23061_Caraustar Mills Redevelopment Completion & FG Soil Assessment Report_20231121

Via Email
November 21, 2023

NCDEQ – Division of Waste Management
Brownfields Redevelopment Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Attn: Mr. Bill Schmithorst

Re: Redevelopment Completion & Final Grade Soil Assessment Report
Mill Building and Parking Deck
Caraustar and Savona Mills
500 & 528 S. Turner Avenue
Charlotte, North Carolina
Brownfields Project No. 23061-19-060
H&H Project No. POR-001

Dear Bill:

Please find the enclosed Redevelopment Completion & Final Grade Soil Assessment Report prepared
for the Savona Mill building and associated parking deck located in the southern portion of the
Caraustar and Savona Mills Brownfields property in Charlotte, Mecklenburg County.

Should you have questions or need additional information, please do not hesitate to contact us at
[phone].

Sincerely,
Hart & Hickman, PC
Haley Martin, PG Ralph McGee, PG
Senior Project Geologist Senior Project Manager

Enclosures

cc: Mr. Reid Scott, Portman Holdings (Via Email)
Mr. Cory Case, Portman Holdings (Via Email)
Mr. Peter McGrath, Moore & Van Allen, PLLC (Via Email)
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Redevelopment Completion & Final Grade Soil Assessment Report
Mill Building and Parking Deck
Caraustar and Savona Mills
Charlotte, North Carolina
Brownfields Project No. 23061-19-060
H&H Job No. POR-001

Table of Contents

1.0 Introduction ............................................................................................................................ 1 
2.0 Final Environment-Related Redevelopment Activities ...................................................... 3 
3.0 Final Grade Soil Assessment Activities ................................................................................ 4 
3.1 Final Grade Soil Sampling Activities ................................................................................... 4 
3.2 Final Grade Soil Sample Results .......................................................................................... 5 
3.3 Soil Direct Exposure Risk Evaluation .................................................................................. 6 
3.4 Quality Assurance – Quality Control ................................................................................... 7 
4.0 Summary and Conclusions ................................................................................................... 9 

List of Tables

Table 1 Summary of Final Grade Soil Sampling Lithology
Table 2 Summary of Final Grade Soil Sample Analytical Results

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Final Grade Soil Sample Location Map

List of Appendices

Appendix A Site Plan – Overall prepared by Kimley Horn (January 3, 2022)
Appendix B Reference Plan prepared by Alliance Architecture (September 21, 2021)
Appendix C Laboratory Analytical Report
Appendix D DEQ Risk Calculators
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Redevelopment Completion & Final Grade Soil Assessment Report
Mill Building and Parking Deck
Caraustar and Savona Mills
Charlotte, North Carolina
Brownfields Project No. 23061-19-060
H&H Job No. POR-001

1.0 Introduction

Hart & Hickman, PC (H&H) has prepared this report to document final grade soil sampling
activities recently completed for the Savona Mill building (Mill Building) and associated parking
deck located in the southern portion of the Caraustar and Savona Mill Brownfields property
(Brownfields Project No. 23061-19-060) at 500 and 528 South Turner Avenue in Charlotte,
Mecklenburg County, North Carolina. The Brownfields property is comprised of nine contiguous
parcels (Parcel ID Nos. [PIN] 07111209, 07111412, 07111410, 07111418, 07111417, 07110551,
07110552, 07110501, and 07110503) that collectively total approximately 30.8 acres of land. The
Mill Building and associated parking deck are located on PIN 07111417 which comprises
approximately 8.6 acres of the larger Caraustar and Savona Mills Brownfields property. For the
purposes of this report, the Mill Building and parking deck are identified as the Site or subject Site.
A Site location map for the Caraustar and Savona Mills Brownfields property is provided as
Figure 1, and the Site and surrounding area are shown in Figure 2.

Redevelopment of the Site is complete and included renovations for adaptive reuse of the Mill
Building for commercial offices and retail spaces. Site redevelopment activities also included the
construction of a multi-story parking deck and paved vehicle access and parking areas. A copy of
the Site Plan prepared by Kimley-Horn dated January 3, 2022, depicts the proposed redevelopment
layout and is provided in Appendix A.

Redevelopment activities at the Site have been completed in general accordance with the North
Carolina Department of Environmental Quality (DEQ) approved Environmental Management
Plan (EMP) dated May 10, 2021. Note that Redevelopment plans for the remaining portions of
the Caraustar and Savona Mill Brownfields property include the construction of multiple high-
density residential buildings. Final grade soil assessment and redevelopment summary reports for
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the remaining portions of the Caraustar and Savona Mill Brownfields property will be submitted
to DEQ Brownfields under separate cover.

The EMP for the Site generally states that a report documenting environment-related activities will
be submitted annually for as long as redevelopment at the Site is ongoing. In addition, the EMP
states that no occupancy of the Brownfields property may occur after redevelopment until
representative final grade soil samples have been collected in areas at the Site that are not covered
with a minimum of 2 ft of demonstrably clean fill soil, building foundations, sidewalks, or asphalt
or concrete parking areas and driveways. A copy of the landscape Reference Plan prepared by
Alliance Architecture dated September 21, 2021 depicts the locations of the unpaved areas at the
Site and is provided in Appendix B.

In accordance with the DEQ-approved EMP, H&H prepared a Final Grade Soil Assessment Work
Plan (Work Plan) dated July 20, 2023. The Work Plan received DEQ-approval in an email dated
September 13, 2023. The final environment-related redevelopment activities and the recently
completed final grade soil assessment activities are discussed in the following sections.

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2.0 Final Environment-Related Redevelopment Activities

Redevelopment activities at the Site are complete and included limited grading and upfit for
adaptive commercial/retail reuse of the Mill Building and construction of a multi-story parking
deck. Improvements also included limited grading for the installation of new parking areas,
dumpster enclosures, landscaped areas, concrete sidewalks and handicap access ramps, and
loading areas. Development activities at the Site have been conducted in accordance with the
DEQ-approved EMP dated May 10, 2021. The DEQ-approved-EMP indicates that a report of
environment-related activities will be prepared for submittal to DEQ Brownfields each year for as
long as physical redevelopment of the Brownfields properties continues. A brief summary of
redevelopment activities is provided below.

In accordance with the EMP, soil generated during limited grading activities and installation of
new parking areas, concrete sidewalks and access ramps, and loading areas was reused on the
Brownfields property. Limited amounts of organic-rich topsoil were procured from a commercial
vendor for use in landscaped areas at the Site. Aside from the landscaping soil, no other import or
export of soil was needed for redevelopment of the Site in 2023.

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3.0 Final Grade Soil Assessment Activities

Final grade soil sampling activities were completed at the Site in September 2023 to evaluate
potential soil direct exposure risks within areas at the Site that will not be covered with impervious
materials upon completion of redevelopment activities. The soil sampling activities were
performed in general accordance with the DEQ Inactive Hazardous Sites Branch (IHSB)
Guidelines for Assessment and Cleanup of Contaminated Sites (Guidelines) dated September
2023, the most recent versions of the U.S. Environmental Protection Agency (EPA) Region IV
Laboratory Services and Applied Science Division (LSASD) Field Branches Quality System and
Technical Procedures guidance, and the DEQ-approved Work Plan.

3.1 Final Grade Soil Sampling Activities

Based on review of the proposed landscaping plan (Appendix B), conversations with the PD, and
observations at the Site, landscaped areas at the Site were divided into six (6) final grade evaluation
areas (FG-1 through FG-6). Five (5) shallow soil borings were advanced in each area for collection
of aliquot soil samples. The final grade evaluation areas and aliquot soil boring locations are
shown in Figure 3.

Each aliquot soil boring was advanced from the surface to approximately two (2) ft below the
ground surface (ft bgs) using a decontaminated stainless steel hand auger. Continuous soil samples
were collected from the center of the hand auger bucket at each boring. Soil samples were
described for lithologic purposes, observed for obvious evidence of staining and unusual odors,
and field screened for the presence of volatile organic vapors using a calibrated photoionization
detector (PID). Field screening results did not identify obvious evidence of potential impacts in
soil samples collected at the Site. Lithologic descriptions and field screening results for final grade
soil borings are summarized in Table 1.

Soil sample aliquots collected from soil borings advanced in each evaluation area were combined
and homogenized to form one composite soil sample representative of shallow soil in that
evaluation area. Composite soil samples selected for laboratory analysis were collected directly
into dedicated laboratory supplied sample containers, labeled with the sample identification, date,
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and requested analyses, and placed in a laboratory supplied cooler with ice. The samples were
delivered to Waypoint Analytical (Waypoint) under standard chain of custody protocols for
analysis of semi-volatile organic compounds (SVOCs) by EPA Method 8270 and Resource
Conservation and Recovery Act (RCRA) metals plus hexavalent chromium by EPA Methods
6020/7471/7199.

In addition to the composite soil samples described above, one representative grab soil sample was
collected from each evaluation area from undisturbed portions of soil in the hand auger bucket.
The grab soil samples were placed directly into laboratory supplied glassware, labeled, and placed
in the laboratory supplied sample cooler with ice. The grab soil samples were submitted to
Waypoint for analysis of volatile organic compounds (VOCs) by EPA Method 8260.

Following sampling activities, the soil borings were abandoned using soil cuttings and/or
bentonite, and the surfaces were repaired similar to pre-drilling conditions. Additionally, the soil
boring locations were estimated using a hand-held global positioning system (GPS) unit.

3.2 Final Grade Soil Sample Results

A tabular summary of the final grade soil sample analytical results is presented in Table 2, and a
copy of the laboratory analytical report and chain of custody record is provided in Appendix C.
The laboratory analytical results were compared to the DEQ Residential Preliminary Soil
Remediation goals (PSRGs) dated July 2023. In addition to the PSRGs, metals results were
compared to published concentrations for naturally occurring metals in North Carolina soil and to
background levels for metals established for a nearby off-Site Brownfields property.

VOCs
Laboratory analytical results indicate that trace levels of acetone (up to 0.091 milligrams per
kilogram {mg/kg}), carbon disulfide (up to 0.001 J mg/kg), n-hexane (up to 0.005 J mg/kg), methyl
ethyl ketone (up to 0.010 J mg/kg), and methylene chloride (up to 0.006 J mg/kg) were detected at
concentrations above the laboratory method detection limits, but well below the DEQ Residential
PSRGs in select final grade soil samples. Note that the J-flag designation indicates that the
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compound was detected at a concentration above the laboratory method detection limit, but below
the laboratory reporting limit and is a laboratory estimated value. No other VOCs were detected
at concentrations above the laboratory method detection limits, and no VOCs were detected at
concentrations above the DEQ Residential PSRGs in final grade soil samples collected at the Site.

SVOCs
Laboratory analytical results indicate low levels of polynuclear aromatic hydrocarbons (PAHs)
detected in select final grade soil samples at concentrations exceeding the DEQ PSRGs.
Benzo(a)pyrene (up to 2.25 J mg/kg) was detected at concentrations above the DEQ Residential
and/or Commercial/Industrial PSRGs in final grade soil samples FG-1 and its duplicate soil sample
FG-DUP, FG-2, FG-3, and FG-4. Benzo(a)anthracene (up to 2.22 J mg/kg) was detected at
concentrations above the DEQ Residential PSRG in final grade soil sample FG-3.
Benzo(b)fluoranthene (up to 2.86 J mg/kg) was detected in final grade soil samples FG-2 and FG-3
at concentrations above the DEQ Residential PSRG. Indeno(1,2,3-cd)pyrene (1.47 J mg/kg) was
detected at a concentration above the DEQ Residential PSRG in sample FG-3.

Several other SVOCs were detected at concentrations above the laboratory method detection limits
in the final grade soil sample, but no other SVOCs were detected at concentrations above the DEQ
Residential PSRGs.

Metals
Several metals including arsenic (up to 6.92 mg/kg), barium (up to 110 mg/kg), cadmium (up to
0.268 J mg/kg), trivalent chromium (up to 92.4 mg/kg), hexavalent chromium (up to 0.707 mg/kg),
lead up to 82.2 mg/kg), mercury (up to 0.156 mg/kg), selenium (up to 0.910 mg/kg), and silver (up
to 0.0859 J mg/kg) were detected at concentrations consistent with naturally occurring levels and
are considered to be representative of background conditions at the Site.

3.3 Soil Direct Exposure Risk Evaluation

The DEQ PSRGs are very conservative and based upon a Target Cancer Risk (TCR) of 1 x 10-6
for potential carcinogenic effects and a Hazard Quotient (HQ) of 0.2 for potential non-carcinogenic
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effects. DEQ and EPA acceptable soil direct exposure risks include a calculated cumulative
lifetime incremental carcinogenic risk (LICR) of 1 x 10-4 or less and a calculated cumulative hazard
index (HI) of 1.0 or less for potential non-carcinogenic risks.

H&H utilized the DEQ Risk Calculator (July 2023) under a residential and commercial land use
to further evaluate potential cumulative risks for the soil direct exposure pathway. To model the
potential risks under a hypothetical “worst-case” scenario, H&H conservatively calculated the
cumulative risks using the highest concentration of any compound detected in any final grade soil
sample collected at the Site. Risk calculator results are summarized in the table below and copies
of the completed risk calculators are provided in Appendix C.

Evaluation Area Land Use
Calculated
Cumulative
LICR
Calculated
Cumulative
HI
Exceeds
Acceptable
Risk Levels?
Cumulative Worst Case
Residential 3.8 x 10-5 0.39 No
Non-Residential 3.8 x 10-6 0.029 No

As shown in the table above, the results of the risk calculations indicate that the calculated
cumulative soil direct exposure risks do not exceed acceptable carcinogenic or noncarcinogenic
risk levels under a residential or commercial use scenario.

3.4 Quality Assurance – Quality Control

For quality assurance and quality control purposes (QA/QC), non-dedicated equipment and tools
were decontaminated prior to use at each evaluation area and following exposure to soil or
groundwater. H&H collected duplicate soil sample (DUP-1) from evaluation area FG-1 to
evaluate the ability of the laboratory to reproduce sample results. Duplicate samples were collected
to evaluate the precision of the field sampling procedures, sample matrix variability, and analytical
reproducibility. The duplicate soil sample was collected directly into individual laboratory
supplied sample containers using sampling methodologies described in previous section. The
duplicate sample was submitted to the laboratory for the same analysis as the corresponding parent
sample.
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Duplicate sample laboratory analytical results are presented in Table 2. Review of the duplicate
sample results in comparison to the parent sample results indicate a discrepancy greater than 10%
for select compounds which is likely associated with sample matrix variability.

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4.0 Summary and Conclusions

H&H has completed final grade soil sampling activities at the mill building and parking deck
portion of the Caraustar and Savona Mills Brownfields property (Brownfields Project No. 23061-
19-060) located at 500 and 528 South Turner Avenue in Charlotte, North Carolina. The final grade
soil sampling activities were conducted in general accordance with the DEQ Brownfields approved
Work Plan dated July 20, 2023. Final grade soil sampling activities included the collection of soil
samples to evaluate potential soil direct exposure risks in areas at the Site that will not be covered
by impervious surfaces following completion of redevelopment.

The Site was divided into six final grade evaluation areas and shallow soil samples were collected
for laboratory analysis within each area. Final grade soil sample laboratory analytical results
indicate that several organic compounds were detected at concentrations above the laboratory
method detection limits in each final grade evaluation area. No compounds were detected at
concentrations above the DEQ Residential PSRGs except low level PAHs in evaluation areas FG-1
through FG-4. Metals concentrations detected in the final grade soil sample are consistent with
published and area-specific background concentrations and are considered representative of
naturally occurring levels.

H&H utilized the most recent version of the DEQ Risk Calculator to further evaluate potential soil
direct exposure risks for residential and non-residential occupants. The risk calculations were
completed for a hypothetical worst-case scenario using the highest concentration of any compound
detected in any final grade evaluation area. Results of the residential and non-residential soil direct
exposure risk calculations confirm that cumulative risks are within acceptable levels for a future
residential or non-residential occupant.

Tables

Table 1 Summary of Final Grade Soil Sampling LithologyCaraustar and Savona Mills - Mill Building and Parking DeckCharlotte, North CarolinaH&H Project No. POR-001Composite Sample AreaComposite Sample AliquotSample DateAliquot Selected for VOC AnalysisDepth (ft bgs)Moisture ContentStiffness Color LithologyPID Readings (ppm)NotesA----0-11-2MoistMoistLooseMedium StiffLight BrownLight BrownSilt, few gravelSandy Clayey Silt, few gravel0.30.2gravel at 1 ft bgsBx--0-11-2MoistMoistMedium StiffMedium StiffLight BrownLight BrownSilt, few gravelSandy Clayey Silt, few gravel0.50.4--C----0-11-2MoistMoistMedium StiffMedium StiffLight BrownLight BrownClayey Silt, some gravelClayey Silt, some gravel, few sand0.30.1--D----0-11-2MoistMoistLooseLooseReddish BrownReddish BrownSilty Sand, few gravelSandy Silt, few medium sand, gravel0.40.3--E----0-11-2MoistMoistMedium StiffMedium StiffReddish BrownReddish BrownSandy Clayey Silt, few gravelSandy Clayey Silt0.30.3gravel at 1.5 ft bgsA----0-11-2MoistMoistMedium StiffMedium StiffLight BrownLight BrownClayey Silt, some gravel, few sandClayey Silt, some gravel2.72.7--Bx--0-11-2MoistMoistMedium StiffMedium StiffLight Reddish BrownLight Reddish BrownSilt, few gravelSandy Clayey Silt, few gravel3.52.8--C----0-11-2MoistMoistLooseLooseLight Reddish BrownLight Reddish BrownSandy Silt, some gravel, few sandClayey Silt, few sand some gravel2.31.7--D----0-11-2MoistMoistMedium StiffMedium StiffLight Reddish BrownLight Reddish BrownClayey Sandy Silt, some gravelClayey Silt, some gravel, sand2.42.0--E----0-11-2MoistMoistMedium StiffMedium StiffLight Reddish BrownLight Reddish BrownSandy Clayey Silt, some gravelClayey Silt, some gravel1.81.2--A----0-11-2MoistMoistMedium StiffMedium StiffLight BrownLight BrownClayey Silt, some gravel, few sandClayey Silt, some gravel0.20.1--B----0-11-2MoistMoistMedium StiffMedium StiffLight BrownLight BrownClayey Silt, some gravel, few sandClayey Silt, some gravel0.40.7--C----0-11-2MoistMoistMedium StiffMedium StiffLight BrownLight BrownSandy Clayey Silt, few gravelSandy Clayey Silt, few gravel0.30.1--D----0-11-2MoistMoistMedium StiffMedium StiffLight BrownLight BrownSandy Clayey Silt, few gravelSandy Clayey Silt, few gravel0.40.9--E--x0-11-2MoistMoistMedium StiffMedium StiffLight BrownLight BrownSandy Clayey Silt, few gravelSandy Clayey Silt, few gravel1.71.9--A----0-11-2MoistMoistLooseMedium StiffLight BrownLight BrownSandy Silt, few gravelSandy Clayey Silt, few gravel0.60.9--B----0-11-2MoistMoistMedium StiffMedium StiffReddish BrownReddish BrownSandy Silt, some clay, few gravelSandy Clayey Silt, few gravel0.70.2--C--x0-11-2MoistMoistMedium StiffMedium StiffReddish BrownReddish BrownSandy Silt, few gravelSandy Clayey Silt, few gravel1.41.8--D----0-11-2MoistMoistMedium StiffMedium StiffReddish BrownReddish BrownSandy Clayey Silt, few gravelSandy Clayey Silt, few gravel1.71.4--E----0-11-2MoistMoistMedium StiffMedium StiffReddish BrownReddish BrownSilt, few gravelSandy Clayey Silt, few gravel1.21.3--A----0-11-2MoistMoistMedium StiffMedium StiffDark BrownDark BrownSandy Clayey Silt, few gravelSandy Clayey Silt, few gravel0.70.4--B----0-11-2MoistMoistMedium StiffMedium StiffReddish BrownReddish BrownSandy Clayey SiltSandy Clayey Silt, few gravel1.21.7--Cx--0-11-2MoistMoistLooseMedium StiffReddish BrownReddish BrownSandy Silt, few gravelSandy Clayey Silt, few gravel3.11.2--D----0-11-2MoistMoistMedium StiffMedium StiffDark BrownDark BrownSandy Clayey Silt, few gravelSandy Clayey Silt, few gravel0.90.8--E----0-11-2MoistMoistMedium StiffMedium StiffReddish BrownReddish BrownSandy Clayey Silt, few gravelSandy Clayey Silt, few gravel1.20.9--A----0-11-2MoistMoistMedium StiffMedium StiffBrownBrownSilt, few gravelSandy Clayey Silt, few gravel0.70.9grass and topsoil 0-4 inchesB----0-11-2MoistMoistMedium StiffMedium StiffBrownBrownSandy Clayey Silt, few gravelSandy Clayey Silt, few gravel1.21.4grass and topsoil 0-4 inchesC----0-11-2MoistMoistMedium StiffMedium StiffBrownBrownSilt, few gravelSandy Clayey Silt, few gravel2.72.3grass and topsoil 0-4 inchesDx--0-11-2MoistMoistMedium StiffMedium StiffBrownBrownSandy Clayey Silt, few gravelSandy Clayey Silt, few gravel4.23.1grass and topsoil 0-4 inchesE----0-11-2MoistMoistMedium StiffMedium StiffBrownBrownSandy Clayey Silt, few gravelSandy Clayey Silt, few gravel0.80.9grass and topsoil 0-4 inchesFG-5 9/21/2023Notes:PID = photoionization detector; ppm = parts per million; VOC = volatile organic compound; ft bgs = feet below ground surface; -- = not applicable * = selected for duplicate sampleFG-2FG-1*FG-3FG-49/21/20239/21/20239/21/20239/21/2023FG-6 9/21/2023https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Portman Holdings/Caraustar & Savona Mill/Mill Building_Final Grade/Tables/TCR.001 Final Grade lithologyTable 1 (Page 1 of 1)Hart & Hickman, PC
Table 2Summary of Final Grade Soil Sample Analytical ResultsCaraustar and Savona Mills - Mill Building and Parking Deck Charlotte, North CarolinaH&H Job No. POR-001Evaluation AreaSample IDDateDepth (ft bgs)0-1 0-2 0-1 0-2 0-1 0-2 1-2 0-2 1-2 0-2 0-1 0-2 0-1 0-2Sample Type Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab CompositeUnitsVOCs (8260D)Acetone0.071NA0.064NA0.052NA0.091NA0.006 JNA0.010 JNA0.034NA14,000 210,000-- --Carbon Disulfide<0.0007 NA <0.0007 NA <0.0007 NA0.001 JNA <0.0007 NA <0.0008 NA <0.0008 NA160 740-- --n-Hexane 0.003 JNA0.005 JNA0.003 JNA0.003 JNA0.004 JNA <0.0008 NA0.003 JNA130 540-- --Methyl Ethyl Ketone (MEK)<0.0007 NA <0.0007 NA0.002 JNA0.010 JNA <0.0007 NA <0.0008 NA <0.0008 NA5,500 40,000-- --Methylene Chloride0.004 JNA0.006 JNA0.005 JNA0.005 JNA0.005 JNA <0.001 NA0.004 JNA58 650-- --SVOCs (8270E)Acenaphthene NA0.144 JNA <0.124 NA0.217 JNA <0.576 NA <0.131 NA <0.563 NA <0.562720 9,000-- --Anthracene NA0.438 JNA0.336 JNA0.388 JNA0.716 JNA0.169 JNA <0.694 NA <0.6933,600 45,000-- --Benzo(a)anthraceneNA0.750NA0.669 JNA1.00NA2.22 JNA0.464 JNA <0.674 NA <0.6731.1 21-- --Benzo(a)pyreneNA0.740NA0.668 JNA0.997NA2.25 JNA0.471 JNA<0.713NA<0.7120.11 2.10-- --Benzo(b)fluorantheneNA1.00NA0.969NA1.33NA2.86 JNA0.547 JNA0.717 JNA0.772 J1.1 21-- --Benzo(g,h,i)perylene NA0.499 JNA0.468 JNA0.615 JNA1.38 JNA0.300 JNA <0.660 NA <0.659NE NE-- --Benzo(k)fluoranthene NA0.360 JNA0.265 JNA0.381 JNA1.00 JNA0.181 JNA <0.665 NA <0.66411 210-- --ChryseneNA0.734NA0.651 JNA0.965NA2.14 JNA0.442 JNA <0.689 NA <0.688110 2,100-- --DibenzofuranNA0.159 JNA <0.127 NA <0.127 NA <0.591 NA <0.135 NA <0.577 NA <0.57616 230-- --FluorantheneNA1.64NA1.38NA1.99NA4.25NA0.737 JNA1.02 JNA1.07 J480 6,000-- --FluoreneNA <0.138 NA <0.137 NA0.156 JNA <0.636 NA <0.145 NA <0.621 NA <0.620480 6,000-- --Indeno(1,2,3-cd)pyreneNA0.510 JNA0.489 JNA0.670 JNA1.47 JNA0.301 JNA <0.868 NA <0.8671.1 21-- --1-MethylnaphthaleneNA0.212 JNA0.117 JNA <0.113 NA <0.526 NA0.130 JNA <0.514 NA <0.51318 73-- --2-MethylnaphthaleneNA0.286 JNA0.160 JNA <0.107 NA <0.496 NA0.120 JNA <0.485 NA <0.48448 600.0-- --Naphthalene NA0.264 JNA <0.154 NA <0.154 NA <0.715 NA <0.163 NA <0.699 NA <0.6982.1 8.8-- --PhenanthreneNA1.63NA1.14NA1.55NA2.80 JNA0.699 JNA <1.01 NA <1.01NE NE-- --PyreneNA1.54NA1.31NA1.80NA3.98NA0.891NA0.956 JNA1.06 J360 4,500-- --Metals (6020B/7471B/7199)ArsenicNA6.92NA5.28NA4.05NA4.71NA1.91NA1.77NA1.88 0.68 3.00 1.1 - 3.0 1.0 - 18BariumNA80.9NA81.6NA73.0NA85.8NA61.1NA110NA102 3,100 47,000 38 - 110 50 - 1,000CadmiumNA0.100 JNA0.0863 JNA0.147 JNA0.268 JNA0.0552 JNA0.0639 JNA0.135 J 1.4 20ND - 0.36 J1.0 - 10Chromium (total)NA23.4NA25.0NA33.7NA92.8NA24.1NA24.0NA30.5 NE NE 14 - 45 7.0 - 300Hexavalent ChromiumNA0.369NA0.408NA0.612NA0.411NA0.389NA0.707NA0.294 0.31 6.5 0.34 J - 0.98 J NSTrivalent ChromiumNA23.0NA24.6NA33.1NA92.4NA23.7NA23.3NA30.2 23,000 350,000 13.7 - 44.0 NSLeadNA16.9NA15.4NA24.9NA82.2NA6.40NA11.3NA23.2 400 800 11 - 36 ND - 50MercuryNA0.0181 JNA0.124NA0.115NA0.0920NA0.0279 JNA0.0421NA0.156 4.7 700.024 J - 0.0970.03 - 0.52SeleniumNA0.615NA0.706NA0.628NA0.904NA0.572NA0.910NA0.683 78 1,200 ND <0.1 - 0.8SilverNA0.0331 JNA0.0312 JNA0.0490 JNA0.0559 JNA0.0219 JNA0.0300 JNA0.0859 J 78 1,200 0.033 J - 0.60 ND - 5.0Cumulative Risk Calculations (4)Worst Case Residential LICRWorst Case Residential Non-Carcinogenic HIWorst Case Non-Residential LICRWorst Case Non-Residential Non-Carcinogenic HINotes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2023 and based upon a TCR of 1 x 10-6 and THQ of 0.2. 2) Background metals data collected from Cotton Warehouse Brownfields property (Brownfields Project No. 24013-20-060). 3) Range values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils. 4) DEQ Cumulative Risk Calculator dated July 2023. Concentrations are reported in milligrams per kilogram (mg/kg).Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses. Aside from metals, only those compounds detected in at least one sample are shown in the table above. Bold values exceed the Residential PSRGs and background levels in the case of metals.Underlined values exceed the Industrial/Commercial PSRGs and background levels in the case of metals.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; LICR = lifetime incremental cancer risk; HI = hazard index; TCR = target cancer risk; THQ = target hazard quotient ft bgs= feet below ground surface; NS = not specified; NE = not established; -- = not applicable; ND = not detected; NA = not analyzedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. <1.0<1.0 x 10-4<1.0Acceptable Risk Levels3.8 x 10-50.393.8 x 10-60.029<1.0 x 10-4FG-5Residential PSRGs (1)Nearby Brownfields Property (2)Published (3)Rangemg/kgBackground Metals 9/21/2023 9/21/2023FG-6FG-4Screening CriteriaIndustrial/ Commercial PSRGs (1)Final Grade9/21/2023 9/21/20239/21/20239/21/2023FG-1 / FG-DUP FG-2 FG-3https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Portman Holdings/Caraustar & Savona Mill/Mill Building_Final Grade/Tables/Data TableTable 2 (Page 1 of 1) Hart & Hickman, PC

Figures

USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset,and National Transportation Dataset; USGS Global Ecosystems; U.S.Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data;U.S. Department of State Humanitarian Information Unit; and NOAANational Centers for Environmental Information, U.S. Coastal ReliefModel. Data refreshed June, 2022.
SITE LOCATION MAP
CARAUSTAR AND SAVONA MILLS MILL BUILDING AND PARKING DECK 500 & 528 S. TURNER AVENUE CHARLOTTE, NORTH CAROLINA
DATE: 10-17-23
JOB NO: POR-001
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: S:\AAA-Master Projects\Portman Holdings\Caraustar & Savona Mill\Blue Blaze - Additional Assessment\Figures\Figure-1-2023.mxdN
U.S.G.S. QUADRANGLE MAP
CHARLOTTE EAST, NORTH CAROLINA 2019
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
WIKOFFCOLOR
FORMER OLD
DOMINION BOX CO.
FORMERINKMANUFACTURINGFACILITYS. TURNER AVENUECOXE AVENUE
CH
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S. GARDNER AVENUESTEWART CREEKBLUEBLAZEBREWING
SAVONA MILLBUILDING
STATE STREET
RES.07
RES.08
RES.09
RES.06
RES.05
RES.01
RES.02RES.04
RES.03
REVISION NO. 0
JOB NO. POR-001
DATE: 10-17-23
FIGURE NO. 2
CARAUSTAR AND SAVONA MILLS
MILL BUILDING AND PARKING DECK500 & 528 S. TURNER AVENUE CHARLOTTE, NORTH CAROLINA
SITE MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL LINE
PROPOSED RESIDENTIAL BUILDING
PARKING DECK
FINAL GRADE EVALUATION AREA
NOTES:
1. AERIAL IMAGERY AND BASE DATA OBTAINED FROMMECKLENBURG COUNTY GIS, 2023.
2. PROPOSED REDEVELOPMENT PLAN OVERLAY TAKENFROM SITE PLAN PREPARED BY KIMLEY HORN DATED1/17/2022.
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
S:\AAA-Master Projects\Portman Holdings\Caraustar & Savona Mill\Mill Building_Final Grade\Figures\SITE MAP.dwg, FIG 2, 10/6/2023 9:36:55 AM, draburn
REVISION NO. 0
JOB NO. POR-001
DATE: 10-17-23
FIGURE NO. 3
FINAL GRADE SOIL SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL LINE
PROPOSED RESIDENTIAL BUILDING
PARKING DECK
PROPOSED LANDSCAPED AREA
PROPOSED PAVED PARKING OR VEHICLE ACCESS
FG-1 SOIL SAMPLE ALIQUOT LOCATION
FG-2 SOIL SAMPLE ALIQUOT LOCATION
FG-3 SOIL SAMPLE ALIQUOT LOCATION
FG-4 SOIL SAMPLE ALIQUOT LOCATION
FG-5 SOIL SAMPLE ALIQUOT LOCATION
FG-6 SOIL SAMPLE ALIQUOT LOCATION
NOTES:
1.BASE DATA OBTAINED FROM MECKLENBURG COUNTY GIS, 2023.
2.LANDSCAPE REFERENCE PLAN PREPARED BY ALLIANCE ARCHITECTURE DATED APRIL 8, 2022.
3. FINAL GRADE SOIL SAMPLES COLLECTED BY H&H ON SEPTEMBER 21, 2023.
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 GeologySAVONA MILL BUILDINGFORMER INK
MANUFACTURING
FACILITY
BLUE BLAZE BREWING
COXE AVENUE
STATE STREETS. TURNER AVENUESTEWART CREEKRES.03
FG-6A
FG-6B
FG-6C
FG-6D
FG-6E
FG-5E
FG-5D
FG-5C
FG-5B
FG-5A
FG-1E
FG-1D
FG-1C
FG-1B
FG-1A
FG-3E
FG-3A
FG-3B
FG-3C
FG-3D
FG-2A
FG-2B
FG-2C FG-2D
FG-2E
FG-4E
FG-4D
FG-4C
FG-4A FG-4B
CARAUSTAR AND SAVONA MILLS
MILL BUILDING AND PARKING DECK500 & 528 S. TURNER AVENUE CHARLOTTE, NORTH CAROLINA
S:\AAA-Master Projects\Portman Holdings\Caraustar & Savona Mill\Mill Building_Final Grade\Figures\SITE MAP.dwg, FIG 3, 10/6/2023 9:37:26 AM, draburn

Appendix A
Site Plan – Overall prepared by Kimley Horn (January 3, 2022)

EV EV EV EV EV EV
CCCCCCCCCCCCCCCCCCCCC C C C C C C C CCCCCCCCCCC CC C C C C C C C C C CCCCCCCCCCCC EXISTING SAVONAMILL BUILDING±192,298 S.F.CCCCCCCCCCCCCC
EXISTING BLUEBLAZE BREWING±8,326 S.F.COX
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FUTURE MULTI-FAMILY
DEVELOPMENT BY
SEPARATE PLAN
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16 17 18
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EXISTING B
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±31,590 S.F.
SAVONA MILL LANE
(PRIVATE ROAD)
FEMA CROSS SECTION 078
EXISTING 100-YEAR W.S.E: 651.1
FUTURE 100-YEAR W.S.E: 651.4
FEMA CROSS SECTION 068
EXISTING 100-YEAR W.S.E: 650.7
FUTURE 100-YEAR W.S.E: 651.1
FEMA CROSS SECTION 086
EXISTING 100 YEAR W.S.E: 651.5
FUTURE 100 YEAR W.S.E: 651.9
MECKLENBURG COUNTY
GREENWAY PROJECT
SHOWN FOR REFERENCE
ONLY. SEE GREENWAY
PLANS FOR DETAILS.
EXISTING 25' SANITARY
SEWER EASEMENT
PROPERTY LINE
PROPERTY LINE
EXISTING FEMA 100- YR
FLOOD PLAIN
EXISTING 25' SANITARY
SEWER EASEMENT
STREAM MANAGED
USE BUFFER
STREAM UPLAND
BUFFER
EXISTING FEMA 100-YR FLOODPLAIN.
DEVELOPMENT WITHIN THE
FLOODPLAIN TO BE PERMITTED
THROUGH MECKLENBURG COUNTY.
STREAM SIDE
ZONE BUFFER
STREAM TOP OF BANK
EXISTING FEMA
100-YR FLOODPLAIN
DUMPSTER ENCLOSURE
EXISTING RAILROAD
PARCEL LINE
SEE SHEETS C810-C844
FOR ROADWAY IMPROVEMENTS
TO CHAMBERLAIN AVE
SEE SHEETS C810-C844
FOR ROADWAY IMPROVEMENTS
TO S. TURNER AVE
ELEVATED DECK
LEVEL AT FIRST
FLOOR. OPEN TO
BASEMENT ACCESS
BELOW AT FIRST
FLOOR ELEVATION
ELEVATED
BRIDGES BETWEEN
TOP OF PARKING
DECK AND
BUILDING
PROPOSED PATIO AREA
1,888 SF
SHARED USE PATH TO BE
CONTINUED WITH FUTURE
DEVELOPMENT PLANS
LOWER DECK
ENTRANCE LOCATION
PROPOSED CONNECTION OF SHARED USE PATH TO
MECKLENBURG COUNTY GREENWAY PROJECT.
SHOULD THE GREENWAY NOT BE COMPLETED AT
TIME OF CONSTRUCTION, CONTRACTOR SHALL
STOP SHARED USE PATH AT EDGE OF GREENWAY.
EXISTING BUILDING
±4,875 SF
PROPOSED TREE SAVE AREA.
REFER TO LANDSCAPE PLANS
UNDISTURBED TREE SAVE AREA.
REFER TO LANDSCAPE PLANS
PROPOSED PAVEMENT
SAWCUT
PROPOSED 30' STORM
DRAINAGE EASEMENT
PROPOSED PARKING DECK .
REFERENCE PLANS BY ARCHITECT.
PARKING SHOWN ON THIS PLAN IS
AT GRADE BELOW THE PARKING
DECK STRUCTURE.
EXISTING ALLEY TO
BE ABANDONED
EXISTING ALLEY TO
BE ABANDONED
PRIMARY ACCESS TO BE EXTENDED
WITH FUTURE DEVELOPMENT. REFER
TO REZONING PETITION #2021-021
UPPER DECK
ENTRANCE LOCATION
PROPOSED COVERED PATIO
REFER TO ARCH. PLANS FOR DETAILS
± 2,279 S.F.
NOTE: NO MODIFICATIONS
ARE PROPOSED TO THESE
EXISTING BUILDINGS/USES
WITH THIS PROJECT.
NOTE: NO MODIFICATIONS
ARE PROPOSED TO THESE
EXISTING BUILDINGS/USES
WITH THIS PROJECT.
3-WAY STOP CONTROLLED INTERSECTION
3-WAY STOP CONTROLLED INTERSECTION
REFERENCE HARDSCAPE /
ARCHITECTURAL PLANS
FOR PAVING / SITE PLAN
ITEMS
10'x50' LOADING ZONE
PROPOSED 25' STORM
DRAINAGE EASEMENT
30.0'
25.0'
PROPOSED TREE SAVE AREA.
REFER TO LANDSCAPE PLANS
NOTE: PARCELS ACROSS S. TURNER
AVE. ARE NOT CONSIDERED PART OF
THIS PROJECT. ALL CODE
REQUIREMENTS ARE MET ON SITE.
PROPOSED OPEN SPACE
±2,454 SF
LEGEND
SAVONA MILLRENOVATIONPREPARED FORPORTMAN HOLDINGSSITE PLAN - OVERALLC301©Know what's
R
NORT
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ZONING SUMMARY TABLE
PARCEL ID 071-11-209, 071-11-403, 071-11-412, 071-11-417
PARCEL ACREAGE 27.65 ACRES
FEMA PANEL MAP 371045400K
CURRENT ZONING MUDD-O (REZONING PETITION #CC 2016-112)
PROPOSED USE OFFICE AND RETAIL
BUILDINGS PROPOSED 0 (1 EXISTING)
SETBACK 14 FEET FROM BACK OF CURB
SIDE YARD 0 FEET
REAR YARD 0 FEET
PARKING REQUIRED PER REZONING 1 SPACE/600 SF204,791SF * 1SPACE/600SF = 342 SPACES
ADA PARKING REQUIRED 11 SPACES
TOTAL PARKING PROVIDED 470 SPACES
ON TOP OF DECK 190 SPACES (INCL. 4 ADA SPACES)
BELOW DECK 159 (INCL. 7 ADA AND 34 COMPACT)
SURFACE PARKING (NOT BELOW DECK)110 SPACES (INCL. 42 COMPACT)
ON-STREET PARKING 11 SPACES (CHAMBERLAIN AVE.)
LONG TERM BIKE PARKING REQUIRED OFFICE: 2 OR 1 PER 10,000 S.F. OR 50 MAXRETAIL: 2 OR 1 PER 12,000 S.F. OR 1 PER 25EMPLOYEES OR 30 MAX
LONG TERM BIKE PARKING PROVIDED 24 SPACES
SHORT TERM BIKE PARKING REQUIRED OFFICE: 2 OR 1 PER 40,000 S.F. OR 30 MAXRETAIL: 5% OF AUTO PARKING OR 50 MAX
SHORT TERM BIKE PARKING PROVIDED 10 SPACES
OPEN SPACE REQUIRED 1 SF OPEN SPACE PER 100 GROSS SF OF FLOORAREA : 204,791 GROSS FLOOR AREA/100 SF = 2048 SF
OPEN SPACE PROVIDED 2,454 SF
PROPOSED USES OFFICE: 185,854 SFRETAIL: 18,937 SF (INCL. PATIOS AND BLUE BLAZE)
OVERALL DEVELOPMENT DATA
EXISTING BUILDING(ADDRESS)BEGINNINGSF
EXPANDED SFALLOWANCE(15% MAX)
ACTUALEXPANSION EXPANSIONDESCRIPTION
DATE OFEXPANSIONPERMIT
% OF SITETOTALOCCUPANCY
500 S TURNER AVE 178,870 26,831 192,298 THIS PLAN
401 S GARDNER AVE 4852 728
411 S GARDNER AVE 60,180 9,027
2426 CHAMBERLAIN AVE 24,544 3,682
528 S TURNER AVE 8,326 1,249
TRANSPORTATION IMPROVEMENT TRACKING TABLEDEVELOPMENTNAME &REZONING #
SUBMITTAL NAME& PHASE #
DEVELOPMENTENTITLEMENTS(SF/UNITS)
PROPOSEDENTITLEMENTS ACELLA PROJECT #ACELLAPROJECT NAME PROJECT DESCRIPTION STATUS ROADWAY IMPROVEMENTDESCRIPTION
ROADWAYIMPROVEMENTSTATUS
SAVONA MILL2021-021 COMMERCIAL /OFFICE
ALL COMMERCIALUSES PERMITTEDBY REZONING LDUMUDD-2021-00037 SAVONA MILLRENOVATION
RENOVATION OF EXISTINGMILL BUILDING(COMMERCIAL SPACE)THIS PLAN 2, 3, 4(PARTIAL), 5, 6,7B(PARTIAL)PROPOSED WITHTHIS PLAN
THE FOLLOWING TRANSPORTATION IMPROVEMENTS ARE REQUIRED AS PART OF THE APPROVED REZONING PLAN.REFER TO THE TABLE BELOW FOR IMPROVEMENTS AND ENTITLEMENTS PROPOSED AS PART OF THIS PLAN.
ON-SITE IMPROVEMENTS1.IMPROVEMENTS ALONG BOTH SIDES OF THE SITE'S FRONTAGE OF GARDNER AVENUE, TO BE IMPROVED TOSTREETSCAPE CONDITIONS AS DEPICTED IN THE CROSS-SECTIONS PROVIDED ON SHEET RZ-05, OR AS OTHERWISEMUTUALLY AGREED UPON IN COORDINATION WITH CDOT,SHALL BE PROVIDED PRIOR TO THE ISSUANCE OF THEFIRST CERTIFICATE OF OCCUPANCY AREA A.2.IMPROVEMENTS ALONG BOTH SIDES OF THE SITE'S FRONTAGE OF CHAMBERLAIN AVENUE, TO BE IMPROVED TOSTREETSCAPE CONDITIONS AS DEPICTED IN THE CROSS-SECTIONS PROVIDED ON SHEET RZ-05, OR AS OTHERWISEMUTUALLY AGREED UPON IN COORDINATION WITH CDOT,SHALL BE PROVIDED PRIOR TO THE ISSUANCE OF THEFIRST CERTIFICATE OF OCCUPANCY AREA A.3.IMPROVEMENTS TO THE SITE'S FRONTAGE OF SOUTH TURNER AVENUE, TO BE IMPROVED TO STREETSCAPECONDITIONS AS DEPICTED IN THE CROSS-SECTIONS PROVIDED ON SHEET RZ-05, OR AS OTHERWISE MUTUALLYAGREED UPON IN COORDINATION WITH CDOT,SHALL BE PROVIDED PRIOR TO THE ISSUANCE OF THE FIRSTCERTIFICATE OF OCCUPANCY AREA A.4.IMPROVEMENTS TO THE NEW ROAD A, AS GENERALLY DEPICTED IN THE CROSS-SECTIONS PROVIDED ON SHEETRZ-05, OR AS OTHERWISE MUTUALLY AGREED UPON IN COORDINATION WITH CDOT, SHALL BE PROVIDED PRIOR TOTHE ISSUANCE OF THE FIRST CERTIFICATE OF OCCUPANCY AREA A.
OFF-SITE IMPROVEMENTS5.AT THE INTERSECTION OF S TURNER AVENUE AND SITE ACCESS ROAD A:5.A.CONSTRUCTION OF THE EASTBOUND APPROACH WITH ONE INGRESS AND ONE EGRESS LANE AND INTERNALPROTECTED STEM OF 100 FEET;5.B.INSTALLATION OF STOP-CONTROL ON ALL THREE APPROACHES TO CREATE AND ALL-WAY STOP CONDITION5.C.INSTALLATION OF A 25 MILES PER HOUR(MPH) POSTED SPEED LIMIT SIGN ALONG S TURNER AVENUE.6.AT THE INTERSECTION OF S TURNER AVENUE AND COXE AVENUE:6.A.INSTALLATION OF STOP-CONTROL ON ALL THREE APPROACHES TO CREATE AND ALL-WAY STOP CONDITION.7.PEDESTRIAN IMPROVEMENTS:7.A.CONSTRUCTION OF TWO (2) PEDESTRIAN CROSSINGS ALONG ROZZELLES FERRY ROAD, ONE WEST OF TURNERAVENUE AND ONE AT STEWART AVENUE. THE REQUIRED SIGNING/SIGNALING OF THIS CROSSING SHOULD BECONFIRMED WITH CDOT;7.B.CONSTRUCTION OF A NORTH-SOUTH GREENWAY ALIGNMENT FOR A SHARED-USE PATH CONNECTION THROUGHTHE PROPOSED SITE TO ADA-COMPLIANT STANDARDS, SUCH AS CLDSM STANDARD DETAIL NUMBER 10.42, WITHA MINIMUM WIDTH OF 12' FOR THE PORTION WITHIN THE PUBLIC RIGHT-OF-WAY AND MINIMUM WIDTH OF 10' FORTHE PORTION ON THE PRIVATE SITE, AND CONSTRUCTED OF MATERIALS SUCH AS ASPHALT, GRAVEL, ORCONCRETE (FINAL MATERIAL TO BE REVIEWED AND APPROVED BY CDOT DURING PERMITTING), IN THELOCATION AS GENERALLY DEPICTED ON THE REZONING PLAN AND PHASED PER REZONING PLAN.
PARCEL DATA TABLE
KEYNOTE DESCRIPTION
SAVONA RESI PROJECT, LLC (C/O PORTMAN HOLDINGS, LLC)PIN: 071-11-412ZONING: MUDD-OSAVONA RESI PROJECT, LLC (C/O PORTMAN HOLDINGS, LLC)PIN: 071-11-417ZONING: MUDD-OSAVONA II LLCPIN: 071-11-418ZONING: MUDD-OSAVONA RESI PROJECT, LLC (C/O PORTMAN HOLDINGS, LLC)PIN: 071-11-209ZONING: MUDD-OBRYANT W. CUTTER & NANCY CUTTERPIN: 071-11-415ZONING: I-2410 SG PARTNERS LLCPIN: 071-11-410ZONING: I-2MECKLENBURG COUNTYPIN: 071-14-340ZONING: I-1DEEPAK SINGH & SHARON SINGHPIN: 071-11-307ZONING:DANNY CHAOPIN: 071-11-313ZONING: R-8KIMBERLY JEAN CRUICKSHANKSPIN: 071-11-312ZONING: R-8KEVIN D. HICKEYPIN: 071-11-303ZONING: R-8MEGAN LYNN FOXPIN: 071-11-302ZONING: R-8WESLEY VANDER LUGT & STEPHANIE VANDER LUGTPIN: 071-11-301ZONING: R-8PRADYUMNA GOPALA LAKSHMIPURAMPIN: 071-11-208ZONING: R-8ROSS TYLER SHAFFERPIN: 071-11-207ZONING: R-8CHRISTOPHER JOEL VAN ROEKEL & HOLLY DYAN VANROEKELPIN: 071-11-206ZONING: R-8WILLIAM BRISLEY & WINFREE S. BRISLEYPIN: 071-11-205ZONING: R-8D. A. COLBERTPIN: 071-11-204ZONING: R-8GREGORY M. MOTLEYPIN: 071-11-213ZONING: I-1GREGORY M. MOTLEYPIN: 071-11-212ZONING: I-1GREGORY MOTLEY & TRACEY MOTLEYPIN: 071-11-211ZONING: I-1CATHERINE HUNTER, TRUSTEE OF GARDNER LAND TRUSTPIN: 071-11-110ZONING: R-8JBH DEVELOPMENT, LLCPIN: 071-11-112ZONING: UR-2 (CD)JUAN CARLOS REYES / JOHN BRICKLEY & JODI BRICKLEYPIN: 071-10-117 / 071-11-118ZONING: R-8CITYSIDE PROPERTIES, LLCPIN: 071-10-402ZONING: I-1CAROLINA URBAN PROPERTIES, LTDPIN: 071-10-403ZONING: I-1CAROLINA URBAN PROPERTIES, LTDPIN: 071-10-404ZONING: I-1CAROLINA URBAN PROPERTIES, LTDPIN: 071-10-405ZONING: I-1 / I-2SAVONA, LLCPIN: 071-11-551ZONING: I-2SAVONA, LLCPIN: 071-11-501ZONING: I-2COMMUNITY BUILDING INVESTMENTS, LLCPIN:071-07-214ZONING: MUDD-OMECKLENBURG COUNTYPIN: 071-11-416ZONING: I-2 / MUDD-OSEABOARD COAST LINE RAILROAD COMPANYPIN: 071-12-206ZONING: R-5MECKLENBURG COUNTYPIN: 071-12-205ZONING: R-5
1
2
3
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5
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21
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28
29
30
31
32
33
34
TREE SAVE AREA
01/03/2022
EROSION CONTROL
ENGINEERING
CDOT
URBAN FORESTRY
NOTE: SCHEDULE PRE-CONSTRUCTION MEETINGAT LEAST 48 HRS. PRIOR TO ANY LAND DISTURBING ACTIVITY USING THE ONLINE FORM FOUND AT http://charlottenc.gov/ld
NOTE: THIS PLAN APPROVAL DOES NOT INCLUDE COMMERCIAL ZONING. ALL BUILDING PERMITS AND ZONING APPROVALS CAN BE OBTAINED AT MECKLENBURG COUNTY CODE ENFORCEMENT. PLEASE CALL CTAC AT
704-314-CODE(2633) FOR MORE INFORMATION.
PCSO / DETENTION / DRAINAGE PLAN
TREE ORDINANCE
PLANNING
UMUDD / MUDD / PED / TOD
NOTE: THIS PLAN APPROVAL DOES NOT INCLUDE CHARLOTTE WATER. FOR MORE INFORMATION, PLEASE CALL 704-336-5499 OR
VISIT http://charlottewater.org
FINAL APPROVAL
PROJECT NUMBER:
2/3/2022
LDUMUDD-2021-00037
Jeu Moua
Peter Rodriguez
Vincent Condon
Alfred Oyoyo
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Appendix B
Reference Plan prepared by Alliance Architecture (September 21, 2021)

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REFER TO L130 FOR MATERIALS PLAN
REFER TO L140 FOR LAYOUT PLAN
REFER TO L150 FOR GRADING PLAN
REFER TO L160 FOR PLANTING PLAN
REFER TO L170 FOR IRRIGATION PLAN
REFER TO L180 FOR SOIL PLAN
REFER TO L131 FOR MATERIALS PLAN
REFER TO L132 FOR LOWER CONCOURSE MATERIALS
REFER TO L141 FOR LAYOUT PLAN
REFER TO L151 FOR GRADING PLAN
REFER TO L161 FOR PLANTING PLAN
REFER TO L170 FOR IRRIGATION PLAN
REFER TO L180 FOR SOIL PLAN
REFERENCE PLAN
Scale: 1" = 30'-0"1 0'15'30'60'
PATIO AREA BASE INFORMATION IS BASED ON FIELD VERIFICATION SKETCH
PROVIDED BY CONTRACTOR AND ALLIANCE ARCHITECTURE DATED 10.20.2021.
LANDSCAPE ARCHITECT IS NOT LIABLE FOR ANY ERRORS CAUSED BY
INACCURACIES FROM ANY BASE INFORMATION RECEIVED. CONTRACTOR TO
FIELD VERIFY AND CONFIRM ALL DIMENSIONS PRIOR TO PROCEEDING WITH
DEMOLITION AND CONSTRUCTION.
GENERAL NOTES - APPLY TO ALL LANDSCAPE SHEETS
1. LOCATION AND TOPOGRAPHICAL INFORMATION WAS
PROVIDED BY KIMLEY-HORN. SURFACE678 ASSUMES NO
RESPONSIBILITY FOR DESIGN OR CONSTRUCTION CHANGES
CAUSED BY INACCURACIES IN SURVEYS.
2. THE CONTRACTOR SHALL VISIT THE SITE AND BECOME
FAMILIAR WITH EXISTING SITE CONDITIONS PRIOR TO
CONSTRUCTION.
3. THE CONTRACTOR IS RESPONSIBLE FOR OBTAINING ALL
NECESSARY PERMITS AND FOR ADHERENCE TO
ORDINANCES, REGULATIONS, LAWS AND CODES HAVING
JURISDICTION OVER THE PROPERTY PRIOR TO
COMMENCING WORK.
4. ALL MATERIALS, CONSTRUCTION, AND WORKMANSHIP
SHALL MEET THE MECKLENBURG COUNTY, AND CITY OF
CHARLOTTE SPECIFICATIONS AND DESIGN STANDARDS.
5. EXISTING UTILITIES SHOWN ARE APPROXIMATE AND SHALL
BE VERIFIED IN THE FIELD PRIOR TO BEGINNING WORK.
CONTRACTOR SHALL CONTACT NC ONE CALL CENTER AT
1-800-632-4949 FOR LOCATION OF EXISTING UTILITIES PRIOR
TO BEGINNING CONSTRUCTION. THE CONTRACTOR SHALL
EXERCISE CAUTION WHEN WORKING AROUND EXISTING
UTILITIES TO REMAIN.
6. THE CONTRACTOR IS RESPONSIBLE FOR INSTALLING
SLEEVING FOR ELECTRIC, DRAINAGE, AND UTILITIES PRIOR TO
THE INSTALLATION OF COMPACTED SUB-GRADE, SUB-BASE
AND PAVEMENT AS NECESSARY. SLEEVES TO BE INSTALLED AT
A MINIMUM DEPTH BELOW GRADE AS PER LOCAL CODES.
7. ROADWAYS AND BUILDINGS MUST BE CAPABLE OF
SUPPORTING FIRE AND EMERGENCY APPARATUS DURING
CONSTRUCTION.
8. SEE CIVIL DRAWINGS FOR SEDIMENTATION AND EROSION
CONTROL MEASURES.
9. SEE CIVIL DRAWINGS FOR UTILITY AND UNDERGROUND
STORM DRAINAGE INFORMATION.
10. SEE CIVIL DRAWINGS FOR VEHICULAR SPECIFICATIONS
AND PLANS OUTSIDE OF SURFACE678'S LIMIT OF WORK
BOUNDARY.
11. SEE SURFACE678'S DRAWINGS FOR ALL HARDSCAPE AND
SOFTSCAPE WITHIN LIMIT OF WORK LINE.
SHEET TITLE:
SHEET NUMBER:5/31/2014 6:30:41 PMCOPYRIGHT ALLIANCE ARCHITECTURE, PC, 2014ABCDEFGHJK123456789101112131415
DATE: 09.21.2021
DRAWN BY: LH, YJ, YZ
CHECKED BY: YJFOR CONSTRUCTION SET - 4.8.2022REVISIONS
NO.DESCRIPTION DATE
ISSUES
DESCRIPTION DATE
SEAL
528 SOUTH TURNER AVE. CHARLOTTE, NC
PROJECT ADDRESS:SAVONA MILL RENOVATION
ARCHITECT:
ALLIANCE ARCHITECTURE, PC
208 RIGSBEE AVE.
DURHAM, NC 27701
TEL: [phone]
CON: JOHN WARASILA, AIA
CON: TEERA GAMES,AIA
CON: SARAH WILHELM
OWNER:
PORTMAN HOLDINGS
303 PEACHTREE CENTER AVE NE #575
ATLANTA, GA 30303
TEL: [phone]
CON: REID SCOTT
CON: JOHN FARMER
MEP ENGINEER:
BARRETT, WOODYARD & ASSOCIATES, INC.
2301 REXWOOD DRIVE #108
RALEIGH, NC 27607
TEL: [phone]
CON: CHAD VICKERY, PE,
CON: JASON MACCALL, PE
STRUCTURAL ENGINEER:
MORRISON ENGINEERS, PLLC
7701 CHAPEL HILL ROAD
CARY, NC 27513
TEL: [phone]
CON: JOHN STEVENSON, PE
CON: AARON MARX, PE
1617
SCHEMATIC DESIGN 6.30.21
DESIGN DEVELOPMENT 8.6.21
FOR PERMIT/ CONSTRUCTION SET 9.21.21
SEAL
GENERAL CONTRACTOR:
EDIFICE
4111 SOUTH BLVD.
CHARLOTTE, NC 28209
TEL: [phone]
CON: MATT TOFFEY
CON: STEVE PIERMATTEI
208 Rigsbee Avenue
Durham, North Carolina 27701
Tel [phone]
LANDSCAPE ARCHITECT:
SURFACE 678
215 MORRIS STREET, SUITE 150
DURHAM, NC 27701
TEL: [phone]
CON: WALT HAVENER
CON: SWATI KHIMESRA
CON: YINGLIN JI
9.17.21 9.17.21
90% GMP SET 10.18.21
04.08.22FCS
L100
REFERENCE PLAN
LD LD LD LIMIT OF WORK BY SURFACE678
NOTES FOR EXISTING TREE PRESERVATION ON SITE:
It was noticed that several of the existing trees tagged to be
preserved on site are already being impacted by the ongoing
construction/demolition activity. Several trees are showing
signs of distress and are leaning over due to grade impacts
with the root zones. Due to the impacts already made to the
trees, Surface 678 does not guarantee the viability of the
tagged trees and recommends the following risk mitigation
steps immediately:
1.It is recommended that metal tree protection fencing be
installed immediatedly to protect the trees and their critical
root zones.
2.It is highly recommended that the Owner enlist the
services of a professional certififed arborist to review tree
health and condition to make recommendations on tree
viability through the construction process.
Arborist report to include recommendations for preservation
of trees and care during the construction period and/or
recommendations for removal. Additional
bracing/stabilization methods needed to protect tress from
falling may be required.

Appendix C
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

11/20/2023
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Revised Lab Report Number: 23-265-0002 Client Project Description: POR-001
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/21/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 93
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/29/202440750State ProgramAlabama
02/07/202488-0650State ProgramArkansas
06/30/20242904State ProgramCalifornia
06/30/2024E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202404015State ProgramGeorgia
10/31/2024200078State Program - NELAPIllinois
06/30/202480215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202404015State Program - NELAPLouisiana
11/14/2025MSState ProgramMississippi
07/31/202447701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202468-03195State Program - NELAPPennsylvania
06/30/202484002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2024T104704180State Program - NELAPTexas
06/30/202400106State ProgramVirginia
09/14/2024460181State Program - NELAPVirginia
Page 1 of 1 00016/23-265-0002
Page 2 of 93
Report Number:
Sample Summary Table
Client Project Description:
23-265-0002
POR-001
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
09/21/2023 13:05Solids 95973 FG-1 09/21/2023 15:30
09/21/2023 13:05Solids 95973 FG-1 09/21/2023 15:30 SW-7199 WP MTN -
09/21/2023 13:05Solids 95973 FG-1 09/21/2023 15:30 6020B WP MTN -
09/21/2023 15:00Solids 95974 FG-2 09/21/2023 15:30
09/21/2023 15:00Solids 95974 FG-2 09/21/2023 15:30 SW-7199 WP MTN -
09/21/2023 15:00Solids 95974 FG-2 09/21/2023 15:30 6020B WP MTN -
09/21/2023 14:20Solids 95975 FG-3 09/21/2023 15:30
09/21/2023 14:20Solids 95975 FG-3 09/21/2023 15:30 SW-7199 WP MTN -
09/21/2023 14:20Solids 95975 FG-3 09/21/2023 15:30 6020B WP MTN -
09/21/2023 15:10Solids 95976 FG-4 09/21/2023 15:30
09/21/2023 15:10Solids 95976 FG-4 09/21/2023 15:30 SW-7199 WP MTN -
09/21/2023 15:10Solids 95976 FG-4 09/21/2023 15:30 6020B WP MTN -
09/21/2023 11:30Solids 95977 FG-5 09/21/2023 15:30
09/21/2023 11:30Solids 95977 FG-5 09/21/2023 15:30 SW-7199 WP MTN -
09/21/2023 11:30Solids 95977 FG-5 09/21/2023 15:30 6020B WP MTN -
09/21/2023 09:15Solids 95978 FG-6 09/21/2023 15:30
09/21/2023 09:15Solids 95978 FG-6 09/21/2023 15:30 SW-7199 WP MTN -
09/21/2023 09:15Solids 95978 FG-6 09/21/2023 15:30 6020B WP MTN -
09/21/2023Solids 95979 FG-DUP 09/21/2023 15:30
09/21/2023Solids 95979 FG-DUP 09/21/2023 15:30 SW-7199 WP MTN -
09/21/2023Solids 95979 FG-DUP 09/21/2023 15:30 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 93
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-265-0002
Report Limit
Project:POR-001
V 95973FG-1
6.92 09/29/2023 15:106020BArsenicmg/Kg - dry 0.0926
80.9 09/29/2023 15:106020BBariummg/Kg - dry 0.046
J0.100 09/29/2023 15:106020BCadmiummg/Kg - dry 0.0281
23.4 09/29/2023 15:106020BChromiummg/Kg - dry 0.125
16.9 09/29/2023 15:106020BLeadmg/Kg - dry 0.0335
0.615 09/29/2023 15:106020BSeleniummg/Kg - dry 0.111
J0.0331 09/29/2023 15:106020BSilvermg/Kg - dry 0.0073
J0.0181 09/26/2023 11:107471BMercury (Total)mg/Kg - dry 0.0130
0.071 09/22/2023 19:138260DAcetonemg/Kg - dry 0.002
J0.003 09/22/2023 19:138260Dn-Hexane mg/Kg - dry 0.0007
J0.004 09/22/2023 19:138260DMethylene Chloride mg/Kg - dry 0.001
J0.144 09/26/2023 19:288270EAcenaphthenemg/Kg - dry 0.125
J0.438 09/26/2023 19:288270EAnthracenemg/Kg - dry 0.154
0.750 09/26/2023 19:288270EBenzo(a)anthracene mg/Kg - dry 0.150
0.740 09/26/2023 19:288270EBenzo(a)pyrene mg/Kg - dry 0.159
1.00 09/26/2023 19:288270EBenzo(b)fluoranthene mg/Kg - dry 0.158
J0.499 09/26/2023 19:288270EBenzo(g,h,i)perylene mg/Kg - dry 0.147
J0.360 09/26/2023 19:288270EBenzo(k)fluoranthene mg/Kg - dry 0.148
0.734 09/26/2023 19:288270EChrysenemg/Kg - dry 0.153
J0.159 09/26/2023 19:288270EDibenzofuranmg/Kg - dry 0.128
1.64 09/26/2023 19:288270EFluoranthenemg/Kg - dry 0.133
J0.510 09/26/2023 19:288270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.193
J0.212 09/26/2023 19:288270E1-Methylnaphthalene mg/Kg - dry 0.114
J0.286 09/26/2023 19:288270E2-Methylnaphthalene mg/Kg - dry 0.108
J0.264 09/26/2023 19:288270ENaphthalenemg/Kg - dry 0.156
1.63 09/26/2023 19:288270EPhenanthrenemg/Kg - dry 0.225
1.54 09/26/2023 19:288270EPyrenemg/Kg - dry 0.145
0.369 10/03/2023 13:46SW-7199 Chromium, Hexavalent mg/Kg - dry 0.152
7.72 09/22/2023 11:55SW-DRYWT Moisture %
V 95974FG-2
4.05 09/29/2023 15:146020BArsenicmg/Kg - dry 0.0916
73.0 09/29/2023 15:146020BBariummg/Kg - dry 0.045
J0.147 09/29/2023 15:146020BCadmiummg/Kg - dry 0.0278
33.7 09/29/2023 15:146020BChromiummg/Kg - dry 0.124
24.9 09/29/2023 15:146020BLeadmg/Kg - dry 0.0332
0.628 09/29/2023 15:146020BSeleniummg/Kg - dry 0.110
Page 4 of 93
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-265-0002
Report Limit
Project:POR-001
V 95974FG-2
J0.0490 09/29/2023 15:146020BSilvermg/Kg - dry 0.0072
0.115 09/26/2023 11:137471BMercury (Total)mg/Kg - dry 0.0129
0.052 09/22/2023 19:408260DAcetonemg/Kg - dry 0.002
J0.003 09/22/2023 19:408260Dn-Hexane mg/Kg - dry 0.0007
J0.002 09/22/2023 19:408260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.005 09/22/2023 19:408260DMethylene Chloride mg/Kg - dry 0.001
J0.217 09/26/2023 19:518270EAcenaphthenemg/Kg - dry 0.124
J0.388 09/26/2023 19:518270EAnthracenemg/Kg - dry 0.153
1.00 09/26/2023 19:518270EBenzo(a)anthracene mg/Kg - dry 0.149
0.997 09/26/2023 19:518270EBenzo(a)pyrene mg/Kg - dry 0.157
1.33 09/26/2023 19:518270EBenzo(b)fluoranthene mg/Kg - dry 0.156
J0.615 09/26/2023 19:518270EBenzo(g,h,i)perylene mg/Kg - dry 0.145
J0.381 09/26/2023 19:518270EBenzo(k)fluoranthene mg/Kg - dry 0.146
0.965 09/26/2023 19:518270EChrysenemg/Kg - dry 0.152
1.99 09/26/2023 19:518270EFluoranthenemg/Kg - dry 0.131
J0.156 09/26/2023 19:518270EFluorenemg/Kg - dry 0.137
J0.670 09/26/2023 19:518270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.191
1.55 09/26/2023 19:518270EPhenanthrenemg/Kg - dry 0.223
1.80 09/26/2023 19:518270EPyrenemg/Kg - dry 0.143
0.612 10/03/2023 13:57SW-7199 Chromium, Hexavalent mg/Kg - dry 0.151
6.74 09/22/2023 11:55SW-DRYWT Moisture %
V 95975FG-3
4.71 09/29/2023 15:186020BArsenicmg/Kg - dry 0.106
85.8 09/29/2023 15:186020BBariummg/Kg - dry 0.053
J0.268 09/29/2023 15:186020BCadmiummg/Kg - dry 0.0322
92.8 09/29/2023 15:186020BChromiummg/Kg - dry 0.144
82.2 09/29/2023 15:186020BLeadmg/Kg - dry 0.0385
0.904 09/29/2023 15:186020BSeleniummg/Kg - dry 0.127
J0.0559 09/29/2023 15:186020BSilvermg/Kg - dry 0.0083
0.0920 09/28/2023 14:177471BMercury (Total)mg/Kg - dry 0.0149
0.091 09/22/2023 20:088260DAcetonemg/Kg - dry 0.002
J0.001 09/22/2023 20:088260DCarbon Disulfide mg/Kg - dry 0.0008
J0.003 09/22/2023 20:088260Dn-Hexane mg/Kg - dry 0.0008
J0.010 09/22/2023 20:088260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.005 09/22/2023 20:088260DMethylene Chloride mg/Kg - dry 0.001
J0.716 09/26/2023 20:588270EAnthracenemg/Kg - dry 0.710
Page 5 of 93
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-265-0002
Report Limit
Project:POR-001
V 95975FG-3
J2.22 09/26/2023 20:588270EBenzo(a)anthracene mg/Kg - dry 0.690
J2.25 09/26/2023 20:588270EBenzo(a)pyrene mg/Kg - dry 0.730
J2.86 09/26/2023 20:588270EBenzo(b)fluoranthene mg/Kg - dry 0.725
J1.38 09/26/2023 20:588270EBenzo(g,h,i)perylene mg/Kg - dry 0.675
J1.00 09/26/2023 20:588270EBenzo(k)fluoranthene mg/Kg - dry 0.680
J2.14 09/26/2023 20:588270EChrysenemg/Kg - dry 0.705
4.25 09/26/2023 20:588270EFluoranthenemg/Kg - dry 0.611
J1.47 09/26/2023 20:588270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.889
J2.80 09/26/2023 20:588270EPhenanthrenemg/Kg - dry 1.03
3.98 09/26/2023 20:588270EPyrenemg/Kg - dry 0.665
0.411 10/03/2023 14:08SW-7199 Chromium, Hexavalent mg/Kg - dry 0.175
19.5 09/25/2023 10:40SW-DRYWT Moisture %
V 95976FG-4
1.91 09/29/2023 15:226020BArsenicmg/Kg - dry 0.0970
61.1 09/29/2023 15:226020BBariummg/Kg - dry 0.048
J0.0552 09/29/2023 15:226020BCadmiummg/Kg - dry 0.0295
24.1 09/29/2023 15:226020BChromiummg/Kg - dry 0.131
6.40 09/29/2023 15:226020BLeadmg/Kg - dry 0.0351
0.572 09/29/2023 15:226020BSeleniummg/Kg - dry 0.116
J0.0219 09/29/2023 15:226020BSilvermg/Kg - dry 0.0076
J0.0279 09/28/2023 14:197471BMercury (Total)mg/Kg - dry 0.0136
J0.006 09/22/2023 20:358260DAcetonemg/Kg - dry 0.002
J0.004 09/22/2023 20:358260Dn-Hexane mg/Kg - dry 0.0007
J0.005 09/22/2023 20:358260DMethylene Chloride mg/Kg - dry 0.001
J0.169 09/26/2023 20:138270EAnthracenemg/Kg - dry 0.162
J0.464 09/26/2023 20:138270EBenzo(a)anthracene mg/Kg - dry 0.157
J0.471 09/26/2023 20:138270EBenzo(a)pyrene mg/Kg - dry 0.166
J0.547 09/26/2023 20:138270EBenzo(b)fluoranthene mg/Kg - dry 0.165
J0.300 09/26/2023 20:138270EBenzo(g,h,i)perylene mg/Kg - dry 0.154
J0.181 09/26/2023 20:138270EBenzo(k)fluoranthene mg/Kg - dry 0.155
J0.442 09/26/2023 20:138270EChrysenemg/Kg - dry 0.161
J0.737 09/26/2023 20:138270EFluoranthenemg/Kg - dry 0.139
J0.301 09/26/2023 20:138270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.203
J0.130 09/26/2023 20:138270E1-Methylnaphthalene mg/Kg - dry 0.120
J0.120 09/26/2023 20:138270E2-Methylnaphthalene mg/Kg - dry 0.113
J0.699 09/26/2023 20:138270EPhenanthrenemg/Kg - dry 0.236
Page 6 of 93
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-265-0002
Report Limit
Project:POR-001
V 95976FG-4
0.891 09/26/2023 20:138270EPyrenemg/Kg - dry 0.152
0.389 10/03/2023 12:52SW-7199 Chromium, Hexavalent mg/Kg - dry 0.160
11.9 09/25/2023 10:40SW-DRYWT Moisture %
V 95977FG-5
1.77 09/29/2023 15:276020BArsenicmg/Kg - dry 0.104
110 09/29/2023 15:276020BBariummg/Kg - dry 0.051
J0.0639 09/29/2023 15:276020BCadmiummg/Kg - dry 0.0315
24.0 09/29/2023 15:276020BChromiummg/Kg - dry 0.140
11.3 09/29/2023 15:276020BLeadmg/Kg - dry 0.0376
0.910 09/29/2023 15:276020BSeleniummg/Kg - dry 0.125
J0.0300 09/29/2023 15:276020BSilvermg/Kg - dry 0.0081
0.0421 09/28/2023 14:227471BMercury (Total)mg/Kg - dry 0.0146
J0.010 09/25/2023 17:478260DAcetonemg/Kg - dry 0.002
J0.717 09/26/2023 21:218270EBenzo(b)fluoranthene mg/Kg - dry 0.708
J1.02 09/26/2023 21:218270EFluoranthenemg/Kg - dry 0.597
J0.956 09/26/2023 21:218270EPyrenemg/Kg - dry 0.650
0.707 10/03/2023 14:41SW-7199 Chromium, Hexavalent mg/Kg - dry 0.171
17.6 09/25/2023 10:40SW-DRYWT Moisture %
V 95978FG-6
1.88 09/29/2023 15:316020BArsenicmg/Kg - dry 0.104
102 09/29/2023 15:316020BBariummg/Kg - dry 0.051
J0.135 09/29/2023 15:316020BCadmiummg/Kg - dry 0.0315
30.5 09/29/2023 15:316020BChromiummg/Kg - dry 0.140
23.2 09/29/2023 15:316020BLeadmg/Kg - dry 0.0375
0.683 09/29/2023 15:316020BSeleniummg/Kg - dry 0.124
J0.0859 09/29/2023 15:316020BSilvermg/Kg - dry 0.0081
0.156 09/28/2023 14:247471BMercury (Total)mg/Kg - dry 0.0145
0.034 09/22/2023 21:298260DAcetonemg/Kg - dry 0.002
J0.003 09/22/2023 21:298260Dn-Hexane mg/Kg - dry 0.0008
J0.004 09/22/2023 21:298260DMethylene Chloride mg/Kg - dry 0.001
J0.772 09/26/2023 21:438270EBenzo(b)fluoranthene mg/Kg - dry 0.707
J1.07 09/26/2023 21:438270EFluoranthenemg/Kg - dry 0.596
J1.06 09/26/2023 21:438270EPyrenemg/Kg - dry 0.649
0.294 10/03/2023 14:52SW-7199 Chromium, Hexavalent mg/Kg - dry 0.174
17.5 09/25/2023 10:40SW-DRYWT Moisture %
Page 7 of 93
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-265-0002
Report Limit
Project:POR-001
V 95979FG-DUP
5.28 09/29/2023 15:356020BArsenicmg/Kg - dry 0.0916
81.6 09/29/2023 15:356020BBariummg/Kg - dry 0.045
J0.0863 09/29/2023 15:356020BCadmiummg/Kg - dry 0.0278
25.0 09/29/2023 15:356020BChromiummg/Kg - dry 0.124
15.4 09/29/2023 15:356020BLeadmg/Kg - dry 0.0332
0.706 09/29/2023 15:356020BSeleniummg/Kg - dry 0.110
J0.0312 09/29/2023 15:356020BSilvermg/Kg - dry 0.0072
0.124 09/28/2023 14:277471BMercury (Total)mg/Kg - dry 0.0129
0.064 09/22/2023 21:568260DAcetonemg/Kg - dry 0.002
J0.005 09/22/2023 21:568260Dn-Hexane mg/Kg - dry 0.0007
J0.006 09/22/2023 21:568260DMethylene Chloride mg/Kg - dry 0.001
J0.336 09/26/2023 20:368270EAnthracenemg/Kg - dry 0.153
J0.669 09/26/2023 20:368270EBenzo(a)anthracene mg/Kg - dry 0.149
J0.668 09/26/2023 20:368270EBenzo(a)pyrene mg/Kg - dry 0.157
0.969 09/26/2023 20:368270EBenzo(b)fluoranthene mg/Kg - dry 0.156
J0.468 09/26/2023 20:368270EBenzo(g,h,i)perylene mg/Kg - dry 0.145
J0.265 09/26/2023 20:368270EBenzo(k)fluoranthene mg/Kg - dry 0.146
J0.651 09/26/2023 20:368270EChrysenemg/Kg - dry 0.152
1.38 09/26/2023 20:368270EFluoranthenemg/Kg - dry 0.131
J0.489 09/26/2023 20:368270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.191
J0.117 09/26/2023 20:368270E1-Methylnaphthalene mg/Kg - dry 0.113
J0.160 09/26/2023 20:368270E2-Methylnaphthalene mg/Kg - dry 0.107
1.14 09/26/2023 20:368270EPhenanthrenemg/Kg - dry 0.223
1.31 09/26/2023 20:368270EPyrenemg/Kg - dry 0.143
0.408 10/03/2023 15:03SW-7199 Chromium, Hexavalent mg/Kg - dry 0.153
6.76 09/25/2023 10:40SW-DRYWT Moisture %
Page 8 of 93

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: POR-001 Lab Report Number: 23-265-0002
Date: 11/20/2023
Report Comments Revised Report: Revision 1. The case narrative has been update.
Metals Analyses Method 6020B
Sample 95419 Analyte: Arsenic
QC Batch No: L707915/L707346 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95419
Analyte: Barium QC Batch No: L707915/L707346
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 95419
Analyte: Chromium QC Batch No: L707915/L707346 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 95419
Analyte: Lead QC Batch No: L707915/L707346
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Hexavalent Chromium by Ion Chromatography Method SW-7199 Sample 95976 (FG-4) Analyte: Hexavalent Chromium
QC Batch No: L708430/L707678 Matrix Spike Recovery Low: A measure of the sample pH and its oxidation reduction potential (ORP) indicate that the sample has reducing qualities which may not allow for the presence of Hexavalent Chromium. Solids Total Mercury Analysis - CVAA Method 7471B Sample 95748
Analyte: Mercury QC Batch No: V38344/V38283 The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control acceptance ranges. Matrix interference is suspected Semivolatile Organic Compounds - GC/MS Method 8270E
Page 9 of 93

Analyte: Aniline
QC Batch No: V38347/V38274 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Benzoic Acid
QC Batch No: V38347/V38274 Analyte was flagged for 0% recovery in the LCS and LCSD due to the result being below the MQL. The actual
result was 13.979 and 14.565 respectively, which calculates to a recovery of 27.958% and 29.13% which is within the acceptable recovery range.

