MO-28112_47377_CA_UST-61_20201112

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases
in NC
This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
suspected release
(DWM USE ONLY) Incident # ________ Risk (H,I,L,U)_______ Received On ________ Received By ________
Reported by (circle one): Phone, Fax or Report Region _______
Suspected Contamination? (Y/N) ________ Confirmed GW Contamination? (Y/N) ______ Confirmed Soil Contamination ?(Y/N) ______
Samples Taken?(Y/N) ______ Free Product? (Y/N) _____ If Yes, State Greatest Thickness ______________
Facility ID Number ______________ Date Leak Discovered ___________ Comm/Non-Commercial? ________
Reg/Non-regulated? _____________
INCIDENT DESCRIPTION
Incident Name:
Address: County:
City/Town: Zip Code:Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by:
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)  GPS
 Topographic map
 GIS Address matching
 Other
 Unknown
Describe location:
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
 Release Detection Equipment or Methods
 During UST Closure/Removal
 Property Transfer
 Visual/Odor
 Water in Tank
 Water Supply Well Contamination
 Groundwater Contamination
 Surface Water Contamination
 Other (specify) _______________
SOURCE OF CONTAMINATION
Source of Release (Check primary source) Cause of Release (Check primary cause) Type of Release (Check one) Product Type Released (Check primary product type released)
 Tank
 Piping
 Dispenser
 Submersible Turbine Pump
 Delivery Problem
 Spill Bucket
 Other
 Unknown
Definitions presented on reverse
 Spill
 Overfill
 Corrosion
 Physical/Mechanical
Damage
 Install Problem
 Other
 Unknown
Definitions presented on reverse
 Petroleum
 Non-Petroleum
 Both
Location
(Check one)
 Facility
 Residence
 Other
 Gasoline/ Diesel/
Kerosene
 Heating Oil
 Other Petroleum
Products
 Metals
 Other Inorganics
 Other Organics
 Diesel/Veg. Oil
Blend
 Vegetable Oil 100%
 E10 – E20
 E21 – E84
 E85 – E99
 Ethanol 100%
 E01 – E09
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2
8325 Old Statesville Road
Charlotte
Mecklenburg
former SM80
35.335972 -80.825430
xDuring Phase II assessment, elevated soil and groundwater constituents
discovered - addendum to UST closure
x x
x
x
x
______
____
______
28269
X
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1.Yes 2. No 3. Unknown
Number of Water Supply Wells Affected __________________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1. 2. 3.
UST SYSTEM OWNER UST Owner/Company
Point of Contact Address
City State Zip Code Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company Address
City State Zip Code Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner Address
City State Zip Code Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/19) Page 2 of 2
Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined
_____
Sam's Real Estate Holdings
Sam's Real Estate Holdings
Sam's Real Estate Holdings
Matthews NC
7935 Council Place Dr., Suite 200 Tonya Martin
28105
Please see attached
Mike Stanforth
Agent for SM ECEA
625 Huntsman Ct., Gastonia NC 28054 11/12/20
704-853-0800
DumpsterAreaCar Wash7-ElevenStore #36779TFormer KeroseneDispenserWT Harris BoulevardOld Statesv
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e

R
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a
d#1#2#3#4Fuel CanopyGoodyearAuto ServiceSherwin-WilliamsPaint StoreCitgo GasolineStationSB-2SB-1SB-3SB-4LEGEND:DispenserUnderground Storage TankTTransformerStorm DrainVent PipesUST #1 DieselUST #2 Premium Unleaded GasolineUST #3 Regular Unleaded GasolineUST #4 Former KeroseneApproximate Property BoundaryNOTE: Kerosene tank removed October 13, 2020.Former DispenserFormer Underground Storage TankSoil Boring LocationNSCALE IN FEET:40400SITE PLANDATE:DRAWN BY:REVIEWED BY:PROJECT NO.:NOTE: ALL MAP FEATURES ARE APPROXIMATEIN SCALE AND LOCATION.FIGURE 2OCT 2020V. MOLDOVANN. PINSKER7-Eleven, Inc.7-Eleven Store #367798325 Old Statesville RoadCharlotte, NCGOOGLE IMAGERY
ANALYTICAL REPORT
Eurofins TestAmerica, Pensacola
3355 McLemore Drive
Pensacola, FL 32514
Tel: [phone]
Laboratory Job ID: 400-194926-1
Client Project/Site: 7-11 No 36779 (NC)
For:
AECOM
1600 Perimeter Park Drive
Suite 400
Morrisville, North Carolina 27560
Attn: Mr. Nathan Pinsker
Authorized for release by:
11/6/2020 12:27:35 PM
Lauren Evans, Project Management Assistant I
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Laboratory Job ID: 400-194926-1
Page 2 of 76 Eurofins TestAmerica, Pensacola11/6/2020
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .40
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .66
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .73
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .74
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .75
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .76
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Case Narrative
Client: AECOM Job ID: 400-194926-1
Project/Site: 7-11 No 36779 (NC)
Job ID: 400-194926-1
Laboratory: Eurofins TestAmerica, Pensacola
Narrative
Job Narrative
400-194926-1
Comments
No additional comments.
Receipt
The samples were received on 10/24/2020 9:05 AM; the samples arrived in good condition, and where required, properly preserved and
on ice. The temperatures of the 2 coolers at receipt time were 0.8º C and 1.1º C.
GC/MS VOA
Method 8260D: The laboratory control sample (LCS) for analytical batch 400-508707 recovered outside control limits for the following
analytes: 2-Hexanone and n-Butylbenzene. These analytes were biased high in the LCS and were not detected in the associated
samples; therefore, the data have been reported.
Method 8260D: The continuing calibration verification (CCV) associated with batch 400-508707 recovered outside acceptance criteria, low
biased, for Chloromethane and Dichlorodifluoromethane. A reporting limit (RL) standard was analyzed, and the target analyte was
detected. Since the associated samples were non-detect for this analyte, the data have been reported.
Method 8260D: The continuing calibration verification (CCV) associated with batch 400-508707 recovered above the upper control limit for
1,1,2,2-Tetrachloroethane, 1,3-Dichloropropane, 2-Chlorotoluene, n-Butylbenzene, N-Propylbenzene, sec-Butylbenzene,
trans-1,3-Dichloropropene, p-Isopropyltoluene, 4-Chlorotoluene and 1,2,4-Trimethylbenzene. The samples associated with this CCV
were non-detects for the affected analytes; therefore, the data have been reported. The associated sample is impacted: (CCVIS
400-508707/3).
Method 8260D: The continuing calibration verification (CCV) associated with batch 400-508704 recovered outside acceptance criteria, low
biased, for 1,1-Dichloropropene and Trichloroethene. A reporting limit (RL) standard was analyzed, and the target analytes were detected.
Since the associated samples were non-detect for these analytes, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270E: Six surrogates are used for this analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance
criteria without performing re-extraction/re-analysis. The following samples contained an allowable number of surrogate compounds
outside limits: B-1 (400-194926-5), B-2 (400-194926-6), B-3 (400-194926-7) and B-4 (400-194926-8). These results have been reported
and qualified.
Method 8270E: The continuing calibration verification (CCV) associated with batch 400-508919 recovered outside acceptance criteria, low
biased, for 4,6-Dinitro-2-methylphenol. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Since the
associated samples were non-detect for this analyte, the data have been reported.
Method 8270E: The continuing calibration verification (CCV) associated with batch 400-508980 recovered outside acceptance criteria, low
biased, for Hexachlorocyclopentadiene. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Since the
associated samples were non-detect for this analyte, the data have been reported.
Method 8270E: The continuing calibration verification (CCV) associated with batch 400-508916 recovered outside acceptance criteria, low
biased, for 4-Nitrophenol and Hexachlorocyclopentadiene. A reporting limit (RL) standard was analyzed, and the target analyte was
detected. Since the associated samples were non-detect for this analyte, the data have been reported.
Method 8270E: The continuing calibration verification (CCV) associated with batch 400-509157 recovered outside acceptance criteria, low
biased, for Hexachlorocyclopentadiene. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Since the
associated samples were non-detect for this analyte, the data have been reported.
Method 8270E: The continuing calibration verification (CCV) associated with batch 400-509329 recovered outside acceptance criteria, low
biased, for Hexachlorocyclopentadiene. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Since the
Eurofins TestAmerica, PensacolaPage 3 of 76 11/6/2020
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Case Narrative
Client: AECOM Job ID: 400-194926-1
Project/Site: 7-11 No 36779 (NC)
Job ID: 400-194926-1 (Continued)
Laboratory: Eurofins TestAmerica, Pensacola (Continued)
associated samples were non-detect for this analyte, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC VOA
Methods 8015C, 8015D: The following samples were diluted because the base dilution for methanol preserved soil analysis is 1:50: B-1
(400-194926-1), B-2 (400-194926-2), B-3 (400-194926-3) and B-4 (400-194926-4)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins TestAmerica, PensacolaPage 4 of 76 11/6/2020
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Detection Summary
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Client Sample ID: B-1 Lab Sample ID: 400-194926-1
☼Acetone
RL
0.0352 mg/Kg
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA10.0397 8260D
Client Sample ID: B-2 Lab Sample ID: 400-194926-2
☼Acetone
RL
0.0316 mg/Kg
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA10.0355 8260D
Client Sample ID: B-3 Lab Sample ID: 400-194926-3
☼Acetone
RL
0.0272 mg/Kg
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA10.0877 8260D
☼C10-C28 6.56 mg/Kg Total/NA16.71 8015C
Client Sample ID: B-4 Lab Sample ID: 400-194926-4
☼Acetone
RL
0.0250 mg/Kg
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA10.0690 8260D
Client Sample ID: B-1 Lab Sample ID: 400-194926-5
Chloroform
RL
1.00 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA11.20 8260D
cis-1,2-Dichloroethene 1.00 ug/L Total/NA11.02 8260D
1,1-Dichloroethene 1.00 ug/L Total/NA15.20 8260D
Trichloroethene 1.00 ug/L Total/NA175.7 8260D
Client Sample ID: B-2 Lab Sample ID: 400-194926-6
Chloroform
RL
1.00 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA110.6 8260D
Methyl tert-butyl ether 1.00 ug/L Total/NA12.44 8260D
Toluene 1.00 ug/L Total/NA12.05 8260D
C10-C28 95.3 ug/L Total/NA198.9 8015C
Client Sample ID: B-3 Lab Sample ID: 400-194926-7
Acetone
RL
25.0 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA131.2 8260D
Bromodichloromethane 1.00 ug/L Total/NA11.49 8260D
Chloroform 1.00 ug/L Total/NA14.93 8260D
Client Sample ID: B-4 Lab Sample ID: 400-194926-8
Chloroform
RL
1.00 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA12.59 8260D
Isopropyl ether 1.00 ug/L Total/NA12.03 8260D
Methyl tert-butyl ether 1.00 ug/L Total/NA128.7 8260D
Toluene 1.00 ug/L Total/NA14.30 8260D
C10-C28 95.1 ug/L Total/NA11798015C
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
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Sample Summary
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID Client Sample ID ReceivedCollectedMatrix Asset ID
400-194926-1 B-1 Solid 10/23/20 12:25 10/24/20 09:05
400-194926-2 B-2 Solid 10/23/20 12:47 10/24/20 09:05
400-194926-3 B-3 Solid 10/23/20 13:05 10/24/20 09:05
400-194926-4 B-4 Solid 10/23/20 13:15 10/24/20 09:05
400-194926-5 B-1 Water 10/23/20 11:10 10/24/20 09:05
400-194926-6 B-2 Water 10/23/20 10:50 10/24/20 09:05
400-194926-7 B-3 Water 10/23/20 11:30 10/24/20 09:05
400-194926-8 B-4 Water 10/23/20 12:30 10/24/20 09:05
Eurofins TestAmerica, Pensacola
Page 6 of 76 11/6/2020
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-1Client Sample ID: B-1
Matrix: SolidDate Collected: 10/23/20 12:25
Percent Solids: 61.3Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 0.0397 0.0352 mg/Kg ☼10/30/20 08:43 10/30/20 14:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Benzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Bromobenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Bromochloromethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Bromodichloromethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Bromoform ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Bromomethane ND
0.0352 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼2-Butanone (MEK)ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Carbon disulfide ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Carbon tetrachloride ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Chlorobenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Chlorodibromomethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Chloroethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Chloroform ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Chloromethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼2-Chlorotoluene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼4-Chlorotoluene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼cis-1,2-Dichloroethene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼cis-1,3-Dichloropropene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,2-Dibromo-3-Chloropropane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,2-Dibromoethane (EDB)ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Dibromomethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,2-Dichlorobenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,3-Dichlorobenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,4-Dichlorobenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Dichlorodifluoromethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,1-Dichloroethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,2-Dichloroethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,1-Dichloroethene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,2-Dichloropropane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,3-Dichloropropane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼2,2-Dichloropropane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,1-Dichloropropene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Ethylbenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Hexachlorobutadiene ND
0.0352 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼2-Hexanone ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Isopropylbenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Isopropyl ether ND
0.0211 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Methylene Chloride ND
0.0352 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼4-Methyl-2-pentanone (MIBK)ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Methyl tert-butyl ether ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Naphthalene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼n-Butylbenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼N-Propylbenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼p-Isopropyltoluene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼sec-Butylbenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Styrene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼tert-Butylbenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,1,1,2-Tetrachloroethane ND
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-1Client Sample ID: B-1
Matrix: SolidDate Collected: 10/23/20 12:25
Percent Solids: 61.3Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00705 mg/Kg ☼10/30/20 08:43 10/30/20 14:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Tetrachloroethene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Toluene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼trans-1,2-Dichloroethene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼trans-1,3-Dichloropropene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,2,3-Trichlorobenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,2,4-Trichlorobenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,1,1-Trichloroethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,1,2-Trichloroethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Trichloroethene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Trichlorofluoromethane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,2,3-Trichloropropane ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,2,4-Trimethylbenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼1,3,5-Trimethylbenzene ND
0.00705 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Vinyl chloride ND
0.0141 mg/Kg 10/30/20 08:43 10/30/20 14:46 1☼Xylenes, Total ND
4-Bromofluorobenzene 97 67-130 10/30/20 08:43 10/30/20 14:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 10/30/20 08:43 10/30/20 14:46 177-127
Toluene-d8 (Surr)99 10/30/20 08:43 10/30/20 14:46 176-127
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.524 mg/Kg ☼10/30/20 14:40 11/04/20 15:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Acenaphthylene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Anthracene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Benzo[a]anthracene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Benzo[a]pyrene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Benzo[b]fluoranthene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Benzo[g,h,i]perylene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Benzo[k]fluoranthene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Bis(2-chloroethoxy)methane ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Bis(2-chloroethyl)ether ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼bis (2-chloroisopropyl) ether ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Bis(2-ethylhexyl) phthalate ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼4-Bromophenyl phenyl ether ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Butyl benzyl phthalate ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Carbazole ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼4-Chloroaniline ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼4-Chloro-3-methylphenol ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2-Chloronaphthalene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2-Chlorophenol ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼4-Chlorophenyl phenyl ether ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Chrysene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Dibenz(a,h)anthracene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Dibenzofuran ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼1,2-Dichlorobenzene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼1,3-Dichlorobenzene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼1,4-Dichlorobenzene ND
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-1Client Sample ID: B-1
Matrix: SolidDate Collected: 10/23/20 12:25
Percent Solids: 61.3Date Received: 10/24/20 09:05
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 0.524 mg/Kg ☼10/30/20 14:40 11/04/20 15:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2,4-Dichlorophenol ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Diethyl phthalate ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2,4-Dimethylphenol ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Dimethyl phthalate ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Di-n-butyl phthalate ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼4,6-Dinitro-2-methylphenol ND
1.57 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2,4-Dinitrophenol ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2,4-Dinitrotoluene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2,6-Dinitrotoluene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Di-n-octyl phthalate ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Fluoranthene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Fluorene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Hexachlorobenzene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Hexachlorobutadiene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Hexachlorocyclopentadiene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Hexachloroethane ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Indeno[1,2,3-cd]pyrene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Isophorone ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼1-Methylnaphthalene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2-Methylnaphthalene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2-Methylphenol ND
1050 ug/Kg 10/30/20 14:40 11/04/20 15:49 1☼3 & 4 Methylphenol ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Naphthalene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2-Nitroaniline ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼3-Nitroaniline ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼4-Nitroaniline ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Nitrobenzene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2-Nitrophenol ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼4-Nitrophenol ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼N-Nitrosodi-n-propylamine ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
1.05 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Pentachlorophenol ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Phenanthrene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Phenol ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼Pyrene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼1,2,4-Trichlorobenzene ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2,4,5-Trichlorophenol ND
0.524 mg/Kg 10/30/20 14:40 11/04/20 15:49 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)48 27-127 10/30/20 14:40 11/04/20 15:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)52 10/30/20 14:40 11/04/20 15:49 125-128
Nitrobenzene-d5 (Surr)50 10/30/20 14:40 11/04/20 15:49 115-136
Phenol-d5 (Surr)56 10/30/20 14:40 11/04/20 15:49 129-130
Terphenyl-d14 (Surr)72 10/30/20 14:40 11/04/20 15:49 124-146
2,4,6-Tribromophenol (Surr)50 10/30/20 14:40 11/04/20 15:49 110-150
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-1Client Sample ID: B-1
Matrix: SolidDate Collected: 10/23/20 12:25
Percent Solids: 61.3Date Received: 10/24/20 09:05
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 ND 10.8 mg/Kg ☼10/29/20 12:00 10/29/20 20:06 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)104 65-125 10/29/20 12:00 10/29/20 20:06 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 ND 7.77 mg/Kg ☼11/03/20 15:22 11/05/20 15:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)84 27-151 11/03/20 15:22 11/05/20 15:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 61.3 0.01 %10/28/20 15:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 %10/28/20 15:41 1Percent Moisture 38.7
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-2Client Sample ID: B-2
Matrix: SolidDate Collected: 10/23/20 12:47
Percent Solids: 62.2Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 0.0355 0.0316 mg/Kg ☼10/30/20 08:43 10/30/20 15:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Benzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Bromobenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Bromochloromethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Bromodichloromethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Bromoform ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Bromomethane ND
0.0316 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼2-Butanone (MEK)ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Carbon disulfide ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Carbon tetrachloride ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Chlorobenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Chlorodibromomethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Chloroethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Chloroform ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Chloromethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼2-Chlorotoluene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼4-Chlorotoluene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼cis-1,2-Dichloroethene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼cis-1,3-Dichloropropene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,2-Dibromo-3-Chloropropane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,2-Dibromoethane (EDB)ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Dibromomethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,2-Dichlorobenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,3-Dichlorobenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,4-Dichlorobenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Dichlorodifluoromethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,1-Dichloroethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,2-Dichloroethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,1-Dichloroethene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,2-Dichloropropane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,3-Dichloropropane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼2,2-Dichloropropane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,1-Dichloropropene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Ethylbenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Hexachlorobutadiene ND
0.0316 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼2-Hexanone ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Isopropylbenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Isopropyl ether ND
0.0190 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Methylene Chloride ND
0.0316 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼4-Methyl-2-pentanone (MIBK)ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Methyl tert-butyl ether ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Naphthalene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼n-Butylbenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼N-Propylbenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼p-Isopropyltoluene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼sec-Butylbenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Styrene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼tert-Butylbenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,1,1,2-Tetrachloroethane ND
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-2Client Sample ID: B-2
Matrix: SolidDate Collected: 10/23/20 12:47
Percent Solids: 62.2Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00632 mg/Kg ☼10/30/20 08:43 10/30/20 15:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Tetrachloroethene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Toluene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼trans-1,2-Dichloroethene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼trans-1,3-Dichloropropene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,2,3-Trichlorobenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,2,4-Trichlorobenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,1,1-Trichloroethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,1,2-Trichloroethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Trichloroethene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Trichlorofluoromethane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,2,3-Trichloropropane ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,2,4-Trimethylbenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼1,3,5-Trimethylbenzene ND
0.00632 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Vinyl chloride ND
0.0126 mg/Kg 10/30/20 08:43 10/30/20 15:13 1☼Xylenes, Total ND
4-Bromofluorobenzene 105 67-130 10/30/20 08:43 10/30/20 15:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 10/30/20 08:43 10/30/20 15:13 177-127
Toluene-d8 (Surr)100 10/30/20 08:43 10/30/20 15:13 176-127
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.521 mg/Kg ☼10/30/20 14:40 11/03/20 16:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Acenaphthylene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Anthracene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Benzo[a]anthracene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Benzo[a]pyrene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Benzo[b]fluoranthene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Benzo[g,h,i]perylene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Benzo[k]fluoranthene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Bis(2-chloroethoxy)methane ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Bis(2-chloroethyl)ether ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼bis (2-chloroisopropyl) ether ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Bis(2-ethylhexyl) phthalate ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼4-Bromophenyl phenyl ether ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Butyl benzyl phthalate ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Carbazole ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼4-Chloroaniline ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼4-Chloro-3-methylphenol ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2-Chloronaphthalene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2-Chlorophenol ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼4-Chlorophenyl phenyl ether ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Chrysene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Dibenz(a,h)anthracene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Dibenzofuran ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼1,2-Dichlorobenzene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼1,3-Dichlorobenzene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼1,4-Dichlorobenzene ND
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-2Client Sample ID: B-2
Matrix: SolidDate Collected: 10/23/20 12:47
Percent Solids: 62.2Date Received: 10/24/20 09:05
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 0.521 mg/Kg ☼10/30/20 14:40 11/03/20 16:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2,4-Dichlorophenol ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Diethyl phthalate ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2,4-Dimethylphenol ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Dimethyl phthalate ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Di-n-butyl phthalate ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼4,6-Dinitro-2-methylphenol ND
1.56 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2,4-Dinitrophenol ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2,4-Dinitrotoluene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2,6-Dinitrotoluene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Di-n-octyl phthalate ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Fluoranthene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Fluorene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Hexachlorobenzene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Hexachlorobutadiene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Hexachlorocyclopentadiene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Hexachloroethane ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Indeno[1,2,3-cd]pyrene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Isophorone ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼1-Methylnaphthalene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2-Methylnaphthalene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2-Methylphenol ND
1040 ug/Kg 10/30/20 14:40 11/03/20 16:45 1☼3 & 4 Methylphenol ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Naphthalene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2-Nitroaniline ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼3-Nitroaniline ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼4-Nitroaniline ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Nitrobenzene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2-Nitrophenol ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼4-Nitrophenol ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼N-Nitrosodi-n-propylamine ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
1.04 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Pentachlorophenol ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Phenanthrene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Phenol ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼Pyrene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼1,2,4-Trichlorobenzene ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2,4,5-Trichlorophenol ND
0.521 mg/Kg 10/30/20 14:40 11/03/20 16:45 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)54 27-127 10/30/20 14:40 11/03/20 16:45 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)59 10/30/20 14:40 11/03/20 16:45 125-128
Nitrobenzene-d5 (Surr)55 10/30/20 14:40 11/03/20 16:45 115-136
Phenol-d5 (Surr)64 10/30/20 14:40 11/03/20 16:45 129-130
Terphenyl-d14 (Surr)77 10/30/20 14:40 11/03/20 16:45 124-146
2,4,6-Tribromophenol (Surr)51 10/30/20 14:40 11/03/20 16:45 110-150
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-2Client Sample ID: B-2
Matrix: SolidDate Collected: 10/23/20 12:47
Percent Solids: 62.2Date Received: 10/24/20 09:05
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 ND 8.93 mg/Kg ☼10/29/20 12:00 10/29/20 20:33 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)107 65-125 10/29/20 12:00 10/29/20 20:33 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 ND 7.57 mg/Kg ☼11/03/20 15:22 11/05/20 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)76 27-151 11/03/20 15:22 11/05/20 15:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 62.2 0.01 %10/28/20 15:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 %10/28/20 15:41 1Percent Moisture 37.8
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-3Client Sample ID: B-3
Matrix: SolidDate Collected: 10/23/20 13:05
Percent Solids: 72.8Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 0.0877 0.0272 mg/Kg ☼10/30/20 08:43 10/30/20 15:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Benzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Bromobenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Bromochloromethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Bromodichloromethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Bromoform ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Bromomethane ND
0.0272 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼2-Butanone (MEK)ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Carbon disulfide ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Carbon tetrachloride ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Chlorobenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Chlorodibromomethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Chloroethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Chloroform ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Chloromethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼2-Chlorotoluene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼4-Chlorotoluene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼cis-1,2-Dichloroethene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼cis-1,3-Dichloropropene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,2-Dibromo-3-Chloropropane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,2-Dibromoethane (EDB)ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Dibromomethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,2-Dichlorobenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,3-Dichlorobenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,4-Dichlorobenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Dichlorodifluoromethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,1-Dichloroethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,2-Dichloroethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,1-Dichloroethene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,2-Dichloropropane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,3-Dichloropropane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼2,2-Dichloropropane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,1-Dichloropropene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Ethylbenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Hexachlorobutadiene ND
0.0272 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼2-Hexanone ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Isopropylbenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Isopropyl ether ND
0.0163 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Methylene Chloride ND
0.0272 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼4-Methyl-2-pentanone (MIBK)ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Methyl tert-butyl ether ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Naphthalene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼n-Butylbenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼N-Propylbenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼p-Isopropyltoluene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼sec-Butylbenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Styrene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼tert-Butylbenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,1,1,2-Tetrachloroethane ND
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-3Client Sample ID: B-3
Matrix: SolidDate Collected: 10/23/20 13:05
Percent Solids: 72.8Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00544 mg/Kg ☼10/30/20 08:43 10/30/20 15:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Tetrachloroethene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Toluene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼trans-1,2-Dichloroethene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼trans-1,3-Dichloropropene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,2,3-Trichlorobenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,2,4-Trichlorobenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,1,1-Trichloroethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,1,2-Trichloroethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Trichloroethene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Trichlorofluoromethane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,2,3-Trichloropropane ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,2,4-Trimethylbenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼1,3,5-Trimethylbenzene ND
0.00544 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Vinyl chloride ND
0.0109 mg/Kg 10/30/20 08:43 10/30/20 15:39 1☼Xylenes, Total ND
4-Bromofluorobenzene 107 67-130 10/30/20 08:43 10/30/20 15:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 10/30/20 08:43 10/30/20 15:39 177-127
Toluene-d8 (Surr)100 10/30/20 08:43 10/30/20 15:39 176-127
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.448 mg/Kg ☼10/30/20 14:40 11/03/20 17:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Acenaphthylene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Anthracene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Benzo[a]anthracene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Benzo[a]pyrene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Benzo[b]fluoranthene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Benzo[g,h,i]perylene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Benzo[k]fluoranthene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Bis(2-chloroethoxy)methane ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Bis(2-chloroethyl)ether ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼bis (2-chloroisopropyl) ether ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Bis(2-ethylhexyl) phthalate ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼4-Bromophenyl phenyl ether ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Butyl benzyl phthalate ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Carbazole ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼4-Chloroaniline ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼4-Chloro-3-methylphenol ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2-Chloronaphthalene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2-Chlorophenol ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼4-Chlorophenyl phenyl ether ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Chrysene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Dibenz(a,h)anthracene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Dibenzofuran ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼1,2-Dichlorobenzene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼1,3-Dichlorobenzene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼1,4-Dichlorobenzene ND
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-3Client Sample ID: B-3
Matrix: SolidDate Collected: 10/23/20 13:05
Percent Solids: 72.8Date Received: 10/24/20 09:05
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 0.448 mg/Kg ☼10/30/20 14:40 11/03/20 17:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2,4-Dichlorophenol ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Diethyl phthalate ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2,4-Dimethylphenol ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Dimethyl phthalate ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Di-n-butyl phthalate ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼4,6-Dinitro-2-methylphenol ND
1.34 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2,4-Dinitrophenol ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2,4-Dinitrotoluene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2,6-Dinitrotoluene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Di-n-octyl phthalate ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Fluoranthene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Fluorene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Hexachlorobenzene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Hexachlorobutadiene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Hexachlorocyclopentadiene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Hexachloroethane ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Indeno[1,2,3-cd]pyrene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Isophorone ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼1-Methylnaphthalene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2-Methylnaphthalene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2-Methylphenol ND
896 ug/Kg 10/30/20 14:40 11/03/20 17:05 1☼3 & 4 Methylphenol ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Naphthalene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2-Nitroaniline ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼3-Nitroaniline ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼4-Nitroaniline ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Nitrobenzene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2-Nitrophenol ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼4-Nitrophenol ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼N-Nitrosodi-n-propylamine ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.896 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Pentachlorophenol ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Phenanthrene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Phenol ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼Pyrene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼1,2,4-Trichlorobenzene ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2,4,5-Trichlorophenol ND
0.448 mg/Kg 10/30/20 14:40 11/03/20 17:05 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)52 27-127 10/30/20 14:40 11/03/20 17:05 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)57 10/30/20 14:40 11/03/20 17:05 125-128
Nitrobenzene-d5 (Surr)42 10/30/20 14:40 11/03/20 17:05 115-136
Phenol-d5 (Surr)60 10/30/20 14:40 11/03/20 17:05 129-130
Terphenyl-d14 (Surr)79 10/30/20 14:40 11/03/20 17:05 124-146
2,4,6-Tribromophenol (Surr)60 10/30/20 14:40 11/03/20 17:05 110-150
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-3Client Sample ID: B-3
Matrix: SolidDate Collected: 10/23/20 13:05
Percent Solids: 72.8Date Received: 10/24/20 09:05
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 ND 7.56 mg/Kg ☼10/29/20 12:00 10/29/20 21:00 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)109 65-125 10/29/20 12:00 10/29/20 21:00 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 6.71 6.56 mg/Kg ☼11/03/20 15:22 11/05/20 15:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)81 27-151 11/03/20 15:22 11/05/20 15:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 72.8 0.01 %10/28/20 15:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 %10/28/20 15:41 1Percent Moisture 27.2
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-4Client Sample ID: B-4
Matrix: SolidDate Collected: 10/23/20 13:15
Percent Solids: 75.0Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 0.0690 0.0250 mg/Kg ☼10/30/20 08:43 10/30/20 16:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Benzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Bromobenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Bromochloromethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Bromodichloromethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Bromoform ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Bromomethane ND
0.0250 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼2-Butanone (MEK)ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Carbon disulfide ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Carbon tetrachloride ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Chlorobenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Chlorodibromomethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Chloroethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Chloroform ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Chloromethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼2-Chlorotoluene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼4-Chlorotoluene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼cis-1,2-Dichloroethene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼cis-1,3-Dichloropropene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,2-Dibromo-3-Chloropropane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,2-Dibromoethane (EDB)ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Dibromomethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,2-Dichlorobenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,3-Dichlorobenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,4-Dichlorobenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Dichlorodifluoromethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,1-Dichloroethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,2-Dichloroethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,1-Dichloroethene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,2-Dichloropropane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,3-Dichloropropane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼2,2-Dichloropropane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,1-Dichloropropene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Ethylbenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Hexachlorobutadiene ND
0.0250 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼2-Hexanone ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Isopropylbenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Isopropyl ether ND
0.0150 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Methylene Chloride ND
0.0250 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼4-Methyl-2-pentanone (MIBK)ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Methyl tert-butyl ether ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Naphthalene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼n-Butylbenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼N-Propylbenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼p-Isopropyltoluene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼sec-Butylbenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Styrene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼tert-Butylbenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,1,1,2-Tetrachloroethane ND
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-4Client Sample ID: B-4
Matrix: SolidDate Collected: 10/23/20 13:15
Percent Solids: 75.0Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00499 mg/Kg ☼10/30/20 08:43 10/30/20 16:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Tetrachloroethene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Toluene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼trans-1,2-Dichloroethene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼trans-1,3-Dichloropropene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,2,3-Trichlorobenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,2,4-Trichlorobenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,1,1-Trichloroethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,1,2-Trichloroethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Trichloroethene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Trichlorofluoromethane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,2,3-Trichloropropane ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,2,4-Trimethylbenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼1,3,5-Trimethylbenzene ND
0.00499 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Vinyl chloride ND
0.00999 mg/Kg 10/30/20 08:43 10/30/20 16:06 1☼Xylenes, Total ND
4-Bromofluorobenzene 100 67-130 10/30/20 08:43 10/30/20 16:06 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)103 10/30/20 08:43 10/30/20 16:06 177-127
Toluene-d8 (Surr)99 10/30/20 08:43 10/30/20 16:06 176-127
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.431 mg/Kg ☼10/30/20 14:40 11/03/20 17:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Acenaphthylene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Anthracene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Benzo[a]anthracene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Benzo[a]pyrene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Benzo[b]fluoranthene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Benzo[g,h,i]perylene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Benzo[k]fluoranthene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Bis(2-chloroethoxy)methane ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Bis(2-chloroethyl)ether ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼bis (2-chloroisopropyl) ether ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Bis(2-ethylhexyl) phthalate ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼4-Bromophenyl phenyl ether ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Butyl benzyl phthalate ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Carbazole ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼4-Chloroaniline ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼4-Chloro-3-methylphenol ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2-Chloronaphthalene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2-Chlorophenol ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼4-Chlorophenyl phenyl ether ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Chrysene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Dibenz(a,h)anthracene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Dibenzofuran ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼1,2-Dichlorobenzene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼1,3-Dichlorobenzene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼1,4-Dichlorobenzene ND
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-4Client Sample ID: B-4
Matrix: SolidDate Collected: 10/23/20 13:15
Percent Solids: 75.0Date Received: 10/24/20 09:05
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 0.431 mg/Kg ☼10/30/20 14:40 11/03/20 17:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2,4-Dichlorophenol ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Diethyl phthalate ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2,4-Dimethylphenol ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Dimethyl phthalate ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Di-n-butyl phthalate ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼4,6-Dinitro-2-methylphenol ND
1.29 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2,4-Dinitrophenol ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2,4-Dinitrotoluene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2,6-Dinitrotoluene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Di-n-octyl phthalate ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Fluoranthene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Fluorene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Hexachlorobenzene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Hexachlorobutadiene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Hexachlorocyclopentadiene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Hexachloroethane ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Indeno[1,2,3-cd]pyrene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Isophorone ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼1-Methylnaphthalene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2-Methylnaphthalene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2-Methylphenol ND
861 ug/Kg 10/30/20 14:40 11/03/20 17:26 1☼3 & 4 Methylphenol ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Naphthalene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2-Nitroaniline ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼3-Nitroaniline ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼4-Nitroaniline ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Nitrobenzene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2-Nitrophenol ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼4-Nitrophenol ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼N-Nitrosodi-n-propylamine ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.861 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Pentachlorophenol ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Phenanthrene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Phenol ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼Pyrene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼1,2,4-Trichlorobenzene ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2,4,5-Trichlorophenol ND
0.431 mg/Kg 10/30/20 14:40 11/03/20 17:26 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)55 27-127 10/30/20 14:40 11/03/20 17:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)62 10/30/20 14:40 11/03/20 17:26 125-128
Nitrobenzene-d5 (Surr)43 10/30/20 14:40 11/03/20 17:26 115-136
Phenol-d5 (Surr)63 10/30/20 14:40 11/03/20 17:26 129-130
Terphenyl-d14 (Surr)82 10/30/20 14:40 11/03/20 17:26 124-146
2,4,6-Tribromophenol (Surr)62 10/30/20 14:40 11/03/20 17:26 110-150
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-4Client Sample ID: B-4
Matrix: SolidDate Collected: 10/23/20 13:15
Percent Solids: 75.0Date Received: 10/24/20 09:05
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 ND 6.69 mg/Kg ☼10/29/20 12:00 10/29/20 21:26 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)105 65-125 10/29/20 12:00 10/29/20 21:26 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 ND 6.58 mg/Kg ☼11/03/20 15:22 11/05/20 15:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)77 27-151 11/03/20 15:22 11/05/20 15:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 75.0 0.01 %10/28/20 15:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 %10/28/20 15:41 1Percent Moisture 25.0
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-5Client Sample ID: B-1
Matrix: WaterDate Collected: 10/23/20 11:10
Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone ND 25.0 ug/L 10/30/20 15:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 10/30/20 15:46 1BenzeneND
1.00 ug/L 10/30/20 15:46 1BromobenzeneND
1.00 ug/L 10/30/20 15:46 1BromochloromethaneND
1.00 ug/L 10/30/20 15:46 1BromodichloromethaneND
5.00 ug/L 10/30/20 15:46 1BromoformND
1.00 ug/L 10/30/20 15:46 1BromomethaneND
25.0 ug/L 10/30/20 15:46 12-Butanone (MEK)ND
1.00 ug/L 10/30/20 15:46 1Carbon disulfide ND
1.00 ug/L 10/30/20 15:46 1Carbon tetrachloride ND
1.00 ug/L 10/30/20 15:46 1ChlorobenzeneND
1.00 ug/L 10/30/20 15:46 1ChlorodibromomethaneND
1.00 ug/L 10/30/20 15:46 1ChloroethaneND
1.00 ug/L 10/30/20 15:46 1Chloroform1.20
1.00 ug/L 10/30/20 15:46 1ChloromethaneND
1.00 ug/L 10/30/20 15:46 12-Chlorotoluene ND
1.00 ug/L 10/30/20 15:46 14-Chlorotoluene ND
1.00 ug/L 10/30/20 15:46 1cis-1,2-Dichloroethene 1.02
5.00 ug/L 10/30/20 15:46 1cis-1,3-Dichloropropene ND
5.00 ug/L 10/30/20 15:46 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 10/30/20 15:46 11,2-Dibromoethane (EDB)ND
5.00 ug/L 10/30/20 15:46 1DibromomethaneND
1.00 ug/L 10/30/20 15:46 11,2-Dichlorobenzene ND
1.00 ug/L 10/30/20 15:46 11,3-Dichlorobenzene ND
1.00 ug/L 10/30/20 15:46 11,4-Dichlorobenzene ND
1.00 ug/L 10/30/20 15:46 1DichlorodifluoromethaneND
1.00 ug/L 10/30/20 15:46 11,1-Dichloroethane ND
1.00 ug/L 10/30/20 15:46 11,2-Dichloroethane ND
1.00 ug/L 10/30/20 15:46 11,1-Dichloroethene 5.20
1.00 ug/L 10/30/20 15:46 11,2-Dichloropropane ND
1.00 ug/L 10/30/20 15:46 11,3-Dichloropropane ND
1.00 ug/L 10/30/20 15:46 12,2-Dichloropropane ND
1.00 ug/L 10/30/20 15:46 11,1-Dichloropropene ND
1.00 ug/L 10/30/20 15:46 1EthylbenzeneND
5.00 ug/L 10/30/20 15:46 1HexachlorobutadieneND
25.0 ug/L 10/30/20 15:46 12-Hexanone ND *
1.00 ug/L 10/30/20 15:46 1IsopropylbenzeneND
1.00 ug/L 10/30/20 15:46 1Isopropyl ether ND
5.00 ug/L 10/30/20 15:46 1Methylene Chloride ND
25.0 ug/L 10/30/20 15:46 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 10/30/20 15:46 1Methyl tert-butyl ether ND
1.00 ug/L 10/30/20 15:46 1NaphthaleneND
1.00 ug/L 10/30/20 15:46 1n-Butylbenzene ND *
1.00 ug/L 10/30/20 15:46 1N-Propylbenzene ND
1.00 ug/L 10/30/20 15:46 1p-Isopropyltoluene ND
1.00 ug/L 10/30/20 15:46 1sec-Butylbenzene ND
1.00 ug/L 10/30/20 15:46 1StyreneND
1.00 ug/L 10/30/20 15:46 1tert-Butylbenzene ND
1.00 ug/L 10/30/20 15:46 11,1,1,2-Tetrachloroethane ND
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-5Client Sample ID: B-1
Matrix: WaterDate Collected: 10/23/20 11:10
Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 1.00 ug/L 10/30/20 15:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 10/30/20 15:46 1TetrachloroetheneND
1.00 ug/L 10/30/20 15:46 1TolueneND
1.00 ug/L 10/30/20 15:46 1trans-1,2-Dichloroethene ND
5.00 ug/L 10/30/20 15:46 1trans-1,3-Dichloropropene ND
1.00 ug/L 10/30/20 15:46 11,2,3-Trichlorobenzene ND
1.00 ug/L 10/30/20 15:46 11,2,4-Trichlorobenzene ND
1.00 ug/L 10/30/20 15:46 11,1,1-Trichloroethane ND
5.00 ug/L 10/30/20 15:46 11,1,2-Trichloroethane ND
1.00 ug/L 10/30/20 15:46 1Trichloroethene75.7
1.00 ug/L 10/30/20 15:46 1TrichlorofluoromethaneND
5.00 ug/L 10/30/20 15:46 11,2,3-Trichloropropane ND
1.00 ug/L 10/30/20 15:46 11,2,4-Trimethylbenzene ND
1.00 ug/L 10/30/20 15:46 11,3,5-Trimethylbenzene ND
1.00 ug/L 10/30/20 15:46 1Vinyl chloride ND
10.0 ug/L 10/30/20 15:46 1Xylenes, Total ND
4-Bromofluorobenzene 101 78-118 10/30/20 15:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)94 10/30/20 15:46 181-121
Toluene-d8 (Surr)111 10/30/20 15:46 180-120
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1AcenaphthyleneND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1AnthraceneND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1Benzo[a]anthracene ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1Benzo[a]pyrene ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1Benzo[b]fluoranthene ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1Benzo[g,h,i]perylene ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1Benzo[k]fluoranthene ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1Bis(2-chloroethoxy)methane ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1Bis(2-chloroethyl)ether ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1bis (2-chloroisopropyl) ether ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1Bis(2-ethylhexyl) phthalate ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 14-Bromophenyl phenyl ether ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1Butyl benzyl phthalate ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1CarbazoleND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 14-Chloroaniline ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 14-Chloro-3-methylphenol ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 12-Chloronaphthalene ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 12-Chlorophenol ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 14-Chlorophenyl phenyl ether ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1ChryseneND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1Dibenz(a,h)anthracene ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1DibenzofuranND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 11,2-Dichlorobenzene ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 11,3-Dichlorobenzene ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 11,4-Dichlorobenzene ND
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-5Client Sample ID: B-1
Matrix: WaterDate Collected: 10/23/20 11:10
Date Received: 10/24/20 09:05
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 12,4-Dichlorophenol ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1Diethyl phthalate ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 12,4-Dimethylphenol ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1Dimethyl phthalate ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1Di-n-butyl phthalate ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 14,6-Dinitro-2-methylphenol ND
39.5 ug/L 10/30/20 09:16 11/01/20 19:52 12,4-Dinitrophenol ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 12,4-Dinitrotoluene ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 12,6-Dinitrotoluene ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1Di-n-octyl phthalate ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1FluorantheneND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1FluoreneND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1HexachlorobenzeneND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1HexachlorobutadieneND
26.3 ug/L 10/30/20 09:16 11/02/20 15:30 1HexachlorocyclopentadieneND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1HexachloroethaneND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1Indeno[1,2,3-cd]pyrene ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1IsophoroneND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 11-Methylnaphthalene ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 12-Methylnaphthalene ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 12-Methylphenol ND
26.3 ug/L 10/30/20 09:16 11/01/20 19:52 13 & 4 Methylphenol ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1NaphthaleneND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 12-Nitroaniline ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 13-Nitroaniline ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 14-Nitroaniline ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1NitrobenzeneND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 12-Nitrophenol ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 14-Nitrophenol ND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1N-Nitrosodi-n-propylamine ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1n-Nitrosodiphenylamine(as
diphenylamine)
ND
26.3 ug/L 10/30/20 09:16 11/01/20 19:52 1PentachlorophenolND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1PhenanthreneND
13.2 ug/L 10/30/20 09:16 11/01/20 19:52 1PhenolND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 1PyreneND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 11,2,4-Trichlorobenzene ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 12,4,5-Trichlorophenol ND
13.2 ug/L 10/30/20 09:16 11/02/20 15:30 12,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)31 X 46-124 10/30/20 09:16 11/01/20 19:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)31 10/30/20 09:16 11/01/20 19:52 113-113
Nitrobenzene-d5 (Surr)42 10/30/20 09:16 11/01/20 19:52 136-126
Phenol-d5 (Surr)26 10/30/20 09:16 11/01/20 19:52 117-127
Terphenyl-d14 (Surr)48 10/30/20 09:16 11/01/20 19:52 144-149
2,4,6-Tribromophenol (Surr)28 10/30/20 09:16 11/01/20 19:52 126-150
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-5Client Sample ID: B-1
Matrix: WaterDate Collected: 10/23/20 11:10
Date Received: 10/24/20 09:05
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 100 ug/L 10/27/20 19:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)94 78-119 10/27/20 19:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 ND 159 ug/L 10/29/20 11:18 10/30/20 08:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)97 20-114 10/29/20 11:18 10/30/20 08:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-6Client Sample ID: B-2
Matrix: WaterDate Collected: 10/23/20 10:50
Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone ND 25.0 ug/L 10/30/20 16:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 10/30/20 16:09 1BenzeneND
1.00 ug/L 10/30/20 16:09 1BromobenzeneND
1.00 ug/L 10/30/20 16:09 1BromochloromethaneND
1.00 ug/L 10/30/20 16:09 1BromodichloromethaneND
5.00 ug/L 10/30/20 16:09 1BromoformND
1.00 ug/L 10/30/20 16:09 1BromomethaneND
25.0 ug/L 10/30/20 16:09 12-Butanone (MEK)ND
1.00 ug/L 10/30/20 16:09 1Carbon disulfide ND
1.00 ug/L 10/30/20 16:09 1Carbon tetrachloride ND
1.00 ug/L 10/30/20 16:09 1ChlorobenzeneND
1.00 ug/L 10/30/20 16:09 1ChlorodibromomethaneND
1.00 ug/L 10/30/20 16:09 1ChloroethaneND
1.00 ug/L 10/30/20 16:09 1Chloroform10.6
1.00 ug/L 10/30/20 16:09 1ChloromethaneND
1.00 ug/L 10/30/20 16:09 12-Chlorotoluene ND
1.00 ug/L 10/30/20 16:09 14-Chlorotoluene ND
1.00 ug/L 10/30/20 16:09 1cis-1,2-Dichloroethene ND
5.00 ug/L 10/30/20 16:09 1cis-1,3-Dichloropropene ND
5.00 ug/L 10/30/20 16:09 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 10/30/20 16:09 11,2-Dibromoethane (EDB)ND
5.00 ug/L 10/30/20 16:09 1DibromomethaneND
1.00 ug/L 10/30/20 16:09 11,2-Dichlorobenzene ND
1.00 ug/L 10/30/20 16:09 11,3-Dichlorobenzene ND
1.00 ug/L 10/30/20 16:09 11,4-Dichlorobenzene ND
1.00 ug/L 10/30/20 16:09 1DichlorodifluoromethaneND
1.00 ug/L 10/30/20 16:09 11,1-Dichloroethane ND
1.00 ug/L 10/30/20 16:09 11,2-Dichloroethane ND
1.00 ug/L 10/30/20 16:09 11,1-Dichloroethene ND
1.00 ug/L 10/30/20 16:09 11,2-Dichloropropane ND
1.00 ug/L 10/30/20 16:09 11,3-Dichloropropane ND
1.00 ug/L 10/30/20 16:09 12,2-Dichloropropane ND
1.00 ug/L 10/30/20 16:09 11,1-Dichloropropene ND
1.00 ug/L 10/30/20 16:09 1EthylbenzeneND
5.00 ug/L 10/30/20 16:09 1HexachlorobutadieneND
25.0 ug/L 10/30/20 16:09 12-Hexanone ND *
1.00 ug/L 10/30/20 16:09 1IsopropylbenzeneND
1.00 ug/L 10/30/20 16:09 1Isopropyl ether ND
5.00 ug/L 10/30/20 16:09 1Methylene Chloride ND
25.0 ug/L 10/30/20 16:09 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 10/30/20 16:09 1Methyl tert-butyl ether 2.44
1.00 ug/L 10/30/20 16:09 1NaphthaleneND
1.00 ug/L 10/30/20 16:09 1n-Butylbenzene ND *
1.00 ug/L 10/30/20 16:09 1N-Propylbenzene ND
1.00 ug/L 10/30/20 16:09 1p-Isopropyltoluene ND
1.00 ug/L 10/30/20 16:09 1sec-Butylbenzene ND
1.00 ug/L 10/30/20 16:09 1StyreneND
1.00 ug/L 10/30/20 16:09 1tert-Butylbenzene ND
1.00 ug/L 10/30/20 16:09 11,1,1,2-Tetrachloroethane ND
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-6Client Sample ID: B-2
Matrix: WaterDate Collected: 10/23/20 10:50
Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 1.00 ug/L 10/30/20 16:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 10/30/20 16:09 1TetrachloroetheneND
1.00 ug/L 10/30/20 16:09 1Toluene2.05
1.00 ug/L 10/30/20 16:09 1trans-1,2-Dichloroethene ND
5.00 ug/L 10/30/20 16:09 1trans-1,3-Dichloropropene ND
1.00 ug/L 10/30/20 16:09 11,2,3-Trichlorobenzene ND
1.00 ug/L 10/30/20 16:09 11,2,4-Trichlorobenzene ND
1.00 ug/L 10/30/20 16:09 11,1,1-Trichloroethane ND
5.00 ug/L 10/30/20 16:09 11,1,2-Trichloroethane ND
1.00 ug/L 10/30/20 16:09 1TrichloroetheneND
1.00 ug/L 10/30/20 16:09 1TrichlorofluoromethaneND
5.00 ug/L 10/30/20 16:09 11,2,3-Trichloropropane ND
1.00 ug/L 10/30/20 16:09 11,2,4-Trimethylbenzene ND
1.00 ug/L 10/30/20 16:09 11,3,5-Trimethylbenzene ND
1.00 ug/L 10/30/20 16:09 1Vinyl chloride ND
10.0 ug/L 10/30/20 16:09 1Xylenes, Total ND
4-Bromofluorobenzene 100 78-118 10/30/20 16:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)96 10/30/20 16:09 181-121
Toluene-d8 (Surr)113 10/30/20 16:09 180-120
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1AcenaphthyleneND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1AnthraceneND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1Benzo[a]anthracene ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1Benzo[a]pyrene ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1Benzo[b]fluoranthene ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1Benzo[g,h,i]perylene ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1Benzo[k]fluoranthene ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1Bis(2-chloroethoxy)methane ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1Bis(2-chloroethyl)ether ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1bis (2-chloroisopropyl) ether ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1Bis(2-ethylhexyl) phthalate ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 14-Bromophenyl phenyl ether ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1Butyl benzyl phthalate ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1CarbazoleND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 14-Chloroaniline ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 14-Chloro-3-methylphenol ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 12-Chloronaphthalene ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 12-Chlorophenol ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 14-Chlorophenyl phenyl ether ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1ChryseneND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1Dibenz(a,h)anthracene ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1DibenzofuranND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 11,2-Dichlorobenzene ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 11,3-Dichlorobenzene ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 11,4-Dichlorobenzene ND
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-6Client Sample ID: B-2
Matrix: WaterDate Collected: 10/23/20 10:50
Date Received: 10/24/20 09:05
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 12,4-Dichlorophenol ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1Diethyl phthalate ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 12,4-Dimethylphenol ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1Dimethyl phthalate ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1Di-n-butyl phthalate ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 14,6-Dinitro-2-methylphenol ND
29.1 ug/L 10/30/20 09:16 11/01/20 20:16 12,4-Dinitrophenol ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 12,4-Dinitrotoluene ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 12,6-Dinitrotoluene ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1Di-n-octyl phthalate ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1FluorantheneND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1FluoreneND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1HexachlorobenzeneND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1HexachlorobutadieneND
19.4 ug/L 10/30/20 09:16 11/02/20 15:51 1HexachlorocyclopentadieneND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1HexachloroethaneND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1Indeno[1,2,3-cd]pyrene ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1IsophoroneND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 11-Methylnaphthalene ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 12-Methylnaphthalene ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 12-Methylphenol ND
19.4 ug/L 10/30/20 09:16 11/01/20 20:16 13 & 4 Methylphenol ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1NaphthaleneND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 12-Nitroaniline ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 13-Nitroaniline ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 14-Nitroaniline ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1NitrobenzeneND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 12-Nitrophenol ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 14-Nitrophenol ND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1N-Nitrosodi-n-propylamine ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1n-Nitrosodiphenylamine(as
diphenylamine)
ND
19.4 ug/L 10/30/20 09:16 11/01/20 20:16 1PentachlorophenolND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1PhenanthreneND
9.70 ug/L 10/30/20 09:16 11/01/20 20:16 1PhenolND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 1PyreneND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 11,2,4-Trichlorobenzene ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 12,4,5-Trichlorophenol ND
9.70 ug/L 10/30/20 09:16 11/02/20 15:51 12,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)36 X 46-124 10/30/20 09:16 11/01/20 20:16 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)33 10/30/20 09:16 11/01/20 20:16 113-113
Nitrobenzene-d5 (Surr)50 10/30/20 09:16 11/01/20 20:16 136-126
Phenol-d5 (Surr)25 10/30/20 09:16 11/01/20 20:16 117-127
Terphenyl-d14 (Surr)57 10/30/20 09:16 11/01/20 20:16 144-149
2,4,6-Tribromophenol (Surr)35 10/30/20 09:16 11/01/20 20:16 126-150
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-6Client Sample ID: B-2
Matrix: WaterDate Collected: 10/23/20 10:50
Date Received: 10/24/20 09:05
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 100 ug/L 10/27/20 19:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)95 78-119 10/27/20 19:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 98.9 95.3 ug/L 10/29/20 11:18 10/30/20 08:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)104 20-114 10/29/20 11:18 10/30/20 08:25 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-7Client Sample ID: B-3
Matrix: WaterDate Collected: 10/23/20 11:30
Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 31.2 25.0 ug/L 10/30/20 16:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 10/30/20 16:37 1BenzeneND
1.00 ug/L 10/30/20 16:37 1BromobenzeneND
1.00 ug/L 10/30/20 16:37 1BromochloromethaneND
1.00 ug/L 10/30/20 16:37 1Bromodichloromethane1.49
5.00 ug/L 10/30/20 16:37 1BromoformND
1.00 ug/L 10/30/20 16:37 1BromomethaneND
25.0 ug/L 10/30/20 16:37 12-Butanone (MEK)ND
1.00 ug/L 10/30/20 16:37 1Carbon disulfide ND
1.00 ug/L 10/30/20 16:37 1Carbon tetrachloride ND
1.00 ug/L 10/30/20 16:37 1ChlorobenzeneND
1.00 ug/L 10/30/20 16:37 1ChlorodibromomethaneND
1.00 ug/L 10/30/20 16:37 1ChloroethaneND
1.00 ug/L 10/30/20 16:37 1Chloroform4.93
1.00 ug/L 10/30/20 16:37 1ChloromethaneND
1.00 ug/L 10/30/20 16:37 12-Chlorotoluene ND
1.00 ug/L 10/30/20 16:37 14-Chlorotoluene ND
1.00 ug/L 10/30/20 16:37 1cis-1,2-Dichloroethene ND
5.00 ug/L 10/30/20 16:37 1cis-1,3-Dichloropropene ND
5.00 ug/L 10/30/20 16:37 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 10/30/20 16:37 11,2-Dibromoethane (EDB)ND
5.00 ug/L 10/30/20 16:37 1DibromomethaneND
1.00 ug/L 10/30/20 16:37 11,2-Dichlorobenzene ND
1.00 ug/L 10/30/20 16:37 11,3-Dichlorobenzene ND
1.00 ug/L 10/30/20 16:37 11,4-Dichlorobenzene ND
1.00 ug/L 10/30/20 16:37 1DichlorodifluoromethaneND
1.00 ug/L 10/30/20 16:37 11,1-Dichloroethane ND
1.00 ug/L 10/30/20 16:37 11,2-Dichloroethane ND
1.00 ug/L 10/30/20 16:37 11,1-Dichloroethene ND
1.00 ug/L 10/30/20 16:37 11,2-Dichloropropane ND
1.00 ug/L 10/30/20 16:37 11,3-Dichloropropane ND
1.00 ug/L 10/30/20 16:37 12,2-Dichloropropane ND
1.00 ug/L 10/30/20 16:37 11,1-Dichloropropene ND
1.00 ug/L 10/30/20 16:37 1EthylbenzeneND
5.00 ug/L 10/30/20 16:37 1HexachlorobutadieneND
25.0 ug/L 10/30/20 16:37 12-Hexanone ND *
1.00 ug/L 10/30/20 16:37 1IsopropylbenzeneND
1.00 ug/L 10/30/20 16:37 1Isopropyl ether ND
5.00 ug/L 10/30/20 16:37 1Methylene Chloride ND
25.0 ug/L 10/30/20 16:37 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 10/30/20 16:37 1Methyl tert-butyl ether ND
1.00 ug/L 10/30/20 16:37 1NaphthaleneND
1.00 ug/L 10/30/20 16:37 1n-Butylbenzene ND *
1.00 ug/L 10/30/20 16:37 1N-Propylbenzene ND
1.00 ug/L 10/30/20 16:37 1p-Isopropyltoluene ND
1.00 ug/L 10/30/20 16:37 1sec-Butylbenzene ND
1.00 ug/L 10/30/20 16:37 1StyreneND
1.00 ug/L 10/30/20 16:37 1tert-Butylbenzene ND
1.00 ug/L 10/30/20 16:37 11,1,1,2-Tetrachloroethane ND
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-7Client Sample ID: B-3
Matrix: WaterDate Collected: 10/23/20 11:30
Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 1.00 ug/L 10/30/20 16:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 10/30/20 16:37 1TetrachloroetheneND
1.00 ug/L 10/30/20 16:37 1TolueneND
1.00 ug/L 10/30/20 16:37 1trans-1,2-Dichloroethene ND
5.00 ug/L 10/30/20 16:37 1trans-1,3-Dichloropropene ND
1.00 ug/L 10/30/20 16:37 11,2,3-Trichlorobenzene ND
1.00 ug/L 10/30/20 16:37 11,2,4-Trichlorobenzene ND
1.00 ug/L 10/30/20 16:37 11,1,1-Trichloroethane ND
5.00 ug/L 10/30/20 16:37 11,1,2-Trichloroethane ND
1.00 ug/L 10/30/20 16:37 1TrichloroetheneND
1.00 ug/L 10/30/20 16:37 1TrichlorofluoromethaneND
5.00 ug/L 10/30/20 16:37 11,2,3-Trichloropropane ND
1.00 ug/L 10/30/20 16:37 11,2,4-Trimethylbenzene ND
1.00 ug/L 10/30/20 16:37 11,3,5-Trimethylbenzene ND
1.00 ug/L 10/30/20 16:37 1Vinyl chloride ND
10.0 ug/L 10/30/20 16:37 1Xylenes, Total ND
4-Bromofluorobenzene 99 78-118 10/30/20 16:37 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)95 10/30/20 16:37 181-121
Toluene-d8 (Surr)112 10/30/20 16:37 180-120
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1AcenaphthyleneND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1AnthraceneND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1Benzo[a]anthracene ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1Benzo[a]pyrene ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1Benzo[b]fluoranthene ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1Benzo[g,h,i]perylene ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1Benzo[k]fluoranthene ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1Bis(2-chloroethoxy)methane ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1Bis(2-chloroethyl)ether ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1bis (2-chloroisopropyl) ether ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1Bis(2-ethylhexyl) phthalate ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 14-Bromophenyl phenyl ether ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1Butyl benzyl phthalate ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1CarbazoleND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 14-Chloroaniline ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 14-Chloro-3-methylphenol ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 12-Chloronaphthalene ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 12-Chlorophenol ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 14-Chlorophenyl phenyl ether ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1ChryseneND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1Dibenz(a,h)anthracene ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1DibenzofuranND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 11,2-Dichlorobenzene ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 11,3-Dichlorobenzene ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 11,4-Dichlorobenzene ND
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-7Client Sample ID: B-3
Matrix: WaterDate Collected: 10/23/20 11:30
Date Received: 10/24/20 09:05
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 12,4-Dichlorophenol ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1Diethyl phthalate ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 12,4-Dimethylphenol ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1Dimethyl phthalate ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1Di-n-butyl phthalate ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 14,6-Dinitro-2-methylphenol ND
31.2 ug/L 10/30/20 09:16 11/01/20 20:40 12,4-Dinitrophenol ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 12,4-Dinitrotoluene ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 12,6-Dinitrotoluene ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1Di-n-octyl phthalate ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1FluorantheneND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1FluoreneND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1HexachlorobenzeneND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1HexachlorobutadieneND
20.8 ug/L 10/30/20 09:16 11/02/20 16:12 1HexachlorocyclopentadieneND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1HexachloroethaneND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1Indeno[1,2,3-cd]pyrene ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1IsophoroneND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 11-Methylnaphthalene ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 12-Methylnaphthalene ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 12-Methylphenol ND
20.8 ug/L 10/30/20 09:16 11/01/20 20:40 13 & 4 Methylphenol ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1NaphthaleneND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 12-Nitroaniline ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 13-Nitroaniline ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 14-Nitroaniline ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1NitrobenzeneND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 12-Nitrophenol ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 14-Nitrophenol ND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1N-Nitrosodi-n-propylamine ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1n-Nitrosodiphenylamine(as
diphenylamine)
ND
20.8 ug/L 10/30/20 09:16 11/01/20 20:40 1PentachlorophenolND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1PhenanthreneND
10.4 ug/L 10/30/20 09:16 11/01/20 20:40 1PhenolND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 1PyreneND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 11,2,4-Trichlorobenzene ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 12,4,5-Trichlorophenol ND
10.4 ug/L 10/30/20 09:16 11/02/20 16:12 12,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)33 X 46-124 10/30/20 09:16 11/01/20 20:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)34 10/30/20 09:16 11/01/20 20:40 113-113
Nitrobenzene-d5 (Surr)47 10/30/20 09:16 11/01/20 20:40 136-126
Phenol-d5 (Surr)26 10/30/20 09:16 11/01/20 20:40 117-127
Terphenyl-d14 (Surr)55 10/30/20 09:16 11/01/20 20:40 144-149
2,4,6-Tribromophenol (Surr)32 10/30/20 09:16 11/01/20 20:40 126-150
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-7Client Sample ID: B-3
Matrix: WaterDate Collected: 10/23/20 11:30
Date Received: 10/24/20 09:05
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 100 ug/L 10/27/20 20:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)94 78-119 10/27/20 20:30 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 ND 135 ug/L 10/29/20 11:18 10/30/20 08:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)70 20-114 10/29/20 11:18 10/30/20 08:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-8Client Sample ID: B-4
Matrix: WaterDate Collected: 10/23/20 12:30
Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone ND 25.0 ug/L 10/30/20 17:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 10/30/20 17:05 1BenzeneND
1.00 ug/L 10/30/20 17:05 1BromobenzeneND
1.00 ug/L 10/30/20 17:05 1BromochloromethaneND
1.00 ug/L 10/30/20 17:05 1BromodichloromethaneND
5.00 ug/L 10/30/20 17:05 1BromoformND
1.00 ug/L 10/30/20 17:05 1BromomethaneND
25.0 ug/L 10/30/20 17:05 12-Butanone (MEK)ND
1.00 ug/L 10/30/20 17:05 1Carbon disulfide ND
1.00 ug/L 10/30/20 17:05 1Carbon tetrachloride ND
1.00 ug/L 10/30/20 17:05 1ChlorobenzeneND
1.00 ug/L 10/30/20 17:05 1ChlorodibromomethaneND
1.00 ug/L 10/30/20 17:05 1ChloroethaneND
1.00 ug/L 10/30/20 17:05 1Chloroform2.59
1.00 ug/L 10/30/20 17:05 1ChloromethaneND
1.00 ug/L 10/30/20 17:05 12-Chlorotoluene ND
1.00 ug/L 10/30/20 17:05 14-Chlorotoluene ND
1.00 ug/L 10/30/20 17:05 1cis-1,2-Dichloroethene ND
5.00 ug/L 10/30/20 17:05 1cis-1,3-Dichloropropene ND
5.00 ug/L 10/30/20 17:05 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 10/30/20 17:05 11,2-Dibromoethane (EDB)ND
5.00 ug/L 10/30/20 17:05 1DibromomethaneND
1.00 ug/L 10/30/20 17:05 11,2-Dichlorobenzene ND
1.00 ug/L 10/30/20 17:05 11,3-Dichlorobenzene ND
1.00 ug/L 10/30/20 17:05 11,4-Dichlorobenzene ND
1.00 ug/L 10/30/20 17:05 1DichlorodifluoromethaneND
1.00 ug/L 10/30/20 17:05 11,1-Dichloroethane ND
1.00 ug/L 10/30/20 17:05 11,2-Dichloroethane ND
1.00 ug/L 10/30/20 17:05 11,1-Dichloroethene ND
1.00 ug/L 10/30/20 17:05 11,2-Dichloropropane ND
1.00 ug/L 10/30/20 17:05 11,3-Dichloropropane ND
1.00 ug/L 10/30/20 17:05 12,2-Dichloropropane ND
1.00 ug/L 10/30/20 17:05 11,1-Dichloropropene ND
1.00 ug/L 10/30/20 17:05 1EthylbenzeneND
5.00 ug/L 10/30/20 17:05 1HexachlorobutadieneND
25.0 ug/L 10/30/20 17:05 12-Hexanone ND *
1.00 ug/L 10/30/20 17:05 1IsopropylbenzeneND
1.00 ug/L 10/30/20 17:05 1Isopropyl ether 2.03
5.00 ug/L 10/30/20 17:05 1Methylene Chloride ND
25.0 ug/L 10/30/20 17:05 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 10/30/20 17:05 1Methyl tert-butyl ether 28.7
1.00 ug/L 10/30/20 17:05 1NaphthaleneND
1.00 ug/L 10/30/20 17:05 1n-Butylbenzene ND *
1.00 ug/L 10/30/20 17:05 1N-Propylbenzene ND
1.00 ug/L 10/30/20 17:05 1p-Isopropyltoluene ND
1.00 ug/L 10/30/20 17:05 1sec-Butylbenzene ND
1.00 ug/L 10/30/20 17:05 1StyreneND
1.00 ug/L 10/30/20 17:05 1tert-Butylbenzene ND
1.00 ug/L 10/30/20 17:05 11,1,1,2-Tetrachloroethane ND
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-8Client Sample ID: B-4
Matrix: WaterDate Collected: 10/23/20 12:30
Date Received: 10/24/20 09:05
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 1.00 ug/L 10/30/20 17:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 10/30/20 17:05 1TetrachloroetheneND
1.00 ug/L 10/30/20 17:05 1Toluene4.30
1.00 ug/L 10/30/20 17:05 1trans-1,2-Dichloroethene ND
5.00 ug/L 10/30/20 17:05 1trans-1,3-Dichloropropene ND
1.00 ug/L 10/30/20 17:05 11,2,3-Trichlorobenzene ND
1.00 ug/L 10/30/20 17:05 11,2,4-Trichlorobenzene ND
1.00 ug/L 10/30/20 17:05 11,1,1-Trichloroethane ND
5.00 ug/L 10/30/20 17:05 11,1,2-Trichloroethane ND
1.00 ug/L 10/30/20 17:05 1TrichloroetheneND
1.00 ug/L 10/30/20 17:05 1TrichlorofluoromethaneND
5.00 ug/L 10/30/20 17:05 11,2,3-Trichloropropane ND
1.00 ug/L 10/30/20 17:05 11,2,4-Trimethylbenzene ND
1.00 ug/L 10/30/20 17:05 11,3,5-Trimethylbenzene ND
1.00 ug/L 10/30/20 17:05 1Vinyl chloride ND
10.0 ug/L 10/30/20 17:05 1Xylenes, Total ND
4-Bromofluorobenzene 98 78-118 10/30/20 17:05 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)96 10/30/20 17:05 181-121
Toluene-d8 (Surr)112 10/30/20 17:05 180-120
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1AcenaphthyleneND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1AnthraceneND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1Benzo[a]anthracene ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1Benzo[a]pyrene ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1Benzo[b]fluoranthene ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1Benzo[g,h,i]perylene ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1Benzo[k]fluoranthene ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1Bis(2-chloroethoxy)methane ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1Bis(2-chloroethyl)ether ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1bis (2-chloroisopropyl) ether ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1Bis(2-ethylhexyl) phthalate ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 14-Bromophenyl phenyl ether ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1Butyl benzyl phthalate ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1CarbazoleND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 14-Chloroaniline ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 14-Chloro-3-methylphenol ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 12-Chloronaphthalene ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 12-Chlorophenol ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 14-Chlorophenyl phenyl ether ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1ChryseneND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1Dibenz(a,h)anthracene ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1DibenzofuranND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 11,2-Dichlorobenzene ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 11,3-Dichlorobenzene ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 11,4-Dichlorobenzene ND
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-8Client Sample ID: B-4
Matrix: WaterDate Collected: 10/23/20 12:30
Date Received: 10/24/20 09:05
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 12,4-Dichlorophenol ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1Diethyl phthalate ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 12,4-Dimethylphenol ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1Dimethyl phthalate ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1Di-n-butyl phthalate ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 14,6-Dinitro-2-methylphenol ND
29.0 ug/L 10/30/20 09:16 11/01/20 21:04 12,4-Dinitrophenol ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 12,4-Dinitrotoluene ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 12,6-Dinitrotoluene ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1Di-n-octyl phthalate ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1FluorantheneND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1FluoreneND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1HexachlorobenzeneND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1HexachlorobutadieneND
19.3 ug/L 10/30/20 09:16 11/02/20 16:32 1HexachlorocyclopentadieneND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1HexachloroethaneND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1Indeno[1,2,3-cd]pyrene ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1IsophoroneND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 11-Methylnaphthalene ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 12-Methylnaphthalene ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 12-Methylphenol ND
19.3 ug/L 10/30/20 09:16 11/01/20 21:04 13 & 4 Methylphenol ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1NaphthaleneND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 12-Nitroaniline ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 13-Nitroaniline ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 14-Nitroaniline ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1NitrobenzeneND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 12-Nitrophenol ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 14-Nitrophenol ND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1N-Nitrosodi-n-propylamine ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1n-Nitrosodiphenylamine(as
diphenylamine)
ND
19.3 ug/L 10/30/20 09:16 11/01/20 21:04 1PentachlorophenolND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1PhenanthreneND
9.67 ug/L 10/30/20 09:16 11/01/20 21:04 1PhenolND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 1PyreneND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 11,2,4-Trichlorobenzene ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 12,4,5-Trichlorophenol ND
9.67 ug/L 10/30/20 09:16 11/02/20 16:32 12,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)39 X 46-124 10/30/20 09:16 11/01/20 21:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)36 10/30/20 09:16 11/01/20 21:04 113-113
Nitrobenzene-d5 (Surr)56 10/30/20 09:16 11/01/20 21:04 136-126
Phenol-d5 (Surr)27 10/30/20 09:16 11/01/20 21:04 117-127
Terphenyl-d14 (Surr)60 10/30/20 09:16 11/01/20 21:04 144-149
2,4,6-Tribromophenol (Surr)40 10/30/20 09:16 11/01/20 21:04 126-150
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Client Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Lab Sample ID: 400-194926-8Client Sample ID: B-4
Matrix: WaterDate Collected: 10/23/20 12:30
Date Received: 10/24/20 09:05
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 100 ug/L 10/27/20 21:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)92 78-119 10/27/20 21:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 179 95.1 ug/L 10/29/20 11:18 10/30/20 08:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)71 20-114 10/29/20 11:18 10/30/20 08:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins TestAmerica, Pensacola
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Definitions/Glossary
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Qualifiers
GC/MS VOA
Qualifier Description
*LCS or LCSD is outside acceptance limits.
Qualifier
GC/MS Semi VOA
Qualifier Description
X Surrogate recovery exceeds control limits
Qualifier
General Chemistry
Qualifier Description
F3 Duplicate RPD exceeds the control limit
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8260D - Volatile Organic Compounds by GC/MS
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (67-130)(77-127)(76-127)
BFB DBFM TOL
97 101 99400-194926-1
Percent Surrogate Recovery (Acceptance Limits)
B-1
105 102 100400-194926-2 B-2
107 100 100400-194926-3 B-3
100 103 99400-194926-4 B-4
103 98 101LCS 400-508750/1-A Lab Control Sample
100 103 102MB 400-508750/2-A Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 8260D - Volatile Organic Compounds by GC/MS
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (78-118)(81-121)(80-120)
BFB DBFM TOL
101 94 111400-194926-5
Percent Surrogate Recovery (Acceptance Limits)
B-1
100 96 113400-194926-6 B-2
99 95 112400-194926-7 B-3
98 96 112400-194926-8 B-4
101 94 112LCS 400-508707/1003 Lab Control Sample
101 94 110MB 400-508707/5 Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (27-127)(25-128)(15-136)(29-130)(24-146)(10-150)
FBP 2FP NBZ PHL TPHL TBP
48 52 50 56 72 50400-194926-1
Percent Surrogate Recovery (Acceptance Limits)
B-1
54 59 55 7764 51400-194926-2 B-2
52 57 42 7960 60400-194926-3 B-3
55 62 43 8263 62400-194926-4 B-4
84 80 74 9778 148LCS 400-508814/2-A Lab Control Sample
83 79 74 10276 149LCSD 400-508814/3-A Lab Control Sample Dup
86 88 72 10184 126MB 400-508814/1-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl (Surr)
2FP = 2-Fluorophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPHL = Terphenyl-d14 (Surr)
TBP = 2,4,6-Tribromophenol (Surr)
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (46-124)(13-113)(36-126)(17-127)(44-149)(26-150)
FBP 2FP NBZ PHL TPHL TBP
31 X 31 42 26 48 28400-194926-5
Percent Surrogate Recovery (Acceptance Limits)
B-1
36 X 33 50 5725 35400-194926-6 B-2
33 X 34 47 5526 32400-194926-7 B-3
39 X 36 56 6027 40400-194926-8 B-4
55 50 69 6642 63LCS 400-508631/2-A Lab Control Sample
57 48 70 6643 62LCSD 400-508631/3-A Lab Control Sample Dup
50 44 52 6733 54MB 400-508631/1-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl (Surr)
2FP = 2-Fluorophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPHL = Terphenyl-d14 (Surr)
TBP = 2,4,6-Tribromophenol (Surr)
Method: 8015C - Gasoline Range Organics (GRO) (GC)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (65-125)
TFT-F2
104400-194926-1
Percent Surrogate Recovery (Acceptance Limits)
B-1
107400-194926-2 B-2
109400-194926-3 B-3
105400-194926-4 B-4
107LCS 400-508723/1-A Lab Control Sample
108MB 400-508723/2-A Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
Method: 8015C - Gasoline Range Organics (GRO) (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (78-119)
TFT-F2
94400-194926-5
Percent Surrogate Recovery (Acceptance Limits)
B-1
95400-194926-6 B-2
94400-194926-7 B-3
92400-194926-8 B-4
92LCS 400-508296/1002 Lab Control Sample
93MB 400-508296/3 Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8015C - Diesel Range Organics (DRO) (GC)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (27-151)
OTPH1
84400-194926-1
Percent Surrogate Recovery (Acceptance Limits)
B-1
81400-194926-1 MS B-1
92400-194926-1 MSD B-1
76400-194926-2 B-2
81400-194926-3 B-3
77400-194926-4 B-4
92LCS 400-509198/2-A Lab Control Sample
77MB 400-509198/1-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl (Surr)
Method: 8015C - Diesel Range Organics (DRO) (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (20-114)
OTPH1
97400-194926-5
Percent Surrogate Recovery (Acceptance Limits)
B-1
104400-194926-6 B-2
70400-194926-7 B-3
71400-194926-8 B-4
104LCS 400-508534/2-A Lab Control Sample
107LCSD 400-508534/3-A Lab Control Sample Dup
98MB 400-508534/1-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl (Surr)
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
GC/MS VOA
Analysis Batch: 508704
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260D 508750400-194926-1 B-1 Total/NA
Solid 8260D 508750400-194926-2 B-2 Total/NA
Solid 8260D 508750400-194926-3 B-3 Total/NA
Solid 8260D 508750400-194926-4 B-4 Total/NA
Solid 8260D 508750MB 400-508750/2-A Method Blank Total/NA
Solid 8260D 508750LCS 400-508750/1-A Lab Control Sample Total/NA
Analysis Batch: 508707
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260D400-194926-5 B-1 Total/NA
Water 8260D400-194926-6 B-2 Total/NA
Water 8260D400-194926-7 B-3 Total/NA
Water 8260D400-194926-8 B-4 Total/NA
Water 8260DMB 400-508707/5 Method Blank Total/NA
Water 8260DLCS 400-508707/1003 Lab Control Sample Total/NA
Prep Batch: 508750
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035400-194926-1 B-1 Total/NA
Solid 5035400-194926-2 B-2 Total/NA
Solid 5035400-194926-3 B-3 Total/NA
Solid 5035400-194926-4 B-4 Total/NA
Solid 5035MB 400-508750/2-A Method Blank Total/NA
Solid 5035LCS 400-508750/1-A Lab Control Sample Total/NA
GC/MS Semi VOA
Prep Batch: 508631
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3520C400-194926-5 B-1 Total/NA
Water 3520C400-194926-6 B-2 Total/NA
Water 3520C400-194926-7 B-3 Total/NA
Water 3520C400-194926-8 B-4 Total/NA
Water 3520CMB 400-508631/1-A Method Blank Total/NA
Water 3520CLCS 400-508631/2-A Lab Control Sample Total/NA
Water 3520CLCSD 400-508631/3-A Lab Control Sample Dup Total/NA
Prep Batch: 508814
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546400-194926-1 B-1 Total/NA
Solid 3546400-194926-2 B-2 Total/NA
Solid 3546400-194926-3 B-3 Total/NA
Solid 3546400-194926-4 B-4 Total/NA
Solid 3546MB 400-508814/1-A Method Blank Total/NA
Solid 3546LCS 400-508814/2-A Lab Control Sample Total/NA
Solid 3546LCSD 400-508814/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 508916
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270E 508631MB 400-508631/1-A Method Blank Total/NA
Water 8270E 508631LCS 400-508631/2-A Lab Control Sample Total/NA
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
GC/MS Semi VOA (Continued)
Analysis Batch: 508916 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270E 508631LCSD 400-508631/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 508919
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270E 508631400-194926-5 B-1 Total/NA
Water 8270E 508631400-194926-6 B-2 Total/NA
Water 8270E 508631400-194926-7 B-3 Total/NA
Water 8270E 508631400-194926-8 B-4 Total/NA
Analysis Batch: 508980
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270E 508631400-194926-5 B-1 Total/NA
Water 8270E 508631400-194926-6 B-2 Total/NA
Water 8270E 508631400-194926-7 B-3 Total/NA
Water 8270E 508631400-194926-8 B-4 Total/NA
Analysis Batch: 509040
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 508814MB 400-508814/1-A Method Blank Total/NA
Solid 8270E 508814LCS 400-508814/2-A Lab Control Sample Total/NA
Solid 8270E 508814LCSD 400-508814/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 509157
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 508814400-194926-2 B-2 Total/NA
Solid 8270E 508814400-194926-3 B-3 Total/NA
Solid 8270E 508814400-194926-4 B-4 Total/NA
Analysis Batch: 509329
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 508814400-194926-1 B-1 Total/NA
GC VOA
Analysis Batch: 508296
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8015C400-194926-5 B-1 Total/NA
Water 8015C400-194926-6 B-2 Total/NA
Water 8015C400-194926-7 B-3 Total/NA
Water 8015C400-194926-8 B-4 Total/NA
Water 8015CMB 400-508296/3 Method Blank Total/NA
Water 8015CLCS 400-508296/1002 Lab Control Sample Total/NA
Analysis Batch: 508593
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 508723400-194926-1 B-1 Total/NA
Solid 8015C 508723400-194926-2 B-2 Total/NA
Solid 8015C 508723400-194926-3 B-3 Total/NA
Solid 8015C 508723400-194926-4 B-4 Total/NA
Solid 8015C 508723MB 400-508723/2-A Method Blank Total/NA
Solid 8015C 508723LCS 400-508723/1-A Lab Control Sample Total/NA
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
GC VOA
Prep Batch: 508723
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035400-194926-1 B-1 Total/NA
Solid 5035400-194926-2 B-2 Total/NA
Solid 5035400-194926-3 B-3 Total/NA
Solid 5035400-194926-4 B-4 Total/NA
Solid 5035MB 400-508723/2-A Method Blank Total/NA
Solid 5035LCS 400-508723/1-A Lab Control Sample Total/NA
GC Semi VOA
Prep Batch: 508534
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C400-194926-5 B-1 Total/NA
Water 3510C400-194926-6 B-2 Total/NA
Water 3510C400-194926-7 B-3 Total/NA
Water 3510C400-194926-8 B-4 Total/NA
Water 3510CMB 400-508534/1-A Method Blank Total/NA
Water 3510CLCS 400-508534/2-A Lab Control Sample Total/NA
Water 3510CLCSD 400-508534/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 508662
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8015C 508534400-194926-5 B-1 Total/NA
Water 8015C 508534400-194926-6 B-2 Total/NA
Water 8015C 508534400-194926-7 B-3 Total/NA
Water 8015C 508534400-194926-8 B-4 Total/NA
Water 8015C 508534MB 400-508534/1-A Method Blank Total/NA
Water 8015C 508534LCS 400-508534/2-A Lab Control Sample Total/NA
Water 8015C 508534LCSD 400-508534/3-A Lab Control Sample Dup Total/NA
Prep Batch: 509198
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546400-194926-1 B-1 Total/NA
Solid 3546400-194926-2 B-2 Total/NA
Solid 3546400-194926-3 B-3 Total/NA
Solid 3546400-194926-4 B-4 Total/NA
Solid 3546MB 400-509198/1-A Method Blank Total/NA
Solid 3546LCS 400-509198/2-A Lab Control Sample Total/NA
Solid 3546400-194926-1 MS B-1 Total/NA
Solid 3546400-194926-1 MSD B-1 Total/NA
Analysis Batch: 509471
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 509198400-194926-1 B-1 Total/NA
Solid 8015C 509198400-194926-2 B-2 Total/NA
Solid 8015C 509198400-194926-3 B-3 Total/NA
Solid 8015C 509198400-194926-4 B-4 Total/NA
Solid 8015C 509198MB 400-509198/1-A Method Blank Total/NA
Solid 8015C 509198LCS 400-509198/2-A Lab Control Sample Total/NA
Solid 8015C 509198400-194926-1 MS B-1 Total/NA
Solid 8015C 509198400-194926-1 MSD B-1 Total/NA
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
General Chemistry
Analysis Batch: 508464
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture400-194926-1 B-1 Total/NA
Solid Moisture400-194926-2 B-2 Total/NA
Solid Moisture400-194926-3 B-3 Total/NA
Solid Moisture400-194926-4 B-4 Total/NA
Solid Moisture400-194926-4 DU B-4 Total/NA
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 400-508707/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508707
RL MDL
Acetone ND 25.0 ug/L 10/30/20 09:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.00 ug/L 10/30/20 09:41 1Benzene
ND 1.00 ug/L 10/30/20 09:41 1Bromobenzene
ND 1.00 ug/L 10/30/20 09:41 1Bromochloromethane
ND 1.00 ug/L 10/30/20 09:41 1Bromodichloromethane
ND 5.00 ug/L 10/30/20 09:41 1Bromoform
ND 1.00 ug/L 10/30/20 09:41 1Bromomethane
ND 25.0 ug/L 10/30/20 09:41 12-Butanone (MEK)
ND 1.00 ug/L 10/30/20 09:41 1Carbon disulfide
ND 1.00 ug/L 10/30/20 09:41 1Carbon tetrachloride
ND 1.00 ug/L 10/30/20 09:41 1Chlorobenzene
ND 1.00 ug/L 10/30/20 09:41 1Chlorodibromomethane
ND 1.00 ug/L 10/30/20 09:41 1Chloroethane
ND 1.00 ug/L 10/30/20 09:41 1Chloroform
ND 1.00 ug/L 10/30/20 09:41 1Chloromethane
ND 1.00 ug/L 10/30/20 09:41 12-Chlorotoluene
ND 1.00 ug/L 10/30/20 09:41 14-Chlorotoluene
ND 1.00 ug/L 10/30/20 09:41 1cis-1,2-Dichloroethene
ND 5.00 ug/L 10/30/20 09:41 1cis-1,3-Dichloropropene
ND 5.00 ug/L 10/30/20 09:41 11,2-Dibromo-3-Chloropropane
ND 1.00 ug/L 10/30/20 09:41 11,2-Dibromoethane (EDB)
ND 5.00 ug/L 10/30/20 09:41 1Dibromomethane
ND 1.00 ug/L 10/30/20 09:41 11,2-Dichlorobenzene
ND 1.00 ug/L 10/30/20 09:41 11,3-Dichlorobenzene
ND 1.00 ug/L 10/30/20 09:41 11,4-Dichlorobenzene
ND 1.00 ug/L 10/30/20 09:41 1Dichlorodifluoromethane
ND 1.00 ug/L 10/30/20 09:41 11,1-Dichloroethane
ND 1.00 ug/L 10/30/20 09:41 11,2-Dichloroethane
ND 1.00 ug/L 10/30/20 09:41 11,1-Dichloroethene
ND 1.00 ug/L 10/30/20 09:41 11,2-Dichloropropane
ND 1.00 ug/L 10/30/20 09:41 11,3-Dichloropropane
ND 1.00 ug/L 10/30/20 09:41 12,2-Dichloropropane
ND 1.00 ug/L 10/30/20 09:41 11,1-Dichloropropene
ND 1.00 ug/L 10/30/20 09:41 1Ethylbenzene
ND 5.00 ug/L 10/30/20 09:41 1Hexachlorobutadiene
ND 25.0 ug/L 10/30/20 09:41 12-Hexanone
ND 1.00 ug/L 10/30/20 09:41 1Isopropylbenzene
ND 1.00 ug/L 10/30/20 09:41 1Isopropyl ether
ND 5.00 ug/L 10/30/20 09:41 1Methylene Chloride
ND 25.0 ug/L 10/30/20 09:41 14-Methyl-2-pentanone (MIBK)
ND 1.00 ug/L 10/30/20 09:41 1Methyl tert-butyl ether
ND 1.00 ug/L 10/30/20 09:41 1Naphthalene
ND 1.00 ug/L 10/30/20 09:41 1n-Butylbenzene
ND 1.00 ug/L 10/30/20 09:41 1N-Propylbenzene
ND 1.00 ug/L 10/30/20 09:41 1p-Isopropyltoluene
ND 1.00 ug/L 10/30/20 09:41 1sec-Butylbenzene
ND 1.00 ug/L 10/30/20 09:41 1Styrene
ND 1.00 ug/L 10/30/20 09:41 1tert-Butylbenzene
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-508707/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508707
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 10/30/20 09:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.00 ug/L 10/30/20 09:41 11,1,2,2-Tetrachloroethane
ND 1.00 ug/L 10/30/20 09:41 1Tetrachloroethene
ND 1.00 ug/L 10/30/20 09:41 1Toluene
ND 1.00 ug/L 10/30/20 09:41 1trans-1,2-Dichloroethene
ND 5.00 ug/L 10/30/20 09:41 1trans-1,3-Dichloropropene
ND 1.00 ug/L 10/30/20 09:41 11,2,3-Trichlorobenzene
ND 1.00 ug/L 10/30/20 09:41 11,2,4-Trichlorobenzene
ND 1.00 ug/L 10/30/20 09:41 11,1,1-Trichloroethane
ND 5.00 ug/L 10/30/20 09:41 11,1,2-Trichloroethane
ND 1.00 ug/L 10/30/20 09:41 1Trichloroethene
ND 1.00 ug/L 10/30/20 09:41 1Trichlorofluoromethane
ND 5.00 ug/L 10/30/20 09:41 11,2,3-Trichloropropane
ND 1.00 ug/L 10/30/20 09:41 11,2,4-Trimethylbenzene
ND 1.00 ug/L 10/30/20 09:41 11,3,5-Trimethylbenzene
ND 1.00 ug/L 10/30/20 09:41 1Vinyl chloride
ND 10.0 ug/L 10/30/20 09:41 1Xylenes, Total
4-Bromofluorobenzene 101 78-118 10/30/20 09:41 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
94 10/30/20 09:41 1Dibromofluoromethane (Surr)81-121
110 10/30/20 09:41 1Toluene-d8 (Surr)80-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508707/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508707
Acetone 200 252.5 ug/L 126 43-160
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 52.32 ug/L 105 70-130
Bromobenzene 50.0 54.09 ug/L 108 70-132
Bromochloromethane 50.0 50.86 ug/L 102 70-130
Bromodichloromethane 50.0 51.02 ug/L 102 67-133
Bromoform 50.0 54.15 ug/L 108 57-140
Bromomethane 50.0 56.64 ug/L 113 10-160
2-Butanone (MEK)200 246.5 ug/L 123 61-145
Carbon disulfide 50.0 44.43 ug/L 89 61-137
Carbon tetrachloride 50.0 44.72 ug/L 89 61-137
Chlorobenzene 50.0 57.44 ug/L 115 70-130
Chlorodibromomethane 50.0 51.98 ug/L 104 67-135
Chloroethane 50.0 47.62 ug/L 95 55-141
Chloroform 50.0 51.91 ug/L 104 69-130
Chloromethane 50.0 39.36 ug/L 79 58-137
2-Chlorotoluene 50.0 60.91 ug/L 122 70-130
4-Chlorotoluene 50.0 61.68 ug/L 123 70-130
cis-1,2-Dichloroethene 50.0 51.53 ug/L 103 68-130
cis-1,3-Dichloropropene 50.0 58.33 ug/L 117 69-132
1,2-Dibromo-3-Chloropropane 50.0 54.60 ug/L 109 54-135
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508707/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508707
1,2-Dibromoethane (EDB)50.0 55.11 ug/L 110 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Dibromomethane 50.0 50.45 ug/L 101 70-130
1,2-Dichlorobenzene 50.0 57.12 ug/L 114 67-130
1,3-Dichlorobenzene 50.0 58.02 ug/L 116 70-130
1,4-Dichlorobenzene 50.0 56.84 ug/L 114 70-130
Dichlorodifluoromethane 50.0 30.75 ug/L 62 41-146
1,1-Dichloroethane 50.0 51.49 ug/L 103 70-130
1,2-Dichloroethane 50.0 49.02 ug/L 98 69-130
1,1-Dichloroethene 50.0 45.28 ug/L 91 63-134
1,2-Dichloropropane 50.0 53.29 ug/L 107 70-130
1,3-Dichloropropane 50.0 64.36 ug/L 129 70-130
2,2-Dichloropropane 50.0 50.82 ug/L 102 52-135
1,1-Dichloropropene 50.0 52.26 ug/L 105 70-130
Ethylbenzene 50.0 59.82 ug/L 120 70-130
Hexachlorobutadiene 50.0 51.76 ug/L 104 53-140
2-Hexanone 200 275.5 *ug/L 138 65-137
Isopropylbenzene 50.0 59.56 ug/L 119 70-130
Methylene Chloride 50.0 50.59 ug/L 101 66-135
4-Methyl-2-pentanone (MIBK)200 238.9 ug/L 119 69-138
Methyl tert-butyl ether 50.0 55.98 ug/L 112 66-130
Naphthalene 50.0 56.52 ug/L 113 47-149
n-Butylbenzene 50.0 73.27 *ug/L 147 67-130
N-Propylbenzene 50.0 62.59 ug/L 125 70-130
p-Isopropyltoluene 50.0 63.96 ug/L 128 65-130
sec-Butylbenzene 50.0 64.28 ug/L 129 66-130
Styrene 50.0 56.17 ug/L 112 70-130
tert-Butylbenzene 50.0 59.48 ug/L 119 64-139
1,1,1,2-Tetrachloroethane 50.0 54.91 ug/L 110 67-131
1,1,2,2-Tetrachloroethane 50.0 63.71 ug/L 127 70-131
Tetrachloroethene 50.0 48.62 ug/L 97 65-130
Toluene 50.0 57.28 ug/L 115 70-130
trans-1,2-Dichloroethene 50.0 47.46 ug/L 95 70-130
trans-1,3-Dichloropropene 50.0 60.97 ug/L 122 63-130
1,2,3-Trichlorobenzene 50.0 49.72 ug/L 99 60-138
1,2,4-Trichlorobenzene 50.0 51.29 ug/L 103 60-140
1,1,1-Trichloroethane 50.0 47.59 ug/L 95 68-130
1,1,2-Trichloroethane 50.0 59.89 ug/L 120 70-130
Trichloroethene 50.0 47.52 ug/L 95 70-130
Trichlorofluoromethane 50.0 41.91 ug/L 84 65-138
1,2,3-Trichloropropane 50.0 58.89 ug/L 118 70-130
1,2,4-Trimethylbenzene 50.0 60.50 ug/L 121 70-130
1,3,5-Trimethylbenzene 50.0 59.37 ug/L 119 69-130
Vinyl chloride 50.0 43.41 ug/L 87 59-136
Xylenes, Total 100 114.1 ug/L 114 70-130
4-Bromofluorobenzene 78 -118
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
94Dibromofluoromethane (Surr)81 -121
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508707/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508707
Toluene-d8 (Surr)80 -120
Surrogate
112
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 400-508750/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 508704 Prep Batch: 508750
RL MDL
Acetone ND 0.0250 mg/Kg 10/30/20 08:43 10/30/20 11:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Benzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Bromobenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Bromochloromethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Bromodichloromethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Bromoform
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Bromomethane
ND 0.0250 mg/Kg 10/30/20 08:43 10/30/20 11:14 12-Butanone (MEK)
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Carbon disulfide
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Carbon tetrachloride
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Chlorobenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Chlorodibromomethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Chloroethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Chloroform
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Chloromethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 12-Chlorotoluene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 14-Chlorotoluene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1cis-1,2-Dichloroethene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1cis-1,3-Dichloropropene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,2-Dibromo-3-Chloropropane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,2-Dibromoethane (EDB)
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Dibromomethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,2-Dichlorobenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,3-Dichlorobenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,4-Dichlorobenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Dichlorodifluoromethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,1-Dichloroethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,2-Dichloroethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,1-Dichloroethene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,2-Dichloropropane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,3-Dichloropropane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 12,2-Dichloropropane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,1-Dichloropropene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Ethylbenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Hexachlorobutadiene
ND 0.0250 mg/Kg 10/30/20 08:43 10/30/20 11:14 12-Hexanone
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Isopropylbenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Isopropyl ether
ND 0.0150 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Methylene Chloride
ND 0.0250 mg/Kg 10/30/20 08:43 10/30/20 11:14 14-Methyl-2-pentanone (MIBK)
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Methyl tert-butyl ether
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-508750/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 508704 Prep Batch: 508750
RL MDL
Naphthalene ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1n-Butylbenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1N-Propylbenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1p-Isopropyltoluene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1sec-Butylbenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Styrene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1tert-Butylbenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,1,1,2-Tetrachloroethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,1,2,2-Tetrachloroethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Tetrachloroethene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Toluene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1trans-1,2-Dichloroethene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1trans-1,3-Dichloropropene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,2,3-Trichlorobenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,2,4-Trichlorobenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,1,1-Trichloroethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,1,2-Trichloroethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Trichloroethene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Trichlorofluoromethane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,2,3-Trichloropropane
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,2,4-Trimethylbenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 11,3,5-Trimethylbenzene
ND 0.00500 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Vinyl chloride
ND 0.0100 mg/Kg 10/30/20 08:43 10/30/20 11:14 1Xylenes, Total
4-Bromofluorobenzene 100 67-130 10/30/20 11:14 1
MB MB
Surrogate
10/30/20 08:43
Dil FacPreparedAnalyzedQualifierLimits%Recovery
103 10/30/20 08:43 10/30/20 11:14 1Dibromofluoromethane (Surr)77-127
102 10/30/20 08:43 10/30/20 11:14 1Toluene-d8 (Surr)76-127
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508750/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 508704 Prep Batch: 508750
Acetone 0.200 0.2252 mg/Kg 113 48-160
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.04187 mg/Kg 84 65-130
Bromobenzene 0.0500 0.04419 mg/Kg 88 65-130
Bromochloromethane 0.0500 0.04554 mg/Kg 91 65-130
Bromodichloromethane 0.0500 0.04247 mg/Kg 85 61-130
Bromoform 0.0500 0.05809 mg/Kg 116 52-136
Bromomethane 0.0500 0.04885 mg/Kg 98 12-160
2-Butanone (MEK)0.200 0.2038 mg/Kg 102 55-130
Carbon disulfide 0.0500 0.04126 mg/Kg 83 46-141
Carbon tetrachloride 0.0500 0.04376 mg/Kg 88 60-130
Chlorobenzene 0.0500 0.04311 mg/Kg 86 70-130
Chlorodibromomethane 0.0500 0.04862 mg/Kg 97 58-132
Chloroethane 0.0500 0.04624 mg/Kg 92 55-134
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508750/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 508704 Prep Batch: 508750
Chloroform 0.0500 0.04231 mg/Kg 85 62-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Chloromethane 0.0500 0.05780 mg/Kg 116 49-136
2-Chlorotoluene 0.0500 0.04754 mg/Kg 95 67-130
4-Chlorotoluene 0.0500 0.04805 mg/Kg 96 66-130
cis-1,2-Dichloroethene 0.0500 0.04413 mg/Kg 88 53-135
cis-1,3-Dichloropropene 0.0500 0.04112 mg/Kg 82 61-130
1,2-Dibromo-3-Chloropropane 0.0500 0.05318 mg/Kg 106 49-130
1,2-Dibromoethane (EDB)0.0500 0.04728 mg/Kg 95 67-130
Dibromomethane 0.0500 0.04337 mg/Kg 87 65-130
1,2-Dichlorobenzene 0.0500 0.04611 mg/Kg 92 64-130
1,3-Dichlorobenzene 0.0500 0.04570 mg/Kg 91 66-130
1,4-Dichlorobenzene 0.0500 0.04646 mg/Kg 93 65-130
Dichlorodifluoromethane 0.0500 0.04524 mg/Kg 90 34-143
1,1-Dichloroethane 0.0500 0.04301 mg/Kg 86 59-130
1,2-Dichloroethane 0.0500 0.04270 mg/Kg 85 62-130
1,1-Dichloroethene 0.0500 0.04211 mg/Kg 84 55-137
1,2-Dichloropropane 0.0500 0.04303 mg/Kg 86 64-130
1,3-Dichloropropane 0.0500 0.04644 mg/Kg 93 67-130
2,2-Dichloropropane 0.0500 0.04166 mg/Kg 83 51-132
1,1-Dichloropropene 0.0500 0.03961 mg/Kg 79 65-130
Ethylbenzene 0.0500 0.04206 mg/Kg 84 70-130
Hexachlorobutadiene 0.0500 0.05013 mg/Kg 100 62-133
2-Hexanone 0.200 0.2203 mg/Kg 110 57-131
Isopropylbenzene 0.0500 0.04162 mg/Kg 83 70-130
Methylene Chloride 0.0500 0.04450 mg/Kg 89 57-132
4-Methyl-2-pentanone (MIBK)0.200 0.2055 mg/Kg 103 58-130
Methyl tert-butyl ether 0.0500 0.04741 mg/Kg 95 63-130
Naphthalene 0.0500 0.04197 mg/Kg 84 45-144
n-Butylbenzene 0.0500 0.04824 mg/Kg 96 66-130
N-Propylbenzene 0.0500 0.04587 mg/Kg 92 67-130
p-Isopropyltoluene 0.0500 0.04493 mg/Kg 90 68-130
sec-Butylbenzene 0.0500 0.04374 mg/Kg 87 67-130
Styrene 0.0500 0.04521 mg/Kg 90 68-130
tert-Butylbenzene 0.0500 0.04396 mg/Kg 88 67-130
1,1,1,2-Tetrachloroethane 0.0500 0.04615 mg/Kg 92 65-130
1,1,2,2-Tetrachloroethane 0.0500 0.05186 mg/Kg 104 60-131
Tetrachloroethene 0.0500 0.04106 mg/Kg 82 67-130
Toluene 0.0500 0.04463 mg/Kg 89 70-130
trans-1,2-Dichloroethene 0.0500 0.04259 mg/Kg 85 58-134
trans-1,3-Dichloropropene 0.0500 0.04522 mg/Kg 90 60-130
1,2,3-Trichlorobenzene 0.0500 0.04362 mg/Kg 87 58-135
1,2,4-Trichlorobenzene 0.0500 0.04369 mg/Kg 87 56-138
1,1,1-Trichloroethane 0.0500 0.04328 mg/Kg 87 63-130
1,1,2-Trichloroethane 0.0500 0.04577 mg/Kg 92 65-130
Trichloroethene 0.0500 0.03929 mg/Kg 79 65-130
Trichlorofluoromethane 0.0500 0.04551 mg/Kg 91 61-136
1,2,3-Trichloropropane 0.0500 0.05448 mg/Kg 109 60-130
1,2,4-Trimethylbenzene 0.0500 0.04574 mg/Kg 91 66-130
1,3,5-Trimethylbenzene 0.0500 0.04567 mg/Kg 91 67-130
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508750/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 508704 Prep Batch: 508750
Vinyl chloride 0.0500 0.05223 mg/Kg 104 52-132
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Xylenes, Total 0.100 0.08489 mg/Kg 85 70-130
4-Bromofluorobenzene 67 -130
Surrogate
103
LCS LCS
Qualifier Limits%Recovery
98Dibromofluoromethane (Surr)77 -127
101Toluene-d8 (Surr)76 -127
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 400-508631/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508916 Prep Batch: 508631
RL MDL
Acenaphthene ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Acenaphthylene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Anthracene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Benzo[a]anthracene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Benzo[a]pyrene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Benzo[b]fluoranthene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Benzo[g,h,i]perylene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Benzo[k]fluoranthene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Bis(2-chloroethoxy)methane
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Bis(2-chloroethyl)ether
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1bis (2-chloroisopropyl) ether
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Bis(2-ethylhexyl) phthalate
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 14-Bromophenyl phenyl ether
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Butyl benzyl phthalate
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Carbazole
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 14-Chloroaniline
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 14-Chloro-3-methylphenol
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 12-Chloronaphthalene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 12-Chlorophenol
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 14-Chlorophenyl phenyl ether
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Chrysene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Dibenz(a,h)anthracene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Dibenzofuran
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 11,2-Dichlorobenzene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 11,3-Dichlorobenzene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 11,4-Dichlorobenzene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 13,3'-Dichlorobenzidine
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 12,4-Dichlorophenol
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Diethyl phthalate
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 12,4-Dimethylphenol
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Dimethyl phthalate
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Di-n-butyl phthalate
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 14,6-Dinitro-2-methylphenol
ND 30.0 ug/L 10/29/20 13:40 11/01/20 13:38 12,4-Dinitrophenol
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-508631/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508916 Prep Batch: 508631
RL MDL
2,4-Dinitrotoluene ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 12,6-Dinitrotoluene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Di-n-octyl phthalate
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Fluoranthene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Fluorene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Hexachlorobenzene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Hexachlorobutadiene
ND 20.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Hexachlorocyclopentadiene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Hexachloroethane
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Indeno[1,2,3-cd]pyrene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Isophorone
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 11-Methylnaphthalene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 12-Methylnaphthalene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 12-Methylphenol
ND 20.0 ug/L 10/29/20 13:40 11/01/20 13:38 13 & 4 Methylphenol
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Naphthalene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 12-Nitroaniline
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 13-Nitroaniline
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 14-Nitroaniline
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Nitrobenzene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 12-Nitrophenol
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 14-Nitrophenol
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1N-Nitrosodi-n-propylamine
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1n-Nitrosodiphenylamine(as
diphenylamine)
ND 20.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Pentachlorophenol
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Phenanthrene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Phenol
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 1Pyrene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 11,2,4-Trichlorobenzene
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 12,4,5-Trichlorophenol
ND 10.0 ug/L 10/29/20 13:40 11/01/20 13:38 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)50 46-124 11/01/20 13:38 1
MB MB
Surrogate
10/29/20 13:40
Dil FacPreparedAnalyzedQualifierLimits%Recovery
44 10/29/20 13:40 11/01/20 13:38 12-Fluorophenol (Surr)13-113
52 10/29/20 13:40 11/01/20 13:38 1Nitrobenzene-d5 (Surr)36-126
33 10/29/20 13:40 11/01/20 13:38 1Phenol-d5 (Surr)17-127
67 10/29/20 13:40 11/01/20 13:38 1Terphenyl-d14 (Surr)44-149
54 10/29/20 13:40 11/01/20 13:38 12,4,6-Tribromophenol (Surr)26-150
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508631/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508916 Prep Batch: 508631
Acenaphthene 120 69.08 ug/L 58 54-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 120 76.06 ug/L 63 44-130
Anthracene 120 81.02 ug/L 68 61-120
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508631/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508916 Prep Batch: 508631
Benzo[a]anthracene 120 82.61 ug/L 69 59-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzo[a]pyrene 120 77.13 ug/L 64 52-126
Benzo[b]fluoranthene 120 82.21 ug/L 69 33-149
Benzo[g,h,i]perylene 120 85.23 ug/L 71 38-150
Benzo[k]fluoranthene 120 75.53 ug/L 63 51-130
Bis(2-chloroethoxy)methane 120 67.50 ug/L 56 47-120
Bis(2-chloroethyl)ether 120 71.61 ug/L 60 44-120
bis (2-chloroisopropyl) ether 120 74.86 ug/L 62 33-121
Bis(2-ethylhexyl) phthalate 120 77.79 ug/L 65 52-147
4-Bromophenyl phenyl ether 120 79.33 ug/L 66 54-122
Butyl benzyl phthalate 120 85.64 ug/L 71 54-133
Carbazole 120 97.65 ug/L 81 54-142
4-Chloroaniline 120 72.42 ug/L 60 26-120
4-Chloro-3-methylphenol 120 82.93 ug/L 69 48-131
2-Chloronaphthalene 120 68.09 ug/L 57 52-121
2-Chlorophenol 120 77.22 ug/L 64 40-120
4-Chlorophenyl phenyl ether 120 76.58 ug/L 64 56-125
Chrysene 120 76.70 ug/L 64 61-121
Dibenz(a,h)anthracene 120 79.29 ug/L 66 40-150
Dibenzofuran 120 71.52 ug/L 60 56-122
1,2-Dichlorobenzene 120 71.81 ug/L 60 46-120
1,3-Dichlorobenzene 120 67.48 ug/L 56 44-120
1,4-Dichlorobenzene 120 72.37 ug/L 60 45-130
3,3'-Dichlorobenzidine 160 138.9 ug/L 87 36-132
2,4-Dichlorophenol 120 79.27 ug/L 66 49-120
Diethyl phthalate 120 85.34 ug/L 71 50-137
2,4-Dimethylphenol 120 73.00 ug/L 61 48-120
Dimethyl phthalate 120 77.59 ug/L 65 57-124
Di-n-butyl phthalate 120 81.13 ug/L 68 58-126
4,6-Dinitro-2-methylphenol 240 166.6 ug/L 69 23-148
2,4-Dinitrophenol 240 179.5 ug/L 75 10-150
2,4-Dinitrotoluene 120 78.14 ug/L 65 54-142
2,6-Dinitrotoluene 120 74.91 ug/L 62 55-130
Di-n-octyl phthalate 120 94.91 ug/L 79 57-138
Fluoranthene 120 84.99 ug/L 71 56-128
Fluorene 120 77.63 ug/L 65 54-124
Hexachlorobenzene 120 77.76 ug/L 65 52-129
Hexachlorobutadiene 120 78.83 ug/L 66 20-120
Hexachlorocyclopentadiene 120 40.93 ug/L 34 10-134
Hexachloroethane 120 79.11 ug/L 66 20-120
Indeno[1,2,3-cd]pyrene 120 85.00 ug/L 71 41-150
Isophorone 120 78.76 ug/L 66 48-120
1-Methylnaphthalene 120 75.22 ug/L 63 50-120
2-Methylnaphthalene 120 75.34 ug/L 63 50-121
2-Methylphenol 120 86.90 ug/L 72 46-124
3 & 4 Methylphenol 120 80.74 ug/L 67 45-120
Naphthalene 120 73.33 ug/L 61 48-120
2-Nitroaniline 120 73.89 ug/L 62 51-145
3-Nitroaniline 120 91.23 ug/L 76 37-127
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508631/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508916 Prep Batch: 508631
4-Nitroaniline 120 81.59 ug/L 68 36-137
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Nitrobenzene 120 70.29 ug/L 59 45-120
2-Nitrophenol 120 71.86 ug/L 60 40-124
4-Nitrophenol 240 121.1 ug/L 50 23-146
N-Nitrosodi-n-propylamine 120 79.96 ug/L 67 45-120
n-Nitrosodiphenylamine(as
diphenylamine)
119 76.34 ug/L 64 54-120
Pentachlorophenol 240 124.0 ug/L 52 31-130
Phenanthrene 120 77.81 ug/L 65 61-120
Phenol 120 58.12 ug/L 48 11-120
Pyrene 120 69.67 ug/L 58 53-128
1,2,4-Trichlorobenzene 120 70.68 ug/L 59 47-120
2,4,5-Trichlorophenol 120 74.58 ug/L 62 51-136
2,4,6-Trichlorophenol 120 74.57 ug/L 62 50-127
2-Fluorobiphenyl (Surr)46 -124
Surrogate
55
LCS LCS
Qualifier Limits%Recovery
502-Fluorophenol (Surr)13 -113
69Nitrobenzene-d5 (Surr)36 -126
42Phenol-d5 (Surr)17 -127
66Terphenyl-d14 (Surr)44 -149
632,4,6-Tribromophenol (Surr)26 -150
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-508631/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508916 Prep Batch: 508631
Acenaphthene 120 73.65 ug/L 61 54-125 6 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 120 80.55 ug/L 67 44-130 6 30
Anthracene 120 85.53 ug/L 71 61-120 5 30
Benzo[a]anthracene 120 87.90 ug/L 73 59-120 6 30
Benzo[a]pyrene 120 83.80 ug/L 70 52-126 8 30
Benzo[b]fluoranthene 120 88.35 ug/L 74 33-149 7 30
Benzo[g,h,i]perylene 120 92.29 ug/L 77 38-150 8 30
Benzo[k]fluoranthene 120 82.38 ug/L 69 51-130 9 30
Bis(2-chloroethoxy)methane 120 71.71 ug/L 60 47-120 6 30
Bis(2-chloroethyl)ether 120 75.87 ug/L 63 44-120 6 30
bis (2-chloroisopropyl) ether 120 78.92 ug/L 66 33-121 5 30
Bis(2-ethylhexyl) phthalate 120 83.46 ug/L 70 52-147 7 30
4-Bromophenyl phenyl ether 120 85.29 ug/L 71 54-122 7 30
Butyl benzyl phthalate 120 91.48 ug/L 76 54-133 7 30
Carbazole 120 104.8 ug/L 87 54-142 7 30
4-Chloroaniline 120 74.33 ug/L 62 26-120 3 30
4-Chloro-3-methylphenol 120 86.37 ug/L 72 48-131 4 30
2-Chloronaphthalene 120 73.11 ug/L 61 52-121 7 30
2-Chlorophenol 120 82.23 ug/L 69 40-120 6 30
4-Chlorophenyl phenyl ether 120 80.40 ug/L 67 56-125 5 30
Chrysene 120 82.76 ug/L 69 61-121 8 30
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-508631/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508916 Prep Batch: 508631
Dibenz(a,h)anthracene 120 86.95 ug/L 72 40-150 9 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Dibenzofuran 120 74.99 ug/L 62 56-122 5 30
1,2-Dichlorobenzene 120 75.81 ug/L 63 46-120 5 30
1,3-Dichlorobenzene 120 72.08 ug/L 60 44-120 7 30
1,4-Dichlorobenzene 120 77.12 ug/L 64 45-130 6 30
3,3'-Dichlorobenzidine 160 151.6 ug/L 95 36-132 9 30
2,4-Dichlorophenol 120 84.13 ug/L 70 49-120 6 30
Diethyl phthalate 120 89.33 ug/L 74 50-137 5 30
2,4-Dimethylphenol 120 79.84 ug/L 67 48-120 9 30
Dimethyl phthalate 120 82.56 ug/L 69 57-124 6 30
Di-n-butyl phthalate 120 85.59 ug/L 71 58-126 5 30
4,6-Dinitro-2-methylphenol 240 186.5 ug/L 78 23-148 11 30
2,4-Dinitrophenol 240 197.6 ug/L 82 10-150 10 30
2,4-Dinitrotoluene 120 82.78 ug/L 69 54-142 6 30
2,6-Dinitrotoluene 120 80.39 ug/L 67 55-130 7 30
Di-n-octyl phthalate 120 100.5 ug/L 84 57-138 6 30
Fluoranthene 120 90.71 ug/L 76 56-128 7 30
Fluorene 120 80.88 ug/L 67 54-124 4 30
Hexachlorobenzene 120 82.00 ug/L 68 52-129 5 30
Hexachlorobutadiene 120 83.51 ug/L 70 20-120 6 30
Hexachlorocyclopentadiene 120 50.69 ug/L 42 10-134 21 30
Hexachloroethane 120 83.75 ug/L 70 20-120 6 30
Indeno[1,2,3-cd]pyrene 120 91.46 ug/L 76 41-150 7 30
Isophorone 120 82.46 ug/L 69 48-120 5 30
1-Methylnaphthalene 120 77.57 ug/L 65 50-120 3 30
2-Methylnaphthalene 120 78.88 ug/L 66 50-121 5 30
2-Methylphenol 120 91.54 ug/L 76 46-124 5 30
3 & 4 Methylphenol 120 84.49 ug/L 70 45-120 5 30
Naphthalene 120 76.85 ug/L 64 48-120 5 30
2-Nitroaniline 120 80.50 ug/L 67 51-145 9 30
3-Nitroaniline 120 96.58 ug/L 80 37-127 6 30
4-Nitroaniline 120 90.34 ug/L 75 36-137 10 30
Nitrobenzene 120 75.76 ug/L 63 45-120 7 30
2-Nitrophenol 120 75.94 ug/L 63 40-124 6 30
4-Nitrophenol 240 133.7 ug/L 56 23-146 10 30
N-Nitrosodi-n-propylamine 120 84.41 ug/L 70 45-120 5 30
n-Nitrosodiphenylamine(as
diphenylamine)
119 82.28 ug/L 69 54-120 7 30
Pentachlorophenol 240 132.6 ug/L 55 31-130 7 30
Phenanthrene 120 83.18 ug/L 69 61-120 7 30
Phenol 120 48.27 ug/L 40 11-120 19 30
Pyrene 120 75.36 ug/L 63 53-128 8 30
1,2,4-Trichlorobenzene 120 74.81 ug/L 62 47-120 6 30
2,4,5-Trichlorophenol 120 80.01 ug/L 67 51-136 7 30
2,4,6-Trichlorophenol 120 78.52 ug/L 65 50-127 5 30
2-Fluorobiphenyl (Surr)46 -124
Surrogate
57
LCSD LCSD
Qualifier Limits%Recovery
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-508631/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508916 Prep Batch: 508631
2-Fluorophenol (Surr)13 -113
Surrogate
48
LCSD LCSD
Qualifier Limits%Recovery
70Nitrobenzene-d5 (Surr)36 -126
43Phenol-d5 (Surr)17 -127
66Terphenyl-d14 (Surr)44 -149
622,4,6-Tribromophenol (Surr)26 -150
Client Sample ID: Method BlankLab Sample ID: MB 400-508814/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509040 Prep Batch: 508814
RL MDL
Acenaphthene ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Acenaphthylene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Anthracene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Benzo[a]anthracene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Benzo[a]pyrene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Benzo[b]fluoranthene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Benzo[g,h,i]perylene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Benzo[k]fluoranthene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Bis(2-chloroethoxy)methane
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Bis(2-chloroethyl)ether
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1bis (2-chloroisopropyl) ether
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Bis(2-ethylhexyl) phthalate
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 14-Bromophenyl phenyl ether
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Butyl benzyl phthalate
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Carbazole
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 14-Chloroaniline
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 14-Chloro-3-methylphenol
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12-Chloronaphthalene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12-Chlorophenol
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 14-Chlorophenyl phenyl ether
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Chrysene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Dibenz(a,h)anthracene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Dibenzofuran
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 11,2-Dichlorobenzene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 11,3-Dichlorobenzene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 11,4-Dichlorobenzene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 13,3'-Dichlorobenzidine
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12,4-Dichlorophenol
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Diethyl phthalate
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12,4-Dimethylphenol
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Dimethyl phthalate
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Di-n-butyl phthalate
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 14,6-Dinitro-2-methylphenol
ND 0.990 mg/Kg 10/30/20 14:40 11/03/20 21:16 12,4-Dinitrophenol
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12,4-Dinitrotoluene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12,6-Dinitrotoluene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Di-n-octyl phthalate
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-508814/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509040 Prep Batch: 508814
RL MDL
Fluoranthene ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Fluorene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Hexachlorobenzene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Hexachlorobutadiene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Hexachlorocyclopentadiene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Hexachloroethane
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Indeno[1,2,3-cd]pyrene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Isophorone
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 11-Methylnaphthalene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12-Methylnaphthalene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12-Methylphenol
ND 660 ug/Kg 10/30/20 14:40 11/03/20 21:16 13 & 4 Methylphenol
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Naphthalene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12-Nitroaniline
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 13-Nitroaniline
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 14-Nitroaniline
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Nitrobenzene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12-Nitrophenol
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 14-Nitrophenol
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1N-Nitrosodi-n-propylamine
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1n-Nitrosodiphenylamine(as
diphenylamine)
ND 0.660 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Pentachlorophenol
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Phenanthrene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Phenol
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 1Pyrene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 11,2,4-Trichlorobenzene
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12,4,5-Trichlorophenol
ND 0.330 mg/Kg 10/30/20 14:40 11/03/20 21:16 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)86 27-127 11/03/20 21:16 1
MB MB
Surrogate
10/30/20 14:40
Dil FacPreparedAnalyzedQualifierLimits%Recovery
88 10/30/20 14:40 11/03/20 21:16 12-Fluorophenol (Surr)25-128
72 10/30/20 14:40 11/03/20 21:16 1Nitrobenzene-d5 (Surr)15-136
84 10/30/20 14:40 11/03/20 21:16 1Phenol-d5 (Surr)29-130
101 10/30/20 14:40 11/03/20 21:16 1Terphenyl-d14 (Surr)24-146
126 10/30/20 14:40 11/03/20 21:16 12,4,6-Tribromophenol (Surr)10-150
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508814/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509040 Prep Batch: 508814
Acenaphthene 2.00 1.580 mg/Kg 79 50-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 2.00 1.651 mg/Kg 83 50-120
Anthracene 2.00 1.755 mg/Kg 88 52-120
Benzo[a]anthracene 2.00 1.672 mg/Kg 84 55-120
Benzo[a]pyrene 2.00 1.719 mg/Kg 86 54-120
Benzo[b]fluoranthene 2.00 1.635 mg/Kg 82 55-120
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508814/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509040 Prep Batch: 508814
Benzo[g,h,i]perylene 2.00 1.772 mg/Kg 89 45-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzo[k]fluoranthene 2.00 1.778 mg/Kg 89 52-120
Bis(2-chloroethoxy)methane 2.00 1.474 mg/Kg 74 52-120
Bis(2-chloroethyl)ether 2.00 1.264 mg/Kg 63 50-120
bis (2-chloroisopropyl) ether 2.00 1.120 mg/Kg 56 34-120
Bis(2-ethylhexyl) phthalate 2.00 1.608 mg/Kg 80 58-158
4-Bromophenyl phenyl ether 2.00 2.030 mg/Kg 102 51-120
Butyl benzyl phthalate 2.00 1.496 mg/Kg 75 58-126
Carbazole 2.00 1.997 mg/Kg 100 61-132
4-Chloroaniline 2.00 1.387 mg/Kg 69 34-120
4-Chloro-3-methylphenol 2.00 1.809 mg/Kg 90 57-124
2-Chloronaphthalene 2.00 1.660 mg/Kg 83 55-120
2-Chlorophenol 2.00 1.545 mg/Kg 77 52-120
4-Chlorophenyl phenyl ether 2.00 1.935 mg/Kg 97 56-120
Chrysene 2.00 1.702 mg/Kg 85 54-120
Dibenz(a,h)anthracene 2.00 1.954 mg/Kg 98 49-120
Dibenzofuran 2.00 1.730 mg/Kg 87 58-120
1,2-Dichlorobenzene 2.00 1.452 mg/Kg 73 49-120
1,3-Dichlorobenzene 2.00 1.423 mg/Kg 71 48-120
1,4-Dichlorobenzene 2.00 1.404 mg/Kg 70 49-120
3,3'-Dichlorobenzidine 2.67 2.304 mg/Kg 86 42-120
2,4-Dichlorophenol 2.00 1.765 mg/Kg 88 56-120
Diethyl phthalate 2.00 1.720 mg/Kg 86 56-128
2,4-Dimethylphenol 2.00 1.635 mg/Kg 82 54-120
Dimethyl phthalate 2.00 1.758 mg/Kg 88 58-120
Di-n-butyl phthalate 2.00 1.881 mg/Kg 94 64-122
4,6-Dinitro-2-methylphenol 4.00 3.334 mg/Kg 83 35-135
2,4-Dinitrophenol 4.00 2.695 mg/Kg 67 10-138
2,4-Dinitrotoluene 2.00 2.001 mg/Kg 100 59-133
2,6-Dinitrotoluene 2.00 1.873 mg/Kg 94 57-123
Di-n-octyl phthalate 2.00 1.726 mg/Kg 86 57-137
Fluoranthene 2.00 2.002 mg/Kg 100 49-120
Fluorene 2.00 1.659 mg/Kg 83 47-120
Hexachlorobenzene 2.00 2.323 mg/Kg 116 49-127
Hexachlorobutadiene 2.00 1.741 mg/Kg 87 43-120
Hexachlorocyclopentadiene 2.00 1.556 mg/Kg 78 10-140
Hexachloroethane 2.00 1.356 mg/Kg 68 45-120
Indeno[1,2,3-cd]pyrene 2.00 1.887 mg/Kg 94 47-120
Isophorone 2.00 1.460 mg/Kg 73 50-120
1-Methylnaphthalene 2.00 1.604 mg/Kg 80 40-120
2-Methylnaphthalene 2.00 1.624 mg/Kg 81 40-120
2-Methylphenol 2.00 1.586 mg/Kg 79 51-123
3 & 4 Methylphenol 2000 1627 ug/Kg 81 47-123
Naphthalene 2.00 1.521 mg/Kg 76 41-120
2-Nitroaniline 2.00 1.548 mg/Kg 77 55-129
3-Nitroaniline 2.00 1.332 mg/Kg 67 45-120
4-Nitroaniline 2.00 1.933 mg/Kg 97 52-126
Nitrobenzene 2.00 1.400 mg/Kg 70 50-120
2-Nitrophenol 2.00 1.696 mg/Kg 85 53-120
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508814/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509040 Prep Batch: 508814
4-Nitrophenol 4.00 3.094 mg/Kg 77 38-133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
N-Nitrosodi-n-propylamine 2.00 1.358 mg/Kg 68 48-120
n-Nitrosodiphenylamine(as
diphenylamine)
1.98 1.667 mg/Kg 84 54-120
Pentachlorophenol 4.00 4.657 mg/Kg 116 32-131
Phenanthrene 2.00 1.669 mg/Kg 83 50-120
Phenol 2.00 1.417 mg/Kg 71 51-120
Pyrene 2.00 1.391 mg/Kg 70 54-120
1,2,4-Trichlorobenzene 2.00 1.633 mg/Kg 82 48-120
2,4,5-Trichlorophenol 2.00 2.005 mg/Kg 100 53-133
2,4,6-Trichlorophenol 2.00 1.750 mg/Kg 88 51-125
2-Fluorobiphenyl (Surr)27 -127
Surrogate
84
LCS LCS
Qualifier Limits%Recovery
802-Fluorophenol (Surr)25 -128
74Nitrobenzene-d5 (Surr)15 -136
78Phenol-d5 (Surr)29 -130
97Terphenyl-d14 (Surr)24 -146
1482,4,6-Tribromophenol (Surr)10 -150
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-508814/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509040 Prep Batch: 508814
Acenaphthene 2.00 1.590 mg/Kg 79 50-120 1 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 2.00 1.654 mg/Kg 83 50-120 0 30
Anthracene 2.00 1.796 mg/Kg 90 52-120 2 30
Benzo[a]anthracene 2.00 1.731 mg/Kg 87 55-120 3 30
Benzo[a]pyrene 2.00 1.799 mg/Kg 90 54-120 5 30
Benzo[b]fluoranthene 2.00 1.673 mg/Kg 84 55-120 2 30
Benzo[g,h,i]perylene 2.00 1.802 mg/Kg 90 45-120 2 30
Benzo[k]fluoranthene 2.00 1.849 mg/Kg 92 52-120 4 30
Bis(2-chloroethoxy)methane 2.00 1.473 mg/Kg 74 52-120 0 30
Bis(2-chloroethyl)ether 2.00 1.419 mg/Kg 71 50-120 12 30
bis (2-chloroisopropyl) ether 2.00 1.107 mg/Kg 55 34-120 1 30
Bis(2-ethylhexyl) phthalate 2.00 1.654 mg/Kg 83 58-158 3 30
4-Bromophenyl phenyl ether 2.00 2.053 mg/Kg 103 51-120 1 30
Butyl benzyl phthalate 2.00 1.566 mg/Kg 78 58-126 5 30
Carbazole 2.00 2.050 mg/Kg 103 61-132 3 30
4-Chloroaniline 2.00 1.433 mg/Kg 72 34-120 3 30
4-Chloro-3-methylphenol 2.00 1.826 mg/Kg 91 57-124 1 30
2-Chloronaphthalene 2.00 1.637 mg/Kg 82 55-120 1 30
2-Chlorophenol 2.00 1.526 mg/Kg 76 52-120 1 30
4-Chlorophenyl phenyl ether 2.00 1.947 mg/Kg 97 56-120 1 30
Chrysene 2.00 1.766 mg/Kg 88 54-120 4 30
Dibenz(a,h)anthracene 2.00 1.992 mg/Kg 100 49-120 2 30
Dibenzofuran 2.00 1.739 mg/Kg 87 58-120 0 30
1,2-Dichlorobenzene 2.00 1.425 mg/Kg 71 49-120 2 30
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-508814/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509040 Prep Batch: 508814
1,3-Dichlorobenzene 2.00 1.376 mg/Kg 69 48-120 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,4-Dichlorobenzene 2.00 1.365 mg/Kg 68 49-120 3 30
3,3'-Dichlorobenzidine 2.67 2.398 mg/Kg 90 42-120 4 30
2,4-Dichlorophenol 2.00 1.762 mg/Kg 88 56-120 0 30
Diethyl phthalate 2.00 1.751 mg/Kg 88 56-128 2 30
2,4-Dimethylphenol 2.00 1.670 mg/Kg 83 54-120 2 30
Dimethyl phthalate 2.00 1.786 mg/Kg 89 58-120 2 30
Di-n-butyl phthalate 2.00 1.933 mg/Kg 97 64-122 3 30
4,6-Dinitro-2-methylphenol 4.00 3.441 mg/Kg 86 35-135 3 30
2,4-Dinitrophenol 4.00 2.922 mg/Kg 73 10-138 8 30
2,4-Dinitrotoluene 2.00 2.068 mg/Kg 103 59-133 3 30
2,6-Dinitrotoluene 2.00 1.902 mg/Kg 95 57-123 2 30
Di-n-octyl phthalate 2.00 1.780 mg/Kg 89 57-137 3 30
Fluoranthene 2.00 2.039 mg/Kg 102 49-120 2 30
Fluorene 2.00 1.672 mg/Kg 84 47-120 1 30
Hexachlorobenzene 2.00 2.348 mg/Kg 117 49-127 1 30
Hexachlorobutadiene 2.00 1.731 mg/Kg 87 43-120 1 30
Hexachlorocyclopentadiene 2.00 1.495 mg/Kg 75 10-140 4 30
Hexachloroethane 2.00 1.308 mg/Kg 65 45-120 4 30
Indeno[1,2,3-cd]pyrene 2.00 1.920 mg/Kg 96 47-120 2 30
Isophorone 2.00 1.447 mg/Kg 72 50-120 1 30
1-Methylnaphthalene 2.00 1.610 mg/Kg 81 40-120 0 30
2-Methylnaphthalene 2.00 1.615 mg/Kg 81 40-120 1 30
2-Methylphenol 2.00 1.513 mg/Kg 76 51-123 5 30
3 & 4 Methylphenol 2000 1672 ug/Kg 84 47-123 3 30
Naphthalene 2.00 1.522 mg/Kg 76 41-120 0 30
2-Nitroaniline 2.00 1.567 mg/Kg 78 55-129 1 30
3-Nitroaniline 2.00 1.383 mg/Kg 69 45-120 4 30
4-Nitroaniline 2.00 2.011 mg/Kg 101 52-126 4 30
Nitrobenzene 2.00 1.378 mg/Kg 69 50-120 2 30
2-Nitrophenol 2.00 1.690 mg/Kg 85 53-120 0 30
4-Nitrophenol 4.00 3.131 mg/Kg 78 38-133 1 30
N-Nitrosodi-n-propylamine 2.00 1.340 mg/Kg 67 48-120 1 30
n-Nitrosodiphenylamine(as
diphenylamine)
1.98 1.685 mg/Kg 85 54-120 1 30
Pentachlorophenol 4.00 4.663 mg/Kg 117 32-131 0 30
Phenanthrene 2.00 1.719 mg/Kg 86 50-120 3 30
Phenol 2.00 1.376 mg/Kg 69 51-120 3 30
Pyrene 2.00 1.439 mg/Kg 72 54-120 3 30
1,2,4-Trichlorobenzene 2.00 1.628 mg/Kg 81 48-120 0 30
2,4,5-Trichlorophenol 2.00 2.068 mg/Kg 103 53-133 3 30
2,4,6-Trichlorophenol 2.00 1.724 mg/Kg 86 51-125 1 30
2-Fluorobiphenyl (Surr)27 -127
Surrogate
83
LCSD LCSD
Qualifier Limits%Recovery
792-Fluorophenol (Surr)25 -128
74Nitrobenzene-d5 (Surr)15 -136
76Phenol-d5 (Surr)29 -130
Eurofins TestAmerica, Pensacola
Page 62 of 76 11/6/2020
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-508814/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509040 Prep Batch: 508814
Terphenyl-d14 (Surr)24 -146
Surrogate
102
LCSD LCSD
Qualifier Limits%Recovery
1492,4,6-Tribromophenol (Surr)10 -150
Method: 8015C - Gasoline Range Organics (GRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-508296/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508296
RL MDL
Gasoline Range Organics [C6 - C10]ND 100 ug/L 10/27/20 12:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene (fid)93 78-119 10/27/20 12:08 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508296/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508296
Gasoline Range Organics [C6 -
C10]
1000 979.4 ug/L 98 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
a,a,a-Trifluorotoluene (fid)78 -119
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 400-508723/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 508593 Prep Batch: 508723
RL MDL
C6-C10 ND 0.100 mg/Kg 10/29/20 12:00 10/29/20 14:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene (fid)108 65-125 10/29/20 14:40 1
MB MB
Surrogate
10/29/20 12:00
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508723/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 508593 Prep Batch: 508723
C6-C10 1.00 0.9912 mg/Kg 99 62-141
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
107
LCS LCS
Qualifier Limits%Recovery
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8015C - Diesel Range Organics (DRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-508534/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508662 Prep Batch: 508534
RL MDL
C10-C28 ND 100 ug/L 10/28/20 12:45 10/30/20 04:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl (Surr)98 20-114 10/30/20 04:43 1
MB MB
Surrogate
10/28/20 12:45
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-508534/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508662 Prep Batch: 508534
C10-C28 20300 18630 ug/L 92 40-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl (Surr)20 -114
Surrogate
104
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-508534/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 508662 Prep Batch: 508534
C10-C28 20300 18310 ug/L 90 40-120 2 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
o-Terphenyl (Surr)20 -114
Surrogate
107
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 400-509198/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509471 Prep Batch: 509198
RL MDL
C10-C28 ND 5.00 mg/Kg 11/03/20 15:21 11/05/20 14:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl (Surr)77 27-151 11/05/20 14:16 1
MB MB
Surrogate
11/03/20 15:21
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-509198/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509471 Prep Batch: 509198
C10-C28 338 261.7 mg/Kg 77 38-138
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl (Surr)27 -151
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method: 8015C - Diesel Range Organics (DRO) (GC) (Continued)
Client Sample ID: B-1Lab Sample ID: 400-194926-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509471 Prep Batch: 509198
C10-C28 ND 545 368.9 mg/Kg 68 62-204☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
o-Terphenyl (Surr)27 -151
Surrogate
81
MS MS
Qualifier Limits%Recovery
Client Sample ID: B-1Lab Sample ID: 400-194926-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 509471 Prep Batch: 509198
C10-C28 ND 522 367.9 mg/Kg 71 62-204 0 30☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
o-Terphenyl (Surr)27 -151
Surrogate
92
MSD MSD
Qualifier Limits%Recovery
Method: Moisture - Percent Moisture
Client Sample ID: B-4Lab Sample ID: 400-194926-4 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 508464
Percent Solids 75.0 73.4 %2 4
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Moisture 25.0 26.6 F3 %6 4
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: AECOM Job ID: 400-194926-1
Project/Site: 7-11 No 36779 (NC)
Client Sample ID: B-1 Lab Sample ID: 400-194926-1
Matrix: SolidDate Collected: 10/23/20 12:25
Date Received: 10/24/20 09:05
Analysis Moisture AW10/28/20 15:411 TAL PEN508464
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: B-1 Lab Sample ID: 400-194926-1
Matrix: SolidDate Collected: 10/23/20 12:25
Percent Solids: 61.3Date Received: 10/24/20 09:05
Prep 5035 AMB10/30/20 08:43 TAL PEN508750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.789 g 5.00 g
Analysis 8260D 1 508704 10/30/20 14:46 AMB TAL PENTotal/NA 5 mL 5 mL
Prep 3546 508814 10/30/20 14:40 BAW TAL PENTotal/NA 15.43 g 1 mL
Analysis 8270E 1 509329 11/04/20 15:49 VC1 TAL PENTotal/NA
Prep 5035 508723 10/29/20 12:00 GRK TAL PENTotal/NA 5.354 g 5.00 g
Analysis 8015C 50 508593 10/29/20 20:06 GRK TAL PENTotal/NA 5 mL 5 mL
Prep 3546 509198 11/03/20 15:22 BAW TAL PENTotal/NA 15.76 g 1 mL
Analysis 8015C 1 509471 11/05/20 15:04 JAW TAL PENTotal/NA
Client Sample ID: B-2 Lab Sample ID: 400-194926-2
Matrix: SolidDate Collected: 10/23/20 12:47
Date Received: 10/24/20 09:05
Analysis Moisture AW10/28/20 15:411 TAL PEN508464
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: B-2 Lab Sample ID: 400-194926-2
Matrix: SolidDate Collected: 10/23/20 12:47
Percent Solids: 62.2Date Received: 10/24/20 09:05
Prep 5035 AMB10/30/20 08:43 TAL PEN508750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.355 g 5.00 g
Analysis 8260D 1 508704 10/30/20 15:13 AMB TAL PENTotal/NA 5 mL 5 mL
Prep 3546 508814 10/30/20 14:40 BAW TAL PENTotal/NA 15.27 g 1 mL
Analysis 8270E 1 509157 11/03/20 16:45 S1B TAL PENTotal/NA
Prep 5035 508723 10/29/20 12:00 GRK TAL PENTotal/NA 6.825 g 5.00 g
Analysis 8015C 50 508593 10/29/20 20:33 GRK TAL PENTotal/NA 5 mL 5 mL
Prep 3546 509198 11/03/20 15:22 BAW TAL PENTotal/NA 15.93 g 1 mL
Analysis 8015C 1 509471 11/05/20 15:17 JAW TAL PENTotal/NA
Client Sample ID: B-3 Lab Sample ID: 400-194926-3
Matrix: SolidDate Collected: 10/23/20 13:05
Date Received: 10/24/20 09:05
Analysis Moisture AW10/28/20 15:411 TAL PEN508464
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: AECOM Job ID: 400-194926-1
Project/Site: 7-11 No 36779 (NC)
Client Sample ID: B-3 Lab Sample ID: 400-194926-3
Matrix: SolidDate Collected: 10/23/20 13:05
Percent Solids: 72.8Date Received: 10/24/20 09:05
Prep 5035 AMB10/30/20 08:43 TAL PEN508750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.319 g 5.00 g
Analysis 8260D 1 508704 10/30/20 15:39 AMB TAL PENTotal/NA 5 mL 5 mL
Prep 3546 508814 10/30/20 14:40 BAW TAL PENTotal/NA 15.19 g 1 mL
Analysis 8270E 1 509157 11/03/20 17:05 S1B TAL PENTotal/NA
Prep 5035 508723 10/29/20 12:00 GRK TAL PENTotal/NA 6.039 g 5.00 g
Analysis 8015C 50 508593 10/29/20 21:00 GRK TAL PENTotal/NA 5 mL 5 mL
Prep 3546 509198 11/03/20 15:22 BAW TAL PENTotal/NA 15.71 g 1 mL
Analysis 8015C 1 509471 11/05/20 15:29 JAW TAL PENTotal/NA
Client Sample ID: B-4 Lab Sample ID: 400-194926-4
Matrix: SolidDate Collected: 10/23/20 13:15
Date Received: 10/24/20 09:05
Analysis Moisture AW10/28/20 15:411 TAL PEN508464
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: B-4 Lab Sample ID: 400-194926-4
Matrix: SolidDate Collected: 10/23/20 13:15
Percent Solids: 75.0Date Received: 10/24/20 09:05
Prep 5035 AMB10/30/20 08:43 TAL PEN508750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.671 g 5.00 g
Analysis 8260D 1 508704 10/30/20 16:06 AMB TAL PENTotal/NA 5 mL 5 mL
Prep 3546 508814 10/30/20 14:40 BAW TAL PENTotal/NA 15.32 g 1 mL
Analysis 8270E 1 509157 11/03/20 17:26 S1B TAL PENTotal/NA
Prep 5035 508723 10/29/20 12:00 GRK TAL PENTotal/NA 6.621 g 5.00 g
Analysis 8015C 50 508593 10/29/20 21:26 GRK TAL PENTotal/NA 5 mL 5 mL
Prep 3546 509198 11/03/20 15:22 BAW TAL PENTotal/NA 15.18 g 1 mL
Analysis 8015C 1 509471 11/05/20 15:41 JAW TAL PENTotal/NA
Client Sample ID: B-1 Lab Sample ID: 400-194926-5
Matrix: WaterDate Collected: 10/23/20 11:10
Date Received: 10/24/20 09:05
Analysis 8260D WPD10/30/20 15:461 TAL PEN508707
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 508631 10/30/20 09:16 KWS TAL PENTotal/NA 190 mL 1 mL
Analysis 8270E 1 508919 11/01/20 19:52 S1B TAL PENTotal/NA
Prep 3520C 508631 10/30/20 09:16 KWS TAL PENTotal/NA 190 mL 1 mL
Analysis 8270E 1 508980 11/02/20 15:30 S1B TAL PENTotal/NA
Analysis 8015C 1 508296 10/27/20 19:27 GRK TAL PENTotal/NA 5 mL 5 mL
Prep 3510C 508534 10/29/20 11:18 KWS TAL PENTotal/NA 157.6 mL 1 mL
Analysis 8015C 1 508662 10/30/20 08:13 JAW TAL PENTotal/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: AECOM Job ID: 400-194926-1
Project/Site: 7-11 No 36779 (NC)
Client Sample ID: B-2 Lab Sample ID: 400-194926-6
Matrix: WaterDate Collected: 10/23/20 10:50
Date Received: 10/24/20 09:05
Analysis 8260D WPD10/30/20 16:091 TAL PEN508707
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 508631 10/30/20 09:16 KWS TAL PENTotal/NA 257.6 mL 1 mL
Analysis 8270E 1 508919 11/01/20 20:16 S1B TAL PENTotal/NA
Prep 3520C 508631 10/30/20 09:16 KWS TAL PENTotal/NA 257.6 mL 1 mL
Analysis 8270E 1 508980 11/02/20 15:51 S1B TAL PENTotal/NA
Analysis 8015C 1 508296 10/27/20 19:59 GRK TAL PENTotal/NA 5 mL 5 mL
Prep 3510C 508534 10/29/20 11:18 KWS TAL PENTotal/NA 262.2 mL 1 mL
Analysis 8015C 1 508662 10/30/20 08:25 JAW TAL PENTotal/NA
Client Sample ID: B-3 Lab Sample ID: 400-194926-7
Matrix: WaterDate Collected: 10/23/20 11:30
Date Received: 10/24/20 09:05
Analysis 8260D WPD10/30/20 16:371 TAL PEN508707
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 508631 10/30/20 09:16 KWS TAL PENTotal/NA 240.4 mL 1 mL
Analysis 8270E 1 508919 11/01/20 20:40 S1B TAL PENTotal/NA
Prep 3520C 508631 10/30/20 09:16 KWS TAL PENTotal/NA 240.4 mL 1 mL
Analysis 8270E 1 508980 11/02/20 16:12 S1B TAL PENTotal/NA
Analysis 8015C 1 508296 10/27/20 20:30 GRK TAL PENTotal/NA 5 mL 5 mL
Prep 3510C 508534 10/29/20 11:18 KWS TAL PENTotal/NA 185.2 mL 1 mL
Analysis 8015C 1 508662 10/30/20 08:38 JAW TAL PENTotal/NA
Client Sample ID: B-4 Lab Sample ID: 400-194926-8
Matrix: WaterDate Collected: 10/23/20 12:30
Date Received: 10/24/20 09:05
Analysis 8260D WPD10/30/20 17:051 TAL PEN508707
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 508631 10/30/20 09:16 KWS TAL PENTotal/NA 258.6 mL 1 mL
Analysis 8270E 1 508919 11/01/20 21:04 S1B TAL PENTotal/NA
Prep 3520C 508631 10/30/20 09:16 KWS TAL PENTotal/NA 258.6 mL 1 mL
Analysis 8270E 1 508980 11/02/20 16:32 S1B TAL PENTotal/NA
Analysis 8015C 1 508296 10/27/20 21:01 GRK TAL PENTotal/NA 5 mL 5 mL
Prep 3510C 508534 10/29/20 11:18 KWS TAL PENTotal/NA 262.8 mL 1 mL
Analysis 8015C 1 508662 10/30/20 08:50 JAW TAL PENTotal/NA
Client Sample ID: Method Blank Lab Sample ID: MB 400-508296/3
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis 8015C GRK10/27/20 12:081 TAL PEN508296
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: AECOM Job ID: 400-194926-1
Project/Site: 7-11 No 36779 (NC)
Client Sample ID: Method Blank Lab Sample ID: MB 400-508534/1-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3510C KWS10/28/20 12:45 TAL PEN508534
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 250 mL 1 mL
Analysis 8015C 1 508662 10/30/20 04:43 JAW TAL PENTotal/NA
Client Sample ID: Method Blank Lab Sample ID: MB 400-508631/1-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3520C KWS10/29/20 13:40 TAL PEN508631
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 250 mL 1 mL
Analysis 8270E 1 508916 11/01/20 13:38 S1B TAL PENTotal/NA
Client Sample ID: Method Blank Lab Sample ID: MB 400-508707/5
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis 8260D WPD10/30/20 09:411 TAL PEN508707
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-508723/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 GRK10/29/20 12:00 TAL PEN508723
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.0 g
Analysis 8015C 1 508593 10/29/20 14:40 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-508750/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 AMB10/30/20 08:43 TAL PEN508750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8260D 1 508704 10/30/20 11:14 AMB TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-508814/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BAW10/30/20 14:40 TAL PEN508814
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8270E 1 509040 11/03/20 21:16 VC1 TAL PENTotal/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: AECOM Job ID: 400-194926-1
Project/Site: 7-11 No 36779 (NC)
Client Sample ID: Method Blank Lab Sample ID: MB 400-509198/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BAW11/03/20 15:21 TAL PEN509198
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8015C 1 509471 11/05/20 14:16 JAW TAL PENTotal/NA
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-508296/1002
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis 8015C GRK10/27/20 11:361 TAL PEN508296
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-508534/2-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3510C KWS10/28/20 12:45 TAL PEN508534
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 250 mL 1 mL
Analysis 8015C 1 508662 10/30/20 04:56 JAW TAL PENTotal/NA
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-508631/2-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3520C KWS10/29/20 13:40 TAL PEN508631
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 250 mL 1 mL
Analysis 8270E 1 508916 11/01/20 13:59 S1B TAL PENTotal/NA
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-508707/1003
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis 8260D WPD10/30/20 08:561 TAL PEN508707
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-508723/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 GRK10/29/20 12:00 TAL PEN508723
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.0 g
Analysis 8015C 1 508593 10/29/20 14:13 GRK TAL PENTotal/NA 5 mL 5 mL
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: AECOM Job ID: 400-194926-1
Project/Site: 7-11 No 36779 (NC)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-508750/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 AMB10/30/20 08:43 TAL PEN508750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8260D 1 508704 10/30/20 09:50 AMB TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-508814/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BAW10/30/20 14:40 TAL PEN508814
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8270E 1 509040 11/03/20 21:42 VC1 TAL PENTotal/NA
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-509198/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BAW11/03/20 15:21 TAL PEN509198
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8015C 1 509471 11/05/20 14:28 JAW TAL PENTotal/NA
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-508534/3-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3510C KWS10/28/20 12:45 TAL PEN508534
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 250 mL 1 mL
Analysis 8015C 1 508662 10/30/20 05:08 JAW TAL PENTotal/NA
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-508631/3-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3520C KWS10/29/20 13:40 TAL PEN508631
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 250 mL 1 mL
Analysis 8270E 1 508916 11/01/20 14:19 S1B TAL PENTotal/NA
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-508814/3-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BAW10/30/20 14:40 TAL PEN508814
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8270E 1 509040 11/03/20 22:08 VC1 TAL PENTotal/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: AECOM Job ID: 400-194926-1
Project/Site: 7-11 No 36779 (NC)
Client Sample ID: B-1 Lab Sample ID: 400-194926-1 MS
Matrix: SolidDate Collected: 10/23/20 12:25
Percent Solids: 61.3Date Received: 10/24/20 09:05
Prep 3546 BAW11/03/20 15:22 TAL PEN509198
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.20 g 1 mL
Analysis 8015C 1 509471 11/05/20 14:40 JAW TAL PENTotal/NA
Client Sample ID: B-1 Lab Sample ID: 400-194926-1 MSD
Matrix: SolidDate Collected: 10/23/20 12:25
Percent Solids: 61.3Date Received: 10/24/20 09:05
Prep 3546 BAW11/03/20 15:22 TAL PEN509198
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.88 g 1 mL
Analysis 8015C 1 509471 11/05/20 14:52 JAW TAL PENTotal/NA
Client Sample ID: B-4 Lab Sample ID: 400-194926-4 DU
Matrix: SolidDate Collected: 10/23/20 13:15
Date Received: 10/24/20 09:05
Analysis Moisture AW10/28/20 16:071 TAL PEN508464
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
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Method Summary
Job ID: 400-194926-1Client: AECOM
Project/Site: 7-11 No 36779 (NC)
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds by GC/MS TAL PEN
SW8468270ESemivolatile Organic Compounds (GC/MS)TAL PEN
SW8468015CGasoline Range Organics (GRO) (GC)TAL PEN
EPA8015CDiesel Range Organics (DRO) (GC)TAL PEN
EPAMoisturePercent Moisture TAL PEN
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)TAL PEN
SW8463520CLiquid-Liquid Extraction (Continuous)TAL PEN
SW8463546Microwave Extraction TAL PEN
SW8465030CPurge and Trap TAL PEN
SW8465035Closed System Purge and Trap TAL PEN
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
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Accreditation/Certification Summary
Client: AECOM Job ID: 400-194926-1
Project/Site: 7-11 No 36779 (NC)
Laboratory: Eurofins TestAmerica, Pensacola
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)314State 12-31-20
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
Moisture Solid Percent Moisture
Moisture Solid Percent Solids
Eurofins TestAmerica, Pensacola
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Login Sample Receipt Checklist
Client: AECOM Job Number: 400-194926-1
Login Number: 194926
Question Answer Comment
Creator: Hinrichsen, Megan E
List Source: Eurofins TestAmerica, Pensacola
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.0.8°C, 1.1°C IR-7
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins TestAmerica, Pensacola
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