RA-613_3831_CA_MRP_20190621

Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

June 21, 2019

Mr. Mark Petermann
NCDEQ, Division of Waste Management, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Reference:
Comprehensive Site Assessment – Mt. Harmony Grocery
1818 Mt. Harmony Church Road
Rougemont, Person County, North Carolina
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

Dear Mr. Petermann:

As authorized by your acceptance of ECS Southeast, LLP (ECS) Task Authorization Request No.
(TAR No. #5) dated March 19, 2019, ECS has completed this Comprehensive Site Assessment
Report for the above referenced site. Included in this report is a description of the field activities,
the results obtained, and our conclusions and recommendations.

ECS appreciates the opportunity to provide our environmental consulting services to you on this
project. If you have any questions concerning this report or this project, please contact us.

Sincerely,

ECS SOUTHEAST, LLP

Samantha M. Szakasits, G.I.T. Matthew Gillis
Assistant Staff Project Manager Sr. Environmental Project Manager
[e-mail] [e-mail]
[phone] [phone]

Matthew H. McDuffie, P.G.
Principal Geologist
NC License No. 2269
[e-mail]
[phone]

Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

SITE INFORMATION

UST Incident No.: 3831
Site Rank: High (H385D)
Land Use Category: Commercial

Site Name and Location: Mt. Harmony Grocery
1818 Mt. Harmony Church Road
Rougemont, Person County, North Carolina

Latitude and Longitude: 36.317431° North, -78.863205°West

Contacts

Property Owner: Billy & Gwendolyn Barber
90 Fletcher Ridge Road
Timberlake, North Carolina 27583
[phone]

Consultant: ECS Southeast, LLP
9001 Glenwood Avenue
Raleigh, North Carolina 27617
[phone]
Attn: Matthew Gillis

Laboratory: Con-Test Analytical Laboratory
39 Spruce Street
East Long Meadow, Massachusetts 01028
[phone]
NC Certification No. 12

Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

EXECUTIVE SUMMARY

The subject site is known as Mt. Harmony Grocery and is located at 1818 Mt. Harmony Church
Road in Rougemont, Person County, North Carolina. The subject site is further identified by
Person County Geographic Information Systems (GIS) Parcel Identification Number (PIN)
0943-00-04-1612.000.

INCIDENT RISK EVALUATION SUMMARY
SOURCE INFORMATION
Source & Nature of Release 2 x 1,000-gal. USTs – Contamination identified in nearby WSWs
Each Known Source Removed? Known USTs/product lines removed in 1990
Additional Sources Likely Present? GPR survey indicated a negative anomaly that appeared to be a mass of
buried metal such as a waste-oil UST located besides the building.
Each Known Source Assessed? No – ECS proposes to assess near suspected waste-oil UST
FREE PRODUCT
Free Product Present? No
SITE SOIL CONDITIONS
TPH Soil Data Available? Yes (1990) – TPH-GRO ranging from 5.8 to 1,780 mg/kg
Risk-Based Soil Data Available? Yes (2017) – Petroleum hydrocarbons were detected in one soil sample collected
near the pump island at concentrations above the Soil-to-Groundwater MSCC.
Extent of Soil Impact
Delineated? No
SITE GROUNDWATER CONDITIONS
Average Depth to Groundwater? 20.07 feet btoc (ranging from approx. 16 to 37 feet btoc.) based
on April 17 and May 3, 2019 measurements
Contaminants Present Above NC2LGWQS? Yes
Contaminants Present Above GCLs? Yes (including benzene, EDB, and MTBE)
Groundwater Plume Delineated? Yes
Groundwater Plume Migrated Off-Site? Yes – MTBE detected in WSWs & MWs located >500 feet off-site
Contaminant Level Trend Generally decreasing
RECEPTOR INFORMATION
Date of Most Current Receptor Survey 2016
Potable Water Supply Wells within 1,000’? Yes – nine active, potable water supply wells
Municipal Water Available to Each Property within
1,000’?
No – municipal water available over 3 miles away
Non-Potable Wells within 250’? Two inactive water supply wells.
Site within Wellhead Protection Area? No
Surface Water Bodies within 500’? No
REMEDIAL ACTIVITIES
What active remedial activities have been conducted? O-Sox Deployment & maintenance
Are active remedial activities working? ECS proposes additional assessment to determine
efficiency
VAPOR INTRUSION
Dissolved Phase Contaminants exceeding Groundwater
Screening Levels for Vapors present within 5’ of Ground Surface?
No
Occupied Structures on the Site? Vacant store & Occupied single-family residence
Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

On April 17-18, 2019, ECS collected a field blank and groundwater samples from monitoring
wells MW-1 through MW-12, and DW-1. ECS also collected groundwater samples from active
water supply wells PW-3R, PW-4B, WSW-2, and WSW-3. On May 3, 2019, ECS contracted
with Quantex to advance two soil borings to collect one soil sample from each boring at depths
ranging from 5 to 10 ft. bgs for risk-based analysis. The borings were located downgradient of
the negative anomaly from a geophysical survey conducted in September 2018. The anomaly
was suspected to be a waste-oil underground storage tank (UST), located adjacent to the
building, in an effort to determine if there potential soil contamination related to the anomaly on
the subject site. Quantex also installed two Type II groundwater monitoring wells: MW-13 and
MW-14. Monitoring well MW-13 was installed near the northeast corner of Latta property and
monitoring well MW-14 was installed near the southeast corner of the Latta property. Following
installation, on May 3, 2019 ECS collected groundwater samples from the two newly installed
monitoring wells (MW-13 and MW-14). On May 9, 2019, ECS horizontally and vertically located
surveyed the two newly installed monitoring wells, relative to the existing well network and
common site benchmark.

Based on the results and conclusions of this Comprehensive Site Assessment and a discussion
with Mr. Mark Petermann of NCDEQ, ECS and NCDEQ have agreed upon the following
recommendation:
 ECS and NCDEQ will have a meeting to discuss the hydrogeology at the site for the
development and approach for future environmental assessments. Topics to discuss but not
limited to, include: developing cross sections, obtaining water supply well depth information,
installation of piezometers, and/or conducting Hydraulic Profiling Tool (HPT) drilling
activities at the site to determine fractures within the bedrock beneath the site.
 Potentially excavate and remove the anomaly indicative of a UST along the southern side of
the site building.
 Potentially excavate and remove the concrete pad, product piping, and residual soils where
the dispensers were formerly located.

Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

TABLE OF CONTENTS
EXECUTIVE SUMMARY................................................................................................. 4
1.0 SITE HISTORY ......................................................................................................... 7
2.0 SITE GEOLOGY AND HYDROGEOLOGY............................................................... 9
3.0 RECEPTOR INFORMATION .................................................................................. 11
4.0 FIELD ACTIVITIES ................................................................................................. 12
5.0 LABORATORY ANALYTICAL RESULTS ............................................................... 14
6.0 CONCLUSIONS ...................................................................................................... 15
7.0 RECOMMENDATIONS ........................................................................................... 16

FIGURES
Figure 1 Site Location Map
Figure 2 Site Aerial Map
Figure 3 Water Supply Well Location Map
Figure 4 Adjacent Properties Map
Figure 5 2019 Soil Boring Location Map
Figure 6 Monitoring Well Location Map
Figure 7 Groundwater Elevation Map
Figure 8 Monitoring Well Groundwater Concentration Map
Figure 9 Water Supply Well Groundwater Concentration Map
Figure 10 Benzene Isoconcentration Map

TABLES

Table 1 UST Information
Table 2 Summary of Historical Soil Sample Analytical Results
Table 3 Water Supply Well Survey Data
Table 4 Adjacent Properties
Table 5 Monitoring Well Construction and Groundwater Elevation Details
Table 6 Summary of Current 2019 Soil Sample Analytical Results
Table 7 Summary of Current Groundwater Analytical Results
Table 8 Summary of Current & Historical Groundwater Analytical Results

APPENDICIES

Appendix A ECS Personnel Field Notes and Sampling Sheets
Appendix B Site Photographs
Appendix C Access Agreement
Appendix D Monitoring Well Construction Forms
Appendix E Laboratory Analytical Data Sheets and Chain of Custody (COC) Records

Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

1.0 SITE HISTORY

The subject site is known as Mt. Harmony Grocery and is located at 1818 Mt. Harmony Church
Road in Rougemont, Person County, North Carolina (Figures 1 and 2). According to information
provided to ECS by the North Carolina Department of Environment Quality (NCDEQ), the site
formerly operated as a convenience store and gasoline station, known as Little Huff Oil Company.
Reportedly, the station operated two 1,000-gallon gasoline USTs, which were removed in March
1990 (Table 1).

In March of 1990, Groundwater Management Associates Inc. (GMA) reportedly conducted soil
and groundwater sampling at the site. GMA collected ten soil samples from the walls and floor
of the excavation after the removal of the two USTs. Composite soil samples from the walls (S1
through S5) were taken from depths of three to nine feet below ground surface (ft. bgs). Grab
soil samples from the bottom of the excavation (S6 through S10) ranged from six to nine feet
bgs. Laboratory analysis reported total petroleum hydrocarbons gasoline range organics (TPH-
GRO) above the current action level of 50 mg/kg in soil samples S1 and S4 through S10.
Laboratory analysis also reported TPH-GRO above the laboratory reporting limit but below the
action level of 50 mg/kg in soil samples S2 and S3 (Table 2). Additionally, GMA collected three
groundwater samples from water supply wells PW-2 through PW-4. Laboratory analysis
reported benzene, toluene, and total xylenes at concentrations above their respective North
Carolina 2L Groundwater Quality Standard (NC2LGWQS) but below their respective Gross
Contaminant Level (GCL) in groundwater sample collected from water supply well PW-2.
Laboratory analysis reported xylenes above the laboratory reporting limits but below its
NC2LGWQS in the groundwater sample collected from PW-3, which reportedly supplied water
to the former store. According to a figure, PW-3 appeared to be located to the south-southwest
behind the building on the subject site. Since then, water supply well PW-3 has been replaced
by the current active water supply well PW-3R located near the subject sites western property
boundary.

In September of 2005, GeoLogix conducted a Phase I and II Limited Site Assessment (LSA).
During the Phase I portion of the LSA, Geologix installed a monitoring well (MW-UST) within the
former location of the USTs. Soil samples were collected at depths of eleven and twenty-one ft
bgs. Laboratory analysis reported benzene and methyl-tert bulyl ether (MTBE) at concentrations
above their respective GCLs in the groundwater sample collected from MW-UST. Based on the
results of the Phase I LSA, Geologix determined a Phase II LSA was required. During the
Phase II LSA, one deep/vertical extent well (DW-1) and three shallow monitoring wells (MW-1
through MW-3), were constructed. Geologix collected groundwater samples from monitoring
well DW-1 and MW-1 through MW-3. Laboratory analysis reported MTBE at a concentration
above its NC2LGWQS but below its GCL in the groundwater sample collected from monitoring
well DW-1. Laboratory analysis reported benzene above its GCL in the groundwater sample
collected from monitoring well MW-1 through MW-3. Laboratory analysis reported several
additional analytes above their respective NC2LGWQSs but below their respective GCLs in the
groundwater sample collected from monitoring wells MW-1 through MW-3. Based on the levels
of benzene and MTBE in the groundwater from monitoring wells MW-1 through MW-3, Geologix
stated it appears the highest level of petroleum contamination is directed to the southeast and
may be an indicator of groundwater flow.

Geologix identified three water supply wells adjacent to the subject site. Geologix stated
laboratory analysis of the water supply well (PW-2) located on the Latta property (adjacent to
Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

the south) reported several targeted analytes in the groundwater sample. Additionally, xylenes
were reported in the currently inactive water supply well (PW-3) located to the south-southwest
of the subject site, replaced by the current active water supply well PW-3R located near the
subject sites western property boundary. Little Huff Oil Company agreed to construct a new
potable water supply well for the Latta residence located south of the subject site (WSW-3).
Reportedly, a new well, replacing its predecessor, was also constructed for the residence
located on the subject property north of the source area (PW-1). Water from that well was also
shared by the grocery store. Geologix stated a Comprehensive Site Assessment (CSA) may be
required.

On October 10, 2016, ECS collected groundwater samples from monitoring wells MW-1
through MW-4 and DW-1. The resident residing on the subject site (1818 Mt. Harmony Church
Road) was not present at at the time of sampling and ECS did not observe an exterior spigot on
the house; therefore, ECS did not sample water supply well PW-1. ECS observed water supply
well structures presumably containing PW-2 and PW-4. ECS did not receive written permission
to collect groundwater samples from these wells.

Additionally ECS performed a receptor survey and identified eleven potable water supply wells
located within 1,000 feet of the subject site. ECS contacted the City of Roxboro Public Services
to inquire if municipal water is available for the subject site and surrounding area. According to
the City of Roxboro Public Services, municipal water is not connected to the subject site and
not available to the surrounding area.

Laboratory analysis from the October 2016 sampling event reported benzene at a concentration
above its GCL in the groundwater sample collected from monitoring well MW-2. Additionally,
laboratory analysis reported benzene and MTBE at concentrations above their respective GCLs in
the groundwater sample collected from monitoring well MW-3. Laboratory analysis reported
methyl butyl ketone at a concentration above its NC2LGWQS but below its GCL in the
groundwater sample collected from monitoring well DW-1.

On August 10, 2017, ECS collected a field blank and groundwater samples from monitoring wells
MW-UST, MW-1 through MW-3, DW-1, and water supply well WSW-3. However, for
consistency’s sake, ECS will hereby refer to the monitoring well previously named MW-UST as
MW-1; MW-1 as MW-2; MW-2 as MW-3; and MW-3 as MW-4 after observing monitoring well
identification cards observed during site reconnaissance and a review of the previous September
2005 Phase I & II Limited Site Assessment (LSA). Quantex, Inc. (Quantex) installed monitoring
wells MW-5 and MW-6 on the adjacent property occupied by Mt. Tirzah Park. ECS also collected
soil samples for risk-based analysis along the sidewalls of the former UST location and dispenser
island to determine the extent of contaminated soils on the subject site. Petroleum hydrocarbons
were detected in one of the soil samples collected adjacent to the former pump island at
concentrations above the Soil-to-Groundwater MSCCs (Table 2).

On August 11, 2017, ECS collected groundwater samples from water supply well PW-4A (Ball
Park) ((formerly identified as WSW-4)) and PW-4B (Fire Department) ((formerly identified as PW-
4). Based on conversations with the NCDEQ and Mr. Ray Foushee of Person County, it was
determined that the Mt. Tirzah Park and the Mt. Moriah Fire Department share water supply well
PW-4B and water supply well PW- 4A is not active. ECS collected a groundwater sample from
monitoring well MW-5 and attempted to sample monitoring well MW-6 but it was dry at the time.
Also, ECS spoke with the rental tenant of the single-family residence associated with the subject
Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

site. She informed ECS that the water supply well (PW-1) is inactive. She indicated that she is not
connected to municipal water and does not currently have water supplied to her home. Before site
departure, ECS horizontally and vertically located surveyed the two newly installed monitoring
wells, relative to the existing well network and common site benchmark.

On August 21, 2017, ECS returned to the site and collected a groundwater sample from
monitoring well MW-6. On August 24, 2017, ECS collected an additional groundwater sample
from water supply well PW-4A.

The September 26, 2017 dated North Carolina DWM Health Risk Evaluation and use
recommendations for the concentrations of 1,2-dichloroethane and MTBE found in the
groundwater samples collected on August 11, 2017 at the Mt. Moriah Volunteer Fire Department
and Mt. Tirzah Park found that:
 “This water is not recommended for any residential use at this time. This water should pose no
significant health risk for its current use, which is to flush toilets and for hand washing at a ball
field.”

Based on the results of the October 2017 groundwater monitoring report, ECS noted that the
contaminant plume had not been delineated to the west, east, south or vertically.

On November 21, 2017, ECS collected a field blank and a groundwater sample from water
supply well WSW-2 after obtaining a signed water supply well permission letter. The laboratory
did not report targeted analytes at concentrations above the laboratory reporting limits in the
groundwater sample collected from water supply well WSW-2 or the field blank.

On January 5, 2018, ECS collected a field blank and groundwater samples from monitoring
wells MW-1 through MW-4, and DW-1. ECS attempted to collect groundwater samples from
monitoring wells MW-5 and MW-6; however, these wells were dry at the time. ECS deployed O-
Sox in monitoring wells MW-1, MW-3, and MW-4. On January 5, 2018, Quantex, on behalf of
ECS, installed one Type II groundwater monitoring well (MW-7) northwest of the former store at
the subject site.

On January 8, 2018, ECS collected a groundwater sample from water supply well PW-3R after
the rental tenant identified the location of the well house in the northwestern portion of the
subject site. She informed ECS that water supply well PW-3R supplies potable water to the
single family residence associated with the subject site. ECS collected a groundwater sample
from monitoring well MW-7 after development and purging. Quantex installed Type II
groundwater monitoring wells MW-8 through MW-10 on the adjacent Mt. Tirzah Park property.
Laboratory analysis reported multiple NC2LGWQS and/or GCL violations.

On September 13, 2018, KCI Technologies, Inc. conducted a geophysical survey at the site
utilizing ground penetrating radar (GPR) to investigate the soil disturbances and an earthen
depression previously documented in the rear of the former store. The GPR survey indicated a
negative anomaly that appeared to be a mass of buried metal such as a waste-oil UST located
besides the building.

On September 18-19, 2018, ECS contracted with Quantex, to install two Type II groundwater
monitoring wells: MW-11 and MW-12. Monitoring well MW-12 was installed north of monitoring
well MW-7 and the former store at the subject site. Monitoring well MW-11 was installed west of
Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

monitoring well MW-3 beside the single-family residence. ECS also collected field blank and a
groundwater sample from active water supply wells PW-3R, PW-4B, WSW-2, and WSW-3 and
monitoring wells MW-1 through MW-10, and DW-1.

On October 1, 2018, ECS deployed O-Sox in monitoring wells DW-1, MW-1, MW-3, MW-4,
MW-5, and MW-7 and collected groundwater samples from newly installed monitoring wells
MW-11 and MW-12. ECS horizontally and vertically located surveyed the two newly installed
monitoring wells, relative to the existing well network and common site benchmark.

The results of the September and October 2018 activities were presented in the February 2019
Groundwater Monitoring Report prepared for the NCDEQ. Based on the results and
conclusions of the report, ECS had the following recommendations:
 Coordinate with Mr. Billy Barber, Mrs. Kristi Williams (Latta), and Mrs. Bobbie Latta to
receive access to install two off-site monitoring wells on the southern properties owned by
the aforementioned grandmother and granddaughter.
 Install two additional monitoring wells on the adjoining, southern Latta/Williams properties
then sample and survey the new monitoring wells to the existing datum.
 Collect a soil sample from down-gradient of the anomaly identified during the GPR
assessment.
 Installing Enviro-Bac or similar devices in monitoring wells MW-1, MW-3, MW-4, MW-7 and
MW-11 and then resampling monitoring wells DW-1, MW-1 through MW-12 within 60 days
to determine efficacy.
 Collect groundwater samples from water supply wells WSW-2, PW-3R, WSW-3 and PW-4B
and attempt to obtain permission for a second time to collect groundwater samples from
water supply wells WSW-5, WSW-6, WSW-7, and WSW-8.

2.0 SITE GEOLOGY AND HYDROGEOLOGY

As determined from the USGS Topographic Maps, Moriah and Timberlake, North Carolina
Quadrangles dated 2016 (Figure 1), the site is at an approximate elevation of 655 feet above
mean sea level. According to the topographic map, the site is located on the northwestern edge
of a topographic high point. Surface runoff from the site appears to flow radially from the site.

The subject site is situated in the Piedmont Physiographic Province. The soils encountered in
this area are the residual product of in-place chemical weathering of rock presently underlying
the site and/or historic depositional events. In general, shallow unconfined groundwater
movement within the overlying soils is controlled largely by topographic gradients. However, as
the groundwater percolates downward, it becomes controlled by the subsurface geologic
conditions. Thus, the direction of groundwater movement in the deeper aquifers may not be
consistent with the reflecting topography. The elevation of the shallow water table is transient
and can vary with seasonal fluctuations in precipitation.

Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

3.0 RECEPTOR INFORMATION

3.1 Water Supply Wells

On October 10, 2016, ECS performed a walking and vehicular reconnaissance of properties
within 1,000 feet of the site. Water supply wells were observed at residences along Mt.
Harmony Church Road within 1,000 feet of the site. ECS contacted the City of Roxboro Public
Services and according to municipal records, municipal water supply wells are not located
within 1,000 feet of the subject site. Water supply well questionnaires were mailed via United
States Postal Service (USPS) to the property owners located within 500 feet of the source area.

On September 26, 2016, ECS received a returned water supply well letter from Mr. Billy Barber
(1818 Mt. Harmony Church Road; subject site) stating the property contains an active water
supply well (PW-1) and is not connected to municipal water. On September 29, 2016, ECS
received a returned water supply well letter from Mr. Pete Thomas (1655 Mt. Harmony Church
Road; Mount Harmony Baptist Church) stating that the property contains an active water supply
well (WSW-1) that supplies drinking water to 250 people. Water supply well WSW-1 is located
745 feet to the north-northeast. On December 13, 2016, ECS received a returned water supply
well letter from Mr. Ray Foushee, the General Services Director of the Person County
Government, associated with the Mt. Tirzah Ball Park. He indicated that the Concessions Stand
near the baseball diamond has an active water supply well (PW-4A (formerly identified as
WSW-4)) that supplies drinking water and restroom fixtures to the public.

On August 10 and 11, 2017, ECS received a returned water supply letter from Mrs. Kristi Latta
(1850 Mt. Harmony Church Road; adjoining southern residence) stating the property contains
one active, potable water supply well (WSW-3) that supplies water to her home. Mrs. Kristi
Latta informed ECS that water supply well PW-2 is inactive but the pump house dispenses
water from water supply well WSW-3. ECS received Ms. Bobbie Latta’s (131 Peed Road;
adjoining vacant agricultural land) permission to sample water supply well WSW-3 on August
10, 2017. Also, on August 10 and 11, 2017, ECS spoke with the rental tenant of the single-
family residence associated with the subject site. She informed ECS that the water supply well
(PW-1) is inactive. She indicated that she is not connected to municipal water and does not
currently have water supplied to her home.

On August 24, 2017, ECS spoke with Mr. Foushee on the phone and concluded that the Mt.
Tirzah Ball Park and the Mt. Moriah Volunteer Fire Department property share active water
supply well (PW-4B) (formerly identified as PW-4) and that water supply well PW-4A (Ballpark)
is not active. He indicated that the Fire Department uses their water supply well for cleaning,
special events, restroom fixtures, and fundraising cook-outs. He noted that they do not fill their
fire-trucks with groundwater from the water supply well.

On November 21, 2017, ECS collected a groundwater sample from active, potable water supply
well WSW-2 (Bradsher Well) after obtaining a signed water supply well permission letter.

On January 8, 2018, ECS collected a groundwater sample from water supply well PW-3R after
the rental tenant identified the location of the well house in the northwestern portion of the
subject site. She informed ECS that water supply well PW-3R supplies potable water to the
single family residence associated with the subject site where she resides.

Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

On September 18, 2018, ECS collected a groundwater sample from active water supply wells
PW-3R, PW-4B, WSW-2, and WSW-3. ECS was informed by the current tenants of 1850 Mt.
Harmony Church Road that the former tenants had moved but the property owner, Ms. Bobbie
Latta, arrived on-site to grant ECS permission to sample the active, potable water supply well
WSW-3, which is located on her property.

The names and addresses of the property owners with water supply wells located within 1,000
feet of the site are included in Table 3 and shown on Figure 3. The names and addresses of the
adjacent property owners are included in Table 4 and shown on Figure 4.

3.2 Public Water Supplies

On November 6, 2018, ECS contacted the City of Roxboro Public Services and was told that
municipal water is not connected to the subject site and not available to the surrounding area. The
closest waterline that could be run to the area is reportedly located approximately 3.5 miles to
the south of the subject site along Helena-Moriah Road.

4.0 FIELD ACTIVITIES

4.1 Soil Borings and Soil Sampling

On May 3, 2019, ECS contracted with Quantex to advance two soil borings to collect two soil
samples (one from each boring) at depths ranging from 5 to 10 ft. bgs for risk-based analysis.
The borings were located adjacent to the anomaly indicative of the UST that was previously
identified during a geophysical survey (Figure 5). The anomaly was suspected to be a waste-oil
UST, and was identified beside the site building. The borings and soil samples were collected in
an effort to assess the soils for potential contamination related to the anomaly. ECS personnel
field notes, boring logs, and monitoring well sampling sheets completed during field activities
are included in Appendix A. Site photographs are included in Appendix B.

The soil samples were placed into laboratory provided sample containers, labeled with ECS
project number, sample identification, sample date and time, and requested analytical analysis.
The containers were then placed into protective packaging material and placed into a cooler
with ice to maintain the samples at approximately 4C. The soil samples were submitted to
Con-Test Laboratories (Con-Test) located in Longmeadow, Massachusetts (MA) for chemical
analysis for volatile organic compounds (VOCs) using EPA Method 8260, semi-volatile organic
compounds (SVOCs) using EPA Method 8270, volatile petroleum hydrocarbons (VPH) and
extractable petroleum hydrocarbons (EPH) using the Massachusetts Department of
Environmental Protection (MADEP) Methods. ECS maintained proper COC procedures
throughout the sample collection and transportation process.

4.2 Monitoring Well Installation

On May 3, 2019, a North Carolina licensed driller with Quantex, on behalf of ECS, installed two
Type II groundwater monitoring wells: MW-13 and MW-14. Prior to the drilling activities, ECS
obtained an access agreement to install the wells on Ms. Kristi Latta’s property, which is south
the subject site. The signed access agreement in included in Appendix C. Monitoring well MW-
13 was installed near the northeast corner of Latta property and monitoring well MW-14 was
Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

installed near the southeast corner of the Latta property. Monitoring well construction details and
groundwater level data is summarized in Table 5 and the locations of site monitoring wells are
shown on Figure 6.

The two monitoring wells were installed using hollow stem auger until refusal was met, then air-
rotary drilling. Drilling with hollow stem augers involves rotating a continuous stem of augers
into the ground. As drilling advances, the soil cuttings are removed by the rotating auger. Prior
to advancing the boring, the down hole equipment and drill rig were decontaminated using high
pressure steam cleaner and municipal water. ECS noted potential petroleum-like odors
emanating from the bore hole of monitoring well MW-13.

The two borings for the monitoring wells were conducted by advancing decontaminated hollow
stem augers to refusal, then continuing by using air rotary drilling. Auger refusal in the two
borings ranged from 45 ft bgs (MW-13) to 40 ft bgs (MW-14). Upon completion of the borings,
the type II monitoring wells were constructed with 2-inch schedule 40 PVC flush threaded
screen and casing. The PVC screen and casing was lowered into the open borehole of
monitoring well MW-13 and MW-14 to a depth of 45 and 40 ft. bgs, respectively. A 20-foot
length of 0.01-inch slotted well screen with a threaded bottom plug was installed to a depth
such that the screened interval intersected the estimated groundwater surface, as encountered
during drilling activities. The solid section of PVC casing was placed above the screened
interval and extended to a point just below the ground surface. The annular space around the
well screens was filled with washed and graded medium sand to approximately 2-feet above the
top of the well screen. A minimum two-foot thick seal of bentonite pellets was placed above the
sand pack and allowed to hydrate before backfilling the remaining borehole annulus with a
bentonite/neat cement mixture. The top of the well casings were equipped with a lockable,
water tight well plug and a flush mounted protective steel cover. Monitoring well construction
diagram and NCDEQ Well Construction Record are included in Appendix D. ECS personnel
field notes are included in Appendix A.

Following installation completion, monitoring wells MW-13 and MW-14 were developed on May
3, 2019. The wells were developed to remove the sand, silt, and other fine sediments that may
have entered the wells during construction.

4.3 Groundwater Sampling

On April 17-18, 2019, ECS collected a field blank and groundwater samples from monitoring
wells MW-1 through MW-14, and DW-1. ECS also collected groundwater samples from water
supply wells WSW-2, WSW-3, PW-3R, and PW-4B. Purging and sampling were accomplished
after allowing the water to run from the water supply wells for approximately 10 minutes.

On May 3, 2019, ECS collected groundwater samples from newly installed monitoring wells
MW-13 and MW-14. On May 9, 2019, ECS horizontally and vertically located surveyed the two
newly installed monitoring wells, relative to the existing well network and common site
benchmark. The relative elevation of the top of casing for each monitoring well and the
measurement of the depth to groundwater surface from the top of the monitoring well casing
were used to determine the relative elevation of groundwater at each monitoring well location. A
summary of the groundwater elevation data is presented in Table 5 and displayed on Figure 7.
Since top of water elevations were collected on differing dates (April then May) an accurate
comparison of groundwater elevations and flow direction cannot be determined. Additionally,
Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

based on the measured depth to water in recently installed MW-13 as compared to the
remaining depth to water measurements (i.e., approximately 20 feet lower in MW-13), it
appears that the groundwater within MW-13 had not stabilized at its final elevation. However,
based on historical data and surface topography, it is estimated that groundwater flows outward
in an approximate radial pattern. Groundwater elevation data collected during future sampling
events can be used to better determine the actual flow direction.

Prior to collecting groundwater samples, the wells were purged in an effort to collect a sample that
is representative of site groundwater. After completing monitoring well sampling activities, ECS
collected a field blank sample by pouring laboratory grade deionized water over the water level
meter probe that was used to collect depth to water measurements, and into the appropriate
laboratory prepared sample containers.

Purging and sampling of monitoring wells were accomplished using a new disposable bailer for
each well, attached to nylon string. ECS was not able to collect geochemical measurements on
April 17-18, 2019 due equipment malfunction; however, was able to collect geochemical
measurements during sampling of MW-13 and MW-14 on May 7, 2019 using an YSI-556 multi-
parameter meter. Immediately after collection, the groundwater samples were transferred into
sample containers provided by the laboratory.

After collection, the sample containers were labeled with ECS project number, sample
identification, sample date and time, and requested analytical analysis. The containers were
placed into protective packaging material and placed into a cooler with ice to maintain the
samples at approximately 4 Celsius ( C). The samples were submitted to Con-Test for
chemical analysis for VOCs using Standard Method 6200B. ECS maintained proper COC
procedures throughout the sample collection and transportation process. ECS sampling
worksheets are included in Appendix B. The laboratory analytical data sheets and COCs are
included in Appendix E.

5.0 LABORATORY ANALYTICAL RESULTS

5.1 Soil Samples

Results of the laboratory analysis of soil samples SS-1 and SS-2 reported only C9-C36 alphatics
and C11-C22 aromatics at concentrations above their respective laboratory reporting limits but
below their respective Soil-to-Water and residential MSCCs in soil sample SS-2. The laboratory
analysis did not report targeted analytes at concentrations above the laboratory reporting limits in
soil sample SS-1.A summary of the soil laboratory analytical results are included in Table 9 and
the locations of the soil borings are shown on Figure 5. The historical soil laboratory analytical
results are included in Table 2. The laboratory analytical reports and COC’s are included in
Appendix E.

5.2 Groundwater Samples

Results of the laboratory analysis of the groundwater samples collected in April and May 2019
reported benzene and EDB at concentrations above their respective GCL and respective
NC2LGWQS in the groundwater sample collected from monitoring wells MW-5 and MW-11.
Laboratory analysis reported benzene at a concentration above its GCL and NC2LGWQS in the
Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

groundwater sample collected from monitoring well MW-13. Laboratory analysis reported MTBE
at concentrations above its GCL and NC2LGWQS in the groundwater sample collected from
monitoring wells MW-4 and DW-1.

Laboratory analysis reported several targeted analytes above their respective NC2LGWQS but
below their respective GCL in the groundwater samples collected from monitoring wells DW-1,
MW-1, MW-3, MW-4, MW-5, MW-7, MW-8, MW-11, MW-12, and MW-13.

Laboratory analysis reported benzene above its laboratory reporting limit but below its respective
NC2LGWQS in the groundwater sample collected from monitoring well MW-2.

Laboratory analysis did not report targeted analytes above their respective laboratory reporting
limits in the field blank or the groundwater samples collected from monitoring wells MW-6, MW-9,
MW-10, and MW-14.

Results of the laboratory analysis of the water supply well samples identified select VOCs at
concentrations above their respective laboratory reporting limit from WSW-3; PW-3R; and PW-4B
with the detected concentrations of MTBE in PW-3R and PW-4B exceeding the NC2LGWQS.
Laboratory analysis did not report targeted analytes above their respective laboratory reporting
limits in the groundwater sample from water supply well WSW-2 and the field blank.

A summary of the current groundwater laboratory analytical results, including water supply well
results, are included in Table 7 and on Figures 8 and 9. An isoconcentration map depicting the
horizontal extent of benzene is shown on Figure 10. A summary of the historical groundwater
laboratory analytical results are included in Table 8. The laboratory analytical data sheets and
COCs are included in Appendix D.

7.0 CONCLUSIONS

Based on the results of this Comprehensive Site Assessment, ECS has the following
conclusions:

 A release from the two USTs has impacted the groundwater with several volatile organic
compounds identified at concentrations exceeding their respective NC2LGWQS, with the
concentrations of benzene, MTBE and EDB also reported above their respective GCLs.
 The extent of soil contamination was previously delineated around the former UST system;
o Petroleum-related hydrocarbons were detected in one of the soil samples
collected adjacent to the former pump island at concentrations above the soil-to-
groundwater MSCCs.
 Based on historical groundwater elevation data and ground surface topography, the
groundwater is anticipated to flow outward from the site in a radial pattern.
 According to the City of Roxboro Public Services, municipal water is not connected to the
subject site and not available to the surrounding area.
 There are nine active water supply wells identified within 1,000 feet of the release. Three of
the active water supply wells, WSW-3, PW-3R, and PW-4B, are located within 500 feet of
the release.
Comprehensive Site Assessment – Mt. Harmony Grocery
Rougemont, Person County, North Carolina
NCDEQ Incident No: TF-3831
NCDEQ Contract: N17006
ECS Project No: 49:3051-E

 A geophysical survey indicated a negative anomaly that is estimated to be a potential UST,
located besides the former store building and behind the former fuel dispenser. However,
laboratory analysis of the soil samples collected adjacent to the anomaly did not report
targeted analytes at concentrations above the Soil-to-Water or residential MSCCs.
 The extent of the contaminant plume has not been delineated to the west and north of the
site.

8.0 RECOMMENDATIONS

Based on the results and conclusions of this Comprehensive Site Assessment and a discussion
with Mr. Mark Petermann of NCDEQ, ECS and NCDEQ have agreed upon the following
recommendation:
 ECS and NCDEQ will have a meeting to discuss the hydrogeology at the site for the
development and approach for future environmental assessments. Topics to discuss but not
limited to developing cross sections, obtaining water supply well depths, installation of
piezometers, and/or conducting HPT drilling activities at the site to determine fractures
within the bedrock beneath the site.
 Potentially excavate and remove the anomaly indicative of a UST along the southern side of
the site building.
 Potentially excavate and remove the concrete pad, product piping, and residual soils where
the dispensers were formerly located.