Page 10 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-1
95973 Matrix:
9/21/2023 13:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
7.72 %Moisture 1 09/22/23 11:55 SW-DRYWTCNC
0.369 mg/Kg - dry 0.152 0.216Chromium, Hexavalent 1 10/03/23 13:46 SW-7199NFP
6.92 mg/Kg - dry 0.0926 0.271Arsenic 5 09/29/23 15:10 6020BCPW
80.9 mg/Kg - dry 0.046 0.270Barium 5 09/29/23 15:10 6020BCPW
0.100 J mg/Kg - dry 0.0281 0.271Cadmium 5 09/29/23 15:10 6020BCPW
23.4 mg/Kg - dry 0.125 0.270
Chromium 5 09/29/23 15:10 6020BCPW
16.9 mg/Kg - dry 0.0335 0.271Lead 5 09/29/23 15:10 6020BCPW
0.0181 J mg/Kg - dry 0.0130 0.0325Mercury (Total)1 09/26/23 11:10 7471BJKC
0.615 mg/Kg - dry 0.111 0.270Selenium 5 09/29/23 15:10 6020BCPW
0.0331 J mg/Kg - dry 0.0073 0.271Silver 5 09/29/23 15:10 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-1
95973 Matrix:
9/21/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.071 mg/Kg - dry 0.002 0.021Acetone 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.021
Acrolein 1 09/22/23 19:13 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 09/22/23 19:13 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 09/22/23 19:13 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 09/22/23 19:13 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010
Bromomethane 1 09/22/23 19:13 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 09/22/23 19:13 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 09/22/23 19:13 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 09/22/23 19:13 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 09/22/23 19:13 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 09/22/23 19:13 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 09/22/23 19:13 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 09/22/23 19:13 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 09/22/23 19:13 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 09/22/23 19:13 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 09/22/23 19:13 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 09/22/23 19:13 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-1
95973 Matrix:
9/21/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 09/22/23 19:13 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,2-Dibromoethane 1 09/22/23 19:13 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 09/22/23 19:13 V38309TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 09/22/23 19:13 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 09/22/23 19:13 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 09/22/23 19:13 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 09/22/23 19:13 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 09/22/23 19:13 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 09/22/23 19:13 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 09/22/23 19:13 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 09/22/23 19:13 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 09/22/23 19:13 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 09/22/23 19:13 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 09/22/23 19:13 V38309TBL
<0.015 mg/Kg - dry 0.015 0.270Ethanol 1 09/22/23 19:13 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 09/22/23 19:13 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.054Ethyl Tertiary Butyl Ether (ETBE)1 09/22/23 19:13 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.010Hexachlorobutadiene 1 09/22/23 19:13 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-1
95973 Matrix:
9/21/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.003 J mg/Kg - dry 0.0007 0.010n-Hexane 1 09/22/23 19:13 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.021
2-Hexanone 1 09/22/23 19:13 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 09/22/23 19:13 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 09/22/23 19:13 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 09/22/23 19:13 V38309TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 09/22/23 19:13 V38309TBL
0.004 J mg/Kg - dry 0.001 0.010Methylene Chloride 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010
Naphthalene 1 09/22/23 19:13 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 09/22/23 19:13 V38309TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 09/22/23 19:13 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 09/22/23 19:13 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 09/22/23 19:13 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 09/22/23 19:13 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 09/22/23 19:13 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 09/22/23 19:13 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.005Trichloroethene 1 09/22/23 19:13 V38309TBL
<0.002 mg/Kg - dry 0.002 0.010Trichlorofluoromethane 1 09/22/23 19:13 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 09/22/23 19:13 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-1
95973 Matrix:
9/21/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 09/22/23 19:13 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 09/22/23 19:13 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 09/22/23 19:13 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 09/22/23 19:13 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 09/22/23 19:13 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 09/22/23 19:13 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 09/22/23 19:13 V38309
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%09/22/23 19:131 TBL V38309
Surrogate: Dibromofluoromethane 106 Limits: 84-123%09/22/23 19:131 TBL V38309
Surrogate: Toluene-d8 98.0 Limits: 76-129%09/22/23 19:131 TBL V38309
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
0.144 J mg/Kg - dry 0.125 0.715Acenaphthene 1 09/26/23 19:28 V38347AMP
<0.113 mg/Kg - dry 0.113 0.715Acenaphthylene 1 09/26/23 19:28 V38347AMP
<0.164 mg/Kg - dry 0.164 0.715Aniline 1 09/26/23 19:28 V38347AMP
0.438 J mg/Kg - dry 0.154 0.715Anthracene 1 09/26/23 19:28 V38347AMP
0.750 mg/Kg - dry 0.150 0.715
Benzo(a)anthracene 1 09/26/23 19:28 V38347AMP
0.740 mg/Kg - dry 0.159 0.715Benzo(a)pyrene 1 09/26/23 19:28 V38347AMP
1.00 mg/Kg - dry 0.158 0.715Benzo(b)fluoranthene 1 09/26/23 19:28 V38347AMP
0.499 J mg/Kg - dry 0.147 0.715Benzo(g,h,i)perylene 1 09/26/23 19:28 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-1
95973 Matrix:
9/21/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
0.360 J mg/Kg - dry 0.148 0.715Benzo(k)fluoranthene 1 09/26/23 19:28 V38347AMP
<0.628 mg/Kg - dry 0.628 2.17
Benzoic Acid 1 09/26/23 19:28 V38347AMP
<0.113 mg/Kg - dry 0.113 0.715Benzyl alcohol 1 09/26/23 19:28 V38347AMP
<0.127 mg/Kg - dry 0.127 0.715Bis(2-Chloroethoxy)methane 1 09/26/23 19:28 V38347AMP
<0.115 mg/Kg - dry 0.115 0.715Bis(2-Chloroethyl)ether 1 09/26/23 19:28 V38347AMP
<0.147 mg/Kg - dry 0.147 0.357Bis(2-Chloroisopropyl)ether 1 09/26/23 19:28 V38347AMP
<0.130 mg/Kg - dry 0.130 0.715Bis(2-ethylhexyl)phthalate 1 09/26/23 19:28 V38347AMP
<0.118 mg/Kg - dry 0.118 0.7154-Bromophenyl phenyl ether 1 09/26/23 19:28 V38347AMP
<0.122 mg/Kg - dry 0.122 0.357
Butyl benzyl phthalate 1 09/26/23 19:28 V38347AMP
<0.100 mg/Kg - dry 0.100 0.7154-Chloro-3-methylphenol 1 09/26/23 19:28 V38347AMP
<0.121 mg/Kg - dry 0.121 0.3574-Chloroaniline 1 09/26/23 19:28 V38347AMP
<0.125 mg/Kg - dry 0.125 0.7152-Chloronaphthalene 1 09/26/23 19:28 V38347AMP
<0.106 mg/Kg - dry 0.106 0.7152-Chlorophenol 1 09/26/23 19:28 V38347AMP
<0.136 mg/Kg - dry 0.136 1.084-Chlorophenyl phenyl ether 1 09/26/23 19:28 V38347AMP
0.734 mg/Kg - dry 0.153 0.715Chrysene 1 09/26/23 19:28 V38347AMP
<0.249 mg/Kg - dry 0.249 0.715Dibenz(a,h)anthracene 1 09/26/23 19:28 V38347AMP
0.159 J mg/Kg - dry 0.128 0.715Dibenzofuran 1 09/26/23 19:28 V38347AMP
<0.102 mg/Kg - dry 0.102 0.7151,2-Dichlorobenzene 1 09/26/23 19:28 V38347AMP
<0.105 mg/Kg - dry 0.105 0.7151,3-Dichlorobenzene 1 09/26/23 19:28 V38347AMP
<0.105 mg/Kg - dry 0.105 0.3571,4-Dichlorobenzene 1 09/26/23 19:28 V38347AMP
<0.159 mg/Kg - dry 0.159 0.7153,3'-Dichlorobenzidine 1 09/26/23 19:28 V38347AMP
<0.103 mg/Kg - dry 0.103 0.7152,4-Dichlorophenol 1 09/26/23 19:28 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-1
95973 Matrix:
9/21/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.195 mg/Kg - dry 0.195 0.715Diethyl phthalate 1 09/26/23 19:28 V38347AMP
<0.188 mg/Kg - dry 0.188 0.715
Dimethyl phthalate 1 09/26/23 19:28 V38347AMP
<0.117 mg/Kg - dry 0.117 0.3572,4-Dimethylphenol 1 09/26/23 19:28 V38347AMP
<0.115 mg/Kg - dry 0.115 0.715Di-n-butyl phthalate 1 09/26/23 19:28 V38347AMP
<0.260 mg/Kg - dry 0.260 1.634,6-Dinitro-2-methylphenol 1 09/26/23 19:28 V38347AMP
<0.563 mg/Kg - dry 0.563 1.632,4-Dinitrophenol 1 09/26/23 19:28 V38347AMP
<0.104 mg/Kg - dry 0.104 0.7152,4-Dinitrotoluene 1 09/26/23 19:28 V38347AMP
<0.117 mg/Kg - dry 0.117 0.7152,6-Dinitrotoluene 1 09/26/23 19:28 V38347AMP
<0.154 mg/Kg - dry 0.154 0.357
Di-n-Octyl Phthalate 1 09/26/23 19:28 V38347AMP
1.64 mg/Kg - dry 0.133 0.715Fluoranthene 1 09/26/23 19:28 V38347AMP
<0.138 mg/Kg - dry 0.138 0.715Fluorene 1 09/26/23 19:28 V38347AMP
<0.114 mg/Kg - dry 0.114 0.715Hexachlorobenzene 1 09/26/23 19:28 V38347AMP
<0.105 mg/Kg - dry 0.105 0.715Hexachlorobutadiene 1 09/26/23 19:28 V38347AMP
<0.170 mg/Kg - dry 0.170 0.715Hexachlorocyclopentadiene 1 09/26/23 19:28 V38347AMP
<0.085 mg/Kg - dry 0.085 0.715Hexachloroethane 1 09/26/23 19:28 V38347AMP
0.510 J mg/Kg - dry 0.193 0.715Indeno(1,2,3-cd)pyrene 1 09/26/23 19:28 V38347AMP
<0.206 mg/Kg - dry 0.206 0.715Isophorone 1 09/26/23 19:28 V38347AMP
0.212 J mg/Kg - dry 0.114 0.7151-Methylnaphthalene 1 09/26/23 19:28 V38347AMP
0.286 J mg/Kg - dry 0.108 0.7152-Methylnaphthalene 1 09/26/23 19:28 V38347AMP
<0.105 mg/Kg - dry 0.105 0.7152-Methylphenol 1 09/26/23 19:28 V38347AMP
<0.092 mg/Kg - dry 0.092 0.7153&4 Methylphenol 1 09/26/23 19:28 V38347AMP
0.264 J mg/Kg - dry 0.156 0.715Naphthalene 1 09/26/23 19:28 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-1
95973 Matrix:
9/21/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.104 mg/Kg - dry 0.104 0.7152-Nitroaniline 1 09/26/23 19:28 V38347AMP
<0.130 mg/Kg - dry 0.130 0.715
3-Nitroaniline 1 09/26/23 19:28 V38347AMP
<0.101 mg/Kg - dry 0.101 0.3574-Nitroaniline 1 09/26/23 19:28 V38347AMP
<0.125 mg/Kg - dry 0.125 0.357Nitrobenzene 1 09/26/23 19:28 V38347AMP
<0.096 mg/Kg - dry 0.096 0.7152-Nitrophenol 1 09/26/23 19:28 V38347AMP
<0.126 mg/Kg - dry 0.126 0.7154-Nitrophenol 1 09/26/23 19:28 V38347AMP
<0.285 mg/Kg - dry 0.285 0.715N-Nitrosodimethylamine 1 09/26/23 19:28 V38347AMP
<0.196 mg/Kg - dry 0.196 0.715N-Nitrosodiphenylamine 1 09/26/23 19:28 V38347AMP
<0.127 mg/Kg - dry 0.127 0.715
N-Nitroso-di-n-propylamine 1 09/26/23 19:28 V38347AMP
<0.376 mg/Kg - dry 0.376 1.08Pentachlorophenol 1 09/26/23 19:28 V38347AMP
1.63 mg/Kg - dry 0.225 0.715Phenanthrene 1 09/26/23 19:28 V38347AMP
<0.121 mg/Kg - dry 0.121 0.715Phenol 1 09/26/23 19:28 V38347AMP
1.54 mg/Kg - dry 0.145 0.715Pyrene 1 09/26/23 19:28 V38347AMP
<0.085 mg/Kg - dry 0.085 0.357Pyridine 1 09/26/23 19:28 V38347AMP
<0.115 mg/Kg - dry 0.115 0.7151,2,4-Trichlorobenzene 1 09/26/23 19:28 V38347AMP
<0.104 mg/Kg - dry 0.104 0.7152,4,5-Trichlorophenol 1 09/26/23 19:28 V38347AMP
<0.104 mg/Kg - dry 0.104 0.7152,4,6-Trichlorophenol 1 09/26/23 19:28 V38347AMP
8270ESurrogate: Phenol-d5 61.6 Limits: 34-121%09/26/23 19:281 AMP
Surrogate: 2-Fluorobiphenyl 75.4 Limits: 44-115%09/26/23 19:281 AMP V38347
Surrogate: 2-Fluorophenol 64.9 Limits: 35-115%09/26/23 19:281 AMP V38347
Surrogate: Nitrobenzene-d5 70.1 Limits: 37-122%09/26/23 19:281 AMP V38347
Surrogate: 4-Terphenyl-d14 82.6 Limits: 54-127%09/26/23 19:281 AMP V38347
Surrogate: 2,4,6-Tribromophenol 68.8 Limits: 39-132%09/26/23 19:281 AMP V38347
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-2
95974 Matrix:
9/21/2023 15:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
6.74 %Moisture 1 09/22/23 11:55 SW-DRYWTCNC
0.612 mg/Kg - dry 0.151 0.214Chromium, Hexavalent 1 10/03/23 13:57 SW-7199NFP
4.05 mg/Kg - dry 0.0916 0.268Arsenic 5 09/29/23 15:14 6020BCPW
73.0 mg/Kg - dry 0.045 0.268Barium 5 09/29/23 15:14 6020BCPW
0.147 J mg/Kg - dry 0.0278 0.268Cadmium 5 09/29/23 15:14 6020BCPW
33.7 mg/Kg - dry 0.124 0.268
Chromium 5 09/29/23 15:14 6020BCPW
24.9 mg/Kg - dry 0.0332 0.268Lead 5 09/29/23 15:14 6020BCPW
0.115 mg/Kg - dry 0.0129 0.0322Mercury (Total)1 09/26/23 11:13 7471BJKC
0.628 mg/Kg - dry 0.110 0.268Selenium 5 09/29/23 15:14 6020BCPW
0.0490 J mg/Kg - dry 0.0072 0.268Silver 5 09/29/23 15:14 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-2
95974 Matrix:
9/21/2023 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.052 mg/Kg - dry 0.002 0.021Acetone 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.021
Acrolein 1 09/22/23 19:40 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 09/22/23 19:40 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 09/22/23 19:40 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 09/22/23 19:40 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010
Bromomethane 1 09/22/23 19:40 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 09/22/23 19:40 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 09/22/23 19:40 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 09/22/23 19:40 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 09/22/23 19:40 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 09/22/23 19:40 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 09/22/23 19:40 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 09/22/23 19:40 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 09/22/23 19:40 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0052-Chlorotoluene 1 09/22/23 19:40 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 09/22/23 19:40 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 09/22/23 19:40 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-2
95974 Matrix:
9/21/2023 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 09/22/23 19:40 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,2-Dibromoethane 1 09/22/23 19:40 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 09/22/23 19:40 V38309TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 09/22/23 19:40 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 09/22/23 19:40 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,4-Dichlorobenzene 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 09/22/23 19:40 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 09/22/23 19:40 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 09/22/23 19:40 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.005cis-1,2-Dichloroethene 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 09/22/23 19:40 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 09/22/23 19:40 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 09/22/23 19:40 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 09/22/23 19:40 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 09/22/23 19:40 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 09/22/23 19:40 V38309TBL
<0.015 mg/Kg - dry 0.015 0.268Ethanol 1 09/22/23 19:40 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 09/22/23 19:40 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.053Ethyl Tertiary Butyl Ether (ETBE)1 09/22/23 19:40 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.010Hexachlorobutadiene 1 09/22/23 19:40 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-2
95974 Matrix:
9/21/2023 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.003 J mg/Kg - dry 0.0007 0.010n-Hexane 1 09/22/23 19:40 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.021
2-Hexanone 1 09/22/23 19:40 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 09/22/23 19:40 V38309TBL
0.002 J mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 09/22/23 19:40 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 09/22/23 19:40 V38309TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 09/22/23 19:40 V38309TBL
0.005 J mg/Kg - dry 0.001 0.010Methylene Chloride 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010
Naphthalene 1 09/22/23 19:40 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 09/22/23 19:40 V38309TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 09/22/23 19:40 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 09/22/23 19:40 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 09/22/23 19:40 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 09/22/23 19:40 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 09/22/23 19:40 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 09/22/23 19:40 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.005Trichloroethene 1 09/22/23 19:40 V38309TBL
<0.002 mg/Kg - dry 0.002 0.010Trichlorofluoromethane 1 09/22/23 19:40 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 09/22/23 19:40 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-2
95974 Matrix:
9/21/2023 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 09/22/23 19:40 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 09/22/23 19:40 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 09/22/23 19:40 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 09/22/23 19:40 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 09/22/23 19:40 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 09/22/23 19:40 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 09/22/23 19:40 V38309
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%09/22/23 19:401 TBL V38309
Surrogate: Dibromofluoromethane 101 Limits: 84-123%09/22/23 19:401 TBL V38309
Surrogate: Toluene-d8 99.1 Limits: 76-129%09/22/23 19:401 TBL V38309
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
0.217 J mg/Kg - dry 0.124 0.707Acenaphthene 1 09/26/23 19:51 V38347AMP
<0.112 mg/Kg - dry 0.112 0.707Acenaphthylene 1 09/26/23 19:51 V38347AMP
<0.162 mg/Kg - dry 0.162 0.707Aniline 1 09/26/23 19:51 V38347AMP
0.388 J mg/Kg - dry 0.153 0.707Anthracene 1 09/26/23 19:51 V38347AMP
1.00 mg/Kg - dry 0.149 0.707
Benzo(a)anthracene 1 09/26/23 19:51 V38347AMP
0.997 mg/Kg - dry 0.157 0.707Benzo(a)pyrene 1 09/26/23 19:51 V38347AMP
1.33 mg/Kg - dry 0.156 0.707Benzo(b)fluoranthene 1 09/26/23 19:51 V38347AMP
0.615 J mg/Kg - dry 0.145 0.707Benzo(g,h,i)perylene 1 09/26/23 19:51 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-2
95974 Matrix:
9/21/2023 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
0.381 J mg/Kg - dry 0.146 0.707Benzo(k)fluoranthene 1 09/26/23 19:51 V38347AMP
<0.621 mg/Kg - dry 0.621 2.14
Benzoic Acid 1 09/26/23 19:51 V38347AMP
<0.112 mg/Kg - dry 0.112 0.707Benzyl alcohol 1 09/26/23 19:51 V38347AMP
<0.126 mg/Kg - dry 0.126 0.707Bis(2-Chloroethoxy)methane 1 09/26/23 19:51 V38347AMP
<0.114 mg/Kg - dry 0.114 0.707Bis(2-Chloroethyl)ether 1 09/26/23 19:51 V38347AMP
<0.145 mg/Kg - dry 0.145 0.353Bis(2-Chloroisopropyl)ether 1 09/26/23 19:51 V38347AMP
<0.128 mg/Kg - dry 0.128 0.707Bis(2-ethylhexyl)phthalate 1 09/26/23 19:51 V38347AMP
<0.116 mg/Kg - dry 0.116 0.7074-Bromophenyl phenyl ether 1 09/26/23 19:51 V38347AMP
<0.121 mg/Kg - dry 0.121 0.353
Butyl benzyl phthalate 1 09/26/23 19:51 V38347AMP
<0.099 mg/Kg - dry 0.099 0.7074-Chloro-3-methylphenol 1 09/26/23 19:51 V38347AMP
<0.120 mg/Kg - dry 0.120 0.3534-Chloroaniline 1 09/26/23 19:51 V38347AMP
<0.124 mg/Kg - dry 0.124 0.7072-Chloronaphthalene 1 09/26/23 19:51 V38347AMP
<0.105 mg/Kg - dry 0.105 0.7072-Chlorophenol 1 09/26/23 19:51 V38347AMP
<0.135 mg/Kg - dry 0.135 1.074-Chlorophenyl phenyl ether 1 09/26/23 19:51 V38347AMP
0.965 mg/Kg - dry 0.152 0.707Chrysene 1 09/26/23 19:51 V38347AMP
<0.246 mg/Kg - dry 0.246 0.707Dibenz(a,h)anthracene 1 09/26/23 19:51 V38347AMP
<0.127 mg/Kg - dry 0.127 0.707Dibenzofuran 1 09/26/23 19:51 V38347AMP
<0.101 mg/Kg - dry 0.101 0.7071,2-Dichlorobenzene 1 09/26/23 19:51 V38347AMP
<0.104 mg/Kg - dry 0.104 0.7071,3-Dichlorobenzene 1 09/26/23 19:51 V38347AMP
<0.104 mg/Kg - dry 0.104 0.3531,4-Dichlorobenzene 1 09/26/23 19:51 V38347AMP
<0.157 mg/Kg - dry 0.157 0.7073,3'-Dichlorobenzidine 1 09/26/23 19:51 V38347AMP
<0.102 mg/Kg - dry 0.102 0.7072,4-Dichlorophenol 1 09/26/23 19:51 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-2
95974 Matrix:
9/21/2023 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.193 mg/Kg - dry 0.193 0.707Diethyl phthalate 1 09/26/23 19:51 V38347AMP
<0.186 mg/Kg - dry 0.186 0.707
Dimethyl phthalate 1 09/26/23 19:51 V38347AMP
<0.115 mg/Kg - dry 0.115 0.3532,4-Dimethylphenol 1 09/26/23 19:51 V38347AMP
<0.114 mg/Kg - dry 0.114 0.707Di-n-butyl phthalate 1 09/26/23 19:51 V38347AMP
<0.257 mg/Kg - dry 0.257 1.614,6-Dinitro-2-methylphenol 1 09/26/23 19:51 V38347AMP
<0.557 mg/Kg - dry 0.557 1.612,4-Dinitrophenol 1 09/26/23 19:51 V38347AMP
<0.103 mg/Kg - dry 0.103 0.7072,4-Dinitrotoluene 1 09/26/23 19:51 V38347AMP
<0.115 mg/Kg - dry 0.115 0.7072,6-Dinitrotoluene 1 09/26/23 19:51 V38347AMP
<0.153 mg/Kg - dry 0.153 0.353
Di-n-Octyl Phthalate 1 09/26/23 19:51 V38347AMP
1.99 mg/Kg - dry 0.131 0.707Fluoranthene 1 09/26/23 19:51 V38347AMP
0.156 J mg/Kg - dry 0.137 0.707Fluorene 1 09/26/23 19:51 V38347AMP
<0.113 mg/Kg - dry 0.113 0.707Hexachlorobenzene 1 09/26/23 19:51 V38347AMP
<0.104 mg/Kg - dry 0.104 0.707Hexachlorobutadiene 1 09/26/23 19:51 V38347AMP
<0.168 mg/Kg - dry 0.168 0.707Hexachlorocyclopentadiene 1 09/26/23 19:51 V38347AMP
<0.084 mg/Kg - dry 0.084 0.707Hexachloroethane 1 09/26/23 19:51 V38347AMP
0.670 J mg/Kg - dry 0.191 0.707Indeno(1,2,3-cd)pyrene 1 09/26/23 19:51 V38347AMP
<0.204 mg/Kg - dry 0.204 0.707Isophorone 1 09/26/23 19:51 V38347AMP
<0.113 mg/Kg - dry 0.113 0.7071-Methylnaphthalene 1 09/26/23 19:51 V38347AMP
<0.107 mg/Kg - dry 0.107 0.7072-Methylnaphthalene 1 09/26/23 19:51 V38347AMP
<0.104 mg/Kg - dry 0.104 0.7072-Methylphenol 1 09/26/23 19:51 V38347AMP
<0.091 mg/Kg - dry 0.091 0.7073&4 Methylphenol 1 09/26/23 19:51 V38347AMP
<0.154 mg/Kg - dry 0.154 0.707Naphthalene 1 09/26/23 19:51 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-2
95974 Matrix:
9/21/2023 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.103 mg/Kg - dry 0.103 0.7072-Nitroaniline 1 09/26/23 19:51 V38347AMP
<0.128 mg/Kg - dry 0.128 0.707
3-Nitroaniline 1 09/26/23 19:51 V38347AMP
<0.100 mg/Kg - dry 0.100 0.3534-Nitroaniline 1 09/26/23 19:51 V38347AMP
<0.124 mg/Kg - dry 0.124 0.353Nitrobenzene 1 09/26/23 19:51 V38347AMP
<0.095 mg/Kg - dry 0.095 0.7072-Nitrophenol 1 09/26/23 19:51 V38347AMP
<0.125 mg/Kg - dry 0.125 0.7074-Nitrophenol 1 09/26/23 19:51 V38347AMP
<0.282 mg/Kg - dry 0.282 0.707N-Nitrosodimethylamine 1 09/26/23 19:51 V38347AMP
<0.194 mg/Kg - dry 0.194 0.707N-Nitrosodiphenylamine 1 09/26/23 19:51 V38347AMP
<0.126 mg/Kg - dry 0.126 0.707
N-Nitroso-di-n-propylamine 1 09/26/23 19:51 V38347AMP
<0.372 mg/Kg - dry 0.372 1.07Pentachlorophenol 1 09/26/23 19:51 V38347AMP
1.55 mg/Kg - dry 0.223 0.707Phenanthrene 1 09/26/23 19:51 V38347AMP
<0.120 mg/Kg - dry 0.120 0.707Phenol 1 09/26/23 19:51 V38347AMP
1.80 mg/Kg - dry 0.143 0.707Pyrene 1 09/26/23 19:51 V38347AMP
<0.084 mg/Kg - dry 0.084 0.353Pyridine 1 09/26/23 19:51 V38347AMP
<0.114 mg/Kg - dry 0.114 0.7071,2,4-Trichlorobenzene 1 09/26/23 19:51 V38347AMP
<0.103 mg/Kg - dry 0.103 0.7072,4,5-Trichlorophenol 1 09/26/23 19:51 V38347AMP
<0.103 mg/Kg - dry 0.103 0.7072,4,6-Trichlorophenol 1 09/26/23 19:51 V38347AMP
8270ESurrogate: Phenol-d5 68.8 Limits: 34-121%09/26/23 19:511 AMP
Surrogate: 2-Fluorobiphenyl 85.6 Limits: 44-115%09/26/23 19:511 AMP V38347
Surrogate: 2-Fluorophenol 72.4 Limits: 35-115%09/26/23 19:511 AMP V38347
Surrogate: Nitrobenzene-d5 78.4 Limits: 37-122%09/26/23 19:511 AMP V38347
Surrogate: 4-Terphenyl-d14 90.4 Limits: 54-127%09/26/23 19:511 AMP V38347
Surrogate: 2,4,6-Tribromophenol 72.4 Limits: 39-132%09/26/23 19:511 AMP V38347
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-3
95975 Matrix:
9/21/2023 14:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.5 %Moisture 1 09/25/23 10:40 SW-DRYWTCNC
0.411 mg/Kg - dry 0.175 0.248Chromium, Hexavalent 1 10/03/23 14:08 SW-7199NFP
4.71 mg/Kg - dry 0.106 0.311Arsenic 5 09/29/23 15:18 6020BCPW
85.8 mg/Kg - dry 0.053 0.310Barium 5 09/29/23 15:18 6020BCPW
0.268 J mg/Kg - dry 0.0322 0.311Cadmium 5 09/29/23 15:18 6020BCPW
92.8 mg/Kg - dry 0.144 0.310
Chromium 5 09/29/23 15:18 6020BCPW
82.2 mg/Kg - dry 0.0385 0.311Lead 5 09/29/23 15:18 6020BCPW
0.0920 mg/Kg - dry 0.0149 0.0373Mercury (Total)1 09/28/23 14:17 7471BJKC
0.904 mg/Kg - dry 0.127 0.310Selenium 5 09/29/23 15:18 6020BCPW
0.0559 J mg/Kg - dry 0.0083 0.311Silver 5 09/29/23 15:18 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-3
95975 Matrix:
9/21/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.091 mg/Kg - dry 0.002 0.024Acetone 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 09/22/23 20:08 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 09/22/23 20:08 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/22/23 20:08 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/22/23 20:08 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/22/23 20:08 V38309TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/22/23 20:08 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/22/23 20:08 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/22/23 20:08 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/22/23 20:08 V38309TBL
0.001 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 09/22/23 20:08 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/22/23 20:08 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/22/23 20:08 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/22/23 20:08 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/22/23 20:08 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/22/23 20:08 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-3
95975 Matrix:
9/21/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 09/22/23 20:08 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 09/22/23 20:08 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/22/23 20:08 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/22/23 20:08 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/22/23 20:08 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/22/23 20:08 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/22/23 20:08 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/22/23 20:08 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 09/22/23 20:08 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/22/23 20:08 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 09/22/23 20:08 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/22/23 20:08 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 09/22/23 20:08 V38309TBL
<0.017 mg/Kg - dry 0.017 0.310Ethanol 1 09/22/23 20:08 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 09/22/23 20:08 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 09/22/23 20:08 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-3
95975 Matrix:
9/21/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.003 J mg/Kg - dry 0.0008 0.012n-Hexane 1 09/22/23 20:08 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 09/22/23 20:08 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/22/23 20:08 V38309TBL
0.010 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 09/22/23 20:08 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/22/23 20:08 V38309TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 09/22/23 20:08 V38309TBL
0.005 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 09/22/23 20:08 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/22/23 20:08 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/22/23 20:08 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/22/23 20:08 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/22/23 20:08 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/22/23 20:08 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/22/23 20:08 V38309TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/22/23 20:08 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/22/23 20:08 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-3
95975 Matrix:
9/21/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/22/23 20:08 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 09/22/23 20:08 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/22/23 20:08 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/22/23 20:08 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/22/23 20:08 V38309TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/22/23 20:08 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/22/23 20:08 V38309
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%09/22/23 20:081 TBL V38309
Surrogate: Dibromofluoromethane 101 Limits: 84-123%09/22/23 20:081 TBL V38309
Surrogate: Toluene-d8 99.1 Limits: 76-129%09/22/23 20:081 TBL V38309
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.576 mg/Kg - dry 0.576 3.28Acenaphthene 4 09/26/23 20:58 V38347AMP
<0.521 mg/Kg - dry 0.521 3.28Acenaphthylene 4 09/26/23 20:58 V38347AMP
<0.755 mg/Kg - dry 0.755 3.28Aniline 4 09/26/23 20:58 V38347AMP
0.716 J mg/Kg - dry 0.710 3.28Anthracene 4 09/26/23 20:58 V38347AMP
2.22 J
mg/Kg - dry 0.690 3.28
Benzo(a)anthracene 4 09/26/23 20:58 V38347AMP
2.25 J mg/Kg - dry 0.730 3.28Benzo(a)pyrene 4 09/26/23 20:58 V38347AMP
2.86 J mg/Kg - dry 0.725 3.28Benzo(b)fluoranthene 4 09/26/23 20:58 V38347AMP
1.38 J mg/Kg - dry 0.675 3.28Benzo(g,h,i)perylene 4 09/26/23 20:58 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-3
95975 Matrix:
9/21/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
1.00 J mg/Kg - dry 0.680 3.28Benzo(k)fluoranthene 4 09/26/23 20:58 V38347AMP
<2.88 mg/Kg - dry 2.88 9.94
Benzoic Acid 4 09/26/23 20:58 V38347AMP
<0.521 mg/Kg - dry 0.521 3.28Benzyl alcohol 4 09/26/23 20:58 V38347AMP
<0.586 mg/Kg - dry 0.586 3.28Bis(2-Chloroethoxy)methane 4 09/26/23 20:58 V38347AMP
<0.531 mg/Kg - dry 0.531 3.28Bis(2-Chloroethyl)ether 4 09/26/23 20:58 V38347AMP
<0.675 mg/Kg - dry 0.675 1.64Bis(2-Chloroisopropyl)ether 4 09/26/23 20:58 V38347AMP
<0.596 mg/Kg - dry 0.596 3.28Bis(2-ethylhexyl)phthalate 4 09/26/23 20:58 V38347AMP
<0.541 mg/Kg - dry 0.541 3.284-Bromophenyl phenyl ether 4 09/26/23 20:58 V38347AMP
<0.561 mg/Kg - dry 0.561 1.64
Butyl benzyl phthalate 4 09/26/23 20:58 V38347AMP
<0.459 mg/Kg - dry 0.459 3.284-Chloro-3-methylphenol 4 09/26/23 20:58 V38347AMP
<0.556 mg/Kg - dry 0.556 1.644-Chloroaniline 4 09/26/23 20:58 V38347AMP
<0.576 mg/Kg - dry 0.576 3.282-Chloronaphthalene 4 09/26/23 20:58 V38347AMP
<0.488 mg/Kg - dry 0.488 3.282-Chlorophenol 4 09/26/23 20:58 V38347AMP
<0.626 mg/Kg - dry 0.626 4.974-Chlorophenyl phenyl ether 4 09/26/23 20:58 V38347AMP
2.14 J mg/Kg - dry 0.705 3.28Chrysene 4 09/26/23 20:58 V38347AMP
<1.14 mg/Kg - dry 1.14 3.28Dibenz(a,h)anthracene 4 09/26/23 20:58 V38347AMP
<0.591 mg/Kg - dry 0.591 3.28Dibenzofuran 4 09/26/23 20:58 V38347AMP
<0.469 mg/Kg - dry 0.469 3.281,2-Dichlorobenzene 4 09/26/23 20:58 V38347AMP
<0.483 mg/Kg - dry 0.483 3.281,3-Dichlorobenzene 4 09/26/23 20:58 V38347AMP
<0.484 mg/Kg - dry 0.484 1.641,4-Dichlorobenzene 4 09/26/23 20:58 V38347AMP
<0.730 mg/Kg - dry 0.730 3.283,3'-Dichlorobenzidine 4 09/26/23 20:58 V38347AMP
<0.475 mg/Kg - dry 0.475 3.282,4-Dichlorophenol 4 09/26/23 20:58 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-3
95975 Matrix:
9/21/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.894 mg/Kg - dry 0.894 3.28Diethyl phthalate 4 09/26/23 20:58 V38347AMP
<0.864 mg/Kg - dry 0.864 3.28
Dimethyl phthalate 4 09/26/23 20:58 V38347AMP
<0.536 mg/Kg - dry 0.536 1.642,4-Dimethylphenol 4 09/26/23 20:58 V38347AMP
<0.531 mg/Kg - dry 0.531 3.28Di-n-butyl phthalate 4 09/26/23 20:58 V38347AMP
<1.19 mg/Kg - dry 1.19 7.454,6-Dinitro-2-methylphenol 4 09/26/23 20:58 V38347AMP
<2.58 mg/Kg - dry 2.58 7.452,4-Dinitrophenol 4 09/26/23 20:58 V38347AMP
<0.479 mg/Kg - dry 0.479 3.282,4-Dinitrotoluene 4 09/26/23 20:58 V38347AMP
<0.536 mg/Kg - dry 0.536 3.282,6-Dinitrotoluene 4 09/26/23 20:58 V38347AMP
<0.710 mg/Kg - dry 0.710 1.64
Di-n-Octyl Phthalate 4 09/26/23 20:58 V38347AMP
4.25 mg/Kg - dry 0.611 3.28Fluoranthene 4 09/26/23 20:58 V38347AMP
<0.636 mg/Kg - dry 0.636 3.28Fluorene 4 09/26/23 20:58 V38347AMP
<0.526 mg/Kg - dry 0.526 3.28Hexachlorobenzene 4 09/26/23 20:58 V38347AMP
<0.484 mg/Kg - dry 0.484 3.28Hexachlorobutadiene 4 09/26/23 20:58 V38347AMP
<0.780 mg/Kg - dry 0.780 3.28Hexachlorocyclopentadiene 4 09/26/23 20:58 V38347AMP
<0.393 mg/Kg - dry 0.393 3.28Hexachloroethane 4 09/26/23 20:58 V38347AMP
1.47 J mg/Kg - dry 0.889 3.28Indeno(1,2,3-cd)pyrene 4 09/26/23 20:58 V38347AMP
<0.949 mg/Kg - dry 0.949 3.28Isophorone 4 09/26/23 20:58 V38347AMP
<0.526 mg/Kg - dry 0.526 3.281-Methylnaphthalene 4 09/26/23 20:58 V38347AMP
<0.496 mg/Kg - dry 0.496 3.282-Methylnaphthalene 4 09/26/23 20:58 V38347AMP
<0.481 mg/Kg - dry 0.481 3.282-Methylphenol 4 09/26/23 20:58 V38347AMP
<0.422 mg/Kg - dry 0.422 3.283&4 Methylphenol 4 09/26/23 20:58 V38347AMP
<0.715 mg/Kg - dry 0.715 3.28Naphthalene 4 09/26/23 20:58 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-3
95975 Matrix:
9/21/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.480 mg/Kg - dry 0.480 3.282-Nitroaniline 4 09/26/23 20:58 V38347AMP
<0.596 mg/Kg - dry 0.596 3.28
3-Nitroaniline 4 09/26/23 20:58 V38347AMP
<0.463 mg/Kg - dry 0.463 1.644-Nitroaniline 4 09/26/23 20:58 V38347AMP
<0.576 mg/Kg - dry 0.576 1.64Nitrobenzene 4 09/26/23 20:58 V38347AMP
<0.440 mg/Kg - dry 0.440 3.282-Nitrophenol 4 09/26/23 20:58 V38347AMP
<0.581 mg/Kg - dry 0.581 3.284-Nitrophenol 4 09/26/23 20:58 V38347AMP
<1.30 mg/Kg - dry 1.30 3.28N-Nitrosodimethylamine 4 09/26/23 20:58 V38347AMP
<0.899 mg/Kg - dry 0.899 3.28N-Nitrosodiphenylamine 4 09/26/23 20:58 V38347AMP
<0.586 mg/Kg - dry 0.586 3.28
N-Nitroso-di-n-propylamine 4 09/26/23 20:58 V38347AMP
<1.73 mg/Kg - dry 1.73 4.97Pentachlorophenol 4 09/26/23 20:58 V38347AMP
2.80 J mg/Kg - dry 1.03 3.28Phenanthrene 4 09/26/23 20:58 V38347AMP
<0.556 mg/Kg - dry 0.556 3.28Phenol 4 09/26/23 20:58 V38347AMP
3.98 mg/Kg - dry 0.665 3.28Pyrene 4 09/26/23 20:58 V38347AMP
<0.393 mg/Kg - dry 0.393 1.64Pyridine 4 09/26/23 20:58 V38347AMP
<0.531 mg/Kg - dry 0.531 3.281,2,4-Trichlorobenzene 4 09/26/23 20:58 V38347AMP
<0.478 mg/Kg - dry 0.478 3.282,4,5-Trichlorophenol 4 09/26/23 20:58 V38347AMP
<0.479 mg/Kg - dry 0.479 3.282,4,6-Trichlorophenol 4 09/26/23 20:58 V38347AMP
8270ESurrogate: Phenol-d5 63.4 Limits: 34-121%09/26/23 20:584 AMP
Surrogate: 2-Fluorobiphenyl 80.1 Limits: 44-115%09/26/23 20:584 AMP V38347
Surrogate: 2-Fluorophenol 64.9 Limits: 35-115%09/26/23 20:584 AMP V38347
Surrogate: Nitrobenzene-d5 74.1 Limits: 37-122%09/26/23 20:584 AMP V38347
Surrogate: 4-Terphenyl-d14 95.2 Limits: 54-127%09/26/23 20:584 AMP V38347
Surrogate: 2,4,6-Tribromophenol 63.1 Limits: 39-132%09/26/23 20:584 AMP V38347
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-4
95976 Matrix:
9/21/2023 15:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.9 %Moisture 1 09/25/23 10:40 SW-DRYWTCNC
0.389 mg/Kg - dry 0.160 0.227Chromium, Hexavalent 1 10/03/23 12:52 SW-7199NFP
1.91 mg/Kg - dry 0.0970 0.284Arsenic 5 09/29/23 15:22 6020BCPW
61.1 mg/Kg - dry 0.048 0.283Barium 5 09/29/23 15:22 6020BCPW
0.0552 J mg/Kg - dry 0.0295 0.284Cadmium 5 09/29/23 15:22 6020BCPW
24.1 mg/Kg - dry 0.131 0.283
Chromium 5 09/29/23 15:22 6020BCPW
6.40 mg/Kg - dry 0.0351 0.284Lead 5 09/29/23 15:22 6020BCPW
0.0279 J mg/Kg - dry 0.0136 0.0341Mercury (Total)1 09/28/23 14:19 7471BJKC
0.572 mg/Kg - dry 0.116 0.283Selenium 5 09/29/23 15:22 6020BCPW
0.0219 J mg/Kg - dry 0.0076 0.284Silver 5 09/29/23 15:22 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-4
95976 Matrix:
9/21/2023 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.006 J mg/Kg - dry 0.002 0.022Acetone 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.022
Acrolein 1 09/22/23 20:35 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 09/22/23 20:35 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 09/22/23 20:35 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 09/22/23 20:35 V38309TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 09/22/23 20:35 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 09/22/23 20:35 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 09/22/23 20:35 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 09/22/23 20:35 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 09/22/23 20:35 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 09/22/23 20:35 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-4
95976 Matrix:
9/21/2023 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 09/22/23 20:35 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 09/22/23 20:35 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 09/22/23 20:35 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 09/22/23 20:35 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 09/22/23 20:35 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 09/22/23 20:35 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 09/22/23 20:35 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 09/22/23 20:35 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 09/22/23 20:35 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 09/22/23 20:35 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 09/22/23 20:35 V38309TBL
<0.015 mg/Kg - dry 0.015 0.283Ethanol 1 09/22/23 20:35 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 09/22/23 20:35 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.056Ethyl Tertiary Butyl Ether (ETBE)1 09/22/23 20:35 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 09/22/23 20:35 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-4
95976 Matrix:
9/21/2023 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.004 J mg/Kg - dry 0.0007 0.011n-Hexane 1 09/22/23 20:35 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.022
2-Hexanone 1 09/22/23 20:35 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 09/22/23 20:35 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 09/22/23 20:35 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 09/22/23 20:35 V38309TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 09/22/23 20:35 V38309TBL
0.005 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 09/22/23 20:35 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 09/22/23 20:35 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 09/22/23 20:35 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 09/22/23 20:35 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 09/22/23 20:35 V38309TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 09/22/23 20:35 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 09/22/23 20:35 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-4
95976 Matrix:
9/21/2023 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 09/22/23 20:35 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 09/22/23 20:35 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 09/22/23 20:35 V38309TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 09/22/23 20:35 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 09/22/23 20:35 V38309
Surrogate: 4-Bromofluorobenzene 98.9 Limits: 70-130%09/22/23 20:351 TBL V38309
Surrogate: Dibromofluoromethane 102 Limits: 84-123%09/22/23 20:351 TBL V38309
Surrogate: Toluene-d8 99.4 Limits: 76-129%09/22/23 20:351 TBL V38309
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.131 mg/Kg - dry 0.131 0.749Acenaphthene 1 09/26/23 20:13 V38347AMP
<0.119 mg/Kg - dry 0.119 0.749Acenaphthylene 1 09/26/23 20:13 V38347AMP
<0.172 mg/Kg - dry 0.172 0.749Aniline 1 09/26/23 20:13 V38347AMP
0.169 J mg/Kg - dry 0.162 0.749Anthracene 1 09/26/23 20:13 V38347AMP
0.464 J
mg/Kg - dry 0.157 0.749
Benzo(a)anthracene 1 09/26/23 20:13 V38347AMP
0.471 J mg/Kg - dry 0.166 0.749Benzo(a)pyrene 1 09/26/23 20:13 V38347AMP
0.547 J mg/Kg - dry 0.165 0.749Benzo(b)fluoranthene 1 09/26/23 20:13 V38347AMP
0.300 J mg/Kg - dry 0.154 0.749Benzo(g,h,i)perylene 1 09/26/23 20:13 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-4
95976 Matrix:
9/21/2023 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
0.181 J mg/Kg - dry 0.155 0.749Benzo(k)fluoranthene 1 09/26/23 20:13 V38347AMP
<0.658 mg/Kg - dry 0.658 2.27
Benzoic Acid 1 09/26/23 20:13 V38347AMP
<0.119 mg/Kg - dry 0.119 0.749Benzyl alcohol 1 09/26/23 20:13 V38347AMP
<0.133 mg/Kg - dry 0.133 0.749Bis(2-Chloroethoxy)methane 1 09/26/23 20:13 V38347AMP
<0.121 mg/Kg - dry 0.121 0.749Bis(2-Chloroethyl)ether 1 09/26/23 20:13 V38347AMP
<0.154 mg/Kg - dry 0.154 0.374Bis(2-Chloroisopropyl)ether 1 09/26/23 20:13 V38347AMP
<0.136 mg/Kg - dry 0.136 0.749Bis(2-ethylhexyl)phthalate 1 09/26/23 20:13 V38347AMP
<0.123 mg/Kg - dry 0.123 0.7494-Bromophenyl phenyl ether 1 09/26/23 20:13 V38347AMP
<0.128 mg/Kg - dry 0.128 0.374
Butyl benzyl phthalate 1 09/26/23 20:13 V38347AMP
<0.104 mg/Kg - dry 0.104 0.7494-Chloro-3-methylphenol 1 09/26/23 20:13 V38347AMP
<0.127 mg/Kg - dry 0.127 0.3744-Chloroaniline 1 09/26/23 20:13 V38347AMP
<0.131 mg/Kg - dry 0.131 0.7492-Chloronaphthalene 1 09/26/23 20:13 V38347AMP
<0.111 mg/Kg - dry 0.111 0.7492-Chlorophenol 1 09/26/23 20:13 V38347AMP
<0.143 mg/Kg - dry 0.143 1.144-Chlorophenyl phenyl ether 1 09/26/23 20:13 V38347AMP
0.442 J mg/Kg - dry 0.161 0.749Chrysene 1 09/26/23 20:13 V38347AMP
<0.261 mg/Kg - dry 0.261 0.749Dibenz(a,h)anthracene 1 09/26/23 20:13 V38347AMP
<0.135 mg/Kg - dry 0.135 0.749Dibenzofuran 1 09/26/23 20:13 V38347AMP
<0.107 mg/Kg - dry 0.107 0.7491,2-Dichlorobenzene 1 09/26/23 20:13 V38347AMP
<0.110 mg/Kg - dry 0.110 0.7491,3-Dichlorobenzene 1 09/26/23 20:13 V38347AMP
<0.110 mg/Kg - dry 0.110 0.3741,4-Dichlorobenzene 1 09/26/23 20:13 V38347AMP
<0.166 mg/Kg - dry 0.166 0.7493,3'-Dichlorobenzidine 1 09/26/23 20:13 V38347AMP
<0.108 mg/Kg - dry 0.108 0.7492,4-Dichlorophenol 1 09/26/23 20:13 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-4
95976 Matrix:
9/21/2023 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.204 mg/Kg - dry 0.204 0.749Diethyl phthalate 1 09/26/23 20:13 V38347AMP
<0.197 mg/Kg - dry 0.197 0.749
Dimethyl phthalate 1 09/26/23 20:13 V38347AMP
<0.122 mg/Kg - dry 0.122 0.3742,4-Dimethylphenol 1 09/26/23 20:13 V38347AMP
<0.121 mg/Kg - dry 0.121 0.749Di-n-butyl phthalate 1 09/26/23 20:13 V38347AMP
<0.272 mg/Kg - dry 0.272 1.704,6-Dinitro-2-methylphenol 1 09/26/23 20:13 V38347AMP
<0.590 mg/Kg - dry 0.590 1.702,4-Dinitrophenol 1 09/26/23 20:13 V38347AMP
<0.109 mg/Kg - dry 0.109 0.7492,4-Dinitrotoluene 1 09/26/23 20:13 V38347AMP
<0.122 mg/Kg - dry 0.122 0.7492,6-Dinitrotoluene 1 09/26/23 20:13 V38347AMP
<0.162 mg/Kg - dry 0.162 0.374
Di-n-Octyl Phthalate 1 09/26/23 20:13 V38347AMP
0.737 J mg/Kg - dry 0.139 0.749Fluoranthene 1 09/26/23 20:13 V38347AMP
<0.145 mg/Kg - dry 0.145 0.749Fluorene 1 09/26/23 20:13 V38347AMP
<0.120 mg/Kg - dry 0.120 0.749Hexachlorobenzene 1 09/26/23 20:13 V38347AMP
<0.110 mg/Kg - dry 0.110 0.749Hexachlorobutadiene 1 09/26/23 20:13 V38347AMP
<0.178 mg/Kg - dry 0.178 0.749Hexachlorocyclopentadiene 1 09/26/23 20:13 V38347AMP
<0.089 mg/Kg - dry 0.089 0.749Hexachloroethane 1 09/26/23 20:13 V38347AMP
0.301 J mg/Kg - dry 0.203 0.749Indeno(1,2,3-cd)pyrene 1 09/26/23 20:13 V38347AMP
<0.216 mg/Kg - dry 0.216 0.749Isophorone 1 09/26/23 20:13 V38347AMP
0.130 J mg/Kg - dry 0.120 0.7491-Methylnaphthalene 1 09/26/23 20:13 V38347AMP
0.120 J mg/Kg - dry 0.113 0.7492-Methylnaphthalene 1 09/26/23 20:13 V38347AMP
<0.110 mg/Kg - dry 0.110 0.7492-Methylphenol 1 09/26/23 20:13 V38347AMP
<0.096 mg/Kg - dry 0.096 0.7493&4 Methylphenol 1 09/26/23 20:13 V38347AMP
<0.163 mg/Kg - dry 0.163 0.749Naphthalene 1 09/26/23 20:13 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-4
95976 Matrix:
9/21/2023 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.109 mg/Kg - dry 0.109 0.7492-Nitroaniline 1 09/26/23 20:13 V38347AMP
<0.136 mg/Kg - dry 0.136 0.749
3-Nitroaniline 1 09/26/23 20:13 V38347AMP
<0.105 mg/Kg - dry 0.105 0.3744-Nitroaniline 1 09/26/23 20:13 V38347AMP
<0.131 mg/Kg - dry 0.131 0.374Nitrobenzene 1 09/26/23 20:13 V38347AMP
<0.100 mg/Kg - dry 0.100 0.7492-Nitrophenol 1 09/26/23 20:13 V38347AMP
<0.132 mg/Kg - dry 0.132 0.7494-Nitrophenol 1 09/26/23 20:13 V38347AMP
<0.298 mg/Kg - dry 0.298 0.749N-Nitrosodimethylamine 1 09/26/23 20:13 V38347AMP
<0.205 mg/Kg - dry 0.205 0.749N-Nitrosodiphenylamine 1 09/26/23 20:13 V38347AMP
<0.133 mg/Kg - dry 0.133 0.749
N-Nitroso-di-n-propylamine 1 09/26/23 20:13 V38347AMP
<0.393 mg/Kg - dry 0.393 1.14Pentachlorophenol 1 09/26/23 20:13 V38347AMP
0.699 J mg/Kg - dry 0.236 0.749Phenanthrene 1 09/26/23 20:13 V38347AMP
<0.127 mg/Kg - dry 0.127 0.749Phenol 1 09/26/23 20:13 V38347AMP
0.891 mg/Kg - dry 0.152 0.749Pyrene 1 09/26/23 20:13 V38347AMP
<0.089 mg/Kg - dry 0.089 0.374Pyridine 1 09/26/23 20:13 V38347AMP
<0.121 mg/Kg - dry 0.121 0.7491,2,4-Trichlorobenzene 1 09/26/23 20:13 V38347AMP
<0.109 mg/Kg - dry 0.109 0.7492,4,5-Trichlorophenol 1 09/26/23 20:13 V38347AMP
<0.109 mg/Kg - dry 0.109 0.7492,4,6-Trichlorophenol 1 09/26/23 20:13 V38347AMP
8270ESurrogate: Phenol-d5 68.6 Limits: 34-121%09/26/23 20:131 AMP
Surrogate: 2-Fluorobiphenyl 84.4 Limits: 44-115%09/26/23 20:131 AMP V38347
Surrogate: 2-Fluorophenol 73.7 Limits: 35-115%09/26/23 20:131 AMP V38347
Surrogate: Nitrobenzene-d5 77.2 Limits: 37-122%09/26/23 20:131 AMP V38347
Surrogate: 4-Terphenyl-d14 90.4 Limits: 54-127%09/26/23 20:131 AMP V38347
Surrogate: 2,4,6-Tribromophenol 74.3 Limits: 39-132%09/26/23 20:131 AMP V38347
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-5
95977 Matrix:
9/21/2023 11:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.6 %Moisture 1 09/25/23 10:40 SW-DRYWTCNC
0.707 mg/Kg - dry 0.171 0.242Chromium, Hexavalent 1 10/03/23 14:41 SW-7199NFP
1.77 mg/Kg - dry 0.104 0.303Arsenic 5 09/29/23 15:27 6020BCPW
110 mg/Kg - dry 0.051 0.303Barium 5 09/29/23 15:27 6020BCPW
0.0639 J mg/Kg - dry 0.0315 0.303Cadmium 5 09/29/23 15:27 6020BCPW
24.0 mg/Kg - dry 0.140 0.303
Chromium 5 09/29/23 15:27 6020BCPW
11.3 mg/Kg - dry 0.0376 0.303Lead 5 09/29/23 15:27 6020BCPW
0.0421 mg/Kg - dry 0.0146 0.0364Mercury (Total)1 09/28/23 14:22 7471BJKC
0.910 mg/Kg - dry 0.125 0.303Selenium 5 09/29/23 15:27 6020BCPW
0.0300 J mg/Kg - dry 0.0081 0.303Silver 5 09/29/23 15:27 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-5
95977 Matrix:
9/21/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38312 09/25/23 08:00
0.010 J mg/Kg - dry 0.002 0.024Acetone 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 09/25/23 17:47 V38313TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 09/25/23 17:47 V38313TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/25/23 17:47 V38313TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/25/23 17:47 V38313TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/25/23 17:47 V38313TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/25/23 17:47 V38313TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/25/23 17:47 V38313TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/25/23 17:47 V38313TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/25/23 17:47 V38313TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 09/25/23 17:47 V38313TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/25/23 17:47 V38313TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/25/23 17:47 V38313TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/25/23 17:47 V38313TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/25/23 17:47 V38313TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/25/23 17:47 V38313TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-5
95977 Matrix:
9/21/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38312 09/25/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 09/25/23 17:47 V38313TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 09/25/23 17:47 V38313TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/25/23 17:47 V38313TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/25/23 17:47 V38313TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/25/23 17:47 V38313TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/25/23 17:47 V38313TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/25/23 17:47 V38313TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/25/23 17:47 V38313TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/25/23 17:47 V38313TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 09/25/23 17:47 V38313TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/25/23 17:47 V38313TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 09/25/23 17:47 V38313TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/25/23 17:47 V38313TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 09/25/23 17:47 V38313TBL
<0.016 mg/Kg - dry 0.016 0.303Ethanol 1 09/25/23 17:47 V38313TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 09/25/23 17:47 V38313TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 09/25/23 17:47 V38313TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-5
95977 Matrix:
9/21/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38312 09/25/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/25/23 17:47 V38313TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 09/25/23 17:47 V38313TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/25/23 17:47 V38313TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 09/25/23 17:47 V38313TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/25/23 17:47 V38313TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 09/25/23 17:47 V38313TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/25/23 17:47 V38313TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/25/23 17:47 V38313TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/25/23 17:47 V38313TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/25/23 17:47 V38313TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/25/23 17:47 V38313TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/25/23 17:47 V38313TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/25/23 17:47 V38313TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/25/23 17:47 V38313TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-5
95977 Matrix:
9/21/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38312 09/25/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/25/23 17:47 V38313TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 09/25/23 17:47 V38313TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/25/23 17:47 V38313TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/25/23 17:47 V38313TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/25/23 17:47 V38313TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/25/23 17:47 V38313TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/25/23 17:47 V38313
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%09/25/23 17:471 TBL V38313
Surrogate: Dibromofluoromethane 102 Limits: 84-123%09/25/23 17:471 TBL V38313
Surrogate: Toluene-d8 99.2 Limits: 76-129%09/25/23 17:471 TBL V38313
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.563 mg/Kg - dry 0.563 3.20Acenaphthene 4 09/26/23 21:21 V38347AMP
<0.509 mg/Kg - dry 0.509 3.20Acenaphthylene 4 09/26/23 21:21 V38347AMP
<0.737 mg/Kg - dry 0.737 3.20Aniline 4 09/26/23 21:21 V38347AMP
<0.694 mg/Kg - dry 0.694 3.20Anthracene 4 09/26/23 21:21 V38347AMP
<0.674 mg/Kg - dry 0.674 3.20
Benzo(a)anthracene 4 09/26/23 21:21 V38347AMP
<0.713 mg/Kg - dry 0.713 3.20Benzo(a)pyrene 4 09/26/23 21:21 V38347AMP
0.717 J mg/Kg - dry 0.708 3.20Benzo(b)fluoranthene 4 09/26/23 21:21 V38347AMP
<0.660 mg/Kg - dry 0.660 3.20Benzo(g,h,i)perylene 4 09/26/23 21:21 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-5
95977 Matrix:
9/21/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.665 mg/Kg - dry 0.665 3.20Benzo(k)fluoranthene 4 09/26/23 21:21 V38347AMP
<2.82 mg/Kg - dry 2.82 9.72
Benzoic Acid 4 09/26/23 21:21 V38347AMP
<0.509 mg/Kg - dry 0.509 3.20Benzyl alcohol 4 09/26/23 21:21 V38347AMP
<0.572 mg/Kg - dry 0.572 3.20Bis(2-Chloroethoxy)methane 4 09/26/23 21:21 V38347AMP
<0.519 mg/Kg - dry 0.519 3.20Bis(2-Chloroethyl)ether 4 09/26/23 21:21 V38347AMP
<0.660 mg/Kg - dry 0.660 1.60Bis(2-Chloroisopropyl)ether 4 09/26/23 21:21 V38347AMP
<0.582 mg/Kg - dry 0.582 3.20Bis(2-ethylhexyl)phthalate 4 09/26/23 21:21 V38347AMP
<0.529 mg/Kg - dry 0.529 3.204-Bromophenyl phenyl ether 4 09/26/23 21:21 V38347AMP
<0.548 mg/Kg - dry 0.548 1.60
Butyl benzyl phthalate 4 09/26/23 21:21 V38347AMP
<0.449 mg/Kg - dry 0.449 3.204-Chloro-3-methylphenol 4 09/26/23 21:21 V38347AMP
<0.543 mg/Kg - dry 0.543 1.604-Chloroaniline 4 09/26/23 21:21 V38347AMP
<0.563 mg/Kg - dry 0.563 3.202-Chloronaphthalene 4 09/26/23 21:21 V38347AMP
<0.476 mg/Kg - dry 0.476 3.202-Chlorophenol 4 09/26/23 21:21 V38347AMP
<0.612 mg/Kg - dry 0.612 4.874-Chlorophenyl phenyl ether 4 09/26/23 21:21 V38347AMP
<0.689 mg/Kg - dry 0.689 3.20Chrysene 4 09/26/23 21:21 V38347AMP
<1.12 mg/Kg - dry 1.12 3.20Dibenz(a,h)anthracene 4 09/26/23 21:21 V38347AMP
<0.577 mg/Kg - dry 0.577 3.20Dibenzofuran 4 09/26/23 21:21 V38347AMP
<0.458 mg/Kg - dry 0.458 3.201,2-Dichlorobenzene 4 09/26/23 21:21 V38347AMP
<0.472 mg/Kg - dry 0.472 3.201,3-Dichlorobenzene 4 09/26/23 21:21 V38347AMP
<0.473 mg/Kg - dry 0.473 1.601,4-Dichlorobenzene 4 09/26/23 21:21 V38347AMP
<0.713 mg/Kg - dry 0.713 3.203,3'-Dichlorobenzidine 4 09/26/23 21:21 V38347AMP
<0.464 mg/Kg - dry 0.464 3.202,4-Dichlorophenol 4 09/26/23 21:21 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-5
95977 Matrix:
9/21/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.873 mg/Kg - dry 0.873 3.20Diethyl phthalate 4 09/26/23 21:21 V38347AMP
<0.844 mg/Kg - dry 0.844 3.20
Dimethyl phthalate 4 09/26/23 21:21 V38347AMP
<0.524 mg/Kg - dry 0.524 1.602,4-Dimethylphenol 4 09/26/23 21:21 V38347AMP
<0.519 mg/Kg - dry 0.519 3.20Di-n-butyl phthalate 4 09/26/23 21:21 V38347AMP
<1.17 mg/Kg - dry 1.17 7.294,6-Dinitro-2-methylphenol 4 09/26/23 21:21 V38347AMP
<2.52 mg/Kg - dry 2.52 7.292,4-Dinitrophenol 4 09/26/23 21:21 V38347AMP
<0.468 mg/Kg - dry 0.468 3.202,4-Dinitrotoluene 4 09/26/23 21:21 V38347AMP
<0.524 mg/Kg - dry 0.524 3.202,6-Dinitrotoluene 4 09/26/23 21:21 V38347AMP
<0.694 mg/Kg - dry 0.694 1.60
Di-n-Octyl Phthalate 4 09/26/23 21:21 V38347AMP
1.02 J mg/Kg - dry 0.597 3.20Fluoranthene 4 09/26/23 21:21 V38347AMP
<0.621 mg/Kg - dry 0.621 3.20Fluorene 4 09/26/23 21:21 V38347AMP
<0.514 mg/Kg - dry 0.514 3.20Hexachlorobenzene 4 09/26/23 21:21 V38347AMP
<0.473 mg/Kg - dry 0.473 3.20Hexachlorobutadiene 4 09/26/23 21:21 V38347AMP
<0.762 mg/Kg - dry 0.762 3.20Hexachlorocyclopentadiene 4 09/26/23 21:21 V38347AMP
<0.384 mg/Kg - dry 0.384 3.20Hexachloroethane 4 09/26/23 21:21 V38347AMP
<0.868 mg/Kg - dry 0.868 3.20Indeno(1,2,3-cd)pyrene 4 09/26/23 21:21 V38347AMP
<0.927 mg/Kg - dry 0.927 3.20Isophorone 4 09/26/23 21:21 V38347AMP
<0.514 mg/Kg - dry 0.514 3.201-Methylnaphthalene 4 09/26/23 21:21 V38347AMP
<0.485 mg/Kg - dry 0.485 3.202-Methylnaphthalene 4 09/26/23 21:21 V38347AMP
<0.470 mg/Kg - dry 0.470 3.202-Methylphenol 4 09/26/23 21:21 V38347AMP
<0.412 mg/Kg - dry 0.412 3.203&4 Methylphenol 4 09/26/23 21:21 V38347AMP
<0.699 mg/Kg - dry 0.699 3.20Naphthalene 4 09/26/23 21:21 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-5
95977 Matrix:
9/21/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.469 mg/Kg - dry 0.469 3.202-Nitroaniline 4 09/26/23 21:21 V38347AMP
<0.582 mg/Kg - dry 0.582 3.20
3-Nitroaniline 4 09/26/23 21:21 V38347AMP
<0.452 mg/Kg - dry 0.452 1.604-Nitroaniline 4 09/26/23 21:21 V38347AMP
<0.563 mg/Kg - dry 0.563 1.60Nitrobenzene 4 09/26/23 21:21 V38347AMP
<0.430 mg/Kg - dry 0.430 3.202-Nitrophenol 4 09/26/23 21:21 V38347AMP
<0.567 mg/Kg - dry 0.567 3.204-Nitrophenol 4 09/26/23 21:21 V38347AMP
<1.27 mg/Kg - dry 1.27 3.20N-Nitrosodimethylamine 4 09/26/23 21:21 V38347AMP
<0.878 mg/Kg - dry 0.878 3.20N-Nitrosodiphenylamine 4 09/26/23 21:21 V38347AMP
<0.572 mg/Kg - dry 0.572 3.20
N-Nitroso-di-n-propylamine 4 09/26/23 21:21 V38347AMP
<1.69 mg/Kg - dry 1.69 4.87Pentachlorophenol 4 09/26/23 21:21 V38347AMP
<1.01 mg/Kg - dry 1.01 3.20Phenanthrene 4 09/26/23 21:21 V38347AMP
<0.543 mg/Kg - dry 0.543 3.20Phenol 4 09/26/23 21:21 V38347AMP
0.956 J mg/Kg - dry 0.650 3.20Pyrene 4 09/26/23 21:21 V38347AMP
<0.384 mg/Kg - dry 0.384 1.60Pyridine 4 09/26/23 21:21 V38347AMP
<0.519 mg/Kg - dry 0.519 3.201,2,4-Trichlorobenzene 4 09/26/23 21:21 V38347AMP
<0.467 mg/Kg - dry 0.467 3.202,4,5-Trichlorophenol 4 09/26/23 21:21 V38347AMP
<0.468 mg/Kg - dry 0.468 3.202,4,6-Trichlorophenol 4 09/26/23 21:21 V38347AMP
8270ESurrogate: Phenol-d5 64.4 Limits: 34-121%09/26/23 21:214 AMP
Surrogate: 2-Fluorobiphenyl 81.4 Limits: 44-115%09/26/23 21:214 AMP V38347
Surrogate: 2-Fluorophenol 68.6 Limits: 35-115%09/26/23 21:214 AMP V38347
Surrogate: Nitrobenzene-d5 73.7 Limits: 37-122%09/26/23 21:214 AMP V38347
Surrogate: 4-Terphenyl-d14 90.4 Limits: 54-127%09/26/23 21:214 AMP V38347
Surrogate: 2,4,6-Tribromophenol 69.2 Limits: 39-132%09/26/23 21:214 AMP V38347
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-6
95978 Matrix:
9/21/2023 9:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.5 %Moisture 1 09/25/23 10:40 SW-DRYWTCNC
0.294 mg/Kg - dry 0.174 0.248Chromium, Hexavalent 1 10/03/23 14:52 SW-7199NFP
1.88 mg/Kg - dry 0.104 0.303Arsenic 5 09/29/23 15:31 6020BCPW
102 mg/Kg - dry 0.051 0.303Barium 5 09/29/23 15:31 6020BCPW
0.135 J mg/Kg - dry 0.0315 0.303Cadmium 5 09/29/23 15:31 6020BCPW
30.5 mg/Kg - dry 0.140 0.303
Chromium 5 09/29/23 15:31 6020BCPW
23.2 mg/Kg - dry 0.0375 0.303Lead 5 09/29/23 15:31 6020BCPW
0.156 mg/Kg - dry 0.0145 0.0364Mercury (Total)1 09/28/23 14:24 7471BJKC
0.683 mg/Kg - dry 0.124 0.303Selenium 5 09/29/23 15:31 6020BCPW
0.0859 J mg/Kg - dry 0.0081 0.303Silver 5 09/29/23 15:31 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-6
95978 Matrix:
9/21/2023 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.034 mg/Kg - dry 0.002 0.024Acetone 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 09/22/23 21:29 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 09/22/23 21:29 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/22/23 21:29 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/22/23 21:29 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/22/23 21:29 V38309TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/22/23 21:29 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/22/23 21:29 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/22/23 21:29 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/22/23 21:29 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 09/22/23 21:29 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/22/23 21:29 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/22/23 21:29 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/22/23 21:29 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/22/23 21:29 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/22/23 21:29 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-6
95978 Matrix:
9/21/2023 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 09/22/23 21:29 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 09/22/23 21:29 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/22/23 21:29 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/22/23 21:29 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/22/23 21:29 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/22/23 21:29 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/22/23 21:29 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/22/23 21:29 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/22/23 21:29 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 09/22/23 21:29 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/22/23 21:29 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 09/22/23 21:29 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/22/23 21:29 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 09/22/23 21:29 V38309TBL
<0.016 mg/Kg - dry 0.016 0.303Ethanol 1 09/22/23 21:29 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 09/22/23 21:29 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 09/22/23 21:29 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-6
95978 Matrix:
9/21/2023 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.003 J mg/Kg - dry 0.0008 0.012n-Hexane 1 09/22/23 21:29 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 09/22/23 21:29 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/22/23 21:29 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 09/22/23 21:29 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/22/23 21:29 V38309TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 09/22/23 21:29 V38309TBL
0.004 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 09/22/23 21:29 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/22/23 21:29 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/22/23 21:29 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/22/23 21:29 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/22/23 21:29 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/22/23 21:29 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/22/23 21:29 V38309TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/22/23 21:29 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/22/23 21:29 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-6
95978 Matrix:
9/21/2023 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/22/23 21:29 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 09/22/23 21:29 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/22/23 21:29 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/22/23 21:29 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/22/23 21:29 V38309TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/22/23 21:29 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/22/23 21:29 V38309
Surrogate: 4-Bromofluorobenzene 98.9 Limits: 70-130%09/22/23 21:291 TBL V38309
Surrogate: Dibromofluoromethane 101 Limits: 84-123%09/22/23 21:291 TBL V38309
Surrogate: Toluene-d8 98.9 Limits: 76-129%09/22/23 21:291 TBL V38309
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.562 mg/Kg - dry 0.562 3.20Acenaphthene 4 09/26/23 21:43 V38347AMP
<0.509 mg/Kg - dry 0.509 3.20Acenaphthylene 4 09/26/23 21:43 V38347AMP
<0.736 mg/Kg - dry 0.736 3.20Aniline 4 09/26/23 21:43 V38347AMP
<0.693 mg/Kg - dry 0.693 3.20Anthracene 4 09/26/23 21:43 V38347AMP
<0.673 mg/Kg - dry 0.673 3.20
Benzo(a)anthracene 4 09/26/23 21:43 V38347AMP
<0.712 mg/Kg - dry 0.712 3.20Benzo(a)pyrene 4 09/26/23 21:43 V38347AMP
0.772 J mg/Kg - dry 0.707 3.20Benzo(b)fluoranthene 4 09/26/23 21:43 V38347AMP
<0.659 mg/Kg - dry 0.659 3.20Benzo(g,h,i)perylene 4 09/26/23 21:43 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-6
95978 Matrix:
9/21/2023 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.664 mg/Kg - dry 0.664 3.20Benzo(k)fluoranthene 4 09/26/23 21:43 V38347AMP
<2.81 mg/Kg - dry 2.81 9.70
Benzoic Acid 4 09/26/23 21:43 V38347AMP
<0.509 mg/Kg - dry 0.509 3.20Benzyl alcohol 4 09/26/23 21:43 V38347AMP
<0.572 mg/Kg - dry 0.572 3.20Bis(2-Chloroethoxy)methane 4 09/26/23 21:43 V38347AMP
<0.518 mg/Kg - dry 0.518 3.20Bis(2-Chloroethyl)ether 4 09/26/23 21:43 V38347AMP
<0.659 mg/Kg - dry 0.659 1.60Bis(2-Chloroisopropyl)ether 4 09/26/23 21:43 V38347AMP
<0.581 mg/Kg - dry 0.581 3.20Bis(2-ethylhexyl)phthalate 4 09/26/23 21:43 V38347AMP
<0.528 mg/Kg - dry 0.528 3.204-Bromophenyl phenyl ether 4 09/26/23 21:43 V38347AMP
<0.547 mg/Kg - dry 0.547 1.60
Butyl benzyl phthalate 4 09/26/23 21:43 V38347AMP
<0.448 mg/Kg - dry 0.448 3.204-Chloro-3-methylphenol 4 09/26/23 21:43 V38347AMP
<0.543 mg/Kg - dry 0.543 1.604-Chloroaniline 4 09/26/23 21:43 V38347AMP
<0.562 mg/Kg - dry 0.562 3.202-Chloronaphthalene 4 09/26/23 21:43 V38347AMP
<0.476 mg/Kg - dry 0.476 3.202-Chlorophenol 4 09/26/23 21:43 V38347AMP
<0.610 mg/Kg - dry 0.610 4.854-Chlorophenyl phenyl ether 4 09/26/23 21:43 V38347AMP
<0.688 mg/Kg - dry 0.688 3.20Chrysene 4 09/26/23 21:43 V38347AMP
<1.12 mg/Kg - dry 1.12 3.20Dibenz(a,h)anthracene 4 09/26/23 21:43 V38347AMP
<0.576 mg/Kg - dry 0.576 3.20Dibenzofuran 4 09/26/23 21:43 V38347AMP
<0.458 mg/Kg - dry 0.458 3.201,2-Dichlorobenzene 4 09/26/23 21:43 V38347AMP
<0.471 mg/Kg - dry 0.471 3.201,3-Dichlorobenzene 4 09/26/23 21:43 V38347AMP
<0.472 mg/Kg - dry 0.472 1.601,4-Dichlorobenzene 4 09/26/23 21:43 V38347AMP
<0.712 mg/Kg - dry 0.712 3.203,3'-Dichlorobenzidine 4 09/26/23 21:43 V38347AMP
<0.464 mg/Kg - dry 0.464 3.202,4-Dichlorophenol 4 09/26/23 21:43 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-6
95978 Matrix:
9/21/2023 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.872 mg/Kg - dry 0.872 3.20Diethyl phthalate 4 09/26/23 21:43 V38347AMP
<0.843 mg/Kg - dry 0.843 3.20
Dimethyl phthalate 4 09/26/23 21:43 V38347AMP
<0.523 mg/Kg - dry 0.523 1.602,4-Dimethylphenol 4 09/26/23 21:43 V38347AMP
<0.518 mg/Kg - dry 0.518 3.20Di-n-butyl phthalate 4 09/26/23 21:43 V38347AMP
<1.16 mg/Kg - dry 1.16 7.274,6-Dinitro-2-methylphenol 4 09/26/23 21:43 V38347AMP
<2.52 mg/Kg - dry 2.52 7.272,4-Dinitrophenol 4 09/26/23 21:43 V38347AMP
<0.467 mg/Kg - dry 0.467 3.202,4-Dinitrotoluene 4 09/26/23 21:43 V38347AMP
<0.523 mg/Kg - dry 0.523 3.202,6-Dinitrotoluene 4 09/26/23 21:43 V38347AMP
<0.693 mg/Kg - dry 0.693 1.60
Di-n-Octyl Phthalate 4 09/26/23 21:43 V38347AMP
1.07 J mg/Kg - dry 0.596 3.20Fluoranthene 4 09/26/23 21:43 V38347AMP
<0.620 mg/Kg - dry 0.620 3.20Fluorene 4 09/26/23 21:43 V38347AMP
<0.513 mg/Kg - dry 0.513 3.20Hexachlorobenzene 4 09/26/23 21:43 V38347AMP
<0.472 mg/Kg - dry 0.472 3.20Hexachlorobutadiene 4 09/26/23 21:43 V38347AMP
<0.761 mg/Kg - dry 0.761 3.20Hexachlorocyclopentadiene 4 09/26/23 21:43 V38347AMP
<0.384 mg/Kg - dry 0.384 3.20Hexachloroethane 4 09/26/23 21:43 V38347AMP
<0.867 mg/Kg - dry 0.867 3.20Indeno(1,2,3-cd)pyrene 4 09/26/23 21:43 V38347AMP
<0.926 mg/Kg - dry 0.926 3.20Isophorone 4 09/26/23 21:43 V38347AMP
<0.513 mg/Kg - dry 0.513 3.201-Methylnaphthalene 4 09/26/23 21:43 V38347AMP
<0.484 mg/Kg - dry 0.484 3.202-Methylnaphthalene 4 09/26/23 21:43 V38347AMP
<0.470 mg/Kg - dry 0.470 3.202-Methylphenol 4 09/26/23 21:43 V38347AMP
<0.412 mg/Kg - dry 0.412 3.203&4 Methylphenol 4 09/26/23 21:43 V38347AMP
<0.698 mg/Kg - dry 0.698 3.20Naphthalene 4 09/26/23 21:43 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-6
95978 Matrix:
9/21/2023 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.469 mg/Kg - dry 0.469 3.202-Nitroaniline 4 09/26/23 21:43 V38347AMP
<0.581 mg/Kg - dry 0.581 3.20
3-Nitroaniline 4 09/26/23 21:43 V38347AMP
<0.452 mg/Kg - dry 0.452 1.604-Nitroaniline 4 09/26/23 21:43 V38347AMP
<0.562 mg/Kg - dry 0.562 1.60Nitrobenzene 4 09/26/23 21:43 V38347AMP
<0.430 mg/Kg - dry 0.430 3.202-Nitrophenol 4 09/26/23 21:43 V38347AMP
<0.567 mg/Kg - dry 0.567 3.204-Nitrophenol 4 09/26/23 21:43 V38347AMP
<1.27 mg/Kg - dry 1.27 3.20N-Nitrosodimethylamine 4 09/26/23 21:43 V38347AMP
<0.877 mg/Kg - dry 0.877 3.20N-Nitrosodiphenylamine 4 09/26/23 21:43 V38347AMP
<0.572 mg/Kg - dry 0.572 3.20
N-Nitroso-di-n-propylamine 4 09/26/23 21:43 V38347AMP
<1.68 mg/Kg - dry 1.68 4.85Pentachlorophenol 4 09/26/23 21:43 V38347AMP
<1.01 mg/Kg - dry 1.01 3.20Phenanthrene 4 09/26/23 21:43 V38347AMP
<0.543 mg/Kg - dry 0.543 3.20Phenol 4 09/26/23 21:43 V38347AMP
1.06 J mg/Kg - dry 0.649 3.20Pyrene 4 09/26/23 21:43 V38347AMP
<0.384 mg/Kg - dry 0.384 1.60Pyridine 4 09/26/23 21:43 V38347AMP
<0.518 mg/Kg - dry 0.518 3.201,2,4-Trichlorobenzene 4 09/26/23 21:43 V38347AMP
<0.466 mg/Kg - dry 0.466 3.202,4,5-Trichlorophenol 4 09/26/23 21:43 V38347AMP
<0.467 mg/Kg - dry 0.467 3.202,4,6-Trichlorophenol 4 09/26/23 21:43 V38347AMP
8270ESurrogate: Phenol-d5 65.2 Limits: 34-121%09/26/23 21:434 AMP
Surrogate: 2-Fluorobiphenyl 82.5 Limits: 44-115%09/26/23 21:434 AMP V38347
Surrogate: 2-Fluorophenol 68.2 Limits: 35-115%09/26/23 21:434 AMP V38347
Surrogate: Nitrobenzene-d5 73.5 Limits: 37-122%09/26/23 21:434 AMP V38347
Surrogate: 4-Terphenyl-d14 88.0 Limits: 54-127%09/26/23 21:434 AMP V38347
Surrogate: 2,4,6-Tribromophenol 68.8 Limits: 39-132%09/26/23 21:434 AMP V38347
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-DUP
95979 Matrix:
9/21/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
6.76 %Moisture 1 09/25/23 10:40 SW-DRYWTCNC
0.408 mg/Kg - dry 0.153 0.218Chromium, Hexavalent 1 10/03/23 15:03 SW-7199NFP
5.28 mg/Kg - dry 0.0916 0.268Arsenic 5 09/29/23 15:35 6020BCPW
81.6 mg/Kg - dry 0.045 0.268Barium 5 09/29/23 15:35 6020BCPW
0.0863 J mg/Kg - dry 0.0278 0.268Cadmium 5 09/29/23 15:35 6020BCPW
25.0 mg/Kg - dry 0.124 0.268
Chromium 5 09/29/23 15:35 6020BCPW
15.4 mg/Kg - dry 0.0332 0.268Lead 5 09/29/23 15:35 6020BCPW
0.124 mg/Kg - dry 0.0129 0.0322Mercury (Total)1 09/28/23 14:27 7471BJKC
0.706 mg/Kg - dry 0.110 0.268Selenium 5 09/29/23 15:35 6020BCPW
0.0312 J mg/Kg - dry 0.0072 0.268Silver 5 09/29/23 15:35 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-DUP
95979 Matrix:
9/21/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.064 mg/Kg - dry 0.002 0.021Acetone 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.021
Acrolein 1 09/22/23 21:56 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 09/22/23 21:56 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 09/22/23 21:56 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 09/22/23 21:56 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010
Bromomethane 1 09/22/23 21:56 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 09/22/23 21:56 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 09/22/23 21:56 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 09/22/23 21:56 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 09/22/23 21:56 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 09/22/23 21:56 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 09/22/23 21:56 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 09/22/23 21:56 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 09/22/23 21:56 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0052-Chlorotoluene 1 09/22/23 21:56 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 09/22/23 21:56 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 09/22/23 21:56 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-DUP
95979 Matrix:
9/21/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 09/22/23 21:56 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,2-Dibromoethane 1 09/22/23 21:56 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 09/22/23 21:56 V38309TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 09/22/23 21:56 V38309TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 09/22/23 21:56 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,4-Dichlorobenzene 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 09/22/23 21:56 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 09/22/23 21:56 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 09/22/23 21:56 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.005cis-1,2-Dichloroethene 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 09/22/23 21:56 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 09/22/23 21:56 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 09/22/23 21:56 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 09/22/23 21:56 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 09/22/23 21:56 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 09/22/23 21:56 V38309TBL
<0.015 mg/Kg - dry 0.015 0.268Ethanol 1 09/22/23 21:56 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 09/22/23 21:56 V38309TBL
<0.0009 mg/Kg - dry 0.0009 0.053Ethyl Tertiary Butyl Ether (ETBE)1 09/22/23 21:56 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.010Hexachlorobutadiene 1 09/22/23 21:56 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-DUP
95979 Matrix:
9/21/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
0.005 J mg/Kg - dry 0.0007 0.010n-Hexane 1 09/22/23 21:56 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.021
2-Hexanone 1 09/22/23 21:56 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 09/22/23 21:56 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 09/22/23 21:56 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 09/22/23 21:56 V38309TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 09/22/23 21:56 V38309TBL
0.006 J mg/Kg - dry 0.001 0.010Methylene Chloride 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010
Naphthalene 1 09/22/23 21:56 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 09/22/23 21:56 V38309TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 09/22/23 21:56 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 09/22/23 21:56 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 09/22/23 21:56 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 09/22/23 21:56 V38309TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 09/22/23 21:56 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 09/22/23 21:56 V38309TBL
<0.0010 mg/Kg - dry 0.0010 0.005Trichloroethene 1 09/22/23 21:56 V38309TBL
<0.002 mg/Kg - dry 0.002 0.010Trichlorofluoromethane 1 09/22/23 21:56 V38309TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 09/22/23 21:56 V38309TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-DUP
95979 Matrix:
9/21/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38308 09/22/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 09/22/23 21:56 V38309TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 09/22/23 21:56 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 09/22/23 21:56 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 09/22/23 21:56 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 09/22/23 21:56 V38309TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 09/22/23 21:56 V38309TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 09/22/23 21:56 V38309
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%09/22/23 21:561 TBL V38309
Surrogate: Dibromofluoromethane 102 Limits: 84-123%09/22/23 21:561 TBL V38309
Surrogate: Toluene-d8 98.8 Limits: 76-129%09/22/23 21:561 TBL V38309
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.124 mg/Kg - dry 0.124 0.707Acenaphthene 1 09/26/23 20:36 V38347AMP
<0.112 mg/Kg - dry 0.112 0.707Acenaphthylene 1 09/26/23 20:36 V38347AMP
<0.163 mg/Kg - dry 0.163 0.707Aniline 1 09/26/23 20:36 V38347AMP
0.336 J mg/Kg - dry 0.153 0.707Anthracene 1 09/26/23 20:36 V38347AMP
0.669 J
mg/Kg - dry 0.149 0.707
Benzo(a)anthracene 1 09/26/23 20:36 V38347AMP
0.668 J mg/Kg - dry 0.157 0.707Benzo(a)pyrene 1 09/26/23 20:36 V38347AMP
0.969 mg/Kg - dry 0.156 0.707Benzo(b)fluoranthene 1 09/26/23 20:36 V38347AMP
0.468 J mg/Kg - dry 0.145 0.707Benzo(g,h,i)perylene 1 09/26/23 20:36 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-DUP
95979 Matrix:
9/21/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
0.265 J mg/Kg - dry 0.146 0.707Benzo(k)fluoranthene 1 09/26/23 20:36 V38347AMP
<0.622 mg/Kg - dry 0.622 2.15
Benzoic Acid 1 09/26/23 20:36 V38347AMP
<0.112 mg/Kg - dry 0.112 0.707Benzyl alcohol 1 09/26/23 20:36 V38347AMP
<0.126 mg/Kg - dry 0.126 0.707Bis(2-Chloroethoxy)methane 1 09/26/23 20:36 V38347AMP
<0.114 mg/Kg - dry 0.114 0.707Bis(2-Chloroethyl)ether 1 09/26/23 20:36 V38347AMP
<0.145 mg/Kg - dry 0.145 0.353Bis(2-Chloroisopropyl)ether 1 09/26/23 20:36 V38347AMP
<0.128 mg/Kg - dry 0.128 0.707Bis(2-ethylhexyl)phthalate 1 09/26/23 20:36 V38347AMP
<0.116 mg/Kg - dry 0.116 0.7074-Bromophenyl phenyl ether 1 09/26/23 20:36 V38347AMP
<0.121 mg/Kg - dry 0.121 0.353
Butyl benzyl phthalate 1 09/26/23 20:36 V38347AMP
<0.099 mg/Kg - dry 0.099 0.7074-Chloro-3-methylphenol 1 09/26/23 20:36 V38347AMP
<0.120 mg/Kg - dry 0.120 0.3534-Chloroaniline 1 09/26/23 20:36 V38347AMP
<0.124 mg/Kg - dry 0.124 0.7072-Chloronaphthalene 1 09/26/23 20:36 V38347AMP
<0.105 mg/Kg - dry 0.105 0.7072-Chlorophenol 1 09/26/23 20:36 V38347AMP
<0.135 mg/Kg - dry 0.135 1.074-Chlorophenyl phenyl ether 1 09/26/23 20:36 V38347AMP
0.651 J mg/Kg - dry 0.152 0.707Chrysene 1 09/26/23 20:36 V38347AMP
<0.246 mg/Kg - dry 0.246 0.707Dibenz(a,h)anthracene 1 09/26/23 20:36 V38347AMP
<0.127 mg/Kg - dry 0.127 0.707Dibenzofuran 1 09/26/23 20:36 V38347AMP
<0.101 mg/Kg - dry 0.101 0.7071,2-Dichlorobenzene 1 09/26/23 20:36 V38347AMP
<0.104 mg/Kg - dry 0.104 0.7071,3-Dichlorobenzene 1 09/26/23 20:36 V38347AMP
<0.104 mg/Kg - dry 0.104 0.3531,4-Dichlorobenzene 1 09/26/23 20:36 V38347AMP
<0.157 mg/Kg - dry 0.157 0.7073,3'-Dichlorobenzidine 1 09/26/23 20:36 V38347AMP
<0.102 mg/Kg - dry 0.102 0.7072,4-Dichlorophenol 1 09/26/23 20:36 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-DUP
95979 Matrix:
9/21/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.193 mg/Kg - dry 0.193 0.707Diethyl phthalate 1 09/26/23 20:36 V38347AMP
<0.186 mg/Kg - dry 0.186 0.707
Dimethyl phthalate 1 09/26/23 20:36 V38347AMP
<0.115 mg/Kg - dry 0.115 0.3532,4-Dimethylphenol 1 09/26/23 20:36 V38347AMP
<0.114 mg/Kg - dry 0.114 0.707Di-n-butyl phthalate 1 09/26/23 20:36 V38347AMP
<0.257 mg/Kg - dry 0.257 1.614,6-Dinitro-2-methylphenol 1 09/26/23 20:36 V38347AMP
<0.557 mg/Kg - dry 0.557 1.612,4-Dinitrophenol 1 09/26/23 20:36 V38347AMP
<0.103 mg/Kg - dry 0.103 0.7072,4-Dinitrotoluene 1 09/26/23 20:36 V38347AMP
<0.115 mg/Kg - dry 0.115 0.7072,6-Dinitrotoluene 1 09/26/23 20:36 V38347AMP
<0.153 mg/Kg - dry 0.153 0.353
Di-n-Octyl Phthalate 1 09/26/23 20:36 V38347AMP
1.38 mg/Kg - dry 0.131 0.707Fluoranthene 1 09/26/23 20:36 V38347AMP
<0.137 mg/Kg - dry 0.137 0.707Fluorene 1 09/26/23 20:36 V38347AMP
<0.113 mg/Kg - dry 0.113 0.707Hexachlorobenzene 1 09/26/23 20:36 V38347AMP
<0.104 mg/Kg - dry 0.104 0.707Hexachlorobutadiene 1 09/26/23 20:36 V38347AMP
<0.168 mg/Kg - dry 0.168 0.707Hexachlorocyclopentadiene 1 09/26/23 20:36 V38347AMP
<0.084 mg/Kg - dry 0.084 0.707Hexachloroethane 1 09/26/23 20:36 V38347AMP
0.489 J mg/Kg - dry 0.191 0.707Indeno(1,2,3-cd)pyrene 1 09/26/23 20:36 V38347AMP
<0.204 mg/Kg - dry 0.204 0.707Isophorone 1 09/26/23 20:36 V38347AMP
0.117 J mg/Kg - dry 0.113 0.7071-Methylnaphthalene 1 09/26/23 20:36 V38347AMP
0.160 J mg/Kg - dry 0.107 0.7072-Methylnaphthalene 1 09/26/23 20:36 V38347AMP
<0.104 mg/Kg - dry 0.104 0.7072-Methylphenol 1 09/26/23 20:36 V38347AMP
<0.091 mg/Kg - dry 0.091 0.7073&4 Methylphenol 1 09/26/23 20:36 V38347AMP
<0.154 mg/Kg - dry 0.154 0.707Naphthalene 1 09/26/23 20:36 V38347AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 93
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-265-0002
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 09/21/2023
POR-001
Revised Report Date: 11/20/2023
Original Report Date : 10/04/2023
Sample ID :
Lab No :
Sampled:FG-DUP
95979 Matrix:
9/21/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38274 09/25/23 12:00
<0.103 mg/Kg - dry 0.103 0.7072-Nitroaniline 1 09/26/23 20:36 V38347AMP
<0.128 mg/Kg - dry 0.128 0.707
3-Nitroaniline 1 09/26/23 20:36 V38347AMP
<0.100 mg/Kg - dry 0.100 0.3534-Nitroaniline 1 09/26/23 20:36 V38347AMP
<0.124 mg/Kg - dry 0.124 0.353Nitrobenzene 1 09/26/23 20:36 V38347AMP
<0.095 mg/Kg - dry 0.095 0.7072-Nitrophenol 1 09/26/23 20:36 V38347AMP
<0.125 mg/Kg - dry 0.125 0.7074-Nitrophenol 1 09/26/23 20:36 V38347AMP
<0.282 mg/Kg - dry 0.282 0.707N-Nitrosodimethylamine 1 09/26/23 20:36 V38347AMP
<0.194 mg/Kg - dry 0.194 0.707N-Nitrosodiphenylamine 1 09/26/23 20:36 V38347AMP
<0.126 mg/Kg - dry 0.126 0.707
N-Nitroso-di-n-propylamine 1 09/26/23 20:36 V38347AMP
<0.372 mg/Kg - dry 0.372 1.07Pentachlorophenol 1 09/26/23 20:36 V38347AMP
1.14 mg/Kg - dry 0.223 0.707Phenanthrene 1 09/26/23 20:36 V38347AMP
<0.120 mg/Kg - dry 0.120 0.707Phenol 1 09/26/23 20:36 V38347AMP
1.31 mg/Kg - dry 0.143 0.707Pyrene 1 09/26/23 20:36 V38347AMP
<0.084 mg/Kg - dry 0.084 0.353Pyridine 1 09/26/23 20:36 V38347AMP
<0.114 mg/Kg - dry 0.114 0.7071,2,4-Trichlorobenzene 1 09/26/23 20:36 V38347AMP
<0.103 mg/Kg - dry 0.103 0.7072,4,5-Trichlorophenol 1 09/26/23 20:36 V38347AMP
<0.103 mg/Kg - dry 0.103 0.7072,4,6-Trichlorophenol 1 09/26/23 20:36 V38347AMP
8270ESurrogate: Phenol-d5 66.5 Limits: 34-121%09/26/23 20:361 AMP
Surrogate: 2-Fluorobiphenyl 80.2 Limits: 44-115%09/26/23 20:361 AMP V38347
Surrogate: 2-Fluorophenol 70.4 Limits: 35-115%09/26/23 20:361 AMP V38347
Surrogate: Nitrobenzene-d5 74.3 Limits: 37-122%09/26/23 20:361 AMP V38347
Surrogate: 4-Terphenyl-d14 85.6 Limits: 54-127%09/26/23 20:361 AMP V38347
Surrogate: 2,4,6-Tribromophenol 71.3 Limits: 39-132%09/26/23 20:361 AMP V38347
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 66 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Metals Analyses
6020B
L707915QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L707346
Associated Lab Samples: 95973, 95974, 95975, 95976, 95977, 95978, 95979
LRB-L707346 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/29/23 14:580.2500.0855<0.0855mg/KgArsenic
09/29/23 14:580.2500.042<0.042mg/KgBarium
09/29/23 14:580.2500.0260<0.0260mg/KgCadmium
09/29/23 14:580.2500.116<0.116mg/KgChromium
09/29/23 14:580.2500.0310<0.0310mg/KgLead
09/29/23 14:580.2500.103<0.103mg/KgSelenium
09/29/23 14:580.2500.0067<0.0067mg/KgSilver
LCS-L707346Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.02.342.50mg/KgArsenic 80-120
90.04.485.00mg/KgBarium 80-120
1010.5040.500mg/KgCadmium 80-120
97.04.855.00mg/KgChromium 80-120
97.02.422.50mg/KgLead 80-120
96.04.825.00mg/KgSelenium 80-120
1010.5040.500mg/KgSilver 80-120
V 95419-MS-L707346 V 95419-MSD-L707346Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
5.78 1234.092.302.402.82mg/KgArsenic 55.0*75-125 34.2 80
35.3 0.0*34.64.594.8152.1mg/KgBarium 0.0*75-125 2.0 80
0.616 1080.5710.4590.4810.0946mg/KgCadmium 104 75-125 7.5 80
21.4 0.0*18.64.594.8133.1mg/KgChromium 0.0*75-125 14.0 80
Page 1 of 25* QC Fail Date:11/20/2023 10:29 AM
Page 67 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Metals Analyses
6020B
L707915QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L707346
V 95419-MS-L707346 V 95419-MSD-L707346Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
11.0 25.0*10.52.302.4010.4mg/KgLead 4.0*75-125 4.6 80
4.67 82.04.394.594.810.724mg/KgSelenium 80.0 75-125 6.1 80
0.466 86.00.4560.4590.4810.0520mg/KgSilver 88.0 75-125 2.1 80
V 95419-PDS-L707346Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/29/23 15:5994.01.43mg/KgArsenic
09/29/23 15:5981.06.24mg/KgBarium
09/29/23 15:591020.262mg/KgCadmium
09/29/23 15:5984.04.85mg/KgChromium
09/29/23 15:5989.02.03mg/KgLead
09/29/23 15:5997.02.47mg/KgSelenium
09/29/23 15:5999.00.251mg/KgSilver
Page 2 of 25* QC Fail Date:11/20/2023 10:29 AM
Page 68 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V38344QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V38283
Associated Lab Samples: 95973, 95974
LRB-V38283 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/26/23 10:240.03000.0120<0.0120mg/KgMercury (Total)
LCS-V38283Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1130.4700.417mg/KgMercury (Total)80-120
V 95748-MS-V38283 V 95748-MSD-V38283Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.187 46.0*0.2200.3970.410<0.0120mg/KgMercury (Total)55.0*80-120 16.2 20
V 95748-PDS-V38283Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/26/23 10:3419.0*0.0393mg/KgMercury (Total)
Page 3 of 25* QC Fail Date:11/20/2023 10:29 AM
Page 69 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V38459QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V38431
Associated Lab Samples: 95975, 95976, 95977, 95978, 95979
LRB-V38431 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/28/23 14:100.03000.0120<0.0120mg/KgMercury (Total)
LCS-V38431Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.00.3990.417mg/KgMercury (Total)80-120
V 95979-MS-V38431 V 95979-MSD-V38431Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.493 90.00.5390.4170.4170.116mg/KgMercury (Total)102 80-120 8.9 20
V 95979-PDS-V38431Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/28/23 14:2998.01.31mg/KgMercury (Total)
Page 4 of 25Date:11/20/2023 10:29 AM
Page 70 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38309QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38308
Associated Lab Samples: 95973, 95974, 95975, 95976, 95978, 95979
LRB-V38308 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/22/23 17:520.0200.002<0.002mg/KgAcetone
09/22/23 17:520.0200.001<0.001mg/KgAcrolein
09/22/23 17:520.0200.0008<0.0008mg/KgAcrylonitrile
09/22/23 17:520.0050.0006<0.0006mg/KgBenzene
09/22/23 17:520.0050.0005<0.0005mg/KgBromobenzene
09/22/23 17:520.0050.0008<0.0008mg/KgBromochloromethane
09/22/23 17:520.0050.001<0.001mg/KgBromodichloromethane
09/22/23 17:520.0050.001<0.001mg/KgBromoform
09/22/23 17:520.0100.001<0.001mg/KgBromomethane
09/22/23 17:520.0050.0005<0.0005mg/Kgn-Butylbenzene
09/22/23 17:520.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/22/23 17:520.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/22/23 17:520.0050.0006<0.0006mg/KgCarbon Disulfide
09/22/23 17:520.0050.001<0.001mg/KgCarbon Tetrachloride
09/22/23 17:520.0050.0007<0.0007mg/KgChlorobenzene
09/22/23 17:520.0050.0009<0.0009mg/KgChlorodibromomethane
09/22/23 17:520.0100.0009<0.0009mg/KgChloroethane
09/22/23 17:520.0050.001<0.001mg/KgChloroform
09/22/23 17:520.0100.0006<0.0006mg/KgChloromethane
09/22/23 17:520.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/22/23 17:520.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/22/23 17:520.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/22/23 17:520.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/22/23 17:520.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/22/23 17:520.0050.0006<0.0006mg/KgDibromomethane
09/22/23 17:520.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/22/23 17:520.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 5 of 25Date:11/20/2023 10:29 AM
Page 71 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38309QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38308
Associated Lab Samples: 95973, 95974, 95975, 95976, 95978, 95979
LRB-V38308 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/22/23 17:520.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/22/23 17:520.0100.001<0.001mg/KgDichlorodifluoromethane
09/22/23 17:520.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/22/23 17:520.0050.001<0.001mg/Kg1,2-Dichloroethane
09/22/23 17:520.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/22/23 17:520.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/22/23 17:520.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/22/23 17:520.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/22/23 17:520.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/22/23 17:520.0050.001<0.001mg/Kg2,2-Dichloropropane
09/22/23 17:520.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/22/23 17:520.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/22/23 17:520.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/22/23 17:520.2500.014<0.014mg/KgEthanol
09/22/23 17:520.0050.0006<0.0006mg/KgEthylbenzene
09/22/23 17:520.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/22/23 17:520.0100.0008<0.0008mg/KgHexachlorobutadiene
09/22/23 17:520.0100.0007<0.0007mg/Kgn-Hexane
09/22/23 17:520.0200.0006<0.0006mg/Kg2-Hexanone
09/22/23 17:520.0050.0005<0.0005mg/KgIsopropylbenzene
09/22/23 17:520.0050.001<0.001mg/Kg4-Isopropyl toluene
09/22/23 17:520.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/22/23 17:520.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/22/23 17:520.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/22/23 17:520.0100.001<0.001mg/KgMethylene Chloride
09/22/23 17:520.0100.0010<0.0010mg/KgNaphthalene
09/22/23 17:520.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 6 of 25Date:11/20/2023 10:29 AM
Page 72 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38309QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38308
Associated Lab Samples: 95973, 95974, 95975, 95976, 95978, 95979
LRB-V38308 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/22/23 17:520.0050.001<0.001mg/KgStyrene
09/22/23 17:520.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/22/23 17:520.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/22/23 17:520.0050.0009<0.0009mg/KgTetrachloroethene
09/22/23 17:520.0050.0007<0.0007mg/KgToluene
09/22/23 17:520.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/22/23 17:520.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/22/23 17:520.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/22/23 17:520.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/22/23 17:520.0050.0009<0.0009mg/KgTrichloroethene
09/22/23 17:520.0100.002<0.002mg/KgTrichlorofluoromethane
09/22/23 17:520.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/22/23 17:520.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
09/22/23 17:520.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/22/23 17:520.0100.0005<0.0005mg/KgVinyl Acetate
09/22/23 17:520.0100.0005<0.0005mg/KgVinyl Chloride
09/22/23 17:520.0050.0005<0.0005mg/Kgo-Xylene
09/22/23 17:520.0100.001<0.001mg/Kgm,p-Xylene
09/22/23 17:524-Bromofluorobenzene (S)99.8 70-130
09/22/23 17:52Dibromofluoromethane (S)96.8 84-123
09/22/23 17:52Toluene-d8 (S)102 76-129
LCS-V38308 LCSD-V38308Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.097 97.791.70.0910.100mg/KgAcetone 29-198 6.3 20
Page 7 of 25Date:11/20/2023 10:29 AM
Page 73 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38309QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38308
LCS-V38308 LCSD-V38308Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.109 1091060.1060.100mg/KgAcrolein 70-130 2.7 20
0.108 1081060.1060.100mg/KgAcrylonitrile 65-134 1.8 20
0.045 90.696.80.0480.050mg/KgBenzene 74-127 6.6 20
0.048 96.21030.0510.050mg/KgBromobenzene 73-125 6.4 20
0.045 90.894.20.0470.050mg/KgBromochloromethane 72-134 3.6 20
0.045 91.294.20.0470.050mg/KgBromodichloromethane 75-122 3.2 20
0.048 96.296.60.0480.050mg/KgBromoform 66-135 0.4 20
0.044 88.41010.0500.050mg/KgBromomethane 20-180 13.1 20
0.048 96.01060.0530.050mg/Kgn-Butylbenzene 65-135 10.0 20
0.045 90.61010.0500.050mg/Kgsec-Butyl benzene 66-131 10.4 20
0.045 90.299.60.0490.050mg/Kgtert-Butyl benzene 67-132 9.9 20
0.044 89.299.40.0490.050mg/KgCarbon Disulfide 61-129 10.8 20
0.042 85.694.20.0470.050mg/KgCarbon Tetrachloride 64-143 9.5 20
0.046 92.296.80.0480.050mg/KgChlorobenzene 74-118 4.8 20
0.047 95.095.60.0470.050mg/KgChlorodibromomethane 73-122 0.6 20
0.044 89.897.80.0480.050mg/KgChloroethane 33-149 8.5 20
0.044 88.493.00.0460.050mg/KgChloroform 73-127 5.0 20
0.045 90.21040.0520.050mg/KgChloromethane 45-143 14.5 20
0.045 91.299.60.0490.050mg/Kg2-Chlorotoluene 67-124 8.8 20
0.045 91.299.60.0490.050mg/Kg4-Chlorotoluene 71-126 8.8 20
0.047 94.099.60.0490.050mg/KgDi-Isopropyl Ether (DIPE)59-159 5.7 20
0.051 1031020.0500.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.3 20
0.050 10199.20.0490.050mg/Kg1,2-Dibromoethane 70-132 1.7 20
0.049 98.099.20.0490.050mg/KgDibromomethane 74-133 1.2 20
0.046 93.898.20.0490.050mg/Kg1,2-Dichlorobenzene 72-123 4.5 20
0.046 93.699.60.0490.050mg/Kg1,3-Dichlorobenzene 71-120 6.2 20
Page 8 of 25Date:11/20/2023 10:29 AM
Page 74 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38309QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38308
LCS-V38308 LCSD-V38308Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 90.696.80.0480.050mg/Kg1,4-Dichlorobenzene 71-123 6.6 20
0.038 77.687.00.0430.050mg/KgDichlorodifluoromethane 26-146 11.4 20
0.045 91.497.20.0480.050mg/Kg1,1-Dichloroethane 74-127 6.1 20
0.045 91.692.40.0460.050mg/Kg1,2-Dichloroethane 68-128 0.8 20
0.044 89.299.20.0490.050mg/Kg1,1-Dichloroethene 67-149 10.6 20
0.046 92.497.20.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 5.0 20
0.046 92.41030.0510.050mg/Kgtrans-1,2-Dichloroethene 73-132 10.6 20
0.047 95.01000.0500.050mg/Kg1,2-Dichloropropane 73-130 5.1 20
0.049 98.498.80.0490.050mg/Kg1,3-Dichloropropane 75-124 0.4 20
0.043 87.096.80.0480.050mg/Kg2,2-Dichloropropane 50-142 10.6 20
0.045 91.098.40.0490.050mg/Kg1,1-Dichloropropene 71-130 7.8 20
0.048 96.21010.0500.050mg/Kgcis-1,3-Dichloropropene 71-125 4.4 20
0.050 1001030.0510.050mg/Kgtrans-1,3-Dichloropropene 68-123 3.1 20
1.38 1101011.261.25mg/KgEthanol 70-130 9.0 20
0.045 90.097.40.0480.050mg/KgEthylbenzene 74-128 7.8 20
0.092 92.793.50.0930.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.8 20
0.045 90.41010.0500.050mg/KgHexachlorobutadiene 64-125 10.8 20
0.047 94.41070.0530.050mg/Kgn-Hexane 70-130 12.5 20
0.048 96.490.80.0450.050mg/Kg2-Hexanone 61-157 5.9 20
0.045 90.21000.0500.050mg/KgIsopropylbenzene 68-126 10.7 20
0.045 91.41010.0500.050mg/Kg4-Isopropyl toluene 68-129 10.1 20
0.041 82.678.00.0390.050mg/KgMethyl Ethyl Ketone (MEK)63-149 5.7 20
0.045 91.893.40.0460.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.7 20
0.048 96.81010.0500.050mg/Kg4-Methyl-2-Pentanone 57-162 4.4 20
0.043 86.491.00.0450.050mg/KgMethylene Chloride 74-129 5.1 20
0.048 96.61010.0500.050mg/KgNaphthalene 57-157 4.6 20
Page 9 of 25Date:11/20/2023 10:29 AM
Page 75 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38309QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38308
LCS-V38308 LCSD-V38308Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.046 92.61040.0510.050mg/Kgn-Propylbenzene 67-130 11.2 20
0.049 98.01020.0510.050mg/KgStyrene 77-121 4.3 20
0.045 90.893.20.0460.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 2.6 20
0.049 99.21010.0500.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.6 20
0.041 83.892.80.0460.050mg/KgTetrachloroethene 68-130 10.1 20
0.044 88.695.60.0470.050mg/KgToluene 71-129 7.6 20
0.047 95.21030.0510.050mg/Kg1,2,3-Trichlorobenzene 68-130 8.2 20
0.048 97.81050.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 6.7 20
0.042 85.093.20.0460.050mg/Kg1,1,1-Trichloroethane 67-131 9.2 20
0.048 97.897.20.0480.050mg/Kg1,1,2-Trichloroethane 70-133 0.6 20
0.044 89.695.00.0470.050mg/KgTrichloroethene 75-133 5.8 20
0.039 78.688.40.0440.050mg/KgTrichlorofluoromethane 44-146 11.7 20
0.047 95.096.60.0480.050mg/Kg1,2,3-Trichloropropane 60-137 1.6 20
0.046 92.81020.0510.050mg/Kg1,2,4-Trimethylbenzene 69-129 9.4 20
0.046 92.81020.0500.050mg/Kg1,3,5-Trimethylbenzene 69-128 9.2 20
0.046 92.21070.0530.050mg/KgVinyl Acetate 60-140 14.6 20
0.043 86.897.80.0480.050mg/KgVinyl Chloride 48-147 11.9 20
0.047 94.499.80.0490.050mg/Kgo-Xylene 74-126 5.5 20
0.092 92.299.20.0990.100mg/Kgm,p-Xylene 75-124 7.3 20
98.61004-Bromofluorobenzene (S)70-130
98.497.0Dibromofluoromethane (S)84-123
103103Toluene-d8 (S)76-129
Page 10 of 25Date:11/20/2023 10:29 AM
Page 76 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38313QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38312
Associated Lab Samples: 95977
LRB-V38312 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/25/23 17:200.0200.002<0.002mg/KgAcetone
09/25/23 17:200.0200.001<0.001mg/KgAcrolein
09/25/23 17:200.0200.0008<0.0008mg/KgAcrylonitrile
09/25/23 17:200.0050.0006<0.0006mg/KgBenzene
09/25/23 17:200.0050.0005<0.0005mg/KgBromobenzene
09/25/23 17:200.0050.0008<0.0008mg/KgBromochloromethane
09/25/23 17:200.0050.001<0.001mg/KgBromodichloromethane
09/25/23 17:200.0050.001<0.001mg/KgBromoform
09/25/23 17:200.0100.001<0.001mg/KgBromomethane
09/25/23 17:200.0050.0005<0.0005mg/Kgn-Butylbenzene
09/25/23 17:200.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/25/23 17:200.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/25/23 17:200.0050.0006<0.0006mg/KgCarbon Disulfide
09/25/23 17:200.0050.001<0.001mg/KgCarbon Tetrachloride
09/25/23 17:200.0050.0007<0.0007mg/KgChlorobenzene
09/25/23 17:200.0050.0009<0.0009mg/KgChlorodibromomethane
09/25/23 17:200.0100.0009<0.0009mg/KgChloroethane
09/25/23 17:200.0050.001<0.001mg/KgChloroform
09/25/23 17:200.0100.0006<0.0006mg/KgChloromethane
09/25/23 17:200.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/25/23 17:200.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/25/23 17:200.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/25/23 17:200.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/25/23 17:200.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/25/23 17:200.0050.0006<0.0006mg/KgDibromomethane
09/25/23 17:200.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/25/23 17:200.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 11 of 25Date:11/20/2023 10:29 AM
Page 77 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38313QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38312
Associated Lab Samples: 95977
LRB-V38312 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/25/23 17:200.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/25/23 17:200.0100.001<0.001mg/KgDichlorodifluoromethane
09/25/23 17:200.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/25/23 17:200.0050.001<0.001mg/Kg1,2-Dichloroethane
09/25/23 17:200.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/25/23 17:200.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/25/23 17:200.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/25/23 17:200.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/25/23 17:200.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/25/23 17:200.0050.001<0.001mg/Kg2,2-Dichloropropane
09/25/23 17:200.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/25/23 17:200.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/25/23 17:200.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/25/23 17:200.2500.014<0.014mg/KgEthanol
09/25/23 17:200.0050.0006<0.0006mg/KgEthylbenzene
09/25/23 17:200.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/25/23 17:200.0100.0008<0.0008mg/KgHexachlorobutadiene
09/25/23 17:200.0100.0007<0.0007mg/Kgn-Hexane
09/25/23 17:200.0200.0006<0.0006mg/Kg2-Hexanone
09/25/23 17:200.0050.0005<0.0005mg/KgIsopropylbenzene
09/25/23 17:200.0050.001<0.001mg/Kg4-Isopropyl toluene
09/25/23 17:200.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/25/23 17:200.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/25/23 17:200.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/25/23 17:200.0100.001<0.001mg/KgMethylene Chloride
09/25/23 17:200.0100.0010<0.0010mg/KgNaphthalene
09/25/23 17:200.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 12 of 25Date:11/20/2023 10:29 AM
Page 78 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38313QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38312
Associated Lab Samples: 95977
LRB-V38312 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/25/23 17:200.0050.001<0.001mg/KgStyrene
09/25/23 17:200.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/25/23 17:200.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/25/23 17:200.0050.0009<0.0009mg/KgTetrachloroethene
09/25/23 17:200.0050.0007<0.0007mg/KgToluene
09/25/23 17:200.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/25/23 17:200.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/25/23 17:200.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/25/23 17:200.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/25/23 17:200.0050.0009<0.0009mg/KgTrichloroethene
09/25/23 17:200.0100.002<0.002mg/KgTrichlorofluoromethane
09/25/23 17:200.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/25/23 17:200.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
09/25/23 17:200.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/25/23 17:200.0100.0005<0.0005mg/KgVinyl Acetate
09/25/23 17:200.0100.0005<0.0005mg/KgVinyl Chloride
09/25/23 17:200.0050.0005<0.0005mg/Kgo-Xylene
09/25/23 17:200.0100.001<0.001mg/Kgm,p-Xylene
09/25/23 17:204-Bromofluorobenzene (S)99.4 70-130
09/25/23 17:20Dibromofluoromethane (S)96.8 84-123
09/25/23 17:20Toluene-d8 (S)100 76-129
LCS-V38312 LCSD-V38312Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.107 1071140.1140.100mg/KgAcetone 29-198 6.3 20
Page 13 of 25Date:11/20/2023 10:29 AM
Page 79 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38313QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38312
LCS-V38312 LCSD-V38312Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.104 1041050.1050.100mg/KgAcrolein 70-130 0.9 20
0.101 10197.00.0970.100mg/KgAcrylonitrile 65-134 4.0 20
0.045 90.693.80.0460.050mg/KgBenzene 74-127 3.4 20
0.044 89.495.40.0470.050mg/KgBromobenzene 73-125 6.4 20
0.048 96.899.20.0490.050mg/KgBromochloromethane 72-134 2.4 20
0.051 10299.20.0490.050mg/KgBromodichloromethane 75-122 3.1 20
0.052 1061120.0560.050mg/KgBromoform 66-135 5.6 20
0.050 1011070.0530.050mg/KgBromomethane 20-180 5.7 20
0.047 95.41040.0520.050mg/Kgn-Butylbenzene 65-135 9.0 20
0.044 89.096.20.0480.050mg/Kgsec-Butyl benzene 66-131 7.7 20
0.044 88.897.20.0480.050mg/Kgtert-Butyl benzene 67-132 9.0 20
0.044 88.695.80.0470.050mg/KgCarbon Disulfide 61-129 7.8 20
0.048 97.01030.0510.050mg/KgCarbon Tetrachloride 64-143 5.6 20
0.051 1021020.0500.050mg/KgChlorobenzene 74-118 0.5 20
0.050 1011040.0520.050mg/KgChlorodibromomethane 73-122 3.5 20
0.049 98.01040.0520.050mg/KgChloroethane 33-149 6.3 20
0.046 93.495.80.0470.050mg/KgChloroform 73-127 2.5 20
0.043 87.690.00.0450.050mg/KgChloromethane 45-143 2.7 20
0.044 88.094.60.0470.050mg/Kg2-Chlorotoluene 67-124 7.2 20
0.044 88.094.60.0470.050mg/Kg4-Chlorotoluene 71-126 7.2 20
0.044 88.490.40.0450.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.2 20
0.052 1051150.0570.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 9.1 20
0.050 1001070.0530.050mg/Kg1,2-Dibromoethane 70-132 6.7 20
0.052 1041020.0510.050mg/KgDibromomethane 74-133 2.1 20
0.047 94.81050.0520.050mg/Kg1,2-Dichlorobenzene 72-123 10.0 20
0.047 94.41060.0520.050mg/Kg1,3-Dichlorobenzene 71-120 11.2 20
Page 14 of 25Date:11/20/2023 10:29 AM
Page 80 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38313QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38312
LCS-V38312 LCSD-V38312Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.046 93.098.00.0490.050mg/Kg1,4-Dichlorobenzene 71-123 5.2 20
0.046 93.099.20.0490.050mg/KgDichlorodifluoromethane 26-146 6.4 20
0.044 89.294.00.0470.050mg/Kg1,1-Dichloroethane 74-127 5.2 20
0.049 99.899.40.0490.050mg/Kg1,2-Dichloroethane 68-128 0.4 20
0.044 88.493.40.0460.050mg/Kg1,1-Dichloroethene 67-149 5.5 20
0.045 90.091.60.0450.050mg/Kgcis-1,2-Dichloroethene 76-134 1.7 20
0.045 90.293.60.0460.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.6 20
0.050 10091.20.0450.050mg/Kg1,2-Dichloropropane 73-130 9.2 20
0.048 96.297.00.0480.050mg/Kg1,3-Dichloropropane 75-124 0.8 20
0.051 10299.20.0490.050mg/Kg2,2-Dichloropropane 50-142 2.7 20
0.046 92.095.20.0470.050mg/Kg1,1-Dichloropropene 71-130 3.4 20
0.048 97.897.80.0480.050mg/Kgcis-1,3-Dichloropropene 71-125 0.0 20
0.054 1091030.0510.050mg/Kgtrans-1,3-Dichloropropene 68-123 5.6 20
1.26 1011051.311.25mg/KgEthanol 70-130 3.8 20
0.047 95.698.60.0490.050mg/KgEthylbenzene 74-128 3.0 20
0.092 92.196.80.0960.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 4.9 20
0.049 98.41050.0520.050mg/KgHexachlorobutadiene 64-125 6.4 20
0.046 93.097.20.0480.050mg/Kgn-Hexane 70-130 4.4 20
0.044 88.697.40.0480.050mg/Kg2-Hexanone 61-157 9.4 20
0.044 89.497.60.0480.050mg/KgIsopropylbenzene 68-126 8.7 20
0.045 90.098.20.0490.050mg/Kg4-Isopropyl toluene 68-129 8.7 20
0.045 91.689.40.0440.050mg/KgMethyl Ethyl Ketone (MEK)63-149 2.4 20
0.048 97.895.80.0470.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.0 20
0.045 91.692.40.0460.050mg/Kg4-Methyl-2-Pentanone 57-162 0.8 20
0.042 84.686.20.0430.050mg/KgMethylene Chloride 74-129 1.8 20
0.050 1011040.0510.050mg/KgNaphthalene 57-157 2.7 20
Page 15 of 25Date:11/20/2023 10:29 AM
Page 81 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38313QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38312
LCS-V38312 LCSD-V38312Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 88.895.80.0470.050mg/Kgn-Propylbenzene 67-130 7.5 20
0.048 97.41060.0520.050mg/KgStyrene 77-121 8.0 20
0.049 98.41030.0510.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.5 20
0.046 93.695.60.0470.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.1 20
0.048 96.41030.0510.050mg/KgTetrachloroethene 68-130 6.4 20
0.048 96.894.80.0470.050mg/KgToluene 71-129 2.0 20
0.053 1071070.0530.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.1 20
0.053 1061100.0540.050mg/Kg1,2,4-Trichlorobenzene 66-125 3.1 20
0.046 93.01010.0500.050mg/Kg1,1,1-Trichloroethane 67-131 8.0 20
0.047 94.41020.0500.050mg/Kg1,1,2-Trichloroethane 70-133 7.3 20
0.047 95.699.00.0490.050mg/KgTrichloroethene 75-133 3.4 20
0.048 96.01050.0520.050mg/KgTrichlorofluoromethane 44-146 9.1 20
0.045 91.496.80.0480.050mg/Kg1,2,3-Trichloropropane 60-137 5.7 20
0.048 96.696.00.0480.050mg/Kg1,2,4-Trimethylbenzene 69-129 0.6 20
0.045 91.297.00.0480.050mg/Kg1,3,5-Trimethylbenzene 69-128 6.1 20
0.050 1011010.0500.050mg/KgVinyl Acetate 60-140 0.0 20
0.044 89.095.20.0470.050mg/KgVinyl Chloride 48-147 6.7 20
0.047 95.098.20.0490.050mg/Kgo-Xylene 74-126 3.3 20
0.091 91.798.80.0980.100mg/Kgm,p-Xylene 75-124 7.4 20
98.41034-Bromofluorobenzene (S)70-130
99.4100Dibromofluoromethane (S)84-123
94.898.2Toluene-d8 (S)76-129
Page 16 of 25Date:11/20/2023 10:29 AM
Page 82 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38347QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38274
Associated Lab Samples: 95973, 95974, 95975, 95976, 95977, 95978, 95979
LRB-V38274 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/26/23 14:110.6600.116<0.116mg/KgAcenaphthene
09/26/23 14:110.6600.105<0.105mg/KgAcenaphthylene
09/26/23 14:110.6600.152<0.152mg/KgAniline
09/26/23 14:110.6600.143<0.143mg/KgAnthracene
09/26/23 14:110.6600.139<0.139mg/KgBenzo(a)anthracene
09/26/23 14:110.6600.147<0.147mg/KgBenzo(a)pyrene
09/26/23 14:110.6600.146<0.146mg/KgBenzo(b)fluoranthene
09/26/23 14:110.6600.136<0.136mg/KgBenzo(g,h,i)perylene
09/26/23 14:110.6600.137<0.137mg/KgBenzo(k)fluoranthene
09/26/23 14:112.000.580<0.580mg/KgBenzoic Acid
09/26/23 14:110.6600.105<0.105mg/KgBenzyl alcohol
09/26/23 14:110.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
09/26/23 14:110.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
09/26/23 14:110.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
09/26/23 14:110.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
09/26/23 14:110.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
09/26/23 14:110.3300.113<0.113mg/KgButyl benzyl phthalate
09/26/23 14:110.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
09/26/23 14:110.3300.112<0.112mg/Kg4-Chloroaniline
09/26/23 14:110.6600.116<0.116mg/Kg2-Chloronaphthalene
09/26/23 14:110.6600.098<0.098mg/Kg2-Chlorophenol
09/26/23 14:111.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
09/26/23 14:110.6600.142<0.142mg/KgChrysene
09/26/23 14:110.6600.230<0.230mg/KgDibenz(a,h)anthracene
09/26/23 14:110.6600.119<0.119mg/KgDibenzofuran
09/26/23 14:110.6600.094<0.094mg/Kg1,2-Dichlorobenzene
09/26/23 14:110.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 17 of 25Date:11/20/2023 10:29 AM
Page 83 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38347QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38274
Associated Lab Samples: 95973, 95974, 95975, 95976, 95977, 95978, 95979
LRB-V38274 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/26/23 14:110.3300.097<0.097mg/Kg1,4-Dichlorobenzene
09/26/23 14:110.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
09/26/23 14:110.6600.095<0.095mg/Kg2,4-Dichlorophenol
09/26/23 14:110.6600.180<0.180mg/KgDiethyl phthalate
09/26/23 14:110.6600.174<0.174mg/KgDimethyl phthalate
09/26/23 14:110.3300.108<0.108mg/Kg2,4-Dimethylphenol
09/26/23 14:110.6600.107<0.107mg/KgDi-n-butyl phthalate
09/26/23 14:111.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
09/26/23 14:111.500.520<0.520mg/Kg2,4-Dinitrophenol
09/26/23 14:110.6600.096<0.096mg/Kg2,4-Dinitrotoluene
09/26/23 14:110.6600.108<0.108mg/Kg2,6-Dinitrotoluene
09/26/23 14:110.3300.143<0.143mg/KgDi-n-Octyl Phthalate
09/26/23 14:110.6600.123<0.123mg/KgFluoranthene
09/26/23 14:110.6600.128<0.128mg/KgFluorene
09/26/23 14:110.6600.106<0.106mg/KgHexachlorobenzene
09/26/23 14:110.6600.097<0.097mg/KgHexachlorobutadiene
09/26/23 14:110.6600.157<0.157mg/KgHexachlorocyclopentadiene
09/26/23 14:110.6600.079<0.079mg/KgHexachloroethane
09/26/23 14:110.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
09/26/23 14:110.6600.191<0.191mg/KgIsophorone
09/26/23 14:110.6600.106<0.106mg/Kg1-Methylnaphthalene
09/26/23 14:110.6600.100<0.100mg/Kg2-Methylnaphthalene
09/26/23 14:110.6600.097<0.097mg/Kg2-Methylphenol
09/26/23 14:110.6600.084<0.084mg/Kg3&4 Methylphenol
09/26/23 14:110.6600.144<0.144mg/KgNaphthalene
09/26/23 14:110.6600.096<0.096mg/Kg2-Nitroaniline
09/26/23 14:110.6600.120<0.120mg/Kg3-Nitroaniline
Page 18 of 25Date:11/20/2023 10:29 AM
Page 84 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38347QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38274
Associated Lab Samples: 95973, 95974, 95975, 95976, 95977, 95978, 95979
LRB-V38274 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/26/23 14:110.3300.093<0.093mg/Kg4-Nitroaniline
09/26/23 14:110.3300.116<0.116mg/KgNitrobenzene
09/26/23 14:110.6600.088<0.088mg/Kg2-Nitrophenol
09/26/23 14:110.6600.117<0.117mg/Kg4-Nitrophenol
09/26/23 14:110.6600.263<0.263mg/KgN-Nitrosodimethylamine
09/26/23 14:110.6600.181<0.181mg/KgN-Nitrosodiphenylamine
09/26/23 14:110.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
09/26/23 14:111.000.347<0.347mg/KgPentachlorophenol
09/26/23 14:110.6600.208<0.208mg/KgPhenanthrene
09/26/23 14:110.6600.112<0.112mg/KgPhenol
09/26/23 14:110.6600.134<0.134mg/KgPyrene
09/26/23 14:110.3300.079<0.079mg/KgPyridine
09/26/23 14:110.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
09/26/23 14:110.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
09/26/23 14:110.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
09/26/23 14:112-Fluorobiphenyl (S)76.6 44-115
09/26/23 14:112-Fluorophenol (S)68.1 35-115
09/26/23 14:11Nitrobenzene-d5 (S)71.8 37-122
09/26/23 14:114-Terphenyl-d14 (S)87.4 54-127
09/26/23 14:112,4,6-Tribromophenol (S)67.2 39-132
09/26/23 14:11Phenol-d5 (S)65.1 34-121
LCS-V38274 LCSD-V38274Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.42 85.084.41.411.67mg/KgAcenaphthene 40-123 0.7 20
Page 19 of 25Date:11/20/2023 10:29 AM
Page 85 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38347QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38274
LCS-V38274 LCSD-V38274Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.42 85.084.41.411.67mg/KgAcenaphthylene 32-132 0.7 20
3.81 228*224*3.741.67mg/KgAniline 12-197 1.8 20
1.58 94.692.81.551.67mg/KgAnthracene 47-123 1.9 20
1.56 93.489.21.491.67mg/KgBenzo(a)anthracene 49-126 4.5 20
1.71 1021001.671.67mg/KgBenzo(a)pyrene 45-129 2.3 20
1.63 97.695.21.591.67mg/KgBenzo(b)fluoranthene 45-132 2.4 20
1.47 88.086.81.451.67mg/KgBenzo(g,h,i)perylene 43-134 1.3 20
1.58 94.692.21.541.67mg/KgBenzo(k)fluoranthene 47-132 2.5 20
<0.580 0.0*0.0*<0.5801.67mg/KgBenzoic Acid 10-83 0.0 20
1.43 85.684.41.411.67mg/KgBenzyl alcohol 29-122 1.4 20
1.25 74.874.21.241.67mg/KgBis(2-Chloroethoxy)methane 36-121 0.8 20
1.33 79.678.41.311.67mg/KgBis(2-Chloroethyl)ether 31-120 1.5 20
1.36 81.480.21.341.67mg/KgBis(2-Chloroisopropyl)ether 33-131 1.4 20
1.60 95.891.61.531.67mg/KgBis(2-ethylhexyl)phthalate 51-133 4.4 20
1.52 91.090.41.511.67mg/Kg4-Bromophenyl phenyl ether 46-124 0.6 20
1.61 96.492.21.541.67mg/KgButyl benzyl phthalate 48-132 4.4 20
1.28 76.676.61.281.67mg/Kg4-Chloro-3-methylphenol 45-122 0.0 20
1.69 10198.81.651.67mg/Kg4-Chloroaniline 17-106 2.3 20
1.43 85.685.61.431.67mg/Kg2-Chloronaphthalene 41-114 0.0 20
1.42 85.083.81.401.67mg/Kg2-Chlorophenol 34-121 1.4 20
1.49 89.289.21.491.67mg/Kg4-Chlorophenyl phenyl ether 45-121 0.0 20
1.55 92.888.61.481.67mg/KgChrysene 50-124 4.6 20
1.16 69.467.01.121.67mg/KgDibenz(a,h)anthracene 45-134 3.5 20
1.42 85.083.21.391.67mg/KgDibenzofuran 44-120 2.1 20
1.26 75.474.81.251.67mg/Kg1,2-Dichlorobenzene 33-117 0.7 20
1.23 73.673.01.221.67mg/Kg1,3-Dichlorobenzene 30-115 0.8 20
Page 20 of 25* QC Fail Date:11/20/2023 10:29 AM
Page 86 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38347QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38274
LCS-V38274 LCSD-V38274Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.23 73.672.41.211.67mg/Kg1,4-Dichlorobenzene 31-115 1.6 20
1.42 85.080.81.351.67mg/Kg3,3'-Dichlorobenzidine 22-121 5.0 20
1.36 81.482.01.371.67mg/Kg2,4-Dichlorophenol 40-122 0.7 20
1.52 91.089.21.491.67mg/KgDiethyl phthalate 50-124 1.9 20
1.55 92.891.61.531.67mg/KgDimethyl phthalate 48-124 1.2 20
1.63 97.698.21.641.67mg/Kg2,4-Dimethylphenol 30-127 0.6 20
1.69 10198.21.641.67mg/KgDi-n-butyl phthalate 51-128 3.0 20
1.57 94.090.41.511.67mg/Kg4,6-Dinitro-2-methylphenol 29-132 3.8 20
0.891 53.349.50.8281.67mg/Kg2,4-Dinitrophenol 27-129 7.3 20
1.56 93.491.61.531.67mg/Kg2,4-Dinitrotoluene 48-126 1.9 20
1.54 92.289.21.491.67mg/Kg2,6-Dinitrotoluene 46-124 3.3 20
1.66 99.497.01.621.67mg/KgDi-n-Octyl Phthalate 45-140 2.4 20
1.44 86.284.41.411.67mg/KgFluoranthene 50-127 2.1 20
1.48 88.686.81.451.67mg/KgFluorene 43-125 2.0 20
1.53 91.689.81.501.67mg/KgHexachlorobenzene 45-122 1.9 20
1.20 71.871.21.191.67mg/KgHexachlorobutadiene 32-123 0.8 20
1.36 81.481.41.361.67mg/KgHexachlorocyclopentadiene 32-117 0.0 20
1.18 70.670.61.181.67mg/KgHexachloroethane 28-117 0.0 20
1.48 88.688.61.481.67mg/KgIndeno(1,2,3-cd)pyrene 45-133 0.0 20
1.15 68.868.21.141.67mg/KgIsophorone 30-122 0.8 20
1.15 68.869.41.161.67mg/Kg1-Methylnaphthalene 40-119 0.8 20
1.15 68.868.21.141.67mg/Kg2-Methylnaphthalene 38-122 0.8 20
1.45 86.886.21.441.67mg/Kg2-Methylphenol 32-122 0.6 20
1.29 77.276.01.271.67mg/Kg3&4 Methylphenol 34-119 1.5 20
1.16 69.469.41.161.67mg/KgNaphthalene 35-123 0.0 20
1.54 92.290.41.511.67mg/Kg2-Nitroaniline 44-127 1.9 20
Page 21 of 25Date:11/20/2023 10:29 AM
Page 87 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38347QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38274
LCS-V38274 LCSD-V38274Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.56 93.488.61.481.67mg/Kg3-Nitroaniline 33-119 5.2 20
1.56 93.489.21.491.67mg/Kg4-Nitroaniline 63-147 4.5 20
1.12 67.065.81.101.67mg/KgNitrobenzene 34-122 1.8 20
1.20 71.871.81.201.67mg/Kg2-Nitrophenol 36-123 0.0 20
1.56 93.492.81.551.67mg/Kg4-Nitrophenol 30-132 0.6 20
1.12 67.066.41.111.67mg/KgN-Nitrosodimethylamine 10-146 0.8 20
1.84 1101101.841.67mg/KgN-Nitrosodiphenylamine 38-127 0.0 20
1.33 79.677.81.301.67mg/KgN-Nitroso-di-n-propylamine 36-120 2.2 20
1.85 1111081.811.67mg/KgPentachlorophenol 25-133 2.1 20
1.52 91.089.81.501.67mg/KgPhenanthrene 50-121 1.3 20
1.35 80.879.61.331.67mg/KgPhenol 34-121 1.4 20
1.53 91.688.61.481.67mg/KgPyrene 47-127 3.3 20
0.931 55.754.10.9051.67mg/KgPyridine 10-80 2.8 20
1.16 69.468.81.151.67mg/Kg1,2,4-Trichlorobenzene 34-118 0.8 20
1.47 88.086.81.451.67mg/Kg2,4,5-Trichlorophenol 41-124 1.3 20
1.49 89.287.41.461.67mg/Kg2,4,6-Trichlorophenol 39-126 2.0 20
82.082.62-Fluorobiphenyl (S)44-115
72.372.32-Fluorophenol (S)35-115
64.665.8Nitrobenzene-d5 (S)37-122
89.888.04-Terphenyl-d14 (S)54-127
79.881.02,4,6-Tribromophenol (S)39-132
69.069.3Phenol-d5 (S)34-121
Page 22 of 25Date:11/20/2023 10:29 AM
Page 88 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L708430QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L707678
Associated Lab Samples: 95973, 95974, 95975, 95976, 95977, 95978, 95979
LRB-L707678 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/03/23 12:300.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L707678Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
97.03.884.00mg/KgChromium, Hexavalent 80-120
V 95976-DUP-L707678Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 10/03/23 13:0228.5*0.4570.343mg/KgChromium, Hexavalent
V 95976-MS-L707678Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
27.4 66.0*41.2< 1.45mg/KgChromium, Hexavalent 75-125
Page 23 of 25* QC Fail Date:11/20/2023 10:29 AM
Page 89 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
Dry Weight Determination
SW-DRYWT
V38196QC Analytical Batch:
Analysis Method:
Analysis Description:
V 95805-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/22/23 11:551.513.113.3%Moisture
V 95882-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/22/23 11:550.014.414.4%Moisture
Page 24 of 25Date:11/20/2023 10:29 AM
Page 90 of 93
Quality Control Data
23-265-0002Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
POR-001
Dry Weight Determination
SW-DRYWT
V38251QC Analytical Batch:
Analysis Method:
Analysis Description:
V 95996-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/25/23 10:401.125.625.3%Moisture
V 96069-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/25/23 10:405.123.822.6%Moisture
Page 25 of 25Date:11/20/2023 10:29 AM
Page 91 of 93
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-265-0002
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:09/22/2023 09:49:07
Special precautions or instructions included?
Comments:
Page 92 of 93
Page 93 of 93

Appendix D
DEQ Risk Calculators
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Prepared By:Hart & Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC
Mill Building and Parking Deck - Site Wide Final Grade Soil
North Carolina Department of Environmental Quality
Risk Calculator
Caraustar and Savona Mills
500 and 528 South Turner Avenue, Charlotte
Brownfields Redevelopment Section
23061-19-060
July 2023
May 2023 EPA RSL Table
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 23061-19-060
Exposure Unit ID: Mill Building and Parking Deck - Site Wide Worst Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2023Basis: May 2023 EPA RSL TableSite ID: 23061-19-060Exposure Unit ID: Mill Building and Parking Deck - Site Wide Worst CaseNOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsExposure Point Concentration (mg/kg)Notes: CAS NumberChemicalFor the chemicals highlighted in blue, data entry notes are provided in the PSRG Table link on the Main MenuMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion0.091 67-64-1Acetonemg/kg6.92 7440-38-2Arsenic, Inorganicmg/kg110 7440-39-3Bariummg/kg0.268 J 7440-43-9Cadmium (Diet)mg/kg0.001 J 75-15-0Carbon Disulfidemg/kg92.4 16065-83-1Chromium(III), Insoluble Saltsmg/kg0.707 18540-29-9Chromium(VI)mg/kg0.159 J 132-64-9~Dibenzofuranmg/kg0.005 J 110-54-3Hexane, N-mg/kg82.2 7439-92-1~Lead and Compoundsmg/kg0.156 7487-94-7~Mercuric Chloride (and other Mercury salts)mg/kg0.01 J 78-93-3Methyl Ethyl Ketone (2-Butanone)mg/kg0.006 J 75-09-2Methylene Chloridemg/kg0.217 J 83-32-9~Acenaphthenemg/kg0.716 J 120-12-7~Anthracenemg/kg2.22 J 56-55-3~Benz[a]anthracenemg/kg2.25 J 50-32-8~Benzo[a]pyrenemg/kg2.86 J 205-99-2~Benzo[b]fluoranthenemg/kg1 J 207-08-9~Benzo[k]fluoranthenemg/kg2.14 J 218-01-9~Chrysenemg/kg4.25 206-44-0~Fluoranthenemg/kg0.156 J 86-73-7~Fluorenemg/kg1.47 J 193-39-5~Indeno[1,2,3-cd]pyrenemg/kg0.212 J 90-12-0~Methylnaphthalene, 1-mg/kg0.286 J 91-57-6~Methylnaphthalene, 2-mg/kg0.264 J 91-20-3~Naphthalenemg/kg3.98 129-00-0~Pyrenemg/kg0.91 7782-49-2Seleniummg/kg0.0859 J 7440-22-4Silvermg/kgInput Form 2ASoil Exposure Point Concentration TableDescription of Exposure Point Concentration Selection:North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 23061-19-060
Exposure Unit ID: Mill Building and Parking Deck - Site Wide Worst Case
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 3.8E-05 3.9E-01 NO
Groundwater Use* NC NC NC
Soil 3.8E-06 2.9E-02 NO
Groundwater Use* NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 23061-19-060
Exposure Unit ID: Mill Building and Parking Deck - Site Wide Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.091 0.091 0.091 1.3E-06 1.3E-06
7440-38-2 Arsenic, Inorganic 6.92 6.92 6.92 9.0E-06 1.3E-06 1.8E-10 1.0E-05 1.8E-01 2.1E-02 7.5E-06 2.0E-01
7440-39-3 Barium 110 110 110 7.0E-03 3.6E-06 7.0E-03
7440-43-9 Cadmium (Diet) 0.268 0.268 0.268 2.9E-12 2.9E-12 3.4E-02 3.3E-03 4.3E-07 3.8E-02
75-15-0 Carbon Disulfide 0.001 0.001 0.001 1.3E-07 4.4E-07 5.6E-07
16065-83-1 Chromium(III), Insoluble Salts 92.4 92.4 92.4 7.9E-04 7.9E-04
18540-29-9 Chromium(VI) 0.707 0.707 0.707 2.3E-06 9.9E-10 2.3E-06 3.0E-03 1.1E-07 3.0E-03
132-64-9 ~Dibenzofuran 0.159 0.159 0.159 2.0E-03 2.0E-03
110-54-3 Hexane, N- 0.005 0.005 0.005 2.2E-06 2.2E-06
7439-92-1 ~Lead and Compounds 82.2 82.2 82.2 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.156 0.156 0.156 6.6E-03 8.4E-09 6.6E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.01 0.01 0.01 2.1E-07 1.5E-07 3.6E-07
75-09-2 Methylene Chloride 0.006 0.006 0.006 7.8E-11 1.9E-11 9.7E-11 1.3E-05 3.1E-06 1.6E-05
83-32-9 ~Acenaphthene 0.217 0.217 0.217 4.6E-05 1.4E-05 6.1E-05
120-12-7 ~Anthracene 0.716 0.716 0.716 3.1E-05 9.4E-06 4.0E-05
56-55-3 ~Benz[a]anthracene 2.22 2.22 2.22 1.4E-06 4.8E-07 2.8E-08 2.0E-06
50-32-8 ~Benzo[a]pyrene 2.25 2.25 2.25 1.5E-05 4.9E-06 2.2E-11 2.0E-05 9.6E-02 3.0E-02 1.8E-05 1.3E-01
205-99-2 ~Benzo[b]fluoranthene 2.86 2.86 2.86 1.9E-06 6.2E-07 2.9E-12 2.5E-06
207-08-9 ~Benzo[k]fluoranthene 1 1 1 6.5E-08 2.2E-08 1.0E-13 8.7E-08
218-01-9 ~Chrysene 2.14 2.14 2.14 1.4E-08 4.7E-09 2.1E-14 1.9E-08
206-44-0 ~Fluoranthene 4.25 4.25 4.25 1.4E-03 4.2E-04 1.8E-03
86-73-7 ~Fluorene 0.156 0.156 0.156 5.0E-05 1.5E-05 6.5E-05
193-39-5 ~Indeno[1,2,3-cd]pyrene 1.47 1.47 1.47 9.6E-07 3.2E-07 1.5E-12 1.3E-06
90-12-0 ~Methylnaphthalene, 1- 0.212 0.212 0.212 8.8E-09 3.2E-09 1.2E-08 3.9E-05 1.2E-05 5.1E-05
91-57-6 ~Methylnaphthalene, 2- 0.286 0.286 0.286 9.1E-04 2.8E-04 1.2E-03
91-20-3 ~Naphthalene 0.264 0.264 0.264 4.6E-08 1.7E-08 6.5E-08 1.3E-07 1.7E-04 5.2E-05 1.7E-03 1.9E-03
129-00-0 ~Pyrene 3.98 3.98 3.98 1.7E-03 5.2E-04 2.2E-03
7782-49-2 Selenium 0.91 0.91 0.91 2.3E-03 7.4E-10 2.3E-03
7440-22-4 Silver 0.0859 0.0859 0.0859 2.2E-04 2.2E-04
Cumulative: 3.8E-05 3.9E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 23061-19-060
Exposure Unit ID: Mill Building and Parking Deck - Site Wide Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.091 0.091 0.091 8.7E-08 8.7E-08
7440-38-2 Arsenic, Inorganic 6.92 6.92 6.92 1.9E-06 4.0E-07 4.1E-11 2.3E-06 1.2E-02 2.5E-03 1.8E-06 1.4E-02
7440-39-3 Barium 110 110 110 4.7E-04 8.5E-07 4.7E-04
7440-43-9 Cadmium (Diet) 0.268 0.268 0.268 6.6E-13 6.6E-13 2.3E-03 3.9E-04 1.0E-07 2.7E-03
75-15-0 Carbon Disulfide 0.001 0.001 0.001 8.6E-09 1.0E-07 1.1E-07
16065-83-1 Chromium(III), Insoluble Salts 92.4 92.4 92.4 5.3E-05 5.3E-05
18540-29-9 Chromium(VI) 0.707 0.707 0.707 1.1E-07 8.2E-11 1.1E-07 2.0E-04 2.7E-08 2.0E-04
132-64-9 ~Dibenzofuran 0.159 0.159 0.159 1.4E-04 1.4E-04
110-54-3 Hexane, N- 0.005 0.005 0.005 5.2E-07 5.2E-07
7439-92-1 ~Lead and Compounds 82.2 82.2 82.2 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.156 0.156 0.156 4.5E-04 2.0E-09 4.5E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.01 0.01 0.01 1.4E-08 3.5E-08 4.9E-08
75-09-2 Methylene Chloride 0.006 0.006 0.006 3.7E-12 1.6E-12 5.2E-12 8.6E-07 7.3E-07 1.6E-06
83-32-9 ~Acenaphthene 0.217 0.217 0.217 3.1E-06 1.7E-06 4.8E-06
120-12-7 ~Anthracene 0.716 0.716 0.716 2.0E-06 1.1E-06 3.2E-06
56-55-3 ~Benz[a]anthracene 2.22 2.22 2.22 6.8E-08 3.7E-08 2.3E-09 1.1E-07
50-32-8 ~Benzo[a]pyrene 2.25 2.25 2.25 6.9E-07 3.8E-07 1.9E-12 1.1E-06 6.4E-03 3.5E-03 4.3E-06 1.0E-02
205-99-2 ~Benzo[b]fluoranthene 2.86 2.86 2.86 8.7E-08 4.8E-08 2.4E-13 1.4E-07
207-08-9 ~Benzo[k]fluoranthene 1 1 1 3.1E-09 1.7E-09 8.2E-15 4.7E-09218-01-9 ~Chrysene 2.14 2.14 2.14 6.5E-10 3.6E-10 1.8E-15 1.0E-09
206-44-0 ~Fluoranthene 4.25 4.25 4.25 9.1E-05 5.0E-05 1.4E-04
86-73-7 ~Fluorene 0.156 0.156 0.156 3.3E-06 1.8E-06 5.2E-06
193-39-5 ~Indeno[1,2,3-cd]pyrene 1.47 1.47 1.47 4.5E-08 2.5E-08 1.2E-13 7.0E-08
90-12-0 ~Methylnaphthalene, 1- 0.212 0.212 0.212 1.9E-09 1.0E-09 2.9E-09 2.6E-06 1.4E-06 4.0E-06
91-57-6 ~Methylnaphthalene, 2- 0.286 0.286 0.286 6.1E-05 3.4E-05 9.5E-05
91-20-3 ~Naphthalene 0.264 0.264 0.264 9.7E-09 5.3E-09 1.5E-08 3.0E-08 1.1E-05 6.2E-06 4.1E-04 4.2E-04
129-00-0 ~Pyrene 3.98 3.98 3.98 1.1E-04 6.2E-05 1.8E-04
7782-49-2 Selenium 0.91 0.91 0.91 1.6E-04 1.8E-10 1.6E-04
7440-22-4 Silver 0.0859 0.0859 0.0859 1.5E-05 1.5E-05
Cumulative: 3.8E-06 2.9E-02
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator