88-31.0 0.24 1 1,2,3-Trichlorobenzene ND ug/L 07/27/23 06:00 87-61-61.0 0.81 1 1,2,4-Trichlorobenzene ND ug/L 07/27/23 06:00 120-82-11.0 0.64 1 1,1,1-Trichloroethane ND ug/L 07/27/23 06:00 71-55-61.0 0.33 1 1,1,2-Trichloroethane ND ug/L 07/27/23 06:00 79-00-51.0 0.32 1 Trichloroethene 6.1 ug/L 07/27/23 06:00 79-01-61.0 0.38 1 Trichlorofluoromethane 2.8 ug/L 07/27/23 06:00 75-69-41.0 0.30 1 1,2,3-Trichloropropane ND ug/L 07/27/23 06:00 96-18-41.0 0.26 1 Vinyl acetate ND ug/L 07/27/23 06:00 108-05-42.0 1.3 1 Vinyl chloride ND ug/L 07/27/23 06:00 75-01-41.0 0.39 1 Xylene (Total)ND ug/L 07/27/23 06:00 1330-20-71.0 0.34 1 m&p-Xylene ND ug/L 07/27/23 06:00 179601-23-12.0 0.71 1 o-Xylene ND ug/L 07/27/23 06:00 95-47-61.0 0.34 1 Surrogates 4-Bromofluorobenzene (S)99 %07/27/23 06:00 460-00-470-130 1 1,2-Dichloroethane-d4 (S)103 %07/27/23 06:00 17060-07-070-130 1 Toluene-d8 (S)98 %07/27/23 06:00 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 52 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-9 Lab ID: 92678743013 Collected: 07/19/23 16:20 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3010A Pace Analytical Services - Asheville 6020 MET ICPMS Arsenic 0.28J ug/L 07/27/23 02:22 7440-38-207/26/23 11:461.0 0.087 1 Barium 127 ug/L 07/27/23 02:22 7440-39-307/26/23 11:461.0 0.21 1 Cadmium 0.10J ug/L 07/27/23 02:22 7440-43-907/26/23 11:460.20 0.060 1 Chromium 0.61J ug/L 07/27/23 02:22 7440-47-307/26/23 11:461.0 0.50 1 Lead 0.091J ug/L 07/27/23 02:22 7439-92-107/26/23 11:461.0 0.077 1 Selenium 2.4 ug/L 07/27/23 02:22 7782-49-207/26/23 11:462.0 0.072 1 Silver ND ug/L 07/27/23 02:22 7440-22-407/26/23 11:460.40 0.070 1 Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services - Asheville 7470 Mercury Mercury ND ug/L 07/31/23 14:23 7439-97-607/31/23 09:370.20 0.12 1 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Acenaphthene ND ug/L 07/25/23 22:36 83-32-907/25/23 11:2210.0 2.0 1 Acenaphthylene ND ug/L 07/25/23 22:36 208-96-807/25/23 11:2210.0 2.0 1 Aniline ND ug/L 07/25/23 22:36 62-53-307/25/23 11:2210.0 1.6 1 Anthracene ND ug/L 07/25/23 22:36 120-12-707/25/23 11:2210.0 2.3 1 Benzo(a)anthracene ND ug/L 07/25/23 22:36 56-55-307/25/23 11:2210.0 2.7 1 Benzo(a)pyrene ND ug/L 07/25/23 22:36 50-32-807/25/23 11:2210.0 2.8 1 Benzo(b)fluoranthene ND ug/L 07/25/23 22:36 205-99-207/25/23 11:2210.0 2.6 1 Benzo(g,h,i)perylene ND ug/L 07/25/23 22:36 191-24-207/25/23 11:2210.0 2.8 1 Benzo(k)fluoranthene ND ug/L 07/25/23 22:36 207-08-907/25/23 11:2210.0 2.7 1 Benzoic Acid 46.0J ug/L 07/25/23 22:36 65-85-0 C707/25/23 11:2250.0 22.0 1 Benzyl alcohol ND ug/L 07/25/23 22:36 100-51-607/25/23 11:2220.0 2.9 1 4-Bromophenylphenyl ether ND ug/L 07/25/23 22:36 101-55-307/25/23 11:2210.0 1.8 1 Butylbenzylphthalate ND ug/L 07/25/23 22:36 85-68-707/25/23 11:2210.0 3.1 1 4-Chloro-3-methylphenol ND ug/L 07/25/23 22:36 59-50-707/25/23 11:2210.0 3.3 1 4-Chloroaniline ND ug/L 07/25/23 22:36 106-47-807/25/23 11:2220.0 3.6 1 bis(2-Chloroethoxy)methane ND ug/L 07/25/23 22:36 111-91-107/25/23 11:2210.0 1.8 1 bis(2-Chloroethyl) ether ND ug/L 07/25/23 22:36 111-44-407/25/23 11:2210.0 1.9 1 2-Chloronaphthalene ND ug/L 07/25/23 22:36 91-58-707/25/23 11:2210.0 1.7 1 2-Chlorophenol ND ug/L 07/25/23 22:36 95-57-807/25/23 11:2210.0 1.2 1 4-Chlorophenylphenyl ether ND ug/L 07/25/23 22:36 7005-72-307/25/23 11:2210.0 2.0 1 Chrysene ND ug/L 07/25/23 22:36 218-01-907/25/23 11:2210.0 2.8 1 Dibenz(a,h)anthracene ND ug/L 07/25/23 22:36 53-70-307/25/23 11:2210.0 3.0 1 Dibenzofuran ND ug/L 07/25/23 22:36 132-64-907/25/23 11:2210.0 2.1 1 1,2-Dichlorobenzene ND ug/L 07/25/23 22:36 95-50-107/25/23 11:2210.0 1.8 1 1,3-Dichlorobenzene ND ug/L 07/25/23 22:36 541-73-107/25/23 11:2210.0 1.6 1 1,4-Dichlorobenzene ND ug/L 07/25/23 22:36 106-46-707/25/23 11:2210.0 1.7 1 3,3'-Dichlorobenzidine ND ug/L 07/25/23 22:36 91-94-107/25/23 11:2220.0 8.1 1 2,4-Dichlorophenol ND ug/L 07/25/23 22:36 120-83-207/25/23 11:2210.0 1.4 1 Diethylphthalate 3.8J ug/L 07/25/23 22:36 84-66-207/25/23 11:2210.0 2.0 1 2,4-Dimethylphenol ND ug/L 07/25/23 22:36 105-67-9 v107/25/23 11:2210.0 1.7 1 Dimethylphthalate ND ug/L 07/25/23 22:36 131-11-307/25/23 11:2210.0 2.1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 53 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-9 Lab ID: 92678743013 Collected: 07/19/23 16:20 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Di-n-butylphthalate ND ug/L 07/25/23 22:36 84-74-207/25/23 11:2210.0 2.2 1 4,6-Dinitro-2-methylphenol ND ug/L 07/25/23 22:36 534-52-107/25/23 11:2220.0 7.8 1 2,4-Dinitrophenol ND ug/L 07/25/23 22:36 51-28-507/25/23 11:2250.0 26.0 1 2,4-Dinitrotoluene ND ug/L 07/25/23 22:36 121-14-207/25/23 11:2210.0 1.6 1 2,6-Dinitrotoluene ND ug/L 07/25/23 22:36 606-20-207/25/23 11:2210.0 1.7 1 Di-n-octylphthalate ND ug/L 07/25/23 22:36 117-84-007/25/23 11:2210.0 3.9 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/25/23 22:36 117-81-707/25/23 11:226.0 3.7 1 Fluoranthene ND ug/L 07/25/23 22:36 206-44-007/25/23 11:2210.0 2.2 1 Fluorene ND ug/L 07/25/23 22:36 86-73-707/25/23 11:2210.0 2.1 1 Hexachloro-1,3-butadiene ND ug/L 07/25/23 22:36 87-68-307/25/23 11:2210.0 1.8 1 Hexachlorobenzene ND ug/L 07/25/23 22:36 118-74-107/25/23 11:2210.0 2.2 1 Hexachlorocyclopentadiene ND ug/L 07/25/23 22:36 77-47-407/25/23 11:2210.0 1.6 1 Hexachloroethane ND ug/L 07/25/23 22:36 67-72-107/25/23 11:2210.0 1.4 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/25/23 22:36 193-39-507/25/23 11:2210.0 2.9 1 Isophorone ND ug/L 07/25/23 22:36 78-59-107/25/23 11:2210.0 1.7 1 1-Methylnaphthalene ND ug/L 07/25/23 22:36 90-12-007/25/23 11:2210.0 2.0 1 2-Methylnaphthalene ND ug/L 07/25/23 22:36 91-57-607/25/23 11:2210.0 1.9 1 2-Methylphenol(o-Cresol)ND ug/L 07/25/23 22:36 95-48-707/25/23 11:2210.0 1.9 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/25/23 22:36 15831-10-407/25/23 11:2210.0 1.2 1 Naphthalene ND ug/L 07/25/23 22:36 91-20-307/25/23 11:2210.0 2.1 1 2-Nitroaniline ND ug/L 07/25/23 22:36 88-74-407/25/23 11:2220.0 3.0 1 3-Nitroaniline ND ug/L 07/25/23 22:36 99-09-207/25/23 11:2220.0 3.8 1 4-Nitroaniline ND ug/L 07/25/23 22:36 100-01-607/25/23 11:2220.0 5.1 1 Nitrobenzene ND ug/L 07/25/23 22:36 98-95-307/25/23 11:2210.0 1.9 1 2-Nitrophenol ND ug/L 07/25/23 22:36 88-75-507/25/23 11:2210.0 1.4 1 4-Nitrophenol ND ug/L 07/25/23 22:36 100-02-707/25/23 11:2250.0 6.6 1 N-Nitrosodimethylamine ND ug/L 07/25/23 22:36 62-75-9 v107/25/23 11:2210.0 1.9 1 N-Nitroso-di-n-propylamine ND ug/L 07/25/23 22:36 621-64-707/25/23 11:2210.0 1.3 1 N-Nitrosodiphenylamine ND ug/L 07/25/23 22:36 86-30-607/25/23 11:2210.0 3.0 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/25/23 22:36 108-60-1 v107/25/23 11:2210.0 1.2 1 Pentachlorophenol ND ug/L 07/25/23 22:36 87-86-507/25/23 11:2220.0 3.8 1 Phenanthrene ND ug/L 07/25/23 22:36 85-01-807/25/23 11:2210.0 2.0 1 Phenol ND ug/L 07/25/23 22:36 108-95-207/25/23 11:2210.0 1.4 1 Pyrene ND ug/L 07/25/23 22:36 129-00-007/25/23 11:2210.0 2.2 1 1,2,4-Trichlorobenzene ND ug/L 07/25/23 22:36 120-82-107/25/23 11:2210.0 1.7 1 2,4,5-Trichlorophenol ND ug/L 07/25/23 22:36 95-95-407/25/23 11:2210.0 1.4 1 2,4,6-Trichlorophenol ND ug/L 07/25/23 22:36 88-06-207/25/23 11:2210.0 1.6 1 Surrogates Nitrobenzene-d5 (S)99 %07/25/23 22:36 4165-60-007/25/23 11:2210-138 1 2-Fluorobiphenyl (S)82 %07/25/23 22:36 321-60-807/25/23 11:2210-130 1 Terphenyl-d14 (S)117 %07/25/23 22:36 1718-51-007/25/23 11:2219-191 1 Phenol-d6 (S)51 %07/25/23 22:36 13127-88-307/25/23 11:2210-130 1 2-Fluorophenol (S)68 %07/25/23 22:36 367-12-407/25/23 11:2210-130 1 2,4,6-Tribromophenol (S)131 %07/25/23 22:36 118-79-607/25/23 11:2210-164 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 54 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-9 Lab ID: 92678743013 Collected: 07/19/23 16:20 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level Acetone ND ug/L 07/27/23 06:18 67-64-125.0 5.1 1 Benzene ND ug/L 07/27/23 06:18 71-43-21.0 0.34 1 Bromobenzene ND ug/L 07/27/23 06:18 108-86-11.0 0.29 1 Bromochloromethane ND ug/L 07/27/23 06:18 74-97-51.0 0.47 1 Bromodichloromethane ND ug/L 07/27/23 06:18 75-27-41.0 0.31 1 Bromoform ND ug/L 07/27/23 06:18 75-25-21.0 0.34 1 Bromomethane ND ug/L 07/27/23 06:18 74-83-92.0 1.7 1 2-Butanone (MEK)ND ug/L 07/27/23 06:18 78-93-35.0 4.0 1 Carbon tetrachloride ND ug/L 07/27/23 06:18 56-23-51.0 0.33 1 Chlorobenzene ND ug/L 07/27/23 06:18 108-90-71.0 0.28 1 Chloroethane ND ug/L 07/27/23 06:18 75-00-31.0 0.65 1 Chloroform ND ug/L 07/27/23 06:18 67-66-31.0 0.43 1 Chloromethane 43.4 ug/L 07/27/23 06:18 74-87-31.0 0.54 1 2-Chlorotoluene ND ug/L 07/27/23 06:18 95-49-81.0 0.32 1 4-Chlorotoluene ND ug/L 07/27/23 06:18 106-43-41.0 0.32 1 1,2-Dibromo-3-chloropropane ND ug/L 07/27/23 06:18 96-12-82.0 0.34 1 Dibromochloromethane ND ug/L 07/27/23 06:18 124-48-11.0 0.36 1 1,2-Dibromoethane (EDB)ND ug/L 07/27/23 06:18 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/27/23 06:18 74-95-31.0 0.39 1 1,2-Dichlorobenzene ND ug/L 07/27/23 06:18 95-50-11.0 0.34 1 1,3-Dichlorobenzene ND ug/L 07/27/23 06:18 541-73-11.0 0.34 1 1,4-Dichlorobenzene ND ug/L 07/27/23 06:18 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/27/23 06:18 75-71-81.0 0.35 1 1,1-Dichloroethane ND ug/L 07/27/23 06:18 75-34-31.0 0.37 1 1,2-Dichloroethane ND ug/L 07/27/23 06:18 107-06-21.0 0.32 1 1,1-Dichloroethene ND ug/L 07/27/23 06:18 75-35-41.0 0.35 1 cis-1,2-Dichloroethene ND ug/L 07/27/23 06:18 156-59-21.0 0.38 1 trans-1,2-Dichloroethene ND ug/L 07/27/23 06:18 156-60-51.0 0.40 1 1,2-Dichloropropane ND ug/L 07/27/23 06:18 78-87-51.0 0.36 1 1,3-Dichloropropane ND ug/L 07/27/23 06:18 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/27/23 06:18 594-20-71.0 0.39 1 1,1-Dichloropropene ND ug/L 07/27/23 06:18 563-58-61.0 0.43 1 cis-1,3-Dichloropropene ND ug/L 07/27/23 06:18 10061-01-51.0 0.36 1 trans-1,3-Dichloropropene ND ug/L 07/27/23 06:18 10061-02-61.0 0.36 1 Diisopropyl ether ND ug/L 07/27/23 06:18 108-20-31.0 0.31 1 Ethylbenzene ND ug/L 07/27/23 06:18 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/27/23 06:18 87-68-32.0 1.5 1 2-Hexanone 0.55J ug/L 07/27/23 06:18 591-78-65.0 0.48 1 p-Isopropyltoluene ND ug/L 07/27/23 06:18 99-87-61.0 0.41 1 Methylene Chloride ND ug/L 07/27/23 06:18 75-09-25.0 2.0 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/27/23 06:18 108-10-15.0 2.7 1 Methyl-tert-butyl ether ND ug/L 07/27/23 06:18 1634-04-41.0 0.42 1 Naphthalene ND ug/L 07/27/23 06:18 91-20-31.0 0.64 1 Styrene ND ug/L 07/27/23 06:18 100-42-51.0 0.29 1 1,1,1,2-Tetrachloroethane ND ug/L 07/27/23 06:18 630-20-61.0 0.31 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 55 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-9 Lab ID: 92678743013 Collected: 07/19/23 16:20 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level 1,1,2,2-Tetrachloroethane ND ug/L 07/27/23 06:18 79-34-51.0 0.22 1 Tetrachloroethene ND ug/L 07/27/23 06:18 127-18-41.0 0.29 1 Toluene ND ug/L 07/27/23 06:18 108-88-31.0 0.24 1 1,2,3-Trichlorobenzene ND ug/L 07/27/23 06:18 87-61-61.0 0.81 1 1,2,4-Trichlorobenzene ND ug/L 07/27/23 06:18 120-82-11.0 0.64 1 1,1,1-Trichloroethane ND ug/L 07/27/23 06:18 71-55-61.0 0.33 1 1,1,2-Trichloroethane ND ug/L 07/27/23 06:18 79-00-51.0 0.32 1 Trichloroethene ND ug/L 07/27/23 06:18 79-01-61.0 0.38 1 Trichlorofluoromethane ND ug/L 07/27/23 06:18 75-69-41.0 0.30 1 1,2,3-Trichloropropane ND ug/L 07/27/23 06:18 96-18-41.0 0.26 1 Vinyl acetate ND ug/L 07/27/23 06:18 108-05-42.0 1.3 1 Vinyl chloride ND ug/L 07/27/23 06:18 75-01-41.0 0.39 1 Xylene (Total)ND ug/L 07/27/23 06:18 1330-20-71.0 0.34 1 m&p-Xylene ND ug/L 07/27/23 06:18 179601-23-12.0 0.71 1 o-Xylene ND ug/L 07/27/23 06:18 95-47-61.0 0.34 1 Surrogates 4-Bromofluorobenzene (S)99 %07/27/23 06:18 460-00-470-130 1 1,2-Dichloroethane-d4 (S)104 %07/27/23 06:18 17060-07-070-130 1 Toluene-d8 (S)99 %07/27/23 06:18 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 56 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-10 Lab ID: 92678743014 Collected: 07/20/23 10:05 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3010A Pace Analytical Services - Asheville 6020 MET ICPMS Arsenic 0.29J ug/L 07/27/23 02:27 7440-38-207/26/23 11:461.0 0.087 1 Barium 80.5 ug/L 07/27/23 02:27 7440-39-307/26/23 11:461.0 0.21 1 Cadmium 0.067J ug/L 07/27/23 02:27 7440-43-907/26/23 11:460.20 0.060 1 Chromium 0.69J ug/L 07/27/23 02:27 7440-47-307/26/23 11:461.0 0.50 1 Lead ND ug/L 07/27/23 02:27 7439-92-107/26/23 11:461.0 0.077 1 Selenium 0.28J ug/L 07/27/23 02:27 7782-49-207/26/23 11:462.0 0.072 1 Silver ND ug/L 07/27/23 02:27 7440-22-407/26/23 11:460.40 0.070 1 Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services - Asheville 7470 Mercury Mercury ND ug/L 07/31/23 14:26 7439-97-607/31/23 09:370.20 0.12 1 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Acenaphthene ND ug/L 07/27/23 11:21 83-32-907/26/23 12:0610.0 2.0 1 Acenaphthylene ND ug/L 07/27/23 11:21 208-96-807/26/23 12:0610.0 2.0 1 Aniline ND ug/L 07/27/23 11:21 62-53-307/26/23 12:0610.0 1.6 1 Anthracene ND ug/L 07/27/23 11:21 120-12-707/26/23 12:0610.0 2.3 1 Benzo(a)anthracene ND ug/L 07/27/23 11:21 56-55-307/26/23 12:0610.0 2.7 1 Benzo(a)pyrene ND ug/L 07/27/23 11:21 50-32-807/26/23 12:0610.0 2.8 1 Benzo(b)fluoranthene ND ug/L 07/27/23 11:21 205-99-207/26/23 12:0610.0 2.6 1 Benzo(g,h,i)perylene ND ug/L 07/27/23 11:21 191-24-207/26/23 12:0610.0 2.8 1 Benzo(k)fluoranthene ND ug/L 07/27/23 11:21 207-08-907/26/23 12:0610.0 2.7 1 Benzoic Acid ND ug/L 07/27/23 11:21 65-85-007/26/23 12:0650.0 22.0 1 Benzyl alcohol ND ug/L 07/27/23 11:21 100-51-607/26/23 12:0620.0 2.9 1 4-Bromophenylphenyl ether ND ug/L 07/27/23 11:21 101-55-307/26/23 12:0610.0 1.8 1 Butylbenzylphthalate ND ug/L 07/27/23 11:21 85-68-707/26/23 12:0610.0 3.1 1 4-Chloro-3-methylphenol ND ug/L 07/27/23 11:21 59-50-707/26/23 12:0610.0 3.3 1 4-Chloroaniline ND ug/L 07/27/23 11:21 106-47-807/26/23 12:0620.0 3.6 1 bis(2-Chloroethoxy)methane ND ug/L 07/27/23 11:21 111-91-107/26/23 12:0610.0 1.8 1 bis(2-Chloroethyl) ether ND ug/L 07/27/23 11:21 111-44-407/26/23 12:0610.0 1.9 1 2-Chloronaphthalene ND ug/L 07/27/23 11:21 91-58-707/26/23 12:0610.0 1.7 1 2-Chlorophenol ND ug/L 07/27/23 11:21 95-57-807/26/23 12:0610.0 1.2 1 4-Chlorophenylphenyl ether ND ug/L 07/27/23 11:21 7005-72-307/26/23 12:0610.0 2.0 1 Chrysene ND ug/L 07/27/23 11:21 218-01-907/26/23 12:0610.0 2.8 1 Dibenz(a,h)anthracene ND ug/L 07/27/23 11:21 53-70-307/26/23 12:0610.0 3.0 1 Dibenzofuran ND ug/L 07/27/23 11:21 132-64-907/26/23 12:0610.0 2.1 1 1,2-Dichlorobenzene ND ug/L 07/27/23 11:21 95-50-107/26/23 12:0610.0 1.8 1 1,3-Dichlorobenzene ND ug/L 07/27/23 11:21 541-73-107/26/23 12:0610.0 1.6 1 1,4-Dichlorobenzene ND ug/L 07/27/23 11:21 106-46-707/26/23 12:0610.0 1.7 1 3,3'-Dichlorobenzidine ND ug/L 07/27/23 11:21 91-94-107/26/23 12:0620.0 8.1 1 2,4-Dichlorophenol ND ug/L 07/27/23 11:21 120-83-207/26/23 12:0610.0 1.4 1 Diethylphthalate 5.1J ug/L 07/27/23 11:21 84-66-207/26/23 12:0610.0 2.0 1 2,4-Dimethylphenol ND ug/L 07/27/23 11:21 105-67-907/26/23 12:0610.0 1.7 1 Dimethylphthalate ND ug/L 07/27/23 11:21 131-11-307/26/23 12:0610.0 2.1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 57 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-10 Lab ID: 92678743014 Collected: 07/20/23 10:05 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Di-n-butylphthalate ND ug/L 07/27/23 11:21 84-74-207/26/23 12:0610.0 2.2 1 4,6-Dinitro-2-methylphenol ND ug/L 07/27/23 11:21 534-52-107/26/23 12:0620.0 7.8 1 2,4-Dinitrophenol ND ug/L 07/27/23 11:21 51-28-507/26/23 12:0650.0 26.0 1 2,4-Dinitrotoluene ND ug/L 07/27/23 11:21 121-14-207/26/23 12:0610.0 1.6 1 2,6-Dinitrotoluene ND ug/L 07/27/23 11:21 606-20-207/26/23 12:0610.0 1.7 1 Di-n-octylphthalate ND ug/L 07/27/23 11:21 117-84-007/26/23 12:0610.0 3.9 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/27/23 11:21 117-81-707/26/23 12:066.0 3.7 1 Fluoranthene ND ug/L 07/27/23 11:21 206-44-007/26/23 12:0610.0 2.2 1 Fluorene ND ug/L 07/27/23 11:21 86-73-707/26/23 12:0610.0 2.1 1 Hexachloro-1,3-butadiene ND ug/L 07/27/23 11:21 87-68-307/26/23 12:0610.0 1.8 1 Hexachlorobenzene ND ug/L 07/27/23 11:21 118-74-107/26/23 12:0610.0 2.2 1 Hexachlorocyclopentadiene ND ug/L 07/27/23 11:21 77-47-407/26/23 12:0610.0 1.6 1 Hexachloroethane ND ug/L 07/27/23 11:21 67-72-107/26/23 12:0610.0 1.4 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/27/23 11:21 193-39-507/26/23 12:0610.0 2.9 1 Isophorone ND ug/L 07/27/23 11:21 78-59-107/26/23 12:0610.0 1.7 1 1-Methylnaphthalene ND ug/L 07/27/23 11:21 90-12-007/26/23 12:0610.0 2.0 1 2-Methylnaphthalene ND ug/L 07/27/23 11:21 91-57-607/26/23 12:0610.0 1.9 1 2-Methylphenol(o-Cresol)ND ug/L 07/27/23 11:21 95-48-707/26/23 12:0610.0 1.9 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/27/23 11:21 15831-10-407/26/23 12:0610.0 1.2 1 Naphthalene ND ug/L 07/27/23 11:21 91-20-307/26/23 12:0610.0 2.1 1 2-Nitroaniline ND ug/L 07/27/23 11:21 88-74-407/26/23 12:0620.0 3.0 1 3-Nitroaniline ND ug/L 07/27/23 11:21 99-09-207/26/23 12:0620.0 3.8 1 4-Nitroaniline ND ug/L 07/27/23 11:21 100-01-607/26/23 12:0620.0 5.1 1 Nitrobenzene ND ug/L 07/27/23 11:21 98-95-307/26/23 12:0610.0 1.9 1 2-Nitrophenol ND ug/L 07/27/23 11:21 88-75-507/26/23 12:0610.0 1.4 1 4-Nitrophenol ND ug/L 07/27/23 11:21 100-02-707/26/23 12:0650.0 6.6 1 N-Nitrosodimethylamine ND ug/L 07/27/23 11:21 62-75-907/26/23 12:0610.0 1.9 1 N-Nitroso-di-n-propylamine ND ug/L 07/27/23 11:21 621-64-707/26/23 12:0610.0 1.3 1 N-Nitrosodiphenylamine ND ug/L 07/27/23 11:21 86-30-607/26/23 12:0610.0 3.0 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/27/23 11:21 108-60-107/26/23 12:0610.0 1.2 1 Pentachlorophenol ND ug/L 07/27/23 11:21 87-86-507/26/23 12:0620.0 3.8 1 Phenanthrene ND ug/L 07/27/23 11:21 85-01-807/26/23 12:0610.0 2.0 1 Phenol ND ug/L 07/27/23 11:21 108-95-207/26/23 12:0610.0 1.4 1 Pyrene ND ug/L 07/27/23 11:21 129-00-007/26/23 12:0610.0 2.2 1 1,2,4-Trichlorobenzene ND ug/L 07/27/23 11:21 120-82-107/26/23 12:0610.0 1.7 1 2,4,5-Trichlorophenol ND ug/L 07/27/23 11:21 95-95-407/26/23 12:0610.0 1.4 1 2,4,6-Trichlorophenol ND ug/L 07/27/23 11:21 88-06-207/26/23 12:0610.0 1.6 1 Surrogates Nitrobenzene-d5 (S)62 %07/27/23 11:21 4165-60-007/26/23 12:0610-138 1 2-Fluorobiphenyl (S)51 %07/27/23 11:21 321-60-807/26/23 12:0610-130 1 Terphenyl-d14 (S)98 %07/27/23 11:21 1718-51-007/26/23 12:0619-191 1 Phenol-d6 (S)35 %07/27/23 11:21 13127-88-307/26/23 12:0610-130 1 2-Fluorophenol (S)45 %07/27/23 11:21 367-12-407/26/23 12:0610-130 1 2,4,6-Tribromophenol (S)88 %07/27/23 11:21 118-79-607/26/23 12:0610-164 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 58 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-10 Lab ID: 92678743014 Collected: 07/20/23 10:05 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level Acetone 8.3J ug/L 07/27/23 00:50 67-64-125.0 5.1 1 Benzene ND ug/L 07/27/23 00:50 71-43-21.0 0.34 1 Bromobenzene ND ug/L 07/27/23 00:50 108-86-11.0 0.29 1 Bromochloromethane ND ug/L 07/27/23 00:50 74-97-51.0 0.47 1 Bromodichloromethane ND ug/L 07/27/23 00:50 75-27-41.0 0.31 1 Bromoform ND ug/L 07/27/23 00:50 75-25-21.0 0.34 1 Bromomethane ND ug/L 07/27/23 00:50 74-83-92.0 1.7 1 2-Butanone (MEK)ND ug/L 07/27/23 00:50 78-93-35.0 4.0 1 Carbon tetrachloride ND ug/L 07/27/23 00:50 56-23-51.0 0.33 1 Chlorobenzene ND ug/L 07/27/23 00:50 108-90-71.0 0.28 1 Chloroethane ND ug/L 07/27/23 00:50 75-00-31.0 0.65 1 Chloroform ND ug/L 07/27/23 00:50 67-66-31.0 0.43 1 Chloromethane 0.80J ug/L 07/27/23 00:50 74-87-31.0 0.54 1 2-Chlorotoluene ND ug/L 07/27/23 00:50 95-49-81.0 0.32 1 4-Chlorotoluene ND ug/L 07/27/23 00:50 106-43-41.0 0.32 1 1,2-Dibromo-3-chloropropane ND ug/L 07/27/23 00:50 96-12-82.0 0.34 1 Dibromochloromethane ND ug/L 07/27/23 00:50 124-48-11.0 0.36 1 1,2-Dibromoethane (EDB)ND ug/L 07/27/23 00:50 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/27/23 00:50 74-95-31.0 0.39 1 1,2-Dichlorobenzene ND ug/L 07/27/23 00:50 95-50-11.0 0.34 1 1,3-Dichlorobenzene ND ug/L 07/27/23 00:50 541-73-11.0 0.34 1 1,4-Dichlorobenzene ND ug/L 07/27/23 00:50 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/27/23 00:50 75-71-81.0 0.35 1 1,1-Dichloroethane ND ug/L 07/27/23 00:50 75-34-31.0 0.37 1 1,2-Dichloroethane ND ug/L 07/27/23 00:50 107-06-21.0 0.32 1 1,1-Dichloroethene ND ug/L 07/27/23 00:50 75-35-41.0 0.35 1 cis-1,2-Dichloroethene ND ug/L 07/27/23 00:50 156-59-21.0 0.38 1 trans-1,2-Dichloroethene ND ug/L 07/27/23 00:50 156-60-51.0 0.40 1 1,2-Dichloropropane ND ug/L 07/27/23 00:50 78-87-51.0 0.36 1 1,3-Dichloropropane ND ug/L 07/27/23 00:50 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/27/23 00:50 594-20-71.0 0.39 1 1,1-Dichloropropene ND ug/L 07/27/23 00:50 563-58-61.0 0.43 1 cis-1,3-Dichloropropene ND ug/L 07/27/23 00:50 10061-01-51.0 0.36 1 trans-1,3-Dichloropropene ND ug/L 07/27/23 00:50 10061-02-61.0 0.36 1 Diisopropyl ether ND ug/L 07/27/23 00:50 108-20-31.0 0.31 1 Ethylbenzene ND ug/L 07/27/23 00:50 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/27/23 00:50 87-68-32.0 1.5 1 2-Hexanone 0.59J ug/L 07/27/23 00:50 591-78-65.0 0.48 1 p-Isopropyltoluene ND ug/L 07/27/23 00:50 99-87-61.0 0.41 1 Methylene Chloride ND ug/L 07/27/23 00:50 75-09-25.0 2.0 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/27/23 00:50 108-10-15.0 2.7 1 Methyl-tert-butyl ether ND ug/L 07/27/23 00:50 1634-04-41.0 0.42 1 Naphthalene ND ug/L 07/27/23 00:50 91-20-31.0 0.64 1 Styrene ND ug/L 07/27/23 00:50 100-42-51.0 0.29 1 1,1,1,2-Tetrachloroethane ND ug/L 07/27/23 00:50 630-20-61.0 0.31 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 59 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-10 Lab ID: 92678743014 Collected: 07/20/23 10:05 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level 1,1,2,2-Tetrachloroethane ND ug/L 07/27/23 00:50 79-34-51.0 0.22 1 Tetrachloroethene ND ug/L 07/27/23 00:50 127-18-41.0 0.29 1 Toluene ND ug/L 07/27/23 00:50 108-88-31.0 0.24 1 1,2,3-Trichlorobenzene ND ug/L 07/27/23 00:50 87-61-61.0 0.81 1 1,2,4-Trichlorobenzene ND ug/L 07/27/23 00:50 120-82-11.0 0.64 1 1,1,1-Trichloroethane ND ug/L 07/27/23 00:50 71-55-61.0 0.33 1 1,1,2-Trichloroethane ND ug/L 07/27/23 00:50 79-00-51.0 0.32 1 Trichloroethene ND ug/L 07/27/23 00:50 79-01-61.0 0.38 1 Trichlorofluoromethane ND ug/L 07/27/23 00:50 75-69-41.0 0.30 1 1,2,3-Trichloropropane ND ug/L 07/27/23 00:50 96-18-41.0 0.26 1 Vinyl acetate ND ug/L 07/27/23 00:50 108-05-42.0 1.3 1 Vinyl chloride ND ug/L 07/27/23 00:50 75-01-41.0 0.39 1 Xylene (Total)ND ug/L 07/27/23 00:50 1330-20-71.0 0.34 1 m&p-Xylene ND ug/L 07/27/23 00:50 179601-23-12.0 0.71 1 o-Xylene ND ug/L 07/27/23 00:50 95-47-61.0 0.34 1 Surrogates 4-Bromofluorobenzene (S)98 %07/27/23 00:50 460-00-470-130 1 1,2-Dichloroethane-d4 (S)103 %07/27/23 00:50 17060-07-070-130 1 Toluene-d8 (S)100 %07/27/23 00:50 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 60 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-11 Lab ID: 92678743015 Collected: 07/21/23 09:45 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3010A Pace Analytical Services - Asheville 6020 MET ICPMS Arsenic 0.17J ug/L 07/27/23 02:32 7440-38-207/26/23 11:461.0 0.087 1 Barium 128 ug/L 07/27/23 02:32 7440-39-307/26/23 11:461.0 0.21 1 Cadmium 0.085J ug/L 07/27/23 02:32 7440-43-907/26/23 11:460.20 0.060 1 Chromium 0.94J ug/L 07/27/23 02:32 7440-47-307/26/23 11:461.0 0.50 1 Lead ND ug/L 07/27/23 02:32 7439-92-107/26/23 11:461.0 0.077 1 Selenium ND ug/L 07/27/23 02:32 7782-49-207/26/23 11:462.0 0.072 1 Silver ND ug/L 07/27/23 02:32 7440-22-407/26/23 11:460.40 0.070 1 Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services - Asheville 7470 Mercury Mercury ND ug/L 07/31/23 14:28 7439-97-607/31/23 09:370.20 0.12 1 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Acenaphthene ND ug/L 07/27/23 11:46 83-32-907/26/23 12:069.1 1.8 1 Acenaphthylene ND ug/L 07/27/23 11:46 208-96-807/26/23 12:069.1 1.8 1 Aniline ND ug/L 07/27/23 11:46 62-53-307/26/23 12:069.1 1.5 1 Anthracene ND ug/L 07/27/23 11:46 120-12-707/26/23 12:069.1 2.1 1 Benzo(a)anthracene ND ug/L 07/27/23 11:46 56-55-307/26/23 12:069.1 2.4 1 Benzo(a)pyrene ND ug/L 07/27/23 11:46 50-32-807/26/23 12:069.1 2.5 1 Benzo(b)fluoranthene ND ug/L 07/27/23 11:46 205-99-207/26/23 12:069.1 2.4 1 Benzo(g,h,i)perylene ND ug/L 07/27/23 11:46 191-24-207/26/23 12:069.1 2.6 1 Benzo(k)fluoranthene ND ug/L 07/27/23 11:46 207-08-907/26/23 12:069.1 2.5 1 Benzoic Acid ND ug/L 07/27/23 11:46 65-85-007/26/23 12:0645.5 20.0 1 Benzyl alcohol ND ug/L 07/27/23 11:46 100-51-607/26/23 12:0618.2 2.6 1 4-Bromophenylphenyl ether ND ug/L 07/27/23 11:46 101-55-307/26/23 12:069.1 1.6 1 Butylbenzylphthalate ND ug/L 07/27/23 11:46 85-68-707/26/23 12:069.1 2.9 1 4-Chloro-3-methylphenol ND ug/L 07/27/23 11:46 59-50-707/26/23 12:069.1 3.0 1 4-Chloroaniline ND ug/L 07/27/23 11:46 106-47-807/26/23 12:0618.2 3.3 1 bis(2-Chloroethoxy)methane ND ug/L 07/27/23 11:46 111-91-107/26/23 12:069.1 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/27/23 11:46 111-44-407/26/23 12:069.1 1.7 1 2-Chloronaphthalene ND ug/L 07/27/23 11:46 91-58-707/26/23 12:069.1 1.6 1 2-Chlorophenol ND ug/L 07/27/23 11:46 95-57-807/26/23 12:069.1 1.1 1 4-Chlorophenylphenyl ether ND ug/L 07/27/23 11:46 7005-72-307/26/23 12:069.1 1.8 1 Chrysene ND ug/L 07/27/23 11:46 218-01-907/26/23 12:069.1 2.5 1 Dibenz(a,h)anthracene ND ug/L 07/27/23 11:46 53-70-307/26/23 12:069.1 2.7 1 Dibenzofuran ND ug/L 07/27/23 11:46 132-64-907/26/23 12:069.1 1.9 1 1,2-Dichlorobenzene ND ug/L 07/27/23 11:46 95-50-107/26/23 12:069.1 1.6 1 1,3-Dichlorobenzene ND ug/L 07/27/23 11:46 541-73-107/26/23 12:069.1 1.5 1 1,4-Dichlorobenzene ND ug/L 07/27/23 11:46 106-46-707/26/23 12:069.1 1.5 1 3,3'-Dichlorobenzidine ND ug/L 07/27/23 11:46 91-94-107/26/23 12:0618.2 7.4 1 2,4-Dichlorophenol ND ug/L 07/27/23 11:46 120-83-207/26/23 12:069.1 1.3 1 Diethylphthalate ND ug/L 07/27/23 11:46 84-66-207/26/23 12:069.1 1.9 1 2,4-Dimethylphenol ND ug/L 07/27/23 11:46 105-67-907/26/23 12:069.1 1.5 1 Dimethylphthalate ND ug/L 07/27/23 11:46 131-11-307/26/23 12:069.1 1.9 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 61 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-11 Lab ID: 92678743015 Collected: 07/21/23 09:45 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Di-n-butylphthalate ND ug/L 07/27/23 11:46 84-74-207/26/23 12:069.1 2.0 1 4,6-Dinitro-2-methylphenol ND ug/L 07/27/23 11:46 534-52-107/26/23 12:0618.2 7.1 1 2,4-Dinitrophenol ND ug/L 07/27/23 11:46 51-28-507/26/23 12:0645.5 23.6 1 2,4-Dinitrotoluene ND ug/L 07/27/23 11:46 121-14-207/26/23 12:069.1 1.5 1 2,6-Dinitrotoluene ND ug/L 07/27/23 11:46 606-20-207/26/23 12:069.1 1.6 1 Di-n-octylphthalate ND ug/L 07/27/23 11:46 117-84-007/26/23 12:069.1 3.6 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/27/23 11:46 117-81-707/26/23 12:065.5 3.4 1 Fluoranthene ND ug/L 07/27/23 11:46 206-44-007/26/23 12:069.1 2.0 1 Fluorene ND ug/L 07/27/23 11:46 86-73-707/26/23 12:069.1 1.9 1 Hexachloro-1,3-butadiene ND ug/L 07/27/23 11:46 87-68-307/26/23 12:069.1 1.6 1 Hexachlorobenzene ND ug/L 07/27/23 11:46 118-74-107/26/23 12:069.1 2.0 1 Hexachlorocyclopentadiene ND ug/L 07/27/23 11:46 77-47-407/26/23 12:069.1 1.4 1 Hexachloroethane ND ug/L 07/27/23 11:46 67-72-107/26/23 12:069.1 1.3 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/27/23 11:46 193-39-507/26/23 12:069.1 2.6 1 Isophorone ND ug/L 07/27/23 11:46 78-59-107/26/23 12:069.1 1.5 1 1-Methylnaphthalene ND ug/L 07/27/23 11:46 90-12-007/26/23 12:069.1 1.8 1 2-Methylnaphthalene ND ug/L 07/27/23 11:46 91-57-607/26/23 12:069.1 1.7 1 2-Methylphenol(o-Cresol)ND ug/L 07/27/23 11:46 95-48-707/26/23 12:069.1 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/27/23 11:46 15831-10-407/26/23 12:069.1 1.1 1 Naphthalene ND ug/L 07/27/23 11:46 91-20-307/26/23 12:069.1 1.9 1 2-Nitroaniline ND ug/L 07/27/23 11:46 88-74-407/26/23 12:0618.2 2.7 1 3-Nitroaniline ND ug/L 07/27/23 11:46 99-09-207/26/23 12:0618.2 3.4 1 4-Nitroaniline ND ug/L 07/27/23 11:46 100-01-607/26/23 12:0618.2 4.6 1 Nitrobenzene ND ug/L 07/27/23 11:46 98-95-307/26/23 12:069.1 1.7 1 2-Nitrophenol ND ug/L 07/27/23 11:46 88-75-507/26/23 12:069.1 1.3 1 4-Nitrophenol ND ug/L 07/27/23 11:46 100-02-707/26/23 12:0645.5 6.0 1 N-Nitrosodimethylamine ND ug/L 07/27/23 11:46 62-75-907/26/23 12:069.1 1.7 1 N-Nitroso-di-n-propylamine ND ug/L 07/27/23 11:46 621-64-707/26/23 12:069.1 1.2 1 N-Nitrosodiphenylamine ND ug/L 07/27/23 11:46 86-30-607/26/23 12:069.1 2.7 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/27/23 11:46 108-60-107/26/23 12:069.1 1.0 1 Pentachlorophenol ND ug/L 07/27/23 11:46 87-86-507/26/23 12:0618.2 3.4 1 Phenanthrene ND ug/L 07/27/23 11:46 85-01-807/26/23 12:069.1 1.8 1 Phenol ND ug/L 07/27/23 11:46 108-95-207/26/23 12:069.1 1.2 1 Pyrene ND ug/L 07/27/23 11:46 129-00-007/26/23 12:069.1 2.0 1 1,2,4-Trichlorobenzene ND ug/L 07/27/23 11:46 120-82-107/26/23 12:069.1 1.6 1 2,4,5-Trichlorophenol ND ug/L 07/27/23 11:46 95-95-407/26/23 12:069.1 1.3 1 2,4,6-Trichlorophenol ND ug/L 07/27/23 11:46 88-06-207/26/23 12:069.1 1.4 1 Surrogates Nitrobenzene-d5 (S)68 %07/27/23 11:46 4165-60-007/26/23 12:0610-138 1 2-Fluorobiphenyl (S)59 %07/27/23 11:46 321-60-807/26/23 12:0610-130 1 Terphenyl-d14 (S)110 %07/27/23 11:46 1718-51-007/26/23 12:0619-191 1 Phenol-d6 (S)36 %07/27/23 11:46 13127-88-307/26/23 12:0610-130 1 2-Fluorophenol (S)47 %07/27/23 11:46 367-12-407/26/23 12:0610-130 1 2,4,6-Tribromophenol (S)102 %07/27/23 11:46 118-79-607/26/23 12:0610-164 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 62 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-11 Lab ID: 92678743015 Collected: 07/21/23 09:45 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level Acetone ND ug/L 07/27/23 01:08 67-64-125.0 5.1 1 Benzene ND ug/L 07/27/23 01:08 71-43-21.0 0.34 1 Bromobenzene ND ug/L 07/27/23 01:08 108-86-11.0 0.29 1 Bromochloromethane ND ug/L 07/27/23 01:08 74-97-51.0 0.47 1 Bromodichloromethane ND ug/L 07/27/23 01:08 75-27-41.0 0.31 1 Bromoform ND ug/L 07/27/23 01:08 75-25-21.0 0.34 1 Bromomethane ND ug/L 07/27/23 01:08 74-83-92.0 1.7 1 2-Butanone (MEK)ND ug/L 07/27/23 01:08 78-93-35.0 4.0 1 Carbon tetrachloride ND ug/L 07/27/23 01:08 56-23-51.0 0.33 1 Chlorobenzene ND ug/L 07/27/23 01:08 108-90-71.0 0.28 1 Chloroethane ND ug/L 07/27/23 01:08 75-00-31.0 0.65 1 Chloroform 1.6 ug/L 07/27/23 01:08 67-66-31.0 0.43 1 Chloromethane 57.6 ug/L 07/27/23 01:08 74-87-31.0 0.54 1 2-Chlorotoluene ND ug/L 07/27/23 01:08 95-49-81.0 0.32 1 4-Chlorotoluene ND ug/L 07/27/23 01:08 106-43-41.0 0.32 1 1,2-Dibromo-3-chloropropane ND ug/L 07/27/23 01:08 96-12-82.0 0.34 1 Dibromochloromethane ND ug/L 07/27/23 01:08 124-48-11.0 0.36 1 1,2-Dibromoethane (EDB)ND ug/L 07/27/23 01:08 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/27/23 01:08 74-95-31.0 0.39 1 1,2-Dichlorobenzene ND ug/L 07/27/23 01:08 95-50-11.0 0.34 1 1,3-Dichlorobenzene ND ug/L 07/27/23 01:08 541-73-11.0 0.34 1 1,4-Dichlorobenzene ND ug/L 07/27/23 01:08 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/27/23 01:08 75-71-8 M11.0 0.35 1 1,1-Dichloroethane ND ug/L 07/27/23 01:08 75-34-31.0 0.37 1 1,2-Dichloroethane ND ug/L 07/27/23 01:08 107-06-21.0 0.32 1 1,1-Dichloroethene ND ug/L 07/27/23 01:08 75-35-41.0 0.35 1 cis-1,2-Dichloroethene ND ug/L 07/27/23 01:08 156-59-21.0 0.38 1 trans-1,2-Dichloroethene ND ug/L 07/27/23 01:08 156-60-51.0 0.40 1 1,2-Dichloropropane ND ug/L 07/27/23 01:08 78-87-51.0 0.36 1 1,3-Dichloropropane ND ug/L 07/27/23 01:08 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/27/23 01:08 594-20-71.0 0.39 1 1,1-Dichloropropene ND ug/L 07/27/23 01:08 563-58-61.0 0.43 1 cis-1,3-Dichloropropene ND ug/L 07/27/23 01:08 10061-01-51.0 0.36 1 trans-1,3-Dichloropropene ND ug/L 07/27/23 01:08 10061-02-61.0 0.36 1 Diisopropyl ether ND ug/L 07/27/23 01:08 108-20-31.0 0.31 1 Ethylbenzene ND ug/L 07/27/23 01:08 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/27/23 01:08 87-68-32.0 1.5 1 2-Hexanone ND ug/L 07/27/23 01:08 591-78-65.0 0.48 1 p-Isopropyltoluene ND ug/L 07/27/23 01:08 99-87-61.0 0.41 1 Methylene Chloride ND ug/L 07/27/23 01:08 75-09-25.0 2.0 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/27/23 01:08 108-10-15.0 2.7 1 Methyl-tert-butyl ether 4.0 ug/L 07/27/23 01:08 1634-04-41.0 0.42 1 Naphthalene ND ug/L 07/27/23 01:08 91-20-31.0 0.64 1 Styrene ND ug/L 07/27/23 01:08 100-42-51.0 0.29 1 1,1,1,2-Tetrachloroethane ND ug/L 07/27/23 01:08 630-20-61.0 0.31 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 63 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-11 Lab ID: 92678743015 Collected: 07/21/23 09:45 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level 1,1,2,2-Tetrachloroethane ND ug/L 07/27/23 01:08 79-34-51.0 0.22 1 Tetrachloroethene ND ug/L 07/27/23 01:08 127-18-41.0 0.29 1 Toluene ND ug/L 07/27/23 01:08 108-88-31.0 0.24 1 1,2,3-Trichlorobenzene ND ug/L 07/27/23 01:08 87-61-61.0 0.81 1 1,2,4-Trichlorobenzene ND ug/L 07/27/23 01:08 120-82-11.0 0.64 1 1,1,1-Trichloroethane ND ug/L 07/27/23 01:08 71-55-61.0 0.33 1 1,1,2-Trichloroethane ND ug/L 07/27/23 01:08 79-00-51.0 0.32 1 Trichloroethene ND ug/L 07/27/23 01:08 79-01-61.0 0.38 1 Trichlorofluoromethane ND ug/L 07/27/23 01:08 75-69-4 M11.0 0.30 1 1,2,3-Trichloropropane ND ug/L 07/27/23 01:08 96-18-41.0 0.26 1 Vinyl acetate ND ug/L 07/27/23 01:08 108-05-42.0 1.3 1 Vinyl chloride ND ug/L 07/27/23 01:08 75-01-41.0 0.39 1 Xylene (Total)ND ug/L 07/27/23 01:08 1330-20-71.0 0.34 1 m&p-Xylene ND ug/L 07/27/23 01:08 179601-23-12.0 0.71 1 o-Xylene ND ug/L 07/27/23 01:08 95-47-61.0 0.34 1 Surrogates 4-Bromofluorobenzene (S)100 %07/27/23 01:08 460-00-470-130 1 1,2-Dichloroethane-d4 (S)103 %07/27/23 01:08 17060-07-070-130 1 Toluene-d8 (S)99 %07/27/23 01:08 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 64 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-12 Lab ID: 92678743016 Collected: 07/20/23 14:15 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3010A Pace Analytical Services - Asheville 6020 MET ICPMS Arsenic 0.18J ug/L 07/27/23 02:37 7440-38-207/26/23 11:461.0 0.087 1 Barium 19.0 ug/L 07/27/23 02:37 7440-39-307/26/23 11:461.0 0.21 1 Cadmium 0.060J ug/L 07/27/23 02:37 7440-43-907/26/23 11:460.20 0.060 1 Chromium 0.92J ug/L 07/27/23 02:37 7440-47-307/26/23 11:461.0 0.50 1 Lead 0.25J ug/L 07/27/23 02:37 7439-92-107/26/23 11:461.0 0.077 1 Selenium ND ug/L 07/27/23 02:37 7782-49-207/26/23 11:462.0 0.072 1 Silver ND ug/L 07/27/23 02:37 7440-22-407/26/23 11:460.40 0.070 1 Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services - Asheville 7470 Mercury Mercury ND ug/L 07/31/23 14:30 7439-97-607/31/23 09:370.20 0.12 1 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Acenaphthene ND ug/L 07/25/23 23:53 83-32-907/25/23 11:228.3 1.7 1 Acenaphthylene ND ug/L 07/25/23 23:53 208-96-807/25/23 11:228.3 1.6 1 Aniline ND ug/L 07/25/23 23:53 62-53-307/25/23 11:228.3 1.4 1 Anthracene ND ug/L 07/25/23 23:53 120-12-707/25/23 11:228.3 1.9 1 Benzo(a)anthracene ND ug/L 07/25/23 23:53 56-55-307/25/23 11:228.3 2.2 1 Benzo(a)pyrene ND ug/L 07/25/23 23:53 50-32-807/25/23 11:228.3 2.3 1 Benzo(b)fluoranthene ND ug/L 07/25/23 23:53 205-99-207/25/23 11:228.3 2.2 1 Benzo(g,h,i)perylene ND ug/L 07/25/23 23:53 191-24-207/25/23 11:228.3 2.4 1 Benzo(k)fluoranthene ND ug/L 07/25/23 23:53 207-08-907/25/23 11:228.3 2.3 1 Benzoic Acid 41.3J ug/L 07/25/23 23:53 65-85-0 C707/25/23 11:2241.7 18.3 1 Benzyl alcohol ND ug/L 07/25/23 23:53 100-51-607/25/23 11:2216.7 2.4 1 4-Bromophenylphenyl ether ND ug/L 07/25/23 23:53 101-55-307/25/23 11:228.3 1.5 1 Butylbenzylphthalate ND ug/L 07/25/23 23:53 85-68-707/25/23 11:228.3 2.6 1 4-Chloro-3-methylphenol ND ug/L 07/25/23 23:53 59-50-707/25/23 11:228.3 2.8 1 4-Chloroaniline ND ug/L 07/25/23 23:53 106-47-807/25/23 11:2216.7 3.0 1 bis(2-Chloroethoxy)methane ND ug/L 07/25/23 23:53 111-91-107/25/23 11:228.3 1.5 1 bis(2-Chloroethyl) ether ND ug/L 07/25/23 23:53 111-44-407/25/23 11:228.3 1.6 1 2-Chloronaphthalene ND ug/L 07/25/23 23:53 91-58-707/25/23 11:228.3 1.4 1 2-Chlorophenol ND ug/L 07/25/23 23:53 95-57-807/25/23 11:228.3 1.0 1 4-Chlorophenylphenyl ether ND ug/L 07/25/23 23:53 7005-72-307/25/23 11:228.3 1.7 1 Chrysene ND ug/L 07/25/23 23:53 218-01-907/25/23 11:228.3 2.3 1 Dibenz(a,h)anthracene ND ug/L 07/25/23 23:53 53-70-307/25/23 11:228.3 2.5 1 Dibenzofuran ND ug/L 07/25/23 23:53 132-64-907/25/23 11:228.3 1.8 1 1,2-Dichlorobenzene ND ug/L 07/25/23 23:53 95-50-107/25/23 11:228.3 1.5 1 1,3-Dichlorobenzene ND ug/L 07/25/23 23:53 541-73-107/25/23 11:228.3 1.3 1 1,4-Dichlorobenzene ND ug/L 07/25/23 23:53 106-46-707/25/23 11:228.3 1.4 1 3,3'-Dichlorobenzidine ND ug/L 07/25/23 23:53 91-94-107/25/23 11:2216.7 6.8 1 2,4-Dichlorophenol ND ug/L 07/25/23 23:53 120-83-207/25/23 11:228.3 1.2 1 Diethylphthalate ND ug/L 07/25/23 23:53 84-66-207/25/23 11:228.3 1.7 1 2,4-Dimethylphenol ND ug/L 07/25/23 23:53 105-67-9 v107/25/23 11:228.3 1.4 1 Dimethylphthalate ND ug/L 07/25/23 23:53 131-11-307/25/23 11:228.3 1.8 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 65 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-12 Lab ID: 92678743016 Collected: 07/20/23 14:15 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Di-n-butylphthalate ND ug/L 07/25/23 23:53 84-74-207/25/23 11:228.3 1.8 1 4,6-Dinitro-2-methylphenol ND ug/L 07/25/23 23:53 534-52-107/25/23 11:2216.7 6.5 1 2,4-Dinitrophenol ND ug/L 07/25/23 23:53 51-28-507/25/23 11:2241.7 21.7 1 2,4-Dinitrotoluene ND ug/L 07/25/23 23:53 121-14-207/25/23 11:228.3 1.4 1 2,6-Dinitrotoluene ND ug/L 07/25/23 23:53 606-20-207/25/23 11:228.3 1.4 1 Di-n-octylphthalate ND ug/L 07/25/23 23:53 117-84-007/25/23 11:228.3 3.3 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/25/23 23:53 117-81-707/25/23 11:225.0 3.1 1 Fluoranthene ND ug/L 07/25/23 23:53 206-44-007/25/23 11:228.3 1.8 1 Fluorene ND ug/L 07/25/23 23:53 86-73-707/25/23 11:228.3 1.7 1 Hexachloro-1,3-butadiene ND ug/L 07/25/23 23:53 87-68-307/25/23 11:228.3 1.5 1 Hexachlorobenzene ND ug/L 07/25/23 23:53 118-74-107/25/23 11:228.3 1.8 1 Hexachlorocyclopentadiene ND ug/L 07/25/23 23:53 77-47-407/25/23 11:228.3 1.3 1 Hexachloroethane ND ug/L 07/25/23 23:53 67-72-107/25/23 11:228.3 1.2 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/25/23 23:53 193-39-507/25/23 11:228.3 2.4 1 Isophorone ND ug/L 07/25/23 23:53 78-59-107/25/23 11:228.3 1.4 1 1-Methylnaphthalene ND ug/L 07/25/23 23:53 90-12-007/25/23 11:228.3 1.7 1 2-Methylnaphthalene ND ug/L 07/25/23 23:53 91-57-607/25/23 11:228.3 1.6 1 2-Methylphenol(o-Cresol)ND ug/L 07/25/23 23:53 95-48-707/25/23 11:228.3 1.6 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/25/23 23:53 15831-10-407/25/23 11:228.3 1.0 1 Naphthalene ND ug/L 07/25/23 23:53 91-20-307/25/23 11:228.3 1.7 1 2-Nitroaniline ND ug/L 07/25/23 23:53 88-74-407/25/23 11:2216.7 2.5 1 3-Nitroaniline ND ug/L 07/25/23 23:53 99-09-207/25/23 11:2216.7 3.1 1 4-Nitroaniline ND ug/L 07/25/23 23:53 100-01-607/25/23 11:2216.7 4.2 1 Nitrobenzene ND ug/L 07/25/23 23:53 98-95-307/25/23 11:228.3 1.6 1 2-Nitrophenol ND ug/L 07/25/23 23:53 88-75-507/25/23 11:228.3 1.2 1 4-Nitrophenol ND ug/L 07/25/23 23:53 100-02-707/25/23 11:2241.7 5.5 1 N-Nitrosodimethylamine ND ug/L 07/25/23 23:53 62-75-9 v107/25/23 11:228.3 1.6 1 N-Nitroso-di-n-propylamine ND ug/L 07/25/23 23:53 621-64-707/25/23 11:228.3 1.1 1 N-Nitrosodiphenylamine ND ug/L 07/25/23 23:53 86-30-607/25/23 11:228.3 2.5 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/25/23 23:53 108-60-1 v107/25/23 11:228.3 0.96 1 Pentachlorophenol ND ug/L 07/25/23 23:53 87-86-507/25/23 11:2216.7 3.1 1 Phenanthrene ND ug/L 07/25/23 23:53 85-01-807/25/23 11:228.3 1.7 1 Phenol ND ug/L 07/25/23 23:53 108-95-207/25/23 11:228.3 1.1 1 Pyrene ND ug/L 07/25/23 23:53 129-00-007/25/23 11:228.3 1.8 1 1,2,4-Trichlorobenzene ND ug/L 07/25/23 23:53 120-82-107/25/23 11:228.3 1.4 1 2,4,5-Trichlorophenol ND ug/L 07/25/23 23:53 95-95-407/25/23 11:228.3 1.2 1 2,4,6-Trichlorophenol ND ug/L 07/25/23 23:53 88-06-207/25/23 11:228.3 1.3 1 Surrogates Nitrobenzene-d5 (S)70 %07/25/23 23:53 4165-60-007/25/23 11:2210-138 1 2-Fluorobiphenyl (S)56 %07/25/23 23:53 321-60-807/25/23 11:2210-130 1 Terphenyl-d14 (S)124 %07/25/23 23:53 1718-51-007/25/23 11:2219-191 1 Phenol-d6 (S)33 %07/25/23 23:53 13127-88-307/25/23 11:2210-130 1 2-Fluorophenol (S)45 %07/25/23 23:53 367-12-407/25/23 11:2210-130 1 2,4,6-Tribromophenol (S)111 %07/25/23 23:53 118-79-607/25/23 11:2210-164 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 66 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-12 Lab ID: 92678743016 Collected: 07/20/23 14:15 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level Acetone ND ug/L 07/27/23 01:27 67-64-125.0 5.1 1 Benzene ND ug/L 07/27/23 01:27 71-43-21.0 0.34 1 Bromobenzene ND ug/L 07/27/23 01:27 108-86-11.0 0.29 1 Bromochloromethane ND ug/L 07/27/23 01:27 74-97-51.0 0.47 1 Bromodichloromethane ND ug/L 07/27/23 01:27 75-27-41.0 0.31 1 Bromoform ND ug/L 07/27/23 01:27 75-25-21.0 0.34 1 Bromomethane ND ug/L 07/27/23 01:27 74-83-92.0 1.7 1 2-Butanone (MEK)ND ug/L 07/27/23 01:27 78-93-35.0 4.0 1 Carbon tetrachloride ND ug/L 07/27/23 01:27 56-23-51.0 0.33 1 Chlorobenzene ND ug/L 07/27/23 01:27 108-90-71.0 0.28 1 Chloroethane ND ug/L 07/27/23 01:27 75-00-31.0 0.65 1 Chloroform ND ug/L 07/27/23 01:27 67-66-31.0 0.43 1 Chloromethane 1.6 ug/L 07/27/23 01:27 74-87-31.0 0.54 1 2-Chlorotoluene ND ug/L 07/27/23 01:27 95-49-81.0 0.32 1 4-Chlorotoluene ND ug/L 07/27/23 01:27 106-43-41.0 0.32 1 1,2-Dibromo-3-chloropropane ND ug/L 07/27/23 01:27 96-12-82.0 0.34 1 Dibromochloromethane ND ug/L 07/27/23 01:27 124-48-11.0 0.36 1 1,2-Dibromoethane (EDB)ND ug/L 07/27/23 01:27 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/27/23 01:27 74-95-31.0 0.39 1 1,2-Dichlorobenzene ND ug/L 07/27/23 01:27 95-50-11.0 0.34 1 1,3-Dichlorobenzene ND ug/L 07/27/23 01:27 541-73-11.0 0.34 1 1,4-Dichlorobenzene ND ug/L 07/27/23 01:27 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/27/23 01:27 75-71-81.0 0.35 1 1,1-Dichloroethane ND ug/L 07/27/23 01:27 75-34-31.0 0.37 1 1,2-Dichloroethane ND ug/L 07/27/23 01:27 107-06-21.0 0.32 1 1,1-Dichloroethene ND ug/L 07/27/23 01:27 75-35-41.0 0.35 1 cis-1,2-Dichloroethene ND ug/L 07/27/23 01:27 156-59-21.0 0.38 1 trans-1,2-Dichloroethene ND ug/L 07/27/23 01:27 156-60-51.0 0.40 1 1,2-Dichloropropane ND ug/L 07/27/23 01:27 78-87-51.0 0.36 1 1,3-Dichloropropane ND ug/L 07/27/23 01:27 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/27/23 01:27 594-20-71.0 0.39 1 1,1-Dichloropropene ND ug/L 07/27/23 01:27 563-58-61.0 0.43 1 cis-1,3-Dichloropropene ND ug/L 07/27/23 01:27 10061-01-51.0 0.36 1 trans-1,3-Dichloropropene ND ug/L 07/27/23 01:27 10061-02-61.0 0.36 1 Diisopropyl ether ND ug/L 07/27/23 01:27 108-20-31.0 0.31 1 Ethylbenzene ND ug/L 07/27/23 01:27 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/27/23 01:27 87-68-32.0 1.5 1 2-Hexanone ND ug/L 07/27/23 01:27 591-78-65.0 0.48 1 p-Isopropyltoluene ND ug/L 07/27/23 01:27 99-87-61.0 0.41 1 Methylene Chloride ND ug/L 07/27/23 01:27 75-09-25.0 2.0 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/27/23 01:27 108-10-15.0 2.7 1 Methyl-tert-butyl ether ND ug/L 07/27/23 01:27 1634-04-41.0 0.42 1 Naphthalene ND ug/L 07/27/23 01:27 91-20-31.0 0.64 1 Styrene ND ug/L 07/27/23 01:27 100-42-51.0 0.29 1 1,1,1,2-Tetrachloroethane ND ug/L 07/27/23 01:27 630-20-61.0 0.31 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 67 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-12 Lab ID: 92678743016 Collected: 07/20/23 14:15 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level 1,1,2,2-Tetrachloroethane ND ug/L 07/27/23 01:27 79-34-51.0 0.22 1 Tetrachloroethene ND ug/L 07/27/23 01:27 127-18-41.0 0.29 1 Toluene ND ug/L 07/27/23 01:27 108-88-31.0 0.24 1 1,2,3-Trichlorobenzene ND ug/L 07/27/23 01:27 87-61-61.0 0.81 1 1,2,4-Trichlorobenzene ND ug/L 07/27/23 01:27 120-82-11.0 0.64 1 1,1,1-Trichloroethane ND ug/L 07/27/23 01:27 71-55-61.0 0.33 1 1,1,2-Trichloroethane ND ug/L 07/27/23 01:27 79-00-51.0 0.32 1 Trichloroethene ND ug/L 07/27/23 01:27 79-01-61.0 0.38 1 Trichlorofluoromethane ND ug/L 07/27/23 01:27 75-69-41.0 0.30 1 1,2,3-Trichloropropane ND ug/L 07/27/23 01:27 96-18-41.0 0.26 1 Vinyl acetate ND ug/L 07/27/23 01:27 108-05-42.0 1.3 1 Vinyl chloride ND ug/L 07/27/23 01:27 75-01-41.0 0.39 1 Xylene (Total)ND ug/L 07/27/23 01:27 1330-20-71.0 0.34 1 m&p-Xylene ND ug/L 07/27/23 01:27 179601-23-12.0 0.71 1 o-Xylene ND ug/L 07/27/23 01:27 95-47-61.0 0.34 1 Surrogates 4-Bromofluorobenzene (S)100 %07/27/23 01:27 460-00-470-130 1 1,2-Dichloroethane-d4 (S)103 %07/27/23 01:27 17060-07-070-130 1 Toluene-d8 (S)100 %07/27/23 01:27 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 68 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-DUP Lab ID: 92678743017 Collected: 07/20/23 00:00 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3010A Pace Analytical Services - Asheville 6020 MET ICPMS Arsenic 0.79J ug/L 07/27/23 02:42 7440-38-207/26/23 11:461.0 0.087 1 Barium 46.7 ug/L 07/27/23 02:42 7440-39-307/26/23 11:461.0 0.21 1 Cadmium 0.38 ug/L 07/27/23 02:42 7440-43-907/26/23 11:460.20 0.060 1 Chromium 0.71J ug/L 07/27/23 02:42 7440-47-307/26/23 11:461.0 0.50 1 Lead 0.079J ug/L 07/27/23 02:42 7439-92-107/26/23 11:461.0 0.077 1 Selenium 2.2 ug/L 07/27/23 02:42 7782-49-207/26/23 11:462.0 0.072 1 Silver ND ug/L 07/27/23 02:42 7440-22-407/26/23 11:460.40 0.070 1 Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services - Asheville 7470 Mercury Mercury ND ug/L 07/31/23 14:37 7439-97-607/31/23 09:370.20 0.12 1 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Acenaphthene ND ug/L 07/25/23 22:35 83-32-907/25/23 11:228.7 1.7 1 Acenaphthylene ND ug/L 07/25/23 22:35 208-96-807/25/23 11:228.7 1.7 1 Aniline ND ug/L 07/25/23 22:35 62-53-307/25/23 11:228.7 1.4 1 Anthracene ND ug/L 07/25/23 22:35 120-12-707/25/23 11:228.7 2.0 1 Benzo(a)anthracene ND ug/L 07/25/23 22:35 56-55-307/25/23 11:228.7 2.3 1 Benzo(a)pyrene ND ug/L 07/25/23 22:35 50-32-807/25/23 11:228.7 2.4 1 Benzo(b)fluoranthene ND ug/L 07/25/23 22:35 205-99-207/25/23 11:228.7 2.3 1 Benzo(g,h,i)perylene ND ug/L 07/25/23 22:35 191-24-207/25/23 11:228.7 2.5 1 Benzo(k)fluoranthene ND ug/L 07/25/23 22:35 207-08-907/25/23 11:228.7 2.4 1 Benzoic Acid 22.0J ug/L 07/25/23 22:35 65-85-0 C707/25/23 11:2243.5 19.1 1 Benzyl alcohol ND ug/L 07/25/23 22:35 100-51-607/25/23 11:2217.4 2.5 1 4-Bromophenylphenyl ether ND ug/L 07/25/23 22:35 101-55-307/25/23 11:228.7 1.5 1 Butylbenzylphthalate ND ug/L 07/25/23 22:35 85-68-707/25/23 11:228.7 2.7 1 4-Chloro-3-methylphenol ND ug/L 07/25/23 22:35 59-50-707/25/23 11:228.7 2.9 1 4-Chloroaniline ND ug/L 07/25/23 22:35 106-47-807/25/23 11:2217.4 3.2 1 bis(2-Chloroethoxy)methane ND ug/L 07/25/23 22:35 111-91-107/25/23 11:228.7 1.6 1 bis(2-Chloroethyl) ether ND ug/L 07/25/23 22:35 111-44-407/25/23 11:228.7 1.7 1 2-Chloronaphthalene ND ug/L 07/25/23 22:35 91-58-707/25/23 11:228.7 1.5 1 2-Chlorophenol ND ug/L 07/25/23 22:35 95-57-807/25/23 11:228.7 1.0 1 4-Chlorophenylphenyl ether ND ug/L 07/25/23 22:35 7005-72-307/25/23 11:228.7 1.7 1 Chrysene ND ug/L 07/25/23 22:35 218-01-907/25/23 11:228.7 2.4 1 Dibenz(a,h)anthracene ND ug/L 07/25/23 22:35 53-70-307/25/23 11:228.7 2.6 1 Dibenzofuran ND ug/L 07/25/23 22:35 132-64-907/25/23 11:228.7 1.8 1 1,2-Dichlorobenzene ND ug/L 07/25/23 22:35 95-50-107/25/23 11:228.7 1.6 1 1,3-Dichlorobenzene ND ug/L 07/25/23 22:35 541-73-107/25/23 11:228.7 1.4 1 1,4-Dichlorobenzene ND ug/L 07/25/23 22:35 106-46-707/25/23 11:228.7 1.5 1 3,3'-Dichlorobenzidine ND ug/L 07/25/23 22:35 91-94-107/25/23 11:2217.4 7.1 1 2,4-Dichlorophenol ND ug/L 07/25/23 22:35 120-83-207/25/23 11:228.7 1.2 1 Diethylphthalate ND ug/L 07/25/23 22:35 84-66-207/25/23 11:228.7 1.8 1 2,4-Dimethylphenol ND ug/L 07/25/23 22:35 105-67-907/25/23 11:228.7 1.5 1 Dimethylphthalate ND ug/L 07/25/23 22:35 131-11-307/25/23 11:228.7 1.9 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 69 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-DUP Lab ID: 92678743017 Collected: 07/20/23 00:00 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 8270E RVE Di-n-butylphthalate ND ug/L 07/25/23 22:35 84-74-207/25/23 11:228.7 1.9 1 4,6-Dinitro-2-methylphenol ND ug/L 07/25/23 22:35 534-52-107/25/23 11:2217.4 6.8 1 2,4-Dinitrophenol ND ug/L 07/25/23 22:35 51-28-507/25/23 11:2243.5 22.6 1 2,4-Dinitrotoluene ND ug/L 07/25/23 22:35 121-14-207/25/23 11:228.7 1.4 1 2,6-Dinitrotoluene ND ug/L 07/25/23 22:35 606-20-207/25/23 11:228.7 1.5 1 Di-n-octylphthalate ND ug/L 07/25/23 22:35 117-84-007/25/23 11:228.7 3.4 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/25/23 22:35 117-81-707/25/23 11:225.2 3.2 1 Fluoranthene ND ug/L 07/25/23 22:35 206-44-007/25/23 11:228.7 1.9 1 Fluorene ND ug/L 07/25/23 22:35 86-73-707/25/23 11:228.7 1.8 1 Hexachloro-1,3-butadiene ND ug/L 07/25/23 22:35 87-68-307/25/23 11:228.7 1.5 1 Hexachlorobenzene ND ug/L 07/25/23 22:35 118-74-107/25/23 11:228.7 1.9 1 Hexachlorocyclopentadiene ND ug/L 07/25/23 22:35 77-47-407/25/23 11:228.7 1.4 1 Hexachloroethane ND ug/L 07/25/23 22:35 67-72-107/25/23 11:228.7 1.2 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/25/23 22:35 193-39-507/25/23 11:228.7 2.5 1 Isophorone ND ug/L 07/25/23 22:35 78-59-107/25/23 11:228.7 1.4 1 1-Methylnaphthalene ND ug/L 07/25/23 22:35 90-12-007/25/23 11:228.7 1.8 1 2-Methylnaphthalene ND ug/L 07/25/23 22:35 91-57-607/25/23 11:228.7 1.6 1 2-Methylphenol(o-Cresol)ND ug/L 07/25/23 22:35 95-48-707/25/23 11:228.7 1.6 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/25/23 22:35 15831-10-407/25/23 11:228.7 1.1 1 Naphthalene ND ug/L 07/25/23 22:35 91-20-307/25/23 11:228.7 1.8 1 2-Nitroaniline ND ug/L 07/25/23 22:35 88-74-407/25/23 11:2217.4 2.6 1 3-Nitroaniline ND ug/L 07/25/23 22:35 99-09-207/25/23 11:2217.4 3.3 1 4-Nitroaniline ND ug/L 07/25/23 22:35 100-01-607/25/23 11:2217.4 4.4 1 Nitrobenzene ND ug/L 07/25/23 22:35 98-95-307/25/23 11:228.7 1.6 1 2-Nitrophenol ND ug/L 07/25/23 22:35 88-75-507/25/23 11:228.7 1.2 1 4-Nitrophenol ND ug/L 07/25/23 22:35 100-02-707/25/23 11:2243.5 5.7 1 N-Nitrosodimethylamine ND ug/L 07/25/23 22:35 62-75-907/25/23 11:228.7 1.6 1 N-Nitroso-di-n-propylamine ND ug/L 07/25/23 22:35 621-64-707/25/23 11:228.7 1.2 1 N-Nitrosodiphenylamine ND ug/L 07/25/23 22:35 86-30-607/25/23 11:228.7 2.6 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/25/23 22:35 108-60-107/25/23 11:228.7 1.0 1 Pentachlorophenol ND ug/L 07/25/23 22:35 87-86-507/25/23 11:2217.4 3.3 1 Phenanthrene ND ug/L 07/25/23 22:35 85-01-807/25/23 11:228.7 1.7 1 Phenol ND ug/L 07/25/23 22:35 108-95-207/25/23 11:228.7 1.2 1 Pyrene ND ug/L 07/25/23 22:35 129-00-007/25/23 11:228.7 1.9 1 1,2,4-Trichlorobenzene ND ug/L 07/25/23 22:35 120-82-107/25/23 11:228.7 1.5 1 2,4,5-Trichlorophenol ND ug/L 07/25/23 22:35 95-95-407/25/23 11:228.7 1.2 1 2,4,6-Trichlorophenol ND ug/L 07/25/23 22:35 88-06-207/25/23 11:228.7 1.3 1 Surrogates Nitrobenzene-d5 (S)55 %07/25/23 22:35 4165-60-007/25/23 11:2210-138 1 2-Fluorobiphenyl (S)47 %07/25/23 22:35 321-60-807/25/23 11:2210-130 1 Terphenyl-d14 (S)112 %07/25/23 22:35 1718-51-007/25/23 11:2219-191 1 Phenol-d6 (S)29 %07/25/23 22:35 13127-88-307/25/23 11:2210-130 1 2-Fluorophenol (S)36 %07/25/23 22:35 367-12-407/25/23 11:2210-130 1 2,4,6-Tribromophenol (S)76 %07/25/23 22:35 118-79-607/25/23 11:2210-164 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 70 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-DUP Lab ID: 92678743017 Collected: 07/20/23 00:00 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level Acetone ND ug/L 07/27/23 02:03 67-64-162.5 12.8 2.5 Benzene ND ug/L 07/27/23 02:03 71-43-22.5 0.86 2.5 Bromobenzene ND ug/L 07/27/23 02:03 108-86-12.5 0.72 2.5 Bromochloromethane ND ug/L 07/27/23 02:03 74-97-52.5 1.2 2.5 Bromodichloromethane ND ug/L 07/27/23 02:03 75-27-42.5 0.77 2.5 Bromoform ND ug/L 07/27/23 02:03 75-25-22.5 0.85 2.5 Bromomethane ND ug/L 07/27/23 02:03 74-83-95.0 4.2 2.5 2-Butanone (MEK)ND ug/L 07/27/23 02:03 78-93-312.5 9.9 2.5 Carbon tetrachloride ND ug/L 07/27/23 02:03 56-23-52.5 0.83 2.5 Chlorobenzene ND ug/L 07/27/23 02:03 108-90-72.5 0.71 2.5 Chloroethane ND ug/L 07/27/23 02:03 75-00-32.5 1.6 2.5 Chloroform ND ug/L 07/27/23 02:03 67-66-32.5 1.1 2.5 Chloromethane ND ug/L 07/27/23 02:03 74-87-32.5 1.4 2.5 2-Chlorotoluene ND ug/L 07/27/23 02:03 95-49-82.5 0.80 2.5 4-Chlorotoluene ND ug/L 07/27/23 02:03 106-43-42.5 0.81 2.5 1,2-Dibromo-3-chloropropane ND ug/L 07/27/23 02:03 96-12-85.0 0.85 2.5 Dibromochloromethane ND ug/L 07/27/23 02:03 124-48-12.5 0.90 2.5 1,2-Dibromoethane (EDB)ND ug/L 07/27/23 02:03 106-93-42.5 0.68 2.5 Dibromomethane ND ug/L 07/27/23 02:03 74-95-32.5 0.98 2.5 1,2-Dichlorobenzene ND ug/L 07/27/23 02:03 95-50-12.5 0.85 2.5 1,3-Dichlorobenzene ND ug/L 07/27/23 02:03 541-73-12.5 0.85 2.5 1,4-Dichlorobenzene ND ug/L 07/27/23 02:03 106-46-72.5 0.83 2.5 Dichlorodifluoromethane ND ug/L 07/27/23 02:03 75-71-82.5 0.86 2.5 1,1-Dichloroethane ND ug/L 07/27/23 02:03 75-34-32.5 0.92 2.5 1,2-Dichloroethane ND ug/L 07/27/23 02:03 107-06-22.5 0.80 2.5 1,1-Dichloroethene ND ug/L 07/27/23 02:03 75-35-42.5 0.87 2.5 cis-1,2-Dichloroethene ND ug/L 07/27/23 02:03 156-59-22.5 0.96 2.5 trans-1,2-Dichloroethene ND ug/L 07/27/23 02:03 156-60-52.5 0.99 2.5 1,2-Dichloropropane ND ug/L 07/27/23 02:03 78-87-52.5 0.89 2.5 1,3-Dichloropropane ND ug/L 07/27/23 02:03 142-28-92.5 0.71 2.5 2,2-Dichloropropane ND ug/L 07/27/23 02:03 594-20-72.5 0.97 2.5 1,1-Dichloropropene ND ug/L 07/27/23 02:03 563-58-62.5 1.1 2.5 cis-1,3-Dichloropropene ND ug/L 07/27/23 02:03 10061-01-52.5 0.91 2.5 trans-1,3-Dichloropropene ND ug/L 07/27/23 02:03 10061-02-62.5 0.91 2.5 Diisopropyl ether ND ug/L 07/27/23 02:03 108-20-32.5 0.77 2.5 Ethylbenzene ND ug/L 07/27/23 02:03 100-41-42.5 0.76 2.5 Hexachloro-1,3-butadiene ND ug/L 07/27/23 02:03 87-68-35.0 3.8 2.5 2-Hexanone ND ug/L 07/27/23 02:03 591-78-612.5 1.2 2.5 p-Isopropyltoluene ND ug/L 07/27/23 02:03 99-87-62.5 1.0 2.5 Methylene Chloride 5.3J ug/L 07/27/23 02:03 75-09-2 C912.5 4.9 2.5 4-Methyl-2-pentanone (MIBK)ND ug/L 07/27/23 02:03 108-10-112.5 6.8 2.5 Methyl-tert-butyl ether ND ug/L 07/27/23 02:03 1634-04-42.5 1.1 2.5 Naphthalene ND ug/L 07/27/23 02:03 91-20-32.5 1.6 2.5 Styrene ND ug/L 07/27/23 02:03 100-42-52.5 0.73 2.5 1,1,1,2-Tetrachloroethane ND ug/L 07/27/23 02:03 630-20-62.5 0.78 2.