WS-28005_47292_CA_CLO_20200904_UsedOilTankClosureRpt

September 03, 2020
Mr. Gene Mao
Hydrogeologist Environmental Health Division Guilford County Dept. of Health and Human Services 400 W. Market Street, Suite 300
Greensboro, NC 27401
Dear Mr. Mao:
Subject: UST System Closure Report Ryder Greensboro NC LC 0134
520 Long Meadow Drive Salisbury, Rowan County, North Carolina CEC Project 190-913
Civil & Environmental Consultants, Inc. (CEC) is pleased to submit the attached UST System
Closure Report for the above referenced Subject Property.
If you have any questions or require additional services, please feel free to contact us at [phone].
Sincerely,
CIVIL & ENVIRONMENTAL CONSULTANTS, INC.
Donald Cobb, P.G. Project Manager Britney C. Barnes Project Manager
Attachments
September 4, 2020
See Section 3.0 on Page 14 for Used
Oil Tank Assessment

UST CLOSURE REPORT RYDER GREENSBORO NC LC 0134 217 ATWELL AVENUE GREENSBORO, GUILFORD COUNTY
NORTH CAROLINA
Prepared For:
RYDER SYSTEM, INC. 800 EAST FAIRFIELD ROAD GREENVILLE, SOUTH CAROLINA 29605 Prepared By:
CIVIL & ENVIRONMENTAL CONSULTANTS, INC.
530 HOWELL ROAD, SUITE 203 GREENVILLE, SOUTH CAROLINA 29615 CEC PROJECT NO. 190-913
SEPTEMBER 03, 2020

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SITE INFORMATION
SITE NAME AND LOCATION: Ryder Greensboro NC LC 0134 Greensboro, Guilford County, North Carolina
INCIDENT NUMBER: Not applicable
LAND OWNER: Ryder Truck Rental, Inc. c/o Ryder Fuel Services, LLC
LATITUDE AND LONGITUDE: 36° 1'50.00"North, 79°47'13.50"West
DATE OF REPORT: September 03, 2020
LAND USE CATEGORY: Commercial
CONTACTS
PRIMARY CONTACT: Ryder Truck Rental, Inc. Ms. Sarah Galloway 800 East Fairfield Road
Greenville, South Carolina 29605 864-277-7020
TANK REMOVAL: Southern Pump & Tank Company 2724 John Deere Drive
Knoxville, Tennessee 37917
PRIMARY CONSULTANT: Civil & Environmental Consultants, Inc. (CEC) 530 Howell Road, Suite 203 Greenville, South Carolina 29615
864-626-3140
LABORATORY: Pace Analytical Services, LLC 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078
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TABLE OF CONTENTS
Page
1.0 INTRODUCTION..............................................................................................................1 2.0 DIESEL & MOTOR OIL UST SYSTEM CLOSURE ...................................................2 2.1 Diesel & Motor Oil Ust Removal ....................................................................................... 2 2.2 Product Piping And Under Dispenser Sump Removal ....................................................... 4 2.3 Soil Sampling, Monitoring Well Installation And Groundwater Sampling ........................ 5 2.3.1 Soil Sampling ...................................................................................................................... 5 2.3.2 Monitoring Well Installation And Groundwater Sampling ................................................ 6 2.4 Soil And Groundwater Analytical Results .......................................................................... 7 2.4.1 Soil Analytical Results ........................................................................................................ 7
2.4.2 Groundwater Analytical Results ......................................................................................... 8 3.0 USED OIL UST CLOSURE ...........................................................................................10 3.1 Used Oil Ust Removal ...................................................................................................... 10 3.2 Soil Sampling, Monitoring Well Installation And Groundwater Sampling ...................... 12 3.2.1 Soil Sampling .................................................................................................................... 12 3.2.2 Monitoring Well Installation And Groundwater Sampling .............................................. 12 3.3 Soil And Groundwater Analytical Results ........................................................................ 13 3.3.1 Soil Analytical Results ...................................................................................................... 14 3.3.2 Groundwater Analytical Results ....................................................................................... 15 4.0 FINDINGS AND CONCLUSIONS ................................................................................16 4.1 Diesel System Closure And Motor Oil Ust Removal ....................................................... 16 4.2 Used Oil Ust Removal ...................................................................................................... 17 5.0 LIMITATIONS ................................................................................................................19
FIGURES
Figure 1 – Site Topographic Location Map Figure 2 – Site Aerial Map Figure 3 – UST Excavation and Sample Location Map
TABLES
Table 1 – Summary of Constituents Detected in the Soil – Diesel System and Motor Oil UST Table 2 – Summary of Constituents Detected in the Soil – Used Oil UST Table 3 – Summary of Constituents Detected in the Groundwater
LISTS OF APPENDICES
Appendix A – Photographic Log Appendix B – NCDEQ UST Forms
Appendix C – Non-Hazardous Waste Manifest and Disposal Documentation
Appendix D – Laboratory Analytical Data Sheets Appendix E –Well Construction Diagrams & Well Construction Records
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September 03, 2020
1.0 INTRODUCTION
On behalf of Ryder Truck Rental, Inc. (Ryder), Civil & Environmental Consultants, Inc. (CEC)
performed observation and documentation of the closure of a diesel underground storage tank (UST)
system, removal of a motor oil UST, and removal of a used oil UST located at 217 Atwell Avenue in
Greensboro, Guilford County, North Carolina (Site), Figure 1 and Figure 2. This facility performs
routine maintenance on leased and rental vehicles and operates a fueling station. The diesel UST
system was closed to facilitate the installation of a new diesel UST system, and the motor oil and used
oil USTs were removed to facilitate a transition from the USTs to above ground storage tanks (ASTs).
The closure activities for the UST system are discussed herein and were performed in accordance
with the North Carolina Department of Environmental Quality Guidelines for Site Checks, Tank
Closure, and Initial Response and Abatement for UST Releases. A photographic log documenting
the closure activities is provided as Appendix A. The location of the former USTs, piping, and under-
dispenser containment (UDC) sumps as well as the approximated closure sample locations are shown
on Figure 3.
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September 03, 2020
2.0 DIESEL & MOTOR OIL UST SYSTEM CLOSURE
CEC mobilized to the Ryder Greensboro facility to perform observation, documentation, and soil
sampling associated with UST closure activities which were conducted March 17 – April 21, 2020.
Closure activities were conducted in accordance with the North Carolina Department of
Environmental Quality (NCDEQ) Guidelines for Site Checks, Tank Closure, and Initial Response
and Abatement for UST Releases.
The diesel UST system included four 12,000-gallon USTs, four satellite UDC sumps, two master
UDC sumps, and below grade product piping. The diesel UST basin also included a 6,000-gallon
motor oil UST which was removed concurrently with the diesel USTs. In addition to the diesel
and motor oil USTs, a 1,000-gallon used oil UST, located in a separate UST basin, was also
removed. The removal activities associated with the 1,000-gallon used oil UST are discussed
further in Section 3 of this report.
The UST system removal activities were conducted by Southern Pump and Tank Company
(SPATCO) in combination with Hazmat Emergency Response & Remediation, Inc. (HERR).
Prior to initiating the UST removal activities, a UST-3 Notice of Intent form was completed and
submitted to the NCDEQ on January 14, 2020. Following removal of the USTs, a UST-2A form
was completed and submitted to the NCDEQ. The completed UST-3 and UST-2A forms are
provided in Appendix B.
2.1 DIESEL & MOTOR OIL UST REMOVAL
The diesel and motor oil USTs were installed in one tank basin located on the northern portion of
the site and adjacent to the eastern side of the fuel canopy. Once concrete was removed from the
top of the basin and the USTs were accessible, the remaining tank content was evacuated and the
USTs were pressure washed. Removal of the content of the USTs was conducted on March 18,
2020 and again on March 21, 2020. According to the non-hazardous waste manifest,
approximately 24,743 gallons of fluid were evacuated on March 18 and approximately 1.22 tons
of fluid (a combination of remnant product, sludge, and wash water) were evacuated on March 21.
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September 03, 2020
After they were washed, a representative from SPATCO measured explosive vapor levels within
each of the USTs while a representative of the Guilford County Fire Department was on site. The
Guilford County Fire Department representative confirmed the measurement of the explosive
vapor levels were acceptable and observed the removal of the USTs in accordance with the
NCDEQ regulations. A copy of the disposal documentation for the USTs is provided in Appendix
C. The location of the UST basin and excavation area is shown on Figure 2 and Figure 3.
The four 12,000-gallon diesel USTs and single 6,000-gallon motor oil UST were oriented east-
west within the tank basin. Once removed from the basin, the USTs were crushed and transported
off-site for disposal. Each of the USTs was constructed of double-walled fiberglass, and apart
from perforations made by the excavator bucket for tank cleaning and removal, evidence of
perforations and/or cracking of the exterior of the USTs was not observed. Upon removal of the
USTs, the excavation extents measured approximately 50 feet east-west by 60 feet north-south by
approximately 12 feet in depth below the ground surface (bgs). Groundwater was encountered in
the excavation at approximately 9 feet bgs.
The tank basin was backfilled with pea gravel during the original installation of the UST system.
As it was removed from the excavation, the pea gravel was observed for visual evidence of
petroleum related impacts (i.e. staining) and screened for relative levels of volatile organic vapors
using a MiniRAE photoionization detector (PID). Visual evidence of petroleum related impact
was not observed and the PID did not detect volatile organic vapors at concentrations above
ambient background (0.0 parts per million). Because of the extent of the gravel backfill present
beyond that which immediately surrounded the USTs, native soil was not observed on the
excavation side walls. In lieu of collecting closure samples of the pea gravel from the excavation
side walls above the groundwater interface, the closure soil samples were collected from native
soil just outside the excavation through the use of direct push drilling and sampling techniques.
Based on the size of the excavation soil samples, EW1 through EW5, were collected to the east of
the UST excavation and soil samples NW1 through NW4 and SW1 through SW4 were collected
to the north and south of the excavation, respectively. One additional soil sample, SW3.2, was
collected approximately 5 feet farther to the south of soil sample SW3 due to a detection of volatile
organic vapors of 4.2 parts per million (ppm) in the SW3 soil sample. Laboratory analysis of soil
sample SW3.2 was placed on hold pending the analysis of SW3. Based on the results of soil
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September 03, 2020
sample SW3, sample SW3.2 was not analyzed by the laboratory. Closure soil samples were not
collected from the west of the excavation due to its proximity to the fuel canopy. Details of the
soil sampling and the laboratory analysis is discussed further in section 2.3. In addition, the
approximate location of the excavation area and soil samples are shown on Figure 3.
Groundwater was encountered in the UST basin at approximately 9-feet bgs, above the bottom of
the USTs. Because soil samples could not be collected from the bottom of the excavation due to
the depth of the groundwater, one groundwater monitoring well, MW-1, was installed on the
northern and presumed down gradient end of the excavation in accordance with the NCDEQ
regulations. Details of the well installation activities and results of the groundwater samples are
provided later in this report.
2.2 PRODUCT PIPING AND UNDER DISPENSER SUMP REMOVAL
Closure of the UST system included removal of the four satellite UDC sumps, two master UDC
sumps, and subgrade product piping. Locations of these system components are shown on Figure
3. The remnant fluid from the sumps and product piping was previously evacuated during the
same time frame as it was evacuated from the USTs. As the trench from where the system
components were removed was backfilled with pea gravel during its initial construction, the pea
gravel immediately surrounding the sumps and product piping was observed for the presence of
staining and screened for the presence of volatile organic vapors using the PID. Obvious visual
evidence of petroleum impacts was not observed and the PID did not detect volatile organic vapors
above ambient background of 0.0 parts per million (ppm).
Soil samples, UDC 1 through UDC 3, UDC 5 and UDC 8, were collected from the native soil
beneath UDC sumps and submitted for laboratory analysis. (It should be noted, the sample UDC
8 was originally labeled UDC 6 during the sampling; however, due to the misinterpretation by the
laboratory, this sample was identified in the laboratory data as UDC 8). A soil sample was not
collected from beneath one of the master UDC sumps, UDC 4, due to the presence of water in the
excavation following the removal of the pea gravel. Because the UST basin was situated
immediately adjacent to the fuel canopy and due to the short length of piping between the UDC
sumps, soil samples were not collected beneath the product piping. The approximate soil sample
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September 03, 2020
locations are shown on Figure 3. Soil sample identifications, associated laboratory analysis, and
corresponding analytical results are summarized on Table 1 and are further discussed in Subsection
2.3 of this report.
2.3 SOIL SAMPLING, MONITORING WELL INSTALLATION AND
GROUNDWATER SAMPLING
2.3.1 Soil Sampling
In general, soil samples beneath the UDC sumps were collected from the excavator bucket and
placed directly into laboratory prepared containers while the sampler was wearing a new pair of
nitrile gloves for each sample collected. Samples were collected from the center of the excavator
bucket where soil was not in direct contact with the side or bottom of the bucket.
In an effort to collect closure soil samples from the native soil adjacent to the excavation, direct
push drilling and sampling techniques were employed. Continuous soil samples were collected
from the ground surface to approximately 9 to 10 feet bgs at each of the sampling locations. Soil
samples retrieved from the boreholes were screened using the PID for relative levels of volatile
organic vapors and observed for visual evidence of petroleum related impacts, such as staining of
the soil. Groundwater was consistently encountered at approximately 9 feet bgs and soil samples
were collected from approximately 7 feet bgs, two feet above the water table interface as it was
observed during drilling and previous excavation activities. Soil samples were collected from the
acetate liners used to retrieve the soil from the borings and placed directly into laboratory prepared
containers while the sampler was wearing a new pair of nitrile gloves for each sample collected.
Once collected, the soil samples were placed in a cooler with ice where they remained until
received by the laboratory for analysis. Proper Chain of Custody (COC) procedures were
maintained throughout the sampling and transportation process. The approximate locations where
the soil samples were collected are shown on Figure 3. The soil sample identifications, laboratory
analysis, and corresponding results are provided on Table 1.
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September 03, 2020
Soil samples collected from beneath the UDC sumps, UDC-1 though UDC-3, UCD-5, and UDC-
8, and the excavation side walls, NW1 though NW4, SW1 through SW4, and EW1 through EW5,
were submitted for analysis to a North Carolina certified laboratory, Pace Analytical Services, for
total petroleum hydrocarbons (TPH) diesel and gasoline range (DRO and GRO, respectively) by
EPA Method 8015C.
2.3.2 Monitoring Well Installation and Groundwater Sampling
On April 21, 2020, CEC observed the installation of one monitoring well, MW-1, from which a
groundwater sample was collected on April 23, 2020 and again on June 5, 2020 and submitted for
laboratory analyses. The approximate location of monitoring well, MW-1, is shown on Figure 3.
MW-1 was advanced using 4.25-inch inside diameter hollow stem augers to a total depth of
approximately 18 feet bgs. Based on conditions of the soil during drilling, groundwater was
encountered at approximately 9 feet bgs. MW-1 was installed to a depth of 18 feet and was
constructed of 2-inch Schedule 40 PVC well casing and screen. The well screen was 0.01-inch
slotted and 10 feet in length. The borehole annulus surrounding the well screen was backfilled
with clean silica filter sand to approximately 6 feet bgs then topped with bentonite to
approximately 4 feet bgs. The remaining annulus surrounding the well casing was backfilled with
cement to just below the ground surface. The monitoring well was secured with an expandable
locking well cap and the surface completed with a flush-mounted manhole cover. A well
construction diagram is provided in Appendix E.
Following its installation, MW-1 was developed in an effort to evacuate the suspended solids in
the sand pack around the well screen. Approximately three well volumes (6 gallons) were
evacuated during the well development activities. Prior to the collection of groundwater samples,
MW-1 was purged of an additional three well volumes. Field parameters including pH,
conductivity, temperature, dissolved oxygen, and oxidation reduction potential, were measured
during groundwater purging and sampling activities. Although MW-1 was both developed and
purged and the field parameters had stabilized, the groundwater sample collected was observed to
be very turbid. Based on the field observations of elevated turbidity in combination with the results
of the laboratory analysis of the April 2020 groundwater sample collected from MW-1, which
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September 03, 2020
identified EPH/VPH range C09-C22 aromatics at a concentration above the North Carolina
Department of Environmental Quality 2L Groundwater Quality Standards (NCDEQ 2L GWQS),
MW-1 was resampled in June 2020. Field parameters were not measured during the re-sampling
due to technical issues with the YSI multiparameter water quality instrument; however, turbidity
was measured at 50.16 NTUs at the time the groundwater sample was collected. Results of the
groundwater sampling are discussed further in the following subsection (2.3.3 – Soil and
Groundwater Analytical Results).
Groundwater was purged and sampled from MW-1 using a peristaltic pump and disposable Teflon
lined tubing. After the well was purged, groundwater pumped to the surface was decanted directly
into laboratory prepared containers. The collected groundwater samples were placed in a cooler
with ice and managed under proper COC procedures from the time of sample collection through
receipt by the laboratory. Sampled groundwater was submitted to a North Carolina Certified
laboratory for analysis for VOCs using EPA Method SM6200B, base/neutrals and acids plus
largest 10 non-target peaks using EPA Method 625, and MADEP VPH and EPH. Results of the
laboratory analysis are discussed in the section below and the laboratory analytical data sheets are
provided in Appendix D.
2.4 SOIL AND GROUNDWATER ANALYTICAL RESULTS
As previously discussed, both soil and groundwater samples were collected for closure of the diesel
UST system. A total of 19 soil samples and two (2) groundwater samples were collected and
submitted for laboratory analysis. A tabularized summary of the soil and groundwater results are
provided on Table 1 and Table 3, respectively, and the laboratory analytical data sheets are
provided in Appendix D.
2.4.1 Soil Analytical Results
A synopsis of the laboratory analytical results of the soil samples collected during the removal
activities is provided below:
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September 03, 2020
•Laboratory analysis did not detect either TPH DRO or TPH GRO at concentrations above
the laboratory reporting limits in soil samples, UDC-01 through UDC-03, UDC-05 and
UDC-08, collected from beneath the UDC sumps.
•Laboratory analysis detected TPH GRO at estimated concentrations above the laboratory
detection limits, but below the NCDEQ Action Level in the each of the side wall soil
samples, apart from one, NW2:
Estimated concentrations of TPH GRO ranged from 1.6 milligrams per kilogram
(mg/kg) to 3.0 mg/kg, below the Action Level of 50 mg/kg.
•Laboratory analysis detected TPH DRO in six of the side wall samples collected, EW2
through EW5, SW1, and SW2, at concentrations above the laboratory detection limits but
below the NCDEQ Action Level:
TPH DRO was detected at an estimated concentration of 4.1 mg/kg in sample
EW2, an estimated concentration of 5.7 mg/kg in sample EW3, an estimated
concentration of 6.9 mg/kg in sample EW4, an estimated concentration of 3.4
mg/kg in sample EW5, a concentration of 8.1 mg/kg in sample SW1, and an
estimated concentration of 5.6 in sample SW2, each below the Action Level of 100
mg/kg.
2.4.2 Groundwater Analytical Results
Groundwater samples were collected from monitoring well MW-1 during April 2020 and June
2020. A synopsis of the laboratory analytical results of these groundwater samples is provided
below:
•During April 2020, laboratory analysis detected VPH range C05-C08 aliphatics and
EPH/VPH range C09-C18 aliphatics at concentrations above the laboratory detection
limits, but below the NC 2L GQWS. In addition, VPH/EPH range C09-C22 aromatics
were detected at a concentration above both the laboratory reporting limits and the NC 2L
GWQS.
VPH range C05-C08 aliphatics were detected at an estimated concentration of 84.4
micrograms per liter (ug/L), below the GWQS of 400 ug/L and EPH/VPH range
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September 03, 2020
C09-C18 aliphatics were detected at a concentration of 298 ug/L, below the GWQS
of 700 ug/L.
VPH/EPH range C09-C22 aromatics were detected at a concentration of 403 ug/L,
above the GWQS of 200 ug/L.
•Apart from one constituent, n-propylbenzene, VOCs were not detected in the April 2020
groundwater sample, MW-1, at concentrations above the laboratory reporting limits.
n-propylbenzene was detected at an estimated concentration of 0.47 ug/L, below
the NC 2L GWQS of 70 ug/L.
•SVOC’s were not detected above the laboratory reporting limits in the April 2020 MW-1
groundwater sample.
•During June 2020, laboratory analysis detected EPH/VPH range C09-C18 aliphatics and
VPH/EPH range C09-C22 aromatics at concentrations above the laboratory detection
limits, but below the associated GWQS for each of the constituents detected.
Concentrations for both of these constituents decreased from when MW-1 was sampled in
April 2020.
EPH/VPH range C09-C18 aliphatics were detected at an estimated concentration
of 241 ug/L, below the GWQS of 700 ug/L.
VPH/EPH range C09-C22 aromatics were detected at a concentration of 171 ug/L,
below the GWQS of 200 ug/L and below the concentration detected in this well
during April 2020 (403 ug/L).
•VOCs were not detected at concentrations above the laboratory reporting limits in the
groundwater sample collected during June 2020.
•Apart from one SVOC, fluorene, SVOCs were not detected at concentrations above the
laboratory reporting limits in the June 2020 groundwater sample collected from MW-1.
Fluorene was detected at an estimated concentration of 1.6 ug/L, below the GWQS
of 300 ug/L.
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3.0 USED OIL UST CLOSURE
In addition to closure of the diesel UST system and motor oil UST at the Ryder Greensboro NC
LC 134 (detailed in the previous section), CEC observed, documented, and collected soil and
groundwater samples in association with the closure of a 1,000-gallon UST containing used oil.
The used oil UST was located to the east of the facility maintenance bays, as shown on Figure 2
and Figure 3. Closure activities were conducted in accordance with the North Carolina Department
of Environmental Quality (NCDEQ) Guidelines for Site Checks, Tank Closure, and Initial
Response and Abatement for UST Releases.
A NCDEQ UST-61 24-hour Release and UST Leak Reporting Form was submitted to the NCDEQ
on February 17, 2020. The 24-hour release notification was submitted as a result of possible
product noticed in an observation well located within the used oil UST basin. This observation
was during a site visit made in preparation for UST closure activities. Immediate response action
was initiated. This action included disconnecting the pump inside the maintenance bay, thus
halting further use of the UST. In addition, the contents of the UST were evacuated on February
18, 2020 by Safety-Kleen Systems, Inc. According to the disposal documentation, 240 gallons of
product were removed from the used oil UST during the immediate response actions. An
additional 7,200 gallons of water/fuel mix was evacuated from the used oil UST basin on March
30, 2020. A copy of the UST-61 form as well as the disposal documentation for the fluid removal
are provided in Appendix B and Appendix C, respectively.
The 1,000-gallon used oil UST was removed concurrently with the closure of the diesel UST
system. Prior to initiating the UST removal activities, a UST-3 Notice of Intent form was
completed and submitted on January 14, 2020 to the NCDEQ. Following removal of the USTs, a
UST-2A form was completed and submitted to the NCDEQ. The completed UST-3 and UST-2A
forms are provided in Appendix B.
3.1 USED OIL UST REMOVAL
The 1,000-gallon used oil UST was located to the east of the maintenance bay, on the opposite
side of the facility from the diesel and motor oil UST basin. Once concrete was removed from the
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September 03, 2020
top of the basin and the UST was accessible, the interior of the tank was pressure washed. Pressure
washing was conducted during the same time frame as the diesel and motor oil tanks were cleaned
and the volume of wash fluid and sludge removed from the used oil UST was a portion of the 1.22
tons of fluid transported off-site for disposal. Prior to the removal of the UST, a representative
from SPATCO measured explosive vapor level within the tank while a representative of the
Guilford County Fire Department was on site. The Guilford County Fire Department
representative confirmed the measurement of the explosive vapor level was acceptable and
observed the removal of the UST in accordance with the NCDEQ regulations. The used oil UST
was removed on March 20, 2020. A copy of the disposal documentation for the USTs is provided
in Appendix C. The location of the UST basin and excavation area is shown on Figure 2 and
Figure 3.
The 1,000-gallon used oil UST was oriented east-west within the tank basin. Once removed from
the basin, the UST was crushed and transported off-site for disposal. The used oil UST was
constructed of double-walled fiberglass, and apart from perforations made by the excavator bucket
for tank cleaning and removal, evidence of perforations and/or cracking of the exterior of the UST
was not observed.
The tank basin was backfilled with pea gravel during the original installation of the UST. As it
was removed from the excavation, the pea gravel was observed for visual evidence of petroleum
related impacts (i.e. staining) and screened for relative levels of volatile organic vapors using a
PID. Discoloration of the pea gravel was observed and the PID detected the presence of volatile
organic vapors at concentrations ranging from 70 ppm to over 300 ppm. Due to incoming
inclement weather at the time the UST was removed from its tank basin, the excavation was
temporarily backfilled with clean fill dirt.
On April 6, 2020, approximately 776 gallons of water, which had accumulated in the used oil tank
basin and was in contact with the impacted soil, was evacuated prior to soil removal activities. On
April 14, 2020, the fill dirt, impacted pea gravel, and impacted soil were removed from the used
oil UST basin. Approximately 129 tons of impacted soil/pea gravel/concrete debris were removed
and transported off-site for disposal. The non-hazardous waste manifests are provided in
Appendix C. At the completion of the excavation activities, the excavation extents measured
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approximately 20 feet east-west by 15 feet north-south, and approximately 12 feet in depth below
the ground surface. Groundwater was encountered in the excavation at approximately 9 feet bgs,
above the bottom of the UST. As such, soil samples, W Wall, E Wall, N Wall, and S Wall, were
collected from each of the four sidewalls at approximately 7 feet bgs and submitted for laboratory
analysis. One monitoring well, MW-2, was installed adjacent to the tank basin and sampled.
Details of the soil sampling and the laboratory analysis is discussed further in section 3.2. In
addition, the approximate location of the excavation area, soil samples, and monitoring well are
shown on Figure 3.
3.2 SOIL SAMPLING, MONITORING WELL INSTALLATION AND GROUNDWATER SAMPLING
3.2.1 Soil Sampling
In general, soil samples (W Wall, E Wall, S Wall, and N Wall) were collected from the center of
the excavator bucket where soil was not in direct contact with the side or bottom of the bucket.
Once collected, the soil samples were placed in a cooler with ice where they remained until
received by the laboratory. Proper Chain of Custody (COC) procedures were maintained
throughout the sampling and transportation process. The approximate locations where the soil
samples were collected are shown on Figure 3. The soil sample identifications, laboratory analysis,
and corresponding results are provided on Table 3.
Soil samples were submitted to Pace Analytical Services for analysis for VOCs using EPA Method
8260B, SVOCs using EPA Method 8270D, and VPH and EPH by MADEP methods.
3.2.2 Monitoring Well Installation and Groundwater Sampling
One monitoring well, MW-2, was installed adjacent to the used oil UST tank basin. The well
installation activities were conducted during the same time frame as the installation of monitoring
well MW-1. Additionally, MW-2 was installed in a manner consistent with the installation of
MW-1. The approximate location of MW-2 is shown on Figure 3.
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September 03, 2020
The boring for MW-2 was advanced to a total depth of approximately 18 feet bgs. MW-2 was
installed to a depth of 18 feet and was constructed of 2-inch Schedule 40 PVC well casing and
screen. The well screen was 0.01-inch slotted and 10 feet in length. The borehole annulus
surrounding the well screen was backfilled with clean silica filter sand to approximately 6 feet bgs,
and then topped with bentonite to approximately 4 feet bgs. The remaining annulus surrounding
the well casing was backfilled with cement to just below the ground surface. The monitoring well
was secured with an expandable locking well cap and the surface completed with a flush-mounted
manhole cover. A well construction diagram is provided in Appendix E.
Following its installation, MW-2 was developed in an effort to evacuate the suspended solids in
the sand pack around the well screen. Approximately three well volumes (6 gallons) were
evacuated during the well development activities. Prior to the collection of groundwater samples,
MW-2 was purged of an additional three well volumes. Field parameters including pH,
conductivity, temperature, dissolved oxygen, and oxidation reduction potential, were measured
during groundwater purging and sampling activities.
Groundwater was purged and sampled from monitoring well, MW-2, using a peristaltic pump and
disposable Teflon lined tubing. After the well was purged, groundwater pumped to the surface
was decanted directly into laboratory prepared containers. The collected groundwater samples
were placed in a cooler with ice and managed under proper COC procedures from the time of
sample collection through receipt by the laboratory for analysis. Sampled groundwater was
submitted to a North Carolina Certified laboratory for analysis for VOCs using EPA Method
SM6200B, base/neutrals and acids plus largest 10 non-target peaks using EPA Method 625,
MADEP VPH and EPH, lead, and chromium. Results of the laboratory analysis are discussed in
the section below and the laboratory analytical data sheets are provided in Appendix D.
3.3 SOIL AND GROUNDWATER ANALYTICAL RESULTS
As previously discussed, both soil and groundwater samples were collected for closure of the used
oil UST. A total of four (4) soil samples and one (1) groundwater sample were collected and
submitted for laboratory analysis. A tabularized summary of the groundwater and soil sampling
-14- UST Closure Report/Ryder Greensboro, NC
September 03, 2020
results are provided on Table 2 and Table 3, respectively, and the laboratory analytical data sheets
are provided in Appendix D.
3.3.1 Soil Analytical Results
A synopsis of the laboratory analytical results of the soil samples collected during the removal
activities is provided below:
•Apart from EPH/VPH range C09-C18 aliphatics and VPH/EPH range C09-C22 aromatics,
EPH and VPH were not detected in the soil samples collected from the excavation side
walls at concentrations above the laboratory detection limits:
EPH/VPH range C09-C18 aliphatics were detected at an estimated concentration
of 3.68 mg/kg in one of the soil samples, W Wall, collected from the western
excavation side wall, below the Soil to Water MSCC of 68 mg/kg;
EPH/VPH range C09-C22 aromatics were detected at an estimated concentration
of 2.58 mg/kg in one of the soil samples, N Wall, collected from the northern
excavation side wall, below the Soil to Water MSCC of 540 mg/kg.
•With the exception of acetone detected in three of the four side wall samples, VOCs were
not detected at concentrations above the laboratory reporting limits in the soil samples
collected:
Acetone was detected at estimated concentrations in soil samples, E Wall (0.036
mg/kg), S Wall (0.070 mg.kg), and N Wall (0.0634 mg.kg), below the Soil-to-
Water MSCC of 24 mg/kg;
Acetone is a common laboratory contaminant, and the low levels detected in these
samples are likely due to such contamination.
•Chromium was detected in each of the soil samples collected at a concentration above the
laboratory reporting limits:
Chromium was detected in three of the four soil samples (W Wall, E Wall, and N
Wall) at concentrations above the Soil-to-Water MSCC, but below the Residential
MSCC. Detected concentrations were 36.9 mg/kg, 34.5 mg/kg, and 37.5 mg/kg,
respectively, versus the MSCC of 5.4 mg/kg; and
-15- UST Closure Report/Ryder Greensboro, NC
September 03, 2020
Chromium was detected at a concentration of 79.6 mg/kg, above the Residential
MSCC of 47 mg/kg, in soil sample S Wall, but below the Industrial MSCC of 1,226
mg/kg for this constituent.
•Lead was detected in one of the soil samples (W Wall) at a concentration above the
laboratory reporting limit, but below the Soil-to-Water MSCC:
Lead was detected at a concentration of 4.18 mg/kg, below the Soil-to-Water
MSCC of 270 mg/kg.
•SVOCs were not detected in the soil samples collected at concentrations above the
laboratory reporting limits.
3.3.2 Groundwater Analytical Results
A synopsis of the laboratory analytical results of the groundwater sample collected from
monitoring well, MW-2, is provided below:
•EPH/VPH range C09-C18 aliphatics and VPH range C05-C08 aliphatics were detected in
the groundwater sample, MW-2, at concentrations above the laboratory detection limits,
but below the GWQS for these constituents.
EPH/VPH range C09-C18 aliphatics were detected at an estimated concentration
of 37.3 ug/L, below the GWQS of 400 ug/L; and
VPH range C05-C08 aliphatics were detected at a concentration of 44.8 ug/L,
below the GWQS of 700 ug/L.
•Both chromium and lead were detected in the groundwater sample collected at
concentrations above the laboratory reporting limits and above the GWQS, but below the
NCDEQ Gross Contamination Levels (GCLs) for each of these constituents:
Chromium was detected at a concentration of 89.1 ug/L, above the GWQS of 10
ug/L, but below the GCL of 10,000 ug/L.
Lead was detected at a concentration of 20 ug/L, above the GWQS of 15 ug/L, but
below the GCL of 15,000 ug/L.
•Neither VOCs nor SVOCs were detected at concentrations above the laboratory reporting
limits in groundwater sample MW-2.
-16- UST Closure Report/Ryder Greensboro, NC
September 03, 2020
4.0 FINDINGS AND CONCLUSIONS
CEC observed the closure of a diesel UST system and the removal of multiple USTs located at the
Ryder Trucking Facility located at 217 Atwell Avenue in Greensboro, Guilford County, North
Carolina. The diesel UST system was comprised of four 12,000-gallon diesel USTs, four satellite
UDC sumps, two master UDC sumps, and associated below grade product piping. The diesel UST
basin also included a 6,000-gallon motor oil UST which was removed concurrently with the diesel
USTs. A 1,000-gallon used oil UST located in a separate tank basin on the opposite side of the
facility was also removed. Because groundwater was encountered above the bottom of the USTs,
two groundwater monitoring wells, MW-1 and MW-2, were installed and sampled. Soil and
groundwater samples were collected in accordance with the NC DEQ Guidelines for Site Checks,
Tank Closure, and Initial Response and Abatement for UST Releases.
4.1 DIESEL SYSTEM CLOSURE AND MOTOR OIL UST REMOVAL
Neither visual nor olfactory evidence of petroleum related impacts were observed in the soil or the
groundwater during the excavation and sampling activities conducted in association with diesel
UST system and motor oil UST closure. Although TPH GRO and DRO were detected in one or
more of the samples collected from the native soil adjacent to the UST basin at concentrations
above the laboratory detection limits, the detected concentrations were below the Action Levels
by one or more order of magnitude. Neither TPH GRO nor DRO were detected in the samples
collected from beneath the UDC sumps.
As groundwater was encountered in the excavation above the bottom of the USTs, one
groundwater monitoring well, MW-1, was installed and sampled. Groundwater samples were
collected from this well during April 2020 and again in June 2020. While EPH/VPH range C09-
C22 aromatics were detected at a concentration above the GWQS in the groundwater sample
collected in April 2020, the concentration of this constituent decreased by more than half when the
well was resampled in June 2020 and was below the GWQS. Apart from EPH/VPH range C09-
C22 aromatics, petroleum related constituents identified in the groundwater samples collected
during both the April and June 2020 sampling events were detected at concentrations below their
respective GWQS.
-17- UST Closure Report/Ryder Greensboro, NC
September 03, 2020
Based on the decrease of the constituent concentrations in the groundwater samples, the presence
of petroleum related constituents detected does not appear to indicate a significant or ongoing
release occurred during the operation of the diesel UST system or motor oil UST. Furthermore,
laboratory analysis of the soil samples in combination with the lack of visual indications of
petroleum impacts also provides evidence there was not a significant or ongoing petroleum release
associated with the operation of the diesel UST system or motor oil UST.
Based on the observations during removal activities and the laboratory analysis for the soil and
groundwater samples collected, CEC requests formal closure of the diesel UST system and motor
oil UST from the NCDEQ with No Further Action.
4.2 USED OIL UST REMOVAL
A 24-hour Release and UST Leak Reporting Form was submitted to the NCDEQ in association
with a product observed in an observation well located within the basin where the used oil UST
was located. Emergency response actions included halting further use through the disconnection
of the pump within the facility leading to the UST and evacuating approximately 240 gallons of
product from the UST. In addition, a total of approximately 7,976 gallons of water, which had
accumulated in the tank basin and was in direct contact with the impacted soil, was evacuated and
transported off-site for disposal. During the removal of the used oil UST, a limited amount of
petroleum impacted soil and pea gravel (approximately 129 tons) was removed and transported
off site for disposal. Soil samples collected from the excavation side walls did not detect petroleum
related constituents at concentrations above the Soil-to-Water MSCCs. Chromium was detected
at concentrations above the Soil-to-Water MSCCs in three of the four samples collected and above
the Residential MSCC in one of the soil samples collected.
As groundwater was encountered in the excavation above the bottom of the UST, one groundwater
monitoring well, MW-2, was installed and sampled. Two petroleum related constituents
(EPH/VPH aliphatics ranges C09-C18 and C04-C08) were detected at concentrations above the
laboratory reporting limits, but below the GWQS for the constituents detected. No other petroleum
related constituents were detected at concentrations above the laboratory reporting limits in the
groundwater sample MW-2. Both chromium and lead were detected in the groundwater sample
-18- UST Closure Report/Ryder Greensboro, NC
September 03, 2020
MW-2 at concentrations above the GWQS, but below the GCL. While these constituents could
potentially be associated with historic operation of the used oil UST, the source material has been
removed and it is expected the lead and chromium will naturally attenuate over time.
Based on the removal of approximately 129 tons of petroleum impacted soil in combination with
the soil and groundwater laboratory analysis, CEC requests formal closure of the used oil UST
from the NCDEQ with No Further Action.
-19- UST Closure Report/Ryder Greensboro, NC
September 03, 2020
5.0 LIMITATIONS
At the request of the client, CEC performed the observation and documentation of the removal of
a diesel UST system, which included four 12,000-gallon USTs, UDC sumps, and below grade
product piping. CEC also performed the observation and documentation of the removal of a 6,000-
gallon motor oil UST, located within the same tank basin as the diesel USTs, and 1,000-gallon
used oil UST, which was located in a separate tank basin. CEC’s observations and documentation
should not be considered an exhaustive assessment of potential environmental conditions at the
subject property.
This report has been prepared in keeping with accepted standards of practice for preparation of
removal activities of this type and using CEC's professional judgment. CEC makes no claim as to
the presence or absence of contamination except at the documented time the closure activities were
observed. No warranties, either expressed or implied, are made herein.
FIGURES
SITE
REFERENCE
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
SITE LOCATION MAP
190-9131"= 2,000'AUGUST 2020
SHP 1
RYDER TRUCK RENTAL
217 ATWELL AVENUE
GREENSBORO, NORTH CAROLINA 27406
GUILFORD COUNTY530 Howell Road · Suite 203 · Greenville, SC 29615
Ph: 864.626.3140 · 855.574.4331 · Fax: [phone]
www.cecinc.com
NORTH
BCB BCB
REFERENCE
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
SITE LAYOUT MAP
190-9131"= 100'AUGUST 2020
SHP BCB BCB 2
RYDER TRUCK RENTAL
217 ATWELL AVENUE
GREENSBORO, NORTH CAROLINA 27406
GUILFORD COUNTY530 Howell Road · Suite 203 · Greenville, SC 29615
Ph: 864.626.3140 · 855.574.4331 · Fax: [phone]
www.cecinc.com
NORTH
LEGEND
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
EXCAVATION AREA &
SAMPLE LOCATION MAP
190-9131"= 60'AUGUST 2020
SHP MSJ BCB 3
RYDER TRUCK RENTAL
217 ATWELL AVENUE
GREENSBORO, NORTH CAROLINA 27406
GUILFORD COUNTY530 Howell Road · Suite 203 · Greenville, SC 29615
Ph: 864.626.3140 · 855.574.4331 · Fax: [phone]
www.cecinc.com
NORTH
TABLES
Table 1Summary of Constituents Detected in SoilDiesel UST System & Motor Oil UST Ryder Greensboro North Carolina LC 0134217 Atwell AvenueGreensboro, Guilford County, North CarolinaCEC Project No: 190‐913NW1 NW2 NW3 NW4 EW1 EW2 EW3 EW4 EW5 SW1 SW2 SW3 SW3.2 SW4Sample Date 4/21/2020 4/21/2020 4/21/2020 4/21/2020 4/21/2020 4/21/2020 4/21/2020 4/21/2020 4/21/2020 4/21/2020 4/21/2020 4/21/2020 4/21/2020 4/21/2020Gasoline and Diesel Range Organics 8015 Diesel Range Organics  100 ND ND ND ND ND4.1J 5.7J 6.9J 3.4J 8.1 5.6JND NA NDGasoline Range Organics  501.7JND1.8J 1.8J1.6J 3.0J 1.8J 4.4J 1.8J1.9J 1.8J 2.6JNA1.7JUDC‐01 UDC‐02 UDC‐03 UDC‐05 UDC‐06Sample Date 3/20/2020 3/20/2020 3/20/2020 3/20/2020 3/20/2020Gasoline and Diesel Range Organics 8015 Diesel Range Organics  100 ND ND ND ND NDGasoline Range Organics  50ND NDNDND NDNotes:1) NCDEQ Action Level = North Carolina Department of Environmental Quality Site Checks, Tank Closure, and Initial Response and Abatement ‐ Action Level2) J = Estimated Concentration3)  NA = Not Analyzed4) ND = Not Detected above the laboratory reporting limit5) Bold = constituent detected above the laboratory reporting or method detection limitsParameterNCDEQAction LevelSample ID & Constituent Concentration mg/kg)ParameterNCDEQAction LevelSample ID & Constituent Concentration mg/kg)
Table 2
Summary of Constituents Detected in Soil
Used Oil UST
Ryder Greensboro North Carolina LC 0134
217 Atwell Avenue
Greensboro, Guilford County, North Carolina
CEC Project No: 190-913
W Wall E Wall S Wall N Wall
Sample Date 4/14/2020 4/14/2020 4/14/2020 4/14/2020
MADEP EPH and VPH
Aliphatics (C09-C18)68 939 24528 3.68J ND ND ND
Aromatics (C09-C22)540 1500 40000 ND ND ND 2.58J
Volatile Organic Compounds (VOCs) 8260D/5035A
Acetone 24 14,000 360,000 ND 0.063J 0.070J 0.0634J
Metals 6010D
Chromium 5.4 47 1,226 36.9 34.5 79.6 37.5
Lead 270 400 400 4.18 ND ND ND
Notes:
1)MSCC = North Carolina Department of Environmental Quality Site Checks, Tank Closure, and Initial Response and Abatement - Maximum Soil Contaminate Concentrations (MSCC)
2)J = Estimated Concentration
3)ND = Not Detected
4) Bold = constituent detected above the laboratory reporting or method detection limit
5)Bold and shaded = constituent concentration exceeds MSCC
Soil Samle ID & Constituent Concentration (mg/kg)
Parameter
Soil-to-Water
MSCC
Residential
MSCC
Industrial/
Commercial
MSCC
Table 3
Summary of Constituents Detected in Groundwater
Used Oil UST
Ryder Greensboro North Carolina LC 0134
217 Atwell Avenue
Greensboro, Guilford County, North Carolina
CEC Project No: 190-913
GWQS
(ug/L)
GCL
(ug/L)MW-1
MW-1
(Resample)MW-2
Well Location Used Oil UST
Sample Date 4/23/2020 6/5/2020 4/23/2020
Aliphatics (C05-C08)400 --84.8J ND 44.8J
Aliphatics (C09-C18)700 --298 241J 37.3
Aromatics (C09-C22)200 --403 171 ND
Chromium 10 10,000 NA NA 89.1
Lead 15 15,000 NA NA 20
n-Propylbenzene 70 30,000 0.47J ND ND
Fluorene 300 990 ND 1.6 J ND
Notes:
1)Concentrations are posted in micrograms per liter (ug/L).
2)GWQS = North Carolina Department of Environmental Quality 2L Groundwater Quality Standards (GWQS)
3)GCL = North Carolina Department of Environmental Quality Gross Contamination Levels for Groundwater (GCL)
4)J = Estimated Concentration
5)ND = Not Detected
6)NA = Not Analyzed
7)Bold and shaded = constituent concentration exceeds GWQS
Semi Volatile Organic Compounds (SVOCs) 625 RVE
Constituents
Comparison Criteria
Monitoring Well & Concentration of Constituents
(ug/L)
MADEP EPH and VPH
Metals 6010D
Volatile Organic Compounds (VOCs) 6200/6200B MSV
Diesel & Motor Oil UST
APPENDIX A
PHOTOGRAPHIC LOG
1 | Page
Photo Number: 1
Description:
View of the fuel canopy and diesel and motor oil UST excavation area prior to removal activities.
Photo Number: 2
Description:
View of fuel canopy showing location of
the fuel island and former location of the
fuel pumps.
Civil & Environmental Consultants, Inc.
Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
2 | Page
Photo Number: 3
Description:
View of the diesel and motor oil UST basin in the process of uncovering the top of the USTs
Photo Number: 4
Description:
Evacuation of the remnant content of the
diesel and motor oil USTs.
Civil & Environmental Consultants, Inc.
Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
3 | Page
Photo Number: 5
Description:
View of measuring LEL in USTs with Fire Marshall prior to removal.
Photo Number: 6
Description:
View of the diesel and motor oil UST
basin, showing example of the extent of
pea gravel backfill toward the fuel canopy.
Civil & Environmental Consultants, Inc.
Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
4 | Page
Photo Number: 7
Description:
View of the diesel and motor oil UST basin.
Photo Number: 8
Description:
View of the diesel and motor oil UST
basin, facing east. Note the extent of the
pea gravel backfill toward the east.
Civil & Environmental Consultants, Inc.
Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
5 | Page
Photo Number: 9
Description:
View of the diesel and motor oil UST basin once the UST have been removed and showing groundwater in the excavation.
Photo Number: 10
Description:
View of the removal of the UDC sumps
and product piping.
Civil & Environmental Consultants, Inc.
Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
6 | Page
Photo Number: 11
Description:
View of the area where the UDC sumps and product piping was removed.
Photo Number: 12
Description:
View of groundwater encountered
beneath UDC 4.
Civil & Environmental Consultants, Inc.
Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
7 | Page
Photo Number: 13
Description:
View of the native soil beneath the UCD sumps and product piping.
Photo Number: 14
Description:
View of area where UCD sumps and
product piping was removed;
groundwater in the vicinity of UCD 4.
Civil & Environmental Consultants, Inc.
Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
8 | Page
Photo Number: 15
Description:
View of the diesel and motor oil UST basin with the new UST installed and basin backfilled.
Photo Number: 16
Description:
Example of direct push soil sampling
outside the diesel and motor oil UST
basin for collection of closure soil samples.
Civil & Environmental Consultants, Inc.
Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
9 | Page
Photo Number: 17
Description:
View of monitoring well, MW-1, located to the north of the diesel and motor oil UST basin.
Photo Number: 18
Description:
View of the used oil UST excavation
area.
Civil & Environmental Consultants, Inc.
Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
10 | Page
Photo Number: 19
Description:
View of the impacted pea gravel and soil
removed from the used oil UST tank basin.
Photo Number: 20
Description:
View of the used oil UST excavation area.
Civil & Environmental Consultants, Inc. Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log
Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
11 | Page
Photo Number: 21
Description:
View of the used oil UST prior to
removal from the tank basin.
Photo Number: 22
Description:
View of removal of wash water and sludge from used oil UST.
Civil & Environmental Consultants, Inc. Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log
Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
12 | Page
Photo Number: 23
Description:
View of the impacted soil removed from
the used oil UST basin.
Photo Number: 24
Description:
View of excavation of impacted soil and pea gravel in the used oil UST basin.
Civil & Environmental Consultants, Inc. Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log
Ryder Greensboro NC LC 0134 217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
13 | Page
Photo Number: 25
Description:
View of the used oil UST basin once impacted soil has been removed.
Photo Number: 26
Description:
View of the used oil UST basin backfilled and capped with concrete; monitoring well, MW-2, is also shown.
Civil & Environmental Consultants, Inc. Greenville, South Carolina Phone [phone] ∙ Toll Free: 855/859-9932 www.cecinc.com
Photographic Log Ryder Greensboro NC LC 0134
217 Atwell Avenue Greensboro, North Carolina
CEC Project No. 190-913
APPENDIX B
NCDEQ UST FORMS
UST-2A Site Investigation Report for Permanent Closure or Change-in-Service of REGISTERED UST

Return completed form to: NC DEQ / DWM / UST SECTION 1646 MAIL SERVICE CENTER RALEIGH, NC 27699-1646 ATTN: REGISTRATION & PERMITTING phone [phone] fax [phone] http://www.wastenotnc.org/
STATE USE ONLY: Facility ID # Date Received
INSTRUCTIONS (READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deq.nc.gov/about/divisions/waste-management/waste-management-permit-guidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change-in-service: Where a UST system will be converted from storing a regulated substance to a non-regulated substance, complete sections I, II, III, IV, and VI
4. For more than 5 registered UST systems, attach additional forms as needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator must submit a written request and include: (1) contact information, (2) federal identification # or SSN, and (3) a copy of UST-2 form. The annual tank fee will be prorated based on the date of permanent closure.
6. UNREGISTERED USTs use Form UST-2B
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity) Facility Name or Company Street Address Facility ID # (If known) City County Street Address State Zip Code City County Zip Code Phone Number Phone Number
III. CONTACT PERSONNEL Contact for Facility: Job Title: Phone #:
Closure Contractor Name: Closure Contractor Company: Address: Phone #
Primary Consultant Name: Primary Consultant Company: Address: Phone #
IV. UST INFORMATION FOR REGISTERED UST SYSTEMS UNREGISTERED USTs use Form UST-2B V. EXCAVATION CONDITION
Tank ID No. Size in Gallons Last Contents Last Use Date
Permanent Close Date Method of Permanent Closure: Indicate REMOVED or enter fill material, such as foam/ concrete/ sand
Change-in-Service Date Water in excavation Free product
Notable odor or visible soil contamination Yes No Yes No Yes No

VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate and complete.
Print name and official title of owner or owner’s authorized representative
Signature Date Signed
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION 1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/ 1/2016
Ryder Truck Rental, Inc.
16155 Park Row #140
Houston
TX 77084
281-647-8900
Ryder Transportation Serv 0134
00-0-0000010418
217 Atwell Ave
Greensboro 27406Guilford
281-647-8900
Sarah Galloway Ryder Project Engineer
864-314-7008
Kent Reed Southern Pump & Tank Company 5518-J David Cox Road,704-400-2739
Britney Barnes Civil & Environmental Consultants, Inc.530 Howell Rd. Suite 203 864-350-3522
1,2,3 & 4 12,000 diesel 3/14/20 3/17/20 removed n/a ■■■
5 6,000 motor oil 3/14/20 3/17/20 n/a ■■■
6 1,000 used oil 2/17/20 3/20/20 n/a ■■■
removed
removed
Sarah Galloway, Ryder Environmental Project Engineer
6/1/20
UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases
in NC
This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
suspected release
(DWM USE ONLY)
Incident # ________ Risk (H,I,L,U)_______
Received On ________ Received By ________
Reported by (circle one): Phone, Fax or Report
Region _______
Suspected Contamination? (Y/N) ________
Confirmed GW Contamination? (Y/N) ______
Confirmed Soil Contamination ?(Y/N) ______
Samples Taken?(Y/N) ______
Free Product? (Y/N) _____ If Yes, State Greatest
Thickness ______________
Facility ID Number ______________
Date Leak Discovered ___________
Comm/Non-Commercial? ________
Reg/Non-regulated? _____________
INCIDENT DESCRIPTION
Incident Name:
Address:County:
City/Town: Zip Code:
Regional Office (circle one): Asheville, Mooresville, Fayetteville,
Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) :Obtained by:
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)T GPS
T Topographic map
T GIS Address matching
T Other
T Unknown
Describe location:
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
T Release Detection Equipment or Methods
T During UST Closure/Removal
T Property Transfer
T Visual/Odor
T Water in Tank
T Water Supply Well Contamination
T Groundwater Contamination
T Surface Water Contamination
T Other (specify) _______________
SOURCE OF CONTAMINATION
Source of Release
(Check one to indicate primary
source)
Cause of Release
(Check one to indicate primary
cause)
Type of Release
(Check one)
Product Type Released
(Check one to indicate primary product type
released)
TTank
TPiping
TDispenser
TSubmersible Turbine Pump
TDelivery Problem
TOther
TUnknown
Definitions presented on reverse
TSpill
TOverfill
TCorrosion
TPhysical or Mechanical
Damage
TInstall Problem
TOther
TUnknown
Definitions presented on reverse
TPetroleum
TNon-Petroleum
TBoth
Location
(Check one)
T Facility
T Residence
T Other
T Gasoline/ Diesel/
Kerosene
T Heating Oil
T Other Petroleum
Products
T Metals
T Other Inorganics
T Other Organics
T Diesel/Veg. Oil
Blend
T Vegetable Oil 100%
T E10 – E20
T E21 – E84
T E85 – E99
T Ethanol 100%
T E01 – E09
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/08)Page 1 of 2
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36 01'50.13 N 79 47'13.83'W
X X
X
X
X
Private
Commercial
TT Unknown
Unknown
Petroleum
Other Petroleum
Products
Visual/Odor
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown
Number of Water Supply Wells Affected __________________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
UST SYSTEM OWNER
UST Owner/Company
Point of Contact Address
City State Zip Code Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company Address
City State Zip Code Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner Address
City State Zip Code Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/08)Page 2 of 2
Definitions of Sources
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser:includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage:use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion:use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined
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REFERENCE
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
SITE AERIAL MAP
190-9131"= 300'FEBRUARY 2020
SHP BCB BCB 1
RYDER TRUCK RENTAL
217 ATWELL AVENUE
GREENSBORO, NORTH CAROLINA 27406
GUILFORD COUNTY530 Howell Road · Suite 203 · Greenville, SC 29615
Ph: 864.626.3140 · 855.574.4331 · Fax: [phone]
www.cecinc.com
NORTH
REFERENCE
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
SITE LAYOUT MAP
190-9131"= 100'FEBRUARY 2020
SHP BCB BCB 2
RYDER TRUCK RENTAL
217 ATWELL AVENUE
GREENSBORO, NORTH CAROLINA 27406
GUILFORD COUNTY530 Howell Road · Suite 203 · Greenville, SC 29615
Ph: 864.626.3140 · 855.574.4331 · Fax: [phone]
www.cecinc.com
NORTH

APPENDIX C

NON-HAZARDOUS WASTE MANIFEST & DISPOSAL
DOCUMENTATION

Great Oaks Landfill Reprint
3565 Old Cedar Falls Rd Ticket# 121001
Randleman, NC, 27317 Ph: [phone]
Customer Name RYDERTRUCK RYDER TRUCK RENTAL Carrier RYDERTRUCK
Ticket Date 04/14/2020 Vehicle# BG7 Volume
Payment Type Credit Account Container
Manual Ticket# Driver BOB GRIMM
Route Check#
Hauling Ticket# Billing# 0000301
Destination Manifest SOIL
PO# LC 0134
Time Scale Operator Gross 57160 lb
In 04/14/2020 14:41:12 Scale 1 lsmithm Tare 23680 lb
Out 04/14/2020 14:59:13 Scale 2 lthomp15 Net 33480 lb
Tons 16.74
Comments 217 ATWELL AVENUE GREENSBORO
Product LD% Qty UOM Rate Fee Amount Origin
--------------------------------------------------------------------------------------------
1 ContSoilPet-RGC-Tons-Con 100 16.74 Tons GUI
Total Fee
Total Ticket
Driver`s Signature
Great Oaks Landfill Reprint
3565 Old Cedar Falls Rd Ticket# 121068
Randleman, NC, 27317 Ph: [phone]
Customer Name RYDERTRUCK RYDER TRUCK RENTAL Carrier RYDERTRUCK
Ticket Date 04/15/2020 Vehicle# HDG-1 Volume
Payment Type Credit Account Container
Manual Ticket# Driver TIMOTHY HODGIN
Route Check#
Hauling Ticket# Billing# 0000301
Destination Manifest SOIL
PO# LC 0134
Time Scale Operator Gross 51660 lb
In 04/15/2020 08:46:16 Scale 1 lsmithm Tare 25100 lb
Out 04/15/2020 09:01:17 Scale 2 lthomp15 Net 26560 lb
Tons 13.28
Comments RYDER FUEL SERVICES 217 ATWELL AVE
Product LD% Qty UOM Rate Fee Amount Origin
--------------------------------------------------------------------------------------------
1 ContSoilPet-RGC-Tons-Con 100 13.28 Tons GUI
Total Fee
Total Ticket
Driver`s Signature
Great Oaks Landfill Reprint
3565 Old Cedar Falls Rd Ticket# 121069
Randleman, NC, 27317 Ph: [phone]
Customer Name RYDERTRUCK RYDER TRUCK RENTAL Carrier RYDERTRUCK
Ticket Date 04/15/2020 Vehicle# BG 7 Volume
Payment Type Credit Account Container
Manual Ticket# Driver BOB GRIMM
Route Check#
Hauling Ticket# Billing# 0000301
Destination Manifest SOIL
PO# LC 0134
Time Scale Operator Gross 53660 lb
In 04/15/2020 08:48:21 Scale 1 lsmithm Tare 23740 lb
Out 04/15/2020 09:03:29 Scale 2 lthomp15 Net 29920 lb
Tons 14.96
Comments RYDER FUEL SERVICES 217 ATWELL AVE
Product LD% Qty UOM Rate Fee Amount Origin
--------------------------------------------------------------------------------------------
1 ContSoilPet-RGC-Tons-Con 100 14.96 Tons GUI
Total Fee
Total Ticket
Driver`s Signature
Great Oaks Landfill Reprint
3565 Old Cedar Falls Rd Ticket# 121111
Randleman, NC, 27317 Ph: [phone]
Customer Name RYDERTRUCK RYDER TRUCK RENTAL Carrier RYDERTRUCK
Ticket Date 04/15/2020 Vehicle# HDG-1 Volume
Payment Type Credit Account Container
Manual Ticket# Driver TIMOTHY HODGIN
Route Check#
Hauling Ticket# Billing# 0000301
Destination Manifest SOIL
PO# LC 0134
Time Scale Operator Gross 50480 lb
In 04/15/2020 10:58:33 Scale 1 lsmithm Tare 25040 lb
Out 04/15/2020 11:14:04 Scale 2 lthomp15 Net 25440 lb
Tons 12.72
Comments 217 ATWELL AVE
Product LD% Qty UOM Rate Fee Amount Origin
--------------------------------------------------------------------------------------------
1 ContSoilPet-RGC-Tons-Con 100 12.72 Tons GUI
Total Fee
Total Ticket
Driver`s Signature
Great Oaks Landfill Reprint
3565 Old Cedar Falls Rd Ticket# 121112
Randleman, NC, 27317 Ph: [phone]
Customer Name RYDERTRUCK RYDER TRUCK RENTAL Carrier RYDERTRUCK
Ticket Date 04/15/2020 Vehicle# BG 7 Volume
Payment Type Credit Account Container
Manual Ticket# Driver BOB GRIMM
Route Check#
Hauling Ticket# Billing# 0000301
Destination Manifest SOIL
PO# LC 0134
Time Scale Operator Gross 55080 lb
In 04/15/2020 11:00:07 Scale 1 lsmithm Tare 23660 lb
Out 04/15/2020 11:16:06 Scale 2 lthomp15 Net 31420 lb
Tons 15.71
Comments 217 ATWELL AVE
Product LD% Qty UOM Rate Fee Amount Origin
--------------------------------------------------------------------------------------------
1 ContSoilPet-RGC-Tons-Con 100 15.71 Tons GUI
Total Fee
Total Ticket
Driver`s Signature
Great Oaks Landfill Reprint
3565 Old Cedar Falls Rd Ticket# 121167
Randleman, NC, 27317 Ph: [phone]
Customer Name RYDERTRUCK RYDER TRUCK RENTAL Carrier RYDERTRUCK
Ticket Date 04/15/2020 Vehicle# HDG-1 Volume
Payment Type Credit Account Container
Manual Ticket# Driver TIMOTHY HODGIN
Route Check#
Hauling Ticket# Billing# 0000301
Destination Manifest SOIL
PO# LC 0134
Time Scale Operator Gross 57380 lb
In 04/15/2020 14:20:43 Scale 1 lsmithm Tare 24960 lb
Out 04/15/2020 14:36:11 Scale 2 lthomp15 Net 32420 lb
Tons 16.21
Comments 217 ATWELL AVE
Product LD% Qty UOM Rate Fee Amount Origin
--------------------------------------------------------------------------------------------
1 ContSoilPet-RGC-Tons-Con 100 16.21 Tons GUI
Total Fee
Total Ticket
Driver`s Signature
Great Oaks Landfill Reprint
3565 Old Cedar Falls Rd Ticket# 121168
Randleman, NC, 27317 Ph: [phone]
Customer Name RYDERTRUCK RYDER TRUCK RENTAL Carrier RYDERTRUCK
Ticket Date 04/15/2020 Vehicle# BG 7 Volume
Payment Type Credit Account Container
Manual Ticket# Driver BOB GRIMM
Route Check#
Hauling Ticket# Billing# 0000301
Destination Manifest SOIL
PO# LC 0134
Time Scale Operator Gross 55540 lb
In 04/15/2020 14:22:59 Scale 1 lsmithm Tare 23600 lb
Out 04/15/2020 14:38:20 Scale 2 lthomp15 Net 31940 lb
Tons 15.97
Comments 217 ATWELL AVE
Product LD% Qty UOM Rate Fee Amount Origin
--------------------------------------------------------------------------------------------
1 ContSoilPet-RGC-Tons-Con 100 15.97 Tons GUI
Total Fee
Total Ticket
Driver`s Signature
Great Oaks Landfill Reprint
3565 Old Cedar Falls Rd Ticket# 121192
Randleman, NC, 27317 Ph: [phone]
Customer Name RYDERTRUCK RYDER TRUCK RENTAL Carrier RYDERTRUCK
Ticket Date 04/15/2020 Vehicle# HDG-1 Volume
Payment Type Credit Account Container
Manual Ticket# Driver TIMOTHY HODGIN
Route Check#
Hauling Ticket# Billing# 0000301
Destination Manifest SOIL
PO# LC 0134
Time Scale Operator Gross 51680 lb
In 04/15/2020 16:52:01 Scale 1 lthomp15 Tare 24900 lb
Out 04/15/2020 17:01:21 Scale 2 lthomp15 Net 26780 lb
Tons 13.39
Comments ATWELL AVENUE
Product LD% Qty UOM Rate Fee Amount Origin
--------------------------------------------------------------------------------------------
1 ContSoilPet-RGC-Tons-Con 100 13.39 Tons GUI
Total Fee
Total Ticket
Driver`s Signature
Great Oaks Landfill Reprint
3565 Old Cedar Falls Rd Ticket# 121193
Randleman, NC, 27317 Ph: [phone]
Customer Name RYDERTRUCK RYDER TRUCK RENTAL Carrier RYDERTRUCK
Ticket Date 04/15/2020 Vehicle# BG 7 Volume
Payment Type Credit Account Container
Manual Ticket# Driver BOB GRIMM
Route Check#
Hauling Ticket# Billing# 0000301
Destination Manifest SOIL
PO# LC 0134
Time Scale Operator Gross 43700 lb
In 04/15/2020 16:53:49 Scale 1 lthomp15 Tare 23540 lb
Out 04/15/2020 17:04:09 Scale 2 lthomp15 Net 20160 lb
Tons 10.08
Comments ATWELL AVENUE
Product LD% Qty UOM Rate Fee Amount Origin
--------------------------------------------------------------------------------------------
1 ContSoilPet-RGC-Tons-Con 100 10.08 Tons GUI
Total Fee
Total Ticket
Driver`s Signature
2111A Bishop Road. Greensboro, NC 27406
PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.
Hazmat Emergency Response & Remediation303 S. Maultsby Street INBOUND
INVOICE
01
March 19, 2020
11:43 am
March 19, 2020
11:43 am
Audrey Otero192774
SITE TICKET WEIGHMASTER
35000 24960 10040
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
CONTRACT:Landfill Inbound
lbs Tare Outlbs Scale In
lbs
LICENCECONT.TRUCKOUTIN
SQ-20
Reference: Origin:
Guilford County
5.02 tn Construction & Demolition Waste
1.00 Environmental Fee
$0.00 Change:
2111A Bishop Road. Greensboro, NC 27406PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.Hazmat Emergency Response & Remediation
303 S. Maultsby Street INBOUND
INVOICE
01
March 19, 2020
12:38 pm
March 19, 2020
12:38 pm
Audrey Otero192785
SITE TICKET WEIGHMASTER
48840 30700 18140
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
CONTRACT:Landfill Inbound
lbs Tare Out
lbs Scale In
lbs
LICENCECONT.TRUCKOUTIN
TC-104
Reference: Origin:
Guilford County
9.07 tn Construction & Demolition Waste
1.00 Environmental Fee
$0.00 Change:
2111A Bishop Road. Greensboro, NC 27406
PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.
Hazmat Emergency Response & Remediation303 S. Maultsby Street INBOUND
INVOICE
01
March 19, 2020
12:50 pm
March 19, 2020
12:50 pm
Audrey Otero192786
SITE TICKET WEIGHMASTER
41720 26900 14820
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
Landfill Inbound
SQ-10
Reference: Origin:
Guilford County
7.41 tn Construction & Demolition Waste
1.00 Environmental Fee
$0.00 Change:
2111A Bishop Road. Greensboro, NC 27406PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.Hazmat Emergency Response & Remediation
303 S. Maultsby Street INBOUND
INVOICE
01
March 19, 2020
1:19 pm
March 19, 2020
1:19 pm
Audrey Otero192788
SITE TICKET WEIGHMASTER
32600 24960 7640
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
Landfill Inbound
SQ-20
Reference: Origin:
Guilford County
3.82 tn Construction & Demolition Waste
1.00 Environmental Fee
$0.00 Change:
2111A Bishop Road. Greensboro, NC 27406
PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.
Hazmat Emergency Response & Remediation303 S. Maultsby Street INBOUND
INVOICE
01
March 19, 2020
2:01 pm
March 19, 2020
2:01 pm
Audrey Otero192801
SITE TICKET WEIGHMASTER
67180 30700 36480
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
Landfill Inbound
TC-104
Reference: Origin:
Guilford County
18.24 tn Construction & Demolition Waste
1.00 Environmental Fee
$0.00 Change:
2111A Bishop Road. Greensboro, NC 27406PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.Hazmat Emergency Response & Remediation
303 S. Maultsby Street INBOUND
INVOICE
01
March 20, 2020
8:43 am
March 20, 2020
8:43 am
Audrey Otero192833
SITE TICKET WEIGHMASTER
58420 30700 27720
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
Landfill Inbound
TC-104
Reference: Origin:
Guilford County
13.86 tn Clean Concrete
1.00 Environmental Fee
$0.00 Change:
2111A Bishop Road. Greensboro, NC 27406
PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.
Hazmat Emergency Response & Remediation303 S. Maultsby Street INBOUND
INVOICE
01
March 20, 2020
10:54 am
March 20, 2020
10:54 am
Audrey Otero192854
SITE TICKET WEIGHMASTER
58620 30700 27920
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
Landfill Inbound
TC-104
Reference: Origin:
Guilford County
13.96 tn Clean Concrete
1.00 Environmental Fee
$0.00 Change:
2111A Bishop Road. Greensboro, NC 27406PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.Hazmat Emergency Response & Remediation
303 S. Maultsby Street INBOUND
INVOICE
01
March 20, 2020
11:53 am
March 20, 2020
11:53 am
Audrey Otero192868
SITE TICKET WEIGHMASTER
75120 30700 44420
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
Landfill Inbound
TC-104
Reference: Origin:
Guilford County
1.00 ea Fill Dirt - In
1.00 Environmental Fee
$0.00 Change:
2111A Bishop Road. Greensboro, NC 27406
PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.
Hazmat Emergency Response & Remediation303 S. Maultsby Street INBOUND
INVOICE
01
March 20, 2020
1:11 pm
March 20, 2020
1:11 pm
Audrey Otero192882
SITE TICKET WEIGHMASTER
80440 30700 49740
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
Landfill Inbound
TC-104
Reference: Origin:
Guilford County
1.00 ea Fill Dirt - In
1.00 Environmental Fee
$0.00 Change:
2111A Bishop Road. Greensboro, NC 27406PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.Hazmat Emergency Response & Remediation
303 S. Maultsby Street INBOUND
INVOICE
01
March 20, 2020
1:29 pm
March 20, 2020
1:29 pm
Audrey Otero192886
SITE TICKET WEIGHMASTER
29220 24960 4260
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
Landfill Inbound
SQ-20
Reference: Origin:
Guilford County
2.13 tn Construction & Demolition Waste
1.00 Environmental Fee
$0.00 Change:
2111A Bishop Road. Greensboro, NC 27406
PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.
Hazmat Emergency Response & Remediation303 S. Maultsby Street INBOUND
INVOICE
01
March 20, 2020
2:26 pm
March 20, 2020
2:26 pm
Audrey Otero192898
SITE TICKET WEIGHMASTER
64920 30700 34220
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
Landfill Inbound
TC-104
Reference: Origin:
Guilford County
17.11 tn Clean Concrete
1.00 Environmental Fee
$0.00 Change:
2111A Bishop Road. Greensboro, NC 27406PHONE: [phone] www.a1sandrockinc.com
001433 - HERR INC.Hazmat Emergency Response & Remediation
303 S. Maultsby Street INBOUND
INVOICE
01
March 20, 2020
3:26 pm
March 20, 2020
3:26 pm
Audrey Otero192905
SITE TICKET WEIGHMASTER
67740 30700 37040
GROSSTARENET
REPRINT
TotalTaxRateDescriptionUnitQtySubtotal
Landfill Inbound
TC-104
Reference: Origin:
Guilford County
18.52 tn Clean Concrete
1.00 Environmental Fee
$0.00 Change:
Soil Disposal - Ryder contracted directly with Waste Management

APPENDIX D

LABORATORY ANALTYICAL DATA SHEETS

#=CL#
May 04, 2020
LIMS USE: FR - BRITNEY BARNES
LIMS OBJECT ID: 92474993
92474993
Project:
Pace Project No.:
RE:
Britney Barnes
Civil & Environmental Consultants
530 Howell Rd
Suite 203
Greenville, SC
Greensboro NC LC 0134 UST Clos
Dear Britney Barnes:
Enclosed are the analytical results for sample(s) received by the laboratory on April 24, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Sarah Galloway, Ryder Systems, Inc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 31
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Lab ID Sample ID Matrix Date Collected Date Received
92474993001 MW-1 Water 04/23/20 00:00 04/24/20 09:54
92474993002 MW-2 Water 04/23/20 00:00 04/24/20 09:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92474993001 MW-1 MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 6010D 2 PANCCE
EPA 625.1 66 PASI-CPKS
SM 6200B 63 PASI-CSAS
92474993002 MW-2 MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 6010D 2 PANCCE
EPA 625.1 60 PASI-CPKS
SM 6200B 16 PASI-CSAS
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-1 Lab ID:92474993001 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)216 ug/L 05/04/20 13:41 L2,N205/01/20 13:431001001
Aliphatic (C19-C36)ND ug/L 05/04/20 13:41 L2,N205/01/20 13:431001001
Aromatic (C11-C22)270 ug/L 05/04/20 13:41 N205/01/20 13:431001001
Surrogates
Nonatriacontane (S)23 %05/04/20 13:41 7194-86-7 P2,S205/01/20 13:4340-140 1
o-Terphenyl (S)40 %05/04/20 13:41 84-15-105/01/20 13:4340-140 1
2-Fluorobiphenyl (S)94 %05/04/20 13:41 321-60-805/01/20 13:4340-140 1
2-Bromonaphthalene (S)94 %05/04/20 13:41 580-13-205/01/20 13:4340-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)84.8J ug/L 04/26/20 15:52 J04/26/20 15:5210033.3 1
Aliphatic (C09-C12)82.0J ug/L 04/26/20 15:52 J04/26/20 15:5210033.3 1
Aromatic (C09-C10),Unadjusted 133 ug/L 04/26/20 15:52 TPHC9C10A04/26/20 15:5210033.3 1
Surrogates
2,5-Dibromotoluene (FID)125 %04/26/20 15:52 615-59-8FID04/26/20 15:5270.0-130 1
2,5-Dibromotoluene (PID)98.0 %04/26/20 15:52 615-59-8PID04/26/20 15:5270.0-130 1
Analytical Method: EPA 6010D Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICP) 6010D
Chromium ND ug/L 05/03/20 18:42 7440-47-305/01/20 11:0810.0 5.00 1
Lead ND ug/L 05/03/20 18:42 7439-92-105/01/20 11:086.00 2.95 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 04/30/20 20:55 83-32-904/24/20 17:015.0 1.4 1
Acenaphthylene ND ug/L 04/30/20 20:55 208-96-804/24/20 17:015.0 1.5 1
Anthracene ND ug/L 04/30/20 20:55 120-12-704/24/20 17:015.0 1.6 1
Benzo(a)anthracene ND ug/L 04/30/20 20:55 56-55-304/24/20 17:015.0 1.5 1
Benzo(a)pyrene ND ug/L 04/30/20 20:55 50-32-804/24/20 17:015.0 1.8 1
Benzo(b)fluoranthene ND ug/L 04/30/20 20:55 205-99-204/24/20 17:015.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 04/30/20 20:55 191-24-204/24/20 17:015.0 1.6 1
Benzo(k)fluoranthene ND ug/L 04/30/20 20:55 207-08-904/24/20 17:015.0 1.5 1
4-Bromophenylphenyl ether ND ug/L 04/30/20 20:55 101-55-304/24/20 17:015.0 1.2 1
Butylbenzylphthalate ND ug/L 04/30/20 20:55 85-68-704/24/20 17:015.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 04/30/20 20:55 59-50-704/24/20 17:015.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 04/30/20 20:55 111-91-104/24/20 17:0110.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 04/30/20 20:55 111-44-404/24/20 17:015.0 1.7 1
2-Chloronaphthalene ND ug/L 04/30/20 20:55 91-58-7 L204/24/20 17:015.0 1.4 1
2-Chlorophenol ND ug/L 04/30/20 20:55 95-57-804/24/20 17:015.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 04/30/20 20:55 7005-72-304/24/20 17:015.0 1.5 1
Chrysene ND ug/L 04/30/20 20:55 218-01-904/24/20 17:015.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 04/30/20 20:55 53-70-304/24/20 17:015.0 1.6 1
3,3'-Dichlorobenzidine ND ug/L 04/30/20 20:55 91-94-104/24/20 17:0110.0 2.7 1
2,4-Dichlorophenol ND ug/L 04/30/20 20:55 120-83-204/24/20 17:015.0 1.5 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-1 Lab ID:92474993001 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Diethylphthalate ND ug/L 04/30/20 20:55 84-66-204/24/20 17:015.0 1.6 1
2,4-Dimethylphenol ND ug/L 04/30/20 20:55 105-67-904/24/20 17:0110.0 1.5 1
Dimethylphthalate ND ug/L 04/30/20 20:55 131-11-304/24/20 17:015.0 1.4 1
Di-n-butylphthalate ND ug/L 04/30/20 20:55 84-74-204/24/20 17:015.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 04/30/20 20:55 534-52-104/24/20 17:0110.0 4.5 1
2,4-Dinitrophenol ND ug/L 04/30/20 20:55 51-28-504/24/20 17:0150.0 7.3 1
2,4-Dinitrotoluene ND ug/L 04/30/20 20:55 121-14-204/24/20 17:015.0 1.7 1
2,6-Dinitrotoluene ND ug/L 04/30/20 20:55 606-20-204/24/20 17:015.0 1.7 1
Di-n-octylphthalate ND ug/L 04/30/20 20:55 117-84-004/24/20 17:015.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/30/20 20:55 117-81-704/24/20 17:015.0 2.0 1
Fluoranthene ND ug/L 04/30/20 20:55 206-44-004/24/20 17:015.0 1.6 1
Fluorene 1.9J ug/L 04/30/20 20:55 86-73-704/24/20 17:015.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 04/30/20 20:55 87-68-304/24/20 17:015.0 1.6 1
Hexachlorobenzene ND ug/L 04/30/20 20:55 118-74-104/24/20 17:015.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 04/30/20 20:55 77-47-404/24/20 17:0110.0 2.4 1
Hexachloroethane ND ug/L 04/30/20 20:55 67-72-104/24/20 17:015.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/30/20 20:55 193-39-504/24/20 17:015.0 1.7 1
Isophorone ND ug/L 04/30/20 20:55 78-59-104/24/20 17:0110.0 1.3 1
Naphthalene ND ug/L 04/30/20 20:55 91-20-304/24/20 17:015.0 1.6 1
Nitrobenzene ND ug/L 04/30/20 20:55 98-95-304/24/20 17:015.0 1.5 1
2-Nitrophenol ND ug/L 04/30/20 20:55 88-75-504/24/20 17:015.0 1.7 1
4-Nitrophenol ND ug/L 04/30/20 20:55 100-02-704/24/20 17:0110.0 9.4 1
N-Nitrosodimethylamine ND ug/L 04/30/20 20:55 62-75-904/24/20 17:015.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 04/30/20 20:55 621-64-704/24/20 17:015.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 04/30/20 20:55 86-30-604/24/20 17:0110.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/30/20 20:55 108-60-104/24/20 17:015.0 1.3 1
Pentachlorophenol ND ug/L 04/30/20 20:55 87-86-504/24/20 17:0110.0 2.8 1
Phenanthrene ND ug/L 04/30/20 20:55 85-01-804/24/20 17:015.0 1.4 1
Phenol ND ug/L 04/30/20 20:55 108-95-204/24/20 17:015.0 1.5 1
Pyrene ND ug/L 04/30/20 20:55 129-00-004/24/20 17:015.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 04/30/20 20:55 120-82-104/24/20 17:015.0 1.6 1
2,4,6-Trichlorophenol ND ug/L 04/30/20 20:55 88-06-204/24/20 17:0110.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)68 %04/30/20 20:55 4165-60-004/24/20 17:0110-120 1
2-Fluorobiphenyl (S)57 %04/30/20 20:55 321-60-804/24/20 17:0115-120 1
Terphenyl-d14 (S)113 %04/30/20 20:55 1718-51-004/24/20 17:0111-131 1
Phenol-d6 (S)34 %04/30/20 20:55 13127-88-304/24/20 17:0110-120 1
2-Fluorophenol (S)29 %04/30/20 20:55 367-12-404/24/20 17:0110-120 1
2,4,6-Tribromophenol (S)54 %04/30/20 20:55 118-79-604/24/20 17:0110-137 1
Tentatively Identified Compounds
1H-Indene, 2,3-dihydro-5 9.8J ug/L 04/30/20 20:55 874-35-1 N04/24/20 17:011
Naphthalene, 1,2,3,4-tet 6.1J ug/L 04/30/20 20:55 3877-19-8 N04/24/20 17:011
Naphthalene, 1,2,3,4-tet 12.3J ug/L 04/30/20 20:55 2809-64-5 N04/24/20 17:011
Naphthalene, 1,2,3,4-tet 9.0J ug/L 04/30/20 20:55 1680-51-9 N04/24/20 17:011
Naphthalene, 2,6-dimethy 5.6J ug/L 04/30/20 20:55 581-42-0 N04/24/20 17:011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-1 Lab ID:92474993001 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Tentatively Identified Compounds
Naphthalene, 1,6-dimethy 6.3J ug/L 04/30/20 20:55 575-43-9 N04/24/20 17:011
Unknown 12.8J ug/L 04/30/20 20:5504/24/20 17:011
n-Hexadecanoic acid 31.2J ug/L 04/30/20 20:55 57-10-3 N04/24/20 17:011
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/30/20 16:17 71-43-20.50 0.24 1
Bromobenzene ND ug/L 04/30/20 16:17 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 04/30/20 16:17 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 04/30/20 16:17 75-27-40.50 0.18 1
Bromoform ND ug/L 04/30/20 16:17 75-25-20.50 0.40 1
Bromomethane ND ug/L 04/30/20 16:17 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 04/30/20 16:17 104-51-80.50 0.35 1
sec-Butylbenzene 1.6 ug/L 04/30/20 16:17 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 04/30/20 16:17 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 04/30/20 16:17 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 04/30/20 16:17 108-90-70.50 0.22 1
Chloroethane ND ug/L 04/30/20 16:17 75-00-31.0 0.58 1
Chloroform ND ug/L 04/30/20 16:17 67-66-30.50 0.35 1
Chloromethane ND ug/L 04/30/20 16:17 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 04/30/20 16:17 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 04/30/20 16:17 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 04/30/20 16:17 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 04/30/20 16:17 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 04/30/20 16:17 106-93-40.50 0.23 1
Dibromomethane ND ug/L 04/30/20 16:17 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 04/30/20 16:17 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 04/30/20 16:17 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 04/30/20 16:17 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 04/30/20 16:17 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 04/30/20 16:17 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 04/30/20 16:17 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 04/30/20 16:17 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 04/30/20 16:17 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 04/30/20 16:17 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 04/30/20 16:17 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 04/30/20 16:17 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 04/30/20 16:17 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 04/30/20 16:17 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 04/30/20 16:17 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/30/20 16:17 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 04/30/20 16:17 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 04/30/20 16:17 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 04/30/20 16:17 87-68-32.0 1.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-1 Lab ID:92474993001 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Isopropylbenzene (Cumene)ND ug/L 04/30/20 16:17 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 04/30/20 16:17 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 04/30/20 16:17 1634-04-40.50 0.44 1
Naphthalene ND ug/L 04/30/20 16:17 91-20-32.0 0.66 1
n-Propylbenzene 0.47J ug/L 04/30/20 16:17 103-65-10.50 0.24 1
Styrene ND ug/L 04/30/20 16:17 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/30/20 16:17 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane ND ug/L 04/30/20 16:17 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 04/30/20 16:17 127-18-40.50 0.23 1
Toluene ND ug/L 04/30/20 16:17 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 04/30/20 16:17 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 04/30/20 16:17 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 04/30/20 16:17 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 04/30/20 16:17 79-00-50.50 0.23 1
Trichloroethene ND ug/L 04/30/20 16:17 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 04/30/20 16:17 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 04/30/20 16:17 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 04/30/20 16:17 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 04/30/20 16:17 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 04/30/20 16:17 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 04/30/20 16:17 179601-23-11.0 0.44 1
o-Xylene ND ug/L 04/30/20 16:17 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %04/30/20 16:17 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %04/30/20 16:17 460-00-470-130 1
Toluene-d8 (S)101 %04/30/20 16:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-2 Lab ID:92474993002 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 05/04/20 14:08 L2,N205/01/20 13:4396.2 96.2 1
Aliphatic (C19-C36)ND ug/L 05/04/20 14:08 L2,N205/01/20 13:4396.2 96.2 1
Aromatic (C11-C22)ND ug/L 05/04/20 14:08 N205/01/20 13:4396.2 96.2 1
Surrogates
Nonatriacontane (S)56 %05/04/20 14:08 7194-86-7 P205/01/20 13:4340-140 1
o-Terphenyl (S)70 %05/04/20 14:08 84-15-105/01/20 13:4340-140 1
2-Fluorobiphenyl (S)98 %05/04/20 14:08 321-60-805/01/20 13:4340-140 1
2-Bromonaphthalene (S)97 %05/04/20 14:08 580-13-205/01/20 13:4340-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)44.8J ug/L 04/26/20 16:25 J04/26/20 16:2510033.3 1
Aliphatic (C09-C12)37.3J ug/L 04/26/20 16:25 J04/26/20 16:2510033.3 1
Aromatic (C09-C10),Unadjusted ND ug/L 04/26/20 16:25 TPHC9C10A04/26/20 16:2510033.3 1
Surrogates
2,5-Dibromotoluene (FID)93.1 %04/26/20 16:25 615-59-8FID04/26/20 16:2570.0-130 1
2,5-Dibromotoluene (PID)85.5 %04/26/20 16:25 615-59-8PID04/26/20 16:2570.0-130 1
Analytical Method: EPA 6010D Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICP) 6010D
Chromium 89.1 ug/L 05/03/20 18:45 7440-47-305/01/20 11:0810.0 5.00 1
Lead 20.0 ug/L 05/03/20 18:45 7439-92-105/01/20 11:086.00 2.95 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 04/30/20 21:20 83-32-904/24/20 17:015.0 1.4 1
Acenaphthylene ND ug/L 04/30/20 21:20 208-96-804/24/20 17:015.0 1.5 1
Anthracene ND ug/L 04/30/20 21:20 120-12-704/24/20 17:015.0 1.6 1
Benzo(a)anthracene ND ug/L 04/30/20 21:20 56-55-304/24/20 17:015.0 1.5 1
Benzo(a)pyrene ND ug/L 04/30/20 21:20 50-32-804/24/20 17:015.0 1.8 1
Benzo(b)fluoranthene ND ug/L 04/30/20 21:20 205-99-204/24/20 17:015.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 04/30/20 21:20 191-24-204/24/20 17:015.0 1.6 1
Benzo(k)fluoranthene ND ug/L 04/30/20 21:20 207-08-904/24/20 17:015.0 1.5 1
4-Bromophenylphenyl ether ND ug/L 04/30/20 21:20 101-55-304/24/20 17:015.0 1.2 1
Butylbenzylphthalate ND ug/L 04/30/20 21:20 85-68-704/24/20 17:015.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 04/30/20 21:20 59-50-704/24/20 17:015.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 04/30/20 21:20 111-91-104/24/20 17:0110.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 04/30/20 21:20 111-44-404/24/20 17:015.0 1.7 1
2-Chloronaphthalene ND ug/L 04/30/20 21:20 91-58-7 L204/24/20 17:015.0 1.4 1
2-Chlorophenol ND ug/L 04/30/20 21:20 95-57-804/24/20 17:015.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 04/30/20 21:20 7005-72-304/24/20 17:015.0 1.5 1
Chrysene ND ug/L 04/30/20 21:20 218-01-904/24/20 17:015.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 04/30/20 21:20 53-70-304/24/20 17:015.0 1.6 1
3,3'-Dichlorobenzidine ND ug/L 04/30/20 21:20 91-94-104/24/20 17:0110.0 2.7 1
2,4-Dichlorophenol ND ug/L 04/30/20 21:20 120-83-204/24/20 17:015.0 1.5 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-2 Lab ID:92474993002 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Diethylphthalate ND ug/L 04/30/20 21:20 84-66-204/24/20 17:015.0 1.6 1
2,4-Dimethylphenol ND ug/L 04/30/20 21:20 105-67-904/24/20 17:0110.0 1.5 1
Dimethylphthalate ND ug/L 04/30/20 21:20 131-11-304/24/20 17:015.0 1.4 1
Di-n-butylphthalate ND ug/L 04/30/20 21:20 84-74-204/24/20 17:015.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 04/30/20 21:20 534-52-104/24/20 17:0110.0 4.5 1
2,4-Dinitrophenol ND ug/L 04/30/20 21:20 51-28-504/24/20 17:0150.0 7.3 1
2,4-Dinitrotoluene ND ug/L 04/30/20 21:20 121-14-204/24/20 17:015.0 1.7 1
2,6-Dinitrotoluene ND ug/L 04/30/20 21:20 606-20-204/24/20 17:015.0 1.7 1
Di-n-octylphthalate ND ug/L 04/30/20 21:20 117-84-004/24/20 17:015.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/30/20 21:20 117-81-704/24/20 17:015.0 2.0 1
Fluoranthene ND ug/L 04/30/20 21:20 206-44-004/24/20 17:015.0 1.6 1
Fluorene ND ug/L 04/30/20 21:20 86-73-704/24/20 17:015.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 04/30/20 21:20 87-68-304/24/20 17:015.0 1.6 1
Hexachlorobenzene ND ug/L 04/30/20 21:20 118-74-104/24/20 17:015.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 04/30/20 21:20 77-47-404/24/20 17:0110.0 2.4 1
Hexachloroethane ND ug/L 04/30/20 21:20 67-72-104/24/20 17:015.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/30/20 21:20 193-39-504/24/20 17:015.0 1.7 1
Isophorone ND ug/L 04/30/20 21:20 78-59-104/24/20 17:0110.0 1.3 1
Naphthalene ND ug/L 04/30/20 21:20 91-20-304/24/20 17:015.0 1.6 1
Nitrobenzene ND ug/L 04/30/20 21:20 98-95-304/24/20 17:015.0 1.5 1
2-Nitrophenol ND ug/L 04/30/20 21:20 88-75-504/24/20 17:015.0 1.7 1
4-Nitrophenol ND ug/L 04/30/20 21:20 100-02-704/24/20 17:0110.0 9.4 1
N-Nitrosodimethylamine ND ug/L 04/30/20 21:20 62-75-904/24/20 17:015.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 04/30/20 21:20 621-64-704/24/20 17:015.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 04/30/20 21:20 86-30-604/24/20 17:0110.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/30/20 21:20 108-60-104/24/20 17:015.0 1.3 1
Pentachlorophenol ND ug/L 04/30/20 21:20 87-86-504/24/20 17:0110.0 2.8 1
Phenanthrene ND ug/L 04/30/20 21:20 85-01-804/24/20 17:015.0 1.4 1
Phenol ND ug/L 04/30/20 21:20 108-95-204/24/20 17:015.0 1.5 1
Pyrene ND ug/L 04/30/20 21:20 129-00-004/24/20 17:015.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 04/30/20 21:20 120-82-104/24/20 17:015.0 1.6 1
2,4,6-Trichlorophenol ND ug/L 04/30/20 21:20 88-06-204/24/20 17:0110.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)51 %04/30/20 21:20 4165-60-004/24/20 17:0110-120 1
2-Fluorobiphenyl (S)43 %04/30/20 21:20 321-60-804/24/20 17:0115-120 1
Terphenyl-d14 (S)67 %04/30/20 21:20 1718-51-004/24/20 17:0111-131 1
Phenol-d6 (S)28 %04/30/20 21:20 13127-88-304/24/20 17:0110-120 1
2-Fluorophenol (S)36 %04/30/20 21:20 367-12-404/24/20 17:0110-120 1
2,4,6-Tribromophenol (S)42 %04/30/20 21:20 118-79-604/24/20 17:0110-137 1
Tentatively Identified Compounds
Unknown 7.3J ug/L 04/30/20 21:2004/24/20 17:011
Ethanol, 2-butoxy-45.7J ug/L 04/30/20 21:20 111-76-2 N04/24/20 17:011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-2 Lab ID:92474993002 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
602 Volatiles by Method 6200
Benzene ND ug/L 04/30/20 02:03 71-43-21.0 0.24 1
Chlorobenzene ND ug/L 04/30/20 02:03 108-90-71.0 0.22 1
1,2-Dichlorobenzene ND ug/L 04/30/20 02:03 95-50-11.0 0.24 1
1,3-Dichlorobenzene ND ug/L 04/30/20 02:03 541-73-11.0 0.25 1
1,4-Dichlorobenzene ND ug/L 04/30/20 02:03 106-46-71.0 0.25 1
Diisopropyl ether ND ug/L 04/30/20 02:03 108-20-31.0 0.33 1
Ethylbenzene ND ug/L 04/30/20 02:03 100-41-41.0 0.24 1
Isopropylbenzene (Cumene)ND ug/L 04/30/20 02:03 98-82-81.0 0.24 1
Methyl-tert-butyl ether ND ug/L 04/30/20 02:03 1634-04-41.0 0.44 1
Naphthalene ND ug/L 04/30/20 02:03 91-20-32.0 0.66 1
Toluene ND ug/L 04/30/20 02:03 108-88-31.0 0.23 1
m&p-Xylene ND ug/L 04/30/20 02:03 179601-23-12.0 0.44 1
o-Xylene ND ug/L 04/30/20 02:03 95-47-61.0 0.24 1
Surrogates
4-Bromofluorobenzene (S)102 %04/30/20 02:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %04/30/20 02:03 17060-07-070-130 1
Toluene-d8 (S)104 %04/30/20 02:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1466497
MADEPV
MADEP VPH
MADEPV
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92474993001, 92474993002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3522712-3
Associated Lab Samples:92474993001, 92474993002
Matrix:Water
AnalyzedMDL
Aliphatic (C05-C08)ug/L ND 100 04/26/20 12:0733.3
Aliphatic (C09-C12)ug/L ND 100 04/26/20 12:0733.3
Aromatic (C09-C10),Unadjusted ug/L ND 100 04/26/20 12:0733.3
2,5-Dibromotoluene (FID)%83.8 70.0-130 04/26/20 12:07
2,5-Dibromotoluene (PID)%76.5 70.0-130 04/26/20 12:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3522712-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3522712-2
Aliphatic (C05-C08)ug/L 13701200 114 70.0-1301131360 0.733 25
Aliphatic (C09-C12)ug/L 16701400 119 70.0-1301171640 1.81 25
Aromatic (C09-C10),Unadjusted ug/L 234200 117 70.0-130117234 0.00 25
2,5-Dibromotoluene (FID)%97.5 70.0-13098.2
2,5-Dibromotoluene (PID)%88.0 70.0-13088.9
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3522712-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1212534-03
R3522712-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aliphatic (C05-C08)ug/L 1200 103 70.0-13095.4 7.29 25120045.5 1280 1190
Aliphatic (C09-C12)ug/L 1400 117 70.0-130110 6.13 25140039.0 1680 1580
Aromatic (C09-
C10),Unadjusted ug/L 200 117 70.0-130113 3.48 25200ND234226
2,5-Dibromotoluene (FID)%97.3 70.0-13097.9
2,5-Dibromotoluene (PID)%88.1 70.0-13089.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1469075
3015
EPA 6010D
Metals (ICP) 6010D
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92474993001, 92474993002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3524340-1
Associated Lab Samples:92474993001, 92474993002
Matrix:Water
AnalyzedMDL
Chromium ug/L ND 10.0 05/03/20 17:335.00
Lead ug/L ND 6.00 05/03/20 17:332.95
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3524340-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium ug/L 9621000 96.2 80.0-120
Lead ug/L 9541000 95.4 80.0-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
538896
SM 6200B
SM 6200B
602 by 6200B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474993002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2872916
Associated Lab Samples:92474993002
Matrix:Water
AnalyzedMDL
1,2-Dichlorobenzene ug/L ND 1.0 04/29/20 19:280.24
1,3-Dichlorobenzene ug/L ND 1.0 04/29/20 19:280.25
1,4-Dichlorobenzene ug/L ND 1.0 04/29/20 19:280.25
Benzene ug/L ND 1.0 04/29/20 19:280.24
Chlorobenzene ug/L ND 1.0 04/29/20 19:280.22
Diisopropyl ether ug/L ND 1.0 04/29/20 19:280.33
Ethylbenzene ug/L ND 1.0 04/29/20 19:280.24
Isopropylbenzene (Cumene)ug/L ND 1.0 04/29/20 19:280.24
m&p-Xylene ug/L ND 2.0 04/29/20 19:280.44
Methyl-tert-butyl ether ug/L ND 1.0 04/29/20 19:280.44
Naphthalene ug/L ND 2.0 04/29/20 19:280.66
o-Xylene ug/L ND 1.0 04/29/20 19:280.24
Toluene ug/L ND 1.0 04/29/20 19:280.23
1,2-Dichloroethane-d4 (S)%98 70-130 04/29/20 19:28
4-Bromofluorobenzene (S)%101 70-130 04/29/20 19:28
Toluene-d8 (S)%104 70-130 04/29/20 19:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2872917LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/L 49.550 99 60-140
1,3-Dichlorobenzene ug/L 49.750 99 60-140
1,4-Dichlorobenzene ug/L 49.850 100 60-140
Benzene ug/L 50.250 100 60-140
Chlorobenzene ug/L 50.050 100 60-140
Diisopropyl ether ug/L 52.950 106 60-140
Ethylbenzene ug/L 46.750 93 60-140
Isopropylbenzene (Cumene)ug/L 50.450 101 60-140
m&p-Xylene ug/L 94.0100 94 60-140
Methyl-tert-butyl ether ug/L 55.850 112 60-140
Naphthalene ug/L 52.450 105 60-140
o-Xylene ug/L 49.650 99 60-140
Toluene ug/L 42.950 86 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2872918MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92475115008
2872919
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dichlorobenzene ug/L 20 103 60-140100 2 3020ND20.5 20.1
1,3-Dichlorobenzene ug/L 20 103 60-140102 1 3020ND20.7 20.4
1,4-Dichlorobenzene ug/L 20 103 60-140102 1 3020ND20.6 20.4
Benzene ug/L 20 106 60-140105 0 3020ND21.1 21.1
Chlorobenzene ug/L 20 104 60-140102 2 3020ND20.8 20.4
Diisopropyl ether ug/L 20 104 60-140101 2 3020ND20.7 20.2
Ethylbenzene ug/L 20 100 60-140100 1 3020ND20.1 19.9
Isopropylbenzene
(Cumene)ug/L 20 107 60-140106 1 3020ND21.4 21.2
m&p-Xylene ug/L 40 99 60-14099 0 3040ND39.6 39.6
Methyl-tert-butyl ether ug/L 20 108 60-140106 2 3020ND21.6 21.2
Naphthalene ug/L 20 104 60-140104 0 3020ND20.8 20.7
o-Xylene ug/L 20 102 60-140102 0 3020ND20.5 20.4
Toluene ug/L 20 93 60-14091 1 3020ND18.6 18.3
1,2-Dichloroethane-d4 (S)%103 70-130103
4-Bromofluorobenzene (S)%101 70-130104
Toluene-d8 (S)%95 70-13098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
538601
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474993001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2871603
Associated Lab Samples:92474993001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/30/20 15:410.42
1,1,1-Trichloroethane ug/L ND 0.50 04/30/20 15:410.28
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/30/20 15:410.19
1,1,2-Trichloroethane ug/L ND 0.50 04/30/20 15:410.23
1,1-Dichloroethane ug/L ND 0.50 04/30/20 15:410.24
1,1-Dichloroethene ug/L ND 0.50 04/30/20 15:410.22
1,1-Dichloropropene ug/L ND 0.50 04/30/20 15:410.35
1,2,3-Trichlorobenzene ug/L ND 2.0 04/30/20 15:410.78
1,2,3-Trichloropropane ug/L ND 0.50 04/30/20 15:410.27
1,2,4-Trichlorobenzene ug/L ND 2.0 04/30/20 15:410.44
1,2,4-Trimethylbenzene ug/L ND 0.50 04/30/20 15:410.19
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/30/20 15:410.38
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/30/20 15:410.23
1,2-Dichlorobenzene ug/L ND 0.50 04/30/20 15:410.24
1,2-Dichloroethane ug/L ND 0.50 04/30/20 15:410.26
1,2-Dichloropropane ug/L ND 0.50 04/30/20 15:410.18
1,3,5-Trimethylbenzene ug/L ND 0.50 04/30/20 15:410.23
1,3-Dichlorobenzene ug/L ND 0.50 04/30/20 15:410.25
1,3-Dichloropropane ug/L ND 0.50 04/30/20 15:410.34
1,4-Dichlorobenzene ug/L ND 0.50 04/30/20 15:410.25
2,2-Dichloropropane ug/L ND 0.50 04/30/20 15:410.28
2-Chlorotoluene ug/L ND 0.50 04/30/20 15:410.21
4-Chlorotoluene ug/L ND 0.50 04/30/20 15:410.21
Benzene ug/L ND 0.50 04/30/20 15:410.24
Bromobenzene ug/L ND 0.50 04/30/20 15:410.22
Bromochloromethane ug/L ND 0.50 04/30/20 15:410.26
Bromodichloromethane ug/L ND 0.50 04/30/20 15:410.18
Bromoform ug/L ND 0.50 04/30/20 15:410.40
Bromomethane ug/L ND 5.0 04/30/20 15:411.7
Carbon tetrachloride ug/L ND 0.50 04/30/20 15:410.23
Chlorobenzene ug/L ND 0.50 04/30/20 15:410.22
Chloroethane ug/L ND 1.0 04/30/20 15:410.58
Chloroform ug/L ND 0.50 04/30/20 15:410.35
Chloromethane ug/L ND 1.0 04/30/20 15:410.42
cis-1,2-Dichloroethene ug/L ND 0.50 04/30/20 15:410.21
cis-1,3-Dichloropropene ug/L ND 0.50 04/30/20 15:410.36
Dibromochloromethane ug/L ND 0.50 04/30/20 15:410.40
Dibromomethane ug/L ND 0.50 04/30/20 15:410.31
Dichlorodifluoromethane ug/L ND 0.50 04/30/20 15:410.28
Diisopropyl ether ug/L ND 0.50 04/30/20 15:410.33
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2871603
Associated Lab Samples:92474993001
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 04/30/20 15:410.24
Hexachloro-1,3-butadiene ug/L ND 2.0 04/30/20 15:411.2
Isopropylbenzene (Cumene)ug/L ND 0.50 04/30/20 15:410.24
m&p-Xylene ug/L ND 1.0 04/30/20 15:410.44
Methyl-tert-butyl ether ug/L ND 0.50 04/30/20 15:410.44
Methylene Chloride ug/L ND 2.0 04/30/20 15:411.5
n-Butylbenzene ug/L ND 0.50 04/30/20 15:410.35
n-Propylbenzene ug/L ND 0.50 04/30/20 15:410.24
Naphthalene ug/L ND 2.0 04/30/20 15:410.66
o-Xylene ug/L ND 0.50 04/30/20 15:410.24
sec-Butylbenzene ug/L ND 0.50 04/30/20 15:410.25
Styrene ug/L ND 0.50 04/30/20 15:410.26
tert-Butylbenzene ug/L ND 0.50 04/30/20 15:410.25
Tetrachloroethene ug/L ND 0.50 04/30/20 15:410.23
Toluene ug/L ND 0.50 04/30/20 15:410.23
trans-1,2-Dichloroethene ug/L ND 0.50 04/30/20 15:410.26
trans-1,3-Dichloropropene ug/L ND 0.50 04/30/20 15:410.39
Trichloroethene ug/L ND 0.50 04/30/20 15:410.23
Trichlorofluoromethane ug/L ND 1.0 04/30/20 15:410.34
Vinyl chloride ug/L ND 1.0 04/30/20 15:410.41
1,2-Dichloroethane-d4 (S)%99 70-130 04/30/20 15:41
4-Bromofluorobenzene (S)%100 70-130 04/30/20 15:41
Toluene-d8 (S)%104 70-130 04/30/20 15:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2871604LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.350 109 60-140
1,1,1-Trichloroethane ug/L 50.150 100 60-140
1,1,2,2-Tetrachloroethane ug/L 51.750 103 60-140
1,1,2-Trichloroethane ug/L 56.150 112 60-140
1,1-Dichloroethane ug/L 45.950 92 60-140
1,1-Dichloroethene ug/L 48.750 97 60-140
1,1-Dichloropropene ug/L 47.050 94 60-140
1,2,3-Trichlorobenzene ug/L 51.650 103 60-140
1,2,3-Trichloropropane ug/L 54.550 109 60-140
1,2,4-Trichlorobenzene ug/L 52.050 104 60-140
1,2,4-Trimethylbenzene ug/L 47.550 95 60-140
1,2-Dibromo-3-chloropropane ug/L 53.050 106 60-140
1,2-Dibromoethane (EDB)ug/L 50.250 100 60-140
1,2-Dichlorobenzene ug/L 50.150 100 60-140
1,2-Dichloroethane ug/L 46.450 93 60-140
1,2-Dichloropropane ug/L 47.450 95 60-140
1,3,5-Trimethylbenzene ug/L 51.050 102 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
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[phone]
Page 17 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2871604LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 49.750 99 60-140
1,3-Dichloropropane ug/L 52.750 105 60-140
1,4-Dichlorobenzene ug/L 49.650 99 60-140
2,2-Dichloropropane ug/L 50.050 100 60-140
2-Chlorotoluene ug/L 49.150 98 60-140
4-Chlorotoluene ug/L 50.250 100 60-140
Benzene ug/L 49.250 98 60-140
Bromobenzene ug/L 51.050 102 60-140
Bromochloromethane ug/L 48.650 97 60-140
Bromodichloromethane ug/L 52.650 105 60-140
Bromoform ug/L 47.350 95 60-140
Bromomethane ug/L 61.950 124 60-140
Carbon tetrachloride ug/L 52.550 105 60-140
Chlorobenzene ug/L 49.350 99 60-140
Chloroethane ug/L 46.450 93 60-140
Chloroform ug/L 48.250 96 60-140
Chloromethane ug/L 44.150 88 60-140
cis-1,2-Dichloroethene ug/L 47.650 95 60-140
cis-1,3-Dichloropropene ug/L 46.950 94 60-140
Dibromochloromethane ug/L 48.350 97 60-140
Dibromomethane ug/L 50.050 100 60-140
Dichlorodifluoromethane ug/L 52.850 106 60-140
Diisopropyl ether ug/L 54.350 109 60-140
Ethylbenzene ug/L 46.550 93 60-140
Hexachloro-1,3-butadiene ug/L 50.950 102 60-140
Isopropylbenzene (Cumene)ug/L 49.150 98 60-140
m&p-Xylene ug/L 93.3100 93 60-140
Methyl-tert-butyl ether ug/L 56.650 113 60-140
Methylene Chloride ug/L 45.950 92 60-140
n-Butylbenzene ug/L 51.750 103 60-140
n-Propylbenzene ug/L 46.150 92 60-140
Naphthalene ug/L 54.550 109 60-140
o-Xylene ug/L 47.150 94 60-140
sec-Butylbenzene ug/L 48.150 96 60-140
Styrene ug/L 51.550 103 60-140
tert-Butylbenzene ug/L 41.750 83 60-140
Tetrachloroethene ug/L 51.150 102 60-140
Toluene ug/L 43.950 88 60-140
trans-1,2-Dichloroethene ug/L 48.050 96 60-140
trans-1,3-Dichloropropene ug/L 54.350 109 60-140
Trichloroethene ug/L 47.450 95 60-140
Trichlorofluoromethane ug/L 47.350 95 60-140
Vinyl chloride ug/L 55.950 112 60-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
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Page 18 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2873852MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92474993001
2873853
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 106 60-140107 1 3020ND21.3 21.4
1,1,1-Trichloroethane ug/L 20 115 60-140111 3 3020ND22.9 22.2
1,1,2,2-Tetrachloroethane ug/L 20 111 60-140111 0 3020ND22.2 22.2
1,1,2-Trichloroethane ug/L 20 112 60-140109 3 3020ND22.4 21.8
1,1-Dichloroethane ug/L 20 106 60-140102 4 3020ND21.2 20.3
1,1-Dichloroethene ug/L 20 112 60-140109 3 3020ND22.5 21.9
1,1-Dichloropropene ug/L 20 103 60-140100 3 3020ND20.7 20.0
1,2,3-Trichlorobenzene ug/L 20 114 60-140113 0 3020ND22.8 22.7
1,2,3-Trichloropropane ug/L 20 105 60-140107 2 3020ND21.0 21.4
1,2,4-Trichlorobenzene ug/L 20 114 60-140114 0 3020ND22.8 22.7
1,2,4-Trimethylbenzene ug/L 20 98 60-140101 3 3020ND19.5 20.2
1,2-Dibromo-3-
chloropropane ug/L 20 110 60-140110 0 3020ND21.9 21.9
1,2-Dibromoethane (EDB)ug/L 20 102 60-140102 0 3020ND20.3 20.3
1,2-Dichlorobenzene ug/L 20 103 60-140107 3 3020ND20.6 21.3
1,2-Dichloroethane ug/L 20 101 60-14099 2 3020ND20.2 19.8
1,2-Dichloropropane ug/L 20 104 60-140102 2 3020ND20.8 20.4
1,3,5-Trimethylbenzene ug/L 20 105 60-140106 1 3020ND21.1 21.2
1,3-Dichlorobenzene ug/L 20 103 60-140104 1 3020ND20.7 20.9
1,3-Dichloropropane ug/L 20 106 60-140106 1 3020ND21.3 21.2
1,4-Dichlorobenzene ug/L 20 103 60-140102 1 3020ND20.5 20.3
2,2-Dichloropropane ug/L 20 103 60-14099 3 3020ND20.5 19.9
2-Chlorotoluene ug/L 20 102 60-140104 3 3020ND20.3 20.9
4-Chlorotoluene ug/L 20 102 60-140104 2 3020ND20.5 20.8
Benzene ug/L 20 109 60-140107 2 3020ND21.8 21.3
Bromobenzene ug/L 20 105 60-140106 1 3020ND20.9 21.2
Bromochloromethane ug/L 20 109 60-140105 4 3020ND21.9 21.0
Bromodichloromethane ug/L 20 112 60-140110 2 3020ND22.4 22.0
Bromoform ug/L 20 96 60-14090 6 3020ND19.2 18.1
Bromomethane ug/L 20 134 60-140127 5 3020ND26.9 25.5
Carbon tetrachloride ug/L 20 121 60-140120 1 3020ND24.2 23.9
Chlorobenzene ug/L 20 105 60-140104 0 3020ND20.9 20.9
Chloroethane ug/L 20 114 60-140111 3 3020ND22.8 22.2
Chloroform ug/L 20 109 60-140109 0 3020ND21.8 21.8
Chloromethane ug/L 20 106 60-14098 7 3020ND21.2 19.7
cis-1,2-Dichloroethene ug/L 20 109 60-140106 3 3020ND21.9 21.2
cis-1,3-Dichloropropene ug/L 20 88 60-14086 2 3020ND17.7 17.3
Dibromochloromethane ug/L 20 94 60-14095 1 3020ND18.8 19.1
Dibromomethane ug/L 20 108 60-140105 3 3020ND21.6 21.0
Dichlorodifluoromethane ug/L 20 119 60-140113 5 3020ND23.9 22.7
Diisopropyl ether ug/L 20 103 60-14099 4 3020ND20.6 19.8
Ethylbenzene ug/L 20 98 60-14098 0 3020ND19.6 19.7
Hexachloro-1,3-butadiene ug/L 20 113 60-140109 3 3020ND22.6 21.9
Isopropylbenzene(Cumene)ug/L 20 105 60-140108 3 3020ND21.0 21.6
m&p-Xylene ug/L 40 100 60-14097 2 3040ND39.8 39.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2873852MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92474993001
2873853
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 109 60-140107 2 3020ND21.8 21.4
Methylene Chloride ug/L 20 105 60-14098 6 3020ND20.9 19.6
n-Butylbenzene ug/L 20 115 60-140114 1 3020ND22.9 22.8
n-Propylbenzene ug/L 20 97 60-14099 3 30200.47J 19.8 20.3
Naphthalene ug/L 20 127 60-140133 4 3020ND25.4 26.5
o-Xylene ug/L 20 101 60-140102 1 3020ND20.2 20.4
sec-Butylbenzene ug/L 20 103 60-140103 0 30201.6 22.2 22.3
Styrene ug/L 20 108 60-140107 1 3020ND21.7 21.4
tert-Butylbenzene ug/L 20 87 60-14088 1 3020ND17.5 17.7
Tetrachloroethene ug/L 20 105 60-140105 0 3020ND21.0 21.1
Toluene ug/L 20 96 60-14090 5 3020ND19.1 18.1
trans-1,2-Dichloroethene ug/L 20 108 60-140105 3 3020ND21.7 21.1
trans-1,3-Dichloropropene ug/L 20 107 60-140100 7 3020ND21.3 19.9
Trichloroethene ug/L 20 103 60-140102 1 3020ND20.6 20.4
Trichlorofluoromethane ug/L 20 111 60-140108 3 3020ND22.1 21.5
Vinyl chloride ug/L 20 132 60-140127 4 3020ND26.4 25.4
1,2-Dichloroethane-d4 (S)%104 70-130100
4-Bromofluorobenzene (S)%102 70-130101
Toluene-d8 (S)%99 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
538113
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474993001, 92474993002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2869500
Associated Lab Samples:92474993001, 92474993002
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 5.0 04/29/20 00:431.6
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 04/29/20 00:431.3
2,4,6-Trichlorophenol ug/L ND 10.0 04/29/20 00:431.4
2,4-Dichlorophenol ug/L ND 5.0 04/29/20 00:431.5
2,4-Dimethylphenol ug/L ND 10.0 04/29/20 00:431.5
2,4-Dinitrophenol ug/L ND 50.0 04/29/20 00:437.3
2,4-Dinitrotoluene ug/L ND 5.0 04/29/20 00:431.7
2,6-Dinitrotoluene ug/L ND 5.0 04/29/20 00:431.7
2-Chloronaphthalene ug/L ND 5.0 04/29/20 00:431.4
2-Chlorophenol ug/L ND 5.0 04/29/20 00:431.4
2-Nitrophenol ug/L ND 5.0 04/29/20 00:431.7
3,3'-Dichlorobenzidine ug/L ND 10.0 04/29/20 00:432.7
4,6-Dinitro-2-methylphenol ug/L ND 10.0 04/29/20 00:434.5
4-Bromophenylphenyl ether ug/L ND 5.0 04/29/20 00:431.2
4-Chloro-3-methylphenol ug/L ND 5.0 04/29/20 00:432.8
4-Chlorophenylphenyl ether ug/L ND 5.0 04/29/20 00:431.5
4-Nitrophenol ug/L ND 10.0 04/29/20 00:439.4
Acenaphthene ug/L ND 5.0 04/29/20 00:431.4
Acenaphthylene ug/L ND 5.0 04/29/20 00:431.5
Anthracene ug/L ND 5.0 04/29/20 00:431.6
Benzo(a)anthracene ug/L ND 5.0 04/29/20 00:431.5
Benzo(a)pyrene ug/L ND 5.0 04/29/20 00:431.8
Benzo(b)fluoranthene ug/L ND 5.0 04/29/20 00:431.7
Benzo(g,h,i)perylene ug/L ND 5.0 04/29/20 00:431.6
Benzo(k)fluoranthene ug/L ND 5.0 04/29/20 00:431.5
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/29/20 00:431.3
bis(2-Chloroethyl) ether ug/L ND 5.0 04/29/20 00:431.7
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/29/20 00:432.0
Butylbenzylphthalate ug/L ND 5.0 04/29/20 00:431.9
Chrysene ug/L ND 5.0 04/29/20 00:431.4
Di-n-butylphthalate ug/L ND 5.0 04/29/20 00:431.6
Di-n-octylphthalate ug/L ND 5.0 04/29/20 00:432.2
Dibenz(a,h)anthracene ug/L ND 5.0 04/29/20 00:431.6
Diethylphthalate ug/L ND 5.0 04/29/20 00:431.6
Dimethylphthalate ug/L ND 5.0 04/29/20 00:431.4
Fluoranthene ug/L ND 5.0 04/29/20 00:431.6
Fluorene ug/L ND 5.0 04/29/20 00:431.4
Hexachloro-1,3-butadiene ug/L ND 5.0 04/29/20 00:431.6
Hexachlorobenzene ug/L ND 5.0 04/29/20 00:431.3
Hexachlorocyclopentadiene ug/L ND 10.0 04/29/20 00:432.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2869500
Associated Lab Samples:92474993001, 92474993002
Matrix:Water
AnalyzedMDL
Hexachloroethane ug/L ND 5.0 04/29/20 00:431.3
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 04/29/20 00:431.7
Isophorone ug/L ND 10.0 04/29/20 00:431.3
N-Nitroso-di-n-propylamine ug/L ND 5.0 04/29/20 00:431.3
N-Nitrosodimethylamine ug/L ND 5.0 04/29/20 00:431.8
N-Nitrosodiphenylamine ug/L ND 10.0 04/29/20 00:431.4
Naphthalene ug/L ND 5.0 04/29/20 00:431.6
Nitrobenzene ug/L ND 5.0 04/29/20 00:431.5
Pentachlorophenol ug/L ND 10.0 04/29/20 00:432.8
Phenanthrene ug/L ND 5.0 04/29/20 00:431.4
Phenol ug/L ND 5.0 04/29/20 00:431.5
Pyrene ug/L ND 5.0 04/29/20 00:431.5
2,4,6-Tribromophenol (S)%65 10-137 04/29/20 00:43
2-Fluorobiphenyl (S)%59 15-120 04/29/20 00:43
2-Fluorophenol (S)%52 10-120 04/29/20 00:43
Nitrobenzene-d5 (S)%69 10-120 04/29/20 00:43
Phenol-d6 (S)%40 10-120 04/29/20 00:43
Terphenyl-d14 (S)%99 11-131 04/29/20 00:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2869501LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 24.250 48 44-142
2,2'-Oxybis(1-chloropropane)ug/L 45.250 90 36-166
2,4,6-Trichlorophenol ug/L 31.650 63 37-144
2,4-Dichlorophenol ug/L 33.750 67 1-191
2,4-Dimethylphenol ug/L 34.350 69 32-119
2,4-Dinitrophenol ug/L 155250 62 1-181
2,4-Dinitrotoluene ug/L 43.850 88 39-139
2,6-Dinitrotoluene ug/L 40.050 80 50-158
2-Chloronaphthalene ug/L 28.5 L2505760-118
2-Chlorophenol ug/L 34.350 69 23-134
2-Nitrophenol ug/L 37.650 75 29-182
3,3'-Dichlorobenzidine ug/L 76.2100 76 1-262
4,6-Dinitro-2-methylphenol ug/L 75.0100 75 1-181
4-Bromophenylphenyl ether ug/L 31.550 63 53-127
4-Chloro-3-methylphenol ug/L 72.4100 72 22-147
4-Chlorophenylphenyl ether ug/L 30.150 60 25-158
4-Nitrophenol ug/L 99.5250 40 1-132
Acenaphthene ug/L 32.150 64 47-145
Acenaphthylene ug/L 34.050 68 33-145
Anthracene ug/L 38.150 76 1-166
Benzo(a)anthracene ug/L 41.950 84 33-143
Benzo(a)pyrene ug/L 43.750 87 17-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2869501LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 42.050 84 24-159
Benzo(g,h,i)perylene ug/L 45.650 91 1-219
Benzo(k)fluoranthene ug/L 43.950 88 11-162
bis(2-Chloroethoxy)methane ug/L 35.850 72 33-184
bis(2-Chloroethyl) ether ug/L 36.650 73 12-158
bis(2-Ethylhexyl)phthalate ug/L 46.150 92 8-158
Butylbenzylphthalate ug/L 46.050 92 1-152
Chrysene ug/L 42.650 85 17-168
Di-n-butylphthalate ug/L 45.050 90 1-118
Di-n-octylphthalate ug/L 49.050 98 4-146
Dibenz(a,h)anthracene ug/L 44.750 89 1-227
Diethylphthalate ug/L 40.750 81 1-114
Dimethylphthalate ug/L 37.150 74 1-112
Fluoranthene ug/L 43.050 86 26-137
Fluorene ug/L 34.250 68 59-121
Hexachloro-1,3-butadiene ug/L 22.550 45 24-116
Hexachlorobenzene ug/L 32.850 66 1-152
Hexachlorocyclopentadiene ug/L 17.650 35 25-150
Hexachloroethane ug/L 25.050 50 40-113
Indeno(1,2,3-cd)pyrene ug/L 44.650 89 1-171
Isophorone ug/L 36.850 74 21-196
N-Nitroso-di-n-propylamine ug/L 35.550 71 1-230
N-Nitrosodimethylamine ug/L 30.350 61 25-150
N-Nitrosodiphenylamine ug/L 37.050 74 25-150
Naphthalene ug/L 29.750 59 21-133
Nitrobenzene ug/L 34.950 70 35-180
Pentachlorophenol ug/L 60.2100 60 14-176
Phenanthrene ug/L 37.850 76 54-120
Phenol ug/L 23.550 47 5-112
Pyrene ug/L 39.950 80 52-115
2,4,6-Tribromophenol (S)%77 10-137
2-Fluorobiphenyl (S)%68 15-120
2-Fluorophenol (S)%57 10-120
Nitrobenzene-d5 (S)%80 10-120
Phenol-d6 (S)%47 10-120
Terphenyl-d14 (S)%100 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2869502MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35544825001
2869503
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 57 44-14247 19 30501.6U 28.4 23.6
2,2'-Oxybis(1-
chloropropane)ug/L 50 109 36-166106 3 30501.3U 54.6 52.8
2,4,6-Trichlorophenol ug/L M1,R1506437-14435 59 30501.4U 32.2 17.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2869502MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35544825001
2869503
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4-Dichlorophenol ug/L 50 73 1-19164 12 30501.5U 36.4 32.2
2,4-Dimethylphenol ug/L 50 77 32-11977 1 30501.5U 38.7 38.4
2,4-Dinitrophenol ug/L M125081-1810 302507.3U 20.3J ND
2,4-Dinitrotoluene ug/L 50 97 39-13988 10 30501.7U 48.6 44.1
2,6-Dinitrotoluene ug/L 50 91 50-15887 4 30501.7U 45.4 43.6
2-Chloronaphthalene ug/L 50 70 60-11863 10 30501.4U 35.1 31.7
2-Chlorophenol ug/L 50 77 23-13468 13 30501.4U 38.5 33.9
2-Nitrophenol ug/L 50 82 29-18267 20 30501.7U 40.9 33.5
3,3'-Dichlorobenzidine ug/L 100 89 1-26275 17 301002.7U 89.3 75.4
4,6-Dinitro-2-methylphenol ug/L 100 39 1-18110 301004.5U 39.0 9.8J
4-Bromophenylphenyl ether ug/L 50 75 53-12774 2 30501.2U 37.6 36.8
4-Chloro-3-methylphenol ug/L 100 82 22-14780 3 301002.8U 82.2 80.1
4-Chlorophenylphenyl ether ug/L 50 75 25-15873 3 30501.5U 37.7 36.6
4-Nitrophenol ug/L 250 17 1-1324 302509.4U 43.0 ND
Acenaphthene ug/L 50 79 47-14574 7 30501.4U 39.6 37.1
Acenaphthylene ug/L 50 82 33-14576 8 30501.5U 41.0 38.0
Anthracene ug/L 50 88 1-16683 5 30501.6U 43.9 41.7
Benzo(a)anthracene ug/L 50 99 33-14385 15 30501.5U 49.6 42.6
Benzo(a)pyrene ug/L 50 101 17-16387 15 30501.8U 50.5 43.5
Benzo(b)fluoranthene ug/L 50 98 24-15986 13 30501.7U 49.0 42.8
Benzo(g,h,i)perylene ug/L 50 106 1-21990 17 30501.6U 53.0 44.9
Benzo(k)fluoranthene ug/L 50 102 11-16288 15 30501.5U 51.0 43.8
bis(2-
Chloroethoxy)methane ug/L 50 81 33-18481 1 30501.3U 40.6 40.3
bis(2-Chloroethyl) ether ug/L 50 85 12-15888 3 30501.7U 42.6 44.0
bis(2-Ethylhexyl)phthalate ug/L 50 110 8-15893 17 30502.0U 55.1 46.7
Butylbenzylphthalate ug/L 50 111 1-15294 17 30501.9U 55.3 46.8
Chrysene ug/L 50 99 17-16885 15 30501.4U 49.4 42.4
Di-n-butylphthalate ug/L 50 107 1-11891 16 30501.6U 53.6 45.6
Di-n-octylphthalate ug/L 50 118 4-14696 20 30502.2U 59.0 48.1
Dibenz(a,h)anthracene ug/L 50 104 1-22788 17 30501.6U 52.1 43.9
Diethylphthalate ug/L 50 93 1-11486 7 30501.6U 46.4 43.1
Dimethylphthalate ug/L 50 86 1-11282 5 30501.4U 42.8 40.8
Fluoranthene ug/L 50 102 26-13788 15 30501.6U 51.2 44.0
Fluorene ug/L 50 84 59-12180 5 30501.4U 41.8 39.8
Hexachloro-1,3-butadiene ug/L 50 51 24-11643 17 30501.6U 25.6 21.4
Hexachlorobenzene ug/L 50 77 1-15274 3 30501.3U 38.5 37.2
Hexachlorocyclopentadiene ug/L 50 39 25-15032 18 30502.4U 19.4 16.2
Hexachloroethane ug/L 50 61 40-11352 16 30501.3U 30.5 26.0
Indeno(1,2,3-cd)pyrene ug/L 50 104 1-17187 17 30501.7U 52.0 43.7
Isophorone ug/L 50 85 21-19683 3 30501.3U 42.7 41.6
N-Nitroso-di-n-propylamine ug/L 50 84 1-23084 0 30501.3U 42.0 42.2
N-Nitrosodimethylamine ug/L 50 65 25-15068 5 30501.8U 32.5 34.2
N-Nitrosodiphenylamine ug/L 50 83 25-15080 3 30501.4U 41.4 40.0
Naphthalene ug/L 50 70 21-13361 12 30501.6U 34.8 30.7
Nitrobenzene ug/L 50 80 35-18080 1 30501.5U 39.8 40.1
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2869502MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35544825001
2869503
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Pentachlorophenol ug/L M11003614-1767 301002.8U 35.8 6.7J
Phenanthrene ug/L 50 89 54-12083 7 30501.4U 44.4 41.5
Phenol ug/L 50 50 5-11248 6 30501.5U 25.2 23.8
Pyrene ug/L 50 95 52-11585 11 30501.5U 47.3 42.4
2,4,6-Tribromophenol (S)%95 10-13759
2-Fluorobiphenyl (S)%88 15-12083
2-Fluorophenol (S)%63 10-12044
Nitrobenzene-d5 (S)%97 10-12093
Phenol-d6 (S)%52 10-12048
Terphenyl-d14 (S)%126 11-131107
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
538963
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474993001, 92474993002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2873261
Associated Lab Samples:92474993001, 92474993002
Matrix:Water
AnalyzedMDL
Aliphatic (C09-C18)ug/L ND 100 N205/04/20 08:41100
Aliphatic (C19-C36)ug/L ND 100 N205/04/20 08:41100
Aromatic (C11-C22)ug/L ND 100 N205/04/20 08:41100
2-Bromonaphthalene (S)%91 40-140 05/04/20 08:41
2-Fluorobiphenyl (S)%91 40-140 05/04/20 08:41
Nonatriacontane (S)%54 40-140 05/04/20 08:41
o-Terphenyl (S)%67 40-140 05/04/20 08:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2873262LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2873263
Aliphatic (C09-C18)ug/L ND L2,N23003140-14039116 50
Aliphatic (C19-C36)ug/L 157 L2,N24003940-14043173 10 50
Aromatic (C11-C22)ug/L 588 N28506940-14071607 3 50
2-Bromonaphthalene (S)%89 40-140105
2-Fluorobiphenyl (S)%92 40-140105
Nonatriacontane (S)%46 40-14040
o-Terphenyl (S)%83 40-14086
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The reported TIC has an 85% or higher match on a mass spectral library search.N
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Re-extraction or re-analysis could not be performed due to insufficient sample amount.P2
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92474993001 538963 539434MW-1 MADEP EPH MADEP EPH
92474993002 538963 539434MW-2 MADEP EPH MADEP EPH
92474993001 1466497 1466497MW-1 MADEPV MADEP VPH
92474993002 1466497 1466497MW-2 MADEPV MADEP VPH
92474993001 1469075 1469075MW-1 3015 EPA 6010D
92474993002 1469075 1469075MW-2 3015 EPA 6010D
92474993001 538113 538662MW-1 EPA 625.1 EPA 625.1
92474993002 538113 538662MW-2 EPA 625.1 EPA 625.1
92474993002 538896MW-2 SM 6200B
92474993001 538601MW-1 SM 6200B
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Page 29 of 31
Page 30 of 31
Page 31 of 31
#=CL#
May 04, 2020
LIMS USE: FR - BRITNEY BARNES
LIMS OBJECT ID: 92474993
92474993
Project:
Pace Project No.:
RE:
Britney Barnes
Civil & Environmental Consultants
530 Howell Rd
Suite 203
Greenville, SC
Greensboro NC LC 0134 UST Clos
Dear Britney Barnes:
Enclosed are the analytical results for sample(s) received by the laboratory on April 24, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Sarah Galloway, Ryder Systems, Inc
REPORT OF LABORATORY ANALYSIS
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Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Lab ID Sample ID Matrix Date Collected Date Received
92474993001 MW-1 Water 04/23/20 00:00 04/24/20 09:54
92474993002 MW-2 Water 04/23/20 00:00 04/24/20 09:54
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92474993001 MW-1 MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 6010D 2 PANCCE
EPA 625.1 66 PASI-CPKS
SM 6200B 63 PASI-CSAS
92474993002 MW-2 MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 6010D 2 PANCCE
EPA 625.1 60 PASI-CPKS
SM 6200B 16 PASI-CSAS
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-1 Lab ID:92474993001 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)216 ug/L 05/04/20 13:41 L2,N205/01/20 13:431001001
Aliphatic (C19-C36)ND ug/L 05/04/20 13:41 L2,N205/01/20 13:431001001
Aromatic (C11-C22)270 ug/L 05/04/20 13:41 N205/01/20 13:431001001
Surrogates
Nonatriacontane (S)23 %05/04/20 13:41 7194-86-7 P2,S205/01/20 13:4340-140 1
o-Terphenyl (S)40 %05/04/20 13:41 84-15-105/01/20 13:4340-140 1
2-Fluorobiphenyl (S)94 %05/04/20 13:41 321-60-805/01/20 13:4340-140 1
2-Bromonaphthalene (S)94 %05/04/20 13:41 580-13-205/01/20 13:4340-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)84.8J ug/L 04/26/20 15:52 J04/26/20 15:5210033.3 1
Aliphatic (C09-C12)82.0J ug/L 04/26/20 15:52 J04/26/20 15:5210033.3 1
Aromatic (C09-C10),Unadjusted 133 ug/L 04/26/20 15:52 TPHC9C10A04/26/20 15:5210033.3 1
Surrogates
2,5-Dibromotoluene (FID)125 %04/26/20 15:52 615-59-8FID04/26/20 15:5270.0-130 1
2,5-Dibromotoluene (PID)98.0 %04/26/20 15:52 615-59-8PID04/26/20 15:5270.0-130 1
Analytical Method: EPA 6010D Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICP) 6010D
Chromium ND ug/L 05/03/20 18:42 7440-47-305/01/20 11:0810.0 5.00 1
Lead ND ug/L 05/03/20 18:42 7439-92-105/01/20 11:086.00 2.95 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 04/30/20 20:55 83-32-904/24/20 17:015.0 1.4 1
Acenaphthylene ND ug/L 04/30/20 20:55 208-96-804/24/20 17:015.0 1.5 1
Anthracene ND ug/L 04/30/20 20:55 120-12-704/24/20 17:015.0 1.6 1
Benzo(a)anthracene ND ug/L 04/30/20 20:55 56-55-304/24/20 17:015.0 1.5 1
Benzo(a)pyrene ND ug/L 04/30/20 20:55 50-32-804/24/20 17:015.0 1.8 1
Benzo(b)fluoranthene ND ug/L 04/30/20 20:55 205-99-204/24/20 17:015.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 04/30/20 20:55 191-24-204/24/20 17:015.0 1.6 1
Benzo(k)fluoranthene ND ug/L 04/30/20 20:55 207-08-904/24/20 17:015.0 1.5 1
4-Bromophenylphenyl ether ND ug/L 04/30/20 20:55 101-55-304/24/20 17:015.0 1.2 1
Butylbenzylphthalate ND ug/L 04/30/20 20:55 85-68-704/24/20 17:015.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 04/30/20 20:55 59-50-704/24/20 17:015.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 04/30/20 20:55 111-91-104/24/20 17:0110.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 04/30/20 20:55 111-44-404/24/20 17:015.0 1.7 1
2-Chloronaphthalene ND ug/L 04/30/20 20:55 91-58-7 L204/24/20 17:015.0 1.4 1
2-Chlorophenol ND ug/L 04/30/20 20:55 95-57-804/24/20 17:015.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 04/30/20 20:55 7005-72-304/24/20 17:015.0 1.5 1
Chrysene ND ug/L 04/30/20 20:55 218-01-904/24/20 17:015.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 04/30/20 20:55 53-70-304/24/20 17:015.0 1.6 1
3,3'-Dichlorobenzidine ND ug/L 04/30/20 20:55 91-94-104/24/20 17:0110.0 2.7 1
2,4-Dichlorophenol ND ug/L 04/30/20 20:55 120-83-204/24/20 17:015.0 1.5 1
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-1 Lab ID:92474993001 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Diethylphthalate ND ug/L 04/30/20 20:55 84-66-204/24/20 17:015.0 1.6 1
2,4-Dimethylphenol ND ug/L 04/30/20 20:55 105-67-904/24/20 17:0110.0 1.5 1
Dimethylphthalate ND ug/L 04/30/20 20:55 131-11-304/24/20 17:015.0 1.4 1
Di-n-butylphthalate ND ug/L 04/30/20 20:55 84-74-204/24/20 17:015.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 04/30/20 20:55 534-52-104/24/20 17:0110.0 4.5 1
2,4-Dinitrophenol ND ug/L 04/30/20 20:55 51-28-504/24/20 17:0150.0 7.3 1
2,4-Dinitrotoluene ND ug/L 04/30/20 20:55 121-14-204/24/20 17:015.0 1.7 1
2,6-Dinitrotoluene ND ug/L 04/30/20 20:55 606-20-204/24/20 17:015.0 1.7 1
Di-n-octylphthalate ND ug/L 04/30/20 20:55 117-84-004/24/20 17:015.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/30/20 20:55 117-81-704/24/20 17:015.0 2.0 1
Fluoranthene ND ug/L 04/30/20 20:55 206-44-004/24/20 17:015.0 1.6 1
Fluorene 1.9J ug/L 04/30/20 20:55 86-73-704/24/20 17:015.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 04/30/20 20:55 87-68-304/24/20 17:015.0 1.6 1
Hexachlorobenzene ND ug/L 04/30/20 20:55 118-74-104/24/20 17:015.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 04/30/20 20:55 77-47-404/24/20 17:0110.0 2.4 1
Hexachloroethane ND ug/L 04/30/20 20:55 67-72-104/24/20 17:015.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/30/20 20:55 193-39-504/24/20 17:015.0 1.7 1
Isophorone ND ug/L 04/30/20 20:55 78-59-104/24/20 17:0110.0 1.3 1
Naphthalene ND ug/L 04/30/20 20:55 91-20-304/24/20 17:015.0 1.6 1
Nitrobenzene ND ug/L 04/30/20 20:55 98-95-304/24/20 17:015.0 1.5 1
2-Nitrophenol ND ug/L 04/30/20 20:55 88-75-504/24/20 17:015.0 1.7 1
4-Nitrophenol ND ug/L 04/30/20 20:55 100-02-704/24/20 17:0110.0 9.4 1
N-Nitrosodimethylamine ND ug/L 04/30/20 20:55 62-75-904/24/20 17:015.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 04/30/20 20:55 621-64-704/24/20 17:015.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 04/30/20 20:55 86-30-604/24/20 17:0110.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/30/20 20:55 108-60-104/24/20 17:015.0 1.3 1
Pentachlorophenol ND ug/L 04/30/20 20:55 87-86-504/24/20 17:0110.0 2.8 1
Phenanthrene ND ug/L 04/30/20 20:55 85-01-804/24/20 17:015.0 1.4 1
Phenol ND ug/L 04/30/20 20:55 108-95-204/24/20 17:015.0 1.5 1
Pyrene ND ug/L 04/30/20 20:55 129-00-004/24/20 17:015.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 04/30/20 20:55 120-82-104/24/20 17:015.0 1.6 1
2,4,6-Trichlorophenol ND ug/L 04/30/20 20:55 88-06-204/24/20 17:0110.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)68 %04/30/20 20:55 4165-60-004/24/20 17:0110-120 1
2-Fluorobiphenyl (S)57 %04/30/20 20:55 321-60-804/24/20 17:0115-120 1
Terphenyl-d14 (S)113 %04/30/20 20:55 1718-51-004/24/20 17:0111-131 1
Phenol-d6 (S)34 %04/30/20 20:55 13127-88-304/24/20 17:0110-120 1
2-Fluorophenol (S)29 %04/30/20 20:55 367-12-404/24/20 17:0110-120 1
2,4,6-Tribromophenol (S)54 %04/30/20 20:55 118-79-604/24/20 17:0110-137 1
Tentatively Identified Compounds
1H-Indene, 2,3-dihydro-5 9.8J ug/L 04/30/20 20:55 874-35-1 N04/24/20 17:011
Naphthalene, 1,2,3,4-tet 6.1J ug/L 04/30/20 20:55 3877-19-8 N04/24/20 17:011
Naphthalene, 1,2,3,4-tet 12.3J ug/L 04/30/20 20:55 2809-64-5 N04/24/20 17:011
Naphthalene, 1,2,3,4-tet 9.0J ug/L 04/30/20 20:55 1680-51-9 N04/24/20 17:011
Naphthalene, 2,6-dimethy 5.6J ug/L 04/30/20 20:55 581-42-0 N04/24/20 17:011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-1 Lab ID:92474993001 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Tentatively Identified Compounds
Naphthalene, 1,6-dimethy 6.3J ug/L 04/30/20 20:55 575-43-9 N04/24/20 17:011
Unknown 12.8J ug/L 04/30/20 20:5504/24/20 17:011
n-Hexadecanoic acid 31.2J ug/L 04/30/20 20:55 57-10-3 N04/24/20 17:011
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/30/20 16:17 71-43-20.50 0.24 1
Bromobenzene ND ug/L 04/30/20 16:17 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 04/30/20 16:17 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 04/30/20 16:17 75-27-40.50 0.18 1
Bromoform ND ug/L 04/30/20 16:17 75-25-20.50 0.40 1
Bromomethane ND ug/L 04/30/20 16:17 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 04/30/20 16:17 104-51-80.50 0.35 1
sec-Butylbenzene 1.6 ug/L 04/30/20 16:17 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 04/30/20 16:17 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 04/30/20 16:17 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 04/30/20 16:17 108-90-70.50 0.22 1
Chloroethane ND ug/L 04/30/20 16:17 75-00-31.0 0.58 1
Chloroform ND ug/L 04/30/20 16:17 67-66-30.50 0.35 1
Chloromethane ND ug/L 04/30/20 16:17 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 04/30/20 16:17 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 04/30/20 16:17 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 04/30/20 16:17 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 04/30/20 16:17 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 04/30/20 16:17 106-93-40.50 0.23 1
Dibromomethane ND ug/L 04/30/20 16:17 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 04/30/20 16:17 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 04/30/20 16:17 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 04/30/20 16:17 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 04/30/20 16:17 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 04/30/20 16:17 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 04/30/20 16:17 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 04/30/20 16:17 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 04/30/20 16:17 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 04/30/20 16:17 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 04/30/20 16:17 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 04/30/20 16:17 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 04/30/20 16:17 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 04/30/20 16:17 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 04/30/20 16:17 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/30/20 16:17 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 04/30/20 16:17 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 04/30/20 16:17 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 04/30/20 16:17 87-68-32.0 1.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-1 Lab ID:92474993001 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Isopropylbenzene (Cumene)ND ug/L 04/30/20 16:17 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 04/30/20 16:17 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 04/30/20 16:17 1634-04-40.50 0.44 1
Naphthalene ND ug/L 04/30/20 16:17 91-20-32.0 0.66 1
n-Propylbenzene 0.47J ug/L 04/30/20 16:17 103-65-10.50 0.24 1
Styrene ND ug/L 04/30/20 16:17 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/30/20 16:17 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane ND ug/L 04/30/20 16:17 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 04/30/20 16:17 127-18-40.50 0.23 1
Toluene ND ug/L 04/30/20 16:17 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 04/30/20 16:17 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 04/30/20 16:17 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 04/30/20 16:17 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 04/30/20 16:17 79-00-50.50 0.23 1
Trichloroethene ND ug/L 04/30/20 16:17 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 04/30/20 16:17 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 04/30/20 16:17 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 04/30/20 16:17 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 04/30/20 16:17 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 04/30/20 16:17 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 04/30/20 16:17 179601-23-11.0 0.44 1
o-Xylene ND ug/L 04/30/20 16:17 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %04/30/20 16:17 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %04/30/20 16:17 460-00-470-130 1
Toluene-d8 (S)101 %04/30/20 16:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-2 Lab ID:92474993002 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 05/04/20 14:08 L2,N205/01/20 13:4396.2 96.2 1
Aliphatic (C19-C36)ND ug/L 05/04/20 14:08 L2,N205/01/20 13:4396.2 96.2 1
Aromatic (C11-C22)ND ug/L 05/04/20 14:08 N205/01/20 13:4396.2 96.2 1
Surrogates
Nonatriacontane (S)56 %05/04/20 14:08 7194-86-7 P205/01/20 13:4340-140 1
o-Terphenyl (S)70 %05/04/20 14:08 84-15-105/01/20 13:4340-140 1
2-Fluorobiphenyl (S)98 %05/04/20 14:08 321-60-805/01/20 13:4340-140 1
2-Bromonaphthalene (S)97 %05/04/20 14:08 580-13-205/01/20 13:4340-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)44.8J ug/L 04/26/20 16:25 J04/26/20 16:2510033.3 1
Aliphatic (C09-C12)37.3J ug/L 04/26/20 16:25 J04/26/20 16:2510033.3 1
Aromatic (C09-C10),Unadjusted ND ug/L 04/26/20 16:25 TPHC9C10A04/26/20 16:2510033.3 1
Surrogates
2,5-Dibromotoluene (FID)93.1 %04/26/20 16:25 615-59-8FID04/26/20 16:2570.0-130 1
2,5-Dibromotoluene (PID)85.5 %04/26/20 16:25 615-59-8PID04/26/20 16:2570.0-130 1
Analytical Method: EPA 6010D Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICP) 6010D
Chromium 89.1 ug/L 05/03/20 18:45 7440-47-305/01/20 11:0810.0 5.00 1
Lead 20.0 ug/L 05/03/20 18:45 7439-92-105/01/20 11:086.00 2.95 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 04/30/20 21:20 83-32-904/24/20 17:015.0 1.4 1
Acenaphthylene ND ug/L 04/30/20 21:20 208-96-804/24/20 17:015.0 1.5 1
Anthracene ND ug/L 04/30/20 21:20 120-12-704/24/20 17:015.0 1.6 1
Benzo(a)anthracene ND ug/L 04/30/20 21:20 56-55-304/24/20 17:015.0 1.5 1
Benzo(a)pyrene ND ug/L 04/30/20 21:20 50-32-804/24/20 17:015.0 1.8 1
Benzo(b)fluoranthene ND ug/L 04/30/20 21:20 205-99-204/24/20 17:015.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 04/30/20 21:20 191-24-204/24/20 17:015.0 1.6 1
Benzo(k)fluoranthene ND ug/L 04/30/20 21:20 207-08-904/24/20 17:015.0 1.5 1
4-Bromophenylphenyl ether ND ug/L 04/30/20 21:20 101-55-304/24/20 17:015.0 1.2 1
Butylbenzylphthalate ND ug/L 04/30/20 21:20 85-68-704/24/20 17:015.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 04/30/20 21:20 59-50-704/24/20 17:015.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 04/30/20 21:20 111-91-104/24/20 17:0110.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 04/30/20 21:20 111-44-404/24/20 17:015.0 1.7 1
2-Chloronaphthalene ND ug/L 04/30/20 21:20 91-58-7 L204/24/20 17:015.0 1.4 1
2-Chlorophenol ND ug/L 04/30/20 21:20 95-57-804/24/20 17:015.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 04/30/20 21:20 7005-72-304/24/20 17:015.0 1.5 1
Chrysene ND ug/L 04/30/20 21:20 218-01-904/24/20 17:015.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 04/30/20 21:20 53-70-304/24/20 17:015.0 1.6 1
3,3'-Dichlorobenzidine ND ug/L 04/30/20 21:20 91-94-104/24/20 17:0110.0 2.7 1
2,4-Dichlorophenol ND ug/L 04/30/20 21:20 120-83-204/24/20 17:015.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-2 Lab ID:92474993002 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Diethylphthalate ND ug/L 04/30/20 21:20 84-66-204/24/20 17:015.0 1.6 1
2,4-Dimethylphenol ND ug/L 04/30/20 21:20 105-67-904/24/20 17:0110.0 1.5 1
Dimethylphthalate ND ug/L 04/30/20 21:20 131-11-304/24/20 17:015.0 1.4 1
Di-n-butylphthalate ND ug/L 04/30/20 21:20 84-74-204/24/20 17:015.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 04/30/20 21:20 534-52-104/24/20 17:0110.0 4.5 1
2,4-Dinitrophenol ND ug/L 04/30/20 21:20 51-28-504/24/20 17:0150.0 7.3 1
2,4-Dinitrotoluene ND ug/L 04/30/20 21:20 121-14-204/24/20 17:015.0 1.7 1
2,6-Dinitrotoluene ND ug/L 04/30/20 21:20 606-20-204/24/20 17:015.0 1.7 1
Di-n-octylphthalate ND ug/L 04/30/20 21:20 117-84-004/24/20 17:015.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/30/20 21:20 117-81-704/24/20 17:015.0 2.0 1
Fluoranthene ND ug/L 04/30/20 21:20 206-44-004/24/20 17:015.0 1.6 1
Fluorene ND ug/L 04/30/20 21:20 86-73-704/24/20 17:015.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 04/30/20 21:20 87-68-304/24/20 17:015.0 1.6 1
Hexachlorobenzene ND ug/L 04/30/20 21:20 118-74-104/24/20 17:015.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 04/30/20 21:20 77-47-404/24/20 17:0110.0 2.4 1
Hexachloroethane ND ug/L 04/30/20 21:20 67-72-104/24/20 17:015.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/30/20 21:20 193-39-504/24/20 17:015.0 1.7 1
Isophorone ND ug/L 04/30/20 21:20 78-59-104/24/20 17:0110.0 1.3 1
Naphthalene ND ug/L 04/30/20 21:20 91-20-304/24/20 17:015.0 1.6 1
Nitrobenzene ND ug/L 04/30/20 21:20 98-95-304/24/20 17:015.0 1.5 1
2-Nitrophenol ND ug/L 04/30/20 21:20 88-75-504/24/20 17:015.0 1.7 1
4-Nitrophenol ND ug/L 04/30/20 21:20 100-02-704/24/20 17:0110.0 9.4 1
N-Nitrosodimethylamine ND ug/L 04/30/20 21:20 62-75-904/24/20 17:015.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 04/30/20 21:20 621-64-704/24/20 17:015.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 04/30/20 21:20 86-30-604/24/20 17:0110.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/30/20 21:20 108-60-104/24/20 17:015.0 1.3 1
Pentachlorophenol ND ug/L 04/30/20 21:20 87-86-504/24/20 17:0110.0 2.8 1
Phenanthrene ND ug/L 04/30/20 21:20 85-01-804/24/20 17:015.0 1.4 1
Phenol ND ug/L 04/30/20 21:20 108-95-204/24/20 17:015.0 1.5 1
Pyrene ND ug/L 04/30/20 21:20 129-00-004/24/20 17:015.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 04/30/20 21:20 120-82-104/24/20 17:015.0 1.6 1
2,4,6-Trichlorophenol ND ug/L 04/30/20 21:20 88-06-204/24/20 17:0110.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)51 %04/30/20 21:20 4165-60-004/24/20 17:0110-120 1
2-Fluorobiphenyl (S)43 %04/30/20 21:20 321-60-804/24/20 17:0115-120 1
Terphenyl-d14 (S)67 %04/30/20 21:20 1718-51-004/24/20 17:0111-131 1
Phenol-d6 (S)28 %04/30/20 21:20 13127-88-304/24/20 17:0110-120 1
2-Fluorophenol (S)36 %04/30/20 21:20 367-12-404/24/20 17:0110-120 1
2,4,6-Tribromophenol (S)42 %04/30/20 21:20 118-79-604/24/20 17:0110-137 1
Tentatively Identified Compounds
Unknown 7.3J ug/L 04/30/20 21:2004/24/20 17:011
Ethanol, 2-butoxy-45.7J ug/L 04/30/20 21:20 111-76-2 N04/24/20 17:011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Sample:MW-2 Lab ID:92474993002 Collected:04/23/20 00:00 Received:04/24/20 09:54 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
602 Volatiles by Method 6200
Benzene ND ug/L 04/30/20 02:03 71-43-21.0 0.24 1
Chlorobenzene ND ug/L 04/30/20 02:03 108-90-71.0 0.22 1
1,2-Dichlorobenzene ND ug/L 04/30/20 02:03 95-50-11.0 0.24 1
1,3-Dichlorobenzene ND ug/L 04/30/20 02:03 541-73-11.0 0.25 1
1,4-Dichlorobenzene ND ug/L 04/30/20 02:03 106-46-71.0 0.25 1
Diisopropyl ether ND ug/L 04/30/20 02:03 108-20-31.0 0.33 1
Ethylbenzene ND ug/L 04/30/20 02:03 100-41-41.0 0.24 1
Isopropylbenzene (Cumene)ND ug/L 04/30/20 02:03 98-82-81.0 0.24 1
Methyl-tert-butyl ether ND ug/L 04/30/20 02:03 1634-04-41.0 0.44 1
Naphthalene ND ug/L 04/30/20 02:03 91-20-32.0 0.66 1
Toluene ND ug/L 04/30/20 02:03 108-88-31.0 0.23 1
m&p-Xylene ND ug/L 04/30/20 02:03 179601-23-12.0 0.44 1
o-Xylene ND ug/L 04/30/20 02:03 95-47-61.0 0.24 1
Surrogates
4-Bromofluorobenzene (S)102 %04/30/20 02:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %04/30/20 02:03 17060-07-070-130 1
Toluene-d8 (S)104 %04/30/20 02:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1466497
MADEPV
MADEP VPH
MADEPV
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92474993001, 92474993002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3522712-3
Associated Lab Samples:92474993001, 92474993002
Matrix:Water
AnalyzedMDL
Aliphatic (C05-C08)ug/L ND 100 04/26/20 12:0733.3
Aliphatic (C09-C12)ug/L ND 100 04/26/20 12:0733.3
Aromatic (C09-C10),Unadjusted ug/L ND 100 04/26/20 12:0733.3
2,5-Dibromotoluene (FID)%83.8 70.0-130 04/26/20 12:07
2,5-Dibromotoluene (PID)%76.5 70.0-130 04/26/20 12:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3522712-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3522712-2
Aliphatic (C05-C08)ug/L 13701200 114 70.0-1301131360 0.733 25
Aliphatic (C09-C12)ug/L 16701400 119 70.0-1301171640 1.81 25
Aromatic (C09-C10),Unadjusted ug/L 234200 117 70.0-130117234 0.00 25
2,5-Dibromotoluene (FID)%97.5 70.0-13098.2
2,5-Dibromotoluene (PID)%88.0 70.0-13088.9
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3522712-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1212534-03
R3522712-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aliphatic (C05-C08)ug/L 1200 103 70.0-13095.4 7.29 25120045.5 1280 1190
Aliphatic (C09-C12)ug/L 1400 117 70.0-130110 6.13 25140039.0 1680 1580
Aromatic (C09-
C10),Unadjusted ug/L 200 117 70.0-130113 3.48 25200ND234226
2,5-Dibromotoluene (FID)%97.3 70.0-13097.9
2,5-Dibromotoluene (PID)%88.1 70.0-13089.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1469075
3015
EPA 6010D
Metals (ICP) 6010D
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92474993001, 92474993002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3524340-1
Associated Lab Samples:92474993001, 92474993002
Matrix:Water
AnalyzedMDL
Chromium ug/L ND 10.0 05/03/20 17:335.00
Lead ug/L ND 6.00 05/03/20 17:332.95
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3524340-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium ug/L 9621000 96.2 80.0-120
Lead ug/L 9541000 95.4 80.0-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
538896
SM 6200B
SM 6200B
602 by 6200B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474993002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2872916
Associated Lab Samples:92474993002
Matrix:Water
AnalyzedMDL
1,2-Dichlorobenzene ug/L ND 1.0 04/29/20 19:280.24
1,3-Dichlorobenzene ug/L ND 1.0 04/29/20 19:280.25
1,4-Dichlorobenzene ug/L ND 1.0 04/29/20 19:280.25
Benzene ug/L ND 1.0 04/29/20 19:280.24
Chlorobenzene ug/L ND 1.0 04/29/20 19:280.22
Diisopropyl ether ug/L ND 1.0 04/29/20 19:280.33
Ethylbenzene ug/L ND 1.0 04/29/20 19:280.24
Isopropylbenzene (Cumene)ug/L ND 1.0 04/29/20 19:280.24
m&p-Xylene ug/L ND 2.0 04/29/20 19:280.44
Methyl-tert-butyl ether ug/L ND 1.0 04/29/20 19:280.44
Naphthalene ug/L ND 2.0 04/29/20 19:280.66
o-Xylene ug/L ND 1.0 04/29/20 19:280.24
Toluene ug/L ND 1.0 04/29/20 19:280.23
1,2-Dichloroethane-d4 (S)%98 70-130 04/29/20 19:28
4-Bromofluorobenzene (S)%101 70-130 04/29/20 19:28
Toluene-d8 (S)%104 70-130 04/29/20 19:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2872917LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/L 49.550 99 60-140
1,3-Dichlorobenzene ug/L 49.750 99 60-140
1,4-Dichlorobenzene ug/L 49.850 100 60-140
Benzene ug/L 50.250 100 60-140
Chlorobenzene ug/L 50.050 100 60-140
Diisopropyl ether ug/L 52.950 106 60-140
Ethylbenzene ug/L 46.750 93 60-140
Isopropylbenzene (Cumene)ug/L 50.450 101 60-140
m&p-Xylene ug/L 94.0100 94 60-140
Methyl-tert-butyl ether ug/L 55.850 112 60-140
Naphthalene ug/L 52.450 105 60-140
o-Xylene ug/L 49.650 99 60-140
Toluene ug/L 42.950 86 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2872918MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92475115008
2872919
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dichlorobenzene ug/L 20 103 60-140100 2 3020ND20.5 20.1
1,3-Dichlorobenzene ug/L 20 103 60-140102 1 3020ND20.7 20.4
1,4-Dichlorobenzene ug/L 20 103 60-140102 1 3020ND20.6 20.4
Benzene ug/L 20 106 60-140105 0 3020ND21.1 21.1
Chlorobenzene ug/L 20 104 60-140102 2 3020ND20.8 20.4
Diisopropyl ether ug/L 20 104 60-140101 2 3020ND20.7 20.2
Ethylbenzene ug/L 20 100 60-140100 1 3020ND20.1 19.9
Isopropylbenzene
(Cumene)ug/L 20 107 60-140106 1 3020ND21.4 21.2
m&p-Xylene ug/L 40 99 60-14099 0 3040ND39.6 39.6
Methyl-tert-butyl ether ug/L 20 108 60-140106 2 3020ND21.6 21.2
Naphthalene ug/L 20 104 60-140104 0 3020ND20.8 20.7
o-Xylene ug/L 20 102 60-140102 0 3020ND20.5 20.4
Toluene ug/L 20 93 60-14091 1 3020ND18.6 18.3
1,2-Dichloroethane-d4 (S)%103 70-130103
4-Bromofluorobenzene (S)%101 70-130104
Toluene-d8 (S)%95 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
538601
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474993001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2871603
Associated Lab Samples:92474993001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/30/20 15:410.42
1,1,1-Trichloroethane ug/L ND 0.50 04/30/20 15:410.28
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/30/20 15:410.19
1,1,2-Trichloroethane ug/L ND 0.50 04/30/20 15:410.23
1,1-Dichloroethane ug/L ND 0.50 04/30/20 15:410.24
1,1-Dichloroethene ug/L ND 0.50 04/30/20 15:410.22
1,1-Dichloropropene ug/L ND 0.50 04/30/20 15:410.35
1,2,3-Trichlorobenzene ug/L ND 2.0 04/30/20 15:410.78
1,2,3-Trichloropropane ug/L ND 0.50 04/30/20 15:410.27
1,2,4-Trichlorobenzene ug/L ND 2.0 04/30/20 15:410.44
1,2,4-Trimethylbenzene ug/L ND 0.50 04/30/20 15:410.19
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/30/20 15:410.38
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/30/20 15:410.23
1,2-Dichlorobenzene ug/L ND 0.50 04/30/20 15:410.24
1,2-Dichloroethane ug/L ND 0.50 04/30/20 15:410.26
1,2-Dichloropropane ug/L ND 0.50 04/30/20 15:410.18
1,3,5-Trimethylbenzene ug/L ND 0.50 04/30/20 15:410.23
1,3-Dichlorobenzene ug/L ND 0.50 04/30/20 15:410.25
1,3-Dichloropropane ug/L ND 0.50 04/30/20 15:410.34
1,4-Dichlorobenzene ug/L ND 0.50 04/30/20 15:410.25
2,2-Dichloropropane ug/L ND 0.50 04/30/20 15:410.28
2-Chlorotoluene ug/L ND 0.50 04/30/20 15:410.21
4-Chlorotoluene ug/L ND 0.50 04/30/20 15:410.21
Benzene ug/L ND 0.50 04/30/20 15:410.24
Bromobenzene ug/L ND 0.50 04/30/20 15:410.22
Bromochloromethane ug/L ND 0.50 04/30/20 15:410.26
Bromodichloromethane ug/L ND 0.50 04/30/20 15:410.18
Bromoform ug/L ND 0.50 04/30/20 15:410.40
Bromomethane ug/L ND 5.0 04/30/20 15:411.7
Carbon tetrachloride ug/L ND 0.50 04/30/20 15:410.23
Chlorobenzene ug/L ND 0.50 04/30/20 15:410.22
Chloroethane ug/L ND 1.0 04/30/20 15:410.58
Chloroform ug/L ND 0.50 04/30/20 15:410.35
Chloromethane ug/L ND 1.0 04/30/20 15:410.42
cis-1,2-Dichloroethene ug/L ND 0.50 04/30/20 15:410.21
cis-1,3-Dichloropropene ug/L ND 0.50 04/30/20 15:410.36
Dibromochloromethane ug/L ND 0.50 04/30/20 15:410.40
Dibromomethane ug/L ND 0.50 04/30/20 15:410.31
Dichlorodifluoromethane ug/L ND 0.50 04/30/20 15:410.28
Diisopropyl ether ug/L ND 0.50 04/30/20 15:410.33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2871603
Associated Lab Samples:92474993001
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 04/30/20 15:410.24
Hexachloro-1,3-butadiene ug/L ND 2.0 04/30/20 15:411.2
Isopropylbenzene (Cumene)ug/L ND 0.50 04/30/20 15:410.24
m&p-Xylene ug/L ND 1.0 04/30/20 15:410.44
Methyl-tert-butyl ether ug/L ND 0.50 04/30/20 15:410.44
Methylene Chloride ug/L ND 2.0 04/30/20 15:411.5
n-Butylbenzene ug/L ND 0.50 04/30/20 15:410.35
n-Propylbenzene ug/L ND 0.50 04/30/20 15:410.24
Naphthalene ug/L ND 2.0 04/30/20 15:410.66
o-Xylene ug/L ND 0.50 04/30/20 15:410.24
sec-Butylbenzene ug/L ND 0.50 04/30/20 15:410.25
Styrene ug/L ND 0.50 04/30/20 15:410.26
tert-Butylbenzene ug/L ND 0.50 04/30/20 15:410.25
Tetrachloroethene ug/L ND 0.50 04/30/20 15:410.23
Toluene ug/L ND 0.50 04/30/20 15:410.23
trans-1,2-Dichloroethene ug/L ND 0.50 04/30/20 15:410.26
trans-1,3-Dichloropropene ug/L ND 0.50 04/30/20 15:410.39
Trichloroethene ug/L ND 0.50 04/30/20 15:410.23
Trichlorofluoromethane ug/L ND 1.0 04/30/20 15:410.34
Vinyl chloride ug/L ND 1.0 04/30/20 15:410.41
1,2-Dichloroethane-d4 (S)%99 70-130 04/30/20 15:41
4-Bromofluorobenzene (S)%100 70-130 04/30/20 15:41
Toluene-d8 (S)%104 70-130 04/30/20 15:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2871604LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.350 109 60-140
1,1,1-Trichloroethane ug/L 50.150 100 60-140
1,1,2,2-Tetrachloroethane ug/L 51.750 103 60-140
1,1,2-Trichloroethane ug/L 56.150 112 60-140
1,1-Dichloroethane ug/L 45.950 92 60-140
1,1-Dichloroethene ug/L 48.750 97 60-140
1,1-Dichloropropene ug/L 47.050 94 60-140
1,2,3-Trichlorobenzene ug/L 51.650 103 60-140
1,2,3-Trichloropropane ug/L 54.550 109 60-140
1,2,4-Trichlorobenzene ug/L 52.050 104 60-140
1,2,4-Trimethylbenzene ug/L 47.550 95 60-140
1,2-Dibromo-3-chloropropane ug/L 53.050 106 60-140
1,2-Dibromoethane (EDB)ug/L 50.250 100 60-140
1,2-Dichlorobenzene ug/L 50.150 100 60-140
1,2-Dichloroethane ug/L 46.450 93 60-140
1,2-Dichloropropane ug/L 47.450 95 60-140
1,3,5-Trimethylbenzene ug/L 51.050 102 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2871604LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 49.750 99 60-140
1,3-Dichloropropane ug/L 52.750 105 60-140
1,4-Dichlorobenzene ug/L 49.650 99 60-140
2,2-Dichloropropane ug/L 50.050 100 60-140
2-Chlorotoluene ug/L 49.150 98 60-140
4-Chlorotoluene ug/L 50.250 100 60-140
Benzene ug/L 49.250 98 60-140
Bromobenzene ug/L 51.050 102 60-140
Bromochloromethane ug/L 48.650 97 60-140
Bromodichloromethane ug/L 52.650 105 60-140
Bromoform ug/L 47.350 95 60-140
Bromomethane ug/L 61.950 124 60-140
Carbon tetrachloride ug/L 52.550 105 60-140
Chlorobenzene ug/L 49.350 99 60-140
Chloroethane ug/L 46.450 93 60-140
Chloroform ug/L 48.250 96 60-140
Chloromethane ug/L 44.150 88 60-140
cis-1,2-Dichloroethene ug/L 47.650 95 60-140
cis-1,3-Dichloropropene ug/L 46.950 94 60-140
Dibromochloromethane ug/L 48.350 97 60-140
Dibromomethane ug/L 50.050 100 60-140
Dichlorodifluoromethane ug/L 52.850 106 60-140
Diisopropyl ether ug/L 54.350 109 60-140
Ethylbenzene ug/L 46.550 93 60-140
Hexachloro-1,3-butadiene ug/L 50.950 102 60-140
Isopropylbenzene (Cumene)ug/L 49.150 98 60-140
m&p-Xylene ug/L 93.3100 93 60-140
Methyl-tert-butyl ether ug/L 56.650 113 60-140
Methylene Chloride ug/L 45.950 92 60-140
n-Butylbenzene ug/L 51.750 103 60-140
n-Propylbenzene ug/L 46.150 92 60-140
Naphthalene ug/L 54.550 109 60-140
o-Xylene ug/L 47.150 94 60-140
sec-Butylbenzene ug/L 48.150 96 60-140
Styrene ug/L 51.550 103 60-140
tert-Butylbenzene ug/L 41.750 83 60-140
Tetrachloroethene ug/L 51.150 102 60-140
Toluene ug/L 43.950 88 60-140
trans-1,2-Dichloroethene ug/L 48.050 96 60-140
trans-1,3-Dichloropropene ug/L 54.350 109 60-140
Trichloroethene ug/L 47.450 95 60-140
Trichlorofluoromethane ug/L 47.350 95 60-140
Vinyl chloride ug/L 55.950 112 60-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2873852MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92474993001
2873853
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 106 60-140107 1 3020ND21.3 21.4
1,1,1-Trichloroethane ug/L 20 115 60-140111 3 3020ND22.9 22.2
1,1,2,2-Tetrachloroethane ug/L 20 111 60-140111 0 3020ND22.2 22.2
1,1,2-Trichloroethane ug/L 20 112 60-140109 3 3020ND22.4 21.8
1,1-Dichloroethane ug/L 20 106 60-140102 4 3020ND21.2 20.3
1,1-Dichloroethene ug/L 20 112 60-140109 3 3020ND22.5 21.9
1,1-Dichloropropene ug/L 20 103 60-140100 3 3020ND20.7 20.0
1,2,3-Trichlorobenzene ug/L 20 114 60-140113 0 3020ND22.8 22.7
1,2,3-Trichloropropane ug/L 20 105 60-140107 2 3020ND21.0 21.4
1,2,4-Trichlorobenzene ug/L 20 114 60-140114 0 3020ND22.8 22.7
1,2,4-Trimethylbenzene ug/L 20 98 60-140101 3 3020ND19.5 20.2
1,2-Dibromo-3-
chloropropane ug/L 20 110 60-140110 0 3020ND21.9 21.9
1,2-Dibromoethane (EDB)ug/L 20 102 60-140102 0 3020ND20.3 20.3
1,2-Dichlorobenzene ug/L 20 103 60-140107 3 3020ND20.6 21.3
1,2-Dichloroethane ug/L 20 101 60-14099 2 3020ND20.2 19.8
1,2-Dichloropropane ug/L 20 104 60-140102 2 3020ND20.8 20.4
1,3,5-Trimethylbenzene ug/L 20 105 60-140106 1 3020ND21.1 21.2
1,3-Dichlorobenzene ug/L 20 103 60-140104 1 3020ND20.7 20.9
1,3-Dichloropropane ug/L 20 106 60-140106 1 3020ND21.3 21.2
1,4-Dichlorobenzene ug/L 20 103 60-140102 1 3020ND20.5 20.3
2,2-Dichloropropane ug/L 20 103 60-14099 3 3020ND20.5 19.9
2-Chlorotoluene ug/L 20 102 60-140104 3 3020ND20.3 20.9
4-Chlorotoluene ug/L 20 102 60-140104 2 3020ND20.5 20.8
Benzene ug/L 20 109 60-140107 2 3020ND21.8 21.3
Bromobenzene ug/L 20 105 60-140106 1 3020ND20.9 21.2
Bromochloromethane ug/L 20 109 60-140105 4 3020ND21.9 21.0
Bromodichloromethane ug/L 20 112 60-140110 2 3020ND22.4 22.0
Bromoform ug/L 20 96 60-14090 6 3020ND19.2 18.1
Bromomethane ug/L 20 134 60-140127 5 3020ND26.9 25.5
Carbon tetrachloride ug/L 20 121 60-140120 1 3020ND24.2 23.9
Chlorobenzene ug/L 20 105 60-140104 0 3020ND20.9 20.9
Chloroethane ug/L 20 114 60-140111 3 3020ND22.8 22.2
Chloroform ug/L 20 109 60-140109 0 3020ND21.8 21.8
Chloromethane ug/L 20 106 60-14098 7 3020ND21.2 19.7
cis-1,2-Dichloroethene ug/L 20 109 60-140106 3 3020ND21.9 21.2
cis-1,3-Dichloropropene ug/L 20 88 60-14086 2 3020ND17.7 17.3
Dibromochloromethane ug/L 20 94 60-14095 1 3020ND18.8 19.1
Dibromomethane ug/L 20 108 60-140105 3 3020ND21.6 21.0
Dichlorodifluoromethane ug/L 20 119 60-140113 5 3020ND23.9 22.7
Diisopropyl ether ug/L 20 103 60-14099 4 3020ND20.6 19.8
Ethylbenzene ug/L 20 98 60-14098 0 3020ND19.6 19.7
Hexachloro-1,3-butadiene ug/L 20 113 60-140109 3 3020ND22.6 21.9
Isopropylbenzene(Cumene)ug/L 20 105 60-140108 3 3020ND21.0 21.6
m&p-Xylene ug/L 40 100 60-14097 2 3040ND39.8 39.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2873852MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92474993001
2873853
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 109 60-140107 2 3020ND21.8 21.4
Methylene Chloride ug/L 20 105 60-14098 6 3020ND20.9 19.6
n-Butylbenzene ug/L 20 115 60-140114 1 3020ND22.9 22.8
n-Propylbenzene ug/L 20 97 60-14099 3 30200.47J 19.8 20.3
Naphthalene ug/L 20 127 60-140133 4 3020ND25.4 26.5
o-Xylene ug/L 20 101 60-140102 1 3020ND20.2 20.4
sec-Butylbenzene ug/L 20 103 60-140103 0 30201.6 22.2 22.3
Styrene ug/L 20 108 60-140107 1 3020ND21.7 21.4
tert-Butylbenzene ug/L 20 87 60-14088 1 3020ND17.5 17.7
Tetrachloroethene ug/L 20 105 60-140105 0 3020ND21.0 21.1
Toluene ug/L 20 96 60-14090 5 3020ND19.1 18.1
trans-1,2-Dichloroethene ug/L 20 108 60-140105 3 3020ND21.7 21.1
trans-1,3-Dichloropropene ug/L 20 107 60-140100 7 3020ND21.3 19.9
Trichloroethene ug/L 20 103 60-140102 1 3020ND20.6 20.4
Trichlorofluoromethane ug/L 20 111 60-140108 3 3020ND22.1 21.5
Vinyl chloride ug/L 20 132 60-140127 4 3020ND26.4 25.4
1,2-Dichloroethane-d4 (S)%104 70-130100
4-Bromofluorobenzene (S)%102 70-130101
Toluene-d8 (S)%99 70-13096
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
538113
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474993001, 92474993002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2869500
Associated Lab Samples:92474993001, 92474993002
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 5.0 04/29/20 00:431.6
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 04/29/20 00:431.3
2,4,6-Trichlorophenol ug/L ND 10.0 04/29/20 00:431.4
2,4-Dichlorophenol ug/L ND 5.0 04/29/20 00:431.5
2,4-Dimethylphenol ug/L ND 10.0 04/29/20 00:431.5
2,4-Dinitrophenol ug/L ND 50.0 04/29/20 00:437.3
2,4-Dinitrotoluene ug/L ND 5.0 04/29/20 00:431.7
2,6-Dinitrotoluene ug/L ND 5.0 04/29/20 00:431.7
2-Chloronaphthalene ug/L ND 5.0 04/29/20 00:431.4
2-Chlorophenol ug/L ND 5.0 04/29/20 00:431.4
2-Nitrophenol ug/L ND 5.0 04/29/20 00:431.7
3,3'-Dichlorobenzidine ug/L ND 10.0 04/29/20 00:432.7
4,6-Dinitro-2-methylphenol ug/L ND 10.0 04/29/20 00:434.5
4-Bromophenylphenyl ether ug/L ND 5.0 04/29/20 00:431.2
4-Chloro-3-methylphenol ug/L ND 5.0 04/29/20 00:432.8
4-Chlorophenylphenyl ether ug/L ND 5.0 04/29/20 00:431.5
4-Nitrophenol ug/L ND 10.0 04/29/20 00:439.4
Acenaphthene ug/L ND 5.0 04/29/20 00:431.4
Acenaphthylene ug/L ND 5.0 04/29/20 00:431.5
Anthracene ug/L ND 5.0 04/29/20 00:431.6
Benzo(a)anthracene ug/L ND 5.0 04/29/20 00:431.5
Benzo(a)pyrene ug/L ND 5.0 04/29/20 00:431.8
Benzo(b)fluoranthene ug/L ND 5.0 04/29/20 00:431.7
Benzo(g,h,i)perylene ug/L ND 5.0 04/29/20 00:431.6
Benzo(k)fluoranthene ug/L ND 5.0 04/29/20 00:431.5
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/29/20 00:431.3
bis(2-Chloroethyl) ether ug/L ND 5.0 04/29/20 00:431.7
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/29/20 00:432.0
Butylbenzylphthalate ug/L ND 5.0 04/29/20 00:431.9
Chrysene ug/L ND 5.0 04/29/20 00:431.4
Di-n-butylphthalate ug/L ND 5.0 04/29/20 00:431.6
Di-n-octylphthalate ug/L ND 5.0 04/29/20 00:432.2
Dibenz(a,h)anthracene ug/L ND 5.0 04/29/20 00:431.6
Diethylphthalate ug/L ND 5.0 04/29/20 00:431.6
Dimethylphthalate ug/L ND 5.0 04/29/20 00:431.4
Fluoranthene ug/L ND 5.0 04/29/20 00:431.6
Fluorene ug/L ND 5.0 04/29/20 00:431.4
Hexachloro-1,3-butadiene ug/L ND 5.0 04/29/20 00:431.6
Hexachlorobenzene ug/L ND 5.0 04/29/20 00:431.3
Hexachlorocyclopentadiene ug/L ND 10.0 04/29/20 00:432.4
REPORT OF LABORATORY ANALYSIS
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Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2869500
Associated Lab Samples:92474993001, 92474993002
Matrix:Water
AnalyzedMDL
Hexachloroethane ug/L ND 5.0 04/29/20 00:431.3
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 04/29/20 00:431.7
Isophorone ug/L ND 10.0 04/29/20 00:431.3
N-Nitroso-di-n-propylamine ug/L ND 5.0 04/29/20 00:431.3
N-Nitrosodimethylamine ug/L ND 5.0 04/29/20 00:431.8
N-Nitrosodiphenylamine ug/L ND 10.0 04/29/20 00:431.4
Naphthalene ug/L ND 5.0 04/29/20 00:431.6
Nitrobenzene ug/L ND 5.0 04/29/20 00:431.5
Pentachlorophenol ug/L ND 10.0 04/29/20 00:432.8
Phenanthrene ug/L ND 5.0 04/29/20 00:431.4
Phenol ug/L ND 5.0 04/29/20 00:431.5
Pyrene ug/L ND 5.0 04/29/20 00:431.5
2,4,6-Tribromophenol (S)%65 10-137 04/29/20 00:43
2-Fluorobiphenyl (S)%59 15-120 04/29/20 00:43
2-Fluorophenol (S)%52 10-120 04/29/20 00:43
Nitrobenzene-d5 (S)%69 10-120 04/29/20 00:43
Phenol-d6 (S)%40 10-120 04/29/20 00:43
Terphenyl-d14 (S)%99 11-131 04/29/20 00:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2869501LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 24.250 48 44-142
2,2'-Oxybis(1-chloropropane)ug/L 45.250 90 36-166
2,4,6-Trichlorophenol ug/L 31.650 63 37-144
2,4-Dichlorophenol ug/L 33.750 67 1-191
2,4-Dimethylphenol ug/L 34.350 69 32-119
2,4-Dinitrophenol ug/L 155250 62 1-181
2,4-Dinitrotoluene ug/L 43.850 88 39-139
2,6-Dinitrotoluene ug/L 40.050 80 50-158
2-Chloronaphthalene ug/L 28.5 L2505760-118
2-Chlorophenol ug/L 34.350 69 23-134
2-Nitrophenol ug/L 37.650 75 29-182
3,3'-Dichlorobenzidine ug/L 76.2100 76 1-262
4,6-Dinitro-2-methylphenol ug/L 75.0100 75 1-181
4-Bromophenylphenyl ether ug/L 31.550 63 53-127
4-Chloro-3-methylphenol ug/L 72.4100 72 22-147
4-Chlorophenylphenyl ether ug/L 30.150 60 25-158
4-Nitrophenol ug/L 99.5250 40 1-132
Acenaphthene ug/L 32.150 64 47-145
Acenaphthylene ug/L 34.050 68 33-145
Anthracene ug/L 38.150 76 1-166
Benzo(a)anthracene ug/L 41.950 84 33-143
Benzo(a)pyrene ug/L 43.750 87 17-163
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
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Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2869501LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 42.050 84 24-159
Benzo(g,h,i)perylene ug/L 45.650 91 1-219
Benzo(k)fluoranthene ug/L 43.950 88 11-162
bis(2-Chloroethoxy)methane ug/L 35.850 72 33-184
bis(2-Chloroethyl) ether ug/L 36.650 73 12-158
bis(2-Ethylhexyl)phthalate ug/L 46.150 92 8-158
Butylbenzylphthalate ug/L 46.050 92 1-152
Chrysene ug/L 42.650 85 17-168
Di-n-butylphthalate ug/L 45.050 90 1-118
Di-n-octylphthalate ug/L 49.050 98 4-146
Dibenz(a,h)anthracene ug/L 44.750 89 1-227
Diethylphthalate ug/L 40.750 81 1-114
Dimethylphthalate ug/L 37.150 74 1-112
Fluoranthene ug/L 43.050 86 26-137
Fluorene ug/L 34.250 68 59-121
Hexachloro-1,3-butadiene ug/L 22.550 45 24-116
Hexachlorobenzene ug/L 32.850 66 1-152
Hexachlorocyclopentadiene ug/L 17.650 35 25-150
Hexachloroethane ug/L 25.050 50 40-113
Indeno(1,2,3-cd)pyrene ug/L 44.650 89 1-171
Isophorone ug/L 36.850 74 21-196
N-Nitroso-di-n-propylamine ug/L 35.550 71 1-230
N-Nitrosodimethylamine ug/L 30.350 61 25-150
N-Nitrosodiphenylamine ug/L 37.050 74 25-150
Naphthalene ug/L 29.750 59 21-133
Nitrobenzene ug/L 34.950 70 35-180
Pentachlorophenol ug/L 60.2100 60 14-176
Phenanthrene ug/L 37.850 76 54-120
Phenol ug/L 23.550 47 5-112
Pyrene ug/L 39.950 80 52-115
2,4,6-Tribromophenol (S)%77 10-137
2-Fluorobiphenyl (S)%68 15-120
2-Fluorophenol (S)%57 10-120
Nitrobenzene-d5 (S)%80 10-120
Phenol-d6 (S)%47 10-120
Terphenyl-d14 (S)%100 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2869502MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35544825001
2869503
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 57 44-14247 19 30501.6U 28.4 23.6
2,2'-Oxybis(1-
chloropropane)ug/L 50 109 36-166106 3 30501.3U 54.6 52.8
2,4,6-Trichlorophenol ug/L M1,R1506437-14435 59 30501.4U 32.2 17.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
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Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2869502MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35544825001
2869503
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4-Dichlorophenol ug/L 50 73 1-19164 12 30501.5U 36.4 32.2
2,4-Dimethylphenol ug/L 50 77 32-11977 1 30501.5U 38.7 38.4
2,4-Dinitrophenol ug/L M125081-1810 302507.3U 20.3J ND
2,4-Dinitrotoluene ug/L 50 97 39-13988 10 30501.7U 48.6 44.1
2,6-Dinitrotoluene ug/L 50 91 50-15887 4 30501.7U 45.4 43.6
2-Chloronaphthalene ug/L 50 70 60-11863 10 30501.4U 35.1 31.7
2-Chlorophenol ug/L 50 77 23-13468 13 30501.4U 38.5 33.9
2-Nitrophenol ug/L 50 82 29-18267 20 30501.7U 40.9 33.5
3,3'-Dichlorobenzidine ug/L 100 89 1-26275 17 301002.7U 89.3 75.4
4,6-Dinitro-2-methylphenol ug/L 100 39 1-18110 301004.5U 39.0 9.8J
4-Bromophenylphenyl ether ug/L 50 75 53-12774 2 30501.2U 37.6 36.8
4-Chloro-3-methylphenol ug/L 100 82 22-14780 3 301002.8U 82.2 80.1
4-Chlorophenylphenyl ether ug/L 50 75 25-15873 3 30501.5U 37.7 36.6
4-Nitrophenol ug/L 250 17 1-1324 302509.4U 43.0 ND
Acenaphthene ug/L 50 79 47-14574 7 30501.4U 39.6 37.1
Acenaphthylene ug/L 50 82 33-14576 8 30501.5U 41.0 38.0
Anthracene ug/L 50 88 1-16683 5 30501.6U 43.9 41.7
Benzo(a)anthracene ug/L 50 99 33-14385 15 30501.5U 49.6 42.6
Benzo(a)pyrene ug/L 50 101 17-16387 15 30501.8U 50.5 43.5
Benzo(b)fluoranthene ug/L 50 98 24-15986 13 30501.7U 49.0 42.8
Benzo(g,h,i)perylene ug/L 50 106 1-21990 17 30501.6U 53.0 44.9
Benzo(k)fluoranthene ug/L 50 102 11-16288 15 30501.5U 51.0 43.8
bis(2-
Chloroethoxy)methane ug/L 50 81 33-18481 1 30501.3U 40.6 40.3
bis(2-Chloroethyl) ether ug/L 50 85 12-15888 3 30501.7U 42.6 44.0
bis(2-Ethylhexyl)phthalate ug/L 50 110 8-15893 17 30502.0U 55.1 46.7
Butylbenzylphthalate ug/L 50 111 1-15294 17 30501.9U 55.3 46.8
Chrysene ug/L 50 99 17-16885 15 30501.4U 49.4 42.4
Di-n-butylphthalate ug/L 50 107 1-11891 16 30501.6U 53.6 45.6
Di-n-octylphthalate ug/L 50 118 4-14696 20 30502.2U 59.0 48.1
Dibenz(a,h)anthracene ug/L 50 104 1-22788 17 30501.6U 52.1 43.9
Diethylphthalate ug/L 50 93 1-11486 7 30501.6U 46.4 43.1
Dimethylphthalate ug/L 50 86 1-11282 5 30501.4U 42.8 40.8
Fluoranthene ug/L 50 102 26-13788 15 30501.6U 51.2 44.0
Fluorene ug/L 50 84 59-12180 5 30501.4U 41.8 39.8
Hexachloro-1,3-butadiene ug/L 50 51 24-11643 17 30501.6U 25.6 21.4
Hexachlorobenzene ug/L 50 77 1-15274 3 30501.3U 38.5 37.2
Hexachlorocyclopentadiene ug/L 50 39 25-15032 18 30502.4U 19.4 16.2
Hexachloroethane ug/L 50 61 40-11352 16 30501.3U 30.5 26.0
Indeno(1,2,3-cd)pyrene ug/L 50 104 1-17187 17 30501.7U 52.0 43.7
Isophorone ug/L 50 85 21-19683 3 30501.3U 42.7 41.6
N-Nitroso-di-n-propylamine ug/L 50 84 1-23084 0 30501.3U 42.0 42.2
N-Nitrosodimethylamine ug/L 50 65 25-15068 5 30501.8U 32.5 34.2
N-Nitrosodiphenylamine ug/L 50 83 25-15080 3 30501.4U 41.4 40.0
Naphthalene ug/L 50 70 21-13361 12 30501.6U 34.8 30.7
Nitrobenzene ug/L 50 80 35-18080 1 30501.5U 39.8 40.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
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Page 24 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2869502MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35544825001
2869503
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Pentachlorophenol ug/L M11003614-1767 301002.8U 35.8 6.7J
Phenanthrene ug/L 50 89 54-12083 7 30501.4U 44.4 41.5
Phenol ug/L 50 50 5-11248 6 30501.5U 25.2 23.8
Pyrene ug/L 50 95 52-11585 11 30501.5U 47.3 42.4
2,4,6-Tribromophenol (S)%95 10-13759
2-Fluorobiphenyl (S)%88 15-12083
2-Fluorophenol (S)%63 10-12044
Nitrobenzene-d5 (S)%97 10-12093
Phenol-d6 (S)%52 10-12048
Terphenyl-d14 (S)%126 11-131107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
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Page 25 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
538963
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474993001, 92474993002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2873261
Associated Lab Samples:92474993001, 92474993002
Matrix:Water
AnalyzedMDL
Aliphatic (C09-C18)ug/L ND 100 N205/04/20 08:41100
Aliphatic (C19-C36)ug/L ND 100 N205/04/20 08:41100
Aromatic (C11-C22)ug/L ND 100 N205/04/20 08:41100
2-Bromonaphthalene (S)%91 40-140 05/04/20 08:41
2-Fluorobiphenyl (S)%91 40-140 05/04/20 08:41
Nonatriacontane (S)%54 40-140 05/04/20 08:41
o-Terphenyl (S)%67 40-140 05/04/20 08:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2873262LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2873263
Aliphatic (C09-C18)ug/L ND L2,N23003140-14039116 50
Aliphatic (C19-C36)ug/L 157 L2,N24003940-14043173 10 50
Aromatic (C11-C22)ug/L 588 N28506940-14071607 3 50
2-Bromonaphthalene (S)%89 40-140105
2-Fluorobiphenyl (S)%92 40-140105
Nonatriacontane (S)%46 40-14040
o-Terphenyl (S)%83 40-14086
REPORT OF LABORATORY ANALYSIS
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Page 26 of 31
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The reported TIC has an 85% or higher match on a mass spectral library search.N
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Re-extraction or re-analysis could not be performed due to insufficient sample amount.P2
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
REPORT OF LABORATORY ANALYSIS
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Page 27 of 31
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92474993
Greensboro NC LC 0134 UST Clos
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92474993001 538963 539434MW-1 MADEP EPH MADEP EPH
92474993002 538963 539434MW-2 MADEP EPH MADEP EPH
92474993001 1466497 1466497MW-1 MADEPV MADEP VPH
92474993002 1466497 1466497MW-2 MADEPV MADEP VPH
92474993001 1469075 1469075MW-1 3015 EPA 6010D
92474993002 1469075 1469075MW-2 3015 EPA 6010D
92474993001 538113 538662MW-1 EPA 625.1 EPA 625.1
92474993002 538113 538662MW-2 EPA 625.1 EPA 625.1
92474993002 538896MW-2 SM 6200B
92474993001 538601MW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2020 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 31
Page 29 of 31
Page 30 of 31
Page 31 of 31
#=CL#
June 12, 2020
LIMS USE: FR - BRITNEY BARNES
LIMS OBJECT ID: 92480688
92480688
Project:
Pace Project No.:
RE:
Britney Barnes
Civil & Environmental Consultants
530 Howell Rd
Suite 203
Greenville, SC
Greensboro NC LC 0134 UST Clos
Dear Britney Barnes:
Enclosed are the analytical results for sample(s) received by the laboratory on June 05, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Sarah Galloway, Ryder Systems, Inc
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
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EPA# TN00003
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Georgia Certification: NELAP
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Kentucky Certification #: 90010
Louisiana Certification #: AI30792
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New Mexico DW Certification
New York Certification #: 11742
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Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
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South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
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USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
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Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
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Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Page 2 of 21
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Lab ID Sample ID Matrix Date Collected Date Received
92480688001 MW-1 Water 06/05/20 11:30 06/05/20 14:25
REPORT OF LABORATORY ANALYSIS
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Page 3 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92480688001 MW-1 MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 625.1 67 PASI-CPKS
SM 6200B 16 PASI-CSAS
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Sample:MW-1 Lab ID:92480688001 Collected:06/05/20 11:30 Received:06/05/20 14:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 06/09/20 16:37 L2,N206/08/20 10:021001001
Aliphatic (C19-C36)ND ug/L 06/09/20 16:37 N206/08/20 10:021001001
Aromatic (C11-C22)171 ug/L 06/09/20 16:37 N206/08/20 10:021001001
Surrogates
Nonatriacontane (S)45 %06/09/20 16:37 7194-86-7 1g06/08/20 10:0240-140 1
o-Terphenyl (S)50 %06/09/20 16:37 84-15-106/08/20 10:0240-140 1
2-Fluorobiphenyl (S)123 %06/09/20 16:37 321-60-806/08/20 10:0240-140 1
2-Bromonaphthalene (S)129 %06/09/20 16:37 580-13-206/08/20 10:0240-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND ug/L 06/08/20 14:1306/08/20 14:135001675
Aliphatic (C09-C12)241J ug/L 06/08/20 14:13 J06/08/20 14:135001675
Aromatic (C09-C10),Unadjusted ND ug/L 06/08/20 14:13 TPHC9C10A06/08/20 14:135001675
Surrogates
2,5-Dibromotoluene (FID)95.1 %06/08/20 14:13 615-59-8FID06/08/20 14:1370.0-130 5
2,5-Dibromotoluene (PID)83.9 %06/08/20 14:13 615-59-8PID06/08/20 14:1370.0-130 5
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 06/09/20 19:48 83-32-906/09/20 10:265.0 1.4 1
Acenaphthylene ND ug/L 06/09/20 19:48 208-96-806/09/20 10:265.0 1.5 1
Anthracene ND ug/L 06/09/20 19:48 120-12-706/09/20 10:265.0 1.6 1
Benzo(a)anthracene ND ug/L 06/09/20 19:48 56-55-306/09/20 10:265.0 1.5 1
Benzo(a)pyrene ND ug/L 06/09/20 19:48 50-32-806/09/20 10:265.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/09/20 19:48 205-99-206/09/20 10:265.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/09/20 19:48 191-24-206/09/20 10:265.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/09/20 19:48 207-08-906/09/20 10:265.0 1.5 1
4-Bromophenylphenyl ether ND ug/L 06/09/20 19:48 101-55-306/09/20 10:265.0 1.2 1
Butylbenzylphthalate ND ug/L 06/09/20 19:48 85-68-706/09/20 10:265.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/09/20 19:48 59-50-706/09/20 10:265.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/09/20 19:48 111-91-106/09/20 10:2610.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/09/20 19:48 111-44-406/09/20 10:265.0 1.7 1
2-Chloronaphthalene ND ug/L 06/09/20 19:48 91-58-706/09/20 10:265.0 1.4 1
2-Chlorophenol ND ug/L 06/09/20 19:48 95-57-806/09/20 10:265.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/09/20 19:48 7005-72-306/09/20 10:265.0 1.5 1
Chrysene ND ug/L 06/09/20 19:48 218-01-906/09/20 10:265.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/09/20 19:48 53-70-306/09/20 10:265.0 1.6 1
3,3'-Dichlorobenzidine ND ug/L 06/09/20 19:48 91-94-106/09/20 10:2610.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/09/20 19:48 120-83-206/09/20 10:265.0 1.5 1
Diethylphthalate ND ug/L 06/09/20 19:48 84-66-206/09/20 10:265.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/09/20 19:48 105-67-906/09/20 10:2610.0 1.5 1
Dimethylphthalate ND ug/L 06/09/20 19:48 131-11-306/09/20 10:265.0 1.4 1
Di-n-butylphthalate ND ug/L 06/09/20 19:48 84-74-206/09/20 10:265.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/09/20 19:48 534-52-106/09/20 10:2610.0 4.5 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Sample:MW-1 Lab ID:92480688001 Collected:06/05/20 11:30 Received:06/05/20 14:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
2,4-Dinitrophenol ND ug/L 06/09/20 19:48 51-28-506/09/20 10:2650.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/09/20 19:48 121-14-206/09/20 10:265.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/09/20 19:48 606-20-206/09/20 10:265.0 1.7 1
Di-n-octylphthalate ND ug/L 06/09/20 19:48 117-84-006/09/20 10:265.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/09/20 19:48 117-81-706/09/20 10:265.0 2.0 1
Fluoranthene ND ug/L 06/09/20 19:48 206-44-006/09/20 10:265.0 1.6 1
Fluorene 1.6J ug/L 06/09/20 19:48 86-73-706/09/20 10:265.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/09/20 19:48 87-68-306/09/20 10:265.0 1.6 1
Hexachlorobenzene ND ug/L 06/09/20 19:48 118-74-106/09/20 10:265.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/09/20 19:48 77-47-406/09/20 10:2610.0 2.4 1
Hexachloroethane ND ug/L 06/09/20 19:48 67-72-106/09/20 10:265.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/09/20 19:48 193-39-506/09/20 10:265.0 1.7 1
Isophorone ND ug/L 06/09/20 19:48 78-59-106/09/20 10:2610.0 1.3 1
Naphthalene ND ug/L 06/09/20 19:48 91-20-306/09/20 10:265.0 1.6 1
Nitrobenzene ND ug/L 06/09/20 19:48 98-95-306/09/20 10:265.0 1.5 1
2-Nitrophenol ND ug/L 06/09/20 19:48 88-75-506/09/20 10:265.0 1.7 1
4-Nitrophenol ND ug/L 06/09/20 19:48 100-02-706/09/20 10:2610.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/09/20 19:48 62-75-906/09/20 10:265.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/09/20 19:48 621-64-706/09/20 10:265.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/09/20 19:48 86-30-606/09/20 10:2610.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/09/20 19:48 108-60-106/09/20 10:265.0 1.3 1
Pentachlorophenol ND ug/L 06/09/20 19:48 87-86-506/09/20 10:2610.0 2.8 1
Phenanthrene ND ug/L 06/09/20 19:48 85-01-806/09/20 10:265.0 1.4 1
Phenol ND ug/L 06/09/20 19:48 108-95-206/09/20 10:265.0 1.5 1
Pyrene ND ug/L 06/09/20 19:48 129-00-006/09/20 10:265.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/09/20 19:48 120-82-106/09/20 10:265.0 1.6 1
2,4,6-Trichlorophenol ND ug/L 06/09/20 19:48 88-06-206/09/20 10:2610.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)75 %06/09/20 19:48 4165-60-006/09/20 10:2610-120 1
2-Fluorobiphenyl (S)71 %06/09/20 19:48 321-60-806/09/20 10:2615-120 1
Terphenyl-d14 (S)110 %06/09/20 19:48 1718-51-006/09/20 10:2611-131 1
Phenol-d6 (S)43 %06/09/20 19:48 13127-88-306/09/20 10:2610-120 1
2-Fluorophenol (S)52 %06/09/20 19:48 367-12-406/09/20 10:2610-120 1
2,4,6-Tribromophenol (S)95 %06/09/20 19:48 118-79-606/09/20 10:2610-137 1
Tentatively Identified Compounds
Toluene 20.0J ug/L 06/09/20 19:48 108-88-3 N06/09/20 10:261
Benzene, 2-ethenyl-1,4-d 10.0J ug/L 06/09/20 19:48 2039-89-6 N06/09/20 10:261
Naphthalene, 1,2,3,4-tet 7.2J ug/L 06/09/20 19:48 3877-19-8 N06/09/20 10:261
Naphthalene, 1,2,3,4-tet 5.8J ug/L 06/09/20 19:48 1559-81-5 N06/09/20 10:261
Naphthalene, 1,2,3,4-tet 11.6J ug/L 06/09/20 19:48 1680-51-9 N06/09/20 10:261
Naphthalene, 1,2,3,4-tet 7.9J ug/L 06/09/20 19:48 1680-51-9 N06/09/20 10:261
Hexadecanoic acid 32.7J ug/L 06/09/20 19:48 57-10-3 N06/09/20 10:261
Octadecanoic acid 9.0J ug/L 06/09/20 19:48 57-11-4 N06/09/20 10:261
Cycloeicosane 12.9J ug/L 06/09/20 19:48 296-56-0 N06/09/20 10:261
REPORT OF LABORATORY ANALYSIS
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Page 6 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Sample:MW-1 Lab ID:92480688001 Collected:06/05/20 11:30 Received:06/05/20 14:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
602 Volatiles by Method 6200
Benzene ND ug/L 06/10/20 02:07 71-43-21.0 0.24 1
Chlorobenzene ND ug/L 06/10/20 02:07 108-90-71.0 0.22 1
1,2-Dichlorobenzene ND ug/L 06/10/20 02:07 95-50-11.0 0.24 1
1,3-Dichlorobenzene ND ug/L 06/10/20 02:07 541-73-11.0 0.25 1
1,4-Dichlorobenzene ND ug/L 06/10/20 02:07 106-46-71.0 0.25 1
Diisopropyl ether ND ug/L 06/10/20 02:07 108-20-31.0 0.33 1
Ethylbenzene ND ug/L 06/10/20 02:07 100-41-41.0 0.24 1
Isopropylbenzene (Cumene)ND ug/L 06/10/20 02:07 98-82-81.0 0.24 1
Methyl-tert-butyl ether ND ug/L 06/10/20 02:07 1634-04-41.0 0.44 1
Naphthalene ND ug/L 06/10/20 02:07 91-20-32.0 0.66 1
Toluene ND ug/L 06/10/20 02:07 108-88-31.0 0.23 1
m&p-Xylene ND ug/L 06/10/20 02:07 179601-23-12.0 0.44 1
o-Xylene ND ug/L 06/10/20 02:07 95-47-6 L11.0 0.24 1
Surrogates
4-Bromofluorobenzene (S)102 %06/10/20 02:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %06/10/20 02:07 17060-07-070-130 1
Toluene-d8 (S)108 %06/10/20 02:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 7 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1488739
MADEPV
MADEP VPH
MADEPV
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92480688001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3537059-3
Associated Lab Samples:92480688001
Matrix:Water
AnalyzedMDL
Aliphatic (C05-C08)ug/L ND 100 06/08/20 12:4833.3
Aliphatic (C09-C12)ug/L ND 100 06/08/20 12:4833.3
Aromatic (C09-C10),Unadjusted ug/L ND 100 06/08/20 12:4833.3
2,5-Dibromotoluene (FID)%82.2 70.0-130 06/08/20 12:48
2,5-Dibromotoluene (PID)%74.6 70.0-130 06/08/20 12:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3537059-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3537059-2
Aliphatic (C05-C08)ug/L 11801200 98.3 70.0-1301031230 4.15 25
Aliphatic (C09-C12)ug/L 13401400 95.7 70.0-13096.41350 0.743 25
Aromatic (C09-C10),Unadjusted ug/L 192200 96.0 70.0-130102204 6.06 25
2,5-Dibromotoluene (FID)%95.5 70.0-13093.9
2,5-Dibromotoluene (PID)%86.5 70.0-13085.8
REPORT OF LABORATORY ANALYSIS
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Page 8 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
546197
SM 6200B
SM 6200B
602 by 6200B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92480688001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2907682
Associated Lab Samples:92480688001
Matrix:Water
AnalyzedMDL
1,2-Dichlorobenzene ug/L ND 1.0 06/09/20 21:510.24
1,3-Dichlorobenzene ug/L ND 1.0 06/09/20 21:510.25
1,4-Dichlorobenzene ug/L ND 1.0 06/09/20 21:510.25
Benzene ug/L ND 1.0 06/09/20 21:510.24
Chlorobenzene ug/L ND 1.0 06/09/20 21:510.22
Diisopropyl ether ug/L ND 1.0 06/09/20 21:510.33
Ethylbenzene ug/L ND 1.0 06/09/20 21:510.24
Isopropylbenzene (Cumene)ug/L ND 1.0 06/09/20 21:510.24
m&p-Xylene ug/L ND 2.0 06/09/20 21:510.44
Methyl-tert-butyl ether ug/L ND 1.0 06/09/20 21:510.44
Naphthalene ug/L ND 2.0 06/09/20 21:510.66
o-Xylene ug/L ND 1.0 06/09/20 21:510.24
Toluene ug/L ND 1.0 06/09/20 21:510.23
1,2-Dichloroethane-d4 (S)%95 70-130 06/09/20 21:51
4-Bromofluorobenzene (S)%100 70-130 06/09/20 21:51
Toluene-d8 (S)%101 70-130 06/09/20 21:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2907683LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/L 51.550 103 60-140
1,3-Dichlorobenzene ug/L 49.550 99 60-140
1,4-Dichlorobenzene ug/L 52.650 105 60-140
Benzene ug/L 48.850 98 60-140
Chlorobenzene ug/L 50.550 101 60-140
Diisopropyl ether ug/L 51.350 103 60-140
Ethylbenzene ug/L 48.950 98 60-140
Isopropylbenzene (Cumene)ug/L 51.750 103 60-140
m&p-Xylene ug/L 98.4100 98 60-140
Methyl-tert-butyl ether ug/L 53.350 107 60-140
Naphthalene ug/L 51.650 103 60-140
o-Xylene ug/L 102 L15020460-140
Toluene ug/L 46.850 94 60-140
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/12/2020 12:26 PM
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[phone]
Page 9 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2907684MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92479992002
2907685
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dichlorobenzene ug/L 20 102 60-140104 2 3020ND20.4 20.9
1,3-Dichlorobenzene ug/L 20 101 60-140102 1 3020ND20.3 20.5
1,4-Dichlorobenzene ug/L 20 101 60-140104 2 3020ND20.3 20.7
Benzene ug/L 20 100 60-140102 2 3020ND20.0 20.3
Chlorobenzene ug/L 20 103 60-140103 0 3020ND20.7 20.7
Diisopropyl ether ug/L 20 98 60-140100 2 3020ND19.6 20.0
Ethylbenzene ug/L 20 101 60-140101 1 3020ND20.1 20.3
Isopropylbenzene
(Cumene)ug/L 20 106 60-140106 0 3020ND21.3 21.2
m&p-Xylene ug/L 40 101 60-140102 1 3040ND40.5 40.8
Methyl-tert-butyl ether ug/L 20 101 60-140104 2 3020ND20.3 20.7
Naphthalene ug/L 20 108 60-140102 6 3020ND21.7 20.3
o-Xylene ug/L 20 103 60-140103 0 3020ND20.6 20.6
Toluene ug/L 20 97 60-14099 2 3020ND19.5 19.8
1,2-Dichloroethane-d4 (S)%100 70-130102
4-Bromofluorobenzene (S)%99 70-13098
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/12/2020 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
545759
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92480688001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2905706
Associated Lab Samples:92480688001
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 5.0 06/09/20 11:391.6
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 06/09/20 11:391.3
2,4,6-Trichlorophenol ug/L ND 10.0 06/09/20 11:391.4
2,4-Dichlorophenol ug/L ND 5.0 06/09/20 11:391.5
2,4-Dimethylphenol ug/L ND 10.0 06/09/20 11:391.5
2,4-Dinitrophenol ug/L ND 50.0 06/09/20 11:397.3
2,4-Dinitrotoluene ug/L ND 5.0 06/09/20 11:391.7
2,6-Dinitrotoluene ug/L ND 5.0 06/09/20 11:391.7
2-Chloronaphthalene ug/L ND 5.0 06/09/20 11:391.4
2-Chlorophenol ug/L ND 5.0 06/09/20 11:391.4
2-Nitrophenol ug/L ND 5.0 06/09/20 11:391.7
3,3'-Dichlorobenzidine ug/L ND 10.0 06/09/20 11:392.7
4,6-Dinitro-2-methylphenol ug/L ND 10.0 06/09/20 11:394.5
4-Bromophenylphenyl ether ug/L ND 5.0 06/09/20 11:391.2
4-Chloro-3-methylphenol ug/L ND 5.0 06/09/20 11:392.8
4-Chlorophenylphenyl ether ug/L ND 5.0 06/09/20 11:391.5
4-Nitrophenol ug/L ND 10.0 06/09/20 11:399.4
Acenaphthene ug/L ND 5.0 06/09/20 11:391.4
Acenaphthylene ug/L ND 5.0 06/09/20 11:391.5
Anthracene ug/L ND 5.0 06/09/20 11:391.6
Benzo(a)anthracene ug/L ND 5.0 06/09/20 11:391.5
Benzo(a)pyrene ug/L ND 5.0 06/09/20 11:391.8
Benzo(b)fluoranthene ug/L ND 5.0 06/09/20 11:391.7
Benzo(g,h,i)perylene ug/L ND 5.0 06/09/20 11:391.6
Benzo(k)fluoranthene ug/L ND 5.0 06/09/20 11:391.5
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/09/20 11:391.3
bis(2-Chloroethyl) ether ug/L ND 5.0 06/09/20 11:391.7
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 06/09/20 11:392.0
Butylbenzylphthalate ug/L ND 5.0 06/09/20 11:391.9
Chrysene ug/L ND 5.0 06/09/20 11:391.4
Di-n-butylphthalate ug/L ND 5.0 06/09/20 11:391.6
Di-n-octylphthalate ug/L ND 5.0 06/09/20 11:392.2
Dibenz(a,h)anthracene ug/L ND 5.0 06/09/20 11:391.6
Diethylphthalate ug/L ND 5.0 06/09/20 11:391.6
Dimethylphthalate ug/L ND 5.0 06/09/20 11:391.4
Fluoranthene ug/L ND 5.0 06/09/20 11:391.6
Fluorene ug/L ND 5.0 06/09/20 11:391.4
Hexachloro-1,3-butadiene ug/L ND 5.0 06/09/20 11:391.6
Hexachlorobenzene ug/L ND 5.0 06/09/20 11:391.3
Hexachlorocyclopentadiene ug/L ND 10.0 06/09/20 11:392.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/12/2020 12:26 PM
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Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2905706
Associated Lab Samples:92480688001
Matrix:Water
AnalyzedMDL
Hexachloroethane ug/L ND 5.0 06/09/20 11:391.3
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 06/09/20 11:391.7
Isophorone ug/L ND 10.0 06/09/20 11:391.3
N-Nitroso-di-n-propylamine ug/L ND 5.0 06/09/20 11:391.3
N-Nitrosodimethylamine ug/L ND 5.0 06/09/20 11:391.8
N-Nitrosodiphenylamine ug/L ND 10.0 06/09/20 11:391.4
Naphthalene ug/L ND 5.0 06/09/20 11:391.6
Nitrobenzene ug/L ND 5.0 06/09/20 11:391.5
Pentachlorophenol ug/L ND 10.0 06/09/20 11:392.8
Phenanthrene ug/L ND 5.0 06/09/20 11:391.4
Phenol ug/L ND 5.0 06/09/20 11:391.5
Pyrene ug/L ND 5.0 06/09/20 11:391.5
2,4,6-Tribromophenol (S)%65 10-137 06/09/20 11:39
2-Fluorobiphenyl (S)%72 15-120 06/09/20 11:39
2-Fluorophenol (S)%56 10-120 06/09/20 11:39
Nitrobenzene-d5 (S)%69 10-120 06/09/20 11:39
Phenol-d6 (S)%42 10-120 06/09/20 11:39
Terphenyl-d14 (S)%98 11-131 06/09/20 11:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2905707LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 39.150 78 44-142
2,2'-Oxybis(1-chloropropane)ug/L 63.350 127 36-166
2,4,6-Trichlorophenol ug/L 49.950 100 37-144
2,4-Dichlorophenol ug/L 48.950 98 1-191
2,4-Dimethylphenol ug/L 43.950 88 32-119
2,4-Dinitrophenol ug/L 341250 136 1-181
2,4-Dinitrotoluene ug/L 59.350 119 39-139
2,6-Dinitrotoluene ug/L 54.450 109 50-158
2-Chloronaphthalene ug/L 44.150 88 60-118
2-Chlorophenol ug/L 48.850 98 23-134
2-Nitrophenol ug/L 57.250 114 29-182
3,3'-Dichlorobenzidine ug/L 89.8100 90 1-262
4,6-Dinitro-2-methylphenol ug/L 138100 138 1-181
4-Bromophenylphenyl ether ug/L 45.150 90 53-127
4-Chloro-3-methylphenol ug/L 96.6100 97 22-147
4-Chlorophenylphenyl ether ug/L 45.350 91 25-158
4-Nitrophenol ug/L 173250 69 1-132
Acenaphthene ug/L 46.950 94 47-145
Acenaphthylene ug/L 48.350 97 33-145
Anthracene ug/L 49.650 99 1-166
Benzo(a)anthracene ug/L 50.650 101 33-143
Benzo(a)pyrene ug/L 51.750 103 17-163
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/12/2020 12:26 PM
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Huntersville, NC 28078
[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2905707LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 51.450 103 24-159
Benzo(g,h,i)perylene ug/L 50.750 101 1-219
Benzo(k)fluoranthene ug/L 52.250 104 11-162
bis(2-Chloroethoxy)methane ug/L 42.950 86 33-184
bis(2-Chloroethyl) ether ug/L 44.050 88 12-158
bis(2-Ethylhexyl)phthalate ug/L 54.650 109 8-158
Butylbenzylphthalate ug/L 55.350 111 1-152
Chrysene ug/L 50.150 100 17-168
Di-n-butylphthalate ug/L 52.550 105 1-118
Di-n-octylphthalate ug/L 56.150 112 4-146
Dibenz(a,h)anthracene ug/L 51.550 103 1-227
Diethylphthalate ug/L 50.550 101 1-114
Dimethylphthalate ug/L 48.650 97 1-112
Fluoranthene ug/L 50.350 101 26-137
Fluorene ug/L 49.150 98 59-121
Hexachloro-1,3-butadiene ug/L 35.450 71 24-116
Hexachlorobenzene ug/L 43.950 88 1-152
Hexachlorocyclopentadiene ug/L 37.050 74 25-150
Hexachloroethane ug/L 36.850 74 40-113
Indeno(1,2,3-cd)pyrene ug/L 51.050 102 1-171
Isophorone ug/L 44.450 89 21-196
N-Nitroso-di-n-propylamine ug/L 45.850 92 1-230
N-Nitrosodimethylamine ug/L 39.550 79 25-150
N-Nitrosodiphenylamine ug/L 47.850 96 25-150
Naphthalene ug/L 43.750 87 21-133
Nitrobenzene ug/L 44.350 89 35-180
Pentachlorophenol ug/L 107100 107 14-176
Phenanthrene ug/L 49.650 99 54-120
Phenol ug/L 33.650 67 5-112
Pyrene ug/L 51.050 102 52-115
2,4,6-Tribromophenol (S)%104 10-137
2-Fluorobiphenyl (S)%92 15-120
2-Fluorophenol (S)%77 10-120
Nitrobenzene-d5 (S)%91 10-120
Phenol-d6 (S)%60 10-120
Terphenyl-d14 (S)%115 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2905708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92480643001
2905709
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 56 44-14257 2 3050ND27.9 28.5
2,2'-Oxybis(1-
chloropropane)ug/L 50 92 36-16695 4 3050ND45.9 47.6
2,4,6-Trichlorophenol ug/L 50 71 37-14473 3 3050ND35.3 36.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/12/2020 12:26 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2905708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92480643001
2905709
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4-Dichlorophenol ug/L 50 68 1-19172 5 3050ND33.9 35.8
2,4-Dimethylphenol ug/L 50 54 32-11955 1 3050ND27.1 27.4
2,4-Dinitrophenol ug/L 250 108 1-181107 1 30250ND269266
2,4-Dinitrotoluene ug/L 50 96 39-13991 6 3050ND48.1 45.5
2,6-Dinitrotoluene ug/L 50 83 50-15882 2 3050ND41.5 40.8
2-Chloronaphthalene ug/L 50 63 60-11865 3 3050ND31.5 32.5
2-Chlorophenol ug/L 50 68 23-13472 5 3050ND34.1 35.8
2-Nitrophenol ug/L 50 80 29-18286 7 3050ND40.2 43.0
3,3'-Dichlorobenzidine ug/L 100 82 1-26281 1 30100ND81.9 81.2
4,6-Dinitro-2-methylphenol ug/L 100 115 1-181114 1 30100ND115114
4-Bromophenylphenyl ether ug/L 50 74 53-12767 10 3050ND37.0 33.6
4-Chloro-3-methylphenol ug/L 100 71 22-14770 1 30100ND70.9 70.3
4-Chlorophenylphenyl ether ug/L 50 68 25-15866 3 3050ND33.8 32.8
4-Nitrophenol ug/L 250 67 1-13265 4 30250ND168161
Acenaphthene ug/L 50 67 47-14568 3 3050ND33.3 34.2
Acenaphthylene ug/L 50 69 33-14571 3 3050ND34.4 35.3
Anthracene ug/L 50 85 1-16681 4 3050ND42.3 40.6
Benzo(a)anthracene ug/L 50 93 33-14392 1 3050ND46.7 46.2
Benzo(a)pyrene ug/L 50 93 17-16392 1 3050ND46.7 46.0
Benzo(b)fluoranthene ug/L 50 93 24-15994 1 3050ND46.3 47.0
Benzo(g,h,i)perylene ug/L 50 89 1-21987 2 3050ND44.5 43.5
Benzo(k)fluoranthene ug/L 50 91 11-16291 0 3050ND45.7 45.6
bis(2-
Chloroethoxy)methane ug/L 50 60 33-18463 4 3050ND30.1 31.3
bis(2-Chloroethyl) ether ug/L 50 65 12-15868 5 3050ND32.3 34.1
bis(2-Ethylhexyl)phthalate ug/L 50 111 8-158108 3 3050ND55.4 53.9
Butylbenzylphthalate ug/L 50 110 1-152110 0 3050ND55.1 55.0
Chrysene ug/L 50 91 17-16890 0 3050ND45.3 45.2
Di-n-butylphthalate ug/L 50 96 1-11897 1 3050ND48.2 48.6
Di-n-octylphthalate ug/L 50 113 4-146111 2 3050ND56.7 55.4
Dibenz(a,h)anthracene ug/L 50 90 1-22789 2 3050ND45.1 44.3
Diethylphthalate ug/L 50 83 1-11478 5 3050ND41.3 39.2
Dimethylphthalate ug/L 50 73 1-11270 4 3050ND36.6 35.2
Fluoranthene ug/L 50 90 26-13790 1 3050ND45.1 44.9
Fluorene ug/L 50 73 59-12171 3 3050ND36.5 35.4
Hexachloro-1,3-butadiene ug/L 50 50 24-11651 2 3050ND25.0 25.5
Hexachlorobenzene ug/L 50 72 1-15267 7 3050ND36.1 33.7
Hexachlorocyclopentadiene ug/L 50 53 25-15053 1 3050ND26.6 26.7
Hexachloroethane ug/L 50 52 40-11353 2 3050ND26.2 26.7
Indeno(1,2,3-cd)pyrene ug/L 50 89 1-17187 2 3050ND44.5 43.6
Isophorone ug/L 50 63 21-19666 4 3050ND31.4 32.8
N-Nitroso-di-n-propylamine ug/L 50 67 1-23071 6 3050ND33.7 35.6
N-Nitrosodimethylamine ug/L 50 60 25-15061 3 3050ND29.8 30.7
N-Nitrosodiphenylamine ug/L 50 81 25-15077 5 3050ND40.6 38.6
Naphthalene ug/L 50 63 21-13364 2 3050ND31.4 32.1
Nitrobenzene ug/L 50 63 35-18066 4 3050ND31.7 33.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/12/2020 12:26 PM
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Huntersville, NC 28078
[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2905708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92480643001
2905709
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Pentachlorophenol ug/L 100 100 14-176100 0 30100ND100100
Phenanthrene ug/L 50 85 54-12080 5 3050ND42.3 40.1
Phenol ug/L 50 54 5-11255 3 3050ND26.9 27.7
Pyrene ug/L 50 96 52-11595 1 3050ND48.2 47.7
2,4,6-Tribromophenol (S)%93 10-13789
2-Fluorobiphenyl (S)%67 15-12070
2-Fluorophenol (S)%58 10-12059
Nitrobenzene-d5 (S)%68 10-12071
Phenol-d6 (S)%53 10-12053
Terphenyl-d14 (S)%107 11-131113
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/12/2020 12:26 PM
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Huntersville, NC 28078
[phone]
Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
545760
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92480688001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2905710
Associated Lab Samples:92480688001
Matrix:Water
AnalyzedMDL
Aliphatic (C09-C18)ug/L ND 100 N206/09/20 14:48100
Aliphatic (C19-C36)ug/L ND 100 N206/09/20 14:48100
Aromatic (C11-C22)ug/L ND 100 N206/09/20 14:48100
2-Bromonaphthalene (S)%114 40-140 06/09/20 14:48
2-Fluorobiphenyl (S)%116 40-140 06/09/20 14:48
Nonatriacontane (S)%69 40-140 06/09/20 14:48
o-Terphenyl (S)%76 40-140 06/09/20 14:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2905711LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2905712
Aliphatic (C09-C18)ug/L 103 L2,N23003440-14040121 16 50
Aliphatic (C19-C36)ug/L 209 N24005240-14062249 18 50
Aromatic (C11-C22)ug/L 542 N28506440-14071605 11 50
2-Bromonaphthalene (S)%110 40-140106
2-Fluorobiphenyl (S)%108 40-140105
Nonatriacontane (S)%60 40-14072
o-Terphenyl (S)%82 40-14088
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/12/2020 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was re-extracted within hold time. Results from re-extraction confirm initial analysis.1g
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
The reported TIC has an 85% or higher match on a mass spectral library search.N
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
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[phone]
Page 17 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92480688
Greensboro NC LC 0134 UST Clos
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92480688001 545760 546149MW-1 MADEP EPH MADEP EPH
92480688001 1488739 1488739MW-1 MADEPV MADEP VPH
92480688001 545759 546107MW-1 EPA 625.1 EPA 625.1
92480688001 546197MW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/12/2020 12:26 PM
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[phone]
Page 18 of 21
Page 19 of 21
Page 20 of 21
Page 21 of 21
#=CL#
April 24, 2020
LIMS USE: FR - BRITNEY BARNES
LIMS OBJECT ID: 92474701
92474701
Project:
Pace Project No.:
RE:
Britney Barnes
Civil & Environmental Consultants
530 Howell Rd
Suite 203
Greenville, SC
GREENSBORO NC LC 0134 UST CLOS
Dear Britney Barnes:
Enclosed are the analytical results for sample(s) received by the laboratory on April 22, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Sarah Galloway, Ryder Systems, Inc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 29
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 29
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Lab ID Sample ID Matrix Date Collected Date Received
92474701001 NW1 Solid 04/21/20 10:20 04/22/20 13:42
92474701002 NW2 Solid 04/21/20 10:30 04/22/20 13:42
92474701003 NW3 Solid 04/21/20 10:45 04/22/20 13:42
92474701004 NW4 Solid 04/21/20 10:55 04/22/20 13:42
92474701005 EW-1 Solid 04/21/20 11:00 04/22/20 13:42
92474701006 EW-2 Solid 04/21/20 11:05 04/22/20 13:42
92474701007 EW-3 Solid 04/21/20 11:10 04/22/20 13:42
92474701008 EW-4 Solid 04/21/20 11:20 04/22/20 13:42
92474701009 EW-5 Solid 04/21/20 11:25 04/22/20 13:42
92474701010 SW1 Solid 04/21/20 11:45 04/22/20 13:42
92474701011 SW2 Solid 04/21/20 11:55 04/22/20 13:42
92474701012 SW3 Solid 04/21/20 12:00 04/22/20 13:42
92474701013 SW4 Solid 04/21/20 12:10 04/22/20 13:42
92474701014 SW3.2 Solid 04/21/20 12:30 04/22/20 13:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 29
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92474701001 NW1 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701002 NW2 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701003 NW3 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701004 NW4 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701005 EW-1 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701006 EW-2 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701007 EW-3 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701008 EW-4 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701009 EW-5 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701010 SW1 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701011 SW2 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701012 SW3 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701013 SW4 EPA 8015C Modified 2 PASI-CBAJ
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 29
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92474701014 SW3.2 ASTM D2974-87 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:NW1 Lab ID:92474701001 Collected:04/21/20 10:20 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 04/23/20 10:1704/22/20 21:195.9 2.7 1
Surrogates
n-Pentacosane (S)70 %04/23/20 10:17 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1.7J mg/kg 04/23/20 13:04 B04/23/20 10:327.2 1.4 1
Surrogates
4-Bromofluorobenzene (S)96 %04/23/20 13:04 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.8 %04/22/20 16:450.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:NW2 Lab ID:92474701002 Collected:04/21/20 10:30 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 04/23/20 10:4004/22/20 21:196.1 2.8 1
Surrogates
n-Pentacosane (S)76 %04/23/20 10:40 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 04/23/20 14:0004/23/20 10:325.4 1.0 1
Surrogates
4-Bromofluorobenzene (S)96 %04/23/20 14:00 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.0 %04/22/20 16:450.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:NW3 Lab ID:92474701003 Collected:04/21/20 10:45 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 04/23/20 11:0404/22/20 21:197.2 3.3 1
Surrogates
n-Pentacosane (S)85 %04/23/20 11:04 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1.8J mg/kg 04/23/20 15:25 B04/23/20 10:327.2 1.4 1
Surrogates
4-Bromofluorobenzene (S)101 %04/23/20 15:25 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 30.4 %04/22/20 16:450.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:NW4 Lab ID:92474701004 Collected:04/21/20 10:55 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 04/23/20 11:2804/22/20 21:196.8 3.1 1
Surrogates
n-Pentacosane (S)76 %04/23/20 11:28 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1.8J mg/kg 04/23/20 15:5304/23/20 10:329.3 1.8 1
Surrogates
4-Bromofluorobenzene (S)100 %04/23/20 15:53 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.9 %04/22/20 16:450.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:EW-1 Lab ID:92474701005 Collected:04/21/20 11:00 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 04/23/20 11:2804/22/20 21:196.0 2.8 1
Surrogates
n-Pentacosane (S)79 %04/23/20 11:28 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1.6J mg/kg 04/23/20 16:21 B04/23/20 10:326.7 1.3 1
Surrogates
4-Bromofluorobenzene (S)97 %04/23/20 16:21 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.0 %04/22/20 17:090.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:EW-2 Lab ID:92474701006 Collected:04/21/20 11:05 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)4.1J mg/kg 04/23/20 11:5204/22/20 21:196.1 2.8 1
Surrogates
n-Pentacosane (S)75 %04/23/20 11:52 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)3.0J mg/kg 04/23/20 20:05 B04/23/20 10:327.0 1.3 1
Surrogates
4-Bromofluorobenzene (S)98 %04/23/20 20:05 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.8 %04/22/20 17:090.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:EW-3 Lab ID:92474701007 Collected:04/21/20 11:10 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)5.7J mg/kg 04/23/20 11:5204/22/20 21:196.5 3.0 1
Surrogates
n-Pentacosane (S)87 %04/23/20 11:52 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1.8J mg/kg 04/23/20 16:49 B04/23/20 10:325.9 1.1 1
Surrogates
4-Bromofluorobenzene (S)101 %04/23/20 16:49 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.3 %04/22/20 17:100.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:EW-4 Lab ID:92474701008 Collected:04/21/20 11:20 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)6.9J mg/kg 04/23/20 12:1604/22/20 21:197.0 3.2 1
Surrogates
n-Pentacosane (S)71 %04/23/20 12:16 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)4.4J mg/kg 04/23/20 17:17 B04/23/20 10:327.5 1.4 1
Surrogates
4-Bromofluorobenzene (S)97 %04/23/20 17:17 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.4 %04/22/20 17:100.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:EW-5 Lab ID:92474701009 Collected:04/21/20 11:25 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)3.4J mg/kg 04/23/20 12:1604/22/20 21:196.6 3.1 1
Surrogates
n-Pentacosane (S)82 %04/23/20 12:16 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1.8J mg/kg 04/23/20 17:45 B04/23/20 10:327.2 1.4 1
Surrogates
4-Bromofluorobenzene (S)99 %04/23/20 17:45 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.7 %04/22/20 17:100.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:SW1 Lab ID:92474701010 Collected:04/21/20 11:45 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)8.1 mg/kg 04/23/20 12:4004/22/20 21:197.0 3.2 1
Surrogates
n-Pentacosane (S)65 %04/23/20 12:40 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1.9J mg/kg 04/23/20 18:13 B04/23/20 10:326.6 1.3 1
Surrogates
4-Bromofluorobenzene (S)97 %04/23/20 18:13 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.1 %04/22/20 17:100.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:SW2 Lab ID:92474701011 Collected:04/21/20 11:55 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)5.6J mg/kg 04/23/20 12:4004/22/20 21:196.8 3.1 1
Surrogates
n-Pentacosane (S)80 %04/23/20 12:40 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1.8J mg/kg 04/23/20 18:41 B04/23/20 10:326.8 1.3 1
Surrogates
4-Bromofluorobenzene (S)99 %04/23/20 18:41 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.9 %04/22/20 17:100.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:SW3 Lab ID:92474701012 Collected:04/21/20 12:00 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 04/23/20 13:0404/22/20 21:196.2 2.9 1
Surrogates
n-Pentacosane (S)70 %04/23/20 13:04 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)2.6J mg/kg 04/23/20 19:09 B04/23/20 10:326.1 1.2 1
Surrogates
4-Bromofluorobenzene (S)98 %04/23/20 19:09 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.9 %04/22/20 17:100.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:SW4 Lab ID:92474701013 Collected:04/21/20 12:10 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 04/23/20 13:0404/22/20 21:197.0 3.2 1
Surrogates
n-Pentacosane (S)76 %04/23/20 13:04 629-99-204/22/20 21:1933-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1.7J mg/kg 04/23/20 19:37 B04/23/20 10:326.9 1.3 1
Surrogates
4-Bromofluorobenzene (S)98 %04/23/20 19:37 460-00-404/23/20 10:3263-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.3 %04/22/20 17:100.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Sample:SW3.2 Lab ID:92474701014 Collected:04/21/20 12:30 Received:04/22/20 13:42 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.3 %04/22/20 17:100.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
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[phone]
Page 19 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
537809
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474701001, 92474701002, 92474701003, 92474701004, 92474701005, 92474701006, 92474701007,
92474701008, 92474701009, 92474701010, 92474701011, 92474701012, 92474701013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2867744
Associated Lab Samples:92474701001, 92474701002, 92474701003, 92474701004, 92474701005, 92474701006, 92474701007,
92474701008, 92474701009, 92474701010, 92474701011, 92474701012, 92474701013
Matrix:Solid
AnalyzedMDL
Gas Range Organics (C6-C10)mg/kg 1.5J 5.9 04/23/20 12:361.1
4-Bromofluorobenzene (S)%97 63-130 04/23/20 12:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2867745LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 57.349.5 116 70-130
4-Bromofluorobenzene (S)%98 63-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2867747MATRIX SPIKE SAMPLE:
MSSpike
Result
92474701002
Gas Range Organics (C6-C10)mg/kg 61.045.3 133 40-155ND
4-Bromofluorobenzene (S)%101 63-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92474701001
2867746SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg 1.7J 301.7J
4-Bromofluorobenzene (S)%9796
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
537716
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474701001, 92474701002, 92474701003, 92474701004, 92474701005, 92474701006, 92474701007,
92474701008, 92474701009, 92474701010, 92474701011, 92474701012, 92474701013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2867412
Associated Lab Samples:92474701001, 92474701002, 92474701003, 92474701004, 92474701005, 92474701006, 92474701007,
92474701008, 92474701009, 92474701010, 92474701011, 92474701012, 92474701013
Matrix:Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 4.9 04/23/20 09:532.3
n-Pentacosane (S)%69 33-129 04/23/20 09:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2867413LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 50.765.6 77 43-130
n-Pentacosane (S)%86 33-129
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2867414MATRIX SPIKE SAMPLE:
MSSpike
Result
92474701001
Diesel Range Organics(C10-C28)mg/kg 63.880.9 77 10-130ND
n-Pentacosane (S)%83 33-129
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92474701001
2867415SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg ND 30ND
n-Pentacosane (S)%6870
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
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9800 Kincey Ave. Suite 100
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Page 21 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
537693
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474701001, 92474701002, 92474701003, 92474701004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92474701001
2867334SAMPLE DUPLICATE:
Percent Moisture %17.3 3 2516.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92474640011
2867335SAMPLE DUPLICATE:
Percent Moisture %14.0 2 2513.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
537698
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92474701005, 92474701006, 92474701007, 92474701008, 92474701009, 92474701010, 92474701011,
92474701012, 92474701013, 92474701014
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92474701005
2867353SAMPLE DUPLICATE:
Percent Moisture %16.8 5 2516.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92474695002
2867354SAMPLE DUPLICATE:
Percent Moisture %23.7 2 2523.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 29
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
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Huntersville, NC 28078
[phone]
Page 24 of 29
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92474701
GREENSBORO NC LC 0134 UST CLOS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92474701001 537716 537827NW1EPA 3546 EPA 8015C Modified
92474701002 537716 537827NW2EPA 3546 EPA 8015C Modified
92474701003 537716 537827NW3EPA 3546 EPA 8015C Modified
92474701004 537716 537827NW4EPA 3546 EPA 8015C Modified
92474701005 537716 537827EW-1 EPA 3546 EPA 8015C Modified
92474701006 537716 537827EW-2 EPA 3546 EPA 8015C Modified
92474701007 537716 537827EW-3 EPA 3546 EPA 8015C Modified
92474701008 537716 537827EW-4 EPA 3546 EPA 8015C Modified
92474701009 537716 537827EW-5 EPA 3546 EPA 8015C Modified
92474701010 537716 537827SW1EPA 3546 EPA 8015C Modified
92474701011 537716 537827SW2EPA 3546 EPA 8015C Modified
92474701012 537716 537827SW3EPA 3546 EPA 8015C Modified
92474701013 537716 537827SW4EPA 3546 EPA 8015C Modified
92474701001 537809 537818NW1EPA 5030B EPA 8015C Modified
92474701002 537809 537818NW2EPA 5030B EPA 8015C Modified
92474701003 537809 537818NW3EPA 5030B EPA 8015C Modified
92474701004 537809 537818NW4EPA 5030B EPA 8015C Modified
92474701005 537809 537818EW-1 EPA 5030B EPA 8015C Modified
92474701006 537809 537818EW-2 EPA 5030B EPA 8015C Modified
92474701007 537809 537818EW-3 EPA 5030B EPA 8015C Modified
92474701008 537809 537818EW-4 EPA 5030B EPA 8015C Modified
92474701009 537809 537818EW-5 EPA 5030B EPA 8015C Modified
92474701010 537809 537818SW1EPA 5030B EPA 8015C Modified
92474701011 537809 537818SW2EPA 5030B EPA 8015C Modified
92474701012 537809 537818SW3EPA 5030B EPA 8015C Modified
92474701013 537809 537818SW4EPA 5030B EPA 8015C Modified
92474701001 537693NW1ASTM D2974-87
92474701002 537693NW2ASTM D2974-87
92474701003 537693NW3ASTM D2974-87
92474701004 537693NW4ASTM D2974-87
92474701005 537698EW-1 ASTM D2974-87
92474701006 537698EW-2 ASTM D2974-87
92474701007 537698EW-3 ASTM D2974-87
92474701008 537698EW-4 ASTM D2974-87
92474701009 537698EW-5 ASTM D2974-87
92474701010 537698SW1ASTM D2974-87
92474701011 537698SW2ASTM D2974-87
92474701012 537698SW3ASTM D2974-87
92474701013 537698SW4ASTM D2974-87
92474701014 537698SW3.2 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/24/2020 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 29
Page 26 of 29
Page 27 of 29
Page 28 of 29
Page 29 of 29
#=CL#
March 25, 2020
LIMS USE: FR - BRITNEY BARNES
LIMS OBJECT ID: 92470345
92470345
Project:
Pace Project No.:
RE:
Britney Barnes
Civil & Environmental Consultants
530 Howell Rd
Suite 203
Greenville, SC
RYDER GREENSBORO NC
Dear Britney Barnes:
Enclosed are the analytical results for sample(s) received by the laboratory on March 20, 2020. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Sarah Galloway, Ryder Systems, Inc
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 15
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92470345
RYDER GREENSBORO NC
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 15
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92470345
RYDER GREENSBORO NC
Lab ID Sample ID Matrix Date Collected Date Received
92470345001 STOCKPILE 01 Solid 03/19/20 17:00 03/20/20 10:23
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 15
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92470345
RYDER GREENSBORO NC
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92470345001 STOCKPILE 01 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
EPA 6010D 7 PASI-ARDT
EPA 7470A 1 PASI-ASOO
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 4 of 15
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470345
RYDER GREENSBORO NC
Sample:STOCKPILE 01 Lab ID:92470345001 Collected:03/19/20 17:00 Received:03/20/20 10:23 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)65.3 mg/kg 03/24/20 11:3803/23/20 15:126.0 2.7 1
Surrogates
n-Pentacosane (S)111 %03/24/20 11:38 629-99-203/23/20 15:1233-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030BGasoline Range Organics
Gas Range Organics (C6-C10)4.0J mg/kg 03/23/20 16:13 B03/23/20 15:107.1 1.4 1
Surrogates
4-Bromofluorobenzene (S)108 %03/23/20 16:13 460-00-403/23/20 15:1063-130 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 03/23/20 14:00 Initial pH: 5.95; Final pH: 4.5
6010 MET ICP, TCLP
Arsenic ND mg/L 03/24/20 15:46 7440-38-203/24/20 10:350.050 0.0047 1
Barium 0.85 mg/L 03/24/20 15:46 7440-39-303/24/20 10:350.25 0.0010 1
Cadmium ND mg/L 03/24/20 15:46 7440-43-903/24/20 10:350.0050 0.00040 1
Chromium 0.0016J mg/L 03/24/20 15:46 7440-47-3 B03/24/20 10:350.050 0.0010 1
Lead ND mg/L 03/24/20 15:46 7439-92-103/24/20 10:350.025 0.0016 1
Selenium ND mg/L 03/24/20 15:46 7782-49-203/24/20 10:350.10 0.0047 1
Silver ND mg/L 03/24/20 15:46 7440-22-403/24/20 10:350.025 0.0025 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 03/23/20 14:00 Initial pH: 5.95; Final pH: 4.5
7470 Mercury, TCLP
Mercury ND mg/L 03/24/20 14:15 7439-97-603/24/20 11:020.00020 0.00010 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.3 %03/23/20 15:240.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/25/2020 04:10 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 5 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470345
RYDER GREENSBORO NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
531994
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Associated Lab Samples:92470345001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2840260
Associated Lab Samples:92470345001
Matrix:Solid
AnalyzedMDL
Gas Range Organics (C6-C10)mg/kg 1.5J 6.0 03/23/20 14:491.1
4-Bromofluorobenzene (S)%94 63-130 03/23/20 14:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2840261LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 50.349.7 101 70-130
4-Bromofluorobenzene (S)%94 63-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2840268MATRIX SPIKE SAMPLE:
MSSpike
Result
92470345001
Gas Range Organics (C6-C10)mg/kg 69.859.5 110 40-1554.0J
4-Bromofluorobenzene (S)%98 63-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92469870001
2840267SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%9394
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/25/2020 04:10 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 6 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470345
RYDER GREENSBORO NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
532146
EPA 7470A
EPA 7470A
7470 Mercury TCLP
Associated Lab Samples:92470345001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2839888
Associated Lab Samples:92470345001
Matrix:Water
AnalyzedMDL
Mercury mg/L ND 0.00020 03/24/20 13:400.00010
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2840737LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/L 0.00250.0025 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2840738MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92469892001
2840739
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/L 0.0025 103 75-12595 8 200.0025ND 0.0026 0.0024
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/25/2020 04:10 PM
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Huntersville, NC 28078
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Page 7 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470345
RYDER GREENSBORO NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
532145
EPA 3010A
EPA 6010D
6010 MET TCLP
Associated Lab Samples:92470345001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2839888
Associated Lab Samples:92470345001
Matrix:Water
AnalyzedMDL
Arsenic mg/L ND 0.050 03/24/20 14:580.0047
Barium mg/L 0.031J 0.25 03/24/20 14:580.0010
Cadmium mg/L ND 0.0050 03/24/20 14:580.00040
Chromium mg/L 0.0019J 0.050 03/24/20 14:580.0010
Lead mg/L ND 0.025 03/24/20 14:580.0016
Selenium mg/L ND 0.10 03/24/20 14:580.0047
Silver mg/L ND 0.025 03/24/20 14:580.0025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2840734LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 2.52.5 101 80-120
Barium mg/L 2.52.5 99 80-120
Cadmium mg/L 2.62.5 106 80-120
Chromium mg/L 2.52.5 98 80-120
Lead mg/L 2.62.5 103 80-120
Selenium mg/L 2.72.5 109 80-120
Silver mg/L 1.31.2 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2840735MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92469892001
2840736
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/L 2.5 101 75-12599 3 202.5ND 2.6 2.5
Barium mg/L 2.5 97 75-12596 2 202.50.33 2.8 2.7
Cadmium mg/L 2.5 106 75-125102 3 202.5ND 2.6 2.6
Chromium mg/L 2.5 98 75-12595 3 202.5ND 2.4 2.4
Lead mg/L 2.5 104 75-125101 3 202.50.041 2.6 2.6
Selenium mg/L 2.5 110 75-125105 4 202.5ND 2.7 2.6
Silver mg/L 1.2 101 75-12598 3 201.2ND 1.3 1.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/25/2020 04:10 PM
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Page 8 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470345
RYDER GREENSBORO NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
532008
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Associated Lab Samples:92470345001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2840326
Associated Lab Samples:92470345001
Matrix:Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 4.9 03/24/20 11:152.3
n-Pentacosane (S)%76 33-129 03/24/20 11:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2840327LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 47.266.7 71 43-130
n-Pentacosane (S)%79 33-129
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2840328MATRIX SPIKE SAMPLE:
MSSpike
Result
92470475001
Diesel Range Organics(C10-C28)mg/kg 24474 97 10-130173
n-Pentacosane (S)%89 33-129
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92470475002
2840329SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 5.3J 308.3
n-Pentacosane (S)%8982
REPORT OF LABORATORY ANALYSIS
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Page 9 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470345
RYDER GREENSBORO NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
532015
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92470345001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92469258030
2840392SAMPLE DUPLICATE:
Percent Moisture %21.7 2 2521.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92470619006
2840395SAMPLE DUPLICATE:
Percent Moisture %20.8 1 2520.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/25/2020 04:10 PM
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Page 10 of 15
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92470345
RYDER GREENSBORO NC
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/25/2020 04:10 PM
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Page 11 of 15
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92470345
RYDER GREENSBORO NC
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92470345001 532008 532193STOCKPILE 01 EPA 3546 EPA 8015C Modified
92470345001 531994 532026STOCKPILE 01 EPA 5030B EPA 8015C Modified
92470345001 532145 532178STOCKPILE 01 EPA 3010A EPA 6010D
92470345001 532146 532213STOCKPILE 01 EPA 7470A EPA 7470A
92470345001 532015STOCKPILE 01 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 12 of 15
Page 13 of 15
Page 14 of 15
Page 15 of 15
#=CL#
March 25, 2020
LIMS USE: FR - BRITNEY BARNES
LIMS OBJECT ID: 92470591
92470591
Project:
Pace Project No.:
RE:
Britney Barnes
Civil & Environmental Consultants
530 Howell Rd
Suite 203
Greenville, SC
Greensboro NC No 190-913
Dear Britney Barnes:
Enclosed are the analytical results for sample(s) received by the laboratory on March 23, 2020. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Sarah Galloway, Ryder Systems, Inc
REPORT OF LABORATORY ANALYSIS
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Page 1 of 17
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 17
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Lab ID Sample ID Matrix Date Collected Date Received
92470591001 UDC-01 Solid 03/20/20 09:00 03/23/20 10:10
92470591002 UDC-02 Solid 03/20/20 09:05 03/23/20 10:10
92470591003 UDC-03 Solid 03/20/20 10:00 03/23/20 10:10
92470591004 UDC-05 Solid 03/20/20 11:00 03/23/20 10:10
92470591005 UDC-08 Solid 03/20/20 11:05 03/23/20 10:10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 17
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92470591001 UDC-01 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92470591002 UDC-02 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92470591003 UDC-03 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92470591004 UDC-05 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
92470591005 UDC-08 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 4 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Sample:UDC-01 Lab ID:92470591001 Collected:03/20/20 09:00 Received:03/23/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 03/24/20 14:2603/24/20 09:216.6 3.0 1
Surrogates
n-Pentacosane (S)92 %03/24/20 14:26 629-99-203/24/20 09:2133-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 03/24/20 16:2603/24/20 13:295.2 1.0 1
Surrogates
4-Bromofluorobenzene (S)87 %03/24/20 16:26 460-00-403/24/20 13:2963-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.6 %03/24/20 17:340.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Sample:UDC-02 Lab ID:92470591002 Collected:03/20/20 09:05 Received:03/23/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 03/24/20 14:5003/24/20 09:216.8 3.1 1
Surrogates
n-Pentacosane (S)89 %03/24/20 14:50 629-99-203/24/20 09:2133-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 03/24/20 16:5403/24/20 13:296.6 1.2 1
Surrogates
4-Bromofluorobenzene (S)88 %03/24/20 16:54 460-00-403/24/20 13:2963-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 26.4 %03/24/20 17:350.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
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Page 6 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Sample:UDC-03 Lab ID:92470591003 Collected:03/20/20 10:00 Received:03/23/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 03/24/20 14:5003/24/20 09:216.7 3.1 1
Surrogates
n-Pentacosane (S)81 %03/24/20 14:50 629-99-203/24/20 09:2133-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 03/24/20 17:2203/24/20 13:296.1 1.2 1
Surrogates
4-Bromofluorobenzene (S)90 %03/24/20 17:22 460-00-403/24/20 13:2963-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 26.8 %03/24/20 17:350.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/25/2020 04:25 PM
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Huntersville, NC 28078
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Page 7 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Sample:UDC-05 Lab ID:92470591004 Collected:03/20/20 11:00 Received:03/23/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 03/24/20 15:1403/24/20 09:217.0 3.2 1
Surrogates
n-Pentacosane (S)75 %03/24/20 15:14 629-99-203/24/20 09:2133-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 03/24/20 15:5803/24/20 13:298.1 1.5 1
Surrogates
4-Bromofluorobenzene (S)91 %03/24/20 15:58 460-00-403/24/20 13:2963-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 28.1 %03/24/20 17:350.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
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Page 8 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Sample:UDC-08 Lab ID:92470591005 Collected:03/20/20 11:05 Received:03/23/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 03/24/20 15:1403/24/20 09:217.2 3.3 1
Surrogates
n-Pentacosane (S)85 %03/24/20 15:14 629-99-203/24/20 09:2133-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 03/24/20 17:5003/24/20 13:297.0 1.3 1
Surrogates
4-Bromofluorobenzene (S)87 %03/24/20 17:50 460-00-403/24/20 13:2963-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 31.5 %03/24/20 17:350.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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Page 9 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
532216
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Associated Lab Samples:92470591001, 92470591002, 92470591003, 92470591004, 92470591005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2841129
Associated Lab Samples:92470591001, 92470591002, 92470591003, 92470591004, 92470591005
Matrix:Solid
AnalyzedMDL
Gas Range Organics (C6-C10)mg/kg 1.2J 6.0 03/24/20 14:341.1
4-Bromofluorobenzene (S)%89 63-130 03/24/20 14:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2841130LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 51.049.8 102 70-130
4-Bromofluorobenzene (S)%91 63-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2841132MATRIX SPIKE SAMPLE:
MSSpike
Result
92470591004
Gas Range Organics (C6-C10)mg/kg 79.167.3 115 40-155ND
4-Bromofluorobenzene (S)%96 63-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92470166002
2841131SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%9091
REPORT OF LABORATORY ANALYSIS
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Page 10 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
532008
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Associated Lab Samples:92470591001, 92470591002, 92470591003, 92470591004, 92470591005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2840326
Associated Lab Samples:92470591001, 92470591002, 92470591003, 92470591004, 92470591005
Matrix:Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 4.9 03/24/20 11:152.3
n-Pentacosane (S)%76 33-129 03/24/20 11:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2840327LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 47.266.7 71 43-130
n-Pentacosane (S)%79 33-129
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2840328MATRIX SPIKE SAMPLE:
MSSpike
Result
92470475001
Diesel Range Organics(C10-C28)mg/kg 24474 97 10-130173
n-Pentacosane (S)%89 33-129
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92470475002
2840329SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 5.3J 308.3
n-Pentacosane (S)%8982
REPORT OF LABORATORY ANALYSIS
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Page 11 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
532304
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92470591001, 92470591002, 92470591003, 92470591004, 92470591005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
2629877001
2841723SAMPLE DUPLICATE:
Percent Moisture %48.2 11 2554.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92470591005
2841724SAMPLE DUPLICATE:
Percent Moisture %30.2 4 2531.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/25/2020 04:25 PM
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Page 12 of 17
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/25/2020 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 17
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92470591
Greensboro NC No 190-913
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92470591001 532008 532193UDC-01 EPA 3546 EPA 8015C Modified
92470591002 532008 532193UDC-02 EPA 3546 EPA 8015C Modified
92470591003 532008 532193UDC-03 EPA 3546 EPA 8015C Modified
92470591004 532008 532193UDC-05 EPA 3546 EPA 8015C Modified
92470591005 532008 532193UDC-08 EPA 3546 EPA 8015C Modified
92470591001 532216 532228UDC-01 EPA 5030B EPA 8015C Modified
92470591002 532216 532228UDC-02 EPA 5030B EPA 8015C Modified
92470591003 532216 532228UDC-03 EPA 5030B EPA 8015C Modified
92470591004 532216 532228UDC-05 EPA 5030B EPA 8015C Modified
92470591005 532216 532228UDC-08 EPA 5030B EPA 8015C Modified
92470591001 532304UDC-01 ASTM D2974-87
92470591002 532304UDC-02 ASTM D2974-87
92470591003 532304UDC-03 ASTM D2974-87
92470591004 532304UDC-05 ASTM D2974-87
92470591005 532304UDC-08 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/25/2020 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 17
Page 15 of 17
Page 16 of 17
Page 17 of 17
#=CL#
April 20, 2020
LIMS USE: FR - BRITNEY BARNES
LIMS OBJECT ID: 92473782
92473782
Project:
Pace Project No.:
RE:
Britney Barnes
Civil & Environmental Consultants
530 Howell Rd
Suite 203
Greenville, SC
GREENSBORO NC LC 0134 UST CLOS
Dear Britney Barnes:
Enclosed are the analytical results for sample(s) received by the laboratory on April 15, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Sarah Galloway, Ryder Systems, Inc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 48
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 48
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Lab ID Sample ID Matrix Date Collected Date Received
92473782001 W WALL Solid 04/14/20 09:30 04/15/20 10:10
92473782002 E WALL Solid 04/14/20 10:00 04/15/20 10:10
92473782003 S WALL Solid 04/14/20 09:40 04/15/20 10:10
92473782004 N WALL Solid 04/14/20 09:50 04/15/20 10:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 48
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92473782001 W WALL MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
92473782002 E WALL MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
92473782003 S WALL MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
92473782004 N WALL MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:W WALL Lab ID:92473782001 Collected:04/14/20 09:30 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/17/20 09:37 N204/16/20 09:1813.9 13.9 1
Aliphatic (C19-C36)ND mg/kg 04/17/20 09:37 N204/16/20 09:1813.9 13.9 1
Aromatic (C11-C22)ND mg/kg 04/17/20 09:37 N204/16/20 09:1813.9 13.9 1
Surrogates
Nonatriacontane (S)70 %04/17/20 09:37 7194-86-704/16/20 09:1840-140 1
o-Terphenyl (S)76 %04/17/20 09:37 84-15-104/16/20 09:1840-140 1
2-Fluorobiphenyl (S)89 %04/17/20 09:37 321-60-804/16/20 09:1840-140 1
2-Bromonaphthalene (S)91 %04/17/20 09:37 580-13-204/16/20 09:1840-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND mg/kg 04/18/20 13:0204/14/20 09:306.87 2.29 1
Aliphatic (C09-C12)3.68J mg/kg 04/18/20 13:02 J04/14/20 09:306.87 2.29 1
Aromatic (C09-C10),Unadjusted ND mg/kg 04/18/20 13:02 TPHC9C10A MH04/14/20 09:306.87 2.29 1
Surrogates
2,5-Dibromotoluene (FID)102 %04/18/20 13:02 615-59-8FID04/14/20 09:3070.0-130 1
2,5-Dibromotoluene (PID)106 %04/18/20 13:02 615-59-8PID04/14/20 09:3070.0-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/17/20 13:55 83-32-904/16/20 15:274641191
Acenaphthylene ND ug/kg 04/17/20 13:55 208-96-804/16/20 15:274641101
Aniline ND ug/kg 04/17/20 13:55 62-53-304/16/20 15:274641041
Anthracene ND ug/kg 04/17/20 13:55 120-12-704/16/20 15:274641201
Benzo(a)anthracene ND ug/kg 04/17/20 13:55 56-55-304/16/20 15:274641481
Benzo(a)pyrene ND ug/kg 04/17/20 13:55 50-32-804/16/20 15:274642011
Benzo(b)fluoranthene ND ug/kg 04/17/20 13:55 205-99-204/16/20 15:274641871
Benzo(g,h,i)perylene ND ug/kg 04/17/20 13:55 191-24-204/16/20 15:274641821
Benzo(k)fluoranthene ND ug/kg 04/17/20 13:55 207-08-904/16/20 15:274641961
Benzoic Acid ND ug/kg 04/17/20 13:55 65-85-004/16/20 15:2723205011
Benzyl alcohol ND ug/kg 04/17/20 13:55 100-51-604/16/20 15:279292461
4-Bromophenylphenyl ether ND ug/kg 04/17/20 13:55 101-55-304/16/20 15:274641221
Butylbenzylphthalate ND ug/kg 04/17/20 13:55 85-68-704/16/20 15:274641241
4-Chloro-3-methylphenol ND ug/kg 04/17/20 13:55 59-50-704/16/20 15:279292831
4-Chloroaniline ND ug/kg 04/17/20 13:55 106-47-804/16/20 15:279292841
bis(2-Chloroethoxy)methane ND ug/kg 04/17/20 13:55 111-91-104/16/20 15:274641241
bis(2-Chloroethyl) ether ND ug/kg 04/17/20 13:55 111-44-404/16/20 15:2746498.6 1
2-Chloronaphthalene ND ug/kg 04/17/20 13:55 91-58-704/16/20 15:274641031
2-Chlorophenol ND ug/kg 04/17/20 13:55 95-57-804/16/20 15:274641081
4-Chlorophenylphenyl ether ND ug/kg 04/17/20 13:55 7005-72-304/16/20 15:274641211
Chrysene ND ug/kg 04/17/20 13:55 218-01-904/16/20 15:274641351
Dibenz(a,h)anthracene ND ug/kg 04/17/20 13:55 53-70-304/16/20 15:274641861
Dibenzofuran ND ug/kg 04/17/20 13:55 132-64-904/16/20 15:274641161
1,2-Dichlorobenzene ND ug/kg 04/17/20 13:55 95-50-104/16/20 15:274641001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:W WALL Lab ID:92473782001 Collected:04/14/20 09:30 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,3-Dichlorobenzene ND ug/kg 04/17/20 13:55 541-73-104/16/20 15:274641051
1,4-Dichlorobenzene ND ug/kg 04/17/20 13:55 106-46-704/16/20 15:274641021
3,3'-Dichlorobenzidine ND ug/kg 04/17/20 13:55 91-94-104/16/20 15:279293241
2,4-Dichlorophenol ND ug/kg 04/17/20 13:55 120-83-204/16/20 15:274641531
Diethylphthalate ND ug/kg 04/17/20 13:55 84-66-204/16/20 15:274641011
2,4-Dimethylphenol ND ug/kg 04/17/20 13:55 105-67-904/16/20 15:274641161
Dimethylphthalate ND ug/kg 04/17/20 13:55 131-11-304/16/20 15:274641051
Di-n-butylphthalate ND ug/kg 04/17/20 13:55 84-74-204/16/20 15:274641151
4,6-Dinitro-2-methylphenol ND ug/kg 04/17/20 13:55 534-52-104/16/20 15:279297491
2,4-Dinitrophenol ND ug/kg 04/17/20 13:55 51-28-504/16/20 15:27232014801
2,4-Dinitrotoluene ND ug/kg 04/17/20 13:55 121-14-204/16/20 15:274641231
2,6-Dinitrotoluene ND ug/kg 04/17/20 13:55 606-20-204/16/20 15:274641211
Di-n-octylphthalate ND ug/kg 04/17/20 13:55 117-84-004/16/20 15:274642651
bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/20 13:55 117-81-704/16/20 15:274641521
Fluoranthene ND ug/kg 04/17/20 13:55 206-44-004/16/20 15:274641401
Fluorene ND ug/kg 04/17/20 13:55 86-73-704/16/20 15:274641241
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 13:55 87-68-304/16/20 15:274641131
Hexachlorobenzene ND ug/kg 04/17/20 13:55 118-74-104/16/20 15:274641181
Hexachlorocyclopentadiene ND ug/kg 04/17/20 13:55 77-47-404/16/20 15:274641861
Hexachloroethane ND ug/kg 04/17/20 13:55 67-72-104/16/20 15:274641061
Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/20 13:55 193-39-504/16/20 15:274642121
Isophorone ND ug/kg 04/17/20 13:55 78-59-104/16/20 15:274641011
1-Methylnaphthalene ND ug/kg 04/17/20 13:55 90-12-004/16/20 15:274641241
2-Methylnaphthalene ND ug/kg 04/17/20 13:55 91-57-604/16/20 15:274641181
2-Methylphenol(o-Cresol)ND ug/kg 04/17/20 13:55 95-48-704/16/20 15:274641031
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/20 13:55 15831-10-404/16/20 15:274641171
Naphthalene ND ug/kg 04/17/20 13:55 91-20-304/16/20 15:274641111
2-Nitroaniline ND ug/kg 04/17/20 13:55 88-74-404/16/20 15:2723202341
3-Nitroaniline ND ug/kg 04/17/20 13:55 99-09-204/16/20 15:2723202461
4-Nitroaniline ND ug/kg 04/17/20 13:55 100-01-604/16/20 15:279292291
Nitrobenzene ND ug/kg 04/17/20 13:55 98-95-304/16/20 15:274641111
2-Nitrophenol ND ug/kg 04/17/20 13:55 88-75-504/16/20 15:274641441
4-Nitrophenol ND ug/kg 04/17/20 13:55 100-02-704/16/20 15:2723207401
N-Nitrosodimethylamine ND ug/kg 04/17/20 13:55 62-75-904/16/20 15:274641311
N-Nitroso-di-n-propylamine ND ug/kg 04/17/20 13:55 621-64-704/16/20 15:274641301
N-Nitrosodiphenylamine ND ug/kg 04/17/20 13:55 86-30-604/16/20 15:274641181
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/20 13:55 108-60-104/16/20 15:274641291
Pentachlorophenol ND ug/kg 04/17/20 13:55 87-86-504/16/20 15:279292121
Phenanthrene ND ug/kg 04/17/20 13:55 85-01-804/16/20 15:274641171
Phenol ND ug/kg 04/17/20 13:55 108-95-204/16/20 15:274641111
Pyrene ND ug/kg 04/17/20 13:55 129-00-004/16/20 15:274641281
Pyridine ND ug/kg 04/17/20 13:55 110-86-104/16/20 15:274641181
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 13:55 120-82-104/16/20 15:274641061
2,4,5-Trichlorophenol ND ug/kg 04/17/20 13:55 95-95-404/16/20 15:274641211
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:W WALL Lab ID:92473782001 Collected:04/14/20 09:30 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,6-Trichlorophenol ND ug/kg 04/17/20 13:55 88-06-204/16/20 15:274641171
Surrogates
Nitrobenzene-d5 (S)56 %04/17/20 13:55 4165-60-004/16/20 15:2723-110 1
2-Fluorobiphenyl (S)28 %04/17/20 13:55 321-60-8 S004/16/20 15:2730-110 1
Terphenyl-d14 (S)68 %04/17/20 13:55 1718-51-004/16/20 15:2728-110 1
Phenol-d6 (S)65 %04/17/20 13:55 13127-88-304/16/20 15:2722-110 1
2-Fluorophenol (S)62 %04/17/20 13:55 367-12-404/16/20 15:2713-110 1
2,4,6-Tribromophenol (S)62 %04/17/20 13:55 118-79-604/16/20 15:2727-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone ND ug/kg 04/17/20 12:06 67-64-104/17/20 10:141059.9 1
Benzene ND ug/kg 04/17/20 12:06 71-43-204/17/20 10:145.2 0.94 1
Bromobenzene ND ug/kg 04/17/20 12:06 108-86-104/17/20 10:145.2 1.4 1
Bromochloromethane ND ug/kg 04/17/20 12:06 74-97-504/17/20 10:145.2 1.3 1
Bromodichloromethane ND ug/kg 04/17/20 12:06 75-27-404/17/20 10:145.2 1.0 1
Bromoform ND ug/kg 04/17/20 12:06 75-25-204/17/20 10:145.2 2.6 1
Bromomethane ND ug/kg 04/17/20 12:06 74-83-9 IH04/17/20 10:1410.5 2.5 1
2-Butanone (MEK)ND ug/kg 04/17/20 12:06 78-93-304/17/20 10:1410512.5 1
n-Butylbenzene ND ug/kg 04/17/20 12:06 104-51-804/17/20 10:145.2 3.0 1
sec-Butylbenzene ND ug/kg 04/17/20 12:06 135-98-804/17/20 10:145.2 2.2 1
tert-Butylbenzene ND ug/kg 04/17/20 12:06 98-06-604/17/20 10:145.2 1.8 1
Carbon tetrachloride ND ug/kg 04/17/20 12:06 56-23-504/17/20 10:145.2 1.0 1
Chlorobenzene ND ug/kg 04/17/20 12:06 108-90-704/17/20 10:145.2 1.0 1
Chloroethane ND ug/kg 04/17/20 12:06 75-00-304/17/20 10:1410.5 2.2 1
Chloroform ND ug/kg 04/17/20 12:06 67-66-304/17/20 10:145.2 1.1 1
Chloromethane ND ug/kg 04/17/20 12:06 74-87-304/17/20 10:1410.5 3.4 1
2-Chlorotoluene ND ug/kg 04/17/20 12:06 95-49-804/17/20 10:145.2 1.6 1
4-Chlorotoluene ND ug/kg 04/17/20 12:06 106-43-404/17/20 10:145.2 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/17/20 12:06 96-12-8 v104/17/20 10:145.2 2.7 1
Dibromochloromethane ND ug/kg 04/17/20 12:06 124-48-104/17/20 10:145.2 2.6 1
1,2-Dibromoethane (EDB)ND ug/kg 04/17/20 12:06 106-93-404/17/20 10:145.2 1.2 1
Dibromomethane ND ug/kg 04/17/20 12:06 74-95-304/17/20 10:145.2 1.6 1
1,2-Dichlorobenzene ND ug/kg 04/17/20 12:06 95-50-104/17/20 10:145.2 1.8 1
1,3-Dichlorobenzene ND ug/kg 04/17/20 12:06 541-73-104/17/20 10:145.2 1.9 1
1,4-Dichlorobenzene ND ug/kg 04/17/20 12:06 106-46-704/17/20 10:145.2 1.8 1
Dichlorodifluoromethane ND ug/kg 04/17/20 12:06 75-71-8 v204/17/20 10:1410.5 4.3 1
1,1-Dichloroethane ND ug/kg 04/17/20 12:06 75-34-304/17/20 10:145.2 0.77 1
1,2-Dichloroethane ND ug/kg 04/17/20 12:06 107-06-204/17/20 10:145.2 1.0 1
1,1-Dichloroethene ND ug/kg 04/17/20 12:06 75-35-404/17/20 10:145.2 1.2 1
cis-1,2-Dichloroethene ND ug/kg 04/17/20 12:06 156-59-204/17/20 10:145.2 0.91 1
trans-1,2-Dichloroethene ND ug/kg 04/17/20 12:06 156-60-504/17/20 10:145.2 1.0 1
1,2-Dichloropropane ND ug/kg 04/17/20 12:06 78-87-504/17/20 10:145.2 2.0 1
1,3-Dichloropropane ND ug/kg 04/17/20 12:06 142-28-904/17/20 10:145.2 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:W WALL Lab ID:92473782001 Collected:04/14/20 09:30 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
2,2-Dichloropropane ND ug/kg 04/17/20 12:06 594-20-704/17/20 10:145.2 0.52 1
1,1-Dichloropropene ND ug/kg 04/17/20 12:06 563-58-604/17/20 10:145.2 2.2 1
cis-1,3-Dichloropropene ND ug/kg 04/17/20 12:06 10061-01-504/17/20 10:145.2 2.4 1
trans-1,3-Dichloropropene ND ug/kg 04/17/20 12:06 10061-02-604/17/20 10:145.2 0.92 1
Diisopropyl ether ND ug/kg 04/17/20 12:06 108-20-304/17/20 10:145.2 3.0 1
Ethylbenzene ND ug/kg 04/17/20 12:06 100-41-404/17/20 10:145.2 1.1 1
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 12:06 87-68-304/17/20 10:145.2 2.6 1
2-Hexanone ND ug/kg 04/17/20 12:06 591-78-604/17/20 10:1452.4 5.4 1
Isopropylbenzene (Cumene)ND ug/kg 04/17/20 12:06 98-82-804/17/20 10:145.2 1.5 1
p-Isopropyltoluene ND ug/kg 04/17/20 12:06 99-87-604/17/20 10:145.2 2.5 1
Methylene Chloride ND ug/kg 04/17/20 12:06 75-09-2 v104/17/20 10:1421.0 6.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/17/20 12:06 108-10-104/17/20 10:1452.4 3.9 1
Methyl-tert-butyl ether ND ug/kg 04/17/20 12:06 1634-04-404/17/20 10:145.2 3.0 1
Naphthalene ND ug/kg 04/17/20 12:06 91-20-304/17/20 10:145.2 4.5 1
n-Propylbenzene ND ug/kg 04/17/20 12:06 103-65-104/17/20 10:145.2 1.8 1
Styrene ND ug/kg 04/17/20 12:06 100-42-504/17/20 10:145.2 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/17/20 12:06 630-20-604/17/20 10:145.2 1.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/17/20 12:06 79-34-504/17/20 10:145.2 1.8 1
Tetrachloroethene ND ug/kg 04/17/20 12:06 127-18-404/17/20 10:145.2 1.7 1
Toluene ND ug/kg 04/17/20 12:06 108-88-304/17/20 10:145.2 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 04/17/20 12:06 87-61-604/17/20 10:145.2 3.7 1
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 12:06 120-82-104/17/20 10:145.2 2.8 1
1,1,1-Trichloroethane ND ug/kg 04/17/20 12:06 71-55-604/17/20 10:145.2 0.91 1
1,1,2-Trichloroethane ND ug/kg 04/17/20 12:06 79-00-504/17/20 10:145.2 1.2 1
Trichloroethene ND ug/kg 04/17/20 12:06 79-01-604/17/20 10:145.2 1.4 1
Trichlorofluoromethane ND ug/kg 04/17/20 12:06 75-69-404/17/20 10:145.2 1.2 1
1,2,3-Trichloropropane ND ug/kg 04/17/20 12:06 96-18-404/17/20 10:145.2 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 04/17/20 12:06 95-63-604/17/20 10:145.2 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/17/20 12:06 108-67-804/17/20 10:145.2 1.8 1
Vinyl acetate ND ug/kg 04/17/20 12:06 108-05-404/17/20 10:1452.4 17.1 1
Vinyl chloride ND ug/kg 04/17/20 12:06 75-01-4 v204/17/20 10:1410.5 2.0 1
Xylene (Total)ND ug/kg 04/17/20 12:06 1330-20-704/17/20 10:1410.5 3.7 1
m&p-Xylene ND ug/kg 04/17/20 12:06 179601-23-104/17/20 10:1410.5 2.5 1
o-Xylene ND ug/kg 04/17/20 12:06 95-47-604/17/20 10:145.2 1.2 1
Surrogates
Toluene-d8 (S)101 %04/17/20 12:06 2037-26-504/17/20 10:1470-130 1
4-Bromofluorobenzene (S)106 %04/17/20 12:06 460-00-404/17/20 10:1470-130 1
1,2-Dichloroethane-d4 (S)98 %04/17/20 12:06 17060-07-004/17/20 10:1470-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.7 %04/16/20 13:290.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:W WALL Lab ID:92473782001 Collected:04/14/20 09:30 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 72.8 %04/20/20 07:5504/20/20 07:491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:E WALL Lab ID:92473782002 Collected:04/14/20 10:00 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/17/20 10:04 N204/16/20 09:1814.3 14.3 1
Aliphatic (C19-C36)ND mg/kg 04/17/20 10:04 N204/16/20 09:1814.3 14.3 1
Aromatic (C11-C22)ND mg/kg 04/17/20 10:04 N204/16/20 09:1814.3 14.3 1
Surrogates
Nonatriacontane (S)92 %04/17/20 10:04 7194-86-704/16/20 09:1840-140 1
o-Terphenyl (S)80 %04/17/20 10:04 84-15-104/16/20 09:1840-140 1
2-Fluorobiphenyl (S)95 %04/17/20 10:04 321-60-804/16/20 09:1840-140 1
2-Bromonaphthalene (S)98 %04/17/20 10:04 580-13-204/16/20 09:1840-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND mg/kg 04/18/20 13:3404/14/20 10:007.10 2.37 1
Aliphatic (C09-C12)ND mg/kg 04/18/20 13:3404/14/20 10:007.10 2.37 1
Aromatic (C09-C10),Unadjusted ND mg/kg 04/18/20 13:34 TPHC9C10A04/14/20 10:007.10 2.37 1
Surrogates
2,5-Dibromotoluene (FID)105 %04/18/20 13:34 615-59-8FID04/14/20 10:0070.0-130 1
2,5-Dibromotoluene (PID)108 %04/18/20 13:34 615-59-8PID04/14/20 10:0070.0-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/17/20 12:04 83-32-904/16/20 15:274631191
Acenaphthylene ND ug/kg 04/17/20 12:04 208-96-804/16/20 15:274631101
Aniline ND ug/kg 04/17/20 12:04 62-53-304/16/20 15:274631041
Anthracene ND ug/kg 04/17/20 12:04 120-12-704/16/20 15:274631201
Benzo(a)anthracene ND ug/kg 04/17/20 12:04 56-55-304/16/20 15:274631471
Benzo(a)pyrene ND ug/kg 04/17/20 12:04 50-32-804/16/20 15:274632011
Benzo(b)fluoranthene ND ug/kg 04/17/20 12:04 205-99-204/16/20 15:274631871
Benzo(g,h,i)perylene ND ug/kg 04/17/20 12:04 191-24-204/16/20 15:274631811
Benzo(k)fluoranthene ND ug/kg 04/17/20 12:04 207-08-904/16/20 15:274631951
Benzoic Acid ND ug/kg 04/17/20 12:04 65-85-004/16/20 15:2723104991
Benzyl alcohol ND ug/kg 04/17/20 12:04 100-51-604/16/20 15:279262461
4-Bromophenylphenyl ether ND ug/kg 04/17/20 12:04 101-55-304/16/20 15:274631221
Butylbenzylphthalate ND ug/kg 04/17/20 12:04 85-68-704/16/20 15:274631231
4-Chloro-3-methylphenol ND ug/kg 04/17/20 12:04 59-50-704/16/20 15:279262821
4-Chloroaniline ND ug/kg 04/17/20 12:04 106-47-804/16/20 15:279262831
bis(2-Chloroethoxy)methane ND ug/kg 04/17/20 12:04 111-91-104/16/20 15:274631241
bis(2-Chloroethyl) ether ND ug/kg 04/17/20 12:04 111-44-404/16/20 15:2746398.4 1
2-Chloronaphthalene ND ug/kg 04/17/20 12:04 91-58-704/16/20 15:274631031
2-Chlorophenol ND ug/kg 04/17/20 12:04 95-57-804/16/20 15:274631081
4-Chlorophenylphenyl ether ND ug/kg 04/17/20 12:04 7005-72-304/16/20 15:274631201
Chrysene ND ug/kg 04/17/20 12:04 218-01-904/16/20 15:274631341
Dibenz(a,h)anthracene ND ug/kg 04/17/20 12:04 53-70-304/16/20 15:274631851
Dibenzofuran ND ug/kg 04/17/20 12:04 132-64-904/16/20 15:274631161
1,2-Dichlorobenzene ND ug/kg 04/17/20 12:04 95-50-104/16/20 15:274631001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:E WALL Lab ID:92473782002 Collected:04/14/20 10:00 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,3-Dichlorobenzene ND ug/kg 04/17/20 12:04 541-73-104/16/20 15:274631041
1,4-Dichlorobenzene ND ug/kg 04/17/20 12:04 106-46-704/16/20 15:274631021
3,3'-Dichlorobenzidine ND ug/kg 04/17/20 12:04 91-94-104/16/20 15:279263231
2,4-Dichlorophenol ND ug/kg 04/17/20 12:04 120-83-204/16/20 15:274631531
Diethylphthalate ND ug/kg 04/17/20 12:04 84-66-204/16/20 15:274631001
2,4-Dimethylphenol ND ug/kg 04/17/20 12:04 105-67-904/16/20 15:274631151
Dimethylphthalate ND ug/kg 04/17/20 12:04 131-11-304/16/20 15:274631051
Di-n-butylphthalate ND ug/kg 04/17/20 12:04 84-74-204/16/20 15:274631141
4,6-Dinitro-2-methylphenol ND ug/kg 04/17/20 12:04 534-52-104/16/20 15:279267461
2,4-Dinitrophenol ND ug/kg 04/17/20 12:04 51-28-504/16/20 15:27231014801
2,4-Dinitrotoluene ND ug/kg 04/17/20 12:04 121-14-204/16/20 15:274631231
2,6-Dinitrotoluene ND ug/kg 04/17/20 12:04 606-20-204/16/20 15:274631211
Di-n-octylphthalate ND ug/kg 04/17/20 12:04 117-84-004/16/20 15:274632641
bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/20 12:04 117-81-704/16/20 15:274631521
Fluoranthene ND ug/kg 04/17/20 12:04 206-44-004/16/20 15:274631401
Fluorene ND ug/kg 04/17/20 12:04 86-73-704/16/20 15:274631241
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 12:04 87-68-304/16/20 15:274631131
Hexachlorobenzene ND ug/kg 04/17/20 12:04 118-74-104/16/20 15:274631181
Hexachlorocyclopentadiene ND ug/kg 04/17/20 12:04 77-47-404/16/20 15:274631851
Hexachloroethane ND ug/kg 04/17/20 12:04 67-72-104/16/20 15:274631061
Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/20 12:04 193-39-504/16/20 15:274632121
Isophorone ND ug/kg 04/17/20 12:04 78-59-104/16/20 15:274631011
1-Methylnaphthalene ND ug/kg 04/17/20 12:04 90-12-004/16/20 15:274631231
2-Methylnaphthalene ND ug/kg 04/17/20 12:04 91-57-604/16/20 15:274631181
2-Methylphenol(o-Cresol)ND ug/kg 04/17/20 12:04 95-48-704/16/20 15:274631031
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/20 12:04 15831-10-404/16/20 15:274631161
Naphthalene ND ug/kg 04/17/20 12:04 91-20-304/16/20 15:274631111
2-Nitroaniline ND ug/kg 04/17/20 12:04 88-74-404/16/20 15:2723102331
3-Nitroaniline ND ug/kg 04/17/20 12:04 99-09-204/16/20 15:2723102461
4-Nitroaniline ND ug/kg 04/17/20 12:04 100-01-604/16/20 15:279262291
Nitrobenzene ND ug/kg 04/17/20 12:04 98-95-304/16/20 15:274631111
2-Nitrophenol ND ug/kg 04/17/20 12:04 88-75-504/16/20 15:274631431
4-Nitrophenol ND ug/kg 04/17/20 12:04 100-02-704/16/20 15:2723107381
N-Nitrosodimethylamine ND ug/kg 04/17/20 12:04 62-75-904/16/20 15:274631301
N-Nitroso-di-n-propylamine ND ug/kg 04/17/20 12:04 621-64-704/16/20 15:274631301
N-Nitrosodiphenylamine ND ug/kg 04/17/20 12:04 86-30-604/16/20 15:274631181
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/20 12:04 108-60-104/16/20 15:274631291
Pentachlorophenol ND ug/kg 04/17/20 12:04 87-86-504/16/20 15:279262121
Phenanthrene ND ug/kg 04/17/20 12:04 85-01-804/16/20 15:274631171
Phenol ND ug/kg 04/17/20 12:04 108-95-204/16/20 15:274631111
Pyrene ND ug/kg 04/17/20 12:04 129-00-004/16/20 15:274631271
Pyridine ND ug/kg 04/17/20 12:04 110-86-104/16/20 15:274631171
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 12:04 120-82-104/16/20 15:274631061
2,4,5-Trichlorophenol ND ug/kg 04/17/20 12:04 95-95-404/16/20 15:274631201
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:E WALL Lab ID:92473782002 Collected:04/14/20 10:00 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,6-Trichlorophenol ND ug/kg 04/17/20 12:04 88-06-204/16/20 15:274631161
Surrogates
Nitrobenzene-d5 (S)69 %04/17/20 12:04 4165-60-004/16/20 15:2723-110 1
2-Fluorobiphenyl (S)61 %04/17/20 12:04 321-60-804/16/20 15:2730-110 1
Terphenyl-d14 (S)92 %04/17/20 12:04 1718-51-004/16/20 15:2728-110 1
Phenol-d6 (S)72 %04/17/20 12:04 13127-88-304/16/20 15:2722-110 1
2-Fluorophenol (S)69 %04/17/20 12:04 367-12-404/16/20 15:2713-110 1
2,4,6-Tribromophenol (S)73 %04/17/20 12:04 118-79-604/16/20 15:2727-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone 63.0J ug/kg 04/17/20 12:30 67-64-104/17/20 10:1411010.4 1
Benzene ND ug/kg 04/17/20 12:30 71-43-204/17/20 10:145.5 0.99 1
Bromobenzene ND ug/kg 04/17/20 12:30 108-86-104/17/20 10:145.5 1.5 1
Bromochloromethane ND ug/kg 04/17/20 12:30 74-97-504/17/20 10:145.5 1.4 1
Bromodichloromethane ND ug/kg 04/17/20 12:30 75-27-404/17/20 10:145.5 1.1 1
Bromoform ND ug/kg 04/17/20 12:30 75-25-204/17/20 10:145.5 2.7 1
Bromomethane ND ug/kg 04/17/20 12:30 74-83-9 IH04/17/20 10:1411.0 2.6 1
2-Butanone (MEK)ND ug/kg 04/17/20 12:30 78-93-304/17/20 10:1411013.1 1
n-Butylbenzene ND ug/kg 04/17/20 12:30 104-51-804/17/20 10:145.5 3.1 1
sec-Butylbenzene ND ug/kg 04/17/20 12:30 135-98-804/17/20 10:145.5 2.3 1
tert-Butylbenzene ND ug/kg 04/17/20 12:30 98-06-604/17/20 10:145.5 1.9 1
Carbon tetrachloride ND ug/kg 04/17/20 12:30 56-23-504/17/20 10:145.5 1.1 1
Chlorobenzene ND ug/kg 04/17/20 12:30 108-90-704/17/20 10:145.5 1.1 1
Chloroethane ND ug/kg 04/17/20 12:30 75-00-304/17/20 10:1411.0 2.3 1
Chloroform ND ug/kg 04/17/20 12:30 67-66-304/17/20 10:145.5 1.2 1
Chloromethane ND ug/kg 04/17/20 12:30 74-87-304/17/20 10:1411.0 3.6 1
2-Chlorotoluene ND ug/kg 04/17/20 12:30 95-49-804/17/20 10:145.5 1.7 1
4-Chlorotoluene ND ug/kg 04/17/20 12:30 106-43-404/17/20 10:145.5 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/17/20 12:30 96-12-8 v104/17/20 10:145.5 2.8 1
Dibromochloromethane ND ug/kg 04/17/20 12:30 124-48-104/17/20 10:145.5 2.8 1
1,2-Dibromoethane (EDB)ND ug/kg 04/17/20 12:30 106-93-404/17/20 10:145.5 1.2 1
Dibromomethane ND ug/kg 04/17/20 12:30 74-95-304/17/20 10:145.5 1.6 1
1,2-Dichlorobenzene ND ug/kg 04/17/20 12:30 95-50-104/17/20 10:145.5 1.9 1
1,3-Dichlorobenzene ND ug/kg 04/17/20 12:30 541-73-104/17/20 10:145.5 2.0 1
1,4-Dichlorobenzene ND ug/kg 04/17/20 12:30 106-46-704/17/20 10:145.5 1.9 1
Dichlorodifluoromethane ND ug/kg 04/17/20 12:30 75-71-8 v304/17/20 10:1411.0 4.5 1
1,1-Dichloroethane ND ug/kg 04/17/20 12:30 75-34-304/17/20 10:145.5 0.81 1
1,2-Dichloroethane ND ug/kg 04/17/20 12:30 107-06-204/17/20 10:145.5 1.1 1
1,1-Dichloroethene ND ug/kg 04/17/20 12:30 75-35-404/17/20 10:145.5 1.3 1
cis-1,2-Dichloroethene ND ug/kg 04/17/20 12:30 156-59-204/17/20 10:145.5 0.96 1
trans-1,2-Dichloroethene ND ug/kg 04/17/20 12:30 156-60-504/17/20 10:145.5 1.1 1
1,2-Dichloropropane ND ug/kg 04/17/20 12:30 78-87-504/17/20 10:145.5 2.1 1
1,3-Dichloropropane ND ug/kg 04/17/20 12:30 142-28-904/17/20 10:145.5 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:E WALL Lab ID:92473782002 Collected:04/14/20 10:00 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
2,2-Dichloropropane ND ug/kg 04/17/20 12:30 594-20-704/17/20 10:145.5 0.55 1
1,1-Dichloropropene ND ug/kg 04/17/20 12:30 563-58-604/17/20 10:145.5 2.3 1
cis-1,3-Dichloropropene ND ug/kg 04/17/20 12:30 10061-01-504/17/20 10:145.5 2.5 1
trans-1,3-Dichloropropene ND ug/kg 04/17/20 12:30 10061-02-604/17/20 10:145.5 0.97 1
Diisopropyl ether ND ug/kg 04/17/20 12:30 108-20-304/17/20 10:145.5 3.2 1
Ethylbenzene ND ug/kg 04/17/20 12:30 100-41-404/17/20 10:145.5 1.2 1
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 12:30 87-68-304/17/20 10:145.5 2.7 1
2-Hexanone ND ug/kg 04/17/20 12:30 591-78-604/17/20 10:1455.2 5.7 1
Isopropylbenzene (Cumene)ND ug/kg 04/17/20 12:30 98-82-804/17/20 10:145.5 1.6 1
p-Isopropyltoluene ND ug/kg 04/17/20 12:30 99-87-604/17/20 10:145.5 2.7 1
Methylene Chloride ND ug/kg 04/17/20 12:30 75-09-2 v104/17/20 10:1422.1 6.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/17/20 12:30 108-10-104/17/20 10:1455.2 4.1 1
Methyl-tert-butyl ether ND ug/kg 04/17/20 12:30 1634-04-404/17/20 10:145.5 3.2 1
Naphthalene ND ug/kg 04/17/20 12:30 91-20-304/17/20 10:145.5 4.7 1
n-Propylbenzene ND ug/kg 04/17/20 12:30 103-65-104/17/20 10:145.5 1.8 1
Styrene ND ug/kg 04/17/20 12:30 100-42-504/17/20 10:145.5 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/17/20 12:30 630-20-604/17/20 10:145.5 1.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/17/20 12:30 79-34-504/17/20 10:145.5 1.9 1
Tetrachloroethene ND ug/kg 04/17/20 12:30 127-18-404/17/20 10:145.5 1.7 1
Toluene ND ug/kg 04/17/20 12:30 108-88-304/17/20 10:145.5 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 04/17/20 12:30 87-61-604/17/20 10:145.5 3.9 1
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 12:30 120-82-104/17/20 10:145.5 2.9 1
1,1,1-Trichloroethane ND ug/kg 04/17/20 12:30 71-55-604/17/20 10:145.5 0.96 1
1,1,2-Trichloroethane ND ug/kg 04/17/20 12:30 79-00-504/17/20 10:145.5 1.2 1
Trichloroethene ND ug/kg 04/17/20 12:30 79-01-604/17/20 10:145.5 1.4 1
Trichlorofluoromethane ND ug/kg 04/17/20 12:30 75-69-404/17/20 10:145.5 1.3 1
1,2,3-Trichloropropane ND ug/kg 04/17/20 12:30 96-18-404/17/20 10:145.5 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 04/17/20 12:30 95-63-604/17/20 10:145.5 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 04/17/20 12:30 108-67-804/17/20 10:145.5 1.8 1
Vinyl acetate ND ug/kg 04/17/20 12:30 108-05-404/17/20 10:1455.2 18.0 1
Vinyl chloride ND ug/kg 04/17/20 12:30 75-01-4 v304/17/20 10:1411.0 2.1 1
Xylene (Total)ND ug/kg 04/17/20 12:30 1330-20-704/17/20 10:1411.0 3.9 1
m&p-Xylene ND ug/kg 04/17/20 12:30 179601-23-104/17/20 10:1411.0 2.6 1
o-Xylene ND ug/kg 04/17/20 12:30 95-47-604/17/20 10:145.5 1.3 1
Surrogates
Toluene-d8 (S)101 %04/17/20 12:30 2037-26-504/17/20 10:1470-130 1
4-Bromofluorobenzene (S)94 %04/17/20 12:30 460-00-404/17/20 10:1470-130 1
1,2-Dichloroethane-d4 (S)98 %04/17/20 12:30 17060-07-004/17/20 10:1470-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 29.4 %04/16/20 13:290.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:E WALL Lab ID:92473782002 Collected:04/14/20 10:00 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 70.4 %04/20/20 07:5504/20/20 07:491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:S WALL Lab ID:92473782003 Collected:04/14/20 09:40 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/17/20 10:31 N204/16/20 09:1814.6 14.6 1
Aliphatic (C19-C36)ND mg/kg 04/17/20 10:31 N204/16/20 09:1814.6 14.6 1
Aromatic (C11-C22)ND mg/kg 04/17/20 10:31 N204/16/20 09:1814.6 14.6 1
Surrogates
Nonatriacontane (S)78 %04/17/20 10:31 7194-86-704/16/20 09:1840-140 1
o-Terphenyl (S)83 %04/17/20 10:31 84-15-104/16/20 09:1840-140 1
2-Fluorobiphenyl (S)99 %04/17/20 10:31 321-60-804/16/20 09:1840-140 1
2-Bromonaphthalene (S)102 %04/17/20 10:31 580-13-204/16/20 09:1840-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND mg/kg 04/18/20 14:0704/14/20 09:407.20 2.40 1
Aliphatic (C09-C12)ND mg/kg 04/18/20 14:0704/14/20 09:407.20 2.40 1
Aromatic (C09-C10),Unadjusted ND mg/kg 04/18/20 14:07 TPHC9C10A04/14/20 09:407.20 2.40 1
Surrogates
2,5-Dibromotoluene (FID)103 %04/18/20 14:07 615-59-8FID04/14/20 09:4070.0-130 1
2,5-Dibromotoluene (PID)106 %04/18/20 14:07 615-59-8PID04/14/20 09:4070.0-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/17/20 12:32 83-32-904/16/20 15:274801231
Acenaphthylene ND ug/kg 04/17/20 12:32 208-96-804/16/20 15:274801141
Aniline ND ug/kg 04/17/20 12:32 62-53-304/16/20 15:274801081
Anthracene ND ug/kg 04/17/20 12:32 120-12-704/16/20 15:274801241
Benzo(a)anthracene ND ug/kg 04/17/20 12:32 56-55-304/16/20 15:274801531
Benzo(a)pyrene ND ug/kg 04/17/20 12:32 50-32-804/16/20 15:274802081
Benzo(b)fluoranthene ND ug/kg 04/17/20 12:32 205-99-204/16/20 15:274801931
Benzo(g,h,i)perylene ND ug/kg 04/17/20 12:32 191-24-204/16/20 15:274801881
Benzo(k)fluoranthene ND ug/kg 04/17/20 12:32 207-08-904/16/20 15:274802021
Benzoic Acid ND ug/kg 04/17/20 12:32 65-85-004/16/20 15:2724005171
Benzyl alcohol ND ug/kg 04/17/20 12:32 100-51-604/16/20 15:279592541
4-Bromophenylphenyl ether ND ug/kg 04/17/20 12:32 101-55-304/16/20 15:274801261
Butylbenzylphthalate ND ug/kg 04/17/20 12:32 85-68-704/16/20 15:274801281
4-Chloro-3-methylphenol ND ug/kg 04/17/20 12:32 59-50-704/16/20 15:279592921
4-Chloroaniline ND ug/kg 04/17/20 12:32 106-47-804/16/20 15:279592941
bis(2-Chloroethoxy)methane ND ug/kg 04/17/20 12:32 111-91-104/16/20 15:274801281
bis(2-Chloroethyl) ether ND ug/kg 04/17/20 12:32 111-44-404/16/20 15:274801021
2-Chloronaphthalene ND ug/kg 04/17/20 12:32 91-58-704/16/20 15:274801071
2-Chlorophenol ND ug/kg 04/17/20 12:32 95-57-804/16/20 15:274801121
4-Chlorophenylphenyl ether ND ug/kg 04/17/20 12:32 7005-72-304/16/20 15:274801251
Chrysene ND ug/kg 04/17/20 12:32 218-01-904/16/20 15:274801391
Dibenz(a,h)anthracene ND ug/kg 04/17/20 12:32 53-70-304/16/20 15:274801921
Dibenzofuran ND ug/kg 04/17/20 12:32 132-64-904/16/20 15:274801201
1,2-Dichlorobenzene ND ug/kg 04/17/20 12:32 95-50-104/16/20 15:274801041
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:S WALL Lab ID:92473782003 Collected:04/14/20 09:40 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,3-Dichlorobenzene ND ug/kg 04/17/20 12:32 541-73-104/16/20 15:274801081
1,4-Dichlorobenzene ND ug/kg 04/17/20 12:32 106-46-704/16/20 15:274801061
3,3'-Dichlorobenzidine ND ug/kg 04/17/20 12:32 91-94-104/16/20 15:279593341
2,4-Dichlorophenol ND ug/kg 04/17/20 12:32 120-83-204/16/20 15:274801581
Diethylphthalate ND ug/kg 04/17/20 12:32 84-66-204/16/20 15:274801041
2,4-Dimethylphenol ND ug/kg 04/17/20 12:32 105-67-904/16/20 15:274801191
Dimethylphthalate ND ug/kg 04/17/20 12:32 131-11-304/16/20 15:274801081
Di-n-butylphthalate ND ug/kg 04/17/20 12:32 84-74-204/16/20 15:274801181
4,6-Dinitro-2-methylphenol ND ug/kg 04/17/20 12:32 534-52-104/16/20 15:279597731
2,4-Dinitrophenol ND ug/kg 04/17/20 12:32 51-28-504/16/20 15:27240015301
2,4-Dinitrotoluene ND ug/kg 04/17/20 12:32 121-14-204/16/20 15:274801271
2,6-Dinitrotoluene ND ug/kg 04/17/20 12:32 606-20-204/16/20 15:274801251
Di-n-octylphthalate ND ug/kg 04/17/20 12:32 117-84-004/16/20 15:274802731
bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/20 12:32 117-81-704/16/20 15:274801571
Fluoranthene ND ug/kg 04/17/20 12:32 206-44-004/16/20 15:274801451
Fluorene ND ug/kg 04/17/20 12:32 86-73-704/16/20 15:274801281
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 12:32 87-68-304/16/20 15:274801171
Hexachlorobenzene ND ug/kg 04/17/20 12:32 118-74-104/16/20 15:274801221
Hexachlorocyclopentadiene ND ug/kg 04/17/20 12:32 77-47-404/16/20 15:274801921
Hexachloroethane ND ug/kg 04/17/20 12:32 67-72-104/16/20 15:274801091
Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/20 12:32 193-39-504/16/20 15:274802191
Isophorone ND ug/kg 04/17/20 12:32 78-59-104/16/20 15:274801041
1-Methylnaphthalene ND ug/kg 04/17/20 12:32 90-12-004/16/20 15:274801281
2-Methylnaphthalene ND ug/kg 04/17/20 12:32 91-57-604/16/20 15:274801221
2-Methylphenol(o-Cresol)ND ug/kg 04/17/20 12:32 95-48-704/16/20 15:274801061
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/20 12:32 15831-10-404/16/20 15:274801211
Naphthalene ND ug/kg 04/17/20 12:32 91-20-304/16/20 15:274801151
2-Nitroaniline ND ug/kg 04/17/20 12:32 88-74-404/16/20 15:2724002411
3-Nitroaniline ND ug/kg 04/17/20 12:32 99-09-204/16/20 15:2724002541
4-Nitroaniline ND ug/kg 04/17/20 12:32 100-01-604/16/20 15:279592371
Nitrobenzene ND ug/kg 04/17/20 12:32 98-95-304/16/20 15:274801151
2-Nitrophenol ND ug/kg 04/17/20 12:32 88-75-504/16/20 15:274801481
4-Nitrophenol ND ug/kg 04/17/20 12:32 100-02-704/16/20 15:2724007651
N-Nitrosodimethylamine ND ug/kg 04/17/20 12:32 62-75-904/16/20 15:274801351
N-Nitroso-di-n-propylamine ND ug/kg 04/17/20 12:32 621-64-704/16/20 15:274801341
N-Nitrosodiphenylamine ND ug/kg 04/17/20 12:32 86-30-604/16/20 15:274801221
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/20 12:32 108-60-104/16/20 15:274801331
Pentachlorophenol ND ug/kg 04/17/20 12:32 87-86-504/16/20 15:279592191
Phenanthrene ND ug/kg 04/17/20 12:32 85-01-804/16/20 15:274801211
Phenol ND ug/kg 04/17/20 12:32 108-95-204/16/20 15:274801151
Pyrene ND ug/kg 04/17/20 12:32 129-00-004/16/20 15:274801321
Pyridine ND ug/kg 04/17/20 12:32 110-86-104/16/20 15:274801211
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 12:32 120-82-104/16/20 15:274801101
2,4,5-Trichlorophenol ND ug/kg 04/17/20 12:32 95-95-404/16/20 15:274801251
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:S WALL Lab ID:92473782003 Collected:04/14/20 09:40 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,6-Trichlorophenol ND ug/kg 04/17/20 12:32 88-06-204/16/20 15:274801211
Surrogates
Nitrobenzene-d5 (S)66 %04/17/20 12:32 4165-60-004/16/20 15:2723-110 1
2-Fluorobiphenyl (S)60 %04/17/20 12:32 321-60-804/16/20 15:2730-110 1
Terphenyl-d14 (S)83 %04/17/20 12:32 1718-51-004/16/20 15:2728-110 1
Phenol-d6 (S)63 %04/17/20 12:32 13127-88-304/16/20 15:2722-110 1
2-Fluorophenol (S)64 %04/17/20 12:32 367-12-404/16/20 15:2713-110 1
2,4,6-Tribromophenol (S)67 %04/17/20 12:32 118-79-604/16/20 15:2727-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone 70.0J ug/kg 04/17/20 12:54 67-64-104/17/20 10:1411010.4 1
Benzene ND ug/kg 04/17/20 12:54 71-43-204/17/20 10:145.5 0.99 1
Bromobenzene ND ug/kg 04/17/20 12:54 108-86-104/17/20 10:145.5 1.5 1
Bromochloromethane ND ug/kg 04/17/20 12:54 74-97-504/17/20 10:145.5 1.4 1
Bromodichloromethane ND ug/kg 04/17/20 12:54 75-27-404/17/20 10:145.5 1.1 1
Bromoform ND ug/kg 04/17/20 12:54 75-25-204/17/20 10:145.5 2.7 1
Bromomethane ND ug/kg 04/17/20 12:54 74-83-9 IH04/17/20 10:1411.0 2.6 1
2-Butanone (MEK)ND ug/kg 04/17/20 12:54 78-93-304/17/20 10:1411013.1 1
n-Butylbenzene ND ug/kg 04/17/20 12:54 104-51-804/17/20 10:145.5 3.1 1
sec-Butylbenzene ND ug/kg 04/17/20 12:54 135-98-804/17/20 10:145.5 2.3 1
tert-Butylbenzene ND ug/kg 04/17/20 12:54 98-06-604/17/20 10:145.5 1.9 1
Carbon tetrachloride ND ug/kg 04/17/20 12:54 56-23-504/17/20 10:145.5 1.1 1
Chlorobenzene ND ug/kg 04/17/20 12:54 108-90-704/17/20 10:145.5 1.1 1
Chloroethane ND ug/kg 04/17/20 12:54 75-00-304/17/20 10:1411.0 2.3 1
Chloroform ND ug/kg 04/17/20 12:54 67-66-304/17/20 10:145.5 1.2 1
Chloromethane ND ug/kg 04/17/20 12:54 74-87-304/17/20 10:1411.0 3.6 1
2-Chlorotoluene ND ug/kg 04/17/20 12:54 95-49-804/17/20 10:145.5 1.7 1
4-Chlorotoluene ND ug/kg 04/17/20 12:54 106-43-404/17/20 10:145.5 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/17/20 12:54 96-12-804/17/20 10:145.5 2.8 1
Dibromochloromethane ND ug/kg 04/17/20 12:54 124-48-104/17/20 10:145.5 2.8 1
1,2-Dibromoethane (EDB)ND ug/kg 04/17/20 12:54 106-93-404/17/20 10:145.5 1.2 1
Dibromomethane ND ug/kg 04/17/20 12:54 74-95-304/17/20 10:145.5 1.6 1
1,2-Dichlorobenzene ND ug/kg 04/17/20 12:54 95-50-104/17/20 10:145.5 1.9 1
1,3-Dichlorobenzene ND ug/kg 04/17/20 12:54 541-73-104/17/20 10:145.5 2.0 1
1,4-Dichlorobenzene ND ug/kg 04/17/20 12:54 106-46-704/17/20 10:145.5 1.9 1
Dichlorodifluoromethane ND ug/kg 04/17/20 12:54 75-71-804/17/20 10:1411.0 4.5 1
1,1-Dichloroethane ND ug/kg 04/17/20 12:54 75-34-304/17/20 10:145.5 0.81 1
1,2-Dichloroethane ND ug/kg 04/17/20 12:54 107-06-204/17/20 10:145.5 1.1 1
1,1-Dichloroethene ND ug/kg 04/17/20 12:54 75-35-404/17/20 10:145.5 1.3 1
cis-1,2-Dichloroethene ND ug/kg 04/17/20 12:54 156-59-204/17/20 10:145.5 0.96 1
trans-1,2-Dichloroethene ND ug/kg 04/17/20 12:54 156-60-504/17/20 10:145.5 1.1 1
1,2-Dichloropropane ND ug/kg 04/17/20 12:54 78-87-504/17/20 10:145.5 2.1 1
1,3-Dichloropropane ND ug/kg 04/17/20 12:54 142-28-904/17/20 10:145.5 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:S WALL Lab ID:92473782003 Collected:04/14/20 09:40 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
2,2-Dichloropropane ND ug/kg 04/17/20 12:54 594-20-704/17/20 10:145.5 0.54 1
1,1-Dichloropropene ND ug/kg 04/17/20 12:54 563-58-604/17/20 10:145.5 2.3 1
cis-1,3-Dichloropropene ND ug/kg 04/17/20 12:54 10061-01-504/17/20 10:145.5 2.5 1
trans-1,3-Dichloropropene ND ug/kg 04/17/20 12:54 10061-02-604/17/20 10:145.5 0.96 1
Diisopropyl ether ND ug/kg 04/17/20 12:54 108-20-304/17/20 10:145.5 3.2 1
Ethylbenzene ND ug/kg 04/17/20 12:54 100-41-404/17/20 10:145.5 1.2 1
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 12:54 87-68-304/17/20 10:145.5 2.7 1
2-Hexanone ND ug/kg 04/17/20 12:54 591-78-604/17/20 10:1455.1 5.7 1
Isopropylbenzene (Cumene)ND ug/kg 04/17/20 12:54 98-82-804/17/20 10:145.5 1.6 1
p-Isopropyltoluene ND ug/kg 04/17/20 12:54 99-87-604/17/20 10:145.5 2.7 1
Methylene Chloride ND ug/kg 04/17/20 12:54 75-09-204/17/20 10:1422.1 6.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/17/20 12:54 108-10-104/17/20 10:1455.1 4.1 1
Methyl-tert-butyl ether ND ug/kg 04/17/20 12:54 1634-04-404/17/20 10:145.5 3.2 1
Naphthalene ND ug/kg 04/17/20 12:54 91-20-304/17/20 10:145.5 4.7 1
n-Propylbenzene ND ug/kg 04/17/20 12:54 103-65-104/17/20 10:145.5 1.8 1
Styrene ND ug/kg 04/17/20 12:54 100-42-504/17/20 10:145.5 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/17/20 12:54 630-20-604/17/20 10:145.5 1.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/17/20 12:54 79-34-504/17/20 10:145.5 1.9 1
Tetrachloroethene ND ug/kg 04/17/20 12:54 127-18-404/17/20 10:145.5 1.7 1
Toluene ND ug/kg 04/17/20 12:54 108-88-304/17/20 10:145.5 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 04/17/20 12:54 87-61-604/17/20 10:145.5 3.9 1
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 12:54 120-82-104/17/20 10:145.5 2.9 1
1,1,1-Trichloroethane ND ug/kg 04/17/20 12:54 71-55-604/17/20 10:145.5 0.96 1
1,1,2-Trichloroethane ND ug/kg 04/17/20 12:54 79-00-504/17/20 10:145.5 1.2 1
Trichloroethene ND ug/kg 04/17/20 12:54 79-01-604/17/20 10:145.5 1.4 1
Trichlorofluoromethane ND ug/kg 04/17/20 12:54 75-69-404/17/20 10:145.5 1.3 1
1,2,3-Trichloropropane ND ug/kg 04/17/20 12:54 96-18-404/17/20 10:145.5 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 04/17/20 12:54 95-63-604/17/20 10:145.5 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 04/17/20 12:54 108-67-804/17/20 10:145.5 1.8 1
Vinyl acetate ND ug/kg 04/17/20 12:54 108-05-404/17/20 10:1455.1 18.0 1
Vinyl chloride ND ug/kg 04/17/20 12:54 75-01-404/17/20 10:1411.0 2.1 1
Xylene (Total)ND ug/kg 04/17/20 12:54 1330-20-704/17/20 10:1411.0 3.9 1
m&p-Xylene ND ug/kg 04/17/20 12:54 179601-23-104/17/20 10:1411.0 2.6 1
o-Xylene ND ug/kg 04/17/20 12:54 95-47-604/17/20 10:145.5 1.3 1
Surrogates
Toluene-d8 (S)101 %04/17/20 12:54 2037-26-504/17/20 10:1470-130 1
4-Bromofluorobenzene (S)94 %04/17/20 12:54 460-00-404/17/20 10:1470-130 1
1,2-Dichloroethane-d4 (S)98 %04/17/20 12:54 17060-07-004/17/20 10:1470-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 31.0 %04/16/20 14:410.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:S WALL Lab ID:92473782003 Collected:04/14/20 09:40 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 69.5 %04/20/20 07:5504/20/20 07:491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:N WALL Lab ID:92473782004 Collected:04/14/20 09:50 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/17/20 10:59 N204/16/20 09:1814.5 14.5 1
Aliphatic (C19-C36)ND mg/kg 04/17/20 10:59 N204/16/20 09:1814.5 14.5 1
Aromatic (C11-C22)ND mg/kg 04/17/20 10:59 N204/16/20 09:1814.5 14.5 1
Surrogates
Nonatriacontane (S)60 %04/17/20 10:59 7194-86-704/16/20 09:1840-140 1
o-Terphenyl (S)65 %04/17/20 10:59 84-15-104/16/20 09:1840-140 1
2-Fluorobiphenyl (S)94 %04/17/20 10:59 321-60-804/16/20 09:1840-140 1
2-Bromonaphthalene (S)96 %04/17/20 10:59 580-13-204/16/20 09:1840-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND mg/kg 04/18/20 14:4004/14/20 09:507.63 2.53 1.06
Aliphatic (C09-C12)ND mg/kg 04/18/20 14:4004/14/20 09:507.63 2.53 1.06
Aromatic (C09-C10),Unadjusted 2.58J mg/kg 04/18/20 14:40 TPHC9C10A J04/14/20 09:507.63 2.53 1.06
Surrogates
2,5-Dibromotoluene (FID)101 %04/18/20 14:40 615-59-8FID04/14/20 09:5070.0-130 1.06
2,5-Dibromotoluene (PID)105 %04/18/20 14:40 615-59-8PID04/14/20 09:5070.0-130 1.06
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/17/20 13:00 83-32-904/16/20 15:274751221
Acenaphthylene ND ug/kg 04/17/20 13:00 208-96-804/16/20 15:274751121
Aniline ND ug/kg 04/17/20 13:00 62-53-304/16/20 15:274751071
Anthracene ND ug/kg 04/17/20 13:00 120-12-704/16/20 15:274751231
Benzo(a)anthracene ND ug/kg 04/17/20 13:00 56-55-304/16/20 15:274751511
Benzo(a)pyrene ND ug/kg 04/17/20 13:00 50-32-804/16/20 15:274752061
Benzo(b)fluoranthene ND ug/kg 04/17/20 13:00 205-99-204/16/20 15:274751911
Benzo(g,h,i)perylene ND ug/kg 04/17/20 13:00 191-24-204/16/20 15:274751861
Benzo(k)fluoranthene ND ug/kg 04/17/20 13:00 207-08-904/16/20 15:274752001
Benzoic Acid ND ug/kg 04/17/20 13:00 65-85-004/16/20 15:2723805131
Benzyl alcohol ND ug/kg 04/17/20 13:00 100-51-604/16/20 15:279502521
4-Bromophenylphenyl ether ND ug/kg 04/17/20 13:00 101-55-304/16/20 15:274751251
Butylbenzylphthalate ND ug/kg 04/17/20 13:00 85-68-704/16/20 15:274751271
4-Chloro-3-methylphenol ND ug/kg 04/17/20 13:00 59-50-704/16/20 15:279502891
4-Chloroaniline ND ug/kg 04/17/20 13:00 106-47-804/16/20 15:279502911
bis(2-Chloroethoxy)methane ND ug/kg 04/17/20 13:00 111-91-104/16/20 15:274751271
bis(2-Chloroethyl) ether ND ug/kg 04/17/20 13:00 111-44-404/16/20 15:274751011
2-Chloronaphthalene ND ug/kg 04/17/20 13:00 91-58-704/16/20 15:274751061
2-Chlorophenol ND ug/kg 04/17/20 13:00 95-57-804/16/20 15:274751111
4-Chlorophenylphenyl ether ND ug/kg 04/17/20 13:00 7005-72-304/16/20 15:274751231
Chrysene ND ug/kg 04/17/20 13:00 218-01-904/16/20 15:274751381
Dibenz(a,h)anthracene ND ug/kg 04/17/20 13:00 53-70-304/16/20 15:274751901
Dibenzofuran ND ug/kg 04/17/20 13:00 132-64-904/16/20 15:274751191
1,2-Dichlorobenzene ND ug/kg 04/17/20 13:00 95-50-104/16/20 15:274751031
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:N WALL Lab ID:92473782004 Collected:04/14/20 09:50 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,3-Dichlorobenzene ND ug/kg 04/17/20 13:00 541-73-104/16/20 15:274751071
1,4-Dichlorobenzene ND ug/kg 04/17/20 13:00 106-46-704/16/20 15:274751051
3,3'-Dichlorobenzidine ND ug/kg 04/17/20 13:00 91-94-104/16/20 15:279503311
2,4-Dichlorophenol ND ug/kg 04/17/20 13:00 120-83-204/16/20 15:274751571
Diethylphthalate ND ug/kg 04/17/20 13:00 84-66-204/16/20 15:274751031
2,4-Dimethylphenol ND ug/kg 04/17/20 13:00 105-67-904/16/20 15:274751181
Dimethylphthalate ND ug/kg 04/17/20 13:00 131-11-304/16/20 15:274751071
Di-n-butylphthalate ND ug/kg 04/17/20 13:00 84-74-204/16/20 15:274751171
4,6-Dinitro-2-methylphenol ND ug/kg 04/17/20 13:00 534-52-104/16/20 15:279507661
2,4-Dinitrophenol ND ug/kg 04/17/20 13:00 51-28-504/16/20 15:27238015201
2,4-Dinitrotoluene ND ug/kg 04/17/20 13:00 121-14-204/16/20 15:274751261
2,6-Dinitrotoluene ND ug/kg 04/17/20 13:00 606-20-204/16/20 15:274751241
Di-n-octylphthalate ND ug/kg 04/17/20 13:00 117-84-004/16/20 15:274752711
bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/20 13:00 117-81-704/16/20 15:274751551
Fluoranthene ND ug/kg 04/17/20 13:00 206-44-004/16/20 15:274751441
Fluorene ND ug/kg 04/17/20 13:00 86-73-704/16/20 15:274751271
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 13:00 87-68-304/16/20 15:274751151
Hexachlorobenzene ND ug/kg 04/17/20 13:00 118-74-104/16/20 15:274751211
Hexachlorocyclopentadiene ND ug/kg 04/17/20 13:00 77-47-404/16/20 15:274751901
Hexachloroethane ND ug/kg 04/17/20 13:00 67-72-104/16/20 15:274751081
Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/20 13:00 193-39-504/16/20 15:274752171
Isophorone ND ug/kg 04/17/20 13:00 78-59-104/16/20 15:274751031
1-Methylnaphthalene ND ug/kg 04/17/20 13:00 90-12-004/16/20 15:274751271
2-Methylnaphthalene ND ug/kg 04/17/20 13:00 91-57-604/16/20 15:274751211
2-Methylphenol(o-Cresol)ND ug/kg 04/17/20 13:00 95-48-704/16/20 15:274751051
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/20 13:00 15831-10-404/16/20 15:274751191
Naphthalene ND ug/kg 04/17/20 13:00 91-20-304/16/20 15:274751141
2-Nitroaniline ND ug/kg 04/17/20 13:00 88-74-404/16/20 15:2723802391
3-Nitroaniline ND ug/kg 04/17/20 13:00 99-09-204/16/20 15:2723802521
4-Nitroaniline ND ug/kg 04/17/20 13:00 100-01-604/16/20 15:279502351
Nitrobenzene ND ug/kg 04/17/20 13:00 98-95-304/16/20 15:274751131
2-Nitrophenol ND ug/kg 04/17/20 13:00 88-75-504/16/20 15:274751471
4-Nitrophenol ND ug/kg 04/17/20 13:00 100-02-704/16/20 15:2723807571
N-Nitrosodimethylamine ND ug/kg 04/17/20 13:00 62-75-904/16/20 15:274751341
N-Nitroso-di-n-propylamine ND ug/kg 04/17/20 13:00 621-64-704/16/20 15:274751331
N-Nitrosodiphenylamine ND ug/kg 04/17/20 13:00 86-30-604/16/20 15:274751211
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/20 13:00 108-60-104/16/20 15:274751321
Pentachlorophenol ND ug/kg 04/17/20 13:00 87-86-504/16/20 15:279502171
Phenanthrene ND ug/kg 04/17/20 13:00 85-01-804/16/20 15:274751201
Phenol ND ug/kg 04/17/20 13:00 108-95-204/16/20 15:274751131
Pyrene ND ug/kg 04/17/20 13:00 129-00-004/16/20 15:274751311
Pyridine ND ug/kg 04/17/20 13:00 110-86-104/16/20 15:274751201
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 13:00 120-82-104/16/20 15:274751091
2,4,5-Trichlorophenol ND ug/kg 04/17/20 13:00 95-95-404/16/20 15:274751231
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:N WALL Lab ID:92473782004 Collected:04/14/20 09:50 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,6-Trichlorophenol ND ug/kg 04/17/20 13:00 88-06-204/16/20 15:274751191
Surrogates
Nitrobenzene-d5 (S)61 %04/17/20 13:00 4165-60-004/16/20 15:2723-110 1
2-Fluorobiphenyl (S)52 %04/17/20 13:00 321-60-804/16/20 15:2730-110 1
Terphenyl-d14 (S)67 %04/17/20 13:00 1718-51-004/16/20 15:2728-110 1
Phenol-d6 (S)61 %04/17/20 13:00 13127-88-304/16/20 15:2722-110 1
2-Fluorophenol (S)60 %04/17/20 13:00 367-12-404/16/20 15:2713-110 1
2,4,6-Tribromophenol (S)61 %04/17/20 13:00 118-79-604/16/20 15:2727-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone 63.4J ug/kg 04/17/20 13:19 67-64-104/17/20 10:1411110.5 1
Benzene ND ug/kg 04/17/20 13:19 71-43-204/17/20 10:145.6 1.0 1
Bromobenzene ND ug/kg 04/17/20 13:19 108-86-104/17/20 10:145.6 1.5 1
Bromochloromethane ND ug/kg 04/17/20 13:19 74-97-504/17/20 10:145.6 1.4 1
Bromodichloromethane ND ug/kg 04/17/20 13:19 75-27-404/17/20 10:145.6 1.1 1
Bromoform ND ug/kg 04/17/20 13:19 75-25-204/17/20 10:145.6 2.7 1
Bromomethane ND ug/kg 04/17/20 13:19 74-83-9 IH04/17/20 10:1411.1 2.6 1
2-Butanone (MEK)ND ug/kg 04/17/20 13:19 78-93-304/17/20 10:1411113.3 1
n-Butylbenzene ND ug/kg 04/17/20 13:19 104-51-804/17/20 10:145.6 3.1 1
sec-Butylbenzene ND ug/kg 04/17/20 13:19 135-98-804/17/20 10:145.6 2.4 1
tert-Butylbenzene ND ug/kg 04/17/20 13:19 98-06-604/17/20 10:145.6 1.9 1
Carbon tetrachloride ND ug/kg 04/17/20 13:19 56-23-504/17/20 10:145.6 1.1 1
Chlorobenzene ND ug/kg 04/17/20 13:19 108-90-704/17/20 10:145.6 1.1 1
Chloroethane ND ug/kg 04/17/20 13:19 75-00-304/17/20 10:1411.1 2.3 1
Chloroform ND ug/kg 04/17/20 13:19 67-66-304/17/20 10:145.6 1.2 1
Chloromethane ND ug/kg 04/17/20 13:19 74-87-304/17/20 10:1411.1 3.7 1
2-Chlorotoluene ND ug/kg 04/17/20 13:19 95-49-804/17/20 10:145.6 1.7 1
4-Chlorotoluene ND ug/kg 04/17/20 13:19 106-43-404/17/20 10:145.6 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/17/20 13:19 96-12-804/17/20 10:145.6 2.8 1
Dibromochloromethane ND ug/kg 04/17/20 13:19 124-48-104/17/20 10:145.6 2.8 1
1,2-Dibromoethane (EDB)ND ug/kg 04/17/20 13:19 106-93-404/17/20 10:145.6 1.2 1
Dibromomethane ND ug/kg 04/17/20 13:19 74-95-304/17/20 10:145.6 1.7 1
1,2-Dichlorobenzene ND ug/kg 04/17/20 13:19 95-50-104/17/20 10:145.6 2.0 1
1,3-Dichlorobenzene ND ug/kg 04/17/20 13:19 541-73-104/17/20 10:145.6 2.0 1
1,4-Dichlorobenzene ND ug/kg 04/17/20 13:19 106-46-704/17/20 10:145.6 1.9 1
Dichlorodifluoromethane ND ug/kg 04/17/20 13:19 75-71-804/17/20 10:1411.1 4.6 1
1,1-Dichloroethane ND ug/kg 04/17/20 13:19 75-34-304/17/20 10:145.6 0.82 1
1,2-Dichloroethane ND ug/kg 04/17/20 13:19 107-06-204/17/20 10:145.6 1.1 1
1,1-Dichloroethene ND ug/kg 04/17/20 13:19 75-35-404/17/20 10:145.6 1.3 1
cis-1,2-Dichloroethene ND ug/kg 04/17/20 13:19 156-59-204/17/20 10:145.6 0.97 1
trans-1,2-Dichloroethene ND ug/kg 04/17/20 13:19 156-60-504/17/20 10:145.6 1.1 1
1,2-Dichloropropane ND ug/kg 04/17/20 13:19 78-87-504/17/20 10:145.6 2.1 1
1,3-Dichloropropane ND ug/kg 04/17/20 13:19 142-28-904/17/20 10:145.6 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:N WALL Lab ID:92473782004 Collected:04/14/20 09:50 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
2,2-Dichloropropane ND ug/kg 04/17/20 13:19 594-20-704/17/20 10:145.6 0.55 1
1,1-Dichloropropene ND ug/kg 04/17/20 13:19 563-58-604/17/20 10:145.6 2.4 1
cis-1,3-Dichloropropene ND ug/kg 04/17/20 13:19 10061-01-504/17/20 10:145.6 2.5 1
trans-1,3-Dichloropropene ND ug/kg 04/17/20 13:19 10061-02-604/17/20 10:145.6 0.98 1
Diisopropyl ether ND ug/kg 04/17/20 13:19 108-20-304/17/20 10:145.6 3.2 1
Ethylbenzene ND ug/kg 04/17/20 13:19 100-41-404/17/20 10:145.6 1.2 1
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 13:19 87-68-304/17/20 10:145.6 2.8 1
2-Hexanone ND ug/kg 04/17/20 13:19 591-78-604/17/20 10:1455.7 5.8 1
Isopropylbenzene (Cumene)ND ug/kg 04/17/20 13:19 98-82-804/17/20 10:145.6 1.6 1
p-Isopropyltoluene ND ug/kg 04/17/20 13:19 99-87-604/17/20 10:145.6 2.7 1
Methylene Chloride ND ug/kg 04/17/20 13:19 75-09-204/17/20 10:1422.3 6.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/17/20 13:19 108-10-104/17/20 10:1455.7 4.2 1
Methyl-tert-butyl ether ND ug/kg 04/17/20 13:19 1634-04-404/17/20 10:145.6 3.2 1
Naphthalene ND ug/kg 04/17/20 13:19 91-20-304/17/20 10:145.6 4.7 1
n-Propylbenzene ND ug/kg 04/17/20 13:19 103-65-104/17/20 10:145.6 1.9 1
Styrene ND ug/kg 04/17/20 13:19 100-42-504/17/20 10:145.6 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/17/20 13:19 630-20-604/17/20 10:145.6 1.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/17/20 13:19 79-34-504/17/20 10:145.6 1.9 1
Tetrachloroethene ND ug/kg 04/17/20 13:19 127-18-404/17/20 10:145.6 1.8 1
Toluene ND ug/kg 04/17/20 13:19 108-88-304/17/20 10:145.6 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 04/17/20 13:19 87-61-604/17/20 10:145.6 4.0 1
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 13:19 120-82-104/17/20 10:145.6 3.0 1
1,1,1-Trichloroethane ND ug/kg 04/17/20 13:19 71-55-604/17/20 10:145.6 0.97 1
1,1,2-Trichloroethane ND ug/kg 04/17/20 13:19 79-00-504/17/20 10:145.6 1.3 1
Trichloroethene ND ug/kg 04/17/20 13:19 79-01-604/17/20 10:145.6 1.4 1
Trichlorofluoromethane ND ug/kg 04/17/20 13:19 75-69-404/17/20 10:145.6 1.3 1
1,2,3-Trichloropropane ND ug/kg 04/17/20 13:19 96-18-404/17/20 10:145.6 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 04/17/20 13:19 95-63-604/17/20 10:145.6 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 04/17/20 13:19 108-67-804/17/20 10:145.6 1.9 1
Vinyl acetate ND ug/kg 04/17/20 13:19 108-05-404/17/20 10:1455.7 18.2 1
Vinyl chloride ND ug/kg 04/17/20 13:19 75-01-404/17/20 10:1411.1 2.1 1
Xylene (Total)ND ug/kg 04/17/20 13:19 1330-20-704/17/20 10:1411.1 3.9 1
m&p-Xylene ND ug/kg 04/17/20 13:19 179601-23-104/17/20 10:1411.1 2.6 1
o-Xylene ND ug/kg 04/17/20 13:19 95-47-604/17/20 10:145.6 1.3 1
Surrogates
Toluene-d8 (S)103 %04/17/20 13:19 2037-26-504/17/20 10:1470-130 1
4-Bromofluorobenzene (S)94 %04/17/20 13:19 460-00-404/17/20 10:1470-130 1
1,2-Dichloroethane-d4 (S)100 %04/17/20 13:19 17060-07-004/17/20 10:1470-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 31.0 %04/16/20 14:410.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:N WALL Lab ID:92473782004 Collected:04/14/20 09:50 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 69.5 %04/20/20 07:5504/20/20 07:491
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1462690
MADEPV
MADEP VPH
MADEPV
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3519880-3
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
Aliphatic (C05-C08)mg/kg ND 5.00 04/18/20 12:291.67
Aliphatic (C09-C12)mg/kg ND 5.00 04/18/20 12:291.67
Aromatic (C09-C10),Unadjusted mg/kg ND 5.00 04/18/20 12:291.67
2,5-Dibromotoluene (FID)%93.4 70.0-130 04/18/20 12:29
2,5-Dibromotoluene (PID)%96.3 70.0-130 04/18/20 12:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3519880-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3519880-2
Aliphatic (C05-C08)mg/kg 63.960.0 107 70.0-13010563.3 0.943 25
Aliphatic (C09-C12)mg/kg 78.970.0 113 70.0-13011278.3 0.763 25
Aromatic (C09-C10),Unadjusted mg/kg 11.610.0 116 70.0-13011511.5 0.866 25
2,5-Dibromotoluene (FID)%102 70.0-130104
2,5-Dibromotoluene (PID)%106 70.0-130108
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3519880-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92473782001
R3519880-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aliphatic (C05-C08)mg/kg 51.9 85.7 70.0-130102 17.5 2551.9ND 44.5 53.0
Aliphatic (C09-C12)mg/kg 60.6 95.5 70.0-130112 15.3 2560.63.68 61.5 71.7
Aromatic (C09-
C10),Unadjusted mg/kg MH8.65 121 70.0-130136 11.6 258.65ND 10.5 11.8
2,5-Dibromotoluene (FID)%104 70.0-130101
2,5-Dibromotoluene (PID)%108 70.0-130104
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
536822
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2863265
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/17/20 10:301.2
1,1,1-Trichloroethane ug/kg ND 5.0 04/17/20 10:300.87
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/17/20 10:301.7
1,1,2-Trichloroethane ug/kg ND 5.0 04/17/20 10:301.1
1,1-Dichloroethane ug/kg ND 5.0 04/17/20 10:300.74
1,1-Dichloroethene ug/kg ND 5.0 04/17/20 10:301.2
1,1-Dichloropropene ug/kg ND 5.0 04/17/20 10:302.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 04/17/20 10:303.6
1,2,3-Trichloropropane ug/kg ND 5.0 04/17/20 10:301.7
1,2,4-Trichlorobenzene ug/kg ND 5.0 04/17/20 10:302.6
1,2,4-Trimethylbenzene ug/kg ND 5.0 04/17/20 10:302.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/17/20 10:302.5
1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/17/20 10:301.1
1,2-Dichlorobenzene ug/kg ND 5.0 04/17/20 10:301.8
1,2-Dichloroethane ug/kg ND 5.0 04/17/20 10:301.0
1,2-Dichloropropane ug/kg ND 5.0 04/17/20 10:301.9
1,3,5-Trimethylbenzene ug/kg ND 5.0 04/17/20 10:301.7
1,3-Dichlorobenzene ug/kg ND 5.0 04/17/20 10:301.8
1,3-Dichloropropane ug/kg ND 5.0 04/17/20 10:301.9
1,4-Dichlorobenzene ug/kg ND 5.0 04/17/20 10:301.7
2,2-Dichloropropane ug/kg ND 5.0 04/17/20 10:300.49
2-Butanone (MEK)ug/kg ND 100 04/17/20 10:3011.9
2-Chlorotoluene ug/kg ND 5.0 04/17/20 10:301.5
2-Hexanone ug/kg ND 50.0 04/17/20 10:305.2
4-Chlorotoluene ug/kg ND 5.0 04/17/20 10:301.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/17/20 10:303.7
Acetone ug/kg ND 100 04/17/20 10:309.4
Benzene ug/kg ND 5.0 04/17/20 10:300.90
Bromobenzene ug/kg ND 5.0 04/17/20 10:301.4
Bromochloromethane ug/kg ND 5.0 04/17/20 10:301.2
Bromodichloromethane ug/kg ND 5.0 04/17/20 10:300.98
Bromoform ug/kg ND 5.0 04/17/20 10:302.4
Bromomethane ug/kg ND 10.0 IH04/17/20 10:302.4
Carbon tetrachloride ug/kg ND 5.0 04/17/20 10:300.96
Chlorobenzene ug/kg ND 5.0 04/17/20 10:300.97
Chloroethane ug/kg ND 10.0 04/17/20 10:302.1
Chloroform ug/kg ND 5.0 04/17/20 10:301.1
Chloromethane ug/kg ND 10.0 04/17/20 10:303.3
cis-1,2-Dichloroethene ug/kg ND 5.0 04/17/20 10:300.87
cis-1,3-Dichloropropene ug/kg ND 5.0 04/17/20 10:302.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2863265
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 04/17/20 10:302.5
Dibromomethane ug/kg ND 5.0 04/17/20 10:301.5
Dichlorodifluoromethane ug/kg ND 10.0 04/17/20 10:304.1
Diisopropyl ether ug/kg ND 5.0 04/17/20 10:302.9
Ethylbenzene ug/kg ND 5.0 04/17/20 10:301.1
Hexachloro-1,3-butadiene ug/kg ND 5.0 04/17/20 10:302.5
Isopropylbenzene (Cumene)ug/kg ND 5.0 04/17/20 10:301.4
m&p-Xylene ug/kg ND 10.0 04/17/20 10:302.4
Methyl-tert-butyl ether ug/kg ND 5.0 04/17/20 10:302.9
Methylene Chloride ug/kg ND 20.0 04/17/20 10:305.9
n-Butylbenzene ug/kg ND 5.0 04/17/20 10:302.8
n-Propylbenzene ug/kg ND 5.0 04/17/20 10:301.7
Naphthalene ug/kg ND 5.0 04/17/20 10:304.2
o-Xylene ug/kg ND 5.0 04/17/20 10:301.2
p-Isopropyltoluene ug/kg ND 5.0 04/17/20 10:302.4
sec-Butylbenzene ug/kg ND 5.0 04/17/20 10:302.1
Styrene ug/kg ND 5.0 04/17/20 10:301.5
tert-Butylbenzene ug/kg ND 5.0 04/17/20 10:301.7
Tetrachloroethene ug/kg ND 5.0 04/17/20 10:301.6
Toluene ug/kg ND 5.0 04/17/20 10:301.6
trans-1,2-Dichloroethene ug/kg ND 5.0 04/17/20 10:300.98
trans-1,3-Dichloropropene ug/kg ND 5.0 04/17/20 10:300.88
Trichloroethene ug/kg ND 5.0 04/17/20 10:301.3
Trichlorofluoromethane ug/kg ND 5.0 04/17/20 10:301.2
Vinyl acetate ug/kg ND 50.0 04/17/20 10:3016.3
Vinyl chloride ug/kg ND 10.0 04/17/20 10:301.9
Xylene (Total)ug/kg ND 10.0 04/17/20 10:303.5
1,2-Dichloroethane-d4 (S)%96 70-132 04/17/20 10:30
4-Bromofluorobenzene (S)%93 70-130 04/17/20 10:30
Toluene-d8 (S)%101 70-130 04/17/20 10:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2863266LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 51.050 102 70-130
1,1,1-Trichloroethane ug/kg 46.450 93 70-130
1,1,2,2-Tetrachloroethane ug/kg 47.550 95 55-130
1,1,2-Trichloroethane ug/kg 51.550 103 70-130
1,1-Dichloroethane ug/kg 47.350 95 68-130
1,1-Dichloroethene ug/kg 49.850 100 70-130
1,1-Dichloropropene ug/kg 47.450 95 70-130
1,2,3-Trichlorobenzene ug/kg 56.950 114 70-130
1,2,3-Trichloropropane ug/kg 49.550 99 70-130
1,2,4-Trichlorobenzene ug/kg 55.750 111 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2863266LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 49.150 98 69-130
1,2-Dibromo-3-chloropropane ug/kg 66.350 133 57-141
1,2-Dibromoethane (EDB)ug/kg 50.550 101 70-130
1,2-Dichlorobenzene ug/kg 51.450 103 70-130
1,2-Dichloroethane ug/kg 48.350 97 70-130
1,2-Dichloropropane ug/kg 52.550 105 70-130
1,3,5-Trimethylbenzene ug/kg 48.750 97 70-130
1,3-Dichlorobenzene ug/kg 50.250 100 70-130
1,3-Dichloropropane ug/kg 47.150 94 70-130
1,4-Dichlorobenzene ug/kg 50.150 100 70-130
2,2-Dichloropropane ug/kg 45.550 91 70-130
2-Butanone (MEK)ug/kg 126100 126 60-130
2-Chlorotoluene ug/kg 49.550 99 70-130
2-Hexanone ug/kg 118100 118 70-132
4-Chlorotoluene ug/kg 48.550 97 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 116100 116 69-130
Acetone ug/kg 129100 129 49-148
Benzene ug/kg 49.250 98 70-130
Bromobenzene ug/kg 55.350 111 70-130
Bromochloromethane ug/kg 51.550 103 70-130
Bromodichloromethane ug/kg 50.650 101 70-130
Bromoform ug/kg 52.350 105 68-136
Bromomethane ug/kg 69.4 IH5013960-140
Carbon tetrachloride ug/kg 54.550 109 70-130
Chlorobenzene ug/kg 47.650 95 70-130
Chloroethane ug/kg 54.450 109 51-147
Chloroform ug/kg 46.750 93 70-130
Chloromethane ug/kg 44.150 88 48-130
cis-1,2-Dichloroethene ug/kg 48.350 97 70-130
cis-1,3-Dichloropropene ug/kg 48.950 98 70-130
Dibromochloromethane ug/kg 52.450 105 70-130
Dibromomethane ug/kg 51.650 103 70-130
Dichlorodifluoromethane ug/kg 44.850 90 49-130
Diisopropyl ether ug/kg 48.250 96 66-130
Ethylbenzene ug/kg 45.050 90 70-130
Hexachloro-1,3-butadiene ug/kg 53.850 108 70-130
Isopropylbenzene (Cumene)ug/kg 46.250 92 70-130
m&p-Xylene ug/kg 91.1100 91 70-130
Methyl-tert-butyl ether ug/kg 46.950 94 70-130
Methylene Chloride ug/kg 50.450 101 50-137
n-Butylbenzene ug/kg 48.750 97 70-130
n-Propylbenzene ug/kg 47.250 94 70-130
Naphthalene ug/kg 58.650 117 70-131
o-Xylene ug/kg 45.750 91 70-130
p-Isopropyltoluene ug/kg 51.050 102 70-130
sec-Butylbenzene ug/kg 48.150 96 70-130
Styrene ug/kg 47.550 95 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2863266LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 44.450 89 69-130
Tetrachloroethene ug/kg 44.750 89 56-130
Toluene ug/kg 47.050 94 70-130
trans-1,2-Dichloroethene ug/kg 49.550 99 70-130
trans-1,3-Dichloropropene ug/kg 49.650 99 70-130
Trichloroethene ug/kg 54.550 109 70-141
Trichlorofluoromethane ug/kg 48.250 96 67-130
Vinyl acetate ug/kg 108100 108 10-136
Vinyl chloride ug/kg 51.950 104 67-130
Xylene (Total)ug/kg 137150 91 70-130
1,2-Dichloroethane-d4 (S)%99 70-132
4-Bromofluorobenzene (S)%91 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2863268MATRIX SPIKE SAMPLE:
MSSpike
Result
92473782002
1,1,1,2-Tetrachloroethane ug/kg 18.622 85 52-133ND
1,1,1-Trichloroethane ug/kg 20.222 92 49-137ND
1,1,2,2-Tetrachloroethane ug/kg 16.622 76 39-150ND
1,1,2-Trichloroethane ug/kg 18.022 82 48-140ND
1,1-Dichloroethane ug/kg 19.622 89 46-135ND
1,1-Dichloroethene ug/kg 22.222 102 38-149ND
1,1-Dichloropropene ug/kg 19.822 90 41-140ND
1,2,3-Trichlorobenzene ug/kg 17.622 80 10-158ND
1,2,3-Trichloropropane ug/kg 15.722 72 33-157ND
1,2,4-Trichlorobenzene ug/kg 17.322 79 10-155ND
1,2,4-Trimethylbenzene ug/kg 20.522 93 24-154ND
1,2-Dibromo-3-chloropropane ug/kg 19.5 v1228933-158ND
1,2-Dibromoethane (EDB)ug/kg 17.222 78 40-136ND
1,2-Dichlorobenzene ug/kg 19.022 87 27-146ND
1,2-Dichloroethane ug/kg 17.222 78 49-140ND
1,2-Dichloropropane ug/kg 20.022 92 44-143ND
1,3,5-Trimethylbenzene ug/kg 20.722 95 40-144ND
1,3-Dichlorobenzene ug/kg 19.222 88 33-140ND
1,3-Dichloropropane ug/kg 16.822 77 47-147ND
1,4-Dichlorobenzene ug/kg 18.722 85 35-139ND
2,2-Dichloropropane ug/kg 18.722 85 41-140ND
2-Butanone (MEK)ug/kg 35.3J43.8 71 10-181ND
2-Chlorotoluene ug/kg 19.122 87 38-147ND
2-Hexanone ug/kg 31.2J43.8 71 18-169ND
4-Chlorotoluene ug/kg 19.222 87 36-145ND
4-Methyl-2-pentanone (MIBK)ug/kg 35.2J43.8 80 16-175ND
Acetone ug/kg 96.4J43.8 76 10-20063.0J
Benzene ug/kg 19.922 91 46-136ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
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Page 29 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2863268MATRIX SPIKE SAMPLE:
MSSpike
Result
92473782002
Bromobenzene ug/kg 20.822 95 38-149ND
Bromochloromethane ug/kg 18.922 86 44-142ND
Bromodichloromethane ug/kg 18.922 87 41-140ND
Bromoform ug/kg 16.922 77 34-145ND
Bromomethane ug/kg 28.4 IH2212914-162ND
Carbon tetrachloride ug/kg 23.622 108 44-141ND
Chlorobenzene ug/kg 19.422 88 39-141ND
Chloroethane ug/kg 26.622 121 10-182ND
Chloroform ug/kg 18.522 84 45-140ND
Chloromethane ug/kg 18.822 86 19-149ND
cis-1,2-Dichloroethene ug/kg 19.122 87 38-150ND
cis-1,3-Dichloropropene ug/kg 17.422 79 30-144ND
Dibromochloromethane ug/kg 17.722 81 36-145ND
Dibromomethane ug/kg 18.222 83 41-145ND
Dichlorodifluoromethane ug/kg 20.6 v3229416-146ND
Diisopropyl ether ug/kg 18.022 82 41-143ND
Ethylbenzene ug/kg 19.322 88 35-144ND
Hexachloro-1,3-butadiene ug/kg 22.022 100 10-160ND
Isopropylbenzene (Cumene)ug/kg 20.022 91 30-152ND
m&p-Xylene ug/kg 38.743.8 88 33-145ND
Methyl-tert-butyl ether ug/kg 15.022 68 49-140ND
Methylene Chloride ug/kg 23.6 v12210810-174ND
n-Butylbenzene ug/kg 19.622 89 10-160ND
n-Propylbenzene ug/kg 20.522 93 24-159ND
Naphthalene ug/kg 17.722 81 10-171ND
o-Xylene ug/kg 18.622 85 31-150ND
p-Isopropyltoluene ug/kg 21.522 98 21-154ND
sec-Butylbenzene ug/kg 20.722 94 19-159ND
Styrene ug/kg 18.022 82 15-152ND
tert-Butylbenzene ug/kg 19.322 88 31-141ND
Tetrachloroethene ug/kg 18.822 86 19-141ND
Toluene ug/kg 20.022 91 31-146ND
trans-1,2-Dichloroethene ug/kg 20.222 92 28-157ND
trans-1,3-Dichloropropene ug/kg 16.422 75 25-146ND
Trichloroethene ug/kg 22.122 101 34-149ND
Trichlorofluoromethane ug/kg 23.322 106 10-167ND
Vinyl acetate ug/kg ND43.8 35 10-200ND
Vinyl chloride ug/kg 22.7 v32210436-155ND
Xylene (Total)ug/kg 57.365.8 87 29-148ND
1,2-Dichloroethane-d4 (S)%93 70-132
4-Bromofluorobenzene (S)%92 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 30 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473782001
2863267SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND v130ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg 13.6J 30ND
Acetone ug/kg 15.9J 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IH30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND v230ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473782001
2863267SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND v130ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND v230ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9598
4-Bromofluorobenzene (S)%110106
Toluene-d8 (S)%105101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
536636
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2862449
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 328 04/17/20 08:2275.1
1,2-Dichlorobenzene ug/kg ND 328 04/17/20 08:2270.9
1,3-Dichlorobenzene ug/kg ND 328 04/17/20 08:2273.8
1,4-Dichlorobenzene ug/kg ND 328 04/17/20 08:2272.1
1-Methylnaphthalene ug/kg ND 328 04/17/20 08:2287.3
2,2'-Oxybis(1-chloropropane)ug/kg ND 328 04/17/20 08:2291.1
2,4,5-Trichlorophenol ug/kg ND 328 04/17/20 08:2285.1
2,4,6-Trichlorophenol ug/kg ND 328 04/17/20 08:2282.4
2,4-Dichlorophenol ug/kg ND 328 04/17/20 08:22108
2,4-Dimethylphenol ug/kg ND 328 04/17/20 08:2281.7
2,4-Dinitrophenol ug/kg ND 1640 04/17/20 08:221050
2,4-Dinitrotoluene ug/kg ND 328 04/17/20 08:2286.8
2,6-Dinitrotoluene ug/kg ND 328 04/17/20 08:2285.7
2-Chloronaphthalene ug/kg ND 328 04/17/20 08:2273.0
2-Chlorophenol ug/kg ND 328 04/17/20 08:2276.3
2-Methylnaphthalene ug/kg ND 328 04/17/20 08:2283.4
2-Methylphenol(o-Cresol)ug/kg ND 328 04/17/20 08:2272.6
2-Nitroaniline ug/kg ND 1640 04/17/20 08:22165
2-Nitrophenol ug/kg ND 328 04/17/20 08:22101
3&4-Methylphenol(m&p Cresol)ug/kg ND 328 04/17/20 08:2282.5
3,3'-Dichlorobenzidine ug/kg ND 656 04/17/20 08:22228
3-Nitroaniline ug/kg ND 1640 04/17/20 08:22174
4,6-Dinitro-2-methylphenol ug/kg ND 656 04/17/20 08:22528
4-Bromophenylphenyl ether ug/kg ND 328 04/17/20 08:2286.0
4-Chloro-3-methylphenol ug/kg ND 656 04/17/20 08:22200
4-Chloroaniline ug/kg ND 656 04/17/20 08:22201
4-Chlorophenylphenyl ether ug/kg ND 328 04/17/20 08:2285.1
4-Nitroaniline ug/kg ND 656 04/17/20 08:22162
4-Nitrophenol ug/kg ND 1640 04/17/20 08:22523
Acenaphthene ug/kg ND 328 04/17/20 08:2284.3
Acenaphthylene ug/kg ND 328 04/17/20 08:2277.6
Aniline ug/kg ND 328 04/17/20 08:2273.6
Anthracene ug/kg ND 328 04/17/20 08:2285.0
Benzo(a)anthracene ug/kg ND 328 04/17/20 08:22104
Benzo(a)pyrene ug/kg ND 328 04/17/20 08:22142
Benzo(b)fluoranthene ug/kg ND 328 04/17/20 08:22132
Benzo(g,h,i)perylene ug/kg ND 328 04/17/20 08:22128
Benzo(k)fluoranthene ug/kg ND 328 04/17/20 08:22138
Benzoic Acid ug/kg ND 1640 04/17/20 08:22354
Benzyl alcohol ug/kg ND 656 04/17/20 08:22174
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2862449
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 328 04/17/20 08:2287.5
bis(2-Chloroethyl) ether ug/kg ND 328 04/17/20 08:2269.6
bis(2-Ethylhexyl)phthalate ug/kg ND 328 04/17/20 08:22107
Butylbenzylphthalate ug/kg ND 328 04/17/20 08:2287.3
Chrysene ug/kg ND 328 04/17/20 08:2295.2
Di-n-butylphthalate ug/kg ND 328 04/17/20 08:2280.9
Di-n-octylphthalate ug/kg ND 328 04/17/20 08:22187
Dibenz(a,h)anthracene ug/kg ND 328 04/17/20 08:22131
Dibenzofuran ug/kg ND 328 04/17/20 08:2282.0
Diethylphthalate ug/kg ND 328 04/17/20 08:2271.1
Dimethylphthalate ug/kg ND 328 04/17/20 08:2274.1
Fluoranthene ug/kg ND 328 04/17/20 08:2299.0
Fluorene ug/kg ND 328 04/17/20 08:2287.7
Hexachloro-1,3-butadiene ug/kg ND 328 04/17/20 08:2279.7
Hexachlorobenzene ug/kg ND 328 04/17/20 08:2283.2
Hexachlorocyclopentadiene ug/kg ND 328 04/17/20 08:22131
Hexachloroethane ug/kg ND 328 04/17/20 08:2274.7
Indeno(1,2,3-cd)pyrene ug/kg ND 328 04/17/20 08:22150
Isophorone ug/kg ND 328 04/17/20 08:2271.2
N-Nitroso-di-n-propylamine ug/kg ND 328 04/17/20 08:2291.8
N-Nitrosodimethylamine ug/kg ND 328 04/17/20 08:2292.2
N-Nitrosodiphenylamine ug/kg ND 328 04/17/20 08:2283.6
Naphthalene ug/kg ND 328 04/17/20 08:2278.5
Nitrobenzene ug/kg ND 328 04/17/20 08:2278.3
Pentachlorophenol ug/kg ND 656 04/17/20 08:22150
Phenanthrene ug/kg ND 328 04/17/20 08:2282.5
Phenol ug/kg ND 328 04/17/20 08:2278.3
Pyrene ug/kg ND 328 04/17/20 08:2290.2
Pyridine ug/kg ND 328 04/17/20 08:2282.9
2,4,6-Tribromophenol (S)%69 27-110 04/17/20 08:22
2-Fluorobiphenyl (S)%70 30-110 04/17/20 08:22
2-Fluorophenol (S)%67 13-110 04/17/20 08:22
Nitrobenzene-d5 (S)%69 23-110 04/17/20 08:22
Phenol-d6 (S)%67 22-110 04/17/20 08:22
Terphenyl-d14 (S)%87 28-110 04/17/20 08:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2862450LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 14701690 87 52-130
1,2-Dichlorobenzene ug/kg 14301690 84 51-130
1,3-Dichlorobenzene ug/kg 14401690 85 50-130
1,4-Dichlorobenzene ug/kg 15201690 89 49-130
1-Methylnaphthalene ug/kg 14001690 83 55-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2862450LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 13801690 81 30-130
2,4,5-Trichlorophenol ug/kg 16101690 95 55-130
2,4,6-Trichlorophenol ug/kg 15601690 92 57-130
2,4-Dichlorophenol ug/kg 15101690 89 56-130
2,4-Dimethylphenol ug/kg 14801690 87 51-130
2,4-Dinitrophenol ug/kg 74508470 88 27-133
2,4-Dinitrotoluene ug/kg 15701690 92 61-130
2,6-Dinitrotoluene ug/kg 16301690 96 60-130
2-Chloronaphthalene ug/kg 15901690 94 52-130
2-Chlorophenol ug/kg 14701690 87 54-130
2-Methylnaphthalene ug/kg 14601690 86 54-130
2-Methylphenol(o-Cresol)ug/kg 14501690 86 51-130
2-Nitroaniline ug/kg 30103390 89 51-130
2-Nitrophenol ug/kg 14501690 85 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 14601690 86 11-163
3,3'-Dichlorobenzidine ug/kg 27903390 82 10-132
3-Nitroaniline ug/kg 27303390 81 55-130
4,6-Dinitro-2-methylphenol ug/kg 32103390 95 47-142
4-Bromophenylphenyl ether ug/kg 16201690 95 59-130
4-Chloro-3-methylphenol ug/kg 29303390 87 55-130
4-Chloroaniline ug/kg 29003390 85 54-130
4-Chlorophenylphenyl ether ug/kg 15201690 89 58-130
4-Nitroaniline ug/kg 28403390 84 54-130
4-Nitrophenol ug/kg 75508470 89 48-130
Acenaphthene ug/kg 15701690 92 60-130
Acenaphthylene ug/kg 16101690 95 60-130
Aniline ug/kg 13801690 81 43-130
Anthracene ug/kg 16101690 95 63-130
Benzo(a)anthracene ug/kg 16301690 96 59-130
Benzo(a)pyrene ug/kg 16401690 97 57-130
Benzo(b)fluoranthene ug/kg 16001690 94 54-130
Benzo(g,h,i)perylene ug/kg 18701690 111 59-130
Benzo(k)fluoranthene ug/kg 16701690 98 54-130
Benzoic Acid ug/kg 64608470 76 19-130
Benzyl alcohol ug/kg 28703390 85 50-130
bis(2-Chloroethoxy)methane ug/kg 14001690 83 54-130
bis(2-Chloroethyl) ether ug/kg 13901690 82 48-130
bis(2-Ethylhexyl)phthalate ug/kg 18501690 109 45-134
Butylbenzylphthalate ug/kg 18501690 109 46-138
Chrysene ug/kg 16301690 96 58-130
Di-n-butylphthalate ug/kg 16201690 96 60-130
Di-n-octylphthalate ug/kg 17301690 102 53-130
Dibenz(a,h)anthracene ug/kg 18501690 109 59-130
Dibenzofuran ug/kg 15501690 91 60-130
Diethylphthalate ug/kg 16201690 95 60-130
Dimethylphthalate ug/kg 16001690 95 60-130
Fluoranthene ug/kg 14901690 88 65-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2862450LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 15401690 91 63-130
Hexachloro-1,3-butadiene ug/kg 14501690 86 46-130
Hexachlorobenzene ug/kg 16501690 97 58-130
Hexachlorocyclopentadiene ug/kg 14101690 83 23-130
Hexachloroethane ug/kg 14101690 83 47-130
Indeno(1,2,3-cd)pyrene ug/kg 17901690 105 60-130
Isophorone ug/kg 14501690 85 49-130
N-Nitroso-di-n-propylamine ug/kg 14401690 85 47-130
N-Nitrosodimethylamine ug/kg 14601690 86 45-130
N-Nitrosodiphenylamine ug/kg 17001690 100 59-130
Naphthalene ug/kg 14601690 86 55-130
Nitrobenzene ug/kg 14801690 87 49-130
Pentachlorophenol ug/kg 32203390 95 10-132
Phenanthrene ug/kg 16401690 97 62-130
Phenol ug/kg 14801690 87 46-130
Pyrene ug/kg 19401690 114 53-130
Pyridine ug/kg 12301690 73 37-130
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%82 30-110
2-Fluorophenol (S)%80 13-110
Nitrobenzene-d5 (S)%76 23-110
Phenol-d6 (S)%80 22-110
Terphenyl-d14 (S)%99 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2862451MATRIX SPIKE SAMPLE:
MSSpike
Result
92473346014
1,2,4-Trichlorobenzene ug/kg 14901930 77 18-130ND
1,2-Dichlorobenzene ug/kg 15101930 78 14-130ND
1,3-Dichlorobenzene ug/kg 15101930 78 12-130ND
1,4-Dichlorobenzene ug/kg 15801930 82 10-130ND
1-Methylnaphthalene ug/kg 14401930 74 12-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 14801930 77 10-130ND
2,4,5-Trichlorophenol ug/kg 17601930 91 13-130ND
2,4,6-Trichlorophenol ug/kg 16901930 88 17-130ND
2,4-Dichlorophenol ug/kg 16701930 86 10-130ND
2,4-Dimethylphenol ug/kg 15501930 80 10-130ND
2,4-Dinitrophenol ug/kg 86609670 90 10-130ND
2,4-Dinitrotoluene ug/kg 17101930 89 24-130ND
2,6-Dinitrotoluene ug/kg 17401930 90 23-130ND
2-Chloronaphthalene ug/kg 15601930 81 19-130ND
2-Chlorophenol ug/kg 15901930 82 10-130ND
2-Methylnaphthalene ug/kg 15001930 77 18-130ND
2-Methylphenol(o-Cresol)ug/kg 16001930 83 10-130ND
2-Nitroaniline ug/kg 32703860 84 17-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2862451MATRIX SPIKE SAMPLE:
MSSpike
Result
92473346014
2-Nitrophenol ug/kg 15701930 81 10-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 16301930 84 10-130ND
3,3'-Dichlorobenzidine ug/kg 2710 IS38607010-130ND
3-Nitroaniline ug/kg 30203860 78 24-130ND
4,6-Dinitro-2-methylphenol ug/kg 36503860 94 10-152ND
4-Bromophenylphenyl ether ug/kg 15701930 81 29-130ND
4-Chloro-3-methylphenol ug/kg 33703860 87 17-130ND
4-Chloroaniline ug/kg 31003860 80 14-130ND
4-Chlorophenylphenyl ether ug/kg 15001930 78 25-130ND
4-Nitroaniline ug/kg 31003860 80 22-130ND
4-Nitrophenol ug/kg 82209670 85 10-130ND
Acenaphthene ug/kg 15401930 80 20-130ND
Acenaphthylene ug/kg 15701930 81 25-130ND
Aniline ug/kg 13001930 67 10-130ND
Anthracene ug/kg 15701930 81 29-130ND
Benzo(a)anthracene ug/kg 1530 IS19307919-130ND
Benzo(a)pyrene ug/kg 14701930 76 12-130ND
Benzo(b)fluoranthene ug/kg 14201930 73 14-130ND
Benzo(g,h,i)perylene ug/kg 15401930 79 10-130ND
Benzo(k)fluoranthene ug/kg 15301930 79 14-130ND
Benzoic Acid ug/kg 79909670 83 10-130ND
Benzyl alcohol ug/kg 32003860 83 13-130ND
bis(2-Chloroethoxy)methane ug/kg 15201930 78 16-130ND
bis(2-Chloroethyl) ether ug/kg 15201930 78 11-130ND
bis(2-Ethylhexyl)phthalate ug/kg 1870 IS19309721-130ND
Butylbenzylphthalate ug/kg 1920 IS19309923-130ND
Chrysene ug/kg 1580 IS19308222-130ND
Di-n-butylphthalate ug/kg 15301930 79 30-130ND
Di-n-octylphthalate ug/kg 1570 IS19308123-142ND
Dibenz(a,h)anthracene ug/kg 16001930 83 10-130ND
Dibenzofuran ug/kg 15401930 80 24-130ND
Diethylphthalate ug/kg 16801930 87 26-130ND
Dimethylphthalate ug/kg 17201930 89 22-130ND
Fluoranthene ug/kg 13301930 69 33-130ND
Fluorene ug/kg 15501930 80 22-130ND
Hexachloro-1,3-butadiene ug/kg 13601930 70 13-130ND
Hexachlorobenzene ug/kg 15501930 80 29-130ND
Hexachlorocyclopentadiene ug/kg 12601930 65 10-130ND
Hexachloroethane ug/kg 14501930 75 10-130ND
Indeno(1,2,3-cd)pyrene ug/kg 15201930 79 10-130ND
Isophorone ug/kg 15901930 82 13-130ND
N-Nitroso-di-n-propylamine ug/kg 15801930 82 12-130ND
N-Nitrosodimethylamine ug/kg 13401930 69 11-130ND
N-Nitrosodiphenylamine ug/kg 17401930 90 15-130ND
Naphthalene ug/kg 15301930 79 15-130ND
Nitrobenzene ug/kg 15801930 82 12-130ND
Pentachlorophenol ug/kg 34003860 88 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2862451MATRIX SPIKE SAMPLE:
MSSpike
Result
92473346014
Phenanthrene ug/kg 15801930 82 27-130ND
Phenol ug/kg 15801930 82 10-130ND
Pyrene ug/kg 2010 IS193010419-130ND
Pyridine ug/kg 11101930 57 10-130ND
2,4,6-Tribromophenol (S)%82 27-110
2-Fluorobiphenyl (S)%66 30-110
2-Fluorophenol (S)%72 13-110
Nitrobenzene-d5 (S)%73 23-110
Phenol-d6 (S)%75 22-110
Terphenyl-d14 (S)%89 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473782001
2862452SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473782001
2862452SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6662
2-Fluorobiphenyl (S)%26 S028
2-Fluorophenol (S)%6462
Nitrobenzene-d5 (S)%6156
Phenol-d6 (S)%6765
Terphenyl-d14 (S)%7468
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
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Page 39 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
536540
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2861946
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
Aliphatic (C09-C18)mg/kg ND 10.0 N204/17/20 08:1510.0
Aliphatic (C19-C36)mg/kg ND 10.0 N204/17/20 08:1510.0
Aromatic (C11-C22)mg/kg ND 10.0 N204/17/20 08:1510.0
2-Bromonaphthalene (S)%101 40-140 04/17/20 08:15
2-Fluorobiphenyl (S)%99 40-140 04/17/20 08:15
Nonatriacontane (S)%66 40-140 04/17/20 08:15
o-Terphenyl (S)%67 40-140 04/17/20 08:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2861947LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2861948
Aliphatic (C09-C18)mg/kg ND N2104440-14055ND 50
Aliphatic (C19-C36)mg/kg ND N213.4 72 40-1408110.9 50
Aromatic (C11-C22)mg/kg 18.6 N228.4 65 40-1407922.8 20 50
2-Bromonaphthalene (S)%83 40-14094
2-Fluorobiphenyl (S)%82 40-14088
Nonatriacontane (S)%58 40-14063
o-Terphenyl (S)%69 40-14083
REPORT OF LABORATORY ANALYSIS
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Page 40 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
536626
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92473782001, 92473782002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473797001
2862390SAMPLE DUPLICATE:
Percent Moisture %24.5 6 2526.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
2630973009
2862391SAMPLE DUPLICATE:
Percent Moisture %43.6 2 2544.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
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Page 41 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
536632
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92473782003, 92473782004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473782003
2862428SAMPLE DUPLICATE:
Percent Moisture %30.8 0 2531.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473841002
2862429SAMPLE DUPLICATE:
Percent Moisture %95.4 0 2595.4
REPORT OF LABORATORY ANALYSIS
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Page 42 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1463205
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3520146-1
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
Total Solids %ND 04/20/20 07:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3520146-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1210056-01
R3520146-3SAMPLE DUPLICATE:
Total Solids %83.9 0.544 1084.3
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 43 of 48
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The internal standard response is below criteria. Results may be biased high.IS
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92473782001 536540 536774W WALL MADEP EPH MADEP EPH
92473782002 536540 536774E WALL MADEP EPH MADEP EPH
92473782003 536540 536774S WALL MADEP EPH MADEP EPH
92473782004 536540 536774N WALL MADEP EPH MADEP EPH
92473782001 1462690 1462690W WALL MADEPV MADEP VPH
92473782002 1462690 1462690E WALL MADEPV MADEP VPH
92473782003 1462690 1462690S WALL MADEPV MADEP VPH
92473782004 1462690 1462690N WALL MADEPV MADEP VPH
92473782001 536636 536777W WALL EPA 3546 EPA 8270E
92473782002 536636 536777E WALL EPA 3546 EPA 8270E
92473782003 536636 536777S WALL EPA 3546 EPA 8270E
92473782004 536636 536777N WALL EPA 3546 EPA 8270E
92473782001 536822 536866W WALL EPA 5035A EPA 8260D
92473782002 536822 536866E WALL EPA 5035A EPA 8260D
92473782003 536822 536866S WALL EPA 5035A EPA 8260D
92473782004 536822 536866N WALL EPA 5035A EPA 8260D
92473782001 536626W WALL ASTM D2974-87
92473782002 536626E WALL ASTM D2974-87
92473782003 536632S WALL ASTM D2974-87
92473782004 536632N WALL ASTM D2974-87
92473782001 1463205 1463205W WALL SM 2540 G SM 2540G
92473782002 1463205 1463205E WALL SM 2540 G SM 2540G
92473782003 1463205 1463205S WALL SM 2540 G SM 2540G
92473782004 1463205 1463205N WALL SM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2020 04:40 PM
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Page 45 of 48
Page 46 of 48
Page 47 of 48
Page 48 of 48
#=CL#
April 29, 2020
LIMS USE: FR - BRITNEY BARNES
LIMS OBJECT ID: 92473782
92473782
Project:
Pace Project No.:
RE:
Britney Barnes
Civil & Environmental Consultants
530 Howell Rd
Suite 203
Greenville, SC
GREENSBORO NC LC 0134 UST CLOS
Dear Britney Barnes:
Enclosed are the analytical results for sample(s) received by the laboratory on April 15, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Sarah Galloway, Ryder Systems, Inc
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 50
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Page 2 of 50
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Lab ID Sample ID Matrix Date Collected Date Received
92473782001 W WALL Solid 04/14/20 09:30 04/15/20 10:10
92473782002 E WALL Solid 04/14/20 10:00 04/15/20 10:10
92473782003 S WALL Solid 04/14/20 09:40 04/15/20 10:10
92473782004 N WALL Solid 04/14/20 09:50 04/15/20 10:10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 50
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92473782001 W WALL MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 6010D 2 PANTRB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC, KDW
92473782002 E WALL MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 6010D 2 PANTRB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC, KDW
92473782003 S WALL MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 6010D 2 PANTRB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC, KDW
92473782004 N WALL MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PANDWR
EPA 6010D 2 PANTRB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC, KDW
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:W WALL Lab ID:92473782001 Collected:04/14/20 09:30 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/17/20 09:37 N204/16/20 09:1813.9 13.9 1
Aliphatic (C19-C36)ND mg/kg 04/17/20 09:37 N204/16/20 09:1813.9 13.9 1
Aromatic (C11-C22)ND mg/kg 04/17/20 09:37 N204/16/20 09:1813.9 13.9 1
Surrogates
Nonatriacontane (S)70 %04/17/20 09:37 7194-86-704/16/20 09:1840-140 1
o-Terphenyl (S)76 %04/17/20 09:37 84-15-104/16/20 09:1840-140 1
2-Fluorobiphenyl (S)89 %04/17/20 09:37 321-60-804/16/20 09:1840-140 1
2-Bromonaphthalene (S)91 %04/17/20 09:37 580-13-204/16/20 09:1840-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND mg/kg 04/18/20 13:0204/14/20 09:306.87 2.29 1
Aliphatic (C09-C12)3.68J mg/kg 04/18/20 13:02 J04/14/20 09:306.87 2.29 1
Aromatic (C09-C10),Unadjusted ND mg/kg 04/18/20 13:02 TPHC9C10A MH04/14/20 09:306.87 2.29 1
Surrogates
2,5-Dibromotoluene (FID)102 %04/18/20 13:02 615-59-8FID04/14/20 09:3070.0-130 1
2,5-Dibromotoluene (PID)106 %04/18/20 13:02 615-59-8PID04/14/20 09:3070.0-130 1
Analytical Method: EPA 6010D Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICP) 6010D
Chromium 36.9 mg/kg 04/25/20 13:37 7440-47-304/24/20 22:491.50 0.751 1
Lead 4.18 mg/kg 04/25/20 13:37 7439-92-104/24/20 22:490.751 0.375 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/17/20 13:55 83-32-904/16/20 15:274641191
Acenaphthylene ND ug/kg 04/17/20 13:55 208-96-804/16/20 15:274641101
Aniline ND ug/kg 04/17/20 13:55 62-53-304/16/20 15:274641041
Anthracene ND ug/kg 04/17/20 13:55 120-12-704/16/20 15:274641201
Benzo(a)anthracene ND ug/kg 04/17/20 13:55 56-55-304/16/20 15:274641481
Benzo(a)pyrene ND ug/kg 04/17/20 13:55 50-32-804/16/20 15:274642011
Benzo(b)fluoranthene ND ug/kg 04/17/20 13:55 205-99-204/16/20 15:274641871
Benzo(g,h,i)perylene ND ug/kg 04/17/20 13:55 191-24-204/16/20 15:274641821
Benzo(k)fluoranthene ND ug/kg 04/17/20 13:55 207-08-904/16/20 15:274641961
Benzoic Acid ND ug/kg 04/17/20 13:55 65-85-004/16/20 15:2723205011
Benzyl alcohol ND ug/kg 04/17/20 13:55 100-51-604/16/20 15:279292461
4-Bromophenylphenyl ether ND ug/kg 04/17/20 13:55 101-55-304/16/20 15:274641221
Butylbenzylphthalate ND ug/kg 04/17/20 13:55 85-68-704/16/20 15:274641241
4-Chloro-3-methylphenol ND ug/kg 04/17/20 13:55 59-50-704/16/20 15:279292831
4-Chloroaniline ND ug/kg 04/17/20 13:55 106-47-804/16/20 15:279292841
bis(2-Chloroethoxy)methane ND ug/kg 04/17/20 13:55 111-91-104/16/20 15:274641241
bis(2-Chloroethyl) ether ND ug/kg 04/17/20 13:55 111-44-404/16/20 15:2746498.6 1
2-Chloronaphthalene ND ug/kg 04/17/20 13:55 91-58-704/16/20 15:274641031
2-Chlorophenol ND ug/kg 04/17/20 13:55 95-57-804/16/20 15:274641081
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
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Page 5 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:W WALL Lab ID:92473782001 Collected:04/14/20 09:30 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
4-Chlorophenylphenyl ether ND ug/kg 04/17/20 13:55 7005-72-304/16/20 15:274641211
Chrysene ND ug/kg 04/17/20 13:55 218-01-904/16/20 15:274641351
Dibenz(a,h)anthracene ND ug/kg 04/17/20 13:55 53-70-304/16/20 15:274641861
Dibenzofuran ND ug/kg 04/17/20 13:55 132-64-904/16/20 15:274641161
1,2-Dichlorobenzene ND ug/kg 04/17/20 13:55 95-50-104/16/20 15:274641001
1,3-Dichlorobenzene ND ug/kg 04/17/20 13:55 541-73-104/16/20 15:274641051
1,4-Dichlorobenzene ND ug/kg 04/17/20 13:55 106-46-704/16/20 15:274641021
3,3'-Dichlorobenzidine ND ug/kg 04/17/20 13:55 91-94-104/16/20 15:279293241
2,4-Dichlorophenol ND ug/kg 04/17/20 13:55 120-83-204/16/20 15:274641531
Diethylphthalate ND ug/kg 04/17/20 13:55 84-66-204/16/20 15:274641011
2,4-Dimethylphenol ND ug/kg 04/17/20 13:55 105-67-904/16/20 15:274641161
Dimethylphthalate ND ug/kg 04/17/20 13:55 131-11-304/16/20 15:274641051
Di-n-butylphthalate ND ug/kg 04/17/20 13:55 84-74-204/16/20 15:274641151
4,6-Dinitro-2-methylphenol ND ug/kg 04/17/20 13:55 534-52-104/16/20 15:279297491
2,4-Dinitrophenol ND ug/kg 04/17/20 13:55 51-28-504/16/20 15:27232014801
2,4-Dinitrotoluene ND ug/kg 04/17/20 13:55 121-14-204/16/20 15:274641231
2,6-Dinitrotoluene ND ug/kg 04/17/20 13:55 606-20-204/16/20 15:274641211
Di-n-octylphthalate ND ug/kg 04/17/20 13:55 117-84-004/16/20 15:274642651
bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/20 13:55 117-81-704/16/20 15:274641521
Fluoranthene ND ug/kg 04/17/20 13:55 206-44-004/16/20 15:274641401
Fluorene ND ug/kg 04/17/20 13:55 86-73-704/16/20 15:274641241
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 13:55 87-68-304/16/20 15:274641131
Hexachlorobenzene ND ug/kg 04/17/20 13:55 118-74-104/16/20 15:274641181
Hexachlorocyclopentadiene ND ug/kg 04/17/20 13:55 77-47-404/16/20 15:274641861
Hexachloroethane ND ug/kg 04/17/20 13:55 67-72-104/16/20 15:274641061
Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/20 13:55 193-39-504/16/20 15:274642121
Isophorone ND ug/kg 04/17/20 13:55 78-59-104/16/20 15:274641011
1-Methylnaphthalene ND ug/kg 04/17/20 13:55 90-12-004/16/20 15:274641241
2-Methylnaphthalene ND ug/kg 04/17/20 13:55 91-57-604/16/20 15:274641181
2-Methylphenol(o-Cresol)ND ug/kg 04/17/20 13:55 95-48-704/16/20 15:274641031
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/20 13:55 15831-10-404/16/20 15:274641171
Naphthalene ND ug/kg 04/17/20 13:55 91-20-304/16/20 15:274641111
2-Nitroaniline ND ug/kg 04/17/20 13:55 88-74-404/16/20 15:2723202341
3-Nitroaniline ND ug/kg 04/17/20 13:55 99-09-204/16/20 15:2723202461
4-Nitroaniline ND ug/kg 04/17/20 13:55 100-01-604/16/20 15:279292291
Nitrobenzene ND ug/kg 04/17/20 13:55 98-95-304/16/20 15:274641111
2-Nitrophenol ND ug/kg 04/17/20 13:55 88-75-504/16/20 15:274641441
4-Nitrophenol ND ug/kg 04/17/20 13:55 100-02-704/16/20 15:2723207401
N-Nitrosodimethylamine ND ug/kg 04/17/20 13:55 62-75-904/16/20 15:274641311
N-Nitroso-di-n-propylamine ND ug/kg 04/17/20 13:55 621-64-704/16/20 15:274641301
N-Nitrosodiphenylamine ND ug/kg 04/17/20 13:55 86-30-604/16/20 15:274641181
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/20 13:55 108-60-104/16/20 15:274641291
Pentachlorophenol ND ug/kg 04/17/20 13:55 87-86-504/16/20 15:279292121
Phenanthrene ND ug/kg 04/17/20 13:55 85-01-804/16/20 15:274641171
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:W WALL Lab ID:92473782001 Collected:04/14/20 09:30 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Phenol ND ug/kg 04/17/20 13:55 108-95-204/16/20 15:274641111
Pyrene ND ug/kg 04/17/20 13:55 129-00-004/16/20 15:274641281
Pyridine ND ug/kg 04/17/20 13:55 110-86-104/16/20 15:274641181
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 13:55 120-82-104/16/20 15:274641061
2,4,5-Trichlorophenol ND ug/kg 04/17/20 13:55 95-95-404/16/20 15:274641211
2,4,6-Trichlorophenol ND ug/kg 04/17/20 13:55 88-06-204/16/20 15:274641171
Surrogates
Nitrobenzene-d5 (S)56 %04/17/20 13:55 4165-60-004/16/20 15:2723-110 1
2-Fluorobiphenyl (S)28 %04/17/20 13:55 321-60-8 S004/16/20 15:2730-110 1
Terphenyl-d14 (S)68 %04/17/20 13:55 1718-51-004/16/20 15:2728-110 1
Phenol-d6 (S)65 %04/17/20 13:55 13127-88-304/16/20 15:2722-110 1
2-Fluorophenol (S)62 %04/17/20 13:55 367-12-404/16/20 15:2713-110 1
2,4,6-Tribromophenol (S)62 %04/17/20 13:55 118-79-604/16/20 15:2727-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone ND ug/kg 04/17/20 12:06 67-64-104/17/20 10:141059.9 1
Benzene ND ug/kg 04/17/20 12:06 71-43-204/17/20 10:145.2 0.94 1
Bromobenzene ND ug/kg 04/17/20 12:06 108-86-104/17/20 10:145.2 1.4 1
Bromochloromethane ND ug/kg 04/17/20 12:06 74-97-504/17/20 10:145.2 1.3 1
Bromodichloromethane ND ug/kg 04/17/20 12:06 75-27-404/17/20 10:145.2 1.0 1
Bromoform ND ug/kg 04/17/20 12:06 75-25-204/17/20 10:145.2 2.6 1
Bromomethane ND ug/kg 04/17/20 12:06 74-83-9 IH04/17/20 10:1410.5 2.5 1
2-Butanone (MEK)ND ug/kg 04/17/20 12:06 78-93-304/17/20 10:1410512.5 1
n-Butylbenzene ND ug/kg 04/17/20 12:06 104-51-804/17/20 10:145.2 3.0 1
sec-Butylbenzene ND ug/kg 04/17/20 12:06 135-98-804/17/20 10:145.2 2.2 1
tert-Butylbenzene ND ug/kg 04/17/20 12:06 98-06-604/17/20 10:145.2 1.8 1
Carbon tetrachloride ND ug/kg 04/17/20 12:06 56-23-504/17/20 10:145.2 1.0 1
Chlorobenzene ND ug/kg 04/17/20 12:06 108-90-704/17/20 10:145.2 1.0 1
Chloroethane ND ug/kg 04/17/20 12:06 75-00-304/17/20 10:1410.5 2.2 1
Chloroform ND ug/kg 04/17/20 12:06 67-66-304/17/20 10:145.2 1.1 1
Chloromethane ND ug/kg 04/17/20 12:06 74-87-304/17/20 10:1410.5 3.4 1
2-Chlorotoluene ND ug/kg 04/17/20 12:06 95-49-804/17/20 10:145.2 1.6 1
4-Chlorotoluene ND ug/kg 04/17/20 12:06 106-43-404/17/20 10:145.2 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/17/20 12:06 96-12-8 v104/17/20 10:145.2 2.7 1
Dibromochloromethane ND ug/kg 04/17/20 12:06 124-48-104/17/20 10:145.2 2.6 1
1,2-Dibromoethane (EDB)ND ug/kg 04/17/20 12:06 106-93-404/17/20 10:145.2 1.2 1
Dibromomethane ND ug/kg 04/17/20 12:06 74-95-304/17/20 10:145.2 1.6 1
1,2-Dichlorobenzene ND ug/kg 04/17/20 12:06 95-50-104/17/20 10:145.2 1.8 1
1,3-Dichlorobenzene ND ug/kg 04/17/20 12:06 541-73-104/17/20 10:145.2 1.9 1
1,4-Dichlorobenzene ND ug/kg 04/17/20 12:06 106-46-704/17/20 10:145.2 1.8 1
Dichlorodifluoromethane ND ug/kg 04/17/20 12:06 75-71-8 v204/17/20 10:1410.5 4.3 1
1,1-Dichloroethane ND ug/kg 04/17/20 12:06 75-34-304/17/20 10:145.2 0.77 1
1,2-Dichloroethane ND ug/kg 04/17/20 12:06 107-06-204/17/20 10:145.2 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:W WALL Lab ID:92473782001 Collected:04/14/20 09:30 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 04/17/20 12:06 75-35-404/17/20 10:145.2 1.2 1
cis-1,2-Dichloroethene ND ug/kg 04/17/20 12:06 156-59-204/17/20 10:145.2 0.91 1
trans-1,2-Dichloroethene ND ug/kg 04/17/20 12:06 156-60-504/17/20 10:145.2 1.0 1
1,2-Dichloropropane ND ug/kg 04/17/20 12:06 78-87-504/17/20 10:145.2 2.0 1
1,3-Dichloropropane ND ug/kg 04/17/20 12:06 142-28-904/17/20 10:145.2 2.0 1
2,2-Dichloropropane ND ug/kg 04/17/20 12:06 594-20-704/17/20 10:145.2 0.52 1
1,1-Dichloropropene ND ug/kg 04/17/20 12:06 563-58-604/17/20 10:145.2 2.2 1
cis-1,3-Dichloropropene ND ug/kg 04/17/20 12:06 10061-01-504/17/20 10:145.2 2.4 1
trans-1,3-Dichloropropene ND ug/kg 04/17/20 12:06 10061-02-604/17/20 10:145.2 0.92 1
Diisopropyl ether ND ug/kg 04/17/20 12:06 108-20-304/17/20 10:145.2 3.0 1
Ethylbenzene ND ug/kg 04/17/20 12:06 100-41-404/17/20 10:145.2 1.1 1
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 12:06 87-68-304/17/20 10:145.2 2.6 1
2-Hexanone ND ug/kg 04/17/20 12:06 591-78-604/17/20 10:1452.4 5.4 1
Isopropylbenzene (Cumene)ND ug/kg 04/17/20 12:06 98-82-804/17/20 10:145.2 1.5 1
p-Isopropyltoluene ND ug/kg 04/17/20 12:06 99-87-604/17/20 10:145.2 2.5 1
Methylene Chloride ND ug/kg 04/17/20 12:06 75-09-2 v104/17/20 10:1421.0 6.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/17/20 12:06 108-10-104/17/20 10:1452.4 3.9 1
Methyl-tert-butyl ether ND ug/kg 04/17/20 12:06 1634-04-404/17/20 10:145.2 3.0 1
Naphthalene ND ug/kg 04/17/20 12:06 91-20-304/17/20 10:145.2 4.5 1
n-Propylbenzene ND ug/kg 04/17/20 12:06 103-65-104/17/20 10:145.2 1.8 1
Styrene ND ug/kg 04/17/20 12:06 100-42-504/17/20 10:145.2 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/17/20 12:06 630-20-604/17/20 10:145.2 1.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/17/20 12:06 79-34-504/17/20 10:145.2 1.8 1
Tetrachloroethene ND ug/kg 04/17/20 12:06 127-18-404/17/20 10:145.2 1.7 1
Toluene ND ug/kg 04/17/20 12:06 108-88-304/17/20 10:145.2 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 04/17/20 12:06 87-61-604/17/20 10:145.2 3.7 1
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 12:06 120-82-104/17/20 10:145.2 2.8 1
1,1,1-Trichloroethane ND ug/kg 04/17/20 12:06 71-55-604/17/20 10:145.2 0.91 1
1,1,2-Trichloroethane ND ug/kg 04/17/20 12:06 79-00-504/17/20 10:145.2 1.2 1
Trichloroethene ND ug/kg 04/17/20 12:06 79-01-604/17/20 10:145.2 1.4 1
Trichlorofluoromethane ND ug/kg 04/17/20 12:06 75-69-404/17/20 10:145.2 1.2 1
1,2,3-Trichloropropane ND ug/kg 04/17/20 12:06 96-18-404/17/20 10:145.2 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 04/17/20 12:06 95-63-604/17/20 10:145.2 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/17/20 12:06 108-67-804/17/20 10:145.2 1.8 1
Vinyl acetate ND ug/kg 04/17/20 12:06 108-05-404/17/20 10:1452.4 17.1 1
Vinyl chloride ND ug/kg 04/17/20 12:06 75-01-4 v204/17/20 10:1410.5 2.0 1
Xylene (Total)ND ug/kg 04/17/20 12:06 1330-20-704/17/20 10:1410.5 3.7 1
m&p-Xylene ND ug/kg 04/17/20 12:06 179601-23-104/17/20 10:1410.5 2.5 1
o-Xylene ND ug/kg 04/17/20 12:06 95-47-604/17/20 10:145.2 1.2 1
Surrogates
Toluene-d8 (S)101 %04/17/20 12:06 2037-26-504/17/20 10:1470-130 1
4-Bromofluorobenzene (S)106 %04/17/20 12:06 460-00-404/17/20 10:1470-130 1
1,2-Dichloroethane-d4 (S)98 %04/17/20 12:06 17060-07-004/17/20 10:1470-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:W WALL Lab ID:92473782001 Collected:04/14/20 09:30 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.7 %04/16/20 13:290.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 66.6 %04/28/20 11:3504/28/20 11:261
Total Solids 72.8 %04/20/20 07:5504/20/20 07:491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:E WALL Lab ID:92473782002 Collected:04/14/20 10:00 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/17/20 10:04 N204/16/20 09:1814.3 14.3 1
Aliphatic (C19-C36)ND mg/kg 04/17/20 10:04 N204/16/20 09:1814.3 14.3 1
Aromatic (C11-C22)ND mg/kg 04/17/20 10:04 N204/16/20 09:1814.3 14.3 1
Surrogates
Nonatriacontane (S)92 %04/17/20 10:04 7194-86-704/16/20 09:1840-140 1
o-Terphenyl (S)80 %04/17/20 10:04 84-15-104/16/20 09:1840-140 1
2-Fluorobiphenyl (S)95 %04/17/20 10:04 321-60-804/16/20 09:1840-140 1
2-Bromonaphthalene (S)98 %04/17/20 10:04 580-13-204/16/20 09:1840-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND mg/kg 04/18/20 13:3404/14/20 10:007.10 2.37 1
Aliphatic (C09-C12)ND mg/kg 04/18/20 13:3404/14/20 10:007.10 2.37 1
Aromatic (C09-C10),Unadjusted ND mg/kg 04/18/20 13:34 TPHC9C10A04/14/20 10:007.10 2.37 1
Surrogates
2,5-Dibromotoluene (FID)105 %04/18/20 13:34 615-59-8FID04/14/20 10:0070.0-130 1
2,5-Dibromotoluene (PID)108 %04/18/20 13:34 615-59-8PID04/14/20 10:0070.0-130 1
Analytical Method: EPA 6010D Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICP) 6010D
Chromium 34.5 mg/kg 04/25/20 13:40 7440-47-304/24/20 22:491.53 0.767 1
Lead ND mg/kg 04/25/20 13:40 7439-92-104/24/20 22:490.767 0.384 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/17/20 12:04 83-32-904/16/20 15:274631191
Acenaphthylene ND ug/kg 04/17/20 12:04 208-96-804/16/20 15:274631101
Aniline ND ug/kg 04/17/20 12:04 62-53-304/16/20 15:274631041
Anthracene ND ug/kg 04/17/20 12:04 120-12-704/16/20 15:274631201
Benzo(a)anthracene ND ug/kg 04/17/20 12:04 56-55-304/16/20 15:274631471
Benzo(a)pyrene ND ug/kg 04/17/20 12:04 50-32-804/16/20 15:274632011
Benzo(b)fluoranthene ND ug/kg 04/17/20 12:04 205-99-204/16/20 15:274631871
Benzo(g,h,i)perylene ND ug/kg 04/17/20 12:04 191-24-204/16/20 15:274631811
Benzo(k)fluoranthene ND ug/kg 04/17/20 12:04 207-08-904/16/20 15:274631951
Benzoic Acid ND ug/kg 04/17/20 12:04 65-85-004/16/20 15:2723104991
Benzyl alcohol ND ug/kg 04/17/20 12:04 100-51-604/16/20 15:279262461
4-Bromophenylphenyl ether ND ug/kg 04/17/20 12:04 101-55-304/16/20 15:274631221
Butylbenzylphthalate ND ug/kg 04/17/20 12:04 85-68-704/16/20 15:274631231
4-Chloro-3-methylphenol ND ug/kg 04/17/20 12:04 59-50-704/16/20 15:279262821
4-Chloroaniline ND ug/kg 04/17/20 12:04 106-47-804/16/20 15:279262831
bis(2-Chloroethoxy)methane ND ug/kg 04/17/20 12:04 111-91-104/16/20 15:274631241
bis(2-Chloroethyl) ether ND ug/kg 04/17/20 12:04 111-44-404/16/20 15:2746398.4 1
2-Chloronaphthalene ND ug/kg 04/17/20 12:04 91-58-704/16/20 15:274631031
2-Chlorophenol ND ug/kg 04/17/20 12:04 95-57-804/16/20 15:274631081
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:E WALL Lab ID:92473782002 Collected:04/14/20 10:00 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
4-Chlorophenylphenyl ether ND ug/kg 04/17/20 12:04 7005-72-304/16/20 15:274631201
Chrysene ND ug/kg 04/17/20 12:04 218-01-904/16/20 15:274631341
Dibenz(a,h)anthracene ND ug/kg 04/17/20 12:04 53-70-304/16/20 15:274631851
Dibenzofuran ND ug/kg 04/17/20 12:04 132-64-904/16/20 15:274631161
1,2-Dichlorobenzene ND ug/kg 04/17/20 12:04 95-50-104/16/20 15:274631001
1,3-Dichlorobenzene ND ug/kg 04/17/20 12:04 541-73-104/16/20 15:274631041
1,4-Dichlorobenzene ND ug/kg 04/17/20 12:04 106-46-704/16/20 15:274631021
3,3'-Dichlorobenzidine ND ug/kg 04/17/20 12:04 91-94-104/16/20 15:279263231
2,4-Dichlorophenol ND ug/kg 04/17/20 12:04 120-83-204/16/20 15:274631531
Diethylphthalate ND ug/kg 04/17/20 12:04 84-66-204/16/20 15:274631001
2,4-Dimethylphenol ND ug/kg 04/17/20 12:04 105-67-904/16/20 15:274631151
Dimethylphthalate ND ug/kg 04/17/20 12:04 131-11-304/16/20 15:274631051
Di-n-butylphthalate ND ug/kg 04/17/20 12:04 84-74-204/16/20 15:274631141
4,6-Dinitro-2-methylphenol ND ug/kg 04/17/20 12:04 534-52-104/16/20 15:279267461
2,4-Dinitrophenol ND ug/kg 04/17/20 12:04 51-28-504/16/20 15:27231014801
2,4-Dinitrotoluene ND ug/kg 04/17/20 12:04 121-14-204/16/20 15:274631231
2,6-Dinitrotoluene ND ug/kg 04/17/20 12:04 606-20-204/16/20 15:274631211
Di-n-octylphthalate ND ug/kg 04/17/20 12:04 117-84-004/16/20 15:274632641
bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/20 12:04 117-81-704/16/20 15:274631521
Fluoranthene ND ug/kg 04/17/20 12:04 206-44-004/16/20 15:274631401
Fluorene ND ug/kg 04/17/20 12:04 86-73-704/16/20 15:274631241
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 12:04 87-68-304/16/20 15:274631131
Hexachlorobenzene ND ug/kg 04/17/20 12:04 118-74-104/16/20 15:274631181
Hexachlorocyclopentadiene ND ug/kg 04/17/20 12:04 77-47-404/16/20 15:274631851
Hexachloroethane ND ug/kg 04/17/20 12:04 67-72-104/16/20 15:274631061
Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/20 12:04 193-39-504/16/20 15:274632121
Isophorone ND ug/kg 04/17/20 12:04 78-59-104/16/20 15:274631011
1-Methylnaphthalene ND ug/kg 04/17/20 12:04 90-12-004/16/20 15:274631231
2-Methylnaphthalene ND ug/kg 04/17/20 12:04 91-57-604/16/20 15:274631181
2-Methylphenol(o-Cresol)ND ug/kg 04/17/20 12:04 95-48-704/16/20 15:274631031
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/20 12:04 15831-10-404/16/20 15:274631161
Naphthalene ND ug/kg 04/17/20 12:04 91-20-304/16/20 15:274631111
2-Nitroaniline ND ug/kg 04/17/20 12:04 88-74-404/16/20 15:2723102331
3-Nitroaniline ND ug/kg 04/17/20 12:04 99-09-204/16/20 15:2723102461
4-Nitroaniline ND ug/kg 04/17/20 12:04 100-01-604/16/20 15:279262291
Nitrobenzene ND ug/kg 04/17/20 12:04 98-95-304/16/20 15:274631111
2-Nitrophenol ND ug/kg 04/17/20 12:04 88-75-504/16/20 15:274631431
4-Nitrophenol ND ug/kg 04/17/20 12:04 100-02-704/16/20 15:2723107381
N-Nitrosodimethylamine ND ug/kg 04/17/20 12:04 62-75-904/16/20 15:274631301
N-Nitroso-di-n-propylamine ND ug/kg 04/17/20 12:04 621-64-704/16/20 15:274631301
N-Nitrosodiphenylamine ND ug/kg 04/17/20 12:04 86-30-604/16/20 15:274631181
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/20 12:04 108-60-104/16/20 15:274631291
Pentachlorophenol ND ug/kg 04/17/20 12:04 87-86-504/16/20 15:279262121
Phenanthrene ND ug/kg 04/17/20 12:04 85-01-804/16/20 15:274631171
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:E WALL Lab ID:92473782002 Collected:04/14/20 10:00 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Phenol ND ug/kg 04/17/20 12:04 108-95-204/16/20 15:274631111
Pyrene ND ug/kg 04/17/20 12:04 129-00-004/16/20 15:274631271
Pyridine ND ug/kg 04/17/20 12:04 110-86-104/16/20 15:274631171
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 12:04 120-82-104/16/20 15:274631061
2,4,5-Trichlorophenol ND ug/kg 04/17/20 12:04 95-95-404/16/20 15:274631201
2,4,6-Trichlorophenol ND ug/kg 04/17/20 12:04 88-06-204/16/20 15:274631161
Surrogates
Nitrobenzene-d5 (S)69 %04/17/20 12:04 4165-60-004/16/20 15:2723-110 1
2-Fluorobiphenyl (S)61 %04/17/20 12:04 321-60-804/16/20 15:2730-110 1
Terphenyl-d14 (S)92 %04/17/20 12:04 1718-51-004/16/20 15:2728-110 1
Phenol-d6 (S)72 %04/17/20 12:04 13127-88-304/16/20 15:2722-110 1
2-Fluorophenol (S)69 %04/17/20 12:04 367-12-404/16/20 15:2713-110 1
2,4,6-Tribromophenol (S)73 %04/17/20 12:04 118-79-604/16/20 15:2727-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone 63.0J ug/kg 04/17/20 12:30 67-64-104/17/20 10:1411010.4 1
Benzene ND ug/kg 04/17/20 12:30 71-43-204/17/20 10:145.5 0.99 1
Bromobenzene ND ug/kg 04/17/20 12:30 108-86-104/17/20 10:145.5 1.5 1
Bromochloromethane ND ug/kg 04/17/20 12:30 74-97-504/17/20 10:145.5 1.4 1
Bromodichloromethane ND ug/kg 04/17/20 12:30 75-27-404/17/20 10:145.5 1.1 1
Bromoform ND ug/kg 04/17/20 12:30 75-25-204/17/20 10:145.5 2.7 1
Bromomethane ND ug/kg 04/17/20 12:30 74-83-9 IH04/17/20 10:1411.0 2.6 1
2-Butanone (MEK)ND ug/kg 04/17/20 12:30 78-93-304/17/20 10:1411013.1 1
n-Butylbenzene ND ug/kg 04/17/20 12:30 104-51-804/17/20 10:145.5 3.1 1
sec-Butylbenzene ND ug/kg 04/17/20 12:30 135-98-804/17/20 10:145.5 2.3 1
tert-Butylbenzene ND ug/kg 04/17/20 12:30 98-06-604/17/20 10:145.5 1.9 1
Carbon tetrachloride ND ug/kg 04/17/20 12:30 56-23-504/17/20 10:145.5 1.1 1
Chlorobenzene ND ug/kg 04/17/20 12:30 108-90-704/17/20 10:145.5 1.1 1
Chloroethane ND ug/kg 04/17/20 12:30 75-00-304/17/20 10:1411.0 2.3 1
Chloroform ND ug/kg 04/17/20 12:30 67-66-304/17/20 10:145.5 1.2 1
Chloromethane ND ug/kg 04/17/20 12:30 74-87-304/17/20 10:1411.0 3.6 1
2-Chlorotoluene ND ug/kg 04/17/20 12:30 95-49-804/17/20 10:145.5 1.7 1
4-Chlorotoluene ND ug/kg 04/17/20 12:30 106-43-404/17/20 10:145.5 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/17/20 12:30 96-12-8 v104/17/20 10:145.5 2.8 1
Dibromochloromethane ND ug/kg 04/17/20 12:30 124-48-104/17/20 10:145.5 2.8 1
1,2-Dibromoethane (EDB)ND ug/kg 04/17/20 12:30 106-93-404/17/20 10:145.5 1.2 1
Dibromomethane ND ug/kg 04/17/20 12:30 74-95-304/17/20 10:145.5 1.6 1
1,2-Dichlorobenzene ND ug/kg 04/17/20 12:30 95-50-104/17/20 10:145.5 1.9 1
1,3-Dichlorobenzene ND ug/kg 04/17/20 12:30 541-73-104/17/20 10:145.5 2.0 1
1,4-Dichlorobenzene ND ug/kg 04/17/20 12:30 106-46-704/17/20 10:145.5 1.9 1
Dichlorodifluoromethane ND ug/kg 04/17/20 12:30 75-71-8 v304/17/20 10:1411.0 4.5 1
1,1-Dichloroethane ND ug/kg 04/17/20 12:30 75-34-304/17/20 10:145.5 0.81 1
1,2-Dichloroethane ND ug/kg 04/17/20 12:30 107-06-204/17/20 10:145.5 1.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:E WALL Lab ID:92473782002 Collected:04/14/20 10:00 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 04/17/20 12:30 75-35-404/17/20 10:145.5 1.3 1
cis-1,2-Dichloroethene ND ug/kg 04/17/20 12:30 156-59-204/17/20 10:145.5 0.96 1
trans-1,2-Dichloroethene ND ug/kg 04/17/20 12:30 156-60-504/17/20 10:145.5 1.1 1
1,2-Dichloropropane ND ug/kg 04/17/20 12:30 78-87-504/17/20 10:145.5 2.1 1
1,3-Dichloropropane ND ug/kg 04/17/20 12:30 142-28-904/17/20 10:145.5 2.1 1
2,2-Dichloropropane ND ug/kg 04/17/20 12:30 594-20-704/17/20 10:145.5 0.55 1
1,1-Dichloropropene ND ug/kg 04/17/20 12:30 563-58-604/17/20 10:145.5 2.3 1
cis-1,3-Dichloropropene ND ug/kg 04/17/20 12:30 10061-01-504/17/20 10:145.5 2.5 1
trans-1,3-Dichloropropene ND ug/kg 04/17/20 12:30 10061-02-604/17/20 10:145.5 0.97 1
Diisopropyl ether ND ug/kg 04/17/20 12:30 108-20-304/17/20 10:145.5 3.2 1
Ethylbenzene ND ug/kg 04/17/20 12:30 100-41-404/17/20 10:145.5 1.2 1
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 12:30 87-68-304/17/20 10:145.5 2.7 1
2-Hexanone ND ug/kg 04/17/20 12:30 591-78-604/17/20 10:1455.2 5.7 1
Isopropylbenzene (Cumene)ND ug/kg 04/17/20 12:30 98-82-804/17/20 10:145.5 1.6 1
p-Isopropyltoluene ND ug/kg 04/17/20 12:30 99-87-604/17/20 10:145.5 2.7 1
Methylene Chloride ND ug/kg 04/17/20 12:30 75-09-2 v104/17/20 10:1422.1 6.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/17/20 12:30 108-10-104/17/20 10:1455.2 4.1 1
Methyl-tert-butyl ether ND ug/kg 04/17/20 12:30 1634-04-404/17/20 10:145.5 3.2 1
Naphthalene ND ug/kg 04/17/20 12:30 91-20-304/17/20 10:145.5 4.7 1
n-Propylbenzene ND ug/kg 04/17/20 12:30 103-65-104/17/20 10:145.5 1.8 1
Styrene ND ug/kg 04/17/20 12:30 100-42-504/17/20 10:145.5 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/17/20 12:30 630-20-604/17/20 10:145.5 1.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/17/20 12:30 79-34-504/17/20 10:145.5 1.9 1
Tetrachloroethene ND ug/kg 04/17/20 12:30 127-18-404/17/20 10:145.5 1.7 1
Toluene ND ug/kg 04/17/20 12:30 108-88-304/17/20 10:145.5 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 04/17/20 12:30 87-61-604/17/20 10:145.5 3.9 1
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 12:30 120-82-104/17/20 10:145.5 2.9 1
1,1,1-Trichloroethane ND ug/kg 04/17/20 12:30 71-55-604/17/20 10:145.5 0.96 1
1,1,2-Trichloroethane ND ug/kg 04/17/20 12:30 79-00-504/17/20 10:145.5 1.2 1
Trichloroethene ND ug/kg 04/17/20 12:30 79-01-604/17/20 10:145.5 1.4 1
Trichlorofluoromethane ND ug/kg 04/17/20 12:30 75-69-404/17/20 10:145.5 1.3 1
1,2,3-Trichloropropane ND ug/kg 04/17/20 12:30 96-18-404/17/20 10:145.5 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 04/17/20 12:30 95-63-604/17/20 10:145.5 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 04/17/20 12:30 108-67-804/17/20 10:145.5 1.8 1
Vinyl acetate ND ug/kg 04/17/20 12:30 108-05-404/17/20 10:1455.2 18.0 1
Vinyl chloride ND ug/kg 04/17/20 12:30 75-01-4 v304/17/20 10:1411.0 2.1 1
Xylene (Total)ND ug/kg 04/17/20 12:30 1330-20-704/17/20 10:1411.0 3.9 1
m&p-Xylene ND ug/kg 04/17/20 12:30 179601-23-104/17/20 10:1411.0 2.6 1
o-Xylene ND ug/kg 04/17/20 12:30 95-47-604/17/20 10:145.5 1.3 1
Surrogates
Toluene-d8 (S)101 %04/17/20 12:30 2037-26-504/17/20 10:1470-130 1
4-Bromofluorobenzene (S)94 %04/17/20 12:30 460-00-404/17/20 10:1470-130 1
1,2-Dichloroethane-d4 (S)98 %04/17/20 12:30 17060-07-004/17/20 10:1470-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:E WALL Lab ID:92473782002 Collected:04/14/20 10:00 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 29.4 %04/16/20 13:290.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 65.2 %04/28/20 11:3504/28/20 11:261
Total Solids 70.4 %04/20/20 07:5504/20/20 07:491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:S WALL Lab ID:92473782003 Collected:04/14/20 09:40 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/17/20 10:31 N204/16/20 09:1814.6 14.6 1
Aliphatic (C19-C36)ND mg/kg 04/17/20 10:31 N204/16/20 09:1814.6 14.6 1
Aromatic (C11-C22)ND mg/kg 04/17/20 10:31 N204/16/20 09:1814.6 14.6 1
Surrogates
Nonatriacontane (S)78 %04/17/20 10:31 7194-86-704/16/20 09:1840-140 1
o-Terphenyl (S)83 %04/17/20 10:31 84-15-104/16/20 09:1840-140 1
2-Fluorobiphenyl (S)99 %04/17/20 10:31 321-60-804/16/20 09:1840-140 1
2-Bromonaphthalene (S)102 %04/17/20 10:31 580-13-204/16/20 09:1840-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND mg/kg 04/18/20 14:0704/14/20 09:407.20 2.40 1
Aliphatic (C09-C12)ND mg/kg 04/18/20 14:0704/14/20 09:407.20 2.40 1
Aromatic (C09-C10),Unadjusted ND mg/kg 04/18/20 14:07 TPHC9C10A04/14/20 09:407.20 2.40 1
Surrogates
2,5-Dibromotoluene (FID)103 %04/18/20 14:07 615-59-8FID04/14/20 09:4070.0-130 1
2,5-Dibromotoluene (PID)106 %04/18/20 14:07 615-59-8PID04/14/20 09:4070.0-130 1
Analytical Method: EPA 6010D Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICP) 6010D
Chromium 79.6 mg/kg 04/25/20 13:42 7440-47-304/24/20 22:491.63 0.813 1
Lead ND mg/kg 04/25/20 13:42 7439-92-104/24/20 22:490.813 0.406 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/17/20 12:32 83-32-904/16/20 15:274801231
Acenaphthylene ND ug/kg 04/17/20 12:32 208-96-804/16/20 15:274801141
Aniline ND ug/kg 04/17/20 12:32 62-53-304/16/20 15:274801081
Anthracene ND ug/kg 04/17/20 12:32 120-12-704/16/20 15:274801241
Benzo(a)anthracene ND ug/kg 04/17/20 12:32 56-55-304/16/20 15:274801531
Benzo(a)pyrene ND ug/kg 04/17/20 12:32 50-32-804/16/20 15:274802081
Benzo(b)fluoranthene ND ug/kg 04/17/20 12:32 205-99-204/16/20 15:274801931
Benzo(g,h,i)perylene ND ug/kg 04/17/20 12:32 191-24-204/16/20 15:274801881
Benzo(k)fluoranthene ND ug/kg 04/17/20 12:32 207-08-904/16/20 15:274802021
Benzoic Acid ND ug/kg 04/17/20 12:32 65-85-004/16/20 15:2724005171
Benzyl alcohol ND ug/kg 04/17/20 12:32 100-51-604/16/20 15:279592541
4-Bromophenylphenyl ether ND ug/kg 04/17/20 12:32 101-55-304/16/20 15:274801261
Butylbenzylphthalate ND ug/kg 04/17/20 12:32 85-68-704/16/20 15:274801281
4-Chloro-3-methylphenol ND ug/kg 04/17/20 12:32 59-50-704/16/20 15:279592921
4-Chloroaniline ND ug/kg 04/17/20 12:32 106-47-804/16/20 15:279592941
bis(2-Chloroethoxy)methane ND ug/kg 04/17/20 12:32 111-91-104/16/20 15:274801281
bis(2-Chloroethyl) ether ND ug/kg 04/17/20 12:32 111-44-404/16/20 15:274801021
2-Chloronaphthalene ND ug/kg 04/17/20 12:32 91-58-704/16/20 15:274801071
2-Chlorophenol ND ug/kg 04/17/20 12:32 95-57-804/16/20 15:274801121
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:S WALL Lab ID:92473782003 Collected:04/14/20 09:40 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
4-Chlorophenylphenyl ether ND ug/kg 04/17/20 12:32 7005-72-304/16/20 15:274801251
Chrysene ND ug/kg 04/17/20 12:32 218-01-904/16/20 15:274801391
Dibenz(a,h)anthracene ND ug/kg 04/17/20 12:32 53-70-304/16/20 15:274801921
Dibenzofuran ND ug/kg 04/17/20 12:32 132-64-904/16/20 15:274801201
1,2-Dichlorobenzene ND ug/kg 04/17/20 12:32 95-50-104/16/20 15:274801041
1,3-Dichlorobenzene ND ug/kg 04/17/20 12:32 541-73-104/16/20 15:274801081
1,4-Dichlorobenzene ND ug/kg 04/17/20 12:32 106-46-704/16/20 15:274801061
3,3'-Dichlorobenzidine ND ug/kg 04/17/20 12:32 91-94-104/16/20 15:279593341
2,4-Dichlorophenol ND ug/kg 04/17/20 12:32 120-83-204/16/20 15:274801581
Diethylphthalate ND ug/kg 04/17/20 12:32 84-66-204/16/20 15:274801041
2,4-Dimethylphenol ND ug/kg 04/17/20 12:32 105-67-904/16/20 15:274801191
Dimethylphthalate ND ug/kg 04/17/20 12:32 131-11-304/16/20 15:274801081
Di-n-butylphthalate ND ug/kg 04/17/20 12:32 84-74-204/16/20 15:274801181
4,6-Dinitro-2-methylphenol ND ug/kg 04/17/20 12:32 534-52-104/16/20 15:279597731
2,4-Dinitrophenol ND ug/kg 04/17/20 12:32 51-28-504/16/20 15:27240015301
2,4-Dinitrotoluene ND ug/kg 04/17/20 12:32 121-14-204/16/20 15:274801271
2,6-Dinitrotoluene ND ug/kg 04/17/20 12:32 606-20-204/16/20 15:274801251
Di-n-octylphthalate ND ug/kg 04/17/20 12:32 117-84-004/16/20 15:274802731
bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/20 12:32 117-81-704/16/20 15:274801571
Fluoranthene ND ug/kg 04/17/20 12:32 206-44-004/16/20 15:274801451
Fluorene ND ug/kg 04/17/20 12:32 86-73-704/16/20 15:274801281
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 12:32 87-68-304/16/20 15:274801171
Hexachlorobenzene ND ug/kg 04/17/20 12:32 118-74-104/16/20 15:274801221
Hexachlorocyclopentadiene ND ug/kg 04/17/20 12:32 77-47-404/16/20 15:274801921
Hexachloroethane ND ug/kg 04/17/20 12:32 67-72-104/16/20 15:274801091
Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/20 12:32 193-39-504/16/20 15:274802191
Isophorone ND ug/kg 04/17/20 12:32 78-59-104/16/20 15:274801041
1-Methylnaphthalene ND ug/kg 04/17/20 12:32 90-12-004/16/20 15:274801281
2-Methylnaphthalene ND ug/kg 04/17/20 12:32 91-57-604/16/20 15:274801221
2-Methylphenol(o-Cresol)ND ug/kg 04/17/20 12:32 95-48-704/16/20 15:274801061
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/20 12:32 15831-10-404/16/20 15:274801211
Naphthalene ND ug/kg 04/17/20 12:32 91-20-304/16/20 15:274801151
2-Nitroaniline ND ug/kg 04/17/20 12:32 88-74-404/16/20 15:2724002411
3-Nitroaniline ND ug/kg 04/17/20 12:32 99-09-204/16/20 15:2724002541
4-Nitroaniline ND ug/kg 04/17/20 12:32 100-01-604/16/20 15:279592371
Nitrobenzene ND ug/kg 04/17/20 12:32 98-95-304/16/20 15:274801151
2-Nitrophenol ND ug/kg 04/17/20 12:32 88-75-504/16/20 15:274801481
4-Nitrophenol ND ug/kg 04/17/20 12:32 100-02-704/16/20 15:2724007651
N-Nitrosodimethylamine ND ug/kg 04/17/20 12:32 62-75-904/16/20 15:274801351
N-Nitroso-di-n-propylamine ND ug/kg 04/17/20 12:32 621-64-704/16/20 15:274801341
N-Nitrosodiphenylamine ND ug/kg 04/17/20 12:32 86-30-604/16/20 15:274801221
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/20 12:32 108-60-104/16/20 15:274801331
Pentachlorophenol ND ug/kg 04/17/20 12:32 87-86-504/16/20 15:279592191
Phenanthrene ND ug/kg 04/17/20 12:32 85-01-804/16/20 15:274801211
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:S WALL Lab ID:92473782003 Collected:04/14/20 09:40 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Phenol ND ug/kg 04/17/20 12:32 108-95-204/16/20 15:274801151
Pyrene ND ug/kg 04/17/20 12:32 129-00-004/16/20 15:274801321
Pyridine ND ug/kg 04/17/20 12:32 110-86-104/16/20 15:274801211
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 12:32 120-82-104/16/20 15:274801101
2,4,5-Trichlorophenol ND ug/kg 04/17/20 12:32 95-95-404/16/20 15:274801251
2,4,6-Trichlorophenol ND ug/kg 04/17/20 12:32 88-06-204/16/20 15:274801211
Surrogates
Nitrobenzene-d5 (S)66 %04/17/20 12:32 4165-60-004/16/20 15:2723-110 1
2-Fluorobiphenyl (S)60 %04/17/20 12:32 321-60-804/16/20 15:2730-110 1
Terphenyl-d14 (S)83 %04/17/20 12:32 1718-51-004/16/20 15:2728-110 1
Phenol-d6 (S)63 %04/17/20 12:32 13127-88-304/16/20 15:2722-110 1
2-Fluorophenol (S)64 %04/17/20 12:32 367-12-404/16/20 15:2713-110 1
2,4,6-Tribromophenol (S)67 %04/17/20 12:32 118-79-604/16/20 15:2727-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone 70.0J ug/kg 04/17/20 12:54 67-64-104/17/20 10:1411010.4 1
Benzene ND ug/kg 04/17/20 12:54 71-43-204/17/20 10:145.5 0.99 1
Bromobenzene ND ug/kg 04/17/20 12:54 108-86-104/17/20 10:145.5 1.5 1
Bromochloromethane ND ug/kg 04/17/20 12:54 74-97-504/17/20 10:145.5 1.4 1
Bromodichloromethane ND ug/kg 04/17/20 12:54 75-27-404/17/20 10:145.5 1.1 1
Bromoform ND ug/kg 04/17/20 12:54 75-25-204/17/20 10:145.5 2.7 1
Bromomethane ND ug/kg 04/17/20 12:54 74-83-9 IH04/17/20 10:1411.0 2.6 1
2-Butanone (MEK)ND ug/kg 04/17/20 12:54 78-93-304/17/20 10:1411013.1 1
n-Butylbenzene ND ug/kg 04/17/20 12:54 104-51-804/17/20 10:145.5 3.1 1
sec-Butylbenzene ND ug/kg 04/17/20 12:54 135-98-804/17/20 10:145.5 2.3 1
tert-Butylbenzene ND ug/kg 04/17/20 12:54 98-06-604/17/20 10:145.5 1.9 1
Carbon tetrachloride ND ug/kg 04/17/20 12:54 56-23-504/17/20 10:145.5 1.1 1
Chlorobenzene ND ug/kg 04/17/20 12:54 108-90-704/17/20 10:145.5 1.1 1
Chloroethane ND ug/kg 04/17/20 12:54 75-00-304/17/20 10:1411.0 2.3 1
Chloroform ND ug/kg 04/17/20 12:54 67-66-304/17/20 10:145.5 1.2 1
Chloromethane ND ug/kg 04/17/20 12:54 74-87-304/17/20 10:1411.0 3.6 1
2-Chlorotoluene ND ug/kg 04/17/20 12:54 95-49-804/17/20 10:145.5 1.7 1
4-Chlorotoluene ND ug/kg 04/17/20 12:54 106-43-404/17/20 10:145.5 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/17/20 12:54 96-12-804/17/20 10:145.5 2.8 1
Dibromochloromethane ND ug/kg 04/17/20 12:54 124-48-104/17/20 10:145.5 2.8 1
1,2-Dibromoethane (EDB)ND ug/kg 04/17/20 12:54 106-93-404/17/20 10:145.5 1.2 1
Dibromomethane ND ug/kg 04/17/20 12:54 74-95-304/17/20 10:145.5 1.6 1
1,2-Dichlorobenzene ND ug/kg 04/17/20 12:54 95-50-104/17/20 10:145.5 1.9 1
1,3-Dichlorobenzene ND ug/kg 04/17/20 12:54 541-73-104/17/20 10:145.5 2.0 1
1,4-Dichlorobenzene ND ug/kg 04/17/20 12:54 106-46-704/17/20 10:145.5 1.9 1
Dichlorodifluoromethane ND ug/kg 04/17/20 12:54 75-71-804/17/20 10:1411.0 4.5 1
1,1-Dichloroethane ND ug/kg 04/17/20 12:54 75-34-304/17/20 10:145.5 0.81 1
1,2-Dichloroethane ND ug/kg 04/17/20 12:54 107-06-204/17/20 10:145.5 1.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:S WALL Lab ID:92473782003 Collected:04/14/20 09:40 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 04/17/20 12:54 75-35-404/17/20 10:145.5 1.3 1
cis-1,2-Dichloroethene ND ug/kg 04/17/20 12:54 156-59-204/17/20 10:145.5 0.96 1
trans-1,2-Dichloroethene ND ug/kg 04/17/20 12:54 156-60-504/17/20 10:145.5 1.1 1
1,2-Dichloropropane ND ug/kg 04/17/20 12:54 78-87-504/17/20 10:145.5 2.1 1
1,3-Dichloropropane ND ug/kg 04/17/20 12:54 142-28-904/17/20 10:145.5 2.1 1
2,2-Dichloropropane ND ug/kg 04/17/20 12:54 594-20-704/17/20 10:145.5 0.54 1
1,1-Dichloropropene ND ug/kg 04/17/20 12:54 563-58-604/17/20 10:145.5 2.3 1
cis-1,3-Dichloropropene ND ug/kg 04/17/20 12:54 10061-01-504/17/20 10:145.5 2.5 1
trans-1,3-Dichloropropene ND ug/kg 04/17/20 12:54 10061-02-604/17/20 10:145.5 0.96 1
Diisopropyl ether ND ug/kg 04/17/20 12:54 108-20-304/17/20 10:145.5 3.2 1
Ethylbenzene ND ug/kg 04/17/20 12:54 100-41-404/17/20 10:145.5 1.2 1
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 12:54 87-68-304/17/20 10:145.5 2.7 1
2-Hexanone ND ug/kg 04/17/20 12:54 591-78-604/17/20 10:1455.1 5.7 1
Isopropylbenzene (Cumene)ND ug/kg 04/17/20 12:54 98-82-804/17/20 10:145.5 1.6 1
p-Isopropyltoluene ND ug/kg 04/17/20 12:54 99-87-604/17/20 10:145.5 2.7 1
Methylene Chloride ND ug/kg 04/17/20 12:54 75-09-204/17/20 10:1422.1 6.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/17/20 12:54 108-10-104/17/20 10:1455.1 4.1 1
Methyl-tert-butyl ether ND ug/kg 04/17/20 12:54 1634-04-404/17/20 10:145.5 3.2 1
Naphthalene ND ug/kg 04/17/20 12:54 91-20-304/17/20 10:145.5 4.7 1
n-Propylbenzene ND ug/kg 04/17/20 12:54 103-65-104/17/20 10:145.5 1.8 1
Styrene ND ug/kg 04/17/20 12:54 100-42-504/17/20 10:145.5 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/17/20 12:54 630-20-604/17/20 10:145.5 1.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/17/20 12:54 79-34-504/17/20 10:145.5 1.9 1
Tetrachloroethene ND ug/kg 04/17/20 12:54 127-18-404/17/20 10:145.5 1.7 1
Toluene ND ug/kg 04/17/20 12:54 108-88-304/17/20 10:145.5 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 04/17/20 12:54 87-61-604/17/20 10:145.5 3.9 1
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 12:54 120-82-104/17/20 10:145.5 2.9 1
1,1,1-Trichloroethane ND ug/kg 04/17/20 12:54 71-55-604/17/20 10:145.5 0.96 1
1,1,2-Trichloroethane ND ug/kg 04/17/20 12:54 79-00-504/17/20 10:145.5 1.2 1
Trichloroethene ND ug/kg 04/17/20 12:54 79-01-604/17/20 10:145.5 1.4 1
Trichlorofluoromethane ND ug/kg 04/17/20 12:54 75-69-404/17/20 10:145.5 1.3 1
1,2,3-Trichloropropane ND ug/kg 04/17/20 12:54 96-18-404/17/20 10:145.5 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 04/17/20 12:54 95-63-604/17/20 10:145.5 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 04/17/20 12:54 108-67-804/17/20 10:145.5 1.8 1
Vinyl acetate ND ug/kg 04/17/20 12:54 108-05-404/17/20 10:1455.1 18.0 1
Vinyl chloride ND ug/kg 04/17/20 12:54 75-01-404/17/20 10:1411.0 2.1 1
Xylene (Total)ND ug/kg 04/17/20 12:54 1330-20-704/17/20 10:1411.0 3.9 1
m&p-Xylene ND ug/kg 04/17/20 12:54 179601-23-104/17/20 10:1411.0 2.6 1
o-Xylene ND ug/kg 04/17/20 12:54 95-47-604/17/20 10:145.5 1.3 1
Surrogates
Toluene-d8 (S)101 %04/17/20 12:54 2037-26-504/17/20 10:1470-130 1
4-Bromofluorobenzene (S)94 %04/17/20 12:54 460-00-404/17/20 10:1470-130 1
1,2-Dichloroethane-d4 (S)98 %04/17/20 12:54 17060-07-004/17/20 10:1470-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:S WALL Lab ID:92473782003 Collected:04/14/20 09:40 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 31.0 %04/16/20 14:410.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 61.5 %04/28/20 11:3504/28/20 11:261
Total Solids 69.5 %04/20/20 07:5504/20/20 07:491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:N WALL Lab ID:92473782004 Collected:04/14/20 09:50 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/17/20 10:59 N204/16/20 09:1814.5 14.5 1
Aliphatic (C19-C36)ND mg/kg 04/17/20 10:59 N204/16/20 09:1814.5 14.5 1
Aromatic (C11-C22)ND mg/kg 04/17/20 10:59 N204/16/20 09:1814.5 14.5 1
Surrogates
Nonatriacontane (S)60 %04/17/20 10:59 7194-86-704/16/20 09:1840-140 1
o-Terphenyl (S)65 %04/17/20 10:59 84-15-104/16/20 09:1840-140 1
2-Fluorobiphenyl (S)94 %04/17/20 10:59 321-60-804/16/20 09:1840-140 1
2-Bromonaphthalene (S)96 %04/17/20 10:59 580-13-204/16/20 09:1840-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND mg/kg 04/18/20 14:4004/14/20 09:507.63 2.53 1.06
Aliphatic (C09-C12)ND mg/kg 04/18/20 14:4004/14/20 09:507.63 2.53 1.06
Aromatic (C09-C10),Unadjusted 2.58J mg/kg 04/18/20 14:40 TPHC9C10A J04/14/20 09:507.63 2.53 1.06
Surrogates
2,5-Dibromotoluene (FID)101 %04/18/20 14:40 615-59-8FID04/14/20 09:5070.0-130 1.06
2,5-Dibromotoluene (PID)105 %04/18/20 14:40 615-59-8PID04/14/20 09:5070.0-130 1.06
Analytical Method: EPA 6010D Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICP) 6010D
Chromium 37.5 mg/kg 04/25/20 13:50 7440-47-304/24/20 22:491.59 0.797 1
Lead ND mg/kg 04/25/20 13:50 7439-92-104/24/20 22:490.797 0.399 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/17/20 13:00 83-32-904/16/20 15:274751221
Acenaphthylene ND ug/kg 04/17/20 13:00 208-96-804/16/20 15:274751121
Aniline ND ug/kg 04/17/20 13:00 62-53-304/16/20 15:274751071
Anthracene ND ug/kg 04/17/20 13:00 120-12-704/16/20 15:274751231
Benzo(a)anthracene ND ug/kg 04/17/20 13:00 56-55-304/16/20 15:274751511
Benzo(a)pyrene ND ug/kg 04/17/20 13:00 50-32-804/16/20 15:274752061
Benzo(b)fluoranthene ND ug/kg 04/17/20 13:00 205-99-204/16/20 15:274751911
Benzo(g,h,i)perylene ND ug/kg 04/17/20 13:00 191-24-204/16/20 15:274751861
Benzo(k)fluoranthene ND ug/kg 04/17/20 13:00 207-08-904/16/20 15:274752001
Benzoic Acid ND ug/kg 04/17/20 13:00 65-85-004/16/20 15:2723805131
Benzyl alcohol ND ug/kg 04/17/20 13:00 100-51-604/16/20 15:279502521
4-Bromophenylphenyl ether ND ug/kg 04/17/20 13:00 101-55-304/16/20 15:274751251
Butylbenzylphthalate ND ug/kg 04/17/20 13:00 85-68-704/16/20 15:274751271
4-Chloro-3-methylphenol ND ug/kg 04/17/20 13:00 59-50-704/16/20 15:279502891
4-Chloroaniline ND ug/kg 04/17/20 13:00 106-47-804/16/20 15:279502911
bis(2-Chloroethoxy)methane ND ug/kg 04/17/20 13:00 111-91-104/16/20 15:274751271
bis(2-Chloroethyl) ether ND ug/kg 04/17/20 13:00 111-44-404/16/20 15:274751011
2-Chloronaphthalene ND ug/kg 04/17/20 13:00 91-58-704/16/20 15:274751061
2-Chlorophenol ND ug/kg 04/17/20 13:00 95-57-804/16/20 15:274751111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:N WALL Lab ID:92473782004 Collected:04/14/20 09:50 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
4-Chlorophenylphenyl ether ND ug/kg 04/17/20 13:00 7005-72-304/16/20 15:274751231
Chrysene ND ug/kg 04/17/20 13:00 218-01-904/16/20 15:274751381
Dibenz(a,h)anthracene ND ug/kg 04/17/20 13:00 53-70-304/16/20 15:274751901
Dibenzofuran ND ug/kg 04/17/20 13:00 132-64-904/16/20 15:274751191
1,2-Dichlorobenzene ND ug/kg 04/17/20 13:00 95-50-104/16/20 15:274751031
1,3-Dichlorobenzene ND ug/kg 04/17/20 13:00 541-73-104/16/20 15:274751071
1,4-Dichlorobenzene ND ug/kg 04/17/20 13:00 106-46-704/16/20 15:274751051
3,3'-Dichlorobenzidine ND ug/kg 04/17/20 13:00 91-94-104/16/20 15:279503311
2,4-Dichlorophenol ND ug/kg 04/17/20 13:00 120-83-204/16/20 15:274751571
Diethylphthalate ND ug/kg 04/17/20 13:00 84-66-204/16/20 15:274751031
2,4-Dimethylphenol ND ug/kg 04/17/20 13:00 105-67-904/16/20 15:274751181
Dimethylphthalate ND ug/kg 04/17/20 13:00 131-11-304/16/20 15:274751071
Di-n-butylphthalate ND ug/kg 04/17/20 13:00 84-74-204/16/20 15:274751171
4,6-Dinitro-2-methylphenol ND ug/kg 04/17/20 13:00 534-52-104/16/20 15:279507661
2,4-Dinitrophenol ND ug/kg 04/17/20 13:00 51-28-504/16/20 15:27238015201
2,4-Dinitrotoluene ND ug/kg 04/17/20 13:00 121-14-204/16/20 15:274751261
2,6-Dinitrotoluene ND ug/kg 04/17/20 13:00 606-20-204/16/20 15:274751241
Di-n-octylphthalate ND ug/kg 04/17/20 13:00 117-84-004/16/20 15:274752711
bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/20 13:00 117-81-704/16/20 15:274751551
Fluoranthene ND ug/kg 04/17/20 13:00 206-44-004/16/20 15:274751441
Fluorene ND ug/kg 04/17/20 13:00 86-73-704/16/20 15:274751271
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 13:00 87-68-304/16/20 15:274751151
Hexachlorobenzene ND ug/kg 04/17/20 13:00 118-74-104/16/20 15:274751211
Hexachlorocyclopentadiene ND ug/kg 04/17/20 13:00 77-47-404/16/20 15:274751901
Hexachloroethane ND ug/kg 04/17/20 13:00 67-72-104/16/20 15:274751081
Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/20 13:00 193-39-504/16/20 15:274752171
Isophorone ND ug/kg 04/17/20 13:00 78-59-104/16/20 15:274751031
1-Methylnaphthalene ND ug/kg 04/17/20 13:00 90-12-004/16/20 15:274751271
2-Methylnaphthalene ND ug/kg 04/17/20 13:00 91-57-604/16/20 15:274751211
2-Methylphenol(o-Cresol)ND ug/kg 04/17/20 13:00 95-48-704/16/20 15:274751051
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/20 13:00 15831-10-404/16/20 15:274751191
Naphthalene ND ug/kg 04/17/20 13:00 91-20-304/16/20 15:274751141
2-Nitroaniline ND ug/kg 04/17/20 13:00 88-74-404/16/20 15:2723802391
3-Nitroaniline ND ug/kg 04/17/20 13:00 99-09-204/16/20 15:2723802521
4-Nitroaniline ND ug/kg 04/17/20 13:00 100-01-604/16/20 15:279502351
Nitrobenzene ND ug/kg 04/17/20 13:00 98-95-304/16/20 15:274751131
2-Nitrophenol ND ug/kg 04/17/20 13:00 88-75-504/16/20 15:274751471
4-Nitrophenol ND ug/kg 04/17/20 13:00 100-02-704/16/20 15:2723807571
N-Nitrosodimethylamine ND ug/kg 04/17/20 13:00 62-75-904/16/20 15:274751341
N-Nitroso-di-n-propylamine ND ug/kg 04/17/20 13:00 621-64-704/16/20 15:274751331
N-Nitrosodiphenylamine ND ug/kg 04/17/20 13:00 86-30-604/16/20 15:274751211
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/20 13:00 108-60-104/16/20 15:274751321
Pentachlorophenol ND ug/kg 04/17/20 13:00 87-86-504/16/20 15:279502171
Phenanthrene ND ug/kg 04/17/20 13:00 85-01-804/16/20 15:274751201
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:N WALL Lab ID:92473782004 Collected:04/14/20 09:50 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Phenol ND ug/kg 04/17/20 13:00 108-95-204/16/20 15:274751131
Pyrene ND ug/kg 04/17/20 13:00 129-00-004/16/20 15:274751311
Pyridine ND ug/kg 04/17/20 13:00 110-86-104/16/20 15:274751201
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 13:00 120-82-104/16/20 15:274751091
2,4,5-Trichlorophenol ND ug/kg 04/17/20 13:00 95-95-404/16/20 15:274751231
2,4,6-Trichlorophenol ND ug/kg 04/17/20 13:00 88-06-204/16/20 15:274751191
Surrogates
Nitrobenzene-d5 (S)61 %04/17/20 13:00 4165-60-004/16/20 15:2723-110 1
2-Fluorobiphenyl (S)52 %04/17/20 13:00 321-60-804/16/20 15:2730-110 1
Terphenyl-d14 (S)67 %04/17/20 13:00 1718-51-004/16/20 15:2728-110 1
Phenol-d6 (S)61 %04/17/20 13:00 13127-88-304/16/20 15:2722-110 1
2-Fluorophenol (S)60 %04/17/20 13:00 367-12-404/16/20 15:2713-110 1
2,4,6-Tribromophenol (S)61 %04/17/20 13:00 118-79-604/16/20 15:2727-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone 63.4J ug/kg 04/17/20 13:19 67-64-104/17/20 10:1411110.5 1
Benzene ND ug/kg 04/17/20 13:19 71-43-204/17/20 10:145.6 1.0 1
Bromobenzene ND ug/kg 04/17/20 13:19 108-86-104/17/20 10:145.6 1.5 1
Bromochloromethane ND ug/kg 04/17/20 13:19 74-97-504/17/20 10:145.6 1.4 1
Bromodichloromethane ND ug/kg 04/17/20 13:19 75-27-404/17/20 10:145.6 1.1 1
Bromoform ND ug/kg 04/17/20 13:19 75-25-204/17/20 10:145.6 2.7 1
Bromomethane ND ug/kg 04/17/20 13:19 74-83-9 IH04/17/20 10:1411.1 2.6 1
2-Butanone (MEK)ND ug/kg 04/17/20 13:19 78-93-304/17/20 10:1411113.3 1
n-Butylbenzene ND ug/kg 04/17/20 13:19 104-51-804/17/20 10:145.6 3.1 1
sec-Butylbenzene ND ug/kg 04/17/20 13:19 135-98-804/17/20 10:145.6 2.4 1
tert-Butylbenzene ND ug/kg 04/17/20 13:19 98-06-604/17/20 10:145.6 1.9 1
Carbon tetrachloride ND ug/kg 04/17/20 13:19 56-23-504/17/20 10:145.6 1.1 1
Chlorobenzene ND ug/kg 04/17/20 13:19 108-90-704/17/20 10:145.6 1.1 1
Chloroethane ND ug/kg 04/17/20 13:19 75-00-304/17/20 10:1411.1 2.3 1
Chloroform ND ug/kg 04/17/20 13:19 67-66-304/17/20 10:145.6 1.2 1
Chloromethane ND ug/kg 04/17/20 13:19 74-87-304/17/20 10:1411.1 3.7 1
2-Chlorotoluene ND ug/kg 04/17/20 13:19 95-49-804/17/20 10:145.6 1.7 1
4-Chlorotoluene ND ug/kg 04/17/20 13:19 106-43-404/17/20 10:145.6 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/17/20 13:19 96-12-804/17/20 10:145.6 2.8 1
Dibromochloromethane ND ug/kg 04/17/20 13:19 124-48-104/17/20 10:145.6 2.8 1
1,2-Dibromoethane (EDB)ND ug/kg 04/17/20 13:19 106-93-404/17/20 10:145.6 1.2 1
Dibromomethane ND ug/kg 04/17/20 13:19 74-95-304/17/20 10:145.6 1.7 1
1,2-Dichlorobenzene ND ug/kg 04/17/20 13:19 95-50-104/17/20 10:145.6 2.0 1
1,3-Dichlorobenzene ND ug/kg 04/17/20 13:19 541-73-104/17/20 10:145.6 2.0 1
1,4-Dichlorobenzene ND ug/kg 04/17/20 13:19 106-46-704/17/20 10:145.6 1.9 1
Dichlorodifluoromethane ND ug/kg 04/17/20 13:19 75-71-804/17/20 10:1411.1 4.6 1
1,1-Dichloroethane ND ug/kg 04/17/20 13:19 75-34-304/17/20 10:145.6 0.82 1
1,2-Dichloroethane ND ug/kg 04/17/20 13:19 107-06-204/17/20 10:145.6 1.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:N WALL Lab ID:92473782004 Collected:04/14/20 09:50 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 04/17/20 13:19 75-35-404/17/20 10:145.6 1.3 1
cis-1,2-Dichloroethene ND ug/kg 04/17/20 13:19 156-59-204/17/20 10:145.6 0.97 1
trans-1,2-Dichloroethene ND ug/kg 04/17/20 13:19 156-60-504/17/20 10:145.6 1.1 1
1,2-Dichloropropane ND ug/kg 04/17/20 13:19 78-87-504/17/20 10:145.6 2.1 1
1,3-Dichloropropane ND ug/kg 04/17/20 13:19 142-28-904/17/20 10:145.6 2.1 1
2,2-Dichloropropane ND ug/kg 04/17/20 13:19 594-20-704/17/20 10:145.6 0.55 1
1,1-Dichloropropene ND ug/kg 04/17/20 13:19 563-58-604/17/20 10:145.6 2.4 1
cis-1,3-Dichloropropene ND ug/kg 04/17/20 13:19 10061-01-504/17/20 10:145.6 2.5 1
trans-1,3-Dichloropropene ND ug/kg 04/17/20 13:19 10061-02-604/17/20 10:145.6 0.98 1
Diisopropyl ether ND ug/kg 04/17/20 13:19 108-20-304/17/20 10:145.6 3.2 1
Ethylbenzene ND ug/kg 04/17/20 13:19 100-41-404/17/20 10:145.6 1.2 1
Hexachloro-1,3-butadiene ND ug/kg 04/17/20 13:19 87-68-304/17/20 10:145.6 2.8 1
2-Hexanone ND ug/kg 04/17/20 13:19 591-78-604/17/20 10:1455.7 5.8 1
Isopropylbenzene (Cumene)ND ug/kg 04/17/20 13:19 98-82-804/17/20 10:145.6 1.6 1
p-Isopropyltoluene ND ug/kg 04/17/20 13:19 99-87-604/17/20 10:145.6 2.7 1
Methylene Chloride ND ug/kg 04/17/20 13:19 75-09-204/17/20 10:1422.3 6.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/17/20 13:19 108-10-104/17/20 10:1455.7 4.2 1
Methyl-tert-butyl ether ND ug/kg 04/17/20 13:19 1634-04-404/17/20 10:145.6 3.2 1
Naphthalene ND ug/kg 04/17/20 13:19 91-20-304/17/20 10:145.6 4.7 1
n-Propylbenzene ND ug/kg 04/17/20 13:19 103-65-104/17/20 10:145.6 1.9 1
Styrene ND ug/kg 04/17/20 13:19 100-42-504/17/20 10:145.6 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/17/20 13:19 630-20-604/17/20 10:145.6 1.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/17/20 13:19 79-34-504/17/20 10:145.6 1.9 1
Tetrachloroethene ND ug/kg 04/17/20 13:19 127-18-404/17/20 10:145.6 1.8 1
Toluene ND ug/kg 04/17/20 13:19 108-88-304/17/20 10:145.6 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 04/17/20 13:19 87-61-604/17/20 10:145.6 4.0 1
1,2,4-Trichlorobenzene ND ug/kg 04/17/20 13:19 120-82-104/17/20 10:145.6 3.0 1
1,1,1-Trichloroethane ND ug/kg 04/17/20 13:19 71-55-604/17/20 10:145.6 0.97 1
1,1,2-Trichloroethane ND ug/kg 04/17/20 13:19 79-00-504/17/20 10:145.6 1.3 1
Trichloroethene ND ug/kg 04/17/20 13:19 79-01-604/17/20 10:145.6 1.4 1
Trichlorofluoromethane ND ug/kg 04/17/20 13:19 75-69-404/17/20 10:145.6 1.3 1
1,2,3-Trichloropropane ND ug/kg 04/17/20 13:19 96-18-404/17/20 10:145.6 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 04/17/20 13:19 95-63-604/17/20 10:145.6 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 04/17/20 13:19 108-67-804/17/20 10:145.6 1.9 1
Vinyl acetate ND ug/kg 04/17/20 13:19 108-05-404/17/20 10:1455.7 18.2 1
Vinyl chloride ND ug/kg 04/17/20 13:19 75-01-404/17/20 10:1411.1 2.1 1
Xylene (Total)ND ug/kg 04/17/20 13:19 1330-20-704/17/20 10:1411.1 3.9 1
m&p-Xylene ND ug/kg 04/17/20 13:19 179601-23-104/17/20 10:1411.1 2.6 1
o-Xylene ND ug/kg 04/17/20 13:19 95-47-604/17/20 10:145.6 1.3 1
Surrogates
Toluene-d8 (S)103 %04/17/20 13:19 2037-26-504/17/20 10:1470-130 1
4-Bromofluorobenzene (S)94 %04/17/20 13:19 460-00-404/17/20 10:1470-130 1
1,2-Dichloroethane-d4 (S)100 %04/17/20 13:19 17060-07-004/17/20 10:1470-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Sample:N WALL Lab ID:92473782004 Collected:04/14/20 09:50 Received:04/15/20 10:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 31.0 %04/16/20 14:410.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 62.7 %04/28/20 11:3504/28/20 11:261
Total Solids 69.5 %04/20/20 07:5504/20/20 07:491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1462690
MADEPV
MADEP VPH
MADEPV
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3519880-3
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
Aliphatic (C05-C08)mg/kg ND 5.00 04/18/20 12:291.67
Aliphatic (C09-C12)mg/kg ND 5.00 04/18/20 12:291.67
Aromatic (C09-C10),Unadjusted mg/kg ND 5.00 04/18/20 12:291.67
2,5-Dibromotoluene (FID)%93.4 70.0-130 04/18/20 12:29
2,5-Dibromotoluene (PID)%96.3 70.0-130 04/18/20 12:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3519880-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3519880-2
Aliphatic (C05-C08)mg/kg 63.960.0 107 70.0-13010563.3 0.943 25
Aliphatic (C09-C12)mg/kg 78.970.0 113 70.0-13011278.3 0.763 25
Aromatic (C09-C10),Unadjusted mg/kg 11.610.0 116 70.0-13011511.5 0.866 25
2,5-Dibromotoluene (FID)%102 70.0-130104
2,5-Dibromotoluene (PID)%106 70.0-130108
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3519880-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92473782001
R3519880-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aliphatic (C05-C08)mg/kg 51.9 85.7 70.0-130102 17.5 2551.9ND 44.5 53.0
Aliphatic (C09-C12)mg/kg 60.6 95.5 70.0-130112 15.3 2560.63.68 61.5 71.7
Aromatic (C09-
C10),Unadjusted mg/kg MH8.65 121 70.0-130136 11.6 258.65ND 10.5 11.8
2,5-Dibromotoluene (FID)%104 70.0-130101
2,5-Dibromotoluene (PID)%108 70.0-130104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1466045
3050B
EPA 6010D
Metals (ICP) 6010D
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3521852-1
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
Chromium mg/kg ND 1.00 04/25/20 13:190.500
Lead mg/kg ND 0.500 04/25/20 13:190.250
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3521852-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium mg/kg 98.6100 98.6 80.0-120
Lead mg/kg 102100 102 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3521852-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1211713-02
R3521852-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium mg/kg ML10084.8 75.0-12565.9 19.8 2010019.7 104 85.6
Lead mg/kg ML,R110093.0 75.0-12573.7 21.0 201008.59 102 82.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
536822
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2863265
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/17/20 10:301.2
1,1,1-Trichloroethane ug/kg ND 5.0 04/17/20 10:300.87
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/17/20 10:301.7
1,1,2-Trichloroethane ug/kg ND 5.0 04/17/20 10:301.1
1,1-Dichloroethane ug/kg ND 5.0 04/17/20 10:300.74
1,1-Dichloroethene ug/kg ND 5.0 04/17/20 10:301.2
1,1-Dichloropropene ug/kg ND 5.0 04/17/20 10:302.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 04/17/20 10:303.6
1,2,3-Trichloropropane ug/kg ND 5.0 04/17/20 10:301.7
1,2,4-Trichlorobenzene ug/kg ND 5.0 04/17/20 10:302.6
1,2,4-Trimethylbenzene ug/kg ND 5.0 04/17/20 10:302.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/17/20 10:302.5
1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/17/20 10:301.1
1,2-Dichlorobenzene ug/kg ND 5.0 04/17/20 10:301.8
1,2-Dichloroethane ug/kg ND 5.0 04/17/20 10:301.0
1,2-Dichloropropane ug/kg ND 5.0 04/17/20 10:301.9
1,3,5-Trimethylbenzene ug/kg ND 5.0 04/17/20 10:301.7
1,3-Dichlorobenzene ug/kg ND 5.0 04/17/20 10:301.8
1,3-Dichloropropane ug/kg ND 5.0 04/17/20 10:301.9
1,4-Dichlorobenzene ug/kg ND 5.0 04/17/20 10:301.7
2,2-Dichloropropane ug/kg ND 5.0 04/17/20 10:300.49
2-Butanone (MEK)ug/kg ND 100 04/17/20 10:3011.9
2-Chlorotoluene ug/kg ND 5.0 04/17/20 10:301.5
2-Hexanone ug/kg ND 50.0 04/17/20 10:305.2
4-Chlorotoluene ug/kg ND 5.0 04/17/20 10:301.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/17/20 10:303.7
Acetone ug/kg ND 100 04/17/20 10:309.4
Benzene ug/kg ND 5.0 04/17/20 10:300.90
Bromobenzene ug/kg ND 5.0 04/17/20 10:301.4
Bromochloromethane ug/kg ND 5.0 04/17/20 10:301.2
Bromodichloromethane ug/kg ND 5.0 04/17/20 10:300.98
Bromoform ug/kg ND 5.0 04/17/20 10:302.4
Bromomethane ug/kg ND 10.0 IH04/17/20 10:302.4
Carbon tetrachloride ug/kg ND 5.0 04/17/20 10:300.96
Chlorobenzene ug/kg ND 5.0 04/17/20 10:300.97
Chloroethane ug/kg ND 10.0 04/17/20 10:302.1
Chloroform ug/kg ND 5.0 04/17/20 10:301.1
Chloromethane ug/kg ND 10.0 04/17/20 10:303.3
cis-1,2-Dichloroethene ug/kg ND 5.0 04/17/20 10:300.87
cis-1,3-Dichloropropene ug/kg ND 5.0 04/17/20 10:302.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2863265
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 04/17/20 10:302.5
Dibromomethane ug/kg ND 5.0 04/17/20 10:301.5
Dichlorodifluoromethane ug/kg ND 10.0 04/17/20 10:304.1
Diisopropyl ether ug/kg ND 5.0 04/17/20 10:302.9
Ethylbenzene ug/kg ND 5.0 04/17/20 10:301.1
Hexachloro-1,3-butadiene ug/kg ND 5.0 04/17/20 10:302.5
Isopropylbenzene (Cumene)ug/kg ND 5.0 04/17/20 10:301.4
m&p-Xylene ug/kg ND 10.0 04/17/20 10:302.4
Methyl-tert-butyl ether ug/kg ND 5.0 04/17/20 10:302.9
Methylene Chloride ug/kg ND 20.0 04/17/20 10:305.9
n-Butylbenzene ug/kg ND 5.0 04/17/20 10:302.8
n-Propylbenzene ug/kg ND 5.0 04/17/20 10:301.7
Naphthalene ug/kg ND 5.0 04/17/20 10:304.2
o-Xylene ug/kg ND 5.0 04/17/20 10:301.2
p-Isopropyltoluene ug/kg ND 5.0 04/17/20 10:302.4
sec-Butylbenzene ug/kg ND 5.0 04/17/20 10:302.1
Styrene ug/kg ND 5.0 04/17/20 10:301.5
tert-Butylbenzene ug/kg ND 5.0 04/17/20 10:301.7
Tetrachloroethene ug/kg ND 5.0 04/17/20 10:301.6
Toluene ug/kg ND 5.0 04/17/20 10:301.6
trans-1,2-Dichloroethene ug/kg ND 5.0 04/17/20 10:300.98
trans-1,3-Dichloropropene ug/kg ND 5.0 04/17/20 10:300.88
Trichloroethene ug/kg ND 5.0 04/17/20 10:301.3
Trichlorofluoromethane ug/kg ND 5.0 04/17/20 10:301.2
Vinyl acetate ug/kg ND 50.0 04/17/20 10:3016.3
Vinyl chloride ug/kg ND 10.0 04/17/20 10:301.9
Xylene (Total)ug/kg ND 10.0 04/17/20 10:303.5
1,2-Dichloroethane-d4 (S)%96 70-132 04/17/20 10:30
4-Bromofluorobenzene (S)%93 70-130 04/17/20 10:30
Toluene-d8 (S)%101 70-130 04/17/20 10:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2863266LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 51.050 102 70-130
1,1,1-Trichloroethane ug/kg 46.450 93 70-130
1,1,2,2-Tetrachloroethane ug/kg 47.550 95 55-130
1,1,2-Trichloroethane ug/kg 51.550 103 70-130
1,1-Dichloroethane ug/kg 47.350 95 68-130
1,1-Dichloroethene ug/kg 49.850 100 70-130
1,1-Dichloropropene ug/kg 47.450 95 70-130
1,2,3-Trichlorobenzene ug/kg 56.950 114 70-130
1,2,3-Trichloropropane ug/kg 49.550 99 70-130
1,2,4-Trichlorobenzene ug/kg 55.750 111 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2863266LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 49.150 98 69-130
1,2-Dibromo-3-chloropropane ug/kg 66.350 133 57-141
1,2-Dibromoethane (EDB)ug/kg 50.550 101 70-130
1,2-Dichlorobenzene ug/kg 51.450 103 70-130
1,2-Dichloroethane ug/kg 48.350 97 70-130
1,2-Dichloropropane ug/kg 52.550 105 70-130
1,3,5-Trimethylbenzene ug/kg 48.750 97 70-130
1,3-Dichlorobenzene ug/kg 50.250 100 70-130
1,3-Dichloropropane ug/kg 47.150 94 70-130
1,4-Dichlorobenzene ug/kg 50.150 100 70-130
2,2-Dichloropropane ug/kg 45.550 91 70-130
2-Butanone (MEK)ug/kg 126100 126 60-130
2-Chlorotoluene ug/kg 49.550 99 70-130
2-Hexanone ug/kg 118100 118 70-132
4-Chlorotoluene ug/kg 48.550 97 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 116100 116 69-130
Acetone ug/kg 129100 129 49-148
Benzene ug/kg 49.250 98 70-130
Bromobenzene ug/kg 55.350 111 70-130
Bromochloromethane ug/kg 51.550 103 70-130
Bromodichloromethane ug/kg 50.650 101 70-130
Bromoform ug/kg 52.350 105 68-136
Bromomethane ug/kg 69.4 IH5013960-140
Carbon tetrachloride ug/kg 54.550 109 70-130
Chlorobenzene ug/kg 47.650 95 70-130
Chloroethane ug/kg 54.450 109 51-147
Chloroform ug/kg 46.750 93 70-130
Chloromethane ug/kg 44.150 88 48-130
cis-1,2-Dichloroethene ug/kg 48.350 97 70-130
cis-1,3-Dichloropropene ug/kg 48.950 98 70-130
Dibromochloromethane ug/kg 52.450 105 70-130
Dibromomethane ug/kg 51.650 103 70-130
Dichlorodifluoromethane ug/kg 44.850 90 49-130
Diisopropyl ether ug/kg 48.250 96 66-130
Ethylbenzene ug/kg 45.050 90 70-130
Hexachloro-1,3-butadiene ug/kg 53.850 108 70-130
Isopropylbenzene (Cumene)ug/kg 46.250 92 70-130
m&p-Xylene ug/kg 91.1100 91 70-130
Methyl-tert-butyl ether ug/kg 46.950 94 70-130
Methylene Chloride ug/kg 50.450 101 50-137
n-Butylbenzene ug/kg 48.750 97 70-130
n-Propylbenzene ug/kg 47.250 94 70-130
Naphthalene ug/kg 58.650 117 70-131
o-Xylene ug/kg 45.750 91 70-130
p-Isopropyltoluene ug/kg 51.050 102 70-130
sec-Butylbenzene ug/kg 48.150 96 70-130
Styrene ug/kg 47.550 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2863266LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 44.450 89 69-130
Tetrachloroethene ug/kg 44.750 89 56-130
Toluene ug/kg 47.050 94 70-130
trans-1,2-Dichloroethene ug/kg 49.550 99 70-130
trans-1,3-Dichloropropene ug/kg 49.650 99 70-130
Trichloroethene ug/kg 54.550 109 70-141
Trichlorofluoromethane ug/kg 48.250 96 67-130
Vinyl acetate ug/kg 108100 108 10-136
Vinyl chloride ug/kg 51.950 104 67-130
Xylene (Total)ug/kg 137150 91 70-130
1,2-Dichloroethane-d4 (S)%99 70-132
4-Bromofluorobenzene (S)%91 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2863268MATRIX SPIKE SAMPLE:
MSSpike
Result
92473782002
1,1,1,2-Tetrachloroethane ug/kg 18.622 85 52-133ND
1,1,1-Trichloroethane ug/kg 20.222 92 49-137ND
1,1,2,2-Tetrachloroethane ug/kg 16.622 76 39-150ND
1,1,2-Trichloroethane ug/kg 18.022 82 48-140ND
1,1-Dichloroethane ug/kg 19.622 89 46-135ND
1,1-Dichloroethene ug/kg 22.222 102 38-149ND
1,1-Dichloropropene ug/kg 19.822 90 41-140ND
1,2,3-Trichlorobenzene ug/kg 17.622 80 10-158ND
1,2,3-Trichloropropane ug/kg 15.722 72 33-157ND
1,2,4-Trichlorobenzene ug/kg 17.322 79 10-155ND
1,2,4-Trimethylbenzene ug/kg 20.522 93 24-154ND
1,2-Dibromo-3-chloropropane ug/kg 19.5 v1228933-158ND
1,2-Dibromoethane (EDB)ug/kg 17.222 78 40-136ND
1,2-Dichlorobenzene ug/kg 19.022 87 27-146ND
1,2-Dichloroethane ug/kg 17.222 78 49-140ND
1,2-Dichloropropane ug/kg 20.022 92 44-143ND
1,3,5-Trimethylbenzene ug/kg 20.722 95 40-144ND
1,3-Dichlorobenzene ug/kg 19.222 88 33-140ND
1,3-Dichloropropane ug/kg 16.822 77 47-147ND
1,4-Dichlorobenzene ug/kg 18.722 85 35-139ND
2,2-Dichloropropane ug/kg 18.722 85 41-140ND
2-Butanone (MEK)ug/kg 35.3J43.8 71 10-181ND
2-Chlorotoluene ug/kg 19.122 87 38-147ND
2-Hexanone ug/kg 31.2J43.8 71 18-169ND
4-Chlorotoluene ug/kg 19.222 87 36-145ND
4-Methyl-2-pentanone (MIBK)ug/kg 35.2J43.8 80 16-175ND
Acetone ug/kg 96.4J43.8 76 10-20063.0J
Benzene ug/kg 19.922 91 46-136ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2863268MATRIX SPIKE SAMPLE:
MSSpike
Result
92473782002
Bromobenzene ug/kg 20.822 95 38-149ND
Bromochloromethane ug/kg 18.922 86 44-142ND
Bromodichloromethane ug/kg 18.922 87 41-140ND
Bromoform ug/kg 16.922 77 34-145ND
Bromomethane ug/kg 28.4 IH2212914-162ND
Carbon tetrachloride ug/kg 23.622 108 44-141ND
Chlorobenzene ug/kg 19.422 88 39-141ND
Chloroethane ug/kg 26.622 121 10-182ND
Chloroform ug/kg 18.522 84 45-140ND
Chloromethane ug/kg 18.822 86 19-149ND
cis-1,2-Dichloroethene ug/kg 19.122 87 38-150ND
cis-1,3-Dichloropropene ug/kg 17.422 79 30-144ND
Dibromochloromethane ug/kg 17.722 81 36-145ND
Dibromomethane ug/kg 18.222 83 41-145ND
Dichlorodifluoromethane ug/kg 20.6 v3229416-146ND
Diisopropyl ether ug/kg 18.022 82 41-143ND
Ethylbenzene ug/kg 19.322 88 35-144ND
Hexachloro-1,3-butadiene ug/kg 22.022 100 10-160ND
Isopropylbenzene (Cumene)ug/kg 20.022 91 30-152ND
m&p-Xylene ug/kg 38.743.8 88 33-145ND
Methyl-tert-butyl ether ug/kg 15.022 68 49-140ND
Methylene Chloride ug/kg 23.6 v12210810-174ND
n-Butylbenzene ug/kg 19.622 89 10-160ND
n-Propylbenzene ug/kg 20.522 93 24-159ND
Naphthalene ug/kg 17.722 81 10-171ND
o-Xylene ug/kg 18.622 85 31-150ND
p-Isopropyltoluene ug/kg 21.522 98 21-154ND
sec-Butylbenzene ug/kg 20.722 94 19-159ND
Styrene ug/kg 18.022 82 15-152ND
tert-Butylbenzene ug/kg 19.322 88 31-141ND
Tetrachloroethene ug/kg 18.822 86 19-141ND
Toluene ug/kg 20.022 91 31-146ND
trans-1,2-Dichloroethene ug/kg 20.222 92 28-157ND
trans-1,3-Dichloropropene ug/kg 16.422 75 25-146ND
Trichloroethene ug/kg 22.122 101 34-149ND
Trichlorofluoromethane ug/kg 23.322 106 10-167ND
Vinyl acetate ug/kg ND43.8 35 10-200ND
Vinyl chloride ug/kg 22.7 v32210436-155ND
Xylene (Total)ug/kg 57.365.8 87 29-148ND
1,2-Dichloroethane-d4 (S)%93 70-132
4-Bromofluorobenzene (S)%92 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473782001
2863267SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND v130ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg 13.6J 30ND
Acetone ug/kg 15.9J 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IH30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND v230ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473782001
2863267SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND v130ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND v230ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9598
4-Bromofluorobenzene (S)%110106
Toluene-d8 (S)%105101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
536636
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2862449
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 328 04/17/20 08:2275.1
1,2-Dichlorobenzene ug/kg ND 328 04/17/20 08:2270.9
1,3-Dichlorobenzene ug/kg ND 328 04/17/20 08:2273.8
1,4-Dichlorobenzene ug/kg ND 328 04/17/20 08:2272.1
1-Methylnaphthalene ug/kg ND 328 04/17/20 08:2287.3
2,2'-Oxybis(1-chloropropane)ug/kg ND 328 04/17/20 08:2291.1
2,4,5-Trichlorophenol ug/kg ND 328 04/17/20 08:2285.1
2,4,6-Trichlorophenol ug/kg ND 328 04/17/20 08:2282.4
2,4-Dichlorophenol ug/kg ND 328 04/17/20 08:22108
2,4-Dimethylphenol ug/kg ND 328 04/17/20 08:2281.7
2,4-Dinitrophenol ug/kg ND 1640 04/17/20 08:221050
2,4-Dinitrotoluene ug/kg ND 328 04/17/20 08:2286.8
2,6-Dinitrotoluene ug/kg ND 328 04/17/20 08:2285.7
2-Chloronaphthalene ug/kg ND 328 04/17/20 08:2273.0
2-Chlorophenol ug/kg ND 328 04/17/20 08:2276.3
2-Methylnaphthalene ug/kg ND 328 04/17/20 08:2283.4
2-Methylphenol(o-Cresol)ug/kg ND 328 04/17/20 08:2272.6
2-Nitroaniline ug/kg ND 1640 04/17/20 08:22165
2-Nitrophenol ug/kg ND 328 04/17/20 08:22101
3&4-Methylphenol(m&p Cresol)ug/kg ND 328 04/17/20 08:2282.5
3,3'-Dichlorobenzidine ug/kg ND 656 04/17/20 08:22228
3-Nitroaniline ug/kg ND 1640 04/17/20 08:22174
4,6-Dinitro-2-methylphenol ug/kg ND 656 04/17/20 08:22528
4-Bromophenylphenyl ether ug/kg ND 328 04/17/20 08:2286.0
4-Chloro-3-methylphenol ug/kg ND 656 04/17/20 08:22200
4-Chloroaniline ug/kg ND 656 04/17/20 08:22201
4-Chlorophenylphenyl ether ug/kg ND 328 04/17/20 08:2285.1
4-Nitroaniline ug/kg ND 656 04/17/20 08:22162
4-Nitrophenol ug/kg ND 1640 04/17/20 08:22523
Acenaphthene ug/kg ND 328 04/17/20 08:2284.3
Acenaphthylene ug/kg ND 328 04/17/20 08:2277.6
Aniline ug/kg ND 328 04/17/20 08:2273.6
Anthracene ug/kg ND 328 04/17/20 08:2285.0
Benzo(a)anthracene ug/kg ND 328 04/17/20 08:22104
Benzo(a)pyrene ug/kg ND 328 04/17/20 08:22142
Benzo(b)fluoranthene ug/kg ND 328 04/17/20 08:22132
Benzo(g,h,i)perylene ug/kg ND 328 04/17/20 08:22128
Benzo(k)fluoranthene ug/kg ND 328 04/17/20 08:22138
Benzoic Acid ug/kg ND 1640 04/17/20 08:22354
Benzyl alcohol ug/kg ND 656 04/17/20 08:22174
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2862449
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 328 04/17/20 08:2287.5
bis(2-Chloroethyl) ether ug/kg ND 328 04/17/20 08:2269.6
bis(2-Ethylhexyl)phthalate ug/kg ND 328 04/17/20 08:22107
Butylbenzylphthalate ug/kg ND 328 04/17/20 08:2287.3
Chrysene ug/kg ND 328 04/17/20 08:2295.2
Di-n-butylphthalate ug/kg ND 328 04/17/20 08:2280.9
Di-n-octylphthalate ug/kg ND 328 04/17/20 08:22187
Dibenz(a,h)anthracene ug/kg ND 328 04/17/20 08:22131
Dibenzofuran ug/kg ND 328 04/17/20 08:2282.0
Diethylphthalate ug/kg ND 328 04/17/20 08:2271.1
Dimethylphthalate ug/kg ND 328 04/17/20 08:2274.1
Fluoranthene ug/kg ND 328 04/17/20 08:2299.0
Fluorene ug/kg ND 328 04/17/20 08:2287.7
Hexachloro-1,3-butadiene ug/kg ND 328 04/17/20 08:2279.7
Hexachlorobenzene ug/kg ND 328 04/17/20 08:2283.2
Hexachlorocyclopentadiene ug/kg ND 328 04/17/20 08:22131
Hexachloroethane ug/kg ND 328 04/17/20 08:2274.7
Indeno(1,2,3-cd)pyrene ug/kg ND 328 04/17/20 08:22150
Isophorone ug/kg ND 328 04/17/20 08:2271.2
N-Nitroso-di-n-propylamine ug/kg ND 328 04/17/20 08:2291.8
N-Nitrosodimethylamine ug/kg ND 328 04/17/20 08:2292.2
N-Nitrosodiphenylamine ug/kg ND 328 04/17/20 08:2283.6
Naphthalene ug/kg ND 328 04/17/20 08:2278.5
Nitrobenzene ug/kg ND 328 04/17/20 08:2278.3
Pentachlorophenol ug/kg ND 656 04/17/20 08:22150
Phenanthrene ug/kg ND 328 04/17/20 08:2282.5
Phenol ug/kg ND 328 04/17/20 08:2278.3
Pyrene ug/kg ND 328 04/17/20 08:2290.2
Pyridine ug/kg ND 328 04/17/20 08:2282.9
2,4,6-Tribromophenol (S)%69 27-110 04/17/20 08:22
2-Fluorobiphenyl (S)%70 30-110 04/17/20 08:22
2-Fluorophenol (S)%67 13-110 04/17/20 08:22
Nitrobenzene-d5 (S)%69 23-110 04/17/20 08:22
Phenol-d6 (S)%67 22-110 04/17/20 08:22
Terphenyl-d14 (S)%87 28-110 04/17/20 08:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2862450LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 14701690 87 52-130
1,2-Dichlorobenzene ug/kg 14301690 84 51-130
1,3-Dichlorobenzene ug/kg 14401690 85 50-130
1,4-Dichlorobenzene ug/kg 15201690 89 49-130
1-Methylnaphthalene ug/kg 14001690 83 55-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2862450LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 13801690 81 30-130
2,4,5-Trichlorophenol ug/kg 16101690 95 55-130
2,4,6-Trichlorophenol ug/kg 15601690 92 57-130
2,4-Dichlorophenol ug/kg 15101690 89 56-130
2,4-Dimethylphenol ug/kg 14801690 87 51-130
2,4-Dinitrophenol ug/kg 74508470 88 27-133
2,4-Dinitrotoluene ug/kg 15701690 92 61-130
2,6-Dinitrotoluene ug/kg 16301690 96 60-130
2-Chloronaphthalene ug/kg 15901690 94 52-130
2-Chlorophenol ug/kg 14701690 87 54-130
2-Methylnaphthalene ug/kg 14601690 86 54-130
2-Methylphenol(o-Cresol)ug/kg 14501690 86 51-130
2-Nitroaniline ug/kg 30103390 89 51-130
2-Nitrophenol ug/kg 14501690 85 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 14601690 86 11-163
3,3'-Dichlorobenzidine ug/kg 27903390 82 10-132
3-Nitroaniline ug/kg 27303390 81 55-130
4,6-Dinitro-2-methylphenol ug/kg 32103390 95 47-142
4-Bromophenylphenyl ether ug/kg 16201690 95 59-130
4-Chloro-3-methylphenol ug/kg 29303390 87 55-130
4-Chloroaniline ug/kg 29003390 85 54-130
4-Chlorophenylphenyl ether ug/kg 15201690 89 58-130
4-Nitroaniline ug/kg 28403390 84 54-130
4-Nitrophenol ug/kg 75508470 89 48-130
Acenaphthene ug/kg 15701690 92 60-130
Acenaphthylene ug/kg 16101690 95 60-130
Aniline ug/kg 13801690 81 43-130
Anthracene ug/kg 16101690 95 63-130
Benzo(a)anthracene ug/kg 16301690 96 59-130
Benzo(a)pyrene ug/kg 16401690 97 57-130
Benzo(b)fluoranthene ug/kg 16001690 94 54-130
Benzo(g,h,i)perylene ug/kg 18701690 111 59-130
Benzo(k)fluoranthene ug/kg 16701690 98 54-130
Benzoic Acid ug/kg 64608470 76 19-130
Benzyl alcohol ug/kg 28703390 85 50-130
bis(2-Chloroethoxy)methane ug/kg 14001690 83 54-130
bis(2-Chloroethyl) ether ug/kg 13901690 82 48-130
bis(2-Ethylhexyl)phthalate ug/kg 18501690 109 45-134
Butylbenzylphthalate ug/kg 18501690 109 46-138
Chrysene ug/kg 16301690 96 58-130
Di-n-butylphthalate ug/kg 16201690 96 60-130
Di-n-octylphthalate ug/kg 17301690 102 53-130
Dibenz(a,h)anthracene ug/kg 18501690 109 59-130
Dibenzofuran ug/kg 15501690 91 60-130
Diethylphthalate ug/kg 16201690 95 60-130
Dimethylphthalate ug/kg 16001690 95 60-130
Fluoranthene ug/kg 14901690 88 65-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2862450LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 15401690 91 63-130
Hexachloro-1,3-butadiene ug/kg 14501690 86 46-130
Hexachlorobenzene ug/kg 16501690 97 58-130
Hexachlorocyclopentadiene ug/kg 14101690 83 23-130
Hexachloroethane ug/kg 14101690 83 47-130
Indeno(1,2,3-cd)pyrene ug/kg 17901690 105 60-130
Isophorone ug/kg 14501690 85 49-130
N-Nitroso-di-n-propylamine ug/kg 14401690 85 47-130
N-Nitrosodimethylamine ug/kg 14601690 86 45-130
N-Nitrosodiphenylamine ug/kg 17001690 100 59-130
Naphthalene ug/kg 14601690 86 55-130
Nitrobenzene ug/kg 14801690 87 49-130
Pentachlorophenol ug/kg 32203390 95 10-132
Phenanthrene ug/kg 16401690 97 62-130
Phenol ug/kg 14801690 87 46-130
Pyrene ug/kg 19401690 114 53-130
Pyridine ug/kg 12301690 73 37-130
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%82 30-110
2-Fluorophenol (S)%80 13-110
Nitrobenzene-d5 (S)%76 23-110
Phenol-d6 (S)%80 22-110
Terphenyl-d14 (S)%99 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2862451MATRIX SPIKE SAMPLE:
MSSpike
Result
92473346014
1,2,4-Trichlorobenzene ug/kg 14901930 77 18-130ND
1,2-Dichlorobenzene ug/kg 15101930 78 14-130ND
1,3-Dichlorobenzene ug/kg 15101930 78 12-130ND
1,4-Dichlorobenzene ug/kg 15801930 82 10-130ND
1-Methylnaphthalene ug/kg 14401930 74 12-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 14801930 77 10-130ND
2,4,5-Trichlorophenol ug/kg 17601930 91 13-130ND
2,4,6-Trichlorophenol ug/kg 16901930 88 17-130ND
2,4-Dichlorophenol ug/kg 16701930 86 10-130ND
2,4-Dimethylphenol ug/kg 15501930 80 10-130ND
2,4-Dinitrophenol ug/kg 86609670 90 10-130ND
2,4-Dinitrotoluene ug/kg 17101930 89 24-130ND
2,6-Dinitrotoluene ug/kg 17401930 90 23-130ND
2-Chloronaphthalene ug/kg 15601930 81 19-130ND
2-Chlorophenol ug/kg 15901930 82 10-130ND
2-Methylnaphthalene ug/kg 15001930 77 18-130ND
2-Methylphenol(o-Cresol)ug/kg 16001930 83 10-130ND
2-Nitroaniline ug/kg 32703860 84 17-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2862451MATRIX SPIKE SAMPLE:
MSSpike
Result
92473346014
2-Nitrophenol ug/kg 15701930 81 10-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 16301930 84 10-130ND
3,3'-Dichlorobenzidine ug/kg 2710 IS38607010-130ND
3-Nitroaniline ug/kg 30203860 78 24-130ND
4,6-Dinitro-2-methylphenol ug/kg 36503860 94 10-152ND
4-Bromophenylphenyl ether ug/kg 15701930 81 29-130ND
4-Chloro-3-methylphenol ug/kg 33703860 87 17-130ND
4-Chloroaniline ug/kg 31003860 80 14-130ND
4-Chlorophenylphenyl ether ug/kg 15001930 78 25-130ND
4-Nitroaniline ug/kg 31003860 80 22-130ND
4-Nitrophenol ug/kg 82209670 85 10-130ND
Acenaphthene ug/kg 15401930 80 20-130ND
Acenaphthylene ug/kg 15701930 81 25-130ND
Aniline ug/kg 13001930 67 10-130ND
Anthracene ug/kg 15701930 81 29-130ND
Benzo(a)anthracene ug/kg 1530 IS19307919-130ND
Benzo(a)pyrene ug/kg 14701930 76 12-130ND
Benzo(b)fluoranthene ug/kg 14201930 73 14-130ND
Benzo(g,h,i)perylene ug/kg 15401930 79 10-130ND
Benzo(k)fluoranthene ug/kg 15301930 79 14-130ND
Benzoic Acid ug/kg 79909670 83 10-130ND
Benzyl alcohol ug/kg 32003860 83 13-130ND
bis(2-Chloroethoxy)methane ug/kg 15201930 78 16-130ND
bis(2-Chloroethyl) ether ug/kg 15201930 78 11-130ND
bis(2-Ethylhexyl)phthalate ug/kg 1870 IS19309721-130ND
Butylbenzylphthalate ug/kg 1920 IS19309923-130ND
Chrysene ug/kg 1580 IS19308222-130ND
Di-n-butylphthalate ug/kg 15301930 79 30-130ND
Di-n-octylphthalate ug/kg 1570 IS19308123-142ND
Dibenz(a,h)anthracene ug/kg 16001930 83 10-130ND
Dibenzofuran ug/kg 15401930 80 24-130ND
Diethylphthalate ug/kg 16801930 87 26-130ND
Dimethylphthalate ug/kg 17201930 89 22-130ND
Fluoranthene ug/kg 13301930 69 33-130ND
Fluorene ug/kg 15501930 80 22-130ND
Hexachloro-1,3-butadiene ug/kg 13601930 70 13-130ND
Hexachlorobenzene ug/kg 15501930 80 29-130ND
Hexachlorocyclopentadiene ug/kg 12601930 65 10-130ND
Hexachloroethane ug/kg 14501930 75 10-130ND
Indeno(1,2,3-cd)pyrene ug/kg 15201930 79 10-130ND
Isophorone ug/kg 15901930 82 13-130ND
N-Nitroso-di-n-propylamine ug/kg 15801930 82 12-130ND
N-Nitrosodimethylamine ug/kg 13401930 69 11-130ND
N-Nitrosodiphenylamine ug/kg 17401930 90 15-130ND
Naphthalene ug/kg 15301930 79 15-130ND
Nitrobenzene ug/kg 15801930 82 12-130ND
Pentachlorophenol ug/kg 34003860 88 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
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Huntersville, NC 28078
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Page 38 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2862451MATRIX SPIKE SAMPLE:
MSSpike
Result
92473346014
Phenanthrene ug/kg 15801930 82 27-130ND
Phenol ug/kg 15801930 82 10-130ND
Pyrene ug/kg 2010 IS193010419-130ND
Pyridine ug/kg 11101930 57 10-130ND
2,4,6-Tribromophenol (S)%82 27-110
2-Fluorobiphenyl (S)%66 30-110
2-Fluorophenol (S)%72 13-110
Nitrobenzene-d5 (S)%73 23-110
Phenol-d6 (S)%75 22-110
Terphenyl-d14 (S)%89 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473782001
2862452SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 39 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473782001
2862452SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6662
2-Fluorobiphenyl (S)%26 S028
2-Fluorophenol (S)%6462
Nitrobenzene-d5 (S)%6156
Phenol-d6 (S)%6765
Terphenyl-d14 (S)%7468
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
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Page 40 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
536540
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2861946
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
Aliphatic (C09-C18)mg/kg ND 10.0 N204/17/20 08:1510.0
Aliphatic (C19-C36)mg/kg ND 10.0 N204/17/20 08:1510.0
Aromatic (C11-C22)mg/kg ND 10.0 N204/17/20 08:1510.0
2-Bromonaphthalene (S)%101 40-140 04/17/20 08:15
2-Fluorobiphenyl (S)%99 40-140 04/17/20 08:15
Nonatriacontane (S)%66 40-140 04/17/20 08:15
o-Terphenyl (S)%67 40-140 04/17/20 08:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2861947LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2861948
Aliphatic (C09-C18)mg/kg ND N2104440-14055ND 50
Aliphatic (C19-C36)mg/kg ND N213.4 72 40-1408110.9 50
Aromatic (C11-C22)mg/kg 18.6 N228.4 65 40-1407922.8 20 50
2-Bromonaphthalene (S)%83 40-14094
2-Fluorobiphenyl (S)%82 40-14088
Nonatriacontane (S)%58 40-14063
o-Terphenyl (S)%69 40-14083
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
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Huntersville, NC 28078
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Page 41 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
536626
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92473782001, 92473782002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473797001
2862390SAMPLE DUPLICATE:
Percent Moisture %24.5 6 2526.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
2630973009
2862391SAMPLE DUPLICATE:
Percent Moisture %43.6 2 2544.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
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Huntersville, NC 28078
[phone]
Page 42 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
536632
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92473782003, 92473782004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473782003
2862428SAMPLE DUPLICATE:
Percent Moisture %30.8 0 2531.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92473841002
2862429SAMPLE DUPLICATE:
Percent Moisture %95.4 0 2595.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
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Huntersville, NC 28078
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Page 43 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1463205
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3520146-1
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
Total Solids %ND 04/20/20 07:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3520146-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1210056-01
R3520146-3SAMPLE DUPLICATE:
Total Solids %83.9 0.544 1084.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
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Huntersville, NC 28078
[phone]
Page 44 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1467046
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3522924-1
Associated Lab Samples:92473782001, 92473782002, 92473782003, 92473782004
Matrix:Solid
AnalyzedMDL
Total Solids %ND 04/28/20 11:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3522924-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1211458-01
R3522924-3SAMPLE DUPLICATE:
Total Solids %78.7 0.0992 1078.7
REPORT OF LABORATORY ANALYSIS
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Page 45 of 50
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The internal standard response is below criteria. Results may be biased high.IS
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 50
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92473782
GREENSBORO NC LC 0134 UST CLOS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92473782001 536540 536774W WALL MADEP EPH MADEP EPH
92473782002 536540 536774E WALL MADEP EPH MADEP EPH
92473782003 536540 536774S WALL MADEP EPH MADEP EPH
92473782004 536540 536774N WALL MADEP EPH MADEP EPH
92473782001 1462690 1462690W WALL MADEPV MADEP VPH
92473782002 1462690 1462690E WALL MADEPV MADEP VPH
92473782003 1462690 1462690S WALL MADEPV MADEP VPH
92473782004 1462690 1462690N WALL MADEPV MADEP VPH
92473782001 1466045 1466045W WALL 3050B EPA 6010D
92473782002 1466045 1466045E WALL 3050B EPA 6010D
92473782003 1466045 1466045S WALL 3050B EPA 6010D
92473782004 1466045 1466045N WALL 3050B EPA 6010D
92473782001 536636 536777W WALL EPA 3546 EPA 8270E
92473782002 536636 536777E WALL EPA 3546 EPA 8270E
92473782003 536636 536777S WALL EPA 3546 EPA 8270E
92473782004 536636 536777N WALL EPA 3546 EPA 8270E
92473782001 536822 536866W WALL EPA 5035A EPA 8260D
92473782002 536822 536866E WALL EPA 5035A EPA 8260D
92473782003 536822 536866S WALL EPA 5035A EPA 8260D
92473782004 536822 536866N WALL EPA 5035A EPA 8260D
92473782001 536626W WALL ASTM D2974-87
92473782002 536626E WALL ASTM D2974-87
92473782003 536632S WALL ASTM D2974-87
92473782004 536632N WALL ASTM D2974-87
92473782001 1463205 1463205W WALL SM 2540 G SM 2540G
92473782001 1467046 1467046W WALL SM 2540 G SM 2540G
92473782002 1463205 1463205E WALL SM 2540 G SM 2540G
92473782002 1467046 1467046E WALL SM 2540 G SM 2540G
92473782003 1463205 1463205S WALL SM 2540 G SM 2540G
92473782003 1467046 1467046S WALL SM 2540 G SM 2540G
92473782004 1463205 1463205N WALL SM 2540 G SM 2540G
92473782004 1467046 1467046N WALL SM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/29/2020 02:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 50
Page 48 of 50
Page 49 of 50
Page 50 of 50

APPENDIX E

WELL CONSTRUCTION DIAGRAM AND WELL CONSTRUCTION
RECORD
CIVIL & ENVIRONMENTAL CONSULTANTS, INC.
WELL CONSTRUCTION DETAIL
MONITORING
WELL NUMBER MW-1 MONITORING
WELL LOCATION
FIELD DATE STARTED 04/23/20
GEOLOGIST DATE COMPLETED 04/23/20
DEVELOPMENT
METHOD
DRILLING METHOD HAS NORTHING NA EASTING NA
GROUND SURFACE FLUSH MOUNTED WELL COMPLETION
TOP OF PVC; EQUIPPED WITH LOCKING EXPANDABLE CAP

CEMENT/GROUT
DEPTH TO TOP OF SEAL 4 FT
BENTONITE CHIPS
8-INCH DIAMETER BOREHOLE
2-INCH, SCHEDULE 40, THREADED FLUSH JOINTED
PVC CASING
DEPTH TO TOP OF SAND PACK 6 FT
DEPTH TO TOP OF WELL SCREEN 8 FT
COARSE SILICA SAND

2-INCH, SCHEDULE 40, THREADED, FLUSH
JOINTED PVC WELL SCREEN (0.01" SLOT SIZE)
2-INCH PVC THREADED DEPTH TO BOTTOM OF WELL SCREEN 18 FT
BOTTOM CAP DEPTH TO BOTTOM OF BORING 18 FT
217 Atwell Avenue
PROJECT NAME Ryder Greensboro
NC LC 0134 B. Barnes
PROJECT NUMBER DRILLER 3D ENVIRONMENTAL
CIVIL & ENVIRONMENTAL CONSULTANTS, INC.
WELL CONSTRUCTION DETAIL
MONITORING
WELL NUMBER MW-2 MONITORING
WELL LOCATION
FIELD DATE STARTED 04/23/20
GEOLOGIST DATE COMPLETED 04/23/20
DEVELOPMENT
METHOD
DRILLING METHOD HAS NORTHING NA EASTING NA
GROUND SURFACE FLUSH MOUNTED WELL COMPLETION
TOP OF PVC; EQUIPPED WITH LOCKING EXPANDABLE CAP

CEMENT/GROUT
DEPTH TO TOP OF SEAL 4 FT
BENTONITE CHIPS
8-INCH DIAMETER BOREHOLE
2-INCH, SCHEDULE 40, THREADED FLUSH JOINTED
PVC CASING
DEPTH TO TOP OF SAND PACK 6 FT
DEPTH TO TOP OF WELL SCREEN 8 FT
COARSE SILICA SAND

2-INCH, SCHEDULE 40, THREADED, FLUSH
JOINTED PVC WELL SCREEN (0.01" SLOT SIZE)
2-INCH PVC THREADED DEPTH TO BOTTOM OF WELL SCREEN 18 FT
BOTTOM CAP DEPTH TO BOTTOM OF BORING 18 FT
217 Atwell Avenue
PROJECT NAME Ryder Greensboro
NC LC 0134 B. Barnes
PROJECT NUMBER DRILLER 3D ENVIRONMENTAL