FIGURES
SOURCE:
USGS TOPOGRAPHIC MAP
MORIAH & TIMBERLAKE
NORTH CAROLINA QUADRANGLE
DATED 2016
SCALE: 1 : 24,000
FIGURE 1
SITE LOCATION MAP
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
SITE
FIGURE 2
SITE AERIAL MAP
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
SOURCE:
GOOGLE EARTH
DATED 2013
SCALE AS SHOWN
Scale: 1 inch = 170 feet
AGRICULTURAL
RESIDENTIALAGRICULTURAL
Mt. Tirzah
Park
LEGEND
Approximate Location of Site Boundary
Volunteer Fire
Department
SITE
SOURCE:
GOOGLE EARTH
DATED 2013
SCALE AS SHOWN
FIGURE 3
WATER SUPPLY WELL LOCATION MAP
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
LEGEND
Approximate Location of Active
Water Supply Well
Approximate Location of Inactive
Water Supply Well
1,000 ft.
Radius
WSW-3
PW-1
Scale: 1 inch = 290 feet
WSW-1
WSW-2
WSW-5
WSW-6
WSW-7WSW-8
WSW-3
PW-4A
500 ft.
Radius
PW-2
WSW-3 supplies
water to the
house associated
with PW-2
PW-4B
SITE
PW-2
PW-3R
SOURCE:
PERSON COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 4
ADJACENT PROPERTIES MAP
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
LEGEND
Property Number Corresponding
with Table 4
SITE
Scale: 1 inch = 210 feet
1
2
3
4
5
3
6
7
FIGURE 5
2019 SOIL BORING LOCATION MAP
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
SOURCE:
PERSON COUNTY GIS
DATED 2016
SCALE AS SHOWN
Scale: 1 inch = 120 feet
LEGEND
Approximate Location of Site Boundary
Approximate Location of Soil Boring
Approximate Location of the Possible UST Basin
SS-1
MW-14
BRL
SS-2
SS-1
FIGURE 6
MONITORING WELL LOCATION MAP
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
SOURCE:
GOOGLE EARTH
DATED 2013
SCALE AS SHOWN
Scale: 1 inch = 120 feet
LEGEND
Approximate Location of Site Boundary
Approximate Location of Monitoring Well
Approximate Location of Former USTs
MW-4
MW-1
MW-7 MW-5
MW-10
MW-2
DW-1
MW-4
MW-6
MW-8
MW-9
MW-3
MW-11
MW-12
MW-13
MW-14
FIGURE 7
GROUNDWATER ELEVATION MAP
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
SOURCE:
GOOGLE EARTH
DATED 2013
SCALE AS SHOWN
Scale: 1 inch = 120 feet
MW-1
73.88
MW-7
74.40
MW-5
76.94
MW-10
74.72
MW-2
76.18
DW-1
66.72
MW-4
73.98
MW-6
77.38
MW-8
77.38
MW-9
75.89
MW-3
74.83
LEGEND
Approximate Location of Site Boundary
Approximate Location of Monitoring Well with
Groundwater Elevation in Feet Below Top of Casing
(Ft. btoc)
* Monitoring well MW-13 was a newly installed well and the static water
level may not have equilibrated prior to measuring and collecting the
groundwater sample.
MW-3
74.83
MW-11
75.47
MW-12
73.01
MW-13*
54.26
MW-14
74.03
FIGURE 8
GROUNDWATER CONCENTRATION MAP
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
SOURCE:
PERSON COUNTY GIS
DATED 2016
SCALE AS SHOWN
Scale: 1 inch = 120 feet
LEGEND
Approximate Location of Site Boundary
Approximate Location of Monitoring Well
Concentration Exceeds NC2LGWQS (μg/L)
Concentration Exceeds GCL (μg/L)
BRL Below Laboratory Reporting Limit
J Estimated Concentration
* Concentrations reported above their respective NC2LGWQS shown above.
MW-4
MW-10
BRL
MW-9
BRL
100
29,000
MW-11
Benzene 29,000
Ethylbenzene 1,600
Toluene 18,000
Total Xylenes 11,700
EDB 620
1,2-Dichloroethane 1,600
DIIPE 280
Isopropylbenzene 120 J
MTBE 2,900
Naphthalene 1,500 J
n-Propropylbenzene 320
1,2,4-Trimethylbenzene 2,200
1,3,5-Trimethylbenzene 560
MW-7
Benzene 1,400
DIIPE 190
MTBE 6,200
MW-5
Benzene 7,600
Ethylbenzene 890
Toluene 3,400
Total Xylenes 5,700
EDB 75 J
1,2-Dichloroethane 1,000
DIIPE 400
MTBE 13,000
Naphthalene 560 J
n-Propropylbenzene 110
1,2,4-Trimethylbenzene 1,100
MW-4
Benzene 2,900
Toluene 3,400
Total Xylenes 4,800
1,2-Dichloroethane 600
DIIPE 760
MTBE 53,000
1,2,4-Trimethylbenzene 1,100
1,3,5-Trimethylbenzene 580
MW-3
Benzene 47
MTBE 28
MW-1
Benzene 100
Total Xylenes 1,320
DIIPE 5.4 J
MTBE 830
Naphthalene 100
1,2,4-Trimethylbenzene 990
MW-14
BRL
MW-6
BRL
MW-13
Benzene 5,000
Toluene 1,100
Total Xylenes 4,700
MTBE 1,800
Naphthalene 520
n-Propropylbenzene 100
1,2,4-Trimethylbenzene 1,100
MW-12
MTBE 310
MW-8
1,2-Dichloroethane 6.9
MTBE 270
DW-1
Benzene 220 J
DIIPE 780
MTBE 88,000
MW-2
Benzene 0.40J
SOURCE:
GOOGLE EARTH
DATED 2013
SCALE AS SHOWN
FIGURE 9
WATER SUPPLY WELL GROUNDWATER
CONCENTRATION MAP
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
LEGEND
Approximate Location of Active
Water Supply Well
Approximate Location of Inactive
Water Supply Well
Concentration Exceeds NC2LGWQS (μg/L)
1,000 ft.
Radius
WSW-3
Scale: 1 inch = 290 feet
WSW-1
WSW-2
BRL
WSW-5
WSW-6
WSW-7
WSW-8
PW-4A
500 ft.
Radius
PW-2
SITE
PW-2
WSW-3
Isopropylbenzene 0.17 J
Methyl tert-Butyl Ether (MTBE) 9.5
930
PW-4B
1,2-Dichloroethane 1.6
Diisopropyl Ether 4.8
Methy tert-Butyl Ether (MTBE) 110
PW-3R (Pre-POE)
Diisopropyl Ether 23
Methyl tert-Butyl Ether (MTBE) 930
PW-1
FIGURE 10
BENZENE ISOCONCENTRATION MAP
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
SOURCE:
PERSON COUNTY GIS
DATED 2016
SCALE AS SHOWN
Scale: 1 inch = 120 feet
MW-7
1,400
MW-10
BRL
MW-6
BRL
MW-8
BRL
MW-9
BRL
10,000
1,000
100
10
MW-11
29,000
MW-12
BRL
MW-1
100
MW-3
47
MW-2
0.40 J MW-5
7,600
MW-4
2,900
DW-1*
220 J
MW-13*
5,000
LEGEND
Approximate Location of Site Boundary
Isoconcentration Contour Line (μg/L)
Approximate Location of Monitoring Well
Concentration Exceeds NC2LGWQS (μg/L)
Concentration Exceeds GCL (μg/L)
BRL Below Laboratory Reporting Limit
J Estimated Concentration
* Deep Well DW-1 was not included in defining the horizontal extent of benzene.
MW-4
100
29,000
MW-14
BRL
TABLES
UST ID
Number
Last
Contents
Capacity
(in Gallons)
Construction
Details
Tank
Dimensions
Installation
Date
Removal
Date Status
1 Gasoline 1,000 Unknown Unknown Unknown 1990 Removed
2 Gasoline 1,000 Unknown Unknown Unknown 1990 Removed
Rougemont, Person County, North Carolina
ECS Project: 49:3051-E
Table 1
UST Information
Mt. Harmony Grocery
1818 Mt. Harmony Church Road
NCDEQ Incident: TF-3831
EPA Method 5030
Sample ID Type Sample Date
Sample Depth (feet
bgs.)
S1 3-6 780 NA NA NA NA
S2 3-6 34 NA NA NA NA
S3 3-8 5.8 NA NA NA NA
S4 3-9 47.0 NA NA NA NA
S5 4 39.7 NA NA NA NA
S6 8 229 NA NA NA NA
S7 9 22.2 NA NA NA NA
S8 9 1,780 NA NA NA NA
S9 8 1,220 NA NA NA NA
S10 6 1,520 NA NA NA NA
SB-1A 4.5-5.5 NA BRL BRL BRL BRL
SB-2A 4.5-6 NA BRL BRL BRL 24.6
SB-2B 7.5-8.5 NA BRL BRL BRL BRL
SB-3A 4.5-6 NA BRL BRL BRL BRL
SB-4A 5.5-7 NA BRL BRL BRL BRL
SB-5A 5-6 NA BRL BRL BRL BRL
SB-6A 6-8.5 NA BRL BRL BRL BRL
SB-6B 8.5-9 NA BRL BRL BRL BRL
SB-7A 3.5-4.5 NA BRL BRL BRL BRL
SB-8A 4-5.5 NA 11.4 6.2 17.7 BRL
50 - - - -
-3.3 0.16 0.2 0.02
-626 313 100 85
Notes:
MSCC = Maximum Soil Contaminant Concentration Levels
mg/kg = milligram per kilogram
BOLD = Detected above the Soil-to-Groundwater MSCC and/or the Action Level
BRL = Below Laboratory Reporting Limit
Ft. bgs = Feet below ground surface
NCDEQ = North Carolina Department of Environmental Quality
Analytical Method
*2017 soil samples were submitted for chemical analysis for volatile organic compounds (VOCs) using EPA Method 8260, semi-
volatile organic compounds (SVOCs) using EPA Method 8270, volatile petroleum hydrocarbons (VPH) and extractable petroleum
hydrocarbons (EPH) using the Massachusetts Department of Environmental Protection (MADEP) Methods.p-IsopropyltolueneMethylene ChlorideSoil-to-Groundwater MSCC (mg/kg)
Residential MSCC (mg/kg)
Grab
Table 2
Summary of Historical Soil Sample Analytical Results
Mt. Harmony Grocery
1818 Mt. Harmony Church Road
Rougemont, Person County, North Carolina
Grab
Composite
Standard Method 8260B
sec-ButylbenzeneNaphthaleneNCDEQ Incident: TF-3831
TPH-GRO = Total Petroleum Hydrocarbons - Gasoline Range Organics
NCDEQ UST Section's Action Level (mg/kg)
All results are listed in mg/kg parts per million.
mg/kg = Milligrams per Kilogram
Contaminant of Concern
TPH-GRO
8/10/2017*
3/8/1990
ECS Project: 49:3051-E
Water Supply Well
ID Well Owner/ Address Well Address Well Use Well Depth
(ft bgs)
Approximate
Distance from
Source Area of
Release (ft)
PW-1
Billy Barber
90 Fletcher Ridge Road
Timberlake, NC 27583
1818 Mt Harmony Church Road
Rougemont, NC 27572
(Subject Site)
Inactive Unknown 165 Feet
North
PW-2
Kristi Latta
1850 Mt. Harmony Church Road*
Rougemont, NC 27572
1850 Mt. Harmony Church Road
Rougemont, NC 27572 Inactive Unknown 165 Feet
South
PW-3R
Billy Barber
90 Fletcher Ridge Road
Timberlake, NC 27583
1818 Mt Harmony Church Road
Rougemont, NC 27572
(Subject Site)
Potable Unknown 265 Feet
Northwest
PW-4B Fire Dept.
County of Person
304 South Morgan Street
Roxboro, NC 27573
Mt. Harmony Church Road
Rougemont, NC 27572 Potable Unknown 430 Feet
Southeast
WSW-1
Mt. Harmony Baptist Church
1655 Mt. Harmony Church Road
Rougemont, NC 27572
1655 Mt. Harmony Church Road
Rougemont, NC 27572 Potable Unknown 745 Feet
North-northeast
WSW-2
Clifton Bradsher
309 Peed Road
Rougemont, NC 27572
50 Glen Fogleman Road
Rougemont, NC 27572 Potable Unknown 620 Feet
Northeast
WSW-3*
Elger and Bobbie Latta
Mt. Harmony Church Road
Rougemont, NC 27572
Mt. Harmony Church Road
Rougemont, NC 27572 Potable Unknown 300 Feet South
PW-4A Ball Park
County of Person
304 South Morgan Street
Roxboro, NC 27573
Mt. Harmony Church Road
Rougemont, NC 27572 Inactive Unknown 290 Feet
East-southeast
WSW-5
Crystal Scott
1915 Mt. Harmony Church Road
Rougemont, NC 27572
1915 Mt. Harmony Church Road
Rougemont, NC 27572 Potable Unknown 530 Feet
South-southeast
WSW-6
Helen Bowling
1941 Mt. Harmony Church Road
Rougemont, NC 27572
1941 Mt. Harmony Church Road
Rougemont, NC 27572 Potable Unknown 640 Feet
South-southeast
WSW-7
Ronald Mooney
1988 Mt. Harmony Church Road
Rougemont, NC 27572
1988 Mt. Harmony Church Road
Rougemont, NC 27572 Potable Unknown 860 Feet
South
WSW-8
Ryan Mooney
2028 Mt. Harmony Church Road
Rougemont, NC 27572
2028 Mt. Harmony Church Road
Rougemont, NC 27572 Potable Unknown 950 Feet
South
Notes:
* = Water Supply Well PW-2 is inactive but WSW-3 dispenses at the pump house associated with WPW-2.
ECS Project: 49:3051-E
ft bgs = feet below the ground surface
Table 3
Water Supply Well Survey Data
Mt. Harmony Grocery
1818 Mt. Harmony Church Road
Rougemont, Person County, North Carolina
NCDEQ Incident: TF-3831
ft = feet
Indentification Number on
Figure 6 Map PIN Parcel Address Owner and Owner Address Active City Water Account
Water Well
On-Site
1 0943-00-05.4578.000 1655 Mt. Harmony Church Road
Mt. Harmony Baptist Church
1655 Mt. Harmony Church Road
Rougemont, NC 27572
No Yes
2 0943-00-04-5687.000 Mt. Harmony Church Road
County of Person
304 South Morgan Street
Roxboro, NC 27573
No Yes
3 0933-00-94-8047.000 Mt. Harmony Church Road
Bobbie Latta
131 Peed Rd
Rougemont, NC 27572
No
(Vacant Land)Yes
4 0933-00-94-9405.000 Mt. Harmony Church Road
Billy Barber
90 Fletcher Ridge Road
Timberlake, NC 27583
No
(Vacant Land)Yes
5 0933-00-95-6209.000 Mt. Harmony Church Road
V & E Farm LLC
180 White Oak Drive
Roxboro, NC 27573
No
(Agricultural)Yes
6 0943-00-04-2396.000 1850 Mt. Harmony Church Road
Kristi Latta (Kristi Williams)
1850 Mt. Harmony Church Road
Rougemont, NC 27572
No Yes
7 0943-00-04-6987.000 50 Glen Fogleman Road
Clifton Bradsher
309 Peed Road
Rougemont, NC 27572
No Yes
*Data was confirmed via Person County GIS viewer at https://gis.personcounty.net/TaxParcelViewer/ on November 6, 2018
NCDEQ Incident: TF-3831
ECS Project: 49:3051-E
Rougemont, Person County, North Carolina
Table 4
Adjacent Properties
Mt. Harmony Grocery
1818 Mt. Harmony Church Road
Monitoring Well ID Date
Measured
Casing Inner
Diameter
(I.D. in. )
Depth to
Groundwater
(ft. btoc)
Date
Installed
Total Well
Depth
(ft. btoc)
Screen
Interval
(ft. btoc)
TOC
Elevation*
Groundwater
Elevation (ft)*
MW-1 4/17/2019 2.00 21.12 5/24/2005 37 27-37 95.00 73.88
MW-2 4/17/2019 2.00 17.87 9/23/2004 30 20-30 94.05 76.18
MW-3 4/17/2019 2.00 18.72 5/25/2005 40 20-40 93.55 74.83
MW-4 4/17/2019 2.00 19.67 5/25/2005 40 20-40 93.65 73.98
MW-5 4/17/2019 2.00 19.38 8/10/2017 34 19-34 96.32 76.94
MW-6 4/17/2019 2.00 19.69 8/10/2017 30 15-30 97.07 77.38
MW-7 4/17/2019 2.00 19.40 1/5/2018 50 30-50 93.80 74.40
MW-8 4/17/2019 2.00 20.87 1/8/2018 50 30-50 98.25 77.38
MW-9 4/17/2019 2.00 16.46 1/8/2018 50 30-50 92.35 75.89
MW-10 4/17/2019 2.00 18.13 1/8/2018 50 30-50 92.85 74.72
MW-11 4/17/2019 2.00 16.69 9/18/2018 34 24-34 92.16 75.47
MW-12 4/17/2019 2.00 17.59 9/18/2018 40 20-40 90.60 73.01
MW-13 5/3/2019 2.00 37.87 5/3/2019 45 25-45 92.13 54.26
MW-14 5/3/2019 2.00 17.57 5/3/2019 40 20-40 91.60 74.03
DW-1 4/17/2019 2.00 20.35 5/26/2005 65 60-65 94.57 74.22
Notes:
ft. btoc = Feet Below Top of Casing
I.D. in. = Inner Diameter in Inches
* TOC Elevations and Groundwater Elevation Data are based on a common site benchmark.
NCDEQ Incident: TF-3831
TOC = Top of Casing Elevation Measured on April 17, 2019 and May 7, 2019
Table 5
Monitoring Well Construction and Groundwater Elevation Details
Mt. Harmony Grocery
1818 Mt. Harmony Church Road
Rougemont, Person County, North Carolina
ECS Project: 49:3051-E
Parameter
Sample ID SS-1 SS-2
Collection Depth (feet bgs.)8-9 8-9
PID Reading (ppm)0.0 0.0
Collection Date 5/3/2019 5/3/2019
METHOD 8260/5035A VOLATILE ORGANIC COMPOUNDS (VOCS)
Targeted VOCs Analyzed BRL BRL VARIES VARIES
Targeted SVOCS Analyzed BRL BRL VARIES VARIES
VPH and EPH BY MADEP
C19-C36 Aliphatics BRL 110 IMMOBILE 810,000
C9-C22 Aromatics BRL 18 31 469
Unadjusted C9-C22 Aromatics BRL 18 31 469
Notes:
MSCC = Maximum Soil Contaminant Concentration Levels
VPH = volatile petroleum hydrocarbons
EPH = extractable petroleum hydrocarbons
MADEP = Massachusetts Department of Environmental Protection
mg/kg = milligram per kilogram
BRL = Below Laboratory Reporting Limit
ft. bgs = feet below ground surface
Soil-to-
Groundwater
MSCC (mg/kg)
Residential MSCC
(mg/kg)
METHOD 8270D SEMI-VOLATILE ORGANIC COMPOUNDS (SVOCS)
*Soil samples were submitted for chemical analysis for volatile organic compounds (VOCs) using EPA
Method 8260, semi-volatile organic compounds (SVOCs) using EPA Method 8270, volatile petroleum
hydrocarbons (VPH) and extractable petroleum hydrocarbons (EPH) using the Massachusetts Department
of Environmental Protection (MADEP) Methods.
Table 6
Summary of Current 2019 Soil Sample Analytical Results
Mt. Harmony Grocery
1818 Mt. Harmony Church Road
Rougemont, Person County, North Carolina
NCDEQ Incident: TF-3831
ECS Project: 49:3051-E
COMPARISON CRITERIA
MW-1 4/18/2019 100 150 390 2,320 BRL 16 8.8 J BRL BRL 5.4 J 27 7.8 J 830 100 66 3.4 J 990 380
MW-2 4/18/2019 0.40 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
MW-3 4/18/2019 47 5.1 2.0 4.5 BRL 0.30 J 0.19 J BRL 1.4 0.95 0.82 BRL 28 3.5 1.5 0.18 J 9.8 1.6
MW-4 4/18/2019 2,900 270 3,400 4,800 BRL BRL BRL BRL 600 760 BRL BRL 53,000 BRL BRL BRL 1,100 580
MW-5 4/17/2019 7,600 890 3,400 5,700 BRL BRL BRL 78 J 1,000 400 52 J BRL 13,000 560 J 110 24 J 1,100 320
MW-6 4/17/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
MW-7 4/17/2019 1,400 80 460 460 BRL BRL BRL BRL BRL 190 BRL BRL 6,200 BRL BRL BRL 62 26 J
MW-8 4/17/2019
BRL BRL BRL BRL BRL BRL BRL BRL 6.9 8.9 BRL BRL 270 BRL BRL BRL BRL BRL
MW-9 4/17/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
MW-10 4/17/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
MW-11 4/17/2019 29,000 1,600 18,000 11,700 BRL BRL BRL 620 1,600 280 120 J BRL 2,900 1,500 J 320 BRL 2,200 560
MW-12 4/17/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL 5.1 BRL BRL 310 BRL BRL BRL BRL BRL
MW-13 5/3/2019 5,000 330 1,100 4,700 310 BRL BRL BRL 100 120 36 BRL 1,800 520 100 47 1,100 230
MW-14 5/3/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
DW-1 4/18/2019 220 J BRL BRL BRL BRL BRL BRL BRL BRL 780 BRL BRL 88,000 BRL BRL BRL BRL BRL
WSW-2 4/18/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
WSW-3 4/18/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.17 J BRL BRL 9.5 BRL BRL BRL BRL BRL
PW-3R 4/18/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL 23 BRL BRL 930 BRL BRL BRL BRL BRL
PW-4B 4/18/2019 BRL BRL BRL BRL BRL BRL BRL BRL 1.6 4.8 BRL BRL 110 BRL BRL BRL BRL BRL
Field Blank 4/17/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
1 600 600 500 6,000 70 70 0.02 6 70 70 25 20 6 70 70 400 400
5,000 84,500 260,000 85,500 6,000,000 6,900 8,500 50 6,000 70,000 25,000 11,700 20,000 6,000 30,000 70,000 28,500 25,000
Notes:
NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013
GCL = NCDEQ's Gross Contamination Levels for Groundwater as of April 16, 2012
(µg/L) = Micrograms per Liter
BOLD = Detected above the NC2LGWQS
BRL = Below Laboratory Reporting Limit
J = Detetcted below laboratory reporting limit; therefore result is an estimated concentration
GCL (µg/L)
Sample ID Sample Date
1,2,4-Trimethylbenzenesec-Butylbenzene1,2-Dibromoethane (EDB)Diisopropyl Ether (DIPE)Isopropylbenzene (Cumene)Table 7
Summary of Current Groundwater Analytical Results
Mt. Harmony Grocery
1818 Mt. Harmony Church Road
Rougemont, Person County, North Carolina
NC2LGWQS (µg/L)p-Isopropyltoluene (p-Cymene)Naphthalenen-Propylbenzene1,2-DichloroethaneECS Project: 49:3051-E
Analytical Method Standard Method 6200B (µg/L)Styrene1,3,5-TrimethylbenzeneMethyl tert-Butyl Ether (MTBE)NCDEQ Incident: TF-3831
BenzeneEthylbenzeneTolueneTotal XylenesAcetonen-Butylbenzene
8/10/2017 8,790 777 14,900 9,000 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 104,000 BRL BRL BRL BRL 1,100 BRL
1/5/2018 12,000 3,400 36,000 28,800 BRL 100 26 BRL BRL BRL 450 180 BRL BRL BRL 48,000 740 400 BRL BRL 3,500 970
9/19/2018 910 BRL 3,200 8,700 BRL BRL BRL BRL BRL BRL 200 BRL BRL BRL BRL 35,000 240 140 J BRL BRL 2,000 700
4/18/2019 100 150 390 2,320 BRL 16 8.8 J BRL BRL BRL 5.4 J 27 7.8 J BRL BRL 830 100 66 3.4 J BRL 990 380
10/10/2016 BRL BRL BRL 5.3 BRL BRL BRL BRL BRL BRL BRL 1.4 BRL BRL BRL BRL 2.5 2.0 BRL BRL 18 5.2
8/10/2017 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
1/5/2018 BRL 0.44 1.1 0.63 BRL 0.17 BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.33 2.5 0.29 BRL BRL BRL BRL
9/19/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
4/18/2019 0.40 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
10/10/2016 18,000 720 690 900 BRL BRL BRL BRL BRL 100 470 69 BRL 760 150 19,000 460 130 BRL BRL 920 250
8/10/2017 13,500 528 578 723 BRL BRL BRL BRL BRL 94.8 BRL BRL BRL BRL BRL 18,800 283 86 BRL BRL 510 510
1/5/2018 2,500 200 200 407 BRL 18 4.6 BRL BRL 40 120 18 BRL BRL BRL 6,200 200 47 39 BRL 420 99
9/19/2018 5.0 BRL 0.42 J 0.77 J 13 J BRL BRL BRL BRL 0.74 3.5 BRL BRL BRL BRL 99 BRL BRL BRL BRL 1.0 0.36 J
4/18/2019 47 5.1 2.0 4.5 BRL 0.30 J 0.19 J BRL BRL 1.4 0.95 0.82 BRL BRL BRL 28 3.5 1.5 0.18 J BRL 9.8 1.6
10/10/2016 8,600 410 7,700 13,000 560 J BRL BRL BRL BRL 860 970 BRL BRL 180 BRL 86,000 590 BRL BRL BRL 2,600 810
8/10/2017 3,900 BRL 3,740 4,450 BRL BRL BRL BRL BRL 554 BRL BRL BRL BRL BRL 61,600 BRL BRL BRL BRL 749 BRL
1/5/2018 9,300 550 11,000 15,900 BRL 65 BRL BRL 31 750 880 19 BRL BRL BRL 84,000 670 41 BRL BRL 3,400 930
9/19/2018 1,400 BRL 1,600 5,100 BRL BRL BRL BRL BRL 510 680 BRL BRL BRL BRL 54,000 230 J BRL BRL BRL 1,400 840
4/18/2019 2,900 270 3,400 4,800 BRL BRL BRL BRL BRL 600 760 BRL BRL BRL BRL 53,000 BRL BRL BRL BRL 1,100 580
8/11/2017 23,400 2,070 11,400 10,150 BRL BRL BRL BRL 165 165 440 67.2 BRL BRL BRL 18,100 BRL 160 75.2 BRL 951 259
9/18/2018 19,000 2,200 11,000 16,200 BRL 55 J BRL BRL 100 J BRL 380 BRL BRL BRL BRL BRL 610 200 BRL BRL 2,400 620
4/17/2019 7,600 890 3,400 5,700 BRL BRL BRL BRL 78 J 1,000 400 52 J BRL BRL BRL 13,000 560 J 110 24 J BRL 1,100 320
8/21/2017 1.2 1.4 1.8 6 BRL BRL BRL 1 BRL BRL BRL BRL BRL BRL BRL 2.0 BRL BRL BRL BRL 2.2 BRL
9/18/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.40 J BRL BRL BRL BRL BRL BRL
4/17/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
1/8/2018 61 110 310 620 BRL 16 5.2 BRL BRL BRL 190 12 2.8 BRL BRL 11,000 77 44 3.3 BRL 310 87
9/19/2018 450 30 J 99 63 J BRL BRL BRL BRL BRL BRL 200 BRL BRL BRL BRL 9,700 BRL BRL BRL BRL 25 J BRL
4/17/2019 1,400 80 460 460 BRL BRL BRL BRL BRL BRL 190 BRL BRL BRL BRL 6,200 BRL BRL BRL BRL 62 26 J
1/11/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL 8.9 6.0 BRL BRL BRL BRL 300 BRL BRL BRL BRL BRL BRL
9/18/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL 8.6 9.0 BRL BRL BRL BRL 200 BRL BRL BRL BRL BRL BRL
4/17/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL 6.9 8.9 BRL BRL BRL BRL 270 BRL BRL BRL BRL BRL BRL
1/11/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
9/18/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
4/17/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
1/11/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
9/18/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
4/17/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
10/1/2018 34,000 1,700 22,000 14,000 BRL 100 BRL BRL 510 2,200 250 150 BRL BRL BRL 3,500 730 400 BRL BRL 2,700 710
4/17/2019 29,000 1,600 18,000 11,700 BRL BRL BRL BRL 620 1,600 280 120 J BRL BRL BRL 2,900 1,500 J 320 BRL BRL 2,200 560
10/1/2018 BRL BRL BRL 0.75 J BRL BRL BRL BRL BRL BRL 5.2 BRL BRL BRL BRL 540 BRL BRL BRL BRL BRL BRL
4/17/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 5.1 BRL BRL BRL BRL 310 BRL BRL BRL BRL BRL BRL
MW-13 5/3/2019 5,000 330 1,100 4,700 310 BRL BRL BRL BRL 100 120 36 BRL BRL BRL 1,800 520 100 47 BRL 1,100 230
MW-14 5/3/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
10/10/2016 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 2.5 BRL BRL 190 BRL BRL BRL BRL BRL BRL BRL BRL
8/10/2017 BRL BRL 15.2 BRL BRL BRL BRL BRL BRL BRL 29.6 BRL BRL BRL BRL 3,210 BRL BRL BRL BRL BRL BRL
1/5/2018 0.93 4.6 14 44 BRL 1.9 0.35 BRL BRL BRL 16 0.79 0.17 BRL BRL 1,900 4.3 2.5 BRL 0.28 21 6.7
9/18/2018 100 J BRL BRL BRL BRL BRL BRL BRL BRL BRL 640 BRL BRL BRL BRL 75,000 BRL BRL BRL BRL BRL BRL
4/18/2019 220 J BRL BRL BRL BRL BRL BRL BRL BRL BRL 780 BRL BRL BRL BRL 88,000 BRL BRL BRL BRL BRL BRL
PW-1 3/9/1990
3/9/1990 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
8/11/2017
PW-3 3/9/1990 BRL BRL BRL 2.7 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
1/8/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.2 10 BRL BRL BRL BRL 440 BRL BRL BRL BRL BRL BRL
9/18/2018 BRL BRL BRL BRL BRL BRL BRL 5.4 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
4/18/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 23 BRL BRL BRL BRL 930 BRL BRL BRL BRL BRL BRL
8/10/2017 BRL BRL BRL BRL BRL BRL BRL BRL BRL 18.4 38.2 BRL BRL BRL BRL 2,030 BRL BRL BRL BRL BRL BRL
9/18/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL 5.2 15 BRL BRL BRL BRL 690 BRL BRL BRL BRL BRL BRL
4/18/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.6 4.8 BRL BRL BRL BRL 110 BRL BRL BRL BRL BRL BRL
PW-4 3/9/1990 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
8/11/2017 BRL BRL BRL BRL BRL BRL BRL BRL BRL 18.3 BRL BRL BRL BRL BRL 2,020 BRL BRL BRL BRL BRL BRL
8/24/2017 BRL BRL BRL BRL BRL BRL BRL BRL BRL 7.9 BRL BRL BRL BRL BRL 674 BRL BRL BRL BRL BRL BRL
4/18/2019
11/21/2017 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
9/18/2018 BRL BRL BRL BRL BRL BRL BRL 4.9 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
4/18/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
8/10/2017 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 9.6 BRL BRL BRL BRL BRL BRL
9/18/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 9 BRL BRL BRL BRL BRL BRL
4/18/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.17 J BRL BRL BRL BRL 9.5 BRL BRL BRL BRL BRL BRL
1 600 600 500 6,000 70 70 3 0.02 6 70 70 25 40 100 20 6 70 70 3 400 400
5,000 84,500 260,000 85,500 6,000,000 6,900 8,500 3,000 50 6,000 70,000 25,000 11,700 40,000 100,000 20,000 6,000 30,000 70,000 3,000 28,500 25,000
Notes:
NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013
GCL = NCDEQ's Gross Contamination Levels for Groundwater as of April 16, 2012
(µg/L) = Micrograms per Liter
BOLD = Detected above the NC2LGWQS
BRL = Below Laboratory Reporting Limit
J = Detetcted below laboratory reporting limit; therefore result is an estimated concentration ChloromethaneTotal XylenesGCL (µg/L)
NC2LGWQS (µg/L)
PW-2
Sample ID Sample Date
Inactive
MW-1
Inactivesec-ButylbenzeneNCDEQ Incident: TF-3831
ECS Project: 49:3051-E
Analytical Method Standard Method 6200B (or Equilvalent)Trichloroethylene (TCE)AcetoneToluenen-ButylbenzeneBenzeneMethyl Isobutyl KetoneMethyl tert-Butyl Ether (MTBE)Methyl Butyl Ketonep-Isopropyltoluene (p-Cymene)Diisopropyl Ether (DIPE)Table 8
Summary of Current and Historical Groundwater Analytical Results
Mt. Harmony Grocery
1818 Mt. Harmony Church Road
Rougemont, Person County, North Carolina
MW-7 Naphthalenen-PropylbenzeneSytrene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzene (Cumene)Ethylbenzene1,2-Dibrmoethane (EDB)1,2-DichloroethaneInactive
MW-10
MW-12
MW-11
DW-1
MW-2
MW-3
MW-4
MW-5
MW-6
PW-3R
PW-4B (Fire Dept.)
MW-8
MW-9
WSW-2
WSW-3
PW-4A (Ball Park)
APPENDIX A
APPENDIX B
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 1: View of the subject site across Mt. Harmony Church Road. View is to the west.
Photograph 2: View of the location of monitoring wells MW-1 and DW-1. View is to the northwest.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 3: View of the location of monitoring well MW-2. View is to the south.
Photograph 4: View of the location of monitoring well MW-3. View is to the north.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 5: View of the location of monitoring well MW-4. View is to the northwest.
Photograph 6: View of the location of monitoring well MW-5. View is to the east.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 7: View of the location of monitoring well MW-6. View is to the southwest.
Photograph 8: View of the location of monitoring well MW-7. View is to the northwest.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 9: View of the location of monitoring well MW-8. View is to the northwest.
Photograph 10: View of the location of monitoring well MW-9. View is to the northwest.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 11: View of the location of monitoring well MW-10. View is to the southeast.
Photograph 12: View of the location of monitoring well MW-11. View is to the southeast.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 13: View of the location of monitoring well MW-12. View is to the east.
Photograph 14: View of active water supply well WSW-3. View is to the north.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 15: View of inactive water supply well PW-4A. View is to the northwest.
Photograph 16: View of active water supply well PW-4B. View is to the southeast.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 17: View of active water supply well PW-3R. View is to the northwest.
Photograph 18: Additional view of active water supply well PW-3R with filtration system.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 19: View of the soil sample locations. View is to the north.
Photograph 20: View of the location of monitoring well MW-14. View is to the east.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 21: View of the location of monitoring well MW-13. View is to the east.
Photograph 22: View of drilling activities conducted at the site. View is to the east.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 23: View of drilling activities conducted at the site. View is to the southwest.
Photograph 24: View of drilling activities conducted at the site. View is to the east.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 25: View of the location of monitoring well MW-13. View is to the northwest.
Photograph 26: View of the location of monitoring well MW-14. View is to the south.
SITE PHOTOGRAPHS
MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-3831
ECS PROJECT: 49:3051-E
Photograph 27: View of the well construction tag for monitoring well MW-13.
Photograph 28: View of the well construction tag for monitoring well MW-14.
APPENDIX C
APPENDIX D

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APPENDIX E
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
April 29, 2019
Matt Gillis
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
Project Location: Roxboro, NC
Client Job Number:
Project Number: 49:3051-E
Laboratory Work Order Number: 19D1069
Enclosed are results of analyses for samples received by the laboratory on April 19, 2019. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 65
Table of Contents
Table of Contents
Sample Summary 4
Hits Only Report 5
Case Narrative 9
Sample Results 10
19D1069-01 10
19D1069-02 12
19D1069-03 14
19D1069-04 16
19D1069-05 18
19D1069-06 20
19D1069-07 22
19D1069-08 24
19D1069-09 26
19D1069-10 28
19D1069-11 30
19D1069-12 32
19D1069-13 34
19D1069-14 36
19D1069-15 38
19D1069-16 40
19D1069-17 42
19D1069-18 44
Sample Preparation Information 46
QC Data 47
Volatile Organic Compounds by GC/MS 47
Page 2 of 65
Table of Contents
Table of Contents (continued)
B229012 47
B229074 51
B229194 55
Flag/Qualifier Summary 59
Certifications 60
Chain of Custody/Sample Receipt 62
Page 3 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
4/29/2019
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
ATTN: Matt Gillis
49:3051-E
19D1069
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Roxboro, NC
Field Blank 19D1069-01 Field Blank SM21-22 6200B
MW-5 19D1069-02 Ground Water SM21-22 6200B
MW-6 19D1069-03 Ground Water SM21-22 6200B
MW-7 19D1069-04 Ground Water SM21-22 6200B
MW-8 19D1069-05 Ground Water SM21-22 6200B
MW-9 19D1069-06 Ground Water SM21-22 6200B
MW-10 19D1069-07 Ground Water SM21-22 6200B
MW-11 19D1069-08 Ground Water SM21-22 6200B
MW-12 19D1069-09 Ground Water SM21-22 6200B
WSW-2 19D1069-10 Ground Water SM21-22 6200B
WSW-3 19D1069-11 Ground Water SM21-22 6200B
PW-4B 19D1069-12 Ground Water SM21-22 6200B
MW-1 19D1069-13 Ground Water SM21-22 6200B
MW-2 19D1069-14 Ground Water SM21-22 6200B
MW-3 19D1069-15 Ground Water SM21-22 6200B
MW-4 19D1069-16 Ground Water SM21-22 6200B
DW-1 19D1069-17 Ground Water SM21-22 6200B
PW-3R 19D1069-18 Ground Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 4 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:19D1069-01Field Blank
No Results Detected
Client ID:Lab ID:19D1069-03MW-6
No Results Detected
Client ID:Lab ID:19D1069-06MW-9
No Results Detected
Client ID:Lab ID:19D1069-07MW-10
No Results Detected
Client ID:Lab ID:19D1069-10WSW-2
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 5 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-02MW-5
DL
1,2,4-Trimethylbenzene 1100 100 g/L SM21-22 6200B36
1,2-Dibromoethane (EDB)78 100 g/L SM21-22 6200BJ38
1,2-Dichloroethane 1000 100 g/L SM21-22 6200B82
1,3,5-Trimethylbenzene 320 100 g/L SM21-22 6200B28
Benzene 7600 100 g/L SM21-22 6200B36
Diisopropyl Ether (DIPE)400 100 g/L SM21-22 6200B34
Ethylbenzene 890 100 g/L SM21-22 6200B26
Isopropylbenzene (Cumene)52 100 g/L SM21-22 6200BJ34
m+p Xylene 3400 200 g/L SM21-22 6200B60
Methyl tert-Butyl Ether (MTBE)13000 100 g/L SM21-22 6200B50
Naphthalene 560 1000 g/L SM21-22 6200BJ62
n-Propylbenzene 110 100 g/L SM21-22 6200B26
o-Xylene 2300 100 g/L SM21-22 6200B34
Styrene 24 100 g/L SM21-22 6200BJ22
Toluene 3400 100 g/L SM21-22 6200B28
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-04MW-7
DL
1,2,4-Trimethylbenzene 62 50 g/L SM21-22 6200B18
1,3,5-Trimethylbenzene 26 50 g/L SM21-22 6200BJ14
Benzene 1400 50 g/L SM21-22 6200B18
Diisopropyl Ether (DIPE)190 50 g/L SM21-22 6200B17
Ethylbenzene 80 50 g/L SM21-22 6200B13
m+p Xylene 240 100 g/L SM21-22 6200B30
Methyl tert-Butyl Ether (MTBE)6200 50 g/L SM21-22 6200B25
o-Xylene 220 50 g/L SM21-22 6200B17
Toluene 460 50 g/L SM21-22 6200B14
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-05MW-8
DL
1,2-Dichloroethane 6.9 0.50 g/L SM21-22 6200B0.41
Diisopropyl Ether (DIPE)8.9 0.50 g/L SM21-22 6200B0.17
Methyl tert-Butyl Ether (MTBE)270 12 g/L SM21-22 6200B6.2
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-08MW-11
DL
1,2,4-Trimethylbenzene 2200 250 g/L SM21-22 6200B90
1,2-Dibromoethane (EDB)620 250 g/L SM21-22 6200B95
1,2-Dichloroethane 1600 250 g/L SM21-22 6200B200
1,3,5-Trimethylbenzene 560 250 g/L SM21-22 6200B70
Benzene 29000 250 g/L SM21-22 6200B90
Diisopropyl Ether (DIPE)280 250 g/L SM21-22 6200B85
Ethylbenzene 1600 250 g/L SM21-22 6200B65
Isopropylbenzene (Cumene)120 250 g/L SM21-22 6200BJ85
m+p Xylene 6400 500 g/L SM21-22 6200B150
Methyl tert-Butyl Ether (MTBE)2900 250 g/L SM21-22 6200B120
Naphthalene 1500 2500 g/L SM21-22 6200BJ160
n-Propylbenzene 320 250 g/L SM21-22 6200B65
o-Xylene 5300 250 g/L SM21-22 6200B85
Toluene 18000 250 g/L SM21-22 6200B70
Page 6 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-09MW-12
DL
Diisopropyl Ether (DIPE)5.1 0.50 g/L SM21-22 6200B0.17
Methyl tert-Butyl Ether (MTBE)310 12 g/L SM21-22 6200B6.2
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-11WSW-3
DL
Diisopropyl Ether (DIPE)0.17 0.50 g/L SM21-22 6200BJ0.17
Methyl tert-Butyl Ether (MTBE)9.5 0.50 g/L SM21-22 6200B0.25
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-12PW-4B
DL
1,2-Dichloroethane 1.6 0.50 g/L SM21-22 6200B0.41
Diisopropyl Ether (DIPE)4.8 0.50 g/L SM21-22 6200B0.17
Methyl tert-Butyl Ether (MTBE)110 0.50 g/L SM21-22 6200B0.25
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-13MW-1
DL
1,2,4-Trimethylbenzene 990 10 g/L SM21-22 6200B3.6
1,3,5-Trimethylbenzene 380 10 g/L SM21-22 6200B2.8
Benzene 100 10 g/L SM21-22 6200B3.6
Diisopropyl Ether (DIPE)5.4 10 g/L SM21-22 6200BJ3.4
Ethylbenzene 150 10 g/L SM21-22 6200B2.6
Isopropylbenzene (Cumene)27 10 g/L SM21-22 6200B3.4
m+p Xylene 1500 20 g/L SM21-22 6200B6.0
Methyl tert-Butyl Ether (MTBE)830 10 g/L SM21-22 6200B5.0
Naphthalene 100 40 g/L SM21-22 6200B6.2
n-Butylbenzene 16 10 g/L SM21-22 6200B4.2
n-Propylbenzene 66 10 g/L SM21-22 6200B2.6
o-Xylene 820 10 g/L SM21-22 6200B3.4
p-Isopropyltoluene (p-Cymene)7.8 10 g/L SM21-22 6200BJ4.0
sec-Butylbenzene 8.8 10 g/L SM21-22 6200BJ3.2
Styrene 3.4 10 g/L SM21-22 6200BJ2.2
Toluene 390 10 g/L SM21-22 6200B2.8
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-14MW-2
DL
Benzene 0.40 0.50 g/L SM21-22 6200BJ0.18
Page 7 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-15MW-3
DL
1,2,4-Trimethylbenzene 9.8 0.50 g/L SM21-22 6200B0.18
1,2-Dichloroethane 1.4 0.50 g/L SM21-22 6200B0.41
1,3,5-Trimethylbenzene 1.6 0.50 g/L SM21-22 6200B0.14
Benzene 47 0.50 g/L SM21-22 6200B0.18
Diisopropyl Ether (DIPE)0.95 0.50 g/L SM21-22 6200B0.17
Ethylbenzene 5.1 0.50 g/L SM21-22 6200B0.13
Isopropylbenzene (Cumene)0.82 0.50 g/L SM21-22 6200B0.17
m+p Xylene 2.4 1.0 g/L SM21-22 6200B0.30
Methyl tert-Butyl Ether (MTBE)28 0.50 g/L SM21-22 6200B0.25
Naphthalene 3.5 2.0 g/L SM21-22 6200B0.31
n-Butylbenzene 0.30 0.50 g/L SM21-22 6200BJ0.21
n-Propylbenzene 1.5 0.50 g/L SM21-22 6200B0.13
o-Xylene 2.1 0.50 g/L SM21-22 6200B0.17
sec-Butylbenzene 0.19 0.50 g/L SM21-22 6200BJ0.16
Styrene 0.18 0.50 g/L SM21-22 6200BJ0.11
Toluene 2.0 0.50 g/L SM21-22 6200B0.14
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-16MW-4
DL
1,2,4-Trimethylbenzene 1100 250 g/L SM21-22 6200B90
1,2-Dichloroethane 600 250 g/L SM21-22 6200B200
1,3,5-Trimethylbenzene 580 250 g/L SM21-22 6200B70
Benzene 2900 250 g/L SM21-22 6200B90
Diisopropyl Ether (DIPE)760 250 g/L SM21-22 6200B85
Ethylbenzene 270 250 g/L SM21-22 6200B65
m+p Xylene 2200 500 g/L SM21-22 6200B150
Methyl tert-Butyl Ether (MTBE)53000 250 g/L SM21-22 6200B120
o-Xylene 2600 250 g/L SM21-22 6200B85
Toluene 3400 250 g/L SM21-22 6200B70
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-17DW-1
DL
Benzene 220 500 g/L SM21-22 6200BJ180
Diisopropyl Ether (DIPE)780 500 g/L SM21-22 6200B170
Methyl tert-Butyl Ether (MTBE)88000 500 g/L SM21-22 6200B250
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19D1069-18PW-3R
DL
Diisopropyl Ether (DIPE)23 5.0 g/L SM21-22 6200B1.7
Methyl tert-Butyl Ether (MTBE)930 5.0 g/L SM21-22 6200B2.5
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 8 of 65
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B elevated reporting limits for samples 19D1069-02,04+08,13,16,17+18 due to high concentrations of target compounds.
[TOC_1]Case Narrative[TOC]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Vinyl Chloride
B229012-BS1, B229012-BSD1, B229074-BS1, B229074-BSD1, B229194-BS1, B229194-BSD1
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Vinyl Acetate
19D1069-13[MW-1], 19D1069-14[MW-2], 19D1069-15[MW-3], 19D1069-16[MW-4], 19D1069-17[DW-1], 19D1069-18[PW-3R], B229074-BLK1, B229074-BS1,
B229074-BSD1, B229194-BLK1, B229194-BS1, B229194-BSD1
pH of sample (pH 7) is outside of method specified preservation criteria.
Analyte & Samples(s) Qualified:
PR-10
19D1069-17[DW-1]
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
19D1069-02[MW-5], 19D1069-04[MW-7], 19D1069-08[MW-11], 19D1069-13[MW-1], 19D1069-16[MW-4], 19D1069-17[DW-1], 19D1069-18[PW-3R]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
Page 9 of 65
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-01
Field Sample #: Field Blank
Sample Matrix: Field Blank
Sampled: 4/17/2019 17:15
[TOC_2]19D1069-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/24/19 15:55 EEHg/L3.8 4/23/19SM21-22 6200B1Acetone
ND 0.50 4/24/19 15:55 EEHg/L0.18 4/23/19SM21-22 6200B1Benzene
ND 0.50 4/24/19 15:55 EEHg/L0.15 4/23/19SM21-22 6200B1Bromobenzene
ND 0.50 4/24/19 15:55 EEHg/L0.32 4/23/19SM21-22 6200B1Bromochloromethane
ND 0.50 4/24/19 15:55 EEHg/L0.16 4/23/19SM21-22 6200B1Bromodichloromethane
ND 2.0 4/24/19 15:55 EEHg/L0.46 4/23/19SM21-22 6200B1Bromoform
ND 2.0 4/24/19 15:55 EEHg/L0.78 4/23/19SM21-22 6200B1Bromomethane
ND 5.0 4/24/19 15:55 EEHg/L1.9 4/23/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 4/24/19 15:55 EEHg/L0.21 4/23/19SM21-22 6200B1n-Butylbenzene
ND 0.50 4/24/19 15:55 EEHg/L0.16 4/23/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 4/24/19 15:55 EEHg/L0.17 4/23/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 4/24/19 15:55 EEHg/L0.11 4/23/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 4/24/19 15:55 EEHg/L0.15 4/23/19SM21-22 6200B1Chlorobenzene
ND 0.50 4/24/19 15:55 EEHg/L0.21 4/23/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 4/24/19 15:55 EEHg/L0.35 4/23/19SM21-22 6200B1Chloroethane
ND 0.50 4/24/19 15:55 EEHg/L0.17 4/23/19SM21-22 6200B1Chloroform
ND 0.60 4/24/19 15:55 EEHg/L0.45 4/23/19SM21-22 6200B1Chloromethane
ND 0.50 4/24/19 15:55 EEHg/L0.12 4/23/19SM21-22 6200B12-Chlorotoluene
ND 0.50 4/24/19 15:55 EEHg/L0.14 4/23/19SM21-22 6200B14-Chlorotoluene
ND 0.50 4/24/19 15:55 EEHg/L0.19 4/23/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/24/19 15:55 EEHg/L0.16 4/23/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 4/24/19 15:55 EEHg/L0.12 4/23/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 4/24/19 15:55 EEHg/L0.13 4/23/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 4/24/19 15:55 EEHg/L0.26 4/23/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/24/19 15:55 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 4/24/19 15:55 EEHg/L0.41 4/23/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 4/24/19 15:55 EEHg/L0.32 4/23/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 4/24/19 15:55 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/24/19 15:55 EEHg/L0.31 4/23/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/24/19 15:55 EEHg/L0.20 4/23/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 4/24/19 15:55 EEHg/L0.11 4/23/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 4/24/19 15:55 EEHg/L0.20 4/23/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 4/24/19 15:55 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 4/24/19 15:55 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 4/24/19 15:55 EEHg/L0.23 4/23/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 4/24/19 15:55 EEHg/L0.17 4/23/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 4/24/19 15:55 EEHg/L0.13 4/23/19SM21-22 6200B1Ethylbenzene
ND 5.0 4/24/19 15:55 EEHg/L1.5 4/23/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 4/24/19 15:55 EEHg/L0.17 4/23/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/24/19 15:55 EEHg/L0.20 4/23/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 4/24/19 15:55 EEHg/L0.25 4/23/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/24/19 15:55 EEHg/L0.34 4/23/19SM21-22 6200B1Methylene Chloride
ND 5.0 4/24/19 15:55 EEHg/L1.7 4/23/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 4/24/19 15:55 EEHg/L0.31 4/23/19SM21-22 6200B1Naphthalene
[TOC_1]Sample Results[TOC]
Page 10 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-01
Field Sample #: Field Blank
Sample Matrix: Field Blank
Sampled: 4/17/2019 17:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/24/19 15:55 EEHg/L0.13 4/23/19SM21-22 6200B1n-Propylbenzene
ND 0.50 4/24/19 15:55 EEHg/L0.11 4/23/19SM21-22 6200B1Styrene
ND 0.50 4/24/19 15:55 EEHg/L0.22 4/23/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/24/19 15:55 EEHg/L0.18 4/23/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 4/24/19 15:55 EEHg/L0.14 4/23/19SM21-22 6200B1Toluene
ND 5.0 4/24/19 15:55 EEHg/L0.57 4/23/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 4/24/19 15:55 EEHg/L0.40 4/23/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 4/24/19 15:55 EEHg/L0.20 4/23/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 4/24/19 15:55 EEHg/L0.16 4/23/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 4/24/19 15:55 EEHg/L0.24 4/23/19SM21-22 6200B1Trichloroethylene
ND 0.50 4/24/19 15:55 EEHg/L0.33 4/23/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/24/19 15:55 EEHg/L0.25 4/23/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 4/24/19 15:55 EEHg/L0.18 4/23/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 4/24/19 15:55 EEHg/L0.14 4/23/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 4/24/19 15:55 EEHg/L10 4/23/19SM21-22 6200B1Vinyl Acetate
ND 0.50 4/24/19 15:55 EEHg/L0.45 4/23/19SM21-22 6200B1Vinyl Chloride
ND 1.0 4/24/19 15:55 EEHg/L0.30 4/23/19SM21-22 6200B1m+p Xylene
ND 0.50 4/24/19 15:55 EEHg/L0.17 4/23/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 87.8 4/24/19 15:5570-130
Toluene-d8 100 4/24/19 15:5570-130
4-Bromofluorobenzene 99.9 4/24/19 15:5570-130
Page 11 of 65
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-02
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 4/17/2019 13:42
[TOC_2]19D1069-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 10000 4/25/19 0:31 EEHg/L760 4/23/19SM21-22 6200B200Acetone
7600 100 4/25/19 0:31 EEHg/L36 4/23/19SM21-22 6200B200Benzene
ND 100 4/25/19 0:31 EEHg/L30 4/23/19SM21-22 6200B200Bromobenzene
ND 100 4/25/19 0:31 EEHg/L64 4/23/19SM21-22 6200B200Bromochloromethane
ND 100 4/25/19 0:31 EEHg/L32 4/23/19SM21-22 6200B200Bromodichloromethane
ND 400 4/25/19 0:31 EEHg/L92 4/23/19SM21-22 6200B200Bromoform
ND 400 4/25/19 0:31 EEHg/L160 4/23/19SM21-22 6200B200Bromomethane
ND 1000 4/25/19 0:31 EEHg/L390 4/23/19SM21-22 6200B2002-Butanone (MEK)
ND 100 4/25/19 0:31 EEHg/L42 4/23/19SM21-22 6200B200n-Butylbenzene
ND 100 4/25/19 0:31 EEHg/L32 4/23/19SM21-22 6200B200sec-Butylbenzene
ND 100 4/25/19 0:31 EEHg/L34 4/23/19SM21-22 6200B200tert-Butylbenzene
ND 100 4/25/19 0:31 EEHg/L22 4/23/19SM21-22 6200B200Carbon Tetrachloride
ND 100 4/25/19 0:31 EEHg/L30 4/23/19SM21-22 6200B200Chlorobenzene
ND 100 4/25/19 0:31 EEHg/L42 4/23/19SM21-22 6200B200Chlorodibromomethane
ND 100 4/25/19 0:31 EEHg/L70 4/23/19SM21-22 6200B200Chloroethane
ND 100 4/25/19 0:31 EEHg/L34 4/23/19SM21-22 6200B200Chloroform
ND 120 4/25/19 0:31 EEHg/L90 4/23/19SM21-22 6200B200Chloromethane
ND 100 4/25/19 0:31 EEHg/L24 4/23/19SM21-22 6200B2002-Chlorotoluene
ND 100 4/25/19 0:31 EEHg/L28 4/23/19SM21-22 6200B2004-Chlorotoluene
78 100 4/25/19 0:31 EEHg/L38 4/23/19SM21-22 6200B200J1,2-Dibromoethane (EDB)
ND 100 4/25/19 0:31 EEHg/L32 4/23/19SM21-22 6200B2001,2-Dichlorobenzene
ND 100 4/25/19 0:31 EEHg/L24 4/23/19SM21-22 6200B2001,3-Dichlorobenzene
ND 100 4/25/19 0:31 EEHg/L26 4/23/19SM21-22 6200B2001,4-Dichlorobenzene
ND 100 4/25/19 0:31 EEHg/L52 4/23/19SM21-22 6200B200Dichlorodifluoromethane (Freon 12)
ND 100 4/25/19 0:31 EEHg/L32 4/23/19SM21-22 6200B2001,1-Dichloroethane
1000 100 4/25/19 0:31 EEHg/L82 4/23/19SM21-22 6200B2001,2-Dichloroethane
ND 100 4/25/19 0:31 EEHg/L64 4/23/19SM21-22 6200B2001,1-Dichloroethylene
ND 100 4/25/19 0:31 EEHg/L26 4/23/19SM21-22 6200B200cis-1,2-Dichloroethylene
ND 100 4/25/19 0:31 EEHg/L62 4/23/19SM21-22 6200B200trans-1,2-Dichloroethylene
ND 100 4/25/19 0:31 EEHg/L40 4/23/19SM21-22 6200B2001,2-Dichloropropane
ND 100 4/25/19 0:31 EEHg/L22 4/23/19SM21-22 6200B2001,3-Dichloropropane
ND 100 4/25/19 0:31 EEHg/L40 4/23/19SM21-22 6200B2002,2-Dichloropropane
ND 100 4/25/19 0:31 EEHg/L32 4/23/19SM21-22 6200B2001,1-Dichloropropene
ND 100 4/25/19 0:31 EEHg/L26 4/23/19SM21-22 6200B200cis-1,3-Dichloropropene
ND 100 4/25/19 0:31 EEHg/L46 4/23/19SM21-22 6200B200trans-1,3-Dichloropropene
400 100 4/25/19 0:31 EEHg/L34 4/23/19SM21-22 6200B200Diisopropyl Ether (DIPE)
890 100 4/25/19 0:31 EEHg/L26 4/23/19SM21-22 6200B200Ethylbenzene
ND 1000 4/25/19 0:31 EEHg/L300 4/23/19SM21-22 6200B2002-Hexanone (MBK)
52 100 4/25/19 0:31 EEHg/L34 4/23/19SM21-22 6200B200JIsopropylbenzene (Cumene)
ND 100 4/25/19 0:31 EEHg/L40 4/23/19SM21-22 6200B200p-Isopropyltoluene (p-Cymene)
13000 100 4/25/19 0:31 EEHg/L50 4/23/19SM21-22 6200B200Methyl tert-Butyl Ether (MTBE)
ND 1000 4/25/19 0:31 EEHg/L68 4/23/19SM21-22 6200B200Methylene Chloride
ND 1000 4/25/19 0:31 EEHg/L330 4/23/19SM21-22 6200B2004-Methyl-2-pentanone (MIBK)
560 1000 4/25/19 0:31 EEHg/L62 4/23/19SM21-22 6200B200JNaphthalene
Page 12 of 65
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-02
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 4/17/2019 13:42
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
110 100 4/25/19 0:31 EEHg/L26 4/23/19SM21-22 6200B200n-Propylbenzene
24 100 4/25/19 0:31 EEHg/L22 4/23/19SM21-22 6200B200JStyrene
ND 100 4/25/19 0:31 EEHg/L44 4/23/19SM21-22 6200B2001,1,2,2-Tetrachloroethane
ND 100 4/25/19 0:31 EEHg/L36 4/23/19SM21-22 6200B200Tetrachloroethylene
3400 100 4/25/19 0:31 EEHg/L28 4/23/19SM21-22 6200B200Toluene
ND 1000 4/25/19 0:31 EEHg/L110 4/23/19SM21-22 6200B2001,2,3-Trichlorobenzene
ND 400 4/25/19 0:31 EEHg/L80 4/23/19SM21-22 6200B2001,2,4-Trichlorobenzene
ND 100 4/25/19 0:31 EEHg/L40 4/23/19SM21-22 6200B2001,1,1-Trichloroethane
ND 100 4/25/19 0:31 EEHg/L32 4/23/19SM21-22 6200B2001,1,2-Trichloroethane
ND 100 4/25/19 0:31 EEHg/L48 4/23/19SM21-22 6200B200Trichloroethylene
ND 100 4/25/19 0:31 EEHg/L66 4/23/19SM21-22 6200B200Trichlorofluoromethane (Freon 11)
ND 100 4/25/19 0:31 EEHg/L50 4/23/19SM21-22 6200B2001,2,3-Trichloropropane
1100 100 4/25/19 0:31 EEHg/L36 4/23/19SM21-22 6200B2001,2,4-Trimethylbenzene
320 100 4/25/19 0:31 EEHg/L28 4/23/19SM21-22 6200B2001,3,5-Trimethylbenzene
ND 4000 4/25/19 0:31 EEHg/L2000 4/23/19SM21-22 6200B200Vinyl Acetate
ND 100 4/25/19 0:31 EEHg/L90 4/23/19SM21-22 6200B200Vinyl Chloride
3400 200 4/25/19 0:31 EEHg/L60 4/23/19SM21-22 6200B200m+p Xylene
2300 100 4/25/19 0:31 EEHg/L34 4/23/19SM21-22 6200B200o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.0 4/25/19 0:3170-130
Toluene-d8 98.2 4/25/19 0:3170-130
4-Bromofluorobenzene 98.8 4/25/19 0:3170-130
Page 13 of 65
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-03
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 4/17/2019 13:10
[TOC_2]19D1069-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/24/19 21:48 EEHg/L3.8 4/23/19SM21-22 6200B1Acetone
ND 0.50 4/24/19 21:48 EEHg/L0.18 4/23/19SM21-22 6200B1Benzene
ND 0.50 4/24/19 21:48 EEHg/L0.15 4/23/19SM21-22 6200B1Bromobenzene
ND 0.50 4/24/19 21:48 EEHg/L0.32 4/23/19SM21-22 6200B1Bromochloromethane
ND 0.50 4/24/19 21:48 EEHg/L0.16 4/23/19SM21-22 6200B1Bromodichloromethane
ND 2.0 4/24/19 21:48 EEHg/L0.46 4/23/19SM21-22 6200B1Bromoform
ND 2.0 4/24/19 21:48 EEHg/L0.78 4/23/19SM21-22 6200B1Bromomethane
ND 5.0 4/24/19 21:48 EEHg/L1.9 4/23/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 4/24/19 21:48 EEHg/L0.21 4/23/19SM21-22 6200B1n-Butylbenzene
ND 0.50 4/24/19 21:48 EEHg/L0.16 4/23/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 4/24/19 21:48 EEHg/L0.17 4/23/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 4/24/19 21:48 EEHg/L0.11 4/23/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 4/24/19 21:48 EEHg/L0.15 4/23/19SM21-22 6200B1Chlorobenzene
ND 0.50 4/24/19 21:48 EEHg/L0.21 4/23/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 4/24/19 21:48 EEHg/L0.35 4/23/19SM21-22 6200B1Chloroethane
ND 0.50 4/24/19 21:48 EEHg/L0.17 4/23/19SM21-22 6200B1Chloroform
ND 0.60 4/24/19 21:48 EEHg/L0.45 4/23/19SM21-22 6200B1Chloromethane
ND 0.50 4/24/19 21:48 EEHg/L0.12 4/23/19SM21-22 6200B12-Chlorotoluene
ND 0.50 4/24/19 21:48 EEHg/L0.14 4/23/19SM21-22 6200B14-Chlorotoluene
ND 0.50 4/24/19 21:48 EEHg/L0.19 4/23/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/24/19 21:48 EEHg/L0.16 4/23/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 4/24/19 21:48 EEHg/L0.12 4/23/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 4/24/19 21:48 EEHg/L0.13 4/23/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 4/24/19 21:48 EEHg/L0.26 4/23/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/24/19 21:48 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 4/24/19 21:48 EEHg/L0.41 4/23/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 4/24/19 21:48 EEHg/L0.32 4/23/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 4/24/19 21:48 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/24/19 21:48 EEHg/L0.31 4/23/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/24/19 21:48 EEHg/L0.20 4/23/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 4/24/19 21:48 EEHg/L0.11 4/23/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 4/24/19 21:48 EEHg/L0.20 4/23/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 4/24/19 21:48 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 4/24/19 21:48 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 4/24/19 21:48 EEHg/L0.23 4/23/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 4/24/19 21:48 EEHg/L0.17 4/23/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 4/24/19 21:48 EEHg/L0.13 4/23/19SM21-22 6200B1Ethylbenzene
ND 5.0 4/24/19 21:48 EEHg/L1.5 4/23/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 4/24/19 21:48 EEHg/L0.17 4/23/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/24/19 21:48 EEHg/L0.20 4/23/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 4/24/19 21:48 EEHg/L0.25 4/23/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/24/19 21:48 EEHg/L0.34 4/23/19SM21-22 6200B1Methylene Chloride
ND 5.0 4/24/19 21:48 EEHg/L1.7 4/23/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 4/24/19 21:48 EEHg/L0.31 4/23/19SM21-22 6200B1Naphthalene
Page 14 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-03
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 4/17/2019 13:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/24/19 21:48 EEHg/L0.13 4/23/19SM21-22 6200B1n-Propylbenzene
ND 0.50 4/24/19 21:48 EEHg/L0.11 4/23/19SM21-22 6200B1Styrene
ND 0.50 4/24/19 21:48 EEHg/L0.22 4/23/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/24/19 21:48 EEHg/L0.18 4/23/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 4/24/19 21:48 EEHg/L0.14 4/23/19SM21-22 6200B1Toluene
ND 5.0 4/24/19 21:48 EEHg/L0.57 4/23/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 4/24/19 21:48 EEHg/L0.40 4/23/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 4/24/19 21:48 EEHg/L0.20 4/23/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 4/24/19 21:48 EEHg/L0.16 4/23/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 4/24/19 21:48 EEHg/L0.24 4/23/19SM21-22 6200B1Trichloroethylene
ND 0.50 4/24/19 21:48 EEHg/L0.33 4/23/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/24/19 21:48 EEHg/L0.25 4/23/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 4/24/19 21:48 EEHg/L0.18 4/23/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 4/24/19 21:48 EEHg/L0.14 4/23/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 4/24/19 21:48 EEHg/L10 4/23/19SM21-22 6200B1Vinyl Acetate
ND 0.50 4/24/19 21:48 EEHg/L0.45 4/23/19SM21-22 6200B1Vinyl Chloride
ND 1.0 4/24/19 21:48 EEHg/L0.30 4/23/19SM21-22 6200B1m+p Xylene
ND 0.50 4/24/19 21:48 EEHg/L0.17 4/23/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.0 4/24/19 21:4870-130
Toluene-d8 98.8 4/24/19 21:4870-130
4-Bromofluorobenzene 99.8 4/24/19 21:4870-130
Page 15 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-04
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 4/17/2019 16:05
[TOC_2]19D1069-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 5000 4/25/19 0:03 EEHg/L380 4/23/19SM21-22 6200B100Acetone
1400 50 4/25/19 0:03 EEHg/L18 4/23/19SM21-22 6200B100Benzene
ND 50 4/25/19 0:03 EEHg/L15 4/23/19SM21-22 6200B100Bromobenzene
ND 50 4/25/19 0:03 EEHg/L32 4/23/19SM21-22 6200B100Bromochloromethane
ND 50 4/25/19 0:03 EEHg/L16 4/23/19SM21-22 6200B100Bromodichloromethane
ND 200 4/25/19 0:03 EEHg/L46 4/23/19SM21-22 6200B100Bromoform
ND 200 4/25/19 0:03 EEHg/L78 4/23/19SM21-22 6200B100Bromomethane
ND 500 4/25/19 0:03 EEHg/L190 4/23/19SM21-22 6200B1002-Butanone (MEK)
ND 50 4/25/19 0:03 EEHg/L21 4/23/19SM21-22 6200B100n-Butylbenzene
ND 50 4/25/19 0:03 EEHg/L16 4/23/19SM21-22 6200B100sec-Butylbenzene
ND 50 4/25/19 0:03 EEHg/L17 4/23/19SM21-22 6200B100tert-Butylbenzene
ND 50 4/25/19 0:03 EEHg/L11 4/23/19SM21-22 6200B100Carbon Tetrachloride
ND 50 4/25/19 0:03 EEHg/L15 4/23/19SM21-22 6200B100Chlorobenzene
ND 50 4/25/19 0:03 EEHg/L21 4/23/19SM21-22 6200B100Chlorodibromomethane
ND 50 4/25/19 0:03 EEHg/L35 4/23/19SM21-22 6200B100Chloroethane
ND 50 4/25/19 0:03 EEHg/L17 4/23/19SM21-22 6200B100Chloroform
ND 60 4/25/19 0:03 EEHg/L45 4/23/19SM21-22 6200B100Chloromethane
ND 50 4/25/19 0:03 EEHg/L12 4/23/19SM21-22 6200B1002-Chlorotoluene
ND 50 4/25/19 0:03 EEHg/L14 4/23/19SM21-22 6200B1004-Chlorotoluene
ND 50 4/25/19 0:03 EEHg/L19 4/23/19SM21-22 6200B1001,2-Dibromoethane (EDB)
ND 50 4/25/19 0:03 EEHg/L16 4/23/19SM21-22 6200B1001,2-Dichlorobenzene
ND 50 4/25/19 0:03 EEHg/L12 4/23/19SM21-22 6200B1001,3-Dichlorobenzene
ND 50 4/25/19 0:03 EEHg/L13 4/23/19SM21-22 6200B1001,4-Dichlorobenzene
ND 50 4/25/19 0:03 EEHg/L26 4/23/19SM21-22 6200B100Dichlorodifluoromethane (Freon 12)
ND 50 4/25/19 0:03 EEHg/L16 4/23/19SM21-22 6200B1001,1-Dichloroethane
ND 50 4/25/19 0:03 EEHg/L41 4/23/19SM21-22 6200B1001,2-Dichloroethane
ND 50 4/25/19 0:03 EEHg/L32 4/23/19SM21-22 6200B1001,1-Dichloroethylene
ND 50 4/25/19 0:03 EEHg/L13 4/23/19SM21-22 6200B100cis-1,2-Dichloroethylene
ND 50 4/25/19 0:03 EEHg/L31 4/23/19SM21-22 6200B100trans-1,2-Dichloroethylene
ND 50 4/25/19 0:03 EEHg/L20 4/23/19SM21-22 6200B1001,2-Dichloropropane
ND 50 4/25/19 0:03 EEHg/L11 4/23/19SM21-22 6200B1001,3-Dichloropropane
ND 50 4/25/19 0:03 EEHg/L20 4/23/19SM21-22 6200B1002,2-Dichloropropane
ND 50 4/25/19 0:03 EEHg/L16 4/23/19SM21-22 6200B1001,1-Dichloropropene
ND 50 4/25/19 0:03 EEHg/L13 4/23/19SM21-22 6200B100cis-1,3-Dichloropropene
ND 50 4/25/19 0:03 EEHg/L23 4/23/19SM21-22 6200B100trans-1,3-Dichloropropene
190 50 4/25/19 0:03 EEHg/L17 4/23/19SM21-22 6200B100Diisopropyl Ether (DIPE)
80 50 4/25/19 0:03 EEHg/L13 4/23/19SM21-22 6200B100Ethylbenzene
ND 500 4/25/19 0:03 EEHg/L150 4/23/19SM21-22 6200B1002-Hexanone (MBK)
ND 50 4/25/19 0:03 EEHg/L17 4/23/19SM21-22 6200B100Isopropylbenzene (Cumene)
ND 50 4/25/19 0:03 EEHg/L20 4/23/19SM21-22 6200B100p-Isopropyltoluene (p-Cymene)
6200 50 4/25/19 0:03 EEHg/L25 4/23/19SM21-22 6200B100Methyl tert-Butyl Ether (MTBE)
ND 500 4/25/19 0:03 EEHg/L34 4/23/19SM21-22 6200B100Methylene Chloride
ND 500 4/25/19 0:03 EEHg/L170 4/23/19SM21-22 6200B1004-Methyl-2-pentanone (MIBK)
ND 500 4/25/19 0:03 EEHg/L31 4/23/19SM21-22 6200B100Naphthalene
Page 16 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-04
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 4/17/2019 16:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 50 4/25/19 0:03 EEHg/L13 4/23/19SM21-22 6200B100n-Propylbenzene
ND 50 4/25/19 0:03 EEHg/L11 4/23/19SM21-22 6200B100Styrene
ND 50 4/25/19 0:03 EEHg/L22 4/23/19SM21-22 6200B1001,1,2,2-Tetrachloroethane
ND 50 4/25/19 0:03 EEHg/L18 4/23/19SM21-22 6200B100Tetrachloroethylene
460 50 4/25/19 0:03 EEHg/L14 4/23/19SM21-22 6200B100Toluene
ND 500 4/25/19 0:03 EEHg/L57 4/23/19SM21-22 6200B1001,2,3-Trichlorobenzene
ND 200 4/25/19 0:03 EEHg/L40 4/23/19SM21-22 6200B1001,2,4-Trichlorobenzene
ND 50 4/25/19 0:03 EEHg/L20 4/23/19SM21-22 6200B1001,1,1-Trichloroethane
ND 50 4/25/19 0:03 EEHg/L16 4/23/19SM21-22 6200B1001,1,2-Trichloroethane
ND 50 4/25/19 0:03 EEHg/L24 4/23/19SM21-22 6200B100Trichloroethylene
ND 50 4/25/19 0:03 EEHg/L33 4/23/19SM21-22 6200B100Trichlorofluoromethane (Freon 11)
ND 50 4/25/19 0:03 EEHg/L25 4/23/19SM21-22 6200B1001,2,3-Trichloropropane
62 50 4/25/19 0:03 EEHg/L18 4/23/19SM21-22 6200B1001,2,4-Trimethylbenzene
26 50 4/25/19 0:03 EEHg/L14 4/23/19SM21-22 6200B100J1,3,5-Trimethylbenzene
ND 2000 4/25/19 0:03 EEHg/L1000 4/23/19SM21-22 6200B100Vinyl Acetate
ND 50 4/25/19 0:03 EEHg/L45 4/23/19SM21-22 6200B100Vinyl Chloride
240 100 4/25/19 0:03 EEHg/L30 4/23/19SM21-22 6200B100m+p Xylene
220 50 4/25/19 0:03 EEHg/L17 4/23/19SM21-22 6200B100o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.7 4/25/19 0:0370-130
Toluene-d8 97.8 4/25/19 0:0370-130
4-Bromofluorobenzene 100 4/25/19 0:0370-130
Page 17 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-05
Field Sample #: MW-8
Sample Matrix: Ground Water
Sampled: 4/17/2019 12:23
[TOC_2]19D1069-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/24/19 22:15 EEHg/L3.8 4/23/19SM21-22 6200B1Acetone
ND 0.50 4/24/19 22:15 EEHg/L0.18 4/23/19SM21-22 6200B1Benzene
ND 0.50 4/24/19 22:15 EEHg/L0.15 4/23/19SM21-22 6200B1Bromobenzene
ND 0.50 4/24/19 22:15 EEHg/L0.32 4/23/19SM21-22 6200B1Bromochloromethane
ND 0.50 4/24/19 22:15 EEHg/L0.16 4/23/19SM21-22 6200B1Bromodichloromethane
ND 2.0 4/24/19 22:15 EEHg/L0.46 4/23/19SM21-22 6200B1Bromoform
ND 2.0 4/24/19 22:15 EEHg/L0.78 4/23/19SM21-22 6200B1Bromomethane
ND 5.0 4/24/19 22:15 EEHg/L1.9 4/23/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 4/24/19 22:15 EEHg/L0.21 4/23/19SM21-22 6200B1n-Butylbenzene
ND 0.50 4/24/19 22:15 EEHg/L0.16 4/23/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 4/24/19 22:15 EEHg/L0.17 4/23/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 4/24/19 22:15 EEHg/L0.11 4/23/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 4/24/19 22:15 EEHg/L0.15 4/23/19SM21-22 6200B1Chlorobenzene
ND 0.50 4/24/19 22:15 EEHg/L0.21 4/23/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 4/24/19 22:15 EEHg/L0.35 4/23/19SM21-22 6200B1Chloroethane
ND 0.50 4/24/19 22:15 EEHg/L0.17 4/23/19SM21-22 6200B1Chloroform
ND 0.60 4/24/19 22:15 EEHg/L0.45 4/23/19SM21-22 6200B1Chloromethane
ND 0.50 4/24/19 22:15 EEHg/L0.12 4/23/19SM21-22 6200B12-Chlorotoluene
ND 0.50 4/24/19 22:15 EEHg/L0.14 4/23/19SM21-22 6200B14-Chlorotoluene
ND 0.50 4/24/19 22:15 EEHg/L0.19 4/23/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/24/19 22:15 EEHg/L0.16 4/23/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 4/24/19 22:15 EEHg/L0.12 4/23/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 4/24/19 22:15 EEHg/L0.13 4/23/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 4/24/19 22:15 EEHg/L0.26 4/23/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/24/19 22:15 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloroethane
6.9 0.50 4/24/19 22:15 EEHg/L0.41 4/23/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 4/24/19 22:15 EEHg/L0.32 4/23/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 4/24/19 22:15 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/24/19 22:15 EEHg/L0.31 4/23/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/24/19 22:15 EEHg/L0.20 4/23/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 4/24/19 22:15 EEHg/L0.11 4/23/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 4/24/19 22:15 EEHg/L0.20 4/23/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 4/24/19 22:15 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 4/24/19 22:15 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 4/24/19 22:15 EEHg/L0.23 4/23/19SM21-22 6200B1trans-1,3-Dichloropropene
8.9 0.50 4/24/19 22:15 EEHg/L0.17 4/23/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 4/24/19 22:15 EEHg/L0.13 4/23/19SM21-22 6200B1Ethylbenzene
ND 5.0 4/24/19 22:15 EEHg/L1.5 4/23/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 4/24/19 22:15 EEHg/L0.17 4/23/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/24/19 22:15 EEHg/L0.20 4/23/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
270 12 4/26/19 20:57 EEHg/L6.2 4/26/19SM21-22 6200B25Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/24/19 22:15 EEHg/L0.34 4/23/19SM21-22 6200B1Methylene Chloride
ND 5.0 4/24/19 22:15 EEHg/L1.7 4/23/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 4/24/19 22:15 EEHg/L0.31 4/23/19SM21-22 6200B1Naphthalene
Page 18 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-05
Field Sample #: MW-8
Sample Matrix: Ground Water
Sampled: 4/17/2019 12:23
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/24/19 22:15 EEHg/L0.13 4/23/19SM21-22 6200B1n-Propylbenzene
ND 0.50 4/24/19 22:15 EEHg/L0.11 4/23/19SM21-22 6200B1Styrene
ND 0.50 4/24/19 22:15 EEHg/L0.22 4/23/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/24/19 22:15 EEHg/L0.18 4/23/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 4/24/19 22:15 EEHg/L0.14 4/23/19SM21-22 6200B1Toluene
ND 5.0 4/24/19 22:15 EEHg/L0.57 4/23/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 4/24/19 22:15 EEHg/L0.40 4/23/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 4/24/19 22:15 EEHg/L0.20 4/23/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 4/24/19 22:15 EEHg/L0.16 4/23/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 4/24/19 22:15 EEHg/L0.24 4/23/19SM21-22 6200B1Trichloroethylene
ND 0.50 4/24/19 22:15 EEHg/L0.33 4/23/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/24/19 22:15 EEHg/L0.25 4/23/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 4/24/19 22:15 EEHg/L0.18 4/23/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 4/24/19 22:15 EEHg/L0.14 4/23/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 4/24/19 22:15 EEHg/L10 4/23/19SM21-22 6200B1Vinyl Acetate
ND 0.50 4/24/19 22:15 EEHg/L0.45 4/23/19SM21-22 6200B1Vinyl Chloride
ND 1.0 4/24/19 22:15 EEHg/L0.30 4/23/19SM21-22 6200B1m+p Xylene
ND 0.50 4/24/19 22:15 EEHg/L0.17 4/23/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.7 4/24/19 22:1570-130
1,2-Dichloroethane-d4 89.6 4/26/19 20:5770-130
Toluene-d8 98.8 4/24/19 22:1570-130
Toluene-d8 98.9 4/26/19 20:5770-130
4-Bromofluorobenzene 97.7 4/24/19 22:1570-130
4-Bromofluorobenzene 97.2 4/26/19 20:5770-130
Page 19 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-06
Field Sample #: MW-9
Sample Matrix: Ground Water
Sampled: 4/17/2019 10:45
[TOC_2]19D1069-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/24/19 22:42 EEHg/L3.8 4/23/19SM21-22 6200B1Acetone
ND 0.50 4/24/19 22:42 EEHg/L0.18 4/23/19SM21-22 6200B1Benzene
ND 0.50 4/24/19 22:42 EEHg/L0.15 4/23/19SM21-22 6200B1Bromobenzene
ND 0.50 4/24/19 22:42 EEHg/L0.32 4/23/19SM21-22 6200B1Bromochloromethane
ND 0.50 4/24/19 22:42 EEHg/L0.16 4/23/19SM21-22 6200B1Bromodichloromethane
ND 2.0 4/24/19 22:42 EEHg/L0.46 4/23/19SM21-22 6200B1Bromoform
ND 2.0 4/24/19 22:42 EEHg/L0.78 4/23/19SM21-22 6200B1Bromomethane
ND 5.0 4/24/19 22:42 EEHg/L1.9 4/23/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 4/24/19 22:42 EEHg/L0.21 4/23/19SM21-22 6200B1n-Butylbenzene
ND 0.50 4/24/19 22:42 EEHg/L0.16 4/23/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 4/24/19 22:42 EEHg/L0.17 4/23/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 4/24/19 22:42 EEHg/L0.11 4/23/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 4/24/19 22:42 EEHg/L0.15 4/23/19SM21-22 6200B1Chlorobenzene
ND 0.50 4/24/19 22:42 EEHg/L0.21 4/23/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 4/24/19 22:42 EEHg/L0.35 4/23/19SM21-22 6200B1Chloroethane
ND 0.50 4/24/19 22:42 EEHg/L0.17 4/23/19SM21-22 6200B1Chloroform
ND 0.60 4/24/19 22:42 EEHg/L0.45 4/23/19SM21-22 6200B1Chloromethane
ND 0.50 4/24/19 22:42 EEHg/L0.12 4/23/19SM21-22 6200B12-Chlorotoluene
ND 0.50 4/24/19 22:42 EEHg/L0.14 4/23/19SM21-22 6200B14-Chlorotoluene
ND 0.50 4/24/19 22:42 EEHg/L0.19 4/23/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/24/19 22:42 EEHg/L0.16 4/23/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 4/24/19 22:42 EEHg/L0.12 4/23/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 4/24/19 22:42 EEHg/L0.13 4/23/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 4/24/19 22:42 EEHg/L0.26 4/23/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/24/19 22:42 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 4/24/19 22:42 EEHg/L0.41 4/23/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 4/24/19 22:42 EEHg/L0.32 4/23/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 4/24/19 22:42 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/24/19 22:42 EEHg/L0.31 4/23/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/24/19 22:42 EEHg/L0.20 4/23/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 4/24/19 22:42 EEHg/L0.11 4/23/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 4/24/19 22:42 EEHg/L0.20 4/23/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 4/24/19 22:42 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 4/24/19 22:42 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 4/24/19 22:42 EEHg/L0.23 4/23/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 4/24/19 22:42 EEHg/L0.17 4/23/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 4/24/19 22:42 EEHg/L0.13 4/23/19SM21-22 6200B1Ethylbenzene
ND 5.0 4/24/19 22:42 EEHg/L1.5 4/23/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 4/24/19 22:42 EEHg/L0.17 4/23/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/24/19 22:42 EEHg/L0.20 4/23/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 4/24/19 22:42 EEHg/L0.25 4/23/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/24/19 22:42 EEHg/L0.34 4/23/19SM21-22 6200B1Methylene Chloride
ND 5.0 4/24/19 22:42 EEHg/L1.7 4/23/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 4/24/19 22:42 EEHg/L0.31 4/23/19SM21-22 6200B1Naphthalene
Page 20 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-06
Field Sample #: MW-9
Sample Matrix: Ground Water
Sampled: 4/17/2019 10:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/24/19 22:42 EEHg/L0.13 4/23/19SM21-22 6200B1n-Propylbenzene
ND 0.50 4/24/19 22:42 EEHg/L0.11 4/23/19SM21-22 6200B1Styrene
ND 0.50 4/24/19 22:42 EEHg/L0.22 4/23/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/24/19 22:42 EEHg/L0.18 4/23/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 4/24/19 22:42 EEHg/L0.14 4/23/19SM21-22 6200B1Toluene
ND 5.0 4/24/19 22:42 EEHg/L0.57 4/23/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 4/24/19 22:42 EEHg/L0.40 4/23/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 4/24/19 22:42 EEHg/L0.20 4/23/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 4/24/19 22:42 EEHg/L0.16 4/23/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 4/24/19 22:42 EEHg/L0.24 4/23/19SM21-22 6200B1Trichloroethylene
ND 0.50 4/24/19 22:42 EEHg/L0.33 4/23/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/24/19 22:42 EEHg/L0.25 4/23/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 4/24/19 22:42 EEHg/L0.18 4/23/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 4/24/19 22:42 EEHg/L0.14 4/23/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 4/24/19 22:42 EEHg/L10 4/23/19SM21-22 6200B1Vinyl Acetate
ND 0.50 4/24/19 22:42 EEHg/L0.45 4/23/19SM21-22 6200B1Vinyl Chloride
ND 1.0 4/24/19 22:42 EEHg/L0.30 4/23/19SM21-22 6200B1m+p Xylene
ND 0.50 4/24/19 22:42 EEHg/L0.17 4/23/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.3 4/24/19 22:4270-130
Toluene-d8 99.3 4/24/19 22:4270-130
4-Bromofluorobenzene 98.5 4/24/19 22:4270-130
Page 21 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-07
Field Sample #: MW-10
Sample Matrix: Ground Water
Sampled: 4/17/2019 11:30
[TOC_2]19D1069-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/24/19 23:09 EEHg/L3.8 4/23/19SM21-22 6200B1Acetone
ND 0.50 4/24/19 23:09 EEHg/L0.18 4/23/19SM21-22 6200B1Benzene
ND 0.50 4/24/19 23:09 EEHg/L0.15 4/23/19SM21-22 6200B1Bromobenzene
ND 0.50 4/24/19 23:09 EEHg/L0.32 4/23/19SM21-22 6200B1Bromochloromethane
ND 0.50 4/24/19 23:09 EEHg/L0.16 4/23/19SM21-22 6200B1Bromodichloromethane
ND 2.0 4/24/19 23:09 EEHg/L0.46 4/23/19SM21-22 6200B1Bromoform
ND 2.0 4/24/19 23:09 EEHg/L0.78 4/23/19SM21-22 6200B1Bromomethane
ND 5.0 4/24/19 23:09 EEHg/L1.9 4/23/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 4/24/19 23:09 EEHg/L0.21 4/23/19SM21-22 6200B1n-Butylbenzene
ND 0.50 4/24/19 23:09 EEHg/L0.16 4/23/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 4/24/19 23:09 EEHg/L0.17 4/23/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 4/24/19 23:09 EEHg/L0.11 4/23/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 4/24/19 23:09 EEHg/L0.15 4/23/19SM21-22 6200B1Chlorobenzene
ND 0.50 4/24/19 23:09 EEHg/L0.21 4/23/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 4/24/19 23:09 EEHg/L0.35 4/23/19SM21-22 6200B1Chloroethane
ND 0.50 4/24/19 23:09 EEHg/L0.17 4/23/19SM21-22 6200B1Chloroform
ND 0.60 4/24/19 23:09 EEHg/L0.45 4/23/19SM21-22 6200B1Chloromethane
ND 0.50 4/24/19 23:09 EEHg/L0.12 4/23/19SM21-22 6200B12-Chlorotoluene
ND 0.50 4/24/19 23:09 EEHg/L0.14 4/23/19SM21-22 6200B14-Chlorotoluene
ND 0.50 4/24/19 23:09 EEHg/L0.19 4/23/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/24/19 23:09 EEHg/L0.16 4/23/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 4/24/19 23:09 EEHg/L0.12 4/23/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 4/24/19 23:09 EEHg/L0.13 4/23/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 4/24/19 23:09 EEHg/L0.26 4/23/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/24/19 23:09 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 4/24/19 23:09 EEHg/L0.41 4/23/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 4/24/19 23:09 EEHg/L0.32 4/23/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 4/24/19 23:09 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/24/19 23:09 EEHg/L0.31 4/23/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/24/19 23:09 EEHg/L0.20 4/23/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 4/24/19 23:09 EEHg/L0.11 4/23/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 4/24/19 23:09 EEHg/L0.20 4/23/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 4/24/19 23:09 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 4/24/19 23:09 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 4/24/19 23:09 EEHg/L0.23 4/23/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 4/24/19 23:09 EEHg/L0.17 4/23/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 4/24/19 23:09 EEHg/L0.13 4/23/19SM21-22 6200B1Ethylbenzene
ND 5.0 4/24/19 23:09 EEHg/L1.5 4/23/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 4/24/19 23:09 EEHg/L0.17 4/23/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/24/19 23:09 EEHg/L0.20 4/23/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 4/24/19 23:09 EEHg/L0.25 4/23/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/24/19 23:09 EEHg/L0.34 4/23/19SM21-22 6200B1Methylene Chloride
ND 5.0 4/24/19 23:09 EEHg/L1.7 4/23/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 4/24/19 23:09 EEHg/L0.31 4/23/19SM21-22 6200B1Naphthalene
Page 22 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-07
Field Sample #: MW-10
Sample Matrix: Ground Water
Sampled: 4/17/2019 11:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/24/19 23:09 EEHg/L0.13 4/23/19SM21-22 6200B1n-Propylbenzene
ND 0.50 4/24/19 23:09 EEHg/L0.11 4/23/19SM21-22 6200B1Styrene
ND 0.50 4/24/19 23:09 EEHg/L0.22 4/23/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/24/19 23:09 EEHg/L0.18 4/23/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 4/24/19 23:09 EEHg/L0.14 4/23/19SM21-22 6200B1Toluene
ND 5.0 4/24/19 23:09 EEHg/L0.57 4/23/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 4/24/19 23:09 EEHg/L0.40 4/23/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 4/24/19 23:09 EEHg/L0.20 4/23/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 4/24/19 23:09 EEHg/L0.16 4/23/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 4/24/19 23:09 EEHg/L0.24 4/23/19SM21-22 6200B1Trichloroethylene
ND 0.50 4/24/19 23:09 EEHg/L0.33 4/23/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/24/19 23:09 EEHg/L0.25 4/23/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 4/24/19 23:09 EEHg/L0.18 4/23/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 4/24/19 23:09 EEHg/L0.14 4/23/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 4/24/19 23:09 EEHg/L10 4/23/19SM21-22 6200B1Vinyl Acetate
ND 0.50 4/24/19 23:09 EEHg/L0.45 4/23/19SM21-22 6200B1Vinyl Chloride
ND 1.0 4/24/19 23:09 EEHg/L0.30 4/23/19SM21-22 6200B1m+p Xylene
ND 0.50 4/24/19 23:09 EEHg/L0.17 4/23/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.2 4/24/19 23:0970-130
Toluene-d8 99.1 4/24/19 23:0970-130
4-Bromofluorobenzene 100 4/24/19 23:0970-130
Page 23 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-08
Field Sample #: MW-11
Sample Matrix: Ground Water
Sampled: 4/17/2019 16:52
[TOC_2]19D1069-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 25000 4/25/19 0:58 EEHg/L1900 4/23/19SM21-22 6200B500Acetone
29000 250 4/25/19 0:58 EEHg/L90 4/23/19SM21-22 6200B500Benzene
ND 250 4/25/19 0:58 EEHg/L75 4/23/19SM21-22 6200B500Bromobenzene
ND 250 4/25/19 0:58 EEHg/L160 4/23/19SM21-22 6200B500Bromochloromethane
ND 250 4/25/19 0:58 EEHg/L80 4/23/19SM21-22 6200B500Bromodichloromethane
ND 1000 4/25/19 0:58 EEHg/L230 4/23/19SM21-22 6200B500Bromoform
ND 1000 4/25/19 0:58 EEHg/L390 4/23/19SM21-22 6200B500Bromomethane
ND 2500 4/25/19 0:58 EEHg/L970 4/23/19SM21-22 6200B5002-Butanone (MEK)
ND 250 4/25/19 0:58 EEHg/L100 4/23/19SM21-22 6200B500n-Butylbenzene
ND 250 4/25/19 0:58 EEHg/L80 4/23/19SM21-22 6200B500sec-Butylbenzene
ND 250 4/25/19 0:58 EEHg/L85 4/23/19SM21-22 6200B500tert-Butylbenzene
ND 250 4/25/19 0:58 EEHg/L55 4/23/19SM21-22 6200B500Carbon Tetrachloride
ND 250 4/25/19 0:58 EEHg/L75 4/23/19SM21-22 6200B500Chlorobenzene
ND 250 4/25/19 0:58 EEHg/L100 4/23/19SM21-22 6200B500Chlorodibromomethane
ND 250 4/25/19 0:58 EEHg/L180 4/23/19SM21-22 6200B500Chloroethane
ND 250 4/25/19 0:58 EEHg/L85 4/23/19SM21-22 6200B500Chloroform
ND 300 4/25/19 0:58 EEHg/L220 4/23/19SM21-22 6200B500Chloromethane
ND 250 4/25/19 0:58 EEHg/L60 4/23/19SM21-22 6200B5002-Chlorotoluene
ND 250 4/25/19 0:58 EEHg/L70 4/23/19SM21-22 6200B5004-Chlorotoluene
620 250 4/25/19 0:58 EEHg/L95 4/23/19SM21-22 6200B5001,2-Dibromoethane (EDB)
ND 250 4/25/19 0:58 EEHg/L80 4/23/19SM21-22 6200B5001,2-Dichlorobenzene
ND 250 4/25/19 0:58 EEHg/L60 4/23/19SM21-22 6200B5001,3-Dichlorobenzene
ND 250 4/25/19 0:58 EEHg/L65 4/23/19SM21-22 6200B5001,4-Dichlorobenzene
ND 250 4/25/19 0:58 EEHg/L130 4/23/19SM21-22 6200B500Dichlorodifluoromethane (Freon 12)
ND 250 4/25/19 0:58 EEHg/L80 4/23/19SM21-22 6200B5001,1-Dichloroethane
1600 250 4/25/19 0:58 EEHg/L200 4/23/19SM21-22 6200B5001,2-Dichloroethane
ND 250 4/25/19 0:58 EEHg/L160 4/23/19SM21-22 6200B5001,1-Dichloroethylene
ND 250 4/25/19 0:58 EEHg/L65 4/23/19SM21-22 6200B500cis-1,2-Dichloroethylene
ND 250 4/25/19 0:58 EEHg/L160 4/23/19SM21-22 6200B500trans-1,2-Dichloroethylene
ND 250 4/25/19 0:58 EEHg/L100 4/23/19SM21-22 6200B5001,2-Dichloropropane
ND 250 4/25/19 0:58 EEHg/L55 4/23/19SM21-22 6200B5001,3-Dichloropropane
ND 250 4/25/19 0:58 EEHg/L100 4/23/19SM21-22 6200B5002,2-Dichloropropane
ND 250 4/25/19 0:58 EEHg/L80 4/23/19SM21-22 6200B5001,1-Dichloropropene
ND 250 4/25/19 0:58 EEHg/L65 4/23/19SM21-22 6200B500cis-1,3-Dichloropropene
ND 250 4/25/19 0:58 EEHg/L120 4/23/19SM21-22 6200B500trans-1,3-Dichloropropene
280 250 4/25/19 0:58 EEHg/L85 4/23/19SM21-22 6200B500Diisopropyl Ether (DIPE)
1600 250 4/25/19 0:58 EEHg/L65 4/23/19SM21-22 6200B500Ethylbenzene
ND 2500 4/25/19 0:58 EEHg/L760 4/23/19SM21-22 6200B5002-Hexanone (MBK)
120 250 4/25/19 0:58 EEHg/L85 4/23/19SM21-22 6200B500JIsopropylbenzene (Cumene)
ND 250 4/25/19 0:58 EEHg/L100 4/23/19SM21-22 6200B500p-Isopropyltoluene (p-Cymene)
2900 250 4/25/19 0:58 EEHg/L120 4/23/19SM21-22 6200B500Methyl tert-Butyl Ether (MTBE)
ND 2500 4/25/19 0:58 EEHg/L170 4/23/19SM21-22 6200B500Methylene Chloride
ND 2500 4/25/19 0:58 EEHg/L840 4/23/19SM21-22 6200B5004-Methyl-2-pentanone (MIBK)
1500 2500 4/25/19 0:58 EEHg/L160 4/23/19SM21-22 6200B500JNaphthalene
Page 24 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-08
Field Sample #: MW-11
Sample Matrix: Ground Water
Sampled: 4/17/2019 16:52
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
320 250 4/25/19 0:58 EEHg/L65 4/23/19SM21-22 6200B500n-Propylbenzene
ND 250 4/25/19 0:58 EEHg/L55 4/23/19SM21-22 6200B500Styrene
ND 250 4/25/19 0:58 EEHg/L110 4/23/19SM21-22 6200B5001,1,2,2-Tetrachloroethane
ND 250 4/25/19 0:58 EEHg/L90 4/23/19SM21-22 6200B500Tetrachloroethylene
18000 250 4/25/19 0:58 EEHg/L70 4/23/19SM21-22 6200B500Toluene
ND 2500 4/25/19 0:58 EEHg/L280 4/23/19SM21-22 6200B5001,2,3-Trichlorobenzene
ND 1000 4/25/19 0:58 EEHg/L200 4/23/19SM21-22 6200B5001,2,4-Trichlorobenzene
ND 250 4/25/19 0:58 EEHg/L100 4/23/19SM21-22 6200B5001,1,1-Trichloroethane
ND 250 4/25/19 0:58 EEHg/L80 4/23/19SM21-22 6200B5001,1,2-Trichloroethane
ND 250 4/25/19 0:58 EEHg/L120 4/23/19SM21-22 6200B500Trichloroethylene
ND 250 4/25/19 0:58 EEHg/L160 4/23/19SM21-22 6200B500Trichlorofluoromethane (Freon 11)
ND 250 4/25/19 0:58 EEHg/L120 4/23/19SM21-22 6200B5001,2,3-Trichloropropane
2200 250 4/25/19 0:58 EEHg/L90 4/23/19SM21-22 6200B5001,2,4-Trimethylbenzene
560 250 4/25/19 0:58 EEHg/L70 4/23/19SM21-22 6200B5001,3,5-Trimethylbenzene
ND 10000 4/25/19 0:58 EEHg/L5100 4/23/19SM21-22 6200B500Vinyl Acetate
ND 250 4/25/19 0:58 EEHg/L220 4/23/19SM21-22 6200B500Vinyl Chloride
6400 500 4/25/19 0:58 EEHg/L150 4/23/19SM21-22 6200B500m+p Xylene
5300 250 4/25/19 0:58 EEHg/L85 4/23/19SM21-22 6200B500o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 92.2 4/25/19 0:5870-130
Toluene-d8 96.5 4/25/19 0:5870-130
4-Bromofluorobenzene 99.1 4/25/19 0:5870-130
Page 25 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-09
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 4/17/2019 17:00
[TOC_2]19D1069-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/24/19 23:36 EEHg/L3.8 4/23/19SM21-22 6200B1Acetone
ND 0.50 4/24/19 23:36 EEHg/L0.18 4/23/19SM21-22 6200B1Benzene
ND 0.50 4/24/19 23:36 EEHg/L0.15 4/23/19SM21-22 6200B1Bromobenzene
ND 0.50 4/24/19 23:36 EEHg/L0.32 4/23/19SM21-22 6200B1Bromochloromethane
ND 0.50 4/24/19 23:36 EEHg/L0.16 4/23/19SM21-22 6200B1Bromodichloromethane
ND 2.0 4/24/19 23:36 EEHg/L0.46 4/23/19SM21-22 6200B1Bromoform
ND 2.0 4/24/19 23:36 EEHg/L0.78 4/23/19SM21-22 6200B1Bromomethane
ND 5.0 4/24/19 23:36 EEHg/L1.9 4/23/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 4/24/19 23:36 EEHg/L0.21 4/23/19SM21-22 6200B1n-Butylbenzene
ND 0.50 4/24/19 23:36 EEHg/L0.16 4/23/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 4/24/19 23:36 EEHg/L0.17 4/23/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 4/24/19 23:36 EEHg/L0.11 4/23/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 4/24/19 23:36 EEHg/L0.15 4/23/19SM21-22 6200B1Chlorobenzene
ND 0.50 4/24/19 23:36 EEHg/L0.21 4/23/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 4/24/19 23:36 EEHg/L0.35 4/23/19SM21-22 6200B1Chloroethane
ND 0.50 4/24/19 23:36 EEHg/L0.17 4/23/19SM21-22 6200B1Chloroform
ND 0.60 4/24/19 23:36 EEHg/L0.45 4/23/19SM21-22 6200B1Chloromethane
ND 0.50 4/24/19 23:36 EEHg/L0.12 4/23/19SM21-22 6200B12-Chlorotoluene
ND 0.50 4/24/19 23:36 EEHg/L0.14 4/23/19SM21-22 6200B14-Chlorotoluene
ND 0.50 4/24/19 23:36 EEHg/L0.19 4/23/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/24/19 23:36 EEHg/L0.16 4/23/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 4/24/19 23:36 EEHg/L0.12 4/23/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 4/24/19 23:36 EEHg/L0.13 4/23/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 4/24/19 23:36 EEHg/L0.26 4/23/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/24/19 23:36 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 4/24/19 23:36 EEHg/L0.41 4/23/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 4/24/19 23:36 EEHg/L0.32 4/23/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 4/24/19 23:36 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/24/19 23:36 EEHg/L0.31 4/23/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/24/19 23:36 EEHg/L0.20 4/23/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 4/24/19 23:36 EEHg/L0.11 4/23/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 4/24/19 23:36 EEHg/L0.20 4/23/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 4/24/19 23:36 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 4/24/19 23:36 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 4/24/19 23:36 EEHg/L0.23 4/23/19SM21-22 6200B1trans-1,3-Dichloropropene
5.1 0.50 4/24/19 23:36 EEHg/L0.17 4/23/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 4/24/19 23:36 EEHg/L0.13 4/23/19SM21-22 6200B1Ethylbenzene
ND 5.0 4/24/19 23:36 EEHg/L1.5 4/23/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 4/24/19 23:36 EEHg/L0.17 4/23/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/24/19 23:36 EEHg/L0.20 4/23/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
310 12 4/26/19 4:12 EEHg/L6.2 4/23/19SM21-22 6200B25Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/24/19 23:36 EEHg/L0.34 4/23/19SM21-22 6200B1Methylene Chloride
ND 5.0 4/24/19 23:36 EEHg/L1.7 4/23/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 4/24/19 23:36 EEHg/L0.31 4/23/19SM21-22 6200B1Naphthalene
Page 26 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-09
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 4/17/2019 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/24/19 23:36 EEHg/L0.13 4/23/19SM21-22 6200B1n-Propylbenzene
ND 0.50 4/24/19 23:36 EEHg/L0.11 4/23/19SM21-22 6200B1Styrene
ND 0.50 4/24/19 23:36 EEHg/L0.22 4/23/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/24/19 23:36 EEHg/L0.18 4/23/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 4/24/19 23:36 EEHg/L0.14 4/23/19SM21-22 6200B1Toluene
ND 5.0 4/24/19 23:36 EEHg/L0.57 4/23/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 4/24/19 23:36 EEHg/L0.40 4/23/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 4/24/19 23:36 EEHg/L0.20 4/23/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 4/24/19 23:36 EEHg/L0.16 4/23/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 4/24/19 23:36 EEHg/L0.24 4/23/19SM21-22 6200B1Trichloroethylene
ND 0.50 4/24/19 23:36 EEHg/L0.33 4/23/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/24/19 23:36 EEHg/L0.25 4/23/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 4/24/19 23:36 EEHg/L0.18 4/23/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 4/24/19 23:36 EEHg/L0.14 4/23/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 4/24/19 23:36 EEHg/L10 4/23/19SM21-22 6200B1Vinyl Acetate
ND 0.50 4/24/19 23:36 EEHg/L0.45 4/23/19SM21-22 6200B1Vinyl Chloride
ND 1.0 4/24/19 23:36 EEHg/L0.30 4/23/19SM21-22 6200B1m+p Xylene
ND 0.50 4/24/19 23:36 EEHg/L0.17 4/23/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.8 4/24/19 23:3670-130
1,2-Dichloroethane-d4 90.7 4/26/19 4:1270-130
Toluene-d8 96.4 4/24/19 23:3670-130
Toluene-d8 99.4 4/26/19 4:1270-130
4-Bromofluorobenzene 95.2 4/24/19 23:3670-130
4-Bromofluorobenzene 99.8 4/26/19 4:1270-130
Page 27 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-10
Field Sample #: WSW-2
Sample Matrix: Ground Water
Sampled: 4/17/2019 14:27
[TOC_2]19D1069-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/24/19 16:22 EEHg/L3.8 4/23/19SM21-22 6200B1Acetone
ND 0.50 4/24/19 16:22 EEHg/L0.18 4/23/19SM21-22 6200B1Benzene
ND 0.50 4/24/19 16:22 EEHg/L0.15 4/23/19SM21-22 6200B1Bromobenzene
ND 0.50 4/24/19 16:22 EEHg/L0.32 4/23/19SM21-22 6200B1Bromochloromethane
ND 0.50 4/24/19 16:22 EEHg/L0.16 4/23/19SM21-22 6200B1Bromodichloromethane
ND 2.0 4/24/19 16:22 EEHg/L0.46 4/23/19SM21-22 6200B1Bromoform
ND 2.0 4/24/19 16:22 EEHg/L0.78 4/23/19SM21-22 6200B1Bromomethane
ND 5.0 4/24/19 16:22 EEHg/L1.9 4/23/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 4/24/19 16:22 EEHg/L0.21 4/23/19SM21-22 6200B1n-Butylbenzene
ND 0.50 4/24/19 16:22 EEHg/L0.16 4/23/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 4/24/19 16:22 EEHg/L0.17 4/23/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 4/24/19 16:22 EEHg/L0.11 4/23/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 4/24/19 16:22 EEHg/L0.15 4/23/19SM21-22 6200B1Chlorobenzene
ND 0.50 4/24/19 16:22 EEHg/L0.21 4/23/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 4/24/19 16:22 EEHg/L0.35 4/23/19SM21-22 6200B1Chloroethane
ND 0.50 4/24/19 16:22 EEHg/L0.17 4/23/19SM21-22 6200B1Chloroform
ND 0.60 4/24/19 16:22 EEHg/L0.45 4/23/19SM21-22 6200B1Chloromethane
ND 0.50 4/24/19 16:22 EEHg/L0.12 4/23/19SM21-22 6200B12-Chlorotoluene
ND 0.50 4/24/19 16:22 EEHg/L0.14 4/23/19SM21-22 6200B14-Chlorotoluene
ND 0.50 4/24/19 16:22 EEHg/L0.19 4/23/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/24/19 16:22 EEHg/L0.16 4/23/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 4/24/19 16:22 EEHg/L0.12 4/23/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 4/24/19 16:22 EEHg/L0.13 4/23/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 4/24/19 16:22 EEHg/L0.26 4/23/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/24/19 16:22 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 4/24/19 16:22 EEHg/L0.41 4/23/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 4/24/19 16:22 EEHg/L0.32 4/23/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 4/24/19 16:22 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/24/19 16:22 EEHg/L0.31 4/23/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/24/19 16:22 EEHg/L0.20 4/23/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 4/24/19 16:22 EEHg/L0.11 4/23/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 4/24/19 16:22 EEHg/L0.20 4/23/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 4/24/19 16:22 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 4/24/19 16:22 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 4/24/19 16:22 EEHg/L0.23 4/23/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 4/24/19 16:22 EEHg/L0.17 4/23/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 4/24/19 16:22 EEHg/L0.13 4/23/19SM21-22 6200B1Ethylbenzene
ND 5.0 4/24/19 16:22 EEHg/L1.5 4/23/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 4/24/19 16:22 EEHg/L0.17 4/23/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/24/19 16:22 EEHg/L0.20 4/23/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 4/24/19 16:22 EEHg/L0.25 4/23/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/24/19 16:22 EEHg/L0.34 4/23/19SM21-22 6200B1Methylene Chloride
ND 5.0 4/24/19 16:22 EEHg/L1.7 4/23/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 4/24/19 16:22 EEHg/L0.31 4/23/19SM21-22 6200B1Naphthalene
Page 28 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-10
Field Sample #: WSW-2
Sample Matrix: Ground Water
Sampled: 4/17/2019 14:27
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/24/19 16:22 EEHg/L0.13 4/23/19SM21-22 6200B1n-Propylbenzene
ND 0.50 4/24/19 16:22 EEHg/L0.11 4/23/19SM21-22 6200B1Styrene
ND 0.50 4/24/19 16:22 EEHg/L0.22 4/23/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/24/19 16:22 EEHg/L0.18 4/23/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 4/24/19 16:22 EEHg/L0.14 4/23/19SM21-22 6200B1Toluene
ND 5.0 4/24/19 16:22 EEHg/L0.57 4/23/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 4/24/19 16:22 EEHg/L0.40 4/23/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 4/24/19 16:22 EEHg/L0.20 4/23/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 4/24/19 16:22 EEHg/L0.16 4/23/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 4/24/19 16:22 EEHg/L0.24 4/23/19SM21-22 6200B1Trichloroethylene
ND 0.50 4/24/19 16:22 EEHg/L0.33 4/23/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/24/19 16:22 EEHg/L0.25 4/23/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 4/24/19 16:22 EEHg/L0.18 4/23/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 4/24/19 16:22 EEHg/L0.14 4/23/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 4/24/19 16:22 EEHg/L10 4/23/19SM21-22 6200B1Vinyl Acetate
ND 0.50 4/24/19 16:22 EEHg/L0.45 4/23/19SM21-22 6200B1Vinyl Chloride
ND 1.0 4/24/19 16:22 EEHg/L0.30 4/23/19SM21-22 6200B1m+p Xylene
ND 0.50 4/24/19 16:22 EEHg/L0.17 4/23/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.2 4/24/19 16:2270-130
Toluene-d8 98.0 4/24/19 16:2270-130
4-Bromofluorobenzene 100 4/24/19 16:2270-130
Page 29 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-11
Field Sample #: WSW-3
Sample Matrix: Ground Water
Sampled: 4/17/2019 15:10
[TOC_2]19D1069-11[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/24/19 16:49 EEHg/L3.8 4/23/19SM21-22 6200B1Acetone
ND 0.50 4/24/19 16:49 EEHg/L0.18 4/23/19SM21-22 6200B1Benzene
ND 0.50 4/24/19 16:49 EEHg/L0.15 4/23/19SM21-22 6200B1Bromobenzene
ND 0.50 4/24/19 16:49 EEHg/L0.32 4/23/19SM21-22 6200B1Bromochloromethane
ND 0.50 4/24/19 16:49 EEHg/L0.16 4/23/19SM21-22 6200B1Bromodichloromethane
ND 2.0 4/24/19 16:49 EEHg/L0.46 4/23/19SM21-22 6200B1Bromoform
ND 2.0 4/24/19 16:49 EEHg/L0.78 4/23/19SM21-22 6200B1Bromomethane
ND 5.0 4/24/19 16:49 EEHg/L1.9 4/23/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 4/24/19 16:49 EEHg/L0.21 4/23/19SM21-22 6200B1n-Butylbenzene
ND 0.50 4/24/19 16:49 EEHg/L0.16 4/23/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 4/24/19 16:49 EEHg/L0.17 4/23/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 4/24/19 16:49 EEHg/L0.11 4/23/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 4/24/19 16:49 EEHg/L0.15 4/23/19SM21-22 6200B1Chlorobenzene
ND 0.50 4/24/19 16:49 EEHg/L0.21 4/23/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 4/24/19 16:49 EEHg/L0.35 4/23/19SM21-22 6200B1Chloroethane
ND 0.50 4/24/19 16:49 EEHg/L0.17 4/23/19SM21-22 6200B1Chloroform
ND 0.60 4/24/19 16:49 EEHg/L0.45 4/23/19SM21-22 6200B1Chloromethane
ND 0.50 4/24/19 16:49 EEHg/L0.12 4/23/19SM21-22 6200B12-Chlorotoluene
ND 0.50 4/24/19 16:49 EEHg/L0.14 4/23/19SM21-22 6200B14-Chlorotoluene
ND 0.50 4/24/19 16:49 EEHg/L0.19 4/23/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/24/19 16:49 EEHg/L0.16 4/23/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 4/24/19 16:49 EEHg/L0.12 4/23/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 4/24/19 16:49 EEHg/L0.13 4/23/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 4/24/19 16:49 EEHg/L0.26 4/23/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/24/19 16:49 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 4/24/19 16:49 EEHg/L0.41 4/23/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 4/24/19 16:49 EEHg/L0.32 4/23/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 4/24/19 16:49 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/24/19 16:49 EEHg/L0.31 4/23/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/24/19 16:49 EEHg/L0.20 4/23/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 4/24/19 16:49 EEHg/L0.11 4/23/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 4/24/19 16:49 EEHg/L0.20 4/23/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 4/24/19 16:49 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 4/24/19 16:49 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 4/24/19 16:49 EEHg/L0.23 4/23/19SM21-22 6200B1trans-1,3-Dichloropropene
0.17 0.50 4/24/19 16:49 EEHg/L0.17 4/23/19SM21-22 6200B1JDiisopropyl Ether (DIPE)
ND 0.50 4/24/19 16:49 EEHg/L0.13 4/23/19SM21-22 6200B1Ethylbenzene
ND 5.0 4/24/19 16:49 EEHg/L1.5 4/23/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 4/24/19 16:49 EEHg/L0.17 4/23/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/24/19 16:49 EEHg/L0.20 4/23/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
9.5 0.50 4/24/19 16:49 EEHg/L0.25 4/23/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/24/19 16:49 EEHg/L0.34 4/23/19SM21-22 6200B1Methylene Chloride
ND 5.0 4/24/19 16:49 EEHg/L1.7 4/23/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 4/24/19 16:49 EEHg/L0.31 4/23/19SM21-22 6200B1Naphthalene
Page 30 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-11
Field Sample #: WSW-3
Sample Matrix: Ground Water
Sampled: 4/17/2019 15:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/24/19 16:49 EEHg/L0.13 4/23/19SM21-22 6200B1n-Propylbenzene
ND 0.50 4/24/19 16:49 EEHg/L0.11 4/23/19SM21-22 6200B1Styrene
ND 0.50 4/24/19 16:49 EEHg/L0.22 4/23/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/24/19 16:49 EEHg/L0.18 4/23/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 4/24/19 16:49 EEHg/L0.14 4/23/19SM21-22 6200B1Toluene
ND 5.0 4/24/19 16:49 EEHg/L0.57 4/23/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 4/24/19 16:49 EEHg/L0.40 4/23/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 4/24/19 16:49 EEHg/L0.20 4/23/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 4/24/19 16:49 EEHg/L0.16 4/23/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 4/24/19 16:49 EEHg/L0.24 4/23/19SM21-22 6200B1Trichloroethylene
ND 0.50 4/24/19 16:49 EEHg/L0.33 4/23/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/24/19 16:49 EEHg/L0.25 4/23/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 4/24/19 16:49 EEHg/L0.18 4/23/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 4/24/19 16:49 EEHg/L0.14 4/23/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 4/24/19 16:49 EEHg/L10 4/23/19SM21-22 6200B1Vinyl Acetate
ND 0.50 4/24/19 16:49 EEHg/L0.45 4/23/19SM21-22 6200B1Vinyl Chloride
ND 1.0 4/24/19 16:49 EEHg/L0.30 4/23/19SM21-22 6200B1m+p Xylene
ND 0.50 4/24/19 16:49 EEHg/L0.17 4/23/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.2 4/24/19 16:4970-130
Toluene-d8 98.4 4/24/19 16:4970-130
4-Bromofluorobenzene 98.3 4/24/19 16:4970-130
Page 31 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-12
Field Sample #: PW-4B
Sample Matrix: Ground Water
Sampled: 4/17/2019 14:10
[TOC_2]19D1069-12[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/24/19 21:21 EEHg/L3.8 4/23/19SM21-22 6200B1Acetone
ND 0.50 4/24/19 21:21 EEHg/L0.18 4/23/19SM21-22 6200B1Benzene
ND 0.50 4/24/19 21:21 EEHg/L0.15 4/23/19SM21-22 6200B1Bromobenzene
ND 0.50 4/24/19 21:21 EEHg/L0.32 4/23/19SM21-22 6200B1Bromochloromethane
ND 0.50 4/24/19 21:21 EEHg/L0.16 4/23/19SM21-22 6200B1Bromodichloromethane
ND 2.0 4/24/19 21:21 EEHg/L0.46 4/23/19SM21-22 6200B1Bromoform
ND 2.0 4/24/19 21:21 EEHg/L0.78 4/23/19SM21-22 6200B1Bromomethane
ND 5.0 4/24/19 21:21 EEHg/L1.9 4/23/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 4/24/19 21:21 EEHg/L0.21 4/23/19SM21-22 6200B1n-Butylbenzene
ND 0.50 4/24/19 21:21 EEHg/L0.16 4/23/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 4/24/19 21:21 EEHg/L0.17 4/23/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 4/24/19 21:21 EEHg/L0.11 4/23/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 4/24/19 21:21 EEHg/L0.15 4/23/19SM21-22 6200B1Chlorobenzene
ND 0.50 4/24/19 21:21 EEHg/L0.21 4/23/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 4/24/19 21:21 EEHg/L0.35 4/23/19SM21-22 6200B1Chloroethane
ND 0.50 4/24/19 21:21 EEHg/L0.17 4/23/19SM21-22 6200B1Chloroform
ND 0.60 4/24/19 21:21 EEHg/L0.45 4/23/19SM21-22 6200B1Chloromethane
ND 0.50 4/24/19 21:21 EEHg/L0.12 4/23/19SM21-22 6200B12-Chlorotoluene
ND 0.50 4/24/19 21:21 EEHg/L0.14 4/23/19SM21-22 6200B14-Chlorotoluene
ND 0.50 4/24/19 21:21 EEHg/L0.19 4/23/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/24/19 21:21 EEHg/L0.16 4/23/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 4/24/19 21:21 EEHg/L0.12 4/23/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 4/24/19 21:21 EEHg/L0.13 4/23/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 4/24/19 21:21 EEHg/L0.26 4/23/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/24/19 21:21 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloroethane
1.6 0.50 4/24/19 21:21 EEHg/L0.41 4/23/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 4/24/19 21:21 EEHg/L0.32 4/23/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 4/24/19 21:21 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/24/19 21:21 EEHg/L0.31 4/23/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/24/19 21:21 EEHg/L0.20 4/23/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 4/24/19 21:21 EEHg/L0.11 4/23/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 4/24/19 21:21 EEHg/L0.20 4/23/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 4/24/19 21:21 EEHg/L0.16 4/23/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 4/24/19 21:21 EEHg/L0.13 4/23/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 4/24/19 21:21 EEHg/L0.23 4/23/19SM21-22 6200B1trans-1,3-Dichloropropene
4.8 0.50 4/24/19 21:21 EEHg/L0.17 4/23/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 4/24/19 21:21 EEHg/L0.13 4/23/19SM21-22 6200B1Ethylbenzene
ND 5.0 4/24/19 21:21 EEHg/L1.5 4/23/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 4/24/19 21:21 EEHg/L0.17 4/23/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/24/19 21:21 EEHg/L0.20 4/23/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
110 0.50 4/24/19 21:21 EEHg/L0.25 4/23/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/24/19 21:21 EEHg/L0.34 4/23/19SM21-22 6200B1Methylene Chloride
ND 5.0 4/24/19 21:21 EEHg/L1.7 4/23/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 4/24/19 21:21 EEHg/L0.31 4/23/19SM21-22 6200B1Naphthalene
Page 32 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-12
Field Sample #: PW-4B
Sample Matrix: Ground Water
Sampled: 4/17/2019 14:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/24/19 21:21 EEHg/L0.13 4/23/19SM21-22 6200B1n-Propylbenzene
ND 0.50 4/24/19 21:21 EEHg/L0.11 4/23/19SM21-22 6200B1Styrene
ND 0.50 4/24/19 21:21 EEHg/L0.22 4/23/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/24/19 21:21 EEHg/L0.18 4/23/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 4/24/19 21:21 EEHg/L0.14 4/23/19SM21-22 6200B1Toluene
ND 5.0 4/24/19 21:21 EEHg/L0.57 4/23/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 4/24/19 21:21 EEHg/L0.40 4/23/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 4/24/19 21:21 EEHg/L0.20 4/23/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 4/24/19 21:21 EEHg/L0.16 4/23/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 4/24/19 21:21 EEHg/L0.24 4/23/19SM21-22 6200B1Trichloroethylene
ND 0.50 4/24/19 21:21 EEHg/L0.33 4/23/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/24/19 21:21 EEHg/L0.25 4/23/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 4/24/19 21:21 EEHg/L0.18 4/23/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 4/24/19 21:21 EEHg/L0.14 4/23/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 4/24/19 21:21 EEHg/L10 4/23/19SM21-22 6200B1Vinyl Acetate
ND 0.50 4/24/19 21:21 EEHg/L0.45 4/23/19SM21-22 6200B1Vinyl Chloride
ND 1.0 4/24/19 21:21 EEHg/L0.30 4/23/19SM21-22 6200B1m+p Xylene
ND 0.50 4/24/19 21:21 EEHg/L0.17 4/23/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 92.0 4/24/19 21:2170-130
Toluene-d8 98.8 4/24/19 21:2170-130
4-Bromofluorobenzene 100 4/24/19 21:2170-130
Page 33 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-13
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 4/18/2019 11:16
[TOC_2]19D1069-13[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 1000 4/26/19 20:30 EEHg/L76 4/26/19SM21-22 6200B20Acetone
100 10 4/26/19 20:30 EEHg/L3.6 4/26/19SM21-22 6200B20Benzene
ND 10 4/26/19 20:30 EEHg/L3.0 4/26/19SM21-22 6200B20Bromobenzene
ND 10 4/26/19 20:30 EEHg/L6.4 4/26/19SM21-22 6200B20Bromochloromethane
ND 10 4/26/19 20:30 EEHg/L3.2 4/26/19SM21-22 6200B20Bromodichloromethane
ND 40 4/26/19 20:30 EEHg/L9.2 4/26/19SM21-22 6200B20Bromoform
ND 40 4/26/19 20:30 EEHg/L16 4/26/19SM21-22 6200B20Bromomethane
ND 100 4/26/19 20:30 EEHg/L39 4/26/19SM21-22 6200B202-Butanone (MEK)
16 10 4/26/19 20:30 EEHg/L4.2 4/26/19SM21-22 6200B20n-Butylbenzene
8.8 10 4/26/19 20:30 EEHg/L3.2 4/26/19SM21-22 6200B20Jsec-Butylbenzene
ND 10 4/26/19 20:30 EEHg/L3.4 4/26/19SM21-22 6200B20tert-Butylbenzene
ND 10 4/26/19 20:30 EEHg/L2.2 4/26/19SM21-22 6200B20Carbon Tetrachloride
ND 10 4/26/19 20:30 EEHg/L3.0 4/26/19SM21-22 6200B20Chlorobenzene
ND 10 4/26/19 20:30 EEHg/L4.2 4/26/19SM21-22 6200B20Chlorodibromomethane
ND 10 4/26/19 20:30 EEHg/L7.0 4/26/19SM21-22 6200B20Chloroethane
ND 10 4/26/19 20:30 EEHg/L3.4 4/26/19SM21-22 6200B20Chloroform
ND 12 4/26/19 20:30 EEHg/L9.0 4/26/19SM21-22 6200B20Chloromethane
ND 10 4/26/19 20:30 EEHg/L2.4 4/26/19SM21-22 6200B202-Chlorotoluene
ND 10 4/26/19 20:30 EEHg/L2.8 4/26/19SM21-22 6200B204-Chlorotoluene
ND 10 4/26/19 20:30 EEHg/L3.8 4/26/19SM21-22 6200B201,2-Dibromoethane (EDB)
ND 10 4/26/19 20:30 EEHg/L3.2 4/26/19SM21-22 6200B201,2-Dichlorobenzene
ND 10 4/26/19 20:30 EEHg/L2.4 4/26/19SM21-22 6200B201,3-Dichlorobenzene
ND 10 4/26/19 20:30 EEHg/L2.6 4/26/19SM21-22 6200B201,4-Dichlorobenzene
ND 10 4/26/19 20:30 EEHg/L5.2 4/26/19SM21-22 6200B20Dichlorodifluoromethane (Freon 12)
ND 10 4/26/19 20:30 EEHg/L3.2 4/26/19SM21-22 6200B201,1-Dichloroethane
ND 10 4/26/19 20:30 EEHg/L8.2 4/26/19SM21-22 6200B201,2-Dichloroethane
ND 10 4/26/19 20:30 EEHg/L6.4 4/26/19SM21-22 6200B201,1-Dichloroethylene
ND 10 4/26/19 20:30 EEHg/L2.6 4/26/19SM21-22 6200B20cis-1,2-Dichloroethylene
ND 10 4/26/19 20:30 EEHg/L6.2 4/26/19SM21-22 6200B20trans-1,2-Dichloroethylene
ND 10 4/26/19 20:30 EEHg/L4.0 4/26/19SM21-22 6200B201,2-Dichloropropane
ND 10 4/26/19 20:30 EEHg/L2.2 4/26/19SM21-22 6200B201,3-Dichloropropane
ND 10 4/26/19 20:30 EEHg/L4.0 4/26/19SM21-22 6200B202,2-Dichloropropane
ND 10 4/26/19 20:30 EEHg/L3.2 4/26/19SM21-22 6200B201,1-Dichloropropene
ND 10 4/26/19 20:30 EEHg/L2.6 4/26/19SM21-22 6200B20cis-1,3-Dichloropropene
ND 10 4/26/19 20:30 EEHg/L4.6 4/26/19SM21-22 6200B20trans-1,3-Dichloropropene
5.4 10 4/26/19 20:30 EEHg/L3.4 4/26/19SM21-22 6200B20JDiisopropyl Ether (DIPE)
150 10 4/26/19 20:30 EEHg/L2.6 4/26/19SM21-22 6200B20Ethylbenzene
ND 100 4/26/19 20:30 EEHg/L30 4/26/19SM21-22 6200B202-Hexanone (MBK)
27 10 4/26/19 20:30 EEHg/L3.4 4/26/19SM21-22 6200B20Isopropylbenzene (Cumene)
7.8 10 4/26/19 20:30 EEHg/L4.0 4/26/19SM21-22 6200B20Jp-Isopropyltoluene (p-Cymene)
830 10 4/26/19 20:30 EEHg/L5.0 4/26/19SM21-22 6200B20Methyl tert-Butyl Ether (MTBE)
ND 100 4/26/19 20:30 EEHg/L6.8 4/26/19SM21-22 6200B20Methylene Chloride
ND 100 4/26/19 20:30 EEHg/L33 4/26/19SM21-22 6200B204-Methyl-2-pentanone (MIBK)
100 40 4/26/19 20:30 EEHg/L6.2 4/26/19SM21-22 6200B20Naphthalene
Page 34 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-13
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 4/18/2019 11:16
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
66 10 4/26/19 20:30 EEHg/L2.6 4/26/19SM21-22 6200B20n-Propylbenzene
3.4 10 4/26/19 20:30 EEHg/L2.2 4/26/19SM21-22 6200B20JStyrene
ND 10 4/26/19 20:30 EEHg/L4.4 4/26/19SM21-22 6200B201,1,2,2-Tetrachloroethane
ND 10 4/26/19 20:30 EEHg/L3.6 4/26/19SM21-22 6200B20Tetrachloroethylene
390 10 4/26/19 20:30 EEHg/L2.8 4/26/19SM21-22 6200B20Toluene
ND 100 4/26/19 20:30 EEHg/L11 4/26/19SM21-22 6200B201,2,3-Trichlorobenzene
ND 40 4/26/19 20:30 EEHg/L8.0 4/26/19SM21-22 6200B201,2,4-Trichlorobenzene
ND 10 4/26/19 20:30 EEHg/L4.0 4/26/19SM21-22 6200B201,1,1-Trichloroethane
ND 10 4/26/19 20:30 EEHg/L3.2 4/26/19SM21-22 6200B201,1,2-Trichloroethane
ND 10 4/26/19 20:30 EEHg/L4.8 4/26/19SM21-22 6200B20Trichloroethylene
ND 10 4/26/19 20:30 EEHg/L6.6 4/26/19SM21-22 6200B20Trichlorofluoromethane (Freon 11)
ND 10 4/26/19 20:30 EEHg/L5.0 4/26/19SM21-22 6200B201,2,3-Trichloropropane
990 10 4/26/19 20:30 EEHg/L3.6 4/26/19SM21-22 6200B201,2,4-Trimethylbenzene
380 10 4/26/19 20:30 EEHg/L2.8 4/26/19SM21-22 6200B201,3,5-Trimethylbenzene
ND 400 4/26/19 20:30 EEHg/L200 4/26/19SM21-22 6200B20L-04Vinyl Acetate
ND 10 4/26/19 20:30 EEHg/L9.0 4/26/19SM21-22 6200B20Vinyl Chloride
1500 20 4/26/19 20:30 EEHg/L6.0 4/26/19SM21-22 6200B20m+p Xylene
820 10 4/26/19 20:30 EEHg/L3.4 4/26/19SM21-22 6200B20o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.2 4/26/19 20:3070-130
Toluene-d8 97.4 4/26/19 20:3070-130
4-Bromofluorobenzene 105 4/26/19 20:3070-130
Page 35 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-14
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 4/18/2019 10:42
[TOC_2]19D1069-14[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/26/19 2:23 EEHg/L3.8 4/25/19SM21-22 6200B1Acetone
0.40 0.50 4/26/19 2:23 EEHg/L0.18 4/25/19SM21-22 6200B1JBenzene
ND 0.50 4/26/19 2:23 EEHg/L0.15 4/25/19SM21-22 6200B1Bromobenzene
ND 0.50 4/26/19 2:23 EEHg/L0.32 4/25/19SM21-22 6200B1Bromochloromethane
ND 0.50 4/26/19 2:23 EEHg/L0.16 4/25/19SM21-22 6200B1Bromodichloromethane
ND 2.0 4/26/19 2:23 EEHg/L0.46 4/25/19SM21-22 6200B1Bromoform
ND 2.0 4/26/19 2:23 EEHg/L0.78 4/25/19SM21-22 6200B1Bromomethane
ND 5.0 4/26/19 2:23 EEHg/L1.9 4/25/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 4/26/19 2:23 EEHg/L0.21 4/25/19SM21-22 6200B1n-Butylbenzene
ND 0.50 4/26/19 2:23 EEHg/L0.16 4/25/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 4/26/19 2:23 EEHg/L0.17 4/25/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 4/26/19 2:23 EEHg/L0.11 4/25/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 4/26/19 2:23 EEHg/L0.15 4/25/19SM21-22 6200B1Chlorobenzene
ND 0.50 4/26/19 2:23 EEHg/L0.21 4/25/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 4/26/19 2:23 EEHg/L0.35 4/25/19SM21-22 6200B1Chloroethane
ND 0.50 4/26/19 2:23 EEHg/L0.17 4/25/19SM21-22 6200B1Chloroform
ND 0.60 4/26/19 2:23 EEHg/L0.45 4/25/19SM21-22 6200B1Chloromethane
ND 0.50 4/26/19 2:23 EEHg/L0.12 4/25/19SM21-22 6200B12-Chlorotoluene
ND 0.50 4/26/19 2:23 EEHg/L0.14 4/25/19SM21-22 6200B14-Chlorotoluene
ND 0.50 4/26/19 2:23 EEHg/L0.19 4/25/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/26/19 2:23 EEHg/L0.16 4/25/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 4/26/19 2:23 EEHg/L0.12 4/25/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 4/26/19 2:23 EEHg/L0.13 4/25/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 4/26/19 2:23 EEHg/L0.26 4/25/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/26/19 2:23 EEHg/L0.16 4/25/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 4/26/19 2:23 EEHg/L0.41 4/25/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 4/26/19 2:23 EEHg/L0.32 4/25/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 4/26/19 2:23 EEHg/L0.13 4/25/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/26/19 2:23 EEHg/L0.31 4/25/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/26/19 2:23 EEHg/L0.20 4/25/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 4/26/19 2:23 EEHg/L0.11 4/25/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 4/26/19 2:23 EEHg/L0.20 4/25/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 4/26/19 2:23 EEHg/L0.16 4/25/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 4/26/19 2:23 EEHg/L0.13 4/25/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 4/26/19 2:23 EEHg/L0.23 4/25/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 4/26/19 2:23 EEHg/L0.17 4/25/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 4/26/19 2:23 EEHg/L0.13 4/25/19SM21-22 6200B1Ethylbenzene
ND 5.0 4/26/19 2:23 EEHg/L1.5 4/25/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 4/26/19 2:23 EEHg/L0.17 4/25/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/26/19 2:23 EEHg/L0.20 4/25/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 4/26/19 2:23 EEHg/L0.25 4/25/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/26/19 2:23 EEHg/L0.34 4/25/19SM21-22 6200B1Methylene Chloride
ND 5.0 4/26/19 2:23 EEHg/L1.7 4/25/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 2.0 4/26/19 2:23 EEHg/L0.31 4/25/19SM21-22 6200B1Naphthalene
Page 36 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-14
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 4/18/2019 10:42
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/26/19 2:23 EEHg/L0.13 4/25/19SM21-22 6200B1n-Propylbenzene
ND 0.50 4/26/19 2:23 EEHg/L0.11 4/25/19SM21-22 6200B1Styrene
ND 0.50 4/26/19 2:23 EEHg/L0.22 4/25/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/26/19 2:23 EEHg/L0.18 4/25/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 4/26/19 2:23 EEHg/L0.14 4/25/19SM21-22 6200B1Toluene
ND 5.0 4/26/19 2:23 EEHg/L0.57 4/25/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 4/26/19 2:23 EEHg/L0.40 4/25/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 4/26/19 2:23 EEHg/L0.20 4/25/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 4/26/19 2:23 EEHg/L0.16 4/25/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 4/26/19 2:23 EEHg/L0.24 4/25/19SM21-22 6200B1Trichloroethylene
ND 0.50 4/26/19 2:23 EEHg/L0.33 4/25/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/26/19 2:23 EEHg/L0.25 4/25/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 4/26/19 2:23 EEHg/L0.18 4/25/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 4/26/19 2:23 EEHg/L0.14 4/25/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 4/26/19 2:23 EEHg/L10 4/25/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 4/26/19 2:23 EEHg/L0.45 4/25/19SM21-22 6200B1Vinyl Chloride
ND 1.0 4/26/19 2:23 EEHg/L0.30 4/25/19SM21-22 6200B1m+p Xylene
ND 0.50 4/26/19 2:23 EEHg/L0.17 4/25/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.8 4/26/19 2:2370-130
Toluene-d8 102 4/26/19 2:2370-130
4-Bromofluorobenzene 96.2 4/26/19 2:2370-130
Page 37 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-15
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 4/18/2019 10:20
[TOC_2]19D1069-15[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/26/19 2:50 EEHg/L3.8 4/25/19SM21-22 6200B1Acetone
47 0.50 4/26/19 2:50 EEHg/L0.18 4/25/19SM21-22 6200B1Benzene
ND 0.50 4/26/19 2:50 EEHg/L0.15 4/25/19SM21-22 6200B1Bromobenzene
ND 0.50 4/26/19 2:50 EEHg/L0.32 4/25/19SM21-22 6200B1Bromochloromethane
ND 0.50 4/26/19 2:50 EEHg/L0.16 4/25/19SM21-22 6200B1Bromodichloromethane
ND 2.0 4/26/19 2:50 EEHg/L0.46 4/25/19SM21-22 6200B1Bromoform
ND 2.0 4/26/19 2:50 EEHg/L0.78 4/25/19SM21-22 6200B1Bromomethane
ND 5.0 4/26/19 2:50 EEHg/L1.9 4/25/19SM21-22 6200B12-Butanone (MEK)
0.30 0.50 4/26/19 2:50 EEHg/L0.21 4/25/19SM21-22 6200B1Jn-Butylbenzene
0.19 0.50 4/26/19 2:50 EEHg/L0.16 4/25/19SM21-22 6200B1Jsec-Butylbenzene
ND 0.50 4/26/19 2:50 EEHg/L0.17 4/25/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 4/26/19 2:50 EEHg/L0.11 4/25/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 4/26/19 2:50 EEHg/L0.15 4/25/19SM21-22 6200B1Chlorobenzene
ND 0.50 4/26/19 2:50 EEHg/L0.21 4/25/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 4/26/19 2:50 EEHg/L0.35 4/25/19SM21-22 6200B1Chloroethane
ND 0.50 4/26/19 2:50 EEHg/L0.17 4/25/19SM21-22 6200B1Chloroform
ND 0.60 4/26/19 2:50 EEHg/L0.45 4/25/19SM21-22 6200B1Chloromethane
ND 0.50 4/26/19 2:50 EEHg/L0.12 4/25/19SM21-22 6200B12-Chlorotoluene
ND 0.50 4/26/19 2:50 EEHg/L0.14 4/25/19SM21-22 6200B14-Chlorotoluene
ND 0.50 4/26/19 2:50 EEHg/L0.19 4/25/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/26/19 2:50 EEHg/L0.16 4/25/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 4/26/19 2:50 EEHg/L0.12 4/25/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 4/26/19 2:50 EEHg/L0.13 4/25/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 4/26/19 2:50 EEHg/L0.26 4/25/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/26/19 2:50 EEHg/L0.16 4/25/19SM21-22 6200B11,1-Dichloroethane
1.4 0.50 4/26/19 2:50 EEHg/L0.41 4/25/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 4/26/19 2:50 EEHg/L0.32 4/25/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 4/26/19 2:50 EEHg/L0.13 4/25/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/26/19 2:50 EEHg/L0.31 4/25/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/26/19 2:50 EEHg/L0.20 4/25/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 4/26/19 2:50 EEHg/L0.11 4/25/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 4/26/19 2:50 EEHg/L0.20 4/25/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 4/26/19 2:50 EEHg/L0.16 4/25/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 4/26/19 2:50 EEHg/L0.13 4/25/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 4/26/19 2:50 EEHg/L0.23 4/25/19SM21-22 6200B1trans-1,3-Dichloropropene
0.95 0.50 4/26/19 2:50 EEHg/L0.17 4/25/19SM21-22 6200B1Diisopropyl Ether (DIPE)
5.1 0.50 4/26/19 2:50 EEHg/L0.13 4/25/19SM21-22 6200B1Ethylbenzene
ND 5.0 4/26/19 2:50 EEHg/L1.5 4/25/19SM21-22 6200B12-Hexanone (MBK)
0.82 0.50 4/26/19 2:50 EEHg/L0.17 4/25/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/26/19 2:50 EEHg/L0.20 4/25/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
28 0.50 4/26/19 2:50 EEHg/L0.25 4/25/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/26/19 2:50 EEHg/L0.34 4/25/19SM21-22 6200B1Methylene Chloride
ND 5.0 4/26/19 2:50 EEHg/L1.7 4/25/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
3.5 2.0 4/26/19 2:50 EEHg/L0.31 4/25/19SM21-22 6200B1Naphthalene
Page 38 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-15
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 4/18/2019 10:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
1.5 0.50 4/26/19 2:50 EEHg/L0.13 4/25/19SM21-22 6200B1n-Propylbenzene
0.18 0.50 4/26/19 2:50 EEHg/L0.11 4/25/19SM21-22 6200B1JStyrene
ND 0.50 4/26/19 2:50 EEHg/L0.22 4/25/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/26/19 2:50 EEHg/L0.18 4/25/19SM21-22 6200B1Tetrachloroethylene
2.0 0.50 4/26/19 2:50 EEHg/L0.14 4/25/19SM21-22 6200B1Toluene
ND 5.0 4/26/19 2:50 EEHg/L0.57 4/25/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 4/26/19 2:50 EEHg/L0.40 4/25/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 4/26/19 2:50 EEHg/L0.20 4/25/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 4/26/19 2:50 EEHg/L0.16 4/25/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 4/26/19 2:50 EEHg/L0.24 4/25/19SM21-22 6200B1Trichloroethylene
ND 0.50 4/26/19 2:50 EEHg/L0.33 4/25/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/26/19 2:50 EEHg/L0.25 4/25/19SM21-22 6200B11,2,3-Trichloropropane
9.8 0.50 4/26/19 2:50 EEHg/L0.18 4/25/19SM21-22 6200B11,2,4-Trimethylbenzene
1.6 0.50 4/26/19 2:50 EEHg/L0.14 4/25/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 4/26/19 2:50 EEHg/L10 4/25/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 4/26/19 2:50 EEHg/L0.45 4/25/19SM21-22 6200B1Vinyl Chloride
2.4 1.0 4/26/19 2:50 EEHg/L0.30 4/25/19SM21-22 6200B1m+p Xylene
2.1 0.50 4/26/19 2:50 EEHg/L0.17 4/25/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.6 4/26/19 2:5070-130
Toluene-d8 98.0 4/26/19 2:5070-130
4-Bromofluorobenzene 99.0 4/26/19 2:5070-130
Page 39 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-16
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 4/18/2019 10:00
[TOC_2]19D1069-16[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 25000 4/26/19 19:36 EEHg/L1900 4/26/19SM21-22 6200B500Acetone
2900 250 4/26/19 19:36 EEHg/L90 4/26/19SM21-22 6200B500Benzene
ND 250 4/26/19 19:36 EEHg/L75 4/26/19SM21-22 6200B500Bromobenzene
ND 250 4/26/19 19:36 EEHg/L160 4/26/19SM21-22 6200B500Bromochloromethane
ND 250 4/26/19 19:36 EEHg/L80 4/26/19SM21-22 6200B500Bromodichloromethane
ND 1000 4/26/19 19:36 EEHg/L230 4/26/19SM21-22 6200B500Bromoform
ND 1000 4/26/19 19:36 EEHg/L390 4/26/19SM21-22 6200B500Bromomethane
ND 2500 4/26/19 19:36 EEHg/L970 4/26/19SM21-22 6200B5002-Butanone (MEK)
ND 250 4/26/19 19:36 EEHg/L100 4/26/19SM21-22 6200B500n-Butylbenzene
ND 250 4/26/19 19:36 EEHg/L80 4/26/19SM21-22 6200B500sec-Butylbenzene
ND 250 4/26/19 19:36 EEHg/L85 4/26/19SM21-22 6200B500tert-Butylbenzene
ND 250 4/26/19 19:36 EEHg/L55 4/26/19SM21-22 6200B500Carbon Tetrachloride
ND 250 4/26/19 19:36 EEHg/L75 4/26/19SM21-22 6200B500Chlorobenzene
ND 250 4/26/19 19:36 EEHg/L100 4/26/19SM21-22 6200B500Chlorodibromomethane
ND 250 4/26/19 19:36 EEHg/L180 4/26/19SM21-22 6200B500Chloroethane
ND 250 4/26/19 19:36 EEHg/L85 4/26/19SM21-22 6200B500Chloroform
ND 300 4/26/19 19:36 EEHg/L220 4/26/19SM21-22 6200B500Chloromethane
ND 250 4/26/19 19:36 EEHg/L60 4/26/19SM21-22 6200B5002-Chlorotoluene
ND 250 4/26/19 19:36 EEHg/L70 4/26/19SM21-22 6200B5004-Chlorotoluene
ND 250 4/26/19 19:36 EEHg/L95 4/26/19SM21-22 6200B5001,2-Dibromoethane (EDB)
ND 250 4/26/19 19:36 EEHg/L80 4/26/19SM21-22 6200B5001,2-Dichlorobenzene
ND 250 4/26/19 19:36 EEHg/L60 4/26/19SM21-22 6200B5001,3-Dichlorobenzene
ND 250 4/26/19 19:36 EEHg/L65 4/26/19SM21-22 6200B5001,4-Dichlorobenzene
ND 250 4/26/19 19:36 EEHg/L130 4/26/19SM21-22 6200B500Dichlorodifluoromethane (Freon 12)
ND 250 4/26/19 19:36 EEHg/L80 4/26/19SM21-22 6200B5001,1-Dichloroethane
600 250 4/26/19 19:36 EEHg/L200 4/26/19SM21-22 6200B5001,2-Dichloroethane
ND 250 4/26/19 19:36 EEHg/L160 4/26/19SM21-22 6200B5001,1-Dichloroethylene
ND 250 4/26/19 19:36 EEHg/L65 4/26/19SM21-22 6200B500cis-1,2-Dichloroethylene
ND 250 4/26/19 19:36 EEHg/L160 4/26/19SM21-22 6200B500trans-1,2-Dichloroethylene
ND 250 4/26/19 19:36 EEHg/L100 4/26/19SM21-22 6200B5001,2-Dichloropropane
ND 250 4/26/19 19:36 EEHg/L55 4/26/19SM21-22 6200B5001,3-Dichloropropane
ND 250 4/26/19 19:36 EEHg/L100 4/26/19SM21-22 6200B5002,2-Dichloropropane
ND 250 4/26/19 19:36 EEHg/L80 4/26/19SM21-22 6200B5001,1-Dichloropropene
ND 250 4/26/19 19:36 EEHg/L65 4/26/19SM21-22 6200B500cis-1,3-Dichloropropene
ND 250 4/26/19 19:36 EEHg/L120 4/26/19SM21-22 6200B500trans-1,3-Dichloropropene
760 250 4/26/19 19:36 EEHg/L85 4/26/19SM21-22 6200B500Diisopropyl Ether (DIPE)
270 250 4/26/19 19:36 EEHg/L65 4/26/19SM21-22 6200B500Ethylbenzene
ND 2500 4/26/19 19:36 EEHg/L760 4/26/19SM21-22 6200B5002-Hexanone (MBK)
ND 250 4/26/19 19:36 EEHg/L85 4/26/19SM21-22 6200B500Isopropylbenzene (Cumene)
ND 250 4/26/19 19:36 EEHg/L100 4/26/19SM21-22 6200B500p-Isopropyltoluene (p-Cymene)
53000 250 4/26/19 19:36 EEHg/L120 4/26/19SM21-22 6200B500Methyl tert-Butyl Ether (MTBE)
ND 2500 4/26/19 19:36 EEHg/L170 4/26/19SM21-22 6200B500Methylene Chloride
ND 2500 4/26/19 19:36 EEHg/L840 4/26/19SM21-22 6200B5004-Methyl-2-pentanone (MIBK)
ND 1000 4/26/19 19:36 EEHg/L160 4/26/19SM21-22 6200B500Naphthalene
Page 40 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-16
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 4/18/2019 10:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 250 4/26/19 19:36 EEHg/L65 4/26/19SM21-22 6200B500n-Propylbenzene
ND 250 4/26/19 19:36 EEHg/L55 4/26/19SM21-22 6200B500Styrene
ND 250 4/26/19 19:36 EEHg/L110 4/26/19SM21-22 6200B5001,1,2,2-Tetrachloroethane
ND 250 4/26/19 19:36 EEHg/L90 4/26/19SM21-22 6200B500Tetrachloroethylene
3400 250 4/26/19 19:36 EEHg/L70 4/26/19SM21-22 6200B500Toluene
ND 2500 4/26/19 19:36 EEHg/L280 4/26/19SM21-22 6200B5001,2,3-Trichlorobenzene
ND 1000 4/26/19 19:36 EEHg/L200 4/26/19SM21-22 6200B5001,2,4-Trichlorobenzene
ND 250 4/26/19 19:36 EEHg/L100 4/26/19SM21-22 6200B5001,1,1-Trichloroethane
ND 250 4/26/19 19:36 EEHg/L80 4/26/19SM21-22 6200B5001,1,2-Trichloroethane
ND 250 4/26/19 19:36 EEHg/L120 4/26/19SM21-22 6200B500Trichloroethylene
ND 250 4/26/19 19:36 EEHg/L160 4/26/19SM21-22 6200B500Trichlorofluoromethane (Freon 11)
ND 250 4/26/19 19:36 EEHg/L120 4/26/19SM21-22 6200B5001,2,3-Trichloropropane
1100 250 4/26/19 19:36 EEHg/L90 4/26/19SM21-22 6200B5001,2,4-Trimethylbenzene
580 250 4/26/19 19:36 EEHg/L70 4/26/19SM21-22 6200B5001,3,5-Trimethylbenzene
ND 10000 4/26/19 19:36 EEHg/L5100 4/26/19SM21-22 6200B500L-04Vinyl Acetate
ND 250 4/26/19 19:36 EEHg/L220 4/26/19SM21-22 6200B500Vinyl Chloride
2200 500 4/26/19 19:36 EEHg/L150 4/26/19SM21-22 6200B500m+p Xylene
2600 250 4/26/19 19:36 EEHg/L85 4/26/19SM21-22 6200B500o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.2 4/26/19 19:3670-130
Toluene-d8 97.4 4/26/19 19:3670-130
4-Bromofluorobenzene 99.4 4/26/19 19:3670-130
Page 41 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-17
Field Sample #: DW-1
Sample Matrix: Ground Water
Sampled: 4/18/2019 12:48
[TOC_2]19D1069-17[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: PR-10, RL-11 Volatile Organic Compounds by GC/MS
ND 50000 4/26/19 20:03 EEHg/L3800 4/26/19SM21-22 6200B1000Acetone
220 500 4/26/19 20:03 EEHg/L180 4/26/19SM21-22 6200B1000JBenzene
ND 500 4/26/19 20:03 EEHg/L150 4/26/19SM21-22 6200B1000Bromobenzene
ND 500 4/26/19 20:03 EEHg/L320 4/26/19SM21-22 6200B1000Bromochloromethane
ND 500 4/26/19 20:03 EEHg/L160 4/26/19SM21-22 6200B1000Bromodichloromethane
ND 2000 4/26/19 20:03 EEHg/L460 4/26/19SM21-22 6200B1000Bromoform
ND 2000 4/26/19 20:03 EEHg/L780 4/26/19SM21-22 6200B1000Bromomethane
ND 5000 4/26/19 20:03 EEHg/L1900 4/26/19SM21-22 6200B10002-Butanone (MEK)
ND 500 4/26/19 20:03 EEHg/L210 4/26/19SM21-22 6200B1000n-Butylbenzene
ND 500 4/26/19 20:03 EEHg/L160 4/26/19SM21-22 6200B1000sec-Butylbenzene
ND 500 4/26/19 20:03 EEHg/L170 4/26/19SM21-22 6200B1000tert-Butylbenzene
ND 500 4/26/19 20:03 EEHg/L110 4/26/19SM21-22 6200B1000Carbon Tetrachloride
ND 500 4/26/19 20:03 EEHg/L150 4/26/19SM21-22 6200B1000Chlorobenzene
ND 500 4/26/19 20:03 EEHg/L210 4/26/19SM21-22 6200B1000Chlorodibromomethane
ND 500 4/26/19 20:03 EEHg/L350 4/26/19SM21-22 6200B1000Chloroethane
ND 500 4/26/19 20:03 EEHg/L170 4/26/19SM21-22 6200B1000Chloroform
ND 600 4/26/19 20:03 EEHg/L450 4/26/19SM21-22 6200B1000Chloromethane
ND 500 4/26/19 20:03 EEHg/L120 4/26/19SM21-22 6200B10002-Chlorotoluene
ND 500 4/26/19 20:03 EEHg/L140 4/26/19SM21-22 6200B10004-Chlorotoluene
ND 500 4/26/19 20:03 EEHg/L190 4/26/19SM21-22 6200B10001,2-Dibromoethane (EDB)
ND 500 4/26/19 20:03 EEHg/L160 4/26/19SM21-22 6200B10001,2-Dichlorobenzene
ND 500 4/26/19 20:03 EEHg/L120 4/26/19SM21-22 6200B10001,3-Dichlorobenzene
ND 500 4/26/19 20:03 EEHg/L130 4/26/19SM21-22 6200B10001,4-Dichlorobenzene
ND 500 4/26/19 20:03 EEHg/L260 4/26/19SM21-22 6200B1000Dichlorodifluoromethane (Freon 12)
ND 500 4/26/19 20:03 EEHg/L160 4/26/19SM21-22 6200B10001,1-Dichloroethane
ND 500 4/26/19 20:03 EEHg/L410 4/26/19SM21-22 6200B10001,2-Dichloroethane
ND 500 4/26/19 20:03 EEHg/L320 4/26/19SM21-22 6200B10001,1-Dichloroethylene
ND 500 4/26/19 20:03 EEHg/L130 4/26/19SM21-22 6200B1000cis-1,2-Dichloroethylene
ND 500 4/26/19 20:03 EEHg/L310 4/26/19SM21-22 6200B1000trans-1,2-Dichloroethylene
ND 500 4/26/19 20:03 EEHg/L200 4/26/19SM21-22 6200B10001,2-Dichloropropane
ND 500 4/26/19 20:03 EEHg/L110 4/26/19SM21-22 6200B10001,3-Dichloropropane
ND 500 4/26/19 20:03 EEHg/L200 4/26/19SM21-22 6200B10002,2-Dichloropropane
ND 500 4/26/19 20:03 EEHg/L160 4/26/19SM21-22 6200B10001,1-Dichloropropene
ND 500 4/26/19 20:03 EEHg/L130 4/26/19SM21-22 6200B1000cis-1,3-Dichloropropene
ND 500 4/26/19 20:03 EEHg/L230 4/26/19SM21-22 6200B1000trans-1,3-Dichloropropene
780 500 4/26/19 20:03 EEHg/L170 4/26/19SM21-22 6200B1000Diisopropyl Ether (DIPE)
ND 500 4/26/19 20:03 EEHg/L130 4/26/19SM21-22 6200B1000Ethylbenzene
ND 5000 4/26/19 20:03 EEHg/L1500 4/26/19SM21-22 6200B10002-Hexanone (MBK)
ND 500 4/26/19 20:03 EEHg/L170 4/26/19SM21-22 6200B1000Isopropylbenzene (Cumene)
ND 500 4/26/19 20:03 EEHg/L200 4/26/19SM21-22 6200B1000p-Isopropyltoluene (p-Cymene)
88000 500 4/26/19 20:03 EEHg/L250 4/26/19SM21-22 6200B1000Methyl tert-Butyl Ether (MTBE)
ND 5000 4/26/19 20:03 EEHg/L340 4/26/19SM21-22 6200B1000Methylene Chloride
ND 5000 4/26/19 20:03 EEHg/L1700 4/26/19SM21-22 6200B10004-Methyl-2-pentanone (MIBK)
ND 2000 4/26/19 20:03 EEHg/L310 4/26/19SM21-22 6200B1000Naphthalene
Page 42 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-17
Field Sample #: DW-1
Sample Matrix: Ground Water
Sampled: 4/18/2019 12:48
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: PR-10, RL-11 Volatile Organic Compounds by GC/MS
ND 500 4/26/19 20:03 EEHg/L130 4/26/19SM21-22 6200B1000n-Propylbenzene
ND 500 4/26/19 20:03 EEHg/L110 4/26/19SM21-22 6200B1000Styrene
ND 500 4/26/19 20:03 EEHg/L220 4/26/19SM21-22 6200B10001,1,2,2-Tetrachloroethane
ND 500 4/26/19 20:03 EEHg/L180 4/26/19SM21-22 6200B1000Tetrachloroethylene
ND 500 4/26/19 20:03 EEHg/L140 4/26/19SM21-22 6200B1000Toluene
ND 5000 4/26/19 20:03 EEHg/L570 4/26/19SM21-22 6200B10001,2,3-Trichlorobenzene
ND 2000 4/26/19 20:03 EEHg/L400 4/26/19SM21-22 6200B10001,2,4-Trichlorobenzene
ND 500 4/26/19 20:03 EEHg/L200 4/26/19SM21-22 6200B10001,1,1-Trichloroethane
ND 500 4/26/19 20:03 EEHg/L160 4/26/19SM21-22 6200B10001,1,2-Trichloroethane
ND 500 4/26/19 20:03 EEHg/L240 4/26/19SM21-22 6200B1000Trichloroethylene
ND 500 4/26/19 20:03 EEHg/L330 4/26/19SM21-22 6200B1000Trichlorofluoromethane (Freon 11)
ND 500 4/26/19 20:03 EEHg/L250 4/26/19SM21-22 6200B10001,2,3-Trichloropropane
ND 500 4/26/19 20:03 EEHg/L180 4/26/19SM21-22 6200B10001,2,4-Trimethylbenzene
ND 500 4/26/19 20:03 EEHg/L140 4/26/19SM21-22 6200B10001,3,5-Trimethylbenzene
ND 20000 4/26/19 20:03 EEHg/L10000 4/26/19SM21-22 6200B1000L-04Vinyl Acetate
ND 500 4/26/19 20:03 EEHg/L450 4/26/19SM21-22 6200B1000Vinyl Chloride
ND 1000 4/26/19 20:03 EEHg/L300 4/26/19SM21-22 6200B1000m+p Xylene
ND 500 4/26/19 20:03 EEHg/L170 4/26/19SM21-22 6200B1000o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.3 4/26/19 20:0370-130
Toluene-d8 98.2 4/26/19 20:0370-130
4-Bromofluorobenzene 97.8 4/26/19 20:0370-130
Page 43 of 65
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-18
Field Sample #: PW-3R
Sample Matrix: Ground Water
Sampled: 4/18/2019 13:46
[TOC_2]19D1069-18[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 500 4/26/19 19:09 EEHg/L38 4/26/19SM21-22 6200B10Acetone
ND 5.0 4/26/19 19:09 EEHg/L1.8 4/26/19SM21-22 6200B10Benzene
ND 5.0 4/26/19 19:09 EEHg/L1.5 4/26/19SM21-22 6200B10Bromobenzene
ND 5.0 4/26/19 19:09 EEHg/L3.2 4/26/19SM21-22 6200B10Bromochloromethane
ND 5.0 4/26/19 19:09 EEHg/L1.6 4/26/19SM21-22 6200B10Bromodichloromethane
ND 20 4/26/19 19:09 EEHg/L4.6 4/26/19SM21-22 6200B10Bromoform
ND 20 4/26/19 19:09 EEHg/L7.8 4/26/19SM21-22 6200B10Bromomethane
ND 50 4/26/19 19:09 EEHg/L19 4/26/19SM21-22 6200B102-Butanone (MEK)
ND 5.0 4/26/19 19:09 EEHg/L2.1 4/26/19SM21-22 6200B10n-Butylbenzene
ND 5.0 4/26/19 19:09 EEHg/L1.6 4/26/19SM21-22 6200B10sec-Butylbenzene
ND 5.0 4/26/19 19:09 EEHg/L1.7 4/26/19SM21-22 6200B10tert-Butylbenzene
ND 5.0 4/26/19 19:09 EEHg/L1.1 4/26/19SM21-22 6200B10Carbon Tetrachloride
ND 5.0 4/26/19 19:09 EEHg/L1.5 4/26/19SM21-22 6200B10Chlorobenzene
ND 5.0 4/26/19 19:09 EEHg/L2.1 4/26/19SM21-22 6200B10Chlorodibromomethane
ND 5.0 4/26/19 19:09 EEHg/L3.5 4/26/19SM21-22 6200B10Chloroethane
ND 5.0 4/26/19 19:09 EEHg/L1.7 4/26/19SM21-22 6200B10Chloroform
ND 6.0 4/26/19 19:09 EEHg/L4.5 4/26/19SM21-22 6200B10Chloromethane
ND 5.0 4/26/19 19:09 EEHg/L1.2 4/26/19SM21-22 6200B102-Chlorotoluene
ND 5.0 4/26/19 19:09 EEHg/L1.4 4/26/19SM21-22 6200B104-Chlorotoluene
ND 5.0 4/26/19 19:09 EEHg/L1.9 4/26/19SM21-22 6200B101,2-Dibromoethane (EDB)
ND 5.0 4/26/19 19:09 EEHg/L1.6 4/26/19SM21-22 6200B101,2-Dichlorobenzene
ND 5.0 4/26/19 19:09 EEHg/L1.2 4/26/19SM21-22 6200B101,3-Dichlorobenzene
ND 5.0 4/26/19 19:09 EEHg/L1.3 4/26/19SM21-22 6200B101,4-Dichlorobenzene
ND 5.0 4/26/19 19:09 EEHg/L2.6 4/26/19SM21-22 6200B10Dichlorodifluoromethane (Freon 12)
ND 5.0 4/26/19 19:09 EEHg/L1.6 4/26/19SM21-22 6200B101,1-Dichloroethane
ND 5.0 4/26/19 19:09 EEHg/L4.1 4/26/19SM21-22 6200B101,2-Dichloroethane
ND 5.0 4/26/19 19:09 EEHg/L3.2 4/26/19SM21-22 6200B101,1-Dichloroethylene
ND 5.0 4/26/19 19:09 EEHg/L1.3 4/26/19SM21-22 6200B10cis-1,2-Dichloroethylene
ND 5.0 4/26/19 19:09 EEHg/L3.1 4/26/19SM21-22 6200B10trans-1,2-Dichloroethylene
ND 5.0 4/26/19 19:09 EEHg/L2.0 4/26/19SM21-22 6200B101,2-Dichloropropane
ND 5.0 4/26/19 19:09 EEHg/L1.1 4/26/19SM21-22 6200B101,3-Dichloropropane
ND 5.0 4/26/19 19:09 EEHg/L2.0 4/26/19SM21-22 6200B102,2-Dichloropropane
ND 5.0 4/26/19 19:09 EEHg/L1.6 4/26/19SM21-22 6200B101,1-Dichloropropene
ND 5.0 4/26/19 19:09 EEHg/L1.3 4/26/19SM21-22 6200B10cis-1,3-Dichloropropene
ND 5.0 4/26/19 19:09 EEHg/L2.3 4/26/19SM21-22 6200B10trans-1,3-Dichloropropene
23 5.0 4/26/19 19:09 EEHg/L1.7 4/26/19SM21-22 6200B10Diisopropyl Ether (DIPE)
ND 5.0 4/26/19 19:09 EEHg/L1.3 4/26/19SM21-22 6200B10Ethylbenzene
ND 50 4/26/19 19:09 EEHg/L15 4/26/19SM21-22 6200B102-Hexanone (MBK)
ND 5.0 4/26/19 19:09 EEHg/L1.7 4/26/19SM21-22 6200B10Isopropylbenzene (Cumene)
ND 5.0 4/26/19 19:09 EEHg/L2.0 4/26/19SM21-22 6200B10p-Isopropyltoluene (p-Cymene)
930 5.0 4/26/19 19:09 EEHg/L2.5 4/26/19SM21-22 6200B10Methyl tert-Butyl Ether (MTBE)
ND 50 4/26/19 19:09 EEHg/L3.4 4/26/19SM21-22 6200B10Methylene Chloride
ND 50 4/26/19 19:09 EEHg/L17 4/26/19SM21-22 6200B104-Methyl-2-pentanone (MIBK)
ND 20 4/26/19 19:09 EEHg/L3.1 4/26/19SM21-22 6200B10Naphthalene
Page 44 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/19/2019
Work Order: 19D1069Sample Description:Project Location: Roxboro, NC
Sample ID: 19D1069-18
Field Sample #: PW-3R
Sample Matrix: Ground Water
Sampled: 4/18/2019 13:46
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 5.0 4/26/19 19:09 EEHg/L1.3 4/26/19SM21-22 6200B10n-Propylbenzene
ND 5.0 4/26/19 19:09 EEHg/L1.1 4/26/19SM21-22 6200B10Styrene
ND 5.0 4/26/19 19:09 EEHg/L2.2 4/26/19SM21-22 6200B101,1,2,2-Tetrachloroethane
ND 5.0 4/26/19 19:09 EEHg/L1.8 4/26/19SM21-22 6200B10Tetrachloroethylene
ND 5.0 4/26/19 19:09 EEHg/L1.4 4/26/19SM21-22 6200B10Toluene
ND 50 4/26/19 19:09 EEHg/L5.7 4/26/19SM21-22 6200B101,2,3-Trichlorobenzene
ND 20 4/26/19 19:09 EEHg/L4.0 4/26/19SM21-22 6200B101,2,4-Trichlorobenzene
ND 5.0 4/26/19 19:09 EEHg/L2.0 4/26/19SM21-22 6200B101,1,1-Trichloroethane
ND 5.0 4/26/19 19:09 EEHg/L1.6 4/26/19SM21-22 6200B101,1,2-Trichloroethane
ND 5.0 4/26/19 19:09 EEHg/L2.4 4/26/19SM21-22 6200B10Trichloroethylene
ND 5.0 4/26/19 19:09 EEHg/L3.3 4/26/19SM21-22 6200B10Trichlorofluoromethane (Freon 11)
ND 5.0 4/26/19 19:09 EEHg/L2.5 4/26/19SM21-22 6200B101,2,3-Trichloropropane
ND 5.0 4/26/19 19:09 EEHg/L1.8 4/26/19SM21-22 6200B101,2,4-Trimethylbenzene
ND 5.0 4/26/19 19:09 EEHg/L1.4 4/26/19SM21-22 6200B101,3,5-Trimethylbenzene
ND 200 4/26/19 19:09 EEHg/L100 4/26/19SM21-22 6200B10L-04Vinyl Acetate
ND 5.0 4/26/19 19:09 EEHg/L4.5 4/26/19SM21-22 6200B10Vinyl Chloride
ND 10 4/26/19 19:09 EEHg/L3.0 4/26/19SM21-22 6200B10m+p Xylene
ND 5.0 4/26/19 19:09 EEHg/L1.7 4/26/19SM21-22 6200B10o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.6 4/26/19 19:0970-130
Toluene-d8 98.3 4/26/19 19:0970-130
4-Bromofluorobenzene 98.3 4/26/19 19:0970-130
Page 45 of 65
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B229012 04/23/195 5.0019D1069-01 [Field Blank]
B229012 04/23/190.025 5.0019D1069-02 [MW-5]
B229012 04/23/195 5.0019D1069-03 [MW-6]
B229012 04/23/190.05 5.0019D1069-04 [MW-7]
B229012 04/23/1955.0019D1069-05 [MW-8]
B229012 04/23/1955.0019D1069-06 [MW-9]
B229012 04/23/1955.0019D1069-07 [MW-10]
B229012 04/23/190.01 5.0019D1069-08 [MW-11]
B229012 04/23/1955.0019D1069-09 [MW-12]
B229012 04/23/1955.0019D1069-10 [WSW-2]
B229012 04/23/1955.0019D1069-11 [WSW-3]
B229012 04/23/1955.0019D1069-12 [PW-4B]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B229074 04/23/190.2 5.0019D1069-09RE1 [MW-12]
B229074 04/25/1955.0019D1069-14 [MW-2]
B229074 04/25/1955.0019D1069-15 [MW-3]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B229194 04/26/190.2 5.0019D1069-05RE1 [MW-8]
B229194 04/26/190.25 5.0019D1069-13 [MW-1]
B229194 04/26/190.01 5.0019D1069-16 [MW-4]
B229194 04/26/190.005 5.0019D1069-17 [DW-1]
B229194 04/26/190.5 5.0019D1069-18 [PW-3R]
[TOC_1]Sample Preparation Information[TOC]
Page 46 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B229012 - SW-846 5030B
[TOC_3]B229012[TOC]
Blank (B229012-BLK1) Prepared & Analyzed: 04/24/19
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
[TOC_1]QC Data[TOC]
Page 47 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B229012 - SW-846 5030B
Blank (B229012-BLK1) Prepared & Analyzed: 04/24/19
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 86.321.6
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 99.324.8
LCS (B229012-BS1) Prepared & Analyzed: 04/24/19
Acetone g/L50 100 70-130118118
Benzene g/L0.50 10.0 70-13097.59.75
Bromobenzene g/L0.50 10.0 70-13011611.6
Bromochloromethane g/L0.50 10.0 70-13010610.6
Bromodichloromethane g/L0.50 10.0 70-13010610.6
Bromoform g/L0.50 10.0 70-13012412.4
Bromomethane g/L1.0 10.0 60-14083.68.36
2-Butanone (MEK)g/L5.0 100 70-13085.385.3
n-Butylbenzene g/L0.50 10.0 70-13011111.1
sec-Butylbenzene g/L0.50 10.0 70-13011411.4
tert-Butylbenzene g/L0.50 10.0 70-13011311.3
Carbon Tetrachloride g/L0.50 10.0 70-13098.39.83
Chlorobenzene g/L0.50 10.0 70-13011911.9
Chlorodibromomethane g/L0.50 10.0 70-13011411.4
Chloroethane g/L0.50 10.0 60-14012212.2
Chloroform g/L0.50 10.0 70-13093.79.37
Chloromethane g/L0.60 10.0 60-14089.78.97
2-Chlorotoluene g/L0.50 10.0 70-13010810.8
4-Chlorotoluene g/L0.50 10.0 70-13011811.8
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13011411.4
1,2-Dichlorobenzene g/L0.50 10.0 70-13011511.5
1,3-Dichlorobenzene g/L0.50 10.0 70-13011611.6
1,4-Dichlorobenzene g/L0.50 10.0 70-13011111.1
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14085.38.53
1,1-Dichloroethane g/L0.50 10.0 70-13093.29.32
1,2-Dichloroethane g/L0.50 10.0 70-13088.18.81
1,1-Dichloroethylene g/L0.50 10.0 70-13010710.7
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13098.19.81
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13097.99.79
1,2-Dichloropropane g/L0.50 10.0 70-13010510.5
1,3-Dichloropropane g/L0.50 10.0 70-13010510.5
2,2-Dichloropropane g/L0.50 10.0 70-13095.89.58
1,1-Dichloropropene g/L0.50 10.0 70-13096.29.62
cis-1,3-Dichloropropene g/L0.50 10.0 70-13011811.8
trans-1,3-Dichloropropene g/L0.50 10.0 70-13012012.0
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13011111.1
Ethylbenzene g/L0.50 10.0 70-13011211.2
Page 48 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B229012 - SW-846 5030B
LCS (B229012-BS1) Prepared & Analyzed: 04/24/19
2-Hexanone (MBK)g/L5.0 100 70-130101101
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13011811.8
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13011311.3
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13091.99.19
Methylene Chloride g/L5.0 10.0 70-13011811.8
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130104104
Naphthalene g/L0.50 10.0 70-13087.88.78
n-Propylbenzene g/L0.50 10.0 70-13011911.9
Styrene g/L0.50 10.0 70-13012912.9
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13011911.9
Tetrachloroethylene g/L0.50 10.0 70-13011211.2
Toluene g/L0.50 10.0 70-13011011.0
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13010010.0
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13095.69.56
1,1,1-Trichloroethane g/L0.50 10.0 70-13093.59.35
1,1,2-Trichloroethane g/L0.50 10.0 70-13011011.0
Trichloroethylene g/L0.50 10.0 70-13010410.4
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13095.29.52
1,2,3-Trichloropropane g/L0.50 10.0 70-13010610.6
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13011011.0
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13011411.4
Vinyl Acetate g/L20 100 70-13070.570.5
Vinyl Chloride g/L0.50 10.0 L-0260-140169*16.9
m+p Xylene g/L1.0 20.0 70-13011723.5
o-Xylene g/L0.50 10.0 70-13012312.3
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 85.221.3
g/L 25.0 70-130Surrogate: Toluene-d8 99.824.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10626.4
LCS Dup (B229012-BSD1) Prepared & Analyzed: 04/24/19
Acetone g/L50 100 2570-130116 1.28116
Benzene g/L0.50 10.0 2570-13093.5 4.199.35
Bromobenzene g/L0.50 10.0 2570-130113 2.1011.3
Bromochloromethane g/L0.50 10.0 2570-130110 3.4211.0
Bromodichloromethane g/L0.50 10.0 2570-130107 0.46910.7
Bromoform g/L0.50 10.0 2570-130118 5.2111.8
Bromomethane g/L1.0 10.0 2560-14087.5 4.568.75
2-Butanone (MEK)g/L5.0 100 2570-13084.9 0.43584.9
n-Butylbenzene g/L0.50 10.0 2570-130107 3.5810.7
sec-Butylbenzene g/L0.50 10.0 2570-130110 3.6511.0
tert-Butylbenzene g/L0.50 10.0 2570-130109 3.9710.9
Carbon Tetrachloride g/L0.50 10.0 2570-13093.5 5.019.35
Chlorobenzene g/L0.50 10.0 2570-130117 2.2011.7
Chlorodibromomethane g/L0.50 10.0 2570-130114 0.17611.4
Chloroethane g/L0.50 10.0 2560-140110 10.911.0
Chloroform g/L0.50 10.0 2570-13092.0 1.839.20
Chloromethane g/L0.60 10.0 2560-14088.5 1.358.85
2-Chlorotoluene g/L0.50 10.0 2570-130108 0.64710.8
4-Chlorotoluene g/L0.50 10.0 2570-130116 1.7911.6
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130111 2.2311.1
1,2-Dichlorobenzene g/L0.50 10.0 2570-130113 2.2811.3
1,3-Dichlorobenzene g/L0.50 10.0 2570-130114 1.7411.4
Page 49 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B229012 - SW-846 5030B
LCS Dup (B229012-BSD1) Prepared & Analyzed: 04/24/19
1,4-Dichlorobenzene g/L0.50 10.0 2570-130110 0.81611.0
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14078.8 7.927.88
1,1-Dichloroethane g/L0.50 10.0 2570-13089.9 3.608.99
1,2-Dichloroethane g/L0.50 10.0 2570-13085.6 2.888.56
1,1-Dichloroethylene g/L0.50 10.0 2570-130101 5.0910.1
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13096.9 1.239.69
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13095.1 2.909.51
1,2-Dichloropropane g/L0.50 10.0 2570-130105 0.19110.5
1,3-Dichloropropane g/L0.50 10.0 2570-130103 2.2110.3
2,2-Dichloropropane g/L0.50 10.0 2570-13092.0 4.059.20
1,1-Dichloropropene g/L0.50 10.0 2570-13091.0 5.569.10
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130117 1.1911.7
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130118 1.9311.8
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130109 1.6410.9
Ethylbenzene g/L0.50 10.0 2570-130113 0.35511.3
2-Hexanone (MBK)g/L5.0 100 2570-130102 1.24102
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130116 1.6311.6
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130109 3.5110.9
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13092.7 0.8679.27
Methylene Chloride g/L5.0 10.0 2570-130115 2.9111.5
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130103 0.339103
Naphthalene g/L0.50 10.0 2570-13089.9 2.368.99
n-Propylbenzene g/L0.50 10.0 2570-130115 2.8211.5
Styrene g/L0.50 10.0 2570-130126 2.0412.6
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130116 2.1311.6
Tetrachloroethylene g/L0.50 10.0 2570-130108 3.0010.8
Toluene g/L0.50 10.0 2570-130108 1.7510.8
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130104 3.0410.4
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13097.0 1.459.70
1,1,1-Trichloroethane g/L0.50 10.0 2570-13090.1 3.709.01
1,1,2-Trichloroethane g/L0.50 10.0 2570-130110 0.45511.0
Trichloroethylene g/L0.50 10.0 2570-130101 2.7310.1
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13090.7 4.849.07
1,2,3-Trichloropropane g/L0.50 10.0 2570-130106 0.47110.6
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130109 1.0910.9
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130114 0.78911.4
Vinyl Acetate g/L20 100 2570-13073.5 4.2473.5
Vinyl Chloride g/L0.50 10.0 25 L-0260-140166 1.49*16.6
m+p Xylene g/L1.0 20.0 2570-130115 1.7623.1
o-Xylene g/L0.50 10.0 2570-130118 3.4011.8
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 88.522.1
g/L 25.0 70-130Surrogate: Toluene-d8 99.024.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10526.2
Page 50 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B229074 - SW-846 5030B
[TOC_3]B229074[TOC]
Blank (B229074-BLK1) Prepared: 04/25/19 Analyzed: 04/26/19
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
Page 51 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B229074 - SW-846 5030B
Blank (B229074-BLK1) Prepared: 04/25/19 Analyzed: 04/26/19
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20 L-04ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 94.023.5
g/L 25.0 70-130Surrogate: Toluene-d8 99.424.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 99.824.9
LCS (B229074-BS1) Prepared & Analyzed: 04/25/19
Acetone g/L50 100 70-130100100
Benzene g/L0.50 10.0 70-13093.59.35
Bromobenzene g/L0.50 10.0 70-13012012.0
Bromochloromethane g/L0.50 10.0 70-13010610.6
Bromodichloromethane g/L0.50 10.0 70-13010610.6
Bromoform g/L0.50 10.0 70-13012212.2
Bromomethane g/L1.0 10.0 60-14080.38.03
2-Butanone (MEK)g/L5.0 100 70-13081.081.0
n-Butylbenzene g/L0.50 10.0 70-13011511.5
sec-Butylbenzene g/L0.50 10.0 70-13011711.7
tert-Butylbenzene g/L0.50 10.0 70-13011211.2
Carbon Tetrachloride g/L0.50 10.0 70-13096.89.68
Chlorobenzene g/L0.50 10.0 70-13012512.5
Chlorodibromomethane g/L0.50 10.0 70-13011411.4
Chloroethane g/L0.50 10.0 60-14011311.3
Chloroform g/L0.50 10.0 70-13092.49.24
Chloromethane g/L0.60 10.0 60-14081.08.10
2-Chlorotoluene g/L0.50 10.0 70-13011411.4
4-Chlorotoluene g/L0.50 10.0 70-13012212.2
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010810.8
1,2-Dichlorobenzene g/L0.50 10.0 70-13012012.0
1,3-Dichlorobenzene g/L0.50 10.0 70-13012312.3
1,4-Dichlorobenzene g/L0.50 10.0 70-13012012.0
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14072.67.26
1,1-Dichloroethane g/L0.50 10.0 70-13091.49.14
1,2-Dichloroethane g/L0.50 10.0 70-13087.98.79
1,1-Dichloroethylene g/L0.50 10.0 70-13010310.3
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13095.39.53
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13094.39.43
1,2-Dichloropropane g/L0.50 10.0 70-13099.19.91
1,3-Dichloropropane g/L0.50 10.0 70-13010410.4
2,2-Dichloropropane g/L0.50 10.0 70-13076.27.62
1,1-Dichloropropene g/L0.50 10.0 70-13090.39.03
cis-1,3-Dichloropropene g/L0.50 10.0 70-13011111.1
trans-1,3-Dichloropropene g/L0.50 10.0 70-13011011.0
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010510.5
Ethylbenzene g/L0.50 10.0 70-13011511.5
Page 52 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B229074 - SW-846 5030B
LCS (B229074-BS1) Prepared & Analyzed: 04/25/19
2-Hexanone (MBK)g/L5.0 100 70-13095.895.8
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13012012.0
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13011611.6
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13089.08.90
Methylene Chloride g/L5.0 10.0 70-13011511.5
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130101101
Naphthalene g/L0.50 10.0 70-13087.78.77
n-Propylbenzene g/L0.50 10.0 70-13012012.0
Styrene g/L0.50 10.0 70-13013013.0
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13012012.0
Tetrachloroethylene g/L0.50 10.0 70-13011111.1
Toluene g/L0.50 10.0 70-13010110.1
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13010710.7
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13010210.2
1,1,1-Trichloroethane g/L0.50 10.0 70-13094.29.42
1,1,2-Trichloroethane g/L0.50 10.0 70-13011011.0
Trichloroethylene g/L0.50 10.0 70-13010310.3
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13091.89.18
1,2,3-Trichloropropane g/L0.50 10.0 70-13010910.9
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13011411.4
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13011911.9
Vinyl Acetate g/L20 100 L-0470-13065.2 *65.2
Vinyl Chloride g/L0.50 10.0 L-0260-140162*16.2
m+p Xylene g/L1.0 20.0 70-13011823.6
o-Xylene g/L0.50 10.0 70-13012212.2
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 93.123.3
g/L 25.0 70-130Surrogate: Toluene-d8 98.424.6
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10426.0
LCS Dup (B229074-BSD1) Prepared: 04/25/19 Analyzed: 04/26/19
Acetone g/L50 100 2570-130115 13.6115
Benzene g/L0.50 10.0 2570-13090.0 3.819.00
Bromobenzene g/L0.50 10.0 2570-130119 0.25111.9
Bromochloromethane g/L0.50 10.0 2570-130106 0.18810.6
Bromodichloromethane g/L0.50 10.0 2570-130108 1.4910.8
Bromoform g/L0.50 10.0 2570-130121 0.16512.1
Bromomethane g/L1.0 10.0 2560-14086.3 7.208.63
2-Butanone (MEK)g/L5.0 100 2570-13089.3 9.6689.3
n-Butylbenzene g/L0.50 10.0 2570-130112 2.4711.2
sec-Butylbenzene g/L0.50 10.0 2570-130118 0.76711.8
tert-Butylbenzene g/L0.50 10.0 2570-130113 1.1611.3
Carbon Tetrachloride g/L0.50 10.0 2570-13093.3 3.689.33
Chlorobenzene g/L0.50 10.0 2570-130122 3.0012.2
Chlorodibromomethane g/L0.50 10.0 2570-130115 1.2211.5
Chloroethane g/L0.50 10.0 2560-140106 6.5610.6
Chloroform g/L0.50 10.0 2570-13090.5 2.089.05
Chloromethane g/L0.60 10.0 2560-14079.1 2.377.91
2-Chlorotoluene g/L0.50 10.0 2570-130107 6.2610.7
4-Chlorotoluene g/L0.50 10.0 2570-130118 3.7511.8
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130108 0.18610.8
1,2-Dichlorobenzene g/L0.50 10.0 2570-130124 2.9512.4
1,3-Dichlorobenzene g/L0.50 10.0 2570-130124 0.89312.4
Page 53 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B229074 - SW-846 5030B
LCS Dup (B229074-BSD1) Prepared: 04/25/19 Analyzed: 04/26/19
1,4-Dichlorobenzene g/L0.50 10.0 2570-130121 1.0812.1
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14068.7 5.526.87
1,1-Dichloroethane g/L0.50 10.0 2570-13088.2 3.568.82
1,2-Dichloroethane g/L0.50 10.0 2570-13089.5 1.808.95
1,1-Dichloroethylene g/L0.50 10.0 2570-13099.0 4.069.90
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13094.5 0.8439.45
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13090.0 4.679.00
1,2-Dichloropropane g/L0.50 10.0 2570-13099.2 0.1019.92
1,3-Dichloropropane g/L0.50 10.0 2570-130104 0.86510.4
2,2-Dichloropropane g/L0.50 10.0 2570-13073.1 4.157.31
1,1-Dichloropropene g/L0.50 10.0 2570-13087.0 3.728.70
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130108 3.3810.8
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130113 2.4111.3
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130108 2.4410.8
Ethylbenzene g/L0.50 10.0 2570-130112 2.2911.2
2-Hexanone (MBK)g/L5.0 100 2570-130104 8.50104
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130116 3.9011.6
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130115 1.2111.5
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13091.9 3.219.19
Methylene Chloride g/L5.0 10.0 2570-130113 1.0511.3
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130108 6.07108
Naphthalene g/L0.50 10.0 2570-13092.6 5.449.26
n-Propylbenzene g/L0.50 10.0 2570-130117 2.5311.7
Styrene g/L0.50 10.0 2570-130125 3.9212.5
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130123 2.0612.3
Tetrachloroethylene g/L0.50 10.0 2570-130109 1.2710.9
Toluene g/L0.50 10.0 2570-13099.5 1.799.95
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130112 4.9311.2
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130106 3.3610.6
1,1,1-Trichloroethane g/L0.50 10.0 2570-13090.0 4.569.00
1,1,2-Trichloroethane g/L0.50 10.0 2570-130111 0.90311.1
Trichloroethylene g/L0.50 10.0 2570-13098.1 4.589.81
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13087.4 4.918.74
1,2,3-Trichloropropane g/L0.50 10.0 2570-130112 2.8911.2
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130110 3.3111.0
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130115 3.0811.5
Vinyl Acetate g/L20 100 25 L-0470-13064.0 1.84*64.0
Vinyl Chloride g/L0.50 10.0 25 L-0260-140155 4.41*15.5
m+p Xylene g/L1.0 20.0 2570-130114 3.1922.8
o-Xylene g/L0.50 10.0 2570-130120 2.1512.0
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 93.323.3
g/L 25.0 70-130Surrogate: Toluene-d8 98.624.6
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10225.6
Page 54 of 65
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B229194 - SW-846 5030B
[TOC_3]B229194[TOC]
Blank (B229194-BLK1) Prepared & Analyzed: 04/26/19
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B229194 - SW-846 5030B
Blank (B229194-BLK1) Prepared & Analyzed: 04/26/19
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20 L-04ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 90.522.6
g/L 25.0 70-130Surrogate: Toluene-d8 98.124.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.224.5
LCS (B229194-BS1) Prepared & Analyzed: 04/26/19
Acetone g/L50 100 70-130108108
Benzene g/L0.50 10.0 70-13090.59.05
Bromobenzene g/L0.50 10.0 70-13011411.4
Bromochloromethane g/L0.50 10.0 70-13010010.0
Bromodichloromethane g/L0.50 10.0 70-13010010.0
Bromoform g/L0.50 10.0 70-13011711.7
Bromomethane g/L1.0 10.0 60-14080.48.04
2-Butanone (MEK)g/L5.0 100 70-13079.179.1
n-Butylbenzene g/L0.50 10.0 70-13011111.1
sec-Butylbenzene g/L0.50 10.0 70-13011311.3
tert-Butylbenzene g/L0.50 10.0 70-13011211.2
Carbon Tetrachloride g/L0.50 10.0 70-13092.19.21
Chlorobenzene g/L0.50 10.0 70-13011811.8
Chlorodibromomethane g/L0.50 10.0 70-13010610.6
Chloroethane g/L0.50 10.0 60-14010110.1
Chloroform g/L0.50 10.0 70-13088.48.84
Chloromethane g/L0.60 10.0 60-14076.77.67
2-Chlorotoluene g/L0.50 10.0 70-13010410.4
4-Chlorotoluene g/L0.50 10.0 70-13011411.4
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010610.6
1,2-Dichlorobenzene g/L0.50 10.0 70-13011811.8
1,3-Dichlorobenzene g/L0.50 10.0 70-13011711.7
1,4-Dichlorobenzene g/L0.50 10.0 70-13011411.4
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14064.66.46
1,1-Dichloroethane g/L0.50 10.0 70-13085.38.53
1,2-Dichloroethane g/L0.50 10.0 70-13084.98.49
1,1-Dichloroethylene g/L0.50 10.0 70-13096.99.69
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13092.29.22
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13088.58.85
1,2-Dichloropropane g/L0.50 10.0 70-13099.99.99
1,3-Dichloropropane g/L0.50 10.0 70-13097.59.75
2,2-Dichloropropane g/L0.50 10.0 70-13090.09.00
1,1-Dichloropropene g/L0.50 10.0 70-13087.48.74
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010710.7
trans-1,3-Dichloropropene g/L0.50 10.0 70-13010710.7
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13098.79.87
Ethylbenzene g/L0.50 10.0 70-13011411.4
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B229194 - SW-846 5030B
LCS (B229194-BS1) Prepared & Analyzed: 04/26/19
2-Hexanone (MBK)g/L5.0 100 70-13093.893.8
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13011711.7
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13011411.4
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13081.98.19
Methylene Chloride g/L5.0 10.0 70-13011011.0
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13097.697.6
Naphthalene g/L0.50 10.0 70-13083.48.34
n-Propylbenzene g/L0.50 10.0 70-13011611.6
Styrene g/L0.50 10.0 70-13012512.5
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13011611.6
Tetrachloroethylene g/L0.50 10.0 70-13010910.9
Toluene g/L0.50 10.0 70-13010110.1
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13010210.2
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13095.89.58
1,1,1-Trichloroethane g/L0.50 10.0 70-13089.18.91
1,1,2-Trichloroethane g/L0.50 10.0 70-13010010.0
Trichloroethylene g/L0.50 10.0 70-13099.09.90
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13086.78.67
1,2,3-Trichloropropane g/L0.50 10.0 70-13010210.2
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010810.8
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13011411.4
Vinyl Acetate g/L20 100 L-0470-13064.5 *64.5
Vinyl Chloride g/L0.50 10.0 L-0260-140145*14.5
m+p Xylene g/L1.0 20.0 70-13011422.8
o-Xylene g/L0.50 10.0 70-13011811.8
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 90.122.5
g/L 25.0 70-130Surrogate: Toluene-d8 98.024.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10125.3
LCS Dup (B229194-BSD1) Prepared & Analyzed: 04/26/19
Acetone g/L50 100 2570-130121 11.9121
Benzene g/L0.50 10.0 2570-13085.4 5.808.54
Bromobenzene g/L0.50 10.0 2570-130112 1.5911.2
Bromochloromethane g/L0.50 10.0 2570-13099.1 1.409.91
Bromodichloromethane g/L0.50 10.0 2570-13099.6 0.5019.96
Bromoform g/L0.50 10.0 2570-130116 0.68811.6
Bromomethane g/L1.0 10.0 2560-14081.9 1.858.19
2-Butanone (MEK)g/L5.0 100 2570-13084.4 6.4184.4
n-Butylbenzene g/L0.50 10.0 2570-130105 5.1810.5
sec-Butylbenzene g/L0.50 10.0 2570-130109 3.9710.9
tert-Butylbenzene g/L0.50 10.0 2570-130107 4.6510.7
Carbon Tetrachloride g/L0.50 10.0 2570-13088.0 4.558.80
Chlorobenzene g/L0.50 10.0 2570-130116 1.9611.6
Chlorodibromomethane g/L0.50 10.0 2570-130108 1.1210.8
Chloroethane g/L0.50 10.0 2560-14097.4 3.939.74
Chloroform g/L0.50 10.0 2570-13085.3 3.578.53
Chloromethane g/L0.60 10.0 2560-14071.7 6.747.17
2-Chlorotoluene g/L0.50 10.0 2570-130105 1.2410.5
4-Chlorotoluene g/L0.50 10.0 2570-130112 1.5011.2
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130102 3.7410.2
1,2-Dichlorobenzene g/L0.50 10.0 2570-130113 4.2411.3
1,3-Dichlorobenzene g/L0.50 10.0 2570-130114 3.2911.4
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B229194 - SW-846 5030B
LCS Dup (B229194-BSD1) Prepared & Analyzed: 04/26/19
1,4-Dichlorobenzene g/L0.50 10.0 2570-130110 3.4911.0
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14060.7 6.236.07
1,1-Dichloroethane g/L0.50 10.0 2570-13080.4 5.918.04
1,2-Dichloroethane g/L0.50 10.0 2570-13080.1 5.828.01
1,1-Dichloroethylene g/L0.50 10.0 2570-13088.5 9.068.85
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13088.2 4.438.82
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13084.6 4.518.46
1,2-Dichloropropane g/L0.50 10.0 2570-13093.9 6.199.39
1,3-Dichloropropane g/L0.50 10.0 2570-13096.9 0.6179.69
2,2-Dichloropropane g/L0.50 10.0 2570-13084.5 6.308.45
1,1-Dichloropropene g/L0.50 10.0 2570-13083.8 4.218.38
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130104 2.9310.4
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130107 0.093210.7
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130103 4.5510.3
Ethylbenzene g/L0.50 10.0 2570-130107 6.1810.7
2-Hexanone (MBK)g/L5.0 100 2570-13096.2 2.4796.2
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130112 4.8911.2
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130108 5.8610.8
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13082.2 0.3668.22
Methylene Chloride g/L5.0 10.0 2570-130102 7.7510.2
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13096.6 1.0296.6
Naphthalene g/L0.50 10.0 2570-13083.9 0.5988.39
n-Propylbenzene g/L0.50 10.0 2570-130110 4.5111.0
Styrene g/L0.50 10.0 2570-130122 2.2612.2
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130114 1.3911.4
Tetrachloroethylene g/L0.50 10.0 2570-130104 4.9010.4
Toluene g/L0.50 10.0 2570-13093.8 7.109.38
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130103 1.0710.3
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13096.3 0.5219.63
1,1,1-Trichloroethane g/L0.50 10.0 2570-13085.5 4.128.55
1,1,2-Trichloroethane g/L0.50 10.0 2570-130102 2.1810.2
Trichloroethylene g/L0.50 10.0 2570-13093.8 5.399.38
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13080.2 7.798.02
1,2,3-Trichloropropane g/L0.50 10.0 2570-130104 1.7510.4
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130104 3.9510.4
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130110 3.7611.0
Vinyl Acetate g/L20 100 25 L-0470-13064.2 0.466*64.2
Vinyl Chloride g/L0.50 10.0 25 L-0260-140141 2.94*14.1
m+p Xylene g/L1.0 20.0 2570-130109 4.3421.9
o-Xylene g/L0.50 10.0 2570-130114 3.7111.4
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 91.522.9
g/L 25.0 70-130Surrogate: Toluene-d8 98.024.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10325.7
Page 58 of 65
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
pH of sample (pH 7) is outside of method specified preservation criteria.PR-10
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,2,2-Tetrachloroethane
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2019
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2019
E871027 NELAPFlorida Department of HealthFL 06/30/2019
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2019
2011028State of MaineME 06/9/2019
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2019
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2019
25703North Carolina Department of HealthNC-DW 07/31/2019
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
May 14, 2019
Matt Gillis
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
Project Location: Roughmont, NC
Client Job Number:
Project Number: 49:3051-E
Laboratory Work Order Number: 19E0276
Enclosed are results of analyses for samples received by the laboratory on May 3, 2019. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 68
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 6
Sample Results 11
19E0276-01 11
19E0276-02 18
19E0276-03 25
19E0276-04 27
Sample Preparation Information 29
QC Data 30
Volatile Organic Compounds by GC/MS 30
B230058 30
B230248 34
B230565 38
Semivolatile Organic Compounds by GC/MS 43
B230431 43
Petroleum Hydrocarbons Analyses - EPH 51
B229933 51
Petroleum Hydrocarbons Analyses - VPH 54
B229919 54
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 56
B230325 56
Flag/Qualifier Summary 57
Certifications 58
Chain of Custody/Sample Receipt 66
Page 2 of 68
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
5/14/2019
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
ATTN: Matt Gillis
49:3051-E
19E0276
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Roughmont, NC
SS-1 19E0276-01 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SW-846 8260D
SW-846 8270E
SS-2 19E0276-02 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SW-846 8260D
SW-846 8270E
MW-13 19E0276-03 Ground Water SM21-22 6200B
MW-14 19E0276-04 Ground Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 68
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:19E0276-04MW-14
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 68
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19E0276-01SS-1
DL
% Solids 91.4 % Wt SM 2540G
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19E0276-02SS-2
DL
C11-C22 Aromatics 18 11 mg/Kg dry MADEP-EPH-04-1.1
C19-C36 Aliphatics 110 11 mg/Kg dry MADEP-EPH-04-1.1
Unadjusted C11-C22 Aromatics 18 11 mg/Kg dry MADEP-EPH-04-1.1
% Solids 88.2 % Wt SM 2540G
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19E0276-03MW-13
DL
1,2,4-Trimethylbenzene 1100 25 g/L SM21-22 6200B9.0
1,2-Dichloroethane 100 25 g/L SM21-22 6200B20
1,3,5-Trimethylbenzene 230 25 g/L SM21-22 6200B7.0
Acetone 310 2500 g/L SM21-22 6200BL-06, J 190
Benzene 5000 25 g/L SM21-22 6200B9.0
Diisopropyl Ether (DIPE)120 25 g/L SM21-22 6200B8.5
Ethylbenzene 330 25 g/L SM21-22 6200B6.5
Isopropylbenzene (Cumene)36 25 g/L SM21-22 6200B8.5
m+p Xylene 2900 50 g/L SM21-22 6200B15
Methyl tert-Butyl Ether (MTBE)1800 25 g/L SM21-22 6200B12
Naphthalene 520 100 g/L SM21-22 6200B16
n-Propylbenzene 100 25 g/L SM21-22 6200B6.5
o-Xylene 1800 25 g/L SM21-22 6200B8.5
Styrene 47 25 g/L SM21-22 6200B5.5
Toluene 1100 25 g/L SM21-22 6200B7.0
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
For method MA EPH, only hydrocarbon ranges were requested and reported.
For method 6200B elevated reporting limits for sample 19E0276-03 due to high concentrations of target compounds.
[TOC_1]Case Narrative[TOC]
Page 6 of 68
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
1,1-Dichloroethylene
B230248-BS1, B230248-BSD1, B230565-BS1, B230565-BSD1
Methylene Chloride
B230248-BS1, B230248-BSD1, B230565-BS1, B230565-BSD1
trans-1,2-Dichloroethylene
B230248-BS1, B230248-BSD1
Vinyl Chloride
B230565-BS1, B230565-BSD1
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the high side.Analyte & Samples(s) Qualified:
L-06
Acetone
19E0276-03[MW-13], B230248-BS1, B230248-BSD1, B230565-BS1, B230565-BSD1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
Vinyl Acetate
19E0276-03[MW-13], B230248-BLK1, B230248-BS1, B230248-BSD1, S035785-CCV1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
19E0276-03[MW-13]
SW-846 8260D
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Carbon Disulfide
B230058-BS1, B230058-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Acetone
B230058-BS1
Tetrachloroethylene
B230058-BSD1
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
1,2-Dibromo-3-chloropropane (DBCP)
19E0276-01[SS-1], 19E0276-02[SS-2], B230058-BLK1, B230058-BS1, B230058-BSD1, S035581-CCV1
2-Butanone (MEK)
19E0276-01[SS-1], 19E0276-02[SS-2], B230058-BLK1, B230058-BS1, B230058-BSD1, S035581-CCV1
Acrylonitrile
19E0276-01[SS-1], 19E0276-02[SS-2], B230058-BLK1, B230058-BS1, B230058-BSD1, S035581-CCV1
Dichlorodifluoromethane (Freon 12)
19E0276-01[SS-1], 19E0276-02[SS-2], B230058-BLK1, B230058-BS1, B230058-BSD1, S035581-CCV1
Methyl tert-Butyl Ether (MTBE)
19E0276-01[SS-1], 19E0276-02[SS-2], B230058-BLK1, B230058-BS1, B230058-BSD1, S035581-CCV1
tert-Butyl Alcohol (TBA)
19E0276-01[SS-1], 19E0276-02[SS-2], B230058-BLK1, B230058-BS1, B230058-BSD1, S035581-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.Analyte & Samples(s) Qualified:
V-20
Tetrachloroethylene
B230058-BS1, B230058-BSD1, S035581-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
Bromomethane
19E0276-01[SS-1], 19E0276-02[SS-2], B230058-BLK1, B230058-BS1, B230058-BSD1, S035581-CCV1
SW-846 8270E
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Pyridine
B230431-BSD1
Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits. Possibility of sample matrix effects that lead to a low
bias for reported result or non-homogeneous sample aliquots cannot be eliminated.
Analyte & Samples(s) Qualified:
MS-09
1,3-Dichlorobenzene
19E0276-01[SS-1], B230431-MS1, B230431-MSD1
Aniline
19E0276-01[SS-1], B230431-MS1, B230431-MSD1
Benzidine
19E0276-01[SS-1], B230431-MS1, B230431-MSD1
N-Nitrosodimethylamine
19E0276-01[SS-1], B230431-MS1, B230431-MSD1
Pyridine
19E0276-01[SS-1], B230431-MS1, B230431-MSD1
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is
within method specified criteria.
Analyte & Samples(s) Qualified:
MS-22
1,2-Dichlorobenzene
B230431-MS1
1,4-Dichlorobenzene
B230431-MS1
1-Methylnaphthalene
B230431-MS1
4-Chloroaniline
B230431-MS1
Acetophenone
B230431-MS1
Benzoic Acid
B230431-MS1
Bis(2-chloroethyl)ether
B230431-MS1
Hexachlorobutadiene
B230431-MS1
Hexachlorocyclopentadiene
B230431-MS1
Hexachloroethane
B230431-MS1
Nitrobenzene
B230431-MS1
N-Nitrosodi-n-propylamine
B230431-MS1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
2-Methylphenol
19E0276-01[SS-1], 19E0276-02[SS-2], B230431-BLK1, B230431-BS1, B230431-BSD1, B230431-MS1, B230431-MSD1, S035746-CCV1
Benzidine
19E0276-01[SS-1], 19E0276-02[SS-2], B230431-BLK1, B230431-BS1, B230431-BSD1, B230431-MS1, B230431-MSD1, S035746-CCV1
Hexachlorocyclopentadiene
19E0276-01[SS-1], 19E0276-02[SS-2], B230431-BLK1, B230431-BS1, B230431-BSD1, B230431-MS1, B230431-MSD1, S035746-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
3,3-Dichlorobenzidine
19E0276-01[SS-1], 19E0276-02[SS-2], B230431-BLK1, B230431-BS1, B230431-BSD1, B230431-MS1, B230431-MSD1, S035746-CCV1
4-Chloroaniline
19E0276-01[SS-1], 19E0276-02[SS-2], B230431-BLK1, B230431-BS1, B230431-BSD1, B230431-MS1, B230431-MSD1, S035746-CCV1
Aniline
19E0276-01[SS-1], 19E0276-02[SS-2], B230431-BLK1, B230431-BS1, B230431-BSD1, B230431-MS1, B230431-MSD1, S035746-CCV1
Page 9 of 68
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
MADEP-EPH-04-1.1
SPE cartridge contamination with non-petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C 11-C22 aromatic
range fraction in all samples in the batch. No significant modifications were made to the method.
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
[TOC_2]19E0276-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.095 5/7/19 7:17 MFFmg/Kg dry0.0080 5/7/19SW-846 8260D1Acetone
ND 0.0057 5/7/19 7:17 MFFmg/Kg dry0.00095 5/7/19SW-846 8260D1V-05Acrylonitrile
ND 0.00095 5/7/19 7:17 MFFmg/Kg dry0.00028 5/7/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00057 5/7/19SW-846 8260D1Benzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D1Bromobenzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00076 5/7/19SW-846 8260D1Bromochloromethane
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00047 5/7/19SW-846 8260D1Bromodichloromethane
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00066 5/7/19SW-846 8260D1Bromoform
ND 0.0095 5/7/19 7:17 MFFmg/Kg dry0.0010 5/7/19SW-846 8260D1V-34Bromomethane
ND 0.038 5/7/19 7:17 MFFmg/Kg dry0.0052 5/7/19SW-846 8260D1V-052-Butanone (MEK)
ND 0.038 5/7/19 7:17 MFFmg/Kg dry0.0043 5/7/19SW-846 8260D1V-05tert-Butyl Alcohol (TBA)
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00047 5/7/19SW-846 8260D1n-Butylbenzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00076 5/7/19SW-846 8260D1sec-Butylbenzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00057 5/7/19SW-846 8260D1tert-Butylbenzene
ND 0.00095 5/7/19 7:17 MFFmg/Kg dry0.00019 5/7/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0057 5/7/19 7:17 MFFmg/Kg dry0.0051 5/7/19SW-846 8260D1Carbon Disulfide
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00066 5/7/19SW-846 8260D1Carbon Tetrachloride
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00047 5/7/19SW-846 8260D1Chlorobenzene
ND 0.00095 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D1Chlorodibromomethane
ND 0.019 5/7/19 7:17 MFFmg/Kg dry0.00076 5/7/19SW-846 8260D1Chloroethane
ND 0.0038 5/7/19 7:17 MFFmg/Kg dry0.00047 5/7/19SW-846 8260D1Chloroform
ND 0.0095 5/7/19 7:17 MFFmg/Kg dry0.00066 5/7/19SW-846 8260D1Chloromethane
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00028 5/7/19SW-846 8260D12-Chlorotoluene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D14-Chlorotoluene
ND 0.0038 5/7/19 7:17 MFFmg/Kg dry0.00095 5/7/19SW-846 8260D1V-051,2-Dibromo-3-chloropropane (DBCP)
ND 0.00095 5/7/19 7:17 MFFmg/Kg dry0.00066 5/7/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00076 5/7/19SW-846 8260D1Dibromomethane
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00076 5/7/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0038 5/7/19 7:17 MFFmg/Kg dry0.00057 5/7/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.019 5/7/19 7:17 MFFmg/Kg dry0.0010 5/7/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D11,1-Dichloroethane
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00047 5/7/19SW-846 8260D11,2-Dichloroethane
ND 0.0038 5/7/19 7:17 MFFmg/Kg dry0.00066 5/7/19SW-846 8260D11,1-Dichloroethylene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00066 5/7/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00057 5/7/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00076 5/7/19SW-846 8260D11,2-Dichloropropane
ND 0.00095 5/7/19 7:17 MFFmg/Kg dry0.00047 5/7/19SW-846 8260D11,3-Dichloropropane
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00076 5/7/19SW-846 8260D12,2-Dichloropropane
ND 0.0038 5/7/19 7:17 MFFmg/Kg dry0.00076 5/7/19SW-846 8260D11,1-Dichloropropene
ND 0.00095 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.00095 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.019 5/7/19 7:17 MFFmg/Kg dry0.00066 5/7/19SW-846 8260D1Diethyl Ether
[TOC_1]Sample Results[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00095 5/7/19 7:17 MFFmg/Kg dry0.00019 5/7/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.19 5/7/19 7:17 MFFmg/Kg dry0.0050 5/7/19SW-846 8260D11,4-Dioxane
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00057 5/7/19SW-846 8260D1Ethylbenzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00066 5/7/19SW-846 8260D1Hexachlorobutadiene
ND 0.019 5/7/19 7:17 MFFmg/Kg dry0.0019 5/7/19SW-846 8260D12-Hexanone (MBK)
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00057 5/7/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00047 5/7/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0038 5/7/19 7:17 MFFmg/Kg dry0.00028 5/7/19SW-846 8260D1V-05Methyl tert-Butyl Ether (MTBE)
ND 0.019 5/7/19 7:17 MFFmg/Kg dry0.00095 5/7/19SW-846 8260D1Methylene Chloride
ND 0.019 5/7/19 7:17 MFFmg/Kg dry0.0024 5/7/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0038 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D1Naphthalene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00057 5/7/19SW-846 8260D1n-Propylbenzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D1Styrene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00095 5/7/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.00095 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.0011 5/7/19SW-846 8260D1Tetrachloroethylene
ND 0.0095 5/7/19 7:17 MFFmg/Kg dry0.0010 5/7/19SW-846 8260D1Tetrahydrofuran
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00057 5/7/19SW-846 8260D1Toluene
ND 0.0038 5/7/19 7:17 MFFmg/Kg dry0.00095 5/7/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00028 5/7/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00047 5/7/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00038 5/7/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00076 5/7/19SW-846 8260D1Trichloroethylene
ND 0.0095 5/7/19 7:17 MFFmg/Kg dry0.00066 5/7/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00076 5/7/19SW-846 8260D11,2,3-Trichloropropane
ND 0.0095 5/7/19 7:17 MFFmg/Kg dry0.00076 5/7/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00028 5/7/19SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00047 5/7/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.0095 5/7/19 7:17 MFFmg/Kg dry0.00085 5/7/19SW-846 8260D1Vinyl Chloride
ND 0.0038 5/7/19 7:17 MFFmg/Kg dry0.00095 5/7/19SW-846 8260D1m+p Xylene
ND 0.0019 5/7/19 7:17 MFFmg/Kg dry0.00057 5/7/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.2 5/7/19 7:1770-130
Toluene-d8 102 5/7/19 7:1770-130
4-Bromofluorobenzene 103 5/7/19 7:1770-130
Page 12 of 68
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.097 5/10/19SW-846 8270E1Acenaphthene
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Acenaphthylene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.14 5/10/19SW-846 8270E1Acetophenone
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.086 5/10/19SW-846 8270E1MS-09, V-34Aniline
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.097 5/10/19SW-846 8270E1Anthracene
ND 0.71 5/13/19 15:39 IMRmg/Kg dry0.19 5/10/19SW-846 8270E1V-05, MS-09Benzidine
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Benzo(a)anthracene
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Benzo(a)pyrene
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Benzo(b)fluoranthene
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1Benzo(g,h,i)perylene
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Benzo(k)fluoranthene
ND 1.1 5/13/19 15:39 IMRmg/Kg dry0.64 5/10/19SW-846 8270E1Benzoic Acid
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.15 5/10/19SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.18 5/10/19SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.25 5/10/19SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E14-Bromophenylphenylether
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Butylbenzylphthalate
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.097 5/10/19SW-846 8270E1Carbazole
ND 0.71 5/13/19 15:39 IMRmg/Kg dry0.15 5/10/19SW-846 8270E1V-344-Chloroaniline
ND 0.71 5/13/19 15:39 IMRmg/Kg dry0.15 5/10/19SW-846 8270E14-Chloro-3-methylphenol
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E12-Chloronaphthalene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E12-Chlorophenol
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E14-Chlorophenylphenylether
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Chrysene
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1Dibenz(a,h)anthracene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Dibenzofuran
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1Di-n-butylphthalate
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E11,2-Dichlorobenzene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1MS-091,3-Dichlorobenzene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.097 5/10/19SW-846 8270E11,4-Dichlorobenzene
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.14 5/10/19SW-846 8270E1V-343,3-Dichlorobenzidine
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E12,4-Dichlorophenol
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.15 5/10/19SW-846 8270E1Diethylphthalate
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E12,4-Dimethylphenol
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.14 5/10/19SW-846 8270E1Dimethylphthalate
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.32 5/10/19SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.71 5/13/19 15:39 IMRmg/Kg dry0.50 5/10/19SW-846 8270E12,4-Dinitrophenol
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.17 5/10/19SW-846 8270E12,4-Dinitrotoluene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.17 5/10/19SW-846 8270E12,6-Dinitrotoluene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.16 5/10/19SW-846 8270E1Di-n-octylphthalate
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1Fluoranthene
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Fluorene
Page 13 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.097 5/10/19SW-846 8270E1Hexachlorobenzene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.14 5/10/19SW-846 8270E1Hexachlorobutadiene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.30 5/10/19SW-846 8270E1V-05Hexachlorocyclopentadiene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Hexachloroethane
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Isophorone
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.097 5/10/19SW-846 8270E11-Methylnaphthalene
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.12 5/10/19SW-846 8270E12-Methylnaphthalene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.14 5/10/19SW-846 8270E1V-052-Methylphenol
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E13/4-Methylphenol
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Naphthalene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.22 5/10/19SW-846 8270E12-Nitroaniline
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.15 5/10/19SW-846 8270E13-Nitroaniline
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.14 5/10/19SW-846 8270E14-Nitroaniline
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.15 5/10/19SW-846 8270E1Nitrobenzene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.15 5/10/19SW-846 8270E12-Nitrophenol
ND 0.71 5/13/19 15:39 IMRmg/Kg dry0.26 5/10/19SW-846 8270E14-Nitrophenol
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.19 5/10/19SW-846 8270E1MS-09N-Nitrosodimethylamine
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.16 5/10/19SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Pentachloronitrobenzene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.25 5/10/19SW-846 8270E1Pentachlorophenol
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.097 5/10/19SW-846 8270E1Phenanthrene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Phenol
ND 0.18 5/13/19 15:39 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Pyrene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1MS-09Pyridine
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.14 5/10/19SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.12 5/10/19SW-846 8270E11,2,4-Trichlorobenzene
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E12,4,5-Trichlorophenol
ND 0.37 5/13/19 15:39 IMRmg/Kg dry0.13 5/10/19SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 52.3 5/13/19 15:3930-130
Phenol-d6 54.8 5/13/19 15:3930-130
Nitrobenzene-d5 53.0 5/13/19 15:3930-130
2-Fluorobiphenyl 59.8 5/13/19 15:3930-130
2,4,6-Tribromophenol 68.5 5/13/19 15:3930-130
p-Terphenyl-d14 75.9 5/13/19 15:3930-130
Page 14 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 11 5/11/19 1:12 KLBmg/Kg dry 5/6/19MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 11 5/11/19 1:12 KLBmg/Kg dry 5/6/19MADEP-EPH-04-1.11C19-C36 Aliphatics
ND 11 5/11/19 1:12 KLBmg/Kg dry 5/6/19MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
ND 11 5/11/19 1:12 KLBmg/Kg dry 5/6/19MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)80.4 5/11/19 1:1240-140
o-Terphenyl (OTP)88.5 5/11/19 1:1240-140
2-Bromonaphthalene 97.8 5/11/19 1:1240-140
2-Fluorobiphenyl 106 5/11/19 1:1240-140
Page 15 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.04
Petroleum Hydrocarbons Analyses - VPH
ND 11 5/6/19 20:05 EEHmg/Kg dry 5/6/19MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 11 5/6/19 20:05 EEHmg/Kg dry 5/6/19MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 11 5/6/19 20:05 EEHmg/Kg dry 5/6/19MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 11 5/6/19 20:05 EEHmg/Kg dry 5/6/19MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 11 5/6/19 20:05 EEHmg/Kg dry 5/6/19MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)105 5/6/19 20:0570-130
2,5-Dibromotoluene (PID)102 5/6/19 20:0570-130
Page 16 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
91.4 5/9/19 22:32 KMG% Wt 5/9/19SM 2540G1% Solids
Page 17 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-02
Field Sample #: SS-2
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
[TOC_2]19E0276-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.10 5/7/19 7:44 MFFmg/Kg dry0.0084 5/7/19SW-846 8260D1Acetone
ND 0.0060 5/7/19 7:44 MFFmg/Kg dry0.0010 5/7/19SW-846 8260D1V-05Acrylonitrile
ND 0.0010 5/7/19 7:44 MFFmg/Kg dry0.00030 5/7/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00060 5/7/19SW-846 8260D1Benzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D1Bromobenzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00080 5/7/19SW-846 8260D1Bromochloromethane
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00050 5/7/19SW-846 8260D1Bromodichloromethane
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00070 5/7/19SW-846 8260D1Bromoform
ND 0.010 5/7/19 7:44 MFFmg/Kg dry0.0011 5/7/19SW-846 8260D1V-34Bromomethane
ND 0.040 5/7/19 7:44 MFFmg/Kg dry0.0055 5/7/19SW-846 8260D1V-052-Butanone (MEK)
ND 0.040 5/7/19 7:44 MFFmg/Kg dry0.0045 5/7/19SW-846 8260D1V-05tert-Butyl Alcohol (TBA)
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00050 5/7/19SW-846 8260D1n-Butylbenzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00080 5/7/19SW-846 8260D1sec-Butylbenzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00060 5/7/19SW-846 8260D1tert-Butylbenzene
ND 0.0010 5/7/19 7:44 MFFmg/Kg dry0.00020 5/7/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0060 5/7/19 7:44 MFFmg/Kg dry0.0054 5/7/19SW-846 8260D1Carbon Disulfide
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00070 5/7/19SW-846 8260D1Carbon Tetrachloride
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00050 5/7/19SW-846 8260D1Chlorobenzene
ND 0.0010 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D1Chlorodibromomethane
ND 0.020 5/7/19 7:44 MFFmg/Kg dry0.00080 5/7/19SW-846 8260D1Chloroethane
ND 0.0040 5/7/19 7:44 MFFmg/Kg dry0.00050 5/7/19SW-846 8260D1Chloroform
ND 0.010 5/7/19 7:44 MFFmg/Kg dry0.00070 5/7/19SW-846 8260D1Chloromethane
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00030 5/7/19SW-846 8260D12-Chlorotoluene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D14-Chlorotoluene
ND 0.0040 5/7/19 7:44 MFFmg/Kg dry0.0010 5/7/19SW-846 8260D1V-051,2-Dibromo-3-chloropropane (DBCP)
ND 0.0010 5/7/19 7:44 MFFmg/Kg dry0.00070 5/7/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00080 5/7/19SW-846 8260D1Dibromomethane
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00080 5/7/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0040 5/7/19 7:44 MFFmg/Kg dry0.00060 5/7/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.020 5/7/19 7:44 MFFmg/Kg dry0.0011 5/7/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D11,1-Dichloroethane
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00050 5/7/19SW-846 8260D11,2-Dichloroethane
ND 0.0040 5/7/19 7:44 MFFmg/Kg dry0.00070 5/7/19SW-846 8260D11,1-Dichloroethylene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00070 5/7/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00060 5/7/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00080 5/7/19SW-846 8260D11,2-Dichloropropane
ND 0.0010 5/7/19 7:44 MFFmg/Kg dry0.00050 5/7/19SW-846 8260D11,3-Dichloropropane
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00080 5/7/19SW-846 8260D12,2-Dichloropropane
ND 0.0040 5/7/19 7:44 MFFmg/Kg dry0.00080 5/7/19SW-846 8260D11,1-Dichloropropene
ND 0.0010 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0010 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.020 5/7/19 7:44 MFFmg/Kg dry0.00070 5/7/19SW-846 8260D1Diethyl Ether
Page 18 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-02
Field Sample #: SS-2
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0010 5/7/19 7:44 MFFmg/Kg dry0.00020 5/7/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.20 5/7/19 7:44 MFFmg/Kg dry0.0053 5/7/19SW-846 8260D11,4-Dioxane
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00060 5/7/19SW-846 8260D1Ethylbenzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00070 5/7/19SW-846 8260D1Hexachlorobutadiene
ND 0.020 5/7/19 7:44 MFFmg/Kg dry0.0020 5/7/19SW-846 8260D12-Hexanone (MBK)
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00060 5/7/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00050 5/7/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0040 5/7/19 7:44 MFFmg/Kg dry0.00030 5/7/19SW-846 8260D1V-05Methyl tert-Butyl Ether (MTBE)
ND 0.020 5/7/19 7:44 MFFmg/Kg dry0.0010 5/7/19SW-846 8260D1Methylene Chloride
ND 0.020 5/7/19 7:44 MFFmg/Kg dry0.0025 5/7/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0040 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D1Naphthalene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00060 5/7/19SW-846 8260D1n-Propylbenzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D1Styrene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.0010 5/7/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0010 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.0012 5/7/19SW-846 8260D1Tetrachloroethylene
ND 0.010 5/7/19 7:44 MFFmg/Kg dry0.0011 5/7/19SW-846 8260D1Tetrahydrofuran
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00060 5/7/19SW-846 8260D1Toluene
ND 0.0040 5/7/19 7:44 MFFmg/Kg dry0.0010 5/7/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00030 5/7/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00050 5/7/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00040 5/7/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00080 5/7/19SW-846 8260D1Trichloroethylene
ND 0.010 5/7/19 7:44 MFFmg/Kg dry0.00070 5/7/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00080 5/7/19SW-846 8260D11,2,3-Trichloropropane
ND 0.010 5/7/19 7:44 MFFmg/Kg dry0.00080 5/7/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00030 5/7/19SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00050 5/7/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.010 5/7/19 7:44 MFFmg/Kg dry0.00090 5/7/19SW-846 8260D1Vinyl Chloride
ND 0.0040 5/7/19 7:44 MFFmg/Kg dry0.0010 5/7/19SW-846 8260D1m+p Xylene
ND 0.0020 5/7/19 7:44 MFFmg/Kg dry0.00060 5/7/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.4 5/7/19 7:4470-130
Toluene-d8 103 5/7/19 7:4470-130
4-Bromofluorobenzene 103 5/7/19 7:4470-130
Page 19 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-02
Field Sample #: SS-2
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.10 5/10/19SW-846 8270E1Acenaphthene
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Acenaphthylene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.15 5/10/19SW-846 8270E1Acetophenone
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.090 5/10/19SW-846 8270E1V-34Aniline
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.10 5/10/19SW-846 8270E1Anthracene
ND 0.74 5/13/19 16:02 IMRmg/Kg dry0.20 5/10/19SW-846 8270E1V-05Benzidine
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Benzo(a)anthracene
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Benzo(a)pyrene
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Benzo(b)fluoranthene
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1Benzo(g,h,i)perylene
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Benzo(k)fluoranthene
ND 1.1 5/13/19 16:02 IMRmg/Kg dry0.66 5/10/19SW-846 8270E1Benzoic Acid
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.16 5/10/19SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.19 5/10/19SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.26 5/10/19SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E14-Bromophenylphenylether
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Butylbenzylphthalate
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.10 5/10/19SW-846 8270E1Carbazole
ND 0.74 5/13/19 16:02 IMRmg/Kg dry0.16 5/10/19SW-846 8270E1V-344-Chloroaniline
ND 0.74 5/13/19 16:02 IMRmg/Kg dry0.16 5/10/19SW-846 8270E14-Chloro-3-methylphenol
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E12-Chloronaphthalene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E12-Chlorophenol
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E14-Chlorophenylphenylether
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Chrysene
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1Dibenz(a,h)anthracene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Dibenzofuran
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1Di-n-butylphthalate
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E11,2-Dichlorobenzene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E11,3-Dichlorobenzene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.10 5/10/19SW-846 8270E11,4-Dichlorobenzene
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.15 5/10/19SW-846 8270E1V-343,3-Dichlorobenzidine
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E12,4-Dichlorophenol
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.16 5/10/19SW-846 8270E1Diethylphthalate
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E12,4-Dimethylphenol
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.15 5/10/19SW-846 8270E1Dimethylphthalate
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.34 5/10/19SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.74 5/13/19 16:02 IMRmg/Kg dry0.51 5/10/19SW-846 8270E12,4-Dinitrophenol
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.18 5/10/19SW-846 8270E12,4-Dinitrotoluene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.18 5/10/19SW-846 8270E12,6-Dinitrotoluene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.17 5/10/19SW-846 8270E1Di-n-octylphthalate
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1Fluoranthene
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Fluorene
Page 20 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-02
Field Sample #: SS-2
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.10 5/10/19SW-846 8270E1Hexachlorobenzene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.15 5/10/19SW-846 8270E1Hexachlorobutadiene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.31 5/10/19SW-846 8270E1V-05Hexachlorocyclopentadiene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Hexachloroethane
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Isophorone
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.10 5/10/19SW-846 8270E11-Methylnaphthalene
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.12 5/10/19SW-846 8270E12-Methylnaphthalene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.15 5/10/19SW-846 8270E1V-052-Methylphenol
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E13/4-Methylphenol
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Naphthalene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.22 5/10/19SW-846 8270E12-Nitroaniline
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.16 5/10/19SW-846 8270E13-Nitroaniline
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.15 5/10/19SW-846 8270E14-Nitroaniline
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.16 5/10/19SW-846 8270E1Nitrobenzene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.16 5/10/19SW-846 8270E12-Nitrophenol
ND 0.74 5/13/19 16:02 IMRmg/Kg dry0.27 5/10/19SW-846 8270E14-Nitrophenol
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.20 5/10/19SW-846 8270E1N-Nitrosodimethylamine
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.17 5/10/19SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Pentachloronitrobenzene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.26 5/10/19SW-846 8270E1Pentachlorophenol
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.10 5/10/19SW-846 8270E1Phenanthrene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E1Phenol
ND 0.19 5/13/19 16:02 IMRmg/Kg dry0.12 5/10/19SW-846 8270E1Pyrene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.11 5/10/19SW-846 8270E1Pyridine
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.15 5/10/19SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.12 5/10/19SW-846 8270E11,2,4-Trichlorobenzene
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E12,4,5-Trichlorophenol
ND 0.38 5/13/19 16:02 IMRmg/Kg dry0.13 5/10/19SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 48.1 5/13/19 16:0230-130
Phenol-d6 53.5 5/13/19 16:0230-130
Nitrobenzene-d5 51.1 5/13/19 16:0230-130
2-Fluorobiphenyl 65.8 5/13/19 16:0230-130
2,4,6-Tribromophenol 70.0 5/13/19 16:0230-130
p-Terphenyl-d14 78.2 5/13/19 16:0230-130
Page 21 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-02
Field Sample #: SS-2
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 11 5/11/19 1:30 KLBmg/Kg dry 5/6/19MADEP-EPH-04-1.11C9-C18 Aliphatics
110 11 5/11/19 1:30 KLBmg/Kg dry 5/6/19MADEP-EPH-04-1.11C19-C36 Aliphatics
18 11 5/11/19 1:30 KLBmg/Kg dry 5/6/19MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
18 11 5/11/19 1:30 KLBmg/Kg dry 5/6/19MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)83.0 5/11/19 1:3040-140
o-Terphenyl (OTP)89.7 5/11/19 1:3040-140
2-Bromonaphthalene 97.7 5/11/19 1:3040-140
2-Fluorobiphenyl 107 5/11/19 1:3040-140
Page 22 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-02
Field Sample #: SS-2
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.16
Petroleum Hydrocarbons Analyses - VPH
ND 11 5/6/19 20:34 EEHmg/Kg dry 5/6/19MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 11 5/6/19 20:34 EEHmg/Kg dry 5/6/19MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 11 5/6/19 20:34 EEHmg/Kg dry 5/6/19MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 11 5/6/19 20:34 EEHmg/Kg dry 5/6/19MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 11 5/6/19 20:34 EEHmg/Kg dry 5/6/19MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)104 5/6/19 20:3470-130
2,5-Dibromotoluene (PID)103 5/6/19 20:3470-130
Page 23 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-02
Field Sample #: SS-2
Sample Matrix: Soil
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
88.2 5/9/19 22:32 KMG% Wt 5/9/19SM 2540G1% Solids
Page 24 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-03
Field Sample #: MW-13
Sample Matrix: Ground Water
Sampled: 5/3/2019 00:00
[TOC_2]19E0276-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
310 2500 5/11/19 4:03 EEHg/L190 5/9/19SM21-22 6200B50L-06, JAcetone
5000 25 5/11/19 4:03 EEHg/L9.0 5/9/19SM21-22 6200B50Benzene
ND 25 5/11/19 4:03 EEHg/L7.5 5/9/19SM21-22 6200B50Bromobenzene
ND 25 5/11/19 4:03 EEHg/L16 5/9/19SM21-22 6200B50Bromochloromethane
ND 25 5/11/19 4:03 EEHg/L8.0 5/9/19SM21-22 6200B50Bromodichloromethane
ND 100 5/11/19 4:03 EEHg/L23 5/9/19SM21-22 6200B50Bromoform
ND 100 5/11/19 4:03 EEHg/L39 5/9/19SM21-22 6200B50Bromomethane
ND 250 5/11/19 4:03 EEHg/L97 5/9/19SM21-22 6200B502-Butanone (MEK)
ND 25 5/11/19 4:03 EEHg/L10 5/9/19SM21-22 6200B50n-Butylbenzene
ND 25 5/11/19 4:03 EEHg/L8.0 5/9/19SM21-22 6200B50sec-Butylbenzene
ND 25 5/11/19 4:03 EEHg/L8.5 5/9/19SM21-22 6200B50tert-Butylbenzene
ND 25 5/11/19 4:03 EEHg/L5.5 5/9/19SM21-22 6200B50Carbon Tetrachloride
ND 25 5/11/19 4:03 EEHg/L7.5 5/9/19SM21-22 6200B50Chlorobenzene
ND 25 5/11/19 4:03 EEHg/L10 5/9/19SM21-22 6200B50Chlorodibromomethane
ND 25 5/11/19 4:03 EEHg/L18 5/9/19SM21-22 6200B50Chloroethane
ND 25 5/11/19 4:03 EEHg/L8.5 5/9/19SM21-22 6200B50Chloroform
ND 30 5/11/19 4:03 EEHg/L22 5/9/19SM21-22 6200B50Chloromethane
ND 25 5/11/19 4:03 EEHg/L6.0 5/9/19SM21-22 6200B502-Chlorotoluene
ND 25 5/11/19 4:03 EEHg/L7.0 5/9/19SM21-22 6200B504-Chlorotoluene
ND 25 5/11/19 4:03 EEHg/L9.5 5/9/19SM21-22 6200B501,2-Dibromoethane (EDB)
ND 25 5/11/19 4:03 EEHg/L8.0 5/9/19SM21-22 6200B501,2-Dichlorobenzene
ND 25 5/11/19 4:03 EEHg/L6.0 5/9/19SM21-22 6200B501,3-Dichlorobenzene
ND 25 5/11/19 4:03 EEHg/L6.5 5/9/19SM21-22 6200B501,4-Dichlorobenzene
ND 25 5/11/19 4:03 EEHg/L13 5/9/19SM21-22 6200B50Dichlorodifluoromethane (Freon 12)
ND 25 5/11/19 4:03 EEHg/L8.0 5/9/19SM21-22 6200B501,1-Dichloroethane
100 25 5/11/19 4:03 EEHg/L20 5/9/19SM21-22 6200B501,2-Dichloroethane
ND 25 5/11/19 4:03 EEHg/L16 5/9/19SM21-22 6200B501,1-Dichloroethylene
ND 25 5/11/19 4:03 EEHg/L6.5 5/9/19SM21-22 6200B50cis-1,2-Dichloroethylene
ND 25 5/11/19 4:03 EEHg/L16 5/9/19SM21-22 6200B50trans-1,2-Dichloroethylene
ND 25 5/11/19 4:03 EEHg/L10 5/9/19SM21-22 6200B501,2-Dichloropropane
ND 25 5/11/19 4:03 EEHg/L5.5 5/9/19SM21-22 6200B501,3-Dichloropropane
ND 25 5/11/19 4:03 EEHg/L10 5/9/19SM21-22 6200B502,2-Dichloropropane
ND 25 5/11/19 4:03 EEHg/L8.0 5/9/19SM21-22 6200B501,1-Dichloropropene
ND 25 5/11/19 4:03 EEHg/L6.5 5/9/19SM21-22 6200B50cis-1,3-Dichloropropene
ND 25 5/11/19 4:03 EEHg/L12 5/9/19SM21-22 6200B50trans-1,3-Dichloropropene
120 25 5/11/19 4:03 EEHg/L8.5 5/9/19SM21-22 6200B50Diisopropyl Ether (DIPE)
330 25 5/11/19 4:03 EEHg/L6.5 5/9/19SM21-22 6200B50Ethylbenzene
ND 250 5/11/19 4:03 EEHg/L76 5/9/19SM21-22 6200B502-Hexanone (MBK)
36 25 5/11/19 4:03 EEHg/L8.5 5/9/19SM21-22 6200B50Isopropylbenzene (Cumene)
ND 25 5/11/19 4:03 EEHg/L10 5/9/19SM21-22 6200B50p-Isopropyltoluene (p-Cymene)
1800 25 5/11/19 4:03 EEHg/L12 5/9/19SM21-22 6200B50Methyl tert-Butyl Ether (MTBE)
ND 250 5/11/19 4:03 EEHg/L17 5/9/19SM21-22 6200B50Methylene Chloride
ND 250 5/11/19 4:03 EEHg/L84 5/9/19SM21-22 6200B504-Methyl-2-pentanone (MIBK)
520 100 5/11/19 4:03 EEHg/L16 5/9/19SM21-22 6200B50Naphthalene
Page 25 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-03
Field Sample #: MW-13
Sample Matrix: Ground Water
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
100 25 5/11/19 4:03 EEHg/L6.5 5/9/19SM21-22 6200B50n-Propylbenzene
47 25 5/11/19 4:03 EEHg/L5.5 5/9/19SM21-22 6200B50Styrene
ND 25 5/11/19 4:03 EEHg/L11 5/9/19SM21-22 6200B501,1,2,2-Tetrachloroethane
ND 25 5/11/19 4:03 EEHg/L9.0 5/9/19SM21-22 6200B50Tetrachloroethylene
1100 25 5/11/19 4:03 EEHg/L7.0 5/9/19SM21-22 6200B50Toluene
ND 250 5/11/19 4:03 EEHg/L28 5/9/19SM21-22 6200B501,2,3-Trichlorobenzene
ND 100 5/11/19 4:03 EEHg/L20 5/9/19SM21-22 6200B501,2,4-Trichlorobenzene
ND 25 5/11/19 4:03 EEHg/L10 5/9/19SM21-22 6200B501,1,1-Trichloroethane
ND 25 5/11/19 4:03 EEHg/L8.0 5/9/19SM21-22 6200B501,1,2-Trichloroethane
ND 25 5/11/19 4:03 EEHg/L12 5/9/19SM21-22 6200B50Trichloroethylene
ND 25 5/11/19 4:03 EEHg/L16 5/9/19SM21-22 6200B50Trichlorofluoromethane (Freon 11)
ND 25 5/11/19 4:03 EEHg/L12 5/9/19SM21-22 6200B501,2,3-Trichloropropane
1100 25 5/11/19 4:03 EEHg/L9.0 5/9/19SM21-22 6200B501,2,4-Trimethylbenzene
230 25 5/11/19 4:03 EEHg/L7.0 5/9/19SM21-22 6200B501,3,5-Trimethylbenzene
ND 1000 5/11/19 4:03 EEHg/L510 5/9/19SM21-22 6200B50R-05Vinyl Acetate
ND 25 5/11/19 4:03 EEHg/L22 5/9/19SM21-22 6200B50Vinyl Chloride
2900 50 5/11/19 4:03 EEHg/L15 5/9/19SM21-22 6200B50m+p Xylene
1800 25 5/11/19 4:03 EEHg/L8.5 5/9/19SM21-22 6200B50o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 115 5/11/19 4:0370-130
Toluene-d8 104 5/11/19 4:0370-130
4-Bromofluorobenzene 103 5/11/19 4:0370-130
Page 26 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-04
Field Sample #: MW-14
Sample Matrix: Ground Water
Sampled: 5/3/2019 00:00
[TOC_2]19E0276-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 5/14/19 0:58 EEHg/L3.8 5/13/19SM21-22 6200B1Acetone
ND 0.50 5/14/19 0:58 EEHg/L0.18 5/13/19SM21-22 6200B1Benzene
ND 0.50 5/14/19 0:58 EEHg/L0.15 5/13/19SM21-22 6200B1Bromobenzene
ND 0.50 5/14/19 0:58 EEHg/L0.32 5/13/19SM21-22 6200B1Bromochloromethane
ND 0.50 5/14/19 0:58 EEHg/L0.16 5/13/19SM21-22 6200B1Bromodichloromethane
ND 2.0 5/14/19 0:58 EEHg/L0.46 5/13/19SM21-22 6200B1Bromoform
ND 2.0 5/14/19 0:58 EEHg/L0.78 5/13/19SM21-22 6200B1Bromomethane
ND 5.0 5/14/19 0:58 EEHg/L1.9 5/13/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 5/14/19 0:58 EEHg/L0.21 5/13/19SM21-22 6200B1n-Butylbenzene
ND 0.50 5/14/19 0:58 EEHg/L0.16 5/13/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 5/14/19 0:58 EEHg/L0.17 5/13/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 5/14/19 0:58 EEHg/L0.11 5/13/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 5/14/19 0:58 EEHg/L0.15 5/13/19SM21-22 6200B1Chlorobenzene
ND 0.50 5/14/19 0:58 EEHg/L0.21 5/13/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 5/14/19 0:58 EEHg/L0.35 5/13/19SM21-22 6200B1Chloroethane
ND 0.50 5/14/19 0:58 EEHg/L0.17 5/13/19SM21-22 6200B1Chloroform
ND 0.60 5/14/19 0:58 EEHg/L0.45 5/13/19SM21-22 6200B1Chloromethane
ND 0.50 5/14/19 0:58 EEHg/L0.12 5/13/19SM21-22 6200B12-Chlorotoluene
ND 0.50 5/14/19 0:58 EEHg/L0.14 5/13/19SM21-22 6200B14-Chlorotoluene
ND 0.50 5/14/19 0:58 EEHg/L0.19 5/13/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 5/14/19 0:58 EEHg/L0.16 5/13/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 5/14/19 0:58 EEHg/L0.12 5/13/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 5/14/19 0:58 EEHg/L0.13 5/13/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 5/14/19 0:58 EEHg/L0.26 5/13/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 5/14/19 0:58 EEHg/L0.16 5/13/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 5/14/19 0:58 EEHg/L0.41 5/13/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 5/14/19 0:58 EEHg/L0.32 5/13/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 5/14/19 0:58 EEHg/L0.13 5/13/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 5/14/19 0:58 EEHg/L0.31 5/13/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 5/14/19 0:58 EEHg/L0.20 5/13/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 5/14/19 0:58 EEHg/L0.11 5/13/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 5/14/19 0:58 EEHg/L0.20 5/13/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 5/14/19 0:58 EEHg/L0.16 5/13/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 5/14/19 0:58 EEHg/L0.13 5/13/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 5/14/19 0:58 EEHg/L0.23 5/13/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 5/14/19 0:58 EEHg/L0.17 5/13/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 5/14/19 0:58 EEHg/L0.13 5/13/19SM21-22 6200B1Ethylbenzene
ND 5.0 5/14/19 0:58 EEHg/L1.5 5/13/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 5/14/19 0:58 EEHg/L0.17 5/13/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 5/14/19 0:58 EEHg/L0.20 5/13/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 5/14/19 0:58 EEHg/L0.25 5/13/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 5/14/19 0:58 EEHg/L0.34 5/13/19SM21-22 6200B1Methylene Chloride
ND 5.0 5/14/19 0:58 EEHg/L1.7 5/13/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 2.0 5/14/19 0:58 EEHg/L0.31 5/13/19SM21-22 6200B1Naphthalene
Page 27 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/3/2019
Work Order: 19E0276Sample Description:Project Location: Roughmont, NC
Sample ID: 19E0276-04
Field Sample #: MW-14
Sample Matrix: Ground Water
Sampled: 5/3/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 5/14/19 0:58 EEHg/L0.13 5/13/19SM21-22 6200B1n-Propylbenzene
ND 0.50 5/14/19 0:58 EEHg/L0.11 5/13/19SM21-22 6200B1Styrene
ND 0.50 5/14/19 0:58 EEHg/L0.22 5/13/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 5/14/19 0:58 EEHg/L0.18 5/13/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 5/14/19 0:58 EEHg/L0.14 5/13/19SM21-22 6200B1Toluene
ND 5.0 5/14/19 0:58 EEHg/L0.57 5/13/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 5/14/19 0:58 EEHg/L0.40 5/13/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 5/14/19 0:58 EEHg/L0.20 5/13/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 5/14/19 0:58 EEHg/L0.16 5/13/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 5/14/19 0:58 EEHg/L0.24 5/13/19SM21-22 6200B1Trichloroethylene
ND 0.50 5/14/19 0:58 EEHg/L0.33 5/13/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 5/14/19 0:58 EEHg/L0.25 5/13/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 5/14/19 0:58 EEHg/L0.18 5/13/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 5/14/19 0:58 EEHg/L0.14 5/13/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 5/14/19 0:58 EEHg/L10 5/13/19SM21-22 6200B1Vinyl Acetate
ND 0.50 5/14/19 0:58 EEHg/L0.45 5/13/19SM21-22 6200B1Vinyl Chloride
ND 1.0 5/14/19 0:58 EEHg/L0.30 5/13/19SM21-22 6200B1m+p Xylene
ND 0.50 5/14/19 0:58 EEHg/L0.17 5/13/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 108 5/14/19 0:5870-130
Toluene-d8 102 5/14/19 0:5870-130
4-Bromofluorobenzene 100 5/14/19 0:5870-130
Page 28 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546-MADEP-EPH-04-1.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B229933 05/06/1920.1 2.0019E0276-01 [SS-1]
B229933 05/06/1920.3 2.0019E0276-02 [SS-2]
Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B229919 05/06/195.20 5.4019E0276-01 [SS-1]
B229919 05/06/195.80 5.7019E0276-02 [SS-2]
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B230325 05/09/1919E0276-01 [SS-1]
B230325 05/09/1919E0276-02 [SS-2]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B230248 05/09/190.1 5.0019E0276-03 [MW-13]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B230565 05/13/195 5.0019E0276-04 [MW-14]
Prep Method: SW-846 5035-SW-846 8260D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B230058 05/07/195.78 10.019E0276-01 [SS-1]
B230058 05/07/195.69 10.019E0276-02 [SS-2]
Prep Method: SW-846 3546-SW-846 8270E
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B230431 05/10/1930.4 1.0019E0276-01 [SS-1]
B230431 05/10/1930.4 1.0019E0276-02 [SS-2]
[TOC_1]Sample Preparation Information[TOC]
Page 29 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B230058 - SW-846 5035
[TOC_3]B230058[TOC]
Blank (B230058-BLK1) Prepared & Analyzed: 05/07/19
Acetone mg/Kg wet0.10ND
Acrylonitrile mg/Kg wet0.0060 V-05ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010ND
Benzene mg/Kg wet0.0020ND
Bromobenzene mg/Kg wet0.0020ND
Bromochloromethane mg/Kg wet0.0020ND
Bromodichloromethane mg/Kg wet0.0020ND
Bromoform mg/Kg wet0.0020ND
Bromomethane mg/Kg wet0.010 V-34ND
2-Butanone (MEK)mg/Kg wet0.040 V-05ND
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 V-05ND
n-Butylbenzene mg/Kg wet0.0020ND
sec-Butylbenzene mg/Kg wet0.0020ND
tert-Butylbenzene mg/Kg wet0.0020ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010ND
Carbon Disulfide mg/Kg wet0.0060ND
Carbon Tetrachloride mg/Kg wet0.0020ND
Chlorobenzene mg/Kg wet0.0020ND
Chlorodibromomethane mg/Kg wet0.0010ND
Chloroethane mg/Kg wet0.020ND
Chloroform mg/Kg wet0.0040ND
Chloromethane mg/Kg wet0.010ND
2-Chlorotoluene mg/Kg wet0.0020ND
4-Chlorotoluene mg/Kg wet0.0020ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 V-05ND
1,2-Dibromoethane (EDB)mg/Kg wet0.0010ND
Dibromomethane mg/Kg wet0.0020ND
1,2-Dichlorobenzene mg/Kg wet0.0020ND
1,3-Dichlorobenzene mg/Kg wet0.0020ND
1,4-Dichlorobenzene mg/Kg wet0.0020ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 V-05ND
1,1-Dichloroethane mg/Kg wet0.0020ND
1,2-Dichloroethane mg/Kg wet0.0020ND
1,1-Dichloroethylene mg/Kg wet0.0040ND
cis-1,2-Dichloroethylene mg/Kg wet0.0020ND
trans-1,2-Dichloroethylene mg/Kg wet0.0020ND
1,2-Dichloropropane mg/Kg wet0.0020ND
1,3-Dichloropropane mg/Kg wet0.0010ND
2,2-Dichloropropane mg/Kg wet0.0020ND
1,1-Dichloropropene mg/Kg wet0.0020ND
cis-1,3-Dichloropropene mg/Kg wet0.0010ND
trans-1,3-Dichloropropene mg/Kg wet0.0010ND
Diethyl Ether mg/Kg wet0.020ND
Diisopropyl Ether (DIPE)mg/Kg wet0.0010ND
1,4-Dioxane mg/Kg wet0.10ND
Ethylbenzene mg/Kg wet0.0020ND
Hexachlorobutadiene mg/Kg wet0.0020ND
2-Hexanone (MBK)mg/Kg wet0.020ND
Isopropylbenzene (Cumene)mg/Kg wet0.0020ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 V-05ND
[TOC_1]QC Data[TOC]
Page 30 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230058 - SW-846 5035
Blank (B230058-BLK1) Prepared & Analyzed: 05/07/19
Methylene Chloride mg/Kg wet0.020ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020ND
Naphthalene mg/Kg wet0.0040ND
n-Propylbenzene mg/Kg wet0.0020ND
Styrene mg/Kg wet0.0020ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010ND
Tetrachloroethylene mg/Kg wet0.0020ND
Tetrahydrofuran mg/Kg wet0.010ND
Toluene mg/Kg wet0.0020ND
1,2,3-Trichlorobenzene mg/Kg wet0.0020ND
1,2,4-Trichlorobenzene mg/Kg wet0.0020ND
1,3,5-Trichlorobenzene mg/Kg wet0.0020ND
1,1,1-Trichloroethane mg/Kg wet0.0020ND
1,1,2-Trichloroethane mg/Kg wet0.0020ND
Trichloroethylene mg/Kg wet0.0020ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010ND
1,2,3-Trichloropropane mg/Kg wet0.0020ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010ND
1,2,4-Trimethylbenzene mg/Kg wet0.0020ND
1,3,5-Trimethylbenzene mg/Kg wet0.0020ND
Vinyl Chloride mg/Kg wet0.010ND
m+p Xylene mg/Kg wet0.0040ND
o-Xylene mg/Kg wet0.0020ND
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 85.60.0428
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 1030.0515
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1000.0501
LCS (B230058-BS1) Prepared & Analyzed: 05/07/19
Acetone mg/Kg wet0.10 0.200 L-0770-160161*0.321
Acrylonitrile mg/Kg wet0.0060 0.0200 V-0570-13071.10.0142
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 70-13088.90.0178
Benzene mg/Kg wet0.0020 0.0200 70-13091.60.0183
Bromobenzene mg/Kg wet0.0020 0.0200 70-1301010.0202
Bromochloromethane mg/Kg wet0.0020 0.0200 70-13089.80.0180
Bromodichloromethane mg/Kg wet0.0020 0.0200 70-1301020.0204
Bromoform mg/Kg wet0.0020 0.0200 70-1301010.0201
Bromomethane mg/Kg wet0.010 0.0200 V-3440-13074.50.0149
2-Butanone (MEK)mg/Kg wet0.040 0.200 V-0570-16097.00.194
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 V-0540-13068.70.137
n-Butylbenzene mg/Kg wet0.0020 0.0200 70-1301040.0208
sec-Butylbenzene mg/Kg wet0.0020 0.0200 70-1301210.0242
tert-Butylbenzene mg/Kg wet0.0020 0.0200 70-1601030.0206
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 70-13084.10.0168
Carbon Disulfide mg/Kg wet0.0060 0.0200 L-0270-130139*0.0278
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 70-1301070.0214
Chlorobenzene mg/Kg wet0.0020 0.0200 70-1301120.0223
Chlorodibromomethane mg/Kg wet0.0010 0.0200 70-1301130.0226
Chloroethane mg/Kg wet0.020 0.0200 70-1301110.0222
Chloroform mg/Kg wet0.0040 0.0200 70-13092.20.0184
Chloromethane mg/Kg wet0.010 0.0200 70-13086.60.0173
2-Chlorotoluene mg/Kg wet0.0020 0.0200 70-1301040.0208
Page 31 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230058 - SW-846 5035
LCS (B230058-BS1) Prepared & Analyzed: 05/07/19
4-Chlorotoluene mg/Kg wet0.0020 0.0200 70-1301090.0218
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 V-0570-13071.00.0142
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 70-13098.30.0197
Dibromomethane mg/Kg wet0.0020 0.0200 70-1301030.0206
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301050.0209
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301080.0216
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301040.0207
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 70-13096.30.0193
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 V-05, J40-16074.20.0148
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 70-13098.90.0198
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 70-13099.10.0198
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 70-1301120.0224
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-13099.10.0198
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-1301000.0201
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-1301010.0201
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 70-13093.60.0187
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-13097.20.0194
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 70-13095.40.0191
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-1301050.0210
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13091.00.0182
Diethyl Ether mg/Kg wet0.020 0.0200 J70-13099.10.0198
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 70-13091.30.0183
1,4-Dioxane mg/Kg wet0.10 0.200 40-16080.30.161
Ethylbenzene mg/Kg wet0.0020 0.0200 70-1301070.0214
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 70-1601200.0240
2-Hexanone (MBK)mg/Kg wet0.020 0.200 70-1601020.204
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 70-1301230.0246
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 70-1301070.0213
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 V-0570-13086.40.0173
Methylene Chloride mg/Kg wet0.020 0.0200 J40-16091.10.0182
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 70-16092.70.185
Naphthalene mg/Kg wet0.0040 0.0200 40-13083.50.0167
n-Propylbenzene mg/Kg wet0.0020 0.0200 70-1301140.0229
Styrene mg/Kg wet0.0020 0.0200 70-1301070.0214
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 70-1301140.0227
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 70-13088.50.0177
Tetrachloroethylene mg/Kg wet0.0020 0.0200 V-2070-1301250.0251
Tetrahydrofuran mg/Kg wet0.010 0.0200 70-13080.10.0160
Toluene mg/Kg wet0.0020 0.0200 70-1301050.0210
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13090.70.0181
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-1301020.0204
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-1301130.0226
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 70-13098.40.0197
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 70-13095.50.0191
Trichloroethylene mg/Kg wet0.0020 0.0200 70-1301010.0201
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 70-1301030.0206
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 70-13087.60.0175
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 70-1301100.0220
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-13095.70.0191
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-1301110.0222
Vinyl Acetate mg/Kg wet0.050 0.200 70-13080.60.161
Page 32 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230058 - SW-846 5035
LCS (B230058-BS1) Prepared & Analyzed: 05/07/19
Vinyl Chloride mg/Kg wet0.010 0.0200 40-13089.70.0179
m+p Xylene mg/Kg wet0.0040 0.0400 70-1301040.0414
o-Xylene mg/Kg wet0.0020 0.0200 70-1301060.0211
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 84.80.0424
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 1020.0509
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1030.0515
LCS Dup (B230058-BSD1) Prepared & Analyzed: 05/07/19
Acetone mg/Kg wet0.10 0.200 2570-160131 20.70.261
Acrylonitrile mg/Kg wet0.0060 0.0200 25 V-0570-13071.5 0.5610.0143
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 2570-13090.1 1.340.0180
Benzene mg/Kg wet0.0020 0.0200 2570-13091.9 0.3270.0184
Bromobenzene mg/Kg wet0.0020 0.0200 2570-13098.7 2.400.0197
Bromochloromethane mg/Kg wet0.0020 0.0200 2570-13095.3 5.940.0191
Bromodichloromethane mg/Kg wet0.0020 0.0200 2570-130106 3.760.0211
Bromoform mg/Kg wet0.0020 0.0200 2570-13098.0 2.720.0196
Bromomethane mg/Kg wet0.010 0.0200 25 V-3440-13085.7 14.00.0171
2-Butanone (MEK)mg/Kg wet0.040 0.200 25 V-0570-16085.0 13.20.170
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 25 V-0540-13064.1 6.990.128
n-Butylbenzene mg/Kg wet0.0020 0.0200 2570-130104 0.1920.0208
sec-Butylbenzene mg/Kg wet0.0020 0.0200 2570-130116 4.310.0231
tert-Butylbenzene mg/Kg wet0.0020 0.0200 2570-160105 2.020.0210
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 2570-13085.2 1.300.0170
Carbon Disulfide mg/Kg wet0.0060 0.0200 25 L-0270-130138 0.868*0.0275
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 2570-130106 1.310.0212
Chlorobenzene mg/Kg wet0.0020 0.0200 2570-130114 1.950.0228
Chlorodibromomethane mg/Kg wet0.0010 0.0200 2570-130108 4.980.0215
Chloroethane mg/Kg wet0.020 0.0200 2570-130105 5.640.0210
Chloroform mg/Kg wet0.0040 0.0200 2570-13097.0 5.070.0194
Chloromethane mg/Kg wet0.010 0.0200 2570-13086.4 0.2310.0173
2-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-130102 1.750.0204
4-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-130108 0.6440.0217
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 25 V-0570-13073.2 3.050.0146
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 2570-13094.2 4.260.0188
Dibromomethane mg/Kg wet0.0020 0.0200 2570-13099.2 3.950.0198
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130106 1.800.0213
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130107 0.7440.0214
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130106 2.580.0212
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 2570-13090.3 6.430.0181
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 25 V-05, J40-16074.8 0.8050.0150
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 2570-13096.3 2.660.0193
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130101 1.500.0201
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 2570-130110 1.530.0220
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-130100 1.300.0201
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-130105 4.000.0209
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-13098.5 2.110.0197
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 2570-13094.9 1.380.0190
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-13094.2 3.130.0188
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 2570-13091.5 4.170.0183
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-130101 3.880.0202
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-13093.7 2.920.0187
Diethyl Ether mg/Kg wet0.020 0.0200 25 J70-13099.9 0.8040.0200
Page 33 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230058 - SW-846 5035
LCS Dup (B230058-BSD1) Prepared & Analyzed: 05/07/19
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 2570-13093.7 2.590.0187
1,4-Dioxane mg/Kg wet0.10 0.200 5040-16069.8 13.90.140
Ethylbenzene mg/Kg wet0.0020 0.0200 2570-130105 1.880.0210
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 2570-160114 5.210.0228
2-Hexanone (MBK)mg/Kg wet0.020 0.200 2570-16087.8 14.80.176
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 2570-130120 2.800.0240
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 2570-130110 2.770.0219
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 25 V-0570-13088.6 2.510.0177
Methylene Chloride mg/Kg wet0.020 0.0200 25 J40-16092.5 1.530.0185
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 2570-16090.2 2.740.180
Naphthalene mg/Kg wet0.0040 0.0200 2540-13084.0 0.5970.0168
n-Propylbenzene mg/Kg wet0.0020 0.0200 2570-130112 2.210.0224
Styrene mg/Kg wet0.0020 0.0200 2570-130108 0.9320.0216
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 2570-130115 0.9640.0229
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 2570-13084.7 4.390.0169
Tetrachloroethylene mg/Kg wet0.0020 0.0200 25 L-07, V-2070-130131 4.22*0.0262
Tetrahydrofuran mg/Kg wet0.010 0.0200 2570-13086.2 7.340.0172
Toluene mg/Kg wet0.0020 0.0200 2570-130107 1.700.0213
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13094.4 4.000.0189
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13096.4 5.450.0193
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-130108 4.800.0215
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 2570-13096.3 2.160.0193
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 2570-13094.5 1.050.0189
Trichloroethylene mg/Kg wet0.0020 0.0200 2570-130106 5.320.0212
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 2570-130103 0.1940.0207
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 2570-13092.3 5.230.0185
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 2570-130113 2.600.0226
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-13094.9 0.8390.0190
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-130107 3.760.0214
Vinyl Acetate mg/Kg wet0.050 0.200 2570-13081.4 1.060.163
Vinyl Chloride mg/Kg wet0.010 0.0200 2540-13087.5 2.480.0175
m+p Xylene mg/Kg wet0.0040 0.0400 2570-130104 0.6250.0417
o-Xylene mg/Kg wet0.0020 0.0200 2570-130104 2.010.0207
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 87.00.0435
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 1050.0527
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1040.0519
Batch B230248 - SW-846 5030B
[TOC_3]B230248[TOC]
Blank (B230248-BLK1) Prepared: 05/09/19 Analyzed: 05/10/19
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Page 34 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230248 - SW-846 5030B
Blank (B230248-BLK1) Prepared: 05/09/19 Analyzed: 05/10/19
Chlorobenzene g/L0.50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20 R-05ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11027.6
g/L 25.0 70-130Surrogate: Toluene-d8 10425.9
Page 35 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230248 - SW-846 5030B
Blank (B230248-BLK1) Prepared: 05/09/19 Analyzed: 05/10/19
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 99.024.7
LCS (B230248-BS1) Prepared: 05/09/19 Analyzed: 05/10/19
Acetone g/L50 100 L-0670-130149*149
Benzene g/L0.50 10.0 70-13010510.5
Bromobenzene g/L0.50 10.0 70-13011011.0
Bromochloromethane g/L0.50 10.0 70-13013013.0
Bromodichloromethane g/L0.50 10.0 70-13010810.8
Bromoform g/L0.50 10.0 70-13075.07.50
Bromomethane g/L1.0 10.0 60-14095.49.54
2-Butanone (MEK)g/L5.0 100 70-13093.893.8
n-Butylbenzene g/L0.50 10.0 70-13012212.2
sec-Butylbenzene g/L0.50 10.0 70-13012312.3
tert-Butylbenzene g/L0.50 10.0 70-13011911.9
Carbon Tetrachloride g/L0.50 10.0 70-13090.49.04
Chlorobenzene g/L0.50 10.0 70-13010810.8
Chlorodibromomethane g/L0.50 10.0 70-13095.19.51
Chloroethane g/L0.50 10.0 60-14012712.7
Chloroform g/L0.50 10.0 70-13010810.8
Chloromethane g/L0.60 10.0 60-14088.48.84
2-Chlorotoluene g/L0.50 10.0 70-13010710.7
4-Chlorotoluene g/L0.50 10.0 70-13011211.2
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010810.8
1,2-Dichlorobenzene g/L0.50 10.0 70-13011411.4
1,3-Dichlorobenzene g/L0.50 10.0 70-13011611.6
1,4-Dichlorobenzene g/L0.50 10.0 70-13011011.0
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14071.37.13
1,1-Dichloroethane g/L0.50 10.0 70-13012812.8
1,2-Dichloroethane g/L0.50 10.0 70-13010410.4
1,1-Dichloroethylene g/L0.50 10.0 L-0270-130150*15.0
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13011511.5
trans-1,2-Dichloroethylene g/L0.50 10.0 L-0270-130138*13.8
1,2-Dichloropropane g/L0.50 10.0 70-13010410.4
1,3-Dichloropropane g/L0.50 10.0 70-13010610.6
2,2-Dichloropropane g/L0.50 10.0 70-13081.98.19
1,1-Dichloropropene g/L0.50 10.0 70-13010910.9
cis-1,3-Dichloropropene g/L0.50 10.0 70-13011111.1
trans-1,3-Dichloropropene g/L0.50 10.0 70-13010810.8
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13012612.6
Ethylbenzene g/L0.50 10.0 70-13010810.8
2-Hexanone (MBK)g/L5.0 100 70-130104104
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010710.7
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13011711.7
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13012412.4
Methylene Chloride g/L5.0 10.0 L-0270-130169*16.9
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130107107
Naphthalene g/L0.50 10.0 70-13088.78.87
n-Propylbenzene g/L0.50 10.0 70-13011311.3
Styrene g/L0.50 10.0 70-13011811.8
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010710.7
Tetrachloroethylene g/L0.50 10.0 70-13010110.1
Toluene g/L0.50 10.0 70-13011011.0
Page 36 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230248 - SW-846 5030B
LCS (B230248-BS1) Prepared: 05/09/19 Analyzed: 05/10/19
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13096.69.66
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13090.09.00
1,1,1-Trichloroethane g/L0.50 10.0 70-13010310.3
1,1,2-Trichloroethane g/L0.50 10.0 70-13010610.6
Trichloroethylene g/L0.50 10.0 70-13010610.6
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13012212.2
1,2,3-Trichloropropane g/L0.50 10.0 70-13099.79.97
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13012012.0
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13011111.1
Vinyl Acetate g/L20 100 R-0570-130101101
Vinyl Chloride g/L0.50 10.0 60-14080.58.05
m+p Xylene g/L1.0 20.0 70-13011322.5
o-Xylene g/L0.50 10.0 70-13011611.6
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11428.4
g/L 25.0 70-130Surrogate: Toluene-d8 10526.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10425.9
LCS Dup (B230248-BSD1) Prepared: 05/09/19 Analyzed: 05/10/19
Acetone g/L50 100 25 L-0670-130176 16.4*176
Benzene g/L0.50 10.0 2570-130103 2.4110.3
Bromobenzene g/L0.50 10.0 2570-130108 1.3810.8
Bromochloromethane g/L0.50 10.0 2570-130126 3.2112.6
Bromodichloromethane g/L0.50 10.0 2570-130106 1.9610.6
Bromoform g/L0.50 10.0 2570-13076.7 2.247.67
Bromomethane g/L1.0 10.0 2560-140107 11.310.7
2-Butanone (MEK)g/L5.0 100 2570-13099.7 6.1299.7
n-Butylbenzene g/L0.50 10.0 2570-130118 3.4211.8
sec-Butylbenzene g/L0.50 10.0 2570-130117 5.0011.7
tert-Butylbenzene g/L0.50 10.0 2570-130115 2.8211.5
Carbon Tetrachloride g/L0.50 10.0 2570-13088.1 2.588.81
Chlorobenzene g/L0.50 10.0 2570-130107 1.1210.7
Chlorodibromomethane g/L0.50 10.0 2570-13094.1 1.069.41
Chloroethane g/L0.50 10.0 2560-140124 2.1512.4
Chloroform g/L0.50 10.0 2570-130106 2.0610.6
Chloromethane g/L0.60 10.0 2560-14085.4 3.458.54
2-Chlorotoluene g/L0.50 10.0 2570-130100 6.3610.0
4-Chlorotoluene g/L0.50 10.0 2570-130110 1.8011.0
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130101 6.4110.1
1,2-Dichlorobenzene g/L0.50 10.0 2570-130112 2.1311.2
1,3-Dichlorobenzene g/L0.50 10.0 2570-130110 5.3311.0
1,4-Dichlorobenzene g/L0.50 10.0 2570-130108 2.1110.8
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14070.2 1.557.02
1,1-Dichloroethane g/L0.50 10.0 2570-130127 0.70512.7
1,2-Dichloroethane g/L0.50 10.0 2570-130103 0.86910.3
1,1-Dichloroethylene g/L0.50 10.0 25 L-0270-130148 1.34*14.8
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130111 3.7211.1
trans-1,2-Dichloroethylene g/L0.50 10.0 25 L-0270-130133 3.61*13.3
1,2-Dichloropropane g/L0.50 10.0 2570-130103 1.7410.3
1,3-Dichloropropane g/L0.50 10.0 2570-130104 2.1010.4
2,2-Dichloropropane g/L0.50 10.0 2570-13076.8 6.437.68
1,1-Dichloropropene g/L0.50 10.0 2570-130104 4.9710.4
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130107 3.5910.7
Page 37 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230248 - SW-846 5030B
LCS Dup (B230248-BSD1) Prepared: 05/09/19 Analyzed: 05/10/19
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130106 2.1410.6
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130120 4.6312.0
Ethylbenzene g/L0.50 10.0 2570-130108 0.0010.8
2-Hexanone (MBK)g/L5.0 100 2570-130104 0.212104
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130105 1.9810.5
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130113 3.4711.3
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-130119 4.7711.9
Methylene Chloride g/L5.0 10.0 25 L-0270-130172 1.47*17.2
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130107 0.345107
Naphthalene g/L0.50 10.0 2570-13088.1 0.6798.81
n-Propylbenzene g/L0.50 10.0 2570-130109 2.9710.9
Styrene g/L0.50 10.0 2570-130115 2.4911.5
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130103 4.0010.3
Tetrachloroethylene g/L0.50 10.0 2570-130101 0.29710.1
Toluene g/L0.50 10.0 2570-130104 5.5310.4
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13096.4 0.2079.64
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13090.8 0.8859.08
1,1,1-Trichloroethane g/L0.50 10.0 2570-130103 0.19510.3
1,1,2-Trichloroethane g/L0.50 10.0 2570-130110 3.9011.0
Trichloroethylene g/L0.50 10.0 2570-130108 2.3410.8
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130118 3.1611.8
1,2,3-Trichloropropane g/L0.50 10.0 2570-130100 0.60010.0
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130116 3.0411.6
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130109 1.4610.9
Vinyl Acetate g/L20 100 25 R-0570-13075.0 29.7 *75.0
Vinyl Chloride g/L0.50 10.0 2560-14073.3 9.367.33
m+p Xylene g/L1.0 20.0 2570-130110 2.7921.9
o-Xylene g/L0.50 10.0 2570-130113 2.5311.3
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11629.0
g/L 25.0 70-130Surrogate: Toluene-d8 10225.6
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10425.9
Batch B230565 - SW-846 5030B [TOC_3]B230565[TOC]
Blank (B230565-BLK1) Prepared & Analyzed: 05/13/19
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
Page 38 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230565 - SW-846 5030B
Blank (B230565-BLK1) Prepared & Analyzed: 05/13/19
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10726.8
g/L 25.0 70-130Surrogate: Toluene-d8 10325.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10025.0
Page 39 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230565 - SW-846 5030B
LCS (B230565-BS1) Prepared & Analyzed: 05/13/19
Acetone g/L50 100 L-0670-130138*138
Benzene g/L0.50 10.0 70-13098.89.88
Bromobenzene g/L0.50 10.0 70-13010310.3
Bromochloromethane g/L0.50 10.0 70-13011711.7
Bromodichloromethane g/L0.50 10.0 70-13010610.6
Bromoform g/L0.50 10.0 70-13077.57.75
Bromomethane g/L1.0 10.0 60-14094.89.48
2-Butanone (MEK)g/L5.0 100 70-13082.882.8
n-Butylbenzene g/L0.50 10.0 70-13011211.2
sec-Butylbenzene g/L0.50 10.0 70-13011111.1
tert-Butylbenzene g/L0.50 10.0 70-13010810.8
Carbon Tetrachloride g/L0.50 10.0 70-13085.78.57
Chlorobenzene g/L0.50 10.0 70-13010210.2
Chlorodibromomethane g/L0.50 10.0 70-13098.09.80
Chloroethane g/L0.50 10.0 60-14013013.0
Chloroform g/L0.50 10.0 70-13098.09.80
Chloromethane g/L0.60 10.0 60-14099.59.95
2-Chlorotoluene g/L0.50 10.0 70-13098.39.83
4-Chlorotoluene g/L0.50 10.0 70-13010410.4
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010210.2
1,2-Dichlorobenzene g/L0.50 10.0 70-13010610.6
1,3-Dichlorobenzene g/L0.50 10.0 70-13010810.8
1,4-Dichlorobenzene g/L0.50 10.0 70-13010310.3
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14071.87.18
1,1-Dichloroethane g/L0.50 10.0 70-13010610.6
1,2-Dichloroethane g/L0.50 10.0 70-13096.99.69
1,1-Dichloroethylene g/L0.50 10.0 L-0270-130142*14.2
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010510.5
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13012612.6
1,2-Dichloropropane g/L0.50 10.0 70-13098.79.87
1,3-Dichloropropane g/L0.50 10.0 70-13010310.3
2,2-Dichloropropane g/L0.50 10.0 70-13075.27.52
1,1-Dichloropropene g/L0.50 10.0 70-13099.79.97
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010410.4
trans-1,3-Dichloropropene g/L0.50 10.0 70-13099.39.93
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13011411.4
Ethylbenzene g/L0.50 10.0 70-13010110.1
2-Hexanone (MBK)g/L5.0 100 70-130101101
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010110.1
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010910.9
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13010510.5
Methylene Chloride g/L5.0 10.0 L-0270-130164*16.4
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130105105
Naphthalene g/L0.50 10.0 70-13080.28.02
n-Propylbenzene g/L0.50 10.0 70-13010510.5
Styrene g/L0.50 10.0 70-13010810.8
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010110.1
Tetrachloroethylene g/L0.50 10.0 70-13096.79.67
Toluene g/L0.50 10.0 70-13010310.3
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13094.69.46
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13086.38.63
1,1,1-Trichloroethane g/L0.50 10.0 70-13093.39.33
Page 40 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230565 - SW-846 5030B
LCS (B230565-BS1) Prepared & Analyzed: 05/13/19
1,1,2-Trichloroethane g/L0.50 10.0 70-13010610.6
Trichloroethylene g/L0.50 10.0 70-13010110.1
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13011111.1
1,2,3-Trichloropropane g/L0.50 10.0 70-13094.79.47
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13011011.0
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010210.2
Vinyl Acetate g/L20 100 70-13084.484.4
Vinyl Chloride g/L0.50 10.0 L-0260-140278*27.8
m+p Xylene g/L1.0 20.0 70-13010420.8
o-Xylene g/L0.50 10.0 70-13010810.8
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10626.6
g/L 25.0 70-130Surrogate: Toluene-d8 10526.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10526.2
LCS Dup (B230565-BSD1) Prepared & Analyzed: 05/13/19
Acetone g/L50 100 25 L-0670-130150 8.83*150
Benzene g/L0.50 10.0 2570-13098.3 0.5079.83
Bromobenzene g/L0.50 10.0 2570-130102 1.3710.2
Bromochloromethane g/L0.50 10.0 2570-130120 2.0312.0
Bromodichloromethane g/L0.50 10.0 2570-130105 0.66510.5
Bromoform g/L0.50 10.0 2570-13083.6 7.578.36
Bromomethane g/L1.0 10.0 2560-140101 6.3310.1
2-Butanone (MEK)g/L5.0 100 2570-13090.3 8.6290.3
n-Butylbenzene g/L0.50 10.0 2570-130106 5.4910.6
sec-Butylbenzene g/L0.50 10.0 2570-130106 4.8810.6
tert-Butylbenzene g/L0.50 10.0 2570-130102 6.2810.2
Carbon Tetrachloride g/L0.50 10.0 2570-13081.9 4.538.19
Chlorobenzene g/L0.50 10.0 2570-130101 1.0810.1
Chlorodibromomethane g/L0.50 10.0 2570-130100 2.0210.0
Chloroethane g/L0.50 10.0 2560-140126 3.1312.6
Chloroform g/L0.50 10.0 2570-130101 2.6210.1
Chloromethane g/L0.60 10.0 2560-14091.3 8.609.13
2-Chlorotoluene g/L0.50 10.0 2570-13096.3 2.069.63
4-Chlorotoluene g/L0.50 10.0 2570-130104 0.096010.4
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130101 0.49310.1
1,2-Dichlorobenzene g/L0.50 10.0 2570-130104 2.8610.4
1,3-Dichlorobenzene g/L0.50 10.0 2570-130103 4.7610.3
1,4-Dichlorobenzene g/L0.50 10.0 2570-130100 3.1410.0
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14070.1 2.407.01
1,1-Dichloroethane g/L0.50 10.0 2570-130120 12.112.0
1,2-Dichloroethane g/L0.50 10.0 2570-13096.9 0.009.69
1,1-Dichloroethylene g/L0.50 10.0 25 L-0270-130142 0.704*14.2
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130105 0.095610.5
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130127 0.55212.7
1,2-Dichloropropane g/L0.50 10.0 2570-13097.3 1.439.73
1,3-Dichloropropane g/L0.50 10.0 2570-13099.0 4.259.90
2,2-Dichloropropane g/L0.50 10.0 2570-13072.3 3.937.23
1,1-Dichloropropene g/L0.50 10.0 2570-13096.0 3.789.60
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130102 2.4210.2
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13096.4 2.969.64
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130113 0.88211.3
Ethylbenzene g/L0.50 10.0 2570-13099.9 1.499.99
Page 41 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230565 - SW-846 5030B
LCS Dup (B230565-BSD1) Prepared & Analyzed: 05/13/19
2-Hexanone (MBK)g/L5.0 100 2570-130102 1.35102
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13098.5 2.909.85
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130100 8.3410.0
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-130124 16.212.4
Methylene Chloride g/L5.0 10.0 25 L-0270-130167 1.63*16.7
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130108 3.28108
Naphthalene g/L0.50 10.0 2570-13087.1 8.258.71
n-Propylbenzene g/L0.50 10.0 2570-130103 1.4410.3
Styrene g/L0.50 10.0 2570-130109 1.2910.9
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130105 3.6910.5
Tetrachloroethylene g/L0.50 10.0 2570-13097.8 1.139.78
Toluene g/L0.50 10.0 2570-130103 0.096910.3
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13099.1 4.659.91
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13090.8 5.089.08
1,1,1-Trichloroethane g/L0.50 10.0 2570-13093.6 0.3219.36
1,1,2-Trichloroethane g/L0.50 10.0 2570-130108 1.9710.8
Trichloroethylene g/L0.50 10.0 2570-13097.4 3.439.74
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130111 0.18111.1
1,2,3-Trichloropropane g/L0.50 10.0 2570-13097.1 2.509.71
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130103 6.1110.3
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13099.5 2.299.95
Vinyl Acetate g/L20 100 2570-13085.4 1.2185.4
Vinyl Chloride g/L0.50 10.0 25 L-0260-140227 20.4*22.7
m+p Xylene g/L1.0 20.0 2570-130102 1.9520.4
o-Xylene g/L0.50 10.0 2570-130104 2.9210.4
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10626.6
g/L 25.0 70-130Surrogate: Toluene-d8 10325.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10325.8
Page 42 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B230431 - SW-846 3546
[TOC_3]B230431[TOC]
Blank (B230431-BLK1) Prepared: 05/10/19 Analyzed: 05/13/19
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34 V-34ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 V-05ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34ND
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66 V-34ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17 V-34ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34ND
2,4-Dinitrophenol mg/Kg wet0.66ND
2,4-Dinitrotoluene mg/Kg wet0.34ND
2,6-Dinitrotoluene mg/Kg wet0.34ND
Di-n-octylphthalate mg/Kg wet0.34ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34ND
Hexachlorocyclopentadiene mg/Kg wet0.34 V-05ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Page 43 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230431 - SW-846 3546
Blank (B230431-BLK1) Prepared: 05/10/19 Analyzed: 05/13/19
2-Methylphenol mg/Kg wet0.34 V-05ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34ND
4-Nitroaniline mg/Kg wet0.34ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34ND
Pentachlorophenol mg/Kg wet0.34ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 65.64.38
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 68.74.58
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 66.02.20
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 75.22.51
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 89.15.94
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 1013.36
LCS (B230431-BS1) Prepared: 05/10/19 Analyzed: 05/13/19
Acenaphthene mg/Kg wet0.17 1.67 40-14071.11.19
Acenaphthylene mg/Kg wet0.17 1.67 40-14077.21.29
Acetophenone mg/Kg wet0.34 1.67 40-14065.71.09
Aniline mg/Kg wet0.34 1.67 V-3410-14051.20.853
Anthracene mg/Kg wet0.17 1.67 40-14085.51.43
Benzidine mg/Kg wet0.66 1.67 V-0540-1401222.03
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-14093.01.55
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-14089.61.49
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-14084.11.40
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-14074.01.23
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-14086.11.44
Benzoic Acid mg/Kg wet1.0 1.67 30-13062.81.05
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 40-14083.11.39
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 40-14070.01.17
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 40-14075.01.25
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 40-1401011.69
4-Bromophenylphenylether mg/Kg wet0.34 1.67 40-14091.71.53
Butylbenzylphthalate mg/Kg wet0.34 1.67 40-14095.11.58
Carbazole mg/Kg wet0.17 1.67 40-14081.91.37
4-Chloroaniline mg/Kg wet0.66 1.67 V-3410-14056.10.936
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 30-13080.61.34
2-Chloronaphthalene mg/Kg wet0.34 1.67 40-14072.61.21
Page 44 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230431 - SW-846 3546
LCS (B230431-BS1) Prepared: 05/10/19 Analyzed: 05/13/19
2-Chlorophenol mg/Kg wet0.34 1.67 30-13071.71.20
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 40-14087.71.46
Chrysene mg/Kg wet0.17 1.67 40-14092.31.54
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-14077.71.30
Dibenzofuran mg/Kg wet0.34 1.67 40-14080.21.34
Di-n-butylphthalate mg/Kg wet0.34 1.67 40-14090.51.51
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 40-14062.41.04
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 40-14060.41.01
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 40-14061.01.02
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 V-3420-14076.51.28
2,4-Dichlorophenol mg/Kg wet0.34 1.67 30-13077.71.30
Diethylphthalate mg/Kg wet0.34 1.67 40-14084.91.41
2,4-Dimethylphenol mg/Kg wet0.34 1.67 30-13066.21.10
Dimethylphthalate mg/Kg wet0.34 1.67 40-14083.51.39
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 30-13086.41.44
2,4-Dinitrophenol mg/Kg wet0.66 1.67 30-13068.31.14
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 40-14081.91.37
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 40-14086.11.43
Di-n-octylphthalate mg/Kg wet0.34 1.67 40-14090.81.51
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 40-14077.91.30
Fluoranthene mg/Kg wet0.17 1.67 40-14086.01.43
Fluorene mg/Kg wet0.17 1.67 40-14083.91.40
Hexachlorobenzene mg/Kg wet0.34 1.67 40-14085.61.43
Hexachlorobutadiene mg/Kg wet0.34 1.67 40-14069.51.16
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 V-0540-14048.40.807
Hexachloroethane mg/Kg wet0.34 1.67 40-14060.91.02
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-14076.91.28
Isophorone mg/Kg wet0.34 1.67 40-14071.81.20
1-Methylnaphthalene mg/Kg wet0.17 1.67 40-14064.81.08
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-14075.51.26
2-Methylphenol mg/Kg wet0.34 1.67 V-0530-13053.70.895
3/4-Methylphenol mg/Kg wet0.34 1.67 30-13066.21.10
Naphthalene mg/Kg wet0.17 1.67 40-14070.41.17
2-Nitroaniline mg/Kg wet0.34 1.67 40-14076.01.27
3-Nitroaniline mg/Kg wet0.34 1.67 30-14074.11.24
4-Nitroaniline mg/Kg wet0.34 1.67 40-14079.31.32
Nitrobenzene mg/Kg wet0.34 1.67 40-14066.31.10
2-Nitrophenol mg/Kg wet0.34 1.67 30-13079.81.33
4-Nitrophenol mg/Kg wet0.66 1.67 30-13076.91.28
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 40-14057.50.958
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 40-14089.61.49
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 40-14066.81.11
Pentachloronitrobenzene mg/Kg wet0.34 1.67 40-14082.71.38
Pentachlorophenol mg/Kg wet0.34 1.67 30-13065.51.09
Phenanthrene mg/Kg wet0.17 1.67 40-14085.41.42
Phenol mg/Kg wet0.34 1.67 30-13072.61.21
Pyrene mg/Kg wet0.17 1.67 40-14090.51.51
Pyridine mg/Kg wet0.34 1.67 30-14037.40.623
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 40-14074.21.24
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 40-14071.21.19
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 30-13083.81.40
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 30-13086.91.45
Page 45 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230431 - SW-846 3546
LCS (B230431-BS1) Prepared: 05/10/19 Analyzed: 05/13/19
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 70.34.69
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 70.44.70
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 70.72.36
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 81.72.72
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 92.46.16
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 1013.36
LCS Dup (B230431-BSD1) Prepared: 05/10/19 Analyzed: 05/13/19
Acenaphthene mg/Kg wet0.17 1.67 3040-14068.1 4.401.13
Acenaphthylene mg/Kg wet0.17 1.67 3040-14073.9 4.471.23
Acetophenone mg/Kg wet0.34 1.67 3040-14055.5 16.80.924
Aniline mg/Kg wet0.34 1.67 50 V-3410-14049.1 4.150.818
Anthracene mg/Kg wet0.17 1.67 3040-14083.9 1.911.40
Benzidine mg/Kg wet0.66 1.67 30 V-0540-140127 4.032.11
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-14089.2 4.191.49
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-14085.5 4.641.43
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-14079.6 5.501.33
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-14077.4 4.521.29
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-14082.5 4.291.37
Benzoic Acid mg/Kg wet1.0 1.67 50 J30-13058.0 8.010.967
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 3040-14076.1 8.791.27
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 3040-14056.9 20.60.948
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 3040-14061.8 19.41.03
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 3040-14096.0 5.531.60
4-Bromophenylphenylether mg/Kg wet0.34 1.67 3040-14088.9 3.171.48
Butylbenzylphthalate mg/Kg wet0.34 1.67 3040-14091.3 4.101.52
Carbazole mg/Kg wet0.17 1.67 3040-14081.1 1.061.35
4-Chloroaniline mg/Kg wet0.66 1.67 30 V-3410-14057.3 2.010.955
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 3030-13076.9 4.721.28
2-Chloronaphthalene mg/Kg wet0.34 1.67 3040-14069.8 3.991.16
2-Chlorophenol mg/Kg wet0.34 1.67 3030-13060.4 17.11.01
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 3040-14083.8 4.571.40
Chrysene mg/Kg wet0.17 1.67 3040-14089.8 2.681.50
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-14076.1 2.161.27
Dibenzofuran mg/Kg wet0.34 1.67 3040-14076.7 4.391.28
Di-n-butylphthalate mg/Kg wet0.34 1.67 3040-14088.1 2.691.47
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14049.5 23.20.824
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14048.2 22.40.804
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14048.5 22.90.808
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 50 V-3420-14078.2 2.171.30
2,4-Dichlorophenol mg/Kg wet0.34 1.67 3030-13073.9 5.041.23
Diethylphthalate mg/Kg wet0.34 1.67 3040-14081.6 3.961.36
2,4-Dimethylphenol mg/Kg wet0.34 1.67 3030-13070.9 6.771.18
Dimethylphthalate mg/Kg wet0.34 1.67 3040-14080.2 3.961.34
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 3030-13082.5 4.551.38
2,4-Dinitrophenol mg/Kg wet0.66 1.67 3030-13062.1 9.471.04
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14079.7 2.701.33
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14083.7 2.831.39
Di-n-octylphthalate mg/Kg wet0.34 1.67 3040-14084.9 6.781.41
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 3040-14076.5 1.791.28
Fluoranthene mg/Kg wet0.17 1.67 3040-14084.9 1.291.42
Fluorene mg/Kg wet0.17 1.67 3040-14079.5 5.391.32
Page 46 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230431 - SW-846 3546
LCS Dup (B230431-BSD1) Prepared: 05/10/19 Analyzed: 05/13/19
Hexachlorobenzene mg/Kg wet0.34 1.67 3040-14082.5 3.741.37
Hexachlorobutadiene mg/Kg wet0.34 1.67 3040-14057.6 18.70.960
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 30 V-0540-14040.3 18.30.672
Hexachloroethane mg/Kg wet0.34 1.67 3040-14048.7 22.40.811
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-14078.4 1.931.31
Isophorone mg/Kg wet0.34 1.67 3040-14065.2 9.661.09
1-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14059.7 8.290.994
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14069.9 7.731.17
2-Methylphenol mg/Kg wet0.34 1.67 30 V-0530-13048.3 10.60.805
3/4-Methylphenol mg/Kg wet0.34 1.67 3030-13060.6 8.811.01
Naphthalene mg/Kg wet0.17 1.67 3040-14060.8 14.51.01
2-Nitroaniline mg/Kg wet0.34 1.67 3040-14072.8 4.351.21
3-Nitroaniline mg/Kg wet0.34 1.67 3030-14071.4 3.741.19
4-Nitroaniline mg/Kg wet0.34 1.67 3040-14077.7 2.091.29
Nitrobenzene mg/Kg wet0.34 1.67 3040-14057.1 14.80.952
2-Nitrophenol mg/Kg wet0.34 1.67 3030-13070.0 13.21.17
4-Nitrophenol mg/Kg wet0.66 1.67 5030-13077.3 0.4671.29
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 3040-14045.0 24.40.749
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 3040-14088.3 1.371.47
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 3040-14058.6 13.10.976
Pentachloronitrobenzene mg/Kg wet0.34 1.67 3040-14080.3 2.971.34
Pentachlorophenol mg/Kg wet0.34 1.67 3030-13065.6 0.1221.09
Phenanthrene mg/Kg wet0.17 1.67 3040-14084.0 1.631.40
Phenol mg/Kg wet0.34 1.67 3030-13064.6 11.71.08
Pyrene mg/Kg wet0.17 1.67 3040-14087.5 3.351.46
Pyridine mg/Kg wet0.34 1.67 30 L-0730-14029.4 24.0*0.490
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 3040-14069.4 6.681.16
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 3040-14060.1 16.81.00
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 3030-13080.2 4.341.34
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 3030-13084.2 3.131.40
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 57.13.81
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 62.34.15
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 60.72.02
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 77.72.59
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 88.05.87
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 96.63.22
Matrix Spike (B230431-MS1) Prepared: 05/10/19 Analyzed: 05/13/19 Source: 19E0276-01
Acenaphthene mg/Kg dry0.18 1.79 40-14044.30.794 ND
Acenaphthylene mg/Kg dry0.18 1.79 40-14048.20.865 ND
Acetophenone mg/Kg dry0.37 1.79 MS-2240-14037.5 *0.673 ND
Aniline mg/Kg dry0.37 1.79 MS-09, V-34, J40-14017.2 *0.309 ND
Anthracene mg/Kg dry0.18 1.79 40-14052.00.932 ND
Benzidine mg/Kg dry0.71 1.79 MS-09, V-0540-140*ND ND
Benzo(a)anthracene mg/Kg dry0.18 1.79 40-14054.90.985 ND
Benzo(a)pyrene mg/Kg dry0.18 1.79 40-14054.30.975 ND
Benzo(b)fluoranthene mg/Kg dry0.18 1.79 40-14051.30.920 ND
Benzo(g,h,i)perylene mg/Kg dry0.18 1.79 40-14045.40.814 ND
Benzo(k)fluoranthene mg/Kg dry0.18 1.79 40-14052.60.944 ND
Benzoic Acid mg/Kg dry1.1 1.79 MS-22, J40-14038.3 *0.687 ND
Bis(2-chloroethoxy)methane mg/Kg dry0.37 1.79 40-14050.40.904 ND
Bis(2-chloroethyl)ether mg/Kg dry0.37 1.79 MS-2240-14038.4 *0.688 ND
Page 47 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230431 - SW-846 3546
Matrix Spike (B230431-MS1) Prepared: 05/10/19 Analyzed: 05/13/19 Source: 19E0276-01
Bis(2-chloroisopropyl)ether mg/Kg dry0.37 1.79 40-14042.90.769 ND
Bis(2-Ethylhexyl)phthalate mg/Kg dry0.37 1.79 40-14062.01.11 ND
4-Bromophenylphenylether mg/Kg dry0.37 1.79 40-14055.30.992 ND
Butylbenzylphthalate mg/Kg dry0.37 1.79 40-14057.31.03 ND
Carbazole mg/Kg dry0.18 1.79 40-14050.70.910 ND
4-Chloroaniline mg/Kg dry0.71 1.79 V-34, MS-22, J40-14038.5 *0.690 ND
4-Chloro-3-methylphenol mg/Kg dry0.71 1.79 30-13048.60.873 ND
2-Chloronaphthalene mg/Kg dry0.37 1.79 40-14040.80.732 ND
2-Chlorophenol mg/Kg dry0.37 1.79 30-13040.60.729 ND
4-Chlorophenylphenylether mg/Kg dry0.37 1.79 40-14052.90.950 ND
Chrysene mg/Kg dry0.18 1.79 40-14055.81.00 ND
Dibenz(a,h)anthracene mg/Kg dry0.18 1.79 40-14047.30.850 ND
Dibenzofuran mg/Kg dry0.37 1.79 40-14049.30.884 ND
Di-n-butylphthalate mg/Kg dry0.37 1.79 40-14056.61.02 ND
1,2-Dichlorobenzene mg/Kg dry0.37 1.79 MS-2240-14034.0 *0.610 ND
1,3-Dichlorobenzene mg/Kg dry0.37 1.79 MS-0940-14032.8 *0.589 ND
1,4-Dichlorobenzene mg/Kg dry0.37 1.79 MS-2240-14033.5 *0.602 ND
3,3-Dichlorobenzidine mg/Kg dry0.18 1.79 V-3440-14055.10.989 ND
2,4-Dichlorophenol mg/Kg dry0.37 1.79 30-13048.30.867 ND
Diethylphthalate mg/Kg dry0.37 1.79 40-14051.70.928 ND
2,4-Dimethylphenol mg/Kg dry0.37 1.79 30-13045.40.815 ND
Dimethylphthalate mg/Kg dry0.37 1.79 40-14051.40.922 ND
4,6-Dinitro-2-methylphenol mg/Kg dry0.37 1.79 30-13050.50.906 ND
2,4-Dinitrophenol mg/Kg dry0.71 1.79 30-13048.60.872 ND
2,4-Dinitrotoluene mg/Kg dry0.37 1.79 40-14049.60.889 ND
2,6-Dinitrotoluene mg/Kg dry0.37 1.79 40-14053.00.951 ND
Di-n-octylphthalate mg/Kg dry0.37 1.79 40-14055.40.993 ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg dry0.37 1.79 40-14049.20.883 ND
Fluoranthene mg/Kg dry0.18 1.79 40-14053.50.960 ND
Fluorene mg/Kg dry0.18 1.79 40-14050.30.902 ND
Hexachlorobenzene mg/Kg dry0.37 1.79 40-14052.30.939 ND
Hexachlorobutadiene mg/Kg dry0.37 1.79 MS-2240-14039.1 *0.702 ND
Hexachlorocyclopentadiene mg/Kg dry0.37 1.79 MS-22, V-0530-13025.2 *0.452 ND
Hexachloroethane mg/Kg dry0.37 1.79 MS-2240-14033.7 *0.605 ND
Indeno(1,2,3-cd)pyrene mg/Kg dry0.18 1.79 40-14047.50.852 ND
Isophorone mg/Kg dry0.37 1.79 40-14042.50.763 ND
1-Methylnaphthalene mg/Kg dry0.18 1.79 MS-2240-14038.8 *0.696 ND
2-Methylnaphthalene mg/Kg dry0.18 1.79 40-14045.50.816 ND
2-Methylphenol mg/Kg dry0.37 1.79 V-0530-13032.80.589 ND
3/4-Methylphenol mg/Kg dry0.37 1.79 30-13040.40.724 ND
Naphthalene mg/Kg dry0.18 1.79 40-14040.60.729 ND
2-Nitroaniline mg/Kg dry0.37 1.79 40-14045.50.816 ND
3-Nitroaniline mg/Kg dry0.37 1.79 40-14047.00.843 ND
4-Nitroaniline mg/Kg dry0.37 1.79 40-14046.60.836 ND
Nitrobenzene mg/Kg dry0.37 1.79 MS-2240-14038.0 *0.682 ND
2-Nitrophenol mg/Kg dry0.37 1.79 30-13045.30.813 ND
4-Nitrophenol mg/Kg dry0.71 1.79 30-13046.90.841 ND
N-Nitrosodimethylamine mg/Kg dry0.37 1.79 MS-0940-14028.7 *0.516 ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg dry0.37 1.79 40-14056.81.02 ND
N-Nitrosodi-n-propylamine mg/Kg dry0.37 1.79 MS-2240-14039.0 *0.700 ND
Pentachloronitrobenzene mg/Kg dry0.37 1.79 40-14050.70.909 ND
Pentachlorophenol mg/Kg dry0.37 1.79 30-13041.10.738 ND
Page 48 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230431 - SW-846 3546
Matrix Spike (B230431-MS1) Prepared: 05/10/19 Analyzed: 05/13/19 Source: 19E0276-01
Phenanthrene mg/Kg dry0.18 1.79 40-14052.60.945 ND
Phenol mg/Kg dry0.37 1.79 30-13042.00.754 ND
Pyrene mg/Kg dry0.18 1.79 40-14055.00.988 ND
Pyridine mg/Kg dry0.37 1.79 MS-0940-140*ND ND
1,2,4,5-Tetrachlorobenzene mg/Kg dry0.37 1.79 40-14044.90.806 ND
1,2,4-Trichlorobenzene mg/Kg dry0.37 1.79 40-14040.20.722 ND
2,4,5-Trichlorophenol mg/Kg dry0.37 1.79 30-13050.20.902 ND
2,4,6-Trichlorophenol mg/Kg dry0.37 1.79 30-13053.60.962 ND
mg/Kg dry 7.18 30-130Surrogate: 2-Fluorophenol 38.52.76
mg/Kg dry 7.18 30-130Surrogate: Phenol-d6 41.72.99
mg/Kg dry 3.59 30-130Surrogate: Nitrobenzene-d5 40.51.45
mg/Kg dry 3.59 30-130Surrogate: 2-Fluorobiphenyl 50.81.83
mg/Kg dry 7.18 30-130Surrogate: 2,4,6-Tribromophenol 55.43.98
mg/Kg dry 3.59 30-130Surrogate: p-Terphenyl-d14 60.32.16
Matrix Spike Dup (B230431-MSD1) Prepared: 05/10/19 Analyzed: 05/13/19 Source: 19E0276-01
Acenaphthene mg/Kg dry0.18 1.79 3040-14047.8 7.360.855 ND
Acenaphthylene mg/Kg dry0.18 1.79 3040-14052.9 8.930.946 ND
Acetophenone mg/Kg dry0.36 1.79 3040-14044.2 16.20.791 ND
Aniline mg/Kg dry0.36 1.79 30 MS-09, V-3440-14022.0 24.0*0.393 ND
Anthracene mg/Kg dry0.18 1.79 3040-14059.2 12.71.06 ND
Benzidine mg/Kg dry0.71 1.79 30 MS-09, V-0540-140*ND ND
Benzo(a)anthracene mg/Kg dry0.18 1.79 3040-14063.3 13.91.13 ND
Benzo(a)pyrene mg/Kg dry0.18 1.79 3040-14060.4 10.21.08 ND
Benzo(b)fluoranthene mg/Kg dry0.18 1.79 3040-14056.1 8.691.00 ND
Benzo(g,h,i)perylene mg/Kg dry0.18 1.79 3040-14050.6 10.60.905 ND
Benzo(k)fluoranthene mg/Kg dry0.18 1.79 3040-14058.7 10.71.05 ND
Benzoic Acid mg/Kg dry1.1 1.79 30 J40-14040.7 5.950.729 ND
Bis(2-chloroethoxy)methane mg/Kg dry0.36 1.79 3040-14057.4 12.61.03 ND
Bis(2-chloroethyl)ether mg/Kg dry0.36 1.79 3040-14046.8 19.60.838 ND
Bis(2-chloroisopropyl)ether mg/Kg dry0.36 1.79 3040-14050.9 16.90.911 ND
Bis(2-Ethylhexyl)phthalate mg/Kg dry0.36 1.79 3040-14068.0 8.931.22 ND
4-Bromophenylphenylether mg/Kg dry0.36 1.79 3040-14061.0 9.541.09 ND
Butylbenzylphthalate mg/Kg dry0.36 1.79 3040-14063.9 10.61.14 ND
Carbazole mg/Kg dry0.18 1.79 3040-14057.2 11.71.02 ND
4-Chloroaniline mg/Kg dry0.71 1.79 30 V-3440-14044.7 14.70.800 ND
4-Chloro-3-methylphenol mg/Kg dry0.71 1.79 3030-13054.1 10.30.967 ND
2-Chloronaphthalene mg/Kg dry0.36 1.79 3040-14044.4 8.030.793 ND
2-Chlorophenol mg/Kg dry0.36 1.79 3030-13047.7 15.80.854 ND
4-Chlorophenylphenylether mg/Kg dry0.36 1.79 3040-14058.6 9.821.05 ND
Chrysene mg/Kg dry0.18 1.79 3040-14062.3 10.71.11 ND
Dibenz(a,h)anthracene mg/Kg dry0.18 1.79 3040-14050.6 6.330.905 ND
Dibenzofuran mg/Kg dry0.36 1.79 3040-14054.5 9.850.976 ND
Di-n-butylphthalate mg/Kg dry0.36 1.79 3040-14062.7 9.831.12 ND
1,2-Dichlorobenzene mg/Kg dry0.36 1.79 3040-14041.4 19.20.740 ND
1,3-Dichlorobenzene mg/Kg dry0.36 1.79 30 MS-0940-14039.8 18.8*0.711 ND
1,4-Dichlorobenzene mg/Kg dry0.36 1.79 3040-14040.1 17.60.717 ND
3,3-Dichlorobenzidine mg/Kg dry0.18 1.79 30 V-3440-14064.0 14.61.15 ND
2,4-Dichlorophenol mg/Kg dry0.36 1.79 3030-13054.1 10.90.967 ND
Diethylphthalate mg/Kg dry0.36 1.79 3040-14056.9 9.251.02 ND
2,4-Dimethylphenol mg/Kg dry0.36 1.79 3030-13048.8 6.800.873 ND
Dimethylphthalate mg/Kg dry0.36 1.79 3040-14057.9 11.51.04 ND
Page 49 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B230431 - SW-846 3546
Matrix Spike Dup (B230431-MSD1) Prepared: 05/10/19 Analyzed: 05/13/19 Source: 19E0276-01
4,6-Dinitro-2-methylphenol mg/Kg dry0.36 1.79 3030-13057.9 13.41.04 ND
2,4-Dinitrophenol mg/Kg dry0.71 1.79 3030-13052.3 6.930.935 ND
2,4-Dinitrotoluene mg/Kg dry0.36 1.79 3040-14055.9 11.71.00 ND
2,6-Dinitrotoluene mg/Kg dry0.36 1.79 3040-14057.3 7.501.03 ND
Di-n-octylphthalate mg/Kg dry0.36 1.79 3040-14061.5 10.11.10 ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg dry0.36 1.79 3040-14053.8 8.530.962 ND
Fluoranthene mg/Kg dry0.18 1.79 3040-14060.5 11.91.08 ND
Fluorene mg/Kg dry0.18 1.79 3040-14055.9 10.31.00 ND
Hexachlorobenzene mg/Kg dry0.36 1.79 3040-14058.6 11.01.05 ND
Hexachlorobutadiene mg/Kg dry0.36 1.79 3040-14047.2 18.40.845 ND
Hexachlorocyclopentadiene mg/Kg dry0.36 1.79 30 V-0530-13030.9 20.10.553 ND
Hexachloroethane mg/Kg dry0.36 1.79 3040-14040.9 18.90.732 ND
Indeno(1,2,3-cd)pyrene mg/Kg dry0.18 1.79 3040-14052.1 9.070.933 ND
Isophorone mg/Kg dry0.36 1.79 3040-14049.9 15.70.893 ND
1-Methylnaphthalene mg/Kg dry0.18 1.79 3040-14044.5 13.30.795 ND
2-Methylnaphthalene mg/Kg dry0.18 1.79 3040-14051.6 12.30.923 ND
2-Methylphenol mg/Kg dry0.36 1.79 30 V-0530-13036.3 9.680.649 ND
3/4-Methylphenol mg/Kg dry0.36 1.79 3030-13044.8 10.10.802 ND
Naphthalene mg/Kg dry0.18 1.79 3040-14048.2 16.90.863 ND
2-Nitroaniline mg/Kg dry0.36 1.79 3040-14050.4 9.900.901 ND
3-Nitroaniline mg/Kg dry0.36 1.79 3040-14051.8 9.440.926 ND
4-Nitroaniline mg/Kg dry0.36 1.79 3040-14053.3 13.10.954 ND
Nitrobenzene mg/Kg dry0.36 1.79 3040-14044.3 15.10.793 ND
2-Nitrophenol mg/Kg dry0.36 1.79 3030-13052.6 14.60.940 ND
4-Nitrophenol mg/Kg dry0.71 1.79 3030-13051.8 9.760.927 ND
N-Nitrosodimethylamine mg/Kg dry0.36 1.79 30 MS-0940-14036.1 22.3*0.645 ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg dry0.36 1.79 3040-14062.8 9.641.12 ND
N-Nitrosodi-n-propylamine mg/Kg dry0.36 1.79 3040-14045.8 15.70.819 ND
Pentachloronitrobenzene mg/Kg dry0.36 1.79 3040-14056.7 10.81.01 ND
Pentachlorophenol mg/Kg dry0.36 1.79 3030-13045.2 9.040.808 ND
Phenanthrene mg/Kg dry0.18 1.79 3040-14058.6 10.31.05 ND
Phenol mg/Kg dry0.36 1.79 3030-13048.5 14.00.868 ND
Pyrene mg/Kg dry0.18 1.79 3040-14062.1 11.81.11 ND
Pyridine mg/Kg dry0.36 1.79 30 MS-0940-140*ND ND
1,2,4,5-Tetrachlorobenzene mg/Kg dry0.36 1.79 3040-14051.1 12.60.915 ND
1,2,4-Trichlorobenzene mg/Kg dry0.36 1.79 3040-14046.7 14.60.836 ND
2,4,5-Trichlorophenol mg/Kg dry0.36 1.79 3030-13056.1 10.71.00 ND
2,4,6-Trichlorophenol mg/Kg dry0.36 1.79 3030-13058.0 7.591.04 ND
mg/Kg dry 7.15 30-130Surrogate: 2-Fluorophenol 46.63.33
mg/Kg dry 7.15 30-130Surrogate: Phenol-d6 48.83.50
mg/Kg dry 3.58 30-130Surrogate: Nitrobenzene-d5 47.71.71
mg/Kg dry 3.58 30-130Surrogate: 2-Fluorobiphenyl 56.42.02
mg/Kg dry 7.15 30-130Surrogate: 2,4,6-Tribromophenol 62.34.45
mg/Kg dry 3.58 30-130Surrogate: p-Terphenyl-d14 68.62.45
Page 50 of 68
Table of Contents
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - EPH[TOC]
Batch B229933 - SW-846 3546
[TOC_3]B229933[TOC]
Blank (B229933-BLK1) Prepared: 05/06/19 Analyzed: 05/08/19
C9-C18 Aliphatics mg/Kg wet10ND
C19-C36 Aliphatics mg/Kg wet10ND
Unadjusted C11-C22 Aromatics mg/Kg wet10ND
C11-C22 Aromatics mg/Kg wet10ND
Acenaphthene mg/Kg wet0.10ND
Acenaphthylene mg/Kg wet0.10ND
Anthracene mg/Kg wet0.10ND
Benzo(a)anthracene mg/Kg wet0.10ND
Benzo(a)pyrene mg/Kg wet0.10ND
Benzo(b)fluoranthene mg/Kg wet0.10ND
Benzo(g,h,i)perylene mg/Kg wet0.10ND
Benzo(k)fluoranthene mg/Kg wet0.10ND
Chrysene mg/Kg wet0.10ND
Dibenz(a,h)anthracene mg/Kg wet0.10ND
Fluoranthene mg/Kg wet0.10ND
Fluorene mg/Kg wet0.10ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10ND
2-Methylnaphthalene mg/Kg wet0.10ND
Naphthalene mg/Kg wet0.10ND
Phenanthrene mg/Kg wet0.10ND
Pyrene mg/Kg wet0.10ND
n-Decane mg/Kg wet0.10ND
n-Docosane mg/Kg wet0.10ND
n-Dodecane mg/Kg wet0.10ND
n-Eicosane mg/Kg wet0.10ND
n-Hexacosane mg/Kg wet0.10ND
n-Hexadecane mg/Kg wet0.10ND
n-Hexatriacontane mg/Kg wet0.10ND
n-Nonadecane mg/Kg wet0.10ND
n-Nonane mg/Kg wet0.10ND
n-Octacosane mg/Kg wet0.10ND
n-Octadecane mg/Kg wet0.10ND
n-Tetracosane mg/Kg wet0.10ND
n-Tetradecane mg/Kg wet0.10ND
n-Triacontane mg/Kg wet0.10ND
Naphthalene-aliphatic fraction mg/Kg wet0.10ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)70.43.52
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)80.54.03
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 81.24.06
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 87.74.38
LCS (B229933-BS1) Prepared: 05/06/19 Analyzed: 05/08/19
C9-C18 Aliphatics mg/Kg wet10 30.0 40-14074.322.3
C19-C36 Aliphatics mg/Kg wet10 40.0 40-14085.734.3
Unadjusted C11-C22 Aromatics mg/Kg wet10 85.0 40-14081.569.2
Acenaphthene mg/Kg wet0.10 5.00 40-14071.43.57
Acenaphthylene mg/Kg wet0.10 5.00 40-14066.23.31
Anthracene mg/Kg wet0.10 5.00 40-14078.43.92
Benzo(a)anthracene mg/Kg wet0.10 5.00 40-14080.54.02
Benzo(a)pyrene mg/Kg wet0.10 5.00 40-14080.34.01
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 40-14081.14.06
Page 51 of 68
Table of Contents
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B229933 - SW-846 3546
LCS (B229933-BS1) Prepared: 05/06/19 Analyzed: 05/08/19
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 40-14076.03.80
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 40-14081.54.07
Chrysene mg/Kg wet0.10 5.00 40-14082.44.12
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 40-14082.84.14
Fluoranthene mg/Kg wet0.10 5.00 40-14080.24.01
Fluorene mg/Kg wet0.10 5.00 40-14072.53.63
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 40-14076.73.83
2-Methylnaphthalene mg/Kg wet0.10 5.00 40-14061.73.09
Naphthalene mg/Kg wet0.10 5.00 40-14064.73.23
Phenanthrene mg/Kg wet0.10 5.00 40-14077.53.88
Pyrene mg/Kg wet0.10 5.00 40-14081.24.06
n-Decane mg/Kg wet0.10 5.00 40-14055.22.76
n-Docosane mg/Kg wet0.10 5.00 40-14081.74.08
n-Dodecane mg/Kg wet0.10 5.00 40-14064.03.20
n-Eicosane mg/Kg wet0.10 5.00 40-14082.34.12
n-Hexacosane mg/Kg wet0.10 5.00 40-14080.54.03
n-Hexadecane mg/Kg wet0.10 5.00 40-14080.04.00
n-Hexatriacontane mg/Kg wet0.10 5.00 40-14079.03.95
n-Nonadecane mg/Kg wet0.10 5.00 40-14079.83.99
n-Nonane mg/Kg wet0.10 5.00 30-14041.72.08
n-Octacosane mg/Kg wet0.10 5.00 40-14077.73.89
n-Octadecane mg/Kg wet0.10 5.00 40-14080.64.03
n-Tetracosane mg/Kg wet0.10 5.00 40-14081.04.05
n-Tetradecane mg/Kg wet0.10 5.00 40-14072.33.62
n-Triacontane mg/Kg wet0.10 5.00 40-14077.03.85
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)73.53.67
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)78.83.94
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 87.34.37
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 96.24.81
LCS Dup (B229933-BSD1) Prepared: 05/06/19 Analyzed: 05/08/19
C9-C18 Aliphatics mg/Kg wet10 30.0 2540-14075.7 1.8722.7
C19-C36 Aliphatics mg/Kg wet10 40.0 2540-14091.0 5.9536.4
Unadjusted C11-C22 Aromatics mg/Kg wet10 85.0 2540-14083.6 2.6071.1
Acenaphthene mg/Kg wet0.10 5.00 2540-14071.9 0.6983.59
Acenaphthylene mg/Kg wet0.10 5.00 2540-14065.9 0.3823.29
Anthracene mg/Kg wet0.10 5.00 2540-14082.6 5.134.13
Benzo(a)anthracene mg/Kg wet0.10 5.00 2540-14083.7 3.974.19
Benzo(a)pyrene mg/Kg wet0.10 5.00 2540-14083.4 3.764.17
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 2540-14084.4 3.914.22
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 2540-14079.0 3.893.95
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 2540-14084.4 3.564.22
Chrysene mg/Kg wet0.10 5.00 2540-14085.2 3.354.26
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 2540-14085.6 3.314.28
Fluoranthene mg/Kg wet0.10 5.00 2540-14083.9 4.574.20
Fluorene mg/Kg wet0.10 5.00 2540-14075.1 3.473.75
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 2540-14079.5 3.593.97
2-Methylnaphthalene mg/Kg wet0.10 5.00 2540-14058.6 5.182.93
Naphthalene mg/Kg wet0.10 5.00 2540-14059.2 8.922.96
Phenanthrene mg/Kg wet0.10 5.00 2540-14081.2 4.634.06
Page 52 of 68
Table of Contents
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B229933 - SW-846 3546
LCS Dup (B229933-BSD1) Prepared: 05/06/19 Analyzed: 05/08/19
Pyrene mg/Kg wet0.10 5.00 2540-14084.9 4.534.25
n-Decane mg/Kg wet0.10 5.00 2540-14046.8 16.62.34
n-Docosane mg/Kg wet0.10 5.00 2540-14085.5 4.584.27
n-Dodecane mg/Kg wet0.10 5.00 2540-14057.7 10.32.89
n-Eicosane mg/Kg wet0.10 5.00 2540-14082.4 0.1244.12
n-Hexacosane mg/Kg wet0.10 5.00 2540-14084.3 4.614.22
n-Hexadecane mg/Kg wet0.10 5.00 2540-14082.5 3.094.12
n-Hexatriacontane mg/Kg wet0.10 5.00 2540-14082.5 4.264.12
n-Nonadecane mg/Kg wet0.10 5.00 2540-14083.5 4.544.18
n-Nonane mg/Kg wet0.10 5.00 2530-14034.2 19.71.71
n-Octacosane mg/Kg wet0.10 5.00 2540-14081.7 5.024.09
n-Octadecane mg/Kg wet0.10 5.00 2540-14084.7 5.034.24
n-Tetracosane mg/Kg wet0.10 5.00 2540-14084.9 4.734.24
n-Tetradecane mg/Kg wet0.10 5.00 2540-14071.0 1.763.55
n-Triacontane mg/Kg wet0.10 5.00 2540-14080.9 5.004.05
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)75.23.76
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)82.24.11
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 88.14.40
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 96.74.83
Page 53 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B229919 - MA VPH
[TOC_3]B229919[TOC]
Blank (B229919-BLK1) Prepared & Analyzed: 05/06/19
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12349.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11546.0
LCS (B229919-BS1) Prepared & Analyzed: 05/06/19
Benzene mg/Kg wet0.0010 0.0500 70-13094.60.0473
Butylcyclohexane mg/Kg wet0.0010 0.0500 70-1301170.0586
Decane mg/Kg wet0.0010 0.0500 70-13093.90.0469
Ethylbenzene mg/Kg wet0.0010 0.0500 70-13094.60.0473
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.0500 70-13089.60.0448
2-Methylpentane mg/Kg wet0.0010 0.0500 70-1301070.0537
Naphthalene mg/Kg wet0.010 0.0500 70-13093.70.0469
Nonane mg/Kg wet0.0010 0.0500 30-1301140.0569
Pentane mg/Kg wet0.0010 0.0500 70-13099.60.0498
Toluene mg/Kg wet0.0010 0.0500 70-13095.00.0475
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.0500 70-13094.70.0474
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.0500 70-1301040.0522
m+p Xylene mg/Kg wet0.0020 0.100 70-13095.30.0953
o-Xylene mg/Kg wet0.0010 0.0500 70-13094.90.0475
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10441.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10341.4
LCS Dup (B229919-BSD1) Prepared & Analyzed: 05/06/19
Benzene mg/Kg wet0.0010 0.0500 2570-13095.3 0.7690.0477
Butylcyclohexane mg/Kg wet0.0010 0.0500 2570-130117 0.1710.0585
Decane mg/Kg wet0.0010 0.0500 2570-13092.4 1.620.0462
Ethylbenzene mg/Kg wet0.0010 0.0500 2570-13096.3 1.760.0481
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.0500 2570-13089.2 0.4700.0446
2-Methylpentane mg/Kg wet0.0010 0.0500 2570-130110 1.930.0548
Naphthalene mg/Kg wet0.010 0.0500 2570-13092.9 0.9560.0464
Nonane mg/Kg wet0.0010 0.0500 2530-130113 0.3650.0567
Pentane mg/Kg wet0.0010 0.0500 2570-130103 3.420.0515
Toluene mg/Kg wet0.0010 0.0500 2570-13095.9 0.9870.0480
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.0500 2570-13096.4 1.700.0482
Page 54 of 68
Table of Contents
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B229919 - MA VPH
LCS Dup (B229919-BSD1) Prepared & Analyzed: 05/06/19
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.0500 2570-130105 0.4070.0524
m+p Xylene mg/Kg wet0.0020 0.100 2570-13097.1 1.850.0971
o-Xylene mg/Kg wet0.0010 0.0500 2570-13096.5 1.640.0483
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12048.1
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11445.4
Page 55 of 68
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)[TOC]
Batch B230325 - % Solids
[TOC_3]B230325[TOC]
Duplicate (B230325-DUP1) Prepared & Analyzed: 05/09/19 Source: 19E0276-01
% Solids % Wt 200.13991.2 91.4
Page 56 of 68
Table of Contents
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the high side.
L-06
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits. Possibility of sample
matrix effects that lead to a low bias for reported result or non-homogeneous sample aliquots cannot be
eliminated.
MS-09
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the
two MS/MSD results is within method specified criteria.
MS-22
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Elevated reporting limit due to high concentration of target compounds.RL-11
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
[TOC_1]Flag/Qualifier Summary[TOC]
Page 57 of 68
Table of Contents
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-EPH-04-1.1 in Soil
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
CT,NC,ME,NH-PAcenaphthene
CT,NC,ME,NH-PAcenaphthylene
CT,NC,ME,NH-PAnthracene
CT,NC,ME,NH-PBenzo(a)anthracene
CT,NC,ME,NH-PBenzo(a)pyrene
CT,NC,ME,NH-PBenzo(b)fluoranthene
CT,NC,ME,NH-PBenzo(g,h,i)perylene
CT,NC,ME,NH-PBenzo(k)fluoranthene
CT,NC,ME,NH-PChrysene
CT,NC,ME,NH-PDibenz(a,h)anthracene
CT,NC,ME,NH-PFluoranthene
CT,NC,MEFluorene
CT,NC,ME,NH-PIndeno(1,2,3-cd)pyrene
CT,NC,ME2-Methylnaphthalene
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PPhenanthrene
CT,NC,ME,NH-PPyrene
MADEP-EPH-04-1.1 in Water
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
CT,NC,ME,NH-PAcenaphthene
CT,NC,ME,NH-PAcenaphthylene
CT,NC,ME,NH-PAnthracene
CT,NC,ME,NH-PBenzo(a)anthracene
CT,NC,ME,NH-PBenzo(a)pyrene
CT,NC,ME,NH-PBenzo(b)fluoranthene
CT,NC,ME,NH-PBenzo(g,h,i)perylene
CT,NC,ME,NH-PBenzo(k)fluoranthene
CT,NC,ME,NH-PChrysene
CT,NC,ME,NH-PDibenz(a,h)anthracene
CT,NC,ME,NH-PFluoranthene
CT,NC,MEFluorene
CT,NC,ME,NH-PIndeno(1,2,3-cd)pyrene
CT,NC,ME2-Methylnaphthalene
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PPhenanthrene
CT,NC,ME,NH-PPyrene
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
[TOC_1]Certifications[TOC]
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Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
CT,NC,ME,NH-PBenzene
CT,NC,ME,NH-PEthylbenzene
CT,NC,ME,NH-PMethyl tert-Butyl Ether (MTBE)
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PToluene
CT,NC,ME,NH-Pm+p Xylene
CT,NC,ME,NH-Po-Xylene
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
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SM21-22 6200B in Water
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8260D in Soil
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
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SW-846 8260D in Soil
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
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SW-846 8260D in Soil
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8270E in Soil
CT,NY,NH,ME,NC,VAAcenaphthene
CT,NY,NH,ME,NC,VAAcenaphthylene
NY,NH,ME,NC,VAAcetophenone
NY,NH,ME,NC,VAAniline
CT,NY,NH,ME,NC,VAAnthracene
CT,NY,NH,ME,NC,VABenzidine
CT,NY,NH,ME,NC,VABenzo(a)anthracene
CT,NY,NH,ME,NC,VABenzo(a)pyrene
CT,NY,NH,ME,NC,VABenzo(b)fluoranthene
CT,NY,NH,ME,NC,VABenzo(g,h,i)perylene
CT,NY,NH,ME,NC,VABenzo(k)fluoranthene
NY,NH,ME,NC,VABenzoic Acid
CT,NY,NH,ME,NC,VABis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VABis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VABis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VABis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA4-Bromophenylphenylether
CT,NY,NH,ME,NC,VAButylbenzylphthalate
NCCarbazole
CT,NY,NH,ME,NC,VA4-Chloroaniline
CT,NY,NH,ME,NC,VA4-Chloro-3-methylphenol
CT,NY,NH,NC,VA2-Chloronaphthalene
CT,NY,NH,ME,NC,VA2-Chlorophenol
CT,NY,NH,ME,NC,VA4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VAChrysene
CT,NY,NH,ME,NC,VADibenz(a,h)anthracene
CT,NY,NH,ME,NC,VADibenzofuran
CT,NY,NH,ME,NC,VADi-n-butylphthalate
NY,NH,ME,NC,VA1,2-Dichlorobenzene
NY,NH,ME,NC,VA1,3-Dichlorobenzene
NY,NH,ME,NC,VA1,4-Dichlorobenzene
CT,NY,NH,ME,NC,VA3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA2,4-Dichlorophenol
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SW-846 8270E in Soil
CT,NY,NH,ME,NC,VADiethylphthalate
CT,NY,NH,ME,NC,VA2,4-Dimethylphenol
CT,NY,NH,ME,NC,VADimethylphthalate
CT,NY,NH,ME,NC,VA4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VADi-n-octylphthalate
NY,NH,ME,NC,VA1,2-Diphenylhydrazine/Azobenzene
CT,NY,NH,ME,NC,VAFluoranthene
NY,NH,ME,NC,VAFluorene
CT,NY,NH,ME,NC,VAHexachlorobenzene
CT,NY,NH,ME,NC,VAHexachlorobutadiene
CT,NY,NH,ME,NC,VAHexachlorocyclopentadiene
CT,NY,NH,ME,NC,VAHexachloroethane
CT,NY,NH,ME,NC,VAIndeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylphenol
CT,NY,NH,ME,NC,VA3/4-Methylphenol
CT,NY,NH,ME,NC,VANaphthalene
CT,NY,NH,ME,NC,VA2-Nitroaniline
CT,NY,NH,ME,NC,VA3-Nitroaniline
CT,NY,NH,ME,NC,VA4-Nitroaniline
CT,NY,NH,ME,NC,VANitrobenzene
CT,NY,NH,ME,NC,VA2-Nitrophenol
CT,NY,NH,ME,NC,VA4-Nitrophenol
CT,NY,NH,ME,NC,VAN-Nitrosodimethylamine
CT,NY,NH,ME,NC,VAN-Nitrosodi-n-propylamine
NY,NCPentachloronitrobenzene
CT,NY,NH,ME,NC,VAPentachlorophenol
CT,NY,NH,ME,NC,VAPhenanthrene
CT,NY,NH,ME,NC,VAPhenol
CT,NY,NH,ME,NC,VAPyrene
CT,NY,NH,ME,NC,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NH,ME,NC,VA1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
SW-846 8270E in Water
CT,NY,NC,ME,NH,VAAcenaphthene
CT,NY,NC,ME,NH,VAAcenaphthylene
NY,NCAcetophenone
CT,NY,NC,ME,VAAniline
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SW-846 8270E in Water
CT,NY,NC,ME,NH,VAAnthracene
CT,NY,NC,ME,NH,VABenzidine
CT,NY,NC,ME,NH,VABenzo(a)anthracene
CT,NY,NC,ME,NH,VABenzo(a)pyrene
CT,NY,NC,ME,NH,VABenzo(b)fluoranthene
CT,NY,NC,ME,NH,VABenzo(g,h,i)perylene
CT,NY,NC,ME,NH,VABenzo(k)fluoranthene
NY,NC,ME,NH,VABenzoic Acid
CT,NY,NC,ME,NH,VABis(2-chloroethoxy)methane
CT,NY,NC,ME,NH,VABis(2-chloroethyl)ether
CT,NY,NC,ME,NH,VABis(2-chloroisopropyl)ether
CT,NY,NC,ME,NH,VABis(2-Ethylhexyl)phthalate
CT,NY,NC,ME,NH,VA4-Bromophenylphenylether
CT,NY,NC,ME,NH,VAButylbenzylphthalate
NCCarbazole
CT,NY,NC,ME,NH,VA4-Chloroaniline
CT,NY,NC,ME,NH,VA4-Chloro-3-methylphenol
CT,NY,NC,ME,NH,VA2-Chloronaphthalene
CT,NY,NC,ME,NH,VA2-Chlorophenol
CT,NY,NC,ME,NH,VA4-Chlorophenylphenylether
CT,NY,NC,ME,NH,VAChrysene
CT,NY,NC,ME,NH,VADibenz(a,h)anthracene
CT,NY,NC,ME,NH,VADibenzofuran
CT,NY,NC,ME,NH,VADi-n-butylphthalate
CT,NY,NC,ME,NH,VA1,2-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,3-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,4-Dichlorobenzene
CT,NY,NC,ME,NH,VA3,3-Dichlorobenzidine
CT,NY,NC,ME,NH,VA2,4-Dichlorophenol
CT,NY,NC,ME,NH,VADiethylphthalate
CT,NY,NC,ME,NH,VA2,4-Dimethylphenol
CT,NY,NC,ME,NH,VADimethylphthalate
CT,NY,NC,ME,NH,VA4,6-Dinitro-2-methylphenol
CT,NY,NC,ME,NH,VA2,4-Dinitrophenol
CT,NY,NC,ME,NH,VA2,4-Dinitrotoluene
CT,NY,NC,ME,NH,VA2,6-Dinitrotoluene
CT,NY,NC,ME,NH,VADi-n-octylphthalate
NY,NC1,2-Diphenylhydrazine/Azobenzene
CT,NY,NC,ME,NH,VAFluoranthene
NY,NC,ME,NH,VAFluorene
CT,NY,NC,ME,NH,VAHexachlorobenzene
CT,NY,NC,ME,NH,VAHexachlorobutadiene
CT,NY,NC,ME,NH,VAHexachlorocyclopentadiene
CT,NY,NC,ME,NH,VAHexachloroethane
CT,NY,NC,ME,NH,VAIndeno(1,2,3-cd)pyrene
CT,NY,NC,ME,NH,VAIsophorone
NC1-Methylnaphthalene
Page 64 of 68
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SW-846 8270E in Water
CT,NY,NC,ME,NH,VA2-Methylnaphthalene
CT,NY,NC,NH,VA2-Methylphenol
CT,NY,NC,NH,VA3/4-Methylphenol
CT,NY,NC,ME,NH,VANaphthalene
CT,NY,NC,ME,NH,VA2-Nitroaniline
CT,NY,NC,ME,NH,VA3-Nitroaniline
CT,NY,NC,ME,NH,VA4-Nitroaniline
CT,NY,NC,ME,NH,VANitrobenzene
CT,NY,NC,ME,NH,VA2-Nitrophenol
CT,NY,NC,ME,NH,VA4-Nitrophenol
CT,NY,NC,ME,NH,VAN-Nitrosodimethylamine
CT,NY,NC,ME,NH,VAN-Nitrosodi-n-propylamine
NCPentachloronitrobenzene
CT,NY,NC,ME,NH,VAPentachlorophenol
CT,NY,NC,ME,NH,VAPhenanthrene
CT,NY,NC,ME,NH,VAPhenol
CT,NY,NC,ME,NH,VAPyrene
CT,NY,NC,ME,NH,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NC,ME,NH,VA1,2,4-Trichlorobenzene
CT,NY,NC,ME,NH,VA2,4,5-Trichlorophenol
CT,NY,NC,ME,NH,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
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