27025_Stay Right Tank_PIIR_20230922

WithersRavenel
04100
Our People. Your Success.
LIMITED PHASE II
ENVIRONMENTAL SITE ASSESSMENT
Hillsborough Street Assemblage
5200 Hillsborough Street
Raleigh, Wake County, North Carolina
WR Project No. 23-0302
Stay Right Tank Site
Brownfields Project No. 27025-23-092
Prepared for:
FRH Realty LLC
33330 Cumberland Boulevard, Suite 375
Atlanta, GA 30339
Prepared by:
WithersRavenel
115 MacKenan Drive
Cary, North Carolina 27511
North Carolina Firm License No. F-1479
September 22, 2023

WithersRavenel
04100
Our People. Your Success.
September 22, 2023
FRH Realty LLC
33330 Cumberland Boulevard, Suite 375
Atlanta, GA 30339
ATTN: Mr. Bryan Condie
RE: Limited Phase II Environmental Site Assessment
Hillsborough Street Assemblage
5200 Hillsborough Street
Raleigh, Wake County, North Carolina
WR Project No. 23-0302
Stay Right Tank Site
Brownfields Project No. 27025-23-092
WithersRavenel (WR) is pleased to submit this report describing the limited Phase II Environmental
Site Assessment (ESA) activities for the above -referenced property. Assessment activities were
completed as a general screen of soil, groundwater, and soil vapor conditions at the subject site
relative to former onsite industrial use of the subject site, a former onsite underground storage tank
(UST), and adjacent properties with known releases of materials, based on information determined
during a Phase I ESA completed on the subject site by WR in May 2022. This report summarizes the
results of WR's field activities and presents the findings of the assessment of existing environmental
conditions at the site.
Sincerely,
WithersRavenel
Austin Pote, E.I.
Assistant Project Engineer
by ..N ° CARp��'o
SEAL =
Awe-
2310
G. Matthew James, P.G. F�\�
Project Geologist'rrHEw° �P
115 MacKenan Drive I Cary, NC 27511
t: 919.469.3340 1 f: 919.467.6008 1 www.withersravenel.com I License No. F-1479
Asheville ICary I Greensboro I Pittsboro I Raleigh I Wilmington

TABLE OF CONTENTS
1 Property Description..............................................................................................1
1.1 Location and Legal Description..........................................................................................1
2 Field Assessment Activities..................................................................................2
2.1 Utility Location and GPR/EM Survey................................................................................. 2
2.2 Soil Borings........................................................................................................................3
2.3 Groundwater Assessment.................................................................................................4
2.4 Soil Vapor Assessment...................................................................................................... 5
2.5 Quality Assurance / Quality Control.................................................................................. 6
3 Findings, Conclusions, and Recommendations................................................7
Figures
Figure 1 General Location Map
Figure 2 Site Map
Figure 3 Phase II ESA Soil Exceedances Map
Figure 4 Phase II ESA Groundwater Contour Map
Figure 5 Phase II ESA Groundwater Exceedances Map
Figure 6 Phase II ESA Soil Vapor Exceedances Map
Tables
Table 1
Summary of Soil Analytical Results
Table 2A
Temporary Monitoring Well Construction Information
Table 2B
Summary of Groundwater Analytical Results
Table 3
Summary of Soil Vapor Analytical Results
Appendices
Appendix A
Boring Logs
Appendix B
Laboratory Analytical Reports
Appendix C
Field Notes and Photographic Record
Appendix D
NCDEQ Risk Calculator Results

::WithersRavenel
Our People. Your Success.
Property Description
1.1 Location and Legal Description
WR has performed a Limited Phase II ESA on a ±3.05-acre site located in the northwestern quadrant of the
intersection of Youth Center Drive and Hillsborough Street in Raleigh, Wake County, North Carolina (Figure
1). According to Wake County GIS records, the subject property consists of the following eight parcels:
1 0784439213
2 0784438203
3 0784437117
4 0784436145
5 0784436239
6 1 0784435399
GATE 3 ENTERPRISES LLC
GATE 3 ENTERPRISES LLC
GBH PARTNERS LLC
GBH PARTNERS LLC
Justin Booth
CSB ENTERPRISES LLC
5200 Hillsborough Street ±0.46
5204 Hillsborough Street ±0.58
5210 Hillsborough Street 1 ±0.35
5212 Hillsborough Street ±0.33
108 Grand Avenue ±0.35
114 Grand Avenue; 5209 ±0.35
Dorcas Street
7 1 0784437326 I GATE 3 ENTERPRISES LLC 5205 Dorcas Street 1 ±0.23
8 0784437389 GATE 3 ENTERPRISES LLC 5203 Dorcas Street ±0.40
The current site layout is provided as Figure 2. This Limited Phase II ESA was completed at the request of
FRH Realty LLC (Client) based on the findings of a Phase I ESA completed by WR on the subject site in May
2022.
The use of the subject property has been for industrial, commercial and residential purposes since at least
1938 with uses including septic tank manufacturing, a beauty shop, radiator and lawn mower service, an
electrical contractor, retail, sanitation service, mulch and stone sales, and car/boat storage. The commercial
structure on Tract 4 was constructed in 1952, the residential structure on Tract 5 was constructed in 1920,
and the residential structures on Tract 6 were constructed in 1925 and 1940. The subject property appears
on the North Carolina Department of Environmental Quality (NCDEQ) underground storage tank (UST)
database due to one 1,000-gallon gasoline UST identified on the subject property. According to information
in an Environmental Database Resources (EDR) report ordered for the May 2022 Phase I ESA, the onsite
UST was installed on May 5, 1966 and removed on September 1, 1988. Based on available information,
there is no indication of a proper UST closure following NCDEQ guidelines. The exact location of the former
onsite UST was not able to be determined during the May 2022 Phase I ESA, as no historical information or
interviewed parties indicated the location of the former UST. A former 2019 Phase I ESA conducted on a
portion of the subject site, and reviewed by WR, indicated that the UST was formerly located in the
southeastern portion of Tract 1, which corresponds to the area of a former residential structure. However,
this information was unable to be confirmed during WR's 2022 Phase I ESA. The former onsite UST was
considered to represent a Recognized Environmental Condition (REC) during the May 2022 Phase I ESA.
Additionally, WR observed a concrete foundation along the shared boundaries of Tracts 1, 2, and 8 (Figure
2). According to the current property owner representative, the foundation corresponds to a small concrete
septic tank manufacturing facility that was built sometime in the 1950s and remained onsite until sometime
in the 1970s or 1980s. The owner indicated that the septic tanks were poured by hand and/or by overhead
Hillsborough Street Assemblage: Raleigh, NC WR No. 23-0302
Limited Phase II Environmental Site Assessment September 2023
1

::WithersRavenel
Our People. Your Success.
cranes and that no other process equipment or petroleum/chemicals were used in the process, to
knowledge. WR was unable to speak with a representative familiar with the site during the use of the site
for septic tank manufacturing to determine if any chemicals/petroleum products common for industrial
processes were used onsite. WR considered the former onsite manufacturing facility to represent an REC
during the May 2022 Phase I ESA.
Furthermore, according to historical resources researched during the completion of the May 2022 Phase I
ESA, businesses such as refueling stations, beverage companies, wood processing facilities, and
garages/auto repair facilities have historically been located in the vicinity of the subject property beginning
by the early- to mid-1900s. Many of these businesses have been located on adjacent properties, and the
associated buildings and USTs have been located as close as 50 feet from the subject property. Some of
these properties are associated with incidents from USTs or spilled chemicals, and others have not had
incidents reported for the facility. Some of the nearby sites were listed in 2022 on NCDEQ's UST database
with remaining onsite USTs. One of the nearby properties with a confirmed release corresponds to a
southeastern adjacent property known as Jean's Starflite (Figure 2). Groundwater contamination reported
in documents available in 2022 indicated contaminants having extended onto the southern portion of Tract
1 of the subject site.
An additional nearby property is listed on the SHWS database and corresponds to a southern adjacent
property known as the Burke's Hardware property (Figure 2). This listing corresponds to numerous vicinity
water supply wells contaminated with chlorinated solvents, including trichloroethylene (TCE) and
tetrachloroethylene (PCE). At the time of the May 2022 Phase I ESA, limited amounts of groundwater
assessments had been conducted. A memo from NCDEQ in 2019 indicated that a groundwater plume is still
present at the Burke's Hardware site. No determination of a source or groundwater flow direction had been
reported at the time of the May 2022 Phase I ESA. WR considered the surrounding vicinity to represent an
REC relative to the subject site.
In light of the findings from the May 2022 Phase I ESA, FRH Realty LLC submitted a Brownfields Property
Application to the NCDEQ Brownfields Redevelopment Section (BRS) and received a Letter of Eligibility
from NCDEQ dated June 19, 2023. This assessment was completed in anticipation of FRH Realty LLC's
participation in the BRS and includes the typical assessment protocols and requirements of the BRS. A BRS
project manager had not yet been assigned to project when this assessment work was conducted and thus
was not conducted pursuant to a BRS-approved work plan.
The following report describes the limited assessment activities conducted at the subject property and the
findings of this Limited Phase II ESA.
2 Field Assessment Activities
2.1 Utility Location and GPR/EM Survey
Prior to conducting subsurface assessment activities at the subject site, WR contacted the North Carolina
One Call Center (NC One Call) to locate underground utilities at the subject property. As NC One Call does
not locate all utilities located within property boundaries, WR's Subsurface Utility Engineering (SUE)
department mobilized to the subject site to locate private lines such as water, sewer, fiber optic, or other
sub -surface utilities located in or near the areas of planned subsurface assessment. Congruent with
assessment activities at the site on May 22, 2023, WR SUE utilized Ground Penetrating Radar (GPR) and
Electromagnetic (EM) equipment to survey the fenced boat storge lot on Tracts 1, 2, 7, and 8 to determine
if any USTs were present on these tracts. No USTs were discovered during the GPR/EM survey, which
implies that the UST listed on NCDEQ's database had been removed from the subject site.
Hillsborough Street Assemblage: Raleigh, NC WR No. 23-0302
Limited Phase II Environmental Site Assessment September 2023
2

::WithersRavenel
Our People. Your Success.
2.2 Soil Borings
On May 11 and 12, 2023, WR, along with drilling subcontractor Quantex utilizing a track -mounted
GeoProbe® drill rig, advanced 10 soil borings (TW-1 through TW-10) at various locations on the subject site
into the subsurface water table, which generally corresponded to depths of approximately 20 or 25 feet
below land surface (BLS). The locations of the soil borings were placed within the proposed footprint of the
planned onsite residential structure, determined by a concept plan provided to WR by the Client. Soil borings
TW-1 and TW-6 were completed on Tract 1, TW-2 was completed on Tract 2, TW-3 was completed on
Tract 7, TW-4 and TW-5 were completed on Tract 8, TW-7 and TW-8 were completed on Tract 6, TW-9
was completed on Tract 5, and TW-10 was completed on Tract 4. See Figure 3 for a map indicating the soil
boring locations.
Soil was collected at approximate 2.5-foot intervals in each of the borings, classified, and placed in individual
zip -lock baggies for field screening by a field calibrated MiniRAE3000 Photoionization Detector (PID) for
the presence of total volatile organic vapors. No petroleum or chemical odors were noted during screening
of the soil samples, with the exception of TW-6. PID readings in TW-6 were below 1 ppm for all intervals
except the 20-22.5 feet BLS interval, which was 238 ppm. A petroleum odor was also noted in the 20-22.5
foot interval. The water table was observed at approximately 17 feet BLS in boring TW-6, indicating that
the interval with the observed odor and elevated PID reading was within the water table below the site. The
general lithology of the site consisted of clays and silts with some occurrences of sand and rock
fragments/mica. Refer to the attached boring logs in Appendix A for soil classifications and PID readings.
Soil samples were submitted for laboratory analysis from the 5-7.5 feet BLS interval in each completed soil
boring, which was determined based on the possible future grading depths at the site and site
observations/PID readings. The soil with the observed petroleum odor and elevated PID reading from TW-
6 was from a depth below the water table (-17.5 feet BLS) and was not submitted for laboratory analysis
due to the soil being saturated with groundwater. A duplicate soil sample (DUP) was submitted from boring
TW-6 from the same depth as the original TW-6 soil sample (5-7.5 feet BLS). Following collection, a small
sample of soil was placed in a Ziplock baggie for vapor screening while the remaining sample was
immediately placed in pre -preserved laboratory supplied glassware specific to the analysis requested for the
samples. Each sample was immediately placed on ice within a cooler, and submitted under chain -of -custody
protocols to Pace Analytical in Mount Juliet, TN. All soil samples submitted from the subject site were
analyzed for volatile organic compounds (VOCs) by Environmental Protection Agency (EPA) Method 8260,
semi-VOCs (SVOCs) by EPA Method 8270, RCRA-8 Metals by EPA Method 6020B, mercury by EPA method
7471B, and hexavalent chromium by EPA Method 7199. Copies of chain -of -custody records are included
with the analytical results in Appendix B.
Soil Analytical Results — VOCs, SVOCs, Metals
Laboratory analytical results for the soil samples indicated the presence of targeted compounds at
concentrations above the method detection limits (MDLs). Those results are summarized by analysis type
below:
• No targeted VOCs were reported at concentrations above MDLs for any of the soil samples
submitted for analysis of VOCs, with the exception of a low concentration of tert-butyl benzene well
below its current applicable NCDEQ preliminary soil remediation goals (PSRGs) in the soil sample
submitted from TW-7.
• Numerous targeted SVOCs were reported at concentrations above MDLs for soil samples submitted
from TW-4 and TW-5. Two of the targeted SVOC concentrations were higher than current PSRGs,
as follows:
o The reported concentration of benzo(a)anthracene was 0.402 mg/kg in soil sample TW-4,
which exceeds its protection of groundwater PSRG of 0.35 mg/kg.
Hillsborough Street Assemblage: Raleigh, NC
Limited Phase II Environmental Site Assessment
WR No. 23-0302
September 2023
3

::WithersRavenel
Our People. Your Success.
o The reported concentration of benzo(a)pyrene was 0.261 mg/kg in soil sample TW-4, which
exceeds its residential health based PSRG of 0.11 mg/kg.
o No targeted SVOCs were reported at concentrations exceeding applicable
industrial/commercial health based PSRGs in any submitted soil sample.
• Numerous targeted metals were reported at concentrations above MDLs for all soil samples
submitted from the subject site. Several of the targeted metals concentrations were higher than
current PSRGs, as follows:
o The reported concentrations of arsenic exceeded the industrial/commercial health based
PSRG for arsenic of 3.0 mg/kg in all soil samples submitted from the subject site, including
elevated concentrations above 10 mg/kg in soil samples TW-3, TW-4, TW-7, TW-8, TW-9,
and TW-10.
o The reported concentrations of hexavalent chromium exceeded the residential health based
PSRG for hexavalent chromium of 0.31 mg/kg, but below hexavalent chromium's
industrial/commercial health based PSRG, in all soil samples submitted from the subject site,
except for soil sample TW-10, which was not reported at a concentration exceeding its
respective MDL.
The laboratory analytical results for the soil samples are summarized in Table 1 and shown on Figure 3.
Copies of the laboratory analytical reports are provided in Appendix B.
2.3 Groundwater Assessment
On May 11 and 12, 2023, all 10 of the soil borings were converted into temporary groundwater monitoring
wells. Locations of each temporary monitoring well are depicted on Figure 4 and Figure 5. The temporary
monitoring wells were constructed with a one -inch diameter PVC screen section extending from the base
of the boring connecting to one -inch diameter PVC risers to surface grade. Sand was placed around the
screen section and bentonite was placed above the sand. The temporary monitoring wells were constructed
as described in the boring logs in Appendix A and shown on Table 2A. Upon completion of temporary
monitoring well construction, each temporary monitoring well was properly developed to remove as much
suspended sediment from the groundwater as possible.
Prior to purging and sampling each well, the depth to groundwater within the temporary monitoring wells
was gauged utilizing an electronic water level indicator. However, the temporary monitoring wells were not
equilibrated on May 11 or 12 due to slow recharge rates. Therefore, WR measured the water level in the 10
temporary groundwater monitoring wells on May 22, 2023 during additional assessment activities. The
measured groundwater depths ranged from 16.52 feet to the top -of -casing (TOC) in TW-4 to 21.06 feet
TOC in TW-7. WR used a laser level and level rod to survey the TOC elevations of all onsite temporary wells
relative to each other based on an assumed elevation of 100 feet applied to TW-5. Based on the relative
elevations and the measured water depths, WR calculated the relative groundwater elevation in each
temporary well and determined the overall groundwater flow direction for the subject site. The groundwater
flow direction for the subject site is to the northwest, following the topographic slope of the subject site.
See Table 2A for all temporary monitoring well groundwater depths and calculated groundwater elevations;
see Figure 4 for a groundwater contour map including groundwater elevations and flow direction.
On May 11 and 12, 2023, each temporary monitoring well was purged of at least three well volumes, or
until dry, utilizing dedicated polyethylene tubing and a peristaltic pump. The groundwater samples were then
collected from the onsite temporary monitoring wells in pre -preserved laboratory supplied glassware
specific to the analysis requested for the samples. A duplicate groundwater sample (DUP) was submitted
from temporary well TW-6. Following collection, all groundwater samples were placed on ice within a cooler,
and submitted under chain -of -custody protocols to Pace Analytical in Mount Juliet, TN for analysis of VOCs
by Standard Method (SM) 6200, SVOCs by SM 625, and select metals including hexavalent chromium by
Hillsborough Street Assemblage: Raleigh, NC WR No. 23-0302
Limited Phase II Environmental Site Assessment September 2023
4

::WithersRavenel
Our People. Your Success.
the appropriate EPA methods. Copies of chain -of -custody records are included with the analytical results in
Appendix B.
Groundwater Analytical Results — VOCs, SVOCs, Metals
Laboratory analysis results for the groundwater samples indicated the presence of targeted compounds at
concentrations above MDLs. Those results are summarized by analysis type below:
• Numerous targeted VOCs were reported at concentrations above MDLs for most groundwater
samples submitted from the subject site. The following VOCs were reported at a concentration that
exceeded their NC Groundwater Standard established in 15A NCAC 2L (NC 2L standard):
o The reported concentration of benzene was 239 µg/L in groundwater sample TW-2, which
exceeds its NC 2L standard of 1.0 µg/L.
o The reported concentration of 1,2-dichloroethane (1,2-DCA) was 10.5 µg/L in groundwater
sample TW-2, which exceeds its NC 2L standard of 0.4 µg/L.
o The reported concentration of naphthalene was 19.2 µg/L in groundwater sample TW-2,
which exceeds its NC 2L standard of 6.0 µg/L.
o The reported concentration of m&p-xylenes was 676 µg/L in groundwater sample TW-2,
which exceeds its NC 2L standard of 500 µg/L.
• Numerous targeted SVOCs were reported at concentrations above MDLs for most groundwater
samples submitted from the subject site. The following SVOC was reported at a concentration that
exceeded its NC 2L standard:
o The reported concentration of naphthalene was 11.3 µg/L in groundwater sample TW-1,
which exceeds its NC 2L standard of 6.0 µg/L.
• Numerous targeted metals were reported above MDLs for each groundwater sample submitted
from the subject site; however, no reported metal concentrations exceeded relative NC 2L
standards.
o Additionally, neither Arsenic or Hexavalent Chromium was reported in the collected
samples at a concentration exceeded 1 µg/L.
• No reported concentrations of targeted compounds in submitted groundwater samples exceeded
their respective gross contaminant levels (GCLs).
The laboratory analysis results for the groundwater samples are summarized in Table 2B and shown on
Figure 5. Copies of the laboratory analytical reports are provided in Appendix B.
2.4 Soil Vapor Assessment
While onsite on May 11 and 12, 2023, 10 temporary soil vapor sampling probes (SVP) (VP-1 through VP-
10) were installed immediately adjacent to the 10 completed soil borings, as depicted on Figure 6. The SVPs
were completed as described in the boring logs in Appendix A. The SVPs were allowed to sit for well over
24 hours to ensure a proper seal was achieved around each SVP. WR purged and sampled the ten SVPs on
May 22, 2023.
Prior to collecting soil vapor samples, each SVP was purged for 3 to 5 minutes using a PID. No elevated PID
readings above 1 ppm were observed for any of the onsite SVPs. Additionally, a helium shroud set up was
utilized to check for leaks in the seal of the bentonite around each SVP and the tubing/controller
connections for each sampling apparatus. WR ensured the recommended shroud ambient helium
concentration between 20% and 30% was utilized for each leak detection test, and that no tubing readings
for each SVP exceeded a concentration of helium more than 1% of the ambient concentration. A duplicate
soil vapor sample was collected from VP-9 by connecting a separate flow controller and summa canister to
Hillsborough Street Assemblage: Raleigh, NC WR No. 23-0302
Limited Phase II Environmental Site Assessment September 2023
5

::WithersRavenel
Our People. Your Success.
the sample train. A helium leak test was also performed on the duplicate soil vapor sample. See Appendix
C for a copy of all field notes, including the soil vapor sampling field forms with helium shroud leak detection
test info. Soil vapor samples were collected in laboratory supplied 1-liter Suma canisters with dedicated flow
controllers. Following collection, samples were submitted under chain -of -custody protocols to Eurofins -
Air Toxics in Folsom, CA for analysis of VOCs by EPA Method TO-15. A copy of the chain -of -custody record
is included with analytical data in Appendix B.
Soil Vapor Analytical Results - VOCs
Laboratory analysis results for the soil vapor samples indicated the presence of targeted VOCs at
concentrations above MDLs. Those results are summarized below:
• Numerous targeted VOCs were reported at concentrations above MDLs for all soil vapor samples
submitted from the subject site. The following VOCs were reported at a concentration that
exceeded applicable NCDEQ residential soil gas screening levels (SGSLs):
o The reported concentration of chloroform was 15 µg/m3 in soil vapor sample VP-2, which
exceeds its residential SGSL standard of 4.1 µg/m3.
o The reported concentration of chloroform was 4.5 µg/m3 in soil vapor sample VP-3, which
exceeds its residential SGSL standard of 4.1 µg/m3.
o The reported concentration of ethylbenzene was 44 µg/m3 in soil vapor sample VP-9, which
exceeds its residential SGSL standard of 37.4 µg/m3.
o The reported concentration of chloroform was 6.1 µg/m3 in soil vapor sample VP-10, which
exceeds its residential SGSL standard of 4.1 µg/m3.
o The reported concentration of ethylbenzene was 53 µg/m3 in soil vapor sample VP-10,
which exceeds its residential SGSL standard of 37.4 µg/m3.
No targeted VOCs were reported above applicable non-residential SGSLs.
The analytical results for the soil vapor samples are summarized in Table 3 and shown on Figure 6. A copy
of the analytical report is provided in Appendix B.
2.5 Quality Assurance/ Quality Control
Soil:
A duplicate soil sample was collected from TW-6. The soil sample and the duplicate were collected from
the same boring interval and the same macrocore. Both the TW-6 soil sample and the duplicate soil sample
were placed in bottleware supplied by the laboratory and transported under chain -of -custody to the
laboratory. Both the TW-6 soil sample and the duplicate soil sample were laboratory analyzed for VOCs by
EPA Method 8260, SVOCs by EPA Method 8270, RCRA-8 Metals by EPA Method 6020B, mercury by EPA
method 7471B, and hexavalent chromium by EPA Method 7199. The laboratory analytical reports were
reported to level II QA/QC including the reporting of J-flags (where the laboratory reported concentration
is an estimated value greater than the MDL but lower than the reporting limit). The duplicate soil sample
results from TW-6 did not exhibit high variability in concentrations when compared to the TW-6 soil sample
results.
Groundwater:
A duplicate groundwater sample was also collected from TW-6. The groundwater sample and the duplicate
groundwater sample were collected during the same sampling event. Both the TW-6 groundwater sample
and the duplicate groundwater sample were placed in bottleware supplied by the laboratory and transported
under chain -of -custody to the laboratory. Both the TW-6 groundwater sample and the duplicate
Hillsborough Street Assemblage: Raleigh, NC WR No. 23-0302
Limited Phase II Environmental Site Assessment September 2023
6

::WithersRavenel
Our People. Your Success.
groundwater sample were laboratory analyzed for VOCs by EPA Method 6200B, SVOCs by EPA Method
625.1, RCRA-8 Metals by EPA Method 6020B, mercury by EPA method 7470A, and hexavalent chromium
by EPA Method 7199. The laboratory analytical reports were reported to level II QA/QC including the
reporting of J-flags (where the laboratory reported concentration is an estimated value greater than the
MDL but lower than the reporting limit). Slight discrepancies were noted in the analytical data associated
with five analytes; however, the differences in analyte concentrations did not exceed 5 µg/L for any one
analyte. Additionally, none of the analyte discrepancies were at concentrations that exceeded the NC 2L
Standard.
Review of the laboratories quality control summary did not identify any analytes of concern that failed the
laboratories QA/QC protocol. A few qualifiers were identified in the Matrix Spike, but those qualifiers did
not appear to negatively affect the analytical data reported by the laboratory.
Soil Vapor.
A duplicate soil vapor sample was collected from VP-9. The VP-9 soil vapor sample and the duplicate soil
vapor sample were collected during the same sampling event and utilized the same helium shroud and
sample train. Different flow controllers were used for each laboratory supplied summa canister. Both the
VP-9 soil vapor sample and the duplicate soil vapor sample were laboratory analyzed for VOCs by EPA
Method TO-15. The laboratory analytical reports were reported to level II QA/QC including the reporting
of J-flags (where the laboratory reported concentration is an estimated value greater than the MDL but
lower than the reporting limit). The laboratory report noted that VP-9 and the duplicate sample were
analyzed at a dilution due to the presence of high-level non -target species. Efforts were made to ensure
that soil gas samples were analyzed with the lowest feasible MDLs under EPA Method TO-15. The duplicate
soil vapor sample results from VP-9 did not exhibit high variability in concentrations when compared to the
VP-9 soil sample results.
3 Findings, Conclusions, and Recommendations
At the request of FRH Realty LLC, WR performed a Limited Phase I I ESA on a ±3.05-acre property addressed
as 5200 Hillsborough Street in Raleigh, Wake County, North Carolina. This investigation was initiated to
evaluate soil, groundwater, and soil vapor conditions at the subject site relative to the former onsite
industrial use of the subject site, a former onsite UST, and adjacent properties with known releases of
materials, based on information determined during a Phase I ESA completed on the subject site by WR in
May 2022. This assessment was conducted in accordance with the typical assessment requirements of the
BRS, though a kickoff meeting has not yet occurred, and no work plan was submitted to the BRS for review
prior to the work.
Based on the findings of this assessment, WR did not identify the presence of existing USTs on Tracts 1, 2,
7, or 8 of the subject site. No apparent assessment was completed during the removal of the former onsite
UST, and therefore, it is possible that residual soil and/or groundwater contamination may be present in
localized areas not sampled during this limited assessment. However, based on the results of this
assessment, any potential release from the former onsite UST has not caused a large-scale impact to the
subject site. WR recommends paying close attention to soils on Tracts 1, 2, 7, and 8 during any future activities
for any evidence of odors or staining indicative of a release of petroleum material from the formerly onsite UST.
Any petroleum impacted soils discovered during grading will need to be managed in accordance with legal
requirements.
The highest concentrations of organic compounds and metals identified in the soil, groundwater, and soil
vapor samples were entered into the NCDEQ Risk Calculator. The risk calculator was developed by NCDEQ
to serve as a tool to help evaluate overall site risk posed by potential contaminants within environmental
media. Copies of the input and output sheets for the risk calculator using laboratory analysis results specific
to the subject site are provided in Appendix D.
Hillsborough Street Assemblage: Raleigh, NC WR No. 23-0302
Limited Phase 11 Environmental Site Assessment September 2023
7

::WithersRavenel
Our People. Your Success.
According to the risk calculator results, the highest concentrations of organic compounds and metals
detected in site soils do not pose an unacceptable risk to current or future site workers, however they would
pose unacceptable risk to potential site residents, construction workers, or trespassers. The highest
concentrations of VOCs detected in soil vapor samples do not pose unacceptable risk to residential or non-
residential receptors. However, the presence of benzene, 1,2-DCA, naphthalene, and m&p-xylenes at
concentrations greater than their respective NC 2L standard would pose an unacceptable risk to all potential
receptors who might come into contact with site groundwater.
WR recommends the following:
- Speaking with an environmental attorney for assistance understanding the risks involved with
development of a property with the type of contamination discovered during this assessment.
- Submitting this report to the BRS and discussing additional assessment requirements during a future BRS
"kickoff" meeting.
- Applying to and following the recommendations of the NC Brownfields Program.
- Including future design features that prevent occupant access to any contaminated soils.
- Avoiding the use of the groundwater beneath the subject site for any reason.
- Further evaluating the need for a vapor mitigation system in designs of any future onsite structures.
WR is pleased to submit this report describing the limited Phase II ESA activities for the site. This report has
summarized the results of WR's field activities and presents the findings of the assessment of existing
environmental conditions at the site.
If you have any questions, please contact us at 919-469-3340.
Sincerely,
WithersRavenel
5;�
Austin Pote, E.I.
Assistant Project Engineer
G. Matthew James, P.G.
Project Geologist
Hillsborough Street Assemblage: Raleigh, NC
Limited Phase II Environmental Site Assessment
WR No. 23-0302
September 2023
E3

FIGURES

r f
RBE CENTER RD
aLLj
I '
i
Lw
Ln
SUBJECT SITE. -lest -over
± 3.05 ACRES _
• pN r is :. ' !+ r; \ r ;''I
Aso c7
WESTER14 Bl
i _ BREW5TER DR-
Ln
4 —GRA ALE y� A
.ti
500 0
NE RQ 1 inch =1000 ft.
W i t h e rs Ra ve n e l HILLSBOROUGH STREET ASSEMBLAGE DRAWN BY: SCALE FIGURE NO
1 / 5200, 5210 & 114 RANDOROUGH STREET
108 & 114 GRAND AVENUE AP 1"=1000 ' 1
5203 & 5205 DORCAS STREET
Engineers I Planners I Surveyors RALEIGH, WAKE COUNTY, INC APPROVED BY: DATE: PROJECT NO.:
115 MacKenan Drive I Cary, NIC 275111 t: 919.469.33401 license #: F-1479 GENERAL LOCATION MAP LW 04/12/22 09211168.00
www.withersravenel.com
\1wnMema101.mm1wrmrpnasunilWRSharelRaleigh�21\2Y71fi0127176&Hillsborough MultifamilylEnviml_Ph.. I ESA Hillsborough St Whihmily\CADIFigures.Avg- April 12, 2022-SWOOTEN

'DENTIAL RESIDENTIAL LEGEND o
RESIDENTIAL 'o r . OF N d
POLE -MOUNTED TRANSFORMER LOCATION z z
w04
O.
GROUNDWATER MONITORING WELL LOCATION LL ii 0
RESIDE N
/ ® INACTIVE WATER SUPPLY WELL LOCATION o
CN
R IDJ` f
4oi r 1 t u M
L
w,+ NOTES: O
t ¢ Ln
/ 1.) LOCATIONS AND SIZES ARE APPROXIMATE AND NOT EXACT. O
E
.r'
x ti + r j �= m a o
dpr z a o 3
'r• 'r=_• RESIDENTIAL + o
.:1j,-
RESIDENTIALol
/� r
- SEPTIC t
FAIRGR
TANK
RAREA NG LOT
RESIDENTIAL }
SHED TRACT 8 ` r
±0.40 ACRES
a RESIDENC ti
RESIDENTIAL ��� �0 A W
OORCPS S 1( RESIDENCE N GRAVEL/GRASS LOT �` Lu
TRACT 6 W FORMERLY USED FOR
±0.35 ACRES �� BOAT STORAGE v7
�.
-.�. CARPORT �A �.� �
N
RESIDENTIAL GARgG ` .4
P ROXQ C- PNK
RESIDENTIAL ♦ TRACTS MERs�c��R\NG
FOR p.NUF REP W
±0.35 ACRES r^ P
VACANT
_ _ a
LOT RESIDENCE GRAVEL/GRASS LOT m W
FORMERLY USED FOR
VACANT BOATSTORAGE \ UJ F
2 w w Z
VACANT LOT T
LOT APPROXIMATE a p W N
AREA OF FORMER W O a � m
TRACT 4 GRAVEL/GRASS LOT RESIDENCE LLI m z 6 O
VACANT ±0.33 ACRES FORMERLY USED FOR O Y
LOT BOAT STORAGE }r! N = , a
r �vo3
ClCj
C!'TWrAI CKADTY 2 N N 2
m
SMITH
WESTO
UNKNOWN +
OFFICES
7 BUY
sy
�L #
� I r
r BURKE GUITARS
RESIDENTIAL BROTHER'S'
ti HARDWARE Y.
TRACT 1
E ±0.46 ACRES Mw-4 O goo-
loop SUBJECT SITE
±3.05 ACRES m 8
MW-5� ♦ 00 AMERICAN WOODYAR r J
(TARLTON PROPERTY LUST) J
o v
s` >_
CAROLINA KETTLE'; N Po
FOR JEAN'S STARFLITE)' i y >
REEF SPORTS
(FORM ER'FAIRGROUNDS N'3
BEVERAGE)"y AMERICAN L_ a u
z
*� WOODYARDS
x ROPO L a, u
aJ w v
b-0p`li
W
';-�'#e-'�6�• GRAPHIC SCALE
0 35 70 41' i P
3ARGAIN ti
ZNITURE ILA
RE
1 inch = 70 ft.

KtJIUtN I IAL
�ORCPS S�R'p-`
t
ki
c �
UNKNOWN
OFFICES
RESIDENTIAL
VACANT
LOT
TW-8 05/12/23
RESULTS mg/kg
ARSENIC 85.:
HEX CR
TRACT 6
±0.35 ACRI
TW-7 05/12/23
RESULTS mg/kg
ARSENIC 17.7* 6
HEX CR 0.507
TRACTS
±0.35 ACRES
TW-9NP-9n
V�
Q
�G
`2
G�
NOW SMITH HAR T
& GARDEN t
(FORMER
WESTOVERCITGO) k
w T .
%L
TRACT 7
±0.23 ACRES
TW-9 05/12/23
►CT 4 RESULTS mg/U
ACRES ARSENIC 116*
HEX CR 0.921
TW-10NP-10
TRACT 8 `
±0.40 ACRES
TW-4 05/11/23
\
AO
RESULTS
mg/kg
G
Ty
BENZO(A)ANTHRACENE
0.402
BENZO(A)PYRENE
0.261
OF,y
ARSENIC
77.5*
TFF,
Of,
HEX CR
0.838
ELF
TW-5 05/11/23
RESULTS mg/kg
-,
ARSENIC 5.44*
HEX CR 1.22
TW-3 05/11/23 /
RESULTS mg/kg
ARSENIC 10.3* r
HEX CR 0.545 J
1111111111111117 IHEX CR 0.404
TW 10 05/12/23
RESULTS mg/kg TW-2NP-2
ARSENIC TRACT 2
±0.58 ACRES
TRACT 3 \ 0
±0.35 ACRES
LEGEND
RESULT SOIL SAMPLE RESULT EXCEEDING PROTECTION OF GROUNDWATER PSRG
RESULT SOIL SAMPLE RESULT EXCEEDING RESIDENTIAL PSRG
RESULT* SOIL SAMPLE RESULT EXCEEDING INDUSTRIAL/COMMERCIAL PSRG
DO SOIL SAMPLE LOCATIONS
® WATER SUPPLY WELL LOCATION
W TRANSFORMER LOCATION
NOTES:
1.) LOCATIONS AND SIZES ARE APPROXIMATE AND NOT EXACT.
2.) HEX CR - HEXAVALENT CHROMIUM
3.) mg/kg - MILLIGRAMS PER KILOGRAM
4.) PSRG - NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY INACTIVE HAZARDOUS SITES
PRELIMINARY SOIL REMEDIATION GOALS (JANUARY 2023)
8.77*
TW-1 05/11/23
RESULTS mg/kg
ARSENIC 4.03*
HEX CR 1.79
NP-1
VGH S,�REE /
N\��SBORp.
\ Krrr
rFR nMER F. JNDS
/ 3EVERAGE)
NC STATE FAIRGROUNDS
PARKING LOT
N
O
M
o Co O
w N
a
02
N N
Q Lu
N U
LU Z
Lu 0
N Lu
aw
2 U
a X
Lu
W
m w
W
V) 2 w w Z
a =p w H
H.2a�z
yWjm000
u
Im J < p 1
a
�4o�
_ C4
16Lz��
�v oo-
O�"�<
TRACT 1 Wof
±0.46 ACRES O
m�
J
J
SUBJECT SITE _
±3.05 ACRES
W �
O o
qW
T/ V1 P
` V
P �
L • ro N 'Fj
z 3
CAROLINA KETTLE v u
(FORMER JEAN'S STARFLITE)
LL
GRAPHIC SCALE Lu
Y
0 25 50 / 100
1 inch = 50 Ft. ,,

IU
t
1
VACANT
LOT
SEPTIC TANK TRACT 7
AREA ±0.23 ACRI
SHED -
0
,I$O
RESIDENCE
TW-8NP-8 /
(78.72)
/±nO�l
ACT 6
.35 ACRE
GARAGE
❑i
O Z
q
TRACTS
±0.35 ACRES
/ RESIDENCE
00
TW-9/VP-9@
(80.24)
1�
7
O
�L
�2
SMITH HARDWAR
& GARDEN
(FORMER
WESTOVERCITGO)
UNKNOWN' �.
OFFICES _ �!
� T .
►CT 4
ACRES
CO TW-
(810NP-101.38)I \
ELECTRICAL 0
COMPANY RIA MATEL w
STORAGE ARE ELSE RP
E�EG"� p\PNy
\� of �-c5
o
PARKING
LOT
TRACT 8 \
±0.40 ACRES
O A
/�9 0 O T
G
TW-4NP-4 /Y
(79.43) Fi(,T
0
/a00 O,F�G
F
GRAVEL/GRASS LOT
FORMERLY USED FOR
BOATSTORAGE
(82.54)
OTW-3/V
VACANTLOT
0
0
M
00
�q—,\\=—.82
C,PG-
,�O 1�1 k)v O�Nt� C---
TRACT 3
±0.35 ACRES
VSBO&GN S�R�E� 0?
GRAVEL/GRASS LOT
FORMERLY USED FOR
BOATSTORAGE
NC STATE FAIRGROUNDS
PARKING LOT
LEGEND
(82.23) MEASURED GROUNDWATER ELEVATION
i — -, GROUNDWATER CONTOUR LINE
--APPROXIMATE GROUNDWATER FLOW DIRECTION
QO PHASE II ESA SAMPLE LOCATIONS
® WATER SUPPLY WELL LOCATION
TRANSFORMER LOCATIONS
NOTES:
1.) LOCATIONS AND SIZES ARE APPROXIMATE AND NOT EXACT.
GRAVEL/GRASS LOT
FORMERLY USED FOR
— BOATSTORAGE
83.00
TW-6/VP-6
(83.31)
APPROXIMATE
AREA OF FORMER
RESIDENCE
/ g4.00
TRACT 1
TW-1NP-1 ±0.46 ACRES
(84.15)
/ EMPTY
GATE
TW-2NP-2 HOUSE
n (83.60) TRACT 2
/ ±0.58 ACRES
0
❑�
REEF SPORTS
(FORMER FAIRGROUNDS
BEVERAGE)
4
SUBJECT SITE
±3.05 ACRES
N
O
O z Co
Z ~ Co
c N
0
LL a
Lu
>I—
o r1
zQ
::)2
O�
�7 O
CN Z
LLI p
- U
LLI
V)
Q
m
W
lin �
W
(A2 w w Z
w
W-z
LLIH 0 a N �
W mz.2ou
OC O w
N 04
= C 4 04 =
' ,z a
OW 0 J
p O 04
0 N ul
mg
2
C W
W\
v o
Vi T 0
v
— a v
ro
LL v —
Nrq N
L 3
z
L v v—
a
c >�
L� 'ao
CAROLINA KETTLE
o LL
(FORMER JEAN'S STARFLITE)
0 �u
L v
GRAPHIC SCALE /
_
0 25 50 100
2 u
inch Ft. MERI
,,
1 = 50

RESIDENTIAL /
C
OORCPS S�RG�
IIIDENTIAL
Aor
UNKNOWN
OFFICES
RESIDENTIAL
❑A
0 TRACT 8�
±0.40 ACRES
TW-8/V
TRACT 6
±0.35 ACRI
TRACT 5
VACANT ±0.35 ACRES
LOT
VACANT
TW-9NP-9@p
TRACT 4
±0.33 ACRES
TRACT 7
±0.23 ACRES X@TW-4NP-4
0 TW-10NP-10
7
71 �
t
7rG
SMITH HARDWARE \
& GARDEN
(FORMER
WESTOVER CITGO)
do
i�
OTW-3/V
TRACT 2
±0.58 ACRES
TRACT 3 \ 0
±0.35 ACRES
�SBOROVGN
N��
REEF SPORTS
(FORMER FAIRGROUNDS
BEVERAGE)
LEGEND
N
O
RESULT GROUNDWATER SAMPLE RESULT EXCEEDING NC 2L STANDARD
d Lo
z
z
c
M
V N
QO GROUNDWATER SAMPLE LOCATION
0
a
® WATER SUPPLY WELL LOCATION
0
o
Ln
❑j TRANSFORMER LOCATION
11
a
Ll� N
o 10
0
NOTES:
1.) LOCATIONS AND SIZES ARE APPROXIMATE AND NOT EXACT.
'm
2.) ug/L -MICROGRAMS PER LITER
Z a
Q
> �
3.) NC 2L STANDARD - NORTH CAROLINA GROUNDWATER QUALITY STANDARD AS PER NC
¢
o
ADMINISTRATIVE CODE 15A NCAC 02L
o
a
4.)NAPHTH-NAPHTHALENE
5.) 1,2-DCA - 1,2-DICHLOROETHANE
6.) VOC - VOLATILE ORGANIC COMPOUND
7.) SVOC - SEMI -VOLATILE ORGANIC COMPOUND
LLJ
Q
d
in
Q
z�
N
LLJ
Ou
in� Z
NC STATE FAIRGROUNDS 0 Q
(n LU
W W
— u
LU LU
Ln
Q
d
W
mW
W �
N 2 w w Z
a m w
I-0QNZ)
W LLI mQU0
J Q o w
~=¢CC7°a
=�vo3
�oa��
O O w
04 � 5
O O
m N
/
SUBJECT SITE
±3.05 ACRES
J
_
N
C;'q
v
\ a o
N u
V v
W
°
A I
V � JO N
°
^L z 3
CAROLINA KETTLE
v
(FORMER JEAN'S STARFLITE)
bA ° LL
w Y v
GRAPHIC SCALE
0 25 50 100
`` �
inch ft.
1 = 50
J[NAF"FRI

t
�p.5 Cl
RESIDENTIAL
UNKNOWN
OFFICES
VACANT
LOT
SMITH HARDWAR�
Ilft
& GARDEN
(FORMER
WESTOVERCITGO)
w T .
❑�
�SBOROVGN Soo,
N��
REEF SPORTS
(FORMER FAIRGROUNDS
BEVERAGE)
LEGEND
RESULT SOIL VAPOR RESULT EXCEEDING RESIDENTIAL SGSL
QO SOIL SAMPLE LOCATION
® WATER SUPPLY WELL LOCATION
❑j TRANSFORMER LOCATION
NOTES:
1.) LOCATIONS AND SIZES ARE APPROXIMATE AND NOT EXACT.
2.) ug/m3 - MICROGRAMS PER CUBIC METER
3.) SGSL - NCDEQ SOIL GAS SCREENING LEVEL (JANUARY 2023)
NC STATE FAIRGROUNDS
PARKING LOT
N
O
`D z Co
Z ~ Cl)
c N
0
LL a
o NN
Ln
n o
- a- Ci N
u o 0
O
m
Z Q O
a
o a
aa
>�
J_ N
O Lu
N U
Qz
W 0
Lu
Lu
LLI U
U-)
Q W
d
W
m �
W
IA 2 w w Z
w
Ow��-
HLLI C >> z
W mzuo
f� p w
(A 0
_ 04
L
W m J
c,
OO 04
O
= N u
mg
IA
J
SUBJECT SITE _
±3.05 ACRES
v
a o
Vi T 0
N
— �
• V
N
L a+ >
� N
^L
Z 333
3
W
i m
v—
CAROLINA KETTLE
(FORMER JEAN'S STARFLITE)
bA ° LL
C
GRAPHIC SCALE w Y
inch = 50 Ft.
100
MERI
VvTrm

TABLES

Table 1
Summary of Soil Analytical Results
Hillsborough Street Assemblage
WR Project Number: 23-0302
5200 Hillsborough Street
Raleigh, Wake County, North Carolina
Client Sample ID
Protection of
Groundwater
PSRG
(mg/kg)
Residential
Health Based
PSRG
(mg/kg)
Industrial/
Commercial
Health Based
PSRG
m /k
TW-1
TW-2
TW-3
TW-4
TW-5
TW-6
DUP
TW-7
TW-8
TW-9
TW-10
Sample Interval (Feet)
(5-7.5)
(5-7.5 )
(5-7.5)
(5-7.5)
(5-7.5)
(5-7.5)
(5-7.5)
(5-7.5)
(5-7.5)
(5-7.5)
(5-7.5)
Collection Date
5/11/2023
5/11/2023
5/11/2023
5/11/2023
5/11/2023
5/11/2023
5/11/2023
5/12/2023
5/12/2023
5/12/2023
5/12/2023
Method Parameter CAS #
(mg/kg) TQal
(mg/kg) Qual
(mg/kg) Qual
(mg/kg) Qual
(mg/kg) Qual
(mg/kg) Qual
(mg/kg) Qual
(mg/kg) Qual
(mg/kg) Qual
(mg/kg) Qual
(mg/kg) Qual
Volatile Organic Compounds (VOCs)
8260D
tert-Butyl benzene 98-06-6
3.1
11 1600
23000
BDL
BDL BDL
BDL
BDL
0.00371 J
BDL
BDL
BDL
8260D
8270E
Remaining Targeted VOCs
Semi-VOCs (SVOCs)
Acenaphthene 83-32-9
16
-
720
-
9000
BDL
BDL
BDL BDL
BDL BDL
L
0.0105
J
BDL BDL
BDL
BDL
4DL
BDL
BDL
BDL
BDL
BDL
BDL
8270E
Anthracene
120-12-7
1300
3600
45000
BDL
BDL
BDL
0.0649
BDL
BDL
BDL
8270E
Benzo[a]anthracene
56-55-3
0.35
1.1
21
BDL
BDL
BDL
0.402
0.0114
J
BDL
BDL
BDL
8270E
Benzo[a]pyrene
50-32-8
0.12
0.11
2.1
BDL
0.261
0.00924
J
BDL
8270E
Benzo[b]fluoranthene
205-99-2
1.2
1.1
21
BDL
BDL
0.335
0.0127
J
BDL
BDL
BDL
8270E
Benzo[g,hJ]perylene
191-24-2
NL
NL
NL
BDL
0.101
BD
BDL
BDL
BDL
8270E
Benzo[k]fluoranthene
207-08-9
12
11
210
5UL
BDL
BDL
0.127
BDL
BDL
BDL
BDL
8270E
Chrysene
218-01-9
36
110
2100
BDL
BDL
BDL
0.344
BDL
BDL
BDL
BDL
8270E
Dibenz(a,h)anthracene
53-70-3
0.38
0.11
2.1
BDL
BDL
BDL
0.0301
J
BD'
BDL
BDL
BDL
8270E
Fluoranthene
206-44-0
670
480
6000
0.759
0.0186
J
BDL
8270E
Fluorene
86-73-7
110
480
6000
BDL
0.0112
J
BDL
8270E
Indeno[1,2,3-cd]pyrene
193-39-5
3.9
1.1
21
BDL
BDL
0.111
BDL
BDL
BDL
8270E
Phenanthrene
85-01-8
NL
NL
NL
BDL
BDL
0.202
0.00795
J
BDL
BDL
BDL
8270E
Pyrene
129-00-0
440
360
4500
BDL
BDL
0.734
0.0182
J
BDL
BDL
BDL
8270E
Remaining Targeted SVOCs
-
-
-
BDL
BDL
BDL
BDL
BDL
Metals
6020B
Arsenic
7440-38-2
5.8
0.68
3
4.03
5.17
10.3
77.5
5.44
8.77
7.77
17.7
85.5
1
116
12.1
6020B
Barium
7440-39-3
580
3100
47000
13.4
10.7
28.7
17.5
20.3
17.8
18.1
30.5
26.8
17.8
11.6
6020B
Cadmium
7440-43-9
3
1.4
20
6020B
Chromium (Total)
7440-47-3
NL
NL
NL
15
17.7
33.2
15.2
20.1
52.6
52.6
36.8
41.8
27.8
16.2
7199
Chromium (Hexavalent)
18540-29-9
3.8
0.31
6.5
1.79
0.404
J
0.545
J
0.838
J
1.22
J
0.843
J
0.689
J
0.507
J, P1
1.81
0.921
J
CALC
Chromium(Trivalent- Calculation)
16065-83-1
360000
23000
350000
13.21
17.296
32.655
14.362
18.88
51.757
51.911
36.293
39.99
26.879
16.2
6020E
Lead
7439-92-1
270
400
800
11.3
5.24
26.3
10.2
6.99
11.2
11.6
16.3
11.7
12.9
9.56
6020B
Selenium
7782-49-2
2.1
78
1200
0.73
J
0.647
J
1.19
J
0.579
J
0.698
J
1.56
J
1.49
J
2.02
J
1.46
J
0.978
J
0.843
J
6020B
Silver
7440-22-4
3.4
78
1200
7471B
Mercury
7439-97-6
1 NL
1 4.7
1 70
1
1
1
0.179
0.0271
J
0.041
J
0.0719
0.083
Notes
Results are compared to NCDEQ's Inactive Hazardous Sites Preliminary Soil Remediation Goals (PSRGs) table (January 2023)
Value = Reportable concentration detected
Value = Reportable Concentration was detected above Protection of Groundwater PSRG only
Value = Reportable Concentration was detected above Residential Health Based PSRG
Value = Reportable Concentration was detected above Industrial/ Commercial Health Based PSRG
Qual: J = The identification of the analyte is acceptable; the reported value is an estimate.
P1 = Relative Percent Difference value not applicable for sample concentrations less than 5 times the reporting limit.
BDL Below Detection Limits
NA Not Analyzed
NL Not Listed
mg/kg Milligrams per Kilogram
Page 1 of 1

Table 2A
Temporary Monitoring Well Construction Information
Hillsborough Street Assemblage
WR Project Number: 23-0302
5200 Hillsborough Street
Raleigh, Wake County, North Carolina
Well ID
Date Installed
Well
Casing
Diameter
(inches)
Total
Depth
feet
()
Screened
Interval
(feet)
Top -of-
Casing
Elevation
(feet)
Date Water
Level
Measured
Depth -to -Water
from
Top -of -Casing
(feet)
LNAPL
Thickness
(feet)
Groundwater
Elevation
(feet)
TW-1
5/11/2023
1
25.0
15-25
101.46
5/22/2023
17.31
84.15
TW-2
5/11/2023
1
25.0
15-25
101.21
5/22/2023
17.61
83.60
TW-3
5/11/2023
1
25.0
15-25
100.64
5/22/2023
18.10
82.54
TW-4
5/11/2023
1
22.0
12-22
95.95
5/22/2023
16.52
79.43
TW-5
5/11/2023
1
25.0
15-25
100.00
5/22/2023
17.77
82.23
TW-6
5/11/2023
1
25.0
15-25
100.63
5/22/2023
17.32
83.31
TW-7
5/12/2023
1
25.0
15-25
99.13
5/22/2023
21.06
78.07
TW-8
5/12/2023
1
25.0
15-25
95.75
5/22/2023
17.03
78.72
TW-9
5/12/2023
1
27.0
17-27
99.57
5/22/2023
19.33
80.24
TW-10
5/12/2023
1
26.0
16-26
99.81
5/22/2023
18.43
81.38
Notes:
1.) All wells identified in this table are temporary groundwater monitoring wells.
2.) Top -of -Casing elevations measured with a laser level, relative to an arbitrary benchmark of 100 feet above mean sea level.
3.) Groundwater elevation calculated by: (Top -of -Casing - Depth -to -Water) + (Free Product Thickness x 0.8581)
4.) LNAPL = Light Non -Aqueous Phase Liquid

Table 2B
Summary Of Groundwater Analytical Results
Hillsborough Street Assemblage
WR Project Number: 23-0302
5200 Hillsborough Street
Raleigh, Wake County, North Carolina
Analytical Method
6200B - Volatile Organic Compounds (VOCs)
625.1 - Semi -Volatile Organic Compounds (SVOCs)
7470A/602013/7199 - Metals
c
0
L
N
N
N
c
c
C
Y
O
N
O
IC6
;0
N
O
N
jL
Sample
Date
O
N
N
O
ID
Collected
o
C
T
w
r
T
J-
o
o
C
T
T
E
E
T
C
c
J
a
Z
C
Z
C
c
N
i�
U
E
J
f6
E
J
X
N
N
N
J
J
m
0
O
U
>.
O
O.
O
.�.
J
L_
Y
N m
LU
�. 0]
L
.L...
L
O
N
N
N
J
~
~
x
a
O
j.
,C
tO N
U
>.
L
t6
OJ
.L...
L
l6
C
,C
N U
J
`
'C
E
J
E
U
>
16
-O
C
N
=
N
m
L
N
L
p
N
m
N~
N
a
O
N
M
4'S
X
N O
C
N
N
L
N O
N
N
N
O
N
N
0]
C
uJ
U
W
N
a
N
Z
C
_
H
E
O
R
LL
Z
0_
R' U1
Q
m
U
H
2
J
(n
(n
1634-04-
1330-20-
7439-97-
7440-38-
7440-39-
7440-43-
7440-47-
1854-02-
7439-92-
-
778249-
--
744022
591-78-6
71-43-2
104-51-8
135-98-8
67-66-3
107-06-2
100-41-4
98 -82-8
99-87-6
78-93-3
108-10-1
91-20-3
103-65-1
79-34-5
108-88-3
95-63-6
108-67-8
95-47-6
---
84-74-2
84-66-2
206-44-0
91-20-3
85-01-8
---
6
2
3
1
2
TWA
5/11/2023
ND
ND
ND
ND
ND
ND
ND
ND
JD
ND
ND
ND
ND
ND
ND
ND
1.28
ND
11.3
43.9
ND
ND
ND
1.61
1.2
ND
TW-2
5/11/2023
32.2
23
16.4
3.06
2.15
10.5
171
12.1
7.64
13.5
9.25
2
19.2
42.5
JD
407
295
121
200
ND
IN
5.13
Nf
-
0.212
42.7
ND
ND
ND
1.25
0.871
IN
TW-3
5/11/2023
ND
ND
ND
ND
ND
1.22
0.218
JD
ND
ND
ND
ND
ND
ND
ND
1
0.121
N1
0.251
ND
JD
ND
21.8
JD
ND
ND
Nn
0.397
ND
TW-4
5/11/2023
D
ND
ND
ND
ND
ND
N
NI
iqL
ND
ND
D
ID
JD
ND
ND
ND
ND
ND
ND
0.658
1.29
NI
N[
NG
ND
0.156
0.779
62.6
JD
ND
0.215
1.65
2.12
ND
TW-5
5/11/2023
D
ND
ND
ND
ND
ND
ND
NI
NL
ND
ND
JD
ID
ND
ND
ND
ND
ND
ND
0.736
3.81
NI
N[
ND
ND
JD
ND
45.6
JD
ND
ND
0.998
4.31
ND
TW-6
5/11/2023
D
ND
6.55
1.06
ND
ND
ND
NI
2.21
NL
ND
ND
JD
ID
0.169
ND
0.722
0.251
ND
4.43dND
INND
ND
NI
N[
ND
ND
JD
0.186
20.4
JD
ND
ND
1.02
0.331
ND
DUP
5/11/2023
D
ND
7.73
1.16
ND
ND
ND
NI
2.48
NL
ND
ND
JD
ID
.J
ND
0.761
0.82
ND
4.97IN0.963
4.22
NI
N[
ND
ND
JD
ND
18.5
JD
ND
ND
ND
0.349
ND
TW-7
5/12/2023
0.942
ND
ND
ND
ND
ND
N[
NI
VD
JD
JD
ND
ND
ND
ND
ND
INND
2.52
NI
ND
ND
JD
17.4
JD
ND
ND
ND
ND
ND
TW-8
5/12/2023
ND
ND
ND
ND
ND
ND
N[
NI
ND
JD
JD
ND
ND
ND
ND
ND
ND
3.41
NI
ND
ND
JD
96.1
JD
ND
ND
ND
ND
ND
TW-9
5/12/2023
ND
ND
ND
ND
ND
ND
N[
NI
ND
JD
JD
ND
ND
ND
ND
ND
1.1
0.966
NI
ND
ND
JD
0.441
182
JD
ND
ND
1.08
0.318
ND
TW-10
5/12/2023
Nn
Nn
Nn
Nn
Nn
Nn
n'
"
lJ
0.133
n
Nn
Nn
Nn
Nn
Nn
2.13
"
Nr
IF
0.187
107
0.36
Nn
ND
1.97
ND
Nn
INC 2L Standard
40
1
70
70
70
0.4
600
70
25
4000
100
20
6
70
0.2
600
400
400
500
500
NA
700
6000
300
6
200
NA
1
10
700
2
10
NIL
15
20
20
GCLs for
C�ftdvvater
40000
5000
5900
8800
70000
400
80000
30500
11700
4000000
100000
20000
6000
26100
200
260000
28500
24100
50000
50000
NA
NIL
NIL
300
6000
550
NA
NL
NL
700000
NIL
10000
NL
15000
NIL
20000
Notes:
1.) All results provided in ug/L (micrograms per liter) or parts per billion
2.) Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents.
3.) NC 2L Standard - North Carolina Groundwater Quality Standard as per INC Administrative Code 15A NCAC 02L
4.) GCLs for Groundwater = NCDENR UST Section Gross Contamination Levels for Groundwater
NA = Not Applicable.
NO = Compound Not Detected.
Result = Result Exceeds Laboratory Detection Limits
= Result Exceeds 2L Standard
Result = Result Exceeds GCL Value
Page 1 of 1

Table 3
Summary of Soil Vapor Results (VOCs - Detections only)
Hillsborough Street Assemblage
WR Project Number: 23-0302
5200 Hillsborough Street
Raleigh, Wake County, North Carolina
Analytical
Method
TO-15
- Volatile
Organic Compounds (VOCs)
00
V
V7
O
N
M
(o
(o
^
7
N
lf')
O
M
V
V
co
(D
W
ap
O
�
00
00
00
0
00
V
OO
O
aA
O
L6
LID
LID
�
lf)
O
M
CA
00
T
Il
O
O,It
N
M
00
O
00
O
O
O
00 O
O
V
,�j
00
00
C0
O
N
00
O
O
,�j
I�
�
(9
(9
�
n
(4
LID
n
co
O
O
(0
CA
Sample
Date
N
O
N
N
ID
Collected
aC
i
@
c
aa))
ate)
°)
o
a
a)
L
U
C
E
Y
41
N
O`
C
N
C
N
�
O
Y
y
t
O
0
O
-6
p
(6
a)
O
O
O
OCD
a)
a)
N
a)
E
E
U
O
C
C
a
T
a)0
C
a) Y
O
L
F
O
O
-C
O
U
00
>.
x
0:
L
F
F
O
a)
>.
c
O
2
a3
L
L
N
X
7 T
m L
O
t
U
V
N
Q
m
L
V
a)
7
@
5.
L
x
E
7
n
2
L
W
L6
CM
V
N
JL
LL
W
U
Q
U
N
a)
00
2
i-
V
O
F
F
W
E
O
U
0-
V
VP-1
5/22/2023
ND
ND
1.2
12
ND
ND
ND
Nf
1.5
ND
0.96
18
2.3
3.7
16
16
1
2
9.9
1.7
27
VP-2
5/22/2023
ND
ND
ND
ND
ND
ND
ND
15
ND
6.4
ND
ND
ND
N
13
ND
ND
ND
ND
ND
ND
VP-3
5/22/2023
ND
1.1
ND
120
ND
ND
ND
19
4.5
ND
ND
ND
ND
ND
1.9
-
ND
ND
4.4
3.9
ND
ND
4.7
5.4
7.9
VP-4
5/22/2023
12
ND
N-
Nn
58
38
ND
16
ND
1.5
ND
43
7.8
11
ND
4.3
80
1.4
31
160
33
8.5
13
55
28
66
VP-5
5/22/2023
ND
1.2
100
ND
ND
ND
ND
1.5
ND
ND
ND
ND
ND
ND
ND
51
ND
ND
ND
ND
ND
ND
ND
VP-6
5/22/2023
AD
ND
1.1
57
20
ND
ND
ND
ND
2.1
ND
40
1.4
ND
ND
ND
ND
7.8
3.3
8.3
4
ND
1.1
2.8
ND
3.3
VP-7
5/22/2023
ND
0.65
1.4
48
190
ND
3.7
ND
ND
1.1
7.9
70
1.1
ND
ND
ND
ND
1.9
1.3
1 3.3
3.8
ND
ND
ND
ND
2
VP-8
5/22/2023
ND
ND
1.2
ND
15
ND
ND
ND
ND
1.8
'ID
0.63
ND
ND
ND
15
3.9
15
120
55
3.5
4.9
35
7.6
47
VP-9
5/22/2023
ND
ND
D
ND
ND
ND
ND
220
5.3
24
ND
ND
120
6.7
290
110
19
100
87
210
DUP
5/22/2023
NO
ND
ND
Nv
160
ND
ND
ND
ND
160
4.4
22
ND
ND
100
ND
38
240
100
Iv
17
88
80
190
VP-10
J 5/22/2023
' ­
"'n
1.3
'In
20
"in
"in
"in
"'
6.1
18
1 12
"'n
1.2
"'n
170
17
53
200
91
8.7
18
69
37
79
Residential SGSL
700
5.6
NL
NL
NL
4900
3400
1 4900
1 35000
4.1
42000
NL
12
2800
13.9
210001
35000
278
37.4
700
700
2800
7000
NL
420
420
Non -Residential SGSL
8800
278
NL
NL
61000
52000
61000
438000
53.3
530000
NL
160
35000
175
260000
440000
3500
490
1 8800
8800
1 35000
1 88000
1 NL
5200
5200
Notes:
1.) All results are provided in Ng/m3 (micrograms per cubic meter)
2.) Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents.
3.) Results are compared to NCDEQ's Soil Gas Screening Levels (SGSLs) table (January 2023).
= Not Detected by Laboratory
Result
= Result Exceeds Laboratory Detection Limits
Result
= Result Exceeds Residential SGSL
Result
= Result Exceeds Non -Residential SGSL
Page 1 of 1

APPENDIX A
Boring Logs

;!WithersRavenel
Engineers I Planners I Survey-rs
SOIL BORING LOG
Boring # TW-1 & VP-1 Job Name Hillsborough Street Assemblage Job # 23-0302
Date 05/11/2023 Site Loc. Raleigh, NC Easting NA
WR Rep AP/SW Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
0
1
Gravel
0
5
0
NR
1
4
Brown/red silty clay, dry, no odor
5
7.5
0
NR
4
9
Red/tan clayey silt, dry, no odor
7.5
10
0
NR
9
25
Multi -color silt, dry to moist with depth, no odor
10
12.5
0
NR
12.5
15
0
NR
Moist soil encountered at approximately 17 feet BLS
15
17.5
0
N R
Temporary monitoring well (TW-1) installed in initial soil boring as follows:
17.5
20
0
N R
25 feet total depth of boring
10 feet of 1-inch 010 slot size PVC screen from base of boring
15 feet of 1-inch sch40 PVC riser to surface
11 feet of #2 sand surrounding screen from boring's base
Bentonite from top of sand to grade
Soil vapor sampling point (VP-1) installed adjacent to temporary well as follows:
6 feet total depth of boring
One foot of sand poured into base of boring
6-inch mesh screen filter on top of foot of sand
Teflon tubing connected on top of screen to grade
Additional one foot of sand poured around screen and tubing
Bentonite from top of sand to grade
Bentonite hydrated to create seal
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unified Soil Classification System
TOC=Top of Casing
VOCs=Volatile Organic Compounds
PID=Photoionization Detector
SVOCs=Semi-VOCs
FID=Flame Ionization Detector
RCRA=Resource Conservation and Recovery Act
EI=Elevation
Hex Cr—Hexavalent Chromium
115 MacKenan Drive, Cary, North Carolina 27511 tel:[phone] fox:919.467.6008 www.withersrovenel.com

;!WithersRavenel
Engineers I Planners I Survey-rs
SOIL BORING LOG
Boring # TW-2 & VP-2 Job Name Hillsborough Street Assemblage Job # 23-0302
Date 05/11/2023 Site Loc. Raleigh, NC Easting NA
WR Rep AP/SW Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
0
0.5
Gravel
0
2.5
0
NR
0.5
7
Red/Brown silty clay, dry, no odor
2.5
5
0
NR
7
20
Multi -color silt, dry to moist with depth, no odor
5
7.5
0
NR
7.5
10
0
NR
10
12.5
0
NR
Moist soil encountered at approximately 17 feet BLS
12.5
15
0
NR
Temporary monitoring well (TW-2) installed in initial soil boring as follows:
25 feet total depth of boring
10 feet of 1-inch 010 slot size PVC screen from base of boring
15 feet of 1-inch sch40 PVC riser to surface
11 feet of #2 sand surrounding screen from boring's base
Bentonite from top of sand to grade
Soil vapor sampling point (VP-2) installed adjacent to temporary well as follows:
6 feet total depth of boring
One foot of sand poured into base of boring
6-inch mesh screen filter on top of foot of sand
Teflon tubing connected on top of screen to grade
Additional one foot of sand poured around screen and tubing
Bentonite from top of sand to grade
Bentonite hydrated to create seal
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unified Soil Classification System
TOC=Top of Casing
VOCs=Volatile Organic Compounds
PID=Photoionization Detector
SVOCs=Semi-VOCs
FID=Flame Ionization Detector
RCRA=Resource Conservation and Recovery Act
EI=Elevation
Hex Cr—Hezavalent Chromium
115 MacKenan Drive, Cary, North Carolina 27511 tel:[phone] fox:919.467.6008 www.withersrovenel.com

;!WithersRavenel
Engineers I Planners I Survey-rs
SOIL BORING LOG
Boring # TW-3 & VP-3 Job Name Hillsborough Street Assemblage Job # 23-0302
Date 05/11/2023 Site Loc. Raleigh, NC Easting NA
WR Rep AP/SW Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
0
5
Red/Brown with some black soil, clayey silt, dry, no odor
0
2.5
0
NR
5
20
deep black and brown clayey silt, dry to moist with depth, no odor
2.5
5
0
NR
IM[5—
7.5
0
NR
7.5
10
0
NR
10
12.5
0
NR
Moist soil encountered at approximately 17 feet BLS
12.5
15
0
NR
Temporary monitoring well (TW-3) installed in initial soil boring as follows:
15
17.5
0
NR
25 feet total depth of boring
10 feet of 1-inch 010 slot size PVC screen from base of boring
17.5
20
0
N R
15 feet of 1-inch sch40 PVC riser to surface
11 feet of #2 sand surrounding screen from boring's base
20
22.5
0
N R
Bentonite from top of sand to grade
22.5
25
0
NR
Soil vapor sampling point (VP-3) installed adjacent to temporary well as follows:
6 feet total depth of boring
One foot of sand poured into base of boring
6-inch mesh screen filter on top of foot of sand
Teflon tubing connected on top of screen to grade
Additional one foot of sand poured around screen and tubing
Bentonite from top of sand to grade
Bentonite hydrated to create seal
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unified Soil Classification System
TOC=Top of Casing
VOCs=Volatile Organic Compounds
PID=Photoionization Detector
SVOCs=Semi-VOCs
FID=Flame Ionization Detector
RCRA=Resource Conservation and Recovery Act
EI=Elevation
Hex Cr—Hezavalent Chromium
115 MacKenan Drive, Cary, North Carolina 27511 tel:[phone] fox:919.467.6008 www.withersrovenel.com

;!WithersRavenel
Engineers I Planners I Surveyors
SOIL BORING LOG
Boring # TW-4 & VP-4 Job Name Hillsborough Street Assemblage Job # 23-0302
Date 05/11/2023 Site Loc. Raleigh, NC Easting NA
WR Rep AP/SW Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
0
5
Brown, sand, dry, no odor
0
5
0
NR
5
7
Red/brown, silty clay, dry, no odor
5
7.5
1.1
NR
7
20
Red/brown, clayey silt, dry to moist with depth, no odor
7.5
10
1.5
NR
10
12.5
1.6
NR
12.5
15
1.4
NR
Moist soil encountered at approximately 17 feet BLS
15
17.5
1.2
NR
Temporary monitoring well (TW-4) installed in initial soil boring as follows:
17.5
20
0
N R
22 feet total depth of boring
10 feet of 1-inch 010 slot size PVC screen from base of boring
12 feet of 1-inch sch40 PVC riser to surface
11 feet of #2 sand surrounding screen from boring's base
Bentonite from top of sand to grade
Soil vapor sampling point (VP-4) installed adjacent to temporary well as follows:
6 feet total depth of boring
One foot of sand poured into base of boring
6-inch mesh screen filter on top of foot of sand
Teflon tubing connected on top of screen to grade
Additional one foot of sand poured around screen and tubing
Bentonite from top of sand to grade
Bentonite hydrated to create seal
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unified Soil Classification System
TOC=Top of Casing
VOCs=Volatile Organic Compounds
PID=Photoionization Detector
SVOCs=Semi-VOCs
FID=Flame Ionization Detector
RCRA=Resource Conservation and Recovery Act
EI=Elevation
Hex Cr—Hezavalent Chromium
115 MacKenan Drive, Cary, North Carolina 27511 tel:[phone] fox:919.467.6008 www.withersrovenel.com

;!WithersRavenel
Engineers I Planners I Surveyors
SOIL BORING LOG
Boring # TW-5 & VP-5 Job Name Hillsborough Street Assemblage Job # 23-0302
Date 05/11/2023 Site Loc. Raleigh, NC Easting NA
WR Rep AP/SW Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
0
0.5
Gravel
0
5
0.7
NR
0.5
20
Red/brown/tan, silty clay, dry to moist with depth, no odor
5
7.5
0.2
NR
7.5
10
0.4
NR
10
12.5
0.2
NR
12.5
15
0.3
NR
Moist soil encountered at approximately 17 feet BLS
15
17.5
0.3
NR
Temporary monitoring well (TW-5) installed in initial soil boring as follows:
17.5
20
0
NR
25 feet total depth of boring
10 feet of 1-inch 010 slot size PVC screen from base of boring
15 feet of 1-inch sch40 PVC riser to surface
11 feet of #2 sand surrounding screen from boring's base
Bentonite from top of sand to grade
Soil vapor sampling point (VP-5) installed adjacent to temporary well as follows:
6 feet total depth of boring
One foot of sand poured into base of boring
6-inch mesh screen filter on top of foot of sand
Teflon tubing connected on top of screen to grade
Additional one foot of sand poured around screen and tubing
Bentonite from top of sand to grade
Bentonite hydrated to create seal
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unified Soil Classification System
TOC=Top of Casing
VOCs=Volatile Organic Compounds
PID=Photoionization Detector
SVOCs=Semi-VOCs
FID=Flame Ionization Detector
RCRA=Resource Conservation and Recovery Act
EI=Elevation
Hex Cr—Hezavalent Chromium
115 MacKenan Drive, Cary, North Carolina 27511 tel:[phone] fox:919.467.6008 www.withersrovenel.com

;!WithersRavenel
Engineers I Planners I Surveyors
SOIL BORING LOG
Boring # TW-6 & VP-6 Job Name Hillsborough Street Assemblage Job # 23-0302
Date 05/11/2023 Site Loc. Raleigh, NC Easting NA
WR Rep AP/SW Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
0
1
Gravel
0
2.5
0.1
NR
1
19.5
Red/brown, clayey silt, dry, no odor
2.5
5
0
NR
19.5
22.5
Red/brown/white, silt with mica and rocks, moist, petroleum odor
MML5
7.5
0.2
NR
22.5
25
Red/brown/white, silt, moist, no odor
7.5
10
0
NR
10
12.5
0.3
NR
Moist soil encountered at approximately 17 feet BLS
12.5
15
0.1
NR
Temporary monitoring well (TW-6) installed in initial soil boring as follows:
15
17.5
0.1
N R
25 feet total depth of boring
10 feet of 1-inch 010 slot size PVC screen from base of boring
17.5
20
0.8
N R
15 feet of 1-inch sch40 PVC riser to surface
11 feet of #2 sand surrounding screen from boring's base
20
22.5
238
N R
Bentonite from top of sand to grade
22.5
25
0.5
NR
Soil vapor sampling point (VP-6) installed adjacent to temporary well as follows:
6 feet total depth of boring
One foot of sand poured into base of boring
6-inch mesh screen filter on top of foot of sand
Teflon tubing connected on top of screen to grade
Additional one foot of sand poured around screen and tubing
Bentonite from top of sand to grade
Bentonite hydrated to create seal
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unified Soil Classification System
TOC=Top of Casing
VOCs=Volatile Organic Compounds
PID=Photoionization Detector
SVOCs=Semi-VOCs
FID=Flame Ionization Detector
RCRA=Resource Conservation and Recovery Act
EI=Elevation
Hex Cr-Hexavalent Chromium
115 MacKenan Drive, Cary, North Carolina 27511 tel:[phone] fox:919.467.6008 www.withersrovenel.com

;!WithersRavenel
Engineers I Planners I Surveyors
SOIL BORING LOG
Boring # TW-7 & VP-7 Job Name Hillsborough Street Assemblage Job # 23-0302
Date 05/12/2023 Site Loc. Raleigh, NC Easting NA
WR Rep AP/SW Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
0
1
Topsoil
0
2.5
0.3
NR
1
12.5
Red/brown, clayey silt, dry, no odor
2.5
5
0.3
NR
12.5
26
Red/brown, silty clay, dry to moist with depth, no odor
5
7.5
0.1
NR
7.5
10
0
NR
10
12.5
0.2
NR
Moist soil encountered at approximately 20 feet BLS
12.5
15
0
NR
Temporary monitoring well (TW-7) installed in initial soil boring as follows:
15
17.5
0.2
N R
25 feet total depth of boring
10 feet of 1-inch 010 slot size PVC screen from base of boring
17.5
20
0.1
N R
15 feet of 1-inch sch40 PVC riser to surface
11 feet of #2 sand surrounding screen from boring's base
20
23
0
N R
Bentonite from top of sand to grade
23
26
0
NR
Soil vapor sampling point (VP-7) installed adjacent to temporary well as follows:
6 feet total depth of boring
One foot of sand poured into base of boring
6-inch mesh screen filter on top of foot of sand
Teflon tubing connected on top of screen to grade
Additional one foot of sand poured around screen and tubing
Bentonite from top of sand to grade
Bentonite hydrated to create seal
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unified Soil Classification System
TOC=Top of Casing
VOCs=Volatile Organic Compounds
PID=Photoionization Detector
SVOCs=Semi-VOCs
FID=Flame Ionization Detector
RCRA=Resource Conservation and Recovery Act
EI=Elevation
Hex Cr—Hezavalent Chromium
115 MacKenan Drive, Cary, North Carolina 27511 tel:[phone] fox:919.467.6008 www.withersrovenel.com

;!WithersRavenel
Engineers I Planners I Surveyors
SOIL BORING LOG
Boring # TW-8 & VP-8 Job Name Hillsborough Street Assemblage Job # 23-0302
Date 05/12/2023 Site Loc. Raleigh, NC Easting NA
WR Rep AP/SW Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
0
0.5
Topsoil
0
2.5
0
NR
0.5
14
Red/brown, clayey silt, dry, no odor
2.5
5
0
NR
14
18
Red/brown/black, silty clay, dry to moist with depth, no odor
MML5
7.5
0
NR
18
20
Red/brown, silt, moist, no odor
7.5
10
0
NR
10
12.5
0
NR
Moist soil encountered at approximately 17 feet BLS
12.5
15
0
N R
Temporary monitoring well (TW-8) installed in initial soil boring as follows:
15
17.5
0
N R
25 feet total depth of boring
10 feet of 1-inch 010 slot size PVC screen from base of boring
17.5
20
0
N R
15 feet of 1-inch sch40 PVC riser to surface
11 feet of #2 sand surrounding screen from boring's base
Bentonite from top of sand to grade
Soil vapor sampling point (VP-8) installed adjacent to temporary well as follows:
6 feet total depth of boring
One foot of sand poured into base of boring
6-inch mesh screen filter on top of foot of sand
Teflon tubing connected on top of screen to grade
Additional one foot of sand poured around screen and tubing
Bentonite from top of sand to grade
Bentonite hydrated to create seal
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unified Soil Classification System
TOC=Top of Casing
VOCs=Volatile Organic Compounds
PID=Photoionization Detector
SVOCs=Semi-VOCs
FID=Flame Ionization Detector
RCRA=Resource Conservation and Recovery Act
EI=Elevation
Hex Cr-Hexavalent Chromium
115 MacKenan Drive, Cary, North Carolina 27511 tel:[phone] fox:919.467.6008 www.withersrovenel.com

;!WithersRavenel
Engineers I Planners I Surveyors
SOIL BORING LOG
Boring # TW-9 & VP-9 Job Name Hillsborough Street Assemblage Job # 23-0302
Date 05/12/2023 Site Loc. Raleigh, NC Easting NA
WR Rep AP/SW Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
0
1
Topsoil
0
2.5
23.3
NR
1
18
Red/brown/black, clayey silt, dry, no odor
2.5
5
18.7
NR
18
25
Red/brown/black, silt, moist, no odor
5
7.5
33.5
NR
7.5
10
15.2
NR
10
12.5
19.1
NR
Moist soil encountered at approximately 17 feet BLS
12.5
15
2.7
NR
Temporary monitoring well (TW-9) installed in initial soil boring as follows:
15
17.5
41.8
NR
27 feet total depth of boring
10 feet of 1-inch 010 slot size PVC screen from base of boring
17.5
20
6.9
N R
17 feet of 1-inch sch40 PVC riser to surface
11 feet of #2 sand surrounding screen from boring's base
20
22.5
16.7
N R
Bentonite from top of sand to grade
22.5
25
1.4
NR
Soil vapor sampling point (VP-9) installed adjacent to temporary well as follows:
6 feet total depth of boring
One foot of sand poured into base of boring
6-inch mesh screen filter on top of foot of sand
Teflon tubing connected on top of screen to grade
Additional one foot of sand poured around screen and tubing
Bentonite from top of sand to grade
Bentonite hydrated to create seal
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unffied Soil Classification System
TOC=Top of Casing
VOCs=Volatile Organic Compounds
PID=Photoionization Detector
SVOCs=Semi-VOCs
FID=Flame Ionization Detector
RCRA=Resource Conservation and Recovery Act
EI=Elevation
Hex Cr—Hezavalent Chromium
115 MacKenan Drive, Cary, North Carolina 27511 tel:[phone] fox:919.467.6008 www.withersrovenel.com

;!WithersRavenel
Engineers I Planners I Surveyors
SOIL BORING LOG
Boring # TW-10 & VP-10 Job Name Hillsborough Street Assemblage Job # 23-0302
Date 05/12/2023 Site Loc. Raleigh, NC Easting NA
WR Rep AP/SW Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
0
1
Gravel and topsoil
0
2.5
0
NR
1
10
Red/brown/black, clayey silt, dry, no odor
2.5
5
0
NR
10
25
Red/brown, silt, dry to moist with depth, no odor
5
7.5
0
NR
7.5
10
0
NR
10
12.5
0
NR
Moist soil encountered at approximately 18 feet BLS
12.5
15
0
N R
Temporary monitoring well (TW-10) installed in initial soil boring as follows:
15
17.5
0
N R
26 feet total depth of boring
10 feet of 1-inch 010 slot size PVC screen from base of boring
17.5
20
0
N R
16 feet of 1-inch sch40 PVC riser to surface
11 feet of #2 sand surrounding screen from boring's base
20
22.5
0
N R
Bentonite from top of sand to grade
22.5
25
0
NR
Soil vapor sampling point (VP-10) installed adjacent to temporary well as follows:
6 feet total depth of boring
One foot of sand poured into base of boring
6-inch mesh screen filter on top of foot of sand
Teflon tubing connected on top of screen to grade
Additional one foot of sand poured around screen and tubing
Bentonite from top of sand to grade
Bentonite hydrated to create seal
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unified Soil Classification System
TOC=Top of Casing
VOCs=Volatile Organic Compounds
PID=Photoionization Detector
SVOCs=Semi-VOCs
FID=Flame Ionization Detector
RCRA=Resource Conservation and Recovery Act
EI=Elevation
Hex Cr—Hezavalent Chromium
115 MacKenan Drive, Cary, North Carolina 27511 tel:[phone] fox:919.467.6008 www.withersrovenel.com

APPENDIX B
Laboratory Analytical Reports

(1�;a'ceAnalyfical-
ANALYTICAL REPORT
June 06, 2023
a
Withers & Ravenel Eng. - Standard
Sample Delivery Group: L1616119
Samples Received: 05/13/2023
Project Number: 23-0302
Description: Hillsborough St. Assemblage
Report To:
Matt James
115 MacKenan Drive
Cary, NC 27511
Entire Report Reviewed By: 4�41
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
41
I
u
FC
E
FAI
FC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 1 of 132

