25044 George Fern Brownfields Assessment Report 20230719

Via Email
July 19, 2023

NCDEQ – Division of Waste Management
Brownfields Redevelopment Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Attn: Mr. Seth Titley

Re: Brownfields Assessment Report
George Fern Company
2310 Old Steele Creek Road
Charlotte, North Carolina
Brownfields Project No. 25044-21-060
H&H Project No. FDI-001

Dear Seth:

On behalf of Furniture Distributors, Inc., please find the enclosed Brownfields Assessment
Report prepared for the George Fern Company Brownfields property. The assessment activities
were completed pursuant to the North Carolina Department of Environmental Quality approved
Brownfields Assessment Work Plan dated December 28, 2022.

Should you have questions or require additional information, please do not hesitate to contact us
at [phone].

Sincerely,
Hart & Hickman, PC
Haley Martin, PG Ralph McGee, PG
Senior Project Geologist Senior Project Manager

Enclosures:

cc: Mr. Ken Corley and Mr. Michael O’Loughlin, Furniture Distributors, Inc. (Via Email)
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Brownfields Assessment Report
George Fern Company
2310 Old Steele Creek Road
Charlotte, North Carolina
Brownfields Project No. 25044-21-060
H&H Job No. FDI-001

Table of Contents

1.0 Introduction and Background ...............................................................................................1 
1.1 Site Background Information ................................................................................................2 
1.2 Previous Assessment Activities .............................................................................................2 
2.0 Brownfields Assessment Activities ........................................................................................6 
3.0 Receptor Survey ......................................................................................................................8 
4.0 Soil Assessment Activities .....................................................................................................11 
4.1 Soil Sampling Activities ......................................................................................................11 
4.2 Soil Sampling Analytical Results ........................................................................................13 
5.0 Groundwater Assessment Activities ....................................................................................15 
5.1 Groundwater Sampling Activities .......................................................................................15 
5.2 Groundwater Sample Analytical Results .............................................................................16 
6.0 Soil Gas Assessment Activities .............................................................................................18 
6.1 Sub-Slab Soil Gas Sampling Activities ...............................................................................18 
6.2 Sub-Slab Soil Gas Sampling Results ...................................................................................20 
6.3 Vapor Intrusion Evaluation .................................................................................................20 
7.0 Quality Assurance – Quality Control ..................................................................................23 
7.1 Trip Blank ............................................................................................................................23 
7.2 Field Duplicates ...................................................................................................................23 
7.3 Investigation Derived Waste ...............................................................................................24 
8.0 Summary and Conclusions ..................................................................................................25 

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List of Tables

Table 1 Summary of Soil Analytical Data
Table 2 Summary of Well Construction and Groundwater Elevation Data
Table 3 Summary of Groundwater Analytical Data
Table 4 Summary of Sub-Slab Soil Gas Analytical Data

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Sample Location Map
Figure 4 Receptor Survey Map
Figure 5 Shallow Groundwater Potentiometric Map

List of Appendices

Appendix A Brownfields Property Receptor Survey Form
Appendix B Boring Logs
Appendix C Laboratory Analytical Reports
Appendix D Groundwater and Soil Gas Sampling Forms
Appendix E DEQ Risk Calculators

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Brownfields Assessment Report
George Fern Company
2310 Old Steele Creek Road
Charlotte, North Carolina
Brownfields Project No. 25044-21-060
H&H Job No. FDI-001

1.0 Introduction

On behalf of Furniture Distributors, Inc. (the Prospective Developer or PD), Hart & Hickman,
PC (H&H) has prepared this Brownfields Assessment Report for the George Fern Brownfields
property (Brownfields Project No. 25044-21-060) located at 2310 Old Steele Creek Road in
Charlotte, Mecklenburg County, North Carolina (Site). The Site consists of one parcel
(Mecklenburg County Parcel Identification No. 11710302) that totals approximately 9.6 acres of
land. A Site location map is provided as Figure 1, and the Site and surrounding area are shown
in Figure 2.

The Site is improved with one approximate 60,000 square feet (sq ft) industrial warehouse
building that is currently occupied by Kimbrell’s Furniture. The Site building was previously
occupied by George Fern Company, a trade show and rental company for conference and
exhibition equipment. A small communications facility operated by a third-party
communications company is located in the north-central portion of the Site and is enclosed
within a chain-link security fence. The remaining portions of the Site consist of asphalt-paved
vehicle access and parking areas, concrete loading areas, and landscaped and vegetated areas.

Since occupying the Site building in 2022, the PD has completed cosmetic interior upfit
activities (i.e. new carpeting, painting, etc.) and utilizes the Site building for corporate office and
furniture distribution. It should be noted that residential development is not an intended use for
the Brownfields property and there are no planned redevelopment activities for the Site at this
time.
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1.1 Background

As early as 1938, the Site consisted predominately of undeveloped land used for agricultural
purposes (e.g., hay fields, pastures, row crops, etc.) and wooded areas. By the early 1950s,
agricultural areas at the Site transitioned to undeveloped wooded land and remained undeveloped
until the mid-1960s, when the northern portion of the Site was partially cleared and graded. By
the mid-1990s, a small communications facility was constructed in the north-central portion of
the Site. The current Site building was constructed in the southern portion of the Site in 2004.
From 2004 to 2020, the Site was occupied by the George Fern Company for rental of trade show,
convention, and exhibition equipment.

1.2 Previous Assessment Activities

To obtain additional information, H&H reviewed several environmental reports prepared to
document previous environmental assessment completed at the Site and nearby off-Site facilities.
A brief summary of information provided in the environmental reports is provided below.

Dupont Charlotte Transportation Terminal
According to information provided in environmental documents, DuPont began leasing the
northern adjoining property (2246 Old Steele Creek Road) in October 1955 and used the
property for temporary storage of old equipment for resale at auction. Additional development at
the former DuPont facility (office and support building construction, rail spur replacement, UST
installation and closure) occurred in several phases between 1955 and 1997. Operations in the
mid to late 1990s involved unloading hydrogen peroxide from railroad cars into aboveground
storage tanks (ASTs), blending raw hydrogen peroxide with water, testing the hydrogen peroxide
with chemicals (i.e., sulfuric acid and potassium permanganate), and loading mixed product into
truck trailers for delivery. Limited storage and mixing of dyes were also conducted at the
facility. DuPont ceased operations at the facility and vacated the property in 1998.

During assessment activities completed at the former DuPont facility in the 1990s, several
chlorinated solvents including the volatile organic compounds (VOCs) tetrachloroethylene
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(PCE) and trichloroethene (TCE) were detected in groundwater at concentrations above the
North Carolina Administrative Code (NCAC) 15A 2L Groundwater Standards (2L Standards).
In 2006, the facility was referred to the DEQ Inactive Hazardous Sites Branch (IHSB) for
additional investigation.

DuPont subsequently entered into an Administrative Agreement (AA) with DEQ for voluntary
assessment and remediation in accordance with the IHSB Registered Environmental Consultant
(REC) program. In the AA, the former DuPont facility is identified as the DuPont Charlotte
Transportation Terminal (IHSB Project No. NCD981861214). Extensive soil and groundwater
assessment activities conducted at the former DuPont facility as part of the REC program
activities indicate the presence of several chlorinated solvents including PCE, TCE, cis-1,2-
dichlorothene (cis-1,2-DCE), and vinyl chloride at low concentrations in groundwater at the
former DuPont facility located on the northern adjoining property (2300 Old Steele Creek Road),
and the subject Site (George E. Fern facility).

During remedial investigation activities completed in 2012, groundwater monitoring wells were
installed on the subject Site (see Figure 2) and downgradient of the subject Site along Primrose
Avenue to further evaluate the extent of the chlorinated solvents in groundwater downgradient of
the former DuPont facility. The 2012 remedial investigation also included collecting
groundwater samples from monitoring wells located upgradient and downgradient of the former
Dupont facility for compound specific isotope analysis (CSIA). Results of the CSIA indicated
several potential and documented sources of PCE and TCE present in the area including a source
at the former DuPont facility, a drycleaners property which is managed through the DEQ Dry-
Cleaning Solvent Cleanup Act (DSCA) Program, and a Brownfields property located to the
northwest.

The remedial investigation also indicated that there is separate source of PCE near monitoring
well OFF-MW-5 (Figure 2) which is located along the southern Site boundary and southwest of
the Site building. DEQ subsequently identified the contamination south of the Site as the
Primrose Avenue PCE Contamination release. The source of the Primrose Avenue PCE
Contamination release is unknown.
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DEQ subsequently performed additional assessment of the Primrose Avenue PCE Contamination
release to verify lack of impact to potential receptors from vapor intrusion at the subject Site
building and residences located south of the Site. As part of additional assessment activities
performed in 2012 and 2013, DEQ performed soil gas and crawlspace sampling at residences
located south of the Site. In 2013, DEQ also collected sub-slab soil gas samples for laboratory
analysis from one location in the southwest portion of the Site building in January and February
2013.

The sub-slab soil gas sample analytical results of the two samples identified PCE (up to 23
micrograms per cubic meter {µg/m3}) at concentrations well below the DEQ Non-Residential
Vapor Intrusion Sub-Slab and Exterior Soil Gas Screening Level (SGSL) of 3,500 µg/m3. Based
on results of the sampling activities completed in 2013, DEQ indicated in a letter dated March 7,
2013, that evaluation for potential structural vapor intrusion into the Site building had been
completed in accordance with DEQ guidelines and that no further vapor intrusion sampling was
warranted.

The selected remedial alternative for groundwater impacts associated with the former DuPont
facility is monitored natural attenuation (MNA). As part of the MNA remedy, DuPont (now
Chemours) collects groundwater samples from monitoring wells installed at the Site and the
northern adjacent properties. Results of recent groundwater monitoring activities performed in
May 2019 indicate PCE and TCE were detected in Site groundwater at concentrations up to 6.2
micrograms per liter (µg/L) and 32 µg/L, respectively. In general, review of the monitoring data
indicates that concentrations of compounds in the Site and adjacent property monitor wells have
decreased with time.

The Site was entered into the DEQ Brownfields Redevelopment Section to address
environmental concerns associated with historical off-Site operations. A Brownfields Property
Application was submitted to DEQ on June 3, 2021, and a Letter of Eligibility was issued for the
Site by DEQ on November 22, 2021. As part of the Brownfields process, a kick-off/data gap
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meeting with the PD, H&H, and DEQ Brownfields personnel was held on October 6, 2022 to
discuss prior Site history, data gaps, and the proposed schedule for completing the Brownfields
Agreement. To address data gaps and DEQ Brownfields requests for additional assessment,
H&H prepared a Brownfields Assessment Work Plan (Work Plan) for DEQ review and approval.
The Work Plan received DEQ-approval in a letter dated February 3, 2023.

Brownfields assessment activities were completed further evaluate the potential for impacts at
the Site for the protection of Site workers. The Brownfields assessment activities discussed in
the following sections include collection of soil, groundwater, and sub-slab soil gas samples. In
addition to the sampling activities, H&H conducted receptor survey activities to obtain
information associated with land use, potable water supply, and potential sensitive receptors in
the area surrounding the Site.

A summary of the Brownfields assessment activities conducted in accordance with the DEQ-
approved Work Plan is provided in the following sections.
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2.0 Brownfields Assessment Activities

Brownfields Assessment activities were completed in March 2023 and included the collection of
soil, groundwater, and sub-slab soil gas samples to further evaluate the potential for impacts
associated with historical off-Site operations and for the protection of Site workers. In addition,
a receptor survey was completed to obtain information about land use, water supply, basements,
underground utilities, drains, and surface water bodies in the vicinity of the Site.

As part of the assessment activities, soil borings were advanced in unpaved and landscaped areas
of the Site, the gravel parking area located west of the Site building, and from background
locations in the northern and western portions of the Site to evaluate potential risks to Site
workers from direct soil exposure in unpaved areas of the Site. H&H also completed
groundwater assessment activities to evaluate current subsurface conditions for potential impacts
associated with nearby off-Site operations. To evaluate the potential for structural vapor
intrusion, H&H collected sub-slab soil gas samples within the existing Site building.

Prior to conducting field activities, H&H contacted North Carolina 811, the public utility locator,
to mark subsurface utilities at the Site. H&H also contracted with a private utility locator to
mark utilities which were not identified by the public locator. The private utility locator also
utilized ground penetrating radar (GPR) survey techniques to identify and mark utilities. In
addition, H&H directed the drilling contractor to hand clear each boring to a depth of
approximately 5 feet below ground surface (ft bgs) to further screen the boring locations for the
presence of subsurface utilities prior to utilizing mechanical drilling equipment.

The Brownfields assessment activities were conducted in general accordance with the DEQ
Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup of
Contaminated Sites (Guidelines) dated September 2022, the DEQ Division of Waste
Management (DWM) Vapor Intrusion Guidance (VI Guidance) dated March 2018, the most
recent versions of the U.S. Environmental Protection Agency (EPA) Region IV Laboratory
Services and Applies Science Division (LSASD) Field Branches Quality System and Technical
Procedures guidance, the Brownfields Redevelopment Section Minimum Requirements
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Checklist Site Assessment Work Plan and Reports dated March 2023, and the DEQ-approved
Work Plan.

A summary of receptor survey results is provided in Section 3.0, details of the soil, groundwater,
and vapor intrusion assessment activities are provided in Section 4.0 through Section 6.0. A
description of the quality assurance and quality control measures and investigation derived waste
is provided in Section 7.0, and a summary and conclusions based on results of the assessment
activities are provided in Section 8.0.
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3.0 Receptor Survey

In March 2023, H&H conducted a receptor survey at the Site and surrounding area. Receptor
survey activities included an intensive pedestrian and vehicular survey for possible potable water
supply wells, springs, and surface water intakes used as a source of water within a 1,500 ft radius
of the Site in accordance with the DEQ-approved Work Plan. H&H also reviewed the online
Mecklenburg County Well Information System for potential wells in the area and utilized the
online DEQ Source Water Assessment Program (SWAP) to identify potential potable water
sources for properties located within a 1,500 ft radius of the Site. In addition, H&H identified
the locations of main underground and aboveground utilities and land use and zoning in the area
of the Site using available Mecklenburg County online resources. A receptor survey map is
provided as Figure 4, and a copy of the completed DEQ Brownfields Property Receptor Survey
form is provided as Appendix A. Results of the receptor survey activities are summarized
below.

Zoning
The George Fern Company property is zoned as industrial manufacturing and logistics (ML-2).
Adjacent properties located to the north, west, and east are zoned as industrial manufacturing and
logistics (ML-1 and ML-2). Adjacent properties located to the south and southeast are zoned as
residential (N1-D and N2-B).

Municipal Water Availability
Municipal water supplied by the City of Charlotte is available to the Site and surrounding area.
H&H did not identify sources of public drinking water within 1,500 ft of the Site based on the
review of information available on Mecklenburg County Well Information System Maps, DEQ
SWAP, and the Annual Water Quality Report published by the City of Charlotte. The City of
Charlotte obtains raw water from Lake Norman and Mountain Island Lake which are located
approximately 15 miles north-northwest of the Site.

Water Supply Wells
H&H conducted a pedestrian and vehicular survey of properties within a 1,500 ft radius of the
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Site to identify potential water supply wells. H&H also utilized DEQ SWAP geographic
information system map and Mecklenburg County Well Information System maps to identify
potential potable water supply wells located within a 1,500 ft radius of the Site. According to the
above sources of information, two active water supply wells and one inactive water supply well
are located greater than 250 ft to the southwest of the Site. One inactive water supply well is
reportedly located greater than 500 ft west of the Site. The reported water supply wells were not
observed during the vehicular survey. No other water supply wells were identified within a
1,500 ft radius of the Site.

Surface Water Bodies
An unnamed tributary of Taggart Creek is located approximately 650 ft to the northwest of the
Site and unnamed ponds associated with the Carolina Golf Club are located approximately 1,050
ft to the southeast of the Site. Based on the DEQ Surface Water Classification system, Taggart
Creek is a Class C surface water body. A Class C surface water body is defined as “waters
protected for uses such as secondary recreation, fishing, wildlife, fish consumption, aquatic life
including propagation, survival and maintenance of biological integrity, and agriculture.
Secondary recreation includes wading, boating, and other uses involving human body contact
with water where such activities take place in an infrequent, unorganized, or incidental manner”.
Based on information obtained from the DEQ Division of Water Resources (DWR) Surface
Water Classifications geographic information system map, the subject Site is not located within a
protected water supply watershed area.

Subsurface Utilities and Structures
H&H contacted North Carolina 811, the public utility locator, to mark subsurface utilities located
on the Site and conducted a visual reconnaissance in the Site area to identify potential subsurface
structures within 100 ft of the subject Site. H&H observed evidence of subsurface utilities
including sanitary sewer, municipal water, electrical, natural gas, and fiber on the Site and
nearby adjacent properties. Overhead electrical lines were observed to the east of the Site along
Old Steele Creek Road and to the southwest of the Site along Primrose Avenue.

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H&H did not observe structures with potential basements within a 1,500 ft radius of the Site
during the visual reconnaissance. Approximate locations of subsurface and overhead utilities
located in the immediate vicinity of the Site are shown in Figure 4.
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4.0 Soil Assessment Activities

In March 2023, H&H advanced twelve (12) soil borings at the Site to evaluate for potential risks
to Site workers from direct exposure pathway in unpaved areas of the Site. In addition, H&H
collected two (2) background soil samples for evaluating the presence of naturally occurring
metals. Locations of the soil borings are shown in Figure 3.

Soil borings were advanced utilizing a decontaminated stainless-steel hand auger. During boring
advancement, continuous soil samples were collected from the center of the hand auger bucket.
The soil samples were logged for lithologic description, observed for obvious evidence of
staining and unusual odors, and field screened for the presence of volatile organic vapors using a
calibrated photoionization detector (PID). Obvious evidence of staining, odors, or elevated PID
readings were not observed by field personnel during soil boring advancement. Boring logs
including lithologic descriptions and field screening results for each soil boring are provided in
Appendix B.

A discussion of the soil sampling activities and results is provided in the following sections.

4.1 Soil Sampling Activities

Gravel Parking Area
H&H advanced two (2) soil borings (BF-SB-01 and BF-SB-02) to approximately 5 ft bgs in the
gravel covered parking area located west of the existing Site building. No obvious evidence of
impacts were observed during field screening; therefore, two samples were collected from
shallow (0-2 ft bgs) and deeper (2-4 ft bgs) soil from each boring (for a total of four samples), in
accordance with the approved Work Plan. The soil samples were analyzed for VOCs by EPA
Method 8260, semi-volatile organic compounds (SVOCs) by EPA Method 8270, and Resource
Conservation and Recovery Act (RCRA) metals plus hexavalent chromium by EPA Methods
6020/7471/7199.
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Composite Soil Samples
Ten (10) soil borings were advanced to approximately 5 ft bgs within the vegetated and
landscaped areas of the Site. Aliquot soil samples were collected from each boring and
homogenized to form one composite soil sample representative of soil conditions in that
evaluation area for a total of two (2) composite soil samples (COMP-1 and COMP-2), in
accordance with the approved Work Plan.

Composite soil samples were submitted for laboratory analysis of SVOCs by EPA Method 8270
and RCRA metals plus hexavalent chromium by EPA Methods 6020/7471/7199. In addition,
one grab sample was collected from a discrete depth interval in one aliquot boring advanced
within each evaluated area for a total of two grab soil samples. The grab soil samples were
collected from undisturbed portions of soil directly into laboratory supplied glassware and
submitted for analysis of VOCs by EPA Method 8260.

Soil samples selected for laboratory analysis were placed in dedicated laboratory supplied
sample containers, labeled with the sample identification, date, and requested analysis, and
placed in a laboratory supplied cooler with ice. The samples were delivered to Pace Analytical
(Pace), a North Carolina certified laboratory, under standard chain of custody protocols for
laboratory analysis.

In addition to the soil samples described above, two (2) background soil samples (BF-BG-1 and
BF-BG-2) were collected at the Site to evaluate background levels of naturally occurring metals.
The soil samples were collected from the northern and western portions of the Site in areas that
appeared to be undisturbed by historical uses. The soil borings were advanced to 5 ft bgs and
soil samples were collected from the depth interval with the highest potential for impacts based
on field screening results. No obvious evidence of impact was observed during field screening;
therefore, samples were collected from shallow soil (0-2 ft bgs), in accordance with the approved
Work Plan. The samples were submitted for laboratory analysis of RCRA metals by EPA
Methods 6020/7471 and hexavalent chromium by EPA Method 7199.

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Following sampling activities, the soil borings were abandoned, and the surfaces were repaired
similar to pre-drilling conditions. In addition, the soil sample locations were estimated using a
hand-held global positioning system (GPS) unit.

4.2 Soil Sampling Analytical Results

A tabular summary of the soil sample analytical results is presented in Table 1. Copies of the
laboratory analytical reports and chain of custody records are provided in Appendix C. The
laboratory analytical results were compared to the most recent versions of the DEQ
Industrial/Commercial PSRGs dated January 2023. In addition to the PSRGs, metals results
were compared to published concentrations for naturally occurring metals as well as Site-specific
background levels. A discussion of the laboratory analytical results in comparison to the
regulatory screening levels and background levels for metals is included below.

Organic Compounds
Laboratory analytical results did not indicate the presence of organic compounds at
concentrations above the DEQ Industrial/Commercial PSRGs in the soil samples collected at the
Site. Laboratory analytical results indicated low levels of 1,4-dichlorobenzene (0.0037 J mg/kg),
chloromethane (up to 00.79 J, C8 mg/kg), and PCE (0.0119 mg/kg) at concentrations above the
laboratory method detection limits, but below the DEQ Industrial/Commercial PSRGs. Note that
the J-Flag designation indicates that the compound was detected at a concentration above the
laboratory method detection limit but below the laboratory reporting limit, resulting in a
laboratory estimated concentration. The C8 designation indicates that the compound
concentration may be biased high due to laboratory carryover from a previously analyzed
sample. No other organic compounds were detected at concentrations above laboratory method
detection limits in the soil samples collected at the Site.

Metals
As expected, several metals were detected at concentrations above the laboratory method
detection limits in each soil sample. No metals were detected at concentrations above the DEQ
Industrial/Commercial PSRGs in soil samples collected at the Site. The detected metals
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concentrations are generally consistent with both published and Site-specific background levels
and are considered representative of naturally occurring levels.
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5.0 Groundwater Assessment Activities

In March 2023, H&H collected groundwater samples from five (5) existing monitoring wells
(OFF-MW-1, OFF-MW-6, MW-11S, OFF-MW-5, and OFF-MW-7) to evaluate current
subsurface conditions for potential impacts associated with nearby off-Site operations. Locations
of the monitoring wells are depicted in Figure 3.

It should be noted monitoring well OFF-MW-8 could not be located during field activities and a
groundwater sample was not collected. H&H informed DEQ of the variance from the approved
Work Plan and DEQ approved the variance in an email dated March 8, 2023. Details of the
groundwater sampling activities and results are provided in the following sections.

5.1 Groundwater Sampling Activities

Prior to sampling, H&H collected depth to groundwater measurements from eleven permanent
groundwater monitoring wells located on the Site. Depth to water measurements were collected
from the top of casing utilizing a decontaminated electronic water level indicator. To minimize
the potential for cross-contamination, depth to water measurements were collected from least
impacted to most impacted wells based on historical data.

During the March 2023 gauging event, groundwater elevations ranged from 717.81 ft above
mean sea level (msl) at OFF-MW-7 to 723.01 ft above msl at MW-10S in the shallow aquifer.
The water table elevations were used to estimate the groundwater flow direction at the Site
toward the southwest. A tabular summary of groundwater elevation data is provided as Table 2,
and the shallow water table potentiometric surface and estimated groundwater flow direction are
shown in Figure 5.

Once depth to water measurements were collected, groundwater samples were collected for
laboratory analysis from existing monitoring wells OFF-MW-1, OFF-MW-6, MW-11S, OFF-
MW-5, and OFF-MW-7 utilizing low flow/low stress purging techniques using a peristaltic and
dedicated polyethylene tubing. During sampling, the intake point of the sample tubing was
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placed in the approximate mid-portion of the screened interval of the well, and groundwater was
removed at a rate no greater than 200 milliliters per minute (mL/min). H&H utilized calibrated
water quality meters to collect measurements of pH, temperature, dissolved oxygen, oxidation
reduction potential, turbidity, and specific conductivity at three to five-minute intervals during
the purging process. Purging was considered complete when the field parameters stabilized (pH
± 0.1 SU, conductivity varied no more than 5%, and turbidity was less than 10 Nephelometric
Turbidity Units [NTUs]). Groundwater sampling forms completed by sampling personnel are
provided in Appendix D.

Once groundwater parameters stabilized, groundwater samples submitted for analysis of SVOCs
and RCRA metals were collected directly into laboratory supplied glassware directly from the
sample tubing discharge. The groundwater samples for VOC analysis were collected directly
into laboratory supplied sample containers using the “soda straw” method to eliminate the
potential for volatile compound loss through the pump head. The sample containers were
labeled with the sample identification, date, time, and requested analysis, and placed in a
laboratory supplied cooler with ice.

The groundwater samples were delivered to Pace under standard chain of custody protocols for
analyses of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and RCRA metals by
EPA Method 6020/7470.

5.2 Groundwater Sample Analytical Results

A tabular summary of the groundwater sample laboratory analytical results is presented in
Table 3. Copies of the laboratory analytical reports and chain of custody records are provided in
Appendix C. Groundwater analytical data were compared to the 2L Standards dated April 2022
and the DEQ Non-Residential Vapor Intrusion Groundwater Screening Levels (GWSLs) dated
January 2023.

Organic Compounds
Laboratory analytical results indicated that PCE (up to 932 µg/L) was detected at concentrations
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above the 2L Standard and/or the DEQ Non-Residential Vapor Intrusion GWSL in the
groundwater samples collected from monitoring wells OFF-MW-1/GW-DUP, OFF-MW-6, MW-
11S, and OFF-MW-5. A concentration of TCE (54.3 µg/L) was detected above the 2L Standard
and DEQ Non-Residential Vapor Intrusion GWSL in the OFF-MW-5 monitoring well sample.
Laboratory analytical results indicate that no other organic compounds were detected at
concentrations above the 2L Standards or the DEQ Non-Residential Vapor Intrusion GWSLs in
the monitoring well samples. The sampling results are generally consistent with historical data
reported in the reports prepared for the upgradient DuPont Charlotte Transportation Terminal
(IHSB Project No. NCD981861214).

Metals
Low levels of arsenic (up to 0.20 J µg/L), barium (up to 72.6 µg/L), chromium (up to 4.8 µg/L),
lead (0.31 J µg/L), and selenium (up to 0.16 J µg/L) were detected at concentrations above the
laboratory method detection limits, but below the 2L Standards. No other metals were detected
at concentrations above the laboratory method detection limits in groundwater samples collected
from the existing groundwater monitoring wells.
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6.0 Soil Gas Assessment Activities

To evaluate the potential for structural vapor intrusion, H&H installed and sampled twelve (12)
temporary sub-slab soil gas sampling points (BF-SSV-01 through BF-SSV-12) within the
existing Site building. The sub-slab soil gas sampling point locations are shown in Figure 3, and
the soil gas sampling activities and results are described below.

6.1 Soil Gas Sampling Activities

Sub-Slab Soil Gas Sample Point Installation
The sub-slab soil gas sampling points were installed using a rotary hammer drill and 1½-inch
diameter drill bit to advance a pilot hole into the concrete slab to a depth of approximately 1¾
inches below the surface. A drill guide was then be placed in the pilot hole and a 5/8-inch
diameter drill bit was utilized to advance the boring through the concrete slab and approximately
6-inches into the underlying soil. Following concrete borehole advancement, loose concrete
cuttings were removed from each boring using a bottlebrush. A Cox-Colvin Vapor Pin™ (vapor
pin) assembly (brass sampling point and silicone sleeve) was then seated in the borehole using an
installation/extraction tool and hammer. Upon installation of the vapor pin assembly, dedicated
Teflon® sample tubing was connected to the barbed end of the sample point. Each sub-slab soil
gas point was allowed to equilibrate for a minimum of 2-hours after installation and prior to
sample collection.

Sub-Slab Soil Gas Sampling
Each sub-slab soil gas sample was collected utilizing a laboratory supplied 1-liter Summa®
canister connected to an air-flow regulator calibrated by the laboratory to collect the soil gas
sample at a rate of approximately 100 mL/min. Prior to collection of the sub-slab soil gas
samples, “shut-in” tests were conducted on the sampling train and helium leak checks were
conducted at each sub-slab soil gas sampling point. A description of the shut-in test and helium
leak testing procedures is provided below.
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The shut-in test was conducted by connecting the flow regulator with the vacuum gauge to the
Summa® canister and sealing the flow regulator with the laboratory provided brass cap. Once
the sampling train was “closed”, the sample valve on the Summa® canister was opened and the
reading on the vacuum gauge was recorded. The Summa® canister sample valve was then closed
and the vacuum gauge was observed to ensure no vacuum loss occurs. If the vacuum reading
remained the same, the shut-in test was considered successful. If vacuum loss occurred, the flow
regulator and/or brass cap and flow regulator were re-seated and the shut-in test was repeated
until the vacuum reading remained stable. Each canister passed the shut-in test criteria.

Following successful shut-in tests, each Summa® canister was connected to the Teflon® sample
tubing using a brass nut and ferrule assembly to create an airtight seal and the leak check was
performed. The leak check was performed by constructing a shroud over the sampling train and
flooding the shroud with helium gas. Helium concentrations inside the shroud were measured
using a helium gas detector and maintained at concentrations ranging from approximately 10%
to 16%. Once helium concentrations stabilized within the shroud, the sample tubing was purged
outside of the shroud using a syringe and a three-way valve to collect purged soil gas into a
Tedlar® bag. The purged soil gas was then analyzed using the helium gas detector to ensure that
helium concentrations in the soil gas sample were less than 10% of the helium concentrations
measured within the shroud. Each sub-slab soil gas sampling point passed the helium leak check
criteria.

Following successful leak checks, the sub-slab soil gas samples were collected by opening the
intake valve on the Summa® canister flow regulator. Vacuum readings for the Summa® canister
were recorded prior to and following the sampling period to ensure adequate sample volume was
collected. A vacuum of approximately 5 inches of mercury or more were maintained within the
canisters at the conclusion of the sampling event in accordance with DEQ DWM Vapor Intrusion
Guidance. Following sample collection, the Summa® canisters were delivered to SGS North
America, Inc. (SGS) under standard chain-of-custody protocols for analysis of VOCs by EPA
Method TO-15. Upon receipt of the samples, the laboratory recorded the final received vacuum
pressure for each Summa® canister.

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After sampling was complete, the sample locations were estimated by measuring from known
benchmarks within the Site building. The sample locations were permanently abandoned and the
surfaces were repaired similar to pre-drilling conditions.

6.2 Soil Gas Sampling Results

Laboratory analytical results for the sub-slab soil gas samples were compared to the DEQ Non-
Residential Vapor Intrusion SGSLs dated January 2023. A summary of the analytical results is
provided as Table 4, and copies of the laboratory analytical data reports and chain of custody
records are included as Appendix C.

Laboratory analytical results of the sub-slab soil gas samples indicate the presence of VOCs at
concentrations above the laboratory reporting limits in each sub-slab soil gas sample. No
organic compounds were detected at concentrations exceeding DEQ Non-Residential Vapor
Intrusion SGSLs in the sub-slab soil gas samples collected at the Site.

It should be noted that low level concentrations of PCE (up to 222 µg/m3) and TCE (up to 98.9
µg/m3) were detected above the laboratory method detection limits but below the DEQ Non-
Residential Vapor Intrusion in sub-slab soil gas samples collected at the Site.

6.3 Vapor Intrusion Evaluation

The DEQ Vapor Intrusion SGSLs are very conservative and based upon a Target Cancer Risk
(TCR) of 1 x 10-6 for potential carcinogenic effects and a Target Hazard Quotient (THQ) of 0.2
for potential non-carcinogenic effects. Vapor intrusion mitigation or additional assessment is not
typically warranted if the calculated cumulative lifetime incremental carcinogenic risk (LICR) is
1 x 10-4 or less and the acceptable level for non-carcinogenic risk is a calculated cumulative
hazard index (HI) of 1.0 or less.

H&H utilized the DEQ Risk Calculator (January 2023) assuming a non-residential land use
scenario to further evaluate potential cumulative risks for the soil gas to indoor air vapor
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intrusion pathway for the existing Site building. To model the potential for vapor intrusion under
a hypothetical “worst-case” scenario, H&H conservatively calculated the cumulative risks using
the highest concentration of any compound detected or identified at an estimated concentration
by the laboratory in any sub-slab soil gas sample collected at the Site. Risk calculator results are
summarized in the table below. A copy of the completed risk calculator is provided in
Appendix E.

As shown in the table above, risk calculator results indicate that under a hypothetical worst-case
scenario for the soil gas to indoor air vapor intrusion pathway for non-residential use, the
cumulative LICR and the cumulative HI are within acceptable threshold limits and indicate that
the risk of potential vapor intrusion at unacceptable levels for the existing Site building is low.
Based on the risk calculator results and the intended commercial/industrial use of the existing
Site building, a vapor mitigation system does not appear to be warranted for the Site building.

Brownfields assessment results indicate that TCE was not detected at a concentration above the
laboratory method detection limits in shallow soil samples collected in landscaped or unpaved
areas of the Site. Results of the Brownfields assessment activities confirm TCE was detected at
a concentration above the 2L Standard and the DEQ Non-Residential Vapor Intrusion GWSLs in
one groundwater sample collected from existing monitoring well OFF-MW-5 located in the
southwestern portion of the Site. Results of the Brownfields sub-slab soil gas sampling activities
indicate concentrations of TCE (up 98.9 µg/m3) were detected above the laboratory method
detection limits, but below the DEQ Non-Residential Vapor Intrusion SGSLs.

Based on the results of the 2023 Brownfields soil gas assessment activities, the TCE detections
in groundwater do not appear to pose a potential vapor intrusion concern at unacceptable levels.
Section 4.3 of the DWM Vapor Intrusion Guidance (March 2018) states as follows: "If soil gas
Evaluation Area Land Use
Scenario
Calculated
Cumulative
LICR
Calculated
Cumulative HI
Exceedance of
Acceptable
Levels?
Site-Wide Non-Residential 5.6 x 10-7 0.15 No
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and/or indoor air data has already been collected, using screening levels for those media are more
appropriate, however, groundwater data may still be used to screen other areas of the site that
may need to be investigated for potential VI." Therefore, consistent with the Vapor Intrusion
Guidance, the soil gas sampling results are more appropriate for evaluating vapor intrusion risks,
and utilizing the groundwater results to impose additional sampling requirements related to TCE
would not follow the conceptual Site model outlined in the DWM Vapor Intrusion Guidance and
generally accepted industry practices.

Furthermore, based on the concentrations of TCE in sub-slab soil gas samples at levels which do
not exceed the DEQ Non-Residential Vapor Intrusion SGSLs and cumulative carcinogenic and
noncarcinogenic risks are within acceptable threshold limits of the hypothetical worst-case
scenario for the soil gas to indoor air vapor intrusion pathway for non-residential use, no further
vapor intrusion sampling or vapor mitigation appear to be warranted.
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7.0 Quality Assurance – Quality Control

For quality assurance and quality control purposes (QA/QC), non-dedicated equipment and tools
were decontaminated prior to use at each boring or sampling location and following exposure to
soil or groundwater. Field QA/QC samples were analyzed along with the investigative samples
to determine potential variability introduced in sampling, handling, shipping, and analysis. One
trip blank was submitted for analysis of VOCs by EPA Method 8260. In addition, H&H
collected duplicate soil, groundwater, and soil gas samples to evaluate the ability of the laboratory
to reproduce sample results. Duplicate samples were submitted to the laboratory for the same
analysis as the corresponding parent sample.

7.1 Trip Blank

The trip blank was prepared by the laboratory and consisted of certified-clean sample containers
filled with analyte-free water. The trip blank accompanied the empty laboratory sample
containers to the Site, remained within the sample cooler during sampling, and traveled back to
the laboratory with field samples. The purpose of a trip blank is to evaluate sample handling
conditions and the potential for external contaminants to compromise investigative samples
during transit. One trip blank accompanied the field VOC groundwater samples and were
submitted for laboratory analysis of VOCs by EPA Method 8260. No VOC constituents were
identified above laboratory method detection limits in the trip blank. Laboratory analytical
results of the trip blank are included in the laboratory analytical reports provided in Appendix C.

7.2 Field Duplicates

Duplicate samples were collected to evaluate the precision of the field sampling procedures,
sample matrix variability, and analytical reproducibility. Duplicate soil and groundwater
samples were collected directly into individual laboratory supplied sample containers using
sampling methodologies described in previous sections. The duplicate soil gas samples were
collected concurrently with the parent samples using a laboratory supplied T-fitting which allows
for collection of two soil gas samples from one soil gas sampling point simultaneously. The
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samples were analyzed for the same parameters as the parent samples, and the analytical results
were compared with those of the parent samples. The analytical results of the parent samples
and the duplicate samples were used to evaluate the cumulative precision of the analytical
method, sample matrix, and sample collection techniques.

Duplicate sample laboratory analytical results for each sample media are presented in the
summary tables (Table 1 for soil, Table 3 for groundwater, and Table 4 for soil gas). Review of
the duplicate sample results for the soil, groundwater, and soil gas samples did not indicate
significant variability compared with the results of the parent samples.

7.3 Investigation Derived Waste

Investigation derived waste (IDW) was generated during the Brownfields assessment activities
and was managed in general accordance with DEQ IHSB Guidelines and the DEQ-approved
Work Plan. IDW soil and water generated during the assessment activities was thin spread on-
Site as there were no evidence of significant impacts in the borings and therefore, no additional
samples were collected.
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8.0 Summary and Conclusions

H&H completed Brownfields assessment activities at the George Fern Company Brownfields
property located at 2310 Old Steele Creek Road Drive in Charlotte, North Carolina. The
assessment activities were conducted in general accordance with the DEQ Brownfields approved
Work Plan dated February 3, 2023. Brownfields assessment activities included collection of soil,
groundwater, and sub-slab soil gas samples for laboratory analysis to further evaluate the
potential for impacts associated with historical off-Site operations and for the protection of Site
workers. In addition, a receptor survey was completed at the Site and in the nearby area to
obtain information about land use, water supply, basements, underground utilities, drains, and
surface water bodies in the vicinity of the Site. A brief summary of the Brownfields assessment
activities is provided below.

 The results of the receptor survey indicate that the Site is located in a mixed industrial
and residential use area of Charlotte. H&H identified two (2) active water supply wells
and four (4) inactive water supply wells within 1,500 ft of the Site. Surface water
features were not observed at the Site.

 Results of soil assessment activities completed at the Site did not identify compounds of
concern at concentrations above the DEQ Industrial/Commercial PSRGs or naturally
occurring levels in the case of metals.

 Results of the groundwater assessment activities identified the presence of PCE at
concentrations above the 2L Standard and/or the DEQ Non-Residential Vapor Intrusion
GWSLs in upgradient and downgradient monitoring wells. TCE was detected at
concentrations above the 2L Standard and DEQ Non-Residential Vapor Intrusion GWSL
in a sample collected from a downgradient area of the Site.

 Results of the sub-slab soil gas assessment activities completed within the existing Site
building did not identify compounds of concern at concentrations exceeding the DEQ
Non-Residential Vapor Intrusion SGSLs. PCE and TCE were detected in several soil gas
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points above the laboratory method detection limits, but below the DEQ Non-Residential
Vapor Intrusion SGSLs. Results of cumulative risk calculations utilizing the highest
concentration of any compound detected or identified at an estimated concentration by
the laboratory in any sub-slab soil gas sample confirm that the cumulative carcinogenic
and noncarcinogenic risks are below the DEQ and EPA unacceptable levels.

In summary, results of soil assessment activities do not indicate significant impacts in Site soil.
Should redevelopment activities be completed in the future, soil at the Site can be managed in
accordance with a DEQ Brownfields approved Environmental Management Plan (EMP).

Results of groundwater sampling activities confirm the presence of chlorinated solvent impacts
at concentrations above the applicable regulatory screening levels and are associated with
historical off-Site operations. Based on the adaptive reuse of the Site building, groundwater will
not be encountered. Should redevelopment activities be completed in the future, groundwater
can safely be managed in accordance with a DEQ-approved EMP, if encountered.

Results of sub-slab soil gas sampling did not identify compounds of concern at concentrations
above the DEQ Non-Residential Vapor intrusion SGSLs. In addition, the hypothetical worst-
case risk calculator results for soil gas to indoor air vapor intrusion pathways do not exceed
unacceptable risk levels for non-residential use. Therefore, further vapor intrusion sampling and
a vapor intrusion mitigation system does not appear to be warranted for the existing Site
building.

Table 1 Summary of Soil Analytical Data George Fern Company Charlotte, North Carolina H&H Job No. FDI-001Evaluation AreaScreening CriteriaSample IDBF-SB-01Date3/7/2023Sample TypeGrab Composite Grab Composite Grab Grab GrabDepth (ft bgs)0-2 0-2 0-2 0-2 0-2 0-2 2-4UnitsVOCs (8260D)1,4-Dichlorobenzene <0.0021 NA <0.0018 NA <0.0019 <0.0020.0037 J12----Chloromethane <0.068NA<0.0059NA0.0079 J, C8<0.0063<0.006199----Tetrachloroethene<0.0025NA0.0119NA<0.0023<0.0024<0.002382----SVOCs (8270E)NAALL BDLNAALL BDLALL BDLALL BDLALL BDL------Metals (6020B/7471B/7199)ArsenicNA2.6NA2.7 1.5 1.7 1.6 3.0 1.9 - 2.11.0 - 18Barium NA51.0NA80.546.445.176.747,00042.6 - 59.350 - 1000Cadmium NA0.038 JNA0.051 J<0.039<0.037<0.03820ND 1.0 - 10Chromium (Total) NA39.0NA65.666.889.048.6NE20.7 - 47.27.0 - 300Chromium (VI)NA1.45NA0.965 J0.741 J0.522 J0.734 J6.50.992 J - 1.54NSChromium (III)NA37.5NA64.666.188.547.9350,00019.2 - 46.1NSLeadNA8.6NA13.07.76.99.880010.9 - 11.1ND - 50Mercury NA0.073NA0.0580.0390.0330.074700.044 - 0.0650.03 - 0.52SeleniumNA0.66NA0.60 J0.65 J0.680.47 J1,2000.57 J - 0.60 J<0.1 - 0.8SilverNA<0.26NA<0.25<0.27<0.25<0.261,200ND - 0.26ND - 5.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023.2) Range values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern and Conterminous U.S. Soils. Concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits. Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above. Trivalent chromium concentrations are calculated.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface NS = not specified; NE = not established; -- = not applicable; BDL = below laboratory method detection limitJ = Compound detected above laboratory method detection limit, but below laboratory reporting limit resulting in a laboratory estimated concentration.C8 = Reported concentration may be biased high due to carryover from previously analyzed sample.Site-Specific RangePublished Range (2)Gravel Parking AreaCOMP-1 COMP-2 BF-SB-01 / BF-SB-DUPIndustrial/ Commercial PSRGs (1)3/7/20233/7/20233/7/2023Background Metals mg/kgShallow Soilhttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Furniture Distributors, Inc. (FDI)/FDI-001/Brownfields/BF Assessment/Tables/Table 1Table 1 (Page 1 of 2)Hart & Hickman, PC
Table 1 Summary of Soil Analytical Data George Fern Company Charlotte, North Carolina H&H Job No. FDI-001Evaluation AreaScreening CriteriaSample IDBF-BG-01 BF-BG-02Date3/7/2023 3/7/2023Sample TypeGrab Grab Grab GrabDepth (ft bgs)0-2 2-4 0-2 0-2UnitsVOCs (8260D)1,4-Dichlorobenzene <0.0019 <0.0019 NA NA12-- --Chloromethane 0.0063 J, C8 <0.0062NANA99----Tetrachloroethene<0.0024<0.0023NANA82----SVOCs (8270E)ALL BDL ALL BDL NANA------Metals (6020B/7471B/7199)Arsenic2.91.82.11.93.01.9 - 2.11.0 - 18Barium 28.06459.342.647,00042.6 - 59.350 - 1000Cadmium <0.036<0.036<0.037<0.03720ND 1.0 - 10Chromium (Total) 44.23647.220.7NE20.7 - 47.27.0 - 300Chromium (VI)1.11 J0.719 J0.992 J1.546.50.992 J - 1.54NSChromium (III)43.135.346.119.2350,00019.2 - 46.1NSLead7.77.610.911.180010.9 - 11.1ND - 50Mercury 0.150.0480.0440.065700.044 - 0.0650.03 - 0.52Selenium0.70.60 J0.57 J0.60 J1,2000.57 J - 0.60 J<0.1 - 0.8Silver<0.25<0.25<0.25<0.261,200ND - 0.26ND - 5.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023.2) Range values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern and Conterminous U.S. Soils. Concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits. Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above. Trivalent chromium concentrations are calculated.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface NS = not specified; NE = not established; -- = not applicable; BDL = below laboratory method detection limitJ = Compound detected above laboratory method detection limit, but below laboratory reporting limit resulting in a laboratory estimated concentration.C8 = Reported concentration may be biased high due to carryover from previously analyzed sample.BF-SB-02Background Metals Site-Specific RangePublished Range (2)mg/kgIndustrial/ Commercial PSRGs (1)3/7/2023Gravel Parking AreaBackgroundhttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Furniture Distributors, Inc. (FDI)/FDI-001/Brownfields/BF Assessment/Tables/Table 1Table 1 (Page 2 of 2)Hart & Hickman, PC
Table 2Summary of Well Construction and Groundwater Elevation DataGeorge Fern CompanyCharlotte, North CarolinaH&H Job No. FDI-001Well IDTotal Well Depth (ft bgs)Screen Interval (ft) TOC Elevation (ft MSL) Depth to Groundwater (ft bTOC)Groundwater Elevation (ft MSL) OFF-MW-1 unknownunknown738.4517.02721.43OFF-MW-43015-30738.44OFF-MW-53722-37742.1622.64719.52OFF-MW-64833-48753.2232.42720.80OFF-MW-7249-24735.8718.06717.81OFF-MW-82510-25742.14OFF-MW-9S2510-25737.4215.54721.88OFF-MW-9D5045-50737.4115.62721.79MW-10S3217-32740.4417.43723.01MW-10D6358-63740.7318.05722.68MW-11S4025-40746.3223.83722.49MW-11D7469-74746.0223.67722.35BMW-110590-105742.6221.08721.54Notes:Depth to groundwater measurements collected by H&H on March 5, 2023.Well information obtained from Technical Memorandum: Phase I Remedial Investigation Summary prepared by H&H dated July 26, 2012. ft bgs = feet below ground surface; ft bTOC = feet below top of casing; ft MSL = feet above mean sea levelNot Located Not Located https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Furniture Distributors, Inc. (FDI)/FDI-001/Brownfields/BF Assessment/Tables/Data Tables4/26/2023Table 2 (Page 1 of 1)Hart & Hickman, PC
Table 3Summary of Groundwater Analytical DataGeorge Fern CompanyCharlotte, North CarolinaH&H Job No. FDI-001Evaluation AreaDowngradientCross-GradientSample IDOFF-MW-6MW-11SOFF-MW-5OFF-MW-7Date3/7/20233/6/20233/6/20233/6/2023UnitsVOCs (8260D)Chloroform<0.86<0.860.71 J<0.43<4.3<0.43703.6cis-1,2-Dichloroethene<0.77<0.77<0.38<0.3826.3<0.3870210Tetrachloroethene18619012.61.2932<0.290.7 48Trichloroethene<0.77 <0.772.2<0.3854.3<0.3834.4SVOCs (8270E)ALL BDLALL BDLALL BDLALL BDLALL BDLALL BDL----Metals (6020B/7470A)Arsenic<0.087<0.0870.12 J0.20 J<0.0870.17 J10NEBarium59.861.414.017.031.272.6700NECadmium<0.060<0.060<0.060<0.060<0.060<0.0602NEChromium4.44.14.80.82 J3.4<0.5010NELead<0.077<0.0770.31 J0.18 J<0.0770.091 J15NEMercury<0.12<0.12<0.12<0.12<0.12<0.1210.75Selenium<0.072<0.0720.16 J0.13 J<0.0720.11 J20NESilver<0.070<0.070<0.070<0.070<0.40<0.07020NENotes:1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) dated April 2022.2)DEQ Vapor Intrusion Groundwater Screening Levels (GWSLs) dated January 2023.Concentrations are reported in micrograms per liter (µg/L).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.Bold values exceed the 2L Standard.Underlined values exceed the Non-Residential Vapor Intrusion GWSL.VOC = volatile organic compound; SVOC = semi-volatile organic compound; NE = not established; -- = not applicable; BDL = below laboratory method detection limits J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.Non-Residential GWSLs (2)Screening Criteria 2L Standards (1)OFF-MW-1/GW-DUPµg/L3/6/2023Upgradient https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Furniture Distributors, Inc. (FDI)/FDI‐001/Brownfields/BF Assessment/Tables/Data Tables4/26/2023Table 3 (Page 1 of 1)Hart & Hickman, PC
Table 4Summary of Sub-Slab Soil Gas Analytical Data George Fern CompanyCharlotte, North CarolinaH&H Job No. FDI-001Evaluation AreaScreening CriteriaSample IDBF-SSV-01 BF-SSV-02 BF-SSV-03 BF-SSV-04 BF-SSV-05BF-SSV-06BF-SSV-07BF-SSV-08Sample Date3/8/20233/8/20233/8/20233/8/20233/8/20233/8/20233/8/20233/8/2023Sample Type UnitsVOCs (TO-15)Acetone30.6 113 56.3 35.9 35.2 35.2 40.6 36.3NEBenzene<0.801.2 J<0.80<0.80<0.80<0.80<0.80<0.801602-Butanone (MEK)2.8<1.33.5<1.3<1.3<1.33.2<1.3440,000Cyclohexane<1.51.9 J<1.5<1.51.8 J<1.51.6 J<1.5530,000Dichlorodifluoromethane2.0 J2.0 J2.3 J2.2 J2.2 J2.2 J2.4 J2.1 J8,800Ethyl acetate<1.5156.5<1.5<1.5<1.5<1.5<1.56,100Ethylbenzene<1.05.2<1.0<1.0<1.0<1.0<1.0<1.0490Isopropyl alcohol5.2121712107.49.31218,000Methylene Chloride<0.769.75.910<0.765.96.36.653,000Naphthalene<2.7<2.7<2.7<2.7<2.7<2.7<2.7<2.736n-Hexane<1.6<1.6<1.61.9 J<1.6<1.61.7 J1.6 J61,000Propylene<0.98<0.98<0.98<0.98<0.98<0.98<0.98<0.98260,000Tetrachloroethene4953147832521430392403,500Tetrahydrofuran<1.1<1.1<1.1<1.1<1.1<1.1<1.1<1.1180,000Toluene1.5 J172.6 J2.0 J2.3 J3.02.1 J2.1 J440,000Trichloroethene5.95.1384.7158.13.37.5180Xylene (total)<1.37.8<1.3<1.3<1.3<1.3<1.3<1.38,800Notes:1) North Carolina Department of Environmental Quality (DEQ) Vapor Intrusion Sub-Slab & Exterior Soil Gas Screening Levels (SGSLs) dated January 2023.Concentrations are reported in micrograms per cubic meter (µg/m3).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses.Only compounds detected in at least one sample are shown in the table above.VOCs = volatile organic compounds; NE = not establishedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.µg/m3Non-Residential SGSLs (1)Existing Site Building Sub-Slab https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Furniture Distributors, Inc. (FDI)/FDI‐001/Brownfields/BF Assessment/Tables/Data Tables4/26/2023Table 4 (Page 1 of 2)Hart & Hickman, PC
Table 4Summary of Sub-Slab Soil Gas Analytical Data George Fern CompanyCharlotte, North CarolinaH&H Job No. FDI-001Evaluation AreaScreening CriteriaSample IDBF-SSV-09 BF-SSV-10 BF-SSV-12Sample Date3/8/2023 3/13/2023 3/8/2023Sample Type UnitsVOCs (TO-15)Acetone35.4 20 30.2 28.0 38.2NEBenzene<0.80<0.80<0.80<0.80<0.801602-Butanone (MEK)<1.3<1.3<1.3<1.31.8 J440,000Cyclohexane<1.5<1.5<1.5<1.51.7 J530,000Dichlorodifluoromethane2.1 J2.1 J2.1 J2.1 J2.7 J8,800Ethyl acetate<1.542.543.657.9<1.56,100Ethylbenzene<1.0<1.0<1.0<1.0<1.0490Isopropyl alcohol119.111119.118,000Methylene Chloride9.09.78.34.95.653,000Naphthalene<2.7<2.7<2.7<2.74.0 J36n-Hexane<1.62.2 J2.81.7 J<1.661,000Propylene<0.98<0.985.5<0.98<0.98260,000Tetrachloroethene222602.12.0503,500Tetrahydrofuran<1.1<1.15.6<1.1<1.1180,000Toluene2.9 J2.5 J1.6 J1.7 J<0.87440,000Trichloroethene5.22.4<0.41<0.4198.9180Xylene (total)<1.3<1.3<1.3<1.3<1.38,800Notes:1) North Carolina Department of Environmental Quality (DEQ) Vapor Intrusion Sub-Slab & Exterior Soil Gas Screening Levels (SGSLs) dated January 2023.Concentrations are reported in micrograms per cubic meter (µg/m3).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses.Only compounds detected in at least one sample are shown in the table above.VOCs = volatile organic compounds; NE = not establishedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.Non-Residential SGSLs (1)BF-SSV-11/BF-SSV-DUP3/13/2023Sub-Slab Existing Site Building µg/m3https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Furniture Distributors, Inc. (FDI)/FDI‐001/Brownfields/BF Assessment/Tables/Data Tables4/26/2023Table 4 (Page 2 of 2)Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset, andNational Transportation Dataset; USGS Global Ecosystems; U.S. CensusBureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S.Department of State Humanitarian Information Unit; and NOAA NationalCenters for Environmental Information, U.S. Coastal Relief Model. Datarefreshed June, 2022.
SITE LOCATION MAP
GEORGE FERN COMPANY2310 OLD STEELE CREEK ROADCHARLOTTE, NORTH CAROLINA
DATE: 5-30-23
JOB NO: FDI-001
REVISION NO: 1
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: S:\AAA-Master Projects\Furniture Distributors, Inc. (FDI)\FDI-001\Brownfields\BF Assessment\Report\Figures\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
CHARLOTTE WEST, NORTH CAROLINA 2019
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
OLD STEELE CREEK ROADOFF-MW-3
OFF-MW-6
OFF-MW-5
OFF-MW-7
OFF-MW-8
MW-15D
MW-14D
MW-10S
MW-11S
OFF-MW-4
MW-13D
MW-10D
MW-12D
OFF-MW-9D
BMW-1
MW-1
MW-2
MW-13S
MW-12S
OFF-MW-9S
MW-11D
PRI
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A
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WILL
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S
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FABER STREETOFFICE
TOLLESON + SAUL DESIGN(2300 OLD STEEL CREEK ROAD)
CAROLINA GOLF CLUB(2415 OLD STEELE CREEK ROAD)
PATRIOT TRANSPORT, INC.(22466 OLD STEELE CREEK ROAD)
WOODED LAND/RESIDENCES
VACANT LAND(3600 PRIMROSE AVENUE)
MW-3R
MW-4
TELECOMMUNICATIONSCOMPOUND WITH GENERATOR
STORMWATER DETENTION POND
REVISION NO. 0
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL LINE
RAILROAD
SHALLOW MONITORING WELL
DEEP MONITORING WELL
BEDROCK MONITORING WELL
ABANDONED SHALLOW MONITORING WELL
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURGCOUNTY GIS, DATED 2023.
2. BASE DATA OBTAINED FROM MECKLENBURG COUNTYGIS (2021).
3. MONITORING WELLS MW-1 THROUGH MW-4 INSTALLEDBY ERM IN 1997.
4. MONITORING WELLS OFF-MW-1 THROUGH OFF-MW-3INSTALLED BY S&ME, INC. IN 2005. MONITORING WELLSOFF-MW-4 THROUGH OFF-MW-6 INSTALLED BY PARSONSIN 2008. MONITORING WELLS OFF-MW-7 THROUGH
OFF-MW-9D WERE INSTALLED IN 2010.
5. MONITORING WELLS MW-10S/D AND MW-11S/D WEREINSTALLED IN 2012.
6. MONITORING WELLS MW-12S/D, MW-13S/D, MW-14D, ANDMW-15D WERE INSTALLED IN 2011.
JOB NO. FDI-001
DATE: 5-30-23
FIGURE NO. 2
SITE MAP
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
GEORGE FERN COMPANY
2310 OLD STEELE CREEK ROAD
CHARLOTTE, NORTH CAROLINA
OFF-MW-6
OFF-MW-5
MW-11S
OFF-MW-7
OFF-MW-1
S:\AAA-Master Projects\Furniture Distributors, Inc. (FDI)\FDI-001\Brownfields\BF Assessment\Report\Figures\Figures 20210510.dwg, FIG2, 5/1/2023 10:19:43 AM, tmarbuery
OLD STEELE CREEK ROADOFF-MW-6
OFF-MW-5
OFF-MW-7
OFF-MW-8
MW-15D
MW-14D
MW-10S
MW-11S
OFF-MW-1
OFF-MW-4
MW-13D
MW-10D
MW-12D
OFF-MW-9D
BMW-1
MW-1
MW-2
MW-13S
MW-12S
OFF-MW-9S
MW-11D
PRIM
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A
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N
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WILL
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FABER STREETTOLLESON + SAUL DESIGN(2300 OLD STEEL CREEK ROAD)
CAROLINA GOLF CLUB(2415 OLD STEELE CREEK ROAD)
PATRIOT TRANSPORT, INC.(22466 OLD STEELE CREEK ROAD)
WOODED LAND/RESIDENCES
VACANT LAND(3600 PRIMROSE AVENUE)
MW-3R
MW-4
TELECOMMUNICATIONSCOMPOUND WITH GENERATOR
BF-SSV-1
BF-SSV-3
BF-BG-1
BF-BG-2
STORMWATER DETENTION POND
COMP-1
COMP-2
BF-SSV-4
BF-SSV-7
BF-SSV-12
BF-SSV-2
BF-SSV-5
BF-SSV-8
BF-SSV-11BF-SSV-6
BF-SSV-9
BF-SSV-10
BF-SB-01
BF-SB-02
REVISION NO. 0
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL LINE
RAILROAD
SHALLOW MONITORING WELL
DEEP MONITORING WELL
BEDROCK MONITORING WELL
ABANDONED SHALLOW MONITORING WELL
SUB-SLAB VAPOR POINT
SOIL BORING
ALIQUOT SOIL BORING
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURG COUNTY GIS, DATED 2023.
2. BASE DATA OBTAINED FROM MECKLENBURG COUNTY
GIS (2021).
3. MONITORING WELLS MW-1 THROUGH MW-4 INSTALLED BY ERM IN 1997.
4. MONITORING WELLS OFF-MW-1 THROUGH OFF-MW-3 INSTALLED BY S&ME, INC. IN 2005. MONITORING WELLS
OFF-MW-4 THROUGH OFF-MW-6 INSTALLED BY PARSONS IN 2008. MONITORING WELLS OFF-MW-7 THROUGH OFF-MW-9D WERE INSTALLED IN 2010.
5. MONITORING WELLS MW-10S/D AND MW-11S/D WERE INSTALLED IN 2012.
6. MONITORING WELLS MW-12S/D, MW-13S/D, MW-14D, AND MW-15D WERE INSTALLED IN 2011.
JOB NO. FDI-001
DATE: 5-30-23
FIGURE NO. 3
GEORGE FERN COMPANY2310 OLD STEELE CREEK ROADCHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
OFFICE
S:\AAA-Master Projects\Furniture Distributors, Inc. (FDI)\FDI-001\Brownfields\BF Assessment\Report\Figures\Figures 20210510.dwg, FIG3, 5/1/2023 10:20:44 AM, tmarbuery
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RECEPTOR SURVEY MAP
GEORGE FERN COMPANY2310 OLD STEELE CREEK ROADCHARLOTTE, NORTH CAROLINA
REVISION NO: 0
FIGURE NO: 4
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
0 500 1,000
SCALE IN FEET
N
DATE: 5-30-23
JOB NO. FDI-001
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURGCOUNTY, 2023.2. PARCEL DATA OBTAINED FROM NC ONEMAP, 202233. ZONING DATA OBTAINED FROM MECKLENBURGCOUNTY, 2021.
1,500 FOOT RADIUS
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
SURFACE WATER FEATURE
BUSINESS ZONING
INDUSTRIAL ZONING
RESIDENTIAL ZONING
SITE BUILDING OUTLINE
\\harthick.sharepoint.com@SSL\DavWWWRoot\sites\MasterFiles-1\Shared Documents\AAA-Master Projects\Furniture Distributors, Inc. (FDI)\FDI-001\Brownfields\BF Assessment\Receptor\CAD files\RECEPTOR_SURVEY.mxdINSET1" = 450'
TITLE
PROJECT
UNNAMED TRIBUTARY TO TAGGART CREEK
GAS LINE
UNDERGROUND UTILITY
WATER LINE
SANITARY SEWER LINE
FIBER LINE
OVERHEAD ELECTRIC LINE
F
SS
G/U
GAS
W
O/H
PARCEL BOUNDARY LINE
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PREMANENTLY ABANDONED WATER SUPPLY WELL
UNNAMED TRIBUTARY
TO TAGGART CREEK
UNNAMED TRIBUTARY
TO TAGGART CREEK
UNNAMED PONDS AT CAROLINA GOLF CLUB
(2415 OLD STEELE CREEK ROAD)
NANA'S NURSERY(2734 WINGATE AVENUE)
&,`INACTIVE WATER SUPPLY WELL
OLD STEELE CREEK ROADOFF-MW-3
OFF-MW-6
OFF-MW-5
OFF-MW-7
OFF-MW-8
MW-15D
MW-14D
MW-10S
MW-11S
OFF-MW-1
OFF-MW-4
MW-13D
MW-10D
MW-12D
OFF-MW-9D
BMW-1
MW-1
MW-2
MW-13S
MW-12S
OFF-MW-9S
MW-11D
PRI
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A
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N
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WILL
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W

S
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FABER STREETOFFICE
TOLLESON + SAUL DESIGN(2300 OLD STEEL CREEK ROAD)
MW-3R
MW-4
STORMWATER DETENTION POND
REVISION NO. 0
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL LINE
RAILROAD
SHALLOW MONITORING WELL
DEEP MONITORING WELL
BEDROCK MONITORING WELL
ABANDONED SHALLOW MONITORING WELL
GROUNDWATER ELEVATION CONTOUR(FT MSL)
GROUNDWATER ELEVATION (FT MSL)
APPROXIMATE GROUNDWATERFLOW DIRECTION
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURG COUNTY GIS, DATED 2023.
2. BASE DATA OBTAINED FROM MECKLENBURG COUNTY GIS (2021).
3. DEPTH TO GROUNDWATER MEASURED BY H&H ON MARCH 5, 2023.
4. NM = NOT MEASUREDFT MSL = FEET ABOVE MEAN SEA LEVEL
JOB NO. FDI-001
DATE: 5-30-23
FIGURE NO. 5
SHALLOW GROUNDWATER
POTENTIOMETRIC MAP
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
GEORGE FERN COMPANY
2310 OLD STEELE CREEK ROAD
CHARLOTTE, NORTH CAROLINA
OFF-MW-6
MW-11S
(NM)
(723.01)
(721.88)
(NM)
(717.81)
720
722
718718720722OFF-MW-7
(719.52)OFF-MW-5
(720.80)
(722.49)
OFF-MW-1(721.43)
MW-10D
722
(721.43)\\harthick.sharepoint.com@SSL\DavWWWRoot\sites\MasterFiles-1\Shared Documents\AAA-Master Projects\Furniture Distributors, Inc. (FDI)\FDI-001\Brownfields\BF Assessment\Report\Figures\Figures 20210510.dwg, FIG5, 5/12/2023 2:49:07 PM, tmarbuery

Appendix A

Brownfields Property Receptor Survey Form
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site:George Fern Company
Address:2310 Old Steele Creek Road
City:Charlotte
County:Mecklenburg
Brownfields Project Number: 25044-21-060
Property and Building Characteristics
a. Provide occupancy and use information.
The Site consists of asphalt-paved vehicle access and parking areas, concrete loading areas, and landscaped and

The Site building is constructed as a one-story industrial warehouse with stucco hardcoat exterior and multiple windows and loading bay doors.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
The foundation construction of the Site building consists of concrete commercial slab-on-grade.
The HVAC systems of the Site building are ducted forced air.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
No sub-slab ventilation systems are currently in place. It is unknown if a moisture barrier is currently in-place
beneath the Site building.
% of property that is wooded/brush
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as needed. If numerous buildings are on-
site, consult with your PM as only information on specific buildings may be needed.
b. Describe the construction of the building including materials (e.g. wood frame, block), type and size of openings (e.g. windows, bay doors), and height
(number of stories).
% of property that is covered by buildings
9.6
~25
~30
~30
vegetated areas. One approximate 60,000 sq ft industrial warehouse building is located in the south eastern portion of the Site.
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information requested below. Distances are
measured from the site property boundary unless otherwise indicated by the DEQ Brownfield’s Project Manager (PM).
Current Usage Proposed UsageSurface Conditions
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and design considerations (e.g.
positive pressure?).
0
~15
The PD has completed cosmetic interior upfit
activities (i.e. new carpeting, painting, etc.) and
utilizes the Site building for corporate offices and
distribution.
% of property that is grassed areas (unpaved)
% of property that is agricultural crops
% of property that is paved
Size of Property (acres)
Rev. 09/2015 Page 1 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
South
East/Southeast
West
Y ~1,200 S
Y<50N
None observed -- --
Utilities
Is there a septic system on-site? (Y or N) No
Please provide the utility providers for the subject property
a. Natural Gas: Piedmont Natural Gas (underground)
b. Sewer: Charlotte Water (underground)
c. Electricity: Duke Energy (above and below ground)
d. Other: Communication (underground)
For surrounding properties, please complete the following table with available information.
Y<10 S
Y<10 S
N-- --
Y<10 S
Y<10 S
Y<10 E
N-- NA
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
Is there a basement within 1,000 ft of the Property
Distance (ft) Address
2734 Wingate Avenue
Zoning/Land Use
See Figure 4 - Receptor Survey Map
--
Proposed Usage Current Use/Occupant
Is a school or daycare center within 1,000 ft of the Property?
DirectionUtility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject property.
NA
Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding areas. If specific receptors are
present, please provide addresses of the facilities.
NA
NA
NA
Industrial
Residential Single Family
Residential and Industrial
Industrial
For the subject property, please provide a map of known buried utilities. If available, include depth to top, construction material, and diameter of the utilities.
In addition, please provide the following information on utility providers. If additional assessment is required, the public utility locators should be contacted.
This information can then be added to a site map.
Y/N *
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses.
Distance
(ft)
Is a sanitary sewer within 100 ft of the Property boundary?
Is there a residence within 1,000 ft of the Property?
Rev. 09/2015 Page 2 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public X Private ______
Charlotte Water
N -- -- --
Y ~250 ft -
330 ft SW 2414 Old Steele Creek and 2838
Willow Street
N -- ----
Surface Water & Wetlands
Y/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a windshield survey within 1,500 ft of
the property boundaries should be completed to determine if water supply or irrigation wells may be present. Information from applicable databases can and
should be utilized; however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the requested radius, please provide a
map of the well locations. If needed, please attach a separate table to list all wells. Please note, the PM may opt for a more extensive water supply well survey
if needed.
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
Address
Provide Information regarding Surface Water and Wetlands
No
Are there surface water features on the property? (If yes,
please complete a. to d.)
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include the water providers name.
Distance
(ft)Direction
a. Is the water body naturally developed or man-made?
NA
NA
NA
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property boundary?
Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity of the Property.
NA
An unnamed tributary of Taggart Creek is located approximately 650 ft northwest of the Site.
No
b. List the uses of the water body.
c. What is the source of the water for the water body?
d. What is the nature of the bottom of the water body
(e.g., rocky or concrete bottom, drainage ways or
impoundments)
If no on-site surface water features, what is the nearest
surface water body?
Are there any wetlands present on the property? If no
wetlands on-site, are wetlands suspected on adjoining
properties?
Rev. 09/2015 Page 3 of 3

Appendix B

Boring Logs
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
BF-BG-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL)
(0.5') SILT (ML); some clay, medium stiff, moist, reddish, with organics (tree roots)
(2.5') SILT (ML); some clay, medium stiff, moist, brown and gray, with organics (tree
roots)
(5') Boring terminated
13.2
3.8
9.3
BF-BG-1
0
5
10
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
BF-BG-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL)
(0.5') SILT (ML); some clay, medium stiff, moist, reddish, with organics (tree roots)
(5') Boring terminated
33.2
11.3
12.0
BF-BG-2
0
5
10
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
BF-SB-01 / BF-SB-DUP
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Other
Hand Auger
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') Well-graded GRAVEL (GW)
(0.5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, reddish-brown
(5') Boring terminated
1.2
1.3
1.2
BF-SB-01(2-4)
0
5
10
BF-SB-01(0-2)
BF-SB-DUP
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
BF-SB-02
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Other
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') Well-graded GRAVEL (GW)
(0.5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, reddish-brown
(5') Boring terminated
1.6
1.6
1.5
BF-SB-02(2-4)
0
5
10
BF-SB-02(0-2)
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
COMP-1A
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL); grass
(0.5') SILT (ML); some clay, medium stiff, moist, reddish
(5') Boring terminated
5.8
6.4
5.1
COMP-1
0
5
10
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
COMP-1B
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL); Grass
(0.5') SILT (ML); some clay, medium stiff, moist, reddish
(4') SILT (ML); some clay, medium stiff, wet, light brown and black
(5') Boring terminated
4.2
3.8
4.8
0
5
10
COMP-1
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
COMP-1C
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL); Grass
(0.5') SILT (ML); some clay, medium stiff, moist, reddish
(0.5') SILT (ML); some clay, medium stiff, moist, brown
(5') Boring terminated
0.8
2.4
4.1
0
5
10
COMP-1
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
COMP-1D
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL)
(0.5') SILT (ML); some clay, medium stiff, moist, reddish, white mottling, trace
organics (tree roots)
(3) SILT (ML); some clay, medium stiff, moist, light brown and gray, trace
organics (tree roots)
(5') Boring terminated
5.1
2.8
3.5
0
5
10
COMP-1
NOTES: VOC Grab sample collected from COMP-1E (0-2).
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
COMP-1E
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL)
(0.5') SILT (ML); some clay, medium stiff, moist, reddish, white mottling, trace
organics (tree roots)
(3) SILT (ML); some clay, medium stiff, moist, light brown and gray, trace
organics (tree roots)
(5') Boring terminated
7.0
5.1
5.6
0
5
10
COMP-1
NOTES: VOC Grab sample collected from COMP-2A (0-2).
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
COMP-2A
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Other
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL)
(0.5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist,
reddish brown
(5') Boring terminated
42.9
31.2
6.2
COMP-2
0
5
10
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
COMP-2B
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Other
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL)
(0.5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, brown,
with debris (glass)
(2') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, reddish
brown
(5') Boring terminated
11.6
5.0
3.6
COMP-2
0
5
10
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
COMP-2C
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Other
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL)
(0.5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist,
reddish brown
(5') Boring terminated
8.3
4.9
3.7
COMP-2
0
5
10
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
COMP-2D
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Other
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL)
(0.5') Lean CLAY (CL); some silt, some fine-medium grained sand, medium
plasticity, soft, moist, reddish brown
(5') Boring terminated
14.2
4.7
3.6
COMP-2
0
5
10
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Furniture Distributors Inc.
George Fern Company
2310 Steele Creek Road, Charlotte ,NC
BORING LOG
Boring No.
Page:
COMP-2E
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/7/23
3/7/23
Hart and Hickman
Other
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL)
(0.5') Lean CLAY (CL); some silt, some fine-medium grained sand, medium
plasticity, soft, moist, reddish
(5') Boring terminated
4.8
3.2
2.8
COMP-2
0
5
10

Appendix C

Laboratory Analytical Reports
#=CL#
March 15, 2023
LIMS USE: FR - HALEY MARTIN
LIMS OBJECT ID: 92655679
92655679
Project:
Pace Project No.:
RE:
Haley Martin
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
GEORGE FERN FDI-001
Dear Haley Martin:
Enclosed are the analytical results for sample(s) received by the laboratory on March 08, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 78
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
1800 Elm Street SE, Minneapolis, MN 55414--Satellite Air
Lab
A2LA Certification #: 2926.01*
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009*
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014*
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
Florida Certification #: E87605*
Georgia Certification #: 959
GMP+ Certification #: GMP050884
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086*
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064*
Maryland Certification #: 322
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137*
Minnesota Dept of Ag Approval: via MN 027-053-137
Minnesota Petrofund Registration #: 1240*
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081*
New Jersey Certification #: MN002
New York Certification #: 11647*
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification (A2LA) #: R-036
North Dakota Certification (MN) #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification (1700) #: CL101
Ohio VAP Certification (1800) #: CL110*
Oklahoma Certification #: 9507*
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001*
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192*
Utah Certification #: MN00064*
Vermont Certification #: VT-027053137
Virginia Certification #: 460163*
Washington Certification #: C486*
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
USDA Permit #: P330-19-00208
*Please Note: Applicable air certifications are denoted with
an asterisk (*).
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 78
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Pace Analytical Services National
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 78
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Lab ID Sample ID Matrix Date Collected Date Received
92655679001 COMP-1 (0-2)Solid 03/07/23 13:00 03/08/23 10:37
92655679002 COMP-2 (0-2)Solid 03/07/23 17:00 03/08/23 10:37
92655679003 BF-SB-01 (0-2)Solid 03/07/23 17:25 03/08/23 10:37
92655679004 BF-SB-02 (0-2)Solid 03/07/23 18:00 03/08/23 10:37
92655679005 BF-BG-1 (0-2)Solid 03/07/23 13:05 03/08/23 10:37
92655679006 BF-BG-2 (0-2)Solid 03/07/23 13:15 03/08/23 10:37
92655679007 BF-SB-DUP Solid 03/07/23 00:00 03/08/23 10:37
92655679008 BF-SB-01 (2-4)Solid 03/07/23 17:40 03/08/23 10:37
92655679009 BF-SB-02 (2-4)Solid 03/07/23 18:10 03/08/23 10:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 78
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92655679001 COMP-1 (0-2)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
92655679002 COMP-2 (0-2)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
92655679003 BF-SB-01 (0-2)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
92655679004 BF-SB-02 (0-2)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
92655679005 BF-BG-1 (0-2)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
ASTM D2974 1 PASI-MJDL
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
92655679006 BF-BG-2 (0-2)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
ASTM D2974 1 PASI-MJDL
SM 2540G 1 PANCMK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 78
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7199 1 PANSET
92655679007 BF-SB-DUP EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
92655679008 BF-SB-01 (2-4)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
92655679009 BF-SB-02 (2-4)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: COMP-1 (0-2)Lab ID: 92655679001 Collected: 03/07/23 13:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.6 mg/kg 03/14/23 16:07 7440-38-203/14/23 10:330.63 0.18 1
Barium 51.0 mg/kg 03/14/23 16:07 7440-39-303/14/23 10:330.38 0.095 1
Cadmium 0.038J mg/kg 03/14/23 16:07 7440-43-903/14/23 10:330.10 0.037 1
Chromium 39.0 mg/kg 03/14/23 16:07 7440-47-303/14/23 10:332.5 0.49 1
Lead 8.6 mg/kg 03/14/23 16:07 7439-92-103/14/23 10:330.63 0.12 1
Selenium 0.66 mg/kg 03/14/23 16:07 7782-49-203/14/23 10:330.63 0.13 1
Silver ND mg/kg 03/14/23 16:07 7440-22-403/14/23 10:330.63 0.26 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.073 mg/kg 03/14/23 11:33 7439-97-603/13/23 15:150.025 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 03/09/23 14:46 83-32-903/08/23 15:03438 154 1
Acenaphthylene ND ug/kg 03/09/23 14:46 208-96-803/08/23 15:03438 154 1
Aniline ND ug/kg 03/09/23 14:46 62-53-303/08/23 15:03438 171 1
Anthracene ND ug/kg 03/09/23 14:46 120-12-703/08/23 15:03438 143 1
Benzo(a)anthracene ND ug/kg 03/09/23 14:46 56-55-303/08/23 15:03438 146 1
Benzo(a)pyrene ND ug/kg 03/09/23 14:46 50-32-803/08/23 15:03438 151 1
Benzo(b)fluoranthene ND ug/kg 03/09/23 14:46 205-99-203/08/23 15:03438 146 1
Benzo(g,h,i)perylene ND ug/kg 03/09/23 14:46 191-24-203/08/23 15:03438 170 1
Benzo(k)fluoranthene ND ug/kg 03/09/23 14:46 207-08-903/08/23 15:03438 154 1
Benzoic Acid ND ug/kg 03/09/23 14:46 65-85-003/08/23 15:032190 942 1
Benzyl alcohol ND ug/kg 03/09/23 14:46 100-51-603/08/23 15:03876 332 1
4-Bromophenylphenyl ether ND ug/kg 03/09/23 14:46 101-55-303/08/23 15:03438 169 1
Butylbenzylphthalate ND ug/kg 03/09/23 14:46 85-68-703/08/23 15:03438 185 1
4-Chloro-3-methylphenol ND ug/kg 03/09/23 14:46 59-50-703/08/23 15:03876 308 1
4-Chloroaniline ND ug/kg 03/09/23 14:46 106-47-803/08/23 15:03876 344 1
bis(2-Chloroethoxy)methane ND ug/kg 03/09/23 14:46 111-91-103/08/23 15:03438 182 1
bis(2-Chloroethyl) ether ND ug/kg 03/09/23 14:46 111-44-403/08/23 15:03438 165 1
2-Chloronaphthalene ND ug/kg 03/09/23 14:46 91-58-703/08/23 15:03438 174 1
2-Chlorophenol ND ug/kg 03/09/23 14:46 95-57-803/08/23 15:03438 165 1
4-Chlorophenylphenyl ether ND ug/kg 03/09/23 14:46 7005-72-303/08/23 15:03438 163 1
Chrysene ND ug/kg 03/09/23 14:46 218-01-903/08/23 15:03438 159 1
Dibenz(a,h)anthracene ND ug/kg 03/09/23 14:46 53-70-303/08/23 15:03438 169 1
Dibenzofuran ND ug/kg 03/09/23 14:46 132-64-903/08/23 15:03438 158 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 14:46 95-50-103/08/23 15:03438 158 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 14:46 541-73-103/08/23 15:03438 155 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 14:46 106-46-703/08/23 15:03438 167 1
3,3'-Dichlorobenzidine ND ug/kg 03/09/23 14:46 91-94-103/08/23 15:03876 296 1
2,4-Dichlorophenol ND ug/kg 03/09/23 14:46 120-83-203/08/23 15:03438 171 1
Diethylphthalate ND ug/kg 03/09/23 14:46 84-66-203/08/23 15:03438 161 1
2,4-Dimethylphenol ND ug/kg 03/09/23 14:46 105-67-903/08/23 15:03438 182 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: COMP-1 (0-2)Lab ID: 92655679001 Collected: 03/07/23 13:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 03/09/23 14:46 131-11-303/08/23 15:03438 159 1
Di-n-butylphthalate ND ug/kg 03/09/23 14:46 84-74-203/08/23 15:03438 147 1
4,6-Dinitro-2-methylphenol ND ug/kg 03/09/23 14:46 534-52-103/08/23 15:03876 409 1
2,4-Dinitrophenol ND ug/kg 03/09/23 14:46 51-28-503/08/23 15:032190 1350 1
2,4-Dinitrotoluene ND ug/kg 03/09/23 14:46 121-14-203/08/23 15:03438 169 1
2,6-Dinitrotoluene ND ug/kg 03/09/23 14:46 606-20-203/08/23 15:03438 161 1
Di-n-octylphthalate ND ug/kg 03/09/23 14:46 117-84-003/08/23 15:03438 173 1
bis(2-Ethylhexyl)phthalate ND ug/kg 03/09/23 14:46 117-81-703/08/23 15:03438 170 1
Fluoranthene ND ug/kg 03/09/23 14:46 206-44-003/08/23 15:03438 150 1
Fluorene ND ug/kg 03/09/23 14:46 86-73-703/08/23 15:03438 154 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 14:46 87-68-303/08/23 15:03438 190 1
Hexachlorobenzene ND ug/kg 03/09/23 14:46 118-74-103/08/23 15:03438 171 1
Hexachlorocyclopentadiene ND ug/kg 03/09/23 14:46 77-47-403/08/23 15:03438 251 1
Hexachloroethane ND ug/kg 03/09/23 14:46 67-72-103/08/23 15:03438 167 1
Indeno(1,2,3-cd)pyrene ND ug/kg 03/09/23 14:46 193-39-503/08/23 15:03438 173 1
Isophorone ND ug/kg 03/09/23 14:46 78-59-103/08/23 15:03438 195 1
1-Methylnaphthalene ND ug/kg 03/09/23 14:46 90-12-003/08/23 15:03438 154 1
2-Methylnaphthalene ND ug/kg 03/09/23 14:46 91-57-603/08/23 15:03438 175 1
2-Methylphenol(o-Cresol)ND ug/kg 03/09/23 14:46 95-48-703/08/23 15:03438 179 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/09/23 14:46 15831-10-403/08/23 15:03438 177 1
Naphthalene ND ug/kg 03/09/23 14:46 91-20-303/08/23 15:03438 149 1
2-Nitroaniline ND ug/kg 03/09/23 14:46 88-74-403/08/23 15:032190 359 1
3-Nitroaniline ND ug/kg 03/09/23 14:46 99-09-203/08/23 15:032190 344 1
4-Nitroaniline ND ug/kg 03/09/23 14:46 100-01-603/08/23 15:03876 333 1
Nitrobenzene ND ug/kg 03/09/23 14:46 98-95-303/08/23 15:03438 203 1
2-Nitrophenol ND ug/kg 03/09/23 14:46 88-75-503/08/23 15:03438 190 1
4-Nitrophenol ND ug/kg 03/09/23 14:46 100-02-703/08/23 15:032190 847 1
N-Nitrosodimethylamine ND ug/kg 03/09/23 14:46 62-75-903/08/23 15:03438 147 1
N-Nitroso-di-n-propylamine ND ug/kg 03/09/23 14:46 621-64-703/08/23 15:03438 165 1
N-Nitrosodiphenylamine ND ug/kg 03/09/23 14:46 86-30-603/08/23 15:03438 155 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/09/23 14:46 108-60-103/08/23 15:03438 208 1
Pentachlorophenol ND ug/kg 03/09/23 14:46 87-86-503/08/23 15:03876 429 1
Phenanthrene ND ug/kg 03/09/23 14:46 85-01-803/08/23 15:03438 143 1
Phenol ND ug/kg 03/09/23 14:46 108-95-203/08/23 15:03438 195 1
Pyrene ND ug/kg 03/09/23 14:46 129-00-003/08/23 15:03438 178 1
Pyridine ND ug/kg 03/09/23 14:46 110-86-103/08/23 15:03438 138 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 14:46 120-82-103/08/23 15:03438 173 1
2,4,5-Trichlorophenol ND ug/kg 03/09/23 14:46 95-95-403/08/23 15:03438 201 1
2,4,6-Trichlorophenol ND ug/kg 03/09/23 14:46 88-06-203/08/23 15:03438 181 1
Surrogates
Nitrobenzene-d5 (S)44 %03/09/23 14:46 4165-60-003/08/23 15:0310-130 1
2-Fluorobiphenyl (S)44 %03/09/23 14:46 321-60-803/08/23 15:0310-130 1
Terphenyl-d14 (S)62 %03/09/23 14:46 1718-51-003/08/23 15:0310-130 1
Phenol-d6 (S)40 %03/09/23 14:46 13127-88-303/08/23 15:0310-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: COMP-1 (0-2)Lab ID: 92655679001 Collected: 03/07/23 13:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)38 %03/09/23 14:46 367-12-403/08/23 15:0310-130 1
2,4,6-Tribromophenol (S)62 %03/09/23 14:46 118-79-603/08/23 15:0310-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/09/23 15:49 67-64-103/08/23 22:56161 51.8 1
Benzene ND ug/kg 03/09/23 15:49 71-43-203/08/23 22:568.1 3.2 1
Bromobenzene ND ug/kg 03/09/23 15:49 108-86-103/08/23 22:568.1 2.6 1
Bromochloromethane ND ug/kg 03/09/23 15:49 74-97-503/08/23 22:568.1 2.4 1
Bromodichloromethane ND ug/kg 03/09/23 15:49 75-27-403/08/23 22:568.1 3.1 1
Bromoform ND ug/kg 03/09/23 15:49 75-25-203/08/23 22:568.1 2.8 1
Bromomethane ND ug/kg 03/09/23 15:49 74-83-903/08/23 22:5632.3 25.0 1
2-Butanone (MEK)ND ug/kg 03/09/23 15:49 78-93-3 v103/08/23 22:56161 38.7 1
n-Butylbenzene ND ug/kg 03/09/23 15:49 104-51-803/08/23 22:568.1 5.1 1
sec-Butylbenzene ND ug/kg 03/09/23 15:49 135-98-803/08/23 22:568.1 3.6 1
tert-Butylbenzene ND ug/kg 03/09/23 15:49 98-06-603/08/23 22:568.1 2.9 1
Carbon tetrachloride ND ug/kg 03/09/23 15:49 56-23-503/08/23 22:568.1 3.0 1
Chlorobenzene ND ug/kg 03/09/23 15:49 108-90-703/08/23 22:568.1 4.6 1
Chloroethane ND ug/kg 03/09/23 15:49 75-00-303/08/23 22:5616.1 6.2 1
Chloroform ND ug/kg 03/09/23 15:49 67-66-303/08/23 22:568.1 6.7 1
Chloromethane ND ug/kg 03/09/23 15:49 74-87-303/08/23 22:5616.1 6.8 1
2-Chlorotoluene ND ug/kg 03/09/23 15:49 95-49-803/08/23 22:568.1 2.9 1
4-Chlorotoluene ND ug/kg 03/09/23 15:49 106-43-403/08/23 22:568.1 4.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/09/23 15:49 96-12-803/08/23 22:568.1 3.1 1
Dibromochloromethane ND ug/kg 03/09/23 15:49 124-48-103/08/23 22:568.1 4.5 1
1,2-Dibromoethane (EDB)ND ug/kg 03/09/23 15:49 106-93-403/08/23 22:568.1 3.6 1
Dibromomethane ND ug/kg 03/09/23 15:49 74-95-303/08/23 22:568.1 1.7 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 15:49 95-50-103/08/23 22:568.1 2.9 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 15:49 541-73-103/08/23 22:568.1 2.5 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 15:49 106-46-703/08/23 22:568.1 2.1 1
Dichlorodifluoromethane ND ug/kg 03/09/23 15:49 75-71-803/08/23 22:5616.1 8.2 1
1,1-Dichloroethane ND ug/kg 03/09/23 15:49 75-34-303/08/23 22:568.1 3.3 1
1,2-Dichloroethane ND ug/kg 03/09/23 15:49 107-06-203/08/23 22:568.1 5.3 1
1,1-Dichloroethene ND ug/kg 03/09/23 15:49 75-35-403/08/23 22:568.1 3.3 1
cis-1,2-Dichloroethene ND ug/kg 03/09/23 15:49 156-59-203/08/23 22:568.1 2.8 1
trans-1,2-Dichloroethene ND ug/kg 03/09/23 15:49 156-60-503/08/23 22:568.1 6.9 1
1,2-Dichloropropane ND ug/kg 03/09/23 15:49 78-87-503/08/23 22:568.1 2.4 1
1,3-Dichloropropane ND ug/kg 03/09/23 15:49 142-28-903/08/23 22:568.1 2.5 1
2,2-Dichloropropane ND ug/kg 03/09/23 15:49 594-20-703/08/23 22:568.1 6.1 1
1,1-Dichloropropene ND ug/kg 03/09/23 15:49 563-58-603/08/23 22:568.1 3.9 1
cis-1,3-Dichloropropene ND ug/kg 03/09/23 15:49 10061-01-503/08/23 22:568.1 2.2 1
trans-1,3-Dichloropropene ND ug/kg 03/09/23 15:49 10061-02-603/08/23 22:568.1 2.8 1
Diisopropyl ether ND ug/kg 03/09/23 15:49 108-20-303/08/23 22:568.1 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: COMP-1 (0-2)Lab ID: 92655679001 Collected: 03/07/23 13:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 03/09/23 15:49 100-41-403/08/23 22:568.1 3.8 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 15:49 87-68-303/08/23 22:5616.1 13.2 1
2-Hexanone ND ug/kg 03/09/23 15:49 591-78-6 L1,M0,
v103/08/23 22:5680.7 7.8 1
Isopropylbenzene (Cumene)ND ug/kg 03/09/23 15:49 98-82-803/08/23 22:568.1 2.7 1
p-Isopropyltoluene ND ug/kg 03/09/23 15:49 99-87-603/08/23 22:568.1 4.0 1
Methylene Chloride ND ug/kg 03/09/23 15:49 75-09-203/08/23 22:5632.3 22.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/09/23 15:49 108-10-1 v103/08/23 22:5680.7 7.8 1
Methyl-tert-butyl ether ND ug/kg 03/09/23 15:49 1634-04-403/08/23 22:568.1 3.0 1
Naphthalene ND ug/kg 03/09/23 15:49 91-20-303/08/23 22:568.1 4.2 1
n-Propylbenzene ND ug/kg 03/09/23 15:49 103-65-103/08/23 22:568.1 2.9 1
Styrene ND ug/kg 03/09/23 15:49 100-42-503/08/23 22:568.1 2.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/09/23 15:49 630-20-603/08/23 22:568.1 3.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/09/23 15:49 79-34-503/08/23 22:568.1 2.1 1
Tetrachloroethene ND ug/kg 03/09/23 15:49 127-18-403/08/23 22:568.1 2.5 1
Toluene ND ug/kg 03/09/23 15:49 108-88-303/08/23 22:568.1 5.6 1
1,2,3-Trichlorobenzene ND ug/kg 03/09/23 15:49 87-61-603/08/23 22:568.1 6.5 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 15:49 120-82-103/08/23 22:568.1 6.8 1
1,1,1-Trichloroethane ND ug/kg 03/09/23 15:49 71-55-603/08/23 22:568.1 4.2 1
1,1,2-Trichloroethane ND ug/kg 03/09/23 15:49 79-00-503/08/23 22:568.1 2.7 1
Trichloroethene ND ug/kg 03/09/23 15:49 79-01-603/08/23 22:568.1 6.5 1
Trichlorofluoromethane ND ug/kg 03/09/23 15:49 75-69-403/08/23 22:568.1 4.4 1
1,2,3-Trichloropropane ND ug/kg 03/09/23 15:49 96-18-4 v103/08/23 22:568.1 4.1 1
1,2,4-Trimethylbenzene ND ug/kg 03/09/23 15:49 95-63-603/08/23 22:568.1 4.8 1
1,3,5-Trimethylbenzene ND ug/kg 03/09/23 15:49 108-67-803/08/23 22:568.1 2.7 1
Vinyl acetate ND ug/kg 03/09/23 15:49 108-05-403/08/23 22:5680.7 16.6 1
Vinyl chloride ND ug/kg 03/09/23 15:49 75-01-403/08/23 22:5616.1 4.1 1
Xylene (Total)ND ug/kg 03/09/23 15:49 1330-20-703/08/23 22:5616.1 4.6 1
m&p-Xylene ND ug/kg 03/09/23 15:49 179601-23-103/08/23 22:5616.1 5.5 1
o-Xylene ND ug/kg 03/09/23 15:49 95-47-603/08/23 22:568.1 3.6 1
Surrogates
Toluene-d8 (S)101 %03/09/23 15:49 2037-26-503/08/23 22:5670-130 1
4-Bromofluorobenzene (S)103 %03/09/23 15:49 460-00-403/08/23 22:5670-130 1
1,2-Dichloroethane-d4 (S)114 %03/09/23 15:49 17060-07-003/08/23 22:5670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.9 %03/08/23 13:58 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 80.6 %03/13/23 15:2803/13/23 15:211
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: COMP-1 (0-2)Lab ID: 92655679001 Collected: 03/07/23 13:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.45 mg/kg 03/14/23 14:59 18540-29-9 D803/14/23 01:161.24 0.316 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: COMP-2 (0-2)Lab ID: 92655679002 Collected: 03/07/23 17:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.7 mg/kg 03/14/23 16:36 7440-38-203/14/23 10:330.61 0.18 1
Barium 80.5 mg/kg 03/14/23 16:36 7440-39-303/14/23 10:330.37 0.092 1
Cadmium 0.051J mg/kg 03/14/23 16:36 7440-43-903/14/23 10:330.098 0.036 1
Chromium 65.6 mg/kg 03/14/23 16:36 7440-47-303/14/23 10:332.5 0.48 1
Lead 13.0 mg/kg 03/14/23 16:36 7439-92-103/14/23 10:330.61 0.11 1
Selenium 0.60J mg/kg 03/14/23 16:36 7782-49-203/14/23 10:330.61 0.13 1
Silver ND mg/kg 03/14/23 16:36 7440-22-403/14/23 10:330.61 0.25 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.058 mg/kg 03/14/23 11:38 7439-97-603/13/23 15:150.023 0.010 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 03/09/23 15:14 83-32-903/08/23 15:03424 149 1
Acenaphthylene ND ug/kg 03/09/23 15:14 208-96-803/08/23 15:03424 149 1
Aniline ND ug/kg 03/09/23 15:14 62-53-303/08/23 15:03424 166 1
Anthracene ND ug/kg 03/09/23 15:14 120-12-703/08/23 15:03424 139 1
Benzo(a)anthracene ND ug/kg 03/09/23 15:14 56-55-303/08/23 15:03424 141 1
Benzo(a)pyrene ND ug/kg 03/09/23 15:14 50-32-803/08/23 15:03424 146 1
Benzo(b)fluoranthene ND ug/kg 03/09/23 15:14 205-99-203/08/23 15:03424 141 1
Benzo(g,h,i)perylene ND ug/kg 03/09/23 15:14 191-24-203/08/23 15:03424 164 1
Benzo(k)fluoranthene ND ug/kg 03/09/23 15:14 207-08-903/08/23 15:03424 149 1
Benzoic Acid ND ug/kg 03/09/23 15:14 65-85-003/08/23 15:032120 910 1
Benzyl alcohol ND ug/kg 03/09/23 15:14 100-51-603/08/23 15:03848 321 1
4-Bromophenylphenyl ether ND ug/kg 03/09/23 15:14 101-55-303/08/23 15:03424 163 1
Butylbenzylphthalate ND ug/kg 03/09/23 15:14 85-68-703/08/23 15:03424 178 1
4-Chloro-3-methylphenol ND ug/kg 03/09/23 15:14 59-50-703/08/23 15:03848 298 1
4-Chloroaniline ND ug/kg 03/09/23 15:14 106-47-803/08/23 15:03848 333 1
bis(2-Chloroethoxy)methane ND ug/kg 03/09/23 15:14 111-91-103/08/23 15:03424 176 1
bis(2-Chloroethyl) ether ND ug/kg 03/09/23 15:14 111-44-403/08/23 15:03424 159 1
2-Chloronaphthalene ND ug/kg 03/09/23 15:14 91-58-703/08/23 15:03424 168 1
2-Chlorophenol ND ug/kg 03/09/23 15:14 95-57-803/08/23 15:03424 159 1
4-Chlorophenylphenyl ether ND ug/kg 03/09/23 15:14 7005-72-303/08/23 15:03424 158 1
Chrysene ND ug/kg 03/09/23 15:14 218-01-903/08/23 15:03424 154 1
Dibenz(a,h)anthracene ND ug/kg 03/09/23 15:14 53-70-303/08/23 15:03424 163 1
Dibenzofuran ND ug/kg 03/09/23 15:14 132-64-903/08/23 15:03424 153 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 15:14 95-50-103/08/23 15:03424 153 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 15:14 541-73-103/08/23 15:03424 150 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 15:14 106-46-703/08/23 15:03424 162 1
3,3'-Dichlorobenzidine ND ug/kg 03/09/23 15:14 91-94-103/08/23 15:03848 286 1
2,4-Dichlorophenol ND ug/kg 03/09/23 15:14 120-83-203/08/23 15:03424 166 1
Diethylphthalate ND ug/kg 03/09/23 15:14 84-66-203/08/23 15:03424 155 1
2,4-Dimethylphenol ND ug/kg 03/09/23 15:14 105-67-903/08/23 15:03424 176 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: COMP-2 (0-2)Lab ID: 92655679002 Collected: 03/07/23 17:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 03/09/23 15:14 131-11-303/08/23 15:03424 154 1
Di-n-butylphthalate ND ug/kg 03/09/23 15:14 84-74-203/08/23 15:03424 143 1
4,6-Dinitro-2-methylphenol ND ug/kg 03/09/23 15:14 534-52-103/08/23 15:03848 396 1
2,4-Dinitrophenol ND ug/kg 03/09/23 15:14 51-28-503/08/23 15:032120 1310 1
2,4-Dinitrotoluene ND ug/kg 03/09/23 15:14 121-14-203/08/23 15:03424 163 1
2,6-Dinitrotoluene ND ug/kg 03/09/23 15:14 606-20-203/08/23 15:03424 155 1
Di-n-octylphthalate ND ug/kg 03/09/23 15:14 117-84-003/08/23 15:03424 167 1
bis(2-Ethylhexyl)phthalate ND ug/kg 03/09/23 15:14 117-81-703/08/23 15:03424 164 1
Fluoranthene ND ug/kg 03/09/23 15:14 206-44-003/08/23 15:03424 145 1
Fluorene ND ug/kg 03/09/23 15:14 86-73-703/08/23 15:03424 149 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 15:14 87-68-303/08/23 15:03424 184 1
Hexachlorobenzene ND ug/kg 03/09/23 15:14 118-74-103/08/23 15:03424 166 1
Hexachlorocyclopentadiene ND ug/kg 03/09/23 15:14 77-47-403/08/23 15:03424 243 1
Hexachloroethane ND ug/kg 03/09/23 15:14 67-72-103/08/23 15:03424 162 1
Indeno(1,2,3-cd)pyrene ND ug/kg 03/09/23 15:14 193-39-503/08/23 15:03424 167 1
Isophorone ND ug/kg 03/09/23 15:14 78-59-103/08/23 15:03424 189 1
1-Methylnaphthalene ND ug/kg 03/09/23 15:14 90-12-003/08/23 15:03424 149 1
2-Methylnaphthalene ND ug/kg 03/09/23 15:14 91-57-603/08/23 15:03424 170 1
2-Methylphenol(o-Cresol)ND ug/kg 03/09/23 15:14 95-48-703/08/23 15:03424 173 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/09/23 15:14 15831-10-403/08/23 15:03424 171 1
Naphthalene ND ug/kg 03/09/23 15:14 91-20-303/08/23 15:03424 144 1
2-Nitroaniline ND ug/kg 03/09/23 15:14 88-74-403/08/23 15:032120 347 1
3-Nitroaniline ND ug/kg 03/09/23 15:14 99-09-203/08/23 15:032120 333 1
4-Nitroaniline ND ug/kg 03/09/23 15:14 100-01-603/08/23 15:03848 322 1
Nitrobenzene ND ug/kg 03/09/23 15:14 98-95-303/08/23 15:03424 196 1
2-Nitrophenol ND ug/kg 03/09/23 15:14 88-75-503/08/23 15:03424 184 1
4-Nitrophenol ND ug/kg 03/09/23 15:14 100-02-703/08/23 15:032120 819 1
N-Nitrosodimethylamine ND ug/kg 03/09/23 15:14 62-75-903/08/23 15:03424 143 1
N-Nitroso-di-n-propylamine ND ug/kg 03/09/23 15:14 621-64-703/08/23 15:03424 159 1
N-Nitrosodiphenylamine ND ug/kg 03/09/23 15:14 86-30-603/08/23 15:03424 150 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/09/23 15:14 108-60-103/08/23 15:03424 202 1
Pentachlorophenol ND ug/kg 03/09/23 15:14 87-86-503/08/23 15:03848 415 1
Phenanthrene ND ug/kg 03/09/23 15:14 85-01-803/08/23 15:03424 139 1
Phenol ND ug/kg 03/09/23 15:14 108-95-203/08/23 15:03424 189 1
Pyrene ND ug/kg 03/09/23 15:14 129-00-003/08/23 15:03424 172 1
Pyridine ND ug/kg 03/09/23 15:14 110-86-103/08/23 15:03424 134 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 15:14 120-82-103/08/23 15:03424 167 1
2,4,5-Trichlorophenol ND ug/kg 03/09/23 15:14 95-95-403/08/23 15:03424 194 1
2,4,6-Trichlorophenol ND ug/kg 03/09/23 15:14 88-06-203/08/23 15:03424 175 1
Surrogates
Nitrobenzene-d5 (S)56 %03/09/23 15:14 4165-60-003/08/23 15:0310-130 1
2-Fluorobiphenyl (S)55 %03/09/23 15:14 321-60-803/08/23 15:0310-130 1
Terphenyl-d14 (S)54 %03/09/23 15:14 1718-51-003/08/23 15:0310-130 1
Phenol-d6 (S)48 %03/09/23 15:14 13127-88-303/08/23 15:0310-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: COMP-2 (0-2)Lab ID: 92655679002 Collected: 03/07/23 17:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)43 %03/09/23 15:14 367-12-403/08/23 15:0310-130 1
2,4,6-Tribromophenol (S)59 %03/09/23 15:14 118-79-603/08/23 15:0310-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/09/23 16:06 67-64-103/08/23 22:56141 45.1 1
Benzene ND ug/kg 03/09/23 16:06 71-43-203/08/23 22:567.0 2.8 1
Bromobenzene ND ug/kg 03/09/23 16:06 108-86-103/08/23 22:567.0 2.3 1
Bromochloromethane ND ug/kg 03/09/23 16:06 74-97-503/08/23 22:567.0 2.1 1
Bromodichloromethane ND ug/kg 03/09/23 16:06 75-27-403/08/23 22:567.0 2.7 1
Bromoform ND ug/kg 03/09/23 16:06 75-25-203/08/23 22:567.0 2.5 1
Bromomethane ND ug/kg 03/09/23 16:06 74-83-903/08/23 22:5628.1 21.8 1
2-Butanone (MEK)ND ug/kg 03/09/23 16:06 78-93-3 v103/08/23 22:56141 33.8 1
n-Butylbenzene ND ug/kg 03/09/23 16:06 104-51-803/08/23 22:567.0 4.4 1
sec-Butylbenzene ND ug/kg 03/09/23 16:06 135-98-803/08/23 22:567.0 3.1 1
tert-Butylbenzene ND ug/kg 03/09/23 16:06 98-06-603/08/23 22:567.0 2.5 1
Carbon tetrachloride ND ug/kg 03/09/23 16:06 56-23-503/08/23 22:567.0 2.6 1
Chlorobenzene ND ug/kg 03/09/23 16:06 108-90-703/08/23 22:567.0 4.0 1
Chloroethane ND ug/kg 03/09/23 16:06 75-00-303/08/23 22:5614.1 5.4 1
Chloroform ND ug/kg 03/09/23 16:06 67-66-303/08/23 22:567.0 5.9 1
Chloromethane ND ug/kg 03/09/23 16:06 74-87-303/08/23 22:5614.1 5.9 1
2-Chlorotoluene ND ug/kg 03/09/23 16:06 95-49-803/08/23 22:567.0 2.5 1
4-Chlorotoluene ND ug/kg 03/09/23 16:06 106-43-403/08/23 22:567.0 3.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/09/23 16:06 96-12-803/08/23 22:567.0 2.7 1
Dibromochloromethane ND ug/kg 03/09/23 16:06 124-48-103/08/23 22:567.0 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 03/09/23 16:06 106-93-403/08/23 22:567.0 3.1 1
Dibromomethane ND ug/kg 03/09/23 16:06 74-95-303/08/23 22:567.0 1.5 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 16:06 95-50-103/08/23 22:567.0 2.5 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 16:06 541-73-103/08/23 22:567.0 2.2 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 16:06 106-46-703/08/23 22:567.0 1.8 1
Dichlorodifluoromethane ND ug/kg 03/09/23 16:06 75-71-803/08/23 22:5614.1 7.2 1
1,1-Dichloroethane ND ug/kg 03/09/23 16:06 75-34-303/08/23 22:567.0 2.9 1
1,2-Dichloroethane ND ug/kg 03/09/23 16:06 107-06-203/08/23 22:567.0 4.7 1
1,1-Dichloroethene ND ug/kg 03/09/23 16:06 75-35-403/08/23 22:567.0 2.9 1
cis-1,2-Dichloroethene ND ug/kg 03/09/23 16:06 156-59-203/08/23 22:567.0 2.4 1
trans-1,2-Dichloroethene ND ug/kg 03/09/23 16:06 156-60-503/08/23 22:567.0 6.0 1
1,2-Dichloropropane ND ug/kg 03/09/23 16:06 78-87-503/08/23 22:567.0 2.1 1
1,3-Dichloropropane ND ug/kg 03/09/23 16:06 142-28-903/08/23 22:567.0 2.2 1
2,2-Dichloropropane ND ug/kg 03/09/23 16:06 594-20-703/08/23 22:567.0 5.3 1
1,1-Dichloropropene ND ug/kg 03/09/23 16:06 563-58-603/08/23 22:567.0 3.4 1
cis-1,3-Dichloropropene ND ug/kg 03/09/23 16:06 10061-01-503/08/23 22:567.0 1.9 1
trans-1,3-Dichloropropene ND ug/kg 03/09/23 16:06 10061-02-603/08/23 22:567.0 2.4 1
Diisopropyl ether ND ug/kg 03/09/23 16:06 108-20-303/08/23 22:567.0 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: COMP-2 (0-2)Lab ID: 92655679002 Collected: 03/07/23 17:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 03/09/23 16:06 100-41-403/08/23 22:567.0 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 16:06 87-68-303/08/23 22:5614.1 11.5 1
2-Hexanone ND ug/kg 03/09/23 16:06 591-78-6 L1,v103/08/23 22:5670.3 6.8 1
Isopropylbenzene (Cumene)ND ug/kg 03/09/23 16:06 98-82-803/08/23 22:567.0 2.4 1
p-Isopropyltoluene ND ug/kg 03/09/23 16:06 99-87-603/08/23 22:567.0 3.5 1
Methylene Chloride ND ug/kg 03/09/23 16:06 75-09-203/08/23 22:5628.1 19.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/09/23 16:06 108-10-1 v103/08/23 22:5670.3 6.8 1
Methyl-tert-butyl ether ND ug/kg 03/09/23 16:06 1634-04-403/08/23 22:567.0 2.6 1
Naphthalene ND ug/kg 03/09/23 16:06 91-20-303/08/23 22:567.0 3.7 1
n-Propylbenzene ND ug/kg 03/09/23 16:06 103-65-103/08/23 22:567.0 2.5 1
Styrene ND ug/kg 03/09/23 16:06 100-42-503/08/23 22:567.0 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/09/23 16:06 630-20-603/08/23 22:567.0 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/09/23 16:06 79-34-503/08/23 22:567.0 1.9 1
Tetrachloroethene 11.9 ug/kg 03/09/23 16:06 127-18-403/08/23 22:567.0 2.2 1
Toluene ND ug/kg 03/09/23 16:06 108-88-303/08/23 22:567.0 4.9 1
1,2,3-Trichlorobenzene ND ug/kg 03/09/23 16:06 87-61-603/08/23 22:567.0 5.7 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 16:06 120-82-103/08/23 22:567.0 5.9 1
1,1,1-Trichloroethane ND ug/kg 03/09/23 16:06 71-55-603/08/23 22:567.0 3.7 1
1,1,2-Trichloroethane ND ug/kg 03/09/23 16:06 79-00-503/08/23 22:567.0 2.3 1
Trichloroethene ND ug/kg 03/09/23 16:06 79-01-603/08/23 22:567.0 5.7 1
Trichlorofluoromethane ND ug/kg 03/09/23 16:06 75-69-403/08/23 22:567.0 3.9 1
1,2,3-Trichloropropane ND ug/kg 03/09/23 16:06 96-18-4 v103/08/23 22:567.0 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 03/09/23 16:06 95-63-603/08/23 22:567.0 4.2 1
1,3,5-Trimethylbenzene ND ug/kg 03/09/23 16:06 108-67-803/08/23 22:567.0 2.4 1
Vinyl acetate ND ug/kg 03/09/23 16:06 108-05-403/08/23 22:5670.3 14.5 1
Vinyl chloride ND ug/kg 03/09/23 16:06 75-01-403/08/23 22:5614.1 3.6 1
Xylene (Total)ND ug/kg 03/09/23 16:06 1330-20-703/08/23 22:5614.1 4.0 1
m&p-Xylene ND ug/kg 03/09/23 16:06 179601-23-103/08/23 22:5614.1 4.8 1
o-Xylene ND ug/kg 03/09/23 16:06 95-47-603/08/23 22:567.0 3.1 1
Surrogates
Toluene-d8 (S)100 %03/09/23 16:06 2037-26-503/08/23 22:5670-130 1
4-Bromofluorobenzene (S)101 %03/09/23 16:06 460-00-403/08/23 22:5670-130 1
1,2-Dichloroethane-d4 (S)111 %03/09/23 16:06 17060-07-003/08/23 22:5670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.6 %03/08/23 13:58 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 79.9 %03/13/23 15:2803/13/23 15:211
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: COMP-2 (0-2)Lab ID: 92655679002 Collected: 03/07/23 17:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.965J mg/kg 03/14/23 15:09 18540-29-9 J03/14/23 01:161.25 0.319 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-01 (0-2)Lab ID: 92655679003 Collected: 03/07/23 17:25 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.5 mg/kg 03/14/23 16:42 7440-38-203/14/23 10:330.66 0.19 1
Barium 46.4 mg/kg 03/14/23 16:42 7440-39-303/14/23 10:330.39 0.099 1
Cadmium ND mg/kg 03/14/23 16:42 7440-43-903/14/23 10:330.11 0.039 1
Chromium 66.8 mg/kg 03/14/23 16:42 7440-47-303/14/23 10:332.6 0.51 1
Lead 7.7 mg/kg 03/14/23 16:42 7439-92-103/14/23 10:330.66 0.12 1
Selenium 0.65J mg/kg 03/14/23 16:42 7782-49-203/14/23 10:330.66 0.14 1
Silver ND mg/kg 03/14/23 16:42 7440-22-403/14/23 10:330.66 0.27 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.039 mg/kg 03/14/23 11:40 7439-97-603/13/23 15:150.025 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 03/09/23 15:42 83-32-903/08/23 15:03437 154 1
Acenaphthylene ND ug/kg 03/09/23 15:42 208-96-803/08/23 15:03437 154 1
Aniline ND ug/kg 03/09/23 15:42 62-53-303/08/23 15:03437 171 1
Anthracene ND ug/kg 03/09/23 15:42 120-12-703/08/23 15:03437 143 1
Benzo(a)anthracene ND ug/kg 03/09/23 15:42 56-55-303/08/23 15:03437 146 1
Benzo(a)pyrene ND ug/kg 03/09/23 15:42 50-32-803/08/23 15:03437 151 1
Benzo(b)fluoranthene ND ug/kg 03/09/23 15:42 205-99-203/08/23 15:03437 146 1
Benzo(g,h,i)perylene ND ug/kg 03/09/23 15:42 191-24-203/08/23 15:03437 170 1
Benzo(k)fluoranthene ND ug/kg 03/09/23 15:42 207-08-903/08/23 15:03437 154 1
Benzoic Acid ND ug/kg 03/09/23 15:42 65-85-003/08/23 15:032190 940 1
Benzyl alcohol ND ug/kg 03/09/23 15:42 100-51-603/08/23 15:03875 331 1
4-Bromophenylphenyl ether ND ug/kg 03/09/23 15:42 101-55-303/08/23 15:03437 168 1
Butylbenzylphthalate ND ug/kg 03/09/23 15:42 85-68-703/08/23 15:03437 184 1
4-Chloro-3-methylphenol ND ug/kg 03/09/23 15:42 59-50-703/08/23 15:03875 307 1
4-Chloroaniline ND ug/kg 03/09/23 15:42 106-47-803/08/23 15:03875 343 1
bis(2-Chloroethoxy)methane ND ug/kg 03/09/23 15:42 111-91-103/08/23 15:03437 182 1
bis(2-Chloroethyl) ether ND ug/kg 03/09/23 15:42 111-44-403/08/23 15:03437 164 1
2-Chloronaphthalene ND ug/kg 03/09/23 15:42 91-58-703/08/23 15:03437 174 1
2-Chlorophenol ND ug/kg 03/09/23 15:42 95-57-803/08/23 15:03437 164 1
4-Chlorophenylphenyl ether ND ug/kg 03/09/23 15:42 7005-72-303/08/23 15:03437 163 1
Chrysene ND ug/kg 03/09/23 15:42 218-01-903/08/23 15:03437 159 1
Dibenz(a,h)anthracene ND ug/kg 03/09/23 15:42 53-70-303/08/23 15:03437 168 1
Dibenzofuran ND ug/kg 03/09/23 15:42 132-64-903/08/23 15:03437 158 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 15:42 95-50-103/08/23 15:03437 158 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 15:42 541-73-103/08/23 15:03437 155 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 15:42 106-46-703/08/23 15:03437 167 1
3,3'-Dichlorobenzidine ND ug/kg 03/09/23 15:42 91-94-103/08/23 15:03875 295 1
2,4-Dichlorophenol ND ug/kg 03/09/23 15:42 120-83-203/08/23 15:03437 171 1
Diethylphthalate ND ug/kg 03/09/23 15:42 84-66-203/08/23 15:03437 160 1
2,4-Dimethylphenol ND ug/kg 03/09/23 15:42 105-67-903/08/23 15:03437 182 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-01 (0-2)Lab ID: 92655679003 Collected: 03/07/23 17:25 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 03/09/23 15:42 131-11-303/08/23 15:03437 159 1
Di-n-butylphthalate ND ug/kg 03/09/23 15:42 84-74-203/08/23 15:03437 147 1
4,6-Dinitro-2-methylphenol ND ug/kg 03/09/23 15:42 534-52-103/08/23 15:03875 408 1
2,4-Dinitrophenol ND ug/kg 03/09/23 15:42 51-28-503/08/23 15:032190 1350 1
2,4-Dinitrotoluene ND ug/kg 03/09/23 15:42 121-14-203/08/23 15:03437 168 1
2,6-Dinitrotoluene ND ug/kg 03/09/23 15:42 606-20-203/08/23 15:03437 160 1
Di-n-octylphthalate ND ug/kg 03/09/23 15:42 117-84-003/08/23 15:03437 172 1
bis(2-Ethylhexyl)phthalate ND ug/kg 03/09/23 15:42 117-81-703/08/23 15:03437 170 1
Fluoranthene ND ug/kg 03/09/23 15:42 206-44-003/08/23 15:03437 150 1
Fluorene ND ug/kg 03/09/23 15:42 86-73-703/08/23 15:03437 154 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 15:42 87-68-303/08/23 15:03437 189 1
Hexachlorobenzene ND ug/kg 03/09/23 15:42 118-74-103/08/23 15:03437 171 1
Hexachlorocyclopentadiene ND ug/kg 03/09/23 15:42 77-47-403/08/23 15:03437 250 1
Hexachloroethane ND ug/kg 03/09/23 15:42 67-72-103/08/23 15:03437 167 1
Indeno(1,2,3-cd)pyrene ND ug/kg 03/09/23 15:42 193-39-503/08/23 15:03437 172 1
Isophorone ND ug/kg 03/09/23 15:42 78-59-103/08/23 15:03437 195 1
1-Methylnaphthalene ND ug/kg 03/09/23 15:42 90-12-003/08/23 15:03437 154 1
2-Methylnaphthalene ND ug/kg 03/09/23 15:42 91-57-603/08/23 15:03437 175 1
2-Methylphenol(o-Cresol)ND ug/kg 03/09/23 15:42 95-48-703/08/23 15:03437 179 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/09/23 15:42 15831-10-403/08/23 15:03437 176 1
Naphthalene ND ug/kg 03/09/23 15:42 91-20-303/08/23 15:03437 148 1
2-Nitroaniline ND ug/kg 03/09/23 15:42 88-74-403/08/23 15:032190 358 1
3-Nitroaniline ND ug/kg 03/09/23 15:42 99-09-203/08/23 15:032190 343 1
4-Nitroaniline ND ug/kg 03/09/23 15:42 100-01-603/08/23 15:03875 333 1
Nitrobenzene ND ug/kg 03/09/23 15:42 98-95-303/08/23 15:03437 203 1
2-Nitrophenol ND ug/kg 03/09/23 15:42 88-75-503/08/23 15:03437 189 1
4-Nitrophenol ND ug/kg 03/09/23 15:42 100-02-703/08/23 15:032190 845 1
N-Nitrosodimethylamine ND ug/kg 03/09/23 15:42 62-75-903/08/23 15:03437 147 1
N-Nitroso-di-n-propylamine ND ug/kg 03/09/23 15:42 621-64-703/08/23 15:03437 164 1
N-Nitrosodiphenylamine ND ug/kg 03/09/23 15:42 86-30-603/08/23 15:03437 155 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/09/23 15:42 108-60-103/08/23 15:03437 208 1
Pentachlorophenol ND ug/kg 03/09/23 15:42 87-86-503/08/23 15:03875 428 1
Phenanthrene ND ug/kg 03/09/23 15:42 85-01-803/08/23 15:03437 143 1
Phenol ND ug/kg 03/09/23 15:42 108-95-203/08/23 15:03437 195 1
Pyrene ND ug/kg 03/09/23 15:42 129-00-003/08/23 15:03437 178 1
Pyridine ND ug/kg 03/09/23 15:42 110-86-103/08/23 15:03437 138 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 15:42 120-82-103/08/23 15:03437 172 1
2,4,5-Trichlorophenol ND ug/kg 03/09/23 15:42 95-95-403/08/23 15:03437 200 1
2,4,6-Trichlorophenol ND ug/kg 03/09/23 15:42 88-06-203/08/23 15:03437 180 1
Surrogates
Nitrobenzene-d5 (S)68 %03/09/23 15:42 4165-60-003/08/23 15:0310-130 1
2-Fluorobiphenyl (S)65 %03/09/23 15:42 321-60-803/08/23 15:0310-130 1
Terphenyl-d14 (S)65 %03/09/23 15:42 1718-51-003/08/23 15:0310-130 1
Phenol-d6 (S)65 %03/09/23 15:42 13127-88-303/08/23 15:0310-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-01 (0-2)Lab ID: 92655679003 Collected: 03/07/23 17:25 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)62 %03/09/23 15:42 367-12-403/08/23 15:0310-130 1
2,4,6-Tribromophenol (S)81 %03/09/23 15:42 118-79-603/08/23 15:0310-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/09/23 21:05 67-64-103/09/23 16:59147 47.3 1
Benzene ND ug/kg 03/09/23 21:05 71-43-203/09/23 16:597.4 2.9 1
Bromobenzene ND ug/kg 03/09/23 21:05 108-86-103/09/23 16:597.4 2.4 1
Bromochloromethane ND ug/kg 03/09/23 21:05 74-97-503/09/23 16:597.4 2.2 1
Bromodichloromethane ND ug/kg 03/09/23 21:05 75-27-403/09/23 16:597.4 2.8 1
Bromoform ND ug/kg 03/09/23 21:05 75-25-203/09/23 16:597.4 2.6 1
Bromomethane ND ug/kg 03/09/23 21:05 74-83-9 v203/09/23 16:5929.4 22.8 1
2-Butanone (MEK)ND ug/kg 03/09/23 21:05 78-93-303/09/23 16:59147 35.3 1
n-Butylbenzene ND ug/kg 03/09/23 21:05 104-51-803/09/23 16:597.4 4.6 1
sec-Butylbenzene ND ug/kg 03/09/23 21:05 135-98-803/09/23 16:597.4 3.2 1
tert-Butylbenzene ND ug/kg 03/09/23 21:05 98-06-603/09/23 16:597.4 2.6 1
Carbon tetrachloride ND ug/kg 03/09/23 21:05 56-23-5 IK03/09/23 16:597.4 2.8 1
Chlorobenzene ND ug/kg 03/09/23 21:05 108-90-703/09/23 16:597.4 4.2 1
Chloroethane ND ug/kg 03/09/23 21:05 75-00-303/09/23 16:5914.7 5.7 1
Chloroform ND ug/kg 03/09/23 21:05 67-66-303/09/23 16:597.4 6.2 1
Chloromethane 7.9J ug/kg 03/09/23 21:05 74-87-3 C803/09/23 16:5914.7 6.2 1
2-Chlorotoluene ND ug/kg 03/09/23 21:05 95-49-803/09/23 16:597.4 2.6 1
4-Chlorotoluene ND ug/kg 03/09/23 21:05 106-43-403/09/23 16:597.4 4.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/09/23 21:05 96-12-803/09/23 16:597.4 2.9 1
Dibromochloromethane ND ug/kg 03/09/23 21:05 124-48-1 IK03/09/23 16:597.4 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 03/09/23 21:05 106-93-403/09/23 16:597.4 3.2 1
Dibromomethane ND ug/kg 03/09/23 21:05 74-95-303/09/23 16:597.4 1.6 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 21:05 95-50-103/09/23 16:597.4 2.6 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 21:05 541-73-103/09/23 16:597.4 2.3 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 21:05 106-46-703/09/23 16:597.4 1.9 1
Dichlorodifluoromethane ND ug/kg 03/09/23 21:05 75-71-803/09/23 16:5914.7 7.5 1
1,1-Dichloroethane ND ug/kg 03/09/23 21:05 75-34-303/09/23 16:597.4 3.0 1
1,2-Dichloroethane ND ug/kg 03/09/23 21:05 107-06-203/09/23 16:597.4 4.9 1
1,1-Dichloroethene ND ug/kg 03/09/23 21:05 75-35-403/09/23 16:597.4 3.0 1
cis-1,2-Dichloroethene ND ug/kg 03/09/23 21:05 156-59-203/09/23 16:597.4 2.5 1
trans-1,2-Dichloroethene ND ug/kg 03/09/23 21:05 156-60-503/09/23 16:597.4 6.3 1
1,2-Dichloropropane ND ug/kg 03/09/23 21:05 78-87-503/09/23 16:597.4 2.2 1
1,3-Dichloropropane ND ug/kg 03/09/23 21:05 142-28-903/09/23 16:597.4 2.3 1
2,2-Dichloropropane ND ug/kg 03/09/23 21:05 594-20-703/09/23 16:597.4 5.6 1
1,1-Dichloropropene ND ug/kg 03/09/23 21:05 563-58-603/09/23 16:597.4 3.5 1
cis-1,3-Dichloropropene ND ug/kg 03/09/23 21:05 10061-01-503/09/23 16:597.4 2.0 1
trans-1,3-Dichloropropene ND ug/kg 03/09/23 21:05 10061-02-603/09/23 16:597.4 2.5 1
Diisopropyl ether ND ug/kg 03/09/23 21:05 108-20-303/09/23 16:597.4 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-01 (0-2)Lab ID: 92655679003 Collected: 03/07/23 17:25 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 03/09/23 21:05 100-41-403/09/23 16:597.4 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 21:05 87-68-303/09/23 16:5914.7 12.0 1
2-Hexanone ND ug/kg 03/09/23 21:05 591-78-603/09/23 16:5973.6 7.1 1
Isopropylbenzene (Cumene)ND ug/kg 03/09/23 21:05 98-82-803/09/23 16:597.4 2.5 1
p-Isopropyltoluene ND ug/kg 03/09/23 21:05 99-87-603/09/23 16:597.4 3.6 1
Methylene Chloride ND ug/kg 03/09/23 21:05 75-09-203/09/23 16:5929.4 20.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/09/23 21:05 108-10-103/09/23 16:5973.6 7.1 1
Methyl-tert-butyl ether ND ug/kg 03/09/23 21:05 1634-04-403/09/23 16:597.4 2.8 1
Naphthalene ND ug/kg 03/09/23 21:05 91-20-303/09/23 16:597.4 3.9 1
n-Propylbenzene ND ug/kg 03/09/23 21:05 103-65-103/09/23 16:597.4 2.6 1
Styrene ND ug/kg 03/09/23 21:05 100-42-5 IK03/09/23 16:597.4 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/09/23 21:05 630-20-603/09/23 16:597.4 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/09/23 21:05 79-34-503/09/23 16:597.4 1.9 1
Tetrachloroethene ND ug/kg 03/09/23 21:05 127-18-403/09/23 16:597.4 2.3 1
Toluene ND ug/kg 03/09/23 21:05 108-88-303/09/23 16:597.4 5.1 1
1,2,3-Trichlorobenzene ND ug/kg 03/09/23 21:05 87-61-603/09/23 16:597.4 5.9 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 21:05 120-82-103/09/23 16:597.4 6.2 1
1,1,1-Trichloroethane ND ug/kg 03/09/23 21:05 71-55-603/09/23 16:597.4 3.8 1
1,1,2-Trichloroethane ND ug/kg 03/09/23 21:05 79-00-503/09/23 16:597.4 2.4 1
Trichloroethene ND ug/kg 03/09/23 21:05 79-01-603/09/23 16:597.4 5.9 1
Trichlorofluoromethane ND ug/kg 03/09/23 21:05 75-69-403/09/23 16:597.4 4.0 1
1,2,3-Trichloropropane ND ug/kg 03/09/23 21:05 96-18-403/09/23 16:597.4 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/09/23 21:05 95-63-603/09/23 16:597.4 4.4 1
1,3,5-Trimethylbenzene ND ug/kg 03/09/23 21:05 108-67-803/09/23 16:597.4 2.5 1
Vinyl acetate ND ug/kg 03/09/23 21:05 108-05-403/09/23 16:5973.6 15.1 1
Vinyl chloride ND ug/kg 03/09/23 21:05 75-01-403/09/23 16:5914.7 3.7 1
Xylene (Total)ND ug/kg 03/09/23 21:05 1330-20-703/09/23 16:5914.7 4.2 1
m&p-Xylene ND ug/kg 03/09/23 21:05 179601-23-103/09/23 16:5914.7 5.0 1
o-Xylene ND ug/kg 03/09/23 21:05 95-47-603/09/23 16:597.4 3.3 1
Surrogates
Toluene-d8 (S)99 %03/09/23 21:05 2037-26-503/09/23 16:5970-130 1
4-Bromofluorobenzene (S)106 %03/09/23 21:05 460-00-403/09/23 16:5970-130 1
1,2-Dichloroethane-d4 (S)110 %03/09/23 21:05 17060-07-003/09/23 16:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.0 %03/08/23 13:58 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 75.3 %03/13/23 15:2803/13/23 15:211
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-01 (0-2)Lab ID: 92655679003 Collected: 03/07/23 17:25 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.741J mg/kg 03/14/23 15:15 18540-29-9 J03/14/23 01:161.33 0.339 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-02 (0-2)Lab ID: 92655679004 Collected: 03/07/23 18:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.9 mg/kg 03/14/23 16:48 7440-38-203/14/23 10:330.61 0.17 1
Barium 28.0 mg/kg 03/14/23 16:48 7440-39-303/14/23 10:330.37 0.091 1
Cadmium ND mg/kg 03/14/23 16:48 7440-43-903/14/23 10:330.098 0.036 1
Chromium 44.2 mg/kg 03/14/23 16:48 7440-47-303/14/23 10:332.4 0.47 1
Lead 7.7 mg/kg 03/14/23 16:48 7439-92-103/14/23 10:330.61 0.11 1
Selenium 0.70 mg/kg 03/14/23 16:48 7782-49-203/14/23 10:330.61 0.13 1
Silver ND mg/kg 03/14/23 16:48 7440-22-403/14/23 10:330.61 0.25 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.15 mg/kg 03/14/23 11:41 7439-97-603/13/23 15:150.024 0.010 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 03/09/23 16:09 83-32-903/08/23 15:03429 151 1
Acenaphthylene ND ug/kg 03/09/23 16:09 208-96-803/08/23 15:03429 151 1
Aniline ND ug/kg 03/09/23 16:09 62-53-303/08/23 15:03429 168 1
Anthracene ND ug/kg 03/09/23 16:09 120-12-703/08/23 15:03429 140 1
Benzo(a)anthracene ND ug/kg 03/09/23 16:09 56-55-303/08/23 15:03429 143 1
Benzo(a)pyrene ND ug/kg 03/09/23 16:09 50-32-803/08/23 15:03429 148 1
Benzo(b)fluoranthene ND ug/kg 03/09/23 16:09 205-99-203/08/23 15:03429 143 1
Benzo(g,h,i)perylene ND ug/kg 03/09/23 16:09 191-24-203/08/23 15:03429 166 1
Benzo(k)fluoranthene ND ug/kg 03/09/23 16:09 207-08-903/08/23 15:03429 151 1
Benzoic Acid ND ug/kg 03/09/23 16:09 65-85-003/08/23 15:032150 922 1
Benzyl alcohol ND ug/kg 03/09/23 16:09 100-51-603/08/23 15:03859 325 1
4-Bromophenylphenyl ether ND ug/kg 03/09/23 16:09 101-55-303/08/23 15:03429 165 1
Butylbenzylphthalate ND ug/kg 03/09/23 16:09 85-68-703/08/23 15:03429 181 1
4-Chloro-3-methylphenol ND ug/kg 03/09/23 16:09 59-50-703/08/23 15:03859 302 1
4-Chloroaniline ND ug/kg 03/09/23 16:09 106-47-803/08/23 15:03859 337 1
bis(2-Chloroethoxy)methane ND ug/kg 03/09/23 16:09 111-91-103/08/23 15:03429 178 1
bis(2-Chloroethyl) ether ND ug/kg 03/09/23 16:09 111-44-403/08/23 15:03429 161 1
2-Chloronaphthalene ND ug/kg 03/09/23 16:09 91-58-703/08/23 15:03429 170 1
2-Chlorophenol ND ug/kg 03/09/23 16:09 95-57-803/08/23 15:03429 161 1
4-Chlorophenylphenyl ether ND ug/kg 03/09/23 16:09 7005-72-303/08/23 15:03429 160 1
Chrysene ND ug/kg 03/09/23 16:09 218-01-903/08/23 15:03429 156 1
Dibenz(a,h)anthracene ND ug/kg 03/09/23 16:09 53-70-303/08/23 15:03429 165 1
Dibenzofuran ND ug/kg 03/09/23 16:09 132-64-903/08/23 15:03429 155 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 16:09 95-50-103/08/23 15:03429 155 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 16:09 541-73-103/08/23 15:03429 152 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 16:09 106-46-703/08/23 15:03429 164 1
3,3'-Dichlorobenzidine ND ug/kg 03/09/23 16:09 91-94-103/08/23 15:03859 290 1
2,4-Dichlorophenol ND ug/kg 03/09/23 16:09 120-83-203/08/23 15:03429 168 1
Diethylphthalate ND ug/kg 03/09/23 16:09 84-66-203/08/23 15:03429 157 1
2,4-Dimethylphenol ND ug/kg 03/09/23 16:09 105-67-903/08/23 15:03429 178 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-02 (0-2)Lab ID: 92655679004 Collected: 03/07/23 18:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 03/09/23 16:09 131-11-303/08/23 15:03429 156 1
Di-n-butylphthalate ND ug/kg 03/09/23 16:09 84-74-203/08/23 15:03429 144 1
4,6-Dinitro-2-methylphenol ND ug/kg 03/09/23 16:09 534-52-103/08/23 15:03859 401 1
2,4-Dinitrophenol ND ug/kg 03/09/23 16:09 51-28-503/08/23 15:032150 1330 1
2,4-Dinitrotoluene ND ug/kg 03/09/23 16:09 121-14-203/08/23 15:03429 165 1
2,6-Dinitrotoluene ND ug/kg 03/09/23 16:09 606-20-203/08/23 15:03429 157 1
Di-n-octylphthalate ND ug/kg 03/09/23 16:09 117-84-003/08/23 15:03429 169 1
bis(2-Ethylhexyl)phthalate ND ug/kg 03/09/23 16:09 117-81-703/08/23 15:03429 166 1
Fluoranthene ND ug/kg 03/09/23 16:09 206-44-003/08/23 15:03429 147 1
Fluorene ND ug/kg 03/09/23 16:09 86-73-703/08/23 15:03429 151 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 16:09 87-68-303/08/23 15:03429 186 1
Hexachlorobenzene ND ug/kg 03/09/23 16:09 118-74-103/08/23 15:03429 168 1
Hexachlorocyclopentadiene ND ug/kg 03/09/23 16:09 77-47-403/08/23 15:03429 246 1
Hexachloroethane ND ug/kg 03/09/23 16:09 67-72-103/08/23 15:03429 164 1
Indeno(1,2,3-cd)pyrene ND ug/kg 03/09/23 16:09 193-39-503/08/23 15:03429 169 1
Isophorone ND ug/kg 03/09/23 16:09 78-59-103/08/23 15:03429 191 1
1-Methylnaphthalene ND ug/kg 03/09/23 16:09 90-12-003/08/23 15:03429 151 1
2-Methylnaphthalene ND ug/kg 03/09/23 16:09 91-57-603/08/23 15:03429 172 1
2-Methylphenol(o-Cresol)ND ug/kg 03/09/23 16:09 95-48-703/08/23 15:03429 176 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/09/23 16:09 15831-10-403/08/23 15:03429 173 1
Naphthalene ND ug/kg 03/09/23 16:09 91-20-303/08/23 15:03429 146 1
2-Nitroaniline ND ug/kg 03/09/23 16:09 88-74-403/08/23 15:032150 351 1
3-Nitroaniline ND ug/kg 03/09/23 16:09 99-09-203/08/23 15:032150 337 1
4-Nitroaniline ND ug/kg 03/09/23 16:09 100-01-603/08/23 15:03859 326 1
Nitrobenzene ND ug/kg 03/09/23 16:09 98-95-303/08/23 15:03429 199 1
2-Nitrophenol ND ug/kg 03/09/23 16:09 88-75-503/08/23 15:03429 186 1
4-Nitrophenol ND ug/kg 03/09/23 16:09 100-02-703/08/23 15:032150 830 1
N-Nitrosodimethylamine ND ug/kg 03/09/23 16:09 62-75-903/08/23 15:03429 144 1
N-Nitroso-di-n-propylamine ND ug/kg 03/09/23 16:09 621-64-703/08/23 15:03429 161 1
N-Nitrosodiphenylamine ND ug/kg 03/09/23 16:09 86-30-603/08/23 15:03429 152 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/09/23 16:09 108-60-103/08/23 15:03429 204 1
Pentachlorophenol ND ug/kg 03/09/23 16:09 87-86-503/08/23 15:03859 420 1
Phenanthrene ND ug/kg 03/09/23 16:09 85-01-803/08/23 15:03429 140 1
Phenol ND ug/kg 03/09/23 16:09 108-95-203/08/23 15:03429 191 1
Pyrene ND ug/kg 03/09/23 16:09 129-00-003/08/23 15:03429 174 1
Pyridine ND ug/kg 03/09/23 16:09 110-86-103/08/23 15:03429 135 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 16:09 120-82-103/08/23 15:03429 169 1
2,4,5-Trichlorophenol ND ug/kg 03/09/23 16:09 95-95-403/08/23 15:03429 196 1
2,4,6-Trichlorophenol ND ug/kg 03/09/23 16:09 88-06-203/08/23 15:03429 177 1
Surrogates
Nitrobenzene-d5 (S)40 %03/09/23 16:09 4165-60-003/08/23 15:0310-130 1
2-Fluorobiphenyl (S)42 %03/09/23 16:09 321-60-803/08/23 15:0310-130 1
Terphenyl-d14 (S)50 %03/09/23 16:09 1718-51-003/08/23 15:0310-130 1
Phenol-d6 (S)39 %03/09/23 16:09 13127-88-303/08/23 15:0310-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-02 (0-2)Lab ID: 92655679004 Collected: 03/07/23 18:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)39 %03/09/23 16:09 367-12-403/08/23 15:0310-130 1
2,4,6-Tribromophenol (S)59 %03/09/23 16:09 118-79-603/08/23 15:0310-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/09/23 21:24 67-64-103/09/23 16:59149 48.0 1
Benzene ND ug/kg 03/09/23 21:24 71-43-203/09/23 16:597.5 3.0 1
Bromobenzene ND ug/kg 03/09/23 21:24 108-86-103/09/23 16:597.5 2.4 1
Bromochloromethane ND ug/kg 03/09/23 21:24 74-97-503/09/23 16:597.5 2.2 1
Bromodichloromethane ND ug/kg 03/09/23 21:24 75-27-403/09/23 16:597.5 2.9 1
Bromoform ND ug/kg 03/09/23 21:24 75-25-203/09/23 16:597.5 2.6 1
Bromomethane ND ug/kg 03/09/23 21:24 74-83-9 v203/09/23 16:5929.9 23.2 1
2-Butanone (MEK)ND ug/kg 03/09/23 21:24 78-93-303/09/23 16:59149 35.9 1
n-Butylbenzene ND ug/kg 03/09/23 21:24 104-51-803/09/23 16:597.5 4.7 1
sec-Butylbenzene ND ug/kg 03/09/23 21:24 135-98-803/09/23 16:597.5 3.3 1
tert-Butylbenzene ND ug/kg 03/09/23 21:24 98-06-603/09/23 16:597.5 2.7 1
Carbon tetrachloride ND ug/kg 03/09/23 21:24 56-23-5 IK03/09/23 16:597.5 2.8 1
Chlorobenzene ND ug/kg 03/09/23 21:24 108-90-703/09/23 16:597.5 4.3 1
Chloroethane ND ug/kg 03/09/23 21:24 75-00-303/09/23 16:5914.9 5.8 1
Chloroform ND ug/kg 03/09/23 21:24 67-66-303/09/23 16:597.5 6.2 1
Chloromethane 6.3J ug/kg 03/09/23 21:24 74-87-3 C803/09/23 16:5914.9 6.3 1
2-Chlorotoluene ND ug/kg 03/09/23 21:24 95-49-803/09/23 16:597.5 2.6 1
4-Chlorotoluene ND ug/kg 03/09/23 21:24 106-43-403/09/23 16:597.5 4.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/09/23 21:24 96-12-803/09/23 16:597.5 2.9 1
Dibromochloromethane ND ug/kg 03/09/23 21:24 124-48-1 IK03/09/23 16:597.5 4.2 1
1,2-Dibromoethane (EDB)ND ug/kg 03/09/23 21:24 106-93-403/09/23 16:597.5 3.3 1
Dibromomethane ND ug/kg 03/09/23 21:24 74-95-303/09/23 16:597.5 1.6 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 21:24 95-50-103/09/23 16:597.5 2.7 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 21:24 541-73-103/09/23 16:597.5 2.3 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 21:24 106-46-703/09/23 16:597.5 1.9 1
Dichlorodifluoromethane ND ug/kg 03/09/23 21:24 75-71-803/09/23 16:5914.9 7.6 1
1,1-Dichloroethane ND ug/kg 03/09/23 21:24 75-34-303/09/23 16:597.5 3.1 1
1,2-Dichloroethane ND ug/kg 03/09/23 21:24 107-06-203/09/23 16:597.5 4.9 1
1,1-Dichloroethene ND ug/kg 03/09/23 21:24 75-35-403/09/23 16:597.5 3.1 1
cis-1,2-Dichloroethene ND ug/kg 03/09/23 21:24 156-59-203/09/23 16:597.5 2.6 1
trans-1,2-Dichloroethene ND ug/kg 03/09/23 21:24 156-60-503/09/23 16:597.5 6.4 1
1,2-Dichloropropane ND ug/kg 03/09/23 21:24 78-87-503/09/23 16:597.5 2.2 1
1,3-Dichloropropane ND ug/kg 03/09/23 21:24 142-28-903/09/23 16:597.5 2.3 1
2,2-Dichloropropane ND ug/kg 03/09/23 21:24 594-20-703/09/23 16:597.5 5.7 1
1,1-Dichloropropene ND ug/kg 03/09/23 21:24 563-58-603/09/23 16:597.5 3.6 1
cis-1,3-Dichloropropene ND ug/kg 03/09/23 21:24 10061-01-503/09/23 16:597.5 2.0 1
trans-1,3-Dichloropropene ND ug/kg 03/09/23 21:24 10061-02-603/09/23 16:597.5 2.6 1
Diisopropyl ether ND ug/kg 03/09/23 21:24 108-20-303/09/23 16:597.5 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-02 (0-2)Lab ID: 92655679004 Collected: 03/07/23 18:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 03/09/23 21:24 100-41-403/09/23 16:597.5 3.5 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 21:24 87-68-303/09/23 16:5914.9 12.2 1
2-Hexanone ND ug/kg 03/09/23 21:24 591-78-603/09/23 16:5974.7 7.2 1
Isopropylbenzene (Cumene)ND ug/kg 03/09/23 21:24 98-82-803/09/23 16:597.5 2.5 1
p-Isopropyltoluene ND ug/kg 03/09/23 21:24 99-87-603/09/23 16:597.5 3.7 1
Methylene Chloride ND ug/kg 03/09/23 21:24 75-09-203/09/23 16:5929.9 20.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/09/23 21:24 108-10-103/09/23 16:5974.7 7.2 1
Methyl-tert-butyl ether ND ug/kg 03/09/23 21:24 1634-04-403/09/23 16:597.5 2.8 1
Naphthalene ND ug/kg 03/09/23 21:24 91-20-303/09/23 16:597.5 3.9 1
n-Propylbenzene ND ug/kg 03/09/23 21:24 103-65-103/09/23 16:597.5 2.7 1
Styrene ND ug/kg 03/09/23 21:24 100-42-5 IK03/09/23 16:597.5 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/09/23 21:24 630-20-603/09/23 16:597.5 2.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/09/23 21:24 79-34-503/09/23 16:597.5 2.0 1
Tetrachloroethene ND ug/kg 03/09/23 21:24 127-18-403/09/23 16:597.5 2.4 1
Toluene ND ug/kg 03/09/23 21:24 108-88-303/09/23 16:597.5 5.2 1
1,2,3-Trichlorobenzene ND ug/kg 03/09/23 21:24 87-61-603/09/23 16:597.5 6.0 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 21:24 120-82-103/09/23 16:597.5 6.3 1
1,1,1-Trichloroethane ND ug/kg 03/09/23 21:24 71-55-603/09/23 16:597.5 3.9 1
1,1,2-Trichloroethane ND ug/kg 03/09/23 21:24 79-00-503/09/23 16:597.5 2.5 1
Trichloroethene ND ug/kg 03/09/23 21:24 79-01-603/09/23 16:597.5 6.0 1
Trichlorofluoromethane ND ug/kg 03/09/23 21:24 75-69-403/09/23 16:597.5 4.1 1
1,2,3-Trichloropropane ND ug/kg 03/09/23 21:24 96-18-403/09/23 16:597.5 3.8 1
1,2,4-Trimethylbenzene ND ug/kg 03/09/23 21:24 95-63-603/09/23 16:597.5 4.4 1
1,3,5-Trimethylbenzene ND ug/kg 03/09/23 21:24 108-67-803/09/23 16:597.5 2.5 1
Vinyl acetate ND ug/kg 03/09/23 21:24 108-05-403/09/23 16:5974.7 15.4 1
Vinyl chloride ND ug/kg 03/09/23 21:24 75-01-403/09/23 16:5914.9 3.8 1
Xylene (Total)ND ug/kg 03/09/23 21:24 1330-20-703/09/23 16:5914.9 4.3 1
m&p-Xylene ND ug/kg 03/09/23 21:24 179601-23-103/09/23 16:5914.9 5.1 1
o-Xylene ND ug/kg 03/09/23 21:24 95-47-603/09/23 16:597.5 3.3 1
Surrogates
Toluene-d8 (S)98 %03/09/23 21:24 2037-26-503/09/23 16:5970-130 1
4-Bromofluorobenzene (S)112 %03/09/23 21:24 460-00-403/09/23 16:5970-130 1
1,2-Dichloroethane-d4 (S)102 %03/09/23 21:24 17060-07-003/09/23 16:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.9 %03/08/23 13:58 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 77.7 %03/13/23 15:2803/13/23 15:211
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-02 (0-2)Lab ID: 92655679004 Collected: 03/07/23 18:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.11J mg/kg 03/14/23 15:20 18540-29-9 J03/14/23 01:161.29 0.328 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-BG-1 (0-2)Lab ID: 92655679005 Collected: 03/07/23 13:05 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.1 mg/kg 03/14/23 16:54 7440-38-203/14/23 10:330.62 0.18 1
Barium 59.3 mg/kg 03/14/23 16:54 7440-39-303/14/23 10:330.37 0.094 1
Cadmium ND mg/kg 03/14/23 16:54 7440-43-903/14/23 10:330.10 0.037 1
Chromium 47.2 mg/kg 03/14/23 16:54 7440-47-303/14/23 10:332.5 0.48 1
Lead 10.9 mg/kg 03/14/23 16:54 7439-92-103/14/23 10:330.62 0.12 1
Selenium 0.57J mg/kg 03/14/23 16:54 7782-49-203/14/23 10:330.62 0.13 1
Silver ND mg/kg 03/14/23 16:54 7440-22-403/14/23 10:330.62 0.25 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.044 mg/kg 03/14/23 11:46 7439-97-603/13/23 15:150.025 0.011 1
Analytical Method: ASTM D2974
Pace Analytical Services - Minneapolis
Dry Weight / %M by ASTM D2974
Percent Moisture 24.1 %03/10/23 12:01 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 79.6 %03/13/23 15:2803/13/23 15:211
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.992J mg/kg 03/14/23 15:56 18540-29-9 J03/14/23 01:161.26 0.320 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-BG-2 (0-2)Lab ID: 92655679006 Collected: 03/07/23 13:15 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.9 mg/kg 03/14/23 17:00 7440-38-203/14/23 10:330.63 0.18 1
Barium 42.6 mg/kg 03/14/23 17:00 7440-39-303/14/23 10:330.38 0.095 1
Cadmium ND mg/kg 03/14/23 17:00 7440-43-903/14/23 10:330.10 0.037 1
Chromium 20.7 mg/kg 03/14/23 17:00 7440-47-303/14/23 10:332.5 0.49 1
Lead 11.1 mg/kg 03/14/23 17:00 7439-92-103/14/23 10:330.63 0.12 1
Selenium 0.60J mg/kg 03/14/23 17:00 7782-49-203/14/23 10:330.63 0.13 1
Silver ND mg/kg 03/14/23 17:00 7440-22-403/14/23 10:330.63 0.26 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.065 mg/kg 03/14/23 11:48 7439-97-603/13/23 15:150.025 0.011 1
Analytical Method: ASTM D2974
Pace Analytical Services - Minneapolis
Dry Weight / %M by ASTM D2974
Percent Moisture 23.5 %03/10/23 12:01 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 76.2 %03/13/23 15:2803/13/23 15:211
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.54 mg/kg 03/14/23 16:01 18540-29-903/14/23 01:161.31 0.334 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-DUP Lab ID: 92655679007 Collected: 03/07/23 00:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.7 mg/kg 03/14/23 17:12 7440-38-203/14/23 10:330.62 0.18 1
Barium 45.1 mg/kg 03/14/23 17:12 7440-39-303/14/23 10:330.37 0.093 1
Cadmium ND mg/kg 03/14/23 17:12 7440-43-903/14/23 10:330.099 0.037 1
Chromium 89.0 mg/kg 03/14/23 17:12 7440-47-303/14/23 10:332.5 0.48 1
Lead 6.9 mg/kg 03/14/23 17:12 7439-92-103/14/23 10:330.62 0.12 1
Selenium 0.68 mg/kg 03/14/23 17:12 7782-49-203/14/23 10:330.62 0.13 1
Silver ND mg/kg 03/14/23 17:12 7440-22-403/14/23 10:330.62 0.25 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.033 mg/kg 03/14/23 11:49 7439-97-603/13/23 15:150.025 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 03/09/23 16:37 83-32-903/08/23 15:03426 150 1
Acenaphthylene ND ug/kg 03/09/23 16:37 208-96-803/08/23 15:03426 150 1
Aniline ND ug/kg 03/09/23 16:37 62-53-303/08/23 15:03426 167 1
Anthracene ND ug/kg 03/09/23 16:37 120-12-703/08/23 15:03426 139 1
Benzo(a)anthracene ND ug/kg 03/09/23 16:37 56-55-303/08/23 15:03426 142 1
Benzo(a)pyrene ND ug/kg 03/09/23 16:37 50-32-803/08/23 15:03426 147 1
Benzo(b)fluoranthene ND ug/kg 03/09/23 16:37 205-99-203/08/23 15:03426 142 1
Benzo(g,h,i)perylene ND ug/kg 03/09/23 16:37 191-24-203/08/23 15:03426 165 1
Benzo(k)fluoranthene ND ug/kg 03/09/23 16:37 207-08-903/08/23 15:03426 150 1
Benzoic Acid ND ug/kg 03/09/23 16:37 65-85-003/08/23 15:032130 916 1
Benzyl alcohol ND ug/kg 03/09/23 16:37 100-51-603/08/23 15:03852 323 1
4-Bromophenylphenyl ether ND ug/kg 03/09/23 16:37 101-55-303/08/23 15:03426 164 1
Butylbenzylphthalate ND ug/kg 03/09/23 16:37 85-68-703/08/23 15:03426 180 1
4-Chloro-3-methylphenol ND ug/kg 03/09/23 16:37 59-50-703/08/23 15:03852 300 1
4-Chloroaniline ND ug/kg 03/09/23 16:37 106-47-803/08/23 15:03852 335 1
bis(2-Chloroethoxy)methane ND ug/kg 03/09/23 16:37 111-91-103/08/23 15:03426 177 1
bis(2-Chloroethyl) ether ND ug/kg 03/09/23 16:37 111-44-403/08/23 15:03426 160 1
2-Chloronaphthalene ND ug/kg 03/09/23 16:37 91-58-703/08/23 15:03426 169 1
2-Chlorophenol ND ug/kg 03/09/23 16:37 95-57-803/08/23 15:03426 160 1
4-Chlorophenylphenyl ether ND ug/kg 03/09/23 16:37 7005-72-303/08/23 15:03426 159 1
Chrysene ND ug/kg 03/09/23 16:37 218-01-903/08/23 15:03426 155 1
Dibenz(a,h)anthracene ND ug/kg 03/09/23 16:37 53-70-303/08/23 15:03426 164 1
Dibenzofuran ND ug/kg 03/09/23 16:37 132-64-903/08/23 15:03426 154 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 16:37 95-50-103/08/23 15:03426 154 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 16:37 541-73-103/08/23 15:03426 151 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 16:37 106-46-703/08/23 15:03426 163 1
3,3'-Dichlorobenzidine ND ug/kg 03/09/23 16:37 91-94-103/08/23 15:03852 288 1
2,4-Dichlorophenol ND ug/kg 03/09/23 16:37 120-83-203/08/23 15:03426 167 1
Diethylphthalate ND ug/kg 03/09/23 16:37 84-66-203/08/23 15:03426 156 1
2,4-Dimethylphenol ND ug/kg 03/09/23 16:37 105-67-903/08/23 15:03426 177 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-DUP Lab ID: 92655679007 Collected: 03/07/23 00:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 03/09/23 16:37 131-11-303/08/23 15:03426 155 1
Di-n-butylphthalate ND ug/kg 03/09/23 16:37 84-74-203/08/23 15:03426 143 1
4,6-Dinitro-2-methylphenol ND ug/kg 03/09/23 16:37 534-52-103/08/23 15:03852 398 1
2,4-Dinitrophenol ND ug/kg 03/09/23 16:37 51-28-503/08/23 15:032130 1320 1
2,4-Dinitrotoluene ND ug/kg 03/09/23 16:37 121-14-203/08/23 15:03426 164 1
2,6-Dinitrotoluene ND ug/kg 03/09/23 16:37 606-20-203/08/23 15:03426 156 1
Di-n-octylphthalate ND ug/kg 03/09/23 16:37 117-84-003/08/23 15:03426 168 1
bis(2-Ethylhexyl)phthalate ND ug/kg 03/09/23 16:37 117-81-703/08/23 15:03426 165 1
Fluoranthene ND ug/kg 03/09/23 16:37 206-44-003/08/23 15:03426 146 1
Fluorene ND ug/kg 03/09/23 16:37 86-73-703/08/23 15:03426 150 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 16:37 87-68-303/08/23 15:03426 185 1
Hexachlorobenzene ND ug/kg 03/09/23 16:37 118-74-103/08/23 15:03426 167 1
Hexachlorocyclopentadiene ND ug/kg 03/09/23 16:37 77-47-403/08/23 15:03426 244 1
Hexachloroethane ND ug/kg 03/09/23 16:37 67-72-103/08/23 15:03426 163 1
Indeno(1,2,3-cd)pyrene ND ug/kg 03/09/23 16:37 193-39-503/08/23 15:03426 168 1
Isophorone ND ug/kg 03/09/23 16:37 78-59-103/08/23 15:03426 190 1
1-Methylnaphthalene ND ug/kg 03/09/23 16:37 90-12-003/08/23 15:03426 150 1
2-Methylnaphthalene ND ug/kg 03/09/23 16:37 91-57-603/08/23 15:03426 170 1
2-Methylphenol(o-Cresol)ND ug/kg 03/09/23 16:37 95-48-703/08/23 15:03426 174 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/09/23 16:37 15831-10-403/08/23 15:03426 172 1
Naphthalene ND ug/kg 03/09/23 16:37 91-20-303/08/23 15:03426 145 1
2-Nitroaniline ND ug/kg 03/09/23 16:37 88-74-403/08/23 15:032130 349 1
3-Nitroaniline ND ug/kg 03/09/23 16:37 99-09-203/08/23 15:032130 335 1
4-Nitroaniline ND ug/kg 03/09/23 16:37 100-01-603/08/23 15:03852 324 1
Nitrobenzene ND ug/kg 03/09/23 16:37 98-95-303/08/23 15:03426 198 1
2-Nitrophenol ND ug/kg 03/09/23 16:37 88-75-503/08/23 15:03426 185 1
4-Nitrophenol ND ug/kg 03/09/23 16:37 100-02-703/08/23 15:032130 824 1
N-Nitrosodimethylamine ND ug/kg 03/09/23 16:37 62-75-903/08/23 15:03426 143 1
N-Nitroso-di-n-propylamine ND ug/kg 03/09/23 16:37 621-64-703/08/23 15:03426 160 1
N-Nitrosodiphenylamine ND ug/kg 03/09/23 16:37 86-30-603/08/23 15:03426 151 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/09/23 16:37 108-60-103/08/23 15:03426 203 1
Pentachlorophenol ND ug/kg 03/09/23 16:37 87-86-503/08/23 15:03852 417 1
Phenanthrene ND ug/kg 03/09/23 16:37 85-01-803/08/23 15:03426 139 1
Phenol ND ug/kg 03/09/23 16:37 108-95-203/08/23 15:03426 190 1
Pyrene ND ug/kg 03/09/23 16:37 129-00-003/08/23 15:03426 173 1
Pyridine ND ug/kg 03/09/23 16:37 110-86-103/08/23 15:03426 134 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 16:37 120-82-103/08/23 15:03426 168 1
2,4,5-Trichlorophenol ND ug/kg 03/09/23 16:37 95-95-403/08/23 15:03426 195 1
2,4,6-Trichlorophenol ND ug/kg 03/09/23 16:37 88-06-203/08/23 15:03426 176 1
Surrogates
Nitrobenzene-d5 (S)66 %03/09/23 16:37 4165-60-003/08/23 15:0310-130 1
2-Fluorobiphenyl (S)66 %03/09/23 16:37 321-60-803/08/23 15:0310-130 1
Terphenyl-d14 (S)62 %03/09/23 16:37 1718-51-003/08/23 15:0310-130 1
Phenol-d6 (S)62 %03/09/23 16:37 13127-88-303/08/23 15:0310-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-DUP Lab ID: 92655679007 Collected: 03/07/23 00:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)61 %03/09/23 16:37 367-12-403/08/23 15:0310-130 1
2,4,6-Tribromophenol (S)78 %03/09/23 16:37 118-79-603/08/23 15:0310-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/09/23 22:57 67-64-103/09/23 16:59151 48.3 1
Benzene ND ug/kg 03/09/23 22:57 71-43-203/09/23 16:597.5 3.0 1
Bromobenzene ND ug/kg 03/09/23 22:57 108-86-103/09/23 16:597.5 2.5 1
Bromochloromethane ND ug/kg 03/09/23 22:57 74-97-503/09/23 16:597.5 2.2 1
Bromodichloromethane ND ug/kg 03/09/23 22:57 75-27-403/09/23 16:597.5 2.9 1
Bromoform ND ug/kg 03/09/23 22:57 75-25-203/09/23 16:597.5 2.7 1
Bromomethane ND ug/kg 03/09/23 22:57 74-83-9 v203/09/23 16:5930.1 23.3 1
2-Butanone (MEK)ND ug/kg 03/09/23 22:57 78-93-303/09/23 16:59151 36.1 1
n-Butylbenzene ND ug/kg 03/09/23 22:57 104-51-803/09/23 16:597.5 4.7 1
sec-Butylbenzene ND ug/kg 03/09/23 22:57 135-98-803/09/23 16:597.5 3.3 1
tert-Butylbenzene ND ug/kg 03/09/23 22:57 98-06-603/09/23 16:597.5 2.7 1
Carbon tetrachloride ND ug/kg 03/09/23 22:57 56-23-5 IK03/09/23 16:597.5 2.8 1
Chlorobenzene ND ug/kg 03/09/23 22:57 108-90-703/09/23 16:597.5 4.3 1
Chloroethane ND ug/kg 03/09/23 22:57 75-00-303/09/23 16:5915.1 5.8 1
Chloroform ND ug/kg 03/09/23 22:57 67-66-303/09/23 16:597.5 6.3 1
Chloromethane ND ug/kg 03/09/23 22:57 74-87-303/09/23 16:5915.1 6.3 1
2-Chlorotoluene ND ug/kg 03/09/23 22:57 95-49-803/09/23 16:597.5 2.7 1
4-Chlorotoluene ND ug/kg 03/09/23 22:57 106-43-403/09/23 16:597.5 4.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/09/23 22:57 96-12-803/09/23 16:597.5 2.9 1
Dibromochloromethane ND ug/kg 03/09/23 22:57 124-48-1 IK03/09/23 16:597.5 4.2 1
1,2-Dibromoethane (EDB)ND ug/kg 03/09/23 22:57 106-93-403/09/23 16:597.5 3.3 1
Dibromomethane ND ug/kg 03/09/23 22:57 74-95-303/09/23 16:597.5 1.6 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 22:57 95-50-103/09/23 16:597.5 2.7 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 22:57 541-73-103/09/23 16:597.5 2.3 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 22:57 106-46-703/09/23 16:597.5 2.0 1
Dichlorodifluoromethane ND ug/kg 03/09/23 22:57 75-71-803/09/23 16:5915.1 7.7 1
1,1-Dichloroethane ND ug/kg 03/09/23 22:57 75-34-303/09/23 16:597.5 3.1 1
1,2-Dichloroethane ND ug/kg 03/09/23 22:57 107-06-203/09/23 16:597.5 5.0 1
1,1-Dichloroethene ND ug/kg 03/09/23 22:57 75-35-403/09/23 16:597.5 3.1 1
cis-1,2-Dichloroethene ND ug/kg 03/09/23 22:57 156-59-203/09/23 16:597.5 2.6 1
trans-1,2-Dichloroethene ND ug/kg 03/09/23 22:57 156-60-503/09/23 16:597.5 6.4 1
1,2-Dichloropropane ND ug/kg 03/09/23 22:57 78-87-503/09/23 16:597.5 2.3 1
1,3-Dichloropropane ND ug/kg 03/09/23 22:57 142-28-903/09/23 16:597.5 2.3 1
2,2-Dichloropropane ND ug/kg 03/09/23 22:57 594-20-703/09/23 16:597.5 5.7 1
1,1-Dichloropropene ND ug/kg 03/09/23 22:57 563-58-603/09/23 16:597.5 3.6 1
cis-1,3-Dichloropropene ND ug/kg 03/09/23 22:57 10061-01-503/09/23 16:597.5 2.0 1
trans-1,3-Dichloropropene ND ug/kg 03/09/23 22:57 10061-02-603/09/23 16:597.5 2.6 1
Diisopropyl ether ND ug/kg 03/09/23 22:57 108-20-303/09/23 16:597.5 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-DUP Lab ID: 92655679007 Collected: 03/07/23 00:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 03/09/23 22:57 100-41-403/09/23 16:597.5 3.5 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 22:57 87-68-303/09/23 16:5915.1 12.3 1
2-Hexanone ND ug/kg 03/09/23 22:57 591-78-603/09/23 16:5975.3 7.3 1
Isopropylbenzene (Cumene)ND ug/kg 03/09/23 22:57 98-82-803/09/23 16:597.5 2.6 1
p-Isopropyltoluene ND ug/kg 03/09/23 22:57 99-87-603/09/23 16:597.5 3.7 1
Methylene Chloride ND ug/kg 03/09/23 22:57 75-09-203/09/23 16:5930.1 20.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/09/23 22:57 108-10-103/09/23 16:5975.3 7.3 1
Methyl-tert-butyl ether ND ug/kg 03/09/23 22:57 1634-04-403/09/23 16:597.5 2.8 1
Naphthalene ND ug/kg 03/09/23 22:57 91-20-303/09/23 16:597.5 4.0 1
n-Propylbenzene ND ug/kg 03/09/23 22:57 103-65-103/09/23 16:597.5 2.7 1
Styrene ND ug/kg 03/09/23 22:57 100-42-5 IK03/09/23 16:597.5 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/09/23 22:57 630-20-603/09/23 16:597.5 2.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/09/23 22:57 79-34-503/09/23 16:597.5 2.0 1
Tetrachloroethene ND ug/kg 03/09/23 22:57 127-18-403/09/23 16:597.5 2.4 1
Toluene ND ug/kg 03/09/23 22:57 108-88-303/09/23 16:597.5 5.2 1
1,2,3-Trichlorobenzene ND ug/kg 03/09/23 22:57 87-61-603/09/23 16:597.5 6.1 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 22:57 120-82-103/09/23 16:597.5 6.3 1
1,1,1-Trichloroethane ND ug/kg 03/09/23 22:57 71-55-603/09/23 16:597.5 3.9 1
1,1,2-Trichloroethane ND ug/kg 03/09/23 22:57 79-00-503/09/23 16:597.5 2.5 1
Trichloroethene ND ug/kg 03/09/23 22:57 79-01-603/09/23 16:597.5 6.1 1
Trichlorofluoromethane ND ug/kg 03/09/23 22:57 75-69-403/09/23 16:597.5 4.1 1
1,2,3-Trichloropropane ND ug/kg 03/09/23 22:57 96-18-403/09/23 16:597.5 3.8 1
1,2,4-Trimethylbenzene ND ug/kg 03/09/23 22:57 95-63-603/09/23 16:597.5 4.5 1
1,3,5-Trimethylbenzene ND ug/kg 03/09/23 22:57 108-67-803/09/23 16:597.5 2.5 1
Vinyl acetate ND ug/kg 03/09/23 22:57 108-05-403/09/23 16:5975.3 15.5 1
Vinyl chloride ND ug/kg 03/09/23 22:57 75-01-403/09/23 16:5915.1 3.8 1
Xylene (Total)ND ug/kg 03/09/23 22:57 1330-20-703/09/23 16:5915.1 4.3 1
m&p-Xylene ND ug/kg 03/09/23 22:57 179601-23-103/09/23 16:5915.1 5.2 1
o-Xylene ND ug/kg 03/09/23 22:57 95-47-603/09/23 16:597.5 3.3 1
Surrogates
Toluene-d8 (S)99 %03/09/23 22:57 2037-26-503/09/23 16:5970-130 1
4-Bromofluorobenzene (S)108 %03/09/23 22:57 460-00-403/09/23 16:5970-130 1
1,2-Dichloroethane-d4 (S)107 %03/09/23 22:57 17060-07-003/09/23 16:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.1 %03/08/23 13:58 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 76.3 %03/13/23 15:2803/13/23 15:211
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-DUP Lab ID: 92655679007 Collected: 03/07/23 00:00 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.522J mg/kg 03/14/23 16:06 18540-29-9 J03/14/23 01:161.31 0.334 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-01 (2-4)Lab ID: 92655679008 Collected: 03/07/23 17:40 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.6 mg/kg 03/14/23 17:18 7440-38-203/14/23 10:330.64 0.18 1
Barium 76.7 mg/kg 03/14/23 17:18 7440-39-303/14/23 10:330.38 0.096 1
Cadmium ND mg/kg 03/14/23 17:18 7440-43-903/14/23 10:330.10 0.038 1
Chromium 48.6 mg/kg 03/14/23 17:18 7440-47-303/14/23 10:332.6 0.50 1
Lead 9.8 mg/kg 03/14/23 17:18 7439-92-103/14/23 10:330.64 0.12 1
Selenium 0.47J mg/kg 03/14/23 17:18 7782-49-203/14/23 10:330.64 0.13 1
Silver ND mg/kg 03/14/23 17:18 7440-22-403/14/23 10:330.64 0.26 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.074 mg/kg 03/14/23 11:51 7439-97-603/13/23 15:150.023 0.010 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 03/09/23 17:05 83-32-903/08/23 15:03441 155 1
Acenaphthylene ND ug/kg 03/09/23 17:05 208-96-803/08/23 15:03441 155 1
Aniline ND ug/kg 03/09/23 17:05 62-53-303/08/23 15:03441 172 1
Anthracene ND ug/kg 03/09/23 17:05 120-12-703/08/23 15:03441 144 1
Benzo(a)anthracene ND ug/kg 03/09/23 17:05 56-55-303/08/23 15:03441 147 1
Benzo(a)pyrene ND ug/kg 03/09/23 17:05 50-32-803/08/23 15:03441 152 1
Benzo(b)fluoranthene ND ug/kg 03/09/23 17:05 205-99-203/08/23 15:03441 147 1
Benzo(g,h,i)perylene ND ug/kg 03/09/23 17:05 191-24-203/08/23 15:03441 171 1
Benzo(k)fluoranthene ND ug/kg 03/09/23 17:05 207-08-903/08/23 15:03441 155 1
Benzoic Acid ND ug/kg 03/09/23 17:05 65-85-003/08/23 15:032200 947 1
Benzyl alcohol ND ug/kg 03/09/23 17:05 100-51-603/08/23 15:03882 334 1
4-Bromophenylphenyl ether ND ug/kg 03/09/23 17:05 101-55-303/08/23 15:03441 170 1
Butylbenzylphthalate ND ug/kg 03/09/23 17:05 85-68-703/08/23 15:03441 186 1
4-Chloro-3-methylphenol ND ug/kg 03/09/23 17:05 59-50-703/08/23 15:03882 310 1
4-Chloroaniline ND ug/kg 03/09/23 17:05 106-47-803/08/23 15:03882 346 1
bis(2-Chloroethoxy)methane ND ug/kg 03/09/23 17:05 111-91-103/08/23 15:03441 183 1
bis(2-Chloroethyl) ether ND ug/kg 03/09/23 17:05 111-44-403/08/23 15:03441 166 1
2-Chloronaphthalene ND ug/kg 03/09/23 17:05 91-58-703/08/23 15:03441 175 1
2-Chlorophenol ND ug/kg 03/09/23 17:05 95-57-803/08/23 15:03441 166 1
4-Chlorophenylphenyl ether ND ug/kg 03/09/23 17:05 7005-72-303/08/23 15:03441 164 1
Chrysene ND ug/kg 03/09/23 17:05 218-01-903/08/23 15:03441 160 1
Dibenz(a,h)anthracene ND ug/kg 03/09/23 17:05 53-70-303/08/23 15:03441 170 1
Dibenzofuran ND ug/kg 03/09/23 17:05 132-64-903/08/23 15:03441 159 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 17:05 95-50-103/08/23 15:03441 159 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 17:05 541-73-103/08/23 15:03441 156 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 17:05 106-46-703/08/23 15:03441 168 1
3,3'-Dichlorobenzidine ND ug/kg 03/09/23 17:05 91-94-103/08/23 15:03882 298 1
2,4-Dichlorophenol ND ug/kg 03/09/23 17:05 120-83-203/08/23 15:03441 172 1
Diethylphthalate ND ug/kg 03/09/23 17:05 84-66-203/08/23 15:03441 162 1
2,4-Dimethylphenol ND ug/kg 03/09/23 17:05 105-67-903/08/23 15:03441 183 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-01 (2-4)Lab ID: 92655679008 Collected: 03/07/23 17:40 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 03/09/23 17:05 131-11-303/08/23 15:03441 160 1
Di-n-butylphthalate ND ug/kg 03/09/23 17:05 84-74-203/08/23 15:03441 148 1
4,6-Dinitro-2-methylphenol ND ug/kg 03/09/23 17:05 534-52-103/08/23 15:03882 411 1
2,4-Dinitrophenol ND ug/kg 03/09/23 17:05 51-28-503/08/23 15:032200 1360 1
2,4-Dinitrotoluene ND ug/kg 03/09/23 17:05 121-14-203/08/23 15:03441 170 1
2,6-Dinitrotoluene ND ug/kg 03/09/23 17:05 606-20-203/08/23 15:03441 162 1
Di-n-octylphthalate ND ug/kg 03/09/23 17:05 117-84-003/08/23 15:03441 174 1
bis(2-Ethylhexyl)phthalate ND ug/kg 03/09/23 17:05 117-81-703/08/23 15:03441 171 1
Fluoranthene ND ug/kg 03/09/23 17:05 206-44-003/08/23 15:03441 151 1
Fluorene ND ug/kg 03/09/23 17:05 86-73-703/08/23 15:03441 155 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 17:05 87-68-303/08/23 15:03441 191 1
Hexachlorobenzene ND ug/kg 03/09/23 17:05 118-74-103/08/23 15:03441 172 1
Hexachlorocyclopentadiene ND ug/kg 03/09/23 17:05 77-47-403/08/23 15:03441 252 1
Hexachloroethane ND ug/kg 03/09/23 17:05 67-72-103/08/23 15:03441 168 1
Indeno(1,2,3-cd)pyrene ND ug/kg 03/09/23 17:05 193-39-503/08/23 15:03441 174 1
Isophorone ND ug/kg 03/09/23 17:05 78-59-103/08/23 15:03441 196 1
1-Methylnaphthalene ND ug/kg 03/09/23 17:05 90-12-003/08/23 15:03441 155 1
2-Methylnaphthalene ND ug/kg 03/09/23 17:05 91-57-603/08/23 15:03441 176 1
2-Methylphenol(o-Cresol)ND ug/kg 03/09/23 17:05 95-48-703/08/23 15:03441 180 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/09/23 17:05 15831-10-403/08/23 15:03441 178 1
Naphthalene ND ug/kg 03/09/23 17:05 91-20-303/08/23 15:03441 150 1
2-Nitroaniline ND ug/kg 03/09/23 17:05 88-74-403/08/23 15:032200 361 1
3-Nitroaniline ND ug/kg 03/09/23 17:05 99-09-203/08/23 15:032200 346 1
4-Nitroaniline ND ug/kg 03/09/23 17:05 100-01-603/08/23 15:03882 335 1
Nitrobenzene ND ug/kg 03/09/23 17:05 98-95-303/08/23 15:03441 204 1
2-Nitrophenol ND ug/kg 03/09/23 17:05 88-75-503/08/23 15:03441 191 1
4-Nitrophenol ND ug/kg 03/09/23 17:05 100-02-703/08/23 15:032200 852 1
N-Nitrosodimethylamine ND ug/kg 03/09/23 17:05 62-75-903/08/23 15:03441 148 1
N-Nitroso-di-n-propylamine ND ug/kg 03/09/23 17:05 621-64-703/08/23 15:03441 166 1
N-Nitrosodiphenylamine ND ug/kg 03/09/23 17:05 86-30-603/08/23 15:03441 156 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/09/23 17:05 108-60-103/08/23 15:03441 210 1
Pentachlorophenol ND ug/kg 03/09/23 17:05 87-86-503/08/23 15:03882 431 1
Phenanthrene ND ug/kg 03/09/23 17:05 85-01-803/08/23 15:03441 144 1
Phenol ND ug/kg 03/09/23 17:05 108-95-203/08/23 15:03441 196 1
Pyrene ND ug/kg 03/09/23 17:05 129-00-003/08/23 15:03441 179 1
Pyridine ND ug/kg 03/09/23 17:05 110-86-103/08/23 15:03441 139 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 17:05 120-82-103/08/23 15:03441 174 1
2,4,5-Trichlorophenol ND ug/kg 03/09/23 17:05 95-95-403/08/23 15:03441 202 1
2,4,6-Trichlorophenol ND ug/kg 03/09/23 17:05 88-06-203/08/23 15:03441 182 1
Surrogates
Nitrobenzene-d5 (S)63 %03/09/23 17:05 4165-60-003/08/23 15:0310-130 1
2-Fluorobiphenyl (S)65 %03/09/23 17:05 321-60-803/08/23 15:0310-130 1
Terphenyl-d14 (S)65 %03/09/23 17:05 1718-51-003/08/23 15:0310-130 1
Phenol-d6 (S)59 %03/09/23 17:05 13127-88-303/08/23 15:0310-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-01 (2-4)Lab ID: 92655679008 Collected: 03/07/23 17:40 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)57 %03/09/23 17:05 367-12-403/08/23 15:0310-130 1
2,4,6-Tribromophenol (S)77 %03/09/23 17:05 118-79-603/08/23 15:0310-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/09/23 23:16 67-64-103/09/23 16:59145 46.5 1
Benzene ND ug/kg 03/09/23 23:16 71-43-203/09/23 16:597.2 2.9 1
Bromobenzene ND ug/kg 03/09/23 23:16 108-86-103/09/23 16:597.2 2.4 1
Bromochloromethane ND ug/kg 03/09/23 23:16 74-97-503/09/23 16:597.2 2.1 1
Bromodichloromethane ND ug/kg 03/09/23 23:16 75-27-403/09/23 16:597.2 2.8 1
Bromoform ND ug/kg 03/09/23 23:16 75-25-203/09/23 16:597.2 2.6 1
Bromomethane ND ug/kg 03/09/23 23:16 74-83-9 v203/09/23 16:5929.0 22.5 1
2-Butanone (MEK)ND ug/kg 03/09/23 23:16 78-93-303/09/23 16:59145 34.8 1
n-Butylbenzene ND ug/kg 03/09/23 23:16 104-51-803/09/23 16:597.2 4.6 1
sec-Butylbenzene ND ug/kg 03/09/23 23:16 135-98-803/09/23 16:597.2 3.2 1
tert-Butylbenzene ND ug/kg 03/09/23 23:16 98-06-603/09/23 16:597.2 2.6 1
Carbon tetrachloride ND ug/kg 03/09/23 23:16 56-23-5 IK03/09/23 16:597.2 2.7 1
Chlorobenzene ND ug/kg 03/09/23 23:16 108-90-703/09/23 16:597.2 4.2 1
Chloroethane ND ug/kg 03/09/23 23:16 75-00-303/09/23 16:5914.5 5.6 1
Chloroform ND ug/kg 03/09/23 23:16 67-66-303/09/23 16:597.2 6.1 1
Chloromethane ND ug/kg 03/09/23 23:16 74-87-303/09/23 16:5914.5 6.1 1
2-Chlorotoluene ND ug/kg 03/09/23 23:16 95-49-803/09/23 16:597.2 2.6 1
4-Chlorotoluene ND ug/kg 03/09/23 23:16 106-43-403/09/23 16:597.2 4.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/09/23 23:16 96-12-803/09/23 16:597.2 2.8 1
Dibromochloromethane ND ug/kg 03/09/23 23:16 124-48-1 IK03/09/23 16:597.2 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 03/09/23 23:16 106-93-403/09/23 16:597.2 3.2 1
Dibromomethane ND ug/kg 03/09/23 23:16 74-95-303/09/23 16:597.2 1.6 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 23:16 95-50-103/09/23 16:597.2 2.6 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 23:16 541-73-103/09/23 16:597.2 2.2 1
1,4-Dichlorobenzene 3.7J ug/kg 03/09/23 23:16 106-46-703/09/23 16:597.2 1.9 1
Dichlorodifluoromethane ND ug/kg 03/09/23 23:16 75-71-803/09/23 16:5914.5 7.4 1
1,1-Dichloroethane ND ug/kg 03/09/23 23:16 75-34-303/09/23 16:597.2 3.0 1
1,2-Dichloroethane ND ug/kg 03/09/23 23:16 107-06-203/09/23 16:597.2 4.8 1
1,1-Dichloroethene ND ug/kg 03/09/23 23:16 75-35-403/09/23 16:597.2 3.0 1
cis-1,2-Dichloroethene ND ug/kg 03/09/23 23:16 156-59-203/09/23 16:597.2 2.5 1
trans-1,2-Dichloroethene ND ug/kg 03/09/23 23:16 156-60-503/09/23 16:597.2 6.2 1
1,2-Dichloropropane ND ug/kg 03/09/23 23:16 78-87-503/09/23 16:597.2 2.2 1
1,3-Dichloropropane ND ug/kg 03/09/23 23:16 142-28-903/09/23 16:597.2 2.3 1
2,2-Dichloropropane ND ug/kg 03/09/23 23:16 594-20-703/09/23 16:597.2 5.5 1
1,1-Dichloropropene ND ug/kg 03/09/23 23:16 563-58-603/09/23 16:597.2 3.5 1
cis-1,3-Dichloropropene ND ug/kg 03/09/23 23:16 10061-01-503/09/23 16:597.2 2.0 1
trans-1,3-Dichloropropene ND ug/kg 03/09/23 23:16 10061-02-603/09/23 16:597.2 2.5 1
Diisopropyl ether ND ug/kg 03/09/23 23:16 108-20-303/09/23 16:597.2 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-01 (2-4)Lab ID: 92655679008 Collected: 03/07/23 17:40 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 03/09/23 23:16 100-41-403/09/23 16:597.2 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 23:16 87-68-303/09/23 16:5914.5 11.9 1
2-Hexanone ND ug/kg 03/09/23 23:16 591-78-603/09/23 16:5972.5 7.0 1
Isopropylbenzene (Cumene)ND ug/kg 03/09/23 23:16 98-82-803/09/23 16:597.2 2.5 1
p-Isopropyltoluene ND ug/kg 03/09/23 23:16 99-87-603/09/23 16:597.2 3.6 1
Methylene Chloride ND ug/kg 03/09/23 23:16 75-09-203/09/23 16:5929.0 19.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/09/23 23:16 108-10-103/09/23 16:5972.5 7.0 1
Methyl-tert-butyl ether ND ug/kg 03/09/23 23:16 1634-04-403/09/23 16:597.2 2.7 1
Naphthalene ND ug/kg 03/09/23 23:16 91-20-303/09/23 16:597.2 3.8 1
n-Propylbenzene ND ug/kg 03/09/23 23:16 103-65-103/09/23 16:597.2 2.6 1
Styrene ND ug/kg 03/09/23 23:16 100-42-5 IK03/09/23 16:597.2 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/09/23 23:16 630-20-603/09/23 16:597.2 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/09/23 23:16 79-34-503/09/23 16:597.2 1.9 1
Tetrachloroethene ND ug/kg 03/09/23 23:16 127-18-403/09/23 16:597.2 2.3 1
Toluene ND ug/kg 03/09/23 23:16 108-88-303/09/23 16:597.2 5.0 1
1,2,3-Trichlorobenzene ND ug/kg 03/09/23 23:16 87-61-603/09/23 16:597.2 5.9 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 23:16 120-82-103/09/23 16:597.2 6.1 1
1,1,1-Trichloroethane ND ug/kg 03/09/23 23:16 71-55-603/09/23 16:597.2 3.8 1
1,1,2-Trichloroethane ND ug/kg 03/09/23 23:16 79-00-503/09/23 16:597.2 2.4 1
Trichloroethene ND ug/kg 03/09/23 23:16 79-01-603/09/23 16:597.2 5.8 1
Trichlorofluoromethane ND ug/kg 03/09/23 23:16 75-69-403/09/23 16:597.2 4.0 1
1,2,3-Trichloropropane ND ug/kg 03/09/23 23:16 96-18-403/09/23 16:597.2 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/09/23 23:16 95-63-603/09/23 16:597.2 4.3 1
1,3,5-Trimethylbenzene ND ug/kg 03/09/23 23:16 108-67-803/09/23 16:597.2 2.4 1
Vinyl acetate ND ug/kg 03/09/23 23:16 108-05-403/09/23 16:5972.5 14.9 1
Vinyl chloride ND ug/kg 03/09/23 23:16 75-01-403/09/23 16:5914.5 3.7 1
Xylene (Total)ND ug/kg 03/09/23 23:16 1330-20-703/09/23 16:5914.5 4.1 1
m&p-Xylene ND ug/kg 03/09/23 23:16 179601-23-103/09/23 16:5914.5 5.0 1
o-Xylene ND ug/kg 03/09/23 23:16 95-47-603/09/23 16:597.2 3.2 1
Surrogates
Toluene-d8 (S)98 %03/09/23 23:16 2037-26-503/09/23 16:5970-130 1
4-Bromofluorobenzene (S)109 %03/09/23 23:16 460-00-403/09/23 16:5970-130 1
1,2-Dichloroethane-d4 (S)102 %03/09/23 23:16 17060-07-003/09/23 16:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.4 %03/08/23 17:05 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 77.0 %03/13/23 15:2803/13/23 15:211
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-01 (2-4)Lab ID: 92655679008 Collected: 03/07/23 17:40 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.734J mg/kg 03/14/23 16:12 18540-29-9 J03/14/23 01:161.30 0.331 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-02 (2-4)Lab ID: 92655679009 Collected: 03/07/23 18:10 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.8 mg/kg 03/14/23 17:24 7440-38-203/14/23 10:330.61 0.17 1
Barium 64.0 mg/kg 03/14/23 17:24 7440-39-303/14/23 10:330.37 0.092 1
Cadmium ND mg/kg 03/14/23 17:24 7440-43-903/14/23 10:330.098 0.036 1
Chromium 36.0 mg/kg 03/14/23 17:24 7440-47-303/14/23 10:332.4 0.47 1
Lead 7.6 mg/kg 03/14/23 17:24 7439-92-103/14/23 10:330.61 0.11 1
Selenium 0.60J mg/kg 03/14/23 17:24 7782-49-203/14/23 10:330.61 0.13 1
Silver ND mg/kg 03/14/23 17:24 7440-22-403/14/23 10:330.61 0.25 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.048 mg/kg 03/14/23 11:53 7439-97-603/13/23 15:150.025 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 03/09/23 17:32 83-32-903/08/23 15:03442 155 1
Acenaphthylene ND ug/kg 03/09/23 17:32 208-96-803/08/23 15:03442 155 1
Aniline ND ug/kg 03/09/23 17:32 62-53-303/08/23 15:03442 173 1
Anthracene ND ug/kg 03/09/23 17:32 120-12-703/08/23 15:03442 145 1
Benzo(a)anthracene ND ug/kg 03/09/23 17:32 56-55-303/08/23 15:03442 147 1
Benzo(a)pyrene ND ug/kg 03/09/23 17:32 50-32-803/08/23 15:03442 153 1
Benzo(b)fluoranthene ND ug/kg 03/09/23 17:32 205-99-203/08/23 15:03442 147 1
Benzo(g,h,i)perylene ND ug/kg 03/09/23 17:32 191-24-203/08/23 15:03442 171 1
Benzo(k)fluoranthene ND ug/kg 03/09/23 17:32 207-08-903/08/23 15:03442 155 1
Benzoic Acid ND ug/kg 03/09/23 17:32 65-85-003/08/23 15:032210 949 1
Benzyl alcohol ND ug/kg 03/09/23 17:32 100-51-603/08/23 15:03883 335 1
4-Bromophenylphenyl ether ND ug/kg 03/09/23 17:32 101-55-303/08/23 15:03442 170 1
Butylbenzylphthalate ND ug/kg 03/09/23 17:32 85-68-703/08/23 15:03442 186 1
4-Chloro-3-methylphenol ND ug/kg 03/09/23 17:32 59-50-703/08/23 15:03883 310 1
4-Chloroaniline ND ug/kg 03/09/23 17:32 106-47-803/08/23 15:03883 347 1
bis(2-Chloroethoxy)methane ND ug/kg 03/09/23 17:32 111-91-103/08/23 15:03442 183 1
bis(2-Chloroethyl) ether ND ug/kg 03/09/23 17:32 111-44-403/08/23 15:03442 166 1
2-Chloronaphthalene ND ug/kg 03/09/23 17:32 91-58-703/08/23 15:03442 175 1
2-Chlorophenol ND ug/kg 03/09/23 17:32 95-57-803/08/23 15:03442 166 1
4-Chlorophenylphenyl ether ND ug/kg 03/09/23 17:32 7005-72-303/08/23 15:03442 165 1
Chrysene ND ug/kg 03/09/23 17:32 218-01-903/08/23 15:03442 161 1
Dibenz(a,h)anthracene ND ug/kg 03/09/23 17:32 53-70-303/08/23 15:03442 170 1
Dibenzofuran ND ug/kg 03/09/23 17:32 132-64-903/08/23 15:03442 159 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 17:32 95-50-103/08/23 15:03442 159 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 17:32 541-73-103/08/23 15:03442 157 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 17:32 106-46-703/08/23 15:03442 169 1
3,3'-Dichlorobenzidine ND ug/kg 03/09/23 17:32 91-94-103/08/23 15:03883 298 1
2,4-Dichlorophenol ND ug/kg 03/09/23 17:32 120-83-203/08/23 15:03442 173 1
Diethylphthalate ND ug/kg 03/09/23 17:32 84-66-203/08/23 15:03442 162 1
2,4-Dimethylphenol ND ug/kg 03/09/23 17:32 105-67-903/08/23 15:03442 183 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-02 (2-4)Lab ID: 92655679009 Collected: 03/07/23 18:10 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 03/09/23 17:32 131-11-303/08/23 15:03442 161 1
Di-n-butylphthalate ND ug/kg 03/09/23 17:32 84-74-203/08/23 15:03442 149 1
4,6-Dinitro-2-methylphenol ND ug/kg 03/09/23 17:32 534-52-103/08/23 15:03883 412 1
2,4-Dinitrophenol ND ug/kg 03/09/23 17:32 51-28-503/08/23 15:032210 1370 1
2,4-Dinitrotoluene ND ug/kg 03/09/23 17:32 121-14-203/08/23 15:03442 170 1
2,6-Dinitrotoluene ND ug/kg 03/09/23 17:32 606-20-203/08/23 15:03442 162 1
Di-n-octylphthalate ND ug/kg 03/09/23 17:32 117-84-003/08/23 15:03442 174 1
bis(2-Ethylhexyl)phthalate ND ug/kg 03/09/23 17:32 117-81-703/08/23 15:03442 171 1
Fluoranthene ND ug/kg 03/09/23 17:32 206-44-003/08/23 15:03442 151 1
Fluorene ND ug/kg 03/09/23 17:32 86-73-703/08/23 15:03442 155 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 17:32 87-68-303/08/23 15:03442 191 1
Hexachlorobenzene ND ug/kg 03/09/23 17:32 118-74-103/08/23 15:03442 173 1
Hexachlorocyclopentadiene ND ug/kg 03/09/23 17:32 77-47-403/08/23 15:03442 253 1
Hexachloroethane ND ug/kg 03/09/23 17:32 67-72-103/08/23 15:03442 169 1
Indeno(1,2,3-cd)pyrene ND ug/kg 03/09/23 17:32 193-39-503/08/23 15:03442 174 1
Isophorone ND ug/kg 03/09/23 17:32 78-59-103/08/23 15:03442 197 1
1-Methylnaphthalene ND ug/kg 03/09/23 17:32 90-12-003/08/23 15:03442 155 1
2-Methylnaphthalene ND ug/kg 03/09/23 17:32 91-57-603/08/23 15:03442 177 1
2-Methylphenol(o-Cresol)ND ug/kg 03/09/23 17:32 95-48-703/08/23 15:03442 181 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/09/23 17:32 15831-10-403/08/23 15:03442 178 1
Naphthalene ND ug/kg 03/09/23 17:32 91-20-303/08/23 15:03442 150 1
2-Nitroaniline ND ug/kg 03/09/23 17:32 88-74-403/08/23 15:032210 361 1
3-Nitroaniline ND ug/kg 03/09/23 17:32 99-09-203/08/23 15:032210 347 1
4-Nitroaniline ND ug/kg 03/09/23 17:32 100-01-603/08/23 15:03883 336 1
Nitrobenzene ND ug/kg 03/09/23 17:32 98-95-303/08/23 15:03442 205 1
2-Nitrophenol ND ug/kg 03/09/23 17:32 88-75-503/08/23 15:03442 191 1
4-Nitrophenol ND ug/kg 03/09/23 17:32 100-02-703/08/23 15:032210 854 1
N-Nitrosodimethylamine ND ug/kg 03/09/23 17:32 62-75-903/08/23 15:03442 149 1
N-Nitroso-di-n-propylamine ND ug/kg 03/09/23 17:32 621-64-703/08/23 15:03442 166 1
N-Nitrosodiphenylamine ND ug/kg 03/09/23 17:32 86-30-603/08/23 15:03442 157 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/09/23 17:32 108-60-103/08/23 15:03442 210 1
Pentachlorophenol ND ug/kg 03/09/23 17:32 87-86-503/08/23 15:03883 432 1
Phenanthrene ND ug/kg 03/09/23 17:32 85-01-803/08/23 15:03442 145 1
Phenol ND ug/kg 03/09/23 17:32 108-95-203/08/23 15:03442 197 1
Pyrene ND ug/kg 03/09/23 17:32 129-00-003/08/23 15:03442 179 1
Pyridine ND ug/kg 03/09/23 17:32 110-86-103/08/23 15:03442 139 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 17:32 120-82-103/08/23 15:03442 174 1
2,4,5-Trichlorophenol ND ug/kg 03/09/23 17:32 95-95-403/08/23 15:03442 202 1
2,4,6-Trichlorophenol ND ug/kg 03/09/23 17:32 88-06-203/08/23 15:03442 182 1
Surrogates
Nitrobenzene-d5 (S)46 %03/09/23 17:32 4165-60-003/08/23 15:0310-130 1
2-Fluorobiphenyl (S)45 %03/09/23 17:32 321-60-803/08/23 15:0310-130 1
Terphenyl-d14 (S)55 %03/09/23 17:32 1718-51-003/08/23 15:0310-130 1
Phenol-d6 (S)44 %03/09/23 17:32 13127-88-303/08/23 15:0310-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-02 (2-4)Lab ID: 92655679009 Collected: 03/07/23 18:10 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)42 %03/09/23 17:32 367-12-403/08/23 15:0310-130 1
2,4,6-Tribromophenol (S)57 %03/09/23 17:32 118-79-603/08/23 15:0310-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/09/23 23:34 67-64-103/09/23 16:59147 47.2 1
Benzene ND ug/kg 03/09/23 23:34 71-43-203/09/23 16:597.3 2.9 1
Bromobenzene ND ug/kg 03/09/23 23:34 108-86-103/09/23 16:597.3 2.4 1
Bromochloromethane ND ug/kg 03/09/23 23:34 74-97-503/09/23 16:597.3 2.2 1
Bromodichloromethane ND ug/kg 03/09/23 23:34 75-27-403/09/23 16:597.3 2.8 1
Bromoform ND ug/kg 03/09/23 23:34 75-25-203/09/23 16:597.3 2.6 1
Bromomethane ND ug/kg 03/09/23 23:34 74-83-9 v203/09/23 16:5929.4 22.8 1
2-Butanone (MEK)ND ug/kg 03/09/23 23:34 78-93-303/09/23 16:59147 35.3 1
n-Butylbenzene ND ug/kg 03/09/23 23:34 104-51-803/09/23 16:597.3 4.6 1
sec-Butylbenzene ND ug/kg 03/09/23 23:34 135-98-803/09/23 16:597.3 3.2 1
tert-Butylbenzene ND ug/kg 03/09/23 23:34 98-06-603/09/23 16:597.3 2.6 1
Carbon tetrachloride ND ug/kg 03/09/23 23:34 56-23-5 IK03/09/23 16:597.3 2.7 1
Chlorobenzene ND ug/kg 03/09/23 23:34 108-90-703/09/23 16:597.3 4.2 1
Chloroethane ND ug/kg 03/09/23 23:34 75-00-303/09/23 16:5914.7 5.7 1
Chloroform ND ug/kg 03/09/23 23:34 67-66-303/09/23 16:597.3 6.1 1
Chloromethane ND ug/kg 03/09/23 23:34 74-87-303/09/23 16:5914.7 6.2 1
2-Chlorotoluene ND ug/kg 03/09/23 23:34 95-49-803/09/23 16:597.3 2.6 1
4-Chlorotoluene ND ug/kg 03/09/23 23:34 106-43-403/09/23 16:597.3 4.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/09/23 23:34 96-12-803/09/23 16:597.3 2.9 1
Dibromochloromethane ND ug/kg 03/09/23 23:34 124-48-1 IK03/09/23 16:597.3 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 03/09/23 23:34 106-93-403/09/23 16:597.3 3.2 1
Dibromomethane ND ug/kg 03/09/23 23:34 74-95-303/09/23 16:597.3 1.6 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 23:34 95-50-103/09/23 16:597.3 2.6 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 23:34 541-73-103/09/23 16:597.3 2.3 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 23:34 106-46-703/09/23 16:597.3 1.9 1
Dichlorodifluoromethane ND ug/kg 03/09/23 23:34 75-71-803/09/23 16:5914.7 7.5 1
1,1-Dichloroethane ND ug/kg 03/09/23 23:34 75-34-303/09/23 16:597.3 3.0 1
1,2-Dichloroethane ND ug/kg 03/09/23 23:34 107-06-203/09/23 16:597.3 4.9 1
1,1-Dichloroethene ND ug/kg 03/09/23 23:34 75-35-403/09/23 16:597.3 3.0 1
cis-1,2-Dichloroethene ND ug/kg 03/09/23 23:34 156-59-203/09/23 16:597.3 2.5 1
trans-1,2-Dichloroethene ND ug/kg 03/09/23 23:34 156-60-503/09/23 16:597.3 6.2 1
1,2-Dichloropropane ND ug/kg 03/09/23 23:34 78-87-503/09/23 16:597.3 2.2 1
1,3-Dichloropropane ND ug/kg 03/09/23 23:34 142-28-903/09/23 16:597.3 2.3 1
2,2-Dichloropropane ND ug/kg 03/09/23 23:34 594-20-703/09/23 16:597.3 5.6 1
1,1-Dichloropropene ND ug/kg 03/09/23 23:34 563-58-603/09/23 16:597.3 3.5 1
cis-1,3-Dichloropropene ND ug/kg 03/09/23 23:34 10061-01-503/09/23 16:597.3 2.0 1
trans-1,3-Dichloropropene ND ug/kg 03/09/23 23:34 10061-02-603/09/23 16:597.3 2.5 1
Diisopropyl ether ND ug/kg 03/09/23 23:34 108-20-303/09/23 16:597.3 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-02 (2-4)Lab ID: 92655679009 Collected: 03/07/23 18:10 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 03/09/23 23:34 100-41-403/09/23 16:597.3 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 23:34 87-68-303/09/23 16:5914.7 12.0 1
2-Hexanone ND ug/kg 03/09/23 23:34 591-78-603/09/23 16:5973.5 7.1 1
Isopropylbenzene (Cumene)ND ug/kg 03/09/23 23:34 98-82-803/09/23 16:597.3 2.5 1
p-Isopropyltoluene ND ug/kg 03/09/23 23:34 99-87-603/09/23 16:597.3 3.6 1
Methylene Chloride ND ug/kg 03/09/23 23:34 75-09-203/09/23 16:5929.4 20.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/09/23 23:34 108-10-103/09/23 16:5973.5 7.1 1
Methyl-tert-butyl ether ND ug/kg 03/09/23 23:34 1634-04-403/09/23 16:597.3 2.7 1
Naphthalene ND ug/kg 03/09/23 23:34 91-20-303/09/23 16:597.3 3.9 1
n-Propylbenzene ND ug/kg 03/09/23 23:34 103-65-103/09/23 16:597.3 2.6 1
Styrene ND ug/kg 03/09/23 23:34 100-42-5 IK03/09/23 16:597.3 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/09/23 23:34 630-20-603/09/23 16:597.3 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/09/23 23:34 79-34-503/09/23 16:597.3 1.9 1
Tetrachloroethene ND ug/kg 03/09/23 23:34 127-18-403/09/23 16:597.3 2.3 1
Toluene ND ug/kg 03/09/23 23:34 108-88-303/09/23 16:597.3 5.1 1
1,2,3-Trichlorobenzene ND ug/kg 03/09/23 23:34 87-61-603/09/23 16:597.3 5.9 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 23:34 120-82-103/09/23 16:597.3 6.2 1
1,1,1-Trichloroethane ND ug/kg 03/09/23 23:34 71-55-603/09/23 16:597.3 3.8 1
1,1,2-Trichloroethane ND ug/kg 03/09/23 23:34 79-00-503/09/23 16:597.3 2.4 1
Trichloroethene ND ug/kg 03/09/23 23:34 79-01-603/09/23 16:597.3 5.9 1
Trichlorofluoromethane ND ug/kg 03/09/23 23:34 75-69-403/09/23 16:597.3 4.0 1
1,2,3-Trichloropropane ND ug/kg 03/09/23 23:34 96-18-403/09/23 16:597.3 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/09/23 23:34 95-63-603/09/23 16:597.3 4.4 1
1,3,5-Trimethylbenzene ND ug/kg 03/09/23 23:34 108-67-803/09/23 16:597.3 2.5 1
Vinyl acetate ND ug/kg 03/09/23 23:34 108-05-403/09/23 16:5973.5 15.1 1
Vinyl chloride ND ug/kg 03/09/23 23:34 75-01-403/09/23 16:5914.7 3.7 1
Xylene (Total)ND ug/kg 03/09/23 23:34 1330-20-703/09/23 16:5914.7 4.2 1
m&p-Xylene ND ug/kg 03/09/23 23:34 179601-23-103/09/23 16:5914.7 5.0 1
o-Xylene ND ug/kg 03/09/23 23:34 95-47-603/09/23 16:597.3 3.2 1
Surrogates
Toluene-d8 (S)101 %03/09/23 23:34 2037-26-503/09/23 16:5970-130 1
4-Bromofluorobenzene (S)109 %03/09/23 23:34 460-00-403/09/23 16:5970-130 1
1,2-Dichloroethane-d4 (S)108 %03/09/23 23:34 17060-07-003/09/23 16:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.3 %03/08/23 17:05 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 76.6 %03/13/23 15:2803/13/23 15:211
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Sample: BF-SB-02 (2-4)Lab ID: 92655679009 Collected: 03/07/23 18:10 Received: 03/08/23 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.719J mg/kg 03/14/23 16:17 18540-29-9 J03/14/23 01:161.31 0.333 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
870786
EPA 7471B
EPA 7471B
7471B Mercury Solids
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92655679001, 92655679002, 92655679003, 92655679004, 92655679005, 92655679006, 92655679007,
92655679008, 92655679009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4592679
Associated Lab Samples: 92655679001, 92655679002, 92655679003, 92655679004, 92655679005, 92655679006, 92655679007,
92655679008, 92655679009
Matrix: Solid
AnalyzedMDL
Mercury mg/kg ND 0.019 03/14/23 11:300.0083
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4592680LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.470.45 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4592681MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655679001
4592682
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.565 100 80-120101 7 200.6050.073 0.64 0.69
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
870782
EPA 3050B
EPA 6020B
6020B Solids UPD5
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92655679001, 92655679002, 92655679003, 92655679004, 92655679005, 92655679006, 92655679007,
92655679008, 92655679009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4592655
Associated Lab Samples: 92655679001, 92655679002, 92655679003, 92655679004, 92655679005, 92655679006, 92655679007,
92655679008, 92655679009
Matrix: Solid
AnalyzedMDL
Arsenic mg/kg ND 0.48 03/14/23 16:010.14
Barium mg/kg ND 0.29 03/14/23 16:010.072
Cadmium mg/kg ND 0.077 03/14/23 16:010.028
Chromium mg/kg ND 1.9 03/14/23 16:010.37
Lead mg/kg ND 0.48 03/14/23 16:010.090
Selenium mg/kg ND 0.48 03/14/23 16:010.10
Silver mg/kg ND 0.48 03/14/23 16:010.20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4592656LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 42.047.1 89 80-120
Barium mg/kg 42.947.1 91 80-120
Cadmium mg/kg 42.047.1 89 80-120
Chromium mg/kg 45.547.1 97 80-120
Lead mg/kg 43.347.1 92 80-120
Selenium mg/kg 42.947.1 91 80-120
Silver mg/kg 21.923.5 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4592657MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655679001
4592658
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 65.7 92 75-12592 3 2064.32.6 63.1 61.5
Barium mg/kg 65.7 108 75-125105 3 2064.351.0 122 118
Cadmium mg/kg 65.7 97 75-12598 1 2064.30.038J 63.8 63.3
Chromium mg/kg 65.7 94 75-125120 14 2064.339.0 101 116
Lead mg/kg 65.7 101 75-125102 1 2064.38.6 74.8 74.0
Selenium mg/kg 65.7 94 75-12594 2 2064.30.66 62.6 61.3
Silver mg/kg 32.9 99 75-125101 1 2032.2ND 32.6 32.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
870730
ASTM D2974
ASTM D2974
Dry Weight / %M by ASTM D2974
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples: 92655679005, 92655679006
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655679005
4592426SAMPLE DUPLICATE:
Percent Moisture %24.1 N203024.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760303
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92655679001, 92655679002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3949131
Associated Lab Samples:92655679001, 92655679002
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 03/09/23 15:311.9
1,1,1-Trichloroethane ug/kg ND 5.0 03/09/23 15:312.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 03/09/23 15:311.3
1,1,2-Trichloroethane ug/kg ND 5.0 03/09/23 15:311.7
1,1-Dichloroethane ug/kg ND 5.0 03/09/23 15:312.1
1,1-Dichloroethene ug/kg ND 5.0 03/09/23 15:312.1
1,1-Dichloropropene ug/kg ND 5.0 03/09/23 15:312.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 03/09/23 15:314.0
1,2,3-Trichloropropane ug/kg ND 5.0 v103/09/23 15:312.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 03/09/23 15:314.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 03/09/23 15:313.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/09/23 15:311.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 03/09/23 15:312.2
1,2-Dichlorobenzene ug/kg ND 5.0 03/09/23 15:311.8
1,2-Dichloroethane ug/kg ND 5.0 03/09/23 15:313.3
1,2-Dichloropropane ug/kg ND 5.0 03/09/23 15:311.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 03/09/23 15:311.7
1,3-Dichlorobenzene ug/kg ND 5.0 03/09/23 15:311.6
1,3-Dichloropropane ug/kg ND 5.0 03/09/23 15:311.6
1,4-Dichlorobenzene ug/kg ND 5.0 03/09/23 15:311.3
2,2-Dichloropropane ug/kg ND 5.0 03/09/23 15:313.8
2-Butanone (MEK)ug/kg ND 100 v103/09/23 15:3124.0
2-Chlorotoluene ug/kg ND 5.0 03/09/23 15:311.8
2-Hexanone ug/kg ND 50.0 v103/09/23 15:314.8
4-Chlorotoluene ug/kg ND 5.0 03/09/23 15:312.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 v103/09/23 15:314.8
Acetone ug/kg ND 100 03/09/23 15:3132.1
Benzene ug/kg ND 5.0 03/09/23 15:312.0
Bromobenzene ug/kg ND 5.0 03/09/23 15:311.6
Bromochloromethane ug/kg ND 5.0 03/09/23 15:311.5
Bromodichloromethane ug/kg ND 5.0 03/09/23 15:311.9
Bromoform ug/kg ND 5.0 03/09/23 15:311.8
Bromomethane ug/kg ND 20.0 03/09/23 15:3115.5
Carbon tetrachloride ug/kg ND 5.0 03/09/23 15:311.9
Chlorobenzene ug/kg ND 5.0 03/09/23 15:312.9
Chloroethane ug/kg ND 10.0 03/09/23 15:313.9
Chloroform ug/kg ND 5.0 03/09/23 15:314.2
Chloromethane ug/kg ND 10.0 03/09/23 15:314.2
cis-1,2-Dichloroethene ug/kg ND 5.0 03/09/23 15:311.7
cis-1,3-Dichloropropene ug/kg ND 5.0 03/09/23 15:311.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3949131
Associated Lab Samples:92655679001, 92655679002
Matrix: Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 03/09/23 15:312.8
Dibromomethane ug/kg ND 5.0 03/09/23 15:311.1
Dichlorodifluoromethane ug/kg ND 10.0 03/09/23 15:315.1
Diisopropyl ether ug/kg ND 5.0 03/09/23 15:311.4
Ethylbenzene ug/kg ND 5.0 03/09/23 15:312.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 03/09/23 15:318.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 03/09/23 15:311.7
m&p-Xylene ug/kg ND 10.0 03/09/23 15:313.4
Methyl-tert-butyl ether ug/kg ND 5.0 03/09/23 15:311.9
Methylene Chloride ug/kg ND 20.0 03/09/23 15:3113.7
n-Butylbenzene ug/kg ND 5.0 03/09/23 15:313.2
n-Propylbenzene ug/kg ND 5.0 03/09/23 15:311.8
Naphthalene ug/kg ND 5.0 03/09/23 15:312.6
o-Xylene ug/kg ND 5.0 03/09/23 15:312.2
p-Isopropyltoluene ug/kg ND 5.0 03/09/23 15:312.5
sec-Butylbenzene ug/kg ND 5.0 03/09/23 15:312.2
Styrene ug/kg ND 5.0 03/09/23 15:311.3
tert-Butylbenzene ug/kg ND 5.0 03/09/23 15:311.8
Tetrachloroethene ug/kg ND 5.0 03/09/23 15:311.6
Toluene ug/kg ND 5.0 03/09/23 15:313.4
trans-1,2-Dichloroethene ug/kg ND 5.0 03/09/23 15:314.2
trans-1,3-Dichloropropene ug/kg ND 5.0 03/09/23 15:311.7
Trichloroethene ug/kg ND 5.0 03/09/23 15:314.0
Trichlorofluoromethane ug/kg ND 5.0 03/09/23 15:312.8
Vinyl acetate ug/kg ND 50.0 03/09/23 15:3110.3
Vinyl chloride ug/kg ND 10.0 03/09/23 15:312.5
Xylene (Total)ug/kg ND 10.0 03/09/23 15:312.8
1,2-Dichloroethane-d4 (S)%115 70-130 03/09/23 15:31
4-Bromofluorobenzene (S)%100 70-130 03/09/23 15:31
Toluene-d8 (S)%100 70-130 03/09/23 15:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3949132LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 465500 93 70-130
1,1,1-Trichloroethane ug/kg 437500 87 70-130
1,1,2,2-Tetrachloroethane ug/kg 524500 105 70-130
1,1,2-Trichloroethane ug/kg 484500 97 70-130
1,1-Dichloroethane ug/kg 458500 92 70-130
1,1-Dichloroethene ug/kg 506500 101 70-130
1,1-Dichloropropene ug/kg 494500 99 70-130
1,2,3-Trichlorobenzene ug/kg 472500 94 70-130
1,2,3-Trichloropropane ug/kg 592 v1500118 70-130
1,2,4-Trichlorobenzene ug/kg 466500 93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3949132LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 508500 102 70-130
1,2-Dibromo-3-chloropropane ug/kg 470500 94 67-130
1,2-Dibromoethane (EDB)ug/kg 488500 98 70-130
1,2-Dichlorobenzene ug/kg 494500 99 70-130
1,2-Dichloroethane ug/kg 499500 100 70-130
1,2-Dichloropropane ug/kg 482500 96 70-130
1,3,5-Trimethylbenzene ug/kg 521500 104 70-130
1,3-Dichlorobenzene ug/kg 498500 100 70-130
1,3-Dichloropropane ug/kg 506500 101 70-130
1,4-Dichlorobenzene ug/kg 467500 93 70-130
2,2-Dichloropropane ug/kg 396500 79 67-130
2-Butanone (MEK)ug/kg 1160 v11000116 66-130
2-Chlorotoluene ug/kg 507500 101 70-130
2-Hexanone ug/kg 1410 L1,v11000141 70-130
4-Chlorotoluene ug/kg 497500 99 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 1250 v11000125 70-130
Acetone ug/kg 10801000 108 67-130
Benzene ug/kg 441500 88 70-130
Bromobenzene ug/kg 497500 99 70-130
Bromochloromethane ug/kg 436500 87 70-130
Bromodichloromethane ug/kg 456500 91 70-130
Bromoform ug/kg 478500 96 70-130
Bromomethane ug/kg 468500 94 53-175
Carbon tetrachloride ug/kg 448500 90 70-130
Chlorobenzene ug/kg 493500 99 70-130
Chloroethane ug/kg 507500 101 70-135
Chloroform ug/kg 434500 87 70-130
Chloromethane ug/kg 513500 103 64-130
cis-1,2-Dichloroethene ug/kg 492500 98 70-130
cis-1,3-Dichloropropene ug/kg 469500 94 70-130
Dibromochloromethane ug/kg 461500 92 70-130
Dibromomethane ug/kg 461500 92 70-130
Dichlorodifluoromethane ug/kg 483500 97 63-145
Diisopropyl ether ug/kg 458500 92 68-130
Ethylbenzene ug/kg 487500 97 70-130
Hexachloro-1,3-butadiene ug/kg 459500 92 70-130
Isopropylbenzene (Cumene)ug/kg 509500 102 70-130
m&p-Xylene ug/kg 10401000 104 70-130
Methyl-tert-butyl ether ug/kg 438500 88 70-130
Methylene Chloride ug/kg 424500 85 67-130
n-Butylbenzene ug/kg 520500 104 70-130
n-Propylbenzene ug/kg 517500 103 70-130
Naphthalene ug/kg 556500 111 70-130
o-Xylene ug/kg 488500 98 70-130
p-Isopropyltoluene ug/kg 512500 102 70-130
sec-Butylbenzene ug/kg 525500 105 70-130
Styrene ug/kg 493500 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3949132LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 495500 99 64-130
Tetrachloroethene ug/kg 512500 102 70-130
Toluene ug/kg 465500 93 70-130
trans-1,2-Dichloroethene ug/kg 470500 94 70-130
trans-1,3-Dichloropropene ug/kg 475500 95 70-130
Trichloroethene ug/kg 455500 91 70-130
Trichlorofluoromethane ug/kg 471500 94 70-130
Vinyl acetate ug/kg 10601000 106 70-134
Vinyl chloride ug/kg 500500 100 68-130
Xylene (Total)ug/kg 15301500 102 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3949133MATRIX SPIKE SAMPLE:
MSSpike
Result
92655679001
1,1,1,2-Tetrachloroethane ug/kg 814807 101 58-140ND
1,1,1-Trichloroethane ug/kg 856807 106 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 968807 120 52-139ND
1,1,2-Trichloroethane ug/kg 831807 103 56-140ND
1,1-Dichloroethane ug/kg 856807 106 58-145ND
1,1-Dichloroethene ug/kg 1040807 129 57-158ND
1,1-Dichloropropene ug/kg 982807 122 58-151ND
1,2,3-Trichlorobenzene ug/kg 550807 68 48-149ND
1,2,3-Trichloropropane ug/kg 1060 v1807131 54-132ND
1,2,4-Trichlorobenzene ug/kg 678807 84 51-151ND
1,2,4-Trimethylbenzene ug/kg 897807 111 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 716807 89 44-134ND
1,2-Dibromoethane (EDB)ug/kg 881807 109 60-138ND
1,2-Dichlorobenzene ug/kg 866807 107 59-147ND
1,2-Dichloroethane ug/kg 902807 112 57-139ND
1,2-Dichloropropane ug/kg 870807 108 62-145ND
1,3,5-Trimethylbenzene ug/kg 921807 114 47-159ND
1,3-Dichlorobenzene ug/kg 876807 109 58-144ND
1,3-Dichloropropane ug/kg 906807 112 60-142ND
1,4-Dichlorobenzene ug/kg 847807 105 57-143ND
2,2-Dichloropropane ug/kg 715807 89 37-144ND
2-Butanone (MEK)ug/kg 2180 v11620135 28-146ND
2-Chlorotoluene ug/kg 908807 113 55-158ND
2-Hexanone ug/kg 2370 M0,v11620147 44-141ND
4-Chlorotoluene ug/kg 865807 107 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 2230 v11620138 50-138ND
Acetone ug/kg 18201620 113 20-136ND
Benzene ug/kg 839807 104 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3949133MATRIX SPIKE SAMPLE:
MSSpike
Result
92655679001
Bromobenzene ug/kg 858807 106 59-145ND
Bromochloromethane ug/kg 799807 99 57-143ND
Bromodichloromethane ug/kg 802807 99 53-133ND
Bromoform ug/kg 803807 100 48-133ND
Bromomethane ug/kg 560807 69 10-167ND
Carbon tetrachloride ug/kg 821807 102 57-147ND
Chlorobenzene ug/kg 908807 112 61-144ND
Chloroethane ug/kg 422807 52 10-153ND
Chloroform ug/kg 774807 96 58-141ND
Chloromethane ug/kg 1010807 126 54-165ND
cis-1,2-Dichloroethene ug/kg 936807 116 59-144ND
cis-1,3-Dichloropropene ug/kg 801807 99 56-137ND
Dibromochloromethane ug/kg 792807 98 53-139ND
Dibromomethane ug/kg 792807 98 60-136ND
Dichlorodifluoromethane ug/kg 1010807 125 49-177ND
Diisopropyl ether ug/kg 868807 108 53-136ND
Ethylbenzene ug/kg 910807 113 53-150ND
Hexachloro-1,3-butadiene ug/kg 812807 101 42-186ND
Isopropylbenzene (Cumene)ug/kg 956807 119 62-154ND
m&p-Xylene ug/kg 19101620 118 49-156ND
Methyl-tert-butyl ether ug/kg 806807 100 54-133ND
Methylene Chloride ug/kg 838807 104 50-153ND
n-Butylbenzene ug/kg 939807 116 44-174ND
n-Propylbenzene ug/kg 941807 117 52-157ND
Naphthalene ug/kg 641807 79 37-150ND
o-Xylene ug/kg 896807 111 54-150ND
p-Isopropyltoluene ug/kg 930807 115 50-164ND
sec-Butylbenzene ug/kg 965807 120 58-161ND
Styrene ug/kg 911807 113 60-148ND
tert-Butylbenzene ug/kg 912807 113 44-151ND
Tetrachloroethene ug/kg 875807 108 53-151ND
Toluene ug/kg 870807 108 52-148ND
trans-1,2-Dichloroethene ug/kg 925807 115 60-148ND
trans-1,3-Dichloropropene ug/kg 821807 102 55-133ND
Trichloroethene ug/kg 829807 103 60-148ND
Trichlorofluoromethane ug/kg 559807 69 10-154ND
Vinyl acetate ug/kg 15001620 93 50-149ND
Vinyl chloride ug/kg 1010807 125 57-157ND
Xylene (Total)ug/kg 28102420 116 52-153ND
1,2-Dichloroethane-d4 (S)%112 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655679002
3949134SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND v130ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND v130ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND v130ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND v130ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655679002
3949134SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg 14.3 18 3011.9
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%111111
4-Bromofluorobenzene (S)%105101
Toluene-d8 (S)%101100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760513
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92655679003, 92655679004, 92655679007, 92655679008, 92655679009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3950509
Associated Lab Samples:92655679003, 92655679004, 92655679007, 92655679008, 92655679009
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 03/09/23 18:551.9
1,1,1-Trichloroethane ug/kg ND 5.0 03/09/23 18:552.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 03/09/23 18:551.3
1,1,2-Trichloroethane ug/kg ND 5.0 03/09/23 18:551.7
1,1-Dichloroethane ug/kg ND 5.0 03/09/23 18:552.1
1,1-Dichloroethene ug/kg ND 5.0 03/09/23 18:552.1
1,1-Dichloropropene ug/kg ND 5.0 03/09/23 18:552.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 03/09/23 18:554.0
1,2,3-Trichloropropane ug/kg ND 5.0 03/09/23 18:552.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 03/09/23 18:554.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 03/09/23 18:553.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/09/23 18:551.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 03/09/23 18:552.2
1,2-Dichlorobenzene ug/kg ND 5.0 03/09/23 18:551.8
1,2-Dichloroethane ug/kg ND 5.0 03/09/23 18:553.3
1,2-Dichloropropane ug/kg ND 5.0 03/09/23 18:551.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 03/09/23 18:551.7
1,3-Dichlorobenzene ug/kg ND 5.0 03/09/23 18:551.6
1,3-Dichloropropane ug/kg ND 5.0 03/09/23 18:551.6
1,4-Dichlorobenzene ug/kg ND 5.0 03/09/23 18:551.3
2,2-Dichloropropane ug/kg ND 5.0 03/09/23 18:553.8
2-Butanone (MEK)ug/kg ND 100 03/09/23 18:5524.0
2-Chlorotoluene ug/kg ND 5.0 03/09/23 18:551.8
2-Hexanone ug/kg ND 50.0 03/09/23 18:554.8
4-Chlorotoluene ug/kg ND 5.0 03/09/23 18:552.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 03/09/23 18:554.8
Acetone ug/kg ND 100 03/09/23 18:5532.1
Benzene ug/kg ND 5.0 03/09/23 18:552.0
Bromobenzene ug/kg ND 5.0 03/09/23 18:551.6
Bromochloromethane ug/kg ND 5.0 03/09/23 18:551.5
Bromodichloromethane ug/kg ND 5.0 03/09/23 18:551.9
Bromoform ug/kg ND 5.0 03/09/23 18:551.8
Bromomethane ug/kg ND 20.0 v203/09/23 18:5515.5
Carbon tetrachloride ug/kg ND 5.0 IK03/09/23 18:551.9
Chlorobenzene ug/kg ND 5.0 03/09/23 18:552.9
Chloroethane ug/kg ND 10.0 03/09/23 18:553.9
Chloroform ug/kg ND 5.0 03/09/23 18:554.2
Chloromethane ug/kg ND 10.0 03/09/23 18:554.2
cis-1,2-Dichloroethene ug/kg ND 5.0 03/09/23 18:551.7
cis-1,3-Dichloropropene ug/kg ND 5.0 03/09/23 18:551.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3950509
Associated Lab Samples:92655679003, 92655679004, 92655679007, 92655679008, 92655679009
Matrix: Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 IK03/09/23 18:552.8
Dibromomethane ug/kg ND 5.0 03/09/23 18:551.1
Dichlorodifluoromethane ug/kg ND 10.0 03/09/23 18:555.1
Diisopropyl ether ug/kg ND 5.0 03/09/23 18:551.4
Ethylbenzene ug/kg ND 5.0 03/09/23 18:552.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 03/09/23 18:558.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 03/09/23 18:551.7
m&p-Xylene ug/kg ND 10.0 03/09/23 18:553.4
Methyl-tert-butyl ether ug/kg ND 5.0 03/09/23 18:551.9
Methylene Chloride ug/kg ND 20.0 03/09/23 18:5513.7
n-Butylbenzene ug/kg ND 5.0 03/09/23 18:553.2
n-Propylbenzene ug/kg ND 5.0 03/09/23 18:551.8
Naphthalene ug/kg ND 5.0 03/09/23 18:552.6
o-Xylene ug/kg ND 5.0 03/09/23 18:552.2
p-Isopropyltoluene ug/kg ND 5.0 03/09/23 18:552.5
sec-Butylbenzene ug/kg ND 5.0 03/09/23 18:552.2
Styrene ug/kg ND 5.0 IK03/09/23 18:551.3
tert-Butylbenzene ug/kg ND 5.0 03/09/23 18:551.8
Tetrachloroethene ug/kg ND 5.0 03/09/23 18:551.6
Toluene ug/kg ND 5.0 03/09/23 18:553.4
trans-1,2-Dichloroethene ug/kg ND 5.0 03/09/23 18:554.2
trans-1,3-Dichloropropene ug/kg ND 5.0 03/09/23 18:551.7
Trichloroethene ug/kg ND 5.0 03/09/23 18:554.0
Trichlorofluoromethane ug/kg ND 5.0 03/09/23 18:552.8
Vinyl acetate ug/kg ND 50.0 03/09/23 18:5510.3
Vinyl chloride ug/kg ND 10.0 03/09/23 18:552.5
Xylene (Total)ug/kg ND 10.0 03/09/23 18:552.8
1,2-Dichloroethane-d4 (S)%102 70-130 03/09/23 18:55
4-Bromofluorobenzene (S)%98 70-130 03/09/23 18:55
Toluene-d8 (S)%97 70-130 03/09/23 18:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3950510LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 465500 93 70-130
1,1,1-Trichloroethane ug/kg 500500 100 70-130
1,1,2,2-Tetrachloroethane ug/kg 491500 98 70-130
1,1,2-Trichloroethane ug/kg 446500 89 70-130
1,1-Dichloroethane ug/kg 469500 94 70-130
1,1-Dichloroethene ug/kg 464500 93 70-130
1,1-Dichloropropene ug/kg 565500 113 70-130
1,2,3-Trichlorobenzene ug/kg 497500 99 70-130
1,2,3-Trichloropropane ug/kg 484500 97 70-130
1,2,4-Trichlorobenzene ug/kg 548500 110 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3950510LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 522500 104 70-130
1,2-Dibromo-3-chloropropane ug/kg 512500 102 67-130
1,2-Dibromoethane (EDB)ug/kg 503500 101 70-130
1,2-Dichlorobenzene ug/kg 526500 105 70-130
1,2-Dichloroethane ug/kg 438500 88 70-130
1,2-Dichloropropane ug/kg 431500 86 70-130
1,3,5-Trimethylbenzene ug/kg 550500 110 70-130
1,3-Dichlorobenzene ug/kg 503500 101 70-130
1,3-Dichloropropane ug/kg 484500 97 70-130
1,4-Dichlorobenzene ug/kg 478500 96 70-130
2,2-Dichloropropane ug/kg 469500 94 67-130
2-Butanone (MEK)ug/kg 8481000 85 66-130
2-Chlorotoluene ug/kg 525500 105 70-130
2-Hexanone ug/kg 8501000 85 70-130
4-Chlorotoluene ug/kg 531500 106 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 8171000 82 70-130
Acetone ug/kg 8051000 80 67-130
Benzene ug/kg 427500 85 70-130
Bromobenzene ug/kg 505500 101 70-130
Bromochloromethane ug/kg 530500 106 70-130
Bromodichloromethane ug/kg 471500 94 70-130
Bromoform ug/kg 489500 98 70-130
Bromomethane ug/kg 322 v350064 53-175
Carbon tetrachloride ug/kg 431 IK50086 70-130
Chlorobenzene ug/kg 488500 98 70-130
Chloroethane ug/kg 431500 86 70-135
Chloroform ug/kg 477500 95 70-130
Chloromethane ug/kg 479500 96 64-130
cis-1,2-Dichloroethene ug/kg 479500 96 70-130
cis-1,3-Dichloropropene ug/kg 477500 95 70-130
Dibromochloromethane ug/kg 453 IK50091 70-130
Dibromomethane ug/kg 441500 88 70-130
Dichlorodifluoromethane ug/kg 522500 104 63-145
Diisopropyl ether ug/kg 434500 87 68-130
Ethylbenzene ug/kg 477500 95 70-130
Hexachloro-1,3-butadiene ug/kg 579500 116 70-130
Isopropylbenzene (Cumene)ug/kg 506500 101 70-130
m&p-Xylene ug/kg 9761000 98 70-130
Methyl-tert-butyl ether ug/kg 443500 89 70-130
Methylene Chloride ug/kg 456500 91 67-130
n-Butylbenzene ug/kg 563500 113 70-130
n-Propylbenzene ug/kg 506500 101 70-130
Naphthalene ug/kg 539500 108 70-130
o-Xylene ug/kg 529500 106 70-130
p-Isopropyltoluene ug/kg 575500 115 70-130
sec-Butylbenzene ug/kg 554500 111 70-130
Styrene ug/kg 544 IK500109 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3950510LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 541500 108 64-130
Tetrachloroethene ug/kg 526500 105 70-130
Toluene ug/kg 456500 91 70-130
trans-1,2-Dichloroethene ug/kg 471500 94 70-130
trans-1,3-Dichloropropene ug/kg 457500 91 70-130
Trichloroethene ug/kg 483500 97 70-130
Trichlorofluoromethane ug/kg 457500 91 70-130
Vinyl acetate ug/kg 9211000 92 70-134
Vinyl chloride ug/kg 437500 87 68-130
Xylene (Total)ug/kg 15001500 100 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3950511MATRIX SPIKE SAMPLE:
MSSpike
Result
92655785001
1,1,1,2-Tetrachloroethane ug/kg 723726 100 58-140ND
1,1,1-Trichloroethane ug/kg 873726 120 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 817726 113 52-139ND
1,1,2-Trichloroethane ug/kg 749726 103 56-140ND
1,1-Dichloroethane ug/kg 834726 115 58-145ND
1,1-Dichloroethene ug/kg 1200 M1726166 57-158ND
1,1-Dichloropropene ug/kg 975726 134 58-151ND
1,2,3-Trichlorobenzene ug/kg 142 M172620 48-149ND
1,2,3-Trichloropropane ug/kg 811726 112 54-132ND
1,2,4-Trichlorobenzene ug/kg 315 M172643 51-151ND
1,2,4-Trimethylbenzene ug/kg 868726 120 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 323726 44 44-134ND
1,2-Dibromoethane (EDB)ug/kg 825726 114 60-138ND
1,2-Dichlorobenzene ug/kg 819726 113 59-147ND
1,2-Dichloroethane ug/kg 787726 109 57-139ND
1,2-Dichloropropane ug/kg 781726 108 62-145ND
1,3,5-Trimethylbenzene ug/kg 891726 123 47-159ND
1,3-Dichlorobenzene ug/kg 814726 112 58-144ND
1,3-Dichloropropane ug/kg 828726 114 60-142ND
1,4-Dichlorobenzene ug/kg 743726 102 57-143ND
2,2-Dichloropropane ug/kg 789726 109 37-144ND
2-Butanone (MEK)ug/kg 16301460 112 28-146ND
2-Chlorotoluene ug/kg 879726 121 55-158ND
2-Hexanone ug/kg 541 M1146037 44-141ND
4-Chlorotoluene ug/kg 847726 117 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 16301460 108 50-138ND
Acetone ug/kg 15101460 100 20-136ND
Benzene ug/kg 749726 103 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3950511MATRIX SPIKE SAMPLE:
MSSpike
Result
92655785001
Bromobenzene ug/kg 798726 110 59-145ND
Bromochloromethane ug/kg 856726 118 57-143ND
Bromodichloromethane ug/kg 767726 106 53-133ND
Bromoform ug/kg 743726 102 48-133ND
Bromomethane ug/kg 726 v372657 10-167312
Carbon tetrachloride ug/kg 529 IK72673 57-147ND
Chlorobenzene ug/kg 762726 105 61-144ND
Chloroethane ug/kg 461726 64 10-153ND
Chloroform ug/kg 848726 117 58-141ND
Chloromethane ug/kg 73400 E,M1726-1330 54-16583000
cis-1,2-Dichloroethene ug/kg 905726 125 59-144ND
cis-1,3-Dichloropropene ug/kg 790726 109 56-137ND
Dibromochloromethane ug/kg 709 IK72698 53-139ND
Dibromomethane ug/kg 728726 100 60-136ND
Dichlorodifluoromethane ug/kg 1020726 141 49-177ND
Diisopropyl ether ug/kg 823726 114 53-136ND
Ethylbenzene ug/kg 737726 102 53-150ND
Hexachloro-1,3-butadiene ug/kg 942726 130 42-186ND
Isopropylbenzene (Cumene)ug/kg 827726 114 62-154ND
m&p-Xylene ug/kg 15501460 107 49-156ND
Methyl-tert-butyl ether ug/kg 831726 115 54-133ND
Methylene Chloride ug/kg 877726 121 50-153ND
n-Butylbenzene ug/kg 986726 136 44-174ND
n-Propylbenzene ug/kg 853726 118 52-157ND
Naphthalene ug/kg 113 M172616 37-150ND
o-Xylene ug/kg 782726 107 54-150ND
p-Isopropyltoluene ug/kg 988726 136 50-164ND
sec-Butylbenzene ug/kg 959726 132 58-161ND
Styrene ug/kg 827 IK726113 60-148ND
tert-Butylbenzene ug/kg 895726 123 44-151ND
Tetrachloroethene ug/kg 722726 100 53-151ND
Toluene ug/kg 730726 101 52-148ND
trans-1,2-Dichloroethene ug/kg 889726 123 60-148ND
trans-1,3-Dichloropropene ug/kg 761726 105 55-133ND
Trichloroethene ug/kg 786726 108 60-148ND
Trichlorofluoromethane ug/kg 597726 82 10-154ND
Vinyl acetate ug/kg 16501460 114 50-149ND
Vinyl chloride ug/kg 765726 105 57-157ND
Xylene (Total)ug/kg 23302180 107 52-153ND
1,2-Dichloroethane-d4 (S)%116 70-130
4-Bromofluorobenzene (S)%113 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655785005
3950512SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND v230ND
Carbon tetrachloride ug/kg ND IK30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg 16.7 C8,D6843040.7
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND IK30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655785005
3950512SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND IK30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%101101
4-Bromofluorobenzene (S)%108104
Toluene-d8 (S)%9998
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760193
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92655679001, 92655679002, 92655679003, 92655679004, 92655679007, 92655679008, 92655679009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3948387
Associated Lab Samples:92655679001, 92655679002, 92655679003, 92655679004, 92655679007, 92655679008, 92655679009
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 329 03/09/23 08:48130
1,2-Dichlorobenzene ug/kg ND 329 03/09/23 08:48119
1,3-Dichlorobenzene ug/kg ND 329 03/09/23 08:48117
1,4-Dichlorobenzene ug/kg ND 329 03/09/23 08:48126
1-Methylnaphthalene ug/kg ND 329 03/09/23 08:48116
2,2'-Oxybis(1-chloropropane)ug/kg ND 329 03/09/23 08:48156
2,4,5-Trichlorophenol ug/kg ND 329 03/09/23 08:48150
2,4,6-Trichlorophenol ug/kg ND 329 03/09/23 08:48136
2,4-Dichlorophenol ug/kg ND 329 03/09/23 08:48129
2,4-Dimethylphenol ug/kg ND 329 03/09/23 08:48137
2,4-Dinitrophenol ug/kg ND 1640 03/09/23 08:481020
2,4-Dinitrotoluene ug/kg ND 329 03/09/23 08:48127
2,6-Dinitrotoluene ug/kg ND 329 03/09/23 08:48121
2-Chloronaphthalene ug/kg ND 329 03/09/23 08:48131
2-Chlorophenol ug/kg ND 329 03/09/23 08:48124
2-Methylnaphthalene ug/kg ND 329 03/09/23 08:48132
2-Methylphenol(o-Cresol)ug/kg ND 329 03/09/23 08:48135
2-Nitroaniline ug/kg ND 1640 03/09/23 08:48269
2-Nitrophenol ug/kg ND 329 03/09/23 08:48143
3&4-Methylphenol(m&p Cresol)ug/kg ND 329 03/09/23 08:48133
3,3'-Dichlorobenzidine ug/kg ND 658 03/09/23 08:48222
3-Nitroaniline ug/kg ND 1640 03/09/23 08:48258
4,6-Dinitro-2-methylphenol ug/kg ND 658 03/09/23 08:48307
4-Bromophenylphenyl ether ug/kg ND 329 03/09/23 08:48127
4-Chloro-3-methylphenol ug/kg ND 658 03/09/23 08:48231
4-Chloroaniline ug/kg ND 658 03/09/23 08:48258
4-Chlorophenylphenyl ether ug/kg ND 329 03/09/23 08:48123
4-Nitroaniline ug/kg ND 658 03/09/23 08:48250
4-Nitrophenol ug/kg ND 1640 03/09/23 08:48636
Acenaphthene ug/kg ND 329 03/09/23 08:48116
Acenaphthylene ug/kg ND 329 03/09/23 08:48116
Aniline ug/kg ND 329 03/09/23 08:48129
Anthracene ug/kg ND 329 03/09/23 08:48108
Benzo(a)anthracene ug/kg ND 329 03/09/23 08:48110
Benzo(a)pyrene ug/kg ND 329 03/09/23 08:48114
Benzo(b)fluoranthene ug/kg ND 329 03/09/23 08:48110
Benzo(g,h,i)perylene ug/kg ND 329 03/09/23 08:48128
Benzo(k)fluoranthene ug/kg ND 329 03/09/23 08:48116
Benzoic Acid ug/kg ND 1640 03/09/23 08:48707
Benzyl alcohol ug/kg ND 658 03/09/23 08:48249
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3948387
Associated Lab Samples:92655679001, 92655679002, 92655679003, 92655679004, 92655679007, 92655679008, 92655679009
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 329 03/09/23 08:48137
bis(2-Chloroethyl) ether ug/kg ND 329 03/09/23 08:48124
bis(2-Ethylhexyl)phthalate ug/kg ND 329 03/09/23 08:48128
Butylbenzylphthalate ug/kg ND 329 03/09/23 08:48139
Chrysene ug/kg ND 329 03/09/23 08:48120
Di-n-butylphthalate ug/kg ND 329 03/09/23 08:48111
Di-n-octylphthalate ug/kg ND 329 03/09/23 08:48130
Dibenz(a,h)anthracene ug/kg ND 329 03/09/23 08:48127
Dibenzofuran ug/kg ND 329 03/09/23 08:48119
Diethylphthalate ug/kg ND 329 03/09/23 08:48121
Dimethylphthalate ug/kg ND 329 03/09/23 08:48120
Fluoranthene ug/kg ND 329 03/09/23 08:48113
Fluorene ug/kg ND 329 03/09/23 08:48116
Hexachloro-1,3-butadiene ug/kg ND 329 03/09/23 08:48143
Hexachlorobenzene ug/kg ND 329 03/09/23 08:48129
Hexachlorocyclopentadiene ug/kg ND 329 03/09/23 08:48188
Hexachloroethane ug/kg ND 329 03/09/23 08:48126
Indeno(1,2,3-cd)pyrene ug/kg ND 329 03/09/23 08:48130
Isophorone ug/kg ND 329 03/09/23 08:48147
N-Nitroso-di-n-propylamine ug/kg ND 329 03/09/23 08:48124
N-Nitrosodimethylamine ug/kg ND 329 03/09/23 08:48111
N-Nitrosodiphenylamine ug/kg ND 329 03/09/23 08:48117
Naphthalene ug/kg ND 329 03/09/23 08:48112
Nitrobenzene ug/kg ND 329 03/09/23 08:48152
Pentachlorophenol ug/kg ND 658 03/09/23 08:48322
Phenanthrene ug/kg ND 329 03/09/23 08:48108
Phenol ug/kg ND 329 03/09/23 08:48147
Pyrene ug/kg ND 329 03/09/23 08:48134
Pyridine ug/kg ND 329 03/09/23 08:48104
2,4,6-Tribromophenol (S)%65 10-131 03/09/23 08:48
2-Fluorobiphenyl (S)%62 10-130 03/09/23 08:48
2-Fluorophenol (S)%57 10-130 03/09/23 08:48
Nitrobenzene-d5 (S)%64 10-130 03/09/23 08:48
Phenol-d6 (S)%59 10-130 03/09/23 08:48
Terphenyl-d14 (S)%66 10-130 03/09/23 08:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3948388LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10601680 63 43-130
1,2-Dichlorobenzene ug/kg 11201680 67 43-130
1,3-Dichlorobenzene ug/kg 10901680 65 43-130
1,4-Dichlorobenzene ug/kg 11001680 65 44-130
1-Methylnaphthalene ug/kg 11101680 66 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3948388LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 12101680 72 29-130
2,4,5-Trichlorophenol ug/kg 12101680 72 47-130
2,4,6-Trichlorophenol ug/kg 12201680 72 47-130
2,4-Dichlorophenol ug/kg 11101680 66 45-130
2,4-Dimethylphenol ug/kg 14501680 86 45-130
2,4-Dinitrophenol ug/kg 62108420 74 27-140
2,4-Dinitrotoluene ug/kg 11401680 68 46-130
2,6-Dinitrotoluene ug/kg 11801680 70 48-130
2-Chloronaphthalene ug/kg 11301680 67 46-130
2-Chlorophenol ug/kg 11201680 66 43-130
2-Methylnaphthalene ug/kg 10501680 62 47-130
2-Methylphenol(o-Cresol)ug/kg 11501680 68 42-130
2-Nitroaniline ug/kg 24703370 73 41-130
2-Nitrophenol ug/kg 11201680 66 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 12101680 72 39-130
3,3'-Dichlorobenzidine ug/kg 21103370 63 41-130
3-Nitroaniline ug/kg 19603370 58 37-130
4,6-Dinitro-2-methylphenol ug/kg 26703370 79 38-141
4-Bromophenylphenyl ether ug/kg 11801680 70 47-130
4-Chloro-3-methylphenol ug/kg 22103370 66 44-130
4-Chloroaniline ug/kg 20203370 60 41-130
4-Chlorophenylphenyl ether ug/kg 11201680 66 45-130
4-Nitroaniline ug/kg 22203370 66 42-130
4-Nitrophenol ug/kg 54308420 65 39-131
Acenaphthene ug/kg 11801680 70 49-130
Acenaphthylene ug/kg 11801680 70 50-130
Aniline ug/kg 9711680 58 38-130
Anthracene ug/kg 11601680 69 49-130
Benzo(a)anthracene ug/kg 11901680 71 51-130
Benzo(a)pyrene ug/kg 10401680 62 51-130
Benzo(b)fluoranthene ug/kg 10201680 61 49-130
Benzo(g,h,i)perylene ug/kg 12001680 71 48-140
Benzo(k)fluoranthene ug/kg 10401680 61 51-130
Benzoic Acid ug/kg 44008420 52 22-130
Benzyl alcohol ug/kg 22203370 66 43-130
bis(2-Chloroethoxy)methane ug/kg 10501680 62 43-130
bis(2-Chloroethyl) ether ug/kg 11001680 65 42-130
bis(2-Ethylhexyl)phthalate ug/kg 12301680 73 43-130
Butylbenzylphthalate ug/kg 12001680 71 44-131
Chrysene ug/kg 12001680 71 51-130
Di-n-butylphthalate ug/kg 12001680 72 46-130
Di-n-octylphthalate ug/kg 12301680 73 45-130
Dibenz(a,h)anthracene ug/kg 11701680 70 48-130
Dibenzofuran ug/kg 11401680 68 10-130
Diethylphthalate ug/kg 11401680 68 48-130
Dimethylphthalate ug/kg 11301680 67 48-130
Fluoranthene ug/kg 11901680 71 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3948388LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 11601680 69 48-130
Hexachloro-1,3-butadiene ug/kg 10301680 61 39-130
Hexachlorobenzene ug/kg 11701680 69 47-130
Hexachlorocyclopentadiene ug/kg 10001680 60 17-130
Hexachloroethane ug/kg 11201680 67 40-130
Indeno(1,2,3-cd)pyrene ug/kg 11801680 70 50-130
Isophorone ug/kg 10901680 65 41-130
N-Nitroso-di-n-propylamine ug/kg 11501680 69 36-130
N-Nitrosodimethylamine ug/kg 10401680 62 34-130
N-Nitrosodiphenylamine ug/kg 12401680 74 48-130
Naphthalene ug/kg 10901680 65 46-130
Nitrobenzene ug/kg 10901680 65 39-130
Pentachlorophenol ug/kg 18503370 55 42-130
Phenanthrene ug/kg 12401680 74 50-130
Phenol ug/kg 11201680 67 42-130
Pyrene ug/kg 11901680 71 50-130
Pyridine ug/kg 7721680 46 26-130
2,4,6-Tribromophenol (S)%75 10-131
2-Fluorobiphenyl (S)%65 10-130
2-Fluorophenol (S)%62 10-130
Nitrobenzene-d5 (S)%61 10-130
Phenol-d6 (S)%63 10-130
Terphenyl-d14 (S)%70 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3948389MATRIX SPIKE SAMPLE:
MSSpike
Result
92655502004
1,2,4-Trichlorobenzene ug/kg 7281850 39 16-130<144
1,2-Dichlorobenzene ug/kg 8121850 44 19-130<132
1,3-Dichlorobenzene ug/kg 7871850 43 19-130<129
1,4-Dichlorobenzene ug/kg 7981850 43 20-130<139
1-Methylnaphthalene ug/kg 7661850 41 19-130<128
2,2'-Oxybis(1-chloropropane)ug/kg 8341850 45 10-130<174
2,4,5-Trichlorophenol ug/kg 8181850 44 19-130<167
2,4,6-Trichlorophenol ug/kg 8421850 46 18-130<150
2,4-Dichlorophenol ug/kg 7471850 40 16-130<143
2,4-Dimethylphenol ug/kg 9631850 52 10-130<151
2,4-Dinitrophenol ug/kg 41409250 45 10-143<1130
2,4-Dinitrotoluene ug/kg 7941850 43 19-130<140
2,6-Dinitrotoluene ug/kg 7921850 43 22-130<134
2-Chloronaphthalene ug/kg 7871850 43 18-130<145
2-Chlorophenol ug/kg 8141850 44 20-130<137
2-Methylnaphthalene ug/kg 7421850 40 18-130<146
2-Methylphenol(o-Cresol)ug/kg 8491850 46 13-130<149
2-Nitroaniline ug/kg 1700J3700 46 18-130<298
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3948389MATRIX SPIKE SAMPLE:
MSSpike
Result
92655502004
2-Nitrophenol ug/kg 7781850 42 19-130<158
3&4-Methylphenol(m&p Cresol)ug/kg 8531850 46 13-130<147
3,3'-Dichlorobenzidine ug/kg 13903700 38 10-130<246
3-Nitroaniline ug/kg 1360J3700 37 22-130<286
4,6-Dinitro-2-methylphenol ug/kg 18403700 50 10-144<340
4-Bromophenylphenyl ether ug/kg 7781850 42 18-130<140
4-Chloro-3-methylphenol ug/kg 14703700 40 16-130<256
4-Chloroaniline ug/kg 13303700 36 17-130<286
4-Chlorophenylphenyl ether ug/kg 7631850 41 17-130<136
4-Nitroaniline ug/kg 14803700 40 21-130<277
4-Nitrophenol ug/kg 38709250 42 13-131<705
Acenaphthene ug/kg 8041850 43 20-130<128
Acenaphthylene ug/kg 7971850 43 21-130<128
Aniline ug/kg 5781850 31 10-130<143
Anthracene ug/kg 7761850 42 19-130<119
Benzo(a)anthracene ug/kg 7981850 43 17-130<122
Benzo(a)pyrene ug/kg 6691850 36 14-130<126
Benzo(b)fluoranthene ug/kg 6611850 36 11-134<122
Benzo(g,h,i)perylene ug/kg 7391850 40 12-130<141
Benzo(k)fluoranthene ug/kg 6701850 36 15-130<128
Benzoic Acid ug/kg 26709250 29 10-130<784
Benzyl alcohol ug/kg 15303700 41 20-130<276
bis(2-Chloroethoxy)methane ug/kg 7041850 38 16-130<151
bis(2-Chloroethyl) ether ug/kg 7831850 42 18-130<137
bis(2-Ethylhexyl)phthalate ug/kg 7751850 42 11-130<141
Butylbenzylphthalate ug/kg 7471850 40 10-130<154
Chrysene ug/kg 8041850 43 17-130<133
Di-n-butylphthalate ug/kg 8091850 44 16-130<123
Di-n-octylphthalate ug/kg 8151850 44 16-130<144
Dibenz(a,h)anthracene ug/kg 7461850 40 13-130<140
Dibenzofuran ug/kg 7991850 43 19-130<132
Diethylphthalate ug/kg 7711850 42 22-130<134
Dimethylphthalate ug/kg 7701850 42 23-130<133
Fluoranthene ug/kg 7981850 43 14-130<125
Fluorene ug/kg 8091850 44 19-130<128
Hexachloro-1,3-butadiene ug/kg 7281850 39 12-130<158
Hexachlorobenzene ug/kg 7751850 42 17-130<143
Hexachlorocyclopentadiene ug/kg 5851850 32 10-130<209
Hexachloroethane ug/kg 8051850 44 14-130<139
Indeno(1,2,3-cd)pyrene ug/kg 7561850 41 13-130<144
Isophorone ug/kg 7421850 40 17-130<162
N-Nitroso-di-n-propylamine ug/kg 7871850 43 10-130<137
N-Nitrosodimethylamine ug/kg 6941850 38 16-130<123
N-Nitrosodiphenylamine ug/kg 8161850 44 19-130<129
Naphthalene ug/kg 7771850 42 18-130<124
Nitrobenzene ug/kg 7451850 40 15-130<169
Pentachlorophenol ug/kg 11703700 32 10-130<357
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3948389MATRIX SPIKE SAMPLE:
MSSpike
Result
92655502004
Phenanthrene ug/kg 8401850 45 17-130<119
Phenol ug/kg 7931850 43 15-130<162
Pyrene ug/kg 7491850 41 31-130<148
Pyridine ug/kg 5431850 29 10-130<115
2,4,6-Tribromophenol (S)%44 10-131
2-Fluorobiphenyl (S)%40 10-130
2-Fluorophenol (S)%39 10-130
Nitrobenzene-d5 (S)%39 10-130
Phenol-d6 (S)%40 10-130
Terphenyl-d14 (S)%38 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655176003
3948390SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655176003
3948390SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%5966
2-Fluorobiphenyl (S)%4056
2-Fluorophenol (S)%4056
Nitrobenzene-d5 (S)%4258
Phenol-d6 (S)%4259
Terphenyl-d14 (S)%4854
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760184
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92655679001, 92655679002, 92655679003, 92655679004, 92655679007
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655337001
3948294SAMPLE DUPLICATE:
Percent Moisture %30.5 N202530.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655679007
3948295SAMPLE DUPLICATE:
Percent Moisture %22.5 N232523.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760194
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92655679008, 92655679009
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655603001
3948397SAMPLE DUPLICATE:
Percent Moisture %26.9 N212527.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655310004
3948974SAMPLE DUPLICATE:
Percent Moisture %13.3 N272512.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2021167
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92655679001, 92655679002, 92655679003, 92655679004, 92655679005, 92655679006, 92655679007,
92655679008, 92655679009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3900865-1
Associated Lab Samples: 92655679001, 92655679002, 92655679003, 92655679004, 92655679005, 92655679006, 92655679007,
92655679008, 92655679009
Matrix: Solid
AnalyzedMDL
Total Solids %0.00200 03/13/23 15:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3900865-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.150.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655679001
R3900865-3SAMPLE DUPLICATE:
Total Solids %82.2 1.94 1080.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
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[phone]
Page 70 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2021568
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92655679001, 92655679002, 92655679003, 92655679004, 92655679005, 92655679006, 92655679007,
92655679008, 92655679009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3901003-1
Associated Lab Samples: 92655679001, 92655679002, 92655679003, 92655679004, 92655679005, 92655679006, 92655679007,
92655679008, 92655679009
Matrix: Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 03/14/23 14:460.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3901003-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.010.0 100 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3901003-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655679004
R3901003-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 25.7 89.5 75.0-12595.2 5.95 2025.71.11 24.1 25.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655679001
R3901003-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 1.01J D8,J36.3 201.45
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1593414-03
R3901003-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
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[phone]
Page 71 of 78
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Result may be biased high due to carryover from previously analyzed sample.C8
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
The sample and duplicate results for this parameter are less than 5 times the reporting limit, the RPD may not bestatistically valid.D8
Analyte concentration exceeded the calibration range. The reported result is estimated.E
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
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Huntersville, NC 28078
[phone]
Page 72 of 78
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
ANALYTE QUALIFIERS
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 78
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92655679001 870782 871170COMP-1 (0-2)EPA 3050B EPA 6020B
92655679002 870782 871170COMP-2 (0-2)EPA 3050B EPA 6020B
92655679003 870782 871170BF-SB-01 (0-2)EPA 3050B EPA 6020B
92655679004 870782 871170BF-SB-02 (0-2)EPA 3050B EPA 6020B
92655679005 870782 871170BF-BG-1 (0-2)EPA 3050B EPA 6020B
92655679006 870782 871170BF-BG-2 (0-2)EPA 3050B EPA 6020B
92655679007 870782 871170BF-SB-DUP EPA 3050B EPA 6020B
92655679008 870782 871170BF-SB-01 (2-4)EPA 3050B EPA 6020B
92655679009 870782 871170BF-SB-02 (2-4)EPA 3050B EPA 6020B
92655679001 870786 871123COMP-1 (0-2)EPA 7471B EPA 7471B
92655679002 870786 871123COMP-2 (0-2)EPA 7471B EPA 7471B
92655679003 870786 871123BF-SB-01 (0-2)EPA 7471B EPA 7471B
92655679004 870786 871123BF-SB-02 (0-2)EPA 7471B EPA 7471B
92655679005 870786 871123BF-BG-1 (0-2)EPA 7471B EPA 7471B
92655679006 870786 871123BF-BG-2 (0-2)EPA 7471B EPA 7471B
92655679007 870786 871123BF-SB-DUP EPA 7471B EPA 7471B
92655679008 870786 871123BF-SB-01 (2-4)EPA 7471B EPA 7471B
92655679009 870786 871123BF-SB-02 (2-4)EPA 7471B EPA 7471B
92655679005 870730BF-BG-1 (0-2)ASTM D2974
92655679006 870730BF-BG-2 (0-2)ASTM D2974
92655679001 760193 760334COMP-1 (0-2)EPA 3546 EPA 8270E
92655679002 760193 760334COMP-2 (0-2)EPA 3546 EPA 8270E
92655679003 760193 760334BF-SB-01 (0-2)EPA 3546 EPA 8270E
92655679004 760193 760334BF-SB-02 (0-2)EPA 3546 EPA 8270E
92655679007 760193 760334BF-SB-DUP EPA 3546 EPA 8270E
92655679008 760193 760334BF-SB-01 (2-4)EPA 3546 EPA 8270E
92655679009 760193 760334BF-SB-02 (2-4)EPA 3546 EPA 8270E
92655679001 760303 760406COMP-1 (0-2)EPA 5035A/5030B EPA 8260D
92655679002 760303 760406COMP-2 (0-2)EPA 5035A/5030B EPA 8260D
92655679003 760513 760534BF-SB-01 (0-2)EPA 5035A/5030B EPA 8260D
92655679004 760513 760534BF-SB-02 (0-2)EPA 5035A/5030B EPA 8260D
92655679007 760513 760534BF-SB-DUP EPA 5035A/5030B EPA 8260D
92655679008 760513 760534BF-SB-01 (2-4)EPA 5035A/5030B EPA 8260D
92655679009 760513 760534BF-SB-02 (2-4)EPA 5035A/5030B EPA 8260D
92655679001 760184COMP-1 (0-2)SW-846
92655679002 760184COMP-2 (0-2)SW-846
92655679003 760184BF-SB-01 (0-2)SW-846
92655679004 760184BF-SB-02 (0-2)SW-846
92655679007 760184BF-SB-DUP SW-846
92655679008 760194BF-SB-01 (2-4)SW-846
92655679009 760194BF-SB-02 (2-4)SW-846
92655679001 2021167 2021167COMP-1 (0-2)SM 2540 G SM 2540G
92655679002 2021167 2021167COMP-2 (0-2)SM 2540 G SM 2540G
92655679003 2021167 2021167BF-SB-01 (0-2)SM 2540 G SM 2540G
92655679004 2021167 2021167BF-SB-02 (0-2)SM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 78
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92655679
GEORGE FERN FDI-001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92655679005 2021167 2021167BF-BG-1 (0-2)SM 2540 G SM 2540G
92655679006 2021167 2021167BF-BG-2 (0-2)SM 2540 G SM 2540G
92655679007 2021167 2021167BF-SB-DUP SM 2540 G SM 2540G
92655679008 2021167 2021167BF-SB-01 (2-4)SM 2540 G SM 2540G
92655679009 2021167 2021167BF-SB-02 (2-4)SM 2540 G SM 2540G
92655679001 2021568 2021568COMP-1 (0-2)3060A EPA 7199
92655679002 2021568 2021568COMP-2 (0-2)3060A EPA 7199
92655679003 2021568 2021568BF-SB-01 (0-2)3060A EPA 7199
92655679004 2021568 2021568BF-SB-02 (0-2)3060A EPA 7199
92655679005 2021568 2021568BF-BG-1 (0-2)3060A EPA 7199
92655679006 2021568 2021568BF-BG-2 (0-2)3060A EPA 7199
92655679007 2021568 2021568BF-SB-DUP 3060A EPA 7199
92655679008 2021568 2021568BF-SB-01 (2-4)3060A EPA 7199
92655679009 2021568 2021568BF-SB-02 (2-4)3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 03:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 75 of 78
Page 76 of 78
Page 77 of 78
Page 78 of 78
#=CL#
March 15, 2023
LIMS USE: FR - HALEY MARTIN
LIMS OBJECT ID: 92655680
92655680
Project:
Pace Project No.:
RE:
Haley Martin
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
GEORGE FERN FDI-001
Dear Haley Martin:
Enclosed are the analytical results for sample(s) received by the laboratory on March 08, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 55
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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[phone]
Page 2 of 55
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Lab ID Sample ID Matrix Date Collected Date Received
92655680001 OFF-MW-1 Water 03/06/23 14:40 03/08/23 10:37
92655680002 OFF-MW-5 Water 03/06/23 17:00 03/08/23 10:37
92655680003 OFF-MW-6 Water 03/07/23 16:35 03/08/23 10:37
92655680004 OFF-MW-7 Water 03/06/23 16:15 03/08/23 10:37
92655680005 MW-11S Water 03/06/23 13:05 03/08/23 10:37
92655680006 GW-DUP Water 03/06/23 00:00 03/08/23 10:37
92655680007 TRIP BLANK Water 03/06/23 00:00 03/08/23 10:37
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 3 of 55
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92655680001 OFF-MW-1 EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ANMP
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92655680002 OFF-MW-5 EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ANMP
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92655680003 OFF-MW-6 EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ANMP
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92655680004 OFF-MW-7 EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ANMP
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CJJK
92655680005 MW-11S EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ANMP
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CJJK
92655680006 GW-DUP EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ANMP
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92655680007 TRIP BLANK EPA 8260D 63 PASI-CJJK
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-1 Lab ID: 92655680001 Collected: 03/06/23 14:40 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic ND ug/L 03/14/23 18:10 7440-38-203/10/23 12:231.0 0.087 1
Barium 59.8 ug/L 03/14/23 18:10 7440-39-303/10/23 12:231.0 0.21 1
Cadmium ND ug/L 03/14/23 18:10 7440-43-903/10/23 12:230.20 0.060 1
Chromium 4.4 ug/L 03/14/23 18:10 7440-47-303/10/23 12:231.0 0.50 1
Lead ND ug/L 03/14/23 18:10 7439-92-103/10/23 12:231.0 0.077 1
Selenium ND ug/L 03/14/23 18:10 7782-49-203/10/23 12:232.0 0.072 1
Silver ND ug/L 03/14/23 18:10 7440-22-403/10/23 12:230.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 03/13/23 10:11 7439-97-603/13/23 07:030.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/10/23 18:43 83-32-903/09/23 13:538.3 1.7 1
Acenaphthylene ND ug/L 03/10/23 18:43 208-96-803/09/23 13:538.3 1.6 1
Aniline ND ug/L 03/10/23 18:43 62-53-3 L203/09/23 13:538.3 1.4 1
Anthracene ND ug/L 03/10/23 18:43 120-12-703/09/23 13:538.3 1.9 1
Benzo(a)anthracene ND ug/L 03/10/23 18:43 56-55-303/09/23 13:538.3 2.2 1
Benzo(a)pyrene ND ug/L 03/10/23 18:43 50-32-803/09/23 13:538.3 2.3 1
Benzo(b)fluoranthene ND ug/L 03/10/23 18:43 205-99-203/09/23 13:538.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 03/10/23 18:43 191-24-203/09/23 13:538.3 2.4 1
Benzo(k)fluoranthene ND ug/L 03/10/23 18:43 207-08-903/09/23 13:538.3 2.3 1
Benzoic Acid ND ug/L 03/10/23 18:43 65-85-003/09/23 13:5341.7 18.3 1
Benzyl alcohol ND ug/L 03/10/23 18:43 100-51-603/09/23 13:5316.7 2.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/23 18:43 101-55-303/09/23 13:538.3 1.5 1
Butylbenzylphthalate ND ug/L 03/10/23 18:43 85-68-703/09/23 13:538.3 2.6 1
4-Chloro-3-methylphenol ND ug/L 03/10/23 18:43 59-50-703/09/23 13:538.3 2.8 1
4-Chloroaniline ND ug/L 03/10/23 18:43 106-47-803/09/23 13:5316.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/23 18:43 111-91-103/09/23 13:538.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 03/10/23 18:43 111-44-403/09/23 13:538.3 1.6 1
2-Chloronaphthalene ND ug/L 03/10/23 18:43 91-58-703/09/23 13:538.3 1.4 1
2-Chlorophenol ND ug/L 03/10/23 18:43 95-57-803/09/23 13:538.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 03/10/23 18:43 7005-72-303/09/23 13:538.3 1.7 1
Chrysene ND ug/L 03/10/23 18:43 218-01-903/09/23 13:538.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 03/10/23 18:43 53-70-303/09/23 13:538.3 2.5 1
Dibenzofuran ND ug/L 03/10/23 18:43 132-64-903/09/23 13:538.3 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/23 18:43 95-50-103/09/23 13:538.3 1.5 1
1,3-Dichlorobenzene ND ug/L 03/10/23 18:43 541-73-103/09/23 13:538.3 1.3 1
1,4-Dichlorobenzene ND ug/L 03/10/23 18:43 106-46-703/09/23 13:538.3 1.4 1
3,3'-Dichlorobenzidine ND ug/L 03/10/23 18:43 91-94-103/09/23 13:5316.7 6.8 1
2,4-Dichlorophenol ND ug/L 03/10/23 18:43 120-83-203/09/23 13:538.3 1.2 1
Diethylphthalate ND ug/L 03/10/23 18:43 84-66-203/09/23 13:538.3 1.7 1
2,4-Dimethylphenol ND ug/L 03/10/23 18:43 105-67-903/09/23 13:538.3 1.4 1
Dimethylphthalate ND ug/L 03/10/23 18:43 131-11-303/09/23 13:538.3 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
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[phone]
Page 5 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-1 Lab ID: 92655680001 Collected: 03/06/23 14:40 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 03/10/23 18:43 84-74-203/09/23 13:538.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/23 18:43 534-52-103/09/23 13:5316.7 6.5 1
2,4-Dinitrophenol ND ug/L 03/10/23 18:43 51-28-503/09/23 13:5341.7 21.7 1
2,4-Dinitrotoluene ND ug/L 03/10/23 18:43 121-14-203/09/23 13:538.3 1.4 1
2,6-Dinitrotoluene ND ug/L 03/10/23 18:43 606-20-203/09/23 13:538.3 1.4 1
Di-n-octylphthalate ND ug/L 03/10/23 18:43 117-84-003/09/23 13:538.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/23 18:43 117-81-703/09/23 13:535.0 3.1 1
Fluoranthene ND ug/L 03/10/23 18:43 206-44-003/09/23 13:538.3 1.8 1
Fluorene ND ug/L 03/10/23 18:43 86-73-703/09/23 13:538.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 03/10/23 18:43 87-68-303/09/23 13:538.3 1.5 1
Hexachlorobenzene ND ug/L 03/10/23 18:43 118-74-103/09/23 13:538.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 03/10/23 18:43 77-47-403/09/23 13:538.3 1.3 1
Hexachloroethane ND ug/L 03/10/23 18:43 67-72-103/09/23 13:538.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/23 18:43 193-39-503/09/23 13:538.3 2.4 1
Isophorone ND ug/L 03/10/23 18:43 78-59-103/09/23 13:538.3 1.4 1
1-Methylnaphthalene ND ug/L 03/10/23 18:43 90-12-003/09/23 13:538.3 1.7 1
2-Methylnaphthalene ND ug/L 03/10/23 18:43 91-57-603/09/23 13:538.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/23 18:43 95-48-703/09/23 13:538.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/23 18:43 15831-10-403/09/23 13:538.3 1.0 1
Naphthalene ND ug/L 03/10/23 18:43 91-20-303/09/23 13:538.3 1.7 1
2-Nitroaniline ND ug/L 03/10/23 18:43 88-74-403/09/23 13:5316.7 2.5 1
3-Nitroaniline ND ug/L 03/10/23 18:43 99-09-203/09/23 13:5316.7 3.1 1
4-Nitroaniline ND ug/L 03/10/23 18:43 100-01-603/09/23 13:5316.7 4.2 1
Nitrobenzene ND ug/L 03/10/23 18:43 98-95-303/09/23 13:538.3 1.6 1
2-Nitrophenol ND ug/L 03/10/23 18:43 88-75-5 v103/09/23 13:538.3 1.2 1
4-Nitrophenol ND ug/L 03/10/23 18:43 100-02-703/09/23 13:5341.7 5.5 1
N-Nitrosodimethylamine ND ug/L 03/10/23 18:43 62-75-9 v103/09/23 13:538.3 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/23 18:43 621-64-703/09/23 13:538.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/23 18:43 86-30-603/09/23 13:538.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/23 18:43 108-60-1 v103/09/23 13:538.3 0.96 1
Pentachlorophenol ND ug/L 03/10/23 18:43 87-86-503/09/23 13:5316.7 3.1 1
Phenanthrene ND ug/L 03/10/23 18:43 85-01-803/09/23 13:538.3 1.7 1
Phenol ND ug/L 03/10/23 18:43 108-95-203/09/23 13:538.3 1.1 1
Pyrene ND ug/L 03/10/23 18:43 129-00-003/09/23 13:538.3 1.8 1
1,2,4-Trichlorobenzene ND ug/L 03/10/23 18:43 120-82-103/09/23 13:538.3 1.4 1
2,4,5-Trichlorophenol ND ug/L 03/10/23 18:43 95-95-403/09/23 13:538.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/23 18:43 88-06-203/09/23 13:538.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)72 %03/10/23 18:43 4165-60-003/09/23 13:5310-138 1
2-Fluorobiphenyl (S)71 %03/10/23 18:43 321-60-803/09/23 13:5310-130 1
Terphenyl-d14 (S)109 %03/10/23 18:43 1718-51-003/09/23 13:5319-191 1
Phenol-d6 (S)44 %03/10/23 18:43 13127-88-303/09/23 13:5310-130 1
2-Fluorophenol (S)57 %03/10/23 18:43 367-12-403/09/23 13:5310-130 1
2,4,6-Tribromophenol (S)88 %03/10/23 18:43 118-79-603/09/23 13:5310-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-1 Lab ID: 92655680001 Collected: 03/06/23 14:40 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 03/09/23 23:09 67-64-150.0 10.2 2
Benzene ND ug/L 03/09/23 23:09 71-43-22.0 0.69 2
Bromobenzene ND ug/L 03/09/23 23:09 108-86-12.0 0.58 2
Bromochloromethane ND ug/L 03/09/23 23:09 74-97-52.0 0.94 2
Bromodichloromethane ND ug/L 03/09/23 23:09 75-27-42.0 0.61 2
Bromoform ND ug/L 03/09/23 23:09 75-25-22.0 0.68 2
Bromomethane ND ug/L 03/09/23 23:09 74-83-94.0 3.3 2
2-Butanone (MEK)ND ug/L 03/09/23 23:09 78-93-310.0 7.9 2
Carbon tetrachloride ND ug/L 03/09/23 23:09 56-23-52.0 0.67 2
Chlorobenzene ND ug/L 03/09/23 23:09 108-90-72.0 0.57 2
Chloroethane ND ug/L 03/09/23 23:09 75-00-32.0 1.3 2
Chloroform ND ug/L 03/09/23 23:09 67-66-32.0 0.86 2
Chloromethane ND ug/L 03/09/23 23:09 74-87-32.0 1.1 2
2-Chlorotoluene ND ug/L 03/09/23 23:09 95-49-82.0 0.64 2
4-Chlorotoluene ND ug/L 03/09/23 23:09 106-43-42.0 0.65 2
1,2-Dibromo-3-chloropropane ND ug/L 03/09/23 23:09 96-12-84.0 0.68 2
Dibromochloromethane ND ug/L 03/09/23 23:09 124-48-12.0 0.72 2
1,2-Dibromoethane (EDB)ND ug/L 03/09/23 23:09 106-93-42.0 0.54 2
Dibromomethane ND ug/L 03/09/23 23:09 74-95-32.0 0.79 2
1,2-Dichlorobenzene ND ug/L 03/09/23 23:09 95-50-12.0 0.68 2
1,3-Dichlorobenzene ND ug/L 03/09/23 23:09 541-73-12.0 0.68 2
1,4-Dichlorobenzene ND ug/L 03/09/23 23:09 106-46-72.0 0.67 2
Dichlorodifluoromethane ND ug/L 03/09/23 23:09 75-71-82.0 0.69 2
1,1-Dichloroethane ND ug/L 03/09/23 23:09 75-34-32.0 0.73 2
1,2-Dichloroethane ND ug/L 03/09/23 23:09 107-06-22.0 0.64 2
1,1-Dichloroethene ND ug/L 03/09/23 23:09 75-35-42.0 0.70 2
cis-1,2-Dichloroethene ND ug/L 03/09/23 23:09 156-59-22.0 0.77 2
trans-1,2-Dichloroethene ND ug/L 03/09/23 23:09 156-60-52.0 0.79 2
1,2-Dichloropropane ND ug/L 03/09/23 23:09 78-87-52.0 0.71 2
1,3-Dichloropropane ND ug/L 03/09/23 23:09 142-28-92.0 0.57 2
2,2-Dichloropropane ND ug/L 03/09/23 23:09 594-20-72.0 0.78 2
1,1-Dichloropropene ND ug/L 03/09/23 23:09 563-58-62.0 0.85 2
cis-1,3-Dichloropropene ND ug/L 03/09/23 23:09 10061-01-52.0 0.73 2
trans-1,3-Dichloropropene ND ug/L 03/09/23 23:09 10061-02-62.0 0.73 2
Diisopropyl ether ND ug/L 03/09/23 23:09 108-20-32.0 0.62 2
Ethylbenzene ND ug/L 03/09/23 23:09 100-41-42.0 0.61 2
Hexachloro-1,3-butadiene ND ug/L 03/09/23 23:09 87-68-34.0 3.1 2
2-Hexanone ND ug/L 03/09/23 23:09 591-78-610.0 0.95 2
p-Isopropyltoluene ND ug/L 03/09/23 23:09 99-87-62.0 0.83 2
Methylene Chloride ND ug/L 03/09/23 23:09 75-09-210.0 3.9 2
4-Methyl-2-pentanone (MIBK)ND ug/L 03/09/23 23:09 108-10-110.0 5.4 2
Methyl-tert-butyl ether ND ug/L 03/09/23 23:09 1634-04-42.0 0.84 2
Naphthalene ND ug/L 03/09/23 23:09 91-20-32.0 1.3 2
Styrene ND ug/L 03/09/23 23:09 100-42-52.0 0.58 2
1,1,1,2-Tetrachloroethane ND ug/L 03/09/23 23:09 630-20-62.0 0.62 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-1 Lab ID: 92655680001 Collected: 03/06/23 14:40 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 03/09/23 23:09 79-34-52.0 0.45 2
Tetrachloroethene 186 ug/L 03/09/23 23:09 127-18-42.0 0.58 2
Toluene ND ug/L 03/09/23 23:09 108-88-32.0 0.48 2
1,2,3-Trichlorobenzene ND ug/L 03/09/23 23:09 87-61-62.0 1.6 2
1,2,4-Trichlorobenzene ND ug/L 03/09/23 23:09 120-82-12.0 1.3 2
1,1,1-Trichloroethane ND ug/L 03/09/23 23:09 71-55-62.0 0.66 2
1,1,2-Trichloroethane ND ug/L 03/09/23 23:09 79-00-52.0 0.65 2
Trichloroethene ND ug/L 03/09/23 23:09 79-01-62.0 0.77 2
Trichlorofluoromethane ND ug/L 03/09/23 23:09 75-69-42.0 0.60 2
1,2,3-Trichloropropane ND ug/L 03/09/23 23:09 96-18-42.0 0.52 2
Vinyl acetate ND ug/L 03/09/23 23:09 108-05-44.0 2.6 2
Vinyl chloride ND ug/L 03/09/23 23:09 75-01-42.0 0.77 2
Xylene (Total)ND ug/L 03/09/23 23:09 1330-20-72.0 0.68 2
m&p-Xylene ND ug/L 03/09/23 23:09 179601-23-14.0 1.4 2
o-Xylene ND ug/L 03/09/23 23:09 95-47-62.0 0.68 2
Surrogates
4-Bromofluorobenzene (S)102 %03/09/23 23:09 460-00-470-130 2
1,2-Dichloroethane-d4 (S)100 %03/09/23 23:09 17060-07-070-130 2
Toluene-d8 (S)101 %03/09/23 23:09 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-5 Lab ID: 92655680002 Collected: 03/06/23 17:00 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic ND ug/L 03/14/23 18:14 7440-38-203/10/23 12:231.0 0.087 1
Barium 31.2 ug/L 03/14/23 18:14 7440-39-303/10/23 12:231.0 0.21 1
Cadmium ND ug/L 03/14/23 18:14 7440-43-903/10/23 12:230.20 0.060 1
Chromium 3.4 ug/L 03/14/23 18:14 7440-47-303/10/23 12:231.0 0.50 1
Lead ND ug/L 03/14/23 18:14 7439-92-103/10/23 12:231.0 0.077 1
Selenium ND ug/L 03/14/23 18:14 7782-49-203/10/23 12:232.0 0.072 1
Silver ND ug/L 03/14/23 18:14 7440-22-403/10/23 12:230.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 03/13/23 10:22 7439-97-603/13/23 07:030.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/10/23 19:08 83-32-903/09/23 13:539.1 1.8 1
Acenaphthylene ND ug/L 03/10/23 19:08 208-96-803/09/23 13:539.1 1.8 1
Aniline ND ug/L 03/10/23 19:08 62-53-3 L203/09/23 13:539.1 1.5 1
Anthracene ND ug/L 03/10/23 19:08 120-12-703/09/23 13:539.1 2.1 1
Benzo(a)anthracene ND ug/L 03/10/23 19:08 56-55-303/09/23 13:539.1 2.4 1
Benzo(a)pyrene ND ug/L 03/10/23 19:08 50-32-803/09/23 13:539.1 2.5 1
Benzo(b)fluoranthene ND ug/L 03/10/23 19:08 205-99-203/09/23 13:539.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 03/10/23 19:08 191-24-203/09/23 13:539.1 2.6 1
Benzo(k)fluoranthene ND ug/L 03/10/23 19:08 207-08-903/09/23 13:539.1 2.5 1
Benzoic Acid ND ug/L 03/10/23 19:08 65-85-003/09/23 13:5345.5 20.0 1
Benzyl alcohol ND ug/L 03/10/23 19:08 100-51-603/09/23 13:5318.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 03/10/23 19:08 101-55-303/09/23 13:539.1 1.6 1
Butylbenzylphthalate ND ug/L 03/10/23 19:08 85-68-703/09/23 13:539.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 03/10/23 19:08 59-50-703/09/23 13:539.1 3.0 1
4-Chloroaniline ND ug/L 03/10/23 19:08 106-47-803/09/23 13:5318.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/23 19:08 111-91-103/09/23 13:539.1 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/23 19:08 111-44-403/09/23 13:539.1 1.7 1
2-Chloronaphthalene ND ug/L 03/10/23 19:08 91-58-703/09/23 13:539.1 1.6 1
2-Chlorophenol ND ug/L 03/10/23 19:08 95-57-803/09/23 13:539.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 03/10/23 19:08 7005-72-303/09/23 13:539.1 1.8 1
Chrysene ND ug/L 03/10/23 19:08 218-01-903/09/23 13:539.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 03/10/23 19:08 53-70-303/09/23 13:539.1 2.7 1
Dibenzofuran ND ug/L 03/10/23 19:08 132-64-903/09/23 13:539.1 1.9 1
1,2-Dichlorobenzene ND ug/L 03/10/23 19:08 95-50-103/09/23 13:539.1 1.6 1
1,3-Dichlorobenzene ND ug/L 03/10/23 19:08 541-73-103/09/23 13:539.1 1.5 1
1,4-Dichlorobenzene ND ug/L 03/10/23 19:08 106-46-703/09/23 13:539.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 03/10/23 19:08 91-94-103/09/23 13:5318.2 7.4 1
2,4-Dichlorophenol ND ug/L 03/10/23 19:08 120-83-203/09/23 13:539.1 1.3 1
Diethylphthalate ND ug/L 03/10/23 19:08 84-66-203/09/23 13:539.1 1.9 1
2,4-Dimethylphenol ND ug/L 03/10/23 19:08 105-67-903/09/23 13:539.1 1.5 1
Dimethylphthalate ND ug/L 03/10/23 19:08 131-11-303/09/23 13:539.1 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-5 Lab ID: 92655680002 Collected: 03/06/23 17:00 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 03/10/23 19:08 84-74-203/09/23 13:539.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/23 19:08 534-52-103/09/23 13:5318.2 7.1 1
2,4-Dinitrophenol ND ug/L 03/10/23 19:08 51-28-503/09/23 13:5345.5 23.6 1
2,4-Dinitrotoluene ND ug/L 03/10/23 19:08 121-14-203/09/23 13:539.1 1.5 1
2,6-Dinitrotoluene ND ug/L 03/10/23 19:08 606-20-203/09/23 13:539.1 1.6 1
Di-n-octylphthalate ND ug/L 03/10/23 19:08 117-84-003/09/23 13:539.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/23 19:08 117-81-703/09/23 13:535.5 3.4 1
Fluoranthene ND ug/L 03/10/23 19:08 206-44-003/09/23 13:539.1 2.0 1
Fluorene ND ug/L 03/10/23 19:08 86-73-703/09/23 13:539.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 03/10/23 19:08 87-68-303/09/23 13:539.1 1.6 1
Hexachlorobenzene ND ug/L 03/10/23 19:08 118-74-103/09/23 13:539.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 03/10/23 19:08 77-47-403/09/23 13:539.1 1.4 1
Hexachloroethane ND ug/L 03/10/23 19:08 67-72-103/09/23 13:539.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/23 19:08 193-39-503/09/23 13:539.1 2.6 1
Isophorone ND ug/L 03/10/23 19:08 78-59-103/09/23 13:539.1 1.5 1
1-Methylnaphthalene ND ug/L 03/10/23 19:08 90-12-003/09/23 13:539.1 1.8 1
2-Methylnaphthalene ND ug/L 03/10/23 19:08 91-57-603/09/23 13:539.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/23 19:08 95-48-703/09/23 13:539.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/23 19:08 15831-10-403/09/23 13:539.1 1.1 1
Naphthalene ND ug/L 03/10/23 19:08 91-20-303/09/23 13:539.1 1.9 1
2-Nitroaniline ND ug/L 03/10/23 19:08 88-74-403/09/23 13:5318.2 2.7 1
3-Nitroaniline ND ug/L 03/10/23 19:08 99-09-203/09/23 13:5318.2 3.4 1
4-Nitroaniline ND ug/L 03/10/23 19:08 100-01-603/09/23 13:5318.2 4.6 1
Nitrobenzene ND ug/L 03/10/23 19:08 98-95-303/09/23 13:539.1 1.7 1
2-Nitrophenol ND ug/L 03/10/23 19:08 88-75-5 v103/09/23 13:539.1 1.3 1
4-Nitrophenol ND ug/L 03/10/23 19:08 100-02-703/09/23 13:5345.5 6.0 1
N-Nitrosodimethylamine ND ug/L 03/10/23 19:08 62-75-9 v103/09/23 13:539.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/23 19:08 621-64-703/09/23 13:539.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 03/10/23 19:08 86-30-603/09/23 13:539.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/23 19:08 108-60-1 v103/09/23 13:539.1 1.0 1
Pentachlorophenol ND ug/L 03/10/23 19:08 87-86-503/09/23 13:5318.2 3.4 1
Phenanthrene ND ug/L 03/10/23 19:08 85-01-803/09/23 13:539.1 1.8 1
Phenol ND ug/L 03/10/23 19:08 108-95-203/09/23 13:539.1 1.2 1
Pyrene ND ug/L 03/10/23 19:08 129-00-003/09/23 13:539.1 2.0 1
1,2,4-Trichlorobenzene ND ug/L 03/10/23 19:08 120-82-103/09/23 13:539.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 03/10/23 19:08 95-95-403/09/23 13:539.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 03/10/23 19:08 88-06-203/09/23 13:539.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)74 %03/10/23 19:08 4165-60-003/09/23 13:5310-138 1
2-Fluorobiphenyl (S)68 %03/10/23 19:08 321-60-803/09/23 13:5310-130 1
Terphenyl-d14 (S)111 %03/10/23 19:08 1718-51-003/09/23 13:5319-191 1
Phenol-d6 (S)43 %03/10/23 19:08 13127-88-303/09/23 13:5310-130 1
2-Fluorophenol (S)52 %03/10/23 19:08 367-12-403/09/23 13:5310-130 1
2,4,6-Tribromophenol (S)79 %03/10/23 19:08 118-79-603/09/23 13:5310-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-5 Lab ID: 92655680002 Collected: 03/06/23 17:00 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 03/09/23 23:45 67-64-1250 51.1 10
Benzene ND ug/L 03/09/23 23:45 71-43-210.0 3.4 10
Bromobenzene ND ug/L 03/09/23 23:45 108-86-110.0 2.9 10
Bromochloromethane ND ug/L 03/09/23 23:45 74-97-510.0 4.7 10
Bromodichloromethane ND ug/L 03/09/23 23:45 75-27-410.0 3.1 10
Bromoform ND ug/L 03/09/23 23:45 75-25-210.0 3.4 10
Bromomethane ND ug/L 03/09/23 23:45 74-83-920.0 16.6 10
2-Butanone (MEK)ND ug/L 03/09/23 23:45 78-93-350.0 39.6 10
Carbon tetrachloride ND ug/L 03/09/23 23:45 56-23-510.0 3.3 10
Chlorobenzene ND ug/L 03/09/23 23:45 108-90-710.0 2.8 10
Chloroethane ND ug/L 03/09/23 23:45 75-00-310.0 6.5 10
Chloroform ND ug/L 03/09/23 23:45 67-66-310.0 4.3 10
Chloromethane ND ug/L 03/09/23 23:45 74-87-310.0 5.4 10
2-Chlorotoluene ND ug/L 03/09/23 23:45 95-49-810.0 3.2 10
4-Chlorotoluene ND ug/L 03/09/23 23:45 106-43-410.0 3.2 10
1,2-Dibromo-3-chloropropane ND ug/L 03/09/23 23:45 96-12-820.0 3.4 10
Dibromochloromethane ND ug/L 03/09/23 23:45 124-48-110.0 3.6 10
1,2-Dibromoethane (EDB)ND ug/L 03/09/23 23:45 106-93-410.0 2.7 10
Dibromomethane ND ug/L 03/09/23 23:45 74-95-310.0 3.9 10
1,2-Dichlorobenzene ND ug/L 03/09/23 23:45 95-50-110.0 3.4 10
1,3-Dichlorobenzene ND ug/L 03/09/23 23:45 541-73-110.0 3.4 10
1,4-Dichlorobenzene ND ug/L 03/09/23 23:45 106-46-710.0 3.3 10
Dichlorodifluoromethane ND ug/L 03/09/23 23:45 75-71-810.0 3.5 10
1,1-Dichloroethane ND ug/L 03/09/23 23:45 75-34-310.0 3.7 10
1,2-Dichloroethane ND ug/L 03/09/23 23:45 107-06-210.0 3.2 10
1,1-Dichloroethene ND ug/L 03/09/23 23:45 75-35-410.0 3.5 10
cis-1,2-Dichloroethene 26.3 ug/L 03/09/23 23:45 156-59-210.0 3.8 10
trans-1,2-Dichloroethene ND ug/L 03/09/23 23:45 156-60-510.0 4.0 10
1,2-Dichloropropane ND ug/L 03/09/23 23:45 78-87-510.0 3.6 10
1,3-Dichloropropane ND ug/L 03/09/23 23:45 142-28-910.0 2.8 10
2,2-Dichloropropane ND ug/L 03/09/23 23:45 594-20-710.0 3.9 10
1,1-Dichloropropene ND ug/L 03/09/23 23:45 563-58-610.0 4.3 10
cis-1,3-Dichloropropene ND ug/L 03/09/23 23:45 10061-01-510.0 3.6 10
trans-1,3-Dichloropropene ND ug/L 03/09/23 23:45 10061-02-610.0 3.6 10
Diisopropyl ether ND ug/L 03/09/23 23:45 108-20-310.0 3.1 10
Ethylbenzene ND ug/L 03/09/23 23:45 100-41-410.0 3.0 10
Hexachloro-1,3-butadiene ND ug/L 03/09/23 23:45 87-68-320.0 15.3 10
2-Hexanone ND ug/L 03/09/23 23:45 591-78-650.0 4.8 10
p-Isopropyltoluene ND ug/L 03/09/23 23:45 99-87-610.0 4.1 10
Methylene Chloride ND ug/L 03/09/23 23:45 75-09-250.0 19.5 10
4-Methyl-2-pentanone (MIBK)ND ug/L 03/09/23 23:45 108-10-150.0 27.1 10
Methyl-tert-butyl ether ND ug/L 03/09/23 23:45 1634-04-410.0 4.2 10
Naphthalene ND ug/L 03/09/23 23:45 91-20-310.0 6.4 10
Styrene ND ug/L 03/09/23 23:45 100-42-510.0 2.9 10
1,1,1,2-Tetrachloroethane ND ug/L 03/09/23 23:45 630-20-610.0 3.1 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-5 Lab ID: 92655680002 Collected: 03/06/23 17:00 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 03/09/23 23:45 79-34-510.0 2.2 10
Tetrachloroethene 932 ug/L 03/09/23 23:45 127-18-410.0 2.9 10
Toluene ND ug/L 03/09/23 23:45 108-88-310.0 2.4 10
1,2,3-Trichlorobenzene ND ug/L 03/09/23 23:45 87-61-610.0 8.1 10
1,2,4-Trichlorobenzene ND ug/L 03/09/23 23:45 120-82-110.0 6.4 10
1,1,1-Trichloroethane ND ug/L 03/09/23 23:45 71-55-610.0 3.3 10
1,1,2-Trichloroethane ND ug/L 03/09/23 23:45 79-00-510.0 3.2 10
Trichloroethene 54.3 ug/L 03/09/23 23:45 79-01-610.0 3.8 10
Trichlorofluoromethane ND ug/L 03/09/23 23:45 75-69-410.0 3.0 10
1,2,3-Trichloropropane ND ug/L 03/09/23 23:45 96-18-410.0 2.6 10
Vinyl acetate ND ug/L 03/09/23 23:45 108-05-420.0 13.1 10
Vinyl chloride ND ug/L 03/09/23 23:45 75-01-410.0 3.9 10
Xylene (Total)ND ug/L 03/09/23 23:45 1330-20-710.0 3.4 10
m&p-Xylene ND ug/L 03/09/23 23:45 179601-23-120.0 7.1 10
o-Xylene ND ug/L 03/09/23 23:45 95-47-610.0 3.4 10
Surrogates
4-Bromofluorobenzene (S)104 %03/09/23 23:45 460-00-470-130 10
1,2-Dichloroethane-d4 (S)102 %03/09/23 23:45 17060-07-070-130 10
Toluene-d8 (S)102 %03/09/23 23:45 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-6 Lab ID: 92655680003 Collected: 03/07/23 16:35 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic 0.12J ug/L 03/14/23 18:18 7440-38-203/10/23 12:231.0 0.087 1
Barium 14.0 ug/L 03/14/23 18:18 7440-39-303/10/23 12:231.0 0.21 1
Cadmium ND ug/L 03/14/23 18:18 7440-43-903/10/23 12:230.20 0.060 1
Chromium 4.8 ug/L 03/14/23 18:18 7440-47-303/10/23 12:231.0 0.50 1
Lead 0.31J ug/L 03/14/23 18:18 7439-92-103/10/23 12:231.0 0.077 1
Selenium 0.16J ug/L 03/14/23 18:18 7782-49-203/10/23 12:232.0 0.072 1
Silver ND ug/L 03/14/23 18:18 7440-22-403/10/23 12:230.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 03/13/23 10:24 7439-97-603/13/23 07:030.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/10/23 19:34 83-32-903/09/23 13:5310.0 2.0 1
Acenaphthylene ND ug/L 03/10/23 19:34 208-96-803/09/23 13:5310.0 2.0 1
Aniline ND ug/L 03/10/23 19:34 62-53-3 L203/09/23 13:5310.0 1.6 1
Anthracene ND ug/L 03/10/23 19:34 120-12-703/09/23 13:5310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/10/23 19:34 56-55-303/09/23 13:5310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/10/23 19:34 50-32-803/09/23 13:5310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/10/23 19:34 205-99-203/09/23 13:5310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/10/23 19:34 191-24-203/09/23 13:5310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/10/23 19:34 207-08-903/09/23 13:5310.0 2.7 1
Benzoic Acid ND ug/L 03/10/23 19:34 65-85-003/09/23 13:5350.0 22.0 1
Benzyl alcohol ND ug/L 03/10/23 19:34 100-51-603/09/23 13:5320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/10/23 19:34 101-55-303/09/23 13:5310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/10/23 19:34 85-68-703/09/23 13:5310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/10/23 19:34 59-50-703/09/23 13:5310.0 3.3 1
4-Chloroaniline ND ug/L 03/10/23 19:34 106-47-803/09/23 13:5320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/23 19:34 111-91-103/09/23 13:5310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/10/23 19:34 111-44-403/09/23 13:5310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/10/23 19:34 91-58-703/09/23 13:5310.0 1.7 1
2-Chlorophenol ND ug/L 03/10/23 19:34 95-57-803/09/23 13:5310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/10/23 19:34 7005-72-303/09/23 13:5310.0 2.0 1
Chrysene ND ug/L 03/10/23 19:34 218-01-903/09/23 13:5310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/10/23 19:34 53-70-303/09/23 13:5310.0 3.0 1
Dibenzofuran ND ug/L 03/10/23 19:34 132-64-903/09/23 13:5310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/10/23 19:34 95-50-103/09/23 13:5310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/10/23 19:34 541-73-103/09/23 13:5310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/10/23 19:34 106-46-703/09/23 13:5310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/10/23 19:34 91-94-103/09/23 13:5320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/10/23 19:34 120-83-203/09/23 13:5310.0 1.4 1
Diethylphthalate ND ug/L 03/10/23 19:34 84-66-203/09/23 13:5310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/10/23 19:34 105-67-903/09/23 13:5310.0 1.7 1
Dimethylphthalate ND ug/L 03/10/23 19:34 131-11-303/09/23 13:5310.0 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-6 Lab ID: 92655680003 Collected: 03/07/23 16:35 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 03/10/23 19:34 84-74-203/09/23 13:5310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/23 19:34 534-52-103/09/23 13:5320.0 7.8 1
2,4-Dinitrophenol ND ug/L 03/10/23 19:34 51-28-503/09/23 13:5350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/10/23 19:34 121-14-203/09/23 13:5310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/10/23 19:34 606-20-203/09/23 13:5310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/23 19:34 117-84-003/09/23 13:5310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/23 19:34 117-81-703/09/23 13:536.0 3.7 1
Fluoranthene ND ug/L 03/10/23 19:34 206-44-003/09/23 13:5310.0 2.2 1
Fluorene ND ug/L 03/10/23 19:34 86-73-703/09/23 13:5310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/10/23 19:34 87-68-303/09/23 13:5310.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/23 19:34 118-74-103/09/23 13:5310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/10/23 19:34 77-47-403/09/23 13:5310.0 1.6 1
Hexachloroethane ND ug/L 03/10/23 19:34 67-72-103/09/23 13:5310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/23 19:34 193-39-503/09/23 13:5310.0 2.9 1
Isophorone ND ug/L 03/10/23 19:34 78-59-103/09/23 13:5310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/10/23 19:34 90-12-003/09/23 13:5310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/10/23 19:34 91-57-603/09/23 13:5310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/23 19:34 95-48-703/09/23 13:5310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/23 19:34 15831-10-403/09/23 13:5310.0 1.2 1
Naphthalene ND ug/L 03/10/23 19:34 91-20-303/09/23 13:5310.0 2.1 1
2-Nitroaniline ND ug/L 03/10/23 19:34 88-74-403/09/23 13:5320.0 3.0 1
3-Nitroaniline ND ug/L 03/10/23 19:34 99-09-203/09/23 13:5320.0 3.8 1
4-Nitroaniline ND ug/L 03/10/23 19:34 100-01-603/09/23 13:5320.0 5.1 1
Nitrobenzene ND ug/L 03/10/23 19:34 98-95-303/09/23 13:5310.0 1.9 1
2-Nitrophenol ND ug/L 03/10/23 19:34 88-75-5 v103/09/23 13:5310.0 1.4 1
4-Nitrophenol ND ug/L 03/10/23 19:34 100-02-703/09/23 13:5350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/10/23 19:34 62-75-9 v103/09/23 13:5310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/23 19:34 621-64-703/09/23 13:5310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/10/23 19:34 86-30-603/09/23 13:5310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/23 19:34 108-60-1 v103/09/23 13:5310.0 1.2 1
Pentachlorophenol ND ug/L 03/10/23 19:34 87-86-503/09/23 13:5320.0 3.8 1
Phenanthrene ND ug/L 03/10/23 19:34 85-01-803/09/23 13:5310.0 2.0 1
Phenol ND ug/L 03/10/23 19:34 108-95-203/09/23 13:5310.0 1.4 1
Pyrene ND ug/L 03/10/23 19:34 129-00-003/09/23 13:5310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/10/23 19:34 120-82-103/09/23 13:5310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/10/23 19:34 95-95-403/09/23 13:5310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/10/23 19:34 88-06-203/09/23 13:5310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)82 %03/10/23 19:34 4165-60-003/09/23 13:5310-138 1
2-Fluorobiphenyl (S)73 %03/10/23 19:34 321-60-803/09/23 13:5310-130 1
Terphenyl-d14 (S)93 %03/10/23 19:34 1718-51-003/09/23 13:5319-191 1
Phenol-d6 (S)49 %03/10/23 19:34 13127-88-303/09/23 13:5310-130 1
2-Fluorophenol (S)63 %03/10/23 19:34 367-12-403/09/23 13:5310-130 1
2,4,6-Tribromophenol (S)75 %03/10/23 19:34 118-79-603/09/23 13:5310-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-6 Lab ID: 92655680003 Collected: 03/07/23 16:35 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 03/09/23 22:51 67-64-125.0 5.1 1
Benzene ND ug/L 03/09/23 22:51 71-43-21.0 0.34 1
Bromobenzene ND ug/L 03/09/23 22:51 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 03/09/23 22:51 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 03/09/23 22:51 75-27-41.0 0.31 1
Bromoform ND ug/L 03/09/23 22:51 75-25-21.0 0.34 1
Bromomethane ND ug/L 03/09/23 22:51 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 03/09/23 22:51 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 03/09/23 22:51 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 03/09/23 22:51 108-90-71.0 0.28 1
Chloroethane ND ug/L 03/09/23 22:51 75-00-31.0 0.65 1
Chloroform 0.71J ug/L 03/09/23 22:51 67-66-31.0 0.43 1
Chloromethane ND ug/L 03/09/23 22:51 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 03/09/23 22:51 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 03/09/23 22:51 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 03/09/23 22:51 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 03/09/23 22:51 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 03/09/23 22:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/09/23 22:51 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 03/09/23 22:51 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 03/09/23 22:51 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 03/09/23 22:51 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/09/23 22:51 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 03/09/23 22:51 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 03/09/23 22:51 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 03/09/23 22:51 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 03/09/23 22:51 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 03/09/23 22:51 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 03/09/23 22:51 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 03/09/23 22:51 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/09/23 22:51 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 03/09/23 22:51 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 03/09/23 22:51 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 03/09/23 22:51 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 03/09/23 22:51 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 03/09/23 22:51 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/09/23 22:51 87-68-32.0 1.5 1
2-Hexanone ND ug/L 03/09/23 22:51 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 03/09/23 22:51 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 03/09/23 22:51 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/09/23 22:51 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 03/09/23 22:51 1634-04-41.0 0.42 1
Naphthalene ND ug/L 03/09/23 22:51 91-20-31.0 0.64 1
Styrene ND ug/L 03/09/23 22:51 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 03/09/23 22:51 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-6 Lab ID: 92655680003 Collected: 03/07/23 16:35 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 03/09/23 22:51 79-34-51.0 0.22 1
Tetrachloroethene 12.6 ug/L 03/09/23 22:51 127-18-41.0 0.29 1
Toluene ND ug/L 03/09/23 22:51 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/09/23 22:51 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 03/09/23 22:51 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 03/09/23 22:51 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 03/09/23 22:51 79-00-51.0 0.32 1
Trichloroethene 2.2 ug/L 03/09/23 22:51 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 03/09/23 22:51 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 03/09/23 22:51 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 03/09/23 22:51 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 03/09/23 22:51 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 03/09/23 22:51 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 03/09/23 22:51 179601-23-12.0 0.71 1
o-Xylene ND ug/L 03/09/23 22:51 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %03/09/23 22:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %03/09/23 22:51 17060-07-070-130 1
Toluene-d8 (S)102 %03/09/23 22:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-7 Lab ID: 92655680004 Collected: 03/06/23 16:15 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic 0.17J ug/L 03/14/23 18:22 7440-38-203/10/23 12:231.0 0.087 1
Barium 72.6 ug/L 03/14/23 18:22 7440-39-303/10/23 12:231.0 0.21 1
Cadmium ND ug/L 03/14/23 18:22 7440-43-903/10/23 12:230.20 0.060 1
Chromium ND ug/L 03/14/23 18:22 7440-47-303/10/23 12:231.0 0.50 1
Lead 0.091J ug/L 03/14/23 18:22 7439-92-103/10/23 12:231.0 0.077 1
Selenium 0.11J ug/L 03/14/23 18:22 7782-49-203/10/23 12:232.0 0.072 1
Silver ND ug/L 03/14/23 18:22 7440-22-403/10/23 12:230.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 03/13/23 10:26 7439-97-603/13/23 07:030.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/10/23 20:00 83-32-903/09/23 13:539.1 1.8 1
Acenaphthylene ND ug/L 03/10/23 20:00 208-96-803/09/23 13:539.1 1.8 1
Aniline ND ug/L 03/10/23 20:00 62-53-3 L203/09/23 13:539.1 1.5 1
Anthracene ND ug/L 03/10/23 20:00 120-12-703/09/23 13:539.1 2.1 1
Benzo(a)anthracene ND ug/L 03/10/23 20:00 56-55-303/09/23 13:539.1 2.4 1
Benzo(a)pyrene ND ug/L 03/10/23 20:00 50-32-803/09/23 13:539.1 2.5 1
Benzo(b)fluoranthene ND ug/L 03/10/23 20:00 205-99-203/09/23 13:539.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 03/10/23 20:00 191-24-203/09/23 13:539.1 2.6 1
Benzo(k)fluoranthene ND ug/L 03/10/23 20:00 207-08-903/09/23 13:539.1 2.5 1
Benzoic Acid ND ug/L 03/10/23 20:00 65-85-003/09/23 13:5345.5 20.0 1
Benzyl alcohol ND ug/L 03/10/23 20:00 100-51-603/09/23 13:5318.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 03/10/23 20:00 101-55-303/09/23 13:539.1 1.6 1
Butylbenzylphthalate ND ug/L 03/10/23 20:00 85-68-703/09/23 13:539.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 03/10/23 20:00 59-50-703/09/23 13:539.1 3.0 1
4-Chloroaniline ND ug/L 03/10/23 20:00 106-47-803/09/23 13:5318.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/23 20:00 111-91-103/09/23 13:539.1 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/23 20:00 111-44-403/09/23 13:539.1 1.7 1
2-Chloronaphthalene ND ug/L 03/10/23 20:00 91-58-703/09/23 13:539.1 1.6 1
2-Chlorophenol ND ug/L 03/10/23 20:00 95-57-803/09/23 13:539.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 03/10/23 20:00 7005-72-303/09/23 13:539.1 1.8 1
Chrysene ND ug/L 03/10/23 20:00 218-01-903/09/23 13:539.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 03/10/23 20:00 53-70-303/09/23 13:539.1 2.7 1
Dibenzofuran ND ug/L 03/10/23 20:00 132-64-903/09/23 13:539.1 1.9 1
1,2-Dichlorobenzene ND ug/L 03/10/23 20:00 95-50-103/09/23 13:539.1 1.6 1
1,3-Dichlorobenzene ND ug/L 03/10/23 20:00 541-73-103/09/23 13:539.1 1.5 1
1,4-Dichlorobenzene ND ug/L 03/10/23 20:00 106-46-703/09/23 13:539.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 03/10/23 20:00 91-94-103/09/23 13:5318.2 7.4 1
2,4-Dichlorophenol ND ug/L 03/10/23 20:00 120-83-203/09/23 13:539.1 1.3 1
Diethylphthalate ND ug/L 03/10/23 20:00 84-66-203/09/23 13:539.1 1.9 1
2,4-Dimethylphenol ND ug/L 03/10/23 20:00 105-67-903/09/23 13:539.1 1.5 1
Dimethylphthalate ND ug/L 03/10/23 20:00 131-11-303/09/23 13:539.1 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-7 Lab ID: 92655680004 Collected: 03/06/23 16:15 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 03/10/23 20:00 84-74-203/09/23 13:539.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/23 20:00 534-52-103/09/23 13:5318.2 7.1 1
2,4-Dinitrophenol ND ug/L 03/10/23 20:00 51-28-503/09/23 13:5345.5 23.6 1
2,4-Dinitrotoluene ND ug/L 03/10/23 20:00 121-14-203/09/23 13:539.1 1.5 1
2,6-Dinitrotoluene ND ug/L 03/10/23 20:00 606-20-203/09/23 13:539.1 1.6 1
Di-n-octylphthalate ND ug/L 03/10/23 20:00 117-84-003/09/23 13:539.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/23 20:00 117-81-703/09/23 13:535.5 3.4 1
Fluoranthene ND ug/L 03/10/23 20:00 206-44-003/09/23 13:539.1 2.0 1
Fluorene ND ug/L 03/10/23 20:00 86-73-703/09/23 13:539.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 03/10/23 20:00 87-68-303/09/23 13:539.1 1.6 1
Hexachlorobenzene ND ug/L 03/10/23 20:00 118-74-103/09/23 13:539.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 03/10/23 20:00 77-47-403/09/23 13:539.1 1.4 1
Hexachloroethane ND ug/L 03/10/23 20:00 67-72-103/09/23 13:539.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/23 20:00 193-39-503/09/23 13:539.1 2.6 1
Isophorone ND ug/L 03/10/23 20:00 78-59-103/09/23 13:539.1 1.5 1
1-Methylnaphthalene ND ug/L 03/10/23 20:00 90-12-003/09/23 13:539.1 1.8 1
2-Methylnaphthalene ND ug/L 03/10/23 20:00 91-57-603/09/23 13:539.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/23 20:00 95-48-703/09/23 13:539.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/23 20:00 15831-10-403/09/23 13:539.1 1.1 1
Naphthalene ND ug/L 03/10/23 20:00 91-20-303/09/23 13:539.1 1.9 1
2-Nitroaniline ND ug/L 03/10/23 20:00 88-74-403/09/23 13:5318.2 2.7 1
3-Nitroaniline ND ug/L 03/10/23 20:00 99-09-203/09/23 13:5318.2 3.4 1
4-Nitroaniline ND ug/L 03/10/23 20:00 100-01-603/09/23 13:5318.2 4.6 1
Nitrobenzene ND ug/L 03/10/23 20:00 98-95-303/09/23 13:539.1 1.7 1
2-Nitrophenol ND ug/L 03/10/23 20:00 88-75-5 v103/09/23 13:539.1 1.3 1
4-Nitrophenol ND ug/L 03/10/23 20:00 100-02-703/09/23 13:5345.5 6.0 1
N-Nitrosodimethylamine ND ug/L 03/10/23 20:00 62-75-9 v103/09/23 13:539.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/23 20:00 621-64-703/09/23 13:539.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 03/10/23 20:00 86-30-603/09/23 13:539.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/23 20:00 108-60-1 v103/09/23 13:539.1 1.0 1
Pentachlorophenol ND ug/L 03/10/23 20:00 87-86-503/09/23 13:5318.2 3.4 1
Phenanthrene ND ug/L 03/10/23 20:00 85-01-803/09/23 13:539.1 1.8 1
Phenol ND ug/L 03/10/23 20:00 108-95-203/09/23 13:539.1 1.2 1
Pyrene ND ug/L 03/10/23 20:00 129-00-003/09/23 13:539.1 2.0 1
1,2,4-Trichlorobenzene ND ug/L 03/10/23 20:00 120-82-103/09/23 13:539.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 03/10/23 20:00 95-95-403/09/23 13:539.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 03/10/23 20:00 88-06-203/09/23 13:539.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)83 %03/10/23 20:00 4165-60-003/09/23 13:5310-138 1
2-Fluorobiphenyl (S)79 %03/10/23 20:00 321-60-803/09/23 13:5310-130 1
Terphenyl-d14 (S)107 %03/10/23 20:00 1718-51-003/09/23 13:5319-191 1
Phenol-d6 (S)49 %03/10/23 20:00 13127-88-303/09/23 13:5310-130 1
2-Fluorophenol (S)60 %03/10/23 20:00 367-12-403/09/23 13:5310-130 1
2,4,6-Tribromophenol (S)87 %03/10/23 20:00 118-79-603/09/23 13:5310-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-7 Lab ID: 92655680004 Collected: 03/06/23 16:15 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 03/09/23 00:44 67-64-125.0 5.1 1
Benzene ND ug/L 03/09/23 00:44 71-43-21.0 0.34 1
Bromobenzene ND ug/L 03/09/23 00:44 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 03/09/23 00:44 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 03/09/23 00:44 75-27-41.0 0.31 1
Bromoform ND ug/L 03/09/23 00:44 75-25-21.0 0.34 1
Bromomethane ND ug/L 03/09/23 00:44 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 03/09/23 00:44 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 03/09/23 00:44 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 03/09/23 00:44 108-90-71.0 0.28 1
Chloroethane ND ug/L 03/09/23 00:44 75-00-31.0 0.65 1
Chloroform ND ug/L 03/09/23 00:44 67-66-31.0 0.43 1
Chloromethane ND ug/L 03/09/23 00:44 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 03/09/23 00:44 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 03/09/23 00:44 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 03/09/23 00:44 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 03/09/23 00:44 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 03/09/23 00:44 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/09/23 00:44 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 03/09/23 00:44 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 03/09/23 00:44 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 03/09/23 00:44 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/09/23 00:44 75-71-8 IH1.0 0.35 1
1,1-Dichloroethane ND ug/L 03/09/23 00:44 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 03/09/23 00:44 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 03/09/23 00:44 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 03/09/23 00:44 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 03/09/23 00:44 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 03/09/23 00:44 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 03/09/23 00:44 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/09/23 00:44 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 03/09/23 00:44 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 03/09/23 00:44 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 03/09/23 00:44 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 03/09/23 00:44 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 03/09/23 00:44 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/09/23 00:44 87-68-32.0 1.5 1
2-Hexanone ND ug/L 03/09/23 00:44 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 03/09/23 00:44 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 03/09/23 00:44 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/09/23 00:44 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 03/09/23 00:44 1634-04-41.0 0.42 1
Naphthalene ND ug/L 03/09/23 00:44 91-20-31.0 0.64 1
Styrene ND ug/L 03/09/23 00:44 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 03/09/23 00:44 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: OFF-MW-7 Lab ID: 92655680004 Collected: 03/06/23 16:15 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 03/09/23 00:44 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 03/09/23 00:44 127-18-41.0 0.29 1
Toluene ND ug/L 03/09/23 00:44 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/09/23 00:44 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 03/09/23 00:44 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 03/09/23 00:44 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 03/09/23 00:44 79-00-51.0 0.32 1
Trichloroethene ND ug/L 03/09/23 00:44 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 03/09/23 00:44 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 03/09/23 00:44 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 03/09/23 00:44 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 03/09/23 00:44 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 03/09/23 00:44 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 03/09/23 00:44 179601-23-12.0 0.71 1
o-Xylene ND ug/L 03/09/23 00:44 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %03/09/23 00:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %03/09/23 00:44 17060-07-070-130 1
Toluene-d8 (S)100 %03/09/23 00:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: MW-11S Lab ID: 92655680005 Collected: 03/06/23 13:05 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic 0.20J ug/L 03/14/23 18:26 7440-38-203/10/23 12:231.0 0.087 1
Barium 17.0 ug/L 03/14/23 18:26 7440-39-303/10/23 12:231.0 0.21 1
Cadmium ND ug/L 03/14/23 18:26 7440-43-903/10/23 12:230.20 0.060 1
Chromium 0.82J ug/L 03/14/23 18:26 7440-47-303/10/23 12:231.0 0.50 1
Lead 0.18J ug/L 03/14/23 18:26 7439-92-103/10/23 12:231.0 0.077 1
Selenium 0.13J ug/L 03/14/23 18:26 7782-49-203/10/23 12:232.0 0.072 1
Silver ND ug/L 03/14/23 18:26 7440-22-403/10/23 12:230.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 03/13/23 10:29 7439-97-603/13/23 07:030.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/10/23 20:25 83-32-903/09/23 13:5310.0 2.0 1
Acenaphthylene ND ug/L 03/10/23 20:25 208-96-803/09/23 13:5310.0 2.0 1
Aniline ND ug/L 03/10/23 20:25 62-53-3 L203/09/23 13:5310.0 1.6 1
Anthracene ND ug/L 03/10/23 20:25 120-12-703/09/23 13:5310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/10/23 20:25 56-55-303/09/23 13:5310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/10/23 20:25 50-32-803/09/23 13:5310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/10/23 20:25 205-99-203/09/23 13:5310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/10/23 20:25 191-24-203/09/23 13:5310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/10/23 20:25 207-08-903/09/23 13:5310.0 2.7 1
Benzoic Acid ND ug/L 03/10/23 20:25 65-85-003/09/23 13:5350.0 22.0 1
Benzyl alcohol ND ug/L 03/10/23 20:25 100-51-603/09/23 13:5320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/10/23 20:25 101-55-303/09/23 13:5310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/10/23 20:25 85-68-703/09/23 13:5310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/10/23 20:25 59-50-703/09/23 13:5310.0 3.3 1
4-Chloroaniline ND ug/L 03/10/23 20:25 106-47-803/09/23 13:5320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/23 20:25 111-91-103/09/23 13:5310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/10/23 20:25 111-44-403/09/23 13:5310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/10/23 20:25 91-58-703/09/23 13:5310.0 1.7 1
2-Chlorophenol ND ug/L 03/10/23 20:25 95-57-803/09/23 13:5310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/10/23 20:25 7005-72-303/09/23 13:5310.0 2.0 1
Chrysene ND ug/L 03/10/23 20:25 218-01-903/09/23 13:5310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/10/23 20:25 53-70-303/09/23 13:5310.0 3.0 1
Dibenzofuran ND ug/L 03/10/23 20:25 132-64-903/09/23 13:5310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/10/23 20:25 95-50-103/09/23 13:5310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/10/23 20:25 541-73-103/09/23 13:5310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/10/23 20:25 106-46-703/09/23 13:5310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/10/23 20:25 91-94-103/09/23 13:5320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/10/23 20:25 120-83-203/09/23 13:5310.0 1.4 1
Diethylphthalate ND ug/L 03/10/23 20:25 84-66-203/09/23 13:5310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/10/23 20:25 105-67-903/09/23 13:5310.0 1.7 1
Dimethylphthalate ND ug/L 03/10/23 20:25 131-11-303/09/23 13:5310.0 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: MW-11S Lab ID: 92655680005 Collected: 03/06/23 13:05 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 03/10/23 20:25 84-74-203/09/23 13:5310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/23 20:25 534-52-103/09/23 13:5320.0 7.8 1
2,4-Dinitrophenol ND ug/L 03/10/23 20:25 51-28-503/09/23 13:5350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/10/23 20:25 121-14-203/09/23 13:5310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/10/23 20:25 606-20-203/09/23 13:5310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/23 20:25 117-84-003/09/23 13:5310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/23 20:25 117-81-703/09/23 13:536.0 3.7 1
Fluoranthene ND ug/L 03/10/23 20:25 206-44-003/09/23 13:5310.0 2.2 1
Fluorene ND ug/L 03/10/23 20:25 86-73-703/09/23 13:5310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/10/23 20:25 87-68-303/09/23 13:5310.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/23 20:25 118-74-103/09/23 13:5310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/10/23 20:25 77-47-403/09/23 13:5310.0 1.6 1
Hexachloroethane ND ug/L 03/10/23 20:25 67-72-103/09/23 13:5310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/23 20:25 193-39-503/09/23 13:5310.0 2.9 1
Isophorone ND ug/L 03/10/23 20:25 78-59-103/09/23 13:5310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/10/23 20:25 90-12-003/09/23 13:5310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/10/23 20:25 91-57-603/09/23 13:5310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/23 20:25 95-48-703/09/23 13:5310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/23 20:25 15831-10-403/09/23 13:5310.0 1.2 1
Naphthalene ND ug/L 03/10/23 20:25 91-20-303/09/23 13:5310.0 2.1 1
2-Nitroaniline ND ug/L 03/10/23 20:25 88-74-403/09/23 13:5320.0 3.0 1
3-Nitroaniline ND ug/L 03/10/23 20:25 99-09-203/09/23 13:5320.0 3.8 1
4-Nitroaniline ND ug/L 03/10/23 20:25 100-01-603/09/23 13:5320.0 5.1 1
Nitrobenzene ND ug/L 03/10/23 20:25 98-95-303/09/23 13:5310.0 1.9 1
2-Nitrophenol ND ug/L 03/10/23 20:25 88-75-5 v103/09/23 13:5310.0 1.4 1
4-Nitrophenol ND ug/L 03/10/23 20:25 100-02-703/09/23 13:5350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/10/23 20:25 62-75-9 v103/09/23 13:5310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/23 20:25 621-64-703/09/23 13:5310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/10/23 20:25 86-30-603/09/23 13:5310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/23 20:25 108-60-1 v103/09/23 13:5310.0 1.2 1
Pentachlorophenol ND ug/L 03/10/23 20:25 87-86-503/09/23 13:5320.0 3.8 1
Phenanthrene ND ug/L 03/10/23 20:25 85-01-803/09/23 13:5310.0 2.0 1
Phenol ND ug/L 03/10/23 20:25 108-95-203/09/23 13:5310.0 1.4 1
Pyrene ND ug/L 03/10/23 20:25 129-00-003/09/23 13:5310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/10/23 20:25 120-82-103/09/23 13:5310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/10/23 20:25 95-95-403/09/23 13:5310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/10/23 20:25 88-06-203/09/23 13:5310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)77 %03/10/23 20:25 4165-60-003/09/23 13:5310-138 1
2-Fluorobiphenyl (S)71 %03/10/23 20:25 321-60-803/09/23 13:5310-130 1
Terphenyl-d14 (S)101 %03/10/23 20:25 1718-51-003/09/23 13:5319-191 1
Phenol-d6 (S)65 %03/10/23 20:25 13127-88-303/09/23 13:5310-130 1
2-Fluorophenol (S)72 %03/10/23 20:25 367-12-403/09/23 13:5310-130 1
2,4,6-Tribromophenol (S)79 %03/10/23 20:25 118-79-603/09/23 13:5310-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: MW-11S Lab ID: 92655680005 Collected: 03/06/23 13:05 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 03/09/23 01:02 67-64-125.0 5.1 1
Benzene ND ug/L 03/09/23 01:02 71-43-21.0 0.34 1
Bromobenzene ND ug/L 03/09/23 01:02 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 03/09/23 01:02 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 03/09/23 01:02 75-27-41.0 0.31 1
Bromoform ND ug/L 03/09/23 01:02 75-25-21.0 0.34 1
Bromomethane ND ug/L 03/09/23 01:02 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 03/09/23 01:02 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 03/09/23 01:02 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 03/09/23 01:02 108-90-71.0 0.28 1
Chloroethane ND ug/L 03/09/23 01:02 75-00-31.0 0.65 1
Chloroform ND ug/L 03/09/23 01:02 67-66-31.0 0.43 1
Chloromethane ND ug/L 03/09/23 01:02 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 03/09/23 01:02 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 03/09/23 01:02 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 03/09/23 01:02 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 03/09/23 01:02 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 03/09/23 01:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/09/23 01:02 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 03/09/23 01:02 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 03/09/23 01:02 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 03/09/23 01:02 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/09/23 01:02 75-71-8 IH1.0 0.35 1
1,1-Dichloroethane ND ug/L 03/09/23 01:02 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 03/09/23 01:02 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 03/09/23 01:02 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 03/09/23 01:02 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 03/09/23 01:02 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 03/09/23 01:02 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 03/09/23 01:02 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/09/23 01:02 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 03/09/23 01:02 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 03/09/23 01:02 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 03/09/23 01:02 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 03/09/23 01:02 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 03/09/23 01:02 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/09/23 01:02 87-68-32.0 1.5 1
2-Hexanone ND ug/L 03/09/23 01:02 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 03/09/23 01:02 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 03/09/23 01:02 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/09/23 01:02 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 03/09/23 01:02 1634-04-41.0 0.42 1
Naphthalene ND ug/L 03/09/23 01:02 91-20-31.0 0.64 1
Styrene ND ug/L 03/09/23 01:02 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 03/09/23 01:02 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: MW-11S Lab ID: 92655680005 Collected: 03/06/23 13:05 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 03/09/23 01:02 79-34-51.0 0.22 1
Tetrachloroethene 1.2 ug/L 03/09/23 01:02 127-18-41.0 0.29 1
Toluene ND ug/L 03/09/23 01:02 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/09/23 01:02 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 03/09/23 01:02 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 03/09/23 01:02 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 03/09/23 01:02 79-00-51.0 0.32 1
Trichloroethene ND ug/L 03/09/23 01:02 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 03/09/23 01:02 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 03/09/23 01:02 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 03/09/23 01:02 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 03/09/23 01:02 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 03/09/23 01:02 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 03/09/23 01:02 179601-23-12.0 0.71 1
o-Xylene ND ug/L 03/09/23 01:02 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %03/09/23 01:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %03/09/23 01:02 17060-07-070-130 1
Toluene-d8 (S)98 %03/09/23 01:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: GW-DUP Lab ID: 92655680006 Collected: 03/06/23 00:00 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic ND ug/L 03/14/23 18:30 7440-38-203/10/23 12:231.0 0.087 1
Barium 61.4 ug/L 03/14/23 18:30 7440-39-303/10/23 12:231.0 0.21 1
Cadmium ND ug/L 03/14/23 18:30 7440-43-903/10/23 12:230.20 0.060 1
Chromium 4.1 ug/L 03/14/23 18:30 7440-47-303/10/23 12:231.0 0.50 1
Lead ND ug/L 03/14/23 18:30 7439-92-103/10/23 12:231.0 0.077 1
Selenium ND ug/L 03/14/23 18:30 7782-49-203/10/23 12:232.0 0.072 1
Silver ND ug/L 03/14/23 18:30 7440-22-403/10/23 12:230.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 03/13/23 10:31 7439-97-603/13/23 07:030.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/10/23 20:50 83-32-903/09/23 13:538.3 1.7 1
Acenaphthylene ND ug/L 03/10/23 20:50 208-96-803/09/23 13:538.3 1.6 1
Aniline ND ug/L 03/10/23 20:50 62-53-3 L203/09/23 13:538.3 1.4 1
Anthracene ND ug/L 03/10/23 20:50 120-12-703/09/23 13:538.3 1.9 1
Benzo(a)anthracene ND ug/L 03/10/23 20:50 56-55-303/09/23 13:538.3 2.2 1
Benzo(a)pyrene ND ug/L 03/10/23 20:50 50-32-803/09/23 13:538.3 2.3 1
Benzo(b)fluoranthene ND ug/L 03/10/23 20:50 205-99-203/09/23 13:538.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 03/10/23 20:50 191-24-203/09/23 13:538.3 2.4 1
Benzo(k)fluoranthene ND ug/L 03/10/23 20:50 207-08-903/09/23 13:538.3 2.3 1
Benzoic Acid ND ug/L 03/10/23 20:50 65-85-003/09/23 13:5341.7 18.3 1
Benzyl alcohol ND ug/L 03/10/23 20:50 100-51-603/09/23 13:5316.7 2.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/23 20:50 101-55-303/09/23 13:538.3 1.5 1
Butylbenzylphthalate ND ug/L 03/10/23 20:50 85-68-703/09/23 13:538.3 2.6 1
4-Chloro-3-methylphenol ND ug/L 03/10/23 20:50 59-50-703/09/23 13:538.3 2.8 1
4-Chloroaniline ND ug/L 03/10/23 20:50 106-47-803/09/23 13:5316.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/23 20:50 111-91-103/09/23 13:538.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 03/10/23 20:50 111-44-403/09/23 13:538.3 1.6 1
2-Chloronaphthalene ND ug/L 03/10/23 20:50 91-58-703/09/23 13:538.3 1.4 1
2-Chlorophenol ND ug/L 03/10/23 20:50 95-57-803/09/23 13:538.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 03/10/23 20:50 7005-72-303/09/23 13:538.3 1.7 1
Chrysene ND ug/L 03/10/23 20:50 218-01-903/09/23 13:538.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 03/10/23 20:50 53-70-303/09/23 13:538.3 2.5 1
Dibenzofuran ND ug/L 03/10/23 20:50 132-64-903/09/23 13:538.3 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/23 20:50 95-50-103/09/23 13:538.3 1.5 1
1,3-Dichlorobenzene ND ug/L 03/10/23 20:50 541-73-103/09/23 13:538.3 1.3 1
1,4-Dichlorobenzene ND ug/L 03/10/23 20:50 106-46-703/09/23 13:538.3 1.4 1
3,3'-Dichlorobenzidine ND ug/L 03/10/23 20:50 91-94-103/09/23 13:5316.7 6.8 1
2,4-Dichlorophenol ND ug/L 03/10/23 20:50 120-83-203/09/23 13:538.3 1.2 1
Diethylphthalate ND ug/L 03/10/23 20:50 84-66-203/09/23 13:538.3 1.7 1
2,4-Dimethylphenol ND ug/L 03/10/23 20:50 105-67-903/09/23 13:538.3 1.4 1
Dimethylphthalate ND ug/L 03/10/23 20:50 131-11-303/09/23 13:538.3 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: GW-DUP Lab ID: 92655680006 Collected: 03/06/23 00:00 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 03/10/23 20:50 84-74-203/09/23 13:538.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/23 20:50 534-52-103/09/23 13:5316.7 6.5 1
2,4-Dinitrophenol ND ug/L 03/10/23 20:50 51-28-503/09/23 13:5341.7 21.7 1
2,4-Dinitrotoluene ND ug/L 03/10/23 20:50 121-14-203/09/23 13:538.3 1.4 1
2,6-Dinitrotoluene ND ug/L 03/10/23 20:50 606-20-203/09/23 13:538.3 1.4 1
Di-n-octylphthalate ND ug/L 03/10/23 20:50 117-84-003/09/23 13:538.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/23 20:50 117-81-703/09/23 13:535.0 3.1 1
Fluoranthene ND ug/L 03/10/23 20:50 206-44-003/09/23 13:538.3 1.8 1
Fluorene ND ug/L 03/10/23 20:50 86-73-703/09/23 13:538.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 03/10/23 20:50 87-68-303/09/23 13:538.3 1.5 1
Hexachlorobenzene ND ug/L 03/10/23 20:50 118-74-103/09/23 13:538.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 03/10/23 20:50 77-47-403/09/23 13:538.3 1.3 1
Hexachloroethane ND ug/L 03/10/23 20:50 67-72-103/09/23 13:538.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/23 20:50 193-39-503/09/23 13:538.3 2.4 1
Isophorone ND ug/L 03/10/23 20:50 78-59-103/09/23 13:538.3 1.4 1
1-Methylnaphthalene ND ug/L 03/10/23 20:50 90-12-003/09/23 13:538.3 1.7 1
2-Methylnaphthalene ND ug/L 03/10/23 20:50 91-57-603/09/23 13:538.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/23 20:50 95-48-703/09/23 13:538.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/23 20:50 15831-10-403/09/23 13:538.3 1.0 1
Naphthalene ND ug/L 03/10/23 20:50 91-20-303/09/23 13:538.3 1.7 1
2-Nitroaniline ND ug/L 03/10/23 20:50 88-74-403/09/23 13:5316.7 2.5 1
3-Nitroaniline ND ug/L 03/10/23 20:50 99-09-203/09/23 13:5316.7 3.1 1
4-Nitroaniline ND ug/L 03/10/23 20:50 100-01-603/09/23 13:5316.7 4.2 1
Nitrobenzene ND ug/L 03/10/23 20:50 98-95-303/09/23 13:538.3 1.6 1
2-Nitrophenol ND ug/L 03/10/23 20:50 88-75-5 v103/09/23 13:538.3 1.2 1
4-Nitrophenol ND ug/L 03/10/23 20:50 100-02-703/09/23 13:5341.7 5.5 1
N-Nitrosodimethylamine ND ug/L 03/10/23 20:50 62-75-9 v103/09/23 13:538.3 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/23 20:50 621-64-703/09/23 13:538.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/23 20:50 86-30-603/09/23 13:538.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/23 20:50 108-60-1 v103/09/23 13:538.3 0.96 1
Pentachlorophenol ND ug/L 03/10/23 20:50 87-86-503/09/23 13:5316.7 3.1 1
Phenanthrene ND ug/L 03/10/23 20:50 85-01-803/09/23 13:538.3 1.7 1
Phenol ND ug/L 03/10/23 20:50 108-95-203/09/23 13:538.3 1.1 1
Pyrene ND ug/L 03/10/23 20:50 129-00-003/09/23 13:538.3 1.8 1
1,2,4-Trichlorobenzene ND ug/L 03/10/23 20:50 120-82-103/09/23 13:538.3 1.4 1
2,4,5-Trichlorophenol ND ug/L 03/10/23 20:50 95-95-403/09/23 13:538.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/23 20:50 88-06-203/09/23 13:538.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)102 %03/10/23 20:50 4165-60-003/09/23 13:5310-138 1
2-Fluorobiphenyl (S)90 %03/10/23 20:50 321-60-803/09/23 13:5310-130 1
Terphenyl-d14 (S)115 %03/10/23 20:50 1718-51-003/09/23 13:5319-191 1
Phenol-d6 (S)50 %03/10/23 20:50 13127-88-303/09/23 13:5310-130 1
2-Fluorophenol (S)66 %03/10/23 20:50 367-12-403/09/23 13:5310-130 1
2,4,6-Tribromophenol (S)86 %03/10/23 20:50 118-79-603/09/23 13:5310-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: GW-DUP Lab ID: 92655680006 Collected: 03/06/23 00:00 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 03/09/23 23:27 67-64-150.0 10.2 2
Benzene ND ug/L 03/09/23 23:27 71-43-22.0 0.69 2
Bromobenzene ND ug/L 03/09/23 23:27 108-86-12.0 0.58 2
Bromochloromethane ND ug/L 03/09/23 23:27 74-97-52.0 0.94 2
Bromodichloromethane ND ug/L 03/09/23 23:27 75-27-42.0 0.61 2
Bromoform ND ug/L 03/09/23 23:27 75-25-22.0 0.68 2
Bromomethane ND ug/L 03/09/23 23:27 74-83-94.0 3.3 2
2-Butanone (MEK)ND ug/L 03/09/23 23:27 78-93-310.0 7.9 2
Carbon tetrachloride ND ug/L 03/09/23 23:27 56-23-52.0 0.67 2
Chlorobenzene ND ug/L 03/09/23 23:27 108-90-72.0 0.57 2
Chloroethane ND ug/L 03/09/23 23:27 75-00-32.0 1.3 2
Chloroform ND ug/L 03/09/23 23:27 67-66-32.0 0.86 2
Chloromethane ND ug/L 03/09/23 23:27 74-87-32.0 1.1 2
2-Chlorotoluene ND ug/L 03/09/23 23:27 95-49-82.0 0.64 2
4-Chlorotoluene ND ug/L 03/09/23 23:27 106-43-42.0 0.65 2
1,2-Dibromo-3-chloropropane ND ug/L 03/09/23 23:27 96-12-84.0 0.68 2
Dibromochloromethane ND ug/L 03/09/23 23:27 124-48-12.0 0.72 2
1,2-Dibromoethane (EDB)ND ug/L 03/09/23 23:27 106-93-42.0 0.54 2
Dibromomethane ND ug/L 03/09/23 23:27 74-95-32.0 0.79 2
1,2-Dichlorobenzene ND ug/L 03/09/23 23:27 95-50-12.0 0.68 2
1,3-Dichlorobenzene ND ug/L 03/09/23 23:27 541-73-12.0 0.68 2
1,4-Dichlorobenzene ND ug/L 03/09/23 23:27 106-46-72.0 0.67 2
Dichlorodifluoromethane ND ug/L 03/09/23 23:27 75-71-82.0 0.69 2
1,1-Dichloroethane ND ug/L 03/09/23 23:27 75-34-32.0 0.73 2
1,2-Dichloroethane ND ug/L 03/09/23 23:27 107-06-22.0 0.64 2
1,1-Dichloroethene ND ug/L 03/09/23 23:27 75-35-42.0 0.70 2
cis-1,2-Dichloroethene ND ug/L 03/09/23 23:27 156-59-22.0 0.77 2
trans-1,2-Dichloroethene ND ug/L 03/09/23 23:27 156-60-52.0 0.79 2
1,2-Dichloropropane ND ug/L 03/09/23 23:27 78-87-52.0 0.71 2
1,3-Dichloropropane ND ug/L 03/09/23 23:27 142-28-92.0 0.57 2
2,2-Dichloropropane ND ug/L 03/09/23 23:27 594-20-72.0 0.78 2
1,1-Dichloropropene ND ug/L 03/09/23 23:27 563-58-62.0 0.85 2
cis-1,3-Dichloropropene ND ug/L 03/09/23 23:27 10061-01-52.0 0.73 2
trans-1,3-Dichloropropene ND ug/L 03/09/23 23:27 10061-02-62.0 0.73 2
Diisopropyl ether ND ug/L 03/09/23 23:27 108-20-32.0 0.62 2
Ethylbenzene ND ug/L 03/09/23 23:27 100-41-42.0 0.61 2
Hexachloro-1,3-butadiene ND ug/L 03/09/23 23:27 87-68-34.0 3.1 2
2-Hexanone ND ug/L 03/09/23 23:27 591-78-610.0 0.95 2
p-Isopropyltoluene ND ug/L 03/09/23 23:27 99-87-62.0 0.83 2
Methylene Chloride ND ug/L 03/09/23 23:27 75-09-210.0 3.9 2
4-Methyl-2-pentanone (MIBK)ND ug/L 03/09/23 23:27 108-10-110.0 5.4 2
Methyl-tert-butyl ether ND ug/L 03/09/23 23:27 1634-04-42.0 0.84 2
Naphthalene ND ug/L 03/09/23 23:27 91-20-32.0 1.3 2
Styrene ND ug/L 03/09/23 23:27 100-42-52.0 0.58 2
1,1,1,2-Tetrachloroethane ND ug/L 03/09/23 23:27 630-20-62.0 0.62 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: GW-DUP Lab ID: 92655680006 Collected: 03/06/23 00:00 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 03/09/23 23:27 79-34-52.0 0.45 2
Tetrachloroethene 190 ug/L 03/09/23 23:27 127-18-42.0 0.58 2
Toluene ND ug/L 03/09/23 23:27 108-88-32.0 0.48 2
1,2,3-Trichlorobenzene ND ug/L 03/09/23 23:27 87-61-62.0 1.6 2
1,2,4-Trichlorobenzene ND ug/L 03/09/23 23:27 120-82-12.0 1.3 2
1,1,1-Trichloroethane ND ug/L 03/09/23 23:27 71-55-62.0 0.66 2
1,1,2-Trichloroethane ND ug/L 03/09/23 23:27 79-00-52.0 0.65 2
Trichloroethene ND ug/L 03/09/23 23:27 79-01-62.0 0.77 2
Trichlorofluoromethane ND ug/L 03/09/23 23:27 75-69-42.0 0.60 2
1,2,3-Trichloropropane ND ug/L 03/09/23 23:27 96-18-42.0 0.52 2
Vinyl acetate ND ug/L 03/09/23 23:27 108-05-44.0 2.6 2
Vinyl chloride ND ug/L 03/09/23 23:27 75-01-42.0 0.77 2
Xylene (Total)ND ug/L 03/09/23 23:27 1330-20-72.0 0.68 2
m&p-Xylene ND ug/L 03/09/23 23:27 179601-23-14.0 1.4 2
o-Xylene ND ug/L 03/09/23 23:27 95-47-62.0 0.68 2
Surrogates
4-Bromofluorobenzene (S)104 %03/09/23 23:27 460-00-470-130 2
1,2-Dichloroethane-d4 (S)99 %03/09/23 23:27 17060-07-070-130 2
Toluene-d8 (S)104 %03/09/23 23:27 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: TRIP BLANK Lab ID: 92655680007 Collected: 03/06/23 00:00 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 03/08/23 22:55 67-64-125.0 5.1 1
Benzene ND ug/L 03/08/23 22:55 71-43-21.0 0.34 1
Bromobenzene ND ug/L 03/08/23 22:55 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 03/08/23 22:55 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 03/08/23 22:55 75-27-41.0 0.31 1
Bromoform ND ug/L 03/08/23 22:55 75-25-21.0 0.34 1
Bromomethane ND ug/L 03/08/23 22:55 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 03/08/23 22:55 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 03/08/23 22:55 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 03/08/23 22:55 108-90-71.0 0.28 1
Chloroethane ND ug/L 03/08/23 22:55 75-00-31.0 0.65 1
Chloroform ND ug/L 03/08/23 22:55 67-66-31.0 0.43 1
Chloromethane ND ug/L 03/08/23 22:55 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 03/08/23 22:55 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 03/08/23 22:55 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 03/08/23 22:55 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 03/08/23 22:55 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 03/08/23 22:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/08/23 22:55 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 03/08/23 22:55 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 03/08/23 22:55 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 03/08/23 22:55 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/08/23 22:55 75-71-8 IH1.0 0.35 1
1,1-Dichloroethane ND ug/L 03/08/23 22:55 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 03/08/23 22:55 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 03/08/23 22:55 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 03/08/23 22:55 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 03/08/23 22:55 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 03/08/23 22:55 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 03/08/23 22:55 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/08/23 22:55 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 03/08/23 22:55 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 03/08/23 22:55 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 03/08/23 22:55 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 03/08/23 22:55 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 03/08/23 22:55 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/08/23 22:55 87-68-32.0 1.5 1
2-Hexanone ND ug/L 03/08/23 22:55 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 03/08/23 22:55 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 03/08/23 22:55 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/08/23 22:55 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 03/08/23 22:55 1634-04-41.0 0.42 1
Naphthalene ND ug/L 03/08/23 22:55 91-20-31.0 0.64 1
Styrene ND ug/L 03/08/23 22:55 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 03/08/23 22:55 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Sample: TRIP BLANK Lab ID: 92655680007 Collected: 03/06/23 00:00 Received: 03/08/23 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 03/08/23 22:55 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 03/08/23 22:55 127-18-41.0 0.29 1
Toluene ND ug/L 03/08/23 22:55 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/08/23 22:55 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 03/08/23 22:55 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 03/08/23 22:55 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 03/08/23 22:55 79-00-51.0 0.32 1
Trichloroethene ND ug/L 03/08/23 22:55 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 03/08/23 22:55 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 03/08/23 22:55 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 03/08/23 22:55 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 03/08/23 22:55 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 03/08/23 22:55 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 03/08/23 22:55 179601-23-12.0 0.71 1
o-Xylene ND ug/L 03/08/23 22:55 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %03/08/23 22:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %03/08/23 22:55 17060-07-070-130 1
Toluene-d8 (S)98 %03/08/23 22:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760869
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92655680001, 92655680002, 92655680003, 92655680004, 92655680005, 92655680006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3952303
Associated Lab Samples:92655680001, 92655680002, 92655680003, 92655680004, 92655680005, 92655680006
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 03/13/23 10:060.12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3952304LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.92.5 114 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3952305MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655680001
3952306
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 112 75-125107 5 252.5ND 2.8 2.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760673
EPA 3010A
EPA 6020B
6020 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92655680001, 92655680002, 92655680003, 92655680004, 92655680005, 92655680006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3951289
Associated Lab Samples:92655680001, 92655680002, 92655680003, 92655680004, 92655680005, 92655680006
Matrix: Water
AnalyzedMDL
Arsenic ug/L ND 1.0 03/14/23 17:360.087
Barium ug/L ND 1.0 03/14/23 17:360.21
Cadmium ug/L ND 0.20 03/14/23 17:360.060
Chromium ug/L ND 1.0 03/14/23 17:360.50
Lead ug/L ND 1.0 03/14/23 17:360.077
Selenium ug/L ND 2.0 03/14/23 17:360.072
Silver ug/L ND 0.40 03/14/23 17:360.070
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3951290LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 50.950 102 80-120
Barium ug/L 51.750 103 80-120
Cadmium ug/L 51.450 103 80-120
Chromium ug/L 52.650 105 80-120
Lead ug/L 51.250 102 80-120
Selenium ug/L 51.850 104 80-120
Silver ug/L 25.425 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3951291MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655319005
3951292
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 50 102 75-125103 1 20500.37J 51.2 51.7
Barium ug/L 50 105 75-125108 2 205028.4 80.7 82.5
Cadmium ug/L 50 100 75-125100 0 2050ND50.0 49.8
Chromium ug/L 50 104 75-125104 0 20500.60J 52.5 52.7
Lead ug/L 50 102 75-125101 0 20500.32J 51.1 51.0
Selenium ug/L 50 101 75-125101 0 2050ND50.7 50.6
Silver ug/L 25 99 75-12598 1 2025ND24.7 24.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760191
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92655680004, 92655680005, 92655680007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3948359
Associated Lab Samples:92655680004, 92655680005, 92655680007
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/08/23 22:190.31
1,1,1-Trichloroethane ug/L ND 1.0 03/08/23 22:190.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/08/23 22:190.22
1,1,2-Trichloroethane ug/L ND 1.0 03/08/23 22:190.32
1,1-Dichloroethane ug/L ND 1.0 03/08/23 22:190.37
1,1-Dichloroethene ug/L ND 1.0 03/08/23 22:190.35
1,1-Dichloropropene ug/L ND 1.0 03/08/23 22:190.43
1,2,3-Trichlorobenzene ug/L ND 1.0 03/08/23 22:190.81
1,2,3-Trichloropropane ug/L ND 1.0 03/08/23 22:190.26
1,2,4-Trichlorobenzene ug/L ND 1.0 03/08/23 22:190.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/08/23 22:190.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/08/23 22:190.27
1,2-Dichlorobenzene ug/L ND 1.0 03/08/23 22:190.34
1,2-Dichloroethane ug/L ND 1.0 03/08/23 22:190.32
1,2-Dichloropropane ug/L ND 1.0 03/08/23 22:190.36
1,3-Dichlorobenzene ug/L ND 1.0 03/08/23 22:190.34
1,3-Dichloropropane ug/L ND 1.0 03/08/23 22:190.28
1,4-Dichlorobenzene ug/L ND 1.0 03/08/23 22:190.33
2,2-Dichloropropane ug/L ND 1.0 03/08/23 22:190.39
2-Butanone (MEK)ug/L ND 5.0 03/08/23 22:194.0
2-Chlorotoluene ug/L ND 1.0 03/08/23 22:190.32
2-Hexanone ug/L ND 5.0 03/08/23 22:190.48
4-Chlorotoluene ug/L ND 1.0 03/08/23 22:190.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/08/23 22:192.7
Acetone ug/L ND 25.0 03/08/23 22:195.1
Benzene ug/L ND 1.0 03/08/23 22:190.34
Bromobenzene ug/L ND 1.0 03/08/23 22:190.29
Bromochloromethane ug/L ND 1.0 03/08/23 22:190.47
Bromodichloromethane ug/L ND 1.0 03/08/23 22:190.31
Bromoform ug/L ND 1.0 03/08/23 22:190.34
Bromomethane ug/L ND 2.0 v203/08/23 22:191.7
Carbon tetrachloride ug/L ND 1.0 03/08/23 22:190.33
Chlorobenzene ug/L ND 1.0 03/08/23 22:190.28
Chloroethane ug/L ND 1.0 03/08/23 22:190.65
Chloroform ug/L ND 1.0 03/08/23 22:190.43
Chloromethane ug/L ND 1.0 03/08/23 22:190.54
cis-1,2-Dichloroethene ug/L ND 1.0 03/08/23 22:190.38
cis-1,3-Dichloropropene ug/L ND 1.0 03/08/23 22:190.36
Dibromochloromethane ug/L ND 1.0 03/08/23 22:190.36
Dibromomethane ug/L ND 1.0 03/08/23 22:190.39
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
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Page 33 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3948359
Associated Lab Samples:92655680004, 92655680005, 92655680007
Matrix: Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 IH03/08/23 22:190.35
Diisopropyl ether ug/L ND 1.0 03/08/23 22:190.31
Ethylbenzene ug/L ND 1.0 03/08/23 22:190.30
Hexachloro-1,3-butadiene ug/L ND 2.0 03/08/23 22:191.5
m&p-Xylene ug/L ND 2.0 03/08/23 22:190.71
Methyl-tert-butyl ether ug/L ND 1.0 03/08/23 22:190.42
Methylene Chloride ug/L ND 5.0 03/08/23 22:192.0
Naphthalene ug/L ND 1.0 03/08/23 22:190.64
o-Xylene ug/L ND 1.0 03/08/23 22:190.34
p-Isopropyltoluene ug/L ND 1.0 03/08/23 22:190.41
Styrene ug/L ND 1.0 03/08/23 22:190.29
Tetrachloroethene ug/L ND 1.0 03/08/23 22:190.29
Toluene ug/L ND 1.0 03/08/23 22:190.24
trans-1,2-Dichloroethene ug/L ND 1.0 03/08/23 22:190.40
trans-1,3-Dichloropropene ug/L ND 1.0 03/08/23 22:190.36
Trichloroethene ug/L ND 1.0 03/08/23 22:190.38
Trichlorofluoromethane ug/L ND 1.0 03/08/23 22:190.30
Vinyl acetate ug/L ND 2.0 03/08/23 22:191.3
Vinyl chloride ug/L ND 1.0 03/08/23 22:190.39
Xylene (Total)ug/L ND 1.0 03/08/23 22:190.34
1,2-Dichloroethane-d4 (S)%99 70-130 03/08/23 22:19
4-Bromofluorobenzene (S)%97 70-130 03/08/23 22:19
Toluene-d8 (S)%99 70-130 03/08/23 22:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3948360LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 22.220 111 70-130
1,1,1-Trichloroethane ug/L 20.620 103 70-130
1,1,2,2-Tetrachloroethane ug/L 21.020 105 70-130
1,1,2-Trichloroethane ug/L 21.120 105 70-130
1,1-Dichloroethane ug/L 20.620 103 70-130
1,1-Dichloroethene ug/L 20.120 100 70-130
1,1-Dichloropropene ug/L 21.520 108 70-130
1,2,3-Trichlorobenzene ug/L 21.420 107 70-130
1,2,3-Trichloropropane ug/L 20.120 100 70-130
1,2,4-Trichlorobenzene ug/L 21.220 106 70-130
1,2-Dibromo-3-chloropropane ug/L 20.420 102 70-131
1,2-Dibromoethane (EDB)ug/L 21.420 107 70-130
1,2-Dichlorobenzene ug/L 21.620 108 70-130
1,2-Dichloroethane ug/L 20.620 103 70-130
1,2-Dichloropropane ug/L 21.020 105 70-130
1,3-Dichlorobenzene ug/L 22.420 112 70-130
1,3-Dichloropropane ug/L 20.320 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3948360LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 22.120 110 70-130
2,2-Dichloropropane ug/L 21.420 107 68-135
2-Butanone (MEK)ug/L 38.140 95 70-134
2-Chlorotoluene ug/L 21.520 108 70-130
2-Hexanone ug/L 40.640 102 70-131
4-Chlorotoluene ug/L 20.920 105 70-130
4-Methyl-2-pentanone (MIBK)ug/L 39.140 98 70-130
Acetone ug/L 36.940 92 70-133
Benzene ug/L 21.120 105 70-130
Bromobenzene ug/L 21.620 108 70-130
Bromochloromethane ug/L 22.220 111 70-130
Bromodichloromethane ug/L 20.720 103 70-130
Bromoform ug/L 20.520 103 70-130
Bromomethane ug/L 16.2 v32081 45-151
Carbon tetrachloride ug/L 21.420 107 70-130
Chlorobenzene ug/L 21.620 108 70-130
Chloroethane ug/L 21.520 107 39-152
Chloroform ug/L 20.320 102 70-130
Chloromethane ug/L 23.020 115 58-130
cis-1,2-Dichloroethene ug/L 20.220 101 70-130
cis-1,3-Dichloropropene ug/L 20.520 103 70-130
Dibromochloromethane ug/L 21.120 105 70-130
Dibromomethane ug/L 20.420 102 70-130
Dichlorodifluoromethane ug/L 25.0 IH20125 54-133
Diisopropyl ether ug/L 18.720 94 70-130
Ethylbenzene ug/L 21.320 106 70-130
Hexachloro-1,3-butadiene ug/L 23.020 115 70-135
m&p-Xylene ug/L 43.540 109 70-130
Methyl-tert-butyl ether ug/L 18.720 93 70-130
Methylene Chloride ug/L 20.020 100 66-130
Naphthalene ug/L 21.320 107 70-130
o-Xylene ug/L 21.620 108 70-130
p-Isopropyltoluene ug/L 22.420 112 70-130
Styrene ug/L 21.920 109 70-130
Tetrachloroethene ug/L 21.620 108 70-130
Toluene ug/L 20.120 100 70-130
trans-1,2-Dichloroethene ug/L 20.320 102 70-130
trans-1,3-Dichloropropene ug/L 20.920 105 70-130
Trichloroethene ug/L 21.620 108 70-130
Trichlorofluoromethane ug/L 19.720 98 62-130
Vinyl acetate ug/L 41.340 103 70-144
Vinyl chloride ug/L 18.320 92 62-130
Xylene (Total)ug/L 65.160 108 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3948362MATRIX SPIKE SAMPLE:
MSSpike
Result
92655697002
1,1,1,2-Tetrachloroethane ug/L 24.720 124 70-141ND
1,1,1-Trichloroethane ug/L 24.320 121 70-150ND
1,1,2,2-Tetrachloroethane ug/L 22.520 113 69-142ND
1,1,2-Trichloroethane ug/L 23.420 117 70-138ND
1,1-Dichloroethane ug/L 22.420 112 70-150ND
1,1-Dichloroethene ug/L 23.820 119 70-156ND
1,1-Dichloropropene ug/L 24.720 123 70-150ND
1,2,3-Trichlorobenzene ug/L 23.120 116 70-148ND
1,2,3-Trichloropropane ug/L 22.920 115 70-140ND
1,2,4-Trichlorobenzene ug/L 23.520 118 70-146ND
1,2-Dibromo-3-chloropropane ug/L 22.620 113 68-146ND
1,2-Dibromoethane (EDB)ug/L 23.620 118 70-138ND
1,2-Dichlorobenzene ug/L 23.620 118 70-141ND
1,2-Dichloroethane ug/L 22.520 113 69-143ND
1,2-Dichloropropane ug/L 23.120 116 68-156ND
1,3-Dichlorobenzene ug/L 24.320 122 70-143ND
1,3-Dichloropropane ug/L 22.420 112 70-138ND
1,4-Dichlorobenzene ug/L 23.720 119 70-142ND
2,2-Dichloropropane ug/L 25.120 126 52-170ND
2-Butanone (MEK)ug/L 44.140 110 60-157ND
2-Chlorotoluene ug/L 24.020 120 70-147ND
2-Hexanone ug/L 44.940 112 68-146ND
4-Chlorotoluene ug/L 23.620 118 70-142ND
4-Methyl-2-pentanone (MIBK)ug/L 43.140 108 70-141ND
Acetone ug/L 40.040 94 58-157ND
Benzene ug/L 24.120 121 70-142ND
Bromobenzene ug/L 23.620 118 70-143ND
Bromochloromethane ug/L 24.720 124 70-146ND
Bromodichloromethane ug/L 23.220 116 70-139ND
Bromoform ug/L 24.120 120 64-140ND
Bromomethane ug/L 20.720 103 28-192ND
Carbon tetrachloride ug/L 26.220 131 70-148ND
Chlorobenzene ug/L 24.320 122 70-141ND
Chloroethane ug/L 24.820 124 58-191ND
Chloroform ug/L 22.820 114 70-148ND
Chloromethane ug/L 26.020 130 43-162ND
cis-1,2-Dichloroethene ug/L 23.420 117 68-151ND
cis-1,3-Dichloropropene ug/L 22.920 115 70-139ND
Dibromochloromethane ug/L 24.120 121 70-144ND
Dibromomethane ug/L 22.920 115 70-139ND
Dichlorodifluoromethane ug/L 33.9 IH,v120169 39-171ND
Diisopropyl ether ug/L 20.520 103 67-142ND
Ethylbenzene ug/L 24.120 120 70-143ND
Hexachloro-1,3-butadiene ug/L 26.820 134 64-163ND
m&p-Xylene ug/L 49.140 123 70-144ND
Methyl-tert-butyl ether ug/L 20.620 103 65-143ND
Methylene Chloride ug/L 21.520 106 62-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3948362MATRIX SPIKE SAMPLE:
MSSpike
Result
92655697002
Naphthalene ug/L 22.920 114 67-147ND
o-Xylene ug/L 23.720 119 70-145ND
p-Isopropyltoluene ug/L 25.520 128 70-147ND
Styrene ug/L 24.120 120 70-143ND
Tetrachloroethene ug/L 24.920 124 70-145ND
Toluene ug/L 22.820 114 70-142ND
trans-1,2-Dichloroethene ug/L 23.220 116 70-151ND
trans-1,3-Dichloropropene ug/L 23.520 118 70-139ND
Trichloroethene ug/L 24.720 124 62-146ND
Trichlorofluoromethane ug/L 26.320 131 63-153ND
Vinyl acetate ug/L 43.840 110 61-162ND
Vinyl chloride ug/L 21.720 109 61-163ND
Xylene (Total)ug/L 72.860 121 70-143ND
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655697001
3948361SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655697001
3948361SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND IH,v130ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%9796
4-Bromofluorobenzene (S)%9899
Toluene-d8 (S)%99100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760455
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92655680001, 92655680002, 92655680003, 92655680006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3950037
Associated Lab Samples:92655680001, 92655680002, 92655680003, 92655680006
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/09/23 21:220.31
1,1,1-Trichloroethane ug/L ND 1.0 03/09/23 21:220.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/09/23 21:220.22
1,1,2-Trichloroethane ug/L ND 1.0 03/09/23 21:220.32
1,1-Dichloroethane ug/L ND 1.0 03/09/23 21:220.37
1,1-Dichloroethene ug/L ND 1.0 03/09/23 21:220.35
1,1-Dichloropropene ug/L ND 1.0 03/09/23 21:220.43
1,2,3-Trichlorobenzene ug/L ND 1.0 03/09/23 21:220.81
1,2,3-Trichloropropane ug/L ND 1.0 03/09/23 21:220.26
1,2,4-Trichlorobenzene ug/L ND 1.0 03/09/23 21:220.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/09/23 21:220.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/09/23 21:220.27
1,2-Dichlorobenzene ug/L ND 1.0 03/09/23 21:220.34
1,2-Dichloroethane ug/L ND 1.0 03/09/23 21:220.32
1,2-Dichloropropane ug/L ND 1.0 03/09/23 21:220.36
1,3-Dichlorobenzene ug/L ND 1.0 03/09/23 21:220.34
1,3-Dichloropropane ug/L ND 1.0 03/09/23 21:220.28
1,4-Dichlorobenzene ug/L ND 1.0 03/09/23 21:220.33
2,2-Dichloropropane ug/L ND 1.0 03/09/23 21:220.39
2-Butanone (MEK)ug/L ND 5.0 03/09/23 21:224.0
2-Chlorotoluene ug/L ND 1.0 03/09/23 21:220.32
2-Hexanone ug/L ND 5.0 03/09/23 21:220.48
4-Chlorotoluene ug/L ND 1.0 03/09/23 21:220.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/09/23 21:222.7
Acetone ug/L ND 25.0 03/09/23 21:225.1
Benzene ug/L ND 1.0 03/09/23 21:220.34
Bromobenzene ug/L ND 1.0 03/09/23 21:220.29
Bromochloromethane ug/L ND 1.0 03/09/23 21:220.47
Bromodichloromethane ug/L ND 1.0 03/09/23 21:220.31
Bromoform ug/L ND 1.0 03/09/23 21:220.34
Bromomethane ug/L ND 2.0 03/09/23 21:221.7
Carbon tetrachloride ug/L ND 1.0 03/09/23 21:220.33
Chlorobenzene ug/L ND 1.0 03/09/23 21:220.28
Chloroethane ug/L ND 1.0 03/09/23 21:220.65
Chloroform ug/L ND 1.0 03/09/23 21:220.43
Chloromethane ug/L ND 1.0 03/09/23 21:220.54
cis-1,2-Dichloroethene ug/L ND 1.0 03/09/23 21:220.38
cis-1,3-Dichloropropene ug/L ND 1.0 03/09/23 21:220.36
Dibromochloromethane ug/L ND 1.0 03/09/23 21:220.36
Dibromomethane ug/L ND 1.0 03/09/23 21:220.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3950037
Associated Lab Samples:92655680001, 92655680002, 92655680003, 92655680006
Matrix: Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 03/09/23 21:220.35
Diisopropyl ether ug/L ND 1.0 03/09/23 21:220.31
Ethylbenzene ug/L ND 1.0 03/09/23 21:220.30
Hexachloro-1,3-butadiene ug/L ND 2.0 03/09/23 21:221.5
m&p-Xylene ug/L ND 2.0 03/09/23 21:220.71
Methyl-tert-butyl ether ug/L ND 1.0 03/09/23 21:220.42
Methylene Chloride ug/L ND 5.0 03/09/23 21:222.0
Naphthalene ug/L ND 1.0 03/09/23 21:220.64
o-Xylene ug/L ND 1.0 03/09/23 21:220.34
p-Isopropyltoluene ug/L ND 1.0 03/09/23 21:220.41
Styrene ug/L ND 1.0 03/09/23 21:220.29
Tetrachloroethene ug/L ND 1.0 03/09/23 21:220.29
Toluene ug/L ND 1.0 03/09/23 21:220.24
trans-1,2-Dichloroethene ug/L ND 1.0 03/09/23 21:220.40
trans-1,3-Dichloropropene ug/L ND 1.0 03/09/23 21:220.36
Trichloroethene ug/L ND 1.0 03/09/23 21:220.38
Trichlorofluoromethane ug/L ND 1.0 03/09/23 21:220.30
Vinyl acetate ug/L ND 2.0 03/09/23 21:221.3
Vinyl chloride ug/L ND 1.0 03/09/23 21:220.39
Xylene (Total)ug/L ND 1.0 03/09/23 21:220.34
1,2-Dichloroethane-d4 (S)%103 70-130 03/09/23 21:22
4-Bromofluorobenzene (S)%104 70-130 03/09/23 21:22
Toluene-d8 (S)%101 70-130 03/09/23 21:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3950038LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.020 105 70-130
1,1,1-Trichloroethane ug/L 21.120 106 70-130
1,1,2,2-Tetrachloroethane ug/L 22.020 110 70-130
1,1,2-Trichloroethane ug/L 21.820 109 70-130
1,1-Dichloroethane ug/L 21.120 105 70-130
1,1-Dichloroethene ug/L 20.620 103 70-130
1,1-Dichloropropene ug/L 21.320 106 70-130
1,2,3-Trichlorobenzene ug/L 20.820 104 70-130
1,2,3-Trichloropropane ug/L 20.220 101 70-130
1,2,4-Trichlorobenzene ug/L 20.520 102 70-130
1,2-Dibromo-3-chloropropane ug/L 19.720 99 70-131
1,2-Dibromoethane (EDB)ug/L 21.120 105 70-130
1,2-Dichlorobenzene ug/L 20.620 103 70-130
1,2-Dichloroethane ug/L 21.020 105 70-130
1,2-Dichloropropane ug/L 21.220 106 70-130
1,3-Dichlorobenzene ug/L 20.820 104 70-130
1,3-Dichloropropane ug/L 19.920 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3950038LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 20.620 103 70-130
2,2-Dichloropropane ug/L 20.320 101 68-135
2-Butanone (MEK)ug/L 46.940 117 70-134
2-Chlorotoluene ug/L 20.520 102 70-130
2-Hexanone ug/L 44.340 111 70-131
4-Chlorotoluene ug/L 20.320 102 70-130
4-Methyl-2-pentanone (MIBK)ug/L 45.340 113 70-130
Acetone ug/L 43.040 108 70-133
Benzene ug/L 21.020 105 70-130
Bromobenzene ug/L 20.720 104 70-130
Bromochloromethane ug/L 21.120 106 70-130
Bromodichloromethane ug/L 21.620 108 70-130
Bromoform ug/L 19.620 98 70-130
Bromomethane ug/L 14.020 70 45-151
Carbon tetrachloride ug/L 20.820 104 70-130
Chlorobenzene ug/L 20.620 103 70-130
Chloroethane ug/L 19.820 99 39-152
Chloroform ug/L 18.620 93 70-130
Chloromethane ug/L 19.520 97 58-130
cis-1,2-Dichloroethene ug/L 20.520 102 70-130
cis-1,3-Dichloropropene ug/L 21.220 106 70-130
Dibromochloromethane ug/L 20.120 100 70-130
Dibromomethane ug/L 21.920 109 70-130
Dichlorodifluoromethane ug/L 18.920 94 54-133
Diisopropyl ether ug/L 20.120 101 70-130
Ethylbenzene ug/L 20.420 102 70-130
Hexachloro-1,3-butadiene ug/L 20.020 100 70-135
m&p-Xylene ug/L 41.040 103 70-130
Methyl-tert-butyl ether ug/L 18.820 94 70-130
Methylene Chloride ug/L 21.420 107 66-130
Naphthalene ug/L 22.320 111 70-130
o-Xylene ug/L 20.520 102 70-130
p-Isopropyltoluene ug/L 20.920 105 70-130
Styrene ug/L 20.920 105 70-130
Tetrachloroethene ug/L 20.220 101 70-130
Toluene ug/L 21.520 108 70-130
trans-1,2-Dichloroethene ug/L 21.120 105 70-130
trans-1,3-Dichloropropene ug/L 21.120 105 70-130
Trichloroethene ug/L 21.020 105 70-130
Trichlorofluoromethane ug/L 18.720 93 62-130
Vinyl acetate ug/L 42.940 107 70-144
Vinyl chloride ug/L 16.120 81 62-130
Xylene (Total)ug/L 61.560 103 70-130
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3950040MATRIX SPIKE SAMPLE:
MSSpike
Result
92655394008
1,1,1,2-Tetrachloroethane ug/L 21.120 105 70-141ND
1,1,1-Trichloroethane ug/L 22.020 110 70-150ND
1,1,2,2-Tetrachloroethane ug/L 19.820 99 69-142ND
1,1,2-Trichloroethane ug/L 19.920 100 70-138ND
1,1-Dichloroethane ug/L 20.220 101 70-150ND
1,1-Dichloroethene ug/L 22.020 110 70-156ND
1,1-Dichloropropene ug/L 23.820 119 70-150ND
1,2,3-Trichlorobenzene ug/L 23.420 117 70-148ND
1,2,3-Trichloropropane ug/L 19.220 96 70-140ND
1,2,4-Trichlorobenzene ug/L 23.020 115 70-146ND
1,2-Dibromo-3-chloropropane ug/L 20.120 100 68-146ND
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-138ND
1,2-Dichlorobenzene ug/L 20.820 104 70-141ND
1,2-Dichloroethane ug/L 19.320 96 69-143ND
1,2-Dichloropropane ug/L 20.920 105 68-156ND
1,3-Dichlorobenzene ug/L 21.520 107 70-143ND
1,3-Dichloropropane ug/L 19.620 98 70-138ND
1,4-Dichlorobenzene ug/L 20.620 103 70-142ND
2,2-Dichloropropane ug/L 21.920 109 52-170ND
2-Butanone (MEK)ug/L 39.940 93 60-157ND
2-Chlorotoluene ug/L 21.520 108 70-147ND
2-Hexanone ug/L 41.240 103 68-146ND
4-Chlorotoluene ug/L 21.220 106 70-142ND
4-Methyl-2-pentanone (MIBK)ug/L 39.140 98 70-141ND
Acetone ug/L 46.240 81 58-157ND
Benzene ug/L 20.920 105 70-142ND
Bromobenzene ug/L 19.920 99 70-143ND
Bromochloromethane ug/L 20.220 101 70-146ND
Bromodichloromethane ug/L 19.720 98 70-139ND
Bromoform ug/L 19.520 98 64-140ND
Bromomethane ug/L 15.1 v32075 28-192ND
Carbon tetrachloride ug/L 22.720 113 70-148ND
Chlorobenzene ug/L 21.020 105 70-141ND
Chloroethane ug/L 21.620 108 58-191ND
Chloroform ug/L 19.920 100 70-148ND
Chloromethane ug/L 21.220 106 43-162ND
cis-1,2-Dichloroethene ug/L 20.020 100 68-151ND
cis-1,3-Dichloropropene ug/L 19.720 98 70-139ND
Dibromochloromethane ug/L 20.120 100 70-144ND
Dibromomethane ug/L 19.820 99 70-139ND
Dichlorodifluoromethane ug/L 21.920 109 39-171ND
Diisopropyl ether ug/L 19.220 96 67-142ND
Ethylbenzene ug/L 23.120 109 70-1431.4
Hexachloro-1,3-butadiene ug/L 27.720 139 64-163ND
m&p-Xylene ug/L 50.140 109 70-1446.6
Methyl-tert-butyl ether ug/L 17.820 89 65-143ND
Methylene Chloride ug/L 19.120 95 62-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3950040MATRIX SPIKE SAMPLE:
MSSpike
Result
92655394008
Naphthalene ug/L 22.520 113 67-147ND
o-Xylene ug/L 23.420 106 70-1452.3
p-Isopropyltoluene ug/L 24.320 121 70-147ND
Styrene ug/L 21.620 108 70-143ND
Tetrachloroethene ug/L 23.020 115 70-145ND
Toluene ug/L 20.520 102 70-142ND
trans-1,2-Dichloroethene ug/L 21.820 109 70-151ND
trans-1,3-Dichloropropene ug/L 19.620 98 70-139ND
Trichloroethene ug/L 22.020 110 62-146ND
Trichlorofluoromethane ug/L 20.6 IK20103 63-153ND
Vinyl acetate ug/L 40.140 100 61-162ND
Vinyl chloride ug/L 18.420 92 61-163ND
Xylene (Total)ug/L 73.660 108 70-1438.9
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655394007
3950039SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L 5.3 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 8.1J 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655394007
3950039SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND IK30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%9696
4-Bromofluorobenzene (S)%125104
Toluene-d8 (S)%106111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760065
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92655680001, 92655680002, 92655680003, 92655680004, 92655680005, 92655680006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3947624
Associated Lab Samples:92655680001, 92655680002, 92655680003, 92655680004, 92655680005, 92655680006
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 03/09/23 10:531.7
1,2-Dichlorobenzene ug/L ND 10.0 03/09/23 10:531.8
1,3-Dichlorobenzene ug/L ND 10.0 03/09/23 10:531.6
1,4-Dichlorobenzene ug/L ND 10.0 03/09/23 10:531.7
1-Methylnaphthalene ug/L ND 10.0 03/09/23 10:532.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 03/09/23 10:531.2
2,4,5-Trichlorophenol ug/L ND 10.0 03/09/23 10:531.4
2,4,6-Trichlorophenol ug/L ND 10.0 03/09/23 10:531.6
2,4-Dichlorophenol ug/L ND 10.0 03/09/23 10:531.4
2,4-Dimethylphenol ug/L ND 10.0 03/09/23 10:531.7
2,4-Dinitrophenol ug/L ND 50.0 03/09/23 10:5326.0
2,4-Dinitrotoluene ug/L ND 10.0 03/09/23 10:531.6
2,6-Dinitrotoluene ug/L ND 10.0 03/09/23 10:531.7
2-Chloronaphthalene ug/L ND 10.0 03/09/23 10:531.7
2-Chlorophenol ug/L ND 10.0 03/09/23 10:531.2
2-Methylnaphthalene ug/L ND 10.0 03/09/23 10:531.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 03/09/23 10:531.9
2-Nitroaniline ug/L ND 20.0 03/09/23 10:533.0
2-Nitrophenol ug/L ND 10.0 v103/09/23 10:531.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 03/09/23 10:531.2
3,3'-Dichlorobenzidine ug/L ND 20.0 03/09/23 10:538.1
3-Nitroaniline ug/L ND 20.0 03/09/23 10:533.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 03/09/23 10:537.8
4-Bromophenylphenyl ether ug/L ND 10.0 03/09/23 10:531.8
4-Chloro-3-methylphenol ug/L ND 10.0 03/09/23 10:533.3
4-Chloroaniline ug/L ND 20.0 03/09/23 10:533.6
4-Chlorophenylphenyl ether ug/L ND 10.0 03/09/23 10:532.0
4-Nitroaniline ug/L ND 20.0 03/09/23 10:535.1
4-Nitrophenol ug/L ND 50.0 03/09/23 10:536.6
Acenaphthene ug/L ND 10.0 03/09/23 10:532.0
Acenaphthylene ug/L ND 10.0 03/09/23 10:532.0
Aniline ug/L ND 10.0 03/09/23 10:531.6
Anthracene ug/L ND 10.0 03/09/23 10:532.3
Benzo(a)anthracene ug/L ND 10.0 03/09/23 10:532.7
Benzo(a)pyrene ug/L ND 10.0 03/09/23 10:532.8
Benzo(b)fluoranthene ug/L ND 10.0 03/09/23 10:532.6
Benzo(g,h,i)perylene ug/L ND 10.0 03/09/23 10:532.8
Benzo(k)fluoranthene ug/L ND 10.0 03/09/23 10:532.7
Benzoic Acid ug/L ND 50.0 03/09/23 10:5322.0
Benzyl alcohol ug/L ND 20.0 03/09/23 10:532.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3947624
Associated Lab Samples:92655680001, 92655680002, 92655680003, 92655680004, 92655680005, 92655680006
Matrix: Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 03/09/23 10:531.8
bis(2-Chloroethyl) ether ug/L ND 10.0 03/09/23 10:531.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 03/09/23 10:533.7
Butylbenzylphthalate ug/L ND 10.0 03/09/23 10:533.1
Chrysene ug/L ND 10.0 03/09/23 10:532.8
Di-n-butylphthalate ug/L ND 10.0 03/09/23 10:532.2
Di-n-octylphthalate ug/L ND 10.0 03/09/23 10:533.9
Dibenz(a,h)anthracene ug/L ND 10.0 03/09/23 10:533.0
Dibenzofuran ug/L ND 10.0 03/09/23 10:532.1
Diethylphthalate ug/L ND 10.0 03/09/23 10:532.0
Dimethylphthalate ug/L ND 10.0 03/09/23 10:532.1
Fluoranthene ug/L ND 10.0 03/09/23 10:532.2
Fluorene ug/L ND 10.0 03/09/23 10:532.1
Hexachloro-1,3-butadiene ug/L ND 10.0 03/09/23 10:531.8
Hexachlorobenzene ug/L ND 10.0 03/09/23 10:532.2
Hexachlorocyclopentadiene ug/L ND 10.0 03/09/23 10:531.6
Hexachloroethane ug/L ND 10.0 03/09/23 10:531.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 03/09/23 10:532.9
Isophorone ug/L ND 10.0 03/09/23 10:531.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 03/09/23 10:531.3
N-Nitrosodimethylamine ug/L ND 10.0 v103/09/23 10:531.9
N-Nitrosodiphenylamine ug/L ND 10.0 03/09/23 10:533.0
Naphthalene ug/L ND 10.0 03/09/23 10:532.1
Nitrobenzene ug/L ND 10.0 03/09/23 10:531.9
Pentachlorophenol ug/L ND 20.0 03/09/23 10:533.8
Phenanthrene ug/L ND 10.0 03/09/23 10:532.0
Phenol ug/L ND 10.0 03/09/23 10:531.4
Pyrene ug/L ND 10.0 03/09/23 10:532.2
2,4,6-Tribromophenol (S)%82 10-164 03/09/23 10:53
2-Fluorobiphenyl (S)%74 10-130 03/09/23 10:53
2-Fluorophenol (S)%63 10-130 03/09/23 10:53
Nitrobenzene-d5 (S)%77 10-138 03/09/23 10:53
Phenol-d6 (S)%50 10-130 03/09/23 10:53
Terphenyl-d14 (S)%93 19-191 03/09/23 10:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3947625LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 28.850 58 11-130
1,2-Dichlorobenzene ug/L 28.350 57 10-130
1,3-Dichlorobenzene ug/L 26.950 54 10-130
1,4-Dichlorobenzene ug/L 27.350 55 10-130
1-Methylnaphthalene ug/L 41.850 84 23-130
2,2'-Oxybis(1-chloropropane)ug/L 46.550 93 21-135
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3947625LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 50.150 100 38-147
2,4,6-Trichlorophenol ug/L 53.150 106 34-142
2,4-Dichlorophenol ug/L 49.350 99 36-136
2,4-Dimethylphenol ug/L 64.850 130 38-134
2,4-Dinitrophenol ug/L 249250 99 10-169
2,4-Dinitrotoluene ug/L 52.750 105 44-154
2,6-Dinitrotoluene ug/L 54.350 109 44-156
2-Chloronaphthalene ug/L 44.750 89 25-130
2-Chlorophenol ug/L 47.850 96 29-130
2-Methylnaphthalene ug/L 40.250 80 23-130
2-Methylphenol(o-Cresol)ug/L 46.150 92 31-130
2-Nitroaniline ug/L 107100 107 39-145
2-Nitrophenol ug/L 54.7 v150109 29-142
3&4-Methylphenol(m&p Cresol)ug/L 43.150 86 30-130
3,3'-Dichlorobenzidine ug/L 88.6100 89 44-158
3-Nitroaniline ug/L 96.9100 97 45-152
4,6-Dinitro-2-methylphenol ug/L 98.7100 99 39-158
4-Bromophenylphenyl ether ug/L 46.650 93 47-147
4-Chloro-3-methylphenol ug/L 92.8100 93 40-138
4-Chloroaniline ug/L 75.8100 76 35-130
4-Chlorophenylphenyl ether ug/L 46.050 92 36-139
4-Nitroaniline ug/L 103100 103 46-157
4-Nitrophenol ug/L 151250 61 17-130
Acenaphthene ug/L 45.550 91 34-135
Acenaphthylene ug/L 46.650 93 35-137
Aniline ug/L 10J L25020 25-130
Anthracene ug/L 46.250 92 47-146
Benzo(a)anthracene ug/L 51.650 103 48-160
Benzo(a)pyrene ug/L 51.650 103 47-165
Benzo(b)fluoranthene ug/L 53.850 108 49-171
Benzo(g,h,i)perylene ug/L 45.350 91 46-166
Benzo(k)fluoranthene ug/L 51.750 103 55-162
Benzoic Acid ug/L 143250 57 10-130
Benzyl alcohol ug/L 92.6100 93 29-132
bis(2-Chloroethoxy)methane ug/L 49.450 99 33-136
bis(2-Chloroethyl) ether ug/L 44.550 89 30-142
bis(2-Ethylhexyl)phthalate ug/L 58.250 116 46-173
Butylbenzylphthalate ug/L 59.250 118 53-169
Chrysene ug/L 48.050 96 54-152
Di-n-butylphthalate ug/L 53.950 108 49-161
Di-n-octylphthalate ug/L 55.250 110 50-166
Dibenz(a,h)anthracene ug/L 50.350 101 46-166
Dibenzofuran ug/L 47.250 94 37-136
Diethylphthalate ug/L 50.050 100 45-149
Dimethylphthalate ug/L 48.750 97 43-145
Fluoranthene ug/L 49.150 98 50-153
Fluorene ug/L 48.550 97 42-142
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
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Huntersville, NC 28078
[phone]
Page 47 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3947625LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 22.950 46 10-130
Hexachlorobenzene ug/L 46.150 92 44-138
Hexachlorocyclopentadiene ug/L 31.650 63 10-130
Hexachloroethane ug/L 23.250 46 10-130
Indeno(1,2,3-cd)pyrene ug/L 48.650 97 46-166
Isophorone ug/L 48.050 96 36-135
N-Nitroso-di-n-propylamine ug/L 47.950 96 33-140
N-Nitrosodimethylamine ug/L 49.3 v15099 24-130
N-Nitrosodiphenylamine ug/L 49.650 99 46-144
Naphthalene ug/L 34.750 69 20-130
Nitrobenzene ug/L 45.350 91 33-133
Pentachlorophenol ug/L 89.6100 90 21-163
Phenanthrene ug/L 48.750 97 47-146
Phenol ug/L 30.050 60 19-130
Pyrene ug/L 52.650 105 53-155
2,4,6-Tribromophenol (S)%126 10-164
2-Fluorobiphenyl (S)%106 10-130
2-Fluorophenol (S)%89 10-130
Nitrobenzene-d5 (S)%110 10-138
Phenol-d6 (S)%72 10-130
Terphenyl-d14 (S)%124 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3947626MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655398001
3947627
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 46 10-13055 19 3050ND22.8 27.7
1,2-Dichlorobenzene ug/L R1503610-13053 37 3050ND18.1 26.4
1,3-Dichlorobenzene ug/L R1503110-13047 41 3050ND15.7 23.7
1,4-Dichlorobenzene ug/L R1503410-13049 37 3050ND16.8 24.5
1-Methylnaphthalene ug/L 50 69 10-13193 30 3050ND34.5 46.7
2,2'-Oxybis(1-chloropropane)ug/L R1507411-143107 37 3050ND36.8 53.6
2,4,5-Trichlorophenol ug/L R1508110-170119 38 3050ND40.5 59.4
2,4,6-Trichlorophenol ug/L R1508310-166124 39 3050ND41.7 62.1
2,4-Dichlorophenol ug/L R1507610-153111 37 3050ND38.1 55.4
2,4-Dimethylphenol ug/L R15010220-147145 34 3050ND51.2 72.3
2,4-Dinitrophenol ug/L R12507310-172111 42 30250ND182 279
2,4-Dinitrotoluene ug/L R1508330-164122 38 3050ND41.5 60.8
2,6-Dinitrotoluene ug/L R1508631-163125 38 3050ND42.8 62.6
2-Chloronaphthalene ug/L R1507815-134109 33 3050ND39.1 54.4
2-Chlorophenol ug/L R1507310-139110 40 3050ND36.7 55.0
2-Methylnaphthalene ug/L 50 67 12-13091 30 3050ND33.7 45.4
2-Methylphenol(o-Cresol) ug/L R1507019-132104 39 3050ND35.0 52.1
2-Nitroaniline ug/L R11008323-154126 41 30100ND82.7 126
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3947626MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655398001
3947627
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitrophenol ug/L R1,v1508610-159126 38 3050ND43.2 63.2
3&4-Methylphenol(m&p
Cresol)ug/L R1506513-136103 45 3050ND32.3 51.3
3,3'-Dichlorobenzidine ug/L R11006710-178110 48 30100ND67.0 110
3-Nitroaniline ug/L R11007420-166113 42 30100ND73.7 113
4,6-Dinitro-2-methylphenol ug/L R11007610-187116 42 30100ND76.2 116
4-Bromophenylphenyl ether ug/L R1507631-157112 38 3050ND38.1 55.8
4-Chloro-3-methylphenol ug/L R11006927-146103 40 30100ND68.8 103
4-Chloroaniline ug/L R11005113-14381 45 30100ND51.0 80.6
4-Chlorophenylphenyl ether ug/L R1507223-149105 37 3050ND36.0 52.5
4-Nitroaniline ug/L R11008324-171119 36 30100ND82.8 119
4-Nitrophenol ug/L R12504410-13068 42 30250ND111 170
Acenaphthene ug/L R1507621-147108 34 3050ND38.2 54.1
Acenaphthylene ug/L R1507619-150111 37 3050ND38.0 55.4
Aniline ug/L 50 10 10-13017 3050ND5.2J 8.7J
Anthracene ug/L R1507536-152109 37 3050ND37.6 54.7
Benzo(a)anthracene ug/L R1508442-163125 39 3050ND42.1 62.5
Benzo(a)pyrene ug/L R1508440-169123 38 3050ND42.1 61.6
Benzo(b)fluoranthene ug/L R1508740-177132 41 3050ND43.4 65.8
Benzo(g,h,i)perylene ug/L R1508238-174113 31 3050ND41.2 56.4
Benzo(k)fluoranthene ug/L R1508541-171123 36 3050ND42.6 61.5
Benzoic Acid ug/L R12503910-13062 45 30250ND97.4 154
Benzyl alcohol ug/L R11007018-141108 43 30100ND69.7 108
bis(2-Chloroethoxy)methane ug/L R1507619-146109 35 3050ND38.2 54.5
bis(2-Chloroethyl) ether ug/L R1507119-151104 38 3050ND35.3 52.0
bis(2-Ethylhexyl)phthalate ug/L R1509442-168145 43 3050ND46.8 72.3
Butylbenzylphthalate ug/L R15010042-177150 40 3050ND50.0 75.0
Chrysene ug/L R1508143-159117 36 3050ND40.6 58.3
Di-n-butylphthalate ug/L R1509042-160131 37 3050ND45.0 65.7
Di-n-octylphthalate ug/L R1508642-171140 47 3050ND43.1 69.8
Dibenz(a,h)anthracene ug/L R1508740-171123 35 3050ND43.3 61.7
Dibenzofuran ug/L R1507623-147109 36 3050ND37.9 54.7
Diethylphthalate ug/L R1508033-157115 37 3050ND39.9 57.7
Dimethylphthalate ug/L R1507727-154113 38 3050ND38.6 56.4
Fluoranthene ug/L R1508342-157117 34 3050ND41.4 58.5
Fluorene ug/L R1507725-155114 39 3050ND38.5 57.2
Hexachloro-1,3-butadiene ug/L 50 30 10-13037 20 3050ND15.0 18.4
Hexachlorobenzene ug/L R1507432-145111 40 3050ND37.2 55.6
Hexachlorocyclopentadiene ug/L 50 55 10-13072 27 3050ND27.4 36.1
Hexachloroethane ug/L R1502510-13037 37 3050ND12.7 18.5
Indeno(1,2,3-cd)pyrene ug/L R1508539-174118 33 3050ND42.4 59.2
Isophorone ug/L R1507419-146108 37 3050ND37.0 53.9
N-Nitroso-di-n-propylamine ug/L R1507320-150114 45 3050ND36.3 57.1
N-Nitrosodimethylamine ug/L R1,v1507313-130112 42 3050ND36.6 56.2
N-Nitrosodiphenylamine ug/L R1508033-149118 38 3050ND40.2 59.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3947626MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655398001
3947627
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Naphthalene ug/L 50 56 10-12872 26 3050ND27.9 36.1
Nitrobenzene ug/L R1507119-145100 33 3050ND35.6 49.8
Pentachlorophenol ug/L R11006810-188107 45 30100ND68.2 107
Phenanthrene ug/L R1508038-150115 35 3050ND40.2 57.4
Phenol ug/L R1504410-13067 41 3050ND22.1 33.4
Pyrene ug/L R1508642-163126 38 3050ND43.0 63.2
2,4,6-Tribromophenol (S) %84 10-164119
2-Fluorobiphenyl (S)%75 10-130103
2-Fluorophenol (S)%57 10-13079
Nitrobenzene-d5 (S)%73 10-138100
Phenol-d6 (S)%45 10-13064
Terphenyl-d14 (S)%86 19-191118
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 55
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 51 of 55
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92655680
GEORGE FERN FDI-001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92655680001 760673 760741OFF-MW-1 EPA 3010A EPA 6020B
92655680002 760673 760741OFF-MW-5 EPA 3010A EPA 6020B
92655680003 760673 760741OFF-MW-6 EPA 3010A EPA 6020B
92655680004 760673 760741OFF-MW-7 EPA 3010A EPA 6020B
92655680005 760673 760741MW-11S EPA 3010A EPA 6020B
92655680006 760673 760741GW-DUP EPA 3010A EPA 6020B
92655680001 760869 760963OFF-MW-1 EPA 7470A EPA 7470A
92655680002 760869 760963OFF-MW-5 EPA 7470A EPA 7470A
92655680003 760869 760963OFF-MW-6 EPA 7470A EPA 7470A
92655680004 760869 760963OFF-MW-7 EPA 7470A EPA 7470A
92655680005 760869 760963MW-11S EPA 7470A EPA 7470A
92655680006 760869 760963GW-DUP EPA 7470A EPA 7470A
92655680001 760065 760344OFF-MW-1 EPA 3510C EPA 8270E
92655680002 760065 760344OFF-MW-5 EPA 3510C EPA 8270E
92655680003 760065 760344OFF-MW-6 EPA 3510C EPA 8270E
92655680004 760065 760344OFF-MW-7 EPA 3510C EPA 8270E
92655680005 760065 760344MW-11S EPA 3510C EPA 8270E
92655680006 760065 760344GW-DUP EPA 3510C EPA 8270E
92655680001 760455OFF-MW-1 EPA 8260D
92655680002 760455OFF-MW-5 EPA 8260D
92655680003 760455OFF-MW-6 EPA 8260D
92655680004 760191OFF-MW-7 EPA 8260D
92655680005 760191MW-11S EPA 8260D
92655680006 760455GW-DUP EPA 8260D
92655680007 760191TRIP BLANK EPA 8260D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
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Huntersville, NC 28078
[phone]
Page 52 of 55
Page 53 of 55
Page 54 of 55
Page 55 of 55
04/07/23
Technical Report for
Hart & Hickman
George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
FD1.001
SGS Job Number: JD62844
Sampling Dates: 03/08/23 - 03/13/23
Report to:
Hart & Hickman
2923 South Tyron Street Suite 101
Charlotte, NC 28203
[e-mail]
ATTN: Haley Martin
Total number of pages in report:
Certifications: NJ(12129), NY(10983), CA, CT, FL, IL, IN, KS, KY, LA, MA, MD, ME, MN, NC,
OH VAP (CL0056), AK (UST-103), AZ (AZ0786), PA(68-00408), RI, SC, TX, UT, VA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 2235 Route 130 • Dayton, NJ 08810 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Kelly Ramos 732-329-0200
David Chastain
General Manager
Dayton, NJ 04/07/23
e-Hardcopy 2.0
Automated Report
100
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 100
JD62844
Table of Contents
-1-
Sections:
Section 1: Sample Summary ................................................................................................... 3
Section 2: Summary of Hits .................................................................................................... 5
Section 3: Sample Results ........................................................................................................11
3.1: JD62844-1: BF-SSV-12 ................................................................................................ 12
3.2: JD62844-2: BF-SSV-01 ................................................................................................ 14
3.3: JD62844-3: BF-SSV-02 ................................................................................................ 16
3.4: JD62844-4: BF-SSV-03 ................................................................................................ 18
3.5: JD62844-5: BF-SSV-04 ................................................................................................ 20
3.6: JD62844-6: BF-SSV-05 ................................................................................................ 22
3.7: JD62844-7: BF-SSV-06 ................................................................................................ 24
3.8: JD62844-8: BF-SSV-07 ................................................................................................ 26
3.9: JD62844-9: BF-SSV-08 ................................................................................................ 28
3.10: JD62844-10: BF-SSV-09 ............................................................................................ 30
3.11: JD62844-11: BF-SSV-11 ............................................................................................ 32
3.12: JD62844-12: BF-SSV-DUP ........................................................................................ 34
3.13: JD62844-13: BF-SSV-10 ............................................................................................ 36
Section 4: Misc. Forms ............................................................................................................38
4.1: Chain of Custody ........................................................................................................... 39
4.2: Summa Canister and Flow Controller Log .................................................................... 43
Section 5: MS Volatiles - QC Data Summaries ..................................................................... 44
5.1: Method Blank Summary ................................................................................................ 45
5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 57
5.3: Duplicate Summary ....................................................................................................... 69
5.4: Summa Cleaning Certification ...................................................................................... 71
5.5: Instrument Performance Checks (BFB) ......................................................................... 85
5.6: Surrogate Recovery Summaries ..................................................................................... 99 123452 of 100
JD62844
SGS North America Inc.
Sample Summary
Hart & Hickman
Job No:JD62844
George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Project No: FD1.001
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
JD62844-1 03/08/23 09:37 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-12
JD62844-2 03/08/23 10:43 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-01
JD62844-3 03/08/23 11:05 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-02
JD62844-4 03/08/23 11:37 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-03
JD62844-5 03/08/23 12:16 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-04
JD62844-6 03/08/23 12:52 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-05
JD62844-7 03/08/23 13:05 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-06
JD62844-8 03/08/23 14:13 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-07
JD62844-9 03/08/23 14:38 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-08
JD62844-10 03/08/23 15:03 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-09
JD62844-11 03/13/23 15:48 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-11
JD62844-12 03/13/23 15:48 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-DUP
3 of 100
JD628441
SGS North America Inc.
Sample Summary
(continued)
Hart & Hickman
Job No:JD62844
George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Project No: FD1.001
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
JD62844-13 03/13/23 16:15 TJS 03/29/23 AIR Soil Vapor Comp.BF-SSV-10
4 of 100
JD628441
Summary of Hits Page 1 of 6
Job Number:JD62844
Account:Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Collected:03/08/23 thru 03/13/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
JD62844-1 BF-SSV-12
Acetone (2-Propanone)16.1 0.80 0.58 ppbv TO-15
Cyclohexane 0.50 J 0.80 0.44 ppbv TO-15
Dichlorodifluoromethane 0.54 J 0.80 0.13 ppbv TO-15
Isopropyl Alcohol 3.7 0.80 0.56 ppbv TO-15
Methylene chloride 1.6 0.80 0.22 ppbv TO-15
Methyl ethyl ketone 0.61 J 0.80 0.44 ppbv TO-15
Tetrachloroethylene 7.3 0.16 0.056 ppbv TO-15
Trichloroethylene 18.4 0.16 0.076 ppbv TO-15
Acetone (2-Propanone)38.2 1.9 1.4 ug/m3 TO-15
Cyclohexane 1.7 J 2.8 1.5 ug/m3 TO-15
Dichlorodifluoromethane 2.7 J 4.0 0.64 ug/m3 TO-15
Isopropyl Alcohol 9.1 2.0 1.4 ug/m3 TO-15
Methylene chloride 5.6 2.8 0.76 ug/m3 TO-15
Methyl ethyl ketone 1.8 J 2.4 1.3 ug/m3 TO-15
Tetrachloroethylene 50 1.1 0.38 ug/m3 TO-15
Trichloroethylene 98.9 0.86 0.41 ug/m3 TO-15
JD62844-2 BF-SSV-01
Acetone (2-Propanone)12.9 0.80 0.58 ppbv TO-15
Dichlorodifluoromethane 0.41 J 0.80 0.13 ppbv TO-15
Isopropyl Alcohol 2.1 0.80 0.56 ppbv TO-15
Methyl ethyl ketone 0.95 0.80 0.44 ppbv TO-15
Tetrachloroethylene 73.0 0.16 0.056 ppbv TO-15
Toluene 0.41 J 0.80 0.23 ppbv TO-15
Trichloroethylene 1.1 0.16 0.076 ppbv TO-15
Acetone (2-Propanone)30.6 1.9 1.4 ug/m3 TO-15
Dichlorodifluoromethane 2.0 J 4.0 0.64 ug/m3 TO-15
Isopropyl Alcohol 5.2 2.0 1.4 ug/m3 TO-15
Methyl ethyl ketone 2.8 2.4 1.3 ug/m3 TO-15
Tetrachloroethylene 495 1.1 0.38 ug/m3 TO-15
Toluene 1.5 J 3.0 0.87 ug/m3 TO-15
Trichloroethylene 5.9 0.86 0.41 ug/m3 TO-15
JD62844-3 BF-SSV-02
Acetone (2-Propanone)47.4 0.80 0.58 ppbv TO-15
Benzene 0.39 J 0.80 0.25 ppbv TO-15
Cyclohexane 0.56 J 0.80 0.44 ppbv TO-15
Dichlorodifluoromethane 0.41 J 0.80 0.13 ppbv TO-15
Ethylbenzene 1.2 0.80 0.24 ppbv TO-15
Ethyl Acetate 4.1 0.80 0.42 ppbv TO-15
Isopropyl Alcohol 4.8 0.80 0.56 ppbv TO-15
5 of 100
JD628442
Summary of Hits Page 2 of 6
Job Number:JD62844
Account:Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Collected:03/08/23 thru 03/13/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Methylene chloride 2.8 0.80 0.22 ppbv TO-15
Tetrachloroethylene 4.5 0.16 0.056 ppbv TO-15
Toluene 4.4 0.80 0.23 ppbv TO-15
Trichloroethylene 0.95 0.16 0.076 ppbv TO-15
m,p-Xylene 1.2 0.80 0.56 ppbv TO-15
o-Xylene 0.60 J 0.80 0.31 ppbv TO-15
Xylenes (total)1.8 0.80 0.31 ppbv TO-15
Acetone (2-Propanone)113 1.9 1.4 ug/m3 TO-15
Benzene 1.2 J 2.6 0.80 ug/m3 TO-15
Cyclohexane 1.9 J 2.8 1.5 ug/m3 TO-15
Dichlorodifluoromethane 2.0 J 4.0 0.64 ug/m3 TO-15
Ethylbenzene 5.2 3.5 1.0 ug/m3 TO-15
Ethyl Acetate 15 2.9 1.5 ug/m3 TO-15
Isopropyl Alcohol 12 2.0 1.4 ug/m3 TO-15
Methylene chloride 9.7 2.8 0.76 ug/m3 TO-15
Tetrachloroethylene 31 1.1 0.38 ug/m3 TO-15
Toluene 17 3.0 0.87 ug/m3 TO-15
Trichloroethylene 5.1 0.86 0.41 ug/m3 TO-15
m,p-Xylene 5.2 3.5 2.4 ug/m3 TO-15
o-Xylene 2.6 J 3.5 1.3 ug/m3 TO-15
Xylenes (total)7.8 3.5 1.3 ug/m3 TO-15
JD62844-4 BF-SSV-03
Acetone (2-Propanone)23.7 0.80 0.58 ppbv TO-15
Dichlorodifluoromethane 0.47 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 1.8 0.80 0.42 ppbv TO-15
Isopropyl Alcohol 6.9 0.80 0.56 ppbv TO-15
Methylene chloride 1.7 0.80 0.22 ppbv TO-15
Methyl ethyl ketone 1.2 0.80 0.44 ppbv TO-15
Tetrachloroethylene 70.5 0.16 0.056 ppbv TO-15
Toluene 0.69 J 0.80 0.23 ppbv TO-15
Trichloroethylene 7.0 0.16 0.076 ppbv TO-15
Acetone (2-Propanone)56.3 1.9 1.4 ug/m3 TO-15
Dichlorodifluoromethane 2.3 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 6.5 2.9 1.5 ug/m3 TO-15
Isopropyl Alcohol 17 2.0 1.4 ug/m3 TO-15
Methylene chloride 5.9 2.8 0.76 ug/m3 TO-15
Methyl ethyl ketone 3.5 2.4 1.3 ug/m3 TO-15
Tetrachloroethylene 478 1.1 0.38 ug/m3 TO-15
Toluene 2.6 J 3.0 0.87 ug/m3 TO-15
Trichloroethylene 38 0.86 0.41 ug/m3 TO-15
6 of 100
JD628442
Summary of Hits Page 3 of 6
Job Number:JD62844
Account:Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Collected:03/08/23 thru 03/13/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
JD62844-5 BF-SSV-04
Acetone (2-Propanone)15.1 0.80 0.58 ppbv TO-15
Dichlorodifluoromethane 0.44 J 0.80 0.13 ppbv TO-15
Hexane 0.54 J 0.80 0.45 ppbv TO-15
Isopropyl Alcohol 4.8 0.80 0.56 ppbv TO-15
Methylene chloride 2.9 0.80 0.22 ppbv TO-15
Tetrachloroethylene 4.7 0.16 0.056 ppbv TO-15
Toluene 0.53 J 0.80 0.23 ppbv TO-15
Trichloroethylene 0.88 0.16 0.076 ppbv TO-15
Acetone (2-Propanone)35.9 1.9 1.4 ug/m3 TO-15
Dichlorodifluoromethane 2.2 J 4.0 0.64 ug/m3 TO-15
Hexane 1.9 J 2.8 1.6 ug/m3 TO-15
Isopropyl Alcohol 12 2.0 1.4 ug/m3 TO-15
Methylene chloride 10 2.8 0.76 ug/m3 TO-15
Tetrachloroethylene 32 1.1 0.38 ug/m3 TO-15
Toluene 2.0 J 3.0 0.87 ug/m3 TO-15
Trichloroethylene 4.7 0.86 0.41 ug/m3 TO-15
JD62844-6 BF-SSV-05
Acetone (2-Propanone)14.8 0.80 0.58 ppbv TO-15
Cyclohexane 0.52 J 0.80 0.44 ppbv TO-15
Dichlorodifluoromethane 0.45 J 0.80 0.13 ppbv TO-15
Isopropyl Alcohol 4.1 0.80 0.56 ppbv TO-15
Tetrachloroethylene 76.8 0.16 0.056 ppbv TO-15
Toluene 0.62 J 0.80 0.23 ppbv TO-15
Trichloroethylene 2.7 0.16 0.076 ppbv TO-15
Acetone (2-Propanone)35.2 1.9 1.4 ug/m3 TO-15
Cyclohexane 1.8 J 2.8 1.5 ug/m3 TO-15
Dichlorodifluoromethane 2.2 J 4.0 0.64 ug/m3 TO-15
Isopropyl Alcohol 10 2.0 1.4 ug/m3 TO-15
Tetrachloroethylene 521 1.1 0.38 ug/m3 TO-15
Toluene 2.3 J 3.0 0.87 ug/m3 TO-15
Trichloroethylene 15 0.86 0.41 ug/m3 TO-15
JD62844-7 BF-SSV-06
Acetone (2-Propanone)14.8 0.80 0.58 ppbv TO-15
Dichlorodifluoromethane 0.45 J 0.80 0.13 ppbv TO-15
Isopropyl Alcohol 3.0 0.80 0.56 ppbv TO-15
Methylene chloride 1.7 0.80 0.22 ppbv TO-15
Tetrachloroethylene 63.4 0.16 0.056 ppbv TO-15
Toluene 0.80 0.80 0.23 ppbv TO-15
Trichloroethylene 1.5 0.16 0.076 ppbv TO-15
7 of 100
JD628442
Summary of Hits Page 4 of 6
Job Number:JD62844
Account:Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Collected:03/08/23 thru 03/13/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Acetone (2-Propanone)35.2 1.9 1.4 ug/m3 TO-15
Dichlorodifluoromethane 2.2 J 4.0 0.64 ug/m3 TO-15
Isopropyl Alcohol 7.4 2.0 1.4 ug/m3 TO-15
Methylene chloride 5.9 2.8 0.76 ug/m3 TO-15
Tetrachloroethylene 430 1.1 0.38 ug/m3 TO-15
Toluene 3.0 3.0 0.87 ug/m3 TO-15
Trichloroethylene 8.1 0.86 0.41 ug/m3 TO-15
JD62844-8 BF-SSV-07
Acetone (2-Propanone)17.1 0.80 0.58 ppbv TO-15
Cyclohexane 0.47 J 0.80 0.44 ppbv TO-15
Dichlorodifluoromethane 0.49 J 0.80 0.13 ppbv TO-15
Hexane 0.47 J 0.80 0.45 ppbv TO-15
Isopropyl Alcohol 3.8 0.80 0.56 ppbv TO-15
Methylene chloride 1.8 0.80 0.22 ppbv TO-15
Methyl ethyl ketone 1.1 0.80 0.44 ppbv TO-15
Tetrachloroethylene 5.8 0.16 0.056 ppbv TO-15
Toluene 0.56 J 0.80 0.23 ppbv TO-15
Trichloroethylene 0.62 0.16 0.076 ppbv TO-15
Acetone (2-Propanone)40.6 1.9 1.4 ug/m3 TO-15
Cyclohexane 1.6 J 2.8 1.5 ug/m3 TO-15
Dichlorodifluoromethane 2.4 J 4.0 0.64 ug/m3 TO-15
Hexane 1.7 J 2.8 1.6 ug/m3 TO-15
Isopropyl Alcohol 9.3 2.0 1.4 ug/m3 TO-15
Methylene chloride 6.3 2.8 0.76 ug/m3 TO-15
Methyl ethyl ketone 3.2 2.4 1.3 ug/m3 TO-15
Tetrachloroethylene 39 1.1 0.38 ug/m3 TO-15
Toluene 2.1 J 3.0 0.87 ug/m3 TO-15
Trichloroethylene 3.3 0.86 0.41 ug/m3 TO-15
JD62844-9 BF-SSV-08
Acetone (2-Propanone)15.3 0.80 0.58 ppbv TO-15
Dichlorodifluoromethane 0.43 J 0.80 0.13 ppbv TO-15
Hexane 0.46 J 0.80 0.45 ppbv TO-15
Isopropyl Alcohol 5.0 0.80 0.56 ppbv TO-15
Methylene chloride 1.9 0.80 0.22 ppbv TO-15
Tetrachloroethylene 35.4 0.16 0.056 ppbv TO-15
Toluene 0.56 J 0.80 0.23 ppbv TO-15
Trichloroethylene 1.4 0.16 0.076 ppbv TO-15
Acetone (2-Propanone)36.3 1.9 1.4 ug/m3 TO-15
Dichlorodifluoromethane 2.1 J 4.0 0.64 ug/m3 TO-15
Hexane 1.6 J 2.8 1.6 ug/m3 TO-15
Isopropyl Alcohol 12 2.0 1.4 ug/m3 TO-15
8 of 100
JD628442
Summary of Hits Page 5 of 6
Job Number:JD62844
Account:Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Collected:03/08/23 thru 03/13/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Methylene chloride 6.6 2.8 0.76 ug/m3 TO-15
Tetrachloroethylene 240 1.1 0.38 ug/m3 TO-15
Toluene 2.1 J 3.0 0.87 ug/m3 TO-15
Trichloroethylene 7.5 0.86 0.41 ug/m3 TO-15
JD62844-10 BF-SSV-09
Acetone (2-Propanone)14.9 0.80 0.58 ppbv TO-15
Dichlorodifluoromethane 0.42 J 0.80 0.13 ppbv TO-15
Isopropyl Alcohol 4.4 0.80 0.56 ppbv TO-15
Methylene chloride 2.6 0.80 0.22 ppbv TO-15
Tetrachloroethylene 32.8 0.16 0.056 ppbv TO-15
Toluene 0.76 J 0.80 0.23 ppbv TO-15
Trichloroethylene 0.96 0.16 0.076 ppbv TO-15
Acetone (2-Propanone)35.4 1.9 1.4 ug/m3 TO-15
Dichlorodifluoromethane 2.1 J 4.0 0.64 ug/m3 TO-15
Isopropyl Alcohol 11 2.0 1.4 ug/m3 TO-15
Methylene chloride 9.0 2.8 0.76 ug/m3 TO-15
Tetrachloroethylene 222 1.1 0.38 ug/m3 TO-15
Toluene 2.9 J 3.0 0.87 ug/m3 TO-15
Trichloroethylene 5.2 0.86 0.41 ug/m3 TO-15
JD62844-11 BF-SSV-11
Acetone (2-Propanone)12.7 0.80 0.58 ppbv TO-15
Dichlorodifluoromethane 0.43 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 12.1 0.80 0.42 ppbv TO-15
Hexane 0.80 0.80 0.45 ppbv TO-15
Isopropyl Alcohol 4.6 0.80 0.56 ppbv TO-15
Methylene chloride 2.4 0.80 0.22 ppbv TO-15
Propylene 3.2 2.0 0.57 ppbv TO-15
Tetrachloroethylene 0.31 0.16 0.056 ppbv TO-15
Tetrahydrofuran 1.9 0.80 0.36 ppbv TO-15
Toluene 0.42 J 0.80 0.23 ppbv TO-15
Acetone (2-Propanone)30.2 1.9 1.4 ug/m3 TO-15
Dichlorodifluoromethane 2.1 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 43.6 2.9 1.5 ug/m3 TO-15
Hexane 2.8 2.8 1.6 ug/m3 TO-15
Isopropyl Alcohol 11 2.0 1.4 ug/m3 TO-15
Methylene chloride 8.3 2.8 0.76 ug/m3 TO-15
Propylene 5.5 3.4 0.98 ug/m3 TO-15
Tetrachloroethylene 2.1 1.1 0.38 ug/m3 TO-15
Tetrahydrofuran 5.6 2.4 1.1 ug/m3 TO-15
Toluene 1.6 J 3.0 0.87 ug/m3 TO-15
9 of 100
JD628442
Summary of Hits Page 6 of 6
Job Number:JD62844
Account:Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Collected:03/08/23 thru 03/13/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
JD62844-12 BF-SSV-DUP
Acetone (2-Propanone)11.8 0.80 0.58 ppbv TO-15
Dichlorodifluoromethane 0.43 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 16.1 0.80 0.42 ppbv TO-15
Hexane 0.49 J 0.80 0.45 ppbv TO-15
Isopropyl Alcohol 4.6 0.80 0.56 ppbv TO-15
Methylene chloride 1.4 0.80 0.22 ppbv TO-15
Tetrachloroethylene 0.29 0.16 0.056 ppbv TO-15
Toluene 0.45 J 0.80 0.23 ppbv TO-15
Acetone (2-Propanone)28.0 1.9 1.4 ug/m3 TO-15
Dichlorodifluoromethane 2.1 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 57.9 2.9 1.5 ug/m3 TO-15
Hexane 1.7 J 2.8 1.6 ug/m3 TO-15
Isopropyl Alcohol 11 2.0 1.4 ug/m3 TO-15
Methylene chloride 4.9 2.8 0.76 ug/m3 TO-15
Tetrachloroethylene 2.0 1.1 0.38 ug/m3 TO-15
Toluene 1.7 J 3.0 0.87 ug/m3 TO-15
JD62844-13 BF-SSV-10
Acetone (2-Propanone)8.3 0.80 0.58 ppbv TO-15
Dichlorodifluoromethane 0.43 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 11.8 0.80 0.42 ppbv TO-15
Hexane 0.63 J 0.80 0.45 ppbv TO-15
Isopropyl Alcohol 3.7 0.80 0.56 ppbv TO-15
Methylene chloride 2.8 0.80 0.22 ppbv TO-15
Tetrachloroethylene 8.8 0.16 0.056 ppbv TO-15
Toluene 0.66 J 0.80 0.23 ppbv TO-15
Trichloroethylene 0.44 0.16 0.076 ppbv TO-15
Acetone (2-Propanone)20 1.9 1.4 ug/m3 TO-15
Dichlorodifluoromethane 2.1 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 42.5 2.9 1.5 ug/m3 TO-15
Hexane 2.2 J 2.8 1.6 ug/m3 TO-15
Isopropyl Alcohol 9.1 2.0 1.4 ug/m3 TO-15
Methylene chloride 9.7 2.8 0.76 ug/m3 TO-15
Tetrachloroethylene 60 1.1 0.38 ug/m3 TO-15
Toluene 2.5 J 3.0 0.87 ug/m3 TO-15
Trichloroethylene 2.4 0.86 0.41 ug/m3 TO-15
10 of 100
JD628442
SGS North America Inc.
Sample Results
Report of Analysis
Dayton, NJ
Section 3
11 of 100
JD628443
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-12
Lab Sample ID:JD62844-1 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2330 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01367.D 1 04/04/23 14:39 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)16.1 0.80 0.58 ppbv 38.2 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane 0.50 0.80 0.44 ppbv J 1.7 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.54 0.80 0.13 ppbv J 2.7 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 3.7 0.80 0.56 ppbv 9.1 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 1.6 0.80 0.22 ppbv 5.6 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 0.61 0.80 0.44 ppbv J 1.8 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 7.3 0.16 0.056 ppbv 50 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 100
JD6284433.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-12
Lab Sample ID:JD62844-1 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2330 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene ND 0.80 0.23 ppbv ND 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene 18.4 0.16 0.076 ppbv 98.9 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 90%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 100
JD6284433.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-01
Lab Sample ID:JD62844-2 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2209 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01369.D 1 04/04/23 16:02 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)12.9 0.80 0.58 ppbv 30.6 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.41 0.80 0.13 ppbv J 2.0 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 2.1 0.80 0.56 ppbv 5.2 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride ND 0.80 0.22 ppbv ND 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 0.95 0.80 0.44 ppbv 2.8 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 73.0 0.16 0.056 ppbv 495 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 100
JD6284433.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-01
Lab Sample ID:JD62844-2 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2209 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.41 0.80 0.23 ppbv J 1.5 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene 1.1 0.16 0.076 ppbv 5.9 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 89%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 100
JD6284433.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-02
Lab Sample ID:JD62844-3 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2222 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01370.D 1 04/04/23 16:36 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)47.4 0.80 0.58 ppbv 113 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene 0.39 0.80 0.25 ppbv J 1.2 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane 0.56 0.80 0.44 ppbv J 1.9 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.41 0.80 0.13 ppbv J 2.0 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene 1.2 0.80 0.24 ppbv 5.2 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 4.1 0.80 0.42 ppbv 15 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 4.8 0.80 0.56 ppbv 12 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 2.8 0.80 0.22 ppbv 9.7 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 4.5 0.16 0.056 ppbv 31 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 100
JD6284433.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-02
Lab Sample ID:JD62844-3 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2222 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 4.4 0.80 0.23 ppbv 17 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene 0.95 0.16 0.076 ppbv 5.1 0.86 0.41 ug/m3
106.2 m,p-Xylene 1.2 0.80 0.56 ppbv 5.2 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene 0.60 0.80 0.31 ppbv J 2.6 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)1.8 0.80 0.31 ppbv 7.8 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 90%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 100
JD6284433.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-03
Lab Sample ID:JD62844-4 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2205 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01371.D 1 04/04/23 17:11 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)23.7 0.80 0.58 ppbv 56.3 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.47 0.80 0.13 ppbv J 2.3 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 1.8 0.80 0.42 ppbv 6.5 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 6.9 0.80 0.56 ppbv 17 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 1.7 0.80 0.22 ppbv 5.9 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 1.2 0.80 0.44 ppbv 3.5 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 70.5 0.16 0.056 ppbv 478 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 100
JD6284433.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-03
Lab Sample ID:JD62844-4 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2205 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.69 0.80 0.23 ppbv J 2.6 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene 7.0 0.16 0.076 ppbv 38 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 92%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 100
JD6284433.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-04
Lab Sample ID:JD62844-5 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2331 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01372.D 1 04/04/23 17:45 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)15.1 0.80 0.58 ppbv 35.9 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.44 0.80 0.13 ppbv J 2.2 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane 0.54 0.80 0.45 ppbv J 1.9 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 4.8 0.80 0.56 ppbv 12 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 2.9 0.80 0.22 ppbv 10 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 4.7 0.16 0.056 ppbv 32 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 100
JD6284433.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-04
Lab Sample ID:JD62844-5 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2331 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.53 0.80 0.23 ppbv J 2.0 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene 0.88 0.16 0.076 ppbv 4.7 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 90%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 100
JD6284433.5
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-05
Lab Sample ID:JD62844-6 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2251 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01373.D 1 04/04/23 18:19 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)14.8 0.80 0.58 ppbv 35.2 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane 0.52 0.80 0.44 ppbv J 1.8 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.45 0.80 0.13 ppbv J 2.2 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 4.1 0.80 0.56 ppbv 10 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride ND 0.80 0.22 ppbv ND 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 76.8 0.16 0.056 ppbv 521 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 100
JD6284433.6
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-05
Lab Sample ID:JD62844-6 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2251 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.62 0.80 0.23 ppbv J 2.3 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene 2.7 0.16 0.076 ppbv 15 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 90%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 100
JD6284433.6
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-06
Lab Sample ID:JD62844-7 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2199 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01374.D 1 04/04/23 18:53 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)14.8 0.80 0.58 ppbv 35.2 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.45 0.80 0.13 ppbv J 2.2 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 3.0 0.80 0.56 ppbv 7.4 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 1.7 0.80 0.22 ppbv 5.9 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 63.4 0.16 0.056 ppbv 430 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 100
JD6284433.7
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-06
Lab Sample ID:JD62844-7 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2199 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.80 0.80 0.23 ppbv 3.0 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene 1.5 0.16 0.076 ppbv 8.1 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 91%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 100
JD6284433.7
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-07
Lab Sample ID:JD62844-8 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2317 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01375.D 1 04/04/23 19:28 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)17.1 0.80 0.58 ppbv 40.6 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane 0.47 0.80 0.44 ppbv J 1.6 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.49 0.80 0.13 ppbv J 2.4 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane 0.47 0.80 0.45 ppbv J 1.7 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 3.8 0.80 0.56 ppbv 9.3 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 1.8 0.80 0.22 ppbv 6.3 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 1.1 0.80 0.44 ppbv 3.2 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 5.8 0.16 0.056 ppbv 39 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 100
JD6284433.8
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-07
Lab Sample ID:JD62844-8 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2317 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.56 0.80 0.23 ppbv J 2.1 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene 0.62 0.16 0.076 ppbv 3.3 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 90%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 100
JD6284433.8
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-08
Lab Sample ID:JD62844-9 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2332 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01376.D 1 04/04/23 20:03 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)15.3 0.80 0.58 ppbv 36.3 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.43 0.80 0.13 ppbv J 2.1 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane 0.46 0.80 0.45 ppbv J 1.6 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 5.0 0.80 0.56 ppbv 12 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 1.9 0.80 0.22 ppbv 6.6 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 35.4 0.16 0.056 ppbv 240 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 100
JD6284433.9
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-08
Lab Sample ID:JD62844-9 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2332 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.56 0.80 0.23 ppbv J 2.1 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene 1.4 0.16 0.076 ppbv 7.5 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 91%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 100
JD6284433.9
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-09
Lab Sample ID:JD62844-10 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2220 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01377.D 1 04/04/23 20:38 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)14.9 0.80 0.58 ppbv 35.4 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.42 0.80 0.13 ppbv J 2.1 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 4.4 0.80 0.56 ppbv 11 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 2.6 0.80 0.22 ppbv 9.0 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 32.8 0.16 0.056 ppbv 222 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 100
JD6284433.10
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-09
Lab Sample ID:JD62844-10 Date Sampled:03/08/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2220 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.76 0.80 0.23 ppbv J 2.9 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene 0.96 0.16 0.076 ppbv 5.2 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 90%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 100
JD6284433.10
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-11
Lab Sample ID:JD62844-11 Date Sampled:03/13/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2313 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01378.D 1 04/04/23 21:13 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)12.7 0.80 0.58 ppbv 30.2 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.43 0.80 0.13 ppbv J 2.1 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 12.1 0.80 0.42 ppbv 43.6 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane 0.80 0.80 0.45 ppbv 2.8 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 4.6 0.80 0.56 ppbv 11 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 2.4 0.80 0.22 ppbv 8.3 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene 3.2 2.0 0.57 ppbv 5.5 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 0.31 0.16 0.056 ppbv 2.1 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 100
JD6284433.11
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-11
Lab Sample ID:JD62844-11 Date Sampled:03/13/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2313 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran 1.9 0.80 0.36 ppbv 5.6 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.42 0.80 0.23 ppbv J 1.6 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 91%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 100
JD6284433.11
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-DUP
Lab Sample ID:JD62844-12 Date Sampled:03/13/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2326 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01379.D 1 04/04/23 21:47 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)11.8 0.80 0.58 ppbv 28.0 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.43 0.80 0.13 ppbv J 2.1 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 16.1 0.80 0.42 ppbv 57.9 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane 0.49 0.80 0.45 ppbv J 1.7 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 4.6 0.80 0.56 ppbv 11 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 1.4 0.80 0.22 ppbv 4.9 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 0.29 0.16 0.056 ppbv 2.0 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 100
JD6284433.12
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-DUP
Lab Sample ID:JD62844-12 Date Sampled:03/13/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A2326 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.45 0.80 0.23 ppbv J 1.7 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 90%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 100
JD6284433.12
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:BF-SSV-10
Lab Sample ID:JD62844-13 Date Sampled:03/13/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A1976 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 7W01380.D 1 04/04/23 22:22 TCH n/a n/a V7W62
Run #2
Initial Volume
Run #1 100 ml
Run #2
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)8.3 0.80 0.58 ppbv 20 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.43 0.80 0.13 ppbv J 2.1 4.0 0.64 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 11.8 0.80 0.42 ppbv 42.5 2.9 1.5 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene
a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane 0.63 0.80 0.45 ppbv J 2.2 2.8 1.6 ug/m3
67-63-0 60.1 Isopropyl Alcohol 3.7 0.80 0.56 ppbv 9.1 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 2.8 0.80 0.22 ppbv 9.7 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 8.8 0.16 0.056 ppbv 60 1.1 0.38 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 100
JD6284433.13
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:BF-SSV-10
Lab Sample ID:JD62844-13 Date Sampled:03/13/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A1976 Date Received:03/29/23
Method:TO-15 Percent Solids:n/a
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
VTO15 Special list
CAS No. MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.66 0.80 0.23 ppbv J 2.5 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene 0.44 0.16 0.076 ppbv 2.4 0.86 0.41 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 91%65-128%
(a) Associated CCV outside of control limits high, sample was ND. This compound in blank spike is outside in house
QC limits bias high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 100
JD6284433.13
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
• Summa Canister and Flow Controller Log
Dayton, NJ
Section 4
38 of 100
JD628444
h\p CHAIN OF CUSTODY.AIR
SGS North America lnc. . Da)don
2235 Roule 130, Day1on, NJ 00610
TEL. 732,329-0200 FA)1 732-329-U99
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JD62844: Chain of Custody
Page 1 of 4
39 of 100
JD6284444.1
CHAIN OF CUSTODY . AIR PAGE C OF Q
SGS North America lnc. - Dayton
2235 Rouie 130, Daylon, NJ 08810
TEL 732-32S0200 FAX 732-32S3499
FED.EXTEcking#kll-016r'l - ) q7
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JD62844: Chain of Custody
Page 2 of 4
40 of 100
JD6284444.1
CLIENTAIN SRT*APLING EQUIPT.AENT RETUNN FONVTH\WPROJECT:G."Fern (f8-oau il3-rq-i-;-D {'arvqJOB #CONTROL#AoDrrroNAL SUMMA CANISTERSNOTES:RoXADDITIONAL CONTROLLERS-ty1(-tsDATE &TIME:RECEIVEDBY:23DATE &TIME:REUNQUISHED BY:,|DATE &TIME:RECEIVEDBY:4DATE &TIME:REUNQUISHED BY:3# OF BOXES OR PIECES IN DELIVERYCusropY SEAL #'s:sM086-03Pub date: 3/12118Iax7ao,OCJD62844: Chain of Custody
Page 3 of 4
41 of 100
JD6284444.1
Job Number:JD62844 Client:SGS - CHARLOTTE SERVICE CENTER
Date / Time Received:3/29/2023 10:30:00 AM Delivery Method:
Project:CANISTER STOCK
4. No. Coolers:N/A
Airbill #'s:
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Cooler temp verification:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
N/A
N/A
Quality Control Preservatio Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
SM089-03Rev. Date 12/7/17
SGS Sample Receipt Summary
Test Strip Lot #s:pH 1-12:231619 pH 12+:203117A Other: (Specify)
JD62844: Chain of Custody
Page 4 of 4
42 of 100
JD6284444.1
Summa Canister and Flow Controller Log Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Received:03/29/23
SUMMA CANISTERS
Shipping Receiving
Summa Vac Date SCC SCC Sample Date Vac Pres Final Dil
ID L " Hg Out By Batch FileID Number In By " Hg psig psig Fact
A2330 1.4 29.4 02/08/23 ML CP120403W78744.D JD62844-1 03/29/23 DG 6 1
A2209 1.4 29.4 02/08/23 ML CP119986W27625.D JD62844-2 03/29/23 DG 5 1
A2222 1.4 29.4 02/08/23 ML CP119963W78330.D JD62844-3 03/29/23 DG 3.5 1
A2205 1.4 29.4 02/08/23 ML CP119986W27625.D JD62844-4 03/29/23 DG 5.5 1
A2331 1.4 29.4 02/08/23 ML CP120403W78744.D JD62844-5 03/29/23 DG 6 1
A2251 1.4 29.4 02/08/23 ML CP119986W27625.D JD62844-6 03/29/23 DG 5 1
A2199 1.4 29.4 02/08/23 ML CP119963W78330.D JD62844-7 03/29/23 DG 7 1
A2317 1.4 29.4 02/08/23 ML CP120372W62771.D JD62844-8 03/29/23 DG 5.5 1
A2332 1.4 29.4 02/08/23 ML CP120403W78744.D JD62844-9 03/29/23 DG 7 1
A2220 1.4 29.4 02/08/23 ML CP120013W78333.D JD62844-10 03/29/23 DG 7.5 1
A2313 1.4 29.4 03/07/23 ML CP119943W78343.D JD62844-11 03/29/23 DG 6.5 1
A2326 1.4 29.4 03/07/23 ML CP120403W78744.D JD62844-12 03/29/23 DG 6 1
A1976 1.4 29.4 03/07/23 ML CP120593W79066.D JD62844-13 03/29/23 DG 4.5 1
FLOW CONTROLLERS / OTHER
Shipping Receiving
Flow Date cc/ Time Date cc/ Flow
Crtl ID Out By min hrs. In By min RPD Equipment Type
FC365 02/08/23 ML 107 .1667 03/29/23 DG 97 9.8 Flow Controller
FC546 02/08/23 ML 109 .1667 03/29/23 DG 107 1.9 Flow Controller
FC661 02/08/23 ML 107 .1667 03/30/23 DG 109 1.9 Flow Controller
FC703 02/08/23 ML 106 .1667 03/29/23 DG 109 2.8 Flow Controller
FC770 02/08/23 ML 108 .1667 03/29/23 DG 92 16 Flow Controller
FC897 03/07/23 ML 100 .1667 03/29/23 DG 91 9.4 Flow Controller
FC989 02/08/23 ML 108 .1667 03/30/23 DG 108 0 Flow Controller
MC228 02/08/23 ML 107 .1667 03/30/23 DG 107 0 Flow Controller
MC270 02/08/23 ML 107 .1667 03/29/23 DG 104 2.8 Flow Controller
FC1019 02/08/23 ML 107 .1667 03/29/23 DG 103 3.8 Flow Controller
FC1050 02/08/23 ML 107 .1667 03/29/23 DG 104 2.8 Flow Controller
FC1194 03/07/23 ML 100 .1667 03/30/23 DG 106 5.8 Flow Controller
FC1241 03/07/23 ML 101 .1667 03/29/23 DG 93 8.2 Flow Controller
FC1249 03/07/23 ML 100 .1667 03/30/23 DG 106 5.8 Flow Controller
SGS Bottle Order(s):
KR-02623-147
KR-03723-21
Prep Date Room Temp(F) Bar Pres "Hg
02/08/23 70 29.92
03/07/23 70 29.92
43 of 100
JD6284444.2
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
• Instrument Performance Checks (BFB)
• Surrogate Recovery Summaries
Dayton, NJ
Section 5
44 of 100
JD628445
Method Blank Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V7W62-MB 7W01366.D 1 04/04/23 TCH n/a n/a V7W62
The QC reported here applies to the following samples:Method: TO-15
JD62844-1, JD62844-2, JD62844-3, JD62844-4, JD62844-5, JD62844-6, JD62844-7, JD62844-8, JD62844-9, JD62844-
10, JD62844-11, JD62844-12, JD62844-13
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
45 of 100
JD6284455.1.1
Method Blank Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V7W62-MB 7W01366.D 1 04/04/23 TCH n/a n/a V7W62
The QC reported here applies to the following samples:Method: TO-15
JD62844-1, JD62844-2, JD62844-3, JD62844-4, JD62844-5, JD62844-6, JD62844-7, JD62844-8, JD62844-9, JD62844-
10, JD62844-11, JD62844-12, JD62844-13
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 90% 65-128%
46 of 100
JD6284455.1.1
Method Blank Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3085-MB 3W78324.D 1 12/11/22 TCH n/a n/a V3W3085
The QC reported here applies to the following samples:Method: TO-15
V3W3085-SCC
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
47 of 100
JD6284455.1.2
Method Blank Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3085-MB 3W78324.D 1 12/11/22 TCH n/a n/a V3W3085
The QC reported here applies to the following samples:Method: TO-15
V3W3085-SCC
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 100% 65-128%
48 of 100
JD6284455.1.2
Method Blank Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V6W1162-MB 6W27616.D 1 12/11/22 TCH n/a n/a V6W1162
The QC reported here applies to the following samples:Method: TO-15
V6W1162-SCC
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
49 of 100
JD6284455.1.3
Method Blank Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V6W1162-MB 6W27616.D 1 12/11/22 TCH n/a n/a V6W1162
The QC reported here applies to the following samples:Method: TO-15
V6W1162-SCC
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 95% 65-128%
50 of 100
JD6284455.1.3
Method Blank Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2791-MB 2W62755.D 1 01/06/23 TCH n/a n/a V2W2791
The QC reported here applies to the following samples:Method: TO-15
V2W2791-SCC
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
51 of 100
JD6284455.1.4
Method Blank Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2791-MB 2W62755.D 1 01/06/23 TCH n/a n/a V2W2791
The QC reported here applies to the following samples:Method: TO-15
V2W2791-SCC
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 110% 65-128%
52 of 100
JD6284455.1.4
Method Blank Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-MB 3W78735.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here applies to the following samples:Method: TO-15
V3W3101-SCC
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
53 of 100
JD6284455.1.5
Method Blank Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-MB 3W78735.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here applies to the following samples:Method: TO-15
V3W3101-SCC
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 99% 65-128%
54 of 100
JD6284455.1.5
Method Blank Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-MB 3W79064.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here applies to the following samples:Method: TO-15
V3W3115-SCC
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
55 of 100
JD6284455.1.6
Method Blank Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-MB 3W79064.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here applies to the following samples:Method: TO-15
V3W3115-SCC
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 96% 65-128%
56 of 100
JD6284455.1.6
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V7W62-BS 7W01362.D 1 04/04/23 TCH n/a n/a V7W62
V7W62-BSD 7W01363.D 1 04/04/23 TCH n/a n/a V7W62
The QC reported here applies to the following samples:Method: TO-15
JD62844-1, JD62844-2, JD62844-3, JD62844-4, JD62844-5, JD62844-6, JD62844-7, JD62844-8, JD62844-9, JD62844-
10, JD62844-11, JD62844-12, JD62844-13
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
67-64-1 Acetone (2-Propanone) 10 9.2 92 9.4 94 2 70-130/30
106-99-0 1,3-Butadiene 10 10.1 101 10.5 105 4 70-130/30
71-43-2 Benzene 10 8.0 80 8.4 84 5 70-130/30
75-15-0 Carbon disulfide 10 9.9 99 10.3 103 4 70-130/30
108-90-7 Chlorobenzene 10 9.4 94 9.5 95 1 70-130/30
67-66-3 Chloroform 10 8.5 85 8.8 88 3 70-130/30
74-87-3 Chloromethane 10 10.9 109 11.1 111 2 70-130/30
56-23-5 Carbon tetrachloride 10 8.7 87 9.1 91 4 70-130/30
110-82-7 Cyclohexane 10 8.7 87 8.8 88 1 70-130/30
75-34-3 1,1-Dichloroethane 10 8.5 85 8.9 89 5 70-130/30
75-35-4 1,1-Dichloroethylene 10 10.4 104 10.9 109 5 70-130/30
107-06-2 1,2-Dichloroethane 10 8.5 85 8.8 88 3 70-130/30
75-71-8 Dichlorodifluoromethane 10 9.2 92 9.4 94 2 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 8.5 85 8.7 87 2 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 8.3 83 8.8 88 6 70-130/30
95-50-1 o-Dichlorobenzene 10 11.6 116 11.6 116 0 70-130/30
100-41-4 Ethylbenzene 10 8.8 88 8.8 88 0 70-130/30
141-78-6 Ethyl Acetate 10 8.7 87 9.3 93 7 70-130/30
142-82-5 Heptane 10 9.0 90 9.2 92 2 70-130/30
87-68-3 Hexachlorobutadiene 10 14.8 148* a 14.8 148* a 0 70-130/30
110-54-3 Hexane 10 9.0 90 9.3 93 3 70-130/30
67-63-0 Isopropyl Alcohol 10 9.7 97 10.0 100 3 70-130/30
75-09-2 Methylene chloride 10 9.5 95 9.8 98 3 70-130/30
78-93-3 Methyl ethyl ketone 10 8.0 80 8.2 82 2 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 8.9 89 9.0 90 1 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 7.2 72 7.5 75 4 70-130/30
115-07-1 Propylene 10 8.3 83 8.5 85 2 70-130/30
71-55-6 1,1,1-Trichloroethane 10 8.4 84 8.7 87 4 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 9.3 93 9.2 92 1 70-130/30
79-00-5 1,1,2-Trichloroethane 10 8.6 86 8.7 87 1 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 11.8 118 11.7 117 1 70-130/30
127-18-4 Tetrachloroethylene 10 11.1 111 11.3 113 2 70-130/30
109-99-9 Tetrahydrofuran 10 8.0 80 8.4 84 5 70-130/30
108-88-3 Toluene 10 8.5 85 8.8 88 3 70-130/30
79-01-6 Trichloroethylene 10 9.3 93 9.4 94 1 70-130/30
m,p-Xylene 20 17.5 88 17.6 88 1 70-130/30
* = Outside of Control Limits.
57 of 100
JD6284455.2.1
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V7W62-BS 7W01362.D 1 04/04/23 TCH n/a n/a V7W62
V7W62-BSD 7W01363.D 1 04/04/23 TCH n/a n/a V7W62
The QC reported here applies to the following samples:Method: TO-15
JD62844-1, JD62844-2, JD62844-3, JD62844-4, JD62844-5, JD62844-6, JD62844-7, JD62844-8, JD62844-9, JD62844-
10, JD62844-11, JD62844-12, JD62844-13
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
95-47-6 o-Xylene 10 9.0 90 9.0 90 0 70-130/30
1330-20-7 Xylenes (total)30 26.5 88 26.6 89 0 70-130/30
CAS No. Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 96%97% 65-128%
(a) High percent recovery and no associated positive reported in the QC batch.
* = Outside of Control Limits.
58 of 100
JD6284455.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3085-BS 3W78321.D 1 12/11/22 TCH n/a n/a V3W3085
V3W3085-BSD 3W78322.D 1 12/11/22 TCH n/a n/a V3W3085
The QC reported here applies to the following samples:Method: TO-15
V3W3085-SCC
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
67-64-1 Acetone (2-Propanone) 10 9.0 90 9.1 91 1 70-130/30
106-99-0 1,3-Butadiene 10 9.4 94 9.3 93 1 70-130/30
71-43-2 Benzene 10 9.9 99 9.9 99 0 70-130/30
75-15-0 Carbon disulfide 10 11.1 111 11.0 110 1 70-130/30
108-90-7 Chlorobenzene 10 9.1 91 9.1 91 0 70-130/30
67-66-3 Chloroform 10 11.8 118 11.9 119 1 70-130/30
74-87-3 Chloromethane 10 10.1 101 9.8 98 3 70-130/30
56-23-5 Carbon tetrachloride 10 12.9 129 13.0 130 1 70-130/30
110-82-7 Cyclohexane 10 9.1 91 9.2 92 1 70-130/30
75-34-3 1,1-Dichloroethane 10 11.0 110 11.0 110 0 70-130/30
75-35-4 1,1-Dichloroethylene 10 10.9 109 10.6 106 3 70-130/30
107-06-2 1,2-Dichloroethane 10 12.7 127 12.7 127 0 70-130/30
75-71-8 Dichlorodifluoromethane 10 12.8 128 12.7 127 1 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 10.9 109 10.9 109 0 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 10.6 106 10.8 108 2 70-130/30
95-50-1 o-Dichlorobenzene 10 10.9 109 10.9 109 0 70-130/30
100-41-4 Ethylbenzene 10 9.1 91 9.1 91 0 70-130/30
141-78-6 Ethyl Acetate 10 10.3 103 10.3 103 0 70-130/30
142-82-5 Heptane 10 8.8 88 9.0 90 2 70-130/30
87-68-3 Hexachlorobutadiene 10 16.7 167* a 16.5 165* a 1 70-130/30
110-54-3 Hexane 10 9.7 97 10 100 3 70-130/30
67-63-0 Isopropyl Alcohol 10 10.6 106 10.3 103 3 70-130/30
75-09-2 Methylene chloride 10 10.2 102 10.1 101 1 70-130/30
78-93-3 Methyl ethyl ketone 10 10.9 109 11.0 110 1 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 10.1 101 10.3 103 2 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 11.6 116 11.7 117 1 70-130/30
115-07-1 Propylene 10 10.1 101 10.1 101 0 70-130/30
71-55-6 1,1,1-Trichloroethane 10 12.3 123 12.4 124 1 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 9.4 94 9.6 96 2 70-130/30
79-00-5 1,1,2-Trichloroethane 10 10.1 101 9.9 99 2 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 15.2 152* a 15.3 153* a 1 70-130/30
127-18-4 Tetrachloroethylene 10 9.5 95 9.6 96 1 70-130/30
109-99-9 Tetrahydrofuran 10 10.8 108 11.1 111 3 70-130/30
108-88-3 Toluene 10 9.8 98 9.5 95 3 70-130/30
79-01-6 Trichloroethylene 10 10.1 101 10.2 102 1 70-130/30
m,p-Xylene 20 17.5 88 17.5 88 0 70-130/30
* = Outside of Control Limits.
59 of 100
JD6284455.2.2
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3085-BS 3W78321.D 1 12/11/22 TCH n/a n/a V3W3085
V3W3085-BSD 3W78322.D 1 12/11/22 TCH n/a n/a V3W3085
The QC reported here applies to the following samples:Method: TO-15
V3W3085-SCC
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
95-47-6 o-Xylene 10 9.0 90 9.1 91 1 70-130/30
1330-20-7 Xylenes (total)30 26.5 88 26.7 89 1 70-130/30
CAS No. Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 107%107% 65-128%
(a) High percent recovery and no associated positive reported in the QC batch.
* = Outside of Control Limits.
60 of 100
JD6284455.2.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V6W1162-BS 6W27613.D 1 12/11/22 TCH n/a n/a V6W1162
V6W1162-BSD 6W27614.D 1 12/11/22 TCH n/a n/a V6W1162
The QC reported here applies to the following samples:Method: TO-15
V6W1162-SCC
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
67-64-1 Acetone (2-Propanone) 10 9.1 91 9.3 93 2 70-130/30
106-99-0 1,3-Butadiene 10 11.1 111 10.7 107 4 70-130/30
71-43-2 Benzene 10 9.4 94 9.4 94 0 70-130/30
75-15-0 Carbon disulfide 10 10.0 100 10.7 107 7 70-130/30
108-90-7 Chlorobenzene 10 10.5 105 10.4 104 1 70-130/30
67-66-3 Chloroform 10 10.2 102 10.0 100 2 70-130/30
74-87-3 Chloromethane 10 10.4 104 9.4 94 10 70-130/30
56-23-5 Carbon tetrachloride 10 10.6 106 10.8 108 2 70-130/30
110-82-7 Cyclohexane 10 9.9 99 10.2 102 3 70-130/30
75-34-3 1,1-Dichloroethane 10 9.6 96 10.2 102 6 70-130/30
75-35-4 1,1-Dichloroethylene 10 10.3 103 10.3 103 0 70-130/30
107-06-2 1,2-Dichloroethane 10 10.7 107 9.9 99 8 70-130/30
75-71-8 Dichlorodifluoromethane 10 11.0 110 10.4 104 6 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 9.8 98 10.3 103 5 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 9.8 98 9.8 98 0 70-130/30
95-50-1 o-Dichlorobenzene 10 11.4 114 11.2 112 2 70-130/30
100-41-4 Ethylbenzene 10 9.3 93 9.3 93 0 70-130/30
141-78-6 Ethyl Acetate 10 10.4 104 10.5 105 1 70-130/30
142-82-5 Heptane 10 11.0 110 10.5 105 5 70-130/30
87-68-3 Hexachlorobutadiene 10 11.0 110 10.8 108 2 70-130/30
110-54-3 Hexane 10 9.6 96 9.5 95 1 70-130/30
67-63-0 Isopropyl Alcohol 10 9.9 99 10.0 100 1 70-130/30
75-09-2 Methylene chloride 10 9.5 95 9.6 96 1 70-130/30
78-93-3 Methyl ethyl ketone 10 10.2 102 10 100 2 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 11.5 115 11.0 110 4 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 9.7 97 10.2 102 5 70-130/30
115-07-1 Propylene 10 10.7 107 10.7 107 0 70-130/30
71-55-6 1,1,1-Trichloroethane 10 10.6 106 10.3 103 3 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 10.4 104 10.4 104 0 70-130/30
79-00-5 1,1,2-Trichloroethane 10 10.5 105 10.2 102 3 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 11.3 113 11.4 114 1 70-130/30
127-18-4 Tetrachloroethylene 10 11.2 112 10.8 108 4 70-130/30
109-99-9 Tetrahydrofuran 10 11.0 110 10.2 102 8 70-130/30
108-88-3 Toluene 10 10.4 104 10.1 101 3 70-130/30
79-01-6 Trichloroethylene 10 10.3 103 10.1 101 2 70-130/30
m,p-Xylene 20 19.7 99 19.7 99 0 70-130/30
* = Outside of Control Limits.
61 of 100
JD6284455.2.3
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V6W1162-BS 6W27613.D 1 12/11/22 TCH n/a n/a V6W1162
V6W1162-BSD 6W27614.D 1 12/11/22 TCH n/a n/a V6W1162
The QC reported here applies to the following samples:Method: TO-15
V6W1162-SCC
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
95-47-6 o-Xylene 10 9.9 99 9.9 99 0 70-130/30
1330-20-7 Xylenes (total)30 29.6 99 29.6 99 0 70-130/30
CAS No. Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 100%100% 65-128%
* = Outside of Control Limits.
62 of 100
JD6284455.2.3
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2791-BS 2W62751.D 1 01/06/23 TCH n/a n/a V2W2791
V2W2791-BSD 2W62752.D 1 01/06/23 TCH n/a n/a V2W2791
The QC reported here applies to the following samples:Method: TO-15
V2W2791-SCC
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
67-64-1 Acetone (2-Propanone) 10 11.3 113 11.3 113 0 70-130/30
106-99-0 1,3-Butadiene 10 12.0 120 12.1 121 1 70-130/30
71-43-2 Benzene 10 10.6 106 10.7 107 1 70-130/30
75-15-0 Carbon disulfide 10 9.7 97 9.9 99 2 70-130/30
108-90-7 Chlorobenzene 10 9.8 98 9.9 99 1 70-130/30
67-66-3 Chloroform 10 11.2 112 11.3 113 1 70-130/30
74-87-3 Chloromethane 10 12.4 124 12.4 124 0 70-130/30
56-23-5 Carbon tetrachloride 10 10 100 10.1 101 1 70-130/30
110-82-7 Cyclohexane 10 11.2 112 11.0 110 2 70-130/30
75-34-3 1,1-Dichloroethane 10 12.7 127 13.0 130 2 70-130/30
75-35-4 1,1-Dichloroethylene 10 8.6 86 8.8 88 2 70-130/30
107-06-2 1,2-Dichloroethane 10 11.9 119 12.2 122 2 70-130/30
75-71-8 Dichlorodifluoromethane 10 9.6 96 9.7 97 1 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 11.1 111 11.1 111 0 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 11.0 110 11.2 112 2 70-130/30
95-50-1 o-Dichlorobenzene 10 9.0 90 9.1 91 1 70-130/30
100-41-4 Ethylbenzene 10 10.1 101 10.2 102 1 70-130/30
141-78-6 Ethyl Acetate 10 12.6 126 13.0 130 3 70-130/30
142-82-5 Heptane 10 12.9 129 12.9 129 0 70-130/30
87-68-3 Hexachlorobutadiene 10 7.6 76 7.7 77 1 70-130/30
110-54-3 Hexane 10 12.5 125 12.6 126 1 70-130/30
67-63-0 Isopropyl Alcohol 10 11.3 113 11.4 114 1 70-130/30
75-09-2 Methylene chloride 10 8.0 80 8.0 80 0 70-130/30
78-93-3 Methyl ethyl ketone 10 11.5 115 11.8 118 3 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 13.2 132* a 13.4 134* a 2 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 10.8 108 10.8 108 0 70-130/30
115-07-1 Propylene 10 13.8 138* a 14.0 140* a 1 70-130/30
71-55-6 1,1,1-Trichloroethane 10 10.5 105 10.7 107 2 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 11.5 115 11.5 115 0 70-130/30
79-00-5 1,1,2-Trichloroethane 10 11.1 111 11.0 110 1 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 8.1 81 8.2 82 1 70-130/30
127-18-4 Tetrachloroethylene 10 9.4 94 9.3 93 1 70-130/30
109-99-9 Tetrahydrofuran 10 11.9 119 12.3 123 3 70-130/30
108-88-3 Toluene 10 10.2 102 10.2 102 0 70-130/30
79-01-6 Trichloroethylene 10 10.8 108 10.8 108 0 70-130/30
m,p-Xylene 20 20.2 101 20.5 103 1 70-130/30
* = Outside of Control Limits.
63 of 100
JD6284455.2.4
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2791-BS 2W62751.D 1 01/06/23 TCH n/a n/a V2W2791
V2W2791-BSD 2W62752.D 1 01/06/23 TCH n/a n/a V2W2791
The QC reported here applies to the following samples:Method: TO-15
V2W2791-SCC
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
95-47-6 o-Xylene 10 10 100 10.1 101 1 70-130/30
1330-20-7 Xylenes (total)30 30.2 101 30.6 102 1 70-130/30
CAS No. Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 110%111% 65-128%
(a) High percent recovery and no associated positive reported in the QC batch.
* = Outside of Control Limits.
64 of 100
JD6284455.2.4
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-BS 3W78732.D 1 01/09/23 TCH n/a n/a V3W3101
V3W3101-BSD 3W78733.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here applies to the following samples:Method: TO-15
V3W3101-SCC
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
67-64-1 Acetone (2-Propanone) 10 8.2 82 8.0 80 2 70-130/30
106-99-0 1,3-Butadiene 10 11.1 111 10.8 108 3 70-130/30
71-43-2 Benzene 10 10.1 101 10.1 101 0 70-130/30
75-15-0 Carbon disulfide 10 10.5 105 10.6 106 1 70-130/30
108-90-7 Chlorobenzene 10 11.0 110 11.2 112 2 70-130/30
67-66-3 Chloroform 10 9.9 99 10.0 100 1 70-130/30
74-87-3 Chloromethane 10 9.8 98 9.8 98 0 70-130/30
56-23-5 Carbon tetrachloride 10 10.6 106 10.7 107 1 70-130/30
110-82-7 Cyclohexane 10 10.6 106 10.5 105 1 70-130/30
75-34-3 1,1-Dichloroethane 10 10.4 104 10.4 104 0 70-130/30
75-35-4 1,1-Dichloroethylene 10 10.1 101 10.2 102 1 70-130/30
107-06-2 1,2-Dichloroethane 10 10.8 108 10.8 108 0 70-130/30
75-71-8 Dichlorodifluoromethane 10 10.3 103 10.4 104 1 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 9.9 99 9.9 99 0 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 10.4 104 10.5 105 1 70-130/30
95-50-1 o-Dichlorobenzene 10 12.3 123 12.3 123 0 70-130/30
100-41-4 Ethylbenzene 10 10.2 102 10.4 104 2 70-130/30
141-78-6 Ethyl Acetate 10 11.4 114 11.4 114 0 70-130/30
142-82-5 Heptane 10 10.1 101 10.2 102 1 70-130/30
87-68-3 Hexachlorobutadiene 10 12.2 122 12.3 123 1 70-130/30
110-54-3 Hexane 10 10.7 107 10.8 108 1 70-130/30
67-63-0 Isopropyl Alcohol 10 10.7 107 10.7 107 0 70-130/30
75-09-2 Methylene chloride 10 9.4 94 9.5 95 1 70-130/30
78-93-3 Methyl ethyl ketone 10 10.7 107 10.8 108 1 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 10.6 106 10.7 107 1 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 10.4 104 10.3 103 1 70-130/30
115-07-1 Propylene 10 10.1 101 10.2 102 1 70-130/30
71-55-6 1,1,1-Trichloroethane 10 9.7 97 9.7 97 0 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 11.3 113 11.4 114 1 70-130/30
79-00-5 1,1,2-Trichloroethane 10 10.2 102 10.3 103 1 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 14.6 146* a 14.9 149* a 2 70-130/30
127-18-4 Tetrachloroethylene 10 10.5 105 10.8 108 3 70-130/30
109-99-9 Tetrahydrofuran 10 10.7 107 10.8 108 1 70-130/30
108-88-3 Toluene 10 9.6 96 9.7 97 1 70-130/30
79-01-6 Trichloroethylene 10 10.0 100 10.1 101 1 70-130/30
m,p-Xylene 20 21.3 107 21.5 108 1 70-130/30
* = Outside of Control Limits.
65 of 100
JD6284455.2.5
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-BS 3W78732.D 1 01/09/23 TCH n/a n/a V3W3101
V3W3101-BSD 3W78733.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here applies to the following samples:Method: TO-15
V3W3101-SCC
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
95-47-6 o-Xylene 10 10.7 107 10.7 107 0 70-130/30
1330-20-7 Xylenes (total)30 32.0 107 32.3 108 1 70-130/30
CAS No. Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 103%100% 65-128%
(a) High percent recovery and no associated positive reported in the QC batch.
* = Outside of Control Limits.
66 of 100
JD6284455.2.5
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-BS 3W79061.D 1 01/30/23 TCH n/a n/a V3W3115
V3W3115-BSD 3W79062.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here applies to the following samples:Method: TO-15
V3W3115-SCC
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
67-64-1 Acetone (2-Propanone) 10 7.1 71 7.0 70 1 70-130/30
106-99-0 1,3-Butadiene 10 8.9 89 8.7 87 2 70-130/30
71-43-2 Benzene 10 10.2 102 10.1 101 1 70-130/30
75-15-0 Carbon disulfide 10 11.0 110 10.9 109 1 70-130/30
108-90-7 Chlorobenzene 10 11.5 115 11.3 113 2 70-130/30
67-66-3 Chloroform 10 11.1 111 11.1 111 0 70-130/30
74-87-3 Chloromethane 10 8.3 83 8.2 82 1 70-130/30
56-23-5 Carbon tetrachloride 10 11.0 110 11.1 111 1 70-130/30
110-82-7 Cyclohexane 10 10.8 108 10.9 109 1 70-130/30
75-34-3 1,1-Dichloroethane 10 10.3 103 10.2 102 1 70-130/30
75-35-4 1,1-Dichloroethylene 10 11.4 114 11.3 113 1 70-130/30
107-06-2 1,2-Dichloroethane 10 11.6 116 11.6 116 0 70-130/30
75-71-8 Dichlorodifluoromethane 10 11.9 119 11.8 118 1 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 11.2 112 11.1 111 1 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 11.8 118 11.8 118 0 70-130/30
95-50-1 o-Dichlorobenzene 10 11.5 115 11.3 113 2 70-130/30
100-41-4 Ethylbenzene 10 10.9 109 10.8 108 1 70-130/30
141-78-6 Ethyl Acetate 10 10.4 104 10.2 102 2 70-130/30
142-82-5 Heptane 10 7.6 76 7.6 76 0 70-130/30
87-68-3 Hexachlorobutadiene 10 12.6 126 12.3 123 2 70-130/30
110-54-3 Hexane 10 9.7 97 9.6 96 1 70-130/30
67-63-0 Isopropyl Alcohol 10 8.6 86 8.6 86 0 70-130/30
75-09-2 Methylene chloride 10 10.3 103 10.2 102 1 70-130/30
78-93-3 Methyl ethyl ketone 10 11.1 111 10.9 109 2 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 9.1 91 9.0 90 1 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 10.9 109 10.9 109 0 70-130/30
115-07-1 Propylene 10 7.4 74 7.4 74 0 70-130/30
71-55-6 1,1,1-Trichloroethane 10 10.6 106 10.6 106 0 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 11.7 117 11.5 115 2 70-130/30
79-00-5 1,1,2-Trichloroethane 10 10.6 106 10.6 106 0 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 14.4 144* a 13.9 139* a 4 70-130/30
127-18-4 Tetrachloroethylene 10 12.1 121 11.8 118 3 70-130/30
109-99-9 Tetrahydrofuran 10 11.0 110 11.1 111 1 70-130/30
108-88-3 Toluene 10 10.2 102 10.1 101 1 70-130/30
79-01-6 Trichloroethylene 10 10.6 106 10.6 106 0 70-130/30
m,p-Xylene 20 22.3 112 22.0 110 1 70-130/30
* = Outside of Control Limits.
67 of 100
JD6284455.2.6
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-BS 3W79061.D 1 01/30/23 TCH n/a n/a V3W3115
V3W3115-BSD 3W79062.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here applies to the following samples:Method: TO-15
V3W3115-SCC
Spike BSP BSP BSD BSD Limits
CAS No. Compound ppbv ppbv % ppbv % RPD Rec/RPD
95-47-6 o-Xylene 10 11.0 110 10.8 108 2 70-130/30
1330-20-7 Xylenes (total)30 33.3 111 32.9 110 1 70-130/30
CAS No. Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 101%101% 65-128%
(a) High percent recovery and no associated positive reported in the QC batch.
* = Outside of Control Limits.
68 of 100
JD6284455.2.6
Duplicate Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
JD62844-1DUP 7W01368.D 1 04/04/23 TCH n/a n/a V7W62
JD62844-1 7W01367.D 1 04/04/23 TCH n/a n/a V7W62
The QC reported here applies to the following samples:Method: TO-15
JD62844-1, JD62844-2, JD62844-3, JD62844-4, JD62844-5, JD62844-6, JD62844-7, JD62844-8, JD62844-9, JD62844-
10, JD62844-11, JD62844-12, JD62844-13
JD62844-1 DUP
CAS No. Compound ppbv Q ppbv Q RPD Limits
67-64-1 Acetone (2-Propanone) 16.1 16.3 1 25
106-99-0 1,3-Butadiene ND ND nc 25
71-43-2 Benzene ND ND nc 25
75-15-0 Carbon disulfide ND ND nc 25
108-90-7 Chlorobenzene ND ND nc 25
67-66-3 Chloroform ND ND nc 25
74-87-3 Chloromethane ND ND nc 25
56-23-5 Carbon tetrachloride ND ND nc 25
110-82-7 Cyclohexane 0.50 J 0.59 J 17 25
75-34-3 1,1-Dichloroethane ND ND nc 25
75-35-4 1,1-Dichloroethylene ND ND nc 25
107-06-2 1,2-Dichloroethane ND ND nc 25
75-71-8 Dichlorodifluoromethane 0.54 J 0.54 J 0 25
156-60-5 trans-1,2-Dichloroethylene ND ND nc 25
156-59-2 cis-1,2-Dichloroethylene ND ND nc 25
95-50-1 o-Dichlorobenzene ND ND nc 25
100-41-4 Ethylbenzene ND ND nc 25
141-78-6 Ethyl Acetate ND ND nc 25
142-82-5 Heptane ND ND nc 25
87-68-3 Hexachlorobutadiene ND ND nc 25
110-54-3 Hexane ND ND nc 25
67-63-0 Isopropyl Alcohol 3.7 4.5 20 25
75-09-2 Methylene chloride 1.6 1.6 0 25
78-93-3 Methyl ethyl ketone 0.61 J 0.75 J 21 25
108-10-1 Methyl Isobutyl Ketone ND ND nc 25
1634-04-4 Methyl Tert Butyl Ether ND ND nc 25
115-07-1 Propylene ND ND nc 25
71-55-6 1,1,1-Trichloroethane ND ND nc 25
79-34-5 1,1,2,2-Tetrachloroethane ND ND nc 25
79-00-5 1,1,2-Trichloroethane ND ND nc 25
120-82-1 1,2,4-Trichlorobenzene ND ND nc 25
127-18-4 Tetrachloroethylene 7.3 7.5 3 25
109-99-9 Tetrahydrofuran ND ND nc 25
108-88-3 Toluene ND ND nc 25
79-01-6 Trichloroethylene 18.4 19.0 3 25
m,p-Xylene ND ND nc 25
* = Outside of Control Limits.
69 of 100
JD6284455.3.1
Duplicate Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
JD62844-1DUP 7W01368.D 1 04/04/23 TCH n/a n/a V7W62
JD62844-1 7W01367.D 1 04/04/23 TCH n/a n/a V7W62
The QC reported here applies to the following samples:Method: TO-15
JD62844-1, JD62844-2, JD62844-3, JD62844-4, JD62844-5, JD62844-6, JD62844-7, JD62844-8, JD62844-9, JD62844-
10, JD62844-11, JD62844-12, JD62844-13
JD62844-1 DUP
CAS No. Compound ppbv Q ppbv Q RPD Limits
95-47-6 o-Xylene ND ND nc 25
1330-20-7 Xylenes (total)ND ND nc 25
CAS No. Surrogate Recoveries DUP JD62844-1 Limits
460-00-4 4-Bromofluorobenzene 91%90% 65-128%
* = Outside of Control Limits.
70 of 100
JD6284455.3.1
Summa Cleaning Certification Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V6W1162-SCC 6W27617.D 1 12/11/22 TCH n/a n/a V6W1162
The QC reported here (Summa A2306) applies to the following samples: Method: TO-15
Batch CP11994 cleaned 12/02/22: JD62844-11(A2313)
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
71 of 100
JD6284455.4.1
Summa Cleaning Certification Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V6W1162-SCC 6W27617.D 1 12/11/22 TCH n/a n/a V6W1162
The QC reported here (Summa A2306) applies to the following samples: Method: TO-15
Batch CP11994 cleaned 12/02/22: JD62844-11(A2313)
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 97% 65-128%
72 of 100
JD6284455.4.1
Summa Cleaning Certification Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3085-SCC 3W78328.D 1 12/11/22 TCH n/a n/a V3W3085
The QC reported here (Summa A2227) applies to the following samples: Method: TO-15
Batch CP11996 cleaned 12/02/22: JD62844-3(A2222), JD62844-7(A2199)
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
73 of 100
JD6284455.4.2
Summa Cleaning Certification Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3085-SCC 3W78328.D 1 12/11/22 TCH n/a n/a V3W3085
The QC reported here (Summa A2227) applies to the following samples: Method: TO-15
Batch CP11996 cleaned 12/02/22: JD62844-3(A2222), JD62844-7(A2199)
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 104% 65-128%
74 of 100
JD6284455.4.2
Summa Cleaning Certification Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3085-SCC 3W78331.D 1 12/11/22 TCH n/a n/a V3W3085
The QC reported here (Summa A1148) applies to the following samples: Method: TO-15
Batch CP12001 cleaned 12/06/22: JD62844-10(A2220)
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
75 of 100
JD6284455.4.3
Summa Cleaning Certification Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3085-SCC 3W78331.D 1 12/11/22 TCH n/a n/a V3W3085
The QC reported here (Summa A1148) applies to the following samples: Method: TO-15
Batch CP12001 cleaned 12/06/22: JD62844-10(A2220)
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 103% 65-128%
76 of 100
JD6284455.4.3
Summa Cleaning Certification Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V6W1162-SCC 6W27623.D 1 12/11/22 TCH n/a n/a V6W1162
The QC reported here (Summa A2202) applies to the following samples: Method: TO-15
Batch CP11998 cleaned 11/30/22: JD62844-2(A2209), JD62844-4(A2205), JD62844-6(A2251)
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
77 of 100
JD6284455.4.4
Summa Cleaning Certification Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V6W1162-SCC 6W27623.D 1 12/11/22 TCH n/a n/a V6W1162
The QC reported here (Summa A2202) applies to the following samples: Method: TO-15
Batch CP11998 cleaned 11/30/22: JD62844-2(A2209), JD62844-4(A2205), JD62844-6(A2251)
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 94% 65-128%
78 of 100
JD6284455.4.4
Summa Cleaning Certification Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2791-SCC 2W62769.D 1 01/06/23 TCH n/a n/a V2W2791
The QC reported here (Summa A1940) applies to the following samples: Method: TO-15
Batch CP12037 cleaned 12/22/22: JD62844-8(A2317)
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
79 of 100
JD6284455.4.5
Summa Cleaning Certification Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2791-SCC 2W62769.D 1 01/06/23 TCH n/a n/a V2W2791
The QC reported here (Summa A1940) applies to the following samples: Method: TO-15
Batch CP12037 cleaned 12/22/22: JD62844-8(A2317)
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 109% 65-128%
80 of 100
JD6284455.4.5
Summa Cleaning Certification Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-SCC 3W78742.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here (Summa A1127) applies to the following samples: Method: TO-15
Batch CP12040 cleaned 01/05/23: JD62844-1(A2330), JD62844-5(A2331), JD62844-9(A2332), JD62844-12(A2326)
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.80 0.58 ppbv ND 1.9 ug/m3
106-99-0 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 ug/m3
71-43-2 Benzene ND 0.80 0.25 ppbv ND 2.6 ug/m3
75-15-0 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 ug/m3
108-90-7 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 ug/m3
67-66-3 Chloroform ND 0.80 0.15 ppbv ND 3.9 ug/m3
74-87-3 Chloromethane ND 0.80 0.36 ppbv ND 1.7 ug/m3
56-23-5 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 ug/m3
110-82-7 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 ug/m3
75-34-3 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 ug/m3
107-06-2 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.80 0.13 ppbv ND 4.0 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 ug/m3
95-50-1 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 ug/m3
100-41-4 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 ug/m3
141-78-6 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 ug/m3
142-82-5 Heptane ND 0.80 0.37 ppbv ND 3.3 ug/m3
87-68-3 Hexachlorobutadiene ND 0.80 0.25 ppbv ND 8.5 ug/m3
110-54-3 Hexane ND 0.80 0.45 ppbv ND 2.8 ug/m3
67-63-0 Isopropyl Alcohol ND 0.80 0.56 ppbv ND 2.0 ug/m3
75-09-2 Methylene chloride ND 0.80 0.22 ppbv ND 2.8 ug/m3
78-93-3 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 ug/m3
115-07-1 Propylene ND 2.0 0.57 ppbv ND 3.4 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 ug/m3
127-18-4 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 ug/m3
109-99-9 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 ug/m3
108-88-3 Toluene ND 0.80 0.23 ppbv ND 3.0 ug/m3
79-01-6 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 ug/m3
m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 ug/m3
81 of 100
JD6284455.4.6
Summa Cleaning Certification Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-SCC 3W78742.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here (Summa A1127) applies to the following samples: Method: TO-15
Batch CP12040 cleaned 01/05/23: JD62844-1(A2330), JD62844-5(A2331), JD62844-9(A2332), JD62844-12(A2326)
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.80 0.31 ppbv ND 3.5 ug/m3
1330-20-7 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 100% 65-128%
82 of 100
JD6284455.4.6
Summa Cleaning Certification Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-SCC 3W79066.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here (Summa A679) applies to the following samples: Method: TO-15
Batch CP12059 cleaned 01/18/23: JD62844-13(A1976)
CAS No. Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
83 of 100
JD6284455.4.7
Summa Cleaning Certification Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-SCC 3W79066.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here (Summa A679) applies to the following samples: Method: TO-15
Batch CP12059 cleaned 01/18/23: JD62844-13(A1976)
CAS No. Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 97% 65-128%
84 of 100
JD6284455.4.7
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V2W2776-BFB Injection Date:12/14/22
Lab File ID:2W62382.D Injection Time:17:23
Instrument ID:GCMS2W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 13015 22.8 Pass
75 30.0 - 66.0% of mass 95 30880 54.0 Pass
95 Base peak, 100% relative abundance 57157 100.0 Pass
96 5.0 - 9.0% of mass 95 3907 6.84 Pass
173 Less than 2.0% of mass 174 242 0.42 (0.57) a Pass
174 50.0 - 120.0% of mass 95 42512 74.4 Pass
175 4.0 - 9.01% of mass 174 3043 5.32 (7.16) a Pass
176 93.0 - 101.0% of mass 174 40504 70.9 (95.3) a Pass
177 5.0 - 9.0% of mass 176 2767 4.84 (6.83) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V2W2776-IC2776 2W62383.D 12/14/22 17:55 00:32 Initial cal 0.04
V2W2776-IC2776 2W62384.D 12/14/22 18:28 01:05 Initial cal 0.1
V2W2776-IC2776 2W62385.D 12/14/22 18:59 01:36 Initial cal 0.2
V2W2776-IC2776 2W62386.D 12/14/22 19:31 02:08 Initial cal 0.5
V2W2776-IC2776 2W62388.D 12/14/22 20:33 03:10 Initial cal 5
V2W2776-ICC2776 2W62389.D 12/14/22 21:05 03:42 Initial cal 10
V2W2776-IC2776 2W62390.D 12/14/22 21:37 04:14 Initial cal 20
V2W2776-IC2776 2W62391.D 12/14/22 22:12 04:49 Initial cal 40
V2W2776-IC2776 2W62392.D 12/14/22 22:47 05:24 Initial cal 50
V2W2776-ICV2776 2W62395.D 12/15/22 00:22 06:59 Initial cal verification 10
85 of 100
JD6284455.5.1
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V2W2791-BFB Injection Date:01/06/23
Lab File ID:2W62747.D Injection Time:08:44
Instrument ID:GCMS2W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 11035 24.6 Pass
75 30.0 - 66.0% of mass 95 24203 54.0 Pass
95 Base peak, 100% relative abundance 44800 100.0 Pass
96 5.0 - 9.0% of mass 95 3056 6.82 Pass
173 Less than 2.0% of mass 174 138 0.31 (0.52) a Pass
174 50.0 - 120.0% of mass 95 26723 59.6 Pass
175 4.0 - 9.01% of mass 174 1907 4.26 (7.14) a Pass
176 93.0 - 101.0% of mass 174 25832 57.7 (96.7) a Pass
177 5.0 - 9.0% of mass 176 1730 3.86 (6.70) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V2W2791-CC2776 2W62750.D 01/06/23 10:48 02:04 Continuing cal 10
V2W2791-BS 2W62751.D 01/06/23 11:24 02:40 Blank Spike
V2W2791-BSD 2W62752.D 01/06/23 11:57 03:13 Blank Spike Duplicate
V2W2791-MB 2W62755.D 01/06/23 14:02 05:18 Method Blank
V2W2791-SCC 2W62756.D 01/06/23 14:52 06:08 Summa Cleaning Certification
V2W2791-SCC 2W62757.D 01/06/23 15:31 06:47 Summa Cleaning Certification
ZZZZZZ 2W62758.D 01/06/23 16:09 07:25 (unrelated sample)
ZZZZZZ 2W62760.D 01/06/23 17:27 08:43 (unrelated sample)
ZZZZZZ 2W62762.D 01/06/23 18:33 09:49 (unrelated sample)
ZZZZZZ 2W62764.D 01/06/23 19:39 10:55 (unrelated sample)
JD58164-2 2W62766.D 01/06/23 20:45 12:01 (used for QC only; not part of job JD62844)
JD58164-2DUP 2W62767.D 01/06/23 21:19 12:35 Duplicate
V2W2791-SCC 2W62769.D 01/06/23 22:24 13:40 Summa Cleaning Certification
V2W2791-SCC 2W62770.D 01/06/23 22:57 14:13 Summa Cleaning Certification
V2W2791-SCC 2W62771.D 01/06/23 23:30 14:46 Summa Cleaning Certification
V2W2791-SCC 2W62772.D 01/07/23 00:09 15:25 Summa Cleaning Certification
V2W2791-SCC 2W62773.D 01/07/23 00:48 16:04 Summa Cleaning Certification
V2W2791-SCC 2W62774.D 01/07/23 01:27 16:43 Summa Cleaning Certification
V2W2791-SCC 2W62775.D 01/07/23 02:06 17:22 Summa Cleaning Certification
V2W2791-SCC 2W62776.D 01/07/23 02:44 18:00 Summa Cleaning Certification
86 of 100
JD6284455.5.2
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V3W3055-BFB Injection Date:11/03/22
Lab File ID:3W77566.D Injection Time:02:37
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 29547 21.0 Pass
75 30.0 - 66.0% of mass 95 73547 52.3 Pass
95 Base peak, 100% relative abundance 140547 100.0 Pass
96 5.0 - 9.0% of mass 95 9241 6.58 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 124965 88.9 Pass
175 4.0 - 9.01% of mass 174 10222 7.27 (8.18) a Pass
176 93.0 - 101.0% of mass 174 121805 86.7 (97.5) a Pass
177 5.0 - 9.0% of mass 176 8004 5.69 (6.57) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3055-IC3055 3W77567.D 11/03/22 03:16 00:39 Initial cal 0.04
V3W3055-IC3055 3W77568.D 11/03/22 03:54 01:17 Initial cal 0.1
V3W3055-IC3055 3W77569.D 11/03/22 04:34 01:57 Initial cal 0.2
V3W3055-IC3055 3W77571.D 11/03/22 05:54 03:17 Initial cal 0.5
V3W3055-IC3055 3W77572.D 11/03/22 06:33 03:56 Initial cal 5
V3W3055-ICC3055 3W77573.D 11/03/22 07:12 04:35 Initial cal 10
V3W3055-IC3055 3W77574.D 11/03/22 07:54 05:17 Initial cal 20
V3W3055-IC3055 3W77575.D 11/03/22 08:38 06:01 Initial cal 40
V3W3055-IC3055 3W77576.D 11/03/22 09:25 06:48 Initial cal 50
87 of 100
JD6284455.5.3
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V3W3055-BFB Injection Date:11/06/22
Lab File ID:3W77583.D Injection Time:15:04
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 44243 25.1 Pass
75 30.0 - 66.0% of mass 95 96336 54.7 Pass
95 Base peak, 100% relative abundance 176213 100.0 Pass
96 5.0 - 9.0% of mass 95 11902 6.75 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 163328 92.7 Pass
175 4.0 - 9.01% of mass 174 13564 7.70 (8.30) a Pass
176 93.0 - 101.0% of mass 174 156501 88.8 (95.8) a Pass
177 5.0 - 9.0% of mass 176 10917 6.20 (6.98) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3055-ICV3055 3W77585.D 11/06/22 16:46 01:42 Initial cal verification 10
V3W3056-CC3055 3W77586.D 11/06/22 21:11 06:07 Continuing cal 10
V3W3056-BS 3W77587.D 11/06/22 21:50 06:46 Blank Spike
V3W3056-BSD 3W77588.D 11/06/22 22:32 07:28 Blank Spike Duplicate
V3W3056-MB 3W77590.D 11/06/22 23:56 08:52 Method Blank
V3W3056-SCC 3W77591.D 11/07/22 00:41 09:37 Summa Cleaning Certification
V3W3056-SCC 3W77592.D 11/07/22 01:26 10:22 Summa Cleaning Certification
V3W3056-SCC 3W77594.D 11/07/22 02:56 11:52 Summa Cleaning Certification
V3W3056-SCC 3W77595.D 11/07/22 03:41 12:37 Summa Cleaning Certification
V3W3056-SCC 3W77596.D 11/07/22 04:26 13:22 Summa Cleaning Certification
V3W3056-SCC 3W77597.D 11/07/22 05:10 14:06 Summa Cleaning Certification
V3W3056-SCC 3W77598.D 11/07/22 05:56 14:52 Summa Cleaning Certification
V3W3056-SCC 3W77599.D 11/07/22 06:40 15:36 Summa Cleaning Certification
V3W3056-SCC 3W77600.D 11/07/22 07:26 16:22 Summa Cleaning Certification
V3W3056-SCC 3W77601.D 11/07/22 08:10 17:06 Summa Cleaning Certification
V3W3056-SCC 3W77602.D 11/07/22 08:55 17:51 Summa Cleaning Certification
V3W3056-SCC 3W77605.D 11/07/22 11:10 20:06 Summa Cleaning Certification
V3W3056-SCC 3W77606.D 11/07/22 11:55 20:51 Summa Cleaning Certification
V3W3056-SCC 3W77607.D 11/07/22 12:40 21:36 Summa Cleaning Certification
V3W3056-SCC 3W77608.D 11/07/22 13:24 22:20 Summa Cleaning Certification
88 of 100
JD6284455.5.4
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V3W3085-BFB Injection Date:12/11/22
Lab File ID:3W78319.D Injection Time:13:20
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 27269 22.1 Pass
75 30.0 - 66.0% of mass 95 73035 59.3 Pass
95 Base peak, 100% relative abundance 123251 100.0 Pass
96 5.0 - 9.0% of mass 95 7914 6.42 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 122000 99.0 Pass
175 4.0 - 9.01% of mass 174 10758 8.73 (8.82) a Pass
176 93.0 - 101.0% of mass 174 119307 96.8 (97.8) a Pass
177 5.0 - 9.0% of mass 176 7849 6.37 (6.58) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3085-CC3055 3W78320.D 12/11/22 14:00 00:40 Continuing cal 10
V3W3085-BS 3W78321.D 12/11/22 14:39 01:19 Blank Spike
V3W3085-BSD 3W78322.D 12/11/22 15:20 02:00 Blank Spike Duplicate
V3W3085-MB 3W78324.D 12/11/22 16:44 03:24 Method Blank
V3W3085-SCC 3W78327.D 12/11/22 18:48 05:28 Summa Cleaning Certification
V3W3085-SCC 3W78328.D 12/11/22 19:28 06:08 Summa Cleaning Certification
V3W3085-SCC 3W78329.D 12/11/22 20:07 06:47 Summa Cleaning Certification
V3W3085-SCC 3W78330.D 12/11/22 20:47 07:27 Summa Cleaning Certification
V3W3085-SCC 3W78331.D 12/11/22 21:26 08:06 Summa Cleaning Certification
V3W3085-SCC 3W78332.D 12/11/22 22:06 08:46 Summa Cleaning Certification
V3W3085-SCC 3W78333.D 12/11/22 22:45 09:25 Summa Cleaning Certification
V3W3085-SCC 3W78334.D 12/11/22 23:25 10:05 Summa Cleaning Certification
V3W3085-SCC 3W78337.D 12/12/22 01:24 12:04 Summa Cleaning Certification
V3W3085-SCC 3W78338.D 12/12/22 02:03 12:43 Summa Cleaning Certification
V3W3085-SCC 3W78339.D 12/12/22 02:43 13:23 Summa Cleaning Certification
V3W3085-SCC 3W78340.D 12/12/22 03:22 14:02 Summa Cleaning Certification
V3W3085-SCC 3W78341.D 12/12/22 04:02 14:42 Summa Cleaning Certification
V3W3085-SCC 3W78343.D 12/12/22 05:21 16:01 Summa Cleaning Certification
V3W3085-SCC 3W78344.D 12/12/22 06:00 16:40 Summa Cleaning Certification
V3W3085-SCC 3W78345.D 12/12/22 06:40 17:20 Summa Cleaning Certification
V3W3085-SCC 3W78346.D 12/12/22 07:25 18:05 Summa Cleaning Certification
V3W3085-SCC 3W78347.D 12/12/22 08:09 18:49 Summa Cleaning Certification
V3W3085-SCC 3W78348.D 12/12/22 08:54 19:34 Summa Cleaning Certification
89 of 100
JD6284455.5.5
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V3W3100-BFB Injection Date:01/06/23
Lab File ID:3W78713.D Injection Time:09:28
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 24491 19.7 Pass
75 30.0 - 66.0% of mass 95 60821 49.0 Pass
95 Base peak, 100% relative abundance 124220 100.0 Pass
96 5.0 - 9.0% of mass 95 8288 6.67 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 91648 73.8 Pass
175 4.0 - 9.01% of mass 174 6856 5.52 (7.48) a Pass
176 93.0 - 101.0% of mass 174 88963 71.6 (97.1) a Pass
177 5.0 - 9.0% of mass 176 5915 4.76 (6.65) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3100-IC3100 3W78714.D 01/06/23 10:20 00:52 Initial cal 0.04
V3W3100-IC3100 3W78715.D 01/06/23 11:00 01:32 Initial cal 0.1
V3W3100-IC3100 3W78716.D 01/06/23 11:40 02:12 Initial cal 0.2
V3W3100-IC3100 3W78717.D 01/06/23 12:21 02:53 Initial cal 0.5
V3W3100-IC3100 3W78719.D 01/06/23 13:39 04:11 Initial cal 5
V3W3100-ICC3100 3W78720.D 01/06/23 14:19 04:51 Initial cal 10
V3W3100-IC3100 3W78721.D 01/06/23 15:01 05:33 Initial cal 20
V3W3100-IC3100 3W78722.D 01/06/23 15:47 06:19 Initial cal 40
V3W3100-IC3100 3W78723.D 01/06/23 16:34 07:06 Initial cal 50
V3W3100-ICV3100 3W78726.D 01/06/23 18:34 09:06 Initial cal verification 10
90 of 100
JD6284455.5.6
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V3W3101-BFB Injection Date:01/09/23
Lab File ID:3W78730.D Injection Time:10:32
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 25421 20.3 Pass
75 30.0 - 66.0% of mass 95 61248 49.0 Pass
95 Base peak, 100% relative abundance 124923 100.0 Pass
96 5.0 - 9.0% of mass 95 8149 6.52 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 90531 72.5 Pass
175 4.0 - 9.01% of mass 174 6719 5.38 (7.42) a Pass
176 93.0 - 101.0% of mass 174 87760 70.3 (96.9) a Pass
177 5.0 - 9.0% of mass 176 5809 4.65 (6.62) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3101-CC3100 3W78731.D 01/09/23 11:11 00:39 Continuing cal 10
V3W3101-BS 3W78732.D 01/09/23 11:53 01:21 Blank Spike
V3W3101-BSD 3W78733.D 01/09/23 12:34 02:02 Blank Spike Duplicate
V3W3101-MB 3W78735.D 01/09/23 14:34 04:02 Method Blank
V3W3101-SCC 3W78738.D 01/09/23 16:57 06:25 Summa Cleaning Certification
V3W3101-SCC 3W78739.D 01/09/23 17:42 07:10 Summa Cleaning Certification
V3W3101-SCC 3W78740.D 01/09/23 18:27 07:55 Summa Cleaning Certification
V3W3101-SCC 3W78742.D 01/09/23 19:54 09:22 Summa Cleaning Certification
V3W3101-SCC 3W78743.D 01/09/23 20:34 10:02 Summa Cleaning Certification
V3W3101-SCC 3W78744.D 01/09/23 21:14 10:42 Summa Cleaning Certification
V3W3101-SCC 3W78745.D 01/09/23 21:54 11:22 Summa Cleaning Certification
V3W3101-SCC 3W78746.D 01/09/23 22:33 12:01 Summa Cleaning Certification
V3W3101-SCC 3W78747.D 01/09/23 23:13 12:41 Summa Cleaning Certification
91 of 100
JD6284455.5.7
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V3W3115-BFB Injection Date:01/30/23
Lab File ID:3W79058.D Injection Time:08:48
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 19875 17.5 Pass
75 30.0 - 66.0% of mass 95 55733 49.1 Pass
95 Base peak, 100% relative abundance 113485 100.0 Pass
96 5.0 - 9.0% of mass 95 8145 7.18 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 91237 80.4 Pass
175 4.0 - 9.01% of mass 174 6705 5.91 (7.35) a Pass
176 93.0 - 101.0% of mass 174 86045 75.8 (94.3) a Pass
177 5.0 - 9.0% of mass 176 5554 4.89 (6.45) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3115-CC3100 3W79060.D 01/30/23 10:14 01:26 Continuing cal 10
V3W3115-BS 3W79061.D 01/30/23 10:57 02:09 Blank Spike
V3W3115-BSD 3W79062.D 01/30/23 11:37 02:49 Blank Spike Duplicate
V3W3115-MB 3W79064.D 01/30/23 13:12 04:24 Method Blank
V3W3115-SCC 3W79066.D 01/30/23 14:38 05:50 Summa Cleaning Certification
JD58999-4 3W79068.D 01/30/23 16:05 07:17 (used for QC only; not part of job JD62844)
JD58999-4DUP 3W79069.D 01/30/23 16:51 08:03 Duplicate
ZZZZZZ 3W79070.D 01/30/23 17:36 08:48 (unrelated sample)
ZZZZZZ 3W79071.D 01/30/23 18:22 09:34 (unrelated sample)
ZZZZZZ 3W79073.D 01/30/23 19:44 10:56 (unrelated sample)
ZZZZZZ 3W79074.D 01/30/23 20:24 11:36 (unrelated sample)
ZZZZZZ 3W79075.D 01/30/23 21:03 12:15 (unrelated sample)
ZZZZZZ 3W79076.D 01/30/23 21:43 12:55 (unrelated sample)
ZZZZZZ 3W79077.D 01/30/23 22:23 13:35 (unrelated sample)
ZZZZZZ 3W79078.D 01/30/23 23:01 14:13 (unrelated sample)
ZZZZZZ 3W79079.D 01/30/23 23:41 14:53 (unrelated sample)
ZZZZZZ 3W79080.D 01/31/23 00:20 15:32 (unrelated sample)
ZZZZZZ 3W79081.D 01/31/23 00:58 16:10 (unrelated sample)
92 of 100
JD6284455.5.8
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V6W1158-BFB Injection Date:12/05/22
Lab File ID:6W27499.D Injection Time:21:18
Instrument ID:GCMS6W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 13227 24.7 Pass
75 30.0 - 66.0% of mass 95 26331 49.2 Pass
95 Base peak, 100% relative abundance 53568 100.0 Pass
96 5.0 - 9.0% of mass 95 3417 6.38 Pass
173 Less than 2.0% of mass 174 420 0.78 (0.97) a Pass
174 50.0 - 120.0% of mass 95 43253 80.7 Pass
175 4.0 - 9.01% of mass 174 3129 5.84 (7.23) a Pass
176 93.0 - 101.0% of mass 174 41891 78.2 (96.9) a Pass
177 5.0 - 9.0% of mass 176 2804 5.23 (6.69) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V6W1158-IC1158 6W27500.D 12/05/22 21:51 00:33 Initial cal 0.04
V6W1158-IC1158 6W27501.D 12/05/22 22:24 01:06 Initial cal 0.1
V6W1158-IC1158 6W27502.D 12/05/22 22:57 01:39 Initial cal 0.2
V6W1158-IC1158 6W27503.D 12/05/22 23:30 02:12 Initial cal 0.5
V6W1158-IC1158 6W27505.D 12/06/22 00:35 03:17 Initial cal 5
V6W1158-ICC1158 6W27506.D 12/06/22 01:07 03:49 Initial cal 10
V6W1158-IC1158 6W27507.D 12/06/22 01:39 04:21 Initial cal 20
V6W1158-IC1158 6W27508.D 12/06/22 02:12 04:54 Initial cal 40
V6W1158-IC1158 6W27509.D 12/06/22 02:47 05:29 Initial cal 50
93 of 100
JD6284455.5.9
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V6W1158-BFB Injection Date:12/07/22
Lab File ID:6W27516.D Injection Time:13:49
Instrument ID:GCMS6W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 14161 24.6 Pass
75 30.0 - 66.0% of mass 95 27760 48.3 Pass
95 Base peak, 100% relative abundance 57517 100.0 Pass
96 5.0 - 9.0% of mass 95 3939 6.85 Pass
173 Less than 2.0% of mass 174 345 0.60 (0.75) a Pass
174 50.0 - 120.0% of mass 95 46243 80.4 Pass
175 4.0 - 9.01% of mass 174 3399 5.91 (7.35) a Pass
176 93.0 - 101.0% of mass 174 43488 75.6 (94.0) a Pass
177 5.0 - 9.0% of mass 176 2778 4.83 (6.39) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V6W1158-ICV1158 6W27517.D 12/07/22 14:22 00:33 Initial cal verification 10
94 of 100
JD6284455.5.10
Instrument Performance Check (BFB)Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V6W1162-BFB Injection Date:12/11/22
Lab File ID:6W27611.D Injection Time:15:36
Instrument ID:GCMS6W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 9691 22.9 Pass
75 30.0 - 66.0% of mass 95 19464 46.1 Pass
95 Base peak, 100% relative abundance 42267 100.0 Pass
96 5.0 - 9.0% of mass 95 2715 6.42 Pass
173 Less than 2.0% of mass 174 331 0.78 (0.93) a Pass
174 50.0 - 120.0% of mass 95 35512 84.0 Pass
175 4.0 - 9.01% of mass 174 2564 6.07 (7.22) a Pass
176 93.0 - 101.0% of mass 174 33715 79.8 (94.9) a Pass
177 5.0 - 9.0% of mass 176 2107 4.98 (6.25) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V6W1162-CC1158 6W27612.D 12/11/22 16:09 00:33 Continuing cal 10
V6W1162-BS 6W27613.D 12/11/22 16:42 01:06 Blank Spike
V6W1162-BSD 6W27614.D 12/11/22 17:15 01:39 Blank Spike Duplicate
V6W1162-MB 6W27616.D 12/11/22 18:21 02:45 Method Blank
V6W1162-SCC 6W27617.D 12/11/22 18:53 03:17 Summa Cleaning Certification
V6W1162-SCC 6W27618.D 12/11/22 19:23 03:47 Summa Cleaning Certification
V6W1162-SCC 6W27619.D 12/11/22 19:56 04:20 Summa Cleaning Certification
V6W1162-SCC 6W27620.D 12/11/22 20:29 04:53 Summa Cleaning Certification
V6W1162-SCC 6W27621.D 12/11/22 21:02 05:26 Summa Cleaning Certification
V6W1162-SCC 6W27622.D 12/11/22 21:36 06:00 Summa Cleaning Certification
V6W1162-SCC 6W27623.D 12/11/22 22:09 06:33 Summa Cleaning Certification
V6W1162-SCC 6W27624.D 12/11/22 22:43 07:07 Summa Cleaning Certification
V6W1162-SCC 6W27625.D 12/11/22 23:16 07:40 Summa Cleaning Certification
V6W1162-SCC 6W27626.D 12/11/22 23:49 08:13 Summa Cleaning Certification
V6W1162-SCC 6W27627.D 12/12/22 00:22 08:46 Summa Cleaning Certification
V6W1162-SCC 6W27628.D 12/12/22 00:55 09:19 Summa Cleaning Certification
V6W1162-SCC 6W27630.D 12/12/22 02:01 10:25 Summa Cleaning Certification
V6W1162-SCC 6W27631.D 12/12/22 02:34 10:58 Summa Cleaning Certification
V6W1162-SCC 6W27632.D 12/12/22 03:07 11:31 Summa Cleaning Certification
V6W1162-SCC 6W27633.D 12/12/22 03:40 12:04 Summa Cleaning Certification
V6W1162-SCC 6W27634.D 12/12/22 04:13 12:37 Summa Cleaning Certification
V6W1162-SCC 6W27635.D 12/12/22 04:45 13:09 Summa Cleaning Certification
V6W1162-SCC 6W27636.D 12/12/22 05:18 13:42 Summa Cleaning Certification
V6W1162-SCC 6W27637.D 12/12/22 05:51 14:15 Summa Cleaning Certification
95 of 100
JD6284455.5.11
Instrument Performance Check (BFB)Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V6W1162-BFB Injection Date:12/11/22
Lab File ID:6W27611.D Injection Time:15:36
Instrument ID:GCMS6W
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V6W1162-SCC 6W27639.D 12/12/22 06:57 15:21 Summa Cleaning Certification
V6W1162-SCC 6W27640.D 12/12/22 07:30 15:54 Summa Cleaning Certification
V6W1162-SCC 6W27641.D 12/12/22 08:03 16:27 Summa Cleaning Certification
V6W1162-SCC 6W27642.D 12/12/22 08:35 16:59 Summa Cleaning Certification
V6W1162-SCC 6W27643.D 12/12/22 09:08 17:32 Summa Cleaning Certification
V6W1162-SCC 6W27644.D 12/12/22 09:41 18:05 Summa Cleaning Certification
V6W1162-SCC 6W27645.D 12/12/22 11:25 19:49 Summa Cleaning Certification
V6W1162-SCC 6W27646.D 12/12/22 11:58 20:22 Summa Cleaning Certification
96 of 100
JD6284455.5.11
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V7W57-BFB Injection Date:03/29/23
Lab File ID:7W01234.D Injection Time:21:16
Instrument ID:GCMS7W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 7503 24.4 Pass
75 30.0 - 66.0% of mass 95 16274 52.9 Pass
95 Base peak, 100% relative abundance 30736 100.0 Pass
96 5.0 - 9.0% of mass 95 1895 6.17 Pass
173 Less than 2.0% of mass 174 186 0.61 (0.82) a Pass
174 50.0 - 120.0% of mass 95 22704 73.9 Pass
175 4.0 - 9.01% of mass 174 1750 5.69 (7.71) a Pass
176 93.0 - 101.0% of mass 174 22899 74.5 (100.9) a Pass
177 5.0 - 9.0% of mass 176 1436 4.67 (6.27) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V7W57-IC57 7W01235.D 03/29/23 21:47 00:31 Initial cal 0.04
V7W57-IC57 7W01236.D 03/29/23 22:19 01:03 Initial cal 0.1
V7W57-IC57 7W01237.D 03/29/23 22:51 01:35 Initial cal 0.2
V7W57-IC57 7W01238.D 03/29/23 23:23 02:07 Initial cal 0.5
V7W57-IC57 7W01240.D 03/30/23 00:25 03:09 Initial cal 5
V7W57-ICC57 7W01241.D 03/30/23 00:58 03:42 Initial cal 10
V7W57-IC57 7W01242.D 03/30/23 01:30 04:14 Initial cal 20
V7W57-IC57 7W01243.D 03/30/23 02:04 04:48 Initial cal 40
V7W57-IC57 7W01244.D 03/30/23 02:40 05:24 Initial cal 50
V7W57-ICV57 7W01247.D 03/30/23 04:17 07:01 Initial cal verification 10
97 of 100
JD6284455.5.12
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Sample:V7W62-BFB Injection Date:04/04/23
Lab File ID:7W01360.D Injection Time:09:06
Instrument ID:GCMS7W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 6468 25.4 Pass
75 30.0 - 66.0% of mass 95 13237 51.9 Pass
95 Base peak, 100% relative abundance 25507 100.0 Pass
96 5.0 - 9.0% of mass 95 1597 6.26 Pass
173 Less than 2.0% of mass 174 266 1.04 (1.05) a Pass
174 50.0 - 120.0% of mass 95 25253 99.0 Pass
175 4.0 - 9.01% of mass 174 1869 7.33 (7.40) a Pass
176 93.0 - 101.0% of mass 174 24645 96.6 (97.6) a Pass
177 5.0 - 9.0% of mass 176 1527 5.99 (6.20) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V7W62-CC0057 7W01361.D 04/04/23 09:40 00:34 Continuing cal 10
V7W62-BS 7W01362.D 04/04/23 10:40 01:34 Blank Spike
V7W62-BSD 7W01363.D 04/04/23 11:15 02:09 Blank Spike Duplicate
V7W62-MB 7W01366.D 04/04/23 13:40 04:34 Method Blank
JD62844-1 7W01367.D 04/04/23 14:39 05:33 BF-SSV-12
JD62844-1DUP 7W01368.D 04/04/23 15:27 06:21 Duplicate
JD62844-2 7W01369.D 04/04/23 16:02 06:56 BF-SSV-01
JD62844-3 7W01370.D 04/04/23 16:36 07:30 BF-SSV-02
JD62844-4 7W01371.D 04/04/23 17:11 08:05 BF-SSV-03
JD62844-5 7W01372.D 04/04/23 17:45 08:39 BF-SSV-04
JD62844-6 7W01373.D 04/04/23 18:19 09:13 BF-SSV-05
JD62844-7 7W01374.D 04/04/23 18:53 09:47 BF-SSV-06
JD62844-8 7W01375.D 04/04/23 19:28 10:22 BF-SSV-07
JD62844-9 7W01376.D 04/04/23 20:03 10:57 BF-SSV-08
JD62844-10 7W01377.D 04/04/23 20:38 11:32 BF-SSV-09
JD62844-11 7W01378.D 04/04/23 21:13 12:07 BF-SSV-11
JD62844-12 7W01379.D 04/04/23 21:47 12:41 BF-SSV-DUP
JD62844-13 7W01380.D 04/04/23 22:22 13:16 BF-SSV-10
ZZZZZZ 7W01382.D 04/04/23 23:30 14:24 (unrelated sample)
98 of 100
JD6284455.5.13
Surrogate Recovery Summary Page 1 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Method:TO-15 Matrix:AIR
Samples and QC shown here apply to the above method
Lab Lab
Sample ID File ID S1
JD62844-1 7W01367.D 90
JD62844-2 7W01369.D 89
JD62844-3 7W01370.D 90
JD62844-4 7W01371.D 92
JD62844-5 7W01372.D 90
JD62844-6 7W01373.D 90
JD62844-7 7W01374.D 91
JD62844-8 7W01375.D 90
JD62844-9 7W01376.D 91
JD62844-10 7W01377.D 90
JD62844-11 7W01378.D 91
JD62844-12 7W01379.D 90
JD62844-13 7W01380.D 91
JD62844-1DUP 7W01368.D 91
V2W2791-SCC 2W62769.D 109
V3W3085-SCC 3W78328.D 104
V3W3085-SCC 3W78331.D 103
V3W3101-SCC 3W78742.D 100
V3W3115-SCC 3W79066.D 97
V6W1162-SCC 6W27617.D 97
V6W1162-SCC 6W27623.D 94
V7W62-BS 7W01362.D 96
V7W62-BSD 7W01363.D 97
V7W62-MB 7W01366.D 90
V2W2791-BS 2W62751.D 110
V2W2791-BSD 2W62752.D 111
V2W2791-MB 2W62755.D 110
V3W3085-BS 3W78321.D 107
V3W3085-BSD 3W78322.D 107
V3W3085-MB 3W78324.D 100
V3W3101-BS 3W78732.D 103
V3W3101-BSD 3W78733.D 100
V3W3101-MB 3W78735.D 99
V3W3115-BS 3W79061.D 101
V3W3115-BSD 3W79062.D 101
V3W3115-MB 3W79064.D 96
V6W1162-BS 6W27613.D 100
V6W1162-BSD 6W27614.D 100
V6W1162-MB 6W27616.D 95
99 of 100
JD6284455.6.1
Surrogate Recovery Summary Page 2 of 2
Job Number:JD62844
Account:HAHNCC Hart & Hickman
Project:George Fern Company, 2310 Steele Creeke Road, Charlotte, NC
Method:TO-15 Matrix:AIR
Samples and QC shown here apply to the above method
Surrogate Recovery
Compounds Limits
Surrogate Recovery
Compounds Limits
S1 = 4-Bromofluorobenzene 65-128%
100 of 100
JD6284455.6.1

Appendix D

Groundwater and Soil Gas Sampling Forms

6?%%%0DVWHU7HPSODWHV?)RUPV)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI/DVW8SGDWHGJob No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization CriteriaPrimary: Secondary:LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORD Well Location:Facility Name: Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft :___________ ___________ Well Diameter:Sampling Personnel:___________________________, __________________________ Screen Interval (ft ): _____________-______________ Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ft Weather Conditions:_______________________________________________________ NOTES:GROUNDWATER SAMPLING PARAMETERSStabilization criteria guidelines from the EPA SESD Operating Procedure for Groundwater Sampling, dated April 26, 2017.Turb. +/- 10% (<10 NTUs for metals)Water Level: slight or stable drawdown during purging pH +/- 0.1 unitS.Cond. +/- 5% ORP +/- 0 mVDO +/- 0.2 mg/LFDI-001George Fern Company3/6/2340AML3370s, sunnypumpingstarted at 12:2012:2512:3012:3512:4012:4512:5012:5513:0013:0524.4725.1625.4225.6825.8626.0426.2126.3826.42500 mL1000 mL1500 mL2000 mL2500 mL3000 mL3500 mL4000 mL4500 mL100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min2.542.752.863.133.423.193.143.113.1021.621.521.521.521.521.621.621.621.699.794.391.587.683.981.379.178.477.35.845.996.005.985.995.985.965.965.9681.080.387.375.891.385.390.193.895.54.092.044.261.094.824.546.653.453.53YSIPP-001Pace courier 3/7/23 19:00VOCs(8260):x3[HCl]; SVOCs(8270):x2[unpreserved];RCRA Metals(6020/7470):x1[HNO3]PeristalticPVC2-inch13:05PaceMW-11S2540PolyethyleneTOC 23.832.65TOCTOCgallons
6?%%%0DVWHU7HPSODWHV?)RUPV)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI/DVW8SGDWHGJob No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization CriteriaPrimary: Secondary:LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORD Well Location:Facility Name: Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft :___________ ___________ Well Diameter:Sampling Personnel:___________________________, __________________________ Screen Interval (ft ): _____________-______________ Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ft Weather Conditions:_______________________________________________________ NOTES:GROUNDWATER SAMPLING PARAMETERSStabilization criteria guidelines from the EPA SESD Operating Procedure for Groundwater Sampling, dated April 26, 2017.Turb. +/- 10% (<10 NTUs for metals)Water Level: slight or stable drawdown during purging pH +/- 0.1 unitS.Cond. +/- 5% ORP +/- 0 mVDO +/- 0.2 mg/LFDI-001George Fern Company3/6/2320AML1870s, sunnypumpingstarted at 14:1014:1514:2014:2514:3014:3514:4017.1717.3017.3517.4017.4817.50500 mL1000 mL1500 mL2000 mL2500 mL3000 mL100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min3.583.293.493.192.982.9420.820.820.820.720.720.782.277.376.876.577.076.55.085.085.075.065.055.05138.3151.7156.6160.5164.7166.30.334.370.600.430.410.40Pace courier3/7/23 19:00VOCs(8260):x3[HCl]; SVOCs(8270):x2[unpreserved];RCRA Metals(6020/7470):x1[HNO3]PeristalticPVC2-inch14:40PaceOFF-MW-1 / GW-DUP1020PolyethyleneTOC17.02 1.47TOCTOCgallons
6?%%%0DVWHU7HPSODWHV?)RUPV)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI/DVW8SGDWHGJob No:Well ID:Water Volume Pumping DOTemp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization CriteriaPrimary: Secondary:LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORD Well Location:Facility Name: Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft :___________________________ Well Diameter:Sampling Personnel:___________________________, __________________________ Screen Interval (ft ): _____________-______________ Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ft Weather Conditions:_______________________________________________________ NOTES:GROUNDWATER SAMPLING PARAMETERSStabilization criteria guidelines from the EPA SESD Operating Procedure for Groundwater Sampling, dated April 26, 2017.Turb. +/- 10% (<10 NTUs for metals)Water Level: slight or stable drawdown during purging pH +/- 0.1 unitS.Cond. +/- 5% ORP +/- 0 mVDO +/- 0.2 mg/LFDI-001George Fern Company3/6/2337AML3070s, sunnypumpingstarted at 16:4016:4516:5016:5517:0022.2722.3022.3222.32500 mL1000 mL1500 mL2000 mL100 mL/min100 mL/min100 mL/min100 mL/min1.471.401.461.3618.418.218.118.1206.3206.4207.9207.15.805.835.845.83116.8107.9104.7106.00.450.000.000.00YSIPP-001Pace courier 3/7/23 19:00VOCs(8260):x3[HCl]; SVOCs(8270):x2[unpreserved];RCRA Metals(6020/7470):x1[HNO3]PeristalticPVC2-inch17:00PaceOFF-MW-52237PolyethyleneTOC22.282.40TOCTOCgallons
6?%%%0DVWHU7HPSODWHV?)RUPV)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI/DVW8SGDWHGJob No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization CriteriaPrimary: Secondary:LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORD Well Location:Facility Name: Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft :___________________________ Well Diameter:Sampling Personnel:___________________________, __________________________ Screen Interval (ft ): _____________-______________ Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ft Weather Conditions:_______________________________________________________ NOTES:GROUNDWATER SAMPLING PARAMETERSStabilization criteria guidelines from the EPA SESD Operating Procedure for Groundwater Sampling, dated April 26, 2017.Turb. +/- 10% (<10 NTUs for metals)Water Level: slight or stable drawdown during purging pH +/- 0.1 unitS.Cond. +/- 5% ORP +/- 0 mVDO +/- 0.2 mg/LFDI-001George Fern Company3/7/2348AML4070s, sunnypumpingstarted at 14:2014:2514:3014:3514:4014:4514:5014:5515:0015:0515:1015:1515:2033.6234.1634.1034.0233.9733.9733.9533.9233.9133.8933.8933.870.5 gal1.0 gal1.5 gal2.0 gal2.5 gal3.0 gal3.5 gal4.0 gal4.5 gal5.0 gal5.5 gal6.0 gal0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min8.283.913.553.643.523.613.503.523.593.713.433.5117.917.918.218.218.418.718.618.618.418.318.318.3183.9185.1184.7184.7184.7184.7184.4183.7184.8184.0183.96.105.885.875.895.905.915.905.905.905.905.895.90119.7134.6130.8127.1126.9126.3127.6126.1124.4127.3128.2129.1311.40200.70167.50191.90162.30191.70132.80115.00117.5086.7968.3861.71YSIPP-001Pace courier 3/7/23 19:00VOCs(8260):x3[HCl]; SVOCs(8270):x2[unpreserved];RCRA Metals(6020/7470):x1[HNO3]BladderPVC2-inch16:35PaceOFF-MW-63348PolyethyleneTOC184.232.425.72TOCTOCgallons
6?%%%0DVWHU7HPSODWHV?)RUPV)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI/DVW8SGDWHGJob No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization CriteriaPrimary: Secondary:LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORD Well Location:Facility Name: Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft :___________________________ Well Diameter:Sampling Personnel:___________________________, __________________________ Screen Interval (ft ): _____________-______________ Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ft Weather Conditions:_______________________________________________________ NOTES:GROUNDWATER SAMPLING PARAMETERSStabilization criteria guidelines from the EPA SESD Operating Procedure for Groundwater Sampling, dated April 26, 2017.Turb. +/- 10% (<10 NTUs for metals)Water Level: slight or stable drawdown during purging pH +/- 0.1 unitS.Cond. +/- 5% ORP +/- 0 mVDO +/- 0.2 mg/LFDI-001George Fern Company3/7/2348AML4070s, sunnypumpingstarted at 14:2015:2515:3515:4515:5516:0516:1516:2516:3533.8633.8233.8133.8233.8033.8133.8033.816.5 gal7.5 gal8.5 gal9.5 gal10.5 gal11.5 gal12.5 gal13.5 gal0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min0.1 gal/min3.503.603.553.463.593.503.563.5018.218.418.518.718.818.718.718.2183.8183.6183.8183.5183.6183.4183.6183.55.895.905.895.905.895.895.895.89129.8130.5131.3131.4128.6139.6128.1131.756.6336.4437.7436.0625.6317.8812.806.91YSIPP-001Pace courier 3/7/23 19:00VOCs(8260):x3[HCl]; SVOCs(8270):x2[unpreserved];RCRA Metals(6020/7470):x1[HNO3]BladderPVC2-inch16:35PaceOFF-MW-63348BondedpolyethyleneTOC32.425.72TOCTOCgallons
6?%%%0DVWHU7HPSODWHV?)RUPV)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI/DVW8SGDWHGJob No:Well ID:Water Volume Pumping DOTemp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization CriteriaPrimary: Secondary:LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORD Well Location:Facility Name: Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft :___________________________ Well Diameter:Sampling Personnel:___________________________, __________________________ Screen Interval (ft ): _____________-______________ Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ft Weather Conditions:_______________________________________________________ NOTES:GROUNDWATER SAMPLING PARAMETERSStabilization criteria guidelines from the EPA SESD Operating Procedure for Groundwater Sampling, dated April 26, 2017.Turb. +/- 10% (<10 NTUs for metals)Water Level: slight or stable drawdown during purging pH +/- 0.1 unitS.Cond. +/- 5% ORP +/- 0 mVDO +/- 0.2 mg/LFDI-001George Fern Company3/6/2324AML1970s, sunnypumpingstarted at 15:5516:0016:0516:1016:1518.1418.4418.6318.74500 mL1000 mL1500 mL2000 mL100 mL/min100 mL/min100 mL/min100 mL/min0.350.190.150.1418.718.418.518.4148.5146.5147.5147.35.025.055.155.19159.2139.3128.1127.60.000.000.000.00YSIPP-001Pace courier 3/7/23 19:00VOCs(8260):x3[HCl]; SVOCs(8270):x2[unpreserved];RCRA Metals(6020/7470):x1[HNO3]PeristalticPVC216:15PaceOFF-MW-7924PolyethyleneTOC17.881.00TOCTOCgallons18.06
&Žƌŵ^sͲϭSub-Slab / Soil Gas Vapor Installation Field FormProject No.:__________________ Sampler:______________________Weather:____________________________________________________________Surface MaterialSlab Thickness (if appl.) Material Below Slab (if appl.)Depth of Screen (if appl.)Type Date & TimeAmbient Temp.Purge MethodVolume PurgedShroud Helium Conc.Purge Helium Conc.Leak Test Pass? (see note)SS, SGPerm., Temp.Concrete, soil, gravel, asphaltInchesGravel, sand, clay, etc.ft bgsFull sample train or point-onlymm/dd/yy 24-hroFSyringe, pumpLiters (see notes for calc.)%% or ppm(indicate units below)Yes / No^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporary; Volume Purged = x3 purge volumes = 3*L*aLast updated: 4/21/2022" Hg = inches of mercury; ppm = parts per millionNotes:________________________________________________________________________________________________________________________________________________________________________________________________________________Sample ID TypeVapor Monitoring Point Construction Helium Leak TestEŽƚĞ͗>ĞĂŬdĞƐƚZĞƋƵŝƌĞŵĞŶƚƐWĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ůĞĂŬƚĞƐƚƉĂƐƐĞƐŝĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƉƵƌŐĞĂŝƌŝƐůĞƐƐƚŚĂŶϭϬйŽĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƐŚƌŽƵĚ͘L = length of tubing/pipe (ft)a = 0.163 for 2" diameter (L/ft)a = 0.010 for 0.25" diameter (L/ft)͗ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽdžͰLJKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ/ŶƐƚĂůůĂƚŝŽŶ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WFDI.001Ted SmithSunny & 63/41BF-SSV-1215067SS Temp Conc 6 Gravel NAFull3/8/2370 Syringe 1 L 16.1 0 ppm YesFC365BF-SSV-0114309SS Temp Conc 6 Gravel NAFull3/8/2370 Syringe 1 L 10.3 0 ppm YesMC270BF-SSV-0215017SS Temp Conc 6 Gravel NAFull3/8/2370 Syringe 1 L 12.2 0 ppm YesFC989BF-SSV-0314383SS Temp Conc 6 Gravel NAFull3/8/2370 Syringe 1 L 12.4 0 ppm YesMC228BF-SSV-0415065SS Temp Conc 6 Gravel NAFull3/8/2370 Syringe 1 L 11.5 0 ppm YesFC661BF-SSV-0514384SS Temp Conc 6 Gravel NAFull3/8/2370 Syringe 1 L 10.3 0 ppm YesFC1019
&Žƌŵ^sͲϭSub-Slab / Soil Gas Vapor Installation Field FormProject No.:__________________ Sampler:______________________Weather:____________________________________________________________Surface MaterialSlab Thickness (if appl.) Material Below Slab (if appl.)Depth of Screen (if appl.)Type Date & TimeAmbient Temp.Purge MethodVolume PurgedShroud Helium Conc.Purge Helium Conc.Leak Test Pass? (see note)SS, SGPerm., Temp.Concrete, soil, gravel, asphaltInchesGravel, sand, clay, etc.ft bgsFull sample train or point-onlymm/dd/yy 24-hroFSyringe, pumpLiters (see notes for calc.)%% or ppm(indicate units below)Yes / No^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporary; Volume Purged = x3 purge volumes = 3*L*aLast updated: 4/21/2022" Hg = inches of mercury; ppm = parts per millionNotes:________________________________________________________________________________________________________________________________________________________________________________________________________________Sample ID TypeVapor Monitoring Point Construction Helium Leak TestEŽƚĞ͗>ĞĂŬdĞƐƚZĞƋƵŝƌĞŵĞŶƚƐWĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ůĞĂŬƚĞƐƚƉĂƐƐĞƐŝĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƉƵƌŐĞĂŝƌŝƐůĞƐƐƚŚĂŶϭϬйŽĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƐŚƌŽƵĚ͘L = length of tubing/pipe (ft)a = 0.163 for 2" diameter (L/ft)a = 0.010 for 0.25" diameter (L/ft)͗ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽdžͰLJKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ/ŶƐƚĂůůĂƚŝŽŶ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WFDI.001Ted SmithSunny & 63/41BF-SSV-0614366SS Temp Conc 6 Gravel NAFull3/8/2370 Syringe 1 L 11.2 0 ppm YesFC703BF-SSV-0715045SS Temp Conc 6 Gravel NAFull3/8/2370 Syringe 1 L 10.7 0 ppm YesFC770BF-SSV-0815052SS Temp Conc 6 Gravel NAFull3/8/2370 Syringe 1 L 10.5 0 ppm YesFC1050BF-SSV-0915028SS Temp Conc 6 Gravel NAFull3/8/2370 Syringe 1 L 11.9 0 ppm YesFC546BF-SSV-1114336SS Temp Conc 6 Gravel NAFull3/13/2370 Syringe 1 L 10.6 0 ppm YesFC1241BF-SSV-1013011SS Temp Conc 6 Gravel NAFull3/13/2370 Syringe 1 L 11.3 0 ppm YesFC1249BF-SSV-DUP taken on BF-SSV-11Can: 15060
&Žƌŵ^sͲϮSub-Slab / Soil Gas Vapor Sampling Field FormProject No.:___________________ Sampler:______________________ Weather:____________________________________________________________Date Proposed Sampling Duration Time Canister PressureOutdoor TemperatureOutdoor HumidityIndoor TemperatureIndoor Humiditymm/dd/yy Minutes24-hr" HgoF%oF%^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporaryLast updated: 6/18/2020" Hg = inches of mercuryNotes:_____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗Sample ID^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗Sampling Information Indoor ParametersOutdoor ParametersSampling PeriodEŽƚĞ͗WĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ƐŚƵƚͲŝŶƚĞƐƚĂŶĚŚĞůŝƵŵůĞĂŬĐŚĞĐŬŵƵƐƚďĞƉĂƐƐĞĚďĞĨŽƌĞƐĂŵƉůŝŶŐ͗͘ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽdžͰLJKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ^ĂŵƉůŝŶŐ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WFDI.001Ted SmithSunny & 64/41BF-SSV-121L1506703/08/2310100 mL/min0931 -12NA NA 70FC3650937 -50927 -2870BF-SSV-011L1033 -261430903/08/23101038 -11NA NA 70 70100 mL/minMC2701043 -5BF-SSV-021055 -301L1501703/08/23 10NA NA 70 70FC989100 mL/min1100 -131105 -5BF-SSV-031127 -281L1438303/08/23101132 -13NA NA 70 70MC228100 mL/min1137 -5BF-SSV-041206 -291L1506503/08/23101211 -13NA NA 70 70100 mL/minFC6611216 -5BF-SSV-051L1242 -2903/08/2314384101247 -13NA NA 70 70FC1019100 mL/min1252 -5
&Žƌŵ^sͲϮSub-Slab / Soil Gas Vapor Sampling Field FormProject No.:___________________ Sampler:______________________ Weather:____________________________________________________________Date Proposed Sampling Duration Time Canister PressureOutdoor TemperatureOutdoor HumidityIndoor TemperatureIndoor Humiditymm/dd/yy Minutes24-hr" HgoF%oF%^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporaryLast updated: 6/18/2020" Hg = inches of mercuryNotes:_____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗Sample ID^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗Sampling Information Indoor ParametersOutdoor ParametersSampling PeriodEŽƚĞ͗WĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ƐŚƵƚͲŝŶƚĞƐƚĂŶĚŚĞůŝƵŵůĞĂŬĐŚĞĐŬŵƵƐƚďĞƉĂƐƐĞĚďĞĨŽƌĞƐĂŵƉůŝŶŐ͗͘ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽdžͰLJKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ^ĂŵƉůŝŶŐ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WFDI.001Ted SmithSunny & 64/41BF-SSV-061L1436603/08/2310100 mL/min1300 -12NA NA 70FC7031305 -51255 -2770BF-SSV-071L1403 -281504503/08/23101408 -13NA NA 70 70100 mL/minFC7701413 -5BF-SSV-081428 -271L1505203/08/23 10NA NA 70 70FC1050100 mL/min1433 -111438 -5BF-SSV-091453 -281L1502803/08/23101458 -12NA NA 70 70FC546100 mL/min1503 -5BF-SSV-111533 -261L1433603/13/23101540 -12NA NA 70 70100 mL/minFC12411548 -5BF-SSV-101L1603 -2903/13/2313011101609 -13NA NA 70 70FC1249100 mL/min1615 -5BF-SSV-DUP taken on BF-SSV-11Can: 15060

Appendix E

DEQ Risk Calculators
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Site-Wide Hypothetical Worst Case Sub-Slab Vapor
North Carolina Department of Environmental Quality
Risk Calculator
George Fern Company
2310 Old Steele Creek Road
Brownfields Redevelopment Section
25044-21-060
January 2023
November 2022 EPA RSL Table
Prepared By:Hart & Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 25044-21-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Sub-Slab Vapor
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: January 2023Basis: November 2022 EPA RSL TableSite ID: 25044-21-060Exposure Unit ID: Site-Wide Hypothetical Worst Case Sub-Slab Vapor Description of Exposure Point Concentration Selection:Exposure Point Concentration (ug/m3)Notes:CAS NumberChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion11367-64-1Acetoneug/m31.2J71-43-2 Benzeneug/m31.9J110-83-8 Cyclohexeneug/m32.7J75-71-8 Dichlorodifluoromethaneug/m357.9141-78-6Ethyl Acetateug/m35..2100-41-4Ethylbenzeneug/m35.6109-99-9~Tetrahydrofuranug/m32.8110-54-3Hexane, N-ug/m31767-63-0Isopropanolug/m33.578-93-3Methyl Ethyl Ketone (2-Butanone)ug/m31075-09-2Methylene Chlorideug/m34J91-20-3 ~Naphthaleneug/m35.5115-07-1Propyleneug/m3521127-18-4Tetrachloroethyleneug/m317108-88-3Tolueneug/m398.979-01-6Trichloroethyleneug/m37.81330-20-7Xylenesug/m3Input Form 2DSoil Gas Exposure Point Concentration TableNote: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsNorth Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 25044-21-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Sub-Slab Vapor
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 5.6E-07 1.5E-01 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 25044-21-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Sub-Slab Vapor
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 113 1.13 --
71-43-2 Benzene 1.2 0.012 1.6E+00 2.6E+01 7.6E-09 9.1E-05
110-83-8 Cyclohexene 1.9 0.019 -8.8E+02 4.3E-06
75-71-8 Dichlorodifluoromethane 2.7 0.027 -8.8E+01 6.2E-05
141-78-6 Ethyl Acetate 57.9 0.579 -6.1E+01 1.9E-03
100-41-4 Ethylbenzene 5..2 4.9E+00 8.8E+02
109-99-9 ~Tetrahydrofuran 5.6 0.056 -1.8E+03 6.4E-06
110-54-3 Hexane, N-2.8 0.028 -6.1E+02 9.1E-06
67-63-0 Isopropanol 17 0.17 -1.8E+02 1.9E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)3.5 0.035 -4.4E+03 1.6E-06
75-09-2 Methylene Chloride 10 0.1 1.2E+03 5.3E+02 8.2E-11 3.8E-05
91-20-3 ~Naphthalene 4 0.04 3.6E-01 2.6E+00 1.1E-07 3.0E-03
115-07-1 Propylene 5.5 0.055 -2.6E+03 4.2E-06
127-18-4 Tetrachloroethylene 521 5.21 4.7E+01 3.5E+01 1.1E-07 3.0E-02
108-88-3 Toluene 17 0.17 -4.4E+03 7.8E-06
79-01-6 Trichloroethylene 98.9 0.989 3.0E+00 1.8E+00 3.3E-07 1.1E-01
1330-20-7 Xylenes 7.8 0.078 -8.8E+01 1.8E-04
Cumulative: 5.6E-07 1.5E-01
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator