RA-493_1943_CA_MRP_20101022_ CES GWM

TABLES
TABLE 1WATER SUPPLY WELL INFORMATIONWISE CONVENIENT MARTWISE, WARREN COUNTYINCIDENT NO. 1943Well ID Parcel ID Property Owner(s) Property Address Owner AddressEstimated Distance and Direction from SourceUsage2021 US Highway 1 N. PO Box 714Norlina, NC 27563Norlina, NC 275632021 US Highway 1 N. PO Box 714Norlina, NC 27563Norlina, NC 275632041 US Highway 1 N. 2041 US Highway 1 N.Norlina, NC 27563Norlina, NC 275632041 US Highway 1 N. 2041 US Highway 1 N.Norlina, NC 27563Norlina, NC 275632049 US Highway 1 N. PO Box 255Norlina, NC 27563Norlina, NC 275632061US Highway 1 N. PO Box 255Norlina, NC 27563Norlina, NC 27563US Highway 1 N. PO Box 255Norlina, NC 27563Norlina, NC 275632007 US Highway 1 N. PO Box 153Norlina, NC 27563 Wise, NC 275941989 US Highway 1 N. 1989 US Highway 1 N.Norlina, NC 27563Norlina, NC 275631971 US Highway 1 N. 807 Rooker Dairy Rd.Norlina, NC 27563Norlina, NC 275632002 US Highway 1 N. 807 Rooker Dairy Rd.Norlina, NC 27563Norlina, NC 275632004 US Highway 1 N. 2004 US Highway 1 N.Norlina, NC 27563Norlina, NC 275631)2)3)WSW-11 2040135011 Judith Sammond 418' Southeast Sole Source, Potable SupplyWSW-10 2040125855 Ashley & Stuart White 441' Southeast Sole Source, Potable SupplyWSW-9 2040124079 Ashley & Stuart White 934' South Sole Source, Potable SupplyWSW-7 2040122925 Joe & Mary Anne Hunt 238' South Sole Source, Potable SupplyWSW-8 2040123522 Annie Morris 591' South Sole Source, Potable SupplySole Source, Potable SupplyWSW-6 2040038915 Willie Felts, Jr. 862' North-Northwest Sole Source, Potable SupplySole Source, Potable SupplyWillie Felts, Jr. 758' North-Northwest Out of ServiceWSW-2 2040131168Donald Paynter, Edward Paynter91' West Out of service, disconnectedWSW-3 2040030515 Walter & Joanne Paynter 432' NorthwestOut of service due to burned pump. Well for irrigation only.WSW-5 2030945267WSW-5AWSW-1 2040131168 Donald Paynter 431' Southwest2040042185 Willie Felts, Jr.1,218' North-NorthwestWSW-4 2040030515 Walter & Joanne Paynter 726' Northwest Sole Source, Potable SupplyNotes:Supply well information adapted from Table 3, Water Supply Wells Information, Comprehensive Site Assessment, Terraquest Environmental Consultants, PC, November 11, 2009.    Current Parcel identifications, property owners and addressing from the Warren County, NC GIS/Mapping System, October 15, 2012. No property address is associated with the parcel on which WSW‐6 is located.  
TABLE 2MONITORING WELL CONSTRUCTION INFORMATIONWISE CONVENIENT MARTWISE, WARREN COUNTYINCIDENT NO. 1943Well ID Install DateWell Casing Depth (ft, bgs)Screened Interval (bgs)Total Depth (ft) TOC (ft)Date MeasuredDTW (ft)Relative GW Elevation (feet)3/8/2006 17.79 79.679/18/2007 20.43 77.038/26/2009 21.52 75.949/25/2012 19.42 78.043/8/2006 20.39 78.419/18/2007 22.18 76.628/26/2009 22.50 76.309/25/2012 21.26 77.543/8/2006 17.74 79.089/18/2007 19.47 77.358/26/2009 19.61 77.219/25/2012 18.43 78.393/18/1969 18.49 78.519/18/2007 NM ---8/26/2009 20.62 76.389/25/2012 19.37 77.633/8/2006 21.80 78.189/18/2007 23.58 76.408/26/2009 23.82 76.169/25/2012 22.71 77.279/18/2007 22.19 74.778/26/2009 22.39 74.579/25/2012 21.48 75.488/26/2009 21.02 66.659/25/2012 19.94 67.738/26/2009 20.81 ---9/25/2012 NM ---1) 2) 5) MW-1MW-297.4698.8011/18/2005 10-2510 25.0311/18/2005 10 10-25 24.99MW-5 3/6/2006 10 10-3060.009/7/2007 10 10-25 25.03 96.96NA Denotes "Not Available"NM Denotes "Not Measured25.44 87.67MW-7 8/26/2009 10 10-25NM4) DTW Denotes "depth to water" as measured from toc.3) bgs Denotes "beneath ground surface"6) toc Denotes "top of casing"Well construction inforation and data pre-dating September 25, 2012 from Table 5, Monitoring Well Construction Information, Comprehensive Site Assessment, Terraquest Environmental Consultants, PC, November 11, 2009. Total well depths for all wells excepting DW-1 from actual field measurements.MW-3 3/6/2006 10 10-25 24.71 96.82MW-4 3/6/2006 10 10-25 24.77 97.0029.51 99.98MW-6DW-1 6/12/2009 55 55-60NOTES:
TABLE 3SUMMARY OF GROUNDWATER SAMPLING  ANALYTICAL RESULTSWISE CONVENIENT MARTWISE, WARREN COUNTYINCIDENT NO. 1943EPA-3030CBenzeneTolueneEthylbenzeneXylenes (Total)IPEMTBEn-Butylbenzenetert-ButylbenzeneIsopropylbenzenep-IsopropyltolueneNaphthaleneChloromethaneChloroethane1,2-Dichloropropeane1,3-Dichloropropanen-Propylbenzene1,2-Dichloroethane1,2-Dibromoethane (EDB)1,1,2-Trichloroethane1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC9-C18 AliphaticsC9-C22 AromaticsTotal Lead11/22/20054100 17000 2100 11800NA ND NA NA NA NA560NA NA NA NA NA NA NA NA NA NA30000 8100 32000 3259/18/20073500 16000 2000 1060032 ND 52220 89NA ND NA ND ND ND210ND200NA1600 440 210032022001288/26/20099/25/20121100 13600 2090 12310ND ND 56.9120ND589ND ND ND ND254 2200 618NA NA NA NA11/22/20051.711 3.4 18.7 NA ND NA NA NA NA ND NA NA NA NA NA NA NA NA NA NA130039 ND3699/18/2007180.72 1.5 8195ND ND ND ND NA ND NA ND ND ND ND ND ND NA 12 4.8 ND 35 1301378/26/2009826.6 10 2821400.79 ND ND 3.5 ND18ND ND ND ND 1.1 3.11.5ND 63 19 NA NA NA NA9/25/201282.3 714183646 82.21.1 ND ND 6.9 ND49.4ND ND ND ND 14.5 20.71113 36.4 NA NA NA NA3/8/2006 ND ND ND ND NA ND ND ND NA NA ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA9/18/2007 ND ND ND ND ND ND ND ND ND NA ND NA ND ND ND ND ND ND NA NA NA ND ND ND3368/26/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA9/25/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA3/8/2006 ND ND ND ND ND ND NA NA NA NA ND NA NA NA NA NA NA NA NA NA NA NA NA NA3699/25/2007 ND ND ND ND ND ND ND ND ND NA ND NA ND ND ND ND ND ND NA ND ND ND ND ND4928/26/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA9/25/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA3/8/2006470500 79870NA78NA NA NA NA ND NA NA NA NA NA NA NA NA NA NA NA NA NA13109/18/20071502.7 2.3 153110 35ND ND 1.8 NA ND NA ND ND ND ND 2523NA 26 7.7 510 66 2501178/26/200952066 51 490210 310.72 ND 4.8 ND19ND ND ND ND 4.3 4014ND 78 26 NA NA NA NA9/25/20121770 15303742749 427 38.4ND ND 21.2 ND173ND ND ND ND 32.6 51.6 ND ND473145 NA NA NA NA9/18/2007 ND ND ND ND 0.77 ND ND ND ND NA ND NA 0.6438 2.2ND 49 ND NA ND ND ND ND ND NA8/26/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA9/25/2012 ND ND ND ND 12.1 2.7 ND ND ND ND ND ND ND ND ND ND 1.6 ND ND ND ND NA NA NA NA8/26/2009 ND ND ND ND 9.2 ND ND ND ND ND ND ND ND ND ND ND 0.75 ND ND ND ND NA NA NA 0.169/25/2012 ND ND ND ND 6.1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA8/26/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA9/25/20121 600 600 500 70 20 70 70 70 210 6 NE NE 0.51 0.38 70 NE 0.4 0.6 400 400 400 700 200 155,000 260,000 84,500 85,500 70,000 20,000 6,900 15,000 25,000 NE 6,000 NE NE 510 380 30,000 NE 400 NE 28,500 25,000 NE NE NE 15,000ND = Not Detected NA = NE= MADEP‐VPH/EPHSM6200BMW-115A NCAC 2L .0202 (2L) StandardGross Contamination Level (GCL)Sample DateWell I.D.MW-2MW-3MW-4Not Sampled - Free ProductNot AnalyzedNot AnalyzedBold - Exceeds compound's 2L StandardNo 2L Standard established for compoundMW-5MW-6MW-7DW-1

APPENDICES

APPENDIX A

Figure 1 - Site Location Map
Terraquest Figure 2 – Site Vicinity Map (Comprehensive Site Assessment, November 11, 2009)
Terraquest Figure 3 – Site Layout Map (Comprehensive Site Assessment, November 11, 2009)

REV
0
Site Location MapWise Convenient Mart2021 US Highway 1 North
Wise, Warren County, North Carolina
Figure Title
DRAWING NUMBER
CK.:
APP'D.: DPK
SCALE: AS SHOWN
CES PROJ. NO.: 16.308
515 S. NewHope Rd., Suite 104Raleigh, NC 27610
919-235-3335 (office)919-235-3345 (fax)
DR.: KBB
GWMSeptember 2012
10/16/2012
INCIDENT # 1934
Reference: Terrain Navigator Pro, Ver. 9.1; USGS Topographic Map, 7.5 Minute Series, Bracey NC, 1968, Revised 1979. Contour Interval = 10 feet..
SITE
Figure 1

APPENDIX B

Laboratory Certificate of Analysis
and Chain-of-Custody Documentation

October 04, 2012
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 92132770
92132770
Project:
Pace Project No.:
RE:
Ms. Linda Blalock
NCDENR - UST Section
1637 Mail Service Center
Raleigh, NC 276991637
Inc.#1943 Wise Conv. Mart
Dear Ms. Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on September 25, 2012.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Charles Hardin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE SUMMARY
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Lab ID Sample ID Matrix Date Collected Date Received
92132770001 MW-1 Water 09/25/12 12:00 09/25/12 15:50
92132770002 MW-2 Water 09/25/12 12:05 09/25/12 15:50
92132770003 MW-3 Water 09/25/12 12:10 09/25/12 15:50
92132770004 MW-4 Water 09/25/12 12:15 09/25/12 15:50
92132770005 MW-5 Water 09/25/12 12:20 09/25/12 15:50
92132770006 MW-6 Water 09/25/12 12:25 09/25/12 15:50
92132770007 MW-7 Water 09/25/12 12:30 09/25/12 15:50
92132770008 WSW-1 Water 09/25/12 13:30 09/25/12 15:50
92132770009 WSW-4 Water 09/25/12 13:50 09/25/12 15:50
92132770010 WSW-5 Water 09/25/12 14:15 09/25/12 15:50
92132770011 WSW-5A Water 09/25/12 14:45 09/25/12 15:50
92132770012 WSW-6 Water 09/25/12 15:15 09/25/12 15:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92132770001 MW-1 SM 6200B 64 PASI-CMCK
92132770002 MW-2 SM 6200B 64 PASI-CMCK
92132770003 MW-3 SM 6200B 64 PASI-CMCK
92132770004 MW-4 SM 6200B 64 PASI-CMCK
92132770005 MW-5 SM 6200B 64 PASI-CMCK
92132770006 MW-6 SM 6200B 64 PASI-CMCK
92132770007 MW-7 SM 6200B 64 PASI-CMCK
92132770008 WSW-1 SM 6200B 64 PASI-CMCK
92132770009 WSW-4 SM 6200B 64 PASI-CMCK
92132770010 WSW-5 SM 6200B 64 PASI-CMCK
92132770011 WSW-5A SM 6200B 64 PASI-CMCK
92132770012 WSW-6 SM 6200B 64 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
HITS ONLY
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92132770001 MW-1
Benzene 1100 ug/L 09/27/12 04:2250.0SM 6200B
n-Butylbenzene 56.9 ug/L 09/27/12 04:2250.0SM 6200B
Ethylbenzene 2090 ug/L 09/27/12 04:2250.0SM 6200B
Isopropylbenzene (Cumene)120 ug/L 09/27/12 04:2250.0SM 6200B
Naphthalene 689 ug/L 09/27/12 04:22200SM 6200B
n-Propylbenzene 254 ug/L 09/27/12 04:2250.0SM 6200B
Toluene 13600 ug/L 09/27/12 04:2250.0SM 6200B
1,2,4-Trimethylbenzene 2200 ug/L 09/27/12 04:2250.0SM 6200B
1,3,5-Trimethylbenzene 618 ug/L 09/27/12 04:2250.0SM 6200B
m&p-Xylene 8290 ug/L 09/27/12 04:22100SM 6200B
o-Xylene 4020 ug/L 09/27/12 04:2250.0SM 6200B
92132770002 MW-2
Benzene 82.3 ug/L 09/27/12 04:410.50SM 6200B
1,2-Dibromoethane (EDB)0.71 ug/L 09/27/12 04:410.50SM 6200B
1,2-Dichloroethane 2.0 ug/L 09/27/12 04:410.50SM 6200B
Diisopropyl ether 82.2 ug/L 09/27/12 04:410.50SM 6200B
Ethylbenzene 183 ug/L 09/27/12 04:410.50SM 6200B
Isopropylbenzene (Cumene)6.9 ug/L 09/27/12 04:410.50SM 6200B
Methyl-tert-butyl ether 1.1 ug/L 09/27/12 04:410.50SM 6200B
Naphthalene 49.4 ug/L 09/27/12 04:412.0SM 6200B
n-Propylbenzene 14.5 ug/L 09/27/12 04:410.50SM 6200B
Toluene 714 ug/L 09/27/12 10:375.0SM 6200B
1,2,4-Trimethylbenzene 113 ug/L 09/27/12 04:410.50SM 6200B
1,3,5-Trimethylbenzene 36.4 ug/L 09/27/12 04:410.50SM 6200B
m&p-Xylene 397 ug/L 09/27/12 04:411.0SM 6200B
o-Xylene 249 ug/L 09/27/12 10:375.0SM 6200B
92132770005 MW-5
Benzene 1770 ug/L 09/27/12 18:545.0SM 6200B
1,2-Dichloroethane 51.6 ug/L 09/27/12 18:545.0SM 6200B
Diisopropyl ether 427 ug/L 09/27/12 18:545.0SM 6200B
Ethylbenzene 374 ug/L 09/27/12 18:545.0SM 6200B
Isopropylbenzene (Cumene)21.2 ug/L 09/27/12 18:545.0SM 6200B
Methyl-tert-butyl ether 38.4 ug/L 09/27/12 18:545.0SM 6200B
Naphthalene 173 ug/L 09/27/12 18:5420.0SM 6200B
n-Propylbenzene 32.6 ug/L 09/27/12 18:545.0SM 6200B
Toluene 1530 ug/L 09/27/12 18:545.0SM 6200B
1,2,4-Trimethylbenzene 473 ug/L 09/27/12 18:545.0SM 6200B
1,3,5-Trimethylbenzene 145 ug/L 09/27/12 18:545.0SM 6200B
m&p-Xylene 1940 ug/L 09/27/12 18:5410.0SM 6200B
o-Xylene 809 ug/L 09/27/12 18:545.0SM 6200B
92132770006 MW-6
1,2-Dichloroethane 1.6 ug/L 09/27/12 05:370.50SM 6200B
Diisopropyl ether 12.1 ug/L 09/27/12 05:370.50SM 6200B
Methyl-tert-butyl ether 2.7 ug/L 09/27/12 05:370.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
HITS ONLY
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92132770007 MW-7
Diisopropyl ether 6.1 ug/L 09/27/12 19:120.50SM 6200B
92132770008 WSW-1
Methyl-tert-butyl ether 0.92 ug/L 09/27/12 19:300.50SM 6200B
92132770009 WSW-4
1,2-Dichloroethane 1.3 ug/L 09/27/12 19:490.50SM 6200B
92132770010 WSW-5
1,2-Dichloroethane 1.7 ug/L 09/27/12 20:070.50SM 6200B
Diisopropyl ether 5.8 ug/L 09/27/12 20:070.50SM 6200B
92132770011 WSW-5A
1,2-Dichloroethane 1.6 ug/L 09/27/12 20:250.50SM 6200B
Diisopropyl ether 5.6 ug/L 09/27/12 20:250.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-1 Lab ID:92132770001 Collected:09/25/12 12:00 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene 1100 ug/L 100 09/27/12 04:22 71-43-250.0 50.0
Bromobenzene ND ug/L 100 09/27/12 04:22 108-86-150.0 50.0
Bromochloromethane ND ug/L 100 09/27/12 04:22 74-97-550.0 50.0
Bromodichloromethane ND ug/L 100 09/27/12 04:22 75-27-450.0 50.0
Bromoform ND ug/L 100 09/27/12 04:22 75-25-250.0 50.0
Bromomethane ND ug/L 100 09/27/12 04:22 74-83-9500100
n-Butylbenzene 56.9 ug/L 100 09/27/12 04:22 104-51-850.0 50.0
sec-Butylbenzene ND ug/L 100 09/27/12 04:22 135-98-850.0 50.0
tert-Butylbenzene ND ug/L 100 09/27/12 04:22 98-06-650.0 50.0
Carbon tetrachloride ND ug/L 100 09/27/12 04:22 56-23-550.0 50.0
Chlorobenzene ND ug/L 100 09/27/12 04:22 108-90-750.0 50.0
Chloroethane ND ug/L 100 09/27/12 04:22 75-00-3100100
Chloroform ND ug/L 100 09/27/12 04:22 67-66-350.0 50.0
Chloromethane ND ug/L 100 09/27/12 04:22 74-87-3100100
2-Chlorotoluene ND ug/L 100 09/27/12 04:22 95-49-850.0 50.0
4-Chlorotoluene ND ug/L 100 09/27/12 04:22 106-43-450.0 50.0
1,2-Dibromo-3-chloropropane ND ug/L 100 09/27/12 04:22 96-12-8100100
Dibromochloromethane ND ug/L 100 09/27/12 04:22 124-48-150.0 50.0
1,2-Dibromoethane (EDB)ND ug/L 100 09/27/12 04:22 106-93-450.0 50.0
Dibromomethane ND ug/L 100 09/27/12 04:22 74-95-350.0 50.0
1,2-Dichlorobenzene ND ug/L 100 09/27/12 04:22 95-50-150.0 50.0
1,3-Dichlorobenzene ND ug/L 100 09/27/12 04:22 541-73-150.0 50.0
1,4-Dichlorobenzene ND ug/L 100 09/27/12 04:22 106-46-750.0 50.0
Dichlorodifluoromethane ND ug/L 100 09/27/12 04:22 75-71-850.0 50.0
1,1-Dichloroethane ND ug/L 100 09/27/12 04:22 75-34-350.0 50.0
1,2-Dichloroethane ND ug/L 100 09/27/12 04:22 107-06-250.0 50.0
1,1-Dichloroethene ND ug/L 100 09/27/12 04:22 75-35-450.0 50.0
cis-1,2-Dichloroethene ND ug/L 100 09/27/12 04:22 156-59-250.0 50.0
trans-1,2-Dichloroethene ND ug/L 100 09/27/12 04:22 156-60-550.0 50.0
1,2-Dichloropropane ND ug/L 100 09/27/12 04:22 78-87-550.0 50.0
1,3-Dichloropropane ND ug/L 100 09/27/12 04:22 142-28-950.0 50.0
2,2-Dichloropropane ND ug/L 100 09/27/12 04:22 594-20-750.0 50.0
1,1-Dichloropropene ND ug/L 100 09/27/12 04:22 563-58-650.0 50.0
cis-1,3-Dichloropropene ND ug/L 100 09/27/12 04:22 10061-01-550.0 50.0
trans-1,3-Dichloropropene ND ug/L 100 09/27/12 04:22 10061-02-650.0 50.0
Diisopropyl ether ND ug/L 100 09/27/12 04:22 108-20-350.0 50.0
Ethylbenzene 2090 ug/L 100 09/27/12 04:22 100-41-450.0 50.0
Hexachloro-1,3-butadiene ND ug/L 100 09/27/12 04:22 87-68-3200200
Isopropylbenzene (Cumene)120 ug/L 100 09/27/12 04:22 98-82-850.0 50.0
Methylene Chloride ND ug/L 100 09/27/12 04:22 75-09-2200200
Methyl-tert-butyl ether ND ug/L 100 09/27/12 04:22 1634-04-450.0 50.0
Naphthalene 689 ug/L 100 09/27/12 04:22 91-20-3200200
n-Propylbenzene 254 ug/L 100 09/27/12 04:22 103-65-150.0 50.0
Styrene ND ug/L 100 09/27/12 04:22 100-42-550.0 50.0
1,1,1,2-Tetrachloroethane ND ug/L 100 09/27/12 04:22 630-20-650.0 50.0
1,1,2,2-Tetrachloroethane ND ug/L 100 09/27/12 04:22 79-34-550.0 50.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 7 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-1 Lab ID:92132770001 Collected:09/25/12 12:00 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 100 09/27/12 04:22 127-18-450.0 50.0
Toluene 13600 ug/L 100 09/27/12 04:22 108-88-350.0 50.0
1,2,3-Trichlorobenzene ND ug/L 100 09/27/12 04:22 87-61-6200200
1,2,4-Trichlorobenzene ND ug/L 100 09/27/12 04:22 120-82-1200200
1,1,1-Trichloroethane ND ug/L 100 09/27/12 04:22 71-55-650.0 50.0
1,1,2-Trichloroethane ND ug/L 100 09/27/12 04:22 79-00-550.0 50.0
Trichloroethene ND ug/L 100 09/27/12 04:22 79-01-650.0 50.0
Trichlorofluoromethane ND ug/L 100 09/27/12 04:22 75-69-4100100
1,2,3-Trichloropropane ND ug/L 100 09/27/12 04:22 96-18-450.0 50.0
1,2,4-Trimethylbenzene 2200 ug/L 100 09/27/12 04:22 95-63-650.0 50.0
1,3,5-Trimethylbenzene 618 ug/L 100 09/27/12 04:22 108-67-850.0 50.0
Vinyl chloride ND ug/L 100 09/27/12 04:22 75-01-4100100
m&p-Xylene 8290 ug/L 100 09/27/12 04:22 179601-23-1100100
o-Xylene 4020 ug/L 100 09/27/12 04:22 95-47-650.0 50.0
Surrogates
1,2-Dichloroethane-d4 (S)100 %100 09/27/12 04:22 17060-07-070-130
Dibromofluoromethane (S)99 %100 09/27/12 04:22 1868-53-770-130
4-Bromofluorobenzene (S)100 %100 09/27/12 04:22 460-00-470-130
Toluene-d8 (S)99 %100 09/27/12 04:22 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 8 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-2 Lab ID:92132770002 Collected:09/25/12 12:05 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene 82.3 ug/L 1 09/27/12 04:41 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/27/12 04:41 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/27/12 04:41 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/27/12 04:41 75-27-40.50 0.50
Bromoform ND ug/L 1 09/27/12 04:41 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/27/12 04:41 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/27/12 04:41 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/27/12 04:41 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/27/12 04:41 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/27/12 04:41 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/27/12 04:41 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/27/12 04:41 75-00-31.0 1.0
Chloroform ND ug/L 1 09/27/12 04:41 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/27/12 04:41 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 09/27/12 04:41 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/27/12 04:41 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/27/12 04:41 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/27/12 04:41 124-48-10.50 0.50
1,2-Dibromoethane (EDB)0.71 ug/L 1 09/27/12 04:41 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/27/12 04:41 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/27/12 04:41 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/27/12 04:41 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/27/12 04:41 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/27/12 04:41 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/27/12 04:41 75-34-30.50 0.50
1,2-Dichloroethane 2.0 ug/L 1 09/27/12 04:41 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/27/12 04:41 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/27/12 04:41 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/27/12 04:41 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/27/12 04:41 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/27/12 04:41 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/27/12 04:41 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/27/12 04:41 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/27/12 04:41 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/27/12 04:41 10061-02-60.50 0.50
Diisopropyl ether 82.2 ug/L 1 09/27/12 04:41 108-20-30.50 0.50
Ethylbenzene 183 ug/L 1 09/27/12 04:41 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/27/12 04:41 87-68-32.0 2.0
Isopropylbenzene (Cumene)6.9 ug/L 1 09/27/12 04:41 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/27/12 04:41 75-09-22.0 2.0
Methyl-tert-butyl ether 1.1 ug/L 1 09/27/12 04:41 1634-04-40.50 0.50
Naphthalene 49.4 ug/L 1 09/27/12 04:41 91-20-32.0 2.0
n-Propylbenzene 14.5 ug/L 1 09/27/12 04:41 103-65-10.50 0.50
Styrene ND ug/L 1 09/27/12 04:41 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/27/12 04:41 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/27/12 04:41 79-34-50.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 9 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-2 Lab ID:92132770002 Collected:09/25/12 12:05 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 09/27/12 04:41 127-18-40.50 0.50
Toluene 714 ug/L 10 09/27/12 10:37 108-88-35.0 5.0
1,2,3-Trichlorobenzene ND ug/L 1 09/27/12 04:41 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/27/12 04:41 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/27/12 04:41 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/27/12 04:41 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/27/12 04:41 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/27/12 04:41 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/27/12 04:41 96-18-40.50 0.50
1,2,4-Trimethylbenzene 113 ug/L 1 09/27/12 04:41 95-63-60.50 0.50
1,3,5-Trimethylbenzene 36.4 ug/L 1 09/27/12 04:41 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/27/12 04:41 75-01-41.0 1.0
m&p-Xylene 397 ug/L 1 09/27/12 04:41 179601-23-11.0 1.0
o-Xylene 249 ug/L 10 09/27/12 10:37 95-47-65.0 5.0
Surrogates
1,2-Dichloroethane-d4 (S)99 %1 09/27/12 04:41 17060-07-070-130
Dibromofluoromethane (S)98 %1 09/27/12 04:41 1868-53-770-130
4-Bromofluorobenzene (S)99 %1 09/27/12 04:41 460-00-470-130
Toluene-d8 (S)100 %1 09/27/12 04:41 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 10 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-3 Lab ID:92132770003 Collected:09/25/12 12:10 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/27/12 10:56 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/27/12 10:56 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/27/12 10:56 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/27/12 10:56 75-27-40.50 0.50
Bromoform ND ug/L 1 09/27/12 10:56 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/27/12 10:56 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/27/12 10:56 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/27/12 10:56 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/27/12 10:56 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/27/12 10:56 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/27/12 10:56 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/27/12 10:56 75-00-31.0 1.0
Chloroform ND ug/L 1 09/27/12 10:56 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/27/12 10:56 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 09/27/12 10:56 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/27/12 10:56 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/27/12 10:56 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/27/12 10:56 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/27/12 10:56 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/27/12 10:56 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/27/12 10:56 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/27/12 10:56 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/27/12 10:56 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/27/12 10:56 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/27/12 10:56 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/27/12 10:56 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/27/12 10:56 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/27/12 10:56 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/27/12 10:56 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/27/12 10:56 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/27/12 10:56 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/27/12 10:56 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/27/12 10:56 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/27/12 10:56 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/27/12 10:56 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/27/12 10:56 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/27/12 10:56 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/27/12 10:56 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/27/12 10:56 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/27/12 10:56 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/27/12 10:56 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/27/12 10:56 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/27/12 10:56 103-65-10.50 0.50
Styrene ND ug/L 1 09/27/12 10:56 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/27/12 10:56 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/27/12 10:56 79-34-50.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 11 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-3 Lab ID:92132770003 Collected:09/25/12 12:10 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 09/27/12 10:56 127-18-40.50 0.50
Toluene ND ug/L 1 09/27/12 10:56 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/27/12 10:56 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/27/12 10:56 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/27/12 10:56 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/27/12 10:56 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/27/12 10:56 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/27/12 10:56 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/27/12 10:56 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/27/12 10:56 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/27/12 10:56 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/27/12 10:56 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/27/12 10:56 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/27/12 10:56 95-47-60.50 0.50
Surrogates
1,2-Dichloroethane-d4 (S)102 %1 09/27/12 10:56 17060-07-070-130
Dibromofluoromethane (S)101 %1 09/27/12 10:56 1868-53-770-130
4-Bromofluorobenzene (S)99 %1 09/27/12 10:56 460-00-470-130
Toluene-d8 (S)99 %1 09/27/12 10:56 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 12 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-4 Lab ID:92132770004 Collected:09/25/12 12:15 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/27/12 05:18 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/27/12 05:18 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/27/12 05:18 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/27/12 05:18 75-27-40.50 0.50
Bromoform ND ug/L 1 09/27/12 05:18 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/27/12 05:18 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/27/12 05:18 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/27/12 05:18 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/27/12 05:18 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/27/12 05:18 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/27/12 05:18 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/27/12 05:18 75-00-31.0 1.0
Chloroform ND ug/L 1 09/27/12 05:18 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/27/12 05:18 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 09/27/12 05:18 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/27/12 05:18 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/27/12 05:18 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/27/12 05:18 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/27/12 05:18 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/27/12 05:18 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/27/12 05:18 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/27/12 05:18 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/27/12 05:18 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/27/12 05:18 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/27/12 05:18 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/27/12 05:18 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/27/12 05:18 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/27/12 05:18 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/27/12 05:18 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/27/12 05:18 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/27/12 05:18 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/27/12 05:18 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/27/12 05:18 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/27/12 05:18 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/27/12 05:18 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/27/12 05:18 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/27/12 05:18 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/27/12 05:18 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/27/12 05:18 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/27/12 05:18 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/27/12 05:18 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/27/12 05:18 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/27/12 05:18 103-65-10.50 0.50
Styrene ND ug/L 1 09/27/12 05:18 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/27/12 05:18 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/27/12 05:18 79-34-50.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 13 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-4 Lab ID:92132770004 Collected:09/25/12 12:15 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 09/27/12 05:18 127-18-40.50 0.50
Toluene ND ug/L 1 09/27/12 05:18 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/27/12 05:18 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/27/12 05:18 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/27/12 05:18 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/27/12 05:18 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/27/12 05:18 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/27/12 05:18 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/27/12 05:18 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/27/12 05:18 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/27/12 05:18 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/27/12 05:18 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/27/12 05:18 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/27/12 05:18 95-47-60.50 0.50
Surrogates
1,2-Dichloroethane-d4 (S)101 %1 09/27/12 05:18 17060-07-070-130
Dibromofluoromethane (S)99 %1 09/27/12 05:18 1868-53-770-130
4-Bromofluorobenzene (S)98 %1 09/27/12 05:18 460-00-470-130
Toluene-d8 (S)99 %1 09/27/12 05:18 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 14 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-5 Lab ID:92132770005 Collected:09/25/12 12:20 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene 1770 ug/L 10 09/27/12 18:54 71-43-25.0 5.0
Bromobenzene ND ug/L 10 09/27/12 18:54 108-86-15.0 5.0
Bromochloromethane ND ug/L 10 09/27/12 18:54 74-97-55.0 5.0
Bromodichloromethane ND ug/L 10 09/27/12 18:54 75-27-45.0 5.0
Bromoform ND ug/L 10 09/27/12 18:54 75-25-25.0 5.0
Bromomethane ND ug/L 10 09/27/12 18:54 74-83-950.0 10.0
n-Butylbenzene ND ug/L 10 09/27/12 18:54 104-51-85.0 5.0
sec-Butylbenzene ND ug/L 10 09/27/12 18:54 135-98-85.0 5.0
tert-Butylbenzene ND ug/L 10 09/27/12 18:54 98-06-65.0 5.0
Carbon tetrachloride ND ug/L 10 09/27/12 18:54 56-23-55.0 5.0
Chlorobenzene ND ug/L 10 09/27/12 18:54 108-90-75.0 5.0
Chloroethane ND ug/L 10 09/27/12 18:54 75-00-310.0 10.0
Chloroform ND ug/L 10 09/27/12 18:54 67-66-35.0 5.0
Chloromethane ND ug/L 10 09/27/12 18:54 74-87-310.0 10.0
2-Chlorotoluene ND ug/L 10 09/27/12 18:54 95-49-85.0 5.0
4-Chlorotoluene ND ug/L 10 09/27/12 18:54 106-43-45.0 5.0
1,2-Dibromo-3-chloropropane ND ug/L 10 09/27/12 18:54 96-12-810.0 10.0
Dibromochloromethane ND ug/L 10 09/27/12 18:54 124-48-15.0 5.0
1,2-Dibromoethane (EDB)ND ug/L 10 09/27/12 18:54 106-93-45.0 5.0
Dibromomethane ND ug/L 10 09/27/12 18:54 74-95-35.0 5.0
1,2-Dichlorobenzene ND ug/L 10 09/27/12 18:54 95-50-15.0 5.0
1,3-Dichlorobenzene ND ug/L 10 09/27/12 18:54 541-73-15.0 5.0
1,4-Dichlorobenzene ND ug/L 10 09/27/12 18:54 106-46-75.0 5.0
Dichlorodifluoromethane ND ug/L 10 09/27/12 18:54 75-71-85.0 5.0
1,1-Dichloroethane ND ug/L 10 09/27/12 18:54 75-34-35.0 5.0
1,2-Dichloroethane 51.6 ug/L 10 09/27/12 18:54 107-06-25.0 5.0
1,1-Dichloroethene ND ug/L 10 09/27/12 18:54 75-35-45.0 5.0
cis-1,2-Dichloroethene ND ug/L 10 09/27/12 18:54 156-59-25.0 5.0
trans-1,2-Dichloroethene ND ug/L 10 09/27/12 18:54 156-60-55.0 5.0
1,2-Dichloropropane ND ug/L 10 09/27/12 18:54 78-87-55.0 5.0
1,3-Dichloropropane ND ug/L 10 09/27/12 18:54 142-28-95.0 5.0
2,2-Dichloropropane ND ug/L 10 09/27/12 18:54 594-20-75.0 5.0
1,1-Dichloropropene ND ug/L 10 09/27/12 18:54 563-58-65.0 5.0
cis-1,3-Dichloropropene ND ug/L 10 09/27/12 18:54 10061-01-55.0 5.0
trans-1,3-Dichloropropene ND ug/L 10 09/27/12 18:54 10061-02-65.0 5.0
Diisopropyl ether 427 ug/L 10 09/27/12 18:54 108-20-35.0 5.0
Ethylbenzene 374 ug/L 10 09/27/12 18:54 100-41-45.0 5.0
Hexachloro-1,3-butadiene ND ug/L 10 09/27/12 18:54 87-68-320.0 20.0
Isopropylbenzene (Cumene)21.2 ug/L 10 09/27/12 18:54 98-82-85.0 5.0
Methylene Chloride ND ug/L 10 09/27/12 18:54 75-09-220.0 20.0
Methyl-tert-butyl ether 38.4 ug/L 10 09/27/12 18:54 1634-04-45.0 5.0
Naphthalene 173 ug/L 10 09/27/12 18:54 91-20-320.0 20.0
n-Propylbenzene 32.6 ug/L 10 09/27/12 18:54 103-65-15.0 5.0
Styrene ND ug/L 10 09/27/12 18:54 100-42-55.0 5.0
1,1,1,2-Tetrachloroethane ND ug/L 10 09/27/12 18:54 630-20-65.0 5.0
1,1,2,2-Tetrachloroethane ND ug/L 10 09/27/12 18:54 79-34-55.0 5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 15 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-5 Lab ID:92132770005 Collected:09/25/12 12:20 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 10 09/27/12 18:54 127-18-45.0 5.0
Toluene 1530 ug/L 10 09/27/12 18:54 108-88-35.0 5.0
1,2,3-Trichlorobenzene ND ug/L 10 09/27/12 18:54 87-61-620.0 20.0
1,2,4-Trichlorobenzene ND ug/L 10 09/27/12 18:54 120-82-120.0 20.0
1,1,1-Trichloroethane ND ug/L 10 09/27/12 18:54 71-55-65.0 5.0
1,1,2-Trichloroethane ND ug/L 10 09/27/12 18:54 79-00-55.0 5.0
Trichloroethene ND ug/L 10 09/27/12 18:54 79-01-65.0 5.0
Trichlorofluoromethane ND ug/L 10 09/27/12 18:54 75-69-410.0 10.0
1,2,3-Trichloropropane ND ug/L 10 09/27/12 18:54 96-18-45.0 5.0
1,2,4-Trimethylbenzene 473 ug/L 10 09/27/12 18:54 95-63-65.0 5.0
1,3,5-Trimethylbenzene 145 ug/L 10 09/27/12 18:54 108-67-85.0 5.0
Vinyl chloride ND ug/L 10 09/27/12 18:54 75-01-410.0 10.0
m&p-Xylene 1940 ug/L 10 09/27/12 18:54 179601-23-110.0 10.0
o-Xylene 809 ug/L 10 09/27/12 18:54 95-47-65.0 5.0
Surrogates
1,2-Dichloroethane-d4 (S)109 %10 09/27/12 18:54 17060-07-070-130
Dibromofluoromethane (S)100 %10 09/27/12 18:54 1868-53-770-130
4-Bromofluorobenzene (S)86 %10 09/27/12 18:54 460-00-470-130
Toluene-d8 (S)96 %10 09/27/12 18:54 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 16 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-6 Lab ID:92132770006 Collected:09/25/12 12:25 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/27/12 05:37 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/27/12 05:37 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/27/12 05:37 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/27/12 05:37 75-27-40.50 0.50
Bromoform ND ug/L 1 09/27/12 05:37 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/27/12 05:37 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/27/12 05:37 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/27/12 05:37 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/27/12 05:37 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/27/12 05:37 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/27/12 05:37 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/27/12 05:37 75-00-31.0 1.0
Chloroform ND ug/L 1 09/27/12 05:37 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/27/12 05:37 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 09/27/12 05:37 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/27/12 05:37 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/27/12 05:37 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/27/12 05:37 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/27/12 05:37 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/27/12 05:37 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/27/12 05:37 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/27/12 05:37 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/27/12 05:37 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/27/12 05:37 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/27/12 05:37 75-34-30.50 0.50
1,2-Dichloroethane 1.6 ug/L 1 09/27/12 05:37 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/27/12 05:37 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/27/12 05:37 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/27/12 05:37 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/27/12 05:37 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/27/12 05:37 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/27/12 05:37 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/27/12 05:37 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/27/12 05:37 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/27/12 05:37 10061-02-60.50 0.50
Diisopropyl ether 12.1 ug/L 1 09/27/12 05:37 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/27/12 05:37 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/27/12 05:37 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/27/12 05:37 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/27/12 05:37 75-09-22.0 2.0
Methyl-tert-butyl ether 2.7 ug/L 1 09/27/12 05:37 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/27/12 05:37 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/27/12 05:37 103-65-10.50 0.50
Styrene ND ug/L 1 09/27/12 05:37 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/27/12 05:37 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/27/12 05:37 79-34-50.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 17 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-6 Lab ID:92132770006 Collected:09/25/12 12:25 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 09/27/12 05:37 127-18-40.50 0.50
Toluene ND ug/L 1 09/27/12 05:37 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/27/12 05:37 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/27/12 05:37 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/27/12 05:37 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/27/12 05:37 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/27/12 05:37 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/27/12 05:37 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/27/12 05:37 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/27/12 05:37 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/27/12 05:37 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/27/12 05:37 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/27/12 05:37 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/27/12 05:37 95-47-60.50 0.50
Surrogates
1,2-Dichloroethane-d4 (S)102 %1 09/27/12 05:37 17060-07-070-130
Dibromofluoromethane (S)100 %1 09/27/12 05:37 1868-53-770-130
4-Bromofluorobenzene (S)98 %1 09/27/12 05:37 460-00-470-130
Toluene-d8 (S)99 %1 09/27/12 05:37 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 18 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-7 Lab ID:92132770007 Collected:09/25/12 12:30 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/27/12 19:12 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/27/12 19:12 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/27/12 19:12 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/27/12 19:12 75-27-40.50 0.50
Bromoform ND ug/L 1 09/27/12 19:12 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/27/12 19:12 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/27/12 19:12 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/27/12 19:12 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/27/12 19:12 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/27/12 19:12 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/27/12 19:12 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/27/12 19:12 75-00-31.0 1.0
Chloroform ND ug/L 1 09/27/12 19:12 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/27/12 19:12 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 09/27/12 19:12 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/27/12 19:12 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/27/12 19:12 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/27/12 19:12 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/27/12 19:12 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/27/12 19:12 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/27/12 19:12 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/27/12 19:12 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/27/12 19:12 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/27/12 19:12 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/27/12 19:12 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/27/12 19:12 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/27/12 19:12 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/27/12 19:12 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/27/12 19:12 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/27/12 19:12 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/27/12 19:12 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/27/12 19:12 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/27/12 19:12 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/27/12 19:12 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/27/12 19:12 10061-02-60.50 0.50
Diisopropyl ether 6.1 ug/L 1 09/27/12 19:12 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/27/12 19:12 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/27/12 19:12 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/27/12 19:12 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/27/12 19:12 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/27/12 19:12 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/27/12 19:12 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/27/12 19:12 103-65-10.50 0.50
Styrene ND ug/L 1 09/27/12 19:12 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/27/12 19:12 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/27/12 19:12 79-34-50.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 19 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:MW-7 Lab ID:92132770007 Collected:09/25/12 12:30 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 09/27/12 19:12 127-18-40.50 0.50
Toluene ND ug/L 1 09/27/12 19:12 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/27/12 19:12 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/27/12 19:12 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/27/12 19:12 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/27/12 19:12 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/27/12 19:12 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/27/12 19:12 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/27/12 19:12 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/27/12 19:12 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/27/12 19:12 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/27/12 19:12 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/27/12 19:12 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/27/12 19:12 95-47-60.50 0.50
Surrogates
1,2-Dichloroethane-d4 (S)115 %1 09/27/12 19:12 17060-07-070-130
Dibromofluoromethane (S)107 %1 09/27/12 19:12 1868-53-770-130
4-Bromofluorobenzene (S)82 %1 09/27/12 19:12 460-00-470-130
Toluene-d8 (S)96 %1 09/27/12 19:12 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 20 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:WSW-1 Lab ID:92132770008 Collected:09/25/12 13:30 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/27/12 19:30 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/27/12 19:30 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/27/12 19:30 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/27/12 19:30 75-27-40.50 0.50
Bromoform ND ug/L 1 09/27/12 19:30 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/27/12 19:30 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/27/12 19:30 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/27/12 19:30 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/27/12 19:30 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/27/12 19:30 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/27/12 19:30 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/27/12 19:30 75-00-31.0 1.0
Chloroform ND ug/L 1 09/27/12 19:30 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/27/12 19:30 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 09/27/12 19:30 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/27/12 19:30 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/27/12 19:30 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/27/12 19:30 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/27/12 19:30 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/27/12 19:30 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/27/12 19:30 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/27/12 19:30 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/27/12 19:30 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/27/12 19:30 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/27/12 19:30 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/27/12 19:30 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/27/12 19:30 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/27/12 19:30 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/27/12 19:30 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/27/12 19:30 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/27/12 19:30 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/27/12 19:30 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/27/12 19:30 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/27/12 19:30 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/27/12 19:30 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/27/12 19:30 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/27/12 19:30 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/27/12 19:30 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/27/12 19:30 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/27/12 19:30 75-09-22.0 2.0
Methyl-tert-butyl ether 0.92 ug/L 1 09/27/12 19:30 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/27/12 19:30 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/27/12 19:30 103-65-10.50 0.50
Styrene ND ug/L 1 09/27/12 19:30 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/27/12 19:30 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/27/12 19:30 79-34-50.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 21 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:WSW-1 Lab ID:92132770008 Collected:09/25/12 13:30 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 09/27/12 19:30 127-18-40.50 0.50
Toluene ND ug/L 1 09/27/12 19:30 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/27/12 19:30 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/27/12 19:30 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/27/12 19:30 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/27/12 19:30 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/27/12 19:30 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/27/12 19:30 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/27/12 19:30 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/27/12 19:30 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/27/12 19:30 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/27/12 19:30 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/27/12 19:30 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/27/12 19:30 95-47-60.50 0.50
Surrogates
1,2-Dichloroethane-d4 (S)116 %1 09/27/12 19:30 17060-07-070-130
Dibromofluoromethane (S)107 %1 09/27/12 19:30 1868-53-770-130
4-Bromofluorobenzene (S)82 %1 09/27/12 19:30 460-00-470-130
Toluene-d8 (S)97 %1 09/27/12 19:30 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 22 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:WSW-4 Lab ID:92132770009 Collected:09/25/12 13:50 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/27/12 19:49 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/27/12 19:49 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/27/12 19:49 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/27/12 19:49 75-27-40.50 0.50
Bromoform ND ug/L 1 09/27/12 19:49 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/27/12 19:49 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/27/12 19:49 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/27/12 19:49 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/27/12 19:49 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/27/12 19:49 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/27/12 19:49 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/27/12 19:49 75-00-31.0 1.0
Chloroform ND ug/L 1 09/27/12 19:49 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/27/12 19:49 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 09/27/12 19:49 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/27/12 19:49 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/27/12 19:49 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/27/12 19:49 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/27/12 19:49 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/27/12 19:49 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/27/12 19:49 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/27/12 19:49 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/27/12 19:49 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/27/12 19:49 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/27/12 19:49 75-34-30.50 0.50
1,2-Dichloroethane 1.3 ug/L 1 09/27/12 19:49 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/27/12 19:49 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/27/12 19:49 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/27/12 19:49 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/27/12 19:49 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/27/12 19:49 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/27/12 19:49 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/27/12 19:49 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/27/12 19:49 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/27/12 19:49 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/27/12 19:49 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/27/12 19:49 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/27/12 19:49 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/27/12 19:49 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/27/12 19:49 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/27/12 19:49 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/27/12 19:49 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/27/12 19:49 103-65-10.50 0.50
Styrene ND ug/L 1 09/27/12 19:49 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/27/12 19:49 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/27/12 19:49 79-34-50.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 23 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:WSW-4 Lab ID:92132770009 Collected:09/25/12 13:50 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 09/27/12 19:49 127-18-40.50 0.50
Toluene ND ug/L 1 09/27/12 19:49 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/27/12 19:49 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/27/12 19:49 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/27/12 19:49 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/27/12 19:49 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/27/12 19:49 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/27/12 19:49 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/27/12 19:49 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/27/12 19:49 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/27/12 19:49 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/27/12 19:49 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/27/12 19:49 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/27/12 19:49 95-47-60.50 0.50
Surrogates
1,2-Dichloroethane-d4 (S)123 %1 09/27/12 19:49 17060-07-070-130
Dibromofluoromethane (S)110 %1 09/27/12 19:49 1868-53-770-130
4-Bromofluorobenzene (S)81 %1 09/27/12 19:49 460-00-470-130
Toluene-d8 (S)98 %1 09/27/12 19:49 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 24 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:WSW-5 Lab ID:92132770010 Collected:09/25/12 14:15 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/27/12 20:07 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/27/12 20:07 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/27/12 20:07 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/27/12 20:07 75-27-40.50 0.50
Bromoform ND ug/L 1 09/27/12 20:07 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/27/12 20:07 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/27/12 20:07 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/27/12 20:07 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/27/12 20:07 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/27/12 20:07 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/27/12 20:07 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/27/12 20:07 75-00-31.0 1.0
Chloroform ND ug/L 1 09/27/12 20:07 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/27/12 20:07 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 09/27/12 20:07 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/27/12 20:07 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/27/12 20:07 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/27/12 20:07 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/27/12 20:07 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/27/12 20:07 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/27/12 20:07 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/27/12 20:07 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/27/12 20:07 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/27/12 20:07 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/27/12 20:07 75-34-30.50 0.50
1,2-Dichloroethane 1.7 ug/L 1 09/27/12 20:07 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/27/12 20:07 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/27/12 20:07 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/27/12 20:07 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/27/12 20:07 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/27/12 20:07 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/27/12 20:07 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/27/12 20:07 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/27/12 20:07 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/27/12 20:07 10061-02-60.50 0.50
Diisopropyl ether 5.8 ug/L 1 09/27/12 20:07 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/27/12 20:07 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/27/12 20:07 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/27/12 20:07 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/27/12 20:07 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/27/12 20:07 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/27/12 20:07 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/27/12 20:07 103-65-10.50 0.50
Styrene ND ug/L 1 09/27/12 20:07 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/27/12 20:07 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/27/12 20:07 79-34-50.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 25 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:WSW-5 Lab ID:92132770010 Collected:09/25/12 14:15 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 09/27/12 20:07 127-18-40.50 0.50
Toluene ND ug/L 1 09/27/12 20:07 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/27/12 20:07 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/27/12 20:07 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/27/12 20:07 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/27/12 20:07 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/27/12 20:07 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/27/12 20:07 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/27/12 20:07 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/27/12 20:07 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/27/12 20:07 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/27/12 20:07 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/27/12 20:07 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/27/12 20:07 95-47-60.50 0.50
Surrogates
1,2-Dichloroethane-d4 (S)123 %1 09/27/12 20:07 17060-07-070-130
Dibromofluoromethane (S)111 %1 09/27/12 20:07 1868-53-770-130
4-Bromofluorobenzene (S)81 %1 09/27/12 20:07 460-00-470-130
Toluene-d8 (S)97 %1 09/27/12 20:07 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 26 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:WSW-5A Lab ID:92132770011 Collected:09/25/12 14:45 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/27/12 20:25 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/27/12 20:25 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/27/12 20:25 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/27/12 20:25 75-27-40.50 0.50
Bromoform ND ug/L 1 09/27/12 20:25 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/27/12 20:25 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/27/12 20:25 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/27/12 20:25 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/27/12 20:25 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/27/12 20:25 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/27/12 20:25 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/27/12 20:25 75-00-31.0 1.0
Chloroform ND ug/L 1 09/27/12 20:25 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/27/12 20:25 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 09/27/12 20:25 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/27/12 20:25 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/27/12 20:25 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/27/12 20:25 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/27/12 20:25 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/27/12 20:25 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/27/12 20:25 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/27/12 20:25 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/27/12 20:25 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/27/12 20:25 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/27/12 20:25 75-34-30.50 0.50
1,2-Dichloroethane 1.6 ug/L 1 09/27/12 20:25 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/27/12 20:25 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/27/12 20:25 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/27/12 20:25 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/27/12 20:25 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/27/12 20:25 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/27/12 20:25 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/27/12 20:25 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/27/12 20:25 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/27/12 20:25 10061-02-60.50 0.50
Diisopropyl ether 5.6 ug/L 1 09/27/12 20:25 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/27/12 20:25 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/27/12 20:25 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/27/12 20:25 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/27/12 20:25 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/27/12 20:25 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/27/12 20:25 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/27/12 20:25 103-65-10.50 0.50
Styrene ND ug/L 1 09/27/12 20:25 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/27/12 20:25 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/27/12 20:25 79-34-50.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 27 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:WSW-5A Lab ID:92132770011 Collected:09/25/12 14:45 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 09/27/12 20:25 127-18-40.50 0.50
Toluene ND ug/L 1 09/27/12 20:25 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/27/12 20:25 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/27/12 20:25 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/27/12 20:25 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/27/12 20:25 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/27/12 20:25 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/27/12 20:25 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/27/12 20:25 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/27/12 20:25 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/27/12 20:25 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/27/12 20:25 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/27/12 20:25 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/27/12 20:25 95-47-60.50 0.50
Surrogates
1,2-Dichloroethane-d4 (S)126 %1 09/27/12 20:25 17060-07-070-130
Dibromofluoromethane (S)111 %1 09/27/12 20:25 1868-53-770-130
4-Bromofluorobenzene (S)81 %1 09/27/12 20:25 460-00-470-130
Toluene-d8 (S)97 %1 09/27/12 20:25 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 28 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:WSW-6 Lab ID:92132770012 Collected:09/25/12 15:15 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/28/12 11:24 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/28/12 11:24 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/28/12 11:24 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/28/12 11:24 75-27-40.50 0.50
Bromoform ND ug/L 1 09/28/12 11:24 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/28/12 11:24 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/28/12 11:24 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/28/12 11:24 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/28/12 11:24 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/28/12 11:24 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/28/12 11:24 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/28/12 11:24 75-00-31.0 1.0
Chloroform ND ug/L 1 09/28/12 11:24 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/28/12 11:24 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 09/28/12 11:24 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/28/12 11:24 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/28/12 11:24 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/28/12 11:24 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/28/12 11:24 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/28/12 11:24 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/28/12 11:24 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/28/12 11:24 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/28/12 11:24 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/28/12 11:24 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/28/12 11:24 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/28/12 11:24 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/28/12 11:24 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/28/12 11:24 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/28/12 11:24 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/28/12 11:24 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/28/12 11:24 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/28/12 11:24 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/28/12 11:24 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/28/12 11:24 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/28/12 11:24 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/28/12 11:24 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/28/12 11:24 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/28/12 11:24 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/28/12 11:24 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/28/12 11:24 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/28/12 11:24 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/28/12 11:24 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/28/12 11:24 103-65-10.50 0.50
Styrene ND ug/L 1 09/28/12 11:24 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/28/12 11:24 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/28/12 11:24 79-34-50.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 29 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Sample:WSW-6 Lab ID:92132770012 Collected:09/25/12 15:15 Received:09/25/12 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 09/28/12 11:24 127-18-40.50 0.50
Toluene ND ug/L 1 09/28/12 11:24 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/28/12 11:24 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/28/12 11:24 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/28/12 11:24 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/28/12 11:24 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/28/12 11:24 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/28/12 11:24 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/28/12 11:24 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/28/12 11:24 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/28/12 11:24 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/28/12 11:24 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/28/12 11:24 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/28/12 11:24 95-47-60.50 0.50
Surrogates
1,2-Dichloroethane-d4 (S)119 %1 09/28/12 11:24 17060-07-070-130
Dibromofluoromethane (S)107 %1 09/28/12 11:24 1868-53-770-130
4-Bromofluorobenzene (S)81 %1 09/28/12 11:24 460-00-470-130
Toluene-d8 (S)96 %1 09/28/12 11:24 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 30 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/20460
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92132770005, 92132770007, 92132770008, 92132770009, 92132770010, 92132770011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:837725
Associated Lab Samples:92132770005, 92132770007, 92132770008, 92132770009, 92132770010, 92132770011
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/27/12 13:42
1,1,1-Trichloroethane ug/L ND 0.50 09/27/12 13:42
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/27/12 13:42
1,1,2-Trichloroethane ug/L ND 0.50 09/27/12 13:42
1,1-Dichloroethane ug/L ND 0.50 09/27/12 13:42
1,1-Dichloroethene ug/L ND 0.50 09/27/12 13:42
1,1-Dichloropropene ug/L ND 0.50 09/27/12 13:42
1,2,3-Trichlorobenzene ug/L ND 2.0 09/27/12 13:42
1,2,3-Trichloropropane ug/L ND 0.50 09/27/12 13:42
1,2,4-Trichlorobenzene ug/L ND 2.0 09/27/12 13:42
1,2,4-Trimethylbenzene ug/L ND 0.50 09/27/12 13:42
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/27/12 13:42
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/27/12 13:42
1,2-Dichlorobenzene ug/L ND 0.50 09/27/12 13:42
1,2-Dichloroethane ug/L ND 0.50 09/27/12 13:42
1,2-Dichloropropane ug/L ND 0.50 09/27/12 13:42
1,3,5-Trimethylbenzene ug/L ND 0.50 09/27/12 13:42
1,3-Dichlorobenzene ug/L ND 0.50 09/27/12 13:42
1,3-Dichloropropane ug/L ND 0.50 09/27/12 13:42
1,4-Dichlorobenzene ug/L ND 0.50 09/27/12 13:42
2,2-Dichloropropane ug/L ND 0.50 09/27/12 13:42
2-Chlorotoluene ug/L ND 0.50 09/27/12 13:42
4-Chlorotoluene ug/L ND 0.50 09/27/12 13:42
Benzene ug/L ND 0.50 09/27/12 13:42
Bromobenzene ug/L ND 0.50 09/27/12 13:42
Bromochloromethane ug/L ND 0.50 09/27/12 13:42
Bromodichloromethane ug/L ND 0.50 09/27/12 13:42
Bromoform ug/L ND 0.50 09/27/12 13:42
Bromomethane ug/L ND 5.0 09/27/12 13:42
Carbon tetrachloride ug/L ND 0.50 09/27/12 13:42
Chlorobenzene ug/L ND 0.50 09/27/12 13:42
Chloroethane ug/L ND 1.0 09/27/12 13:42
Chloroform ug/L ND 0.50 09/27/12 13:42
Chloromethane ug/L ND 1.0 09/27/12 13:42
cis-1,2-Dichloroethene ug/L ND 0.50 09/27/12 13:42
cis-1,3-Dichloropropene ug/L ND 0.50 09/27/12 13:42
Dibromochloromethane ug/L ND 0.50 09/27/12 13:42
Dibromomethane ug/L ND 0.50 09/27/12 13:42
Dichlorodifluoromethane ug/L ND 0.50 09/27/12 13:42
Diisopropyl ether ug/L ND 0.50 09/27/12 13:42
Ethylbenzene ug/L ND 0.50 09/27/12 13:42
Hexachloro-1,3-butadiene ug/L ND 2.0 09/27/12 13:42
Isopropylbenzene (Cumene)ug/L ND 0.50 09/27/12 13:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 31 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:837725
Associated Lab Samples:92132770005, 92132770007, 92132770008, 92132770009, 92132770010, 92132770011
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 09/27/12 13:42
Methyl-tert-butyl ether ug/L ND 0.50 09/27/12 13:42
Methylene Chloride ug/L ND 2.0 09/27/12 13:42
n-Butylbenzene ug/L ND 0.50 09/27/12 13:42
n-Propylbenzene ug/L ND 0.50 09/27/12 13:42
Naphthalene ug/L ND 2.0 09/27/12 13:42
o-Xylene ug/L ND 0.50 09/27/12 13:42
sec-Butylbenzene ug/L ND 0.50 09/27/12 13:42
Styrene ug/L ND 0.50 09/27/12 13:42
tert-Butylbenzene ug/L ND 0.50 09/27/12 13:42
Tetrachloroethene ug/L ND 0.50 09/27/12 13:42
Toluene ug/L ND 0.50 09/27/12 13:42
trans-1,2-Dichloroethene ug/L ND 0.50 09/27/12 13:42
trans-1,3-Dichloropropene ug/L ND 0.50 09/27/12 13:42
Trichloroethene ug/L ND 0.50 09/27/12 13:42
Trichlorofluoromethane ug/L ND 1.0 09/27/12 13:42
Vinyl chloride ug/L ND 1.0 09/27/12 13:42
1,2-Dichloroethane-d4 (S)%114 70-130 09/27/12 13:42
4-Bromofluorobenzene (S)%83 70-130 09/27/12 13:42
Dibromofluoromethane (S)%105 70-130 09/27/12 13:42
Toluene-d8 (S)%96 70-130 09/27/12 13:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
837726LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.650 105 60-140
1,1,1-Trichloroethane ug/L 50.250 100 60-140
1,1,2,2-Tetrachloroethane ug/L 44.450 89 60-140
1,1,2-Trichloroethane ug/L 46.750 93 60-140
1,1-Dichloroethane ug/L 48.650 97 60-140
1,1-Dichloroethene ug/L 48.050 96 60-140
1,1-Dichloropropene ug/L 43.850 88 60-140
1,2,3-Trichlorobenzene ug/L 54.850 110 60-140
1,2,3-Trichloropropane ug/L 46.150 92 60-140
1,2,4-Trichlorobenzene ug/L 53.350 107 60-140
1,2,4-Trimethylbenzene ug/L 53.650 107 60-140
1,2-Dibromo-3-chloropropane ug/L 74.9 CU5015060-140
1,2-Dibromoethane (EDB)ug/L 53.150 106 60-140
1,2-Dichlorobenzene ug/L 52.150 104 60-140
1,2-Dichloroethane ug/L 45.450 91 60-140
1,2-Dichloropropane ug/L 45.450 91 60-140
1,3,5-Trimethylbenzene ug/L 53.050 106 60-140
1,3-Dichlorobenzene ug/L 51.250 102 60-140
1,3-Dichloropropane ug/L 50.650 101 60-140
1,4-Dichlorobenzene ug/L 50.450 101 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 32 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
837726LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 35.950 72 60-140
2-Chlorotoluene ug/L 50.650 101 60-140
4-Chlorotoluene ug/L 50.950 102 60-140
Benzene ug/L 46.150 92 60-140
Bromobenzene ug/L 51.850 104 60-140
Bromochloromethane ug/L 47.150 94 60-140
Bromodichloromethane ug/L 51.350 103 60-140
Bromoform ug/L 51.050 102 60-140
Bromomethane ug/L 32.950 66 60-140
Carbon tetrachloride ug/L 52.950 106 60-140
Chlorobenzene ug/L 49.150 98 60-140
Chloroethane ug/L 38.350 77 60-140
Chloroform ug/L 47.250 94 60-140
Chloromethane ug/L 40.050 80 60-140
cis-1,2-Dichloroethene ug/L 47.650 95 60-140
cis-1,3-Dichloropropene ug/L 48.750 97 60-140
Dibromochloromethane ug/L 60.050 120 60-140
Dibromomethane ug/L 46.650 93 60-140
Dichlorodifluoromethane ug/L 41.150 82 60-140
Diisopropyl ether ug/L 45.950 92 60-140
Ethylbenzene ug/L 49.450 99 60-140
Hexachloro-1,3-butadiene ug/L 50.350 101 60-140
Isopropylbenzene (Cumene)ug/L 48.750 97 60-140
m&p-Xylene ug/L 99.5100 99 60-140
Methyl-tert-butyl ether ug/L 49.850 100 60-140
Methylene Chloride ug/L 41.150 82 60-140
n-Butylbenzene ug/L 52.650 105 60-140
n-Propylbenzene ug/L 52.450 105 60-140
Naphthalene ug/L 58.950 118 60-140
o-Xylene ug/L 48.050 96 60-140
sec-Butylbenzene ug/L 53.550 107 60-140
Styrene ug/L 50.350 101 60-140
tert-Butylbenzene ug/L 53.350 107 60-140
Tetrachloroethene ug/L 50.950 102 60-140
Toluene ug/L 45.250 90 60-140
trans-1,2-Dichloroethene ug/L 45.350 91 60-140
trans-1,3-Dichloropropene ug/L 52.050 104 60-140
Trichloroethene ug/L 47.650 95 60-140
Trichlorofluoromethane ug/L 46.950 94 60-140
Vinyl chloride ug/L 42.550 85 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%89 70-130
Dibromofluoromethane (S)%101 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 33 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
842221MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92132496015
842222
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 117 60-140116 1 3020ND23.5 23.3
1,1,1-Trichloroethane ug/L 20 121 60-140116 4 3020ND24.3 23.2
1,1,2,2-Tetrachloroethane ug/L 20 100 60-14097 2 3020ND20.0 19.5
1,1,2-Trichloroethane ug/L 20 106 60-140105 1 3020ND21.2 21.0
1,1-Dichloroethane ug/L 20 121 60-140116 5 3020ND24.2 23.1
1,1-Dichloroethene ug/L 20 120 60-140114 5 3020ND24.0 22.7
1,1-Dichloropropene ug/L 20 106 60-140100 5 3020ND21.1 20.0
1,2,3-Trichlorobenzene ug/L 20 112 60-140113 1 3020ND22.4 22.6
1,2,3-Trichloropropane ug/L 20 102 60-140102 1 3020ND20.3 20.5
1,2,4-Trichlorobenzene ug/L 20 106 60-140105 1 3020ND21.2 21.1
1,2,4-Trimethylbenzene ug/L 20 120 60-140117 3 3020ND24.0 23.3
1,2-Dibromo-3-chloropropane ug/L M02015960-140156 2 3020ND31.7 31.1
1,2-Dibromoethane (EDB)ug/L 20 116 60-140115 1 3020ND23.2 22.9
1,2-Dichlorobenzene ug/L 20 116 60-140114 1 3020ND23.1 22.8
1,2-Dichloroethane ug/L 20 112 60-140107 5 3020ND22.5 21.3
1,2-Dichloropropane ug/L 20 106 60-140103 4 3020ND21.3 20.5
1,3,5-Trimethylbenzene ug/L 20 119 60-140115 3 3020ND23.7 23.1
1,3-Dichlorobenzene ug/L 20 113 60-140112 1 3020ND22.6 22.5
1,3-Dichloropropane ug/L 20 116 60-140113 2 3020ND23.1 22.6
1,4-Dichlorobenzene ug/L 20 113 60-140112 1 3020ND22.6 22.3
2,2-Dichloropropane ug/L 20 69 60-14068 2 3020ND13.9 13.6
2-Chlorotoluene ug/L 20 118 60-140114 4 3020ND23.6 22.7
4-Chlorotoluene ug/L 20 119 60-140117 2 3020ND23.9 23.4
Benzene ug/L 20 107 60-140105 2 3020ND21.4 21.1
Bromobenzene ug/L 20 124 60-140119 4 3020ND24.7 23.8
Bromochloromethane ug/L 20 107 60-140106 2 3020ND21.5 21.1
Bromodichloromethane ug/L 20 117 60-140113 4 3020ND23.4 22.6
Bromoform ug/L 20 110 60-140109 1 3020ND22.0 21.8
Bromomethane ug/L 20 93 60-140103 10 3020ND18.6 20.7
Carbon tetrachloride ug/L 20 124 60-140118 5 3020ND24.8 23.7
Chlorobenzene ug/L 20 113 60-140112 0 3020ND22.5 22.4
Chloroethane ug/L 20 110 60-140104 6 3020ND22.0 20.7
Chloroform ug/L 20 114 60-140111 3 3020ND22.8 22.1
Chloromethane ug/L 20 90 60-14091 1 3020ND18.0 18.3
cis-1,2-Dichloroethene ug/L 20 112 60-140109 3 3020ND22.4 21.8
cis-1,3-Dichloropropene ug/L 20 95 60-14094 2 3020ND19.1 18.7
Dibromochloromethane ug/L 20 128 60-140127 1 3020ND25.6 25.4
Dibromomethane ug/L 20 103 60-140103 0 3020ND20.7 20.6
Dichlorodifluoromethane ug/L 20 107 60-140100 6 3020ND21.3 20.0
Diisopropyl ether ug/L 20 106 60-140102 4 3020ND21.3 20.5
Ethylbenzene ug/L 20 114 60-140111 2 3020ND22.8 22.3
Hexachloro-1,3-butadiene ug/L 20 91 60-14091 0 3020ND18.3 18.3
Isopropylbenzene (Cumene)ug/L 20 106 60-140104 3 3020ND21.3 20.7
m&p-Xylene ug/L 40 115 60-140112 2 3040ND45.9 44.9
Methyl-tert-butyl ether ug/L 20 112 60-140110 2 3020ND22.4 22.1
Methylene Chloride ug/L 20 100 60-14096 4 3020ND20.0 19.2
n-Butylbenzene ug/L 20 109 60-140106 2 3020ND21.7 21.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 34 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
842221MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92132496015
842222
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 120 60-140117 2 3020ND24.0 23.4
Naphthalene ug/L 20 119 60-140120 1 3020ND23.8 23.9
o-Xylene ug/L 20 106 60-140103 2 3020ND21.1 20.7
sec-Butylbenzene ug/L 20 115 60-140112 2 3020ND23.0 22.5
Styrene ug/L 20 108 60-140106 2 3020ND21.6 21.2
tert-Butylbenzene ug/L 20 115 60-140115 0 3020ND23.0 23.0
Tetrachloroethene ug/L 20 112 60-140110 2 3020ND22.4 22.1
Toluene ug/L 20 105 60-140103 2 3020ND21.0 20.5
trans-1,2-Dichloroethene ug/L 20 111 60-140108 3 3020ND22.2 21.5
trans-1,3-Dichloropropene ug/L 20 108 60-140106 2 3020ND21.6 21.3
Trichloroethene ug/L 20 109 60-140107 2 3020ND21.7 21.4
Trichlorofluoromethane ug/L 20 124 60-140115 8 3020ND24.9 23.1
Vinyl chloride ug/L 20 108 60-140103 5 3020ND21.6 20.6
1,2-Dichloroethane-d4 (S)%107 70-130103
4-Bromofluorobenzene (S)%88 70-13087
Dibromofluoromethane (S)%103 70-130101
Toluene-d8 (S)%95 70-13095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 35 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/20515
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92132770001, 92132770002, 92132770003, 92132770004, 92132770006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:841479
Associated Lab Samples:92132770001, 92132770002, 92132770003, 92132770004, 92132770006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/27/12 04:02
1,1,1-Trichloroethane ug/L ND 0.50 09/27/12 04:02
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/27/12 04:02
1,1,2-Trichloroethane ug/L ND 0.50 09/27/12 04:02
1,1-Dichloroethane ug/L ND 0.50 09/27/12 04:02
1,1-Dichloroethene ug/L ND 0.50 09/27/12 04:02
1,1-Dichloropropene ug/L ND 0.50 09/27/12 04:02
1,2,3-Trichlorobenzene ug/L ND 2.0 09/27/12 04:02
1,2,3-Trichloropropane ug/L ND 0.50 09/27/12 04:02
1,2,4-Trichlorobenzene ug/L ND 2.0 09/27/12 04:02
1,2,4-Trimethylbenzene ug/L ND 0.50 09/27/12 04:02
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/27/12 04:02
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/27/12 04:02
1,2-Dichlorobenzene ug/L ND 0.50 09/27/12 04:02
1,2-Dichloroethane ug/L ND 0.50 09/27/12 04:02
1,2-Dichloropropane ug/L ND 0.50 09/27/12 04:02
1,3,5-Trimethylbenzene ug/L ND 0.50 09/27/12 04:02
1,3-Dichlorobenzene ug/L ND 0.50 09/27/12 04:02
1,3-Dichloropropane ug/L ND 0.50 09/27/12 04:02
1,4-Dichlorobenzene ug/L ND 0.50 09/27/12 04:02
2,2-Dichloropropane ug/L ND 0.50 09/27/12 04:02
2-Chlorotoluene ug/L ND 0.50 09/27/12 04:02
4-Chlorotoluene ug/L ND 0.50 09/27/12 04:02
Benzene ug/L ND 0.50 09/27/12 04:02
Bromobenzene ug/L ND 0.50 09/27/12 04:02
Bromochloromethane ug/L ND 0.50 09/27/12 04:02
Bromodichloromethane ug/L ND 0.50 09/27/12 04:02
Bromoform ug/L ND 0.50 09/27/12 04:02
Bromomethane ug/L ND 5.0 09/27/12 04:02
Carbon tetrachloride ug/L ND 0.50 09/27/12 04:02
Chlorobenzene ug/L ND 0.50 09/27/12 04:02
Chloroethane ug/L ND 1.0 09/27/12 04:02
Chloroform ug/L ND 0.50 09/27/12 04:02
Chloromethane ug/L ND 1.0 09/27/12 04:02
cis-1,2-Dichloroethene ug/L ND 0.50 09/27/12 04:02
cis-1,3-Dichloropropene ug/L ND 0.50 09/27/12 04:02
Dibromochloromethane ug/L ND 0.50 09/27/12 04:02
Dibromomethane ug/L ND 0.50 09/27/12 04:02
Dichlorodifluoromethane ug/L ND 0.50 09/27/12 04:02
Diisopropyl ether ug/L ND 0.50 09/27/12 04:02
Ethylbenzene ug/L ND 0.50 09/27/12 04:02
Hexachloro-1,3-butadiene ug/L ND 2.0 09/27/12 04:02
Isopropylbenzene (Cumene)ug/L ND 0.50 09/27/12 04:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 36 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:841479
Associated Lab Samples:92132770001, 92132770002, 92132770003, 92132770004, 92132770006
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 09/27/12 04:02
Methyl-tert-butyl ether ug/L ND 0.50 09/27/12 04:02
Methylene Chloride ug/L ND 2.0 09/27/12 04:02
n-Butylbenzene ug/L ND 0.50 09/27/12 04:02
n-Propylbenzene ug/L ND 0.50 09/27/12 04:02
Naphthalene ug/L ND 2.0 09/27/12 04:02
o-Xylene ug/L ND 0.50 09/27/12 04:02
sec-Butylbenzene ug/L ND 0.50 09/27/12 04:02
Styrene ug/L ND 0.50 09/27/12 04:02
tert-Butylbenzene ug/L ND 0.50 09/27/12 04:02
Tetrachloroethene ug/L ND 0.50 09/27/12 04:02
Toluene ug/L ND 0.50 09/27/12 04:02
trans-1,2-Dichloroethene ug/L ND 0.50 09/27/12 04:02
trans-1,3-Dichloropropene ug/L ND 0.50 09/27/12 04:02
Trichloroethene ug/L ND 0.50 09/27/12 04:02
Trichlorofluoromethane ug/L ND 1.0 09/27/12 04:02
Vinyl chloride ug/L ND 1.0 09/27/12 04:02
1,2-Dichloroethane-d4 (S)%101 70-130 09/27/12 04:02
4-Bromofluorobenzene (S)%99 70-130 09/27/12 04:02
Dibromofluoromethane (S)%100 70-130 09/27/12 04:02
Toluene-d8 (S)%98 70-130 09/27/12 04:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
841480LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.750 95 60-140
1,1,1-Trichloroethane ug/L 48.850 98 60-140
1,1,2,2-Tetrachloroethane ug/L 48.250 96 60-140
1,1,2-Trichloroethane ug/L 49.750 99 60-140
1,1-Dichloroethane ug/L 45.950 92 60-140
1,1-Dichloroethene ug/L 46.850 94 60-140
1,1-Dichloropropene ug/L 48.550 97 60-140
1,2,3-Trichlorobenzene ug/L 51.350 103 60-140
1,2,3-Trichloropropane ug/L 49.250 98 60-140
1,2,4-Trichlorobenzene ug/L 52.650 105 60-140
1,2,4-Trimethylbenzene ug/L 49.050 98 60-140
1,2-Dibromo-3-chloropropane ug/L 52.150 104 60-140
1,2-Dibromoethane (EDB)ug/L 48.950 98 60-140
1,2-Dichlorobenzene ug/L 49.750 99 60-140
1,2-Dichloroethane ug/L 44.750 89 60-140
1,2-Dichloropropane ug/L 45.450 91 60-140
1,3,5-Trimethylbenzene ug/L 47.850 96 60-140
1,3-Dichlorobenzene ug/L 49.250 98 60-140
1,3-Dichloropropane ug/L 47.850 96 60-140
1,4-Dichlorobenzene ug/L 47.550 95 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 37 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
841480LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 41.250 82 60-140
2-Chlorotoluene ug/L 48.450 97 60-140
4-Chlorotoluene ug/L 48.050 96 60-140
Benzene ug/L 46.650 93 60-140
Bromobenzene ug/L 46.750 93 60-140
Bromochloromethane ug/L 48.250 96 60-140
Bromodichloromethane ug/L 48.450 97 60-140
Bromoform ug/L 53.450 107 60-140
Bromomethane ug/L 40.250 80 60-140
Carbon tetrachloride ug/L 46.750 93 60-140
Chlorobenzene ug/L 48.550 97 60-140
Chloroethane ug/L 19.2 1g503860-140
Chloroform ug/L 46.850 94 60-140
Chloromethane ug/L 41.250 82 60-140
cis-1,2-Dichloroethene ug/L 45.950 92 60-140
cis-1,3-Dichloropropene ug/L 47.850 96 60-140
Dibromochloromethane ug/L 51.250 102 60-140
Dibromomethane ug/L 48.050 96 60-140
Dichlorodifluoromethane ug/L 44.750 89 60-140
Diisopropyl ether ug/L 45.250 90 60-140
Ethylbenzene ug/L 48.450 97 60-140
Hexachloro-1,3-butadiene ug/L 51.650 103 60-140
Isopropylbenzene (Cumene)ug/L 48.150 96 60-140
m&p-Xylene ug/L 99.4100 99 60-140
Methyl-tert-butyl ether ug/L 49.050 98 60-140
Methylene Chloride ug/L 46.350 93 60-140
n-Butylbenzene ug/L 49.250 98 60-140
n-Propylbenzene ug/L 47.450 95 60-140
Naphthalene ug/L 52.250 104 60-140
o-Xylene ug/L 47.750 95 60-140
sec-Butylbenzene ug/L 48.450 97 60-140
Styrene ug/L 51.350 103 60-140
tert-Butylbenzene ug/L 47.750 95 60-140
Tetrachloroethene ug/L 47.950 96 60-140
Toluene ug/L 46.850 94 60-140
trans-1,2-Dichloroethene ug/L 45.650 91 60-140
trans-1,3-Dichloropropene ug/L 49.350 99 60-140
Trichloroethene ug/L 46.250 92 60-140
Trichlorofluoromethane ug/L 37.950 76 60-140
Vinyl chloride ug/L 45.050 90 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%104 70-130
Dibromofluoromethane (S)%99 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 38 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
841481MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92132770004
841482
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 110 60-140109 1 3020ND22.0 21.7
1,1,1-Trichloroethane ug/L 20 115 60-140112 3 3020ND23.1 22.3
1,1,2,2-Tetrachloroethane ug/L 20 103 60-140100 3 3020ND20.5 19.9
1,1,2-Trichloroethane ug/L 20 113 60-140109 4 3020ND22.6 21.8
1,1-Dichloroethane ug/L 20 103 60-140102 2 3020ND20.6 20.3
1,1-Dichloroethene ug/L 20 113 60-140108 4 3020ND22.6 21.7
1,1-Dichloropropene ug/L 20 112 60-140108 3 3020ND22.3 21.7
1,2,3-Trichlorobenzene ug/L 20 109 60-140108 1 3020ND21.7 21.5
1,2,3-Trichloropropane ug/L 20 105 60-140102 3 3020ND21.0 20.4
1,2,4-Trichlorobenzene ug/L 20 112 60-140111 1 3020ND22.5 22.2
1,2,4-Trimethylbenzene ug/L 20 116 60-140113 3 3020ND23.2 22.5
1,2-Dibromo-3-chloropropane ug/L 20 107 60-140105 1 3020ND21.4 21.1
1,2-Dibromoethane (EDB)ug/L 20 108 60-140105 2 3020ND21.6 21.1
1,2-Dichlorobenzene ug/L 20 112 60-140109 3 3020ND22.3 21.8
1,2-Dichloroethane ug/L 20 101 60-14099 3 3020ND20.3 19.7
1,2-Dichloropropane ug/L 20 101 60-14098 3 3020ND20.2 19.5
1,3,5-Trimethylbenzene ug/L 20 115 60-140112 3 3020ND23.1 22.4
1,3-Dichlorobenzene ug/L 20 114 60-140110 4 3020ND22.8 22.0
1,3-Dichloropropane ug/L 20 106 60-140104 2 3020ND21.2 20.8
1,4-Dichlorobenzene ug/L 20 109 60-140108 1 3020ND21.9 21.6
2,2-Dichloropropane ug/L 20 109 60-140106 3 3020ND21.9 21.1
2-Chlorotoluene ug/L 20 114 60-140110 3 3020ND22.8 22.1
4-Chlorotoluene ug/L 20 114 60-140112 1 3020ND22.7 22.4
Benzene ug/L 20 109 60-140105 5 3020ND21.9 20.9
Bromobenzene ug/L 20 109 60-140106 3 3020ND21.8 21.2
Bromochloromethane ug/L 20 108 60-140105 3 3020ND21.6 21.0
Bromodichloromethane ug/L 20 112 60-140108 4 3020ND22.5 21.6
Bromoform ug/L 20 115 60-140112 3 3020ND22.9 22.3
Bromomethane ug/L 20 65 60-14077 17 3020ND13.1 15.5
Carbon tetrachloride ug/L 20 117 60-140112 5 3020ND23.5 22.4
Chlorobenzene ug/L 20 115 60-140111 3 3020ND23.0 22.2
Chloroethane ug/L 20 97 60-14092 5 3020ND19.3 18.4
Chloroform ug/L 20 108 60-140107 1 3020ND21.5 21.4
Chloromethane ug/L 20 80 60-14080 1 3020ND16.1 15.9
cis-1,2-Dichloroethene ug/L 20 103 60-140100 3 3020ND20.6 20.0
cis-1,3-Dichloropropene ug/L 20 105 60-140103 2 3020ND21.0 20.6
Dibromochloromethane ug/L 20 115 60-140112 3 3020ND23.0 22.5
Dibromomethane ug/L 20 111 60-140108 3 3020ND22.2 21.6
Dichlorodifluoromethane ug/L 20 93 60-14090 3 3020ND18.6 18.0
Diisopropyl ether ug/L 20 96 60-14094 2 3020ND19.2 18.9
Ethylbenzene ug/L 20 114 60-140111 3 3020ND22.8 22.2
Hexachloro-1,3-butadiene ug/L 20 114 60-140115 1 3020ND22.8 23.0
Isopropylbenzene (Cumene)ug/L 20 112 60-140110 1 3020ND22.4 22.1
m&p-Xylene ug/L 40 118 60-140115 3 3040ND47.4 46.1
Methyl-tert-butyl ether ug/L 20 106 60-140102 4 3020ND21.1 20.4
Methylene Chloride ug/L 20 106 60-140100 6 3020ND22.0 20.7
n-Butylbenzene ug/L 20 115 60-140113 1 3020ND23.0 22.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 39 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
841481MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92132770004
841482
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 115 60-140112 3 3020ND23.1 22.5
Naphthalene ug/L 20 108 60-140106 1 3020ND21.6 21.3
o-Xylene ug/L 20 111 60-140110 1 3020ND22.2 21.9
sec-Butylbenzene ug/L 20 117 60-140113 3 3020ND23.3 22.7
Styrene ug/L 20 116 60-140112 4 3020ND23.3 22.4
tert-Butylbenzene ug/L 20 114 60-140113 2 3020ND22.9 22.5
Tetrachloroethene ug/L 20 119 60-140117 2 3020ND23.7 23.3
Toluene ug/L 20 109 60-140105 4 3020ND22.0 21.2
trans-1,2-Dichloroethene ug/L 20 103 60-140101 2 3020ND20.6 20.2
trans-1,3-Dichloropropene ug/L 20 112 60-140108 4 3020ND22.5 21.5
Trichloroethene ug/L 20 110 60-140106 3 3020ND22.0 21.3
Trichlorofluoromethane ug/L 20 109 60-140103 5 3020ND21.9 20.8
Vinyl chloride ug/L 20 91 60-14090 1 3020ND18.2 18.0
1,2-Dichloroethane-d4 (S)%95 70-13096
4-Bromofluorobenzene (S)%102 70-130102
Dibromofluoromethane (S)%98 70-13097
Toluene-d8 (S)%99 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 40 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/20527
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92132770012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:843038
Associated Lab Samples:92132770012
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/28/12 06:42
1,1,1-Trichloroethane ug/L ND 0.50 09/28/12 06:42
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/28/12 06:42
1,1,2-Trichloroethane ug/L ND 0.50 09/28/12 06:42
1,1-Dichloroethane ug/L ND 0.50 09/28/12 06:42
1,1-Dichloroethene ug/L ND 0.50 09/28/12 06:42
1,1-Dichloropropene ug/L ND 0.50 09/28/12 06:42
1,2,3-Trichlorobenzene ug/L ND 2.0 09/28/12 06:42
1,2,3-Trichloropropane ug/L ND 0.50 09/28/12 06:42
1,2,4-Trichlorobenzene ug/L ND 2.0 09/28/12 06:42
1,2,4-Trimethylbenzene ug/L ND 0.50 09/28/12 06:42
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/28/12 06:42
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/28/12 06:42
1,2-Dichlorobenzene ug/L ND 0.50 09/28/12 06:42
1,2-Dichloroethane ug/L ND 0.50 09/28/12 06:42
1,2-Dichloropropane ug/L ND 0.50 09/28/12 06:42
1,3,5-Trimethylbenzene ug/L ND 0.50 09/28/12 06:42
1,3-Dichlorobenzene ug/L ND 0.50 09/28/12 06:42
1,3-Dichloropropane ug/L ND 0.50 09/28/12 06:42
1,4-Dichlorobenzene ug/L ND 0.50 09/28/12 06:42
2,2-Dichloropropane ug/L ND 0.50 09/28/12 06:42
2-Chlorotoluene ug/L ND 0.50 09/28/12 06:42
4-Chlorotoluene ug/L ND 0.50 09/28/12 06:42
Benzene ug/L ND 0.50 09/28/12 06:42
Bromobenzene ug/L ND 0.50 09/28/12 06:42
Bromochloromethane ug/L ND 0.50 09/28/12 06:42
Bromodichloromethane ug/L ND 0.50 09/28/12 06:42
Bromoform ug/L ND 0.50 09/28/12 06:42
Bromomethane ug/L ND 5.0 09/28/12 06:42
Carbon tetrachloride ug/L ND 0.50 09/28/12 06:42
Chlorobenzene ug/L ND 0.50 09/28/12 06:42
Chloroethane ug/L ND 1.0 09/28/12 06:42
Chloroform ug/L ND 0.50 09/28/12 06:42
Chloromethane ug/L ND 1.0 09/28/12 06:42
cis-1,2-Dichloroethene ug/L ND 0.50 09/28/12 06:42
cis-1,3-Dichloropropene ug/L ND 0.50 09/28/12 06:42
Dibromochloromethane ug/L ND 0.50 09/28/12 06:42
Dibromomethane ug/L ND 0.50 09/28/12 06:42
Dichlorodifluoromethane ug/L ND 0.50 09/28/12 06:42
Diisopropyl ether ug/L ND 0.50 09/28/12 06:42
Ethylbenzene ug/L ND 0.50 09/28/12 06:42
Hexachloro-1,3-butadiene ug/L ND 2.0 09/28/12 06:42
Isopropylbenzene (Cumene)ug/L ND 0.50 09/28/12 06:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 41 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:843038
Associated Lab Samples:92132770012
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 09/28/12 06:42
Methyl-tert-butyl ether ug/L ND 0.50 09/28/12 06:42
Methylene Chloride ug/L ND 2.0 09/28/12 06:42
n-Butylbenzene ug/L ND 0.50 09/28/12 06:42
n-Propylbenzene ug/L ND 0.50 09/28/12 06:42
Naphthalene ug/L ND 2.0 09/28/12 06:42
o-Xylene ug/L ND 0.50 09/28/12 06:42
sec-Butylbenzene ug/L ND 0.50 09/28/12 06:42
Styrene ug/L ND 0.50 09/28/12 06:42
tert-Butylbenzene ug/L ND 0.50 09/28/12 06:42
Tetrachloroethene ug/L ND 0.50 09/28/12 06:42
Toluene ug/L ND 0.50 09/28/12 06:42
trans-1,2-Dichloroethene ug/L ND 0.50 09/28/12 06:42
trans-1,3-Dichloropropene ug/L ND 0.50 09/28/12 06:42
Trichloroethene ug/L ND 0.50 09/28/12 06:42
Trichlorofluoromethane ug/L ND 1.0 09/28/12 06:42
Vinyl chloride ug/L ND 1.0 09/28/12 06:42
1,2-Dichloroethane-d4 (S)%123 70-130 09/28/12 06:42
4-Bromofluorobenzene (S)%82 70-130 09/28/12 06:42
Dibromofluoromethane (S)%110 70-130 09/28/12 06:42
Toluene-d8 (S)%97 70-130 09/28/12 06:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
843039LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.950 110 60-140
1,1,1-Trichloroethane ug/L 52.350 105 60-140
1,1,2,2-Tetrachloroethane ug/L 45.950 92 60-140
1,1,2-Trichloroethane ug/L 47.750 95 60-140
1,1-Dichloroethane ug/L 51.050 102 60-140
1,1-Dichloroethene ug/L 50.050 100 60-140
1,1-Dichloropropene ug/L 45.950 92 60-140
1,2,3-Trichlorobenzene ug/L 54.550 109 60-140
1,2,3-Trichloropropane ug/L 47.750 95 60-140
1,2,4-Trichlorobenzene ug/L 53.550 107 60-140
1,2,4-Trimethylbenzene ug/L 54.850 110 60-140
1,2-Dibromo-3-chloropropane ug/L 74.4 CU5014960-140
1,2-Dibromoethane (EDB)ug/L 54.050 108 60-140
1,2-Dichlorobenzene ug/L 52.650 105 60-140
1,2-Dichloroethane ug/L 48.050 96 60-140
1,2-Dichloropropane ug/L 46.150 92 60-140
1,3,5-Trimethylbenzene ug/L 54.350 109 60-140
1,3-Dichlorobenzene ug/L 52.250 104 60-140
1,3-Dichloropropane ug/L 51.550 103 60-140
1,4-Dichlorobenzene ug/L 51.450 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 42 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
843039LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 41.150 82 60-140
2-Chlorotoluene ug/L 51.150 102 60-140
4-Chlorotoluene ug/L 52.950 106 60-140
Benzene ug/L 46.650 93 60-140
Bromobenzene ug/L 52.050 104 60-140
Bromochloromethane ug/L 47.350 95 60-140
Bromodichloromethane ug/L 52.450 105 60-140
Bromoform ug/L 51.650 103 60-140
Bromomethane ug/L 36.550 73 60-140
Carbon tetrachloride ug/L 54.450 109 60-140
Chlorobenzene ug/L 50.950 102 60-140
Chloroethane ug/L 40.050 80 60-140
Chloroform ug/L 49.450 99 60-140
Chloromethane ug/L 39.650 79 60-140
cis-1,2-Dichloroethene ug/L 49.250 98 60-140
cis-1,3-Dichloropropene ug/L 50.650 101 60-140
Dibromochloromethane ug/L 61.650 123 60-140
Dibromomethane ug/L 46.850 94 60-140
Dichlorodifluoromethane ug/L 36.450 73 60-140
Diisopropyl ether ug/L 47.650 95 60-140
Ethylbenzene ug/L 51.150 102 60-140
Hexachloro-1,3-butadiene ug/L 50.250 100 60-140
Isopropylbenzene (Cumene)ug/L 50.950 102 60-140
m&p-Xylene ug/L 103100 103 60-140
Methyl-tert-butyl ether ug/L 50.050 100 60-140
Methylene Chloride ug/L 44.250 88 60-140
n-Butylbenzene ug/L 53.750 107 60-140
n-Propylbenzene ug/L 53.250 106 60-140
Naphthalene ug/L 57.850 116 60-140
o-Xylene ug/L 49.850 100 60-140
sec-Butylbenzene ug/L 54.450 109 60-140
Styrene ug/L 52.150 104 60-140
tert-Butylbenzene ug/L 54.750 109 60-140
Tetrachloroethene ug/L 52.550 105 60-140
Toluene ug/L 46.350 93 60-140
trans-1,2-Dichloroethene ug/L 48.150 96 60-140
trans-1,3-Dichloropropene ug/L 54.250 108 60-140
Trichloroethene ug/L 48.750 97 60-140
Trichlorofluoromethane ug/L 48.250 96 60-140
Vinyl chloride ug/L 41.050 82 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%90 70-130
Dibromofluoromethane (S)%101 70-130
Toluene-d8 (S)%95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 43 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
843040MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92133172001
843041
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 115 60-140113 2 3020ND23.1 22.6
1,1,1-Trichloroethane ug/L 20 117 60-140116 1 3020ND23.5 23.2
1,1,2,2-Tetrachloroethane ug/L 20 87 60-14087 0 3020ND17.4 17.4
1,1,2-Trichloroethane ug/L 20 98 60-14098 0 3020ND19.6 19.6
1,1-Dichloroethane ug/L 20 112 60-140111 0 3020ND22.4 22.3
1,1-Dichloroethene ug/L 20 116 60-140114 1 3020ND23.2 22.9
1,1-Dichloropropene ug/L 20 101 60-14099 2 3020ND20.2 19.9
1,2,3-Trichlorobenzene ug/L 20 111 60-140112 1 3020ND22.3 22.4
1,2,3-Trichloropropane ug/L 20 93 60-14093 0 3020ND18.6 18.5
1,2,4-Trichlorobenzene ug/L 20 113 60-140111 2 3020ND22.6 22.3
1,2,4-Trimethylbenzene ug/L 20 123 60-140118 4 3020ND24.6 23.6
1,2-Dibromo-3-chloropropane ug/L M02014360-140147 3 3020ND28.7 29.4
1,2-Dibromoethane (EDB)ug/L 20 108 60-140108 1 3020ND21.7 21.5
1,2-Dichlorobenzene ug/L 20 114 60-140110 3 3020ND22.7 22.1
1,2-Dichloroethane ug/L 20 103 60-140105 2 3020ND20.6 21.1
1,2-Dichloropropane ug/L 20 99 60-14098 1 3020ND19.8 19.6
1,3,5-Trimethylbenzene ug/L 20 120 60-140117 3 3020ND24.1 23.4
1,3-Dichlorobenzene ug/L 20 114 60-140111 3 3020ND22.7 22.1
1,3-Dichloropropane ug/L 20 106 60-140106 1 3020ND21.1 21.3
1,4-Dichlorobenzene ug/L 20 113 60-140111 2 3020ND22.6 22.2
2,2-Dichloropropane ug/L 20 117 60-140115 2 3020ND23.5 23.1
2-Chlorotoluene ug/L 20 115 60-140114 1 3020ND23.0 22.7
4-Chlorotoluene ug/L 20 115 60-140117 1 3020ND23.0 23.3
Benzene ug/L 20 101 60-140100 1 3020ND20.2 20.1
Bromobenzene ug/L 20 116 60-140117 0 3020ND23.3 23.4
Bromochloromethane ug/L 20 101 60-140100 1 3020ND20.2 20.0
Bromodichloromethane ug/L 20 111 60-140111 0 3020ND22.3 22.2
Bromoform ug/L 20 103 60-140103 0 3020ND20.6 20.5
Bromomethane ug/L 20 103 60-140107 3 3020ND20.7 21.3
Carbon tetrachloride ug/L 20 120 60-140118 2 3020ND24.1 23.5
Chlorobenzene ug/L 20 110 60-140108 2 3020ND22.0 21.6
Chloroethane ug/L 20 98 60-14098 0 3020ND19.6 19.6
Chloroform ug/L 20 111 60-140109 2 3020ND22.1 21.7
Chloromethane ug/L 20 75 60-14073 2 3020ND15.1 14.8
cis-1,2-Dichloroethene ug/L 20 107 60-140107 0 3020ND21.4 21.5
cis-1,3-Dichloropropene ug/L 20 103 60-140102 1 3020ND20.5 20.4
Dibromochloromethane ug/L 20 122 60-140123 1 3020ND24.4 24.5
Dibromomethane ug/L 20 96 60-14094 2 3020ND19.1 18.8
Dichlorodifluoromethane ug/L 20 82 60-14080 2 3020ND16.3 15.9
Diisopropyl ether ug/L 20 102 60-140102 1 3020ND20.4 20.5
Ethylbenzene ug/L 20 111 60-140108 3 3020ND22.3 21.7
Hexachloro-1,3-butadiene ug/L 20 115 60-140117 2 3020ND23.0 23.4
Isopropylbenzene (Cumene)ug/L 20 107 60-140104 2 3020ND21.4 20.9
m&p-Xylene ug/L 40 112 60-140111 1 3040ND44.7 44.3
Methyl-tert-butyl ether ug/L 20 103 60-140105 1 3020ND20.6 20.9
Methylene Chloride ug/L 20 94 60-14096 3 3020ND18.7 19.2
n-Butylbenzene ug/L 20 123 60-140122 1 3020ND24.5 24.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 44 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
843040MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92133172001
843041
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 121 60-140120 1 3020ND24.2 24.0
Naphthalene ug/L 20 115 60-140112 3 3020ND22.9 22.3
o-Xylene ug/L 20 104 60-140102 2 3020ND20.8 20.4
sec-Butylbenzene ug/L 20 122 60-140118 4 3020ND24.4 23.5
Styrene ug/L 20 105 60-140104 1 3020ND21.0 20.8
tert-Butylbenzene ug/L 20 120 60-140117 2 3020ND23.9 23.4
Tetrachloroethene ug/L 20 116 60-140113 3 3020ND23.3 22.5
Toluene ug/L 20 99 60-14099 1 3020ND19.9 19.8
trans-1,2-Dichloroethene ug/L 20 109 60-140110 1 3020ND21.8 22.0
trans-1,3-Dichloropropene ug/L 20 110 60-140113 2 3020ND22.1 22.5
Trichloroethene ug/L 20 106 60-140104 2 3020ND21.2 20.7
Trichlorofluoromethane ug/L 20 115 60-140112 3 3020ND23.1 22.5
Vinyl chloride ug/L 20 93 60-14091 2 3020ND18.5 18.2
1,2-Dichloroethane-d4 (S)%101 70-130106
4-Bromofluorobenzene (S)%87 70-13087
Dibromofluoromethane (S)%101 70-130103
Toluene-d8 (S)%94 70-13095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 45 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The initial calibration for this compound was outside of method control limits. A PRL check was analyzed to verify that the
low level standard could be detected. No analyte presence was detected in the associated samples. Results unaffected
by low bias.
1g
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. Analyte presence below
reporting limits in associated samples. Results unaffected by high bias.CU
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 46 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92132770
Inc.#1943 Wise Conv. Mart
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92132770001 MSV/20515MW-1 SM 6200B
92132770002 MSV/20515MW-2 SM 6200B
92132770003 MSV/20515MW-3 SM 6200B
92132770004 MSV/20515MW-4 SM 6200B
92132770005 MSV/20460MW-5 SM 6200B
92132770006 MSV/20515MW-6 SM 6200B
92132770007 MSV/20460MW-7 SM 6200B
92132770008 MSV/20460WSW-1 SM 6200B
92132770009 MSV/20460WSW-4 SM 6200B
92132770010 MSV/20460WSW-5 SM 6200B
92132770011 MSV/20460WSW-5A SM 6200B
92132770012 MSV/20527WSW-6 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2012 11:03 AM Page 47 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]

APPENDIX C

Field Notes