WS-3285_9846_CA_HRE_20230912_Results

North Carolina Department of Environmental Quality | Division of Waste Management
Winston-Salem Regional Office | 450 West Hanes Mill Road | Suite 300 | Winston-Salem,
NC 27105 | [phone]
September 12, 2023
Ms. Carla G. Duszlak
1211 May Court
Burlington, NC 27215
Re: Health Risk Evaluation of Water Supply
Tracking ID: #9846
Dear Ms. Nelson:
Please find attached the Sample Analytical Results for a water sample collected from your well, identified
as #8458, located at 1606 NC Highway 61 South, Whitsett, NC 27377, Guilford County, on May 17, 2023.
The sample was collected by Pyramid Environmental as part of a groundwater monitoring event and
analyzed by Waypoint Analytical. The water sample was analyzed for specific target analytes
(contaminants), which are listed on the attached Sample Analytical Results. Contaminants were detected
in the water sample, as shown on the attached Sample Analytical Results.
Because contaminants were detected in the water sample, a Health Risk Evaluation of the water supply
was performed by an environmental toxicologist in the Division of Waste Management. The Health Risk
Evaluation, which is attached also, compares the detected concentration of contaminants to acceptable
concentrations and provides a recommendation for safe use of the water.
If you have any questions, please contact Dave Lilley at [phone] or contact Gene Mao at the
Guilford County Department of Health and Human Services, 400 W. Market Street, Suite 300, North
Carolina 27401 and/or [phone].
Sincerely,
James W. Brown
Winston-Salem Regional Supervisor
UST Section, Division of Waste Management, NCDEQ
Attachments: Well Water Sample Analytical Results
Health Risk Evaluation
cc: Ms. Carla G. Duszlak, Water Supply Well Owner
Dr. Iulia Vann, Director, Guilford County Department of Public Health
Mr. Michael Halford, County Manager, Guilford County

September 12, 2023 TO: Gene Mao
Guilford County Department of Health and Human Services for
Winston-Salem Regional Office NC UST Section RE: Health Risk Evaluation
Incident # 9846
1606 NC Highway 61 South Well Sampling Results Whitsett, NC During this sampling event, one contaminant was detected in the well water. The standards used
to determine if the water is suitable for drinking and cooking are the United States Environmental
Protection Agency’s Maximum Contaminant Levels (MCLs) or, if no MCLs exist, North Carolina Groundwater Standards (2L). If the contaminant concentration exceeds the applicable standard for using the water for drinking
and cooking, the contaminant concentration is further analyzed to determine if the water is suitable for
other household uses, such as showering, bathing, washing dishes, flushing toilets, and hand washing. The chart below compares the detected contaminant concentration with the applicable standard: Sample ID Contaminant Concentration (µg/L) MCL (µg/L) 2L (µg/L)
96583 Chloroform 1.72 80*
µg/L – Stands for micrograms of contaminant per liter of water and is roughly equivalent to parts per billion. * As total trihalomethanes.
RECOMMENDATION: The detected contaminant did not exceed the applicable water standard. Therefore, no restrictions on the use of this water are recommended at this time.
David Lilley, Environmental Toxicologist
Division of Waste Management, NCDEQ
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27416-0265
23-139-0016
01168
Pyramid Environmental & Engineering, P.C.
PO Box 16265
Mika Trifunovic
Greensboro
Received : 05/19/2023
Taylor's Groc
Report Date : 05/30/2023
Sample ID :
Lab No :
Sampled:SW-3
96583 Matrix:
5/17/2023 15:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V33727 05/25/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 05/25/23 23:37 V33730MSA
<0.180 µg/L 0.180 0.500Benzene 1 05/25/23 23:37 V33730MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 05/25/23 23:37 V33730MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 05/25/23 23:37 V33730MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 05/25/23 23:37 V33730MSA
<1.50 µg/L 1.50 5.00Bromoform 1 05/25/23 23:37 V33730MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 05/25/23 23:37 V33730MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 05/25/23 23:37 V33730MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 05/25/23 23:37 V33730MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/25/23 23:37 V33730MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/25/23 23:37 V33730MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 05/25/23 23:37 V33730MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/25/23 23:37 V33730MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 05/25/23 23:37 V33730MSA
1.72 µg/L 0.220 0.500Chloroform 1 05/25/23 23:37 V33730MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 05/25/23 23:37 V33730MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/25/23 23:37 V33730MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/25/23 23:37 V33730MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 05/25/23 23:37 V33730MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/25/23 23:37 V33730MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 05/25/23 23:37 V33730MSA
<0.230 M µg/L 0.230 0.500Dibromomethane 1 05/25/23 23:37 V33730MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 23 of 41
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27416-0265
23-139-0016
01168
Pyramid Environmental & Engineering, P.C.
PO Box 16265
Mika Trifunovic
Greensboro
Received : 05/19/2023
Taylor's Groc
Report Date : 05/30/2023
Sample ID :
Lab No :
Sampled:SW-3
96583 Matrix:
5/17/2023 15:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V33727 05/25/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/25/23 23:37 V33730MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/25/23 23:37 V33730MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/25/23 23:37 V33730MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/25/23 23:37 V33730MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/25/23 23:37 V33730MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/25/23 23:37 V33730MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/25/23 23:37 V33730MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/25/23 23:37 V33730MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 05/25/23 23:37 V33730MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/25/23 23:37 V33730MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/25/23 23:37 V33730MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/25/23 23:37 V33730MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/25/23 23:37 V33730MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/25/23 23:37 V33730MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/25/23 23:37 V33730MSA
<42.0 µg/L 42.0 200
Ethanol 1 05/25/23 23:37 V33730MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 05/25/23 23:37 V33730MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 05/25/23 23:37 V33730MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 05/25/23 23:37 V33730MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 05/25/23 23:37 V33730MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 05/25/23 23:37 V33730MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/25/23 23:37 V33730MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 24 of 41
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27416-0265
23-139-0016
01168
Pyramid Environmental & Engineering, P.C.
PO Box 16265
Mika Trifunovic
Greensboro
Received : 05/19/2023
Taylor's Groc
Report Date : 05/30/2023
Sample ID :
Lab No :
Sampled:SW-3
96583 Matrix:
5/17/2023 15:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V33727 05/25/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 05/25/23 23:37 V33730MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 05/25/23 23:37 V33730MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 05/25/23 23:37 V33730MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 05/25/23 23:37 V33730MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 05/25/23 23:37 V33730MSA
<0.220 µg/L 0.220 0.500Styrene 1 05/25/23 23:37 V33730MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/25/23 23:37 V33730MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/25/23 23:37 V33730MSA
<0.220 µg/L 0.220 0.500
Tetrachloroethene 1 05/25/23 23:37 V33730MSA
<0.220 µg/L 0.220 0.500Toluene 1 05/25/23 23:37 V33730MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 05/25/23 23:37 V33730MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 05/25/23 23:37 V33730MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/25/23 23:37 V33730MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/25/23 23:37 V33730MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 05/25/23 23:37 V33730MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 05/25/23 23:37 V33730MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 05/25/23 23:37 V33730MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 05/25/23 23:37 V33730MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/25/23 23:37 V33730MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 05/25/23 23:37 V33730MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/25/23 23:37 V33730MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 05/25/23 23:37 V33730MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 25 of 41