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 71 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TMW-DUP Lab ID: 92678743017 Collected: 07/20/23 00:00 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level 1,1,2,2-Tetrachloroethane ND ug/L 07/27/23 02:03 79-34-52.5 0.56 2.5 Tetrachloroethene 327 ug/L 07/27/23 02:03 127-18-42.5 0.73 2.5 Toluene ND ug/L 07/27/23 02:03 108-88-32.5 0.60 2.5 1,2,3-Trichlorobenzene ND ug/L 07/27/23 02:03 87-61-62.5 2.0 2.5 1,2,4-Trichlorobenzene ND ug/L 07/27/23 02:03 120-82-12.5 1.6 2.5 1,1,1-Trichloroethane ND ug/L 07/27/23 02:03 71-55-62.5 0.83 2.5 1,1,2-Trichloroethane ND ug/L 07/27/23 02:03 79-00-52.5 0.81 2.5 Trichloroethene 1.1J ug/L 07/27/23 02:03 79-01-62.5 0.96 2.5 Trichlorofluoromethane ND ug/L 07/27/23 02:03 75-69-42.5 0.74 2.5 1,2,3-Trichloropropane ND ug/L 07/27/23 02:03 96-18-42.5 0.65 2.5 Vinyl acetate ND ug/L 07/27/23 02:03 108-05-45.0 3.3 2.5 Vinyl chloride ND ug/L 07/27/23 02:03 75-01-42.5 0.96 2.5 Xylene (Total)ND ug/L 07/27/23 02:03 1330-20-72.5 0.84 2.5 m&p-Xylene ND ug/L 07/27/23 02:03 179601-23-15.0 1.8 2.5 o-Xylene ND ug/L 07/27/23 02:03 95-47-62.5 0.84 2.5 Surrogates 4-Bromofluorobenzene (S)98 %07/27/23 02:03 460-00-470-130 2.5 1,2-Dichloroethane-d4 (S)103 %07/27/23 02:03 17060-07-070-130 2.5 Toluene-d8 (S)99 %07/27/23 02:03 2037-26-570-130 2.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 72 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: SB-DUP Lab ID: 92678743018 Collected: 07/19/23 00:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: 3050B Pace National - Mt. Juliet Metals (ICPMS) 6020B Arsenic 11.8 mg/kg 08/01/23 16:00 7440-38-207/27/23 03:221.26 0.126 5 Barium 27.1 mg/kg 08/01/23 16:00 7440-39-307/27/23 03:223.16 0.192 5 Cadmium 0.211J mg/kg 08/01/23 16:00 7440-43-9 J07/27/23 03:221.26 0.108 5 Chromium 31.3 mg/kg 08/01/23 16:00 7440-47-307/27/23 03:226.32 0.374 5 Lead 11.8 mg/kg 08/01/23 16:00 7439-92-107/27/23 03:222.53 0.125 5 Selenium 2.14J mg/kg 08/01/23 16:00 7782-49-2 J07/27/23 03:223.16 0.227 5 Silver ND mg/kg 08/01/23 16:00 7440-22-407/27/23 03:220.632 0.109 5 Analytical Method: EPA 7471B Preparation Method: 7471A Pace National - Mt. Juliet Mercury 7471B Mercury 0.0698 mg/kg 07/30/23 18:48 7439-97-607/28/23 10:460.0505 0.0227 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene 174J ug/kg 07/30/23 13:54 83-32-907/27/23 18:30402 141 1 Acenaphthylene ND ug/kg 07/30/23 13:54 208-96-807/27/23 18:30402 141 1 Aniline ND ug/kg 07/30/23 13:54 62-53-307/27/23 18:30402 157 1 Anthracene 408 ug/kg 07/30/23 13:54 120-12-707/27/23 18:30402 132 1 Benzo(a)anthracene 1320 ug/kg 07/30/23 13:54 56-55-307/27/23 18:30402 134 1 Benzo(a)pyrene 1150 ug/kg 07/30/23 13:54 50-32-807/27/23 18:30402 139 1 Benzo(b)fluoranthene 1520 ug/kg 07/30/23 13:54 205-99-207/27/23 18:30402 134 1 Benzo(g,h,i)perylene 871 ug/kg 07/30/23 13:54 191-24-207/27/23 18:30402 156 1 Benzo(k)fluoranthene 584 ug/kg 07/30/23 13:54 207-08-907/27/23 18:30402 141 1 Benzoic Acid ND ug/kg 07/30/23 13:54 65-85-007/27/23 18:302010 864 1 Benzyl alcohol ND ug/kg 07/30/23 13:54 100-51-607/27/23 18:30805 305 1 4-Bromophenylphenyl ether ND ug/kg 07/30/23 13:54 101-55-307/27/23 18:30402 155 1 Butylbenzylphthalate ND ug/kg 07/30/23 13:54 85-68-707/27/23 18:30402 169 1 4-Chloro-3-methylphenol ND ug/kg 07/30/23 13:54 59-50-707/27/23 18:30805 283 1 4-Chloroaniline ND ug/kg 07/30/23 13:54 106-47-807/27/23 18:30805 316 1 bis(2-Chloroethoxy)methane ND ug/kg 07/30/23 13:54 111-91-107/27/23 18:30402 167 1 bis(2-Chloroethyl) ether ND ug/kg 07/30/23 13:54 111-44-407/27/23 18:30402 151 1 2-Chloronaphthalene ND ug/kg 07/30/23 13:54 91-58-707/27/23 18:30402 160 1 2-Chlorophenol ND ug/kg 07/30/23 13:54 95-57-807/27/23 18:30402 151 1 4-Chlorophenylphenyl ether ND ug/kg 07/30/23 13:54 7005-72-307/27/23 18:30402 150 1 Chrysene 1420 ug/kg 07/30/23 13:54 218-01-907/27/23 18:30402 146 1 Dibenz(a,h)anthracene 256J ug/kg 07/30/23 13:54 53-70-307/27/23 18:30402 155 1 Dibenzofuran ND ug/kg 07/30/23 13:54 132-64-907/27/23 18:30402 145 1 1,2-Dichlorobenzene ND ug/kg 07/30/23 13:54 95-50-107/27/23 18:30402 145 1 1,3-Dichlorobenzene ND ug/kg 07/30/23 13:54 541-73-107/27/23 18:30402 143 1 1,4-Dichlorobenzene ND ug/kg 07/30/23 13:54 106-46-707/27/23 18:30402 154 1 3,3'-Dichlorobenzidine ND ug/kg 07/30/23 13:54 91-94-107/27/23 18:30805 272 1 2,4-Dichlorophenol ND ug/kg 07/30/23 13:54 120-83-207/27/23 18:30402 157 1 Diethylphthalate ND ug/kg 07/30/23 13:54 84-66-207/27/23 18:30402 148 1 2,4-Dimethylphenol ND ug/kg 07/30/23 13:54 105-67-9 v107/27/23 18:30402 167 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 73 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: SB-DUP Lab ID: 92678743018 Collected: 07/19/23 00:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 07/30/23 13:54 131-11-307/27/23 18:30402 146 1 Di-n-butylphthalate ND ug/kg 07/30/23 13:54 84-74-207/27/23 18:30402 135 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/30/23 13:54 534-52-107/27/23 18:30805 376 1 2,4-Dinitrophenol ND ug/kg 07/30/23 13:54 51-28-507/27/23 18:302010 1240 1 2,4-Dinitrotoluene ND ug/kg 07/30/23 13:54 121-14-207/27/23 18:30402 155 1 2,6-Dinitrotoluene ND ug/kg 07/30/23 13:54 606-20-207/27/23 18:30402 148 1 Di-n-octylphthalate ND ug/kg 07/30/23 13:54 117-84-007/27/23 18:30402 158 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/30/23 13:54 117-81-707/27/23 18:30402 156 1 Fluoranthene 2640 ug/kg 07/30/23 13:54 206-44-007/27/23 18:30402 138 1 Fluorene ND ug/kg 07/30/23 13:54 86-73-707/27/23 18:30402 141 1 Hexachloro-1,3-butadiene ND ug/kg 07/30/23 13:54 87-68-307/27/23 18:30402 174 1 Hexachlorobenzene ND ug/kg 07/30/23 13:54 118-74-107/27/23 18:30402 157 1 Hexachlorocyclopentadiene ND ug/kg 07/30/23 13:54 77-47-4 v207/27/23 18:30402 230 1 Hexachloroethane ND ug/kg 07/30/23 13:54 67-72-107/27/23 18:30402 154 1 Indeno(1,2,3-cd)pyrene 757 ug/kg 07/30/23 13:54 193-39-507/27/23 18:30402 158 1 Isophorone ND ug/kg 07/30/23 13:54 78-59-107/27/23 18:30402 179 1 1-Methylnaphthalene ND ug/kg 07/30/23 13:54 90-12-007/27/23 18:30402 141 1 2-Methylnaphthalene ND ug/kg 07/30/23 13:54 91-57-607/27/23 18:30402 161 1 2-Methylphenol(o-Cresol)ND ug/kg 07/30/23 13:54 95-48-707/27/23 18:30402 165 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/30/23 13:54 15831-10-407/27/23 18:30402 162 1 Naphthalene ND ug/kg 07/30/23 13:54 91-20-307/27/23 18:30402 137 1 2-Nitroaniline ND ug/kg 07/30/23 13:54 88-74-407/27/23 18:302010 329 1 3-Nitroaniline ND ug/kg 07/30/23 13:54 99-09-207/27/23 18:302010 316 1 4-Nitroaniline ND ug/kg 07/30/23 13:54 100-01-607/27/23 18:30805 306 1 Nitrobenzene ND ug/kg 07/30/23 13:54 98-95-307/27/23 18:30402 187 1 2-Nitrophenol ND ug/kg 07/30/23 13:54 88-75-507/27/23 18:30402 174 1 4-Nitrophenol ND ug/kg 07/30/23 13:54 100-02-7 v207/27/23 18:302010 778 1 N-Nitrosodimethylamine ND ug/kg 07/30/23 13:54 62-75-907/27/23 18:30402 135 1 N-Nitroso-di-n-propylamine ND ug/kg 07/30/23 13:54 621-64-707/27/23 18:30402 151 1 N-Nitrosodiphenylamine ND ug/kg 07/30/23 13:54 86-30-607/27/23 18:30402 143 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/30/23 13:54 108-60-107/27/23 18:30402 191 1 Pentachlorophenol ND ug/kg 07/30/23 13:54 87-86-5 v207/27/23 18:30805 394 1 Phenanthrene 1960 ug/kg 07/30/23 13:54 85-01-807/27/23 18:30402 132 1 Phenol ND ug/kg 07/30/23 13:54 108-95-207/27/23 18:30402 179 1 Pyrene 2490 ug/kg 07/30/23 13:54 129-00-007/27/23 18:30402 163 1 Pyridine ND ug/kg 07/30/23 13:54 110-86-107/27/23 18:30402 127 1 1,2,4-Trichlorobenzene ND ug/kg 07/30/23 13:54 120-82-107/27/23 18:30402 158 1 2,4,5-Trichlorophenol ND ug/kg 07/30/23 13:54 95-95-407/27/23 18:30402 184 1 2,4,6-Trichlorophenol ND ug/kg 07/30/23 13:54 88-06-207/27/23 18:30402 166 1 Surrogates Nitrobenzene-d5 (S)59 %07/30/23 13:54 4165-60-007/27/23 18:3010-130 1 2-Fluorobiphenyl (S)63 %07/30/23 13:54 321-60-807/27/23 18:3010-130 1 Terphenyl-d14 (S)59 %07/30/23 13:54 1718-51-007/27/23 18:3010-130 1 Phenol-d6 (S)51 %07/30/23 13:54 13127-88-307/27/23 18:3010-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 74 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: SB-DUP Lab ID: 92678743018 Collected: 07/19/23 00:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)50 %07/30/23 13:54 367-12-407/27/23 18:3010-130 1 2,4,6-Tribromophenol (S)62 %07/30/23 13:54 118-79-607/27/23 18:3010-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 07/25/23 20:03 67-64-107/25/23 18:31138 44.3 1 Benzene ND ug/kg 07/25/23 20:03 71-43-207/25/23 18:316.9 2.7 1 Bromobenzene ND ug/kg 07/25/23 20:03 108-86-107/25/23 18:316.9 2.2 1 Bromochloromethane ND ug/kg 07/25/23 20:03 74-97-507/25/23 18:316.9 2.0 1 Bromodichloromethane ND ug/kg 07/25/23 20:03 75-27-407/25/23 18:316.9 2.7 1 Bromoform ND ug/kg 07/25/23 20:03 75-25-207/25/23 18:316.9 2.4 1 Bromomethane ND ug/kg 07/25/23 20:03 74-83-9 IH07/25/23 18:3127.6 21.4 1 2-Butanone (MEK)ND ug/kg 07/25/23 20:03 78-93-307/25/23 18:31138 33.1 1 n-Butylbenzene ND ug/kg 07/25/23 20:03 104-51-807/25/23 18:316.9 4.3 1 sec-Butylbenzene ND ug/kg 07/25/23 20:03 135-98-807/25/23 18:316.9 3.0 1 tert-Butylbenzene ND ug/kg 07/25/23 20:03 98-06-607/25/23 18:316.9 2.5 1 Carbon tetrachloride ND ug/kg 07/25/23 20:03 56-23-507/25/23 18:316.9 2.6 1 Chlorobenzene ND ug/kg 07/25/23 20:03 108-90-707/25/23 18:316.9 4.0 1 Chloroethane ND ug/kg 07/25/23 20:03 75-00-307/25/23 18:3113.8 5.3 1 Chloroform ND ug/kg 07/25/23 20:03 67-66-307/25/23 18:316.9 5.8 1 Chloromethane ND ug/kg 07/25/23 20:03 74-87-307/25/23 18:3113.8 5.8 1 2-Chlorotoluene ND ug/kg 07/25/23 20:03 95-49-807/25/23 18:316.9 2.4 1 4-Chlorotoluene ND ug/kg 07/25/23 20:03 106-43-407/25/23 18:316.9 3.8 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/25/23 20:03 96-12-807/25/23 18:316.9 2.7 1 Dibromochloromethane ND ug/kg 07/25/23 20:03 124-48-107/25/23 18:316.9 3.9 1 1,2-Dibromoethane (EDB)ND ug/kg 07/25/23 20:03 106-93-407/25/23 18:316.9 3.0 1 Dibromomethane ND ug/kg 07/25/23 20:03 74-95-307/25/23 18:316.9 1.5 1 1,2-Dichlorobenzene ND ug/kg 07/25/23 20:03 95-50-107/25/23 18:316.9 2.5 1 1,3-Dichlorobenzene ND ug/kg 07/25/23 20:03 541-73-107/25/23 18:316.9 2.1 1 1,4-Dichlorobenzene ND ug/kg 07/25/23 20:03 106-46-707/25/23 18:316.9 1.8 1 Dichlorodifluoromethane ND ug/kg 07/25/23 20:03 75-71-807/25/23 18:3113.8 7.0 1 1,1-Dichloroethane ND ug/kg 07/25/23 20:03 75-34-307/25/23 18:316.9 2.8 1 1,2-Dichloroethane ND ug/kg 07/25/23 20:03 107-06-207/25/23 18:316.9 4.6 1 1,1-Dichloroethene ND ug/kg 07/25/23 20:03 75-35-407/25/23 18:316.9 2.8 1 cis-1,2-Dichloroethene ND ug/kg 07/25/23 20:03 156-59-207/25/23 18:316.9 2.4 1 trans-1,2-Dichloroethene ND ug/kg 07/25/23 20:03 156-60-507/25/23 18:316.9 5.9 1 1,2-Dichloropropane ND ug/kg 07/25/23 20:03 78-87-507/25/23 18:316.9 2.1 1 1,3-Dichloropropane ND ug/kg 07/25/23 20:03 142-28-907/25/23 18:316.9 2.2 1 2,2-Dichloropropane ND ug/kg 07/25/23 20:03 594-20-7 v207/25/23 18:316.9 5.2 1 1,1-Dichloropropene ND ug/kg 07/25/23 20:03 563-58-607/25/23 18:316.9 3.3 1 cis-1,3-Dichloropropene ND ug/kg 07/25/23 20:03 10061-01-507/25/23 18:316.9 1.9 1 trans-1,3-Dichloropropene ND ug/kg 07/25/23 20:03 10061-02-607/25/23 18:316.9 2.4 1 Diisopropyl ether ND ug/kg 07/25/23 20:03 108-20-307/25/23 18:316.9 1.9 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 75 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: SB-DUP Lab ID: 92678743018 Collected: 07/19/23 00:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene ND ug/kg 07/25/23 20:03 100-41-407/25/23 18:316.9 3.2 1 Hexachloro-1,3-butadiene ND ug/kg 07/25/23 20:03 87-68-307/25/23 18:3113.8 11.3 1 2-Hexanone ND ug/kg 07/25/23 20:03 591-78-607/25/23 18:3168.9 6.6 1 Isopropylbenzene (Cumene)ND ug/kg 07/25/23 20:03 98-82-807/25/23 18:316.9 2.3 1 p-Isopropyltoluene ND ug/kg 07/25/23 20:03 99-87-607/25/23 18:316.9 3.4 1 Methylene Chloride ND ug/kg 07/25/23 20:03 75-09-207/25/23 18:3127.6 18.9 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/25/23 20:03 108-10-107/25/23 18:3168.9 6.6 1 Methyl-tert-butyl ether ND ug/kg 07/25/23 20:03 1634-04-4 v207/25/23 18:316.9 2.6 1 Naphthalene 6.3J ug/kg 07/25/23 20:03 91-20-307/25/23 18:316.9 3.6 1 n-Propylbenzene ND ug/kg 07/25/23 20:03 103-65-107/25/23 18:316.9 2.5 1 Styrene ND ug/kg 07/25/23 20:03 100-42-507/25/23 18:316.9 1.8 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/25/23 20:03 630-20-607/25/23 18:316.9 2.6 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/25/23 20:03 79-34-507/25/23 18:316.9 1.8 1 Tetrachloroethene ND ug/kg 07/25/23 20:03 127-18-407/25/23 18:316.9 2.2 1 Toluene ND ug/kg 07/25/23 20:03 108-88-307/25/23 18:316.9 4.8 1 1,2,3-Trichlorobenzene ND ug/kg 07/25/23 20:03 87-61-607/25/23 18:316.9 5.6 1 1,2,4-Trichlorobenzene ND ug/kg 07/25/23 20:03 120-82-107/25/23 18:316.9 5.8 1 1,1,1-Trichloroethane ND ug/kg 07/25/23 20:03 71-55-607/25/23 18:316.9 3.6 1 1,1,2-Trichloroethane ND ug/kg 07/25/23 20:03 79-00-507/25/23 18:316.9 2.3 1 Trichloroethene ND ug/kg 07/25/23 20:03 79-01-607/25/23 18:316.9 5.6 1 Trichlorofluoromethane ND ug/kg 07/25/23 20:03 75-69-407/25/23 18:316.9 3.8 1 1,2,3-Trichloropropane ND ug/kg 07/25/23 20:03 96-18-407/25/23 18:316.9 3.5 1 1,2,4-Trimethylbenzene ND ug/kg 07/25/23 20:03 95-63-607/25/23 18:316.9 4.1 1 1,3,5-Trimethylbenzene ND ug/kg 07/25/23 20:03 108-67-807/25/23 18:316.9 2.3 1 Vinyl acetate ND ug/kg 07/25/23 20:03 108-05-407/25/23 18:3168.9 14.2 1 Vinyl chloride ND ug/kg 07/25/23 20:03 75-01-4 v207/25/23 18:3113.8 3.5 1 Xylene (Total)ND ug/kg 07/25/23 20:03 1330-20-707/25/23 18:3113.8 3.9 1 m&p-Xylene ND ug/kg 07/25/23 20:03 179601-23-107/25/23 18:3113.8 4.7 1 o-Xylene ND ug/kg 07/25/23 20:03 95-47-607/25/23 18:316.9 3.0 1 Surrogates Toluene-d8 (S)101 %07/25/23 20:03 2037-26-507/25/23 18:3170-130 1 4-Bromofluorobenzene (S)102 %07/25/23 20:03 460-00-407/25/23 18:3170-130 1 1,2-Dichloroethane-d4 (S)107 %07/25/23 20:03 17060-07-007/25/23 18:3170-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 16.9 %07/24/23 14:07 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 79.1 %07/27/23 10:5907/27/23 10:531 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 76 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: SB-DUP Lab ID: 92678743018 Collected: 07/19/23 00:00 Received: 07/21/23 16:37 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 1.44 mg/kg 07/28/23 15:57 18540-29-907/28/23 10:001.26 0.322 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 77 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TRIP BLANK Lab ID: 92678743019 Collected: 07/19/23 00:00 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level Acetone ND ug/L 07/25/23 07:18 67-64-125.0 5.1 1 Benzene ND ug/L 07/25/23 07:18 71-43-21.0 0.34 1 Bromobenzene ND ug/L 07/25/23 07:18 108-86-11.0 0.29 1 Bromochloromethane ND ug/L 07/25/23 07:18 74-97-51.0 0.47 1 Bromodichloromethane ND ug/L 07/25/23 07:18 75-27-41.0 0.31 1 Bromoform ND ug/L 07/25/23 07:18 75-25-21.0 0.34 1 Bromomethane ND ug/L 07/25/23 07:18 74-83-92.0 1.7 1 2-Butanone (MEK)ND ug/L 07/25/23 07:18 78-93-35.0 4.0 1 Carbon tetrachloride ND ug/L 07/25/23 07:18 56-23-51.0 0.33 1 Chlorobenzene ND ug/L 07/25/23 07:18 108-90-71.0 0.28 1 Chloroethane ND ug/L 07/25/23 07:18 75-00-31.0 0.65 1 Chloroform ND ug/L 07/25/23 07:18 67-66-31.0 0.43 1 Chloromethane ND ug/L 07/25/23 07:18 74-87-31.0 0.54 1 2-Chlorotoluene ND ug/L 07/25/23 07:18 95-49-81.0 0.32 1 4-Chlorotoluene ND ug/L 07/25/23 07:18 106-43-41.0 0.32 1 1,2-Dibromo-3-chloropropane ND ug/L 07/25/23 07:18 96-12-82.0 0.34 1 Dibromochloromethane ND ug/L 07/25/23 07:18 124-48-11.0 0.36 1 1,2-Dibromoethane (EDB)ND ug/L 07/25/23 07:18 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/25/23 07:18 74-95-31.0 0.39 1 1,2-Dichlorobenzene ND ug/L 07/25/23 07:18 95-50-11.0 0.34 1 1,3-Dichlorobenzene ND ug/L 07/25/23 07:18 541-73-11.0 0.34 1 1,4-Dichlorobenzene ND ug/L 07/25/23 07:18 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/25/23 07:18 75-71-81.0 0.35 1 1,1-Dichloroethane ND ug/L 07/25/23 07:18 75-34-31.0 0.37 1 1,2-Dichloroethane ND ug/L 07/25/23 07:18 107-06-21.0 0.32 1 1,1-Dichloroethene ND ug/L 07/25/23 07:18 75-35-41.0 0.35 1 cis-1,2-Dichloroethene ND ug/L 07/25/23 07:18 156-59-21.0 0.38 1 trans-1,2-Dichloroethene ND ug/L 07/25/23 07:18 156-60-51.0 0.40 1 1,2-Dichloropropane ND ug/L 07/25/23 07:18 78-87-51.0 0.36 1 1,3-Dichloropropane ND ug/L 07/25/23 07:18 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/25/23 07:18 594-20-71.0 0.39 1 1,1-Dichloropropene ND ug/L 07/25/23 07:18 563-58-61.0 0.43 1 cis-1,3-Dichloropropene ND ug/L 07/25/23 07:18 10061-01-51.0 0.36 1 trans-1,3-Dichloropropene ND ug/L 07/25/23 07:18 10061-02-61.0 0.36 1 Diisopropyl ether ND ug/L 07/25/23 07:18 108-20-31.0 0.31 1 Ethylbenzene ND ug/L 07/25/23 07:18 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/25/23 07:18 87-68-32.0 1.5 1 2-Hexanone ND ug/L 07/25/23 07:18 591-78-65.0 0.48 1 p-Isopropyltoluene ND ug/L 07/25/23 07:18 99-87-61.0 0.41 1 Methylene Chloride ND ug/L 07/25/23 07:18 75-09-25.0 2.0 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/25/23 07:18 108-10-15.0 2.7 1 Methyl-tert-butyl ether ND ug/L 07/25/23 07:18 1634-04-41.0 0.42 1 Naphthalene ND ug/L 07/25/23 07:18 91-20-31.0 0.64 1 Styrene ND ug/L 07/25/23 07:18 100-42-51.0 0.29 1 1,1,1,2-Tetrachloroethane ND ug/L 07/25/23 07:18 630-20-61.0 0.31 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 78 of 147 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92678743 HNY-001 Sample: TRIP BLANK Lab ID: 92678743019 Collected: 07/19/23 00:00 Received: 07/21/23 16:37 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 8260D MSV Low Level 1,1,2,2-Tetrachloroethane ND ug/L 07/25/23 07:18 79-34-51.0 0.22 1 Tetrachloroethene ND ug/L 07/25/23 07:18 127-18-41.0 0.29 1 Toluene ND ug/L 07/25/23 07:18 108-88-31.0 0.24 1 1,2,3-Trichlorobenzene ND ug/L 07/25/23 07:18 87-61-61.0 0.81 1 1,2,4-Trichlorobenzene ND ug/L 07/25/23 07:18 120-82-11.0 0.64 1 1,1,1-Trichloroethane ND ug/L 07/25/23 07:18 71-55-61.0 0.33 1 1,1,2-Trichloroethane ND ug/L 07/25/23 07:18 79-00-51.0 0.32 1 Trichloroethene ND ug/L 07/25/23 07:18 79-01-61.0 0.38 1 Trichlorofluoromethane ND ug/L 07/25/23 07:18 75-69-41.0 0.30 1 1,2,3-Trichloropropane ND ug/L 07/25/23 07:18 96-18-41.0 0.26 1 Vinyl acetate ND ug/L 07/25/23 07:18 108-05-42.0 1.3 1 Vinyl chloride ND ug/L 07/25/23 07:18 75-01-41.0 0.39 1 Xylene (Total)ND ug/L 07/25/23 07:18 1330-20-71.0 0.34 1 m&p-Xylene ND ug/L 07/25/23 07:18 179601-23-12.0 0.71 1 o-Xylene ND ug/L 07/25/23 07:18 95-47-61.0 0.34 1 Surrogates 4-Bromofluorobenzene (S)96 %07/25/23 07:18 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/25/23 07:18 17060-07-070-130 1 Toluene-d8 (S)101 %07/25/23 07:18 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 79 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2102447 3050B EPA 6020B Metals (ICPMS) 6020B Laboratory:Pace National - Mt. Juliet Associated Lab Samples:92678743001, 92678743002, 92678743003, 92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010, 92678743018 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3955471-1 Associated Lab Samples: 92678743001, 92678743002, 92678743003, 92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010, 92678743018 Matrix: Solid AnalyzedMDL Arsenic mg/kg ND 1.00 08/01/23 16:110.100 Barium mg/kg ND 2.50 08/01/23 16:110.152 Cadmium mg/kg ND 1.00 08/01/23 16:110.0855 Chromium mg/kg ND 5.00 08/01/23 16:110.297 Lead mg/kg ND 2.00 08/01/23 16:110.0990 Selenium mg/kg ND 2.50 08/01/23 16:110.180 Silver mg/kg ND 0.500 08/01/23 16:110.0865 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3955471-2LABORATORY CONTROL SAMPLE: LCSSpike Arsenic mg/kg 106100 106 80.0-120 Barium mg/kg 102100 102 80.0-120 Cadmium mg/kg 107100 107 80.0-120 Chromium mg/kg 105100 105 80.0-120 Lead mg/kg 101100 101 80.0-120 Selenium mg/kg 114100 114 80.0-120 Silver mg/kg 20.620.0 103 80.0-120 Parameter Units MS Result % Rec Limits Qual% RecConc. R3955471-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result L1638713-06 R3955471-6 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic mg/kg 108 102 75.0-125104 2.55 201083.17 113 116 Barium mg/kg 108 102 75.0-125109 4.23 2010867.8 178 186 Cadmium mg/kg 108 105 75.0-125105 0.579 20108ND113 114 Chromium mg/kg 108 103 75.0-125104 0.253 2010819.3 131 131 Lead mg/kg 108 97.4 75.0-125102 4.17 201082.23 108 112 Selenium mg/kg E10811475.0-125114 0.026 20108ND124 124 Silver mg/kg 21.6 101 75.0-125103 2.47 2021.6ND 21.8 22.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 80 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2102597 7471A EPA 7471B Mercury 7471B Laboratory:Pace National - Mt. Juliet Associated Lab Samples:92678743001, 92678743002, 92678743003, 92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010, 92678743018 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3954532-1 Associated Lab Samples: 92678743001, 92678743002, 92678743003, 92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010, 92678743018 Matrix: Solid AnalyzedMDL Mercury mg/kg ND 0.0400 07/30/23 17:540.0180 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3954532-2LABORATORY CONTROL SAMPLE: LCSSpike Mercury mg/kg 0.4680.500 93.6 80.0-120 Parameter Units MS Result % Rec Limits Qual% RecConc. R3954532-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result L1638913-03 R3954532-4 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury mg/kg 0.533 98.4 75.0-12595.8 2.46 200.5330.0475 0.572 0.558 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 81 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 790262 EPA 7470A EPA 7470A 7470 Mercury Laboratory:Pace Analytical Services - Asheville Associated Lab Samples: 92678743011, 92678743012, 92678743013, 92678743014, 92678743015, 92678743016, 92678743017 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4095711 Associated Lab Samples:92678743011, 92678743012, 92678743013, 92678743014, 92678743015, 92678743016, 92678743017 Matrix: Water AnalyzedMDL Mercury ug/L ND 0.20 07/31/23 14:090.12 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4095712LABORATORY CONTROL SAMPLE: LCSSpike Mercury ug/L 2.52.5 100 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 4095713MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92678743011 4095714 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury ug/L 2.5 96 75-12598 2 252.5ND 2.4 2.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 82 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 789135 EPA 3010A EPA 6020B 6020 MET Laboratory:Pace Analytical Services - Asheville Associated Lab Samples: 92678743011, 92678743012, 92678743013, 92678743014, 92678743015, 92678743016, 92678743017 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4090315 Associated Lab Samples:92678743011, 92678743012, 92678743013, 92678743014, 92678743015, 92678743016, 92678743017 Matrix: Water AnalyzedMDL Arsenic ug/L ND 1.0 07/27/23 01:160.087 Barium ug/L ND 1.0 07/27/23 01:160.21 Cadmium ug/L ND 0.20 07/27/23 01:160.060 Chromium ug/L ND 1.0 07/27/23 01:160.50 Lead ug/L ND 1.0 07/27/23 01:160.077 Selenium ug/L ND 2.0 07/27/23 01:160.072 Silver ug/L ND 0.40 07/27/23 01:160.070 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4090316LABORATORY CONTROL SAMPLE: LCSSpike Arsenic ug/L 49.750 99 80-120 Barium ug/L 49.750 99 80-120 Cadmium ug/L 50.550 101 80-120 Chromium ug/L 51.050 102 80-120 Lead ug/L 50.250 100 80-120 Selenium ug/L 50.750 101 80-120 Silver ug/L 25.325 101 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 4090317MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92678191008 4090318 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic ug/L 50 101 75-125101 0 20500.32J 50.7 50.8 Barium ug/L 50 98 75-12596 1 205087.5 136 136 Cadmium ug/L 50 101 75-125101 1 20500.17J 50.6 50.9 Chromium ug/L 50 101 75-125102 1 2050ND50.9 51.3 Lead ug/L 50 101 75-125103 1 2050ND50.7 51.4 Selenium ug/L 50 101 75-125101 0 20500.21J 50.9 50.9 Silver ug/L 25 101 75-125101 0 2025ND25.2 25.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 83 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 789111 EPA 5035A/5030B EPA 8260D 8260D 5035A 5030B Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples: 92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4090208 Associated Lab Samples:92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009 Matrix: Solid AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/25/23 16:371.9 1,1,1-Trichloroethane ug/kg ND 5.0 07/25/23 16:372.6 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/25/23 16:371.3 1,1,2-Trichloroethane ug/kg ND 5.0 07/25/23 16:371.7 1,1-Dichloroethane ug/kg ND 5.0 07/25/23 16:372.1 1,1-Dichloroethene ug/kg ND 5.0 07/25/23 16:372.1 1,1-Dichloropropene ug/kg ND 5.0 07/25/23 16:372.4 1,2,3-Trichlorobenzene ug/kg ND 5.0 07/25/23 16:374.0 1,2,3-Trichloropropane ug/kg ND 5.0 07/25/23 16:372.5 1,2,4-Trichlorobenzene ug/kg ND 5.0 07/25/23 16:374.2 1,2,4-Trimethylbenzene ug/kg ND 5.0 07/25/23 16:373.0 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/25/23 16:371.9 1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/25/23 16:372.2 1,2-Dichlorobenzene ug/kg ND 5.0 07/25/23 16:371.8 1,2-Dichloroethane ug/kg ND 5.0 07/25/23 16:373.3 1,2-Dichloropropane ug/kg ND 5.0 07/25/23 16:371.5 1,3,5-Trimethylbenzene ug/kg ND 5.0 07/25/23 16:371.7 1,3-Dichlorobenzene ug/kg ND 5.0 07/25/23 16:371.6 1,3-Dichloropropane ug/kg ND 5.0 07/25/23 16:371.6 1,4-Dichlorobenzene ug/kg ND 5.0 07/25/23 16:371.3 2,2-Dichloropropane ug/kg ND 5.0 v207/25/23 16:373.8 2-Butanone (MEK)ug/kg ND 100 07/25/23 16:3724.0 2-Chlorotoluene ug/kg ND 5.0 07/25/23 16:371.8 2-Hexanone ug/kg ND 50.0 07/25/23 16:374.8 4-Chlorotoluene ug/kg ND 5.0 07/25/23 16:372.8 4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/25/23 16:374.8 Acetone ug/kg ND 100 07/25/23 16:3732.1 Benzene ug/kg ND 5.0 07/25/23 16:372.0 Bromobenzene ug/kg ND 5.0 07/25/23 16:371.6 Bromochloromethane ug/kg ND 5.0 07/25/23 16:371.5 Bromodichloromethane ug/kg ND 5.0 07/25/23 16:371.9 Bromoform ug/kg ND 5.0 07/25/23 16:371.8 Bromomethane ug/kg ND 20.0 IH07/25/23 16:3715.5 Carbon tetrachloride ug/kg ND 5.0 07/25/23 16:371.9 Chlorobenzene ug/kg ND 5.0 07/25/23 16:372.9 Chloroethane ug/kg ND 10.0 07/25/23 16:373.9 Chloroform ug/kg ND 5.0 07/25/23 16:374.2 Chloromethane ug/kg ND 10.0 07/25/23 16:374.2 cis-1,2-Dichloroethene ug/kg ND 5.0 07/25/23 16:371.7 cis-1,3-Dichloropropene ug/kg ND 5.0 07/25/23 16:371.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 84 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4090208 Associated Lab Samples:92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009 Matrix: Solid AnalyzedMDL Dibromochloromethane ug/kg ND 5.0 07/25/23 16:372.8 Dibromomethane ug/kg ND 5.0 07/25/23 16:371.1 Dichlorodifluoromethane ug/kg ND 10.0 07/25/23 16:375.1 Diisopropyl ether ug/kg ND 5.0 07/25/23 16:371.4 Ethylbenzene ug/kg ND 5.0 07/25/23 16:372.3 Hexachloro-1,3-butadiene ug/kg ND 10.0 07/25/23 16:378.2 Isopropylbenzene (Cumene)ug/kg ND 5.0 07/25/23 16:371.7 m&p-Xylene ug/kg ND 10.0 07/25/23 16:373.4 Methyl-tert-butyl ether ug/kg ND 5.0 v207/25/23 16:371.9 Methylene Chloride ug/kg ND 20.0 07/25/23 16:3713.7 n-Butylbenzene ug/kg ND 5.0 07/25/23 16:373.2 n-Propylbenzene ug/kg ND 5.0 07/25/23 16:371.8 Naphthalene ug/kg ND 5.0 07/25/23 16:372.6 o-Xylene ug/kg ND 5.0 07/25/23 16:372.2 p-Isopropyltoluene ug/kg ND 5.0 07/25/23 16:372.5 sec-Butylbenzene ug/kg ND 5.0 07/25/23 16:372.2 Styrene ug/kg ND 5.0 07/25/23 16:371.3 tert-Butylbenzene ug/kg ND 5.0 07/25/23 16:371.8 Tetrachloroethene ug/kg ND 5.0 07/25/23 16:371.6 Toluene ug/kg ND 5.0 07/25/23 16:373.4 trans-1,2-Dichloroethene ug/kg ND 5.0 07/25/23 16:374.2 trans-1,3-Dichloropropene ug/kg ND 5.0 07/25/23 16:371.7 Trichloroethene ug/kg ND 5.0 07/25/23 16:374.0 Trichlorofluoromethane ug/kg ND 5.0 07/25/23 16:372.8 Vinyl acetate ug/kg ND 50.0 07/25/23 16:3710.3 Vinyl chloride ug/kg ND 10.0 v207/25/23 16:372.5 Xylene (Total)ug/kg ND 10.0 07/25/23 16:372.8 1,2-Dichloroethane-d4 (S)%94 70-130 07/25/23 16:37 4-Bromofluorobenzene (S)%99 70-130 07/25/23 16:37 Toluene-d8 (S)%99 70-130 07/25/23 16:37 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4090209LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 444500 89 70-130 1,1,1-Trichloroethane ug/kg 418500 84 70-130 1,1,2,2-Tetrachloroethane ug/kg 439500 88 70-130 1,1,2-Trichloroethane ug/kg 431500 86 70-130 1,1-Dichloroethane ug/kg 423500 85 70-130 1,1-Dichloroethene ug/kg 438500 88 70-130 1,1-Dichloropropene ug/kg 419500 84 70-130 1,2,3-Trichlorobenzene ug/kg 449500 90 70-130 1,2,3-Trichloropropane ug/kg 432500 86 70-130 1,2,4-Trichlorobenzene ug/kg 408500 82 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 85 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4090209LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trimethylbenzene ug/kg 432500 86 70-130 1,2-Dibromo-3-chloropropane ug/kg 422500 84 67-130 1,2-Dibromoethane (EDB)ug/kg 433500 87 70-130 1,2-Dichlorobenzene ug/kg 434500 87 70-130 1,2-Dichloroethane ug/kg 408500 82 70-130 1,2-Dichloropropane ug/kg 424500 85 70-130 1,3,5-Trimethylbenzene ug/kg 417500 83 70-130 1,3-Dichlorobenzene ug/kg 416500 83 70-130 1,3-Dichloropropane ug/kg 415500 83 70-130 1,4-Dichlorobenzene ug/kg 411500 82 70-130 2,2-Dichloropropane ug/kg 357 v350071 67-130 2-Butanone (MEK)ug/kg 8791000 88 66-130 2-Chlorotoluene ug/kg 432500 86 70-130 2-Hexanone ug/kg 9221000 92 70-130 4-Chlorotoluene ug/kg 430500 86 70-130 4-Methyl-2-pentanone (MIBK)ug/kg 8971000 90 70-130 Acetone ug/kg 9081000 91 67-130 Benzene ug/kg 415500 83 70-130 Bromobenzene ug/kg 437500 87 70-130 Bromochloromethane ug/kg 441500 88 70-130 Bromodichloromethane ug/kg 417500 83 70-130 Bromoform ug/kg 440500 88 70-130 Bromomethane ug/kg 400 IH50080 53-175 Carbon tetrachloride ug/kg 446500 89 70-130 Chlorobenzene ug/kg 437500 87 70-130 Chloroethane ug/kg 412500 82 70-135 Chloroform ug/kg 422500 84 70-130 Chloromethane ug/kg 402500 80 64-130 cis-1,2-Dichloroethene ug/kg 412500 82 70-130 cis-1,3-Dichloropropene ug/kg 401500 80 70-130 Dibromochloromethane ug/kg 430500 86 70-130 Dibromomethane ug/kg 444500 89 70-130 Dichlorodifluoromethane ug/kg 541500 108 63-145 Diisopropyl ether ug/kg 398500 80 68-130 Ethylbenzene ug/kg 398500 80 70-130 Hexachloro-1,3-butadiene ug/kg 409500 82 70-130 Isopropylbenzene (Cumene)ug/kg 435500 87 70-130 m&p-Xylene ug/kg 8511000 85 70-130 Methyl-tert-butyl ether ug/kg 386 v350077 70-130 Methylene Chloride ug/kg 411500 82 67-130 n-Butylbenzene ug/kg 407500 81 70-130 n-Propylbenzene ug/kg 413500 83 70-130 Naphthalene ug/kg 440500 88 70-130 o-Xylene ug/kg 428500 86 70-130 p-Isopropyltoluene ug/kg 437500 87 70-130 sec-Butylbenzene ug/kg 412500 82 70-130 Styrene ug/kg 433500 87 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 86 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4090209LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 446500 89 64-130 Tetrachloroethene ug/kg 450500 90 70-130 Toluene ug/kg 420500 84 70-130 trans-1,2-Dichloroethene ug/kg 421500 84 70-130 trans-1,3-Dichloropropene ug/kg 412500 82 70-130 Trichloroethene ug/kg 435500 87 70-130 Trichlorofluoromethane ug/kg 434500 87 70-130 Vinyl acetate ug/kg 8581000 86 70-134 Vinyl chloride ug/kg 367 v350073 68-130 Xylene (Total)ug/kg 12801500 85 70-130 1,2-Dichloroethane-d4 (S)%91 70-130 4-Bromofluorobenzene (S)%99 70-130 Toluene-d8 (S)%99 70-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4090210MATRIX SPIKE SAMPLE: MSSpike Result 92678743004 1,1,1,2-Tetrachloroethane ug/kg 749595 126 58-140ND 1,1,1-Trichloroethane ug/kg 760595 128 58-144ND 1,1,2,2-Tetrachloroethane ug/kg 678595 114 52-139ND 1,1,2-Trichloroethane ug/kg 713595 120 56-140ND 1,1-Dichloroethane ug/kg 712595 120 58-145ND 1,1-Dichloroethene ug/kg 783595 132 57-158ND 1,1-Dichloropropene ug/kg 764595 128 58-151ND 1,2,3-Trichlorobenzene ug/kg 642595 108 48-149ND 1,2,3-Trichloropropane ug/kg 680595 114 54-132ND 1,2,4-Trichlorobenzene ug/kg 607595 102 51-151ND 1,2,4-Trimethylbenzene ug/kg 667595 111 38-1703.9J 1,2-Dibromo-3-chloropropane ug/kg 613595 103 44-134ND 1,2-Dibromoethane (EDB)ug/kg 708595 119 60-138ND 1,2-Dichlorobenzene ug/kg 683595 115 59-147ND 1,2-Dichloroethane ug/kg 698595 117 57-139ND 1,2-Dichloropropane ug/kg 716595 120 62-145ND 1,3,5-Trimethylbenzene ug/kg 680595 114 47-159ND 1,3-Dichlorobenzene ug/kg 661595 111 58-144ND 1,3-Dichloropropane ug/kg 687595 115 60-142ND 1,4-Dichlorobenzene ug/kg 630595 106 57-143ND 2,2-Dichloropropane ug/kg 615 v3595103 37-144ND 2-Butanone (MEK)ug/kg 11501190 97 28-146ND 2-Chlorotoluene ug/kg 678595 114 55-158ND 2-Hexanone ug/kg 13801190 116 44-141ND 4-Chlorotoluene ug/kg 663595 111 55-146ND 4-Methyl-2-pentanone (MIBK)ug/kg 13601190 115 50-138ND Acetone ug/kg 10301190 86 20-136ND Benzene ug/kg 717595 121 60-145ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 87 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4090210MATRIX SPIKE SAMPLE: MSSpike Result 92678743004 Bromobenzene ug/kg 687595 115 59-145ND Bromochloromethane ug/kg 744595 125 57-143ND Bromodichloromethane ug/kg 686595 115 53-133ND Bromoform ug/kg 724595 122 48-133ND Bromomethane ug/kg 210 IH59535 10-167ND Carbon tetrachloride ug/kg 686595 115 57-147ND Chlorobenzene ug/kg 731595 123 61-144ND Chloroethane ug/kg 219595 37 10-153ND Chloroform ug/kg 737595 124 58-141ND Chloromethane ug/kg 816595 136 54-1655.5J cis-1,2-Dichloroethene ug/kg 723595 121 59-144ND cis-1,3-Dichloropropene ug/kg 668595 112 56-137ND Dibromochloromethane ug/kg 698595 117 53-139ND Dibromomethane ug/kg 707595 119 60-136ND Dichlorodifluoromethane ug/kg 1050595 176 49-177ND Diisopropyl ether ug/kg 678595 114 53-136ND Ethylbenzene ug/kg 661595 111 53-150ND Hexachloro-1,3-butadiene ug/kg 730595 123 42-186ND Isopropylbenzene (Cumene)ug/kg 744595 125 62-154ND m&p-Xylene ug/kg 14201190 118 49-1566.4J Methyl-tert-butyl ether ug/kg 646 v3595109 54-133ND Methylene Chloride ug/kg 708595 119 50-153ND n-Butylbenzene ug/kg 653595 110 44-174ND n-Propylbenzene ug/kg 655595 110 52-157ND Naphthalene ug/kg 725595 103 37-150111 o-Xylene ug/kg 712595 119 54-1503.2J p-Isopropyltoluene ug/kg 707595 119 50-164ND sec-Butylbenzene ug/kg 685595 115 58-161ND Styrene ug/kg 723595 122 60-148ND tert-Butylbenzene ug/kg 560595 94 44-151ND Tetrachloroethene ug/kg 686595 115 53-151ND Toluene ug/kg 716595 119 52-1485.7J trans-1,2-Dichloroethene ug/kg 720595 121 60-148ND trans-1,3-Dichloropropene ug/kg 665595 112 55-133ND Trichloroethene ug/kg 752595 126 60-148ND Trichlorofluoromethane ug/kg 252595 42 10-154ND Vinyl acetate ug/kg 12501190 105 50-149ND Vinyl chloride ug/kg 650 v3595109 57-157ND Xylene (Total)ug/kg 21301780 119 52-1539.6J 1,2-Dichloroethane-d4 (S)%115 70-130 4-Bromofluorobenzene (S)%101 70-130 Toluene-d8 (S)%99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 88 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92678743005 4090211SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/kg ND 30ND 1,1,1-Trichloroethane ug/kg ND 30ND 1,1,2,2-Tetrachloroethane ug/kg ND 30ND 1,1,2-Trichloroethane ug/kg ND 30ND 1,1-Dichloroethane ug/kg ND 30ND 1,1-Dichloroethene ug/kg ND 30ND 1,1-Dichloropropene ug/kg ND 30ND 1,2,3-Trichlorobenzene ug/kg ND 30ND 1,2,3-Trichloropropane ug/kg ND 30ND 1,2,4-Trichlorobenzene ug/kg ND 30ND 1,2,4-Trimethylbenzene ug/kg ND 30ND 1,2-Dibromo-3-chloropropane ug/kg ND 30ND 1,2-Dibromoethane (EDB)ug/kg ND 30ND 1,2-Dichlorobenzene ug/kg ND 30ND 1,2-Dichloroethane ug/kg ND 30ND 1,2-Dichloropropane ug/kg ND 30ND 1,3,5-Trimethylbenzene ug/kg ND 30ND 1,3-Dichlorobenzene ug/kg ND 30ND 1,3-Dichloropropane ug/kg ND 30ND 1,4-Dichlorobenzene ug/kg ND 30ND 2,2-Dichloropropane ug/kg ND v230ND 2-Butanone (MEK)ug/kg ND 30ND 2-Chlorotoluene ug/kg ND 30ND 2-Hexanone ug/kg ND 30ND 4-Chlorotoluene ug/kg ND 30ND 4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND Acetone ug/kg ND 30ND Benzene ug/kg ND 30ND Bromobenzene ug/kg ND 30ND Bromochloromethane ug/kg ND 30ND Bromodichloromethane ug/kg ND 30ND Bromoform ug/kg ND 30ND Bromomethane ug/kg ND IH30ND Carbon tetrachloride ug/kg ND 30ND Chlorobenzene ug/kg ND 30ND Chloroethane ug/kg ND 30ND Chloroform ug/kg ND 30ND Chloromethane ug/kg ND 30ND cis-1,2-Dichloroethene ug/kg ND 30ND cis-1,3-Dichloropropene ug/kg ND 30ND Dibromochloromethane ug/kg ND 30ND Dibromomethane ug/kg ND 30ND Dichlorodifluoromethane ug/kg ND 30ND Diisopropyl ether ug/kg ND 30ND Ethylbenzene ug/kg ND 30ND Hexachloro-1,3-butadiene ug/kg ND 30ND Isopropylbenzene (Cumene)ug/kg ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 89 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92678743005 4090211SAMPLE DUPLICATE: m&p-Xylene ug/kg ND 30ND Methyl-tert-butyl ether ug/kg ND v230ND Methylene Chloride ug/kg ND 30ND n-Butylbenzene ug/kg ND 30ND n-Propylbenzene ug/kg ND 30ND Naphthalene ug/kg 7.0J 309.8 o-Xylene ug/kg ND 30ND p-Isopropyltoluene ug/kg ND 30ND sec-Butylbenzene ug/kg ND 30ND Styrene ug/kg ND 30ND tert-Butylbenzene ug/kg ND 30ND Tetrachloroethene ug/kg ND 30ND Toluene ug/kg ND 30ND trans-1,2-Dichloroethene ug/kg ND 30ND trans-1,3-Dichloropropene ug/kg ND 30ND Trichloroethene ug/kg ND 30ND Trichlorofluoromethane ug/kg ND 30ND Vinyl acetate ug/kg ND 30ND Vinyl chloride ug/kg ND v230ND Xylene (Total)ug/kg ND 30ND 1,2-Dichloroethane-d4 (S)%111110 4-Bromofluorobenzene (S)%100104 Toluene-d8 (S)%102101 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 90 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 789195 EPA 5035A/5030B EPA 8260D 8260D 5035A 5030B Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples: 92678743010, 92678743018 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4090656 Associated Lab Samples:92678743010, 92678743018 Matrix: Solid AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/25/23 16:561.9 1,1,1-Trichloroethane ug/kg ND 5.0 07/25/23 16:562.6 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/25/23 16:561.3 1,1,2-Trichloroethane ug/kg ND 5.0 07/25/23 16:561.7 1,1-Dichloroethane ug/kg ND 5.0 07/25/23 16:562.1 1,1-Dichloroethene ug/kg ND 5.0 07/25/23 16:562.1 1,1-Dichloropropene ug/kg ND 5.0 07/25/23 16:562.4 1,2,3-Trichlorobenzene ug/kg ND 5.0 07/25/23 16:564.0 1,2,3-Trichloropropane ug/kg ND 5.0 07/25/23 16:562.5 1,2,4-Trichlorobenzene ug/kg ND 5.0 07/25/23 16:564.2 1,2,4-Trimethylbenzene ug/kg ND 5.0 07/25/23 16:563.0 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/25/23 16:561.9 1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/25/23 16:562.2 1,2-Dichlorobenzene ug/kg ND 5.0 07/25/23 16:561.8 1,2-Dichloroethane ug/kg ND 5.0 07/25/23 16:563.3 1,2-Dichloropropane ug/kg ND 5.0 07/25/23 16:561.5 1,3,5-Trimethylbenzene ug/kg ND 5.0 07/25/23 16:561.7 1,3-Dichlorobenzene ug/kg ND 5.0 07/25/23 16:561.6 1,3-Dichloropropane ug/kg ND 5.0 07/25/23 16:561.6 1,4-Dichlorobenzene ug/kg ND 5.0 07/25/23 16:561.3 2,2-Dichloropropane ug/kg ND 5.0 v207/25/23 16:563.8 2-Butanone (MEK)ug/kg ND 100 07/25/23 16:5624.0 2-Chlorotoluene ug/kg ND 5.0 07/25/23 16:561.8 2-Hexanone ug/kg ND 50.0 07/25/23 16:564.8 4-Chlorotoluene ug/kg ND 5.0 07/25/23 16:562.8 4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/25/23 16:564.8 Acetone ug/kg ND 100 07/25/23 16:5632.1 Benzene ug/kg ND 5.0 07/25/23 16:562.0 Bromobenzene ug/kg ND 5.0 07/25/23 16:561.6 Bromochloromethane ug/kg ND 5.0 07/25/23 16:561.5 Bromodichloromethane ug/kg ND 5.0 07/25/23 16:561.9 Bromoform ug/kg ND 5.0 07/25/23 16:561.8 Bromomethane ug/kg ND 20.0 IH07/25/23 16:5615.5 Carbon tetrachloride ug/kg ND 5.0 07/25/23 16:561.9 Chlorobenzene ug/kg ND 5.0 07/25/23 16:562.9 Chloroethane ug/kg ND 10.0 07/25/23 16:563.9 Chloroform ug/kg ND 5.0 07/25/23 16:564.2 Chloromethane ug/kg ND 10.0 07/25/23 16:564.2 cis-1,2-Dichloroethene ug/kg ND 5.0 07/25/23 16:561.7 cis-1,3-Dichloropropene ug/kg ND 5.0 07/25/23 16:561.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 91 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4090656 Associated Lab Samples:92678743010, 92678743018 Matrix: Solid AnalyzedMDL Dibromochloromethane ug/kg ND 5.0 07/25/23 16:562.8 Dibromomethane ug/kg ND 5.0 07/25/23 16:561.1 Dichlorodifluoromethane ug/kg ND 10.0 07/25/23 16:565.1 Diisopropyl ether ug/kg ND 5.0 07/25/23 16:561.4 Ethylbenzene ug/kg ND 5.0 07/25/23 16:562.3 Hexachloro-1,3-butadiene ug/kg ND 10.0 07/25/23 16:568.2 Isopropylbenzene (Cumene)ug/kg ND 5.0 07/25/23 16:561.7 m&p-Xylene ug/kg ND 10.0 07/25/23 16:563.4 Methyl-tert-butyl ether ug/kg ND 5.0 v207/25/23 16:561.9 Methylene Chloride ug/kg ND 20.0 07/25/23 16:5613.7 n-Butylbenzene ug/kg ND 5.0 07/25/23 16:563.2 n-Propylbenzene ug/kg ND 5.0 07/25/23 16:561.8 Naphthalene ug/kg ND 5.0 07/25/23 16:562.6 o-Xylene ug/kg ND 5.0 07/25/23 16:562.2 p-Isopropyltoluene ug/kg ND 5.0 07/25/23 16:562.5 sec-Butylbenzene ug/kg ND 5.0 07/25/23 16:562.2 Styrene ug/kg ND 5.0 07/25/23 16:561.3 tert-Butylbenzene ug/kg ND 5.0 07/25/23 16:561.8 Tetrachloroethene ug/kg ND 5.0 07/25/23 16:561.6 Toluene ug/kg ND 5.0 07/25/23 16:563.4 trans-1,2-Dichloroethene ug/kg ND 5.0 07/25/23 16:564.2 trans-1,3-Dichloropropene ug/kg ND 5.0 07/25/23 16:561.7 Trichloroethene ug/kg ND 5.0 07/25/23 16:564.0 Trichlorofluoromethane ug/kg ND 5.0 07/25/23 16:562.8 Vinyl acetate ug/kg ND 50.0 07/25/23 16:5610.3 Vinyl chloride ug/kg ND 10.0 v207/25/23 16:562.5 Xylene (Total)ug/kg ND 10.0 07/25/23 16:562.8 1,2-Dichloroethane-d4 (S)%104 70-130 07/25/23 16:56 4-Bromofluorobenzene (S)%100 70-130 07/25/23 16:56 Toluene-d8 (S)%101 70-130 07/25/23 16:56 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4090657LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 530500 106 70-130 1,1,1-Trichloroethane ug/kg 484500 97 70-130 1,1,2,2-Tetrachloroethane ug/kg 510500 102 70-130 1,1,2-Trichloroethane ug/kg 502500 100 70-130 1,1-Dichloroethane ug/kg 492500 98 70-130 1,1-Dichloroethene ug/kg 508500 102 70-130 1,1-Dichloropropene ug/kg 488500 98 70-130 1,2,3-Trichlorobenzene ug/kg 500500 100 70-130 1,2,3-Trichloropropane ug/kg 515500 103 70-130 1,2,4-Trichlorobenzene ug/kg 452500 90 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 92 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4090657LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trimethylbenzene ug/kg 491500 98 70-130 1,2-Dibromo-3-chloropropane ug/kg 470500 94 67-130 1,2-Dibromoethane (EDB)ug/kg 519500 104 70-130 1,2-Dichlorobenzene ug/kg 491500 98 70-130 1,2-Dichloroethane ug/kg 479500 96 70-130 1,2-Dichloropropane ug/kg 495500 99 70-130 1,3,5-Trimethylbenzene ug/kg 485500 97 70-130 1,3-Dichlorobenzene ug/kg 473500 95 70-130 1,3-Dichloropropane ug/kg 495500 99 70-130 1,4-Dichlorobenzene ug/kg 435500 87 70-130 2,2-Dichloropropane ug/kg 404 v350081 67-130 2-Butanone (MEK)ug/kg 10301000 103 66-130 2-Chlorotoluene ug/kg 491500 98 70-130 2-Hexanone ug/kg 10801000 108 70-130 4-Chlorotoluene ug/kg 490500 98 70-130 4-Methyl-2-pentanone (MIBK)ug/kg 10501000 105 70-130 Acetone ug/kg 10201000 102 67-130 Benzene ug/kg 488500 98 70-130 Bromobenzene ug/kg 497500 99 70-130 Bromochloromethane ug/kg 509500 102 70-130 Bromodichloromethane ug/kg 486500 97 70-130 Bromoform ug/kg 539500 108 70-130 Bromomethane ug/kg 480 IH50096 53-175 Carbon tetrachloride ug/kg 496500 99 70-130 Chlorobenzene ug/kg 513500 103 70-130 Chloroethane ug/kg 480500 96 70-135 Chloroform ug/kg 490500 98 70-130 Chloromethane ug/kg 467500 93 64-130 cis-1,2-Dichloroethene ug/kg 478500 96 70-130 cis-1,3-Dichloropropene ug/kg 468500 94 70-130 Dibromochloromethane ug/kg 505500 101 70-130 Dibromomethane ug/kg 516500 103 70-130 Dichlorodifluoromethane ug/kg 578500 116 63-145 Diisopropyl ether ug/kg 463500 93 68-130 Ethylbenzene ug/kg 472500 94 70-130 Hexachloro-1,3-butadiene ug/kg 473500 95 70-130 Isopropylbenzene (Cumene)ug/kg 519500 104 70-130 m&p-Xylene ug/kg 10001000 100 70-130 Methyl-tert-butyl ether ug/kg 449 v350090 70-130 Methylene Chloride ug/kg 476500 95 67-130 n-Butylbenzene ug/kg 463500 93 70-130 n-Propylbenzene ug/kg 473500 95 70-130 Naphthalene ug/kg 498500 100 70-130 o-Xylene ug/kg 508500 102 70-130 p-Isopropyltoluene ug/kg 499500 100 70-130 sec-Butylbenzene ug/kg 473500 95 70-130 Styrene ug/kg 515500 103 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 93 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4090657LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 412500 82 64-130 Tetrachloroethene ug/kg 518500 104 70-130 Toluene ug/kg 482500 96 70-130 trans-1,2-Dichloroethene ug/kg 488500 98 70-130 trans-1,3-Dichloropropene ug/kg 478500 96 70-130 Trichloroethene ug/kg 505500 101 70-130 Trichlorofluoromethane ug/kg 477500 95 70-130 Vinyl acetate ug/kg 10101000 101 70-134 Vinyl chloride ug/kg 434 v350087 68-130 Xylene (Total)ug/kg 15101500 101 70-130 1,2-Dichloroethane-d4 (S)%92 70-130 4-Bromofluorobenzene (S)%101 70-130 Toluene-d8 (S)%99 70-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4090658MATRIX SPIKE SAMPLE: MSSpike Result 92678743010 1,1,1,2-Tetrachloroethane ug/kg 967767 126 58-140ND 1,1,1-Trichloroethane ug/kg 934767 122 58-144ND 1,1,2,2-Tetrachloroethane ug/kg 881767 115 52-139ND 1,1,2-Trichloroethane ug/kg 921767 120 56-140ND 1,1-Dichloroethane ug/kg 882767 115 58-145ND 1,1-Dichloroethene ug/kg 994767 130 57-158ND 1,1-Dichloropropene ug/kg 989767 129 58-151ND 1,2,3-Trichlorobenzene ug/kg 840767 110 48-149ND 1,2,3-Trichloropropane ug/kg 896767 117 54-132ND 1,2,4-Trichlorobenzene ug/kg 832767 109 51-151ND 1,2,4-Trimethylbenzene ug/kg 954767 122 38-17019.3 1,2-Dibromo-3-chloropropane ug/kg 799767 104 44-134ND 1,2-Dibromoethane (EDB)ug/kg 932767 122 60-138ND 1,2-Dichlorobenzene ug/kg 925767 121 59-147ND 1,2-Dichloroethane ug/kg 839767 110 57-139ND 1,2-Dichloropropane ug/kg 934767 122 62-145ND 1,3,5-Trimethylbenzene ug/kg 935767 122 47-159ND 1,3-Dichlorobenzene ug/kg 907767 118 58-144ND 1,3-Dichloropropane ug/kg 889767 116 60-142ND 1,4-Dichlorobenzene ug/kg 873767 114 57-143ND 2,2-Dichloropropane ug/kg 794 v3767104 37-144ND 2-Butanone (MEK)ug/kg 14301530 93 28-146ND 2-Chlorotoluene ug/kg 920767 120 55-158ND 2-Hexanone ug/kg 17401530 113 44-141ND 4-Chlorotoluene ug/kg 911767 119 55-146ND 4-Methyl-2-pentanone (MIBK)ug/kg 17101530 111 50-138ND Acetone ug/kg 11001530 72 20-136ND Benzene ug/kg 936767 122 60-1454.4J REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 94 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4090658MATRIX SPIKE SAMPLE: MSSpike Result 92678743010 Bromobenzene ug/kg 926767 121 59-145ND Bromochloromethane ug/kg 957767 125 57-143ND Bromodichloromethane ug/kg 880767 115 53-133ND Bromoform ug/kg 942767 123 48-133ND Bromomethane ug/kg 254 IH76733 10-167ND Carbon tetrachloride ug/kg 868767 113 57-147ND Chlorobenzene ug/kg 981767 128 61-144ND Chloroethane ug/kg 258767 34 10-153ND Chloroform ug/kg 921767 120 58-141ND Chloromethane ug/kg 1020767 133 54-1657.0J cis-1,2-Dichloroethene ug/kg 896767 117 59-144ND cis-1,3-Dichloropropene ug/kg 873767 114 56-137ND Dibromochloromethane ug/kg 906767 118 53-139ND Dibromomethane ug/kg 978767 128 60-136ND Dichlorodifluoromethane ug/kg 1390 M1767181 49-177ND Diisopropyl ether ug/kg 821767 107 53-136ND Ethylbenzene ug/kg 913767 117 53-15015.9 Hexachloro-1,3-butadiene ug/kg 1020767 134 42-186ND Isopropylbenzene (Cumene)ug/kg 1000767 130 62-1544.8J m&p-Xylene ug/kg 19801530 125 49-15662.2 Methyl-tert-butyl ether ug/kg 801 v3767105 54-133ND Methylene Chloride ug/kg 797767 104 50-153ND n-Butylbenzene ug/kg 950767 124 44-174ND n-Propylbenzene ug/kg 920767 120 52-157ND Naphthalene ug/kg 851767 105 37-15047.2 o-Xylene ug/kg 1000767 125 54-15042.4 p-Isopropyltoluene ug/kg 1000767 131 50-164ND sec-Butylbenzene ug/kg 944767 123 58-161ND Styrene ug/kg 977767 128 60-148ND tert-Butylbenzene ug/kg 760767 99 44-151ND Tetrachloroethene ug/kg 1010767 131 53-151ND Toluene ug/kg 966767 123 52-14826.2 trans-1,2-Dichloroethene ug/kg 906767 118 60-148ND trans-1,3-Dichloropropene ug/kg 872767 114 55-133ND Trichloroethene ug/kg 1020767 133 60-148ND Trichlorofluoromethane ug/kg 315767 41 10-154ND Vinyl acetate ug/kg 14801530 97 50-149ND Vinyl chloride ug/kg 831 v3767109 57-157ND Xylene (Total)ug/kg 29802300 125 52-153105 1,2-Dichloroethane-d4 (S)%107 70-130 4-Bromofluorobenzene (S)%101 70-130 Toluene-d8 (S)%99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 95 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92678743018 4090659SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/kg ND 30ND 1,1,1-Trichloroethane ug/kg ND 30ND 1,1,2,2-Tetrachloroethane ug/kg ND 30ND 1,1,2-Trichloroethane ug/kg ND 30ND 1,1-Dichloroethane ug/kg ND 30ND 1,1-Dichloroethene ug/kg ND 30ND 1,1-Dichloropropene ug/kg ND 30ND 1,2,3-Trichlorobenzene ug/kg ND 30ND 1,2,3-Trichloropropane ug/kg ND 30ND 1,2,4-Trichlorobenzene ug/kg ND 30ND 1,2,4-Trimethylbenzene ug/kg ND 30ND 1,2-Dibromo-3-chloropropane ug/kg ND 30ND 1,2-Dibromoethane (EDB)ug/kg ND 30ND 1,2-Dichlorobenzene ug/kg ND 30ND 1,2-Dichloroethane ug/kg ND 30ND 1,2-Dichloropropane ug/kg ND 30ND 1,3,5-Trimethylbenzene ug/kg ND 30ND 1,3-Dichlorobenzene ug/kg ND 30ND 1,3-Dichloropropane ug/kg ND 30ND 1,4-Dichlorobenzene ug/kg ND 30ND 2,2-Dichloropropane ug/kg ND v230ND 2-Butanone (MEK)ug/kg ND 30ND 2-Chlorotoluene ug/kg ND 30ND 2-Hexanone ug/kg ND 30ND 4-Chlorotoluene ug/kg ND 30ND 4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND Acetone ug/kg ND 30ND Benzene ug/kg ND 30ND Bromobenzene ug/kg ND 30ND Bromochloromethane ug/kg ND 30ND Bromodichloromethane ug/kg ND 30ND Bromoform ug/kg ND 30ND Bromomethane ug/kg ND IH30ND Carbon tetrachloride ug/kg ND 30ND Chlorobenzene ug/kg ND 30ND Chloroethane ug/kg ND 30ND Chloroform ug/kg ND 30ND Chloromethane ug/kg ND 30ND cis-1,2-Dichloroethene ug/kg ND 30ND cis-1,3-Dichloropropene ug/kg ND 30ND Dibromochloromethane ug/kg ND 30ND Dibromomethane ug/kg ND 30ND Dichlorodifluoromethane ug/kg ND 30ND Diisopropyl ether ug/kg ND 30ND Ethylbenzene ug/kg ND 30ND Hexachloro-1,3-butadiene ug/kg ND 30ND Isopropylbenzene (Cumene)ug/kg ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 96 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92678743018 4090659SAMPLE DUPLICATE: m&p-Xylene ug/kg ND 30ND Methyl-tert-butyl ether ug/kg ND v230ND Methylene Chloride ug/kg ND 30ND n-Butylbenzene ug/kg ND 30ND n-Propylbenzene ug/kg ND 30ND Naphthalene ug/kg 5.8J 306.3J o-Xylene ug/kg ND 30ND p-Isopropyltoluene ug/kg ND 30ND sec-Butylbenzene ug/kg ND 30ND Styrene ug/kg ND 30ND tert-Butylbenzene ug/kg ND 30ND Tetrachloroethene ug/kg ND 30ND Toluene ug/kg ND 30ND trans-1,2-Dichloroethene ug/kg ND 30ND trans-1,3-Dichloropropene ug/kg ND 30ND Trichloroethene ug/kg ND 30ND Trichlorofluoromethane ug/kg ND 30ND Vinyl acetate ug/kg ND 30ND Vinyl chloride ug/kg ND v230ND Xylene (Total)ug/kg ND 30ND 1,2-Dichloroethane-d4 (S)%109107 4-Bromofluorobenzene (S)%97102 Toluene-d8 (S)%102101 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 97 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 788852 EPA 8260D EPA 8260D 8260D MSV Low Level Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples: 92678743019 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4089058 Associated Lab Samples:92678743019 Matrix: Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/25/23 01:260.31 1,1,1-Trichloroethane ug/L ND 1.0 07/25/23 01:260.33 1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/25/23 01:260.22 1,1,2-Trichloroethane ug/L ND 1.0 07/25/23 01:260.32 1,1-Dichloroethane ug/L ND 1.0 07/25/23 01:260.37 1,1-Dichloroethene ug/L ND 1.0 07/25/23 01:260.35 1,1-Dichloropropene ug/L ND 1.0 07/25/23 01:260.43 1,2,3-Trichlorobenzene ug/L ND 1.0 07/25/23 01:260.81 1,2,3-Trichloropropane ug/L ND 1.0 07/25/23 01:260.26 1,2,4-Trichlorobenzene ug/L ND 1.0 07/25/23 01:260.64 1,2-Dibromo-3-chloropropane ug/L ND 2.0 07/25/23 01:260.34 1,2-Dibromoethane (EDB)ug/L ND 1.0 07/25/23 01:260.27 1,2-Dichlorobenzene ug/L ND 1.0 07/25/23 01:260.34 1,2-Dichloroethane ug/L ND 1.0 07/25/23 01:260.32 1,2-Dichloropropane ug/L ND 1.0 07/25/23 01:260.36 1,3-Dichlorobenzene ug/L ND 1.0 07/25/23 01:260.34 1,3-Dichloropropane ug/L ND 1.0 07/25/23 01:260.28 1,4-Dichlorobenzene ug/L ND 1.0 07/25/23 01:260.33 2,2-Dichloropropane ug/L ND 1.0 07/25/23 01:260.39 2-Butanone (MEK)ug/L ND 5.0 07/25/23 01:264.0 2-Chlorotoluene ug/L ND 1.0 07/25/23 01:260.32 2-Hexanone ug/L ND 5.0 07/25/23 01:260.48 4-Chlorotoluene ug/L ND 1.0 07/25/23 01:260.32 4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/25/23 01:262.7 Acetone ug/L ND 25.0 07/25/23 01:265.1 Benzene ug/L ND 1.0 07/25/23 01:260.34 Bromobenzene ug/L ND 1.0 07/25/23 01:260.29 Bromochloromethane ug/L ND 1.0 07/25/23 01:260.47 Bromodichloromethane ug/L ND 1.0 07/25/23 01:260.31 Bromoform ug/L ND 1.0 07/25/23 01:260.34 Bromomethane ug/L ND 2.0 07/25/23 01:261.7 Carbon tetrachloride ug/L ND 1.0 07/25/23 01:260.33 Chlorobenzene ug/L ND 1.0 07/25/23 01:260.28 Chloroethane ug/L ND 1.0 07/25/23 01:260.65 Chloroform ug/L ND 1.0 07/25/23 01:260.43 Chloromethane ug/L ND 1.0 07/25/23 01:260.54 cis-1,2-Dichloroethene ug/L ND 1.0 07/25/23 01:260.38 cis-1,3-Dichloropropene ug/L ND 1.0 07/25/23 01:260.36 Dibromochloromethane ug/L ND 1.0 07/25/23 01:260.36 Dibromomethane ug/L ND 1.0 07/25/23 01:260.39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 98 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4089058 Associated Lab Samples:92678743019 Matrix: Water AnalyzedMDL Dichlorodifluoromethane ug/L ND 1.0 07/25/23 01:260.35 Diisopropyl ether ug/L ND 1.0 07/25/23 01:260.31 Ethylbenzene ug/L ND 1.0 07/25/23 01:260.30 Hexachloro-1,3-butadiene ug/L ND 2.0 07/25/23 01:261.5 m&p-Xylene ug/L ND 2.0 07/25/23 01:260.71 Methyl-tert-butyl ether ug/L ND 1.0 07/25/23 01:260.42 Methylene Chloride ug/L ND 5.0 07/25/23 01:262.0 Naphthalene ug/L ND 1.0 07/25/23 01:260.64 o-Xylene ug/L ND 1.0 07/25/23 01:260.34 p-Isopropyltoluene ug/L ND 1.0 07/25/23 01:260.41 Styrene ug/L ND 1.0 07/25/23 01:260.29 Tetrachloroethene ug/L ND 1.0 07/25/23 01:260.29 Toluene ug/L ND 1.0 07/25/23 01:260.24 trans-1,2-Dichloroethene ug/L ND 1.0 07/25/23 01:260.40 trans-1,3-Dichloropropene ug/L ND 1.0 07/25/23 01:260.36 Trichloroethene ug/L ND 1.0 07/25/23 01:260.38 Trichlorofluoromethane ug/L ND 1.0 07/25/23 01:260.30 Vinyl acetate ug/L ND 2.0 07/25/23 01:261.3 Vinyl chloride ug/L ND 1.0 07/25/23 01:260.39 Xylene (Total)ug/L ND 1.0 07/25/23 01:260.34 1,2-Dichloroethane-d4 (S)%101 70-130 07/25/23 01:26 4-Bromofluorobenzene (S)%97 70-130 07/25/23 01:26 Toluene-d8 (S)%104 70-130 07/25/23 01:26 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4089059LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 20.820 104 70-130 1,1,1-Trichloroethane ug/L 20.420 102 70-130 1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130 1,1,2-Trichloroethane ug/L 20.320 101 70-130 1,1-Dichloroethane ug/L 19.120 95 70-130 1,1-Dichloroethene ug/L 20.820 104 70-130 1,1-Dichloropropene ug/L 22.220 111 70-130 1,2,3-Trichlorobenzene ug/L 19.120 96 70-130 1,2,3-Trichloropropane ug/L 18.220 91 70-130 1,2,4-Trichlorobenzene ug/L 19.620 98 70-130 1,2-Dibromo-3-chloropropane ug/L 19.020 95 70-131 1,2-Dibromoethane (EDB)ug/L 20.620 103 70-130 1,2-Dichlorobenzene ug/L 20.120 100 70-130 1,2-Dichloroethane ug/L 19.720 99 70-130 1,2-Dichloropropane ug/L 20.020 100 70-130 1,3-Dichlorobenzene ug/L 20.320 101 70-130 1,3-Dichloropropane ug/L 20.120 101 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 99 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4089059LABORATORY CONTROL SAMPLE: LCSSpike 1,4-Dichlorobenzene ug/L 20.120 100 70-130 2,2-Dichloropropane ug/L 21.020 105 68-135 2-Butanone (MEK)ug/L 40.740 102 70-134 2-Chlorotoluene ug/L 20.620 103 70-130 2-Hexanone ug/L 42.340 106 70-131 4-Chlorotoluene ug/L 20.420 102 70-130 4-Methyl-2-pentanone (MIBK)ug/L 40.740 102 70-130 Acetone ug/L 38.940 97 70-133 Benzene ug/L 19.820 99 70-130 Bromobenzene ug/L 20.320 101 70-130 Bromochloromethane ug/L 20.620 103 70-130 Bromodichloromethane ug/L 18.620 93 70-130 Bromoform ug/L 19.020 95 70-130 Bromomethane ug/L 21.820 109 45-151 Carbon tetrachloride ug/L 19.320 96 70-130 Chlorobenzene ug/L 20.220 101 70-130 Chloroethane ug/L 20.120 100 39-152 Chloroform ug/L 18.920 95 70-130 Chloromethane ug/L 19.020 95 58-130 cis-1,2-Dichloroethene ug/L 19.420 97 70-130 cis-1,3-Dichloropropene ug/L 19.920 99 70-130 Dibromochloromethane ug/L 20.120 101 70-130 Dibromomethane ug/L 19.020 95 70-130 Dichlorodifluoromethane ug/L 20.920 105 54-133 Diisopropyl ether ug/L 19.920 99 70-130 Ethylbenzene ug/L 19.920 100 70-130 Hexachloro-1,3-butadiene ug/L 21.220 106 70-135 m&p-Xylene ug/L 38.940 97 70-130 Methyl-tert-butyl ether ug/L 19.920 100 70-130 Methylene Chloride ug/L 18.820 94 66-130 Naphthalene ug/L 19.320 97 70-130 o-Xylene ug/L 19.820 99 70-130 p-Isopropyltoluene ug/L 20.920 105 70-130 Styrene ug/L 19.820 99 70-130 Tetrachloroethene ug/L 19.720 98 70-130 Toluene ug/L 19.220 96 70-130 trans-1,2-Dichloroethene ug/L 19.020 95 70-130 trans-1,3-Dichloropropene ug/L 20.120 100 70-130 Trichloroethene ug/L 20.620 103 70-130 Trichlorofluoromethane ug/L 19.220 96 62-130 Vinyl acetate ug/L 43.140 108 70-144 Vinyl chloride ug/L 18.020 90 62-130 Xylene (Total)ug/L 58.660 98 70-130 1,2-Dichloroethane-d4 (S)%101 70-130 4-Bromofluorobenzene (S)%96 70-130 Toluene-d8 (S)%98 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 100 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4089955MATRIX SPIKE SAMPLE: MSSpike Result 92678311003 1,1,1,2-Tetrachloroethane ug/L 17.920 89 70-141ND 1,1,1-Trichloroethane ug/L 16.820 84 70-150ND 1,1,2,2-Tetrachloroethane ug/L 17.120 86 69-142ND 1,1,2-Trichloroethane ug/L 16.820 84 70-138ND 1,1-Dichloroethane ug/L 17.520 88 70-150ND 1,1-Dichloroethene ug/L 19.120 96 70-156ND 1,1-Dichloropropene ug/L 18.020 90 70-150ND 1,2,3-Trichlorobenzene ug/L 17.320 86 70-148ND 1,2,3-Trichloropropane ug/L 18.120 91 70-140ND 1,2,4-Trichlorobenzene ug/L 16.620 83 70-146ND 1,2-Dibromo-3-chloropropane ug/L 14.120 71 68-146ND 1,2-Dibromoethane (EDB)ug/L 17.620 88 70-138ND 1,2-Dichlorobenzene ug/L 17.820 89 70-141ND 1,2-Dichloroethane ug/L 17.120 86 69-143ND 1,2-Dichloropropane ug/L 17.720 89 68-156ND 1,3-Dichlorobenzene ug/L 17.920 89 70-143ND 1,3-Dichloropropane ug/L 17.720 89 70-138ND 1,4-Dichlorobenzene ug/L 18.120 91 70-142ND 2,2-Dichloropropane ug/L 16.620 83 52-170ND 2-Butanone (MEK)ug/L 32.640 81 60-157ND 2-Chlorotoluene ug/L 17.320 87 70-147ND 2-Hexanone ug/L 33.940 85 68-146ND 4-Chlorotoluene ug/L 17.120 86 70-142ND 4-Methyl-2-pentanone (MIBK)ug/L 31.440 78 70-141ND Acetone ug/L 31.540 79 58-157ND Benzene ug/L 18.520 93 70-142ND Bromobenzene ug/L 17.820 89 70-143ND Bromochloromethane ug/L 18.120 90 70-146ND Bromodichloromethane ug/L 15.320 76 70-139ND Bromoform ug/L 13.520 68 64-140ND Bromomethane ug/L 12.520 63 28-192ND Carbon tetrachloride ug/L 19.220 96 70-148ND Chlorobenzene ug/L 18.720 94 70-141ND Chloroethane ug/L 20.620 103 58-191ND Chloroform ug/L 16.920 84 70-148ND Chloromethane ug/L 19.220 96 43-162ND cis-1,2-Dichloroethene ug/L 17.020 85 68-151ND cis-1,3-Dichloropropene ug/L 15.720 78 70-139ND Dibromochloromethane ug/L 15.520 78 70-144ND Dibromomethane ug/L 18.220 91 70-139ND Dichlorodifluoromethane ug/L 23.320 116 39-171ND Diisopropyl ether ug/L 15.120 76 67-142ND Ethylbenzene ug/L 18.820 94 70-143ND Hexachloro-1,3-butadiene ug/L 17.720 89 64-163ND m&p-Xylene ug/L 36.340 91 70-144ND Methyl-tert-butyl ether ug/L 14.020 70 65-143ND Methylene Chloride ug/L 18.420 92 62-149ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 101 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4089955MATRIX SPIKE SAMPLE: MSSpike Result 92678311003 Naphthalene ug/L 15.920 80 67-147ND o-Xylene ug/L 17.920 90 70-145ND p-Isopropyltoluene ug/L 17.320 86 70-147ND Styrene ug/L 17.220 86 70-143ND Tetrachloroethene ug/L 19.320 96 70-145ND Toluene ug/L 17.820 89 70-142ND trans-1,2-Dichloroethene ug/L 17.820 89 70-151ND trans-1,3-Dichloropropene ug/L 15.620 78 70-139ND Trichloroethene ug/L 18.320 91 62-146ND Trichlorofluoromethane ug/L 19.420 97 63-153ND Vinyl acetate ug/L 27.640 69 61-162ND Vinyl chloride ug/L 16.020 80 61-163ND Xylene (Total)ug/L 54.260 90 70-143ND 1,2-Dichloroethane-d4 (S)%96 70-130 4-Bromofluorobenzene (S)%95 70-130 Toluene-d8 (S)%98 70-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92678311002 4089954SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/L ND 30ND 1,1,1-Trichloroethane ug/L ND 30ND 1,1,2,2-Tetrachloroethane ug/L ND 30ND 1,1,2-Trichloroethane ug/L ND 30ND 1,1-Dichloroethane ug/L ND 30ND 1,1-Dichloroethene ug/L ND 30ND 1,1-Dichloropropene ug/L ND 30ND 1,2,3-Trichlorobenzene ug/L ND 30ND 1,2,3-Trichloropropane ug/L ND 30ND 1,2,4-Trichlorobenzene ug/L ND 30ND 1,2-Dibromo-3-chloropropane ug/L ND 30ND 1,2-Dibromoethane (EDB)ug/L ND 30ND 1,2-Dichlorobenzene ug/L ND 30ND 1,2-Dichloroethane ug/L ND 30ND 1,2-Dichloropropane ug/L ND 30ND 1,3-Dichlorobenzene ug/L ND 30ND 1,3-Dichloropropane ug/L ND 30ND 1,4-Dichlorobenzene ug/L ND 30ND 2,2-Dichloropropane ug/L ND 30ND 2-Butanone (MEK)ug/L ND 30ND 2-Chlorotoluene ug/L ND 30ND 2-Hexanone ug/L ND 30ND 4-Chlorotoluene ug/L ND 30ND 4-Methyl-2-pentanone (MIBK)ug/L ND 30ND Acetone ug/L ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 102 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92678311002 4089954SAMPLE DUPLICATE: Benzene ug/L ND 30ND Bromobenzene ug/L ND 30ND Bromochloromethane ug/L ND 30ND Bromodichloromethane ug/L ND 30ND Bromoform ug/L ND 30ND Bromomethane ug/L ND 30ND Carbon tetrachloride ug/L ND 30ND Chlorobenzene ug/L ND 30ND Chloroethane ug/L ND 30ND Chloroform ug/L ND 30ND Chloromethane ug/L ND 30ND cis-1,2-Dichloroethene ug/L ND 30ND cis-1,3-Dichloropropene ug/L ND 30ND Dibromochloromethane ug/L ND 30ND Dibromomethane ug/L ND 30ND Dichlorodifluoromethane ug/L ND 30ND Diisopropyl ether ug/L ND 30ND Ethylbenzene ug/L ND 30ND Hexachloro-1,3-butadiene ug/L ND 30ND m&p-Xylene ug/L ND 30ND Methyl-tert-butyl ether ug/L ND 30ND Methylene Chloride ug/L ND 30ND Naphthalene ug/L ND 30ND o-Xylene ug/L ND 30ND p-Isopropyltoluene ug/L ND 30ND Styrene ug/L ND 30ND Tetrachloroethene ug/L ND 30ND Toluene ug/L ND 30ND trans-1,2-Dichloroethene ug/L ND 30ND trans-1,3-Dichloropropene ug/L ND 30ND Trichloroethene ug/L ND 30ND Trichlorofluoromethane ug/L ND 30ND Vinyl acetate ug/L ND 30ND Vinyl chloride ug/L ND 30ND Xylene (Total)ug/L ND 30ND 1,2-Dichloroethane-d4 (S)%90103 4-Bromofluorobenzene (S)%9196 Toluene-d8 (S)%105102 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 103 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 789175 EPA 8260D EPA 8260D 8260D MSV Low Level Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples: 92678743011, 92678743012, 92678743013 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4090531 Associated Lab Samples:92678743011, 92678743012, 92678743013 Matrix: Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/27/23 00:320.31 1,1,1-Trichloroethane ug/L ND 1.0 07/27/23 00:320.33 1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/27/23 00:320.22 1,1,2-Trichloroethane ug/L ND 1.0 07/27/23 00:320.32 1,1-Dichloroethane ug/L ND 1.0 07/27/23 00:320.37 1,1-Dichloroethene ug/L ND 1.0 07/27/23 00:320.35 1,1-Dichloropropene ug/L ND 1.0 07/27/23 00:320.43 1,2,3-Trichlorobenzene ug/L ND 1.0 07/27/23 00:320.81 1,2,3-Trichloropropane ug/L ND 1.0 07/27/23 00:320.26 1,2,4-Trichlorobenzene ug/L ND 1.0 07/27/23 00:320.64 1,2-Dibromo-3-chloropropane ug/L ND 2.0 07/27/23 00:320.34 1,2-Dibromoethane (EDB)ug/L ND 1.0 07/27/23 00:320.27 1,2-Dichlorobenzene ug/L ND 1.0 07/27/23 00:320.34 1,2-Dichloroethane ug/L ND 1.0 07/27/23 00:320.32 1,2-Dichloropropane ug/L ND 1.0 07/27/23 00:320.36 1,3-Dichlorobenzene ug/L ND 1.0 07/27/23 00:320.34 1,3-Dichloropropane ug/L ND 1.0 07/27/23 00:320.28 1,4-Dichlorobenzene ug/L ND 1.0 07/27/23 00:320.33 2,2-Dichloropropane ug/L ND 1.0 07/27/23 00:320.39 2-Butanone (MEK)ug/L ND 5.0 07/27/23 00:324.0 2-Chlorotoluene ug/L ND 1.0 07/27/23 00:320.32 2-Hexanone ug/L ND 5.0 07/27/23 00:320.48 4-Chlorotoluene ug/L ND 1.0 07/27/23 00:320.32 4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/27/23 00:322.7 Acetone ug/L ND 25.0 07/27/23 00:325.1 Benzene ug/L ND 1.0 07/27/23 00:320.34 Bromobenzene ug/L ND 1.0 07/27/23 00:320.29 Bromochloromethane ug/L ND 1.0 07/27/23 00:320.47 Bromodichloromethane ug/L ND 1.0 07/27/23 00:320.31 Bromoform ug/L ND 1.0 07/27/23 00:320.34 Bromomethane ug/L ND 2.0 07/27/23 00:321.7 Carbon tetrachloride ug/L ND 1.0 07/27/23 00:320.33 Chlorobenzene ug/L ND 1.0 07/27/23 00:320.28 Chloroethane ug/L ND 1.0 07/27/23 00:320.65 Chloroform ug/L ND 1.0 07/27/23 00:320.43 Chloromethane ug/L ND 1.0 07/27/23 00:320.54 cis-1,2-Dichloroethene ug/L ND 1.0 07/27/23 00:320.38 cis-1,3-Dichloropropene ug/L ND 1.0 07/27/23 00:320.36 Dibromochloromethane ug/L ND 1.0 07/27/23 00:320.36 Dibromomethane ug/L ND 1.0 07/27/23 00:320.39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 104 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4090531 Associated Lab Samples:92678743011, 92678743012, 92678743013 Matrix: Water AnalyzedMDL Dichlorodifluoromethane ug/L ND 1.0 07/27/23 00:320.35 Diisopropyl ether ug/L ND 1.0 07/27/23 00:320.31 Ethylbenzene ug/L ND 1.0 07/27/23 00:320.30 Hexachloro-1,3-butadiene ug/L ND 2.0 07/27/23 00:321.5 m&p-Xylene ug/L ND 2.0 07/27/23 00:320.71 Methyl-tert-butyl ether ug/L ND 1.0 07/27/23 00:320.42 Methylene Chloride ug/L ND 5.0 07/27/23 00:322.0 Naphthalene ug/L ND 1.0 07/27/23 00:320.64 o-Xylene ug/L ND 1.0 07/27/23 00:320.34 p-Isopropyltoluene ug/L ND 1.0 07/27/23 00:320.41 Styrene ug/L ND 1.0 07/27/23 00:320.29 Tetrachloroethene ug/L ND 1.0 07/27/23 00:320.29 Toluene ug/L ND 1.0 07/27/23 00:320.24 trans-1,2-Dichloroethene ug/L ND 1.0 07/27/23 00:320.40 trans-1,3-Dichloropropene ug/L ND 1.0 07/27/23 00:320.36 Trichloroethene ug/L ND 1.0 07/27/23 00:320.38 Trichlorofluoromethane ug/L ND 1.0 07/27/23 00:320.30 Vinyl acetate ug/L ND 2.0 07/27/23 00:321.3 Vinyl chloride ug/L ND 1.0 07/27/23 00:320.39 Xylene (Total)ug/L ND 1.0 07/27/23 00:320.34 1,2-Dichloroethane-d4 (S)%103 70-130 07/27/23 00:32 4-Bromofluorobenzene (S)%99 70-130 07/27/23 00:32 Toluene-d8 (S)%100 70-130 07/27/23 00:32 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4090532LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 20.320 101 70-130 1,1,1-Trichloroethane ug/L 20.320 102 70-130 1,1,2,2-Tetrachloroethane ug/L 20.920 105 70-130 1,1,2-Trichloroethane ug/L 20.220 101 70-130 1,1-Dichloroethane ug/L 20.720 103 70-130 1,1-Dichloroethene ug/L 20.920 105 70-130 1,1-Dichloropropene ug/L 21.120 105 70-130 1,2,3-Trichlorobenzene ug/L 20.420 102 70-130 1,2,3-Trichloropropane ug/L 19.820 99 70-130 1,2,4-Trichlorobenzene ug/L 20.020 100 70-130 1,2-Dibromo-3-chloropropane ug/L 19.520 97 70-131 1,2-Dibromoethane (EDB)ug/L 20.520 103 70-130 1,2-Dichlorobenzene ug/L 20.020 100 70-130 1,2-Dichloroethane ug/L 20.320 101 70-130 1,2-Dichloropropane ug/L 20.720 104 70-130 1,3-Dichlorobenzene ug/L 20.320 101 70-130 1,3-Dichloropropane ug/L 19.720 99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 105 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4090532LABORATORY CONTROL SAMPLE: LCSSpike 1,4-Dichlorobenzene ug/L 20.320 101 70-130 2,2-Dichloropropane ug/L 19.320 97 68-135 2-Butanone (MEK)ug/L 40.340 101 70-134 2-Chlorotoluene ug/L 20.020 100 70-130 2-Hexanone ug/L 41.640 104 70-131 4-Chlorotoluene ug/L 20.220 101 70-130 4-Methyl-2-pentanone (MIBK)ug/L 40.040 100 70-130 Acetone ug/L 42.040 105 70-133 Benzene ug/L 20.020 100 70-130 Bromobenzene ug/L 19.420 97 70-130 Bromochloromethane ug/L 21.620 108 70-130 Bromodichloromethane ug/L 19.520 98 70-130 Bromoform ug/L 19.520 98 70-130 Bromomethane ug/L 17.720 89 45-151 Carbon tetrachloride ug/L 20.020 100 70-130 Chlorobenzene ug/L 20.420 102 70-130 Chloroethane ug/L 21.420 107 39-152 Chloroform ug/L 20.020 100 70-130 Chloromethane ug/L 21.220 106 58-130 cis-1,2-Dichloroethene ug/L 20.720 104 70-130 cis-1,3-Dichloropropene ug/L 19.920 100 70-130 Dibromochloromethane ug/L 20.120 100 70-130 Dibromomethane ug/L 19.620 98 70-130 Dichlorodifluoromethane ug/L 23.820 119 54-133 Diisopropyl ether ug/L 20.320 101 70-130 Ethylbenzene ug/L 19.820 99 70-130 Hexachloro-1,3-butadiene ug/L 20.120 101 70-135 m&p-Xylene ug/L 40.640 102 70-130 Methyl-tert-butyl ether ug/L 19.220 96 70-130 Methylene Chloride ug/L 19.620 98 66-130 Naphthalene ug/L 20.920 105 70-130 o-Xylene ug/L 20.020 100 70-130 p-Isopropyltoluene ug/L 20.120 101 70-130 Styrene ug/L 20.620 103 70-130 Tetrachloroethene ug/L 19.420 97 70-130 Toluene ug/L 19.520 98 70-130 trans-1,2-Dichloroethene ug/L 20.520 103 70-130 trans-1,3-Dichloropropene ug/L 19.920 99 70-130 Trichloroethene ug/L 20.020 100 70-130 Trichlorofluoromethane ug/L 21.320 107 62-130 Vinyl acetate ug/L 40.440 101 70-144 Vinyl chloride ug/L 17.320 86 62-130 Xylene (Total)ug/L 60.660 101 70-130 1,2-Dichloroethane-d4 (S)%102 70-130 4-Bromofluorobenzene (S)%101 70-130 Toluene-d8 (S)%99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 106 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4090534MATRIX SPIKE SAMPLE: MSSpike Result 92678339001 1,1,1,2-Tetrachloroethane ug/L 24.020 120 70-141ND 1,1,1-Trichloroethane ug/L 25.520 128 70-150ND 1,1,2,2-Tetrachloroethane ug/L 23.320 116 69-142ND 1,1,2-Trichloroethane ug/L 23.420 117 70-138ND 1,1-Dichloroethane ug/L 24.920 124 70-150ND 1,1-Dichloroethene ug/L 27.120 136 70-156ND 1,1-Dichloropropene ug/L 27.320 136 70-150ND 1,2,3-Trichlorobenzene ug/L 22.820 114 70-148ND 1,2,3-Trichloropropane ug/L 22.920 115 70-140ND 1,2,4-Trichlorobenzene ug/L 22.920 115 70-146ND 1,2-Dibromo-3-chloropropane ug/L 21.620 108 68-146ND 1,2-Dibromoethane (EDB)ug/L 23.220 116 70-138ND 1,2-Dichlorobenzene ug/L 23.920 120 70-141ND 1,2-Dichloroethane ug/L 23.320 117 69-143ND 1,2-Dichloropropane ug/L 24.320 122 68-156ND 1,3-Dichlorobenzene ug/L 24.120 120 70-143ND 1,3-Dichloropropane ug/L 22.720 114 70-138ND 1,4-Dichlorobenzene ug/L 23.820 119 70-142ND 2,2-Dichloropropane ug/L 25.820 129 52-170ND 2-Butanone (MEK)ug/L 47.340 118 60-157ND 2-Chlorotoluene ug/L 24.320 121 70-147ND 2-Hexanone ug/L 45.940 115 68-146ND 4-Chlorotoluene ug/L 24.320 122 70-142ND 4-Methyl-2-pentanone (MIBK)ug/L 45.740 114 70-141ND Acetone ug/L 45.640 110 58-157ND Benzene ug/L 24.520 122 70-142ND Bromobenzene ug/L 23.320 117 70-143ND Bromochloromethane ug/L 25.020 125 70-146ND Bromodichloromethane ug/L 23.020 115 70-139ND Bromoform ug/L 22.120 110 64-140ND Bromomethane ug/L 9.9 v32050 28-192ND Carbon tetrachloride ug/L 25.920 129 70-148ND Chlorobenzene ug/L 23.920 120 70-141ND Chloroethane ug/L 27.720 139 58-191ND Chloroform ug/L 24.720 124 70-148ND Chloromethane ug/L 25.420 127 43-162ND cis-1,2-Dichloroethene ug/L 26.620 126 68-1511.4 cis-1,3-Dichloropropene ug/L 22.420 112 70-139ND Dibromochloromethane ug/L 23.020 115 70-144ND Dibromomethane ug/L 22.720 113 70-139ND Dichlorodifluoromethane ug/L 34.5 M120172 39-171ND Diisopropyl ether ug/L 23.520 117 67-142ND Ethylbenzene ug/L 23.720 118 70-143ND Hexachloro-1,3-butadiene ug/L 26.220 131 64-163ND m&p-Xylene ug/L 47.940 120 70-144ND Methyl-tert-butyl ether ug/L 21.920 109 65-143ND Methylene Chloride ug/L 22.120 109 62-149ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 107 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4090534MATRIX SPIKE SAMPLE: MSSpike Result 92678339001 Naphthalene ug/L 21.920 109 67-147ND o-Xylene ug/L 23.020 115 70-145ND p-Isopropyltoluene ug/L 25.120 125 70-147ND Styrene ug/L 23.820 119 70-143ND Tetrachloroethene ug/L 24.120 121 70-145ND Toluene ug/L 23.920 119 70-142ND trans-1,2-Dichloroethene ug/L 26.020 130 70-151ND trans-1,3-Dichloropropene ug/L 22.720 113 70-139ND Trichloroethene ug/L 13320 138 62-146105 Trichlorofluoromethane ug/L 30.120 150 63-153ND Vinyl acetate ug/L 46.040 115 61-162ND Vinyl chloride ug/L 22.420 112 61-163ND Xylene (Total)ug/L 71.060 118 70-143ND 1,2-Dichloroethane-d4 (S)%104 70-130 4-Bromofluorobenzene (S)%98 70-130 Toluene-d8 (S)%99 70-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92678339002 4090533SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/L ND 30ND 1,1,1-Trichloroethane ug/L ND 30ND 1,1,2,2-Tetrachloroethane ug/L ND 30ND 1,1,2-Trichloroethane ug/L ND 30ND 1,1-Dichloroethane ug/L ND 30ND 1,1-Dichloroethene ug/L ND 30ND 1,1-Dichloropropene ug/L ND 30ND 1,2,3-Trichlorobenzene ug/L ND 30ND 1,2,3-Trichloropropane ug/L ND 30ND 1,2,4-Trichlorobenzene ug/L ND 30ND 1,2-Dibromo-3-chloropropane ug/L ND 30ND 1,2-Dibromoethane (EDB)ug/L ND 30ND 1,2-Dichlorobenzene ug/L ND 30ND 1,2-Dichloroethane ug/L ND 30ND 1,2-Dichloropropane ug/L ND 30ND 1,3-Dichlorobenzene ug/L ND 30ND 1,3-Dichloropropane ug/L ND 30ND 1,4-Dichlorobenzene ug/L ND 30ND 2,2-Dichloropropane ug/L ND 30ND 2-Butanone (MEK)ug/L ND 30ND 2-Chlorotoluene ug/L ND 30ND 2-Hexanone ug/L ND 30ND 4-Chlorotoluene ug/L ND 30ND 4-Methyl-2-pentanone (MIBK)ug/L ND 30ND Acetone ug/L ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 108 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92678339002 4090533SAMPLE DUPLICATE: Benzene ug/L ND 30ND Bromobenzene ug/L ND 30ND Bromochloromethane ug/L ND 30ND Bromodichloromethane ug/L ND 30ND Bromoform ug/L ND 30ND Bromomethane ug/L ND v230ND Carbon tetrachloride ug/L ND 30ND Chlorobenzene ug/L ND 30ND Chloroethane ug/L ND 30ND Chloroform ug/L 0.46J 30ND Chloromethane ug/L ND 30ND cis-1,2-Dichloroethene ug/L ND 30ND cis-1,3-Dichloropropene ug/L ND 30ND Dibromochloromethane ug/L ND 30ND Dibromomethane ug/L ND 30ND Dichlorodifluoromethane ug/L ND 30ND Diisopropyl ether ug/L ND 30ND Ethylbenzene ug/L ND 30ND Hexachloro-1,3-butadiene ug/L ND 30ND m&p-Xylene ug/L ND 30ND Methyl-tert-butyl ether ug/L ND 30ND Methylene Chloride ug/L ND 30ND Naphthalene ug/L ND 30ND o-Xylene ug/L ND 30ND p-Isopropyltoluene ug/L ND 30ND Styrene ug/L ND 30ND Tetrachloroethene ug/L ND 30ND Toluene ug/L ND 30ND trans-1,2-Dichloroethene ug/L ND 30ND trans-1,3-Dichloropropene ug/L ND 30ND Trichloroethene ug/L 7.6 3 307.3 Trichlorofluoromethane ug/L ND 30ND Vinyl acetate ug/L ND 30ND Vinyl chloride ug/L ND 30ND Xylene (Total)ug/L ND 30ND 1,2-Dichloroethane-d4 (S)%103103 4-Bromofluorobenzene (S)%99100 Toluene-d8 (S)%9999 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 109 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 789177 EPA 8260D EPA 8260D 8260D MSV Low Level Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples: 92678743014, 92678743015, 92678743016, 92678743017 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4090551 Associated Lab Samples:92678743014, 92678743015, 92678743016, 92678743017 Matrix: Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/27/23 00:140.31 1,1,1-Trichloroethane ug/L ND 1.0 07/27/23 00:140.33 1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/27/23 00:140.22 1,1,2-Trichloroethane ug/L ND 1.0 07/27/23 00:140.32 1,1-Dichloroethane ug/L ND 1.0 07/27/23 00:140.37 1,1-Dichloroethene ug/L ND 1.0 07/27/23 00:140.35 1,1-Dichloropropene ug/L ND 1.0 07/27/23 00:140.43 1,2,3-Trichlorobenzene ug/L ND 1.0 07/27/23 00:140.81 1,2,3-Trichloropropane ug/L ND 1.0 07/27/23 00:140.26 1,2,4-Trichlorobenzene ug/L ND 1.0 07/27/23 00:140.64 1,2-Dibromo-3-chloropropane ug/L ND 2.0 07/27/23 00:140.34 1,2-Dibromoethane (EDB)ug/L ND 1.0 07/27/23 00:140.27 1,2-Dichlorobenzene ug/L ND 1.0 07/27/23 00:140.34 1,2-Dichloroethane ug/L ND 1.0 07/27/23 00:140.32 1,2-Dichloropropane ug/L ND 1.0 07/27/23 00:140.36 1,3-Dichlorobenzene ug/L ND 1.0 07/27/23 00:140.34 1,3-Dichloropropane ug/L ND 1.0 07/27/23 00:140.28 1,4-Dichlorobenzene ug/L ND 1.0 07/27/23 00:140.33 2,2-Dichloropropane ug/L ND 1.0 07/27/23 00:140.39 2-Butanone (MEK)ug/L ND 5.0 07/27/23 00:144.0 2-Chlorotoluene ug/L ND 1.0 07/27/23 00:140.32 2-Hexanone ug/L ND 5.0 07/27/23 00:140.48 4-Chlorotoluene ug/L ND 1.0 07/27/23 00:140.32 4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/27/23 00:142.7 Acetone ug/L ND 25.0 07/27/23 00:145.1 Benzene ug/L ND 1.0 07/27/23 00:140.34 Bromobenzene ug/L ND 1.0 07/27/23 00:140.29 Bromochloromethane ug/L ND 1.0 07/27/23 00:140.47 Bromodichloromethane ug/L ND 1.0 07/27/23 00:140.31 Bromoform ug/L ND 1.0 07/27/23 00:140.34 Bromomethane ug/L ND 2.0 07/27/23 00:141.7 Carbon tetrachloride ug/L ND 1.0 07/27/23 00:140.33 Chlorobenzene ug/L ND 1.0 07/27/23 00:140.28 Chloroethane ug/L ND 1.0 07/27/23 00:140.65 Chloroform ug/L ND 1.0 07/27/23 00:140.43 Chloromethane ug/L ND 1.0 07/27/23 00:140.54 cis-1,2-Dichloroethene ug/L ND 1.0 07/27/23 00:140.38 cis-1,3-Dichloropropene ug/L ND 1.0 07/27/23 00:140.36 Dibromochloromethane ug/L ND 1.0 07/27/23 00:140.36 Dibromomethane ug/L ND 1.0 07/27/23 00:140.39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 110 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4090551 Associated Lab Samples:92678743014, 92678743015, 92678743016, 92678743017 Matrix: Water AnalyzedMDL Dichlorodifluoromethane ug/L ND 1.0 07/27/23 00:140.35 Diisopropyl ether ug/L ND 1.0 07/27/23 00:140.31 Ethylbenzene ug/L ND 1.0 07/27/23 00:140.30 Hexachloro-1,3-butadiene ug/L ND 2.0 07/27/23 00:141.5 m&p-Xylene ug/L ND 2.0 07/27/23 00:140.71 Methyl-tert-butyl ether ug/L ND 1.0 07/27/23 00:140.42 Methylene Chloride ug/L ND 5.0 07/27/23 00:142.0 Naphthalene ug/L ND 1.0 07/27/23 00:140.64 o-Xylene ug/L ND 1.0 07/27/23 00:140.34 p-Isopropyltoluene ug/L ND 1.0 07/27/23 00:140.41 Styrene ug/L ND 1.0 07/27/23 00:140.29 Tetrachloroethene ug/L ND 1.0 07/27/23 00:140.29 Toluene ug/L ND 1.0 07/27/23 00:140.24 trans-1,2-Dichloroethene ug/L ND 1.0 07/27/23 00:140.40 trans-1,3-Dichloropropene ug/L ND 1.0 07/27/23 00:140.36 Trichloroethene ug/L ND 1.0 07/27/23 00:140.38 Trichlorofluoromethane ug/L ND 1.0 07/27/23 00:140.30 Vinyl acetate ug/L ND 2.0 07/27/23 00:141.3 Vinyl chloride ug/L ND 1.0 07/27/23 00:140.39 Xylene (Total)ug/L ND 1.0 07/27/23 00:140.34 1,2-Dichloroethane-d4 (S)%102 70-130 07/27/23 00:14 4-Bromofluorobenzene (S)%98 70-130 07/27/23 00:14 Toluene-d8 (S)%100 70-130 07/27/23 00:14 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4090552LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 20.520 102 70-130 1,1,1-Trichloroethane ug/L 20.920 105 70-130 1,1,2,2-Tetrachloroethane ug/L 20.420 102 70-130 1,1,2-Trichloroethane ug/L 20.320 101 70-130 1,1-Dichloroethane ug/L 20.920 105 70-130 1,1-Dichloroethene ug/L 21.520 108 70-130 1,1-Dichloropropene ug/L 21.720 109 70-130 1,2,3-Trichlorobenzene ug/L 20.420 102 70-130 1,2,3-Trichloropropane ug/L 19.420 97 70-130 1,2,4-Trichlorobenzene ug/L 20.120 100 70-130 1,2-Dibromo-3-chloropropane ug/L 19.320 97 70-131 1,2-Dibromoethane (EDB)ug/L 20.520 102 70-130 1,2-Dichlorobenzene ug/L 20.620 103 70-130 1,2-Dichloroethane ug/L 20.620 103 70-130 1,2-Dichloropropane ug/L 20.720 103 70-130 1,3-Dichlorobenzene ug/L 20.720 103 70-130 1,3-Dichloropropane ug/L 19.720 98 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 111 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4090552LABORATORY CONTROL SAMPLE: LCSSpike 1,4-Dichlorobenzene ug/L 20.420 102 70-130 2,2-Dichloropropane ug/L 19.820 99 68-135 2-Butanone (MEK)ug/L 40.540 101 70-134 2-Chlorotoluene ug/L 20.820 104 70-130 2-Hexanone ug/L 41.440 103 70-131 4-Chlorotoluene ug/L 20.820 104 70-130 4-Methyl-2-pentanone (MIBK)ug/L 39.740 99 70-130 Acetone ug/L 41.840 104 70-133 Benzene ug/L 20.620 103 70-130 Bromobenzene ug/L 19.820 99 70-130 Bromochloromethane ug/L 21.520 107 70-130 Bromodichloromethane ug/L 20.020 100 70-130 Bromoform ug/L 19.420 97 70-130 Bromomethane ug/L 18.720 94 45-151 Carbon tetrachloride ug/L 20.320 102 70-130 Chlorobenzene ug/L 20.520 102 70-130 Chloroethane ug/L 22.420 112 39-152 Chloroform ug/L 20.620 103 70-130 Chloromethane ug/L 21.820 109 58-130 cis-1,2-Dichloroethene ug/L 21.420 107 70-130 cis-1,3-Dichloropropene ug/L 20.120 101 70-130 Dibromochloromethane ug/L 20.420 102 70-130 Dibromomethane ug/L 20.020 100 70-130 Dichlorodifluoromethane ug/L 24.120 120 54-133 Diisopropyl ether ug/L 20.320 101 70-130 Ethylbenzene ug/L 20.320 101 70-130 Hexachloro-1,3-butadiene ug/L 21.520 107 70-135 m&p-Xylene ug/L 41.240 103 70-130 Methyl-tert-butyl ether ug/L 19.320 97 70-130 Methylene Chloride ug/L 19.620 98 66-130 Naphthalene ug/L 20.620 103 70-130 o-Xylene ug/L 20.320 102 70-130 p-Isopropyltoluene ug/L 20.820 104 70-130 Styrene ug/L 20.420 102 70-130 Tetrachloroethene ug/L 19.520 98 70-130 Toluene ug/L 20.020 100 70-130 trans-1,2-Dichloroethene ug/L 21.620 108 70-130 trans-1,3-Dichloropropene ug/L 20.120 100 70-130 Trichloroethene ug/L 20.320 101 70-130 Trichlorofluoromethane ug/L 21.920 109 62-130 Vinyl acetate ug/L 40.340 101 70-144 Vinyl chloride ug/L 17.620 88 62-130 Xylene (Total)ug/L 61.560 102 70-130 1,2-Dichloroethane-d4 (S)%103 70-130 4-Bromofluorobenzene (S)%100 70-130 Toluene-d8 (S)%100 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 112 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4090554MATRIX SPIKE SAMPLE: MSSpike Result 92678743015 1,1,1,2-Tetrachloroethane ug/L 25.820 129 70-141ND 1,1,1-Trichloroethane ug/L 27.820 139 70-150ND 1,1,2,2-Tetrachloroethane ug/L 25.420 127 69-142ND 1,1,2-Trichloroethane ug/L 25.420 127 70-138ND 1,1-Dichloroethane ug/L 26.920 134 70-150ND 1,1-Dichloroethene ug/L 29.220 146 70-156ND 1,1-Dichloropropene ug/L 29.520 147 70-150ND 1,2,3-Trichlorobenzene ug/L 25.020 125 70-148ND 1,2,3-Trichloropropane ug/L 24.420 122 70-140ND 1,2,4-Trichlorobenzene ug/L 24.620 123 70-146ND 1,2-Dibromo-3-chloropropane ug/L 24.520 123 68-146ND 1,2-Dibromoethane (EDB)ug/L 25.620 128 70-138ND 1,2-Dichlorobenzene ug/L 25.720 128 70-141ND 1,2-Dichloroethane ug/L 25.520 128 69-143ND 1,2-Dichloropropane ug/L 26.220 131 68-156ND 1,3-Dichlorobenzene ug/L 25.820 129 70-143ND 1,3-Dichloropropane ug/L 24.820 124 70-138ND 1,4-Dichlorobenzene ug/L 25.420 127 70-142ND 2,2-Dichloropropane ug/L 26.520 132 52-170ND 2-Butanone (MEK)ug/L 58.240 145 60-157ND 2-Chlorotoluene ug/L 26.120 131 70-147ND 2-Hexanone ug/L 53.540 133 68-146ND 4-Chlorotoluene ug/L 26.020 130 70-142ND 4-Methyl-2-pentanone (MIBK)ug/L 51.740 129 70-141ND Acetone ug/L 52.340 122 58-157ND Benzene ug/L 26.620 133 70-142ND Bromobenzene ug/L 24.920 125 70-143ND Bromochloromethane ug/L 26.520 132 70-146ND Bromodichloromethane ug/L 24.820 124 70-139ND Bromoform ug/L 23.920 119 64-140ND Bromomethane ug/L 15.9 v32073 28-192ND Carbon tetrachloride ug/L 27.620 138 70-148ND Chlorobenzene ug/L 26.020 130 70-141ND Chloroethane ug/L 28.920 144 58-191ND Chloroform ug/L 28.320 133 70-1481.6 Chloromethane ug/L 73.320 79 43-16257.6 cis-1,2-Dichloroethene ug/L 26.820 134 68-151ND cis-1,3-Dichloropropene ug/L 24.120 121 70-139ND Dibromochloromethane ug/L 25.020 125 70-144ND Dibromomethane ug/L 24.720 123 70-139ND Dichlorodifluoromethane ug/L 37.2 M120186 39-171ND Diisopropyl ether ug/L 25.720 128 67-142ND Ethylbenzene ug/L 25.720 129 70-143ND Hexachloro-1,3-butadiene ug/L 27.020 135 64-163ND m&p-Xylene ug/L 52.040 130 70-144ND Methyl-tert-butyl ether ug/L 28.620 123 65-1434.0 Methylene Chloride ug/L 23.920 118 62-149ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 113 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4090554MATRIX SPIKE SAMPLE: MSSpike Result 92678743015 Naphthalene ug/L 25.720 129 67-147ND o-Xylene ug/L 25.320 126 70-145ND p-Isopropyltoluene ug/L 26.520 132 70-147ND Styrene ug/L 26.120 130 70-143ND Tetrachloroethene ug/L 26.020 130 70-145ND Toluene ug/L 25.720 128 70-142ND trans-1,2-Dichloroethene ug/L 27.420 137 70-151ND trans-1,3-Dichloropropene ug/L 24.320 122 70-139ND Trichloroethene ug/L 26.120 130 62-146ND Trichlorofluoromethane ug/L 31.8 M120159 63-153ND Vinyl acetate ug/L 47.340 118 61-162ND Vinyl chloride ug/L 23.820 119 61-163ND Xylene (Total)ug/L 77.360 129 70-143ND 1,2-Dichloroethane-d4 (S)%103 70-130 4-Bromofluorobenzene (S)%101 70-130 Toluene-d8 (S)%99 70-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92678743014 4090553SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/L ND 30ND 1,1,1-Trichloroethane ug/L ND 30ND 1,1,2,2-Tetrachloroethane ug/L ND 30ND 1,1,2-Trichloroethane ug/L ND 30ND 1,1-Dichloroethane ug/L ND 30ND 1,1-Dichloroethene ug/L ND 30ND 1,1-Dichloropropene ug/L ND 30ND 1,2,3-Trichlorobenzene ug/L ND 30ND 1,2,3-Trichloropropane ug/L ND 30ND 1,2,4-Trichlorobenzene ug/L ND 30ND 1,2-Dibromo-3-chloropropane ug/L ND 30ND 1,2-Dibromoethane (EDB)ug/L ND 30ND 1,2-Dichlorobenzene ug/L ND 30ND 1,2-Dichloroethane ug/L ND 30ND 1,2-Dichloropropane ug/L ND 30ND 1,3-Dichlorobenzene ug/L ND 30ND 1,3-Dichloropropane ug/L ND 30ND 1,4-Dichlorobenzene ug/L ND 30ND 2,2-Dichloropropane ug/L ND 30ND 2-Butanone (MEK)ug/L ND 30ND 2-Chlorotoluene ug/L ND 30ND 2-Hexanone ug/L 0.56J 300.59J 4-Chlorotoluene ug/L ND 30ND 4-Methyl-2-pentanone (MIBK)ug/L ND 30ND Acetone ug/L 8.7J 308.3J REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 114 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92678743014 4090553SAMPLE DUPLICATE: Benzene ug/L ND 30ND Bromobenzene ug/L ND 30ND Bromochloromethane ug/L ND 30ND Bromodichloromethane ug/L ND 30ND Bromoform ug/L ND 30ND Bromomethane ug/L ND v230ND Carbon tetrachloride ug/L ND 30ND Chlorobenzene ug/L ND 30ND Chloroethane ug/L ND 30ND Chloroform ug/L ND 30ND Chloromethane ug/L ND 300.80J cis-1,2-Dichloroethene ug/L ND 30ND cis-1,3-Dichloropropene ug/L ND 30ND Dibromochloromethane ug/L ND 30ND Dibromomethane ug/L ND 30ND Dichlorodifluoromethane ug/L ND 30ND Diisopropyl ether ug/L ND 30ND Ethylbenzene ug/L ND 30ND Hexachloro-1,3-butadiene ug/L ND 30ND m&p-Xylene ug/L ND 30ND Methyl-tert-butyl ether ug/L ND 30ND Methylene Chloride ug/L ND 30ND Naphthalene ug/L ND 30ND o-Xylene ug/L ND 30ND p-Isopropyltoluene ug/L ND 30ND Styrene ug/L ND 30ND Tetrachloroethene ug/L ND 30ND Toluene ug/L ND 30ND trans-1,2-Dichloroethene ug/L ND 30ND trans-1,3-Dichloropropene ug/L ND 30ND Trichloroethene ug/L ND 30ND Trichlorofluoromethane ug/L ND 30ND Vinyl acetate ug/L ND 30ND Vinyl chloride ug/L ND 30ND Xylene (Total)ug/L ND 30ND 1,2-Dichloroethane-d4 (S)%103103 4-Bromofluorobenzene (S)%9998 Toluene-d8 (S)%99100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 115 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 788712 EPA 3510C EPA 8270E 8270E Water MSSV RVE Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples: 92678743011, 92678743012, 92678743013, 92678743016, 92678743017 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4088006 Associated Lab Samples:92678743011, 92678743012, 92678743013, 92678743016, 92678743017 Matrix: Water AnalyzedMDL 1,2,4-Trichlorobenzene ug/L ND 10.0 07/25/23 12:231.7 1,2-Dichlorobenzene ug/L ND 10.0 07/25/23 12:231.8 1,3-Dichlorobenzene ug/L ND 10.0 07/25/23 12:231.6 1,4-Dichlorobenzene ug/L ND 10.0 07/25/23 12:231.7 1-Methylnaphthalene ug/L ND 10.0 07/25/23 12:232.0 2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 07/25/23 12:231.2 2,4,5-Trichlorophenol ug/L ND 10.0 07/25/23 12:231.4 2,4,6-Trichlorophenol ug/L ND 10.0 07/25/23 12:231.6 2,4-Dichlorophenol ug/L ND 10.0 07/25/23 12:231.4 2,4-Dimethylphenol ug/L ND 10.0 07/25/23 12:231.7 2,4-Dinitrophenol ug/L ND 50.0 07/25/23 12:2326.0 2,4-Dinitrotoluene ug/L ND 10.0 07/25/23 12:231.6 2,6-Dinitrotoluene ug/L ND 10.0 07/25/23 12:231.7 2-Chloronaphthalene ug/L ND 10.0 07/25/23 12:231.7 2-Chlorophenol ug/L ND 10.0 07/25/23 12:231.2 2-Methylnaphthalene ug/L ND 10.0 07/25/23 12:231.9 2-Methylphenol(o-Cresol)ug/L ND 10.0 07/25/23 12:231.9 2-Nitroaniline ug/L ND 20.0 07/25/23 12:233.0 2-Nitrophenol ug/L ND 10.0 07/25/23 12:231.4 3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 07/25/23 12:231.2 3,3'-Dichlorobenzidine ug/L ND 20.0 07/25/23 12:238.1 3-Nitroaniline ug/L ND 20.0 07/25/23 12:233.8 4,6-Dinitro-2-methylphenol ug/L ND 20.0 07/25/23 12:237.8 4-Bromophenylphenyl ether ug/L ND 10.0 07/25/23 12:231.8 4-Chloro-3-methylphenol ug/L ND 10.0 07/25/23 12:233.3 4-Chloroaniline ug/L ND 20.0 07/25/23 12:233.6 4-Chlorophenylphenyl ether ug/L ND 10.0 07/25/23 12:232.0 4-Nitroaniline ug/L ND 20.0 07/25/23 12:235.1 4-Nitrophenol ug/L ND 50.0 07/25/23 12:236.6 Acenaphthene ug/L ND 10.0 07/25/23 12:232.0 Acenaphthylene ug/L ND 10.0 07/25/23 12:232.0 Aniline ug/L ND 10.0 07/25/23 12:231.6 Anthracene ug/L ND 10.0 07/25/23 12:232.3 Benzo(a)anthracene ug/L ND 10.0 07/25/23 12:232.7 Benzo(a)pyrene ug/L ND 10.0 07/25/23 12:232.8 Benzo(b)fluoranthene ug/L ND 10.0 07/25/23 12:232.6 Benzo(g,h,i)perylene ug/L ND 10.0 07/25/23 12:232.8 Benzo(k)fluoranthene ug/L ND 10.0 07/25/23 12:232.7 Benzoic Acid ug/L ND 50.0 07/25/23 12:2322.0 Benzyl alcohol ug/L ND 20.0 07/25/23 12:232.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 116 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4088006 Associated Lab Samples:92678743011, 92678743012, 92678743013, 92678743016, 92678743017 Matrix: Water AnalyzedMDL bis(2-Chloroethoxy)methane ug/L ND 10.0 07/25/23 12:231.8 bis(2-Chloroethyl) ether ug/L ND 10.0 07/25/23 12:231.9 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 07/25/23 12:233.7 Butylbenzylphthalate ug/L ND 10.0 07/25/23 12:233.1 Chrysene ug/L ND 10.0 07/25/23 12:232.8 Di-n-butylphthalate ug/L ND 10.0 07/25/23 12:232.2 Di-n-octylphthalate ug/L ND 10.0 07/25/23 12:233.9 Dibenz(a,h)anthracene ug/L ND 10.0 07/25/23 12:233.0 Dibenzofuran ug/L ND 10.0 07/25/23 12:232.1 Diethylphthalate ug/L ND 10.0 07/25/23 12:232.0 Dimethylphthalate ug/L ND 10.0 07/25/23 12:232.1 Fluoranthene ug/L ND 10.0 07/25/23 12:232.2 Fluorene ug/L ND 10.0 07/25/23 12:232.1 Hexachloro-1,3-butadiene ug/L ND 10.0 07/25/23 12:231.8 Hexachlorobenzene ug/L ND 10.0 07/25/23 12:232.2 Hexachlorocyclopentadiene ug/L ND 10.0 07/25/23 12:231.6 Hexachloroethane ug/L ND 10.0 07/25/23 12:231.4 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/25/23 12:232.9 Isophorone ug/L ND 10.0 07/25/23 12:231.7 N-Nitroso-di-n-propylamine ug/L ND 10.0 07/25/23 12:231.3 N-Nitrosodimethylamine ug/L ND 10.0 07/25/23 12:231.9 N-Nitrosodiphenylamine ug/L ND 10.0 07/25/23 12:233.0 Naphthalene ug/L ND 10.0 07/25/23 12:232.1 Nitrobenzene ug/L ND 10.0 07/25/23 12:231.9 Pentachlorophenol ug/L ND 20.0 07/25/23 12:233.8 Phenanthrene ug/L ND 10.0 07/25/23 12:232.0 Phenol ug/L ND 10.0 07/25/23 12:231.4 Pyrene ug/L ND 10.0 07/25/23 12:232.2 2,4,6-Tribromophenol (S)%117 10-164 07/25/23 12:23 2-Fluorobiphenyl (S)%80 10-130 07/25/23 12:23 2-Fluorophenol (S)%72 10-130 07/25/23 12:23 Nitrobenzene-d5 (S)%96 10-138 07/25/23 12:23 Phenol-d6 (S)%56 10-130 07/25/23 12:23 Terphenyl-d14 (S)%125 19-191 07/25/23 12:23 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4088007LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/L 37.450 75 11-130 1,2-Dichlorobenzene ug/L 32.950 66 10-130 1,3-Dichlorobenzene ug/L 30.950 62 10-130 1,4-Dichlorobenzene ug/L 31.850 64 10-130 1-Methylnaphthalene ug/L 46.150 92 23-130 2,2'-Oxybis(1-chloropropane)ug/L 43.850 88 21-135 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 117 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4088007LABORATORY CONTROL SAMPLE: LCSSpike 2,4,5-Trichlorophenol ug/L 55.450 111 38-147 2,4,6-Trichlorophenol ug/L 58.450 117 34-142 2,4-Dichlorophenol ug/L 50.150 100 36-136 2,4-Dimethylphenol ug/L 50.650 101 38-134 2,4-Dinitrophenol ug/L 273250 109 10-169 2,4-Dinitrotoluene ug/L 52.450 105 44-154 2,6-Dinitrotoluene ug/L 53.950 108 44-156 2-Chloronaphthalene ug/L 45.550 91 25-130 2-Chlorophenol ug/L 49.850 100 29-130 2-Methylnaphthalene ug/L 42.650 85 23-130 2-Methylphenol(o-Cresol)ug/L 44.550 89 31-130 2-Nitroaniline ug/L 91.2100 91 39-145 2-Nitrophenol ug/L 57.850 116 29-142 3&4-Methylphenol(m&p Cresol)ug/L 47.450 95 30-130 3,3'-Dichlorobenzidine ug/L 100100 100 44-158 3-Nitroaniline ug/L 105100 105 45-152 4,6-Dinitro-2-methylphenol ug/L 116100 116 39-158 4-Bromophenylphenyl ether ug/L 55.150 110 47-147 4-Chloro-3-methylphenol ug/L 98.3100 98 40-138 4-Chloroaniline ug/L 84.9100 85 35-130 4-Chlorophenylphenyl ether ug/L 49.950 100 36-139 4-Nitroaniline ug/L 88.5100 89 46-157 4-Nitrophenol ug/L 163250 65 17-130 Acenaphthene ug/L 47.450 95 34-135 Acenaphthylene ug/L 47.150 94 35-137 Aniline ug/L 31.350 63 25-130 Anthracene ug/L 48.150 96 47-146 Benzo(a)anthracene ug/L 53.050 106 48-160 Benzo(a)pyrene ug/L 53.050 106 47-165 Benzo(b)fluoranthene ug/L 61.550 123 49-171 Benzo(g,h,i)perylene ug/L 52.650 105 46-166 Benzo(k)fluoranthene ug/L 54.650 109 55-162 Benzoic Acid ug/L 147250 59 10-130 Benzyl alcohol ug/L 94.4100 94 29-132 bis(2-Chloroethoxy)methane ug/L 49.050 98 33-136 bis(2-Chloroethyl) ether ug/L 46.350 93 30-142 bis(2-Ethylhexyl)phthalate ug/L 53.350 107 46-173 Butylbenzylphthalate ug/L 59.050 118 53-169 Chrysene ug/L 51.950 104 54-152 Di-n-butylphthalate ug/L 48.850 98 49-161 Di-n-octylphthalate ug/L 51.150 102 50-166 Dibenz(a,h)anthracene ug/L 51.050 102 46-166 Dibenzofuran ug/L 46.650 93 37-136 Diethylphthalate ug/L 47.950 96 45-149 Dimethylphthalate ug/L 47.650 95 43-145 Fluoranthene ug/L 47.850 96 50-153 Fluorene ug/L 48.450 97 42-142 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 118 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4088007LABORATORY CONTROL SAMPLE: LCSSpike Hexachloro-1,3-butadiene ug/L 33.750 67 10-130 Hexachlorobenzene ug/L 54.050 108 44-138 Hexachlorocyclopentadiene ug/L 38.450 77 10-130 Hexachloroethane ug/L 29.850 60 10-130 Indeno(1,2,3-cd)pyrene ug/L 50.250 100 46-166 Isophorone ug/L 49.450 99 36-135 N-Nitroso-di-n-propylamine ug/L 50.650 101 33-140 N-Nitrosodimethylamine ug/L 38.150 76 24-130 N-Nitrosodiphenylamine ug/L 54.150 108 46-144 Naphthalene ug/L 42.550 85 20-130 Nitrobenzene ug/L 48.350 97 33-133 Pentachlorophenol ug/L 125100 125 21-163 Phenanthrene ug/L 51.650 103 47-146 Phenol ug/L 34.050 68 19-130 Pyrene ug/L 61.150 122 53-155 2,4,6-Tribromophenol (S)%150 10-164 2-Fluorobiphenyl (S)%107 10-130 2-Fluorophenol (S)%89 10-130 Nitrobenzene-d5 (S)%119 10-138 Phenol-d6 (S)%70 10-130 Terphenyl-d14 (S)%143 19-191 Parameter Units MS Result % Rec Limits Qual% RecConc. 4088008MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92674992004 4088009 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,2,4-Trichlorobenzene ug/L 83.3 76 10-13067 12 3083.3ND 63.4 56.2 1,2-Dichlorobenzene ug/L 83.3 70 10-13062 11 3083.3ND 58.1 51.8 1,3-Dichlorobenzene ug/L 83.3 68 10-13060 11 3083.3ND 56.4 50.3 1,4-Dichlorobenzene ug/L 83.3 68 10-13060 13 3083.3ND 56.7 49.7 1-Methylnaphthalene ug/L 83.3 87 10-13178 11 3083.3ND 72.3 65.1 2,2'-Oxybis(1-chloropropane)ug/L 83.3 84 11-14377 8 3083.3ND 69.7 64.5 2,4,5-Trichlorophenol ug/L 83.3 103 10-17093 10 3083.3ND 85.8 77.3 2,4,6-Trichlorophenol ug/L 83.3 113 10-166100 12 3083.3ND 93.9 83.3 2,4-Dichlorophenol ug/L 83.3 95 10-15385 11 3083.3ND 79.3 71.0 2,4-Dimethylphenol ug/L 83.3 94 20-14784 12 3083.3ND 78.5 69.6 2,4-Dinitrophenol ug/L 417 100 10-17289 12 30417ND418 369 2,4-Dinitrotoluene ug/L 83.3 93 30-16484 11 3083.3ND 77.8 69.8 2,6-Dinitrotoluene ug/L 83.3 100 31-16392 9 3083.3ND 83.5 76.5 2-Chloronaphthalene ug/L 83.3 88 15-13480 9 3083.3ND 73.2 66.7 2-Chlorophenol ug/L 83.3 93 10-13985 9 3083.3ND 77.2 70.6 2-Methylnaphthalene ug/L 83.3 83 12-13075 11 3083.3ND 69.3 62.1 2-Methylphenol(o-Cresol) ug/L 83.3 86 19-13279 8 3083.3ND 71.4 65.6 2-Nitroaniline ug/L 167 82 23-15476 7 30167ND136 127 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 119 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 4088008MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92674992004 4088009 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 2-Nitrophenol ug/L 83.3 110 10-15998 11 3083.3ND 91.3 82.1 3&4-Methylphenol(m&p Cresol)ug/L 83.3 90 13-13684 7 3083.3ND 74.8 69.9 3,3'-Dichlorobenzidine ug/L 167 85 10-17881 5 30167ND141 135 3-Nitroaniline ug/L 167 97 20-16689 9 30167ND162 148 4,6-Dinitro-2-methylphenol ug/L 167 106 10-18797 9 30167ND177 162 4-Bromophenylphenyl ether ug/L 83.3 98 31-15792 6 3083.3ND 81.6 76.6 4-Chloro-3-methylphenol ug/L 167 88 27-14679 11 30167ND147 132 4-Chloroaniline ug/L 167 78 13-14370 11 30167ND131 117 4-Chlorophenylphenyl ether ug/L 83.3 92 23-14982 11 3083.3ND 76.3 68.3 4-Nitroaniline ug/L 167 80 24-17171 12 30167ND134 119 4-Nitrophenol ug/L 417 59 10-13054 9 30417ND245 224 Acenaphthene ug/L 83.3 90 21-14782 9 3083.3ND 75.0 68.2 Acenaphthylene ug/L 83.3 90 19-15083 8 3083.3ND 74.9 69.2 Aniline ug/L 83.3 52 10-13059 12 3083.3ND 43.7 49.4 Anthracene ug/L 83.3 85 36-15281 5 3083.3ND 70.8 67.3 Benzo(a)anthracene ug/L 83.3 102 42-16392 10 3083.3ND 84.9 76.4 Benzo(a)pyrene ug/L 83.3 97 40-16993 5 3083.3ND 81.1 77.3 Benzo(b)fluoranthene ug/L 83.3 113 40-177101 11 3083.3ND 93.9 84.0 Benzo(g,h,i)perylene ug/L 83.3 99 38-17498 1 3083.3ND 82.3 81.3 Benzo(k)fluoranthene ug/L 83.3 97 41-17191 7 3083.3ND 81.2 75.5 Benzoic Acid ug/L 417 62 10-13054 14 30417ND257 223 Benzyl alcohol ug/L 167 90 18-14184 7 30167ND150 140 bis(2-Chloroethoxy)methane ug/L 83.3 88 19-14682 8 3083.3ND 73.5 68.1 bis(2-Chloroethyl) ether ug/L 83.3 87 19-15180 8 3083.3ND 72.8 66.9 bis(2-Ethylhexyl)phthalate ug/L 83.3 103 42-16893 9 3083.3ND 85.4 77.9 Butylbenzylphthalate ug/L 83.3 113 42-177101 12 3083.3ND 94.6 84.0 Chrysene ug/L 83.3 96 43-15988 8 3083.3ND 79.6 73.4 Di-n-butylphthalate ug/L 83.3 90 42-16081 10 3083.3ND 74.7 67.4 Di-n-octylphthalate ug/L 83.3 97 42-17190 8 3083.3ND 81.1 74.9 Dibenz(a,h)anthracene ug/L 83.3 96 40-17193 3 3083.3ND 80.4 77.7 Dibenzofuran ug/L 83.3 88 23-14779 11 3083.3ND 73.5 65.7 Diethylphthalate ug/L 83.3 86 33-15778 10 3083.3ND 71.5 64.7 Dimethylphthalate ug/L 83.3 87 27-15478 10 3083.3ND 72.5 65.3 Fluoranthene ug/L 83.3 85 42-15777 10 3083.3ND 71.0 64.3 Fluorene ug/L 83.3 90 25-15583 8 3083.3ND 75.4 69.3 Hexachloro-1,3-butadiene ug/L 83.3 73 10-13061 18 3083.3ND 60.6 50.7 Hexachlorobenzene ug/L 83.3 99 32-14592 8 3083.3ND 82.6 76.5 Hexachlorocyclopentadiene ug/L 83.3 80 10-13070 13 3083.3ND 66.5 58.2 Hexachloroethane ug/L 83.3 66 10-13058 13 3083.3ND 54.9 48.1 Indeno(1,2,3-cd)pyrene ug/L 83.3 94 39-17493 2 3083.3ND 78.7 77.4 Isophorone ug/L 83.3 91 19-14681 11 3083.3ND 75.5 67.6 N-Nitroso-di-n-propylamine ug/L 83.3 96 20-15088 9 3083.3ND 79.7 73.2 N-Nitrosodimethylamine ug/L 83.3 70 13-13066 6 3083.3ND 58.3 55.0 N-Nitrosodiphenylamine ug/L 83.3 94 33-14990 5 3083.3ND 78.5 74.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 120 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 4088008MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92674992004 4088009 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Naphthalene ug/L 83.3 81 10-12873 11 3083.3ND 67.9 60.9 Nitrobenzene ug/L 83.3 89 19-14581 10 3083.3ND 74.3 67.4 Pentachlorophenol ug/L 167 112 10-188104 8 30167ND187 173 Phenanthrene ug/L 83.3 93 38-15086 7 3083.3ND 77.1 72.0 Phenol ug/L 83.3 63 10-13060 5 3083.3ND 52.6 49.8 Pyrene ug/L 83.3 112 42-163105 7 3083.3ND 93.6 87.1 2,4,6-Tribromophenol (S) %134 10-164123 2-Fluorobiphenyl (S)%104 10-13094 2-Fluorophenol (S)%78 10-13074 Nitrobenzene-d5 (S)%106 10-13896 Phenol-d6 (S)%65 10-13061 Terphenyl-d14 (S)%129 19-191119 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 121 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 789319 EPA 3510C EPA 8270E 8270E Water MSSV RVE Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples: 92678743014, 92678743015 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4091036 Associated Lab Samples:92678743014, 92678743015 Matrix: Water AnalyzedMDL 1,2,4-Trichlorobenzene ug/L ND 10.0 07/27/23 19:521.7 1,2-Dichlorobenzene ug/L ND 10.0 07/27/23 19:521.8 1,3-Dichlorobenzene ug/L ND 10.0 07/27/23 19:521.6 1,4-Dichlorobenzene ug/L ND 10.0 07/27/23 19:521.7 1-Methylnaphthalene ug/L ND 10.0 07/27/23 19:522.0 2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 07/27/23 19:521.2 2,4,5-Trichlorophenol ug/L ND 10.0 07/27/23 19:521.4 2,4,6-Trichlorophenol ug/L ND 10.0 07/27/23 19:521.6 2,4-Dichlorophenol ug/L ND 10.0 07/27/23 19:521.4 2,4-Dimethylphenol ug/L ND 10.0 07/27/23 19:521.7 2,4-Dinitrophenol ug/L ND 50.0 07/27/23 19:5226.0 2,4-Dinitrotoluene ug/L ND 10.0 07/27/23 19:521.6 2,6-Dinitrotoluene ug/L ND 10.0 07/27/23 19:521.7 2-Chloronaphthalene ug/L ND 10.0 07/27/23 19:521.7 2-Chlorophenol ug/L ND 10.0 07/27/23 19:521.2 2-Methylnaphthalene ug/L ND 10.0 07/27/23 19:521.9 2-Methylphenol(o-Cresol)ug/L ND 10.0 07/27/23 19:521.9 2-Nitroaniline ug/L ND 20.0 07/27/23 19:523.0 2-Nitrophenol ug/L ND 10.0 07/27/23 19:521.4 3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 07/27/23 19:521.2 3,3'-Dichlorobenzidine ug/L ND 20.0 07/27/23 19:528.1 3-Nitroaniline ug/L ND 20.0 07/27/23 19:523.8 4,6-Dinitro-2-methylphenol ug/L ND 20.0 07/27/23 19:527.8 4-Bromophenylphenyl ether ug/L ND 10.0 07/27/23 19:521.8 4-Chloro-3-methylphenol ug/L ND 10.0 07/27/23 19:523.3 4-Chloroaniline ug/L ND 20.0 07/27/23 19:523.6 4-Chlorophenylphenyl ether ug/L ND 10.0 07/27/23 19:522.0 4-Nitroaniline ug/L ND 20.0 07/27/23 19:525.1 4-Nitrophenol ug/L ND 50.0 07/27/23 19:526.6 Acenaphthene ug/L ND 10.0 07/27/23 19:522.0 Acenaphthylene ug/L ND 10.0 07/27/23 19:522.0 Aniline ug/L ND 10.0 07/27/23 19:521.6 Anthracene ug/L ND 10.0 07/27/23 19:522.3 Benzo(a)anthracene ug/L ND 10.0 07/27/23 19:522.7 Benzo(a)pyrene ug/L ND 10.0 07/27/23 19:522.8 Benzo(b)fluoranthene ug/L ND 10.0 07/27/23 19:522.6 Benzo(g,h,i)perylene ug/L ND 10.0 07/27/23 19:522.8 Benzo(k)fluoranthene ug/L ND 10.0 07/27/23 19:522.7 Benzoic Acid ug/L ND 50.0 07/27/23 19:5222.0 Benzyl alcohol ug/L ND 20.0 07/27/23 19:522.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 122 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4091036 Associated Lab Samples:92678743014, 92678743015 Matrix: Water AnalyzedMDL bis(2-Chloroethoxy)methane ug/L ND 10.0 07/27/23 19:521.8 bis(2-Chloroethyl) ether ug/L ND 10.0 07/27/23 19:521.9 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 07/27/23 19:523.7 Butylbenzylphthalate ug/L ND 10.0 07/27/23 19:523.1 Chrysene ug/L ND 10.0 07/27/23 19:522.8 Di-n-butylphthalate ug/L ND 10.0 07/27/23 19:522.2 Di-n-octylphthalate ug/L ND 10.0 07/27/23 19:523.9 Dibenz(a,h)anthracene ug/L ND 10.0 07/27/23 19:523.0 Dibenzofuran ug/L ND 10.0 07/27/23 19:522.1 Diethylphthalate ug/L ND 10.0 07/27/23 19:522.0 Dimethylphthalate ug/L ND 10.0 07/27/23 19:522.1 Fluoranthene ug/L ND 10.0 07/27/23 19:522.2 Fluorene ug/L ND 10.0 07/27/23 19:522.1 Hexachloro-1,3-butadiene ug/L ND 10.0 07/27/23 19:521.8 Hexachlorobenzene ug/L ND 10.0 07/27/23 19:522.2 Hexachlorocyclopentadiene ug/L ND 10.0 07/27/23 19:521.6 Hexachloroethane ug/L ND 10.0 07/27/23 19:521.4 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/27/23 19:522.9 Isophorone ug/L ND 10.0 07/27/23 19:521.7 N-Nitroso-di-n-propylamine ug/L ND 10.0 07/27/23 19:521.3 N-Nitrosodimethylamine ug/L ND 10.0 07/27/23 19:521.9 N-Nitrosodiphenylamine ug/L ND 10.0 07/27/23 19:523.0 Naphthalene ug/L ND 10.0 07/27/23 19:522.1 Nitrobenzene ug/L ND 10.0 07/27/23 19:521.9 Pentachlorophenol ug/L ND 20.0 07/27/23 19:523.8 Phenanthrene ug/L ND 10.0 07/27/23 19:522.0 Phenol ug/L ND 10.0 07/27/23 19:521.4 Pyrene ug/L ND 10.0 07/27/23 19:522.2 2,4,6-Tribromophenol (S)%140 10-164 07/27/23 19:52 2-Fluorobiphenyl (S)%107 10-130 07/27/23 19:52 2-Fluorophenol (S)%79 10-130 07/27/23 19:52 Nitrobenzene-d5 (S)%112 10-138 07/27/23 19:52 Phenol-d6 (S)%62 10-130 07/27/23 19:52 Terphenyl-d14 (S)%134 19-191 07/27/23 19:52 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4091037LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/L 32.750 65 11-130 1,2-Dichlorobenzene ug/L 28.950 58 10-130 1,3-Dichlorobenzene ug/L 27.850 56 10-130 1,4-Dichlorobenzene ug/L 28.950 58 10-130 1-Methylnaphthalene ug/L 37.950 76 23-130 2,2'-Oxybis(1-chloropropane)ug/L 37.150 74 21-135 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 123 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4091037LABORATORY CONTROL SAMPLE: LCSSpike 2,4,5-Trichlorophenol ug/L 51.050 102 38-147 2,4,6-Trichlorophenol ug/L 51.950 104 34-142 2,4-Dichlorophenol ug/L 42.550 85 36-136 2,4-Dimethylphenol ug/L 42.850 86 38-134 2,4-Dinitrophenol ug/L 245250 98 10-169 2,4-Dinitrotoluene ug/L 49.850 100 44-154 2,6-Dinitrotoluene ug/L 50.150 100 44-156 2-Chloronaphthalene ug/L 39.050 78 25-130 2-Chlorophenol ug/L 42.750 85 29-130 2-Methylnaphthalene ug/L 36.750 73 23-130 2-Methylphenol(o-Cresol)ug/L 37.350 75 31-130 2-Nitroaniline ug/L 84.6100 85 39-145 2-Nitrophenol ug/L 50.050 100 29-142 3&4-Methylphenol(m&p Cresol)ug/L 40.050 80 30-130 3,3'-Dichlorobenzidine ug/L 92.3100 92 44-158 3-Nitroaniline ug/L 96.0100 96 45-152 4,6-Dinitro-2-methylphenol ug/L 104100 104 39-158 4-Bromophenylphenyl ether ug/L 47.750 95 47-147 4-Chloro-3-methylphenol ug/L 84.2100 84 40-138 4-Chloroaniline ug/L 67.9100 68 35-130 4-Chlorophenylphenyl ether ug/L 45.550 91 36-139 4-Nitroaniline ug/L 86.4100 86 46-157 4-Nitrophenol ug/L 153250 61 17-130 Acenaphthene ug/L 40.550 81 34-135 Acenaphthylene ug/L 40.450 81 35-137 Aniline ug/L 27.350 55 25-130 Anthracene ug/L 43.050 86 47-146 Benzo(a)anthracene ug/L 48.750 97 48-160 Benzo(a)pyrene ug/L 46.950 94 47-165 Benzo(b)fluoranthene ug/L 54.350 109 49-171 Benzo(g,h,i)perylene ug/L 53.350 107 46-166 Benzo(k)fluoranthene ug/L 47.450 95 55-162 Benzoic Acid ug/L 123250 49 10-130 Benzyl alcohol ug/L 78.1100 78 29-132 bis(2-Chloroethoxy)methane ug/L 41.050 82 33-136 bis(2-Chloroethyl) ether ug/L 39.250 78 30-142 bis(2-Ethylhexyl)phthalate ug/L 47.750 95 46-173 Butylbenzylphthalate ug/L 53.950 108 53-169 Chrysene ug/L 46.050 92 54-152 Di-n-butylphthalate ug/L 44.750 89 49-161 Di-n-octylphthalate ug/L 49.650 99 50-166 Dibenz(a,h)anthracene ug/L 51.350 103 46-166 Dibenzofuran ug/L 41.450 83 37-136 Diethylphthalate ug/L 44.050 88 45-149 Dimethylphthalate ug/L 44.150 88 43-145 Fluoranthene ug/L 46.150 92 50-153 Fluorene ug/L 43.150 86 42-142 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 124 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4091037LABORATORY CONTROL SAMPLE: LCSSpike Hexachloro-1,3-butadiene ug/L 29.250 58 10-130 Hexachlorobenzene ug/L 47.150 94 44-138 Hexachlorocyclopentadiene ug/L 32.150 64 10-130 Hexachloroethane ug/L 26.950 54 10-130 Indeno(1,2,3-cd)pyrene ug/L 49.350 99 46-166 Isophorone ug/L 41.150 82 36-135 N-Nitroso-di-n-propylamine ug/L 42.550 85 33-140 N-Nitrosodimethylamine ug/L 32.350 65 24-130 N-Nitrosodiphenylamine ug/L 45.550 91 46-144 Naphthalene ug/L 36.150 72 20-130 Nitrobenzene ug/L 41.450 83 33-133 Pentachlorophenol ug/L 108100 108 21-163 Phenanthrene ug/L 46.150 92 47-146 Phenol ug/L 28.650 57 19-130 Pyrene ug/L 52.150 104 53-155 2,4,6-Tribromophenol (S)%126 10-164 2-Fluorobiphenyl (S)%88 10-130 2-Fluorophenol (S)%68 10-130 Nitrobenzene-d5 (S)%92 10-138 Phenol-d6 (S)%54 10-130 Terphenyl-d14 (S)%110 19-191 Parameter Units MS Result % Rec Limits Qual% RecConc. 4091038MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92674992005 4091039 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,2,4-Trichlorobenzene ug/L 83.3 47 10-13048 2 3083.3ND 39.0 39.8 1,2-Dichlorobenzene ug/L 83.3 45 10-13045 1 3083.3ND 37.6 37.2 1,3-Dichlorobenzene ug/L 83.3 43 10-13044 1 3083.3ND 36.2 36.4 1,4-Dichlorobenzene ug/L 83.3 45 10-13045 1 3083.3ND 37.2 37.5 1-Methylnaphthalene ug/L 83.3 57 10-13157 1 3083.3ND 47.6 47.8 2,2'-Oxybis(1-chloropropane)ug/L 83.3 45 11-14346 2 3083.3ND 37.9 38.6 2,4,5-Trichlorophenol ug/L 83.3 113 10-170107 6 3083.3ND 94.0 88.9 2,4,6-Trichlorophenol ug/L 83.3 96 10-16693 2 3083.3ND 79.6 77.7 2,4-Dichlorophenol ug/L 83.3 69 10-15367 2 3083.3ND 57.2 56.0 2,4-Dimethylphenol ug/L 83.3 66 20-14764 2 3083.3ND 54.9 53.6 2,4-Dinitrophenol ug/L 417 67 10-17255 19 30417ND278 229 2,4-Dinitrotoluene ug/L 83.3 97 30-16494 3 3083.3ND 80.9 78.6 2,6-Dinitrotoluene ug/L 83.3 88 31-16390 2 3083.3ND 73.4 75.1 2-Chloronaphthalene ug/L 83.3 57 15-13453 8 3083.3ND 47.5 43.9 2-Chlorophenol ug/L 83.3 53 10-13955 3 3083.3ND 44.4 45.9 2-Methylnaphthalene ug/L 83.3 54 12-13054 1 3083.3ND 44.8 45.4 2-Methylphenol(o-Cresol) ug/L 83.3 56 19-13255 1 3083.3ND 46.6 46.2 2-Nitroaniline ug/L 167 84 23-15481 3 30167ND140 136 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 125 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 4091038MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92674992005 4091039 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 2-Nitrophenol ug/L 83.3 57 10-15960 6 3083.3ND 47.1 50.1 3&4-Methylphenol(m&p Cresol)ug/L 83.3 58 13-13656 4 3083.3ND 48.6 46.7 3,3'-Dichlorobenzidine ug/L 167 55 10-17854 2 30167ND91.2 89.6 3-Nitroaniline ug/L 167 98 20-16694 4 30167ND164 157 4,6-Dinitro-2-methylphenol ug/L 167 102 10-18793 9 30167ND169 155 4-Bromophenylphenyl ether ug/L 83.3 95 31-15790 6 3083.3ND 79.4 75.1 4-Chloro-3-methylphenol ug/L 167 94 27-14694 0 30167ND157 157 4-Chloroaniline ug/L 167 49 13-14348 3 30167ND81.5 79.3 4-Chlorophenylphenyl ether ug/L 83.3 78 23-14981 3 3083.3ND 65.3 67.3 4-Nitroaniline ug/L 167 87 24-17181 7 30167ND144 135 4-Nitrophenol ug/L 417 59 10-13052 12 30417ND247 218 Acenaphthene ug/L 83.3 66 21-14764 2 3083.3ND 54.8 53.5 Acenaphthylene ug/L 83.3 66 19-15063 4 3083.3ND 54.6 52.5 Aniline ug/L 83.3 37 10-13038 2 3083.3ND 30.6 31.4 Anthracene ug/L 83.3 94 36-15289 5 3083.3ND 77.9 74.4 Benzo(a)anthracene ug/L 83.3 114 42-163101 12 3083.3ND 94.8 84.1 Benzo(a)pyrene ug/L 83.3 114 40-169103 10 3083.3ND 95.3 86.2 Benzo(b)fluoranthene ug/L 83.3 123 40-177110 11 3083.3ND 102 91.8 Benzo(g,h,i)perylene ug/L 83.3 122 38-174111 9 3083.3ND 101 92.8 Benzo(k)fluoranthene ug/L 83.3 113 41-171100 12 3083.3ND 94.5 83.6 Benzoic Acid ug/L M1417610-1305 30417ND36.8J ND Benzyl alcohol ug/L 167 56 18-14156 0 30167ND92.7 93.0 bis(2-Chloroethoxy)methane ug/L 83.3 49 19-14651 3 3083.3ND 40.9 42.2 bis(2-Chloroethyl) ether ug/L 83.3 48 19-15150 4 3083.3ND 39.7 41.4 bis(2-Ethylhexyl)phthalate ug/L 83.3 121 42-168108 11 3083.3ND 103 92.0 Butylbenzylphthalate ug/L 83.3 125 42-177111 12 3083.3ND 105 92.5 Chrysene ug/L 83.3 109 43-15999 10 3083.3ND 90.9 82.4 Di-n-butylphthalate ug/L 83.3 107 42-16095 12 3083.3ND 89.5 79.3 Di-n-octylphthalate ug/L 83.3 122 42-171110 11 3083.3ND 102 91.4 Dibenz(a,h)anthracene ug/L 83.3 118 40-171109 8 3083.3ND 98.2 91.1 Dibenzofuran ug/L 83.3 70 23-14769 2 3083.3ND 58.7 57.6 Diethylphthalate ug/L 83.3 90 33-15787 3 3083.3ND 75.3 72.7 Dimethylphthalate ug/L 83.3 77 27-15478 1 3083.3ND 64.3 64.9 Fluoranthene ug/L 83.3 104 42-15793 11 3083.3ND 86.6 77.9 Fluorene ug/L 83.3 79 25-15579 0 3083.3ND 65.9 65.7 Hexachloro-1,3-butadiene ug/L 83.3 45 10-13047 4 3083.3ND 37.4 38.9 Hexachlorobenzene ug/L 83.3 93 32-14593 0 3083.3ND 77.3 77.7 Hexachlorocyclopentadiene ug/L 83.3 36 10-13034 3 3083.3ND 29.6 28.7 Hexachloroethane ug/L 83.3 41 10-13041 1 3083.3ND 34.3 34.0 Indeno(1,2,3-cd)pyrene ug/L 83.3 113 39-174106 7 3083.3ND 94.4 88.3 Isophorone ug/L 83.3 50 19-14652 5 3083.3ND 41.7 43.7 N-Nitroso-di-n-propylamine ug/L 83.3 53 20-15054 3 3083.3ND 44.1 45.2 N-Nitrosodimethylamine ug/L 83.3 38 13-13040 4 3083.3ND 32.0 33.4 N-Nitrosodiphenylamine ug/L 83.3 104 33-14997 7 3083.3ND 86.6 80.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 126 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 4091038MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92674992005 4091039 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Naphthalene ug/L 83.3 51 10-12850 1 3083.3ND 42.1 41.8 Nitrobenzene ug/L 83.3 49 19-14550 0 3083.3ND 41.2 41.4 Pentachlorophenol ug/L v116712510-188113 10 30167ND208 188 Phenanthrene ug/L 83.3 101 38-15096 5 3083.3ND 84.1 79.7 Phenol ug/L 83.3 40 10-13040 1 3083.3ND 33.4 33.2 Pyrene ug/L 83.3 125 42-163110 13 3083.3ND 104 91.5 2,4,6-Tribromophenol (S) %139 10-164139 2-Fluorobiphenyl (S)%62 10-13062 2-Fluorophenol (S)%40 10-13044 Nitrobenzene-d5 (S)%54 10-13857 Phenol-d6 (S)%38 10-13039 Terphenyl-d14 (S)%125 19-191116 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 127 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 789567 EPA 3546 EPA 8270E 8270E Solid MSSV Microwave Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010, 92678743018 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4092374 Associated Lab Samples: 92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010, 92678743018 Matrix: Solid AnalyzedMDL 1,2,4-Trichlorobenzene ug/kg ND 330 07/30/23 09:53130 1,2-Dichlorobenzene ug/kg ND 330 07/30/23 09:53119 1,3-Dichlorobenzene ug/kg ND 330 07/30/23 09:53117 1,4-Dichlorobenzene ug/kg ND 330 07/30/23 09:53126 1-Methylnaphthalene ug/kg ND 330 07/30/23 09:53116 2,2'-Oxybis(1-chloropropane)ug/kg ND 330 07/30/23 09:53157 2,4,5-Trichlorophenol ug/kg ND 330 07/30/23 09:53151 2,4,6-Trichlorophenol ug/kg ND 330 07/30/23 09:53136 2,4-Dichlorophenol ug/kg ND 330 07/30/23 09:53129 2,4-Dimethylphenol ug/kg ND 330 v107/30/23 09:53137 2,4-Dinitrophenol ug/kg ND 1650 v107/30/23 09:531020 2,4-Dinitrotoluene ug/kg ND 330 07/30/23 09:53127 2,6-Dinitrotoluene ug/kg ND 330 07/30/23 09:53121 2-Chloronaphthalene ug/kg ND 330 07/30/23 09:53131 2-Chlorophenol ug/kg ND 330 07/30/23 09:53124 2-Methylnaphthalene ug/kg ND 330 07/30/23 09:53132 2-Methylphenol(o-Cresol)ug/kg ND 330 07/30/23 09:53135 2-Nitroaniline ug/kg ND 1650 07/30/23 09:53270 2-Nitrophenol ug/kg ND 330 07/30/23 09:53143 3&4-Methylphenol(m&p Cresol)ug/kg ND 330 07/30/23 09:53133 3,3'-Dichlorobenzidine ug/kg ND 660 07/30/23 09:53223 3-Nitroaniline ug/kg ND 1650 07/30/23 09:53259 4,6-Dinitro-2-methylphenol ug/kg ND 660 07/30/23 09:53308 4-Bromophenylphenyl ether ug/kg ND 330 07/30/23 09:53127 4-Chloro-3-methylphenol ug/kg ND 660 07/30/23 09:53232 4-Chloroaniline ug/kg ND 660 07/30/23 09:53259 4-Chlorophenylphenyl ether ug/kg ND 330 07/30/23 09:53123 4-Nitroaniline ug/kg ND 660 07/30/23 09:53251 4-Nitrophenol ug/kg ND 1650 07/30/23 09:53638 Acenaphthene ug/kg ND 330 07/30/23 09:53116 Acenaphthylene ug/kg ND 330 07/30/23 09:53116 Aniline ug/kg ND 330 07/30/23 09:53129 Anthracene ug/kg ND 330 07/30/23 09:53108 Benzo(a)anthracene ug/kg ND 330 07/30/23 09:53110 Benzo(a)pyrene ug/kg ND 330 07/30/23 09:53114 Benzo(b)fluoranthene ug/kg ND 330 07/30/23 09:53110 Benzo(g,h,i)perylene ug/kg ND 330 07/30/23 09:53128 Benzo(k)fluoranthene ug/kg ND 330 07/30/23 09:53116 Benzoic Acid ug/kg ND 1650 07/30/23 09:53709 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 128 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4092374 Associated Lab Samples: 92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010, 92678743018 Matrix: Solid AnalyzedMDL Benzyl alcohol ug/kg ND 660 07/30/23 09:53250 bis(2-Chloroethoxy)methane ug/kg ND 330 07/30/23 09:53137 bis(2-Chloroethyl) ether ug/kg ND 330 07/30/23 09:53124 bis(2-Ethylhexyl)phthalate ug/kg ND 330 07/30/23 09:53128 Butylbenzylphthalate ug/kg ND 330 07/30/23 09:53139 Chrysene ug/kg ND 330 07/30/23 09:53120 Di-n-butylphthalate ug/kg ND 330 07/30/23 09:53111 Di-n-octylphthalate ug/kg ND 330 07/30/23 09:53130 Dibenz(a,h)anthracene ug/kg ND 330 07/30/23 09:53127 Dibenzofuran ug/kg ND 330 07/30/23 09:53119 Diethylphthalate ug/kg ND 330 07/30/23 09:53121 Dimethylphthalate ug/kg ND 330 07/30/23 09:53120 Fluoranthene ug/kg ND 330 07/30/23 09:53113 Fluorene ug/kg ND 330 07/30/23 09:53116 Hexachloro-1,3-butadiene ug/kg ND 330 07/30/23 09:53143 Hexachlorobenzene ug/kg ND 330 07/30/23 09:53129 Hexachlorocyclopentadiene ug/kg ND 330 07/30/23 09:53189 Hexachloroethane ug/kg ND 330 07/30/23 09:53126 Indeno(1,2,3-cd)pyrene ug/kg ND 330 07/30/23 09:53130 Isophorone ug/kg ND 330 07/30/23 09:53147 N-Nitroso-di-n-propylamine ug/kg ND 330 07/30/23 09:53124 N-Nitrosodimethylamine ug/kg ND 330 07/30/23 09:53111 N-Nitrosodiphenylamine ug/kg ND 330 07/30/23 09:53117 Naphthalene ug/kg ND 330 07/30/23 09:53112 Nitrobenzene ug/kg ND 330 07/30/23 09:53153 Pentachlorophenol ug/kg ND 660 07/30/23 09:53323 Phenanthrene ug/kg ND 330 07/30/23 09:53108 Phenol ug/kg ND 330 07/30/23 09:53147 Pyrene ug/kg ND 330 07/30/23 09:53134 Pyridine ug/kg ND 330 07/30/23 09:53104 2,4,6-Tribromophenol (S)%59 10-131 07/30/23 09:53 2-Fluorobiphenyl (S)%48 10-130 07/30/23 09:53 2-Fluorophenol (S)%50 10-130 07/30/23 09:53 Nitrobenzene-d5 (S)%56 10-130 07/30/23 09:53 Phenol-d6 (S)%49 10-130 07/30/23 09:53 Terphenyl-d14 (S)%59 10-130 07/30/23 09:53 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4092375LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/kg 8381640 51 43-130 1,2-Dichlorobenzene ug/kg 7551640 46 43-130 1,3-Dichlorobenzene ug/kg 7601640 46 43-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 129 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4092375LABORATORY CONTROL SAMPLE: LCSSpike 1,4-Dichlorobenzene ug/kg 7751640 47 44-130 1-Methylnaphthalene ug/kg 10201640 62 47-130 2,2'-Oxybis(1-chloropropane)ug/kg 7871640 48 29-130 2,4,5-Trichlorophenol ug/kg 10601640 64 47-130 2,4,6-Trichlorophenol ug/kg 10101640 62 47-130 2,4-Dichlorophenol ug/kg 10001640 61 45-130 2,4-Dimethylphenol ug/kg 1390 v1164085 45-130 2,4-Dinitrophenol ug/kg 6250 v1820076 27-140 2,4-Dinitrotoluene ug/kg 12601640 77 46-130 2,6-Dinitrotoluene ug/kg 11701640 71 48-130 2-Chloronaphthalene ug/kg 8731640 53 46-130 2-Chlorophenol ug/kg 8661640 53 43-130 2-Methylnaphthalene ug/kg 9631640 59 47-130 2-Methylphenol(o-Cresol)ug/kg 9061640 55 42-130 2-Nitroaniline ug/kg 21603280 66 41-130 2-Nitrophenol ug/kg 9691640 59 48-130 3&4-Methylphenol(m&p Cresol)ug/kg 9421640 57 39-130 3,3'-Dichlorobenzidine ug/kg 20903280 64 41-130 3-Nitroaniline ug/kg 21303280 65 37-130 4,6-Dinitro-2-methylphenol ug/kg 23003280 70 38-141 4-Bromophenylphenyl ether ug/kg 10201640 62 47-130 4-Chloro-3-methylphenol ug/kg 23703280 72 44-130 4-Chloroaniline ug/kg 17903280 55 41-130 4-Chlorophenylphenyl ether ug/kg 10501640 64 45-130 4-Nitroaniline ug/kg 21903280 67 42-130 4-Nitrophenol ug/kg 59908200 73 39-131 Acenaphthene ug/kg 10501640 64 49-130 Acenaphthylene ug/kg 10501640 64 50-130 Aniline ug/kg 6541640 40 38-130 Anthracene ug/kg 10301640 63 49-130 Benzo(a)anthracene ug/kg 10901640 66 51-130 Benzo(a)pyrene ug/kg 11201640 69 51-130 Benzo(b)fluoranthene ug/kg 11001640 67 49-130 Benzo(g,h,i)perylene ug/kg 11501640 70 48-140 Benzo(k)fluoranthene ug/kg 11401640 69 51-130 Benzoic Acid ug/kg 35408200 43 22-130 Benzyl alcohol ug/kg 17403280 53 43-130 bis(2-Chloroethoxy)methane ug/kg 8601640 52 43-130 bis(2-Chloroethyl) ether ug/kg 7911640 48 42-130 bis(2-Ethylhexyl)phthalate ug/kg 11301640 69 43-130 Butylbenzylphthalate ug/kg 10201640 62 44-131 Chrysene ug/kg 11601640 71 51-130 Di-n-butylphthalate ug/kg 10801640 66 46-130 Di-n-octylphthalate ug/kg 11001640 67 45-130 Dibenz(a,h)anthracene ug/kg 11801640 72 48-130 Dibenzofuran ug/kg 10501640 64 10-130 Diethylphthalate ug/kg 11701640 71 48-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 130 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4092375LABORATORY CONTROL SAMPLE: LCSSpike Dimethylphthalate ug/kg 11901640 72 48-130 Fluoranthene ug/kg 11701640 72 48-130 Fluorene ug/kg 10701640 65 48-130 Hexachloro-1,3-butadiene ug/kg 8631640 53 39-130 Hexachlorobenzene ug/kg 11001640 67 47-130 Hexachlorocyclopentadiene ug/kg 5821640 36 17-130 Hexachloroethane ug/kg 7401640 45 40-130 Indeno(1,2,3-cd)pyrene ug/kg 12001640 73 50-130 Isophorone ug/kg 10301640 63 41-130 N-Nitroso-di-n-propylamine ug/kg 9421640 57 36-130 N-Nitrosodimethylamine ug/kg 7141640 44 34-130 N-Nitrosodiphenylamine ug/kg 9521640 58 48-130 Naphthalene ug/kg 8781640 54 46-130 Nitrobenzene ug/kg 8651640 53 39-130 Pentachlorophenol ug/kg 20203280 62 42-130 Phenanthrene ug/kg 11201640 69 50-130 Phenol ug/kg 9131640 56 42-130 Pyrene ug/kg 10401640 64 50-130 Pyridine ug/kg 4741640 29 26-130 2,4,6-Tribromophenol (S)%70 10-131 2-Fluorobiphenyl (S)%53 10-130 2-Fluorophenol (S)%48 10-130 Nitrobenzene-d5 (S)%52 10-130 Phenol-d6 (S)%53 10-130 Terphenyl-d14 (S)%63 10-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4092376MATRIX SPIKE SAMPLE: MSSpike Result 92679115001 1,2,4-Trichlorobenzene ug/kg 8791830 48 16-130ND 1,2-Dichlorobenzene ug/kg 8591830 47 19-130ND 1,3-Dichlorobenzene ug/kg 8281830 45 19-130ND 1,4-Dichlorobenzene ug/kg 8361830 46 20-130ND 1-Methylnaphthalene ug/kg 9311830 51 19-130ND 2,2'-Oxybis(1-chloropropane)ug/kg 8451830 46 10-130ND 2,4,5-Trichlorophenol ug/kg 8301830 45 19-130ND 2,4,6-Trichlorophenol ug/kg 8411830 46 18-130ND 2,4-Dichlorophenol ug/kg 9101830 50 16-130ND 2,4-Dimethylphenol ug/kg 966 v1183053 10-130ND 2,4-Dinitrophenol ug/kg 4790 v1913053 10-143ND 2,4-Dinitrotoluene ug/kg 9111830 50 19-130ND 2,6-Dinitrotoluene ug/kg 9021830 49 22-130ND 2-Chloronaphthalene ug/kg 7741830 42 18-130ND 2-Chlorophenol ug/kg 8591830 47 20-130ND 2-Methylnaphthalene ug/kg 8771830 48 18-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 131 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4092376MATRIX SPIKE SAMPLE: MSSpike Result 92679115001 2-Methylphenol(o-Cresol)ug/kg 8371830 46 13-130ND 2-Nitroaniline ug/kg 1610J3650 44 18-130ND 2-Nitrophenol ug/kg 9641830 53 19-130ND 3&4-Methylphenol(m&p Cresol)ug/kg 8491830 46 13-130ND 3,3'-Dichlorobenzidine ug/kg 13703650 37 10-130ND 3-Nitroaniline ug/kg 1480J3650 41 22-130ND 4,6-Dinitro-2-methylphenol ug/kg 19203650 53 10-144ND 4-Bromophenylphenyl ether ug/kg 8561830 47 18-130ND 4-Chloro-3-methylphenol ug/kg 18503650 51 16-130ND 4-Chloroaniline ug/kg 15203650 41 17-130ND 4-Chlorophenylphenyl ether ug/kg 8791830 48 17-130ND 4-Nitroaniline ug/kg 15203650 42 21-130ND 4-Nitrophenol ug/kg 42009130 46 13-131ND Acenaphthene ug/kg 8291830 45 20-130ND Acenaphthylene ug/kg 8241830 45 21-130ND Aniline ug/kg 4921830 27 10-130ND Anthracene ug/kg 7971830 44 19-130ND Benzo(a)anthracene ug/kg 8131830 45 17-130ND Benzo(a)pyrene ug/kg 8081830 44 14-130ND Benzo(b)fluoranthene ug/kg 7801830 43 11-134ND Benzo(g,h,i)perylene ug/kg 7441830 41 12-130ND Benzo(k)fluoranthene ug/kg 8521830 47 15-130ND Benzoic Acid ug/kg 22809130 25 10-130ND Benzyl alcohol ug/kg 16903650 46 20-130ND bis(2-Chloroethoxy)methane ug/kg 7931830 43 16-130ND bis(2-Chloroethyl) ether ug/kg 7951830 44 18-130ND bis(2-Ethylhexyl)phthalate ug/kg 8341830 46 11-130ND Butylbenzylphthalate ug/kg 8521830 47 10-130ND Chrysene ug/kg 8801830 48 17-130ND Di-n-butylphthalate ug/kg 8621830 47 16-130ND Di-n-octylphthalate ug/kg 8511830 47 16-130ND Dibenz(a,h)anthracene ug/kg 8091830 44 13-130ND Dibenzofuran ug/kg 8251830 45 19-130ND Diethylphthalate ug/kg 9041830 49 22-130ND Dimethylphthalate ug/kg 8761830 48 23-130ND Fluoranthene ug/kg 9101830 50 14-130ND Fluorene ug/kg 8611830 47 19-130ND Hexachloro-1,3-butadiene ug/kg 9271830 51 12-130ND Hexachlorobenzene ug/kg 8951830 49 17-130ND Hexachlorocyclopentadiene ug/kg 5431830 30 10-130ND Hexachloroethane ug/kg 8691830 48 14-130ND Indeno(1,2,3-cd)pyrene ug/kg 7631830 42 13-130ND Isophorone ug/kg 8891830 49 17-130ND N-Nitroso-di-n-propylamine ug/kg 9341830 51 10-130ND N-Nitrosodimethylamine ug/kg 7401830 41 16-130ND N-Nitrosodiphenylamine ug/kg 7951830 44 19-130ND Naphthalene ug/kg 8571830 47 18-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 132 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4092376MATRIX SPIKE SAMPLE: MSSpike Result 92679115001 Nitrobenzene ug/kg 8411830 46 15-130ND Pentachlorophenol ug/kg 14603650 40 10-130ND Phenanthrene ug/kg 8701830 48 17-130ND Phenol ug/kg 8761830 48 15-130ND Pyrene ug/kg 8231830 45 31-130ND Pyridine ug/kg 6111830 33 10-130ND 2,4,6-Tribromophenol (S)%48 10-131 2-Fluorobiphenyl (S)%42 10-130 2-Fluorophenol (S)%42 10-130 Nitrobenzene-d5 (S)%46 10-130 Phenol-d6 (S)%45 10-130 Terphenyl-d14 (S)%46 10-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92679115002 4092377SAMPLE DUPLICATE: 1,2,4-Trichlorobenzene ug/kg ND 30ND 1,2-Dichlorobenzene ug/kg ND 30ND 1,3-Dichlorobenzene ug/kg ND 30ND 1,4-Dichlorobenzene ug/kg ND 30ND 1-Methylnaphthalene ug/kg ND 30ND 2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND 2,4,5-Trichlorophenol ug/kg ND 30ND 2,4,6-Trichlorophenol ug/kg ND 30ND 2,4-Dichlorophenol ug/kg ND 30ND 2,4-Dimethylphenol ug/kg ND v130ND 2,4-Dinitrophenol ug/kg ND v130ND 2,4-Dinitrotoluene ug/kg ND 30ND 2,6-Dinitrotoluene ug/kg ND 30ND 2-Chloronaphthalene ug/kg ND 30ND 2-Chlorophenol ug/kg ND 30ND 2-Methylnaphthalene ug/kg ND 30ND 2-Methylphenol(o-Cresol)ug/kg ND 30ND 2-Nitroaniline ug/kg ND 30ND 2-Nitrophenol ug/kg ND 30ND 3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND 3,3'-Dichlorobenzidine ug/kg ND 30ND 3-Nitroaniline ug/kg ND 30ND 4,6-Dinitro-2-methylphenol ug/kg ND 30ND 4-Bromophenylphenyl ether ug/kg ND 30ND 4-Chloro-3-methylphenol ug/kg ND 30ND 4-Chloroaniline ug/kg ND 30ND 4-Chlorophenylphenyl ether ug/kg ND 30ND 4-Nitroaniline ug/kg ND 30ND 4-Nitrophenol ug/kg ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 133 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92679115002 4092377SAMPLE DUPLICATE: Acenaphthene ug/kg ND 30ND Acenaphthylene ug/kg ND 30ND Aniline ug/kg ND 30ND Anthracene ug/kg ND 30ND Benzo(a)anthracene ug/kg ND 30ND Benzo(a)pyrene ug/kg ND 30ND Benzo(b)fluoranthene ug/kg ND 30ND Benzo(g,h,i)perylene ug/kg ND 30ND Benzo(k)fluoranthene ug/kg ND 30ND Benzoic Acid ug/kg ND 30ND Benzyl alcohol ug/kg ND 30ND bis(2-Chloroethoxy)methane ug/kg ND 30ND bis(2-Chloroethyl) ether ug/kg ND 30ND bis(2-Ethylhexyl)phthalate ug/kg ND 30ND Butylbenzylphthalate ug/kg ND 30ND Chrysene ug/kg ND 30ND Di-n-butylphthalate ug/kg ND 30ND Di-n-octylphthalate ug/kg ND 30ND Dibenz(a,h)anthracene ug/kg ND 30ND Dibenzofuran ug/kg ND 30ND Diethylphthalate ug/kg ND 30ND Dimethylphthalate ug/kg ND 30ND Fluoranthene ug/kg ND 30ND Fluorene ug/kg ND 30ND Hexachloro-1,3-butadiene ug/kg ND 30ND Hexachlorobenzene ug/kg ND 30ND Hexachlorocyclopentadiene ug/kg ND 30ND Hexachloroethane ug/kg ND 30ND Indeno(1,2,3-cd)pyrene ug/kg ND 30ND Isophorone ug/kg ND 30ND N-Nitroso-di-n-propylamine ug/kg ND 30ND N-Nitrosodimethylamine ug/kg ND 30ND N-Nitrosodiphenylamine ug/kg ND 30ND Naphthalene ug/kg ND 30ND Nitrobenzene ug/kg ND 30ND Pentachlorophenol ug/kg ND 30ND Phenanthrene ug/kg ND 30ND Phenol ug/kg ND 30ND Pyrene ug/kg ND 30ND Pyridine ug/kg ND 30ND 2,4,6-Tribromophenol (S)%4845 2-Fluorobiphenyl (S)%3937 2-Fluorophenol (S)%3937 Nitrobenzene-d5 (S)%4742 Phenol-d6 (S)%4138 Terphenyl-d14 (S)%5248 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 134 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 788805 SW-846 SW-846 Dry Weight/Percent Moisture Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010, 92678743018 Parameter Units Dup Result Max RPD QualifiersRPDResult 92678750001 4088610SAMPLE DUPLICATE: Percent Moisture %10.9 N212511.0 Parameter Units Dup Result Max RPD QualifiersRPDResult 92678746004 4088611SAMPLE DUPLICATE: Percent Moisture %20.7 N222520.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 135 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2102699 SM 2540 G SM 2540G Total Solids 2540 G-2011 Laboratory:Pace National - Mt. Juliet Associated Lab Samples:92678743001, 92678743002, 92678743003, 92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3953807-1 Associated Lab Samples: 92678743001, 92678743002, 92678743003, 92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010 Matrix: Solid AnalyzedMDL Total Solids %0.00400 07/27/23 12:46 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3953807-2LABORATORY CONTROL SAMPLE: LCSSpike Total Solids %50.050.0 99.9 85.0-115 Parameter Units Dup Result Max RPD QualifiersRPDResult 92678743009 R3953807-3SAMPLE DUPLICATE: Total Solids %80.5 0.570 1080.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 136 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2102701 SM 2540 G SM 2540G Total Solids 2540 G-2011 Laboratory:Pace National - Mt. Juliet Associated Lab Samples: 92678743018 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3953772-1 Associated Lab Samples:92678743018 Matrix: Solid AnalyzedMDL Total Solids %0.00200 07/27/23 10:59 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3953772-2LABORATORY CONTROL SAMPLE: LCSSpike Total Solids %50.050.0 100 85.0-115 Parameter Units Dup Result Max RPD QualifiersRPDResult L1638832-02 R3953772-3SAMPLE DUPLICATE: Total Solids %93.2 1.72 1091.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 137 of 147 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92678743 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2102469 3060A EPA 7199 Wet Chemistry 7199 Laboratory:Pace National - Mt. Juliet Associated Lab Samples:92678743001, 92678743002, 92678743003, 92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010, 92678743018 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3954163-1 Associated Lab Samples: 92678743001, 92678743002, 92678743003, 92678743004, 92678743005, 92678743006, 92678743007, 92678743008, 92678743009, 92678743010, 92678743018 Matrix: Solid AnalyzedMDL Chromium, Hexavalent mg/kg ND 1.00 07/28/23 13:450.255 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3954163-2LABORATORY CONTROL SAMPLE: LCSSpike Chromium, Hexavalent mg/kg 10.510.0 105 80.0-120 Parameter Units MS Result % Rec Limits Qual% RecConc. R3954163-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result L1638772-04 R3954163-4 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Chromium, Hexavalent mg/kg 22.9 82.6 75.0-12594.7 12.9 2022.91.14 20.1 22.9 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. R3954163-5MATRIX SPIKE SAMPLE: MSSpike Result L1638772-04 Chromium, Hexavalent mg/kg 550731 75.2 75.0-1251.14 Parameter Units Dup Result Max RPD QualifiersRPDResult 92678743001 R3954163-7SAMPLE DUPLICATE: Chromium, Hexavalent mg/kg ND 0.00 20ND Parameter Units Dup Result Max RPD QualifiersRPDResult 92678743007 R3954163-8SAMPLE DUPLICATE: Chromium, Hexavalent mg/kg 0.638J D8,J36.5 200.922 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 138 of 147 #=QL# QUALIFIERS Pace Project No.: Project: 92678743 HNY-001 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Analyte is a possible laboratory contaminant (not present in method blank).C7 Common Laboratory Contaminant.C9 The sample and duplicate results for this parameter are less than 5 times the reporting limit, the RPD may not bestatistically valid.D8 Analyte concentration exceeded the calibration range. The reported result is estimated.E This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be considered an estimated value.IH Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request.N2 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias.v1 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias.v3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 139 of 147 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92678743 HNY-001 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92678743001 2102447 2102447BG-1 (0-2)3050B EPA 6020B 92678743002 2102447 2102447BG-2 (0-2)3050B EPA 6020B 92678743003 2102447 2102447BG-3 (0-2)3050B EPA 6020B 92678743004 2102447 2102447CS-1 (0-2)3050B EPA 6020B 92678743005 2102447 2102447CS-2 (0-2)3050B EPA 6020B 92678743006 2102447 2102447CS-3 (0-2)3050B EPA 6020B 92678743007 2102447 2102447CS-4 (0-2)3050B EPA 6020B 92678743008 2102447 2102447CS-5 (0-2)3050B EPA 6020B 92678743009 2102447 2102447CS-6 (0-2)3050B EPA 6020B 92678743010 2102447 2102447CS-7 (0-2)3050B EPA 6020B 92678743018 2102447 2102447SB-DUP 3050B EPA 6020B 92678743011 789135 789376TMW-7 EPA 3010A EPA 6020B 92678743012 789135 789376TMW-8 EPA 3010A EPA 6020B 92678743013 789135 789376TMW-9 EPA 3010A EPA 6020B 92678743014 789135 789376TMW-10 EPA 3010A EPA 6020B 92678743015 789135 789376TMW-11 EPA 3010A EPA 6020B 92678743016 789135 789376TMW-12 EPA 3010A EPA 6020B 92678743017 789135 789376TMW-DUP EPA 3010A EPA 6020B 92678743001 2102597 2102597BG-1 (0-2)7471A EPA 7471B 92678743002 2102597 2102597BG-2 (0-2)7471A EPA 7471B 92678743003 2102597 2102597BG-3 (0-2)7471A EPA 7471B 92678743004 2102597 2102597CS-1 (0-2)7471A EPA 7471B 92678743005 2102597 2102597CS-2 (0-2)7471A EPA 7471B 92678743006 2102597 2102597CS-3 (0-2)7471A EPA 7471B 92678743007 2102597 2102597CS-4 (0-2)7471A EPA 7471B 92678743008 2102597 2102597CS-5 (0-2)7471A EPA 7471B 92678743009 2102597 2102597CS-6 (0-2)7471A EPA 7471B 92678743010 2102597 2102597CS-7 (0-2)7471A EPA 7471B 92678743018 2102597 2102597SB-DUP 7471A EPA 7471B 92678743011 790262 790363TMW-7 EPA 7470A EPA 7470A 92678743012 790262 790363TMW-8 EPA 7470A EPA 7470A 92678743013 790262 790363TMW-9 EPA 7470A EPA 7470A 92678743014 790262 790363TMW-10 EPA 7470A EPA 7470A 92678743015 790262 790363TMW-11 EPA 7470A EPA 7470A 92678743016 790262 790363TMW-12 EPA 7470A EPA 7470A 92678743017 790262 790363TMW-DUP EPA 7470A EPA 7470A 92678743011 788712 789088TMW-7 EPA 3510C EPA 8270E 92678743012 788712 789088TMW-8 EPA 3510C EPA 8270E 92678743013 788712 789088TMW-9 EPA 3510C EPA 8270E 92678743014 789319 789739TMW-10 EPA 3510C EPA 8270E 92678743015 789319 789739TMW-11 EPA 3510C EPA 8270E 92678743016 788712 789088TMW-12 EPA 3510C EPA 8270E 92678743017 788712 789088TMW-DUP EPA 3510C EPA 8270E 92678743004 789567 790239CS-1 (0-2)EPA 3546 EPA 8270E 92678743005 789567 790239CS-2 (0-2)EPA 3546 EPA 8270E REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 140 of 147 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92678743 HNY-001 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92678743006 789567 790239CS-3 (0-2)EPA 3546 EPA 8270E 92678743007 789567 790239CS-4 (0-2)EPA 3546 EPA 8270E 92678743008 789567 790239CS-5 (0-2)EPA 3546 EPA 8270E 92678743009 789567 790239CS-6 (0-2)EPA 3546 EPA 8270E 92678743010 789567 790239CS-7 (0-2)EPA 3546 EPA 8270E 92678743018 789567 790239SB-DUP EPA 3546 EPA 8270E 92678743004 789111 789154CS-1 (0-2)EPA 5035A/5030B EPA 8260D 92678743005 789111 789154CS-2 (0-2)EPA 5035A/5030B EPA 8260D 92678743006 789111 789154CS-3 (0-2)EPA 5035A/5030B EPA 8260D 92678743007 789111 789154CS-4 (0-2)EPA 5035A/5030B EPA 8260D 92678743008 789111 789154CS-5 (0-2)EPA 5035A/5030B EPA 8260D 92678743009 789111 789154CS-6 (0-2)EPA 5035A/5030B EPA 8260D 92678743010 789195 789261CS-7 (0-2)EPA 5035A/5030B EPA 8260D 92678743018 789195 789261SB-DUP EPA 5035A/5030B EPA 8260D 92678743011 789175TMW-7 EPA 8260D 92678743012 789175TMW-8 EPA 8260D 92678743013 789175TMW-9 EPA 8260D 92678743014 789177TMW-10 EPA 8260D 92678743015 789177TMW-11 EPA 8260D 92678743016 789177TMW-12 EPA 8260D 92678743017 789177TMW-DUP EPA 8260D 92678743019 788852TRIP BLANK EPA 8260D 92678743004 788805CS-1 (0-2)SW-846 92678743005 788805CS-2 (0-2)SW-846 92678743006 788805CS-3 (0-2)SW-846 92678743007 788805CS-4 (0-2)SW-846 92678743008 788805CS-5 (0-2)SW-846 92678743009 788805CS-6 (0-2)SW-846 92678743010 788805CS-7 (0-2)SW-846 92678743018 788805SB-DUP SW-846 92678743001 2102699 2102699BG-1 (0-2)SM 2540 G SM 2540G 92678743002 2102699 2102699BG-2 (0-2)SM 2540 G SM 2540G 92678743003 2102699 2102699BG-3 (0-2)SM 2540 G SM 2540G 92678743004 2102699 2102699CS-1 (0-2)SM 2540 G SM 2540G 92678743005 2102699 2102699CS-2 (0-2)SM 2540 G SM 2540G 92678743006 2102699 2102699CS-3 (0-2)SM 2540 G SM 2540G 92678743007 2102699 2102699CS-4 (0-2)SM 2540 G SM 2540G 92678743008 2102699 2102699CS-5 (0-2)SM 2540 G SM 2540G 92678743009 2102699 2102699CS-6 (0-2)SM 2540 G SM 2540G 92678743010 2102699 2102699CS-7 (0-2)SM 2540 G SM 2540G 92678743018 2102701 2102701SB-DUP SM 2540 G SM 2540G 92678743001 2102469 2102469BG-1 (0-2)3060A EPA 7199 92678743002 2102469 2102469BG-2 (0-2)3060A EPA 7199 92678743003 2102469 2102469BG-3 (0-2)3060A EPA 7199 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 141 of 147 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92678743 HNY-001 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92678743004 2102469 2102469CS-1 (0-2)3060A EPA 7199 92678743005 2102469 2102469CS-2 (0-2)3060A EPA 7199 92678743006 2102469 2102469CS-3 (0-2)3060A EPA 7199 92678743007 2102469 2102469CS-4 (0-2)3060A EPA 7199 92678743008 2102469 2102469CS-5 (0-2)3060A EPA 7199 92678743009 2102469 2102469CS-6 (0-2)3060A EPA 7199 92678743010 2102469 2102469CS-7 (0-2)3060A EPA 7199 92678743018 2102469 2102469SB-DUP 3060A EPA 7199 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 09:02 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 142 of 147 Page 143 of 147 Page 144 of 147 Page 145 of 147 Page 146 of 147 Page 147 of 147 #=CL# August 03, 2023 LIMS USE: FR - BO CAPPLEMAN LIMS OBJECT ID: 92679117 92679117 Project: Pace Project No.: RE: Bo Cappleman Hart & Hickman 2923 South Tryon Street Charlotte, NC 28203 HNY-001 Dear Bo Cappleman: Enclosed are the analytical results for sample(s) received by the laboratory on July 25, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor M Cannon taylor.cannon@pacelabs.com Project Manager (704)875-9092 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 68 #=CP# CERTIFICATIONS Pace Project No.: Project: 92679117 HNY-001 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: AI30792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TN003 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification #: CERT0086 Nebraska Certification #: NE-OS-15-05 Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TN002 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LAO00356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Certification #: T 104704245-17-14 Texas Mold Certification #: LAB0152 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A2LA 2926.01 A2LA-ISO 17025 Certification #: 1461.01 A2LA-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 68 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92679117 HNY-001 Lab ID Sample ID Matrix Date Collected Date Received 92679117001 SG-1 Air 07/20/23 15:35 07/25/23 09:30 92679117002 SG-2 Air 07/20/23 16:06 07/25/23 09:30 92679117003 SG-3 Air 07/21/23 11:21 07/25/23 09:30 92679117004 SG-4 Air 07/21/23 11:49 07/25/23 09:30 92679117005 SG-5 Air 07/21/23 13:01 07/25/23 09:30 92679117006 SG-6 Air 07/21/23 13:26 07/25/23 09:30 92679117007 SG-7 Air 07/21/23 14:02 07/25/23 09:30 92679117008 SG-8 Air 07/21/23 13:25 07/25/23 09:30 92679117009 SG-9 Air 07/21/23 11:30 07/25/23 09:30 92679117010 SG-10 Air 07/21/23 11:26 07/25/23 09:30 92679117011 SG-11 Air 07/21/23 10:05 07/25/23 09:30 92679117012 SG-12 Air 07/21/23 09:52 07/25/23 09:30 92679117013 SG-13 Air 07/21/23 09:27 07/25/23 09:30 92679117014 SG-14 Air 07/21/23 09:00 07/25/23 09:30 92679117015 SG-15 Air 07/21/23 09:04 07/25/23 09:30 92679117016 SG-16 Air 07/20/23 09:38 07/25/23 09:30 92679117017 SG-17 Air 07/20/23 10:05 07/25/23 09:30 92679117018 SG-18 Air 07/20/23 10:59 07/25/23 09:30 92679117019 SG-19 Air 07/20/23 12:03 07/25/23 09:30 92679117020 SG-20 Air 07/20/23 12:42 07/25/23 09:30 92679117021 SG-21 Air 07/20/23 13:17 07/25/23 09:30 92679117022 SG-22 Air 07/20/23 14:17 07/25/23 09:30 92679117023 SG-23 Air 07/20/23 14:58 07/25/23 09:30 92679117024 SG-DUP Air 07/20/23 00:00 07/25/23 09:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 68 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92679117 HNY-001 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92679117001 SG-1 TO-15 69 PANSDS 92679117002 SG-2 TO-15 69 PANSDS 92679117003 SG-3 TO-15 69 PANSDS 92679117004 SG-4 TO-15 69 PANSDS 92679117005 SG-5 TO-15 69 PANSDS 92679117006 SG-6 TO-15 69 PANDBB, SDS 92679117007 SG-7 TO-15 69 PANSDS 92679117008 SG-8 TO-15 69 PANSDS 92679117009 SG-9 TO-15 69 PANSDS 92679117010 SG-10 TO-15 69 PANDBB, SDS 92679117011 SG-11 TO-15 69 PANDBB, SDS 92679117012 SG-12 TO-15 69 PANSDS 92679117013 SG-13 TO-15 69 PANSDS 92679117014 SG-14 TO-15 69 PANJAP, SDS 92679117015 SG-15 TO-15 69 PANSDS 92679117016 SG-16 TO-15 69 PANSDS 92679117017 SG-17 TO-15 69 PANSDS 92679117018 SG-18 TO-15 69 PANSDS 92679117019 SG-19 TO-15 69 PANSDS 92679117020 SG-20 TO-15 69 PANSDS 92679117021 SG-21 TO-15 69 PANJAP 92679117022 SG-22 TO-15 69 PANJAP 92679117023 SG-23 TO-15 69 PANJAP 92679117024 SG-DUP TO-15 69 PANJAP PAN = Pace National - Mt. Juliet REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-1 Lab ID: 92679117001 Collected: 07/20/23 15:35 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 15.4 ug/m3 07/26/23 11:38 67-64-107/26/23 11:382.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 11:38 107-05-107/26/23 11:380.626 0.357 1 Benzene 7.09 ug/m3 07/26/23 11:38 71-43-207/26/23 11:380.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 11:38 100-44-707/26/23 11:381.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 11:38 75-27-407/26/23 11:381.34 0.471 1 Bromoform ND ug/m3 07/26/23 11:38 75-25-207/26/23 11:386.21 0.757 1 Bromomethane ND ug/m3 07/26/23 11:38 74-83-907/26/23 11:380.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 11:38 106-99-007/26/23 11:384.43 0.230 1 Carbon disulfide 5.98 ug/m3 07/26/23 11:38 75-15-007/26/23 11:380.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 11:38 56-23-507/26/23 11:381.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 11:38 108-90-707/26/23 11:380.924 0.385 1 Chloroethane ND ug/m3 07/26/23 11:38 75-00-307/26/23 11:380.528 0.263 1 Chloroform 2.64 ug/m3 07/26/23 11:38 67-66-307/26/23 11:380.973 0.349 1 Chloromethane 1.35 ug/m3 07/26/23 11:38 74-87-307/26/23 11:380.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 11:38 95-49-807/26/23 11:381.03 0.427 1 Cyclohexane 1.18 ug/m3 07/26/23 11:38 110-82-707/26/23 11:380.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 11:38 124-48-107/26/23 11:381.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 11:38 106-93-407/26/23 11:381.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 11:38 95-50-107/26/23 11:381.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 11:38 541-73-107/26/23 11:381.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 11:38 106-46-707/26/23 11:381.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 11:38 107-06-207/26/23 11:380.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 11:38 75-34-307/26/23 11:380.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 11:38 75-35-407/26/23 11:380.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 11:38 156-59-207/26/23 11:380.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 11:38 156-60-507/26/23 11:380.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 11:38 78-87-507/26/23 11:380.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 11:38 10061-01-507/26/23 11:380.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 11:38 10061-02-607/26/23 11:380.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 11:38 123-91-107/26/23 11:380.721 0.300 1 Ethanol 27.5 ug/m3 07/26/23 11:38 64-17-507/26/23 11:384.71 0.500 1 Ethylbenzene 6.50 ug/m3 07/26/23 11:38 100-41-407/26/23 11:380.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 11:38 141-78-607/26/23 11:380.720 0.360 1 4-Ethyltoluene 1.29 ug/m3 07/26/23 11:38 622-96-807/26/23 11:380.982 0.384 1 Trichlorofluoromethane 32.5 ug/m3 07/26/23 11:38 75-69-407/26/23 11:381.12 0.460 1 Dichlorodifluoromethane 0.989J ug/m3 07/26/23 11:38 75-71-8 J07/26/23 11:380.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 11:38 76-13-107/26/23 11:381.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 11:38 76-14-207/26/23 11:381.40 0.622 1 n-Heptane 9.86 ug/m3 07/26/23 11:38 142-82-507/26/23 11:380.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 11:38 87-68-307/26/23 11:386.73 1.12 1 n-Hexane 2.93 ug/m3 07/26/23 11:38 110-54-307/26/23 11:382.22 0.726 1 Isopropylbenzene (Cumene)1.44 ug/m3 07/26/23 11:38 98-82-807/26/23 11:380.983 0.382 1 Methylene Chloride 0.712 ug/m3 07/26/23 11:38 75-09-207/26/23 11:380.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 11:38 591-78-607/26/23 11:385.11 0.544 1 2-Butanone (MEK)3.39J ug/m3 07/26/23 11:38 78-93-3 J07/26/23 11:383.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-1 Lab ID: 92679117001 Collected: 07/20/23 15:35 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 11:38 108-10-107/26/23 11:385.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 11:38 80-62-607/26/23 11:380.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 11:38 1634-04-407/26/23 11:380.721 0.233 1 Naphthalene ND ug/m3 07/26/23 11:38 91-20-307/26/23 11:383.30 1.83 1 2-Propanol 6.10 ug/m3 07/26/23 11:38 67-63-007/26/23 11:383.07 0.649 1 Propylene ND ug/m3 07/26/23 11:38 115-07-107/26/23 11:382.15 0.160 1 Styrene ND ug/m3 07/26/23 11:38 100-42-507/26/23 11:380.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 11:38 79-34-507/26/23 11:381.37 0.511 1 Tetrachloroethene 97.8 ug/m3 07/26/23 11:38 127-18-407/26/23 11:381.36 0.553 1 Tetrahydrofuran 0.445J ug/m3 07/26/23 11:38 109-99-9 J07/26/23 11:380.590 0.216 1 Toluene 67.1 ug/m3 07/26/23 11:38 108-88-307/26/23 11:381.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 11:38 120-82-107/26/23 11:384.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 11:38 71-55-607/26/23 11:381.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 11:38 79-00-507/26/23 11:381.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 11:38 79-01-607/26/23 11:381.07 0.364 1 1,2,4-Trimethylbenzene 4.31 ug/m3 07/26/23 11:38 95-63-607/26/23 11:380.982 0.375 1 1,3,5-Trimethylbenzene 1.48 ug/m3 07/26/23 11:38 108-67-807/26/23 11:380.982 0.382 1 2,2,4-Trimethylpentane 4.09 ug/m3 07/26/23 11:38 540-84-107/26/23 11:380.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 11:38 75-01-407/26/23 11:380.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 11:38 593-60-207/26/23 11:380.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 11:38 108-05-407/26/23 11:380.704 0.408 1 m&p-Xylene 20.6 ug/m3 07/26/23 11:38 179601-23-107/26/23 11:381.73 0.585 1 o-Xylene 7.98 ug/m3 07/26/23 11:38 95-47-607/26/23 11:380.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)105 %07/26/23 11:38 460-00-407/26/23 11:3860.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-2 Lab ID: 92679117002 Collected: 07/20/23 16:06 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 58.0 ug/m3 07/26/23 12:07 67-64-107/26/23 12:072.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 12:07 107-05-107/26/23 12:070.626 0.357 1 Benzene 38.3 ug/m3 07/26/23 12:07 71-43-207/26/23 12:070.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 12:07 100-44-707/26/23 12:071.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 12:07 75-27-407/26/23 12:071.34 0.471 1 Bromoform ND ug/m3 07/26/23 12:07 75-25-207/26/23 12:076.21 0.757 1 Bromomethane ND ug/m3 07/26/23 12:07 74-83-907/26/23 12:070.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 12:07 106-99-007/26/23 12:074.43 0.230 1 Carbon disulfide 58.5 ug/m3 07/26/23 12:07 75-15-007/26/23 12:070.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 12:07 56-23-507/26/23 12:071.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 12:07 108-90-707/26/23 12:070.924 0.385 1 Chloroethane ND ug/m3 07/26/23 12:07 75-00-307/26/23 12:070.528 0.263 1 Chloroform 1.59 ug/m3 07/26/23 12:07 67-66-307/26/23 12:070.973 0.349 1 Chloromethane 0.314J ug/m3 07/26/23 12:07 74-87-3 J07/26/23 12:070.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 12:07 95-49-807/26/23 12:071.03 0.427 1 Cyclohexane 18.9 ug/m3 07/26/23 12:07 110-82-707/26/23 12:070.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 12:07 124-48-107/26/23 12:071.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 12:07 106-93-407/26/23 12:071.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 12:07 95-50-107/26/23 12:071.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 12:07 541-73-107/26/23 12:071.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 12:07 106-46-707/26/23 12:071.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 12:07 107-06-207/26/23 12:070.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 12:07 75-34-307/26/23 12:070.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 12:07 75-35-407/26/23 12:070.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 12:07 156-59-207/26/23 12:070.793 0.311 1 trans-1,2-Dichloroethene 1.32 ug/m3 07/26/23 12:07 156-60-507/26/23 12:070.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 12:07 78-87-507/26/23 12:070.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 12:07 10061-01-507/26/23 12:070.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 12:07 10061-02-607/26/23 12:070.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 12:07 123-91-107/26/23 12:070.721 0.300 1 Ethanol 26.8 ug/m3 07/26/23 12:07 64-17-507/26/23 12:074.71 0.500 1 Ethylbenzene 27.3 ug/m3 07/26/23 12:07 100-41-407/26/23 12:070.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 12:07 141-78-607/26/23 12:070.720 0.360 1 4-Ethyltoluene 3.80 ug/m3 07/26/23 12:07 622-96-807/26/23 12:070.982 0.384 1 Trichlorofluoromethane 10.6 ug/m3 07/26/23 12:07 75-69-407/26/23 12:071.12 0.460 1 Dichlorodifluoromethane 1.96 ug/m3 07/26/23 12:07 75-71-807/26/23 12:070.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 12:07 76-13-107/26/23 12:071.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 12:07 76-14-207/26/23 12:071.40 0.622 1 n-Heptane 198 ug/m3 07/26/23 12:07 142-82-507/26/23 12:070.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 12:07 87-68-307/26/23 12:076.73 1.12 1 n-Hexane 76.5 ug/m3 07/26/23 12:07 110-54-307/26/23 12:072.22 0.726 1 Isopropylbenzene (Cumene)4.79 ug/m3 07/26/23 12:07 98-82-807/26/23 12:070.983 0.382 1 Methylene Chloride 1.08 ug/m3 07/26/23 12:07 75-09-207/26/23 12:070.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 12:07 591-78-607/26/23 12:075.11 0.544 1 2-Butanone (MEK)14.7 ug/m3 07/26/23 12:07 78-93-307/26/23 12:073.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-2 Lab ID: 92679117002 Collected: 07/20/23 16:06 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 12:07 108-10-107/26/23 12:075.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 12:07 80-62-607/26/23 12:070.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 12:07 1634-04-407/26/23 12:070.721 0.233 1 Naphthalene 2.37J ug/m3 07/26/23 12:07 91-20-3 J07/26/23 12:073.30 1.83 1 2-Propanol 5.75 ug/m3 07/26/23 12:07 67-63-007/26/23 12:073.07 0.649 1 Propylene 9.68 ug/m3 07/26/23 12:07 115-07-107/26/23 12:072.15 0.160 1 Styrene 0.766J ug/m3 07/26/23 12:07 100-42-5 J07/26/23 12:070.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 12:07 79-34-507/26/23 12:071.37 0.511 1 Tetrachloroethene 277 ug/m3 07/26/23 12:07 127-18-407/26/23 12:071.36 0.553 1 Tetrahydrofuran 1.52 ug/m3 07/26/23 12:07 109-99-907/26/23 12:070.590 0.216 1 Toluene 246 ug/m3 07/26/23 12:07 108-88-307/26/23 12:071.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 12:07 120-82-107/26/23 12:074.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 12:07 71-55-607/26/23 12:071.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 12:07 79-00-507/26/23 12:071.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 12:07 79-01-607/26/23 12:071.07 0.364 1 1,2,4-Trimethylbenzene 11.2 ug/m3 07/26/23 12:07 95-63-607/26/23 12:070.982 0.375 1 1,3,5-Trimethylbenzene 3.21 ug/m3 07/26/23 12:07 108-67-807/26/23 12:070.982 0.382 1 2,2,4-Trimethylpentane 134 ug/m3 07/26/23 12:07 540-84-107/26/23 12:070.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 12:07 75-01-407/26/23 12:070.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 12:07 593-60-207/26/23 12:070.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 12:07 108-05-407/26/23 12:070.704 0.408 1 m&p-Xylene 70.7 ug/m3 07/26/23 12:07 179601-23-107/26/23 12:071.73 0.585 1 o-Xylene 25.7 ug/m3 07/26/23 12:07 95-47-607/26/23 12:070.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)107 %07/26/23 12:07 460-00-407/26/23 12:0760.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-3 Lab ID: 92679117003 Collected: 07/21/23 11:21 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 25.0 ug/m3 07/26/23 12:35 67-64-107/26/23 12:352.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 12:35 107-05-107/26/23 12:350.626 0.357 1 Benzene 14.7 ug/m3 07/26/23 12:35 71-43-207/26/23 12:350.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 12:35 100-44-707/26/23 12:351.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 12:35 75-27-407/26/23 12:351.34 0.471 1 Bromoform ND ug/m3 07/26/23 12:35 75-25-207/26/23 12:356.21 0.757 1 Bromomethane ND ug/m3 07/26/23 12:35 74-83-907/26/23 12:350.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 12:35 106-99-007/26/23 12:354.43 0.230 1 Carbon disulfide 33.3 ug/m3 07/26/23 12:35 75-15-007/26/23 12:350.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 12:35 56-23-507/26/23 12:351.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 12:35 108-90-707/26/23 12:350.924 0.385 1 Chloroethane ND ug/m3 07/26/23 12:35 75-00-307/26/23 12:350.528 0.263 1 Chloroform 16.1 ug/m3 07/26/23 12:35 67-66-307/26/23 12:350.973 0.349 1 Chloromethane 0.547 ug/m3 07/26/23 12:35 74-87-307/26/23 12:350.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 12:35 95-49-807/26/23 12:351.03 0.427 1 Cyclohexane 6.20 ug/m3 07/26/23 12:35 110-82-707/26/23 12:350.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 12:35 124-48-107/26/23 12:351.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 12:35 106-93-407/26/23 12:351.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 12:35 95-50-107/26/23 12:351.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 12:35 541-73-107/26/23 12:351.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 12:35 106-46-707/26/23 12:351.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 12:35 107-06-207/26/23 12:350.810 0.283 1 1,1-Dichloroethane 0.291J ug/m3 07/26/23 12:35 75-34-3 J07/26/23 12:350.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 12:35 75-35-407/26/23 12:350.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 12:35 156-59-207/26/23 12:350.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 12:35 156-60-507/26/23 12:350.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 12:35 78-87-507/26/23 12:350.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 12:35 10061-01-507/26/23 12:350.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 12:35 10061-02-607/26/23 12:350.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 12:35 123-91-107/26/23 12:350.721 0.300 1 Ethanol 42.8 ug/m3 07/26/23 12:35 64-17-507/26/23 12:354.71 0.500 1 Ethylbenzene 12.8 ug/m3 07/26/23 12:35 100-41-407/26/23 12:350.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 12:35 141-78-607/26/23 12:350.720 0.360 1 4-Ethyltoluene 2.38 ug/m3 07/26/23 12:35 622-96-807/26/23 12:350.982 0.384 1 Trichlorofluoromethane 120 ug/m3 07/26/23 12:35 75-69-407/26/23 12:351.12 0.460 1 Dichlorodifluoromethane 1.58 ug/m3 07/26/23 12:35 75-71-807/26/23 12:350.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 12:35 76-13-107/26/23 12:351.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 12:35 76-14-207/26/23 12:351.40 0.622 1 n-Heptane 52.8 ug/m3 07/26/23 12:35 142-82-507/26/23 12:350.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 12:35 87-68-307/26/23 12:356.73 1.12 1 n-Hexane 16.6 ug/m3 07/26/23 12:35 110-54-307/26/23 12:352.22 0.726 1 Isopropylbenzene (Cumene)2.32 ug/m3 07/26/23 12:35 98-82-807/26/23 12:350.983 0.382 1 Methylene Chloride ND ug/m3 07/26/23 12:35 75-09-207/26/23 12:350.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 12:35 591-78-607/26/23 12:355.11 0.544 1 2-Butanone (MEK)4.84 ug/m3 07/26/23 12:35 78-93-307/26/23 12:353.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-3 Lab ID: 92679117003 Collected: 07/21/23 11:21 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 12:35 108-10-107/26/23 12:355.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 12:35 80-62-607/26/23 12:350.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 12:35 1634-04-407/26/23 12:350.721 0.233 1 Naphthalene ND ug/m3 07/26/23 12:35 91-20-307/26/23 12:353.30 1.83 1 2-Propanol 5.53 ug/m3 07/26/23 12:35 67-63-007/26/23 12:353.07 0.649 1 Propylene 1.84J ug/m3 07/26/23 12:35 115-07-1 J07/26/23 12:352.15 0.160 1 Styrene 0.570J ug/m3 07/26/23 12:35 100-42-5 J07/26/23 12:350.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 12:35 79-34-507/26/23 12:351.37 0.511 1 Tetrachloroethene 143 ug/m3 07/26/23 12:35 127-18-407/26/23 12:351.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 12:35 109-99-907/26/23 12:350.590 0.216 1 Toluene 123 ug/m3 07/26/23 12:35 108-88-307/26/23 12:351.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 12:35 120-82-107/26/23 12:354.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 12:35 71-55-607/26/23 12:351.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 12:35 79-00-507/26/23 12:351.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 12:35 79-01-607/26/23 12:351.07 0.364 1 1,2,4-Trimethylbenzene 9.18 ug/m3 07/26/23 12:35 95-63-607/26/23 12:350.982 0.375 1 1,3,5-Trimethylbenzene 2.97 ug/m3 07/26/23 12:35 108-67-807/26/23 12:350.982 0.382 1 2,2,4-Trimethylpentane 40.6 ug/m3 07/26/23 12:35 540-84-107/26/23 12:350.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 12:35 75-01-407/26/23 12:350.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 12:35 593-60-207/26/23 12:350.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 12:35 108-05-407/26/23 12:350.704 0.408 1 m&p-Xylene 38.6 ug/m3 07/26/23 12:35 179601-23-107/26/23 12:351.73 0.585 1 o-Xylene 14.0 ug/m3 07/26/23 12:35 95-47-607/26/23 12:350.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)106 %07/26/23 12:35 460-00-407/26/23 12:3560.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-4 Lab ID: 92679117004 Collected: 07/21/23 11:49 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 53.2 ug/m3 07/26/23 13:03 67-64-107/26/23 13:032.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 13:03 107-05-107/26/23 13:030.626 0.357 1 Benzene 30.6 ug/m3 07/26/23 13:03 71-43-207/26/23 13:030.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 13:03 100-44-707/26/23 13:031.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 13:03 75-27-407/26/23 13:031.34 0.471 1 Bromoform ND ug/m3 07/26/23 13:03 75-25-207/26/23 13:036.21 0.757 1 Bromomethane ND ug/m3 07/26/23 13:03 74-83-907/26/23 13:030.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 13:03 106-99-007/26/23 13:034.43 0.230 1 Carbon disulfide 167 ug/m3 07/26/23 13:03 75-15-007/26/23 13:030.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 13:03 56-23-507/26/23 13:031.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 13:03 108-90-707/26/23 13:030.924 0.385 1 Chloroethane ND ug/m3 07/26/23 13:03 75-00-307/26/23 13:030.528 0.263 1 Chloroform ND ug/m3 07/26/23 13:03 67-66-307/26/23 13:030.973 0.349 1 Chloromethane 1.04 ug/m3 07/26/23 13:03 74-87-307/26/23 13:030.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 13:03 95-49-807/26/23 13:031.03 0.427 1 Cyclohexane 59.2 ug/m3 07/26/23 13:03 110-82-707/26/23 13:030.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 13:03 124-48-107/26/23 13:031.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 13:03 106-93-407/26/23 13:031.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 13:03 95-50-107/26/23 13:031.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 13:03 541-73-107/26/23 13:031.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 13:03 106-46-707/26/23 13:031.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 13:03 107-06-207/26/23 13:030.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 13:03 75-34-307/26/23 13:030.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 13:03 75-35-407/26/23 13:030.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 13:03 156-59-207/26/23 13:030.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 13:03 156-60-507/26/23 13:030.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 13:03 78-87-507/26/23 13:030.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 13:03 10061-01-507/26/23 13:030.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 13:03 10061-02-607/26/23 13:030.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 13:03 123-91-107/26/23 13:030.721 0.300 1 Ethanol 79.2 ug/m3 07/26/23 13:03 64-17-507/26/23 13:034.71 0.500 1 Ethylbenzene 35.2 ug/m3 07/26/23 13:03 100-41-407/26/23 13:030.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 13:03 141-78-607/26/23 13:030.720 0.360 1 4-Ethyltoluene 5.06 ug/m3 07/26/23 13:03 622-96-807/26/23 13:030.982 0.384 1 Trichlorofluoromethane 127 ug/m3 07/26/23 13:03 75-69-407/26/23 13:031.12 0.460 1 Dichlorodifluoromethane 2.07 ug/m3 07/26/23 13:03 75-71-807/26/23 13:030.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 13:03 76-13-107/26/23 13:031.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 13:03 76-14-207/26/23 13:031.40 0.622 1 n-Heptane 274 ug/m3 07/26/23 13:03 142-82-507/26/23 13:030.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 13:03 87-68-307/26/23 13:036.73 1.12 1 n-Hexane 93.1 ug/m3 07/26/23 13:03 110-54-307/26/23 13:032.22 0.726 1 Isopropylbenzene (Cumene)7.18 ug/m3 07/26/23 13:03 98-82-807/26/23 13:030.983 0.382 1 Methylene Chloride 8.65 ug/m3 07/26/23 13:03 75-09-207/26/23 13:030.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 13:03 591-78-607/26/23 13:035.11 0.544 1 2-Butanone (MEK)10.5 ug/m3 07/26/23 13:03 78-93-307/26/23 13:033.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-4 Lab ID: 92679117004 Collected: 07/21/23 11:49 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 13:03 108-10-107/26/23 13:035.