27027_Ables Auto_Phase II ESA_20231016

Via Email
October 16, 2023

NCDEQ – Division of Waste Management
Brownfields Redevelopment Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Attn: Ms. Carolyn Minnich

Re: Phase II ESA
Fromer Ables Auto
2501, 2511, and 2533 Wilkinson Boulevard
Charlotte, North Carolina
Brownfields Project No. 27027-23-060
H&H Project No. TPI-002

Dear Carolyn:

On behalf of SBBH Wilkinson, LLC, please find the enclosed Phase II Environmental Site
Assessment (ESA) report prepared for the above referenced Site. Because the Site was entered
into the Brownfields Redevelopment Section, the Phase II ESA sampling approach and methods
were designed to be consistent with a comprehensive Brownfields assessment to evaluate the
potential for impacts and risks associated with the planned redevelopment.

Should you have questions or need additional information, please do not hesitate to contact us at
[phone].

Sincerely,
Hart & Hickman, PC
Haley Martin, PG Justin Ballard, PG
Senior Project Geologist Project Manager

Enclosure:

cc: Mr. Scott Bortz, Tribek Properties (via email)
Mr. Chris Walker, Alexander Ricks, PLLC (via email)
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Phase II Environmental Site Assessment
Former Ables Auto
2501, 2511, and 2533 Wilkinson Boulevard
Charlotte, North Carolina
Brownfields Project No. 27027-23-060
H&H Job No. TPI-001

Table of Contents

1.0 Introduction .............................................................................................................................1 
1.1 Background ............................................................................................................................1 
1.2 Previous Assessment Activities .............................................................................................1 
2.0 Phase II ESA Activities ...........................................................................................................4 
3.0 Receptor Survey ......................................................................................................................6 
4.0 Soil Assessment Activities .......................................................................................................9 
4.1 Soil Sampling Activities ........................................................................................................9 
4.2 Soil Sampling Analytical Results .........................................................................................11 
5.0 Groundwater Assessment Activities ....................................................................................13 
5.1 Groundwater Sampling Activities ........................................................................................13 
5.2 Groundwater Sample Analytical Results .............................................................................15 
6.0 Soil Gas Assessment Activities .............................................................................................17 
6.1 Soil Gas Sampling Activities ...............................................................................................17 
6.2 Soil Gas Sampling Results ..................................................................................................19 
6.3 Vapor Intrusion Evaluation .................................................................................................20 
7.0 Quality Assurance – Quality Control ..................................................................................22 
7.1 Trip Blank ............................................................................................................................22 
7.2 Field Duplicates ...................................................................................................................22 
8.0 Summary and Conclusions ..................................................................................................24 

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List of Tables

Table 1 Summary of Soil Analytical Data
Table 2 Summary of Well Construction and Groundwater Elevation Data
Table 3 Summary of Groundwater Analytical Data
Table 4 Summary of Soil Gas Analytical Data

List of Figures

Figure 1 Site Location Map
Figure 2 Site and Historical Operations Map
Figure 3 Sample Location Map
Figure 4 Receptor Survey Map
Figure 5 Shallow Groundwater Potentiometric Surface Map

List of Appendices

Appendix A Receptor Survey Form
Appendix B Boring Logs & Well Construction and Abandonment Records
Appendix C Laboratory Analytical Reports
Appendix D Groundwater and Soil Gas Sampling Forms
Appendix E DEQ Risk Calculators

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Phase II Environmental Site Assessment
Former Ables Auto
2501, 2511, and 2533 Wilkinson Boulevard
Charlotte, North Carolina
Brownfields Project No. 27027-23-060
H&H Job No. TPI-002
1.0 Introduction
Hart & Hickman, PC (H&H) has prepared this Phase II Environmental Site Assessment (ESA)
report for the Former Ables Auto Brownfields property (Brownfields Project No. 27027-23-060)
located at 2501, 2511, and 2533 Wilkinson Boulevard in Charlotte, Mecklenburg County, North
Carolina (Site). The Site consists of two contiguous parcels (Mecklenburg County Parcel
Identification Nos. 11701109 [2501/2511 Wilkinson Boulevard] and 11701110 [2533 Wilkinson
Boulevard]) that collectively total approximately 3.12 acres of land approximately two miles
west of uptown Charlotte. The Site is currently vacant land but was most recently utilized as an
automotive repair facility. A Site location map is provided as Figure 1, and the Site, historical
Site features, and the area surrounding the Site are shown in Figure 2.
1.1 Background
As early as the 1930s, the Site consisted predominantly of vacant land. By the late 1940s, the
Site was developed with multiple buildings utilized for auto repair and tire retreading operations.
Based on review of a 1950 Sanborn Map and a 1963 Sanborn Map, the Site buildings were also
utilized for foundry operations, paint storage, a machine shop, and a junkyard. Former Site
buildings were demolished in the early 2010s. Approximate locations of former Site structures
present during the 1950s and 1960s and during the Ables Auto operational period are shown in
Figure 2.
1.2 Previous Assessment Activities
A brief summary of former environmental assessment activities conducted at the Site and their
corresponding dates is provided below.
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1992 UST Removal
Information provided in underground storage tank (UST) closure documentation prepared for the
Site by Nationwide Tank and Environmental Services, Inc. indicates that one (1) 1,000-gallon
gasoline UST, associated product lines, and dispenser were removed from the northwestern
portion of the 2533 Wilkinson Boulevard Site parcel in July 1992. Two (2) closure soil samples
(#1 and #2) were collected from the bottom of the UST basin and submitted for analysis of total
petroleum hydrocarbons (TPH) by EPA Methods 3550/5030. Results of the closure soil samples
did not identify TPH at concentrations above the laboratory reporting limits. Based on the
closure soil sample laboratory analytical results, the North Carolina Department of
Environmental Quality (DEQ) UST Section issued a No Further Action letter on
October 1, 1992.

Based upon review of a 1950 Sanborn Map, two (2) gasoline USTs were located at the 2533
Wilkinson Boulevard Site parcel (see Figure 2). As previously mentioned, one of the USTs was
removed in 1992. There is no information related to the removal or closure of the second UST in
the environmental and/or regulatory records. Therefore, the status of the second tank on the
2533 Wilkinson Boulevard Site parcel is unknown.

February 2022 Phase I ESA
In February 2022, Summit Engineering, Laboratory, and Testing Inc. (Summit) completed Phase
I ESA activities for the 2501/2511 Wilkinson Boulevard Site parcel. Summit considered the
former use of the Site for auto repair operations to be an environmental concern and
recommended additional assessment, which is described below.

June 2022 Limited Groundwater Sampling
In June 2022, Summit completed limited groundwater sampling activities at the Site to evaluate
the potential for impacts associated with historical on-Site auto repair operations. Information
provided in a Limited Phase I Environmental Site Assessment report prepared by Summit dated
June 6, 2022, indicates that assessment activities included the collection of two (2) groundwater
samples for laboratory analysis from two (2) temporary groundwater monitoring points (TMW-1
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and TMW-2). A third temporary groundwater monitoring point (TMW-3) was installed as part
of groundwater assessment activities; however, shallow refusal above the surficial groundwater
table was encountered by the drill rig. As such, a groundwater sample could not be collected for
laboratory analysis. The locations of temporary groundwater monitoring wells TMW-1 and
TMW-2 are shown in Figure 3.

The TMW-1 and TMW-2 groundwater samples were submitted for laboratory analysis of
volatile organic compounds (VOCs) by EPA Method 8260 and semi-VOCs (SVOCs) by EPA
Method 8270. Groundwater sample laboratory analytical results identified trichloroethylene or
TCE (35.8 micrograms per liter [g/L]) at a concentration above the North Carolina Department
of Environmental Quality 2L Groundwater Quality Standard (2L Standard) of 3.0 g/L in the
TMW-1 groundwater sample collected in the northeastern portion of the Site (Figure 3). No
other organic compounds were detected at concentrations above the 2L Standards in the June
2022 groundwater sampling event.

November 2022 Phase I ESA
In November 2022, Summit completed Phase I ESA activities at the 2533 Wilkinson Boulevard
Site parcel. Results of the Phase I ESA did not identify environmental concerns in connection
with the 2533 Wilkinson Boulevard Site parcel.

To manage potentials risks associated with future redevelopment activities, which may consist of
residential land use, SBBH Wilkinson, LLC submitted a Brownfields Property Application to the
DEQ Brownfields Redevelopment Section on May 5, 2023. The Brownfields Redevelopment
Section issued a Letter of Eligibility (LOE) on August 25, 2023. To minimize the potential for
data gaps and expedite the Brownfields process, H&H designed the Phase II ESA sampling
approach to be consistent with assessment activities typically requested by the Brownfields
Redevelopment Section. A brief description of the Phase II ESA sampling activities is provided
in Section 2.0.

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2.0 Phase II ESA Activities

In July 2023, H&H conducted Phase II ESA activities at the Site which included collection of
soil, groundwater, and exterior soil gas samples for laboratory analysis. The purpose of the
assessment activities was to further evaluate the potential for impacts at the Site associated with
historical on-Site operations. In addition, H&H performed a receptor survey to obtain
information about land use, water supply, basements, underground utilities, drains, and surface
water bodies at and in the vicinity of the Site.

The assessment activities were conducted in general accordance with the DEQ Inactive
Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup of Contaminated Sites
(Guidelines) dated September 2022, the DEQ Division of Waste Management (DWM) Vapor
Intrusion Guidance (VI Guidance) dated March 2018, most recent versions of the U.S. EPA
Region IV Laboratory Services and Applied Science Division (LSASD) Field Branches Quality
System and Technical Procedures guidance, and the Brownfields Minimum Requirements
Checklist - Site Assessment Work Plans and Reports dated March 2023.

Prior to conducting field activities, H&H contacted North Carolina 811, the public utility locator,
to mark subsurface utilities at the Site. H&H also contracted with a private utility locator to
mark utilities which were not identified by the public locator. The private utility locator utilized
ground penetrating radar (GPR) and electromagnetic survey techniques to identify anomalies
consistent with current and/or former USTs. In addition, H&H directed the drilling contractor to
hand clear each boring to a depth of approximately 5 feet below ground surface (ft bgs) to further
screen the boring locations for the presence of subsurface utilities. H&H obtained a
Mecklenburg County Subsurface Investigation Permit (SIP No. 70003149) prior to temporary
monitoring well installation and sampling.

A summary of receptor survey results is provided in Section 3.0, details of the soil, groundwater,
and soil gas assessment activities are provided in Sections 4.0 through 6.0, respectively.

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A description of the quality assurance and quality control measures implemented during the
sampling and analysis are provided in Section 7.0, and summary and conclusions based on
results of the assessment activities are provided in Section 8.0.
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3.0 Receptor Survey

In July 2023, H&H conducted a receptor survey at the Site and surrounding area. Receptor
survey activities included an intensive pedestrian and vehicular survey for possible potable water
supply wells, springs, and surface water intakes used as a source of water within a 1,500 ft radius
of the Site. H&H also reviewed the online Mecklenburg County Well Information System for
potential wells in the area and utilized the online DEQ Source Water Assessment Program
(SWAP) to identify potential potable water sources for properties located within a 1,500 ft radius
of the Site. In addition, H&H identified the locations of main underground and aboveground
utilities, and land use and zoning in the area of the Site using available Mecklenburg County
online resources. A receptor survey map is provided as Figure 4, and a copy of the completed
DEQ Brownfields Property Receptor Survey form is provided as Appendix A.

Results of the receptor survey activities are summarized below.

Zoning
The Site is zoned as industrial manufacturing and logistics (ML-2). The adjacent properties
located to the east, west, and south are zoned as industrial manufacturing and logistics (ML-1
and ML-2). Adjacent properties to the north are zoned as industrial manufacturing and logistics
(ML-1), light-industrial (I-1), and office flex campus (OFC).

Properties located to the north of the Site across Wilkinson Boulevard are developed with
commercial buildings occupied by an electrical equipment supplier and an automotive
dealership. The western adjoining property is developed with a vacant commercial/industrial
warehouse building and sports complex. Properties located south of the Site across Southern
Railway are developed with a commercial building occupied by a tree service company and
several single-family residences. Properties located to the east of the Site across Remount Road
are developed with commercial buildings used for offices and automotive sales.

Municipal Water Availability
Municipal water supplied by the City of Charlotte is available to the Site and surrounding area.
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H&H did not identify sources of public drinking water within 1,500 ft of the Site based on the
review of information available on Mecklenburg County Well Information System Maps, DEQ
SWAP, and the Annual Water Quality Report published by the City of Charlotte. The City of
Charlotte obtains raw water from Lake Norman and Mountain Island Lake which are located
approximately 8 miles northwest of the Site (at the closest point to Mountain Lake).

Water Supply Wells
H&H conducted a pedestrian and vehicular survey of properties within a 1,500 ft radius of the
Site to identify potential potable water supply wells. H&H also utilized DEQ SWAP geographic
information system map and Mecklenburg County Well Information System maps to identify
potential potable water supply wells located within a 1,500 ft radius of the Site. Based on review
of the Mecklenburg County Well Information System, one (1) abandoned private water supply
well was reported for the property located at 5010 Pammell Drive in Charlotte, North Carolina
(approximately 900 ft southwest of the Site). No active water supply wells were identified
within a 1,500 ft radius of the Site.

Surface Water Bodies
Based on the DEQ Surface Water Classification system, Irwin Creek is a Class C surface water
body. A Class C surface water body is defined as “waters protected for uses such as secondary
recreation, fishing, wildlife, fish consumption, aquatic life including propagation, survival and
maintenance of biological integrity, and agriculture. Secondary recreation includes wading,
boating, and other uses involving human body contact with water where such activities take
place in an infrequent, unorganized, or incidental manner”. Based on information obtained from
the DEQ Division of Water Resources (DWR) Surface Water Classifications geographic
information system map, the subject Site is not located within a protected water supply
watershed area. Irwin Creek is a natural surface water feature that generally flows north to south
across west Charlotte, and it consists of a rocky or sediment bottom.

The Mecklenburg County Polaris 3G online geographic information system (GIS) depicts a
surface water feature in the southern portion of the Site. Based on visual observations during the
pedestrian survey, surface water features are not present on Site. Portions of unnamed tributaries
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of Irwin Creek are located approximately 1,100 ft southeast and to the southwest approximately
1,350 ft from the Site.

Subsurface Utilities and Structures
H&H contacted North Carolina 811, the public utility locator, to mark subsurface utilities located
on the Site and conducted a visual reconnaissance in the Site area to identify potential subsurface
structures within 100 ft of the subject Site. H&H observed evidence of subsurface utilities
including storm sewer, municipal water, and natural gas adjacent to the Site and nearby adjacent
properties. Natural gas, storm sewer, and overhead electric lines were observed along the
northern Site boundary along Wilkinson Boulevard and municipal water lines were observed
along the western Site boundary. During the vehicular survey, a childcare facility (2425 Morton
Street) was observed approximately 1,250 ft to the northeast of the Site. H&H did not observe
structures with potential basements within a 100 ft radius of the Site during the visual
reconnaissance. Approximate locations of subsurface and overhead utilities located in the
immediate vicinity of the Site are shown in Figure 4.
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4.0 Soil Assessment Activities

In July 2023, AmeriProbe advanced five (5) soil borings at the Site to evaluate subsurface
conditions in areas of potential environmental concern. Two (2) soil borings were advanced in
the vicinity of the former UST and suspect UST in the northwestern portion of the Site. Three
(3) soil borings were advanced within the footprints of former on-Site buildings in the northern
and central portions of the Site. In addition, two (2) soil borings were advanced in the southern
portion of the Site for the collection of background soil samples to establish Site-specific
background conditions. The locations of the soil borings are shown in Figure 3.

Soil borings were advanced utilizing a decontaminated stainless-steel hand auger and/or a
track-mounted direct push technology (DPT) drill rig. During boring advancement, continuous
soil samples were collected from the center of the hand auger bucket or from acetate lined
macrocore liners at each boring location. The soil samples were logged for lithologic
description, observed for obvious evidence of staining and unusual odors, and field screened for
the presence of volatile organic vapors using a calibrated photoionization detector (PID). Field
screening results identified elevated PID readings in soil boring SB-2 (near the suspect UST in
the northwestern portion of the Site) and staining was observed in deeper soil (i.e., 8-10 ft bgs) in
soil boring SB-4 (within the footprint of a former paint storage area). Aside from soil boring
locations SB-2 and SB-4, obvious evidence of staining, odors, or elevated PID readings were not
observed by field personnel during soil boring advancement. Boring logs with lithologic
descriptions and field screening results for each soil boring are provided in Appendix B.

A discussion of the soil sampling activities and results is provided in the following sections.

4.1 Soil Sampling Activities

Former UST and Suspect UST
Two soil borings (SB-1 and SB-2) were advanced adjacent to the former UST and suspect UST,
respectively. Specifically, the borings were advanced along the exterior sides of a former
building used for automotive repair and as a foundry. The soil borings were advanced to
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approximately 15 ft bgs and one soil sample was collected from each boring for laboratory
analysis.

Based on historical Site uses in the general vicinity of the boring locations, field observations,
and results of field screening, soil samples were collected from the depth interval with the
highest potential for impacts and a depth interpreted to be near or below the base of the USTs
(i.e., 8-10 ft bgs in soil boring SB-1 and the 4-6 ft bgs in soil boring SB-2).

Former Paint Storage Buildings
Two soil borings (SB-3 and SB-4) were advanced within the footprints of former paint storage
areas. The borings were advanced to approximately 15 ft bgs and one sample was collected from
each boring for laboratory analysis.

Based on historical Site uses in the general vicinity of the boring locations, field observations,
and results of field screening, soil samples were collected from the depth interval with the
highest potential for impacts (i.e., 0-2 ft bgs in soil boring SB-3 and 8-10 ft bgs in soil boring
SB-4).

Former Machine Shop Area
One soil boring (SB-5) was advanced within the footprint of the former machine shop building
located in the west-central portion of the Site. The soil boring was advanced to approximately
15 ft bgs. No obvious evidence of impact was observed during field screening. As such, one soil
sample was collected for laboratory analysis from shallow soil (i.e., 0-2 ft bgs).

The soil samples selected for laboratory analysis were placed in dedicated laboratory supplied
sample containers, labeled with the sample identification, date, and requested analysis, and
placed in a laboratory supplied cooler with ice. The samples were delivered to Waypoint
Analytical (Waypoint), a North Carolina certified laboratory, under standard chain of custody
protocols. Soil samples were analyzed for VOCs by EPA Method 8260, SVOCs by EPA
Method 8270, Resource Conservation and Recovery Act (RCRA) metals by EPA Methods
6020/7471, and hexavalent chromium by EPA Method 7199.
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Following sampling activities, the soil borings were converted into temporary monitoring wells
as discussed below in Section 5.0, converted into temporary soil gas sampling points as
discussed in section 6.0, or abandoned using hydrated bentonite, and the surfaces were repaired
similar to pre-drilling conditions. Soil boring location were estimated using a hand-held global
positioning system (GPS) unit.

4.2 Soil Sampling Analytical Results

A tabular summary of the soil sample analytical results is provided as Table 1. The laboratory
analytical reports and chain of custody records are provided in Appendix C. The laboratory
analytical results were compared to the most recent versions of the DEQ Residential and
Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs) dated July 2023. In
addition to the PSRGs, metals were compared to published concentrations for naturally occurring
metals as well as Site-specific background levels of metals.

A discussion of the laboratory analytical results in comparison to the regulatory screening levels
and background levels for metals is included below.

VOCs
Laboratory analytical results indicate that acetone, n-butylbenzene, sec-butylbenzene, tert-
butylbenzene, carbon disulfide, chloroethane, ethylbenzene, n-hexane, isopropylbenzene, methyl
ethyl ketone, 4-isopropyl toluene, methylene chloride, naphthalene, n-propylbenzene, 1,2,4-
trimethylbenzene, and 1,3,5-trimethylbenzene were detected at concentrations above the
laboratory method detection limits, but below the DEQ Residential PSRGs. No other VOCs
were detected at concentrations above the laboratory method detection limits.

SVOCs
Laboratory analytical results indicate that the polynuclear aromatic hydrocarbon (PAH, a subset
of SVOCs) benzo(a)pyrene (0.232 J milligrams per kilogram [mg/kg]) was detected above the
DEQ Residential PSRG of 0.11 mg/kg in the soil sample collected within the footprint of the
former machine shop (SB-5). The J-Flag designation indicates that the compound was detected
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at a concentration above the laboratory method detection limit but below the laboratory reporting
limit, resulting in a laboratory estimated concentration. PAHs are typically generated by the
incomplete combustion of petroleum and non-petroleum related fuels (such as coal and wood)
and are commonly found in urban areas and industrial properties such as the subject Site. No
other SVOCs were detected at concentrations above the DEQ PSRGs.

Metals
As expected, several metals were detected at concentrations above laboratory method detection
limits in the soil samples collected at the Site. Hexavalent chromium (up to 1.16 mg/kg) was
detected in soil samples SB-1 and SB-2 (near the former UST and suspect UST) at
concentrations above the DEQ Residential PSRG (0.31 mg/kg) and the upper limit of published
and Site-specific background levels (0.705 mg/kg). Remaining detected concentrations of metals
were generally consistent with background levels established for the Site area and published
background levels for North Carolina soils.

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5.0 Groundwater Assessment Activities

In July 2023, H&H provided oversight of AmeriProbe, a North Carolina licensed well driller,
during installation of four (4) temporary groundwater monitoring wells (HH-TMW-1 through
HH-TMW-3 and HH-TMW-5) at the Site. Based upon review of area topography (see Figure 1),
the topographic gradient at the Site generally slopes from north to south toward the Southern
Railway.

Due to shallow refusal by the hollow stem auger drill rig, proposed temporary monitoring well
HH-TMW-4 was not installed during Phase II ESA activities. Groundwater samples were
collected for laboratory analysis from the installed temporary monitoring wells to further
evaluate subsurface groundwater conditions. Locations of the temporary monitoring wells are
depicted in Figure 3 and were installed in the locations described below.

 Two (2) temporary monitoring wells (HH-TMW-1 and HH-TMW-2) were installed in the
northwestern portion of the Site and downgradient of the reported USTs and former auto
repair and foundry operations;
 One temporary monitoring well (HH-TMW-3) was installed in the northern and
upgradient portion of the Site; and
 One temporary monitoring well (HH-TMW-5) was installed in the southern and
downgradient portion of the Site.

Details of the temporary monitoring well installations, groundwater sampling activities, and
laboratory analytical results are provided in the following sections.

5.1 Groundwater Sampling Activities

The temporary monitoring wells were installed utilizing DPT and hollow stem auger drilling
techniques to advance each boring until sufficient groundwater was encountered. Continuous
soil samples were collected from the temporary monitoring well borings and logged for
lithologic description, observed for obvious evidence of staining and unusual odors, and field
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screened for the presence of volatile organic vapors using a calibrated PID. No obvious evidence
of impacts was observed in vadose zone soil based on field screening results.

Temporary monitoring wells were constructed of 2-inch diameter PVC with 15 ft of pre-packed
well screen set to bracket the water table and 2-inch diameter PVC well casing to the ground
surface. Temporary monitoring wells were installed to depths ranging from approximately 23 to
25 ft bgs. A filter sand pack was installed from the bottom of each temporary well boring to
approximately 2 ft above each well screen and a hydrated bentonite seal was then installed above
the filter sand pack. Temporary monitoring well boring logs with well construction details and
driller provided well construction records are provided in Appendix B.

Following installation, the wells were allowed to equilibrate to static conditions and a
decontaminated electronic water level indicator was used to measure the depth to the water table
relative to the ground surface. Groundwater was measured at depths ranging from approximately
15.51 ft below top of casing (TMW-2) at higher elevations in the northwestern portion of the
Site, to 20.19 ft below top of casing (TMW-5) at lower elevations in the southern portion of the
Site. This is generally consistent with the topographic gradient for the Site.

H&H surveyed the temporary well elevations relative to a storm drain manhole at 741.96 ft
above mean sea level (MSL) located in the sidewalk located along the northern boundary of the
Site (information acquired from a survey plat). The depth to groundwater measurements and the
temporary well elevations were then used to estimate the groundwater table elevations at each
temporary well location. The groundwater table elevations were subsequently used to estimate
the implied groundwater flow direction at the Site, which is generally to the southeast toward the
tributary of Irwin Creek. A tabular summary of well construction details and groundwater
elevation data is provided as Table 2, and the shallow groundwater table potentiometric surface
and inferred groundwater flow direction are shown in Figure 5.

Once depth to water and surveying measurements were collected, the temporary wells were
developed by removing a minimum of 3 to 5 volumes and until field parameters had stabilized
(pH± 0.1 Standard Units [SU] and conductivity varies no more than 5%). Following
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development, wells were allowed to equilibrate to static conditions and a groundwater sample
was collected for laboratory analysis from each temporary monitoring well utilizing low
flow/low stress purging techniques using a peristaltic and dedicated polyethylene tubing.

During sampling, the intake point of the sample tubing was placed in the approximate mid-
portion of the screened interval of the well, and groundwater was removed at a rate no greater
than 200 milliliters per minute (mL/min). H&H utilized calibrated water quality meters to
collect measurements of pH, temperature, dissolved oxygen, oxidation reduction potential,
turbidity, and specific conductivity at five-minute intervals during the purging process. Purging
was considered complete when the field parameters stabilized (pH ± 0.1 SU, conductivity varied
no more than 5%, and turbidity was less than 10 Nephelometric Turbidity Units [NTUs]).
Groundwater sampling forms completed by sampling personnel are provided in Appendix D.

Once groundwater parameters stabilized, groundwater samples submitted for analysis of SVOCs
and RCRA metals were collected directly into laboratory supplied glassware directly from the
sample tubing discharge. The groundwater samples submitted for VOC analysis were collected
directly into laboratory supplied sample containers using the “soda straw” method to eliminate
the potential for volatile compound loss through the pump head. The sample containers were
labeled with the sample identification, date, time, and requested analysis, and placed in a
laboratory supplied cooler with ice. The groundwater samples were delivered to Waypoint under
standard chain of custody protocols for analyses of VOCs by EPA Method 8260, SVOCs by
EPA Method 8270, and RCRA metals by EPA Method 6020/7470.

After the sampling activities were complete, the temporary monitoring well locations were
estimated using a hand-held GPS unit. The temporary monitoring wells were then permanently
abandoned by AmeriProbe and the surfaces were repaired to pre-drilling conditions. Driller
provided temporary monitoring well abandonment records are provided in Appendix B.

5.2 Groundwater Sample Analytical Results

A tabular summary of the groundwater sample laboratory analytical results is presented in
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Table 3. Copies of the laboratory analytical reports and chain of custody records are provided in
Appendix C. Groundwater analytical data were compared to the DEQ 2L Standards dated April
2022 and the DEQ Residential and Non-Residential Vapor Intrusion Groundwater Screening
Levels (GWSLs) dated July 2023.

VOCs
Laboratory analytical results indicate chloroform (16.5 µg/L) was detected at a concentration
above the DEQ Residential and Non-Residential Vapor Intrusion GWSLs in temporary
monitoring well HH-TWM-3, which was installed in an upgradient location along the northern
Site boundary. Chloroform is a by-product of the chlorination process for municipal drinking
water and is likely associated with water lines in the Site vicinity rather than a release associated
with historical operations. No other VOCs were detected at concentrations above the 2L
Standards or the DEQ Vapor Intrusion GWSLs in the groundwater samples.

SVOCs
Laboratory analytical results identified the presence of diethyl phthalate at concentrations above
the laboratory method detection limits but below the 2L Standard. No other SVOCs were
detected at concentrations above the laboratory method detection limits in groundwater samples.

Metals
Laboratory analytical results detected the presence of arsenic, barium, and chromium at
concentrations above the laboratory method detection limits but below the 2L Standards. No
other metals were detected at concentration above the laboratory method detection limits in the
groundwater samples.

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6.0 Soil Gas Assessment Activities

To evaluate the potential for structural vapor intrusion into potential residential buildings, H&H
installed and sampled seven (7) temporary exterior soil gas monitoring points within former
building footprints and in the eastern portion of the Site. The exterior soil gas sampling point
locations are shown in Figure 3. The soil gas sampling activities and results are described in the
following sections.

6.1 Soil Gas Sampling Activities

Exterior Soil Gas Sample Point Installation
Under the direction of H&H, AmeriProbe advanced seven (7) soil borings for installation of
temporary exterior soil gas monitoring points within the footprint of the former auto repair
buildings (SG-1 through SG-3, SG-6, and SG-7), within the footprint of the former machine shop
(SG-5), and in the eastern portion of the Site (SG-4).

The soil gas monitoring points were installed at a depth of approximately 7.5 ft bgs using a
stainless-steel hand auger and DPT drilling methods. Continuous soil samples were collected
from the soil gas monitoring point borings and logged for lithologic description, observed for
obvious evidence of staining and unusual odors, and field screened for the presence of volatile
organic vapors using a calibrated PID. Field screening results did not indicate obvious evidence
of potential impacts in the soil gas monitoring point borings.

Once at target depth, a six-inch stainless steel vapor implant screen attached to a length of
Teflon® tubing was installed at the base of each borehole. Filter sand was then placed within the
annulus of the boring from the base of the boring to a depth of approximately 6-inches above the
top of the vapor screen. The sampling points were completed by placing hydrated bentonite
from the top of the filter sand to the ground surface. Boring logs with soil gas monitoring point
construction details are provided in Appendix B. The soil gas monitoring points were allowed to
equilibrate for a minimum of 24-hours after installation and prior to sample collection.

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Soil Gas Sampling
Each gas sample was collected utilizing a laboratory supplied 1.4-liter Summa® canister
connected to an air-flow regulator calibrated by the laboratory to collect the soil gas sample at a
rate of approximately 100 mL/min. Prior to collection of the soil gas samples, “shut-in” tests
were conducted on the sampling train and helium leak checks were conducted at each soil gas
sampling point. A description of the shut-in test and helium leak testing procedures is provided
below.

The shut-in test was conducted by connecting the flow regulator with the vacuum gauge to the
Summa® canister and sealing the flow regulator with the laboratory provided brass cap. Once
the sampling train was “closed”, the sample valve on the Summa® canister was opened and the
reading on the vacuum gauge was recorded. The Summa® canister sample valve was then
closed, and the vacuum gauge was observed to ensure no vacuum loss occurred. If the vacuum
reading remained the same, the shut-in test was considered successful. If vacuum loss occurred,
the flow regulator and/or brass cap and flow regulator were reseated, and the shut-in test was
repeated until the vacuum reading remained stable. Each canister passed the shut-in test criteria.

Following successful shut-in tests, each Summa® canister was connected to the Teflon® sample
tubing using a brass nut and ferrule assembly to create an airtight seal and the leak check was
performed. The leak check was performed by constructing a shroud over the sampling train and
flooding the shroud with helium gas. Helium concentrations inside the shroud were measured
using a helium gas detector and maintained at concentrations ranging from approximately 10%
to 11%. Once helium concentrations stabilized within the shroud, the sample tubing was purged
outside of the shroud using a syringe and a three-way valve to collect purged soil gas into a
Tedlar® bag. The purged soil gas was then analyzed using the helium gas detector to ensure that
helium concentrations in the soil gas sample were less than 10% of the helium concentrations
measured within the shroud. Each soil gas sampling point passed the helium leak check criteria.

Following successful leak checks, the soil gas samples were collected by opening the intake
valve on the Summa® canister flow regulator. Vacuum readings for the Summa® canister were
recorded prior to and following the sampling period to ensure adequate sample volume was
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collected. A vacuum of approximately 5 inches of mercury or more were maintained within the
canisters at the conclusion of the sampling event in accordance with DEQ DWM VI Guidance.
Following sample collection, the Summa® canisters were delivered to Waypoint under standard
chain-of-custody protocols for analysis of VOCs by EPA Method TO-15. Upon receipt of the
samples, the laboratory recorded the final received vacuum pressure for each Summa® canister.

After sampling was completed, the sample locations were estimated by using a hand-held GPS
unit. The sample locations were permanently abandoned, and the surfaces were repaired similar
to pre-drilling conditions.

6.2 Soil Gas Sampling Results

Laboratory analytical results for the soil gas samples were compared to the DEQ Residential and
Non-Residential Vapor Intrusion Sub-Slab and Exterior Soil Gas Screening Levels (SGSLs)
dated July 2023. A summary of the analytical results is provided as Table 4, and copies of the
laboratory analytical reports and chain of custody records are included as Appendix C.

Laboratory analytical results indicate that VOCs were detected at concentrations above the
laboratory method detection limits in each sample. Of the VOCs detected, petroleum-related
compounds and chlorinated compounds were detected above the Residential SGSLs.
Specifically, benzene (up to 35 micrograms per cubic meter [µg/m3]) was detected above the
Residential SGSL in samples SG-2/SG-DUP, SG-3, SG-4, SG-5, and SG-6. Naphthalene was
detected above the Residential SGSL in SG-3 (5.59 µg/m3) and SG-4 (7.11 µg/m3).
Tetrachloroethylene or PCE (485 µg/m3) was detected above the Residential SGSL in sample
SG-3. TCE (up to 24.7 µg/m3) was detected above the Residential SGSL in samples SG-4 and
SG-5.

In addition, chloroform (up to 44.5 µg/m3) and 1,3-butadiene (up to 29.6 µg/m3) were detected
above the Residential SGSLs in samples SG-1, SG-2/SG-DUP, SG-3, SG-4, SG-5, and/or SG-6.
As previously mentioned, chloroform is likely associated with municipal water service lines
rather than potential vapor intrusion associated with an on-Site release. 1,3-butadiene is likely
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associated with volatilization of DPT drilling tooling and is also not considered a vapor intrusion
concern. No other compounds were detected at concentrations above the DEQ Vapor Intrusion
SGSLs in the exterior soil gas samples collected at the Site.

6.3 Vapor Intrusion Evaluation

The DEQ Vapor Intrusion SGSLs are very conservative and based upon a Target Cancer Risk
(TCR) of 1 x 10-6 for potential carcinogenic effects and a Target Hazard Quotient (THQ) of 0.2
for potential non-carcinogenic effects. Vapor intrusion mitigation or additional assessment is not
typically warranted if the calculated cumulative lifetime incremental carcinogenic risk (LICR) is
1 x 10-4 or less and the acceptable level for non-carcinogenic risk is a calculated cumulative
hazard index (HI) of 1.0 or less.

H&H utilized the DEQ Risk Calculator (July 2023) assuming residential and non-residential land
use scenarios to further evaluate potential cumulative risks for the soil gas to indoor air vapor
intrusion pathway for the potential Site building. To model the potential for structural vapor
intrusion under a hypothetical “worst-case” scenario, H&H conservatively calculated the
cumulative risks using the highest concentration of any compound detected in exterior soil gas
sample collected at the Site. In addition, H&H calculated the cumulative risks excluding 1,3-
butadiene and chloroform, which are likely associated with volatilization of DPT drilling tooling
and leaking municipal water lines, respectively. Risk calculator results are summarized in the
table below. Copies of the completed risk calculators are provided in Appendix E.

Evaluation Area Land Use
Scenario
Calculated
Cumulative
LICR
Calculated
Cumulative HI
Exceedance of
Acceptable
Levels?
Site-Wide Worst Case Residential 3.1 x 10-5 1.4 Yes
Non-Residential 2.3 x 10-6 0.11 No
Site-Wide
(no chloroform or 1,3-
butadiene)
Residential 1.1 x 10-5 0.94 No
Non-Residential 7.5 x 10-7 0.074 No
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As shown in the table above, risk calculator results indicate that under a hypothetical worst-case
scenario for the soil gas to indoor air vapor intrusion pathway for residential use, the cumulative
LICR is less than 1 x 10-4, but the cumulative HI (1.4) is greater than 1.0, indicating there may be
potential for structural vapor intrusion into future residential buildings at unacceptable levels.
Risk calculator results indicate that under a hypothetical worst-case scenario for the soil gas to
indoor air vapor intrusion pathway for non-residential use, the cumulative LICR is less than
1 x 10-4and the cumulative HI is less than 1.0. Note that risk calculations omitting 1,3-butdiene
and chloroform indicate that the soil gas to indoor air vapor intrusion pathway for residential use,
the cumulative LICR is less than 1 x 10-4, and the cumulative HI (0.94) is less than 1.0.

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7.0 Quality Assurance – Quality Control

For quality assurance and quality control purposes (QA/QC), non-dedicated equipment and tools
were decontaminated prior to use at each boring or sampling location and following exposure to
soil, groundwater, surface water, or sediment. Field QA/QC samples were analyzed along with
the investigative samples to determine potential variability introduced in sampling, handling,
shipping, and analysis. One trip blank was submitted for analysis of VOCs by EPA Method
8260. In addition, H&H collected duplicate soil, groundwater, and soil gas samples to evaluate
the ability of the laboratory to reproduce sample results. Duplicate samples were submitted to the
laboratory for the same analysis as the corresponding parent sample.

7.1 Trip Blank

The trip blank was prepared by the laboratory and consisted of certified-clean sample containers
filled with analyte-free water. The trip blank accompanied the empty laboratory sample
containers to the Site, remained within the sample cooler during sampling, and traveled back to
the laboratory with field samples. The purpose of a trip blank is to evaluate sample handling
conditions and the potential for external contaminants to compromise investigative samples
during transit. A trip blank accompanied the field VOC groundwater and surface water samples
and was submitted for laboratory analysis of VOCs by EPA Method 8260 (Trip Blank).

Laboratory analytical results indicate no VOCs were detected in the Trip Blank sample. As such
it is unlikely for external contamination to have been introduced to the investigative samples
during handling or transit. Laboratory analytical results of the trip blank are included in the
laboratory analytical report in Appendix C.

7.2 Field Duplicates

Duplicate samples were collected to evaluate the precision of the field sampling procedures,
sample matrix variability, and analytical reproducibility. Duplicate soil and groundwater
samples were collected directly into individual laboratory supplied sample containers using
sampling methodologies described in previous sections. The duplicate soil gas sample was
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collected concurrently with the parent sample using a laboratory supplied T-fitting which allows
for collection of two soil gas samples from one soil gas sampling point simultaneously. The
samples were analyzed for the same parameters as the parent samples, and the analytical results
were compared with those of the parent sample. The analytical results of the parent sample and
the duplicate sample were used to evaluate the cumulative precision of the analytical method,
sample matrix, and sample collection techniques.

Duplicate sample laboratory analytical results for each sample media are presented in the
summary tables (Table 1 for soil, Table 3 groundwater, and Table 4 for soil gas). Review of the
duplicate sample results for the soil, groundwater, and soil gas samples did not indicate
significant variability compared with the results of the parent samples. The conclusions of the
data review are that laboratory data generally meet QA/QC objectives and are usable for the
intended purpose.

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8.0 Summary and Conclusions

H&H completed Phase II ESA activities at the Former Ables Auto Brownfields property
(Brownfields Project No. 27027-23-060) located at 2501, 2511, and 2533 Wilkinson Boulevard
in Charlotte, North Carolina. The assessment activities included collection of soil, groundwater,
and exterior soil gas samples for laboratory analysis to evaluate potential risks associated with
potential residential redevelopment of the Site. A brief summary of the assessment activities is
provided below.

Receptor Survey
The results of the receptor survey did not identify active public or private water supply wells
within a 1,500 ft radius of the Site. Two unnamed tributaries of Irwin Creek are located within a
1,500 ft radius of the Site. H&H observed one childcare center, Graham Day Care Center,
located approximately 1,250 ft to the northeast of the Site. H&H did not observe structures with
potential basements within a 100 ft radius of the Site during the visual reconnaissance.

Soil Sampling
Results of soil assessment activities completed in the central portion of the Site within the
footprint of the former machine shop (SB-5) indicate a low level of PAH benzo(a)pyrene was
detected above the DEQ Residential PSRG. In addition, hexavalent chromium was detected in
soil samples collected near the former/suspect USTs (SB-1 and SB-2) at concentrations above
the DEQ Residential PSRG and the upper limit of Site-specific background levels. No other
compounds were detected at concentrations above the DEQ PSRGs or naturally occurring
background levels of metals.

Groundwater Sampling
Results of groundwater assessment activities completed in the northern and upgradient portion of
the Site indicate chloroform was detected at concentrations above the DEQ Residential and Non-
Residential Vapor Intrusion GWSLs. Chloroform is likely associated with municipal water from
water lines. No other compounds were detected at concentrations above the 2L Standards or
DEQ Vapor Intrusion GWSLs in the groundwater samples collected at the Site.
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Soil Gas Sampling
Results of the soil gas assessment activities completed on the Site indicated the presence of
benzene, 1,3-butadiene, chloroform, naphthalene, PCE, and TCE at concentrations exceeding
their respective DEQ Residential Vapor Intrusion SGSLs in select soil gas samples collected at
the Site. No other compounds were detected at concentrations above the DEQ Vapor Intrusion
SGSLs. Results of cumulative risk calculations utilizing the highest concentration of any
compound detected in any soil gas sample indicate that cumulative carcinogenic risks exceed the
acceptable threshold for residential uses. However, results of risk calculations omitting 1,3-
butdiene and chloroform, which are likely associated with volatilization of DPT drilling tooling
and leaking municipal water lines, indicate that the soil gas to indoor air vapor intrusion pathway
for residential use, the cumulative LICR is less than 1 x 10-4, and the cumulative HI is less than
1.0.

In summary, results of soil and groundwater assessment activities indicate low level impacts
associated with former Site operations and municipal water. Based on results of the July 2023
assessment activities, soil and groundwater at the Site can be managed during proposed
redevelopment activities in accordance with a DEQ Brownfields approved Environmental
Management Plan (EMP).

Risk calculator results indicate that under a hypothetical worst-case scenario (without chloroform
and 1,3-butadiene) for the soil gas to indoor air vapor intrusion pathway for residential use, the
cumulative LICR is less than 1 x 10-4, and the cumulative HI is less than 1.0. H&H understands
that a vapor intrusion mitigation system will be considered during construction of proposed
buildings to address potential vapor intrusion risks.

Table 1 Summary of Soil Analytical DataFormer Ables AutoCharlotte, North CarolinaH&H Job No. TPI-002Evaluation AreaFormer Machine ShopSample IDSB-1 SB-3 SB-4 SB-5 BG-1 BG-2Date7/10/2023 7/12/2023 7/12/2023 7/12/2023 7/11/2023 7/11/2023Depth (ft bgs)8-10 0-2 8-10 0-2 1-3 1-3Sample Type UnitsVOCs (8260D)Acetone<0.0020.006 J 0.007 J 0.090 0.007 J 0.035NA NA14,000 210,000-- --n-Butylbenzene<0.00060.008 0.016<0.0007 <0.0006 <0.0006 NA NA780 12,000-- --sec-Butylbenzene<0.00070.017 0.036<0.0008 <0.0006 <0.0006 NA NA1,600 23,000-- --tert-Butylbenzene <0.0006 <0.00060.0007 J <0.0007 <0.0006 <0.0006 NA NA1,600 23,000-- --Carbon Disulfide<0.00080.001 J 0.002 J<0.00090.0010 J<0.0007 NA NA160 740-- --Chloroethane<0.001 <0.001 <0.001 <0.0010.001 J<0.001 NA NA1,100 48,000-- --Ethylbenzene<0.00070.001 J 0.002 J<0.0009 <0.0007 <0.0007 NA NA6.1 27-- --n-Hexane 0.001 J<0.00080.001 J 0.003 J 0.0010 J<0.0008 NA NA130 540-- --Isopropylbenzene<0.00060.003 J 0.008<0.0007 <0.0005 <0.0005 NA NA410 2,100-- --Methyl Ethyl Ketone (MEK)<0.0008 <0.0008 <0.00080.017 J<0.0007 <0.0007 NA NA5,500 40,000-- --4-Isopropyl Toluene<0.0010.004 J 0.009<0.001 <0.001 <0.001 NA NANE NE-- --Methylene Chloride 0.006 J 0.003 J 0.006 J 0.008 J 0.003 J 0.003 JNA NA58 650-- --Naphthalene<0.0010.063 0.101<0.001 <0.001 <0.001 NA NA2.1 8.8-- --n-Propylbenzene<0.00070.009 0.020<0.0008 <0.0006 <0.0006 NA NA780 5,100-- --1,2,4-Trimethylbenzene<0.00060.035 0.078<0.0007 <0.0006 <0.0006 NA NA63 370-- --1,3,5-Trimethylbenzene<0.00070.004 J 0.009<0.0008 <0.0006 <0.0006 NA NA56 320-- --SVOCs (8270E)Benzo(a)anthracene<0.171 <0.168 <0.169 <0.206 <0.1600.201 JNA NA1.1 21-- --Benzo(a)pyrene<0.181 <0.178 <0.179 <0.218 <0.1690.232 JNA NA0.11 2.1-- --Benzo(b)fluoranthene<0.180 <0.176 <0.178 <0.216 <0.1680.325 JNA NA1.1 21-- --Chrysene<0.175 <0.171 <0.173 <0.210 <0.1630.184 JNA NA110 2,100-- --Fluoranthene<0.152 <0.149 <0.150 <0.182 <0.1410.296 JNA NA480 6,000-- --Phenanthrene<0.256 <0.2510.258 J<0.308 <0.239 <0.238 NA NANE NE-- --Pyrene<0.165 <0.162 <0.163 <0.199 <0.1540.303 JNA NA360 4,500-- --1-Methylnaphthalene<0.1310.319 J 0.460 J<0.157 <0.122 <0.121 NA NA18 73-- --2-Methylnaphthalene<0.1230.163 J 0.217 J<0.148 <0.115 <0.114 NA NA48 600-- --Metals (6020B/7471B/7199)Arsenic 1.57 0.372 0.339 1.22 1.04 1.06 1.62 1.62 0.68 3 1.62 1.0 - 18Barium 41.7 43.4 41.8 178 334 62.4 95.4 90.8 3,100 47,000 90.8 - 95.4 50 - 1,000Cadmium <0.0320 <0.0314 <0.0316 <0.03850.205 J 0.0384 J 0.0805 J<0.03231.4 20<0.0323 - 0.0805 J1.0 - 10 Chromium (total) 78.2 5.46 4.74 19.3 16.4 30.7 68.9 59.7 NE NE 59.7 - 68.9 7.0 - 300Chromium (VI)0.864 1.160.397 0.234 J<0.1620.384 0.705 0.205 J 0.31 6.50 0.205 J - 0.705 NSChromium (III) 77.3 4.30 4.34 19.1 16.430.3 68.1 59.523,000 350,000 59.50 - 68.12 NSLead 7.61 7.15 6.79 10.7 88.4 10.8 17.1 8.92 400 800 8.92 - 17.1 ND - 50Mercury<0.0148 <0.0145 <0.01460.0399 J 0.0295 J 0.0353 0.0290 J 0.0219 J 4.7 70 0.0219 J - 0.0290 0.03 - 0.52Selenium 3.32 0.894 0.873 0.985 0.260 J 1.09 0.804 0.758 78 1,200 0.758 - 0.804 <0.1 - 0.8Silver 0.0469 J<0.0081 <0.00810.0274 J 0.0239 J 0.0173 J 0.0236 J 0.0162 J 78 1,200 0.0162 J - 0.0236 J ND - 5.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2023.2) Range values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005; Cd and Ag concentrations were taken from Southeastern and Conterminous U.S. Soils.Soil concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.Bold values exceed the Residential PSRGs and background levels in the case of metals. VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; UST = underground storage tank; ft bgs= feet below ground surface; NS = not specified; NE = not established; -- = not applicable; ND = not detected; NA = not analyzedJ = Compound was detected above laboratory method detection limit, but below laboratory reporting limit resulting in a laboratory estimated concentration. Screening Criteria Background Metals Site-Specific Range Published Range (2)mg/kgBackgroundResidential PSRGS (1)Industrial/Commercial PSRGS (1) GrabFormer/Suspect USTs Former Paint Storage BuildingsSB-2 / SB-DUP7/10/20234-6https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Tribek Properties/Wilkinson Boulevard Properties/Phase II ESA/Tables/data tablesTable 1 (Page 1 of 1)Hart & Hickman, PC
Table 2Summary of Well Construction and Groundwater Elevation DataFormer Ables AutoCharlotte, North CarolinaH&H Job No. TPI-002Well IDWell Diameter (inches) Total Well Depth (ft bgs)Screened Interval (ft bgs)Static Depth to Groundwater (ft bTOC)TOC Elevation (ft MSL)Groundwater Elevation (ft MSL)HH-TMW-1 2.0 25 10-25 16.29 740.73 724.44HH-TMW-2 2.0 23 8-23 15.51 741.56 726.05HH-TMW-3 2.0 25 10-25 17.19 742.34 725.15HH-TMW-4HH-TMW-5 2.0 25 10-25 20.19 742.75 722.56Notes:Depth to groundwater measurements were collected by H&H on July 14, 2023.Elevations were surveyed by H&H on July 14, 2023 relative to a known elevation of 741.96 ft MSL at a storm drain manhole (SDMH) located along the northern Site boundary near Wilkinson Boulevard. MSL = mean sea level; ft bgs = feet below ground surface; ft bTOC = feet below top of casing; HSA = hollow stem augerNot installed due to shallow HSA refusal https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Tribek Properties/Wilkinson Boulevard Properties/Phase II ESA/Tables/data tables9/14/2023Table 2 (Page 1 of 1)Hart & Hickman, PC
Table 3 Summary of Groundwater Analytical DataFormer Ables AutoCharlotte, North CarolinaH&H Job No. TPI-002Evaluation AreaUpgradient Downgradient QA/QCSample IDHH-TMW-1 HH-TMW-3 HH-TMW-5 Trip BlankDate7/14/2023 7/14/2023 7/14/2023 7/14/2023UnitsVOCs (8260D)Acetone<1.803.34 J 2.96 J<1.8016.3<1.806,000 NENEsec-Butylbenzene 1.78<0.200 <0.200 <0.200 <0.200 <0.20070 NE NEChlorobenzene 10.7<0.190 <0.190 <0.190 <0.190 <0.19050 82 340Chloroform 0.379 J 0.691 0.72716.5<0.220 <0.22070 0.81 3.61,4-Dichlorobenzene 0.951<0.210 <0.210 <0.210 <0.210 <0.21062.6114-Isopropyl toluene<0.0890.236 J 0.237 J<0.089 <0.089 <0.08925 NE NETetrachloroethene<0.220 <0.220 <0.2200.469 J <0.220 <0.2200.7 12 48SVOCs (8270E)Diethyl phthalate <0.7450.871 J 0.943 J<0.745 <0.745 NA6,000 NE NEMetals (6020B/7470A)Arsenic<0.297 <0.297 <0.297 <0.2970.421 JNA10 NE NEBarium 77.7 90.9 90.9 41.8 108NA700 NE NECadmium<0.350 <0.350 <0.350 <0.350 <0.350 NA2NENEChromium (Total) 0.481 J<0.346 <0.3460.387 J<0.346 NA10 NE NELead<0.264 <0.264 <0.264 <0.264 <0.264 NA15 NE NEMercury<0.13 <0.13 <0.13 <0.13 <0.13 NA1 0.18 0.75Selenium<0.703 <0.703 <0.703 <0.703 <0.703 NA20 NE NESilver<0.0570 <0.0570 <0.0570 <0.0570 <0.0570 NA20 NE NENotes:1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) dated April 2022.2) DEQ Vapor Intrusion Groundwater Screening Levels (GWSLs) dated July 2023. Concentrations are reported in micrograms per liter (µg/L).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.Bold values exceed the Residential Vapor Intrusion GWSL.Underlined values exceed the Non-Residential Vapor Intrusion GWSLs.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; NE = not established; NA = not analyzed; QA/QC = quality assurance/quality control J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. Downgradient of Former/Suspect USTs and Former Auto Repair OperationsScreening Criteria µg/L7/14/20232L Standards (1) Residential GWSLs (2)Non-Residential GWSLs (2)HH-TMW-2 / GW-DUPhttps://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Tribek Properties/Wilkinson Boulevard Properties/Phase II ESA/Tables/data tables10/11/2023Table 3 (Page 1 of 1)Hart & Hickman, PC
Table 4Summary of Soil Gas Analytical DataFormer Ables AutoCharlotte, North CarolinaH&H Job No. TPI-002Evaluation AreaFormer/Suspect UST AreaFormer Tire Recap BuildingEastern Portion of Site Sample IDSG-1 SG-3 SG-4 SG-5 SG-6 SG-7Sample Date7/12/2023 7/13/2023 7/13/2023 7/13/2023 7/12/2023 7/12/2023Sample Type UnitsVOCs (TO-15)Acetone 33.1 84.2 77.3 28.4 40.7 47.3 357 59.0 NE NEBenzene 4.3614.9 15.1 35.0 16.7 15.0 21.02.92 12 1601,3-Butadiene 1.44 1.966.59 22.8 14.3 24.2 29.6<0.3283.1 41Carbon Disulfide 18.1 32.5 31.5 176 42.9 46.4 70.9 6.29 4,900 61,000Chloroethane<0.164 <0.164 <0.164 <0.1641.20 J 0.303 J<0.164 <0.16428,000 350,000Chloroform33.7 44.5 42.8 16.00.761 J0.463 J0.497 J 0.434 J 4.1 53Cyclohexane<0.161 <0.161 <0.16110.3 8.95 13.0<0.1618.12 42,000 530,0001,4-Dichlorobenzene<0.186 <0.186 <0.186 <0.186 <0.1861.50 J<0.186 <0.1868.5 110Dichlorodifluoromethane 3.35 4.39 4.39 3.62 3.48 4.22 3.53 1.22 J 700 8,8001,1-Dichloroethane<0.101 <0.101 <0.101 <0.10128.6 1.53 J 11.7 1.31 J 58 770cis-1,2-Dichloroethene<0.095 <0.095 <0.095 <0.09527.5 5.54 2.28 0.535 J 280 3,500Ethyl Acetate<0.1360.526 J<0.136 <0.136 <0.1361.79 J<0.136 <0.136490 6,100Ethylbenzene 6.40 21.2 20.6 35.5 2.27 5.35 14.1 1.02 J 37 4904-Ethyltoluene 1.72 J 7.33 6.92 8.37 0.737 J 1.37 J 5.48<0.128NE NE1,1,2-Trichloro-1,2,2-trifluoroethane 0.582 J<0.5610.743 J 0.881 J 0.712 J 0.620 J 0.796 J<0.56135,000 440,000Heptane 13.0 16.4 16.8 155 21.4 35.1 36.7 10.3 2,800 35,000n-Hexane 10.0 5.03 4.53 24.8 37.9 22.6 19.1 13.1 4,900 61,0002-Hexanone<0.2853.33 3.24<0.285 <0.28521.5<0.285 <0.285210 2,600Isopropyl Alcohol 2.15 B, J 1.76 B, J 1.32 B, J 2.87 B, J 3.86 J 5.50 6.54 5.92 1,400 18,000Methyl Ethyl Ketone (MEK) 6.66 17.6 17.2 7.73 10.0 7.53 58.2 14.0 35,000 440,0004-Methyl-2-Pentanone 3.05 3.59 3.83 4.02 2.55 2.32 1.98 J 1.14 J 21,000 260,000Methylene Chloride 0.753 J 22.3 21.2 1.61 J 1.18 J 1.79 0.958 J<0.4883,400 53,000Naphthalene<0.183 <0.183 <0.1835.59 7.11<0.183 <0.183 <0.1832.8 36Propene 13.7 20.3 19.7 21.3 294 514 424 92.6 21,000 260,000Styrene 3.95 4.31<0.1244.26 4.36 4.17 4.19 4.16 7,000 8,800Tetrachloroethene 54.1 234 22248522.5 77.5 181 12.6 280 3,500Tetrahydrofuran 0.757 J 0.852 J 1.28 J 0.660 J 6.65 15.1 3.44 6.39 14,000 180,000Toluene 26.6 118 113 222 15.7 42.3 71.2 12.5 35,000 440,0001,1,1-Trichloroethane<0.1441.21 J 1.11 J 0.840 J 2.67 J<0.1440.878 J<0.14435,000 440,000Trichloroethene<0.199 <0.199 <0.199 <0.19924.7 15.72.59 2.00 J 14 180Trichlorofluoromethane 3.06 7.88 8.15 4.60 3.51 5.56 3.19 1.50 J NE NE1,2,4-Trimethylbenzene 5.57 25.8 25.0 27.9 3.34 6.44 21.4<0.110420 5,3001,3,5-Trimethylbenzene 1.43 J 6.64 6.35 8.27 0.963 J 2.22 J 4.94<0.236420 5,300Vinyl Chloride<0.127 <0.127 <0.127 <0.1275.47 3.68<0.127 <0.1275.6 280o-Xylene 6.74 25.4 24.8 37.1 2.49 7.23 20.6 4.49 700 8,800m&p-Xylene 22.8 63.9 61.9 101 8.49 17.1 43.4 5.47 J 700 8,800Notes:1) North Carolina Department of Environmental Quality (DEQ) Vapor Intrusion Sub-Slab & Exterior Soil Gas Screening Levels (SGSLs) dated July 2023.Concentrations are reported in micrograms per cubic meter (µg/m3).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses. Only compounds detected in at least one sample are shown in the above table.Bold values exceed the Residential Vapor Intrusion SGSL or unacceptable risk levels. VOCs = volatile organic compounds; NE = not establishedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.B = Analyte detected in laboratory blank. Exterior Soil Gasµg/m3Former Junk Storage Building Former Ables Auto Buildings Screening CriteriaSG-2/SG-DUPResidential SGSLs (1)Non-Residential SGSLs (1)7/13/2023https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Tribek Properties/Wilkinson Boulevard Properties/Phase II ESA/Tables/data tables10/11/2023Table 4 (Page 1 of 1)Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset, andNational Transportation Dataset; USGS Global Ecosystems; U.S. CensusBureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S.Department of State Humanitarian Information Unit; and NOAA NationalCenters for Environmental Information, U.S. Coastal Relief Model. Datarefreshed April, 2023.
SITE LOCATION MAP
FORMER ABLES AUTO2501,2511, AND 2533 WILKINSON BOULEVARDCHARLOTTE, NORTH CAROLINA
DATE: 9-12-23
JOB NO: TPI-002
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: S:\AAA-Master Projects\Tribek Properties\Wilkinson Boulevard Properties\Brownfields\Figures\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
CHARLOTTE WEST, NORTH CAROLINA 2022
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
FORMER BUILDING FOOTPRINT
FORMER ABLES BUILDING
FOOTPRINT
FORMER UST
POTENTIAL UST
JOB NO. TPI-002
REVISION NO. 0DATE: 9-12-23
FIGURE NO. 2
FORMER ABLES AUTO
2501, 2511, AND 2533 WILKINSON BOULEVARD
CHARLOTTE, NORTH CAROLINA
SITE AND HISTORICAL OPERATIONS MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
FORMER JUNK
STORAGE BUILDING
(1950 SANBORN MAP)
FORMER TIRE
RECAP BUILDING
(1950 SANBORN MAP)FORMER AUTO
REPAIR AND FOUNDARY
(1950 SANBORN MAP)
WILKINSON BOULEVA
R
D
REMOUNT ROADCAMP GREENE STREETSOUTHERN RAILWAY
VACANT
(2601 WILKINSON BLVD)
GRAYBAR ELECTRICAL SUPPLY
(2500 WILKINSON BLVD)
UNDEVELOPED
(2009 REMOUNT RD)
HEARTWOOD TREE SERVICE
(1622 PARKER RD)
RESIDENTIAL
ABM IMDUSTRIES
(2020 REMOUNT RD)
WESTSIDE AUTO SALES
(2479 WILKINSON BLVD)
FORMER STORAGE BUILDING
(1950 SANBORN MAP)
FORMER MACHINE SHOP
(1963 SANBORN MAP)
METAL PARTS AND
PAINT STORAGE
(1963 SANBORN MAP)
UNIDENTIFIED STORE
(1950 SANBORN MAP)
NOTES:
1. AERIAL IMAGERY AND BASE DATA OBTAINED FROM
MECKLENBURG COUNTY GIS, 2023.
2. FORMER BUILDING FOOTPRINTS BASED ON 1950 AND
1963 SANBORN MAPS.
3. UST = UNDERGROUND STORAGETANK
S:\AAA-Master Projects\Tribek Properties\Wilkinson Boulevard Properties\Brownfields\Figures\TPI.002_SITE.dwg, FIG 2, 6/23/2023 11:36:28 AM, bwest
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
FORMER BUILDING FOOTPRINT
FORMER ABLES AUTO BUILDING FOOTPRINT
FORMER UST
POTENTIAL UST
SOIL BORING
SOIL GAS MONITORING POINT
TEMPORARY MONITORING WELL
CO-LOCATED SOIL BORING AND SOIL GAS
POINT
CO-LOCATED SOIL BORING AND
TEMPORARY MONITORING WELL
PREVIOUS TEMPORARY MONITORING WELL
JOB NO. TPI-002
REVISION NO. 0DATE: 9-12-23
FIGURE NO. 3
FORMER ABLES AUTO
2501, 2511, AND 2533 WILKINSON BOULEVARD
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
WILKINSON BOULEVARD
REMOUNT ROADCAMP GREENE STREETSOUTHERN RAILWAY
GRAYBAR ELECTRICAL SUPPLY
(2500 WILKINSON BLVD)
SB-1
SB-4
SG-5/SB-5
SG-2/SB-3
BG-1
SG-1
HH-TMW-1 SG-4
SG-7
FORMER JUNK
STORAGE BUILDING
(1950 SANBORN MAP)
FORMER TIRE
RECAP BUILDING
(1950 SANBORN MAP)FORMER AUTO
REPAIR AND FOUNDARY
(1950 SANBORN MAP)
FORMER STORAGE BUILDING
(1950 SANBORN MAP)
FORMER MACHINE SHOP
(1963 SANBORN MAP)
UNIDENTIFIED STORE
(1950 SANBORN MAP)
NOTES:
1. AERIAL IMAGERY AND BASE DATA OBTAINED FROM
MECKLENBURG COUNTY GIS, 2023.
2. FORMER BUILDING FOOTPRINTS BASED ON 1950 AND
1963 SANBORN MAPS
3. PREVIOUS TEMPORARY MONITORING WELLS TMW-1 AND
TMW-2 WERE INSTALLED AND SAMPLED IN JUNE 2022.
4. UST = UNDERGROUND STORAGE TANK.
HH-TMW-5
BG-2
TMW-2
TMW-1
HH-TMW-3
SG-3
HH-TMW-2/SB-2
SG-6
FORMER ABLE'S AUTO FACILITY
S:\AAA-Master Projects\Tribek Properties\Wilkinson Boulevard Properties\Brownfields\Figures\TPI.002_SITE_230725.dwg, FIG 3, 7/25/2023 10:59:08 AM, kmckinney
FORMER ABLES AUTO
2501, 2511, AND 2533 WILKINSON BOULEVARD
CHARLOTTE, NORTH CAROLINA
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
GROUNDWATER ELEVATION (FT MSL)
GROUNDWATER ELEVATION CONTOUR (FT MSL)
DASHING INDICATES EXTRAPOLATED CONTOUR
INFERRED GROUNDWATER FLOW DIRECTION
PREVIOUS TEMPORARY MONITORING WELL
TEMPORARY MONITORING WELL
CO-LOCATED SOIL BORING AND TEMPORARY
MONITORING WELL LOCATION
JOB NO. TPI-002
REVISION NO. 0DATE: 9-13-23
FIGURE NO. 5
FORMER ABLES AUTO
2501, 2511, AND 2533 WILKINSON BOULEVARD
CHARLOTTE, NORTH CAROLINA
SHALLOW GROUNDWATER
POTENTIOMATRIC SURFACE MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
WILKINSON BOULEVARD
REMOUNT ROADCAMP GREENE STREETSOUTHERN RAILWAY
GRAYBAR ELECTRICAL SUPPLY
(2500 WILKINSON BLVD)
HH-TMW-1
NOTES:
1. AERIAL IMAGERY AND BASE DATA OBTAINED FROM
MECKLENBURG COUNTY GIS, 2023.
2. FT MSL = FEET ABOVE MEAN SEA LEVEL
3. PREVIOUS TEMPORARY MONITORING WELLS TMW-1 AND
TMW-2 WERE INSTALLED AND SAMPLED IN JUNE 2022.
4. ELEVATIONS WERE SURVEYED BY H&H ON JULY 14, 2023
RELATIVE TO A KNOWN ELEVATION OF 741.96 FT MSL AT
STORM DRAIN MANHOLE LOCATED IN WILKINSON
BOULEVARD.
HH-TMW-5
TMW-2
TMW-1
HH-TMW-3
HH-TMW-2/SB-2
723
(724.44)
(722.56)
(724.44)
(725.15)
(726.05)
723
724
725
725
724
723
S:\AAA-Master Projects\Tribek Properties\Wilkinson Boulevard Properties\Brownfields\Figures\TPI.002_SITE_20230804.dwg, FIG 5, 9/13/2023 12:58:17 PM, tmarbuery

Appendix A

Receptor Survey Form
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site: Former Ables Auto
Address: 2501, 2511, and 2533 Wilkinson Boulevard
City: Charlotte
County: Mecklenburg
Brownfields Project Number: 27027-23-060
Date 8/15/2023
Property and Building Characteristics
a. Provide occupancy and use information.
The Site is currently vacant land but was most recently utilized as an automotive repair facility.
No buildings presently on the Site.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
No buildings presently on the Site. There is a remnant concrete slab from a former building on
parcel 11701110.
No buildings presently on the Site.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
No buildings presently on the Site.
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as needed.
If numerous buildings are on-site, consult with your PM as only information on specific buildings may be needed.
b. Describe the construction of the building including materials (e.g. wood frame, block), type and size of openings (e.g.
windows, bay doors), and height (number of stories).
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and
design considerations (e.g. positive pressure?).
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information
requested below. Distances are measured from the site property boundary unless otherwise indicated by the DEQ
Brownfield’s Project Manager (PM).
Current Usage Proposed UsageSurface Conditions
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved
0%
0%
The Brownfields property will
be developed with multi-story
mixed use residential and
commercial buildings with
associated parking areas, access
roads, and landscaped areas
Size of Property (acres)
% of property that is wooded/brush
3.12
20%
70%
% of property that is covered by buildings
10%
Rev. 09/2015 Page 1 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
South
East
West
N
Y 130 SW
N
Utilities
Is there a septic system on-site? (Y or N) N
Please provide the utility providers for the subject property
a. Natural Gas Piedmont Natural Gas
b. Sewer City of Charlotte
c. Electricity Duke Energy
d. Other ____________________________
For surrounding properties, please complete the following table with available information.
YOn-Site~E-W
Y On-Site ~E-W
N----
Y On-Site ~N-S
Y On-Site ~E-W
Y On-Site ~E-WIs a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
Is a sanitary sewer within 100 ft of the Property boundary?
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject
property.
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
N - Overhead
Is there a residence within 1,000 ft of the Property?
Is there a basement within 1,000 ft of the Property
Proposed Usage Current Use/Occupant
1945 Remount Rd
Southern Railway and Industrial Manufacturing and
Logistics (ML-1 and ML-2)
Industrial Manufacturing and Logistics (ML-2)
Industrial Manufacturing and Logistics (ML-2)
Light Industrial (I-1)
Zoning/Land Use
For the subject property, please provide a map of known buried utilities. If available, include depth to top, construction
material, and diameter of the utilities. In addition, please provide the following information on utility providers. If additional
assessment is required, the public utility locators should be contacted. This information can then be added to a site map.
Y/N *
Is a school or daycare center within 1,000 ft of the Property?
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses.
Distance
(ft)
--
Utility/Potential Receptor Direction
--
NA
DirectionDistance
(ft)Address
Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding
areas. If specific receptors are present, please provide addresses of the facilities.
Rev. 09/2015 Page 2 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public X Private ______
Charlotte Water
N -- -- --
N -- -- --
N -- ----
Surface Water & Wetlands
Irwin Creek is located approximately 1,100 ft north of the Site.
No wetlands are present on the property.
b. List the uses of the water body.
c. What is the source of the water for the water body?
d. What is the nature of the bottom of the water body
(e.g., rocky or concrete bottom, drainage ways or
impoundments)
If no on-site surface water features, what is the nearest
surface water body?
Are there any wetlands present on the property? If no
wetlands on-site, are wetlands suspected on adjoining
properties?
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
No
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include
the water providers name.
a. Is the water body naturally developed or man-made?
AddressY/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a
windshield survey within 1,500 ft of the property boundaries should be completed to determine if water supply or irrigation
wells may be present. Information from applicable databases can and should be utilized; however, should not be utilized in
lieu of the windshield survey. If multiple wells are present within the requested radius, please provide a map of the well
locations. If needed, please attach a separate table to list all wells. Please note, the PM may opt for a more extensive water
supply well survey if needed.
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property boundary?
Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity
of the Property.
Are there surface water features on the property? (If yes,
please complete a. to d.)
Provide Information regarding Surface Water and
Wetlands
Distance
(ft)Direction
Rev. 09/2015 Page 3 of 3

Appendix B

Boring Logs & Well Construction and Abandonment Records
NOTES: Boring advanced using a hand auger. Grab sample collected from 1-3' bgs for analysis of RCRA metals and hexavalent chromium.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
BORING LOG
Boring No.
Page:
BG-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
07/11/2023
07/11/2023
IET
Hand Auger
Hand Auger
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL); vegetation
(0.5') SILT (ML); some fine-medium sand, medium stiff, moist, brown/red
(4') As Above: asphalt and gravel debris
(5') Boring terminated
0.0
0.0
0.1
BG-1(1-3)
0
5
10
NOTES: Boring advanced using a hand auger. Grab sample collected from 1-3' bgs for analysis of RCRA metals and hexavalent chromium.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
BORING LOG
Boring No.
Page:
BG-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
07/11/2023
07/11/2023
IET
Hand Auger
Hand Auger
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') ORGANIC SOIL (OL); vegetation
(0.5') SILT (ML); some fine-medium sand, medium stiff, moist, brown/red
(3') As Above: white and yellow mottling
(5') Boring terminated
1.9
3.8
3.5
BG-2(1-3)
0
5
10
NOTES: Boring hand cleared to 5' bgs using a hand auger. DPT to 15' bgs. HSA to 25' bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
WELL LOG
Well No.
Page:
HH-TMW-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
07/10/2023
07/10/2023
IET
Hand Auger/DPT/HSA
AMS-9520
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
25.0
8.00
DP, GR, HSA
17.2
16.29
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
25.0
2.0
0.100
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
GR
DP
HSA
(0') Asphalt, some gravel
(0.5') Silty SAND (SM); loose, moist, light yellow/brown
(2.5') As Above: few clay, faint oil smell
(7') SILT (ML); some medium sand, some clay, medium stiff, moist, light yellow,
orange and white mottling
(14') As Above: wet
(16') Lean CLAY (CL); some silt, medium plasticity, medium stiff, wet, light brown
(25') Boring terminated
0.2
0.9
1.3
0.9
0.7
0.6
1.1
0.8
1.2
0.9
1.1
0.7
0.6
0
5
10
15
20
25
30
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
NOTES: Boring hand cleared to 5' bgs using a hand auger. DPT to 15' bgs. HSA to 25' bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
WELL LOG
Well No.
Page:
HH-TMW-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
7/10/2023
7/11/2023
IET
Hand Auger/DPT/HSA
AMS-9520
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
25.0
8.00
DP, GR, HSA
18.0
17.19
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
25.0
2.0
0.100
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
GR
DP
HSA
GR
0.30 (0') ORGANIC SOIL (OL); vegetation
(0.5') Brick and concrete debris
(3.5') SILT (ML); some clay, medium stiff, moist, light brown
(5') Lean CLAY (CL); few fine sand, some silt, medium plasticity, medium stiff, moist,
light brown, tan and white mottling
(15') Fat CLAY (CH); few fine sand, some silt, high plasticity, medium stiff, wet, light
brown
(23') As Above: some coarse sand
(25') Boring terminated
1.1
1.3
1.2
1.1
1.0
1.2
1.3
1.1
0.8
1.5
2.0
1.5
1.6
0
5
10
15
20
25
30
NOTES: Boring hand cleared to 5 ' bgs using a hand auger. DPT to 15' bgs. HSA to 25' bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
WELL LOG
Well No.
Page:
HH-TMW-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
7/11/23
7/11/23
IET
Hand Auger/DPT/HSA
AMS-9520
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
25.0
8.00
DP, GR, HSA
24.5
20.19
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
2.0
0.100
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
GR
DP
HSA
(0') ORGANIC SOIL (OL); vegetation
(0.5') SILT (ML); some clay, medium stiff, moist, Brown/Red, asphalt debris
(7') As Above: gray staining, faint oil smell
(8') Asphalt
(9') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, dark gray,
asphalt debris, faint oil smell
(13') As Above: few medium-fine sand, wet, no staining or oil smell
(25') Boring terminated
3.6
4.3
2.5
4.5
3.3
4.1
5.3
6.7
7.3
5.0
5.1
6.3
2.4
0
5
10
15
20
25
30
25.0
NOTES: Boring hand cleared to 5' bgs using a hand aguer. DPT to 15' bgs . Grab soil sample collected from 8-10' bgs for analysis of VOCs, SVOCs, RCRA metals, and hexavalent chromium.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
7/10/23
7/10/23
IET
Hand Auger, Direct Push
AMS-9520
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
15.0
2.25
DP, GR
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
GR
DP
(0') Asphalt
(0.5') SILT (ML); some clay, medium stiff, moist, brown/red
(2') SILT (ML); some fine sand, some clay, medium stiff, moist, brown/light yellow, white
mottling
(9.5') SILT (ML); some clay, medium stiff, moist, black and white mottling
(12') Poorly graded SAND (SP); mostly coarse grained sand, some silt, some clay,
loose, wet, pink/white, black mottling, partially weathered rock
(15') Boring terminated
1.0
1.3
1.1
1.3
1.5
1.1
0.7
0.6
SB-1(8-10)
0
5
10
15
20
NOTES: NOTES: Boring hand cleared to 5' bgs using a hand aguer. DPT to 15' bgs . HSA to 23' bgs. Grab soil sample collected from
4-6' bgs for analysis of VOCs, SVOCs, RCRA metals, and hexavalent chromium.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
WELL LOG
Well No.
Page:
SB-2 / HH-TMW-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
23.0
8.00
DP, GR, HSA
13.0
15.51
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
23.0
2.0
0.100
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
GR
DP
HSA
(0') SILT (ML); some medium sand, medium stiff, moist, light brown
(2') SILT (ML); some medium sand, medium stiff, moist, light brown, white mottling,
gray staining, faint oil odor
(11') Poorly graded SAND (SP); some silt, loose, wet, white, some saprolite,
micaceous
(12') As Above: black mottling
(16') As Above: some brown clay
(23') Boring terminated
0.7
54.1
44.6
3.3
0.2
4.3
0.2
0.1
1.2
0.2
0.1
0.1
SB-2(4-6)
0
5
10
15
20
25
30
07/10/2023
07/10/2023
IET
Hand Auger/DPT/HSA
AMS-9520
TR White
AML
NOTES: Boring hand cleared to 5' bgs using a hand auger. Grab sample collected from 0-2' bgs for analysis of VOCs, SVOCs, RCRA metals,
and hexavalent chromium. DPT to 15' bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
SOIL BORING/SOIL GAS LOG
Well No.
Page:
SB-3/SG-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
7/12/2023
7/12/2023
IET
Hand Auger, Direct Push
AMS-9520
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
15.0
2.25
DP, GR
14.0
13.2
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
7.5
0.25
Teflon Tubing
Stainless Steel Wire Wrap
Bent. Powder
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
GR
DP
(0') ORGANIC SOIL (OL); vegetation
(0.5') SILT (ML); some clay, medium stiff, dry, light brown/red
(2') As Above: few fine gravel, some partially weathered rock
(4') Poorly graded GRAVEL (GP); some solid rock, concrete debris
(4.5') Well-graded SAND (SW); mostly fine-coarse grained sand, some silt, medium
dense, moist, light brown/red, partially weathered rock
(6') SILT (ML); some fine sand, some clay, soft, moist, light brown, red and white
mottling increasing with depth, saprolitic
(14') As Above: wet
(15') Boring terminated
4.0
5.3
5.4
5.3
4.5
2.8
2.8
1.0
SB-3(0-2)
0
5
10
15
20
NOTES: Boring hand cleared to 5' bgs using a hand auger. Grab sample collected from 8-10' bgs for analysis of VOCs, SVOCs, RCRA metals,
and hexavalent chromium. DPT to 15' bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
7/12/2023
7/12/2023
AMS-9520
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
15.0
DP, GR
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
GR
DP
(0') ORGANIC SOIL (OL); vegetation
(0.5') SILT (ML); some fine-medium sand, some clay, medium stiff, moist, brown/red,
asphalt debris
(2') Well-graded SAND (SW); some silt, some clay, medium dense, moist, white,
partially weathered rock
(3') SILT (ML); some fine-medium sand, some clay, medium stiff, moist, brown/red,
asphalt debris
(6') As Above: white mottling
(7') As Above: slight gray staining, faint oil odor
(8') As Above: thin layer of black material, slight black staining
(8.5') As Above: slight gray staining
(14') SILT (ML); some fine-medium sand, some clay, stiff, wet, white, partially
weathered rock
(15') Boring terminated
0.1
0.3
0.7
2.4
3.0
0.7
0.3
0.2
SB-4(8-10)
0
5
10
15
20
Hand Auger/DPT
TR White
2.25
13.91
13.00
IET
NOTES: Boring hand cleared to 5' bgs using a hand auger. Grab sample collected from 0-2' bgs for analysis of VOCs, SVOCs, RCRA metals,
and hexavalanet chromium. DPT to 15' bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
SOIL BORING/SOIL GAS LOG
Well No.
Page:
SB-5/SG-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
7/12/2023
7/12/2023
IET
Hand Auger, Direct Push
AMS-9520
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
2.25
DP, GR
13.0
12.2
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
7.5
0.25
Teflon Tubing
Stainless Steel Wire Wrap
Bent. Powder
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
GR
DP
(0') ORGANIC SOIL (OL); vegetation
(0.5') SILT (ML); some clay, soft, dry, brown/red
(1.5') SILT (ML); medium stiff, moist, white, partially weathered rock
(2') Lean CLAY (CL); few fine-coarse gravel, some silt, medium stiff, moist, brown,
asphalt debris
(7') As Above: interbedded with partially weathered rock
(8') As Above: slight gray staining, slight odor
(9') As Above: slight black staining, metal debris
0.3
0.4
0.3
1.3
2.4
2.2
1.2
1.8
SB-5(0-2)
0
5
10
15
20
15
NOTES: Boring hand cleared to 5' bgs using a hand auger. DPT to 7.5' bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
SOIL GAS LOG
Well No.
Page:
SG-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
07/10/2023
07/10/2023
IET
Hand Auger, Direct Push
AMS-9520
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
7.5
2.25
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
0.25
Teflon
Stainless Steel Wire Wrap
Bent. Powder
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Asphalt
(0.5') SILT (ML); some clay, medium stiff, moist, brown/red
(3') As Above: tan mottling
(6') As Above: brown/light yellow, tan mottling
(7.5') Boring terminated
0.2
0.4
0.3
0.6
0
5
10
7.5
DP, GR
GR
DP
NOTES: Boring hand cleared to 5' bgs using a hand auger. DPT to 7.5' bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
SOIL GAS LOG
Well No.
Page:
SG-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
07/12/2023
07/12/2023
IET
Hand Auger, Direct Push
AMS-9520
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
7.5
2.25
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
0.25
Teflon
Stainless Steel Wire Wrap
Bent. Powder
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') ORGANIC SOIL (OL); vegetation
(2') SILT (ML); some fine gravel, some clay, medium stiff, dry, light brown/red
(3') Poorly graded GRAVEL (GP); concrete debris
(3.5') Lean CLAY (CL); some silt, medium stiff, moist, light brown, red mottling
(7.5') Boring terminated
3.2
1.2
6.5
5.1
0
5
10
7.5
DP, GR
GR
DP
NOTES: Boring hand cleared to 5' bgs using a hand auger. DPT to 7.5' bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
SOIL GAS LOG
Well No.
Page:
SG-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
07/12/2023
07/12/2023
IET
Hand Auger, Direct Push
AMS-9520
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
7.5
2.25
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
0.25
Teflon
Stainless Steel Wire Wrap
Bent. Powder
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Poorly graded GRAVEL (GP)
(0.5') SILT (ML); some fine-medium sand, some clay, medium stiff, dry, brown,
asphalt debris
(3') SILT (ML); some clay, medium stiff, moist, light brown/yellow, white mottling
(7.5') Boring terminated
5.3
6.3
7.4
3.3
0
5
10
7.5
DP, GR
GR
DP
NOTES: Boring hand cleared to 5' bgs using hand auger. DPT to 7.5' bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
SOIL GAS LOG
Well No.
Page:
SG-6
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
07/11/2023
07/11/2023
IET
Hand Auger, Direct Push
AMS-9520
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
7.5
2.25
DP, GR
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
7.5
0.25
Teflon Tubing
Stainless Steel Wire Wrap
Bent. Powder
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR
DP
(0') ORGANIC SOIL (OL); vegetation
(0.5') SILT (ML); some fine-medium sand, medium stiff, moist, brown/red, yellow
mottling, asphalt debris
(3') As Above: brown
(6') Lean CLAY (CL); some silt, medium stiff, moist, brown, faint oil odor
(7.5') Boring terminated
0.9
4.3
3.0
1.2
0
5
10
NOTES: Boring hand cleared to 5' bgs using a hand auger. DPT to 7.5' bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Tribek Properties
TPI-002
2501 Wilkinson Blvd, Charlotte, NC
SOIL GAS LOG
Well No.
Page:
SG-7
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
7/11/2023
7/11/2023
IET
Hand Auger, Direct Push
AMS-9250
TR White
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
7.5
2.25
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
7.5
0.25
Stainless Steel Wire Wrap
Bent. Powder
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') ORGANIC SOIL (OL); vegetation
(0.5') SILT (ML); some medium-coarse sand, medium stiff, moist, brown/red
(6') As Above: asphalt debris, red and yellow mottling
(7') Organic matter
(7.5') Boring terminated
0.6
0.5
0.7
0.1
0
5
10
DP, GR
Teflon tubing
DP
GR
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
ertification:
ature of Certified Well Contracto
Terry White
3287-A one
1.5
IET
SIP70003149
40LB
7/19/2023
Bentonited holes from bottom to top. Capped with soil.
Former Ables Auto
2501 Wilkinson Blvd. Charlotte 28208 7/20/2023
Mecklenburg
35 13 25 80 53 02
TMW-1
25
8
14
NA
10
15
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): □Permanent or □Temporary
7. Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10. Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
ertification:
ure of Certified Well Contractor
i hi f I h b if
Terry White
3287-A
IET
SIP70003149
one
7/10/2023 TMW-1
Former Ables Auto
2501 Wilkinson Blvd. Charlotte 28208
Mecklenburg
35 13 25 80 53 02
25
14
8
Auger
7/20/2023
0 10 2 sch40 PVC
10 25 2 0.010 sch40 pvc
0
8
8
25
Bentonite
#2 Sand Poured
Poured/170LB
See Consultant Log
Prepack Screens used
Print Form
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
.Certification:
ignature of Certified Well Contr
Terry White
3287-A one
1.5
IET
SIP70003149
35LB
7/19/2023
Bentonited holes from bottom to top. Capped with soil.
Former Ables Auto
2501 Wilkinson Blvd. Charlotte 28208 7/20/2023
Mecklenburg
35 13 25 80 53 02
TMW-2
23
8
12
NA
8
15
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): □Permanent or □Temporary
7. Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10. Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Certification:
nature of Certified Well Contrac
ii thif Ih b t
Terry White
3287-A
IET
SIP70003149
one
7/10/2023 TMW-2
Former Ables Auto
2501 Wilkinson Blvd. Charlotte 28208
Mecklenburg
35 13 25 80 53 02
23
12
8
Auger
7/20/2023
0 8 2 sch40 PVC
8 23 2 0.010 sch40 pvc
0
6
6
23
Bentonite
#2 Sand Poured
Poured/135LB
See Consultant Log
Prepack Screens used
Print Form
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
ification:
e of Certified Well Contractor or
Terry White
3287-A one
1
IET
SIP70003149
40LB
7/19/2023
Bentonited holes from bottom to top. Capped with soil.
Former Ables Auto
2501 Wilkinson Blvd. Charlotte 28208 7/20/2023
Mecklenburg
35 13 25 80 53 02
TMW-3
25
8
18
NA
10
15
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): □Permanent or □Temporary
7. Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10. Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
.Certification:
gnature of Certified Well Contra
Terry White
3287-A
IET
SIP70003149
one
7/11/2023 TMW-3
Former Ables Auto
2501 Wilkinson Blvd. Charlotte 28208
Mecklenburg
35 13 25 80 53 02
25
18
8
Auger
7/20/2023
0 10 2 sch40 PVC
10 25 2 0.010 sch40 pvc
0
8
8
25
Bentonite
#2 Sand Poured
Poured/175LB
See Consultant Log
Prepack Screens used
Print Form
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
8.Certification:
Signature of Certified Well Con
Terry White
3287-A one
0.4
IET
SIP70003149
40LB
7/19/2023
Bentonited holes from bottom to top. Capped with soil.
Former Ables Auto
2501 Wilkinson Blvd. Charlotte 28208 7/20/2023
Mecklenburg
35 13 25 80 53 02
TMW-5
25
8
24
NA
10
15
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): □Permanent or □Temporary
7. Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10. Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Certification:
ture of Certified Well Contracto
Terry White
3287-A
IET
SIP70003149
one
7/11/2023 TMW-5
Former Ables Auto
2501 Wilkinson Blvd. Charlotte 28208
Mecklenburg
35 13 25 80 53 02
25
24
8
Auger
7/20/2023
0 10 2 sch40 PVC
10 25 2 0.010 sch40 pvc
0
8
8
25
Bentonite
#2 Sand Poured
Poured/175LB
See Consultant Log
Prepack Screens used
Print Form

Appendix C

Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

8/2/2023
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 23-198-0001 Client Project Description: TPI-002
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/14/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 151
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/29/202440750State ProgramAlabama
02/07/202488-0650State ProgramArkansas
06/30/20242904State ProgramCalifornia
06/30/2024E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202404015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202480215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202404015State Program - NELAPLouisiana
11/14/2025MSState ProgramMississippi
07/31/202447701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202468-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2023T104704180State Program - NELAPTexas
06/30/202400106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/23-198-0001
Page 2 of 151
Report Number:
Sample Summary Table
Client Project Description:
23-198-0001
TPI-002
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
07/10/2023 14:20Solids 89735 SB-1 07/14/2023 14:55
07/10/2023 14:20Solids 89735 SB-1 07/14/2023 14:55 SW-7199 WP MTN -
07/10/2023 14:20Solids 89735 SB-1 07/14/2023 14:55 6020B WP MTN -
07/10/2023 14:05Solids 89736 SB-2 07/14/2023 14:55
07/10/2023 14:05Solids 89736 SB-2 07/14/2023 14:55 SW-7199 WP MTN -
07/10/2023 14:05Solids 89736 SB-2 07/14/2023 14:55 6020B WP MTN -
07/12/2023 11:45Solids 89737 SB-3 07/14/2023 14:55
07/12/2023 11:45Solids 89737 SB-3 07/14/2023 14:55 6020B WP MTN -
07/12/2023 11:45Solids 89737 SB-3 07/14/2023 14:55 SW-7199 WP MTN -
07/12/2023 09:35Solids 89738 SB-4 07/14/2023 14:55
07/12/2023 09:35Solids 89738 SB-4 07/14/2023 14:55 SW-7199 WP MTN -
07/12/2023 09:35Solids 89738 SB-4 07/14/2023 14:55 6020B WP MTN -
07/12/2023 10:35Solids 89739 SB-5 07/14/2023 14:55
07/12/2023 10:35Solids 89739 SB-5 07/14/2023 14:55 SW-7199 WP MTN -
07/12/2023 10:35Solids 89739 SB-5 07/14/2023 14:55 6020B WP MTN -
07/10/2023Solids 89740 SB-Dup 07/14/2023 14:55
07/10/2023Solids 89740 SB-Dup 07/14/2023 14:55 SW-7199 WP MTN -
07/10/2023Solids 89740 SB-Dup 07/14/2023 14:55 6020B WP MTN -
07/11/2023 15:40Solids 89741 BG-1 07/14/2023 14:55
07/11/2023 15:40Solids 89741 BG-1 07/14/2023 14:55 SW-7199 WP MTN -
07/11/2023 15:40Solids 89741 BG-1 07/14/2023 14:55 6020B WP MTN -
07/11/2023 15:50Solids 89742 BG-2 07/14/2023 14:55
07/11/2023 15:50Solids 89742 BG-2 07/14/2023 14:55 SW-7199 WP MTN -
07/11/2023 15:50Solids 89742 BG-2 07/14/2023 14:55 6020B WP MTN -
07/14/2023Aqueous 89743 GW-DUP 07/14/2023 14:55
07/14/2023Aqueous 89743 GW-DUP 07/14/2023 14:55 7470A WP MTN -
07/14/2023Aqueous 89743 GW-DUP 07/14/2023 14:55 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 151
Report Number:
Sample Summary Table
Client Project Description:
23-198-0001
TPI-002
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
07/14/2023 15:05Aqueous 89744 HH-TMW-1 07/14/2023 14:55
07/14/2023 15:05Aqueous 89744 HH-TMW-1 07/14/2023 14:55 7470A WP MTN -
07/14/2023 15:05Aqueous 89744 HH-TMW-1 07/14/2023 14:55 6020B WP MTN -
07/14/2023 13:40Aqueous 89745 HH-TMW-2 07/14/2023 14:55
07/14/2023 13:40Aqueous 89745 HH-TMW-2 07/14/2023 14:55 7470A WP MTN -
07/14/2023 13:40Aqueous 89745 HH-TMW-2 07/14/2023 14:55 6020B WP MTN -
07/14/2023 12:35Aqueous 89746 HH-TMW-3 07/14/2023 14:55
07/14/2023 12:35Aqueous 89746 HH-TMW-3 07/14/2023 14:55 7470A WP MTN -
07/14/2023 12:35Aqueous 89746 HH-TMW-3 07/14/2023 14:55 6020B WP MTN -
07/14/2023 11:10Aqueous 89747 HH-TMW-5 07/14/2023 14:55
07/14/2023 11:10Aqueous 89747 HH-TMW-5 07/14/2023 14:55 7470A WP MTN -
07/14/2023 11:10Aqueous 89747 HH-TMW-5 07/14/2023 14:55 6020B WP MTN -
07/14/2023Aqueous 89748 Trip Blank 07/14/2023 14:55
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 4 of 151
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0001
Report Limit
Project:TPI-002
V 89735SB-1
1.57 07/21/2023 16:426020BArsenicmg/Kg - dry 0.105
41.7 07/21/2023 16:426020BBariummg/Kg - dry 0.052
78.2 07/21/2023 16:426020BChromiummg/Kg - dry 0.143
7.61 07/21/2023 16:426020BLeadmg/Kg - dry 0.0382
3.32 07/21/2023 16:426020BSeleniummg/Kg - dry 0.127
J0.0469 07/21/2023 16:426020BSilvermg/Kg - dry 0.0083
J0.001 07/17/2023 15:008260Dn-Hexane mg/Kg - dry 0.0008
J0.006 07/17/2023 15:008260DMethylene Chloride mg/Kg - dry 0.001
0.864 07/31/2023 17:10SW-7199 Chromium, Hexavalent mg/Kg - dry 0.173
18.9 07/18/2023 18:45SW-DRYWT Moisture %
V 89736SB-2
0.372 07/21/2023 16:466020BArsenicmg/Kg - dry 0.103
43.4 07/21/2023 16:466020BBariummg/Kg - dry 0.051
5.46 07/21/2023 16:466020BChromiummg/Kg - dry 0.140
7.15 07/21/2023 16:466020BLeadmg/Kg - dry 0.0374
0.894 07/21/2023 16:466020BSeleniummg/Kg - dry 0.124
J0.006 07/18/2023 15:168260DAcetonemg/Kg - dry 0.002
0.008 07/18/2023 15:168260Dn-Butylbenzene mg/Kg - dry 0.0006
0.017 07/18/2023 15:168260Dsec-Butyl benzene mg/Kg - dry 0.0007
J0.001 07/18/2023 15:168260DCarbon Disulfide mg/Kg - dry 0.0008
J0.001 07/18/2023 15:168260DEthylbenzenemg/Kg - dry 0.0007
J0.003 07/18/2023 15:168260DIsopropylbenzenemg/Kg - dry 0.0006
J0.004 07/18/2023 15:168260D4-Isopropyl toluene mg/Kg - dry 0.001
J0.003 07/18/2023 15:168260DMethylene Chloride mg/Kg - dry 0.001
0.063 07/18/2023 15:168260DNaphthalenemg/Kg - dry 0.001
0.009 07/18/2023 15:168260Dn-Propylbenzene mg/Kg - dry 0.0007
0.035 07/18/2023 15:168260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.004 07/18/2023 15:168260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J31907/20/2023 01:538270E1-Methylnaphthalene µg/Kg - dry 128
J16307/20/2023 01:538270E2-Methylnaphthalene µg/Kg - dry 121
1.16 07/31/2023 17:53SW-7199 Chromium, Hexavalent mg/Kg - dry 0.170
17.2 07/18/2023 18:45SW-DRYWT Moisture %
V 89737SB-3
1.22 07/21/2023 16:506020BArsenicmg/Kg - dry 0.127
178 07/21/2023 16:506020BBariummg/Kg - dry 0.063
19.3 07/21/2023 16:506020BChromiummg/Kg - dry 0.171
Page 5 of 151
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0001
Report Limit
Project:TPI-002
V 89737SB-3
10.7 07/21/2023 16:506020BLeadmg/Kg - dry 0.0459
0.985 07/21/2023 16:506020BSeleniummg/Kg - dry 0.152
J0.0274 07/21/2023 16:506020BSilvermg/Kg - dry 0.0099
J0.0399 07/19/2023 16:187471BMercury (Total)mg/Kg - dry 0.0178
0.090 07/17/2023 15:278260DAcetonemg/Kg - dry 0.003
J0.003 07/17/2023 15:278260Dn-Hexane mg/Kg - dry 0.001
J0.017 07/17/2023 15:278260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.001
J0.008 07/17/2023 15:278260DMethylene Chloride mg/Kg - dry 0.002
J0.234 07/31/2023 18:04SW-7199 Chromium, Hexavalent mg/Kg - dry 0.208
32.5 07/18/2023 18:45SW-DRYWT Moisture %
V 89738SB-4
1.04 07/21/2023 16:546020BArsenicmg/Kg - dry 0.0982
334 07/21/2023 16:546020BBariummg/Kg - dry 0.049
J0.205 07/21/2023 16:546020BCadmiummg/Kg - dry 0.0298
16.4 07/21/2023 16:546020BChromiummg/Kg - dry 0.133
88.4 07/21/2023 16:546020BLeadmg/Kg - dry 0.0356
J0.260 07/21/2023 16:546020BSeleniummg/Kg - dry 0.118
J0.0239 07/21/2023 16:546020BSilvermg/Kg - dry 0.0077
J0.0295 07/19/2023 16:207471BMercury (Total)mg/Kg - dry 0.0138
J0.007 07/17/2023 15:548260DAcetonemg/Kg - dry 0.002
J0.0010 07/17/2023 15:548260DCarbon Disulfide mg/Kg - dry 0.0007
J0.001 07/17/2023 15:548260DChloroethanemg/Kg - dry 0.001
J0.0010 07/17/2023 15:548260Dn-Hexane mg/Kg - dry 0.0008
J0.003 07/17/2023 15:548260DMethylene Chloride mg/Kg - dry 0.001
13.0 07/18/2023 18:45SW-DRYWT Moisture %
V 89739SB-5
1.06 07/21/2023 16:586020BArsenicmg/Kg - dry 0.0977
62.4 07/21/2023 16:586020BBariummg/Kg - dry 0.048
J0.0384 07/21/2023 16:586020BCadmiummg/Kg - dry 0.0297
30.7 07/21/2023 16:586020BChromiummg/Kg - dry 0.132
10.8 07/21/2023 16:586020BLeadmg/Kg - dry 0.0354
1.09 07/21/2023 16:586020BSeleniummg/Kg - dry 0.117
J0.0173 07/21/2023 16:586020BSilvermg/Kg - dry 0.0077
0.0353 07/19/2023 16:237471BMercury (Total)mg/Kg - dry 0.0137
0.035 07/17/2023 16:228260DAcetonemg/Kg - dry 0.002
J0.003 07/17/2023 16:228260DMethylene Chloride mg/Kg - dry 0.001
Page 6 of 151
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0001
Report Limit
Project:TPI-002
V 89739SB-5
J20107/21/2023 15:118270EBenzo(a)anthracene µg/Kg - dry 159
J23207/21/2023 15:118270EBenzo(a)pyrene µg/Kg - dry 168
J32507/21/2023 15:118270EBenzo(b)fluoranthene µg/Kg - dry 167
J18407/21/2023 15:118270EChryseneµg/Kg - dry 162
J29607/21/2023 15:118270EFluorantheneµg/Kg - dry 141
J30307/21/2023 15:118270EPyreneµg/Kg - dry 153
0.384 07/31/2023 18:26SW-7199 Chromium, Hexavalent mg/Kg - dry 0.161
12.5 07/18/2023 18:45SW-DRYWT Moisture %
V 89740SB-Dup
0.339 07/21/2023 17:026020BArsenicmg/Kg - dry 0.104
41.8 07/21/2023 17:026020BBariummg/Kg - dry 0.052
4.74 07/21/2023 17:026020BChromiummg/Kg - dry 0.141
6.79 07/21/2023 17:026020BLeadmg/Kg - dry 0.0377
0.873 07/21/2023 17:026020BSeleniummg/Kg - dry 0.125
J0.007 07/17/2023 16:498260DAcetonemg/Kg - dry 0.002
0.016 07/17/2023 16:498260Dn-Butylbenzene mg/Kg - dry 0.0006
0.036 07/17/2023 16:498260Dsec-Butyl benzene mg/Kg - dry 0.0007
J0.0007 07/17/2023 16:498260Dtert-Butyl benzene mg/Kg - dry 0.0006
J0.002 07/17/2023 16:498260DCarbon Disulfide mg/Kg - dry 0.0008
J0.002 07/17/2023 16:498260DEthylbenzenemg/Kg - dry 0.0007
J0.001 07/17/2023 16:498260Dn-Hexane mg/Kg - dry 0.0008
0.008 07/17/2023 16:498260DIsopropylbenzenemg/Kg - dry 0.0006
0.009 07/17/2023 16:498260D4-Isopropyl toluene mg/Kg - dry 0.001
J0.006 07/17/2023 16:498260DMethylene Chloride mg/Kg - dry 0.001
0.101 07/17/2023 16:498260DNaphthalenemg/Kg - dry 0.001
0.020 07/17/2023 16:498260Dn-Propylbenzene mg/Kg - dry 0.0007
0.078 07/17/2023 16:498260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
0.009 07/17/2023 16:498260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J46007/20/2023 01:068270E1-Methylnaphthalene µg/Kg - dry 129
J21707/20/2023 01:068270E2-Methylnaphthalene µg/Kg - dry 122
J25807/20/2023 01:068270EPhenanthreneµg/Kg - dry 253
0.397 07/31/2023 18:37SW-7199 Chromium, Hexavalent mg/Kg - dry 0.171
17.8 07/19/2023 11:50SW-DRYWT Moisture %
V 89741BG-1
1.62 07/21/2023 17:066020BArsenicmg/Kg - dry 0.0990
95.4 07/21/2023 17:066020BBariummg/Kg - dry 0.049
Page 7 of 151
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0001
Report Limit
Project:TPI-002
V 89741BG-1
J0.0805 07/21/2023 17:066020BCadmiummg/Kg - dry 0.0301
68.9 07/21/2023 17:066020BChromiummg/Kg - dry 0.134
17.1 07/21/2023 17:066020BLeadmg/Kg - dry 0.0359
0.804 07/21/2023 17:066020BSeleniummg/Kg - dry 0.119
J0.0236 07/21/2023 17:066020BSilvermg/Kg - dry 0.0078
J0.0290 07/19/2023 16:287471BMercury (Total)mg/Kg - dry 0.0139
0.705 07/31/2023 18:48SW-7199 Chromium, Hexavalent mg/Kg - dry 0.163
13.7 07/19/2023 18:30SW-DRYWT Moisture %
V 89742BG-2
1.62 07/21/2023 17:106020BArsenicmg/Kg - dry 0.106
90.8 07/21/2023 17:106020BBariummg/Kg - dry 0.053
59.7 07/21/2023 17:106020BChromiummg/Kg - dry 0.144
8.92 07/21/2023 17:106020BLeadmg/Kg - dry 0.0385
0.758 07/21/2023 17:106020BSeleniummg/Kg - dry 0.128
J0.0162 07/21/2023 17:106020BSilvermg/Kg - dry 0.0083
J0.0219 07/19/2023 16:367471BMercury (Total)mg/Kg - dry 0.0149
J0.205 07/31/2023 19:21SW-7199 Chromium, Hexavalent mg/Kg - dry 0.175
19.6 07/19/2023 18:30SW-DRYWT Moisture %
V 89743GW-DUP
90.9 07/21/2023 21:576020BBariumµg/L 0.453
J2.96 07/21/2023 21:248260DAcetoneµg/L 1.80
0.727 07/21/2023 21:248260DChloroformµg/L 0.220
J0.237 07/21/2023 21:248260D4-Isopropyl toluene µg/L 0.089
J0.943 07/21/2023 15:348270EDiethyl phthalate µg/L 0.745
V 89744HH-TMW-1
77.7 07/21/2023 22:086020BBariumµg/L 0.453
J0.481 07/21/2023 22:086020BChromiumµg/L 0.346
1.78 07/21/2023 21:498260Dsec-Butyl benzene µg/L 0.200
10.7 07/21/2023 21:498260DChlorobenzeneµg/L 0.190
J0.379 07/21/2023 21:498260DChloroformµg/L 0.220
0.951 07/21/2023 21:498260D1,4-Dichlorobenzene µg/L 0.210
V 89745HH-TMW-2
90.9 07/21/2023 22:126020BBariumµg/L 0.453
J3.34 07/21/2023 22:148260DAcetoneµg/L 1.80
Page 8 of 151
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0001
Report Limit
Project:TPI-002
V 89745HH-TMW-2
0.691 07/21/2023 22:148260DChloroformµg/L 0.220
J0.236 07/21/2023 22:148260D4-Isopropyl toluene µg/L 0.089
J0.871 07/21/2023 16:438270EDiethyl phthalate µg/L 0.745
V 89746HH-TMW-3
41.8 07/21/2023 22:166020BBariumµg/L 0.453
J0.387 07/21/2023 22:166020BChromiumµg/L 0.346
16.5 07/21/2023 22:388260DChloroformµg/L 0.220
J0.469 07/21/2023 22:388260DTetrachloroetheneµg/L 0.220
V 89747HH-TMW-5
J0.421 07/21/2023 22:206020BArsenicµg/L 0.297
108 07/21/2023 22:206020BBariumµg/L 0.453
16.3 07/21/2023 23:038260DAcetoneµg/L 1.80
Page 9 of 151

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: TPI-002 Lab Report Number: 23-198-0001
Date: 8/1/2023
Metals Analyses Method 6020B Sample 82670 (Digester #3) Analyte: Barium
QC Batch No: L694733/L693937 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected. Hexavalent Chromium by Ion Chromatography Method SW-7199 Analyte: Hexavalent Chromium
QC Batch No: L694239 Matrix Spike Recovery Low: A measure of the sample pH and its oxidation reduction potential (ORP) indicate that
the sample has reducing qualities which may not allow for the presence of Hexavalent Chromium. Total Aqueous Mercury Analysis - CVAA Method 7470A Sample 89747 (HH-TMW-5)
Analyte: Mercury QC Batch No: L693993/L693779
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected. Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: 2,4-Dinitrophenol
QC Batch No: V35527/V35515 Refer to LCS/LCSD.
Analyte: 2,4-Dinitrophenol
QC Batch No: V35527/V35515 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Aniline
QC Batch No: V35527/V35515 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Benzoic Acid
QC Batch No: V35527/V35515 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Analyte: Pyridine QC Batch No: V35550/V35515
Page 10 of 151

Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 89743 (GW-DUP)
Analyte: 2-Fluorobiphenyl QC Batch No: V35550/V35516
Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all
showed surrogates within QC limits.
Sample 89743 (GW-DUP) Analyte: 4-Terphenyl-d14
QC Batch No: V35550/V35516 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Sample 89744 (HH-TMW-1)
Analyte: Nitrobenzene-d5 QC Batch No: V35550/V35516
Surrogate(s) was flagged for low recovery in this project sample. This sample will be re-analyzed for verification. Surrogate is low. Associated QC is passing. No further action taken.

Page 11 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-1
89735 Matrix:
7/10/2023 14:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.9 %Moisture 1 07/18/23 18:45 SW-DRYWTCNC
0.864 mg/Kg - dry 0.173 0.246Chromium, Hexavalent 1 07/31/23 17:10 SW-7199SWB
1.57 mg/Kg - dry 0.105 0.308Arsenic 5 07/21/23 16:42 6020BCPW
41.7 mg/Kg - dry 0.052 0.308Barium 5 07/21/23 16:42 6020BCPW
<0.0320 mg/Kg - dry 0.0320 0.308Cadmium 5 07/21/23 16:42 6020BCPW
78.2 mg/Kg - dry 0.143 0.308
Chromium 5 07/21/23 16:42 6020BCPW
7.61 mg/Kg - dry 0.0382 0.308Lead 5 07/21/23 16:42 6020BCPW
<0.0148 mg/Kg - dry 0.0148 0.0370Mercury (Total)1 07/19/23 16:12 7471BJKC
3.32 mg/Kg - dry 0.127 0.308Selenium 5 07/21/23 16:42 6020BCPW
0.0469 J mg/Kg - dry 0.0083 0.308Silver 5 07/21/23 16:42 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-1
89735 Matrix:
7/10/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00 V35515 07/19/23 09:50
<0.002 mg/Kg - dry 0.002 0.024Acetone 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 07/17/23 15:00 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 07/17/23 15:00 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 07/17/23 15:00 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 07/17/23 15:00 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 07/17/23 15:00 V35423TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 07/17/23 15:00 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 07/17/23 15:00 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 07/17/23 15:00 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 07/17/23 15:00 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 07/17/23 15:00 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 07/17/23 15:00 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 07/17/23 15:00 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 07/17/23 15:00 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 07/17/23 15:00 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 07/17/23 15:00 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-1
89735 Matrix:
7/10/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00 V35515 07/19/23 09:50
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 07/17/23 15:00 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 07/17/23 15:00 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 07/17/23 15:00 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 07/17/23 15:00 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 07/17/23 15:00 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 07/17/23 15:00 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 07/17/23 15:00 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 07/17/23 15:00 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 07/17/23 15:00 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 07/17/23 15:00 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 07/17/23 15:00 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 07/17/23 15:00 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 07/17/23 15:00 V35423TBL
<0.017 mg/Kg - dry 0.017 0.308Ethanol 1 07/17/23 15:00 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 07/17/23 15:00 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 07/17/23 15:00 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-1
89735 Matrix:
7/10/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00 V35515 07/19/23 09:50
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 07/17/23 15:00 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 07/17/23 15:00 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 07/17/23 15:00 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 07/17/23 15:00 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 07/17/23 15:00 V35423TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 07/17/23 15:00 V35423TBL
0.006 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 07/17/23 15:00 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 07/17/23 15:00 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 07/17/23 15:00 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 07/17/23 15:00 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 07/17/23 15:00 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 07/17/23 15:00 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 07/17/23 15:00 V35423TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 07/17/23 15:00 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 07/17/23 15:00 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-1
89735 Matrix:
7/10/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00 V35515 07/19/23 09:50
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 07/17/23 15:00 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 07/17/23 15:00 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 07/17/23 15:00 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 07/17/23 15:00 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 07/17/23 15:00 V35423TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 07/17/23 15:00 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 07/17/23 15:00 V35423
Surrogate: 4-Bromofluorobenzene 98.5 Limits: 70-130%07/17/23 15:001 TBL V35423
Surrogate: Dibromofluoromethane 104 Limits: 84-123%07/17/23 15:001 TBL V35423
Surrogate: Toluene-d8 98.7 Limits: 76-129%07/17/23 15:001 TBL V35423
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<143 µg/Kg - dry 143 814Acenaphthene 1 07/19/23 19:20 V35527AMP
<129 µg/Kg - dry 129 814Acenaphthylene 1 07/19/23 19:20 V35527AMP
<187 µg/Kg - dry 187 814Aniline 1 07/19/23 19:20 V35527AMP
<176 µg/Kg - dry 176 814Anthracene 1 07/19/23 19:20 V35527AMP
<171 µg/Kg - dry 171 814
Benzo(a)anthracene 1 07/19/23 19:20 V35527AMP
<181 µg/Kg - dry 181 814Benzo(a)pyrene 1 07/19/23 19:20 V35527AMP
<180 µg/Kg - dry 180 814Benzo(b)fluoranthene 1 07/19/23 19:20 V35527AMP
<168 µg/Kg - dry 168 814Benzo(g,h,i)perylene 1 07/19/23 19:20 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-1
89735 Matrix:
7/10/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<169 µg/Kg - dry 169 814Benzo(k)fluoranthene 1 07/19/23 19:20 V35527AMP
<715 µg/Kg - dry 715 2470
Benzoic Acid 1 07/19/23 19:20 V35527AMP
<129 µg/Kg - dry 129 814Benzyl alcohol 1 07/19/23 19:20 V35527AMP
<145 µg/Kg - dry 145 814Bis(2-Chloroethoxy)methane 1 07/19/23 19:20 V35527AMP
<132 µg/Kg - dry 132 814Bis(2-Chloroethyl)ether 1 07/19/23 19:20 V35527AMP
<168 µg/Kg - dry 168 407Bis(2-Chloroisopropyl)ether 1 07/19/23 19:20 V35527AMP
<148 µg/Kg - dry 148 814Bis(2-ethylhexyl)phthalate 1 07/19/23 19:20 V35527AMP
<134 µg/Kg - dry 134 8144-Bromophenyl phenyl ether 1 07/19/23 19:20 V35527AMP
<139 µg/Kg - dry 139 407
Butyl benzyl phthalate 1 07/19/23 19:20 V35527AMP
<114 µg/Kg - dry 114 8144-Chloro-3-methylphenol 1 07/19/23 19:20 V35527AMP
<138 µg/Kg - dry 138 4074-Chloroaniline 1 07/19/23 19:20 V35527AMP
<143 µg/Kg - dry 143 8142-Chloronaphthalene 1 07/19/23 19:20 V35527AMP
<121 µg/Kg - dry 121 8142-Chlorophenol 1 07/19/23 19:20 V35527AMP
<155 µg/Kg - dry 155 12304-Chlorophenyl phenyl ether 1 07/19/23 19:20 V35527AMP
<175 µg/Kg - dry 175 814Chrysene 1 07/19/23 19:20 V35527AMP
<284 µg/Kg - dry 284 814Dibenz(a,h)anthracene 1 07/19/23 19:20 V35527AMP
<147 µg/Kg - dry 147 814Dibenzofuran 1 07/19/23 19:20 V35527AMP
<116 µg/Kg - dry 116 8141,2-Dichlorobenzene 1 07/19/23 19:20 V35527AMP
<120 µg/Kg - dry 120 8141,3-Dichlorobenzene 1 07/19/23 19:20 V35527AMP
<120 µg/Kg - dry 120 4071,4-Dichlorobenzene 1 07/19/23 19:20 V35527AMP
<181 µg/Kg - dry 181 8143,3'-Dichlorobenzidine 1 07/19/23 19:20 V35527AMP
<118 µg/Kg - dry 118 8142,4-Dichlorophenol 1 07/19/23 19:20 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-1
89735 Matrix:
7/10/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<222 µg/Kg - dry 222 814Diethyl phthalate 1 07/19/23 19:20 V35527AMP
<215 µg/Kg - dry 215 814
Dimethyl phthalate 1 07/19/23 19:20 V35527AMP
<133 µg/Kg - dry 133 4072,4-Dimethylphenol 1 07/19/23 19:20 V35527AMP
<132 µg/Kg - dry 132 814Di-n-butyl phthalate 1 07/19/23 19:20 V35527AMP
<296 µg/Kg - dry 296 18504,6-Dinitro-2-methylphenol 1 07/19/23 19:20 V35527AMP
<641 µg/Kg - dry 641 18502,4-Dinitrophenol 1 07/19/23 19:20 V35527AMP
<119 µg/Kg - dry 119 8142,4-Dinitrotoluene 1 07/19/23 19:20 V35527AMP
<133 µg/Kg - dry 133 8142,6-Dinitrotoluene 1 07/19/23 19:20 V35527AMP
<176 µg/Kg - dry 176 407
Di-n-Octyl Phthalate 1 07/19/23 19:20 V35527AMP
<152 µg/Kg - dry 152 814Fluoranthene 1 07/19/23 19:20 V35527AMP
<158 µg/Kg - dry 158 814Fluorene 1 07/19/23 19:20 V35527AMP
<131 µg/Kg - dry 131 814Hexachlorobenzene 1 07/19/23 19:20 V35527AMP
<120 µg/Kg - dry 120 814Hexachlorobutadiene 1 07/19/23 19:20 V35527AMP
<194 µg/Kg - dry 194 814Hexachlorocyclopentadiene 1 07/19/23 19:20 V35527AMP
<97.7 µg/Kg - dry 97.7 814Hexachloroethane 1 07/19/23 19:20 V35527AMP
<221 µg/Kg - dry 221 814Indeno(1,2,3-cd)pyrene 1 07/19/23 19:20 V35527AMP
<236 µg/Kg - dry 236 814Isophorone 1 07/19/23 19:20 V35527AMP
<131 µg/Kg - dry 131 8141-Methylnaphthalene 1 07/19/23 19:20 V35527AMP
<123 µg/Kg - dry 123 8142-Methylnaphthalene 1 07/19/23 19:20 V35527AMP
<120 µg/Kg - dry 120 8142-Methylphenol 1 07/19/23 19:20 V35527AMP
<105 µg/Kg - dry 105 8143&4 Methylphenol 1 07/19/23 19:20 V35527AMP
<178 µg/Kg - dry 178 814Naphthalene 1 07/19/23 19:20 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-1
89735 Matrix:
7/10/2023 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<119 µg/Kg - dry 119 8142-Nitroaniline 1 07/19/23 19:20 V35527AMP
<148 µg/Kg - dry 148 814
3-Nitroaniline 1 07/19/23 19:20 V35527AMP
<115 µg/Kg - dry 115 4074-Nitroaniline 1 07/19/23 19:20 V35527AMP
<143 µg/Kg - dry 143 407Nitrobenzene 1 07/19/23 19:20 V35527AMP
<109 µg/Kg - dry 109 8142-Nitrophenol 1 07/19/23 19:20 V35527AMP
<144 µg/Kg - dry 144 8144-Nitrophenol 1 07/19/23 19:20 V35527AMP
<324 µg/Kg - dry 324 814N-Nitrosodimethylamine 1 07/19/23 19:20 V35527AMP
<223 µg/Kg - dry 223 814N-Nitrosodiphenylamine 1 07/19/23 19:20 V35527AMP
<145 µg/Kg - dry 145 814
N-Nitroso-di-n-propylamine 1 07/19/23 19:20 V35527AMP
<428 µg/Kg - dry 428 1230Pentachlorophenol 1 07/19/23 19:20 V35527AMP
<256 µg/Kg - dry 256 814Phenanthrene 1 07/19/23 19:20 V35527AMP
<138 µg/Kg - dry 138 814Phenol 1 07/19/23 19:20 V35527AMP
<165 µg/Kg - dry 165 814Pyrene 1 07/19/23 19:20 V35527AMP
<97.7 µg/Kg - dry 97.7 407Pyridine 1 07/19/23 19:20 V35527AMP
<132 µg/Kg - dry 132 8141,2,4-Trichlorobenzene 1 07/19/23 19:20 V35527AMP
<119 µg/Kg - dry 119 8142,4,5-Trichlorophenol 1 07/19/23 19:20 V35527AMP
<119 µg/Kg - dry 119 8142,4,6-Trichlorophenol 1 07/19/23 19:20 V35527AMP
8270ESurrogate: Phenol-d5 61.6 Limits: 34-121%07/19/23 19:201 AMP
Surrogate: 2-Fluorobiphenyl 85.6 Limits: 44-115%07/19/23 19:201 AMP V35527
Surrogate: 2-Fluorophenol 73.9 Limits: 35-115%07/19/23 19:201 AMP V35527
Surrogate: Nitrobenzene-d5 81.4 Limits: 37-122%07/19/23 19:201 AMP V35527
Surrogate: 4-Terphenyl-d14 94.6 Limits: 54-127%07/19/23 19:201 AMP V35527
Surrogate: 2,4,6-Tribromophenol 78.1 Limits: 39-132%07/19/23 19:201 AMP V35527
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-2
89736 Matrix:
7/10/2023 14:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.2 %Moisture 1 07/18/23 18:45 SW-DRYWTCNC
1.16 mg/Kg - dry 0.170 0.241Chromium, Hexavalent 1 07/31/23 17:53 SW-7199SWB
0.372 mg/Kg - dry 0.103 0.302Arsenic 5 07/21/23 16:46 6020BCPW
43.4 mg/Kg - dry 0.051 0.301Barium 5 07/21/23 16:46 6020BCPW
<0.0314 mg/Kg - dry 0.0314 0.302Cadmium 5 07/21/23 16:46 6020BCPW
5.46 mg/Kg - dry 0.140 0.301
Chromium 5 07/21/23 16:46 6020BCPW
7.15 mg/Kg - dry 0.0374 0.302Lead 5 07/21/23 16:46 6020BCPW
<0.0145 mg/Kg - dry 0.0145 0.0362Mercury (Total)1 07/19/23 16:15 7471BJKC
0.894 mg/Kg - dry 0.124 0.301Selenium 5 07/21/23 16:46 6020BCPW
<0.0081 mg/Kg - dry 0.0081 0.302Silver 5 07/21/23 16:46 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-2
89736 Matrix:
7/10/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35489 07/18/23 08:00
0.006 J mg/Kg - dry 0.002 0.024Acetone 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 07/18/23 15:16 V35490TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 07/18/23 15:16 V35490TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 07/18/23 15:16 V35490TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 07/18/23 15:16 V35490TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 07/18/23 15:16 V35490TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 07/18/23 15:16 V35490TBL
0.008 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 07/18/23 15:16 V35490TBL
0.017 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 07/18/23 15:16 V35490TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 07/18/23 15:16 V35490TBL
0.001 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 07/18/23 15:16 V35490TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 07/18/23 15:16 V35490TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 07/18/23 15:16 V35490TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 07/18/23 15:16 V35490TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 07/18/23 15:16 V35490TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 07/18/23 15:16 V35490TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-2
89736 Matrix:
7/10/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35489 07/18/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 07/18/23 15:16 V35490TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 07/18/23 15:16 V35490TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 07/18/23 15:16 V35490TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 07/18/23 15:16 V35490TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 07/18/23 15:16 V35490TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 07/18/23 15:16 V35490TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 07/18/23 15:16 V35490TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 07/18/23 15:16 V35490TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 07/18/23 15:16 V35490TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 07/18/23 15:16 V35490TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 07/18/23 15:16 V35490TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 07/18/23 15:16 V35490TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 07/18/23 15:16 V35490TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 07/18/23 15:16 V35490TBL
<0.016 mg/Kg - dry 0.016 0.301Ethanol 1 07/18/23 15:16 V35490TBL
0.001 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 07/18/23 15:16 V35490TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 07/18/23 15:16 V35490TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-2
89736 Matrix:
7/10/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35489 07/18/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 07/18/23 15:16 V35490TBL
<0.0007 mg/Kg - dry 0.0007 0.024
2-Hexanone 1 07/18/23 15:16 V35490TBL
0.003 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 07/18/23 15:16 V35490TBL
0.004 J mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 07/18/23 15:16 V35490TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 07/18/23 15:16 V35490TBL
<0.0007 mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 07/18/23 15:16 V35490TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 07/18/23 15:16 V35490TBL
0.003 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 07/18/23 15:16 V35490TBL
0.063 mg/Kg - dry 0.001 0.012
Naphthalene 1 07/18/23 15:16 V35490TBL
0.009 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 07/18/23 15:16 V35490TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 07/18/23 15:16 V35490TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 07/18/23 15:16 V35490TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 07/18/23 15:16 V35490TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 07/18/23 15:16 V35490TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 07/18/23 15:16 V35490TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 07/18/23 15:16 V35490TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 07/18/23 15:16 V35490TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-2
89736 Matrix:
7/10/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35489 07/18/23 08:00
0.035 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 07/18/23 15:16 V35490TBL
0.004 J
mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 07/18/23 15:16 V35490TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 07/18/23 15:16 V35490TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 07/18/23 15:16 V35490TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 07/18/23 15:16 V35490TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 07/18/23 15:16 V35490TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 07/18/23 15:16 V35490
Surrogate: 4-Bromofluorobenzene 97.6 Limits: 70-130%07/18/23 15:161 TBL V35490
Surrogate: Dibromofluoromethane 100 Limits: 84-123%07/18/23 15:161 TBL V35490
Surrogate: Toluene-d8 96.8 Limits: 76-129%07/18/23 15:161 TBL V35490
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<140 µg/Kg - dry 140 797Acenaphthene 1 07/20/23 01:53 V35527AMP
<127 µg/Kg - dry 127 797Acenaphthylene 1 07/20/23 01:53 V35527AMP
<184 µg/Kg - dry 184 797Aniline 1 07/20/23 01:53 V35527AMP
<173 µg/Kg - dry 173 797Anthracene 1 07/20/23 01:53 V35527AMP
<168 µg/Kg - dry 168 797
Benzo(a)anthracene 1 07/20/23 01:53 V35527AMP
<178 µg/Kg - dry 178 797Benzo(a)pyrene 1 07/20/23 01:53 V35527AMP
<176 µg/Kg - dry 176 797Benzo(b)fluoranthene 1 07/20/23 01:53 V35527AMP
<164 µg/Kg - dry 164 797Benzo(g,h,i)perylene 1 07/20/23 01:53 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-2
89736 Matrix:
7/10/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<165 µg/Kg - dry 165 797Benzo(k)fluoranthene 1 07/20/23 01:53 V35527AMP
<700 µg/Kg - dry 700 2420
Benzoic Acid 1 07/20/23 01:53 V35527AMP
<127 µg/Kg - dry 127 797Benzyl alcohol 1 07/20/23 01:53 V35527AMP
<143 µg/Kg - dry 143 797Bis(2-Chloroethoxy)methane 1 07/20/23 01:53 V35527AMP
<129 µg/Kg - dry 129 797Bis(2-Chloroethyl)ether 1 07/20/23 01:53 V35527AMP
<164 µg/Kg - dry 164 399Bis(2-Chloroisopropyl)ether 1 07/20/23 01:53 V35527AMP
<145 µg/Kg - dry 145 797Bis(2-ethylhexyl)phthalate 1 07/20/23 01:53 V35527AMP
<132 µg/Kg - dry 132 7974-Bromophenyl phenyl ether 1 07/20/23 01:53 V35527AMP
<136 µg/Kg - dry 136 399
Butyl benzyl phthalate 1 07/20/23 01:53 V35527AMP
<112 µg/Kg - dry 112 7974-Chloro-3-methylphenol 1 07/20/23 01:53 V35527AMP
<135 µg/Kg - dry 135 3994-Chloroaniline 1 07/20/23 01:53 V35527AMP
<140 µg/Kg - dry 140 7972-Chloronaphthalene 1 07/20/23 01:53 V35527AMP
<119 µg/Kg - dry 119 7972-Chlorophenol 1 07/20/23 01:53 V35527AMP
<152 µg/Kg - dry 152 12104-Chlorophenyl phenyl ether 1 07/20/23 01:53 V35527AMP
<171 µg/Kg - dry 171 797Chrysene 1 07/20/23 01:53 V35527AMP
<278 µg/Kg - dry 278 797Dibenz(a,h)anthracene 1 07/20/23 01:53 V35527AMP
<144 µg/Kg - dry 144 797Dibenzofuran 1 07/20/23 01:53 V35527AMP
<114 µg/Kg - dry 114 7971,2-Dichlorobenzene 1 07/20/23 01:53 V35527AMP
<118 µg/Kg - dry 118 7971,3-Dichlorobenzene 1 07/20/23 01:53 V35527AMP
<118 µg/Kg - dry 118 3991,4-Dichlorobenzene 1 07/20/23 01:53 V35527AMP
<178 µg/Kg - dry 178 7973,3'-Dichlorobenzidine 1 07/20/23 01:53 V35527AMP
<116 µg/Kg - dry 116 7972,4-Dichlorophenol 1 07/20/23 01:53 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-2
89736 Matrix:
7/10/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<217 µg/Kg - dry 217 797Diethyl phthalate 1 07/20/23 01:53 V35527AMP
<210 µg/Kg - dry 210 797
Dimethyl phthalate 1 07/20/23 01:53 V35527AMP
<130 µg/Kg - dry 130 3992,4-Dimethylphenol 1 07/20/23 01:53 V35527AMP
<129 µg/Kg - dry 129 797Di-n-butyl phthalate 1 07/20/23 01:53 V35527AMP
<290 µg/Kg - dry 290 18104,6-Dinitro-2-methylphenol 1 07/20/23 01:53 V35527AMP
<628 µg/Kg - dry 628 18102,4-Dinitrophenol 1 07/20/23 01:53 V35527AMP
<117 µg/Kg - dry 117 7972,4-Dinitrotoluene 1 07/20/23 01:53 V35527AMP
<130 µg/Kg - dry 130 7972,6-Dinitrotoluene 1 07/20/23 01:53 V35527AMP
<173 µg/Kg - dry 173 399
Di-n-Octyl Phthalate 1 07/20/23 01:53 V35527AMP
<149 µg/Kg - dry 149 797Fluoranthene 1 07/20/23 01:53 V35527AMP
<155 µg/Kg - dry 155 797Fluorene 1 07/20/23 01:53 V35527AMP
<128 µg/Kg - dry 128 797Hexachlorobenzene 1 07/20/23 01:53 V35527AMP
<118 µg/Kg - dry 118 797Hexachlorobutadiene 1 07/20/23 01:53 V35527AMP
<190 µg/Kg - dry 190 797Hexachlorocyclopentadiene 1 07/20/23 01:53 V35527AMP
<95.7 µg/Kg - dry 95.7 797Hexachloroethane 1 07/20/23 01:53 V35527AMP
<216 µg/Kg - dry 216 797Indeno(1,2,3-cd)pyrene 1 07/20/23 01:53 V35527AMP
<231 µg/Kg - dry 231 797Isophorone 1 07/20/23 01:53 V35527AMP
319 J µg/Kg - dry 128 7971-Methylnaphthalene 1 07/20/23 01:53 V35527AMP
163 J µg/Kg - dry 121 7972-Methylnaphthalene 1 07/20/23 01:53 V35527AMP
<117 µg/Kg - dry 117 7972-Methylphenol 1 07/20/23 01:53 V35527AMP
<103 µg/Kg - dry 103 7973&4 Methylphenol 1 07/20/23 01:53 V35527AMP
<174 µg/Kg - dry 174 797Naphthalene 1 07/20/23 01:53 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-2
89736 Matrix:
7/10/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<117 µg/Kg - dry 117 7972-Nitroaniline 1 07/20/23 01:53 V35527AMP
<145 µg/Kg - dry 145 797
3-Nitroaniline 1 07/20/23 01:53 V35527AMP
<113 µg/Kg - dry 113 3994-Nitroaniline 1 07/20/23 01:53 V35527AMP
<140 µg/Kg - dry 140 399Nitrobenzene 1 07/20/23 01:53 V35527AMP
<107 µg/Kg - dry 107 7972-Nitrophenol 1 07/20/23 01:53 V35527AMP
<141 µg/Kg - dry 141 7974-Nitrophenol 1 07/20/23 01:53 V35527AMP
<318 µg/Kg - dry 318 797N-Nitrosodimethylamine 1 07/20/23 01:53 V35527AMP
<219 µg/Kg - dry 219 797N-Nitrosodiphenylamine 1 07/20/23 01:53 V35527AMP
<143 µg/Kg - dry 143 797
N-Nitroso-di-n-propylamine 1 07/20/23 01:53 V35527AMP
<419 µg/Kg - dry 419 1210Pentachlorophenol 1 07/20/23 01:53 V35527AMP
<251 µg/Kg - dry 251 797Phenanthrene 1 07/20/23 01:53 V35527AMP
<135 µg/Kg - dry 135 797Phenol 1 07/20/23 01:53 V35527AMP
<162 µg/Kg - dry 162 797Pyrene 1 07/20/23 01:53 V35527AMP
<95.7 µg/Kg - dry 95.7 399Pyridine 1 07/20/23 01:53 V35527AMP
<129 µg/Kg - dry 129 7971,2,4-Trichlorobenzene 1 07/20/23 01:53 V35527AMP
<116 µg/Kg - dry 116 7972,4,5-Trichlorophenol 1 07/20/23 01:53 V35527AMP
<117 µg/Kg - dry 117 7972,4,6-Trichlorophenol 1 07/20/23 01:53 V35527AMP
8270ESurrogate: Phenol-d5 56.2 Limits: 34-121%07/20/23 01:531 AMP
Surrogate: 2-Fluorobiphenyl 81.4 Limits: 44-115%07/20/23 01:531 AMP V35527
Surrogate: 2-Fluorophenol 66.1 Limits: 35-115%07/20/23 01:531 AMP V35527
Surrogate: Nitrobenzene-d5 57.2 Limits: 37-122%07/20/23 01:531 AMP V35527
Surrogate: 4-Terphenyl-d14 93.4 Limits: 54-127%07/20/23 01:531 AMP V35527
Surrogate: 2,4,6-Tribromophenol 83.8 Limits: 39-132%07/20/23 01:531 AMP V35527
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-3
89737 Matrix:
7/12/2023 11:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
32.5 %Moisture 1 07/18/23 18:45 SW-DRYWTCNC
0.234 J mg/Kg - dry 0.208 0.296Chromium, Hexavalent 1 07/31/23 18:04 SW-7199SWB
1.22 mg/Kg - dry 0.127 0.370Arsenic 5 07/21/23 16:50 6020BCPW
178 mg/Kg - dry 0.063 0.370Barium 5 07/21/23 16:50 6020BCPW
<0.0385 mg/Kg - dry 0.0385 0.370Cadmium 5 07/21/23 16:50 6020BCPW
19.3 mg/Kg - dry 0.171 0.370
Chromium 5 07/21/23 16:50 6020BCPW
10.7 mg/Kg - dry 0.0459 0.370Lead 5 07/21/23 16:50 6020BCPW
0.0399 J mg/Kg - dry 0.0178 0.0444Mercury (Total)1 07/19/23 16:18 7471BJKC
0.985 mg/Kg - dry 0.152 0.370Selenium 5 07/21/23 16:50 6020BCPW
0.0274 J mg/Kg - dry 0.0099 0.370Silver 5 07/21/23 16:50 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-3
89737 Matrix:
7/12/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
0.090 mg/Kg - dry 0.003 0.029Acetone 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.029
Acrolein 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.029Acrylonitrile 1 07/17/23 15:27 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.007Benzene 1 07/17/23 15:27 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 07/17/23 15:27 V35423TBL
<0.002 mg/Kg - dry 0.002 0.014
Bromomethane 1 07/17/23 15:27 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 07/17/23 15:27 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 07/17/23 15:27 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 07/17/23 15:27 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 07/17/23 15:27 V35423TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 07/17/23 15:27 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.007Chlorobenzene 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.007Chlorodibromomethane 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 07/17/23 15:27 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 07/17/23 15:27 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.0072-Chlorotoluene 1 07/17/23 15:27 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0074-Chlorotoluene 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 07/17/23 15:27 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-3
89737 Matrix:
7/12/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0141,2-Dibromo-3-Chloropropane 1 07/17/23 15:27 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.007
1,2-Dibromoethane 1 07/17/23 15:27 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 07/17/23 15:27 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,2-Dichlorobenzene 1 07/17/23 15:27 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,3-Dichlorobenzene 1 07/17/23 15:27 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,4-Dichlorobenzene 1 07/17/23 15:27 V35423TBL
<0.002 mg/Kg - dry 0.002 0.014Dichlorodifluoromethane 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 07/17/23 15:27 V35423TBL
<0.002 mg/Kg - dry 0.002 0.007
1,2-Dichloroethane 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 07/17/23 15:27 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,2-Dichloropropane 1 07/17/23 15:27 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloropropene 1 07/17/23 15:27 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 07/17/23 15:27 V35423TBL
<0.020 mg/Kg - dry 0.020 0.370Ethanol 1 07/17/23 15:27 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.007Ethylbenzene 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.074Ethyl Tertiary Butyl Ether (ETBE)1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 07/17/23 15:27 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-3
89737 Matrix:
7/12/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
0.003 J mg/Kg - dry 0.0010 0.014n-Hexane 1 07/17/23 15:27 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.029
2-Hexanone 1 07/17/23 15:27 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.007Isopropylbenzene 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 07/17/23 15:27 V35423TBL
0.017 J mg/Kg - dry 0.0010 0.029Methyl Ethyl Ketone (MEK)1 07/17/23 15:27 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 07/17/23 15:27 V35423TBL
<0.022 mg/Kg - dry 0.022 0.0294-Methyl-2-Pentanone 1 07/17/23 15:27 V35423TBL
0.008 J mg/Kg - dry 0.002 0.014Methylene Chloride 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.014
Naphthalene 1 07/17/23 15:27 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 07/17/23 15:27 V35423TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 07/17/23 15:27 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 07/17/23 15:27 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.007Toluene 1 07/17/23 15:27 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.0141,2,3-Trichlorobenzene 1 07/17/23 15:27 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0141,2,4-Trichlorobenzene 1 07/17/23 15:27 V35423TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 07/17/23 15:27 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 07/17/23 15:27 V35423TBL
<0.003 mg/Kg - dry 0.003 0.014Trichlorofluoromethane 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 07/17/23 15:27 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-3
89737 Matrix:
7/12/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 07/17/23 15:27 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.007
1,3,5-Trimethylbenzene 1 07/17/23 15:27 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Acetate 1 07/17/23 15:27 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 07/17/23 15:27 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.007o-Xylene 1 07/17/23 15:27 V35423TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 07/17/23 15:27 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.007Xylene (Total)1 07/17/23 15:27 V35423
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%07/17/23 15:271 TBL V35423
Surrogate: Dibromofluoromethane 101 Limits: 84-123%07/17/23 15:271 TBL V35423
Surrogate: Toluene-d8 99.0 Limits: 76-129%07/17/23 15:271 TBL V35423
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<172 µg/Kg - dry 172 978Acenaphthene 1 07/20/23 02:16 V35527AMP
<156 µg/Kg - dry 156 978Acenaphthylene 1 07/20/23 02:16 V35527AMP
<225 µg/Kg - dry 225 978Aniline 1 07/20/23 02:16 V35527AMP
<212 µg/Kg - dry 212 978Anthracene 1 07/20/23 02:16 V35527AMP
<206 µg/Kg - dry 206 978
Benzo(a)anthracene 1 07/20/23 02:16 V35527AMP
<218 µg/Kg - dry 218 978Benzo(a)pyrene 1 07/20/23 02:16 V35527AMP
<216 µg/Kg - dry 216 978Benzo(b)fluoranthene 1 07/20/23 02:16 V35527AMP
<201 µg/Kg - dry 201 978Benzo(g,h,i)perylene 1 07/20/23 02:16 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 32 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-3
89737 Matrix:
7/12/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<203 µg/Kg - dry 203 978Benzo(k)fluoranthene 1 07/20/23 02:16 V35527AMP
<859 µg/Kg - dry 859 2960
Benzoic Acid 1 07/20/23 02:16 V35527AMP
<156 µg/Kg - dry 156 978Benzyl alcohol 1 07/20/23 02:16 V35527AMP
<175 µg/Kg - dry 175 978Bis(2-Chloroethoxy)methane 1 07/20/23 02:16 V35527AMP
<159 µg/Kg - dry 159 978Bis(2-Chloroethyl)ether 1 07/20/23 02:16 V35527AMP
<201 µg/Kg - dry 201 489Bis(2-Chloroisopropyl)ether 1 07/20/23 02:16 V35527AMP
<178 µg/Kg - dry 178 978Bis(2-ethylhexyl)phthalate 1 07/20/23 02:16 V35527AMP
<161 µg/Kg - dry 161 9784-Bromophenyl phenyl ether 1 07/20/23 02:16 V35527AMP
<167 µg/Kg - dry 167 489
Butyl benzyl phthalate 1 07/20/23 02:16 V35527AMP
<137 µg/Kg - dry 137 9784-Chloro-3-methylphenol 1 07/20/23 02:16 V35527AMP
<166 µg/Kg - dry 166 4894-Chloroaniline 1 07/20/23 02:16 V35527AMP
<172 µg/Kg - dry 172 9782-Chloronaphthalene 1 07/20/23 02:16 V35527AMP
<145 µg/Kg - dry 145 9782-Chlorophenol 1 07/20/23 02:16 V35527AMP
<187 µg/Kg - dry 187 14804-Chlorophenyl phenyl ether 1 07/20/23 02:16 V35527AMP
<210 µg/Kg - dry 210 978Chrysene 1 07/20/23 02:16 V35527AMP
<341 µg/Kg - dry 341 978Dibenz(a,h)anthracene 1 07/20/23 02:16 V35527AMP
<176 µg/Kg - dry 176 978Dibenzofuran 1 07/20/23 02:16 V35527AMP
<140 µg/Kg - dry 140 9781,2-Dichlorobenzene 1 07/20/23 02:16 V35527AMP
<144 µg/Kg - dry 144 9781,3-Dichlorobenzene 1 07/20/23 02:16 V35527AMP
<144 µg/Kg - dry 144 4891,4-Dichlorobenzene 1 07/20/23 02:16 V35527AMP
<218 µg/Kg - dry 218 9783,3'-Dichlorobenzidine 1 07/20/23 02:16 V35527AMP
<142 µg/Kg - dry 142 9782,4-Dichlorophenol 1 07/20/23 02:16 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 33 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-3
89737 Matrix:
7/12/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<267 µg/Kg - dry 267 978Diethyl phthalate 1 07/20/23 02:16 V35527AMP
<258 µg/Kg - dry 258 978
Dimethyl phthalate 1 07/20/23 02:16 V35527AMP
<160 µg/Kg - dry 160 4892,4-Dimethylphenol 1 07/20/23 02:16 V35527AMP
<159 µg/Kg - dry 159 978Di-n-butyl phthalate 1 07/20/23 02:16 V35527AMP
<356 µg/Kg - dry 356 22204,6-Dinitro-2-methylphenol 1 07/20/23 02:16 V35527AMP
<770 µg/Kg - dry 770 22202,4-Dinitrophenol 1 07/20/23 02:16 V35527AMP
<143 µg/Kg - dry 143 9782,4-Dinitrotoluene 1 07/20/23 02:16 V35527AMP
<160 µg/Kg - dry 160 9782,6-Dinitrotoluene 1 07/20/23 02:16 V35527AMP
<212 µg/Kg - dry 212 489
Di-n-Octyl Phthalate 1 07/20/23 02:16 V35527AMP
<182 µg/Kg - dry 182 978Fluoranthene 1 07/20/23 02:16 V35527AMP
<190 µg/Kg - dry 190 978Fluorene 1 07/20/23 02:16 V35527AMP
<157 µg/Kg - dry 157 978Hexachlorobenzene 1 07/20/23 02:16 V35527AMP
<145 µg/Kg - dry 145 978Hexachlorobutadiene 1 07/20/23 02:16 V35527AMP
<233 µg/Kg - dry 233 978Hexachlorocyclopentadiene 1 07/20/23 02:16 V35527AMP
<117 µg/Kg - dry 117 978Hexachloroethane 1 07/20/23 02:16 V35527AMP
<265 µg/Kg - dry 265 978Indeno(1,2,3-cd)pyrene 1 07/20/23 02:16 V35527AMP
<283 µg/Kg - dry 283 978Isophorone 1 07/20/23 02:16 V35527AMP
<157 µg/Kg - dry 157 9781-Methylnaphthalene 1 07/20/23 02:16 V35527AMP
<148 µg/Kg - dry 148 9782-Methylnaphthalene 1 07/20/23 02:16 V35527AMP
<144 µg/Kg - dry 144 9782-Methylphenol 1 07/20/23 02:16 V35527AMP
<126 µg/Kg - dry 126 9783&4 Methylphenol 1 07/20/23 02:16 V35527AMP
<213 µg/Kg - dry 213 978Naphthalene 1 07/20/23 02:16 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 34 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-3
89737 Matrix:
7/12/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<143 µg/Kg - dry 143 9782-Nitroaniline 1 07/20/23 02:16 V35527AMP
<178 µg/Kg - dry 178 978
3-Nitroaniline 1 07/20/23 02:16 V35527AMP
<138 µg/Kg - dry 138 4894-Nitroaniline 1 07/20/23 02:16 V35527AMP
<172 µg/Kg - dry 172 489Nitrobenzene 1 07/20/23 02:16 V35527AMP
<132 µg/Kg - dry 132 9782-Nitrophenol 1 07/20/23 02:16 V35527AMP
<173 µg/Kg - dry 173 9784-Nitrophenol 1 07/20/23 02:16 V35527AMP
<390 µg/Kg - dry 390 978N-Nitrosodimethylamine 1 07/20/23 02:16 V35527AMP
<268 µg/Kg - dry 268 978N-Nitrosodiphenylamine 1 07/20/23 02:16 V35527AMP
<175 µg/Kg - dry 175 978
N-Nitroso-di-n-propylamine 1 07/20/23 02:16 V35527AMP
<514 µg/Kg - dry 514 1480Pentachlorophenol 1 07/20/23 02:16 V35527AMP
<308 µg/Kg - dry 308 978Phenanthrene 1 07/20/23 02:16 V35527AMP
<166 µg/Kg - dry 166 978Phenol 1 07/20/23 02:16 V35527AMP
<199 µg/Kg - dry 199 978Pyrene 1 07/20/23 02:16 V35527AMP
<117 µg/Kg - dry 117 489Pyridine 1 07/20/23 02:16 V35527AMP
<159 µg/Kg - dry 159 9781,2,4-Trichlorobenzene 1 07/20/23 02:16 V35527AMP
<143 µg/Kg - dry 143 9782,4,5-Trichlorophenol 1 07/20/23 02:16 V35527AMP
<143 µg/Kg - dry 143 9782,4,6-Trichlorophenol 1 07/20/23 02:16 V35527AMP
8270ESurrogate: Phenol-d5 41.4 Limits: 34-121%07/20/23 02:161 AMP
Surrogate: 2-Fluorobiphenyl 74.1 Limits: 44-115%07/20/23 02:161 AMP V35527
Surrogate: 2-Fluorophenol 46.8 Limits: 35-115%07/20/23 02:161 AMP V35527
Surrogate: Nitrobenzene-d5 68.1 Limits: 37-122%07/20/23 02:161 AMP V35527
Surrogate: 4-Terphenyl-d14 79.5 Limits: 54-127%07/20/23 02:161 AMP V35527
Surrogate: 2,4,6-Tribromophenol 55.0 Limits: 39-132%07/20/23 02:161 AMP V35527
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 35 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-4
89738 Matrix:
7/12/2023 9:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.0 %Moisture 1 07/18/23 18:45 SW-DRYWTCNC
<0.162 mg/Kg - dry 0.162 0.229Chromium, Hexavalent 1 07/31/23 18:15 SW-7199SWB
1.04 mg/Kg - dry 0.0982 0.287Arsenic 5 07/21/23 16:54 6020BCPW
334 mg/Kg - dry 0.049 0.287Barium 5 07/21/23 16:54 6020BCPW
0.205 J mg/Kg - dry 0.0298 0.287Cadmium 5 07/21/23 16:54 6020BCPW
16.4 mg/Kg - dry 0.133 0.287
Chromium 5 07/21/23 16:54 6020BCPW
88.4 mg/Kg - dry 0.0356 0.287Lead 5 07/21/23 16:54 6020BCPW
0.0295 J mg/Kg - dry 0.0138 0.0345Mercury (Total)1 07/19/23 16:20 7471BJKC
0.260 J mg/Kg - dry 0.118 0.287Selenium 5 07/21/23 16:54 6020BCPW
0.0239 J mg/Kg - dry 0.0077 0.287Silver 5 07/21/23 16:54 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 36 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-4
89738 Matrix:
7/12/2023 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
0.007 J mg/Kg - dry 0.002 0.022Acetone 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.022
Acrolein 1 07/17/23 15:54 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 07/17/23 15:54 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 07/17/23 15:54 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 07/17/23 15:54 V35423TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 07/17/23 15:54 V35423TBL
0.0010 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 07/17/23 15:54 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 07/17/23 15:54 V35423TBL
0.001 J mg/Kg - dry 0.001 0.011Chloroethane 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 07/17/23 15:54 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 07/17/23 15:54 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 07/17/23 15:54 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 07/17/23 15:54 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 37 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-4
89738 Matrix:
7/12/2023 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 07/17/23 15:54 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 07/17/23 15:54 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 07/17/23 15:54 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 07/17/23 15:54 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 07/17/23 15:54 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 07/17/23 15:54 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 07/17/23 15:54 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 07/17/23 15:54 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 07/17/23 15:54 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 07/17/23 15:54 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 07/17/23 15:54 V35423TBL
<0.016 mg/Kg - dry 0.016 0.287Ethanol 1 07/17/23 15:54 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 07/17/23 15:54 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 07/17/23 15:54 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 07/17/23 15:54 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 38 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-4
89738 Matrix:
7/12/2023 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
0.0010 J mg/Kg - dry 0.0008 0.011n-Hexane 1 07/17/23 15:54 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.022
2-Hexanone 1 07/17/23 15:54 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 07/17/23 15:54 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 07/17/23 15:54 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 07/17/23 15:54 V35423TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 07/17/23 15:54 V35423TBL
0.003 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 07/17/23 15:54 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 07/17/23 15:54 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 07/17/23 15:54 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 07/17/23 15:54 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 07/17/23 15:54 V35423TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 07/17/23 15:54 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 07/17/23 15:54 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 39 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-4
89738 Matrix:
7/12/2023 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 07/17/23 15:54 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 07/17/23 15:54 V35423TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 07/17/23 15:54 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 07/17/23 15:54 V35423
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/17/23 15:541 TBL V35423
Surrogate: Dibromofluoromethane 105 Limits: 84-123%07/17/23 15:541 TBL V35423
Surrogate: Toluene-d8 98.7 Limits: 76-129%07/17/23 15:541 TBL V35423
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<133 µg/Kg - dry 133 759Acenaphthene 1 07/20/23 00:20 V35527AMP
<121 µg/Kg - dry 121 759Acenaphthylene 1 07/20/23 00:20 V35527AMP
<175 µg/Kg - dry 175 759Aniline 1 07/20/23 00:20 V35527AMP
<164 µg/Kg - dry 164 759Anthracene 1 07/20/23 00:20 V35527AMP
<160 µg/Kg - dry 160 759
Benzo(a)anthracene 1 07/20/23 00:20 V35527AMP
<169 µg/Kg - dry 169 759Benzo(a)pyrene 1 07/20/23 00:20 V35527AMP
<168 µg/Kg - dry 168 759Benzo(b)fluoranthene 1 07/20/23 00:20 V35527AMP
<156 µg/Kg - dry 156 759Benzo(g,h,i)perylene 1 07/20/23 00:20 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 40 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-4
89738 Matrix:
7/12/2023 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<157 µg/Kg - dry 157 759Benzo(k)fluoranthene 1 07/20/23 00:20 V35527AMP
<667 µg/Kg - dry 667 2300
Benzoic Acid 1 07/20/23 00:20 V35527AMP
<121 µg/Kg - dry 121 759Benzyl alcohol 1 07/20/23 00:20 V35527AMP
<136 µg/Kg - dry 136 759Bis(2-Chloroethoxy)methane 1 07/20/23 00:20 V35527AMP
<123 µg/Kg - dry 123 759Bis(2-Chloroethyl)ether 1 07/20/23 00:20 V35527AMP
<156 µg/Kg - dry 156 379Bis(2-Chloroisopropyl)ether 1 07/20/23 00:20 V35527AMP
<138 µg/Kg - dry 138 759Bis(2-ethylhexyl)phthalate 1 07/20/23 00:20 V35527AMP
<125 µg/Kg - dry 125 7594-Bromophenyl phenyl ether 1 07/20/23 00:20 V35527AMP
<130 µg/Kg - dry 130 379
Butyl benzyl phthalate 1 07/20/23 00:20 V35527AMP
<106 µg/Kg - dry 106 7594-Chloro-3-methylphenol 1 07/20/23 00:20 V35527AMP
<129 µg/Kg - dry 129 3794-Chloroaniline 1 07/20/23 00:20 V35527AMP
<133 µg/Kg - dry 133 7592-Chloronaphthalene 1 07/20/23 00:20 V35527AMP
<113 µg/Kg - dry 113 7592-Chlorophenol 1 07/20/23 00:20 V35527AMP
<145 µg/Kg - dry 145 11504-Chlorophenyl phenyl ether 1 07/20/23 00:20 V35527AMP
<163 µg/Kg - dry 163 759Chrysene 1 07/20/23 00:20 V35527AMP
<264 µg/Kg - dry 264 759Dibenz(a,h)anthracene 1 07/20/23 00:20 V35527AMP
<137 µg/Kg - dry 137 759Dibenzofuran 1 07/20/23 00:20 V35527AMP
<109 µg/Kg - dry 109 7591,2-Dichlorobenzene 1 07/20/23 00:20 V35527AMP
<112 µg/Kg - dry 112 7591,3-Dichlorobenzene 1 07/20/23 00:20 V35527AMP
<112 µg/Kg - dry 112 3791,4-Dichlorobenzene 1 07/20/23 00:20 V35527AMP
<169 µg/Kg - dry 169 7593,3'-Dichlorobenzidine 1 07/20/23 00:20 V35527AMP
<110 µg/Kg - dry 110 7592,4-Dichlorophenol 1 07/20/23 00:20 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 41 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-4
89738 Matrix:
7/12/2023 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<207 µg/Kg - dry 207 759Diethyl phthalate 1 07/20/23 00:20 V35527AMP
<200 µg/Kg - dry 200 759
Dimethyl phthalate 1 07/20/23 00:20 V35527AMP
<124 µg/Kg - dry 124 3792,4-Dimethylphenol 1 07/20/23 00:20 V35527AMP
<123 µg/Kg - dry 123 759Di-n-butyl phthalate 1 07/20/23 00:20 V35527AMP
<276 µg/Kg - dry 276 17204,6-Dinitro-2-methylphenol 1 07/20/23 00:20 V35527AMP
<598 µg/Kg - dry 598 17202,4-Dinitrophenol 1 07/20/23 00:20 V35527AMP
<111 µg/Kg - dry 111 7592,4-Dinitrotoluene 1 07/20/23 00:20 V35527AMP
<124 µg/Kg - dry 124 7592,6-Dinitrotoluene 1 07/20/23 00:20 V35527AMP
<164 µg/Kg - dry 164 379
Di-n-Octyl Phthalate 1 07/20/23 00:20 V35527AMP
<141 µg/Kg - dry 141 759Fluoranthene 1 07/20/23 00:20 V35527AMP
<147 µg/Kg - dry 147 759Fluorene 1 07/20/23 00:20 V35527AMP
<122 µg/Kg - dry 122 759Hexachlorobenzene 1 07/20/23 00:20 V35527AMP
<112 µg/Kg - dry 112 759Hexachlorobutadiene 1 07/20/23 00:20 V35527AMP
<180 µg/Kg - dry 180 759Hexachlorocyclopentadiene 1 07/20/23 00:20 V35527AMP
<91.0 µg/Kg - dry 91.0 759Hexachloroethane 1 07/20/23 00:20 V35527AMP
<206 µg/Kg - dry 206 759Indeno(1,2,3-cd)pyrene 1 07/20/23 00:20 V35527AMP
<220 µg/Kg - dry 220 759Isophorone 1 07/20/23 00:20 V35527AMP
<122 µg/Kg - dry 122 7591-Methylnaphthalene 1 07/20/23 00:20 V35527AMP
<115 µg/Kg - dry 115 7592-Methylnaphthalene 1 07/20/23 00:20 V35527AMP
<111 µg/Kg - dry 111 7592-Methylphenol 1 07/20/23 00:20 V35527AMP
<97.6 µg/Kg - dry 97.6 7593&4 Methylphenol 1 07/20/23 00:20 V35527AMP
<166 µg/Kg - dry 166 759Naphthalene 1 07/20/23 00:20 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 42 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-4
89738 Matrix:
7/12/2023 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<111 µg/Kg - dry 111 7592-Nitroaniline 1 07/20/23 00:20 V35527AMP
<138 µg/Kg - dry 138 759
3-Nitroaniline 1 07/20/23 00:20 V35527AMP
<107 µg/Kg - dry 107 3794-Nitroaniline 1 07/20/23 00:20 V35527AMP
<133 µg/Kg - dry 133 379Nitrobenzene 1 07/20/23 00:20 V35527AMP
<102 µg/Kg - dry 102 7592-Nitrophenol 1 07/20/23 00:20 V35527AMP
<134 µg/Kg - dry 134 7594-Nitrophenol 1 07/20/23 00:20 V35527AMP
<302 µg/Kg - dry 302 759N-Nitrosodimethylamine 1 07/20/23 00:20 V35527AMP
<208 µg/Kg - dry 208 759N-Nitrosodiphenylamine 1 07/20/23 00:20 V35527AMP
<136 µg/Kg - dry 136 759
N-Nitroso-di-n-propylamine 1 07/20/23 00:20 V35527AMP
<399 µg/Kg - dry 399 1150Pentachlorophenol 1 07/20/23 00:20 V35527AMP
<239 µg/Kg - dry 239 759Phenanthrene 1 07/20/23 00:20 V35527AMP
<129 µg/Kg - dry 129 759Phenol 1 07/20/23 00:20 V35527AMP
<154 µg/Kg - dry 154 759Pyrene 1 07/20/23 00:20 V35527AMP
<91.0 µg/Kg - dry 91.0 379Pyridine 1 07/20/23 00:20 V35527AMP
<123 µg/Kg - dry 123 7591,2,4-Trichlorobenzene 1 07/20/23 00:20 V35527AMP
<111 µg/Kg - dry 111 7592,4,5-Trichlorophenol 1 07/20/23 00:20 V35527AMP
<111 µg/Kg - dry 111 7592,4,6-Trichlorophenol 1 07/20/23 00:20 V35527AMP
8270ESurrogate: Phenol-d5 63.7 Limits: 34-121%07/20/23 00:201 AMP
Surrogate: 2-Fluorobiphenyl 89.2 Limits: 44-115%07/20/23 00:201 AMP V35527
Surrogate: 2-Fluorophenol 74.8 Limits: 35-115%07/20/23 00:201 AMP V35527
Surrogate: Nitrobenzene-d5 81.4 Limits: 37-122%07/20/23 00:201 AMP V35527
Surrogate: 4-Terphenyl-d14 102 Limits: 54-127%07/20/23 00:201 AMP V35527
Surrogate: 2,4,6-Tribromophenol 83.2 Limits: 39-132%07/20/23 00:201 AMP V35527
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 43 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-5
89739 Matrix:
7/12/2023 10:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.5 %Moisture 1 07/18/23 18:45 SW-DRYWTCNC
0.384 mg/Kg - dry 0.161 0.228Chromium, Hexavalent 1 07/31/23 18:26 SW-7199SWB
1.06 mg/Kg - dry 0.0977 0.286Arsenic 5 07/21/23 16:58 6020BCPW
62.4 mg/Kg - dry 0.048 0.285Barium 5 07/21/23 16:58 6020BCPW
0.0384 J mg/Kg - dry 0.0297 0.286Cadmium 5 07/21/23 16:58 6020BCPW
30.7 mg/Kg - dry 0.132 0.285
Chromium 5 07/21/23 16:58 6020BCPW
10.8 mg/Kg - dry 0.0354 0.286Lead 5 07/21/23 16:58 6020BCPW
0.0353 mg/Kg - dry 0.0137 0.0343Mercury (Total)1 07/19/23 16:23 7471BJKC
1.09 mg/Kg - dry 0.117 0.285Selenium 5 07/21/23 16:58 6020BCPW
0.0173 J mg/Kg - dry 0.0077 0.286Silver 5 07/21/23 16:58 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 44 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-5
89739 Matrix:
7/12/2023 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
0.035 mg/Kg - dry 0.002 0.022Acetone 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.022
Acrolein 1 07/17/23 16:22 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 07/17/23 16:22 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 07/17/23 16:22 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 07/17/23 16:22 V35423TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 07/17/23 16:22 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 07/17/23 16:22 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 07/17/23 16:22 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 07/17/23 16:22 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 07/17/23 16:22 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 07/17/23 16:22 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 45 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-5
89739 Matrix:
7/12/2023 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 07/17/23 16:22 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 07/17/23 16:22 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 07/17/23 16:22 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 07/17/23 16:22 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 07/17/23 16:22 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 07/17/23 16:22 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 07/17/23 16:22 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 07/17/23 16:22 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 07/17/23 16:22 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 07/17/23 16:22 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 07/17/23 16:22 V35423TBL
<0.016 mg/Kg - dry 0.016 0.285Ethanol 1 07/17/23 16:22 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 07/17/23 16:22 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.057Ethyl Tertiary Butyl Ether (ETBE)1 07/17/23 16:22 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 07/17/23 16:22 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 46 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-5
89739 Matrix:
7/12/2023 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 07/17/23 16:22 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.022
2-Hexanone 1 07/17/23 16:22 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 07/17/23 16:22 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 07/17/23 16:22 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 07/17/23 16:22 V35423TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 07/17/23 16:22 V35423TBL
0.003 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 07/17/23 16:22 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 07/17/23 16:22 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 07/17/23 16:22 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 07/17/23 16:22 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 07/17/23 16:22 V35423TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 07/17/23 16:22 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 07/17/23 16:22 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 47 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-5
89739 Matrix:
7/12/2023 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 07/17/23 16:22 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 07/17/23 16:22 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 07/17/23 16:22 V35423TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 07/17/23 16:22 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 07/17/23 16:22 V35423
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/17/23 16:221 TBL V35423
Surrogate: Dibromofluoromethane 103 Limits: 84-123%07/17/23 16:221 TBL V35423
Surrogate: Toluene-d8 96.6 Limits: 76-129%07/17/23 16:221 TBL V35423
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<133 µg/Kg - dry 133 754Acenaphthene 1 07/21/23 15:11 V35527AMP
<120 µg/Kg - dry 120 754Acenaphthylene 1 07/21/23 15:11 V35527AMP
<174 µg/Kg - dry 174 754Aniline 1 07/21/23 15:11 V35527AMP
<163 µg/Kg - dry 163 754Anthracene 1 07/21/23 15:11 V35527AMP
201 J
µg/Kg - dry 159 754
Benzo(a)anthracene 1 07/21/23 15:11 V35527AMP
232 J µg/Kg - dry 168 754Benzo(a)pyrene 1 07/21/23 15:11 V35527AMP
325 J µg/Kg - dry 167 754Benzo(b)fluoranthene 1 07/21/23 15:11 V35527AMP
<155 µg/Kg - dry 155 754Benzo(g,h,i)perylene 1 07/21/23 15:11 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 48 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-5
89739 Matrix:
7/12/2023 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<157 µg/Kg - dry 157 754Benzo(k)fluoranthene 1 07/21/23 15:11 V35527AMP
<663 µg/Kg - dry 663 2290
Benzoic Acid 1 07/21/23 15:11 V35527AMP
<120 µg/Kg - dry 120 754Benzyl alcohol 1 07/21/23 15:11 V35527AMP
<135 µg/Kg - dry 135 754Bis(2-Chloroethoxy)methane 1 07/21/23 15:11 V35527AMP
<122 µg/Kg - dry 122 754Bis(2-Chloroethyl)ether 1 07/21/23 15:11 V35527AMP
<155 µg/Kg - dry 155 377Bis(2-Chloroisopropyl)ether 1 07/21/23 15:11 V35527AMP
<137 µg/Kg - dry 137 754Bis(2-ethylhexyl)phthalate 1 07/21/23 15:11 V35527AMP
<125 µg/Kg - dry 125 7544-Bromophenyl phenyl ether 1 07/21/23 15:11 V35527AMP
<129 µg/Kg - dry 129 377
Butyl benzyl phthalate 1 07/21/23 15:11 V35527AMP
<106 µg/Kg - dry 106 7544-Chloro-3-methylphenol 1 07/21/23 15:11 V35527AMP
<128 µg/Kg - dry 128 3774-Chloroaniline 1 07/21/23 15:11 V35527AMP
<133 µg/Kg - dry 133 7542-Chloronaphthalene 1 07/21/23 15:11 V35527AMP
<112 µg/Kg - dry 112 7542-Chlorophenol 1 07/21/23 15:11 V35527AMP
<144 µg/Kg - dry 144 11404-Chlorophenyl phenyl ether 1 07/21/23 15:11 V35527AMP
184 J µg/Kg - dry 162 754Chrysene 1 07/21/23 15:11 V35527AMP
<263 µg/Kg - dry 263 754Dibenz(a,h)anthracene 1 07/21/23 15:11 V35527AMP
<136 µg/Kg - dry 136 754Dibenzofuran 1 07/21/23 15:11 V35527AMP
<108 µg/Kg - dry 108 7541,2-Dichlorobenzene 1 07/21/23 15:11 V35527AMP
<111 µg/Kg - dry 111 7541,3-Dichlorobenzene 1 07/21/23 15:11 V35527AMP
<111 µg/Kg - dry 111 3771,4-Dichlorobenzene 1 07/21/23 15:11 V35527AMP
<168 µg/Kg - dry 168 7543,3'-Dichlorobenzidine 1 07/21/23 15:11 V35527AMP
<109 µg/Kg - dry 109 7542,4-Dichlorophenol 1 07/21/23 15:11 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 49 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-5
89739 Matrix:
7/12/2023 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<206 µg/Kg - dry 206 754Diethyl phthalate 1 07/21/23 15:11 V35527AMP
<199 µg/Kg - dry 199 754
Dimethyl phthalate 1 07/21/23 15:11 V35527AMP
<123 µg/Kg - dry 123 3772,4-Dimethylphenol 1 07/21/23 15:11 V35527AMP
<122 µg/Kg - dry 122 754Di-n-butyl phthalate 1 07/21/23 15:11 V35527AMP
<274 µg/Kg - dry 274 17104,6-Dinitro-2-methylphenol 1 07/21/23 15:11 V35527AMP
<594 µg/Kg - dry 594 17102,4-Dinitrophenol 1 07/21/23 15:11 V35527AMP
<110 µg/Kg - dry 110 7542,4-Dinitrotoluene 1 07/21/23 15:11 V35527AMP
<123 µg/Kg - dry 123 7542,6-Dinitrotoluene 1 07/21/23 15:11 V35527AMP
<163 µg/Kg - dry 163 377
Di-n-Octyl Phthalate 1 07/21/23 15:11 V35527AMP
296 J µg/Kg - dry 141 754Fluoranthene 1 07/21/23 15:11 V35527AMP
<146 µg/Kg - dry 146 754Fluorene 1 07/21/23 15:11 V35527AMP
<121 µg/Kg - dry 121 754Hexachlorobenzene 1 07/21/23 15:11 V35527AMP
<112 µg/Kg - dry 112 754Hexachlorobutadiene 1 07/21/23 15:11 V35527AMP
<179 µg/Kg - dry 179 754Hexachlorocyclopentadiene 1 07/21/23 15:11 V35527AMP
<90.5 µg/Kg - dry 90.5 754Hexachloroethane 1 07/21/23 15:11 V35527AMP
<205 µg/Kg - dry 205 754Indeno(1,2,3-cd)pyrene 1 07/21/23 15:11 V35527AMP
<218 µg/Kg - dry 218 754Isophorone 1 07/21/23 15:11 V35527AMP
<121 µg/Kg - dry 121 7541-Methylnaphthalene 1 07/21/23 15:11 V35527AMP
<114 µg/Kg - dry 114 7542-Methylnaphthalene 1 07/21/23 15:11 V35527AMP
<111 µg/Kg - dry 111 7542-Methylphenol 1 07/21/23 15:11 V35527AMP
<97.0 µg/Kg - dry 97.0 7543&4 Methylphenol 1 07/21/23 15:11 V35527AMP
<165 µg/Kg - dry 165 754Naphthalene 1 07/21/23 15:11 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 50 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-5
89739 Matrix:
7/12/2023 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<111 µg/Kg - dry 111 7542-Nitroaniline 1 07/21/23 15:11 V35527AMP
<137 µg/Kg - dry 137 754
3-Nitroaniline 1 07/21/23 15:11 V35527AMP
<107 µg/Kg - dry 107 3774-Nitroaniline 1 07/21/23 15:11 V35527AMP
<133 µg/Kg - dry 133 377Nitrobenzene 1 07/21/23 15:11 V35527AMP
<101 µg/Kg - dry 101 7542-Nitrophenol 1 07/21/23 15:11 V35527AMP
<134 µg/Kg - dry 134 7544-Nitrophenol 1 07/21/23 15:11 V35527AMP
<301 µg/Kg - dry 301 754N-Nitrosodimethylamine 1 07/21/23 15:11 V35527AMP
<207 µg/Kg - dry 207 754N-Nitrosodiphenylamine 1 07/21/23 15:11 V35527AMP
<135 µg/Kg - dry 135 754
N-Nitroso-di-n-propylamine 1 07/21/23 15:11 V35527AMP
<397 µg/Kg - dry 397 1140Pentachlorophenol 1 07/21/23 15:11 V35527AMP
<238 µg/Kg - dry 238 754Phenanthrene 1 07/21/23 15:11 V35527AMP
<128 µg/Kg - dry 128 754Phenol 1 07/21/23 15:11 V35527AMP
303 J µg/Kg - dry 153 754Pyrene 1 07/21/23 15:11 V35527AMP
<90.5 µg/Kg - dry 90.5 377Pyridine 1 07/21/23 15:11 V35527AMP
<122 µg/Kg - dry 122 7541,2,4-Trichlorobenzene 1 07/21/23 15:11 V35527AMP
<110 µg/Kg - dry 110 7542,4,5-Trichlorophenol 1 07/21/23 15:11 V35527AMP
<110 µg/Kg - dry 110 7542,4,6-Trichlorophenol 1 07/21/23 15:11 V35527AMP
8270ESurrogate: Phenol-d5 58.3 Limits: 34-121%07/21/23 15:111 AMP
Surrogate: 2-Fluorobiphenyl 78.9 Limits: 44-115%07/21/23 15:111 AMP V35527
Surrogate: 2-Fluorophenol 65.2 Limits: 35-115%07/21/23 15:111 AMP V35527
Surrogate: Nitrobenzene-d5 72.9 Limits: 37-122%07/21/23 15:111 AMP V35527
Surrogate: 4-Terphenyl-d14 84.3 Limits: 54-127%07/21/23 15:111 AMP V35527
Surrogate: 2,4,6-Tribromophenol 70.0 Limits: 39-132%07/21/23 15:111 AMP V35527
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 51 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-Dup
89740 Matrix:
7/10/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.8 %Moisture 1 07/19/23 11:50 SW-DRYWTCNC
0.397 mg/Kg - dry 0.171 0.243Chromium, Hexavalent 1 07/31/23 18:37 SW-7199SWB
0.339 mg/Kg - dry 0.104 0.304Arsenic 5 07/21/23 17:02 6020BCPW
41.8 mg/Kg - dry 0.052 0.304Barium 5 07/21/23 17:02 6020BCPW
<0.0316 mg/Kg - dry 0.0316 0.304Cadmium 5 07/21/23 17:02 6020BCPW
4.74 mg/Kg - dry 0.141 0.304
Chromium 5 07/21/23 17:02 6020BCPW
6.79 mg/Kg - dry 0.0377 0.304Lead 5 07/21/23 17:02 6020BCPW
<0.0146 mg/Kg - dry 0.0146 0.0365Mercury (Total)1 07/19/23 16:25 7471BJKC
0.873 mg/Kg - dry 0.125 0.304Selenium 5 07/21/23 17:02 6020BCPW
<0.0081 mg/Kg - dry 0.0081 0.304Silver 5 07/21/23 17:02 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 52 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-Dup
89740 Matrix:
7/10/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
0.007 J mg/Kg - dry 0.002 0.024Acetone 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 07/17/23 16:49 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 07/17/23 16:49 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 07/17/23 16:49 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 07/17/23 16:49 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 07/17/23 16:49 V35423TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 07/17/23 16:49 V35423TBL
0.016 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 07/17/23 16:49 V35423TBL
0.036 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 07/17/23 16:49 V35423TBL
0.0007 J mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 07/17/23 16:49 V35423TBL
0.002 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 07/17/23 16:49 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 07/17/23 16:49 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 07/17/23 16:49 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 07/17/23 16:49 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 07/17/23 16:49 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 07/17/23 16:49 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 53 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-Dup
89740 Matrix:
7/10/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 07/17/23 16:49 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 07/17/23 16:49 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 07/17/23 16:49 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 07/17/23 16:49 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 07/17/23 16:49 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 07/17/23 16:49 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 07/17/23 16:49 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 07/17/23 16:49 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 07/17/23 16:49 V35423TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 07/17/23 16:49 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 07/17/23 16:49 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 07/17/23 16:49 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 07/17/23 16:49 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 07/17/23 16:49 V35423TBL
<0.017 mg/Kg - dry 0.017 0.304Ethanol 1 07/17/23 16:49 V35423TBL
0.002 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 07/17/23 16:49 V35423TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 07/17/23 16:49 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 54 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-Dup
89740 Matrix:
7/10/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 07/17/23 16:49 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 07/17/23 16:49 V35423TBL
0.008 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 07/17/23 16:49 V35423TBL
0.009 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 07/17/23 16:49 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 07/17/23 16:49 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 07/17/23 16:49 V35423TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 07/17/23 16:49 V35423TBL
0.006 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 07/17/23 16:49 V35423TBL
0.101 mg/Kg - dry 0.001 0.012
Naphthalene 1 07/17/23 16:49 V35423TBL
0.020 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 07/17/23 16:49 V35423TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 07/17/23 16:49 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 07/17/23 16:49 V35423TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 07/17/23 16:49 V35423TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 07/17/23 16:49 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 07/17/23 16:49 V35423TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 07/17/23 16:49 V35423TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 07/17/23 16:49 V35423TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 55 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-Dup
89740 Matrix:
7/10/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V35422 07/17/23 08:00
0.078 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 07/17/23 16:49 V35423TBL
0.009 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 07/17/23 16:49 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 07/17/23 16:49 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 07/17/23 16:49 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 07/17/23 16:49 V35423TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 07/17/23 16:49 V35423TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 07/17/23 16:49 V35423
Surrogate: 4-Bromofluorobenzene 98.1 Limits: 70-130%07/17/23 16:491 TBL V35423
Surrogate: Dibromofluoromethane 101 Limits: 84-123%07/17/23 16:491 TBL V35423
Surrogate: Toluene-d8 98.8 Limits: 76-129%07/17/23 16:491 TBL V35423
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<141 µg/Kg - dry 141 803Acenaphthene 1 07/20/23 01:06 V35527AMP
<128 µg/Kg - dry 128 803Acenaphthylene 1 07/20/23 01:06 V35527AMP
<185 µg/Kg - dry 185 803Aniline 1 07/20/23 01:06 V35527AMP
<174 µg/Kg - dry 174 803Anthracene 1 07/20/23 01:06 V35527AMP
<169 µg/Kg - dry 169 803
Benzo(a)anthracene 1 07/20/23 01:06 V35527AMP
<179 µg/Kg - dry 179 803Benzo(a)pyrene 1 07/20/23 01:06 V35527AMP
<178 µg/Kg - dry 178 803Benzo(b)fluoranthene 1 07/20/23 01:06 V35527AMP
<165 µg/Kg - dry 165 803Benzo(g,h,i)perylene 1 07/20/23 01:06 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 56 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-Dup
89740 Matrix:
7/10/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<167 µg/Kg - dry 167 803Benzo(k)fluoranthene 1 07/20/23 01:06 V35527AMP
<706 µg/Kg - dry 706 2430
Benzoic Acid 1 07/20/23 01:06 V35527AMP
<128 µg/Kg - dry 128 803Benzyl alcohol 1 07/20/23 01:06 V35527AMP
<144 µg/Kg - dry 144 803Bis(2-Chloroethoxy)methane 1 07/20/23 01:06 V35527AMP
<130 µg/Kg - dry 130 803Bis(2-Chloroethyl)ether 1 07/20/23 01:06 V35527AMP
<165 µg/Kg - dry 165 401Bis(2-Chloroisopropyl)ether 1 07/20/23 01:06 V35527AMP
<146 µg/Kg - dry 146 803Bis(2-ethylhexyl)phthalate 1 07/20/23 01:06 V35527AMP
<133 µg/Kg - dry 133 8034-Bromophenyl phenyl ether 1 07/20/23 01:06 V35527AMP
<137 µg/Kg - dry 137 401
Butyl benzyl phthalate 1 07/20/23 01:06 V35527AMP
<112 µg/Kg - dry 112 8034-Chloro-3-methylphenol 1 07/20/23 01:06 V35527AMP
<136 µg/Kg - dry 136 4014-Chloroaniline 1 07/20/23 01:06 V35527AMP
<141 µg/Kg - dry 141 8032-Chloronaphthalene 1 07/20/23 01:06 V35527AMP
<119 µg/Kg - dry 119 8032-Chlorophenol 1 07/20/23 01:06 V35527AMP
<153 µg/Kg - dry 153 12204-Chlorophenyl phenyl ether 1 07/20/23 01:06 V35527AMP
<173 µg/Kg - dry 173 803Chrysene 1 07/20/23 01:06 V35527AMP
<280 µg/Kg - dry 280 803Dibenz(a,h)anthracene 1 07/20/23 01:06 V35527AMP
<145 µg/Kg - dry 145 803Dibenzofuran 1 07/20/23 01:06 V35527AMP
<115 µg/Kg - dry 115 8031,2-Dichlorobenzene 1 07/20/23 01:06 V35527AMP
<118 µg/Kg - dry 118 8031,3-Dichlorobenzene 1 07/20/23 01:06 V35527AMP
<119 µg/Kg - dry 119 4011,4-Dichlorobenzene 1 07/20/23 01:06 V35527AMP
<179 µg/Kg - dry 179 8033,3'-Dichlorobenzidine 1 07/20/23 01:06 V35527AMP
<117 µg/Kg - dry 117 8032,4-Dichlorophenol 1 07/20/23 01:06 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 57 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-Dup
89740 Matrix:
7/10/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<219 µg/Kg - dry 219 803Diethyl phthalate 1 07/20/23 01:06 V35527AMP
<212 µg/Kg - dry 212 803
Dimethyl phthalate 1 07/20/23 01:06 V35527AMP
<131 µg/Kg - dry 131 4012,4-Dimethylphenol 1 07/20/23 01:06 V35527AMP
<130 µg/Kg - dry 130 803Di-n-butyl phthalate 1 07/20/23 01:06 V35527AMP
<292 µg/Kg - dry 292 18204,6-Dinitro-2-methylphenol 1 07/20/23 01:06 V35527AMP
<633 µg/Kg - dry 633 18202,4-Dinitrophenol 1 07/20/23 01:06 V35527AMP
<118 µg/Kg - dry 118 8032,4-Dinitrotoluene 1 07/20/23 01:06 V35527AMP
<131 µg/Kg - dry 131 8032,6-Dinitrotoluene 1 07/20/23 01:06 V35527AMP
<174 µg/Kg - dry 174 401
Di-n-Octyl Phthalate 1 07/20/23 01:06 V35527AMP
<150 µg/Kg - dry 150 803Fluoranthene 1 07/20/23 01:06 V35527AMP
<156 µg/Kg - dry 156 803Fluorene 1 07/20/23 01:06 V35527AMP
<129 µg/Kg - dry 129 803Hexachlorobenzene 1 07/20/23 01:06 V35527AMP
<119 µg/Kg - dry 119 803Hexachlorobutadiene 1 07/20/23 01:06 V35527AMP
<191 µg/Kg - dry 191 803Hexachlorocyclopentadiene 1 07/20/23 01:06 V35527AMP
<96.4 µg/Kg - dry 96.4 803Hexachloroethane 1 07/20/23 01:06 V35527AMP
<218 µg/Kg - dry 218 803Indeno(1,2,3-cd)pyrene 1 07/20/23 01:06 V35527AMP
<232 µg/Kg - dry 232 803Isophorone 1 07/20/23 01:06 V35527AMP
460 J µg/Kg - dry 129 8031-Methylnaphthalene 1 07/20/23 01:06 V35527AMP
217 J µg/Kg - dry 122 8032-Methylnaphthalene 1 07/20/23 01:06 V35527AMP
<118 µg/Kg - dry 118 8032-Methylphenol 1 07/20/23 01:06 V35527AMP
<103 µg/Kg - dry 103 8033&4 Methylphenol 1 07/20/23 01:06 V35527AMP
<175 µg/Kg - dry 175 803Naphthalene 1 07/20/23 01:06 V35527AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 58 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:SB-Dup
89740 Matrix:
7/10/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V35515 07/19/23 09:50
<118 µg/Kg - dry 118 8032-Nitroaniline 1 07/20/23 01:06 V35527AMP
<146 µg/Kg - dry 146 803
3-Nitroaniline 1 07/20/23 01:06 V35527AMP
<114 µg/Kg - dry 114 4014-Nitroaniline 1 07/20/23 01:06 V35527AMP
<141 µg/Kg - dry 141 401Nitrobenzene 1 07/20/23 01:06 V35527AMP
<108 µg/Kg - dry 108 8032-Nitrophenol 1 07/20/23 01:06 V35527AMP
<142 µg/Kg - dry 142 8034-Nitrophenol 1 07/20/23 01:06 V35527AMP
<320 µg/Kg - dry 320 803N-Nitrosodimethylamine 1 07/20/23 01:06 V35527AMP
<220 µg/Kg - dry 220 803N-Nitrosodiphenylamine 1 07/20/23 01:06 V35527AMP
<144 µg/Kg - dry 144 803
N-Nitroso-di-n-propylamine 1 07/20/23 01:06 V35527AMP
<422 µg/Kg - dry 422 1220Pentachlorophenol 1 07/20/23 01:06 V35527AMP
258 J µg/Kg - dry 253 803Phenanthrene 1 07/20/23 01:06 V35527AMP
<136 µg/Kg - dry 136 803Phenol 1 07/20/23 01:06 V35527AMP
<163 µg/Kg - dry 163 803Pyrene 1 07/20/23 01:06 V35527AMP
<96.4 µg/Kg - dry 96.4 401Pyridine 1 07/20/23 01:06 V35527AMP
<130 µg/Kg - dry 130 8031,2,4-Trichlorobenzene 1 07/20/23 01:06 V35527AMP
<117 µg/Kg - dry 117 8032,4,5-Trichlorophenol 1 07/20/23 01:06 V35527AMP
<118 µg/Kg - dry 118 8032,4,6-Trichlorophenol 1 07/20/23 01:06 V35527AMP
8270ESurrogate: Phenol-d5 56.2 Limits: 34-121%07/20/23 01:061 AMP
Surrogate: 2-Fluorobiphenyl 80.8 Limits: 44-115%07/20/23 01:061 AMP V35527
Surrogate: 2-Fluorophenol 64.3 Limits: 35-115%07/20/23 01:061 AMP V35527
Surrogate: Nitrobenzene-d5 58.0 Limits: 37-122%07/20/23 01:061 AMP V35527
Surrogate: 4-Terphenyl-d14 92.8 Limits: 54-127%07/20/23 01:061 AMP V35527
Surrogate: 2,4,6-Tribromophenol 82.9 Limits: 39-132%07/20/23 01:061 AMP V35527
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 59 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:BG-1
89741 Matrix:
7/11/2023 15:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.7 %Moisture 1 07/19/23 18:30 SW-DRYWTCNC
0.705 mg/Kg - dry 0.163 0.231Chromium, Hexavalent 1 07/31/23 18:48 SW-7199SWB
1.62 mg/Kg - dry 0.0990 0.290Arsenic 5 07/21/23 17:06 6020BCPW
95.4 mg/Kg - dry 0.049 0.289Barium 5 07/21/23 17:06 6020BCPW
0.0805 J mg/Kg - dry 0.0301 0.290Cadmium 5 07/21/23 17:06 6020BCPW
68.9 mg/Kg - dry 0.134 0.289
Chromium 5 07/21/23 17:06 6020BCPW
17.1 mg/Kg - dry 0.0359 0.290Lead 5 07/21/23 17:06 6020BCPW
0.0290 J mg/Kg - dry 0.0139 0.0348Mercury (Total)1 07/19/23 16:28 7471BJKC
0.804 mg/Kg - dry 0.119 0.289Selenium 5 07/21/23 17:06 6020BCPW
0.0236 J mg/Kg - dry 0.0078 0.290Silver 5 07/21/23 17:06 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 60 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:BG-2
89742 Matrix:
7/11/2023 15:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.6 %Moisture 1 07/19/23 18:30 SW-DRYWTCNC
0.205 J mg/Kg - dry 0.175 0.248Chromium, Hexavalent 1 07/31/23 19:21 SW-7199SWB
1.62 mg/Kg - dry 0.106 0.311Arsenic 5 07/21/23 17:10 6020BCPW
90.8 mg/Kg - dry 0.053 0.310Barium 5 07/21/23 17:10 6020BCPW
<0.0323 mg/Kg - dry 0.0323 0.311Cadmium 5 07/21/23 17:10 6020BCPW
59.7 mg/Kg - dry 0.144 0.310
Chromium 5 07/21/23 17:10 6020BCPW
8.92 mg/Kg - dry 0.0385 0.311Lead 5 07/21/23 17:10 6020BCPW
0.0219 J mg/Kg - dry 0.0149 0.0373Mercury (Total)1 07/19/23 16:36 7471BJKC
0.758 mg/Kg - dry 0.128 0.310Selenium 5 07/21/23 17:10 6020BCPW
0.0162 J mg/Kg - dry 0.0083 0.311Silver 5 07/21/23 17:10 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 61 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:GW-DUP
89743 Matrix:
7/14/2023 0:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.297 µg/L 0.297 1.00Arsenic 1 07/21/23 21:57 6020BCPW
90.9 µg/L 0.453 1.00Barium 1 07/21/23 21:57 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 07/21/23 21:57 6020BCPW
<0.346 µg/L 0.346 1.00Chromium 1 07/21/23 21:57 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 07/21/23 21:57 6020BCPW
<0.00013 mg/L 0.00013 0.00020
Mercury (Total)1 07/20/23 13:31 7470AFDS
<0.703 µg/L 0.703 1.00Selenium 1 07/21/23 21:57 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 07/21/23 21:57 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 62 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:GW-DUP
89743 Matrix:
7/14/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
2.96 J µg/L 1.80 5.00Acetone 1 07/21/23 21:24 V35670MSA
<2.00 µg/L 2.00 5.00
Acrolein 1 07/21/23 21:24 V35670MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 07/21/23 21:24 V35670MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/21/23 21:24 V35670MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/21/23 21:24 V35670MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/21/23 21:24 V35670MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/21/23 21:24 V35670MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/21/23 21:24 V35670MSA
<0.280 µg/L 0.280 1.00
Bromomethane 1 07/21/23 21:24 V35670MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 07/21/23 21:24 V35670MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/21/23 21:24 V35670MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/21/23 21:24 V35670MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 07/21/23 21:24 V35670MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/21/23 21:24 V35670MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/21/23 21:24 V35670MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/21/23 21:24 V35670MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/21/23 21:24 V35670MSA
0.727 µg/L 0.220 0.500Chloroform 1 07/21/23 21:24 V35670MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/21/23 21:24 V35670MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/21/23 21:24 V35670MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/21/23 21:24 V35670MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 07/21/23 21:24 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 63 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:GW-DUP
89743 Matrix:
7/14/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/21/23 21:24 V35670MSA
<0.200 µg/L 0.200 0.500
1,2-Dibromoethane 1 07/21/23 21:24 V35670MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/21/23 21:24 V35670MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/21/23 21:24 V35670MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/21/23 21:24 V35670MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/21/23 21:24 V35670MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/21/23 21:24 V35670MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/21/23 21:24 V35670MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 07/21/23 21:24 V35670MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/21/23 21:24 V35670MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/21/23 21:24 V35670MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/21/23 21:24 V35670MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/21/23 21:24 V35670MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/21/23 21:24 V35670MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/21/23 21:24 V35670MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/21/23 21:24 V35670MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/21/23 21:24 V35670MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/21/23 21:24 V35670MSA
<42.0 µg/L 42.0 200Ethanol 1 07/21/23 21:24 V35670MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/21/23 21:24 V35670MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 07/21/23 21:24 V35670MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 07/21/23 21:24 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 64 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:GW-DUP
89743 Matrix:
7/14/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 07/21/23 21:24 V35670MSA
<0.380 µg/L 0.380 5.00
2-Hexanone 1 07/21/23 21:24 V35670MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 07/21/23 21:24 V35670MSA
0.237 J µg/L 0.089 0.5004-Isopropyl toluene 1 07/21/23 21:24 V35670MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/21/23 21:24 V35670MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 07/21/23 21:24 V35670MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 07/21/23 21:24 V35670MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 07/21/23 21:24 V35670MSA
<0.470 µg/L 0.470 1.00
Naphthalene 1 07/21/23 21:24 V35670MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/21/23 21:24 V35670MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/21/23 21:24 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/21/23 21:24 V35670MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/21/23 21:24 V35670MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/21/23 21:24 V35670MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/21/23 21:24 V35670MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 07/21/23 21:24 V35670MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 07/21/23 21:24 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/21/23 21:24 V35670MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/21/23 21:24 V35670MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/21/23 21:24 V35670MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/21/23 21:24 V35670MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 07/21/23 21:24 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 65 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:GW-DUP
89743 Matrix:
7/14/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/21/23 21:24 V35670MSA
<1.00 µg/L 1.00 2.00
Vinyl Acetate 1 07/21/23 21:24 V35670MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/21/23 21:24 V35670MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/21/23 21:24 V35670MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/21/23 21:24 V35670MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/21/23 21:24 V35670
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 80-124%07/21/23 21:241 MSA V35670
Surrogate: Dibromofluoromethane 98.4 Limits: 75-129%07/21/23 21:241 MSA V35670
Surrogate: 1,2-Dichloroethane - d4 99.8 Limits: 63-136%07/21/23 21:241 MSA V35670
Surrogate: Toluene-d8 94.4 Limits: 77-123%07/21/23 21:241 MSA V35670
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<0.302 µg/L 0.302 2.00Acenaphthene 1 07/21/23 15:34 V35550AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 07/21/23 15:34 V35550AMP
<2.05 µg/L 2.05 5.00Aniline 1 07/21/23 15:34 V35550AMP
<0.836 µg/L 0.836 2.00Anthracene 1 07/21/23 15:34 V35550AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 07/21/23 15:34 V35550AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 07/21/23 15:34 V35550AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 07/21/23 15:34 V35550AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 07/21/23 15:34 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 66 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:GW-DUP
89743 Matrix:
7/14/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 07/21/23 15:34 V35550AMP
<1.10 µg/L 1.10 10.0
Benzoic Acid 1 07/21/23 15:34 V35550AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 07/21/23 15:34 V35550AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 07/21/23 15:34 V35550AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 07/21/23 15:34 V35550AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 07/21/23 15:34 V35550AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 07/21/23 15:34 V35550AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 07/21/23 15:34 V35550AMP
<1.83 µg/L 1.83 5.00
Butyl benzyl phthalate 1 07/21/23 15:34 V35550AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 07/21/23 15:34 V35550AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 07/21/23 15:34 V35550AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 07/21/23 15:34 V35550AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 07/21/23 15:34 V35550AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 07/21/23 15:34 V35550AMP
<0.405 µg/L 0.405 2.00Chrysene 1 07/21/23 15:34 V35550AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 07/21/23 15:34 V35550AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 07/21/23 15:34 V35550AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 07/21/23 15:34 V35550AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 07/21/23 15:34 V35550AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 07/21/23 15:34 V35550AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 07/21/23 15:34 V35550AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 07/21/23 15:34 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 67 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:GW-DUP
89743 Matrix:
7/14/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
0.943 J µg/L 0.745 5.00Diethyl phthalate 1 07/21/23 15:34 V35550AMP
<0.939 µg/L 0.939 5.00
Dimethyl phthalate 1 07/21/23 15:34 V35550AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 07/21/23 15:34 V35550AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 07/21/23 15:34 V35550AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 07/21/23 15:34 V35550AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 07/21/23 15:34 V35550AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 07/21/23 15:34 V35550AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 07/21/23 15:34 V35550AMP
<1.65 µg/L 1.65 5.00
Di-n-Octyl Phthalate 1 07/21/23 15:34 V35550AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 07/21/23 15:34 V35550AMP
<0.807 µg/L 0.807 2.00Fluorene 1 07/21/23 15:34 V35550AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 07/21/23 15:34 V35550AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 07/21/23 15:34 V35550AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 07/21/23 15:34 V35550AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 07/21/23 15:34 V35550AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 07/21/23 15:34 V35550AMP
<0.444 µg/L 0.444 5.00Isophorone 1 07/21/23 15:34 V35550AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 07/21/23 15:34 V35550AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 07/21/23 15:34 V35550AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 07/21/23 15:34 V35550AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 07/21/23 15:34 V35550AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 07/21/23 15:34 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 68 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:GW-DUP
89743 Matrix:
7/14/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<1.39 µg/L 1.39 5.002-Nitroaniline 1 07/21/23 15:34 V35550AMP
<1.39 µg/L 1.39 5.00
3-Nitroaniline 1 07/21/23 15:34 V35550AMP
<1.53 µg/L 1.53 5.004-Nitroaniline 1 07/21/23 15:34 V35550AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 07/21/23 15:34 V35550AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 07/21/23 15:34 V35550AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 07/21/23 15:34 V35550AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 07/21/23 15:34 V35550AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 07/21/23 15:34 V35550AMP
<0.641 µg/L 0.641 5.00
N-Nitroso-di-n-propylamine 1 07/21/23 15:34 V35550AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 07/21/23 15:34 V35550AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 07/21/23 15:34 V35550AMP
<0.651 µg/L 0.651 5.00Phenol 1 07/21/23 15:34 V35550AMP
<0.434 µg/L 0.434 2.00Pyrene 1 07/21/23 15:34 V35550AMP
<1.20 µg/L 1.20 5.00Pyridine 1 07/21/23 15:34 V35550AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 07/21/23 15:34 V35550AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 07/21/23 15:34 V35550AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 07/21/23 15:34 V35550AMP
8270ESurrogate: Phenol-d5 34.7 Limits: 11-100%07/21/23 15:341 AMP
Surrogate: 2-Fluorobiphenyl 128 *Limits: 44-119%07/21/23 15:341 AMP V35550
Surrogate: 2-Fluorophenol 31.1 Limits: 19-119%07/21/23 15:341 AMP V35550
Surrogate: Nitrobenzene-d5 111 Limits: 44-120%07/21/23 15:341 AMP V35550
Surrogate: 4-Terphenyl-d14 187 *Limits: 50-134%07/21/23 15:341 AMP V35550
Surrogate: 2,4,6-Tribromophenol 88.1 Limits: 43-140%07/21/23 15:341 AMP V35550
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 69 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-1
89744 Matrix:
7/14/2023 15:05
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.297 µg/L 0.297 1.00Arsenic 1 07/21/23 22:08 6020BCPW
77.7 µg/L 0.453 1.00Barium 1 07/21/23 22:08 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 07/21/23 22:08 6020BCPW
0.481 J µg/L 0.346 1.00Chromium 1 07/21/23 22:08 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 07/21/23 22:08 6020BCPW
<0.00013 mg/L 0.00013 0.00020
Mercury (Total)1 07/20/23 13:33 7470AFDS
<0.703 µg/L 0.703 1.00Selenium 1 07/21/23 22:08 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 07/21/23 22:08 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 70 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-1
89744 Matrix:
7/14/2023 15:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.80 µg/L 1.80 5.00Acetone 1 07/21/23 21:49 V35670MSA
<2.00 µg/L 2.00 5.00
Acrolein 1 07/21/23 21:49 V35670MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 07/21/23 21:49 V35670MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/21/23 21:49 V35670MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/21/23 21:49 V35670MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/21/23 21:49 V35670MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/21/23 21:49 V35670MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/21/23 21:49 V35670MSA
<0.280 µg/L 0.280 1.00
Bromomethane 1 07/21/23 21:49 V35670MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 07/21/23 21:49 V35670MSA
1.78 µg/L 0.200 0.500sec-Butyl benzene 1 07/21/23 21:49 V35670MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/21/23 21:49 V35670MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 07/21/23 21:49 V35670MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/21/23 21:49 V35670MSA
10.7 µg/L 0.190 0.500Chlorobenzene 1 07/21/23 21:49 V35670MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/21/23 21:49 V35670MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/21/23 21:49 V35670MSA
0.379 J µg/L 0.220 0.500Chloroform 1 07/21/23 21:49 V35670MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/21/23 21:49 V35670MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/21/23 21:49 V35670MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/21/23 21:49 V35670MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 07/21/23 21:49 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 71 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-1
89744 Matrix:
7/14/2023 15:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/21/23 21:49 V35670MSA
<0.200 µg/L 0.200 0.500
1,2-Dibromoethane 1 07/21/23 21:49 V35670MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/21/23 21:49 V35670MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/21/23 21:49 V35670MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/21/23 21:49 V35670MSA
0.951 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/21/23 21:49 V35670MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/21/23 21:49 V35670MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/21/23 21:49 V35670MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 07/21/23 21:49 V35670MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/21/23 21:49 V35670MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/21/23 21:49 V35670MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/21/23 21:49 V35670MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/21/23 21:49 V35670MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/21/23 21:49 V35670MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/21/23 21:49 V35670MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/21/23 21:49 V35670MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/21/23 21:49 V35670MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/21/23 21:49 V35670MSA
<42.0 µg/L 42.0 200Ethanol 1 07/21/23 21:49 V35670MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/21/23 21:49 V35670MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 07/21/23 21:49 V35670MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 07/21/23 21:49 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 72 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-1
89744 Matrix:
7/14/2023 15:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 07/21/23 21:49 V35670MSA
<0.380 µg/L 0.380 5.00
2-Hexanone 1 07/21/23 21:49 V35670MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 07/21/23 21:49 V35670MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/21/23 21:49 V35670MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/21/23 21:49 V35670MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 07/21/23 21:49 V35670MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 07/21/23 21:49 V35670MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 07/21/23 21:49 V35670MSA
<0.470 µg/L 0.470 1.00
Naphthalene 1 07/21/23 21:49 V35670MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/21/23 21:49 V35670MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/21/23 21:49 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/21/23 21:49 V35670MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/21/23 21:49 V35670MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/21/23 21:49 V35670MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/21/23 21:49 V35670MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 07/21/23 21:49 V35670MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 07/21/23 21:49 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/21/23 21:49 V35670MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/21/23 21:49 V35670MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/21/23 21:49 V35670MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/21/23 21:49 V35670MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 07/21/23 21:49 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 73 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-1
89744 Matrix:
7/14/2023 15:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/21/23 21:49 V35670MSA
<1.00 µg/L 1.00 2.00
Vinyl Acetate 1 07/21/23 21:49 V35670MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/21/23 21:49 V35670MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/21/23 21:49 V35670MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/21/23 21:49 V35670MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/21/23 21:49 V35670
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 80-124%07/21/23 21:491 MSA V35670
Surrogate: Dibromofluoromethane 98.8 Limits: 75-129%07/21/23 21:491 MSA V35670
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 63-136%07/21/23 21:491 MSA V35670
Surrogate: Toluene-d8 95.0 Limits: 77-123%07/21/23 21:491 MSA V35670
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<0.302 µg/L 0.302 2.00Acenaphthene 1 07/21/23 17:06 V35550AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 07/21/23 17:06 V35550AMP
<2.05 µg/L 2.05 5.00Aniline 1 07/21/23 17:06 V35550AMP
<0.836 µg/L 0.836 2.00Anthracene 1 07/21/23 17:06 V35550AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 07/21/23 17:06 V35550AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 07/21/23 17:06 V35550AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 07/21/23 17:06 V35550AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 07/21/23 17:06 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 74 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-1
89744 Matrix:
7/14/2023 15:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 07/21/23 17:06 V35550AMP
<1.10 µg/L 1.10 10.0
Benzoic Acid 1 07/21/23 17:06 V35550AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 07/21/23 17:06 V35550AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 07/21/23 17:06 V35550AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 07/21/23 17:06 V35550AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 07/21/23 17:06 V35550AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 07/21/23 17:06 V35550AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 07/21/23 17:06 V35550AMP
<1.83 µg/L 1.83 5.00
Butyl benzyl phthalate 1 07/21/23 17:06 V35550AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 07/21/23 17:06 V35550AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 07/21/23 17:06 V35550AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 07/21/23 17:06 V35550AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 07/21/23 17:06 V35550AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 07/21/23 17:06 V35550AMP
<0.405 µg/L 0.405 2.00Chrysene 1 07/21/23 17:06 V35550AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 07/21/23 17:06 V35550AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 07/21/23 17:06 V35550AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 07/21/23 17:06 V35550AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 07/21/23 17:06 V35550AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 07/21/23 17:06 V35550AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 07/21/23 17:06 V35550AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 07/21/23 17:06 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 75 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-1
89744 Matrix:
7/14/2023 15:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 07/21/23 17:06 V35550AMP
<0.939 µg/L 0.939 5.00
Dimethyl phthalate 1 07/21/23 17:06 V35550AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 07/21/23 17:06 V35550AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 07/21/23 17:06 V35550AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 07/21/23 17:06 V35550AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 07/21/23 17:06 V35550AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 07/21/23 17:06 V35550AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 07/21/23 17:06 V35550AMP
<1.65 µg/L 1.65 5.00
Di-n-Octyl Phthalate 1 07/21/23 17:06 V35550AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 07/21/23 17:06 V35550AMP
<0.807 µg/L 0.807 2.00Fluorene 1 07/21/23 17:06 V35550AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 07/21/23 17:06 V35550AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 07/21/23 17:06 V35550AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 07/21/23 17:06 V35550AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 07/21/23 17:06 V35550AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 07/21/23 17:06 V35550AMP
<0.444 µg/L 0.444 5.00Isophorone 1 07/21/23 17:06 V35550AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 07/21/23 17:06 V35550AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 07/21/23 17:06 V35550AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 07/21/23 17:06 V35550AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 07/21/23 17:06 V35550AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 07/21/23 17:06 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 76 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-1
89744 Matrix:
7/14/2023 15:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<1.39 µg/L 1.39 5.002-Nitroaniline 1 07/21/23 17:06 V35550AMP
<1.39 µg/L 1.39 5.00
3-Nitroaniline 1 07/21/23 17:06 V35550AMP
<1.53 µg/L 1.53 5.004-Nitroaniline 1 07/21/23 17:06 V35550AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 07/21/23 17:06 V35550AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 07/21/23 17:06 V35550AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 07/21/23 17:06 V35550AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 07/21/23 17:06 V35550AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 07/21/23 17:06 V35550AMP
<0.641 µg/L 0.641 5.00
N-Nitroso-di-n-propylamine 1 07/21/23 17:06 V35550AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 07/21/23 17:06 V35550AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 07/21/23 17:06 V35550AMP
<0.651 µg/L 0.651 5.00Phenol 1 07/21/23 17:06 V35550AMP
<0.434 µg/L 0.434 2.00Pyrene 1 07/21/23 17:06 V35550AMP
<1.20 µg/L 1.20 5.00Pyridine 1 07/21/23 17:06 V35550AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 07/21/23 17:06 V35550AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 07/21/23 17:06 V35550AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 07/21/23 17:06 V35550AMP
8270ESurrogate: Phenol-d5 15.2 Limits: 11-100%07/21/23 17:061 AMP
Surrogate: 2-Fluorobiphenyl 51.0 Limits: 44-119%07/21/23 17:061 AMP V35550
Surrogate: 2-Fluorophenol 24.8 Limits: 19-119%07/21/23 17:061 AMP V35550
Surrogate: Nitrobenzene-d5 43.8 *Limits: 44-120%07/21/23 17:061 AMP V35550
Surrogate: 4-Terphenyl-d14 83.8 Limits: 50-134%07/21/23 17:061 AMP V35550
Surrogate: 2,4,6-Tribromophenol 75.5 Limits: 43-140%07/21/23 17:061 AMP V35550
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 77 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-2
89745 Matrix:
7/14/2023 13:40
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.297 µg/L 0.297 1.00Arsenic 1 07/21/23 22:12 6020BCPW
90.9 µg/L 0.453 1.00Barium 1 07/21/23 22:12 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 07/21/23 22:12 6020BCPW
<0.346 µg/L 0.346 1.00Chromium 1 07/21/23 22:12 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 07/21/23 22:12 6020BCPW
<0.00013 mg/L 0.00013 0.00020
Mercury (Total)1 07/20/23 13:37 7470AFDS
<0.703 µg/L 0.703 1.00Selenium 1 07/21/23 22:12 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 07/21/23 22:12 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 78 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-2
89745 Matrix:
7/14/2023 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
3.34 J µg/L 1.80 5.00Acetone 1 07/21/23 22:14 V35670MSA
<2.00 µg/L 2.00 5.00
Acrolein 1 07/21/23 22:14 V35670MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 07/21/23 22:14 V35670MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/21/23 22:14 V35670MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/21/23 22:14 V35670MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/21/23 22:14 V35670MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/21/23 22:14 V35670MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/21/23 22:14 V35670MSA
<0.280 µg/L 0.280 1.00
Bromomethane 1 07/21/23 22:14 V35670MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 07/21/23 22:14 V35670MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/21/23 22:14 V35670MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/21/23 22:14 V35670MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 07/21/23 22:14 V35670MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/21/23 22:14 V35670MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/21/23 22:14 V35670MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/21/23 22:14 V35670MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/21/23 22:14 V35670MSA
0.691 µg/L 0.220 0.500Chloroform 1 07/21/23 22:14 V35670MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/21/23 22:14 V35670MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/21/23 22:14 V35670MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/21/23 22:14 V35670MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 07/21/23 22:14 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 79 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-2
89745 Matrix:
7/14/2023 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/21/23 22:14 V35670MSA
<0.200 µg/L 0.200 0.500
1,2-Dibromoethane 1 07/21/23 22:14 V35670MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/21/23 22:14 V35670MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/21/23 22:14 V35670MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/21/23 22:14 V35670MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/21/23 22:14 V35670MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/21/23 22:14 V35670MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/21/23 22:14 V35670MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 07/21/23 22:14 V35670MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/21/23 22:14 V35670MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/21/23 22:14 V35670MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/21/23 22:14 V35670MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/21/23 22:14 V35670MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/21/23 22:14 V35670MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/21/23 22:14 V35670MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/21/23 22:14 V35670MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/21/23 22:14 V35670MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/21/23 22:14 V35670MSA
<42.0 µg/L 42.0 200Ethanol 1 07/21/23 22:14 V35670MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/21/23 22:14 V35670MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 07/21/23 22:14 V35670MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 07/21/23 22:14 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 80 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-2
89745 Matrix:
7/14/2023 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 07/21/23 22:14 V35670MSA
<0.380 µg/L 0.380 5.00
2-Hexanone 1 07/21/23 22:14 V35670MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 07/21/23 22:14 V35670MSA
0.236 J µg/L 0.089 0.5004-Isopropyl toluene 1 07/21/23 22:14 V35670MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/21/23 22:14 V35670MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 07/21/23 22:14 V35670MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 07/21/23 22:14 V35670MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 07/21/23 22:14 V35670MSA
<0.470 µg/L 0.470 1.00
Naphthalene 1 07/21/23 22:14 V35670MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/21/23 22:14 V35670MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/21/23 22:14 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/21/23 22:14 V35670MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/21/23 22:14 V35670MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/21/23 22:14 V35670MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/21/23 22:14 V35670MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 07/21/23 22:14 V35670MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 07/21/23 22:14 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/21/23 22:14 V35670MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/21/23 22:14 V35670MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/21/23 22:14 V35670MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/21/23 22:14 V35670MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 07/21/23 22:14 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 81 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-2