TABLE OF CONTENTS
Cp: Cover Page
1
FP1
Tc: Table of Contents
2
Ss: Sample Summary
4
Cn: Case Narrative
9
Sr: Sample Results
10
FS
TW-1(5-7.5) L1616119-01
10
[Cn]
TW-2(5-7.5) L1616119-02
13
TW-3(5-7.5) L1616119-03
16
Fr
TW-4(5-7.5) L1616119-04
19
TW-5(5-7.5) L1616119-05
22
RC
TW-6(5-7.5) L1616119-06
25
F,
TW-7(5-7.5) L1616119-07
28
TW-8(5-7.5) L1616119-08
31
rAl
TW-9(5-7.5) L1616119-09
34
TW-10(5-7.5) L1616119-10
37
FSC
DUP L1616119-11
40
TW-1 L1616119-12
43
TW-2 L1616119-13
46
TW-3 L1616119-14
49
TW-4 L1616119-15
52
TW-5 L1616119-16
55
TW-6 L1616119-17
58
TW-7 L1616119-18
61
TW-8 L1616119-19
64
TW-9 L1616119-20
67
TW-10 L1616119-21
70
DUP L1616119-22
73
Qc: Quality Control Summary
76
Total Solids by Method 2540 G-2011
76
Wet Chemistry by Method 7199
78
Mercury by Method 7470A
85
Mercury by Method 7471B
86
Metals (ICPMS) by Method 6020B
88
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
90
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
94
Volatile Organic Compounds (GC/MS) by Method 8260D
95
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
107
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
117
GI: Glossary of Terms
129
Al: Accreditations & Locations
130
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
06/06/23 12:28
2 of 132

Sc: Sample Chain of Custody
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 3 of 132

SAMPLE SUMMARY
Collected by
Collected date/time
Received date/time
TW-1(5-7.5) L1616119-01 Solid
Austin Pote
05/11/2308:45
05/13/2309:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Total Solids by Method 2540 G-2011
WG2060621
1
05/16/2316:11
05/16/2316:32
CMK
Mt. Juliet, TN
Wet Chemistry by Method 7199
WG2061030
1
05/17/23 07:12
05/17/2318:28
VSS
Mt. Juliet, TN
Mercury by Method 7471B
WG2061958
1
06/05/2310:42
06/05/2318:11
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2061326
5
05/17/23 09:25
05/17/23 20:31
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2062683
1
05/11/23 08:45
05/18/23 21:20
ACG
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2062836
1
05/19/23 07:43
05/19/23 22:41
AMG
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-2(5-7.5) L1616119-02 Solid
Austin Pote
05/11/2309:45
05/13/2309:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Total Solids by Method 2540 G-2011
WG2060621
1
05/16/2316:11
05/16/2316:32
CMK
Mt. Juliet, TN
Wet Chemistry by Method 7199
WG2061030
1
05/17/23 07:12
05/17/2318:33
VSS
Mt. Juliet, TN
Mercury by Method 7471E
WG2059805
1
06/02/2314:32
06/04/2317:50
AKB
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2061326
5
05/17/23 09:25
05/17/23 20:34
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2062683
1
05/11/23 09:45
05/18/23 21:40
ACG
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2062836
1
05/19/23 07:43
05/19/2319:30
AMG
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-3(5-7.5) L1616119-03 Solid
Austin Pote
05/11/2311:45
05/13/2309:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Total Solids by Method 2540 G-2011
WG2060621
1
05/16/2316:11
05/16/2316:32
CMK
Mt. Juliet, TN
Wet Chemistry by Method 7199
WG2061030
1
05/17/23 07:12
05/17/2318:39
VSS
Mt. Juliet, TN
Mercury by Method 7471B
WG2059805
1
06/02/2314:32
06/04/2317:57
AKB
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2061326
5
05/17/23 09:25
05/17/23 20:38
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2062683
1
05/11/2311:45
05/18/23 21:59
ACG
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2062836
1
05/19/23 07:43
05/19/23 20:33
AMG
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-4(5-7.5) L1616119-04 Solid
Austin Pote
05/11/2312:45
05/13/2309:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Total Solids by Method 2540 G-2011
WG2060621
1
05116/2316:11
05/16/2316:32
CMK
Mt. Juliet, TN
Wet Chemistry by Method 7199
WG2061030
1
05/17/23 07:12
05/17/2318:44
VSS
Mt. Juliet, TN
Mercury by Method 7471E
WG2059805
1
06/02/2314:32
06/04/2318:05
AKB
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2061326
5
05/17/23 09:25
05/17/23 20:41
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2062683
1
05/11/2312:45
05/18/23 22:19
ACG
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2062836
1
05/19/23 07:43
05/19/23 20:54
AMG
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-5(5-7.5) L1616119-05 Solid
Austin Pote
05/11/2314:10
05/13/2309:15
FP1
FTC
4
Cn
FSr
RC
F,
FAI
FSC
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Total Solids by Method 2540 G-2011
WG2060621
1 05/16/2316:11
05/16/2316:32
CMK
Mt. Juliet, TN
Wet Chemistry by Method 7199
WG2061030
1 05/17/23 07:12
05/17/2318:49
VSS
Mt. Juliet, TN
Mercury by Method 7471B
WG2061958
1 06/05/2310:42
06/05/2318:13
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2061326
5 05/17/23 09:25
05/17/23 20:44
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2062683
1 05/11/2314:10
05/18/23 22:39
ACG
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2062836
1 05/19/23 07:43
05/19/2319:51
AMG
Mt. Juliet, TN
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23
12:28
4 of 132

SAMPLE SUMMARY
Collected by
Collected date/time
Received date/time
TW-6(5-7.5) L1616119-06 Solid
Austin Pote
05/11/2315:15
05/13/2309:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Total Solids by Method 2540 G-2011
WG2060621
1
05/16/2316:11
05/16/2316:32
CMK
Mt. Juliet, TN
Wet Chemistry by Method 7199
WG2061030
1
05/17/23 07:12
05/17/2318:54
VSS
Mt. Juliet, TN
Mercury by Method 7471B
WG2059805
1
06/02/2314:32
06/04/2318:07
AKB
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2061326
5
05/17/23 09:25
05/17/23 20:48
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2063443
1
05/11/2315:15
05/19/23 22:06
JBE
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2063159
1
05/19/2316:28
05/19/23 23:52
JRM
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-7(5-7.5) L1616119-07 Solid
Austin Pote
05/12/2309:15
05/13/2309:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Total Solids by Method 2540 G-2011
WG2060827
1
05/16/2315:09
05/16/2315:46
CMK
Mt. Juliet, TN
Wet Chemistry by Method 7199
WG2061030
1
05/17/23 07:12
05/17/2318:59
VSS
Mt. Juliet, TN
Mercury by Method 7471E
WG2059805
1
06/02/2314:32
06/04/2318:09
AKB
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2061326
5
05/17/23 09:25
05/17/23 20:51
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2063443
1
05/12/23 09:15
05/19/23 22:28
JBE
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2063159
1
05/19/2316:28
05/20/23 00:13
AGW
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-8(5-7.5) L1616119-08 Solid
Austin Pote
05/12/2310:20
05/13/2309:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Total Solids by Method 2540 G-2011
WG2060827
1
05/16/2315:09
05/16/2315:46
CMK
Mt. Juliet, TN
Wet Chemistry by Method 7199
WG2061030
1
05/17/23 07:12
05/17/2319:20
VSS
Mt. Juliet, TN
Mercury by Method 7471B
WG2061958
1
06/05/2310:42
06/0512318:16
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2061326
5
05/17/23 09:25
05/17/23 20:54
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2063443
1
05/12/2310:20
05/19/23 22:49
JBE
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2063159
1
05/19/2316:28
05/20/23 00:35
AGW
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-9(5-7.5) L1616119-09 Solid
Austin Pote
05/12/2311:45
05/13/2309:15
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Total Solids by Method 2540 G-2011
WG2060827
1 05116/2315:09
05/16/2315:46
CMK
Mt. Juliet, TN
Wet Chemistry by Method 7199
WG2061030
1 05/17/23 07:12
05/17/2319:25
VSS
Mt. Juliet, TN
Mercury by Method 7471E
WG2061958
1 06/05/2310:42
06/05/2318:18
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2061326
5 05/17/23 09:25
05/17/23 20:58
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2063443
1 05/12/2311:45
05/19/23 23:11
JBE
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2063159
1 05/19/2316:28
05/20/23 00:57
AGW
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-10(5-7.5) L1616119-10 Solid
Austin Pote
05/12/2314:00
05/13/2309:15
FP1
FTC
4
Cn
FSr
RC
F,
FAI
FSC
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Total Solids by Method 2540 G-2011
WG2060827
1 05/16/2315:09
05/16/2315:46
CMK
Mt. Juliet, TN
Wet Chemistry by Method 7199
WG2061030
1 05/17/23 07:12
05/17/2319:30
VSS
Mt. Juliet, TN
Mercury by Method 7471B
WG2061958
1 06/05/2310:42
06/05/2318:20
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2061326
5 05/17/23 09:25
05/17/23 21:01
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2063443
1 05/12/2314:00
05/19/23 23:32
JBE
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2063159
1 05/19/2316:28
05/20/23 01:19
AGW
Mt. Juliet, TN
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23
12:28
5 of 132

DUP L1616119-11 Solid
SAMPLE SUMMARY
Collected by
Austin Pote
Method Batch
Collected date/time Received date/time
05/11/2312:00 05/13/23 09:15
Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011
WG2060827
1 05/16/2315:09
05/16/2315:46
CMK
Mt. Juliet, TN
Wet Chemistry by Method 7199
WG2061041
1 05/17/23 03:21
05/17/2311:56
SET
Mt. Juliet, TN
Mercury by Method 7471B
WG2061958
1 06/05/2310:42
06/05/2318:28
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2061326
5 05/17/23 09:25
05/17/23 21:12
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2064295
1 05/11/2312:00
05/22/2310:25
BAM
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2063159
1 05/19/2316:28
05/20/23 01:41
AGW
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-1 L1616119-12 GW
Austin Pote
05/11/2310:45
05/13/23 09:15
Method
Wet Chemistry by Method 7199
Mercury by Method 7470A
Metals (ICPMS) by Method 6020B
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
TW-2 L1616119-13 GW
Batch Dilution Preparation Analysis Analyst Location
date/time date/time
WG2059859
1 05/18/23 04:51
05/18/23 04:51
SET
Mt. Juliet, TN
WG2060584
1 06/04/23 21:29
06/05/2319:50
LAS
Mt. Juliet, TN
WG2060154
1 05/17/23 22:34
05/23/23 22:03
LD
Mt. Juliet, TN
WG2064057
1 05/22/23 01:36
05/22/23 01:36
BAM
Mt. Juliet, TN
WG2059503
1.05 05/16/2311:33
05/17/23 02:08
DSH
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
Austin Pote
05/11/2313:05
05/13/23 09:15
FP1
FTC
4
Cn
FSr
RC
FGI
rAl
FSC
Method
Wet Chemistry by Method 7199
Mercury by Method 7470A
Metals (ICPMS) by Method 6020B
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
TW-3 L1616119-14 GW
Batch
WG2059859
WG2060584
WG2060154
WG2064057
WG2064510
WG2059503
Dilution
1
1
1
1
10
1.05
Preparation
date/time
05/18/23 05:15
06/04/23 21:29
05/17/23 22:34
05/22/23 01:55
05/23/23 04:14
05/16/2311:33
Collected by
Austin Pote
Analysis
date/time
05/18/23 05:15
06/05/2319:53
05/23/23 22:06
05/22/23 01:55
05/23/23 04:14
05/17/23 02:29
Collected date/time
05/11/2316:00
Analyst Location
SET Mt. Juliet, TN
LAS Mt. Juliet, TN
LD Mt. Juliet, TN
BAM Mt. Juliet, TN
ACG Mt. Juliet, TN
DSH Mt. Juliet, TN
Received date/time
05/13/23 09:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Wet Chemistry by Method 7199
WG2059859
1
05/18/23 05:30
05/18/23 05:30
SET
Mt. Juliet, TN
Mercury by Method 7470A
WG2060584
1
06/04/23 21:29
06/05/2319:55
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2060154
1
05/17/23 22:34
05/23/23 22:10
LD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
WG2064057
1
05/22/23 02:14
05/22/23 02:14
BAM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200E-2011
WG2064510
1
05/23/23 03:09
05/23/23 03:09
ACG
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG2059503
1
05/16/2311:33
05/17/23 02:50
DSH
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-4 L1616119-15 GW
Austin Pote
05/11/2315:00
05/13/23 09:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Wet Chemistry by Method 7199
WG2059859
1
05/18/23 05:38
05/18/23 05:38
SET
Mt. Juliet, TN
Mercury by Method 7470A
WG2060584
1
06/04/23 21:29
06/05/2319:57
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2060154
1
05/17/23 22:34
05/23/23 22:13
LD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
WG2064057
1
05/22/23 02:33
05/22/23 02:33
BAM
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG2059503
1
05/16/2311:33
05/17/23 03:12
DSH
Mt. Juliet, TN
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
6 of 132

SAMPLE SUMMARY
Collected by
Collected date/time
Received date/time
TW-5 L1616119-16 GW
Austin Pote
05/11/2316:45
05/13/23 09:15
C p
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
FTC
Wet Chemistry by Method 7199
WG2059859
1
05/18/23 06:01
05/18/23 06:01
SET
Mt. Juliet, TN
Mercury by Method 7470A
WG2060584
1
06/04/23 21:29
06/05/23 20:00
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2060154
1
05/17/23 22:34
05/23/23 22:33
LD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
WG2064057
1
05/22/23 02:52
05/22/23 02:52
BAM
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG2059503
1
05/16/2311:33
05/17/23 03:34
DSH
Mt. Juliet, TN
4
Cn
Collected by
Collected date/time
Received date/time
FSr
TW-6 L1616119-17 GW
AustinPote
05/11/2317:30
05/13/2309:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
RCdate/time
date/time
Wet Chemistry by Method 7199
WG2059859
1
05/18/23 06:08
05/18/23 06:08
SET
Mt. Juliet, TN
Mercury by Method 7470A
WG2060584
1
06/04/23 21:29
06/05/23 20:02
LAS
Mt. Juliet, TN
GI
Metals (ICPMS) by Method 6020B
WG2060154
1
05/17/23 22:34
05/23/23 22:37
LD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
WG2064057
1
05/22/23 03:11
05/22/23 03:11
BAM
Mt. Juliet, TN
FAI
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG2059503
1
05/16/2311:33
05/17/23 03:55
DSH
Mt. Juliet, TN
FSC
Collected by
Collected date/time
Received date/time
TW-7 L1616119-18 GW
Austin Pote
05/12/2312:10
05/13/23 09:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Wet Chemistry by Method 7199
WG2059859
1
05/18/23 06:16
05/18/23 06:16
SET
Mt. Juliet, TN
Mercury by Method 7470A
WG2060584
1
06/04/23 21:29
06/05/23 20:05
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2060154
1
05/17/23 22:34
05/23/23 22:41
LD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
WG2064057
1
05/22/23 03:30
05/22/23 03:30
BAM
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG2061246
1
05/18/23 06:45
05/20/23 01:41
AMG
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-8 L1616119-19 GW
Austin Pote
05/12/2311:45
05/13/23 09:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Wet Chemistry by Method 7199
WG2059859
1
05/18/23 06:24
05/18/23 06:24
SET
Mt. Juliet, TN
Mercury by Method 7470A
WG2060584
1
06/04/23 21:29
06/05/2319:29
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2060154
1
05/17/23 22:34
05/23/23 22:44
LD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
WG2064057
1
05/22/23 03:49
05/22/23 03:49
BAM
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG2061246
1
05/18/23 06:45
05/20/23 02:02
AMG
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TW-9 L1616119-20 GW
Austin Pote
05/12/2314:00
05/13/23 09:15
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Wet Chemistry by Method 7199
WG2059859
1
05/18/23 06:31
05/18/23 06:31
SET
Mt. Juliet, TN
Mercury by Method 7470A
WG2060584
1
06/04/23 21:29
06/05/23 20:12
LAS
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2060154
1
05/17/23 22:34
05/23/23 22:47
LD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
WG2064057
1
05/22/23 04:08
05/22/23 04:08
BAM
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG2061246
1
05/18/23 06:45
05/20/23 02:23
AMG
Mt. Juliet, TN
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
7 of 132

TW-10 L1616119-21 GW
Method
Wet Chemistry by Method 7199
Mercury by Method 7470A
Metals (ICPMS) by Method 6020B
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
DUP L1616119-22 GW
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
Austin Pote 05/12/2315:15 05/13/23 09:15 C
P
Batch Dilution Preparation Analysis Analyst Location L—J
date/time date/time FT,]
WG2059859
1 05/18/23 06:47
05/18/23 06:47
SET
Mt. Juliet, TN
WG2060584
1 06/04/23 21:29
06/05/23 20:14
LAS
Mt. Juliet, TN
WG2060154
1 05/17/23 22:34
05/23/23 22:51
LD
Mt. Juliet, TN
WG2064057
1 05/22/23 04:27
05/22/23 04:27
BAM
Mt. Juliet, TN
WG2061246
1 05/18/23 06:45
05/20/23 02:44
AMG
Mt. Juliet, TN
rCn
Collected by
Collected date/time
Received date/time
FSr
Austin Pote
05/11/2312:00
05/13/23 09:15
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
RCdate/time
date/time
Wet Chemistry by Method 7199
WG2061989
1 05/22/23 02:20
05/22/23 02:20
SET
Mt. Juliet, TN
Mercury by Method 7470A
WG2060584
1 06/04/23 21:29
06/05/23 20:17
LAS
Mt. Juliet, TN
GI
Metals (ICPMS) by Method 6020B
WG2060154
1 05/17/23 22:34
05/23/23 22:54
LD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
WG2064057
1 05/22/23 04:46
05/22/23 04:46
BAM
Mt. Juliet, TN
FAI
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG2061246
1 05/18/23 06:45
05/20/23 03:06
AMG
Mt. Juliet, TN
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 8 of 132

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FSS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Fr
RC
F,
Heather J Wagner
[Al
Project Manager
FSC
Sample Delivery Group (SDG) Narrative
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
Lab Sample ID
Project Sample ID
Method
L1616119-12
TW-1
7199
L1616119-13
TW-2
7199
L1616119-14
TW-3
7199
L1616119-15
TW-4
7199
L1616119-16
TW-5
7199
L1616119-17
TW-6
7199
L1616119-18
TW-7
7199
L1616119-19
TW-8
7199
L1616119-20
TW-9
7199
L1616119-21
TW-10
7199
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 9 of 132

SAMPLE RESULTS - 01
-1616119
TW-1(5-7.5)
Collected date/time: 05/11/23 08:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 78.0 1 05/16/202316:32 WG2060621
Wet Chemistry by Method 7199
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Hexavalent Chromium 1.79
0.327
1.28
1 05/17/202318:28
WG2061030
Mercury by Method 7471B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Mercury U
0.0231
0.0513
1 06/05/202318:11
WG2061958
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry)
Analyte
Barium
13.4
0.195
Cadmium
U
0.110
Chromium
15.0
0.380
Lead
11.3
0.127
Selenium
0.730
J_ 0.231
Silver
U
0.111
Volatile Organic Compounds (GC/MS) by Method 8260D
Analyte
Acetone
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec -Butyl benzene
ter[-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ACCOUNT:
Withers & Ravenel Eng. - Standard
Qualifier
MDL (dry)
mg/kg
C3 J3
0.0594
0.00587
0.000760
0.00146
0.00118
0.00190
0.00320
0.00854
0.00468
0.00317
0.00146
0.000342
0.000995
0.00276
0.00168
J3
0.00707
0.00141
0.000732
C3
0.00634
0.00105
0.00122
0.000691
0.000976
0.00114
0.00262
0.000799
0.00106
0.000986
PROJECT:
23-0302
RDL (dry)
Dilution
Analysis
Batch
mg/kg
date / time
1.28
5
05/17/2023 20:31
WG2061326
3.21
5
05/17/2023 20:31
WG2061326
1.28
5
05/17/2023 20:31
WG2061326
6.41
5
05/17/2023 20:31
WG2061326
2.56
5
05/17/2023 20:31
WG2061326
3.21
5
05/17/2023 20:31
WG2061326
0.641
5
05/17/2023 20:31
WG2061326
RDL (dry)
Dilution Analysis
mg/kg
date / time
0.0813
1 05/18/2023 21:20
0.0203
1 05/18/2023 21:20
0.00163
1 05/18/2023 21:20
0.0203
1 05/18/2023 21:20
0.00407
1 05/18/2023 21:20
0.0407
1 05/18/2023 21:20
0.0203
1 05/18/2023 21:20
0.0203
1 05/18/2023 21:20
0.0203
1 05/18/2023 21:20
0.00813
1 05/18/2023 21:20
0.00813
1 05/18/2023 21:20
0.00407
1 05/18/2023 21:20
0.00407
1 05/18/2023 21:20
0.00813
1 05/18/2023 21:20
0.00407
1 05/18/2023 21:20
0.0203
1 05/18/2023 21:20
0.00407
1 05/18/2023 21:20
0.00813
1 05/18/2023 21:20
0.0407
1 05/18/2023 21:20
0.00407
1 05/18/2023 21:20
0.00813
1 05/18/2023 21:20
0.00813
1 05/18/2023 21:20
0.00813
1 05/18/2023 21:20
0.00813
1 05/18/2023 21:20
0.00407
1 05/18/2023 21:20
0.00407
1 05/18/2023 21:20
0.00407
1 05/18/2023 21:20
0.00407
1 05/18/2023 21:20
SDG:
L1616119
Batch
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
DATE/TIME:
06/06/23 12:28
FP1
FTC
FSS
4
Cn
rqc
F,
FAI
FSC
PAGE:
10 of 132

TW-1(5-7.5) SAMPLE RESULTS - 01
Collected date/time: 05/11/23 08:45 L1616119
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
cis-1,2-Dichloroethene
U
C3 J4
0.00119
0.00407
1 05/18/2023 21:20
WG2062683
trans-1,2-Dichloroethene
U
0.00169
0.00813
1 05/18/2023 21:20
WG2062683
1,2-Dichloropropane
U
0.00231
0.00813
1 05/18/2023 21:20
WG2062683
1,1-Dichloropropene
U
0.00132
0.00407
1 05/18/2023 21:20
WG2062683
1,3-Dichloropropane
U
0.000815
0.00813
1 05/18/2023 21:20
WG2062683
cis-1,3-Dichloropropene
U
0.00123
0.00407
1 05/18/2023 21:20
WG2062683
trans-1,3-Dichloropropene
U
0.00185
0.00813
1 05/18/2023 21:20
WG2062683
2,2-Dichloropropane
U
0.00224
0.00407
1 05/18/2023 21:20
WG2062683
Di -isopropyl ether
U
0.000667
0.00163
1 05/18/2023 21:20
WG2062683
Ethylbenzene
U
0.00120
0.00407
1 05/18/2023 21:20
WG2062683
Hexachloro-1,3-butadiene
U
0.00976
0.0407
1 05/18/2023 21:20
WG2062683
Isopropylbenzene
U
0.000691
0.00407
1 05/18/2023 21:20
WG2062683
p-Isopropyltoluene
U
0.00415
0.00813
1 05/18/2023 21:20
WG2062683
2-Butanone (MEK)
U
0.103
0.163
1 05/18/2023 21:20
WG2062683
Methylene Chloride
U
0.0108
0.0407
1 05/18/2023 21:20
WG2062683
4-Methyl-2-pentanone (MIBK)
U
0.00371
0.0407
1 05/18/2023 21:20
WG2062683
Methyl tert-butyl ether
U
0.000569
0.00163
1 05/18/2023 21:20
WG2062683
Naphthalene
U
C3
0.00794
0.0203
1 05/18/2023 21:20
WG2062683
n-Propylbenzene
U
0.00155
0.00813
1 05/18/2023 21:20
WG2062683
Styrene
U
C3
0.000372
0.0203
1 05/18/2023 21:20
WG2062683
1,1,1,2-Tetrachloroethane
U
0.00154
0.00407
1 05/18/2023 21:20
WG2062683
1,1,2,2-Tetrachloroethane
U
0.00113
0.00407
1 05/18/2023 21:20
WG2062683
Tetrachloroethene
U
0.00146
0.00407
1 05/18/2023 21:20
WG2062683
Toluene
U
0.00211
0.00813
1 05/18/2023 21:20
WG2062683
1,2,3-Trichlorobenzene
U
C3
0.0119
0.0203
1 05/18/2023 21:20
WG2062683
1,2,4-Trichlorobenzene
U
C3
0.00716
0.0203
1 05/18/2023 21:20
WG2062683
1,1,1-Trichloroethane
U
0.00150
0.00407
1 05/18/2023 21:20
WG2062683
1,1,2-Trichloroethane
U
0.000971
0.00407
1 05/18/2023 21:20
WG2062683
1,1,2-Trichlorotrifluoroethane
U
0.00123
0.00407
1 05/18/2023 21:20
WG2062683
Trichloroethene
U
0.000950
0.00163
1 05/18/2023 21:20
WG2062683
Trichlorofluoromethane
U
0.00135
0.00407
1 05/18/2023 21:20
WG2062683
1,2,3-Trichloropropane
U
0.00263
0.0203
1 05/18/2023 21:20
WG2062683
1,2,4-Trimethylbenzene
U
0.00257
0.00813
1 05/18/2023 21:20
WG2062683
1,3,5-Trimethyl benzene
U
0.00325
0.00813
1 05/18/2023 21:20
WG2062683
Vinyl chloride
U
0.00189
0.00407
1 05/18/2023 21:20
WG2062683
Xylenes, Total
U
0.00143
0.0106
1 05/18/2023 21:20
WG2062683
(S) Toluene-d8
104
75.0-131
051181202321:20
WG2062683
(S)4-Bromof/uorobenzene
89.9
67.0-138
051181202321:20
WG2062683
(S)1,2-Dich/oroethone-d4
88.6
70.0-130
051181202321:20
WG2062683
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acenaphthene
U
0.00691
0.0427
1 05/19/2023 22:41
WG2062836
Acenaphthylene
U
0.00601
0.0427
1 05/19/2023 22:41
WG2062836
Anthracene
U
0.00760
0.0427
1 05/19/2023 22:41
WG2062836
Benzidine
U
0.0803
2.14
1 05/19/2023 22:41
WG2062836
Benzo(a)anth race ne
U
0.00753
0.0427
1 05/19/2023 22:41
WG2062836
Benzo(b)fluoranthene
U
0.00796
0.0427
1 05/19/2023 22:41
WG2062836
Benzo(k)fluoranthene
U
0.00759
0.0427
1 05/19/2023 22:41
WG2062836
Benzo(g,h,i)perylene
U
0.00781
0.0427
1 05/19/2023 22:41
WG2062836
Benzo(a)pyrene
U
0.00794
0.0427
1 05/19/2023 22:41
WG2062836
Bis(2-chlorethoxy)methane
U
0.0128
0.427
1 05/19/2023 22:41
WG2062836
Bis(2-chloroethyl)ether
U
0.0141
0.427
1 05/19/2023 22:41
WG2062836
2,2-Oxybis(1-Chloropropane)
U
0.0185
0.427
1 05/19/2023 22:41
WG2062836
4-Bromophenyl-phenylether
U
0.0150
0.427
1 05/19/2023 22:41
WG2062836
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
FP1
FTc
FSS
4
Cn
Rc
F ql
FAI
FSC
PAGE:
11 of 132

TW-1(5-7.5) SAMPLE RESULTS - 01
Collected date/time: 05/11/23 08:45 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
2-Chloronaphthalene
4-ChIcrop henyl-phenylether
Chrysene
Dibenz(a,h)anth racene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
HexachIoro-1,3-butadiene
HexachIorocyclopentadiene
Hexachloroethane
Ind eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a mine
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-methyl phen of
2-Chorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
52.9
48.9
41.9
52.0
55.9
56.5
Qualifier MDL (dry)
RDL (dry)
mg/kg
mg/kg
0.00750
0.0427
0.0149
0.427
0.00849
0.0427
0.0118
0.0427
0.0127
0.427
0.0130
0.427
0.0127
0.427
0.0158
0.427
0.0122
0.427
0.0140
0.427
0.00771
0.0427
0.00695
0.0427
0.0151
0.427
0.0144
0.427
0.0224
0.427
0.0168
0.427
0.0121
0.0427
0.0131
0.427
0.0107
0.0427
0.0149
0.427
0.0633
0.427
0.0323
0.427
0.0142
0.427
0.00848
0.0427
0.0133
0.427
0.0541
0.427
0.0146
0.427
0.0141
0.427
0.0905
0.427
0.0289
0.427
0.00831
0.0427
0.0133
0.427
0.0138
0.427
0.0141
0.427
0.0124
0.427
0.0112
0.427
0.0968
0.427
0.0999
0.427
0.0153
0.427
0.0133
0.427
0.0115
0.427
0.0172
0.427
0.0137
0.427
12.0-120
10.0-120
10.0-122
15.0-120
10.0-127
10.0-120
Dilution Analysis Batch
date / time
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
05/19/2023 22:41
0511912023 22.41
0511912023 22.41
0511912023 22.41
0511912023 22.41
0511912023 22.41
0511912023 22.41
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
12 of 132

SAMPLE RESULTS - 02
L1616119
TW-2(5-7.5)
Collected date/time: 05/11/23 09:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 82.6 1 05/16/202316:32 WG2060621
Wet Chemistry by Method 7199
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Hexavalent Chromium 0.404
J 0.309
1.21
1 05/17/202318:33
WG2061030
Mercury by Method 7471B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date/time
Mercury U
0.0218
0.0484
1 06/04/202317:50
WG2059805
Metals (ICPMS) by Method 6020B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
_ mg/kg
mg/kg
mg/kg
date / time
Arsenic
5.17
0.121
1.21
5
05/17/2023 20:34
WG2061326
Barium
10.7
0.184
3.03
5
05/17/2023 20:34
WG2061326
Cadmium
U
0.104
1.21
5
05/17/2023 20:34
WG2061326
Chromium
17.7
0.359
6.06
5
05/17/2023 20:34
WG2061326
Lead
5.24
0.120
2.42
5
05/17/2023 20:34
WG2061326
Selenium
0.647
1_ 0.218
3.03
5
05/17/2023 20:34
WG2061326
Silver
U
0.105
0.606
5
05/17/2023 20:34
WG2061326
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acetone
U
C3 J3
0.0529
0.0725
1 05/18/2023 21:40
WG2062683
Acrylonitrile
U
0.00523
0.0181
1 05/18/2023 21:40
WG2062683
Benzene
U
0.000677
0.00145
1 05/18/2023 21:40
WG2062683
Bromobenzene
U
0.00130
0.0181
1 05/18/2023 21:40
WG2062683
Bromodichloromethane
U
0.00105
0.00362
1 05/18/2023 21:40
WG2062683
Bromoform
U
0.00170
0.0362
1 05/18/2023 21:40
WG2062683
Bromomethane
U
0.00286
0.0181
1 05/18/2023 21:40
WG2062683
n-Butylbenzene
U
0.00761
0.0181
1 05/18/2023 21:40
WG2062683
sec -Butyl benzene
U
0.00418
0.0181
1 05/18/2023 21:40
WG2062683
ter[-Butylbenzene
U
0.00283
0.00725
1 05/18/2023 21:40
WG2062683
Carbon tetrachloride
U
0.00130
0.00725
1 05/18/2023 21:40
WG2062683
Chlorobenzene
U
0.000304
0.00362
1 05/18/2023 21:40
WG2062683
Chlorodibromomethane
U
0.000887
0.00362
1 05/18/2023 21:40
WG2062683
Chloroethane
U
0.00246
0.00725
1 05/18/2023 21:40
WG2062683
Chloroform
U
0.00149
0.00362
1 05/18/2023 21:40
WG2062683
Chloromethane
U
J3
0.00631
0.0181
1 05/18/2023 21:40
WG2062683
2-Chlorotoluene
U
0.00125
0.00362
1 05/18/2023 21:40
WG2062683
4-Chlorotoluene
U
0.000652
0.00725
1 05/18/2023 21:40
WG2062683
1,2-Dibromo-3-Chloropropane
U
C3
0.00565
0.0362
1 05/18/2023 21:40
WG2062683
1,2-Dibromoethane
U
0.000939
0.00362
1 05/18/2023 21:40
WG2062683
Dibromomethane
U
0.00109
0.00725
1 05/18/2023 21:40
WG2062683
1,2-Dichlorobenzene
U
0.000616
0.00725
1 05/18/2023 21:40
WG2062683
1,3-Dichlorobenzene
U
0.000870
0.00725
1 05/18/2023 21:40
WG2062683
1,4-Dichlorobenzene
U
0.00101
0.00725
1 05/18/2023 21:40
WG2062683
Dichlorodifluoromethane
U
0.00233
0.00362
1 05/18/2023 21:40
WG2062683
1,1-Dichloroethane
U
0.000712
0.00362
1 05/18/2023 21:40
WG2062683
1,2-Dichloroethane
U
0.000941
0.00362
1 05/18/2023 21:40
WG2062683
1,1-Dichloroethene
U
0.000879
0.00362
1 05/18/2023 21:40
WG2062683
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
FP1
FTC
FSS
4
Cn
rqc
F,
FAI
FSC
PAGE:
13 of 132

TW-2(5-7.5) SAMPLE
Collected date/time: 05/11/23 09:45
Volatile Organic Compounds (GC/MS) by Method 8260D
RESULTS - 02
L1616119
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
FP1
Analyte
mg/kg
mg/kg
mg/kg
date / time
cis-1,2-Dichloroethene
U
C3 J4
0.00106
0.00362
1 05/18/2023 21:40
WG2062683
z
Tc
trans-1,2-Dichloroethene
U
0.00151
0.00725
1 05/18/2023 21:40
WG2062683
1,2-Dichloropropane
U
0.00206
0.00725
1 05/18/2023 21:40
WG2062683
1,1-Dichloropropene
U
0.00117
0.00362
1 05/18/2023 21:40
WG2062683
FSS
1,3-Dichloropropane
U
0.000726
0.00725
1 05/18/2023 21:40
WG2062683
cis-1,3-Dichloropropene
U
0.00110
0.00362
1 05/18/2023 21:40
WG2062683
4
Cn
trans-1,3-Dichloropropene
U
0.00165
0.00725
1 05/18/2023 21:40
WG2062683
2,2-Dichloropropane
U
0.00200
0.00362
1 05/18/2023 21:40
WG2062683
Di -isopropyl ether
U
0.000594
0.00145
1 05/18/2023 21:40
WG2062683
Ethylbenzene
U
0.00107
0.00362
1 05/18/2023 21:40
WG2062683
Hexachloro-1,3-butadiene
U
0.00870
0.0362
1 05/18/2023 21:40
WG2062683
Rc
Isopropylbenzene
U
0.000616
0.00362
1 05/18/2023 21:40
WG2062683
p-Isopropyltoluene
U
0.00370
0.00725
1 05/18/2023 21:40
WG2062683
2-Butanone (MEK)
U
0.0921
0.145
1 05/18/2023 21:40
WG2062683
GI
Methylene Chloride
U
0.00963
0.0362
1 05/18/2023 21:40
WG2062683
4-Methyl-2-pentanone (MIBK)
U
0.00331
0.0362
1 05/18/2023 21:40
WG2062683
FAI
Methyl tert-butyl ether
U
0.000507
0.00145
1 05/18/2023 21:40
WG2062683
Naphthalene
U
C3
0.00708
0.0181
1 05/18/2023 21:40
WG2062683
n-Propylbenzene
U
0.00138
0.00725
1 05/18/2023 21:40
WG2062683
FSC
Styrene
U
C3
0.000332
0.0181
1 05/18/2023 21:40
WG2062683
1,1,1,2-Tetrachloroethane
U
0.00137
0.00362
1 05/18/2023 21:40
WG2062683
1,1,2,2-Tetrachloroethane
U
0.00101
0.00362
1 05/18/2023 21:40
WG2062683
Tetrachloroethene
U
0.00130
0.00362
1 05/18/2023 21:40
WG2062683
Toluene
U
0.00188
0.00725
1 05/18/2023 21:40
WG2062683
1,2,3-Trichlorobenzene
U
C3
0.0106
0.0181
1 05/18/2023 21:40
WG2062683
1,2,4-Trichlorobenzene
U
C3
0.00638
0.0181
1 05/18/2023 21:40
WG2062683
1,1,1-Trichloroethane
U
0.00134
0.00362
1 05/18/2023 21:40
WG2062683
1,1,2-Trichloroethane
U
0.000866
0.00362
1 05/18/2023 21:40
WG2062683
1,1,2-Trichlorotrifluoroethane
U
0.00109
0.00362
1 05/18/2023 21:40
WG2062683
Trichloroethene
U
0.000847
0.00145
1 05/18/2023 21:40
WG2062683
Trichlorofluoromethane
U
0.00120
0.00362
1 05/18/2023 21:40
WG2062683
1,2,3-Trichloropropane
U
0.00235
0.0181
1 05/18/2023 21:40
WG2062683
1,2,4-Trimethylbenzene
U
0.00229
0.00725
1 05/18/2023 21:40
WG2062683
1,3,5-Trimethyl benzene
U
0.00290
0.00725
1 05/18/2023 21:40
WG2062683
Vinyl chloride
U
0.00168
0.00362
1 05/18/2023 21:40
WG2062683
Xylenes, Total
U
0.00128
0.00942
1 05/18/2023 21:40
WG2062683
(S) Toluene-d8
108
75.0-131
051181202321.40
WG2062683
(S)4-Bromof/uorobenzene
88.9
67.0-138
051181202321.40
WG2062683
(S)1,2-Dich/oroethone-d4
85.4
70.0-130
051181202321.40
WG2062683
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acenaphthene
U
0.00653
0.0403
1 05/19/202319:30
WG2062836
Acenaphthylene
U
0.00568
0.0403
1 05/19/202319:30
WG2062836
Anthracene
U
0.00718
0.0403
1 05/19/202319:30
WG2062836
Benzidine
U
0.0758
2.02
1 05/19/202319:30
WG2062836
Benzo(a)anth race ne
U
0.00711
0.0403
1 05/19/202319:30
WG2062836
Benzo(b)fluoranthene
U
0.00752
0.0403
1 05/19/202319:30
WG2062836
Benzo(k)fluoranthene
U
0.00717
0.0403
1 05/19/202319:30
WG2062836
Benzo(g,h,i)perylene
U
0.00738
0.0403
1 05/19/202319:30
WG2062836
Benzo(a)pyrene
U
0.00750
0.0403
1 05/19/202319:30
WG2062836
Bis(2-chlorethoxy)methane
U
0.0121
0.403
1 05/19/202319:30
WG2062836
Bis(2-chloroethyl)ether
U
0.0133
0.403
1 05/19/202319:30
WG2062836
2,2-Oxybis(1-Chloropropane)
U
0.0174
0.403
1 05/19/202319:30
WG2062836
4-Bromophenyl-phenylether
U
0.0142
0.403
1 05/19/202319:30
WG2062836
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
14 of 132

TW-2(5-7.5) SAMPLE RESULTS - 02
Collected date/time: 05/11/23 09:45 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
2-Chloronaphthalene
4-ChIcrop henyl-phenylether
Chrysene
Dibenz(a,h)anth racene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
HexachIoro-1,3-butadiene
HexachIorocyclopentadiene
Hexachloroethane
Ind eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a mine
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-methyl phen of
2-Chorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
48.0
40.9
42.1
48.2
46.5
54.5
Qualifier MDL (dry)
RDL (dry)
mg/kg
mg/kg
0.00709
0.0403
0.0140
0.403
0.00802
0.0403
0.0112
0.0403
0.0120
0.403
0.0122
0.403
0.0120
0.403
0.0149
0.403
0.0116
0.403
0.0132
0.403
0.00728
0.0403
0.00656
0.0403
0.0143
0.403
0.0136
0.403
0.0212
0.403
0.0159
0.403
0.0114
0.0403
0.0124
0.403
0.0101
0.0403
0.0140
0.403
0.0598
0.403
0.0305
0.403
0.0134
0.403
0.00801
0.0403
0.0126
0.403
0.0511
0.403
0.0138
0.403
0.0133
0.403
0.0855
0.403
0.0273
0.403
0.00785
0.0403
0.0126
0.403
0.0131
0.403
0.0133
0.403
0.0117
0.403
0.0105
0.403
0.0914
0.403
0.0944
0.403
0.0144
0.403
0.0126
0.403
0.0109
0.403
0.0162
0.403
0.0130
0.403
12.0-120
10.0-120
10.0-122
15.0-120
10.0-127
10.0-120
Dilution Analysis Batch
date / time
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
05/19/202319:30
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
15 of132

SAMPLE RESULTS - 03
L1616119
TW-3(5-7.5)
Collected date/time: 05/11/23 11:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 83.2 1 05/16/202316:32 WG2060621
Wet Chemistry by Method 7199
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Hexavalent Chromium 0.545
J 0.307
1.20
1 05/17/202318:39
WG2061030
Mercury by Method 7471B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date/time
Mercury 0.179
0.0216
0.0481
1 06/04/202317:57
WG2059805
Metals (ICPMS) by Method 6020B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
_ mg/kg
mg/kg
mg/kg
date / time
Arsenic
10.3
0.120
1.20
5
05/17/2023 20:38
WG2061326
Barium
28.7
0.183
3.01
5
05/17/2023 20:38
WG2061326
Cadmium
U
0.103
1.20
5
05/17/2023 20:38
WG2061326
Chromium
33.2
0.356
6.01
5
05/17/2023 20:38
WG2061326
Lead
26.3
0.119
2.40
5
05/17/2023 20:38
WG2061326
Selenium
1.19
1_ 0.216
3.01
5
05/17/2023 20:38
WG2061326
Silver
U
0.104
0.601
5
05/17/2023 20:38
WG2061326
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acetone
U
C3 J3
0.0521
0.0713
1 05/18/2023 21:59
WG2062683
Acrylonitrile
U
0.00515
0.0178
1 05/18/2023 21:59
WG2062683
Benzene
U
0.000666
0.00143
1 05/18/2023 21:59
WG2062683
Bromobenzene
U
0.00128
0.0178
1 05/18/2023 21:59
WG2062683
Bromodichloromethane
U
0.00103
0.00357
1 05/18/2023 21:59
WG2062683
Bromoform
U
0.00167
0.0357
1 05/18/2023 21:59
WG2062683
Bromomethane
U
0.00281
0.0178
1 05/18/2023 21:59
WG2062683
n-Butylbenzene
U
0.00749
0.0178
1 05/18/2023 21:59
WG2062683
sec -Butyl benzene
U
0.00411
0.0178
1 05/18/2023 21:59
WG2062683
ter[-Butylbenzene
U
0.00278
0.00713
1 05/18/2023 21:59
WG2062683
Carbon tetrachloride
U
0.00128
0.00713
1 05/18/2023 21:59
WG2062683
Chlorobenzene
U
0.000300
0.00357
1 05/18/2023 21:59
WG2062683
Chlorodibromomethane
U
0.000873
0.00357
1 05/18/2023 21:59
WG2062683
Chloroethane
U
0.00243
0.00713
1 05/18/2023 21:59
WG2062683
Chloroform
U
0.00147
0.00357
1 05/18/2023 21:59
WG2062683
Chloromethane
U
J3
0.00621
0.0178
1 05/18/2023 21:59
WG2062683
2-Chlorotoluene
U
0.00123
0.00357
1 05/18/2023 21:59
WG2062683
4-Chlorotoluene
U
0.000642
0.00713
1 05/18/2023 21:59
WG2062683
1,2-Dibromo-3-Chloropropane
U
C3
0.00556
0.0357
1 05/18/2023 21:59
WG2062683
1,2-Dibromoethane
U
0.000924
0.00357
1 05/18/2023 21:59
WG2062683
Dibromomethane
U
0.00107
0.00713
1 05/18/2023 21:59
WG2062683
1,2-Dichlorobenzene
U
0.000606
0.00713
1 05/18/2023 21:59
WG2062683
1,3-Dichlorobenzene
U
0.000856
0.00713
1 05/18/2023 21:59
WG2062683
1,4-Dichlorobenzene
U
0.000999
0.00713
1 05/18/2023 21:59
WG2062683
Dichlorodifluoromethane
U
0.00230
0.00357
1 05/18/2023 21:59
WG2062683
1,1-Dichloroethane
U
0.000700
0.00357
1 05/18/2023 21:59
WG2062683
1,2-Dichloroethane
U
0.000926
0.00357
1 05/18/2023 21:59
WG2062683
1,1-Dichloroethene
U
0.000865
0.00357
1 05/18/2023 21:59
WG2062683
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
FP1
FTC
FSS
4
Cn
rqc
F,
FAI
FSC
PAGE:
16 of 132

TW-3(5-7.5) SAMPLE RESULTS - 03
Collected date/time: 05/11/23 11:45 L1616119
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Analyte
mg/kg
mg/kg
mg/kg
cis-1,2-Dichloroethene
U
C3 J4
0.00105
0.00357
trans-1,2-Dichloroethene
U
0.00148
0.00713
1,2-Dichloropropane
U
0.00203
0.00713
1,1-Dichloropropene
U
0.00115
0.00357
1,3-Dichloropropane
U
0.000715
0.00713
cis-1,3-Dichloropropene
U
0.00108
0.00357
trans-1,3-Dichloropropene
U
0.00163
0.00713
2,2-Dichloropropane
U
0.00197
0.00357
Di -isopropyl ether
U
0.000585
0.00143
Ethylbenzene
U
0.00105
0.00357
Hexachloro-1,3-butadiene
U
0.00856
0.0357
Isopropylbenzene
U
0.000606
0.00357
p-Isopropyltoluene
U
0.00364
0.00713
2-Butanone (MEK)
U
0.0906
0.143
Methylene Chloride
U
0.00947
0.0357
4-Methyl-2-pentanone (MIBK)
U
0.00325
0.0357
Methyl tert-butyl ether
U
0.000499
0.00143
Naphthalene
U
C3
0.00696
0.0178
n-Propylbenzene
U
0.00136
0.00713
Styrene
U
C3
0.000327
0.0178
1,1,1,2-Tetrachloroethane
U
0.00135
0.00357
1,1,2,2-Tetrachloroethane
U
0.000992
0.00357
Tetrachloroethene
U
0.00128
0.00357
Toluene
U
0.00185
0.00713
1,2,3-Trichlorobenzene
U
C3
0.0105
0.0178
1,2,4-Trichlorobenzene
U
C3
0.00628
0.0178
1,1,1-Trichloroethane
U
0.00132
0.00357
1,1,2-Trichloroethane
U
0.000852
0.00357
1,1,2-Trichlorotrifluoroethane
U
0.00108
0.00357
Trichloroethene
U
0.000833
0.00143
Trichlorofluoromethane
U
0.00118
0.00357
1,2,3-Trichloropropane
U
0.00231
0.0178
1,2,4-Trimethylbenzene
U
0.00225
0.00713
1,3,5-Trimethyl benzene
U
0.00285
0.00713
Vinyl chloride
U
0.00165
0.00357
Xylenes, Total
U
0.00126
0.00927
(S) Toluene-d8
103
75.0-131
(S) 4-Bromof/uorobenzene
91.6
67.0-138
(S) 1,2-Dich/oroethone-d4
90.0
70.0-130
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anth race ne
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis(2-chlorethoxy)methane
Bis(2-ch loroethyl)ether
2, 2-Oxybis(1-Ch I oropro pane)
4-Bromophenyl-phenylether
Result (dry) Qualifier MDL (dry)
mg/kg mg/kg
U
U
U
U
0.0114
0.0127
U
U
0.00924
U
U
U
U
J
0.00648
0.00564
0.00713
0.0753
0.00706
0.00747
0.00712
0.00732
0.00744
0.0120
0.0132
0.0173
0.0141
RDL (dry)
mg/kg
0.0400
0.0400
0.0400
2.01
0.0400
0.0400
0.0400
0.0400
0.0400
0.400
0.400
0.400
0.400
Dilution Analysis
date / time
Batch
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
1 05/18/2023 21:59
WG2062683
051181202321.59
WG2062683
051181202321.59
WG2062683
051181202321.59
WG2062683
Dilution Analysis
date / time
Batch
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
1 05/19/2023 20:33
WG2062836
FP1
FTc
FSS
4
Cn
Rc
F ql
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 17 of 132

TW-3(5-7.5) SAMPLE RESULTS - 03
Collected date/time: 05/11/23 11:45 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
2-Chloronaphthalene
4-ChIcrop henyl-phenylether
Chrysene
Dibenz(a,h)anth racene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
HexachIoro-1,3-butadiene
HexachIorocyclopentadiene
Hexachloroethane
Ind eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a mine
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-methyl phen of
2-Chorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
Result (dry)
mg/kg
Qualifier
MDL (dry)
mg/kg
RDL (dry)
mg/kg
U
0.00703
0.0400
U
0.0139
0.400
U
0.00796
0.0400
U
0.0111
0.0400
U
0.0119
0.400
U
0.0121
0.400
U
0.0119
0.400
U
0.0148
0.400
U
0.0115
0.400
U
0.0131
0.400
0.0186
1_
0.00722
0.0400
U
0.00652
0.0400
U
0.0142
0.400
U
0.0135
0.400
U
0.0210
0.400
U
0.0157
0.400
U
0.0113
0.0400
U
0.0123
0.400
U
0.0100
0.0400
U
0.0139
0.400
U
0.0594
0.400
U
0.0303
0.400
U
0.0133
0.400
0.00795
1_
0.00795
0.0400
U
0.0125
0.400
U
0.0507
0.400
U
0.0137
0.400
U
0.0132
0.400
U
0.0849
0.400
U
0.0270
0.400
0.0182
1_
0.00779
0.0400
U
0.0125
0.400
U
0.0130
0.400
U
0.0132
0.400
U
0.0117
0.400
U
0.0105
0.400
U
0.0908
0.400
U
0.0936
0.400
U
0.0143
0.400
U
0.0125
0.400
U
0.0108
0.400
U
0.0161
0.400
U
0.0129
0.400
49.4
12.0-120
44.3
10.0-120
45.6
10.0-122
49.2
15.0-120
51.1
10.0-127
57.8
10.0-120
Dilution Analysis Batch
date / time
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
05/19/2023 20:33
0511912023 2033
0511912023 2033
0511912023 2033
0511912023 2033
0511912023 2033
0511912023 2033
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
18 of132

SAMPLE RESULTS - 04
L1616119
TW-4(5-7.5)
Collected date/time: 05/11/23 12:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 69.5 1 05/16/202316:32 WG2060621
Wet Chemistry by Method 7199
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Hexavalent Chromium 0.838
J
0.367
1.44
1 05/17/202318:44
WG2061030
Mercury by Method 7471B
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date/time
Mercury 0.0271
J
0.0259
0.0576
1 06/04/202318:05
WG2059805
Metals (ICPMS) by Method 6020B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
_ mg/kg
mg/kg
mg/kg
date / time
Arsenic
77.5
0.144
1.44
5
05/17/2023 20:41
WG2061326
Barium
17.5
0.219
3.60
5
05/17/2023 20:41
WG2061326
Cadmium
U
0.123
1.44
5
05/17/2023 20:41
WG2061326
Chromium
15.2
0.426
7.20
5
05/17/2023 20:41
WG2061326
Lead
10.2
0.143
2.88
5
05/17/2023 20:41
WG2061326
Selenium
0.579
1_ 0.259
3.60
5
05/17/2023 20:41
WG2061326
Silver
U
0.125
0.720
5
05/17/2023 20:41
WG2061326
Volatile Organic Compounds (GC/MS) by Method 8260D
Analyte
Acetone
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec -Butyl benzene
ter[-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ACCOUNT:
Withers & Ravenel Eng. - Standard
Qualifier
MDL (dry)
RDL (dry)
mg/kg
mg/kg
C3 J3
0.0749
0.103
0.00740
0.0256
0.000958
0.00205
0.00185
0.0256
0.00149
0.00513
0.00240
0.0513
0.00404
0.0256
0.0108
0.0256
0.00591
0.0256
0.00400
0.0103
0.00184
0.0103
0.000431
0.00513
0.00126
0.00513
0.00349
0.0103
0.00211
0.00513
J3
0.00892
0.0256
0.00177
0.00513
0.000923
0.0103
C3
0.00800
0.0513
0.00133
0.00513
0.00154
0.0103
0.000872
0.0103
0.00123
0.0103
0.00144
0.0103
0.00330
0.00513
0.00101
0.00513
0.00133
0.00513
0.00124
0.00513
PROJECT:
23-0302
Dilution Analysis
date / time
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
1 05/18/2023 22:19
SDG:
L1616119
Batch
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
WG2062683
DATE/TIME:
06/06/23 12:28
FP1
FTC
FSS
4
Cn
rqc
F,
FAI
FSC
PAGE:
19 of 132

TW-4(5-7.5) SAMPLE RESULTS - 04
Collected date/time: 05/11/23 12:45 L1616119
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Analyte
mg/kg
mg/kg
mg/kg
cis-1,2-Dichloroethene
U
C3 J4
0.00151
0.00513
trans-1,2-Dichloroethene
U
0.00213
0.0103
1,2-Dichloropropane
U
0.00291
0.0103
1,1-Dichloropropene
U
0.00166
0.00513
1,3-Dichloropropane
U
0.00103
0.0103
cis-1,3-Dichloropropene
U
0.00155
0.00513
trans-1,3-Dichloropropene
U
0.00234
0.0103
2,2-Dichloropropane
U
0.00283
0.00513
Di -isopropyl ether
U
0.000841
0.00205
Ethylbenzene
U
0.00151
0.00513
Hexachloro-1,3-butadiene
U
0.0123
0.0513
Isopropylbenzene
U
0.000872
0.00513
p-Isopropyltoluene
U
0.00523
0.0103
2-Butanone (MEK)
U
0.130
0.205
Methylene Chloride
U
0.0136
0.0513
4-Methyl-2-pentanone (MIBK)
U
0.00468
0.0513
Methyl tert-butyl ether
U
0.000718
0.00205
Naphthalene
U
C3
0.0100
0.0256
n-Propylbenzene
U
0.00195
0.0103
Styrene
U
C3
0.000470
0.0256
1,1,1,2-Tetrachloroethane
U
0.00194
0.00513
1,1,2,2-Tetrachloroethane
U
0.00143
0.00513
Tetrachloroethene
U
0.00184
0.00513
Toluene
U
0.00267
0.0103
1,2,3-Trichlorobenzene
U
C3
0.0150
0.0256
1,2,4-Trichlorobenzene
U
C3
0.00903
0.0256
1,1,1-Trichloroethane
U
0.00189
0.00513
1,1,2-Trichloroethane
U
0.00122
0.00513
1,1,2-Trichlorotrifluoroethane
U
0.00155
0.00513
Trichloroethene
U
0.00120
0.00205
Trichlorofluoromethane
U
0.00170
0.00513
1,2,3-Trichloropropane
U
0.00332
0.0256
1,2,4-Trimethylbenzene
U
0.00324
0.0103
1,3,5-Trimethyl benzene
U
0.00410
0.0103
Vinyl chloride
U
0.00238
0.00513
Xylenes, Total
U
0.00181
0.0133
(S) Toluene-d8
106
75.0-131
(S) 4-Bromof/uorobenzene
89.6
67.0-138
(S) 1,2-Dich/oroethone-d4
88.5
70.0-130
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Analyte
mg/kg
mg/kg
mg/kg
Acenaphthene
0.0105
J_ 0.00776
0.0479
Acenaphthylene
U
0.00675
0.0479
Anthracene
0.0649
0.00854
0.0479
Benzidine
U
0.0901
2.40
Benzo(a)anth race ne
0.402
0.00845
0.0479
Benzo(b)fluoranthene
0.335
0.00894
0.0479
Benzo(k)fluoranthene
0.127
0.00852
0.0479
Benzo(g,h,i)perylene
0.101
0.00877
0.0479
Benzo(a)pyrene
0.261
0.00891
0.0479
Bis(2-chlorethoxy)methane
U
0.0144
0.479
Bis(2-chloroethyl)ether
U
0.0158
0.479
2,2-Oxybis(1-Chloropropane)
U
0.0207
0.479
4-Bromophenyl-phenylether
U
0.0168
0.479
ACCOUNT:
PROJECT:
Withers & Ravenel Eng.
- Standard
23-0302
Dilution Analysis
date / time
Batch
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
1 05/18/2023 22:19
WG2062683
051181202322:19
WG2062683
051181202322:19
WG2062683
051181202322:19
WG2062683
Dilution Analysis Batch
date / time
FP1
FTc
FSS
4
Cn
Rc
F ql
FAI
FSC
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
1 05/19/2023
20:54
WG2062836
SDG:
DATE/TIME: PAGE:
L1616119
06/06/23 12:28 20 of 132

TW-4(5-7.5) SAMPLE RESULTS - 04
Collected date/time: 05/11/23 12:45 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
2-Chloronaphthalene
4-ChIcrop henyl-phenylether
Chrysene
Dibenz(a,h)anth racene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
HexachIoro-1,3-butadiene
HexachIorocyclopentadiene
Hexachloroethane
Ind eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a mine
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-methyl phen of
2-Chorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
Result (dry)
mg/kg
U
U
0.344
0.0301
U
U
U
U
U
U
0.759
0.0112
U
U
U
U
0.111
U
U
U
U
U
U
0.202
U
U
U
U
U
U
0.734
U
U
U
U
U
U
U
U
U
U
U
U
40.4
37.1
36.6
41.3
43.5
50.3
Qualifier MDL (dry)
RDL (dry)
mg/kg
mg/kg
0.00842
0.0479
0.0167
0.479
0.00953
0.0479
J 0.0133
0.0479
0.0142
0.479
0.0145
0.479
0.0143
0.479
0.0177
0.479
0.0138
0.479
0.0157
0.479
0.00865
0.0479
J 0.00780
0.0479
0.0170
0.479
0.0161
0.479
0.0252
0.479
0.0189
0.479
0.0135
0.0479
0.0147
0.479
0.0120
0.0479
0.0167
0.479
0.0711
0.479
0.0363
0.479
0.0160
0.479
0.00952
0.0479
0.0150
0.479
0.0608
0.479
0.0164
0.479
0.0158
0.479
0.102
0.479
0.0324
0.479
0.00933
0.0479
0.0150
0.479
0.0156
0.479
0.0158
0.479
0.0140
0.479
0.0125
0.479
0.109
0.479
0.112
0.479
0.0171
0.479
0.0150
0.479
0.0129
0.479
0.0193
0.479
0.0154
0.479
12.0-120
10.0-120
10.0-122
15.0-120
10.0-127
10.0-120
Dilution Analysis Batch
date / time
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
05/19/2023 20:54
0511912023 20:54
0511912023 20:54
0511912023 20:54
0511912023 20:54
0511912023 20:54
0511912023 20:54
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
21 of 132

SAMPLE RESULTS - 05
L1616119
TW-5(5-7.5)
Collected date/time: 05/11/23 14:10
Total Solids by Method 2540 G-2011
Result
Analyte
Total Solids 79.9
Wet Chemistry by Method 7199
Qualifier Dilution Analysis
date / time
1 05/16/202316:32
Batch
WG2060621
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Hexavalent Chromium 1.22
J 0.319
1.25
1 05/17/202318:49
WG2061030
Mercury by Method 7471B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Mercury U
0.0225
0.0501
1 06/05/202318:13
WG2061958
Metals (ICPMS) by Method 6020B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
_ mg/kg
mg/kg
mg/kg
date / time
Arsenic
5.44
0.125
1.25
5
05/17/2023 20:44
WG2061326
Barium
20.3
0.190
3.13
5
05/17/2023 20:44
WG2061326
Cadmium
U
0.107
1.25
5
05/17/2023 20:44
WG2061326
Chromium
20.1
0.371
6.26
5
05/17/2023 20:44
WG2061326
Lead
6.99
0.124
2.50
5
05/17/2023 20:44
WG2061326
Selenium
0.698
1_ 0.225
3.13
5
05/17/2023 20:44
WG2061326
Silver
U
0.108
0.626
5
05/17/2023 20:44
WG2061326
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acetone
U
C3 J3
0.0569
0.0779
1 05/18/2023 22:39
WG2062683
Acrylonitrile
U
0.00562
0.0195
1 05/18/2023 22:39
WG2062683
Benzene
U
0.000728
0.00156
1 05/18/2023 22:39
WG2062683
Bromobenzene
U
0.00140
0.0195
1 05/18/2023 22:39
WG2062683
Bromodichloromethane
U
0.00113
0.00389
1 05/18/2023 22:39
WG2062683
Bromoform
U
0.00182
0.0389
1 05/18/2023 22:39
WG2062683
Bromomethane
U
0.00307
0.0195
1 05/18/2023 22:39
WG2062683
n-Butylbenzene
U
0.00818
0.0195
1 05/18/2023 22:39
WG2062683
sec -Butyl benzene
U
0.00449
0.0195
1 05/18/2023 22:39
WG2062683
ter[-Butylbenzene
U
0.00304
0.00779
1 05/18/2023 22:39
WG2062683
Carbon tetrachloride
U
0.00140
0.00779
1 05/18/2023 22:39
WG2062683
Chlorobenzene
U
0.000327
0.00389
1 05/18/2023 22:39
WG2062683
Chlorodibromomethane
U
0.000953
0.00389
1 05/18/2023 22:39
WG2062683
Chloroethane
U
0.00265
0.00779
1 05/18/2023 22:39
WG2062683
Chloroform
U
0.00160
0.00389
1 05/18/2023 22:39
WG2062683
Chloromethane
U
J3
0.00678
0.0195
1 05/18/2023 22:39
WG2062683
2-Chlorotoluene
U
0.00135
0.00389
1 05/18/2023 22:39
WG2062683
4-Chlorotoluene
U
0.000701
0.00779
1 05/18/2023 22:39
WG2062683
1,2-Dibromo-3-Chloropropane
U
C3
0.00608
0.0389
1 05/18/2023 22:39
WG2062683
1,2-Dibromoethane
U
0.00101
0.00389
1 05/18/2023 22:39
WG2062683
Dibromomethane
U
0.00117
0.00779
1 05/18/2023 22:39
WG2062683
1,2-Dichlorobenzene
U
0.000662
0.00779
1 05/18/2023 22:39
WG2062683
1,3-Dichlorobenzene
U
0.000935
0.00779
1 05/18/2023 22:39
WG2062683
1,4-Dichlorobenzene
U
0.00109
0.00779
1 05/18/2023 22:39
WG2062683
Dichlorodifluoromethane
U
0.00251
0.00389
1 05/18/2023 22:39
WG2062683
1,1-Dichloroethane
U
0.000765
0.00389
1 05/18/2023 22:39
WG2062683
1,2-Dichloroethane
U
0.00101
0.00389
1 05/18/2023 22:39
WG2062683
1,1-Dichloroethene
U
0.000944
0.00389
1 05/18/2023 22:39
WG2062683
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
FP1
FTC
FSS
4
Cn
rqc
F,
FAI
FSC
PAGE:
22 of 132

TW-5(5-7.5) SAMPLE RESULTS - 05
Collected date/time: 05/11/23 14:10 L1616119
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
cis-1,2-Dichloroethene
U
C3 J4
0.00114
0.00389
1 05/18/2023 22:39
WG2062683
trans-1,2-Dichloroethene
U
0.00162
0.00779
1 05/18/2023 22:39
WG2062683
1,2-Dichloropropane
U
0.00221
0.00779
1 05/18/2023 22:39
WG2062683
1,1-Dichloropropene
U
0.00126
0.00389
1 05/18/2023 22:39
WG2062683
1,3-Dichloropropane
U
0.000780
0.00779
1 05/18/2023 22:39
WG2062683
cis-1,3-Dichloropropene
U
0.00118
0.00389
1 05/18/2023 22:39
WG2062683
trans-1,3-Dichloropropene
U
0.00178
0.00779
1 05/18/2023 22:39
WG2062683
2,2-Dichloropropane
U
0.00215
0.00389
1 05/18/2023 22:39
WG2062683
Di -isopropyl ether
U
0.000639
0.00156
1 05/18/2023 22:39
WG2062683
Ethylbenzene
U
0.00115
0.00389
1 05/18/2023 22:39
WG2062683
Hexachloro-1,3-butadiene
U
0.00935
0.0389
1 05/18/2023 22:39
WG2062683
Isopropylbenzene
U
0.000662
0.00389
1 05/18/2023 22:39
WG2062683
p-Isopropyltoluene
U
0.00397
0.00779
1 05/18/2023 22:39
WG2062683
2-Butanone (MEK)
U
0.0989
0.156
1 05/18/2023 22:39
WG2062683
Methylene Chloride
U
0.0103
0.0389
1 05/18/2023 22:39
WG2062683
4-Methyl-2-pentanone (MIBK)
U
0.00355
0.0389
1 05/18/2023 22:39
WG2062683
Methyl tert-butyl ether
U
0.000545
0.00156
1 05/18/2023 22:39
WG2062683
Naphthalene
U
C3
0.00760
0.0195
1 05/18/2023 22:39
WG2062683
n-Propylbenzene
U
0.00148
0.00779
1 05/18/2023 22:39
WG2062683
Styrene
U
C3
0.000357
0.0195
1 05/18/2023 22:39
WG2062683
1,1,1,2-Tetrachloroethane
U
0.00148
0.00389
1 05/18/2023 22:39
WG2062683
1,1,2,2-Tetrachloroethane
U
0.00108
0.00389
1 05/18/2023 22:39
WG2062683
Tetrachloroethene
U
0.00140
0.00389
1 05/18/2023 22:39
WG2062683
Toluene
U
0.00203
0.00779
1 05/18/2023 22:39
WG2062683
1,2,3-Trichlorobenzene
U
C3
0.0114
0.0195
1 05/18/2023 22:39
WG2062683
1,2,4-Trichlorobenzene
U
C3
0.00685
0.0195
1 05/18/2023 22:39
WG2062683
1,1,1-Trichloroethane
U
0.00144
0.00389
1 05/18/2023 22:39
WG2062683
1,1,2-Trichloroethane
U
0.000930
0.00389
1 05/18/2023 22:39
WG2062683
1,1,2-Trichlorotrifluoroethane
U
0.00117
0.00389
1 05/18/2023 22:39
WG2062683
Trichloroethene
U
0.000910
0.00156
1 05/18/2023 22:39
WG2062683
Trichlorofluoromethane
U
0.00129
0.00389
1 05/18/2023 22:39
WG2062683
1,2,3-Trichloropropane
U
0.00252
0.0195
1 05/18/2023 22:39
WG2062683
1,2,4-Trimethylbenzene
U
0.00246
0.00779
1 05/18/2023 22:39
WG2062683
1,3,5-Trimethyl benzene
U
0.00312
0.00779
1 05/18/2023 22:39
WG2062683
Vinyl chloride
U
0.00181
0.00389
1 05/18/2023 22:39
WG2062683
Xylenes, Total
U
0.00137
0.0101
1 05/18/2023 22:39
WG2062683
(S) Toluene-d8
103
75.0-131
05118120232239
WG2062683
(S)4-Bromof/uorobenzene
91.3
67.0-138
051181202322:39
WG2062683
(S)1,2-Dich/oroethone-d4
87.4
70.0-130
05118120232239
WG2062683
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acenaphthene
U
0.00675
0.0417
1 05/19/202319:51
WG2062836
Acenaphthylene
U
0.00587
0.0417
1 05/19/202319:51
WG2062836
Anthracene
U
0.00742
0.0417
1 05/19/202319:51
WG2062836
Benzidine
U
0.0784
2.09
1 05/19/202319:51
WG2062836
Benzo(a)anth race ne
U
0.00735
0.0417
1 05/19/202319:51
WG2062836
Benzo(b)fluoranthene
U
0.00777
0.0417
1 05/19/202319:51
WG2062836
Benzo(k)fluoranthene
U
0.00741
0.0417
1 05/19/202319:51
WG2062836
Benzo(g,h,i)perylene
U
0.00762
0.0417
1 05/19/202319:51
WG2062836
Benzo(a)pyrene
U
0.00775
0.0417
1 05/19/202319:51
WG2062836
Bis(2-chlorethoxy)methane
U
0.0125
0.417
1 05/19/202319:51
WG2062836
Bis(2-chloroethyl)ether
U
0.0138
0.417
1 05/19/202319:51
WG2062836
2,2-Oxybis(1-Chloropropane)
U
0.0180
0.417
1 05/19/202319:51
WG2062836
4-Bromophenyl-phenylether
U
0.0146
0.417
1 05/19/202319:51
WG2062836
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
FP1
FTc
FSS
4
Cn
Rc
F ql
FAI
FSC
PAGE:
23 of 132

TW-5(5-7.5) SAMPLE RESULTS - 05
Collected date/time: 05/11/23 14:10 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
2-Chloronaphthalene
4-ChIcrop henyl-phenylether
Chrysene
Dibenz(a,h)anth racene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
HexachIoro-1,3-butadiene
HexachIorocyclopentadiene
Hexachloroethane
Ind eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a mine
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-methyl phen of
2-Chorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
46.3
40.7
42.4
47.9
42.2
55.5
Qualifier MDL (dry)
RDL (dry)
mg/kg
mg/kg
0.00732
0.0417
0.0145
0.417
0.00829
0.0417
0.0116
0.0417
0.0124
0.417
0.0126
0.417
0.0124
0.417
0.0154
0.417
0.0120
0.417
0.0136
0.417
0.00752
0.0417
0.00678
0.0417
0.0148
0.417
0.0140
0.417
0.0219
0.417
0.0164
0.417
0.0118
0.0417
0.0128
0.417
0.0105
0.0417
0.0145
0.417
0.0618
0.417
0.0315
0.417
0.0139
0.417
0.00827
0.0417
0.0130
0.417
0.0528
0.417
0.0143
0.417
0.0138
0.417
0.0884
0.417
0.0282
0.417
0.00811
0.0417
0.0130
0.417
0.0135
0.417
0.0138
0.417
0.0121
0.417
0.0109
0.417
0.0945
0.417
0.0975
0.417
0.0149
0.417
0.0130
0.417
0.0112
0.417
0.0168
0.417
0.0134
0.417
12.0-120
10.0-120
10.0-122
15.0-120
10.0-127
10.0-120
Dilution Analysis Batch
date / time
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
05/19/202319:51
051191202319:51
051191202319:51
051191202319:51
051191202319:51
051191202319:51
051191202319:51
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
WG2062836
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
24 of 132

SAMPLE RESULTS - 06
L1616119
TW-6(5-7.5)
Collected date/time: 05/11/23 15:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 75.5 1 05/16/202316:32 WG2060621
Wet Chemistry by Method 7199
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Hexavalent Chromium 0.843
J 0.338
1.32
1 05/17/202318:54
WG2061030
Mercury by Method 7471B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date/time
Mercury U
0.0238
0.0530
1 06/04/202318:07
WG2059805
Metals (ICPMS) by Method 6020B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
_ mg/kg
mg/kg
mg/kg
date / time
Arsenic
8.77
0.132
1.32
5
05/17/2023 20:48
WG2061326
Barium
17.8
0.201
3.31
5
05/17/2023 20:48
WG2061326
Cadmium
U
0.113
1.32
5
05/17/2023 20:48
WG2061326
Chromium
52.6
0.392
6.62
5
05/17/2023 20:48
WG2061326
Lead
11.2
0.131
2.65
5
05/17/2023 20:48
WG2061326
Selenium
1.56
1_ 0.238
3.31
5
05/17/2023 20:48
WG2061326
Silver
U
0.115
0.662
5
05/17/2023 20:48
WG2061326
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acetone
U
0.0627
0.0858
1 05/19/2023 22:06
WG2063443
Acrylonitrile
U
0.00620
0.0215
1 05/19/2023 22:06
WG2063443
Benzene
U
0.000802
0.00172
1 05/19/2023 22:06
WG2063443
Bromobenzene
U
0.00155
0.0215
1 05/19/2023 22:06
WG2063443
Bromodichloromethane
U
0.00124
0.00429
1 05/19/2023 22:06
WG2063443
Bromoform
U
C3
0.00201
0.0429
1 05/19/2023 22:06
WG2063443
Bromomethane
U
0.00338
0.0215
1 05/19/2023 22:06
WG2063443
n-Butylbenzene
U
0.00901
0.0215
1 05/19/2023 22:06
WG2063443
sec -Butyl benzene
U
0.00494
0.0215
1 05/19/2023 22:06
WG2063443
ter[-Butylbenzene
U
0.00335
0.00858
1 05/19/2023 22:06
WG2063443
Carbon tetrachloride
U
0.00154
0.00858
1 05/19/2023 22:06
WG2063443
Chlorobenzene
U
0.000361
0.00429
1 05/19/2023 22:06
WG2063443
Chlorodibromomethane
U
0.00105
0.00429
1 05/19/2023 22:06
WG2063443
Chloroethane
U
0.00292
0.00858
1 05/19/2023 22:06
WG2063443
Chloroform
U
0.00177
0.00429
1 05/19/2023 22:06
WG2063443
Chloromethane
U
0.00747
0.0215
1 05/19/2023 22:06
WG2063443
2-Chlorotoluene
U
0.00149
0.00429
1 05/19/2023 22:06
WG2063443
4-Chlorotoluene
U
0.000773
0.00858
1 05/19/2023 22:06
WG2063443
1,2-Dibromo-3-Chloropropane
U
C3
0.00670
0.0429
1 05/19/2023 22:06
WG2063443
1,2-Dibromoethane
U
0.00111
0.00429
1 05/19/2023 22:06
WG2063443
Dibromomethane
U
0.00129
0.00858
1 05/19/2023 22:06
WG2063443
1,2-Dichlorobenzene
U
0.000730
0.00858
1 05/19/2023 22:06
WG2063443
1,3-Dichlorobenzene
U
0.00103
0.00858
1 05/19/2023 22:06
WG2063443
1,4-Dichlorobenzene
U
0.00120
0.00858
1 05/19/2023 22:06
WG2063443
Dichlorodifluoromethane
U
C3
0.00276
0.00429
1 05/19/2023 22:06
WG2063443
1,1-Dichloroethane
U
0.000843
0.00429
1 05/19/2023 22:06
WG2063443
1,2-Dichloroethane
U
0.00111
0.00429
1 05/19/2023 22:06
WG2063443
1,1-Dichloroethene
U
0.00104
0.00429
1 05/19/2023 22:06
WG2063443
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
FP1
FTc
FSS
4
Cn
rqc
F,
FAI
FSC
25 of 132

TW-6(5-7.5) SAMPLE RESULTS - 06
Collected date/time: 05/11/23 15:15 L1616119
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Analyte
mg/kg
mg/kg
mg/kg
cis-1,2-Dichloroethene
U
0.00126
0.00429
trans-1,2-Dichloroethene
U
0.00179
0.00858
1,2-Dichloropropane
U
0.00244
0.00858
1,1-Dichloropropene
U
0.00139
0.00429
1,3-Dichloropropane
U
0.000860
0.00858
cis-1,3-Dichloropropene
U
0.00130
0.00429
trans-1,3-Dichloropropene
U
0.00196
0.00858
2,2-Dichloropropane
U
0.00237
0.00429
Di -isopropyl ether
U
0.000704
0.00172
Ethylbenzene
U
0.00127
0.00429
Hexachloro-1,3-butadiene
U
0.0103
0.0429
Isopropylbenzene
U
0.000730
0.00429
p-Isopropyltoluene
U
0.00438
0.00858
2-Butanone (MEK)
U
0.109
0.172
Methylene Chloride
U
0.0114
0.0429
4-Methyl-2-pentanone (MIBK)
U
0.00391
0.0429
Methyl tert-butyl ether
U
0.000601
0.00172
Naphthalene
U
0.00838
0.0215
n-Propylbenzene
U
0.00163
0.00858
Styrene
U
0.000393
0.0215
1,1,1,2-Tetrachloroethane
U
0.00163
0.00429
1,1,2,2-Tetrachloroethane
U
0.00119
0.00429
Tetrachloroethene
U
0.00154
0.00429
Toluene
U
0.00223
0.00858
1,2,3-Trichlorobenzene
U
0.0126
0.0215
1,2,4-Trichlorobenzene
U
0.00755
0.0215
1,1,1-Trichloroethane
U
0.00158
0.00429
1,1,2-Trichloroethane
U
0.00102
0.00429
1,1,2-Trichlorotrifluoroethane
U
0.00129
0.00429
Trichloroethene
U
0.00100
0.00172
Trichlorofluoromethane
U
0.00142
0.00429
1,2,3-Trichloropropane
U
0.00278
0.0215
1,2,4-Trimethylbenzene
U
0.00271
0.00858
1,3,5-Trimethyl benzene
U
0.00343
0.00858
Vinyl chloride
U
0.00199
0.00429
Xylenes, Total
U
0.00151
0.0112
(S) Toluene-d8
102
75.0-131
(S) 4-Bromof/uorobenzene
95.3
67.0-138
(S) 1,2-Dich/oroethone-d4
107
70.0-130
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anth race ne
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis(2-chlorethoxy)methane
Bis(2-ch loroethyl)ether
2, 2-Oxybis(1-Ch I oropro pane)
4-Bromophenyl-phenylether
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
ACCOUNT:
Withers & Ravenel Eng. - Standard
Qualifier MDL (dry)
mg/kg
0.00714
0.00621
0.00786
0.0829
0.00778
0.00823
0.00784
0.00807
0.00820
0.0132
0.0146
0.0191
0.0155
PROJECT:
23-0302
RDL (dry)
mg/kg
0.0441
0.0441
0.0441
2.21
0.0441
0.0441
0.0441
0.0441
0.0441
0.441
0.441
0.441
0.441
Dilution Analysis
date / time
Batch
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
1 05/19/2023 22:06
WG2063443
051191202322:06
WG2063443
051191202322:06
WG2063443
051191202322:06
WG2063443
Dilution Analysis
date / time
Batch
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
1 05/19/2023 23:52
WG2063159
SDG:
DATE/TIME:
L1616119
06/06/23 12:28
FP1
FTc
FSS
4
Cn
Rc
I ql
FAI
FSC
PAGE:
26 of 132

TW-6(5-7.5)
Collected date/time: 05/11/23 15:15
Semi Volatile Organic Compounds
SAMPLE RESULTS
L1616119
(GC/MS) by Method 8270E
- 06
Result (dry)
Qualifier MDL (dry)
RDL (dry) Dilution Analysis
Batch
Cp
Analyte
mg/kg
mg/kg
mg/kg
date / time
2-Chloronaphthalene
U
0.00775
0.0441 1
05/19/2023 23:52
WG2063159
z
Tc
4-C h I o ro p h e nyl -p h e nyl et h e r
U
0.0154
0.441 1
05/19/2023 23:52
WG2063159
Chrysene
U
0.00877
0.0441 1
05/19/2023 23:52
WG2063159
Dibenz(a,h)anthracene
U
0.0122
0.0441 1
05/19/2023 23:52
WG2063159
F
1,2-Dichlorobenzene
U
0.0131
0.441 1
05/19/2023 23:52
WG2063159
1,3-Dichlorobenzene
U
0.0134
0.441 1
05/19/2023 23:52
WG2063159
4
Cn
1,4-Dichlorobenzene
U
0.0131
0.441 1
05/19/2023 23:52
WG2063159
3,3-D1chIorobenzidine
U
0.0163
0.441 1
05/19/2023 23:52
WG2063159
2,4-Dinitrotoluene
U
0.0127
0.441 1
05/19/2023 23:52
WG2063159
2,6-Dinitrotoluene
U
0.0144
0.441 1
05/19/2023 23:52
WG2063159
Fluoranthene
U
0.00796
0.0441 1
05/19/2023 23:52
WG2063159
h
QC
Fluorene
U
0.00718
0.0441 1
05/19/2023 23:52
WG2063159
Hexachlorobenzene
U
0.0156
0.441 1
05/19/2023 23:52
WG2063159
HexachIoro-1,Ibutadiene
U
0.0148
0.441 1
05/19/2023 23:52
WG2063159
GI
H exa c h I o rocyc I o p e nta d i e n e
U
0.0232
0.441 1
05/19/2023 23:52
WG2063159
Hexachloroethane
U
0.0174
0.441 1
05/19/2023 23:52
WG2063159
FAI
Indeno(1,2,3-cd)pyre ne
U
0.0125
0.0441 1
05/19/2023 23:52
WG2063159
Isophorone
U
0.0135
0.441 1
05/19/2023 23:52
WG2063159
Naphthalene
U
0.0111
0.0441 1
05/19/2023 23:52
WG2063159
FSC
Nitrobenzene
U
0.0154
0.441 1
05/19/2023 23:52
WG2063159
n-Nitrosodimethyla mine
U
0.0655
0.441 1
05/19/2023 23:52
WG2063159
n-Nitrosodiphenyla mine
U
0.0334
0.441 1
05/19/2023 23:52
WG2063159
n-Nitrosodi-n-propylamine
U
0.0147
0.441 1
05/19/2023 23:52
WG2063159
Phenanthrene
U
0.00876
0.0441 1
05/19/2023 23:52
WG2063159
Benzylbutyl phthalate
U
0.0138
0.441 1
05/19/2023 23:52
WG2063159
Bis(2-ethylhexyl)phthalate
U
0.0559
0.441 1
05/19/2023 23:52
WG2063159
Di-n-butyl phthalate
U
0.0151
0.441 1
05/19/2023 23:52
WG2063159
Diethyl phthalate
U
0.0146
0.441 1
05/19/2023 23:52
WG2063159
Dimethyl phthalate
U
0.0935
0.441 1
05/19/2023 23:52
WG2063159
Di-n-octyl phthalate
U
0.0298
0.441 1
05/19/2023 23:52
WG2063159
Pyrene
U
0.00859
0.0441 1
05/19/2023 23:52
WG2063159
1,2,4-Trichlorobenzene
U
0.0138
0.441 1
05/19/2023 23:52
WG2063159
4-Chloro-3-methylphenol
U
0.0143
0.441 1
05/19/2023 23:52
WG2063159
2-Chorophenol
U
0.0146
0.441 1
05/19/2023 23:52
WG2063159
2,4-Dichlorophenol
U
0.0129
0.441 1
05/19/2023 23:52
WG2063159
2,4-Dimethylphenol
U
0.0115
0.441 1
05/19/2023 23:52
WG2063159
4,6-Dinitro-2-methylphenol
U
0.100
0.441 1
05/19/2023 23:52
WG2063159
2,4-Dinitrophenol
U
0.103
0.441 1
05/19/2023 23:52
WG2063159
2-Nitrophenol
U
0.0158
0.441 1
05/19/2023 23:52
WG2063159
4-Nitrophenol
U
0.0138
0.441 1
05/19/2023 23:52
WG2063159
Pentachlorophenol
U
0.0119
0.441 1
05/19/2023 23:52
WG2063159
Phenol
U
0.0178
0.441 1
05/19/2023 23:52
WG2063159
2,4,6-Trichlorophenol
U
0.0142
0.441 1
05/19/2023 23:52
WG2063159
(S)2-Fluorophenol
45.3
12.0-120
051191202323.52
WG2063159
(S)Phenol-d5
43.3
10.0-120
051191202323.52
WG2063159
(S)Nitrobenzene-d5
43.4
10.0-122
051191202323.52
WG2063159
(S)2-F/uorobipheny/
40.9
15.0-120
051191202323.52
WG2063159
(S)2,4,6-Tribromopheno/
52.0
10.0-127
051191202323.52
WG2063159
(S)p-Terphenyl-d14
53.7
10.0-120
051191202323.52
WG2063159
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
27 of 132

SAMPLE RESULTS - 07
L1616119
TW-7(5-7.5)
Collected date/time: 05/12/23 09:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 70.7 1 05/16/202315:46 WG2060827
Wet Chemistry by Method 7199
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Hexavalent Chromium 0.507
J P1 0.361
1.41
1 05/17/202318:59 WG2061030
Mercury by Method 7471B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis Batch
Analyte mg/kg
mg/kg
mg/kg
date/time
Mercury 0.0410 J
Metals (ICPMS) by Method 6020B
0.0255 0.0566 1 06/04/202318:09 WG2059805
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
_ mg/kg
mg/kg
mg/kg
date / time
Arsenic
17.7
0.141
1.41
5
05/17/2023 20:51
WG2061326
Barium
30.5
0.215
3.54
5
05/17/2023 20:51
WG2061326
Cadmium
U
0.121
1.41
5
05/17/2023 20:51
WG2061326
Chromium
36.8
0.419
7.07
5
05/17/2023 20:51
WG2061326
Lead
16.3
0.140
2.83
5
05/17/2023 20:51
WG2061326
Selenium
2.02
1_ 0.255
3.54
5
05/17/2023 20:51
WG2061326
Silver
U
0.122
0.707
5
05/17/2023 20:51
WG2061326
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acetone
U
0.0690
0.0945
1 05/19/2023 22:28
WG2063443
Acrylonitrile
U
0.00682
0.0236
1 05/19/2023 22:28
WG2063443
Benzene
U
0.000882
0.00189
1 05/19/2023 22:28
WG2063443
Bromobenzene
U
0.00170
0.0236
1 05/19/2023 22:28
WG2063443
Bromodichloromethane
U
0.00137
0.00472
1 05/19/2023 22:28
WG2063443
Bromoform
U
C3
0.00221
0.0472
1 05/19/2023 22:28
WG2063443
Bromomethane
U
0.00372
0.0236
1 05/19/2023 22:28
WG2063443
n-Butylbenzene
U
0.00992
0.0236
1 05/19/2023 22:28
WG2063443
sec -Butyl benzene
U
0.00544
0.0236
1 05/19/2023 22:28
WG2063443
ter[-Butylbenzene
U
0.00368
0.00945
1 05/19/2023 22:28
WG2063443
Carbon tetrachloride
U
0.00170
0.00945
1 05/19/2023 22:28
WG2063443
Chlorobenzene
U
0.000397
0.00472
1 05/19/2023 22:28
WG2063443
Chlorodibromomethane
U
0.00116
0.00472
1 05/19/2023 22:28
WG2063443
Chloroethane
U
0.00321
0.00945
1 05/19/2023 22:28
WG2063443
Chloroform
U
0.00195
0.00472
1 05/19/2023 22:28
WG2063443
Chloromethane
U
0.00822
0.0236
1 05/19/2023 22:28
WG2063443
2-Chlorotoluene
U
0.00163
0.00472
1 05/19/2023 22:28
WG2063443
4-Chlorotoluene
U
0.000850
0.00945
1 05/19/2023 22:28
WG2063443
1,2-Dibromo-3-Chloropropane
U
C3
0.00737
0.0472
1 05/19/2023 22:28
WG2063443
1,2-Dibromoethane
U
0.00122
0.00472
1 05/19/2023 22:28
WG2063443
Dibromomethane
U
0.00142
0.00945
1 05/19/2023 22:28
WG2063443
1,2-Dichlorobenzene
U
0.000803
0.00945
1 05/19/2023 22:28
WG2063443
1,3-Dichlorobenzene
U
0.00113
0.00945
1 05/19/2023 22:28
WG2063443
1,4-Dichlorobenzene
U
0.00132
0.00945
1 05/19/2023 22:28
WG2063443
Dichlorodifluoromethane
U
C3
0.00304
0.00472
1 05/19/2023 22:28
WG2063443
1,1-Dichloroethane
U
0.000928
0.00472
1 05/19/2023 22:28
WG2063443
1,2-Dichloroethane
U
0.00123
0.00472
1 05/19/2023 22:28
WG2063443
1,1-Dichloroethene
U
0.00115
0.00472
1 05/19/2023 22:28
WG2063443
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
FP1
FTC
FSS
4
Cn
rqc
F,
FAI
FSC
NAU=:
28 of 132

TW-7(5-7.5) SAMPLE RESULTS - 07
Collected date/time: 05/12/23 09:15 L1616119
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
cis-1,2-Dichloroethene
U
0.00139
0.00472
1 05/19/2023 22:28
WG2063443
trans-1,2-Dichloroethene
U
0.00197
0.00945
1 05/19/2023 22:28
WG2063443
1,2-Dichloropropane
U
0.00268
0.00945
1 05/19/2023 22:28
WG2063443
1,1-Dichloropropene
U
0.00153
0.00472
1 05/19/2023 22:28
WG2063443
1,3-Dichloropropane
U
0.000947
0.00945
1 05/19/2023 22:28
WG2063443
cis-1,3-Dichloropropene
U
0.00143
0.00472
1 05/19/2023 22:28
WG2063443
trans-1,3-Dichloropropene
U
0.00215
0.00945
1 05/19/2023 22:28
WG2063443
2,2-Dichloropropane
U
0.00261
0.00472
1 05/19/2023 22:28
WG2063443
Di -isopropyl ether
U
0.000775
0.00189
1 05/19/2023 22:28
WG2063443
Ethylbenzene
U
0.00139
0.00472
1 05/19/2023 22:28
WG2063443
Hexachloro-1,3-butadiene
U
0.0113
0.0472
1 05/19/2023 22:28
WG2063443
Isopropylbenzene
U
0.000803
0.00472
1 05/19/2023 22:28
WG2063443
p-Isopropyltoluene
U
0.00482
0.00945
1 05/19/2023 22:28
WG2063443
2-Butanone (MEK)
U
0.120
0.189
1 05/19/2023 22:28
WG2063443
Methylene Chloride
U
0.0125
0.0472
1 05/19/2023 22:28
WG2063443
4-Methyl-2-pentanone (MIBK)
U
0.00431
0.0472
1 05/19/2023 22:28
WG2063443
Methyl tert-butyl ether
U
0.000661
0.00189
1 05/19/2023 22:28
WG2063443
Naphthalene
U
0.00922
0.0236
1 05/19/2023 22:28
WG2063443
n-Propylbenzene
U
0.00180
0.00945
1 05/19/2023 22:28
WG2063443
Styrene
U
0.000433
0.0236
1 05/19/2023 22:28
WG2063443
1,1,1,2-Tetrachloroethane
U
0.00179
0.00472
1 05/19/2023 22:28
WG2063443
1,1,2,2-Tetrachloroethane
U
0.00131
0.00472
1 05/19/2023 22:28
WG2063443
Tetrachloroethene
U
0.00169
0.00472
1 05/19/2023 22:28
WG2063443
Toluene
U
0.00246
0.00945
1 05/19/2023 22:28
WG2063443
1,2,3-Trichlorobenzene
U
0.0139
0.0236
1 05/19/2023 22:28
WG2063443
1,2,4-Trichlorobenzene
U
0.00831
0.0236
1 05/19/2023 22:28
WG2063443
1,1,1-Trichloroethane
U
0.00174
0.00472
1 05/19/2023 22:28
WG2063443
1,1,2-Trichloroethane
U
0.00113
0.00472
1 05/19/2023 22:28
WG2063443
1,1,2-Trichlorotrifluoroethane
U
0.00142
0.00472
1 05/19/2023 22:28
WG2063443
Trichloroethene
U
0.00110
0.00189
1 05/19/2023 22:28
WG2063443
Trichlorofluoromethane
U
0.00156
0.00472
1 05/19/2023 22:28
WG2063443
1,2,3-Trichloropropane
U
0.00306
0.0236
1 05/19/2023 22:28
WG2063443
1,2,4-Trimethylbenzene
U
0.00299
0.00945
1 05/19/2023 22:28
WG2063443
1,3,5-Trimethyl benzene
U
0.00378
0.00945
1 05/19/2023 22:28
WG2063443
Vinyl chloride
U
0.00219
0.00472
1 05/19/2023 22:28
WG2063443
Xylenes, Total
U
0.00166
0.0123
1 05/19/2023 22:28
WG2063443
(S)Toluene-d8
107
75.0-131
051191202322:28
WG2063443
(S)4-Bromof/uorobenzene
96.1
67.0-138
051191202322:28
WG2063443
(S)1,2-Dich/oroethone-d4
108
70.0-130
051191202322:28
WG2063443
Semi Volatile Organic Compounds
(GC/MS) by Method
8270E
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acenaphthene
U
0.00763
0.0471
1 05/20/2023 00:13
WG2063159
Acenaphthylene
U
0.00664
0.0471
1 05/20/2023 00:13
WG2063159
Anthracene
U
0.00839
0.0471
1 05/20/2023 00:13
WG2063159
Benzidine
U
0.0886
2.36
1 05/20/2023 00:13
WG2063159
Benzo(a)anth race ne
U
0.00830
0.0471
1 05/20/2023 00:13
WG2063159
Benzo(b)fluoranthene
U
0.00879
0.0471
1 05/20/2023 00:13
WG2063159
Benzo(k)fluoranthene
U
0.00838
0.0471
1 05/20/2023 00:13
WG2063159
Benzo(g,h,i)perylene
U
0.00862
0.0471
1 05/20/2023 00:13
WG2063159
Benzo(a)pyrene
U
0.00876
0.0471
1 05/20/2023 00:13
WG2063159
Bis(2-chlorethoxy)methane
U
0.0141
0.471
1 05/20/2023 00:13
WG2063159
Bis(2-chloroethyl)ether
U
0.0156
0.471
1 05/20/2023 00:13
WG2063159
2,2-Oxybis(1-Chloropropane)
U
0.0204
0.471
1 05/20/2023 00:13
WG2063159
4-Bromophenyl-phenylether
U
0.0166
0.471
1 05/20/2023 00:13
WG2063159
FP1
FTc
FSS
4
Cn
Rc
I ql
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 29 of 132

TW-7(5-7.5) SAMPLE RESULTS - 07
Collected date/time: 05/12/23 09:15 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
2-Chloronaphthalene
4-ChIcrop henyl-phenylether
Chrysene
Dibenz(a,h)anth racene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
HexachIoro-1,3-butadiene
HexachIorocyclopentadiene
Hexachloroethane
Ind eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a mine
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-methyl phen of
2-Chorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
48.9
47.1
477
45.6
62.0
57.4
Qualifier MDL (dry)
RDL (dry)
mg/kg
mg/kg
0.00828
0.0471
0.0164
0.471
0.00937
0.0471
0.0131
0.0471
0.0140
0.471
0.0143
0.471
0.0140
0.471
0.0174
0.471
0.0135
0.471
0.0154
0.471
0.00850
0.0471
0.00767
0.0471
0.0167
0.471
0.0158
0.471
0.0248
0.471
0.0185
0.471
0.0133
0.0471
0.0144
0.471
0.0118
0.0471
0.0164
0.471
0.0699
0.471
0.0357
0.471
0.0157
0.471
0.00935
0.0471
0.0147
0.471
0.0597
0.471
0.0161
0.471
0.0156
0.471
0.0999
0.471
0.0318
0.471
0.00917
0.0471
0.0147
0.471
0.0153
0.471
0.0156
0.471
0.0137
0.471
0.0123
0.471
0.107
0.471
0.110
0.471
0.0168
0.471
0.0147
0.471
0.0127
0.471
0.0190
0.471
0.0151
0.471
12.0-120
10.0-120
10.0-122
15.0-120
10.0-127
10.0-120
Dilution Analysis Batch
date / time
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
05/20/2023 00:13
0512012023 00:13
0512012023 00:13
0512012023 00:13
0512012023 00:13
0512012023 00:13
0512012023 00:13
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
30 of 132

SAMPLE RESULTS - 08
L1616119
TW-8(5-7.5)
Collected date/time: 05/12/23 10:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 77.0 1 05/16/202315:46 WG2060827
Wet Chemistry by Method 7199
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Hexavalent Chromium 1.81
0.331
1.30
1 05/17/202319:20
WG2061030
Mercury by Method 7471B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Mercury 0.0719
0.0234
0.0520
1 06/05/202318:16
WG2061958
Metals (ICPMS) by Method 6020B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
_ mg/kg
mg/kg
mg/kg
date / time
Arsenic
85.5
0.130
1.30
5
05/17/2023 20:54
WG2061326
Barium
26.8
0.198
3.25
5
05/17/2023 20:54
WG2061326
Cadmium
U
0.111
1.30
5
05/17/2023 20:54
WG2061326
Chromium
41.8
0.385
6.50
5
05/17/2023 20:54
WG2061326
Lead
11.7
0.129
2.60
5
05/17/2023 20:54
WG2061326
Selenium
1.46
1_ 0.234
3.25
5
05/17/2023 20:54
WG2061326
Silver
U
0.112
0.650
5
05/17/2023 20:54
WG2061326
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acetone
U
0.0612
0.0839
1 05/19/2023 22:49
WG2063443
Acrylonitrile
U
0.00606
0.0210
1 05/19/2023 22:49
WG2063443
Benzene
U
0.000783
0.00168
1 05/19/2023 22:49
WG2063443
Bromobenzene
U
0.00151
0.0210
1 05/19/2023 22:49
WG2063443
Bromodichloromethane
U
0.00122
0.00419
1 05/19/2023 22:49
WG2063443
Bromoform
U
C3
0.00196
0.0419
1 05/19/2023 22:49
WG2063443
Bromomethane
U
0.00331
0.0210
1 05/19/2023 22:49
WG2063443
n-Butylbenzene
U
0.00881
0.0210
1 05/19/2023 22:49
WG2063443
sec -Butyl benzene
U
0.00483
0.0210
1 05/19/2023 22:49
WG2063443
ter[-Butylbenzene
0.00371
1_
0.00327
0.00839
1 05/19/2023 22:49
WG2063443
Carbon tetrachloride
U
0.00151
0.00839
1 05/19/2023 22:49
WG2063443
Chlorobenzene
U
0.000352
0.00419
1 05/19/2023 22:49
WG2063443
Chlorodibromomethane
U
0.00103
0.00419
1 05/19/2023 22:49
WG2063443
Chloroethane
U
0.00285
0.00839
1 05/19/2023 22:49
WG2063443
Chloroform
U
0.00173
0.00419
1 05/19/2023 22:49
WG2063443
Chloromethane
U
0.00730
0.0210
1 05/19/2023 22:49
WG2063443
2-Chlorotoluene
U
0.00145
0.00419
1 05/19/2023 22:49
WG2063443
4-Chlorotoluene
U
0.000755
0.00839
1 05/19/2023 22:49
WG2063443
1,2-Dibromo-3-Chloropropane
U
C3
0.00654
0.0419
1 05/19/2023 22:49
WG2063443
1,2-Dibromoethane
U
0.00109
0.00419
1 05/19/2023 22:49
WG2063443
Dibromomethane
U
0.00126
0.00839
1 05/19/2023 22:49
WG2063443
1,2-Dichlorobenzene
U
0.000713
0.00839
1 05/19/2023 22:49
WG2063443
1,3-Dichlorobenzene
U
0.00101
0.00839
1 05/19/2023 22:49
WG2063443
1,4-Dichlorobenzene
U
0.00117
0.00839
1 05/19/2023 22:49
WG2063443
Dichlorodifluoromethane
U
C3
0.00270
0.00419
1 05/19/2023 22:49
WG2063443
1,1-Dichloroethane
U
0.000824
0.00419
1 05/19/2023 22:49
WG2063443
1,2-Dichloroethane
U
0.00109
0.00419
1 05/19/2023 22:49
WG2063443
1,1-Dichloroethene
U
0.00102
0.00419
1 05/19/2023 22:49
WG2063443
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
FP1
FTC
FSS
4
Cn
rqc
F,
FAI
FSC
PAGE:
31 of 132

TW-8(5-7.5) SAMPLE RESULTS - 08
Collected date/time: 05/12/23 10:20 L1616119
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Analyte
mg/kg
mg/kg
mg/kg
cis-1,2-Dichloroethene
U
0.00123
0.00419
trans-1,2-Dichloroethene
U
0.00174
0.00839
1,2-Dichloropropane
U
0.00238
0.00839
1,1-Dichloropropene
U
0.00136
0.00419
1,3-Dichloropropane
U
0.000841
0.00839
cis-1,3-Dichloropropene
U
0.00127
0.00419
trans-1,3-Dichloropropene
U
0.00191
0.00839
2,2-Dichloropropane
U
0.00232
0.00419
Di -isopropyl ether
U
0.000688
0.00168
Ethylbenzene
U
0.00124
0.00419
Hexachloro-1,3-butadiene
U
0.0101
0.0419
Isopropylbenzene
U
0.000713
0.00419
p-Isopropyltoluene
U
0.00428
0.00839
2-Butanone (MEK)
U
0.107
0.168
Methylene Chloride
U
0.0111
0.0419
4-Methyl-2-pentanone (MIBK)
U
0.00383
0.0419
Methyl tert-butyl ether
U
0.000587
0.00168
Naphthalene
U
0.00819
0.0210
n-Propylbenzene
U
0.00159
0.00839
Styrene
U
0.000384
0.0210
1,1,1,2-Tetrachloroethane
U
0.00159
0.00419
1,1,2,2-Tetrachloroethane
U
0.00117
0.00419
Tetrachloroethene
U
0.00150
0.00419
Toluene
U
0.00218
0.00839
1,2,3-Trichlorobenzene
U
0.0123
0.0210
1,2,4-Trichlorobenzene
U
0.00738
0.0210
1,1,1-Trichloroethane
U
0.00155
0.00419
1,1,2-Trichloroethane
U
0.00100
0.00419
1,1,2-Trichlorotrifluoroethane
U
0.00126
0.00419
Trichloroethene
U
0.000980
0.00168
Trichlorofluoromethane
U
0.00139
0.00419
1,2,3-Trichloropropane
U
0.00272
0.0210
1,2,4-Trimethylbenzene
U
0.00265
0.00839
1,3,5-Trimethyl benzene
U
0.00336
0.00839
Vinyl chloride
U
0.00195
0.00419
Xylenes, Total
U
0.00148
0.0109
(S) Toluene-d8
106
75.0-131
(S) 4-Bromof/uorobenzene
96.3
67.0-138
(S) 1,2-Dich/oroethone-d4
106
70.0-130
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anth race ne
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis(2-chlorethoxy)methane
Bis(2-ch loroethyl)ether
2, 2-Oxybis(1-Ch I oropro pane)
4-Bromophenyl-phenylether
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
ACCOUNT:
Withers & Ravenel Eng. - Standard
Qualifier MDL (dry)
mg/kg
0.00700
0.00609
0.00771
0.0813
0.00763
0.00807
0.00769
0.00791
0.00804
0.0130
0.0143
0.0187
0.0152
PROJECT:
23-0302
RDL (dry)
mg/kg
0.0433
0.0433
0.0433
2.17
0.0433
0.0433
0.0433
0.0433
0.0433
0.433
0.433
0.433
0.433
Dilution Analysis
date / time
Batch
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
1 05/19/2023 22:49
WG2063443
051191202322.49
WG2063443
051191202322.49
WG2063443
051191202322.49
WG2063443
Dilution Analysis
date / time
Batch
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
1 05/20/2023 00:35
WG2063159
SDG:
DATE/TIME:
L1616119
06/06/23 12:28
FP1
FTc
FSS
4
Cn
Rc
I ql
FAI
FSC
PAGE:
32 of 132

TW-8(5-7.5) SAMPLE RESULTS - 08
Collected date/time: 05/12/23 10:20 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
2-Chloronaphthalene
4-ChIorophenyl-phenylether
Chrysene
Dibenz(a,h)anth racene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
HexachIoro-1,3-butadiene
HexachIorocyclopentadiene
Hexachloroethane
Ind eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a mine
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-methyl phen of
2-Chorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
54.7
53.0
52.5
53.1
66.7
65.7
Qualifier MDL (dry)
RDL (dry)
mg/kg
mg/kg
0.00760
0.0433
0.0151
0.433
0.00860
0.0433
0.0120
0.0433
0.0128
0.433
0.0131
0.433
0.0129
0.433
0.0160
0.433
0.0124
0.433
0.0142
0.433
0.00781
0.0433
0.00704
0.0433
0.0153
0.433
0.0146
0.433
0.0227
0.433
0.0170
0.433
0.0122
0.0433
0.0133
0.433
0.0109
0.0433
0.0151
0.433
0.0642
0.433
0.0327
0.433
0.0144
0.433
0.00859
0.0433
0.0135
0.433
0.0548
0.433
0.0148
0.433
0.0143
0.433
0.0917
0.433
0.0292
0.433
0.00842
0.0433
0.0135
0.433
0.0140
0.433
0.0143
0.433
0.0126
0.433
0.0113
0.433
0.0981
0.433
0.101
0.433
0.0155
0.433
0.0135
0.433
0.0116
0.433
0.0174
0.433
0.0139
0.433
12.0-120
10.0-120
10.0-122
15.0-120
10.0-127
10.0-120
Dilution Analysis Batch
date / time
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
05/20/2023 00:35
0512012023 0035
0512012023 0035
0512012023 0035
0512012023 0035
0512012023 0035
0512012023 0035
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
33 of 132

SAMPLE RESULTS - 09
L1616119
TW-9(5-7.5)
Collected date/time: 05/12/23 11:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 80.4 1 05/16/202315:46 WG2060827
Wet Chemistry by Method 7199
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Hexavalent Chromium 0.921
J 0.317
1.24
1 05/17/202319:25
WG2061030
Mercury by Method 7471B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Mercury U
0.0224
0.0498
1 06/05/202318:18
WG2061958
Metals (ICPMS) by Method 6020B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
_ mg/kg
mg/kg
mg/kg
date / time
Arsenic
116
0.124
1.24
5
05/17/2023 20:58
WG2061326
Barium
17.8
0.189
3.11
5
05/17/2023 20:58
WG2061326
Cadmium
U
0.106
1.24
5
05/17/2023 20:58
WG2061326
Chromium
27.8
0.368
6.22
5
05/17/2023 20:58
WG2061326
Lead
12.9
0.123
2.49
5
05/17/2023 20:58
WG2061326
Selenium
0.978
1_ 0.224
3.11
5
05/17/2023 20:58
WG2061326
Silver
U
0.108
0.622
5
05/17/2023 20:58
WG2061326
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acetone
U
0.0559
0.0766
1 05/19/2023 23:11
WG2063443
Acrylonitrile
U
0.00553
0.0191
1 05/19/2023 23:11
WG2063443
Benzene
U
0.000715
0.00153
1 05/19/2023 23:11
WG2063443
Bromobenzene
U
0.00138
0.0191
1 05/19/2023 23:11
WG2063443
Bromodichloromethane
U
0.00111
0.00383
1 05/19/2023 23:11
WG2063443
Bromoform
U
C3
0.00179
0.0383
1 05/19/2023 23:11
WG2063443
Bromomethane
U
0.00302
0.0191
1 05/19/2023 23:11
WG2063443
n-Butylbenzene
U
0.00804
0.0191
1 05/19/2023 23:11
WG2063443
sec -Butyl benzene
U
0.00441
0.0191
1 05/19/2023 23:11
WG2063443
ter[-Butylbenzene
U
0.00299
0.00766
1 05/19/2023 23:11
WG2063443
Carbon tetrachloride
U
0.00138
0.00766
1 05/19/2023 23:11
WG2063443
Chlorobenzene
U
0.000322
0.00383
1 05/19/2023 23:11
WG2063443
Chlorodibromomethane
U
0.000937
0.00383
1 05/19/2023 23:11
WG2063443
Chloroethane
U
0.00260
0.00766
1 05/19/2023 23:11
WG2063443
Chloroform
U
0.00158
0.00383
1 05/19/2023 23:11
WG2063443
Chloromethane
U
0.00666
0.0191
1 05/19/2023 23:11
WG2063443
2-Chlorotoluene
U
0.00132
0.00383
1 05/19/2023 23:11
WG2063443
4-Chlorotoluene
U
0.000689
0.00766
1 05/19/2023 23:11
WG2063443
1,2-Dibromo-3-Chloropropane
U
C3
0.00597
0.0383
1 05/19/2023 23:11
WG2063443
1,2-Dibromoethane
U
0.000992
0.00383
1 05/19/2023 23:11
WG2063443
Dibromomethane
U
0.00115
0.00766
1 05/19/2023 23:11
WG2063443
1,2-Dichlorobenzene
U
0.000651
0.00766
1 05/19/2023 23:11
WG2063443
1,3-Dichlorobenzene
U
0.000919
0.00766
1 05/19/2023 23:11
WG2063443
1,4-Dichlorobenzene
U
0.00107
0.00766
1 05/19/2023 23:11
WG2063443
Dichlorodifluoromethane
U
C3
0.00247
0.00383
1 05/19/2023 23:11
WG2063443
1,1-Dichloroethane
U
0.000752
0.00383
1 05/19/2023 23:11
WG2063443
1,2-Dichloroethane
U
0.000994
0.00383
1 05/19/2023 23:11
WG2063443
1,1-Dichloroethene
U
0.000928
0.00383
1 05/19/2023 23:11
WG2063443
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
FP1
FTc
FSS
4
Cn
rqc
F,
FAI
FSC
PAU=:
34 of 132

TW-9(5-7.5) SAMPLE RESULTS - 09
Collected date/time: 05/12/23 11:45 L1616119
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Analyte
mg/kg
mg/kg
mg/kg
cis-1,2-Dichloroethene
U
0.00112
0.00383
trans-1,2-Dichloroethene
U
0.00159
0.00766
1,2-Dichloropropane
U
0.00217
0.00766
1,1-Dichloropropene
U
0.00124
0.00383
1,3-Dichloropropane
U
0.000767
0.00766
cis-1,3-Dichloropropene
U
0.00116
0.00383
trans-1,3-Dichloropropene
U
0.00175
0.00766
2,2-Dichloropropane
U
0.00211
0.00383
Di -isopropyl ether
U
0.000628
0.00153
Ethylbenzene
U
0.00113
0.00383
Hexachloro-1,3-butadiene
U
0.00919
0.0383
Isopropylbenzene
U
0.000651
0.00383
p-Isopropyltoluene
U
0.00391
0.00766
2-Butanone (MEK)
U
0.0973
0.153
Methylene Chloride
U
0.0102
0.0383
4-Methyl-2-pentanone (MIBK)
U
0.00349
0.0383
Methyl tert-butyl ether
U
0.000536
0.00153
Naphthalene
U
0.00747
0.0191
n-Propylbenzene
U
0.00146
0.00766
Styrene
U
0.000351
0.0191
1,1,1,2-Tetrachloroethane
U
0.00145
0.00383
1,1,2,2-Tetrachloroethane
U
0.00106
0.00383
Tetrachloroethene
U
0.00137
0.00383
Toluene
U
0.00199
0.00766
1,2,3-Trichlorobenzene
U
0.0112
0.0191
1,2,4-Trichlorobenzene
U
0.00674
0.0191
1,1,1-Trichloroethane
U
0.00141
0.00383
1,1,2-Trichloroethane
U
0.000914
0.00383
1,1,2-Trichlorotrifluoroethane
U
0.00115
0.00383
Trichloroethene
U
0.000894
0.00153
Trichlorofluoromethane
U
0.00127
0.00383
1,2,3-Trichloropropane
U
0.00248
0.0191
1,2,4-Trimethylbenzene
U
0.00242
0.00766
1,3,5-Trimethyl benzene
U
0.00306
0.00766
Vinyl chloride
U
0.00178
0.00383
Xylenes, Total
U
0.00135
0.00996
(S) Toluene-d8
109
75.0-131
(S) 4-Bromof/uorobenzene
96.3
67.0-138
(S) 1,2-Dich/oroethone-d4
106
70.0-130
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anth race ne
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis(2-chlorethoxy)methane
Bis(2-ch loroethyl)ether
2, 2-Oxybis(1-Ch I oropro pane)
4-Bromophenyl-phenylether
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
ACCOUNT:
Withers & Ravenel Eng. - Standard
Qualifier MDL (dry)
mg/kg
0.00671
0.00584
0.00738
0.0779
0.00730
0.00773
0.00737
0.00758
0.00770
0.0124
0.0137
0.0179
0.0146
PROJECT:
23-0302
RDL (dry)
mg/kg
0.0414
0.0414
0.0414
2.08
0.0414
0.0414
0.0414
0.0414
0.0414
0.414
0.414
0.414
0.414
Dilution Analysis
date / time
Batch
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
1 05/19/2023 23:11
WG2063443
051191202323.11
WG2063443
051191202323.11
WG2063443
051191202323.11
WG2063443
Dilution Analysis
date / time
Batch
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
1 05/20/2023 00:57
WG2063159
SDG:
DATE/TIME:
L1616119
06/06/23 12:28
FP1
FTc
FSS
4
Cn
Rc
I ql
FAI
FSC
PAGE:
35 of 132

TW-9(5-7.5) SAMPLE RESULTS - 09
Collected date/time: 05/12/23 11:45 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
2-Chloronaphthalene
4-ChIcrop henyl-phenylether
Chrysene
Dibenz(a,h)anth racene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
HexachIoro-1,3-butadiene
HexachIorocyclopentadiene
Hexachloroethane
Ind eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a mine
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-methyl phen of
2-Chorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
51.8
48.2
474
49.8
55.3
53.5
Qualifier MDL (dry)
RDL (dry)
mg/kg
mg/kg
0.00728
0.0414
0.0144
0.414
0.00824
0.0414
0.0115
0.0414
0.0123
0.414
0.0126
0.414
0.0123
0.414
0.0153
0.414
0.0119
0.414
0.0136
0.414
0.00748
0.0414
0.00674
0.0414
0.0147
0.414
0.0139
0.414
0.0218
0.414
0.0163
0.414
0.0117
0.0414
0.0127
0.414
0.0104
0.0414
0.0144
0.414
0.0615
0.414
0.0314
0.414
0.0138
0.414
0.00822
0.0414
0.0129
0.414
0.0525
0.414
0.0142
0.414
0.0137
0.414
0.0878
0.414
0.0280
0.414
0.00806
0.0414
0.0129
0.414
0.0134
0.414
0.0137
0.414
0.0121
0.414
0.0108
0.414
0.0939
0.414
0.0969
0.414
0.0148
0.414
0.0129
0.414
0.0111
0.414
0.0167
0.414
0.0133
0.414
12.0-120
10.0-120
10.0-122
15.0-120
10.0-127
10.0-120
Dilution Analysis Batch
date / time
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
05/20/2023 00:57
0512012023 00:57
0512012023 00:57
0512012023 00:57
0512012023 00:57
0512012023 00:57
0512012023 00:57
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
36 of 132

SAMPLE RESULTS - 10
L1616119
TW-10(5-7.5)
Collected date/time: 05/12/23 14:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 77.3 1 05/16/202315:46 WG2060827
Wet Chemistry by Method 7199
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Hexavalent Chromium U
0.330
1.29
1 05/17/202319:30
WG2061030
Mercury by Method 7471B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Mercury 0.0830
0.0233
0.0517
1 06/05/202318:20
WG2061958
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry)
Analyte
Barium
11.6
0.197
Cadmium
U
0.111
Chromium
16.2
0.383
Lead
9.56
0.128
Selenium
0.843
J_ 0.233
Silver
U
0.112
Volatile Organic Compounds (GC/MS) by Method 8260D
RDL (dry)
Dilution
Analysis
Batch
mg/kg
date / time
1.29
5
05/17/2023 21:01
WG2061326
3.23
5
05/17/2023 21:01
WG2061326
1.29
5
05/17/2023 21:01
WG2061326
6.47
5
05/17/2023 21:01
WG2061326
2.59
5
05/17/2023 21:01
WG2061326
3.23
5
05/17/2023 21:01
WG2061326
0.647
5
05/17/2023 21:01
WG2061326
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acetone
U
0.0598
0.0820
1 05/19/2023 23:32
WG2063443
Acrylonitrile
U
0.00592
0.0205
1 05/19/2023 23:32
WG2063443
Benzene
U
0.000766
0.00164
1 05/19/2023 23:32
WG2063443
Bromobenzene
U
0.00148
0.0205
1 05/19/2023 23:32
WG2063443
Bromodichloromethane
U
0.00119
0.00410
1 05/19/2023 23:32
WG2063443
Bromoform
U
C3
0.00192
0.0410
1 05/19/2023 23:32
WG2063443
Bromomethane
U
0.00323
0.0205
1 05/19/2023 23:32
WG2063443
n-Butylbenzene
U
0.00861
0.0205
1 05/19/2023 23:32
WG2063443
sec -Butyl benzene
U
0.00472
0.0205
1 05/19/2023 23:32
WG2063443
ter[-Butylbenzene
U
0.00320
0.00820
1 05/19/2023 23:32
WG2063443
Carbon tetrachloride
U
0.00147
0.00820
1 05/19/2023 23:32
WG2063443
Chlorobenzene
U
0.000344
0.00410
1 05/19/2023 23:32
WG2063443
Chlorodibromomethane
U
0.00100
0.00410
1 05/19/2023 23:32
WG2063443
Chloroethane
U
0.00279
0.00820
1 05/19/2023 23:32
WG2063443
Chloroform
U
0.00169
0.00410
1 05/19/2023 23:32
WG2063443
Chloromethane
U
0.00713
0.0205
1 05/19/2023 23:32
WG2063443
2-Chlorotoluene
U
0.00142
0.00410
1 05/19/2023 23:32
WG2063443
4-Chlorotoluene
U
0.000738
0.00820
1 05/19/2023 23:32
WG2063443
1,2-Dibromo-3-Chloropropane
U
C3
0.00639
0.0410
1 05/19/2023 23:32
WG2063443
1,2-Dibromoethane
U
0.00106
0.00410
1 05/19/2023 23:32
WG2063443
Dibromomethane
U
0.00123
0.00820
1 05/19/2023 23:32
WG2063443
1,2-Dichlorobenzene
U
0.000697
0.00820
1 05/19/2023 23:32
WG2063443
1,3-Dichlorobenzene
U
0.000984
0.00820
1 05/19/2023 23:32
WG2063443
1,4-Dichlorobenzene
U
0.00115
0.00820
1 05/19/2023 23:32
WG2063443
Dichlorodifluoromethane
U
C3
0.00264
0.00410
1 05/19/2023 23:32
WG2063443
1,1-Dichloroethane
U
0.000805
0.00410
1 05/19/2023 23:32
WG2063443
1,2-Dichloroethane
U
0.00106
0.00410
1 05/19/2023 23:32
WG2063443
1,1-Dichloroethene
U
0.000994
0.00410
1 05/19/2023 23:32
WG2063443
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
FP1
FTC
FSS
4
Cn
rqc
F,
FAI
FSC
PAGE:
37 of 132

TW-10(5-7.5) SAMPLE RESULTS - 10
Collected date/time: 05/12/23 14:00 L1616119
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Analyte
mg/kg
mg/kg
mg/kg
cis-1,2-Dichloroethene
U
0.00120
0.00410
trans-1,2-Dichloroethene
U
0.00171
0.00820
1,2-Dichloropropane
U
0.00233
0.00820
1,1-Dichloropropene
U
0.00133
0.00410
1,3-Dichloropropane
U
0.000821
0.00820
cis-1,3-Dichloropropene
U
0.00124
0.00410
trans-1,3-Dichloropropene
U
0.00187
0.00820
2,2-Dichloropropane
U
0.00226
0.00410
Di -isopropyl ether
U
0.000672
0.00164
Ethylbenzene
U
0.00121
0.00410
Hexachloro-1,3-butadiene
U
0.00984
0.0410
Isopropylbenzene
U
0.000697
0.00410
p-Isopropyltoluene
U
0.00418
0.00820
2-Butanone (MEK)
U
0.104
0.164
Methylene Chloride
U
0.0109
0.0410
4-Methyl-2-pentanone (MIBK)
U
0.00374
0.0410
Methyl tert-butyl ether
U
0.000574
0.00164
Naphthalene
U
0.00800
0.0205
n-Propylbenzene
U
0.00156
0.00820
Styrene
U
0.000375
0.0205
1,1,1,2-Tetrachloroethane
U
0.00155
0.00410
1,1,2,2-Tetrachloroethane
U
0.00114
0.00410
Tetrachloroethene
U
0.00147
0.00410
Toluene
U
0.00213
0.00820
1,2,3-Trichlorobenzene
U
0.0120
0.0205
1,2,4-Trichlorobenzene
U
0.00721
0.0205
1,1,1-Trichloroethane
U
0.00151
0.00410
1,1,2-Trichloroethane
U
0.000979
0.00410
1,1,2-Trichlorotrifluoroethane
U
0.00124
0.00410
Trichloroethene
U
0.000958
0.00164
Trichlorofluoromethane
U
0.00136
0.00410
1,2,3-Trichloropropane
U
0.00266
0.0205
1,2,4-Trimethylbenzene
U
0.00259
0.00820
1,3,5-Trimethyl benzene
U
0.00328
0.00820
Vinyl chloride
U
0.00190
0.00410
Xylenes, Total
U
0.00144
0.0107
(S) Toluene-d8
106
75.0-131
(S) 4-Bromof/uorobenzene
96.4
67.0-138
(S) 1,2-Dich/oroethone-d4
108
70.0-130
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anth race ne
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis(2-chlorethoxy)methane
Bis(2-ch loroethyl)ether
2, 2-Oxybis(1-Ch I oropro pane)
4-Bromophenyl-phenylether
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
ACCOUNT:
Withers & Ravenel Eng. - Standard
Qualifier MDL (dry)
mg/kg
0.00697
0.00606
0.00767
0.0810
0.00759
0.00803
0.00766
0.00788
0.00800
0.0129
0.0142
0.0186
0.0151
PROJECT:
23-0302
RDL (dry)
mg/kg
0.0431
0.0431
0.0431
2.16
0.0431
0.0431
0.0431
0.0431
0.0431
0.431
0.431
0.431
0.431
Dilution Analysis
date / time
Batch
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
1 05/19/2023 23:32
WG2063443
051191202323:32
WG2063443
051191202323:32
WG2063443
051191202323:32
WG2063443
Dilution Analysis
date / time
Batch
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
1 05/20/2023 01:19
WG2063159
SDG:
DATE/TIME:
L1616119
06/06/23 12:28
FP1
FTc
FSS
4
Cn
Rc
I ql
FAI
FSC
PAGE:
38 of 132

TW-10(5-7.5) SAMPLE RESULTS - 10
Collected date/time: 05/12/23 14:00 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
2-Chloronaphthalene
4-ChIorophenyl-phenylether
Chrysene
Dibenz(a,h)anth racene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
HexachIoro-1,3-butadiene
HexachIorocyclopentadiene
Hexachloroethane
Ind eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a mine
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-methyl phen of
2-Chorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
55.0
53.3
52.4
53.3
65.0
62.7
Qualifier MDL (dry)
RDL (dry)
mg/kg
mg/kg
0.00756
0.0431
0.0150
0.431
0.00856
0.0431
0.0119
0.0431
0.0128
0.431
0.0131
0.431
0.0128
0.431
0.0159
0.431
0.0123
0.431
0.0141
0.431
0.00777
0.0431
0.00701
0.0431
0.0153
0.431
0.0145
0.431
0.0226
0.431
0.0169
0.431
0.0122
0.0431
0.0132
0.431
0.0108
0.0431
0.0150
0.431
0.0639
0.431
0.0326
0.431
0.0144
0.431
0.00855
0.0431
0.0134
0.431
0.0546
0.431
0.0147
0.431
0.0142
0.431
0.0913
0.431
0.0291
0.431
0.00838
0.0431
0.0134
0.431
0.0140
0.431
0.0142
0.431
0.0125
0.431
0.0113
0.431
0.0976
0.431
0.101
0.431
0.0154
0.431
0.0134
0.431
0.0116
0.431
0.0173
0.431
0.0138
0.431
12.0-120
10.0-120
10.0-122
15.0-120
10.0-127
10.0-120
Dilution Analysis Batch
date / time
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
05/20/2023 01:19
0512012023 01:19
0512012023 01:19
0512012023 01:19
0512012023 01:19
0512012023 01:19
0512012023 01:19
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
39 of 132

SAMPLE RESULTS - 11
L1616119
DUP
Collected date/time: 05/11/23 12:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 76.4 1 05/16/202315:46 WG2060827
Wet Chemistry by Method 7199
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Hexavalent Chromium 0.689
J 0.334
1.31
1 05/17/202311:56
WG2061041
Mercury by Method 7471B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
mg/kg
date / time
Mercury U
0.0236
0.0524
1 06/05/202318:28
WG2061958
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry)
Analyte
Barium
18.1
0.199
Cadmium
U
0.112
Chromium
52.6
0.387
Lead
11.6
0.130
Selenium
1.49
J_ 0.236
Silver
U
0.113
Volatile Organic Compounds (GC/MS) by Method 8260D
RDL (dry)
Dilution
Analysis
Batch
mg/kg
date / time
1.31
5
05/17/2023 21:12
WG2061326
3.27
5
05/17/2023 21:12
WG2061326
1.31
5
05/17/2023 21:12
WG2061326
6.54
5
05/17/2023 21:12
WG2061326
2.62
5
05/17/2023 21:12
WG2061326
3.27
5
05/17/2023 21:12
WG2061326
0.654
5
05/17/2023 21:12
WG2061326
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acetone
U
0.0602
0.0825
1 05/22/202310:25
WG2064295
Acrylonitrile
U
0.00596
0.0206
1 05/22/202310:25
WG2064295
Benzene
U
0.000771
0.00165
1 05/22/202310:25
WG2064295
Bromobenzene
U
0.00149
0.0206
1 05/22/202310:25
WG2064295
Bromodichloromethane
U
0.00120
0.00413
1 05/22/202310:25
WG2064295
Bromoform
U
0.00193
0.0413
1 05/22/202310:25
WG2064295
Bromomethane
U
0.00325
0.0206
1 05/22/202310:25
WG2064295
n-Butylbenzene
U
0.00867
0.0206
1 05/22/202310:25
WG2064295
sec -Butyl benzene
U
0.00475
0.0206
1 05/22/202310:25
WG2064295
tert-Butylbenzene
U
0.00322
0.00825
1 05/22/202310:25
WG2064295
Carbon tetrachloride
U
0.00148
0.00825
1 05/22/202310:25
WG2064295
Chlorobenzene
U
0.000347
0.00413
1 05/22/202310:25
WG2064295
Chlorodibromomethane
U
0.00101
0.00413
1 05/22/202310:25
WG2064295
Chloroethane
U
0.00281
0.00825
1 05/22/202310:25
WG2064295
Chloroform
U
0.00170
0.00413
1 05/22/202310:25
WG2064295
Chloromethane
U
0.00718
0.0206
1 05/22/202310:25
WG2064295
2-Chlorotoluene
U
0.00143
0.00413
1 05/22/202310:25
WG2064295
4-Chlorotoluene
U
C3 0.000743
0.00825
1 05/22/202310:25
WG2064295
1,2-Dibromo-3-Chloropropane
U
0.00644
0.0413
1 05/22/202310:25
WG2064295
1,2-Dibromoethane
U
0.00107
0.00413
1 05/22/202310:25
WG2064295
Dibromomethane
U
0.00124
0.00825
1 05/22/202310:25
WG2064295
1,2-Dichlorobenzene
U
0.000702
0.00825
1 05/22/202310:25
WG2064295
1,3-Dichlorobenzene
U
0.000990
0.00825
1 05/22/202310:25
WG2064295
1,4-Dichlorobenzene
U
0.00116
0.00825
1 05/22/202310:25
WG2064295
Dichlorodifluoromethane
U
0.00266
0.00413
1 05/22/202310:25
WG2064295
1,1-Dichloroethane
U
0.000810
0.00413
1 05/22/202310:25
WG2064295
1,2-Dichloroethane
U
0.00107
0.00413
1 05/22/202310:25
WG2064295
1,1-Dichloroethene
U
0.00100
0.00413
1 05/22/202310:25
WG2064295
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng.
- Standard
23-0302
L1616119
06/06/23 12:28
FP1
FTC
FSS
4
Cn
rqc
F,
FAI
FSC
PAGE:
40 of 132

DUP SAMPLE RESULTS - 11
Collected date/time: 05/11/23 12:00 L1616119
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
cis-1,2-Dichloroethene
U
0.00121
0.00413
1 05/22/202310:25
WG2064295
trans-1,2-Dichloroethene
U
0.00172
0.00825
1 05/22/202310:25
WG2064295
1,2-Dichloropropane
U
0.00234
0.00825
1 05/22/202310:25
WG2064295
1,1-Dichloropropene
U
0.00134
0.00413
1 05/22/202310:25
WG2064295
1,3-Dichloropropane
U
0.000827
0.00825
1 05/22/202310:25
WG2064295
cis-1,3-Dichloropropene
U
0.00125
0.00413
1 05/22/202310:25
WG2064295
trans-1,3-Dichloropropene
U
0.00188
0.00825
1 05/22/202310:25
WG2064295
2,2-Dichloropropane
U
0.00228
0.00413
1 05/22/202310:25
WG2064295
Di -isopropyl ether
U
0.000677
0.00165
1 05/22/202310:25
WG2064295
Ethylbenzene
U
0.00122
0.00413
1 05/22/202310:25
WG2064295
Hexachloro-1,3-butadiene
U
0.00990
0.0413
1 05/22/202310:25
WG2064295
Isopropylbenzene
U
0.000702
0.00413
1 05/22/202310:25
WG2064295
p-Isopropyltoluene
U
0.00421
0.00825
1 05/22/202310:25
WG2064295
2-Butanone (MEK)
U
0.105
0.165
1 05/22/202310:25
WG2064295
Methylene Chloride
U
0.0110
0.0413
1 05/22/202310:25
WG2064295
4-Methyl-2-pentanone (MIBK)
U
0.00376
0.0413
1 05/22/202310:25
WG2064295
Methyl tert-butyl ether
U
0.000578
0.00165
1 05/22/202310:25
WG2064295
Naphthalene
U
0.00806
0.0206
1 05/22/202310:25
WG2064295
n-Propylbenzene
U
0.00157
0.00825
1 05/22/202310:25
WG2064295
Styrene
U
C3 0.000378
0.0206
1 05/22/202310:25
WG2064295
1,1,1,2-Tetrachloroethane
U
0.00156
0.00413
1 05/22/202310:25
WG2064295
1,1,2,2-Tetrachloroethane
U
0.00115
0.00413
1 05/22/202310:25
WG2064295
Tetrachloroethene
U
0.00148
0.00413
1 05/22/202310:25
WG2064295
Toluene
U
0.00215
0.00825
1 05/22/202310:25
WG2064295
1,2,3-Trichlorobenzene
U
0.0121
0.0206
1 05/22/202310:25
WG2064295
1,2,4-Trichlorobenzene
U
0.00726
0.0206
1 05/22/202310:25
WG2064295
1,1,1-Trichloroethane
U
0.00152
0.00413
1 05/22/202310:25
WG2064295
1,1,2-Trichloroethane
U
0.000985
0.00413
1 05/22/202310:25
WG2064295
1,1,2-Trichlorotrifluoroethane
U
0.00124
0.00413
1 05/22/202310:25
WG2064295
Trichloroethene
U
0.000964
0.00165
1 05/22/202310:25
WG2064295
Trichlorofluoromethane
U
0.00137
0.00413
1 05/22/202310:25
WG2064295
1,2,3-Trichloropropane
U
0.00267
0.0206
1 05/22/202310:25
WG2064295
1,2,4-Trimethylbenzene
U
0.00261
0.00825
1 05/22/202310:25
WG2064295
1,3,5-Trimethyl benzene
U
0.00330
0.00825
1 05/22/202310:25
WG2064295
Vinyl chloride
U
0.00191
0.00413
1 05/22/202310:25
WG2064295
Xylenes, Total
U
0.00145
0.0107
1 05/22/202310:25
WG2064295
(S) Toluene-d8
105
75.0-131
051221202310:25
WG2064295
(S) 4-Bromof/uorobenzene
94.4
67.0-138
05722/202310:25
WG2064295
(S)1,2-Dich/oroethone-d4
92.6
70.0-130
051221202310:25
WG2064295
Semi Volatile Organic Compounds
(GC/MS) by Method
8270E
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Acenaphthene
U
0.00705
0.0436
1 05/20/2023 01:41
WG2063159
Acenaphthylene
U
0.00614
0.0436
1 05/20/2023 01:41
WG2063159
Anthracene
U
0.00776
0.0436
1 05/20/2023 01:41
WG2063159
Benzidine
U
0.0819
2.19
1 05/20/2023 01:41
WG2063159
Benzo(a)anth race ne
U
0.00768
0.0436
1 05/20/2023 01:41
WG2063159
Benzo(b)fluoranthene
U
0.00813
0.0436
1 05/20/2023 01:41
WG2063159
Benzo(k)fluoranthene
U
0.00775
0.0436
1 05/20/2023 01:41
WG2063159
Benzo(g,h,i)perylene
U
0.00797
0.0436
1 05/20/2023 01:41
WG2063159
Benzo(a)pyrene
U
0.00810
0.0436
1 05/20/2023 01:41
WG2063159
Bis(2-chlorethoxy)methane
U
0.0131
0.436
1 05/20/2023 01:41
WG2063159
Bis(2-chloroethyl)ether
U
0.0144
0.436
1 05/20/2023 01:41
WG2063159
2,2-Oxybis(1-Chloropropane)
U
0.0188
0.436
1 05/20/2023 01:41
WG2063159
4-Bromophenyl-phenylether
U
0.0153
0.436
1 05/20/2023 01:41
WG2063159
FP1
FTc
FSS
4
Cn
Rc
I ql
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 41 of 132

DUP SAMPLE RESULTS - 11
Collected date/time: 05/11/23 12:00 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
2-Chloronaphthalene
4-ChIorophenyl-phenylether
Chrysene
Dibenz(a,h)anth racene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
HexachIoro-1,3-butadiene
HexachIorocyclopentadiene
Hexachloroethane
Ind eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a mine
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-methyl phen of
2-Chorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
Result (dry)
mg/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
50.6
50.2
49.8
49.2
56.6
57.5
Qualifier MDL (dry)
RDL (dry)
mg/kg
mg/kg
0.00766
0.0436
0.0152
0.436
0.00866
0.0436
0.0121
0.0436
0.0129
0.436
0.0132
0.436
0.0130
0.436
0.0161
0.436
0.0125
0.436
0.0143
0.436
0.00787
0.0436
0.00709
0.0436
0.0154
0.436
0.0147
0.436
0.0229
0.436
0.0171
0.436
0.0123
0.0436
0.0133
0.436
0.0109
0.0436
0.0152
0.436
0.0647
0.436
0.0330
0.436
0.0145
0.436
0.00865
0.0436
0.0136
0.436
0.0552
0.436
0.0149
0.436
0.0144
0.436
0.0924
0.436
0.0294
0.436
0.00848
0.0436
0.0136
0.436
0.0141
0.436
0.0144
0.436
0.0127
0.436
0.0114
0.436
0.0988
0.436
0.102
0.436
0.0156
0.436
0.0136
0.436
0.0117
0.436
0.0175
0.436
0.0140
0.436
12.0-120
10.0-120
10.0-122
15.0-120
10.0-127
10.0-120
Dilution Analysis Batch
date / time
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
05/20/2023 01:41
0512012023 01.41
0512012023 01.41
0512012023 01.41
0512012023 01.41
0512012023 01.41
0512012023 01.41
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
WG2063159
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
42 of 132

TW-1
Collected date/time: 05/11/23 10:45
Wet Chemistry by Method 7199
SAMPLE
RESULTS - 12
L1616119
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Hexavalent Chromium -Low U
0.0400
0.100
1 05/18/2023 04:51
WG2059859
Level
Mercury by Method 7470A
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Mercury U
0.100
0.200
1 06/05/202319:50
WG2060584
Metals (ICPMS) by Method 6020B
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Arsenic
U
0.180
2.00
1 05/23/2023 22:03
WG2060154
Barium
43.9
0.381
2.00
1 05/23/2023 22:03
WG2060154
Cadmium
U
0.150
1.00
1 05/23/2023 22:03
WG2060154
Chromium
U
1.24
2.00
1 05/23/2023 22:03
WG2060154
Lead
1.61
J
0.849
2.00
1 05/23/2023 22:03
WG2060154
Selenium
1.20
J
0.300
2.00
1 05/23/2023 22:03
WG2060154
Silver
U
0.0700
2.00
1 05/23/2023 22:03
WG2060154
Volatile Organic Compounds (GC/MS)
by Method 620OB-1997/620OB-2011
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
11.3
50.0
1 05/22/2023 01:36
WG2064057
Acrolein
U
2.54
50.0
1 05/22/2023 01:36
WG2064057
Acrylonitrile
U
0.671
10.0
1 05/22/2023 01:36
WG2064057
Benzene
U
0.0941
1.00
1 05/22/2023 01:36
WG2064057
Bromobenzene
U
0.118
1.00
1 05/22/2023 01:36
WG2064057
Bromochloromethane
U
0.128
1.00
1 05/22/2023 01:36
WG2064057
Bromodichloromethane
U
0.136
1.00
1 05/22/2023 01:36
WG2064057
Bromoform
U
0.129
1.00
1 05/22/2023 01:36
WG2064057
Bromomethane
U
0.605
5.00
1 05/22/2023 01:36
WG2064057
n-Butylbenzene
U
0.157
1.00
1 05/22/2023 01:36
WG2064057
sec -Butyl benzene
U
0.125
1.00
1 05/22/2023 01:36
WG2064057
tert-Butylbenzene
U
0.127
1.00
1 05/22/2023 01:36
WG2064057
Carbon tetrachloride
U
0.128
1.00
1 05/22/2023 01:36
WG2064057
Chlorobenzene
U
0.116
1.00
1 05/22/2023 01:36
WG2064057
Chlorodibromomethane
U
0.140
1.00
1 05/22/2023 01:36
WG2064057
Chloroethane
U
0.192
5.00
1 05/22/2023 01:36
WG2064057
Chloroform
U
0.111
5.00
1 05/22/2023 01:36
WG2064057
Chloromethane
U
0.960
2.50
1 05/22/2023 01:36
WG2064057
2-Chlorotoluene
U
0.106
1.00
1 05/22/2023 01:36
WG2064057
4-Chlorotoluene
U
0.114
1.00
1 05/22/2023 01:36
WG2064057
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1 05/22/2023 01:36
WG2064057
1,2-Dibromoethane
U
0.126
1.00
1 05/22/2023 01:36
WG2064057
Dibromomethane
U
0.122
1.00
1 05/22/2023 01:36
WG2064057
1,2-Dichlorobenzene
U
0.107
1.00
1 05/22/2023 01:36
WG2064057
1,3-Dichlorobenzene
U
0.110
1.00
1 05/22/2023 01:36
WG2064057
1,4-Dichlorobenzene
U
0.120
1.00
1 05/22/2023 01:36
WG2064057
Dichlorodifluoromethane
U
0.374
5.00
1 05/22/2023 01:36
WG2064057
1,1-Dichloroethane
U
0.100
1.00
1 05/22/2023 01:36
WG2064057
1,2-Dichloroethane
U
0.0819
1.00
1 05/22/2023 01:36
WG2064057
1,1-Dichloroethene
U
0.188
1.00
1 05/22/2023 01:36
WG2064057
cis-1,2-Dichloroethene
U
0.126
1.00
1 05/22/2023 01:36
WG2064057
trans-1,2-Dichloroethene
U
0.149
1.00
1 05/22/2023 01:36
WG2064057
1,2-Dichloropropane
U
0.149
1.00
1 05/22/2023 01:36
WG2064057
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
Fp]
FTC
FSS
4
Cn
RC
F ql
FAI
FSC
43 of 132

TW-1 SAMPLE RESULTS - 12
Collected date/time: 05/11/23 10:45 L1616119
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
1,1-Dichloropropene
U
0.142
1.00
1 05/22/2023 01:36
WG2064057
1,3-Dichloropropane
U
0.110
1.00
1 05/22/2023 01:36
WG2064057
cis-1,3-Dichloropropene
U
0.111
1.00
1 05/22/2023 01:36
WG2064057
trans-1,3-Dichloropropene
U
0.118
1.00
1 05/22/2023 01:36
WG2064057
2,2-Dichloropropane
U
0.161
1.00
1 05/22/2023 01:36
WG2064057
Di -isopropyl ether
U
0.105
1.00
1 05/22/2023 01:36
WG2064057
Ethylbenzene
U
0.137
1.00
1 05/22/2023 01:36
WG2064057
Hexachloro-1,3-butadiene
U
0.337
1.00
1 05/22/2023 01:36
WG2064057
2-Hexanone
U
0.787
10.0
1 05/22/2023 01:36
WG2064057
Isopropylbenzene
U
0.105
1.00
1 05/22/2023 01:36
WG2064057
p-Isopropyltoluene
U
0.120
1.00
1 05/22/2023 01:36
WG2064057
2-Butanone (MEK)
U
1.19
10.0
1 05/22/2023 01:36
WG2064057
Methylene Chloride
U
0.430
5.00
1 05/22/2023 01:36
WG2064057
4-Methyl-2-pentanone (MIBK)
U
0.478
10.0
1 05/22/2023 01:36
WG2064057
Methyl tert-butyl ether
U
0.101
1.00
1 05/22/2023 01:36
WG2064057
Naphthalene
U
1.00
5.00
1 05/22/2023 01:36
WG2064057
n-Propylbenzene
U
0.0993
1.00
1 05/22/2023 01:36
WG2064057
Styrene
U
0.118
1.00
1 05/22/2023 01:36
WG2064057
1,1,1,2-Tetrachloroethane
U
0.147
1.00
1 05/22/2023 01:36
WG2064057
1,1,2,2-Tetrachloroethane
U
0.133
1.00
1 05/22/2023 01:36
WG2064057
Tetrachloroethene
U
0.300
1.00
1 05/22/2023 01:36
WG2064057
Toluene
U
0.278
1.00
1 05/22/2023 01:36
WG2064057
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/22/2023 01:36
WG2064057
1,2,4-Trichlorobenzene
U
0.481
1.00
1 05/22/2023 01:36
WG2064057
1,1,1-Trichloroethane
U
0.149
1.00
1 05/22/2023 01:36
WG2064057
1,1,2-Trichloroethane
U
0.158
1.00
1 05/22/2023 01:36
WG2064057
Trichloroethene
U
0.190
1.00
1 05/22/2023 01:36
WG2064057
Trichlorofluoromethane
U
0.160
5.00
1 05/22/2023 01:36
WG2064057
1,2,3-Trichloropropane
U
0.237
2.50
1 05/22/2023 01:36
WG2064057
1,2,4-Trimethylbenzene
U
0.322
1.00
1 05/22/2023 01:36
WG2064057
1,3,5-Trimethyl benzene
U
0.104
1.00
1 05/22/2023 01:36
WG2064057
Vinyl acetate
U
0.692
10.0
1 05/22/2023 01:36
WG2064057
Vinyl chloride
U
0.234
1.00
1 05/22/2023 01:36
WG2064057
o-Xylene
U
J4 0.174
1.00
1 05/22/2023 01:36
WG2064057
m&p-Xylenes
U
0.430
2.00
1 05/22/2023 01:36
WG2064057
(S) Toluene-d8
105
80.0-120
0512212023 0136
WG2064057
(S) 4-Bromof/uorobenzene
96.1
77.0-126
0512212023 01:36
WG2064057
(S) 1,2-Dich/oroethone-d4
90.1
70.0-130
0512212023 0136
WG2064057
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/I ug/I ug/I date / time
Acenaphthene
U
0.0930
1.05
1.05
05/17/2023 02:08
WG2059503
Acenaphthylene
U
0.0967
1.05
1.05
05/17/2023 02:08
WG2059503
Anthracene
U
0.0844
1.05
1.05
05/17/2023 02:08
WG2059503
Benzidine
U
3.93
10.5
1.05
05/17/2023 02:08
WG2059503
Benzo(a)anth race ne
U
0.209
1.05
1.05
05/17/2023 02:08
WG2059503
Benzo(b)fluoranthene
U
0.136
1.05
1.05
05/17/2023 02:08
WG2059503
Benzo(k)fluoranthene
U
0.126
1.05
1.05
05/17/2023 02:08
WG2059503
Benzo(g,h,i)perylene
U
0.127
1.05
1.05
05/17/2023 02:08
WG2059503
Benzo(a)pyrene
U
0.0400
1.05
1.05
05/17/2023 02:08
WG2059503
Bis(2-chlorethoxy)methane
U
0.122
10.5
1.05
05/17/2023 02:08
WG2059503
Bis(2-chloroethyl)ether
U
0.144
10.5
1.05
05/17/2023 02:08
WG2059503
2,2-Oxybis(1-Chloropropane)
U
0.221
10.5
1.05
05/17/2023 02:08
WG2059503
4-Bromophenyl-phenylether
U
0.0921
10.5
1.05
05/17/2023 02:08
WG2059503
2-Chloronaphthalene
U
0.0680
1.05
1.05
05/17/2023 02:08
WG2059503
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 44 of 132

TW-1 SAMPLE RESULTS - 12
Collected date/time: 05/11/23 10:45 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Analyte
Result
ug/I
Qualifier MDL
ug/I
RDL
ug/I
Dilution
Analysis
date / time
Batch
4-Chlorophenyl-phenylether
U
0.0972
10.5
1.05
05/17/2023 02:08
WG2059503
Chrysene
U
0.136
1.05
1.05
05/17/2023 02:08
WG2059503
Dibenz(a,h)anthracene
U
0.0676
1.05
1.05
05/17/2023 02:08
WG2059503
3,3-Dichlorobenzidine
U
0.223
10.5
1.05
05/17/2023 02:08
WG2059503
2,4-Dinitrotoluene
U
0.103
10.5
1.05
05/17/2023 02:08
WG2059503
2,6-Dinitrotoluene
U
0.263
10.5
1.05
05/17/2023 02:08
WG2059503
Fluoranthene
U
0.107
1.05
1.05
05/17/2023 02:08
WG2059503
Fluorene
U
0.0886
1.05
1.05
05/17/2023 02:08
WG2059503
Hexachlorobenzene
U
0.0793
1.05
1.05
05/17/2023 02:08
WG2059503
Hexachloro-1,3-butadiene
U
0.102
10.5
1.05
05/17/2023 02:08
WG2059503
Hexachlorocyclopentadiene
U
0.0628
10.5
1.05
05/17/2023 02:08
WG2059503
Hexachloroethane
U
0.133
10.5
1.05
05/17/2023 02:08
WG2059503
Indeno(1,2,3-cd)pyrene
U
0.293
1.05
1.05
05/17/2023 02:08
WG2059503
Isophorone
U
0.150
10.5
1.05
05/17/2023 02:08
WG2059503
Naphthalene
11.3
0.167
1.05
1.05
05/17/2023 02:08
WG2059503
Nitrobenzene
U
0.312
10.5
1.05
05/17/2023 02:08
WG2059503
n-Nitrosodimethyla mine
U
1.05
10.5
1.05
05/17/2023 02:08
WG2059503
n-Nitrosodiphenyla mine
U
2.49
10.5
1.05
05/17/2023 02:08
WG2059503
n-Nitrosodi-n-propylamine
U
0.274
10.5
1.05
05/17/2023 02:08
WG2059503
Phenanthrene
U
0.118
1.05
1.05
05/17/2023 02:08
WG2059503
Benzylbutyl phthalate
U
0.803
3.15
1.05
05/17/2023 02:08
WG2059503
Bis(2-ethylhexyl)phthalate
U
0.940
3.15
1.05
05/17/2023 02:08
WG2059503
Di-n-butyl phthalate
U
0.476
3.15
1.05
05/17/2023 02:08
WG2059503
Diethyl phthalate
1.28
J_ 0.301
3.15
1.05
05/17/2023 02:08
WG2059503
Dimethyl phthalate
U
0.273
3.15
1.05
05/17/2023 02:08
WG2059503
Di-n-octyl phthalate
U
0.979
3.15
1.05
05/17/2023 02:08
WG2059503
Pyrene
U
0.112
1.05
1.05
05/17/2023 02:08
WG2059503
1,2,4-Trichlorobenzene
U
0.0733
10.5
1.05
05/17/2023 02:08
WG2059503
4-Chloro-3-methylphenol
U
0.138
10.5
1.05
05/17/2023 02:08
WG2059503
2-Chlorophenol
U
0.140
10.5
1.05
05/17/2023 02:08
WG2059503
2,4-Dichlorophenol
U
0.107
10.5
1.05
05/17/2023 02:08
WG2059503
2,4-Dimethylphenol
U
0.0668
10.5
1.05
05/17/2023 02:08
WG2059503
4,6-Dinitro-2-methylphenol
U
1.18
10.5
1.05
05/17/2023 02:08
WG2059503
2,4-Dinitrophenol
U
6.23
10.5
1.05
05/17/2023 02:08
WG2059503
2-Nitrophenol
U
0.123
10.5
1.05
05/17/2023 02:08
WG2059503
4-Nitrophenol
U
0.150
10.5
1.05
05/17/2023 02:08
WG2059503
Pentachlorophenol
U
0.329
10.5
1.05
05/17/2023 02:08
WG2059503
Phenol
U
4.55
10.5
1.05
05/17/2023 02:08
WG2059503
2,4,6-Trichlorophenol
U
0.105
10.5
1.05
05/17/2023 02:08
WG2059503
(S) Nitrobenzene-d5
49.1
15.0-314
0511712023 02:08
WG2059503
(S) 2-Fluorobiphenyl
44.7
22.0-127
0511712023 02:08
WG2059503
(S) p-Terphenyl-d14
66.4
29.0-141
0511712023 02:08
WG2059503
(S) Phenol-d5
13.8
8.00-424
0511712023 02:08
WG2059503
(S) 2-F/uorophenol
26.1
10.0-120
0511712023 02:08
WG2059503
(S) 2,4,6- Tribromophenol
52.4
10.0-153
0511712023 02:08
WG2059503
FP1
FTc
FSS
4
Cn
RC
I ql
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 45 of 132

TW-2
Collected date/time: 05/11/23 13:05
Wet Chemistry by Method 7199
SAMPLE
RESULTS - 13
L1616119
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Hexavalent Chromium -Low U
0.0400
0.100
1 05/18/2023 05:15
WG2059859
Level
Mercury by Method 7470A
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Mercury U
0.100
0.200
1 06/05/202319:53
WG2060584
Metals (ICPMS) by Method 6020B
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Arsenic
0.212
J
0.180
2.00
1 05/23/2023 22:06
WG2060154
Barium
42.7
0.381
2.00
1 05/23/2023 22:06
WG2060154
Cadmium
U
0.150
1.00
1 05/23/2023 22:06
WG2060154
Chromium
U
1.24
2.00
1 05/23/2023 22:06
WG2060154
Lead
1.25
J
0.849
2.00
1 05/23/2023 22:06
WG2060154
Selenium
0.871
J
0.300
2.00
1 05/23/2023 22:06
WG2060154
Silver
U
0.0700
2.00
1 05/23/2023 22:06
WG2060154
Volatile Organic Compounds (GC/MS)
by Method 620OB-1997/620OB-2011
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
11.3
50.0
1 05/22/2023 01:55
WG2064057
Acrolein
U
2.54
50.0
1 05/22/2023 01:55
WG2064057
Acrylonitrile
U
0.671
10.0
1 05/22/2023 01:55
WG2064057
Benzene
239
0.941
10.0
10 05/23/2023 04:14
WG2064510
Bromobenzene
U
0.118
1.00
1 05/22/2023 01:55
WG2064057
Bromochloromethane
U
0.128
1.00
1 05/22/2023 01:55
WG2064057
Bromodichloromethane
U
0.136
1.00
1 05/22/2023 01:55
WG2064057
Bromoform
U
0.129
1.00
1 05/22/2023 01:55
WG2064057
Bromomethane
U
0.605
5.00
1 05/22/2023 01:55
WG2064057
n-Butylbenzene
16.4
0.157
1.00
1 05/22/2023 01:55
WG2064057
sec -Butyl benzene
3.06
0.125
1.00
1 05/22/2023 01:55
WG2064057
tert-Butylbenzene
U
0.127
1.00
1 05/22/2023 01:55
WG2064057
Carbon tetrachloride
U
0.128
1.00
1 05/22/2023 01:55
WG2064057
Chlorobenzene
U
0.116
1.00
1 05/22/2023 01:55
WG2064057
Chlorodibromomethane
U
0.140
1.00
1 05/22/2023 01:55
WG2064057
Chloroethane
U
0.192
5.00
1 05/22/2023 01:55
WG2064057
Chloroform
2.15
1_
0.111
5.00
1 05/22/2023 01:55
WG2064057
Chloromethane
U
0.960
2.50
1 05/22/2023 01:55
WG2064057
2-Chlorotoluene
U
0.106
1.00
1 05/22/2023 01:55
WG2064057
4-Chlorotoluene
U
0.114
1.00
1 05/22/2023 01:55
WG2064057
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1 05/22/2023 01:55
WG2064057
1,2-Dibromoethane
U
0.126
1.00
1 05/22/2023 01:55
WG2064057
Dibromomethane
U
0.122
1.00
1 05/22/2023 01:55
WG2064057
1,2-Dichlorobenzene
U
0.107
1.00
1 05/22/2023 01:55
WG2064057
1,3-Dichlorobenzene
U
0.110
1.00
1 05/22/2023 01:55
WG2064057
1,4-Dichlorobenzene
U
0.120
1.00
1 05/22/2023 01:55
WG2064057
Dichlorodifluoromethane
U
0.374
5.00
1 05/22/2023 01:55
WG2064057
1,1-Dichloroethane
U
0.100
1.00
1 05/22/2023 01:55
WG2064057
1,2-Dichloroethane
10.5
0.0819
1.00
1 05/22/2023 01:55
WG2064057
1,1-Dichloroethene
U
0.188
1.00
1 05/22/2023 01:55
WG2064057
cis-1,2-Dichloroethene
U
0.126
1.00
1 05/22/2023 01:55
WG2064057
trans-1,2-Dichloroethene
U
0.149
1.00
1 05/22/2023 01:55
WG2064057
1,2-Dichloropropane
U
0.149
1.00
1 05/22/2023 01:55
WG2064057
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
Fp]
FTC
FSS
4
Cn
RC
F ql
FAI
FSC
PAGE:
46 of 132

TW-2 SAMPLE RESULTS - 13
Collected date/time: 05/11/23 13:05 L1616119
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result Qualifier
MDL
RDL
Dilution
Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
1,1-Dichloropropene
U
0.142
1.00
1
05/22/2023 01:55
WG2064057
1,3-Dichloropropane
U
0.110
1.00
1
05/22/2023 01:55
WG2064057
cis-1,3-Dichloropropene
U
0.111
1.00
1
05/22/2023 01:55
WG2064057
trans-1,3-Dichloropropene
U
0.118
1.00
1
05/22/2023 01:55
WG2064057
2,2-Dichloropropane
U
0.161
1.00
1
05/22/2023 01:55
WG2064057
Di -isopropyl ether
U
0.105
1.00
1
05/22/2023 01:55
WG2064057
Ethylbenzene
171
1.37
10.0
10
05/23/2023 04:14
WG2064510
Hexachloro-1,3-butadiene
U
0.337
1.00
1
05/22/2023 01:55
WG2064057
2-Hexanone
32.2
0.787
10.0
1
05/22/2023 01:55
WG2064057
Isopropylbenzene
12.1
0.105
1.00
1
05/22/2023 01:55
WG2064057
p-Isopropyltoluene
7.64
0.120
1.00
1
05/22/2023 01:55
WG2064057
2-Butanone (MEK)
13.5
1.19
10.0
1
05/22/2023 01:55
WG2064057
Methylene Chloride
U
0.430
5.00
1
05/22/2023 01:55
WG2064057
4-Methyl-2-pentanone (MIBK)
9.25 J
0.478
10.0
1
05/22/2023 01:55
WG2064057
Methyl tert-butyl ether
2.00
0.101
1.00
1
05/22/2023 01:55
WG2064057
Naphthalene
19.2
1.00
5.00
1
05/22/2023 01:55
WG2064057
n-Propylbenzene
42.5
0.0993
1.00
1
05/22/2023 01:55
WG2064057
Styrene
U
0.118
1.00
1
05/22/2023 01:55
WG2064057
1,1,1,2-Tetrachloroethane
U
0.147
1.00
1
05/22/2023 01:55
WG2064057
1,1,2,2-Tetrachloroethane
U
0.133
1.00
1
05/22/2023 01:55
WG2064057
Tetrachloroethene
U
0.300
1.00
1
05/22/2023 01:55
WG2064057
Toluene
407
2.78
10.0
10
05/23/2023 04:14
WG2064510
1,2,3-Trichlorobenzene
U
0.230
1.00
1
05/22/2023 01:55
WG2064057
1,2,4-Trichlorobenzene
U
0.481
1.00
1
05/22/2023 01:55
WG2064057
1,1,1-Trichloroethane
U
0.149
1.00
1
05/22/2023 01:55
WG2064057
1,1,2-Trichloroethane
U
0.158
1.00
1
05/22/2023 01:55
WG2064057
Trichloroethene
U
0.190
1.00
1
05/22/2023 01:55
WG2064057
Trichlorofluoromethane
U
0.160
5.00
1
05/22/2023 01:55
WG2064057
1,2,3-Trichloropropane
U
0.237
2.50
1
05/22/2023 01:55
WG2064057
1,2,4-Trimethylbenzene
295
3.22
10.0
10
05/23/2023 04:14
WG2064510
1,3,5-Trimethyl benzene
121
1.04
10.0
10
05/23/2023 04:14
WG2064510
Vinyl acetate
U
0.692
10.0
1
05/22/2023 01:55
WG2064057
Vinyl chloride
U
0.234
1.00
1
05/22/2023 01:55
WG2064057
o-Xylene
200
1.74
10.0
10
05/23/2023 04:14
WG2064510
m&p-Xylenes
676
4.30
20.0
10
05/23/2023 04:14
WG2064510
(S) Toluene-d8
103
80.0-120
0512212023 01:55
WG2064057
(S) Toluene-d8
98.8
80.0-120
0512312023 04:14
WG2064510
(S) 4-Bromof/uorobenzene
99.7
77.0-126
0512212023 01:55
WG2064057
(S) 4-Bromofluorobenzene
99.4
77.0-126
0512312023 04:14
WG2064510
(S)1,2-Dich/oroethone-d4
93.5
70.0-130
0512212023 01:55
WG2064057
(S)1,2-Dlch/oroethone-d4
110
70.0-130
0512312023 04:14
WG2064510
Semi Volatile Organic
Compounds (GC/MS)
by
Method 625.1
Result Qualifier
MDL
RDL
Dilution
Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acenaphthene
U
0.0930
1.05
1.05
05/17/2023 02:29
WG2059503
Acenaphthylene
U
0.0967
1.05
1.05
05/17/2023 02:29
WG2059503
Anthracene
U
0.0844
1.05
1.05
05/17/2023 02:29
WG2059503
Benzidine
U
3.93
10.5
1.05
05/17/2023 02:29
WG2059503
Benzo(a)anth race ne
U
0.209
1.05
1.05
05/17/2023 02:29
WG2059503
Benzo(b)fluoranthene
U
0.136
1.05
1.05
05/17/2023 02:29
WG2059503
Benzo(k)fluoranthene
U
0.126
1.05
1.05
05/17/2023 02:29
WG2059503
Benzo(g,h,i)perylene
U
0.127
1.05
1.05
05/17/2023 02:29
WG2059503
Benzo(a)pyrene
U
0.0400
1.05
1.05
05/17/2023 02:29
WG2059503
Bis(2-chlorethoxy)methane
U
0.122
10.5
1.05
05/17/2023 02:29
WG2059503
Bis(2-chloroethyl)ether
U
0.144
10.5
1.05
05/17/2023 02:29
WG2059503
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 47 of 132

TW-2 SAMPLE RESULTS - 13
Collected date/time: 05/11/23 13:05 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier MDL
RDL
Dilution
Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
2,2-Oxybis(1-Chloropropane)
U
0.221
10.5
1.05
05/17/2023 02:29
WG2059503
4-Bromophenyl-phenylether
U
0.0921
10.5
1.05
05/17/2023 02:29
WG2059503
2-Chloronaphthalene
U
0.0680
1.05
1.05
05/17/2023 02:29
WG2059503
4-Chlorophenyl-phenylether
U
0.0972
10.5
1.05
05/17/2023 02:29
WG2059503
Chrysene
U
0.136
1.05
1.05
05/17/2023 02:29
WG2059503
Dibenz(a,h)anthracene
U
0.0676
1.05
1.05
05/17/2023 02:29
WG2059503
3,3-Dichlorobenzidine
U
0.223
10.5
1.05
05/17/2023 02:29
WG2059503
2,4-Dinitrotoluene
U
0.103
10.5
1.05
05/17/2023 02:29
WG2059503
2,6-Dinitrotoluene
U
0.263
10.5
1.05
05/17/2023 02:29
WG2059503
Fluoranthene
U
0.107
1.05
1.05
05/17/2023 02:29
WG2059503
Fluorene
U
0.0886
1.05
1.05
05/17/2023 02:29
WG2059503
Hexachlorobenzene
U
0.0793
1.05
1.05
05/17/2023 02:29
WG2059503
Hexachloro-1,3-butadiene
U
0.102
10.5
1.05
05/17/2023 02:29
WG2059503
Hexachlorocyclopentadiene
U
0.0628
10.5
1.05
05/17/2023 02:29
WG2059503
Hexachloroethane
U
0.133
10.5
1.05
05/17/2023 02:29
WG2059503
Indeno(1,2,3-cd)pyrene
U
0.293
1.05
1.05
05/17/2023 02:29
WG2059503
Isophorone
U
0.150
10.5
1.05
05/17/2023 02:29
WG2059503
Naphthalene
U
0.167
1.05
1.05
05/17/2023 02:29
WG2059503
Nitrobenzene
U
0.312
10.5
1.05
05/17/2023 02:29
WG2059503
n-Nitrosodimethyla mine
U
1.05
10.5
1.05
05/17/2023 02:29
WG2059503
n-Nitrosodiphenyla mine
U
2.49
10.5
1.05
05/17/2023 02:29
WG2059503
n-Nitrosodi-n-propylamine
U
0.274
10.5
1.05
05/17/2023 02:29
WG2059503
Phenanthrene
U
0.118
1.05
1.05
05/17/2023 02:29
WG2059503
Benzylbutyl phthalate
U
0.803
3.15
1.05
05/17/2023 02:29
WG2059503
Bis(2-ethylhexyl)phthalate
U
0.940
3.15
1.05
05/17/2023 02:29
WG2059503
Di-n-butyl phthalate
U
0.476
3.15
1.05
05/17/2023 02:29
WG2059503
Diethyl phthalate
5.13
0.301
3.15
1.05
05/17/2023 02:29
WG2059503
Dimethyl phthalate
U
0.273
3.15
1.05
05/17/2023 02:29
WG2059503
Di-n-octyl phthalate
U
0.979
3.15
1.05
05/17/2023 02:29
WG2059503
Pyrene
U
0.112
1.05
1.05
05/17/2023 02:29
WG2059503
1,2,4-Trichlorobenzene
U
0.0733
10.5
1.05
05/17/2023 02:29
WG2059503
4-ChIoro-3-methyl phenol
U
0.138
10.5
1.05
05/17/2023 02:29
WG2059503
2-Chlorophenol
U
0.140
10.5
1.05
05/17/2023 02:29
WG2059503
2,4-Dichlorophenol
U
0.107
10.5
1.05
05/17/2023 02:29
WG2059503
2,4-Dimethylphenol
U
0.0668
10.5
1.05
05/17/2023 02:29
WG2059503
4,6-Dinitro-2-methylphenol
U
1.18
10.5
1.05
05/17/2023 02:29
WG2059503
2,4-Dinitrophenol
U
6.23
10.5
1.05
05/17/2023 02:29
WG2059503
2-Nitrophenol
U
0.123
10.5
1.05
05/17/2023 02:29
WG2059503
4-Nitrophenol
U
0.150
10.5
1.05
05/17/2023 02:29
WG2059503
Pentachlorophenol
U
0.329
10.5
1.05
05/17/2023 02:29
WG2059503
Phenol
U
4.55
10.5
1.05
05/17/2023 02:29
WG2059503
2,4,6-Trichlorophenol
U
0.105
10.5
1.05
05/17/2023 02:29
WG2059503
(S) Nitrobenzene-d5
62.8
15.0-314
0511712023 02:29
WG2059503
(S) 2-Fluorobiphenyl
58.3
22.0-127
0511712023 02:29
WG2059503
(S) p-Terphenyl-d14
72.5
29.0-141
0511712023 02:29
WG2059503
(S) Phenol-d5
18.3
8.00-424
0511712023 02:29
WG2059503
(S) 2-F/uorophenol
27.7
10.0-120
0511712023 02:29
WG2059503
(S)2,4,6-Tribromopheno/
59.5
10.0-153
051171202302:29
WG2059503
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 48 of 132

TW-3
Collected date/time: 05/11/23 16:00
Wet Chemistry by Method 7199
SAMPLE
RESULTS - 14
L1616119
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Hexavalent Chromium -Low U
0.0400
0.100
1 05/18/2023 05:30
WG2059859
Level
Mercury by Method 7470A
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Mercury U
0.100
0.200
1 06/05/202319:55
WG2060584
Metals (ICPMS) by Method 6020B
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Arsenic
U
0.180
2.00
1 05/23/2023 22:10
WG2060154
Barium
21.8
0.381
2.00
1 05/23/2023 22:10
WG2060154
Cadmium
U
0.150
1.00
1 05/23/2023 22:10
WG2060154
Chromium
U
1.24
2.00
1 05/23/2023 22:10
WG2060154
Lead
U
0.849
2.00
1 05/23/2023 22:10
WG2060154
Selenium
0.397 J
0.300
2.00
1 05/23/2023 22:10
WG2060154
Silver
U
0.0700
2.00
1 05/23/2023 22:10
WG2060154
Volatile Organic Compounds (GC/MS)
by Method 620OB-1997/620OB-2011
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
11.3
50.0
1 05/22/2023 02:14
WG2064057
Acrolein
U
2.54
50.0
1 05/22/2023 02:14
WG2064057
Acrylonitrile
U
0.671
10.0
1 05/22/2023 02:14
WG2064057
Benzene
U
0.0941
1.00
1 05/22/2023 02:14
WG2064057
Bromobenzene
U
0.118
1.00
1 05/22/2023 02:14
WG2064057
Bromochloromethane
U
0.128
1.00
1 05/22/2023 02:14
WG2064057
Bromodichloromethane
U
0.136
1.00
1 05/22/2023 02:14
WG2064057
Bromoform
U
0.129
1.00
1 05/22/2023 02:14
WG2064057
Bromomethane
U
0.605
5.00
1 05/22/2023 02:14
WG2064057
n-Butylbenzene
U
0.157
1.00
1 05/22/2023 02:14
WG2064057
sec -Butyl benzene
U
0.125
1.00
1 05/22/2023 02:14
WG2064057
tert-Butylbenzene
U
0.127
1.00
1 05/22/2023 02:14
WG2064057
Carbon tetrachloride
U
0.128
1.00
1 05/22/2023 02:14
WG2064057
Chlorobenzene
U
0.116
1.00
1 05/22/2023 02:14
WG2064057
Chlorodibromomethane
U
0.140
1.00
1 05/22/2023 02:14
WG2064057
Chloroethane
U
0.192
5.00
1 05/22/2023 02:14
WG2064057
Chloroform
U
0.111
5.00
1 05/22/2023 02:14
WG2064057
Chloromethane
U
0.960
2.50
1 05/22/2023 02:14
WG2064057
2-Chlorotoluene
U
0.106
1.00
1 05/22/2023 02:14
WG2064057
4-Chlorotoluene
U
0.114
1.00
1 05/22/2023 02:14
WG2064057
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1 05/22/2023 02:14
WG2064057
1,2-Dibromoethane
U
0.126
1.00
1 05/22/2023 02:14
WG2064057
Dibromomethane
U
0.122
1.00
1 05/22/2023 02:14
WG2064057
1,2-Dichlorobenzene
U
0.107
1.00
1 05/22/2023 02:14
WG2064057
1,3-Dichlorobenzene
U
0.110
1.00
1 05/22/2023 02:14
WG2064057
1,4-Dichlorobenzene
U
0.120
1.00
1 05/22/2023 02:14
WG2064057
Dichlorodifluoromethane
U
0.374
5.00
1 05/22/2023 02:14
WG2064057
1,1-Dichloroethane
U
0.100
1.00
1 05/22/2023 02:14
WG2064057
1,2-Dichloroethane
U
0.0819
1.00
1 05/22/2023 02:14
WG2064057
1,1-Dichloroethene
U
0.188
1.00
1 05/22/2023 02:14
WG2064057
cis-1,2-Dichloroethene
U
0.126
1.00
1 05/22/2023 02:14
WG2064057
trans-1,2-Dichloroethene
U
0.149
1.00
1 05/22/2023 02:14
WG2064057
1,2-Dichloropropane
U
0.149
1.00
1 05/22/2023 02:14
WG2064057
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
Fp]
FTC
FSS
4
Cn
RC
F ql
FAI
FSC
PAGE:
49 of 132

TW-3 SAMPLE RESULTS - 14
Collected date/time: 05/11/23 16:00 L1616119
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result
Qualifier
MDL
RDL Dilution
Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
1,1-Dichloropropene
U
0.142
1.00 1
05/22/2023 02:14
WG2064057
1,3-Dichloropropane
U
0.110
1.00 1
05/22/2023 02:14
WG2064057
cis-1,3-Dichloropropene
U
0.111
1.00 1
05/22/2023 02:14
WG2064057
trans-1,3-Dichloropropene
U
0.118
1.00 1
05/22/2023 02:14
WG2064057
2,2-Dichloropropane
U
0.161
1.00 1
05/22/2023 02:14
WG2064057
Di -isopropyl ether
U
0.105
1.00 1
05/22/2023 02:14
WG2064057
Ethylbenzene
U
0.137
1.00 1
05/23/2023 03:09
WG2064510
Hexachloro-1,3-butadiene
U
0.337
1.00 1
05/22/2023 02:14
WG2064057
2-Hexanone
U
0.787
10.0 1
05/22/2023 02:14
WG2064057
Isopropylbenzene
U
0.105
1.00 1
05/22/2023 02:14
WG2064057
p-Isopropyltoluene
U
0.120
1.00 1
05/22/2023 02:14
WG2064057
2-Butanone (MEK)
U
1.19
10.0 1
05/22/2023 02:14
WG2064057
Methylene Chloride
U
0.430
5.00 1
05/22/2023 02:14
WG2064057
4-Methyl-2-pentanone (MIBK)
U
0.478
10.0 1
05/22/2023 02:14
WG2064057
Methyl tert-butyl ether
U
0.101
1.00 1
05/22/2023 02:14
WG2064057
Naphthalene
1.22
J
1.00
5.00 1
05/22/2023 02:14
WG2064057
n-Propylbenzene
0.218
J_
0.0993
1.00 1
05/22/2023 02:14
WG2064057
Styrene
U
0.118
1.00 1
05/22/2023 02:14
WG2064057
1,1,1,2-Tetrachloroethane
U
0.147
1.00 1
05/22/2023 02:14
WG2064057
1,1,2,2-Tetrachloroethane
U
0.133
1.00 1
05/22/2023 02:14
WG2064057
Tetrachloroethene
U
0.300
1.00 1
05/22/2023 02:14
WG2064057
Toluene
U
0.278
1.00 1
05/23/2023 03:09
WG2064510
1,2,3-Trichlorobenzene
U
0.230
1.00 1
05/22/2023 02:14
WG2064057
1,2,4-Trichlorobenzene
U
0.481
1.00 1
05/22/2023 02:14
WG2064057
1,1,1-Trichloroethane
U
0.149
1.00 1
05/22/2023 02:14
WG2064057
1,1,2-Trichloroethane
U
0.158
1.00 1
05/22/2023 02:14
WG2064057
Trichloroethene
U
0.190
1.00 1
05/22/2023 02:14
WG2064057
Trichlorofluoromethane
U
0.160
5.00 1
05/22/2023 02:14
WG2064057
1,2,3-Trichloropropane
U
0.237
2.50 1
05/22/2023 02:14
WG2064057
1,2,4-Trimethylbenzene
U
0.322
1.00 1
05/23/2023 03:09
WG2064510
1,3,5-Trimethyl benzene
U
0.104
1.00 1
05/23/2023 03:09
WG2064510
Vinyl acetate
U
0.692
10.0 1
05/22/2023 02:14
WG2064057
Vinyl chloride
U
0.234
1.00 1
05/22/2023 02:14
WG2064057
o-Xylene
U
0.174
1.00 1
05/23/2023 03:09
WG2064510
m&p-Xylenes
U
0.430
2.00 1
05/23/2023 03:09
WG2064510
(S) Toluene-d8
104
80.0-120
0512212023 02.14
WG2064057
(S) Toluene-d8
101
80.0-120
0512312023 03:09
WG2064510
(S) 4-Bromof/uorobenzene
97.8
77.0-126
0512212023 02.14
WG2064057
(S) 4-Bromofluorobenzene
96.6
77.0-126
0512312023 03:09
WG2064510
(S)1,2-Dich/oroethane-d4
90.8
70.0-130
0512212023 02.14
WG2064057
(S)1,2-Dlch/oroethone-d4
114
70.0-130
0512312023 03:09
WG2064510
Semi Volatile Organic
Compounds (GC/MS)
by
Method 625.1
Result
Qualifier
MDL
RDL Dilution
Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acenaphthene
U
0.0886
1.00 1
05/17/2023 02:50
WG2059503
Acenaphthylene
U
0.0921
1.00 1
05/17/2023 02:50
WG2059503
Anthracene
U
0.0804
1.00 1
05/17/2023 02:50
WG2059503
Benzidine
U
3.74
10.0 1
05/17/2023 02:50
WG2059503
Benzo(a)anth race ne
U
0.199
1.00 1
05/17/2023 02:50
WG2059503
Benzo(b)fluoranthene
U
0.130
1.00 1
05/17/2023 02:50
WG2059503
Benzo(k)fluoranthene
U
0.120
1.00 1
05/17/2023 02:50
WG2059503
Benzo(g,h,i)perylene
U
0.121
1.00 1
05/17/2023 02:50
WG2059503
Benzo(a)pyrene
U
0.0381
1.00 1
05/17/2023 02:50
WG2059503
Bis(2-chlorethoxy)methane
U
0.116
10.0 1
05/17/2023 02:50
WG2059503
Bis(2-chloroethyl)ether
U
0.137
10.0 1
05/17/2023 02:50
WG2059503
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 50 of 132

TW-3 SAMPLE RESULTS - 14
Collected date/time: 05/11/23 16:00 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
2,2-Oxybis(1-Chloropropane)
U
0.210
10.0
1 05/17/2023 02:50
WG2059503
4-Bromophenyl-phenylether
U
0.0877
10.0
1 05/17/2023 02:50
WG2059503
2-Chloronaphthalene
U
0.0648
1.00
1 05/17/2023 02:50
WG2059503
4-Chlorophenyl-phenylether
U
0.0926
10.0
1 05/17/2023 02:50
WG2059503
Chrysene
U
0.130
1.00
1 05/17/2023 02:50
WG2059503
Dibenz(a,h)anthracene
U
0.0644
1.00
1 05/17/2023 02:50
WG2059503
3,3-Dichlorobenzidine
U
0.212
10.0
1 05/17/2023 02:50
WG2059503
2,4-Dinitrotoluene
U
0.0983
10.0
1 05/17/2023 02:50
WG2059503
2,6-Dinitrotoluene
U
0.250
10.0
1 05/17/2023 02:50
WG2059503
Fluoranthene
0.121
J
0.102
1.00
1 05/17/2023 02:50
WG2059503
Fluorene
U
0.0844
1.00
1 05/17/2023 02:50
WG2059503
Hexachlorobenzene
U
0.0755
1.00
1 05/17/2023 02:50
WG2059503
Hexachloro-1,3-butadiene
U
0.0968
10.0
1 05/17/2023 02:50
WG2059503
Hexachlorocyclopentadiene
U
0.0598
10.0
1 05/17/2023 02:50
WG2059503
Hexachloroethane
U
0.127
10.0
1 05/17/2023 02:50
WG2059503
Indeno(1,2,3-cd)pyrene
U
0.279
1.00
1 05/17/2023 02:50
WG2059503
Isophorone
U
0.143
10.0
1 05/17/2023 02:50
WG2059503
Naphthalene
U
0.159
1.00
1 05/17/2023 02:50
WG2059503
Nitrobenzene
U
0.297
10.0
1 05/17/2023 02:50
WG2059503
n-Nitrosodimethyla mine
U
0.998
10.0
1 05/17/2023 02:50
WG2059503
n-Nitrosodiphenyla mine
U
2.37
10.0
1 05/17/2023 02:50
WG2059503
n-Nitrosodi-n-propylamine
U
0.261
10.0
1 05/17/2023 02:50
WG2059503
Phenanthrene
0.251
1_
0.112
1.00
1 05/17/2023 02:50
WG2059503
Benzylbutyl phthalate
U
0.765
3.00
1 05/17/2023 02:50
WG2059503
Bis(2-ethylhexyl)phthalate
U
0.895
3.00
1 05/17/2023 02:50
WG2059503
Di-n-butyl phthalate
U
0.453
3.00
1 05/17/2023 02:50
WG2059503
Diethyl phthalate
1.00
J_
0.287
3.00
1 05/17/2023 02:50
WG2059503
Dimethyl phthalate
U
0.260
3.00
1 05/17/2023 02:50
WG2059503
Di-n-octyl phthalate
U
0.932
3.00
1 05/17/2023 02:50
WG2059503
Pyrene
U
0.107
1.00
1 05/17/2023 02:50
WG2059503
1,2,4-Trichlorobenzene
U
0.0698
10.0
1 05/17/2023 02:50
WG2059503
4-ChIoro-3-methyl phenol
U
0.131
10.0
1 05/17/2023 02:50
WG2059503
2-Chlorophenol
U
0.133
10.0
1 05/17/2023 02:50
WG2059503
2,4-Dichlorophenol
U
0.102
10.0
1 05/17/2023 02:50
WG2059503
2,4-Dimethylphenol
U
0.0636
10.0
1 05/17/2023 02:50
WG2059503
4,6-Dinitro-2-methylphenol
U
1.12
10.0
1 05/17/2023 02:50
WG2059503
2,4-Dinitrophenol
U
5.93
10.0
1 05/17/2023 02:50
WG2059503
2-Nitrophenol
U
0.117
10.0
1 05/17/2023 02:50
WG2059503
4-Nitrophenol
U
0.143
10.0
1 05/17/2023 02:50
WG2059503
Pentachlorophenol
U
0.313
10.0
1 05/17/2023 02:50
WG2059503
Phenol
U
4.33
10.0
1 05/17/2023 02:50
WG2059503
2,4,6-Trichlorophenol
U
0.100
10.0
1 05/17/2023 02:50
WG2059503
(S) Nitrobenzene-d5
59.8
15.0-314
0511712023 02:50
WG2059503
(S) 2-Fluorobiphenyl
58.0
22.0-127
0511712023 02:50
WG2059503
(S) p-Terphenyl-d14
50.0
29.0-141
0511712023 02:50
WG2059503
(S) Phenol-d5
15.0
8.00-424
0511712023 02:50
WG2059503
(S) 2-F/uorophenol
19.6
10.0-120
0511712023 02:50
WG2059503
(S)2,4,6-Tribromopheno/
42.4
10.0-153
051171202302:50
WG2059503
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 51 of 132

-------------
TW-4
SAMPLE
RESULTS - 15
Collected date/time: 05/11/23 15:00
L1616119
Wet Chemistry by Method 7199
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Hexavalent Chromium -Low 0.215
0.0400
0.100
1 05/18/2023 05:38
WG2059859
Level
Mercury by Method 7470A
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Mercury 0.156 J
0.100
0.200
1 06/05/202319:57
WG2060584
Metals (ICPMS) by Method 6020B
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Arsenic
0.779
J
0.180
2.00
1 05/23/2023 22:13
WG2060154
Barium
62.6
0.381
2.00
1 05/23/2023 22:13
WG2060154
Cadmium
U
0.150
1.00
1 05/23/2023 22:13
WG2060154
Chromium
U
1.24
2.00
1 05/23/2023 22:13
WG2060154
Lead
1.65
J
0.849
2.00
1 05/23/2023 22:13
WG2060154
Selenium
2.12
0.300
2.00
1 05/23/2023 22:13
WG2060154
Silver
U
0.0700
2.00
1 05/23/2023 22:13
WG2060154
Volatile Organic Compounds (GC/MS)
by Method 620OB-1997/620OB-2011
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
11.3
50.0
1 05/22/2023 02:33
WG2064057
Acrolein
U
2.54
50.0
1 05/22/2023 02:33
WG2064057
Acrylonitrile
U
0.671
10.0
1 05/22/2023 02:33
WG2064057
Benzene
U
0.0941
1.00
1 05/22/2023 02:33
WG2064057
Bromobenzene
U
0.118
1.00
1 05/22/2023 02:33
WG2064057
Bromochloromethane
U
0.128
1.00
1 05/22/2023 02:33
WG2064057
Bromodichloromethane
U
0.136
1.00
1 05/22/2023 02:33
WG2064057
Bromoform
U
0.129
1.00
1 05/22/2023 02:33
WG2064057
Bromomethane
U
0.605
5.00
1 05/22/2023 02:33
WG2064057
n-Butylbenzene
U
0.157
1.00
1 05/22/2023 02:33
WG2064057
sec -Butyl benzene
U
0.125
1.00
1 05/22/2023 02:33
WG2064057
tert-Butylbenzene
U
0.127
1.00
1 05/22/2023 02:33
WG2064057
Carbon tetrachloride
U
0.128
1.00
1 05/22/2023 02:33
WG2064057
Chlorobenzene
U
0.116
1.00
1 05/22/2023 02:33
WG2064057
Chlorodibromomethane
U
0.140
1.00
1 05/22/2023 02:33
WG2064057
Chloroethane
U
0.192
5.00
1 05/22/2023 02:33
WG2064057
Chloroform
U
0.111
5.00
1 05/22/2023 02:33
WG2064057
Chloromethane
U
0.960
2.50
1 05/22/2023 02:33
WG2064057
2-Chlorotoluene
U
0.106
1.00
1 05/22/2023 02:33
WG2064057
4-Chlorotoluene
U
0.114
1.00
1 05/22/2023 02:33
WG2064057
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1 05/22/2023 02:33
WG2064057
1,2-Dibromoethane
U
0.126
1.00
1 05/22/2023 02:33
WG2064057
Dibromomethane
U
0.122
1.00
1 05/22/2023 02:33
WG2064057
1,2-Dichlorobenzene
U
0.107
1.00
1 05/22/2023 02:33
WG2064057
1,3-Dichlorobenzene
U
0.110
1.00
1 05/22/2023 02:33
WG2064057
1,4-Dichlorobenzene
U
0.120
1.00
1 05/22/2023 02:33
WG2064057
Dichlorodifluoromethane
U
0.374
5.00
1 05/22/2023 02:33
WG2064057
1,1-Dichloroethane
U
0.100
1.00
1 05/22/2023 02:33
WG2064057
1,2-Dichloroethane
U
0.0819
1.00
1 05/22/2023 02:33
WG2064057
1,1-Dichloroethene
U
0.188
1.00
1 05/22/2023 02:33
WG2064057
cis-1,2-Dichloroethene
U
0.126
1.00
1 05/22/2023 02:33
WG2064057
trans-1,2-Dichloroethene
U
0.149
1.00
1 05/22/2023 02:33
WG2064057
1,2-Dichloropropane
U
0.149
1.00
1 05/22/2023 02:33
WG2064057
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
Fp]
FTC
FSS
4
Cn
RC
F ql
FAI
FSC
PAGE:
52 of 132

TW-4 SAMPLE RESULTS - 15
Collected date/time: 05/11/23 15:00 L1616119
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
1,1-Dichloropropene
U
0.142
1.00
1 05/22/2023 02:33
WG2064057
1,3-Dichloropropane
U
0.110
1.00
1 05/22/2023 02:33
WG2064057
cis-1,3-Dichloropropene
U
0.111
1.00
1 05/22/2023 02:33
WG2064057
trans-1,3-Dichloropropene
U
0.118
1.00
1 05/22/2023 02:33
WG2064057
2,2-Dichloropropane
U
0.161
1.00
1 05/22/2023 02:33
WG2064057
Di -isopropyl ether
U
0.105
1.00
1 05/22/2023 02:33
WG2064057
Ethylbenzene
U
0.137
1.00
1 05/22/2023 02:33
WG2064057
Hexachloro-1,3-butadiene
U
0.337
1.00
1 05/22/2023 02:33
WG2064057
2-Hexanone
U
0.787
10.0
1 05/22/2023 02:33
WG2064057
Isopropylbenzene
U
0.105
1.00
1 05/22/2023 02:33
WG2064057
p-Isopropyltoluene
U
0.120
1.00
1 05/22/2023 02:33
WG2064057
2-Butanone (MEK)
U
1.19
10.0
1 05/22/2023 02:33
WG2064057
Methylene Chloride
U
0.430
5.00
1 05/22/2023 02:33
WG2064057
4-Methyl-2-pentanone (MIBK)
U
0.478
10.0
1 05/22/2023 02:33
WG2064057
Methyl tert-butyl ether
U
0.101
1.00
1 05/22/2023 02:33
WG2064057
Naphthalene
U
1.00
5.00
1 05/22/2023 02:33
WG2064057
n-Propylbenzene
U
0.0993
1.00
1 05/22/2023 02:33
WG2064057
Styrene
U
0.118
1.00
1 05/22/2023 02:33
WG2064057
1,1,1,2-Tetrachloroethane
U
0.147
1.00
1 05/22/2023 02:33
WG2064057
1,1,2,2-Tetrachloroethane
U
0.133
1.00
1 05/22/2023 02:33
WG2064057
Tetrachloroethene
U
0.300
1.00
1 05/22/2023 02:33
WG2064057
Toluene
U
0.278
1.00
1 05/22/2023 02:33
WG2064057
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/22/2023 02:33
WG2064057
1,2,4-Trichlorobenzene
U
0.481
1.00
1 05/22/2023 02:33
WG2064057
1,1,1-Trichloroethane
U
0.149
1.00
1 05/22/2023 02:33
WG2064057
1,1,2-Trichloroethane
U
0.158
1.00
1 05/22/2023 02:33
WG2064057
Trichloroethene
U
0.190
1.00
1 05/22/2023 02:33
WG2064057
Trichlorofluoromethane
U
0.160
5.00
1 05/22/2023 02:33
WG2064057
1,2,3-Trichloropropane
U
0.237
2.50
1 05/22/2023 02:33
WG2064057
1,2,4-Trimethylbenzene
U
0.322
1.00
1 05/22/2023 02:33
WG2064057
1,3,5-Trimethyl benzene
U
0.104
1.00
1 05/22/2023 02:33
WG2064057
Vinyl acetate
U
0.692
10.0
1 05/22/2023 02:33
WG2064057
Vinyl chloride
U
0.234
1.00
1 05/22/2023 02:33
WG2064057
o-Xylene
U
J4 0.174
1.00
1 05/22/2023 02:33
WG2064057
m&p-Xylenes
U
0.430
2.00
1 05/22/2023 02:33
WG2064057
(S) Toluene-d8
104
80.0-120
0512212023 0233
WG2064057
(S) 4-Bromof/uorobenzene
94.3
77.0-126
0512212023 02:33
WG2064057
(S) 1,2-Dich/oroethone-d4
92.4
70.0-130
0512212023 0233
WG2064057
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/I ug/I ug/I date / time
Acenaphthene
U
0.0886
1.00
1 05/17/2023 03:12
WG2059503
Acenaphthylene
U
0.0921
1.00
1 05/17/2023 03:12
WG2059503
Anthracene
U
0.0804
1.00
1 05/17/2023 03:12
WG2059503
Benzidine
U
3.74
10.0
1 05/17/2023 03:12
WG2059503
Benzo(a)anth race ne
U
0.199
1.00
1 05/17/2023 03:12
WG2059503
Benzo(b)fluoranthene
U
0.130
1.00
1 05/17/2023 03:12
WG2059503
Benzo(k)fluoranthene
U
0.120
1.00
1 05/17/2023 03:12
WG2059503
Benzo(g,h,i)perylene
U
0.121
1.00
1 05/17/2023 03:12
WG2059503
Benzo(a)pyrene
U
0.0381
1.00
1 05/17/2023 03:12
WG2059503
Bis(2-chlorethoxy)methane
U
0.116
10.0
1 05/17/2023 03:12
WG2059503
Bis(2-chloroethyl)ether
U
0.137
10.0
1 05/17/2023 03:12
WG2059503
2,2-Oxybis(1-Chloropropane)
U
0.210
10.0
1 05/17/2023 03:12
WG2059503
4-Bromophenyl-phenylether
U
0.0877
10.0
1 05/17/2023 03:12
WG2059503
2-Chloronaphthalene
U
0.0648
1.00
1 05/17/2023 03:12
WG2059503
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 53 of 132

TW-4 SAMPLE RESULTS - 15
Collected date/time: 05/11/23 15:00 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
4-Chlorophenyl-phenylether
U
0.0926
10.0
1 05/17/2023 03:12
WG2059503
Chrysene
U
0.130
1.00
1 05/17/2023 03:12
WG2059503
Dibenz(a,h)anthracene
U
0.0644
1.00
1 05/17/2023 03:12
WG2059503
3,3-Dichlorobenzidine
U
0.212
10.0
1 05/17/2023 03:12
WG2059503
2,4-Dinitrotoluene
U
0.0983
10.0
1 05/17/2023 03:12
WG2059503
2,6-Dinitrotoluene
U
0.250
10.0
1 05/17/2023 03:12
WG2059503
Fluoranthene
U
0.102
1.00
1 05/17/2023 03:12
WG2059503
Fluorene
U
0.0844
1.00
1 05/17/2023 03:12
WG2059503
Hexachlorobenzene
U
0.0755
1.00
1 05/17/2023 03:12
WG2059503
Hexachloro-1,3-butadiene
U
0.0968
10.0
1 05/17/2023 03:12
WG2059503
Hexachlorocyclopentadiene
U
0.0598
10.0
1 05/17/2023 03:12
WG2059503
Hexachloroethane
U
0.127
10.0
1 05/17/2023 03:12
WG2059503
Indeno(1,2,3-cd)pyrene
U
0.279
1.00
1 05/17/2023 03:12
WG2059503
Isophorone
U
0.143
10.0
1 05/17/2023 03:12
WG2059503
Naphthalene
U
0.159
1.00
1 05/17/2023 03:12
WG2059503
Nitrobenzene
U
0.297
10.0
1 05/17/2023 03:12
WG2059503
n-Nitrosodimethyla mine
U
0.998
10.0
1 05/17/2023 03:12
WG2059503
n-Nitrosodiphenyla mine
U
2.37
10.0
1 05/17/2023 03:12
WG2059503
n-Nitrosodi-n-propylamine
U
0.261
10.0
1 05/17/2023 03:12
WG2059503
Phenanthrene
U
0.112
1.00
1 05/17/2023 03:12
WG2059503
Benzylbutyl phthalate
U
0.765
3.00
1 05/17/2023 03:12
WG2059503
Bis(2-ethylhexyl)phthalate
U
0.895
3.00
1 05/17/2023 03:12
WG2059503
Di-n-butyl phthalate
0.658
B J 0.453
3.00
1 05/17/2023 03:12
WG2059503
Diethyl phthalate
1.29
J_ 0.287
3.00
1 05/17/2023 03:12
WG2059503
Dimethyl phthalate
U
0.260
3.00
1 05/17/2023 03:12
WG2059503
Di-n-octyl phthalate
U
0.932
3.00
1 05/17/2023 03:12
WG2059503
Pyrene
U
0.107
1.00
1 05/17/2023 03:12
WG2059503
1,2,4-Trichlorobenzene
U
0.0698
10.0
1 05/17/2023 03:12
WG2059503
4-Chloro-3-methylphenol
U
0.131
10.0
1 05/17/2023 03:12
WG2059503
2-Chlorophenol
U
0.133
10.0
1 05/17/2023 03:12
WG2059503
2,4-Dichlorophenol
U
0.102
10.0
1 05/17/2023 03:12
WG2059503
2,4-Dimethylphenol
U
0.0636
10.0
1 05/17/2023 03:12
WG2059503
4,6-Dinitro-2-methylphenol
U
1.12
10.0
1 05/17/2023 03:12
WG2059503
2,4-Dinitrophenol
U
5.93
10.0
1 05/17/2023 03:12
WG2059503
2-Nitrophenol
U
0.117
10.0
1 05/17/2023 03:12
WG2059503
4-Nitrophenol
U
0.143
10.0
1 05/17/2023 03:12
WG2059503
Pentachlorophenol
U
0.313
10.0
1 05/17/2023 03:12
WG2059503
Phenol
U
4.33
10.0
1 05/17/2023 03:12
WG2059503
2,4,6-Trichlorophenol
U
0.100
10.0
1 05/17/2023 03:12
WG2059503
(S) Nitrobenzene-d5
59.8
15.0-314
0511712023 0312
WG2059503
(S) 2-Fluorobiphenyl
62.5
22.0-127
0511712023 0312
WG2059503
(S) p-Terphenyl-d14
69.8
29.0-141
0511712023 0312
WG2059503
(S) Phenol-d5
18.5
8.00-424
0511712023 0312
WG2059503
(S) 2-F/uorophenol
29.1
10.0-120
0511712023 0312
WG2059503
(S) 2,4,6- Tribromophenol
57.5
10.0-153
05117120230312
WG2059503
FP1
FTc
FSS
4
Cn
RC
F
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 54 of 132

TW-5
Collected date/time: 05/11/23 16:45
Wet Chemistry by Method 7199
SAMPLE
RESULTS - 16
L1616119
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Hexavalent Chromium -Low U
0.0400
0.100
1 05/18/2023 06:01
WG2059859
Level
Mercury by Method 7470A
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Mercury U
0.100
0.200
1 06/05/2023 20:00
WG2060584
Metals (ICPMS) by Method 6020B
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Arsenic
U
0.180
2.00
1 05/23/2023 22:33
WG2060154
Barium
45.6
0.381
2.00
1 05/23/2023 22:33
WG2060154
Cadmium
U
0.150
1.00
1 05/23/2023 22:33
WG2060154
Chromium
U
1.24
2.00
1 05/23/2023 22:33
WG2060154
Lead
0.998 J
0.849
2.00
1 05/23/2023 22:33
WG2060154
Selenium
4.31
0.300
2.00
1 05/23/2023 22:33
WG2060154
Silver
U
0.0700
2.00
1 05/23/2023 22:33
WG2060154
Volatile Organic Compounds (GC/MS)
by Method 620OB-1997/620OB-2011
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
11.3
50.0
1 05/22/2023 02:52
WG2064057
Acrolein
U
2.54
50.0
1 05/22/2023 02:52
WG2064057
Acrylonitrile
U
0.671
10.0
1 05/22/2023 02:52
WG2064057
Benzene
U
0.0941
1.00
1 05/22/2023 02:52
WG2064057
Bromobenzene
U
0.118
1.00
1 05/22/2023 02:52
WG2064057
Bromochloromethane
U
0.128
1.00
1 05/22/2023 02:52
WG2064057
Bromodichloromethane
U
0.136
1.00
1 05/22/2023 02:52
WG2064057
Bromoform
U
0.129
1.00
1 05/22/2023 02:52
WG2064057
Bromomethane
U
0.605
5.00
1 05/22/2023 02:52
WG2064057
n-Butylbenzene
U
0.157
1.00
1 05/22/2023 02:52
WG2064057
sec -Butyl benzene
U
0.125
1.00
1 05/22/2023 02:52
WG2064057
tert-Butylbenzene
U
0.127
1.00
1 05/22/2023 02:52
WG2064057
Carbon tetrachloride
U
0.128
1.00
1 05/22/2023 02:52
WG2064057
Chlorobenzene
U
0.116
1.00
1 05/22/2023 02:52
WG2064057
Chlorodibromomethane
U
0.140
1.00
1 05/22/2023 02:52
WG2064057
Chloroethane
U
0.192
5.00
1 05/22/2023 02:52
WG2064057
Chloroform
U
0.111
5.00
1 05/22/2023 02:52
WG2064057
Chloromethane
U
0.960
2.50
1 05/22/2023 02:52
WG2064057
2-Chlorotoluene
U
0.106
1.00
1 05/22/2023 02:52
WG2064057
4-Chlorotoluene
U
0.114
1.00
1 05/22/2023 02:52
WG2064057
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1 05/22/2023 02:52
WG2064057
1,2-Dibromoethane
U
0.126
1.00
1 05/22/2023 02:52
WG2064057
Dibromomethane
U
0.122
1.00
1 05/22/2023 02:52
WG2064057
1,2-Dichlorobenzene
U
0.107
1.00
1 05/22/2023 02:52
WG2064057
1,3-Dichlorobenzene
U
0.110
1.00
1 05/22/2023 02:52
WG2064057
1,4-Dichlorobenzene
U
0.120
1.00
1 05/22/2023 02:52
WG2064057
Dichlorodifluoromethane
U
0.374
5.00
1 05/22/2023 02:52
WG2064057
1,1-Dichloroethane
U
0.100
1.00
1 05/22/2023 02:52
WG2064057
1,2-Dichloroethane
U
0.0819
1.00
1 05/22/2023 02:52
WG2064057
1,1-Dichloroethene
U
0.188
1.00
1 05/22/2023 02:52
WG2064057
cis-1,2-Dichloroethene
U
0.126
1.00
1 05/22/2023 02:52
WG2064057
trans-1,2-Dichloroethene
U
0.149
1.00
1 05/22/2023 02:52
WG2064057
1,2-Dichloropropane
U
0.149
1.00
1 05/22/2023 02:52
WG2064057
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
Fp]
FTC
FSS
4
Cn
RC
F ql
FAI
FSC
PAGE:
55 of 132

TW-5 SAMPLE RESULTS - 16
Collected date/time: 05/11/23 16:45 L1616119
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
1,1-Dichloropropene
U
0.142
1.00
1 05/22/2023 02:52
WG2064057
1,3-Dichloropropane
U
0.110
1.00
1 05/22/2023 02:52
WG2064057
cis-1,3-Dichloropropene
U
0.111
1.00
1 05/22/2023 02:52
WG2064057
trans-1,3-Dichloropropene
U
0.118
1.00
1 05/22/2023 02:52
WG2064057
2,2-Dichloropropane
U
0.161
1.00
1 05/22/2023 02:52
WG2064057
Di -isopropyl ether
U
0.105
1.00
1 05/22/2023 02:52
WG2064057
Ethylbenzene
U
0.137
1.00
1 05/22/2023 02:52
WG2064057
Hexachloro-1,3-butadiene
U
0.337
1.00
1 05/22/2023 02:52
WG2064057
2-Hexanone
U
0.787
10.0
1 05/22/2023 02:52
WG2064057
Isopropylbenzene
U
0.105
1.00
1 05/22/2023 02:52
WG2064057
p-Isopropyltoluene
U
0.120
1.00
1 05/22/2023 02:52
WG2064057
2-Butanone (MEK)
U
1.19
10.0
1 05/22/2023 02:52
WG2064057
Methylene Chloride
U
0.430
5.00
1 05/22/2023 02:52
WG2064057
4-Methyl-2-pentanone (MIBK)
U
0.478
10.0
1 05/22/2023 02:52
WG2064057
Methyl tert-butyl ether
U
0.101
1.00
1 05/22/2023 02:52
WG2064057
Naphthalene
U
1.00
5.00
1 05/22/2023 02:52
WG2064057
n-Propylbenzene
U
0.0993
1.00
1 05/22/2023 02:52
WG2064057
Styrene
U
0.118
1.00
1 05/22/2023 02:52
WG2064057
1,1,1,2-Tetrachloroethane
U
0.147
1.00
1 05/22/2023 02:52
WG2064057
1,1,2,2-Tetrachloroethane
U
0.133
1.00
1 05/22/2023 02:52
WG2064057
Tetrachloroethene
U
0.300
1.00
1 05/22/2023 02:52
WG2064057
Toluene
U
0.278
1.00
1 05/22/2023 02:52
WG2064057
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/22/2023 02:52
WG2064057
1,2,4-Trichlorobenzene
U
0.481
1.00
1 05/22/2023 02:52
WG2064057
1,1,1-Trichloroethane
U
0.149
1.00
1 05/22/2023 02:52
WG2064057
1,1,2-Trichloroethane
U
0.158
1.00
1 05/22/2023 02:52
WG2064057
Trichloroethene
U
0.190
1.00
1 05/22/2023 02:52
WG2064057
Trichlorofluoromethane
U
0.160
5.00
1 05/22/2023 02:52
WG2064057
1,2,3-Trichloropropane
U
0.237
2.50
1 05/22/2023 02:52
WG2064057
1,2,4-Trimethylbenzene
U
0.322
1.00
1 05/22/2023 02:52
WG2064057
1,3,5-Trimethyl benzene
U
0.104
1.00
1 05/22/2023 02:52
WG2064057
Vinyl acetate
U
0.692
10.0
1 05/22/2023 02:52
WG2064057
Vinyl chloride
U
0.234
1.00
1 05/22/2023 02:52
WG2064057
o-Xylene
U
J4 0.174
1.00
1 05/22/2023 02:52
WG2064057
m&p-Xylenes
U
0.430
2.00
1 05/22/2023 02:52
WG2064057
(S) Toluene-d8
103
80.0-120
0512212023 02:52
WG2064057
(S) 4-Bromof/uorobenzene
96.6
77.0-126
0512212023 02:52
WG2064057
(S)1,2-Dich/oroethone-d4
90.1
70.0-130
0512212023 02:52
WG2064057
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/I ug/I ug/I date / time
Acenaphthene
U
0.0886
1.00
1 05/17/2023 03:34
WG2059503
Acenaphthylene
U
0.0921
1.00
1 05/17/2023 03:34
WG2059503
Anthracene
U
0.0804
1.00
1 05/17/2023 03:34
WG2059503
Benzidine
U
3.74
10.0
1 05/17/2023 03:34
WG2059503
Benzo(a)anth race ne
U
0.199
1.00
1 05/17/2023 03:34
WG2059503
Benzo(b)fluoranthene
U
0.130
1.00
1 05/17/2023 03:34
WG2059503
Benzo(k)fluoranthene
U
0.120
1.00
1 05/17/2023 03:34
WG2059503
Benzo(g,h,i)perylene
U
0.121
1.00
1 05/17/2023 03:34
WG2059503
Benzo(a)pyrene
U
0.0381
1.00
1 05/17/2023 03:34
WG2059503
Bis(2-chlorethoxy)methane
U
0.116
10.0
1 05/17/2023 03:34
WG2059503
Bis(2-chloroethyl)ether
U
0.137
10.0
1 05/17/2023 03:34
WG2059503
2,2-Oxybis(1-Chloropropane)
U
0.210
10.0
1 05/17/2023 03:34
WG2059503
4-Bromophenyl-phenylether
U
0.0877
10.0
1 05/17/2023 03:34
WG2059503
2-Chloronaphthalene
U
0.0648
1.00
1 05/17/2023 03:34
WG2059503
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 56 of 132

TW-5 SAMPLE RESULTS - 16
Collected date/time: 05/11/23 16:45 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
4-Chlorophenyl-phenylether
U
0.0926
10.0
1 05/17/2023 03:34
WG2059503
Chrysene
U
0.130
1.00
1 05/17/2023 03:34
WG2059503
Dibenz(a,h)anthracene
U
0.0644
1.00
1 05/17/2023 03:34
WG2059503
3,3-Dichlorobenzidine
U
0.212
10.0
1 05/17/2023 03:34
WG2059503
2,4-Dinitrotoluene
U
0.0983
10.0
1 05/17/2023 03:34
WG2059503
2,6-Dinitrotoluene
U
0.250
10.0
1 05/17/2023 03:34
WG2059503
Fluoranthene
U
0.102
1.00
1 05/17/2023 03:34
WG2059503
Fluorene
U
0.0844
1.00
1 05/17/2023 03:34
WG2059503
Hexachlorobenzene
U
0.0755
1.00
1 05/17/2023 03:34
WG2059503
Hexachloro-1,3-butadiene
U
0.0968
10.0
1 05/17/2023 03:34
WG2059503
Hexachlorocyclopentadiene
U
0.0598
10.0
1 05/17/2023 03:34
WG2059503
Hexachloroethane
U
0.127
10.0
1 05/17/2023 03:34
WG2059503
Indeno(1,2,3-cd)pyrene
U
0.279
1.00
1 05/17/2023 03:34
WG2059503
Isophorone
U
0.143
10.0
1 05/17/2023 03:34
WG2059503
Naphthalene
U
0.159
1.00
1 05/17/2023 03:34
WG2059503
Nitrobenzene
U
0.297
10.0
1 05/17/2023 03:34
WG2059503
n-Nitrosodimethyla mine
U
0.998
10.0
1 05/17/2023 03:34
WG2059503
n-Nitrosodiphenyla mine
U
2.37
10.0
1 05/17/2023 03:34
WG2059503
n-Nitrosodi-n-propylamine
U
0.261
10.0
1 05/17/2023 03:34
WG2059503
Phenanthrene
U
0.112
1.00
1 05/17/2023 03:34
WG2059503
Benzylbutyl phthalate
U
0.765
3.00
1 05/17/2023 03:34
WG2059503
Bis(2-ethylhexyl)phthalate
U
0.895
3.00
1 05/17/2023 03:34
WG2059503
Di-n-butyl phthalate
0.736
B J 0.453
3.00
1 05/17/2023 03:34
WG2059503
Diethyl phthalate
3.81
0.287
3.00
1 05/17/2023 03:34
WG2059503
Dimethyl phthalate
U
0.260
3.00
1 05/17/2023 03:34
WG2059503
Di-n-octyl phthalate
U
0.932
3.00
1 05/17/2023 03:34
WG2059503
Pyrene
U
0.107
1.00
1 05/17/2023 03:34
WG2059503
1,2,4-Trichlorobenzene
U
0.0698
10.0
1 05/17/2023 03:34
WG2059503
4-Chloro-3-methylphenol
U
0.131
10.0
1 05/17/2023 03:34
WG2059503
2-Chlorophenol
U
0.133
10.0
1 05/17/2023 03:34
WG2059503
2,4-Dichlorophenol
U
0.102
10.0
1 05/17/2023 03:34
WG2059503
2,4-Dimethylphenol
U
0.0636
10.0
1 05/17/2023 03:34
WG2059503
4,6-Dinitro-2-methylphenol
U
1.12
10.0
1 05/17/2023 03:34
WG2059503
2,4-Dinitrophenol
U
5.93
10.0
1 05/17/2023 03:34
WG2059503
2-Nitrophenol
U
0.117
10.0
1 05/17/2023 03:34
WG2059503
4-Nitrophenol
U
0.143
10.0
1 05/17/2023 03:34
WG2059503
Pentachlorophenol
U
0.313
10.0
1 05/17/2023 03:34
WG2059503
Phenol
U
4.33
10.0
1 05/17/2023 03:34
WG2059503
2,4,6-Trichlorophenol
U
0.100
10.0
1 05/17/2023 03:34
WG2059503
(S) Nitrobenzene-d5
56.8
15.0-314
0511712023 03:34
WG2059503
(S) 2-Fluorobiphenyl
55.7
22.0-127
0511712023 03:34
WG2059503
(S) p-Terphenyl-d14
65.4
29.0-141
0511712023 03:34
WG2059503
(S) Phenol-d5
14.8
8.00-424
0511712023 03:34
WG2059503
(S) 2-F/uorophenol
18.2
10.0-120
0511712023 03:34
WG2059503
(S) 2,4,6- Tribromophenol
40.7
10.0-153
051171202303:34
WG2059503
FP1
FTc
FSS
4
Cn
RC
F
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 57 of 132

TW-6
Collected date/time: 05/11/23 17:30
Wet Chemistry by Method 7199
SAMPLE
RESULTS - 17
L1616119
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Hexavalent Chromium -Low U
0.0400
0.100
1 05/18/2023 06:08
WG2059859
Level
Mercury by Method 7470A
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Mercury U
0.100
0.200
1 06/05/2023 20:02
WG2060584
Metals (ICPMS) by Method 6020B
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Arsenic
0.186
J
0.180
2.00
1 05/23/2023 22:37
WG2060154
Barium
20.4
0.381
2.00
1 05/23/2023 22:37
WG2060154
Cadmium
U
0.150
1.00
1 05/23/2023 22:37
WG2060154
Chromium
U
1.24
2.00
1 05/23/2023 22:37
WG2060154
Lead
1.02
J
0.849
2.00
1 05/23/2023 22:37
WG2060154
Selenium
0.331
J
0.300
2.00
1 05/23/2023 22:37
WG2060154
Silver
U
0.0700
2.00
1 05/23/2023 22:37
WG2060154
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
11.3
50.0
1 05/22/2023 03:11
WG2064057
Acrolein
U
2.54
50.0
1 05/22/2023 03:11
WG2064057
Acrylonitrile
U
0.671
10.0
1 05/22/2023 03:11
WG2064057
Benzene
U
0.0941
1.00
1 05/22/2023 03:11
WG2064057
Bromobenzene
U
0.118
1.00
1 05/22/2023 03:11
WG2064057
Bromochloromethane
U
0.128
1.00
1 05/22/2023 03:11
WG2064057
Bromodichloromethane
U
0.136
1.00
1 05/22/2023 03:11
WG2064057
Bromoform
U
0.129
1.00
1 05/22/2023 03:11
WG2064057
Bromomethane
U
0.605
5.00
1 05/22/2023 03:11
WG2064057
n-Butylbenzene
6.55
0.157
1.00
1 05/22/2023 03:11
WG2064057
sec -Butyl benzene
1.06
0.125
1.00
1 05/22/2023 03:11
WG2064057
tert-Butylbenzene
U
0.127
1.00
1 05/22/2023 03:11
WG2064057
Carbon tetrachloride
U
0.128
1.00
1 05/22/2023 03:11
WG2064057
Chlorobenzene
U
0.116
1.00
1 05/22/2023 03:11
WG2064057
Chlorodibromomethane
U
0.140
1.00
1 05/22/2023 03:11
WG2064057
Chloroethane
U
0.192
5.00
1 05/22/2023 03:11
WG2064057
Chloroform
U
0.111
5.00
1 05/22/2023 03:11
WG2064057
Chloromethane
U
0.960
2.50
1 05/22/2023 03:11
WG2064057
2-Chlorotoluene
U
0.106
1.00
1 05/22/2023 03:11
WG2064057
4-Chlorotoluene
U
0.114
1.00
1 05/22/2023 03:11
WG2064057
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1 05/22/2023 03:11
WG2064057
1,2-Dibromoethane
U
0.126
1.00
1 05/22/2023 03:11
WG2064057
Dibromomethane
U
0.122
1.00
1 05/22/2023 03:11
WG2064057
1,2-Dichlorobenzene
U
0.107
1.00
1 05/22/2023 03:11
WG2064057
1,3-Dichlorobenzene
U
0.110
1.00
1 05/22/2023 03:11
WG2064057
1,4-Dichlorobenzene
U
0.120
1.00
1 05/22/2023 03:11
WG2064057
Dichlorodifluoromethane
U
0.374
5.00
1 05/22/2023 03:11
WG2064057
1,1-Dichloroethane
U
0.100
1.00
1 05/22/2023 03:11
WG2064057
1,2-Dichloroethane
U
0.0819
1.00
1 05/22/2023 03:11
WG2064057
1,1-Dichloroethene
U
0.188
1.00
1 05/22/2023 03:11
WG2064057
cis-1,2-Dichloroethene
U
0.126
1.00
1 05/22/2023 03:11
WG2064057
trans-1,2-Dichloroethene
U
0.149
1.00
1 05/22/2023 03:11
WG2064057
1,2-Dichloropropane
U
0.149
1.00
1 05/22/2023 03:11
WG2064057
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
Fp]
FTC
FSS
4
Cn
RC
F ql
FAI
FSC
PAGE:
58 of 132

TW-6 SAMPLE RESULTS - 17
Collected date/time: 05/11/23 17:30 L1616119
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
1,1-Dichloropropene
U
0.142
1.00
1 05/22/2023 03:11
WG2064057
1,3-Dichloropropane
U
0.110
1.00
1 05/22/2023 03:11
WG2064057
cis-1,3-Dichloropropene
U
0.111
1.00
1 05/22/2023 03:11
WG2064057
trans-1,3-Dichloropropene
U
0.118
1.00
1 05/22/2023 03:11
WG2064057
2,2-Dichloropropane
U
0.161
1.00
1 05/22/2023 03:11
WG2064057
Di -isopropyl ether
U
0.105
1.00
1 05/22/2023 03:11
WG2064057
Ethylbenzene
U
0.137
1.00
1 05/22/2023 03:11
WG2064057
Hexachloro-1,3-butadiene
U
0.337
1.00
1 05/22/2023 03:11
WG2064057
2-Hexanone
U
0.787
10.0
1 05/22/2023 03:11
WG2064057
Isopropylbenzene
U
0.105
1.00
1 05/22/2023 03:11
WG2064057
p-Isopropyltoluene
2.21
0.120
1.00
1 05/22/2023 03:11
WG2064057
2-Butanone (MEK)
U
1.19
10.0
1 05/22/2023 03:11
WG2064057
Methylene Chloride
U
0.430
5.00
1 05/22/2023 03:11
WG2064057
4-Methyl-2-pentanone (MIBK)
U
0.478
10.0
1 05/22/2023 03:11
WG2064057
Methyl tert-butyl ether
U
0.101
1.00
1 05/22/2023 03:11
WG2064057
Naphthalene
U
1.00
5.00
1 05/22/2023 03:11
WG2064057
n-Propylbenzene
U
0.0993
1.00
1 05/22/2023 03:11
WG2064057
Styrene
U
0.118
1.00
1 05/22/2023 03:11
WG2064057
1,1,1,2-Tetrachloroethane
U
0.147
1.00
1 05/22/2023 03:11
WG2064057
1,1,2,2-Tetrachloroethane
0.169
J
0.133
1.00
1 05/22/2023 03:11
WG2064057
Tetrachloroethene
U
0.300
1.00
1 05/22/2023 03:11
WG2064057
Toluene
U
0.278
1.00
1 05/22/2023 03:11
WG2064057
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/22/2023 03:11
WG2064057
1,2,4-Trichlorobenzene
U
0.481
1.00
1 05/22/2023 03:11
WG2064057
1,1,1-Trichloroethane
U
0.149
1.00
1 05/22/2023 03:11
WG2064057
1,1,2-Trichloroethane
U
0.158
1.00
1 05/22/2023 03:11
WG2064057
Trichloroethene
U
0.190
1.00
1 05/22/2023 03:11
WG2064057
Trichlorofluoromethane
U
0.160
5.00
1 05/22/2023 03:11
WG2064057
1,2,3-Trichloropropane
U
0.237
2.50
1 05/22/2023 03:11
WG2064057
1,2,4-Trimethylbenzene
0.722
J
0.322
1.00
1 05/22/2023 03:11
WG2064057
1,3,5-Trimethyl benzene
0.251
J_
0.104
1.00
1 05/22/2023 03:11
WG2064057
Vinyl acetate
U
0.692
10.0
1 05/22/2023 03:11
WG2064057
Vinyl chloride
U
0.234
1.00
1 05/22/2023 03:11
WG2064057
o-Xylene
4.43
J4
0.174
1.00
1 05/22/2023 03:11
WG2064057
m&p-Xylenes
U
0.430
2.00
1 05/22/2023 03:11
WG2064057
(S) Toluene-d8
102
80.0-120
0512212023 03:11
WG2064057
(S) 4-Bromof/uorobenzene
95.7
77.0-126
0512212023 03:11
WG2064057
(S)1,2-Dich/oroethone-d4
91.3
70.0-130
0512212023 03:11
WG2064057
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/I ug/I ug/I date / time
Acenaphthene
U
0.0886
1.00
1 05/17/2023 03:55
WG2059503
Acenaphthylene
U
0.0921
1.00
1 05/17/2023 03:55
WG2059503
Anthracene
U
0.0804
1.00
1 05/17/2023 03:55
WG2059503
Benzidine
U
3.74
10.0
1 05/17/2023 03:55
WG2059503
Benzo(a)anth race ne
U
0.199
1.00
1 05/17/2023 03:55
WG2059503
Benzo(b)fluoranthene
U
0.130
1.00
1 05/17/2023 03:55
WG2059503
Benzo(k)fluoranthene
U
0.120
1.00
1 05/17/2023 03:55
WG2059503
Benzo(g,h,i)perylene
U
0.121
1.00
1 05/17/2023 03:55
WG2059503
Benzo(a)pyrene
U
0.0381
1.00
1 05/17/2023 03:55
WG2059503
Bis(2-chlorethoxy)methane
U
0.116
10.0
1 05/17/2023 03:55
WG2059503
Bis(2-chloroethyl)ether
U
0.137
10.0
1 05/17/2023 03:55
WG2059503
2,2-Oxybis(1-Chloropropane)
U
0.210
10.0
1 05/17/2023 03:55
WG2059503
4-Bromophenyl-phenylether
U
0.0877
10.0
1 05/17/2023 03:55
WG2059503
2-Chloronaphthalene
U
0.0648
1.00
1 05/17/2023 03:55
WG2059503
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 59 of 132

TW-6 SAMPLE RESULTS - 17
Collected date/time: 05/11/23 17:30 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
4-Chlorophenyl-phenylether
U
0.0926
10.0
1 05/17/2023 03:55
WG2059503
Chrysene
U
0.130
1.00
1 05/17/2023 03:55
WG2059503
Dibenz(a,h)anthracene
U
0.0644
1.00
1 05/17/2023 03:55
WG2059503
3,3-Dichlorobenzidine
U
0.212
10.0
1 05/17/2023 03:55
WG2059503
2,4-Dinitrotoluene
U
0.0983
10.0
1 05/17/2023 03:55
WG2059503
2,6-Dinitrotoluene
U
0.250
10.0
1 05/17/2023 03:55
WG2059503
Fluoranthene
U
0.102
1.00
1 05/17/2023 03:55
WG2059503
Fluorene
U
0.0844
1.00
1 05/17/2023 03:55
WG2059503
Hexachlorobenzene
U
0.0755
1.00
1 05/17/2023 03:55
WG2059503
Hexachloro-1,3-butadiene
U
0.0968
10.0
1 05/17/2023 03:55
WG2059503
Hexachlorocyclopentadiene
U
0.0598
10.0
1 05/17/2023 03:55
WG2059503
Hexachloroethane
U
0.127
10.0
1 05/17/2023 03:55
WG2059503
Indeno(1,2,3-cd)pyrene
U
0.279
1.00
1 05/17/2023 03:55
WG2059503
Isophorone
U
0.143
10.0
1 05/17/2023 03:55
WG2059503
Naphthalene
U
0.159
1.00
1 05/17/2023 03:55
WG2059503
Nitrobenzene
U
0.297
10.0
1 05/17/2023 03:55
WG2059503
n-Nitrosodimethyla mine
U
0.998
10.0
1 05/17/2023 03:55
WG2059503
n-Nitrosodiphenyla mine
U
2.37
10.0
1 05/17/2023 03:55
WG2059503
n-Nitrosodi-n-propylamine
U
0.261
10.0
1 05/17/2023 03:55
WG2059503
Phenanthrene
U
0.112
1.00
1 05/17/2023 03:55
WG2059503
Benzylbutyl phthalate
U
0.765
3.00
1 05/17/2023 03:55
WG2059503
Bis(2-ethylhexyl)phthalate
U
0.895
3.00
1 05/17/2023 03:55
WG2059503
Di-n-butyl phthalate
U
0.453
3.00
1 05/17/2023 03:55
WG2059503
Diethyl phthalate
U
0.287
3.00
1 05/17/2023 03:55
WG2059503
Dimethyl phthalate
U
0.260
3.00
1 05/17/2023 03:55
WG2059503
Di-n-octyl phthalate
U
0.932
3.00
1 05/17/2023 03:55
WG2059503
Pyrene
U
0.107
1.00
1 05/17/2023 03:55
WG2059503
1,2,4-Trichlorobenzene
U
0.0698
10.0
1 05/17/2023 03:55
WG2059503
4-Chloro-3-methylphenol
U
0.131
10.0
1 05/17/2023 03:55
WG2059503
2-Chlorophenol
U
0.133
10.0
1 05/17/2023 03:55
WG2059503
2,4-Dichlorophenol
U
0.102
10.0
1 05/17/2023 03:55
WG2059503
2,4-Dimethylphenol
U
0.0636
10.0
1 05/17/2023 03:55
WG2059503
4,6-Dinitro-2-methylphenol
U
1.12
10.0
1 05/17/2023 03:55
WG2059503
2,4-Dinitrophenol
U
5.93
10.0
1 05/17/2023 03:55
WG2059503
2-Nitrophenol
U
0.117
10.0
1 05/17/2023 03:55
WG2059503
4-Nitrophenol
U
0.143
10.0
1 05/17/2023 03:55
WG2059503
Pentachlorophenol
U
0.313
10.0
1 05/17/2023 03:55
WG2059503
Phenol
U
4.33
10.0
1 05/17/2023 03:55
WG2059503
2,4,6-Trichlorophenol
U
0.100
10.0
1 05/17/2023 03:55
WG2059503
(S) Nitrobenzene-d5
46.4
15.0-314
0511712023 03:55
WG2059503
(S) 2-Fluorobiphenyl
46.6
22.0-127
0511712023 03:55
WG2059503
(S) p-Terphenyl-d14
45.8
29.0-141
0511712023 03:55
WG2059503
(S) Phenol-d5
15.4
8.00-424
0511712023 03:55
WG2059503
(S) 2-F/uorophenol
19.5
10.0-120
0511712023 03:55
WG2059503
(S) 2,4,6- Tribromophenol
32.3
10.0-153
051171202303:55
WG2059503
FP1
FTc
FSS
4
Cn
RC
F
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 60 of 132

-------------
TW-7
Collected date/time: 05/12/23 12:10
Wet Chemistry by Method 7199
SAMPLE
RESULTS - 18
L1616119
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Hexavalent Chromium -Low U
0.0400
0.100
1 05/18/2023 06:16
WG2059859
Level
Mercury by Method 7470A
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Mercury U
0.100
0.200
1 06/05/2023 20:05
WG2060584
Metals (ICPMS) by Method 6020B
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Arsenic
U
0.180
2.00
1 05/23/2023 22:41
WG2060154
Barium
17.4
0.381
2.00
1 05/23/2023 22:41
WG2060154
Cadmium
U
0.150
1.00
1 05/23/2023 22:41
WG2060154
Chromium
U
1.24
2.00
1 05/23/2023 22:41
WG2060154
Lead
U
0.849
2.00
1 05/23/2023 22:41
WG2060154
Selenium
U
0.300
2.00
1 05/23/2023 22:41
WG2060154
Silver
U
0.0700
2.00
1 05/23/2023 22:41
WG2060154
Volatile Organic Compounds (GC/MS)
by Method 620OB-1997/620OB-2011
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
11.3
50.0
1 05/22/2023 03:30
WG2064057
Acrolein
U
2.54
50.0
1 05/22/2023 03:30
WG2064057
Acrylonitrile
U
0.671
10.0
1 05/22/2023 03:30
WG2064057
Benzene
U
0.0941
1.00
1 05/22/2023 03:30
WG2064057
Bromobenzene
U
0.118
1.00
1 05/22/2023 03:30
WG2064057
Bromochloromethane
U
0.128
1.00
1 05/22/2023 03:30
WG2064057
Bromodichloromethane
U
0.136
1.00
1 05/22/2023 03:30
WG2064057
Bromoform
U
0.129
1.00
1 05/22/2023 03:30
WG2064057
Bromomethane
U
0.605
5.00
1 05/22/2023 03:30
WG2064057
n-Butylbenzene
U
0.157
1.00
1 05/22/2023 03:30
WG2064057
sec -Butyl benzene
U
0.125
1.00
1 05/22/2023 03:30
WG2064057
tert-Butylbenzene
U
0.127
1.00
1 05/22/2023 03:30
WG2064057
Carbon tetrachloride
U
0.128
1.00
1 05/22/2023 03:30
WG2064057
Chlorobenzene
U
0.116
1.00
1 05/22/2023 03:30
WG2064057
Chlorodibromomethane
U
0.140
1.00
1 05/22/2023 03:30
WG2064057
Chloroethane
U
0.192
5.00
1 05/22/2023 03:30
WG2064057
Chloroform
U
0.111
5.00
1 05/22/2023 03:30
WG2064057
Chloromethane
U
0.960
2.50
1 05/22/2023 03:30
WG2064057
2-Chlorotoluene
U
0.106
1.00
1 05/22/2023 03:30
WG2064057
4-Chlorotoluene
U
0.114
1.00
1 05/22/2023 03:30
WG2064057
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1 05/22/2023 03:30
WG2064057
1,2-Dibromoethane
U
0.126
1.00
1 05/22/2023 03:30
WG2064057
Dibromomethane
U
0.122
1.00
1 05/22/2023 03:30
WG2064057
1,2-Dichlorobenzene
U
0.107
1.00
1 05/22/2023 03:30
WG2064057
1,3-Dichlorobenzene
U
0.110
1.00
1 05/22/2023 03:30
WG2064057
1,4-Dichlorobenzene
U
0.120
1.00
1 05/22/2023 03:30
WG2064057
Dichlorodifluoromethane
U
0.374
5.00
1 05/22/2023 03:30
WG2064057
1,1-Dichloroethane
U
0.100
1.00
1 05/22/2023 03:30
WG2064057
1,2-Dichloroethane
U
0.0819
1.00
1 05/22/2023 03:30
WG2064057
1,1-Dichloroethene
U
0.188
1.00
1 05/22/2023 03:30
WG2064057
cis-1,2-Dichloroethene
U
0.126
1.00
1 05/22/2023 03:30
WG2064057
trans-1,2-Dichloroethene
U
0.149
1.00
1 05/22/2023 03:30
WG2064057
1,2-Dichloropropane
U
0.149
1.00
1 05/22/2023 03:30
WG2064057
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
Fp]
FTC
FSS
4
Cn
RC
F ql
FAI
FSC
61 of 132

TW-7 SAMPLE RESULTS - 18
Collected date/time: 05/12/23 12:10 L1616119
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
1,1-Dichloropropene
U
0.142
1.00
1 05/22/2023 03:30
WG2064057
1,3-Dichloropropane
U
0.110
1.00
1 05/22/2023 03:30
WG2064057
cis-1,3-Dichloropropene
U
0.111
1.00
1 05/22/2023 03:30
WG2064057
trans-1,3-Dichloropropene
U
0.118
1.00
1 05/22/2023 03:30
WG2064057
2,2-Dichloropropane
U
0.161
1.00
1 05/22/2023 03:30
WG2064057
Di -isopropyl ether
U
0.105
1.00
1 05/22/2023 03:30
WG2064057
Ethylbenzene
U
0.137
1.00
1 05/22/2023 03:30
WG2064057
Hexachloro-1,3-butadiene
U
0.337
1.00
1 05/22/2023 03:30
WG2064057
2-Hexanone
U
0.787
10.0
1 05/22/2023 03:30
WG2064057
Isopropylbenzene
U
0.105
1.00
1 05/22/2023 03:30
WG2064057
p-Isopropyltoluene
U
0.120
1.00
1 05/22/2023 03:30
WG2064057
2-Butanone (MEK)
U
1.19
10.0
1 05/22/2023 03:30
WG2064057
Methylene Chloride
U
0.430
5.00
1 05/22/2023 03:30
WG2064057
4-Methyl-2-pentanone (MIBK)
U
0.478
10.0
1 05/22/2023 03:30
WG2064057
Methyl tert-butyl ether
U
0.101
1.00
1 05/22/2023 03:30
WG2064057
Naphthalene
U
1.00
5.00
1 05/22/2023 03:30
WG2064057
n-Propylbenzene
U
0.0993
1.00
1 05/22/2023 03:30
WG2064057
Styrene
U
0.118
1.00
1 05/22/2023 03:30
WG2064057
1,1,1,2-Tetrachloroethane
U
0.147
1.00
1 05/22/2023 03:30
WG2064057
1,1,2,2-Tetrachloroethane
U
0.133
1.00
1 05/22/2023 03:30
WG2064057
Tetrachloroethene
U
0.300
1.00
1 05/22/2023 03:30
WG2064057
Toluene
U
0.278
1.00
1 05/22/2023 03:30
WG2064057
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/22/2023 03:30
WG2064057
1,2,4-Trichlorobenzene
U
0.481
1.00
1 05/22/2023 03:30
WG2064057
1,1,1-Trichloroethane
U
0.149
1.00
1 05/22/2023 03:30
WG2064057
1,1,2-Trichloroethane
U
0.158
1.00
1 05/22/2023 03:30
WG2064057
Trichloroethene
U
0.190
1.00
1 05/22/2023 03:30
WG2064057
Trichlorofluoromethane
U
0.160
5.00
1 05/22/2023 03:30
WG2064057
1,2,3-Trichloropropane
U
0.237
2.50
1 05/22/2023 03:30
WG2064057
1,2,4-Trimethylbenzene
U
0.322
1.00
1 05/22/2023 03:30
WG2064057
1,3,5-Trimethyl benzene
U
0.104
1.00
1 05/22/2023 03:30
WG2064057
Vinyl acetate
U
0.692
10.0
1 05/22/2023 03:30
WG2064057
Vinyl chloride
U
0.234
1.00
1 05/22/2023 03:30
WG2064057
o-Xylene
U
J4 0.174
1.00
1 05/22/2023 03:30
WG2064057
m&p-Xylenes
U
0.430
2.00
1 05/22/2023 03:30
WG2064057
(S) Toluene-d8
104
80.0-120
0512212023 0330
WG2064057
(S) 4-Bromof/uorobenzene
98.4
77.0-126
0512212023 03:30
WG2064057
(S) 1,2-Dich/oroethone-d4
92.1
70.0-130
0512212023 0330
WG2064057
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/I ug/I ug/I date / time
Acenaphthene
U
0.0886
1.00
1 05/20/2023 01:41
WG2061246
Acenaphthylene
U
0.0921
1.00
1 05/20/2023 01:41
WG2061246
Anthracene
U
0.0804
1.00
1 05/20/2023 01:41
WG2061246
Benzidine
U
3.74
10.0
1 05/20/2023 01:41
WG2061246
Benzo(a)anth race ne
U
0.199
1.00
1 05/20/2023 01:41
WG2061246
Benzo(b)fluoranthene
U
0.130
1.00
1 05/20/2023 01:41
WG2061246
Benzo(k)fluoranthene
U
0.120
1.00
1 05/20/2023 01:41
WG2061246
Benzo(g,h,i)perylene
U
0.121
1.00
1 05/20/2023 01:41
WG2061246
Benzo(a)pyrene
U
0.0381
1.00
1 05/20/2023 01:41
WG2061246
Bis(2-chlorethoxy)methane
U
0.116
10.0
1 05/20/2023 01:41
WG2061246
Bis(2-chloroethyl)ether
U
0.137
10.0
1 05/20/2023 01:41
WG2061246
2,2-Oxybis(1-Chloropropane)
U
0.210
10.0
1 05/20/2023 01:41
WG2061246
4-Bromophenyl-phenylether
U
0.0877
10.0
1 05/20/2023 01:41
WG2061246
2-Chloronaphthalene
U
0.0648
1.00
1 05/20/2023 01:41
WG2061246
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 62 of 132

TW-7 SAMPLE RESULTS - 18
Collected date/time: 05/12/23 12:10 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
4-Chlorophenyl-phenylether
U
0.0926
10.0
1 05/20/2023 01:41
WG2061246
Chrysene
U
0.130
1.00
1 05/20/2023 01:41
WG2061246
Dibenz(a,h)anthracene
U
0.0644
1.00
1 05/20/2023 01:41
WG2061246
3,3-Dichlorobenzidine
U
0.212
10.0
1 05/20/2023 01:41
WG2061246
2,4-Dinitrotoluene
U
0.0983
10.0
1 05/20/2023 01:41
WG2061246
2,6-Dinitrotoluene
U
0.250
10.0
1 05/20/2023 01:41
WG2061246
Fluoranthene
U
0.102
1.00
1 05/20/2023 01:41
WG2061246
Fluorene
U
0.0844
1.00
1 05/20/2023 01:41
WG2061246
Hexachlorobenzene
U
0.0755
1.00
1 05/20/2023 01:41
WG2061246
Hexachloro-1,3-butadiene
U
0.0968
10.0
1 05/20/2023 01:41
WG2061246
Hexachlorocyclopentadiene
U
0.0598
10.0
1 05/20/2023 01:41
WG2061246
Hexachloroethane
U
0.127
10.0
1 05/20/2023 01:41
WG2061246
Indeno(1,2,3-cd)pyrene
U
0.279
1.00
1 05/20/2023 01:41
WG2061246
Isophorone
U
0.143
10.0
1 05/20/2023 01:41
WG2061246
Naphthalene
U
0.159
1.00
1 05/20/2023 01:41
WG2061246
Nitrobenzene
U
0.297
10.0
1 05/20/2023 01:41
WG2061246
n-Nitrosodimethyla mine
U
0.998
10.0
1 05/20/2023 01:41
WG2061246
n-Nitrosodiphenyla mine
U
2.37
10.0
1 05/20/2023 01:41
WG2061246
n-Nitrosodi-n-propylamine
U
0.261
10.0
1 05/20/2023 01:41
WG2061246
Phenanthrene
U
0.112
1.00
1 05/20/2023 01:41
WG2061246
Benzylbutyl phthalate
U
0.765
3.00
1 05/20/2023 01:41
WG2061246
Bis(2-ethylhexyl)phthalate
U
0.895
3.00
1 05/20/2023 01:41
WG2061246
Di-n-butyl phthalate
U
0.453
3.00
1 05/20/2023 01:41
WG2061246
Diethyl phthalate
2.52
J_ 0.287
3.00
1 05/20/2023 01:41
WG2061246
Dimethyl phthalate
U
0.260
3.00
1 05/20/2023 01:41
WG2061246
Di-n-octyl phthalate
U
0.932
3.00
1 05/20/2023 01:41
WG2061246
Pyrene
U
0.107
1.00
1 05/20/2023 01:41
WG2061246
1,2,4-Trichlorobenzene
U
0.0698
10.0
1 05/20/2023 01:41
WG2061246
4-Chloro-3-methylphenol
U
0.131
10.0
1 05/20/2023 01:41
WG2061246
2-Chlorophenol
U
0.133
10.0
1 05/20/2023 01:41
WG2061246
2,4-Dichlorophenol
U
0.102
10.0
1 05/20/2023 01:41
WG2061246
2,4-Dimethylphenol
U
0.0636
10.0
1 05/20/2023 01:41
WG2061246
4,6-Dinitro-2-methylphenol
U
1.12
10.0
1 05/20/2023 01:41
WG2061246
2,4-Dinitrophenol
U
5.93
10.0
1 05/20/2023 01:41
WG2061246
2-Nitrophenol
U
0.117
10.0
1 05/20/2023 01:41
WG2061246
4-Nitrophenol
U
J4 0.143
10.0
1 05/20/2023 01:41
WG2061246
Pentachlorophenol
U
0.313
10.0
1 05/20/2023 01:41
WG2061246
Phenol
U
4.33
10.0
1 05/20/2023 01:41
WG2061246
2,4,6-Trichlorophenol
U
0.100
10.0
1 05/20/2023 01:41
WG2061246
(S) Nitrobenzene-d5
71.8
15.0-314
0512012023 01.41
WG2061246
(S) 2-Fluorobiphenyl
54.1
22.0-127
0512012023 01.41
WG2061246
(S) p-Terphenyl-d14
75.1
29.0-141
0512012023 01.41
WG2061246
(S) Phenol-d5
14.5
8.00-424
0512012023 01.41
WG2061246
(S) 2-F/uorophenol
25.5
10.0-120
0512012023 01.41
WG2061246
(S) 2,4,6- Tribromophenol
51.0
10.0-153
051201202301.41
WG2061246
FP1
FTc
FSS
4
Cn
RC
F
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 63 of 132

TW-8
Collected date/time: 05/12/23 11:45
Wet Chemistry by Method 7199
SAMPLE
RESULTS - 19
L1616119
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Hexavalent Chromium -Low U
0.0400
0.100
1 05/18/2023 06:24
WG2059859
Level
Mercury by Method 7470A
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Mercury U
0.100
0.200
1 06/05/202319:29
WG2060584
Metals (ICPMS) by Method 6020B
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Arsenic
U
0.180
2.00
1 05/23/2023 22:44
WG2060154
Barium
96.1
0.381
2.00
1 05/23/2023 22:44
WG2060154
Cadmium
U
0.150
1.00
1 05/23/2023 22:44
WG2060154
Chromium
U
1.24
2.00
1 05/23/2023 22:44
WG2060154
Lead
U
0.849
2.00
1 05/23/2023 22:44
WG2060154
Selenium
U
0.300
2.00
1 05/23/2023 22:44
WG2060154
Silver
U
0.0700
2.00
1 05/23/2023 22:44
WG2060154
Volatile Organic Compounds (GC/MS)
by Method 620OB-1997/620OB-2011
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
11.3
50.0
1 05/22/2023 03:49
WG2064057
Acrolein
U
2.54
50.0
1 05/22/2023 03:49
WG2064057
Acrylonitrile
U
0.671
10.0
1 05/22/2023 03:49
WG2064057
Benzene
U
0.0941
1.00
1 05/22/2023 03:49
WG2064057
Bromobenzene
U
0.118
1.00
1 05/22/2023 03:49
WG2064057
Bromochloromethane
U
0.128
1.00
1 05/22/2023 03:49
WG2064057
Bromodichloromethane
U
0.136
1.00
1 05/22/2023 03:49
WG2064057
Bromoform
U
0.129
1.00
1 05/22/2023 03:49
WG2064057
Bromomethane
U
0.605
5.00
1 05/22/2023 03:49
WG2064057
n-Butylbenzene
U
0.157
1.00
1 05/22/2023 03:49
WG2064057
sec -Butyl benzene
U
0.125
1.00
1 05/22/2023 03:49
WG2064057
tert-Butylbenzene
U
0.127
1.00
1 05/22/2023 03:49
WG2064057
Carbon tetrachloride
U
0.128
1.00
1 05/22/2023 03:49
WG2064057
Chlorobenzene
U
0.116
1.00
1 05/22/2023 03:49
WG2064057
Chlorodibromomethane
U
0.140
1.00
1 05/22/2023 03:49
WG2064057
Chloroethane
U
0.192
5.00
1 05/22/2023 03:49
WG2064057
Chloroform
U
0.111
5.00
1 05/22/2023 03:49
WG2064057
Chloromethane
U
0.960
2.50
1 05/22/2023 03:49
WG2064057
2-Chlorotoluene
U
0.106
1.00
1 05/22/2023 03:49
WG2064057
4-Chlorotoluene
U
0.114
1.00
1 05/22/2023 03:49
WG2064057
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1 05/22/2023 03:49
WG2064057
1,2-Dibromoethane
U
0.126
1.00
1 05/22/2023 03:49
WG2064057
Dibromomethane
U
0.122
1.00
1 05/22/2023 03:49
WG2064057
1,2-Dichlorobenzene
U
0.107
1.00
1 05/22/2023 03:49
WG2064057
1,3-Dichlorobenzene
U
0.110
1.00
1 05/22/2023 03:49
WG2064057
1,4-Dichlorobenzene
U
0.120
1.00
1 05/22/2023 03:49
WG2064057
Dichlorodifluoromethane
U
0.374
5.00
1 05/22/2023 03:49
WG2064057
1,1-Dichloroethane
U
0.100
1.00
1 05/22/2023 03:49
WG2064057
1,2-Dichloroethane
U
0.0819
1.00
1 05/22/2023 03:49
WG2064057
1,1-Dichloroethene
U
0.188
1.00
1 05/22/2023 03:49
WG2064057
cis-1,2-Dichloroethene
U
0.126
1.00
1 05/22/2023 03:49
WG2064057
trans-1,2-Dichloroethene
U
0.149
1.00
1 05/22/2023 03:49
WG2064057
1,2-Dichloropropane
U
0.149
1.00
1 05/22/2023 03:49
WG2064057
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
Fp]
FTC
FSS
4
Cn
RC
F ql
FAI
FSC
PAGE:
64 of 132

TW-8 SAMPLE RESULTS - 19
Collected date/time: 05/12/23 11:45 L1616119
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
1,1-Dichloropropene
U
0.142
1.00
1 05/22/2023 03:49
WG2064057
1,3-Dichloropropane
U
0.110
1.00
1 05/22/2023 03:49
WG2064057
cis-1,3-Dichloropropene
U
0.111
1.00
1 05/22/2023 03:49
WG2064057
trans-1,3-Dichloropropene
U
0.118
1.00
1 05/22/2023 03:49
WG2064057
2,2-Dichloropropane
U
0.161
1.00
1 05/22/2023 03:49
WG2064057
Di -isopropyl ether
U
0.105
1.00
1 05/22/2023 03:49
WG2064057
Ethylbenzene
U
0.137
1.00
1 05/22/2023 03:49
WG2064057
Hexachloro-1,3-butadiene
U
0.337
1.00
1 05/22/2023 03:49
WG2064057
2-Hexanone
U
0.787
10.0
1 05/22/2023 03:49
WG2064057
Isopropylbenzene
U
0.105
1.00
1 05/22/2023 03:49
WG2064057
p-Isopropyltoluene
U
0.120
1.00
1 05/22/2023 03:49
WG2064057
2-Butanone (MEK)
U
1.19
10.0
1 05/22/2023 03:49
WG2064057
Methylene Chloride
U
0.430
5.00
1 05/22/2023 03:49
WG2064057
4-Methyl-2-pentanone (MIBK)
U
0.478
10.0
1 05/22/2023 03:49
WG2064057
Methyl tert-butyl ether
U
0.101
1.00
1 05/22/2023 03:49
WG2064057
Naphthalene
U
1.00
5.00
1 05/22/2023 03:49
WG2064057
n-Propylbenzene
U
0.0993
1.00
1 05/22/2023 03:49
WG2064057
Styrene
U
0.118
1.00
1 05/22/2023 03:49
WG2064057
1,1,1,2-Tetrachloroethane
U
0.147
1.00
1 05/22/2023 03:49
WG2064057
1,1,2,2-Tetrachloroethane
U
0.133
1.00
1 05/22/2023 03:49
WG2064057
Tetrachloroethene
U
0.300
1.00
1 05/22/2023 03:49
WG2064057
Toluene
U
0.278
1.00
1 05/22/2023 03:49
WG2064057
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/22/2023 03:49
WG2064057
1,2,4-Trichlorobenzene
U
0.481
1.00
1 05/22/2023 03:49
WG2064057
1,1,1-Trichloroethane
U
0.149
1.00
1 05/22/2023 03:49
WG2064057
1,1,2-Trichloroethane
U
0.158
1.00
1 05/22/2023 03:49
WG2064057
Trichloroethene
U
0.190
1.00
1 05/22/2023 03:49
WG2064057
Trichlorofluoromethane
U
0.160
5.00
1 05/22/2023 03:49
WG2064057
1,2,3-Trichloropropane
U
0.237
2.50
1 05/22/2023 03:49
WG2064057
1,2,4-Trimethylbenzene
U
0.322
1.00
1 05/22/2023 03:49
WG2064057
1,3,5-Trimethyl benzene
U
0.104
1.00
1 05/22/2023 03:49
WG2064057
Vinyl acetate
U
0.692
10.0
1 05/22/2023 03:49
WG2064057
Vinyl chloride
U
0.234
1.00
1 05/22/2023 03:49
WG2064057
o-Xylene
U
J4 0.174
1.00
1 05/22/2023 03:49
WG2064057
m&p-Xylenes
U
0.430
2.00
1 05/22/2023 03:49
WG2064057
(S) Toluene-d8
103
80.0-120
0512212023 03:49
WG2064057
(S) 4-Bromof/uorobenzene
97.6
77.0-126
0512212023 03:49
WG2064057
(S) 1,2-Dich/oroethone-d4
93.4
70.0-130
0512212023 03:49
WG2064057
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/I ug/I ug/I date / time
Acenaphthene
U
0.0886
1.00
1 05/20/2023 02:02
WG2061246
Acenaphthylene
U
0.0921
1.00
1 05/20/2023 02:02
WG2061246
Anthracene
U
0.0804
1.00
1 05/20/2023 02:02
WG2061246
Benzidine
U
3.74
10.0
1 05/20/2023 02:02
WG2061246
Benzo(a)anth race ne
U
0.199
1.00
1 05/20/2023 02:02
WG2061246
Benzo(b)fluoranthene
U
0.130
1.00
1 05/20/2023 02:02
WG2061246
Benzo(k)fluoranthene
U
0.120
1.00
1 05/20/2023 02:02
WG2061246
Benzo(g,h,i)perylene
U
0.121
1.00
1 05/20/2023 02:02
WG2061246
Benzo(a)pyrene
U
0.0381
1.00
1 05/20/2023 02:02
WG2061246
Bis(2-chlorethoxy)methane
U
0.116
10.0
1 05/20/2023 02:02
WG2061246
Bis(2-chloroethyl)ether
U
0.137
10.0
1 05/20/2023 02:02
WG2061246
2,2-Oxybis(1-Chloropropane)
U
0.210
10.0
1 05/20/2023 02:02
WG2061246
4-Bromophenyl-phenylether
U
0.0877
10.0
1 05/20/2023 02:02
WG2061246
2-Chloronaphthalene
U
0.0648
1.00
1 05/20/2023 02:02
WG2061246
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 65 of 132

TW-8 SAMPLE RESULTS - 19
Collected date/time: 05/12/23 11:45 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
4-Chlorophenyl-phenylether
U
0.0926
10.0
1 05/20/2023 02:02
WG2061246
Chrysene
U
0.130
1.00
1 05/20/2023 02:02
WG2061246
Dibenz(a,h)anthracene
U
0.0644
1.00
1 05/20/2023 02:02
WG2061246
3,3-Dichlorobenzidine
U
0.212
10.0
1 05/20/2023 02:02
WG2061246
2,4-Dinitrotoluene
U
0.0983
10.0
1 05/20/2023 02:02
WG2061246
2,6-Dinitrotoluene
U
0.250
10.0
1 05/20/2023 02:02
WG2061246
Fluoranthene
U
0.102
1.00
1 05/20/2023 02:02
WG2061246
Fluorene
U
0.0844
1.00
1 05/20/2023 02:02
WG2061246
Hexachlorobenzene
U
0.0755
1.00
1 05/20/2023 02:02
WG2061246
Hexachloro-1,3-butadiene
U
0.0968
10.0
1 05/20/2023 02:02
WG2061246
Hexachlorocyclopentadiene
U
0.0598
10.0
1 05/20/2023 02:02
WG2061246
Hexachloroethane
U
0.127
10.0
1 05/20/2023 02:02
WG2061246
Indeno(1,2,3-cd)pyrene
U
0.279
1.00
1 05/20/2023 02:02
WG2061246
Isophorone
U
0.143
10.0
1 05/20/2023 02:02
WG2061246
Naphthalene
U
0.159
1.00
1 05/20/2023 02:02
WG2061246
Nitrobenzene
U
0.297
10.0
1 05/20/2023 02:02
WG2061246
n-Nitrosodimethyla mine
U
0.998
10.0
1 05/20/2023 02:02
WG2061246
n-Nitrosodiphenyla mine
U
2.37
10.0
1 05/20/2023 02:02
WG2061246
n-Nitrosodi-n-propylamine
U
0.261
10.0
1 05/20/2023 02:02
WG2061246
Phenanthrene
U
0.112
1.00
1 05/20/2023 02:02
WG2061246
Benzylbutyl phthalate
U
0.765
3.00
1 05/20/2023 02:02
WG2061246
Bis(2-ethylhexyl)phthalate
U
0.895
3.00
1 05/20/2023 02:02
WG2061246
Di-n-butyl phthalate
U
0.453
3.00
1 05/20/2023 02:02
WG2061246
Diethyl phthalate
3.41
0.287
3.00
1 05/20/2023 02:02
WG2061246
Dimethyl phthalate
U
0.260
3.00
1 05/20/2023 02:02
WG2061246
Di-n-octyl phthalate
U
0.932
3.00
1 05/20/2023 02:02
WG2061246
Pyrene
U
0.107
1.00
1 05/20/2023 02:02
WG2061246
1,2,4-Trichlorobenzene
U
0.0698
10.0
1 05/20/2023 02:02
WG2061246
4-Chloro-3-methylphenol
U
0.131
10.0
1 05/20/2023 02:02
WG2061246
2-Chlorophenol
U
0.133
10.0
1 05/20/2023 02:02
WG2061246
2,4-Dichlorophenol
U
0.102
10.0
1 05/20/2023 02:02
WG2061246
2,4-Dimethylphenol
U
0.0636
10.0
1 05/20/2023 02:02
WG2061246
4,6-Dinitro-2-methylphenol
U
1.12
10.0
1 05/20/2023 02:02
WG2061246
2,4-Dinitrophenol
U
5.93
10.0
1 05/20/2023 02:02
WG2061246
2-Nitrophenol
U
0.117
10.0
1 05/20/2023 02:02
WG2061246
4-Nitrophenol
U
J4 0.143
10.0
1 05/20/2023 02:02
WG2061246
Pentachlorophenol
U
0.313
10.0
1 05/20/2023 02:02
WG2061246
Phenol
U
4.33
10.0
1 05/20/2023 02:02
WG2061246
2,4,6-Trichlorophenol
U
0.100
10.0
1 05/20/2023 02:02
WG2061246
(S) Nitrobenzene-d5
80.9
15.0-314
0512012023 02:02
WG2061246
(S) 2-Fluorobiphenyl
60.3
22.0-127
0512012023 02:02
WG2061246
(S) p-Terphenyl-d14
80.8
29.0-141
0512012023 02:02
WG2061246
(S) Phenol-d5
16.3
8.00-424
0512012023 02:02
WG2061246
(S) 2-F/uorophenol
27.6
10.0-120
0512012023 02:02
WG2061246
(S) 2,4,6- Tribromophenol
56.8
10.0-153
051201202302:02
WG2061246
FP1
FTc
FSS
4
Cn
RC
F
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 66 of 132

TW-9
Collected date/time: 05/12/23 14:00
Wet Chemistry by Method 7199
SAMPLE
RESULTS - 20
L1616119
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Hexavalent Chromium -Low U
0.0400
0.100
1 05/18/2023 06:31
WG2059859
Level
Mercury by Method 7470A
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Mercury U
0.100
0.200
1 06/05/2023 20:12
WG2060584
Metals (ICPMS) by Method 6020B
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Arsenic
0.441
J
0.180
2.00
1 05/23/2023 22:47
WG2060154
Barium
182
0.381
2.00
1 05/23/2023 22:47
WG2060154
Cadmium
U
0.150
1.00
1 05/23/2023 22:47
WG2060154
Chromium
U
1.24
2.00
1 05/23/2023 22:47
WG2060154
Lead
1.08
J
0.849
2.00
1 05/23/2023 22:47
WG2060154
Selenium
0.318
J
0.300
2.00
1 05/23/2023 22:47
WG2060154
Silver
U
0.0700
2.00
1 05/23/2023 22:47
WG2060154
Volatile Organic Compounds (GC/MS)
by Method 620OB-1997/620OB-2011
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
11.3
50.0
1 05/22/2023 04:08
WG2064057
Acrolein
U
2.54
50.0
1 05/22/2023 04:08
WG2064057
Acrylonitrile
U
0.671
10.0
1 05/22/2023 04:08
WG2064057
Benzene
U
0.0941
1.00
1 05/22/2023 04:08
WG2064057
Bromobenzene
U
0.118
1.00
1 05/22/2023 04:08
WG2064057
Bromochloromethane
U
0.128
1.00
1 05/22/2023 04:08
WG2064057
Bromodichloromethane
U
0.136
1.00
1 05/22/2023 04:08
WG2064057
Bromoform
U
0.129
1.00
1 05/22/2023 04:08
WG2064057
Bromomethane
U
0.605
5.00
1 05/22/2023 04:08
WG2064057
n-Butylbenzene
U
0.157
1.00
1 05/22/2023 04:08
WG2064057
sec -Butyl benzene
U
0.125
1.00
1 05/22/2023 04:08
WG2064057
tert-Butylbenzene
U
0.127
1.00
1 05/22/2023 04:08
WG2064057
Carbon tetrachloride
U
0.128
1.00
1 05/22/2023 04:08
WG2064057
Chlorobenzene
U
0.116
1.00
1 05/22/2023 04:08
WG2064057
Chlorodibromomethane
U
0.140
1.00
1 05/22/2023 04:08
WG2064057
Chloroethane
U
0.192
5.00
1 05/22/2023 04:08
WG2064057
Chloroform
U
0.111
5.00
1 05/22/2023 04:08
WG2064057
Chloromethane
U
0.960
2.50
1 05/22/2023 04:08
WG2064057
2-Chlorotoluene
U
0.106
1.00
1 05/22/2023 04:08
WG2064057
4-Chlorotoluene
U
0.114
1.00
1 05/22/2023 04:08
WG2064057
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1 05/22/2023 04:08
WG2064057
1,2-Dibromoethane
U
0.126
1.00
1 05/22/2023 04:08
WG2064057
Dibromomethane
U
0.122
1.00
1 05/22/2023 04:08
WG2064057
1,2-Dichlorobenzene
U
0.107
1.00
1 05/22/2023 04:08
WG2064057
1,3-Dichlorobenzene
U
0.110
1.00
1 05/22/2023 04:08
WG2064057
1,4-Dichlorobenzene
U
0.120
1.00
1 05/22/2023 04:08
WG2064057
Dichlorodifluoromethane
U
0.374
5.00
1 05/22/2023 04:08
WG2064057
1,1-Dichloroethane
U
0.100
1.00
1 05/22/2023 04:08
WG2064057
1,2-Dichloroethane
U
0.0819
1.00
1 05/22/2023 04:08
WG2064057
1,1-Dichloroethene
U
0.188
1.00
1 05/22/2023 04:08
WG2064057
cis-1,2-Dichloroethene
U
0.126
1.00
1 05/22/2023 04:08
WG2064057
trans-1,2-Dichloroethene
U
0.149
1.00
1 05/22/2023 04:08
WG2064057
1,2-Dichloropropane
U
0.149
1.00
1 05/22/2023 04:08
WG2064057
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
Fp]
FTC
FSS
4
Cn
RC
F ql
FAI
FSC
67 of 132

TW-9 SAMPLE RESULTS - 20
Collected date/time: 05/12/23 14:00 L1616119
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
1,1-Dichloropropene
U
0.142
1.00
1 05/22/2023 04:08
WG2064057
1,3-Dichloropropane
U
0.110
1.00
1 05/22/2023 04:08
WG2064057
cis-1,3-Dichloropropene
U
0.111
1.00
1 05/22/2023 04:08
WG2064057
trans-1,3-Dichloropropene
U
0.118
1.00
1 05/22/2023 04:08
WG2064057
2,2-Dichloropropane
U
0.161
1.00
1 05/22/2023 04:08
WG2064057
Di -isopropyl ether
U
0.105
1.00
1 05/22/2023 04:08
WG2064057
Ethylbenzene
U
0.137
1.00
1 05/22/2023 04:08
WG2064057
Hexachloro-1,3-butadiene
U
0.337
1.00
1 05/22/2023 04:08
WG2064057
2-Hexanone
U
0.787
10.0
1 05/22/2023 04:08
WG2064057
Isopropylbenzene
U
0.105
1.00
1 05/22/2023 04:08
WG2064057
p-Isopropyltoluene
U
0.120
1.00
1 05/22/2023 04:08
WG2064057
2-Butanone (MEK)
U
1.19
10.0
1 05/22/2023 04:08
WG2064057
Methylene Chloride
U
0.430
5.00
1 05/22/2023 04:08
WG2064057
4-Methyl-2-pentanone (MIBK)
U
0.478
10.0
1 05/22/2023 04:08
WG2064057
Methyl tert-butyl ether
U
0.101
1.00
1 05/22/2023 04:08
WG2064057
Naphthalene
U
1.00
5.00
1 05/22/2023 04:08
WG2064057
n-Propylbenzene
U
0.0993
1.00
1 05/22/2023 04:08
WG2064057
Styrene
U
0.118
1.00
1 05/22/2023 04:08
WG2064057
1,1,1,2-Tetrachloroethane
U
0.147
1.00
1 05/22/2023 04:08
WG2064057
1,1,2,2-Tetrachloroethane
U
0.133
1.00
1 05/22/2023 04:08
WG2064057
Tetrachloroethene
U
0.300
1.00
1 05/22/2023 04:08
WG2064057
Toluene
U
0.278
1.00
1 05/22/2023 04:08
WG2064057
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/22/2023 04:08
WG2064057
1,2,4-Trichlorobenzene
U
0.481
1.00
1 05/22/2023 04:08
WG2064057
1,1,1-Trichloroethane
U
0.149
1.00
1 05/22/2023 04:08
WG2064057
1,1,2-Trichloroethane
U
0.158
1.00
1 05/22/2023 04:08
WG2064057
Trichloroethene
U
0.190
1.00
1 05/22/2023 04:08
WG2064057
Trichlorofluoromethane
U
0.160
5.00
1 05/22/2023 04:08
WG2064057
1,2,3-Trichloropropane
U
0.237
2.50
1 05/22/2023 04:08
WG2064057
1,2,4-Trimethylbenzene
U
0.322
1.00
1 05/22/2023 04:08
WG2064057
1,3,5-Trimethyl benzene
U
0.104
1.00
1 05/22/2023 04:08
WG2064057
Vinyl acetate
U
0.692
10.0
1 05/22/2023 04:08
WG2064057
Vinyl chloride
U
0.234
1.00
1 05/22/2023 04:08
WG2064057
o-Xylene
U
J4 0.174
1.00
1 05/22/2023 04:08
WG2064057
m&p-Xylenes
U
0.430
2.00
1 05/22/2023 04:08
WG2064057
(S) Toluene-d8
103
80.0-120
0512212023 04:08
WG2064057
(S) 4-Bromof/uorobenzene
97.1
77.0-126
0512212023 04:08
WG2064057
(S)1,2-Dich/oroethone-d4
94.6
70.0-130
0512212023 04:08
WG2064057
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/I ug/I ug/I date / time
Acenaphthene
U
0.0886
1.00
1 05/20/2023 02:23
WG2061246
Acenaphthylene
U
0.0921
1.00
1 05/20/2023 02:23
WG2061246
Anthracene
U
0.0804
1.00
1 05/20/2023 02:23
WG2061246
Benzidine
U
3.74
10.0
1 05/20/2023 02:23
WG2061246
Benzo(a)anth race ne
U
0.199
1.00
1 05/20/2023 02:23
WG2061246
Benzo(b)fluoranthene
U
0.130
1.00
1 05/20/2023 02:23
WG2061246
Benzo(k)fluoranthene
U
0.120
1.00
1 05/20/2023 02:23
WG2061246
Benzo(g,h,i)perylene
U
0.121
1.00
1 05/20/2023 02:23
WG2061246
Benzo(a)pyrene
U
0.0381
1.00
1 05/20/2023 02:23
WG2061246
Bis(2-chlorethoxy)methane
U
0.116
10.0
1 05/20/2023 02:23
WG2061246
Bis(2-chloroethyl)ether
U
0.137
10.0
1 05/20/2023 02:23
WG2061246
2,2-Oxybis(1-Chloropropane)
U
0.210
10.0
1 05/20/2023 02:23
WG2061246
4-Bromophenyl-phenylether
U
0.0877
10.0
1 05/20/2023 02:23
WG2061246
2-Chloronaphthalene
U
0.0648
1.00
1 05/20/2023 02:23
WG2061246
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 68 of 132

TW-9 SAMPLE RESULTS - 20
Collected date/time: 05/12/23 14:00 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
4-Chlorophenyl-phenylether
U
0.0926
10.0
1 05/20/2023 02:23
WG2061246
Chrysene
U
0.130
1.00
1 05/20/2023 02:23
WG2061246
Dibenz(a,h)anthracene
U
0.0644
1.00
1 05/20/2023 02:23
WG2061246
3,3-Dichlorobenzidine
U
0.212
10.0
1 05/20/2023 02:23
WG2061246
2,4-Dinitrotoluene
U
0.0983
10.0
1 05/20/2023 02:23
WG2061246
2,6-Dinitrotoluene
U
0.250
10.0
1 05/20/2023 02:23
WG2061246
Fluoranthene
U
0.102
1.00
1 05/20/2023 02:23
WG2061246
Fluorene
U
0.0844
1.00
1 05/20/2023 02:23
WG2061246
Hexachlorobenzene
U
0.0755
1.00
1 05/20/2023 02:23
WG2061246
Hexachloro-1,3-butadiene
U
0.0968
10.0
1 05/20/2023 02:23
WG2061246
Hexachlorocyclopentadiene
U
0.0598
10.0
1 05/20/2023 02:23
WG2061246
Hexachloroethane
U
0.127
10.0
1 05/20/2023 02:23
WG2061246
Indeno(1,2,3-cd)pyrene
U
0.279
1.00
1 05/20/2023 02:23
WG2061246
Isophorone
U
0.143
10.0
1 05/20/2023 02:23
WG2061246
Naphthalene
U
0.159
1.00
1 05/20/2023 02:23
WG2061246
Nitrobenzene
U
0.297
10.0
1 05/20/2023 02:23
WG2061246
n-Nitrosodimethyla mine
U
0.998
10.0
1 05/20/2023 02:23
WG2061246
n-Nitrosodiphenyla mine
U
2.37
10.0
1 05/20/2023 02:23
WG2061246
n-Nitrosodi-n-propylamine
U
0.261
10.0
1 05/20/2023 02:23
WG2061246
Phenanthrene
U
0.112
1.00
1 05/20/2023 02:23
WG2061246
Benzylbutyl phthalate
U
0.765
3.00
1 05/20/2023 02:23
WG2061246
Bis(2-ethylhexyl)phthalate
U
0.895
3.00
1 05/20/2023 02:23
WG2061246
Di-n-butyl phthalate
1.10
J
0.453
3.00
1 05/20/2023 02:23
WG2061246
Diethyl phthalate
0.966
J_
0.287
3.00
1 05/20/2023 02:23
WG2061246
Dimethyl phthalate
U
0.260
3.00
1 05/20/2023 02:23
WG2061246
Di-n-octyl phthalate
U
0.932
3.00
1 05/20/2023 02:23
WG2061246
Pyrene
U
0.107
1.00
1 05/20/2023 02:23
WG2061246
1,2,4-Trichlorobenzene
U
0.0698
10.0
1 05/20/2023 02:23
WG2061246
4-Chloro-3-methylphenol
U
0.131
10.0
1 05/20/2023 02:23
WG2061246
2-Chlorophenol
U
0.133
10.0
1 05/20/2023 02:23
WG2061246
2,4-Dichlorophenol
U
0.102
10.0
1 05/20/2023 02:23
WG2061246
2,4-Dimethylphenol
U
0.0636
10.0
1 05/20/2023 02:23
WG2061246
4,6-Dinitro-2-methylphenol
U
1.12
10.0
1 05/20/2023 02:23
WG2061246
2,4-Dinitrophenol
U
5.93
10.0
1 05/20/2023 02:23
WG2061246
2-Nitrophenol
U
0.117
10.0
1 05/20/2023 02:23
WG2061246
4-Nitrophenol
U
J4
0.143
10.0
1 05/20/2023 02:23
WG2061246
Pentachlorophenol
U
0.313
10.0
1 05/20/2023 02:23
WG2061246
Phenol
U
4.33
10.0
1 05/20/2023 02:23
WG2061246
2,4,6-Trichlorophenol
U
0.100
10.0
1 05/20/2023 02:23
WG2061246
(S) Nitrobenzene-d5
91.4
15.0-314
0512012023 02:23
WG2061246
(S) 2-Fluorobiphenyl
75.6
22.0-127
0512012023 02:23
WG2061246
(S) p-Terphenyl-d14
83.8
29.0-141
0512012023 02:23
WG2061246
(S) Phenol-d5
21.9
8.00-424
0512012023 02:23
WG2061246
(S) 2-F/uorophenol
31.9
10.0-120
0512012023 02:23
WG2061246
(S) 2,4,6- Tribromophenol
78.6
10.0-153
0512012023 02:23
WG2061246
FP1
FTc
FSS
4
Cn
RC
F
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 69 of 132

-------------
TW-10
Collected date/time: 05/12/23 15:15
Wet Chemistry by Method 7199
SAMPLE
RESULTS - 21
L1616119
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Hexavalent Chromium -Low U
0.0400
0.100
1 05/18/2023 06:47
WG2059859
Level
Mercury by Method 7470A
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Mercury U
0.100
0.200
1 06/05/2023 20:14
WG2060584
Metals (ICPMS) by Method 6020B
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Arsenic
0.187
J
0.180
2.00
1 05/23/2023 22:51
WG2060154
Barium
107
0.381
2.00
1 05/23/2023 22:51
WG2060154
Cadmium
0.360
J
0.150
1.00
1 05/23/2023 22:51
WG2060154
Chromium
U
1.24
2.00
1 05/23/2023 22:51
WG2060154
Lead
1.97
J
0.849
2.00
1 05/23/2023 22:51
WG2060154
Selenium
U
0.300
2.00
1 05/23/2023 22:51
WG2060154
Silver
U
0.0700
2.00
1 05/23/2023 22:51
WG2060154
Volatile Organic Compounds (GC/MS)
by Method 620OB-1997/620OB-2011
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
11.3
50.0
1 05/22/2023 04:27
WG2064057
Acrolein
U
2.54
50.0
1 05/22/2023 04:27
WG2064057
Acrylonitrile
U
0.671
10.0
1 05/22/2023 04:27
WG2064057
Benzene
U
0.0941
1.00
1 05/22/2023 04:27
WG2064057
Bromobenzene
U
0.118
1.00
1 05/22/2023 04:27
WG2064057
Bromochloromethane
U
0.128
1.00
1 05/22/2023 04:27
WG2064057
Bromodichloromethane
U
0.136
1.00
1 05/22/2023 04:27
WG2064057
Bromoform
U
0.129
1.00
1 05/22/2023 04:27
WG2064057
Bromomethane
U
0.605
5.00
1 05/22/2023 04:27
WG2064057
n-Butylbenzene
U
0.157
1.00
1 05/22/2023 04:27
WG2064057
sec -Butyl benzene
U
0.125
1.00
1 05/22/2023 04:27
WG2064057
tert-Butylbenzene
U
0.127
1.00
1 05/22/2023 04:27
WG2064057
Carbon tetrachloride
U
0.128
1.00
1 05/22/2023 04:27
WG2064057
Chlorobenzene
U
0.116
1.00
1 05/22/2023 04:27
WG2064057
Chlorodibromomethane
U
0.140
1.00
1 05/22/2023 04:27
WG2064057
Chloroethane
U
0.192
5.00
1 05/22/2023 04:27
WG2064057
Chloroform
U
0.111
5.00
1 05/22/2023 04:27
WG2064057
Chloromethane
U
0.960
2.50
1 05/22/2023 04:27
WG2064057
2-Chlorotoluene
U
0.106
1.00
1 05/22/2023 04:27
WG2064057
4-Chlorotoluene
U
0.114
1.00
1 05/22/2023 04:27
WG2064057
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1 05/22/2023 04:27
WG2064057
1,2-Dibromoethane
U
0.126
1.00
1 05/22/2023 04:27
WG2064057
Dibromomethane
U
0.122
1.00
1 05/22/2023 04:27
WG2064057
1,2-Dichlorobenzene
U
0.107
1.00
1 05/22/2023 04:27
WG2064057
1,3-Dichlorobenzene
U
0.110
1.00
1 05/22/2023 04:27
WG2064057
1,4-Dichlorobenzene
U
0.120
1.00
1 05/22/2023 04:27
WG2064057
Dichlorodifluoromethane
U
0.374
5.00
1 05/22/2023 04:27
WG2064057
1,1-Dichloroethane
U
0.100
1.00
1 05/22/2023 04:27
WG2064057
1,2-Dichloroethane
U
0.0819
1.00
1 05/22/2023 04:27
WG2064057
1,1-Dichloroethene
U
0.188
1.00
1 05/22/2023 04:27
WG2064057
cis-1,2-Dichloroethene
U
0.126
1.00
1 05/22/2023 04:27
WG2064057
trans-1,2-Dichloroethene
U
0.149
1.00
1 05/22/2023 04:27
WG2064057
1,2-Dichloropropane
U
0.149
1.00
1 05/22/2023 04:27
WG2064057
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
Fp]
FTC
FSS
4
Cn
RC
F ql
FAI
FSC
PAGE:
70 of 132

TW-10 SAMPLE RESULTS - 21
Collected date/time: 05/12/23 15:15 L1616119
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
1,1-Dichloropropene
U
0.142
1.00
1 05/22/2023 04:27
WG2064057
1,3-Dichloropropane
U
0.110
1.00
1 05/22/2023 04:27
WG2064057
cis-1,3-Dichloropropene
U
0.111
1.00
1 05/22/2023 04:27
WG2064057
trans-1,3-Dichloropropene
U
0.118
1.00
1 05/22/2023 04:27
WG2064057
2,2-Dichloropropane
U
0.161
1.00
1 05/22/2023 04:27
WG2064057
Di -isopropyl ether
U
0.105
1.00
1 05/22/2023 04:27
WG2064057
Ethylbenzene
U
0.137
1.00
1 05/22/2023 04:27
WG2064057
Hexachloro-1,3-butadiene
U
0.337
1.00
1 05/22/2023 04:27
WG2064057
2-Hexanone
U
0.787
10.0
1 05/22/2023 04:27
WG2064057
Isopropylbenzene
U
0.105
1.00
1 05/22/2023 04:27
WG2064057
p-Isopropyltoluene
U
0.120
1.00
1 05/22/2023 04:27
WG2064057
2-Butanone (MEK)
U
1.19
10.0
1 05/22/2023 04:27
WG2064057
Methylene Chloride
U
0.430
5.00
1 05/22/2023 04:27
WG2064057
4-Methyl-2-pentanone (MIBK)
U
0.478
10.0
1 05/22/2023 04:27
WG2064057
Methyl tert-butyl ether
0.133
J_ 0.101
1.00
1 05/22/2023 04:27
WG2064057
Naphthalene
U
1.00
5.00
1 05/22/2023 04:27
WG2064057
n-Propylbenzene
U
0.0993
1.00
1 05/22/2023 04:27
WG2064057
Styrene
U
0.118
1.00
1 05/22/2023 04:27
WG2064057
1,1,1,2-Tetrachloroethane
U
0.147
1.00
1 05/22/2023 04:27
WG2064057
1,1,2,2-Tetrachloroethane
U
0.133
1.00
1 05/22/2023 04:27
WG2064057
Tetrachloroethene
U
0.300
1.00
1 05/22/2023 04:27
WG2064057
Toluene
U
0.278
1.00
1 05/22/2023 04:27
WG2064057
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/22/2023 04:27
WG2064057
1,2,4-Trichlorobenzene
U
0.481
1.00
1 05/22/2023 04:27
WG2064057
1,1,1-Trichloroethane
U
0.149
1.00
1 05/22/2023 04:27
WG2064057
1,1,2-Trichloroethane
U
0.158
1.00
1 05/22/2023 04:27
WG2064057
Trichloroethene
U
0.190
1.00
1 05/22/2023 04:27
WG2064057
Trichlorofluoromethane
U
0.160
5.00
1 05/22/2023 04:27
WG2064057
1,2,3-Trichloropropane
U
0.237
2.50
1 05/22/2023 04:27
WG2064057
1,2,4-Trimethylbenzene
U
0.322
1.00
1 05/22/2023 04:27
WG2064057
1,3,5-Trimethyl benzene
U
0.104
1.00
1 05/22/2023 04:27
WG2064057
Vinyl acetate
U
0.692
10.0
1 05/22/2023 04:27
WG2064057
Vinyl chloride
U
0.234
1.00
1 05/22/2023 04:27
WG2064057
o-Xylene
U
J4 0.174
1.00
1 05/22/2023 04:27
WG2064057
m&p-Xylenes
U
0.430
2.00
1 05/22/2023 04:27
WG2064057
(S) Toluene-d8
105
80.0-120
0512212023 04:27
WG2064057
(S) 4-Bromof/uorobenzene
95.3
77.0-126
0512212023 04:27
WG2064057
(S)1,2-Dich/oroethone-d4
90.3
70.0-130
0512212023 04:27
WG2064057
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/I ug/I ug/I date / time
Acenaphthene
U
0.0886
1.00
1 05/20/2023 02:44
WG2061246
Acenaphthylene
U
0.0921
1.00
1 05/20/2023 02:44
WG2061246
Anthracene
U
0.0804
1.00
1 05/20/2023 02:44
WG2061246
Benzidine
U
3.74
10.0
1 05/20/2023 02:44
WG2061246
Benzo(a)anth race ne
U
0.199
1.00
1 05/20/2023 02:44
WG2061246
Benzo(b)fluoranthene
U
0.130
1.00
1 05/20/2023 02:44
WG2061246
Benzo(k)fluoranthene
U
0.120
1.00
1 05/20/2023 02:44
WG2061246
Benzo(g,h,i)perylene
U
0.121
1.00
1 05/20/2023 02:44
WG2061246
Benzo(a)pyrene
U
0.0381
1.00
1 05/20/2023 02:44
WG2061246
Bis(2-chlorethoxy)methane
U
0.116
10.0
1 05/20/2023 02:44
WG2061246
Bis(2-chloroethyl)ether
U
0.137
10.0
1 05/20/2023 02:44
WG2061246
2,2-Oxybis(1-Chloropropane)
U
0.210
10.0
1 05/20/2023 02:44
WG2061246
4-Bromophenyl-phenylether
U
0.0877
10.0
1 05/20/2023 02:44
WG2061246
2-Chloronaphthalene
U
0.0648
1.00
1 05/20/2023 02:44
WG2061246
FP1
FTc
FSS
4
Cn
RC
7G1
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 71 of 132

TW-10
Collected date/time: 05/12/23 15:15
Semi Volatile Organic Compounds
SAMPLE RESULTS - 21
L1616119
(GC/MS) by Method 625.1
Result Qualifier MDL
RDL
Dilution Analysis
Batch
FP1
Analyte
ug/I
ug/I
ug/I
date / time
4-Chlorophenyl-phenylether
U
0.0926
10.0
1 05/20/2023 02:44
WG2061246
z
Tc
Chrysene
U
0.130
1.00
1 05/20/2023 02:44
WG2061246
Dibenz(a,h)anthracene
U
0.0644
1.00
1 05/20/2023 02:44
WG2061246
3,3-Dichlorobenzidine
U
0.212
10.0
1 05/20/2023 02:44
WG2061246
FSS
2,4-Dinitrotoluene
U
0.0983
10.0
1 05/20/2023 02:44
WG2061246
2,6-Dinitrotoluene
U
0.250
10.0
1 05/20/2023 02:44
WG2061246
4
Cn
Fluoranthene
U
0.102
1.00
1 05/20/2023 02:44
WG2061246
Fluorene
U
0.0844
1.00
1 05/20/2023 02:44
WG2061246
Hexachlorobenzene
U
0.0755
1.00
1 05/20/2023 02:44
WG2061246
Hexachloro-1,3-butadiene
U
0.0968
10.0
1 05/20/2023 02:44
WG2061246
Hexachlorocyclopentadiene
U
0.0598
10.0
1 05/20/2023 02:44
WG2061246
RC
Hexachloroethane
U
0.127
10.0
1 05/20/2023 02:44
WG2061246
Indeno(1,2,3-cd)pyrene
U
0.279
1.00
1 05/20/2023 02:44
WG2061246
Isophorone
U
0.143
10.0
1 05/20/2023 02:44
WG2061246
GI
Naphthalene
U
0.159
1.00
1 05/20/2023 02:44
WG2061246
Nitrobenzene
U
0.297
10.0
1 05/20/2023 02:44
WG2061246
FAI
n-Nitrosodimethyla mine
U
0.998
10.0
1 05/20/2023 02:44
WG2061246
n-Nitrosodiphenyla mine
U
2.37
10.0
1 05/20/2023 02:44
WG2061246
n-Nitrosodi-n-propylamine
U
0.261
10.0
1 05/20/2023 02:44
WG2061246
F
Phenanthrene
U
0.112
1.00
1 05/20/2023 02:44
WG2061246
Benzylbutyl phthalate
U
0.765
3.00
1 05/20/2023 02:44
WG2061246
Bis(2-ethylhexyl)phthalate
U
0.895
3.00
1 05/20/2023 02:44
WG2061246
Di-n-butyl phthalate
U
0.453
3.00
1 05/20/2023 02:44
WG2061246
Diethyl phthalate
2.13 J_
0.287
3.00
1 05/20/2023 02:44
WG2061246
Dimethyl phthalate
U
0.260
3.00
1 05/20/2023 02:44
WG2061246
Di-n-octyl phthalate
U
0.932
3.00
1 05/20/2023 02:44
WG2061246
Pyrene
U
0.107
1.00
1 05/20/2023 02:44
WG2061246
1,2,4-Trichlorobenzene
U
0.0698
10.0
1 05/20/2023 02:44
WG2061246
4-Chloro-3-methylphenol
U
0.131
10.0
1 05/20/2023 02:44
WG2061246
2-Chlorophenol
U
0.133
10.0
1 05/20/2023 02:44
WG2061246
2,4-Dichlorophenol
U
0.102
10.0
1 05/20/2023 02:44
WG2061246
2,4-Dimethylphenol
U
0.0636
10.0
1 05/20/2023 02:44
WG2061246
4,6-Dinitro-2-methylphenol
U
1.12
10.0
1 05/20/2023 02:44
WG2061246
2,4-Dinitrophenol
U
5.93
10.0
1 05/20/2023 02:44
WG2061246
2-Nitrophenol
U
0.117
10.0
1 05/20/2023 02:44
WG2061246
4-Nitrophenol
U J4
0.143
10.0
1 05/20/2023 02:44
WG2061246
Pentachlorophenol
U
0.313
10.0
1 05/20/2023 02:44
WG2061246
Phenol
U
4.33
10.0
1 05/20/2023 02:44
WG2061246
2,4,6-Trichlorophenol
U
0.100
10.0
1 05/20/2023 02:44
WG2061246
(S) Nitrobenzene-d5
82.3
15.0-314
0512012023 02.44
WG2061246
(S) 2-Fluorobiphenyl
67.0
22.0-127
0512012023 02:44
WG2061246
(S) p-Terphenyl-d14
80.4
29.0-141
0512012023 02.44
WG2061246
(S) Phenol-d5
175
8.00-424
0512012023 02:44
WG2061246
(S) 2-F/uorophenol
30.5
10.0-120
0512012023 02.44
WG2061246
(S) 2,4,6- Tribromophenol
63.2
10.0-153
051201202302:44
WG2061246
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Withers & Ravenel
Eng. - Standard
23-0302
L1616119
06/06/23 12:28
72 of 132

DUP
Collected date/time: 05/11/23 12:00
Wet Chemistry by Method 7199
SAMPLE
RESULTS - 22
L1616119
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Hexavalent Chromium -Low U
0.0400
0.100
1 05/22/2023 02:20
WG2061989
Level
Mercury by Method 7470A
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
ug/I
date / time
Mercury U
0.100
0.200
1 06/05/2023 20:17
WG2060584
Metals (ICPMS) by Method 6020B
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Arsenic
U
0.180
2.00
1 05/23/2023 22:54
WG2060154
Barium
18.5
0.381
2.00
1 05/23/2023 22:54
WG2060154
Cadmium
U
0.150
1.00
1 05/23/2023 22:54
WG2060154
Chromium
U
1.24
2.00
1 05/23/2023 22:54
WG2060154
Lead
U
0.849
2.00
1 05/23/2023 22:54
WG2060154
Selenium
0.349 J
0.300
2.00
1 05/23/2023 22:54
WG2060154
Silver
U
0.0700
2.00
1 05/23/2023 22:54
WG2060154
Volatile Organic Compounds (GC/MS)
by Method 620OB-1997/620OB-2011
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
11.3
50.0
1 05/22/2023 04:46
WG2064057
Acrolein
U
2.54
50.0
1 05/22/2023 04:46
WG2064057
Acrylonitrile
U
0.671
10.0
1 05/22/2023 04:46
WG2064057
Benzene
U
0.0941
1.00
1 05/22/2023 04:46
WG2064057
Bromobenzene
U
0.118
1.00
1 05/22/2023 04:46
WG2064057
Bromochloromethane
U
0.128
1.00
1 05/22/2023 04:46
WG2064057
Bromodichloromethane
U
0.136
1.00
1 05/22/2023 04:46
WG2064057
Bromoform
U
0.129
1.00
1 05/22/2023 04:46
WG2064057
Bromomethane
U
0.605
5.00
1 05/22/2023 04:46
WG2064057
n-Butylbenzene
7.73
0.157
1.00
1 05/22/2023 04:46
WG2064057
sec -Butyl benzene
1.16
0.125
1.00
1 05/22/2023 04:46
WG2064057
tert-Butylbenzene
U
0.127
1.00
1 05/22/2023 04:46
WG2064057
Carbon tetrachloride
U
0.128
1.00
1 05/22/2023 04:46
WG2064057
Chlorobenzene
U
0.116
1.00
1 05/22/2023 04:46
WG2064057
Chlorodibromomethane
U
0.140
1.00
1 05/22/2023 04:46
WG2064057
Chloroethane
U
0.192
5.00
1 05/22/2023 04:46
WG2064057
Chloroform
U
0.111
5.00
1 05/22/2023 04:46
WG2064057
Chloromethane
U
0.960
2.50
1 05/22/2023 04:46
WG2064057
2-Chlorotoluene
U
0.106
1.00
1 05/22/2023 04:46
WG2064057
4-Chlorotoluene
U
0.114
1.00
1 05/22/2023 04:46
WG2064057
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1 05/22/2023 04:46
WG2064057
1,2-Dibromoethane
U
0.126
1.00
1 05/22/2023 04:46
WG2064057
Dibromomethane
U
0.122
1.00
1 05/22/2023 04:46
WG2064057
1,2-Dichlorobenzene
U
0.107
1.00
1 05/22/2023 04:46
WG2064057
1,3-Dichlorobenzene
U
0.110
1.00
1 05/22/2023 04:46
WG2064057
1,4-Dichlorobenzene
U
0.120
1.00
1 05/22/2023 04:46
WG2064057
Dichlorodifluoromethane
U
0.374
5.00
1 05/22/2023 04:46
WG2064057
1,1-Dichloroethane
U
0.100
1.00
1 05/22/2023 04:46
WG2064057
1,2-Dichloroethane
U
0.0819
1.00
1 05/22/2023 04:46
WG2064057
1,1-Dichloroethene
U
0.188
1.00
1 05/22/2023 04:46
WG2064057
cis-1,2-Dichloroethene
U
0.126
1.00
1 05/22/2023 04:46
WG2064057
trans-1,2-Dichloroethene
U
0.149
1.00
1 05/22/2023 04:46
WG2064057
1,2-Dichloropropane
U
0.149
1.00
1 05/22/2023 04:46
WG2064057
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
Fp]
FTC
FSS
4
Cn
RC
F ql
FAI
FSC
PAGE:
73 of 132

DUP SAMPLE RESULTS - 22
Collected date/time: 05/11/23 12:00 L1616119
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
1,1-Dichloropropene
U
0.142
1.00
1 05/22/2023 04:46
WG2064057
1,3-Dichloropropane
U
0.110
1.00
1 05/22/2023 04:46
WG2064057
cis-1,3-Dichloropropene
U
0.111
1.00
1 05/22/2023 04:46
WG2064057
trans-1,3-Dichloropropene
U
0.118
1.00
1 05/22/2023 04:46
WG2064057
2,2-Dichloropropane
U
0.161
1.00
1 05/22/2023 04:46
WG2064057
Di -isopropyl ether
U
0.105
1.00
1 05/22/2023 04:46
WG2064057
Ethylbenzene
U
0.137
1.00
1 05/22/2023 04:46
WG2064057
Hexachloro-1,3-butadiene
U
0.337
1.00
1 05/22/2023 04:46
WG2064057
2-Hexanone
0.942
1_
0.787
10.0
1 05/22/2023 04:46
WG2064057
Isopropylbenzene
U
0.105
1.00
1 05/22/2023 04:46
WG2064057
p-Isopropyltoluene
2.48
0.120
1.00
1 05/22/2023 04:46
WG2064057
2-Butanone (MEK)
U
1.19
10.0
1 05/22/2023 04:46
WG2064057
Methylene Chloride
U
0.430
5.00
1 05/22/2023 04:46
WG2064057
4-Methyl-2-pentanone (MIBK)
U
0.478
10.0
1 05/22/2023 04:46
WG2064057
Methyl tert-butyl ether
U
0.101
1.00
1 05/22/2023 04:46
WG2064057
Naphthalene
U
1.00
5.00
1 05/22/2023 04:46
WG2064057
n-Propylbenzene
U
0.0993
1.00
1 05/22/2023 04:46
WG2064057
Styrene
U
0.118
1.00
1 05/22/2023 04:46
WG2064057
1,1,1,2-Tetrachloroethane
U
0.147
1.00
1 05/22/2023 04:46
WG2064057
1,1,2,2-Tetrachloroethane
U
0.133
1.00
1 05/22/2023 04:46
WG2064057
Tetrachloroethene
U
0.300
1.00
1 05/22/2023 04:46
WG2064057
Toluene
U
0.278
1.00
1 05/22/2023 04:46
WG2064057
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/22/2023 04:46
WG2064057
1,2,4-Trichlorobenzene
U
0.481
1.00
1 05/22/2023 04:46
WG2064057
1,1,1-Trichloroethane
U
0.149
1.00
1 05/22/2023 04:46
WG2064057
1,1,2-Trichloroethane
U
0.158
1.00
1 05/22/2023 04:46
WG2064057
Trichloroethene
U
0.190
1.00
1 05/22/2023 04:46
WG2064057
Trichlorofluoromethane
U
0.160
5.00
1 05/22/2023 04:46
WG2064057
1,2,3-Trichloropropane
U
0.237
2.50
1 05/22/2023 04:46
WG2064057
1,2,4-Trimethylbenzene
0.761
J
0.322
1.00
1 05/22/2023 04:46
WG2064057
1,3,5-Trimethyl benzene
0.820
J_
0.104
1.00
1 05/22/2023 04:46
WG2064057
Vinyl acetate
U
0.692
10.0
1 05/22/2023 04:46
WG2064057
Vinyl chloride
U
0.234
1.00
1 05/22/2023 04:46
WG2064057
o-Xylene
4.97
J4
0.174
1.00
1 05/22/2023 04:46
WG2064057
m&p-Xylenes
U
0.430
2.00
1 05/22/2023 04:46
WG2064057
(S) Toluene-d8
106
80.0-120
0512212023 04.46
WG2064057
(S) 4-Bromof/uorobenzene
97.2
77.0-126
0512212023 04.46
WG2064057
(S)1,2-Dich/oroethone-d4
92.8
70.0-130
0512212023 04.46
WG2064057
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/I ug/I ug/I date / time
Acenaphthene
U
0.0886
1.00
1 05/20/2023 03:06
WG2061246
Acenaphthylene
U
0.0921
1.00
1 05/20/2023 03:06
WG2061246
Anthracene
U
0.0804
1.00
1 05/20/2023 03:06
WG2061246
Benzidine
U
3.74
10.0
1 05/20/2023 03:06
WG2061246
Benzo(a)anth race ne
U
0.199
1.00
1 05/20/2023 03:06
WG2061246
Benzo(b)fluoranthene
U
0.130
1.00
1 05/20/2023 03:06
WG2061246
Benzo(k)fluoranthene
U
0.120
1.00
1 05/20/2023 03:06
WG2061246
Benzo(g,h,i)perylene
U
0.121
1.00
1 05/20/2023 03:06
WG2061246
Benzo(a)pyrene
U
0.0381
1.00
1 05/20/2023 03:06
WG2061246
Bis(2-chlorethoxy)methane
U
0.116
10.0
1 05/20/2023 03:06
WG2061246
Bis(2-chloroethyl)ether
U
0.137
10.0
1 05/20/2023 03:06
WG2061246
2,2-Oxybis(1-Chloropropane)
U
0.210
10.0
1 05/20/2023 03:06
WG2061246
4-Bromophenyl-phenylether
U
0.0877
10.0
1 05/20/2023 03:06
WG2061246
2-Chloronaphthalene
U
0.0648
1.00
1 05/20/2023 03:06
WG2061246
FP1
FTc
FSS
4
Cn
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 74 of 132

DUP SAMPLE RESULTS - 22
Collected date/time: 05/11/23 12:00 L1616119
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
4-Chlorophenyl-phenylether
U
0.0926
10.0
1 05/20/2023 03:06
WG2061246
Chrysene
U
0.130
1.00
1 05/20/2023 03:06
WG2061246
Dibenz(a,h)anthracene
U
0.0644
1.00
1 05/20/2023 03:06
WG2061246
3,3-Dichlorobenzidine
U
0.212
10.0
1 05/20/2023 03:06
WG2061246
2,4-Dinitrotoluene
U
0.0983
10.0
1 05/20/2023 03:06
WG2061246
2,6-Dinitrotoluene
U
0.250
10.0
1 05/20/2023 03:06
WG2061246
Fluoranthene
U
0.102
1.00
1 05/20/2023 03:06
WG2061246
Fluorene
U
0.0844
1.00
1 05/20/2023 03:06
WG2061246
Hexachlorobenzene
U
0.0755
1.00
1 05/20/2023 03:06
WG2061246
Hexachloro-1,3-butadiene
U
0.0968
10.0
1 05/20/2023 03:06
WG2061246
Hexachlorocyclopentadiene
U
0.0598
10.0
1 05/20/2023 03:06
WG2061246
Hexachloroethane
U
0.127
10.0
1 05/20/2023 03:06
WG2061246
Indeno(1,2,3-cd)pyrene
U
0.279
1.00
1 05/20/2023 03:06
WG2061246
Isophorone
U
0.143
10.0
1 05/20/2023 03:06
WG2061246
Naphthalene
U
0.159
1.00
1 05/20/2023 03:06
WG2061246
Nitrobenzene
U
0.297
10.0
1 05/20/2023 03:06
WG2061246
n-Nitrosodimethyla mine
U
0.998
10.0
1 05/20/2023 03:06
WG2061246
n-Nitrosodiphenyla mine
U
2.37
10.0
1 05/20/2023 03:06
WG2061246
n-Nitrosodi-n-propylamine
U
0.261
10.0
1 05/20/2023 03:06
WG2061246
Phenanthrene
U
0.112
1.00
1 05/20/2023 03:06
WG2061246
Benzylbutyl phthalate
U
0.765
3.00
1 05/20/2023 03:06
WG2061246
Bis(2-ethylhexyl)phthalate
U
0.895
3.00
1 05/20/2023 03:06
WG2061246
Di-n-butyl phthalate
0.963
J 0.453
3.00
1 05/20/2023 03:06
WG2061246
Diethyl phthalate
4.22
0.287
3.00
1 05/20/2023 03:06
WG2061246
Dimethyl phthalate
U
0.260
3.00
1 05/20/2023 03:06
WG2061246
Di-n-octyl phthalate
U
0.932
3.00
1 05/20/2023 03:06
WG2061246
Pyrene
U
0.107
1.00
1 05/20/2023 03:06
WG2061246
1,2,4-Trichlorobenzene
U
0.0698
10.0
1 05/20/2023 03:06
WG2061246
4-Chloro-3-methylphenol
U
0.131
10.0
1 05/20/2023 03:06
WG2061246
2-Chlorophenol
U
0.133
10.0
1 05/20/2023 03:06
WG2061246
2,4-Dichlorophenol
U
0.102
10.0
1 05/20/2023 03:06
WG2061246
2,4-Dimethylphenol
U
0.0636
10.0
1 05/20/2023 03:06
WG2061246
4,6-Dinitro-2-methylphenol
U
1.12
10.0
1 05/20/2023 03:06
WG2061246
2,4-Dinitrophenol
U
5.93
10.0
1 05/20/2023 03:06
WG2061246
2-Nitrophenol
U
0.117
10.0
1 05/20/2023 03:06
WG2061246
4-Nitrophenol
U
J4 0.143
10.0
1 05/20/2023 03:06
WG2061246
Pentachlorophenol
U
0.313
10.0
1 05/20/2023 03:06
WG2061246
Phenol
U
4.33
10.0
1 05/20/2023 03:06
WG2061246
2,4,6-Trichlorophenol
U
0.100
10.0
1 05/20/2023 03:06
WG2061246
(S) Nitrobenzene-d5
94.9
15.0-314
0512012023 03:06
WG2061246
(S) 2-Fluorobiphenyl
72.4
22.0-127
0512012023 03:06
WG2061246
(S) p-Terphenyl-d14
87.1
29.0-141
0512012023 03:06
WG2061246
(S) Phenol-d5
20.2
8.00-424
0512012023 03:06
WG2061246
(S) 2-F/uorophenol
31.3
10.0-120
0512012023 03:06
WG2061246
(S) 2,4,6- Tribromophenol
66.3
10.0-153
0512012023 03:06
WG2061246
FP1
FTc
FSS
4
Cn
RC
F
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 75 of 132

WG2060621
Total Solids by Method 2540 G-2011
Method Blank (MB)
(MB) R3925723-1 05/16/2316:32
MB Result
Analyte %
Total Solids 0.00100
MB Qualifier MB MDL MB RDL
L1616209-20 Original Sample (OS) • Duplicate (DUP)
(OS) L1616209-20 05/16/2316:32 • (DUP) R3925723-3 05/16/2316:32
Original Result DUP Result Dilution DUP RPD
Analyte % % %
Total Solids 81.7 80.5 1 1.44
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1616119-01,02,03,04,05,06
DUP Qualifier DUP RPD
Limits
10
(LCS) R3925723-2 05/16/2316:32
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte % %_ % %
Total Solids 50.0 50.0 100 85.0-115
— I
Cp
Fc
FSS
4
Cn
FSr
_ �GI
FAI
FSC
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 76 of 132

WG2060827
Total Solids by Method 2540 G-2011
Method Blank (MB)
(MB) R3925705-1 05/16/2315:46
MB Result MB Qualifier MB MDL
Analyte % %
Total Solids 0.00200
L1615718-01 Original Sample (OS) • Duplicate (DUP)
MB RDL
(OS) L1615718-01 05/16/2315:46 • (DUP) R3925705-3 05/16/2315:46
Original Result DUP Result Dilution DUP RPD
Analyte % % %
Total Solids 88.9 88.5 1 0.480
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1616119-07,08,09,10,11
DUP Qualifier DUP RPD
Limits
10
(LCS) R3925705-2 05/16/2315:46
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte % % % %
Total Solids 50.0 49.9 99.9 85.0-115
— I
Cp
FC
FSS
4
Cn
FSr
_ �GI
FAI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 77 of 132

WG2059859
Wet Chemistry by Method 7199
Method Blank (MB)
(MB) R3926258-1 05/18/23 04:26
MB Result
Analyte ug/I
Hexavalent Chromium -Low U
Level
MB Qualifier MB MDL MB RDL
ug/I ug/1
0.0400 0.100
L1616119-13 Original Sample (OS) • Duplicate (DUP)
(OS) L1616119-13 05/18/23 05:15 • (DUP) R3926258-5 05/18/23 05:22
Original Result DUP Result Dilution DUP RPD
Analyte ug/I ug/I %
Hexavalent Chromium -Low U U 1 0.000
Level
L1616119-21 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1616119-12,13,14,15,16,17,18,19,20,21
DUP Qualifier DUP RPD
Limits
20
(OS) L1616119-21 05/18/23 06:47 • (DUP) R3926258-7 05/18/23 06:55
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Hexavalent Chromium -Low U U 1 0.000 20
Level
Laboratory Control Sample (LCS)
(LCS) R3926258-2 05/18/23 04:36
Spike Amount LCS Result LCS Rec.
Analyte ug/I ug/I %
Hexavalent Chromium -Low 2.00 2.18 109
Level
Rec. Limits LCS Qualifier
90.0-110
L1616119-12 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1616119-12 05/18/23 04:51 • (MS) R3926258-3 05/18/23 04:59 • (MSD) R3926258-4 05/18/23 05:07
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I % % % % %
Hexavalent Chromium -Low 1.00 U 0.989 1.05 98.9 105 1 90.0-110 5.48 20
Level
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 78 of 132
FP1
Fc
FSS
4
Cn
FSr
�GI
$AI
FSC

WG2059859
Wet Chemistry by Method 7199
QUALITY CONTROL SUMMARY
L1616119-12,13,14,15,16,17,18,19,20,21
L1616119-20 Original Sample (OS) • Matrix Spike (MS)
(OS) L1616119-20 05/18/23 06:31 • (MS) R3926258-6 05/18/23 06:39
Spike Amount Original Result MS Result
Analyte ug/I ug/1 ug/1
Hexavalent Chromium -Low 1.00 U 1.03
Level
MS Rec. Dilution Rec. Limits MS Qualifier
103 1 90.0-110
FP1
Fc
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 79 of 132

WG2061989
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 7199
L1616119-22
Method Blank (MB)
(MB) R3927764-1 05/22/23 01:46
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/1 ug/1 ug/1
Hexavalent Chromium -Low U 0.0400 0.100
Level
L1616635-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1616635-02 05/22/23 02:46 • (DUP) R3927764-4 05/22/23 02:53
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %
%
Hexavalent Chromium -Low U U 1 0.000
20
Level
L1616635-14 Original Sample (OS) • Duplicate (DUP)
(OS) L1616635-14 05/22/23 04:41 • (DUP) R3927764-5 05/22/23 04:49
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/1 % %
Hexavalent Chromium -Low U U 1 0.000 20
Level
Laboratory Control Sample (LCS)
(LCS) R3927764-2 05/22/23 01:56
Spike Amount LCS Result LCS Rec.
Analyte ug/I ug/1 %
Hexavalent Chromium -Low 2.00 1.95 97.3
Level
Rec. Limits LCS Qualifier
90.0-110
L1616635-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1616635-01 05/22/23 02:30 • (MS) R3927764-3 05/22/23 02:38
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte ug/I ug/1 ug/1 % %
Hexavalent Chromium -Low 1.00 U 0.938 93.8 1 90.0-110
Level
FP1
Fc
FSS
4
Cn
FSr
�GI
$AI
[Sc
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 80 of 132

WG2061989 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 7199 L1616119-22
L1618226-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1618226-05 05/22/23 05:42 • (MS) R3927764-6 05/22/23 05:50 • (MSD) R3927764-7 05/22/23 05:58
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I % % % % %
Hexavalent Chromium -Low 1.00 U 0.911 0.921 91.1 92.1 1 90.0-110 1.11 20
Level
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 81 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2061030
Wet Chemistry by Method 7199
Method Blank (MB)
(MB) R3926139-1 05/17/23 17:13
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1616114-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1616114-01 05/17/2317:26 • (DUP) R3926139-3 05/17/2317.31
Original Result DUP Result Dilution DUP RPD
(dry) (dry)
Analyte mg/kg mg/kg %
Hexavalent Chromium 0.681 0.553 1 20.8
L1616119-07 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1616119-01,02,03,04,05,06,07,08,09,10
DUP Qualifier DUP RPD
Limits
J P1 20
(OS) L1616119-07 05/17/2318:59 • (DUP) R3926139-8 05/17/2319:05
Original Result DUP Result DUP RPD
Dilution DUP RPD DUP Qualifier
(dry) (dry) Limits
Analyte mg/kg mg/kg % %
Hexavalent Chromium 0.507 0.683 1 29.5 J P1 20
Laboratory Control Sample (LCS)
(LCS) R3926139-2 05/17/2317:21
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg % %
Hexavalent Chromium 10.0 8.80 88.0 80.0-120
L1616114-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1616114-05 05/17/2317:52 • (MS) R3926139-4 05/17/2317:57 • (MSD) R3926139-5 05/17/2318:02
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg % % % %
Hexavalent Chromium 24.1 0.574 20.3 19.7 81.9 79.5 1 75.0-125 2.85
RPD Limits
20
— I
Cp
FC
FSS
4
Cn
FSr
_ �GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 82 of 132

WG2061030 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 7199 L1616119-01,02,03,04,05,06,07,08,09,10
L1616114-05 Original Sample (OS) • Matrix Spike (MS)
(OS) L1616114-05 05/17/2317:52 • (MS) R3926139-6 05/17/2318:18
Spike Amount Original Result MS Result (dry) MS Rec. Dilution Rec. Limits MS Qualifier
(dry) (dry)
Analyte mg/kg mg/kg mg/kg % %
Hexavalent Chromium 771 0.574 938 122 50 75.0-125
FP1
Fc
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 83 of 132

WG2061041
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 7199
L1616119-11
Method Blank (MB)
(MB) R3925906-1 05/17/2310:25
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1615483-08 Original Sample (OS) • Duplicate (DUP)
(OS) L1615483-08 05/17/2311:45 • (DUP) R3925906-7 05/17/2311:50
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %
%
Hexavalent Chromium U U 1 0.000
20
L1616119-11 Original Sample (OS) • Duplicate (DUP)
(OS) L1616119-11 05/17/2311:56 • (DUP) R3925906-8 05/17/2312:01
Original Result DUP Result DUP RPD
Dilution DUP RPD DUP Qualifier
(dry) (dry) Limits
Analyte mg/kg mg/kg % %
Hexavalent Chromium 0.689 0.585 1 16.2 J 20
Laboratory Control Sample (LCS)
(LCS) R3925906-2 05/17/2310:33
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg % %
Hexavalent Chromium 10.0 9.78 97.8 80.0-120
L1615483-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615483-01 05/17/2310:38 • (MS) R3925906-3 05/17/2310:43 • (MSD) R3925906-4 05/17/2310:48
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/kg mg/kg mg/kg mg/kg % % % %
Hexavalent Chromium 20.0 U 17.1 12.9 85.6 64.6 1 75.0-125 J3 J6 28.0
L1615483-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1615483-01 05/17/2310:38 • (MS) R3925906-5 05/17/2310:53
Spike Amount Original Result MS Result MS Rec.
Analyte mg/kg mg/kg mg/kg %
Hexavalent Chromium 638 U 336 52.7
Dilution Rec. Limits MS Qualifier
50 75.0-125 J6
RPD Limits
20
— I
Cp
Fc
FSS
4
Cn
FSr
_ �GI
FAI
FSC
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 84 of 132

WG2060584
Mercury by Method 7470A
Method Blank (MB)
(MB) R3933053-1 06/05/2319:24
MB Result
Analyte ug/1
Mercury U
MB Qualifier MB MDL MB RDL
ug/1 ug/I
0.100 0.200
Laboratory Control Sample (LCS)
(LCS) R3933053-2 06/05/2319:26
Spike Amount LCS Result LCS Rec.
Analyte ug/I ug/1 %
Mercury 3.00 3.02 101
QUALITY CONTROL SUMMARY
L1616119-12,13,14,15,16,17,18,19,20,21,22
Rec. Limits LCS Qualifier
80.0-120
L1616119-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1616119-19 06/05/2319:29 • (MS) R3933053-3 06/05/2319:31 • (MSD) R3933053-4 06/05/2319:33
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte ug/I ug/1 ug/1 ug/I % % % %
Mercury 3.00 U 3.03 3.08 101 103 1 75.0-125 1.70
RPD Limits
20
— I
Cp
FC
FSS
4
Cn
FSr
�GI
_ $AI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 85 of 132

--------------
WG2059805
Mercury by Method 7471B
Method Blank (MB)
(MB) R3932641-1 06/04/23 17:46
MB Result
Analyte mg/kg
Mercury U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3932641-2 06/04/2317:48
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg %
Mercury 0.500 0.507 101
QUALITY CONTROL SUMMARY
1-1616119-02,03,04,06,07
Rec. Limits LCS Qualifier
80.0-120
L1616119-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1616119-02 06/04/2317:50 • (MS) R3932641-3 06/04/2317:53 • (MSD) R3932641-4 06/04/2317:55
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg % % % % %
Mercury 0.606 U 0.554 0.534 91.6 88.2 1 75.0-125 3.76 20
— I
Cp
Fc
FSS
4
Cn
FSr
�GI
FAI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 86 of 132

--------------
WG2061958
Mercury by Method 7471B
Method Blank (MB)
(MB) R3933042-1 06/05/23 17:59
MB Result
Analyte mg/kg
Mercury U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0180 0.0400
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1616119-01,05,08,09,10,11
(LCS) R3933042-2 06/05/2318:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg % %
Mercury 0.500 0.493 98.7 80.0-120
L1616160-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1616160-01 06/05/2318:04 • (MS) R3933042-3 06/05/2318:06 • (MSD) R3933042-4 06/05/2318:09
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec. MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg % %
%
% %
Mercury 0.630 0.0923
0.691
0.713 95.0 98.6
1 75.0-125
3.18 20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28 87 of 132
— I
Cp
Fc
FSS
4
Cn
FSr
�GI
FAI
[Sc

WG2060154
Metals (ICPMS) by Method 6020B
Method Blank (MB)
(MB) R3928492-1 05/23/23 21:43
MB Result
MB Qualifier MB MDL
MB RDL
Analyte ug/I
ug/I
ug/I
Arsenic U
0.180
2.00
Barium U
0.381
2.00
Cadmium U
0.150
1.00
Chromium U
1.24
2.00
Lead U
0.849
2.00
Selenium U
0.300
2.00
Silver U
0.0700
2.00
Laboratory Control Sample (LCS)
(LCS) R3928492-2 05/23/23 21:46
Spike Amount
LCS Result
LCS Rec.
Analyte ug/I
ug/I
%
Arsenic 50.0
51.2
102
Barium 50.0
51.5
103
Cadmium 50.0
52.1
104
Chromium 50.0
51.7
103
Lead 50.0
51.7
103
Selenium 50.0
53.9
108
Silver 50.0
52.4
105
QUALITY CONTROL SUMMARY
L1616119-12,13,14,15,16,17,18,19,20,21,22
Rec. Limits LCS Qualifier
o/
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
L1616068-21 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1616068-21 05/23/23 21:50 • (MS) R3928492-4 05/23/23 21:56 • (MSD) R3928492-5 05/23/23 22:00
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/I
ug/I
ug/I
%
%
Arsenic
50.0
0.447
53.7
51.4
106
102
Barium
50.0
5.27
56.7
58.0
103
106
Cadmium
50.0
U
53.7
54.3
107
109
Chromium
50.0
U
52.6
50.3
105
101
Lead
50.0
U
51.5
55.4
103
111
Selenium
50.0
1.06
55.2
55.4
108
109
Silver
50.0
U
53.4
53.5
107
107
Dilution Rec. Limits
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
MS Qualifier
MSD Qualifier RPD
4.35
2.41
1.23
4.57
7.25
0.444
0.226
RPD Limits
20
20
20
20
20
20
20
FP1
Fc
FSS
4
Cn
FSr
�GI
FAI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 88 of 132

WG2061326 QUALITY CONTROL SUMMARY
Metals (ICPMS) by Method 6020B L1616119-01,02,03,04,05,06,07,08,09,10,11
Method Blank (MB)
(MB) R3926217-1 05/17/2319:48
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/kg
mg/kg
mg/kg
Arsenic U
0.100
1.00
Barium U
0.152
2.50
Cadmium U
0.0855
1.00
Chromium U
0.297
5.00
Lead U
0.0990
2.00
Selenium U
0.180
2.50
Silver U
0.0865
0.500
Laboratory Control Sample (LCS)
(LCS) R3926217-2 05/17/2319:52
Spike Amount
LCS Result
LCS Rec.
Analyte mg/kg
mg/kg
%
Arsenic 100
102
102
Barium 100
100
100
Cadmium 100
106
106
Chromium 100
101
101
Lead 100
98.0
98.0
Selenium 100
108
108
Silver 20.0
20.1
101
Rec. Limits LCS Qualifier
°/
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
L1616575-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1616575-05 05/17/2319:55 • (MS) R3926217-5 05/17/23 20:05 • (MSD) R3926217-6 05/17/23 20:08
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution
Rec. Limits
MS Qualifier MSD Qualifier RPD
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
Arsenic
100
3.05
87.7
89.7
84.7
86.6
5
75.0-125
2.18
Barium
100
162
263
247
101
84.7
5
75.0-125
6.36
Cadmium
100
0.139
93.7
95.7
93.6
95.6
5
75.0-125
2.15
Chromium
100
31.8
120
122
88.4
90.6
5
75.0-125
1.90
Lead
100
12.6
100
105
87.8
92.8
5
75.0-125
4.83
Selenium
100
0.422
95.7
95.5
95.3
95.1
5
75.0-125
0.262
Silver
20.0
U
17.8
18.1
88.9
90.7
5
75.0-125
1.98
RPD Limits
20
20
20
20
20
20
20
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
[Sc
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 89 of 132

WG2064057 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1616119-12,13,14,15,16,17,18,19,20,21,22
Method Blank (MB)
(MB) R3927763-3 05/21/23 23:51
MB Result
Analyte
ug/I
Acetone
U
Acrolein
U
Acrylonitrile
U
Benzene
U
Bromobenzene
U
Bromochloromethane
U
Bromodichloromethane
U
Bromoform
U
Bromomethane
U
n-Butylbenzene
U
sec -Butyl benzene
U
tert-Butylbenzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chlorodibromomethane
U
Chloroethane
U
Chloroform
U
Chloromethane
U
2-Chlorotoluene
U
4-Chlorotoluene
U
1,2-Dibromo-3-Chloropropane
U
1,2-Dibromoethane
U
Dibromomethane
U
1,2-Dichlorobenzene
U
1,3-Dichlorobenzene
U
1,4-Dichlorobenzene
U
Dichlorodifluoromethane
U
1,1-Dichloroethane
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
cis-1,2-Dichloroethene
U
trans-1,2-Dichloroethene
U
1,2-Dichloropropane
U
1,1-Dichloropropene
U
1,3-Dichloropropane
U
cis-1,3-Dichloropropene
U
trans-1,3-Dichloropropene
U
2,2-Dichloropropane
U
Di -isopropyl ether
U
Ethylbenzene
U
MB Qualifier MB MDL
ug/I
MB RDL
ug/I
11.3
50.0
2.54
50.0
0.671
10.0
0.0941
1.00
0.118
1.00
0.128
1.00
0.136
1.00
0.129
1.00
0.605
5.00
0.157
1.00
0.125
1.00
0.127
1.00
0.128
1.00
0.116
1.00
0.140
1.00
0.192
5.00
0.111
5.00
0.960
2.50
0.106
1.00
0.114
1.00
0.276
5.00
0.126
1.00
0.122
1.00
0.107
1.00
0.110
1.00
0.120
1.00
0.374
5.00
0.100
1.00
0.0819
1.00
0.188
1.00
0.126
1.00
0.149
1.00
0.149
1.00
0.142
1.00
0.110
1.00
0.111
1.00
0.118
1.00
0.161
1.00
0.105
1.00
0.137
1.00
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 90 of 132

WG2064057 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1616119-12,13,14,15,16,17,18,19,20,21,22
Method Blank (MB)
(MB) R3927763-3 05/21/23 23:51
MB Result
Analyte ug/I
MB Qualifier
MB MDL MB RDL
ug/I ug/I
Hexachloro-1,3-butadiene
U
0.337
1.00
2-Hexanone
U
0.787
10.0
Isopropylbenzene
U
0.105
1.00
p-Isopropyltoluene
U
0.120
1.00
2-Butanone (MEK)
U
1.19
10.0
Methylene Chloride
U
0.430
5.00
4-Methyl-2-pentanone (MIBK)
U
0.478
10.0
Methyl tert-butyl ether
U
0.101
1.00
Naphthalene
U
1.00
5.00
n-Propylbenzene
U
0.0993
1.00
Styrene
U
0.118
1.00
1,1,1,2-Tetrachloroethane
U
0.147
1.00
1,1,2,2-Tetrachloroethane
U
0.133
1.00
Tetrachloroethene
U
0.300
1.00
Toluene
U
0.278
1.00
1,2,3-Trichlorobenzene
U
0.230
1.00
1,2,4-Trichlorobenzene
U
0.481
1.00
1,1,1-Trichloroethane
U
0.149
1.00
1,1,2-Trichloroethane
U
0.158
1.00
Trichloroethene
U
0.190
1.00
Trichlorofluoromethane
U
0.160
5.00
1,2,3-Trichloropropane
U
0.237
2.50
1,2,4-Trimethylbenzene
U
0.322
1.00
1,3,5-Trimethyl benzene
U
0.104
1.00
Vinyl acetate
U
0.692
10.0
Vinyl chloride
U
0.234
1.00
o-Xylene
U
0.174
1.00
m&p-Xylenes
U
0.430
2.00
(S) Toluene-d8
106
80.0-120
(S) 4-Bromof/uorobenzene
96.4
77.0-126
(S) 1,2-Dich/oroethone-d4
92.4
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3927763-1 05/21/23 22:35 • (LCSD) R3927763-2 05/21/23 22:54
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte ug/I
ug/I
ug/I
%
%
%
Acetone 25.0
21.0
20.5
84.0
82.0
19.0-160
Acrolein 25.0
20.5
16.5
82.0
66.0
10.0-160
ACCOUNT: PROJECT:
Withers & Ravenel Eng. - Standard 23-0302
LCS Qualifier LCSD Qualifier RPD RPD Limits
2.41 27
21.6 26
SDG: DATE/TIME: PAGE:
L1616119 06/06/23 12:28 91 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2064057 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1616119-12,13,14,15,16,17,18,19,20,21,22
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3927763-1 05/21/23 22:35 • (LCSD) R3927763-2 05/21/23 22:54
Spike Amount
LCS Result
LCSD Result
LCS Rec.
Analyte
ug/I
ug/I
ug/I
%
Acrylonitrile
25.0
27.1
26.3
108
Benzene
5.00
4.71
4.42
94.2
Bromobenzene
5.00
4.55
4.10
91.0
Bromochloromethane
5.00
4.47
4.01
89.4
Bromodichloromethane
5.00
4.77
4.41
95.4
Bromoform
5.00
4.19
3.89
83.8
Bromomethane
5.00
5.36
4.71
107
n-Butylbenzene
5.00
4.52
4.26
90.4
sec -Butyl benzene
5.00
4.68
4.28
93.6
tert-Butylbenzene
5.00
4.75
4.20
95.0
Carbon tetrachloride
5.00
4.27
3.77
85.4
Chlorobenzene
5.00
4.64
4.38
92.8
Chlorodibromomethane
5.00
4.26
3.97
85.2
Chloroethane
5.00
5.35
4.93
107
Chloroform
5.00
4.59
4.12
91.8
Chloromethane
5.00
5.46
5.41
109
2-Chlorotoluene
5.00
4.45
4.11
89.0
4-Chlorotoluene
5.00
4.47
4.28
89.4
1,2-Dibromo-3-Chloropropane
5.00
4.02
4.16
80.4
1,2-Dibromoethane
5.00
4.71
4.28
94.2
Dibromomethane
5.00
4.55
4.05
91.0
1,2-Dichlorobenzene
5.00
4.37
4.11
87.4
1,3-Dichlorobenzene
5.00
4.34
4.13
86.8
1,4-Dichlorobenzene
5.00
4.44
4.20
88.8
Dichlorodifluoromethane
5.00
4.11
3.62
82.2
1,1-Dichloroethane
5.00
4.46
4.05
89.2
1,2-Dichloroethane
5.00
4.73
4.22
94.6
1,1-Dichloroethene
5.00
4.42
4.14
88.4
cis-1,2-Dichloroethene
5.00
4.63
4.24
92.6
trans-1,2-Dichloroethene
5.00
4.75
4.30
95.0
1,2-Dichloropropane
5.00
4.48
4.30
89.6
1,1-Dichloropropene
5.00
4.55
4.15
91.0
1,3-Dichloropropane
5.00
4.98
4.54
99.6
cis-1,3-Dichloropropene
5.00
4.69
4.37
93.8
trans-1,3-Dichloropropene
5.00
4.62
4.34
92.4
2,2-Dichloropropane
5.00
4.84
4.04
96.8
Di -isopropyl ether
5.00
4.45
4.11
89.0
Ethylbenzene
5.00
4.64
4.32
92.8
Hexachloro-1,3-butadiene
5.00
5.16
5.21
103
2-Hexanone
25.0
25.9
25.9
104
ACCOUNT:
Withers & Ravenel Eng. - Standard
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
105
55.0-149
3.00
20
88.4
70.0-123
6.35
20
82.0
73.0-121
10.4
20
80.2
76.0-122
10.8
20
88.2
75.0-120
7.84
20
77.8
68.0-132
7.43
20
94.2
10.0-160
12.9
25
85.2
73.0-125
5.92
20
85.6
75.0-125
8.93
20
84.0
76.0-124
12.3
20
75.4
68.0-126
12.4
20
87.6
80.0-121
5.76
20
79.4
77.0-125
7.05
20
98.6
47.0-150
8.17
20
82.4
73.0-120
10.8
20
108
41.0-142
0.920
20
82.2
76.0-123
7.94
20
85.6
75.0-122
4.34
20
83.2
58.0-134
3.42
20
85.6
80.0-122
9.57
20
81.0
80.0-120
11.6
20
82.2
79.0-121
6.13
20
82.6
79.0-120
4.96
20
84.0
79.0-120
5.56
20
72.4
51.0-149
12.7
20
81.0
70.0-126
9.64
20
84.4
70.0-128
11.4
20
82.8
71.0-124
6.54
20
84.8
73.0-120
8.79
20
86.0
73.0-120
9.94
20
86.0
77.0-125
4.10
20
83.0
74.0-126
9.20
20
90.8
80.0-120
9.24
20
87.4
80.0-123
7.06
20
86.8
78.0-124
6.25
20
80.8
58.0-130
18.0
20
82.2
58.0-138
7.94
20
86.4
79.0-123
7.14
20
104
54.0-138
0.964
20
104
67.0-149
0.000
20
PROJECT:
SDG:
DATE/TIME: PAGE:
23-0302
L1616119
06/06/23 12:28 92 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2064057 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1616119-12,13,14,15,16,17,18,19,20,21,22
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3927763-1 05/21/23 22:35 • (LCSD) R3927763-2 05/21/23 22:54
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
ug/I
ug/I
ug/I
%
%
%
%
%
Isopropylbenzene
5.00
4.51
4.21
90.2
84.2
76.0-127
6.88
20
p-Isopropyltoluene
5.00
4.49
4.16
89.8
83.2
76.0-125
7.63
20
2-Butanone (MEK)
25.0
25.9
22.8
104
91.2
44.0-160
12.7
20
Methylene Chloride
5.00
4.76
4.30
95.2
86.0
67.0-120
10.2
20
4-Methyl-2-pentanone (MIBK)
25.0
25.2
24.0
101
96.0
68.0-142
4.88
20
Methyl tert-butyl ether
5.00
4.37
4.06
87.4
81.2
68.0-125
7.35
20
Naphthalene
5.00
4.02
4.70
80.4
94.0
54.0-135
15.6
20
n-Propylbenzene
5.00
4.60
4.31
92.0
86.2
77.0-124
6.51
20
Styrene
5.00
3.96
3.80
79.2
76.0
73.0-130
4.12
20
1,1,1,2-Tetrachloroethane
5.00
4.23
3.94
84.6
78.8
75.0-125
7.10
20
1,1,2,2-Tetrachloroethane
5.00
4.58
4.27
91.6
85.4
65.0-130
7.01
20
Tetrachloroethene
5.00
4.97
4.53
99.4
90.6
72.0-132
9.26
20
Toluene
5.00
4.65
4.36
93.0
87.2
79.0-120
6.44
20
1,2,3-Trichlorobenzene
5.00
4.17
4.76
83.4
95.2
50.0-138
13.2
20
1,2,4-Trichlorobenzene
5.00
4.17
4.62
83.4
92.4
57.0-137
10.2
20
1,1,1-Trichloroethane
5.00
4.48
4.04
89.6
80.8
73.0-124
10.3
20
1,1,2-Trichloroethane
5.00
4.95
4.71
99.0
94.2
80.0-120
4.97
20
Trichloroethene
5.00
4.83
4.46
96.6
89.2
78.0-124
7.97
20
Trichlorofluoromethane
5.00
4.80
4.43
96.0
88.6
59.0-147
8.02
20
1,2,3-Trichloropropane
5.00
4.64
4.27
92.8
85.4
73.0-130
8.31
20
1,2,4-Trimethylbenzene
5.00
4.41
4.07
88.2
81.4
76.0-121
8.02
20
1,3,5-Trimethyl benzene
5.00
4.43
4.05
88.6
81.0
76.0-122
8.96
20
Vinyl acetate
25.0
24.2
23.0
96.8
92.0
11.0-160
5.08
20
Vinyl chloride
5.00
5.74
5.19
115
104
67.0-131
10.1
20
o-Xylene
5.00
4.21
3.97
84.2
79.4
80.0-122
J4 5.87
20
m&p-Xylenes
10.0
9.13
8.56
91.3
85.6
80.0-122
6.44
20
(S) Toluene-d8
104
106
80.0-120
(S) 4-Bromof/uorobenzene
95.3
97.4
77.0-126
(S)1,2-Dich/oroethane-d4
92.0
90.3
70.0-130
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28 93 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2064510
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
QUALITY CONTROL SUMMARY
L1616119-13,14
Method Blank (MB)
(MB) R3928279-3 05/22/23 23:12
MB Result
Analyte
ug/I
Benzene
U
Ethylbenzene
U
Toluene
U
1,2,4-Trimethylbenzene
U
1,3,5-Trimethyl benzene
U
o-Xylene
U
m&p-Xylenes
U
(S) Toluene-d8
98.4
(S) 4-Bromofluorobenzene 98.6
(S) 1,2-Dich/oroethone-d4 108
MB Qualifier
MB MDL
ug/I
0.0941
0.137
0.278
0.322
0.104
0.174
0.430
MB RDL
ug/I
1.00
1.00
1.00
1.00
1.00
1.00
2.00
80.0-120
77.0-126
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3928279-1 05/22/23 22:08 • (LCSD) R3928279-2 05/22/23 22:30
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
ug/I
ug/I
ug/I
%
%
%
%
%
Benzene
5.00
5.17
5.43
103
109
70.0-123
4.91
20
Ethylbenzene
5.00
4.80
4.75
96.0
95.0
79.0-123
1.05
20
Toluene
5.00
4.99
5.05
99.8
101
79.0-120
1.20
20
1,2,4-Trimethylbenzene
5.00
5.16
5.48
103
110
76.0-121
6.02
20
1,3,5-Trimethyl benzene
5.00
5.39
5.45
108
109
76.0-122
1.11
20
o-Xylene
5.00
4.87
5.01
97.4
100
80.0-122
2.83
20
m&p-Xylenes
10.0
10.2
9.90
102
99.0
80.0-122
2.99
20
(S) Toluene-d8
97.2
95.3
80.0-120
(S) 4-Bromofluorobenzene
101
96.1
77 0-126
(S)1,2-Dich/oroethone-d4
110
ill
70.0-130
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 94 of 132

WG2062683
Volatile Organic Compounds (GC/MS) by Method 8260D
QUALITY CONTROL SUMMARY
L1616119-01,02,03,04,05
Method Blank (MB)
(MB) R3926851-3 05/18/23 16:10
MB Result MB Qualifier
Analyte mg/kg
Acetone
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec -Butyl benzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MB MDL
mg/kg
0.0365
0.00361
0.000467
0.000900
0.000725
0.00117
0.00197
0.00525
0.00288
0.00195
0.000898
0.000210
0.000612
0.00170
0.00103
0.00435
0.000865
0.000450
0.00390
0.000648
0.000750
0.000425
0.000600
0.000700
0.00161
0.000491
0.000649
0.000606
0.000734
0.00104
0.00142
0.000809
0.000501
0.000757
0.00114
0.00138
0.000410
0.000737
0.00600
0.000425
MB RDL
mg/kg
0.0500
0.0125
0.00100
0.0125
0.00250
0.0250
0.0125
0.0125
0.0125
0.00500
0.00500
0.00250
0.00250
0.00500
0.00250
0.0125
0.00250
0.00500
0.0250
0.00250
0.00500
0.00500
0.00500
0.00500
0.00250
0.00250
0.00250
0.00250
0.00250
0.00500
0.00500
0.00250
0.00500
0.00250
0.00500
0.00250
0.00100
0.00250
0.0250
0.00250
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 95 of 132

WG2062683
Volatile Organic Compounds (GC/MS) by Method 8260D
QUALITY CONTROL SUMMARY
L1616119-01,02,03,04,05
Method Blank (MB)
(MB) R3926851-3 05/18/23 16:10
MB Result
Analyte mg/kg
p-Isopropyltoluene
U
2-Butanone (MEK)
U
Methylene Chloride
U
4-Methyl-2-pentanone (MIBK)
U
Methyl tert-butyl ether
U
Naphthalene
U
n-Propylbenzene
U
Styrene
0.00123
1,1,1,2-Tetrachloroethane
U
1,1,2,2-Tetrachloroethane
U
Tetrachloroethene
U
Toluene
U
1,2,3-Trichlorobenzene
U
1,2,4-Trichlorobenzene
U
1,1,1-Trichloroethane
U
1,1,2-Trichloroethane
U
1,1,2-Trichlorotrifluoroethane
U
Trichloroethene
U
Trichlorofluoromethane
U
1,2,3-Trichloropropane
U
1,2,4-Trimethylbenzene
U
1,3,5-Trimethyl benzene
U
Vinyl chloride
U
Xylenes, Total
U
(S) Toluene-d8
105
(S) 4-Bromofluorobenzene
91.3
(S) 1,2-Dich/oroethone-d4
88.3
MB Qualifier MB MDL
mg/kg
MB RDL
mg/kg
0.00255
0.00500
0.0635
0.100
0.00664
0.0250
0.00228
0.0250
0.000350
0.00100
0.00488
0.0125
0.000950
0.00500
J 0.000229
0.0125
0.000948
0.00250
0.000695
0.00250
0.000896
0.00250
0.00130
0.00500
0.00733
0.0125
0.00440
0.0125
0.000923
0.00250
0.000597
0.00250
0.000754
0.00250
0.000584
0.00100
0.000827
0.00250
0.00162
0.0125
0.00158
0.00500
0.00200
0.00500
0.00116
0.00250
0.000880 0.00650
75.0-131
67.0-138
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3926851-1 05/18/2311:15 • (LCSD) R3926851-2 05/18/2311:35
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/kg
mg/kg
mg/kg
%
%
%
Acetone
0.625
0.281
0.549
45.0
87.8
10.0-160
Acrylonitrile
0.625
0.534
0.500
85.4
80.0
45.0-153
Benzene
0.125
0.109
0.104
87.2
83.2
70.0-123
Bromobenzene
0.125
0.115
0.123
92.0
98.4
73.0-121
Bromodichloromethane
0.125
0.115
0.119
92.0
95.2
73.0-121
Bromoform
0.125
0.107
0.106
85.6
84.8
64.0-132
ACCOUNT: PROJECT:
Withers & Ravenel Eng. - Standard 23-0302
LCS Qualifier LCSD Qualifier RPD
RPD Limits
J3 64.6
31
6.58
22
4.69
20
6.72
20
3.42
20
0.939
20
SDG:
DATE/TIME: PAGE:
L1616119
06/06/23 12:28 96 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2062683 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1616119-01,02,03,04,05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3926851-1 05/18/2311:15 • (LCSD) R3926851-2 05/18/2311:35
Spike Amount
LCS Result
LCSD Result
Analyte
mg/kg
mg/kg
mg/kg
Bromomethane
0.125
0.110
0.0963
n-Butylbenzene
0.125
0.101
0.105
sec -Butyl benzene
0.125
0.109
0.115
tert-Butylbenzene
0.125
0.102
0.112
Carbon tetrachloride
0.125
0.105
0.0938
Chlorobenzene
0.125
0.110
0.109
Chlorodibromomethane
0.125
0.111
0.112
Chloroethane
0.125
0.115
0.104
Chloroform
0.125
0.104
0.0919
Chloromethane
0.125
0.142
0.114
2-Chlorotoluene
0.125
0.104
0.108
4-Chlorotoluene
0.125
0.116
0.118
1,2-Dibromo-3-Chloropropane
0.125
0.0926
0.0971
1,2-Dibromoethane
0.125
0.115
0.119
Dibromomethane
0.125
0.116
0.117
1,2-Dichlorobenzene
0.125
0.109
0.112
1,3-Dichlorobenzene
0.125
0.110
0.119
1,4-Dichlorobenzene
0.125
0.108
0.110
Dichlorodifluoromethane
0.125
0.129
0.122
1,1-Dichloroethane
0.125
0.103
0.0956
1,2-Dichloroethane
0.125
0.109
0.106
1,1-Dichloroethene
0.125
0.100
0.0917
cis-1,2-Dichloroethene
0.125
0.0974
0.0881
trans-1,2-Dichloroethene
0.125
0.104
0.0941
1,2-Dichloropropane
0.125
0.113
0.113
1,1-Dichloropropene
0.125
0.111
0.109
1,3-Dichloropropane
0.125
0.117
0.123
cis-1,3-Dichloropropene
0.125
0.120
0.123
trans-1,3-Dichloropropene
0.125
0.114
0.121
2,2-Dichloropropane
0.125
0.108
0.0972
Di -isopropyl ether
0.125
0.106
0.0956
Ethylbenzene
0.125
0.109
0.104
Hexachloro-1,3-butadiene
0.125
0.107
0.108
Isopropylbenzene
0.125
0.101
0.0972
p-Isopropyltoluene
0.125
0.101
0.109
2-Butanone (MEK)
0.625
0.613
0.624
Methylene Chloride
0.125
0.101
0.0885
4-Methyl-2-pentanone (MIBK)
0.625
0.538
0.532
Methyl tert-butyl ether
0.125
0.106
0.0937
Naphthalene
0.125
0.0815
0.0888
ACCOUNT:
Withers & Ravenel Eng. - Standard
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
88.0
77.0
56.0-147
13.3
20
80.8
84.0
68.0-135
3.88
20
87.2
92.0
74.0-130
5.36
20
81.6
89.6
75.0-127
9.35
20
84.0
75.0
66.0-128
11.3
20
88.0
87.2
76.0-128
0.913
20
88.8
89.6
74.0-127
0.897
20
92.0
83.2
61.0-134
10.0
20
83.2
73.5
72.0-123
12.4
20
114
91.2
51.0-138
J3 21.9
20
83.2
86.4
75.0-124
3.77
20
92.8
94.4
75.0-124
1.71
20
74.1
77.7
59.0-130
4.74
20
92.0
95.2
74.0-128
3.42
20
92.8
93.6
75.0-122
0.858
20
87.2
89.6
76.0-124
2.71
20
88.0
95.2
76.0-125
7.86
20
86.4
88.0
77.0-121
1.83
20
103
97.6
43.0-156
5.58
20
82.4
76.5
70.0-127
7.45
20
87.2
84.8
65.0-131
2.79
20
80.0
73.4
65.0-131
8.66
20
77.9
70.5
73.0-125
J4 10.0
20
83.2
75.3
71.0-125
9.99
20
90.4
90.4
74.0-125
0.000
20
88.8
87.2
73.0-125
1.82
20
93.6
98.4
80.0-125
5.00
20
96.0
98.4
76.0-127
2.47
20
91.2
96.8
73.0-127
5.96
20
86.4
77.8
59.0-135
10.5
20
84.8
76.5
60.0-136
10.3
20
87.2
83.2
74.0-126
4.69
20
85.6
86.4
57.0-150
0.930
20
80.8
77.8
72.0-127
3.83
20
80.8
87.2
72.0-133
7.62
20
98.1
99.8
30.0-160
1.78
24
80.8
70.8
68.0-123
13.2
20
86.1
85.1
56.0-143
1.12
20
84.8
75.0
66.0-132
12.3
20
65.2
71.0
59.0-130
8.57
20
PROJECT:
SDG:
DATE/TIME: PAGE:
23-0302
L1616119
06/06/23 12:28 97 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2062683 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1616119-01,02,03,04,05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3926851-1 05/18/2311:15 • (LCSD) R3926851-2 05/18/2311:35
Spike Amount
LCS Result
LCSD Result
Analyte
mg/kg
mg/kg
mg/kg
n-Propylbenzene
0.125
0.108
0.119
Styrene
0.125
0.0958
0.0954
1,1,1,2-Tetrachloroethane
0.125
0.105
0.0968
1,1,2,2-Tetrachloroethane
0.125
0.117
0.124
Tetrachloroethene
0.125
0.102
0.106
Toluene
0.125
0.103
0.106
1,2,3-Trichlorobenzene
0.125
0.0913
0.0947
1,2,4-Trichlorobenzene
0.125
0.0975
0.105
1,1,1-Trichloroethane
0.125
0.103
0.0977
1,1,2-Trichloroethane
0.125
0.119
0.120
1,1,2-Trichlorotrifluoroethane
0.125
0.105
0.0970
Trichloroethene
0.125
0.104
0.107
Trichlorofluoromethane
0.125
0.138
0.129
1,2,3-Trichloropropane
0.125
0.110
0.117
1,2,4-Trimethylbenzene
0.125
0.101
0.105
1,3,5-Trimethyl benzene
0.125
0.113
0.117
Vinyl chloride
0.125
0.121
0.104
Xylenes, Total
0.375
0.309
0.298
(S) Toluene-d8
(S) 4-Bromof/uorobenzene
(S) 1,2-Dich/oroethane-d4
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
86.4
95.2
74.0-126
9.69
20
76.6
76.3
72.0-127
0.418
20
84.0
77.4
74.0-129
8.13
20
93.6
99.2
68.0-128
5.81
20
81.6
84.8
70.0-136
3.85
20
82.4
84.8
75.0-121
2.87
20
73.0
75.8
59.0-139
3.66
20
78.0
84.0
62.0-137
7.41
20
82.4
78.2
69.0-126
5.28
20
95.2
96.0
78.0-123
0.837
20
84.0
77.6
61.0-139
7.92
20
83.2
85.6
76.0-126
2.84
20
110
103
61.0-142
6.74
20
88.0
93.6
67.0-129
6.17
20
80.8
84.0
70.0-126
3.88
20
90.4
93.6
73.0-127
3.48
20
96.8
83.2
63.0-134
15.1
20
82.4
79.5
72.0-127
3.62
20
99.3
100
75.0-131
94.8
90.9
67.0-138
99.7
97.1
70.0-130
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 98 of 132

WG2063443
Volatile Organic Compounds (GC/MS) by Method 8260D
QUALITY CONTROL SUMMARY
L1616119-06,07,08,09,10
Method Blank (MB)
(MB) R3928086-3 05/19/2313:58
MB Result MB Qualifier
Analyte mg/kg
Acetone
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec -Butyl benzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MB MDL
mg/kg
0.0365
0.00361
0.000467
0.000900
0.000725
0.00117
0.00197
0.00525
0.00288
0.00195
0.000898
0.000210
0.000612
0.00170
0.00103
0.00435
0.000865
0.000450
0.00390
0.000648
0.000750
0.000425
0.000600
0.000700
0.00161
0.000491
0.000649
0.000606
0.000734
0.00104
0.00142
0.000809
0.000501
0.000757
0.00114
0.00138
0.000410
0.000737
0.00600
0.000425
MB RDL
mg/kg
0.0500
0.0125
0.00100
0.0125
0.00250
0.0250
0.0125
0.0125
0.0125
0.00500
0.00500
0.00250
0.00250
0.00500
0.00250
0.0125
0.00250
0.00500
0.0250
0.00250
0.00500
0.00500
0.00500
0.00500
0.00250
0.00250
0.00250
0.00250
0.00250
0.00500
0.00500
0.00250
0.00500
0.00250
0.00500
0.00250
0.00100
0.00250
0.0250
0.00250
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 99 of 132

WG2063443
Volatile Organic Compounds (GC/MS) by Method 8260D
QUALITY CONTROL SUMMARY
L1616119-06,07,08,09,10
Method Blank (MB)
(MB) R3928086-3 05/19/2313:58
Analyte
MB Result
mg/kg
MB Qualifier
MB MDL
mg/kg
MB RDL
mg/kg
p-Isopropyltoluene
U
0.00255
0.00500
2-Butanone (MEK)
U
0.0635
0.100
Methylene Chloride
U
0.00664
0.0250
4-Methyl-2-pentanone (MIBK)
U
0.00228
0.0250
Methyl tert-butyl ether
U
0.000350
0.00100
Naphthalene
U
0.00488
0.0125
n-Propylbenzene
U
0.000950
0.00500
Styrene
U
0.000229
0.0125
1,1,1,2-Tetrachloroethane
U
0.000948
0.00250
1,1,2,2-Tetrachloroethane
U
0.000695
0.00250
Tetrachloroethene
U
0.000896
0.00250
Toluene
U
0.00130
0.00500
1,2,3-Trichlorobenzene
U
0.00733
0.0125
1,2,4-Trichlorobenzene
U
0.00440
0.0125
1,1,1-Trichloroethane
U
0.000923
0.00250
1,1,2-Trichloroethane
U
0.000597
0.00250
1,1,2-Trichlorotrifluoroethane
U
0.000754
0.00250
Trichloroethene
U
0.000584
0.00100
Trichlorofluoromethane
U
0.000827
0.00250
1,2,3-Trichloropropane
U
0.00162
0.0125
1,2,4-Trimethylbenzene
U
0.00158
0.00500
1,3,5-Trimethyl benzene
U
0.00200
0.00500
Vinyl chloride
U
0.00116
0.00250
Xylenes, Total
U
0.000880
0.00650
(S) Toluene-d8
108
75.0-131
(S) 4-Bromofluorobenzene
93.6
67.0-138
(S)1,2-Dich/oroethone-d4
107
70.0-130
Laboratory Control
Sample (LCS) • Laboratory
Control Sample
Duplicate (LCSD)
(LCS) R3928086-1 05/19/2312:10 • (LCSD) R3928086-2 05/19/2312:31
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/kg
mg/kg
mg/kg
%
%
%
Acetone
0.625
0.567
0.576
90.7
92.2
10.0-160
Acrylonitrile
0.625
0.577
0.614
92.3
98.2
45.0-153
Benzene
0.125
0.112
0.120
89.6
96.0
70.0-123
Bromobenzene
0.125
0.118
0.130
94.4
104
73.0-121
Bromodichloromethane
0.125
0.113
0.121
90.4
96.8
73.0-121
Bromoform
0.125
0.0909
0.101
72.7
80.8
64.0-132
ACCOUNT: PROJECT:
Withers & Ravenel Eng. - Standard 23-0302
LCS Qualifier LCSD Qualifier RPD
RPD Limits
1.57
31
6.21
22
6.90
20
9.68
20
6.84
20
10.5
20
SDG:
DATE/TIME: PAGE:
L1616119
06/06/23 12:28 100 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2063443 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1616119-06,07,08,09,10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3928086-1 05/19/2312:10 • (LCSD) R3928086-2 05/19/2312:31
Spike Amount
LCS Result
LCSD Result
Analyte
mg/kg
mg/kg
mg/kg
Bromomethane
0.125
0.110
0.121
n-Butylbenzene
0.125
0.116
0.130
sec -Butyl benzene
0.125
0.128
0.133
tert-Butylbenzene
0.125
0.102
0.123
Carbon tetrachloride
0.125
0.110
0.119
Chlorobenzene
0.125
0.115
0.118
Chlorodibromomethane
0.125
0.104
0.108
Chloroethane
0.125
0.118
0.122
Chloroform
0.125
0.116
0.123
Chloromethane
0.125
0.141
0.157
2-Chlorotoluene
0.125
0.127
0.131
4-Chlorotoluene
0.125
0.127
0.135
1,2-Dibromo-3-Chloropropane
0.125
0.0971
0.104
1,2-Dibromoethane
0.125
0.107
0.115
Dibromomethane
0.125
0.112
0.119
1,2-Dichlorobenzene
0.125
0.119
0.132
1,3-Dichlorobenzene
0.125
0.120
0.127
1,4-Dichlorobenzene
0.125
0.123
0.128
Dichlorodifluoromethane
0.125
0.0894
0.0997
1,1-Dichloroethane
0.125
0.115
0.125
1,2-Dichloroethane
0.125
0.120
0.126
1,1-Dichloroethene
0.125
0.117
0.126
cis-1,2-Dichloroethene
0.125
0.105
0.115
trans-1,2-Dichloroethene
0.125
0.105
0.115
1,2-Dichloropropane
0.125
0.106
0.116
1,1-Dichloropropene
0.125
0.125
0.132
1,3-Dichloropropane
0.125
0.115
0.123
cis-1,3-Dichloropropene
0.125
0.116
0.125
trans-1,3-Dichloropropene
0.125
0.117
0.124
2,2-Dichloropropane
0.125
0.104
0.109
Di -isopropyl ether
0.125
0.129
0.133
Ethylbenzene
0.125
0.113
0.124
Hexachloro-1,3-butadiene
0.125
0.104
0.104
Isopropylbenzene
0.125
0.110
0.122
p-Isopropyltoluene
0.125
0.126
0.131
2-Butanone (MEK)
0.625
0.698
0.706
Methylene Chloride
0.125
0.107
0.112
4-Methyl-2-pentanone (MIBK)
0.625
0.654
0.680
Methyl tert-butyl ether
0.125
0.102
0.109
Naphthalene
0.125
0.112
0.119
ACCOUNT:
Withers & Ravenel Eng. - Standard
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
88.0
96.8
56.0-147
9.52
20
92.8
104
68.0-135
11.4
20
102
106
74.0-130
3.83
20
81.6
98.4
75.0-127
18.7
20
88.0
95.2
66.0-128
7.86
20
92.0
94.4
76.0-128
2.58
20
83.2
86.4
74.0-127
3.77
20
94.4
97.6
61.0-134
3.33
20
92.8
98.4
72.0-123
5.86
20
113
126
51.0-138
10.7
20
102
105
75.0-124
3.10
20
102
108
75.0-124
6.11
20
77.7
83.2
59.0-130
6.86
20
85.6
92.0
74.0-128
7.21
20
89.6
95.2
75.0-122
6.06
20
95.2
106
76.0-124
10.4
20
96.0
102
76.0-125
5.67
20
98.4
102
77.0-121
3.98
20
71.5
79.8
43.0-156
10.9
20
92.0
100
70.0-127
8.33
20
96.0
101
65.0-131
4.88
20
93.6
101
65.0-131
7.41
20
84.0
92.0
73.0-125
9.09
20
84.0
92.0
71.0-125
9.09
20
84.8
92.8
74.0-125
9.01
20
100
106
73.0-125
5.45
20
92.0
98.4
80.0-125
6.72
20
92.8
100
76.0-127
7.47
20
93.6
99.2
73.0-127
5.81
20
83.2
87.2
59.0-135
4.69
20
103
106
60.0-136
3.05
20
90.4
99.2
74.0-126
9.28
20
83.2
83.2
57.0-150
0.000
20
88.0
97.6
72.0-127
10.3
20
101
105
72.0-133
3.89
20
112
113
30.0-160
1.14
24
85.6
89.6
68.0-123
4.57
20
105
109
56.0-143
3.90
20
81.6
87.2
66.0-132
6.64
20
89.6
95.2
59.0-130
6.06
20
PROJECT:
SDG:
DATE/TIME: PAGE:
23-0302
L1616119
06/06/23 12:28 101 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2063443 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1616119-06,07,08,09,10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3928086-1 05/19/2312:10 • (LCSD) R3928086-2 05/19/2312:31
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/kg
mg/kg
mg/kg
%
%
%
%
%
n-Propylbenzene
0.125
0.132
0.136
106
109
74.0-126
2.99
20
Styrene
0.125
0.103
0.110
82.4
88.0
72.0-127
6.57
20
1,1,1,2-Tetrachloroethane
0.125
0.102
0.110
81.6
88.0
74.0-129
7.55
20
1,1,2,2-Tetrachloroethane
0.125
0.122
0.128
97.6
102
68.0-128
4.80
20
Tetrachloroethene
0.125
0.122
0.128
97.6
102
70.0-136
4.80
20
Toluene
0.125
0.113
0.121
90.4
96.8
75.0-121
6.84
20
1,2,3-Trichlorobenzene
0.125
0.116
0.125
92.8
100
59.0-139
7.47
20
1,2,4-Trichlorobenzene
0.125
0.105
0.114
84.0
91.2
62.0-137
8.22
20
1,1,1-Trichloroethane
0.125
0.106
0.118
84.8
94.4
69.0-126
10.7
20
1,1,2-Trichloroethane
0.125
0.115
0.127
92.0
102
78.0-123
9.92
20
1,1,2-Trichlorotrifluoroethane
0.125
0.107
0.116
85.6
92.8
61.0-139
8.07
20
Trichloroethene
0.125
0.113
0.122
90.4
97.6
76.0-126
7.66
20
Trichlorofluoromethane
0.125
0.112
0.123
89.6
98.4
61.0-142
9.36
20
1,2,3-Trichloropropane
0.125
0.130
0.135
104
108
67.0-129
3.77
20
1,2,4-Trimethylbenzene
0.125
0.122
0.129
97.6
103
70.0-126
5.58
20
1,3,5-Trimethyl benzene
0.125
0.123
0.134
98.4
107
73.0-127
8.56
20
Vinyl chloride
0.125
0.107
0.117
85.6
93.6
63.0-134
8.93
20
Xylenes, Total
0.375
0.335
0.360
89.3
96.0
72.0-127
7.19
20
(S) Toluene-d8
105
105
75.0-131
(S) 4-Bromof/uorobenzene
91.9
93.6
67.0-138
(S)1,2-Dich/oroethane-d4
118
118
70.0-130
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 102 of 132

WG2064295
Volatile Organic Compounds (GC/MS) by Method 8260D
QUALITY CONTROL SUMMARY
L1616119-11
Method Blank (MB)
(MB) R3928239-2 05/22/23 08:54
MB Result MB Qualifier
Analyte mg/kg
Acetone
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec -Butyl benzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MB MDL
mg/kg
0.0365
0.00361
0.000467
0.000900
0.000725
0.00117
0.00197
0.00525
0.00288
0.00195
0.000898
0.000210
0.000612
0.00170
0.00103
0.00435
0.000865
0.000450
0.00390
0.000648
0.000750
0.000425
0.000600
0.000700
0.00161
0.000491
0.000649
0.000606
0.000734
0.00104
0.00142
0.000809
0.000501
0.000757
0.00114
0.00138
0.000410
0.000737
0.00600
0.000425
MB RDL
mg/kg
0.0500
0.0125
0.00100
0.0125
0.00250
0.0250
0.0125
0.0125
0.0125
0.00500
0.00500
0.00250
0.00250
0.00500
0.00250
0.0125
0.00250
0.00500
0.0250
0.00250
0.00500
0.00500
0.00500
0.00500
0.00250
0.00250
0.00250
0.00250
0.00250
0.00500
0.00500
0.00250
0.00500
0.00250
0.00500
0.00250
0.00100
0.00250
0.0250
0.00250
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 103 of 132

WG2064295
Volatile Organic Compounds (GC/MS) by Method 8260D
QUALITY CONTROL SUMMARY
L1616119-11
Method Blank (MB)
(MB) R3928239-2 05/22/23 08:54
MB Result
Analyte mg/kg
p-Isopropyltoluene
U
2-Butanone (MEK)
U
Methylene Chloride
0.00833
4-Methyl-2-pentanone (MIBK)
U
Methyl tert-butyl ether
U
Naphthalene
U
n-Propylbenzene
U
Styrene
0.00125
1,1,1,2-Tetrachloroethane
U
1,1,2,2-Tetrachloroethane
U
Tetrachloroethene
U
Toluene
U
1,2,3-Trichlorobenzene
U
1,2,4-Trichlorobenzene
U
1,1,1-Trichloroethane
U
1,1,2-Trichloroethane
U
1,1,2-Trichlorotrifluoroethane
U
Trichloroethene
U
Trichlorofluoromethane
U
1,2,3-Trichloropropane
U
1,2,4-Trimethylbenzene
U
1,3,5-Trimethyl benzene
U
Vinyl chloride
U
Xylenes, Total
U
(S) Toluene-d8
107
(S) 4-Bromofluorobenzene
93.8
(S)1,2-Dich/oroethone-d4
874
MB Qualifier MB MDL
mg/kg
MB RDL
mg/kg
0.00255
0.00500
0.0635
0.100
J 0.00664
0.0250
0.00228
0.0250
0.000350
0.00100
0.00488
0.0125
0.000950
0.00500
J 0.000229
0.0125
0.000948
0.00250
0.000695
0.00250
0.000896
0.00250
0.00130
0.00500
0.00733
0.0125
0.00440
0.0125
0.000923
0.00250
0.000597
0.00250
0.000754
0.00250
0.000584
0.00100
0.000827
0.00250
0.00162
0.0125
0.00158
0.00500
0.00200
0.00500
0.00116
0.00250
Laboratory Control Sample (LCS)
(LCS) R3928239-1 05/22/23 07:38
Spike Amount
Analyte
mg/kg
Acetone
0.625
Acrylonitrile
0.625
Benzene
0.125
Bromobenzene
0.125
Bromodichloromethane
0.125
Bromoform
0.125
LCS Result
mg/kg
0.442
0.748
0.120
0.109
0.123
0.104
ACCOUNT:
Withers & Ravenel Eng. - Standard
0.000880 0.00650
75.0-131
67.0-138
70.0-130
LCS Rec.
Rec. Limits LCS Qualifier
70.7
10.0-160
120
45.0-153
96.0
70.0-123
87.2
73.0-121
98.4
73.0-121
83.2
64.0-132
PROJECT:
23-0302
SDG:
L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
104 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2064295 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1616119-11
Laboratory Control Sample (LCS)
(LCS) R3928239-1 05/22/23 07:38
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/kg
mg/kg
%
%
Bromomethane
0.125
0.132
106
56.0-147
n-Butylbenzene
0.125
0.113
90.4
68.0-135
sec -Butyl benzene
0.125
0.115
92.0
74.0-130
tert-Butylbenzene
0.125
0.113
90.4
75.0-127
Carbon tetrachloride
0.125
0.106
84.8
66.0-128
Chlorobenzene
0.125
0.116
92.8
76.0-128
Chlorodibromomethane
0.125
0.104
83.2
74.0-127
Chloroethane
0.125
0.137
110
61.0-134
Chloroform
0.125
0.116
92.8
72.0-123
Chloromethane
0.125
0.144
115
51.0-138
2-Chlorotoluene
0.125
0.107
85.6
75.0-124
4-Chlorotoluene
0.125
0.0962
77.0
75.0-124
1,2-Dibromo-3-Chloropropane
0.125
0.109
87.2
59.0-130
1,2-Dibromoethane
0.125
0.111
88.8
74.0-128
Dibromomethane
0.125
0.111
88.8
75.0-122
1,2-Dichlorobenzene
0.125
0.109
87.2
76.0-124
1,3-Dichlorobenzene
0.125
0.108
86.4
76.0-125
1,4-Dichlorobenzene
0.125
0.107
85.6
77.0-121
Dichlorodifluoromethane
0.125
0.101
80.8
43.0-156
1,1-Dichloroethane
0.125
0.112
89.6
70.0-127
1,2-Dichloroethane
0.125
0.121
96.8
65.0-131
1,1-Dichloroethene
0.125
0.115
92.0
65.0-131
cis-1,2-Dichloroethene
0.125
0.116
92.8
73.0-125
trans-1,2-Dichloroethene
0.125
0.120
96.0
71.0-125
1,2-Dichloropropane
0.125
0.115
92.0
74.0-125
1,1-Dichloropropene
0.125
0.115
92.0
73.0-125
1,3-Dichloropropane
0.125
0.118
94.4
80.0-125
cis-1,3-Dichloropropene
0.125
0.117
93.6
76.0-127
trans-1,3-Dichloropropene
0.125
0.114
91.2
73.0-127
2,2-Dichloropropane
0.125
0.114
91.2
59.0-135
Di -isopropyl ether
0.125
0.118
94.4
60.0-136
Ethylbenzene
0.125
0.113
90.4
74.0-126
Hexachloro-1,3-butadiene
0.125
0.130
104
57.0-150
Isopropylbenzene
0.125
0.109
87.2
72.0-127
p-Isopropyltoluene
0.125
0.109
87.2
72.0-133
2-Butanone (MEK)
0.625
0.655
105
30.0-160
Methylene Chloride
0.125
0.123
98.4
68.0-123
4-Methyl-2-pentanone (MIBK)
0.625
0.641
103
56.0-143
Methyl tert-butyl ether
0.125
0.108
86.4
66.0-132
Naphthalene
0.125
0.117
93.6
59.0-130
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard
23-0302 L1616119 06/06/23 12:28 105 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2064295
Volatile Organic Compounds (GC/MS) by Method 8260D
QUALITY CONTROL SUMMARY
L1616119-11
Laboratory Control Sample (LCS)
(LCS) R3928239-1 05/22/23 07:38
Spike Amount
Analyte mg/kg
LCS Result
mg/kg
n-Propylbenzene
0.125
0.111
Styrene
0.125
0.0994
1,1,1,2-Tetrachloroethane
0.125
0.105
1,1,2,2-Tetrachloroethane
0.125
0.112
Tetrachloroethene
0.125
0.118
Toluene
0.125
0.113
1,2,3-Trichlorobenzene
0.125
0.115
1,2,4-Trichlorobenzene
0.125
0.113
1,1,1-Trichloroethane
0.125
0.111
1,1,2-Trichloroethane
0.125
0.121
1,1,2-Trichlorotrifluoroethane
0.125
0.113
Trichloroethene
0.125
0.122
Trichlorofluoromethane
0.125
0.122
1,2,3-Trichloropropane
0.125
0.115
1,2,4-Trimethylbenzene
0.125
0.106
1,3,5-Trimethyl benzene
0.125
0.110
Vinyl chloride
0.125
0.140
Xylenes, Total
0.375
0.328
(S) Toluene-d8
(S) 4-Bromof/uorobenzene
(S) 1,2-Dich/oroethane-d4
LCS Rec. Rec. Limits LCS Qualifier
88.8
74.0-126
79.5
72.0-127
84.0
74.0-129
89.6
68.0-128
94.4
70.0-136
90.4
75.0-121
92.0
59.0-139
90.4
62.0-137
88.8
69.0-126
96.8
78.0-123
90.4
61.0-139
97.6
76.0-126
97.6
61.0-142
92.0
67.0-129
84.8
70.0-126
88.0
73.0-127
112
63.0-134
87.5
72.0-127
102
75.0-131
96.8
67.0-138
93.1
70.0-130
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 106 of 132

WG2059503
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
QUALITY CONTROL SUMMARY
L1616119-12,13,14,15,16,17
Method Blank (MB)
(MB) R3927842-2 05/16/23 23:39
MB Result
Analyte
ug/I
Acenaphthene
U
Acenaphthylene
U
Anthracene
U
Benzidine
U
Benzo(a)anth race ne
U
Benzo(b)fluoranthene
U
Benzo(k)fluoranthene
U
Benzo(g,h,i)perylene
U
Benzo(a)pyrene
U
Bis(2-chlorethoxy)methane
U
Bis(2-chloroethyl)ether
U
2,2-Oxybis(1-Chloropropane)
U
4-Bromophenyl-phenylether
U
2-Chloronaphthalene
U
4-Chlorophenyl-phenylether
U
Chrysene
U
Dibenz(a,h)anthracene
U
3,3-Dichlorobenzidine
U
2,4-Dinitrotoluene
U
2,6-Dinitrotoluene
U
Fluoranthene
U
Fluorene
0.0859
Hexachlorobenzene
U
Hexachloro-1,3-butadiene
U
Hexachlorocyclopentadiene
U
Hexachloroethane
U
Indeno(1,2,3-cd)pyrene
U
Isophorone
U
Naphthalene
U
Nitrobenzene
U
n-Nitrosodimethyla mine
U
n-Nitrosodiphenylamine
U
n-Nitrosodi-n-propylamine
U
Phenanthrene
U
Benzylbutyl phthalate
U
Bis(2-ethylhexyl)phthalate
U
Di-n-butyl phthalate
0.546
Diethyl phthalate
U
Dimethyl phthalate
U
Di-n-octyl phthalate
U
MB Qualifier MB MDL
ug/I
MB RDL
ug/I
0.0886
1.00
0.0921
1.00
0.0804
1.00
3.74
10.0
0.199
1.00
0.130
1.00
0.120
1.00
0.121
1.00
0.0381
1.00
0.116
10.0
0.137
10.0
0.210
10.0
0.0877
10.0
0.0648
1.00
0.0926
10.0
0.130
1.00
0.0644
1.00
0.212
10.0
0.0983
10.0
0.250
10.0
0.102
1.00
J 0.0844
1.00
0.0755
1.00
0.0968
10.0
0.0598
10.0
0.127
10.0
0.279
1.00
0.143
10.0
0.159
1.00
0.297
10.0
0.998
10.0
2.37
10.0
0.261
10.0
0.112
1.00
0.765
3.00
0.895
3.00
J 0.453
3.00
0.287
3.00
0.260
3.00
0.932
3.00
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 107 of 132

WG2059503
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
QUALITY CONTROL SUMMARY
L1616119-12,13,14,15,16,17
Method Blank (MB)
(MB) R3927842-2 05/16/23 23:39
MB Result
Analyte
ug/I
Pyrene
U
1,2,4-Trichlorobenzene
U
4-ChIoro-3-methyl phenol
U
2-Chlorophenol
U
2,4-Dichlorophenol
U
2,4-Dimethylphenol
U
4,6-Dinitro-2-methylphenol
U
2,4-Dinitrophenol
U
2-Nitrophenol
U
4-Nitrophenol
U
Pentachlorophenol
U
Phenol
U
2,4,6-Trichlorophenol
U
(S) Nitrobenzene-d5
63.5
(S) 2-Fluorobiphenyl
59.6
(S) p-Terphenyl-d14
70.1
(S) Phenol-d5
21.0
(S) 2-F/uorophenol
31.8
(S)2,4,6-Tribromopheno/ 56.5
MB Qualifier MB MDL MB RDL
ug/I ug/I
Laboratory Control Sample (LCS)
(LCS) R3927842-1 05/16/23 23:17
Spike Amount
LCS Result
Analyte
ug/I
ug/I
Acenaphthene
50.0
45.1
Acenaphthylene
50.0
49.0
Anthracene
50.0
46.7
Benzidine
100
7.23
Benzo(a)anth race ne
50.0
49.2
Benzo(b)fluoranthene
50.0
46.3
Benzo(k)fluoranthene
50.0
46.3
Benzo(g,h,i)perylene
50.0
50.7
Benzo(a)pyrene
50.0
46.5
Bis(2-chlorethoxy)methane
50.0
42.0
Bis(2-chloroethyl)ether
50.0
45.4
2,2-Oxybis(1-Chloropropane)
50.0
41.8
4-Bromophenyl-phenylether
50.0
41.2
2-Chloronaphthalene
50.0
44.3
0.107
0.0698
0.131
0.133
0.102
0.0636
1.12
5.93
0.117
0.143
0.313
4.33
0.100
LCS Rec
90.2
98.0
93.4
7.23
98.4
92.6
92.6
101
93.0
84.0
90.8
83.6
82.4
88.6
1.00
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
15.0-314
22.0-127
29.0-141
8.00-424
10.0-120
10.0-153
Rec. Limits
47.0-145
33.0-145
27.0-133
1.00-120
33.0-143
24.0-159
11.0-162
1.00-219
17.0-163
1.00-219
33.0-185
36.0-166
53.0-127
60.0-120
LCS Qualifier
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 108 of 132

WG2059503 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1616119-12,13,14,15,16,17
Laboratory Control Sample (LCS)
(LCS) R3927842-1 05/16/23 23:17
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
%
%
4-Chlorophenyl-phenylether
50.0
42.2
84.4
25.0-158
Chrysene
50.0
48.7
97.4
17.0-168
Dibenz(a,h)anthracene
50.0
54.5
109
1.00-227
3,3-Dichlorobenzidine
100
92.4
92.4
1.00-262
2,4-Dinitrotoluene
50.0
52.5
105
39.0-139
2,6-Dinitrotoluene
50.0
51.1
102
50.0-158
Fluoranthene
50.0
49.0
98.0
26.0-137
Fluorene
50.0
45.9
91.8
59.0-121
Hexachlorobenzene
50.0
40.1
80.2
1.00-152
Hexachloro-1,3-butadiene
50.0
32.5
65.0
24.0-120
Hexachlorocyclopentadiene
50.0
21.4
42.8
10.0-120
Hexachloroethane
50.0
39.9
79.8
40.0-120
Indeno(1,2,3-cd)pyrene
50.0
50.7
101
1.00-171
Isophorone
50.0
41.5
83.0
21.0-196
Naphthalene
50.0
39.2
78.4
21.0-133
Nitrobenzene
50.0
42.8
85.6
35.0-180
n-Nitrosodimethyla mine
50.0
36.6
73.2
10.0-120
n-Nitrosodiphenylamine
50.0
44.9
89.8
44.0-120
n-Nitrosodi-n-propylamine
50.0
44.6
89.2
1.00-230
Phenanthrene
50.0
46.2
92.4
54.0-120
Benzylbutyl phthalate
50.0
57.1
114
1.00-152
Bis(2-ethylhexyl)phthalate
50.0
57.0
114
8.00-158
Di-n-butyl phthalate
50.0
57.0
114
1.00-120
Diethyl phthalate
50.0
50.4
101
1.00-120
Dimethyl phthalate
50.0
48.1
96.2
1.00-120
Di-n-octyl phthalate
50.0
54.2
108
4.00-146
Pyrene
50.0
48.8
97.6
52.0-120
1,2,4-Trichlorobenzene
50.0
35.8
71.6
44.0-142
4-Chloro-3-methylphenol
50.0
31.4
62.8
22.0-147
2-Chlorophenol
50.0
30.5
61.0
23.0-134
2,4-Dichlorophenol
50.0
32.6
65.2
39.0-135
2,4-Dimethylphenol
50.0
32.3
64.6
32.0-120
4,6-Dinitro-2-methylphenol
50.0
58.0
116
1.00-181
2,4-Dinitrophenol
50.0
54.5
109
1.00-191
2-Nitrophenol
50.0
42.5
85.0
29.0-182
4-Nitrophenol
50.0
12.0
24.0
1.00-132
Pentachlorophenol
50.0
38.8
77.6
14.0-176
Phenol
50.0
16.5
33.0
5.00-120
2,4,6-Trichlorophenol
50.0
42.1
84.2
37.0-144
(S) Nitrobenzene-d5
79.2
15.0-314
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard
23-0302 L1616119 06/06/23 12:28 109 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2059503 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1616119-12,13,14,15,16,17
Laboratory Control Sample (LCS)
(LCS) R3927842-1 05/16/23 23:17
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
LCS Qualifier
Analyte
ug/I
ug/I
%
%
(S) 2-Fluorobipheny/
88.3
22.0-127
(S) p-Terphenyl-d14
86.9
29.0-141
(S) Phenol-d5
29.3
8.00-424
(S) 2-F/uorophenol
40.5
10.0-120
(S) 2,4,6-Tribromopheno/
80.0
10.0-153
L1615956-01 Original
Sample (OS) • Matrix
Spike (MS) • Matrix Spike Duplicate
(MSD)
(OS) L1615956-01 05/17/23 04:17 • (MS) R3927842-3 05/17/23 04:38 • (MSD) R3927842-4 05/17/23 05:00
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec. Dilution
Rec. Limits
MS Qualifier
MSD Qualifier RPD
RPD Limits
Analyte
ug/I
ug/I
ug/I
ug/I
%
%
%
%
%
Acenaphthene
50.0
U
37.3
32.9
74.6
65.8 1
47.0-145
12.5
48
Acenaphthylene
50.0
U
37.6
32.9
75.2
65.8 1
33.0-145
13.3
74
Anthracene
50.0
U
34.1
30.3
68.2
60.6 1
27.0-133
11.8
66
Benzidine
100
U
U
U
0.000
0.000 1
1.00-120
J6
J6 0.000
40
Benzo(a)anth race ne
50.0
U
34.9
29.1
69.8
58.2 1
33.0-143
18.1
53
Benzo(b)fluoranthene
50.0
U
35.3
27.6
70.6
55.2 1
24.0-159
24.5
71
Benzo(k)fluoranthene
50.0
U
33.3
26.5
66.6
53.0 1
11.0-162
22.7
63
Benzo(g,h,i)perylene
50.0
U
36.2
27.2
72.4
54.4 1
1.00-219
28.4
97
Benzo(a)pyrene
50.0
U
32.4
27.0
64.8
54.0 1
17.0-163
18.2
72
Bis(2-chlorethoxy)methane
50.0
U
42.2
34.4
84.4
68.8 1
33.0-184
20.4
54
Bis(2-chloroethyl)ether
50.0
U
50.2
35.1
100
70.2 1
12.0-158
35.4
108
2,2-Oxybis(1-Chloropropane)
50.0
U
36.7
29.7
73.4
59.4 1
36.0-166
21.1
76
4-Bromophenyl-phenylether
50.0
U
44.3
29.1
88.6
58.2 1
53.0-127
41.4
43
2-Chloronaphthalene
50.0
U
29.0
29.5
58.0
59.0 1
60.0-120
J6
J6 1.71
24
4-Chlorophenyl-phenylether
50.0
U
27.1
30.7
54.2
61.4 1
25.0-158
12.5
61
Chrysene
50.0
U
35.4
28.7
70.8
57.4 1
17.0-168
20.9
87
Dibenz(a,h)anthracene
50.0
U
37.1
27.7
74.2
55.4 1
1.00-227
29.0
126
3,3-Dichlorobenzidine
100
U
U
U
0.000
0.000 1
1.00-262
J6
J6 0.000
108
2,4-Dinitrotoluene
50.0
U
U
40.5
0.000
81.0 1
39.0-139
J6
J3 200
42
2,6-Dinitrotoluene
50.0
U
42.9
33.6
85.8
67.2 1
50.0-158
24.3
48
Fluoranthene
50.0
U
36.4
31.8
72.8
63.6 1
26.0-137
13.5
66
Fluorene
50.0
0.626
40.6
34.1
79.9
66.9 1
59.0-121
17.4
38
Hexachlorobenzene
50.0
U
31.3
26.7
62.6
53.4 1
1.00-152
15.9
55
Hexachloro-1,3-butadiene
50.0
U
32.1
25.8
64.2
51.6 1
24.0-120
21.8
62
Hexachlorocyclopentadiene
50.0
U
17.9
20.9
35.8
41.8 1
10.0-146
15.5
34
Hexachloroethane
50.0
U
136
36.3
272
72.6 1
40.0-120
J5
J3 116
52
Indeno(1,2,3-cd)pyrene
50.0
U
33.9
25.4
67.8
50.8 1
1.00-171
28.7
99
Isophorone
50.0
U
67.3
36.9
135
73.8 1
21.0-196
58.3
93
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
PAGE:
110 of 132

WG2059503 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1616119-12,13,14,15,16,17
L1615956-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1615956-01 05/17/23 04:17 • (MS) R3927842-3 05/17/23 04:38 • (MSD) R3927842-4 05/17/23 05:00
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/I
ug/I
ug/I
%
%
Naphthalene
50.0
U
53.8
33.9
108
67.8
Nitrobenzene
50.0
U
51.0
44.7
102
89.4
n-Nitrosodimethyla mine
50.0
U
27.4
28.3
54.8
56.6
n-Nitrosodiphenyla mine
50.0
U
90.3
33.3
181
66.6
n-Nitrosodi-n-propylamine
50.0
U
U
34.6
0.000
69.2
Phenanthrene
50.0
0.284
48.4
33.8
96.2
67.0
Benzylbutyl phthalate
50.0
U
46.7
39.3
93.4
78.6
Bis(2-ethylhexyl)phthalate
50.0
U
38.8
31.1
77.6
62.2
Di-n-butyl phthalate
50.0
U
42.4
39.0
84.8
78.0
Diethyl phthalate
50.0
U
33.0
42.5
66.0
85.0
Dimethyl phthalate
50.0
U
31.1
36.6
62.2
73.2
Di-n-octyl phthalate
50.0
U
39.9
32.0
79.8
64.0
Pyrene
50.0
U
39.1
33.0
78.2
66.0
1,2,4-Trichlorobenzene
50.0
U
30.1
28.5
60.2
57.0
4-ChIoro-3-methyl phenol
50.0
U
26.8
26.0
53.6
52.0
2-Chlorophenol
50.0
U
23.2
22.1
46.4
44.2
2,4-Dichlorophenol
50.0
U
44.4
24.6
88.8
49.2
2,4-Dimethylphenol
50.0
U
31.3
25.7
62.6
51.4
4,6-Dinitro-2-methylphenol
50.0
U
43.9
34.2
87.8
68.4
2,4-Dinitrophenol
50.0
U
35.5
40.5
71.0
81.0
2-Nitrophenol
50.0
U
57.6
39.2
115
78.4
4-Nitrophenol
50.0
U
U
15.2
0.000
30.4
Pentachlorophenol
50.0
U
27.9
26.6
55.8
53.2
Phenol
50.0
U
12.1
12.0
24.2
24.0
2,4,6-Trichlorophenol
50.0
U
38.3
28.3
76.6
56.6
(S) Nitrobenzene-d5
0.000
64.4
(S) 2-Fluorobiphenyl
54.2
65.6
(S) p-Terphenyl-d14
64.4
54.2
(S) Phenol-d5
20.3
24.8
(S) 2-F/uorophenol
29.4
30.6
(S)2,4,6-Tribromopheno/
58.0
47.9
Dilution Rec. Limits MS Qualifier MSD Qualifier
1 21.0-133
1 35.0-180
1 10.0-120
1 16.0-160
1 1.00-230
1 54.0-120
1 1.00-152
1 8.00-158
1 1.00-120
1 1.00-120
1 1.00-120
1 4.00-146
1 52.0-120
1 44.0-142
1 22.0-147
1 23.0-134
1 39.0-135
1 32.0-120
1 1.00-181
1 1.00-191
1 29.0-182
1 1.00-132
1 14.0-176
1 5.00-120
1 37.0-144
15.0-314
22.0-127
29.0-141
8.00-424
10.0-120
10.0-153
J5 J3
J6 J3
J3
J6 J3
J2
RPD
45.4
13.2
3.23
92.2
200
35.5
17.2
22.0
8.35
25.2
16.2
22.0
16.9
5.46
3.03
4.86
57.4
19.6
24.8
13.2
38.0
200
4.77
0.830
30.0
RPD Limits
65
62
40
28
87
39
60
82
47
100
183
69
49
50
73
61
50
58
203
132
55
131
86
64
58
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT:
Withers & Ravenel Eng. - Standard 23-0302
SDG: DATE/TIME: PAGE:
L1616119 06/06/23 12:28 111 of 132

WG2061246
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
QUALITY CONTROL SUMMARY
L1616119-18,19,20,21,22
Method Blank (MB)
(MB) R3928852-2 05/20/23 00:37
MB Result
Analyte
ug/I
Acenaphthene
U
Acenaphthylene
U
Anthracene
U
Benzidine
U
Benzo(a)anth race ne
U
Benzo(b)fluoranthene
U
Benzo(k)fluoranthene
U
Benzo(g,h,i)perylene
U
Benzo(a)pyrene
U
Bis(2-chlorethoxy)methane
U
Bis(2-chloroethyl)ether
U
2,2-Oxybis(1-Chloropropane)
U
4-Bromophenyl-phenylether
U
2-Chloronaphthalene
U
4-Chlorophenyl-phenylether
U
Chrysene
U
Dibenz(a,h)anthracene
U
3,3-Dichlorobenzidine
U
2,4-Dinitrotoluene
U
2,6-Dinitrotoluene
U
Fluoranthene
U
Fluorene
U
Hexachlorobenzene
U
Hexachloro-1,3-butadiene
U
Hexachlorocyclopentadiene
U
Hexachloroethane
U
Indeno(1,2,3-cd)pyrene
U
Isophorone
U
Naphthalene
U
Nitrobenzene
U
n-Nitrosodimethyla mine
U
n-Nitrosodiphenylamine
U
n-Nitrosodi-n-propylamine
U
Phenanthrene
U
Benzylbutyl phthalate
U
Bis(2-ethylhexyl)phthalate
U
Di-n-butyl phthalate
U
Diethyl phthalate
U
Dimethyl phthalate
U
Di-n-octyl phthalate
U
MB Qualifier MB MDL
ug/I
MB RDL
ug/I
0.0886
1.00
0.0921
1.00
0.0804
1.00
3.74
10.0
0.199
1.00
0.130
1.00
0.120
1.00
0.121
1.00
0.0381
1.00
0.116
10.0
0.137
10.0
0.210
10.0
0.0877
10.0
0.0648
1.00
0.0926
10.0
0.130
1.00
0.0644
1.00
0.212
10.0
0.0983
10.0
0.250
10.0
0.102
1.00
0.0844
1.00
0.0755
1.00
0.0968
10.0
0.0598
10.0
0.127
10.0
0.279
1.00
0.143
10.0
0.159
1.00
0.297
10.0
0.998
10.0
2.37
10.0
0.261
10.0
0.112
1.00
0.765
3.00
0.895
3.00
0.453
3.00
0.287
3.00
0.260
3.00
0.932
3.00
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 112 of 132

WG2061246
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
QUALITY CONTROL SUMMARY
L1616119-18,19,20,21,22
Method Blank (MB)
(MB) R3928852-2 05/20/23 00:37
MB Result
Analyte
ug/I
Pyrene
U
1,2,4-Trichlorobenzene
U
4-ChIoro-3-methyl phenol
U
2-Chlorophenol
U
2,4-Dichlorophenol
U
2,4-Dimethylphenol
U
4,6-Dinitro-2-methylphenol
U
2,4-Dinitrophenol
U
2-Nitrophenol
U
4-Nitrophenol
U
Pentachlorophenol
U
Phenol
U
2,4,6-Trichlorophenol
U
(S) Nitrobenzene-d5
110
(S) 2-Fluorobiphenyl
79.8
(S) p-Terphenyl-d14
95.6
(S) Phenol-d5
23.5
(S) 2-F/uorophenol
37.4
(S)2,4,6-Tribromopheno/ 82.0
MB Qualifier MB MDL MB RDL
ug/I ug/I
Laboratory Control Sample (LCS)
(LCS) R3928852-1 05/20/23 00:15
Spike Amount
LCS Result
Analyte
ug/I
ug/I
Acenaphthene
50.0
41.8
Acenaphthylene
50.0
41.0
Anthracene
50.0
44.0
Benzidine
100
57.6
Benzo(a)anth race ne
50.0
46.3
Benzo(b)fluoranthene
50.0
49.7
Benzo(k)fluoranthene
50.0
45.5
Benzo(g,h,i)perylene
50.0
41.9
Benzo(a)pyrene
50.0
52.8
Bis(2-chlorethoxy)methane
50.0
45.5
Bis(2-chloroethyl)ether
50.0
41.1
2,2-Oxybis(1-Chloropropane)
50.0
37.0
4-Bromophenyl-phenylether
50.0
49.7
2-Chloronaphthalene
50.0
41.1
0.107
0.0698
0.131
0.133
0.102
0.0636
1.12
5.93
0.117
0.143
0.313
4.33
0.100
LCS Rec
83.6
82.0
88.0
57.6
92.6
99.4
91.0
83.8
106
91.0
82.2
74.0
99.4
82.2
1.00
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
15.0-314
22.0-127
29.0-141
8.00-424
10.0-120
10.0-153
Rec. Limits
47.0-145
33.0-145
27.0-133
1.00-120
33.0-143
24.0-159
11.0-162
1.00-219
17.0-163
1.00-219
33.0-185
36.0-166
53.0-127
60.0-120
LCS Qualifier
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 113 of 132

WG2061246
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
QUALITY CONTROL SUMMARY
L1616119-18,19,20,21,22
Laboratory Control Sample (LCS)
(LCS) R3928852-1 05/20/23 00:15
Spike Amount
Analyte ug/I
4-Chlorophenyl-phenylether
Chrysene
Dibenz(a,h)anthracene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethyla mine
n-Nitrosodiphenylamine
n-N itros o d i-n-p ro pyl a m i n e
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha late
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-methyl phen of
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
(S) Nitrobenzene-d5
50.0
50.0
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
LCS Result
ug/I
49.4
42.9
42.2
92.1
47.0
40.9
45.9
42.7
47.8
57.7
41.0
41.8
40.2
52.6
38.2
51.3
32.2
41.1
49.6
42.6
44.6
45.8
47.7
47.4
44.7
40.4
44.3
42.7
48.0
31.6
42.1
47.9
42.2
38.3
38.8
116
37.9
14.1
45.0
LCS Rec. Rec. Limits
98.8
85.8
84.4
92.1
94.0
81.8
91.8
85.4
95.6
115
82.0
83.6
80.4
105
76.4
103
64.4
82.2
99.2
85.2
89.2
91.6
95.4
94.8
89.4
80.8
88.6
85.4
96.0
63.2
84.2
95.8
84.4
76.6
77.6
232
75.8
28.2
90.0
102
25.0-158
17.0-168
1.00-227
1.00-262
39.0-139
50.0-158
26.0-137
59.0-121
1.00-152
24.0-120
10.0-120
40.0-120
1.00-171
21.0-196
21.0-133
35.0-180
10.0-120
44.0-120
1.00-230
54.0-120
1.00-152
8.00-158
1.00-120
1.00-120
1.00-120
4.00-146
52.0-120
44.0-142
22.0-147
23.0-134
39.0-135
32.0-120
1.00-181
1.00-191
29.0-182
1.00-132
14.0-176
5.00-120
37.0-144
15.0-314
LCS Qualifier
J4
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 114 of 132

WG2061246 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1616119-18,19,20,21,22
Laboratory Control Sample (LCS)
(LCS) R3928852-1 05/20/23 00:15
Spike Amount LCS Result LCS Rec.
Analyte ug/I ug/I %
(S) 2-Fluorobipheny/ 83.5
(S) p-Terphenyl-d14 87.2
(S) Phenol-d5 22.1
(S) 2-F/uorophenol 33.8
(S) 2,4,6-Tribromopheno/ 88.0
Rec. Limits LCS Qualifier
22.0-127
29.0-141
8.00-424
10.0-120
10.0-153
L1616738-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1616738-01 05/20/23 05:13 • (MS) R3928852-3 05/20/23 05:34 • (MSD) R3928852-4 05/20/23 05:55
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/I
ug/I
ug/I
%
%
Acenaphthene
50.0
U
31.5
32.2
63.0
64.4
Acenaphthylene
50.0
U
32.0
33.0
64.0
66.0
Anthracene
50.0
U
35.5
38.0
71.0
76.0
Benzidine
100
U
U
U
0.000
0.000
Benzo(a)anth race ne
50.0
U
38.9
42.3
77.8
84.6
Benzo(b)fluoranthene
50.0
U
40.3
42.8
80.6
85.6
Benzo(k)fluoranthene
50.0
U
35.1
39.2
70.2
78.4
Benzo(g,h,i)perylene
50.0
U
43.4
46.9
86.8
93.8
Benzo(a)pyrene
50.0
U
43.7
47.1
87.4
94.2
Bis(2-chlorethoxy)methane
50.0
U
33.1
32.7
66.2
65.4
Bis(2-chloroethyl)ether
50.0
U
28.2
27.3
56.4
54.6
2,2-Oxybis(1-Chloropropane)
50.0
U
23.1
23.1
46.2
46.2
4-Bromophenyl-phenylether
50.0
U
40.7
44.2
81.4
88.4
2-Chloronaphthalene
50.0
U
37.9
37.9
75.8
75.8
4-Chlorophenyl-phenylether
50.0
U
37.7
38.3
75.4
76.6
Chrysene
50.0
U
38.7
41.5
77.4
83.0
Dibenz(a,h)anthracene
50.0
U
42.7
45.4
85.4
90.8
3,3-Dichlorobenzidine
100
U
61.7
61.2
61.7
61.2
2,4-Dinitrotoluene
50.0
U
36.2
38.5
72.4
77.0
2,6-Dinitrotoluene
50.0
U
33.7
35.6
67.4
71.2
Fluoranthene
50.0
U
38.6
41.7
77.2
83.4
Fluorene
50.0
U
32.5
32.8
65.0
65.6
Hexachlorobenzene
50.0
U
41.0
42.1
82.0
84.2
Hexachloro-1,3-butadiene
50.0
U
40.4
38.8
80.8
77.6
Hexachlorocyclopentadiene
50.0
U
13.7
9.74
27.4
19.5
Hexachloroethane
50.0
U
26.4
26.6
52.8
53.2
Indeno(1,2,3-cd)pyrene
50.0
U
41.1
44.5
82.2
89.0
Isophorone
50.0
U
36.2
35.8
72.4
71.6
ACCOUNT: PROJECT:
Withers & Ravenel Eng. - Standard 23-0302
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 47.0-145
2.20
48
1 33.0-145
3.08
74
1 27.0-133
6.80
66
1 1.00-120
J6 J6 0.000
40
1 33.0-143
8.37
53
1 24.0-159
6.02
71
1 11.0-162
11.0
63
1 1.00-219
7.75
97
1 17.0-163
7.49
72
1 33.0-184
1.22
54
1 12.0-158
3.24
108
1 36.0-166
0.000
76
1 53.0-127
8.24
43
1 60.0-120
0.000
24
1 25.0-158
1.58
61
1 17.0-168
6.98
87
1 1.00-227
6.13
126
1 1.00-262
0.814
108
1 39.0-139
6.16
42
1 50.0-158
5.48
48
1 26.0-137
7.72
66
1 59.0-121
0.919
38
1 1.00-152
2.65
55
1 24.0-120
4.04
62
1 10.0-146
33.8
34
1 40.0-120
0.755
52
1 1.00-171
7.94
99
1 21.0-196
1.11
93
SDG:
DATE/TIME:
PAGE:
L1616119
06/06/23 12:28
115 of 132

WG2061246 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1616119-18,19,20,21,22
L1616738-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1616738-01 05/20/23 05:13 • (MS) R3928852-3 05/20/23 05:34 • (MSD) R3928852-4 05/20/23 05:55
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/I
ug/I
ug/I
%
%
Naphthalene
50.0
U
26.6
25.2
53.2
50.4
Nitrobenzene
50.0
U
37.3
36.7
74.6
73.4
n-Nitrosodimethyla mine
50.0
U
24.7
26.5
49.4
53.0
n-Nitrosodiphenyla mine
50.0
U
33.3
36.4
66.6
72.8
n-Nitrosodi-n-propylamine
50.0
U
31.1
31.7
62.2
63.4
Phenanthrene
50.0
U
34.9
36.7
69.8
73.4
Benzylbutyl phthalate
50.0
U
41.6
46.1
83.2
92.2
Bis(2-ethylhexyl)phthalate
50.0
1.30
41.6
47.0
80.6
91.4
Di-n-butyl phthalate
50.0
U
41.3
43.9
82.6
87.8
Diethyl phthalate
50.0
U
38.0
41.5
76.0
83.0
Dimethyl phthalate
50.0
U
37.1
39.0
74.2
78.0
Di-n-octyl phthalate
50.0
U
36.6
40.0
73.2
80.0
Pyrene
50.0
U
38.4
43.3
76.8
86.6
1,2,4-Trichlorobenzene
50.0
U
30.0
28.2
60.0
56.4
4-ChIoro-3-methyl phenol
50.0
U
37.0
36.5
74.0
73.0
2-Chlorophenol
50.0
U
21.1
20.7
42.2
41.4
2,4-Dichlorophenol
50.0
U
32.3
31.7
64.6
63.4
2,4-Dimethylphenol
50.0
U
36.7
35.7
73.4
71.4
4,6-Dinitro-2-methylphenol
50.0
U
8.21
10.0
16.4
20.0
2,4-Dinitrophenol
50.0
U
7.11
8.29
14.2
16.6
2-Nitrophenol
50.0
U
26.8
26.7
53.6
53.4
4-Nitrophenol
50.0
U
7.41
7.67
14.8
15.3
Pentachlorophenol
50.0
U
13.4
16.5
26.8
33.0
Phenol
50.0
U
8.51
8.13
17.0
16.3
2,4,6-Trichlorophenol
50.0
U
33.0
33.9
66.0
67.8
(S) Nitrobenzene-d5
73.6
70.3
(S) 2-Fluorobiphenyl
57.5
58.1
(S) p-Terphenyl-d14
79.6
89.3
(S) Phenol-d5
17.5
16.8
(S) 2-F/uorophenol
26.5
25.1
(S)2,4,6-Tribromopheno/
67.5
69.0
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
21.0-133
35.0-180
10.0-120
16.0-160
1.00-230
54.0-120
1.00-152
8.00-158
1.00-120
1.00-120
1.00-120
4.00-146
52.0-120
44.0-142
22.0-147
23.0-134
39.0-135
32.0-120
1.00-181
1.00-191
29.0-182
1.00-132
14.0-176
5.00-120
37.0-144
15.0-314
22.0-127
29.0-141
8.00-424
10.0-120
10.0-153
5.41
1.62
7.03
8.90
1.91
5.03
10.3
12.2
6.10
8.81
4.99
8.88
12.0
6.19
1.36
1.91
1.87
2.76
19.7
15.3
0.374
3.45
20.7
4.57
2.69
65
62
40
28
87
39
60
82
47
100
183
69
49
50
73
61
50
58
203
132
55
131
86
64
58
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG:
Withers & Ravenel Eng. - Standard 23-0302 L1616119
DATE/TIME:
06/06/23 12:28
PAGE:
116 of 132

WG2062836 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1616119-01,02,03,04,05
Method Blank (MB)
(MB) R3927761-3 05/19/2318:48
MB Result MB Qualifier
MB MDL
MB RDL
Analyte mg/kg
mg/kg
mg/kg
Acenaphthene U
0.00539
0.0333
Acenaphthylene U
0.00469
0.0333
Anthracene U
0.00593
0.0333
Benzidine U
0.0626
1.67
Benzo(a)anth race ne U
0.00587
0.0333
Benzo(b)fluoranthene U
0.00621
0.0333
Benzo(k)fluoranthene U
0.00592
0.0333
Benzo(g,h,i)perylene U
0.00609
0.0333
Benzo(a)pyrene U
0.00619
0.0333
Bis(2-chlorethoxy)methane U
0.0100
0.333
Bis(2-chloroethyl)ether U
0.0110
0.333
2,2-Oxybis(1-Chloropropane) U
0.0144
0.333
4-Bromophenyl-phenylether U
0.0117
0.333
2-Chloronaphthalene U
0.00585
0.0333
4-Chlorophenyl-phenylether U
0.0116
0.333
Chrysene U
0.00662
0.0333
Dibenz(a,h)anthracene U
0.00923
0.0333
1,2-Dichlorobenzene U
0.00987
0.333
1,3-Dichlorobenzene U
0.0101
0.333
1,4-Dichlorobenzene U
0.00991
0.333
3,3-Dichlorobenzidine U
0.0123
0.333
2,4-Dinitrotoluene U
0.00955
0.333
2,6-Dinitrotoluene U
0.0109
0.333
Fluoranthene U
0.00601
0.0333
Fluorene U
0.00542
0.0333
Hexachlorobenzene U
0.0118
0.333
Hexachloro-1,3-butadiene U
0.0112
0.333
Hexachlorocyclopentadiene U
0.0175
0.333
Hexachloroethane U
0.0131
0.333
Indeno(1,2,3-cd)pyrene U
0.00941
0.0333
Isophorone U
0.0102
0.333
Naphthalene U
0.00836
0.0333
Nitrobenzene U
0.0116
0.333
n-Nitrosodimethyla mine U
0.0494
0.333
n-Nitrosodiphenyla mine U
0.0252
0.333
n-Nitrosodi-n-propylamine U
0.0111
0.333
Phenanthrene U
0.00661
0.0333
Benzylbutyl phthalate U
0.0104
0.333
Bis(2-ethylhexyl)phthalate U
0.0422
0.333
Di-n-butyl phthalate U
0.0114
0.333
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard
23-0302 L1616119 06/06/23 12:28 117 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2062836 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1616119-01,02,03,04,05
Method Blank (MB)
(MB) R3927761-3 05/19/2318:48
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/kg
mg/kg
mg/kg
Diethyl phthalate U
0.0110
0.333
Dimethyl phthalate U
0.0706
0.333
Di-n-octyl phthalate U
0.0225
0.333
Pyrene U
0.00648
0.0333
1,2,4-Trichlorobenzene U
0.0104
0.333
4-ChIoro-3-methyl phenol U
0.0108
0.333
2-Chorophenol U
0.0110
0.333
2,4-Dichlorophenol U
0.00970
0.333
2,4-Dimethylphenol U
0.00870
0.333
4,6-Dinitro-2-methylphenol U
0.0755
0.333
2,4-Dinitrophenol U
0.0779
0.333
2-Nitrophenol U
0.0119
0.333
4-Nitrophenol U
0.0104
0.333
Pentachlorophenol U
0.00896
0.333
Phenol U
0.0134
0.333
2,4,6-Trichlorophenol U
0.0107
0.333
(S) 2-Fluorophenol 53.5
12.0-120
(S) Phenol-d5 44.6
10.0-120
(S) Nitrobenzene-d5 46.2
10.0-122
(S) 2-F/uorobipheny/ 56.8
15.0-120
(S) 2,4,6-Tribromophenol 42.3
10.0-127
(S) p-Terphenyl-d14 67.3
10.0-120
Laboratory Control Sample (LCS)
(LCS) R3927761-1 05/19/2318:05
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/kg
mg/kg
%
%
Acenaphthene 0.666
0.436
65.5
38.0-120
Acenaphthylene 0.666
0.452
67.9
40.0-120
Anthracene 0.666
0.456
68.5
42.0-120
Benzidine 1.33
0.272
20.5
10.0-120
Benzo(a)anth race ne 0.666
0.481
72.2
44.0-120
Benzo(b)fluoranthene 0.666
0.507
76.1
43.0-120
Benzo(k)fluoranthene 0.666
0.503
75.5
44.0-120
Benzo(g,h,i)perylene 0.666
0.502
75.4
43.0-120
Benzo(a)pyrene 0.666
0.556
83.5
45.0-120
Bis(2-chlorethoxy)methane 0.666
0.338
50.8
20.0-120
Bis(2-chloroethyl)ether 0.666
0.443
66.5
16.0-120
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard
23-0302 L1616119 06/06/23 12:28 118 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2062836 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1616119-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3927761-1 05/19/2318:05
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/kg
mg/kg
%
%
2,2-Oxybis(1-Chloropropane)
0.666
0.370
55.6
23.0-120
4-Bromophenyl-phenylether
0.666
0.472
70.9
40.0-120
2-Chloronaphthalene
0.666
0.417
62.6
35.0-120
4-Chlorophenyl-phenylether
0.666
0.441
66.2
40.0-120
Chrysene
0.666
0.481
72.2
43.0-120
Dibenz(a,h)anthracene
0.666
0.500
75.1
44.0-120
1,2-Dichlorobenzene
0.666
0.410
61.6
32.0-120
1,3-Dichlorobenzene
0.666
0.382
57.4
30.0-120
1,4-Dichlorobenzene
0.666
0.380
57.1
31.0-120
3,3-Dichlorobenzidine
1.33
0.819
61.6
28.0-120
2,4-Dinitrotoluene
0.666
0.471
70.7
45.0-120
2,6-Dinitrotoluene
0.666
0.434
65.2
42.0-120
Fluoranthene
0.666
0.462
69.4
44.0-120
Fluorene
0.666
0.431
64.7
41.0-120
Hexachlorobenzene
0.666
0.457
68.6
39.0-120
Hexachloro-1,3-butadiene
0.666
0.344
51.7
15.0-120
Hexachlorocyclopentadiene
0.666
0.428
64.3
15.0-120
Hexachloroethane
0.666
0.351
52.7
17.0-120
Indeno(1,2,3-cd)pyrene
0.666
0.485
72.8
45.0-120
Isophorone
0.666
0.329
49.4
23.0-120
Naphthalene
0.666
0.342
51.4
18.0-120
Nitrobenzene
0.666
0.318
47.7
17.0-120
n-Nitrosodimethyla mine
0.666
0.292
43.8
10.0-125
n-Nitrosodiphenyla mine
0.666
0.447
67.1
40.0-120
n-Nitrosodi-n-propylamine
0.666
0.370
55.6
26.0-120
Phenanthrene
0.666
0.442
66.4
42.0-120
Benzylbutyl phthalate
0.666
0.492
73.9
40.0-120
Bis(2-ethylhexyl)phthalate
0.666
0.460
69.1
41.0-120
Di-n-butyl phthalate
0.666
0.467
70.1
43.0-120
Diethyl phthalate
0.666
0.456
68.5
43.0-120
Dimethyl phthalate
0.666
0.451
67.7
43.0-120
Di-n-octyl phthalate
0.666
0.421
63.2
40.0-120
Pyrene
0.666
0.471
70.7
41.0-120
1,2,4-Trichlorobenzene
0.666
0.364
54.7
17.0-120
4-ChIoro-3-methyl phenol
0.666
0.351
52.7
28.0-120
2-Chlorophenol
0.666
0.403
60.5
28.0-120
2,4-Dichlorophenol
0.666
0.340
51.1
25.0-120
2,4-Dimethylphenol
0.666
0.329
49.4
15.0-120
4,6-Dinitro-2-methylphenol
0.666
0.324
48.6
16.0-120
2,4-Dinitrophenol
0.666
0.230
34.5
10.0-120
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard
23-0302 L1616119 06/06/23 12:28 119 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG2062836 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1616119-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R3927761-1 05/19/2318:05
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
LCS Qualifier
Analyte
mg/kg
mg/kg
%
%
2-Nitrophenol
0.666
0.359
53.9
20.0-120
4-Nitrophenol
0.666
0.213
32.0
27.0-120
Pentachlorophenol
0.666
0.395
59.3
29.0-120
Phenol
0.666
0.313
47.0
28.0-120
2,4,6-Trichlorophenol
0.666
0.336
50.5
37.0-120
(S) 2-Fluorophenol
63.4
12.0-120
(S) Phenol-d5
54.1
10.0-120
(S) Nitrobenzene-d5
49.2
10.0-122
(S) 2-F/uorobipheny/
65.8
15.0-120
(S) 2,4,6-Tribromopheno/
69.4
10.0-127
(S) p-Terphenyl-d14
72.7
10.0-120
L1616047-01 Original
Sample (OS)
• Matrix Spike (MS) • Matrix
Spike Duplicate
(MSD)
(OS) L1616047-01 05/19/23 21:16 • (MS) R3927761-5 05/19/23 21:37 • (MSD)
R3927761-6 05/19/23 21:58
Spike Amount
Original Result
MS Result (dry)
MSD Result
MS Rec.
MSD Rec. Dilution
Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
(dry)
(dry)
(dry)
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
%
Acenaphthene
0.716
U
0.399
0.413
55.7
57.8 1
18.0-120
3.44
32
Acenaphthylene
0.716
U
0.411
0.424
57.4
59.3 1
25.0-120
3.09
32
Anthracene
0.716
U
0.441
0.454
61.6
63.6 1
22.0-120
2.88
29
Benzidine
1.43
U
0.701
0.812
49.0
56.8 1
10.0-120
14.6
40
Benzo(a)anth race ne
0.716
U
0.490
0.487
68.5
68.2 1
25.0-120
0.660
29
Benzo(b)fluoranthene
0.716
U
0.457
0.475
63.8
66.6 1
19.0-122
3.92
31
Benzo(k)fluoranthene
0.716
U
0.460
0.452
64.3
63.3 1
23.0-120
1.89
30
Benzo(g,h,i)perylene
0.716
U
0.478
0.472
66.8
66.1 1
10.0-120
1.36
33
Benzo(a)pyrene
0.716
U
0.525
0.536
73.3
75.2 1
24.0-120
2.23
30
B i s (2 -ch I o ret h oxy) m eth a n e
0.716
U
0.348
0.371
48.6
52.0 1
10.0-120
6.28
34
Bis(2-chIoroethyl) ether
0.716
U
0.358
0.403
50.0
56.5 1
10.0-120
11.9
40
2,2-Oxybis(1-ChIoropropane)
0.716
U
0.302
0.343
42.2
48.0 1
10.0-120
12.7
40
4-Bromophenyl-phenylether
0.716
U
0.439
0.443
61.3
62.0 1
27.0-120
0.976
30
2-Chloronaphthalene
0.716
U
0.364
0.398
50.9
55.7 1
20.0-120
8.74
32
4-C h I o ro p h e nyl -p h e nyl et h e r
0.716
U
0.401
0.424
56.0
59.3 1
24.0-120
5.48
29
Chrysene
0.716
U
0.455
0.448
63.5
62.8 1
21.0-120
1.43
29
Dibenz(a,h)anth racene
0.716
U
0.473
0.486
66.1
68.1 1
10.0-120
2.69
32
1,2-Dichlorobenzene
0.716
U
0.331
0.368
46.2
51.5 1
10.0-120
10.5
38
1,3-Dichlorobenzene
0.716
U
0.303
0.343
42.3
48.0 1
10.0-120
12.3
40
1,4-Dichlorobenzene
0.716
U
0.305
0.343
42.6
48.0 1
10.0-120
11.6
39
3,3-DichIorobenzidine
1.43
U
0.974
0.980
68.1
68.6 1
10.0-120
0.660
34
2,4-Dinitrotoluene
0.716
U
0.478
0.467
66.8
65.4 1
30.0-120
2.50
31
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
120 of 132
FP1
Fc
FSS
4
Cn
FSr
�GI
FAI
[Sc

WG2062836 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1616119-01,02,03,04,05
L1616O47-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1616047-01 05/19/23 21:16 • (MS) R3927761-5 05/19/23 21:37 • (MSD) R3927761-6 05/19/23 21:58
Spike Amount
Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
(dry)
(dry)
(dry)
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
%
2,6-Dinitrotoluene
0.716
U
0.428
0.434
59.8
60.8
1 25.0-120
1.50
31
Fluoranthene
0.716
U
0.440
0.449
61.4
63.0
1 18.0-126
2.18
32
Fluorene
0.716
U
0.404
0.415
56.5
58.1
1 25.0-120
2.62
30
Hexachlorobenzene
0.716
U
0.405
0.418
56.6
58.6
1 27.0-120
3.13
28
HexachIoro-1,3-butadiene
0.716
U
0.331
0.378
46.2
53.0
1 10.0-120
13.3
38
H exa c h I o rocyc I o p e nta d i e n e
0.716
U
0.343
0.369
47.9
51.7
1 10.0-120
7.25
40
Hexachloroethane
0.716
U
0.287
0.326
40.1
45.6
1 10.0-120
12.6
40
Indeno(1,2,3-cd)pyre ne
0.716
U
0.487
0.478
68.0
67.0
1 10.0-120
1.78
32
Isophorone
0.716
U
0.340
0.373
47.4
52.3
1 13.0-120
9.35
34
Naphthalene
0.716
U
0.333
0.366
46.5
51.2
1 10.0-120
9.23
35
Nitrobenzene
0.716
U
0.320
0.349
44.7
48.9
1 10.0-120
8.67
36
n-Nitrosod1methylamine
0.716
U
0.256
0.283
35.7
39.6
1 10.0-127
9.98
40
n-Nitrosodiphenylamine
0.716
U
0.430
0.435
60.1
61.0
1 17.0-120
1.24
29
n-Nitrosodi-n-propylamine
0.716
U
0.328
0.363
45.8
50.9
1 10.0-120
10.3
37
Phenanthrene
0.716
U
0.414
0.422
57.8
59.2
1 17.0-120
2.06
31
Benzylbutyl phthalate
0.716
U
0.544
0.539
76.0
75.5
1 23.0-120
0.993
30
Bis(2-ethylhexyl)phthalate
0.716
U
0.502
0.493
70.1
69.1
1 17.0-126
1.73
30
Di-n-butyl phthalate
0.716
U
0.473
0.468
66.1
65.5
1 30.0-120
1.14
29
Diethyl phthalate
0.716
U
0.446
0.449
62.3
63.0
1 26.0-120
0.720
28
Dimethyl phthalate
0.716
U
0.424
0.435
59.2
61.0
1 25.0-120
2.75
29
Di-n-octyl phthalate
0.716
U
0.509
0.501
71.0
70.2
1 21.0-123
1.49
29
Pyrene
0.716
U
0.461
0.461
64.4
64.6
1 16.0-121
0.000
32
1,2,4-Trichlorobenzene
0.716
U
0.355
0.395
49.5
55.3
1 12.0-120
10.6
37
4-ChIoro-3-methyl phenol
0.716
U
0.329
0.331
45.9
46.4
1 15.0-120
0.651
30
2-Chlorophenol
0.716
U
0.345
0.382
48.2
53.5
1 15.0-120
10.1
37
2,4-Dichlorophenol
0.716
U
0.369
0.407
51.5
57.1
1 20.0-120
9.97
31
2,4-Dimethylphenol
0.716
U
0.330
0.371
46.1
52.0
1 10.0-120
11.7
33
4,6-Dinitro-2-methylphenol
0.716
U
0.420
0.339
58.7
47.4
1 10.0-120
21.5
39
2,4-Dinitrophenol
0.716
U
0.364
0.231
50.9
32.4
1 10.0-121
J3 44.8
40
2-Nitrophenol
0.716
U
0.385
0.427
53.8
59.8
1 12.0-120
10.3
39
4-Nitrophenol
0.716
U
0.276
0.289
38.6
40.5
1 10.0-137
4.56
32
Pentachlorophenol
0.716
U
0.468
0.473
65.3
66.3
1 10.0-160
1.14
31
Phenol
0.716
U
0.272
0.301
38.0
42.2
1 12.0-120
10.1
38
2,4,6-Trichlorophenol
0.716
U
0.370
0.383
51.7
53.6
1 19.0-120
3.43
32
(S) 2-F/uorophenol
51.5
57.4
12.0-120
(S) Phenol-d5
45.0
49.4
10.0-120
(S) Nitrobenzene-d5
47.1
52.4
10.0-122
(S) 2-F/uorobipheny/
53.8
56.6
15.0-120
(S)2,4,6-Tribromophenol
65.0
64.9
10.0-127
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
121 of 132
FP1
Fc
FSS
H
FSr
�GI
$AI
[Sc

WG2062836 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1616119-01,02,03,04,05
L1616O47-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1616047-01 05/19/23 21:16 • (MS) R3927761-5 05/19/23 21:37 • (MSD) R3927761-6 05/19/23 21:58
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg % % % %
(S) p-Terphenyl-d14 65.8 64.8 10.0-120
RPD Limits
FP1
Fc
FSS
4
Cn
FSr
�GI
FAI
[Sc
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 122 of 132

WG2063159
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
QUALITY CONTROL SUMMARY
L1616119-06,07,08,09,10,11
Method Blank (MB)
(MB) R3927330-2 05/19/23 22:02
MB Result MB Qualifier
Analyte mg/kg
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anth race ne
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis(2-chlorethoxy)methane
Bis(2-ch loroethyl)ether
2, 2-Oxybis(1-Ch I oropro pa ne)
4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chlorophenyl-phenylether
Chrysene
Dibenz(a,h)anthracene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene
Hexachloroethane
I nd eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethyla mine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a m i n e
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MB MDL
mg/kg
0.00539
0.00469
0.00593
0.0626
0.00587
0.00621
0.00592
0.00609
0.00619
0.0100
0.0110
0.0144
0.0117
0.00585
0.0116
0.00662
0.00923
0.00987
0.0101
0.00991
0.0123
0.00955
0.0109
0.00601
0.00542
0.0118
0.0112
0.0175
0.0131
0.00941
0.0102
0.00836
0.0116
0.0494
0.0252
0.0111
0.00661
0.0104
0.0422
0.0114
MB RDL
mg/kg
0.0333
0.0333
0.0333
1.67
0.0333
0.0333
0.0333
0.0333
0.0333
0.333
0.333
0.333
0.333
0.0333
0.333
0.0333
0.0333
0.333
0.333
0.333
0.333
0.333
0.333
0.0333
0.0333
0.333
0.333
0.333
0.333
0.0333
0.333
0.0333
0.333
0.333
0.333
0.333
0.0333
0.333
0.333
0.333
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 123 of 132

WG2063159
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
QUALITY CONTROL SUMMARY
L1616119-06,07,08,09,10,11
Method Blank (MB)
(MB) R3927330-2 05/19/23 22:02
MB Result MB Qualifier
Analyte mg/kg
Diethyl phthalate
U
Dimethyl phthalate
U
Di-n-octyl phthalate
U
Pyrene
U
1,2,4-Trichlorobenzene
U
4-ChIoro-3-methyl phenol
U
2-Chorophenol
U
2,4-Dichlorophenol
U
2,4-Dimethylphenol
U
4,6-Dinitro-2-methylphenol
U
2,4-Dinitrophenol
U
2-Nitrophenol
U
4-Nitrophenol
U
Pentachlorophenol
U
Phenol
U
2,4,6-Trichlorophenol
U
(S) 2-Fluorophenol
60.8
(S) Phenol-d5
59.2
(S) Nitrobenzene-d5
57.4
(S) 2-F/uorobipheny/
58.6
(S)2,4,6-Tribromopheno/
59.6
(S) p-Terphenyl-d14
68.5
Laboratory Control Sample (LCS)
MB MDL
mg/kg
0.0110
0.0706
0.0225
0.00648
0.0104
0.0108
0.0110
0.00970
0.00870
0.0755
0.0779
0.0119
0.0104
0.00896
0.0134
0.0107
MB RDL
mg/kg
0.333
0.333
0.333
0.0333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
12.0-120
10.0-120
10.0-122
15.0-120
10.0-127
10.0-120
(LCS) R3927330-1 05/19/23 21:40
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte
mg/kg
mg/kg
%
%
Acenaphthene
0.666
0.388
58.3
38.0-120
Acenaphthylene
0.666
0.406
61.0
40.0-120
Anthracene
0.666
0.434
65.2
42.0-120
Benzidine
1.33
0.306
23.0
10.0-120
Benzo(a)anth race ne
0.666
0.442
66.4
44.0-120
Benzo(b)fluoranthene
0.666
0.459
68.9
43.0-120
Benzo(k)fluoranthene
0.666
0.455
68.3
44.0-120
Benzo(g,h,i)perylene
0.666
0.461
69.2
43.0-120
Benzo(a)pyrene
0.666
0.494
74.2
45.0-120
Bis(2-chlorethoxy)methane
0.666
0.324
48.6
20.0-120
Bis(2-chloroethyl)ether
0.666
0.387
58.1
16.0-120
LCS Qualifier
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT:
Withers & Ravenel Eng. - Standard
PROJECT: SDG: DATE/TIME: PAGE:
23-0302 L1616119 06/06/23 12:28 124 of 132

WG2063159
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
QUALITY CONTROL SUMMARY
L1616119-06,07,08,09,10,11
Laboratory Control Sample (LCS)
(LCS) R3927330-1 05/19/23 21:40
Spike Amount
Analyte mq/kq
2, 2-Oxybis(1-Ch I oropro pa ne)
4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chlorophenyl-phenylether
Chrysene
Dibenz(a,h)anthracene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene
Hexachloroethane
I nd eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethyla mine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a m i n e
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-m ethyl phenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phen of
2,4-Dinitrophenol
O.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
1.33
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
LCS Result
mg/kg
0.346
0.391
0.374
0.404
0.444
0.447
0.362
0.337
0.342
0.779
0.472
0.396
0.451
0.399
0.409
0.324
0.310
0.342
0.401
0.323
0.314
0.318
0.424
0.391
0.335
0.421
0.396
0.397
0.425
0.417
0.417
0.390
0.409
0.314
0.338
0.359
0.340
0.326
0.355
0.283
LCS Rec.
52.0
58.7
56.2
60.7
66.7
67.1
54.4
50.6
51.4
58.6
70.9
59.5
67.7
59.9
61.4
48.6
46.5
51.4
60.2
48.5
47.1
47.7
63.7
58.7
50.3
63.2
59.5
59.6
63.8
62.6
62.6
58.6
61.4
47.1
50.8
53.9
51.1
48.9
53.3
42.5
Rec. Limits LCS Qualifier
23.0-120
40.0-120
35.0-120
40.0-120
43.0-120
44.0-120
32.0-120
30.0-120
31.0-120
28.0-120
45.0-120
42.0-120
44.0-120
41.0-120
39.0-120
15.0-120
15.0-120
17.0-120
45.0-120
23.0-120
18.0-120
17.0-120
10.0-125
40.0-120
26.0-120
42.0-120
40.0-120
41.0-120
43.0-120
43.0-120
43.0-120
40.0-120
41.0-120
17.0-120
28.0-120
28.0-120
25.0-120
15.0-120
16.0-120
10.0-120
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 125 of 132

WG2063159 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1616119-06,07,08,09,10,11
Laboratory Control Sample (LCS)
(LCS) R3927330-1 05/19/23 21:40
Spike Amount
LCS Result
Analyte
mg/kg
mg/kg
2-Nitrophenol
0.666
0.332
4-Nitrophenol
0.666
0.395
Pentachlorophenol
0.666
0.394
Phenol
0.666
0.341
2,4,6-Trichlorophenol
0.666
0.394
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
LCS Rec.
Rec. Limits LCS Qualifier
49.8
20.0-120
59.3
27.0-120
59.2
29.0-120
51.2
28.0-120
59.2
37.0-120
58.0
12.0-120
54.4
10.0-120
48.6
10.0-122
59.2
15.0-120
66.5
10.0-127
62.2
10.0-120
L1617561-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1617561-01 05/23/2312:12 • (MS) R3928247-1 05/23/2312:32 • (MSD) R3928247-2 05/23/2312:52
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec.
(dry) (dry) (dry)
Analyte mg/kg % %
Acenaphthene
0.747
U
0.541
0.505
72.5
66.6
Acenaphthylene
0.747
U
0.467
0.476
62.6
62.7
Anthracene
0.747
U
0.551
0.560
73.7
73.8
Benzidine
1.49
U
U
U
0.000
0.000
Benzo(a)anth race ne
0.747
U
0.602
0.572
80.7
75.4
Benzo(b)fluoranthene
0.747
U
0.575
0.574
77.0
75.7
Benzo(k)fluoranthene
0.747
U
0.551
0.586
73.7
77.2
Benzo(g,h,i)perylene
0.747
0.0183
0.521
0.531
67.4
67.6
Benzo(a)pyrene
0.747
U
0.624
0.608
83.5
80.2
B i s (2 -ch I o ret h oxy) m eth a n e
0.747
U
0.511
0.458
68.4
60.4
Bis(2-chIoroethyl) ether
0.747
U
0.470
0.416
62.9
54.8
2,2-Oxybis(1-ChIoropropane)
0.747
U
0.485
0.464
64.9
61.1
4-Bromophenyl-phenylether
0.747
U
0.528
0.579
70.8
76.3
2-Chloronaphthalene
0.747
U
0.490
0.489
65.6
64.4
4-C h I o ro p h e nyl -p h e nyl et h e r
0.747
U
0.595
0.619
79.7
81.6
Chrysene
0.747
U
0.599
0.595
80.2
78.5
Dibenz(a,h)anth racene
0.747
U
0.496
0.530
66.4
69.8
1,2-Dichlorobenzene
0.747
U
0.418
0.411
56.0
54.2
1,3-Dichlorobenzene
0.747
U
0.388
0.388
51.9
51.1
1,4-Dichlorobenzene
0.747
U
0.415
0.400
55.5
52.8
3,3-DichIorobenzidine
1.49
U
0.398
0.540
26.7
35.7
2,4-Dinitrotoluene
0.747
U
0.609
0.647
81.6
85.3
ACCOUNT:
PROJECT:
Withers & Ravenel Eng.
- Standard
23-0302
Dilution Rec. Limits
2 18.0-120
2 25.0-120
2 22.0-120
2 10.0-120
2 25.0-120
2 19.0-122
2 23.0-120
2 10.0-120
2 24.0-120
2 10.0-120
2 10.0-120
2 10.0-120
2 27.0-120
2 20.0-120
2 24.0-120
2 21.0-120
2 10.0-120
2 10.0-120
2 10.0-120
2 10.0-120
2 10.0-120
2 30.0-120
MS Qualifier
J6
MSD Qualifier RPD
6.96
1.74
1.69
J6 0.000
5.20
0.204
6.20
1.79
2.48
10.9
12.2
4.46
9.12
0.240
3.87
0.590
6.64
1.70
0.000
3.46
30.3
5.98
RPD Limits
o�
32
32
29
40
29
31
30
33
30
34
40
40
30
32
29
29
32
38
40
39
34
31
SDG: DATE/TIME: PAGE:
L1616119 06/06/23 12:28 126 of 132
FP1
FC
FSS
4
Cn
FSr
�GI
FAI
[Sc

WG2063159 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1616119-06,07,08,09,10,11
L1617561-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1617561-01 05/23/2312:12 • (MS) R3928247-1 05/23/2312:32 • (MSD) R3928247-2 05/23/2312:52
Spike Amount
Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec.
Dilution
Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
(dry)
(dry)
(dry)
Analyte
mg/kg
%
%
%
%
%
2,6-Dinitrotoluene
0.747
U
0.565
0.585
75.6
77.1
2
25.0-120
3.47
31
Fluoranthene
0.747
0.0149
0.737
0.653
96.7
84.1
2
18.0-126
12.2
32
Fluorene
0.747
U
0.525
0.543
70.3
71.5
2
25.0-120
3.30
30
Hexachlorobenzene
0.747
U
0.510
0.538
68.2
70.9
2
27.0-120
5.38
28
HexachIoro-1,3-butadiene
0.747
U
0.614
0.570
82.2
75.1
2
10.0-120
7.54
38
H exa c h I o rocyc I o p e nta d i e n e
0.747
U
0.263
0.369
35.2
48.6
2
10.0-120
33.5
40
Hexachloroethane
0.747
U
0.479
0.498
64.2
65.6
2
10.0-120
3.85
40
Indeno(1,2,3-cd)pyre ne
0.747
U
0.487
0.500
65.3
65.9
2
10.0-120
2.62
32
Isophorone
0.747
U
0.516
0.484
69.0
63.8
2
13.0-120
6.35
34
Naphthalene
0.747
U
0.476
0.418
63.7
55.1
2
10.0-120
12.9
35
Nitrobenzene
0.747
U
0.501
0.443
67.1
58.4
2
10.0-120
12.4
36
n-Nitrosod1methylamine
0.747
U
0.435
0.361
58.2
47.5
2
10.0-127
18.6
40
n-Nitrosodiphenylamine
0.747
U
0.476
0.506
63.7
66.7
2
17.0-120
6.22
29
n-Nitrosodi-n-propylamine
0.747
U
0.528
0.525
70.8
69.2
2
10.0-120
0.669
37
Phenanthrene
0.747
U
0.635
0.530
85.1
69.8
2
17.0-120
18.1
31
Benzylbutyl phthalate
0.747
U
0.557
0.594
74.5
78.3
2
23.0-120
6.53
30
Bis(2-ethylhexyl)phthalate
0.747
U
0.633
0.674
84.7
88.9
2
17.0-126
6.29
30
Di-n-butyl phthalate
0.747
U
0.530
0.565
70.9
74.5
2
30.0-120
6.44
29
Diethyl phthalate
0.747
U
0.554
0.577
74.2
76.0
2
26.0-120
3.95
28
Dimethyl phthalate
0.747
U
0.560
0.566
75.0
74.6
2
25.0-120
1.04
29
Di-n-octyl phthalate
0.747
U
0.627
0.680
84.0
89.6
2
21.0-123
8.09
29
Pyrene
0.747
0.0154
0.689
0.578
90.2
74.1
2
16.0-121
17.6
32
1,2,4-Trichlorobenzene
0.747
U
0.510
0.469
68.2
61.8
2
12.0-120
8.40
37
4-ChIoro-3-methyl phenol
0.747
U
0.645
0.590
86.3
77.7
2
15.0-120
8.94
30
2-Chlorophenol
0.747
U
0.491
0.492
65.7
64.9
2
15.0-120
0.239
37
2,4-Dichlorophenol
0.747
U
0.534
0.497
71.5
65.5
2
20.0-120
7.29
31
2,4-Dimethylphenol
0.747
U
0.611
0.575
81.8
75.9
2
10.0-120
5.94
33
4,6-Dinitro-2-methylphenol
0.747
U
0.373
0.370
50.0
48.8
2
10.0-120
0.948
39
2,4-Dinitrophenol
0.747
U
0.254
0.228
34.0
30.0
2
10.0-121
10.7
40
2-Nitrophenol
0.747
U
0.553
0.483
74.1
63.6
2
12.0-120
13.6
39
4-Nitrophenol
0.747
U
0.429
0.557
57.4
73.4
2
10.0-137
26.0
32
Pentachlorophenol
0.747
U
0.234
0.411
31.3
54.2
2
10.0-160
J3 55.0
31
Phenol
0.747
U
0.443
0.450
59.3
59.3
2
12.0-120
1.58
38
2,4,6-Trichlorophenol
0.747
U
0.489
0.561
65.4
74.0
2
19.0-120
13.9
32
(S) 2-F/uorophenol
70.4
65.4
12.0-120
(S) Phenol-d5
69.3
69.6
10.0-120
(S) Nitrobenzene-d5
72.6
60.7
10.0-122
(S) 2-F/uorobipheny/
63.2
63.8
15.0-120
(S) 2,4,6-Tribromophenol
78.1
84.5
10.0-127
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Withers & Ravenel Eng. - Standard
23-0302
L1616119
06/06/23 12:28
127 of 132
FP1
Fc
FSS
H
FSr
�GI
$AI
FSC

WG2063159 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1616119-06,07,08,09,10,11
L1617561-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1617561-01 05/23/2312:12 • (MS) R3928247-1 05/23/2312:32 • (MSD) R3928247-2 05/23/2312:52
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec.
(dry) (dry) (dry)
Analyte mg/kg % %
(S) p-Terphenyl-d14 71.1 75.2
Sample Narrative:
OS: Dilution due to matrix impact during extraction procedure
MS: Dilution due to matrix impact during extraction procedure
MSD: Dilution due to matrix impact during extraction procedure
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
10.0-120
FP1
Fc
FSS
H
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 128 of 132

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)
Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
MDL (dry)
Method Detection Limit.
RDL
Reported Detection Limit.
RDL (dry)
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
B
The same analyte is found in the associated blank.
C3
The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
J
The identification of the analyte is acceptable; the reported value is an estimate.
J2
Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
J5
The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
FP1
FTC
FSS
4
Cn
FSr
RC
$AI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 129 of 132

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TN002
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolinas
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhodelsland
LA000356
Kentucky16
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' °
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TN003
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A21-A
A21-A — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21-A — ISO 17025 s
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity ° Chemical/Microbiological 'Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
FP1
FTc
FSS
4
Cn
FSr
Rc
I ql
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Withers & Ravenel Eng. - Standard 23-0302 L1616119 06/06/23 12:28 130 of 132

�- � I � Saar 1e kece t Che�'k1isG
j re,..- ..��1 Fra4c:r,tiIntaCt: Af It Appli•:able
!J
r -- - ---
Company Name/Address:
--
Sill Information: Signed
a;ttles are>_Ve
intact:
used:
P!
V
VOA Zero
Pras.Carrect`CheCk:Custody
r❑ HeadspaGe : -Fr +
�-
Page of_
Withers & RaVenel Eng.
115 MaclCenan Drive
WITHRAVS - Regular -rre�t of*-lzs
- rU5 Und=:,fEatient volume
ra_ 7--czar, cC.5
ears:
MR..h
1d
.4ESC
Cary, NC 27511
WITHRAVS-6200FULL
a-A-g s-c-t•e-ti-c•e•s
WITH RAVS - STATE LEAD
L
Email To: G� C
mjambs@withersra�enef.com
O
Z
W
d
L
N 1, a%S Lebanon Rd ti
o 1%1ouRt Juliet, TN 37122
Phone: [phone]i ia• _
Phone, 800.767.6ass
Fax: 6i5-758-5859 �-
T
Reporl : ��
to
Matt James /.�„�g� .1 Pv�
Project
Hillsborough St. Assemblage
City/State
Collected: ��/
Description:
c; e + r
°i
`
" ((A
i?
x
❑ Z 17
Phone: [phone]
Client Project #
lab Project #
Fax:
23-0302
Q
nu'i
aW,
ur
=
V
i
0
r4
p
2
G
l
I o 1
1 w Acctnum: WITH RAVS
Collected (pri 0:
Site/Facility I #
P.C. #
=
$
o
o
0
E
a)
ht
I CD ' Template:
U
Collected b ur
Rush? (Lab MUST Be Notified)
Date Results Needed
R Q
Immediately /
Same Da
_Next day.............................100%
Two Day ....... ....................... 50%
_ l ,
E I LO
d C4
r
�`
d
1*
U
Q
(D ` Prelogun:
TSR: Wagner
CO
Email? No es
No.
Packed on Ice N Y �I
_Three Day.............................a596
FAIL? NO ___,YeS
of
' i.7
Q
L 7
a)00
�
V7
Cooler:
s
Shipped Via:
Sample fA
Comp/Grab
Matrix '
Depth
Date
Time
ntrs
0
d
N
0000
Rem.IContaminam Sample R (lab only)
S t 12-3
ak45
3
w.z
o
`t32.
(-q 5-
s 7.
t w _ 5 - 7-5
1515-
I
-�
W -(y- q•5)
5- z z
0'�Js
-Cn
,-, - 5
V WOt 23 ZO �/
Matrix: SS - Soil GW - Groundwater W WasteWater DW Drinking Water imp
- - pH
Remarks r , 4 L0.n ` n Cap [e'r Flow Other Hold #
c OL,G
Relinquished . i ure
Date:
Time:
Received by: (Sig lure)
Samples returned via: ❑ UPS
Condition: (lab use only)
❑ FedEx ❑ Courier ❑
Relin uished : (Si at
Date:
Time:
R d b�grtature
Temp: ° Bottles Received:
--
COC Seal Intact: Y N NA
_
Relln re
te:
Time:
a ture)
Date: Time:
pH Checked: NCF:
Z v�

Company Name/Address:
Billing Information:
Analysis
1
Container
Preservative
Chain of custody Page_of —
Withers & RaVenel Eng.
ITHRAVS - Regular
7�
- rust Fund
OESC
115 MacKenan Drive
Cary, NC 27511
WITHRAVS -6200FULL
L-A-la S•C-I•E•N_C•E•s
WITHRAVS -STATE LEAD
x
zPhone:
Q
Leib— lid
MoOunt)u%L-t TN 57122
615-758-5858
Repoli to:
Matt James n a
Email To: gPCTC+
11-
m)ames@wi#hersravene�.cnm
�j,�7hone:
�
L
800.767.5859ax:--MR!b
Project
Hilishorough St. Assemblage
City/State
Collected: R"It. ca�(�r
L#MCA
Description:
IJ '
_
fa -
U
x
Phone: [phone]
Client Project #
Lab Project #
Table #
Fax:
23-Q3Q2
.Q
N
Lu
a
L]
2
E
a
CD
0
2
-
D
v
1
Coll e ted by (print)
`�
n ❑ L
Site/Facility ID #
P.O. #
Atctnum: WITHRAVS
'-{tA S
E
v
0
Template:
Collected b nature]:
Rush? (Lab MUST Be Notified)
Date Results Needed
Prelogin:
Same Day ....... ___ ............. 200%
_ Next Day.............................100%
d
11e72
y
Ol
--
p
U
D
N
TsRWagner
Email? No es
Immediately /
Packed on Ice N Y✓
_ Two Day..............................SO%
Three Day ------------- 25%
FAX? —No —Yes
Na.
�
,
Cat
V
oC
n
,
w
Cio
Cooler:
_ ................
of
v
M
to
D
7
(/j
Q
�
U
K
m
�
I:V
00
v
cV
00
U
Shipped via:
Sample ID
Comp/Grab
Matrix'
Depth
Date
Time
ntrs
Rem.�[antaminant
Sample N (lab only)
Tw-
V,
l w -
(P Li's
►�'
f S
all✓
��
t W -
S rz
Tw_ $
l S
✓
✓-
✓
-
rw-
,ova
✓
"I
✓
� 5�,t � _ i zoo r - T -- -- - - - —
' Matrix: SS • Soil GW - Groundwater WW - Wastewater DW - Drinking Water (]T- th r pH Temp
Remarks: Tp . P �i(4A 1 n 9 rlc k C66 +e r Flow other Hold #
Relinquished by • na
Date:
Time:
Received b gnatu
Samples returned via: ❑ UPS
Condition: (lab use only)
T
❑ FedEx ❑ Courier ❑
Relinquished bLy�(Si re
Date:
Trnie:
R I i
Tem Bottles Received:
p:N
�1
- A Q_:& % 73
COC Seal intact: _ Y _N _NA
Rely d 6aL.-Ign3
Date:
Time
R y: rgnaturej
Date: Time-.
pH Checked:
NCF:
v
a 0 J/�

eurofins
Air Toxics
6/13/2023
Mr. Matt James
Withers Ravenel Inc.
115 Mackenan Drive
Cary NC 27511
Project Name: Hillsborough Assemb.
Project #: 23-0302
Workorder #: 2305750
Dear Mr. Matt James
The following report includes the data for the above referenced project for sample(s)
received on 5/30/2023 at Eurofins Air Toxics LLC.
The data and associated QC analyzed by Modified TO-15 are compliant with the
project requirements or laboratory criteria with the exception of the deviations noted in
the attached case narrative.
Thank you for choosing Eurofins Air Toxics LLC. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contact the Project Manager: Brian Whittaker at 916-985-1000 if you have any
questions regarding the data in this report.
Regards,
Brian Whittaker
Project Manager
Eur-Ons AJr To ics, LLC
180 Blue Ravine Road, Suite 8
Folsom, CA 95630
T 916-SBS-1000
IF 916-351-8279
Vo w,airtoxics.com
Page 1 of 40

ti% eurofins
Air Toxics
WORK ORDER #: 2305750
Work Order Summary
CLIENT: Mr. Matt James BILL TO: Mr. Matt James
WithersRavenel Inc. WithersRavenel Inc.
115 Mackenan Drive 115 Mackenan Drive
Cary, NC 27511 Cary, NC 27511
PHONE: [phone] P.O. #
FAX: [phone] PROJECT # 23-0302 Hillsborough Assemb.
DATE RECEIVED: 05/30/2023 CONTACT: Brian Whittaker
DATE COMPLETED: 06/13/2023
RECEIPT
FINAL
FRACTION #
NAME
TEST
VAC./PRES.
PRESSURE
01A
VP-1
Modified TO-15
4.7 "Hg
10.1 psi
02A
VP-2
Modified TO-15
4.7 "Hg
10 psi
03A
VP-3
Modified TO-15
4.3 "Hg
10 psi
04A
VP-4
Modified TO-15
5.1 "Hg
9.9 psi
05A
VP-5
Modified TO-15
3.9 "Hg
10 psi
06A
VP-6
Modified TO-15
3.3 "Hg
9.8 psi
07A
VP-7
Modified TO-15
5.3 "Hg
10.1 psi
08A
VP-8
Modified TO-15
5.1 "Hg
9.9 psi
09A
VP-9
Modified TO-15
3.9 "Hg
10 psi
10A
VP-10
Modified TO-15
7.1 "Hg
10 psi
11A
DUP
Modified TO-15
4.5 "Hg
9.9 psi
12A
Lab Blank
Modified TO-15
NA
NA
13A
CCV
Modified TO-15
NA
NA
14A
LCS
Modified TO-15
NA
NA
14AA
LCSD
Modified TO-15
NA
NA
CERTIFIED BY: r DATE:
Technical Director
06/13/23
Certification numbers: AZ Licensure AZ0775, FL NELAP — E87680, LA NELAP — 02089, NH NELAP — 209222, NJ NELAP - CA016,
NY NELAP - 11291, TX NELAP — T104704434-22-18, UT NELAP — CA009332022-14, VA NELAP - 12240, WA ELAP - C935
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program) CA300005-017
Eurofins Environment Testing Northern California, LLC certifies that the test results contained in this report meet
all requirements of the 2016 TNI Standard.
This report shall not be reproduced, except in full, without the written approval ofEurofins Air Toxics, LLC.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630
[phone] . [phone] . FAX [phone]
Page 2 of 40

ti% eurofins
Air Toxics
LABORATORY NARRATIVE
Modified TO-15
Withers Ravenel Inc.
Workorder# 2305750
Eleven 1 Liter Summa Canister (100% Certified) samples were received on May 30, 2023. The
laboratory performed analysis via modified EPA Method TO-15 using GUMS in the full scan mode.
Method modifications taken to run these samples are summarized in the table below. Specific project
requirements may over -ride the EATL modifications.
Requirement
TO-15
ATL Modifications
Initial Calibration
</=30% RSD with 2
</=30% RSD with 4 compounds allowed out to < 40%
compounds allowed out
RSD
to < 40% RSD
Blank and standards
Zero Air
UHP Nitrogen provides a higher purity gas matrix than
zero air
Receiving Notes
The Chain of Custody (COC) information for samples VP-7, VP-8, VP-9 and VP-10 did not match the
entries on the sample tags with regard to sample identification. Therefore the information on the COC
was used to process and report the samples.
Analytical Notes
All Quality Control Limit exceedances and affected sample results are noted by flags. Each flag is
defined at the bottom of this Case Narrative and on each Sample Result Summary page. Target
compound non -detects in the samples that are associated with high bias in QC analyses have not been
flagged.
The reporting limit for Ethanol was raised from 2.0 ppbv to 6.2 ppbv due to anomalous linearity in the
Initial Calibration.
Dilution was performed on samples VP-9 and DUP due to the presence of high level non -target
species.
Definition of Data Oualifying Flags
Eight qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction
not performed).
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit, LOD, or MDL value. See
data page for project specific U-flag definition.
UJ- Non -detected compound associated with low bias in the CCV
N - The identification is based on presumptive evidence.
Page 3 of 40

�% eurofins
Air Toxics
File extensions may have been used on the data analysis sheets and indicates
as follows:
a -File was requantified
b-File was quantified by a second column and detector
rl-File was requantified for the purpose of reissue
Page 4 of 40

tiff e u rof i n s
Air Toxics
Summary of Detected Compounds
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
Client Sample ID: VP-1
Lab ID#: 2305750-01A
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 11
0.20
0.22
1.1
1.2
Acetone
4.0
5.2
9.5
12
Chloroform
0.20
0.31
0.98
1.5
Benzene
0.20
0.30
0.64
0.96
Toluene
2.0
4.7
7.5
18
Tetrachloroethene
0.20
0.34
1.4
2.3
Ethyl Benzene
0.20
0.85
0.87
3.7
m,p-Xylene
0.20
3.8
0.87
16
o-Xylene
0.20
3.6
0.87
16
Cumene
0.20
0.21
0.98
1.0
Propylbenzene
0.20
0.41
0.98
2.0
4-Ethyltoluene
0.20
2.0
0.98
9.9
1,3,5-Trimethyl benzene
0.20
0.34
0.98
1.7
1,2,4-Trimethyl benzene
0.20
5.4
0.98
27
Client Sample ID: VP-2
Lab ID#: 2305750-02A
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Chloroform
0.20
3.0
0.97
15
2,2,4-Trimethylpentane
1.0
1.4
4.6
6.4
Tetrachloroethene
0.20
1.9
1.3
13
Client Sample ID: VP-3
Lab ID#: 2305750-03A
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 11
0.20
0.20
1.1
1.1
Acetone
3.9
51
9.3
120
2-Butanone (Methyl Ethyl Ketone)
3.9
6.5
12
19
Chloroform
0.20
0.93
0.96
4.5
4-Methyl-2-pentanone
0.20
0.46
0.80
1.9
m,p-Xylene
0.20
1.0
0.85
4.4
Page 5 of 40

tiff e u rof i n s
Air Toxics
Summary of Detected Compounds
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
Client Sample ID: VP-3
Lab ID#: 2305750-03A
o-Xylene
0.20
0.91
0.85
3.9
4-Ethyltoluene
0.20
0.96
0.96
4.7
1,3,5-Trimethyl benzene
0.20
1.1
0.96
5.4
1,2,4-Trimethyl benzene
0.20
1.6
0.96
7.9
Client Sample ID: VP-4
Lab ID#: 2305750-04A
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
1.0
2.4
5.0
12
Acetone
4.0
24
9.6
58
Carbon Disulfide
10
12
31
38
Hexane
1.0
4.4
3.6
16
Chloroform
0.20
0.31
0.99
1.5
2,2,4-Trimethylpentane
1.0
9.1
4.7
43
Benzene
0.20
2.4
0.64
7.8
Heptane
1.0
2.6
4.1
11
4-Methyl-2-pentanone
0.20
1.0
0.83
4.3
Toluene
2.0
21
7.6
80
Tetrachloroethene
0.20
0.21
1.4
1.4
Ethyl Benzene
0.20
7.1
0.88
31
m,p-Xylene
0.20
37
0.88
160
o-Xylene
0.20
7.5
0.88
33
Cumene
0.20
1.7
0.99
8.5
Propylbenzene
0.20
2.6
0.99
13
4-Ethyltoluene
0.20
11
0.99
55
1,3,5-Trimethyl benzene
0.20
5.7
0.99
28
1,2,4-Trimethyl benzene
0.20
13
0.99
66
Client Sample ID: VP-5
Lab ID#: 2305750-05A
Compound
Rpt. Limit Amount Rpt. Limit Amount
(ppbv) (ppbv) (ug/m3) (ug/m3)
Freon 11 0.19 0.21 1.1 1.2
Page 6 of 40

tiff e u rof i n s
Air Toxics
Summary of Detected Compounds
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
Client Sample ID: VP-5
Lab ID#: 2305750-05A
Acetone
Chloroform
Tetrachloroethene
Client Sample ID: VP-6
Lab ID#: 2305750-06A
Compound
3.9
0.19
0.19
Rpt. Limit
(ppbv)
43
0.31
7.5
Amount
(ppbv)
9.2
0.94
1.3
Rpt. Limit
(ug/m3)
100
1.5
51
Amount
(ug/m3)
Freon 11
0.19
0.20
1.0
1.1
Ethanol
12
30
22
57
Acetone
3.7
8.3
8.9
20
Chloroform
0.19
0.43
0.91
2.1
2,2,4-Trimethylpentane
0.94
8.5
4.4
40
Benzene
0.19
0.43
0.60
1.4
Tetrachloroethene
0.19
1.1
1.3
7.8
Ethyl Benzene
0.19
0.76
0.81
3.3
m,p-Xylene
0.19
1.9
0.81
8.3
o-Xylene
0.19
0.92
0.81
4.0
Propylbenzene
0.19
0.22
0.92
1.1
4-Ethyltoluene
0.19
0.56
0.92
2.8
1,2,4-Trimethylbenzene
0.19
0.67
0.92
3.3
Client Sample ID: VP-7
Lab ID#: 2305750-07A
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Vinyl Chloride
0.20
0.26
0.52
0.65
Freon 11
0.20
0.26
1.2
1.4
Ethanol
13
26
24
48
Acetone
4.1
80
9.7
190
Methylene Chloride
1.0
1.0
3.6
3.7
Chloroform
0.20
0.22
1.0
1.1
Cyclohexane
1.0
2.3
3.5
7.9
2,2,4-Trimethylpentane
1.0
15
4.8
70
Page 7 of 40

tiff e u rof i n s
Air Toxics
Summary of Detected Compounds
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
Client Sample ID: VP-7
Lab ID#: 2305750-07A
Benzene
0.20
0.34
0.65
1.1
Tetrachloroethene
0.20
0.28
1.4
1.9
Ethyl Benzene
0.20
0.31
0.89
1.3
m,p-Xylene
0.20
0.76
0.89
3.3
o-Xylene
0.20
0.88
0.89
3.8
1,2,4-Trimethyl benzene
0.20
0.40
1.0
2.0
Client Sample ID: VP-8
Lab ID#: 2305750-08A
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 11
0.20
0.21
1.1
1.2
Acetone
4.0
6.5
9.6
15
Chloroform
0.20
0.38
0.99
1.8
Benzene
0.20
0.20 J
0.64
0.63 J
Toluene
2.0
4.1
7.6
15
Tetrachloroethene
0.20
0.58
1.4
3.9
Ethyl Benzene
0.20
3.4
0.88
15
m,p-Xylene
0.20
28
0.88
120
o-Xylene
0.20
13
0.88
55
Cumene
0.20
0.71
0.99
3.5
Propylbenzene
0.20
1.0
0.99
4.9
4-Ethyltoluene
0.20
7.1
0.99
35
1,3,5-Trimethyl benzene
0.20
1.6
0.99
7.6
1,2,4-Trimethyl benzene
0.20
9.5
0.99
47
Client Sample ID: VP-9
Lab ID#: 2305750-09A
Compound
Rpt. Limit
(ppbv)
Amount
(ppbv)
Rpt. Limit
(ug/m3)
Amount
(ug/m3)
2,2,4-Trimethylpentane
4.8
47
22
220
Benzene
0.96
1.7
3.1
5.3
Heptane
4.8
5.8
20
24
Toluene
9.6
30
36
120
Page 8 of 40

tiff e u rof i n s
Air Toxics
Summary of Detected Compounds
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
Client Sample ID: VP-9
Lab ID#: 2305750-09A
Tetrachloroethene
0.96
0.99
6.5
6.7
Ethyl Benzene
0.96
10
4.2
44
m,p-Xylene
0.96
68
4.2
290
o-Xylene
0.96
26
4.2
110
Propylbenzene
0.96
4.0
4.7
19
4-Ethyltoluene
0.96
21
4.7
100
1,3,5-Trimethyl benzene
0.96
18
4.7
87
1,2,4-Trimethyl benzene
0.96
42
4.7
210
Client Sample ID: VP-10
Lab ID#: 2305750-10A
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 11
0.22
0.24
1.2
1.3
Acetone
4.4
8.2
10
20
Chloroform
0.22
1.2
1.1
6.1
2,2,4-Trimethylpentane
1.1
3.7
5.1
18
Benzene
0.22
3.8
0.70
12
Trichloroethene
0.22
0.22
1.2
1.2
Toluene
2.2
45
8.3
170
Tetrachloroethene
0.22
2.6
1.5
17
Ethyl Benzene
0.22
12
0.96
53
m,p-Xylene
0.22
46
0.96
200
o-Xylene
0.22
21
0.96
91
Cumene
0.22
1.8
1.1
8.7
Propylbenzene
0.22
3.6
1.1
18
4-Ethyltoluene
0.22
14
1.1
69
1,3,5-Trimethyl benzene
0.22
7.5
1.1
37
1,2,4-Trimethylbenzene
0.22
16
1.1
79
Client Sample ID: DUP
Lab ID#: 2305750-11 A
Rpt. Limit Amount Rpt. Limit Amount
Compound (ppbv) (ppbv) (ug/m3) (ug/m3)
Page 9 of 40

tiff eurof ins
Air Toxics
Summary of Detected Compounds
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
Client Sample ID: DUP
Lab ID#: 2305750-11A
Compound
Rpt. Limit
(ppbv)
Amount
(ppbv)
Rpt. Limit
(ug/m3)
Amount
(ug/m3)
Acetone
20
69
47
160
2,2,4-Trimethylpentane
4.9
34
23
160
Benzene
0.98
1.4
3.1
4.4
Heptane
4.9
5.5
20
22
Toluene
9.8
27
37
100
Ethyl Benzene
0.98
8.9
4.3
38
m,p-Xylene
0.98
56
4.3
240
o-Xylene
0.98
23
4.3
100
Propylbenzene
0.98
3.5
4.8
17
4-Ethyltoluene
0.98
18
4.8
88
1,3,5-Trimethyl benzene
0.98
16
4.8
80
1,2,4-Trimethyl benzene
0.98
39
4.8
190
Page 10 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-1
Lab ID#: 2305750-01A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061213 Date of Collection: 5/22/23 9:35:00 AM
Dil. Factor: 2.00 Date of Analysis: 6/12/23 06:55 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
1.0
Not Detected
4.9
Not Detected
Freon 114
0.20
Not Detected
1.4
Not Detected
Chloromethane
1.0
Not Detected
2.1
Not Detected
Vinyl Chloride
0.20
Not Detected
0.51
Not Detected
1,3-Butadiene
0.20
Not Detected
0.44
Not Detected
Bromomethane
10
Not Detected
39
Not Detected
Chloroethane
1.0
Not Detected
2.6
Not Detected
Freon 11
0.20
0.22
1.1
1.2
Ethanol
12
Not Detected
23
Not Detected
Freon 113
0.20
Not Detected
1.5
Not Detected
1,1-Dichloroethene
0.20
Not Detected
0.79
Not Detected
Acetone
4.0
5.2
9.5
12
2-Propanol
4.0
Not Detected
9.8
Not Detected
Carbon Disulfide
10
Not Detected
31
Not Detected
3-Chloropropene
1.0
Not Detected
3.1
Not Detected
Methylene Chloride
1.0
Not Detected
3.5
Not Detected
Methyl tert-butyl ether
0.20
Not Detected
0.72
Not Detected
trans- 1,2-Dichloroethene
0.20
Not Detected
0.79
Not Detected
Hexane
1.0
Not Detected
3.5
Not Detected
1,1-Dichloroethane
0.20
Not Detected
0.81
Not Detected
2-Butanone (Methyl Ethyl Ketone)
4.0
Not Detected
12
Not Detected
cis-1,2-Dichloroethene
0.20
Not Detected
0.79
Not Detected
Tetrahydrofuran
1.0
Not Detected
2.9
Not Detected
Chloroform
0.20
0.31
0.98
1.5
1, 1, 1 -Trichloroethane
0.20
Not Detected
1.1
Not Detected
Cyclohexane
1.0
Not Detected
3.4
Not Detected
Carbon Tetrachloride
0.20
Not Detected UJ
1.2
Not Detected UJ
2,2,4-Trimethylpentane
1.0
Not Detected
4.7
Not Detected
Benzene
0.20
0.30
0.64
0.96
1,2-Dichloroethane
0.20
Not Detected
0.81
Not Detected
Heptane
1.0
Not Detected
4.1
Not Detected
Trichloroethene
0.20
Not Detected
1.1
Not Detected
1,2-Dichloropropane
0.20
Not Detected
0.92
Not Detected
1,4-Dioxane
1.0
Not Detected
3.6
Not Detected
Bromodichloromethane
0.20
Not Detected
1.3
Not Detected
cis-1,3-Dichloropropene
0.20
Not Detected
0.91
Not Detected
4-Methyl-2-pentanone
0.20
Not Detected
0.82
Not Detected
Toluene
2.0
4.7
7.5
18
trans-1,3-Dichloropropene
0.20
Not Detected
0.91
Not Detected
1,1,2-Trichloroethane
0.20
Not Detected
1.1
Not Detected
Tetrachloroethene
0.20
0.34
1.4
2.3
2-Hexanone
1.0
Not Detected
4.1
Not Detected
Page 11 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-1
Lab ID#: 2305750-01A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061213 Date of Collection: 5/22/23 9:35:00 AM
Dil. Factor: 2.00 Date of Analysis: 6/12/23 06:55 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.20
Not Detected
1.7
Not Detected
1,2-Dibromoethane (EDB)
0.20
Not Detected
1.5
Not Detected
Chlorobenzene
0.20
Not Detected
0.92
Not Detected
Ethyl Benzene
0.20
0.85
0.87
3.7
m, p-Xylene
0.20
3.8
0.87
16
o-Xylene
0.20
3.6
0.87
16
Styrene
0.20
Not Detected
0.85
Not Detected
Bromoform
0.20
Not Detected
2.1
Not Detected
Cumene
0.20
0.21
0.98
1.0
1,1,2,2-Tetrachloroethane
0.20
Not Detected
1.4
Not Detected
Propylbenzene
0.20
0.41
0.98
2.0
4-Ethyltoluene
0.20
2.0
0.98
9.9
1,3,5-Trimethyl benzene
0.20
0.34
0.98
1.7
1,2,4-Trimethyl benzene
0.20
5.4
0.98
27
1,3-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,4-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
alpha-Chlorotoluene
0.20
Not Detected
1.0
Not Detected
1,2-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,2,4-Trichlorobenzene
1.0
Not Detected
7.4
Not Detected
Hexachlorobutadiene
1.0
Not Detected
11
Not Detected
Naphthalene
0.40
Not Detected
2.1
Not Detected
UJ = Analyte associated with low bias in the CCV.
Container Type: 1 Liter Summa Canister (100% Certified)
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 122 70-130
Toluene-d8 108 70-130
4-Bromofluorobenzene 88 70-130
Page 12 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-2
Lab ID#: 2305750-02A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061214 Date of Collection: 5/22/23 9:46:00 AM
Dil. Factor: 1.99 Date of Analysis: 6/12/23 07:49 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
1.0
Not Detected
4.9
Not Detected
Freon 114
0.20
Not Detected
1.4
Not Detected
Chloromethane
1.0
Not Detected
2.0
Not Detected
Vinyl Chloride
0.20
Not Detected
0.51
Not Detected
1,3-Butadiene
0.20
Not Detected
0.44
Not Detected
Bromomethane
10
Not Detected
39
Not Detected
Chloroethane
1.0
Not Detected
2.6
Not Detected
Freon 11
0.20
Not Detected
1.1
Not Detected
Ethanol
12
Not Detected
23
Not Detected
Freon 113
0.20
Not Detected
1.5
Not Detected
1,1-Dichloroethene
0.20
Not Detected
0.79
Not Detected
Acetone
4.0
Not Detected
9.4
Not Detected
2-Propanol
4.0
Not Detected
9.8
Not Detected
Carbon Disulfide
10
Not Detected
31
Not Detected
3-Chloropropene
1.0
Not Detected
3.1
Not Detected
Methylene Chloride
1.0
Not Detected
3.4
Not Detected
Methyl tert-butyl ether
0.20
Not Detected
0.72
Not Detected
trans- 1,2-Dichloroethene
0.20
Not Detected
0.79
Not Detected
Hexane
1.0
Not Detected
3.5
Not Detected
1,1-Dichloroethane
0.20
Not Detected
0.80
Not Detected
2-Butanone (Methyl Ethyl Ketone)
4.0
Not Detected
12
Not Detected
cis-1,2-Dichloroethene
0.20
Not Detected
0.79
Not Detected
Tetrahydrofuran
1.0
Not Detected
2.9
Not Detected
Chloroform
0.20
3.0
0.97
15
1, 1, 1 -Trichloroethane
0.20
Not Detected
1.1
Not Detected
Cyclohexane
1.0
Not Detected
3.4
Not Detected
Carbon Tetrachloride
0.20
Not Detected UJ
1.2
Not Detected UJ
2,2,4-Trimethylpentane
1.0
1.4
4.6
6.4
Benzene
0.20
Not Detected
0.64
Not Detected
1,2-Dichloroethane
0.20
Not Detected
0.80
Not Detected
Heptane
1.0
Not Detected
4.1
Not Detected
Trichloroethene
0.20
Not Detected
1.1
Not Detected
1,2-Dichloropropane
0.20
Not Detected
0.92
Not Detected
1,4-Dioxane
1.0
Not Detected
3.6
Not Detected
Bromodichloromethane
0.20
Not Detected
1.3
Not Detected
cis-1,3-Dichloropropene
0.20
Not Detected
0.90
Not Detected
4-Methyl-2-pentanone
0.20
Not Detected
0.82
Not Detected
Toluene
2.0
Not Detected
7.5
Not Detected
trans-1,3-Dichloropropene
0.20
Not Detected
0.90
Not Detected
1,1,2-Trichloroethane
0.20
Not Detected
1.1
Not Detected
Tetrachloroethene
0.20
1.9
1.3
13
2-Hexanone
1.0
Not Detected
4.1
Not Detected
Page 13 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-2
Lab ID#: 2305750-02A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061214 Date of Collection: 5/22/23 9:46:00 AM
Dil. Factor: 1.99 Date of Analysis: 6/12/23 07:49 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.20
Not Detected
1.7
Not Detected
1,2-Dibromoethane (EDB)
0.20
Not Detected
1.5
Not Detected
Chlorobenzene
0.20
Not Detected
0.92
Not Detected
Ethyl Benzene
0.20
Not Detected
0.86
Not Detected
m,p-Xylene
0.20
Not Detected
0.86
Not Detected
o-Xylene
0.20
Not Detected
0.86
Not Detected
Styrene
0.20
Not Detected
0.85
Not Detected
Bromoform
0.20
Not Detected
2.0
Not Detected
Cumene
0.20
Not Detected
0.98
Not Detected
1,1,2,2-Tetrachloroethane
0.20
Not Detected
1.4
Not Detected
Propylbenzene
0.20
Not Detected
0.98
Not Detected
4-Ethyltoluene
0.20
Not Detected
0.98
Not Detected
1,3,5-Trimethyl benzene
0.20
Not Detected
0.98
Not Detected
1,2,4-Trimethyl benzene
0.20
Not Detected
0.98
Not Detected
1,3-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,4-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
alpha-Chlorotoluene
0.20
Not Detected
1.0
Not Detected
1,2-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,2,4-Trichlorobenzene
1.0
Not Detected
7.4
Not Detected
Hexachlorobutadiene
1.0
Not Detected
11
Not Detected
Naphthalene
0.40
Not Detected
2.1
Not Detected
UJ = Analyte associated with low bias in the CCV.
Container Type: 1 Liter Summa Canister (100% Certified)
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 125 70-130
Toluene-d8 105 70-130
4-Bromofluorobenzene 81 70-130
Page 14 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-3
Lab ID#: 2305750-03A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061215 Date of Collection: 5/22/23 10:20:00 AM
Dil. Factor: 1.96 Date of Analysis: 6/12/23 08:33 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
0.98
Not Detected
4.8
Not Detected
Freon 114
0.20
Not Detected
1.4
Not Detected
Chloromethane
0.98
Not Detected
2.0
Not Detected
Vinyl Chloride
0.20
Not Detected
0.50
Not Detected
1,3-Butadiene
0.20
Not Detected
0.43
Not Detected
Bromomethane
9.8
Not Detected
38
Not Detected
Chloroethane
0.98
Not Detected
2.6
Not Detected
Freon 11
0.20
0.20
1.1
1.1
Ethanol
12
Not Detected
23
Not Detected
Freon 113
0.20
Not Detected
1.5
Not Detected
1,1-Dichloroethene
0.20
Not Detected
0.78
Not Detected
Acetone
3.9
51
9.3
120
2-Propanol
3.9
Not Detected
9.6
Not Detected
Carbon Disulfide
9.8
Not Detected
30
Not Detected
3-Chloropropene
0.98
Not Detected
3.1
Not Detected
Methylene Chloride
0.98
Not Detected
3.4
Not Detected
Methyl tert-butyl ether
0.20
Not Detected
0.71
Not Detected
trans- 1,2-Dichloroethene
0.20
Not Detected
0.78
Not Detected
Hexane
0.98
Not Detected
3.4
Not Detected
1,1-Dichloroethane
0.20
Not Detected
0.79
Not Detected
2-Butanone (Methyl Ethyl Ketone)
3.9
6.5
12
19
cis-1,2-Dichloroethene
0.20
Not Detected
0.78
Not Detected
Tetrahydrofuran
0.98
Not Detected
2.9
Not Detected
Chloroform
0.20
0.93
0.96
4.5
1, 1, 1 -Trichloroethane
0.20
Not Detected
1.1
Not Detected
Cyclohexane
0.98
Not Detected
3.4
Not Detected
Carbon Tetrachloride
0.20
Not Detected UJ
1.2
Not Detected UJ
2,2,4-Trimethylpentane
0.98
Not Detected
4.6
Not Detected
Benzene
0.20
Not Detected
0.63
Not Detected
1,2-Dichloroethane
0.20
Not Detected
0.79
Not Detected
Heptane
0.98
Not Detected
4.0
Not Detected
Trichloroethene
0.20
Not Detected
1.0
Not Detected
1,2-Dichloropropane
0.20
Not Detected
0.90
Not Detected
1,4-Dioxane
0.98
Not Detected
3.5
Not Detected
Bromodichloromethane
0.20
Not Detected
1.3
Not Detected
cis-1,3-Dichloropropene
0.20
Not Detected
0.89
Not Detected
4-Methyl-2-pentanone
0.20
0.46
0.80
1.9
Toluene
2.0
Not Detected
7.4
Not Detected
trans-1,3-Dichloropropene
0.20
Not Detected
0.89
Not Detected
1,1,2-Trichloroethane
0.20
Not Detected
1.1
Not Detected
Tetrachloroethene
0.20
Not Detected
1.3
Not Detected
2-Hexanone
0.98
Not Detected
4.0
Not Detected
Page 15 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-3
Lab ID#: 2305750-03A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061215 Date of Collection: 5/22/23 10:20:00 AM
Dil. Factor: 1.96 Date of Analysis: 6/12/23 08:33 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.20
Not Detected
1.7
Not Detected
1,2-Dibromoethane (EDB)
0.20
Not Detected
1.5
Not Detected
Chlorobenzene
0.20
Not Detected
0.90
Not Detected
Ethyl Benzene
0.20
Not Detected
0.85
Not Detected
m, p-Xylene
0.20
1.0
0.85
4.4
o-Xylene
0.20
0.91
0.85
3.9
Styrene
0.20
Not Detected
0.83
Not Detected
Bromoform
0.20
Not Detected
2.0
Not Detected
Cumene
0.20
Not Detected
0.96
Not Detected
1,1,2,2-Tetrachloroethane
0.20
Not Detected
1.3
Not Detected
Propylbenzene
0.20
Not Detected
0.96
Not Detected
4-Ethyltoluene
0.20
0.96
0.96
4.7
1,3,5-Trimethyl benzene
0.20
1.1
0.96
5.4
1,2,4-Trimethyl benzene
0.20
1.6
0.96
7.9
1,3-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,4-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
alpha-Chlorotoluene
0.20
Not Detected
1.0
Not Detected
1,2-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,2,4-Trichlorobenzene
0.98
Not Detected
7.3
Not Detected
Hexachlorobutadiene
0.98
Not Detected
10
Not Detected
Naphthalene
0.39
Not Detected
2.0
Not Detected
UJ = Analyte associated with low bias in the CCV.
Container Type: 1 Liter Summa Canister (100% Certified)
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 117 70-130
Toluene-d8 102 70-130
4-Bromofluorobenzene 97 70-130
Page 16 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-4
Lab ID#: 2305750-04A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061216 Date of Collection: 5/22/23 10:55:00 AM
Dil. Factor: 2.02 Date of Analysis: 6/12/23 09:10 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
1.0
2.4
5.0
12
Freon 114
0.20
Not Detected
1.4
Not Detected
Chloromethane
1.0
Not Detected
2.1
Not Detected
Vinyl Chloride
0.20
Not Detected
0.52
Not Detected
1,3-Butadiene
0.20
Not Detected
0.45
Not Detected
Bromomethane
10
Not Detected
39
Not Detected
Chloroethane
1.0
Not Detected
2.7
Not Detected
Freon 11
0.20
Not Detected
1.1
Not Detected
Ethanol
12
Not Detected
24
Not Detected
Freon 113
0.20
Not Detected
1.5
Not Detected
1,1-Dichloroethene
0.20
Not Detected
0.80
Not Detected
Acetone
4.0
24
9.6
58
2-Propanol
4.0
Not Detected
9.9
Not Detected
Carbon Disulfide
10
12
31
38
3-Chloropropene
1.0
Not Detected
3.2
Not Detected
Methylene Chloride
1.0
Not Detected
3.5
Not Detected
Methyl tert-butyl ether
0.20
Not Detected
0.73
Not Detected
trans- 1,2-Dichloroethene
0.20
Not Detected
0.80
Not Detected
Hexane
1.0
4.4
3.6
16
1,1-Dichloroethane
0.20
Not Detected
0.82
Not Detected
2-Butanone (Methyl Ethyl Ketone)
4.0
Not Detected
12
Not Detected
cis-1,2-Dichloroethene
0.20
Not Detected
0.80
Not Detected
Tetrahydrofuran
1.0
Not Detected
3.0
Not Detected
Chloroform
0.20
0.31
0.99
1.5
1, 1, 1 -Trichloroethane
0.20
Not Detected
1.1
Not Detected
Cyclohexane
1.0
Not Detected
3.5
Not Detected
Carbon Tetrachloride
0.20
Not Detected UJ
1.3
Not Detected UJ
2,2,4-Trimethylpentane
1.0
9.1
4.7
43
Benzene
0.20
2.4
0.64
7.8
1,2-Dichloroethane
0.20
Not Detected
0.82
Not Detected
Heptane
1.0
2.6
4.1
11
Trichloroethene
0.20
Not Detected
1.1
Not Detected
1,2-Dichloropropane
0.20
Not Detected
0.93
Not Detected
1,4-Dioxane
1.0
Not Detected
3.6
Not Detected
Bromodichloromethane
0.20
Not Detected
1.4
Not Detected
cis-1,3-Dichloropropene
0.20
Not Detected
0.92
Not Detected
4-Methyl-2-pentanone
0.20
1.0
0.83
4.3
Toluene
2.0
21
7.6
80
trans-1,3-Dichloropropene
0.20
Not Detected
0.92
Not Detected
1,1,2-Trichloroethane
0.20
Not Detected
1.1
Not Detected
Tetrachloroethene
0.20
0.21
1.4
1.4
2-Hexanone
1.0
Not Detected
4.1
Not Detected
Page 17 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-4
Lab ID#: 2305750-04A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061216 Date of Collection: 5/22/23 10:55:00 AM
Dil. Factor: 2.02 Date of Analysis: 6/12/23 09:10 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.20
Not Detected
1.7
Not Detected
1,2-Dibromoethane (EDB)
0.20
Not Detected
1.6
Not Detected
Chlorobenzene
0.20
Not Detected
0.93
Not Detected
Ethyl Benzene
0.20
7.1
0.88
31
m, p-Xylene
0.20
37
0.88
160
o-Xylene
0.20
7.5
0.88
33
Styrene
0.20
Not Detected
0.86
Not Detected
Bromoform
0.20
Not Detected
2.1
Not Detected
Cumene
0.20
1.7
0.99
8.5
1,1,2,2-Tetrachloroethane
0.20
Not Detected
1.4
Not Detected
Propylbenzene
0.20
2.6
0.99
13
4-Ethyltoluene
0.20
11
0.99
55
1,3,5-Trimethyl benzene
0.20
5.7
0.99
28
1,2,4-Trimethyl benzene
0.20
13
0.99
66
1,3-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,4-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
alpha-Chlorotoluene
0.20
Not Detected
1.0
Not Detected
1,2-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,2,4-Trichlorobenzene
1.0
Not Detected
7.5
Not Detected
Hexachlorobutadiene
1.0
Not Detected
11
Not Detected
Naphthalene
0.40
Not Detected
2.1
Not Detected
UJ = Analyte associated with low bias in the CCV.
Container Type: 1 Liter Summa Canister (100% Certified)
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 120 70-130
Toluene-d8 114 70-130
4-Bromofluorobenzene ill 70-130
Page 18 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-5
Lab ID#: 2305750-05A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061217 Date of Collection: 5/22/23 10:21:00 AM
Dil. Factor: 1.93 Date of Analysis: 6/12/23 09:53 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
0.96
Not Detected
4.8
Not Detected
Freon 114
0.19
Not Detected
1.3
Not Detected
Chloromethane
0.96
Not Detected
2.0
Not Detected
Vinyl Chloride
0.19
Not Detected
0.49
Not Detected
1,3-Butadiene
0.19
Not Detected
0.43
Not Detected
Bromomethane
9.6
Not Detected
37
Not Detected
Chloroethane
0.96
Not Detected
2.5
Not Detected
Freon 11
0.19
0.21
1.1
1.2
Ethanol
12
Not Detected
22
Not Detected
Freon 113
0.19
Not Detected
1.5
Not Detected
1,1-Dichloroethene
0.19
Not Detected
0.76
Not Detected
Acetone
3.9
43
9.2
100
2-Propanol
3.9
Not Detected
9.5
Not Detected
Carbon Disulfide
9.6
Not Detected
30
Not Detected
3-Chloropropene
0.96
Not Detected
3.0
Not Detected
Methylene Chloride
0.96
Not Detected
3.4
Not Detected
Methyl tert-butyl ether
0.19
Not Detected
0.70
Not Detected
trans- 1,2-Dichloroethene
0.19
Not Detected
0.76
Not Detected
Hexane
0.96
Not Detected
3.4
Not Detected
1,1-Dichloroethane
0.19
Not Detected
0.78
Not Detected
2-Butanone (Methyl Ethyl Ketone)
3.9
Not Detected
11
Not Detected
cis-1,2-Dichloroethene
0.19
Not Detected
0.76
Not Detected
Tetrahydrofuran
0.96
Not Detected
2.8
Not Detected
Chloroform
0.19
0.31
0.94
1.5
1, 1, 1 -Trichloroethane
0.19
Not Detected
1.0
Not Detected
Cyclohexane
0.96
Not Detected
3.3
Not Detected
Carbon Tetrachloride
0.19
Not Detected UJ
1.2
Not Detected UJ
2,2,4-Trimethylpentane
0.96
Not Detected
4.5
Not Detected
Benzene
0.19
Not Detected
0.62
Not Detected
1,2-Dichloroethane
0.19
Not Detected
0.78
Not Detected
Heptane
0.96
Not Detected
4.0
Not Detected
Trichloroethene
0.19
Not Detected
1.0
Not Detected
1,2-Dichloropropane
0.19
Not Detected
0.89
Not Detected
1,4-Dioxane
0.96
Not Detected
3.5
Not Detected
Bromodichloromethane
0.19
Not Detected
1.3
Not Detected
cis-1,3-Dichloropropene
0.19
Not Detected
0.88
Not Detected
4-Methyl-2-pentanone
0.19
Not Detected
0.79
Not Detected
Toluene
1.9
Not Detected
7.3
Not Detected
trans-1,3-Dichloropropene
0.19
Not Detected
0.88
Not Detected
1,1,2-Trichloroethane
0.19
Not Detected
1.0
Not Detected
Tetrachloroethene
0.19
7.5
1.3
51
2-Hexanone
0.96
Not Detected
4.0
Not Detected
Page 19 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-5
Lab ID#: 2305750-05A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061217 Date of Collection: 5/22/23 10:21:00 AM
Dil. Factor: 1.93 Date of Analysis: 6/12/23 09:53 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.19
Not Detected
1.6
Not Detected
1,2-Dibromoethane (EDB)
0.19
Not Detected
1.5
Not Detected
Chlorobenzene
0.19
Not Detected
0.89
Not Detected
Ethyl Benzene
0.19
Not Detected
0.84
Not Detected
m,p-Xylene
0.19
Not Detected
0.84
Not Detected
o-Xylene
0.19
Not Detected
0.84
Not Detected
Styrene
0.19
Not Detected
0.82
Not Detected
Bromoform
0.19
Not Detected
2.0
Not Detected
Cumene
0.19
Not Detected
0.95
Not Detected
1,1,2,2-Tetrachloroethane
0.19
Not Detected
1.3
Not Detected
Propylbenzene
0.19
Not Detected
0.95
Not Detected
4-Ethyltoluene
0.19
Not Detected
0.95
Not Detected
1,3,5-Trimethyl benzene
0.19
Not Detected
0.95
Not Detected
1,2,4-Trimethyl benzene
0.19
Not Detected
0.95
Not Detected
1,3-Dichlorobenzene
0.19
Not Detected
1.2
Not Detected
1,4-Dichlorobenzene
0.19
Not Detected
1.2
Not Detected
alpha-Chlorotoluene
0.19
Not Detected
1.0
Not Detected
1,2-Dichlorobenzene
0.19
Not Detected
1.2
Not Detected
1,2,4-Trichlorobenzene
0.96
Not Detected
7.2
Not Detected
Hexachlorobutadiene
0.96
Not Detected
10
Not Detected
Naphthalene
0.39
Not Detected
2.0
Not Detected
UJ = Analyte associated with low bias in the CCV.
Container Type: 1 Liter Summa Canister (100% Certified)
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 118 70-130
Toluene-d8 104 70-130
4-Bromofluorobenzene 94 70-130
Page 20 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-6
Lab ID#: 2305750-06A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061218 Date of Collection: 5/22/23 8:55:00 AM
Dil. Factor: 1.87 Date of Analysis: 6/12/23 10:31 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
0.94
Not Detected
4.6
Not Detected
Freon 114
0.19
Not Detected
1.3
Not Detected
Chloromethane
0.94
Not Detected
1.9
Not Detected
Vinyl Chloride
0.19
Not Detected
0.48
Not Detected
1,3-Butadiene
0.19
Not Detected
0.41
Not Detected
Bromomethane
9.4
Not Detected
36
Not Detected
Chloroethane
0.94
Not Detected
2.5
Not Detected
Freon 11
0.19
0.20
1.0
1.1
Ethanol
12
30
22
57
Freon 113
0.19
Not Detected
1.4
Not Detected
1,1-Dichloroethene
0.19
Not Detected
0.74
Not Detected
Acetone
3.7
8.3
8.9
20
2-Propanol
3.7
Not Detected
9.2
Not Detected
Carbon Disulfide
9.4
Not Detected
29
Not Detected
3-Chloropropene
0.94
Not Detected
2.9
Not Detected
Methylene Chloride
0.94
Not Detected
3.2
Not Detected
Methyl tert-butyl ether
0.19
Not Detected
0.67
Not Detected
trans- 1,2-Dichloroethene
0.19
Not Detected
0.74
Not Detected
Hexane
0.94
Not Detected
3.3
Not Detected
1,1-Dichloroethane
0.19
Not Detected
0.76
Not Detected
2-Butanone (Methyl Ethyl Ketone)
3.7
Not Detected
11
Not Detected
cis-1,2-Dichloroethene
0.19
Not Detected
0.74
Not Detected
Tetrahydrofuran
0.94
Not Detected
2.8
Not Detected
Chloroform
0.19
0.43
0.91
2.1
1, 1, 1 -Trichloroethane
0.19
Not Detected
1.0
Not Detected
Cyclohexane
0.94
Not Detected
3.2
Not Detected
Carbon Tetrachloride
0.19
Not Detected UJ
1.2
Not Detected UJ
2,2,4-Trimethylpentane
0.94
8.5
4.4
40
Benzene
0.19
0.43
0.60
1.4
1,2-Dichloroethane
0.19
Not Detected
0.76
Not Detected
Heptane
0.94
Not Detected
3.8
Not Detected
Trichloroethene
0.19
Not Detected
1.0
Not Detected
1,2-Dichloropropane
0.19
Not Detected
0.86
Not Detected
1,4-Dioxane
0.94
Not Detected
3.4
Not Detected
Bromodichloromethane
0.19
Not Detected
1.2
Not Detected
cis-1,3-Dichloropropene
0.19
Not Detected
0.85
Not Detected
4-Methyl-2-pentanone
0.19
Not Detected
0.77
Not Detected
Toluene
1.9
Not Detected
7.0
Not Detected
trans-1,3-Dichloropropene
0.19
Not Detected
0.85
Not Detected
1,1,2-Trichloroethane
0.19
Not Detected
1.0
Not Detected
Tetrachloroethene
0.19
1.1
1.3
7.8
2-Hexanone
0.94
Not Detected
3.8
Not Detected
Page 21 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-6
Lab ID#: 2305750-06A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061218 Date of Collection: 5/22/23 8:55:00 AM
Dil. Factor: 1.87 Date of Analysis: 6/12/23 10:31 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.19
Not Detected
1.6
Not Detected
1,2-Dibromoethane (EDB)
0.19
Not Detected
1.4
Not Detected
Chlorobenzene
0.19
Not Detected
0.86
Not Detected
Ethyl Benzene
0.19
0.76
0.81
3.3
m,p-Xylene
0.19
1.9
0.81
8.3
o-Xylene
0.19
0.92
0.81
4.0
Styrene
0.19
Not Detected
0.80
Not Detected
Bromoform
0.19
Not Detected
1.9
Not Detected
Cumene
0.19
Not Detected
0.92
Not Detected
1,1,2,2-Tetrachloroethane
0.19
Not Detected
1.3
Not Detected
Propylbenzene
0.19
0.22
0.92
1.1
4-Ethyltoluene
0.19
0.56
0.92
2.8
1,3,5-Trimethyl benzene
0.19
Not Detected
0.92
Not Detected
1,2,4-Trimethyl benzene
0.19
0.67
0.92
3.3
1,3-Dichlorobenzene
0.19
Not Detected
1.1
Not Detected
1,4-Dichlorobenzene
0.19
Not Detected
1.1
Not Detected
alpha-Chlorotoluene
0.19
Not Detected
0.97
Not Detected
1,2-Dichlorobenzene
0.19
Not Detected
1.1
Not Detected
1,2,4-Trichlorobenzene
0.94
Not Detected
6.9
Not Detected
Hexachlorobutadiene
0.94
Not Detected
10
Not Detected
Naphthalene
0.37
Not Detected
2.0
Not Detected
UJ = Analyte associated with low bias in the CCV.
Container Type: 1 Liter Summa Canister (100% Certified)
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 119 70-130
Toluene-d8 106 70-130
4-Bromofluorobenzene 95 70-130
Page 22 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-7
Lab ID#: 2305750-07A
MODIFIED EPA METHOD TO-15 GUMS FULL SCAN
File Name: 21061219 Date of Collection: 5/22/23 2:26:00 PM
Dil. Factor: 2.05 Date of Analysis: 6/12/23 11:09 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
1.0
Not Detected
5.1
Not Detected
Freon 114
0.20
Not Detected
1.4
Not Detected
Chloromethane
1.0
Not Detected
2.1
Not Detected
Vinyl Chloride
0.20
0.26
0.52
0.65
1,3-Butadiene
0.20
Not Detected
0.45
Not Detected
Bromomethane
10
Not Detected
40
Not Detected
Chloroethane
1.0
Not Detected
2.7
Not Detected
Freon 11
0.20
0.26
1.2
1.4
Ethanol
13
26
24
48
Freon 113
0.20
Not Detected
1.6
Not Detected
1,1-Dichloroethene
0.20
Not Detected
0.81
Not Detected
Acetone
4.1
80
9.7
190
2-Propanol
4.1
Not Detected
10
Not Detected
Carbon Disulfide
10
Not Detected
32
Not Detected
3-Chloropropene
1.0
Not Detected
3.2
Not Detected
Methylene Chloride
1.0
1.0
3.6
3.7
Methyl tert-butyl ether
0.20
Not Detected
0.74
Not Detected
trans- 1,2-Dichloroethene
0.20
Not Detected
0.81
Not Detected
Hexane
1.0
Not Detected
3.6
Not Detected
1,1-Dichloroethane
0.20
Not Detected
0.83
Not Detected
2-Butanone (Methyl Ethyl Ketone)
4.1
Not Detected
12
Not Detected
cis-1,2-Dichloroethene
0.20
Not Detected
0.81
Not Detected
Tetrahydrofuran
1.0
Not Detected
3.0
Not Detected
Chloroform
0.20
0.22
1.0
1.1
1, 1, 1 -Trichloroethane
0.20
Not Detected
1.1
Not Detected
Cyclohexane
1.0
2.3
3.5
7.9
Carbon Tetrachloride
0.20
Not Detected UJ
1.3
Not Detected UJ
2,2,4-Trimethylpentane
1.0
15
4.8
70
Benzene
0.20
0.34
0.65
1.1
1,2-Dichloroethane
0.20
Not Detected
0.83
Not Detected
Heptane
1.0
Not Detected
4.2
Not Detected
Trichloroethene
0.20
Not Detected
1.1
Not Detected
1,2-Dichloropropane
0.20
Not Detected
0.95
Not Detected
1,4-Dioxane
1.0
Not Detected
3.7
Not Detected
Bromodichloromethane
0.20
Not Detected
1.4
Not Detected
cis-1,3-Dichloropropene
0.20
Not Detected
0.93
Not Detected
4-Methyl-2-pentanone
0.20
Not Detected
0.84
Not Detected
Toluene
2.0
Not Detected
7.7
Not Detected
trans-1,3-Dichloropropene
0.20
Not Detected
0.93
Not Detected
1,1,2-Trichloroethane
0.20
Not Detected
1.1
Not Detected
Tetrachloroethene
0.20
0.28
1.4
1.9
2-Hexanone
1.0
Not Detected
4.2
Not Detected
Page 23 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-7
Lab ID#: 2305750-07A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061219 Date of Collection: 5/22/23 2:26:00 PM
Dil. Factor: 2.05 Date of Analysis: 6/12/23 11:09 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.20
Not Detected
1.7
Not Detected
1,2-Dibromoethane (EDB)
0.20
Not Detected
1.6
Not Detected
Chlorobenzene
0.20
Not Detected
0.94
Not Detected
Ethyl Benzene
0.20
0.31
0.89
1.3
m, p-Xylene
0.20
0.76
0.89
3.3
o-Xylene
0.20
0.88
0.89
3.8
Styrene
0.20
Not Detected
0.87
Not Detected
Bromoform
0.20
Not Detected
2.1
Not Detected
Cumene
0.20
Not Detected
1.0
Not Detected
1,1,2,2-Tetrachloroethane
0.20
Not Detected
1.4
Not Detected
Propylbenzene
0.20
Not Detected
1.0
Not Detected
4-Ethyltoluene
0.20
Not Detected
1.0
Not Detected
1,3,5-Trimethyl benzene
0.20
Not Detected
1.0
Not Detected
1,2,4-Trimethyl benzene
0.20
0.40
1.0
2.0
1,3-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,4-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
alpha-Chlorotoluene
0.20
Not Detected
1.1
Not Detected
1,2-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,2,4-Trichlorobenzene
1.0
Not Detected
7.6
Not Detected
Hexachlorobutadiene
1.0
Not Detected
11
Not Detected
Naphthalene
0.41
Not Detected
2.1
Not Detected
UJ = Analyte associated with low bias in the CCV.
Container Type: 1 Liter Summa Canister (100% Certified)
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 118 70-130
Toluene-d8 100 70-130
4-Bromofluorobenzene 96 70-130
Page 24 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-8
Lab ID#: 2305750-08A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061220 Date of Collection: 5/22/23 2:17:00 PM
Dil. Factor: 2.02 Date of Analysis: 6/12/23 11:46 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
1.0
Not Detected
5.0
Not Detected
Freon 114
0.20
Not Detected
1.4
Not Detected
Chloromethane
1.0
Not Detected
2.1
Not Detected
Vinyl Chloride
0.20
Not Detected
0.52
Not Detected
1,3-Butadiene
0.20
Not Detected
0.45
Not Detected
Bromomethane
10
Not Detected
39
Not Detected
Chloroethane
1.0
Not Detected
2.7
Not Detected
Freon 11
0.20
0.21
1.1
1.2
Ethanol
12
Not Detected
24
Not Detected
Freon 113
0.20
Not Detected
1.5
Not Detected
1,1-Dichloroethene
0.20
Not Detected
0.80
Not Detected
Acetone
4.0
6.5
9.6
15
2-Propanol
4.0
Not Detected
9.9
Not Detected
Carbon Disulfide
10
Not Detected
31
Not Detected
3-Chloropropene
1.0
Not Detected
3.2
Not Detected
Methylene Chloride
1.0
Not Detected
3.5
Not Detected
Methyl tert-butyl ether
0.20
Not Detected
0.73
Not Detected
trans- 1,2-Dichloroethene
0.20
Not Detected
0.80
Not Detected
Hexane
1.0
Not Detected
3.6
Not Detected
1,1-Dichloroethane
0.20
Not Detected
0.82
Not Detected
2-Butanone (Methyl Ethyl Ketone)
4.0
Not Detected
12
Not Detected
cis-1,2-Dichloroethene
0.20
Not Detected
0.80
Not Detected
Tetrahydrofuran
1.0
Not Detected
3.0
Not Detected
Chloroform
0.20
0.38
0.99
1.8
1, 1, 1 -Trichloroethane
0.20
Not Detected
1.1
Not Detected
Cyclohexane
1.0
Not Detected
3.5
Not Detected
Carbon Tetrachloride
0.20
Not Detected UJ
1.3
Not Detected UJ
2,2,4-Trimethylpentane
1.0
Not Detected
4.7
Not Detected
Benzene
0.20
0.20 J
0.64
0.63 J
1,2-Dichloroethane
0.20
Not Detected
0.82
Not Detected
Heptane
1.0
Not Detected
4.1
Not Detected
Trichloroethene
0.20
Not Detected
1.1
Not Detected
1,2-Dichloropropane
0.20
Not Detected
0.93
Not Detected
1,4-Dioxane
1.0
Not Detected
3.6
Not Detected
Bromodichloromethane
0.20
Not Detected
1.4
Not Detected
cis-1,3-Dichloropropene
0.20
Not Detected
0.92
Not Detected
4-Methyl-2-pentanone
0.20
Not Detected
0.83
Not Detected
Toluene
2.0
4.1
7.6
15
trans-1,3-Dichloropropene
0.20
Not Detected
0.92
Not Detected
1,1,2-Trichloroethane
0.20
Not Detected
1.1
Not Detected
Tetrachloroethene
0.20
0.58
1.4
3.9
2-Hexanone
1.0
Not Detected
4.1
Not Detected
Page 25 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-8
Lab ID#: 2305750-08A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061220 Date of Collection: 5/22/23 2:17:00 PM
Dil. Factor: 2.02 Date of Analysis: 6/12/23 11:46 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.20
Not Detected
1.7
Not Detected
1,2-Dibromoethane (EDB)
0.20
Not Detected
1.6
Not Detected
Chlorobenzene
0.20
Not Detected
0.93
Not Detected
Ethyl Benzene
0.20
3.4
0.88
15
m, p-Xylene
0.20
28
0.88
120
o-Xylene
0.20
13
0.88
55
Styrene
0.20
Not Detected
0.86
Not Detected
Bromoform
0.20
Not Detected
2.1
Not Detected
Cumene
0.20
0.71
0.99
3.5
1,1,2,2-Tetrachloroethane
0.20
Not Detected
1.4
Not Detected
Propylbenzene
0.20
1.0
0.99
4.9
4-Ethyltoluene
0.20
7.1
0.99
35
1,3,5-Trimethyl benzene
0.20
1.6
0.99
7.6
1,2,4-Trimethyl benzene
0.20
9.5
0.99
47
1,3-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,4-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
alpha-Chlorotoluene
0.20
Not Detected
1.0
Not Detected
1,2-Dichlorobenzene
0.20
Not Detected
1.2
Not Detected
1,2,4-Trichlorobenzene
1.0
Not Detected
7.5
Not Detected
Hexachlorobutadiene
1.0
Not Detected
11
Not Detected
Naphthalene
0.40
Not Detected
2.1
Not Detected
UJ = Analyte associated with low bias in the CCV.
J = Estimated value.
Container Type: 1 Liter Summa Canister (100% Certified)
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 123 70-130
Toluene-d8 103 70-130
4-Bromofluorobenzene 97 70-130
Page 26 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-9
Lab ID#: 2305750-09A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061221 Date of Collection: 5/22/23 2:34:00 PM
Dil. Factor: 9.65 Date of Analysis: 6/13/23 12:24 AM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
4.8
Not Detected
24
Not Detected
Freon 114
0.96
Not Detected
6.7
Not Detected
Chloromethane
4.8
Not Detected
10
Not Detected
Vinyl Chloride
0.96
Not Detected
2.5
Not Detected
1,3-Butadiene
0.96
Not Detected
2.1
Not Detected
Bromomethane
48
Not Detected
190
Not Detected
Chloroethane
4.8
Not Detected
13
Not Detected
Freon 11
0.96
Not Detected
5.4
Not Detected
Ethanol
60
Not Detected
110
Not Detected
Freon 113
0.96
Not Detected
7.4
Not Detected
1,1-Dichloroethene
0.96
Not Detected
3.8
Not Detected
Acetone
19
Not Detected
46
Not Detected
2-Propanol
19
Not Detected
47
Not Detected
Carbon Disulfide
48
Not Detected
150
Not Detected
3-Chloropropene
4.8
Not Detected
15
Not Detected
Methylene Chloride
4.8
Not Detected
17
Not Detected
Methyl tert-butyl ether
0.96
Not Detected
3.5
Not Detected
trans- 1,2-Dichloroethene
0.96
Not Detected
3.8
Not Detected
Hexane
4.8
Not Detected
17
Not Detected
1,1-Dichloroethane
0.96
Not Detected
3.9
Not Detected
2-Butanone (Methyl Ethyl Ketone)
19
Not Detected
57
Not Detected
cis-1,2-Dichloroethene
0.96
Not Detected
3.8
Not Detected
Tetrahydrofuran
4.8
Not Detected
14
Not Detected
Chloroform
0.96
Not Detected
4.7
Not Detected
1, 1, 1 -Trichloroethane
0.96
Not Detected
5.3
Not Detected
Cyclohexane
4.8
Not Detected
17
Not Detected
Carbon Tetrachloride
0.96
Not Detected UJ
6.1
Not Detected UJ
2,2,4-Trimethylpentane
4.8
47
22
220
Benzene
0.96
1.7
3.1
5.3
1,2-Dichloroethane
0.96
Not Detected
3.9
Not Detected
Heptane
4.8
5.8
20
24
Trichloroethene
0.96
Not Detected
5.2
Not Detected
1,2-Dichloropropane
0.96
Not Detected
4.4
Not Detected
1,4-Dioxane
4.8
Not Detected
17
Not Detected
Bromodichloromethane
0.96
Not Detected
6.5
Not Detected
cis-1,3-Dichloropropene
0.96
Not Detected
4.4
Not Detected
4-Methyl-2-pentanone
0.96
Not Detected
4.0
Not Detected
Toluene
9.6
30
36
120
trans-1,3-Dichloropropene
0.96
Not Detected
4.4
Not Detected
1,1,2-Trichloroethane
0.96
Not Detected
5.3
Not Detected
Tetrachloroethene
0.96
0.99
6.5
6.7
2-Hexanone
4.8
Not Detected
20
Not Detected
Page 27 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-9
Lab ID#: 2305750-09A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061221 Date of Collection: 5/22/23 2:34:00 PM
Dil. Factor: 9.65 Date of Analysis: 6/13/23 12:24 AM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.96
Not Detected
8.2
Not Detected
1,2-Dibromoethane (EDB)
0.96
Not Detected
7.4
Not Detected
Chlorobenzene
0.96
Not Detected
4.4
Not Detected
Ethyl Benzene
0.96
10
4.2
44
m, p-Xylene
0.96
68
4.2
290
o-Xylene
0.96
26
4.2
110
Styrene
0.96
Not Detected
4.1
Not Detected
Bromoform
0.96
Not Detected
10
Not Detected
Cumene
0.96
Not Detected
4.7
Not Detected
1,1,2,2-Tetrachloroethane
0.96
Not Detected
6.6
Not Detected
Propylbenzene
0.96
4.0
4.7
19
4-Ethyltoluene
0.96
21
4.7
100
1,3,5-Trimethyl benzene
0.96
18
4.7
87
1,2,4-Trimethyl benzene
0.96
42
4.7
210
1,3-Dichlorobenzene
0.96
Not Detected
5.8
Not Detected
1,4-Dichlorobenzene
0.96
Not Detected
5.8
Not Detected
alpha-Chlorotoluene
0.96
Not Detected
5.0
Not Detected
1,2-Dichlorobenzene
0.96
Not Detected
5.8
Not Detected
1,2,4-Trichlorobenzene
4.8
Not Detected
36
Not Detected
Hexachlorobutadiene
4.8
Not Detected
51
Not Detected
Naphthalene
1.9
Not Detected
10
Not Detected
UJ = Analyte associated with low bias in the CCV.
Container Type: 1 Liter Summa Canister (100% Certified)
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 116 70-130
Toluene-d8 103 70-130
4-Bromofluorobenzene 126 70-130
Page 28 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-10
Lab ID#: 2305750-10A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061223 Date of Collection: 5/22/23 2:42:00 PM
Dil. Factor: 2.20 Date of Analysis: 6/13/23 02:32 AM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
1.1
Not Detected
5.4
Not Detected
Freon 114
0.22
Not Detected
1.5
Not Detected
Chloromethane
1.1
Not Detected
2.3
Not Detected
Vinyl Chloride
0.22
Not Detected
0.56
Not Detected
1,3-Butadiene
0.22
Not Detected
0.49
Not Detected
Bromomethane
11
Not Detected
43
Not Detected
Chloroethane
1.1
Not Detected
2.9
Not Detected
Freon 11
0.22
0.24
1.2
1.3
Ethanol
14
Not Detected
26
Not Detected
Freon 113
0.22
Not Detected
1.7
Not Detected
1,1-Dichloroethene
0.22
Not Detected
0.87
Not Detected
Acetone
4.4
8.2
10
20
2-Propanol
4.4
Not Detected
11
Not Detected
Carbon Disulfide
11
Not Detected
34
Not Detected
3-Chloropropene
1.1
Not Detected
3.4
Not Detected
Methylene Chloride
1.1
Not Detected
3.8
Not Detected
Methyl tert-butyl ether
0.22
Not Detected
0.79
Not Detected
trans- 1,2-Dichloroethene
0.22
Not Detected
0.87
Not Detected
Hexane
1.1
Not Detected
3.9
Not Detected
1,1-Dichloroethane
0.22
Not Detected
0.89
Not Detected
2-Butanone (Methyl Ethyl Ketone)
4.4
Not Detected
13
Not Detected
cis-1,2-Dichloroethene
0.22
Not Detected
0.87
Not Detected
Tetrahydrofuran
1.1
Not Detected
3.2
Not Detected
Chloroform
0.22
1.2
1.1
6.1
1, 1, 1 -Trichloroethane
0.22
Not Detected
1.2
Not Detected
Cyclohexane
1.1
Not Detected
3.8
Not Detected
Carbon Tetrachloride
0.22
Not Detected UJ
1.4
Not Detected UJ
2,2,4-Trimethylpentane
1.1
3.7
5.1
18
Benzene
0.22
3.8
0.70
12
1,2-Dichloroethane
0.22
Not Detected
0.89
Not Detected
Heptane
1.1
Not Detected
4.5
Not Detected
Trichloroethene
0.22
0.22
1.2
1.2
1,2-Dichloropropane
0.22
Not Detected
1.0
Not Detected
1,4-Dioxane
1.1
Not Detected
4.0
Not Detected
Bromodichloromethane
0.22
Not Detected
1.5
Not Detected
cis-1,3-Dichloropropene
0.22
Not Detected
1.0
Not Detected
4-Methyl-2-pentanone
0.22
Not Detected
0.90
Not Detected
Toluene
2.2
45
8.3
170
trans-1,3-Dichloropropene
0.22
Not Detected
1.0
Not Detected
1,1,2-Trichloroethane
0.22
Not Detected
1.2
Not Detected
Tetrachloroethene
0.22
2.6
1.5
17
2-Hexanone
1.1
Not Detected
4.5
Not Detected
Page 29 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: VP-10
Lab ID#: 2305750-10A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061223 Date of Collection: 5/22/23 2:42:00 PM
Dil. Factor: 2.20 Date of Analysis: 6/13/23 02:32 AM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.22
Not Detected
1.9
Not Detected
1,2-Dibromoethane (EDB)
0.22
Not Detected
1.7
Not Detected
Chlorobenzene
0.22
Not Detected
1.0
Not Detected
Ethyl Benzene
0.22
12
0.96
53
m, p-Xylene
0.22
46
0.96
200
o-Xylene
0.22
21
0.96
91
Styrene
0.22
Not Detected
0.94
Not Detected
Bromoform
0.22
Not Detected
2.3
Not Detected
Cumene
0.22
1.8
1.1
8.7
1,1,2,2-Tetrachloroethane
0.22
Not Detected
1.5
Not Detected
Propylbenzene
0.22
3.6
1.1
18
4-Ethyltoluene
0.22
14
1.1
69
1,3,5-Trimethyl benzene
0.22
7.5
1.1
37
1,2,4-Trimethyl benzene
0.22
16
1.1
79
1,3-Dichlorobenzene
0.22
Not Detected
1.3
Not Detected
1,4-Dichlorobenzene
0.22
Not Detected
1.3
Not Detected
alpha-Chlorotoluene
0.22
Not Detected
1.1
Not Detected
1,2-Dichlorobenzene
0.22
Not Detected
1.3
Not Detected
1,2,4-Trichlorobenzene
1.1
Not Detected
8.2
Not Detected
Hexachlorobutadiene
1.1
Not Detected
12
Not Detected
Naphthalene
0.44
Not Detected
2.3
Not Detected
UJ = Analyte associated with low bias in the CCV.
Container Type: 1 Liter Summa Canister (100% Certified)
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 126 70-130
Toluene-d8 108 70-130
4-Bromofluorobenzene 100 70-130
Page 30 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: DUP
Lab ID#: 2305750-11A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061224 Date of Collection: 5/22/23 12:06:00 PM
Dil. Factor: 9.85 Date of Analysis: 6/13/23 04:02 AM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
4.9
Not Detected
24
Not Detected
Freon 114
0.98
Not Detected
6.9
Not Detected
Chloromethane
4.9
Not Detected
10
Not Detected
Vinyl Chloride
0.98
Not Detected
2.5
Not Detected
1,3-Butadiene
0.98
Not Detected
2.2
Not Detected
Bromomethane
49
Not Detected
190
Not Detected
Chloroethane
4.9
Not Detected
13
Not Detected
Freon 11
0.98
Not Detected
5.5
Not Detected
Ethanol
61
Not Detected
120
Not Detected
Freon 113
0.98
Not Detected
7.5
Not Detected
1,1-Dichloroethene
0.98
Not Detected
3.9
Not Detected
Acetone
20
69
47
160
2-Propanol
20
Not Detected
48
Not Detected
Carbon Disulfide
49
Not Detected
150
Not Detected
3-Chloropropene
4.9
Not Detected
15
Not Detected
Methylene Chloride
4.9
Not Detected
17
Not Detected
Methyl tert-butyl ether
0.98
Not Detected
3.6
Not Detected
trans- 1,2-Dichloroethene
0.98
Not Detected
3.9
Not Detected
Hexane
4.9
Not Detected
17
Not Detected
1,1-Dichloroethane
0.98
Not Detected
4.0
Not Detected
2-Butanone (Methyl Ethyl Ketone)
20
Not Detected
58
Not Detected
cis-1,2-Dichloroethene
0.98
Not Detected
3.9
Not Detected
Tetrahydrofuran
4.9
Not Detected
14
Not Detected
Chloroform
0.98
Not Detected
4.8
Not Detected
1, 1, 1 -Trichloroethane
0.98
Not Detected
5.4
Not Detected
Cyclohexane
4.9
Not Detected
17
Not Detected
Carbon Tetrachloride
0.98
Not Detected UJ
6.2
Not Detected UJ
2,2,4-Trimethylpentane
4.9
34
23
160
Benzene
0.98
1.4
3.1
4.4
1,2-Dichloroethane
0.98
Not Detected
4.0
Not Detected
Heptane
4.9
5.5
20
22
Trichloroethene
0.98
Not Detected
5.3
Not Detected
1,2-Dichloropropane
0.98
Not Detected
4.6
Not Detected
1,4-Dioxane
4.9
Not Detected
18
Not Detected
Bromodichloromethane
0.98
Not Detected
6.6
Not Detected
cis-1,3-Dichloropropene
0.98
Not Detected
4.5
Not Detected
4-Methyl-2-pentanone
0.98
Not Detected
4.0
Not Detected
Toluene
9.8
27
37
100
trans-1,3-Dichloropropene
0.98
Not Detected
4.5
Not Detected
1,1,2-Trichloroethane
0.98
Not Detected
5.4
Not Detected
Tetrachloroethene
0.98
Not Detected
6.7
Not Detected
2-Hexanone
4.9
Not Detected
20
Not Detected
Page 31 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: DUP
Lab ID#: 2305750-11A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061224 Date of Collection: 5/22/23 12:06:00 PM
Dil. Factor: 9.85 Date of Analysis: 6/13/23 04:02 AM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.98
Not Detected
8.4
Not Detected
1,2-Dibromoethane (EDB)
0.98
Not Detected
7.6
Not Detected
Chlorobenzene
0.98
Not Detected
4.5
Not Detected
Ethyl Benzene
0.98
8.9
4.3
38
m, p-Xylene
0.98
56
4.3
240
o-Xylene
0.98
23
4.3
100
Styrene
0.98
Not Detected
4.2
Not Detected
Bromoform
0.98
Not Detected
10
Not Detected
Cumene
0.98
Not Detected
4.8
Not Detected
1,1,2,2-Tetrachloroethane
0.98
Not Detected
6.8
Not Detected
Propylbenzene
0.98
3.5
4.8
17
4-Ethyltoluene
0.98
18
4.8
88
1,3,5-Trimethyl benzene
0.98
16
4.8
80
1,2,4-Trimethyl benzene
0.98
39
4.8
190
1,3-Dichlorobenzene
0.98
Not Detected
5.9
Not Detected
1,4-Dichlorobenzene
0.98
Not Detected
5.9
Not Detected
alpha-Chlorotoluene
0.98
Not Detected
5.1
Not Detected
1,2-Dichlorobenzene
0.98
Not Detected
5.9
Not Detected
1,2,4-Trichlorobenzene
4.9
Not Detected
36
Not Detected
Hexachlorobutadiene
4.9
Not Detected
52
Not Detected
Naphthalene
2.0
Not Detected
10
Not Detected
UJ = Analyte associated with low bias in the CCV.
Container Type: 1 Liter Summa Canister (100% Certified)
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 115 70-130
Toluene-d8 99 70-130
4-Bromofluorobenzene 118 70-130
Page 32 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: Lab Blank
Lab ID#: 2305750-12A
MODIFIED EPA METHOD TO-15 GUMS FULL SCAN
File Name: 21061206c Date of Collection: NA
Dil. Factor: 1.00 Date of Analysis: 6/12/23 12:05 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Freon 12
0.50
Not Detected
2.5
Not Detected
Freon 114
0.10
Not Detected
0.70
Not Detected
Chloromethane
0.50
Not Detected
1.0
Not Detected
Vinyl Chloride
0.10
Not Detected
0.26
Not Detected
1,3-Butadiene
0.10
Not Detected
0.22
Not Detected
Bromomethane
5.0
Not Detected
19
Not Detected
Chloroethane
0.50
Not Detected
1.3
Not Detected
Freon 11
0.10
Not Detected
0.56
Not Detected
Ethanol
6.2
Not Detected
12
Not Detected
Freon 113
0.10
Not Detected
0.77
Not Detected
1,1-Dichloroethene
0.10
Not Detected
0.40
Not Detected
Acetone
2.0
Not Detected
4.8
Not Detected
2-Propanol
2.0
Not Detected
4.9
Not Detected
Carbon Disulfide
5.0
Not Detected
16
Not Detected
3-Chloropropene
0.50
Not Detected
1.6
Not Detected
Methylene Chloride
0.50
Not Detected
1.7
Not Detected
Methyl tert-butyl ether
0.10
Not Detected
0.36
Not Detected
trans- 1,2-Dichloroethene
0.10
Not Detected
0.40
Not Detected
Hexane
0.50
Not Detected
1.8
Not Detected
1,1-Dichloroethane
0.10
Not Detected
0.40
Not Detected
2-Butanone (Methyl Ethyl Ketone)
2.0
Not Detected
5.9
Not Detected
cis-1,2-Dichloroethene
0.10
Not Detected
0.40
Not Detected
Tetrahydrofuran
0.50
Not Detected
1.5
Not Detected
Chloroform
0.10
Not Detected
0.49
Not Detected
1, 1, 1 -Trichloroethane
0.10
Not Detected
0.54
Not Detected
Cyclohexane
0.50
Not Detected
1.7
Not Detected
Carbon Tetrachloride
0.10
Not Detected UJ
0.63
Not Detected UJ
2,2,4-Trimethylpentane
0.50
Not Detected
2.3
Not Detected
Benzene
0.10
Not Detected
0.32
Not Detected
1,2-Dichloroethane
0.10
Not Detected
0.40
Not Detected
Heptane
0.50
Not Detected
2.0
Not Detected
Trichloroethene
0.10
Not Detected
0.54
Not Detected
1,2-Dichloropropane
0.10
Not Detected
0.46
Not Detected
1,4-Dioxane
0.50
Not Detected
1.8
Not Detected
Bromodichloromethane
0.10
Not Detected
0.67
Not Detected
cis-1,3-Dichloropropene
0.10
Not Detected
0.45
Not Detected
4-Methyl-2-pentanone
0.10
Not Detected
0.41
Not Detected
Toluene
1.0
Not Detected
3.8
Not Detected
trans-1,3-Dichloropropene
0.10
Not Detected
0.45
Not Detected
1,1,2-Trichloroethane
0.10
Not Detected
0.54
Not Detected
Tetrachloroethene
0.10
Not Detected
0.68
Not Detected
2-Hexanone
0.50
Not Detected
2.0
Not Detected
Page 33 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: Lab Blank
Lab ID#: 2305750-12A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061206c Date of Collection: NA
Dil. Factor: 1.00 Date of Analysis: 6/12/23 12:05 PM
Rpt. Limit
Amount
Rpt. Limit
Amount
Compound
(ppbv)
(ppbv)
(ug/m3)
(ug/m3)
Dibromochloromethane
0.10
Not Detected
0.85
Not Detected
1,2-Dibromoethane (EDB)
0.10
Not Detected
0.77
Not Detected
Chlorobenzene
0.10
Not Detected
0.46
Not Detected
Ethyl Benzene
0.10
Not Detected
0.43
Not Detected
m,p-Xylene
0.10
Not Detected
0.43
Not Detected
o-Xylene
0.10
Not Detected
0.43
Not Detected
Styrene
0.10
Not Detected
0.42
Not Detected
Bromoform
0.10
Not Detected
1.0
Not Detected
Cumene
0.10
Not Detected
0.49
Not Detected
1,1,2,2-Tetrachloroethane
0.10
Not Detected
0.69
Not Detected
Propylbenzene
0.10
Not Detected
0.49
Not Detected
4-Ethyltoluene
0.10
Not Detected
0.49
Not Detected
1,3,5-Trimethyl benzene
0.10
Not Detected
0.49
Not Detected
1,2,4-Trimethyl benzene
0.10
Not Detected
0.49
Not Detected
1,3-Dichlorobenzene
0.10
Not Detected
0.60
Not Detected
1,4-Dichlorobenzene
0.10
Not Detected
0.60
Not Detected
alpha-Chlorotoluene
0.10
Not Detected
0.52
Not Detected
1,2-Dichlorobenzene
0.10
Not Detected
0.60
Not Detected
1,2,4-Trichlorobenzene
0.50
Not Detected
3.7
Not Detected
Hexachlorobutadiene
0.50
Not Detected
5.3
Not Detected
Naphthalene
0.20
Not Detected
1.0
Not Detected
UJ = Analyte associated with low bias in the CCV.
Container Type: NA - Not Applicable
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 130 70-130
Toluene-d8 100 70-130
4-Bromofluorobenzene 88 70-130
Page 34 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: CCV
Lab ID#: 2305750-13A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061202 Date of Collection: NA
Dil. Factor: 1.00 Date of Analysis: 6/12/23 08:22 AM
Compound %Recovery
Freon 12
94
Freon 114
85
Chloromethane
81
Vinyl Chloride
93
1,3-Butadiene
96
Bromomethane
129
Chloroethane
85
Freon 11
86
Ethanol
91
Freon 113
84
1,1-Dichloroethene
90
Acetone
89
2-Propanol
86
Carbon Disulfide
93
3-Chloropropene
96
Methylene Chloride
87
Methyl tert-butyl ether
85
trans- 1,2-Dichloroethene
90
Hexane
90
1,1-Dichloroethane
93
2-Butanone (Methyl Ethyl Ketone)
98
cis-1,2-Dichloroethene
85
Tetrahydrofuran
90
Chloroform
90
1,1,1-Trichloroethane
85
Cyclohexane
87
Carbon Tetrachloride
67 Q
2,2,4-Trimethylpentane
93
Benzene
112
1,2-Dichloroethane
109
Heptane
114
Trichloroethene
104
1,2-Dichloropropane
112
1,4-Dioxane
107
Bromodichloromethane
98
cis-1,3-Dichloropropene
105
4-Methyl-2-pentanone
108
Toluene
108
trans-1,3-Dichloropropene
100
1,1,2-Trichloroethane
94
Tetrachloroethene
86
2-Hexanone
102
Page 35 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: CCV
Lab ID#: 2305750-13A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061202 Date of Collection: NA
Dil. Factor: 1.00 Date of Analysis: 6/12/23 08:22 AM
Compound %Recovery
Dibromochloromethane
88
1,2-Dibromoethane (EDB)
94
Chlorobenzene
89
Ethyl Benzene
98
m,p-Xylene
89
o-Xylene
82
Styrene
94
Bromoform
82
Cumene
88
1,1,2,2-Tetrachloroethane
91
Propylbenzene
80
4-Ethyltoluene
80
1,3,5-Trimethyl benzene
96
1,2,4-Trimethyl benzene
90
1,3-Dichlorobenzene
86
1,4-Dichlorobenzene
80
alpha-Chlorotoluene
94
1,2-Dichlorobenzene
82
1,2,4-Trichlorobenzene
85
Hexachlorobutadiene
77
Naphthalene
76
Q = Exceeds Quality Control limits.
Container Type: NA - Not Applicable
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 122 70-130
4-Bromofluorobenzene 118 70-130
Page 36 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: LCS
Lab ID#: 2305750-14A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061203 Date of Collection: NA
Dil. Factor: 1.00 Date of Analysis: 6/12/23 08:59 AM
Method
Compound
%Recovery
Limits
Freon 12
91
70-130
Freon 114
86
70-130
Chloromethane
80
70-130
Vinyl Chloride
92
70-130
1,3-Butadiene
90
70-130
Bromomethane
122
70-130
Chloroethane
84
70-130
Freon 11
85
70-130
Ethanol
110
70-130
Freon 113
73
70-130
1,1-Dichloroethene
86
70-130
Acetone
92
70-130
2-Propanol
96
70-130
Carbon Disulfide
93
70-130
3-Chloropropene
87
70-130
Methylene Chloride
85
70-130
Methyl tert-butyl ether
85
70-130
trans- 1,2-Dichloroethene
88
70-130
Hexane
89
70-130
1,1-Dichloroethane
93
70-130
2-Butanone (Methyl Ethyl Ketone)
99
70-130
cis-1,2-Dichloroethene
84
70-130
Tetrahydrofuran
96
70-130
Chloroform
87
70-130
1,1,1-Trichloroethane
84
70-130
Cyclohexane
88
70-130
Carbon Tetrachloride
78
70-130
2,2,4-Trimethylpentane
89
70-130
Benzene
112
70-130
1,2-Dichloroethane
110
70-130
Heptane
117
70-130
Trichloroethene
98
70-130
1,2-Dichloropropane
ill
70-130
1,4-Dioxane
110
70-130
Bromodichloromethane
102
70-130
cis-1,3-Dichloropropene
106
70-130
4-Methyl-2-pentanone
ill
70-130
Toluene
103
70-130
trans-1,3-Dichloropropene
103
70-130
1,1,2-Trichloroethane
98
70-130
Tetrachloroethene
86
70-130
2-Hexanone
101
70-130
Page 37 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: LCS
Lab ID#: 2305750-14A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061203 Date of Collection: NA
Dil. Factor: 1.00 Date of Analysis: 6/12/23 08:59 AM
Method
Compound
%Recovery
Limits
Dibromochloromethane
91
70-130
1,2-Dibromoethane (EDB)
96
70-130
Chlorobenzene
89
70-130
Ethyl Benzene
100
70-130
m,p-Xylene
88
70-130
o-Xylene
81
70-130
Styrene
92
70-130
Bromoform
87
70-130
Cumene
87
70-130
1,1,2,2-Tetrachloroethane
101
70-130
Propylbenzene
77
70-130
4-Ethyltoluene
76
70-130
1,3,5-Trimethyl benzene
78
70-130
1,2,4-Trimethyl benzene
86
70-130
1,3-Dichlorobenzene
81
70-130
1,4-Dichlorobenzene
76
70-130
alpha-Chlorotoluene
98
70-130
1,2-Dichlorobenzene
78
70-130
1,2,4-Trichlorobenzene
93
70-130
Hexachlorobutadiene
84
70-130
Naphthalene
97
60-140
Container Type: NA - Not Applicable
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 118 70-130
4-Bromofluorobenzene 112 70-130
Page 38 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: LCSD
Lab ID#: 2305750-14AA
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061204 Date of Collection: NA
Dil. Factor: 1.00 Date of Analysis: 6/12/23 09:55 AM
Method
Compound
%Recovery
Limits
Freon 12
92
70-130
Freon 114
84
70-130
Chloromethane
83
70-130
Vinyl Chloride
95
70-130
1,3-Butadiene
91
70-130
Bromomethane
119
70-130
Chloroethane
86
70-130
Freon 11
83
70-130
Ethanol
110
70-130
Freon 113
74
70-130
1,1-Dichloroethene
84
70-130
Acetone
88
70-130
2-Propanol
91
70-130
Carbon Disulfide
94
70-130
3-Chloropropene
89
70-130
Methylene Chloride
85
70-130
Methyl tert-butyl ether
85
70-130
trans- 1,2-Dichloroethene
87
70-130
Hexane
90
70-130
1,1-Dichloroethane
93
70-130
2-Butanone (Methyl Ethyl Ketone)
98
70-130
cis-1,2-Dichloroethene
82
70-130
Tetrahydrofuran
94
70-130
Chloroform
87
70-130
1,1,1-Trichloroethane
84
70-130
Cyclohexane
88
70-130
Carbon Tetrachloride
79
70-130
2,2,4-Trimethylpentane
92
70-130
Benzene
106
70-130
1,2-Dichloroethane
105
70-130
Heptane
110
70-130
Trichloroethene
92
70-130
1,2-Dichloropropane
107
70-130
1,4-Dioxane
105
70-130
Bromodichloromethane
98
70-130
cis-1,3-Dichloropropene
102
70-130
4-Methyl-2-pentanone
108
70-130
Toluene
99
70-130
trans-1,3-Dichloropropene
100
70-130
1,1,2-Trichloroethane
94
70-130
Tetrachloroethene
85
70-130
2-Hexanone
103
70-130
Page 39 of 40

■r
tiff e u rof i n s
Air Toxics
Client Sample ID: LCSD
Lab ID#: 2305750-14AA
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
File Name: 21061204 Date of Collection: NA
Dil. Factor: 1.00 Date of Analysis: 6/12/23 09:55 AM
Method
Compound
%Recovery
Limits
Dibromochloromethane
88
70-130
1,2-Dibromoethane (EDB)
94
70-130
Chlorobenzene
89
70-130
Ethyl Benzene
97
70-130
m,p-Xylene
88
70-130
o-Xylene
83
70-130
Styrene
93
70-130
Bromoform
85
70-130
Cumene
86
70-130
1,1,2,2-Tetrachloroethane
98
70-130
Propylbenzene
78
70-130
4-Ethyltoluene
80
70-130
1,3,5-Trimethyl benzene
100
70-130
1,2,4-Trimethyl benzene
94
70-130
1,3-Dichlorobenzene
84
70-130
1,4-Dichlorobenzene
78
70-130
alpha-Chlorotoluene
97
70-130
1,2-Dichlorobenzene
78
70-130
1,2,4-Trichlorobenzene
94
70-130
Hexachlorobutadiene
81
70-130
Naphthalene
97
60-140
Container Type: NA - Not Applicable
Method
Surrogates %Recovery Limits
1,2-Dichloroethane-d4 104 70-130
Toluene-d8 112 70-130
4-Bromofluorobenzene ill 70-130
Page 40 of 40

APPENDIX C
Field Notes and Photographic Record

-"
_ •I r � 1
;; sou• ',
� A
r5 ' l
io
t-
_ • _.�` �� _ lw - .mom- `
rt — ` '}
1p
L 1 &
— LLm ti
f
IL
un
d >
m .Y s
! '
.Ir
0 1W i t h e rs R a ve n e l HILLSBOROUGH STREET ASSEMBLAGE DRr•WN BY- SCALE, HWHf NO. / 5200.5204, & 5212 HILLSBOROUGH STREET PHASE II ASSESSMENT M1 1"=50' III
Engineers I Planners I Surveyors 108& 114 GRAND AVENUE MAP APPK)VED BY DATE: PROJECT NO.:
115 MacKenan Drive I Cary, NC 275111 t: 919.469.3340 5203 & 5205 DORCAS STREET RALEIGH. WAKE COUNTY, NC
license k: F-1479 I www withersraveneLcom ?_W 05/03/2022 09211168.00
. �_. __.nrvs. _ _i-e. _„,mne„o�•ey,., �x. e:,m zm-iumaic

�`Il�lw�euyh A.sse�.l
AP _ P E5,4
' ))2 4 3
C o �n � je j•e.d -
A !e Ccc��'��s
ced

Boring # TW - 1
Date q
WR Rep
140 WithersRavenel
1 _; ,
SOIL BORING LOG
Job Name Hiflsborough Street Assemblage Job # 23-0302
Site Loc. Raleigh, NC Easting NA
Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (p m)
PID
FID
D
1
t-1
01
1
3
ll
a
)5
�j0-M �k
b►vwV\, I f J � Clot, o��n ;Inc OL—A '
1elcL� , 6yt 1 Ino cac�
U
i ecl / kun , Oct- si j � , , no �Cr
1 � � �i. �s�� v' cA a,r,t vYM-hC_ , 511 i , ck, ry CdcA.A—
} )
5071 b� w� MML C ULUWI V
�,�. w� �I ;►�a�l�� A-v
Sul) i`2.ku1w
'30�X og y5
)
Un
Z
5
�C
� _ 5
) o
C
Ne
I o
I,� . 7
nf2
15
IT-6
-)
NtQ
1�.5
20
0
►vi
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Defector
EI=Elevation
115 MocKenon Drive, Cory, North Carolina 27511
AIk &/IS'' -E
Npurymw P- numm..
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Defector
Page 1 of 1
tel:[phone] fox:919.461,6008 www,withersrovenel.com
7 — SJ,I S-1gP1'E1 G.I/f,- Q A.- tf0C-S� SUOC" �(RA /-'tk</S/ 1�eK �l

NOWithei-sRavenet
- I , - - -
SOIL BORING LOG
Boring # W — •-Q Job Name Hillsborough Street Assemblage Job # 23-0302
Date 5 I l XSite Loc. Raleigh, NC Easting NA
WR Rep i Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Totai-VOCs m
PID
FID
D 5
O
DUI
,V�.cu , CT-
Y+1u�l�, — cn icr 5► �� y � y YVJ DCic*r
y
w ( l o' �ro�.r, �- �►' sect , bt.�n�t . .
4-sa.0110Q C
1)
6.
Nr-
5
5
R
ID
G
14�1_
NR=Na Reading
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
EI=Elevation
ppm=parts per million
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
Page 1 of 1
115 MncKenon Drive, Cary, North Caroline 27511 tel:[phone] fox:919.467.6008 www.withersrovenel,com

Boring # �� 3
Date ( 3
WR Rep e,J
WithersRavenel
- I ,,_ -
SOIL BORING LOG
Job Name Hillsborough Street Assemblage Job # 23-0302
Site Loc. Raleigh, NC Easting NA
Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID.
S
=-
$r
2�
ftaI bYl] LIA , t6�, � ��
5i\
arse.
uie2 �w+' is�c�'g�l+`4t-
61(4(k �/ $VAe- bra-n CtQ Cy Sr�fr !{rr
%.W �4.9 A S I,`y � f /no t-K�u2 MdL/ JAPA
�,, �- r I osuca� an _ 1 i' •1, bn :
va�Gr \�vr,�� �vp- 3�
1n5k�1\ d _ 6' A)CaQA
AS
WAS
a
lvrz
NIL
r
l0
7
N
lD
la 5
Nlc
1 d. 5
1 b
z��
2 .
v
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unified Soil Classification System
TOC=Top of Casing
r VOCs=Volatile Organic Compounds
PID=Photoionization Detector
FID=Flame Ionization Detector
EI=Elevation
Page 1 of 1 w
115 MocKenon Drive, Cary, North Corolino 27511 tei:919.469.3340 fox:919,467-6008 www.withersrovenel,com

-- 'ithersRavenet
SOIL BORING LOG
Boring # Job Name Hillsborough Street Assemblage Job # 23-0302
Date Site Loc. Raleigh, NC Eastin NA
WR Re g
P /gyp S'w Driller Ouantex NorthinG NA
Depth in Feet Soil Description
From To {Field USCS Classification}
71- zo s; /1 y , c i►M , Y)°
TLYV\p. x 0 ►r�s�l�� �i �� Via' b�S w/
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
EI=Elevation
D- 5*t 5- t o 1v, iota: ;,\ rt�,Vn
r-5'MP1'e j w-y (F- 7. s) cv / 2 q
ppm=parts permiltion
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
Page 1 of 1
115 MocKenon Drive, Cary, North Carolina 27511 tel:[phone] fox:919.467.6008 www,withersrovenel.com
otal VOCs (pp,
PID FID

40 WithersRavenet
SOIL BORING LOG
Boring # Job Name Hillsborough Street Assemblage Job # 23-0302
Date Site Loc. Raleigh, NC Easting NA
WR Rep Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (p m
PID
I FID
I G'L
�! 1 a'\1 w.5ka.1 qo A0�5� m's
��Qg,11 � `�1 SCt-t'1L(� iO��li D�jCrlf. SGUZ C� .
L
\I �
Tw-5. -
• � -.� Luau ��� sir I r�-�.�•
-S
Nti=Nd Reading
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Defector
EI=Elevation
ppm=parts per million
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
Page 1 of 1
115 MocKenon Drive, Cary, North Carolina 2 75 11 tel:[phone] (ax:919.467,6008 www.withersrovenel.com

Boring #
Date
WR Rep jam]
4: WthersRavenel
SOIL BORING LOG
Job Name Hillsborough Street Assemblage Job # 23-0302
Site Loc. Raleigh, NC Easting NA
Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
(feet BLS
Total VC s (p m
PID
FID
'
NR'N6 R d'
4.5
<�Ymt.0
!E� i 1 , C.W. , Io ock{
4;aF„
4A/ :A 51 l ' } 5'VjG�S� I Q ►mil • Uc �r
wLe
YI+1,{ CO- f U(.1CS11
7 t a j cu a VkA 11 = U .
* 1
Y . 5
i5 I
NFL
;Q. -
b
NZ
7- `5
! 0
NZ
U
Z
AjiL
Z
5
r:0
D .
/Vg-
2 _>
6. 5
M-e--
ea mg
ppm=parts per million
NA=Not Applicable GW=Ground Water
BLS=Below Land Surface USCS=Unified Soil Classification System
TOC=Top of Casing VOCs=Volatile Organic Compounds
PID=Photoicnization Detector FID=Flame Ionization Detector
EI=Elevation
Page 1 of 1
115 MocKenon Drive, Cary, North Carolina 27511 tel:[phone] fox:919-467 6008 www.withersravenel.com

Boring # 1V'j -
Date_r�11�j�3
WR Rep
4rWitnersRavenel
SOIL BORING LOG
Job Name Hillsborough Street Assemblage Job # 23-0302
Site Loc. Raleigh, NC Easting NA
Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
(feet BLS)
Total VOCs (ppm)
PID
FID
o
� a 5
I
� Lr
h,Ps���
YV cAo'-
Imo. Sid ;VV-1xf
ram{ j 1or-�uti. , �s l�,] �� , � r ►�a cYl��
w� D SG"te..
A-0 5 add auzrt} iV� - -
o
a .
5
��
. s
��
N�c
1U
,a.s
N-Z
5
AK-
a
?
M
4tA
NRn Reading
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Pholoionization Detector
EI=Elevation
115 MocKenon Drive, Cory, North Corolino 27511
ppm=parts per million
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
Page 1 of 1
te1:919.469.3340 (ax:919-467.6008 www.withersravenel.com

Boring # KJ
Date D j
WR Rep p I,7
WthersRavenel
SOIL BORING LOG
Job Name Hillsborough Street Assemblage Job # 23-0302
Site Loc. Raleigh, NC Easting NA
Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs m
PID
FID
C). s
1
)y
l
j46
�1
15
\g
9LO
red t Gl 0
qq ��, ��•s i 1 � ',n cs� '�- I de�
CJIQ>Lj� SiI C 0��` y1U ocic+- t0
rQGt�ltw,�II,C�-0 vL� C`C�-
�" ►pia r� .�1rci, c� C.) ,
..} Y"%0 l Y10 crlc--
fkAI br MA1_, Si l11131 1 ?VLCAS no 014 -✓
� DV_ lox
-suaw d- ll' Sam , blZnt.
a)0CM 5a.nrd _'(CDf K Ton- �w
NZ
s
N>z
N�
�.5
Ic7
lU
0
Pic_
13-5
15
5
I
1 .5
c)
1�L
fffl + o Rea Q ng
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Pholoionization Detector
EI=Elevation
ppm=parts per million
GW=Ground Water
USCS=Unwed Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
Page 1 of 1
115 MocKenon Drive, Cary, North Carolina 27511 tel:[phone] rox:919.467.6008 www.withersroveneLcom

Boring # Tw - q
Date -6
WR Rep W—
;0 With ersRavenel
,,_,
SOIL BORING LOG
Job Name Hillsborough Street Assemblage Job # 23-0302
Site Loc. Raleigh, NC Easting NA
Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
1
tiF
'20
r-,A j b*vu,&, C�pu i CLV l I. flo ty,
�>51 1(I[A051 W I � *
blcak 5► trvv v I � Oct
VQLCA/brcWA 5'11� w) SOI(V . c1au� ,Wb15i ,nv cx(cv
101 aztL, sit 1 wluis'� MU 'rlc✓
'Co Y1(�}CCC- Via ectc r
U4
5c reev,- -1C' oj)6 VOLO ,, a-b� e, send. /
5
5
i.-
N ZL
-
C
f
L
-
1 5
ivrr=ivo rreaaing ppm=parts per million
NA=Not Applicable GW=Ground Water
BLS=Below Land Surface USCS=Unified Soil Classification System
TOC=Top of Casing VOCs=Volatile Organic Compounds
PID=Photoionization Detector FID=Flame Ionization Detector
EI=Elevation
Page 1 of 1
115 MocKenon Drive, Cary, North Carolina 27511 tel:919.469,3340 (ax:919-467.600E www,withersrovenel.com

Boring #
Date
WR Rep W
140 WithersRavenel
SOIL BORING LOG
Job Name Hillsborough Street Assemblage Job # 23-0302
Site Loc. Raleigh, NC Easting NA
Driller Quantex Northing NA
Depth in Feet
From To
Soil Description
(Field USCS Classification)
Sample Interval
feet BLS
Total VOCs (ppm)
PID
FID
I�
1
9
nI
7
/l�
Li + (-OpSG, i '+ _n
4�Y4u+•` W .S J�I!'�' Gi. l�to a!�
plaj-lC�
.sil �G r ►19 cxPcr
sanA "OL v-[.�-�lQr YICi- "JOL ati
., �a 5' ��a1um I Aw -W.
-5
i
�-rJ
Jr
�
{�/
5
1 v
TT
N
S
`)
ML
0
NR-No ading
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
EI=Elevation
ppm=parts per million
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
Page 1 of 1
115 MocKenon Drive, Cary, North Corolino 2 75 11 tel:[phone] fox:919.467.6008 www.withersraveneLcom

Page of l C)
Job Number 23-0302
Groundwater Sampling Form State ID
Well ID mow- f
Site Name Hillsborough Street Assemblage 13 1 �G Date S rT1.2
Well Depth 2S' *?kDepth to Water ! Well Diameter i"
Casing Material Screen Length 10' Well Water Volume 3pr
Sampling Crew �Q 5 V4
Pump Type Dtr ; Tubing Type go IV Intake set at
Weather Conditions 5.4n ny s f`7� F Notes (eg. odor or color) c lt-z, .W ajar -
Time Water Level Volume Purged DO Temp S�EC pH ORP Turbidity
(24 Hr 1 (from TOC) (Gsls 1 Imnll 1 01C:1 f SJrm1 IctanH.,r& !m\J) INTI h
ueptn to Ijroauct ni/ ii
Sampled at [I1�5 Parameters taken with q5T
Samples delivered to Nfe by at
Analysis
Preservative
Bottle ware Number of Bottles
Hold Time
VOCs x 8260
HCL
40 ml VOAs glass
13
14 Days
SVOCs x 8270
None
100 Liter glass
2
7 Days
RCRA Metals
Nitric Acid
250 mL plastic
1
180 Days
Hex Chromium
None
3bTgt3 mL plastic PtU-P§Wc4
1
-24-RouTs-
PJi4rate-
None
125 mL plastic (FF)
1
48 Hours
Well Volume Calculation
1" well [well depth -depth to water] ` 0.0408 gallons
2" well [well depth -depth to water] " 0.163 gallons
4" well [well depth -depth to water] ' 0.653 gallons
I-C 'icI v•\ da�� v�- dl.c,rcfsP.�ni b-. �-Vp h-� -a I ..as •,- Jt ALS L—�-
5,01 wks r.ccaratd &/, 3/2_1-1/33
I:\EnvUser\Austin\Revised GW Sampling Form 2016

WithersRavenel
Page � of
Job Number 23-0302
Groundwater Sampling Form State ID AJ 4
Well ID T V- 2-
Site Name Hillsborough Street Assemblage 'GI Date
Well Depth ZS t � Depth to Water Well Diameter ("
Casing Material AV L� Screen Length l o ' Well Water Volume
Sampling Crew AE 15W
Pump Type R r: lv> Tubing Type Intake set at �J
Weather Conditions 5 -AAJ �f ^'f�° �rJ Notes (eg. odor or color) 1, /10 o d a i
Time Water Level Volume Purged DO Temp ,,,SEC pH ORP Turbidity
(24 Hr.) (from TOC) (Gals-] fmoll..) (°(l) (rnglrm) (standard) (mV) (NT1)1
"I
=
ueptn to rroauct
r//k
Sampled at
I Parameters taken with
Samples delivered to
r.'-'
by
S W at
Analysis
Preservative
Bottle ware
Dumber of Bottles
Hold Time
VOCs x 8260
HCL
40 ml VOAs glass
13
14 Days
SVOCs x 8270
None
100 Liter glass
2
7 Days
RCRA Metals
Nitric Acid
250 mL plastic
1
180 Days
PtAr'-A
Hex Chromium
None
sc' ttU mL plastic
1
-24-Hams_ k_ef-IJ
w try
None
125 mL plastic
1
48 Hours I (FF)
Well Volume Calculation
1" well [well depth -depth to water] * 0.0408 gallons
2" well [well depth -depth to water] * 0.163 gallons
4" well [well depth -depth to water] * 0.653 gallons
I r,
�t,5 g�jjf� �'F
;/,11
I:\EnvUser\Austin\Revised GW Sampling Form 2016

WitheFSRavenel
Page � of ` O
Job Number 3-0302
Groundwater Sampling Form State ID
Well ID W-
Site Name Hillsborough Street Assemblage S O Date s' 2
Well Depth 2i' Depth to Water r*c- Well Diameter
Casing Material PVC, Screen Length jai Well Water Volume
Sampling Crew AP ISw
Pump Type fir: Tubing Type_ Intake set at
Weather Conditions _ 51c�1n4 ti- fld°F Notes (eg. odor or color)
Time Water Level Volume Purged DO Temp ,,,%EC pH ORP Turbidity
(24 Hr ) Ifrnm TO('.) IC;alc 1 Irnr,ll 1 (Or,) LmClrml Icf=nr4nrr6 Im\A Ih1Ti 11
ueptn to rroauct
N/4
Sampled at
Parameters taken with
Samples delivered to
p� L4
by S w
at
Hold Time
Analysis
Preservative
Bottle ware
Number of Bottles
VOCs x 8260
HCL
40 ml VOAs glass
2 3
14 Days
SVOCs x 8270
None
100 Liter glass
2
7 Days
RCRA Metals
Nitric Acid
250 mL plastic
1
180 Days
Hex Chromium
None
5.t,90-mL plastic
1
-241°l ars-
FF
None
125 mL plastic
1
48 Hours
Well Volume Calculation
1" well [well depth -depth to water] * 0.0408 gallons
2" well [well depth -depth to water] * 0.163 gallons
4" well [well depth -depth to water] * 0.653 gallons
n n �-/rl /z,) , ;.� S411 rtL ti
L� w, l iJ I kl /I t�a�-a o A !!! S 11 W;9
I:\EnvUser\Austin\Revised GW Sampling Form 2016

44 With
Page
q
of to
Job Number 33-0302
Groundwater Sampling Form State ID/Vt A,
Well ID w»
Site Name Hillsborough Street Assemblage b s� ��� Date & s
Well Depth SV Depth to Water Well Diameter_
Casing Material V �_ Screen Length ) — Well Water Volume )r
Sampling Crew j? )SW
Pump Type f7f.l; Tubing Type Intake set at ^-2/
Weather Conditions S-AAX 'k3°i` ate; (eg. odor or color) t ItCie,ILV
Time Water Level Volume Purged DO Temp AS EC pH ORP Turbidity
(24 W1 (from TOC.) (GRIC; 1 (rnnll ) toM f%-a.qlr^.m% (c+,;mHnrH) lmV1 (KITI h
uepin io rroauci
Sampled at
Samples delivered to
Analysis
VOCs x 8260
SVOCs x 8270
RCRA Metals
Hex Chromium
N
�. 50 p Parameters taken with
?•.c A_ by
Z
reservative
Bottle ware
HCL
40 ml VOAs glass
None
100 Liter glass
Nitric Acid
250 mL plastic
None
SD +G13 mL plastic
None
125 mL plastic
W at
Number of Bottles
4r3
2
1
1
1
Well Volume Calculation
1" well
[well depth -depth to water] " 0.0408
gallons
2" well
[well depth -depth to water] " 0.163
gallons
4" well
[well depth -depth to water] ' 0.653
gallons
'Z$7_
trW /_ , - ' Q 0 1
b,-A -SOS r-ft
Cl- c�1 �6y"�_j rccv �d-
v-�. Zz6�3
14 Days
7 Days
180 Days
_24-Hnur-s- FF
48 Hours
I:\EnvUser\Austin\Revised GW Sampling Form 2016

V'JithersRavenel
Page S_ of I O
Job Number 33-0302
Groundwater Sampling Form State ID
Well ID
Site Name Hillsborough Street Assemblage Date � �j i J a3
Well Depth -L5' Depth to Water Well Diameter 1
Casing Material pVC Screen Length t o r Well Water Volume
Sampling Crew AP)/ j c, �
Pump Type J2LA Tubing Type_12QWIntake set at "- Z�
Weather Conditions��u�y�u $° F No s (eg. odor or color)
Time Water Level Volume Purged DO Temp EC pH ORP Turbidity
(24 Hr.1 [from TOC) (Gals.] (Mali 1 for) (m.1;/r.m) (ctanrlarrl] fm111 rNTI h
ueptn to rroauct
Sampled at
Samples delivered to
7
Parameters taken with
by
.S w
at
Analysis
Preservative
Bottle ware
Number of Bottles
Hold Time
VOCs x 8260
HCL
40 ml VOAs glass
-q-3
14 Days
Y
SVOCs x 8270
None
100 Liter glass
2
7 Days
RCRA Metals
Nitric Acid
250 mL plastic
1
180 Days
Hex Chromium
None
s0 -190 mL plastic
1
-24t11UUM
FP
N+#rate
None
125 mL plastic
1
48 Hours
Well Volume Calculation
1" well [well depth -depth to water] " 0.0408 gallons
2" well [well depth -depth to water] " 0.163 gallons
4" well [well depth -depth to water] " 0.653 gallons
b r-J " Ig' 13" v r< s 1i/173 6 sill
/
C,jC,k.,I recorcltJ vn
I:\EnvUser\Austin\Revised GW Sampling Form 2016

�I
WithersRavenel Page of /0
Job Number 23-0302
Groundwater Sampling Form
State ID jV4
_
Well ID W—
Site Name Hillsborough Street Assemblage
Date S" r
17.
Well Depth 25
�► V Depth to Water
3Z• ioG Well Diameter "
Casing Material pvc
Screen Length
; p' Well Water Volume.
Sampling Crew 015 a
Pump Type pex ;
Tubing Type
i0oly Intake set at "- LI/
Weather Conditions Su A n ►
^��'
otes {eg{eg. odor or color) C-/en r p end i
0
Time Water Level Volume Purged
DO Temp
-Ee } pH dFt' "~ Turbidity
(24 Hr.) (from TOO) if,alfi l
fmnll 1 M71
(KITI 1�
EUMM_
09=®V—
uepin io rroauct IV 14
Sampled at
Samples delivered to
Parameters taken with
by
at
Analysis
Preservative
Bottle ware
Number of Bottles
Hold Time
VOCs x 8260
HCL
40 ml VOAs glass
4 3
14 Days
SVOCs x 8270
None
100 Liter glass
2
7 Days
RCRA Metals
Nitric Acid
250 mL plastic
1
180 Days
Hex Chromium
None
50 4�-mL plastic
1
ours
C3#�et~
None
125 mL plastic
1
48 Hours
vven volume talculanon
1" well [well depth -depth to water] * 0.0408 gallons
2" well [well depth -depth to water] * 0.163 gallons
4" well [well depth -depth to water] * 0.653 gallons
'P' �UP
FF
a c 1« 1 6TQ tam rid n
y� z�
I:IEnvUser\Austin\Revised GW Sampling Form 2016

j
WithersRavenei Page
of l D
Job Number 23-0302
Groundwater Sampling Form State ID
Well ID Tt,/'
Site Name Hillsborough Street Assemblage Date Z
Well Depth 25 { Depth to Water Z1• 0(o T°c, Well Diarheter "
Casing Material V C. Screen Length / & ` Well Water Volume �e-
Sampling Crew AP15W ,
Pump Type Tubing Type (7oT lntakeet at ^' 2-3Weather Conditions .114 SC441'e , " ?� "F o#es (eg. odor or color _ eG1' f el a e,jj.-
Time Water Level Volume Purged DO Temp A^EC pH ORP Turbidity
(24 Hr.) (frorn TOM foals ) lmrill 1 IUM ImSlrrn) (etnnrinrrh tm1/) (AITI h
Uepin io rracuciIA-
Sampled at IV v Parameters taken with $;ti
Samples delivered to 6 cG by Q at
Analysis
Preservative
Bottle ware
Number of Bottles
Hold Time
VOCs x 8260
HCL
40 ml VOAs glass
4.)t
14 Days
SVOCs x 8270
None
100 Liter glass
2
7 Days
RCRA Metals
Nitric Acid
250 mL plastic
1
180 Days
Hex Chromium
None
3V 4.-Ge-rnL plastic
1
2A-Keufs--
oLtrzte
None
125 mL plastic
1
48 Hours
Other
well Volume Galculatlon
1" well [well depth -depth to water] * 0.0408 gallons
2" well [well depth -depth to water] * 0.163 gallons
4" well [well depth -depth to water] * 0.653 gallons
TW r- 21 r LS v n 5/Z.��•� % s1411 Ms
uC,k,,-, S az��3
F,=
I:\EnvUser\Austin\Revised GW Sampling Form 2016

WitheFsRavenel Page of
Job Number 23- 302
Groundwater Sampling Form State ID 1,4
Well ID W -
Site Name Hillsborough Street Assemblage Date 57 2.5-
Well Depth 25 ' `r Depth to Water f 3 n,- Well Diameter
Casing Material P V c_ Screen Length i o ` Well Water Volume
Sampling Crew AV s W
Pump Type Qe.t, Tubing Type Intake set at
Weather Conditions l (,tw, ���°F Notes (eg. odor or color) c /cam �� °.�✓
Time Water Level Volume Purged DO Temp - ft EC pH ORP Turbidity
(24 Hr.) (from TOC) (Gals.) fmo1L1 !°(1] (m5fcm) fstanrlarr0 (mV1 (NIT(11
ueptn to rroouct /V iIt
Sampled at I t 4 Parameters taken with (S T _
Samples delivered to I W by C uJ at
Analysis
Preservative
Bottle ware
Number of Bottles
hold Time
VOCs x 8260
HCL
40 ml VOAs glass
923
14 Days
SVOCs x 8270
None
100 Liter glass
2
7 Days
RCRA Metals
Nitric Acid
250 mL plastic
1
180 Days
Hex Chromium
None
5-D # mL plastic
1
24-Hours - ­
Nitrate
None
125 mL plastic
1
48 Hours
Other
Well Volume Calculation
1" well [well depth -depth to water] ` 0.0408 gallons
2" well [well depth -depth to water] * 0.163 gallons
4" well [well depth -depth to water] " 0.653 gallons
7 ��//2, 1-2 /111
J
PP
I:\EnvUser\Austin\Revised GW Sampling Form 2016

Wither-sRavenel
Groundwater Sampling Form
Site Name Hillsborough Street Assemblage
Well Depth 2 * Depth to Water
Casing Material I?vc- Screen Length
Sampling Crew ,4pLs,.,r
Pump Type per: Tubing Type
Weather Conditions 5wn^y , bf4+xL, "I&VF
Page of `-D
Job Number 23-0302
State ID IV114
Well ID Tfv-�
Date 5 /s 2 3
33 Tom Well Diameter i "
t o , Well Water Volume
Intake set at '`' 2 L
Notes (eg. odor or color) -% G cold r _ G
Time Water Level Volume Purged DO Temp AAEC pH ORP Turbidity
(24 Hr.) ffrnm TOM (C'Ak.1 tmnlf 1 rar'1 G2m_gJrml (Qfnnrinrr0 (m\n iKITI it
uepm io Product /u /M
Sampled at pp Parameters taken with
Samples delivered to )C,ct by
5z
at
Analysis
Preservative
Bottle ware
Number of Bottles
Hold Time
VOCs x 8260
HCL
40 ml VOAs glass
0,3
14 Days
SVOCs x 8270
None
100 Liter glass
2
7 Days
RCRA Metals
Nitric Acid
250 mL plastic
1
180 Days
Hex Chromium
None
SD 44 -mL plastic
1
ours
Nitrate
None
125 mL plastic
1
48 Hours
Other
vveli volume calculation
1" well [well depth -depth to water] " 0.0408 gallons
2" well [well depth -depth to water] " 0.163 gallons
4" well [well depth -depth to water] " 0.653 gallons
- 6,Tw / - '9 a 6.� -SN/ r.�
ejC.P-1-It I pTw r(-Catot '-a v r ��221
FF
I:\EnvUser\Austin\Revised GW Sampling Form 2016

Wlti ersRavenet Page / L) of
Job Number 23-0302
Groundwater Sampling Form State ID NA
Well IDJ 'r w —1 Z)
Site Name Hillsborough Street Assemblage Date { z Z]
Well Depth 2 [9' Depth to Wafer 1 ,?- Y3 7-, L Well Diameter r "
Casing Material Pl L Screen Length 1p> Well Water Volume
Sampling Crew / 5 W 2S ,
Pump Type Gr: Tubing Tay a Intake set at
Weather Conditions r,.g�y br+sze { ^-C—Notes (eg. odor or color) ( (C-, ; 4o
Time Water Level Volume Purged DO Temp ,,,SEC pH ORP Turbidity
(24 Hr ) (frnm TCfa l(;alc ) fmnll 1 (orb L=aClrm) (CtaneiaMl rmuA rniT3 n
UUPLf l LU r-f UUUGL I -I P'
Sampled at Is
Samples delivered to
Parameters taken with y _S
by S w
Analysis
Preservative
Bottle ware
VOCs x 8260
HCL
40 ml VOAs glass
SVOCs x 8270
None
100 Liter glass
RCRA Metals
Nitric Acid
250 mL plastic
Hex Chromium
None
s0 1-00 mL plastic
Nitrate
None
125 mL plastic
Well Volume Calculation -
1" well [well depth -depth to water] " 0.0408 gallons
2" well [well depth -depth to water] ' 0.163 gallons
4" well [well depth -depth to water] ' 0.653 gallons
81-5 C.9 (-\ j Af—.z7,
Sw
!�c G� �r n Z
at
Number of Bottles Hold Time
21 14 Days
2 7 Days
1 180 Days
1 24-Hatt Fr-
1 48 Hours
I:\EnvU,ser\Austin\Revised GW Sampling Form 2016

WithersRavenel
SOIL VAPOR SAMPLING FIELD FORM
ID UP— 1 Job Name Hillsborough Street Assemblage Job # 23-0302
Date 22 Z Site Loc. Raleigh, NC Depth�L j
WR Rep Lab Eurofins Air Toxics Weather $ 0
Purging and Leak Check Info
Sampling Apparatus Info
Shroud Ambient Helium Reading
2I c,70
Canister ID IL- 3 Z 9
Vapor Probe Helium Reading
O M
Flow Regulator ID L D I y (V
Sample Apparatus Helium Reading I] M
Starting Vacuum ag "
Purge Start Time
q go
Starting Time Q C
I
Purge End Time
/`
V
Ending Vacuum " I{
PID Reading
Ending Time o -6
Additonal Comments:
ran=rva rreEr g
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
EI=Elevation
ppm=parts per million
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
115 MacKenon Drive, Cary, North Corclino 27511 te1:919A69.3340 (ox:919.467.6008 www.withersrovenel.com

IDv f —
Date
WR Rep A,j] I SAD
N1 WithersRavenel
SOIL VAPOR SAMPLING FIELD FORM
Job Name Hillsborough Street Assemblage
Site Loc. Raleigh, NC
Lab Eurofins Air Toxics
Job # 23-0302
Depth
Weather 9+ r 5 `' 3t7 If It
Purging and Leak Check Info
Sampling Apparatus Info
Shroud Ambient Helium Reading -Z( `7D
Canister ID
Vapor Probe Helium Reading 0 M
Flow Regulator ID c ody+
Sample Apparatus Helium Reading O M
Starting Vacuum 5
Purge Start Time D �
Starting Time `"4lon
Pure End Time
9 q'�g
Ending Vacuum `1 � , 5 l�
PID Reading D
Ending Time'"1
Additonal Comments:
1— rteaumy
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
EI=Elevation
ppm=parts per million
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=F)ame Ionization Detector
115 MocKenon Drive, Cory, North Corolino 2 75 11 tel:919.469,3340 (ox:919.467.6008 www.withersrovenel.com

40 WithersRavenel
,,
SOIL VAPOR SAMPLING FIELD FORM
ID — Job Name Hillsborough Street Assemblage Job # 23-0302
Date _ Site Loc. Raleigh, NC Depth (TS
WR Rep Lab Eurofins Air Toxics Weather Y rUz_+Z t!° 6j
Purging and Leak Check Info
Sampling Apparatus Info
Shroud Ambient Helium Reading - /e
Canister ID' QA A 3
Vapor Probe Helium Reading C,e 0M
Flow Regulator ID C © O` 0
Sample Apparatus Helium Reading ZS r ,164 D,y'%a
Starting Vacuum 2g. S *' 14
Purge Start Time a G 50
Starting Time (Q 3
Purge End Time U G 5$
Ending Vacuum (f cJ
PID Reading
[Ending Time I D ZQ
Additonal Comments:
NH=NO f pada:g
NA=Nat Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
EI=Elevation
ppm=parts permiltran
GW=Ground Water
USCS=Unified Sail Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
115 MccKenon Drive, Cory. North Corolinc 27511 tel:919,469.3340 fox:919.467.6008 www.withersrovenel.com

With ersRavenet
SOIL VAPOR SAMPLING FIELD FORM
ID V l" "- L Job Name Hillsborough Street Assemblage Job # 23-0302
Date - - Site Loc. Raleigh, NC Depth
WR Rep F I 4.L3 Lab Eurofins Air Toxics Weather f I''
Purging and Leak Check Info
Sampling Apparatus Info
Shroud Ambient Helium Reading 7Z3 7o
Canister ID I LLA 1 Uq
'Vapor Probe Helium Reading ©
Flow Regulator ID G0 `I 3
Sample Apparatus Helium Reading M
Starting Vacuum 91� it
Purge Start Time Q 36
Starting Time I V 4
Purge End Time I Qy0
Ending Vacuum
PID Reading U`
Ending Time
Additonal Comments-
�7CYr Q Ili iv s� ovav"
ivn=fvo Heaaing
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
B=Elevation
ppm=parts per million
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
115 MocKenan Drive, Cory, North Carolina 27511 tel:[phone] fox:919,467.6008 wwv✓.withersraveneLcom

%0 WitheFSPavenet
SOIL VAPOR SAMPLING FIELD FORM
ID\J2 - 5 _ Job Name HIllsborough Street Assemblage Job # 23-0302
Date _ g9, - a3 Site Loc. Ra€eigh, NC Depth 7 L
WR Rep Lab Eurofns Air Toxics Weather a b I {
Purging and Leak Check Info
Sampling Apparatus Info
Shroud Ambient Helium Reading
Z D `%p
Canister ID t `.- to y o(5
Vapor Probe Helium Reading
Q M
Flow Regulator ID C UIJ 0'
Sample Apparatus Helium Reading Q P -1
Starting Vacuum
Purge Start Time
1 0 00
Starting Time
Purge End Time
Ending Vacuum
.S
PID Reading
Q D
(Ending Time 10 Z
Additonal Comments:
'
-rt—Ive/ nuourfog
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
EI=Elevation
ppm=parts per million
GW=Ground Water
USCS=Unifi'ed Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
115 MocKenon Drive, Cary. North Corohna 27511 tel:[phone] fox:919.467.6008 www.withersrovenel.com

WithersRavenet
SOIL VAPOR SAMPLING FIELD FORM
ID V l - b Job Name Hillsborough Street Assemblage Job # 23-0302
Date 43"12-.3 Site Loc. Raleigh, NC Depth
u
WR Rep 41cw Lab Eurofins Air Toxics Weather S,AAX Ittt-g
Purging and Leak Check Info
Sampling Apparatus Info
Shroud Ambient Helium Reading 26`%
Canister ID
L 21 9,0
'Vapor Probe Helium Reading PP M
Flow Regulator ID
lr O QS
Sample Apparatus Helium Reading Sb P M
Starting Vacuum
27_5 u /1—
Purge Start Time O
Starting Time
pgY 8
Purge End Time D 'ya
Ending Vacuum
3'r
PID Reading O M
Ending Time
D B,SS
Additonal Comments:
NR=No Reading
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
EI=Elevation
ppm=parts per million
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
115 MccKenon Drive, Cary, North Carolina 2 75 11 tel:[phone] fox:919.467.60C8 wvdw.withersrovenel.com

4 WithersRavenel
SOIL VAPOR SAMPLING FIELD FORM
ID - '7L Job Name Hillsborough Street Assemblage Job # 23-0302
Date - Site Loc. Raleigh, NC Depth `
WR Rep Lab Eurofins Air Toxics Weather UA
Purging and Leak Check Info
Sampling Apparatus Info
Shroud Ambient Helium Reading
f] F) ''
�+
Canister ID l 1� A k, � a
Vapor Probe Helium Reading
Flow Regulator ID�1
Sample Apparatus Helium Reading
O
Starting Vacuum
Purge Start Time
13t1
Starting Time
Purge End Time
' �A 0
Ending Vacuum Ll "
PID Reading
[Ending Time
Additonal Comme s: s
I O�' GU V � l0W desQ,w UA �r�
,vmrvv rceavmg
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
EI=Elevation
ppm=Parts per
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
115 MccKenon Drive, Cary, North Corolina 27511 tel:919.469,3340 (ox:919.467 6008 www.withersrovenel.corn

Withef-sRavenet
Y SOIL VAPOR SAMPLING FIELD FORM
ID — 0 Job Name Hillsborough Street Assemblage Job # 23-0302
Date . — - d. 7 Site Loc. Raleigh, NC Depth C2 '
WR Rep A� l _ L Lab Eurofins Air Toxics Weather
Purging and Leak Check Info
Sampling Apparatus Info
Shroud Ambient Helium Reading
2—& /a
Canister ID a—%U
Vapor Probe Helium Reading
p f 1
Flow Regulator ID E0g 1
Sample Apparatus Helium Reading O PFMStarting
Vacuum ,I Sl
Purge Start Time I W 5
Starting Time , D
Purge End Time ILA
1 D
Ending Vacuum
PID Reading
Ending Time 1�I
Additonal Comments:
NR=No Reading
ppm=parts per million
NA=Not Applicable
GW=Ground Water
BLS=Below Land Surface
USCS=Unified Soil Classification System
TOC=Top of Casing
VOCs=Volatile Organic Compounds
PID=Photoionization Detector
FID=Flame Ionization Detector
EI=Elevation
115 NocKenon Drive, Cary, North Corolino 27511 tel:919;469.3340 fox:919.467,6008 www.withersrovenel,cot?

--4p
ID
Date — a q -
WR Rep
WithersRavenel
SOIL VAPOR SAMPLING FIELD FORM
Job Name Hillsborough Street Assemblage Job # 23-0302
Site Loc. Raleigh, NC Depth
Lab Eurofins Air Toxics Weather ba tl
i
Purging and Leak Check Info
Sampling Apparatus Info
Shroud Ambient Helium Reading
23
Canister ID - 0 oOgO -
Vapor Probe Helium Reading
(`� t„ �
Flow Regulator ID
eV 1 -+q
Sample Apparatus Helium Reading
J-1
Starting Vacuum
Purge Start Time
VA 1 q
Starting Time
Pure End Time
9
1
Ending Vacuum
t
PID Reading
Ending Time
Additonal Comments:
l) q ti Cgt3
A,,V- lip'. E o
40Ava�w�v�
WNW
Q..�cl'� va.tWuv�
NR4Vu F..--ad,rig
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
El=Elevation
ppm=parts per million
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
115 MocKenon Drive, Cory, North Corclino 27511 tel:[phone] (ox:919 467.6008 www.withersraveneLcorn

.IV
ID
Date
WR Rep
WithersRavenel
SOIL VAPOR SAMPLING FIELD FORM
Job Name Hillsborough Street Assemblage Job # 23-0302
Site Loc. Raleigh, NC Depth
Lab Eurofins Air Toxics Weathe
Purging and Leak Check Info
Sampling Apparatus Info
Shroud Ambient Helium Reading
Z 1 %
Canister ID I LISL U
Vapor Probe Helium Reading
PP M
Flow Regulator ID C —I
Sample Apparatus Helium Reading vc PP M
Starting Vacuum a I�
Purge Start Time
q ) o
c_
Starting Time 1
y
Purge End Time
1
Ending Vacuum 3 5 I
PID Reading
Ending Time `�1 ``'
1
Additonal Comments:
NR= vu Reaming
NA=Not Applicable
BLS=Below Land Surface
TOC=Top of Casing
PID=Photoionization Detector
EI=Elevalion
ppm=parts permilFion
GW=Ground Water
USCS=Unified Soil Classification System
VOCs=Volatile Organic Compounds
FID=Flame Ionization Detector
115 WcKenon Drive, Cory, North Corolino 27511 tel:919A69.3340 fox:919.467 6008 www-witliersrovenel.com

Sr I
w--
i
7w-3
°I
TV)
OK
I
Tip -
i
1-4.s�
\J . �j l

::WithersRavenel
Our People. Your Success.
Frame No. 1
Description: View of the area of TW-1/VP-1.
Frame No. 2
Description: View of the area of TW-2/VP-2.
Hillsborough Street Assemblage: Raleigh, NC WR No. 23-0302
Photographic Record June 2023

::WithersRavenel
Our People. Your Success.
Frame No. 3
Description: View of the area of TW-3/VP-3.
Frame No. 4
Description: View of the area of TW-4/VP-4.
Hillsborough Street Assemblage: Raleigh, NC WR No. 23-0302
Photographic Record June 2023

::WithersRavenel
Our People. Your Success.
Frame No. 5
Description: View of the area of TW-5/VP-5.
Frame No. 6
Description: View of the area of TW-6/VP-6.
Hillsborough Street Assemblage: Raleigh, NC WR No. 23-0302
Photographic Record June 2023

::WithersRavenel
Our People. Your Success.
Frame No. 7
Description: View of the area of TW-8/VP-8.
Frame No. 8
Description: View of the area of TW-9/VP-9.
Hillsborough Street Assemblage: Raleigh, NC WR No. 23-0302
Photographic Record June 2023

::WithersRavenel
Our People. Your Success.
Frame No. 9
Description: View of the area of TW-10/VP-10.
Hillsborough Street Assemblage: Raleigh, NC WR No. 23-0302
Photographic Record June 2023

APPENDIX D
NCDEQ Risk Calculator Results

North Carolina Department of Environmental Quality
Risk Calculator
Version Date:
January 2023
Basis:
November 2022 EPA RSL Table
Site Name:
Hillsborough Street Assemblage
Site Address:
5200 Hillsborough Street, Raleigh, NC
DEQ Section:
N/A
Site ID:
23-0302
Exposure Unit ID:
N/A
Submittal Date:
6/14/2023
Prepared By•
Austin Pote, E.I.
WithersRavenel
Reviewed By:
Matthew James, P.G.
North Carolina DEQ Risk Calculator

Table of Contents
1
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 23-0302
Exposure Unit ID:
N/A
Form No.
Description
Check box
if included
DATA INPUT SHEETS
Input Section 1 - Exposure Pathways & Parameters
Input Form IA
Complete Exposure Pathways
0
Input Form 1B
Exposure Factors and Target Risks
❑
Input Form I
Contaminant Migration Parameters
❑
Input Form 11)
Sample Statistics
❑
Input Section 2 - Exposure Point Concentrations
Input Form 2A
Soil Exposure Point Concentration Table
0
Input Form 2B
Groundwater Exposure Point Concentration Table
0
Input Form 2C
Surface Water Exposure Point Concentration Table
❑
Input Form 21)
Soil Gas Exposure Point Concentration Table
0
In ut Form 2E
Indoor Air Exposure Point Concentration Table
❑
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Form lA
Risk for Individual Pathways
0
Output Form I
Sitewide Risk
0
Output Section 2 - Direct Contact Soil and Groundwater Calculators
Output Form 2A
Resident Soil
0
Output Form 2B
Resident Groundwater Use
0
Output Form 2C
Non -Residential Worker Soil
0
Output Form 21)
Non -Residential Worker Groundwater Use
0
Output Form 2E
Construction Worker Soil
0
Output Form 2F
Recreator/Trespasser Soil
0
Output Form 2G
Recreator/Tres asser Surface Water
❑
Output Section 3 - Vapor Intrusion Calculators
Output Form 3A
Resident Groundwater to Indoor Air
0
Output Form 3B
Resident Soil Gas to Indoor Air
0
Output Form 3C
Resident Indoor Air
❑
Output Form 31)
Non -Residential Worker Groundwater to Indoor Air
0
Output Form 3E
Non -Residential Worker Soil Gas to Indoor Air
0
Output Form 3F
Non -Residential Worker Indoor Air
❑
Output Section 4 - Contaminant Migration Worksheets
Output Form 4A
Soil to Groundwater - Forward Mode
❑
Output Form 4B
Groundwater to Groundwater - Forward Mode
❑
Output Form 4C
Soil to Surface Water - Forward Mode
❑
Output Form 41)
Groundwater to Surface Water - Forward Mode
❑
Output Form 4E
Soil to Groundwater - Backward Mode
❑
Output Form 4F
Groundwater to Groundwater - Backward Mode
❑
Output Form 4G
Soil to Surface Water - Backward Mode
❑
Output Form 4H
Groundwater to Surface Water - Backward Mode
❑
North Carolina DEQ Risk Calculator

Complete Exposure Pathways
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 23-0302
Exposure Unit ID: N/A
Note: Risk output will only be calculated for complete exposure pathways.
Receptor
Pathway
Check box if
pathway
complete
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Soil
0
Groundwater Use
0
Non -Residential Worker
Soil
0
Groundwater Use
0
Construction Worker
Soil
0
Recreator/Trespasser
Soil
0
Surface Water
❑
VAPOR INTRUSION PATHWAYS
Resident
Groundwater to Indoor Air
0
Soil Gas to Indoor Air
0
Indoor Air
❑
Non -Residential Worker
Groundwater to Indoor Air
0
Soil Gas to Indoor Air
0
Indoor Air
❑
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Source Soil
0
Source Groundwater
0
Surface Water
Source Soil
❑
Source Groundwater
❑
North Carolina DEQ Risk Calculator

osure Point Concentrations
pion Date: January 2023
s: November 2022 EPA RSL Table
ID: 23-0302
osure Unit ID: N/A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
NOTE: If the chemical list is chanted from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(mg/kg)
Notes:
CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
116
TW-9
7440-38-2
Arsenic, Inorganic
mg/kg
30.5
TW-7
7440-39-3
Barium
mg/kg
0.00371
TW-7
98-06-6
Butylbenzene,tert-
mg/kg
51.911
TW-6
16065-83-1
Chromium(III), Insoluble Salts
mg/kg
1.81
TW-8
18540-29-9
Chromium(VI)
mg/kg
26.3
TW-3
7439-92-1
—Lead and Compounds
mg/kg
0.179
TW-3
7439-97-6
Mercury (elemental)
mg/kg
0.0105
TW-4
83-32-9
—Acenaphthene
mg/kg
0.0649
TW-4
120-12-7
—Anthracene
mg/kg
0.402
TW-4
56-55-3
—Benz[a]anthracene
— kg
0.261
TW-4
50-32-8
—Benzo[a]pyrene
mg/kg
0.335
TW-4
205-99-2
—Benzo[b]fluoranthene
mg/kg
0.127
TW-4
207-08-9
—Benzo[k]fluoranthene
mg/kg
0.344
TW-4
218-01-9
—Chrysene
mg/kg
0.0301
TW-4
53-70-3
—Dibenz[a,h]anthracene
mg/kg
0.759
TW-4
206-44-0
—Fluoranthene
mg/kg
0.0112
TW-4
86-73-7
—Fluorene
mg/kg
0.111
TW4
193-39-5
—Indeno[1,2,3-cd]pyrene
mg/kg
0.734
TW4
129-00-0
—Pyrene
m k
2.02
TW-7
778249-2
Selenium
mg/kg
North Carolina DEQ Risk Calculator

osure Point Concentrations
lion Date: January 2023
s: November 2022 EPA RSL Table
ID: 23-0302
osure Unit ID: N/A
Groundwater Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(ug/L)
Notes:
CAS Number
Chemical
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection
Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
0.779
TW-4
7440-38-2
Arsenic, Inorganic
ug/L
182
TW-9
7440-39-3
Barium
u
239
TW-2
71-43-2
Benzene
u
16.4
TW-2
104-51-8
Butylbenzene, n-
ug/L
3.06
TW-2
135-98-8
Butylbenzene, sec-
u
0.36
TW-10
7440-43-9
Cadmium (Water)
ug/L
2.15
TW-2
67-66-3
Chloroform
u
0.215
TW-4
18540-29-9
omium(VI)
u L
12.1
TW-2
98-82-8
Cumene
u
10.5
TW-2
107-06-2
Dichloroethane,l,2-
ug/L
171
TW-2
100-41-4
Ethylbenzene
u
32.2
TW-2
591-78-6
Hexanone, 2-
ug/L
1.97
TW-10
7439-92-1
—Lead and Compounds
u
0.156
TW-4
7439-97-6
—Mercury (elemental)
ug/L
13.5
TW-2
78-93-3
Methyl Ethyl Ketone (2-Butanone)
u
9.25
TW-2
108-10-1
Methyl Isobutyl Ketone (4-methyl-2-pentanone)
ug/L
2
TW-2
1634-04-4
Methyl tert-Butyl Ether (MTBE)
u
1.1
TW-9
84-74-2
—Dibutyl Phthalate
ug/L
5.13
TW-2
84-66-2
—Diethyl Phthalate
u
0.121
TW-3
206-44-0
—Fluoranthene
u
19.2
TW-2
91-20-3
—Naphthalene
u
42.5
TW-2
103-65-1
Propylbenzene
ug/L
4.31
TW-5
7782-49-2
Selenium
u
0.169
TW-6
79-34-5
Tetrachloroethane, 1,1,2,2-
ug/L
407
TW-2
108-88-3
Toluene
u
295
TW-2
95-63-6
Trimethylbenzene, 1,2,4-
ug/L
121
TW-2
108-67-8
Trimethylbenzene, 1,3,5-
u
676
TW-2
108-38-3
X lene, m-
ug/L
200
TW-2
95-47-6
X lene, o-
u
676
TW-2
106-42-3
X lene, -
u L
North Carolina DEQ Risk Calculator

osure Point Concentrations
lion Date: January 2023
s: November 2022 EPA RSL Table
ID: 23-0302
osure Unit ID: N/A
Soil Gas Exoosure Point Concentration Table
Description of Exposure Point Concentration Selection:
Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Minimum
Maximum
Location of
Range of
Concentration
ScreeningPotential
Potential
Rationale for
Concentration
Notes:
CAS Number
Chemical
Concentration
Concentration
Units
Maximum
Detection
Used for
Background
Toxicity Value
ARAR/TBC
ARAR/TBC
COPC Flagation
Selection or
(ug/m)
(Qualifier)
(Qualifier)
Concentration
Frequency
Limits
Screening
Value
(Screening
Value
Source
(Y/N)
Deletion
Level) (n/c)
190
VP-7
67-64-1
Acetone
ug/m3
12
VP-10
71-43-2
Benzene
ug/m3
38
VP-4
75-15-0
Carbon Disulfide
ug/m3
15
VP-2
67-66-3
Chloroform
ug/m3
8.7
VP-10
98-82-8
Cumene
ug/m3
7.9
VP-7
110-82-7
C clohexane
ug/m3
12
VP-4
75-71-8
Dichlorodifluoromethane
ug/m3
53
VP-10
100-41-4
Eth lbenzene
ug/m3
24
VP-9
142-82-5
Heptane, N-
ug/m3
16
VP-4
110-54-3
Hexane, N-
ug/m3
19
VP-3
78-93-3
Methyl Ethyl Ketone (2-Butanone)
ug/m3
4.3
VP-4
108-10-1
Methyl Isobutyl Ketone (4-meth 1-2- entanone)
ug/m3
3.7
VP-7
75-09-2
Methylene Chloride
ug/m3
19
VP-9
103-65-1
Propylbenzene
ug/m3
51
VP-5
127-18-4
Tetrachloroethylene
ug/m3
170
VP-10
108-88-3
Toluene
ug/m3
1.2
VP-10
79-01-6
Trichloroethylene
ug/m3
1.4
VP-7
75-69-4
Trichlorofluoromethane
ug/m3
210
VP-9
95-63-6
Trimethylbenzene, 1,2,4-
u9/m3
87
VP-9
108-67-8
Trimeth lbenzene, 1,3,5-
ug/m3
0.65
VP-7
75-01-4
Vinyl Chloride
ug/m3
290
VP-9
108-38-3
X lene, m-
ug/m3
110
VP-9
95-47-6
Xylene,o-
u9/m3
290
VP-9
106-42-3
X lene, -
ug/m3
North Carolina DED Risk Calmlalor

Risk for Individual Pathways
1
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 23-0302
Exposure Unit ID: N/A
DIRECT CONTACT SOIL AND WATER CALCULATORS
Receptor
Pathway
CarcinogenicRisk
Hazard Index
Risk exceeded?
Resident
Soil
1.8E-04
3.4E+00
YES
Groundwater Use*
9.0E-04
2.9E+01
YES
Non -Residential Worker
Soil
3.9E-05
2.5E-01
NO
Groundwater Use*
2.2E-04
6.8E+00
YES
Construction Worker
Soil
7.0E-06
2.6E+00
YES
Recreator/Trespasser
Soil
1.0E-04
1.9E+00
YES
Surface Water*
NC
NC
NC
VAPOR INTRUSION CALCULATORS
Receptor
Pathway
CarcinogenicRisk
Hazard Index
Risk exceeded?
Resident
Groundwater to Indoor Air
2.1E-04
8.2E+00
YES
Soil Gas to Indoor Air
6.4E-06
4.2E-01
NO
Indoor Air
NC
NC
NC
Non -Residential Worker
Groundwater to Indoor Air
4.8E-05
2.0E+00
YES
Soil Gas to Indoor Air
4.8E-07
3.4E-02
NO
Indoor Air
NC
NC
NC
CONTAMINANT MIGRATION CALCULATORS
Pathway
Source
Target Receptor Concentrations Exceeded?
Groundwater
Source Soil
Exceedence of 2L at Receptor?
NM
Source Groundwater
Exceedence of 21, at Receptor?
NM
Surface Water
Source Soil
Exceedence of 2B at Receptor?
NC
Source Groundwater
Exceedence of 213 at Receptor?
NC
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based
closure.
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
North Carolina DEQ Risk Calculator

Sitewide Risk
Version Date: January 2023 NOTE: If any changes were made, select "Update Sitewide Risk Values" to obtain updated values.
Basis: November 2022 EPA RSL Table
Site ID: 23-0302
Exposure Unit ID: N/A
Resident - Current Scenario
Resident - Future Scenario
Non -Residential Worker - Current Scenario
Non -Residential Worker - Future Scenario
Construction Worker
Recreator/Trespasser
Receptor
Pathway
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk
Hazard Index
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk
Hazard Index
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk
Hazard Index
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk
Hazard Index
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk
Hazard Index
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk
Hazard Index
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Soil
1.8E-04
3.4E+0U
1.5E-04
3.3E+00
Groundwater Use*
9.0E-04
2.9E+01
r
9,0E-04
2.9E+01
Soil
'•
3.9F-05
2.5E-01
3.9F-05
2.5F,-01
Non -Residential Worker
Groundwater Use*
r
2.2E-01
6.8E+00
2.2E-04
6.8E+00
Construction Worker
Soil
R
7.OF-06
2.6F+00
Recreator/Trespasser
Soil
r
1.0E-04
1.9E+00
Surface Water Use*
NM
NM
VAPOR INTRUSION CALCULATORS
Groundwater to Indoor Air
r
NM
NM
r
NM
NM
Resident
Soil Gas to Indoor Air
R
6.4E-06
4.2E-01
R
6.4E-06
4.2E-01
Indoor Air
r
NM
NM
7
NM
NM
Groundwater to Indoor Air
r
NM
NM
r
NM
NM
Non -Residential Worker
Soil Gas to Indoor Air
7
4.8E-07
3.4E-02
Pr
4.8E-07
3.4E-02
Indoor Air
r
NM
NM
r
NM
NM
TOTAL SITEWIDE RISK FOR EACH RECEPTOR
1.1E-03
3.3E+01
1.1E-03
3.3E+01
2.6E-04
7.1E+00
2.6E-04
7.1E+00
7.0E-06
2.6E+00
1.0E-04
1.9E+00
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure.
3. NM = Not Modeled
4. NC -Pathway not calculated
North Carolina DEQ Risk Calculator

NorU Carolina DEO Rlak Calculabr

NorU Carolina DEO Rlak Calculabr

DEQ Risk Calculator - Vapor Intrusion - Resident Groundwater to Indoor Air r
Version Date: January 2023
November 2022 EPA RSL Table
Site ID: 23-0302
Exposure Unit ID: N/A
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor
intrusion risk, no risk values are calculated for these chemicals.
Groundwater concentrations are in ug/L. Air concentrations are in ug/m3
CAS #
Chemical Name:
Groundwater
Concentration
(ugh-)
Target Indoor
r Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non -
Carcinogenic
Hazard
Quotient
7440-38-2
Arsenic, Inorganic
0.779
6.5E-04
3.1E-03
7440-39-3
Barium
182
1.0E-01
71-43-2
Benzene
239
3.6E-01
6.3E+00
1.5E-04
1.7E+00
104-51-8
Butylbenzene, n-
16.4
135-98-8
Butylbenzene, sec-
3.06
7440-43-9
Cadmium (Water)
0.36
1.6E-03
2.1E-03
67-66-3
Chloroform
2.15
1.2E-01
2.0E+01
2.6E-06
3.2E-03
18540-29-9
Chromium(VI)
0.215
1.2E-05
2.1E-02
98-82-8
Cumene
12.1
8.3E+01
1.4E-02
107-06-2
Dichloroethane, 1,2-
10.5
1.1E-01
1.5E+00
4.7E-06
6.9E-02
100-41-4
Ethylbenzene
171
1.1 E+00
2.1 E+02
4.9E-05
5.3E-02
591-78-6
Hexanone, 2-
32.2
6.3E+00
3.9E-03
7439-92-1
-Lead and Compounds
1.97
7439-97-6
Mercury (elemental)
0.156
6.3E-02
1.8E-01
78-93-3
Methyl Ethyl Ketone (2-Butanone)
13.5
1.0E+03
6.0E-06
108-10-1
Methyl Isobutyl Ketone (4-methyl-2-pentanone)
9.25
6.3E+02
1.7E-05
1634-04-4
Methyl tert-Butyl Ether (MTBE)
2
1.1E+01
6.3E+02
4.4E-09
1.5E-05
84-74-2
-Dibutyl Phthalate
1.1
84-66-2
-Diethyl Phthalate
5.13
206-44-0
-Fluoranthene
0.121
91-20-3
--Naphthalene
19.2
8.3E-02
6.3E-01
4.2E-06
1.1E-01
103-65-1
Propyl benzene
42.5
2.1E+02
1.7E-02
7782-49-2
Selenium
4.31
4.2E+00
79-34-5
Tetrachloroethane, 1,1,2,2-
0.169
4.8E-02
5.2E-08
108-88-3
Toluene
407
1.0E+03
2.1E-02
95-63-6
Trimeth lbenzene, 1,2,4-
295
1.3E+01
1.2E+00
108-67-8
Trimeth lbenzene, 1,3,5-
121
1.3E+01
6.9E-01
108-38-3
X lene, m-
676
2.1E+01
1.9E+00
95-47-6
X lene, o-
200
2.1E+01
4.1E-01
106-42-3
X lene, -
676
2.1E+01
1.5E+00
Cumulative: I 2.1E-04 8.2E+00
North Carolina DEQ Risk Calculator

Date: January 2023
November 2022 EPA RSL Table
Site ID: 23-0302
Exposure Unit ID: N/A
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
All concentrations are in us/m3
CAS #
Chemical Name:
Soil Gas
Concentration
s
(ug/m)
Calculated
Indoor Air
Concentration
Co
(ug/ms)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1 E-06
Target Indoor Air
Conc. for Non -
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non -
Carcinogenic
Hazard
Quotient
67-64-1
Acetone
190
5.7
71-43-2
Benzene
12
0.36
3.6E-01
6.3E+00
1.0E-06
1.2E-02
75-15-0
Carbon Disulfide
38
1.14
1.5E+02
1.6E-03
67-66-3
Chloroform
15
0.45
1.2E-01
2.0E+01
3.7E-06
4.4E-03
98-82-8
Cumene
8.7
0.261
8.3E+01
6.3E-04
110-82-7
C clohexane
7.9
0.237
1.3E+03
3.8E-05
75-71-8
Dichlorodifluoromethane
12
0.36
2.1E+01
3.5E-03
100-41-4
Eth lbenzene
53
1.59
1.1E+00
2.1E+02
1.4E-06
1.5E-03
142-82-5
He tane, N-
24
0.72
8.3E+01
1.7E-03
110-54-3
Hexane, N-
16
0.48
1.5E+02
6.6E-04
78-93-3
Methyl Ethyl Ketone (2-Butanone)
19
0.57
1.0E+03
1.1E-04
108-10-1
Methyl Isobutyl Ketone (4-meth 1-2- entanone)
4.3
0.129
1
6.3E+02
4.1E-05
75-09-2
Methylene Chloride
3.7
0.111
1.0E+02
1.3E+02
1.1E-09
1.8E-04
103-65-1
Propylbenzene
19
0.57
2.1E+02
5.5E-04
127-18-4
Tetrachloroethylene
51
1.53
1.1E+01
8.3E+00
1.4E-07
3.7E-02
108-88-3
Toluene
170
5.1
1.0E+03
9.8E-04
79-01-6
Trichloroeth lene
1.2
0.036
4.8E-01
4.2E-01
7.5E-08
1.7E-02
75-69-4
Trichlorofluoromethane
1.4
0.042
95-63-6
Trimeth lbenzene, 1,2,4-
210
6.3
1.3E+01
1.0E-01
108-67-8
Trimeth lbenzene, 1,3,5-
87
2.61
1.3E+01
4.2E-02
75-01-4
Vinyl Chloride
0.65
0.0195
1.7E-01
1.7E+01
1.2E-07
2.3E-04
108-38-3
X lene, m-
290
8.7
2.1E+01
8.3E-02
95-47-6
X lene, o-
110
3.3
2.1E+01
3.2E-02
106-42-3
X lene, -
290
8.7
2.1E+01
8.3E-02
Cumulative: I 6.4E-06 4.2E-01
North Carolina DEC Risk Calculator

ersion Date: January 2023
asis: November 2022 EPA RSL Table
ID: 23-0302
asure Unit ID: N/A
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
Groundwater concentrations are in ue/L. Air concentrations are in ue/m3
CAS #
Chemical Name:
Groundwater
Concentration
(ugh)
Calculated
Indoor Air
Concentration
(ug/m)
Target Indoor
Air Cone. for
Carcinogens @
TCR = 1 E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non -
Carcinogenic
Hazard
Quotient
7440-38-2
Arsenic, Inorganic
0.779
2.9E-03
1.3E-02
7440-39-3
Barium
182
-
4.4E-01
71-43-2
Benzene
239
54.22935405
1.6E+00
2.6E+01
3.4E-05
4.1E-01
104-51-8
Butylbenzene, n-
16.4
10.66067048
-
135-98-8
Butylbenzene, sec-
3.06
2.201798855
7440-43-9
Cadmium (Water)
0.36
6.8E-03
8.8E-03
67-66-3
Chloroform
2.15
0.322587899
5.3E-01
8.6E+01
6.0E-07
7.5E-04
18540-29-9
Chromiurri
0.215
1.5E-04
8.8E-02
98-82-8
Cumene
12.1
5.688879804
3.5E+02
3.2E-03
107-06-2
Dichloroethane, 1,2-
10.5
0.506541292
4.7E-01
6.1E+00
1.1E-06
1.7E-02
100-41-4
Eth lbenzene
171
55.0891251
4.9E+00
8.8E+02
1.1E-05
1.3E-02
591-78-6
Hexanone, 2-
32.2
0.122691742
2.6E+01
9.3E-04
7439-92-1
Lead and Compounds
1.97
7439-97-6
-Mercury (elemental)
0.156
0.054912
2.6E-01
4.2E-02
78-93-3
Methyl Ethyl Ketone (2-Butanone)
13.5
0.031404334
4.4E+03
1.4E-06
108-10-1
Methyl Isobutyl Ketone (4-meth 1-2- entanone)
9.25
0.052187244
2.6E+03
4.0E-06
1634-04-4
Methyl tert-Butyl Ether (MTBE)
2
0.047996729
4.7E+01
2.6E+03
I 1.0E-09
3.7E-06
84-74-2
-Dibutyl Phthalate
1.1
8.13982E-05
84-66-2
-Diethyl Phthalate
5.13
0.000127935
206-44-0
-Fluoranthene
0.121
4.38291E-05
91-20-3
-Naphthalene
19.2
0.345380213
3.6E-01
2.6E+00
9.6E-07
2.6E-02
103-65-1
Propylbenzene
42.5
18.24407195
8.8E+02
4.2E-03
7782-49-2
Selenium
4.31
1.8E+01
79-34-5
Tetrachloroethane, 1,1,2,2-
0.169
0.002535691
2.1E-01
1.2E-08
108-88-3
Toluene
407
110.4856909
4.4E+03
5.0E-03
95-63-6
Trimeth lbenzene, 1,2,4-
295
74.29272281
5.3E+01
2.8E-01
108-67-8
Trimeth lbenzene, 1,3,5-
121
43.38389207
5.3E+01
1.7E-01
108-38-3
X lene, m-
676
198.4333606
8.8E+01
4.5E-01
95-47-6
X lene, o-
200
42.35486509
8.8E+01
9.7E-02
106-42-3
X lene, -
676
190.6950123
8.8E+01
4.4E-01
Cumulative: I 4.8E-05 I 2.0E+00
North Carolina DEC Risk Calculator

ersion Date: January 2023
asis: November 2022 EPA RSL Table
ID: 23-0302
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
All concentrations are in ue/m3
CAS #
Chemical Name:
Soil Gas
Concentration
s
(ug/m)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Cone. for
Carcinogens @
TCR=1E-06
Target Indoor Air
Cone. for Non-
Carcinogens @
THQ=0.2
Calculated
Carcinogenic
Risk
Calculated
Non -
Carcinogenic
Hazard
Quotient
67-64-1
Acetone
190
1.9
71-43-2
Benzene
12
0.12
1.6E+00
2.6E+01
7.6E-08
9.1E-04
75-15-0
Carbon Disulfide
38
0.38
6.1E+02
1.2E-04
67-66-3
Chloroform
15
0.15
5.3E-01
8.6E+01
2.8E-07
3.5E-04
98-82-8
Cumene
8.7
0.087
3.5E+02
5.0E-05
110-82-7
C clohexane
7.9
0.079
5.3E+03
3.0E-06
75-71-8
Dichlorodifluoromethane
12
0.12
8.8E+01
2.7E-04
100-41-4
Eth lbenzene
53
0.53
4.9E+00
8.8E+02
1.1E-07
1.2E-04
142-82-5
Heptane, N-
24
0.24
3.5E+02
1.4E-04
110-54-3
Hexane, N-
16
0.16
6.1E+02
5.2E-05
78-93-3
Methyl Ethyl Ketone (2-Butanone)
19
0.19
4.4E+03
8.7E-06
108-10-1
Methyl Isobutyl Ketone (4-meth 1-2- entanone)
4.3
0.043
2.6E+03
3.3E-06
75-09-2
Methylene Chloride
3.7
0.037
1.2E+03
5.3E+02
3.0E-I I
1.4E-05
103-65-1
Propylbenzene
19
0.19
8.8E+02
4.3E-05
127-18-4
Tetrachloroethylene
51
0.51
4.7E+01
3.5E+01
1.1E-08
2.9E-03
108-88-3
Toluene
170
1.7
4.4E+03
7.8E-05
79-01-6
Trichloroethylene
1.2
0.012
3.0E+00
1.8E+00
4.0E-09
1.4E-03
75-69-4
Trichlorofluoromethane
1.4
0.014
95-63-6
Trimethylbenzene, 1,2,4-
210
2.1
5.3E+01
8.0E-03
108-67-8
Trimethylbenzene, 1,3,5-
87
0.87
5.3E+01
3.3E-03
75-01-4
Vinyl Chloride
0.65
1 0.0065
2.8E+00
7.0E+01
2.3E-09
1.9E-05
108-38-3
Xylene, m-
290
2.9
8.8E+01
6.6E-03
95-47-6
Xylene, o-
110
1.1
8.8E+01
2.5E-03
106-42-3
Xylene, p-
290
2.9
8.8E+01
6.6E-03
Cumulative: I 4.8E-07 I 3.4E-02
North Carolina DEC Risk Calculator