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 13:03 80-62-607/26/23 13:030.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 13:03 1634-04-407/26/23 13:030.721 0.233 1 Naphthalene ND ug/m3 07/26/23 13:03 91-20-307/26/23 13:033.30 1.83 1 2-Propanol 16.5 ug/m3 07/26/23 13:03 67-63-007/26/23 13:033.07 0.649 1 Propylene 115 ug/m3 07/26/23 13:03 115-07-107/26/23 13:032.15 0.160 1 Styrene 1.15 ug/m3 07/26/23 13:03 100-42-507/26/23 13:030.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 13:03 79-34-507/26/23 13:031.37 0.511 1 Tetrachloroethene 267 ug/m3 07/26/23 13:03 127-18-407/26/23 13:031.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 13:03 109-99-907/26/23 13:030.590 0.216 1 Toluene 277 ug/m3 07/26/23 13:03 108-88-307/26/23 13:031.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 13:03 120-82-107/26/23 13:034.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 13:03 71-55-607/26/23 13:031.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 13:03 79-00-507/26/23 13:031.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 13:03 79-01-607/26/23 13:031.07 0.364 1 1,2,4-Trimethylbenzene 17.7 ug/m3 07/26/23 13:03 95-63-607/26/23 13:030.982 0.375 1 1,3,5-Trimethylbenzene 6.38 ug/m3 07/26/23 13:03 108-67-807/26/23 13:030.982 0.382 1 2,2,4-Trimethylpentane 157 ug/m3 07/26/23 13:03 540-84-107/26/23 13:030.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 13:03 75-01-407/26/23 13:030.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 13:03 593-60-207/26/23 13:030.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 13:03 108-05-407/26/23 13:030.704 0.408 1 m&p-Xylene 95.4 ug/m3 07/26/23 13:03 179601-23-107/26/23 13:031.73 0.585 1 o-Xylene 31.1 ug/m3 07/26/23 13:03 95-47-607/26/23 13:030.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)107 %07/26/23 13:03 460-00-407/26/23 13:0360.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-5 Lab ID: 92679117005 Collected: 07/21/23 13:01 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 37.1 ug/m3 07/26/23 13:31 67-64-107/26/23 13:312.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 13:31 107-05-107/26/23 13:310.626 0.357 1 Benzene 20.2 ug/m3 07/26/23 13:31 71-43-207/26/23 13:310.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 13:31 100-44-707/26/23 13:311.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 13:31 75-27-407/26/23 13:311.34 0.471 1 Bromoform ND ug/m3 07/26/23 13:31 75-25-207/26/23 13:316.21 0.757 1 Bromomethane ND ug/m3 07/26/23 13:31 74-83-907/26/23 13:310.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 13:31 106-99-007/26/23 13:314.43 0.230 1 Carbon disulfide 59.1 ug/m3 07/26/23 13:31 75-15-007/26/23 13:310.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 13:31 56-23-507/26/23 13:311.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 13:31 108-90-707/26/23 13:310.924 0.385 1 Chloroethane 0.353J ug/m3 07/26/23 13:31 75-00-3 J07/26/23 13:310.528 0.263 1 Chloroform 9.59 ug/m3 07/26/23 13:31 67-66-307/26/23 13:310.973 0.349 1 Chloromethane 1.18 ug/m3 07/26/23 13:31 74-87-307/26/23 13:310.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 13:31 95-49-807/26/23 13:311.03 0.427 1 Cyclohexane 10.8 ug/m3 07/26/23 13:31 110-82-707/26/23 13:310.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 13:31 124-48-107/26/23 13:311.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 13:31 106-93-407/26/23 13:311.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 13:31 95-50-107/26/23 13:311.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 13:31 541-73-107/26/23 13:311.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 13:31 106-46-707/26/23 13:311.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 13:31 107-06-207/26/23 13:310.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 13:31 75-34-307/26/23 13:310.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 13:31 75-35-407/26/23 13:310.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 13:31 156-59-207/26/23 13:310.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 13:31 156-60-507/26/23 13:310.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 13:31 78-87-507/26/23 13:310.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 13:31 10061-01-507/26/23 13:310.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 13:31 10061-02-607/26/23 13:310.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 13:31 123-91-107/26/23 13:310.721 0.300 1 Ethanol 99.9 ug/m3 07/26/23 13:31 64-17-507/26/23 13:314.71 0.500 1 Ethylbenzene 18.4 ug/m3 07/26/23 13:31 100-41-407/26/23 13:310.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 13:31 141-78-607/26/23 13:310.720 0.360 1 4-Ethyltoluene 5.20 ug/m3 07/26/23 13:31 622-96-807/26/23 13:310.982 0.384 1 Trichlorofluoromethane 34.1 ug/m3 07/26/23 13:31 75-69-407/26/23 13:311.12 0.460 1 Dichlorodifluoromethane 1.59 ug/m3 07/26/23 13:31 75-71-807/26/23 13:310.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 13:31 76-13-107/26/23 13:311.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 13:31 76-14-207/26/23 13:311.40 0.622 1 n-Heptane 87.9 ug/m3 07/26/23 13:31 142-82-507/26/23 13:310.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 13:31 87-68-307/26/23 13:316.73 1.12 1 n-Hexane 36.0 ug/m3 07/26/23 13:31 110-54-307/26/23 13:312.22 0.726 1 Isopropylbenzene (Cumene)7.82 ug/m3 07/26/23 13:31 98-82-807/26/23 13:310.983 0.382 1 Methylene Chloride 3.14 ug/m3 07/26/23 13:31 75-09-207/26/23 13:310.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 13:31 591-78-607/26/23 13:315.11 0.544 1 2-Butanone (MEK)5.93 ug/m3 07/26/23 13:31 78-93-307/26/23 13:313.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-5 Lab ID: 92679117005 Collected: 07/21/23 13:01 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 13:31 108-10-107/26/23 13:315.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 13:31 80-62-607/26/23 13:310.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 13:31 1634-04-407/26/23 13:310.721 0.233 1 Naphthalene ND ug/m3 07/26/23 13:31 91-20-307/26/23 13:313.30 1.83 1 2-Propanol 18.5 ug/m3 07/26/23 13:31 67-63-007/26/23 13:313.07 0.649 1 Propylene 14.6 ug/m3 07/26/23 13:31 115-07-107/26/23 13:312.15 0.160 1 Styrene 1.56 ug/m3 07/26/23 13:31 100-42-507/26/23 13:310.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 13:31 79-34-507/26/23 13:311.37 0.511 1 Tetrachloroethene 111 ug/m3 07/26/23 13:31 127-18-407/26/23 13:311.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 13:31 109-99-907/26/23 13:310.590 0.216 1 Toluene 148 ug/m3 07/26/23 13:31 108-88-307/26/23 13:311.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 13:31 120-82-107/26/23 13:314.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 13:31 71-55-607/26/23 13:311.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 13:31 79-00-507/26/23 13:311.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 13:31 79-01-607/26/23 13:311.07 0.364 1 1,2,4-Trimethylbenzene 17.9 ug/m3 07/26/23 13:31 95-63-607/26/23 13:310.982 0.375 1 1,3,5-Trimethylbenzene 5.25 ug/m3 07/26/23 13:31 108-67-807/26/23 13:310.982 0.382 1 2,2,4-Trimethylpentane 64.9 ug/m3 07/26/23 13:31 540-84-107/26/23 13:310.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 13:31 75-01-407/26/23 13:310.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 13:31 593-60-207/26/23 13:310.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 13:31 108-05-407/26/23 13:310.704 0.408 1 m&p-Xylene 55.9 ug/m3 07/26/23 13:31 179601-23-107/26/23 13:311.73 0.585 1 o-Xylene 19.3 ug/m3 07/26/23 13:31 95-47-607/26/23 13:310.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)113 %07/26/23 13:31 460-00-407/26/23 13:3160.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-6 Lab ID: 92679117006 Collected: 07/21/23 13:26 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 23.1 ug/m3 07/26/23 13:59 67-64-107/26/23 13:592.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 13:59 107-05-107/26/23 13:590.626 0.357 1 Benzene 7.86 ug/m3 07/26/23 13:59 71-43-207/26/23 13:590.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 13:59 100-44-707/26/23 13:591.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 13:59 75-27-407/26/23 13:591.34 0.471 1 Bromoform ND ug/m3 07/26/23 13:59 75-25-207/26/23 13:596.21 0.757 1 Bromomethane ND ug/m3 07/26/23 13:59 74-83-907/26/23 13:590.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 13:59 106-99-007/26/23 13:594.43 0.230 1 Carbon disulfide ND ug/m3 07/26/23 13:59 75-15-007/26/23 13:590.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 13:59 56-23-507/26/23 13:591.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 13:59 108-90-707/26/23 13:590.924 0.385 1 Chloroethane ND ug/m3 07/26/23 13:59 75-00-307/26/23 13:590.528 0.263 1 Chloroform 9.93 ug/m3 07/26/23 13:59 67-66-307/26/23 13:590.973 0.349 1 Chloromethane 0.795 ug/m3 07/26/23 13:59 74-87-307/26/23 13:590.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 13:59 95-49-807/26/23 13:591.03 0.427 1 Cyclohexane 3.58 ug/m3 07/26/23 13:59 110-82-707/26/23 13:590.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 13:59 124-48-107/26/23 13:591.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 13:59 106-93-407/26/23 13:591.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 13:59 95-50-107/26/23 13:591.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 13:59 541-73-107/26/23 13:591.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 13:59 106-46-707/26/23 13:591.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 13:59 107-06-207/26/23 13:590.810 0.283 1 1,1-Dichloroethane 0.323J ug/m3 07/26/23 13:59 75-34-3 J07/26/23 13:590.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 13:59 75-35-407/26/23 13:590.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 13:59 156-59-207/26/23 13:590.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 13:59 156-60-507/26/23 13:590.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 13:59 78-87-507/26/23 13:590.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 13:59 10061-01-507/26/23 13:590.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 13:59 10061-02-607/26/23 13:590.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 13:59 123-91-107/26/23 13:590.721 0.300 1 Ethanol 32.4 ug/m3 07/26/23 13:59 64-17-507/26/23 13:594.71 0.500 1 Ethylbenzene 6.55 ug/m3 07/26/23 13:59 100-41-407/26/23 13:590.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 13:59 141-78-607/26/23 13:590.720 0.360 1 4-Ethyltoluene 1.70 ug/m3 07/26/23 13:59 622-96-807/26/23 13:590.982 0.384 1 Trichlorofluoromethane 26.1 ug/m3 07/26/23 13:59 75-69-407/26/23 13:591.12 0.460 1 Dichlorodifluoromethane 1.06 ug/m3 07/26/23 13:59 75-71-807/26/23 13:590.989 0.678 1 1,1,2-Trichlorotrifluoroethane 1200 ug/m3 08/02/23 19:20 76-13-108/02/23 19:2015.3 6.08 10 Dichlorotetrafluoroethane ND ug/m3 07/26/23 13:59 76-14-207/26/23 13:591.40 0.622 1 n-Heptane 31.2 ug/m3 07/26/23 13:59 142-82-507/26/23 13:590.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 13:59 87-68-307/26/23 13:596.73 1.12 1 n-Hexane 7.97 ug/m3 07/26/23 13:59 110-54-307/26/23 13:592.22 0.726 1 Isopropylbenzene (Cumene)4.43 ug/m3 07/26/23 13:59 98-82-807/26/23 13:590.983 0.382 1 Methylene Chloride ND ug/m3 07/26/23 13:59 75-09-207/26/23 13:590.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 13:59 591-78-607/26/23 13:595.11 0.544 1 2-Butanone (MEK)3.98 ug/m3 07/26/23 13:59 78-93-307/26/23 13:593.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-6 Lab ID: 92679117006 Collected: 07/21/23 13:26 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 13:59 108-10-107/26/23 13:595.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 13:59 80-62-607/26/23 13:590.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 13:59 1634-04-407/26/23 13:590.721 0.233 1 Naphthalene ND ug/m3 07/26/23 13:59 91-20-307/26/23 13:593.30 1.83 1 2-Propanol 5.51 ug/m3 07/26/23 13:59 67-63-007/26/23 13:593.07 0.649 1 Propylene ND ug/m3 07/26/23 13:59 115-07-107/26/23 13:592.15 0.160 1 Styrene 0.966 ug/m3 07/26/23 13:59 100-42-507/26/23 13:590.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 13:59 79-34-507/26/23 13:591.37 0.511 1 Tetrachloroethene 88.9 ug/m3 07/26/23 13:59 127-18-407/26/23 13:591.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 13:59 109-99-907/26/23 13:590.590 0.216 1 Toluene 67.4 ug/m3 07/26/23 13:59 108-88-307/26/23 13:591.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 13:59 120-82-107/26/23 13:594.66 1.10 1 1,1,1-Trichloroethane 1.51 ug/m3 07/26/23 13:59 71-55-607/26/23 13:591.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 13:59 79-00-507/26/23 13:591.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 13:59 79-01-607/26/23 13:591.07 0.364 1 1,2,4-Trimethylbenzene 6.82 ug/m3 07/26/23 13:59 95-63-607/26/23 13:590.982 0.375 1 1,3,5-Trimethylbenzene 1.63 ug/m3 07/26/23 13:59 108-67-807/26/23 13:590.982 0.382 1 2,2,4-Trimethylpentane 19.3 ug/m3 07/26/23 13:59 540-84-107/26/23 13:590.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 13:59 75-01-407/26/23 13:590.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 13:59 593-60-207/26/23 13:590.875 0.373 1 Vinyl acetate 8.13 ug/m3 07/26/23 13:59 108-05-407/26/23 13:590.704 0.408 1 m&p-Xylene 20.3 ug/m3 07/26/23 13:59 179601-23-107/26/23 13:591.73 0.585 1 o-Xylene 8.06 ug/m3 07/26/23 13:59 95-47-607/26/23 13:590.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)106 %07/26/23 13:59 460-00-407/26/23 13:5960.0-140 1 4-Bromofluorobenzene (S)92.6 %08/02/23 19:20 460-00-408/02/23 19:2060.0-140 10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-7 Lab ID: 92679117007 Collected: 07/21/23 14:02 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 34.9 ug/m3 07/26/23 14:28 67-64-107/26/23 14:282.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 14:28 107-05-107/26/23 14:280.626 0.357 1 Benzene 15.9 ug/m3 07/26/23 14:28 71-43-207/26/23 14:280.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 14:28 100-44-707/26/23 14:281.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 14:28 75-27-407/26/23 14:281.34 0.471 1 Bromoform ND ug/m3 07/26/23 14:28 75-25-207/26/23 14:286.21 0.757 1 Bromomethane ND ug/m3 07/26/23 14:28 74-83-907/26/23 14:280.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 14:28 106-99-007/26/23 14:284.43 0.230 1 Carbon disulfide 34.2 ug/m3 07/26/23 14:28 75-15-007/26/23 14:280.622 0.317 1 Carbon tetrachloride 0.585J ug/m3 07/26/23 14:28 56-23-5 J07/26/23 14:281.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 14:28 108-90-707/26/23 14:280.924 0.385 1 Chloroethane 0.327J ug/m3 07/26/23 14:28 75-00-3 J07/26/23 14:280.528 0.263 1 Chloroform 1.33 ug/m3 07/26/23 14:28 67-66-307/26/23 14:280.973 0.349 1 Chloromethane 1.68 ug/m3 07/26/23 14:28 74-87-307/26/23 14:280.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 14:28 95-49-807/26/23 14:281.03 0.427 1 Cyclohexane 11.2 ug/m3 07/26/23 14:28 110-82-707/26/23 14:280.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 14:28 124-48-107/26/23 14:281.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 14:28 106-93-407/26/23 14:281.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 14:28 95-50-107/26/23 14:281.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 14:28 541-73-107/26/23 14:281.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 14:28 106-46-707/26/23 14:281.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 14:28 107-06-207/26/23 14:280.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 14:28 75-34-307/26/23 14:280.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 14:28 75-35-407/26/23 14:280.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 14:28 156-59-207/26/23 14:280.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 14:28 156-60-507/26/23 14:280.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 14:28 78-87-507/26/23 14:280.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 14:28 10061-01-507/26/23 14:280.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 14:28 10061-02-607/26/23 14:280.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 14:28 123-91-107/26/23 14:280.721 0.300 1 Ethanol 25.3 ug/m3 07/26/23 14:28 64-17-507/26/23 14:284.71 0.500 1 Ethylbenzene 11.7 ug/m3 07/26/23 14:28 100-41-407/26/23 14:280.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 14:28 141-78-607/26/23 14:280.720 0.360 1 4-Ethyltoluene 2.46 ug/m3 07/26/23 14:28 622-96-807/26/23 14:280.982 0.384 1 Trichlorofluoromethane 2.03 ug/m3 07/26/23 14:28 75-69-407/26/23 14:281.12 0.460 1 Dichlorodifluoromethane 2.00 ug/m3 07/26/23 14:28 75-71-807/26/23 14:280.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 14:28 76-13-107/26/23 14:281.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 14:28 76-14-207/26/23 14:281.40 0.622 1 n-Heptane 56.4 ug/m3 07/26/23 14:28 142-82-507/26/23 14:280.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 14:28 87-68-307/26/23 14:286.73 1.12 1 n-Hexane 23.1 ug/m3 07/26/23 14:28 110-54-307/26/23 14:282.22 0.726 1 Isopropylbenzene (Cumene)1.21 ug/m3 07/26/23 14:28 98-82-807/26/23 14:280.983 0.382 1 Methylene Chloride 1.14 ug/m3 07/26/23 14:28 75-09-207/26/23 14:280.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 14:28 591-78-607/26/23 14:285.11 0.544 1 2-Butanone (MEK)4.42 ug/m3 07/26/23 14:28 78-93-307/26/23 14:283.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-7 Lab ID: 92679117007 Collected: 07/21/23 14:02 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 14:28 108-10-107/26/23 14:285.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 14:28 80-62-607/26/23 14:280.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 14:28 1634-04-407/26/23 14:280.721 0.233 1 Naphthalene ND ug/m3 07/26/23 14:28 91-20-307/26/23 14:283.30 1.83 1 2-Propanol 5.41 ug/m3 07/26/23 14:28 67-63-007/26/23 14:283.07 0.649 1 Propylene 16.1 ug/m3 07/26/23 14:28 115-07-107/26/23 14:282.15 0.160 1 Styrene 0.506J ug/m3 07/26/23 14:28 100-42-5 J07/26/23 14:280.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 14:28 79-34-507/26/23 14:281.37 0.511 1 Tetrachloroethene 94.4 ug/m3 07/26/23 14:28 127-18-407/26/23 14:281.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 14:28 109-99-907/26/23 14:280.590 0.216 1 Toluene 112 ug/m3 07/26/23 14:28 108-88-307/26/23 14:281.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 14:28 120-82-107/26/23 14:284.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 14:28 71-55-607/26/23 14:281.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 14:28 79-00-507/26/23 14:281.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 14:28 79-01-607/26/23 14:281.07 0.364 1 1,2,4-Trimethylbenzene 8.83 ug/m3 07/26/23 14:28 95-63-607/26/23 14:280.982 0.375 1 1,3,5-Trimethylbenzene 2.44 ug/m3 07/26/23 14:28 108-67-807/26/23 14:280.982 0.382 1 2,2,4-Trimethylpentane 51.4 ug/m3 07/26/23 14:28 540-84-107/26/23 14:280.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 14:28 75-01-407/26/23 14:280.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 14:28 593-60-207/26/23 14:280.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 14:28 108-05-407/26/23 14:280.704 0.408 1 m&p-Xylene 34.6 ug/m3 07/26/23 14:28 179601-23-107/26/23 14:281.73 0.585 1 o-Xylene 12.4 ug/m3 07/26/23 14:28 95-47-607/26/23 14:280.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)105 %07/26/23 14:28 460-00-407/26/23 14:2860.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-8 Lab ID: 92679117008 Collected: 07/21/23 13:25 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 51.8 ug/m3 07/26/23 14:56 67-64-107/26/23 14:562.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 14:56 107-05-107/26/23 14:560.626 0.357 1 Benzene 31.7 ug/m3 07/26/23 14:56 71-43-207/26/23 14:560.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 14:56 100-44-707/26/23 14:561.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 14:56 75-27-407/26/23 14:561.34 0.471 1 Bromoform ND ug/m3 07/26/23 14:56 75-25-207/26/23 14:566.21 0.757 1 Bromomethane ND ug/m3 07/26/23 14:56 74-83-907/26/23 14:560.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 14:56 106-99-007/26/23 14:564.43 0.230 1 Carbon disulfide 77.8 ug/m3 07/26/23 14:56 75-15-007/26/23 14:560.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 14:56 56-23-507/26/23 14:561.26 0.461 1 Chlorobenzene 0.568J ug/m3 07/26/23 14:56 108-90-7 J07/26/23 14:560.924 0.385 1 Chloroethane 0.353J ug/m3 07/26/23 14:56 75-00-3 J07/26/23 14:560.528 0.263 1 Chloroform 6.91 ug/m3 07/26/23 14:56 67-66-307/26/23 14:560.973 0.349 1 Chloromethane 0.717 ug/m3 07/26/23 14:56 74-87-307/26/23 14:560.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 14:56 95-49-807/26/23 14:561.03 0.427 1 Cyclohexane 16.5 ug/m3 07/26/23 14:56 110-82-707/26/23 14:560.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 14:56 124-48-107/26/23 14:561.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 14:56 106-93-407/26/23 14:561.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 14:56 95-50-107/26/23 14:561.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 14:56 541-73-107/26/23 14:561.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 14:56 106-46-707/26/23 14:561.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 14:56 107-06-207/26/23 14:560.810 0.283 1 1,1-Dichloroethane 0.513J ug/m3 07/26/23 14:56 75-34-3 J07/26/23 14:560.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 14:56 75-35-407/26/23 14:560.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 14:56 156-59-207/26/23 14:560.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 14:56 156-60-507/26/23 14:560.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 14:56 78-87-507/26/23 14:560.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 14:56 10061-01-507/26/23 14:560.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 14:56 10061-02-607/26/23 14:560.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 14:56 123-91-107/26/23 14:560.721 0.300 1 Ethanol 32.1 ug/m3 07/26/23 14:56 64-17-507/26/23 14:564.71 0.500 1 Ethylbenzene 21.1 ug/m3 07/26/23 14:56 100-41-407/26/23 14:560.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 14:56 141-78-607/26/23 14:560.720 0.360 1 4-Ethyltoluene 3.21 ug/m3 07/26/23 14:56 622-96-807/26/23 14:560.982 0.384 1 Trichlorofluoromethane 487 ug/m3 08/03/23 11:37 75-69-408/03/23 11:3711.2 4.60 10 Dichlorodifluoromethane 1.86 ug/m3 07/26/23 14:56 75-71-807/26/23 14:560.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 14:56 76-13-107/26/23 14:561.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 14:56 76-14-207/26/23 14:561.40 0.622 1 n-Heptane 113 ug/m3 07/26/23 14:56 142-82-507/26/23 14:560.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 14:56 87-68-307/26/23 14:566.73 1.12 1 n-Hexane 98.0 ug/m3 07/26/23 14:56 110-54-307/26/23 14:562.22 0.726 1 Isopropylbenzene (Cumene)2.50 ug/m3 07/26/23 14:56 98-82-807/26/23 14:560.983 0.382 1 Methylene Chloride 1.51 ug/m3 07/26/23 14:56 75-09-207/26/23 14:560.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 14:56 591-78-607/26/23 14:565.11 0.544 1 2-Butanone (MEK)7.55 ug/m3 07/26/23 14:56 78-93-307/26/23 14:563.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-8 Lab ID: 92679117008 Collected: 07/21/23 13:25 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 14:56 108-10-107/26/23 14:565.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 14:56 80-62-607/26/23 14:560.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 14:56 1634-04-407/26/23 14:560.721 0.233 1 Naphthalene ND ug/m3 07/26/23 14:56 91-20-307/26/23 14:563.30 1.83 1 2-Propanol ND ug/m3 07/26/23 14:56 67-63-007/26/23 14:563.07 0.649 1 Propylene 84.2 ug/m3 07/26/23 14:56 115-07-107/26/23 14:562.15 0.160 1 Styrene 1.82 ug/m3 07/26/23 14:56 100-42-507/26/23 14:560.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 14:56 79-34-507/26/23 14:561.37 0.511 1 Tetrachloroethene 227 ug/m3 07/26/23 14:56 127-18-407/26/23 14:561.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 14:56 109-99-907/26/23 14:560.590 0.216 1 Toluene 182 ug/m3 07/26/23 14:56 108-88-307/26/23 14:561.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 14:56 120-82-107/26/23 14:564.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 14:56 71-55-607/26/23 14:561.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 14:56 79-00-507/26/23 14:561.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 14:56 79-01-607/26/23 14:561.07 0.364 1 1,2,4-Trimethylbenzene 11.6 ug/m3 07/26/23 14:56 95-63-607/26/23 14:560.982 0.375 1 1,3,5-Trimethylbenzene 3.96 ug/m3 07/26/23 14:56 108-67-807/26/23 14:560.982 0.382 1 2,2,4-Trimethylpentane 94.8 ug/m3 07/26/23 14:56 540-84-107/26/23 14:560.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 14:56 75-01-407/26/23 14:560.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 14:56 593-60-207/26/23 14:560.875 0.373 1 Vinyl acetate 74.3 ug/m3 07/26/23 14:56 108-05-407/26/23 14:560.704 0.408 1 m&p-Xylene 65.5 ug/m3 07/26/23 14:56 179601-23-107/26/23 14:561.73 0.585 1 o-Xylene 22.3 ug/m3 07/26/23 14:56 95-47-607/26/23 14:560.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)108 %07/26/23 14:56 460-00-407/26/23 14:5660.0-140 1 4-Bromofluorobenzene (S)97.7 %08/03/23 11:37 460-00-408/03/23 11:3760.0-140 10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-9 Lab ID: 92679117009 Collected: 07/21/23 11:30 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 54.7 ug/m3 07/26/23 15:24 67-64-107/26/23 15:242.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 15:24 107-05-107/26/23 15:240.626 0.357 1 Benzene 53.7 ug/m3 07/26/23 15:24 71-43-207/26/23 15:240.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 15:24 100-44-707/26/23 15:241.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 15:24 75-27-407/26/23 15:241.34 0.471 1 Bromoform ND ug/m3 07/26/23 15:24 75-25-207/26/23 15:246.21 0.757 1 Bromomethane ND ug/m3 07/26/23 15:24 74-83-907/26/23 15:240.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 15:24 106-99-007/26/23 15:244.43 0.230 1 Carbon disulfide 183 ug/m3 07/26/23 15:24 75-15-007/26/23 15:240.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 15:24 56-23-507/26/23 15:241.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 15:24 108-90-707/26/23 15:240.924 0.385 1 Chloroethane 0.351J ug/m3 07/26/23 15:24 75-00-3 J07/26/23 15:240.528 0.263 1 Chloroform 11.0 ug/m3 07/26/23 15:24 67-66-307/26/23 15:240.973 0.349 1 Chloromethane 0.872 ug/m3 07/26/23 15:24 74-87-307/26/23 15:240.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 15:24 95-49-807/26/23 15:241.03 0.427 1 Cyclohexane 54.4 ug/m3 07/26/23 15:24 110-82-707/26/23 15:240.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 15:24 124-48-107/26/23 15:241.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 15:24 106-93-407/26/23 15:241.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 15:24 95-50-107/26/23 15:241.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 15:24 541-73-107/26/23 15:241.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 15:24 106-46-707/26/23 15:241.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 15:24 107-06-207/26/23 15:240.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 15:24 75-34-307/26/23 15:240.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 15:24 75-35-407/26/23 15:240.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 15:24 156-59-207/26/23 15:240.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 15:24 156-60-507/26/23 15:240.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 15:24 78-87-507/26/23 15:240.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 15:24 10061-01-507/26/23 15:240.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 15:24 10061-02-607/26/23 15:240.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 15:24 123-91-107/26/23 15:240.721 0.300 1 Ethanol 76.9 ug/m3 07/26/23 15:24 64-17-507/26/23 15:244.71 0.500 1 Ethylbenzene 43.8 ug/m3 07/26/23 15:24 100-41-407/26/23 15:240.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 15:24 141-78-607/26/23 15:240.720 0.360 1 4-Ethyltoluene 7.21 ug/m3 07/26/23 15:24 622-96-807/26/23 15:240.982 0.384 1 Trichlorofluoromethane 10.7 ug/m3 07/26/23 15:24 75-69-407/26/23 15:241.12 0.460 1 Dichlorodifluoromethane 1.90 ug/m3 07/26/23 15:24 75-71-807/26/23 15:240.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 15:24 76-13-107/26/23 15:241.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 15:24 76-14-207/26/23 15:241.40 0.622 1 n-Heptane 275 ug/m3 07/26/23 15:24 142-82-507/26/23 15:240.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 15:24 87-68-307/26/23 15:246.73 1.12 1 n-Hexane 106 ug/m3 07/26/23 15:24 110-54-307/26/23 15:242.22 0.726 1 Isopropylbenzene (Cumene)14.9 ug/m3 07/26/23 15:24 98-82-807/26/23 15:240.983 0.382 1 Methylene Chloride 1.50 ug/m3 07/26/23 15:24 75-09-207/26/23 15:240.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 15:24 591-78-607/26/23 15:245.11 0.544 1 2-Butanone (MEK)10.5 ug/m3 07/26/23 15:24 78-93-307/26/23 15:243.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-9 Lab ID: 92679117009 Collected: 07/21/23 11:30 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 15:24 108-10-107/26/23 15:245.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 15:24 80-62-607/26/23 15:240.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 15:24 1634-04-407/26/23 15:240.721 0.233 1 Naphthalene ND ug/m3 07/26/23 15:24 91-20-307/26/23 15:243.30 1.83 1 2-Propanol 9.29 ug/m3 07/26/23 15:24 67-63-007/26/23 15:243.07 0.649 1 Propylene 52.0 ug/m3 07/26/23 15:24 115-07-107/26/23 15:242.15 0.160 1 Styrene 2.18 ug/m3 07/26/23 15:24 100-42-507/26/23 15:240.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 15:24 79-34-507/26/23 15:241.37 0.511 1 Tetrachloroethene 384 ug/m3 07/26/23 15:24 127-18-407/26/23 15:241.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 15:24 109-99-907/26/23 15:240.590 0.216 1 Toluene 372 ug/m3 07/26/23 15:24 108-88-307/26/23 15:241.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 15:24 120-82-107/26/23 15:244.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 15:24 71-55-607/26/23 15:241.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 15:24 79-00-507/26/23 15:241.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 15:24 79-01-607/26/23 15:241.07 0.364 1 1,2,4-Trimethylbenzene 26.8 ug/m3 07/26/23 15:24 95-63-607/26/23 15:240.982 0.375 1 1,3,5-Trimethylbenzene 7.75 ug/m3 07/26/23 15:24 108-67-807/26/23 15:240.982 0.382 1 2,2,4-Trimethylpentane 221 ug/m3 07/26/23 15:24 540-84-107/26/23 15:240.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 15:24 75-01-407/26/23 15:240.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 15:24 593-60-207/26/23 15:240.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 15:24 108-05-407/26/23 15:240.704 0.408 1 m&p-Xylene 124 ug/m3 07/26/23 15:24 179601-23-107/26/23 15:241.73 0.585 1 o-Xylene 47.3 ug/m3 07/26/23 15:24 95-47-607/26/23 15:240.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)108 %07/26/23 15:24 460-00-407/26/23 15:2460.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-10 Lab ID: 92679117010 Collected: 07/21/23 11:26 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 30.4 ug/m3 07/26/23 15:52 67-64-107/26/23 15:522.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 15:52 107-05-107/26/23 15:520.626 0.357 1 Benzene 77.3 ug/m3 07/26/23 15:52 71-43-207/26/23 15:520.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 15:52 100-44-707/26/23 15:521.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 15:52 75-27-407/26/23 15:521.34 0.471 1 Bromoform ND ug/m3 07/26/23 15:52 75-25-207/26/23 15:526.21 0.757 1 Bromomethane ND ug/m3 07/26/23 15:52 74-83-907/26/23 15:520.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 15:52 106-99-007/26/23 15:524.43 0.230 1 Carbon disulfide 208 ug/m3 08/02/23 20:19 75-15-008/02/23 20:196.22 3.17 10 Carbon tetrachloride ND ug/m3 07/26/23 15:52 56-23-507/26/23 15:521.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 15:52 108-90-707/26/23 15:520.924 0.385 1 Chloroethane 0.372J ug/m3 07/26/23 15:52 75-00-3 J07/26/23 15:520.528 0.263 1 Chloroform 31.8 ug/m3 07/26/23 15:52 67-66-307/26/23 15:520.973 0.349 1 Chloromethane 0.568 ug/m3 07/26/23 15:52 74-87-307/26/23 15:520.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 15:52 95-49-807/26/23 15:521.03 0.427 1 Cyclohexane 38.6 ug/m3 07/26/23 15:52 110-82-707/26/23 15:520.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 15:52 124-48-107/26/23 15:521.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 15:52 106-93-407/26/23 15:521.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 15:52 95-50-107/26/23 15:521.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 15:52 541-73-107/26/23 15:521.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 15:52 106-46-707/26/23 15:521.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 15:52 107-06-207/26/23 15:520.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 15:52 75-34-307/26/23 15:520.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 15:52 75-35-407/26/23 15:520.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 15:52 156-59-207/26/23 15:520.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 15:52 156-60-507/26/23 15:520.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 15:52 78-87-507/26/23 15:520.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 15:52 10061-01-507/26/23 15:520.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 15:52 10061-02-607/26/23 15:520.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 15:52 123-91-107/26/23 15:520.721 0.300 1 Ethanol 74.3 ug/m3 07/26/23 15:52 64-17-507/26/23 15:524.71 0.500 1 Ethylbenzene 72.0 ug/m3 07/26/23 15:52 100-41-407/26/23 15:520.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 15:52 141-78-607/26/23 15:520.720 0.360 1 4-Ethyltoluene 11.4 ug/m3 07/26/23 15:52 622-96-807/26/23 15:520.982 0.384 1 Trichlorofluoromethane 2.23 ug/m3 07/26/23 15:52 75-69-407/26/23 15:521.12 0.460 1 Dichlorodifluoromethane 1.84 ug/m3 07/26/23 15:52 75-71-807/26/23 15:520.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 15:52 76-13-107/26/23 15:521.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 15:52 76-14-207/26/23 15:521.40 0.622 1 n-Heptane 386 ug/m3 08/02/23 20:19 142-82-508/02/23 20:198.18 4.25 10 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 15:52 87-68-307/26/23 15:526.73 1.12 1 n-Hexane 145 ug/m3 07/26/23 15:52 110-54-307/26/23 15:522.22 0.726 1 Isopropylbenzene (Cumene)10.1 ug/m3 07/26/23 15:52 98-82-807/26/23 15:520.983 0.382 1 Methylene Chloride 1.38 ug/m3 07/26/23 15:52 75-09-207/26/23 15:520.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 15:52 591-78-607/26/23 15:525.11 0.544 1 2-Butanone (MEK)4.04 ug/m3 07/26/23 15:52 78-93-307/26/23 15:523.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-10 Lab ID: 92679117010 Collected: 07/21/23 11:26 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 15:52 108-10-107/26/23 15:525.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 15:52 80-62-607/26/23 15:520.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 15:52 1634-04-407/26/23 15:520.721 0.233 1 Naphthalene ND ug/m3 07/26/23 15:52 91-20-307/26/23 15:523.30 1.83 1 2-Propanol 9.86 ug/m3 07/26/23 15:52 67-63-007/26/23 15:523.07 0.649 1 Propylene 55.8 ug/m3 07/26/23 15:52 115-07-107/26/23 15:522.15 0.160 1 Styrene 1.24 ug/m3 07/26/23 15:52 100-42-507/26/23 15:520.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 15:52 79-34-507/26/23 15:521.37 0.511 1 Tetrachloroethene 605 ug/m3 07/26/23 15:52 127-18-407/26/23 15:521.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 15:52 109-99-907/26/23 15:520.590 0.216 1 Toluene 505 ug/m3 08/02/23 20:19 108-88-308/02/23 20:1918.8 3.28 10 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 15:52 120-82-107/26/23 15:524.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 15:52 71-55-607/26/23 15:521.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 15:52 79-00-507/26/23 15:521.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 15:52 79-01-607/26/23 15:521.07 0.364 1 1,2,4-Trimethylbenzene 30.0 ug/m3 07/26/23 15:52 95-63-607/26/23 15:520.982 0.375 1 1,3,5-Trimethylbenzene 9.96 ug/m3 07/26/23 15:52 108-67-807/26/23 15:520.982 0.382 1 2,2,4-Trimethylpentane 307 ug/m3 07/26/23 15:52 540-84-107/26/23 15:520.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 15:52 75-01-407/26/23 15:520.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 15:52 593-60-207/26/23 15:520.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 15:52 108-05-407/26/23 15:520.704 0.408 1 m&p-Xylene 194 ug/m3 07/26/23 15:52 179601-23-107/26/23 15:521.73 0.585 1 o-Xylene 61.6 ug/m3 07/26/23 15:52 95-47-607/26/23 15:520.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)107 %07/26/23 15:52 460-00-407/26/23 15:5260.0-140 1 4-Bromofluorobenzene (S)101 %08/02/23 20:19 460-00-408/02/23 20:1960.0-140 10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-11 Lab ID: 92679117011 Collected: 07/21/23 10:05 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 17.2 ug/m3 07/26/23 16:20 67-64-107/26/23 16:202.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 16:20 107-05-107/26/23 16:200.626 0.357 1 Benzene 27.8 ug/m3 07/26/23 16:20 71-43-207/26/23 16:200.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 16:20 100-44-707/26/23 16:201.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 16:20 75-27-407/26/23 16:201.34 0.471 1 Bromoform ND ug/m3 07/26/23 16:20 75-25-207/26/23 16:206.21 0.757 1 Bromomethane ND ug/m3 07/26/23 16:20 74-83-907/26/23 16:200.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 16:20 106-99-007/26/23 16:204.43 0.230 1 Carbon disulfide ND ug/m3 07/26/23 16:20 75-15-007/26/23 16:200.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 16:20 56-23-507/26/23 16:201.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 16:20 108-90-707/26/23 16:200.924 0.385 1 Chloroethane 0.372J ug/m3 07/26/23 16:20 75-00-3 J07/26/23 16:200.528 0.263 1 Chloroform 4.74 ug/m3 07/26/23 16:20 67-66-307/26/23 16:200.973 0.349 1 Chloromethane 0.483 ug/m3 07/26/23 16:20 74-87-307/26/23 16:200.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 16:20 95-49-807/26/23 16:201.03 0.427 1 Cyclohexane 23.3 ug/m3 07/26/23 16:20 110-82-707/26/23 16:200.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 16:20 124-48-107/26/23 16:201.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 16:20 106-93-407/26/23 16:201.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 16:20 95-50-107/26/23 16:201.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 16:20 541-73-107/26/23 16:201.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 16:20 106-46-707/26/23 16:201.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 16:20 107-06-207/26/23 16:200.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 16:20 75-34-307/26/23 16:200.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 16:20 75-35-407/26/23 16:200.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 16:20 156-59-207/26/23 16:200.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 16:20 156-60-507/26/23 16:200.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 16:20 78-87-507/26/23 16:200.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 16:20 10061-01-507/26/23 16:200.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 16:20 10061-02-607/26/23 16:200.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 16:20 123-91-107/26/23 16:200.721 0.300 1 Ethanol 23.9 ug/m3 07/26/23 16:20 64-17-507/26/23 16:204.71 0.500 1 Ethylbenzene 24.8 ug/m3 07/26/23 16:20 100-41-407/26/23 16:200.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 16:20 141-78-607/26/23 16:200.720 0.360 1 4-Ethyltoluene 3.95 ug/m3 07/26/23 16:20 622-96-807/26/23 16:200.982 0.384 1 Trichlorofluoromethane 9.33 ug/m3 07/26/23 16:20 75-69-407/26/23 16:201.12 0.460 1 Dichlorodifluoromethane 1.58 ug/m3 07/26/23 16:20 75-71-807/26/23 16:200.989 0.678 1 1,1,2-Trichlorotrifluoroethane 1200 ug/m3 08/02/23 20:49 76-13-108/02/23 20:4915.3 6.08 10 Dichlorotetrafluoroethane ND ug/m3 07/26/23 16:20 76-14-207/26/23 16:201.40 0.622 1 n-Heptane 344 ug/m3 07/26/23 16:20 142-82-507/26/23 16:200.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 16:20 87-68-307/26/23 16:206.73 1.12 1 n-Hexane 104 ug/m3 07/26/23 16:20 110-54-307/26/23 16:202.22 0.726 1 Isopropylbenzene (Cumene)5.01 ug/m3 07/26/23 16:20 98-82-807/26/23 16:200.983 0.382 1 Methylene Chloride ND ug/m3 07/26/23 16:20 75-09-207/26/23 16:200.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 16:20 591-78-607/26/23 16:205.11 0.544 1 2-Butanone (MEK)2.82J ug/m3 07/26/23 16:20 78-93-3 J07/26/23 16:203.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-11 Lab ID: 92679117011 Collected: 07/21/23 10:05 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 16:20 108-10-107/26/23 16:205.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 16:20 80-62-607/26/23 16:200.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 16:20 1634-04-407/26/23 16:200.721 0.233 1 Naphthalene ND ug/m3 07/26/23 16:20 91-20-307/26/23 16:203.30 1.83 1 2-Propanol 4.52 ug/m3 07/26/23 16:20 67-63-007/26/23 16:203.07 0.649 1 Propylene 27.4 ug/m3 07/26/23 16:20 115-07-107/26/23 16:202.15 0.160 1 Styrene 0.944 ug/m3 07/26/23 16:20 100-42-507/26/23 16:200.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 16:20 79-34-507/26/23 16:201.37 0.511 1 Tetrachloroethene 273 ug/m3 07/26/23 16:20 127-18-407/26/23 16:201.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 16:20 109-99-907/26/23 16:200.590 0.216 1 Toluene 209 ug/m3 07/26/23 16:20 108-88-307/26/23 16:201.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 16:20 120-82-107/26/23 16:204.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 16:20 71-55-607/26/23 16:201.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 16:20 79-00-507/26/23 16:201.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 16:20 79-01-607/26/23 16:201.07 0.364 1 1,2,4-Trimethylbenzene 10.7 ug/m3 07/26/23 16:20 95-63-607/26/23 16:200.982 0.375 1 1,3,5-Trimethylbenzene 3.50 ug/m3 07/26/23 16:20 108-67-807/26/23 16:200.982 0.382 1 2,2,4-Trimethylpentane 221 ug/m3 07/26/23 16:20 540-84-107/26/23 16:200.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 16:20 75-01-407/26/23 16:200.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 16:20 593-60-207/26/23 16:200.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 16:20 108-05-407/26/23 16:200.704 0.408 1 m&p-Xylene 68.5 ug/m3 07/26/23 16:20 179601-23-107/26/23 16:201.73 0.585 1 o-Xylene 22.1 ug/m3 07/26/23 16:20 95-47-607/26/23 16:200.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)107 %07/26/23 16:20 460-00-407/26/23 16:2060.0-140 1 4-Bromofluorobenzene (S)97.0 %08/02/23 20:49 460-00-408/02/23 20:4960.0-140 10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-12 Lab ID: 92679117012 Collected: 07/21/23 09:52 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 28.8 ug/m3 07/26/23 17:19 67-64-107/26/23 17:192.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 17:19 107-05-107/26/23 17:190.626 0.357 1 Benzene 25.7 ug/m3 07/26/23 17:19 71-43-207/26/23 17:190.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 17:19 100-44-707/26/23 17:191.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 17:19 75-27-407/26/23 17:191.34 0.471 1 Bromoform ND ug/m3 07/26/23 17:19 75-25-207/26/23 17:196.21 0.757 1 Bromomethane ND ug/m3 07/26/23 17:19 74-83-907/26/23 17:190.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 17:19 106-99-007/26/23 17:194.43 0.230 1 Carbon disulfide 201 ug/m3 07/26/23 17:19 75-15-007/26/23 17:190.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 17:19 56-23-507/26/23 17:191.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 17:19 108-90-707/26/23 17:190.924 0.385 1 Chloroethane 0.514J ug/m3 07/26/23 17:19 75-00-3 J07/26/23 17:190.528 0.263 1 Chloroform 4.08 ug/m3 07/26/23 17:19 67-66-307/26/23 17:190.973 0.349 1 Chloromethane 0.671 ug/m3 07/26/23 17:19 74-87-307/26/23 17:190.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 17:19 95-49-807/26/23 17:191.03 0.427 1 Cyclohexane 23.7 ug/m3 07/26/23 17:19 110-82-707/26/23 17:190.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 17:19 124-48-107/26/23 17:191.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 17:19 106-93-407/26/23 17:191.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 17:19 95-50-107/26/23 17:191.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 17:19 541-73-107/26/23 17:191.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 17:19 106-46-707/26/23 17:191.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 17:19 107-06-207/26/23 17:190.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 17:19 75-34-307/26/23 17:190.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 17:19 75-35-407/26/23 17:190.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 17:19 156-59-207/26/23 17:190.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 17:19 156-60-507/26/23 17:190.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 17:19 78-87-507/26/23 17:190.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 17:19 10061-01-507/26/23 17:190.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 17:19 10061-02-607/26/23 17:190.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 17:19 123-91-107/26/23 17:190.721 0.300 1 Ethanol 70.0 ug/m3 07/26/23 17:19 64-17-507/26/23 17:194.71 0.500 1 Ethylbenzene 25.3 ug/m3 07/26/23 17:19 100-41-407/26/23 17:190.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 17:19 141-78-607/26/23 17:190.720 0.360 1 4-Ethyltoluene 3.71 ug/m3 07/26/23 17:19 622-96-807/26/23 17:190.982 0.384 1 Trichlorofluoromethane 2.17 ug/m3 07/26/23 17:19 75-69-407/26/23 17:191.12 0.460 1 Dichlorodifluoromethane 2.64 ug/m3 07/26/23 17:19 75-71-807/26/23 17:190.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 17:19 76-13-107/26/23 17:191.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 17:19 76-14-207/26/23 17:191.40 0.622 1 n-Heptane 355 ug/m3 07/26/23 17:19 142-82-507/26/23 17:190.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 17:19 87-68-307/26/23 17:196.73 1.12 1 n-Hexane 94.8 ug/m3 07/26/23 17:19 110-54-307/26/23 17:192.22 0.726 1 Isopropylbenzene (Cumene)5.41 ug/m3 07/26/23 17:19 98-82-807/26/23 17:190.983 0.382 1 Methylene Chloride 2.97 ug/m3 07/26/23 17:19 75-09-207/26/23 17:190.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 17:19 591-78-607/26/23 17:195.11 0.544 1 2-Butanone (MEK)ND ug/m3 07/26/23 17:19 78-93-307/26/23 17:193.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-12 Lab ID: 92679117012 Collected: 07/21/23 09:52 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 17:19 108-10-107/26/23 17:195.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 17:19 80-62-607/26/23 17:190.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 17:19 1634-04-407/26/23 17:190.721 0.233 1 Naphthalene ND ug/m3 07/26/23 17:19 91-20-307/26/23 17:193.30 1.83 1 2-Propanol 17.1 ug/m3 07/26/23 17:19 67-63-007/26/23 17:193.07 0.649 1 Propylene 53.0 ug/m3 07/26/23 17:19 115-07-107/26/23 17:192.15 0.160 1 Styrene 1.15 ug/m3 07/26/23 17:19 100-42-507/26/23 17:190.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 17:19 79-34-507/26/23 17:191.37 0.511 1 Tetrachloroethene 226 ug/m3 07/26/23 17:19 127-18-407/26/23 17:191.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 17:19 109-99-907/26/23 17:190.590 0.216 1 Toluene 213 ug/m3 07/26/23 17:19 108-88-307/26/23 17:191.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 17:19 120-82-107/26/23 17:194.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 17:19 71-55-607/26/23 17:191.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 17:19 79-00-507/26/23 17:191.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 17:19 79-01-607/26/23 17:191.07 0.364 1 1,2,4-Trimethylbenzene 11.8 ug/m3 07/26/23 17:19 95-63-607/26/23 17:190.982 0.375 1 1,3,5-Trimethylbenzene 3.71 ug/m3 07/26/23 17:19 108-67-807/26/23 17:190.982 0.382 1 2,2,4-Trimethylpentane 212 ug/m3 07/26/23 17:19 540-84-107/26/23 17:190.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 17:19 75-01-407/26/23 17:190.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 17:19 593-60-207/26/23 17:190.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 17:19 108-05-407/26/23 17:190.704 0.408 1 m&p-Xylene 65.0 ug/m3 07/26/23 17:19 179601-23-107/26/23 17:191.73 0.585 1 o-Xylene 20.0 ug/m3 07/26/23 17:19 95-47-607/26/23 17:190.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)107 %07/26/23 17:19 460-00-407/26/23 17:1960.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-13 Lab ID: 92679117013 Collected: 07/21/23 09:27 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 30.7 ug/m3 07/26/23 17:47 67-64-107/26/23 17:472.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 17:47 107-05-107/26/23 17:470.626 0.357 1 Benzene 28.9 ug/m3 07/26/23 17:47 71-43-207/26/23 17:470.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 17:47 100-44-707/26/23 17:471.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 17:47 75-27-407/26/23 17:471.34 0.471 1 Bromoform ND ug/m3 07/26/23 17:47 75-25-207/26/23 17:476.21 0.757 1 Bromomethane ND ug/m3 07/26/23 17:47 74-83-907/26/23 17:470.776 0.381 1 1,3-Butadiene 1.88J ug/m3 07/26/23 17:47 106-99-0 J07/26/23 17:474.43 0.230 1 Carbon disulfide ND ug/m3 07/26/23 17:47 75-15-007/26/23 17:470.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 17:47 56-23-507/26/23 17:471.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 17:47 108-90-707/26/23 17:470.924 0.385 1 Chloroethane ND ug/m3 07/26/23 17:47 75-00-307/26/23 17:470.528 0.263 1 Chloroform 19.7 ug/m3 07/26/23 17:47 67-66-307/26/23 17:470.973 0.349 1 Chloromethane 0.500 ug/m3 07/26/23 17:47 74-87-307/26/23 17:470.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 17:47 95-49-807/26/23 17:471.03 0.427 1 Cyclohexane 17.9 ug/m3 07/26/23 17:47 110-82-707/26/23 17:470.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 17:47 124-48-107/26/23 17:471.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 17:47 106-93-407/26/23 17:471.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 17:47 95-50-107/26/23 17:471.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 17:47 541-73-107/26/23 17:471.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 17:47 106-46-707/26/23 17:471.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 17:47 107-06-207/26/23 17:470.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 17:47 75-34-307/26/23 17:470.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 17:47 75-35-407/26/23 17:470.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 17:47 156-59-207/26/23 17:470.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 17:47 156-60-507/26/23 17:470.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 17:47 78-87-507/26/23 17:470.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 17:47 10061-01-507/26/23 17:470.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 17:47 10061-02-607/26/23 17:470.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 17:47 123-91-107/26/23 17:470.721 0.300 1 Ethanol 33.9 ug/m3 07/26/23 17:47 64-17-507/26/23 17:474.71 0.500 1 Ethylbenzene 27.7 ug/m3 07/26/23 17:47 100-41-407/26/23 17:470.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 17:47 141-78-607/26/23 17:470.720 0.360 1 4-Ethyltoluene 4.09 ug/m3 07/26/23 17:47 622-96-807/26/23 17:470.982 0.384 1 Trichlorofluoromethane 3.43 ug/m3 07/26/23 17:47 75-69-407/26/23 17:471.12 0.460 1 Dichlorodifluoromethane 1.85 ug/m3 07/26/23 17:47 75-71-807/26/23 17:470.989 0.678 1 1,1,2-Trichlorotrifluoroethane 600 ug/m3 07/26/23 17:47 76-13-107/26/23 17:471.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 17:47 76-14-207/26/23 17:471.40 0.622 1 n-Heptane 252 ug/m3 07/26/23 17:47 142-82-507/26/23 17:470.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 17:47 87-68-307/26/23 17:476.73 1.12 1 n-Hexane 70.9 ug/m3 07/26/23 17:47 110-54-307/26/23 17:472.22 0.726 1 Isopropylbenzene (Cumene)5.41 ug/m3 07/26/23 17:47 98-82-807/26/23 17:470.983 0.382 1 Methylene Chloride 1.73 ug/m3 07/26/23 17:47 75-09-207/26/23 17:470.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 17:47 591-78-607/26/23 17:475.11 0.544 1 2-Butanone (MEK)6.72 ug/m3 07/26/23 17:47 78-93-307/26/23 17:473.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 29 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-13 Lab ID: 92679117013 Collected: 07/21/23 09:27 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 17:47 108-10-107/26/23 17:475.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 17:47 80-62-607/26/23 17:470.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 17:47 1634-04-407/26/23 17:470.721 0.233 1 Naphthalene ND ug/m3 07/26/23 17:47 91-20-307/26/23 17:473.30 1.83 1 2-Propanol 5.46 ug/m3 07/26/23 17:47 67-63-007/26/23 17:473.07 0.649 1 Propylene 22.0 ug/m3 07/26/23 17:47 115-07-107/26/23 17:472.15 0.160 1 Styrene 0.863 ug/m3 07/26/23 17:47 100-42-507/26/23 17:470.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 17:47 79-34-507/26/23 17:471.37 0.511 1 Tetrachloroethene 284 ug/m3 07/26/23 17:47 127-18-407/26/23 17:471.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 17:47 109-99-907/26/23 17:470.590 0.216 1 Toluene 241 ug/m3 07/26/23 17:47 108-88-307/26/23 17:471.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 17:47 120-82-107/26/23 17:474.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 17:47 71-55-607/26/23 17:471.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 17:47 79-00-507/26/23 17:471.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 17:47 79-01-607/26/23 17:471.07 0.364 1 1,2,4-Trimethylbenzene 11.6 ug/m3 07/26/23 17:47 95-63-607/26/23 17:470.982 0.375 1 1,3,5-Trimethylbenzene 3.79 ug/m3 07/26/23 17:47 108-67-807/26/23 17:470.982 0.382 1 2,2,4-Trimethylpentane 168 ug/m3 07/26/23 17:47 540-84-107/26/23 17:470.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 17:47 75-01-407/26/23 17:470.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 17:47 593-60-207/26/23 17:470.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 17:47 108-05-407/26/23 17:470.704 0.408 1 m&p-Xylene 75.4 ug/m3 07/26/23 17:47 179601-23-107/26/23 17:471.73 0.585 1 o-Xylene 25.5 ug/m3 07/26/23 17:47 95-47-607/26/23 17:470.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)106 %07/26/23 17:47 460-00-407/26/23 17:4760.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 30 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-14 Lab ID: 92679117014 Collected: 07/21/23 09:00 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 17.8 ug/m3 07/26/23 18:16 67-64-107/26/23 18:162.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 18:16 107-05-107/26/23 18:160.626 0.357 1 Benzene 68.4 ug/m3 07/26/23 18:16 71-43-207/26/23 18:160.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 18:16 100-44-707/26/23 18:161.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 18:16 75-27-407/26/23 18:161.34 0.471 1 Bromoform ND ug/m3 07/26/23 18:16 75-25-207/26/23 18:166.21 0.757 1 Bromomethane ND ug/m3 07/26/23 18:16 74-83-907/26/23 18:160.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 18:16 106-99-007/26/23 18:164.43 0.230 1 Carbon disulfide 166 ug/m3 07/26/23 18:16 75-15-007/26/23 18:160.622 0.317 1 Carbon tetrachloride 0.642J ug/m3 07/26/23 18:16 56-23-5 J07/26/23 18:161.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 18:16 108-90-707/26/23 18:160.924 0.385 1 Chloroethane 0.493J ug/m3 07/26/23 18:16 75-00-3 J07/26/23 18:160.528 0.263 1 Chloroform 43.0 ug/m3 07/26/23 18:16 67-66-307/26/23 18:160.973 0.349 1 Chloromethane 0.341J ug/m3 07/26/23 18:16 74-87-3 J07/26/23 18:160.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 18:16 95-49-807/26/23 18:161.03 0.427 1 Cyclohexane 27.2 ug/m3 07/26/23 18:16 110-82-707/26/23 18:160.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 18:16 124-48-107/26/23 18:161.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 18:16 106-93-407/26/23 18:161.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 18:16 95-50-107/26/23 18:161.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 18:16 541-73-107/26/23 18:161.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 18:16 106-46-707/26/23 18:161.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 18:16 107-06-207/26/23 18:160.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 18:16 75-34-307/26/23 18:160.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 18:16 75-35-407/26/23 18:160.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 18:16 156-59-207/26/23 18:160.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 18:16 156-60-507/26/23 18:160.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 18:16 78-87-507/26/23 18:160.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 18:16 10061-01-507/26/23 18:160.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 18:16 10061-02-607/26/23 18:160.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 18:16 123-91-107/26/23 18:160.721 0.300 1 Ethanol 15.0 ug/m3 07/26/23 18:16 64-17-507/26/23 18:164.71 0.500 1 Ethylbenzene 68.1 ug/m3 07/26/23 18:16 100-41-407/26/23 18:160.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 18:16 141-78-607/26/23 18:160.720 0.360 1 4-Ethyltoluene 12.7 ug/m3 07/26/23 18:16 622-96-807/26/23 18:160.982 0.384 1 Trichlorofluoromethane 1.57 ug/m3 07/26/23 18:16 75-69-407/26/23 18:161.12 0.460 1 Dichlorodifluoromethane ND ug/m3 07/26/23 18:16 75-71-807/26/23 18:160.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 18:16 76-13-107/26/23 18:161.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 18:16 76-14-207/26/23 18:161.40 0.622 1 n-Heptane 182 ug/m3 07/26/23 18:16 142-82-507/26/23 18:160.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 18:16 87-68-307/26/23 18:166.73 1.12 1 n-Hexane 36.7 ug/m3 07/26/23 18:16 110-54-307/26/23 18:162.22 0.726 1 Isopropylbenzene (Cumene)9.14 ug/m3 07/26/23 18:16 98-82-807/26/23 18:160.983 0.382 1 Methylene Chloride 0.990 ug/m3 07/26/23 18:16 75-09-207/26/23 18:160.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 18:16 591-78-607/26/23 18:165.11 0.544 1 2-Butanone (MEK)3.39J ug/m3 07/26/23 18:16 78-93-3 J07/26/23 18:163.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 31 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-14 Lab ID: 92679117014 Collected: 07/21/23 09:00 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 18:16 108-10-107/26/23 18:165.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 18:16 80-62-607/26/23 18:160.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 18:16 1634-04-407/26/23 18:160.721 0.233 1 Naphthalene ND ug/m3 07/26/23 18:16 91-20-307/26/23 18:163.30 1.83 1 2-Propanol 4.50 ug/m3 07/26/23 18:16 67-63-007/26/23 18:163.07 0.649 1 Propylene 7.06 ug/m3 07/26/23 18:16 115-07-107/26/23 18:162.15 0.160 1 Styrene 0.659J ug/m3 07/26/23 18:16 100-42-5 J07/26/23 18:160.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 18:16 79-34-507/26/23 18:161.37 0.511 1 Tetrachloroethene 551 ug/m3 07/26/23 18:16 127-18-407/26/23 18:161.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 18:16 109-99-907/26/23 18:160.590 0.216 1 Toluene 512 ug/m3 08/03/23 13:10 108-88-308/03/23 13:1018.8 3.28 10 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 18:16 120-82-107/26/23 18:164.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 18:16 71-55-607/26/23 18:161.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 18:16 79-00-507/26/23 18:161.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 18:16 79-01-607/26/23 18:161.07 0.364 1 1,2,4-Trimethylbenzene 35.4 ug/m3 07/26/23 18:16 95-63-607/26/23 18:160.982 0.375 1 1,3,5-Trimethylbenzene 12.4 ug/m3 07/26/23 18:16 108-67-807/26/23 18:160.982 0.382 1 2,2,4-Trimethylpentane 64.5 ug/m3 07/26/23 18:16 540-84-107/26/23 18:160.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 18:16 75-01-407/26/23 18:160.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 18:16 593-60-207/26/23 18:160.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 18:16 108-05-407/26/23 18:160.704 0.408 1 m&p-Xylene 188 ug/m3 07/26/23 18:16 179601-23-107/26/23 18:161.73 0.585 1 o-Xylene 65.0 ug/m3 07/26/23 18:16 95-47-607/26/23 18:160.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)108 %07/26/23 18:16 460-00-407/26/23 18:1660.0-140 1 4-Bromofluorobenzene (S)99.6 %08/03/23 13:10 460-00-408/03/23 13:1060.0-140 10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 32 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-15 Lab ID: 92679117015 Collected: 07/21/23 09:04 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 18.9 ug/m3 07/26/23 18:44 67-64-107/26/23 18:442.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 18:44 107-05-107/26/23 18:440.626 0.357 1 Benzene 6.04 ug/m3 07/26/23 18:44 71-43-207/26/23 18:440.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 18:44 100-44-707/26/23 18:441.04 0.311 1 Bromodichloromethane 1.39 ug/m3 07/26/23 18:44 75-27-407/26/23 18:441.34 0.471 1 Bromoform ND ug/m3 07/26/23 18:44 75-25-207/26/23 18:446.21 0.757 1 Bromomethane ND ug/m3 07/26/23 18:44 74-83-907/26/23 18:440.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 18:44 106-99-007/26/23 18:444.43 0.230 1 Carbon disulfide 6.44 ug/m3 07/26/23 18:44 75-15-007/26/23 18:440.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 18:44 56-23-507/26/23 18:441.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 18:44 108-90-707/26/23 18:440.924 0.385 1 Chloroethane ND ug/m3 07/26/23 18:44 75-00-307/26/23 18:440.528 0.263 1 Chloroform 17.1 ug/m3 07/26/23 18:44 67-66-307/26/23 18:440.973 0.349 1 Chloromethane ND ug/m3 07/26/23 18:44 74-87-307/26/23 18:440.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 18:44 95-49-807/26/23 18:441.03 0.427 1 Cyclohexane 1.35 ug/m3 07/26/23 18:44 110-82-707/26/23 18:440.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 18:44 124-48-107/26/23 18:441.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 18:44 106-93-407/26/23 18:441.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 18:44 95-50-107/26/23 18:441.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 18:44 541-73-107/26/23 18:441.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 18:44 106-46-707/26/23 18:441.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 18:44 107-06-207/26/23 18:440.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 18:44 75-34-307/26/23 18:440.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 18:44 75-35-407/26/23 18:440.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 18:44 156-59-207/26/23 18:440.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 18:44 156-60-507/26/23 18:440.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 18:44 78-87-507/26/23 18:440.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 18:44 10061-01-507/26/23 18:440.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 18:44 10061-02-607/26/23 18:440.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 18:44 123-91-107/26/23 18:440.721 0.300 1 Ethanol 36.6 ug/m3 07/26/23 18:44 64-17-507/26/23 18:444.71 0.500 1 Ethylbenzene 23.6 ug/m3 07/26/23 18:44 100-41-407/26/23 18:440.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 18:44 141-78-607/26/23 18:440.720 0.360 1 4-Ethyltoluene 6.18 ug/m3 07/26/23 18:44 622-96-807/26/23 18:440.982 0.384 1 Trichlorofluoromethane 1.35 ug/m3 07/26/23 18:44 75-69-407/26/23 18:441.12 0.460 1 Dichlorodifluoromethane 1.29 ug/m3 07/26/23 18:44 75-71-807/26/23 18:440.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 18:44 76-13-107/26/23 18:441.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 18:44 76-14-207/26/23 18:441.40 0.622 1 n-Heptane 13.2 ug/m3 07/26/23 18:44 142-82-507/26/23 18:440.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 18:44 87-68-307/26/23 18:446.73 1.12 1 n-Hexane 2.49 ug/m3 07/26/23 18:44 110-54-307/26/23 18:442.22 0.726 1 Isopropylbenzene (Cumene)3.80 ug/m3 07/26/23 18:44 98-82-807/26/23 18:440.983 0.382 1 Methylene Chloride 1.21 ug/m3 07/26/23 18:44 75-09-207/26/23 18:440.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 18:44 591-78-607/26/23 18:445.11 0.544 1 2-Butanone (MEK)2.95J ug/m3 07/26/23 18:44 78-93-3 J07/26/23 18:443.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 33 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-15 Lab ID: 92679117015 Collected: 07/21/23 09:04 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 18:44 108-10-107/26/23 18:445.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 18:44 80-62-607/26/23 18:440.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 18:44 1634-04-407/26/23 18:440.721 0.233 1 Naphthalene ND ug/m3 07/26/23 18:44 91-20-307/26/23 18:443.30 1.83 1 2-Propanol 5.48 ug/m3 07/26/23 18:44 67-63-007/26/23 18:443.07 0.649 1 Propylene ND ug/m3 07/26/23 18:44 115-07-107/26/23 18:442.15 0.160 1 Styrene 0.424J ug/m3 07/26/23 18:44 100-42-5 J07/26/23 18:440.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 18:44 79-34-507/26/23 18:441.37 0.511 1 Tetrachloroethene 109 ug/m3 07/26/23 18:44 127-18-407/26/23 18:441.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 18:44 109-99-907/26/23 18:440.590 0.216 1 Toluene 127 ug/m3 07/26/23 18:44 108-88-307/26/23 18:441.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 18:44 120-82-107/26/23 18:444.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 18:44 71-55-607/26/23 18:441.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 18:44 79-00-507/26/23 18:441.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 18:44 79-01-607/26/23 18:441.07 0.364 1 1,2,4-Trimethylbenzene 26.3 ug/m3 07/26/23 18:44 95-63-607/26/23 18:440.982 0.375 1 1,3,5-Trimethylbenzene 7.71 ug/m3 07/26/23 18:44 108-67-807/26/23 18:440.982 0.382 1 2,2,4-Trimethylpentane 5.56 ug/m3 07/26/23 18:44 540-84-107/26/23 18:440.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 18:44 75-01-407/26/23 18:440.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 18:44 593-60-207/26/23 18:440.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 18:44 108-05-407/26/23 18:440.704 0.408 1 m&p-Xylene 72.0 ug/m3 07/26/23 18:44 179601-23-107/26/23 18:441.73 0.585 1 o-Xylene 27.6 ug/m3 07/26/23 18:44 95-47-607/26/23 18:440.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)107 %07/26/23 18:44 460-00-407/26/23 18:4460.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 34 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-16 Lab ID: 92679117016 Collected: 07/20/23 09:38 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 18.0 ug/m3 07/26/23 19:12 67-64-107/26/23 19:122.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 19:12 107-05-107/26/23 19:120.626 0.357 1 Benzene 13.6 ug/m3 07/26/23 19:12 71-43-207/26/23 19:120.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 19:12 100-44-707/26/23 19:121.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 19:12 75-27-407/26/23 19:121.34 0.471 1 Bromoform ND ug/m3 07/26/23 19:12 75-25-207/26/23 19:126.21 0.757 1 Bromomethane ND ug/m3 07/26/23 19:12 74-83-907/26/23 19:120.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 19:12 106-99-007/26/23 19:124.43 0.230 1 Carbon disulfide 17.1 ug/m3 07/26/23 19:12 75-15-007/26/23 19:120.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 19:12 56-23-507/26/23 19:121.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 19:12 108-90-707/26/23 19:120.924 0.385 1 Chloroethane ND ug/m3 07/26/23 19:12 75-00-307/26/23 19:120.528 0.263 1 Chloroform 9.10 ug/m3 07/26/23 19:12 67-66-307/26/23 19:120.973 0.349 1 Chloromethane 0.374J ug/m3 07/26/23 19:12 74-87-3 J07/26/23 19:120.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 19:12 95-49-807/26/23 19:121.03 0.427 1 Cyclohexane 10.9 ug/m3 07/26/23 19:12 110-82-707/26/23 19:120.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 19:12 124-48-107/26/23 19:121.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 19:12 106-93-407/26/23 19:121.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 19:12 95-50-107/26/23 19:121.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 19:12 541-73-107/26/23 19:121.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 19:12 106-46-707/26/23 19:121.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 19:12 107-06-207/26/23 19:120.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 19:12 75-34-307/26/23 19:120.802 0.290 1 1,1-Dichloroethene 0.472J ug/m3 07/26/23 19:12 75-35-4 J07/26/23 19:120.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 19:12 156-59-207/26/23 19:120.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 19:12 156-60-507/26/23 19:120.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 19:12 78-87-507/26/23 19:120.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 19:12 10061-01-507/26/23 19:120.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 19:12 10061-02-607/26/23 19:120.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 19:12 123-91-107/26/23 19:120.721 0.300 1 Ethanol 21.9 ug/m3 07/26/23 19:12 64-17-507/26/23 19:124.71 0.500 1 Ethylbenzene 13.8 ug/m3 07/26/23 19:12 100-41-407/26/23 19:120.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 19:12 141-78-607/26/23 19:120.720 0.360 1 4-Ethyltoluene 2.19 ug/m3 07/26/23 19:12 622-96-807/26/23 19:120.982 0.384 1 Trichlorofluoromethane 1.43 ug/m3 07/26/23 19:12 75-69-407/26/23 19:121.12 0.460 1 Dichlorodifluoromethane 1.77 ug/m3 07/26/23 19:12 75-71-807/26/23 19:120.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 19:12 76-13-107/26/23 19:121.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 19:12 76-14-207/26/23 19:121.40 0.622 1 n-Heptane 83.4 ug/m3 07/26/23 19:12 142-82-507/26/23 19:120.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 19:12 87-68-307/26/23 19:126.73 1.12 1 n-Hexane 38.8 ug/m3 07/26/23 19:12 110-54-307/26/23 19:122.22 0.726 1 Isopropylbenzene (Cumene)4.02 ug/m3 07/26/23 19:12 98-82-807/26/23 19:120.983 0.382 1 Methylene Chloride 0.833 ug/m3 07/26/23 19:12 75-09-207/26/23 19:120.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 19:12 591-78-607/26/23 19:125.11 0.544 1 2-Butanone (MEK)5.51 ug/m3 07/26/23 19:12 78-93-307/26/23 19:123.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 35 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-16 Lab ID: 92679117016 Collected: 07/20/23 09:38 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 19:12 108-10-107/26/23 19:125.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 19:12 80-62-607/26/23 19:120.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 19:12 1634-04-407/26/23 19:120.721 0.233 1 Naphthalene ND ug/m3 07/26/23 19:12 91-20-307/26/23 19:123.30 1.83 1 2-Propanol 2.88J ug/m3 07/26/23 19:12 67-63-0 J07/26/23 19:123.07 0.649 1 Propylene 5.06 ug/m3 07/26/23 19:12 115-07-107/26/23 19:122.15 0.160 1 Styrene 0.519J ug/m3 07/26/23 19:12 100-42-5 J07/26/23 19:120.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 19:12 79-34-507/26/23 19:121.37 0.511 1 Tetrachloroethene 99.1 ug/m3 07/26/23 19:12 127-18-407/26/23 19:121.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 19:12 109-99-907/26/23 19:120.590 0.216 1 Toluene 113 ug/m3 07/26/23 19:12 108-88-307/26/23 19:121.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 19:12 120-82-107/26/23 19:124.66 1.10 1 1,1,1-Trichloroethane 1.82 ug/m3 07/26/23 19:12 71-55-607/26/23 19:121.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 19:12 79-00-507/26/23 19:121.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 19:12 79-01-607/26/23 19:121.07 0.364 1 1,2,4-Trimethylbenzene 7.71 ug/m3 07/26/23 19:12 95-63-607/26/23 19:120.982 0.375 1 1,3,5-Trimethylbenzene 2.52 ug/m3 07/26/23 19:12 108-67-807/26/23 19:120.982 0.382 1 2,2,4-Trimethylpentane 60.7 ug/m3 07/26/23 19:12 540-84-107/26/23 19:120.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 19:12 75-01-407/26/23 19:120.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 19:12 593-60-207/26/23 19:120.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 19:12 108-05-407/26/23 19:120.704 0.408 1 m&p-Xylene 37.8 ug/m3 07/26/23 19:12 179601-23-107/26/23 19:121.73 0.585 1 o-Xylene 13.0 ug/m3 07/26/23 19:12 95-47-607/26/23 19:120.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)106 %07/26/23 19:12 460-00-407/26/23 19:1260.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 36 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-17 Lab ID: 92679117017 Collected: 07/20/23 10:05 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 14.6 ug/m3 07/26/23 19:40 67-64-107/26/23 19:402.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 19:40 107-05-107/26/23 19:400.626 0.357 1 Benzene 15.4 ug/m3 07/26/23 19:40 71-43-207/26/23 19:400.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 19:40 100-44-707/26/23 19:401.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 19:40 75-27-407/26/23 19:401.34 0.471 1 Bromoform ND ug/m3 07/26/23 19:40 75-25-207/26/23 19:406.21 0.757 1 Bromomethane ND ug/m3 07/26/23 19:40 74-83-907/26/23 19:400.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 19:40 106-99-007/26/23 19:404.43 0.230 1 Carbon disulfide 13.8 ug/m3 07/26/23 19:40 75-15-007/26/23 19:400.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 19:40 56-23-507/26/23 19:401.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 19:40 108-90-707/26/23 19:400.924 0.385 1 Chloroethane ND ug/m3 07/26/23 19:40 75-00-307/26/23 19:400.528 0.263 1 Chloroform 37.3 ug/m3 07/26/23 19:40 67-66-307/26/23 19:400.973 0.349 1 Chloromethane 0.628 ug/m3 07/26/23 19:40 74-87-307/26/23 19:400.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 19:40 95-49-807/26/23 19:401.03 0.427 1 Cyclohexane 6.99 ug/m3 07/26/23 19:40 110-82-707/26/23 19:400.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 19:40 124-48-107/26/23 19:401.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 19:40 106-93-407/26/23 19:401.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 19:40 95-50-107/26/23 19:401.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 19:40 541-73-107/26/23 19:401.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 19:40 106-46-707/26/23 19:401.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 19:40 107-06-207/26/23 19:400.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 19:40 75-34-307/26/23 19:400.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 19:40 75-35-407/26/23 19:400.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 19:40 156-59-207/26/23 19:400.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 19:40 156-60-507/26/23 19:400.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 19:40 78-87-507/26/23 19:400.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 19:40 10061-01-507/26/23 19:400.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 19:40 10061-02-607/26/23 19:400.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 19:40 123-91-107/26/23 19:400.721 0.300 1 Ethanol 69.8 ug/m3 07/26/23 19:40 64-17-507/26/23 19:404.71 0.500 1 Ethylbenzene 20.0 ug/m3 07/26/23 19:40 100-41-407/26/23 19:400.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 19:40 141-78-607/26/23 19:400.720 0.360 1 4-Ethyltoluene 4.45 ug/m3 07/26/23 19:40 622-96-807/26/23 19:400.982 0.384 1 Trichlorofluoromethane 1.48 ug/m3 07/26/23 19:40 75-69-407/26/23 19:401.12 0.460 1 Dichlorodifluoromethane 1.70 ug/m3 07/26/23 19:40 75-71-807/26/23 19:400.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 19:40 76-13-107/26/23 19:401.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 19:40 76-14-207/26/23 19:401.40 0.622 1 n-Heptane 90.0 ug/m3 07/26/23 19:40 142-82-507/26/23 19:400.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 19:40 87-68-307/26/23 19:406.73 1.12 1 n-Hexane 22.8 ug/m3 07/26/23 19:40 110-54-307/26/23 19:402.22 0.726 1 Isopropylbenzene (Cumene)3.89 ug/m3 07/26/23 19:40 98-82-807/26/23 19:400.983 0.382 1 Methylene Chloride 4.13 ug/m3 07/26/23 19:40 75-09-207/26/23 19:400.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 19:40 591-78-607/26/23 19:405.11 0.544 1 2-Butanone (MEK)2.36J ug/m3 07/26/23 19:40 78-93-3 J07/26/23 19:403.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 37 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-17 Lab ID: 92679117017 Collected: 07/20/23 10:05 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 19:40 108-10-107/26/23 19:405.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 19:40 80-62-607/26/23 19:400.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 19:40 1634-04-407/26/23 19:400.721 0.233 1 Naphthalene ND ug/m3 07/26/23 19:40 91-20-307/26/23 19:403.30 1.83 1 2-Propanol 7.52 ug/m3 07/26/23 19:40 67-63-007/26/23 19:403.07 0.649 1 Propylene 1.83J ug/m3 07/26/23 19:40 115-07-1 J07/26/23 19:402.15 0.160 1 Styrene 0.425J ug/m3 07/26/23 19:40 100-42-5 J07/26/23 19:400.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 19:40 79-34-507/26/23 19:401.37 0.511 1 Tetrachloroethene 139 ug/m3 07/26/23 19:40 127-18-407/26/23 19:401.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 19:40 109-99-907/26/23 19:400.590 0.216 1 Toluene 142 ug/m3 07/26/23 19:40 108-88-307/26/23 19:401.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 19:40 120-82-107/26/23 19:404.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 19:40 71-55-607/26/23 19:401.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 19:40 79-00-507/26/23 19:401.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 19:40 79-01-607/26/23 19:401.07 0.364 1 1,2,4-Trimethylbenzene 13.1 ug/m3 07/26/23 19:40 95-63-607/26/23 19:400.982 0.375 1 1,3,5-Trimethylbenzene 4.50 ug/m3 07/26/23 19:40 108-67-807/26/23 19:400.982 0.382 1 2,2,4-Trimethylpentane 56.5 ug/m3 07/26/23 19:40 540-84-107/26/23 19:400.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 19:40 75-01-407/26/23 19:400.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 19:40 593-60-207/26/23 19:400.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 19:40 108-05-407/26/23 19:400.704 0.408 1 m&p-Xylene 56.8 ug/m3 07/26/23 19:40 179601-23-107/26/23 19:401.73 0.585 1 o-Xylene 18.9 ug/m3 07/26/23 19:40 95-47-607/26/23 19:400.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)108 %07/26/23 19:40 460-00-407/26/23 19:4060.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 38 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-18 Lab ID: 92679117018 Collected: 07/20/23 10:59 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 13.3 ug/m3 07/26/23 20:09 67-64-107/26/23 20:092.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 20:09 107-05-107/26/23 20:090.626 0.357 1 Benzene 15.7 ug/m3 07/26/23 20:09 71-43-207/26/23 20:090.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 20:09 100-44-707/26/23 20:091.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 20:09 75-27-407/26/23 20:091.34 0.471 1 Bromoform ND ug/m3 07/26/23 20:09 75-25-207/26/23 20:096.21 0.757 1 Bromomethane ND ug/m3 07/26/23 20:09 74-83-907/26/23 20:090.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 20:09 106-99-007/26/23 20:094.43 0.230 1 Carbon disulfide 30.2 ug/m3 07/26/23 20:09 75-15-007/26/23 20:090.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 20:09 56-23-507/26/23 20:091.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 20:09 108-90-707/26/23 20:090.924 0.385 1 Chloroethane ND ug/m3 07/26/23 20:09 75-00-307/26/23 20:090.528 0.263 1 Chloroform 22.6 ug/m3 07/26/23 20:09 67-66-307/26/23 20:090.973 0.349 1 Chloromethane ND ug/m3 07/26/23 20:09 74-87-307/26/23 20:090.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 20:09 95-49-807/26/23 20:091.03 0.427 1 Cyclohexane 14.7 ug/m3 07/26/23 20:09 110-82-707/26/23 20:090.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 20:09 124-48-107/26/23 20:091.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 20:09 106-93-407/26/23 20:091.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 20:09 95-50-107/26/23 20:091.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 20:09 541-73-107/26/23 20:091.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 20:09 106-46-707/26/23 20:091.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 20:09 107-06-207/26/23 20:090.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 20:09 75-34-307/26/23 20:090.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 20:09 75-35-407/26/23 20:090.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 20:09 156-59-207/26/23 20:090.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 20:09 156-60-507/26/23 20:090.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 20:09 78-87-507/26/23 20:090.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 20:09 10061-01-507/26/23 20:090.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 20:09 10061-02-607/26/23 20:090.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 20:09 123-91-107/26/23 20:090.721 0.300 1 Ethanol 53.5 ug/m3 07/26/23 20:09 64-17-507/26/23 20:094.71 0.500 1 Ethylbenzene 9.06 ug/m3 07/26/23 20:09 100-41-407/26/23 20:090.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 20:09 141-78-607/26/23 20:090.720 0.360 1 4-Ethyltoluene 1.31 ug/m3 07/26/23 20:09 622-96-807/26/23 20:090.982 0.384 1 Trichlorofluoromethane 51.4 ug/m3 07/26/23 20:09 75-69-407/26/23 20:091.12 0.460 1 Dichlorodifluoromethane 1.71 ug/m3 07/26/23 20:09 75-71-807/26/23 20:090.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 20:09 76-13-107/26/23 20:091.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 20:09 76-14-207/26/23 20:091.40 0.622 1 n-Heptane 141 ug/m3 07/26/23 20:09 142-82-507/26/23 20:090.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 20:09 87-68-307/26/23 20:096.73 1.12 1 n-Hexane 45.5 ug/m3 07/26/23 20:09 110-54-307/26/23 20:092.22 0.726 1 Isopropylbenzene (Cumene)3.26 ug/m3 07/26/23 20:09 98-82-807/26/23 20:090.983 0.382 1 Methylene Chloride 3.58 ug/m3 07/26/23 20:09 75-09-207/26/23 20:090.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 20:09 591-78-607/26/23 20:095.11 0.544 1 2-Butanone (MEK)2.77J ug/m3 07/26/23 20:09 78-93-3 J07/26/23 20:093.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 39 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-18 Lab ID: 92679117018 Collected: 07/20/23 10:59 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 20:09 108-10-107/26/23 20:095.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 20:09 80-62-607/26/23 20:090.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 20:09 1634-04-407/26/23 20:090.721 0.233 1 Naphthalene ND ug/m3 07/26/23 20:09 91-20-307/26/23 20:093.30 1.83 1 2-Propanol 6.10 ug/m3 07/26/23 20:09 67-63-007/26/23 20:093.07 0.649 1 Propylene ND ug/m3 07/26/23 20:09 115-07-107/26/23 20:092.15 0.160 1 Styrene 1.33 ug/m3 07/26/23 20:09 100-42-507/26/23 20:090.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 20:09 79-34-507/26/23 20:091.37 0.511 1 Tetrachloroethene 151 ug/m3 07/26/23 20:09 127-18-407/26/23 20:091.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 20:09 109-99-907/26/23 20:090.590 0.216 1 Toluene 98.7 ug/m3 07/26/23 20:09 108-88-307/26/23 20:091.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 20:09 120-82-107/26/23 20:094.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 20:09 71-55-607/26/23 20:091.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 20:09 79-00-507/26/23 20:091.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 20:09 79-01-607/26/23 20:091.07 0.364 1 1,2,4-Trimethylbenzene 4.15 ug/m3 07/26/23 20:09 95-63-607/26/23 20:090.982 0.375 1 1,3,5-Trimethylbenzene 1.40 ug/m3 07/26/23 20:09 108-67-807/26/23 20:090.982 0.382 1 2,2,4-Trimethylpentane 81.3 ug/m3 07/26/23 20:09 540-84-107/26/23 20:090.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 20:09 75-01-407/26/23 20:090.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 20:09 593-60-207/26/23 20:090.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 20:09 108-05-407/26/23 20:090.704 0.408 1 m&p-Xylene 25.4 ug/m3 07/26/23 20:09 179601-23-107/26/23 20:091.73 0.585 1 o-Xylene 8.89 ug/m3 07/26/23 20:09 95-47-607/26/23 20:090.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)106 %07/26/23 20:09 460-00-407/26/23 20:0960.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 40 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-19 Lab ID: 92679117019 Collected: 07/20/23 12:03 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 30.4J ug/m3 07/26/23 21:02 67-64-1 J07/26/23 21:0259.4 27.8 20 Allyl chloride ND ug/m3 07/26/23 21:02 107-05-107/26/23 21:0212.5 7.14 20 Benzene 17.2 ug/m3 07/26/23 21:02 71-43-207/26/23 21:0212.8 4.57 20 Benzyl chloride ND ug/m3 07/26/23 21:02 100-44-707/26/23 21:0220.8 6.23 20 Bromodichloromethane ND ug/m3 07/26/23 21:02 75-27-407/26/23 21:0226.8 9.39 20 Bromoform ND ug/m3 07/26/23 21:02 75-25-207/26/23 21:02124 15.1 20 Bromomethane ND ug/m3 07/26/23 21:02 74-83-907/26/23 21:0215.5 7.61 20 1,3-Butadiene ND ug/m3 07/26/23 21:02 106-99-007/26/23 21:0288.5 4.60 20 Carbon disulfide 28.7 ug/m3 07/26/23 21:02 75-15-007/26/23 21:0212.4 6.35 20 Carbon tetrachloride ND ug/m3 07/26/23 21:02 56-23-507/26/23 21:0225.2 9.20 20 Chlorobenzene ND ug/m3 07/26/23 21:02 108-90-707/26/23 21:0218.5 7.67 20 Chloroethane ND ug/m3 07/26/23 21:02 75-00-307/26/23 21:0210.6 5.25 20 Chloroform ND ug/m3 07/26/23 21:02 67-66-307/26/23 21:0219.5 6.96 20 Chloromethane ND ug/m3 07/26/23 21:02 74-87-307/26/23 21:028.26 4.25 20 2-Chlorotoluene ND ug/m3 07/26/23 21:02 95-49-807/26/23 21:0220.6 8.55 20 Cyclohexane ND ug/m3 07/26/23 21:02 110-82-707/26/23 21:0213.8 5.20 20 Dibromochloromethane ND ug/m3 07/26/23 21:02 124-48-107/26/23 21:0234.0 12.3 20 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 21:02 106-93-407/26/23 21:0230.8 11.1 20 1,2-Dichlorobenzene ND ug/m3 07/26/23 21:02 95-50-107/26/23 21:0224.0 15.4 20 1,3-Dichlorobenzene ND ug/m3 07/26/23 21:02 541-73-107/26/23 21:0224.0 21.9 20 1,4-Dichlorobenzene ND ug/m3 07/26/23 21:02 106-46-707/26/23 21:0224.0 6.67 20 1,2-Dichloroethane ND ug/m3 07/26/23 21:02 107-06-207/26/23 21:0216.2 5.67 20 1,1-Dichloroethane ND ug/m3 07/26/23 21:02 75-34-307/26/23 21:0216.0 5.81 20 1,1-Dichloroethene ND ug/m3 07/26/23 21:02 75-35-407/26/23 21:0215.9 6.02 20 cis-1,2-Dichloroethene ND ug/m3 07/26/23 21:02 156-59-207/26/23 21:0215.9 6.22 20 trans-1,2-Dichloroethene ND ug/m3 07/26/23 21:02 156-60-507/26/23 21:0215.9 5.35 20 1,2-Dichloropropane ND ug/m3 07/26/23 21:02 78-87-507/26/23 21:0218.5 7.02 20 cis-1,3-Dichloropropene ND ug/m3 07/26/23 21:02 10061-01-507/26/23 21:0218.2 6.27 20 trans-1,3-Dichloropropene ND ug/m3 07/26/23 21:02 10061-02-607/26/23 21:0218.2 6.63 20 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 21:02 123-91-107/26/23 21:0214.4 6.02 20 Ethanol 27.0J ug/m3 07/26/23 21:02 64-17-5 B,J07/26/23 21:0294.3 9.99 20 Ethylbenzene 22.9 ug/m3 07/26/23 21:02 100-41-407/26/23 21:0217.3 7.24 20 Ethyl acetate ND ug/m3 07/26/23 21:02 141-78-607/26/23 21:0214.4 7.20 20 4-Ethyltoluene ND ug/m3 07/26/23 21:02 622-96-807/26/23 21:0219.6 7.71 20 Trichlorofluoromethane ND ug/m3 07/26/23 21:02 75-69-407/26/23 21:0222.5 9.22 20 Dichlorodifluoromethane ND ug/m3 07/26/23 21:02 75-71-807/26/23 21:0219.8 13.6 20 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 21:02 76-13-107/26/23 21:0230.7 12.2 20 Dichlorotetrafluoroethane ND ug/m3 07/26/23 21:02 76-14-207/26/23 21:0228.0 12.4 20 n-Heptane 99.4 ug/m3 07/26/23 21:02 142-82-507/26/23 21:0216.4 8.51 20 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 21:02 87-68-307/26/23 21:02135 22.4 20 n-Hexane ND ug/m3 07/26/23 21:02 110-54-307/26/23 21:0244.4 14.5 20 Isopropylbenzene (Cumene)ND ug/m3 07/26/23 21:02 98-82-807/26/23 21:0219.7 7.62 20 Methylene Chloride ND ug/m3 07/26/23 21:02 75-09-207/26/23 21:0213.9 6.81 20 2-Hexanone ND ug/m3 07/26/23 21:02 591-78-607/26/23 21:02102 10.9 20 2-Butanone (MEK)9.61J ug/m3 07/26/23 21:02 78-93-3 J07/26/23 21:0273.7 4.81 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 41 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-19 Lab ID: 92679117019 Collected: 07/20/23 12:03 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 21:02 108-10-107/26/23 21:02102 6.26 20 Methyl methacrylate ND ug/m3 07/26/23 21:02 80-62-607/26/23 21:0216.4 7.17 20 Methyl-tert-butyl ether ND ug/m3 07/26/23 21:02 1634-04-407/26/23 21:0214.4 4.65 20 Naphthalene ND ug/m3 07/26/23 21:02 91-20-307/26/23 21:0266.0 36.6 20 2-Propanol ND ug/m3 07/26/23 21:02 67-63-007/26/23 21:0261.5 13.0 20 Propylene ND ug/m3 07/26/23 21:02 115-07-107/26/23 21:0243.0 3.20 20 Styrene ND ug/m3 07/26/23 21:02 100-42-507/26/23 21:0217.0 6.72 20 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 21:02 79-34-507/26/23 21:0227.5 10.2 20 Tetrachloroethene 292 ug/m3 07/26/23 21:02 127-18-407/26/23 21:0227.2 11.1 20 Tetrahydrofuran ND ug/m3 07/26/23 21:02 109-99-907/26/23 21:0211.8 4.33 20 Toluene 217 ug/m3 07/26/23 21:02 108-88-307/26/23 21:0237.7 6.55 20 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 21:02 120-82-107/26/23 21:0293.3 21.9 20 1,1,1-Trichloroethane ND ug/m3 07/26/23 21:02 71-55-607/26/23 21:0221.8 8.00 20 1,1,2-Trichloroethane ND ug/m3 07/26/23 21:02 79-00-507/26/23 21:0221.8 8.43 20 Trichloroethene ND ug/m3 07/26/23 21:02 79-01-607/26/23 21:0221.4 7.29 20 1,2,4-Trimethylbenzene ND ug/m3 07/26/23 21:02 95-63-607/26/23 21:0219.6 7.51 20 1,3,5-Trimethylbenzene ND ug/m3 07/26/23 21:02 108-67-807/26/23 21:0219.6 7.66 20 2,2,4-Trimethylpentane 41.9 ug/m3 07/26/23 21:02 540-84-107/26/23 21:0218.7 12.4 20 Vinyl chloride ND ug/m3 07/26/23 21:02 75-01-407/26/23 21:0210.2 4.86 20 Vinyl bromide ND ug/m3 07/26/23 21:02 593-60-207/26/23 21:0217.5 7.44 20 Vinyl acetate ND ug/m3 07/26/23 21:02 108-05-407/26/23 21:0214.1 8.17 20 m&p-Xylene 61.6 ug/m3 07/26/23 21:02 179601-23-107/26/23 21:0234.7 11.7 20 o-Xylene 24.5 ug/m3 07/26/23 21:02 95-47-607/26/23 21:0217.3 7.20 20 Surrogates 4-Bromofluorobenzene (S)103 %07/26/23 21:02 460-00-407/26/23 21:0260.0-140 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 42 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-20 Lab ID: 92679117020 Collected: 07/20/23 12:42 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 19.1 ug/m3 07/26/23 20:37 67-64-107/26/23 20:372.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 20:37 107-05-107/26/23 20:370.626 0.357 1 Benzene 9.58 ug/m3 07/26/23 20:37 71-43-207/26/23 20:370.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 20:37 100-44-707/26/23 20:371.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 20:37 75-27-407/26/23 20:371.34 0.471 1 Bromoform ND ug/m3 07/26/23 20:37 75-25-207/26/23 20:376.21 0.757 1 Bromomethane ND ug/m3 07/26/23 20:37 74-83-907/26/23 20:370.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 20:37 106-99-007/26/23 20:374.43 0.230 1 Carbon disulfide 25.0 ug/m3 07/26/23 20:37 75-15-007/26/23 20:370.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 20:37 56-23-507/26/23 20:371.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 20:37 108-90-707/26/23 20:370.924 0.385 1 Chloroethane ND ug/m3 07/26/23 20:37 75-00-307/26/23 20:370.528 0.263 1 Chloroform 0.579J ug/m3 07/26/23 20:37 67-66-3 J07/26/23 20:370.973 0.349 1 Chloromethane 2.01 ug/m3 07/26/23 20:37 74-87-307/26/23 20:370.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 20:37 95-49-807/26/23 20:371.03 0.427 1 Cyclohexane 3.65 ug/m3 07/26/23 20:37 110-82-707/26/23 20:370.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 20:37 124-48-107/26/23 20:371.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 20:37 106-93-407/26/23 20:371.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 20:37 95-50-107/26/23 20:371.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 20:37 541-73-107/26/23 20:371.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 20:37 106-46-707/26/23 20:371.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 20:37 107-06-207/26/23 20:370.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 20:37 75-34-307/26/23 20:370.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 20:37 75-35-407/26/23 20:370.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 20:37 156-59-207/26/23 20:370.793 0.311 1 trans-1,2-Dichloroethene 0.307J ug/m3 07/26/23 20:37 156-60-5 J07/26/23 20:370.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 20:37 78-87-507/26/23 20:370.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 20:37 10061-01-507/26/23 20:370.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 20:37 10061-02-607/26/23 20:370.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 20:37 123-91-107/26/23 20:370.721 0.300 1 Ethanol 27.7 ug/m3 07/26/23 20:37 64-17-507/26/23 20:374.71 0.500 1 Ethylbenzene 21.1 ug/m3 07/26/23 20:37 100-41-407/26/23 20:370.867 0.362 1 Ethyl acetate ND ug/m3 07/26/23 20:37 141-78-607/26/23 20:370.720 0.360 1 4-Ethyltoluene 4.08 ug/m3 07/26/23 20:37 622-96-807/26/23 20:370.982 0.384 1 Trichlorofluoromethane 1.29 ug/m3 07/26/23 20:37 75-69-407/26/23 20:371.12 0.460 1 Dichlorodifluoromethane 1.22 ug/m3 07/26/23 20:37 75-71-807/26/23 20:370.989 0.678 1 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 20:37 76-13-107/26/23 20:371.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 20:37 76-14-207/26/23 20:371.40 0.622 1 n-Heptane 63.0 ug/m3 07/26/23 20:37 142-82-507/26/23 20:370.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 20:37 87-68-307/26/23 20:376.73 1.12 1 n-Hexane 7.54 ug/m3 07/26/23 20:37 110-54-307/26/23 20:372.22 0.726 1 Isopropylbenzene (Cumene)3.55 ug/m3 07/26/23 20:37 98-82-807/26/23 20:370.983 0.382 1 Methylene Chloride 0.819 ug/m3 07/26/23 20:37 75-09-207/26/23 20:370.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 20:37 591-78-607/26/23 20:375.11 0.544 1 2-Butanone (MEK)7.73 ug/m3 07/26/23 20:37 78-93-307/26/23 20:373.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 43 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-20 Lab ID: 92679117020 Collected: 07/20/23 12:42 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 20:37 108-10-107/26/23 20:375.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 20:37 80-62-607/26/23 20:370.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 20:37 1634-04-407/26/23 20:370.721 0.233 1 Naphthalene ND ug/m3 07/26/23 20:37 91-20-307/26/23 20:373.30 1.83 1 2-Propanol 6.83 ug/m3 07/26/23 20:37 67-63-007/26/23 20:373.07 0.649 1 Propylene ND ug/m3 07/26/23 20:37 115-07-107/26/23 20:372.15 0.160 1 Styrene 0.966 ug/m3 07/26/23 20:37 100-42-507/26/23 20:370.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 20:37 79-34-507/26/23 20:371.37 0.511 1 Tetrachloroethene 208 ug/m3 07/26/23 20:37 127-18-407/26/23 20:371.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 20:37 109-99-907/26/23 20:370.590 0.216 1 Toluene 149 ug/m3 07/26/23 20:37 108-88-307/26/23 20:371.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 20:37 120-82-107/26/23 20:374.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 20:37 71-55-607/26/23 20:371.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 20:37 79-00-507/26/23 20:371.09 0.422 1 Trichloroethene ND ug/m3 07/26/23 20:37 79-01-607/26/23 20:371.07 0.364 1 1,2,4-Trimethylbenzene 12.1 ug/m3 07/26/23 20:37 95-63-607/26/23 20:370.982 0.375 1 1,3,5-Trimethylbenzene 3.29 ug/m3 07/26/23 20:37 108-67-807/26/23 20:370.982 0.382 1 2,2,4-Trimethylpentane 26.2 ug/m3 07/26/23 20:37 540-84-107/26/23 20:370.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 20:37 75-01-407/26/23 20:370.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 20:37 593-60-207/26/23 20:370.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 20:37 108-05-407/26/23 20:370.704 0.408 1 m&p-Xylene 58.1 ug/m3 07/26/23 20:37 179601-23-107/26/23 20:371.73 0.585 1 o-Xylene 20.4 ug/m3 07/26/23 20:37 95-47-607/26/23 20:370.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)107 %07/26/23 20:37 460-00-407/26/23 20:3760.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 44 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-21 Lab ID: 92679117021 Collected: 07/20/23 13:17 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 28.8 ug/m3 07/26/23 18:40 67-64-107/26/23 18:402.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 18:40 107-05-107/26/23 18:400.626 0.357 1 Benzene 34.5 ug/m3 07/26/23 18:40 71-43-207/26/23 18:400.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 18:40 100-44-707/26/23 18:401.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 18:40 75-27-407/26/23 18:401.34 0.471 1 Bromoform ND ug/m3 07/26/23 18:40 75-25-207/26/23 18:406.21 0.757 1 Bromomethane ND ug/m3 07/26/23 18:40 74-83-907/26/23 18:400.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 18:40 106-99-007/26/23 18:404.43 0.230 1 Carbon disulfide 129 ug/m3 07/26/23 18:40 75-15-007/26/23 18:400.622 0.317 1 Carbon tetrachloride 0.584J ug/m3 07/26/23 18:40 56-23-5 J07/26/23 18:401.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 18:40 108-90-707/26/23 18:400.924 0.385 1 Chloroethane ND ug/m3 07/26/23 18:40 75-00-307/26/23 18:400.528 0.263 1 Chloroform ND ug/m3 07/26/23 18:40 67-66-307/26/23 18:400.973 0.349 1 Chloromethane 5.87 ug/m3 07/26/23 18:40 74-87-307/26/23 18:400.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 18:40 95-49-807/26/23 18:401.03 0.427 1 Cyclohexane ND ug/m3 07/26/23 18:40 110-82-707/26/23 18:400.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 18:40 124-48-107/26/23 18:401.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 18:40 106-93-407/26/23 18:401.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 18:40 95-50-107/26/23 18:401.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 18:40 541-73-107/26/23 18:401.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 18:40 106-46-707/26/23 18:401.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 18:40 107-06-207/26/23 18:400.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 18:40 75-34-307/26/23 18:400.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 18:40 75-35-407/26/23 18:400.793 0.302 1 cis-1,2-Dichloroethene 0.749J ug/m3 07/26/23 18:40 156-59-2 J07/26/23 18:400.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 18:40 156-60-507/26/23 18:400.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 18:40 78-87-507/26/23 18:400.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 18:40 10061-01-507/26/23 18:400.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 18:40 10061-02-607/26/23 18:400.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 18:40 123-91-107/26/23 18:400.721 0.300 1 Ethanol 108 ug/m3 07/26/23 18:40 64-17-507/26/23 18:404.71 0.500 1 Ethylbenzene 36.6 ug/m3 07/26/23 18:40 100-41-407/26/23 18:400.867 0.362 1 Ethyl acetate 1.62 ug/m3 07/26/23 18:40 141-78-607/26/23 18:400.720 0.360 1 4-Ethyltoluene 5.20 ug/m3 07/26/23 18:40 622-96-807/26/23 18:400.982 0.384 1 Trichlorofluoromethane 7.14 ug/m3 07/26/23 18:40 75-69-407/26/23 18:401.12 0.460 1 Dichlorodifluoromethane 2.71 ug/m3 07/26/23 18:40 75-71-807/26/23 18:400.989 0.678 1 1,1,2-Trichlorotrifluoroethane 1.02J ug/m3 07/26/23 18:40 76-13-1 J07/26/23 18:401.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 18:40 76-14-207/26/23 18:401.40 0.622 1 n-Heptane 203 ug/m3 07/26/23 18:40 142-82-507/26/23 18:400.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 18:40 87-68-307/26/23 18:406.73 1.12 1 n-Hexane 62.4 ug/m3 07/26/23 18:40 110-54-307/26/23 18:402.22 0.726 1 Isopropylbenzene (Cumene)ND ug/m3 07/26/23 18:40 98-82-807/26/23 18:400.983 0.382 1 Methylene Chloride 3.24 ug/m3 07/26/23 18:40 75-09-207/26/23 18:400.694 0.340 1 2-Hexanone ND ug/m3 07/26/23 18:40 591-78-607/26/23 18:405.11 0.544 1 2-Butanone (MEK)6.61 ug/m3 07/26/23 18:40 78-93-307/26/23 18:403.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 45 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-21 Lab ID: 92679117021 Collected: 07/20/23 13:17 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 18:40 108-10-107/26/23 18:405.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 18:40 80-62-607/26/23 18:400.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 18:40 1634-04-407/26/23 18:400.721 0.233 1 Naphthalene ND ug/m3 07/26/23 18:40 91-20-307/26/23 18:403.30 1.83 1 2-Propanol 19.3 ug/m3 07/26/23 18:40 67-63-007/26/23 18:403.07 0.649 1 Propylene 29.6 ug/m3 07/26/23 18:40 115-07-107/26/23 18:402.15 0.160 1 Styrene ND ug/m3 07/26/23 18:40 100-42-507/26/23 18:400.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 18:40 79-34-507/26/23 18:401.37 0.511 1 Tetrachloroethene 363 ug/m3 07/26/23 18:40 127-18-407/26/23 18:401.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 18:40 109-99-907/26/23 18:400.590 0.216 1 Toluene 268 ug/m3 07/26/23 18:40 108-88-307/26/23 18:401.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 18:40 120-82-107/26/23 18:404.66 1.10 1 1,1,1-Trichloroethane 0.480J ug/m3 07/26/23 18:40 71-55-6 J07/26/23 18:401.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 18:40 79-00-507/26/23 18:401.09 0.422 1 Trichloroethene 27.8 ug/m3 07/26/23 18:40 79-01-607/26/23 18:401.07 0.364 1 1,2,4-Trimethylbenzene 22.7 ug/m3 07/26/23 18:40 95-63-607/26/23 18:400.982 0.375 1 1,3,5-Trimethylbenzene 6.38 ug/m3 07/26/23 18:40 108-67-807/26/23 18:400.982 0.382 1 2,2,4-Trimethylpentane 122 ug/m3 07/26/23 18:40 540-84-107/26/23 18:400.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 18:40 75-01-407/26/23 18:400.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 18:40 593-60-207/26/23 18:400.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 18:40 108-05-407/26/23 18:400.704 0.408 1 m&p-Xylene 104 ug/m3 07/26/23 18:40 179601-23-107/26/23 18:401.73 0.585 1 o-Xylene 34.1 ug/m3 07/26/23 18:40 95-47-607/26/23 18:400.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)96.9 %07/26/23 18:40 460-00-407/26/23 18:4060.