89745 Matrix:
7/14/2023 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/21/23 22:14 V35670MSA
<1.00 µg/L 1.00 2.00
Vinyl Acetate 1 07/21/23 22:14 V35670MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/21/23 22:14 V35670MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/21/23 22:14 V35670MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/21/23 22:14 V35670MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/21/23 22:14 V35670
Surrogate: 4-Bromofluorobenzene 100 Limits: 80-124%07/21/23 22:141 MSA V35670
Surrogate: Dibromofluoromethane 99.8 Limits: 75-129%07/21/23 22:141 MSA V35670
Surrogate: 1,2-Dichloroethane - d4 99.4 Limits: 63-136%07/21/23 22:141 MSA V35670
Surrogate: Toluene-d8 93.6 Limits: 77-123%07/21/23 22:141 MSA V35670
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<0.302 µg/L 0.302 2.00Acenaphthene 1 07/21/23 16:43 V35550AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 07/21/23 16:43 V35550AMP
<2.05 µg/L 2.05 5.00Aniline 1 07/21/23 16:43 V35550AMP
<0.836 µg/L 0.836 2.00Anthracene 1 07/21/23 16:43 V35550AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 07/21/23 16:43 V35550AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 07/21/23 16:43 V35550AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 07/21/23 16:43 V35550AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 07/21/23 16:43 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 82 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-2
89745 Matrix:
7/14/2023 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 07/21/23 16:43 V35550AMP
<1.10 µg/L 1.10 10.0
Benzoic Acid 1 07/21/23 16:43 V35550AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 07/21/23 16:43 V35550AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 07/21/23 16:43 V35550AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 07/21/23 16:43 V35550AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 07/21/23 16:43 V35550AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 07/21/23 16:43 V35550AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 07/21/23 16:43 V35550AMP
<1.83 µg/L 1.83 5.00
Butyl benzyl phthalate 1 07/21/23 16:43 V35550AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 07/21/23 16:43 V35550AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 07/21/23 16:43 V35550AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 07/21/23 16:43 V35550AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 07/21/23 16:43 V35550AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 07/21/23 16:43 V35550AMP
<0.405 µg/L 0.405 2.00Chrysene 1 07/21/23 16:43 V35550AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 07/21/23 16:43 V35550AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 07/21/23 16:43 V35550AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 07/21/23 16:43 V35550AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 07/21/23 16:43 V35550AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 07/21/23 16:43 V35550AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 07/21/23 16:43 V35550AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 07/21/23 16:43 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 83 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-2
89745 Matrix:
7/14/2023 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
0.871 J µg/L 0.745 5.00Diethyl phthalate 1 07/21/23 16:43 V35550AMP
<0.939 µg/L 0.939 5.00
Dimethyl phthalate 1 07/21/23 16:43 V35550AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 07/21/23 16:43 V35550AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 07/21/23 16:43 V35550AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 07/21/23 16:43 V35550AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 07/21/23 16:43 V35550AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 07/21/23 16:43 V35550AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 07/21/23 16:43 V35550AMP
<1.65 µg/L 1.65 5.00
Di-n-Octyl Phthalate 1 07/21/23 16:43 V35550AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 07/21/23 16:43 V35550AMP
<0.807 µg/L 0.807 2.00Fluorene 1 07/21/23 16:43 V35550AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 07/21/23 16:43 V35550AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 07/21/23 16:43 V35550AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 07/21/23 16:43 V35550AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 07/21/23 16:43 V35550AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 07/21/23 16:43 V35550AMP
<0.444 µg/L 0.444 5.00Isophorone 1 07/21/23 16:43 V35550AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 07/21/23 16:43 V35550AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 07/21/23 16:43 V35550AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 07/21/23 16:43 V35550AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 07/21/23 16:43 V35550AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 07/21/23 16:43 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 84 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-2
89745 Matrix:
7/14/2023 13:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<1.39 µg/L 1.39 5.002-Nitroaniline 1 07/21/23 16:43 V35550AMP
<1.39 µg/L 1.39 5.00
3-Nitroaniline 1 07/21/23 16:43 V35550AMP
<1.53 µg/L 1.53 5.004-Nitroaniline 1 07/21/23 16:43 V35550AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 07/21/23 16:43 V35550AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 07/21/23 16:43 V35550AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 07/21/23 16:43 V35550AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 07/21/23 16:43 V35550AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 07/21/23 16:43 V35550AMP
<0.641 µg/L 0.641 5.00
N-Nitroso-di-n-propylamine 1 07/21/23 16:43 V35550AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 07/21/23 16:43 V35550AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 07/21/23 16:43 V35550AMP
<0.651 µg/L 0.651 5.00Phenol 1 07/21/23 16:43 V35550AMP
<0.434 µg/L 0.434 2.00Pyrene 1 07/21/23 16:43 V35550AMP
<1.20 µg/L 1.20 5.00Pyridine 1 07/21/23 16:43 V35550AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 07/21/23 16:43 V35550AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 07/21/23 16:43 V35550AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 07/21/23 16:43 V35550AMP
8270ESurrogate: Phenol-d5 17.6 Limits: 11-100%07/21/23 16:431 AMP
Surrogate: 2-Fluorobiphenyl 60.6 Limits: 44-119%07/21/23 16:431 AMP V35550
Surrogate: 2-Fluorophenol 28.5 Limits: 19-119%07/21/23 16:431 AMP V35550
Surrogate: Nitrobenzene-d5 51.0 Limits: 44-120%07/21/23 16:431 AMP V35550
Surrogate: 4-Terphenyl-d14 84.6 Limits: 50-134%07/21/23 16:431 AMP V35550
Surrogate: 2,4,6-Tribromophenol 77.8 Limits: 43-140%07/21/23 16:431 AMP V35550
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 85 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-3
89746 Matrix:
7/14/2023 12:35
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.297 µg/L 0.297 1.00Arsenic 1 07/21/23 22:16 6020BCPW
41.8 µg/L 0.453 1.00Barium 1 07/21/23 22:16 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 07/21/23 22:16 6020BCPW
0.387 J µg/L 0.346 1.00Chromium 1 07/21/23 22:16 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 07/21/23 22:16 6020BCPW
<0.00013 mg/L 0.00013 0.00020
Mercury (Total)1 07/20/23 13:39 7470AFDS
<0.703 µg/L 0.703 1.00Selenium 1 07/21/23 22:16 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 07/21/23 22:16 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 86 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-3
89746 Matrix:
7/14/2023 12:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.80 µg/L 1.80 5.00Acetone 1 07/21/23 22:38 V35670MSA
<2.00 µg/L 2.00 5.00
Acrolein 1 07/21/23 22:38 V35670MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 07/21/23 22:38 V35670MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/21/23 22:38 V35670MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/21/23 22:38 V35670MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/21/23 22:38 V35670MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/21/23 22:38 V35670MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/21/23 22:38 V35670MSA
<0.280 µg/L 0.280 1.00
Bromomethane 1 07/21/23 22:38 V35670MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 07/21/23 22:38 V35670MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/21/23 22:38 V35670MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/21/23 22:38 V35670MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 07/21/23 22:38 V35670MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/21/23 22:38 V35670MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/21/23 22:38 V35670MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/21/23 22:38 V35670MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/21/23 22:38 V35670MSA
16.5 µg/L 0.220 0.500Chloroform 1 07/21/23 22:38 V35670MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/21/23 22:38 V35670MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/21/23 22:38 V35670MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/21/23 22:38 V35670MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 07/21/23 22:38 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 87 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-3
89746 Matrix:
7/14/2023 12:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/21/23 22:38 V35670MSA
<0.200 µg/L 0.200 0.500
1,2-Dibromoethane 1 07/21/23 22:38 V35670MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/21/23 22:38 V35670MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/21/23 22:38 V35670MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/21/23 22:38 V35670MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/21/23 22:38 V35670MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/21/23 22:38 V35670MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/21/23 22:38 V35670MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 07/21/23 22:38 V35670MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/21/23 22:38 V35670MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/21/23 22:38 V35670MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/21/23 22:38 V35670MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/21/23 22:38 V35670MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/21/23 22:38 V35670MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/21/23 22:38 V35670MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/21/23 22:38 V35670MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/21/23 22:38 V35670MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/21/23 22:38 V35670MSA
<42.0 µg/L 42.0 200Ethanol 1 07/21/23 22:38 V35670MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/21/23 22:38 V35670MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 07/21/23 22:38 V35670MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 07/21/23 22:38 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 88 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-3
89746 Matrix:
7/14/2023 12:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 07/21/23 22:38 V35670MSA
<0.380 µg/L 0.380 5.00
2-Hexanone 1 07/21/23 22:38 V35670MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 07/21/23 22:38 V35670MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/21/23 22:38 V35670MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/21/23 22:38 V35670MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 07/21/23 22:38 V35670MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 07/21/23 22:38 V35670MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 07/21/23 22:38 V35670MSA
<0.470 µg/L 0.470 1.00
Naphthalene 1 07/21/23 22:38 V35670MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/21/23 22:38 V35670MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/21/23 22:38 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/21/23 22:38 V35670MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/21/23 22:38 V35670MSA
0.469 J µg/L 0.220 0.500Tetrachloroethene 1 07/21/23 22:38 V35670MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/21/23 22:38 V35670MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 07/21/23 22:38 V35670MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 07/21/23 22:38 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/21/23 22:38 V35670MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/21/23 22:38 V35670MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/21/23 22:38 V35670MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/21/23 22:38 V35670MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 07/21/23 22:38 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 89 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-3
89746 Matrix:
7/14/2023 12:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/21/23 22:38 V35670MSA
<1.00 µg/L 1.00 2.00
Vinyl Acetate 1 07/21/23 22:38 V35670MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/21/23 22:38 V35670MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/21/23 22:38 V35670MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/21/23 22:38 V35670MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/21/23 22:38 V35670
Surrogate: 4-Bromofluorobenzene 100 Limits: 80-124%07/21/23 22:381 MSA V35670
Surrogate: Dibromofluoromethane 99.2 Limits: 75-129%07/21/23 22:381 MSA V35670
Surrogate: 1,2-Dichloroethane - d4 99.6 Limits: 63-136%07/21/23 22:381 MSA V35670
Surrogate: Toluene-d8 93.8 Limits: 77-123%07/21/23 22:381 MSA V35670
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<0.302 µg/L 0.302 2.00Acenaphthene 1 07/21/23 16:20 V35550AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 07/21/23 16:20 V35550AMP
<2.05 µg/L 2.05 5.00Aniline 1 07/21/23 16:20 V35550AMP
<0.836 µg/L 0.836 2.00Anthracene 1 07/21/23 16:20 V35550AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 07/21/23 16:20 V35550AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 07/21/23 16:20 V35550AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 07/21/23 16:20 V35550AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 07/21/23 16:20 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 90 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-3
89746 Matrix:
7/14/2023 12:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 07/21/23 16:20 V35550AMP
<1.10 µg/L 1.10 10.0
Benzoic Acid 1 07/21/23 16:20 V35550AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 07/21/23 16:20 V35550AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 07/21/23 16:20 V35550AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 07/21/23 16:20 V35550AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 07/21/23 16:20 V35550AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 07/21/23 16:20 V35550AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 07/21/23 16:20 V35550AMP
<1.83 µg/L 1.83 5.00
Butyl benzyl phthalate 1 07/21/23 16:20 V35550AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 07/21/23 16:20 V35550AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 07/21/23 16:20 V35550AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 07/21/23 16:20 V35550AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 07/21/23 16:20 V35550AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 07/21/23 16:20 V35550AMP
<0.405 µg/L 0.405 2.00Chrysene 1 07/21/23 16:20 V35550AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 07/21/23 16:20 V35550AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 07/21/23 16:20 V35550AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 07/21/23 16:20 V35550AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 07/21/23 16:20 V35550AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 07/21/23 16:20 V35550AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 07/21/23 16:20 V35550AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 07/21/23 16:20 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 91 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-3
89746 Matrix:
7/14/2023 12:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 07/21/23 16:20 V35550AMP
<0.939 µg/L 0.939 5.00
Dimethyl phthalate 1 07/21/23 16:20 V35550AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 07/21/23 16:20 V35550AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 07/21/23 16:20 V35550AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 07/21/23 16:20 V35550AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 07/21/23 16:20 V35550AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 07/21/23 16:20 V35550AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 07/21/23 16:20 V35550AMP
<1.65 µg/L 1.65 5.00
Di-n-Octyl Phthalate 1 07/21/23 16:20 V35550AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 07/21/23 16:20 V35550AMP
<0.807 µg/L 0.807 2.00Fluorene 1 07/21/23 16:20 V35550AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 07/21/23 16:20 V35550AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 07/21/23 16:20 V35550AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 07/21/23 16:20 V35550AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 07/21/23 16:20 V35550AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 07/21/23 16:20 V35550AMP
<0.444 µg/L 0.444 5.00Isophorone 1 07/21/23 16:20 V35550AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 07/21/23 16:20 V35550AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 07/21/23 16:20 V35550AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 07/21/23 16:20 V35550AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 07/21/23 16:20 V35550AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 07/21/23 16:20 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 92 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-3
89746 Matrix:
7/14/2023 12:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<1.39 µg/L 1.39 5.002-Nitroaniline 1 07/21/23 16:20 V35550AMP
<1.39 µg/L 1.39 5.00
3-Nitroaniline 1 07/21/23 16:20 V35550AMP
<1.53 µg/L 1.53 5.004-Nitroaniline 1 07/21/23 16:20 V35550AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 07/21/23 16:20 V35550AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 07/21/23 16:20 V35550AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 07/21/23 16:20 V35550AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 07/21/23 16:20 V35550AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 07/21/23 16:20 V35550AMP
<0.641 µg/L 0.641 5.00
N-Nitroso-di-n-propylamine 1 07/21/23 16:20 V35550AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 07/21/23 16:20 V35550AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 07/21/23 16:20 V35550AMP
<0.651 µg/L 0.651 5.00Phenol 1 07/21/23 16:20 V35550AMP
<0.434 µg/L 0.434 2.00Pyrene 1 07/21/23 16:20 V35550AMP
<1.20 µg/L 1.20 5.00Pyridine 1 07/21/23 16:20 V35550AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 07/21/23 16:20 V35550AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 07/21/23 16:20 V35550AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 07/21/23 16:20 V35550AMP
8270ESurrogate: Phenol-d5 15.4 Limits: 11-100%07/21/23 16:201 AMP
Surrogate: 2-Fluorobiphenyl 52.0 Limits: 44-119%07/21/23 16:201 AMP V35550
Surrogate: 2-Fluorophenol 25.4 Limits: 19-119%07/21/23 16:201 AMP V35550
Surrogate: Nitrobenzene-d5 48.6 Limits: 44-120%07/21/23 16:201 AMP V35550
Surrogate: 4-Terphenyl-d14 84.6 Limits: 50-134%07/21/23 16:201 AMP V35550
Surrogate: 2,4,6-Tribromophenol 65.0 Limits: 43-140%07/21/23 16:201 AMP V35550
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 93 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-5
89747 Matrix:
7/14/2023 11:10
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
0.421 J µg/L 0.297 1.00Arsenic 1 07/21/23 22:20 6020BCPW
108 µg/L 0.453 1.00Barium 1 07/21/23 22:20 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 07/21/23 22:20 6020BCPW
<0.346 µg/L 0.346 1.00Chromium 1 07/21/23 22:20 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 07/21/23 22:20 6020BCPW
<0.00013 mg/L 0.00013 0.00020
Mercury (Total)1 07/20/23 13:40 7470AFDS
<0.703 µg/L 0.703 1.00Selenium 1 07/21/23 22:20 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 07/21/23 22:20 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 94 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-5
89747 Matrix:
7/14/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
16.3 µg/L 1.80 5.00Acetone 1 07/21/23 23:03 V35670MSA
<2.00 µg/L 2.00 5.00
Acrolein 1 07/21/23 23:03 V35670MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 07/21/23 23:03 V35670MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/21/23 23:03 V35670MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/21/23 23:03 V35670MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/21/23 23:03 V35670MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/21/23 23:03 V35670MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/21/23 23:03 V35670MSA
<0.280 µg/L 0.280 1.00
Bromomethane 1 07/21/23 23:03 V35670MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 07/21/23 23:03 V35670MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/21/23 23:03 V35670MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/21/23 23:03 V35670MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 07/21/23 23:03 V35670MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/21/23 23:03 V35670MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/21/23 23:03 V35670MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/21/23 23:03 V35670MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/21/23 23:03 V35670MSA
<0.220 µg/L 0.220 0.500Chloroform 1 07/21/23 23:03 V35670MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/21/23 23:03 V35670MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/21/23 23:03 V35670MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/21/23 23:03 V35670MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 07/21/23 23:03 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 95 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-5
89747 Matrix:
7/14/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/21/23 23:03 V35670MSA
<0.200 µg/L 0.200 0.500
1,2-Dibromoethane 1 07/21/23 23:03 V35670MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/21/23 23:03 V35670MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/21/23 23:03 V35670MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/21/23 23:03 V35670MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/21/23 23:03 V35670MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/21/23 23:03 V35670MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/21/23 23:03 V35670MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 07/21/23 23:03 V35670MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/21/23 23:03 V35670MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/21/23 23:03 V35670MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/21/23 23:03 V35670MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/21/23 23:03 V35670MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/21/23 23:03 V35670MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/21/23 23:03 V35670MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/21/23 23:03 V35670MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/21/23 23:03 V35670MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/21/23 23:03 V35670MSA
<42.0 µg/L 42.0 200Ethanol 1 07/21/23 23:03 V35670MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/21/23 23:03 V35670MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 07/21/23 23:03 V35670MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 07/21/23 23:03 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 96 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-5
89747 Matrix:
7/14/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 07/21/23 23:03 V35670MSA
<0.380 µg/L 0.380 5.00
2-Hexanone 1 07/21/23 23:03 V35670MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 07/21/23 23:03 V35670MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/21/23 23:03 V35670MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/21/23 23:03 V35670MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 07/21/23 23:03 V35670MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 07/21/23 23:03 V35670MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 07/21/23 23:03 V35670MSA
<0.470 µg/L 0.470 1.00
Naphthalene 1 07/21/23 23:03 V35670MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/21/23 23:03 V35670MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/21/23 23:03 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/21/23 23:03 V35670MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/21/23 23:03 V35670MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/21/23 23:03 V35670MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/21/23 23:03 V35670MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 07/21/23 23:03 V35670MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 07/21/23 23:03 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/21/23 23:03 V35670MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/21/23 23:03 V35670MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/21/23 23:03 V35670MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/21/23 23:03 V35670MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 07/21/23 23:03 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 97 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-5
89747 Matrix:
7/14/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/21/23 23:03 V35670MSA
<1.00 µg/L 1.00 2.00
Vinyl Acetate 1 07/21/23 23:03 V35670MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/21/23 23:03 V35670MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/21/23 23:03 V35670MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/21/23 23:03 V35670MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/21/23 23:03 V35670
Surrogate: 4-Bromofluorobenzene 101 Limits: 80-124%07/21/23 23:031 MSA V35670
Surrogate: Dibromofluoromethane 99.4 Limits: 75-129%07/21/23 23:031 MSA V35670
Surrogate: 1,2-Dichloroethane - d4 96.8 Limits: 63-136%07/21/23 23:031 MSA V35670
Surrogate: Toluene-d8 94.6 Limits: 77-123%07/21/23 23:031 MSA V35670
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<0.302 µg/L 0.302 2.00Acenaphthene 1 07/21/23 15:57 V35550AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 07/21/23 15:57 V35550AMP
<2.05 µg/L 2.05 5.00Aniline 1 07/21/23 15:57 V35550AMP
<0.836 µg/L 0.836 2.00Anthracene 1 07/21/23 15:57 V35550AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 07/21/23 15:57 V35550AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 07/21/23 15:57 V35550AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 07/21/23 15:57 V35550AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 07/21/23 15:57 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 98 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-5
89747 Matrix:
7/14/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 07/21/23 15:57 V35550AMP
<1.10 µg/L 1.10 10.0
Benzoic Acid 1 07/21/23 15:57 V35550AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 07/21/23 15:57 V35550AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 07/21/23 15:57 V35550AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 07/21/23 15:57 V35550AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 07/21/23 15:57 V35550AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 07/21/23 15:57 V35550AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 07/21/23 15:57 V35550AMP
<1.83 µg/L 1.83 5.00
Butyl benzyl phthalate 1 07/21/23 15:57 V35550AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 07/21/23 15:57 V35550AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 07/21/23 15:57 V35550AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 07/21/23 15:57 V35550AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 07/21/23 15:57 V35550AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 07/21/23 15:57 V35550AMP
<0.405 µg/L 0.405 2.00Chrysene 1 07/21/23 15:57 V35550AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 07/21/23 15:57 V35550AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 07/21/23 15:57 V35550AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 07/21/23 15:57 V35550AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 07/21/23 15:57 V35550AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 07/21/23 15:57 V35550AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 07/21/23 15:57 V35550AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 07/21/23 15:57 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 99 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-5
89747 Matrix:
7/14/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 07/21/23 15:57 V35550AMP
<0.939 µg/L 0.939 5.00
Dimethyl phthalate 1 07/21/23 15:57 V35550AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 07/21/23 15:57 V35550AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 07/21/23 15:57 V35550AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 07/21/23 15:57 V35550AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 07/21/23 15:57 V35550AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 07/21/23 15:57 V35550AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 07/21/23 15:57 V35550AMP
<1.65 µg/L 1.65 5.00
Di-n-Octyl Phthalate 1 07/21/23 15:57 V35550AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 07/21/23 15:57 V35550AMP
<0.807 µg/L 0.807 2.00Fluorene 1 07/21/23 15:57 V35550AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 07/21/23 15:57 V35550AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 07/21/23 15:57 V35550AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 07/21/23 15:57 V35550AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 07/21/23 15:57 V35550AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 07/21/23 15:57 V35550AMP
<0.444 µg/L 0.444 5.00Isophorone 1 07/21/23 15:57 V35550AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 07/21/23 15:57 V35550AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 07/21/23 15:57 V35550AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 07/21/23 15:57 V35550AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 07/21/23 15:57 V35550AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 07/21/23 15:57 V35550AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 100 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:HH-TMW-5
89747 Matrix:
7/14/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V35516 07/19/23 10:17
<1.39 µg/L 1.39 5.002-Nitroaniline 1 07/21/23 15:57 V35550AMP
<1.39 µg/L 1.39 5.00
3-Nitroaniline 1 07/21/23 15:57 V35550AMP
<1.53 µg/L 1.53 5.004-Nitroaniline 1 07/21/23 15:57 V35550AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 07/21/23 15:57 V35550AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 07/21/23 15:57 V35550AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 07/21/23 15:57 V35550AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 07/21/23 15:57 V35550AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 07/21/23 15:57 V35550AMP
<0.641 µg/L 0.641 5.00
N-Nitroso-di-n-propylamine 1 07/21/23 15:57 V35550AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 07/21/23 15:57 V35550AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 07/21/23 15:57 V35550AMP
<0.651 µg/L 0.651 5.00Phenol 1 07/21/23 15:57 V35550AMP
<0.434 µg/L 0.434 2.00Pyrene 1 07/21/23 15:57 V35550AMP
<1.20 µg/L 1.20 5.00Pyridine 1 07/21/23 15:57 V35550AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 07/21/23 15:57 V35550AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 07/21/23 15:57 V35550AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 07/21/23 15:57 V35550AMP
8270ESurrogate: Phenol-d5 31.5 Limits: 11-100%07/21/23 15:571 AMP
Surrogate: 2-Fluorobiphenyl 96.2 Limits: 44-119%07/21/23 15:571 AMP V35550
Surrogate: 2-Fluorophenol 48.3 Limits: 19-119%07/21/23 15:571 AMP V35550
Surrogate: Nitrobenzene-d5 87.8 Limits: 44-120%07/21/23 15:571 AMP V35550
Surrogate: 4-Terphenyl-d14 119 Limits: 50-134%07/21/23 15:571 AMP V35550
Surrogate: 2,4,6-Tribromophenol 112 Limits: 43-140%07/21/23 15:571 AMP V35550
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 101 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89748 Matrix:
7/14/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.80 µg/L 1.80 5.00Acetone 1 07/21/23 16:52 V35670MSA
<2.00 µg/L 2.00 5.00
Acrolein 1 07/21/23 16:52 V35670MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 07/21/23 16:52 V35670MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/21/23 16:52 V35670MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/21/23 16:52 V35670MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/21/23 16:52 V35670MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/21/23 16:52 V35670MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/21/23 16:52 V35670MSA
<0.280 µg/L 0.280 1.00
Bromomethane 1 07/21/23 16:52 V35670MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 07/21/23 16:52 V35670MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/21/23 16:52 V35670MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/21/23 16:52 V35670MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 07/21/23 16:52 V35670MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/21/23 16:52 V35670MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/21/23 16:52 V35670MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/21/23 16:52 V35670MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/21/23 16:52 V35670MSA
<0.220 µg/L 0.220 0.500Chloroform 1 07/21/23 16:52 V35670MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/21/23 16:52 V35670MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/21/23 16:52 V35670MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/21/23 16:52 V35670MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 07/21/23 16:52 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 102 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89748 Matrix:
7/14/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/21/23 16:52 V35670MSA
<0.200 µg/L 0.200 0.500
1,2-Dibromoethane 1 07/21/23 16:52 V35670MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/21/23 16:52 V35670MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/21/23 16:52 V35670MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/21/23 16:52 V35670MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/21/23 16:52 V35670MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/21/23 16:52 V35670MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/21/23 16:52 V35670MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 07/21/23 16:52 V35670MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/21/23 16:52 V35670MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/21/23 16:52 V35670MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/21/23 16:52 V35670MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/21/23 16:52 V35670MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/21/23 16:52 V35670MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/21/23 16:52 V35670MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/21/23 16:52 V35670MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/21/23 16:52 V35670MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/21/23 16:52 V35670MSA
<42.0 µg/L 42.0 200Ethanol 1 07/21/23 16:52 V35670MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/21/23 16:52 V35670MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 07/21/23 16:52 V35670MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 07/21/23 16:52 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 103 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89748 Matrix:
7/14/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 07/21/23 16:52 V35670MSA
<0.380 µg/L 0.380 5.00
2-Hexanone 1 07/21/23 16:52 V35670MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 07/21/23 16:52 V35670MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/21/23 16:52 V35670MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/21/23 16:52 V35670MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 07/21/23 16:52 V35670MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 07/21/23 16:52 V35670MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 07/21/23 16:52 V35670MSA
<0.470 µg/L 0.470 1.00
Naphthalene 1 07/21/23 16:52 V35670MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/21/23 16:52 V35670MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/21/23 16:52 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/21/23 16:52 V35670MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/21/23 16:52 V35670MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/21/23 16:52 V35670MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/21/23 16:52 V35670MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 07/21/23 16:52 V35670MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 07/21/23 16:52 V35670MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/21/23 16:52 V35670MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/21/23 16:52 V35670MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/21/23 16:52 V35670MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/21/23 16:52 V35670MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 07/21/23 16:52 V35670MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 104 of 151
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 07/14/2023
TPI-002
Report Date : 08/02/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89748 Matrix:
7/14/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V35668 07/21/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/21/23 16:52 V35670MSA
<1.00 µg/L 1.00 2.00
Vinyl Acetate 1 07/21/23 16:52 V35670MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/21/23 16:52 V35670MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/21/23 16:52 V35670MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/21/23 16:52 V35670MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/21/23 16:52 V35670
Surrogate: 4-Bromofluorobenzene 101 Limits: 80-124%07/21/23 16:521 MSA V35670
Surrogate: Dibromofluoromethane 99.0 Limits: 75-129%07/21/23 16:521 MSA V35670
Surrogate: 1,2-Dichloroethane - d4 96.6 Limits: 63-136%07/21/23 16:521 MSA V35670
Surrogate: Toluene-d8 94.2 Limits: 77-123%07/21/23 16:521 MSA V35670
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 105 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Metals Analyses
6020B
L694385QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:L693917
Associated Lab Samples: 89743, 89744, 89745, 89746, 89747
LRB-L693917 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
07/21/23 21:491.000.297<0.297µg/LArsenic
07/21/23 21:491.000.453<0.453µg/LBarium
07/21/23 21:491.000.350<0.350µg/LCadmium
07/21/23 21:491.000.346<0.346µg/LChromium
07/21/23 21:491.000.264<0.264µg/LLead
07/21/23 21:491.000.703<0.703µg/LSelenium
07/21/23 21:491.000.0570<0.0570µg/LSilver
LCS-L693917Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10050.050.0µg/LArsenic 80-120
94.093.5100µg/LBarium 80-120
1009.9810.0µg/LCadmium 80-120
91.091.1100µg/LChromium 80-120
95.047.550.0µg/LLead 80-120
10099.6100µg/LSelenium 80-120
98.09.7510.0µg/LSilver 80-120
V 89577-MS-L693917 V 89577-MSD-L693917Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
50.6 10148.750.050.0< 0.297µg/LArsenic 97.0 75-125 3.8 20.0
131 98.012410010033.0µg/LBarium 91.0 75-125 5.4 20.0
10.1 1019.5110.010.0< 0.350µg/LCadmium 95.0 75-125 6.0 20.0
92.7 93.088.3100100< 0.346µg/LChromium 88.0 75-125 4.8 20.0
Page 1 of 43Date:08/02/2023 09:05 AM
Page 106 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Metals Analyses
6020B
L694385QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:L693917
V 89577-MS-L693917 V 89577-MSD-L693917Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
48.4 97.045.350.050.0< 0.264µg/LLead 91.0 75-125 6.6 20.0
101 10195.3100100< 0.703µg/LSelenium 95.0 75-125 5.8 20.0
9.77 98.09.1810.010.0< 0.0570µg/LSilver 92.0 75-125 6.2 20.0
V 89577-PDS-L693917Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
07/21/23 23:4399.024.6µg/LArsenic
07/21/23 23:4310166.9µg/LBarium
07/21/23 23:4398.04.88µg/LCadmium
07/21/23 23:4393.046.3µg/LChromium
07/21/23 23:4397.024.3µg/LLead
07/21/23 23:4397.048.7µg/LSelenium
07/21/23 23:4398.04.91µg/LSilver
Page 2 of 43Date:08/02/2023 09:05 AM
Page 107 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Metals Analyses
6020B
L694733QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L693937
Associated Lab Samples: 89735, 89736, 89737, 89738, 89739, 89740, 89741, 89742
LRB-L693937 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
07/21/23 16:270.2500.0855<0.0855mg/KgArsenic
07/21/23 16:270.2500.042<0.042mg/KgBarium
07/21/23 16:270.2500.0260<0.0260mg/KgCadmium
07/21/23 16:270.2500.116<0.116mg/KgChromium
07/21/23 16:270.2500.0310<0.0310mg/KgLead
07/21/23 16:270.2500.103<0.103mg/KgSelenium
07/21/23 16:270.2500.0067<0.0067mg/KgSilver
LCS-L693937Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.02.362.50mg/KgArsenic 80-120
89.04.475.00mg/KgBarium 80-120
92.00.4610.500mg/KgCadmium 80-120
95.04.735.00mg/KgChromium 80-120
94.02.342.50mg/KgLead 80-120
94.04.715.00mg/KgSelenium 80-120
95.00.4730.500mg/KgSilver 80-120
L 82670-MS-L693937 L 82670-MSD-L693937Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2.56 88.02.602.442.420.423mg/KgArsenic 89.0 75-125 1.5 80
88.5 0.0*83.54.874.84104mg/KgBarium 0.0*75-125 5.8 80
0.482 92.00.4760.4870.4840.0359mg/KgCadmium 90.0 75-125 1.2 80
6.02 90.05.984.874.841.66mg/KgChromium 89.0 75-125 0.6 80
Page 3 of 43* QC Fail Date:08/02/2023 09:05 AM
Page 108 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Metals Analyses
6020B
L694733QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L693937
L 82670-MS-L693937 L 82670-MSD-L693937Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2.93 82.02.912.442.420.934mg/KgLead 81.0 75-125 0.6 80
4.38 86.04.554.874.840.202mg/KgSelenium 89.0 75-125 3.8 80
0.529 93.00.5090.4870.4840.0763mg/KgSilver 89.0 75-125 3.8 80
L 82670-PDS-L693937Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
07/21/23 17:371001.22mg/KgArsenic
07/21/23 17:3781.010.3mg/KgBarium
07/21/23 17:371020.242mg/KgCadmium
07/21/23 17:371032.57mg/KgChromium
07/21/23 17:371021.28mg/KgLead
07/21/23 17:3798.02.32mg/KgSelenium
07/21/23 17:371040.252mg/KgSilver
Page 4 of 43Date:08/02/2023 09:05 AM
Page 109 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Total Aqueous Mercury Analysis - CVAA
7470A
L693993QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7470A
QC Prep:L693779
Associated Lab Samples: 89743, 89744, 89745, 89746, 89747
LRB-L693779 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
07/20/23 13:280.000200.00013<0.00013mg/LMercury (Total)
LCS-L693779Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.00.003740.00400mg/LMercury (Total)80-120
V 89747-MS-L693779 V 89747-MSD-L693779Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.00275 69.0*0.002780.004000.00400< 0.00013mg/LMercury (Total)70.0*80-120 1.0 20.0
V 89747-PDS-L693779Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
07/20/23 13:4689.00.00447mg/LMercury (Total)
Page 5 of 43* QC Fail Date:08/02/2023 09:05 AM
Page 110 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V35543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V35494
Associated Lab Samples: 89735, 89736, 89737, 89738, 89739, 89740, 89741, 89742
LRB-V35494 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
07/19/23 16:040.03000.0120<0.0120mg/KgMercury (Total)
LCS-V35494Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1020.4270.417mg/KgMercury (Total)80-120
V 89659-MS-V35494 V 89659-MSD-V35494Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.376 96.00.3860.4030.3910.0144mg/KgMercury (Total)96.0 80-120 2.6 20
V 89659-PDS-V35494Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
07/19/23 16:521010.203mg/KgMercury (Total)
Page 6 of 43Date:08/02/2023 09:05 AM
Page 111 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35423QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35422
Associated Lab Samples: 89735, 89737, 89738, 89739, 89740
LRB-V35422 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/17/23 11:500.0200.002<0.002mg/KgAcetone
07/17/23 11:500.0200.001<0.001mg/KgAcrolein
07/17/23 11:500.0200.0008<0.0008mg/KgAcrylonitrile
07/17/23 11:500.0050.0006<0.0006mg/KgBenzene
07/17/23 11:500.0050.0005<0.0005mg/KgBromobenzene
07/17/23 11:500.0050.0008<0.0008mg/KgBromochloromethane
07/17/23 11:500.0050.001<0.001mg/KgBromodichloromethane
07/17/23 11:500.0050.001<0.001mg/KgBromoform
07/17/23 11:500.0100.001<0.001mg/KgBromomethane
07/17/23 11:500.0050.0005<0.0005mg/Kgn-Butylbenzene
07/17/23 11:500.0050.0006<0.0006mg/Kgsec-Butyl benzene
07/17/23 11:500.0050.0005<0.0005mg/Kgtert-Butyl benzene
07/17/23 11:500.0050.0006<0.0006mg/KgCarbon Disulfide
07/17/23 11:500.0050.001<0.001mg/KgCarbon Tetrachloride
07/17/23 11:500.0050.0007<0.0007mg/KgChlorobenzene
07/17/23 11:500.0050.0009<0.0009mg/KgChlorodibromomethane
07/17/23 11:500.0100.0009<0.0009mg/KgChloroethane
07/17/23 11:500.0050.001<0.001mg/KgChloroform
07/17/23 11:500.0100.0006<0.0006mg/KgChloromethane
07/17/23 11:500.0050.0005<0.0005mg/Kg2-Chlorotoluene
07/17/23 11:500.0050.0004<0.0004mg/Kg4-Chlorotoluene
07/17/23 11:500.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
07/17/23 11:500.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
07/17/23 11:500.0050.0006<0.0006mg/Kg1,2-Dibromoethane
07/17/23 11:500.0050.0006<0.0006mg/KgDibromomethane
07/17/23 11:500.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
07/17/23 11:500.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 7 of 43Date:08/02/2023 09:05 AM
Page 112 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35423QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35422
Associated Lab Samples: 89735, 89737, 89738, 89739, 89740
LRB-V35422 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/17/23 11:500.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
07/17/23 11:500.0100.001<0.001mg/KgDichlorodifluoromethane
07/17/23 11:500.0050.0008<0.0008mg/Kg1,1-Dichloroethane
07/17/23 11:500.0050.001<0.001mg/Kg1,2-Dichloroethane
07/17/23 11:500.0050.0007<0.0007mg/Kg1,1-Dichloroethene
07/17/23 11:500.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
07/17/23 11:500.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
07/17/23 11:500.0050.0004<0.0004mg/Kg1,2-Dichloropropane
07/17/23 11:500.0050.0006<0.0006mg/Kg1,3-Dichloropropane
07/17/23 11:500.0050.001<0.001mg/Kg2,2-Dichloropropane
07/17/23 11:500.0050.0008<0.0008mg/Kg1,1-Dichloropropene
07/17/23 11:500.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
07/17/23 11:500.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
07/17/23 11:500.2500.014<0.014mg/KgEthanol
07/17/23 11:500.0050.0006<0.0006mg/KgEthylbenzene
07/17/23 11:500.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
07/17/23 11:500.0100.0008<0.0008mg/KgHexachlorobutadiene
07/17/23 11:500.0100.0007<0.0007mg/Kgn-Hexane
07/17/23 11:500.0200.0006<0.0006mg/Kg2-Hexanone
07/17/23 11:500.0050.0005<0.0005mg/KgIsopropylbenzene
07/17/23 11:500.0050.001<0.001mg/Kg4-Isopropyl toluene
07/17/23 11:500.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
07/17/23 11:500.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
07/17/23 11:500.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
07/17/23 11:500.0100.001<0.001mg/KgMethylene Chloride
07/17/23 11:500.0100.0010<0.0010mg/KgNaphthalene
07/17/23 11:500.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 8 of 43Date:08/02/2023 09:05 AM
Page 113 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35423QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35422
Associated Lab Samples: 89735, 89737, 89738, 89739, 89740
LRB-V35422 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/17/23 11:500.0050.001<0.001mg/KgStyrene
07/17/23 11:500.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
07/17/23 11:500.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
07/17/23 11:500.0050.0009<0.0009mg/KgTetrachloroethene
07/17/23 11:500.0050.0007<0.0007mg/KgToluene
07/17/23 11:500.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
07/17/23 11:500.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
07/17/23 11:500.0050.001<0.001mg/Kg1,1,1-Trichloroethane
07/17/23 11:500.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
07/17/23 11:500.0050.0009<0.0009mg/KgTrichloroethene
07/17/23 11:500.0100.002<0.002mg/KgTrichlorofluoromethane
07/17/23 11:500.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
07/17/23 11:500.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
07/17/23 11:500.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
07/17/23 11:500.0100.0005<0.0005mg/KgVinyl Acetate
07/17/23 11:500.0100.0005<0.0005mg/KgVinyl Chloride
07/17/23 11:500.0050.0005<0.0005mg/Kgo-Xylene
07/17/23 11:500.0100.001<0.001mg/Kgm,p-Xylene
07/17/23 11:504-Bromofluorobenzene (S)100 70-130
07/17/23 11:50Dibromofluoromethane (S)100 84-123
07/17/23 11:50Toluene-d8 (S)100 76-129
LCS-V35422 LCSD-V35422Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.091 91.395.20.0950.100mg/KgAcetone 29-198 4.1 20
Page 9 of 43Date:08/02/2023 09:05 AM
Page 114 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35423QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35422
LCS-V35422 LCSD-V35422Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.097 97.299.20.0990.100mg/KgAcrolein 70-130 2.0 20
0.104 1041060.1060.100mg/KgAcrylonitrile 65-134 1.9 20
0.044 88.894.60.0470.050mg/KgBenzene 74-127 6.3 20
0.043 86.698.20.0490.050mg/KgBromobenzene 73-125 12.5 20
0.045 91.493.80.0460.050mg/KgBromochloromethane 72-134 2.5 20
0.045 90.694.20.0470.050mg/KgBromodichloromethane 75-122 3.8 20
0.047 95.696.60.0480.050mg/KgBromoform 66-135 1.0 20
0.041 83.882.40.0410.050mg/KgBromomethane 20-180 1.6 20
0.043 86.291.60.0450.050mg/Kgn-Butylbenzene 65-135 6.0 20
0.042 84.090.00.0450.050mg/Kgsec-Butyl benzene 66-131 6.8 20
0.041 83.088.00.0440.050mg/Kgtert-Butyl benzene 67-132 5.8 20
0.042 85.890.40.0450.050mg/KgCarbon Disulfide 61-129 5.2 20
0.040 81.685.00.0420.050mg/KgCarbon Tetrachloride 64-143 4.0 20
0.045 90.491.60.0450.050mg/KgChlorobenzene 74-118 1.3 20
0.046 92.091.80.0450.050mg/KgChlorodibromomethane 73-122 0.2 20
0.047 94.685.00.0420.050mg/KgChloroethane 33-149 10.6 20
0.044 88.893.60.0460.050mg/KgChloroform 73-127 5.2 20
0.041 82.885.40.0420.050mg/KgChloromethane 45-143 3.0 20
0.042 85.893.80.0460.050mg/Kg2-Chlorotoluene 67-124 8.9 20
0.042 85.893.60.0460.050mg/Kg4-Chlorotoluene 71-126 8.6 20
0.045 90.291.00.0450.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.8 20
0.045 90.496.20.0480.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 6.2 20
0.046 93.496.40.0480.050mg/Kg1,2-Dibromoethane 70-132 3.1 20
0.046 92.295.40.0470.050mg/KgDibromomethane 74-133 3.4 20
0.044 89.092.00.0460.050mg/Kg1,2-Dichlorobenzene 72-123 3.3 20
0.043 87.291.60.0450.050mg/Kg1,3-Dichlorobenzene 71-120 4.9 20
Page 10 of 43Date:08/02/2023 09:05 AM
Page 115 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35423QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35422
LCS-V35422 LCSD-V35422Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.043 86.688.80.0440.050mg/Kg1,4-Dichlorobenzene 71-123 2.5 20
0.048 96.492.80.0460.050mg/KgDichlorodifluoromethane 26-146 3.8 20
0.044 88.693.80.0460.050mg/Kg1,1-Dichloroethane 74-127 5.7 20
0.043 87.894.60.0470.050mg/Kg1,2-Dichloroethane 68-128 7.4 20
0.042 84.890.40.0450.050mg/Kg1,1-Dichloroethene 67-149 6.3 20
0.044 88.896.20.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 8.0 20
0.043 86.895.80.0470.050mg/Kgtrans-1,2-Dichloroethene 73-132 9.8 20
0.044 89.898.20.0490.050mg/Kg1,2-Dichloropropane 73-130 8.9 20
0.046 92.096.40.0480.050mg/Kg1,3-Dichloropropane 75-124 4.6 20
0.041 82.490.20.0450.050mg/Kg2,2-Dichloropropane 50-142 9.0 20
0.042 84.091.40.0450.050mg/Kg1,1-Dichloropropene 71-130 8.4 20
0.045 91.698.00.0490.050mg/Kgcis-1,3-Dichloropropene 71-125 6.7 20
0.046 92.097.60.0480.050mg/Kgtrans-1,3-Dichloropropene 68-123 5.9 20
1.23 98.496.81.211.25mg/KgEthanol 70-130 1.6 20
0.043 87.890.00.0450.050mg/KgEthylbenzene 74-128 2.4 20
0.090 90.091.70.0910.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.8 20
0.042 84.486.40.0430.050mg/KgHexachlorobutadiene 64-125 2.3 20
0.043 87.293.60.0460.050mg/Kgn-Hexane 70-130 7.0 20
0.039 79.283.40.0410.050mg/Kg2-Hexanone 61-157 5.1 20
0.042 84.088.60.0440.050mg/KgIsopropylbenzene 68-126 5.3 20
0.043 86.289.80.0440.050mg/Kg4-Isopropyl toluene 68-129 4.0 20
0.043 86.681.40.0400.050mg/KgMethyl Ethyl Ketone (MEK)63-149 6.1 20
0.045 90.694.00.0470.050mg/KgMethyl tert-butyl ether (MTBE)70-130 3.6 20
0.048 96.099.80.0490.050mg/Kg4-Methyl-2-Pentanone 57-162 3.8 20
0.045 90.692.60.0460.050mg/KgMethylene Chloride 74-129 2.1 20
0.043 87.494.20.0470.050mg/KgNaphthalene 57-157 7.4 20
Page 11 of 43Date:08/02/2023 09:05 AM
Page 116 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35423QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35422
LCS-V35422 LCSD-V35422Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 84.290.80.0450.050mg/Kgn-Propylbenzene 67-130 7.5 20
0.046 92.095.60.0470.050mg/KgStyrene 77-121 3.8 20
0.045 90.891.40.0450.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.6 20
0.044 88.094.20.0470.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 6.8 20
0.042 85.888.00.0440.050mg/KgTetrachloroethene 68-130 2.5 20
0.043 86.091.60.0450.050mg/KgToluene 71-129 6.3 20
0.043 86.493.80.0460.050mg/Kg1,2,3-Trichlorobenzene 68-130 8.2 20
0.044 89.094.40.0470.050mg/Kg1,2,4-Trichlorobenzene 66-125 5.8 20
0.042 85.088.20.0440.050mg/Kg1,1,1-Trichloroethane 67-131 3.6 20
0.046 92.296.60.0480.050mg/Kg1,1,2-Trichloroethane 70-133 4.6 20
0.042 85.489.60.0440.050mg/KgTrichloroethene 75-133 4.8 20
0.041 82.480.40.0400.050mg/KgTrichlorofluoromethane 44-146 2.4 20
0.044 89.693.40.0460.050mg/Kg1,2,3-Trichloropropane 60-137 4.1 20
0.043 86.692.20.0460.050mg/Kg1,2,4-Trimethylbenzene 69-129 6.2 20
0.042 85.492.20.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 7.6 20
0.052 1061130.0560.050mg/KgVinyl Acetate 60-140 6.5 20
0.044 89.487.60.0430.050mg/KgVinyl Chloride 48-147 2.0 20
0.044 88.493.40.0460.050mg/Kgo-Xylene 74-126 5.5 20
0.087 87.192.80.0920.100mg/Kgm,p-Xylene 75-124 6.3 20
98.01004-Bromofluorobenzene (S)70-130
98.099.2Dibromofluoromethane (S)84-123
101101Toluene-d8 (S)76-129
Page 12 of 43Date:08/02/2023 09:05 AM
Page 117 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35490QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35489
Associated Lab Samples: 89736
LRB-V35489 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/18/23 13:000.0200.002<0.002mg/KgAcetone
07/18/23 13:000.0200.001<0.001mg/KgAcrolein
07/18/23 13:000.0200.0008<0.0008mg/KgAcrylonitrile
07/18/23 13:000.0050.0006<0.0006mg/KgBenzene
07/18/23 13:000.0050.0005<0.0005mg/KgBromobenzene
07/18/23 13:000.0050.0008<0.0008mg/KgBromochloromethane
07/18/23 13:000.0050.001<0.001mg/KgBromodichloromethane
07/18/23 13:000.0050.001<0.001mg/KgBromoform
07/18/23 13:000.0100.001<0.001mg/KgBromomethane
07/18/23 13:000.0050.0005<0.0005mg/Kgn-Butylbenzene
07/18/23 13:000.0050.0006<0.0006mg/Kgsec-Butyl benzene
07/18/23 13:000.0050.0005<0.0005mg/Kgtert-Butyl benzene
07/18/23 13:000.0050.0006<0.0006mg/KgCarbon Disulfide
07/18/23 13:000.0050.001<0.001mg/KgCarbon Tetrachloride
07/18/23 13:000.0050.0007<0.0007mg/KgChlorobenzene
07/18/23 13:000.0050.0009<0.0009mg/KgChlorodibromomethane
07/18/23 13:000.0100.0009<0.0009mg/KgChloroethane
07/18/23 13:000.0050.001<0.001mg/KgChloroform
07/18/23 13:000.0100.0006<0.0006mg/KgChloromethane
07/18/23 13:000.0050.0005<0.0005mg/Kg2-Chlorotoluene
07/18/23 13:000.0050.0004<0.0004mg/Kg4-Chlorotoluene
07/18/23 13:000.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
07/18/23 13:000.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
07/18/23 13:000.0050.0006<0.0006mg/Kg1,2-Dibromoethane
07/18/23 13:000.0050.0006<0.0006mg/KgDibromomethane
07/18/23 13:000.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
07/18/23 13:000.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 13 of 43Date:08/02/2023 09:05 AM
Page 118 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35490QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35489
Associated Lab Samples: 89736
LRB-V35489 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/18/23 13:000.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
07/18/23 13:000.0100.001<0.001mg/KgDichlorodifluoromethane
07/18/23 13:000.0050.0008<0.0008mg/Kg1,1-Dichloroethane
07/18/23 13:000.0050.001<0.001mg/Kg1,2-Dichloroethane
07/18/23 13:000.0050.0007<0.0007mg/Kg1,1-Dichloroethene
07/18/23 13:000.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
07/18/23 13:000.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
07/18/23 13:000.0050.0004<0.0004mg/Kg1,2-Dichloropropane
07/18/23 13:000.0050.0006<0.0006mg/Kg1,3-Dichloropropane
07/18/23 13:000.0050.001<0.001mg/Kg2,2-Dichloropropane
07/18/23 13:000.0050.0008<0.0008mg/Kg1,1-Dichloropropene
07/18/23 13:000.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
07/18/23 13:000.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
07/18/23 13:000.2500.014<0.014mg/KgEthanol
07/18/23 13:000.0050.0006<0.0006mg/KgEthylbenzene
07/18/23 13:000.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
07/18/23 13:000.0100.0008<0.0008mg/KgHexachlorobutadiene
07/18/23 13:000.0100.0007<0.0007mg/Kgn-Hexane
07/18/23 13:000.0200.0006<0.0006mg/Kg2-Hexanone
07/18/23 13:000.0050.0005<0.0005mg/KgIsopropylbenzene
07/18/23 13:000.0050.001<0.001mg/Kg4-Isopropyl toluene
07/18/23 13:000.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
07/18/23 13:000.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
07/18/23 13:000.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
07/18/23 13:000.0100.001<0.001mg/KgMethylene Chloride
07/18/23 13:000.0100.0010<0.0010mg/KgNaphthalene
07/18/23 13:000.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 14 of 43Date:08/02/2023 09:05 AM
Page 119 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35490QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35489
Associated Lab Samples: 89736
LRB-V35489 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/18/23 13:000.0050.001<0.001mg/KgStyrene
07/18/23 13:000.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
07/18/23 13:000.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
07/18/23 13:000.0050.0009<0.0009mg/KgTetrachloroethene
07/18/23 13:000.0050.0007<0.0007mg/KgToluene
07/18/23 13:000.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
07/18/23 13:000.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
07/18/23 13:000.0050.001<0.001mg/Kg1,1,1-Trichloroethane
07/18/23 13:000.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
07/18/23 13:000.0050.0009<0.0009mg/KgTrichloroethene
07/18/23 13:000.0100.002<0.002mg/KgTrichlorofluoromethane
07/18/23 13:000.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
07/18/23 13:000.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
07/18/23 13:000.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
07/18/23 13:000.0100.0005<0.0005mg/KgVinyl Acetate
07/18/23 13:000.0100.0005<0.0005mg/KgVinyl Chloride
07/18/23 13:000.0050.0005<0.0005mg/Kgo-Xylene
07/18/23 13:000.0100.001<0.001mg/Kgm,p-Xylene
07/18/23 13:004-Bromofluorobenzene (S)99.0 70-130
07/18/23 13:00Dibromofluoromethane (S)98.4 84-123
07/18/23 13:00Toluene-d8 (S)98.4 76-129
LCS-V35489 LCSD-V35489Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.099 99.71030.1030.100mg/KgAcetone 29-198 3.2 20
Page 15 of 43Date:08/02/2023 09:05 AM
Page 120 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35490QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35489
LCS-V35489 LCSD-V35489Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.098 98.41060.1060.100mg/KgAcrolein 70-130 7.4 20
0.097 97.71030.1030.100mg/KgAcrylonitrile 65-134 5.2 20
0.047 94.898.00.0490.050mg/KgBenzene 74-127 3.3 20
0.046 92.492.40.0460.050mg/KgBromobenzene 73-125 0.0 20
0.048 96.81000.0500.050mg/KgBromochloromethane 72-134 3.4 20
0.048 96.298.00.0490.050mg/KgBromodichloromethane 75-122 1.8 20
0.048 97.61010.0500.050mg/KgBromoform 66-135 3.6 20
0.051 1031100.0540.050mg/KgBromomethane 20-180 6.7 20
0.045 91.895.00.0470.050mg/Kgn-Butylbenzene 65-135 3.4 20
0.044 89.493.20.0460.050mg/Kgsec-Butyl benzene 66-131 4.1 20
0.043 87.890.60.0450.050mg/Kgtert-Butyl benzene 67-132 3.1 20
0.045 90.696.20.0480.050mg/KgCarbon Disulfide 61-129 5.9 20
0.043 87.493.00.0460.050mg/KgCarbon Tetrachloride 64-143 6.2 20
0.047 94.095.80.0470.050mg/KgChlorobenzene 74-118 1.8 20
0.047 95.897.60.0480.050mg/KgChlorodibromomethane 73-122 1.8 20
0.051 1031100.0550.050mg/KgChloroethane 33-149 6.7 20
0.047 94.896.60.0480.050mg/KgChloroform 73-127 1.8 20
0.039 79.088.00.0440.050mg/KgChloromethane 45-143 10.7 20
0.045 90.291.40.0450.050mg/Kg2-Chlorotoluene 67-124 1.3 20
0.045 90.291.40.0450.050mg/Kg4-Chlorotoluene 71-126 1.3 20
0.046 93.495.40.0470.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.1 20
0.046 93.295.00.0470.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.9 20
0.048 96.695.60.0470.050mg/Kg1,2-Dibromoethane 70-132 1.0 20
0.049 98.099.60.0490.050mg/KgDibromomethane 74-133 1.6 20
0.047 94.293.80.0460.050mg/Kg1,2-Dichlorobenzene 72-123 0.4 20
0.046 92.692.40.0460.050mg/Kg1,3-Dichlorobenzene 71-120 0.2 20
Page 16 of 43Date:08/02/2023 09:05 AM
Page 121 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35490QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35489
LCS-V35489 LCSD-V35489Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.046 92.091.00.0450.050mg/Kg1,4-Dichlorobenzene 71-123 1.0 20
0.035 71.478.00.0390.050mg/KgDichlorodifluoromethane 26-146 8.8 20
0.045 91.697.60.0480.050mg/Kg1,1-Dichloroethane 74-127 6.3 20
0.046 92.693.40.0460.050mg/Kg1,2-Dichloroethane 68-128 0.8 20
0.045 90.496.40.0480.050mg/Kg1,1-Dichloroethene 67-149 6.4 20
0.046 93.495.40.0470.050mg/Kgcis-1,2-Dichloroethene 76-134 2.1 20
0.046 92.498.00.0490.050mg/Kgtrans-1,2-Dichloroethene 73-132 5.8 20
0.048 96.61010.0500.050mg/Kg1,2-Dichloropropane 73-130 4.0 20
0.047 95.895.80.0470.050mg/Kg1,3-Dichloropropane 75-124 0.0 20
0.044 88.091.60.0450.050mg/Kg2,2-Dichloropropane 50-142 4.0 20
0.045 91.695.60.0470.050mg/Kg1,1-Dichloropropene 71-130 4.2 20
0.048 96.099.20.0490.050mg/Kgcis-1,3-Dichloropropene 71-125 3.2 20
0.047 95.698.60.0490.050mg/Kgtrans-1,3-Dichloropropene 68-123 3.0 20
1.21 96.899.21.241.25mg/KgEthanol 70-130 2.4 20
0.045 91.694.00.0470.050mg/KgEthylbenzene 74-128 2.5 20
0.094 94.495.10.0950.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.7 20
0.044 89.094.60.0470.050mg/KgHexachlorobutadiene 64-125 6.1 20
0.046 92.01050.0520.050mg/Kgn-Hexane 70-130 12.8 20
0.042 85.082.80.0410.050mg/Kg2-Hexanone 61-157 2.6 20
0.044 89.091.20.0450.050mg/KgIsopropylbenzene 68-126 2.4 20
0.045 91.494.00.0470.050mg/Kg4-Isopropyl toluene 68-129 2.8 20
0.045 91.698.00.0490.050mg/KgMethyl Ethyl Ketone (MEK)63-149 6.7 20
0.046 93.694.60.0470.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.0 20
0.047 95.296.60.0480.050mg/Kg4-Methyl-2-Pentanone 57-162 1.4 20
0.047 94.697.00.0480.050mg/KgMethylene Chloride 74-129 2.5 20
0.045 90.693.20.0460.050mg/KgNaphthalene 57-157 2.8 20
Page 17 of 43Date:08/02/2023 09:05 AM
Page 122 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35490QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V35489
LCS-V35489 LCSD-V35489Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 90.892.80.0460.050mg/Kgn-Propylbenzene 67-130 2.1 20
0.048 97.098.00.0490.050mg/KgStyrene 77-121 1.0 20
0.047 94.694.20.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.4 20
0.045 91.692.80.0460.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.3 20
0.045 91.897.00.0480.050mg/KgTetrachloroethene 68-130 5.5 20
0.046 92.097.00.0480.050mg/KgToluene 71-129 5.2 20
0.045 91.493.20.0460.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.9 20
0.047 94.697.60.0480.050mg/Kg1,2,4-Trichlorobenzene 66-125 3.1 20
0.044 89.894.60.0470.050mg/Kg1,1,1-Trichloroethane 67-131 5.2 20
0.047 95.295.40.0470.050mg/Kg1,1,2-Trichloroethane 70-133 0.2 20
0.046 93.296.20.0480.050mg/KgTrichloroethene 75-133 3.1 20
0.045 90.897.40.0480.050mg/KgTrichlorofluoromethane 44-146 7.0 20
0.045 90.491.60.0450.050mg/Kg1,2,3-Trichloropropane 60-137 1.3 20
0.045 90.092.80.0460.050mg/Kg1,2,4-Trimethylbenzene 69-129 3.0 20
0.044 89.892.40.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 2.8 20
0.055 1111170.0580.050mg/KgVinyl Acetate 60-140 5.4 20
0.044 88.695.80.0470.050mg/KgVinyl Chloride 48-147 7.8 20
0.046 92.295.40.0470.050mg/Kgo-Xylene 74-126 3.4 20
0.091 91.994.70.0940.100mg/Kgm,p-Xylene 75-124 3.0 20
99.097.04-Bromofluorobenzene (S)70-130
98.8100Dibromofluoromethane (S)84-123
99.498.2Toluene-d8 (S)76-129
Page 18 of 43Date:08/02/2023 09:05 AM
Page 123 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35670QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V35668
Associated Lab Samples: 89743, 89744, 89745, 89746, 89747, 89748
LRB-V35668 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/21/23 16:275.001.80<1.80µg/LAcetone
07/21/23 16:275.002.00<2.00µg/LAcrolein
07/21/23 16:275.000.230<0.230µg/LAcrylonitrile
07/21/23 16:270.5000.180<0.180µg/LBenzene
07/21/23 16:270.5000.210<0.210µg/LBromobenzene
07/21/23 16:271.000.420<0.420µg/LBromochloromethane
07/21/23 16:270.5000.160<0.160µg/LBromodichloromethane
07/21/23 16:275.001.50<1.50µg/LBromoform
07/21/23 16:271.000.280<0.280µg/LBromomethane
07/21/23 16:271.000.185<0.185µg/Ln-Butylbenzene
07/21/23 16:270.5000.200<0.200µg/Lsec-Butyl benzene
07/21/23 16:272.000.920<0.920µg/Ltert-Butyl benzene
07/21/23 16:275.000.150<0.150µg/LCarbon Disulfide
07/21/23 16:270.5000.180<0.180µg/LCarbon Tetrachloride
07/21/23 16:270.5000.190<0.190µg/LChlorobenzene
07/21/23 16:270.5000.190<0.190µg/LChlorodibromomethane
07/21/23 16:271.000.430<0.430µg/LChloroethane
07/21/23 16:270.5000.220<0.220µg/LChloroform
07/21/23 16:270.5000.220<0.220µg/LChloromethane
07/21/23 16:270.5000.200<0.200µg/L2-Chlorotoluene
07/21/23 16:270.5000.200<0.200µg/L4-Chlorotoluene
07/21/23 16:275.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
07/21/23 16:272.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/21/23 16:270.5000.200<0.200µg/L1,2-Dibromoethane
07/21/23 16:270.5000.230<0.230µg/LDibromomethane
07/21/23 16:270.5000.220<0.220µg/L1,2-Dichlorobenzene
07/21/23 16:270.5000.190<0.190µg/L1,3-Dichlorobenzene
Page 19 of 43Date:08/02/2023 09:05 AM
Page 124 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35670QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V35668
Associated Lab Samples: 89743, 89744, 89745, 89746, 89747, 89748
LRB-V35668 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/21/23 16:270.5000.210<0.210µg/L1,4-Dichlorobenzene
07/21/23 16:275.001.20<1.20µg/LDichlorodifluoromethane
07/21/23 16:270.5000.240<0.240µg/L1,1-Dichloroethane
07/21/23 16:270.5000.150<0.150µg/L1,2-Dichloroethane
07/21/23 16:270.5000.150<0.150µg/L1,1-Dichloroethene
07/21/23 16:270.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/21/23 16:270.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/21/23 16:270.5000.190<0.190µg/L1,2-Dichloropropane
07/21/23 16:270.5000.130<0.130µg/L1,3-Dichloropropane
07/21/23 16:272.000.210<0.210µg/L2,2-Dichloropropane
07/21/23 16:270.5000.200<0.200µg/L1,1-Dichloropropene
07/21/23 16:270.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/21/23 16:270.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/21/23 16:2720042.0<42.0µg/LEthanol
07/21/23 16:270.5000.170<0.170µg/LEthylbenzene
07/21/23 16:2710.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
07/21/23 16:272.000.350<0.350µg/LHexachlorobutadiene
07/21/23 16:2710.01.30<1.30µg/Ln-Hexane
07/21/23 16:275.000.380<0.380µg/L2-Hexanone
07/21/23 16:275.000.180<0.180µg/LIsopropylbenzene
07/21/23 16:270.5000.089<0.089µg/L4-Isopropyl toluene
07/21/23 16:275.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/21/23 16:270.5000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/21/23 16:275.001.00<1.00µg/L4-Methyl-2-Pentanone
07/21/23 16:271.000.330<0.330µg/LMethylene Chloride
07/21/23 16:271.000.470<0.470µg/LNaphthalene
07/21/23 16:270.5000.190<0.190µg/Ln-Propylbenzene
Page 20 of 43Date:08/02/2023 09:05 AM
Page 125 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35670QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V35668
Associated Lab Samples: 89743, 89744, 89745, 89746, 89747, 89748
LRB-V35668 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/21/23 16:270.5000.220<0.220µg/LStyrene
07/21/23 16:270.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
07/21/23 16:270.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/21/23 16:270.5000.220<0.220µg/LTetrachloroethene
07/21/23 16:270.5000.220<0.220µg/LToluene
07/21/23 16:272.000.380<0.380µg/L1,2,3-Trichlorobenzene
07/21/23 16:271.000.310<0.310µg/L1,2,4-Trichlorobenzene
07/21/23 16:270.5000.160<0.160µg/L1,1,1-Trichloroethane
07/21/23 16:270.5000.096<0.096µg/L1,1,2-Trichloroethane
07/21/23 16:270.5000.180<0.180µg/LTrichloroethene
07/21/23 16:270.5000.180<0.180µg/LTrichlorofluoromethane
07/21/23 16:271.000.270<0.270µg/L1,2,3-Trichloropropane
07/21/23 16:270.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/21/23 16:272.001.00<1.00µg/LVinyl Acetate
07/21/23 16:270.5000.170<0.170µg/LVinyl Chloride
07/21/23 16:270.5000.210<0.210µg/Lo-Xylene
07/21/23 16:271.000.420<0.420µg/Lm,p-Xylene
07/21/23 16:274-Bromofluorobenzene (S)99.8 80-124
07/21/23 16:27Dibromofluoromethane (S)97.6 75-129
07/21/23 16:271,2-Dichloroethane - d4 (S)96.8 63-136
07/21/23 16:27Toluene-d8 (S)94.8 77-123
LCS-V35668 LCSD-V35668Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
28.1 70.267.727.140.0µg/LAcetone 40-166 3.6 20
Page 21 of 43Date:08/02/2023 09:05 AM
Page 126 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35670QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V35668
LCS-V35668 LCSD-V35668Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
47.3 11811445.640.0µg/LAcrolein 70-130 3.6 20
48.3 12111545.840.0µg/LAcrylonitrile 81-127 5.3 20
22.5 11310921.820.0µg/LBenzene 77-128 3.1 20
19.6 98.098.519.720.0µg/LBromobenzene 78-129 0.5 20
22.2 11110821.620.0µg/LBromochloromethane 78-135 2.7 20
22.2 11110921.720.0µg/LBromodichloromethane 76-138 2.2 20
20.9 10510120.220.0µg/LBromoform 71-135 3.4 20
19.8 99.088.517.720.0µg/LBromomethane 41-168 11.2 20
19.6 98.097.019.420.0µg/Ln-Butylbenzene 68-134 1.0 20
19.3 96.595.519.120.0µg/Lsec-Butyl benzene 71-131 1.0 20
19.2 96.096.019.220.0µg/Ltert-Butyl benzene 70-132 0.0 20
20.0 10099.519.920.0µg/LCarbon Disulfide 59-135 0.5 20
23.2 11611021.920.0µg/LCarbon Tetrachloride 72-142 5.7 20
20.8 10410220.320.0µg/LChlorobenzene 78-119 2.4 20
20.6 10310220.420.0µg/LChlorodibromomethane 75-134 0.9 20
23.5 11811422.720.0µg/LChloroethane 57-142 3.4 20
22.0 11010921.820.0µg/LChloroform 77-130 0.9 20
22.6 11310420.820.0µg/LChloromethane 47-145 8.2 20
18.9 94.595.019.020.0µg/L2-Chlorotoluene 74-126 0.5 20
19.5 97.599.519.920.0µg/L4-Chlorotoluene 78-129 2.0 20
22.5 11311022.020.0µg/LDi-Isopropyl Ether (DIPE)60-154 2.2 20
21.0 10510420.720.0µg/L1,2-Dibromo-3-Chloropropane 63-134 1.4 20
20.7 10410220.320.0µg/L1,2-Dibromoethane 77-135 1.9 20
22.5 11311122.120.0µg/LDibromomethane 76-138 1.7 20
19.8 99.097.519.520.0µg/L1,2-Dichlorobenzene 78-128 1.5 20
19.5 97.595.519.120.0µg/L1,3-Dichlorobenzene 77-125 2.0 20
Page 22 of 43Date:08/02/2023 09:05 AM
Page 127 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35670QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V35668
LCS-V35668 LCSD-V35668Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.5 97.596.519.320.0µg/L1,4-Dichlorobenzene 75-126 1.0 20
19.6 98.093.018.620.0µg/LDichlorodifluoromethane 28-163 5.2 20
22.9 11511222.320.0µg/L1,1-Dichloroethane 70-130 2.6 20
23.3 11711222.420.0µg/L1,2-Dichloroethane 68-131 3.9 20
22.3 11210921.720.0µg/L1,1-Dichloroethene 70-154 2.7 20
22.5 11311122.120.0µg/Lcis-1,2-Dichloroethene 76-141 1.7 20
22.6 11311222.320.0µg/Ltrans-1,2-Dichloroethene 76-135 1.3 20
22.7 11411122.220.0µg/L1,2-Dichloropropane 77-130 2.2 20
20.5 10310120.220.0µg/L1,3-Dichloropropane 76-132 1.4 20
22.0 11010921.820.0µg/L2,2-Dichloropropane 29-149 0.9 20
23.5 11811422.820.0µg/L1,1-Dichloropropene 71-136 3.0 20
22.6 11311021.920.0µg/Lcis-1,3-Dichloropropene 65-140 3.1 20
23.1 11611122.120.0µg/Ltrans-1,3-Dichloropropene 67-140 4.4 20
536 107126630500µg/LEthanol 70-130 16.1 20
20.2 10199.019.820.0µg/LEthylbenzene 80-127 2.0 20
47.4 11911546.040.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 2.9 20
19.5 97.598.019.620.0µg/LHexachlorobutadiene 61-134 0.5 20
22.6 11311021.920.0µg/Ln-Hexane 70-130 3.1 20
19.5 97.595.019.020.0µg/L2-Hexanone 64-137 2.5 20
19.8 99.099.519.920.0µg/LIsopropylbenzene 70-130 0.5 20
20.0 10099.519.920.0µg/L4-Isopropyl toluene 69-132 0.5 20
18.8 94.089.517.920.0µg/LMethyl Ethyl Ketone (MEK)71-134 4.9 20
22.3 11210821.520.0µg/LMethyl tert-butyl ether (MTBE)68-135 3.6 20
24.1 12111623.220.0µg/L4-Methyl-2-Pentanone 69-134 3.8 20
23.5 11811422.820.0µg/LMethylene Chloride 73-131 3.0 20
21.1 10610621.120.0µg/LNaphthalene 64-136 0.0 20
Page 23 of 43Date:08/02/2023 09:05 AM
Page 128 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V35670QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V35668
LCS-V35668 LCSD-V35668Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.5 97.597.519.520.0µg/Ln-Propylbenzene 72-132 0.0 20
21.0 10510621.220.0µg/LStyrene 78-129 0.9 20
21.0 10510520.920.0µg/L1,1,1,2-Tetrachloroethane 79-134 0.4 20
20.2 10110020.020.0µg/L1,1,2,2-Tetrachloroethane 62-127 0.9 20
20.7 10410220.420.0µg/LTetrachloroethene 80-129 1.4 20
22.0 11010921.820.0µg/LToluene 76-131 0.9 20
25.4 12712224.420.0µg/L1,2,3-Trichlorobenzene 58-144 4.0 20
21.9 11010821.520.0µg/L1,2,4-Trichlorobenzene 66-139 1.8 20
22.3 11210921.820.0µg/L1,1,1-Trichloroethane 75-135 2.2 20
23.1 11611422.820.0µg/L1,1,2-Trichloroethane 70-140 1.3 20
22.4 11211122.120.0µg/LTrichloroethene 77-133 1.3 20
22.8 11411322.620.0µg/LTrichlorofluoromethane 62-148 0.8 20
19.3 96.594.518.920.0µg/L1,2,3-Trichloropropane 71-127 2.0 20
20.0 10010120.120.0µg/L1,3,5-Trimethylbenzene 75-131 0.4 20
23.3 11711222.320.0µg/LVinyl Acetate 34-167 4.3 20
22.4 11210921.720.0µg/LVinyl Chloride 57-141 3.1 20
20.4 10210120.120.0µg/Lo-Xylene 78-128 1.4 20
43.7 10910742.640.0µg/Lm,p-Xylene 77-133 2.5 20
97.499.44-Bromofluorobenzene (S)80-124
97.898.2Dibromofluoromethane (S)75-129
10299.61,2-Dichloroethane - d4 (S)63-136
94.294.6Toluene-d8 (S)77-123
Page 24 of 43Date:08/02/2023 09:05 AM
Page 129 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35527QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V35515
Associated Lab Samples: 89735, 89736, 89737, 89738, 89739, 89740
LRB-V35515 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/19/23 17:24660116<116µg/KgAcenaphthene
07/19/23 17:24660105<105µg/KgAcenaphthylene
07/19/23 17:24660152<152µg/KgAniline
07/19/23 17:24660143<143µg/KgAnthracene
07/19/23 17:24660139<139µg/KgBenzo(a)anthracene
07/19/23 17:24660147<147µg/KgBenzo(a)pyrene
07/19/23 17:24660146<146µg/KgBenzo(b)fluoranthene
07/19/23 17:24660136<136µg/KgBenzo(g,h,i)perylene
07/19/23 17:24660137<137µg/KgBenzo(k)fluoranthene
07/19/23 17:242000580<580µg/KgBenzoic Acid
07/19/23 17:24660105<105µg/KgBenzyl alcohol
07/19/23 17:24660118<118µg/KgBis(2-Chloroethoxy)methane
07/19/23 17:24660107<107µg/KgBis(2-Chloroethyl)ether
07/19/23 17:24330136<136µg/KgBis(2-Chloroisopropyl)ether
07/19/23 17:24660120<120µg/KgBis(2-ethylhexyl)phthalate
07/19/23 17:24660109<109µg/Kg4-Bromophenyl phenyl ether
07/19/23 17:24330113<113µg/KgButyl benzyl phthalate
07/19/23 17:2466092.4<92.4µg/Kg4-Chloro-3-methylphenol
07/19/23 17:24330112<112µg/Kg4-Chloroaniline
07/19/23 17:24660116<116µg/Kg2-Chloronaphthalene
07/19/23 17:2466098.2<98.2µg/Kg2-Chlorophenol
07/19/23 17:241000126<126µg/Kg4-Chlorophenyl phenyl ether
07/19/23 17:24660142<142µg/KgChrysene
07/19/23 17:24660230<230µg/KgDibenz(a,h)anthracene
07/19/23 17:24660119<119µg/KgDibenzofuran
07/19/23 17:2466094.4<94.4µg/Kg1,2-Dichlorobenzene
07/19/23 17:2466097.3<97.3µg/Kg1,3-Dichlorobenzene
Page 25 of 43Date:08/02/2023 09:05 AM
Page 130 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35527QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V35515
Associated Lab Samples: 89735, 89736, 89737, 89738, 89739, 89740
LRB-V35515 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/19/23 17:2433097.5<97.5µg/Kg1,4-Dichlorobenzene
07/19/23 17:24660147<147µg/Kg3,3'-Dichlorobenzidine
07/19/23 17:2466095.8<95.8µg/Kg2,4-Dichlorophenol
07/19/23 17:24660180<180µg/KgDiethyl phthalate
07/19/23 17:24660174<174µg/KgDimethyl phthalate
07/19/23 17:24330108<108µg/Kg2,4-Dimethylphenol
07/19/23 17:24660107<107µg/KgDi-n-butyl phthalate
07/19/23 17:241500240<240µg/Kg4,6-Dinitro-2-methylphenol
07/19/23 17:241500520<520µg/Kg2,4-Dinitrophenol
07/19/23 17:2466096.6<96.6µg/Kg2,4-Dinitrotoluene
07/19/23 17:24660108<108µg/Kg2,6-Dinitrotoluene
07/19/23 17:24330143<143µg/KgDi-n-Octyl Phthalate
07/19/23 17:24660123<123µg/KgFluoranthene
07/19/23 17:24660128<128µg/KgFluorene
07/19/23 17:24660106<106µg/KgHexachlorobenzene
07/19/23 17:2466097.6<97.6µg/KgHexachlorobutadiene
07/19/23 17:24660157<157µg/KgHexachlorocyclopentadiene
07/19/23 17:2466079.2<79.2µg/KgHexachloroethane
07/19/23 17:24660179<179µg/KgIndeno(1,2,3-cd)pyrene
07/19/23 17:24660191<191µg/KgIsophorone
07/19/23 17:24660106<106µg/Kg1-Methylnaphthalene
07/19/23 17:24660100<100µg/Kg2-Methylnaphthalene
07/19/23 17:2466097.0<97.0µg/Kg2-Methylphenol
07/19/23 17:2466084.9<84.9µg/Kg3&4 Methylphenol
07/19/23 17:24660144<144µg/KgNaphthalene
07/19/23 17:2466096.7<96.7µg/Kg2-Nitroaniline
07/19/23 17:24660120<120µg/Kg3-Nitroaniline
Page 26 of 43Date:08/02/2023 09:05 AM
Page 131 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35527QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V35515
Associated Lab Samples: 89735, 89736, 89737, 89738, 89739, 89740
LRB-V35515 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/19/23 17:2433093.3<93.3µg/Kg4-Nitroaniline
07/19/23 17:24330116<116µg/KgNitrobenzene
07/19/23 17:2466088.8<88.8µg/Kg2-Nitrophenol
07/19/23 17:24660117<117µg/Kg4-Nitrophenol
07/19/23 17:24660263<263µg/KgN-Nitrosodimethylamine
07/19/23 17:24660181<181µg/KgN-Nitrosodiphenylamine
07/19/23 17:24660118<118µg/KgN-Nitroso-di-n-propylamine
07/19/23 17:241000347<347µg/KgPentachlorophenol
07/19/23 17:24660208<208µg/KgPhenanthrene
07/19/23 17:24660112<112µg/KgPhenol
07/19/23 17:24660134<134µg/KgPyrene
07/19/23 17:2433079.2<79.2µg/KgPyridine
07/19/23 17:24660107<107µg/Kg1,2,4-Trichlorobenzene
07/19/23 17:2466096.2<96.2µg/Kg2,4,5-Trichlorophenol
07/19/23 17:2466096.6<96.6µg/Kg2,4,6-Trichlorophenol
07/19/23 17:242-Fluorobiphenyl (S)86.2 44-115
07/19/23 17:242-Fluorophenol (S)69.9 35-115
07/19/23 17:24Nitrobenzene-d5 (S)81.4 37-122
07/19/23 17:244-Terphenyl-d14 (S)101 54-127
07/19/23 17:242,4,6-Tribromophenol (S)74.7 39-132
07/19/23 17:24Phenol-d5 (S)60.0 34-121
LCS-V35515Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
85.014201670µg/KgAcenaphthene 40-123
84.414101670µg/KgAcenaphthylene 32-132
Page 27 of 43Date:08/02/2023 09:05 AM
Page 132 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35527QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V35515
LCS-V35515Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
204*34001670µg/KgAniline 12-197
89.815001670µg/KgAnthracene 47-123
90.415101670µg/KgBenzo(a)anthracene 49-126
98.816501670µg/KgBenzo(a)pyrene 45-129
88.614801670µg/KgBenzo(b)fluoranthene 45-132
89.815001670µg/KgBenzo(g,h,i)perylene 43-134
95.215901670µg/KgBenzo(k)fluoranthene 47-132
49.48251670µg/KgBenzoic Acid 10-83
90.415101670µg/KgBenzyl alcohol 29-122
84.414101670µg/KgBis(2-Chloroethoxy)methane 36-121
65.811001670µg/KgBis(2-Chloroethyl)ether 31-120
67.011201670µg/KgBis(2-Chloroisopropyl)ether 33-131
88.014701670µg/KgBis(2-ethylhexyl)phthalate 51-133
99.416601670µg/Kg4-Bromophenyl phenyl ether 46-124
83.213901670µg/KgButyl benzyl phthalate 48-132
87.414601670µg/Kg4-Chloro-3-methylphenol 45-122
10417301670µg/Kg4-Chloroaniline 17-106
87.414601670µg/Kg2-Chloronaphthalene 41-114
79.013201670µg/Kg2-Chlorophenol 34-121
93.415601670µg/Kg4-Chlorophenyl phenyl ether 45-121
88.014701670µg/KgChrysene 50-124
83.213901670µg/KgDibenz(a,h)anthracene 45-134
87.414601670µg/KgDibenzofuran 44-120
73.612301670µg/Kg1,2-Dichlorobenzene 33-117
70.011701670µg/Kg1,3-Dichlorobenzene 30-115
68.811501670µg/Kg1,4-Dichlorobenzene 31-115
86.214401670µg/Kg3,3'-Dichlorobenzidine 22-121
Page 28 of 43* QC Fail Date:08/02/2023 09:05 AM
Page 133 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35527QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V35515
LCS-V35515Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
93.415601670µg/Kg2,4-Dichlorophenol 40-122
89.815001670µg/KgDiethyl phthalate 50-124
90.415101670µg/KgDimethyl phthalate 48-124
11318901670µg/Kg2,4-Dimethylphenol 30-127
92.815501670µg/KgDi-n-butyl phthalate 51-128
97.016201670µg/Kg4,6-Dinitro-2-methylphenol 29-132
135*22501670µg/Kg2,4-Dinitrophenol 27-129
97.016201670µg/Kg2,4-Dinitrotoluene 48-126
95.215901670µg/Kg2,6-Dinitrotoluene 46-124
86.814501670µg/KgDi-n-Octyl Phthalate 45-140
85.014201670µg/KgFluoranthene 50-127
89.214901670µg/KgFluorene 43-125
97.616301670µg/KgHexachlorobenzene 45-122
90.415101670µg/KgHexachlorobutadiene 32-123
84.414101670µg/KgHexachlorocyclopentadiene 32-117
68.811501670µg/KgHexachloroethane 28-117
90.415101670µg/KgIndeno(1,2,3-cd)pyrene 45-133
73.612301670µg/KgIsophorone 30-122
80.813501670µg/Kg1-Methylnaphthalene 40-119
81.413601670µg/Kg2-Methylnaphthalene 38-122
77.813001670µg/Kg2-Methylphenol 32-122
10317201670µg/Kg3&4 Methylphenol 34-119
77.813001670µg/KgNaphthalene 35-123
97.616301670µg/Kg2-Nitroaniline 44-127
97.616301670µg/Kg3-Nitroaniline 33-119
96.416101670µg/Kg4-Nitroaniline 63-147
56.89501670µg/KgNitrobenzene 34-122
Page 29 of 43* QC Fail Date:08/02/2023 09:05 AM
Page 134 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35527QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V35515
LCS-V35515Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10016701670µg/Kg2-Nitrophenol 36-123
10217001670µg/Kg4-Nitrophenol 30-132
59.39911670µg/KgN-Nitrosodimethylamine 10-146
10617701670µg/KgN-Nitrosodiphenylamine 38-127
72.412101670µg/KgN-Nitroso-di-n-propylamine 36-120
90.415101670µg/KgPentachlorophenol 25-133
86.814501670µg/KgPhenanthrene 50-121
71.211901670µg/KgPhenol 34-121
87.414601670µg/KgPyrene 47-127
45.57601670µg/KgPyridine 10-80
82.613801670µg/Kg1,2,4-Trichlorobenzene 34-118
97.616301670µg/Kg2,4,5-Trichlorophenol 41-124
98.216401670µg/Kg2,4,6-Trichlorophenol 39-126
91.02-Fluorobiphenyl (S)44-115
70.82-Fluorophenol (S)35-115
80.2Nitrobenzene-d5 (S)37-122
97.04-Terphenyl-d14 (S)54-127
83.12,4,6-Tribromophenol (S)39-132
63.9Phenol-d5 (S)34-121
V 89735-MS-V35515 V 89735-MSD-V35515Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1340 80.7130016701660< 116µg/KgAcenaphthene 77.8 40-123 3.0 20.0
1350 81.3133016701660< 105µg/KgAcenaphthylene 79.6 32-132 1.4 20.0
2410 145243016701660< 152µg/KgAniline 146 12-197 0.8 20.0
Page 30 of 43Date:08/02/2023 09:05 AM
Page 135 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35527QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V35515
V 89735-MS-V35515 V 89735-MSD-V35515Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1490 89.7148016701660< 143µg/KgAnthracene 88.6 47-123 0.6 20.0
1480 89.1149016701660< 139µg/KgBenzo(a)anthracene 89.2 49-126 0.6 20.0
1620 97.5163016701660< 147µg/KgBenzo(a)pyrene 97.6 45-129 0.6 20.0
1470 88.5146016701660< 146µg/KgBenzo(b)fluoranthene 87.4 45-132 0.6 20.0
1470 88.5149016701660< 136µg/KgBenzo(g,h,i)perylene 89.2 43-134 1.3 20.0
1550 93.3158016701660< 137µg/KgBenzo(k)fluoranthene 94.6 47-132 1.9 20.0
1520 91.5*172016701660< 580µg/KgBenzoic Acid 103*10-83 12.3 20.0
1430 86.1127016701660< 105µg/KgBenzyl alcohol 76.0 29-122 11.8 20.0
1350 81.3128016701660< 118µg/KgBis(2-Chloroethoxy)methane 76.6 36-121 5.3 20.0
1130 68.0104016701660< 107µg/KgBis(2-Chloroethyl)ether 62.2 31-120 8.2 20.0
1090 65.697516701660< 136µg/KgBis(2-Chloroisopropyl)ether 58.3 33-131 11.1 20.0
1420 85.5144016701660< 120µg/KgBis(2-ethylhexyl)phthalate 86.2 51-133 1.3 20.0
1580 95.1159016701660< 109µg/Kg4-Bromophenyl phenyl ether 95.2 46-124 0.6 20.0
1360 81.9138016701660< 113µg/KgButyl benzyl phthalate 82.6 48-132 1.4 20.0
1380 83.1135016701660< 92.4µg/Kg4-Chloro-3-methylphenol 80.8 45-122 2.1 20.0
1500 90.3145016701660< 112µg/Kg4-Chloroaniline 86.8 17-106 3.3 20.0
1390 83.7133016701660< 116µg/Kg2-Chloronaphthalene 79.6 41-114 4.4 20.0
1300 78.3118016701660< 98.2µg/Kg2-Chlorophenol 70.6 34-121 9.6 20.0
1490 89.7148016701660< 126µg/Kg4-Chlorophenyl phenyl ether 88.6 45-121 0.6 20.0
1440 86.7145016701660< 142µg/KgChrysene 86.8 50-124 0.6 20.0
1380 83.1139016701660< 230µg/KgDibenz(a,h)anthracene 83.2 45-134 0.7 20.0
1380 83.1136016701660< 119µg/KgDibenzofuran 81.4 44-120 1.4 20.0
1180 71.0105016701660< 94.4µg/Kg1,2-Dichlorobenzene 62.8 33-117 11.6 20.0
1150 69.2101016701660< 97.3µg/Kg1,3-Dichlorobenzene 60.4 30-115 12.9 20.0
1130 68.0100016701660< 97.5µg/Kg1,4-Dichlorobenzene 59.8 31-115 12.2 20.0
1110 66.8122016701660< 147µg/Kg3,3'-Dichlorobenzidine 73.0 22-121 9.4 20.0
Page 31 of 43* QC Fail Date:08/02/2023 09:05 AM
Page 136 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35527QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V35515
V 89735-MS-V35515 V 89735-MSD-V35515Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1500 90.3142016701660< 95.8µg/Kg2,4-Dichlorophenol 85.0 40-122 5.4 20.0
1410 84.9146016701660< 180µg/KgDiethyl phthalate 87.4 50-124 3.4 20.0
1440 86.7145016701660< 174µg/KgDimethyl phthalate 86.8 48-124 0.6 30.0
1880 113176016701660< 108µg/Kg2,4-Dimethylphenol 105 30-127 6.5 20.0
1540 92.7155016701660< 107µg/KgDi-n-butyl phthalate 92.8 51-128 0.6 20.0
1700 102180016701660< 240µg/Kg4,6-Dinitro-2-methylphenol 108 29-132 5.7 20.0
2660 160*293016701660< 520µg/Kg2,4-Dinitrophenol 175*27-129 9.6 20.0
1550 93.3160016701660< 96.6µg/Kg2,4-Dinitrotoluene 95.8 48-126 3.1 20.0
1520 91.5155016701660< 108µg/Kg2,6-Dinitrotoluene 92.8 46-124 1.9 20.0
1400 84.3141016701660< 143µg/KgDi-n-Octyl Phthalate 84.4 45-140 0.7 20.0
1410 84.9140016701660< 123µg/KgFluoranthene 83.8 50-127 0.7 20.0
1400 84.3139016701660< 128µg/KgFluorene 83.2 43-125 0.7 20.0
1600 96.3159016701660< 106µg/KgHexachlorobenzene 95.2 45-122 0.6 20.0
1440 86.7129016701660< 97.6µg/KgHexachlorobutadiene 77.2 32-123 10.9 20.0
1390 83.7126016701660< 157µg/KgHexachlorocyclopentadiene 75.4 32-117 9.8 20.0
1110 66.898516701660< 79.2µg/KgHexachloroethane 58.9 28-117 11.9 20.0
1490 89.7151016701660< 179µg/KgIndeno(1,2,3-cd)pyrene 90.4 45-133 1.3 20.0
1150 69.2110016701660< 191µg/KgIsophorone 65.8 30-122 4.4 20.0
1280 77.1121016701660< 106µg/Kg1-Methylnaphthalene 72.4 40-119 5.6 20.0
1310 78.9122016701660< 100µg/Kg2-Methylnaphthalene 73.0 38-122 7.1 20.0
1290 77.7122016701660< 97.0µg/Kg2-Methylphenol 73.0 32-122 5.5 20.0
1680 101157016701660< 84.9µg/Kg3&4 Methylphenol 94.0 34-119 6.7 20.0
1250 75.3114016701660< 144µg/KgNaphthalene 68.2 35-123 9.2 20.0
1530 92.1158016701660< 96.7µg/Kg2-Nitroaniline 94.6 44-127 3.2 20.0
1530 92.1158016701660< 120µg/Kg3-Nitroaniline 94.6 33-119 3.2 20.0
1400 84.3146016701660< 93.3µg/Kg4-Nitroaniline 87.4 63-147 4.1 20.0
Page 32 of 43* QC Fail Date:08/02/2023 09:05 AM
Page 137 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35527QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V35515
V 89735-MS-V35515 V 89735-MSD-V35515Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
934 56.286516701660< 116µg/KgNitrobenzene 51.7 34-122 7.6 20.0
1580 95.1144016701660< 88.8µg/Kg2-Nitrophenol 86.2 32-123 9.2 20.0
1730 104166016701660< 117µg/Kg4-Nitrophenol 99.4 30-132 4.1 20.0
938 56.583616701660< 263µg/KgN-Nitrosodimethylamine 50.0 10-146 11.4 30.0
1740 105172016701660< 181µg/KgN-Nitrosodiphenylamine 103 38-127 1.1 20.0
1150 69.2110016701660< 118µg/KgN-Nitroso-di-n-propylamine 65.8 36-120 4.4 20.0
1770 107194016701660< 347µg/KgPentachlorophenol 116 25-133 9.1 20.0
1400 84.3142016701660< 208µg/KgPhenanthrene 85.0 50-121 1.4 20.0
1160 69.8108016701660< 112µg/KgPhenol 64.6 34-121 7.1 20.0
1430 86.1145016701660< 134µg/KgPyrene 86.8 47-127 1.3 20.0
240 14.427016701660< 79.2µg/KgPyridine 16.1 10-80 11.7 20.0
1280 77.1118016701660< 107µg/Kg1,2,4-Trichlorobenzene 70.6 34-118 8.1 20.0
1510 90.9154016701660< 96.2µg/Kg2,4,5-Trichlorophenol 92.2 41-124 1.9 20.0
1570 94.5149016701660< 96.6µg/Kg2,4,6-Trichlorophenol 89.2 39-126 5.2 20.0
78.92-Fluorobiphenyl (S)75.4 44-115
65.42-Fluorophenol (S)60.3 35-115
73.4Nitrobenzene-d5 (S)67.6 37-122
89.74-Terphenyl-d14 (S)88.6 54-127
77.12,4,6-Tribromophenol (S)77.4 39-132
58.2Phenol-d5 (S)54.3 34-121
Page 33 of 43Date:08/02/2023 09:05 AM
Page 138 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V35516
Associated Lab Samples: 89743, 89744, 89745, 89746, 89747
LRB-V35516 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/21/23 14:012.000.302<0.302µg/LAcenaphthene
07/21/23 14:012.000.297<0.297µg/LAcenaphthylene
07/21/23 14:015.002.05<2.05µg/LAniline
07/21/23 14:012.000.836<0.836µg/LAnthracene
07/21/23 14:012.000.637<0.637µg/LBenzo(a)anthracene
07/21/23 14:012.001.02<1.02µg/LBenzo(a)pyrene
07/21/23 14:015.002.49<2.49µg/LBenzo(b)fluoranthene
07/21/23 14:015.001.01<1.01µg/LBenzo(g,h,i)perylene
07/21/23 14:015.001.99<1.99µg/LBenzo(k)fluoranthene
07/21/23 14:0110.01.10<1.10µg/LBenzoic Acid
07/21/23 14:015.000.684<0.684µg/LBenzyl alcohol
07/21/23 14:015.000.468<0.468µg/LBis(2-Chloroethoxy)methane
07/21/23 14:015.001.04<1.04µg/LBis(2-Chloroethyl)ether
07/21/23 14:015.001.08<1.08µg/LBis(2-Chloroisopropyl)ether
07/21/23 14:0110.03.46<3.46µg/LBis(2-ethylhexyl)phthalate
07/21/23 14:015.001.11<1.11µg/L4-Bromophenyl phenyl ether
07/21/23 14:015.001.83<1.83µg/LButyl benzyl phthalate
07/21/23 14:015.001.18<1.18µg/L4-Chloro-3-methylphenol
07/21/23 14:015.001.33<1.33µg/L4-Chloroaniline
07/21/23 14:0120.01.83<1.83µg/L2-Chloronaphthalene
07/21/23 14:0110.00.938<0.938µg/L2-Chlorophenol
07/21/23 14:015.001.71<1.71µg/L4-Chlorophenyl phenyl ether
07/21/23 14:012.000.405<0.405µg/LChrysene
07/21/23 14:012.000.434<0.434µg/LDibenz(a,h)anthracene
07/21/23 14:015.000.856<0.856µg/LDibenzofuran
07/21/23 14:015.002.00<2.00µg/L1,2-Dichlorobenzene
07/21/23 14:015.002.00<2.00µg/L1,3-Dichlorobenzene
Page 34 of 43Date:08/02/2023 09:05 AM
Page 139 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V35516
Associated Lab Samples: 89743, 89744, 89745, 89746, 89747
LRB-V35516 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/21/23 14:015.002.05<2.05µg/L1,4-Dichlorobenzene
07/21/23 14:015.001.89<1.89µg/L3,3'-Dichlorobenzidine
07/21/23 14:0110.01.46<1.46µg/L2,4-Dichlorophenol
07/21/23 14:015.000.745<0.745µg/LDiethyl phthalate
07/21/23 14:015.000.939<0.939µg/LDimethyl phthalate
07/21/23 14:0120.01.57<1.57µg/L2,4-Dimethylphenol
07/21/23 14:015.002.06<2.06µg/LDi-n-butyl phthalate
07/21/23 14:0110.02.07<2.07µg/L4,6-Dinitro-2-methylphenol
07/21/23 14:0110.01.92<1.92µg/L2,4-Dinitrophenol
07/21/23 14:015.001.11<1.11µg/L2,4-Dinitrotoluene
07/21/23 14:015.000.809<0.809µg/L2,6-Dinitrotoluene
07/21/23 14:015.001.65<1.65µg/LDi-n-Octyl Phthalate
07/21/23 14:012.000.250<0.250µg/LFluoranthene
07/21/23 14:012.000.807<0.807µg/LFluorene
07/21/23 14:015.000.979<0.979µg/LHexachlorobenzene
07/21/23 14:015.002.73<2.73µg/LHexachlorobutadiene
07/21/23 14:015.002.05<2.05µg/LHexachlorocyclopentadiene
07/21/23 14:015.001.76<1.76µg/LHexachloroethane
07/21/23 14:012.000.477<0.477µg/LIndeno(1,2,3-cd)pyrene
07/21/23 14:015.000.444<0.444µg/LIsophorone
07/21/23 14:012.001.14<1.14µg/L1-Methylnaphthalene
07/21/23 14:012.000.666<0.666µg/L2-Methylnaphthalene
07/21/23 14:015.001.15<1.15µg/L2-Methylphenol
07/21/23 14:0110.00.880<0.880µg/L3&4 Methylphenol
07/21/23 14:012.000.728<0.728µg/LNaphthalene
07/21/23 14:015.001.39<1.39µg/L2-Nitroaniline
07/21/23 14:015.001.39<1.39µg/L3-Nitroaniline
Page 35 of 43Date:08/02/2023 09:05 AM
Page 140 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V35516
Associated Lab Samples: 89743, 89744, 89745, 89746, 89747
LRB-V35516 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/21/23 14:015.001.53<1.53µg/L4-Nitroaniline
07/21/23 14:015.000.905<0.905µg/LNitrobenzene
07/21/23 14:015.000.493<0.493µg/L2-Nitrophenol
07/21/23 14:0110.01.23<1.23µg/L4-Nitrophenol
07/21/23 14:015.000.450<0.450µg/LN-Nitrosodimethylamine
07/21/23 14:015.001.10<1.10µg/LN-Nitrosodiphenylamine
07/21/23 14:015.000.641<0.641µg/LN-Nitroso-di-n-propylamine
07/21/23 14:015.001.43<1.43µg/LPentachlorophenol
07/21/23 14:012.000.428<0.428µg/LPhenanthrene
07/21/23 14:015.000.651<0.651µg/LPhenol
07/21/23 14:012.000.434<0.434µg/LPyrene
07/21/23 14:015.001.20<1.20µg/LPyridine
07/21/23 14:015.002.21<2.21µg/L1,2,4-Trichlorobenzene
07/21/23 14:015.001.31<1.31µg/L2,4,5-Trichlorophenol
07/21/23 14:015.001.32<1.32µg/L2,4,6-Trichlorophenol
07/21/23 14:012-Fluorobiphenyl (S)71.2 44-119
07/21/23 14:012-Fluorophenol (S)35.3 19-119
07/21/23 14:01Nitrobenzene-d5 (S)67.4 44-120
07/21/23 14:014-Terphenyl-d14 (S)85.8 50-134
07/21/23 14:012,4,6-Tribromophenol (S)68.1 43-140
07/21/23 14:01Phenol-d5 (S)23.5 11-100
LCS-V35516 LCSD-V35516Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
31.5 63.066.433.250.0µg/LAcenaphthene 38-117 5.2 20.0
Page 36 of 43Date:08/02/2023 09:05 AM
Page 141 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V35516
LCS-V35516 LCSD-V35516Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
31.8 63.666.233.150.0µg/LAcenaphthylene 41-130 4.0 20.0
78.3 15717687.950.0µg/LAniline 12-197 11.5 20.0
39.2 78.478.439.250.0µg/LAnthracene 57-123 0.0 20.0
39.8 79.680.840.450.0µg/LBenzo(a)anthracene 58-125 1.4 20.0
43.6 87.287.243.650.0µg/LBenzo(a)pyrene 54-128 0.0 20.0
41.0 82.083.041.550.0µg/LBenzo(b)fluoranthene 53-131 1.2 20.0
39.2 78.477.838.950.0µg/LBenzo(g,h,i)perylene 50-134 0.7 20.0
42.9 85.883.241.650.0µg/LBenzo(k)fluoranthene 53-131 3.0 20.0
15.9 31.835.217.650.0µg/LBenzoic Acid 10-125 10.1 20.0
36.4 72.879.639.850.0µg/LBenzyl alcohol 31-112 8.9 20.0
34.8 69.671.635.850.0µg/LBis(2-Chloroethoxy)methane 48-120 2.8 20.0
27.3 54.653.626.850.0µg/LBis(2-Chloroethyl)ether 43-118 1.8 20.0
30.6 61.263.031.550.0µg/LBis(2-Chloroisopropyl)ether 37-130 2.8 20.0
41.4 82.885.442.750.0µg/LBis(2-ethylhexyl)phthalate 55-135 3.0 20.0
38.9 77.875.237.650.0µg/L4-Bromophenyl phenyl ether 55-124 3.3 20.0
41.1 82.285.642.850.0µg/LButyl benzyl phthalate 53-134 4.0 20.0
39.6 79.285.442.750.0µg/L4-Chloro-3-methylphenol 52-119 7.5 20.0
53.9 10810552.750.0µg/L4-Chloroaniline 33-117 2.2 20.0
31.0 62.065.032.550.0µg/L2-Chloronaphthalene 40-116 4.7 20.0
30.8 61.664.432.250.0µg/L2-Chlorophenol 38-117 4.4 20.0
36.9 73.874.837.450.0µg/L4-Chlorophenyl phenyl ether 53-121 1.3 20.0
39.5 79.080.040.050.0µg/LChrysene 59-123 1.2 20.0
36.4 72.873.836.950.0µg/LDibenz(a,h)anthracene 51-134 1.3 20.0
33.2 66.467.833.950.0µg/LDibenzofuran 53-118 2.0 20.0
24.1 48.250.825.450.0µg/L1,2-Dichlorobenzene 32-111 5.2 20.0
22.9 45.848.224.150.0µg/L1,3-Dichlorobenzene 28-110 5.1 20.0
Page 37 of 43Date:08/02/2023 09:05 AM
Page 142 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V35516
LCS-V35516 LCSD-V35516Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.7 45.450.425.250.0µg/L1,4-Dichlorobenzene 29-112 10.4 20.0
34.9 69.872.236.150.0µg/L3,3'-Dichlorobenzidine 27-129 3.3 20.0
37.2 74.474.237.150.0µg/L2,4-Dichlorophenol 47-121 0.2 20.0
37.9 75.880.640.350.0µg/LDiethyl phthalate 56-125 6.1 20.0
38.8 77.680.040.050.0µg/LDimethyl phthalate 45-127 3.0 20.0
44.9 89.891.645.850.0µg/L2,4-Dimethylphenol 31-124 1.9 20.0
43.5 87.086.843.450.0µg/LDi-n-butyl phthalate 59-127 0.2 20.0
37.0 74.072.636.350.0µg/L4,6-Dinitro-2-methylphenol 44-137 1.9 20.0
33.4 66.870.835.450.0µg/L2,4-Dinitrophenol 23-143 5.8 20.0
39.9 79.880.640.350.0µg/L2,4-Dinitrotoluene 57-128 0.9 20.0
39.4 78.880.040.050.0µg/L2,6-Dinitrotoluene 57-124 1.5 20.0
42.4 84.885.642.850.0µg/LDi-n-Octyl Phthalate 51-140 0.9 20.0
36.4 72.871.835.950.0µg/LFluoranthene 57-128 1.3 20.0
35.3 70.671.835.950.0µg/LFluorene 52-124 1.6 20.0
40.1 80.278.039.050.0µg/LHexachlorobenzene 53-125 2.7 20.0
26.4 52.854.027.050.0µg/LHexachlorobutadiene 22-124 2.2 20.0
22.2 44.445.422.750.0µg/LHexachlorocyclopentadiene 32-117 2.2 20.0
21.5 43.046.823.450.0µg/LHexachloroethane 21-115 8.4 20.0
38.9 77.878.639.350.0µg/LIndeno(1,2,3-cd)pyrene 52-134 1.0 20.0
31.0 62.064.232.150.0µg/LIsophorone 42-124 3.4 20.0
29.9 59.865.632.850.0µg/L1-Methylnaphthalene 41-119 9.2 20.0
27.6 55.262.031.050.0µg/L2-Methylnaphthalene 40-121 11.6 20.0
30.3 60.664.232.150.0µg/L2-Methylphenol 30-117 5.7 20.0
25.6 51.255.627.850.0µg/L3&4 Methylphenol 29-110 8.2 20.0
28.0 56.058.229.150.0µg/LNaphthalene 40-121 3.8 20.0
46.7 93.492.846.450.0µg/L2-Nitroaniline 55-127 0.6 20.0
Page 38 of 43Date:08/02/2023 09:05 AM
Page 143 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V35550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V35516
LCS-V35516 LCSD-V35516Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
46.7 93.492.846.450.0µg/L3-Nitroaniline 41-128 0.6 20.0
44.7 89.487.843.950.0µg/L4-Nitroaniline 45-135 1.8 20.0
29.6 59.260.230.150.0µg/LNitrobenzene 45-121 1.6 20.0
31.5 63.064.032.050.0µg/L2-Nitrophenol 47-123 1.5 20.0
29.9 59.864.432.250.0µg/L4-Nitrophenol 10-105 7.4 20.0
22.4 44.848.224.150.0µg/LN-Nitrosodimethylamine 10-119 7.3 20.0
46.1 92.292.246.150.0µg/LN-Nitrosodiphenylamine 51-123 0.0 20.0
32.9 65.866.833.450.0µg/LN-Nitroso-di-n-propylamine 49-119 1.5 20.0
41.8 83.673.636.850.0µg/LPentachlorophenol 35-138 12.7 20.0
39.7 79.476.838.450.0µg/LPhenanthrene 59-120 3.3 20.0
13.9 27.830.615.350.0µg/LPhenol 12-58 9.5 20.0
39.1 78.278.239.150.0µg/LPyrene 57-126 0.0 20.0
12.2 24.432.616.350.0µg/LPyridine 10-80 28.7*20.0
25.8 51.654.427.250.0µg/L1,2,4-Trichlorobenzene 29-126 5.2 20.0
36.5 73.077.238.650.0µg/L2,4,5-Trichlorophenol 53-123 5.5 20.0
35.4 70.874.237.150.0µg/L2,4,6-Trichlorophenol 50-125 4.6 20.0
66.070.02-Fluorobiphenyl (S)44-119
35.040.62-Fluorophenol (S)19-119
58.662.6Nitrobenzene-d5 (S)44-120
84.686.04-Terphenyl-d14 (S)50-134
74.272.42,4,6-Tribromophenol (S)43-140
20.524.7Phenol-d5 (S)11-100
Page 39 of 43* QC Fail Date:08/02/2023 09:05 AM
Page 144 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L694239QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L693875
Associated Lab Samples: 89735, 89736, 89737, 89738, 89739, 89740, 89741, 89742
LRB-L693875 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
07/31/23 16:260.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L693875Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
82.53.304.00mg/KgChromium, Hexavalent 80-120
V 89735-DUP-L693875Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/31/23 17:20111*<0.2000.701mg/KgChromium, Hexavalent
V 89735-MS-L693875Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
25.7 62.8*39.80.701mg/KgChromium, Hexavalent 75-125
Page 40 of 43* QC Fail Date:08/02/2023 09:05 AM
Page 145 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
Dry Weight Determination
SW-DRYWT
V35484QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89647-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/18/23 18:455.112.011.4%Moisture
V 89665-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/18/23 18:453.019.119.7%Moisture
Page 41 of 43Date:08/02/2023 09:05 AM
Page 146 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
Dry Weight Determination
SW-DRYWT
V35506QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89512-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/19/23 11:501.717.016.7%Moisture
V 89979-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/19/23 11:501.433.133.6%Moisture
Page 42 of 43Date:08/02/2023 09:05 AM
Page 147 of 151
Quality Control Data
23-198-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TPI-002
Dry Weight Determination
SW-DRYWT
V35528QC Analytical Batch:
Analysis Method:
Analysis Description:
V 90002-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/19/23 18:301.413.713.5%Moisture
V 90011-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/19/23 18:302.920.419.8%Moisture
Page 43 of 43Date:08/02/2023 09:05 AM
Page 148 of 151
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-198-0001
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.2C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:07/17/2023 09:24:41
Special precautions or instructions included?
Comments:
Page 149 of 151
Page 150 of 151
Page 151 of 151

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

7/21/2023
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 23-198-0006 Client Project Description: Former Abels Auto
TPI-002
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/14/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 43
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-198-0006
Page 2 of 43
Report Number:
Sample Summary Table
Client Project Description:
23-198-0006
Former Abels Auto
TPI-002
Lab No Client Sample ID Matrix Date Collected Date Received
07/13/2023 11:11Air 89804 SG-2 07/14/2023 16:50
07/13/2023Air 89805 SG-DUP 07/14/2023 16:50
07/12/2023 15:35Air 89806 SG-7 07/14/2023 16:50
07/12/2023 16:49Air 89807 SG-6 07/14/2023 16:50
07/13/2023 10:25Air 89808 SG-5 07/14/2023 16:50
07/12/2023 14:58Air 89809 SG-1 07/14/2023 16:50
07/13/2023 13:05Air 89810 SG-4 07/14/2023 16:50
07/13/2023 11:52Air 89811 SG-3 07/14/2023 16:50
Page 3 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0006
Report Limit
Project:Former Abels Auto
V 89804SG-2
84.2 07/18/2023 16:56TO-15 Acetone µg/m3 0.202
14.9 07/18/2023 16:56TO-15 Benzene µg/m3 0.073
1.96 07/18/2023 16:56TO-15 1,3-Butadiene µg/m3 0.328
32.5 07/18/2023 16:56TO-15 Carbon Disulfide µg/m3 0.060
44.5 07/18/2023 16:56TO-15 Chloroform µg/m3 0.086
4.39 07/18/2023 16:56TO-15 Dichlorodifluoromethane µg/m3 0.134
J0.526 07/18/2023 16:56TO-15 Ethyl Acetate µg/m3 0.136
21.2 07/18/2023 16:56TO-15 Ethylbenzene µg/m3 0.106
7.33 07/18/2023 16:56TO-15 4-Ethyltoluene µg/m3 0.128
16.4 07/18/2023 16:56TO-15 Heptane µg/m3 0.143
5.03 07/18/2023 16:56TO-15 n-Hexane µg/m3 0.047
3.33 07/18/2023 16:56TO-15 2-Hexanone µg/m3 0.285
JB1.76 07/18/2023 16:56TO-15 Isopropyl Alcohol µg/m3 0.139
17.6 07/18/2023 16:56TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
3.59 07/18/2023 16:56TO-15 4-Methyl-2-Pentanone µg/m3 0.121
22.3 07/18/2023 16:56TO-15 Methylene Chloride µg/m3 0.488
20.3 07/18/2023 16:56TO-15 Propene µg/m3 0.242
4.31 07/18/2023 16:56TO-15 Styrene µg/m3 0.124
234 07/18/2023 16:56TO-15 Tetrachloroethene µg/m3 0.181
J0.852 07/18/2023 16:56TO-15 Tetrahydrofuran µg/m3 0.107
118 07/18/2023 16:56TO-15 Toluene µg/m3 0.090
J1.21 07/18/2023 16:56TO-15 1,1,1-Trichloroethane µg/m3 0.144
7.88 07/18/2023 16:56TO-15 Trichlorofluoromethane µg/m3 0.130
25.8 07/18/2023 16:56TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
6.64 07/18/2023 16:56TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
25.4 07/18/2023 16:56TO-15 o-Xylene µg/m3 0.157
63.9 07/18/2023 16:56TO-15 m,p-Xylene µg/m3 0.217
89.3 07/18/2023 16:56TO-15 Xylene (Total)µg/m3 0.157
V 89805SG-DUP
77.3 07/18/2023 17:50TO-15 Acetone µg/m3 0.202
15.1 07/18/2023 17:50TO-15 Benzene µg/m3 0.073
6.59 07/18/2023 17:50TO-15 1,3-Butadiene µg/m3 0.328
31.5 07/18/2023 17:50TO-15 Carbon Disulfide µg/m3 0.060
42.8 07/18/2023 17:50TO-15 Chloroform µg/m3 0.086
4.39 07/18/2023 17:50TO-15 Dichlorodifluoromethane µg/m3 0.134
20.6 07/18/2023 17:50TO-15 Ethylbenzene µg/m3 0.106
Page 4 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0006
Report Limit
Project:Former Abels Auto
V 89805SG-DUP
6.92 07/18/2023 17:50TO-15 4-Ethyltoluene µg/m3 0.128
J0.743 07/18/2023 17:50TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
16.8 07/18/2023 17:50TO-15 Heptane µg/m3 0.143
4.53 07/18/2023 17:50TO-15 n-Hexane µg/m3 0.047
3.24 07/18/2023 17:50TO-15 2-Hexanone µg/m3 0.285
JB1.32 07/18/2023 17:50TO-15 Isopropyl Alcohol µg/m3 0.139
17.2 07/18/2023 17:50TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
3.83 07/18/2023 17:50TO-15 4-Methyl-2-Pentanone µg/m3 0.121
21.2 07/18/2023 17:50TO-15 Methylene Chloride µg/m3 0.488
19.7 07/18/2023 17:50TO-15 Propene µg/m3 0.242
222 07/18/2023 17:50TO-15 Tetrachloroethene µg/m3 0.181
J1.28 07/18/2023 17:50TO-15 Tetrahydrofuran µg/m3 0.107
113 07/18/2023 17:50TO-15 Toluene µg/m3 0.090
J1.11 07/18/2023 17:50TO-15 1,1,1-Trichloroethane µg/m3 0.144
8.15 07/18/2023 17:50TO-15 Trichlorofluoromethane µg/m3 0.130
25.0 07/18/2023 17:50TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
6.35 07/18/2023 17:50TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
24.8 07/18/2023 17:50TO-15 o-Xylene µg/m3 0.157
61.9 07/18/2023 17:50TO-15 m,p-Xylene µg/m3 0.217
86.7 07/18/2023 17:50TO-15 Xylene (Total)µg/m3 0.157
V 89806SG-7
59.0 07/18/2023 18:49TO-15 Acetone µg/m3 0.202
2.92 07/18/2023 18:49TO-15 Benzene µg/m3 0.073
6.29 07/18/2023 18:49TO-15 Carbon Disulfide µg/m3 0.060
J0.434 07/18/2023 18:49TO-15 Chloroform µg/m3 0.086
8.12 07/18/2023 18:49TO-15 Cyclohexane µg/m3 0.161
J1.22 07/18/2023 18:49TO-15 Dichlorodifluoromethane µg/m3 0.134
J1.31 07/18/2023 18:49TO-15 1,1-Dichloroethane µg/m3 0.101
J0.535 07/18/2023 18:49TO-15 cis-1,2-Dichloroethene µg/m3 0.095
J1.02 07/18/2023 18:49TO-15 Ethylbenzene µg/m3 0.106
10.3 07/18/2023 18:49TO-15 Heptane µg/m3 0.143
13.1 07/18/2023 18:49TO-15 n-Hexane µg/m3 0.047
5.92 07/18/2023 18:49TO-15 Isopropyl Alcohol µg/m3 0.139
14.0 07/18/2023 18:49TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J1.14 07/18/2023 18:49TO-15 4-Methyl-2-Pentanone µg/m3 0.121
92.6 07/17/2023 17:04TO-15 Propene µg/m3 4.84
Page 5 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0006
Report Limit
Project:Former Abels Auto
V 89806SG-7
4.16 07/18/2023 18:49TO-15 Styrene µg/m3 0.124
12.6 07/18/2023 18:49TO-15 Tetrachloroethene µg/m3 0.181
6.39 07/18/2023 18:49TO-15 Tetrahydrofuran µg/m3 0.107
12.5 07/18/2023 18:49TO-15 Toluene µg/m3 0.090
J2.00 07/18/2023 18:49TO-15 Trichloroethene µg/m3 0.199
J1.50 07/18/2023 18:49TO-15 Trichlorofluoromethane µg/m3 0.130
4.49 07/18/2023 18:49TO-15 o-Xylene µg/m3 0.157
J5.47 07/18/2023 18:49TO-15 m,p-Xylene µg/m3 0.217
J9.96 07/18/2023 18:49TO-15 Xylene (Total)µg/m3 0.157
V 89807SG-6
357 07/17/2023 17:41TO-15 Acetone µg/m3 4.04
21.0 07/18/2023 19:45TO-15 Benzene µg/m3 0.073
29.6 07/18/2023 19:45TO-15 1,3-Butadiene µg/m3 0.328
70.9 07/18/2023 19:45TO-15 Carbon Disulfide µg/m3 0.060
J0.497 07/18/2023 19:45TO-15 Chloroform µg/m3 0.086
3.53 07/18/2023 19:45TO-15 Dichlorodifluoromethane µg/m3 0.134
11.7 07/18/2023 19:45TO-15 1,1-Dichloroethane µg/m3 0.101
2.28 07/18/2023 19:45TO-15 cis-1,2-Dichloroethene µg/m3 0.095
14.1 07/18/2023 19:45TO-15 Ethylbenzene µg/m3 0.106
5.48 07/18/2023 19:45TO-15 4-Ethyltoluene µg/m3 0.128
J0.796 07/18/2023 19:45TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
36.7 07/18/2023 19:45TO-15 Heptane µg/m3 0.143
19.1 07/18/2023 19:45TO-15 n-Hexane µg/m3 0.047
6.54 07/18/2023 19:45TO-15 Isopropyl Alcohol µg/m3 0.139
58.2 07/18/2023 19:45TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J1.98 07/18/2023 19:45TO-15 4-Methyl-2-Pentanone µg/m3 0.121
J0.958 07/18/2023 19:45TO-15 Methylene Chloride µg/m3 0.488
424 07/17/2023 17:41TO-15 Propene µg/m3 4.84
4.19 07/18/2023 19:45TO-15 Styrene µg/m3 0.124
181 07/18/2023 19:45TO-15 Tetrachloroethene µg/m3 0.181
3.44 07/18/2023 19:45TO-15 Tetrahydrofuran µg/m3 0.107
71.2 07/18/2023 19:45TO-15 Toluene µg/m3 0.090
J0.878 07/18/2023 19:45TO-15 1,1,1-Trichloroethane µg/m3 0.144
2.59 07/18/2023 19:45TO-15 Trichloroethene µg/m3 0.199
3.19 07/18/2023 19:45TO-15 Trichlorofluoromethane µg/m3 0.130
21.4 07/18/2023 19:45TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
Page 6 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0006
Report Limit
Project:Former Abels Auto
V 89807SG-6
4.94 07/18/2023 19:45TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
20.6 07/18/2023 19:45TO-15 o-Xylene µg/m3 0.157
43.4 07/18/2023 19:45TO-15 m,p-Xylene µg/m3 0.217
64.0 07/18/2023 19:45TO-15 Xylene (Total)µg/m3 0.157
V 89808SG-5
47.3 07/18/2023 20:41TO-15 Acetone µg/m3 0.202
15.0 07/18/2023 20:41TO-15 Benzene µg/m3 0.073
24.2 07/18/2023 20:41TO-15 1,3-Butadiene µg/m3 0.328
46.4 07/18/2023 20:41TO-15 Carbon Disulfide µg/m3 0.060
J0.303 07/18/2023 20:41TO-15 Chloroethane µg/m3 0.164
J0.463 07/18/2023 20:41TO-15 Chloroform µg/m3 0.086
13.0 07/18/2023 20:41TO-15 Cyclohexane µg/m3 0.161
J1.50 07/18/2023 20:41TO-15 1,4-Dichlorobenzene µg/m3 0.186
4.22 07/18/2023 20:41TO-15 Dichlorodifluoromethane µg/m3 0.134
J1.53 07/18/2023 20:41TO-15 1,1-Dichloroethane µg/m3 0.101
5.54 07/18/2023 20:41TO-15 cis-1,2-Dichloroethene µg/m3 0.095
J1.79 07/18/2023 20:41TO-15 Ethyl Acetate µg/m3 0.136
5.35 07/18/2023 20:41TO-15 Ethylbenzene µg/m3 0.106
J1.37 07/18/2023 20:41TO-15 4-Ethyltoluene µg/m3 0.128
J0.620 07/18/2023 20:41TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
35.1 07/18/2023 20:41TO-15 Heptane µg/m3 0.143
22.6 07/18/2023 20:41TO-15 n-Hexane µg/m3 0.047
21.5 07/18/2023 20:41TO-15 2-Hexanone µg/m3 0.285
5.50 07/18/2023 20:41TO-15 Isopropyl Alcohol µg/m3 0.139
7.53 07/18/2023 20:41TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
2.32 07/18/2023 20:41TO-15 4-Methyl-2-Pentanone µg/m3 0.121
1.79 07/18/2023 20:41TO-15 Methylene Chloride µg/m3 0.488
514 07/17/2023 18:18TO-15 Propene µg/m3 4.84
4.17 07/18/2023 20:41TO-15 Styrene µg/m3 0.124
77.5 07/18/2023 20:41TO-15 Tetrachloroethene µg/m3 0.181
15.1 07/18/2023 20:41TO-15 Tetrahydrofuran µg/m3 0.107
42.3 07/18/2023 20:41TO-15 Toluene µg/m3 0.090
15.7 07/18/2023 20:41TO-15 Trichloroethene µg/m3 0.199
5.56 07/18/2023 20:41TO-15 Trichlorofluoromethane µg/m3 0.130
6.44 07/18/2023 20:41TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J2.22 07/18/2023 20:41TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
Page 7 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0006
Report Limit
Project:Former Abels Auto
V 89808SG-5
3.68 07/18/2023 20:41TO-15 Vinyl Chloride µg/m3 0.127
7.23 07/18/2023 20:41TO-15 o-Xylene µg/m3 0.157
17.1 07/18/2023 20:41TO-15 m,p-Xylene µg/m3 0.217
24.3 07/18/2023 20:41TO-15 Xylene (Total)µg/m3 0.157
V 89809SG-1
33.1 07/18/2023 21:39TO-15 Acetone µg/m3 0.202
4.36 07/18/2023 21:39TO-15 Benzene µg/m3 0.073
1.44 07/18/2023 21:39TO-15 1,3-Butadiene µg/m3 0.328
18.1 07/18/2023 21:39TO-15 Carbon Disulfide µg/m3 0.060
33.7 07/18/2023 21:39TO-15 Chloroform µg/m3 0.086
3.35 07/18/2023 21:39TO-15 Dichlorodifluoromethane µg/m3 0.134
6.40 07/18/2023 21:39TO-15 Ethylbenzene µg/m3 0.106
J1.72 07/18/2023 21:39TO-15 4-Ethyltoluene µg/m3 0.128
J0.582 07/18/2023 21:39TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
13.0 07/18/2023 21:39TO-15 Heptane µg/m3 0.143
10.0 07/18/2023 21:39TO-15 n-Hexane µg/m3 0.047
JB2.15 07/18/2023 21:39TO-15 Isopropyl Alcohol µg/m3 0.139
6.66 07/18/2023 21:39TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
3.05 07/18/2023 21:39TO-15 4-Methyl-2-Pentanone µg/m3 0.121
J0.753 07/18/2023 21:39TO-15 Methylene Chloride µg/m3 0.488
13.7 07/18/2023 21:39TO-15 Propene µg/m3 0.242
3.95 07/18/2023 21:39TO-15 Styrene µg/m3 0.124
54.1 07/18/2023 21:39TO-15 Tetrachloroethene µg/m3 0.181
J0.757 07/18/2023 21:39TO-15 Tetrahydrofuran µg/m3 0.107
26.6 07/18/2023 21:39TO-15 Toluene µg/m3 0.090
3.06 07/18/2023 21:39TO-15 Trichlorofluoromethane µg/m3 0.130
5.57 07/18/2023 21:39TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J1.43 07/18/2023 21:39TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
6.74 07/18/2023 21:39TO-15 o-Xylene µg/m3 0.157
22.8 07/18/2023 21:39TO-15 m,p-Xylene µg/m3 0.217
29.5 07/18/2023 21:39TO-15 Xylene (Total)µg/m3 0.157
V 89810SG-4
40.7 07/18/2023 22:34TO-15 Acetone µg/m3 0.202
16.7 07/18/2023 22:34TO-15 Benzene µg/m3 0.073
14.3 07/18/2023 22:34TO-15 1,3-Butadiene µg/m3 0.328
42.9 07/18/2023 22:34TO-15 Carbon Disulfide µg/m3 0.060
Page 8 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0006
Report Limit
Project:Former Abels Auto
V 89810SG-4
J1.20 07/18/2023 22:34TO-15 Chloroethane µg/m3 0.164
J0.761 07/18/2023 22:34TO-15 Chloroform µg/m3 0.086
8.95 07/18/2023 22:34TO-15 Cyclohexane µg/m3 0.161
3.48 07/18/2023 22:34TO-15 Dichlorodifluoromethane µg/m3 0.134
28.6 07/18/2023 22:34TO-15 1,1-Dichloroethane µg/m3 0.101
27.5 07/18/2023 22:34TO-15 cis-1,2-Dichloroethene µg/m3 0.095
2.27 07/18/2023 22:34TO-15 Ethylbenzene µg/m3 0.106
J0.737 07/18/2023 22:34TO-15 4-Ethyltoluene µg/m3 0.128
J0.712 07/18/2023 22:34TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
21.4 07/18/2023 22:34TO-15 Heptane µg/m3 0.143
37.9 07/18/2023 22:34TO-15 n-Hexane µg/m3 0.047
J3.86 07/18/2023 22:34TO-15 Isopropyl Alcohol µg/m3 0.139
10.0 07/18/2023 22:34TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
2.55 07/18/2023 22:34TO-15 4-Methyl-2-Pentanone µg/m3 0.121
J1.18 07/18/2023 22:34TO-15 Methylene Chloride µg/m3 0.488
7.11 07/18/2023 22:34TO-15 Naphthalene µg/m3 0.183
294 07/17/2023 19:31TO-15 Propene µg/m3 4.84
4.36 07/18/2023 22:34TO-15 Styrene µg/m3 0.124
22.5 07/18/2023 22:34TO-15 Tetrachloroethene µg/m3 0.181
6.65 07/18/2023 22:34TO-15 Tetrahydrofuran µg/m3 0.107
15.7 07/18/2023 22:34TO-15 Toluene µg/m3 0.090
J2.67 07/18/2023 22:34TO-15 1,1,1-Trichloroethane µg/m3 0.144
24.7 07/18/2023 22:34TO-15 Trichloroethene µg/m3 0.199
3.51 07/18/2023 22:34TO-15 Trichlorofluoromethane µg/m3 0.130
3.34 07/18/2023 22:34TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J0.963 07/18/2023 22:34TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
5.47 07/18/2023 22:34TO-15 Vinyl Chloride µg/m3 0.127
2.49 07/18/2023 22:34TO-15 o-Xylene µg/m3 0.157
8.49 07/18/2023 22:34TO-15 m,p-Xylene µg/m3 0.217
11.0 07/18/2023 22:34TO-15 Xylene (Total)µg/m3 0.157
V 89811SG-3
28.4 07/18/2023 23:31TO-15 Acetone µg/m3 0.202
35.0 07/18/2023 23:31TO-15 Benzene µg/m3 0.073
22.8 07/18/2023 23:31TO-15 1,3-Butadiene µg/m3 0.328
176 07/17/2023 20:08TO-15 Carbon Disulfide µg/m3 1.22
16.0 07/18/2023 23:31TO-15 Chloroform µg/m3 0.086
Page 9 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-198-0006
Report Limit
Project:Former Abels Auto
V 89811SG-3
10.3 07/18/2023 23:31TO-15 Cyclohexane µg/m3 0.161
3.62 07/18/2023 23:31TO-15 Dichlorodifluoromethane µg/m3 0.134
35.5 07/18/2023 23:31TO-15 Ethylbenzene µg/m3 0.106
8.37 07/18/2023 23:31TO-15 4-Ethyltoluene µg/m3 0.128
J0.881 07/18/2023 23:31TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
155 07/18/2023 23:31TO-15 Heptane µg/m3 0.143
24.8 07/18/2023 23:31TO-15 n-Hexane µg/m3 0.047
JB2.87 07/18/2023 23:31TO-15 Isopropyl Alcohol µg/m3 0.139
7.73 07/18/2023 23:31TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
4.02 07/18/2023 23:31TO-15 4-Methyl-2-Pentanone µg/m3 0.121
J1.61 07/18/2023 23:31TO-15 Methylene Chloride µg/m3 0.488
5.59 07/18/2023 23:31TO-15 Naphthalene µg/m3 0.183
21.3 07/18/2023 23:31TO-15 Propene µg/m3 0.242
4.26 07/18/2023 23:31TO-15 Styrene µg/m3 0.124
485 07/17/2023 20:08TO-15 Tetrachloroethene µg/m3 3.62
J0.660 07/18/2023 23:31TO-15 Tetrahydrofuran µg/m3 0.107
222 07/17/2023 20:08TO-15 Toluene µg/m3 1.80
J0.840 07/18/2023 23:31TO-15 1,1,1-Trichloroethane µg/m3 0.144
4.60 07/18/2023 23:31TO-15 Trichlorofluoromethane µg/m3 0.130
27.9 07/18/2023 23:31TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
8.27 07/18/2023 23:31TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
37.1 07/18/2023 23:31TO-15 o-Xylene µg/m3 0.157
101 07/18/2023 23:31TO-15 m,p-Xylene µg/m3 0.217
138 07/18/2023 23:31TO-15 Xylene (Total)µg/m3 0.157
Page 10 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-2
89804 Matrix:
7/13/2023 11:11
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00
84.2 µg/m3 0.202 4.75Acetone 1 07/18/23 16:56 V35511ENM
14.9 µg/m3 0.073 1.60
Benzene 1 07/18/23 16:56 V35511ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 07/18/23 16:56 V35511ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 07/18/23 16:56 V35511ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 07/18/23 16:56 V35511ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 07/18/23 16:56 V35511ENM
1.96 µg/m3 0.328 1.111,3-Butadiene 1 07/18/23 16:56 V35511ENM
32.5 µg/m3 0.060 6.23Carbon Disulfide 1 07/18/23 16:56 V35511ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 07/18/23 16:56 V35511ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 07/18/23 16:56 V35511ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 07/18/23 16:56 V35511ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 07/18/23 16:56 V35511ENM
44.5 µg/m3 0.086 2.44Chloroform 1 07/18/23 16:56 V35511ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 07/18/23 16:56 V35511ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 07/18/23 16:56 V35511ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 07/18/23 16:56 V35511ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 07/18/23 16:56 V35511ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 07/18/23 16:56 V35511ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 07/18/23 16:56 V35511ENM
4.39 µg/m3 0.134 2.47Dichlorodifluoromethane 1 07/18/23 16:56 V35511ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 07/18/23 16:56 V35511ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 07/18/23 16:56 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-2
89804 Matrix:
7/13/2023 11:11
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 07/18/23 16:56 V35511ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 07/18/23 16:56 V35511ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 07/18/23 16:56 V35511ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 07/18/23 16:56 V35511ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 07/18/23 16:56 V35511ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 07/18/23 16:56 V35511ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 07/18/23 16:56 V35511ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 07/18/23 16:56 V35511ENM
0.526 J
µg/m3 0.136 1.80
Ethyl Acetate 1 07/18/23 16:56 V35511ENM
21.2 µg/m3 0.106 2.17Ethylbenzene 1 07/18/23 16:56 V35511ENM
7.33 µg/m3 0.128 2.464-Ethyltoluene 1 07/18/23 16:56 V35511ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 07/18/23 16:56 V35511ENM
16.4 µg/m3 0.143 2.05Heptane 1 07/18/23 16:56 V35511ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 07/18/23 16:56 V35511ENM
5.03 µg/m3 0.047 1.76n-Hexane 1 07/18/23 16:56 V35511ENM
3.33 µg/m3 0.285 2.052-Hexanone 1 07/18/23 16:56 V35511ENM
1.76 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 07/18/23 16:56 V35511ENM
17.6 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 07/18/23 16:56 V35511ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 07/18/23 16:56 V35511ENM
3.59 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 07/18/23 16:56 V35511ENM
22.3 µg/m3 0.488 1.74Methylene Chloride 1 07/18/23 16:56 V35511ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 07/18/23 16:56 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-2
89804 Matrix:
7/13/2023 11:11
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00
20.3 µg/m3 0.242 0.860Propene 1 07/18/23 16:56 V35511ENM
4.31 µg/m3 0.124 2.13
Styrene 1 07/18/23 16:56 V35511ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 07/18/23 16:56 V35511ENM
234 µg/m3 0.181 3.39Tetrachloroethene 1 07/18/23 16:56 V35511ENM
0.852 J µg/m3 0.107 1.47Tetrahydrofuran 1 07/18/23 16:56 V35511ENM
118 µg/m3 0.090 1.88Toluene 1 07/18/23 16:56 V35511ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 07/18/23 16:56 V35511ENM
1.21 J µg/m3 0.144 2.731,1,1-Trichloroethane 1 07/18/23 16:56 V35511ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 07/18/23 16:56 V35511ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 07/18/23 16:56 V35511ENM
7.88 µg/m3 0.130 2.81Trichlorofluoromethane 1 07/18/23 16:56 V35511ENM
25.8 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 07/18/23 16:56 V35511ENM
6.64 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 07/18/23 16:56 V35511ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 07/18/23 16:56 V35511ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 07/18/23 16:56 V35511ENM
25.4 µg/m3 0.157 2.17o-Xylene 1 07/18/23 16:56 V35511ENM
63.9 µg/m3 0.217 5.65m,p-Xylene 1 07/18/23 16:56 V35511ENM
89.3 µg/m3 0.157 2.17Xylene (Total)1 07/18/23 16:56 V35511
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%07/18/23 16:561 ENM V35511
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-DUP
89805 Matrix:
7/13/2023 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00
77.3 µg/m3 0.202 4.75Acetone 1 07/18/23 17:50 V35511ENM
15.1 µg/m3 0.073 1.60
Benzene 1 07/18/23 17:50 V35511ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 07/18/23 17:50 V35511ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 07/18/23 17:50 V35511ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 07/18/23 17:50 V35511ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 07/18/23 17:50 V35511ENM
6.59 µg/m3 0.328 1.111,3-Butadiene 1 07/18/23 17:50 V35511ENM
31.5 µg/m3 0.060 6.23Carbon Disulfide 1 07/18/23 17:50 V35511ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 07/18/23 17:50 V35511ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 07/18/23 17:50 V35511ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 07/18/23 17:50 V35511ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 07/18/23 17:50 V35511ENM
42.8 µg/m3 0.086 2.44Chloroform 1 07/18/23 17:50 V35511ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 07/18/23 17:50 V35511ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 07/18/23 17:50 V35511ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 07/18/23 17:50 V35511ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 07/18/23 17:50 V35511ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 07/18/23 17:50 V35511ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 07/18/23 17:50 V35511ENM
4.39 µg/m3 0.134 2.47Dichlorodifluoromethane 1 07/18/23 17:50 V35511ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 07/18/23 17:50 V35511ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 07/18/23 17:50 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-DUP
89805 Matrix:
7/13/2023 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 07/18/23 17:50 V35511ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 07/18/23 17:50 V35511ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 07/18/23 17:50 V35511ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 07/18/23 17:50 V35511ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 07/18/23 17:50 V35511ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 07/18/23 17:50 V35511ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 07/18/23 17:50 V35511ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 07/18/23 17:50 V35511ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 07/18/23 17:50 V35511ENM
20.6 µg/m3 0.106 2.17Ethylbenzene 1 07/18/23 17:50 V35511ENM
6.92 µg/m3 0.128 2.464-Ethyltoluene 1 07/18/23 17:50 V35511ENM
0.743 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 07/18/23 17:50 V35511ENM
16.8 µg/m3 0.143 2.05Heptane 1 07/18/23 17:50 V35511ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 07/18/23 17:50 V35511ENM
4.53 µg/m3 0.047 1.76n-Hexane 1 07/18/23 17:50 V35511ENM
3.24 µg/m3 0.285 2.052-Hexanone 1 07/18/23 17:50 V35511ENM
1.32 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 07/18/23 17:50 V35511ENM
17.2 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 07/18/23 17:50 V35511ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 07/18/23 17:50 V35511ENM
3.83 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 07/18/23 17:50 V35511ENM
21.2 µg/m3 0.488 1.74Methylene Chloride 1 07/18/23 17:50 V35511ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 07/18/23 17:50 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-DUP
89805 Matrix:
7/13/2023 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00
19.7 µg/m3 0.242 0.860Propene 1 07/18/23 17:50 V35511ENM
<0.124 µg/m3 0.124 2.13
Styrene 1 07/18/23 17:50 V35511ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 07/18/23 17:50 V35511ENM
222 µg/m3 0.181 3.39Tetrachloroethene 1 07/18/23 17:50 V35511ENM
1.28 J µg/m3 0.107 1.47Tetrahydrofuran 1 07/18/23 17:50 V35511ENM
113 µg/m3 0.090 1.88Toluene 1 07/18/23 17:50 V35511ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 07/18/23 17:50 V35511ENM
1.11 J µg/m3 0.144 2.731,1,1-Trichloroethane 1 07/18/23 17:50 V35511ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 07/18/23 17:50 V35511ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 07/18/23 17:50 V35511ENM
8.15 µg/m3 0.130 2.81Trichlorofluoromethane 1 07/18/23 17:50 V35511ENM
25.0 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 07/18/23 17:50 V35511ENM
6.35 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 07/18/23 17:50 V35511ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 07/18/23 17:50 V35511ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 07/18/23 17:50 V35511ENM
24.8 µg/m3 0.157 2.17o-Xylene 1 07/18/23 17:50 V35511ENM
61.9 µg/m3 0.217 5.65m,p-Xylene 1 07/18/23 17:50 V35511ENM
86.7 µg/m3 0.157 2.17Xylene (Total)1 07/18/23 17:50 V35511
Surrogate: 4-Bromofluorobenzene 99.7 Limits: 70-130%07/18/23 17:501 ENM V35511
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-7
89806 Matrix:
7/12/2023 15:35
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
59.0 µg/m3 0.202 4.75Acetone 1 07/18/23 18:49 V35511ENM
2.92 µg/m3 0.073 1.60
Benzene 1 07/18/23 18:49 V35511ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 07/18/23 18:49 V35511ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 07/18/23 18:49 V35511ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 07/18/23 18:49 V35511ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 07/18/23 18:49 V35511ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 07/18/23 18:49 V35511ENM
6.29 µg/m3 0.060 6.23Carbon Disulfide 1 07/18/23 18:49 V35511ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 07/18/23 18:49 V35511ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 07/18/23 18:49 V35511ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 07/18/23 18:49 V35511ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 07/18/23 18:49 V35511ENM
0.434 J µg/m3 0.086 2.44Chloroform 1 07/18/23 18:49 V35511ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 07/18/23 18:49 V35511ENM
8.12 µg/m3 0.161 3.44Cyclohexane 1 07/18/23 18:49 V35511ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 07/18/23 18:49 V35511ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 07/18/23 18:49 V35511ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 07/18/23 18:49 V35511ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 07/18/23 18:49 V35511ENM
1.22 J µg/m3 0.134 2.47Dichlorodifluoromethane 1 07/18/23 18:49 V35511ENM
1.31 J µg/m3 0.101 2.021,1-Dichloroethane 1 07/18/23 18:49 V35511ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 07/18/23 18:49 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-7
89806 Matrix:
7/12/2023 15:35
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 07/18/23 18:49 V35511ENM
0.535 J
µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 07/18/23 18:49 V35511ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 07/18/23 18:49 V35511ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 07/18/23 18:49 V35511ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 07/18/23 18:49 V35511ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 07/18/23 18:49 V35511ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 07/18/23 18:49 V35511ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 07/18/23 18:49 V35511ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 07/18/23 18:49 V35511ENM
1.02 J µg/m3 0.106 2.17Ethylbenzene 1 07/18/23 18:49 V35511ENM
<0.128 µg/m3 0.128 2.464-Ethyltoluene 1 07/18/23 18:49 V35511ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 07/18/23 18:49 V35511ENM
10.3 µg/m3 0.143 2.05Heptane 1 07/18/23 18:49 V35511ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 07/18/23 18:49 V35511ENM
13.1 µg/m3 0.047 1.76n-Hexane 1 07/18/23 18:49 V35511ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 07/18/23 18:49 V35511ENM
5.92 µg/m3 0.139 4.92Isopropyl Alcohol 1 07/18/23 18:49 V35511ENM
14.0 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 07/18/23 18:49 V35511ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 07/18/23 18:49 V35511ENM
1.14 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 07/18/23 18:49 V35511ENM
<0.488 µg/m3 0.488 1.74Methylene Chloride 1 07/18/23 18:49 V35511ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 07/18/23 18:49 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-7
89806 Matrix:
7/12/2023 15:35
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
92.6 µg/m3 4.84 17.2Propene 20 07/17/23 17:04 V35576ENM
4.16 µg/m3 0.124 2.13
Styrene 1 07/18/23 18:49 V35511ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 07/18/23 18:49 V35511ENM
12.6 µg/m3 0.181 3.39Tetrachloroethene 1 07/18/23 18:49 V35511ENM
6.39 µg/m3 0.107 1.47Tetrahydrofuran 1 07/18/23 18:49 V35511ENM
12.5 µg/m3 0.090 1.88Toluene 1 07/18/23 18:49 V35511ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 07/18/23 18:49 V35511ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 07/18/23 18:49 V35511ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 07/18/23 18:49 V35511ENM
2.00 J µg/m3 0.199 2.15Trichloroethene 1 07/18/23 18:49 V35511ENM
1.50 J µg/m3 0.130 2.81Trichlorofluoromethane 1 07/18/23 18:49 V35511ENM
<0.110 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 07/18/23 18:49 V35511ENM
<0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 07/18/23 18:49 V35511ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 07/18/23 18:49 V35511ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 07/18/23 18:49 V35511ENM
4.49 µg/m3 0.157 2.17o-Xylene 1 07/18/23 18:49 V35511ENM
5.47 J µg/m3 0.217 5.65m,p-Xylene 1 07/18/23 18:49 V35511ENM
9.96 J µg/m3 0.157 2.17Xylene (Total)1 07/18/23 18:49 V35511
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%07/18/23 18:491 ENM V35511
Surrogate: 4-Bromofluorobenzene 94.1 Limits: 70-130%07/17/23 17:0420 ENM V35576
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-6
89807 Matrix:
7/12/2023 16:49
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
357 µg/m3 4.04 95.0Acetone 20 07/17/23 17:41 V35576ENM
21.0 µg/m3 0.073 1.60
Benzene 1 07/18/23 19:45 V35511ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 07/18/23 19:45 V35511ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 07/18/23 19:45 V35511ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 07/18/23 19:45 V35511ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 07/18/23 19:45 V35511ENM
29.6 µg/m3 0.328 1.111,3-Butadiene 1 07/18/23 19:45 V35511ENM
70.9 µg/m3 0.060 6.23Carbon Disulfide 1 07/18/23 19:45 V35511ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 07/18/23 19:45 V35511ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 07/18/23 19:45 V35511ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 07/18/23 19:45 V35511ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 07/18/23 19:45 V35511ENM
0.497 J µg/m3 0.086 2.44Chloroform 1 07/18/23 19:45 V35511ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 07/18/23 19:45 V35511ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 07/18/23 19:45 V35511ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 07/18/23 19:45 V35511ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 07/18/23 19:45 V35511ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 07/18/23 19:45 V35511ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 07/18/23 19:45 V35511ENM
3.53 µg/m3 0.134 2.47Dichlorodifluoromethane 1 07/18/23 19:45 V35511ENM
11.7 µg/m3 0.101 2.021,1-Dichloroethane 1 07/18/23 19:45 V35511ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 07/18/23 19:45 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-6
89807 Matrix:
7/12/2023 16:49
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 07/18/23 19:45 V35511ENM
2.28 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 07/18/23 19:45 V35511ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 07/18/23 19:45 V35511ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 07/18/23 19:45 V35511ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 07/18/23 19:45 V35511ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 07/18/23 19:45 V35511ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 07/18/23 19:45 V35511ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 07/18/23 19:45 V35511ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 07/18/23 19:45 V35511ENM
14.1 µg/m3 0.106 2.17Ethylbenzene 1 07/18/23 19:45 V35511ENM
5.48 µg/m3 0.128 2.464-Ethyltoluene 1 07/18/23 19:45 V35511ENM
0.796 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 07/18/23 19:45 V35511ENM
36.7 µg/m3 0.143 2.05Heptane 1 07/18/23 19:45 V35511ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 07/18/23 19:45 V35511ENM
19.1 µg/m3 0.047 1.76n-Hexane 1 07/18/23 19:45 V35511ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 07/18/23 19:45 V35511ENM
6.54 µg/m3 0.139 4.92Isopropyl Alcohol 1 07/18/23 19:45 V35511ENM
58.2 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 07/18/23 19:45 V35511ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 07/18/23 19:45 V35511ENM
1.98 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 07/18/23 19:45 V35511ENM
0.958 J µg/m3 0.488 1.74Methylene Chloride 1 07/18/23 19:45 V35511ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 07/18/23 19:45 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-6
89807 Matrix:
7/12/2023 16:49
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
424 µg/m3 4.84 17.2Propene 20 07/17/23 17:41 V35576ENM
4.19 µg/m3 0.124 2.13
Styrene 1 07/18/23 19:45 V35511ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 07/18/23 19:45 V35511ENM
181 µg/m3 0.181 3.39Tetrachloroethene 1 07/18/23 19:45 V35511ENM
3.44 µg/m3 0.107 1.47Tetrahydrofuran 1 07/18/23 19:45 V35511ENM
71.2 µg/m3 0.090 1.88Toluene 1 07/18/23 19:45 V35511ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 07/18/23 19:45 V35511ENM
0.878 J µg/m3 0.144 2.731,1,1-Trichloroethane 1 07/18/23 19:45 V35511ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 07/18/23 19:45 V35511ENM
2.59 µg/m3 0.199 2.15Trichloroethene 1 07/18/23 19:45 V35511ENM
3.19 µg/m3 0.130 2.81Trichlorofluoromethane 1 07/18/23 19:45 V35511ENM
21.4 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 07/18/23 19:45 V35511ENM
4.94 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 07/18/23 19:45 V35511ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 07/18/23 19:45 V35511ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 07/18/23 19:45 V35511ENM
20.6 µg/m3 0.157 2.17o-Xylene 1 07/18/23 19:45 V35511ENM
43.4 µg/m3 0.217 5.65m,p-Xylene 1 07/18/23 19:45 V35511ENM
64.0 µg/m3 0.157 2.17Xylene (Total)1 07/18/23 19:45 V35511
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%07/18/23 19:451 ENM V35511
Surrogate: 4-Bromofluorobenzene 92.5 Limits: 70-130%07/17/23 17:4120 ENM V35576
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-5
89808 Matrix:
7/13/2023 10:25
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
47.3 µg/m3 0.202 4.75Acetone 1 07/18/23 20:41 V35511ENM
15.0 µg/m3 0.073 1.60
Benzene 1 07/18/23 20:41 V35511ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 07/18/23 20:41 V35511ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 07/18/23 20:41 V35511ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 07/18/23 20:41 V35511ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 07/18/23 20:41 V35511ENM
24.2 µg/m3 0.328 1.111,3-Butadiene 1 07/18/23 20:41 V35511ENM
46.4 µg/m3 0.060 6.23Carbon Disulfide 1 07/18/23 20:41 V35511ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 07/18/23 20:41 V35511ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 07/18/23 20:41 V35511ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 07/18/23 20:41 V35511ENM
0.303 J µg/m3 0.164 1.32Chloroethane 1 07/18/23 20:41 V35511ENM
0.463 J µg/m3 0.086 2.44Chloroform 1 07/18/23 20:41 V35511ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 07/18/23 20:41 V35511ENM
13.0 µg/m3 0.161 3.44Cyclohexane 1 07/18/23 20:41 V35511ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 07/18/23 20:41 V35511ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 07/18/23 20:41 V35511ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 07/18/23 20:41 V35511ENM
1.50 J µg/m3 0.186 3.011,4-Dichlorobenzene 1 07/18/23 20:41 V35511ENM
4.22 µg/m3 0.134 2.47Dichlorodifluoromethane 1 07/18/23 20:41 V35511ENM
1.53 J µg/m3 0.101 2.021,1-Dichloroethane 1 07/18/23 20:41 V35511ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 07/18/23 20:41 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-5
89808 Matrix:
7/13/2023 10:25
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 07/18/23 20:41 V35511ENM
5.54 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 07/18/23 20:41 V35511ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 07/18/23 20:41 V35511ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 07/18/23 20:41 V35511ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 07/18/23 20:41 V35511ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 07/18/23 20:41 V35511ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 07/18/23 20:41 V35511ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 07/18/23 20:41 V35511ENM
1.79 J
µg/m3 0.136 1.80
Ethyl Acetate 1 07/18/23 20:41 V35511ENM
5.35 µg/m3 0.106 2.17Ethylbenzene 1 07/18/23 20:41 V35511ENM
1.37 J µg/m3 0.128 2.464-Ethyltoluene 1 07/18/23 20:41 V35511ENM
0.620 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 07/18/23 20:41 V35511ENM
35.1 µg/m3 0.143 2.05Heptane 1 07/18/23 20:41 V35511ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 07/18/23 20:41 V35511ENM
22.6 µg/m3 0.047 1.76n-Hexane 1 07/18/23 20:41 V35511ENM
21.5 µg/m3 0.285 2.052-Hexanone 1 07/18/23 20:41 V35511ENM
5.50 µg/m3 0.139 4.92Isopropyl Alcohol 1 07/18/23 20:41 V35511ENM
7.53 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 07/18/23 20:41 V35511ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 07/18/23 20:41 V35511ENM
2.32 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 07/18/23 20:41 V35511ENM
1.79 µg/m3 0.488 1.74Methylene Chloride 1 07/18/23 20:41 V35511ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 07/18/23 20:41 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-5
89808 Matrix:
7/13/2023 10:25
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
514 µg/m3 4.84 17.2Propene 20 07/17/23 18:18 V35576ENM
4.17 µg/m3 0.124 2.13
Styrene 1 07/18/23 20:41 V35511ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 07/18/23 20:41 V35511ENM
77.5 µg/m3 0.181 3.39Tetrachloroethene 1 07/18/23 20:41 V35511ENM
15.1 µg/m3 0.107 1.47Tetrahydrofuran 1 07/18/23 20:41 V35511ENM
42.3 µg/m3 0.090 1.88Toluene 1 07/18/23 20:41 V35511ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 07/18/23 20:41 V35511ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 07/18/23 20:41 V35511ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 07/18/23 20:41 V35511ENM
15.7 µg/m3 0.199 2.15Trichloroethene 1 07/18/23 20:41 V35511ENM
5.56 µg/m3 0.130 2.81Trichlorofluoromethane 1 07/18/23 20:41 V35511ENM
6.44 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 07/18/23 20:41 V35511ENM
2.22 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 07/18/23 20:41 V35511ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 07/18/23 20:41 V35511ENM
3.68 µg/m3 0.127 1.28Vinyl Chloride 1 07/18/23 20:41 V35511ENM
7.23 µg/m3 0.157 2.17o-Xylene 1 07/18/23 20:41 V35511ENM
17.1 µg/m3 0.217 5.65m,p-Xylene 1 07/18/23 20:41 V35511ENM
24.3 µg/m3 0.157 2.17Xylene (Total)1 07/18/23 20:41 V35511
Surrogate: 4-Bromofluorobenzene 98.9 Limits: 70-130%07/18/23 20:411 ENM V35511
Surrogate: 4-Bromofluorobenzene 90.8 Limits: 70-130%07/17/23 18:1820 ENM V35576
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-1
89809 Matrix:
7/12/2023 14:58
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00
33.1 µg/m3 0.202 4.75Acetone 1 07/18/23 21:39 V35511ENM
4.36 µg/m3 0.073 1.60
Benzene 1 07/18/23 21:39 V35511ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 07/18/23 21:39 V35511ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 07/18/23 21:39 V35511ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 07/18/23 21:39 V35511ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 07/18/23 21:39 V35511ENM
1.44 µg/m3 0.328 1.111,3-Butadiene 1 07/18/23 21:39 V35511ENM
18.1 µg/m3 0.060 6.23Carbon Disulfide 1 07/18/23 21:39 V35511ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 07/18/23 21:39 V35511ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 07/18/23 21:39 V35511ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 07/18/23 21:39 V35511ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 07/18/23 21:39 V35511ENM
33.7 µg/m3 0.086 2.44Chloroform 1 07/18/23 21:39 V35511ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 07/18/23 21:39 V35511ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 07/18/23 21:39 V35511ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 07/18/23 21:39 V35511ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 07/18/23 21:39 V35511ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 07/18/23 21:39 V35511ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 07/18/23 21:39 V35511ENM
3.35 µg/m3 0.134 2.47Dichlorodifluoromethane 1 07/18/23 21:39 V35511ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 07/18/23 21:39 V35511ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 07/18/23 21:39 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-1
89809 Matrix:
7/12/2023 14:58
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 07/18/23 21:39 V35511ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 07/18/23 21:39 V35511ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 07/18/23 21:39 V35511ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 07/18/23 21:39 V35511ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 07/18/23 21:39 V35511ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 07/18/23 21:39 V35511ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 07/18/23 21:39 V35511ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 07/18/23 21:39 V35511ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 07/18/23 21:39 V35511ENM
6.40 µg/m3 0.106 2.17Ethylbenzene 1 07/18/23 21:39 V35511ENM
1.72 J µg/m3 0.128 2.464-Ethyltoluene 1 07/18/23 21:39 V35511ENM
0.582 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 07/18/23 21:39 V35511ENM
13.0 µg/m3 0.143 2.05Heptane 1 07/18/23 21:39 V35511ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 07/18/23 21:39 V35511ENM
10.0 µg/m3 0.047 1.76n-Hexane 1 07/18/23 21:39 V35511ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 07/18/23 21:39 V35511ENM
2.15 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 07/18/23 21:39 V35511ENM
6.66 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 07/18/23 21:39 V35511ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 07/18/23 21:39 V35511ENM
3.05 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 07/18/23 21:39 V35511ENM
0.753 J µg/m3 0.488 1.74Methylene Chloride 1 07/18/23 21:39 V35511ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 07/18/23 21:39 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-1
89809 Matrix:
7/12/2023 14:58
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00
13.7 µg/m3 0.242 0.860Propene 1 07/18/23 21:39 V35511ENM
3.95 µg/m3 0.124 2.13
Styrene 1 07/18/23 21:39 V35511ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 07/18/23 21:39 V35511ENM
54.1 µg/m3 0.181 3.39Tetrachloroethene 1 07/18/23 21:39 V35511ENM
0.757 J µg/m3 0.107 1.47Tetrahydrofuran 1 07/18/23 21:39 V35511ENM
26.6 µg/m3 0.090 1.88Toluene 1 07/18/23 21:39 V35511ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 07/18/23 21:39 V35511ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 07/18/23 21:39 V35511ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 07/18/23 21:39 V35511ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 07/18/23 21:39 V35511ENM
3.06 µg/m3 0.130 2.81Trichlorofluoromethane 1 07/18/23 21:39 V35511ENM
5.57 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 07/18/23 21:39 V35511ENM
1.43 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 07/18/23 21:39 V35511ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 07/18/23 21:39 V35511ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 07/18/23 21:39 V35511ENM
6.74 µg/m3 0.157 2.17o-Xylene 1 07/18/23 21:39 V35511ENM
22.8 µg/m3 0.217 5.65m,p-Xylene 1 07/18/23 21:39 V35511ENM
29.5 µg/m3 0.157 2.17Xylene (Total)1 07/18/23 21:39 V35511
Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%07/18/23 21:391 ENM V35511
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-4
89810 Matrix:
7/13/2023 13:05
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
40.7 µg/m3 0.202 4.75Acetone 1 07/18/23 22:34 V35511ENM
16.7 µg/m3 0.073 1.60
Benzene 1 07/18/23 22:34 V35511ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 07/18/23 22:34 V35511ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 07/18/23 22:34 V35511ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 07/18/23 22:34 V35511ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 07/18/23 22:34 V35511ENM
14.3 µg/m3 0.328 1.111,3-Butadiene 1 07/18/23 22:34 V35511ENM
42.9 µg/m3 0.060 6.23Carbon Disulfide 1 07/18/23 22:34 V35511ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 07/18/23 22:34 V35511ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 07/18/23 22:34 V35511ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 07/18/23 22:34 V35511ENM
1.20 J µg/m3 0.164 1.32Chloroethane 1 07/18/23 22:34 V35511ENM
0.761 J µg/m3 0.086 2.44Chloroform 1 07/18/23 22:34 V35511ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 07/18/23 22:34 V35511ENM
8.95 µg/m3 0.161 3.44Cyclohexane 1 07/18/23 22:34 V35511ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 07/18/23 22:34 V35511ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 07/18/23 22:34 V35511ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 07/18/23 22:34 V35511ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 07/18/23 22:34 V35511ENM
3.48 µg/m3 0.134 2.47Dichlorodifluoromethane 1 07/18/23 22:34 V35511ENM
28.6 µg/m3 0.101 2.021,1-Dichloroethane 1 07/18/23 22:34 V35511ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 07/18/23 22:34 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-4
89810 Matrix:
7/13/2023 13:05
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 07/18/23 22:34 V35511ENM
27.5 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 07/18/23 22:34 V35511ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 07/18/23 22:34 V35511ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 07/18/23 22:34 V35511ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 07/18/23 22:34 V35511ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 07/18/23 22:34 V35511ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 07/18/23 22:34 V35511ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 07/18/23 22:34 V35511ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 07/18/23 22:34 V35511ENM
2.27 µg/m3 0.106 2.17Ethylbenzene 1 07/18/23 22:34 V35511ENM
0.737 J µg/m3 0.128 2.464-Ethyltoluene 1 07/18/23 22:34 V35511ENM
0.712 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 07/18/23 22:34 V35511ENM
21.4 µg/m3 0.143 2.05Heptane 1 07/18/23 22:34 V35511ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 07/18/23 22:34 V35511ENM
37.9 µg/m3 0.047 1.76n-Hexane 1 07/18/23 22:34 V35511ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 07/18/23 22:34 V35511ENM
3.86 J µg/m3 0.139 4.92Isopropyl Alcohol 1 07/18/23 22:34 V35511ENM
10.0 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 07/18/23 22:34 V35511ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 07/18/23 22:34 V35511ENM
2.55 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 07/18/23 22:34 V35511ENM
1.18 J µg/m3 0.488 1.74Methylene Chloride 1 07/18/23 22:34 V35511ENM
7.11 µg/m3 0.183 2.62Naphthalene 1 07/18/23 22:34 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-4
89810 Matrix:
7/13/2023 13:05
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
294 µg/m3 4.84 17.2Propene 20 07/17/23 19:31 V35576ENM
4.36 µg/m3 0.124 2.13
Styrene 1 07/18/23 22:34 V35511ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 07/18/23 22:34 V35511ENM
22.5 µg/m3 0.181 3.39Tetrachloroethene 1 07/18/23 22:34 V35511ENM
6.65 µg/m3 0.107 1.47Tetrahydrofuran 1 07/18/23 22:34 V35511ENM
15.7 µg/m3 0.090 1.88Toluene 1 07/18/23 22:34 V35511ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 07/18/23 22:34 V35511ENM
2.67 J µg/m3 0.144 2.731,1,1-Trichloroethane 1 07/18/23 22:34 V35511ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 07/18/23 22:34 V35511ENM
24.7 µg/m3 0.199 2.15Trichloroethene 1 07/18/23 22:34 V35511ENM
3.51 µg/m3 0.130 2.81Trichlorofluoromethane 1 07/18/23 22:34 V35511ENM
3.34 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 07/18/23 22:34 V35511ENM
0.963 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 07/18/23 22:34 V35511ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 07/18/23 22:34 V35511ENM
5.47 µg/m3 0.127 1.28Vinyl Chloride 1 07/18/23 22:34 V35511ENM
2.49 µg/m3 0.157 2.17o-Xylene 1 07/18/23 22:34 V35511ENM
8.49 µg/m3 0.217 5.65m,p-Xylene 1 07/18/23 22:34 V35511ENM
11.0 µg/m3 0.157 2.17Xylene (Total)1 07/18/23 22:34 V35511
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/18/23 22:341 ENM V35511
Surrogate: 4-Bromofluorobenzene 96.1 Limits: 70-130%07/17/23 19:3120 ENM V35576
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-3
89811 Matrix:
7/13/2023 11:52
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
28.4 µg/m3 0.202 4.75Acetone 1 07/18/23 23:31 V35511ENM
35.0 µg/m3 0.073 1.60
Benzene 1 07/18/23 23:31 V35511ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 07/18/23 23:31 V35511ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 07/18/23 23:31 V35511ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 07/18/23 23:31 V35511ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 07/18/23 23:31 V35511ENM
22.8 µg/m3 0.328 1.111,3-Butadiene 1 07/18/23 23:31 V35511ENM
176 µg/m3 1.22 125Carbon Disulfide 20 07/17/23 20:08 V35576ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 07/18/23 23:31 V35511ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 07/18/23 23:31 V35511ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 07/18/23 23:31 V35511ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 07/18/23 23:31 V35511ENM
16.0 µg/m3 0.086 2.44Chloroform 1 07/18/23 23:31 V35511ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 07/18/23 23:31 V35511ENM
10.3 µg/m3 0.161 3.44Cyclohexane 1 07/18/23 23:31 V35511ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 07/18/23 23:31 V35511ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 07/18/23 23:31 V35511ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 07/18/23 23:31 V35511ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 07/18/23 23:31 V35511ENM
3.62 µg/m3 0.134 2.47Dichlorodifluoromethane 1 07/18/23 23:31 V35511ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 07/18/23 23:31 V35511ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 07/18/23 23:31 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 32 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-3
89811 Matrix:
7/13/2023 11:52
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 07/18/23 23:31 V35511ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 07/18/23 23:31 V35511ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 07/18/23 23:31 V35511ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 07/18/23 23:31 V35511ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 07/18/23 23:31 V35511ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 07/18/23 23:31 V35511ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 07/18/23 23:31 V35511ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 07/18/23 23:31 V35511ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 07/18/23 23:31 V35511ENM
35.5 µg/m3 0.106 2.17Ethylbenzene 1 07/18/23 23:31 V35511ENM
8.37 µg/m3 0.128 2.464-Ethyltoluene 1 07/18/23 23:31 V35511ENM
0.881 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 07/18/23 23:31 V35511ENM
155 µg/m3 0.143 2.05Heptane 1 07/18/23 23:31 V35511ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 07/18/23 23:31 V35511ENM
24.8 µg/m3 0.047 1.76n-Hexane 1 07/18/23 23:31 V35511ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 07/18/23 23:31 V35511ENM
2.87 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 07/18/23 23:31 V35511ENM
7.73 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 07/18/23 23:31 V35511ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 07/18/23 23:31 V35511ENM
4.02 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 07/18/23 23:31 V35511ENM
1.61 J µg/m3 0.488 1.74Methylene Chloride 1 07/18/23 23:31 V35511ENM
5.59 µg/m3 0.183 2.62Naphthalene 1 07/18/23 23:31 V35511ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 33 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-198-0006
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
TPI-002 Received : 07/14/2023
Former Abels Auto
Report Date : 07/21/2023
Sample ID :
Lab No :
Sampled:SG-3
89811 Matrix:
7/13/2023 11:52
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V35508 07/18/23 09:00 V35570 07/17/23 09:00
21.3 µg/m3 0.242 0.860Propene 1 07/18/23 23:31 V35511ENM
4.26 µg/m3 0.124 2.13
Styrene 1 07/18/23 23:31 V35511ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 07/18/23 23:31 V35511ENM
485 µg/m3 3.62 67.8Tetrachloroethene 20 07/17/23 20:08 V35576ENM
0.660 J µg/m3 0.107 1.47Tetrahydrofuran 1 07/18/23 23:31 V35511ENM
222 µg/m3 1.80 37.7Toluene 20 07/17/23 20:08 V35576ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 07/18/23 23:31 V35511ENM
0.840 J µg/m3 0.144 2.731,1,1-Trichloroethane 1 07/18/23 23:31 V35511ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 07/18/23 23:31 V35511ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 07/18/23 23:31 V35511ENM
4.60 µg/m3 0.130 2.81Trichlorofluoromethane 1 07/18/23 23:31 V35511ENM
27.9 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 07/18/23 23:31 V35511ENM
8.27 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 07/18/23 23:31 V35511ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 07/18/23 23:31 V35511ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 07/18/23 23:31 V35511ENM
37.1 µg/m3 0.157 2.17o-Xylene 1 07/18/23 23:31 V35511ENM
101 µg/m3 0.217 5.65m,p-Xylene 1 07/18/23 23:31 V35511ENM
138 µg/m3 0.157 2.17Xylene (Total)1 07/18/23 23:31 V35511
Surrogate: 4-Bromofluorobenzene 109 Limits: 70-130%07/18/23 23:311 ENM V35511
Surrogate: 4-Bromofluorobenzene 91.3 Limits: 70-130%07/17/23 20:0820 ENM V35576
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 34 of 43
Quality Control Data
23-198-0006Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Former Abels Auto
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V35511QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V35508
Associated Lab Samples: 89804, 89805, 89806, 89807, 89808, 89809, 89810, 89811
LRB-V35508 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/18/23 12:204.750.2020.337µg/m3Acetone
07/18/23 12:201.600.073<0.073µg/m3Benzene
07/18/23 12:2010.40.147<0.147µg/m3Benzyl Chloride
07/18/23 12:203.350.150<0.150µg/m3Bromodichloromethane
07/18/23 12:205.170.153<0.153µg/m3Bromoform
07/18/23 12:201.940.115<0.115µg/m3Bromomethane
07/18/23 12:201.110.328<0.328µg/m31,3-Butadiene
07/18/23 12:206.230.0600.554µg/m3Carbon Disulfide
07/18/23 12:203.150.155<0.155µg/m3Carbon Tetrachloride
07/18/23 12:202.300.107<0.107µg/m3Chlorobenzene
07/18/23 12:204.260.208<0.208µg/m3Chlorodibromomethane
07/18/23 12:201.320.164<0.164µg/m3Chloroethane
07/18/23 12:202.440.086<0.086µg/m3Chloroform
07/18/23 12:201.030.067<0.067µg/m3Chloromethane
07/18/23 12:203.440.161<0.161µg/m3Cyclohexane
07/18/23 12:203.840.151<0.151µg/m31,2-Dibromoethane
07/18/23 12:203.010.096<0.096µg/m31,2-Dichlorobenzene
07/18/23 12:2012.00.174<0.174µg/m31,3-Dichlorobenzene
07/18/23 12:203.010.186<0.186µg/m31,4-Dichlorobenzene
07/18/23 12:202.470.134<0.134µg/m3Dichlorodifluoromethane
07/18/23 12:202.020.101<0.101µg/m31,1-Dichloroethane
07/18/23 12:202.020.129<0.129µg/m31,2-Dichloroethane
07/18/23 12:201.980.107<0.107µg/m31,1-Dichloroethene
07/18/23 12:201.980.095<0.095µg/m3cis-1,2-Dichloroethene
07/18/23 12:201.980.108<0.108µg/m3trans-1,2-Dichloroethene
07/18/23 12:202.310.205<0.205µg/m31,2-Dichloropropane
07/18/23 12:203.500.622<0.622µg/m31,2-Dichlorotetrafluoroethane
Page 1 of 6Date:07/21/2023 10:14 AM
Page 35 of 43
Quality Control Data
23-198-0006Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Former Abels Auto
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V35511QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V35508
Associated Lab Samples: 89804, 89805, 89806, 89807, 89808, 89809, 89810, 89811
LRB-V35508 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/18/23 12:202.270.178<0.178µg/m3cis-1,3-Dichloropropene
07/18/23 12:202.270.178<0.178µg/m3trans-1,3-Dichloropropene
07/18/23 12:201.800.435<0.435µg/m31,4-Dioxane
07/18/23 12:201.800.136<0.136µg/m3Ethyl Acetate
07/18/23 12:202.170.106<0.106µg/m3Ethylbenzene
07/18/23 12:202.460.128<0.128µg/m34-Ethyltoluene
07/18/23 12:203.830.561<0.561µg/m31,1,2-Trichloro-1,2,2-trifluoroethane
07/18/23 12:202.050.143<0.143µg/m3Heptane
07/18/23 12:205.330.330<0.330µg/m3Hexachlorobutadiene
07/18/23 12:201.760.047<0.047µg/m3n-Hexane
07/18/23 12:202.050.285<0.285µg/m32-Hexanone
07/18/23 12:204.920.1390.385µg/m3Isopropyl Alcohol
07/18/23 12:201.470.224<0.224µg/m3Methyl Ethyl Ketone (MEK)
07/18/23 12:201.800.033<0.033µg/m3Methyl tert-butyl ether (MTBE)
07/18/23 12:202.050.121<0.121µg/m34-Methyl-2-Pentanone
07/18/23 12:201.740.488<0.488µg/m3Methylene Chloride
07/18/23 12:202.620.183<0.183µg/m3Naphthalene
07/18/23 12:200.8600.242<0.242µg/m3Propene
07/18/23 12:202.130.124<0.124µg/m3Styrene
07/18/23 12:203.430.104<0.104µg/m31,1,2,2-Tetrachloroethane
07/18/23 12:203.390.1811.10µg/m3Tetrachloroethene
07/18/23 12:201.470.107<0.107µg/m3Tetrahydrofuran
07/18/23 12:201.880.090<0.090µg/m3Toluene
07/18/23 12:203.710.209<0.209µg/m31,2,4-Trichlorobenzene
07/18/23 12:202.730.144<0.144µg/m31,1,1-Trichloroethane
07/18/23 12:202.730.087<0.087µg/m31,1,2-Trichloroethane
07/18/23 12:202.150.199<0.199µg/m3Trichloroethene
Page 2 of 6Date:07/21/2023 10:14 AM
Page 36 of 43
Quality Control Data
23-198-0006Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Former Abels Auto
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V35511QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V35508
Associated Lab Samples: 89804, 89805, 89806, 89807, 89808, 89809, 89810, 89811
LRB-V35508 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/18/23 12:202.810.130<0.130µg/m3Trichlorofluoromethane
07/18/23 12:202.460.110<0.110µg/m31,2,4-Trimethylbenzene
07/18/23 12:202.460.236<0.236µg/m31,3,5-Trimethylbenzene
07/18/23 12:201.760.224<0.224µg/m3Vinyl Acetate
07/18/23 12:201.280.127<0.127µg/m3Vinyl Chloride
07/18/23 12:202.170.157<0.157µg/m3o-Xylene
07/18/23 12:205.650.217<0.217µg/m3m,p-Xylene
07/18/23 12:204-Bromofluorobenzene (S)91.3 70-130
LCS-V35508Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10312.211.9µg/m3Acetone 70-130
10016.016.0µg/m3Benzene 70-130
10727.625.9µg/m3Benzyl Chloride 70-130
10234.333.5µg/m3Bromodichloromethane 70-130
10554.451.7µg/m3Bromoform 70-130
11622.619.4µg/m3Bromomethane 70-130
10011.111.1µg/m31,3-Butadiene 70-130
11217.415.6µg/m3Carbon Disulfide 70-130
10332.531.5µg/m3Carbon Tetrachloride 70-130
10925.023.0µg/m3Chlorobenzene 70-130
11147.442.6µg/m3Chlorodibromomethane 70-130
10814.213.2µg/m3Chloroethane 70-130
10425.324.4µg/m3Chloroform 70-130
10911.210.3µg/m3Chloromethane 70-130
95.916.517.2µg/m3Cyclohexane 70-130
Page 3 of 6Date:07/21/2023 10:14 AM
Page 37 of 43
Quality Control Data
23-198-0006Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Former Abels Auto
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V35511QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V35508
LCS-V35508Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
11042.238.4µg/m31,2-Dibromoethane 70-130
11835.530.1µg/m31,2-Dichlorobenzene 70-130
12036.130.1µg/m31,3-Dichlorobenzene 70-130
12236.630.1µg/m31,4-Dichlorobenzene 70-130
11327.824.7µg/m3Dichlorodifluoromethane 70-130
10821.920.2µg/m31,1-Dichloroethane 70-130
10120.420.2µg/m31,2-Dichloroethane 70-130
10821.319.8µg/m31,1-Dichloroethene 70-130
10520.719.8µg/m3cis-1,2-Dichloroethene 70-130
10520.719.8µg/m3trans-1,2-Dichloroethene 70-130
96.922.423.1µg/m31,2-Dichloropropane 70-130
11239.335.0µg/m31,2-Dichlorotetrafluoroethane 70-130
98.222.322.7µg/m3cis-1,3-Dichloropropene 70-130
98.222.322.7µg/m3trans-1,3-Dichloropropene 70-130
96.117.318.0µg/m31,4-Dioxane 70-130
93.316.818.0µg/m3Ethyl Acetate 70-130
10122.021.7µg/m3Ethylbenzene 70-130
10225.124.6µg/m34-Ethyltoluene 70-130
11443.838.3µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 70-130
91.718.820.5µg/m3Heptane 70-130
11360.453.3µg/m3Hexachlorobutadiene 70-130
10117.817.6µg/m3n-Hexane 70-130
97.520.020.5µg/m32-Hexanone 70-130
91.011.212.3µg/m3Isopropyl Alcohol 70-130
94.514.014.8µg/m3Methyl Ethyl Ketone (MEK)70-130
97.717.618.0µg/m3Methyl tert-butyl ether (MTBE)70-130
88.218.120.5µg/m34-Methyl-2-Pentanone 70-130
Page 4 of 6Date:07/21/2023 10:14 AM
Page 38 of 43
Quality Control Data
23-198-0006Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Former Abels Auto
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V35511QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V35508
LCS-V35508Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10017.417.4µg/m3Methylene Chloride 70-130
10326.926.2µg/m3Naphthalene 70-130
94.88.178.61µg/m3Propene 70-130
96.220.521.3µg/m3Styrene 70-130
10837.234.3µg/m31,1,2,2-Tetrachloroethane 70-130
10234.633.9µg/m3Tetrachloroethene 70-130
87.012.814.7µg/m3Tetrahydrofuran 70-130
95.718.018.8µg/m3Toluene 70-130
10539.137.1µg/m31,2,4-Trichlorobenzene 70-130
10328.027.3µg/m31,1,1-Trichloroethane 70-130
11130.427.3µg/m31,1,2-Trichloroethane 70-130
10528.226.9µg/m3Trichloroethene 70-130
11431.928.1µg/m3Trichlorofluoromethane 70-130
10626.024.6µg/m31,2,4-Trimethylbenzene 70-130
10726.224.6µg/m31,3,5-Trimethylbenzene 70-130
10117.717.6µg/m3Vinyl Acetate 70-130
10513.412.8µg/m3Vinyl Chloride 70-130
10622.921.7µg/m3o-Xylene 70-130
97.042.143.4µg/m3m,p-Xylene 70-130
99.14-Bromofluorobenzene (S)70-130
Page 5 of 6Date:07/21/2023 10:14 AM
Page 39 of 43
Quality Control Data
23-198-0006Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Former Abels Auto
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V35576QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V35570
Associated Lab Samples: 89806, 89807, 89808, 89810, 89811
LRB-V35570 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/17/23 11:094.750.2020.662µg/m3Acetone
07/17/23 11:096.230.0600.591µg/m3Carbon Disulfide
07/17/23 11:090.8600.242<0.242µg/m3Propene
07/17/23 11:093.390.181<0.181µg/m3Tetrachloroethene
07/17/23 11:091.880.090<0.090µg/m3Toluene
07/17/23 11:094-Bromofluorobenzene (S)91.0 70-130
LCS-V35570Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10412.411.9µg/m3Acetone 70-130
11017.215.6µg/m3Carbon Disulfide 70-130
96.58.318.61µg/m3Propene 70-130
97.633.133.9µg/m3Tetrachloroethene 70-130
92.517.418.8µg/m3Toluene 70-130
97.44-Bromofluorobenzene (S)70-130
Page 6 of 6Date:07/21/2023 10:14 AM
Page 40 of 43
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-198-0006
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:N/A
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:07/17/2023 11:11:57
Special precautions or instructions included?
Comments:
Page 41 of 43
Page 42 of 43
Page 43 of 43

Appendix D

Groundwater and Soil Gas Sampling Forms
6?%%%0DVWHU7HPSODWHV?)RUPV)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI/DVW8SGDWHGJob No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________Depth to Water (ft :___________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIW BBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ftWeather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6&RQG253P9'2PJ/TPI-002Former Ables Auto Charlotte, NC7/14/23740.7325AML2090° F, sunny, light windPumpingstarted at 14:2014:2514:3014:3514:4014:4514:5014:5515:0015:0516.5616.5816.5116.5416.5416.6016.6116.6216.63500 mL1000 mL1500 mL2000 mL2500 mL3500 mL4500 mL5500 mL6500 mL100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min2.462.192.242.001.781.781.751.691.6122.722.522.022.023.022.022.221.922.0256.9255.4253.4254.1253.5252.7250.2249.5247.95.125.235.245.245.245.245.295.265.29215.7211.5211.4210.3209.2208.7205.4205.1205.2156.00144.00107.0045.7029.2020.2014.7011.707.08YSI PP-003, HACH-003AML 7/14/23 16:50VOCs(8260D):x3[HCl], SVOCs(8270E):x2[unpreserved]RCRA Metals(6020B/7470A):x1[HNO3]PeristalticPVC2-inch15:05Waypoint AnalyticalHH-TMW-11025PolyethyleneTOC16.291.26TOCTOCgallons
6?%%%0DVWHU7HPSODWHV?)RUPV)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI/DVW8SGDWHGJob No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________Depth to Water (ft :___________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIW BBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ftWeather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6&RQG253P9'2PJ/TPI-002Former Ables Auto Charlotte, NC7/14/23741.5623AML2090° F, sunny, light windPumpingstarted at 13:0513:1013:1513:2013:2513:3013:3513:4015.6815.8015.8315.8515.8815.8915.90500 mL1000 mL1500 mL2000 mL2500 mL3500 mL4500 mL100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min2.242.172.412.381.971.861.7922.122.022.522.522.522.422.4215.1207.7198.9195.8191.9187.3186.85.505.535.695.655.625.595.58142.0114.5100.497.695.499.293.939.0033.5020.7014.0015.2013.609.83YSI PP-003, HACH-003AML 7/14/23VOCs(8260D):x3[HCl], SVOCs(8270E):x2[unpreserved]RCRA Metals(6020B/7470A):x1[HNO3]PeristalticPVC2-inch13:40Waypoint AnalyticalHH-TMW-2 / GW-DUP823PolyethyleneTOC15.511.22TOCTOCgallons
6?%%%0DVWHU7HPSODWHV?)RUPV)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI/DVW8SGDWHGJob No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________Depth to Water (ft :___________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIW BBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ftWeather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6&RQG253P9'2PJ/TPI-002Former Ables Auto Charlotte, NC7/14/23742.3425AML2090° F, sunny, light windPumpingstarted at 13:0512:1012:1512:2012:2512:3012:3517.3117.3717.4117.4217.4417.44500 mL1000 mL1500 mL2000 mL2500 mL3500 mL100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min4.654.554.665.575.615.5322.022.121.821.921.722.2130.4127.3126.8122.6121.7119.15.295.495.645.515.525.59170.7174.1174.5184.8189.5190.918.1012.7010.509.489.936.96YSI PP-003, HACH-003AML 7/14/23VOCs(8260D):x3[HCl], SVOCs(8270E):x2[unpreserved]RCRA Metals(6020B/7470A):x1[HNO3]PeristalticPVC2-inch12:35Waypoint AnalyticalHH-TMW-31025PolyethyleneTOC17.191.27TOCTOCgallons
6?%%%0DVWHU7HPSODWHV?)RUPV)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI/DVW8SGDWHGJob No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________Depth to Water (ft :___________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIW BBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ftWeather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6&RQG253P9'2PJ/TPI-002Former Ables Auto Charlotte, NC7/14/23742.7525AML2390° F, sunny, light windPumpingstarted at 10:3010:3510:4010:4510:5010:5511:0011:0511:1020.4620.7220.8920.9921.0521.1621.3221.53500 mL1000 mL1500 mL2000 mL2500 mL3500 mL4000 mL4500 mL100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min4.144.536.804.894.783.803.833.9620.620.720.921.221.321.521.421.3424.6364.7349.4342.1334.2329.5324.8329.15.775.695.705.505.765.765.765.7849.466.671.081.768.968.569.565.036.5014.5011.1011.0011.208.257.987.91YSI PP-003, HACH-003AML 7/14/23VOCs(8260D):x3[HCl], SVOCs(8270E):x2[unpreserved]RCRA Metals(6020B/7470A):x1[HNO3]PeristalticPVC2-inch11:10Waypoint AnalyticalHH-TMW-51025PolyethyleneTOC20.190.78TOCTOCgallons
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D/DVWXSGDWHG+J LQFKHVRIPHUFXU\SSP SDUWVSHUPLOOLRQ1RWHVBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB6DPSOH,'7\SH9DSRU0RQLWRULQJ3RLQW&RQVWUXFWLRQ +HOLXP/HDN7HVWEŽƚĞ͗>ĞĂŬdĞƐƚZĞƋƵŝƌĞŵĞŶƚƐWĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ůĞĂŬƚĞƐƚƉĂƐƐĞƐŝĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƉƵƌŐĞĂŝƌŝƐůĞƐƐƚŚĂŶϭϬйŽĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƐŚƌŽƵĚ͘/ OHQJWKRIWXELQJSLSHIWD IRUGLDPHWHU/IWD IRUGLDPHWHU/IW͗ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽdžͰLJKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ/ŶƐƚĂůůĂƚŝŽŶ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WTPI-002 AML90s, sunny, light windSG-15999SG Temp. Conc. 6 Soil 7.5Full7/12/23 145089 Syringe 1 L 10.5 0 ppm Yes14300SG-75992SG Temp. Soil -- -- 7.5Full7/12/23 153090 Syringe 1 L 11.1 0 ppm Yes13140SG-611361SG Temp. Soil -- -- 7.5Full7/12/23 150090 Syringe 1 L 10.5 0 ppm Yes16243SG-55990SG Temp. Soil -- -- 7.5Full7/13/23 101585 Syringe 1 L 10.1 0 ppm Yes13112SG-25919SG Temp. Soil -- -- 7.5Full7/13/23 110087 Syringe 1 L 10.2 0 ppm Yes14320SG-DUP5982SG Temp. Soil -- -- 7.5Full7/13/23 110087 Syringe 1 L 10.2 0 ppm Yes14320
SG-36010SGTemp.SoilFull88 Syringe 1 LYes14325SG-4599516241
TPI-002AML90s, sunny, light wind1.4 L10100 mL/min1503151014581535101540154610171310251.4 L10104611111.4 L101.4 L1111101123
TPI-002AML90s, sunny, light wind1.4 L10100 mL/min11571212115213051013101323

Appendix E

DEQ Risk Calculators
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Site-Wide Hypothetical Worst Case Soil Gas
North Carolina Department of Environmental Quality
Risk Calculator
Former Ables Auto (TPI-002)
2501, 2511, and 2533 Wilkinson Boulevard, Charlotte, NC
Brownfields Redevelopment Section
27027-23-060
July 2023
May 2023 EPA RSL Table
Prepared By:Hart and Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 27027-23-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Soil Gas
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2023Basis: May 2023 EPA RSL TableSite ID: 27027-23-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Soil Gas
Description of Exposure Point Concentration Selection:
Exposure Point Concentration
(ug/m3)
Notes:CAS Number Chemical Minimum Concentration (Qualifier)
Maximum Concentration (Qualifier)Units Location of Maximum Concentration
Detection Frequency
Range of Detection Limits
Concentration Used for Screening
Background Value
Screening Toxicity Value (Screening Level) (n/c)
Potential ARAR/TBC Value
Potential ARAR/TBC Source
COPC Flag (Y/N)
Rationale for Selection or Deletion
357 SG-6 67-64-1 Acetone ug/m3
35 SG-3 71-43-2 Benzene ug/m3
29.6 SG-6 106-99-0 Butadiene, 1,3-ug/m3
176 SG-3 75-15-0 Carbon Disulfide ug/m3
44.5 SG-2 67-66-3 Chloroform ug/m3
13 SG-5 110-82-7 Cyclohexane ug/m3
1.5 SG-5, J 106-46-7 Dichlorobenzene, 1,4-ug/m3
4.39 SG-2/SG-DUP 75-71-8 Dichlorodifluoromethane ug/m3
28.6 SG-4, J 75-34-3 Dichloroethane, 1,1-ug/m3
27.5 SG-4, J 156-59-2 Dichloroethylene, cis-1,2-ug/m3
1.79 SG-5, J 141-78-6 Ethyl Acetate ug/m3
1.2 SG-4, J 75-00-3 Ethyl Chloride (Chloroethane)ug/m3
35.5 SG-3 100-41-4 Ethylbenzene ug/m3
15.1 SG-5 109-99-9 ~Tetrahydrofuran ug/m3
155 SG-3 142-82-5 Heptane, N-ug/m3
37.9 SG-3 110-54-3 Hexane, N-ug/m3
21.5 SG-5 591-78-6 Hexanone, 2-ug/m3
6.54 SG-6 67-63-0 Isopropanol ug/m3
58.2 SG-6 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3
4.02 SG-3 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/m3
22.3 SG-2 75-09-2 Methylene Chloride ug/m3
7.11 SG-4 91-20-3 ~Naphthalene ug/m3
514 SG-4 115-07-1 Propylene ug/m3
4.36 SG-4 100-42-5 Styrene ug/m3
485 SG-3 127-18-4 Tetrachloroethylene ug/m3
222 SG-3 108-88-3 Toluene ug/m3
0.881 SG-3, J 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-ug/m3
2.67 SG-4 71-55-6 Trichloroethane, 1,1,1-ug/m3
24.7 SG-4 79-01-6 Trichloroethylene ug/m3
8.15 SG-DUP 75-69-4 Trichlorofluoromethane ug/m3
27.9 SG-3 95-63-6 Trimethylbenzene, 1,2,4-ug/m3
8.27 SG-3 108-67-8 Trimethylbenzene, 1,3,5-ug/m3
5.47 SG-4 75-01-4 Vinyl Chloride ug/m3
138 SG-3 1330-20-7 Xylenes ug/m3
Input Form 2D
Soil Gas Exposure Point Concentration Table
Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 27027-23-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Soil Gas
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 3.1E-05 1.4E+00 YES
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.3E-06 1.1E-01 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 27027-23-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Soil Gas
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor Air Concentration
(ug/m3)
Target Indoor Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated Carcinogenic Risk
Calculated
Non-Carcinogenic Hazard Quotient
67-64-1 Acetone 357 10.71 --71-43-2 Benzene 35 1.05 3.6E-01 6.3E+00 2.9E-06 3.4E-02106-99-0 Butadiene, 1,3-29.6 0.888 9.4E-02 4.2E-01 9.5E-06 4.3E-0175-15-0 Carbon Disulfide 176 5.28 -1.5E+02 7.2E-0367-66-3 Chloroform 44.5 1.335 1.2E-01 2.0E+01 1.1E-05 1.3E-02110-82-7 Cyclohexane 13 0.39 -1.3E+03 6.2E-05106-46-7 Dichlorobenzene, 1,4-1.5 0.045 2.6E-01 1.7E+02 1.8E-07 5.4E-0575-71-8 Dichlorodifluoromethane 4.39 0.1317 -2.1E+01 1.3E-0375-34-3 Dichloroethane, 1,1-28.6 0.858 1.8E+00 -4.9E-07156-59-2 Dichloroethylene, cis-1,2-27.5 0.825 -8.3E+00 2.0E-02141-78-6 Ethyl Acetate 1.79 0.0537 -1.5E+01 7.4E-0475-00-3 Ethyl Chloride (Chloroethane)1.2 0.036 -8.3E+02 8.6E-06100-41-4 Ethylbenzene 35.5 1.065 1.1E+00 2.1E+02 9.5E-07 1.0E-03109-99-9 ~Tetrahydrofuran 15.1 0.453 -4.2E+02 2.2E-04142-82-5 Heptane, N-155 4.65 -8.3E+01 1.1E-02110-54-3 Hexane, N-37.9 1.137 -1.5E+02 1.6E-03591-78-6 Hexanone, 2-21.5 0.645 -6.3E+00 2.1E-0267-63-0 Isopropanol 6.54 0.1962 -4.2E+01 9.4E-0478-93-3 Methyl Ethyl Ketone (2-Butanone)58.2 1.746 -1.0E+03 3.3E-04108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)4.02 0.1206 -6.3E+02 3.9E-0575-09-2 Methylene Chloride 22.3 0.669 1.0E+02 1.3E+02 6.6E-09 1.1E-0391-20-3 ~Naphthalene 7.11 0.2133 8.3E-02 6.3E-01 2.6E-06 6.8E-02115-07-1 Propylene 514 15.42 -6.3E+02 4.9E-03100-42-5 Styrene 4.36 0.1308 -2.1E+02 1.3E-04127-18-4 Tetrachloroethylene 485 14.55 1.1E+01 8.3E+00 1.3E-06 3.5E-01108-88-3 Toluene 222 6.66 -1.0E+03 1.3E-0376-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-0.881 0.02643 -1.0E+03 5.1E-0671-55-6 Trichloroethane, 1,1,1-2.67 0.0801 -1.0E+03 1.5E-0579-01-6 Trichloroethylene 24.7 0.741 4.8E-01 4.2E-01 1.5E-06 3.6E-0175-69-4 Trichlorofluoromethane 8.15 0.2445 --95-63-6 Trimethylbenzene, 1,2,4-27.9 0.837 -1.3E+01 1.3E-02108-67-8 Trimethylbenzene, 1,3,5-8.27 0.2481 -1.3E+01 4.0E-0375-01-4 Vinyl Chloride 5.47 0.1641 1.7E-01 2.1E+01 9.8E-07 1.6E-031330-20-7 Xylenes 138 4.14 -2.1E+01 4.0E-02
Cumulative:3.1E-05 1.4E+00
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 27027-23-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Soil Gas
CAS #Chemical Name:
Soil Gas Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor Air Conc. for Carcinogens @
TCR = 1E-06
Target Indoor Air Conc. for Non-Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 357 3.57 --71-43-2 Benzene 35 0.35 1.6E+00 2.6E+01 2.2E-07 2.7E-03106-99-0 Butadiene, 1,3-29.6 0.296 4.1E-01 1.8E+00 7.2E-07 3.4E-0275-15-0 Carbon Disulfide 176 1.76 -6.1E+02 5.7E-0467-66-3 Chloroform 44.5 0.445 5.3E-01 8.6E+01 8.3E-07 1.0E-03
110-82-7 Cyclohexane 13 0.13 -5.3E+03 4.9E-06
106-46-7 Dichlorobenzene, 1,4-1.5 0.015 1.1E+00 7.0E+02 1.3E-08 4.3E-06
75-71-8 Dichlorodifluoromethane 4.39 0.0439 -8.8E+01 1.0E-04
75-34-3 Dichloroethane, 1,1-28.6 0.286 7.7E+00 -3.7E-08
156-59-2 Dichloroethylene, cis-1,2-27.5 0.275 -3.5E+01 1.6E-03141-78-6 Ethyl Acetate 1.79 0.0179 -6.1E+01 5.8E-0575-00-3 Ethyl Chloride (Chloroethane)1.2 0.012 -3.5E+03 6.8E-07100-41-4 Ethylbenzene 35.5 0.355 4.9E+00 8.8E+02 7.2E-08 8.1E-05
109-99-9 ~Tetrahydrofuran 15.1 0.151 -1.8E+03 1.7E-05
142-82-5 Heptane, N-155 1.55 -3.5E+02 8.8E-04
110-54-3 Hexane, N-37.9 0.379 -6.1E+02 1.2E-04
591-78-6 Hexanone, 2-21.5 0.215 -2.6E+01 1.6E-03
67-63-0 Isopropanol 6.54 0.0654 -1.8E+02 7.5E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)58.2 0.582 -4.4E+03 2.7E-05
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)4.02 0.0402 -2.6E+03 3.1E-06
75-09-2 Methylene Chloride 22.3 0.223 1.2E+03 5.3E+02 1.8E-10 8.5E-0591-20-3 ~Naphthalene 7.11 0.0711 3.6E-01 2.6E+00 2.0E-07 5.4E-03
115-07-1 Propylene 514 5.14 -2.6E+03 3.9E-04
100-42-5 Styrene 4.36 0.0436 -8.8E+02 1.0E-05127-18-4 Tetrachloroethylene 485 4.85 4.7E+01 3.5E+01 1.0E-07 2.8E-02108-88-3 Toluene 222 2.22 -4.4E+03 1.0E-04
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-0.881 0.00881 -4.4E+03 4.0E-07
71-55-6 Trichloroethane, 1,1,1-2.67 0.0267 -4.4E+03 1.2E-06
79-01-6 Trichloroethylene 24.7 0.247 3.0E+00 1.8E+00 8.3E-08 2.8E-02
75-69-4 Trichlorofluoromethane 8.15 0.0815 --
95-63-6 Trimethylbenzene, 1,2,4-27.9 0.279 -5.3E+01 1.1E-03108-67-8 Trimethylbenzene, 1,3,5-8.27 0.0827 -5.3E+01 3.1E-0475-01-4 Vinyl Chloride 5.47 0.0547 2.8E+00 8.8E+01 2.0E-08 1.2E-041330-20-7 Xylenes 138 1.38 -8.8E+01 3.2E-03
Cumulative:2.3E-06 1.1E-01
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Prepared By:Hart and Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC
Site-Wide Worst Case Soil Gas - No Chloroform or 1,3-Butadiene
North Carolina Department of Environmental Quality
Risk Calculator
Former Ables Auto (TPI-002)
2501, 2511, and 2533 Wilkinson Boulevard, Charlotte, NC
Brownfields Redevelopment Section
27027-23-060
July 2023
May 2023 EPA RSL Table
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 27027-23-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Soil Gas
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2023Basis: May 2023 EPA RSL TableSite ID: 27027-23-060Exposure Unit ID: Site-Wide Hypothetical Worst Case Soil GasDescription of Exposure Point Concentration Selection:Exposure Point Concentration (ug/m3)Notes: CAS Number ChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion357 SG-6 67-64-1 Acetoneug/m335 SG-3 71-43-2 Benzeneug/m3176 SG-3 75-15-0 Carbon Disulfide ug/m313 SG-5 110-82-7 Cyclohexaneug/m31.5 SG-5, J 106-46-7 Dichlorobenzene, 1,4- ug/m34.39 SG-2/SG-DUP 75-71-8 Dichlorodifluoromethane ug/m328.6 SG-4, J 75-34-3 Dichloroethane, 1,1- ug/m327.5 SG-4, J 156-59-2 Dichloroethylene, cis-1,2- ug/m31.79 SG-5, J 141-78-6 Ethyl Acetateug/m31.2 SG-4, J 75-00-3 Ethyl Chloride (Chloroethane) ug/m335.5 SG-3 100-41-4 Ethylbenzeneug/m315.1 SG-5 109-99-9 ~Tetrahydrofuran ug/m3155 SG-3 142-82-5 Heptane, N-ug/m337.9 SG-3 110-54-3 Hexane, N-ug/m321.5 SG-5 591-78-6 Hexanone, 2-ug/m36.54 SG-6 67-63-0 Isopropanolug/m358.2 SG-6 78-93-3 Methyl Ethyl Ketone (2-Butanone) ug/m34.02 SG-3 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) ug/m322.3 SG-2 75-09-2 Methylene Chloride ug/m37.11 SG-4 91-20-3 ~Naphthaleneug/m3514 SG-4 115-07-1 Propyleneug/m34.36 SG-4 100-42-5 Styreneug/m3485 SG-3 127-18-4 Tetrachloroethylene ug/m3222 SG-3 108-88-3 Tolueneug/m30.881 SG-3, J 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- ug/m32.67 SG-4 71-55-6 Trichloroethane, 1,1,1- ug/m324.7 SG-4 79-01-6 Trichloroethylene ug/m38.15 SG-DUP 75-69-4 Trichlorofluoromethane ug/m327.9 SG-3 95-63-6 Trimethylbenzene, 1,2,4- ug/m38.27 SG-3 108-67-8 Trimethylbenzene, 1,3,5- ug/m35.47 SG-4 75-01-4 Vinyl Chloride ug/m3138 SG-3 1330-20-7 Xylenesug/m3Input Form 2DSoil Gas Exposure Point Concentration TableNote: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsNorth Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 27027-23-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Soil Gas
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use* NC NC NC
Soil NC NC NC
Groundwater Use* NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.1E-05 9.4E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 7.5E-07 7.4E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 27027-23-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Soil Gas
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 357 10.71 - -
71-43-2 Benzene 35 1.05 3.6E-01 6.3E+00 2.9E-06 3.4E-02
75-15-0 Carbon Disulfide 176 5.28 - 1.5E+02 7.2E-03
110-82-7 Cyclohexane 13 0.39 - 1.3E+03 6.2E-05
106-46-7 Dichlorobenzene, 1,4- 1.5 0.045 2.6E-01 1.7E+02 1.8E-07 5.4E-05
75-71-8 Dichlorodifluoromethane 4.39 0.1317 - 2.1E+01 1.3E-03
75-34-3 Dichloroethane, 1,1- 28.6 0.858 1.8E+00 - 4.9E-07
156-59-2 Dichloroethylene, cis-1,2- 27.5 0.825 - 8.3E+00 2.0E-02
141-78-6 Ethyl Acetate 1.79 0.0537 - 1.5E+01 7.4E-04
75-00-3 Ethyl Chloride (Chloroethane) 1.2 0.036 - 8.3E+02 8.6E-06
100-41-4 Ethylbenzene 35.5 1.065 1.1E+00 2.1E+02 9.5E-07 1.0E-03
109-99-9 ~Tetrahydrofuran 15.1 0.453 - 4.2E+02 2.2E-04
142-82-5 Heptane, N- 155 4.65 - 8.3E+01 1.1E-02
110-54-3 Hexane, N- 37.9 1.137 - 1.5E+02 1.6E-03
591-78-6 Hexanone, 2- 21.5 0.645 - 6.3E+00 2.1E-02
67-63-0 Isopropanol 6.54 0.1962 - 4.2E+01 9.4E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone) 58.2 1.746 - 1.0E+03 3.3E-04
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 4.02 0.1206 - 6.3E+02 3.9E-05
75-09-2 Methylene Chloride 22.3 0.669 1.0E+02 1.3E+02 6.6E-09 1.1E-03
91-20-3 ~Naphthalene 7.11 0.2133 8.3E-02 6.3E-01 2.6E-06 6.8E-02
115-07-1 Propylene 514 15.42 - 6.3E+02 4.9E-03
100-42-5 Styrene 4.36 0.1308 - 2.1E+02 1.3E-04
127-18-4 Tetrachloroethylene 485 14.55 1.1E+01 8.3E+00 1.3E-06 3.5E-01
108-88-3 Toluene 222 6.66 - 1.0E+03 1.3E-03
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.881 0.02643 - 1.0E+03 5.1E-06
71-55-6 Trichloroethane, 1,1,1- 2.67 0.0801 - 1.0E+03 1.5E-05
79-01-6 Trichloroethylene 24.7 0.741 4.8E-01 4.2E-01 1.5E-06 3.6E-01
75-69-4 Trichlorofluoromethane 8.15 0.2445 - -
95-63-6 Trimethylbenzene, 1,2,4- 27.9 0.837 - 1.3E+01 1.3E-02
108-67-8 Trimethylbenzene, 1,3,5- 8.27 0.2481 - 1.3E+01 4.0E-03
75-01-4 Vinyl Chloride 5.47 0.1641 1.7E-01 2.1E+01 9.8E-07 1.6E-03
1330-20-7 Xylenes 138 4.14 - 2.1E+01 4.0E-02
Cumulative: 1.1E-05 9.4E-01
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 27027-23-060
Exposure Unit ID: Site-Wide Hypothetical Worst Case Soil Gas
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 357 3.57 - -
71-43-2 Benzene 35 0.35 1.6E+00 2.6E+01 2.2E-07 2.7E-03
75-15-0 Carbon Disulfide 176 1.76 - 6.1E+02 5.7E-04
110-82-7 Cyclohexane 13 0.13 - 5.3E+03 4.9E-06
106-46-7 Dichlorobenzene, 1,4- 1.5 0.015 1.1E+00 7.0E+02 1.3E-08 4.3E-06
75-71-8 Dichlorodifluoromethane 4.39 0.0439 - 8.8E+01 1.0E-04
75-34-3 Dichloroethane, 1,1- 28.6 0.286 7.7E+00 - 3.7E-08
156-59-2 Dichloroethylene, cis-1,2- 27.5 0.275 - 3.5E+01 1.6E-03
141-78-6 Ethyl Acetate 1.79 0.0179 - 6.1E+01 5.8E-05
75-00-3 Ethyl Chloride (Chloroethane) 1.2 0.012 - 3.5E+03 6.8E-07
100-41-4 Ethylbenzene 35.5 0.355 4.9E+00 8.8E+02 7.2E-08 8.1E-05
109-99-9 ~Tetrahydrofuran 15.1 0.151 - 1.8E+03 1.7E-05
142-82-5 Heptane, N- 155 1.55 - 3.5E+02 8.8E-04
110-54-3 Hexane, N- 37.9 0.379 - 6.1E+02 1.2E-04
591-78-6 Hexanone, 2- 21.5 0.215 - 2.6E+01 1.6E-03
67-63-0 Isopropanol 6.54 0.0654 - 1.8E+02 7.5E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone) 58.2 0.582 - 4.4E+03 2.7E-05
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 4.02 0.0402 - 2.6E+03 3.1E-06
75-09-2 Methylene Chloride 22.3 0.223 1.2E+03 5.3E+02 1.8E-10 8.5E-05
91-20-3 ~Naphthalene 7.11 0.0711 3.6E-01 2.6E+00 2.0E-07 5.4E-03
115-07-1 Propylene 514 5.14 - 2.6E+03 3.9E-04
100-42-5 Styrene 4.36 0.0436 - 8.8E+02 1.0E-05
127-18-4 Tetrachloroethylene 485 4.85 4.7E+01 3.5E+01 1.0E-07 2.8E-02
108-88-3 Toluene 222 2.22 - 4.4E+03 1.0E-04
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.881 0.00881 - 4.4E+03 4.0E-07
71-55-6 Trichloroethane, 1,1,1- 2.67 0.0267 - 4.4E+03 1.2E-06
79-01-6 Trichloroethylene 24.7 0.247 3.0E+00 1.8E+00 8.3E-08 2.8E-02
75-69-4 Trichlorofluoromethane 8.15 0.0815 - -
95-63-6 Trimethylbenzene, 1,2,4- 27.9 0.279 - 5.3E+01 1.1E-03
108-67-8 Trimethylbenzene, 1,3,5- 8.27 0.0827 - 5.3E+01 3.1E-04
75-01-4 Vinyl Chloride 5.47 0.0547 2.8E+00 8.8E+01 2.0E-08 1.2E-04
1330-20-7 Xylenes 138 1.38 - 8.8E+01 3.2E-03
Cumulative: 7.5E-07 7.4E-02
All concentrations are in ug/m3
Output Form
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator