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HomeMy WebLinkAboutMO-8561_40099_CA_MRP_20231019 October 20, 2023 Mr. Brad Newton NCDEQ-UST Section Mooresville Regional Office 610 East Center Ave. Mooresville, NC 28115 Re: Ground Water Monitoring Report July - September 2023 Fast Track #145 2443 NC Highway 10 West Newton, Catawba County North Carolina Facility ID Number: 00-0-0000036548 Incident Number: 40099 GRI Project Number: 5398 Dear Mr. Newton, Please find enclosed the referenced report for the above-mentioned site. If you have any questions, please contact Joanna Alley at 704-845-4010. Sincerely, Geological Resources, Inc. Johanna Moats AP / AR Coordinator Enclosure Cc: Mr. Matthew Redmond; Raymer Oil Company, file 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 Engineering Certification: C-2727 • Geology Certification: C-127 Ground Water Monitoring Report July - September 2023 Fast Track #145 2443 NC Highway 10 West Newton, Catawba County North Carolina Facility ID Number: 00-0-0000036548 Incident Number: 40099 GRI Project Number: 5398 Prepared for: Mr. Matthew Redmond Raymer Oil Company P.O. Box 327 Troutman, North Carolina 28166 October 19, 2023 Joanna Alley, P.E. Project Manager ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 i SITE INFORMATION 1. Site Identification  Fast Track #145 (Facility ID 00-0-0000036548)  Incident Number 40099 – Intermediate Risk (I125D)  Location of Source Area: 2443 NC Highway 10 West Newton, NC 28658 Catawba County 35.644579°N, 81.268800°W (Topographical Map) 2. Information about Contacts Associated with the Leaking UST System UST Owner Fast Track Inc. P.O. Box 410 Wilkesboro, NC 28697 Email Unknown 336-838-4000 UST Operator Raymer Brothers, Inc. P.O. Box 327 Troutman, NC 28166 matthew@fastphils.net 704-873-7285 Property Owner KLR Real Estate, LLC. 589 North Main Street Troutman, NC 28166 Email Unknown Phone No. Unknown Property Occupant Valero/Fast Phil’s #145 2443 NC Highway 10 West Newton, NC 28658 Email Unknown 828-466-0161 Consultant/Contractor Geological Resources, Inc. 3502 Hayes Road Monroe, NC 28110 jra@geologicalresourcesinc.com 704-845-4010 Analytical Laboratory Waypoint Analytical 4449 Springbrook Road Charlotte, NC 28217 State Certification No. 37735/402 704-529-6364 3. Information about Release  Release was discovered on July 5, 2012  An unknown amount of product was released from the leaking UST System  Currently, one 12,000-gallon gasoline UST, one 8,000-gallon gasoline UST, and one 5,000-gallon diesel UST and associated pumps and product piping are active at the site. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 ii EXECUTIVE SUMMARY Fast Track #145 is located at 2443 NC Highway 10 West in Newton, Catawba County, North Carolina. The site is currently owned by KLR Real Estate, LLC. and is operated by Raymer Brothers, Inc. as a petroleum retail facility. In May 2020, Raymer Oil Company became the responsible party for incident 40099. A release was discovered during a Phase II ESA conducted in July 2012. Currently, one 12,000-gallon gasoline UST, one 8,000-gallon gasoline UST, and one 5,000-gallon diesel UST and associated pumps and product piping are active at the site. The adjoining properties are a mixture of residential and commercial properties. According to the information determined during 2012 receptor survey activities, six active potable water supply wells were identified within a 1,000- foot radius of the site. Public water is available to the site and surrounding properties within a 1,500-foot radius of the site. The November 2014 CAP submitted by Paragon Environmental Consultants, Inc. proposed connecting the residences with potable water supply wells to municipal water and reducing contaminant concentrations to below GCLs at the site using MMPE events in combination with a dual-phase extraction and air sparging system. In accordance with the March 2021 remediation system design, an AS/SVE system was installed at the site and started on March 17, 2023. Additionally, several MMPE events have been conducted at the site. O&M site visits were conducted on July 17, August 21, and September 19, 2023. Hour meter, system vacuum, pressure, air flow, temperature, AS well pressure, and SVE well vacuum readings were collected during each site visit. On September 21, 2023, six Type II monitoring wells were gauged, purged, and/or sampled. MW-8 was dry and could not be sampled. The field where MW-4, MW-9, MW-10, and MW-15 are located was overgrown and these wells could not be found. Free product was not observed during the September 2023 gauging activities. The concentrations of benzene, toluene, ethylbenzene, xylenes, naphthalene, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene reported in the ground water samples collected from MW-1, MW-3, MW-6, MW-14 and MW-17 exceeded the MACs. The concentrations of benzene, toluene, ethylbenzene, xylenes and/or naphthalene reported in the ground water samples collected from MW-1 and MW-14 exceeded 10 times the 2B Standards. The concentration of benzene reported in the ground water sample collected from MW-6 exceeded the GCL. Calculations based on the September 2023 ground water sampling event indicate that the contaminant mass has decreased by 35.1%, 39.5%, and 78.8% in Areas 1, 2, and 3, respectively, when compared to the baseline sampling event. The overall contaminant mass at the site has decreased by approximately 65.4% from the baseline event to the September 2023 sampling event. Based on this information, the risk classification for the site should remain Intermediate risk. GRI recommends the continued operation of the remediation system until contaminant concentrations have been reduced to below 10 times the 2B Standards. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 iii ACRONYMS ACM: Asbestos Containing Materials AFVR: Aggressive Fluid-Vapor Recovery ARR: Acknowledgement of Report Receipt AS: Air Sparging AST: Aboveground Storage Tank ASTM: American Society for Testing and Materials BGS: Below Ground Surface CAP: Corrective Action Plan CFR: Code of Federal Regulations CSA: Comprehensive Site Assessment DPE: Dual Phase Extraction DRO: Total Petroleum Hydrocarbons Diesel Range Organics DWM: Division of Waste Management DWR: Department of Water Resources EPA: Environmental Protection Agency EPH: Extractible Petroleum Hydrocarbons ESA: Environmental Site Assessment GCL: Gross Contamination Level GRI: Geological Resources, Inc. GRO: Total Petroleum Hydrocarbons Gasoline Range Organics LSA: Limited Site Assessment MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202 MADEP: Massachusetts Department of Environmental Protection MCC: Maximum Contaminant Concentrations MMPE: Mobile Multi-Phase Extraction NAPL: Non-Aqueous Phase Liquid, “Free Product” NCDEQ: North Carolina Department of Environmental Quality NCDOT: North Carolina Department of Transportation NFA: Notice of No Further Action NORR: Notice of Regulatory Requirements NOV: Notice of Violation NPDES: National Pollutant Discharge Elimination System NRP: Notice of Residual Petroleum O&M: Operation and Maintenance PAHs: Polynuclear Aromatic Hydrocarbons PCA: Pre-Construction Assessment PRM: Product Recovery Management, Inc. RAL: Regulatory Action Level SCLs: Soil Cleanup Level SPCC: Spill Prevention Control and Countermeasures SVE: Soil Vapor Extraction SVOCs: Semi-Volatile Organic Compounds SWPPP: Stormwater Pollution Prevention Plan TCLP: Toxicity Characteristic Leaching Procedure (EPA Method SW-846 1311) TOC: Top of Casing TPH: Total Petroleum Hydrocarbons USGS: United States Geological Survey UST: Underground Storage Tank UVF: Ultraviolet Fluorescence VOCs: Volatile Organic Compounds VPH: Volatile Petroleum Hydrocarbons ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 TABLE OF CONTENTS SITE INFORMATION ............................................................................................................................ i EXECUTIVE SUMMARY ....................................................................................................................... ii ACRONYMS ....................................................................................................................................... iii 1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION ...................................................................................................3 3.0 FREE PRODUCT REMOVAL ........................................................................................................4 4.0 REMEDIATION SYSTEM ............................................................................................................4 5.0 AIR SAMPLING.........................................................................................................................5 6.0 SOIL AND GROUND WATER REMEDIATION ...............................................................................6 7.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................8 8.0 CONCLUSIONS .........................................................................................................................8 9.0 LIMITATIONS ...........................................................................................................................8 10.0 STATEMENTS AND CERTIFICATION ...........................................................................................9 FIGURES Figure 1: Site Location Map Figure 2: Site Map Figure 3: Site Vicinity Map Figure 4: Water Table Surface Map Figure 5: Ground Water Quality Map Figure 6: Benzene Isoconcentration Map Figure 7: Toluene Isoconcentration Map Figure 8: Ethylbenzene Isoconcentration Map Figure 9: Xylenes Isoconcentration Map Figure 10: Naphthalene Isoconcentration Map Figure 11: Remediation Well Location Map Figure 12: Estimated Contaminant Mass Area Map TABLES Table 1: UST Owner and Operator Information Table 2: UST System Information Table 3: Water Supply Well Information Table 4: Adjacent Property Owner Information Table 5: Well Construction and Gauging Information Table 6: Summary of Ground Water Sample Analytical Results Table 7: Summary of Remediation System O&M Visits Table 8: Summary of Air Analytical Results ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 APPENDICES Appendix A: State Correspondence Appendix B: Land Use Information Appendix C: Incident Reports Appendix D: Historical Soil Quality Information Appendix E: Laboratory Analytical Reports Appendix F: O&M Field Data Sheets Appendix G: Overall Remediation Costs Appendix H: Contaminant Mass Calculations ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 1 1.0 SITE HISTORY AND CHARACTERIZATION GRI presents the results of the July through September 2023 O&M activities and the September 2023 ground water sampling event at the Fast Track #145 site located at 2443 NC Highway 10 West in Newton, Catawba County, North Carolina. These activities were conducted in accordance with GRI Proposal No. 23-421, which was submitted to the NCDEQ on June 30, 2023, and approved as Task Authorization No. 40099-24 on July 3, 2023. A topographical map showing the location of the site is included as Figure 1. State correspondence is included as Appendix A. The site is currently owned by KLR Real Estate, LLC and is operated by Raymer Brothers, Inc. as a petroleum retail facility. In May 2020, Raymer Oil Company became the responsible party of incident 40099. A release was discovered during a Phase II ESA conducted in July 2012. Currently, one 12,000-gallon gasoline UST, one 8,000-gallon gasoline UST, and one 5,000-gallon diesel UST and associated pumps and product piping are active at the site. UST owner/operator information and UST system information are included in Tables 1 and 2, respectively. The Registered Tank Report is shown below: The site and surrounding area are a mixture of residential and commercial properties. A copy of the Land Use table is included as Appendix B. The site contains one building (the store) and is primarily capped with concrete and asphalt. The overall topography at the site is relatively flat; the eastern portion of the site slopes eastward towards an unnamed creek, located approximately 250 feet east of the source area. Seventeen Type II monitoring wells (MW-1 through MW-17) were installed at the site during previous ground water assessment activities. A Site Map showing the locations of the monitoring wells and the structures on-site is included as Figure 2. A receptor survey was conducted at the site by Paragon Environmental Consultants, Inc. (Paragon) in July 2012. Fourteen water supply wells were identified within a 1,000-foot radius of the site. Six of the fourteen water supply wells (WSW-3, WSW-4, WSW-7, WSW-11, WSW-12, and WSW-14) identified were determined to be active potable wells. According to available information, the six residences with potable water supply wells were connected to municipal water and as a result, the site’s risk classification was lowered by the NCDEQ to Intermediate in January 2016. Municipal water is available to the site and ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 2 surrounding properties. Two branches of an unknown tributary are located within a 500-foot radius of the site. Water supply well information is included in Table 3. Adjacent property owner information is included in Table 4. A Site Vicinity Map showing the adjacent properties and a Zoning Map showing the zoning information are included as Figures 3A and 3B, respectively. Please note that the historical information contained in this report was obtained under the supervision of the previous consultants. Although GRI cannot verify the accuracy of the information obtained by previous consultants, for the purpose of this report it is assumed to be correct, and any inferences or interpretations made by GRI based on data that may be incorrect are not the responsibility of GRI. Please refer to earlier submittals for additional information regarding previous assessment activities. One additional incident (Incident No. 22431) was reported on the site. Based on the NCDEQ Incident Report, it does not appear that this incident was assessed. One incident (Incident No. 10359) was reported on an adjacent property. These incidents have both been closed. Copies of the NCDEQ Incident Reports are included as Appendix C. A map showing the locations of additional incidents in the vicinity of the site is shown below: Paragon submitted a CAP on November 18, 2014, that proposed to reduce contaminant concentrations using MMPE events in combination with dual-phase extraction and air sparging system. To date, several MMPE events have been conducted at the site. No projected milestones were established in the CAP. In March 2021, GRI submitted a remediation system design to implement the 2014 CAP. In accordance with 40099 22431 10359 ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 3 the system design, an AS/SVE remediation system was installed at the site and was started on March 17, 2023. The remediation system is currently in operation. Based on the presence of surface water and contaminant concentrations exceeding 10 times the 2B standards, the risk classification should remain intermediate risk. 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION Soil assessment was not conducted during the current scope of work. Historical soil quality information from previous consultants is included as Appendix D. On September 21, 2023, six Type II monitoring wells (MW-1, MW-3, MW-6, MW-8, MW-14 and MW-17) were gauged, purged and/or sampled. MW-8 was dry and could not be sampled. The field where MW-4, MW-9, MW-10 and MW-15 are located was overgrown and these wells could not be found. Additionally, the creek adjacent to the site was dry; therefore, a surface water sample could not be collected. Free product was not observed during the September 2023 gauging activities. Depths to ground water in the Type II monitoring wells ranged from 25.65 feet to 32.55 feet. Ground water elevations in the Type II monitoring wells relative to an arbitrary datum of 100.00 feet ranged from 65.26 feet to 73.39 feet. Ground water flow was generally to the east with a horizontal gradient of approximately 0.10 feet per foot. The vertical gradient was not calculated. Well construction and gauging information is included in Table 5. A Water Table Surface Map based on the Type II monitoring wells is included as Figure 4. A summary of the current ground water gauging data is shown below: Well ID Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) MW-1 25-45 45 97.81 32.55 --- 65.26 MW-3 19-39 39 100.00 25.85 --- 74.15 MW-4 4-19 19 66.37 NM NM NM MW-6 16-36 36 100.50 27.11 --- 73.39 MW-8 17-37 37 98.64 NM NM NM MW-9 3-13 13 55.86 NM NM NM MW-10 3-13 13 58.47 NM NM NM MW-14 16-36 36 98.93 27.27 --- 71.66 MW-15 4-14 14 55.44 NM NM NM MW-17 10-35 35 97.75 25.65 --- 72.10 Ground water samples collected from the monitoring wells were submitted for laboratory analyses of VOCs by EPA Method 6200B. The concentrations of benzene, toluene, ethylbenzene, xylenes, naphthalene, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene, and/or 1,3,5- trimethylbenzene reported in the ground water samples collected from MW-1, MW-3, MW-6, MW-14 and MW-17 exceeded the MACs. The concentrations of benzene, toluene, ethylbenzene, xylenes and/or naphthalene reported in the ground water samples collected from MW-1, MW-6, MW-14 and MW-17 ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 4 exceeded 10 times the 2B Standards. The concentration of benzene reported in the ground water sample collected from MW-6 exceeded the GCL. A summary of the analytical results for ground water samples collected on September 21, 2023, is included in Table 6. A Ground Water Quality Map based on the September 2023 data is included as Figure 5. Isoconcentration maps for all contaminants that exceeded 10 times the 2B Standards are included as Figure 6 through Figure 10. A telescoping well has not been installed at the site; therefore, cross sections have not been included. A complete report of laboratory analyses of the ground water samples collected from the monitoring wells during the September 2023 sampling event is included in Appendix E. A summary of the current ground water analytical data is shown below: Contaminant of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well ID MACs (µg/l) 1 600 600 500 20 6 GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000 10 x 2B Standard (µg/l) 510 110 1,300 6,700 15,000 120 MW-1 828 1,700 232 1,380 <14.0 940 MW-3 29.4 3.07 1.24 9.36 <0.140 6.80 MW-4 NS NS NS NS NS NS MW-6 8,790 28,100 2,640 14,300 <14.0 730 MW-8 NS NS NS NS NS NS MW-9 NS NS NS NS NS NS MW-10 NS NS NS NS NS NS MW-14 133 193 32.7 235 <0.140 <0.470 MW-15 NS NS NS NS NS NS MW-17 <18.0 107 137 1,360 <14.0 902 A laboratory supplied trip blank was submitted with the ground water samples for analysis of VOCS by EPA Method 6200B. No detectable concentrations of requested method constituents were reported in the trip blank. The site is in the Piedmont Physiographic Province of North Carolina. The seasonal high water table at the site was observed in June 2021 and has a depth to water of approximately twenty to twenty-four feet BGS. 3.0 FREE PRODUCT REMOVAL Free product has not been historically observed at the subject site. Multiple MMPEs have been conducted since the CAP was developed in November 2014. The goal of the MMPEs was to reduce contaminant concentrations in ground water. 4.0 REMEDIATION SYSTEM In accordance with the 2014 CAP and 2021 system design, an AS/SVE system was installed at the site and activated on March 17, 2023. The system installation included the connection of a total of seven AS wells ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 5 and seven SVE wells throughout the contaminant plume. A map showing the locations of the remediation wells is included as Figure 11. O&M site visits were conducted on July 17, August 21 and September 19, 2023. Hour meter, system vacuum, pressure, air flow, temperature, AS well pressure, and SVE well vacuum readings were collected during the site visits and SVE exhaust air samples were collected monthly and submitted for laboratory analysis of BTEX. The SVE system operated for a total of 1,438 hours and the system vacuum ranged from 69.95 to 70.10 inches of water during the current quarter of O&M (July through September 2023). The AS system operated for a total of 1,439 hours during the reporting period with system pressures ranging from 15.62 to 16.27 PSI. Please refer to the individual O&M data sheets for additional system measurements. System flows were adjusted as needed. The general condition of the system was also noted. Work conducted during the site visits along with hour meter readings is summarized in Table 7. O&M field data sheets are included as Appendix F. 5.0 AIR SAMPLING Air samples were collected from the exhaust of the SVE system on July 17, August 21 and September 19, 2023. A summary of the analytical results for air samples collected during the current quarter of system operation is presented in Table 8. Complete reports of laboratory analyses are included as Appendix E. A summary of air sampling results during the current quarter is shown below: Sample Date Benzene Toluene Ethylbenzene Xylenes Total BTEX TRPH 07/17/23 <3.1 <2.6 <2.3 <6.9 <14.9 34 08/21/23 <3.1 <2.6 <2.3 <6.9 <14.9 <31 09/19/23 <3.1 <2.6 <2.3 <6.9 <14.9 <31 Overall, remediation and monitoring activities from CAP implementation through the current quarter have cost $274,793.10. A breakdown of current quarter’s costs is included as Appendix G and summarized below: Claim Number Task Code Task Code Description Cost Claim Amount (claim has not been submitted) 4.031 Cost for Sampling Wells $561.00 $7,432.50 4.090 Cost for Analytical $849.00 6.090 Ground Water Monitoring Report $1,125.00 7.201 Cost for Scheduled Maintenance $697.50 7.260 Cost for Remediation Operating Expenses (assumed, pending receipt of all power bills) $3,300.00 12.050 Consultant Travel $750.00 12.055 Temporary Impact Increase $150.00 Total Cost Since System Installation $274,793.10 ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 6 6.0 GROUND WATER REMEDIATION The baseline contaminant mass at the site was determined based on the total BTEX, MTBE, and naphthalene concentrations reported in the January 2014 CSA as well as the maximum historical water column height observed in each area. The contaminant plume was divided into three areas (Areas 1 through 3) based on the benzene concentrations during the July 2020 ground water sampling event. A map showing the estimated contaminant mass areas is included as Figure 12. Available historical data for the site was reviewed in order to develop a strategy for measuring remediation progress against an established baseline for the contaminant plume. To calculate contaminant mass present at the site, the following three avenues of contaminant migration/source were evaluated as well as the data required for each source. The calculations were revised to estimate the influence of fluctuations in ground water elevation. 1. Contamination present in ground water: The November 2012 and March 2013 ground water sampling data and total BTEX, MTBE, and naphthalene constituents were used to determine the baseline contaminant mass in each area. Area #1 had approximately 76,258.29 grams of contaminant mass; Area #2 had approximately 102,686.65 grams of contaminant mass and Area #3 had approximately 1,428.39 grams of contaminant mass. Calculations based on the September 2023 ground water sampling event indicate that the contaminant mass has decreased by 35.1%, 39.5%, and 78.8% in Areas 1, 2, and 3, respectively, when compared to the baseline sampling event. The contaminant concentrations in Area 1 through Area 3 have generally decreased over time; however, additional monitoring is necessary to determine the effect of the remediation system on the contaminant plume. The overall contaminant mass at the site has decreased by approximately 65.4% from the baseline event to the September 2023 sampling event. Contaminant mass calculations are included as Appendix H. A chart depicting the overall trend in contaminant mass and the changes in average water column depth over time is shown below: ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 7 2. Contamination due to leaching effect from unsaturated soils: Soil quality data from the former source areas as well as from the vicinity of the above referenced source area monitoring wells is not available. Therefore, it is not possible at this point to factor in the effect of this potential on- going source of ground water contamination. If soil sampling is deemed necessary for the calculation of any secondary source inputs, they will be proposed at a later date. 3. Contamination input due to the presence of free product: Free product has not been historically observed at the subject site. Monitoring Plan: Based on the Intermediate site risk ranking, the following monitoring plan is recommended:  Conduct a comprehensive ground water sampling event that includes wells MW-1, MW-3, MW- 4, MW-6, MW-8 through MW-10, MW-14, MW-15, and MW-17 on a quarterly basis for the initial year of operation to monitor the effect of the remediation system. Following the initial year of operation, any wells with contaminant concentrations exceeding 10 times the 2B Standard should be sampled on a semi-annual basis and a comprehensive sampling event for the above listed wells should be conducted on an annual basis.  Conduct soil sampling on an as-needed basis. Performance Monitoring:  The remediation system appears to have been effective at reducing ground water contaminant concentration in the targeted wells; however, additional monitoring is necessary to establish a trend for the remedial efforts. Please note that milestones were not established in the CAP.  The remediation system should remain running for the next quarter of operation. 0.00 2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 30,000 80,000 130,000 180,000 230,000 280,000 Average Water Column Height (ft)Contaminant Mass (grams)Time Total Contaminant Mass vs. Time Fast Track #145 (Incident No. 40099) Contaminant Mass (grams)Water Column Height (ft) Linear (Contaminant Mass (grams)) ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 8 7.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS Due to the site being in the active remediation phase, no natural attenuation monitoring plan is currently in place at the site. 8.0 CONCLUSIONS  O&M site visits were conducted on July 17, August 21 and September 19, 2023. Hour meter, system vacuum, pressure, air flow, temperature, AS well pressure, and SVE well vacuum readings were collected during each site visit.  On September 21, 2023, six Type II monitoring wells were gauged, purged, and/or sampled. MW- 8 was dry and could not be sampled. The field where MW-4, MW-9, MW-10, and MW-15 are located was overgrown and these wells could not be found. Free product was not observed during the September 2023 gauging activities. Ground water flow was generally to the east with a horizontal gradient of approximately 0.10 feet per foot. The vertical gradient was not calculated.  The concentrations of benzene, toluene, ethylbenzene, xylenes, naphthalene, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene reported in the ground water samples collected from MW-1, MW-3, MW-6, MW-14 and MW-17 exceeded the MACs.  The concentrations of benzene, toluene, ethylbenzene, xylenes and/or naphthalene reported in the ground water samples collected from MW-1, MW-6, MW-14 and MW-17 exceeded 10 times the 2B Standards. The concentration of benzene reported in the ground water sample collected from MW-6 exceeded the GCL.  Calculations based on the September 2023 ground water sampling event indicate that the contaminant mass has decreased by 35.1%, 39.5%, and 78.8% in Areas 1, 2, and 3, respectively, when compared to the baseline sampling event. The overall contaminant mass at the site has decreased by approximately 65.4% from the baseline event to the September 2023 sampling event.  Based on this information, the risk classification for the site should remain Intermediate risk. GRI recommends the continued operation of the remediation system until contaminant concentrations have been reduced to below 10 times the 2B Standards. 9.0 LIMITATIONS This report has been prepared for the exclusive use of Raymer Oil Company and the NCDEQ for specific application to the referenced site in Catawba County, North Carolina. The assessment was conducted based on the scope of work and level of effort desired by the NCDEQ and with resources adequate only for that scope of work. Our findings have been developed in accordance with generally accepted standards of environmental practices in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied. The data that is presented in this report is indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. In addition, the data obtained from samples would be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No additional information can logically be inferred from this data. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 19, 2023 Fast Track #145 Project Manager: Joanna Alley, P.E. GRI Project No. 5398 9 10.0 STATEMENTS AND CERTIFICATION 1 Enter the date the monitoring report was due. n/a Will this report be submitted after the established due date? YES NO 2 Was any required information from the above template missing from this report? YES NO IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain what was missing and why. 3 If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? (within a reasonable margin of error) YES NO IF the answer to question #3 is “NO”, skip to the certification under #8 below. IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and outline proposed remedies. (This should be described in more detail in the report text above.) N/A 4 Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? YES NO 5 Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? YES NO IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions recommended to further assess or clean up this known or suspected source. (This should be described in more detail in the report text above.) 6 Certification: I, Samuel L. McKay, III, a Licensed Geologist for Geological Resources, Inc., do certify that the information contained in this report is correct and accurate to the best of my knowledge. Geological Resources, Inc. is licensed to practice engineering and geology in North Carolina. The certification number of the company or corporation is C-2727/C-127. FIGURES SITE LOCATION Figure 1 Site Location Fast Track #145 2443 NC Highway 10 West Newton, Catawba County, NC Incident No. 40099 GRI Project No. 5398 500 M 2000 FT Date: 07/19/2020 Location: 35.644579°N -81.268800°W D a d "J "J "J "J "J "J "J "J "J "J "J "J "J "J SITE 362911678025 362911571253 362911564459 362911670179 362907573779 362911672327 362911661942 362907576636 362911565735 362911566946 362907682129 362911576481 362907577597 362911577137362907586014 362907672635362911562820 3 6 2 9 0 7 6 7 0 5 2 4 WSW-6 WSW-9 WSW-5 WSW-7 WSW-8 WSW-4 WSW-3 WSW-2 WSW-1 WSW-14 WSW-13 WSW-12 WSW-11 WSW-10 Unknown Tributary Unknown TributaryU n k n o w n T rib u ta ry N C 1 0 H W YSTARTOWN RDNOTTI NGHAM DRS T A R D R K E N S IN G T O N C IRO R C H A R D S T DO V E STPOOVEY ST S T O N E H E N G E S T ISHMAL AVE KNI GHTBRI DGE DRC A M B R I D G E S T JERRY AVE HALLPOINT LN L IT T L E J O H N T RRAD ER STDOVE ST TRACK #1452443 NC HIGHWAY 10 WESTNEWTON, CATAWBA COUNTYNORTH CAROLINAINCIDENT NO. 40099GRI NO. 5398 PREPARED BY:GEOLOGICAL RESOURCES, INC.AUGUST 13, 2020 1,500-FOOT RADIUS 1,000-FOOT RADIUS 250-FOOT RADIUS ³ 0 300150Feet1 inch = 300 feet 500-FOOT RADIUS LEGEND "J Water Supply Well Catawba County_RoadCenterlines Catawba County_Streams Well Owners and Adjacent Properties Catawba County_Parcels FIGURE 3A: SITE VICINITY MAP FAST SS SS SS SS SS SS SS SSSSSSSS SS TABLES UST ID Number 1A, 1B, 1C Facility ID Number Owner or Operator? Operator UST ID Number 1A, 1B, 1C Facility ID Number Owner or Operator? Owner UST ID Number 1A, 1B, 1C Facility ID Number Owner or Operator? Operator Telephone Number 00-0-0000036548 Name of Owner or Operator Dates of Ownership / Operation Address Telephone Number 00-0-0000036548 1-336-766-9801 P.O. Box 410, Wilkesboro, NC 28697 1-336-766-9801 00-0-0000036548 Name of Owner or Operator Dates of Ownership / Operation Raymer Brothers, Inc. 03/05/2019 - Current Address Fast Track Inc. 11/02/2002 - 03/05/2019 Name of Owner or Operator Dates of Ownership / Operation Address Fast Track Inc. 11/02/2002 - Current P.O. Box 410, Wilkesboro, NC 28697 P.O. Box 327, Troutman, NC 28166 1-704-873-7285 Telephone Number TABLE 1 UST OWNER/OPERATOR INFORMATION FAST TRACK #145 (INCIDENT NO. 40099) Page 1 of 1 Date: 07/15/21 Facility ID # : 00-0-0000036548 Was Release Associated with UST System? (Yes / No) 1A Gasoline NA 12,000 11/1/2002 Double Wall Steel 8' x 32' Other Current Yes 1B Gasoline NA 8,000 11/1/2002 Double Wall Steel 8' x 21' 4" Other Current Yes 1C Diesel NA 5,000 11/1/2002 Double Wall Steel 8' x 13' 6" Other Current Yes TABLE 2 UST SYSTEM INFORMATION FAST TRACK #145 (INCIDENT NO. 40099) Status of UST UST ID No. Current or Most Recent Contents Previous Contents Capacity (gallons) Date Installed Construction Details Tank Dimensions Description of Associated Product Piping and Pumps Page 1 of 1 Facility ID # : 00-0-0000036548 Well ID. Parcel ID No. Well Owner Mailing Address Well Address Well Use (Potable / Non- Potable etc.) Connected to Municipal Water Yes/No Distance from source area of release (ft.) WSW-1 36291167-2327 Rollin Acres, LLC 2421 W NC Highway 10 Newton, NC 28658 2421 W NC Highway 10 Newton, NC 28658 Abandoned 12/10/2015 Unknown ~240' WSW-2 36291157-7137 Jerry & Michael Houser 2120 Peeler Road Vale, NC 28168 3907 Startown Road Newton, NC 28658 Unknown Inactive Unknown ~250' WSW-3 36290767-2635 Glenda R. Mathis & Terry Robinson 5905 Old Shelby Vale, NC 28168 2420 W NC Highway 10 Newton, NC 28658 Unknown Inactive Reportedly Connected ~425' WSW-4 36291157-6481 Startown Tire Center, Inc. 2466 W NC Highway 10 Newton, NC 28658 3867 Startown Road Newton, NC 28658 Unknown Inactive Reportedly Connected ~430' WSW-5 36290757-6636 Gerald & John Arrowood 2433 Poovey Street Newton, NC 28658 2433 Poovey Street Newton, NC 28658 Unknown Inactive Unknown ~500' WSW-6 36291167-8025 Jeanne F. Davis & Brian McCurdy 4133 Wild Partridge Road Charlotte, NC 28226 2393 W NC Highway 10 Newton, NC 28658 Unknown Inactive Unknown ~540' WSW-7 36291156-5735 Dale & Diane Caldwell P.O. Bx 562 Hudson, NC 28638 2511 W NC Highway 10 Newton, NC 28658 Unknown Inactive Reportedly Connected ~620' WSW-8 36291156-4459 Jacqueline Yoder 3991 Startown Road Newton, NC 28658 3967 Startown Road Newton, NC 28658 Unknown Inactive Unknown ~680' WSW-9 36291157-1253 Gena E. Poovey & Noah S. Lindemann 117 Rest Street Gaffney, SC 29340 2506 W NC Highway 10 Newton, NC 28658 Unknown Inactive Unknown ~700' WSW-10 36291156-2820 Cody and Kendra Beal 3993 Joe Crouse Road Maiden, NC 28650 2541 W NC Highway 10 Newton, NC 28658 Unknown Unknown ~750' WSW-11 36290757-3779 Kenneth & Peggy Bissette 2465 Poovey Street Newton, NC 28658 2465 Poovey Street Newton, NC 28658 Unknown Inactive Reportedly Connected ~825' WSW-12 36290758-6014 Shannon M. Mincer 2454 Poovey Street Newton, NC 28658 2454 Poovey Street Newton, NC 28658 Unknown Inactive Reportedly Connected ~900' WSW-13 36290768-2129 Integra Colorado Springs, LLC & Mark S. Judd P.O. Box 167 Hennepin, IL 61327 3802 Startown Road Newton, NC 28658 Unknown Unknown ~900' WSW-14 36290757-3779 Kenneth & Peggy Bissette 2465 Poovey Street Newton, NC 28685 2465 Poovey Street Newton, NC 28658 Unknown Inactive Reportedly Connected ~950' Note: • Water supply well information was obtained from the 2012 LSA report submitted by a previous consultant. • Water supply wells are keyed to Figure 3. TABLE 3 WATER SUPPLY WELL INFORMATION FAST TRACK #145 (INCIDENT NO. 40099) Date: 07/15/21 Page 1 of 1 Date: 07/15/21 Facility ID # : 00-0-0000036548 Parcel Number Owner Name Address 362911670179 (Site) KLR Real Estate, LLC 589 North Main Street Troutman, NC 28166 362911672327 Rollin Acres, LLC 2421 West NC 10 Highway Newton, NC 28658 362911661942 Bonnie Jo Bumgarner 3938 Startown Road Newton, NC 28658 362911566946 Dale & Diane Cynthia Caldwell P.O. Box 562 Hudson, NC 28638 362911577137 Jerry & Michael Houser 2120 Peeler Road Vale, NC 28168 362911576481 Startown Tire Center, Inc. 2466 West NC 10 Highway Newton, NC 28658 362907577597 Stephen Paul Herzig Revocable Living Trust 16137 Connor Court Los Gatos, CA 95032 362907670524 Barakah Investments NC, LLC 419 Commons Park Lane Tucker, GA 30084 362907672635 Glenda R Mathis Terry M Robinson 5905 Old Shelby Road Vale, NC 28168 Note: • Properties are keyed to Figure 3. TABLE 4 ADJACENT PROPERTY OWNER INFORMATION FAST TRACK #145 (INCIDENT NO. 40099) Page 1 of 1 Date: 10/09/23 Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) Comments 07/02/20 23.86 ---73.95 LSA 06/08/21 23.34 ---74.47 02/14/22 25.66 ---72.15 Slight odor 11/10/22 26.79 ---71.02 06/12/23 30.77 ---67.04 09/21/23 32.55 ---65.26 07/02/20 NM NM NM 06/08/21 NM NM NM 07/02/20 21.05 ---78.95 LSA 06/08/21 20.15 ---79.85 02/14/22 23.69 ---76.31 11/10/22 25.24 ---74.76 06/12/23 24.28 ---75.72 09/21/23 25.85 ---74.15 07/02/20 NM NM NM Not Found 06/08/21 NM NM NM Not Found 02/14/22 6.96 ---59.41 Slight odor 11/10/22 NM NM NM 06/12/23 NM NM NM Not Found 09/21/23 NM NM NM Not Found 07/02/20 NM NM NM 06/08/21 NM NM NM 07/02/20 22.46 ---78.04 CSA 06/08/21 21.53 ---78.97 02/14/22 24.96 ---75.54 11/10/22 26.61 ---73.89 06/12/23 26.36 ---74.14 09/21/23 27.11 ---73.39 07/02/20 NM NM NM 06/08/21 NM NM NM 07/02/20 25.02 ---73.62 CSA 06/08/21 24.47 ---74.17 02/14/22 27.23 ---71.41 Sheen/odor 11/10/22 29.58 ---69.06 06/12/23 NM NM NM Dry 09/21/23 NM NM NM Dry 07/02/20 1.91 ---53.95 CSA 06/08/21 NM NM NM Not Found 02/14/22 1.54 ---54.32 11/10/22 1.76 ---54.10 06/12/23 NM NM NM Not Found 09/21/23 NM NM NM Not Found 07/02/20 NM NM NM Not Found 06/08/21 NM NM NM Not Found 02/14/22 2.21 ---56.26 11/10/22 1.90 ---56.57 06/12/23 NM NM NM Not Found 09/21/23 NM NM NM Not Found 07/02/20 NM NM NM 06/08/21 NM NM NM 07/02/20 NM NM NM 06/08/21 NM NM NM 07/02/20 NM NM NM 06/08/21 NM NM NM MW-8 03/11/13 17 17 - 37 37 98.64 55.86133 - 13303/11/13MW-9 MW-10 03/11/13 3 3 - 13 13 58.47 MW-2 MW-5 MW-7 MW-11 11/01/12 03/08/13 Unknown 05/23/13 05/23/13 MW-12 MW-13 99.11 101.78 32 39 37 63.07 101.31 102.97 TABLE 5 WELL CONSTRUCTION AND GAUGING INFORMATION FAST TRACK #145 (INCIDENT NO. 40099) Facility ID # : 00-0-0000036548 19 - 39 17 - 37 Unknown 4 - 14 17 - 37 12 - 32 Unknown 19 17 Unknown 4 17 12 03/11/13 14 37 81.39 MW-1 11/01/12 25 25 - 45 45 97.81 100.003919 - 391911/01/12MW-3 MW-4 11/01/12 4 4 - 19 19 66.37 100.503616 - 361603/08/13MW-6 Page 1 of 2 Date: 10/09/23 Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) Comments TABLE 5 WELL CONSTRUCTION AND GAUGING INFORMATION FAST TRACK #145 (INCIDENT NO. 40099) Facility ID # : 00-0-0000036548 07/02/20 23.06 ---75.87 CSA 06/08/21 22.33 ---76.60 02/14/22 25.99 ---72.94 11/10/22 27.73 ---71.20 06/12/23 26.48 ---72.45 09/21/23 27.27 ---71.66 07/02/20 NM NM NM Not Found 06/08/21 NM NM NM Not Found 02/14/22 2.35 ---53.09 11/10/22 2.48 ---52.96 06/12/23 NM NM NM Not Found 09/21/23 NM NM NM Not Found 07/02/20 NM NM NM 06/08/21 NM NM NM 07/02/20 23.79 ---73.96 06/08/21 NM NM NM Not Accessible 02/14/22 NM NM NM Not Accessible 11/10/22 NM NM NM 06/12/23 NM NM NM Not Found 09/21/23 25.65 ---72.10 Notes: MW-15 05/24/13 4 4 - 14 14 55.44 97.753510 - 3510UnknownMW-17 98.933616 - 361605/24/13MW-14 • ft BGS : feet below ground surface. • NM : Not measured. • Elevation relative to an arbitrary datum of 100.00 feet. 14 53.00MW-16 05/24/13 4 4 - 14 Page 2 of 2 Facility ID # : 00-0-0000036548 Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 70 70 70 400 400 510 110 1,300 6,700 15,000 120 39 2,500 800 3,900 2,150 5,000 260,000 80,000 50,000 20,000 6,000 5,900 30,500 26,100 28,500 24,100 10/23/19 642 11,700 2,350 11,920 134 615 <50.0 86.0 259 1,760 502 07/02/20 2,560 6,180 1,790 7,230 <25 362 <25 42.3 J 161 1,200 294 06/08/21 104 1,970 1,260 6,030 25.5 257 12.2 J 42.4 J 155 1,290 313 02/14/22 2,250 11,500 2,000 10,600 <63 421 <63 <63 190 J 1,470 509 11/10/22 1,750 3,370 1,420 4,880 40.1 493 30.6 82.5 209 1,090 308 06/12/23 1,840 4,550 486 3,770 <14.0 969 24.7 J 26.9 J 90.9 1,510 340 09/21/23 828 1,700 232 1,380 <14.0 940 <18.0 <18.0 <19.0 258 59.4 07/02/20 NS NS NS NS NS NS NS NS NS NS NS 06/08/21 NS NS NS NS NS NS NS NS NS NS NS 10/23/19 90.6 3.74 35.5 3.41 <0.500 13.2 15.9 15.5 18.4 11.8 6.86 07/02/20 23.2 0.76 5.8 1.7 <0.13 6.5 4.1 6.0 4.2 0.86 0.94 06/08/21 25.3 0.41 J 8.8 0.44 J <0.13 6.1 6.0 12.3 6.2 0.27 J <0.13 02/14/22 26.1 <0.13 1.3 <0.25 <0.13 6.6 8.5 9.5 6.5 0.14 J <0.13 11/10/22 39.7 0.621 1.89 0.706 J 1.62 9.23 11.6 7.91 7.89 0.363 J <0.180 06/12/23 34.6 3.76 1.81 10.6 1.10 11.3 10.6 6.96 6.80 1.81 1.58 09/21/23 29.4 3.07 1.24 9.36 <0.140 6.80 10.4 5.54 4.26 1.18 1.65 10/23/19 4,130 1,730 3,080 5,220 56.0 781 <50.0 111 320 1,540 412 07/02/20 NS NS NS NS NS NS NS NS NS NS NS 06/08/21 NS NS NS NS NS NS NS NS NS NS NS 02/14/22 1,940 1,250 2,580 4,460 <13 551 <13 74.9 213 1,110 311 11/10/22 NS NS NS NS NS NS NS NS NS NS NS 06/12/23 NS NS NS NS NS NS NS NS NS NS NS 09/21/23 NS NS NS NS NS NS NS NS NS NS NS 07/02/20 NS NS NS NS NS NS NS NS NS NS NS 06/08/21 NS NS NS NS NS NS NS NS NS NS NS 10/23/19 12,200 27,200 2,630 15,240 <100 766 <100 106 310 2,350 678 07/02/20 12,900 43,700 2,910 14,700 <130 509 <130 <130 261 J 1,570 482 J 06/08/21 8,110 21,200 1,670 8,560 <63 274 <63 <63 195 J 1,310 397 02/14/22 11,200 44,000 3,300 17,800 <130 662 <130 <130 319 J 2,280 708 11/10/22 9,380 33,100 2,790 14,000 <14.0 698 51.2 134 412 2,700 743 06/12/23 8,850 23,100 1,940 10,900 <14.0 588 44.6 J 92.3 290 2,070 601 09/21/23 8,790 28,100 2,640 14,300 <14.0 730 34.9 J 99.8 315 2,560 687 MW-7 07/02/20 NS NS NS NS NS NS NS NS NS NS NS 10/23/19 8,400 24,700 3,900 21,660 <50.0 1,170 <50.0 157 453 3,310 959 07/02/20 5,650 33,800 3,090 16,300 <130 635 <130 <130 274 J 1,870 543 06/08/21 8,620 36,500 3,270 18,100 <130 512 <130 <130 286 J 1,970 576 02/14/22 3,840 68,800 E 14,500 81,200 <130 8,460 1,280 1,300 5,390 37,600 11,100 11/10/22 4,010 39,100 3,620 17,900 <14.0 771 34.9 J 137 399 2,860 733 06/12/23 NS NS NS NS NS NS NS NS NS NS NS 09/21/23 NS NS NS NS NS NS NS NS NS NS NS 07/02/20 51.0 1.9 2.3 <0.50 <0.25 2.5 0.87 J 3.1 0.57 J <0.25 <0.25 06/08/21 NS NS NS NS NS NS NS NS NS NS NS 02/14/22 0.95 J <0.63 <0.63 <1.3 <0.63 0.74 J <0.63 <0.63 <0.63 0.79 J <0.63 11/10/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180 06/12/23 NS NS NS NS NS NS NS NS NS NS NS 09/21/23 NS NS NS NS NS NS NS NS NS NS NS 10/23/19 <0.500 <0.500 <0.500 <1.500 3.42 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 07/02/20 NS NS NS NS NS NS NS NS NS NS NS 06/08/21 NS NS NS NS NS NS NS NS NS NS NS 02/14/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 11/10/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180 06/12/23 NS NS NS NS NS NS NS NS NS NS NS 09/21/23 NS NS NS NS NS NS NS NS NS NS NS 07/02/20 NS NS NS NS NS NS NS NS NS NS NS 06/08/21 NS NS NS NS NS NS NS NS NS NS NS 07/02/20 NS NS NS NS NS NS NS NS NS NS NS 06/08/21 NS NS NS NS NS NS NS NS NS NS NS 07/02/20 NS NS NS NS NS NS NS NS NS NS NS 06/08/21 NS NS NS NS NS NS NS NS NS NS NS MW-3 MW-1 Date: 10/09/23 Analytical Method → MACs (μg/l) GCL (μg/l) Contaminant of Concern →BenzeneTolueneEthylbenzeneMW-10 MW-9 MW-8 MW-6 MW-4 10 x 2B Standards (µg/l) MW-2 TABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS FAST TRACK #145 (INCIDENT NO. 40099)Total XylenesMTBEn-Butylbenzenen-PropylbenzeneNaphthaleneMW-5 EPA Method 6200B Isopropylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMW-11 MW-12 MW-13 Page 1 of 2 Facility ID # : 00-0-0000036548 Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 70 70 70 400 400 510 110 1,300 6,700 15,000 120 39 2,500 800 3,900 2,150 5,000 260,000 80,000 50,000 20,000 6,000 5,900 30,500 26,100 28,500 24,100 Date: 10/09/23 Analytical Method → MACs (μg/l) GCL (μg/l) Contaminant of Concern →BenzeneTolueneEthylbenzene10 x 2B Standards (µg/l) TABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS FAST TRACK #145 (INCIDENT NO. 40099)Total XylenesMTBEn-Butylbenzenen-PropylbenzeneNaphthaleneEPA Method 6200B Isopropylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene10/23/19 <0.500 <0.500 <0.500 <1.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 07/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 06/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 02/14/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 11/10/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180 06/12/23 22.5 57.0 7.00 51.4 <0.140 <0.470 <0.180 0.562 1.13 9.88 5.67 09/21/23 133 193 32.7 235 <0.140 <0.470 2.79 2.07 3.94 55.7 23.1 10/23/19 <0.500 <0.500 <0.500 <1.500 2.45 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 07/02/20 NS NS NS NS NS NS NS NS NS NS NS 06/08/21 NS NS NS NS NS NS NS NS NS NS NS 02/14/22 10.3 0.56 1.3 1.5 1.5 0.90 <0.13 0.81 0.15 J 0.20 J <0.13 11/10/22 0.529 <0.220 <0.170 <0.210 0.792 J <0.470 <0.180 0.206 J <0.190 <0.190 <0.180 06/12/23 NS NS NS NS NS NS NS NS NS NS NS 09/21/23 NS NS NS NS NS NS NS NS NS NS NS 07/02/20 NS NS NS NS NS NS NS NS NS NS NS 06/08/21 NS NS NS NS NS NS NS NS NS NS NS 10/23/19 99.7 356 44.9 204.9 <5.00 12.7 <5.00 <5.00 6.40 37.5 8.30 07/02/20 2,590 8,080 1,430 6,540 <25 250 <25 37.4 J 142 965 256 06/08/21 NS NS NS NS NS NS NS NS NS NS NS 02/14/22 NS NS NS NS NS NS NS NS NS NS NS 11/10/22 NS NS NS NS NS NS NS NS NS NS NS 06/12/23 NS NS NS NS NS NS NS NS NS NS NS 09/21/23 <18.0 107 137 1,360 <14.0 902 <18.0 22.1 J 88.3 1,140 255 10/23/19 3.53 0.600 0.500 <1.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 07/02/20 06/08/21 02/14/22 11/10/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180 06/12/23 09/21/23 10/23/19 49 17.7 13.4 15.46 <0.500 7.37 <0.500 2.40 2.17 2.69 2.24 07/02/20 06/08/21 07/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 06/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 02/14/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 11/10/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180 06/12/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180 09/21/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180 Notes: • 2B Standards: North Carolina Surface Water Standards for Class C waters specified in T15A NCAC 2B.0200. • October 23, 2019 laboratory results from the Groundwater Monitoring Report by Paragon Environmental Consultants, Inc. dated November 4, 2019. Dry Dry Dry • For other compounds reported which did not exceed the MACs, refer to the laboratory reports. Creek Sample #2 • Other compounds exceeding the MACs: 6/8/21 - methylene chloride in MW-8. • Other compounds exceeding the MAC: 11/10/22 - styrene and p-isopropyltoluene in MW-8. • Other compounds exceeding the MACs: 2/14/22 - methylene chloride in MW-1, MW-6, and MW-8 and p-isopropyltoluene and styrene in MW-8. • Concentrations in italics indicate the GCLs were below the reported concentrations. • Concentrations in bold face type indicate the MACs were below the reported concentrations. • J: Estimated value. • Results reported in µg/l (micrograms per liter) • MAC: Maximum Allowable Concenration as specified in T15A NCAC 2L.0202. • GCL: Gross contamination level. • NE: Standard not established. • < : Less than the method detection limit specified in the laboratory report. • NS: Not sampled. Dry TRIP BLANK Creek Sample #1 MW-17 MW-15 MW-14 Dry Dry MW-16 Dry Page 2 of 2 Facility ID # : 00-0-0000036548 SVE AS SVE AS 07/17/23 11:25-14:05 Scheduled 2.75 Collected system readings, checked oil levels, adjusted flows and collected air sample 1,710 1,620 1,711 1,621 08/21/23 07:45-10:15 Scheduled 2.50 Collected system readings, checked oil levels, adjusted flows and collected air sample 2,540 2,450 2,542 2,452 09/19/23 09:30-11:45 Scheduled 2.25 Collected system readings, checked oil levels, adjusted flows and collected air sample 3,238 3,148 3,240 3,150 7.50 Total Operational Hours SVE: 1,438 AS: 1,439 Note: TABLE 7 SUMMARY OF REMEDIATION SYSTEM O&M VISITS FAST TRACK #145 (INCIDENT NO. 40099) Date: 10/10/23 • Operation and Maintenance (hrs.) includes only time spent onsite. Hour Meter Reading Upon Departure Hour Meter Reading Upon Arrival Date (mm/dd/yy)Site Purpose of Maintenance Visit (Scheduled or Unscheduled) O&M (hrs.)Description of Maintance Activities Total (hrs) Facility ID # : 00-0-0000036548 Benzene Toluene Ethylbenzene Xylenes Total BTEX TRPH 04/10/23 <3.1 <2.3 <2.3 <6.9 <14.6 NR 05/04/23 <3.1 <2.3 <2.3 <6.9 <14.6 <31 05/11/23 <3.1 <2.3 <2.3 <6.9 <14.6 55 06/12/23 <3.1 <2.3 <2.3 <6.9 <14.6 <31 07/17/23 <3.1 <2.6 <2.3 <6.9 <14.9 34 08/21/23 <3.1 <2.6 <2.3 <6.9 <14.9 <31 09/19/23 <3.1 <2.6 <2.3 <6.9 <14.9 <31 Notes: • Results reported in ppmv (parts per million volume). • *Air samples collected from the exhaust of the vacuum blower may be named differently in the lab report. • <: Less than the method detection limit specified in the laboratory report. • NR: Not Reported. • TRPH is based on benzene. SVE EXHAUST* TABLE 8 SUMMARY OF AIR ANALYTICAL RESULTS FAST TRACK #145 (INCIDENT NO. 40099) Date: 10/11/23 Well No.Sample Date (mm/dd/yy) EPA METHOD 18 Parge 1 of 1 APPENDICES APPENDIX A State Correspondence July 17, 2023 Raymer Oil Company 589 North Main Street Troutman, North Carolina 28166 Attention: Matthew Redmond Re: Fast Track #145 2443 NC Highway 10 West, Newton Catawba County Incident Number: 40099 Risk Classification: Intermediate Ranking: I125D Dear Mr. Redmond: On June 30, 2023, the Underground Storage Tank Section of the Division of Waste Management, Mooresville Regional Office, received the Corrective Action Performance Report for the above-referenced site. This information has been reviewed and will remain in the UST Section’s files. Per the NORR dated March 28, 2022, sampling should be conducted on a quarterly basis for the first year of system operation. The next sampling event should therefore be conducted September 2023, with the CAPR received by this office no later than October 31, 2023. If monitoring wells MW-4 and MW-17 cannot be located and/or accessed during the September 2023 groundwater sampling event, they must be replaced prior to the December 2023 groundwater sampling event. If you have any questions regarding the actions that must be taken, or the rules mentioned in this letter, please contact me at the address or telephone number listed below for the Mooresville Regional Office. Sincerely, Brad C. Newton, P.G. Hydrogeologist Mooresville Regional Office UST Section, Division of Waste Management, NCDEQ cc: Joanna Alley – Geologic Resources, Inc. (via e-mail) Catawba County Health Department 5398 Received JUL 18 2023 Site Name City / County /Catawba Incident #40099 Resp Pty Name / Contact Incident Mgr Region MORRP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #23 Consultant / Project Mgr /Joanna R Alley Telephone / Fax Number /Task Authorization Number:24 ChangeOrd: Project Mgr Email Site Risk / Rank / Abatement:I125D RRA Date: Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%) Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date) With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?  Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab / SubCode RO AuthProposed Rate/Price (Consultant)CO AuthProposed Task Subtotal (Consultant) Final Preapproved Subtotal (UST Section) Claimed Amount3 (Consultant) 4.031 10 /wells y $110.00 Y $1,100.00 $1,100.00 / 4.051 1 /sample pt.y $50.00 Y $50.00 $50.00 / 4.090 #272 12 /samples y $66.00 Y $792.00 $792.00 / 4.090 #880 3 /samples y $151.00 Y $453.00 $453.00 / 4.091 3 /shipments y $60.00 Y $180.00 $180.00 / 6.090 1 /report y $1,125.00 Y $1,125.00 $1,125.00 / 7.201 15 /hours y $93.00 Y $1,395.00 $1,395.00 / 7.250 1 /system y $2,000.00 Y $2,000.00 $2,000.00 / 7.260 1 /system y $3,300.00 Y $3,300.00 $3,300.00 / 12.050 3 /trips y $250.00 Y $750.00 $750.00 / 12.055 3 /trips y $50.00 Y $150.00 $150.00 / // // // // // // // // // // // // // // // // Requested Preapproved Claimed 3 TOTAL:$11,295.00 $11,295.00 TOTAL: Total Standard Costs (Not Third Party)$11,295.00 $11,295.00 Total Standard Costs Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty CostsProcess Tracking (Date) TA Submittal:6/30/23 by:(PM)(Reserved for RO) RO Review:7/3/23 by:(IM)Joint UST Preapproval Confirmed By:Date1 7/3/2023 CO Review:7/3/23 by:(STF)RP or Designee Receipt Confirmation By:Date 4 1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable. 3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned. 4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/costnegotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RPis not to be modified without written consent by all signatories. 5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full. DWM/UST ePATA 4/1/2022 JRA Proposed Units / Type (Consultant) YES23-421 July-September 2023 704-845-4012 Dates of Work (Consultant) Started1 / Completed2 FINAL REIMBURSEMENT JRA@geologicalresourcesinc.com Raymer Oil Company Matthew Redmond Geological Resources, Inc. DIRECTED COSTS Newton (Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization) Owner/Operator 704-845-4010 (Reserved for Incident Manager) PREAPPROVAL / TASK AUTHORIZATION Fast Track 145 Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA, you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA requestdesignated as a "Change Order" in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been completed within 12months ofthe completion date of the FIRST completed task to remain within the Statute ofLimitations.All ePATAs submitted withina claim areclosed with that claim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimedamount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and necessary expenses per 15A NCAC 2P .0402 and .0404. bcn LP (Initials) ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORMDept of Environmental Quality -Division of Waste Management APPENDIX B Land Use Information Date: 06/29/23 Facility ID # : 00-0-0000036548 Map ID No. Land Use Feature Zoning Description Address Distance from Source Area (feet) n/a B-2 Business n/a n/a n/a PD-SC Planned Development Shopping Center n/a n/a n/a R-20 Residential n/a n/a n/a R-20A Residential n/a n/a 1 Fresenius Kedney Care Newton PD-SC Doctor's Office 3802 Startown Road Newton, NC 28658 ~990 2 St. Paul Lutheran Church R-20 Church 3761 Startown Road Newton, NC 28658 ~1,095 Note: • Properties are keyed to Figure 3B. APPENDIX B LAND USE INFORMATION FAST TRACK #145 (INCIDENT NO. 40099) Page 1 of 1 APPENDIX C Incident Reports NCDEQ Incident Report RP/Company FAST TRACK, INC. RPAddress P.O. BOX 410 RPCity WILKESBORO Contact J.C. FAW RPState NC TELEPHONE IncidentNumber 40099 USTNum MO-8561 IncidentName FAST TRACK #145 FacilID 00-0-0000036548 Address 2443 WEST NC 10 HIGHWAY CityTown NEWTON State NC ZipCode 28658- DateOccurred 7 /5 /2012 DateReported 8 /9 /2012 ConfRisk I CloseOut COMMENT system operational by 110-31-21 RptType Rcvd Rvwd Appvd Incident Mgr BCNLongitude-81.268361 Latitude 35.644438 County CATAW LSA2 12/3/2012 12/20/2012 12/20/2012 CSAS 1/14/2014 2/20/2014 2/20/2014 CAP 11/24/2014 12/15/2014 MRPI 5/31/2016 6/2/2016 6/2/2016 RMR 5/15/2017 6/2/2017 6/2/2017 Tuesday, October 10, 2023 Page 1 of 2 RMR 11/9/2017 11/29/2017 11/29/2017 RMR 5/24/2018 6/6/2018 6/6/2018 RMR 12/3/2018 12/17/2018 12/17/2018 RMR 5/30/2019 6/10/2019 6/10/2019 RMR 9/1/2020 9/9/2020 9/9/2020 MRP 7/20/2021 7/28/2021 7/28/2021 MRP 11/29/2022 12/15/2022 12/15/2022 CAPR 7/3/2023 7/17/2023 7/17/2023 Tuesday, October 10, 2023 Page 2 of 2 NCDEQ Incident Report RP/Company PETROLEUM WORLD, INC. RPAddress 681 NC 120 HWY RPCity MOORESBORO Contact DEBBIE SAILORS RPState NC TELEPHONE IncidentNumber 10359 USTNum MO-3817 IncidentName QUICK STOP #76 FacilID 00-0-0000007821 Address 2442 NC HIGHWAY 10 WEST CityTown NEWTON State NC ZipCode 28658- DateOccurred 2 /10/1993 DateReported 5 /31/1995 ConfRisk L CloseOut 8/29/2016 COMMENT WSW-1 REPORTEDLY ABANDONED PRIOR TO CONSTRUCTION OF CAR WASH ON THAT PROPERTY. NO DOCUMENTATION PROVIDED. RptType Rcvd Rvwd Appvd Incident Mgr BCNLongitude-81.268775 Latitude 35.645419 County CATAW CSA 3/1/1996 5/30/1996 CAP 12/27/1996 9/11/1997 9/11/1997 RMR 9/9/2002 9/25/2002 9/24/2002 RMR 3/3/2003 3/21/2003 3/21/2003 RMR 8/29/2003 9/17/2003 9/17/2003 Thursday, June 29, 2023 Page 1 of 3 RMR 3/3/2004 4/8/2004 4/8/2004 RMR 8/31/2004 9/10/2004 9/15/2004 RMR 8/23/2007 9/7/2007 9/7/2007 RMR 2/15/2008 3/4/2008 3/4/2008 RMR 8/7/2008 8/14/2008 8/14/2008 RMR 1/29/2009 2/16/2009 2/16/2009 RMR 7/15/2009 7/22/2009 7/22/2009 RMR 2/1/2010 2/18/2010 2/18/2010 RMR 7/20/2010 8/5/2010 8/5/2010 RMR 2/1/2011 2/15/2011 2/15/2011 Thursday, June 29, 2023 Page 2 of 3 RMR 8/1/2011 8/15/2011 8/15/2011 RMR 1/30/2012 2/17/2012 2/17/2012 RMR 8/8/2012 8/31/2012 8/31/2012 RMR 2/6/2013 2/22/2013 2/22/2013 RMR 2/3/2014 3/7/2014 3/7/2014 RMR 8/5/2014 8/22/2014 8/22/2014 RMR 1/30/2015 2/24/2015 2/24/2015 RMR 7/24/2015 8/18/2015 8/18/2015 DR 8/26/2016 8/29/2016 8/29/2016 PN 10/12/2016 Thursday, June 29, 2023 Page 3 of 3 NCDEQ Incident Information RP/Company ROAM K. JARRETT Contact ROAM K. JARRETT RPAddress 3910 STARTOWN-LINCOLNTON RPCity NEWTON RPZipCode 28658- RPState NC TELEPHONE 8284642482 IncidentNumber 22431 IncidentName STARTOWN SERVICE (J.C. FAW PROP.) Address 3910 STARTOWN-LINCOLNTON HWY. CityTown NEWTON State NC County CATAWZipCode28658- Lattitude 35.644553 Longitude -81.268736 COMMENT 3 GAS UST'S CLOSED 8/15/91. REPORT NEVER SUBMITTED. 10 PPM DETECTED UNDER ONE TANK. THEY WANT TO DO ADD. SOIL SAMPLES AND RUN RISK-BASED. WE NEED SAMPLES UNDER LINES AND DISPENSER TOO. DateOccurred 8 /15/1991 DateReported 9 /25/2000 CloseOut 2/2/2004 FacilID 00-0-000000704 USTNum MO-6009 Mgr FTF Conf Risk L Site Priority Thursday, June 29, 2023 Page 1 of 1 APPENDIX D Historical Soil Quality Information APPENDIX E Laboratory Analytical Reports   Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.   7/20/2023 Geological Resources, Inc. Joanna Alley 3502 Hayes Road Monroe, NC, 28110 Ref: Analytical Testing Lab Report Number: 23-198-0010 Client Project Description: Fast Track 145 GRI #5398 Dear Joanna Alley: Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/17/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Page 1 of 12 Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date 07/31/202337735State ProgramNorth Carolina 12/31/2023402State ProgramNorth Carolina 07/31/202399012State ProgramSouth Carolina 12/31/202299012State ProgramSouth Carolina Page 1 of 1 00016/23-198-0010 Page 2 of 12 Report Number: Sample Summary Table Client Project Description: 23-198-0010 Fast Track 145 GRI #5398 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 07/17/2023 13:58Air 89826 AS-1 07/17/2023 15:13 SUBCONTRACT AES AES: Analytical Environmental Services, Inc., Atlanta, GA Page 3 of 12 July 20, 2023 LABORATORY REPORT NUMBER PROJECT ID Primary Data Review By Project Manager, AES 2307G32 Terri W Cole Waypoint Analytical 449 Springbrook Road Charlotte NC 28217 23-198-0010 Chris Pafford Project Manager, Access Analytical Ashley Amick PLEASE NOTE: -Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. -AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 - AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. - Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed Secondary Data Review By ATTENTION DATE CLIENT ANALYTICAL REPORT Page 1 of 7Page 4 of 12 Page 2 of 7Page 5 of 12 Analytical Results for 20-Jul-23Date: Workorder: Client Reference: Qual Date Analyzed /Analyst Reportin gLimit (ug) Concentration Total (ug) (mg/m3) (ppm) Analyte 2307G32 Waypoint Analytical 23-198-0010 Front (ug) Back (ug) Test Method 7/17/2023Lab ID:89826 Tedlar Bag 1Air Vol.(L):Media:Client ID:2307G32-001A Date Sampled: <3.1<10Benzene <10 10 EPA187/19/2023 BHI<10 <10 <2.3<10Ethylbenzene <10 10 EPA187/19/2023 BHI<10 <10 <4.6<20m,p-Xylene <20 20 EPA187/19/2023 BHI<20 <20 <2.3<10o-Xylene <10 10 EPA187/19/2023 BHI<10 <10 <2.6<10Toluene <10 10 EPA187/19/2023 BHI<10 <10 <250TPH (Gasoline) <250 250 SW8015BM7/19/2023 BHI<250 <250 34110TRPH (Based on Benzene) 110 100 EPA187/19/2023 BHI108.702 <100 85 Surr:1,4 Difluorobenzene 85 0 SW8015BM7/19/2023 BHI85.062 Qualifiers: < Less than the indicated Reporting Limit H Holding time for preparation or analysis B Analyte detected in the associated Method Blank (a) Analysis indicates possible breakthrough; back section result is greater than % of the front section result.10 Page 3 of 7Page 6 of 12 Page 4 of 7Page 7 of 12 20-Jul-23Date:Analytical Environmental Services, Inc Client: BatchID:Workorder: Project Name ANALYTICAL QC SUMMARY REPORT 23-198-0010 2307G32 Waypoint Analytical 359866 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:359866MBLK07/18/2023Aromatic Volatiles in Air EPA18 Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 07/14/2023 521621MB-359866 12333265 Benzene 10BRL Ethylbenzene 10BRL m,p-Xylene 20BRL o-Xylene 10BRL Toluene 10BRL TRPH (Based on Benzene) 100BRL RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:359866MBLK07/18/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 07/14/2023 521641MB-359866 12333897 TPH (Gasoline)250BRL Surr: 1,4 Difluorobenzene 084.59 100.0 84.6 67.1 119 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:359866LCS07/18/2023Aromatic Volatiles in Air EPA18 Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 07/14/2023 521621LCS-359866 12333266 Benzene 10101.2 100.0 101 82.3 119 Ethylbenzene 10104.8 100.0 105 83.7 126 m,p-Xylene 20202.8 200.0 101 81.3 124 o-Xylene 1096.79 100.0 96.8 78.4 123 Toluene 10101.1 100.0 101 82 124 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:359866LCS 07/18/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 07/14/2023 521641LCS-359866-2 12333898 Qualifiers: J Estimated value detected below Reporting Limit BRL Below reporting limit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank E Estimated (value above quantitation range) S Spike Recovery outside limits due to matrix < Less than Result value> Greater than Result value R RPD outside limits due to matrix Rpt Lim Reporting Limit Page 5 of 7Page 8 of 12 20-Jul-23Date:Analytical Environmental Services, Inc Client: BatchID:Workorder: Project Name ANALYTICAL QC SUMMARY REPORT 23-198-0010 2307G32 Waypoint Analytical 359866 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:359866LCS07/18/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 07/14/2023 521641LCS-359866-2 12333898 TPH (Gasoline)250989.6 1000 99.0 75.1 120 Surr: 1,4 Difluorobenzene 089.18 100.0 89.2 67.1 119 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:359866LCSD07/18/2023Aromatic Volatiles in Air EPA18 Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 07/14/2023 521621LCSD-359866 12333267 Benzene 10102.9 15100.0 103 82.3 119 101.2 1.68 Ethylbenzene 10106.6 15100.0 107 83.7 126 104.8 1.63 m,p-Xylene 20206.0 15200.0 103 81.3 124 202.8 1.57 o-Xylene 1098.31 15100.0 98.3 78.4 123 96.79 1.56 Toluene 10102.5 15100.0 103 82 124 101.1 1.46 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:359866LCSD07/18/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 07/14/2023 521641LCSD-359866-2 12333899 TPH (Gasoline)2501027 27.71000 103 75.1 120 989.6 3.69 Surr: 1,4 Difluorobenzene 091.48 0100.0 91.5 67.1 119 89.18 0 Qualifiers: J Estimated value detected below Reporting Limit BRL Below reporting limit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank E Estimated (value above quantitation range) S Spike Recovery outside limits due to matrix < Less than Result value> Greater than Result value R RPD outside limits due to matrix Rpt Lim Reporting Limit Page 6 of 7Page 9 of 12 End of Report Page 7 of 7Page 10 of 12 Fed Ex UPS US Postal Client Lab Courier Other : Shipment Receipt Form Customer Number: Customer Name: Report Number:23-198-0010 Geological Resources, Inc. 00087 Shipping Method Shipping container/cooler uncompromised? Thermometer ID:N/A Chain of Custody (COC) present?Yes No Yes No Not Present Yes No Not Present Yes No COC agrees with sample label(s)? Yes No COC properly completed Samples in proper containers? Sample containers intact? Sufficient sample volume for indicated test(s)? All samples received within holding time? Cooler temperature in compliance? Yes No Yes No Yes No Yes No Yes No Yes NoCooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Yes No N/A Yes No N/A Yes No N/ASoil VOA method 5035 – compliance criteria met Water - Sample containers properly preserved Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) High concentration container (48 hr) Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Number of coolers/boxes received Yes No 1 Signature:Angelo Norvell Date & Time:07/17/2023 15:18:58 Special precautions or instructions included? Comments: Page 11 of 12 Page 12 of 12   Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.   8/31/2023 Geological Resources, Inc. Joanna Alley 3502 Hayes Road Monroe, NC, 28110 Ref: Analytical Testing Lab Report Number: 23-233-0006 Client Project Description: Fast Track #145 GRI #5398 Dear Joanna Alley: Waypoint Analytical, LLC (Charlotte) received sample(s) on 8/21/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Page 1 of 12 Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date 07/31/202437735State ProgramNorth Carolina 12/31/2023402State ProgramNorth Carolina 07/31/202399012State ProgramSouth Carolina 12/31/202299012State ProgramSouth Carolina Page 1 of 1 00016/23-233-0006 Page 2 of 12 Report Number: Sample Summary Table Client Project Description: 23-233-0006 Fast Track #145 GRI #5398 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 08/21/2023 08:15Air 93059 AIR 08/21/2023 10:55 SUBCONTRACT AES AES: Analytical Environmental Services, Inc., Atlanta, GA Page 3 of 12 August 28, 2023 LABORATORY REPORT NUMBER PROJECT ID Primary Data Review By Project Manager, AES 2308Q03 Terri W Cole Waypoint Analytical 449 Springbrook Road Charlotte NC 28217 23-233-0006 Chris Pafford Project Manager, Access Analytical Ashley Amick PLEASE NOTE: -Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. -AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 - AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. - Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed Secondary Data Review By ATTENTION DATE CLIENT ANALYTICAL REPORT Page 1 of 7Page 4 of 12 Page 2 of 7Page 5 of 12 Analytical Results for 28-Aug-23Date: Workorder: Client Reference: Qual Date Analyzed /Analyst Reportin gLimit (ug) Concentration Total (ug) (mg/m3) (ppm) Analyte 2308Q03 Waypoint Analytical 23-233-0006 Front (ug) Back (ug) Test Method 8/21/2023Lab ID:92059 Tedlar Bag 1Air Vol.(L):Media:Client ID:2308Q03-001A Date Sampled: <3.1<10Benzene <10 10 EPA188/25/2023 BHI<10 <10 <2.3<10Ethylbenzene <10 10 EPA188/25/2023 BHI<10 <10 <4.6<20m,p-Xylene <20 20 EPA188/25/2023 BHI<20 <20 <2.3<10o-Xylene <10 10 EPA188/25/2023 BHI<10 <10 <2.6<10Toluene <10 10 EPA188/25/2023 BHI<10 <10 <250TPH (Gasoline) <250 250 SW8015BM8/25/2023 BHI<250 <250 <31<100TRPH (Based on Benzene) <100 100 EPA188/25/2023 BHI<100 <100 76 Surr:1,4 Difluorobenzene 76 0 SW8015BM8/25/2023 BHI75.96 Qualifiers: < Less than the indicated Reporting Limit H Holding time for preparation or analysis B Analyte detected in the associated Method Blank (a) Analysis indicates possible breakthrough; back section result is greater than % of the front section result.10 Page 3 of 7Page 6 of 12 Page 4 of 7Page 7 of 12 28-Aug-23Date:Analytical Environmental Services, Inc Client: BatchID:Workorder: Project Name ANALYTICAL QC SUMMARY REPORT 23-233-0006 2308Q03 Waypoint Analytical 361964 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:361964MBLK08/25/2023Aromatic Volatiles in Air EPA18 Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 08/22/2023 524649MB-361964 12420245 Benzene 10BRL Ethylbenzene 10BRL m,p-Xylene 20BRL o-Xylene 10BRL Toluene 10BRL TRPH (Based on Benzene) 100BRL RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:361964MBLK08/25/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 08/22/2023 524650MB-361964 12420420 TPH (Gasoline)250BRL Surr: 1,4 Difluorobenzene 091.51 100.0 91.5 67.1 119 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:361964LCS08/25/2023Aromatic Volatiles in Air EPA18 Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 08/22/2023 524649LCS-361964 12420247 Benzene 10116.0 100.0 116 82.3 119 Ethylbenzene 10122.2 100.0 122 83.7 126 m,p-Xylene 20236.7 200.0 118 81.3 124 o-Xylene 10113.8 100.0 114 78.4 123 Toluene 10117.0 100.0 117 82 124 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:361964LCS08/25/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 08/22/2023 524650LCS-361964-2 12420421 Qualifiers: J Estimated value detected below Reporting Limit BRL Below reporting limit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank E Estimated (value above quantitation range) S Spike Recovery outside limits due to matrix < Less than Result value> Greater than Result value R RPD outside limits due to matrix Rpt Lim Reporting Limit Page 5 of 7Page 8 of 12 28-Aug-23Date:Analytical Environmental Services, Inc Client: BatchID:Workorder: Project Name ANALYTICAL QC SUMMARY REPORT 23-233-0006 2308Q03 Waypoint Analytical 361964 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:361964LCS08/25/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 08/22/2023 524650LCS-361964-2 12420421 TPH (Gasoline)2501149 1000 115 75.1 120 Surr: 1,4 Difluorobenzene 099.65 100.0 99.7 67.1 119 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:361964LCSD08/25/2023Aromatic Volatiles in Air EPA18 Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 08/22/2023 524649LCSD-361964 12420248 Benzene 10100.9 15100.0 101 82.3 119 116.0 13.9 Ethylbenzene 10105.4 15100.0 105 83.7 126 122.2 14.7 m,p-Xylene 20204.1 15200.0 102 81.3 124 236.7 14.8 o-Xylene 1098.16 15100.0 98.2 78.4 123 113.8 14.8 Toluene 10101.3 15100.0 101 82 124 117.0 14.3 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:361964LCSD08/25/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 08/22/2023 524650LCSD-361964-2 12420422 TPH (Gasoline)2501009 27.71000 101 75.1 120 1149 12.9 Surr: 1,4 Difluorobenzene 086.86 0100.0 86.9 67.1 119 99.65 0 Qualifiers: J Estimated value detected below Reporting Limit BRL Below reporting limit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank E Estimated (value above quantitation range) S Spike Recovery outside limits due to matrix < Less than Result value> Greater than Result value R RPD outside limits due to matrix Rpt Lim Reporting Limit Page 6 of 7Page 9 of 12 End of Report Page 7 of 7Page 10 of 12 Fed Ex UPS US Postal Client Lab Courier Other : Shipment Receipt Form Customer Number: Customer Name: Report Number:23-233-0006 Geological Resources, Inc. 00087 Shipping Method Shipping container/cooler uncompromised? Thermometer ID:NA Chain of Custody (COC) present?Yes No Yes No Not Present Yes No Not Present Yes No COC agrees with sample label(s)? Yes No COC properly completed Samples in proper containers? Sample containers intact? Sufficient sample volume for indicated test(s)? All samples received within holding time? Cooler temperature in compliance? Yes No Yes No Yes No Yes No Yes No Yes NoCooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Yes No N/A Yes No N/A Yes No N/ASoil VOA method 5035 – compliance criteria met Water - Sample containers properly preserved Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) High concentration container (48 hr) Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Number of coolers/boxes received Yes No 1 Signature:Angelo Norvell Date & Time:08/21/2023 11:13:14 Special precautions or instructions included? Comments: Page 11 of 12 Page 12 of 12   Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.   9/29/2023 Geological Resources, Inc. Joanna Alley 3502 Hayes Road Monroe, NC, 28110 Ref: Analytical Testing Lab Report Number: 23-264-0030 Client Project Description: Fast Track #145 GRI #5398 Dear Joanna Alley: Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/21/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Page 1 of 49 Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date 07/31/202437735State ProgramNorth Carolina 12/31/2023402State ProgramNorth Carolina 07/31/202499012State ProgramSouth Carolina 12/31/202399012State ProgramSouth Carolina Page 1 of 1 00016/23-264-0030 Page 2 of 49 Report Number: Sample Summary Table Client Project Description: 23-264-0030 Fast Track #145 GRI #5398 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 09/21/2023 09:23Aqueous 95894 MW-1 09/21/2023 13:40 09/21/2023 09:32Aqueous 95895 MW-3 09/21/2023 13:40 09/21/2023 09:44Aqueous 95896 MW-6 09/21/2023 13:40 09/21/2023 09:00Aqueous 95897 MW-14 09/21/2023 13:40 09/21/2023 09:11Aqueous 95898 MW-17 09/21/2023 13:40 09/21/2023 08:00Aqueous 95899 TB 09/21/2023 13:40 09/19/2023 11:58Air 95900 Air 09/21/2023 13:40 SUBCONTRACT AES AES: Analytical Environmental Services, Inc., Atlanta, GA Page 3 of 49 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-264-0030 Report Limit Project:Fast Track #145 V 95894MW-1 828 09/26/2023 23:596200BBenzeneµg/L 18.0 232 09/26/2023 23:596200BEthylbenzeneµg/L 17.0 940 09/26/2023 23:596200BNaphthaleneµg/L 47.0 1700 09/26/2023 23:596200BTolueneµg/L 22.0 258 09/26/2023 23:596200B1,2,4-Trimethylbenzene µg/L 19.0 59.4 09/26/2023 23:596200B1,3,5-Trimethylbenzene µg/L 18.0 516 09/26/2023 23:596200Bo-Xylene µg/L 21.0 867 09/26/2023 23:596200Bm,p-Xylene µg/L 42.0 1380 09/26/2023 23:596200BXylene (Total)µg/L 21.0 V 95895MW-3 29.4 09/26/2023 18:386200BBenzeneµg/L 0.180 10.4 09/26/2023 18:386200Bn-Butylbenzene µg/L 0.180 5.27 09/26/2023 18:386200Bsec-Butyl benzene µg/L 0.200 1.24 09/26/2023 18:386200BEthylbenzeneµg/L 0.170 5.54 09/26/2023 18:386200BIsopropylbenzeneµg/L 0.180 4.14 09/26/2023 18:386200B4-Isopropyl toluene µg/L 0.089 6.80 09/26/2023 18:386200BNaphthaleneµg/L 0.470 4.26 09/26/2023 18:386200Bn-Propylbenzene µg/L 0.190 3.07 09/26/2023 18:386200BTolueneµg/L 0.220 1.18 09/26/2023 18:386200B1,2,4-Trimethylbenzene µg/L 0.190 1.65 09/26/2023 18:386200B1,3,5-Trimethylbenzene µg/L 0.180 3.49 09/26/2023 18:386200Bo-Xylene µg/L 0.210 5.87 09/26/2023 18:386200Bm,p-Xylene µg/L 0.420 9.36 09/26/2023 18:386200BXylene (Total)µg/L 0.210 V 95896MW-6 8790 09/27/2023 00:236200BBenzeneµg/L 18.0 J34.9 09/27/2023 00:236200Bn-Butylbenzene µg/L 18.0 J24.6 09/27/2023 00:236200Bsec-Butyl benzene µg/L 20.0 2640 09/27/2023 00:236200BEthylbenzeneµg/L 17.0 99.8 09/27/2023 00:236200BIsopropylbenzeneµg/L 18.0 730 09/27/2023 00:236200BNaphthaleneµg/L 47.0 315 09/27/2023 00:236200Bn-Propylbenzene µg/L 19.0 64.5 09/27/2023 00:236200BStyreneµg/L 22.0 28100 09/27/2023 22:346200BTolueneµg/L 220 2560 09/27/2023 00:236200B1,2,4-Trimethylbenzene µg/L 19.0 687 09/27/2023 00:236200B1,3,5-Trimethylbenzene µg/L 18.0 Page 4 of 49 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-264-0030 Report Limit Project:Fast Track #145 V 95896MW-6 4030 09/27/2023 00:236200Bo-Xylene µg/L 21.0 10300 09/27/2023 00:236200Bm,p-Xylene µg/L 42.0 14300 09/27/2023 00:236200BXylene (Total)µg/L 21.0 V 95897MW-14 133 09/27/2023 19:416200BBenzeneµg/L 1.80 2.79 09/26/2023 19:026200Bn-Butylbenzene µg/L 0.180 0.575 09/26/2023 19:026200BDi-Isopropyl Ether (DIPE)µg/L 0.500 32.7 09/26/2023 19:026200BEthylbenzeneµg/L 0.170 2.07 09/26/2023 19:026200BIsopropylbenzeneµg/L 0.180 J0.466 09/26/2023 19:026200B4-Isopropyl toluene µg/L 0.089 3.94 09/26/2023 19:026200Bn-Propylbenzene µg/L 0.190 193 09/27/2023 19:416200BTolueneµg/L 2.20 55.7 09/26/2023 19:026200B1,2,4-Trimethylbenzene µg/L 0.190 23.1 09/26/2023 19:026200B1,3,5-Trimethylbenzene µg/L 0.180 74.5 09/26/2023 19:026200Bo-Xylene µg/L 0.210 160 09/26/2023 19:026200Bm,p-Xylene µg/L 0.420 235 09/26/2023 19:026200BXylene (Total)µg/L 0.210 V 95898MW-17 J44809/27/2023 00:486200BAcetoneµg/L 180 137 09/27/2023 00:486200BEthylbenzeneµg/L 17.0 J22.1 09/27/2023 00:486200BIsopropylbenzeneµg/L 18.0 902 09/27/2023 00:486200BNaphthaleneµg/L 47.0 88.3 09/27/2023 00:486200Bn-Propylbenzene µg/L 19.0 107 09/27/2023 00:486200BTolueneµg/L 22.0 1140 09/27/2023 00:486200B1,2,4-Trimethylbenzene µg/L 19.0 255 09/27/2023 00:486200B1,3,5-Trimethylbenzene µg/L 18.0 560 09/27/2023 00:486200Bo-Xylene µg/L 21.0 797 09/27/2023 00:486200Bm,p-Xylene µg/L 42.0 1360 09/27/2023 00:486200BXylene (Total)µg/L 21.0 Page 5 of 49   Client: Geological Resources, Inc. CASE NARRATIVE Project: Fast Track #145 Lab Report Number: 23-264-0030 Date: 9/29/2023 Volatile Organic Compounds - GC/MS Method 6200B Analyte: 1,2,3-Trichlorobenzene QC Batch No: V38416/V38414 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: 1,2,3-Trichlorobenzene QC Batch No: V38456/V38414 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: 1,2,4-Trichlorobenzene QC Batch No: V38416/V38414 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: 1,2,4-Trichlorobenzene QC Batch No: V38456/V38414 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: 2,2-Dichloropropane QC Batch No: V38416/V38414 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Carbon Tetrachloride QC Batch No: V38416/V38414 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Carbon Tetrachloride QC Batch No: V38456/V38414 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Page 6 of 49   Analyte: Chloromethane QC Batch No: V38416/V38414 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Chloromethane QC Batch No: V38456/V38414 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Dichlorodifluoromethane QC Batch No: V38416/V38414 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Dichlorodifluoromethane QC Batch No: V38456/V38414 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Hexachlorobutadiene QC Batch No: V38416/V38414 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Hexachlorobutadiene QC Batch No: V38456/V38414 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Vinyl chloride QC Batch No: V38416/V38414 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Page 7 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-1 95894 Matrix: 9/21/2023 9:23 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <180 µg/L 180 1000Acetone 100 09/26/23 23:59 V38416ENM 828 µg/L 18.0 50.0Benzene 100 09/26/23 23:59 V38416ENM <21.0 µg/L 21.0 50.0Bromobenzene 100 09/26/23 23:59 V38416ENM <42.0 µg/L 42.0 100Bromochloromethane 100 09/26/23 23:59 V38416ENM <16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/26/23 23:59 V38416ENM <150 µg/L 150 500Bromoform 100 09/26/23 23:59 V38416ENM <28.0 µg/L 28.0 100Bromomethane 100 09/26/23 23:59 V38416ENM <18.0 µg/L 18.0 50.0n-Butylbenzene 100 09/26/23 23:59 V38416ENM <20.0 µg/L 20.0 50.0sec-Butyl benzene 100 09/26/23 23:59 V38416ENM <92.0 µg/L 92.0 200tert-Butyl benzene 100 09/26/23 23:59 V38416ENM <18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/26/23 23:59 V38416ENM <19.0 µg/L 19.0 50.0Chlorobenzene 100 09/26/23 23:59 V38416ENM <19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/26/23 23:59 V38416ENM <43.0 µg/L 43.0 100Chloroethane 100 09/26/23 23:59 V38416ENM <22.0 µg/L 22.0 50.0Chloroform 100 09/26/23 23:59 V38416ENM <22.0 M µg/L 22.0 50.0Chloromethane 100 09/26/23 23:59 V38416ENM <20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/26/23 23:59 V38416ENM <20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/26/23 23:59 V38416ENM <50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/26/23 23:59 V38416ENM <110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/26/23 23:59 V38416ENM <20.0 µg/L 20.0 50.01,2-Dibromoethane 100 09/26/23 23:59 V38416ENM <23.0 µg/L 23.0 50.0Dibromomethane 100 09/26/23 23:59 V38416ENM <22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/26/23 23:59 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 8 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-1 95894 Matrix: 9/21/2023 9:23 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/26/23 23:59 V38416ENM <21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/26/23 23:59 V38416ENM <120 M µg/L 120 500Dichlorodifluoromethane 100 09/26/23 23:59 V38416ENM <24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/26/23 23:59 V38416ENM <15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/26/23 23:59 V38416ENM <15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/26/23 23:59 V38416ENM <20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/26/23 23:59 V38416ENM <18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/26/23 23:59 V38416ENM <19.0 µg/L 19.0 50.01,2-Dichloropropane 100 09/26/23 23:59 V38416ENM <13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/26/23 23:59 V38416ENM <21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/26/23 23:59 V38416ENM <20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/26/23 23:59 V38416ENM <21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/26/23 23:59 V38416ENM <15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/26/23 23:59 V38416ENM <4200 µg/L 4200 20000Ethanol 100 09/26/23 23:59 V38416ENM 232 µg/L 17.0 50.0Ethylbenzene 100 09/26/23 23:59 V38416ENM <35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/26/23 23:59 V38416ENM <38.0 µg/L 38.0 1002-Hexanone 100 09/26/23 23:59 V38416ENM <18.0 µg/L 18.0 50.0Isopropylbenzene 100 09/26/23 23:59 V38416ENM <8.90 µg/L 8.90 50.04-Isopropyl toluene 100 09/26/23 23:59 V38416ENM <71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/26/23 23:59 V38416ENM <14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 09/26/23 23:59 V38416ENM <7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/26/23 23:59 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 9 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-1 95894 Matrix: 9/21/2023 9:23 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <33.0 µg/L 33.0 200Methylene Chloride 100 09/26/23 23:59 V38416ENM 940 µg/L 47.0 100Naphthalene 100 09/26/23 23:59 V38416ENM <19.0 µg/L 19.0 50.0n-Propylbenzene 100 09/26/23 23:59 V38416ENM <22.0 µg/L 22.0 50.0Styrene 100 09/26/23 23:59 V38416ENM <16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/26/23 23:59 V38416ENM <16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/26/23 23:59 V38416ENM <22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/26/23 23:59 V38416ENM 1700 µg/L 22.0 50.0Toluene 100 09/26/23 23:59 V38416ENM <38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/26/23 23:59 V38416ENM <31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/26/23 23:59 V38416ENM <16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/26/23 23:59 V38416ENM <9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/26/23 23:59 V38416ENM <18.0 µg/L 18.0 50.0Trichloroethene 100 09/26/23 23:59 V38416ENM <18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/26/23 23:59 V38416ENM <27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/26/23 23:59 V38416ENM 258 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/26/23 23:59 V38416ENM 59.4 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/26/23 23:59 V38416ENM <100 µg/L 100 500Vinyl Acetate 100 09/26/23 23:59 V38416ENM <17.0 M µg/L 17.0 50.0Vinyl Chloride 100 09/26/23 23:59 V38416ENM 516 µg/L 21.0 50.0o-Xylene 100 09/26/23 23:59 V38416ENM 867 µg/L 42.0 100m,p-Xylene 100 09/26/23 23:59 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 10 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-1 95894 Matrix: 9/21/2023 9:23 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 1380 µg/L 21.0 50.0Xylene (Total)100 09/26/23 23:59 V38416 Surrogate: 4-Bromofluorobenzene 93.6 Limits: 70-130%09/26/23 23:59100 ENM V38416 Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/26/23 23:59100 ENM V38416 Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%09/26/23 23:59100 ENM V38416 Surrogate: Toluene-d8 97.8 Limits: 70-130%09/26/23 23:59100 ENM V38416 Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 11 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-3 95895 Matrix: 9/21/2023 9:32 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <1.80 µg/L 1.80 10.0Acetone 1 09/26/23 18:38 V38416ENM 29.4 µg/L 0.180 0.500Benzene 1 09/26/23 18:38 V38416ENM <0.210 µg/L 0.210 0.500Bromobenzene 1 09/26/23 18:38 V38416ENM <0.420 µg/L 0.420 1.00Bromochloromethane 1 09/26/23 18:38 V38416ENM <0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/26/23 18:38 V38416ENM <1.50 µg/L 1.50 5.00Bromoform 1 09/26/23 18:38 V38416ENM <0.280 µg/L 0.280 1.00Bromomethane 1 09/26/23 18:38 V38416ENM 10.4 µg/L 0.180 0.500n-Butylbenzene 1 09/26/23 18:38 V38416ENM 5.27 µg/L 0.200 0.500sec-Butyl benzene 1 09/26/23 18:38 V38416ENM <0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/26/23 18:38 V38416ENM <0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/26/23 18:38 V38416ENM <0.190 µg/L 0.190 0.500Chlorobenzene 1 09/26/23 18:38 V38416ENM <0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/26/23 18:38 V38416ENM <0.430 µg/L 0.430 1.00Chloroethane 1 09/26/23 18:38 V38416ENM <0.220 µg/L 0.220 0.500Chloroform 1 09/26/23 18:38 V38416ENM <0.220 µg/L 0.220 0.500Chloromethane 1 09/26/23 18:38 V38416ENM <0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/26/23 18:38 V38416ENM <0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/26/23 18:38 V38416ENM <0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/26/23 18:38 V38416ENM <1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/26/23 18:38 V38416ENM <0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/26/23 18:38 V38416ENM <0.230 µg/L 0.230 0.500Dibromomethane 1 09/26/23 18:38 V38416ENM <0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/26/23 18:38 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 12 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-3 95895 Matrix: 9/21/2023 9:32 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/26/23 18:38 V38416ENM <0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/26/23 18:38 V38416ENM <1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/26/23 18:38 V38416ENM <0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/26/23 18:38 V38416ENM <0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/26/23 18:38 V38416ENM <0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/26/23 18:38 V38416ENM <0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/26/23 18:38 V38416ENM <0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/26/23 18:38 V38416ENM <0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/26/23 18:38 V38416ENM <0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/26/23 18:38 V38416ENM <0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/26/23 18:38 V38416ENM <0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/26/23 18:38 V38416ENM <0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/26/23 18:38 V38416ENM <0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/26/23 18:38 V38416ENM <42.0 µg/L 42.0 200Ethanol 1 09/26/23 18:38 V38416ENM 1.24 µg/L 0.170 0.500Ethylbenzene 1 09/26/23 18:38 V38416ENM <0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/26/23 18:38 V38416ENM <0.380 µg/L 0.380 1.002-Hexanone 1 09/26/23 18:38 V38416ENM 5.54 µg/L 0.180 0.500Isopropylbenzene 1 09/26/23 18:38 V38416ENM 4.14 µg/L 0.089 0.5004-Isopropyl toluene 1 09/26/23 18:38 V38416ENM <0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/26/23 18:38 V38416ENM <0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/26/23 18:38 V38416ENM <0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/26/23 18:38 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 13 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-3 95895 Matrix: 9/21/2023 9:32 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <0.330 µg/L 0.330 2.00Methylene Chloride 1 09/26/23 18:38 V38416ENM 6.80 µg/L 0.470 1.00Naphthalene 1 09/26/23 18:38 V38416ENM 4.26 µg/L 0.190 0.500n-Propylbenzene 1 09/26/23 18:38 V38416ENM <0.220 µg/L 0.220 0.500Styrene 1 09/26/23 18:38 V38416ENM <0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/26/23 18:38 V38416ENM <0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/26/23 18:38 V38416ENM <0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/26/23 18:38 V38416ENM 3.07 µg/L 0.220 0.500Toluene 1 09/26/23 18:38 V38416ENM <0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/26/23 18:38 V38416ENM <0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/26/23 18:38 V38416ENM <0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/26/23 18:38 V38416ENM <0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/26/23 18:38 V38416ENM <0.180 µg/L 0.180 0.500Trichloroethene 1 09/26/23 18:38 V38416ENM <0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/26/23 18:38 V38416ENM <0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/26/23 18:38 V38416ENM 1.18 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/26/23 18:38 V38416ENM 1.65 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/26/23 18:38 V38416ENM <1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/26/23 18:38 V38416ENM <0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/26/23 18:38 V38416ENM 3.49 µg/L 0.210 0.500o-Xylene 1 09/26/23 18:38 V38416ENM 5.87 µg/L 0.420 1.00m,p-Xylene 1 09/26/23 18:38 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 14 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-3 95895 Matrix: 9/21/2023 9:32 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 9.36 µg/L 0.210 0.500Xylene (Total)1 09/26/23 18:38 V38416 Surrogate: 4-Bromofluorobenzene 93.4 Limits: 70-130%09/26/23 18:381 ENM V38416 Surrogate: Dibromofluoromethane 104 Limits: 70-130%09/26/23 18:381 ENM V38416 Surrogate: 1,2-Dichloroethane - d4 112 Limits: 70-130%09/26/23 18:381 ENM V38416 Surrogate: Toluene-d8 96.2 Limits: 70-130%09/26/23 18:381 ENM V38416 Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 15 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-6 95896 Matrix: 9/21/2023 9:44 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 V38455 09/27/23 09:00 <180 µg/L 180 1000Acetone 100 09/27/23 00:23 V38416ENM 8790 µg/L 18.0 50.0Benzene 100 09/27/23 00:23 V38416ENM <21.0 µg/L 21.0 50.0Bromobenzene 100 09/27/23 00:23 V38416ENM <42.0 µg/L 42.0 100Bromochloromethane 100 09/27/23 00:23 V38416ENM <16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/27/23 00:23 V38416ENM <150 µg/L 150 500Bromoform 100 09/27/23 00:23 V38416ENM <28.0 µg/L 28.0 100Bromomethane 100 09/27/23 00:23 V38416ENM 34.9 J µg/L 18.0 50.0n-Butylbenzene 100 09/27/23 00:23 V38416ENM 24.6 J µg/L 20.0 50.0sec-Butyl benzene 100 09/27/23 00:23 V38416ENM <92.0 µg/L 92.0 200tert-Butyl benzene 100 09/27/23 00:23 V38416ENM <18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/27/23 00:23 V38416ENM <19.0 µg/L 19.0 50.0Chlorobenzene 100 09/27/23 00:23 V38416ENM <19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/27/23 00:23 V38416ENM <43.0 µg/L 43.0 100Chloroethane 100 09/27/23 00:23 V38416ENM <22.0 µg/L 22.0 50.0Chloroform 100 09/27/23 00:23 V38416ENM <22.0 M µg/L 22.0 50.0Chloromethane 100 09/27/23 00:23 V38416ENM <20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/27/23 00:23 V38416ENM <20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/27/23 00:23 V38416ENM <50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/27/23 00:23 V38416ENM <110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/27/23 00:23 V38416ENM <20.0 µg/L 20.0 50.01,2-Dibromoethane 100 09/27/23 00:23 V38416ENM <23.0 µg/L 23.0 50.0Dibromomethane 100 09/27/23 00:23 V38416ENM <22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/27/23 00:23 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 16 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-6 95896 Matrix: 9/21/2023 9:44 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 V38455 09/27/23 09:00 <19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/27/23 00:23 V38416ENM <21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/27/23 00:23 V38416ENM <120 M µg/L 120 500Dichlorodifluoromethane 100 09/27/23 00:23 V38416ENM <24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/27/23 00:23 V38416ENM <15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/27/23 00:23 V38416ENM <15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/27/23 00:23 V38416ENM <20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/27/23 00:23 V38416ENM <18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/27/23 00:23 V38416ENM <19.0 µg/L 19.0 50.01,2-Dichloropropane 100 09/27/23 00:23 V38416ENM <13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/27/23 00:23 V38416ENM <21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/27/23 00:23 V38416ENM <20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/27/23 00:23 V38416ENM <21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/27/23 00:23 V38416ENM <15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/27/23 00:23 V38416ENM <4200 µg/L 4200 20000Ethanol 100 09/27/23 00:23 V38416ENM 2640 µg/L 17.0 50.0Ethylbenzene 100 09/27/23 00:23 V38416ENM <35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/27/23 00:23 V38416ENM <38.0 µg/L 38.0 1002-Hexanone 100 09/27/23 00:23 V38416ENM 99.8 µg/L 18.0 50.0Isopropylbenzene 100 09/27/23 00:23 V38416ENM <8.90 µg/L 8.90 50.04-Isopropyl toluene 100 09/27/23 00:23 V38416ENM <71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/27/23 00:23 V38416ENM <14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 09/27/23 00:23 V38416ENM <7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/27/23 00:23 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 17 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-6 95896 Matrix: 9/21/2023 9:44 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 V38455 09/27/23 09:00 <33.0 µg/L 33.0 200Methylene Chloride 100 09/27/23 00:23 V38416ENM 730 µg/L 47.0 100Naphthalene 100 09/27/23 00:23 V38416ENM 315 µg/L 19.0 50.0n-Propylbenzene 100 09/27/23 00:23 V38416ENM 64.5 µg/L 22.0 50.0Styrene 100 09/27/23 00:23 V38416ENM <16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/27/23 00:23 V38416ENM <16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/27/23 00:23 V38416ENM <22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/27/23 00:23 V38416ENM 28100 µg/L 220 500Toluene 1000 09/27/23 22:34 V38456MSA <38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/27/23 00:23 V38416ENM <31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/27/23 00:23 V38416ENM <16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/27/23 00:23 V38416ENM <9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/27/23 00:23 V38416ENM <18.0 µg/L 18.0 50.0Trichloroethene 100 09/27/23 00:23 V38416ENM <18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/27/23 00:23 V38416ENM <27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/27/23 00:23 V38416ENM 2560 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/27/23 00:23 V38416ENM 687 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/27/23 00:23 V38416ENM <100 µg/L 100 500Vinyl Acetate 100 09/27/23 00:23 V38416ENM <17.0 M µg/L 17.0 50.0Vinyl Chloride 100 09/27/23 00:23 V38416ENM 4030 µg/L 21.0 50.0o-Xylene 100 09/27/23 00:23 V38416ENM 10300 µg/L 42.0 100m,p-Xylene 100 09/27/23 00:23 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 18 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-6 95896 Matrix: 9/21/2023 9:44 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 V38455 09/27/23 09:00 14300 µg/L 21.0 50.0Xylene (Total)100 09/27/23 00:23 V38416 Surrogate: 4-Bromofluorobenzene 90.6 Limits: 70-130%09/27/23 00:23100 ENM V38416 Surrogate: Dibromofluoromethane 99.4 Limits: 70-130%09/27/23 00:23100 ENM V38416 Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%09/27/23 00:23100 ENM V38416 Surrogate: Toluene-d8 98.4 Limits: 70-130%09/27/23 00:23100 ENM V38416 Surrogate: 4-Bromofluorobenzene 91.2 Limits: 70-130%09/27/23 22:341000 MSA V38456 Surrogate: Dibromofluoromethane 99.4 Limits: 70-130%09/27/23 22:341000 MSA V38456 Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%09/27/23 22:341000 MSA V38456 Surrogate: Toluene-d8 96.8 Limits: 70-130%09/27/23 22:341000 MSA V38456 Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 19 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-14 95897 Matrix: 9/21/2023 9:00 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 V38455 09/27/23 09:00 <1.80 µg/L 1.80 10.0Acetone 1 09/26/23 19:02 V38416ENM 133 µg/L 1.80 5.00Benzene 10 09/27/23 19:41 V38456MSA <0.210 µg/L 0.210 0.500Bromobenzene 1 09/26/23 19:02 V38416ENM <0.420 µg/L 0.420 1.00Bromochloromethane 1 09/26/23 19:02 V38416ENM <0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/26/23 19:02 V38416ENM <1.50 µg/L 1.50 5.00Bromoform 1 09/26/23 19:02 V38416ENM <0.280 µg/L 0.280 1.00Bromomethane 1 09/26/23 19:02 V38416ENM 2.79 µg/L 0.180 0.500n-Butylbenzene 1 09/26/23 19:02 V38416ENM <0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/26/23 19:02 V38416ENM <0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/26/23 19:02 V38416ENM <0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/26/23 19:02 V38416ENM <0.190 µg/L 0.190 0.500Chlorobenzene 1 09/26/23 19:02 V38416ENM <0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/26/23 19:02 V38416ENM <0.430 µg/L 0.430 1.00Chloroethane 1 09/26/23 19:02 V38416ENM <0.220 µg/L 0.220 0.500Chloroform 1 09/26/23 19:02 V38416ENM <0.220 M µg/L 0.220 0.500Chloromethane 1 09/26/23 19:02 V38416ENM <0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/26/23 19:02 V38416ENM <0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/26/23 19:02 V38416ENM 0.575 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/26/23 19:02 V38416ENM <1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/26/23 19:02 V38416ENM <0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/26/23 19:02 V38416ENM <0.230 µg/L 0.230 0.500Dibromomethane 1 09/26/23 19:02 V38416ENM <0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/26/23 19:02 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 20 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-14 95897 Matrix: 9/21/2023 9:00 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 V38455 09/27/23 09:00 <0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/26/23 19:02 V38416ENM <0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/26/23 19:02 V38416ENM <1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/26/23 19:02 V38416ENM <0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/26/23 19:02 V38416ENM <0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/26/23 19:02 V38416ENM <0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/26/23 19:02 V38416ENM <0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/26/23 19:02 V38416ENM <0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/26/23 19:02 V38416ENM <0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/26/23 19:02 V38416ENM <0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/26/23 19:02 V38416ENM <0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/26/23 19:02 V38416ENM <0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/26/23 19:02 V38416ENM <0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/26/23 19:02 V38416ENM <0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/26/23 19:02 V38416ENM <42.0 µg/L 42.0 200Ethanol 1 09/26/23 19:02 V38416ENM 32.7 µg/L 0.170 0.500Ethylbenzene 1 09/26/23 19:02 V38416ENM <0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/26/23 19:02 V38416ENM <0.380 µg/L 0.380 1.002-Hexanone 1 09/26/23 19:02 V38416ENM 2.07 µg/L 0.180 0.500Isopropylbenzene 1 09/26/23 19:02 V38416ENM 0.466 J µg/L 0.089 0.5004-Isopropyl toluene 1 09/26/23 19:02 V38416ENM <0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/26/23 19:02 V38416ENM <0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/26/23 19:02 V38416ENM <0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/26/23 19:02 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 21 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-14 95897 Matrix: 9/21/2023 9:00 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 V38455 09/27/23 09:00 <0.330 µg/L 0.330 2.00Methylene Chloride 1 09/26/23 19:02 V38416ENM <0.470 µg/L 0.470 1.00Naphthalene 1 09/26/23 19:02 V38416ENM 3.94 µg/L 0.190 0.500n-Propylbenzene 1 09/26/23 19:02 V38416ENM <0.220 µg/L 0.220 0.500Styrene 1 09/26/23 19:02 V38416ENM <0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/26/23 19:02 V38416ENM <0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/26/23 19:02 V38416ENM <0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/26/23 19:02 V38416ENM 193 µg/L 2.20 5.00Toluene 10 09/27/23 19:41 V38456MSA <0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/26/23 19:02 V38416ENM <0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/26/23 19:02 V38416ENM <0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/26/23 19:02 V38416ENM <0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/26/23 19:02 V38416ENM <0.180 µg/L 0.180 0.500Trichloroethene 1 09/26/23 19:02 V38416ENM <0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/26/23 19:02 V38416ENM <0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/26/23 19:02 V38416ENM 55.7 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/26/23 19:02 V38416ENM 23.1 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/26/23 19:02 V38416ENM <1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/26/23 19:02 V38416ENM <0.170 M µg/L 0.170 0.500Vinyl Chloride 1 09/26/23 19:02 V38416ENM 74.5 µg/L 0.210 0.500o-Xylene 1 09/26/23 19:02 V38416ENM 160 µg/L 0.420 1.00m,p-Xylene 1 09/26/23 19:02 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 22 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-14 95897 Matrix: 9/21/2023 9:00 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 V38455 09/27/23 09:00 235 µg/L 0.210 0.500Xylene (Total)1 09/26/23 19:02 V38416 Surrogate: 4-Bromofluorobenzene 93.2 Limits: 70-130%09/26/23 19:021 ENM V38416 Surrogate: Dibromofluoromethane 99.4 Limits: 70-130%09/26/23 19:021 ENM V38416 Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%09/26/23 19:021 ENM V38416 Surrogate: Toluene-d8 98.0 Limits: 70-130%09/26/23 19:021 ENM V38416 Surrogate: 4-Bromofluorobenzene 90.8 Limits: 70-130%09/27/23 19:4110 MSA V38456 Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/27/23 19:4110 MSA V38456 Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%09/27/23 19:4110 MSA V38456 Surrogate: Toluene-d8 94.8 Limits: 70-130%09/27/23 19:4110 MSA V38456 Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 23 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-17 95898 Matrix: 9/21/2023 9:11 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 448 J µg/L 180 1000Acetone 100 09/27/23 00:48 V38416ENM <18.0 µg/L 18.0 50.0Benzene 100 09/27/23 00:48 V38416ENM <21.0 µg/L 21.0 50.0Bromobenzene 100 09/27/23 00:48 V38416ENM <42.0 µg/L 42.0 100Bromochloromethane 100 09/27/23 00:48 V38416ENM <16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/27/23 00:48 V38416ENM <150 µg/L 150 500Bromoform 100 09/27/23 00:48 V38416ENM <28.0 µg/L 28.0 100Bromomethane 100 09/27/23 00:48 V38416ENM <18.0 µg/L 18.0 50.0n-Butylbenzene 100 09/27/23 00:48 V38416ENM <20.0 µg/L 20.0 50.0sec-Butyl benzene 100 09/27/23 00:48 V38416ENM <92.0 µg/L 92.0 200tert-Butyl benzene 100 09/27/23 00:48 V38416ENM <18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/27/23 00:48 V38416ENM <19.0 µg/L 19.0 50.0Chlorobenzene 100 09/27/23 00:48 V38416ENM <19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/27/23 00:48 V38416ENM <43.0 µg/L 43.0 100Chloroethane 100 09/27/23 00:48 V38416ENM <22.0 µg/L 22.0 50.0Chloroform 100 09/27/23 00:48 V38416ENM <22.0 M µg/L 22.0 50.0Chloromethane 100 09/27/23 00:48 V38416ENM <20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/27/23 00:48 V38416ENM <20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/27/23 00:48 V38416ENM <50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/27/23 00:48 V38416ENM <110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/27/23 00:48 V38416ENM <20.0 µg/L 20.0 50.01,2-Dibromoethane 100 09/27/23 00:48 V38416ENM <23.0 µg/L 23.0 50.0Dibromomethane 100 09/27/23 00:48 V38416ENM <22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/27/23 00:48 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 24 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-17 95898 Matrix: 9/21/2023 9:11 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/27/23 00:48 V38416ENM <21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/27/23 00:48 V38416ENM <120 M µg/L 120 500Dichlorodifluoromethane 100 09/27/23 00:48 V38416ENM <24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/27/23 00:48 V38416ENM <15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/27/23 00:48 V38416ENM <15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/27/23 00:48 V38416ENM <20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/27/23 00:48 V38416ENM <18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/27/23 00:48 V38416ENM <19.0 µg/L 19.0 50.01,2-Dichloropropane 100 09/27/23 00:48 V38416ENM <13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/27/23 00:48 V38416ENM <21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/27/23 00:48 V38416ENM <20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/27/23 00:48 V38416ENM <21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/27/23 00:48 V38416ENM <15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/27/23 00:48 V38416ENM <4200 µg/L 4200 20000Ethanol 100 09/27/23 00:48 V38416ENM 137 µg/L 17.0 50.0Ethylbenzene 100 09/27/23 00:48 V38416ENM <35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/27/23 00:48 V38416ENM <38.0 µg/L 38.0 1002-Hexanone 100 09/27/23 00:48 V38416ENM 22.1 J µg/L 18.0 50.0Isopropylbenzene 100 09/27/23 00:48 V38416ENM <8.90 µg/L 8.90 50.04-Isopropyl toluene 100 09/27/23 00:48 V38416ENM <71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/27/23 00:48 V38416ENM <14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 09/27/23 00:48 V38416ENM <7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/27/23 00:48 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 25 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-17 95898 Matrix: 9/21/2023 9:11 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <33.0 µg/L 33.0 200Methylene Chloride 100 09/27/23 00:48 V38416ENM 902 µg/L 47.0 100Naphthalene 100 09/27/23 00:48 V38416ENM 88.3 µg/L 19.0 50.0n-Propylbenzene 100 09/27/23 00:48 V38416ENM <22.0 µg/L 22.0 50.0Styrene 100 09/27/23 00:48 V38416ENM <16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/27/23 00:48 V38416ENM <16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/27/23 00:48 V38416ENM <22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/27/23 00:48 V38416ENM 107 µg/L 22.0 50.0Toluene 100 09/27/23 00:48 V38416ENM <38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/27/23 00:48 V38416ENM <31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/27/23 00:48 V38416ENM <16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/27/23 00:48 V38416ENM <9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/27/23 00:48 V38416ENM <18.0 µg/L 18.0 50.0Trichloroethene 100 09/27/23 00:48 V38416ENM <18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/27/23 00:48 V38416ENM <27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/27/23 00:48 V38416ENM 1140 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/27/23 00:48 V38416ENM 255 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/27/23 00:48 V38416ENM <100 µg/L 100 500Vinyl Acetate 100 09/27/23 00:48 V38416ENM <17.0 M µg/L 17.0 50.0Vinyl Chloride 100 09/27/23 00:48 V38416ENM 560 µg/L 21.0 50.0o-Xylene 100 09/27/23 00:48 V38416ENM 797 µg/L 42.0 100m,p-Xylene 100 09/27/23 00:48 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 26 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:MW-17 95898 Matrix: 9/21/2023 9:11 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 1360 µg/L 21.0 50.0Xylene (Total)100 09/27/23 00:48 V38416 Surrogate: 4-Bromofluorobenzene 93.4 Limits: 70-130%09/27/23 00:48100 ENM V38416 Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/27/23 00:48100 ENM V38416 Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%09/27/23 00:48100 ENM V38416 Surrogate: Toluene-d8 98.2 Limits: 70-130%09/27/23 00:48100 ENM V38416 Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 27 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:TB 95899 Matrix: 9/21/2023 8:00 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <1.80 µg/L 1.80 10.0Acetone 1 09/26/23 17:24 V38416ENM <0.180 µg/L 0.180 0.500Benzene 1 09/26/23 17:24 V38416ENM <0.210 µg/L 0.210 0.500Bromobenzene 1 09/26/23 17:24 V38416ENM <0.420 µg/L 0.420 1.00Bromochloromethane 1 09/26/23 17:24 V38416ENM <0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/26/23 17:24 V38416ENM <1.50 µg/L 1.50 5.00Bromoform 1 09/26/23 17:24 V38416ENM <0.280 µg/L 0.280 1.00Bromomethane 1 09/26/23 17:24 V38416ENM <0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/26/23 17:24 V38416ENM <0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/26/23 17:24 V38416ENM <0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/26/23 17:24 V38416ENM <0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/26/23 17:24 V38416ENM <0.190 µg/L 0.190 0.500Chlorobenzene 1 09/26/23 17:24 V38416ENM <0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/26/23 17:24 V38416ENM <0.430 µg/L 0.430 1.00Chloroethane 1 09/26/23 17:24 V38416ENM <0.220 µg/L 0.220 0.500Chloroform 1 09/26/23 17:24 V38416ENM <0.220 M µg/L 0.220 0.500Chloromethane 1 09/26/23 17:24 V38416ENM <0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/26/23 17:24 V38416ENM <0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/26/23 17:24 V38416ENM <0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/26/23 17:24 V38416ENM <1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/26/23 17:24 V38416ENM <0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/26/23 17:24 V38416ENM <0.230 µg/L 0.230 0.500Dibromomethane 1 09/26/23 17:24 V38416ENM <0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/26/23 17:24 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 28 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:TB 95899 Matrix: 9/21/2023 8:00 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/26/23 17:24 V38416ENM <0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/26/23 17:24 V38416ENM <1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/26/23 17:24 V38416ENM <0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/26/23 17:24 V38416ENM <0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/26/23 17:24 V38416ENM <0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/26/23 17:24 V38416ENM <0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/26/23 17:24 V38416ENM <0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/26/23 17:24 V38416ENM <0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/26/23 17:24 V38416ENM <0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/26/23 17:24 V38416ENM <0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/26/23 17:24 V38416ENM <0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/26/23 17:24 V38416ENM <0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/26/23 17:24 V38416ENM <0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/26/23 17:24 V38416ENM <42.0 µg/L 42.0 200Ethanol 1 09/26/23 17:24 V38416ENM <0.170 µg/L 0.170 0.500Ethylbenzene 1 09/26/23 17:24 V38416ENM <0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/26/23 17:24 V38416ENM <0.380 µg/L 0.380 1.002-Hexanone 1 09/26/23 17:24 V38416ENM <0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/26/23 17:24 V38416ENM <0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/26/23 17:24 V38416ENM <0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/26/23 17:24 V38416ENM <0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/26/23 17:24 V38416ENM <0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/26/23 17:24 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 29 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:TB 95899 Matrix: 9/21/2023 8:00 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <0.330 µg/L 0.330 2.00Methylene Chloride 1 09/26/23 17:24 V38416ENM <0.470 µg/L 0.470 1.00Naphthalene 1 09/26/23 17:24 V38416ENM <0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/26/23 17:24 V38416ENM <0.220 µg/L 0.220 0.500Styrene 1 09/26/23 17:24 V38416ENM <0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/26/23 17:24 V38416ENM <0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/26/23 17:24 V38416ENM <0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/26/23 17:24 V38416ENM <0.220 µg/L 0.220 0.500Toluene 1 09/26/23 17:24 V38416ENM <0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/26/23 17:24 V38416ENM <0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/26/23 17:24 V38416ENM <0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/26/23 17:24 V38416ENM <0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/26/23 17:24 V38416ENM <0.180 µg/L 0.180 0.500Trichloroethene 1 09/26/23 17:24 V38416ENM <0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/26/23 17:24 V38416ENM <0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/26/23 17:24 V38416ENM <0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/26/23 17:24 V38416ENM <0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/26/23 17:24 V38416ENM <1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/26/23 17:24 V38416ENM <0.170 M µg/L 0.170 0.500Vinyl Chloride 1 09/26/23 17:24 V38416ENM <0.210 µg/L 0.210 0.500o-Xylene 1 09/26/23 17:24 V38416ENM <0.420 µg/L 0.420 1.00m,p-Xylene 1 09/26/23 17:24 V38416ENM Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 30 of 49 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-264-0030 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #5398 Received : 09/21/2023 Fast Track #145 Report Date : 09/29/2023 Sample ID : Lab No : Sampled:TB 95899 Matrix: 9/21/2023 8:00 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V38414 09/26/23 09:00 <0.21 µg/L 0.210 0.500Xylene (Total)1 09/26/23 17:24 V38416 Surrogate: 4-Bromofluorobenzene 91.0 Limits: 70-130%09/26/23 17:241 ENM V38416 Surrogate: Dibromofluoromethane 104 Limits: 70-130%09/26/23 17:241 ENM V38416 Surrogate: 1,2-Dichloroethane - d4 111 Limits: 70-130%09/26/23 17:241 ENM V38416 Surrogate: Toluene-d8 97.8 Limits: 70-130%09/26/23 17:241 ENM V38416 Qualifiers/ Definitions Recovery out of rangeIDilution FactorDF Minimum valueMEstimated valueJ Method Quantitation LimitMQL Page 31 of 49 September 28, 2023 LABORATORY REPORT NUMBER PROJECT ID Primary Data Review By Project Manager, AES 2309N99 Terri W Cole Waypoint Analytical 449 Springbrook Road Charlotte NC 28217 23-264-0030 Chris Pafford Project Manager, Access Analytical Ashley Amick PLEASE NOTE: -Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. -AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 - AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. - Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed Secondary Data Review By ATTENTION DATE CLIENT ANALYTICAL REPORT Page 1 of 9Page 32 of 49 Page 2 of 9Page 33 of 49 28-Sep-23Date:Analytical Environmental Services, Inc Client: Case Narrative23-264-0030 Waypoint Analytical Lab ID: Project: 2309N99 Aromatic Volatiles in Air Analysis by Method EPA-18: Sample 2309N99-001 was extracted and/or analyzed outside the recommended holding time of 72 hours. Sample was received with insufficient holding time remaining to meet holding time requirements. Page 3 of 9Page 34 of 49 Analytical Results for 28-Sep-23Date: Workorder: Client Reference: Qual Date Analyzed /Analyst Reportin gLimit (ug) Concentration Total (ug) (mg/m3) (ppm) Analyte 2309N99 Waypoint Analytical 23-264-0030 Front (ug) Back (ug) Test Method 9/19/2023Lab ID:95900 Tedlar Bag 1Air Vol.(L):Media:Client ID:2309N99-001A Date Sampled: <3.1<10Benzene <10 10 H EPA189/26/2023 BHI<10 <10 <2.3<10Ethylbenzene <10 10 H EPA189/26/2023 BHI<10 <10 <4.6<20m,p-Xylene <20 20 H EPA189/26/2023 BHI<20 <20 <2.3<10o-Xylene <10 10 H EPA189/26/2023 BHI<10 <10 <2.6<10Toluene <10 10 H EPA189/26/2023 BHI<10 <10 <250TPH (Gasoline) <250 250 H SW8015BM9/26/2023 BHI<250 <250 <31<100TRPH (Based on Benzene) <100 100 H EPA189/26/2023 BHI<100 <100 83 Surr:1,4 Difluorobenzene 83 0 H SW8015BM9/26/2023 BHI83.201 Qualifiers: < Less than the indicated Reporting Limit H Holding time for preparation or analysis B Analyte detected in the associated Method Blank (a) Analysis indicates possible breakthrough; back section result is greater than % of the front section result.10 Page 4 of 9Page 35 of 49 Page 5 of 9Page 36 of 49 28-Sep-23Date:Analytical Environmental Services, Inc Client: Dates ReportLab Order: Project Name: Lab Sample ID Client Sample ID Test NameCollection Date Matrix TCLP Date Prep Date Analysis Date 2309N99 23-264-0030 Waypoint Analytical 2309N99-001A 95900 9/19/2023 11:58:00AM Air Aromatic Volatiles in Air 9/22/2023 3:54:00PM 09/26/2023 2309N99-001A 95900 9/19/2023 11:58:00AM Air GASOLINE RANGE ORGANICS 9/22/2023 3:54:00PM 09/26/2023 Page 6 of 9Page 37 of 49 28-Sep-23Date:Analytical Environmental Services, Inc Client: BatchID:Workorder: Project Name ANALYTICAL QC SUMMARY REPORT 23-264-0030 2309N99 Waypoint Analytical 363478 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:363478MBLK09/25/2023Aromatic Volatiles in Air EPA18 Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 09/22/2023 526928MB-363478 12486355 Benzene 10BRL Ethylbenzene 10BRL m,p-Xylene 20BRL o-Xylene 10BRL Toluene 10BRL TRPH (Based on Benzene) 100BRL RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:363478MBLK09/26/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 09/22/2023 526942MB-363478 12487981 TPH (Gasoline)250BRL Surr: 1,4 Difluorobenzene 079.03 100.0 79.0 67.1 119 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:363478LCS09/25/2023Aromatic Volatiles in Air EPA18 Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 09/22/2023 526928LCS-363478 12486358 Benzene 1091.94 100.0 91.9 82.3 119 Ethylbenzene 1095.15 100.0 95.2 83.7 126 m,p-Xylene 20183.8 200.0 91.9 81.3 124 o-Xylene 1087.79 100.0 87.8 78.4 123 Toluene 1091.74 100.0 91.7 82 124 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:363478LCS 09/26/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 09/22/2023 526942LCS-363478-2 12487982 Qualifiers: J Estimated value detected below Reporting Limit BRL Below reporting limit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank E Estimated (value above quantitation range) S Spike Recovery outside limits due to matrix < Less than Result value> Greater than Result value R RPD outside limits due to matrix Rpt Lim Reporting Limit Page 7 of 9Page 38 of 49 28-Sep-23Date:Analytical Environmental Services, Inc Client: BatchID:Workorder: Project Name ANALYTICAL QC SUMMARY REPORT 23-264-0030 2309N99 Waypoint Analytical 363478 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:363478LCS09/26/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 09/22/2023 526942LCS-363478-2 12487982 TPH (Gasoline)2501046 1000 105 75.1 120 Surr: 1,4 Difluorobenzene 088.71 100.0 88.7 67.1 119 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:363478LCSD09/25/2023Aromatic Volatiles in Air EPA18 Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 09/22/2023 526928LCSD-363478 12486360 Benzene 1099.62 15100.0 99.6 82.3 119 91.94 8.02 Ethylbenzene 10103.4 15100.0 103 83.7 126 95.15 8.27 m,p-Xylene 20199.3 15200.0 99.7 81.3 124 183.8 8.10 o-Xylene 1094.89 15100.0 94.9 78.4 123 87.79 7.77 Toluene 1099.44 15100.0 99.4 82 124 91.74 8.06 RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit SampleType:BatchID: Analysis Date: Seq No:TestCode:363478LCSD09/26/20238015M SW8015CM Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 09/22/2023 526942LCSD-363478-2 12487983 TPH (Gasoline)2501094 27.71000 109 75.1 120 1046 4.57 Surr: 1,4 Difluorobenzene 093.31 0100.0 93.3 67.1 119 88.71 0 Qualifiers: J Estimated value detected below Reporting Limit BRL Below reporting limit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank E Estimated (value above quantitation range) S Spike Recovery outside limits due to matrix < Less than Result value> Greater than Result value R RPD outside limits due to matrix Rpt Lim Reporting Limit Page 8 of 9Page 39 of 49 End of Report Page 9 of 9Page 40 of 49 Quality Control Data 23-264-0030Report No: Project Description: Client ID:Geological Resources, Inc. Fast Track #145 QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V38416QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V38414 Associated Lab Samples: 95894, 95895, 95896, 95897, 95898, 95899 LRB-V38414 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 09/26/23 16:5910.01.80<1.80µg/LAcetone 09/26/23 16:590.5000.180<0.180µg/LBenzene 09/26/23 16:590.5000.210<0.210µg/LBromobenzene 09/26/23 16:591.000.420<0.420µg/LBromochloromethane 09/26/23 16:590.5000.160<0.160µg/LBromodichloromethane 09/26/23 16:595.001.50<1.50µg/LBromoform 09/26/23 16:591.000.280<0.280µg/LBromomethane 09/26/23 16:590.5000.180<0.180µg/Ln-Butylbenzene 09/26/23 16:590.5000.200<0.200µg/Lsec-Butyl benzene 09/26/23 16:592.000.920<0.920µg/Ltert-Butyl benzene 09/26/23 16:590.5000.180<0.180µg/LCarbon Tetrachloride 09/26/23 16:590.5000.190<0.190µg/LChlorobenzene 09/26/23 16:590.5000.190<0.190µg/LChlorodibromomethane 09/26/23 16:591.000.430<0.430µg/LChloroethane 09/26/23 16:590.5000.220<0.220µg/LChloroform 09/26/23 16:590.5000.220<0.220µg/LChloromethane 09/26/23 16:590.5000.200<0.200µg/L2-Chlorotoluene 09/26/23 16:590.5000.200<0.200µg/L4-Chlorotoluene 09/26/23 16:590.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE) 09/26/23 16:592.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane 09/26/23 16:590.5000.200<0.200µg/L1,2-Dibromoethane 09/26/23 16:590.5000.230<0.230µg/LDibromomethane 09/26/23 16:590.5000.220<0.220µg/L1,2-Dichlorobenzene 09/26/23 16:590.5000.190<0.190µg/L1,3-Dichlorobenzene 09/26/23 16:590.5000.210<0.210µg/L1,4-Dichlorobenzene 09/26/23 16:595.001.20<1.20µg/LDichlorodifluoromethane 09/26/23 16:590.5000.240<0.240µg/L1,1-Dichloroethane Page 1 of 7Date:09/29/2023 11:18 AM Page 41 of 49 Quality Control Data 23-264-0030Report No: Project Description: Client ID:Geological Resources, Inc. Fast Track #145 QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V38416QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V38414 Associated Lab Samples: 95894, 95895, 95896, 95897, 95898, 95899 LRB-V38414 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 09/26/23 16:590.5000.150<0.150µg/L1,2-Dichloroethane 09/26/23 16:590.5000.150<0.150µg/L1,1-Dichloroethene 09/26/23 16:590.5000.200<0.200µg/Lcis-1,2-Dichloroethene 09/26/23 16:590.5000.180<0.180µg/Ltrans-1,2-Dichloroethene 09/26/23 16:590.5000.190<0.190µg/L1,2-Dichloropropane 09/26/23 16:590.5000.130<0.130µg/L1,3-Dichloropropane 09/26/23 16:592.000.210<0.210µg/L2,2-Dichloropropane 09/26/23 16:590.5000.200<0.200µg/L1,1-Dichloropropene 09/26/23 16:590.5000.210<0.210µg/Lcis-1,3-Dichloropropene 09/26/23 16:590.5000.150<0.150µg/Ltrans-1,3-Dichloropropene 09/26/23 16:5920042.0<42.0µg/LEthanol 09/26/23 16:590.5000.170<0.170µg/LEthylbenzene 09/26/23 16:593.000.350<0.350µg/LHexachlorobutadiene 09/26/23 16:591.000.380<0.380µg/L2-Hexanone 09/26/23 16:590.5000.180<0.180µg/LIsopropylbenzene 09/26/23 16:590.5000.089<0.089µg/L4-Isopropyl toluene 09/26/23 16:595.000.710<0.710µg/LMethyl Ethyl Ketone (MEK) 09/26/23 16:591.000.140<0.140µg/LMethyl tert-butyl ether (MTBE) 09/26/23 16:591.000.078<0.078µg/L4-Methyl-2-Pentanone 09/26/23 16:592.000.330<0.330µg/LMethylene Chloride 09/26/23 16:591.000.470<0.470µg/LNaphthalene 09/26/23 16:590.5000.190<0.190µg/Ln-Propylbenzene 09/26/23 16:590.5000.220<0.220µg/LStyrene 09/26/23 16:590.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane 09/26/23 16:590.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane 09/26/23 16:590.5000.220<0.220µg/LTetrachloroethene 09/26/23 16:590.5000.220<0.220µg/LToluene Page 2 of 7Date:09/29/2023 11:18 AM Page 42 of 49 Quality Control Data 23-264-0030Report No: Project Description: Client ID:Geological Resources, Inc. Fast Track #145 QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V38416QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V38414 Associated Lab Samples: 95894, 95895, 95896, 95897, 95898, 95899 LRB-V38414 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 09/26/23 16:590.5000.380<0.380µg/L1,2,3-Trichlorobenzene 09/26/23 16:590.5000.310<0.310µg/L1,2,4-Trichlorobenzene 09/26/23 16:590.5000.160<0.160µg/L1,1,1-Trichloroethane 09/26/23 16:590.5000.096<0.096µg/L1,1,2-Trichloroethane 09/26/23 16:590.5000.180<0.180µg/LTrichloroethene 09/26/23 16:590.5000.180<0.180µg/LTrichlorofluoromethane 09/26/23 16:590.5000.270<0.270µg/L1,2,3-Trichloropropane 09/26/23 16:590.5000.190<0.190µg/L1,2,4-Trimethylbenzene 09/26/23 16:590.5000.180<0.180µg/L1,3,5-Trimethylbenzene 09/26/23 16:595.001.00<1.00µg/LVinyl Acetate 09/26/23 16:590.5000.170<0.170µg/LVinyl Chloride 09/26/23 16:590.5000.210<0.210µg/Lo-Xylene 09/26/23 16:591.000.420<0.420µg/Lm,p-Xylene 09/26/23 16:594-Bromofluorobenzene (S)92.8 70-130 09/26/23 16:59Dibromofluoromethane (S)100 70-130 09/26/23 16:591,2-Dichloroethane - d4 (S)106 70-130 09/26/23 16:59Toluene-d8 (S)98.4 70-130 LCS-V38414 LCSD-V38414Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 40.0 10011345.140.0µg/LAcetone 40-160 11.9 20.0 18.8 94.096.519.320.0µg/LBenzene 70-130 2.6 20.0 20.1 10199.519.920.0µg/LBromobenzene 70-130 1.0 20.0 21.1 10611422.820.0µg/LBromochloromethane 70-130 7.7 20.0 20.8 10411222.420.0µg/LBromodichloromethane 70-130 7.4 20.0 Page 3 of 7Date:09/29/2023 11:18 AM Page 43 of 49 Quality Control Data 23-264-0030Report No: Project Description: Client ID:Geological Resources, Inc. Fast Track #145 QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V38416QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V38414 LCS-V38414 LCSD-V38414Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 23.5 11812725.320.0µg/LBromoform 70-130 7.3 20.0 18.2 91.099.519.920.0µg/LBromomethane 60-140 8.9 20.0 21.6 10810721.420.0µg/Ln-Butylbenzene 70-130 0.9 20.0 20.5 10310520.920.0µg/Lsec-Butyl benzene 70-130 1.9 20.0 21.5 10811021.920.0µg/Ltert-Butyl benzene 70-130 1.8 20.0 26.6 133*139*27.820.0µg/LCarbon Tetrachloride 70-130 4.4 20.0 21.3 10711222.420.0µg/LChlorobenzene 70-130 5.0 20.0 22.4 11212124.120.0µg/LChlorodibromomethane 70-130 7.3 20.0 13.1 65.565.513.120.0µg/LChloroethane 60-140 0.0 20.0 20.7 10411122.120.0µg/LChloroform 70-130 6.5 20.0 10.7 53.5*58.0*11.620.0µg/LChloromethane 60-140 8.0 20.0 19.9 99.598.519.720.0µg/L2-Chlorotoluene 70-130 1.0 20.0 20.1 10110320.520.0µg/L4-Chlorotoluene 70-130 1.9 20.0 14.7 73.578.515.720.0µg/LDi-Isopropyl Ether (DIPE)70-130 6.5 20.0 24.3 12212024.020.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.2 20.0 19.6 98.010520.920.0µg/L1,2-Dibromoethane 70-130 6.4 20.0 21.0 10511322.520.0µg/LDibromomethane 70-130 6.8 20.0 21.9 11011623.120.0µg/L1,2-Dichlorobenzene 70-130 5.3 20.0 22.2 11111623.120.0µg/L1,3-Dichlorobenzene 70-130 3.9 20.0 21.5 10810921.820.0µg/L1,4-Dichlorobenzene 70-130 1.3 20.0 11.9 59.5*59.0*11.820.0µg/LDichlorodifluoromethane 60-140 0.8 20.0 18.0 90.096.519.320.0µg/L1,1-Dichloroethane 70-130 6.9 20.0 22.0 11011823.520.0µg/L1,2-Dichloroethane 70-130 6.5 20.0 20.4 10210420.720.0µg/L1,1-Dichloroethene 70-130 1.4 20.0 19.5 97.599.519.920.0µg/Lcis-1,2-Dichloroethene 70-130 2.0 20.0 18.4 92.010120.120.0µg/Ltrans-1,2-Dichloroethene 70-130 8.8 20.0 Page 4 of 7* QC Fail Date:09/29/2023 11:18 AM Page 44 of 49 Quality Control Data 23-264-0030Report No: Project Description: Client ID:Geological Resources, Inc. Fast Track #145 QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V38416QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V38414 LCS-V38414 LCSD-V38414Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 15.5 77.584.016.820.0µg/L1,2-Dichloropropane 70-130 8.0 20.0 18.9 94.596.519.320.0µg/L1,3-Dichloropropane 70-130 2.0 20.0 24.3 122135*26.920.0µg/L2,2-Dichloropropane 70-130 10.1 20.0 21.1 10611623.220.0µg/L1,1-Dichloropropene 70-130 9.4 20.0 19.2 96.010120.120.0µg/Lcis-1,3-Dichloropropene 70-130 4.5 20.0 20.6 10311222.420.0µg/Ltrans-1,3-Dichloropropene 70-130 8.3 20.0 316 63.270.4352500µg/LEthanol 60-140 10.7 20.0 19.9 99.510220.420.0µg/LEthylbenzene 70-130 2.4 20.0 27.0 135*132*26.320.0µg/LHexachlorobutadiene 70-130 2.6 20.0 17.0 85.099.519.920.0µg/L2-Hexanone 60-140 15.7 20.0 21.9 11011122.120.0µg/LIsopropylbenzene 70-130 0.9 20.0 22.8 11411723.420.0µg/L4-Isopropyl toluene 70-130 2.5 20.0 16.0 80.085.517.120.0µg/LMethyl Ethyl Ketone (MEK)60-140 6.6 20.0 20.5 10310921.720.0µg/LMethyl tert-butyl ether (MTBE)70-130 5.6 20.0 15.2 76.086.017.220.0µg/L4-Methyl-2-Pentanone 60-140 12.3 20.0 14.9 74.578.515.720.0µg/LMethylene Chloride 70-130 5.2 20.0 22.2 11112625.220.0µg/LNaphthalene 70-130 12.6 20.0 20.0 10010320.520.0µg/Ln-Propylbenzene 70-130 2.4 20.0 21.5 10810921.820.0µg/LStyrene 70-130 1.3 20.0 22.3 11211823.520.0µg/L1,1,1,2-Tetrachloroethane 70-130 5.2 20.0 16.9 84.594.018.820.0µg/L1,1,2,2-Tetrachloroethane 70-130 10.6 20.0 23.2 11612023.920.0µg/LTetrachloroethene 70-130 2.9 20.0 19.4 97.010220.420.0µg/LToluene 70-130 5.0 20.0 27.0 135*158*31.620.0µg/L1,2,3-Trichlorobenzene 70-130 15.6 20.0 26.8 134*142*28.320.0µg/L1,2,4-Trichlorobenzene 70-130 5.4 20.0 24.4 12212525.020.0µg/L1,1,1-Trichloroethane 70-130 2.4 20.0 Page 5 of 7* QC Fail Date:09/29/2023 11:18 AM Page 45 of 49 Quality Control Data 23-264-0030Report No: Project Description: Client ID:Geological Resources, Inc. Fast Track #145 QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V38416QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V38414 LCS-V38414 LCSD-V38414Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 19.2 96.010120.120.0µg/L1,1,2-Trichloroethane 70-130 4.5 20.0 21.9 11011222.320.0µg/LTrichloroethene 70-130 1.8 20.0 24.5 12312424.820.0µg/LTrichlorofluoromethane 60-140 1.2 20.0 18.6 93.099.019.820.0µg/L1,2,3-Trichloropropane 70-130 6.2 20.0 22.2 11111322.520.0µg/L1,2,4-Trimethylbenzene 70-130 1.3 20.0 21.5 10811022.020.0µg/L1,3,5-Trimethylbenzene 70-130 2.2 20.0 22.9 11513226.420.0µg/LVinyl Acetate 60-140 14.1 20.0 11.7 58.5*60.512.120.0µg/LVinyl Chloride 60-140 3.3 20.0 20.7 10410721.420.0µg/Lo-Xylene 70-130 3.3 20.0 44.7 11211445.740.0µg/Lm,p-Xylene 70-130 2.2 20.0 91.891.44-Bromofluorobenzene (S)70-130 103102Dibromofluoromethane (S)70-130 1101101,2-Dichloroethane - d4 (S)70-130 97.697.8Toluene-d8 (S)70-130 Page 6 of 7* QC Fail Date:09/29/2023 11:18 AM Page 46 of 49 Quality Control Data 23-264-0030Report No: Project Description: Client ID:Geological Resources, Inc. Fast Track #145 QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V38456QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V38455 Associated Lab Samples: 95896, 95897 LRB-V38455 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 09/27/23 13:300.5000.180<0.180µg/LBenzene 09/27/23 13:300.5000.220<0.220µg/LToluene 09/27/23 13:304-Bromofluorobenzene (S)91.0 70-130 09/27/23 13:30Dibromofluoromethane (S)101 70-130 09/27/23 13:301,2-Dichloroethane - d4 (S)110 70-130 09/27/23 13:30Toluene-d8 (S)96.8 70-130 LCS-V38455 LCSD-V38455Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 19.3 96.598.019.620.0µg/LBenzene 70-130 1.5 20.0 19.6 98.010220.420.0µg/LToluene 70-130 4.0 20.0 92.892.24-Bromofluorobenzene (S)70-130 97.699.2Dibromofluoromethane (S)70-130 1041091,2-Dichloroethane - d4 (S)70-130 98.898.0Toluene-d8 (S)70-130 Page 7 of 7Date:09/29/2023 11:18 AM Page 47 of 49 Fed Ex UPS US Postal Client Lab Courier Other : Shipment Receipt Form Customer Number: Customer Name: Report Number:23-264-0030 Geological Resources, Inc. 00087 Shipping Method Shipping container/cooler uncompromised? Thermometer ID:IRT-15 3.4C Chain of Custody (COC) present?Yes No Yes No Not Present Yes No Not Present Yes No COC agrees with sample label(s)? Yes No COC properly completed Samples in proper containers? Sample containers intact? Sufficient sample volume for indicated test(s)? All samples received within holding time? Cooler temperature in compliance? Yes No Yes No Yes No Yes No Yes No Yes NoCooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Yes No N/A Yes No N/A Yes No N/ASoil VOA method 5035 – compliance criteria met Water - Sample containers properly preserved Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) High concentration container (48 hr) Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Number of coolers/boxes received Yes No 1 Signature:Caitlyn Cummins Date & Time:09/21/2023 15:01:25 Special precautions or instructions included? Comments: Page 48 of 49 Page 49 of 49 APPENDIX F O&M Field Data Sheets APPENDIX G Overall Remediation Date: 10/19/23 Facility ID #: 0-031674 Claim Number Task Code Task Code Description Cost Claim Amount 3.101 Supervision of Field Work $5,037.50 3.113 Installation of 2-inch Well $13,500.00 3.114 Installation of 4-inch Well $7,980.00 3.118 Temporary Impact Increase $2,015.00 3.397 Temporary Impact Increase $100.00 3.398 Cost for Drill Rig Mobization $350.00 3.500 Driller Per Diem $1,354.00 4.031 Cost for Sampling Wells $1,331.00 4.051 Cost for Sampling Surface Water $50.00 4.090 Cost for Analytical $1,594.00 6.090 Ground Water Monitoring Report $2,250.00 7.040 Cost for SVE System $58,234.75 7.060 Cost for Air Sparge System $58,234.75 7.081 Remediation System Installation Inspection $5,208.00 7.100 Cost for Installation of Remediation System $99,025.00 7.201 Cost for Scheduled Maintenance $3,324.75 7.250 Cost for Remediation Supplies and Equipment $296.77 7.260 Cost for Remediation Operating Expenses (assumed, pending receipt of all power bills)$1,422.08 8.055 Injection Notice of Intent $500.00 12.030 Overnight Lodging $453.00 12.050 Consultant Travel $4,250.00 12.055 Temporary Impact Increase $850.00 4.031 Cost for Sampling Wells $561.00 4.09 Cost for Analytical $849.00 6.09 Ground Water Monitoring Report $1,125.00 7.201 Cost for Scheduled Maintenance $697.50 7.26 Cost for Remediation Operating Expenses (assumed, pending receipt of all power bills)$3,300.00 12.05 Consultant Travel $750.00 12.055 Temporary Impact Increase $150.00 $274,793.10Total Cost Since System Installation APPENDIX G OVERALL REMEDIATION COSTS (TO DATE) FAST TRACK #145 (INCIDENT NO. 40099) 211 $267,360.60 (claim has not been submitted) $7,432.50 Page 1 of 1 APPENDIX H Contaminant Mass Calculations Area ID Well ID Area (ft²) Average Well Depth (ft.) Average Depth to Water (ft.) Water Column Height (ft) Volume (ft³) Volume (L) Effective Porosity Effective Volume (L) MW-1 MW-6 MW-4 MW-8 MW-9 MW-15 3 MW-3 79,994 39 26.36 12.64 1,011,126 28,631,858 5,726,372 Area Date Well Benzene (μg/L) Toluene (μg/L) Ethylbenzene (μg/L) Xylenes (μg/L) MTBE (μg/L) Naphthalene (μg/L) Total (μg/L) DTW (ft.) Average Water Column Height (ft.) Total Average Mass (g)Percent Red. To Date Red. MW-1 13500.00 9640.00 1670.00 6570.00 225.00 409.00 32014.00 27.96 MW-6 504.00 25500.00 3510.00 15260.00 0.00 504.00 45278.00 27.98 Avg.7002.00 17570.00 2590.00 10915.00 112.50 456.50 38646.00 27.97 MW-1 2560.00 6180.00 1790.00 7230.00 0.00 362.00 18122.00 23.86 MW-6 12900.00 43700.00 2910.00 14700.00 0.00 509.00 74719.00 22.46 Avg.7730.00 24940.00 2350.00 10965.00 0.00 435.50 46420.50 23.16 MW-1 104.00 1970.00 1260.00 6030.00 25.50 257.00 9646.50 23.34 MW-6 8110.00 21200.00 1670.00 8560.00 0.00 274.00 39814.00 21.53 Avg.4107.00 11585.00 1465.00 7295.00 12.75 265.50 24730.25 22.44 MW-1 2250 11500 2000 10600 0.00 421 26771.00 25.66 MW-6 11200 44000 3300 17800 0.00 662 38481.00 24.96 Avg.6725.00 27750.00 2650.00 14200.00 0.00 541.50 32626.00 25.31 MW-1 1750 3370 1420 4880 40.10 493 11953.10 26.79 MW-6 9380 33100 2790 14000 0.00 698 29984.00 26.61 Avg.5565.00 18235.00 2105.00 9440.00 20.05 595.50 20968.55 26.70 MW-1 1840 4550 486 3770 0.00 969 10646.00 30.77 MW-6 8850 23100 1940 10900 0.00 588 44790.00 24.28 Avg.5345.00 13825.00 1213.00 7335.00 0.00 778.50 27718.00 27.53 MW-1 828.00 1,700.00 232.00 1,380.00 0.00 940.00 5080.00 32.55 MW-6 8790.00 28100.00 2640.00 14300.00 0.00 730 53830.00 27.11 Avg. 4809.00 14900.00 1436.00 7840.00 0.00 835.00 29,455.00 29.83 Area 1 09/21/23 10.67 49,494.26 12.6% 35.1% 12.53 44.5% 7.7% 17.34 40.2% 70,355.48 11/13/12 - 03/12/13 9.9715.032536,642 06/08/21 11/10/22 13.80 45,569.99 41.6% 2,068,966365,325 10,344,830 0.20 12.53 348,424 9,866,259 126,762.37 -2.3%15.19 78,046.43 -10.9% -24.3%12.98 56,637.0606/12/23 APPENDIX H CONTAMINANT MASS CALCULATIONS FAST TRACK #145 (INCIDENT NO. 40099) 76,258.29 ------ 18.07 -66.2% 25.7% 2 -66.2% Baseline Event 1 27,807 40.5 27.97 1,973,252 02/14/22 07/02/20 Area ID Well ID Area (ft²) Average Well Depth (ft.) Average Depth to Water (ft.) Water Column Height (ft) Volume (ft³) Volume (L) Effective Porosity Effective Volume (L) MW-1 MW-6 MW-4 MW-8 MW-9 MW-15 3 MW-3 79,994 39 26.36 12.64 1,011,126 28,631,858 5,726,372 Area Date Well Benzene (μg/L) Toluene (μg/L) Ethylbenzene (μg/L) Xylenes (μg/L) MTBE (μg/L) Naphthalene (μg/L) Total (μg/L) DTW (ft.) Average Water Column Height (ft.) Total Average Mass (g)Percent Red. To Date Red. 9.9715.032536,642 2,068,966365,325 10,344,830 0.20 12.53 348,424 9,866,259 APPENDIX H CONTAMINANT MASS CALCULATIONS FAST TRACK #145 (INCIDENT NO. 40099) 2 Baseline Event 1 27,807 40.5 27.97 1,973,252 MW-8 9540.00 21300.00 3030.00 14120.00 0.00 336.00 48326.00 28.41 MW-9 1200.00 18.90 13.40 29.16 5.31 39.10 1305.87 1.65 Avg.5370.00 10659.45 1521.70 7074.58 2.66 187.55 49631.87 15.03 MW-8 5650.00 33800.00 3090.00 16300.00 0.00 635.00 59475.00 25.02 MW-9 51.00 1.90 2.30 0.00 0.00 2.50 57.70 1.91 Avg.2850.50 16900.95 1546.15 8150.00 0.00 318.75 29766.35 13.47 MW-8 8620.00 36500.00 3270.00 18100.00 0.00 512.00 67002.00 24.47 MW-9 51.00 1.90 2.30 0.00 0.00 2.50 57.70 1.91 Avg.4335.50 18250.95 1636.15 9050.00 0.00 257.25 33529.85 13.19 MW-4 1940.00 1250.00 2580.00 4460.00 0.00 551.00 10781.00 6.96 MW-8 3840.00 68800.00 14500.00 81200.00 0.00 8460.00 176800.00 27.23 MW-9 0.00 0.00 0.00 0.00 0.00 0.74 0.74 1.54 MW-15 10.30 0.56 1.30 1.50 1.50 0.90 16.06 2.35 Avg.1447.58 17512.64 4270.33 21415.38 0.38 2253.16 46899.45 9.52 MW-4 NM NM NM NM NM NM NM NM MW-8 4010.00 39100.00 3620.00 17900.00 0.00 771.00 65401.00 29.58 MW-9 0.00 0.00 0.00 0.00 0.00 0.00 0.00 1.76 MW-15 0.53 0.00 0.00 0.00 0.79 0.00 1.32 2.48 Avg.1336.84 13033.33 1206.67 5966.67 0.26 257.00 21800.77 11.27 MW-4 NM NM NM NM NM NM NM NM MW-8 NM NM NM NM NM NM NM NM MW-9 NM NM NM NM NM NM NM NM MW-15 NM NM NM NM NM NM NM NM Avg.NM NM NM NM NM NM NM NM MW-4 NM NM NM NM NM NM NM NM MW-8 NM NM NM NM NM NM NM NM MW-9 NM NM NM NM NM NM NM NM MW-15 NM NM NM NM NM NM NM NM Avg. NM NM NM NM NM NM NM NM Area 2 09/21/23 13.73 62,100.51 0.0% 39.5% 15.48 150,659.6302/14/22 20.0% 39.5% -83.3% 30.6% 06/12/23 62,100.51 0.0%13.73 -15.3% 07/02/20 71,252.7111.54 -46.7% 11/10/22 13.73 62,100.51 58.8% 39.5% 30.6% 06/08/21 82,175.0011.81 03/12/13 102,686.65 --- ---9.97 Area ID Well ID Area (ft²) Average Well Depth (ft.) Average Depth to Water (ft.) Water Column Height (ft) Volume (ft³) Volume (L) Effective Porosity Effective Volume (L) MW-1 MW-6 MW-4 MW-8 MW-9 MW-15 3 MW-3 79,994 39 26.36 12.64 1,011,126 28,631,858 5,726,372 Area Date Well Benzene (μg/L) Toluene (μg/L) Ethylbenzene (μg/L) Xylenes (μg/L) MTBE (μg/L) Naphthalene (μg/L) Total (μg/L) DTW (ft.) Average Water Column Height (ft.) Total Average Mass (g)Percent Red. To Date Red. 9.9715.032536,642 2,068,966365,325 10,344,830 0.20 12.53 348,424 9,866,259 APPENDIX H CONTAMINANT MASS CALCULATIONS FAST TRACK #145 (INCIDENT NO. 40099) 2 Baseline Event 1 27,807 40.5 27.97 1,973,252 11/13/12 164.00 20.00 23.50 36.50 2.38 3.06 249.44 26.36 12.64 1,428.39 ------ 07/02/20 23.20 0.76 5.80 1.70 0.00 6.50 37.96 21.05 17.95 308.69 78.4%78.4% 06/08/21 25.30 0.41 8.80 0.44 0.00 6.10 41.05 20.15 18.85 350.56 -13.6%75.5% 02/14/22 26.1 0 1.3 0 0 6.6 34.00 23.69 15.31 235.82 32.7% 83.5% 11/10/22 39.7 0.621 1.89 0.706 1.62 9.23 53.77 25.24 13.76 335.17 -42.1%76.5% 06/12/23 34.6 3.76 1.81 10.6 1.1 11.3 63.17 24.28 14.72 421.26 -25.7%70.5% 09/21/23 29.40 3.07 1.24 9.36 0.00 6.8 49.87 25.58 13.42 303.20 28.0% 78.8% Date Average Water Column Height (ft.) 11/13/12 11.71 07/02/20 15.61 06/08/21 16.24 02/14/22 15.33 11/10/22 13.76 06/12/23 13.81 09/21/23 13.42 Notes: • Area of the contaminant plume is calculated from Figure #6 • The January 2014 CSA report ground water data was used to create the baseline event for the purposes of this calculation. Ground water samples were collected on 11/13/12 and 3/12/13. • Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells • Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event • Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs • Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume • When areas couldn’t be sampled, the last known concentrations were used in the calculations. • Monitoring wells MW-4 and MW-15 were not included in the baseline sampling event and are not included in the baseline water column height. 62,404 47.6%65.4% Area 3 MW-3 Percent Reduction Compared to Previous Event ---180,373 Total Contaminant Mass (g)Percent Reduction To Date 119,159 -10.3%33.9% -10.0%-10.0% -26.9%-49.8%228,942 15.2% 108,006 52.8%40.1% 152,881 22.9% 198,324 ---