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 46 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-22 Lab ID: 92679117022 Collected: 07/20/23 14:17 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 1570 ug/m3 07/26/23 19:17 67-64-107/26/23 19:17297 139 100 Allyl chloride ND ug/m3 07/26/23 19:17 107-05-107/26/23 19:1762.6 35.7 100 Benzene 54.6J ug/m3 07/26/23 19:17 71-43-2 J07/26/23 19:1763.9 22.8 100 Benzyl chloride ND ug/m3 07/26/23 19:17 100-44-707/26/23 19:17104 31.1 100 Bromodichloromethane ND ug/m3 07/26/23 19:17 75-27-407/26/23 19:17134 47.1 100 Bromoform ND ug/m3 07/26/23 19:17 75-25-207/26/23 19:17621 75.7 100 Bromomethane ND ug/m3 07/26/23 19:17 74-83-907/26/23 19:1777.6 38.1 100 1,3-Butadiene ND ug/m3 07/26/23 19:17 106-99-007/26/23 19:17443 23.0 100 Carbon disulfide 43.3J ug/m3 07/26/23 19:17 75-15-0 J07/26/23 19:1762.2 31.7 100 Carbon tetrachloride ND ug/m3 07/26/23 19:17 56-23-507/26/23 19:17126 46.1 100 Chlorobenzene ND ug/m3 07/26/23 19:17 108-90-707/26/23 19:1792.4 38.5 100 Chloroethane ND ug/m3 07/26/23 19:17 75-00-307/26/23 19:1752.8 26.3 100 Chloroform ND ug/m3 07/26/23 19:17 67-66-307/26/23 19:1797.3 34.9 100 Chloromethane ND ug/m3 07/26/23 19:17 74-87-307/26/23 19:1741.3 21.3 100 2-Chlorotoluene ND ug/m3 07/26/23 19:17 95-49-807/26/23 19:17103 42.7 100 Cyclohexane 80.2 ug/m3 07/26/23 19:17 110-82-707/26/23 19:1768.9 25.9 100 Dibromochloromethane ND ug/m3 07/26/23 19:17 124-48-107/26/23 19:17170 61.8 100 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 19:17 106-93-407/26/23 19:17154 55.4 100 1,2-Dichlorobenzene ND ug/m3 07/26/23 19:17 95-50-107/26/23 19:17120 77.0 100 1,3-Dichlorobenzene ND ug/m3 07/26/23 19:17 541-73-107/26/23 19:17120 109 100 1,4-Dichlorobenzene ND ug/m3 07/26/23 19:17 106-46-707/26/23 19:17120 33.5 100 1,2-Dichloroethane ND ug/m3 07/26/23 19:17 107-06-207/26/23 19:1781.0 28.3 100 1,1-Dichloroethane ND ug/m3 07/26/23 19:17 75-34-307/26/23 19:1780.2 29.0 100 1,1-Dichloroethene ND ug/m3 07/26/23 19:17 75-35-407/26/23 19:1779.3 30.2 100 cis-1,2-Dichloroethene ND ug/m3 07/26/23 19:17 156-59-207/26/23 19:1779.3 31.1 100 trans-1,2-Dichloroethene ND ug/m3 07/26/23 19:17 156-60-507/26/23 19:1779.3 26.7 100 1,2-Dichloropropane ND ug/m3 07/26/23 19:17 78-87-507/26/23 19:1792.4 35.1 100 cis-1,3-Dichloropropene ND ug/m3 07/26/23 19:17 10061-01-507/26/23 19:1790.8 31.3 100 trans-1,3-Dichloropropene ND ug/m3 07/26/23 19:17 10061-02-607/26/23 19:1790.8 33.1 100 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 19:17 123-91-107/26/23 19:1772.1 30.0 100 Ethanol 2920 ug/m3 07/26/23 19:17 64-17-507/26/23 19:17471 50.0 100 Ethylbenzene 63.3J ug/m3 07/26/23 19:17 100-41-4 J07/26/23 19:1786.7 36.2 100 Ethyl acetate ND ug/m3 07/26/23 19:17 141-78-607/26/23 19:1772.0 36.0 100 4-Ethyltoluene ND ug/m3 07/26/23 19:17 622-96-807/26/23 19:1798.2 38.4 100 Trichlorofluoromethane ND ug/m3 07/26/23 19:17 75-69-407/26/23 19:17112 46.0 100 Dichlorodifluoromethane ND ug/m3 07/26/23 19:17 75-71-807/26/23 19:1798.9 67.8 100 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 19:17 76-13-107/26/23 19:17153 60.8 100 Dichlorotetrafluoroethane ND ug/m3 07/26/23 19:17 76-14-207/26/23 19:17140 62.2 100 n-Heptane 285 ug/m3 07/26/23 19:17 142-82-507/26/23 19:1781.8 42.5 100 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 19:17 87-68-307/26/23 19:17673 112 100 n-Hexane 4340 ug/m3 07/26/23 19:17 110-54-307/26/23 19:17222 72.6 100 Isopropylbenzene (Cumene)ND ug/m3 07/26/23 19:17 98-82-807/26/23 19:1798.3 38.2 100 Methylene Chloride 270 ug/m3 07/26/23 19:17 75-09-207/26/23 19:1769.4 34.0 100 2-Hexanone ND ug/m3 07/26/23 19:17 591-78-607/26/23 19:17511 54.4 100 2-Butanone (MEK)174J ug/m3 07/26/23 19:17 78-93-3 J07/26/23 19:17369 24.0 100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 47 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-22 Lab ID: 92679117022 Collected: 07/20/23 14:17 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)226J ug/m3 07/26/23 19:17 108-10-1 J07/26/23 19:17512 31.3 100 Methyl methacrylate 647 ug/m3 07/26/23 19:17 80-62-607/26/23 19:1781.9 35.9 100 Methyl-tert-butyl ether ND ug/m3 07/26/23 19:17 1634-04-407/26/23 19:1772.1 23.3 100 Naphthalene ND ug/m3 07/26/23 19:17 91-20-307/26/23 19:17330 183 100 2-Propanol 32400 ug/m3 07/26/23 19:17 67-63-0 E07/26/23 19:17307 64.9 100 Propylene ND ug/m3 07/26/23 19:17 115-07-107/26/23 19:17215 16.0 100 Styrene 69.8J ug/m3 07/26/23 19:17 100-42-5 J07/26/23 19:1785.1 33.5 100 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 19:17 79-34-507/26/23 19:17137 51.1 100 Tetrachloroethene 355 ug/m3 07/26/23 19:17 127-18-407/26/23 19:17136 55.3 100 Tetrahydrofuran ND ug/m3 07/26/23 19:17 109-99-907/26/23 19:1759.0 21.6 100 Toluene 433 ug/m3 07/26/23 19:17 108-88-307/26/23 19:17188 32.8 100 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 19:17 120-82-107/26/23 19:17466 110 100 1,1,1-Trichloroethane ND ug/m3 07/26/23 19:17 71-55-607/26/23 19:17109 40.0 100 1,1,2-Trichloroethane ND ug/m3 07/26/23 19:17 79-00-507/26/23 19:17109 42.2 100 Trichloroethene ND ug/m3 07/26/23 19:17 79-01-607/26/23 19:17107 36.4 100 1,2,4-Trimethylbenzene 86.4J ug/m3 07/26/23 19:17 95-63-6 J07/26/23 19:1798.2 37.5 100 1,3,5-Trimethylbenzene ND ug/m3 07/26/23 19:17 108-67-807/26/23 19:1798.2 38.2 100 2,2,4-Trimethylpentane 144 ug/m3 07/26/23 19:17 540-84-107/26/23 19:1793.4 62.1 100 Vinyl chloride ND ug/m3 07/26/23 19:17 75-01-407/26/23 19:1751.1 24.3 100 Vinyl bromide ND ug/m3 07/26/23 19:17 593-60-207/26/23 19:1787.5 37.3 100 Vinyl acetate ND ug/m3 07/26/23 19:17 108-05-407/26/23 19:1770.4 40.8 100 m&p-Xylene 215 ug/m3 07/26/23 19:17 179601-23-107/26/23 19:17173 58.5 100 o-Xylene 76.3J ug/m3 07/26/23 19:17 95-47-6 J07/26/23 19:1786.7 35.9 100 Surrogates 4-Bromofluorobenzene (S)95.5 %07/26/23 19:17 460-00-407/26/23 19:1760.0-140 100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 48 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-23 Lab ID: 92679117023 Collected: 07/20/23 14:58 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 21.0 ug/m3 07/26/23 19:55 67-64-107/26/23 19:552.97 1.39 1 Allyl chloride ND ug/m3 07/26/23 19:55 107-05-107/26/23 19:550.626 0.357 1 Benzene 30.4 ug/m3 07/26/23 19:55 71-43-207/26/23 19:550.639 0.228 1 Benzyl chloride ND ug/m3 07/26/23 19:55 100-44-707/26/23 19:551.04 0.311 1 Bromodichloromethane ND ug/m3 07/26/23 19:55 75-27-407/26/23 19:551.34 0.471 1 Bromoform ND ug/m3 07/26/23 19:55 75-25-207/26/23 19:556.21 0.757 1 Bromomethane ND ug/m3 07/26/23 19:55 74-83-907/26/23 19:550.776 0.381 1 1,3-Butadiene ND ug/m3 07/26/23 19:55 106-99-007/26/23 19:554.43 0.230 1 Carbon disulfide 54.2 ug/m3 07/26/23 19:55 75-15-007/26/23 19:550.622 0.317 1 Carbon tetrachloride ND ug/m3 07/26/23 19:55 56-23-507/26/23 19:551.26 0.461 1 Chlorobenzene ND ug/m3 07/26/23 19:55 108-90-707/26/23 19:550.924 0.385 1 Chloroethane ND ug/m3 07/26/23 19:55 75-00-307/26/23 19:550.528 0.263 1 Chloroform ND ug/m3 07/26/23 19:55 67-66-307/26/23 19:550.973 0.349 1 Chloromethane 0.921 ug/m3 07/26/23 19:55 74-87-307/26/23 19:550.413 0.213 1 2-Chlorotoluene ND ug/m3 07/26/23 19:55 95-49-807/26/23 19:551.03 0.427 1 Cyclohexane ND ug/m3 07/26/23 19:55 110-82-707/26/23 19:550.689 0.259 1 Dibromochloromethane ND ug/m3 07/26/23 19:55 124-48-107/26/23 19:551.70 0.618 1 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 19:55 106-93-407/26/23 19:551.54 0.554 1 1,2-Dichlorobenzene ND ug/m3 07/26/23 19:55 95-50-107/26/23 19:551.20 0.770 1 1,3-Dichlorobenzene ND ug/m3 07/26/23 19:55 541-73-107/26/23 19:551.20 1.09 1 1,4-Dichlorobenzene ND ug/m3 07/26/23 19:55 106-46-707/26/23 19:551.20 0.335 1 1,2-Dichloroethane ND ug/m3 07/26/23 19:55 107-06-207/26/23 19:550.810 0.283 1 1,1-Dichloroethane ND ug/m3 07/26/23 19:55 75-34-307/26/23 19:550.802 0.290 1 1,1-Dichloroethene ND ug/m3 07/26/23 19:55 75-35-407/26/23 19:550.793 0.302 1 cis-1,2-Dichloroethene ND ug/m3 07/26/23 19:55 156-59-207/26/23 19:550.793 0.311 1 trans-1,2-Dichloroethene ND ug/m3 07/26/23 19:55 156-60-507/26/23 19:550.793 0.267 1 1,2-Dichloropropane ND ug/m3 07/26/23 19:55 78-87-507/26/23 19:550.924 0.351 1 cis-1,3-Dichloropropene ND ug/m3 07/26/23 19:55 10061-01-507/26/23 19:550.908 0.313 1 trans-1,3-Dichloropropene ND ug/m3 07/26/23 19:55 10061-02-607/26/23 19:550.908 0.331 1 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 19:55 123-91-107/26/23 19:550.721 0.300 1 Ethanol 76.2 ug/m3 07/26/23 19:55 64-17-507/26/23 19:554.71 0.500 1 Ethylbenzene 32.2 ug/m3 07/26/23 19:55 100-41-407/26/23 19:550.867 0.362 1 Ethyl acetate 1.01 ug/m3 07/26/23 19:55 141-78-607/26/23 19:550.720 0.360 1 4-Ethyltoluene 5.45 ug/m3 07/26/23 19:55 622-96-807/26/23 19:550.982 0.384 1 Trichlorofluoromethane 7.47 ug/m3 07/26/23 19:55 75-69-407/26/23 19:551.12 0.460 1 Dichlorodifluoromethane 2.43 ug/m3 07/26/23 19:55 75-71-807/26/23 19:550.989 0.678 1 1,1,2-Trichlorotrifluoroethane 0.742J ug/m3 07/26/23 19:55 76-13-1 J07/26/23 19:551.53 0.608 1 Dichlorotetrafluoroethane ND ug/m3 07/26/23 19:55 76-14-207/26/23 19:551.40 0.622 1 n-Heptane 163 ug/m3 07/26/23 19:55 142-82-507/26/23 19:550.818 0.425 1 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 19:55 87-68-307/26/23 19:556.73 1.12 1 n-Hexane 58.2 ug/m3 07/26/23 19:55 110-54-307/26/23 19:552.22 0.726 1 Isopropylbenzene (Cumene)ND ug/m3 07/26/23 19:55 98-82-807/26/23 19:550.983 0.382 1 Methylene Chloride 1.78 ug/m3 07/26/23 19:55 75-09-207/26/23 19:550.694 0.340 1 2-Hexanone 4.54J ug/m3 07/26/23 19:55 591-78-6 J07/26/23 19:555.11 0.544 1 2-Butanone (MEK)5.28 ug/m3 07/26/23 19:55 78-93-307/26/23 19:553.69 0.240 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 49 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-23 Lab ID: 92679117023 Collected: 07/20/23 14:58 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 19:55 108-10-107/26/23 19:555.12 0.313 1 Methyl methacrylate ND ug/m3 07/26/23 19:55 80-62-607/26/23 19:550.819 0.359 1 Methyl-tert-butyl ether ND ug/m3 07/26/23 19:55 1634-04-407/26/23 19:550.721 0.233 1 Naphthalene ND ug/m3 07/26/23 19:55 91-20-307/26/23 19:553.30 1.83 1 2-Propanol 10.1 ug/m3 07/26/23 19:55 67-63-007/26/23 19:553.07 0.649 1 Propylene 12.3 ug/m3 07/26/23 19:55 115-07-107/26/23 19:552.15 0.160 1 Styrene 7.53 ug/m3 07/26/23 19:55 100-42-507/26/23 19:550.851 0.335 1 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 19:55 79-34-507/26/23 19:551.37 0.511 1 Tetrachloroethene 243 ug/m3 07/26/23 19:55 127-18-407/26/23 19:551.36 0.553 1 Tetrahydrofuran ND ug/m3 07/26/23 19:55 109-99-907/26/23 19:550.590 0.216 1 Toluene 216 ug/m3 07/26/23 19:55 108-88-307/26/23 19:551.88 0.328 1 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 19:55 120-82-107/26/23 19:554.66 1.10 1 1,1,1-Trichloroethane ND ug/m3 07/26/23 19:55 71-55-607/26/23 19:551.09 0.400 1 1,1,2-Trichloroethane ND ug/m3 07/26/23 19:55 79-00-507/26/23 19:551.09 0.422 1 Trichloroethene 2.75 ug/m3 07/26/23 19:55 79-01-607/26/23 19:551.07 0.364 1 1,2,4-Trimethylbenzene 20.9 ug/m3 07/26/23 19:55 95-63-607/26/23 19:550.982 0.375 1 1,3,5-Trimethylbenzene 7.41 ug/m3 07/26/23 19:55 108-67-807/26/23 19:550.982 0.382 1 2,2,4-Trimethylpentane 99.5 ug/m3 07/26/23 19:55 540-84-107/26/23 19:550.934 0.621 1 Vinyl chloride ND ug/m3 07/26/23 19:55 75-01-407/26/23 19:550.511 0.243 1 Vinyl bromide ND ug/m3 07/26/23 19:55 593-60-207/26/23 19:550.875 0.373 1 Vinyl acetate ND ug/m3 07/26/23 19:55 108-05-407/26/23 19:550.704 0.408 1 m&p-Xylene 93.2 ug/m3 07/26/23 19:55 179601-23-107/26/23 19:551.73 0.585 1 o-Xylene 30.9 ug/m3 07/26/23 19:55 95-47-607/26/23 19:550.867 0.359 1 Surrogates 4-Bromofluorobenzene (S)97.2 %07/26/23 19:55 460-00-407/26/23 19:5560.0-140 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 50 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-DUP Lab ID: 92679117024 Collected: 07/20/23 00:00 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 Acetone 28.5J ug/m3 07/26/23 20:30 67-64-1 J07/26/23 20:3029.7 13.9 10 Allyl chloride ND ug/m3 07/26/23 20:30 107-05-107/26/23 20:306.26 3.57 10 Benzene 18.2 ug/m3 07/26/23 20:30 71-43-207/26/23 20:306.39 2.28 10 Benzyl chloride ND ug/m3 07/26/23 20:30 100-44-707/26/23 20:3010.4 3.11 10 Bromodichloromethane ND ug/m3 07/26/23 20:30 75-27-407/26/23 20:3013.4 4.71 10 Bromoform ND ug/m3 07/26/23 20:30 75-25-207/26/23 20:3062.1 7.57 10 Bromomethane ND ug/m3 07/26/23 20:30 74-83-907/26/23 20:307.76 3.81 10 1,3-Butadiene ND ug/m3 07/26/23 20:30 106-99-007/26/23 20:3044.3 2.30 10 Carbon disulfide 30.0 ug/m3 07/26/23 20:30 75-15-007/26/23 20:306.22 3.17 10 Carbon tetrachloride ND ug/m3 07/26/23 20:30 56-23-507/26/23 20:3012.6 4.61 10 Chlorobenzene ND ug/m3 07/26/23 20:30 108-90-707/26/23 20:309.24 3.85 10 Chloroethane ND ug/m3 07/26/23 20:30 75-00-307/26/23 20:305.28 2.63 10 Chloroform ND ug/m3 07/26/23 20:30 67-66-307/26/23 20:309.73 3.49 10 Chloromethane ND ug/m3 07/26/23 20:30 74-87-307/26/23 20:304.13 2.13 10 2-Chlorotoluene ND ug/m3 07/26/23 20:30 95-49-807/26/23 20:3010.3 4.27 10 Cyclohexane ND ug/m3 07/26/23 20:30 110-82-707/26/23 20:306.89 2.59 10 Dibromochloromethane ND ug/m3 07/26/23 20:30 124-48-107/26/23 20:3017.0 6.18 10 1,2-Dibromoethane (EDB)ND ug/m3 07/26/23 20:30 106-93-407/26/23 20:3015.4 5.54 10 1,2-Dichlorobenzene ND ug/m3 07/26/23 20:30 95-50-107/26/23 20:3012.0 7.70 10 1,3-Dichlorobenzene ND ug/m3 07/26/23 20:30 541-73-107/26/23 20:3012.0 10.9 10 1,4-Dichlorobenzene ND ug/m3 07/26/23 20:30 106-46-707/26/23 20:3012.0 3.35 10 1,2-Dichloroethane ND ug/m3 07/26/23 20:30 107-06-207/26/23 20:308.10 2.83 10 1,1-Dichloroethane ND ug/m3 07/26/23 20:30 75-34-307/26/23 20:308.02 2.90 10 1,1-Dichloroethene ND ug/m3 07/26/23 20:30 75-35-407/26/23 20:307.93 3.02 10 cis-1,2-Dichloroethene ND ug/m3 07/26/23 20:30 156-59-207/26/23 20:307.93 3.11 10 trans-1,2-Dichloroethene ND ug/m3 07/26/23 20:30 156-60-507/26/23 20:307.93 2.67 10 1,2-Dichloropropane ND ug/m3 07/26/23 20:30 78-87-507/26/23 20:309.24 3.51 10 cis-1,3-Dichloropropene ND ug/m3 07/26/23 20:30 10061-01-507/26/23 20:309.08 3.13 10 trans-1,3-Dichloropropene ND ug/m3 07/26/23 20:30 10061-02-607/26/23 20:309.08 3.31 10 1,4-Dioxane (p-Dioxane)ND ug/m3 07/26/23 20:30 123-91-107/26/23 20:307.21 3.00 10 Ethanol 57.7 ug/m3 07/26/23 20:30 64-17-5 B07/26/23 20:3047.1 5.00 10 Ethylbenzene 25.2 ug/m3 07/26/23 20:30 100-41-407/26/23 20:308.67 3.62 10 Ethyl acetate ND ug/m3 07/26/23 20:30 141-78-607/26/23 20:307.20 3.60 10 4-Ethyltoluene ND ug/m3 07/26/23 20:30 622-96-807/26/23 20:309.82 3.84 10 Trichlorofluoromethane ND ug/m3 07/26/23 20:30 75-69-407/26/23 20:3011.2 4.60 10 Dichlorodifluoromethane ND ug/m3 07/26/23 20:30 75-71-807/26/23 20:309.89 6.78 10 1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/23 20:30 76-13-107/26/23 20:3015.3 6.08 10 Dichlorotetrafluoroethane ND ug/m3 07/26/23 20:30 76-14-207/26/23 20:3014.0 6.22 10 n-Heptane 95.3 ug/m3 07/26/23 20:30 142-82-507/26/23 20:308.18 4.25 10 Hexachloro-1,3-butadiene ND ug/m3 07/26/23 20:30 87-68-307/26/23 20:3067.3 11.2 10 n-Hexane 12.0J ug/m3 07/26/23 20:30 110-54-3 J07/26/23 20:3022.2 7.26 10 Isopropylbenzene (Cumene)ND ug/m3 07/26/23 20:30 98-82-807/26/23 20:309.83 3.82 10 Methylene Chloride ND ug/m3 07/26/23 20:30 75-09-207/26/23 20:306.94 3.40 10 2-Hexanone ND ug/m3 07/26/23 20:30 591-78-607/26/23 20:3051.1 5.44 10 2-Butanone (MEK)4.84J ug/m3 07/26/23 20:30 78-93-3 J07/26/23 20:3036.9 2.40 10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 51 of 68 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92679117 HNY-001 Sample: SG-DUP Lab ID: 92679117024 Collected: 07/20/23 00:00 Received: 07/25/23 09:30 Matrix: Air Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: TO-15 Preparation Method: TO-15 Pace National - Mt. Juliet VOA (MS) TO-15 4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/23 20:30 108-10-107/26/23 20:3051.2 3.13 10 Methyl methacrylate ND ug/m3 07/26/23 20:30 80-62-607/26/23 20:308.19 3.59 10 Methyl-tert-butyl ether ND ug/m3 07/26/23 20:30 1634-04-407/26/23 20:307.21 2.33 10 Naphthalene ND ug/m3 07/26/23 20:30 91-20-307/26/23 20:3033.0 18.3 10 2-Propanol 10.7J ug/m3 07/26/23 20:30 67-63-0 J07/26/23 20:3030.7 6.49 10 Propylene ND ug/m3 07/26/23 20:30 115-07-107/26/23 20:3021.5 1.60 10 Styrene ND ug/m3 07/26/23 20:30 100-42-507/26/23 20:308.51 3.35 10 1,1,2,2-Tetrachloroethane ND ug/m3 07/26/23 20:30 79-34-507/26/23 20:3013.7 5.11 10 Tetrachloroethene 327 ug/m3 07/26/23 20:30 127-18-407/26/23 20:3013.6 5.53 10 Tetrahydrofuran ND ug/m3 07/26/23 20:30 109-99-907/26/23 20:305.90 2.16 10 Toluene 225 ug/m3 07/26/23 20:30 108-88-307/26/23 20:3018.8 3.28 10 1,2,4-Trichlorobenzene ND ug/m3 07/26/23 20:30 120-82-107/26/23 20:3046.6 11.0 10 1,1,1-Trichloroethane ND ug/m3 07/26/23 20:30 71-55-607/26/23 20:3010.9 4.00 10 1,1,2-Trichloroethane ND ug/m3 07/26/23 20:30 79-00-507/26/23 20:3010.9 4.22 10 Trichloroethene ND ug/m3 07/26/23 20:30 79-01-607/26/23 20:3010.7 3.64 10 1,2,4-Trimethylbenzene 13.8 ug/m3 07/26/23 20:30 95-63-607/26/23 20:309.82 3.75 10 1,3,5-Trimethylbenzene 3.90J ug/m3 07/26/23 20:30 108-67-8 J07/26/23 20:309.82 3.82 10 2,2,4-Trimethylpentane 39.7 ug/m3 07/26/23 20:30 540-84-107/26/23 20:309.34 6.21 10 Vinyl chloride ND ug/m3 07/26/23 20:30 75-01-407/26/23 20:305.11 2.43 10 Vinyl bromide ND ug/m3 07/26/23 20:30 593-60-207/26/23 20:308.75 3.73 10 Vinyl acetate ND ug/m3 07/26/23 20:30 108-05-407/26/23 20:307.04 4.08 10 m&p-Xylene 73.7 ug/m3 07/26/23 20:30 179601-23-107/26/23 20:3017.3 5.85 10 o-Xylene 23.3 ug/m3 07/26/23 20:30 95-47-607/26/23 20:308.67 3.59 10 Surrogates 4-Bromofluorobenzene (S)93.8 %07/26/23 20:30 460-00-407/26/23 20:3060.0-140 10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 52 of 68 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92679117 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2101932 TO-15 TO-15 VOA (MS) TO-15 Laboratory:Pace National - Mt. Juliet Associated Lab Samples:92679117001, 92679117002, 92679117003, 92679117004, 92679117005, 92679117006, 92679117007, 92679117008, 92679117009, 92679117010, 92679117011, 92679117012, 92679117013, 92679117014, 92679117015, 92679117016, 92679117017, 92679117018, 92679117019, 92679117020 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3955937-3 Associated Lab Samples: 92679117001, 92679117002, 92679117003, 92679117004, 92679117005, 92679117006, 92679117007, 92679117008, 92679117009, 92679117010, 92679117011, 92679117012, 92679117013, 92679117014, 92679117015, 92679117016, 92679117017, 92679117018, 92679117019, 92679117020 Matrix: Air AnalyzedMDL Acetone ug/m3 ND 2.97 07/26/23 09:451.39 Allyl chloride ug/m3 ND 0.626 07/26/23 09:450.357 Benzene ug/m3 ND 0.639 07/26/23 09:450.228 Benzyl chloride ug/m3 ND 1.04 07/26/23 09:450.311 Bromodichloromethane ug/m3 ND 1.34 07/26/23 09:450.471 Bromoform ug/m3 ND 6.21 07/26/23 09:450.757 Bromomethane ug/m3 ND 0.776 07/26/23 09:450.381 1,3-Butadiene ug/m3 ND 4.43 07/26/23 09:450.230 Carbon disulfide ug/m3 ND 0.622 07/26/23 09:450.317 Carbon tetrachloride ug/m3 ND 1.26 07/26/23 09:450.461 Chlorobenzene ug/m3 ND 0.924 07/26/23 09:450.385 Chloroethane ug/m3 ND 0.528 07/26/23 09:450.263 Chloroform ug/m3 ND 0.973 07/26/23 09:450.349 Chloromethane ug/m3 ND 0.413 07/26/23 09:450.213 2-Chlorotoluene ug/m3 ND 1.03 07/26/23 09:450.427 Cyclohexane ug/m3 ND 0.689 07/26/23 09:450.259 Dibromochloromethane ug/m3 ND 1.70 07/26/23 09:450.618 1,2-Dibromoethane (EDB)ug/m3 ND 1.54 07/26/23 09:450.554 1,2-Dichlorobenzene ug/m3 ND 1.20 07/26/23 09:450.770 1,3-Dichlorobenzene ug/m3 ND 1.20 07/26/23 09:451.09 1,4-Dichlorobenzene ug/m3 ND 1.20 07/26/23 09:450.335 1,2-Dichloroethane ug/m3 ND 0.810 07/26/23 09:450.283 1,1-Dichloroethane ug/m3 ND 0.802 07/26/23 09:450.290 1,1-Dichloroethene ug/m3 ND 0.793 07/26/23 09:450.302 cis-1,2-Dichloroethene ug/m3 ND 0.793 07/26/23 09:450.311 trans-1,2-Dichloroethene ug/m3 ND 0.793 07/26/23 09:450.267 1,2-Dichloropropane ug/m3 ND 0.924 07/26/23 09:450.351 cis-1,3-Dichloropropene ug/m3 ND 0.908 07/26/23 09:450.313 trans-1,3-Dichloropropene ug/m3 ND 0.908 07/26/23 09:450.331 1,4-Dioxane (p-Dioxane)ug/m3 ND 0.721 07/26/23 09:450.300 Ethanol ug/m3 0.639J 4.71 J07/26/23 09:450.500 Ethylbenzene ug/m3 ND 0.867 07/26/23 09:450.362 Ethyl acetate ug/m3 ND 0.720 07/26/23 09:450.360 4-Ethyltoluene ug/m3 ND 0.982 07/26/23 09:450.384 Trichlorofluoromethane ug/m3 ND 1.12 07/26/23 09:450.460 Dichlorodifluoromethane ug/m3 ND 0.989 07/26/23 09:450.678 1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.53 07/26/23 09:450.608 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 53 of 68 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92679117 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3955937-3 Associated Lab Samples: 92679117001, 92679117002, 92679117003, 92679117004, 92679117005, 92679117006, 92679117007, 92679117008, 92679117009, 92679117010, 92679117011, 92679117012, 92679117013, 92679117014, 92679117015, 92679117016, 92679117017, 92679117018, 92679117019, 92679117020 Matrix: Air AnalyzedMDL Dichlorotetrafluoroethane ug/m3 ND 1.40 07/26/23 09:450.622 n-Heptane ug/m3 ND 0.818 07/26/23 09:450.425 Hexachloro-1,3-butadiene ug/m3 ND 6.73 07/26/23 09:451.12 n-Hexane ug/m3 ND 2.22 07/26/23 09:450.726 Isopropylbenzene (Cumene)ug/m3 ND 0.983 07/26/23 09:450.382 Methylene Chloride ug/m3 ND 0.694 07/26/23 09:450.340 2-Hexanone ug/m3 ND 5.11 07/26/23 09:450.544 2-Butanone (MEK)ug/m3 ND 3.69 07/26/23 09:450.240 4-Methyl-2-pentanone (MIBK)ug/m3 ND 5.12 07/26/23 09:450.313 Methyl methacrylate ug/m3 ND 0.819 07/26/23 09:450.359 Methyl-tert-butyl ether ug/m3 ND 0.721 07/26/23 09:450.233 Naphthalene ug/m3 ND 3.30 07/26/23 09:451.83 2-Propanol ug/m3 ND 3.07 07/26/23 09:450.649 Propylene ug/m3 ND 2.15 07/26/23 09:450.160 Styrene ug/m3 ND 0.851 07/26/23 09:450.335 1,1,2,2-Tetrachloroethane ug/m3 ND 1.37 07/26/23 09:450.511 Tetrachloroethene ug/m3 ND 1.36 07/26/23 09:450.553 Tetrahydrofuran ug/m3 ND 0.590 07/26/23 09:450.216 Toluene ug/m3 ND 1.88 07/26/23 09:450.328 1,2,4-Trichlorobenzene ug/m3 ND 4.66 07/26/23 09:451.10 1,1,1-Trichloroethane ug/m3 ND 1.09 07/26/23 09:450.400 1,1,2-Trichloroethane ug/m3 ND 1.09 07/26/23 09:450.422 Trichloroethene ug/m3 ND 1.07 07/26/23 09:450.364 1,2,4-Trimethylbenzene ug/m3 ND 0.982 07/26/23 09:450.375 1,3,5-Trimethylbenzene ug/m3 ND 0.982 07/26/23 09:450.382 2,2,4-Trimethylpentane ug/m3 ND 0.934 07/26/23 09:450.621 Vinyl chloride ug/m3 ND 0.511 07/26/23 09:450.243 Vinyl bromide ug/m3 ND 0.875 07/26/23 09:450.373 Vinyl acetate ug/m3 ND 0.704 07/26/23 09:450.408 m&p-Xylene ug/m3 ND 1.73 07/26/23 09:450.585 o-Xylene ug/m3 ND 0.867 07/26/23 09:450.359 4-Bromofluorobenzene (S)%99.8 60.0-140 07/26/23 09:45 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3955937-1LABORATORY CONTROL SAMPLE & LCSD: LCSSpike LCSD % Rec RPD Max RPD LCSD Result R3955937-2 Acetone ug/m3 9.348.91 105 70.0-1301079.58 2.51 25 Allyl chloride ug/m3 12.711.7 109 70.0-13010912.8 0.734 25 Benzene ug/m3 12.612.0 105 70.0-13010712.8 2.01 25 Benzyl chloride ug/m3 19.519.5 100 70.0-15299.519.4 0.535 25 Bromodichloromethane ug/m3 26.325.2 105 70.0-13010626.8 1.77 25 Bromoform ug/m3 37.538.8 96.5 70.0-13096.537.5 0.00 25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 54 of 68 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92679117 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3955937-1LABORATORY CONTROL SAMPLE & LCSD: LCSSpike LCSD % Rec RPD Max RPD LCSD Result R3955937-2 Bromomethane ug/m3 14.814.6 102 70.0-13010314.9 1.04 25 1,3-Butadiene ug/m3 8.788.30 106 70.0-1301068.81 0.252 25 Carbon disulfide ug/m3 12.511.7 107 70.0-13011012.9 3.19 25 Carbon tetrachloride ug/m3 24.223.6 103 70.0-13010524.8 2.31 25 Chlorobenzene ug/m3 16.817.3 96.8 70.0-13010117.4 3.78 25 Chloroethane ug/m3 10.69.89 107 70.0-13010910.8 1.98 25 Chloroform ug/m3 19.518.3 107 70.0-13011020.1 2.96 25 Chloromethane ug/m3 8.207.75 106 70.0-1301078.30 1.25 25 2-Chlorotoluene ug/m3 19.719.3 102 70.0-13010520.4 3.35 25 Cyclohexane ug/m3 13.312.9 103 70.0-13010613.7 2.55 25 Dibromochloromethane ug/m3 31.931.9 100 70.0-13010433.3 4.18 25 1,2-Dibromoethane (EDB)ug/m3 29.628.8 103 70.0-13010630.4 2.82 25 1,2-Dichlorobenzene ug/m3 22.722.5 101 70.0-13010122.8 0.528 25 1,3-Dichlorobenzene ug/m3 22.722.5 101 70.0-13010523.7 4.66 25 1,4-Dichlorobenzene ug/m3 23.622.5 105 70.0-13010623.9 1.27 25 1,2-Dichloroethane ug/m3 15.515.2 102 70.0-13010415.8 2.33 25 1,1-Dichloroethane ug/m3 16.615.0 110 70.0-13011116.8 1.20 25 1,1-Dichloroethene ug/m3 16.014.9 108 70.0-13011116.6 3.41 25 cis-1,2-Dichloroethene ug/m3 15.814.9 106 70.0-13010716.0 0.998 25 trans-1,2-Dichloroethene ug/m3 14.614.9 98.1 70.0-13010215.1 3.47 25 1,2-Dichloropropane ug/m3 18.717.3 108 70.0-13011119.3 3.41 25 cis-1,3-Dichloropropene ug/m3 16.717.0 98.1 70.0-13010117.2 2.68 25 trans-1,3-Dichloropropene ug/m3 16.817.0 98.9 70.0-13010217.4 3.44 25 1,4-Dioxane (p-Dioxane)ug/m3 13.513.5 99.7 70.0-14098.413.3 1.35 25 Ethanol ug/m3 7.567.07 107 55.0-1481037.32 3.30 25 Ethylbenzene ug/m3 16.416.3 101 70.0-13010316.7 1.83 25 Ethyl acetate ug/m3 14.113.5 105 70.0-13010714.4 2.02 25 4-Ethyltoluene ug/m3 19.218.4 105 70.0-13010819.8 3.02 25 Trichlorofluoromethane ug/m3 22.521.1 107 70.0-13010923.0 2.22 25 Dichlorodifluoromethane ug/m3 19.018.5 102 64.0-13910419.3 1.55 25 1,1,2-Trichlorotrifluoroethane ug/m3 30.728.7 107 70.0-13010931.3 1.98 25 Dichlorotetrafluoroethane ug/m3 27.426.2 105 70.0-13010627.7 1.02 25 n-Heptane ug/m3 16.315.3 106 70.0-13011016.8 2.96 25 Hexachloro-1,3-butadiene ug/m3 35.040.0 87.5 70.0-15192.336.9 5.34 25 n-Hexane ug/m3 14.313.2 108 70.0-13010914.4 0.736 25 Isopropylbenzene (Cumene)ug/m3 18.518.4 101 70.0-13010319.1 2.88 25 Methylene Chloride ug/m3 14.013.0 107 70.0-13010914.2 1.73 25 2-Hexanone ug/m3 15.615.3 102 70.0-14910616.3 4.35 25 2-Butanone (MEK)ug/m3 11.811.1 107 70.0-13010611.7 1.25 25 4-Methyl-2-pentanone (MIBK)ug/m3 13.815.4 89.6 70.0-13996.514.8 7.45 25 Methyl methacrylate ug/m3 15.615.4 102 70.0-13010315.9 1.82 25 Methyl-tert-butyl ether ug/m3 13.613.5 101 70.0-13010213.8 1.05 25 Naphthalene ug/m3 20.119.6 102 70.0-15910721.0 4.59 25 2-Propanol ug/m3 9.689.22 105 70.0-1391079.83 1.51 25 Propylene ug/m3 6.586.46 102 64.0-1441036.65 1.04 25 Styrene ug/m3 16.416.0 103 70.0-13010516.7 1.80 25 1,1,2,2-Tetrachloroethane ug/m3 28.925.8 112 70.0-13011329.1 0.948 25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 55 of 68 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92679117 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3955937-1LABORATORY CONTROL SAMPLE & LCSD: LCSSpike LCSD % Rec RPD Max RPD LCSD Result R3955937-2 Tetrachloroethene ug/m3 23.225.5 90.9 70.0-13089.122.7 2.07 25 Tetrahydrofuran ug/m3 11.011.1 99.5 70.0-13710111.1 1.07 25 Toluene ug/m3 14.214.1 100 70.0-13010314.5 2.37 25 1,2,4-Trichlorobenzene ug/m3 24.727.8 88.8 70.0-16096.526.8 8.35 25 1,1,1-Trichloroethane ug/m3 20.820.4 102 70.0-13010421.2 1.82 25 1,1,2-Trichloroethane ug/m3 21.220.4 104 70.0-13010721.9 3.29 25 Trichloroethene ug/m3 20.520.1 102 70.0-13010521.2 3.08 25 1,2,4-Trimethylbenzene ug/m3 19.118.4 104 70.0-13010920.0 4.52 25 1,3,5-Trimethylbenzene ug/m3 19.118.4 104 70.0-13010719.7 3.03 25 2,2,4-Trimethylpentane ug/m3 18.717.5 107 70.0-13010919.2 2.22 25 Vinyl chloride ug/m3 10.19.59 106 70.0-13010610.2 0.503 25 Vinyl bromide ug/m3 16.316.4 99.5 70.0-13010417.1 4.46 25 Vinyl acetate ug/m3 13.813.2 104 70.0-13010714.1 2.28 25 m&p-Xylene ug/m3 34.132.5 105 70.0-13010835.1 3.01 25 o-Xylene ug/m3 16.916.3 104 70.0-13010817.5 3.53 25 4-Bromofluorobenzene (S)%101 60.0-140105 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 56 of 68 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92679117 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2101941 TO-15 TO-15 VOA (MS) TO-15 Laboratory:Pace National - Mt. Juliet Associated Lab Samples: 92679117021, 92679117022, 92679117023, 92679117024 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3953345-3 Associated Lab Samples:92679117021, 92679117022, 92679117023, 92679117024 Matrix: Air AnalyzedMDL Acetone ug/m3 ND 2.97 07/26/23 10:001.39 Allyl chloride ug/m3 ND 0.626 07/26/23 10:000.357 Benzene ug/m3 ND 0.639 07/26/23 10:000.228 Benzyl chloride ug/m3 ND 1.04 07/26/23 10:000.311 Bromodichloromethane ug/m3 ND 1.34 07/26/23 10:000.471 Bromoform ug/m3 ND 6.21 07/26/23 10:000.757 Bromomethane ug/m3 ND 0.776 07/26/23 10:000.381 1,3-Butadiene ug/m3 ND 4.43 07/26/23 10:000.230 Carbon disulfide ug/m3 ND 0.622 07/26/23 10:000.317 Carbon tetrachloride ug/m3 ND 1.26 07/26/23 10:000.461 Chlorobenzene ug/m3 ND 0.924 07/26/23 10:000.385 Chloroethane ug/m3 ND 0.528 07/26/23 10:000.263 Chloroform ug/m3 ND 0.973 07/26/23 10:000.349 Chloromethane ug/m3 ND 0.413 07/26/23 10:000.213 2-Chlorotoluene ug/m3 ND 1.03 07/26/23 10:000.427 Cyclohexane ug/m3 ND 0.689 07/26/23 10:000.259 Dibromochloromethane ug/m3 ND 1.70 07/26/23 10:000.618 1,2-Dibromoethane (EDB)ug/m3 ND 1.54 07/26/23 10:000.554 1,2-Dichlorobenzene ug/m3 ND 1.20 07/26/23 10:000.770 1,3-Dichlorobenzene ug/m3 ND 1.20 07/26/23 10:001.09 1,4-Dichlorobenzene ug/m3 ND 1.20 07/26/23 10:000.335 1,2-Dichloroethane ug/m3 ND 0.810 07/26/23 10:000.283 1,1-Dichloroethane ug/m3 ND 0.802 07/26/23 10:000.290 1,1-Dichloroethene ug/m3 ND 0.793 07/26/23 10:000.302 cis-1,2-Dichloroethene ug/m3 ND 0.793 07/26/23 10:000.311 trans-1,2-Dichloroethene ug/m3 ND 0.793 07/26/23 10:000.267 1,2-Dichloropropane ug/m3 ND 0.924 07/26/23 10:000.351 cis-1,3-Dichloropropene ug/m3 ND 0.908 07/26/23 10:000.313 trans-1,3-Dichloropropene ug/m3 ND 0.908 07/26/23 10:000.331 1,4-Dioxane (p-Dioxane)ug/m3 ND 0.721 07/26/23 10:000.300 Ethanol ug/m3 0.994J 4.71 J07/26/23 10:000.500 Ethylbenzene ug/m3 ND 0.867 07/26/23 10:000.362 Ethyl acetate ug/m3 ND 0.720 07/26/23 10:000.360 4-Ethyltoluene ug/m3 ND 0.982 07/26/23 10:000.384 Trichlorofluoromethane ug/m3 ND 1.12 07/26/23 10:000.460 Dichlorodifluoromethane ug/m3 ND 0.989 07/26/23 10:000.678 1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.53 07/26/23 10:000.608 Dichlorotetrafluoroethane ug/m3 ND 1.40 07/26/23 10:000.622 n-Heptane ug/m3 ND 0.818 07/26/23 10:000.425 Hexachloro-1,3-butadiene ug/m3 ND 6.73 07/26/23 10:001.12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 57 of 68 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92679117 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3953345-3 Associated Lab Samples:92679117021, 92679117022, 92679117023, 92679117024 Matrix: Air AnalyzedMDL n-Hexane ug/m3 ND 2.22 07/26/23 10:000.726 Isopropylbenzene (Cumene)ug/m3 ND 0.983 07/26/23 10:000.382 Methylene Chloride ug/m3 ND 0.694 07/26/23 10:000.340 2-Hexanone ug/m3 ND 5.11 07/26/23 10:000.544 2-Butanone (MEK)ug/m3 ND 3.69 07/26/23 10:000.240 4-Methyl-2-pentanone (MIBK)ug/m3 ND 5.12 07/26/23 10:000.313 Methyl methacrylate ug/m3 ND 0.819 07/26/23 10:000.359 Methyl-tert-butyl ether ug/m3 ND 0.721 07/26/23 10:000.233 Naphthalene ug/m3 ND 3.30 07/26/23 10:001.83 2-Propanol ug/m3 ND 3.07 07/26/23 10:000.649 Propylene ug/m3 ND 2.15 07/26/23 10:000.160 Styrene ug/m3 ND 0.851 07/26/23 10:000.335 1,1,2,2-Tetrachloroethane ug/m3 ND 1.37 07/26/23 10:000.511 Tetrachloroethene ug/m3 ND 1.36 07/26/23 10:000.553 Tetrahydrofuran ug/m3 ND 0.590 07/26/23 10:000.216 Toluene ug/m3 ND 1.88 07/26/23 10:000.328 1,2,4-Trichlorobenzene ug/m3 ND 4.66 07/26/23 10:001.10 1,1,1-Trichloroethane ug/m3 ND 1.09 07/26/23 10:000.400 1,1,2-Trichloroethane ug/m3 ND 1.09 07/26/23 10:000.422 Trichloroethene ug/m3 ND 1.07 07/26/23 10:000.364 1,2,4-Trimethylbenzene ug/m3 ND 0.982 07/26/23 10:000.375 1,3,5-Trimethylbenzene ug/m3 ND 0.982 07/26/23 10:000.382 2,2,4-Trimethylpentane ug/m3 ND 0.934 07/26/23 10:000.621 Vinyl chloride ug/m3 ND 0.511 07/26/23 10:000.243 Vinyl bromide ug/m3 ND 0.875 07/26/23 10:000.373 Vinyl acetate ug/m3 ND 0.704 07/26/23 10:000.408 m&p-Xylene ug/m3 ND 1.73 07/26/23 10:000.585 o-Xylene ug/m3 ND 0.867 07/26/23 10:000.359 4-Bromofluorobenzene (S)%95.5 60.0-140 07/26/23 10:00 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3953345-1LABORATORY CONTROL SAMPLE & LCSD: LCSSpike LCSD % Rec RPD Max RPD LCSD Result R3953345-2 Acetone ug/m3 9.418.91 106 70.0-1301069.46 0.504 25 Allyl chloride ug/m3 12.311.7 105 70.0-13010512.3 0.00 25 Benzene ug/m3 13.512.0 113 70.0-13011313.5 0.236 25 Benzyl chloride ug/m3 23.119.5 118 70.0-15211823.0 0.451 25 Bromodichloromethane ug/m3 28.225.2 112 70.0-13011228.2 0.00 25 Bromoform ug/m3 44.138.8 114 70.0-13011343.9 0.471 25 Bromomethane ug/m3 14.814.6 102 70.0-13010214.9 0.784 25 1,3-Butadiene ug/m3 8.988.30 108 70.0-1301169.60 6.67 25 Carbon disulfide ug/m3 13.311.7 114 70.0-13011413.3 0.234 25 Carbon tetrachloride ug/m3 25.623.6 108 70.0-13010825.6 0.00 25 Chlorobenzene ug/m3 19.817.3 114 70.0-13011419.8 0.00 25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 58 of 68 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92679117 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3953345-1LABORATORY CONTROL SAMPLE & LCSD: LCSSpike LCSD % Rec RPD Max RPD LCSD Result R3953345-2 Chloroethane ug/m3 9.379.89 94.7 70.0-13095.29.42 0.562 25 Chloroform ug/m3 19.818.3 108 70.0-13010919.8 0.246 25 Chloromethane ug/m3 8.267.75 107 70.0-1301068.22 0.501 25 2-Chlorotoluene ug/m3 21.919.3 113 70.0-13011422.0 0.471 25 Cyclohexane ug/m3 13.912.9 108 70.0-13011014.2 1.71 25 Dibromochloromethane ug/m3 36.931.9 116 70.0-13011536.7 0.694 25 1,2-Dibromoethane (EDB)ug/m3 33.128.8 115 70.0-13011533.2 0.232 25 1,2-Dichlorobenzene ug/m3 25.922.5 115 70.0-13011425.8 0.465 25 1,3-Dichlorobenzene ug/m3 25.722.5 114 70.0-13011425.6 0.468 25 1,4-Dichlorobenzene ug/m3 26.822.5 119 70.0-13011826.7 0.225 25 1,2-Dichloroethane ug/m3 15.715.2 103 70.0-13010315.6 0.518 25 1,1-Dichloroethane ug/m3 16.215.0 107 70.0-13010916.4 1.23 25 1,1-Dichloroethene ug/m3 15.914.9 107 70.0-13010816.1 0.990 25 cis-1,2-Dichloroethene ug/m3 15.014.9 101 70.0-13010215.2 1.57 25 trans-1,2-Dichloroethene ug/m3 16.114.9 108 70.0-13010816.1 0.247 25 1,2-Dichloropropane ug/m3 19.317.3 111 70.0-13011119.2 0.480 25 cis-1,3-Dichloropropene ug/m3 19.617.0 115 70.0-13011519.7 0.463 25 trans-1,3-Dichloropropene ug/m3 18.517.0 109 70.0-13010718.3 0.988 25 1,4-Dioxane (p-Dioxane)ug/m3 15.213.5 113 70.0-14011215.2 0.237 25 Ethanol ug/m3 6.137.07 86.7 55.0-14890.46.39 4.22 25 Ethylbenzene ug/m3 17.916.3 110 70.0-13011017.9 0.484 25 Ethyl acetate ug/m3 14.213.5 105 70.0-13010414.0 1.28 25 4-Ethyltoluene ug/m3 21.118.4 114 70.0-13011421.1 0.00 25 Trichlorofluoromethane ug/m3 18.721.1 88.5 70.0-13010121.4 13.5 25 Dichlorodifluoromethane ug/m3 19.618.5 106 64.0-13910920.1 2.49 25 1,1,2-Trichlorotrifluoroethane ug/m3 32.428.7 113 70.0-13011332.5 0.236 25 Dichlorotetrafluoroethane ug/m3 29.426.2 112 70.0-13011129.2 0.955 25 n-Heptane ug/m3 17.115.3 112 70.0-13011117.1 0.239 25 Hexachloro-1,3-butadiene ug/m3 46.040.0 115 70.0-15111546.0 0.00 25 n-Hexane ug/m3 14.313.2 109 70.0-13010814.3 0.246 25 Isopropylbenzene (Cumene)ug/m3 20.318.4 110 70.0-13011020.3 0.00 25 Methylene Chloride ug/m3 13.513.0 103 70.0-13010313.5 0.00 25 2-Hexanone ug/m3 17.215.3 112 70.0-14910115.5 10.3 25 2-Butanone (MEK)ug/m3 12.111.1 110 70.0-13010912.1 0.731 25 4-Methyl-2-pentanone (MIBK)ug/m3 16.715.4 109 70.0-13910816.6 0.246 25 Methyl methacrylate ug/m3 16.315.4 106 70.0-13010616.3 0.252 25 Methyl-tert-butyl ether ug/m3 14.413.5 107 70.0-13010714.4 0.250 25 Naphthalene ug/m3 24.019.6 122 70.0-15912123.8 0.657 25 2-Propanol ug/m3 9.839.22 107 70.0-1391069.78 0.501 25 Propylene ug/m3 6.876.46 106 64.0-1441066.82 0.755 25 Styrene ug/m3 18.016.0 113 70.0-13011318.0 0.00 25 1,1,2,2-Tetrachloroethane ug/m3 29.125.8 113 70.0-13011429.3 0.471 25 Tetrachloroethene ug/m3 28.625.5 112 70.0-13011228.6 0.00 25 Tetrahydrofuran ug/m3 11.811.1 107 70.0-13710711.8 0.250 25 Toluene ug/m3 15.914.1 113 70.0-13011316.0 0.236 25 1,2,4-Trichlorobenzene ug/m3 33.227.8 120 70.0-16012033.2 0.00 25 1,1,1-Trichloroethane ug/m3 22.420.4 110 70.0-13010922.2 0.733 25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 59 of 68 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92679117 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3953345-1LABORATORY CONTROL SAMPLE & LCSD: LCSSpike LCSD % Rec RPD Max RPD LCSD Result R3953345-2 1,1,2-Trichloroethane ug/m3 23.220.4 114 70.0-13011423.2 0.00 25 Trichloroethene ug/m3 22.420.1 111 70.0-13011122.2 0.720 25 1,2,4-Trimethylbenzene ug/m3 21.018.4 114 70.0-13011320.8 0.705 25 1,3,5-Trimethylbenzene ug/m3 21.318.4 116 70.0-13011421.1 1.16 25 2,2,4-Trimethylpentane ug/m3 19.217.5 109 70.0-13010919.2 0.00 25 Vinyl chloride ug/m3 11.19.59 116 70.0-13012311.8 5.82 25 Vinyl bromide ug/m3 12.016.4 73.3 70.0-13093.915.4 24.6 25 Vinyl acetate ug/m3 14.513.2 110 70.0-13010614.0 3.71 25 m&p-Xylene ug/m3 36.832.5 113 70.0-13011336.9 0.118 25 o-Xylene ug/m3 17.816.3 110 70.0-13011017.9 0.243 25 4-Bromofluorobenzene (S)%95.6 60.0-14095.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 60 of 68 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92679117 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2106382 TO-15 TO-15 VOA (MS) TO-15 Laboratory:Pace National - Mt. Juliet Associated Lab Samples: 92679117006, 92679117010, 92679117011 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3956231-1 Associated Lab Samples:92679117006, 92679117010, 92679117011 Matrix: Air AnalyzedMDL Carbon disulfide ug/m3 ND 0.622 08/02/23 10:550.317 1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.53 08/02/23 10:550.608 n-Heptane ug/m3 ND 0.818 08/02/23 10:550.425 Toluene ug/m3 ND 1.88 08/02/23 10:550.328 4-Bromofluorobenzene (S)%94.3 60.0-140 08/02/23 10:55 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3956231-2LABORATORY CONTROL SAMPLE & LCSD: LCSSpike LCSD % Rec RPD Max RPD LCSD Result R3956231-3 Carbon disulfide ug/m3 11.111.7 94.9 70.0-13094.911.1 0.00 25 1,1,2-Trichlorotrifluoroethane ug/m3 29.728.7 103 70.0-13010730.7 3.05 25 n-Heptane ug/m3 14.415.3 93.6 70.0-13089.913.8 4.07 25 Toluene ug/m3 14.114.1 99.7 70.0-13010114.3 1.33 25 4-Bromofluorobenzene (S)%99.3 60.0-140102 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 61 of 68 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92679117 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2107030 TO-15 TO-15 VOA (MS) TO-15 Laboratory:Pace National - Mt. Juliet Associated Lab Samples: 92679117008 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3956405-3 Associated Lab Samples:92679117008 Matrix: Air AnalyzedMDL Trichlorofluoromethane ug/m3 ND 1.12 08/03/23 10:040.460 4-Bromofluorobenzene (S)%96.5 60.0-140 08/03/23 10:04 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3956405-1LABORATORY CONTROL SAMPLE & LCSD: LCSSpike LCSD % Rec RPD Max RPD LCSD Result R3956405-2 Trichlorofluoromethane ug/m3 21.621.1 103 70.0-13010221.5 0.782 25 4-Bromofluorobenzene (S)%96.6 60.0-14096.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 62 of 68 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92679117 HNY-001 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2107072 TO-15 TO-15 VOA (MS) TO-15 Laboratory:Pace National - Mt. Juliet Associated Lab Samples: 92679117014 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3956465-3 Associated Lab Samples:92679117014 Matrix: Air AnalyzedMDL Toluene ug/m3 ND 1.88 08/03/23 10:090.328 4-Bromofluorobenzene (S)%98.5 60.0-140 08/03/23 10:09 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3956465-1LABORATORY CONTROL SAMPLE & LCSD: LCSSpike LCSD % Rec RPD Max RPD LCSD Result R3956465-2 Toluene ug/m3 14.814.1 105 70.0-13010715.1 1.76 25 4-Bromofluorobenzene (S)%99.2 60.0-14098.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 63 of 68 #=QL# QUALIFIERS Pace Project No.: Project: 92679117 HNY-001 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. SAMPLE QUALIFIERS Sample: 92679117019 Volatile Organic Compounds (MS) by Method TO-15 - Non-target compounds too high to run at a lower dilution.[1] ANALYTE QUALIFIERS Analyte was detected in the associated method blank.B Analyte concentration exceeded the calibration range. The reported result is estimated.E Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 64 of 68 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92679117 HNY-001 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92679117001 2101932 2101932SG-1 TO-15 TO-15 92679117002 2101932 2101932SG-2 TO-15 TO-15 92679117003 2101932 2101932SG-3 TO-15 TO-15 92679117004 2101932 2101932SG-4 TO-15 TO-15 92679117005 2101932 2101932SG-5 TO-15 TO-15 92679117006 2101932 2101932SG-6 TO-15 TO-15 92679117006 2106382 2106382SG-6 TO-15 TO-15 92679117007 2101932 2101932SG-7 TO-15 TO-15 92679117008 2101932 2101932SG-8 TO-15 TO-15 92679117008 2107030 2107030SG-8 TO-15 TO-15 92679117009 2101932 2101932SG-9 TO-15 TO-15 92679117010 2101932 2101932SG-10 TO-15 TO-15 92679117010 2106382 2106382SG-10 TO-15 TO-15 92679117011 2101932 2101932SG-11 TO-15 TO-15 92679117011 2106382 2106382SG-11 TO-15 TO-15 92679117012 2101932 2101932SG-12 TO-15 TO-15 92679117013 2101932 2101932SG-13 TO-15 TO-15 92679117014 2101932 2101932SG-14 TO-15 TO-15 92679117014 2107072 2107072SG-14 TO-15 TO-15 92679117015 2101932 2101932SG-15 TO-15 TO-15 92679117016 2101932 2101932SG-16 TO-15 TO-15 92679117017 2101932 2101932SG-17 TO-15 TO-15 92679117018 2101932 2101932SG-18 TO-15 TO-15 92679117019 2101932 2101932SG-19 TO-15 TO-15 92679117020 2101932 2101932SG-20 TO-15 TO-15 92679117021 2101941 2101941SG-21 TO-15 TO-15 92679117022 2101941 2101941SG-22 TO-15 TO-15 92679117023 2101941 2101941SG-23 TO-15 TO-15 92679117024 2101941 2101941SG-DUP TO-15 TO-15 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 08/03/2023 04:30 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 65 of 68 Page 66 of 68 Page 67 of 68 Page 68 of 68 Appendix C Groundwater and Soil Gas Sampling Forms 6?%%%0DVWHU7HPSODWHV?)RUPV3)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI /DVW8SGDWHG5263Job No:Well ID:Water Volume PXUJingDOTemp. 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Cond. pH ORP TurbidityTimeLevelPuUJHGRate(mg//)(oC)(PS/cm)(SU)(mV)(NTU)*HQHUDOL]HGStabilization CriteriaLOW-FLOW GROUNDWATER Other)LHOGParameters:B__________________________________________________________________________________________________BParameters taken with:Field Filtration: YesNoSAMPLING RECORD 'DWH: GROUNDWATER),(/'PARAMETERSStabilization criteria guidelines from the EPA 5HJLRQ/6$SD Operating Procedure for Groundwater SamplingApril 22, 2023.6WDELOL]DWLRQRFFXUVZKHQSDUDPHWHUVDUHVWDEOHIRUWKUHHFRQVHFXWLYHUHDGLQJVPHDVXUHGDWDSSUR[LPDWHO\ILYHPLQXWHLQWHUYDOV7KHDERYHVWDELOL]DWLRQFULWHULDPD\YDU\EDVHGRQUHJXODWRU\SURJUDPDQGRUVLWHFRQGLWLRQV&KHFNZLWK3URMHFW0DQDJHUIRUVLWHVSHFLILFUHTXLUHPHQWV7XUELGLW\YDOXHV178VPD\EHUHTXLUHGIRUVHOHFWDQDO\VHVHJPHWDOV,IVWDELOL]DWLRQFULWHULDLVQRWDWWDLQDEOHFRQWDFW3URMHFW0DQDJHUTurbLGLW\ 178VRU VWDELOL]HGWater Level: slight DQG stabledrawdown IWpH +/- 0.1 68SSHFLILFCondXFWLYLW\ +/- 5% DLVVROYHGO[\JHQ +/- 0.2 mg/L6LWH1DPH: 6LWH/RFDWLRQ::6DPSOLQJ3HUVRQQHO___________________, _____________________ :HDWKHU:Well Diameter:7RWDO:HOO'HSWKIW____________6FUHHQ,QWHUYDOIW'HSWKWR:DWHUIW7XELQJ0DWHULDOT\SHRI3XPS&DVLQJ0DWHULDO7RSRI&DVLQJ(OHYDWLRQIWPVO3XPS7XELQJVHWDW (ft)127(66DPSOHGDW6DPSOH&RQGLWLRQ&OHDU&ORXG\ 2WKHUIfyes, which sample parameters were field filtered:6DPSOH'HOLYHUHGWR$QDO\WLFDOPDUDPHWHUVDQG&RQWDLQHUV7\SHV1XPEHURI&RQWDLQHUV3UHVHUYDWLYHVHNY.001Pharr Yarns - Lowell7/20/23Lowell,NCDJH3026Beganpumping@1520.15:2515:3015:3515:4022.6822.6922.6922.70500 mL1000 mL1500 mL2000 mL100 mL/min100 mL/min100 mL/min100 mL/min24.2024.5023.9023.80231.5231.0232.5234.75.65.65.55.660.5067.8072.4073.1032.610.79.710.02.302.402.522.58YSI Pro Plus & HACH 2100Q40 mL VOAs w/HCl(x3 - 8260 VOCs);100 mL amber unpres.(x2 - 8270 SVOCs); 250 mLplastic w/ HNO3(x1 - 6020/7470 RCRA Metals)PeristalticPVC15:40TMW-7/TMW-DUP1530PolyethyleneTOC22.5189°F,Clear SkiesTOCSMT2-inTOCClear 6?%%%0DVWHU7HPSODWHV?)RUPV3)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI /DVW8SGDWHG5263Job No:Well ID:Water Volume PXUJingDOTemp. 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Cond. pH ORP TurbidityTimeLevelPuUJHGRate(mg//)(oC)(PS/cm)(SU)(mV)(NTU)*HQHUDOL]HGStabilization CriteriaLOW-FLOW GROUNDWATER Other)LHOGParameters:B__________________________________________________________________________________________________BParameters taken with:Field Filtration: YesNoSAMPLING RECORD 'DWH: GROUNDWATER),(/'PARAMETERSStabilization criteria guidelines from the EPA 5HJLRQ/6$SD Operating Procedure for Groundwater SamplingApril 22, 2023.6WDELOL]DWLRQRFFXUVZKHQSDUDPHWHUVDUHVWDEOHIRUWKUHHFRQVHFXWLYHUHDGLQJVPHDVXUHGDWDSSUR[LPDWHO\ILYHPLQXWHLQWHUYDOV7KHDERYHVWDELOL]DWLRQFULWHULDPD\YDU\EDVHGRQUHJXODWRU\SURJUDPDQGRUVLWHFRQGLWLRQV&KHFNZLWK3URMHFW0DQDJHUIRUVLWHVSHFLILFUHTXLUHPHQWV7XUELGLW\YDOXHV178VPD\EHUHTXLUHGIRUVHOHFWDQDO\VHVHJPHWDOV,IVWDELOL]DWLRQFULWHULDLVQRWDWWDLQDEOHFRQWDFW3URMHFW0DQDJHUTurbLGLW\ 178VRU VWDELOL]HGWater Level: slight DQG stabledrawdown IWpH +/- 0.1 68SSHFLILFCondXFWLYLW\ +/- 5% DLVVROYHGO[\JHQ +/- 0.2 mg/L6LWH1DPH: 6LWH/RFDWLRQ::6DPSOLQJ3HUVRQQHO___________________, _____________________ :HDWKHU:Well Diameter:7RWDO:HOO'HSWKIW____________6FUHHQ,QWHUYDOIW'HSWKWR:DWHUIW7XELQJ0DWHULDOT\SHRI3XPS&DVLQJ0DWHULDO7RSRI&DVLQJ(OHYDWLRQIWPVO3XPS7XELQJVHWDW (ft)127(66DPSOHGDW6DPSOH&RQGLWLRQ&OHDU&ORXG\ 2WKHUIfyes, which sample parameters were field filtered:6DPSOH'HOLYHUHGWR$QDO\WLFDOPDUDPHWHUVDQG&RQWDLQHUV7\SHV1XPEHURI&RQWDLQHUV3UHVHUYDWLYHVHNY.001Pharr Yarns - Lowell7/20/23Lowell,NCDJH3025Beganpumping@162516:3016:3516:4016:4520.7920.9821.0321.10500 mL1000 mL1500 mL2000 mL100 mL/min100 mL/min100 mL/min100 mL/min20.8020.7020.8020.60146.7145.4145.3144.65.75.75.75.760.5066.4070.3076.2011.36.24.93.12.552.572.632.61YSI Pro Plus & HACH 2100Q40 mL VOAs w/HCl(x3 - 8260 VOCs);100 mL amber unpres.(x2 - 8270 SVOCs); 250 mLplastic w/ HNO3(x1 - 6020/7470 RCRA Metals)PeristalticPVC16:45TMW-81530PolyethyleneTOC20.0089°F,Clear SkiesTOCSMT2-inTOCClear 6?%%%0DVWHU7HPSODWHV?)RUPV3)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI /DVW8SGDWHG5263Job No:Well ID:Water Volume PXUJingDOTemp. 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Cond. pH ORP TurbidityTimeLevelPuUJHGRate(mg//)(oC)(PS/cm)(SU)(mV)(NTU)*HQHUDOL]HGStabilization CriteriaLOW-FLOW GROUNDWATER Other)LHOGParameters:B__________________________________________________________________________________________________BParameters taken with:Field Filtration: YesNoSAMPLING RECORD 'DWH: GROUNDWATER),(/'PARAMETERSStabilization criteria guidelines from the EPA 5HJLRQ/6$SD Operating Procedure for Groundwater SamplingApril 22, 2023.6WDELOL]DWLRQRFFXUVZKHQSDUDPHWHUVDUHVWDEOHIRUWKUHHFRQVHFXWLYHUHDGLQJVPHDVXUHGDWDSSUR[LPDWHO\ILYHPLQXWHLQWHUYDOV7KHDERYHVWDELOL]DWLRQFULWHULDPD\YDU\EDVHGRQUHJXODWRU\SURJUDPDQGRUVLWHFRQGLWLRQV&KHFNZLWK3URMHFW0DQDJHUIRUVLWHVSHFLILFUHTXLUHPHQWV7XUELGLW\YDOXHV178VPD\EHUHTXLUHGIRUVHOHFWDQDO\VHVHJPHWDOV,IVWDELOL]DWLRQFULWHULDLVQRWDWWDLQDEOHFRQWDFW3URMHFW0DQDJHUTurbLGLW\ 178VRU VWDELOL]HGWater Level: slight DQG stabledrawdown IWpH +/- 0.1 68SSHFLILFCondXFWLYLW\ +/- 5% DLVVROYHGO[\JHQ +/- 0.2 mg/L6LWH1DPH: 6LWH/RFDWLRQ::6DPSOLQJ3HUVRQQHO___________________, _____________________ :HDWKHU:Well Diameter:7RWDO:HOO'HSWKIW____________6FUHHQ,QWHUYDOIW'HSWKWR:DWHUIW7XELQJ0DWHULDOT\SHRI3XPS&DVLQJ0DWHULDO7RSRI&DVLQJ(OHYDWLRQIWPVO3XPS7XELQJVHWDW (ft)127(66DPSOHGDW6DPSOH&RQGLWLRQ&OHDU&ORXG\ 2WKHUIfyes, which sample parameters were field filtered:6DPSOH'HOLYHUHGWR$QDO\WLFDOPDUDPHWHUVDQG&RQWDLQHUV7\SHV1XPEHURI&RQWDLQHUV3UHVHUYDWLYHVHNY.001Pharr Yarns - Lowell7/20/23Lowell,NCDJH2524.5Beganpumping@15:4515:5015:5516:0016:0516:1016:1516:2023.4323.5323.6523.7723.8523.9123.960.75 L1.5 L2.0 L2.5 L3.0 L3.5 L4.0 L150 mL/min150 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min18.2017.9018.3018.9019.4019.6019.80315.8305.8298.5295.5297.0293.4286.95.25.25.35.45.45.45.4212.30218.80219.90220.30225.30228.80235.601.61.31.72.12.72.62.17.397.306.846.196.065.876.01YSI Pro Plus & HACH 2100Q40 mL VOAs w/HCl(x3 - 8260 VOCs);100 mL amber unpres.(x2 - 8270 SVOCs); 250 mLplastic w/ HNO3(x1 - 6020/7470 RCRA Metals)PeristalticPVC16:20TMW-91025PolyethyleneTOC23.1689°F,Clear SkiesTOCSMT2-inTOC 6?%%%0DVWHU7HPSODWHV?)RUPV3)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI /DVW8SGDWHG5263Job No:Well ID:Water Volume PXUJingDOTemp. 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Cond. pH ORP TurbidityTimeLevelPuUJHGRate(mg//)(oC)(PS/cm)(SU)(mV)(NTU)*HQHUDOL]HGStabilization CriteriaLOW-FLOW GROUNDWATER Other)LHOGParameters:B__________________________________________________________________________________________________BParameters taken with:Field Filtration: YesNoSAMPLING RECORD 'DWH: GROUNDWATER),(/'PARAMETERSStabilization criteria guidelines from the EPA 5HJLRQ/6$SD Operating Procedure for Groundwater SamplingApril 22, 2023.6WDELOL]DWLRQRFFXUVZKHQSDUDPHWHUVDUHVWDEOHIRUWKUHHFRQVHFXWLYHUHDGLQJVPHDVXUHGDWDSSUR[LPDWHO\ILYHPLQXWHLQWHUYDOV7KHDERYHVWDELOL]DWLRQFULWHULDPD\YDU\EDVHGRQUHJXODWRU\SURJUDPDQGRUVLWHFRQGLWLRQV&KHFNZLWK3URMHFW0DQDJHUIRUVLWHVSHFLILFUHTXLUHPHQWV7XUELGLW\YDOXHV178VPD\EHUHTXLUHGIRUVHOHFWDQDO\VHVHJPHWDOV,IVWDELOL]DWLRQFULWHULDLVQRWDWWDLQDEOHFRQWDFW3URMHFW0DQDJHUTurbLGLW\ 178VRU VWDELOL]HGWater Level: slight DQG stabledrawdown IWpH +/- 0.1 68SSHFLILFCondXFWLYLW\ +/- 5% DLVVROYHGO[\JHQ +/- 0.2 mg/L6LWH1DPH: 6LWH/RFDWLRQ::6DPSOLQJ3HUVRQQHO___________________, _____________________ :HDWKHU:Well Diameter:7RWDO:HOO'HSWKIW____________6FUHHQ,QWHUYDOIW'HSWKWR:DWHUIW7XELQJ0DWHULDOT\SHRI3XPS&DVLQJ0DWHULDO7RSRI&DVLQJ(OHYDWLRQIWPVO3XPS7XELQJVHWDW (ft)127(66DPSOHGDW6DPSOH&RQGLWLRQ&OHDU&ORXG\ 2WKHUIfyes, which sample parameters were field filtered:6DPSOH'HOLYHUHGWR$QDO\WLFDOPDUDPHWHUVDQG&RQWDLQHUV7\SHV1XPEHURI&RQWDLQHUV3UHVHUYDWLYHVHNY.001Pharr Yarns - Lowell7/20/23Lowell,NCDJH3029.80Beganpumping@091009:1509:2009:2509:3009:3509:4009:4509:5009:5510:0010:0529.2129.3029.4229.5029.5929.5929.6129.6129.6129.7129.82250 mL500 mL750 mL1000 mL1250 mL1500 mL1750 mL2000 mL2250 mL2500 mL2750 mL50 mL/min50 mL/min50 mL/min50 mL/min50 mL/min50 mL/min50 mL/min50 mL/min50 mL/min50 mL/min50 mL/min24.5026.3025.8023.6024.1023.4024.9025.9026.8027.6027.00151.0147.5149.5162.5153.098.9100.1101.1102.2103.6104.06.16.16.26.06.05.75.65.75.75.893.5075.0056.9051.7051.1086.9099.5090.7089.8083.9073.8074.676.480.7129.060.122.717.818.720.518.121.43.592.842.892.622.372.382.132.001.861.811.91YSI Pro Plus & HACH 2100QTurbidityfiltered for RCRA metals.40 mL VOAs w/HCl(x3 - 8260 VOCs);100 mL amber unpres.(x2 - 8270 SVOCs); 250 mLplastic w/ HNO3(x1 - 6020/7470 RCRA Metals)PeristalticPVC10:05TMW-101530PolyethyleneTOC5.729.1289°F,Clear SkiesTOCSMT2-inTOCClear 6?%%%0DVWHU7HPSODWHV?)RUPV3)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI /DVW8SGDWHG5263Job No:Well ID:Water Volume PXUJingDOTemp. 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Cond. pH ORP TurbidityTimeLevelPuUJHGRate(mg//)(oC)(PS/cm)(SU)(mV)(NTU)*HQHUDOL]HGStabilization CriteriaLOW-FLOW GROUNDWATER Other)LHOGParameters:B__________________________________________________________________________________________________BParameters taken with:Field Filtration: YesNoSAMPLING RECORD 'DWH: GROUNDWATER),(/'PARAMETERSStabilization criteria guidelines from the EPA 5HJLRQ/6$SD Operating Procedure for Groundwater SamplingApril 22, 2023.6WDELOL]DWLRQRFFXUVZKHQSDUDPHWHUVDUHVWDEOHIRUWKUHHFRQVHFXWLYHUHDGLQJVPHDVXUHGDWDSSUR[LPDWHO\ILYHPLQXWHLQWHUYDOV7KHDERYHVWDELOL]DWLRQFULWHULDPD\YDU\EDVHGRQUHJXODWRU\SURJUDPDQGRUVLWHFRQGLWLRQV&KHFNZLWK3URMHFW0DQDJHUIRUVLWHVSHFLILFUHTXLUHPHQWV7XUELGLW\YDOXHV178VPD\EHUHTXLUHGIRUVHOHFWDQDO\VHVHJPHWDOV,IVWDELOL]DWLRQFULWHULDLVQRWDWWDLQDEOHFRQWDFW3URMHFW0DQDJHUTurbLGLW\ 178VRU VWDELOL]HGWater Level: slight DQG stabledrawdown IWpH +/- 0.1 68SSHFLILFCondXFWLYLW\ +/- 5% DLVVROYHGO[\JHQ +/- 0.2 mg/L6LWH1DPH: 6LWH/RFDWLRQ::6DPSOLQJ3HUVRQQHO___________________, _____________________ :HDWKHU:Well Diameter:7RWDO:HOO'HSWKIW____________6FUHHQ,QWHUYDOIW'HSWKWR:DWHUIW7XELQJ0DWHULDOT\SHRI3XPS&DVLQJ0DWHULDO7RSRI&DVLQJ(OHYDWLRQIWPVO3XPS7XELQJVHWDW (ft)127(66DPSOHGDW6DPSOH&RQGLWLRQ&OHDU&ORXG\ 2WKHUIfyes, which sample parameters were field filtered:6DPSOH'HOLYHUHGWR$QDO\WLFDOPDUDPHWHUVDQG&RQWDLQHUV7\SHV1XPEHURI&RQWDLQHUV3UHVHUYDWLYHVHNY.001Pharr Yarns - Lowell7/21/23Lowell,NCDJH30.3527Beganpumping@091509:2009:2509:3009:3509:4009:4523.4423.5523.6323.6923.7423.791L2L2.5L3.0L3.5L4.0L200 mL/min200 mL/min100 mL/min100 mL/min100 mL/min100 mL/min17.9017.9018.3018.9019.0018.80194.3194.0194.0193.7194.6193.95.05.15.25.25.15.188.1092.9097.70110.30112.30114.107.19.012.58.48.37.45.485.295.084.884.824.83YSI Pro Plus & HACH 2100Q40 mL VOAs w/HCl(x3 - 8260 VOCs);100 mL amber unpres.(x2 - 8270 SVOCs); 250 mLplastic w/ HNO3(x1 - 6020/7470 RCRA Metals)PeristalticPVC09:45TMW-111530PolyethyleneTOC23.2076°F,SunnyTOCSMT2-inTOCClear 6?%%%0DVWHU7HPSODWHV?)RUPV3)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI /DVW8SGDWHG5263Job No:Well ID:Water Volume PXUJingDOTemp. 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Cond. pH ORP TurbidityTimeLevelPuUJHGRate(mg//)(oC)(PS/cm)(SU)(mV)(NTU)*HQHUDOL]HGStabilization CriteriaLOW-FLOW GROUNDWATER Other)LHOGParameters:B__________________________________________________________________________________________________BParameters taken with:Field Filtration: YesNoSAMPLING RECORD 'DWH: GROUNDWATER),(/'PARAMETERSStabilization criteria guidelines from the EPA 5HJLRQ/6$SD Operating Procedure for Groundwater SamplingApril 22, 2023.6WDELOL]DWLRQRFFXUVZKHQSDUDPHWHUVDUHVWDEOHIRUWKUHHFRQVHFXWLYHUHDGLQJVPHDVXUHGDWDSSUR[LPDWHO\ILYHPLQXWHLQWHUYDOV7KHDERYHVWDELOL]DWLRQFULWHULDPD\YDU\EDVHGRQUHJXODWRU\SURJUDPDQGRUVLWHFRQGLWLRQV&KHFNZLWK3URMHFW0DQDJHUIRUVLWHVSHFLILFUHTXLUHPHQWV7XUELGLW\YDOXHV178VPD\EHUHTXLUHGIRUVHOHFWDQDO\VHVHJPHWDOV,IVWDELOL]DWLRQFULWHULDLVQRWDWWDLQDEOHFRQWDFW3URMHFW0DQDJHUTurbLGLW\ 178VRU VWDELOL]HGWater Level: slight DQG stabledrawdown IWpH +/- 0.1 68SSHFLILFCondXFWLYLW\ +/- 5% DLVVROYHGO[\JHQ +/- 0.2 mg/L6LWH1DPH: 6LWH/RFDWLRQ::6DPSOLQJ3HUVRQQHO___________________, _____________________ :HDWKHU:Well Diameter:7RWDO:HOO'HSWKIW____________6FUHHQ,QWHUYDOIW'HSWKWR:DWHUIW7XELQJ0DWHULDOT\SHRI3XPS&DVLQJ0DWHULDO7RSRI&DVLQJ(OHYDWLRQIWPVO3XPS7XELQJVHWDW (ft)127(66DPSOHGDW6DPSOH&RQGLWLRQ&OHDU&ORXG\ 2WKHUIfyes, which sample parameters were field filtered:6DPSOH'HOLYHUHGWR$QDO\WLFDOPDUDPHWHUVDQG&RQWDLQHUV7\SHV1XPEHURI&RQWDLQHUV3UHVHUYDWLYHVHNY.001Pharr Yarns - Lowell7/20/23Lowell,NCDJH3025Beganpumping@132013:2513:3013:3513:4013:4513:5013:5514:0014:0514:1014:1522.1122.1222.1422.1722.1822.1822.1822.1822.1822.1822.18500 mL1000 mL1500 mL2000 mL2500 mL3000 mL3500 mL4000 mL4500 mL5000 mL5500 mL100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min22.5022.5022.1021.7022.1021.9021.6021.8022.0022.6022.3097.797.597.496.495.995.294.793.893.892.591.66.26.26.36.26.25.95.85.95.95.827.7029.8034.7036.2044.2048.6047.6052.6052.8058.5059.2027.722.821.425.618.016.311.411.212.99.87.82.192.182.262.272.292.292.312.272.212.172.20YSI Pro Plus & HACH 2100Q40 mL VOAs w/HCl(x3 - 8260 VOCs);100 mL amber unpres.(x2 - 8270 SVOCs); 250 mLplastic w/ HNO3(x1 - 6020/7470 RCRA Metals)PeristalticPVC14:15TMW-121530PolyethyleneTOC5.821.8889°F,Clear SkiesTOCSMT2-inTOCClear &Žƌŵ^sͲϭSub-Slab / Soil Gas Vapor Installation Field FormProject No.:__________________ Sampler:______________________Weather:____________________________________________________________Surface MaterialSlab Thickness (if appl.) Material Below Slab (if appl.)Depth of Screen (if appl.)Type Date & TimeAmbient Temp.Purge MethodVolume PurgedShroud Helium Conc.Purge Helium Conc.Leak Test Pass? (see note)SS, SGPerm., Temp.Concrete, soil, gravel, asphaltInchesGravel, sand, clay, etc.ft bgsFull sample train or point-onlymm/dd/yy 24-hroFSyringe, pumpLiters (see notes for calc.)%% or ppm(indicate units below)Yes / No^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporary; Volume Purged = x3 purge volumes = 3*L*aLast updated: 4/21/2022" Hg = inches of mercury; ppm = parts per millionNotes:________________________________________________________________________________________________________________________________________________________________________________________________________________Sample ID TypeVapor Monitoring Point Construction Helium Leak TestEŽƚĞ͗>ĞĂŬdĞƐƚZĞƋƵŝƌĞŵĞŶƚƐWĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ůĞĂŬƚĞƐƚƉĂƐƐĞƐŝĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƉƵƌŐĞĂŝƌŝƐůĞƐƐƚŚĂŶϭϬйŽĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƐŚƌŽƵĚ͘L = length of tubing/pipe (ft)a = 0.163 for 2" diameter (L/ft)a = 0.010 for 0.25" diameter (L/ft)͗ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽǆͰǇKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ/ŶƐƚĂůůĂƚŝŽŶ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WHNY.001DJH/JLH90°Fs, Overcast, HumidSG-1020402SG TempSoilN/A N/A 5.5Full7/20/23 152388 Syringe 0.15 11.4 0 ppm Yes007568SG-2021885SG TempSoilN/A N/A 5.5Full7/20/23 155586 Syringe 0.15 11.8 0 ppm Yes012429SG-3008486SG TempSoilN/A N/A 5.5Full7/21/23 111084 Syringe 0.15 11.4 0 ppm Yes021484SG-4021931SG TempSoilN/A N/A 5.5Full7/21/23 113485 Syringe 0.15 10.9 0 ppm Yes015278SG-5010678SG TempSoilN/A N/A 5.5Full7/21/23 124089 Syringe 0.15 10.4 0 ppm Yes015505SG-6028140SG TempSoilN/A N/A 5.5Full7/21/23 130590 Syringe 0.15 10.7 0 ppm Yes009295 &Žƌŵ^sͲϭSub-Slab / Soil Gas Vapor Installation Field FormProject No.:__________________ Sampler:______________________Weather:____________________________________________________________Surface MaterialSlab Thickness (if appl.) Material Below Slab (if appl.)Depth of Screen (if appl.)Type Date & TimeAmbient Temp.Purge MethodVolume PurgedShroud Helium Conc.Purge Helium Conc.Leak Test Pass? (see note)SS, SGPerm., Temp.Concrete, soil, gravel, asphaltInchesGravel, sand, clay, etc.ft bgsFull sample train or point-onlymm/dd/yy 24-hroFSyringe, pumpLiters (see notes for calc.)%% or ppm(indicate units below)Yes / No^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporary; Volume Purged = x3 purge volumes = 3*L*aLast updated: 4/21/2022" Hg = inches of mercury; ppm = parts per millionNotes:________________________________________________________________________________________________________________________________________________________________________________________________________________Sample ID TypeVapor Monitoring Point Construction Helium Leak TestEŽƚĞ͗>ĞĂŬdĞƐƚZĞƋƵŝƌĞŵĞŶƚƐWĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ůĞĂŬƚĞƐƚƉĂƐƐĞƐŝĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƉƵƌŐĞĂŝƌŝƐůĞƐƐƚŚĂŶϭϬйŽĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƐŚƌŽƵĚ͘L = length of tubing/pipe (ft)a = 0.163 for 2" diameter (L/ft)a = 0.010 for 0.25" diameter (L/ft)͗ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽǆͰǇKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ/ŶƐƚĂůůĂƚŝŽŶ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WHNY.001DJH/JLH80°Fs, SunnySG-7009627SG TempSoilN/A N/A 5.5Full7/21/23 134190 Syringe 0.15 10.7 0 ppm Yes012677SG-8010587SG TempSoilN/A N/A 5.5Full7/21/23 124688 Syringe 0.15 10.9 0 ppm Yes012736SG-9022042SG TempSoilN/A N/A 5.5Full7/21/23 103084 Syringe 0.15 10.8 0 ppm Yes005956SG-10023383SG TempSoilN/A N/A 5.5Full7/21/23 111086 Syringe 0.15 10.4 0 ppm Yes012357SG-11028493SG TempSoilN/A N/A 5.5Full7/21/23 095581 Syringe 0.15 10.6 0 ppm Yes012708SG-12007920SG TempSoilN/A N/A 5.5Full7/21/23 093580 Syringe 0.15 10.4 0 ppm Yes009940 &Žƌŵ^sͲϭSub-Slab / Soil Gas Vapor Installation Field FormProject No.:__________________ Sampler:______________________Weather:____________________________________________________________Surface MaterialSlab Thickness (if appl.) Material Below Slab (if appl.)Depth of Screen (if appl.)Type Date & TimeAmbient Temp.Purge MethodVolume PurgedShroud Helium Conc.Purge Helium Conc.Leak Test Pass? (see note)SS, SGPerm., Temp.Concrete, soil, gravel, asphaltInchesGravel, sand, clay, etc.ft bgsFull sample train or point-onlymm/dd/yy 24-hroFSyringe, pumpLiters (see notes for calc.)%% or ppm(indicate units below)Yes / No^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporary; Volume Purged = x3 purge volumes = 3*L*aLast updated: 4/21/2022" Hg = inches of mercury; ppm = parts per millionNotes:________________________________________________________________________________________________________________________________________________________________________________________________________________Sample ID TypeVapor Monitoring Point Construction Helium Leak TestEŽƚĞ͗>ĞĂŬdĞƐƚZĞƋƵŝƌĞŵĞŶƚƐWĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ůĞĂŬƚĞƐƚƉĂƐƐĞƐŝĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƉƵƌŐĞĂŝƌŝƐůĞƐƐƚŚĂŶϭϬйŽĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƐŚƌŽƵĚ͘L = length of tubing/pipe (ft)a = 0.163 for 2" diameter (L/ft)a = 0.010 for 0.25" diameter (L/ft)͗ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽǆͰǇKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ/ŶƐƚĂůůĂƚŝŽŶ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WHNY.001DJH/JLH90°Fs, Overcast, HumidSG-13024523SG TempSoilN/A N/A 5.5Full7/21/23 091078 Syringe 0.15 10.6 0 ppm Yes012353SG-14021552SG TempSoilN/A N/A 5.5Full7/21/23 084575 Syringe 0.15 11.5 0 ppm Yes028678SG-15023574SG TempSoilN/A N/A 5.5Full7/20/23 084874 Syringe 0.15 10.3 0 ppm Yes028628SG-16021993SG TempSoilN/A N/A 5.5Full7/20/23 092076 Syringe 0.15 10.5 0 ppm Yes015467SG-17007645SG TempSoilN/A N/A 5.5Full7/20/23 094879 Syringe 0.15 11.0 0 ppm Yes009397SG-18022052SG TempSoilN/A N/A 5.5Full7/20/23 103581 Syringe 0.15 10.2 0 ppm Yes005912 &Žƌŵ^sͲϭSub-Slab / Soil Gas Vapor Installation Field FormProject No.:__________________ Sampler:______________________Weather:____________________________________________________________Surface MaterialSlab Thickness (if appl.) Material Below Slab (if appl.)Depth of Screen (if appl.)Type Date & TimeAmbient Temp.Purge MethodVolume PurgedShroud Helium Conc.Purge Helium Conc.Leak Test Pass? (see note)SS, SGPerm., Temp.Concrete, soil, gravel, asphaltInchesGravel, sand, clay, etc.ft bgsFull sample train or point-onlymm/dd/yy 24-hroFSyringe, pumpLiters (see notes for calc.)%% or ppm(indicate units below)Yes / No^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporary; Volume Purged = x3 purge volumes = 3*L*aLast updated: 4/21/2022" Hg = inches of mercury; ppm = parts per millionNotes:________________________________________________________________________________________________________________________________________________________________________________________________________________Sample ID TypeVapor Monitoring Point Construction Helium Leak TestEŽƚĞ͗>ĞĂŬdĞƐƚZĞƋƵŝƌĞŵĞŶƚƐWĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ůĞĂŬƚĞƐƚƉĂƐƐĞƐŝĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƉƵƌŐĞĂŝƌŝƐůĞƐƐƚŚĂŶϭϬйŽĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƐŚƌŽƵĚ͘L = length of tubing/pipe (ft)a = 0.163 for 2" diameter (L/ft)a = 0.010 for 0.25" diameter (L/ft)͗ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽǆͰǇKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ/ŶƐƚĂůůĂƚŝŽŶ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WHNY.001DJH/JLH90°Fs, Overcast, HumidSG-19/SG-DUP020071/023816SG TempSoilN/A N/A 5.5Full7/20/23 115086 Syringe 0.15 10.3 0 ppm Yes012852/006650SG-20022865SG TempSoilN/A N/A 5.5Full7/20/23 122987 Syringe 0.15 10.2 0 ppm Yes021454SG-21022256SG TempSoilN/A N/A 5.5Full7/20/23 130588 Syringe 0.15 10.3 0 ppm Yes010191SG-22010766SG TempSoilN/A N/A 5.5Full7/20/23 140388 Syringe 0.15 11.8 0 ppm Yes008397SG-23015010SG TempSoilN/A N/A 5.5Full7/20/23 144389 Syringe 0.15 11.0 0 ppm Yes006646 &Žƌŵ^sͲϮSub-Slab / Soil Gas Vapor Sampling Field FormProject No.:___________________ Sampler:______________________ Weather:____________________________________________________________Date Proposed Sampling Duration Time Canister PressureOutdoor TemperatureOutdoor HumidityIndoor TemperatureIndoor Humiditymm/dd/yy Minutes24-hr" HgoF%oF%^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporaryLast updated: 6/18/2020" Hg = inches of mercuryNotes:_____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗Sample ID^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗Sampling Information Indoor ParametersOutdoor ParametersSampling PeriodEŽƚĞ͗WĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ƐŚƵƚͲŝŶƚĞƐƚĂŶĚŚĞůŝƵŵůĞĂŬĐŚĞĐŬŵƵƐƚďĞƉĂƐƐĞĚďĞĨŽƌĞƐĂŵƉůŝŶŐ͗͘ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽǆͰǇKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ^ĂŵƉůŝŶŐ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WHNY.001DJH/JLH90°Fs, Overcast, HumidSG-11-L0204027/20/2310100 mL/min1533 -1488 58 -0075681535 -51528 -29-SG-21-L1558 -280218857/20/23101603 -1586 63--100 mL/min0124291606 -5SG-31114 -271-L0084867/21/23 1084 64--021484100 mL/min1119 -111121 -5SG-41138 -271-L0219317/21/23101143 -1685 62 - -015278100 mL/min1149 -5SG-51250 -291-L0106787/21/23101255 -1789 52--100 mL/min0155051301 -5SG-61-L1315 -307/21/23028140101320 -1890 50 - -009295100 mL/min1326 -5 &Žƌŵ^sͲϮSub-Slab / Soil Gas Vapor Sampling Field FormProject No.:___________________ Sampler:______________________ Weather:____________________________________________________________Date Proposed Sampling Duration Time Canister PressureOutdoor TemperatureOutdoor HumidityIndoor TemperatureIndoor Humiditymm/dd/yy Minutes24-hr" HgoF%oF%^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporaryLast updated: 6/18/2020" Hg = inches of mercuryNotes:_____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗Sample ID^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗Sampling Information Indoor ParametersOutdoor ParametersSampling PeriodEŽƚĞ͗WĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ƐŚƵƚͲŝŶƚĞƐƚĂŶĚŚĞůŝƵŵůĞĂŬĐŚĞĐŬŵƵƐƚďĞƉĂƐƐĞĚďĞĨŽƌĞƐĂŵƉůŝŶŐ͗͘ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽǆͰǇKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ^ĂŵƉůŝŶŐ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WHNY.001DJH/JLH90°Fs, Overcast, HumidSG-71-L0096277/21/2310100 mL/min1349 -2390 53 -0126771402 -51344 -30-SG-81-L1249 -300105877/21/23101254 -2888 55--100 mL/min0127361300 -5SG-91035 -281-L0220427/21/23 1084 59--005956100 mL/min1040 -241045 -5SG-101115 -301-L0233837/21/23101120 -1886 55 - -012357100 mL/min1126 -5SG-111000 -271-L0284937/21/23101005 -581 62--100 mL/min0127081005 -5SG-121-L0945 -27.57/21/23007920100950 -1080 65 - -009940100 mL/min0952 -5 &Žƌŵ^sͲϮSub-Slab / Soil Gas Vapor Sampling Field FormProject No.:___________________ Sampler:______________________ Weather:____________________________________________________________Date Proposed Sampling Duration Time Canister PressureOutdoor TemperatureOutdoor HumidityIndoor TemperatureIndoor Humiditymm/dd/yy Minutes24-hr" HgoF%oF%^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporaryLast updated: 6/18/2020" Hg = inches of mercuryNotes:_____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗Sample ID^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗Sampling Information Indoor ParametersOutdoor ParametersSampling PeriodEŽƚĞ͗WĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ƐŚƵƚͲŝŶƚĞƐƚĂŶĚŚĞůŝƵŵůĞĂŬĐŚĞĐŬŵƵƐƚďĞƉĂƐƐĞĚďĞĨŽƌĞƐĂŵƉůŝŶŐ͗͘ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽǆͰǇKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ^ĂŵƉůŝŶŐ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WHNY.001DJH/JLH90°Fs, Overcast, HumidSG-131-L0245237/21/2310100 mL/min0920 -1878 70 -0123530927 -50915 -28-SG-141-L0850 -300215527/21/23100855 -1776 73--100 mL/min0286780900 -5SG-150853 -291-L0235747/20/23 1074 81--028628100 mL/min0858 -180904 -5SG-160925 -291-L0219937/20/23100930 -2076 77 - -015467100 mL/min0938 -5SG-170955 -321-L0076457/20/23101000 -1879 70--100 mL/min0093971005 -5SG-181-L1041 -297/20/23022052101046 -2081 66 - -005912100 mL/min1059 -5 &Žƌŵ^sͲϮSub-Slab / Soil Gas Vapor Sampling Field FormProject No.:___________________ Sampler:______________________ Weather:____________________________________________________________Date Proposed Sampling Duration Time Canister PressureOutdoor TemperatureOutdoor HumidityIndoor TemperatureIndoor Humiditymm/dd/yy Minutes24-hr" HgoF%oF%^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporaryLast updated: 6/18/2020" Hg = inches of mercuryNotes:_____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗Sample ID^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗^ŝǌĞ͗&ůŽǁZĂƚĞ͗Sampling Information Indoor ParametersOutdoor ParametersSampling PeriodEŽƚĞ͗WĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ƐŚƵƚͲŝŶƚĞƐƚĂŶĚŚĞůŝƵŵůĞĂŬĐŚĞĐŬŵƵƐƚďĞƉĂƐƐĞĚďĞĨŽƌĞƐĂŵƉůŝŶŐ͗͘ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽǆͰǇKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ^ĂŵƉůŝŶŐ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WHNY.001DJH/JLH90°Fs, Overcast, HumidSG-19/SG-DUP*1-L020071/0238167/20/2310100 mL/min1200 -13/-1786 58 -012852/0066501203 -51155 -29/-29-SG-201-L1235 -270228657/20/23101240 -1187 56--100 mL/min0214541242 -5SG-211310 -271-L0222567/20/23 1088 58--010191100 mL/min1315 -111317 -5SG-221407 -291-L0107667/20/23101412 -1688 58 - -008397100 mL/min1417 -5SG-231445 -301-L0150107/20/23101450 -2089 57--100 mL/min0066461458 -5*Two (2) regulators used due to tee-connectorSG-19 can stopped @ 1203; SG-DUP canstopped @ 1206. *Stopped sample @ 1410 due to homeless; start back up @ 1413. Appendix D DEQ Risk Calculator Input/Output Forms Version Date: Basis: Site Name: Site Address: DEQ Section: Site ID: Exposure Unit ID: Submittal Date: Reviewed By: Hypothetical Worst-Case Building A (SG 1-4) North Carolina Department of Environmental Quality Risk Calculator Pharr Yarns - Lowell 700 West 1st Street, Lowell, NC Brownfields Redevelopment Section 25027-21-036 July 2023 May 2023 EPA RSL Table Prepared By:Hart & Hickman, PC 2923 S. Tryon Street, Suite 100, Charlotte, NC North Carolina DEQ Risk Calculator Complete Exposure Pathways Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building A (SG 1-4) Note: Risk output will only be calculated for complete exposure pathways. Receptor Pathway Check box if pathway complete Soil Groundwater Use Soil Groundwater Use Construction Worker Soil Soil Surface Water Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Source Soil Source Groundwater Source Soil Source Groundwater Resident Non-Residential Worker CONTAMINANT MIGRATION PATHWAYS Groundwater Surface Water Input Form 1A VAPOR INTRUSION PATHWAYS DIRECT CONTACT SOIL AND WATER PATHWAYS Resident Non-Residential Worker Recreator/Trespasser North Carolina DEQ Risk Calculator Exposure Point Concentrations Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building A (SG 1-4) Description of Exposure Point Concentration Selection: Exposure Point Concentration (ug/m3) Notes:CAS Number Chemical Minimum Concentration (Qualifier) Maximum Concentration (Qualifier) Units Location of Maximum Concentration Detection Frequency Range of Detection Limits Concentration Used for Screening Background Value Screening Toxicity Value (Screening Level) (n/c) Potential ARAR/TBC Value Potential ARAR/TBC Source COPC Flag (Y/N) Rationale for Selection or Deletion 58 67-64-1 Acetone ug/m3 38.3 71-43-2 Benzene ug/m3 167 75-15-0 Carbon Disulfide ug/m3 16.1 67-66-3 Chloroform ug/m3 1.35 74-87-3 Chloromethane ug/m3 7.18 98-82-8 Cumene ug/m3 59.2 110-82-7 Cyclohexane ug/m3 2.07 75-71-8 Dichlorodifluoromethane ug/m3 1.32 156-60-5 Dichloroethylene, trans-1,2-ug/m3 35.2 100-41-4 Ethylbenzene ug/m3 1.52 109-99-9 ~Tetrahydrofuran ug/m3 274 142-82-5 Heptane, N-ug/m3 93.1 110-54-3 Hexane, N-ug/m3 16.5 67-63-0 Isopropanol ug/m3 14.7 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3 8.65 75-09-2 Methylene Chloride ug/m3 2.37 91-20-3 ~Naphthalene ug/m3 115 115-07-1 Propylene ug/m3 1.15 100-42-5 Styrene ug/m3 277 127-18-4 Tetrachloroethylene ug/m3 277 108-88-3 Toluene ug/m3 127 75-69-4 Trichlorofluoromethane ug/m3 17.7 95-63-6 Trimethylbenzene, 1,2,4-ug/m3 6.38 108-67-8 Trimethylbenzene, 1,3,5-ug/m3 95.4 108-38-3 Xylene, m-ug/m3 31.1 95-47-6 Xylene, o-ug/m3 Input Form 2D Soil Gas Exposure Point Concentration Table Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations North Carolina DEQ Risk Calculator Risk for Individual Pathways Output Form 1A Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building A (SG 1-4) Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Soil NC NC NC Groundwater Use*NC NC NC Soil NC NC NC Groundwater Use*NC NC NC Construction Worker Soil NC NC NC Soil NC NC NC Surface Water*NC NC NC Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 9.7E-06 3.5E-01 NO Indoor Air NC NC NC Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 7.4E-07 2.8E-02 NO Indoor Air NC NC NC Pathway Source Source Soil NC Source Groundwater NC Source Soil NC Source Groundwater NC Groundwater Exceedence of 2L at Receptor? Exceedence of 2L at Receptor? 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. Notes: 3. NM = Not modeled, user did not check this pathway as complete. 4. NC = Pathway not calculated, required contaminant migration parameters were not entered. DIRECT CONTACT SOIL AND WATER CALCULATORS Resident Non-Residential Worker Recreator/Trespasser 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure. Surface Water Exceedence of 2B at Receptor? Exceedence of 2B at Receptor? VAPOR INTRUSION CALCULATORS Resident Non-Residential Worker CONTAMINANT MIGRATION CALCULATORS Target Receptor Concentrations Exceeded? North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building A (SG 1-4) CAS #Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 58 1.74 -- 71-43-2 Benzene 38.3 1.149 3.6E-01 6.3E+00 3.2E-06 3.7E-02 75-15-0 Carbon Disulfide 167 5.01 -1.5E+02 6.9E-03 67-66-3 Chloroform 16.1 0.483 1.2E-01 2.0E+01 4.0E-06 4.7E-03 74-87-3 Chloromethane 1.35 0.0405 -1.9E+01 4.3E-04 98-82-8 Cumene 7.18 0.2154 -8.3E+01 5.2E-04 110-82-7 Cyclohexane 59.2 1.776 -1.3E+03 2.8E-04 75-71-8 Dichlorodifluoromethane 2.07 0.0621 -2.1E+01 6.0E-04 156-60-5 Dichloroethylene, trans-1,2-1.32 0.0396 -8.3E+00 9.5E-04 100-41-4 Ethylbenzene 35.2 1.056 1.1E+00 2.1E+02 9.4E-07 1.0E-03 109-99-9 ~Tetrahydrofuran 1.52 0.0456 -4.2E+02 2.2E-05 142-82-5 Heptane, N-274 8.22 -8.3E+01 2.0E-02 110-54-3 Hexane, N-93.1 2.793 -1.5E+02 3.8E-03 67-63-0 Isopropanol 16.5 0.495 -4.2E+01 2.4E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)14.7 0.441 -1.0E+03 8.5E-05 75-09-2 Methylene Chloride 8.65 0.2595 1.0E+02 1.3E+02 2.6E-09 4.1E-04 91-20-3 ~Naphthalene 2.37 0.0711 8.3E-02 6.3E-01 8.6E-07 2.3E-02 115-07-1 Propylene 115 3.45 -6.3E+02 1.1E-03 100-42-5 Styrene 1.15 0.0345 -2.1E+02 3.3E-05 127-18-4 Tetrachloroethylene 277 8.31 1.1E+01 8.3E+00 7.7E-07 2.0E-01 108-88-3 Toluene 277 8.31 -1.0E+03 1.6E-03 75-69-4 Trichlorofluoromethane 127 3.81 -- 95-63-6 Trimethylbenzene, 1,2,4-17.7 0.531 -1.3E+01 8.5E-03 108-67-8 Trimethylbenzene, 1,3,5-6.38 0.1914 -1.3E+01 3.1E-03 108-38-3 Xylene, m-95.4 2.862 -2.1E+01 2.7E-02 95-47-6 Xylene, o-31.1 0.933 -2.1E+01 8.9E-03 Cumulative:9.7E-06 3.5E-01 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building A (SG 1-4) CAS #Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 58 0.58 -- 71-43-2 Benzene 38.3 0.383 1.6E+00 2.6E+01 2.4E-07 2.9E-03 75-15-0 Carbon Disulfide 167 1.67 -6.1E+02 5.4E-04 67-66-3 Chloroform 16.1 0.161 5.3E-01 8.6E+01 3.0E-07 3.8E-04 74-87-3 Chloromethane 1.35 0.0135 -7.9E+01 3.4E-05 98-82-8 Cumene 7.18 0.0718 -3.5E+02 4.1E-05 110-82-7 Cyclohexane 59.2 0.592 -5.3E+03 2.3E-05 75-71-8 Dichlorodifluoromethane 2.07 0.0207 -8.8E+01 4.7E-05 156-60-5 Dichloroethylene, trans-1,2-1.32 0.0132 -3.5E+01 7.5E-05 100-41-4 Ethylbenzene 35.2 0.352 4.9E+00 8.8E+02 7.2E-08 8.0E-05 109-99-9 ~Tetrahydrofuran 1.52 0.0152 -1.8E+03 1.7E-06 142-82-5 Heptane, N-274 2.74 -3.5E+02 1.6E-03 110-54-3 Hexane, N-93.1 0.931 -6.1E+02 3.0E-04 67-63-0 Isopropanol 16.5 0.165 -1.8E+02 1.9E-04 78-93-3 Methyl Ethyl Ketone (2-Butanone)14.7 0.147 -4.4E+03 6.7E-06 75-09-2 Methylene Chloride 8.65 0.0865 1.2E+03 5.3E+02 7.1E-11 3.3E-05 91-20-3 ~Naphthalene 2.37 0.0237 3.6E-01 2.6E+00 6.6E-08 1.8E-03 115-07-1 Propylene 115 1.15 -2.6E+03 8.8E-05 100-42-5 Styrene 1.15 0.0115 -8.8E+02 2.6E-06 127-18-4 Tetrachloroethylene 277 2.77 4.7E+01 3.5E+01 5.9E-08 1.6E-02 108-88-3 Toluene 277 2.77 -4.4E+03 1.3E-04 75-69-4 Trichlorofluoromethane 127 1.27 -- 95-63-6 Trimethylbenzene, 1,2,4-17.7 0.177 -5.3E+01 6.7E-04 108-67-8 Trimethylbenzene, 1,3,5-6.38 0.0638 -5.3E+01 2.4E-04 108-38-3 Xylene, m-95.4 0.954 -8.8E+01 2.2E-03 95-47-6 Xylene, o-31.1 0.311 -8.8E+01 7.1E-04 Cumulative:7.4E-07 2.8E-02 All concentrations are in ug/m3 Output Form 3E Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator Version Date: Basis: Site Name: Site Address: DEQ Section: Site ID: Exposure Unit ID: Submittal Date: Reviewed By: Prepared By:Hart & Hickman, PC 2923 S. Tryon Street, Suite 100, Charlotte, NC Hypothetical Worst-Case Building B (SG 5-10) North Carolina Department of Environmental Quality Risk Calculator Pharr Yarns - Lowell 700 West 1st Street, Lowell, NC Brownfields Redevelopment Section 25027-21-036 July 2023 May 2023 EPA RSL Table North Carolina DEQ Risk Calculator Complete Exposure Pathways Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building B (SG 5-10) Note: Risk output will only be calculated for complete exposure pathways. Receptor Pathway Check box if pathway complete Soil Groundwater Use Soil Groundwater Use Construction Worker Soil Soil Surface Water Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Source Soil Source Groundwater Source Soil Source Groundwater Input Form 1A VAPOR INTRUSION PATHWAYS DIRECT CONTACT SOIL AND WATER PATHWAYS Resident Non-Residential Worker Recreator/Trespasser Resident Non-Residential Worker CONTAMINANT MIGRATION PATHWAYS Groundwater Surface Water North Carolina DEQ Risk Calculator Exposure Point Concentrations Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building B (SG 5-10) Description of Exposure Point Concentration Selection: Exposure Point Concentration (ug/m3) Notes:CAS Number Chemical Minimum Concentration (Qualifier) Maximum Concentration (Qualifier) Units Location of Maximum Concentration Detection Frequency Range of Detection Limits Concentration Used for Screening Background Value Screening Toxicity Value (Screening Level) (n/c) Potential ARAR/TBC Value Potential ARAR/TBC Source COPC Flag (Y/N) Rationale for Selection or Deletion 54.7 67-64-1 Acetone ug/m3 77.3 71-43-2 Benzene ug/m3 208 75-15-0 Carbon Disulfide ug/m3 0.585 56-23-5 Carbon Tetrachloride ug/m3 0.568 108-90-7 Chlorobenzene ug/m3 1.68 74-87-3 Chloromethane ug/m3 14.9 98-82-8 Cumene ug/m3 54.4 110-82-7 Cyclohexane ug/m3 2 75-71-8 Dichlorodifluoromethane ug/m3 0.513 75-34-3 Dichloroethane, 1,1-ug/m3 0.372 75-00-3 Ethyl Chloride (Chloroethane)ug/m3 72 100-41-4 Ethylbenzene ug/m3 386 142-82-5 Heptane, N-ug/m3 145 110-54-3 Hexane, N-ug/m3 18.5 67-63-0 Isopropanol ug/m3 10.5 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3 3.14 75-09-2 Methylene Chloride ug/m3 84.2 115-07-1 Propylene ug/m3 2.18 100-42-5 Styrene ug/m3 605 127-18-4 Tetrachloroethylene ug/m3 505 108-88-3 Toluene ug/m3 1200 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-ug/m3 1.51 71-55-6 Trichloroethane, 1,1,1-ug/m3 487 75-69-4 Trichlorofluoromethane ug/m3 30 95-63-6 Trimethylbenzene, 1,2,4-ug/m3 9.96 108-67-8 Trimethylbenzene, 1,3,5-ug/m3 194 108-38-3 Xylene, m-ug/m3 61.6 95-47-6 Xylene, o-ug/m3 Input Form 2D Soil Gas Exposure Point Concentration Table Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations North Carolina DEQ Risk Calculator Risk for Individual Pathways Output Form 1A Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building B (SG 5-10) Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Soil NC NC NC Groundwater Use*NC NC NC Soil NC NC NC Groundwater Use*NC NC NC Construction Worker Soil NC NC NC Soil NC NC NC Surface Water*NC NC NC Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 1.0E-05 6.6E-01 NO Indoor Air NC NC NC Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 7.7E-07 5.3E-02 NO Indoor Air NC NC NC Pathway Source Source Soil NC Source Groundwater NC Source Soil NC Source Groundwater NC 3. NM = Not modeled, user did not check this pathway as complete. 4. NC = Pathway not calculated, required contaminant migration parameters were not entered. DIRECT CONTACT SOIL AND WATER CALCULATORS Resident Non-Residential Worker Recreator/Trespasser 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure. Surface Water Exceedence of 2B at Receptor? Exceedence of 2B at Receptor? VAPOR INTRUSION CALCULATORS Resident Non-Residential Worker CONTAMINANT MIGRATION CALCULATORS Target Receptor Concentrations Exceeded? Groundwater Exceedence of 2L at Receptor? Exceedence of 2L at Receptor? 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. Notes: North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building B (SG 5-10) CAS #Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 54.7 1.641 -- 71-43-2 Benzene 77.3 2.319 3.6E-01 6.3E+00 6.4E-06 7.4E-02 75-15-0 Carbon Disulfide 208 6.24 -1.5E+02 8.5E-03 56-23-5 Carbon Tetrachloride 0.585 0.01755 4.7E-01 2.1E+01 3.8E-08 1.7E-04 108-90-7 Chlorobenzene 0.568 0.01704 -1.0E+01 3.3E-04 74-87-3 Chloromethane 1.68 0.0504 -1.9E+01 5.4E-04 98-82-8 Cumene 14.9 0.447 -8.3E+01 1.1E-03 110-82-7 Cyclohexane 54.4 1.632 -1.3E+03 2.6E-04 75-71-8 Dichlorodifluoromethane 2 0.06 -2.1E+01 5.8E-04 75-34-3 Dichloroethane, 1,1-0.513 0.01539 1.8E+00 -8.8E-09 75-00-3 Ethyl Chloride (Chloroethane)0.372 0.01116 -8.3E+02 2.7E-06 100-41-4 Ethylbenzene 72 2.16 1.1E+00 2.1E+02 1.9E-06 2.1E-03 142-82-5 Heptane, N-386 11.58 -8.3E+01 2.8E-02 110-54-3 Hexane, N-145 4.35 -1.5E+02 6.0E-03 67-63-0 Isopropanol 18.5 0.555 -4.2E+01 2.7E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)10.5 0.315 -1.0E+03 6.0E-05 75-09-2 Methylene Chloride 3.14 0.0942 1.0E+02 1.3E+02 9.3E-10 1.5E-04 115-07-1 Propylene 84.2 2.526 -6.3E+02 8.1E-04 100-42-5 Styrene 2.18 0.0654 -2.1E+02 6.3E-05 127-18-4 Tetrachloroethylene 605 18.15 1.1E+01 8.3E+00 1.7E-06 4.4E-01 108-88-3 Toluene 505 15.15 -1.0E+03 2.9E-03 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-1200 36 -1.0E+03 6.9E-03 71-55-6 Trichloroethane, 1,1,1-1.51 0.0453 -1.0E+03 8.7E-06 75-69-4 Trichlorofluoromethane 487 14.61 -- 95-63-6 Trimethylbenzene, 1,2,4-30 0.9 -1.3E+01 1.4E-02 108-67-8 Trimethylbenzene, 1,3,5-9.96 0.2988 -1.3E+01 4.8E-03 108-38-3 Xylene, m-194 5.82 -2.1E+01 5.6E-02 95-47-6 Xylene, o-61.6 1.848 -2.1E+01 1.8E-02 Cumulative:1.0E-05 6.6E-01 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building B (SG 5-10) CAS #Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 54.7 0.547 -- 71-43-2 Benzene 77.3 0.773 1.6E+00 2.6E+01 4.9E-07 5.9E-03 75-15-0 Carbon Disulfide 208 2.08 -6.1E+02 6.8E-04 56-23-5 Carbon Tetrachloride 0.585 0.00585 2.0E+00 8.8E+01 2.9E-09 1.3E-05 108-90-7 Chlorobenzene 0.568 0.00568 -4.4E+01 2.6E-05 74-87-3 Chloromethane 1.68 0.0168 -7.9E+01 4.3E-05 98-82-8 Cumene 14.9 0.149 -3.5E+02 8.5E-05 110-82-7 Cyclohexane 54.4 0.544 -5.3E+03 2.1E-05 75-71-8 Dichlorodifluoromethane 2 0.02 -8.8E+01 4.6E-05 75-34-3 Dichloroethane, 1,1-0.513 0.00513 7.7E+00 -6.7E-10 75-00-3 Ethyl Chloride (Chloroethane)0.372 0.00372 -3.5E+03 2.1E-07 100-41-4 Ethylbenzene 72 0.72 4.9E+00 8.8E+02 1.5E-07 1.6E-04 142-82-5 Heptane, N-386 3.86 -3.5E+02 2.2E-03 110-54-3 Hexane, N-145 1.45 -6.1E+02 4.7E-04 67-63-0 Isopropanol 18.5 0.185 -1.8E+02 2.1E-04 78-93-3 Methyl Ethyl Ketone (2-Butanone)10.5 0.105 -4.4E+03 4.8E-06 75-09-2 Methylene Chloride 3.14 0.0314 1.2E+03 5.3E+02 2.6E-11 1.2E-05 115-07-1 Propylene 84.2 0.842 -2.6E+03 6.4E-05 100-42-5 Styrene 2.18 0.0218 -8.8E+02 5.0E-06 127-18-4 Tetrachloroethylene 605 6.05 4.7E+01 3.5E+01 1.3E-07 3.5E-02 108-88-3 Toluene 505 5.05 -4.4E+03 2.3E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-1200 12 -4.4E+03 5.5E-04 71-55-6 Trichloroethane, 1,1,1-1.51 0.0151 -4.4E+03 6.9E-07 75-69-4 Trichlorofluoromethane 487 4.87 -- 95-63-6 Trimethylbenzene, 1,2,4-30 0.3 -5.3E+01 1.1E-03 108-67-8 Trimethylbenzene, 1,3,5-9.96 0.0996 -5.3E+01 3.8E-04 108-38-3 Xylene, m-194 1.94 -8.8E+01 4.4E-03 95-47-6 Xylene, o-61.6 0.616 -8.8E+01 1.4E-03 Cumulative:7.7E-07 5.3E-02 All concentrations are in ug/m3 Output Form 3E Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator Version Date: Basis: Site Name: Site Address: DEQ Section: Site ID: Exposure Unit ID: Submittal Date: Reviewed By: Hypothetical Worst-Case Building C (SG 11-14) North Carolina Department of Environmental Quality Risk Calculator Pharr Yarns - Lowell 700 West 1st Street, Lowell, NC Brownfields Redevelopment Section 25027-21-036 July 2023 May 2023 EPA RSL Table Prepared By:Hart & Hickman, PC 2923 S. Tryon Street, Suite 100, Charlotte, NC North Carolina DEQ Risk Calculator Complete Exposure Pathways Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building C (SG 11-14) Note: Risk output will only be calculated for complete exposure pathways. Receptor Pathway Check box if pathway complete Soil Groundwater Use Soil Groundwater Use Construction Worker Soil Soil Surface Water Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Source Soil Source Groundwater Source Soil Source Groundwater Resident Non-Residential Worker CONTAMINANT MIGRATION PATHWAYS Groundwater Surface Water Input Form 1A VAPOR INTRUSION PATHWAYS DIRECT CONTACT SOIL AND WATER PATHWAYS Resident Non-Residential Worker Recreator/Trespasser North Carolina DEQ Risk Calculator Exposure Point ConcentrationsVersion Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building C (SG 11-14) Description of Exposure Point Concentration Selection: Exposure Point Concentration (ug/m3) Notes:CAS Number Chemical Minimum Concentration (Qualifier) Maximum Concentration (Qualifier) Units Location of Maximum Concentration Detection Frequency Range of Detection Limits Concentration Used for Screening Background Value Screening Toxicity Value (Screening Level) (n/c) Potential ARAR/TBC Value Potential ARAR/TBC Source COPC Flag (Y/N) Rationale for Selection or Deletion 30.7 67-64-1 Acetone ug/m3 68.4 71-43-2 Benzene ug/m3 1.88 106-99-0 Butadiene, 1,3-ug/m3 201 75-15-0 Carbon Disulfide ug/m3 0.642 56-23-5 Carbon Tetrachloride ug/m3 43 67-66-3 Chloroform ug/m3 0.671 74-87-3 Chloromethane ug/m3 9.14 98-82-8 Cumene ug/m3 27.2 110-82-7 Cyclohexane ug/m3 2.64 75-71-8 Dichlorodifluoromethane ug/m3 0.514 75-00-3 Ethyl Chloride (Chloroethane)ug/m3 68.1 100-41-4 Ethylbenzene ug/m3 355 142-82-5 Heptane, N-ug/m3 104 110-54-3 Hexane, N-ug/m3 17.1 67-63-0 Isopropanol ug/m3 6.72 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3 2.97 75-09-2 Methylene Chloride ug/m3 53 115-07-1 Propylene ug/m3 1.15 100-42-5 Styrene ug/m3 551 127-18-4 Tetrachloroethylene ug/m3 512 108-88-3 Toluene ug/m3 1200 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-ug/m3 9.33 75-69-4 Trichlorofluoromethane ug/m3 35.4 95-63-6 Trimethylbenzene, 1,2,4-ug/m3 12.4 108-67-8 Trimethylbenzene, 1,3,5-ug/m3 188 108-38-3 Xylene, m-ug/m3 65 95-47-6 Xylene, o-ug/m3 Input Form 2D Soil Gas Exposure Point Concentration Table Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations North Carolina DEQ Risk Calculator Risk for Individual Pathways Output Form 1A Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building C (SG 11-14) Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Soil NC NC NC Groundwater Use*NC NC NC Soil NC NC NC Groundwater Use*NC NC NC Construction Worker Soil NC NC NC Soil NC NC NC Surface Water*NC NC NC Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 2.0E-05 6.5E-01 NO Indoor Air NC NC NC Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 1.5E-06 5.2E-02 NO Indoor Air NC NC NC Pathway Source Source Soil NC Source Groundwater NC Source Soil NC Source Groundwater NC Groundwater Exceedence of 2L at Receptor? Exceedence of 2L at Receptor? 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. Notes: 3. NM = Not modeled, user did not check this pathway as complete. 4. NC = Pathway not calculated, required contaminant migration parameters were not entered. DIRECT CONTACT SOIL AND WATER CALCULATORS Resident Non-Residential Worker Recreator/Trespasser 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure. Surface Water Exceedence of 2B at Receptor? Exceedence of 2B at Receptor? VAPOR INTRUSION CALCULATORS Resident Non-Residential Worker CONTAMINANT MIGRATION CALCULATORS Target Receptor Concentrations Exceeded? North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building C (SG 11-14) CAS #Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 30.7 0.921 -- 71-43-2 Benzene 68.4 2.052 3.6E-01 6.3E+00 5.7E-06 6.6E-02 106-99-0 Butadiene, 1,3-1.88 0.0564 9.4E-02 4.2E-01 6.0E-07 2.7E-02 75-15-0 Carbon Disulfide 201 6.03 -1.5E+02 8.3E-03 56-23-5 Carbon Tetrachloride 0.642 0.01926 4.7E-01 2.1E+01 4.1E-08 1.8E-04 67-66-3 Chloroform 43 1.29 1.2E-01 2.0E+01 1.1E-05 1.3E-02 74-87-3 Chloromethane 0.671 0.02013 -1.9E+01 2.1E-04 98-82-8 Cumene 9.14 0.2742 -8.3E+01 6.6E-04 110-82-7 Cyclohexane 27.2 0.816 -1.3E+03 1.3E-04 75-71-8 Dichlorodifluoromethane 2.64 0.0792 -2.1E+01 7.6E-04 75-00-3 Ethyl Chloride (Chloroethane)0.514 0.01542 -8.3E+02 3.7E-06 100-41-4 Ethylbenzene 68.1 2.043 1.1E+00 2.1E+02 1.8E-06 2.0E-03 142-82-5 Heptane, N-355 10.65 -8.3E+01 2.6E-02 110-54-3 Hexane, N-104 3.12 -1.5E+02 4.3E-03 67-63-0 Isopropanol 17.1 0.513 -4.2E+01 2.5E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)6.72 0.2016 -1.0E+03 3.9E-05 75-09-2 Methylene Chloride 2.97 0.0891 1.0E+02 1.3E+02 8.8E-10 1.4E-04 115-07-1 Propylene 53 1.59 -6.3E+02 5.1E-04 100-42-5 Styrene 1.15 0.0345 -2.1E+02 3.3E-05 127-18-4 Tetrachloroethylene 551 16.53 1.1E+01 8.3E+00 1.5E-06 4.0E-01 108-88-3 Toluene 512 15.36 -1.0E+03 2.9E-03 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-1200 36 -1.0E+03 6.9E-03 75-69-4 Trichlorofluoromethane 9.33 0.2799 -- 95-63-6 Trimethylbenzene, 1,2,4-35.4 1.062 -1.3E+01 1.7E-02 108-67-8 Trimethylbenzene, 1,3,5-12.4 0.372 -1.3E+01 5.9E-03 108-38-3 Xylene, m-188 5.64 -2.1E+01 5.4E-02 95-47-6 Xylene, o-65 1.95 -2.1E+01 1.9E-02 Cumulative:2.0E-05 6.5E-01 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building C (SG 11-14) CAS #Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 30.7 0.307 -- 71-43-2 Benzene 68.4 0.684 1.6E+00 2.6E+01 4.4E-07 5.2E-03 106-99-0 Butadiene, 1,3-1.88 0.0188 4.1E-01 1.8E+00 4.6E-08 2.1E-03 75-15-0 Carbon Disulfide 201 2.01 -6.1E+02 6.6E-04 56-23-5 Carbon Tetrachloride 0.642 0.00642 2.0E+00 8.8E+01 3.1E-09 1.5E-05 67-66-3 Chloroform 43 0.43 5.3E-01 8.6E+01 8.1E-07 1.0E-03 74-87-3 Chloromethane 0.671 0.00671 -7.9E+01 1.7E-05 98-82-8 Cumene 9.14 0.0914 -3.5E+02 5.2E-05 110-82-7 Cyclohexane 27.2 0.272 -5.3E+03 1.0E-05 75-71-8 Dichlorodifluoromethane 2.64 0.0264 -8.8E+01 6.0E-05 75-00-3 Ethyl Chloride (Chloroethane)0.514 0.00514 -3.5E+03 2.9E-07 100-41-4 Ethylbenzene 68.1 0.681 4.9E+00 8.8E+02 1.4E-07 1.6E-04 142-82-5 Heptane, N-355 3.55 -3.5E+02 2.0E-03 110-54-3 Hexane, N-104 1.04 -6.1E+02 3.4E-04 67-63-0 Isopropanol 17.1 0.171 -1.8E+02 2.0E-04 78-93-3 Methyl Ethyl Ketone (2-Butanone)6.72 0.0672 -4.4E+03 3.1E-06 75-09-2 Methylene Chloride 2.97 0.0297 1.2E+03 5.3E+02 2.4E-11 1.1E-05 115-07-1 Propylene 53 0.53 -2.6E+03 4.0E-05 100-42-5 Styrene 1.15 0.0115 -8.8E+02 2.6E-06 127-18-4 Tetrachloroethylene 551 5.51 4.7E+01 3.5E+01 1.2E-07 3.1E-02 108-88-3 Toluene 512 5.12 -4.4E+03 2.3E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-1200 12 -4.4E+03 5.5E-04 75-69-4 Trichlorofluoromethane 9.33 0.0933 -- 95-63-6 Trimethylbenzene, 1,2,4-35.4 0.354 -5.3E+01 1.3E-03 108-67-8 Trimethylbenzene, 1,3,5-12.4 0.124 -5.3E+01 4.7E-04 108-38-3 Xylene, m-188 1.88 -8.8E+01 4.3E-03 95-47-6 Xylene, o-65 0.65 -8.8E+01 1.5E-03 Cumulative:1.5E-06 5.2E-02 All concentrations are in ug/m3 Output Form 3E Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator Version Date: Basis: Site Name: Site Address: DEQ Section: Site ID: Exposure Unit ID: Submittal Date: Reviewed By: Prepared By:Hart & Hickman, PC 2923 S. Tryon Street, Suite 100, Charlotte, NC Hypothetical Worst-Case Building A (SG 15-17) North Carolina Department of Environmental Quality Risk Calculator Pharr Yarns - Lowell 700 West 1st Street, Lowell, NC Brownfields Redevelopment Section 25027-21-036 July 2023 May 2023 EPA RSL Table North Carolina DEQ Risk Calculator Complete Exposure Pathways Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building A (SG 15-17) Note: Risk output will only be calculated for complete exposure pathways. Receptor Pathway Check box if pathway complete Soil Groundwater Use Soil Groundwater Use Construction Worker Soil Soil Surface Water Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Source Soil Source Groundwater Source Soil Source Groundwater Input Form 1A VAPOR INTRUSION PATHWAYS DIRECT CONTACT SOIL AND WATER PATHWAYS Resident Non-Residential Worker Recreator/Trespasser Resident Non-Residential Worker CONTAMINANT MIGRATION PATHWAYS Groundwater Surface Water North Carolina DEQ Risk Calculator Exposure Point ConcentrationsVersion Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building A (SG 15-17) Description of Exposure Point Concentration Selection: Exposure Point Concentration (ug/m3) Notes:CAS Number Chemical Minimum Concentration (Qualifier) Maximum Concentration (Qualifier) Units Location of Maximum Concentration Detection Frequency Range of Detection Limits Concentration Used for Screening Background Value Screening Toxicity Value (Screening Level) (n/c) Potential ARAR/TBC Value Potential ARAR/TBC Source COPC Flag (Y/N) Rationale for Selection or Deletion 18.9 67-64-1 Acetone ug/m3 15.4 71-43-2 Benzene ug/m3 1.39 75-27-4 Bromodichloromethane ug/m3 17.1 75-15-0 Carbon Disulfide ug/m3 37.3 67-66-3 Chloroform ug/m3 0.628 74-87-3 Chloromethane ug/m3 4.02 98-82-8 Cumene ug/m3 10.9 110-82-7 Cyclohexane ug/m3 1.77 75-71-8 Dichlorodifluoromethane ug/m3 0.472 75-35-4 Dichloroethylene, 1,1-ug/m3 23.6 100-41-4 Ethylbenzene ug/m3 90 142-82-5 Heptane, N-ug/m3 38.8 110-54-3 Hexane, N-ug/m3 7.52 67-63-0 Isopropanol ug/m3 5.51 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3 4.13 75-09-2 Methylene Chloride ug/m3 5.06 115-07-1 Propylene ug/m3 0.519 100-42-5 Styrene ug/m3 139 127-18-4 Tetrachloroethylene ug/m3 142 108-88-3 Toluene ug/m3 1.82 71-55-6 Trichloroethane, 1,1,1-ug/m3 1.48 75-69-4 Trichlorofluoromethane ug/m3 26.3 95-63-6 Trimethylbenzene, 1,2,4-ug/m3 7.71 108-67-8 Trimethylbenzene, 1,3,5-ug/m3 72 108-38-3 Xylene, m-ug/m3 27.6 95-47-6 Xylene, o-ug/m3 Input Form 2D Soil Gas Exposure Point Concentration Table Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations North Carolina DEQ Risk Calculator Risk for Individual Pathways Output Form 1A Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building A (SG 15-17) Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Soil NC NC NC Groundwater Use*NC NC NC Soil NC NC NC Groundwater Use*NC NC NC Construction Worker Soil NC NC NC Soil NC NC NC Surface Water*NC NC NC Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 1.2E-05 1.8E-01 NO Indoor Air NC NC NC Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 9.2E-07 1.5E-02 NO Indoor Air NC NC NC Pathway Source Source Soil NC Source Groundwater NC Source Soil NC Source Groundwater NC 3. NM = Not modeled, user did not check this pathway as complete. 4. NC = Pathway not calculated, required contaminant migration parameters were not entered. DIRECT CONTACT SOIL AND WATER CALCULATORS Resident Non-Residential Worker Recreator/Trespasser 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure. Surface Water Exceedence of 2B at Receptor? Exceedence of 2B at Receptor? VAPOR INTRUSION CALCULATORS Resident Non-Residential Worker CONTAMINANT MIGRATION CALCULATORS Target Receptor Concentrations Exceeded? Groundwater Exceedence of 2L at Receptor? Exceedence of 2L at Receptor? 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. Notes: North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building A (SG 15-17) CAS #Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 18.9 0.567 -- 71-43-2 Benzene 15.4 0.462 3.6E-01 6.3E+00 1.3E-06 1.5E-02 75-27-4 Bromodichloromethane 1.39 0.0417 7.6E-02 -5.5E-07 75-15-0 Carbon Disulfide 17.1 0.513 -1.5E+02 7.0E-04 67-66-3 Chloroform 37.3 1.119 1.2E-01 2.0E+01 9.2E-06 1.1E-02 74-87-3 Chloromethane 0.628 0.01884 -1.9E+01 2.0E-04 98-82-8 Cumene 4.02 0.1206 -8.3E+01 2.9E-04 110-82-7 Cyclohexane 10.9 0.327 -1.3E+03 5.2E-05 75-71-8 Dichlorodifluoromethane 1.77 0.0531 -2.1E+01 5.1E-04 75-35-4 Dichloroethylene, 1,1-0.472 0.01416 -4.2E+01 6.8E-05 100-41-4 Ethylbenzene 23.6 0.708 1.1E+00 2.1E+02 6.3E-07 6.8E-04 142-82-5 Heptane, N-90 2.7 -8.3E+01 6.5E-03 110-54-3 Hexane, N-38.8 1.164 -1.5E+02 1.6E-03 67-63-0 Isopropanol 7.52 0.2256 -4.2E+01 1.1E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone)5.51 0.1653 -1.0E+03 3.2E-05 75-09-2 Methylene Chloride 4.13 0.1239 1.0E+02 1.3E+02 1.2E-09 2.0E-04 115-07-1 Propylene 5.06 0.1518 -6.3E+02 4.9E-05 100-42-5 Styrene 0.519 0.01557 -2.1E+02 1.5E-05 127-18-4 Tetrachloroethylene 139 4.17 1.1E+01 8.3E+00 3.9E-07 1.0E-01 108-88-3 Toluene 142 4.26 -1.0E+03 8.2E-04 71-55-6 Trichloroethane, 1,1,1-1.82 0.0546 -1.0E+03 1.0E-05 75-69-4 Trichlorofluoromethane 1.48 0.0444 -- 95-63-6 Trimethylbenzene, 1,2,4-26.3 0.789 -1.3E+01 1.3E-02 108-67-8 Trimethylbenzene, 1,3,5-7.71 0.2313 -1.3E+01 3.7E-03 108-38-3 Xylene, m-72 2.16 -2.1E+01 2.1E-02 95-47-6 Xylene, o-27.6 0.828 -2.1E+01 7.9E-03 Cumulative:1.2E-05 1.8E-01 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building A (SG 15-17) CAS #Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 18.9 0.189 -- 71-43-2 Benzene 15.4 0.154 1.6E+00 2.6E+01 9.8E-08 1.2E-03 75-27-4 Bromodichloromethane 1.39 0.0139 3.3E-01 -4.2E-08 75-15-0 Carbon Disulfide 17.1 0.171 -6.1E+02 5.6E-05 67-66-3 Chloroform 37.3 0.373 5.3E-01 8.6E+01 7.0E-07 8.7E-04 74-87-3 Chloromethane 0.628 0.00628 -7.9E+01 1.6E-05 98-82-8 Cumene 4.02 0.0402 -3.5E+02 2.3E-05 110-82-7 Cyclohexane 10.9 0.109 -5.3E+03 4.1E-06 75-71-8 Dichlorodifluoromethane 1.77 0.0177 -8.8E+01 4.0E-05 75-35-4 Dichloroethylene, 1,1-0.472 0.00472 -1.8E+02 5.4E-06 100-41-4 Ethylbenzene 23.6 0.236 4.9E+00 8.8E+02 4.8E-08 5.4E-05 142-82-5 Heptane, N-90 0.9 -3.5E+02 5.1E-04 110-54-3 Hexane, N-38.8 0.388 -6.1E+02 1.3E-04 67-63-0 Isopropanol 7.52 0.0752 -1.8E+02 8.6E-05 78-93-3 Methyl Ethyl Ketone (2-Butanone)5.51 0.0551 -4.4E+03 2.5E-06 75-09-2 Methylene Chloride 4.13 0.0413 1.2E+03 5.3E+02 3.4E-11 1.6E-05 115-07-1 Propylene 5.06 0.0506 -2.6E+03 3.9E-06 100-42-5 Styrene 0.519 0.00519 -8.8E+02 1.2E-06 127-18-4 Tetrachloroethylene 139 1.39 4.7E+01 3.5E+01 2.9E-08 7.9E-03 108-88-3 Toluene 142 1.42 -4.4E+03 6.5E-05 71-55-6 Trichloroethane, 1,1,1-1.82 0.0182 -4.4E+03 8.3E-07 75-69-4 Trichlorofluoromethane 1.48 0.0148 -- 95-63-6 Trimethylbenzene, 1,2,4-26.3 0.263 -5.3E+01 1.0E-03 108-67-8 Trimethylbenzene, 1,3,5-7.71 0.0771 -5.3E+01 2.9E-04 108-38-3 Xylene, m-72 0.72 -8.8E+01 1.6E-03 95-47-6 Xylene, o-27.6 0.276 -8.8E+01 6.3E-04 Cumulative:9.2E-07 1.5E-02 All concentrations are in ug/m3 Output Form 3E Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator Version Date: Basis: Site Name: Site Address: DEQ Section: Site ID: Exposure Unit ID: Submittal Date: Reviewed By: Prepared By:Hart & Hickman, PC 2923 S. Tryon Street, Suite 100, Charlotte, NC Hypothetical Worst-Case Building B (SG 18-23) North Carolina Department of Environmental Quality Risk Calculator Pharr Yarns - Lowell 700 West 1st Street, Lowell, NC Brownfields Redevelopment Section 25027-21-036 July 2023 May 2023 EPA RSL Table North Carolina DEQ Risk Calculator Complete Exposure Pathways Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building B (SG 18-23) Note: Risk output will only be calculated for complete exposure pathways. Receptor Pathway Check box if pathway complete Soil Groundwater Use Soil Groundwater Use Construction Worker Soil Soil Surface Water Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Source Soil Source Groundwater Source Soil Source Groundwater Input Form 1A VAPOR INTRUSION PATHWAYS DIRECT CONTACT SOIL AND WATER PATHWAYS Resident Non-Residential Worker Recreator/Trespasser Resident Non-Residential Worker CONTAMINANT MIGRATION PATHWAYS Groundwater Surface Water North Carolina DEQ Risk Calculator Exposure Point ConcentrationsVersion Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building B (SG 18-23) Description of Exposure Point Concentration Selection: Exposure Point Concentration (ug/m3) Notes:CAS Number Chemical Minimum Concentration (Qualifier) Maximum Concentration (Qualifier) Units Location of Maximum Concentration Detection Frequency Range of Detection Limits Concentration Used for Screening Background Value Screening Toxicity Value (Screening Level) (n/c) Potential ARAR/TBC Value Potential ARAR/TBC Source COPC Flag (Y/N) Rationale for Selection or Deletion 1570 67-64-1 Acetone ug/m3 54.6 71-43-2 Benzene ug/m3 129 75-15-0 Carbon Disulfide ug/m3 0.584 56-23-5 Carbon Tetrachloride ug/m3 22.6 67-66-3 Chloroform ug/m3 5.87 74-87-3 Chloromethane ug/m3 3.55 98-82-8 Cumene ug/m3 80.2 110-82-7 Cyclohexane ug/m3 2.71 75-71-8 Dichlorodifluoromethane ug/m3 0.749 156-59-2 Dichloroethylene, cis-1,2-ug/m3 0.307 156-60-5 Dichloroethylene, trans-1,2-ug/m3 1.62 141-78-6 Ethyl Acetate ug/m3 63.3 100-41-4 Ethylbenzene ug/m3 285 142-82-5 Heptane, N-ug/m3 4340 110-54-3 Hexane, N-ug/m3 4.54 591-78-6 Hexanone, 2-ug/m3 32400 67-63-0 Isopropanol ug/m3 174 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3 226 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/m3 647 80-62-6 Methyl Methacrylate ug/m3 270 75-09-2 Methylene Chloride ug/m3 29.6 115-07-1 Propylene ug/m3 69.8 100-42-5 Styrene ug/m3 363 127-18-4 Tetrachloroethylene ug/m3 433 108-88-3 Toluene ug/m3 1.02 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-ug/m3 0.48 71-55-6 Trichloroethane, 1,1,1-ug/m3 27.8 79-01-6 Trichloroethylene ug/m3 51.4 75-69-4 Trichlorofluoromethane ug/m3 86.4 95-63-6 Trimethylbenzene, 1,2,4-ug/m3 7.41 108-67-8 Trimethylbenzene, 1,3,5-ug/m3 215 108-38-3 Xylene, m-ug/m3 76.3 95-47-6 Xylene, o-ug/m3 Input Form 2D Soil Gas Exposure Point Concentration Table Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations North Carolina DEQ Risk Calculator Risk for Individual Pathways Output Form 1A Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building B (SG 18-23) Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Soil NC NC NC Groundwater Use*NC NC NC Soil NC NC NC Groundwater Use*NC NC NC Construction Worker Soil NC NC NC Soil NC NC NC Surface Water*NC NC NC Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 1.5E-05 5.8E+00 YES Indoor Air NC NC NC Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 1.1E-06 4.6E-01 NO Indoor Air NC NC NC Pathway Source Source Soil NC Source Groundwater NC Source Soil NC Source Groundwater NC 3. NM = Not modeled, user did not check this pathway as complete. 4. NC = Pathway not calculated, required contaminant migration parameters were not entered. DIRECT CONTACT SOIL AND WATER CALCULATORS Resident Non-Residential Worker Recreator/Trespasser 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure. Surface Water Exceedence of 2B at Receptor? Exceedence of 2B at Receptor? VAPOR INTRUSION CALCULATORS Resident Non-Residential Worker CONTAMINANT MIGRATION CALCULATORS Target Receptor Concentrations Exceeded? Groundwater Exceedence of 2L at Receptor? Exceedence of 2L at Receptor? 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. Notes: North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building B (SG 18-23) CAS #Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 1570 47.1 -- 71-43-2 Benzene 54.6 1.638 3.6E-01 6.3E+00 4.6E-06 5.2E-02 75-15-0 Carbon Disulfide 129 3.87 -1.5E+02 5.3E-03 56-23-5 Carbon Tetrachloride 0.584 0.01752 4.7E-01 2.1E+01 3.7E-08 1.7E-04 67-66-3 Chloroform 22.6 0.678 1.2E-01 2.0E+01 5.6E-06 6.6E-03 74-87-3 Chloromethane 5.87 0.1761 -1.9E+01 1.9E-03 98-82-8 Cumene 3.55 0.1065 -8.3E+01 2.6E-04 110-82-7 Cyclohexane 80.2 2.406 -1.3E+03 3.8E-04 75-71-8 Dichlorodifluoromethane 2.71 0.0813 -2.1E+01 7.8E-04 156-59-2 Dichloroethylene, cis-1,2-0.749 0.02247 -8.3E+00 5.4E-04 156-60-5 Dichloroethylene, trans-1,2-0.307 0.00921 -8.3E+00 2.2E-04 141-78-6 Ethyl Acetate 1.62 0.0486 -1.5E+01 6.7E-04 100-41-4 Ethylbenzene 63.3 1.899 1.1E+00 2.1E+02 1.7E-06 1.8E-03 142-82-5 Heptane, N-285 8.55 -8.3E+01 2.0E-02 110-54-3 Hexane, N-4340 130.2 -1.5E+02 1.8E-01 591-78-6 Hexanone, 2-4.54 0.1362 -6.3E+00 4.4E-03 67-63-0 Isopropanol 32400 972 -4.2E+01 4.7E+00 78-93-3 Methyl Ethyl Ketone (2-Butanone)174 5.22 -1.0E+03 1.0E-03 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)226 6.78 -6.3E+02 2.2E-03 80-62-6 Methyl Methacrylate 647 19.41 -1.5E+02 2.7E-02 75-09-2 Methylene Chloride 270 8.1 1.0E+02 1.3E+02 8.0E-08 1.3E-02 115-07-1 Propylene 29.6 0.888 -6.3E+02 2.8E-04 100-42-5 Styrene 69.8 2.094 -2.1E+02 2.0E-03 127-18-4 Tetrachloroethylene 363 10.89 1.1E+01 8.3E+00 1.0E-06 2.6E-01 108-88-3 Toluene 433 12.99 -1.0E+03 2.5E-03 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-1.02 0.0306 -1.0E+03 5.9E-06 71-55-6 Trichloroethane, 1,1,1-0.48 0.0144 -1.0E+03 2.8E-06 79-01-6 Trichloroethylene 27.8 0.834 4.8E-01 4.2E-01 1.7E-06 4.0E-01 75-69-4 Trichlorofluoromethane 51.4 1.542 -- 95-63-6 Trimethylbenzene, 1,2,4-86.4 2.592 -1.3E+01 4.1E-02 108-67-8 Trimethylbenzene, 1,3,5-7.41 0.2223 -1.3E+01 3.6E-03 108-38-3 Xylene, m-215 6.45 -2.1E+01 6.2E-02 95-47-6 Xylene, o-76.3 2.289 -2.1E+01 2.2E-02 Cumulative:1.5E-05 5.8E+00 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 25027-21-036 Exposure Unit ID: Hypothetical Worst-Case Building B (SG 18-23) CAS #Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 1570 15.7 -- 71-43-2 Benzene 54.6 0.546 1.6E+00 2.6E+01 3.5E-07 4.2E-03 75-15-0 Carbon Disulfide 129 1.29 -6.1E+02 4.2E-04 56-23-5 Carbon Tetrachloride 0.584 0.00584 2.0E+00 8.8E+01 2.9E-09 1.3E-05 67-66-3 Chloroform 22.6 0.226 5.3E-01 8.6E+01 4.2E-07 5.3E-04 74-87-3 Chloromethane 5.87 0.0587 -7.9E+01 1.5E-04 98-82-8 Cumene 3.55 0.0355 -3.5E+02 2.0E-05 110-82-7 Cyclohexane 80.2 0.802 -5.3E+03 3.1E-05 75-71-8 Dichlorodifluoromethane 2.71 0.0271 -8.8E+01 6.2E-05 156-59-2 Dichloroethylene, cis-1,2-0.749 0.00749 -3.5E+01 4.3E-05 156-60-5 Dichloroethylene, trans-1,2-0.307 0.00307 -3.5E+01 1.8E-05 141-78-6 Ethyl Acetate 1.62 0.0162 -6.1E+01 5.3E-05 100-41-4 Ethylbenzene 63.3 0.633 4.9E+00 8.8E+02 1.3E-07 1.4E-04 142-82-5 Heptane, N-285 2.85 -3.5E+02 1.6E-03 110-54-3 Hexane, N-4340 43.4 -6.1E+02 1.4E-02 591-78-6 Hexanone, 2-4.54 0.0454 -2.6E+01 3.5E-04 67-63-0 Isopropanol 32400 324 -1.8E+02 3.7E-01 78-93-3 Methyl Ethyl Ketone (2-Butanone)174 1.74 -4.4E+03 7.9E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)226 2.26 -2.6E+03 1.7E-04 80-62-6 Methyl Methacrylate 647 6.47 -6.1E+02 2.1E-03 75-09-2 Methylene Chloride 270 2.7 1.2E+03 5.3E+02 2.2E-09 1.0E-03 115-07-1 Propylene 29.6 0.296 -2.6E+03 2.3E-05 100-42-5 Styrene 69.8 0.698 -8.8E+02 1.6E-04 127-18-4 Tetrachloroethylene 363 3.63 4.7E+01 3.5E+01 7.7E-08 2.1E-02 108-88-3 Toluene 433 4.33 -4.4E+03 2.0E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-1.02 0.0102 -4.4E+03 4.7E-07 71-55-6 Trichloroethane, 1,1,1-0.48 0.0048 -4.4E+03 2.2E-07 79-01-6 Trichloroethylene 27.8 0.278 3.0E+00 1.8E+00 9.3E-08 3.2E-02 75-69-4 Trichlorofluoromethane 51.4 0.514 -- 95-63-6 Trimethylbenzene, 1,2,4-86.4 0.864 -5.3E+01 3.3E-03 108-67-8 Trimethylbenzene, 1,3,5-7.41 0.0741 -5.3E+01 2.8E-04 108-38-3 Xylene, m-215 2.15 -8.8E+01 4.9E-03 95-47-6 Xylene, o-76.3 0.763 -8.8E+01 1.7E-03 Cumulative:1.1E-06 4.6E-01 All concentrations are in ug/m3 Output Form 3E Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator Appendix E Receptor Survey Form North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program Site:Pharr Yarns - Lowell Address: 700 West 1st Street City:Lowell County:Gaston Brownfields Project Number: 25027-21-036 Date 8/3/2023 Property and Building Characteristics a. Provide occupancy and use information. NA NA c. Describe the foundation construction. Include details on type, floor construction, and depth below grade. NA NA e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details. NA ~20 BROWNFIELDS PROPERTY RECEPTOR SURVEY This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information requested below. Distances are measured from the site property boundary unless otherwise indicated by the DEQ Brownfield’s Project Manager (PM). Current Usage Proposed UsageSurface Conditions % of property that is grassed areas % of property that is agricultural crops % of property that is paved d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and design considerations (e.g. positive pressure?). NA ~5 If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as needed. If numerous buildings are on-site, consult with your PM as only information on specific buildings may be needed. b. Describe the construction of the building including materials (e.g. wood frame, block), type and size of openings (e.g. windows, bay doors), and height (number of stories). % of property that is covered by buildings 17.46 ~20 NA ~30 ~30 NA Size of Property (acres) % of property that is wooded/brush 17.46 ~80 ~15 Rev. 09/2015 Page 1 of 3 North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program Surrounding Property Land Use North South East West Y ~700 SE YAdjacentN, W N Utilities Is there a septic system on-site? (Y or N) N Please provide the utility providers for the subject property a. Natural Gas Piedmont Natural Gas b. Sewer City of Lowell c. Electricity Duke Energy d. Other __________________________ For surrounding properties, please complete the following table with available information. YAdjacentN/S YAdjacentN/S N---- YAdjacentN/S YAdjacentN/S N/A Is there a basement within 1,000 ft of the Property 418 S. Church Street Is there a residence within 1,000 ft of the Property? Utility/Potential Receptor Is a buried electrical cable main within 100 ft of Property boundary? * If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject property. Is a water line main within 100 ft of Property boundary? Is a natural gas line main within 100 ft of the Property boundary? Is a buried telephone/ cable main within 100 ft of the Property boundary? Is a septic system leach field within 500 ft of the Property boundary? Residential Commercial/Industrial Residential For the subject property, please provide a map of known buried utilities. If available, include depth to top, construction material, and diameter of the utilities. In addition, please provide the following information on utility providers. If additional assessment is required, the public utility locators should be contacted. This information can then be added to a site map. Y/N * Is a school or daycare center within 1,000 ft of the Specific Land Uses of Interest Y/N * * If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses. Distance (ft) See Figure 8 Is a storm water pipe within 100 ft of the Property boundary? DirectionDistance (ft)Address Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding areas. If specific receptors are present, please provide addresses of the facilities. Residential Proposed Usage Current Use/Occupant Zoning/Land Use -- N - Overhead only Unknown - Not Identified Direction Is a sanitary sewer within 100 ft of the Property boundary? Rev. 09/2015 Page 2 of 3 North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program Water Supply What is the potable water supply for the property? Public Yes Private ______ N Y N Surface Water & Wetlands Unnamed pond approximately 800 feet south of the Site. No wetlands were observed on the Site and none are suspected on adjoining properties. b. List the uses of the water body. c. What is the source of the water for the water body? d. What is the nature of the bottom of the water body (e.g., rocky or concrete bottom, drainage ways or impoundments) If no on-site surface water features, what is the nearest surface water body? Are there any wetlands present on the property? If no wetlands on-site, are wetlands suspected on adjoining properties? -- -- Response/Comments The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity of the Property. -- a. Is the water body naturally developed or man-made?-- Is a public water supply well within 1 mile of the Property boundary? Y/N Are there surface water features on the property? (If yes, please complete a. to d.) Provide Information regarding Surface Water and Wetlands Distance (ft) The purpose of this section is to provide information on the water supply for the site and surrounding areas. No Water Supply Wells Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if water supply or irrigation wells may be present. Information from applicable databases can and should be utilized; however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the requested radius, please provide a map of the well locations. If needed, please attach a separate table to list all wells. Please note, the PM may opt for a more extensive water supply well survey if needed. -- -- Central portion of Site If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include the water providers name. Direction Address Is a private water supply well within 1,500 ft of the Property bdIs an irrigation well within 1,500 ft of the Property boundary? Rev. 09/2015 Page 3 of 3