WS-4363_14151_CA_LAB_20141118_Bowman POE Monitoring Data

#=CL#
December 03, 2014
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 92226232
92226232
Project:
Pace Project No.:
RE:
Linda Blalock
NCDENR-UST Section
1637 Mail Service Canter
Raleigh, NC 276991637
HOWARD BOWMAN TF 14151
Dear Linda Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on November 19, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc:Amber Shelor, Carbonair
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 16
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 16
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92226232001 D1 SM 6200B 63 PASI-CCAH
92226232002 D3 SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Sample:D1 Lab ID:92226232001 Collected:11/18/14 11:45 Received:11/19/14 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 244 ug/L 11/27/14 15:41 71-43-21.2 2.5
Bromobenzene ND ug/L 11/27/14 15:41 108-86-11.2 2.5
Bromochloromethane ND ug/L 11/27/14 15:41 74-97-51.2 2.5
Bromodichloromethane ND ug/L 11/27/14 15:41 75-27-41.2 2.5
Bromoform ND ug/L 11/27/14 15:41 75-25-21.2 2.5
Bromomethane ND ug/L 11/27/14 15:41 74-83-912.5 2.5
n-Butylbenzene ND ug/L 11/27/14 15:41 104-51-81.2 2.5
sec-Butylbenzene ND ug/L 11/27/14 15:41 135-98-81.2 2.5
tert-Butylbenzene ND ug/L 11/27/14 15:41 98-06-61.2 2.5
Carbon tetrachloride ND ug/L 11/27/14 15:41 56-23-51.2 2.5
Chlorobenzene ND ug/L 11/27/14 15:41 108-90-71.2 2.5
Chloroethane ND ug/L 11/27/14 15:41 75-00-32.5 2.5
Chloroform ND ug/L 11/27/14 15:41 67-66-31.2 2.5
Chloromethane ND ug/L 11/27/14 15:41 74-87-32.5 2.5
2-Chlorotoluene ND ug/L 11/27/14 15:41 95-49-81.2 2.5
4-Chlorotoluene ND ug/L 11/27/14 15:41 106-43-41.2 2.5
1,2-Dibromo-3-chloropropane ND ug/L 11/27/14 15:41 96-12-82.5 2.5
Dibromochloromethane ND ug/L 11/27/14 15:41 124-48-11.2 2.5
1,2-Dibromoethane (EDB)ND ug/L 11/27/14 15:41 106-93-41.2 2.5
Dibromomethane ND ug/L 11/27/14 15:41 74-95-31.2 2.5
1,2-Dichlorobenzene ND ug/L 11/27/14 15:41 95-50-11.2 2.5
1,3-Dichlorobenzene ND ug/L 11/27/14 15:41 541-73-11.2 2.5
1,4-Dichlorobenzene ND ug/L 11/27/14 15:41 106-46-71.2 2.5
Dichlorodifluoromethane ND ug/L 11/27/14 15:41 75-71-81.2 2.5
1,1-Dichloroethane ND ug/L 11/27/14 15:41 75-34-31.2 2.5
1,2-Dichloroethane 8.0 ug/L 11/27/14 15:41 107-06-21.2 2.5
1,1-Dichloroethene ND ug/L 11/27/14 15:41 75-35-41.2 2.5
cis-1,2-Dichloroethene ND ug/L 11/27/14 15:41 156-59-21.2 2.5
trans-1,2-Dichloroethene ND ug/L 11/27/14 15:41 156-60-51.2 2.5
1,2-Dichloropropane ND ug/L 11/27/14 15:41 78-87-51.2 2.5
1,3-Dichloropropane ND ug/L 11/27/14 15:41 142-28-91.2 2.5
2,2-Dichloropropane ND ug/L 11/27/14 15:41 594-20-71.2 2.5
1,1-Dichloropropene ND ug/L 11/27/14 15:41 563-58-61.2 2.5
cis-1,3-Dichloropropene ND ug/L 11/27/14 15:41 10061-01-51.2 2.5
trans-1,3-Dichloropropene ND ug/L 11/27/14 15:41 10061-02-61.2 2.5
Diisopropyl ether 310 ug/L 11/27/14 15:41 108-20-31.2 2.5
Ethylbenzene ND ug/L 11/27/14 15:41 100-41-41.2 2.5
Hexachloro-1,3-butadiene ND ug/L 11/27/14 15:41 87-68-35.0 2.5
Isopropylbenzene (Cumene)4.1 ug/L 11/27/14 15:41 98-82-81.2 2.5
Methylene Chloride ND ug/L 11/27/14 15:41 75-09-25.0 2.5
Methyl-tert-butyl ether 2.6 ug/L 11/27/14 15:41 1634-04-41.2 2.5
Naphthalene 22.3 ug/L 11/27/14 15:41 91-20-35.0 2.5
n-Propylbenzene 4.1 ug/L 11/27/14 15:41 103-65-11.2 2.5
Styrene ND ug/L 11/27/14 15:41 100-42-51.2 2.5
1,1,1,2-Tetrachloroethane ND ug/L 11/27/14 15:41 630-20-61.2 2.5
1,1,2,2-Tetrachloroethane ND ug/L 11/27/14 15:41 79-34-51.2 2.5
Tetrachloroethene ND ug/L 11/27/14 15:41 127-18-41.2 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2014 01:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Sample:D1 Lab ID:92226232001 Collected:11/18/14 11:45 Received:11/19/14 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 11/27/14 15:41 108-88-31.2 2.5
1,2,3-Trichlorobenzene ND ug/L 11/27/14 15:41 87-61-65.0 2.5
1,2,4-Trichlorobenzene ND ug/L 11/27/14 15:41 120-82-15.0 2.5
1,1,1-Trichloroethane ND ug/L 11/27/14 15:41 71-55-61.2 2.5
1,1,2-Trichloroethane ND ug/L 11/27/14 15:41 79-00-51.2 2.5
Trichloroethene ND ug/L 11/27/14 15:41 79-01-61.2 2.5
Trichlorofluoromethane ND ug/L 11/27/14 15:41 75-69-42.5 2.5
1,2,3-Trichloropropane ND ug/L 11/27/14 15:41 96-18-41.2 2.5
1,2,4-Trimethylbenzene 82.7 ug/L 11/27/14 15:41 95-63-61.2 2.5
1,3,5-Trimethylbenzene 12.4 ug/L 11/27/14 15:41 108-67-81.2 2.5
Vinyl chloride ND ug/L 11/27/14 15:41 75-01-42.5 2.5
m&p-Xylene 107 ug/L 11/27/14 15:41 179601-23-12.5 2.5
o-Xylene 80.3 ug/L 11/27/14 15:41 95-47-61.2 2.5
Surrogates
1,2-Dichloroethane-d4 (S)107 %11/27/14 15:41 17060-07-070-130 2.5
4-Bromofluorobenzene (S)97 %11/27/14 15:41 460-00-470-130 2.5
Toluene-d8 (S)100 %11/27/14 15:41 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2014 01:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Sample:D3 Lab ID:92226232002 Collected:11/18/14 11:40 Received:11/19/14 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 11/27/14 12:53 71-43-20.50 1
Bromobenzene ND ug/L 11/27/14 12:53 108-86-10.50 1
Bromochloromethane ND ug/L 11/27/14 12:53 74-97-50.50 1
Bromodichloromethane ND ug/L 11/27/14 12:53 75-27-40.50 1
Bromoform ND ug/L 11/27/14 12:53 75-25-20.50 1
Bromomethane ND ug/L 11/27/14 12:53 74-83-95.0 1
n-Butylbenzene ND ug/L 11/27/14 12:53 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/27/14 12:53 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/27/14 12:53 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/27/14 12:53 56-23-50.50 1
Chlorobenzene ND ug/L 11/27/14 12:53 108-90-70.50 1
Chloroethane ND ug/L 11/27/14 12:53 75-00-31.0 1
Chloroform ND ug/L 11/27/14 12:53 67-66-30.50 1
Chloromethane ND ug/L 11/27/14 12:53 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/27/14 12:53 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/27/14 12:53 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/27/14 12:53 96-12-81.0 1
Dibromochloromethane ND ug/L 11/27/14 12:53 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/27/14 12:53 106-93-40.50 1
Dibromomethane ND ug/L 11/27/14 12:53 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/27/14 12:53 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/27/14 12:53 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/27/14 12:53 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/27/14 12:53 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/27/14 12:53 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/27/14 12:53 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/27/14 12:53 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/27/14 12:53 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/27/14 12:53 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/27/14 12:53 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/27/14 12:53 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/27/14 12:53 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/27/14 12:53 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/27/14 12:53 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/27/14 12:53 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/27/14 12:53 108-20-30.50 1
Ethylbenzene ND ug/L 11/27/14 12:53 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/27/14 12:53 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/27/14 12:53 98-82-80.50 1
Methylene Chloride ND ug/L 11/27/14 12:53 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/27/14 12:53 1634-04-40.50 1
Naphthalene ND ug/L 11/27/14 12:53 91-20-32.0 1
n-Propylbenzene ND ug/L 11/27/14 12:53 103-65-10.50 1
Styrene ND ug/L 11/27/14 12:53 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/27/14 12:53 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/27/14 12:53 79-34-50.50 1
Tetrachloroethene ND ug/L 11/27/14 12:53 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2014 01:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Sample:D3 Lab ID:92226232002 Collected:11/18/14 11:40 Received:11/19/14 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 11/27/14 12:53 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/27/14 12:53 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/27/14 12:53 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/27/14 12:53 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/27/14 12:53 79-00-50.50 1
Trichloroethene ND ug/L 11/27/14 12:53 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/27/14 12:53 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/27/14 12:53 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/27/14 12:53 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/27/14 12:53 108-67-80.50 1
Vinyl chloride ND ug/L 11/27/14 12:53 75-01-41.0 1
m&p-Xylene ND ug/L 11/27/14 12:53 179601-23-11.0 1
o-Xylene ND ug/L 11/27/14 12:53 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %11/27/14 12:53 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %11/27/14 12:53 460-00-470-130 1
Toluene-d8 (S)101 %11/27/14 12:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2014 01:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/29406
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92226232001, 92226232002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1339924
Associated Lab Samples:92226232001, 92226232002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/27/14 10:06
1,1,1-Trichloroethane ug/L ND 0.50 11/27/14 10:06
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/27/14 10:06
1,1,2-Trichloroethane ug/L ND 0.50 11/27/14 10:06
1,1-Dichloroethane ug/L ND 0.50 11/27/14 10:06
1,1-Dichloroethene ug/L ND 0.50 11/27/14 10:06
1,1-Dichloropropene ug/L ND 0.50 11/27/14 10:06
1,2,3-Trichlorobenzene ug/L ND 2.0 11/27/14 10:06
1,2,3-Trichloropropane ug/L ND 0.50 11/27/14 10:06
1,2,4-Trichlorobenzene ug/L ND 2.0 11/27/14 10:06
1,2,4-Trimethylbenzene ug/L ND 0.50 11/27/14 10:06
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/27/14 10:06
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/27/14 10:06
1,2-Dichlorobenzene ug/L ND 0.50 11/27/14 10:06
1,2-Dichloroethane ug/L ND 0.50 11/27/14 10:06
1,2-Dichloropropane ug/L ND 0.50 11/27/14 10:06
1,3,5-Trimethylbenzene ug/L ND 0.50 11/27/14 10:06
1,3-Dichlorobenzene ug/L ND 0.50 11/27/14 10:06
1,3-Dichloropropane ug/L ND 0.50 11/27/14 10:06
1,4-Dichlorobenzene ug/L ND 0.50 11/27/14 10:06
2,2-Dichloropropane ug/L ND 0.50 11/27/14 10:06
2-Chlorotoluene ug/L ND 0.50 11/27/14 10:06
4-Chlorotoluene ug/L ND 0.50 11/27/14 10:06
Benzene ug/L ND 0.50 11/27/14 10:06
Bromobenzene ug/L ND 0.50 11/27/14 10:06
Bromochloromethane ug/L ND 0.50 11/27/14 10:06
Bromodichloromethane ug/L ND 0.50 11/27/14 10:06
Bromoform ug/L ND 0.50 11/27/14 10:06
Bromomethane ug/L ND 5.0 11/27/14 10:06
Carbon tetrachloride ug/L ND 0.50 11/27/14 10:06
Chlorobenzene ug/L ND 0.50 11/27/14 10:06
Chloroethane ug/L ND 1.0 11/27/14 10:06
Chloroform ug/L ND 0.50 11/27/14 10:06
Chloromethane ug/L ND 1.0 11/27/14 10:06
cis-1,2-Dichloroethene ug/L ND 0.50 11/27/14 10:06
cis-1,3-Dichloropropene ug/L ND 0.50 11/27/14 10:06
Dibromochloromethane ug/L ND 0.50 11/27/14 10:06
Dibromomethane ug/L ND 0.50 11/27/14 10:06
Dichlorodifluoromethane ug/L ND 0.50 11/27/14 10:06
Diisopropyl ether ug/L ND 0.50 11/27/14 10:06
Ethylbenzene ug/L ND 0.50 11/27/14 10:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2014 01:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1339924
Associated Lab Samples:92226232001, 92226232002
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 11/27/14 10:06
Isopropylbenzene (Cumene)ug/L ND 0.50 11/27/14 10:06
m&p-Xylene ug/L ND 1.0 11/27/14 10:06
Methyl-tert-butyl ether ug/L ND 0.50 11/27/14 10:06
Methylene Chloride ug/L ND 2.0 11/27/14 10:06
n-Butylbenzene ug/L ND 0.50 11/27/14 10:06
n-Propylbenzene ug/L ND 0.50 11/27/14 10:06
Naphthalene ug/L ND 2.0 11/27/14 10:06
o-Xylene ug/L ND 0.50 11/27/14 10:06
sec-Butylbenzene ug/L ND 0.50 11/27/14 10:06
Styrene ug/L ND 0.50 11/27/14 10:06
tert-Butylbenzene ug/L ND 0.50 11/27/14 10:06
Tetrachloroethene ug/L ND 0.50 11/27/14 10:06
Toluene ug/L ND 0.50 11/27/14 10:06
trans-1,2-Dichloroethene ug/L ND 0.50 11/27/14 10:06
trans-1,3-Dichloropropene ug/L ND 0.50 11/27/14 10:06
Trichloroethene ug/L ND 0.50 11/27/14 10:06
Trichlorofluoromethane ug/L ND 1.0 11/27/14 10:06
Vinyl chloride ug/L ND 1.0 11/27/14 10:06
1,2-Dichloroethane-d4 (S)%102 70-130 11/27/14 10:06
4-Bromofluorobenzene (S)%97 70-130 11/27/14 10:06
Toluene-d8 (S)%100 70-130 11/27/14 10:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1339925LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.450 105 60-140
1,1,1-Trichloroethane ug/L 51.950 104 60-140
1,1,2,2-Tetrachloroethane ug/L 51.950 104 60-140
1,1,2-Trichloroethane ug/L 52.450 105 60-140
1,1-Dichloroethane ug/L 51.850 104 60-140
1,1-Dichloroethene ug/L 45.550 91 60-140
1,1-Dichloropropene ug/L 55.650 111 60-140
1,2,3-Trichlorobenzene ug/L 54.350 109 60-140
1,2,3-Trichloropropane ug/L 49.550 99 60-140
1,2,4-Trichlorobenzene ug/L 55.050 110 60-140
1,2,4-Trimethylbenzene ug/L 54.050 108 60-140
1,2-Dibromo-3-chloropropane ug/L 90.8 CU,L35018260-140
1,2-Dibromoethane (EDB)ug/L 52.850 106 60-140
1,2-Dichlorobenzene ug/L 52.150 104 60-140
1,2-Dichloroethane ug/L 48.350 97 60-140
1,2-Dichloropropane ug/L 49.950 100 60-140
1,3,5-Trimethylbenzene ug/L 54.250 108 60-140
1,3-Dichlorobenzene ug/L 51.550 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2014 01:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1339925LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 50.550 101 60-140
1,4-Dichlorobenzene ug/L 50.750 101 60-140
2,2-Dichloropropane ug/L 54.650 109 60-140
2-Chlorotoluene ug/L 51.550 103 60-140
4-Chlorotoluene ug/L 52.450 105 60-140
Benzene ug/L 52.850 106 60-140
Bromobenzene ug/L 50.750 101 60-140
Bromochloromethane ug/L 49.150 98 60-140
Bromodichloromethane ug/L 47.850 96 60-140
Bromoform ug/L 43.150 86 60-140
Bromomethane ug/L 40.650 81 60-140
Carbon tetrachloride ug/L 52.050 104 60-140
Chlorobenzene ug/L 50.050 100 60-140
Chloroethane ug/L 38.350 77 60-140
Chloroform ug/L 46.750 93 60-140
Chloromethane ug/L 53.050 106 60-140
cis-1,2-Dichloroethene ug/L 52.450 105 60-140
cis-1,3-Dichloropropene ug/L 54.450 109 60-140
Dibromochloromethane ug/L 49.050 98 60-140
Dibromomethane ug/L 50.350 101 60-140
Dichlorodifluoromethane ug/L 50.150 100 60-140
Diisopropyl ether ug/L 48.850 98 60-140
Ethylbenzene ug/L 52.050 104 60-140
Hexachloro-1,3-butadiene ug/L 55.550 111 60-140
Isopropylbenzene (Cumene)ug/L 53.350 107 60-140
m&p-Xylene ug/L 104100 104 60-140
Methyl-tert-butyl ether ug/L 46.550 93 60-140
Methylene Chloride ug/L 45.950 92 60-140
n-Butylbenzene ug/L 56.350 113 60-140
n-Propylbenzene ug/L 52.550 105 60-140
Naphthalene ug/L 56.150 112 60-140
o-Xylene ug/L 51.050 102 60-140
sec-Butylbenzene ug/L 53.650 107 60-140
Styrene ug/L 55.950 112 60-140
tert-Butylbenzene ug/L 46.050 92 60-140
Tetrachloroethene ug/L 48.250 96 60-140
Toluene ug/L 51.350 103 60-140
trans-1,2-Dichloroethene ug/L 47.250 94 60-140
trans-1,3-Dichloropropene ug/L 55.550 111 60-140
Trichloroethene ug/L 51.150 102 60-140
Trichlorofluoromethane ug/L 48.150 96 60-140
Vinyl chloride ug/L 56.050 112 60-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2014 01:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1339926MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92226135022
1339927
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 104 60-140107 320ND20.9 21.5
1,1,1-Trichloroethane ug/L 20 114 60-140115 120ND22.8 23.0
1,1,2,2-Tetrachloroethane ug/L 20 101 60-140105 420ND20.1 21.0
1,1,2-Trichloroethane ug/L 20 104 60-140109 420ND20.9 21.8
1,1-Dichloroethane ug/L 20 113 60-140114 120ND22.6 22.8
1,1-Dichloroethene ug/L 20 107 60-140108 020ND21.5 21.5
1,1-Dichloropropene ug/L 20 121 60-140122 120ND24.3 24.5
1,2,3-Trichlorobenzene ug/L 20 99 60-140107 720ND20.0 21.5
1,2,3-Trichloropropane ug/L 20 98 60-140103 520ND19.5 20.6
1,2,4-Trichlorobenzene ug/L 20 100 60-140105 520ND20.2 21.1
1,2,4-Trimethylbenzene ug/L 20 111 60-140113 220ND22.1 22.6
1,2-Dibromo-3-chloropropane ug/L M02015760-140164 420ND31.4 32.9
1,2-Dibromoethane (EDB)ug/L 20 102 60-140106 320ND20.5 21.1
1,2-Dichlorobenzene ug/L 20 104 60-140108 420ND20.8 21.6
1,2-Dichloroethane ug/L 20 104 60-140106 220ND20.8 21.2
1,2-Dichloropropane ug/L 20 104 60-140107 320ND20.9 21.5
1,3,5-Trimethylbenzene ug/L 20 111 60-140114 320ND22.1 22.8
1,3-Dichlorobenzene ug/L 20 104 60-140107 320ND20.7 21.5
1,3-Dichloropropane ug/L 20 100 60-140105 620ND19.9 21.1
1,4-Dichlorobenzene ug/L 20 102 60-140105 420ND20.4 21.2
2,2-Dichloropropane ug/L 20 105 60-140107 220ND20.9 21.4
2-Chlorotoluene ug/L 20 104 60-140107 220ND20.9 21.3
4-Chlorotoluene ug/L 20 106 60-140109 320ND21.2 21.8
Benzene ug/L 20 112 60-140113 020ND22.5 22.6
Bromobenzene ug/L 20 100 60-140107 720ND20.0 21.4
Bromochloromethane ug/L 20 112 60-140113 020ND22.5 22.6
Bromodichloromethane ug/L 20 95 60-14096 020ND19.1 19.1
Bromoform ug/L 20 78 60-14082 520ND15.5 16.3
Bromomethane ug/L 20 103 60-14094 1020ND20.6 18.8
Carbon tetrachloride ug/L 20 109 60-140111 220ND21.7 22.3
Chlorobenzene ug/L 20 105 60-140106 220ND21.0 21.3
Chloroethane ug/L 20 111 60-140105 520ND22.2 21.1
Chloroform ug/L 20 101 60-140103 220ND20.2 20.5
Chloromethane ug/L 20 116 60-140118 120ND23.3 23.6
cis-1,2-Dichloroethene ug/L 20 113 60-140115 220ND22.7 23.1
cis-1,3-Dichloropropene ug/L 20 100 60-140104 420ND20.0 20.8
Dibromochloromethane ug/L 20 89 60-14096 720ND17.8 19.2
Dibromomethane ug/L 20 101 60-140104 320ND20.3 20.8
Dichlorodifluoromethane ug/L 20 112 60-140111 120ND22.4 22.2
Diisopropyl ether ug/L 20 106 60-140106 120ND21.1 21.2
Ethylbenzene ug/L 20 108 60-140112 420ND21.6 22.5
Hexachloro-1,3-butadiene ug/L 20 104 60-140109 620ND20.7 21.9
Isopropylbenzene (Cumene)ug/L 20 111 60-140114 320ND22.3 22.8
m&p-Xylene ug/L 40 110 60-140113 340ND44.0 45.2
Methyl-tert-butyl ether ug/L 20 91 60-14087 420ND18.2 17.5
Methylene Chloride ug/L 20 98 60-140102 420ND19.6 20.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2014 01:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1339926MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92226135022
1339927
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 111 60-140114 320ND22.3 22.8
n-Propylbenzene ug/L 20 109 60-140111 220ND21.8 22.3
Naphthalene ug/L 20 103 60-140110 620ND20.8 22.1
o-Xylene ug/L 20 104 60-140106 220ND20.8 21.3
sec-Butylbenzene ug/L 20 110 60-140113 220ND22.1 22.5
Styrene ug/L 20 110 60-140115 420ND22.1 22.9
tert-Butylbenzene ug/L 20 94 60-14097 320ND18.8 19.3
Tetrachloroethene ug/L 20 100 60-140104 420ND19.9 20.7
Toluene ug/L 20 109 60-140110 020ND21.9 22.0
trans-1,2-Dichloroethene ug/L 20 109 60-140112 320ND21.8 22.4
trans-1,3-Dichloropropene ug/L 20 103 60-140108 520ND20.7 21.7
Trichloroethene ug/L 20 109 60-140111 120ND21.8 22.1
Trichlorofluoromethane ug/L 20 122 60-140120 220ND24.4 23.9
Vinyl chloride ug/L 20 127 60-140128 120ND25.4 25.7
1,2-Dichloroethane-d4 (S)%103 70-130102
4-Bromofluorobenzene (S)%99 70-130100
Toluene-d8 (S)%101 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2014 01:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 16
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. Analyte presence below
reporting limits in associated samples. Results unaffected by high bias.CU
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2014 01:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 16
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92226232
HOWARD BOWMAN TF 14151
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92226232001 MSV/29406D1SM 6200B
92226232002 MSV/29406D3SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2014 01:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 16
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