26067_Tarmac Virginia_Addendum to Supplemental Phase II EA Report_20230929

September 29, 2023

Mr. Peter Doorn
NCDEQ - Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, NC 27699-1646

Reference: ADDENDUM TO REPORT OF SUPPLEMENTAL PHASE II
ENVIRONMENTAL ASSESSMENT
Proposed Abernethy Lofts Residential Development Site
Tarmac Virginia Brownfields Property
3934 Raleigh Street
Charlotte, North Carolina
Brownfields Project No. 26067-22-060
ESP Project No. E6-KO31.600

Dear Mr. Doorn:

ESP Associates, Inc. (ESP), on behalf of Abernethy Lofts LLC, is pleased to submit the attached
addendum to our report titled “Report of Supplemental Phase II Environmental Assessment -
Proposed Abernethy Lofts Residential Development Site’ dated February 9, 2023 for the above-
referenced site (Site). The Site is the Tarmac Virginia Brownfields Property located at 3934 Raleigh
Street in Charlotte, North Carolina. This addendum documents supplemental soil sampling and
laboratory analyses activities performed as part of redevelopment of the Brownfields property.

If you should have any questions, please do not hesitate to contact Chris Ward at [phone].

Sincerely,
ESP Associates, Inc.
Erin Tollinger Christopher J. Ward, PG, RSM
Staff Scientist Senior Geologist
NC License No. 1600

ADDENDUM TO REPORT OF 
SUPPLEMENTAL PHASE II 
ENVIRONMENTAL ASSESSMENT 

PROPOSED ABERNETHY LOFTS RESIDENTIAL DEVELOPMENT SITE ‐ 
TARMAC VIRGINIA BROWNFIELDS PROPERTY 
3934 RALEIGH STREET 
CHARLOTTE, NORTH CAROLINA 
BROWNFIELDS PROJECT NO. 26067‐22‐060
ESP PROJECT NO. E6‐KO31.600 

Prepared For: 
North Carolina Department of Environmental Quality 
Division of Waste Management – UST Section 
1646 Mail Service Center 
Raleigh, North Carolina 27699‐1646

On Behalf: 
Abernethy Lofts LLC 
1228 Euclid Avenue, 4th Floor 
Cleveland, Ohio 44115 

Prepared By: 
ESP Associates, Inc. 
P. O. Box 7030 
Charlotte, North Carolina 28241

September 29, 2023 

TABLE OF CONTENTS

Section Page

1.0 INTRODUCTION............................................................................................................. 1
2.0 SOIL INVESTIGATION ................................................................................................. 1
3.0 SOIL ANALYTICAL RESULTS .................................................................................... 2
4.0 INVESTIGATION DERIVED WASTE MANAGEMENT .......................................... 2
5.0 SUMMARY AND CONCLUSIONS ............................................................................... 2

FIGURES

Figure 1 USGS Topographic Site Location Map
Figure 2 Sample Locations Map
Figure 3 Supplemental Soil Contaminant Concentration Map

TABLES

Table 1 Summary of Soil Analytical Results

APPENDICES

Appendix A Laboratory Analysis Reports

Addendum to Report of Suplemental Phase II Environmental Assessment ESP Project No. E6-KO31.600
Proposed Abernethy Lofts Residential Development (Tarmac Virginia Brownfields Property) September 29, 2023
1

1.0 INTRODUCTION

This addendum to our previously submitted report titled “Report of Supplemental Phase II
Environmental Assessment - Proposed Abernethy Lofts Residential Development Site’ dated
February 9, 2023, has been prepared by ESP Associates, Inc. (ESP) on behalf of Abernethy Lofts
LLC. The Proposed Abernethy Lofts Residential Development Site (Site), also referred to as the
Tarmac Virginia Brownfields Property, is located at 3934 Raleigh Street in Charlotte,
Mecklenburg County, North Carolina (see Figure 1).

As detailed below, this addendum includes the collection and laboratory analysis of shallow soil
samples to augment previously reported soils data. These data were collected to assist with future
deposition options for cut soils resulting from upcoming grading operations associated with
redevelopment of the property for multi-family residential use. The assessment activities were
performed in accordance with your August 9, 2023, email and in general accordance with
NCDEQ’s Inactive Hazardous Sites Branch (IHSB) “Guidelines for Assessment and Cleanup of
Contaminated Sites” dated September 2022.

2.0 SOIL INVESTIGATION

On August 22, 2023, ESP conducted a supplemental Phase II environmental assessment (EA) on
the Site which included the collection of seven soil samples (plus one duplicate quality control
[QC] sample) for laboratory analysis. The soil samples, designated as SS-1, SS-2, SS-3, SS-5, SS-
7, SS-8, SS-9, and SS-DUP (duplicate of SS-9), were collected from a depth of interval of 0 - 3
feet below ground surface (ft bgs) to further characterize shallow soil quality in those areas to be
cut as part of planned Site grading. As depicted on Figure 3, the above seven soil samples were
completed at the approximate locations of samples collected in November 2022 for SS-1, SS-2,
SS-3, SS-5, SS-7, SS-8, and SS-9.

Soil samples SS-1, SS-2, SS-3, SS-5, SS-7, SS-8, SS-9, and SS-DUP, collected using a
decontaminated stainless-steel hand auger, were placed in laboratory-provided labeled containers
with appropriate preservatives for delivery under standard chain-of-custody procedures to Pace
Analytical Services (Pace), a North Carolina-certified laboratory. Pace analyzed the soil samples for
the following analytes:
• SS-1, SS-2, SS-7, SS-8, and SS-9 - 8 RCRA metals (arsenic, barium, cadmium, total
chromium, lead, mercury selenium, and silver) by EPA Methods 6020B/7471B plus
hexavalent chromium by EPA Method 7199; and
• SS-3 and SS-5 - hexavalent chromium by EPA Method 7199.

The following field QC sample was also collected:
• Duplicate soil sample (SS-DUP) of SS-9 was analyzed for the 8 RCRA metals by EPA
Methods 6020B/7471B plus hexavalent chromium by EPA Method 7199.

It should be noted that the glass container for soil sample SS-1 was found to be broken upon
delivery to the laboratory; therefore, ESP collected another soil sample from the SS-1 location per
the above sampling protocol on August 28, 2023.
Addendum to Report of Suplemental Phase II Environmental Assessment ESP Project No. E6-KO31.600
Proposed Abernethy Lofts Residential Development (Tarmac Virginia Brownfields Property) September 29, 2023
3.0 SOIL ANALYTICAL RESULTS

A summary of soil sample analytical results for SS-1, SS-2, SS-3, SS-5, SS-7, SS-8, SS-9, and SS-
DUP along with previous soil samples collected by ESP is presented in Table 1. The laboratory
analytical reports for this sampling event are provided in Appendix A. The soil sample analytical
results are compared to the Residential Health - Preliminary Soil Remediation Goals (RH-PSRGs),
also shown in Table 1, which have been established by the NCDEQ’s IHSB. Soil sample analytical
results that exceeded their corresponding RH-PSRGs for these samples along with previous SS-1
through SS-10 samples are presented on Figure 3.

As shown in Table 1 and on Figure 3, two metals (arsenic and hexavalent chromium) were detected
above their corresponding RH-PSRGs during this sampling event. The two metals were detected
at concentrations exceeding their corresponding RH-PSRGs in one or more of the soil samples
collected during this sampling event as noted below:
• Arsenic was detected above its RH-PSRG in 3 of 7 soil samples at concentrations ranging
from 0.883J to 3.33 mg/kg. Arsenic exceeded its RH-PSRG of 0.68 mg/kg in samples:
SS-1 (3.29 mg/kg), SS-2 (0.883J), and SS-9 (3.33 mg/kg).
• Hexavalent chromium was detected above its RH-PSRG in 4 of 7 soil samples at
concentrations ranging from 0.414J to 0.821J mg/kg. Hexavalent chromium exceeded its
RH-PSRG of 0.31 mg/kg in samples: SS-1 (0.735J mg/kg), SS-7 (0.559J mg/kg), SS-8
(0.414J mg/kg), and SS-9 (0.821J mg/kg).

One blind field duplicate soil sample was collected and analyzed during the supplemental soil
investigation. SS-DUP was collected on August 22, 2023, as a duplicate of SS-9. As shown in
Table 1, sample analytical results for the duplicate pair were generally consistent.

4.0 INVESTIGATION DERIVED WASTE MANAGEMENT

Investigation-derived wastes (IDW) consisted of boring cuttings, disposable sampling equipment,
and used personal protective equipment (PPE). Boring cuttings from the seven shallow soil
borings not used for soil sample collection were returned to the boreholes from which they
originated. Used PPE and disposable sampling equipment were bagged and disposed off-Site at
an appropriate location (e.g., a municipal landfill).

5.0 SUMMARY AND CONCLUSIONS

This section presents a summary of and conclusions associated with the supplemental Phase II EA
activities as follows:
• A total of 7 shallow soil samples were collected for laboratory analysis from the 0 to 3 ft
bgs interval to further characterize shallow soil quality in those areas to be cut as part of
planned Site grading;
• The soil samples were analyzed for either the 8 RCRA metals by EPA Methods
6020B/7471B plus hexavalent chromium by EPA Method 7199 (SS-1, SS-2, SS-7, SS-8,
and SS-9) or for hexavalent chromium by EPA Method 7199 (SS-3 and SS-5);
Addendum to Report of Suplemental Phase II Environmental Assessment ESP Project No. E6-KO31.600
Proposed Abernethy Lofts Residential Development (Tarmac Virginia Brownfields Property) September 29, 2023
• Two metals (arsenic and hexavalent chromium) were detected above their corresponding
RH-PSRGs during this sampling event;
• Arsenic was detected above its RH-PSRG in 3 of 7 soil samples at concentrations ranging
from 0.883J to 3.33 mg/kg. Arsenic exceeded its RH-PSRG of 0.68 mg/kg in samples:
SS-1 (3.29 mg/kg), SS-2 (0.883J), and SS-9 (3.33 mg/kg); and
• Hexavalent chromium was detected above its RH-PSRG in 4 of 7 soil samples at
concentrations ranging from 0.414J to 0.821J mg/kg. Hexavalent chromium exceeded its
RH-PSRG of 0.31 mg/kg in samples: SS-1 (0.735J mg/kg), SS-7 (0.559J mg/kg), SS-8
(0.414J mg/kg), and SS-9 (0.821J mg/kg).

Results of the above soil sampling and analysis along with previous assessment results will be
used in determining options for the final deposition of excavated soil from the Site. These soil
deposition options will likely include, based on prior Brownfields Program approval, reuse on-Site
as structural fill (with appropriate surface cover), transport to another Brownfields site for their
use as structural fill, or transport to landfill for permitted disposal/use.

FIGURES

0 1,250 2,500Feet
ESP Associates, Inc.
P.O. Box 7030Charlotte, NC 28241
phone [phone]
www.espassociates.com
SHEET TITLE
PROJECT
PROJECT NO.
SCALE
DRAWN BY
CHECKED BY
KO31.600
CD
NZDATE07/07/2022
FIGURE 1USGS TOPOGRAPHIC SITE LOCATION MAPµAs Shown
CHARLOTTE, NORTH CAROLINA
All locations are approximate.
ABERNETHY LOFTS
LEGEND:
ABERNETHY LOFTS BOUNDARY
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0 30 60Feet
ESP Associates, Inc.
P.O. Box 7030Charlotte, NC 28241
phone [phone]
www.espassociates.com
SHEET TITLE
PROJECT
PROJECT NO.
SCALE
DRAWN BY
CHECKED BY
KO31.600
ET
CWDATE04/27/2023
FIGURE 2SAMPLE LOCATIONS MAPµAs Shown
CHARLOTTE, NORTH CAROLINA
PROPOSED ABERNETHY LOFTSRESIDENTIAL DEVELOPMENT SITE
LEGEND:
ABERNETHY LOFTS BOUNDARY
SOIL BORING
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SAMPLE LOCATIONS SHOWN WERELOCATED BY A LAND SURVEYORWITH THE EXCEPTION OF PSG-1 THROUGH PSG-8SOIL GAS PROBE
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0 40 80Feet
ESP Associates, Inc.
P.O. Box 7030Charlotte, NC 28241
phone [phone]
www.espassociates.com
SHEET TITLE
PROJECT
PROJECT NO.
SCALE
DRAWN BY
CHECKED BY
KO31.600
CD
CWDATE9/12/2023
FIGURE 3SUPPLEMENTAL SOIL CONTAMINANT CONCENTRATION MAPµAs Shown
CHARLOTTE, NORTH CAROLINA
PROPOSED ABERNETHY LOFTSRESIDENTIAL DEVELOPMENT SITE
LEGEND:
ABERNETHY LOFTS BOUNDARY
SOIL BORING&>
SAMPLE LOCATIONS SHOWN WERELOCATED BY A LAND SURVEYOR

TABLES

Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 1 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DateArsenic0.68 C2.0 1.3 1.8 2.5 1.8 1.9 3.3 1.8 7.5 0.89 2.4Barium3,100 N28.5 63.2 73.5 14.6 27.0 128 40.7 66.3 124 108 70.6Cadmium1.4 N <0.038U0.13 0.047 J<0.037U<0.040U<0.040U0.13<0.052U0.84 0.053 J 0.21Chromium, Total23,000 N g21.1 4.5 6.3 18.8 29.5 16.1 35.1 103 49.2 6.5 16.0Lead40010.5 3.6 4.6 6.4 4.6 6.0 9.6 3.4 107 3.1 19.6Mercury2.3 N0.079<0.011U<0.012U0.033 0.033 0.053 0.049<0.013U0.35<0.0095U0.034Selenium78 N0.22 J 0.32 J 0.37 J 0.39 J 0.28 J 0.36 J 0.29 J 0.29 J 0.72<0.097U0.40 JSilver78 N <0.18U<0.21U<0.21U<0.17U<0.18U<0.18U<0.18U<0.24U<0.16U<0.16U<0.18UChromium, Hexavalent0.31 C <3.2U<4.2U<4.5U<2.7U<3.0U<3.7U<46.6U<6.3U<4.7U<4.0U<6.4UVOCs - 8260DAcetone14,000 N <0.045U<0.059U<0.060U<0.039U<0.045U<0.046U<0.043U<0.075U<0.040U<0.037U<0.041UBenzene1.2 C <0.0028U<0.0036U<0.0037U<0.0024U<0.0028U<0.0028U<0.0027U<0.0046U<0.0025U<0.0023U<0.0025UBromochloromethane32 N <0.0021U<0.0027U<0.0028U<0.0018U<0.0021U<0.0021U<0.0020U<0.0035U<0.0018U<0.0017U<0.0019UBromodichloromethane0.31 C <0.0027U<0.0035U<0.0036U<0.0024U<0.0027U<0.0027U<0.0026U<0.0045U<0.0024U<0.0022U<0.0025UBromoform20 C <0.0025U<0.0032U<0.0033U<0.0022U<0.0025U<0.0025U<0.0024U<0.0041U<0.0022U<0.0020U<0.0023UBromomethane1.4 N <0.011U<0.014U<0.015U<0.0097U<0.011U<0.011U<0.011U<0.018U<0.0098U<0.0091U<0.010U2-Butanone (MEK)5,500 N <0.033U0.049 J<0.045U<0.029U0.035 J<0.034U<0.032U<0.056U0.037 J 0.035 J<0.031UCarbon disulfide160 N <0.0087U<0.012U<0.012U<0.0077U<0.0088U<0.0089U<0.0084U<0.015U<0.0078U<0.0072U<0.0080UCarbon tetrachloride0.69 C <0.0026U<0.0034U<0.0035U<0.0023U<0.0026U<0.0027U<0.0025U<0.0044U<0.0023U<0.0021U<0.0024UChlorobenzene58 N <0.0013U<0.0018U<0.0018U<0.0012U<0.0013U<0.0014U<0.0013U<0.0022U<0.0012U<0.0011U<0.0012UChloroethane1,100 N <0.0054U<0.0071U<0.0072U<0.0047U<0.0054U<0.0055U<0.0052U<0.0090U<0.0048U<0.0044U<0.0049UChloroform0.34 C <0.0042U<0.0056U<0.0057U<0.0037U<0.0042U<0.0043U<0.0041U<0.0071U<0.0038U<0.0035U<0.0039UChloromethane23 N <0.0059U<0.0077U<0.0078U<0.0051U<0.0059U<0.0060U<0.0056U<0.0098U<0.0052U<0.0048U<0.0054UCyclohexane1,400 N <0.0042U<0.0055U<0.0056U<0.0037U<0.0042U<0.0043U<0.0040U<0.0070U0.0078<0.0035U<0.0039U1,2-Dibromo-3-chloropropane0.0056 C <0.0027U<0.0036U<0.0036U<0.0024U<0.0027U<0.0028U<0.0026U<0.0045U<0.0024U<0.0022U<0.0025UDibromochloromethane8.3 C <0.0039U<0.0051U<0.0052U<0.0034U<0.0039U<0.0040U<0.0038U<0.0066U<0.0035U<0.0032U<0.0036U1,2-Dibromoethane (EDB)0.038 C <0.0031U<0.0040U<0.0041U<0.0027U<0.0031U<0.0031U<0.0029U<0.0051U<0.0027U<0.0025U<0.0028U1,2-Dichlorobenzene380 N <0.0025U<0.0033U<0.0034U<0.0022U<0.0025U<0.0026U<0.0024U<0.0042U<0.0022U<0.0021U<0.0023U1,3-Dichlorobenzene~ <0.0022U<0.0028U<0.0029U<0.0019U<0.0022U<0.0022U<0.0021U<0.0036U<0.0019U<0.0018U<0.0020U1,4-Dichlorobenzene2.8 C <0.0018U<0.0024U<0.0024U<0.0016U<0.0018U<0.0018U<0.0017U<0.0030U<0.0016U<0.0015U<0.0017UDichlorodifluoromethane18 N <0.0030U<0.0040U<0.0040U<0.0027U<0.0030U<0.0031U<0.0029U<0.0051U<0.0027U<0.0025U<0.0028U1,1-Dichloroethane3.8 C <0.0029U<0.0038U<0.0038U<0.0025U<0.0029U<0.0029U<0.0028U<0.0048U<0.0026U<0.0024U<0.0026U1,2-Dichloroethane0.49 C <0.0046U<0.0061U<0.0062U<0.0041U<0.0046U<0.0047U<0.0044U<0.0077U<0.0041U<0.0038U<0.0042U1,1-Dichloroethene48 N <0.0029U<0.0038U<0.0038U<0.0025U<0.0029U<0.0029U<0.0028U<0.0048U<0.0026U<0.0024U<0.0026Ucis-1,2-Dichloroethene13 N <0.0024U<0.0031U<0.0032U<0.0021U<0.0024U<0.0024U<0.0023U<0.0040U<0.0021U<0.0020U<0.0022Utrans-1,2-Dichloroethene15 N <0.0024U<0.0032U<0.0033U<0.0021U<0.0024U<0.0025U<0.0023U<0.0041U<0.0022U<0.0020U<0.0022U1,2-Dichloropropane2.6 C <0.0021U<0.0027U<0.0028U<0.0018U<0.0021U<0.0021U<0.0020U<0.0035U<0.0019U<0.0017U<0.0019Ucis-1,3-Dichloropropene~ <0.0019U<0.0025U<0.0025U<0.0017U<0.0019U<0.0019U<0.0018U<0.0032U<0.0017U<0.0016U<0.0017Utrans-1,3-Dichloropropene~ <0.0024U<0.0031U<0.0032U<0.0021U<0.0024U<0.0024U<0.0023U<0.0040U<0.0021U<0.0020U<0.0022U1,4-Dioxane (p-Dioxane)5.4 C <0.13U<0.17U<0.17U<0.11U<0.13U<0.13U<0.12U<0.21U<0.11U<0.10U<0.12UEthylbenzene6.1 C <0.0032U<0.0043U<0.0043U<0.0029U<0.0033U<0.0033U<0.0031U<0.0054U0.020<0.0027U<0.0030U2-Hexanone42 N <0.0067U<0.0088U<0.0090U<0.0059U<0.0067U<0.0068U<0.0064U<0.011U<0.0060U<0.0055U<0.0062UIsopropylbenzene (Cumene)410 N <0.0024U<0.0031U<0.0032U<0.0021U<0.0024U<0.0024U<0.0023U<0.0040U<0.0021U<0.0020U<0.0022UMethyl acetate16,000 N <0.012U<0.016U<0.016U<0.011U<0.012U<0.012U<0.012U<0.020U0.019<0.0099U<0.011UMethylcyclohexane~ <0.0073U<0.0096U<0.0098U<0.0064U<0.0074U<0.0075U<0.0070U<0.012U<0.0065U<0.0060U<0.0067UMethylene Chloride58 C <0.019U<0.025U<0.026U<0.017U<0.019U<0.019U<0.018U<0.032U<0.017U<0.016U<0.018U4-Methyl-2-pentanone (MIBK)7,000 N <0.0067U<0.0088U<0.0090U<0.0059U<0.0067U<0.0068U<0.0064U<0.011U<0.0060U<0.0055U<0.0062UMethyl-tert-butyl ether49 C <0.0026U<0.0034U<0.0035U0.0048 J<0.0026U0.0043 J<0.0025U<0.0044U<0.0023U<0.0021U<0.0024UNaphthalene2.1 C <0.0037U<0.0048U<0.0049U<0.0032U<0.0037U<0.0037U<0.0035U<0.0061U0.035<0.0030U<0.0034UStyrene1,200 N <0.0018U<0.0024U<0.0025U<0.0016U<0.0018U<0.0019U<0.0018U<0.0031U<0.0016U<0.0015U<0.0017U1,1,2,2-Tetrachloroethane0.64 C <0.0018U<0.0024U<0.0025U<0.0016U<0.0018U<0.0019U<0.0018U<0.0031U<0.0016U<0.0015U<0.0017UTetrachloroethene17 N <0.0022U<0.0029U<0.0029U<0.0019U<0.0022U<0.0022U<0.0021U<0.0037U<0.0020U<0.0018U<0.0020UToluene990 N <0.0020U<0.0026U<0.0026U<0.0017U0.0054 J<0.0020U<0.0019U<0.0033U0.12<0.0016U<0.0018U1,2,3-Trichlorobenzene13 N <0.0056U<0.0074U<0.0075U<0.0049U<0.0056U<0.0057U<0.0054U<0.0094U<0.0050U<0.0046U<0.0052U1,2,4-Trichlorobenzene12 N <0.0059U<0.0077U<0.0078U<0.0051U<0.0059U<0.0060U<0.0056U<0.0098U<0.0052U<0.0048U<0.0054U1,1,1-Trichloroethane1,700 N <0.0036U<0.0048U<0.0048U<0.0032U<0.0036U<0.0037U<0.0035U<0.0061U<0.0032U<0.0030U<0.0033U1,1,2-Trichloroethane0.32 N <0.0023U<0.0030U<0.0031U<0.0020U<0.0023U<0.0024U<0.0022U<0.0039U<0.0021U<0.0019U<0.0021UTrichloroethene0.87 N <0.0018U<0.0024U<0.0024U<0.0016U<0.0018U<0.0018U<0.0017U<0.0030U<0.0016U<0.0015U<0.0017UTrichlorofluoromethane4,700 N <0.0038U<0.0050U<0.0051U<0.0034U<0.0038U<0.0039U<0.0037U<0.0064U<0.0034U<0.0032U<0.0035U1,1,2-Trichlorotrifluoroethane1,400 N <0.0039U<0.0051U<0.0052U<0.0034U<0.0039U<0.0039U<0.0037U<0.0065U<0.0035U<0.0032U<0.0036UVinyl chloride0.061 C <0.0035U<0.0047U<0.0047U<0.0031U<0.0035U<0.0036U<0.0034U<0.0059U<0.0032U<0.0029U<0.0032UXylene (Total)120 N <0.0040U<0.0052U<0.0053U<0.0035U<0.0040U<0.0040U<0.0038U<0.0067U0.097<0.0033U<0.0036Um&p-Xylene120 N <0.0048U<0.0063U<0.0064U<0.0042U<0.0048U<0.0049U<0.0046U<0.0080U0.069<0.0039U<0.0044Uo-Xylene140 N <0.0031U<0.0040U<0.0041U<0.0027U<0.0031U<0.0031U<0.0030U<0.0052U0.028<0.0025U<0.0028UChromium, Hexavalent - 7196A6/7/2022MW-4 (24-28)6/8/2022MW-3 (12-16) MW-4 (0-2.5)6/8/2022 6/8/20226/8/20226/7/20226/7/2022SB-1 (0-2)MW-2 (4-8)SL-DUP-2 cMW-3 (0-2)6/8/2022Analytical Results (mg/kg)6/7/2022 6/7/2022RCRA Metals - 6020B, 7471B, 6010DMW-1 (0-4) MW-1 (12-16)SL-DUP-1 bMW-2 (0-2)6/8/2022
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 2 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling Date6/7/2022MW-4 (24-28)6/8/2022MW-3 (12-16) MW-4 (0-2.5)6/8/2022 6/8/20226/8/20226/7/20226/7/2022SB-1 (0-2)MW-2 (4-8)SL-DUP-2 cMW-3 (0-2)6/8/2022Analytical Results (mg/kg)6/7/2022 6/7/2022MW-1 (0-4) MW-1 (12-16)SL-DUP-1 bMW-2 (0-2)6/8/2022SVOCs - 8270EAcenaphthene720 N <0.14U<0.17U<0.17U<0.15U<0.15U<0.15U<0.15U<0.20U<0.13U<0.13U<0.15UAcenaphthylene~ <0.14U<0.17U<0.17U<0.15U<0.15U<0.15U<0.15U<0.20U<0.13U<0.13U<0.15UAcetophenone1,600 N <0.11U<0.13U<0.13U<0.11U<0.11U<0.11U<0.11U<0.14U<0.098U<0.098U<0.11UAnthracene3,600 N <0.13U<0.16U<0.16U<0.14U<0.14U<0.14U<0.14U<0.18U0.34 J<0.12U<0.14UAtrazine2.4 C <0.13U<0.16U<0.16U<0.13U<0.14U<0.14U<0.14U<0.18U<0.12U<0.12U<0.13UBenzaldehyde170 C <0.14U<0.16U<0.16U<0.14U<0.14U<0.14U<0.14U<0.19U<0.13U<0.13U<0.14UBenzo(a)anthracene1.1 C <0.14U<0.16U<0.16U<0.14U<0.14U<0.14U0.42 J <0.19U0.79<0.13U<0.14UBenzo(a)pyrene0.11 C <0.14U<0.17U<0.17U<0.14U<0.15U<0.15U0.37 J<0.19U0.78<0.13U<0.15UBenzo(b)fluoranthene1.1 C <0.14U<0.16U<0.16U<0.14U<0.14U<0.14U0.61<0.19U1.0<0.13U<0.14UBenzo(g,h,i)perylene~ <0.16U<0.19U<0.19U<0.16U<0.17U<0.17U0.25 J<0.22U0.54<0.15U<0.16UBenzo(k)fluoranthene11 C <0.14U<0.17U<0.17U<0.15U<0.15U<0.15U0.21 J<0.20U0.40<0.13U<0.15UBiphenyl (Diphenyl)10 N <0.098U<0.12U<0.12U<0.098U<0.10U<0.10U<0.10U<0.13U<0.090U<0.090U<0.10U4-Bromophenylphenyl ether~ <0.16U<0.19U<0.19U<0.16U<0.17U<0.17U<0.16U<0.22U<0.15U<0.15U<0.16UButylbenzylphthalate290 C <0.17U<0.21U<0.21U<0.17U<0.18U<0.18U<0.18U<0.24U<0.16U<0.16U<0.18UCaprolactam6,300 N <0.22U<0.26U<0.26U<0.22U<0.23U<0.23U<0.23U<0.30U<0.20U<0.20U<0.23UCarbazole~ <0.14U<0.17U<0.17U<0.14U<0.15U<0.15U<0.14U<0.19U0.18 J<0.13U<0.14U4-Chloro-3-methylphenol1,300 N <0.29U<0.34U<0.35U<0.29U<0.30U<0.30U<0.30U<0.40U<0.27U<0.27U<0.30U4-Chloroaniline2.7 C <0.32U<0.38U<0.39U<0.32U<0.34U<0.34U<0.33U<0.44U<0.30U<0.30U<0.33Ubis(2-Chloroethoxy)methane38 N <0.17U<0.20U<0.20U<0.17U<0.18U<0.18U<0.18U<0.23U<0.16U<0.16U<0.17Ubis(2-Chloroethyl) ether0.24 C <0.15U<0.18U<0.18U<0.16U<0.16U<0.16U<0.16U<0.21U<0.14U<0.14U<0.16U2-Chloronaphthalene960 N <0.16U<0.19U<0.19U<0.16U<0.17U<0.17U<0.17U<0.22U<0.15U<0.15U<0.17U2-Chlorophenol78 N <0.15U<0.18U<0.18U<0.16U<0.16U<0.16U<0.16U<0.21U<0.14U<0.14U<0.16U4-Chlorophenylphenyl ether~ <0.15U<0.18U<0.18U<0.15U<0.16U<0.16U<0.16U<0.21U<0.14U<0.14U<0.16UChrysene110 C <0.15U<0.18U<0.18U<0.15U<0.16U<0.16U0.41 J<0.20U0.81<0.14U<0.15UDibenz(a,h)anthracene0.11 C <0.16U<0.19U<0.19U<0.16U<0.17U<0.17U<0.16U<0.22U<0.15U<0.15U<0.16UDibenzofuran16 N <0.15U<0.18U<0.18U<0.15U<0.16U<0.16U<0.15U<0.20U<0.14U<0.14U<0.15U3,3'-Dichlorobenzidine1.2 C <0.28U<0.33U<0.33U<0.28U<0.29U<0.29U<0.29U<0.38U<0.26U<0.26U<0.28U2,4-Dichlorophenol38 N <0.16U<0.19U<0.19U<0.16U<0.17U<0.17U<0.16U<0.22U<0.15U<0.15U<0.16UDiethylphthalate10,000 N <0.15U<0.18U<0.18U<0.15U<0.16U<0.16U<0.15U<0.21U<0.14U<0.14U<0.15U2,4-Dimethylphenol250 N <0.17U<0.20U<0.20U<0.17U<0.18U<0.18U<0.18U<0.23U<0.16U<0.16U<0.17UDimethylphthalate~ <0.15U<0.18U<0.18U<0.15U<0.16U<0.16U<0.15U<0.20U<0.14U<0.14U<0.15UDi-n-butylphthalate1,300 N <0.14U<0.16U<0.17U<0.14U<0.15U<0.14U<0.14U<0.19U<0.13U<0.13U<0.14U4,6-Dinitro-2-methylphenol1 N <0.38U<0.46U<0.46U<0.39U<0.40U<0.40U<0.39U<0.52U<0.36U<0.35U<0.39U2,4-Dinitrophenol25 N <1.3U<1.5U<1.5U<1.3U<1.3U<1.3U<1.3U<1.7U<1.2U<1.2U<1.3U2,4-Dinitrotoluene1.7 C <0.16U<0.19U<0.19U<0.16U<0.17U<0.17U<0.16U<0.22U<0.15U<0.15U<0.16U2,6-Dinitrotoluene0.36 C <0.15U<0.18U<0.18U<0.15U<0.16U<0.16U<0.15U<0.21U<0.14U<0.14U<0.15UDi-n-octylphthalate130 N <0.16U<0.19U<0.19U<0.16U<0.17U<0.17U<0.17U<0.22U<0.15U<0.15U<0.17Ubis(2-Ethylhexyl)phthalate39 C <0.16U<0.19U<0.19U<0.16U<0.17U<0.17U<0.16U<0.22U<0.15U<0.15U<0.16UFluoranthene480 N <0.14U<0.17U<0.17U<0.14U<0.15U<0.15U0.69<0.19U1.8<0.13U<0.14UFluorene480 N <0.14U<0.17U<0.17U<0.15U<0.15U<0.15U<0.15U<0.20U<0.13U<0.13U<0.15UHexachloro-1,3-butadiene1.3 C <0.18U<0.21U<0.21U<0.18U<0.19U<0.19U<0.18U<0.24U<0.17U<0.16U<0.18UHexachlorobenzene0.16 N <0.16U<0.19U<0.19U<0.16U<0.17U<0.17U<0.16U<0.22U<0.15U<0.15U<0.16UHexachlorocyclopentadiene0.38 N <0.24U<0.28U<0.28U<0.24U<0.25U<0.25U<0.24U<0.32U<0.22U<0.22U<0.24UHexachloroethane1.9 C <0.16U<0.19U<0.19U<0.16U<0.16U<0.16U<0.16U<0.21U<0.15U<0.14U<0.16UIndeno(1,2,3-cd)pyrene1.1 C <0.16U<0.19U<0.19U<0.16U<0.17U<0.17U0.22 J<0.22U0.46<0.15U<0.17UIsophorone570 C <0.18U<0.22U<0.22U<0.18U<0.19U<0.19U<0.19U<0.25U<0.17U<0.17U<0.19U1-Methylnaphthalene18 C <0.145U<0.172U<0.173U<0.15U<0.15U<0.15U<0.15U<0.20U<0.134U<0.133U<0.15U2-Methylnaphthalene48 N <0.16U<0.20U<0.20U<0.17U<0.17U<0.17U<0.17U<0.22U<0.15U<0.15U<0.17U2-Methylphenol(o-Cresol)630 N <0.17U<0.20U<0.20U<0.17U<0.18U<0.18U<0.17U<0.23U<0.16U<0.16U<0.17U3&4-Methylphenol(m&p Cresol)250 N <0.17U<0.20U<0.20U<0.17U<0.17U<0.17U<0.17U<0.23U<0.15U<0.15U<0.17UNaphthalene2.1 C <0.14U<0.17U<0.17U<0.14U<0.15U<0.15U<0.14U<0.19U<0.13U<0.13U<0.14U2-Nitroaniline130 N <0.34U<0.40U<0.40U<0.34U<0.35U<0.35U<0.35U<0.46U<0.31U<0.31U<0.34U3-Nitroaniline~ <0.32U<0.38U<0.39U<0.32U<0.34U<0.34U<0.33U<0.44U<0.30U<0.30U<0.33U4-Nitroaniline27 C <0.31U<0.37U<0.37U<0.31U<0.33U<0.33U<0.32U<0.43U<0.29U<0.29U<0.32UNitrobenzene5.5 C <0.19U<0.23U<0.23U<0.19U<0.20U<0.20U<0.20U<0.26U<0.18U<0.18U<0.19U2-Nitrophenol~ <0.18U<0.21U<0.21U<0.18U<0.19U<0.19U<0.18U<0.24U<0.17U<0.16U<0.18U4-Nitrophenol~ <0.80U<0.95U<0.95U<0.80U<0.84U<0.83U<0.82U<1.1U<0.74U<0.73U<0.81UN-Nitroso-di-n-propylamine0.078 C <0.15U<0.18U<0.18U<0.16U<0.16U<0.16U<0.16U<0.21U<0.14U<0.14U<0.16UN-Nitrosodiphenylamine110 C <0.15U<0.17U<0.17U<0.15U<0.15U<0.15U<0.15U<0.20U<0.14U<0.13U<0.15U2,2'-Oxybis(1-chloropropane)630 N <0.20U<0.23U<0.23U<0.20U<0.21U<0.21U<0.20U<0.27U<0.18U<0.18U<0.20UPentachlorophenol1 C <0.40U<0.48U<0.48U<0.40U<0.42U<0.42U<0.41U<0.55U<0.37U<0.37U<0.41UPhenanthrene~ <0.13U<0.16U<0.16U<0.14U<0.14U<0.14U0.18 J<0.18U1.4<0.12U<0.14UPhenol3,800 N <0.18U<0.22U<0.22U<0.18U<0.19U<0.19U<0.19U<0.25U<0.17U<0.17U<0.19UPyrene360 N <0.17U<0.20U<0.20U<0.17U<0.18U<0.18U0.61<0.23U1.5<0.15U<0.17U1,2,4,5-Tetrachlorobenzene0.47 N <0.10U<0.12U<0.12U<0.10U<0.11U<0.11U<0.10U<0.14U<0.093U<0.092U<0.10U2,3,4,6-Tetrachlorophenol380 N <0.10U<0.12U<0.12U<0.10U<0.11U<0.11U<0.11U<0.14U<0.096U<0.095U<0.11U2,4,5-Trichlorophenol1,300 N <0.19U<0.22U<0.22U<0.19U<0.20U<0.20U<0.19U<0.26U<0.17U<0.17U<0.19U2,4,6-Trichlorophenol13 N <0.17U<0.20U<0.20U<0.17U<0.18U<0.18U<0.17U<0.23U<0.16U<0.16U<0.17U
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 3 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling Date6/7/2022MW-4 (24-28)6/8/2022MW-3 (12-16) MW-4 (0-2.5)6/8/2022 6/8/20226/8/20226/7/20226/7/2022SB-1 (0-2)MW-2 (4-8)SL-DUP-2 cMW-3 (0-2)6/8/2022Analytical Results (mg/kg)6/7/2022 6/7/2022MW-1 (0-4) MW-1 (12-16)SL-DUP-1 bMW-2 (0-2)6/8/2022PCBs - 8082APCB-1016 (Aroclor 1016)0.82 N -- -- -- -- -- -- -- -- -- -- --PCB-1221 (Aroclor 1221)0.2 C -- -- -- -- -- -- -- -- -- -- --PCB-1232 (Aroclor 1232)0.18 C -- -- -- -- -- -- -- -- -- -- --PCB-1242 (Aroclor 1242)0.23 C -- -- -- -- -- -- -- -- -- -- --PCB-1248 (Aroclor 1248)0.23 C -- -- -- -- -- -- -- -- -- -- --PCB-1254 (Aroclor 1254)0.23 N -- -- -- -- -- -- -- -- -- -- --PCB-1260 (Aroclor 1260)0.24 C -- -- -- -- -- -- -- -- -- -- --
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 4 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DateArsenic0.68 CBarium3,100 NCadmium1.4 NChromium, Total23,000 N gLead400Mercury2.3 NSelenium78 NSilver78 NChromium, Hexavalent0.31 CVOCs - 8260DAcetone14,000 NBenzene1.2 CBromochloromethane32 NBromodichloromethane0.31 CBromoform20 CBromomethane1.4 N2-Butanone (MEK)5,500 NCarbon disulfide160 NCarbon tetrachloride0.69 CChlorobenzene58 NChloroethane1,100 NChloroform0.34 CChloromethane23 NCyclohexane1,400 N1,2-Dibromo-3-chloropropane0.0056 CDibromochloromethane8.3 C1,2-Dibromoethane (EDB)0.038 C1,2-Dichlorobenzene380 N1,3-Dichlorobenzene~1,4-Dichlorobenzene2.8 CDichlorodifluoromethane18 N1,1-Dichloroethane3.8 C1,2-Dichloroethane0.49 C1,1-Dichloroethene48 Ncis-1,2-Dichloroethene13 Ntrans-1,2-Dichloroethene15 N1,2-Dichloropropane2.6 Ccis-1,3-Dichloropropene~trans-1,3-Dichloropropene~1,4-Dioxane (p-Dioxane)5.4 CEthylbenzene6.1 C2-Hexanone42 NIsopropylbenzene (Cumene)410 NMethyl acetate16,000 NMethylcyclohexane~Methylene Chloride58 C4-Methyl-2-pentanone (MIBK)7,000 NMethyl-tert-butyl ether49 CNaphthalene2.1 CStyrene1,200 N1,1,2,2-Tetrachloroethane0.64 CTetrachloroethene17 NToluene990 N1,2,3-Trichlorobenzene13 N1,2,4-Trichlorobenzene12 N1,1,1-Trichloroethane1,700 N1,1,2-Trichloroethane0.32 NTrichloroethene0.87 NTrichlorofluoromethane4,700 N1,1,2-Trichlorotrifluoroethane1,400 NVinyl chloride0.061 CXylene (Total)120 Nm&p-Xylene120 No-Xylene140 NChromium, Hexavalent - 7196ARCRA Metals - 6020B, 7471B, 6010D1.4 1.5 2.0 3.2 3.1 1.8 2.1 1.8 2.6 1.3<1.0U192 50.3 9.2 42.1 10.8 16.8 16.3 16.3 11.9 8.5 91.80.055 J 0.97<0.042U0.076 J<0.039U<0.043U<0.041U<0.043U<0.043U<0.041U<0.23U4.5 28.1 27.8 28.8 33.8 29.9 36.2 32.7 36.1 21.1 5.45.3 24.0 4.8 17.1 7.4 6.4 7.7 9.3 7.1 5.6 6.0<0.011U0.038 0.061 0.059 0.042 0.046 0.041 0.037 0.038 0.032 0.013 J0.30 J 0.85 J<0.41U0.54 J 0.79 0.79 J<0.40U<0.42U0.74 J 0.55 J<2.2U<0.20U<0.040U<0.043U<0.17U<0.18U<0.044U<0.042U<0.044U<0.045U<0.042U<0.24U<3.8U<28.4U<3.5U<3.9U<3.9U<5.2U<3.2U<3.6U<3.7U<3.2U<5.2U<2.5U<0.039U<0.044U<0.040U<0.044U<0.039U<0.041U<0.044U<0.041U<0.042U<0.059U<0.15U<0.0024U<0.0027U<0.0025U<0.0027U<0.0024U<0.0026U<0.0027U<0.0026U<0.0026U<0.0037U<0.11U<0.0018U<0.0020U<0.0019U<0.0020U<0.0018U<0.0019U<0.0020U<0.0019U<0.0019U<0.0027U<0.15U<0.0024U<0.0027U<0.0024U<0.0027U<0.0024U<0.0025U<0.0026U<0.0025U<0.0025U<0.0036U<0.14U<0.0022U<0.0024U<0.0022U<0.0024U<0.0021U<0.0023U<0.0024U<0.0023U<0.0023U<0.0033U<0.61U<0.0097U<0.011U<0.0099U<0.011U<0.0096U<0.010U<0.011U<0.010U<0.010U<0.015U<1.9U0.061 J 0.049 J<0.030U<0.033U0.051 J 0.040 J 0.039 J 0.041 J 0.040 J 0.051 J<0.49U<0.0077U<0.0087U<0.0079U<0.0087U<0.0076U<0.0081U<0.0086U<0.0081U<0.0081U<0.012U<0.14U<0.0023U<0.0026U<0.0023U<0.0026U<0.0023U<0.0024U<0.0025U<0.0024U<0.0024U<0.0035U<0.074U<0.0012U<0.0013U<0.0012U<0.0013U<0.0012U<0.0012U<0.0013U<0.0012U<0.0012U<0.0018U<0.30U<0.0047U<0.0053U<0.0048U<0.0053U<0.0047U<0.0050U<0.0053U<0.0050U<0.0050U<0.0071U<0.24U<0.0037U<0.0042U<0.0038U<0.0042U<0.0037U<0.0039U<0.0041U<0.0039U<0.0039U<0.0056U<0.32U<0.0051U<0.0058U<0.0053U<0.0058U<0.0051U<0.0054U<0.0057U<0.0054U<0.0054U<0.0078U<0.23U<0.0037U<0.0042U<0.0038U<0.0042U<0.0037U<0.0039U<0.0041U<0.0039U<0.0039U<0.0056U<0.15U<0.0024U<0.0027U<0.0024U<0.0027U<0.0024U<0.0025U<0.0026U<0.0025U<0.0025U<0.0036U<0.22U<0.0034U<0.0039U<0.0035U<0.0039U<0.0034U<0.0036U<0.0038U<0.0036U<0.0036U<0.0052U<0.17U<0.0027U<0.0030U<0.0028U<0.0030U<0.0027U<0.0028U<0.0030U<0.0028U<0.0029U<0.0041U<0.14U<0.0022U<0.0025U<0.0023U<0.0025U<0.0022U<0.0023U<0.0025U<0.0023U<0.0023U<0.0033U<0.12U<0.0019U<0.0021U<0.0019U<0.0021U<0.0019U<0.0020U<0.0021U<0.0020U<0.0020U<0.0029U<0.10U<0.0016U<0.0018U<0.0016U<0.0018U<0.0016U<0.0017U<0.0018U<0.0017U<0.0017U<0.0024U<0.17U<0.0027U<0.0030U<0.0027U<0.0030U<0.0026U<0.0028U<0.0030U<0.0028U<0.0028U<0.0040U<0.16U<0.0025U<0.0028U<0.0026U<0.0028U<0.0025U<0.0026U<0.0028U<0.0027U<0.0027U<0.0038U<0.26U<0.0041U<0.0046U<0.0042U<0.0046U<0.0040U<0.0043U<0.0045U<0.0043U<0.0043U<0.0061U<0.16U<0.0025U<0.0028U<0.0026U<0.0028U<0.0025U<0.0026U<0.0028U<0.0027U<0.0027U<0.0038U<0.13U<0.0021U<0.0024U<0.0021U<0.0024U<0.0021U<0.0022U<0.0023U<0.0022U<0.0022U<0.0032U<0.14U<0.0021U<0.0024U<0.0022U<0.0024U<0.0021U<0.0022U<0.0024U<0.0023U<0.0023U<0.0032U<0.12U<0.0018U<0.0021U<0.0019U<0.0021U<0.0018U<0.0019U<0.0020U<0.0019U<0.0019U<0.0028U<0.11U<0.0017U<0.0019U<0.0017U<0.0019U<0.0017U<0.0017U<0.0019U<0.0018U<0.0018U<0.0025U<0.13U<0.0021U<0.0024U<0.0022U<0.0024U<0.0021U<0.0022U<0.0023U<0.0022U<0.0022U<0.0032U<7.1U1.3 1.0<0.11U<0.13U1.0 1.1 1.2 1.2 1.1 1.2<0.18U<0.0029U<0.0032U<0.0029U<0.0032U<0.0028U<0.0030U<0.0032U<0.0030U<0.0030U<0.0043U<0.37U<0.0059U<0.0066U<0.0060U<0.0067U<0.0059U<0.0062U<0.0066U<0.0062U<0.0063U<0.0089U2.7<0.0021U<0.0023U<0.0021U<0.0023U<0.0021U<0.0022U<0.0023U<0.0022U<0.0022U<0.0031U<0.67U0.12 0.080 0.013<0.012U<0.011U0.067 0.036 0.11 0.083 0.067<0.41U<0.0064U<0.0073U<0.0066U<0.0073U<0.0064U<0.0068U<0.0072U<0.0068U<0.0068U<0.0097U<1.1U<0.017U<0.019U<0.017U<0.019U<0.017U<0.018U<0.019U<0.018U<0.018U<0.025U<0.37U<0.0059U<0.0066U<0.0060U<0.0067U<0.0059U<0.0062U<0.0066U<0.0062U<0.0063U<0.0089U0.20 J<0.0023U<0.0026U0.0040 J 0.0038 J<0.0023U<0.0024U<0.0025U<0.0024U<0.0024U<0.0035U25.6<0.0032U<0.0036U<0.0033U<0.0036U<0.0032U<0.0034U<0.0036U<0.0034U<0.0034U<0.0049U<0.10U<0.0016U<0.0018U<0.0017U<0.0018U<0.0016U<0.0017U<0.0018U<0.0017U<0.0017U<0.0024U<0.10U<0.0016U<0.0018U<0.0017U<0.0018U<0.0016U<0.0017U<0.0018U<0.0017U<0.0017U<0.0024U<0.12U<0.0019U<0.0022U<0.0020U<0.0022U<0.0019U<0.0020U<0.0022U<0.0020U<0.0020U<0.0029U0.25 J<0.0017U<0.0020U<0.0018U<0.0020U<0.0017U<0.0018U<0.0019U<0.0018U<0.0018U<0.0026U<0.31U<0.0049U<0.0056U<0.0051U<0.0056U<0.0049U<0.0052U<0.0055U<0.0052U<0.0052U<0.0075U<0.32U<0.0051U<0.0058U<0.0053U<0.0058U<0.0051U<0.0054U<0.0057U<0.0054U<0.0054U<0.0078U<0.20U<0.0032U<0.0036U<0.0033U<0.0036U<0.0032U<0.0033U<0.0035U<0.0034U<0.0034U<0.0048U<0.13U<0.0020U<0.0023U<0.0021U<0.0023U<0.0020U<0.0021U<0.0023U<0.0021U<0.0022U<0.0031U<0.10U<0.0016U<0.0018U<0.0016U<0.0018U<0.0016U<0.0017U<0.0018U<0.0017U<0.0017U<0.0024U<0.21U<0.0034U<0.0038U<0.0035U<0.0038U<0.0033U<0.0035U<0.0037U<0.0036U<0.0036U<0.0051U<0.21U<0.0034U<0.0038U<0.0035U<0.0038U<0.0034U<0.0036U<0.0038U<0.0036U<0.0036U<0.0051U<0.20U<0.0031U<0.0035U<0.0032U<0.0035U<0.0031U<0.0033U<0.0035U<0.0033U<0.0033U<0.0047U12.9<0.0035U<0.0039U<0.0036U<0.0039U<0.0035U<0.0037U<0.0039U<0.0037U<0.0037U<0.0053U7.6<0.0042U<0.0047U<0.0043U<0.0047U<0.0042U<0.0044U<0.0047U<0.0044U<0.0044U<0.0063U5.3<0.0027U<0.0030U<0.0028U<0.0031U<0.0027U<0.0028U<0.0030U<0.0029U<0.0029U<0.0041UTMW-5 (4-6)6/8/2022 6/9/20226/9/20226/9/2022 6/8/2022TMW-3 (8-10)SL-DUP-3 dTMW-4 (0-2)6/9/2022TMW-2 (0-2)6/8/2022 6/9/2022TMW-4 (2-4)6/9/20226/9/20226/9/2022SB-1 (16-20)Analytical Results (mg/kg)TMW-2 (4-8) TMW-3 (0-2)TMW-1 (0-2) TMW-1 (4-6)
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 5 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DateSVOCs - 8270EAcenaphthene720 NAcenaphthylene~Acetophenone1,600 NAnthracene3,600 NAtrazine2.4 CBenzaldehyde170 CBenzo(a)anthracene1.1 CBenzo(a)pyrene0.11 CBenzo(b)fluoranthene1.1 CBenzo(g,h,i)perylene~Benzo(k)fluoranthene11 CBiphenyl (Diphenyl)10 N4-Bromophenylphenyl ether~Butylbenzylphthalate290 CCaprolactam6,300 NCarbazole~4-Chloro-3-methylphenol1,300 N4-Chloroaniline2.7 Cbis(2-Chloroethoxy)methane38 Nbis(2-Chloroethyl) ether0.24 C2-Chloronaphthalene960 N2-Chlorophenol78 N4-Chlorophenylphenyl ether~Chrysene110 CDibenz(a,h)anthracene0.11 CDibenzofuran16 N3,3'-Dichlorobenzidine1.2 C2,4-Dichlorophenol38 NDiethylphthalate10,000 N2,4-Dimethylphenol250 NDimethylphthalate~Di-n-butylphthalate1,300 N4,6-Dinitro-2-methylphenol1 N2,4-Dinitrophenol25 N2,4-Dinitrotoluene1.7 C2,6-Dinitrotoluene0.36 CDi-n-octylphthalate130 Nbis(2-Ethylhexyl)phthalate39 CFluoranthene480 NFluorene480 NHexachloro-1,3-butadiene1.3 CHexachlorobenzene0.16 NHexachlorocyclopentadiene0.38 NHexachloroethane1.9 CIndeno(1,2,3-cd)pyrene1.1 CIsophorone570 C1-Methylnaphthalene18 C2-Methylnaphthalene48 N2-Methylphenol(o-Cresol)630 N3&4-Methylphenol(m&p Cresol)250 NNaphthalene2.1 C2-Nitroaniline130 N3-Nitroaniline~4-Nitroaniline27 CNitrobenzene5.5 C2-Nitrophenol~4-Nitrophenol~N-Nitroso-di-n-propylamine0.078 CN-Nitrosodiphenylamine110 C2,2'-Oxybis(1-chloropropane)630 NPentachlorophenol1 CPhenanthrene~Phenol3,800 NPyrene360 N1,2,4,5-Tetrachlorobenzene0.47 N2,3,4,6-Tetrachlorophenol380 N2,4,5-Trichlorophenol1,300 N2,4,6-Trichlorophenol13 NTMW-5 (4-6)6/8/2022 6/9/20226/9/20226/9/2022 6/8/2022TMW-3 (8-10)SL-DUP-3 dTMW-4 (0-2)6/9/2022TMW-2 (0-2)6/8/2022 6/9/2022TMW-4 (2-4)6/9/20226/9/20226/9/2022SB-1 (16-20)Analytical Results (mg/kg)TMW-2 (4-8) TMW-3 (0-2)TMW-1 (0-2) TMW-1 (4-6)<1.6U<0.14U<0.15U<1.4U<0.15U<0.15U<0.15U<0.15U<0.15U<0.15U<0.17U<1.6U<0.14U<0.15U<1.4U<0.15U<0.15U<0.15U<0.15U<0.15U<0.15U<0.17U<1.2U<0.10U<0.11U<1.0U<0.11U<0.11U<0.11U<0.11U<0.11U<0.11U<0.12U<1.5U0.15 J<0.14U4.7<0.14U<0.14U<0.14U<0.14U<0.14U<0.14U<0.16U<1.5U<0.13U<0.14U<1.3U<0.14U<0.13U<0.14U<0.14U<0.14U<0.14U<0.16U<1.5U<0.13U<0.14U<1.3U<0.14U<0.14U<0.14U<0.14U<0.14U<0.14U<0.16U<1.5U0.60<0.14U18.5<0.14U0.16 J<0.14U<0.14U<0.14U<0.14U<0.16U<1.6U0.46<0.15U12.9<0.15U<0.14U<0.15U<0.15U<0.15U<0.15U<0.17U<1.5U0.68<0.14U18.4<0.14U0.18 J<0.14U<0.14U<0.14U<0.14U<0.16U<1.8U0.33 J<0.17U8.2<0.17U<0.16U<0.17U<0.16U<0.17U<0.16U<0.19U<1.6U0.26 J<0.15U6.3<0.15U<0.15U<0.15U<0.15U<0.15U<0.15U<0.17U3.9 J<0.093U<0.10U<0.96U<0.10U<0.098U<0.10U<0.10U<0.10U<0.10U<0.11U<1.7U<0.15U<0.17U<1.6U<0.17U<0.16U<0.16U<0.16U<0.16U<0.16U<0.19U<1.9U<0.17U<0.18U<1.7U<0.18U<0.17U<0.18U<0.18U<0.18U<0.18U<0.20U<2.4U<0.21U<0.23U<2.2U<0.23U<0.22U<0.23U<0.23U<0.23U<0.23U<0.26U<1.5U<0.13U<0.15U1.5 J<0.15U<0.14U<0.15U<0.14U<0.15U<0.14U<0.17U<3.2U<0.28U<0.30U<2.8U<0.30U<0.29U<0.30U<0.30U<0.30U<0.30U<0.34U<3.6U<0.31U<0.34U<3.2U<0.34U<0.32U<0.33U<0.33U<0.33U<0.33U<0.38U<1.9U<0.16U<0.18U<1.7U<0.18U<0.17U<0.18U<0.18U<0.18U<0.18U<0.20U<1.7U<0.15U<0.16U<1.5U<0.16U<0.16U<0.16U<0.16U<0.16U<0.16U<0.18U<1.8U<0.16U<0.17U<1.6U<0.17U<0.16U<0.17U<0.17U<0.17U<0.17U<0.19U<1.7U<0.15U<0.16U<1.5U<0.16U<0.16U<0.16U<0.16U<0.16U<0.16U<0.18U<1.7U<0.15U<0.16U<1.5U<0.16U<0.15U<0.16U<0.16U<0.16U<0.16U<0.18U<1.6U0.64<0.16U18.6<0.16U0.17 J<0.15U<0.15U<0.16U<0.15U<0.18U<1.7U<0.15U<0.17U<1.6U<0.17U<0.16U<0.16U<0.16U<0.16U<0.16U<0.19U2.1 J<0.14U<0.15U<1.5U<0.16U<0.15U<0.15U<0.15U<0.15U<0.15U<0.17U<3.1U<0.26U<0.29U<2.7U<0.29U<0.28U<0.29U<0.29U<0.29U<0.29U<0.33U<1.8U<0.15U<0.17U<1.6U<0.17U<0.16U<0.17U<0.17U<0.17U<0.17U<0.19U<1.7U<0.14U<0.16U<1.5U<0.16U<0.15U<0.16U<0.16U<0.16U<0.15U<0.18U<1.9U<0.16U<0.18U<1.7U<0.18U<0.17U<0.18U<0.18U<0.18U<0.18U<0.20U<1.6U<0.14U<0.16U<1.5U<0.16U<0.15U<0.15U<0.15U<0.16U<0.15U<0.18U<1.5U<0.13U<0.14U<1.4U<0.15U<0.14U<0.14U<0.14U<0.14U<0.14U<0.16U<4.2U<0.37U<0.40U<3.8U<0.40U<0.39U<0.40U<0.39U<0.40U<0.39U<0.45U<14.0U<1.2U<1.3U<12.5U<1.3U<1.3U<1.3U<1.3U<1.3U<1.3U<1.5U<1.7U<0.15U<0.17U<1.6U<0.17U<0.16U<0.16U<0.16U<0.16U<0.16U<0.19U<1.7U<0.14U<0.16U<1.5U<0.16U<0.15U<0.16U<0.16U<0.16U<0.15U<0.18U<1.8U<0.15U<0.17U<1.6U<0.17U<0.16U<0.17U<0.17U<0.17U<0.17U<0.19U<1.8U<0.15U<0.17U<1.6U<0.17U<0.16U<0.17U<0.16U<0.17U<0.16U<0.19U<1.5U1.4<0.15U39.3<0.15U0.29 J<0.15U<0.14U<0.15U<0.14U<0.17U<1.6U<0.14U<0.15U<1.4U<0.15U<0.15U<0.15U<0.15U<0.15U<0.15U<0.17U<2.0U<0.17U<0.19U<1.7U<0.19U<0.18U<0.18U<0.18U<0.18U<0.18U<0.21U<1.8U<0.15U<0.17U<1.6U<0.17U<0.16U<0.17U<0.17U<0.17U<0.17U<0.19U<2.6U<0.22U<0.25U<2.3U<0.25U<0.24U<0.24U<0.24U<0.24U<0.24U<0.28U<1.7U<0.15U<0.16U<1.5U<0.17U<0.16U<0.16U<0.16U<0.16U<0.16U<0.18U<1.8U0.30 J<0.17U7.7<0.17U<0.16U<0.17U<0.17U<0.17U<0.17U<0.19U<2.0U<0.17U<0.19U<1.8U<0.19U<0.18U<0.19U<0.19U<0.19U<0.19U<0.22U19.1<0.138U<0.151U<1.4U<0.15U<0.145U<0.150U<0.149U<0.150U<0.148U<0.170U27.4<0.16U<0.17U<1.6U<0.17U<0.17U<0.17U<0.17U<0.17U<0.17U<0.19U<1.9U<0.16U<0.18U<1.7U<0.18U<0.17U<0.17U<0.17U<0.17U<0.17U<0.20U<1.8U<0.16U<0.17U<1.6U<0.17U<0.17U<0.17U<0.17U<0.17U<0.17U<0.19U10.6<0.13U<0.15U<1.4U<0.15U<0.14U<0.14U<0.14U<0.14U<0.14U<0.16U<3.7U<0.32U<0.35U<3.3U<0.35U<0.34U<0.35U<0.35U<0.35U<0.35U<0.40U<3.6U<0.31U<0.34U<3.2U<0.34U<0.32U<0.33U<0.33U<0.33U<0.33U<0.38U<3.4U<0.30U<0.33U<3.1U<0.33U<0.31U<0.32U<0.32U<0.32U<0.32U<0.37U<2.1U<0.18U<0.20U<1.9U<0.20U<0.19U<0.20U<0.20U<0.20U<0.20U<0.22U<2.0U<0.17U<0.19U<1.7U<0.19U<0.18U<0.18U<0.18U<0.18U<0.18U<0.21U<8.8U<0.76U<0.83U<7.8U<0.84U<0.80U<0.82U<0.82U<0.82U<0.82U<0.93U<1.7U<0.15U<0.16U<1.5U<0.16U<0.16U<0.16U<0.16U<0.16U<0.16U<0.18U<1.6U<0.14U<0.15U<1.4U<0.15U<0.15U<0.15U<0.15U<0.15U<0.15U<0.17U<2.2U<0.19U<0.20U<1.9U<0.21U<0.20U<0.20U<0.20U<0.20U<0.20U<0.23U<4.4U<0.38U<0.42U<4.0U<0.42U<0.40U<0.42U<0.41U<0.42U<0.41U<0.47U2.6 J 0.90<0.14U21.6<0.14U<0.14U<0.14U<0.14U<0.14U<0.14U<0.16U<2.0U<0.17U<0.19U<1.8U<0.19U<0.18U<0.19U<0.19U<0.19U<0.19U<0.22U<1.8U1.1<0.17U31.0<0.18U0.22 J<0.17U<0.17U<0.17U<0.17U<0.20U<1.1U<0.095U<0.10U<0.98U<0.11U<0.10U<0.10U<0.10U<0.10U<0.10U<0.12U<1.1U<0.098U<0.11U<1.0U<0.11U<0.10U<0.11U<0.11U<0.11U<0.11U<0.12U<2.1U<0.18U<0.20U<1.8U<0.20U<0.19U<0.19U<0.19U<0.20U<0.19U<0.22U<1.9U<0.16U<0.18U<1.7U<0.18U<0.17U<0.18U<0.17U<0.18U<0.17U<0.20U
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 6 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DatePCBs - 8082APCB-1016 (Aroclor 1016)0.82 NPCB-1221 (Aroclor 1221)0.2 CPCB-1232 (Aroclor 1232)0.18 CPCB-1242 (Aroclor 1242)0.23 CPCB-1248 (Aroclor 1248)0.23 CPCB-1254 (Aroclor 1254)0.23 NPCB-1260 (Aroclor 1260)0.24 CTMW-5 (4-6)6/8/2022 6/9/20226/9/20226/9/2022 6/8/2022TMW-3 (8-10)SL-DUP-3 dTMW-4 (0-2)6/9/2022TMW-2 (0-2)6/8/2022 6/9/2022TMW-4 (2-4)6/9/20226/9/20226/9/2022SB-1 (16-20)Analytical Results (mg/kg)TMW-2 (4-8) TMW-3 (0-2)TMW-1 (0-2) TMW-1 (4-6)-- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- --
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 7 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DateArsenic0.68 CBarium3,100 NCadmium1.4 NChromium, Total23,000 N gLead400Mercury2.3 NSelenium78 NSilver78 NChromium, Hexavalent0.31 CVOCs - 8260DAcetone14,000 NBenzene1.2 CBromochloromethane32 NBromodichloromethane0.31 CBromoform20 CBromomethane1.4 N2-Butanone (MEK)5,500 NCarbon disulfide160 NCarbon tetrachloride0.69 CChlorobenzene58 NChloroethane1,100 NChloroform0.34 CChloromethane23 NCyclohexane1,400 N1,2-Dibromo-3-chloropropane0.0056 CDibromochloromethane8.3 C1,2-Dibromoethane (EDB)0.038 C1,2-Dichlorobenzene380 N1,3-Dichlorobenzene~1,4-Dichlorobenzene2.8 CDichlorodifluoromethane18 N1,1-Dichloroethane3.8 C1,2-Dichloroethane0.49 C1,1-Dichloroethene48 Ncis-1,2-Dichloroethene13 Ntrans-1,2-Dichloroethene15 N1,2-Dichloropropane2.6 Ccis-1,3-Dichloropropene~trans-1,3-Dichloropropene~1,4-Dioxane (p-Dioxane)5.4 CEthylbenzene6.1 C2-Hexanone42 NIsopropylbenzene (Cumene)410 NMethyl acetate16,000 NMethylcyclohexane~Methylene Chloride58 C4-Methyl-2-pentanone (MIBK)7,000 NMethyl-tert-butyl ether49 CNaphthalene2.1 CStyrene1,200 N1,1,2,2-Tetrachloroethane0.64 CTetrachloroethene17 NToluene990 N1,2,3-Trichlorobenzene13 N1,2,4-Trichlorobenzene12 N1,1,1-Trichloroethane1,700 N1,1,2-Trichloroethane0.32 NTrichloroethene0.87 NTrichlorofluoromethane4,700 N1,1,2-Trichlorotrifluoroethane1,400 NVinyl chloride0.061 CXylene (Total)120 Nm&p-Xylene120 No-Xylene140 NChromium, Hexavalent - 7196ARCRA Metals - 6020B, 7471B, 6010D<2.2U2.8 0.95 3.6 1.1-- -- --3.0--83.5 20.9 46.0 53.2 111-- -- --22.2--<0.48U0.036 J<0.043U0.094 J 0.099 J-- -- -- <0.038U--1.8 J 21.0 15.5 30.3 27.0-- -- --29.0--5.5 J 5.3 3.9 26.4 9.3-- -- --8.2--<0.011U0.017 J<0.012U0.059 0.014 J-- -- --0.051--<4.7U0.33 J 0.18 J 0.65 0.23 J-- -- --0.84--<0.50U<0.16U<0.20U0.25 J<0.19U-- -- -- <0.18U--<3.9U<4.6U<3.0U<5.3U<5.8U<4.3U--<0.059U<0.038U<0.065U<0.045U<0.061U-- -- -- <0.039U--<0.0037U<0.0023U<0.0040U<0.0028U<0.0038U-- -- -- <0.0024U--<0.0027U<0.0017U<0.0030U<0.0021U<0.0028U-- -- -- <0.0018U--<0.0036U<0.0023U<0.0039U<0.0027U<0.0036U-- -- -- <0.0024U--<0.0033U<0.0021U<0.0035U<0.0024U<0.0033U-- -- -- <0.0022U--<0.015U<0.0093U<0.016U<0.011U<0.015U-- -- -- <0.0097U--0.062 J 0.028 J<0.048U<0.033U0.054 J-- -- -- <0.029U--<0.012U<0.0074U<0.013U<0.0087U<0.012U-- -- -- <0.0077U--<0.0035U<0.0022U<0.0038U<0.0026U<0.0035U-- -- -- <0.0023U--<0.0018U<0.0011U<0.0019U<0.0013U<0.0018U-- -- -- <0.0012U--<0.0071U<0.0045U<0.0078U<0.0054U<0.0073U-- -- -- <0.0047U--<0.0056U<0.0036U<0.0061U<0.0042U<0.0057U-- -- -- <0.0037U--<0.0078U<0.0049U<0.0085U<0.0058U<0.0079U-- -- -- <0.0052U--<0.0056U<0.0035U<0.0061U<0.0042U<0.0057U-- -- -- <0.0037U--<0.0036U<0.0023U<0.0039U<0.0027U<0.0037U-- -- -- <0.0024U--<0.0052U<0.0033U<0.0057U<0.0039U<0.0053U-- -- -- <0.0035U--<0.0041U<0.0026U<0.0044U<0.0031U<0.0042U-- -- -- <0.0027U--<0.0033U<0.0021U<0.0036U<0.0025U<0.0034U-- -- -- <0.0022U--<0.0029U<0.0018U<0.0031U<0.0022U<0.0029U-- -- -- <0.0019U--<0.0024U<0.0015U<0.0026U<0.0018U<0.0025U-- -- -- <0.0016U--<0.0040U<0.0026U<0.0044U<0.0030U<0.0041U-- -- -- <0.0027U--<0.0038U<0.0024U<0.0041U<0.0029U<0.0039U-- -- -- <0.0025U--<0.0061U<0.0039U<0.0067U<0.0046U<0.0063U-- -- -- <0.0041U--<0.0038U<0.0024U<0.0041U<0.0029U<0.0039U-- -- -- <0.0025U--<0.0032U<0.0020U<0.0034U<0.0024U<0.0032U-- -- -- <0.0021U--<0.0032U<0.0021U<0.0035U<0.0024U<0.0033U-- -- -- <0.0021U--<0.0028U<0.0018U<0.0030U<0.0021U<0.0028U-- -- -- <0.0018U--<0.0025U<0.0016U<0.0027U<0.0019U<0.0026U-- -- -- <0.0017U--<0.0032U<0.0020U<0.0035U<0.0024U<0.0033U-- -- -- <0.0021U--1.4<0.11U<0.18U<0.13U<0.17U-- -- -- <0.11U--<0.0043U<0.0027U<0.0047U<0.0032U<0.0044U-- -- -- <0.0029U--<0.0089U<0.0057U<0.0097U<0.0067U<0.0091U-- -- -- <0.0059U--<0.0031U<0.0020U<0.0034U<0.0024U<0.0032U-- -- -- <0.0021U--0.066<0.010U<0.017U<0.012U<0.016U-- -- -- <0.011U--<0.0097U<0.0062U<0.011U<0.0073U<0.0099U-- -- -- <0.0065U--<0.025U<0.016U<0.028U<0.019U<0.026U-- -- -- <0.017U--<0.0089U<0.0057U<0.0097U<0.0067U<0.0091U-- -- -- <0.0059U--<0.0035U<0.0022U<0.0038U<0.0026U<0.0035U-- -- -- <0.0023U--<0.0049U<0.0031U<0.0053U0.023<0.0050U-- -- -- <0.0032U--<0.0024U<0.0016U<0.0027U<0.0018U<0.0025U-- -- -- <0.0016U--<0.0024U<0.0016U<0.0027U<0.0018U<0.0025U-- -- -- <0.0016U--<0.0029U<0.0019U<0.0032U<0.0022U<0.0030U-- -- -- <0.0019U--<0.0026U<0.0017U<0.0029U<0.0020U<0.0027U-- -- -- <0.0017U--<0.0075U<0.0048U<0.0081U<0.0056U<0.0076U-- -- -- <0.0050U--<0.0078U<0.0049U<0.0085U<0.0058U<0.0079U-- -- -- <0.0052U--<0.0048U<0.0031U<0.0052U<0.0036U<0.0049U-- -- -- <0.0032U--<0.0031U<0.0020U<0.0033U<0.0023U<0.0031U-- -- -- <0.0020U--<0.0024U<0.0015U<0.0026U<0.0018U<0.0024U-- -- -- <0.0016U--<0.0051U<0.0032U<0.0055U<0.0038U<0.0052U-- -- -- <0.0034U--<0.0051U<0.0033U<0.0056U<0.0039U<0.0053U-- -- -- <0.0034U--<0.0047U<0.0030U<0.0051U<0.0035U<0.0048U-- -- -- <0.0031U--<0.0053U<0.0034U<0.0057U<0.0040U<0.0054U-- -- -- <0.0035U--<0.0063U<0.0040U<0.0069U<0.0048U<0.0065U-- -- -- <0.0042U--<0.0041U<0.0026U<0.0045U<0.0031U<0.0042U-- -- -- <0.0027U--6/7/20226/8/20226/9/2022TMW-6 (8-12) TMW-7 (0-4) SSB-2 (0-2)SSB-1 (0-2) SSB-1 (2-4) SSB-3 (0-2)6/9/2022 6/8/2022SSB-4 (0-2)TMW-5 (6-8) TMW-6 (0-4)6/9/20226/7/2022 6/7/2022 6/7/2022TMW-7 (8-12)6/9/2022Analytical Results (mg/kg)
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 8 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DateSVOCs - 8270EAcenaphthene720 NAcenaphthylene~Acetophenone1,600 NAnthracene3,600 NAtrazine2.4 CBenzaldehyde170 CBenzo(a)anthracene1.1 CBenzo(a)pyrene0.11 CBenzo(b)fluoranthene1.1 CBenzo(g,h,i)perylene~Benzo(k)fluoranthene11 CBiphenyl (Diphenyl)10 N4-Bromophenylphenyl ether~Butylbenzylphthalate290 CCaprolactam6,300 NCarbazole~4-Chloro-3-methylphenol1,300 N4-Chloroaniline2.7 Cbis(2-Chloroethoxy)methane38 Nbis(2-Chloroethyl) ether0.24 C2-Chloronaphthalene960 N2-Chlorophenol78 N4-Chlorophenylphenyl ether~Chrysene110 CDibenz(a,h)anthracene0.11 CDibenzofuran16 N3,3'-Dichlorobenzidine1.2 C2,4-Dichlorophenol38 NDiethylphthalate10,000 N2,4-Dimethylphenol250 NDimethylphthalate~Di-n-butylphthalate1,300 N4,6-Dinitro-2-methylphenol1 N2,4-Dinitrophenol25 N2,4-Dinitrotoluene1.7 C2,6-Dinitrotoluene0.36 CDi-n-octylphthalate130 Nbis(2-Ethylhexyl)phthalate39 CFluoranthene480 NFluorene480 NHexachloro-1,3-butadiene1.3 CHexachlorobenzene0.16 NHexachlorocyclopentadiene0.38 NHexachloroethane1.9 CIndeno(1,2,3-cd)pyrene1.1 CIsophorone570 C1-Methylnaphthalene18 C2-Methylnaphthalene48 N2-Methylphenol(o-Cresol)630 N3&4-Methylphenol(m&p Cresol)250 NNaphthalene2.1 C2-Nitroaniline130 N3-Nitroaniline~4-Nitroaniline27 CNitrobenzene5.5 C2-Nitrophenol~4-Nitrophenol~N-Nitroso-di-n-propylamine0.078 CN-Nitrosodiphenylamine110 C2,2'-Oxybis(1-chloropropane)630 NPentachlorophenol1 CPhenanthrene~Phenol3,800 NPyrene360 N1,2,4,5-Tetrachlorobenzene0.47 N2,3,4,6-Tetrachlorophenol380 N2,4,5-Trichlorophenol1,300 N2,4,6-Trichlorophenol13 N6/7/20226/8/20226/9/2022TMW-6 (8-12) TMW-7 (0-4) SSB-2 (0-2)SSB-1 (0-2) SSB-1 (2-4) SSB-3 (0-2)6/9/2022 6/8/2022SSB-4 (0-2)TMW-5 (6-8) TMW-6 (0-4)6/9/20226/7/2022 6/7/2022 6/7/2022TMW-7 (8-12)6/9/2022Analytical Results (mg/kg)<0.18U<0.14U<0.16U<0.15U<0.15U-- -- -- <0.15U0.091<0.18U<0.14U<0.16U<0.15U<0.15U-- -- -- <0.15U0.018<0.13U<0.10U<0.12U<0.11U<0.11U-- -- -- <0.11U--<0.16U<0.13U<0.15U<0.14U<0.14U-- -- -- <0.14U0.40<0.16U<0.13U<0.15U<0.13U<0.14U-- -- -- <0.13U--<0.17U<0.13U<0.15U<0.14U<0.15U-- -- -- <0.14U--<0.17U<0.13U<0.15U<0.14U<0.15U-- -- -- <0.14U1.3<0.17U<0.14U<0.16U<0.14U<0.15U-- -- -- <0.14U1.1<0.17U<0.13U<0.15U<0.14U<0.15U-- -- -- <0.14U1.1<0.19U<0.15U<0.18U<0.16U<0.17U-- -- -- <0.16U0.32<0.18U<0.14U<0.16U<0.15U<0.15U-- -- -- <0.15U0.77<0.12U<0.094U<0.11U<0.099U<0.10U-- -- -- <0.098U--<0.19U<0.15U<0.18U<0.16U<0.17U-- -- -- <0.16U--<0.21U<0.17U<0.20U<0.18U<0.19U-- -- -- <0.17U--<0.27U<0.21U<0.25U<0.22U<0.24U-- -- -- <0.22U--<0.17U<0.14U<0.16U<0.14U<0.15U-- -- -- <0.14U--<0.35U<0.28U<0.33U<0.29U<0.31U-- -- -- <0.29U--<0.39U<0.31U<0.36U<0.33U<0.35U-- -- -- <0.32U--<0.21U<0.17U<0.19U<0.17U<0.18U-- -- -- <0.17U--<0.19U<0.15U<0.17U<0.16U<0.17U-- -- -- <0.16U--<0.20U<0.16U<0.18U<0.17U<0.18U-- -- -- <0.16U--<0.19U<0.15U<0.17U<0.16U<0.17U-- -- -- <0.16U--<0.19U<0.15U<0.17U<0.16U<0.16U-- -- -- <0.15U--<0.18U<0.14U<0.17U<0.15U<0.16U-- -- -- <0.15U0.84<0.19U<0.15U<0.18U<0.16U<0.17U-- -- -- <0.16U0.12<0.18U<0.14U<0.17U<0.15U<0.16U-- -- -- <0.15U--<0.34U<0.27U<0.31U<0.28U<0.30U-- -- -- <0.28U--<0.20U<0.16U<0.18U<0.16U<0.17U-- -- -- <0.16U--<0.18U<0.15U<0.17U<0.15U<0.16U-- -- -- <0.15U--<0.21U<0.17U<0.19U<0.17U<0.18U-- -- -- <0.17U--<0.18U<0.14U<0.17U<0.15U<0.16U-- -- -- <0.15U--<0.17U<0.13U<0.16U<0.14U<0.15U-- -- -- <0.14U--<0.47U<0.37U<0.43U<0.39U<0.41U-- -- -- <0.39U--<1.5U<1.2U<1.4U<1.3U<1.4U-- -- -- <1.3U--<0.19U<0.15U<0.18U<0.16U<0.17U-- -- -- <0.16U--<0.18U<0.15U<0.17U<0.15U<0.16U-- -- -- <0.15U--<0.20U<0.16U<0.18U<0.16U<0.17U-- -- -- <0.16U--<0.19U<0.15U<0.18U<0.16U<0.17U-- -- -- <0.16U--<0.17U<0.14U<0.16U0.16 J<0.15U-- -- -- <0.14U2.6<0.18U<0.14U<0.16U<0.15U<0.15U-- -- -- <0.15U0.11<0.22U<0.17U<0.20U<0.18U<0.19U-- -- -- <0.18U--<0.20U<0.16U<0.18U<0.16U<0.17U-- -- -- <0.16U--<0.29U<0.23U<0.27U<0.24U<0.25U-- -- -- <0.24U--<0.19U<0.15U<0.18U<0.16U<0.17U-- -- -- <0.16U--<0.20U<0.16U<0.18U<0.16U<0.17U-- -- -- <0.16U0.30<0.22U<0.18U<0.21U<0.19U<0.20U-- -- -- <0.18U--<0.176U<0.140U<0.163U<0.146U<0.155U-- -- -- <0.15U0.014<0.20U<0.16U<0.19U<0.17U<0.18U-- -- -- <0.17U0.017<0.20U<0.16U<0.19U<0.17U<0.18U-- -- -- <0.17U--<0.20U<0.16U<0.19U<0.17U<0.18U-- -- -- <0.17U--<0.17U<0.13U<0.16U<0.14U<0.15U-- -- -- <0.14U0.018<0.41U<0.33U<0.38U<0.34U<0.36U-- -- -- <0.34U--<0.39U<0.31U<0.36U<0.33U<0.35U-- -- -- <0.32U--<0.38U<0.30U<0.35U<0.32U<0.34U-- -- -- <0.31U--<0.23U<0.18U<0.22U<0.19U<0.20U-- -- -- <0.19U--<0.22U<0.17U<0.20U<0.18U<0.19U-- -- -- <0.18U--<0.97U<0.77U<0.90U<0.80U<0.85U-- -- -- <0.80U--<0.19U<0.15U<0.17U<0.16U<0.17U-- -- -- <0.16U--<0.18U<0.14U<0.16U<0.15U<0.16U-- -- -- <0.15U--<0.24U<0.19U<0.22U<0.20U<0.21U-- -- -- <0.20U--<0.49U<0.39U<0.45U<0.41U<0.43U-- -- -- <0.40U--<0.16U<0.13U<0.15U<0.14U<0.14U-- -- -- <0.14U1.8<0.22U<0.18U<0.21U<0.19U<0.20U-- -- -- <0.18U--<0.20U<0.16U<0.19U<0.17U<0.18U-- -- -- <0.17U2.0<0.12U<0.097U<0.11U<0.10U<0.11U-- -- -- <0.10U--<0.13U<0.10U<0.12U<0.10U<0.11U-- -- -- <0.10U--<0.23U<0.18U<0.21U<0.19U<0.20U-- -- -- <0.19U--<0.21U<0.16U<0.19U<0.17U<0.18U-- -- -- <0.17U--
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 9 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DatePCBs - 8082APCB-1016 (Aroclor 1016)0.82 NPCB-1221 (Aroclor 1221)0.2 CPCB-1232 (Aroclor 1232)0.18 CPCB-1242 (Aroclor 1242)0.23 CPCB-1248 (Aroclor 1248)0.23 CPCB-1254 (Aroclor 1254)0.23 NPCB-1260 (Aroclor 1260)0.24 C6/7/20226/8/20226/9/2022TMW-6 (8-12) TMW-7 (0-4) SSB-2 (0-2)SSB-1 (0-2) SSB-1 (2-4) SSB-3 (0-2)6/9/2022 6/8/2022SSB-4 (0-2)TMW-5 (6-8) TMW-6 (0-4)6/9/20226/7/2022 6/7/2022 6/7/2022TMW-7 (8-12)6/9/2022Analytical Results (mg/kg)-- -- -- -- -- <0.015U<0.016U<0.017U-- ---- -- -- -- -- <0.026U<0.027U<0.028U-- ---- -- -- -- -- <0.017U<0.018U<0.019U-- ---- -- -- -- -- <0.0092U<0.0098U<0.010U-- ---- -- -- -- -- <0.010U<0.011U<0.011U-- ---- -- -- -- -- <0.017U<0.018U<0.018U-- ---- -- -- -- -- <0.017U<0.018U<0.019U-- --
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 10 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DateArsenic0.68 CBarium3,100 NCadmium1.4 NChromium, Total23,000 N gLead400Mercury2.3 NSelenium78 NSilver78 NChromium, Hexavalent0.31 CVOCs - 8260DAcetone14,000 NBenzene1.2 CBromochloromethane32 NBromodichloromethane0.31 CBromoform20 CBromomethane1.4 N2-Butanone (MEK)5,500 NCarbon disulfide160 NCarbon tetrachloride0.69 CChlorobenzene58 NChloroethane1,100 NChloroform0.34 CChloromethane23 NCyclohexane1,400 N1,2-Dibromo-3-chloropropane0.0056 CDibromochloromethane8.3 C1,2-Dibromoethane (EDB)0.038 C1,2-Dichlorobenzene380 N1,3-Dichlorobenzene~1,4-Dichlorobenzene2.8 CDichlorodifluoromethane18 N1,1-Dichloroethane3.8 C1,2-Dichloroethane0.49 C1,1-Dichloroethene48 Ncis-1,2-Dichloroethene13 Ntrans-1,2-Dichloroethene15 N1,2-Dichloropropane2.6 Ccis-1,3-Dichloropropene~trans-1,3-Dichloropropene~1,4-Dioxane (p-Dioxane)5.4 CEthylbenzene6.1 C2-Hexanone42 NIsopropylbenzene (Cumene)410 NMethyl acetate16,000 NMethylcyclohexane~Methylene Chloride58 C4-Methyl-2-pentanone (MIBK)7,000 NMethyl-tert-butyl ether49 CNaphthalene2.1 CStyrene1,200 N1,1,2,2-Tetrachloroethane0.64 CTetrachloroethene17 NToluene990 N1,2,3-Trichlorobenzene13 N1,2,4-Trichlorobenzene12 N1,1,1-Trichloroethane1,700 N1,1,2-Trichloroethane0.32 NTrichloroethene0.87 NTrichlorofluoromethane4,700 N1,1,2-Trichlorotrifluoroethane1,400 NVinyl chloride0.061 CXylene (Total)120 Nm&p-Xylene120 No-Xylene140 NChromium, Hexavalent - 7196ARCRA Metals - 6020B, 7471B, 6010D<2.3U<2.8U<2.6U<2.4U<2.5U<2.8U<2.8U<2.8U<2.6U2.5 J<2.7U-- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- --<0.046 U <0.047 U <0.041 U <0.040 U <0.045 U <0.051 U <0.047 U <0.048 U <0.047 U<0.039 U0.079 J<0.0029 U <0.0029 U -- <0.0025 U <0.0028 U <0.0032 U <0.0029 U -- <0.0029 U <0.0024 U <0.0027 U<0.0021 U <0.0022 U <0.0019 U <0.0018 U <0.0021 U <0.0024 U <0.0022 U <0.0022U <0.0021 U <0.0018 U <0.0020 U<0.0028 U <0.0028 U <0.0025 U <0.0024 U <0.0027 U <0.0031 U <0.0028 U <0.0029U <0.0028 U <0.0023 U <0.0026 U<0.0025 U <0.0026 U <0.0023 U <0.0022 U <0.0025 U <0.0028 U <0.0026 U <0.0026U <0.0026 U <0.0021 U <0.0024 U<0.011 U <0.012 U <0.010 U <0.0099 U <0.011 U <0.013 U <0.012 U <0.012 U <0.011U <0.0096 U <0.011 U<0.035 U <0.035 U <0.031 U <0.030 U <0.034 U <0.038 U <0.035 U <0.036 U <0.035 U<0.029 U <0.032 U-- -- -- -- -- -- -- -- -- -- --<0.0027 U <0.0027 U <0.0024 U <0.0023 U <0.0026 U <0.0030 U <0.0028 U <0.0028U <0.0027 U <0.0023 U <0.0025 U<0.0014 U <0.0014 U <0.0012 U <0.0012 U <0.0013 U <0.0015 U <0.0014 U <0.0014U <0.0014 U <0.0012 U <0.0013 U<0.0056 U <0.0057 U <0.0049 U <0.0048 U <0.0054 U <0.0061 U <0.0057 U <0.0058U <0.0056 U <0.0047 U <0.0052 U<0.0044 U <0.0045 U <0.0039 U <0.0038 U <0.0043 U <0.0048 U <0.0045 U <0.0046U <0.0044 U <0.0037 U <0.0041 U<0.0061 U <0.0062 U <0.0054 U <0.0052 U <0.0059 U <0.0067 U <0.0062 U <0.0063U <0.0061 U <0.0051 U <0.0057 U-- -- -- -- -- -- -- -- -- -- --<0.0028 U <0.0029 U <0.0025 U <0.0024 U <0.0027 U <0.0031 U <0.0029 U <0.0029U <0.0028 U <0.0024 U <0.0026 U<0.0040 U <0.0041 U <0.0036 U <0.0035 U <0.0039 U <0.0045 U <0.0041 U <0.0042U <0.0041 U <0.0034 U <0.0038 U<0.0032 U <0.0032 U <0.0028 U <0.0027 U <0.0031 U <0.0035 U <0.0032 U <0.0033U <0.0032 U <0.0027 U <0.0030 U<0.0026 U <0.0026 U <0.0023 U <0.0022 U <0.0025 U <0.0029 U <0.0026 U <0.0027U <0.0026 U <0.0022 U <0.0024 U<0.0022 U <0.0023 U <0.0020 U <0.0019 U <0.0022 U <0.0025 U <0.0023 U <0.0023U <0.0023 U <0.0019 U <0.0021 U<0.0019 U <0.0019 U <0.0017 U <0.0016 U <0.0018 U <0.0021 U <0.0019 U <0.0020U <0.0019 U <0.0016 U <0.0018 U<0.0031 U <0.0032 U <0.0028 U <0.0027 U <0.0030 U <0.0035 U <0.0032 U <0.0033U <0.0032 U <0.0026 U <0.0029 U<0.0030 U <0.0030 U <0.0026 U <0.0026 U <0.0029 U <0.0033 U <0.0030 U <0.0031U <0.0030 U <0.0025 U <0.0028 U<0.0048 U <0.0049 U <0.0042 U <0.0041 U <0.0046 U <0.0053 U <0.0049 U <0.0050U <0.0048 U <0.0040 U <0.0045 U<0.0030 U <0.0030 U <0.0026 U <0.0026 U <0.0029 U <0.0033 U <0.0030 U <0.0031U <0.0030 U <0.0025 U <0.0028 U<0.0025 U <0.0025 U <0.0022 U <0.0021 U <0.0024 U <0.0027 U <0.0025 U <0.0026U <0.0025 U <0.0021 U <0.0023 U<0.0025 U <0.0026 U <0.0022 U <0.0022 U <0.0025 U <0.0028 U <0.0026 U <0.0026U <0.0025 U <0.0021 U <0.0024 U<0.0022 U <0.0022 U <0.0019 U <0.0019 U <0.0021 U <0.0024 U <0.0022 U <0.0023U <0.0022 U <0.0018 U <0.0020 U<0.0020 U <0.0020 U <0.0017 U <0.0017 U <0.0019 U <0.0022 U <0.0020 U <0.0020U <0.0020 U <0.0016 U <0.0018 U<0.0025 U <0.0025 U <0.0022 U <0.0021 U <0.0024 U <0.0027 U <0.0025 U <0.0026U <0.0025 U <0.0021 U <0.0023 U-- -- -- -- -- -- -- -- -- -- --<0.0034 U <0.0034 U <0.0029 U <0.0033 U <0.0037 U <0.0034 U <0.0034 U <0.0028U <0.0032 U<0.0069 U <0.0071 U <0.0062 U <0.0060 U <0.0068 U <0.0077 U <0.0071 U <0.0072U <0.0070 U <0.0058 U <0.0065 U<0.0024 U <0.0025 U <0.0022 U <0.0021 U <0.0024 U <0.0027 U <0.0025 U <0.0026U <0.0025 U <0.0021 U <0.0023 U-- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- --0.056<0.020 U <0.018 U <0.017 U <0.019 U <0.022 U <0.020 U <0.021 U <0.020 U <0.017 U<0.019 U<0.0069 U <0.0071 U <0.0062 U <0.0060 U <0.0068 U <0.0077 U <0.0071 U <0.0072U <0.0070 U <0.0058 U <0.0065 U<0.0027 U <0.0027 U -- <0.0023 U <0.0026 U <0.0030 U <0.0028 U <0.0027 U <0.0023 U <0.0025 U<0.0038U<0.0039U<0.0034U<0.0033U<0.0037U<0.0042U<0.0039U<0.0040U<0.0038U<0.0032U<0.0036U<0.0019 U <0.0019 U -- <0.0016 U -- -- -- -- -- -- --<0.0019 U <0.0019 U -- <0.0016 U -- -- -- -- -- -- --<0.0023U<0.0023U<0.0020U<0.0020U<0.0022U<0.0025U<0.0023U<0.0024U<0.0023U<0.0019U<0.0021U0.0071 J<0.0021 U -- <0.0018 U <0.0020 U <0.0023 U <0.0021 U <0.0021 U <0.0017 U0.0035 J<0.0058 U <0.0059 U <0.0052 U <0.0050 U <0.0057 U <0.0064 U <0.0059 U <0.0061U <0.0059 U <0.0049 U <0.0055 U<0.0061 U <0.0062 U <0.0054 U <0.0052 U <0.0059 U <0.0067 U <0.0062 U <0.0063U <0.0061 U <0.0051 U <0.0057 U<0.0037 U <0.0038 U <0.0033 U <0.0032 U <0.0036 U <0.0041 U <0.0038 U <0.0039U <0.0038 U <0.0032 U <0.0035 U<0.0024 U <0.0024 U <0.0021 U <0.0021 U <0.0023 U <0.0026 U <0.0024 U <0.0025U <0.0024 U <0.0020 U <0.0022 U<0.0019U<0.0019U<0.0017U<0.0016U<0.0018U<0.0021U<0.0019U<0.0019U<0.0019U<0.0016U<0.0017U<0.0040 U <0.0040 U <0.0035 U <0.0034 U <0.0039 U <0.0044 U <0.0040 U <0.0041U <0.0040 U <0.0033 U <0.0037 U-- -- -- -- -- -- -- -- -- -- --<0.0037 U <0.0037 U <0.0032 U <0.0032 U <0.0036 U <0.0040 U <0.0037 U <0.0038U <0.0037 U <0.0031 U <0.0034 U0.0053 J<0.0042 U -- <0.0036 U <0.0040 U <0.0045 U <0.0042 U -- <0.0041 U <0.0035 U <0.0039 U0.0053 J<0.0050 U -- <0.0043 U <0.0048 U <0.0054 U <0.0050 U -- <0.0050 U <0.0041 U <0.0046 U<0.0032 U <0.0032 U -- <0.0028 U <0.0031 U <0.0035 U <0.0033 U -- <0.0032 U <0.0027 U <0.0030 USS-4 (0-3)SS-3 (0-3)11/17/202211/17/2022SS-DUP eSS-9 (0-3) SS-10 (0-3)11/17/2022SS-8 (0-3)Analytical Results (mg/kg)11/17/2022 11/17/2022 11/17/2022 11/17/2022SS-1 (0-3)11/17/202211/17/2022 11/17/2022SS-2 (0-3) SS-7 (0-3)11/17/2022SS-5 (0-3) SS-6 (0-3)
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 11 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DateSVOCs - 8270EAcenaphthene720 NAcenaphthylene~Acetophenone1,600 NAnthracene3,600 NAtrazine2.4 CBenzaldehyde170 CBenzo(a)anthracene1.1 CBenzo(a)pyrene0.11 CBenzo(b)fluoranthene1.1 CBenzo(g,h,i)perylene~Benzo(k)fluoranthene11 CBiphenyl (Diphenyl)10 N4-Bromophenylphenyl ether~Butylbenzylphthalate290 CCaprolactam6,300 NCarbazole~4-Chloro-3-methylphenol1,300 N4-Chloroaniline2.7 Cbis(2-Chloroethoxy)methane38 Nbis(2-Chloroethyl) ether0.24 C2-Chloronaphthalene960 N2-Chlorophenol78 N4-Chlorophenylphenyl ether~Chrysene110 CDibenz(a,h)anthracene0.11 CDibenzofuran16 N3,3'-Dichlorobenzidine1.2 C2,4-Dichlorophenol38 NDiethylphthalate10,000 N2,4-Dimethylphenol250 NDimethylphthalate~Di-n-butylphthalate1,300 N4,6-Dinitro-2-methylphenol1 N2,4-Dinitrophenol25 N2,4-Dinitrotoluene1.7 C2,6-Dinitrotoluene0.36 CDi-n-octylphthalate130 Nbis(2-Ethylhexyl)phthalate39 CFluoranthene480 NFluorene480 NHexachloro-1,3-butadiene1.3 CHexachlorobenzene0.16 NHexachlorocyclopentadiene0.38 NHexachloroethane1.9 CIndeno(1,2,3-cd)pyrene1.1 CIsophorone570 C1-Methylnaphthalene18 C2-Methylnaphthalene48 N2-Methylphenol(o-Cresol)630 N3&4-Methylphenol(m&p Cresol)250 NNaphthalene2.1 C2-Nitroaniline130 N3-Nitroaniline~4-Nitroaniline27 CNitrobenzene5.5 C2-Nitrophenol~4-Nitrophenol~N-Nitroso-di-n-propylamine0.078 CN-Nitrosodiphenylamine110 C2,2'-Oxybis(1-chloropropane)630 NPentachlorophenol1 CPhenanthrene~Phenol3,800 NPyrene360 N1,2,4,5-Tetrachlorobenzene0.47 N2,3,4,6-Tetrachlorophenol380 N2,4,5-Trichlorophenol1,300 N2,4,6-Trichlorophenol13 NSS-4 (0-3)SS-3 (0-3)11/17/202211/17/2022SS-DUP eSS-9 (0-3) SS-10 (0-3)11/17/2022SS-8 (0-3)Analytical Results (mg/kg)11/17/2022 11/17/2022 11/17/2022 11/17/2022SS-1 (0-3)11/17/202211/17/2022 11/17/2022SS-2 (0-3) SS-7 (0-3)11/17/2022SS-5 (0-3) SS-6 (0-3)<0.15U<0.15U<0.15U<0.14U<0.15U<0.15U<0.15U<0.15U<0.15U0.63<0.15U<0.15U<0.15U<0.15U<0.14U<0.15U<0.15U<0.15U<0.15U<0.15U<0.14U<0.15U-- -- -- -- -- -- -- -- -- -- --<0.14U<0.14U<0.14U<0.13U<0.14U<0.14U0.34 J<0.14U<0.14U1.9<0.14U-- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- --<0.14U<0.14U<0.14U<0.14U<0.14U<0.15U2.1<0.14U<0.14U7.7<0.14U<0.15U<0.15U<0.15U<0.14U<0.15U<0.15U1.6<0.15U<0.15U5.9<0.15U0.15 J<0.14U<0.14U<0.14U<0.14U<0.15U2.6 0.17 J 0.19 J 9.3 0.22 J<0.16U<0.17U<0.16U<0.16U<0.17U<0.17U1.1<0.17U<0.17U3.5<0.16U<0.15U<0.15U<0.15U<0.14U<0.15U<0.15U0.90<0.15U<0.15U2.8<0.15U-- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- --<0.15U<0.16U<0.15U<0.15U<0.16U<0.16U2.1<0.16U<0.16U8.3 0.16 J<0.16U<0.17U<0.16U<0.16U<0.16U<0.17U0.36 J<0.17U<0.17U<0.15U<0.16U-- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- --0.20 J<0.15U<0.14U<0.14U<0.15U<0.15U3.5<0.15U0.19 J 16.6 0.27 J<0.15U<0.15U<0.15U<0.14U<0.15U<0.15U<0.15U<0.15U<0.15U0.70<0.15U-- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- --<0.17U<0.17U<0.17U<0.16U<0.17U<0.17U0.98<0.17U<0.17U3.6<0.17U-- -- -- -- -- -- -- -- -- -- --<0.15U<0.15U<0.15U<0.14U<0.15U<0.15U<0.15U<0.15U<0.15U<0.14U<0.15U<0.17U<0.17U<0.17U<0.16U<0.17U<0.18U<0.17U<0.17U<0.17U<0.16U<0.17U-- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- --<0.14U<0.15U<0.14U<0.14U<0.15U<0.15U<0.14U<0.15U<0.15U<0.13U<0.14U-- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- --0.16 J<0.14U<0.14U<0.13U<0.14U<0.14U1.5<0.14U<0.14U13.3 0.21 J-- -- -- -- -- -- -- -- -- -- --<0.17U<0.18U<0.17U<0.17U<0.17U<0.18U2.8<0.18U0.20 J 12.2 0.23 J-- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- --
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 12 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DatePCBs - 8082APCB-1016 (Aroclor 1016)0.82 NPCB-1221 (Aroclor 1221)0.2 CPCB-1232 (Aroclor 1232)0.18 CPCB-1242 (Aroclor 1242)0.23 CPCB-1248 (Aroclor 1248)0.23 CPCB-1254 (Aroclor 1254)0.23 NPCB-1260 (Aroclor 1260)0.24 CSS-4 (0-3)SS-3 (0-3)11/17/202211/17/2022SS-DUP eSS-9 (0-3) SS-10 (0-3)11/17/2022SS-8 (0-3)Analytical Results (mg/kg)11/17/2022 11/17/2022 11/17/2022 11/17/2022SS-1 (0-3)11/17/202211/17/2022 11/17/2022SS-2 (0-3) SS-7 (0-3)11/17/2022SS-5 (0-3) SS-6 (0-3)-- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- -- -- -- -- -- --
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 13 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DateArsenic0.68 CBarium3,100 NCadmium1.4 NChromium, Total23,000 N gLead400Mercury2.3 NSelenium78 NSilver78 NChromium, Hexavalent0.31 CVOCs - 8260DAcetone14,000 NBenzene1.2 CBromochloromethane32 NBromodichloromethane0.31 CBromoform20 CBromomethane1.4 N2-Butanone (MEK)5,500 NCarbon disulfide160 NCarbon tetrachloride0.69 CChlorobenzene58 NChloroethane1,100 NChloroform0.34 CChloromethane23 NCyclohexane1,400 N1,2-Dibromo-3-chloropropane0.0056 CDibromochloromethane8.3 C1,2-Dibromoethane (EDB)0.038 C1,2-Dichlorobenzene380 N1,3-Dichlorobenzene~1,4-Dichlorobenzene2.8 CDichlorodifluoromethane18 N1,1-Dichloroethane3.8 C1,2-Dichloroethane0.49 C1,1-Dichloroethene48 Ncis-1,2-Dichloroethene13 Ntrans-1,2-Dichloroethene15 N1,2-Dichloropropane2.6 Ccis-1,3-Dichloropropene~trans-1,3-Dichloropropene~1,4-Dioxane (p-Dioxane)5.4 CEthylbenzene6.1 C2-Hexanone42 NIsopropylbenzene (Cumene)410 NMethyl acetate16,000 NMethylcyclohexane~Methylene Chloride58 C4-Methyl-2-pentanone (MIBK)7,000 NMethyl-tert-butyl ether49 CNaphthalene2.1 CStyrene1,200 N1,1,2,2-Tetrachloroethane0.64 CTetrachloroethene17 NToluene990 N1,2,3-Trichlorobenzene13 N1,2,4-Trichlorobenzene12 N1,1,1-Trichloroethane1,700 N1,1,2-Trichloroethane0.32 NTrichloroethene0.87 NTrichlorofluoromethane4,700 N1,1,2-Trichlorotrifluoroethane1,400 NVinyl chloride0.061 CXylene (Total)120 Nm&p-Xylene120 No-Xylene140 NChromium, Hexavalent - 7196ARCRA Metals - 6020B, 7471B, 6010D3.29 0.883 J -- -- 0.645 J 0.467 J 3.33 1.9247.9 8.21 -- -- 67.1 84.2 53.3 32.40.115 J <0.110 U -- -- 0.153 J <0.105 U 0.294 J 0.239 J30.4 11.9 -- -- 17.0 18.6 33.2 32.715.7 4.77 -- -- 25.9 9.42 43.8 14.90.0368 J 0.0244 J -- -- 0.0507 J <0.0211 U 0.0461 J 0.05040.591 J 0.388 J -- -- <0.230 U <0.221 U 0.398 J 0.243 J<0.115 U <0.112 U -- -- 0.358 J <0.106 U 0.329 J <0.101 U0.735 J <0.329 U <0.327 U <0.342 U 0.559 J 0.414 J 0.821 J 0.417 J-- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- --8/28/2023 8/22/2023 8/22/2023 8/22/2023 8/22/2023Analytical Results (mg/kg)SS-1 (0-3) SS-2 (0-3) SS-3 (0-3) SS-5 (0-3)8/22/2023 8/22/2023SS-9 (0-3)SS-DUPfSS-7 (0-3) SS-8 (0-3)8/22/2023
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 14 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DateSVOCs - 8270EAcenaphthene720 NAcenaphthylene~Acetophenone1,600 NAnthracene3,600 NAtrazine2.4 CBenzaldehyde170 CBenzo(a)anthracene1.1 CBenzo(a)pyrene0.11 CBenzo(b)fluoranthene1.1 CBenzo(g,h,i)perylene~Benzo(k)fluoranthene11 CBiphenyl (Diphenyl)10 N4-Bromophenylphenyl ether~Butylbenzylphthalate290 CCaprolactam6,300 NCarbazole~4-Chloro-3-methylphenol1,300 N4-Chloroaniline2.7 Cbis(2-Chloroethoxy)methane38 Nbis(2-Chloroethyl) ether0.24 C2-Chloronaphthalene960 N2-Chlorophenol78 N4-Chlorophenylphenyl ether~Chrysene110 CDibenz(a,h)anthracene0.11 CDibenzofuran16 N3,3'-Dichlorobenzidine1.2 C2,4-Dichlorophenol38 NDiethylphthalate10,000 N2,4-Dimethylphenol250 NDimethylphthalate~Di-n-butylphthalate1,300 N4,6-Dinitro-2-methylphenol1 N2,4-Dinitrophenol25 N2,4-Dinitrotoluene1.7 C2,6-Dinitrotoluene0.36 CDi-n-octylphthalate130 Nbis(2-Ethylhexyl)phthalate39 CFluoranthene480 NFluorene480 NHexachloro-1,3-butadiene1.3 CHexachlorobenzene0.16 NHexachlorocyclopentadiene0.38 NHexachloroethane1.9 CIndeno(1,2,3-cd)pyrene1.1 CIsophorone570 C1-Methylnaphthalene18 C2-Methylnaphthalene48 N2-Methylphenol(o-Cresol)630 N3&4-Methylphenol(m&p Cresol)250 NNaphthalene2.1 C2-Nitroaniline130 N3-Nitroaniline~4-Nitroaniline27 CNitrobenzene5.5 C2-Nitrophenol~4-Nitrophenol~N-Nitroso-di-n-propylamine0.078 CN-Nitrosodiphenylamine110 C2,2'-Oxybis(1-chloropropane)630 NPentachlorophenol1 CPhenanthrene~Phenol3,800 NPyrene360 N1,2,4,5-Tetrachlorobenzene0.47 N2,3,4,6-Tetrachlorophenol380 N2,4,5-Trichlorophenol1,300 N2,4,6-Trichlorophenol13 N8/28/2023 8/22/2023 8/22/2023 8/22/2023 8/22/2023Analytical Results (mg/kg)SS-1 (0-3) SS-2 (0-3) SS-3 (0-3) SS-5 (0-3)8/22/2023 8/22/2023SS-9 (0-3)SS-DUPfSS-7 (0-3) SS-8 (0-3)8/22/2023-- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- --
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 15 of 16)AnalyteResidential Health PSRG (mg/kg)Sample ID aSampling DatePCBs - 8082APCB-1016 (Aroclor 1016)0.82 NPCB-1221 (Aroclor 1221)0.2 CPCB-1232 (Aroclor 1232)0.18 CPCB-1242 (Aroclor 1242)0.23 CPCB-1248 (Aroclor 1248)0.23 CPCB-1254 (Aroclor 1254)0.23 NPCB-1260 (Aroclor 1260)0.24 C8/28/2023 8/22/2023 8/22/2023 8/22/2023 8/22/2023Analytical Results (mg/kg)SS-1 (0-3) SS-2 (0-3) SS-3 (0-3) SS-5 (0-3)8/22/2023 8/22/2023SS-9 (0-3)SS-DUPfSS-7 (0-3) SS-8 (0-3)8/22/2023-- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- ---- -- -- -- -- -- -- --
Table ASoil Sample Analytical ResultsProposed Abernethy Lofts Residential Development SiteCharlotte, NC(Page 16 of 16)Shaded values (yellow) exceed the corresponding residential health PSRGs.Shaded value (green) exceeds the corresponding residential health PSRG and maximum USGS regional soil concentration for arsenic of 3.9 mg/kg.a Sample ID includes the sample depth. For example, MW-1 (12-16) indicates that the soil sample was collected from soil boring MW-1 from the 12 ft to 16 ft depth interval.b Duplicate of MW-1 (12-16).c Duplicate of MW-2 (4-8).d Duplicate of TMW-3 (8-10).e Duplicate of SS-8 (0-3).f Duplicate of SS-9 (0-3).g Chromium III value.~ - Not established for this analyte.-- - Not analyzed.C - Carcinogenic.ft - Feet.J - Result is less than the reporting limit but greater than or equal to the MDL; the concentration is an approximate value.mg/kg - Milligrams per kilogram.N - Noncarcinogenic.NCDEQ - North Carolina Department of Environmental Quality.PCB - Polychlorinated biphenyl.SVOC - Semi-volatile organic compound.USGS - United States Geologic Survey.VOC - Volatile organic compound.PSRG - Preliminary Soil Remediation Goal (NCDEQ Inactive Hazardous Sites Branch PSRG Table - January 2023). PSRGs are based on a cancer risk of 1E-06 and a non-cancer hazard quotient of 0.2.RCRA - Resource Conservation and Recovery Act.Bold values were detected above the corresponding laboratory MDL.MDL - Method detection limit.U - Analyte was not detected in the sample. The indicated concentration is the MDL.

APPENDICES

APPENDIX A

#=CL#
September 01, 2023
LIMS USE: FR - NORA ZIRPS
LIMS OBJECT ID: 92683915
92683915
Project:
Pace Project No.:
RE:
Nora Zirps
ESP Associates
7011 Albert Pick Rd.
Suite E
Greensboro, NC 27409
Proposed Abernethy Site
Dear Nora Zirps:
Enclosed are the analytical results for sample(s) received by the laboratory on August 22, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni for
[e-mail]
Project Manager
Bonnie Vang
[phone]
Enclosures
cc:Matt Craig, ESP Associates
Account Payable, ESP Associates
Chris Ward, ESP Associates
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Lab ID Sample ID Matrix Date Collected Date Received
92683915002 SS-2 Solid 08/22/23 11:40 08/22/23 13:54
92683915003 SS-3 Solid 08/22/23 09:08 08/22/23 13:54
92683915004 SS-5 Solid 08/22/23 09:33 08/22/23 13:54
92683915005 SS-7 Solid 08/22/23 10:35 08/22/23 13:54
92683915006 SS-8 Solid 08/22/23 10:13 08/22/23 13:54
92683915007 SS-9 Solid 08/22/23 11:15 08/22/23 13:54
92683915008 FIELD DUP.Solid 08/22/23 11:15 08/22/23 13:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92683915002 SS-2 EPA 6020B 7 PANSJM
EPA 7471B 1 PANNDL
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92683915003 SS-3 EPA 6020B 7 PANSJM
EPA 7471B 1 PANNDL
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92683915004 SS-5 EPA 6020B 7 PANSJM
EPA 7471B 1 PANNDL
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92683915005 SS-7 EPA 6020B 7 PANSJM
EPA 7471B 1 PANNDL
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92683915006 SS-8 EPA 6020B 7 PANSJM
EPA 7471B 1 PANNDL
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92683915007 SS-9 EPA 6020B 7 PANSJM
EPA 7471B 1 PANNDL
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92683915008 FIELD DUP.EPA 6020B 7 PANSJM
EPA 7471B 1 PANNDL
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
PAN = Pace National - Mt. Juliet
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Sample:SS-2 Lab ID:92683915002 Collected:08/22/23 11:40 Received:08/22/23 13:54 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.833J mg/kg 08/30/23 02:53 7440-38-2 J08/28/23 12:521.29 0.129 5
Barium 8.21 mg/kg 08/30/23 02:53 7440-39-308/28/23 12:523.22 0.196 5
Cadmium <0.110 mg/kg 08/30/23 02:53 7440-43-908/28/23 12:521.29 0.110 5
Chromium 11.9 mg/kg 08/30/23 02:53 7440-47-308/28/23 12:526.45 0.382 5
Lead 4.77 mg/kg 08/30/23 02:53 7439-92-108/28/23 12:522.58 0.128 5
Selenium 0.388J mg/kg 08/30/23 02:53 7782-49-2 J08/28/23 12:523.22 0.232 5
Silver <0.112 mg/kg 08/30/23 02:53 7440-22-408/28/23 12:520.645 0.112 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0244J mg/kg 08/31/23 14:16 7439-97-6 J08/30/23 13:190.0516 0.0232 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 77.6 %08/26/23 09:2708/26/23 09:151
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent <0.329 mg/kg 08/28/23 19:53 18540-29-908/25/23 17:571.29 0.329 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Sample:SS-3 Lab ID:92683915003 Collected:08/22/23 09:08 Received:08/22/23 13:54 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.926J mg/kg 08/30/23 02:57 7440-38-2 J08/28/23 12:521.28 0.128 5
Barium 52.0 mg/kg 08/30/23 02:57 7440-39-308/28/23 12:523.20 0.195 5
Cadmium <0.110 mg/kg 08/30/23 02:57 7440-43-908/28/23 12:521.28 0.110 5
Chromium 14.4 mg/kg 08/30/23 02:57 7440-47-308/28/23 12:526.41 0.379 5
Lead 10.7 mg/kg 08/30/23 02:57 7439-92-108/28/23 12:522.56 0.127 5
Selenium 0.336J mg/kg 08/30/23 02:57 7782-49-2 J08/28/23 12:523.20 0.231 5
Silver <0.111 mg/kg 08/30/23 02:57 7440-22-408/28/23 12:520.641 0.111 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury <0.0231 mg/kg 08/31/23 14:18 7439-97-608/30/23 13:190.0512 0.0231 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 78.1 %08/26/23 09:2708/26/23 09:151
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent <0.327 mg/kg 08/28/23 19:58 18540-29-908/28/23 07:051.28 0.327 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Sample:SS-5 Lab ID:92683915004 Collected:08/22/23 09:33 Received:08/22/23 13:54 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.334J mg/kg 08/30/23 03:00 7440-38-2 J08/28/23 12:521.34 0.134 5
Barium 24.0 mg/kg 08/30/23 03:00 7440-39-308/28/23 12:523.35 0.204 5
Cadmium <0.115 mg/kg 08/30/23 03:00 7440-43-908/28/23 12:521.34 0.115 5
Chromium 26.6 mg/kg 08/30/23 03:00 7440-47-308/28/23 12:526.70 0.397 5
Lead 6.24 mg/kg 08/30/23 03:00 7439-92-108/28/23 12:522.68 0.133 5
Selenium <0.241 mg/kg 08/30/23 03:00 7782-49-208/28/23 12:523.35 0.241 5
Silver <0.116 mg/kg 08/30/23 03:00 7440-22-408/28/23 12:520.670 0.116 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0405J mg/kg 08/31/23 16:18 7439-97-6 J08/30/23 13:190.0536 0.0241 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 74.6 %08/26/23 09:2708/26/23 09:151
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent <0.342 mg/kg 08/28/23 20:03 18540-29-908/28/23 07:051.34 0.342 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Sample:SS-7 Lab ID:92683915005 Collected:08/22/23 10:35 Received:08/22/23 13:54 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.645J mg/kg 08/30/23 03:10 7440-38-2 J08/28/23 12:521.28 0.128 5
Barium 67.1 mg/kg 08/30/23 03:10 7440-39-308/28/23 12:523.19 0.194 5
Cadmium 0.153J mg/kg 08/30/23 03:10 7440-43-9 J08/28/23 12:521.28 0.109 5
Chromium 17.0 mg/kg 08/30/23 03:10 7440-47-308/28/23 12:526.38 0.377 5
Lead 25.9 mg/kg 08/30/23 03:10 7439-92-108/28/23 12:522.55 0.126 5
Selenium <0.230 mg/kg 08/30/23 03:10 7782-49-208/28/23 12:523.19 0.230 5
Silver 0.358J mg/kg 08/30/23 03:10 7440-22-4 J08/28/23 12:520.638 0.110 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0507J mg/kg 08/31/23 16:27 7439-97-6 J08/30/23 13:190.0510 0.0230 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 78.4 %08/26/23 09:2708/26/23 09:151
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.559J mg/kg 08/28/23 20:13 18540-29-9 J08/28/23 07:051.28 0.325 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Sample:SS-8 Lab ID:92683915006 Collected:08/22/23 10:13 Received:08/22/23 13:54 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.467J mg/kg 08/30/23 03:14 7440-38-2 J08/28/23 12:521.23 0.123 5
Barium 84.2 mg/kg 08/30/23 03:14 7440-39-308/28/23 12:523.07 0.187 5
Cadmium <0.105 mg/kg 08/30/23 03:14 7440-43-908/28/23 12:521.23 0.105 5
Chromium 18.6 mg/kg 08/30/23 03:14 7440-47-308/28/23 12:526.15 0.364 5
Lead 9.42 mg/kg 08/30/23 03:14 7439-92-108/28/23 12:522.46 0.122 5
Selenium <0.221 mg/kg 08/30/23 03:14 7782-49-208/28/23 12:523.07 0.221 5
Silver <0.106 mg/kg 08/30/23 03:14 7440-22-408/28/23 12:520.615 0.106 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury <0.0221 mg/kg 08/31/23 16:30 7439-97-608/30/23 13:190.0492 0.0221 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 81.3 %08/26/23 09:2708/26/23 09:151
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.414J mg/kg 08/28/23 20:19 18540-29-9 J08/28/23 07:051.23 0.314 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Sample:SS-9 Lab ID:92683915007 Collected:08/22/23 11:15 Received:08/22/23 13:54 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 3.33 mg/kg 08/30/23 03:17 7440-38-208/28/23 12:521.22 0.122 5
Barium 53.3 mg/kg 08/30/23 03:17 7440-39-308/28/23 12:523.05 0.186 5
Cadmium 0.294J mg/kg 08/30/23 03:17 7440-43-9 J08/28/23 12:521.22 0.104 5
Chromium 33.2 mg/kg 08/30/23 03:17 7440-47-308/28/23 12:526.10 0.361 5
Lead 43.8 mg/kg 08/30/23 03:17 7439-92-108/28/23 12:522.44 0.121 5
Selenium 0.398J mg/kg 08/30/23 03:17 7782-49-2 J08/28/23 12:523.05 0.220 5
Silver 0.329J mg/kg 08/30/23 03:17 7440-22-4 J08/28/23 12:520.610 0.106 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0461J mg/kg 08/31/23 16:32 7439-97-6 J08/30/23 13:190.0488 0.0220 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 81.9 %08/26/23 09:2708/26/23 09:151
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.821J mg/kg 08/28/23 20:24 18540-29-9 J08/25/23 17:571.22 0.311 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Sample:FIELD DUP.Lab ID:92683915008 Collected:08/22/23 11:15 Received:08/22/23 13:54 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 1.92 mg/kg 08/30/23 03:21 7440-38-208/28/23 12:521.17 0.117 5
Barium 32.4 mg/kg 08/30/23 03:21 7440-39-308/28/23 12:522.93 0.178 5
Cadmium 0.239J mg/kg 08/30/23 03:21 7440-43-9 J08/28/23 12:521.17 0.100 5
Chromium 32.7 mg/kg 08/30/23 03:21 7440-47-308/28/23 12:525.86 0.347 5
Lead 14.9 mg/kg 08/30/23 03:21 7439-92-108/28/23 12:522.35 0.116 5
Selenium 0.243J mg/kg 08/30/23 03:21 7782-49-2 J08/28/23 12:522.93 0.211 5
Silver <0.101 mg/kg 08/30/23 03:21 7440-22-408/28/23 12:520.586 0.101 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0504 mg/kg 08/31/23 16:35 7439-97-608/30/23 13:190.0469 0.0211 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 85.3 %08/26/23 09:2708/26/23 09:151
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.417J mg/kg 08/28/23 20:29 18540-29-9 J08/25/23 17:571.17 0.299 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2121858
3051
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92683915002, 92683915003, 92683915004, 92683915005, 92683915006, 92683915007, 92683915008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3967071-1
Associated Lab Samples:92683915002, 92683915003, 92683915004, 92683915005, 92683915006, 92683915007, 92683915008
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg <0.100 1.00 08/30/23 02:300.100
Barium mg/kg <0.152 2.50 08/30/23 02:300.152
Cadmium mg/kg <0.0855 1.00 08/30/23 02:300.0855
Chromium mg/kg <0.297 5.00 08/30/23 02:300.297
Lead mg/kg <0.0990 2.00 08/30/23 02:300.0990
Selenium mg/kg <0.180 2.50 08/30/23 02:300.180
Silver mg/kg <0.0865 0.500 08/30/23 02:300.0865
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3967071-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 97.3100 97.3 80.0-120
Barium mg/kg 92.8100 92.8 80.0-120
Cadmium mg/kg 98.6100 98.6 80.0-120
Chromium mg/kg 98.2100 98.2 80.0-120
Lead mg/kg 94.4100 94.4 80.0-120
Selenium mg/kg 102100 102 80.0-120
Silver mg/kg 21.120.0 105 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3967071-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1649973-10
R3967071-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 100 89.6 75.0-12591.3 1.83 201001.97 91.5 93.2
Barium mg/kg 100 114 75.0-125107 3.08 2010096.0 210 203
Cadmium mg/kg 100 91.3 75.0-12594.4 3.29 20100ND91.3 94.4
Chromium mg/kg 100 89.0 75.0-12590.0 0.983 201005.95 95.0 95.9
Lead mg/kg 100 90.4 75.0-12591.5 1.20 201003.00 93.4 94.5
Selenium mg/kg 100 94.7 75.0-12595.0 0.334 20100ND94.7 95.0
Silver mg/kg 20.0 97.9 75.0-12598.0 0.126 2020.0ND 19.6 19.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2122917
7471A
EPA 7471B
Mercury 7471B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92683915002, 92683915003, 92683915004, 92683915005, 92683915006, 92683915007, 92683915008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3968027-1
Associated Lab Samples:92683915002, 92683915003, 92683915004, 92683915005, 92683915006, 92683915007, 92683915008
Matrix:Solid
AnalyzedMDL
Mercury mg/kg <0.0180 0.0400 08/31/23 14:010.0180
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3968027-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.4380.500 87.6 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3968027-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1649385-10
R3968027-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.597 85.7 75.0-12578.3 9.11 200.597ND 0.512 0.467
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2121433
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92683915002, 92683915003, 92683915004, 92683915005, 92683915006, 92683915007, 92683915008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3966066-1
Associated Lab Samples:92683915002, 92683915003, 92683915004, 92683915005, 92683915006, 92683915007, 92683915008
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 08/26/23 09:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3966066-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683915002
R3966066-3SAMPLE DUPLICATE:
Total Solids %77.8 0.263 1077.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2121342
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92683915002, 92683915003, 92683915004, 92683915005, 92683915006, 92683915007, 92683915008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3966439-1
Associated Lab Samples:92683915002, 92683915003, 92683915004, 92683915005, 92683915006, 92683915007, 92683915008
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg <0.255 1.00 08/28/23 17:460.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3966439-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.910.0 109 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3966439-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1649004-01
R3966439-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 20.0 102 75.0-125106 3.91 2020.00.286 20.6 21.4
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3966439-5MATRIX SPIKE SAMPLE:
MSSpike
Result
L1649004-01
Chromium, Hexavalent mg/kg 613643 95.4 75.0-1250.286
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1649004-03
R3966439-7SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg <0.255 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683915004
R3966439-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg <0.342 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92683915
Proposed Abernethy Site
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92683915002 2121858 2121858SS-2 3051 EPA 6020B
92683915003 2121858 2121858SS-3 3051 EPA 6020B
92683915004 2121858 2121858SS-5 3051 EPA 6020B
92683915005 2121858 2121858SS-7 3051 EPA 6020B
92683915006 2121858 2121858SS-8 3051 EPA 6020B
92683915007 2121858 2121858SS-9 3051 EPA 6020B
92683915008 2121858 2121858FIELD DUP.3051 EPA 6020B
92683915002 2122917 2122917SS-2 7471A EPA 7471B
92683915003 2122917 2122917SS-3 7471A EPA 7471B
92683915004 2122917 2122917SS-5 7471A EPA 7471B
92683915005 2122917 2122917SS-7 7471A EPA 7471B
92683915006 2122917 2122917SS-8 7471A EPA 7471B
92683915007 2122917 2122917SS-9 7471A EPA 7471B
92683915008 2122917 2122917FIELD DUP.7471A EPA 7471B
92683915002 2121433 2121433SS-2 SM 2540 G SM 2540G
92683915003 2121433 2121433SS-3 SM 2540 G SM 2540G
92683915004 2121433 2121433SS-5 SM 2540 G SM 2540G
92683915005 2121433 2121433SS-7 SM 2540 G SM 2540G
92683915006 2121433 2121433SS-8 SM 2540 G SM 2540G
92683915007 2121433 2121433SS-9 SM 2540 G SM 2540G
92683915008 2121433 2121433FIELD DUP.SM 2540 G SM 2540G
92683915002 2121342 2121342SS-2 3060A EPA 7199
92683915003 2121342 2121342SS-3 3060A EPA 7199
92683915004 2121342 2121342SS-5 3060A EPA 7199
92683915005 2121342 2121342SS-7 3060A EPA 7199
92683915006 2121342 2121342SS-8 3060A EPA 7199
92683915007 2121342 2121342SS-9 3060A EPA 7199
92683915008 2121342 2121342FIELD DUP.3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/01/2023 07:11 PM
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Huntersville, NC 28078
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Page 17 of 19
Page 18 of 19
Page 19 of 19
#=CL#
September 07, 2023
LIMS USE: FR - NORA ZIRPS
LIMS OBJECT ID: 92684831
92684831
Project:
Pace Project No.:
RE:
Nora Zirps
ESP Associates
7011 Albert Pick Rd.
Suite E
Greensboro, NC 27409
Proposed Abernethy Site
Dear Nora Zirps:
Enclosed are the analytical results for sample(s) received by the laboratory on August 28, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
cc:Matt Craig, ESP Associates
Account Payable, ESP Associates
Chris Ward, ESP Associates
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 13
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92684831
Proposed Abernethy Site
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 13
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92684831
Proposed Abernethy Site
Lab ID Sample ID Matrix Date Collected Date Received
92684831001 SS-1 Solid 08/28/23 10:06 08/28/23 10:55
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 13
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92684831
Proposed Abernethy Site
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92684831001 SS-1 EPA 6020B 7 PANJPD
EPA 7471B 1 PANAKB
SM 2540G 1 PANKDW
EPA 7199 1 PANVSS
PAN = Pace National - Mt. Juliet
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92684831
Proposed Abernethy Site
Sample:SS-1 Lab ID:92684831001 Collected:08/28/23 10:06 Received:08/28/23 10:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 3.29 mg/kg 09/01/23 11:37 7440-38-209/01/23 08:181.33 0.133 5
Barium 47.9 mg/kg 09/01/23 11:37 7440-39-309/01/23 08:183.34 0.203 5
Cadmium 0.115J mg/kg 09/01/23 11:37 7440-43-9 J09/01/23 08:181.33 0.114 5
Chromium 30.4 mg/kg 09/01/23 11:37 7440-47-309/01/23 08:186.67 0.395 5
Lead 15.7 mg/kg 09/01/23 11:37 7439-92-109/01/23 08:182.67 0.132 5
Selenium 0.591J mg/kg 09/01/23 11:37 7782-49-2 J09/01/23 08:183.34 0.240 5
Silver ND mg/kg 09/01/23 11:37 7440-22-409/01/23 08:180.667 0.115 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0368J mg/kg 09/06/23 16:28 7439-97-6 J09/05/23 13:190.0534 0.0240 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 74.9 %09/01/23 10:4109/01/23 10:221
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.735J mg/kg 09/04/23 04:55 18540-29-9 J09/01/23 08:381.33 0.340 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/07/2023 09:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92684831
Proposed Abernethy Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2124812
3051
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92684831001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3968269-1
Associated Lab Samples:92684831001
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 1.00 09/01/23 10:540.100
Barium mg/kg ND 2.50 09/01/23 10:540.152
Cadmium mg/kg ND 1.00 09/01/23 10:540.0855
Chromium mg/kg ND 5.00 09/01/23 10:540.297
Lead mg/kg ND 2.00 09/01/23 10:540.0990
Selenium mg/kg ND 2.50 09/01/23 10:540.180
Silver mg/kg ND 0.500 09/01/23 10:540.0865
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3968269-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 94.0100 94.0 80.0-120
Barium mg/kg 90.8100 90.8 80.0-120
Cadmium mg/kg 94.6100 94.6 80.0-120
Chromium mg/kg 92.7100 92.7 80.0-120
Lead mg/kg 92.0100 92.0 80.0-120
Selenium mg/kg 97.3100 97.3 80.0-120
Silver mg/kg 18.420.0 91.9 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3968269-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1651252-04
R3968269-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 107 81.4 75.0-12578.1 3.98 201074.28 91.7 88.1
Barium mg/kg 107 82.9 75.0-12579.8 1.64 20107118207204
Cadmium mg/kg 107 86.2 75.0-12582.9 3.99 201070.0918 92.7 89.1
Chromium mg/kg 107 81.6 75.0-12576.9 4.87 2010718.6 106 101
Lead mg/kg ML10780.5 75.0-12574.6 6.42 2010714.5 101 94.6
Selenium mg/kg 107 88.9 75.0-12582.9 7.02 201070.264 95.7 89.3
Silver mg/kg 21.5 84.0 75.0-12581.0 3.60 2021.5ND 18.0 17.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/07/2023 09:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92684831
Proposed Abernethy Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2125391
7471A
EPA 7471B
Mercury 7471B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92684831001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3969958-1
Associated Lab Samples:92684831001
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0400 09/06/23 15:520.0180
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3969958-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.4930.500 98.6 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3969958-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1651092-03
R3969958-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.598 112 75.0-125103 8.71 200.598ND 0.673 0.617
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/07/2023 09:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92684831
Proposed Abernethy Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2125098
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92684831001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3968566-1
Associated Lab Samples:92684831001
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 09/01/23 10:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3968566-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1651189-01
R3968566-3SAMPLE DUPLICATE:
Total Solids %81.1 0.849 1080.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/07/2023 09:02 AM
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Huntersville, NC 28078
[phone]
Page 8 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92684831
Proposed Abernethy Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2124753
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92684831001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3968823-1
Associated Lab Samples:92684831001
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 09/04/23 03:350.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3968823-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.5210.0 95.2 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3968823-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1651102-01
R3968823-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 20.0 100 75.0-12590.4 10.5 2020.0ND 20.1 18.1
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3968823-7MATRIX SPIKE SAMPLE:
MSSpike
Result
L1651102-01
Chromium, Hexavalent mg/kg 646641 101 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1651099-01
R3968823-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.300J D8,J20020ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1651288-03
R3968823-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2023 09:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 13
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92684831
Proposed Abernethy Site
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The sample and duplicate results for this parameter are less than 5 times the reporting limit, the RPD may not be
statistically valid.D8
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/07/2023 09:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 13
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92684831
Proposed Abernethy Site
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92684831001 2124812 2124812SS-1 3051 EPA 6020B
92684831001 2125391 2125391SS-1 7471A EPA 7471B
92684831001 2125098 2125098SS-1 SM 2540 G SM 2540G
92684831001 2124753 2124753SS-1 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/07/2023 09:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 13
Page 12 of 13
Page 13 of 13

ESP Corporate Office
3475 Lakemont Boulevard
Fort Mill, SC 29708
803.802.2440

Mailing Address: P.O. Box 7030 Charlotte, NC 28241
800.960.7317 | www.espassociates.com

Concord
7144 Weddington Rd. NW
Suite 110
Concord, NC 28027
704.793.9855

Cornelius
20484 Chartwell Center Dr.
Suite D
Cornelius, NC 28031
704.649.2863

Raleigh
2200 Gateway Centre Blvd.
Suite 216
Morrisville, NC 27560
919.678.1070

Greensboro
7011 Albert Pick Rd
Suite E
Greensboro, NC 27409
336.334.7724

Wilmington
211 Racine Drive
Suite 101
Wilmington, NC 28403
910.313.6648

Charleston
2154 North Center Street
Suite E-503
North Charleston, SC 29406
843.714.2040

Nashville
500 Wilson Pike Circle
Suite 310
Brentwood, TN 37027
615.760.8300

Pittsburgh
One Williamsburg Place
Suite G-5, Box 13
Warrendale, PA 15086
724.462.6606
Bradenton
518 13th Street
West Bradenton, FL 34205
941.345.5451

Indianapolis
8673 Bash Street
Indianapolis, IN 46256
317.537.6979

Albuquerque
1203 West Ella Drive
Corrales, NM 87048
505.314.1322

Birmingham
291 Cahaba Valley Parkway North Suite A
Pelham, AL 35124
205.664.8498

Vickrey & Associates, LLC - An ESP Company

San Antonio
12970 Country Parkway
San Antonio TX 78216
210.349.3271

Austin
3600 West Parmer Lane
Suite 175
Austin, TX 78727
512.494.8014

McAllen
1216 East Jasmine Avenue
Suite C
McAllen, TX 78501
956.340.0045