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27416-0265
23-139-0016
01168
Pyramid Environmental & Engineering, P.C.
PO Box 16265
Mika Trifunovic
Greensboro
Received : 05/19/2023
Taylor's Groc
Report Date : 05/30/2023
Sample ID :
Lab No :
Sampled:SW-3
96583 Matrix:
5/17/2023 15:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V33727 05/25/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 05/25/23 23:37 V33730MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 05/25/23 23:37 V33730
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/24/23 03:561 MSA V33606
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%05/24/23 03:561 MSA V33606
Surrogate: 1,2-Dichloroethane - d4 99.6 Limits: 70-130%05/24/23 03:561 MSA V33606
Surrogate: Toluene-d8 100 Limits: 70-130%05/24/23 03:561 MSA V33606
Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%05/25/23 23:371 MSA V33730
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%05/25/23 23:371 MSA V33730
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%05/25/23 23:371 MSA V33730
Surrogate: Toluene-d8 96.4 Limits: 70-130%05/25/23 23:371 MSA V33730
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 26 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33606QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33605
Associated Lab Samples: 96579, 96580, 96581, 96582
LRB-V33605 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/23/23 23:5310.01.80<1.80µg/LAcetone
05/23/23 23:530.5000.180<0.180µg/LBenzene
05/23/23 23:530.5000.210<0.210µg/LBromobenzene
05/23/23 23:531.000.420<0.420µg/LBromochloromethane
05/23/23 23:530.5000.160<0.160µg/LBromodichloromethane
05/23/23 23:535.001.50<1.50µg/LBromoform
05/23/23 23:531.000.280<0.280µg/LBromomethane
05/23/23 23:530.5000.180<0.180µg/Ln-Butylbenzene
05/23/23 23:530.5000.200<0.200µg/Lsec-Butyl benzene
05/23/23 23:532.000.920<0.920µg/Ltert-Butyl benzene
05/23/23 23:530.5000.180<0.180µg/LCarbon Tetrachloride
05/23/23 23:530.5000.190<0.190µg/LChlorobenzene
05/23/23 23:530.5000.190<0.190µg/LChlorodibromomethane
05/23/23 23:531.000.430<0.430µg/LChloroethane
05/23/23 23:530.5000.220<0.220µg/LChloroform
05/23/23 23:530.5000.220<0.220µg/LChloromethane
05/23/23 23:530.5000.200<0.200µg/L2-Chlorotoluene
05/23/23 23:530.5000.200<0.200µg/L4-Chlorotoluene
05/23/23 23:530.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
05/23/23 23:532.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
05/23/23 23:530.5000.200<0.200µg/L1,2-Dibromoethane
05/23/23 23:530.5000.230<0.230µg/LDibromomethane
05/23/23 23:530.5000.220<0.220µg/L1,2-Dichlorobenzene
05/23/23 23:530.5000.190<0.190µg/L1,3-Dichlorobenzene
05/23/23 23:530.5000.210<0.210µg/L1,4-Dichlorobenzene
05/23/23 23:535.001.20<1.20µg/LDichlorodifluoromethane
05/23/23 23:530.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 13Date:05/30/2023 02:55 PM
Page 27 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33606QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33605
Associated Lab Samples: 96579, 96580, 96581, 96582
LRB-V33605 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/23/23 23:530.5000.150<0.150µg/L1,2-Dichloroethane
05/23/23 23:530.5000.150<0.150µg/L1,1-Dichloroethene
05/23/23 23:530.5000.200<0.200µg/Lcis-1,2-Dichloroethene
05/23/23 23:530.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
05/23/23 23:530.5000.190<0.190µg/L1,2-Dichloropropane
05/23/23 23:530.5000.130<0.130µg/L1,3-Dichloropropane
05/23/23 23:532.000.210<0.210µg/L2,2-Dichloropropane
05/23/23 23:530.5000.200<0.200µg/L1,1-Dichloropropene
05/23/23 23:530.5000.210<0.210µg/Lcis-1,3-Dichloropropene
05/23/23 23:530.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
05/23/23 23:5320042.0<42.0µg/LEthanol
05/23/23 23:530.5000.170<0.170µg/LEthylbenzene
05/23/23 23:533.000.350<0.350µg/LHexachlorobutadiene
05/23/23 23:531.000.380<0.380µg/L2-Hexanone
05/23/23 23:530.5000.180<0.180µg/LIsopropylbenzene
05/23/23 23:530.5000.089<0.089µg/L4-Isopropyl toluene
05/23/23 23:535.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
05/23/23 23:531.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
05/23/23 23:531.000.078<0.078µg/L4-Methyl-2-Pentanone
05/23/23 23:532.000.330<0.330µg/LMethylene Chloride
05/23/23 23:531.000.470<0.470µg/LNaphthalene
05/23/23 23:530.5000.190<0.190µg/Ln-Propylbenzene
05/23/23 23:530.5000.220<0.220µg/LStyrene
05/23/23 23:530.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
05/23/23 23:530.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
05/23/23 23:530.5000.220<0.220µg/LTetrachloroethene
05/23/23 23:530.5000.220<0.220µg/LToluene
Page 2 of 13Date:05/30/2023 02:55 PM
Page 28 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33606QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33605
Associated Lab Samples: 96579, 96580, 96581, 96582
LRB-V33605 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/23/23 23:530.5000.380<0.380µg/L1,2,3-Trichlorobenzene
05/23/23 23:530.5000.310<0.310µg/L1,2,4-Trichlorobenzene
05/23/23 23:530.5000.160<0.160µg/L1,1,1-Trichloroethane
05/23/23 23:530.5000.096<0.096µg/L1,1,2-Trichloroethane
05/23/23 23:530.5000.180<0.180µg/LTrichloroethene
05/23/23 23:530.5000.180<0.180µg/LTrichlorofluoromethane
05/23/23 23:530.5000.270<0.270µg/L1,2,3-Trichloropropane
05/23/23 23:530.5000.190<0.190µg/L1,2,4-Trimethylbenzene
05/23/23 23:530.5000.180<0.180µg/L1,3,5-Trimethylbenzene
05/23/23 23:535.001.00<1.00µg/LVinyl Acetate
05/23/23 23:530.5000.170<0.170µg/LVinyl Chloride
05/23/23 23:530.5000.210<0.210µg/Lo-Xylene
05/23/23 23:531.000.420<0.420µg/Lm,p-Xylene
05/23/23 23:534-Bromofluorobenzene (S)98.8 70-130
05/23/23 23:53Dibromofluoromethane (S)99.2 70-130
05/23/23 23:531,2-Dichloroethane - d4 (S)98.0 70-130
05/23/23 23:53Toluene-d8 (S)101 70-130
LCS-V33605 LCSD-V33605Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.6 81.584.033.640.0µg/LAcetone 40-160 3.0 20.0
18.3 91.595.519.120.0µg/LBenzene 70-130 4.2 20.0
18.1 90.594.018.820.0µg/LBromobenzene 70-130 3.7 20.0
20.1 10110320.520.0µg/LBromochloromethane 70-130 1.9 20.0
17.9 89.591.518.320.0µg/LBromodichloromethane 70-130 2.2 20.0
Page 3 of 13Date:05/30/2023 02:55 PM
Page 29 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33606QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33605
LCS-V33605 LCSD-V33605Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.3 91.591.518.320.0µg/LBromoform 70-130 0.0 20.0
22.9 11511723.420.0µg/LBromomethane 60-140 2.1 20.0
18.3 91.598.519.720.0µg/Ln-Butylbenzene 70-130 7.3 20.0
17.8 89.095.019.020.0µg/Lsec-Butyl benzene 70-130 6.5 20.0
18.1 90.595.519.120.0µg/Ltert-Butyl benzene 70-130 5.3 20.0
19.6 98.010020.020.0µg/LCarbon Tetrachloride 70-130 2.0 20.0
18.2 91.094.018.820.0µg/LChlorobenzene 70-130 3.2 20.0
18.5 92.594.018.820.0µg/LChlorodibromomethane 70-130 1.6 20.0
20.7 10411122.120.0µg/LChloroethane 60-140 6.5 20.0
19.0 95.096.519.320.0µg/LChloroform 70-130 1.5 20.0
18.9 94.596.019.220.0µg/LChloromethane 60-140 1.5 20.0
18.1 90.595.019.020.0µg/L2-Chlorotoluene 70-130 4.8 20.0
18.3 91.597.019.420.0µg/L4-Chlorotoluene 70-130 5.8 20.0
18.4 92.092.518.520.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.5 20.0
18.4 92.010220.420.0µg/L1,2-Dibromo-3-Chloropropane 70-130 10.3 20.0
18.8 94.095.519.120.0µg/L1,2-Dibromoethane 70-130 1.5 20.0
18.4 92.094.518.920.0µg/LDibromomethane 70-130 2.6 20.0
18.7 93.598.019.620.0µg/L1,2-Dichlorobenzene 70-130 4.6 20.0
18.2 91.097.519.520.0µg/L1,3-Dichlorobenzene 70-130 6.8 20.0
18.7 93.598.019.620.0µg/L1,4-Dichlorobenzene 70-130 4.6 20.0
16.3 81.589.017.820.0µg/LDichlorodifluoromethane 60-140 8.7 20.0
19.0 95.098.519.720.0µg/L1,1-Dichloroethane 70-130 3.6 20.0
20.1 10110020.020.0µg/L1,2-Dichloroethane 70-130 0.4 20.0
18.7 93.596.519.320.0µg/L1,1-Dichloroethene 70-130 3.1 20.0
19.8 99.010120.120.0µg/Lcis-1,2-Dichloroethene 70-130 1.5 20.0
18.6 93.099.019.820.0µg/Ltrans-1,2-Dichloroethene 70-130 6.2 20.0
Page 4 of 13Date:05/30/2023 02:55 PM
Page 30 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33606QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33605
LCS-V33605 LCSD-V33605Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.6 93.094.518.920.0µg/L1,2-Dichloropropane 70-130 1.6 20.0
18.3 91.595.519.120.0µg/L1,3-Dichloropropane 70-130 4.2 20.0
18.7 93.598.519.720.0µg/L2,2-Dichloropropane 70-130 5.2 20.0
19.8 99.010420.720.0µg/L1,1-Dichloropropene 70-130 4.4 20.0
18.6 93.097.519.520.0µg/Lcis-1,3-Dichloropropene 70-130 4.7 20.0
18.5 92.598.019.620.0µg/Ltrans-1,3-Dichloropropene 70-130 5.7 20.0
441 88.2101507500µg/LEthanol 60-140 13.9 20.0
18.9 94.598.019.620.0µg/LEthylbenzene 70-130 3.6 20.0
20.2 10111021.920.0µg/LHexachlorobutadiene 70-130 8.0 20.0
16.5 82.587.017.420.0µg/L2-Hexanone 60-140 5.3 20.0
18.8 94.098.019.620.0µg/LIsopropylbenzene 70-130 4.1 20.0
18.6 93.098.519.720.0µg/L4-Isopropyl toluene 70-130 5.7 20.0
17.7 88.586.017.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 2.8 20.0
18.7 93.593.018.620.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.5 20.0
17.7 88.590.018.020.0µg/L4-Methyl-2-Pentanone 60-140 1.6 20.0
18.9 94.597.019.420.0µg/LMethylene Chloride 70-130 2.6 20.0
19.9 99.510821.520.0µg/LNaphthalene 70-130 7.7 20.0
18.2 91.096.019.220.0µg/Ln-Propylbenzene 70-130 5.3 20.0
18.9 94.593.018.620.0µg/LStyrene 70-130 1.6 20.0
19.2 96.098.019.620.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.0 20.0
18.3 91.593.018.620.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.6 20.0
18.1 90.596.019.220.0µg/LTetrachloroethene 70-130 5.8 20.0
18.2 91.094.518.920.0µg/LToluene 70-130 3.7 20.0
22.0 11012124.120.0µg/L1,2,3-Trichlorobenzene 70-130 9.1 20.0
19.3 96.510020.020.0µg/L1,2,4-Trichlorobenzene 70-130 3.5 20.0
18.3 91.595.019.020.0µg/L1,1,1-Trichloroethane 70-130 3.7 20.0
Page 5 of 13Date:05/30/2023 02:55 PM
Page 31 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33606QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33605
LCS-V33605 LCSD-V33605Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.9 94.596.019.220.0µg/L1,1,2-Trichloroethane 70-130 1.5 20.0
19.2 96.010020.020.0µg/LTrichloroethene 70-130 4.0 20.0
18.3 91.596.519.320.0µg/LTrichlorofluoromethane 60-140 5.3 20.0
18.2 91.092.018.420.0µg/L1,2,3-Trichloropropane 70-130 1.0 20.0
18.6 93.097.019.420.0µg/L1,2,4-Trimethylbenzene 70-130 4.2 20.0
18.7 93.598.019.620.0µg/L1,3,5-Trimethylbenzene 70-130 4.6 20.0
21.6 10811021.920.0µg/LVinyl Acetate 60-140 1.3 20.0
18.7 93.599.519.920.0µg/LVinyl Chloride 60-140 6.2 20.0
18.6 93.094.518.920.0µg/Lo-Xylene 70-130 1.6 20.0
37.6 94.097.539.040.0µg/Lm,p-Xylene 70-130 3.6 20.0
1001014-Bromofluorobenzene (S)70-130
99.298.2Dibromofluoromethane (S)70-130
1011011,2-Dichloroethane - d4 (S)70-130
10199.6Toluene-d8 (S)70-130
Page 6 of 13Date:05/30/2023 02:55 PM
Page 32 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33670QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33669
Associated Lab Samples: 96580, 96582
LRB-V33669 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/24/23 14:550.5000.170<0.170µg/LEthylbenzene
05/24/23 14:550.5000.220<0.220µg/LToluene
05/24/23 14:550.5000.190<0.190µg/L1,2,4-Trimethylbenzene
05/24/23 14:550.5000.210<0.210µg/Lo-Xylene
05/24/23 14:551.000.420<0.420µg/Lm,p-Xylene
05/24/23 14:554-Bromofluorobenzene (S)103 70-130
05/24/23 14:55Dibromofluoromethane (S)99.4 70-130
05/24/23 14:551,2-Dichloroethane - d4 (S)106 70-130
05/24/23 14:55Toluene-d8 (S)101 70-130
LCS-V33669 LCSD-V33669Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.0 90.093.518.720.0µg/LEthylbenzene 70-130 3.8 20.0
17.6 88.090.018.020.0µg/LToluene 70-130 2.2 20.0
17.4 87.090.518.120.0µg/L1,2,4-Trimethylbenzene 70-130 3.9 20.0
17.4 87.090.018.020.0µg/Lo-Xylene 70-130 3.3 20.0
35.4 88.592.236.940.0µg/Lm,p-Xylene 70-130 4.1 20.0
99.299.04-Bromofluorobenzene (S)70-130
101101Dibromofluoromethane (S)70-130
1071081,2-Dichloroethane - d4 (S)70-130
99.8101Toluene-d8 (S)70-130
Page 7 of 13Date:05/30/2023 02:55 PM
Page 33 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33730QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33727
Associated Lab Samples: 96583
LRB-V33727 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/25/23 22:1310.01.80<1.80µg/LAcetone
05/25/23 22:130.5000.180<0.180µg/LBenzene
05/25/23 22:130.5000.210<0.210µg/LBromobenzene
05/25/23 22:131.000.420<0.420µg/LBromochloromethane
05/25/23 22:130.5000.160<0.160µg/LBromodichloromethane
05/25/23 22:135.001.50<1.50µg/LBromoform
05/25/23 22:131.000.280<0.280µg/LBromomethane
05/25/23 22:130.5000.180<0.180µg/Ln-Butylbenzene
05/25/23 22:130.5000.200<0.200µg/Lsec-Butyl benzene
05/25/23 22:132.000.920<0.920µg/Ltert-Butyl benzene
05/25/23 22:130.5000.180<0.180µg/LCarbon Tetrachloride
05/25/23 22:130.5000.190<0.190µg/LChlorobenzene
05/25/23 22:130.5000.190<0.190µg/LChlorodibromomethane
05/25/23 22:131.000.430<0.430µg/LChloroethane
05/25/23 22:130.5000.220<0.220µg/LChloroform
05/25/23 22:130.5000.220<0.220µg/LChloromethane
05/25/23 22:130.5000.200<0.200µg/L2-Chlorotoluene
05/25/23 22:130.5000.200<0.200µg/L4-Chlorotoluene
05/25/23 22:130.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
05/25/23 22:132.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
05/25/23 22:130.5000.200<0.200µg/L1,2-Dibromoethane
05/25/23 22:130.5000.230<0.230µg/LDibromomethane
05/25/23 22:130.5000.220<0.220µg/L1,2-Dichlorobenzene
05/25/23 22:130.5000.190<0.190µg/L1,3-Dichlorobenzene
05/25/23 22:130.5000.210<0.210µg/L1,4-Dichlorobenzene
05/25/23 22:135.001.20<1.20µg/LDichlorodifluoromethane
05/25/23 22:130.5000.240<0.240µg/L1,1-Dichloroethane
Page 8 of 13Date:05/30/2023 02:55 PM
Page 34 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33730QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33727
Associated Lab Samples: 96583
LRB-V33727 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/25/23 22:130.5000.150<0.150µg/L1,2-Dichloroethane
05/25/23 22:130.5000.150<0.150µg/L1,1-Dichloroethene
05/25/23 22:130.5000.200<0.200µg/Lcis-1,2-Dichloroethene
05/25/23 22:130.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
05/25/23 22:130.5000.190<0.190µg/L1,2-Dichloropropane
05/25/23 22:130.5000.130<0.130µg/L1,3-Dichloropropane
05/25/23 22:132.000.210<0.210µg/L2,2-Dichloropropane
05/25/23 22:130.5000.200<0.200µg/L1,1-Dichloropropene
05/25/23 22:130.5000.210<0.210µg/Lcis-1,3-Dichloropropene
05/25/23 22:130.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
05/25/23 22:1320042.0<42.0µg/LEthanol
05/25/23 22:130.5000.170<0.170µg/LEthylbenzene
05/25/23 22:133.000.350<0.350µg/LHexachlorobutadiene
05/25/23 22:131.000.380<0.380µg/L2-Hexanone
05/25/23 22:130.5000.180<0.180µg/LIsopropylbenzene
05/25/23 22:130.5000.089<0.089µg/L4-Isopropyl toluene
05/25/23 22:135.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
05/25/23 22:131.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
05/25/23 22:131.000.078<0.078µg/L4-Methyl-2-Pentanone
05/25/23 22:132.000.330<0.330µg/LMethylene Chloride
05/25/23 22:131.000.470<0.470µg/LNaphthalene
05/25/23 22:130.5000.190<0.190µg/Ln-Propylbenzene
05/25/23 22:130.5000.220<0.220µg/LStyrene
05/25/23 22:130.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
05/25/23 22:130.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
05/25/23 22:130.5000.220<0.220µg/LTetrachloroethene
05/25/23 22:130.5000.220<0.220µg/LToluene
Page 9 of 13Date:05/30/2023 02:55 PM
Page 35 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33730QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33727
Associated Lab Samples: 96583
LRB-V33727 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/25/23 22:130.5000.380<0.380µg/L1,2,3-Trichlorobenzene
05/25/23 22:130.5000.310<0.310µg/L1,2,4-Trichlorobenzene
05/25/23 22:130.5000.160<0.160µg/L1,1,1-Trichloroethane
05/25/23 22:130.5000.096<0.096µg/L1,1,2-Trichloroethane
05/25/23 22:130.5000.180<0.180µg/LTrichloroethene
05/25/23 22:130.5000.180<0.180µg/LTrichlorofluoromethane
05/25/23 22:130.5000.270<0.270µg/L1,2,3-Trichloropropane
05/25/23 22:130.5000.190<0.190µg/L1,2,4-Trimethylbenzene
05/25/23 22:130.5000.180<0.180µg/L1,3,5-Trimethylbenzene
05/25/23 22:135.001.00<1.00µg/LVinyl Acetate
05/25/23 22:130.5000.170<0.170µg/LVinyl Chloride
05/25/23 22:130.5000.210<0.210µg/Lo-Xylene
05/25/23 22:131.000.420<0.420µg/Lm,p-Xylene
05/25/23 22:134-Bromofluorobenzene (S)107 70-130
05/25/23 22:13Dibromofluoromethane (S)96.0 70-130
05/25/23 22:131,2-Dichloroethane - d4 (S)99.4 70-130
05/25/23 22:13Toluene-d8 (S)100 70-130
LCS-V33727 LCSD-V33727Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
28.2 70.585.034.040.0µg/LAcetone 40-160 18.6 20.0
18.8 94.011122.220.0µg/LBenzene 70-130 16.5 20.0
19.6 98.010220.420.0µg/LBromobenzene 70-130 4.0 20.0
19.8 99.010621.120.0µg/LBromochloromethane 70-130 6.3 20.0
18.0 90.072.514.520.0µg/LBromodichloromethane 70-130 21.5*20.0
Page 10 of 13* QC Fail Date:05/30/2023 02:55 PM
Page 36 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33730QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33727
LCS-V33727 LCSD-V33727Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.2 96.095.519.120.0µg/LBromoform 70-130 0.5 20.0
20.9 10596.019.220.0µg/LBromomethane 60-140 8.4 20.0
18.9 94.593.018.620.0µg/Ln-Butylbenzene 70-130 1.6 20.0
17.3 86.587.517.520.0µg/Lsec-Butyl benzene 70-130 1.1 20.0
17.4 87.088.017.620.0µg/Ltert-Butyl benzene 70-130 1.1 20.0
20.1 10110220.320.0µg/LCarbon Tetrachloride 70-130 0.9 20.0
18.3 91.592.518.520.0µg/LChlorobenzene 70-130 1.0 20.0
19.2 96.010320.520.0µg/LChlorodibromomethane 70-130 6.5 20.0
23.6 11810220.420.0µg/LChloroethane 60-140 14.5 20.0
18.9 94.510821.620.0µg/LChloroform 70-130 13.3 20.0
20.2 10177.515.520.0µg/LChloromethane 60-140 26.3*20.0
18.6 93.096.519.320.0µg/L2-Chlorotoluene 70-130 3.6 20.0
20.0 10095.019.020.0µg/L4-Chlorotoluene 70-130 5.1 20.0
18.7 93.510821.620.0µg/LDi-Isopropyl Ether (DIPE)70-130 14.3 20.0
24.1 12112124.120.0µg/L1,2-Dibromo-3-Chloropropane 70-130 0.0 20.0
17.5 87.589.517.920.0µg/L1,2-Dibromoethane 70-130 2.2 20.0
18.7 93.568.5*13.720.0µg/LDibromomethane 70-130 30.8*20.0
20.7 10410521.020.0µg/L1,2-Dichlorobenzene 70-130 1.4 20.0
18.3 91.597.019.420.0µg/L1,3-Dichlorobenzene 70-130 5.8 20.0
19.5 97.599.519.920.0µg/L1,4-Dichlorobenzene 70-130 2.0 20.0
19.0 95.079.515.920.0µg/LDichlorodifluoromethane 60-140 17.7 20.0
18.5 92.510621.220.0µg/L1,1-Dichloroethane 70-130 13.6 20.0
18.2 91.095.019.020.0µg/L1,2-Dichloroethane 70-130 4.3 20.0
17.3 86.510420.820.0µg/L1,1-Dichloroethene 70-130 18.3 20.0
18.5 92.510921.720.0µg/Lcis-1,2-Dichloroethene 70-130 15.9 20.0
19.3 96.511122.120.0µg/Ltrans-1,2-Dichloroethene 70-130 13.5 20.0
Page 11 of 13* QC Fail Date:05/30/2023 02:55 PM
Page 37 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33730QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33727
LCS-V33727 LCSD-V33727Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.8 89.073.014.620.0µg/L1,2-Dichloropropane 70-130 19.7 20.0
16.7 83.588.517.720.0µg/L1,3-Dichloropropane 70-130 5.8 20.0
18.2 91.010621.220.0µg/L2,2-Dichloropropane 70-130 15.2 20.0
19.6 98.011522.920.0µg/L1,1-Dichloropropene 70-130 15.5 20.0
17.3 86.570.014.020.0µg/Lcis-1,3-Dichloropropene 70-130 21.0*20.0
19.0 95.074.014.820.0µg/Ltrans-1,3-Dichloropropene 70-130 24.8*20.0
456 91.2103515500µg/LEthanol 60-140 12.1 20.0
18.5 92.598.019.620.0µg/LEthylbenzene 70-130 5.7 20.0
22.0 11010120.220.0µg/LHexachlorobutadiene 70-130 8.5 20.0
16.7 83.582.016.420.0µg/L2-Hexanone 60-140 1.8 20.0
18.4 92.093.518.720.0µg/LIsopropylbenzene 70-130 1.6 20.0
17.9 89.592.518.520.0µg/L4-Isopropyl toluene 70-130 3.2 20.0
16.7 83.591.018.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 8.5 20.0
17.3 86.597.519.520.0µg/LMethyl tert-butyl ether (MTBE)70-130 11.9 20.0
17.8 89.074.514.920.0µg/L4-Methyl-2-Pentanone 60-140 17.7 20.0
18.4 92.010120.120.0µg/LMethylene Chloride 70-130 8.8 20.0
18.5 92.510220.420.0µg/LNaphthalene 70-130 9.7 20.0
17.8 89.093.018.620.0µg/Ln-Propylbenzene 70-130 4.3 20.0
18.9 94.591.018.220.0µg/LStyrene 70-130 3.7 20.0
16.7 83.593.518.720.0µg/L1,1,1,2-Tetrachloroethane 70-130 11.2 20.0
18.3 91.593.518.720.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.1 20.0
18.6 93.099.519.920.0µg/LTetrachloroethene 70-130 6.7 20.0
17.1 85.572.514.520.0µg/LToluene 70-130 16.4 20.0
22.0 11011723.320.0µg/L1,2,3-Trichlorobenzene 70-130 5.7 20.0
20.2 10110420.720.0µg/L1,2,4-Trichlorobenzene 70-130 2.4 20.0
18.6 93.010120.120.0µg/L1,1,1-Trichloroethane 70-130 7.7 20.0
Page 12 of 13* QC Fail Date:05/30/2023 02:55 PM
Page 38 of 41
Quality Control Data
23-139-0016Report No:
Project Description:
Client ID:Pyramid Environmental & Engineering, P.C.
Taylor's Groc
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V33730QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V33727
LCS-V33727 LCSD-V33727Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.5 97.579.015.820.0µg/L1,1,2-Trichloroethane 70-130 20.9*20.0
17.6 88.091.018.220.0µg/LTrichloroethene 70-130 3.3 20.0
19.9 99.587.517.520.0µg/LTrichlorofluoromethane 60-140 12.8 20.0
19.2 96.094.518.920.0µg/L1,2,3-Trichloropropane 70-130 1.5 20.0
17.4 87.088.017.620.0µg/L1,2,4-Trimethylbenzene 70-130 1.1 20.0
17.8 89.089.517.920.0µg/L1,3,5-Trimethylbenzene 70-130 0.5 20.0
22.1 11199.519.920.0µg/LVinyl Acetate 60-140 10.4 20.0
19.7 98.575.515.120.0µg/LVinyl Chloride 60-140 26.4*20.0
18.2 91.091.018.220.0µg/Lo-Xylene 70-130 0.0 20.0
38.3 95.799.239.740.0µg/Lm,p-Xylene 70-130 3.5 20.0
1021034-Bromofluorobenzene (S)70-130
98.2101Dibromofluoromethane (S)70-130
98.21001,2-Dichloroethane - d4 (S)70-130
101108Toluene-d8 (S)70-130
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Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-139-0016
Pyramid Environmental & Engineering, P.C.
01168
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.2C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:05/19/2023 13:00:40
Special precautions or instructions included?
Comments:
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