WS-4363_14151_CA_LAB_20140605_Bowman_POE_Monitoring_Data

#=CL#
June 05, 2014
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 92202989
92202989
Project:
Pace Project No.:
RE:
Linda Blalock
NCDENR-UST Section
1637 Mail Service Canter
Raleigh, NC 276991637
Howard Bowman TF#14151
Dear Linda Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on May 28, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc:Amber Shelor, Carbonair
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92202989001 D1 SM 6200B 63 PASI-CCAH
92202989002 D3 SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Sample:D1 Lab ID:92202989001 Collected:05/27/14 08:45 Received:05/28/14 11:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene 258 ug/L 05/30/14 03:34 71-43-21.2 2.5
Bromobenzene ND ug/L 05/30/14 03:34 108-86-11.2 2.5
Bromochloromethane ND ug/L 05/30/14 03:34 74-97-51.2 2.5
Bromodichloromethane ND ug/L 05/30/14 03:34 75-27-41.2 2.5
Bromoform ND ug/L 05/30/14 03:34 75-25-21.2 2.5
Bromomethane ND ug/L 05/30/14 03:34 74-83-912.5 2.5
n-Butylbenzene ND ug/L 05/30/14 03:34 104-51-81.2 2.5
sec-Butylbenzene ND ug/L 05/30/14 03:34 135-98-81.2 2.5
tert-Butylbenzene ND ug/L 05/30/14 03:34 98-06-61.2 2.5
Carbon tetrachloride ND ug/L 05/30/14 03:34 56-23-51.2 2.5
Chlorobenzene ND ug/L 05/30/14 03:34 108-90-71.2 2.5
Chloroethane ND ug/L 05/30/14 03:34 75-00-32.5 2.5
Chloroform ND ug/L 05/30/14 03:34 67-66-31.2 2.5
Chloromethane ND ug/L 05/30/14 03:34 74-87-32.5 2.5
2-Chlorotoluene ND ug/L 05/30/14 03:34 95-49-81.2 2.5
4-Chlorotoluene ND ug/L 05/30/14 03:34 106-43-41.2 2.5
1,2-Dibromo-3-chloropropane ND ug/L 05/30/14 03:34 96-12-82.5 2.5
Dibromochloromethane ND ug/L 05/30/14 03:34 124-48-11.2 2.5
1,2-Dibromoethane (EDB)ND ug/L 05/30/14 03:34 106-93-41.2 2.5
Dibromomethane ND ug/L 05/30/14 03:34 74-95-31.2 2.5
1,2-Dichlorobenzene ND ug/L 05/30/14 03:34 95-50-11.2 2.5
1,3-Dichlorobenzene ND ug/L 05/30/14 03:34 541-73-11.2 2.5
1,4-Dichlorobenzene ND ug/L 05/30/14 03:34 106-46-71.2 2.5
Dichlorodifluoromethane ND ug/L 05/30/14 03:34 75-71-81.2 2.5
1,1-Dichloroethane ND ug/L 05/30/14 03:34 75-34-31.2 2.5
1,2-Dichloroethane 8.1 ug/L 05/30/14 03:34 107-06-21.2 2.5
1,1-Dichloroethene ND ug/L 05/30/14 03:34 75-35-41.2 2.5
cis-1,2-Dichloroethene ND ug/L 05/30/14 03:34 156-59-21.2 2.5
trans-1,2-Dichloroethene ND ug/L 05/30/14 03:34 156-60-51.2 2.5
1,2-Dichloropropane ND ug/L 05/30/14 03:34 78-87-51.2 2.5
1,3-Dichloropropane ND ug/L 05/30/14 03:34 142-28-91.2 2.5
2,2-Dichloropropane ND ug/L 05/30/14 03:34 594-20-71.2 2.5
1,1-Dichloropropene ND ug/L 05/30/14 03:34 563-58-61.2 2.5
cis-1,3-Dichloropropene ND ug/L 05/30/14 03:34 10061-01-51.2 2.5
trans-1,3-Dichloropropene ND ug/L 05/30/14 03:34 10061-02-61.2 2.5
Diisopropyl ether 294 ug/L 05/30/14 03:34 108-20-31.2 2.5
Ethylbenzene ND ug/L 05/30/14 03:34 100-41-41.2 2.5
Hexachloro-1,3-butadiene ND ug/L 05/30/14 03:34 87-68-35.0 2.5
Isopropylbenzene (Cumene)4.6 ug/L 05/30/14 03:34 98-82-81.2 2.5
Methylene Chloride ND ug/L 05/30/14 03:34 75-09-25.0 2.5
Methyl-tert-butyl ether 2.7 ug/L 05/30/14 03:34 1634-04-41.2 2.5
Naphthalene 21.4 ug/L 05/30/14 03:34 91-20-35.0 2.5
n-Propylbenzene 5.1 ug/L 05/30/14 03:34 103-65-11.2 2.5
Styrene ND ug/L 05/30/14 03:34 100-42-51.2 2.5
1,1,1,2-Tetrachloroethane ND ug/L 05/30/14 03:34 630-20-61.2 2.5
1,1,2,2-Tetrachloroethane ND ug/L 05/30/14 03:34 79-34-51.2 2.5
Tetrachloroethene ND ug/L 05/30/14 03:34 127-18-41.2 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Sample:D1 Lab ID:92202989001 Collected:05/27/14 08:45 Received:05/28/14 11:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 05/30/14 03:34 108-88-31.2 2.5
1,2,3-Trichlorobenzene ND ug/L 05/30/14 03:34 87-61-65.0 2.5
1,2,4-Trichlorobenzene ND ug/L 05/30/14 03:34 120-82-15.0 2.5
1,1,1-Trichloroethane ND ug/L 05/30/14 03:34 71-55-61.2 2.5
1,1,2-Trichloroethane ND ug/L 05/30/14 03:34 79-00-51.2 2.5
Trichloroethene ND ug/L 05/30/14 03:34 79-01-61.2 2.5
Trichlorofluoromethane ND ug/L 05/30/14 03:34 75-69-42.5 2.5
1,2,3-Trichloropropane ND ug/L 05/30/14 03:34 96-18-41.2 2.5
1,2,4-Trimethylbenzene 80.4 ug/L 05/30/14 03:34 95-63-61.2 2.5
1,3,5-Trimethylbenzene 11.2 ug/L 05/30/14 03:34 108-67-81.2 2.5
Vinyl chloride ND ug/L 05/30/14 03:34 75-01-42.5 2.5
m&p-Xylene 110 ug/L 05/30/14 03:34 179601-23-12.5 2.5
o-Xylene 80.7 ug/L 05/30/14 03:34 95-47-61.2 2.5
Surrogates
1,2-Dichloroethane-d4 (S)99 %05/30/14 03:34 17060-07-070-130 2.5
4-Bromofluorobenzene (S)98 %05/30/14 03:34 460-00-470-130 2.5
Toluene-d8 (S)99 %05/30/14 03:34 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Sample:D3 Lab ID:92202989002 Collected:05/27/14 08:40 Received:05/28/14 11:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 06/03/14 22:09 71-43-20.50 1
Bromobenzene ND ug/L 06/03/14 22:09 108-86-10.50 1
Bromochloromethane ND ug/L 06/03/14 22:09 74-97-50.50 1
Bromodichloromethane ND ug/L 06/03/14 22:09 75-27-40.50 1
Bromoform ND ug/L 06/03/14 22:09 75-25-20.50 1
Bromomethane ND ug/L 06/03/14 22:09 74-83-95.0 1
n-Butylbenzene ND ug/L 06/03/14 22:09 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/03/14 22:09 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/03/14 22:09 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/03/14 22:09 56-23-50.50 1
Chlorobenzene ND ug/L 06/03/14 22:09 108-90-70.50 1
Chloroethane ND ug/L 06/03/14 22:09 75-00-31.0 1
Chloroform ND ug/L 06/03/14 22:09 67-66-30.50 1
Chloromethane ND ug/L 06/03/14 22:09 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/03/14 22:09 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/03/14 22:09 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/03/14 22:09 96-12-81.0 1
Dibromochloromethane ND ug/L 06/03/14 22:09 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/03/14 22:09 106-93-40.50 1
Dibromomethane ND ug/L 06/03/14 22:09 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/03/14 22:09 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/03/14 22:09 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/03/14 22:09 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/03/14 22:09 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/03/14 22:09 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/03/14 22:09 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/03/14 22:09 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/03/14 22:09 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/03/14 22:09 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/03/14 22:09 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/03/14 22:09 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/03/14 22:09 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/03/14 22:09 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/03/14 22:09 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/03/14 22:09 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/03/14 22:09 108-20-30.50 1
Ethylbenzene ND ug/L 06/03/14 22:09 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/03/14 22:09 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/03/14 22:09 98-82-80.50 1
Methylene Chloride ND ug/L 06/03/14 22:09 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/03/14 22:09 1634-04-40.50 1
Naphthalene ND ug/L 06/03/14 22:09 91-20-32.0 1
n-Propylbenzene ND ug/L 06/03/14 22:09 103-65-10.50 1
Styrene ND ug/L 06/03/14 22:09 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/03/14 22:09 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/03/14 22:09 79-34-50.50 1
Tetrachloroethene ND ug/L 06/03/14 22:09 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Sample:D3 Lab ID:92202989002 Collected:05/27/14 08:40 Received:05/28/14 11:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 06/03/14 22:09 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/03/14 22:09 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/03/14 22:09 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/03/14 22:09 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/03/14 22:09 79-00-50.50 1
Trichloroethene ND ug/L 06/03/14 22:09 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/03/14 22:09 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/03/14 22:09 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/03/14 22:09 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/03/14 22:09 108-67-80.50 1
Vinyl chloride ND ug/L 06/03/14 22:09 75-01-41.0 1
m&p-Xylene ND ug/L 06/03/14 22:09 179601-23-11.0 1
o-Xylene ND ug/L 06/03/14 22:09 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %06/03/14 22:09 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %06/03/14 22:09 460-00-470-130 1
Toluene-d8 (S)101 %06/03/14 22:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27001
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92202989001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1209398
Associated Lab Samples:92202989001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/29/14 22:36
1,1,1-Trichloroethane ug/L ND 0.50 05/29/14 22:36
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/29/14 22:36
1,1,2-Trichloroethane ug/L ND 0.50 05/29/14 22:36
1,1-Dichloroethane ug/L ND 0.50 05/29/14 22:36
1,1-Dichloroethene ug/L ND 0.50 05/29/14 22:36
1,1-Dichloropropene ug/L ND 0.50 05/29/14 22:36
1,2,3-Trichlorobenzene ug/L ND 2.0 05/29/14 22:36
1,2,3-Trichloropropane ug/L ND 0.50 05/29/14 22:36
1,2,4-Trichlorobenzene ug/L ND 2.0 05/29/14 22:36
1,2,4-Trimethylbenzene ug/L ND 0.50 05/29/14 22:36
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/29/14 22:36
1,2-Dibromoethane (EDB)ug/L ND 0.50 05/29/14 22:36
1,2-Dichlorobenzene ug/L ND 0.50 05/29/14 22:36
1,2-Dichloroethane ug/L ND 0.50 05/29/14 22:36
1,2-Dichloropropane ug/L ND 0.50 05/29/14 22:36
1,3,5-Trimethylbenzene ug/L ND 0.50 05/29/14 22:36
1,3-Dichlorobenzene ug/L ND 0.50 05/29/14 22:36
1,3-Dichloropropane ug/L ND 0.50 05/29/14 22:36
1,4-Dichlorobenzene ug/L ND 0.50 05/29/14 22:36
2,2-Dichloropropane ug/L ND 0.50 05/29/14 22:36
2-Chlorotoluene ug/L ND 0.50 05/29/14 22:36
4-Chlorotoluene ug/L ND 0.50 05/29/14 22:36
Benzene ug/L ND 0.50 05/29/14 22:36
Bromobenzene ug/L ND 0.50 05/29/14 22:36
Bromochloromethane ug/L ND 0.50 05/29/14 22:36
Bromodichloromethane ug/L ND 0.50 05/29/14 22:36
Bromoform ug/L ND 0.50 05/29/14 22:36
Bromomethane ug/L ND 5.0 05/29/14 22:36
Carbon tetrachloride ug/L ND 0.50 05/29/14 22:36
Chlorobenzene ug/L ND 0.50 05/29/14 22:36
Chloroethane ug/L ND 1.0 05/29/14 22:36
Chloroform ug/L ND 0.50 05/29/14 22:36
Chloromethane ug/L ND 1.0 05/29/14 22:36
cis-1,2-Dichloroethene ug/L ND 0.50 05/29/14 22:36
cis-1,3-Dichloropropene ug/L ND 0.50 05/29/14 22:36
Dibromochloromethane ug/L ND 0.50 05/29/14 22:36
Dibromomethane ug/L ND 0.50 05/29/14 22:36
Dichlorodifluoromethane ug/L ND 0.50 05/29/14 22:36
Diisopropyl ether ug/L ND 0.50 05/29/14 22:36
Ethylbenzene ug/L ND 0.50 05/29/14 22:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1209398
Associated Lab Samples:92202989001
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 05/29/14 22:36
Isopropylbenzene (Cumene)ug/L ND 0.50 05/29/14 22:36
m&p-Xylene ug/L ND 1.0 05/29/14 22:36
Methyl-tert-butyl ether ug/L ND 0.50 05/29/14 22:36
Methylene Chloride ug/L ND 2.0 05/29/14 22:36
n-Butylbenzene ug/L ND 0.50 05/29/14 22:36
n-Propylbenzene ug/L ND 0.50 05/29/14 22:36
Naphthalene ug/L ND 2.0 05/29/14 22:36
o-Xylene ug/L ND 0.50 05/29/14 22:36
sec-Butylbenzene ug/L ND 0.50 05/29/14 22:36
Styrene ug/L ND 0.50 05/29/14 22:36
tert-Butylbenzene ug/L ND 0.50 05/29/14 22:36
Tetrachloroethene ug/L ND 0.50 05/29/14 22:36
Toluene ug/L ND 0.50 05/29/14 22:36
trans-1,2-Dichloroethene ug/L ND 0.50 05/29/14 22:36
trans-1,3-Dichloropropene ug/L ND 0.50 05/29/14 22:36
Trichloroethene ug/L ND 0.50 05/29/14 22:36
Trichlorofluoromethane ug/L ND 1.0 05/29/14 22:36
Vinyl chloride ug/L ND 1.0 05/29/14 22:36
1,2-Dichloroethane-d4 (S)%96 70-130 05/29/14 22:36
4-Bromofluorobenzene (S)%97 70-130 05/29/14 22:36
Toluene-d8 (S)%100 70-130 05/29/14 22:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1209399LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 58.950 118 60-140
1,1,1-Trichloroethane ug/L 50.150 100 60-140
1,1,2,2-Tetrachloroethane ug/L 52.650 105 60-140
1,1,2-Trichloroethane ug/L 53.750 107 60-140
1,1-Dichloroethane ug/L 47.150 94 60-140
1,1-Dichloroethene ug/L 50.250 100 60-140
1,1-Dichloropropene ug/L 50.550 101 60-140
1,2,3-Trichlorobenzene ug/L 56.850 114 60-140
1,2,3-Trichloropropane ug/L 53.250 106 60-140
1,2,4-Trichlorobenzene ug/L 55.050 110 60-140
1,2,4-Trimethylbenzene ug/L 56.050 112 60-140
1,2-Dibromo-3-chloropropane ug/L 57.850 116 60-140
1,2-Dibromoethane (EDB)ug/L 54.450 109 60-140
1,2-Dichlorobenzene ug/L 54.050 108 60-140
1,2-Dichloroethane ug/L 48.750 97 60-140
1,2-Dichloropropane ug/L 49.050 98 60-140
1,3,5-Trimethylbenzene ug/L 54.850 110 60-140
1,3-Dichlorobenzene ug/L 53.950 108 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1209399LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 51.450 103 60-140
1,4-Dichlorobenzene ug/L 52.250 104 60-140
2,2-Dichloropropane ug/L 46.650 93 60-140
2-Chlorotoluene ug/L 52.450 105 60-140
4-Chlorotoluene ug/L 51.350 103 60-140
Benzene ug/L 51.750 103 60-140
Bromobenzene ug/L 52.650 105 60-140
Bromochloromethane ug/L 50.850 102 60-140
Bromodichloromethane ug/L 56.650 113 60-140
Bromoform ug/L 50.650 101 60-140
Bromomethane ug/L 42.050 84 60-140
Carbon tetrachloride ug/L 55.050 110 60-140
Chlorobenzene ug/L 50.150 100 60-140
Chloroethane ug/L 50.150 100 60-140
Chloroform ug/L 51.150 102 60-140
Chloromethane ug/L 47.050 94 60-140
cis-1,2-Dichloroethene ug/L 50.650 101 60-140
cis-1,3-Dichloropropene ug/L 54.650 109 60-140
Dibromochloromethane ug/L 48.650 97 60-140
Dibromomethane ug/L 50.950 102 60-140
Dichlorodifluoromethane ug/L 46.750 93 60-140
Diisopropyl ether ug/L 51.850 104 60-140
Ethylbenzene ug/L 51.450 103 60-140
Hexachloro-1,3-butadiene ug/L 55.350 111 60-140
Isopropylbenzene (Cumene)ug/L 56.650 113 60-140
m&p-Xylene ug/L 106100 106 60-140
Methyl-tert-butyl ether ug/L 52.950 106 60-140
Methylene Chloride ug/L 53.350 107 60-140
n-Butylbenzene ug/L 55.550 111 60-140
n-Propylbenzene ug/L 54.150 108 60-140
Naphthalene ug/L 56.950 114 60-140
o-Xylene ug/L 54.450 109 60-140
sec-Butylbenzene ug/L 55.150 110 60-140
Styrene ug/L 58.350 117 60-140
tert-Butylbenzene ug/L 55.750 111 60-140
Tetrachloroethene ug/L 50.850 102 60-140
Toluene ug/L 50.450 101 60-140
trans-1,2-Dichloroethene ug/L 49.550 99 60-140
trans-1,3-Dichloropropene ug/L 48.550 97 60-140
Trichloroethene ug/L 50.650 101 60-140
Trichlorofluoromethane ug/L 49.850 100 60-140
Vinyl chloride ug/L 56.250 112 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1209400MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92202992002
1209401
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 115 60-140118 320ND23.0 23.7
1,1,1-Trichloroethane ug/L 20 112 60-140112 120ND22.3 22.5
1,1,2,2-Tetrachloroethane ug/L 20 108 60-140108 020ND21.6 21.6
1,1,2-Trichloroethane ug/L 20 110 60-140112 120ND22.1 22.4
1,1-Dichloroethane ug/L 20 103 60-140101 120ND20.6 20.3
1,1-Dichloroethene ug/L 20 122 60-140121 120ND24.4 24.1
1,1-Dichloropropene ug/L 20 116 60-140114 220ND23.3 22.9
1,2,3-Trichlorobenzene ug/L 20 116 60-140111 420ND23.1 22.2
1,2,3-Trichloropropane ug/L 20 109 60-140112 320ND21.7 22.4
1,2,4-Trichlorobenzene ug/L 20 113 60-140111 120ND22.5 22.3
1,2,4-Trimethylbenzene ug/L 20 119 60-140117 120ND23.7 23.5
1,2-Dibromo-3-chloropropane ug/L 20 112 60-140115 220ND22.4 22.9
1,2-Dibromoethane (EDB)ug/L 20 114 60-140112 220ND22.8 22.4
1,2-Dichlorobenzene ug/L 20 114 60-140111 220ND22.8 22.3
1,2-Dichloroethane ug/L 20 106 60-140104 220ND21.2 20.8
1,2-Dichloropropane ug/L 20 105 60-140104 120ND21.0 20.7
1,3,5-Trimethylbenzene ug/L 20 116 60-140114 120ND23.2 22.9
1,3-Dichlorobenzene ug/L 20 117 60-140113 320ND23.4 22.7
1,3-Dichloropropane ug/L 20 107 60-140107 020ND21.5 21.4
1,4-Dichlorobenzene ug/L 20 110 60-140108 220ND22.0 21.6
2,2-Dichloropropane ug/L 20 104 60-140105 220ND20.7 21.1
2-Chlorotoluene ug/L 20 109 60-140109 120ND21.9 21.7
4-Chlorotoluene ug/L 20 110 60-140108 220ND22.0 21.6
Benzene ug/L 20 110 60-140113 220ND22.0 22.6
Bromobenzene ug/L 20 110 60-140111 020ND22.1 22.1
Bromochloromethane ug/L 20 117 60-140115 220ND23.5 23.0
Bromodichloromethane ug/L 20 114 60-140118 420ND22.7 23.6
Bromoform ug/L 20 98 60-140101 320ND19.5 20.2
Bromomethane ug/L 20 89 60-14091 120ND17.9 18.1
Carbon tetrachloride ug/L 20 125 60-140127 220ND25.0 25.4
Chlorobenzene ug/L 20 106 60-140107 120ND21.2 21.4
Chloroethane ug/L 20 117 60-140126 820ND23.3 25.2
Chloroform ug/L 20 109 60-140112 220ND21.9 22.4
Chloromethane ug/L 20 93 60-14091 320ND18.7 18.2
cis-1,2-Dichloroethene ug/L 20 109 60-140109 020ND21.8 21.9
cis-1,3-Dichloropropene ug/L 20 107 60-140111 420ND21.3 22.2
Dibromochloromethane ug/L 20 97 60-140101 420ND19.4 20.2
Dibromomethane ug/L 20 106 60-140107 120ND21.2 21.4
Dichlorodifluoromethane ug/L 20 134 60-140134 020ND26.8 26.7
Diisopropyl ether ug/L 20 108 60-140110 220ND21.6 21.9
Ethylbenzene ug/L 20 109 60-140111 220ND21.7 22.2
Hexachloro-1,3-butadiene ug/L 20 118 60-140117 120ND23.6 23.4
Isopropylbenzene (Cumene)ug/L 20 119 60-140120 020ND23.8 23.9
m&p-Xylene ug/L 40 113 60-140113 140ND45.4 45.1
Methyl-tert-butyl ether ug/L 20 115 60-140113 120ND23.0 22.7
Methylene Chloride ug/L 20 105 60-140103 220ND21.1 20.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1209400MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92202992002
1209401
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 116 60-140114 120ND23.2 22.9
n-Propylbenzene ug/L 20 115 60-140112 220ND23.0 22.4
Naphthalene ug/L 20 115 60-140112 220ND23.0 22.5
o-Xylene ug/L 20 113 60-140115 220ND22.7 23.0
sec-Butylbenzene ug/L 20 116 60-140115 120ND23.2 23.1
Styrene ug/L 20 118 60-140118 120ND23.7 23.5
tert-Butylbenzene ug/L 20 118 60-140117 120ND23.6 23.4
Tetrachloroethene ug/L 20 112 60-140109 320ND22.4 21.8
Toluene ug/L 20 106 60-140111 420ND21.3 22.2
trans-1,2-Dichloroethene ug/L 20 112 60-140111 020ND22.4 22.3
trans-1,3-Dichloropropene ug/L 20 96 60-14096 120ND19.3 19.2
Trichloroethene ug/L 20 112 60-140112 020ND22.4 22.3
Trichlorofluoromethane ug/L 20 126 60-140124 120ND25.2 24.9
Vinyl chloride ug/L 20 137 60-140138 120ND27.3 27.6
1,2-Dichloroethane-d4 (S)%97 70-13096
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27063
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92202989002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1211907
Associated Lab Samples:92202989002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/03/14 20:29
1,1,1-Trichloroethane ug/L ND 0.50 06/03/14 20:29
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/03/14 20:29
1,1,2-Trichloroethane ug/L ND 0.50 06/03/14 20:29
1,1-Dichloroethane ug/L ND 0.50 06/03/14 20:29
1,1-Dichloroethene ug/L ND 0.50 06/03/14 20:29
1,1-Dichloropropene ug/L ND 0.50 06/03/14 20:29
1,2,3-Trichlorobenzene ug/L ND 2.0 06/03/14 20:29
1,2,3-Trichloropropane ug/L ND 0.50 06/03/14 20:29
1,2,4-Trichlorobenzene ug/L ND 2.0 06/03/14 20:29
1,2,4-Trimethylbenzene ug/L ND 0.50 06/03/14 20:29
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/03/14 20:29
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/03/14 20:29
1,2-Dichlorobenzene ug/L ND 0.50 06/03/14 20:29
1,2-Dichloroethane ug/L ND 0.50 06/03/14 20:29
1,2-Dichloropropane ug/L ND 0.50 06/03/14 20:29
1,3,5-Trimethylbenzene ug/L ND 0.50 06/03/14 20:29
1,3-Dichlorobenzene ug/L ND 0.50 06/03/14 20:29
1,3-Dichloropropane ug/L ND 0.50 06/03/14 20:29
1,4-Dichlorobenzene ug/L ND 0.50 06/03/14 20:29
2,2-Dichloropropane ug/L ND 0.50 06/03/14 20:29
2-Chlorotoluene ug/L ND 0.50 06/03/14 20:29
4-Chlorotoluene ug/L ND 0.50 06/03/14 20:29
Benzene ug/L ND 0.50 06/03/14 20:29
Bromobenzene ug/L ND 0.50 06/03/14 20:29
Bromochloromethane ug/L ND 0.50 06/03/14 20:29
Bromodichloromethane ug/L ND 0.50 06/03/14 20:29
Bromoform ug/L ND 0.50 06/03/14 20:29
Bromomethane ug/L ND 5.0 06/03/14 20:29
Carbon tetrachloride ug/L ND 0.50 06/03/14 20:29
Chlorobenzene ug/L ND 0.50 06/03/14 20:29
Chloroethane ug/L ND 1.0 06/03/14 20:29
Chloroform ug/L ND 0.50 06/03/14 20:29
Chloromethane ug/L ND 1.0 06/03/14 20:29
cis-1,2-Dichloroethene ug/L ND 0.50 06/03/14 20:29
cis-1,3-Dichloropropene ug/L ND 0.50 06/03/14 20:29
Dibromochloromethane ug/L ND 0.50 06/03/14 20:29
Dibromomethane ug/L ND 0.50 06/03/14 20:29
Dichlorodifluoromethane ug/L ND 0.50 06/03/14 20:29
Diisopropyl ether ug/L ND 0.50 06/03/14 20:29
Ethylbenzene ug/L ND 0.50 06/03/14 20:29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1211907
Associated Lab Samples:92202989002
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 06/03/14 20:29
Isopropylbenzene (Cumene)ug/L ND 0.50 06/03/14 20:29
m&p-Xylene ug/L ND 1.0 06/03/14 20:29
Methyl-tert-butyl ether ug/L ND 0.50 06/03/14 20:29
Methylene Chloride ug/L ND 2.0 06/03/14 20:29
n-Butylbenzene ug/L ND 0.50 06/03/14 20:29
n-Propylbenzene ug/L ND 0.50 06/03/14 20:29
Naphthalene ug/L ND 2.0 06/03/14 20:29
o-Xylene ug/L ND 0.50 06/03/14 20:29
sec-Butylbenzene ug/L ND 0.50 06/03/14 20:29
Styrene ug/L ND 0.50 06/03/14 20:29
tert-Butylbenzene ug/L ND 0.50 06/03/14 20:29
Tetrachloroethene ug/L ND 0.50 06/03/14 20:29
Toluene ug/L ND 0.50 06/03/14 20:29
trans-1,2-Dichloroethene ug/L ND 0.50 06/03/14 20:29
trans-1,3-Dichloropropene ug/L ND 0.50 06/03/14 20:29
Trichloroethene ug/L ND 0.50 06/03/14 20:29
Trichlorofluoromethane ug/L ND 1.0 06/03/14 20:29
Vinyl chloride ug/L ND 1.0 06/03/14 20:29
1,2-Dichloroethane-d4 (S)%95 70-130 06/03/14 20:29
4-Bromofluorobenzene (S)%94 70-130 06/03/14 20:29
Toluene-d8 (S)%100 70-130 06/03/14 20:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1211908LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.750 99 60-140
1,1,1-Trichloroethane ug/L 46.150 92 60-140
1,1,2,2-Tetrachloroethane ug/L 50.350 101 60-140
1,1,2-Trichloroethane ug/L 51.750 103 60-140
1,1-Dichloroethane ug/L 46.050 92 60-140
1,1-Dichloroethene ug/L 46.250 92 60-140
1,1-Dichloropropene ug/L 49.750 99 60-140
1,2,3-Trichlorobenzene ug/L 50.250 100 60-140
1,2,3-Trichloropropane ug/L 47.950 96 60-140
1,2,4-Trichlorobenzene ug/L 49.450 99 60-140
1,2,4-Trimethylbenzene ug/L 50.150 100 60-140
1,2-Dibromo-3-chloropropane ug/L 48.350 97 60-140
1,2-Dibromoethane (EDB)ug/L 51.150 102 60-140
1,2-Dichlorobenzene ug/L 49.550 99 60-140
1,2-Dichloroethane ug/L 44.250 88 60-140
1,2-Dichloropropane ug/L 47.550 95 60-140
1,3,5-Trimethylbenzene ug/L 49.550 99 60-140
1,3-Dichlorobenzene ug/L 49.450 99 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1211908LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 49.850 100 60-140
1,4-Dichlorobenzene ug/L 47.950 96 60-140
2,2-Dichloropropane ug/L 46.450 93 60-140
2-Chlorotoluene ug/L 49.450 99 60-140
4-Chlorotoluene ug/L 47.050 94 60-140
Benzene ug/L 51.550 103 60-140
Bromobenzene ug/L 49.250 98 60-140
Bromochloromethane ug/L 49.350 99 60-140
Bromodichloromethane ug/L 49.150 98 60-140
Bromoform ug/L 45.450 91 60-140
Bromomethane ug/L 60.450 121 60-140
Carbon tetrachloride ug/L 48.850 98 60-140
Chlorobenzene ug/L 48.050 96 60-140
Chloroethane ug/L 49.750 99 60-140
Chloroform ug/L 48.250 96 60-140
Chloromethane ug/L 56.250 112 60-140
cis-1,2-Dichloroethene ug/L 49.250 98 60-140
cis-1,3-Dichloropropene ug/L 52.950 106 60-140
Dibromochloromethane ug/L 50.650 101 60-140
Dibromomethane ug/L 50.450 101 60-140
Dichlorodifluoromethane ug/L 46.850 94 60-140
Diisopropyl ether ug/L 50.750 101 60-140
Ethylbenzene ug/L 48.350 97 60-140
Hexachloro-1,3-butadiene ug/L 43.750 87 60-140
Isopropylbenzene (Cumene)ug/L 49.550 99 60-140
m&p-Xylene ug/L 99.5100 99 60-140
Methyl-tert-butyl ether ug/L 51.150 102 60-140
Methylene Chloride ug/L 48.350 97 60-140
n-Butylbenzene ug/L 48.950 98 60-140
n-Propylbenzene ug/L 48.850 98 60-140
Naphthalene ug/L 52.450 105 60-140
o-Xylene ug/L 49.250 98 60-140
sec-Butylbenzene ug/L 47.950 96 60-140
Styrene ug/L 53.950 108 60-140
tert-Butylbenzene ug/L 48.650 97 60-140
Tetrachloroethene ug/L 47.450 95 60-140
Toluene ug/L 48.550 97 60-140
trans-1,2-Dichloroethene ug/L 46.750 93 60-140
trans-1,3-Dichloropropene ug/L 52.350 105 60-140
Trichloroethene ug/L 48.450 97 60-140
Trichlorofluoromethane ug/L 44.450 89 60-140
Vinyl chloride ug/L 59.150 118 60-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1211909MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203232028
1211910
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 112 60-14096 1620ND22.5 19.2
1,1,1-Trichloroethane ug/L 20 114 60-14098 1620ND22.9 19.5
1,1,2,2-Tetrachloroethane ug/L 20 111 60-14091 1920ND22.1 18.2
1,1,2-Trichloroethane ug/L 20 115 60-14098 1620ND23.1 19.6
1,1-Dichloroethane ug/L 20 110 60-14094 1620ND22.0 18.8
1,1-Dichloroethene ug/L 20 119 60-140102 1520ND23.8 20.4
1,1-Dichloropropene ug/L 20 122 60-140107 1320ND24.5 21.5
1,2,3-Trichlorobenzene ug/L 20 106 60-14095 1220ND21.2 18.9
1,2,3-Trichloropropane ug/L 20 110 60-14092 1820ND22.0 18.4
1,2,4-Trichlorobenzene ug/L 20 107 60-14095 1120ND21.3 19.1
1,2,4-Trimethylbenzene ug/L 20 118 60-140105 1220ND23.7 21.0
1,2-Dibromo-3-chloropropane ug/L 20 102 60-14083 2120ND20.5 16.7
1,2-Dibromoethane (EDB)ug/L 20 115 60-14097 1720ND23.0 19.3
1,2-Dichlorobenzene ug/L 20 113 60-14098 1420ND22.5 19.5
1,2-Dichloroethane ug/L 20 105 60-14087 1920ND21.1 17.3
1,2-Dichloropropane ug/L 20 110 60-14096 1420ND22.1 19.2
1,3,5-Trimethylbenzene ug/L 20 118 60-140104 1320ND23.6 20.7
1,3-Dichlorobenzene ug/L 20 113 60-140100 1120ND22.5 20.1
1,3-Dichloropropane ug/L 20 115 60-14096 1820ND22.9 19.1
1,4-Dichlorobenzene ug/L 20 109 60-14096 1320ND21.9 19.3
2,2-Dichloropropane ug/L 20 121 60-140102 1720ND24.2 20.4
2-Chlorotoluene ug/L 20 115 60-14098 1620ND23.0 19.7
4-Chlorotoluene ug/L 20 108 60-14096 1220ND21.7 19.2
Benzene ug/L 20 121 60-140104 1520ND24.1 20.8
Bromobenzene ug/L 20 115 60-140100 1420ND23.0 20.0
Bromochloromethane ug/L 20 120 60-140104 1520ND24.1 20.8
Bromodichloromethane ug/L 20 117 60-14098 15203.4 26.8 23.0
Bromoform ug/L 20 96 60-14083 1520ND19.3 16.6
Bromomethane ug/L 20 112 60-14098 1320ND22.5 19.7
Carbon tetrachloride ug/L 20 119 60-140103 1420ND23.8 20.7
Chlorobenzene ug/L 20 113 60-14098 1420ND22.6 19.7
Chloroethane ug/L 20 118 60-140107 1020ND23.7 21.4
Chloroform ug/L 20 119 60-140100 14205.6 29.5 25.7
Chloromethane ug/L 20 102 60-14086 1720ND20.5 17.2
cis-1,2-Dichloroethene ug/L 20 116 60-14099 1520ND23.1 19.9
cis-1,3-Dichloropropene ug/L 20 113 60-14098 1520ND22.7 19.6
Dibromochloromethane ug/L 20 113 60-14094 17201.9 24.5 20.7
Dibromomethane ug/L 20 112 60-14095 1720ND22.3 18.9
Dichlorodifluoromethane ug/L 20 119 60-140105 1320ND23.8 20.9
Diisopropyl ether ug/L 20 117 60-140100 1620ND23.4 19.9
Ethylbenzene ug/L 20 115 60-140100 1520ND23.1 19.9
Hexachloro-1,3-butadiene ug/L 20 109 60-14094 1520ND21.7 18.8
Isopropylbenzene (Cumene)ug/L 20 118 60-140104 1220ND23.5 20.8
m&p-Xylene ug/L 40 119 60-140104 1340ND47.6 41.7
Methyl-tert-butyl ether ug/L 20 116 60-14096 1820ND23.1 19.3
Methylene Chloride ug/L 20 106 60-14090 1620ND21.1 18.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1211909MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203232028
1211910
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 119 60-140105 1220ND23.7 21.0
n-Propylbenzene ug/L 20 118 60-140105 1220ND23.7 21.0
Naphthalene ug/L 20 110 60-14095 1420ND21.9 19.1
o-Xylene ug/L 20 113 60-14099 1320ND22.6 19.9
sec-Butylbenzene ug/L 20 117 60-140104 1220ND23.5 20.7
Styrene ug/L 20 123 60-140106 1520ND24.6 21.2
tert-Butylbenzene ug/L 20 118 60-140104 1220ND23.5 20.8
Tetrachloroethene ug/L 20 115 60-140101 1320ND23.0 20.2
Toluene ug/L 20 112 60-14098 1320ND22.7 19.8
trans-1,2-Dichloroethene ug/L 20 117 60-140102 1320ND23.4 20.5
trans-1,3-Dichloropropene ug/L 20 111 60-14094 1720ND22.2 18.8
Trichloroethene ug/L 20 113 60-14099 1320ND22.7 19.8
Trichlorofluoromethane ug/L 20 125 60-140105 1720ND25.0 21.1
Vinyl chloride ug/L M02014660-140126 1520ND29.3 25.3
1,2-Dichloroethane-d4 (S)%97 70-13095
4-Bromofluorobenzene (S)%101 70-13099
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92202989
Howard Bowman TF#14151
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92202989001 MSV/27001D1SM 6200B
92202989002 MSV/27063D3SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 03:42 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 21
Page 20 of 21
Page 21 of 21